{{Adams | number = ML17009A183 | issue date = 12/14/2016 | title = Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey, Rev. 1, Appendix G: Certificates of Analysis (Coa 405235, 406240 and 405245), P | author name = | author affiliation = State of NY, Energy Research & Development Authority | addressee name = | addressee affiliation = NRC/NMSS, NRC/NRR | docket = 05000201, P00M-032 | license number = | contact person = | package number = ML17006A156 | document type = Environmental Monitoring Report | page count = 2696 }}

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{{#Wiki_filter:Appendix G: Certificates of Analysis (405235, 406240 and 405245) COA 405235 1§13

II Laboratories uuc :ai mmOOr <OOThe GEL Grow:p HWC PO eox :!-0712 Charlestllll, SC29417 2\14-0 Road Ctlactest<m. SC 29407 p 343.556.8171 F 843.7CG.1l73 October 04, 2016 Ms. Laurie Losey MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Re: Soil Radioisotopes Work Order: 405235

Dear Ms. Losey:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on September 06, 2016. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4422. Purchase Order: GELPlS-0894 Sincerely, Jake Crook Project Manager Chain of Custody: NYSERDA-29 and NYSERDA-31 Enclosures UllU U lllUI 11 IU U get com MJW Technical Services Soil Radioisotopes SDG: 405235 Table of Contents Case Narrative ...................................................................................... 1 Chain of Custody and Supporting Documentation ............................... 6 Data Review Qualifier Definitions ..................................................... 22 Radiological Analysis ......................................................................... 25 Case Narrative ............................................................................ 26 Sample Data Summary ............................................................. 102 Quality Control Summary ........................................................ 337 Alpha Spectroscopy Raw Data ................................................. 377 Continuing Calibration Data ........................................... 1004 Background and Efficiency Data .................................... 103 0 RAD Standards Traceability ........................................... 1946 Runlogs ........................................................................... 2020 Gamma Spectroscopy Raw Data ............................................ 2046 Continuing Calibration Data .......................................... .4783 Background and Efficiency Data ................................... .4 793 RAD Standards Traceability .......................................... .4922 Runlogs .. ; ..................................................................... ; .. 4947 Gas Flow Raw Data ............................................................ : ... 495.6 Continuing Calibration Data ................................ : .......... 5 026 Background and Efficiency Data .................................... 5047 RAD Standards Traceability ........................................... 5176 Runlogs ........................................................................... 5185 Liquid Scintillation Raw Data ................................................ 5194 Continuing Calibration Data ........................................... 5709 Background and Efficiency Data ..................................... 5752 RAD Standards Traceability ................................... , .. , .... 5761 Runlogs ........................................................................... 5785 Case Narrative .................................................................................... 26 Sample Data Summary ......................................... ...... .................... 102 Quality Control Summary .............................................................. :.337 Alpha Spectroscopy Raw Data ............... * ........................................ Continuing Calibration Data .......... : .................... : .. ; ................ 1004 Background and Efficiency Data ............................................ 1030 RAD Standards Traceability ................................................... 1946 Runlogs* ..................................................... ............................ 2020 Gamma Spectroscopy Raw Data .................................... .': .............. .2046 Continuing Calibration Data ... , .............................................. .4783 Background and Efficiency Data .. : ........ ; ............................... .4 793 RAD Standards Traceability ................. ; ................................. 4922 Runlogs .................................................................................... 4947 Gas Flow Raw Data ........................................................................ 4956 Continuing Calibration Data ................................................... 5026 Background and Efficiency Data ............................................ 5 04 7 RAD Standards Traceability ................................................... 5176 Runlogs ................................................................................... 5185 Liquid Scintillation Raw Data ........................................................ 5194 Continuing Calibration Data ................................................... 5709 Background and Efficiency Data ..................... ...................... 5752 RAD Standards Traceability ................................................... 5761 Runlogs ................................................................................... 5785 Case Narrative Page 1 of 5809 October 04, 2016 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary Case Narrative for MJW Technical Services SDG: 405235 Sample Receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on September 06, 2016 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample Identification The laboratory received the following samples: Laboratory ID Client ID 405235001 4.1.B.R. l.2 405235002 4.1.B.R. l.3 405235003 4.1.B.R. l .4 405235004 4.1.B.R.7.2 405235005 4.1.C.R. l .3 405235006 4.1.C.R.l.4 405235007 4.1.C.R.2.3 405235008 4.1.C.R.2.4 405235009 4.1.D.R. l.3 405235010 4.1.D.R. l .4 405235011 4.1.D.R.3.2 405235012 4.1.D.R.2.4 405235013 4.2A.R.2.3 405235014 4.2A.R.l.3 405235015 4.2A.R.l.4 405235016 4.2A.R.2.4 405235017 4.2A.R.3.2 405235018 4.2A.R.4.2 405235019 4.2B.R.2.4 405235020 4.2B.R.l.4 405235021 4.2B.R.2.3 405235022 4.2B.R.l.3 405235023 4.2B.R.l l.2 405235024 4.2B.R.2.2 405235025 4.2B.R.l.2 405235026 4.2C.R.l.3 405235027 4.2C.R.l.4 405235028 4.3.ARI.3 405235029 4.3.B.R.l.3 Page 2 of 5 809 405235030 4.3A.R.2.3 405235031 4.3.BR19.2 405235032 4.3B.R.3.3 405235033 4.3B.R.3.4 405235034 4.3.B.R.1.4 405235035 .4.3B.R.2.3 405235036 4.3B.R.2.4 405235037 4.4C.R.2.4 405235038 4.4C.R.l.3 405235039 4.4C.R.1.4 405235040 4.4D.R.1.3 405235041 4.4D.R.1.4 405235042 4.4D.R.2.3 405235043 4.4D.R.2.4 405235044 4.4D.R.4.2 405235045 4.4D.R.5.2 405235046 4.SA.R.1.3 405235047 4.SA.R.1.4 405235048 4.5B.R.1.2 405235049 4.5B.R.1.3 405235050 4.5B.R.1.4 405235051 4.5B.R.2.3 405235052 4.5B.R.2.4 405235053 4.5C.R.5.2 405235054 4.5C.R.l.3 405235055 4.5C.R.1.4 405235056 4.5C.R.2.2 405235057 4.5C.R.2.3 405235058 4.SC.R.2.4 405235059 5.IA.R.1.2 405235060 5.lA.R.1.3 405235061 5.lB.R.2.2 405235062 5 .2.A.R.1.2 405235063 5.2.A.R.1.3 405235064 5.2.A.R.1.4 405235065 5.2A.R.2.3 405235066 5.2.A.R.2.4 405235067 5.2A.R.6.2 405235068 5.2A.R.4.2 405235069 5.2.B.R.1.4 405235070 5.2.B.R.3.2 405235071 5.2.B.R.4.2 405235072 5.2.B.R.2.4 405235073 5.2.B.R.8.2 405235074 5 .3 .A.R.1.3 405235075 5.4A.R.l.3 405235076 5.4A.R.4.2 405235077 5.5A.R.l.3 405235078 5.6A.R.l.3 Case Narrative Page 3 of 5809 Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Data Package The enclosed data package contains the following sections: General Narrative, Chain of Custody and Supporting Documentation, and data from the following fractions: Radiochemistry. Page 4 of 5809 Jake Crook Project Manager List of current GEL Certifications as of 04 October 2016 State Certification Alaska UST-0110 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 Delaware SC00012 DoD ELAP/IS017025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283,P330-15-00253 Georgia SC00012 Georgia SDW A 967 Hawaii SC00012 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C-SC-01 Kansas NELAP E-10332 Kentucky.SDWA 90129 Kentucky Wastewater 90129 Louisiana NELAP 03046 (Al33904) Louisiana SDWA \ LA160006 Maryland 270 Massachusetts M-SC012 Michigan 9976 Mississippi SC00012 Nebraska NE-OS-26-13 Nevada scooo 122016-1 New Hampshire NELAP 205415 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 9904 Pennsylvania NELAP 68-00485 S.Carolina Radchem 10120002 South Carolina Chemistry 10120001 Tennessee TN02934 TexasNELAP Tl04704235-16-11 UtahNELAP SC000122016-20 Vermont VT87156 Virginia NELAP 460202 Washington C780 West Virginia 997404 Page 5 of 5809 Page 6 of 5809 Chain of Custody and

Supporting Documentation

>i:::i p:L. ............ _ .......... . . ****** .. --********----*--******* ...................... ...... _ .. , ... -....... -* ....................... -....... __ , ........... _ ................. ,_,, ________ *********** (IQ -(1) -.i 0 Hi Vl 00 0 '° Page: I of 3 GEL Laboratories, LLC Project#: NIA GEL Chain of Custody and A:naiyticai Request 2040 Savage Road GEL Quote#: -NI A-Charleston, SC 29407 COCNumbef11>:---/V A-ZC) -If 5, JFY ... --.. __ -------...... ----------------*---***** --.... o* -:;__-' --------............ -------*******-*---*** " ... , ---*---*,.-*--*-.--*----.. -* Phone:-(843)-.556-817-1-----**--*--* rV Jrt GEL Work Order Number: * ... --*--*-*** PO Number: Fax: (843) 766-1178 Client Name: /\'\j ¥V Te c\I\ V\ 1 c <\ \ '5'e..; >J I C:.C'..'> Phone#: 7 t G. 312-.> Sample Requested <5l (Fill in the number of containers for each test) Project/Site Name: 4--Fax#: 71G,31z,.$3 07 Should this !'.! i;/ <**Preservative Type (6) "' = sample be *; Address: Z 't b (Lr,(){ ST. 5 u J-r?; lOO t OL--f<")J'lll\/'1 lit-I c,;o considered: c 0 u 0 .... Comments Collected by: i-O (I I ?-'-1. t-(1 s 0 Send Results To: l-t\ v f'.._, \ C(_ .. Note: extra sample is .. ,.Q *Time -; e required for sample *uate Collected g_ = Sample ID Coilcc1ed QC Code Field Sample c: specific QC (Military) 1'1 Filtered IJI Matrix .2 -< 'B ?'; *For composites. indicate start and stop date/time (mm*dd-yy) .,, u 0 \)J (hhmm) "' ... f-.< 4: I \. L 1-2{16} \5 IAi-26 tJ rJrJ so ;J ;J 1 / Lr.\, 13 . IZ. ' Lz..110/ \S 1-4-30 rJ r.Ju go ,J fV ' vi . L\-. \. B .l'Z \ . L\-12-\1 o\\. <; ll\-'35 rl NO 50 7V I" t / i-*' .. -IS,((_l,L_ \-i,h \ \S \L\Q C) rJ rJ CJ t.J rJ *1 / lf-.\ .c. e.. \ 1z\1 o(\S N NO 0 N Al t / tt. I -G. iz. \ .L-f" 1&/tdfl> 1*32..s tJ ;JO $0 N tJ *1 / 1t-j 'C,f(., . 2 ,3 L.../10/15 J3SS rJ tJ*D qd /\} Pl \ ii .Lt . \ .c. e ' ?. .+ IL/10/f .5 l-to.> .l.'\f tJO f,d tJ rJ \ il / "1.,, I, l), <<.. l ,3 1 l-)n>I 15 lGJD rJ ND tJ tJ. \ v' v ir, I ,P.>Z. ( J Lf-n,,/10(15 } 6;5 rJ ,JD s:) tJ "1 r r/ . --TAT ReQuested: Normal: ,/Rush: Specifv: (Subject 10 Surcharge) I Fax Results: VYes I No Circle Deliverable: CofA I QC Summarv I Level 1 I Level 2 I Level 3 el 4 Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Samnle Collection Time Zone -r-J d' ><C l-fovD po l't.. _ Pacific '--""""' Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details . Relinquished By (Signed) Date Time Received by (signed) Date Time Ar,:1--tlz l16 qjlil h (Q GEL PM: I , .q-CJ () q:.x:, Method of Shipment: Date Shipped: 2 {) v 2 ,/ Airbill#: *-,_ 3 3 Airbill#: I.) Chain of Cuslody Number= Clienl Detennined For Lab Receiving Use Only 2.) QC Codes: N = Nonnnl Somplc, TB= Trip Blnnk, FD= Field Duplicate, EB= Equipmenl Blank, MS= Matrix Spike Sample. MSD =Matrix Spike Duplicale Sample, G =Grab, C = Composile ).) Field Filtered: For liquid mo1rices, indicate with a

V. for yes the sample was field fillcred or -N -for sample was nol field filtered. Custody Seal Intact? 4.) Matrix Codes: DW=Drinking Waler, GW=Groundwa1cr, SW=Surface Waler. WW=Waste Water, W=Wa1cr, SO=Soil. SD=Sedimenl, SL=Sludge, SS=Solid Waste, O=Oil, F=Filler, P=Wipc, U=Urinc, F=Fecnl, N=Nasol YES NO S.) Sample Analysis Reque.ncd: Analytical mclhod requested (i.e. 82608. 6010Bn470A) and number of con1ainers provided for cnch (i.e. 82608 -3. 60/0B/7470A *I). Cooler Temp: 6.) Preservaiive Type: HA= Hydrochloric Acid. NI= Ni11ic Acid. SH= Sodium Hydroxide, SA= Sulfuric Acid. AA= Ascorbic Acid, HX =Hexane, ST= Sodium Thiosulfate, If no prcservnlivc is added= leave field blank c Page: 'Z.._ of "'2, GEL Laboratories, LLC Project#: NIA GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#: /\//A Charleston, SC 29407 ** COCNumber-\1.l: .. -../l/ .. ..,J_.,,,,, /).A--t."":'I -GELWorkUrdetNumbcr:*** -*----.. -**---**-... --***-**-* -. 7I _____ ;/\f J Jly--, ,_ *****--*-*****"* .. ..... -... PO Number: Fax: (843) 766-1178 Client Name: MJ v.J TE q-trv \ Ct\ L $£-..C:vlC Phone 11:71(;, 312 -530 & Sample Analysis Requested <5> (Fill in the number of containers for each test) Project/Site Name: "' ./ /V \f <; l: ILO A-Fax#: 7Jk ;-12.53 07 Should this .. <-* Preservative Type (6) .. c sample be ... Address: '2.-tn n..oaTST-1 t;v 1rcc_ } () C 1 0 J.-tf: tfTrJ J f" VJ /4-1 bO considered: = Q u , ... Comments Q \}..) Collected by: l-LJ (J Send Results To: L-E. L .:.:>$ 2-'-j .. ft£1\J il "' 0 Note: extra sample is ;; .Q *Time " :; e required for sample *Dale Collected .. = { Sample ID Collec1ed QC Code Field Som pie c specific QC " :; (Military) C1J Filtered (J) Matrix 141 0 < :;; u *For composites -indicate start and srop date/time (mm-tld-yy) (hhmm) 01 "' Q \tJ '" .... 4.1 ' P-* Q ,3-L. t z/q Ii> ro1*3 N ;J 0 so N (\} \ v L(-. I I J) ,f<_, t ./-f-i 2--{ /t7 { I ) 105 v" Lf'. 2-1\-I (?._.2,3 IL-}[{/1_) ' I { 2-3 ../ 4-. 2-A.R, I , 3 IL-{ .P}J S J 011 v 4-. 2A, (?. I* Lt-, , Jg-/ is* I rl5-b J .q-. z.. *A' IZ . t_, 4-1*i.-kf1s } I ,.,/ 4-.z..A .-3 n .. } 2-/I) /f>d2_ ./ t-t ' 2.-f:,. 1 " ' it'* L_ i lb I°{ ./ Lt-, '2 ... J'.5 ( R.' 2-, t"' I 2-/&-JlJ 14-JO j £.j-7-*s, f(... I I, t-f.l_,}&' f I 5 }350 ' .... 'It ' 'I / TAT Requested: Normal: /Rush:_ Specify: (Subject to Surcharge) I Fax Results: I No Circle Deliverable: C of A I QC Summary I Level I I Level 2 I Remarks: Are there any known hazards applicable to these samples? If so. please list the hazards rollection Time Z"ne--:--( 17/v tJ 0 /Ci\i() I..\-f{2 A , f' (; t-A-t;. rto\..p FO rz A-L 'f A l\i A L'1 .. tlS. """" =r Mountain ......... _ .... Chain of Custody Signatures sample* shipphig-ind.DetivefY Details ....................... ************ Date Time Received by (signed) Date Time GEL PM: Pl /-i./i 6 1tt-oo '1:30 Method of Shipment: Date Shipped: /V 2/ Airbill #: -3 3 Airbill #: I.) Chain ofCuslody Number= Client Determined For Lab Receiving Use Only 2.) QC Codes: N =Normal Semple. TB= Trip Blank, FD= Field Duplicate, EB= Equipment Blunk. MS= Matrix Spike Sample. MSD =Matrix Spike Duplic*te Sample. G =Grab, C =Composite J.) Field Filtered: For liquid malrices. indicate with a -Y -for yes the sample was field fihcred or -N -for sample wos not field filtered. Cuslody Seal In/act? 4.) Matrix Codes: DW=Drinkins Water. GW=Groundwnter. SW=Surfacc Water, WW=Waste Waler, W=Water. SO=Soil. SD=Sediment. SL=Sludgc, SS=Solid Waste, O=Oil, F=Fil!er. P=Wipe. U=Urine, F=FecRl, N=Nasal YES NO 5.) Sample Analysis Requested: Analytical method requested (i.e. 8260B. 60101l17470A) and number of con1niners provided for eoeh (Le. 82608 -3, 60/0817470A
1). Cooler Temp: 6.) Prescrva\ive Type: HA= Hydrochloric Acid. NI =Nitric Acid, SH= Sodium Hydroxide, SA= Sulfuric Acid. AA= Ascorbic Acid. HX =Hexane. ST= Sodium Thiosulfale. If no preservotive is added= leave field blank c PINK = Cl .IF.NT Page: of ":2. GEL Laboratories, LLC rJ J '14 GEL Chain of Custody and Analytical Request Project#: 2040 Savage Road GEL Quote#: !VIA Charleston, SC 29407 COC Number {ll: '°t ... .GEL .Work .Order.Number:
Phone: (843) 556-8171 i'c5'Number:-----"7\F7."JL *** . ---***-*** .. ,, .. -. **-** ----*-*--** -. _ _. . *--*** -** ----* *-.. *** **-** ---*-. . **-.' --** Fai<:. (843} 7()6:1 f78 *-,_ ----**-* . Client Name: r'\ .....) W ti:.Crtl /Cpf-L.. Sf/Z\i'IC.Z:.C. Phone #:7 /6
377 $.30 Cl Sample Analysis Requested <5l (Fill in the number of containers for each test) Project/Site Name: NiS..f;i,c 0 A "' Fax#: 716 .31? .S.3<J l Should this .. <-* Preservative Type (6) ., = sample be *;; Address: '2 .<-\'"? 50 11Z. 0 i-£;/JrJ ) 1"'1 l-+"'10b considered: c 10 a, Q u / ... Comments Q 9' Collected by: t:.c tr<Cr' Send Results To: t.{JVl'LF\*£. '-0 $f?;Y t.j .. v ., 2 Note: extra sample is .E .c *Time " " E q:;-required for sample *Date Collcc1ed > if* = Sample ID Collected QC Code Field Sample ... a: c )'-specific QC " -;; (Military) "' Filtered IJJ Matrix141 .E < *For composites -indicate s1art and stop da1eltime (mm-dd*))') "' u (hhmm) .;.i Lf-',2.,,g j R-12-13 1s i+r-, f\) iJ () s.o rV {\) I ,/ Lf-.L-6 ((_ \. l ,3 I q-.;; I I ,,/ 1-,z g, R...,j\12-1.:i:h .. hs ].04-D J / 4--Zi> ((_ .z I[__ I lL\-13 1 ... v "v ,11 ..," *v v . TAT Reauested: Nonna!: SnecifV: (Subject to Surcharge) I Fax Results: I No Circle Deliverable: C of A I QCSummarv I Level I I Level2 I Level 30 i Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards SamhtP f'ollection Time Zone IV o /e;.r..µ 1-tA'V\Yl t?Si Pt er.tS'C '/¥),.0 F 01< P u r(1* 'ft'E{L t'1 N ft L-V s,1.S, . <'.' Eastern '\ PacitiC' Central Other ---Mountain ... Chain of Custody Signatures Sample Shipping*and**DeliveryDetails * ***-***"'* ..... ....... *-***** . Relinquished By (Signed) Date Time Received by (signed) Date Time I .,-..,_ryv?)* GEL PM: 4/z,f16 I I '2,,.,,. ./ C/!:.3c. Method of Shipment: Date Shiooed: J v ,/ , Airbill#: -3 3 Airbill#: I.) Chain of Custody Client Detennined For Lab Receiving Use Only 2.) QC Codes: N =Normal Sample. TB =Trip Blank, FD = Field Duplicate, EB= equipment Blank. MS= Matrix Spike Sample. MSD = Matrix Spike Duplicate Sample. G =Grab, C =Composite J.) Field Filtered: For liquid matrices. indicate with a
Y
for yes the sample was field filtered or -N -for sample was not field filierod. Custody Seal Intact? 4.) Motri* Codes: DW=Drinking Woter, GW=Groundwater. SW=Surface Water. WW=Wastc Waler. W=Watcr, SO=Soil. SD=Scdiment, SL=Sludge, SS=Solid Waste, O=Oil. f'=Filter, P=Wipe. U=Urine, F=Fec*I. N=Nasal YES NO 5.) Sample Analysis Reques!Od: Analytical method requested (i.e. 82608, 6DIOB/747DA) and number of containers provided for each (i.e. 82608
3, 60J0817470A. -1). Cooler Temp: 6.) Preservaiive Type: HA= Hydrochloric Acid, NI = Nitric Acid, SH =Sodium Hydroxide, SA =Sulfuric Acid, AA = Ascorbic Acid, HX = Hexane, ST= Sodium Thiosulfatc, If no preservative is added= leave field blank c WHITE= LABORATORY YELLOW = FILE PINK= CLIENT 01 Appendix C -Analytical Methodology Analytical Parameter Method MDC Standard Analysis 0 ........ VI 00 0 \0 -Page: 'I of .I .. GEL Laboratories, LLC Project#: "'° 'f .S E 11..D Ii -GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#: NIP. Charleston, SC 29407 COC Number Cll: /\1'1.SFIC..JJA---$-i . GEI. Phone: (843) 556-8171 --PO-N\Jirioer:-*----*--N*-J-1\ -.. --*-. ,..-*---****-**----*-*-. ...*... *-*--* ***-------** *' ***** *-**-"'"'" *---*-.. *--*-****-**--**--*-**--*--*-**--Fax:(S4J"f16i5=rr1s------------* --------* ***------*-*---* Client Name: M.JW 'ftett"3\C I\\.. r f...S Phone#: 716 :Jr? . .)3W Sample Requested <5> (Fill in the number of containers for each test) Project/Site Name: I\) '-1 > f::ILO A Fax#:']/.(, .)72 ,S,,3.lYJ "' Should this ... <--Preservative Type (6) .. c sample be *; Address: 'Z...t-; 7 IZool':>I* /::;v 1\£:--loo ,6 L-f:::T\rl 1 /\.l'1 lt/-160 considered: E 0 u ... Comments " Collected by: u /tCctJ(l.( Send Results To: /..fJW fZ-L CZ:-1 ... Note: extra sample-is .. .,Q *Time ;; e z required for sample *Date Collected .. = ct Sample ID Collcc1ed QC Code Field Sample &! i:: specific QC (Mililary) "' Filtered (JJ Matrix f4l < ;; -fo. *For composites* indicate start and stop date/time (mm-dd-yy) :0 u -e {hhmm) &! .... ¢' -;) 'z 1.6, ll.. 2.. t-f15 sJ . N t\JcJ 50 rJ /\] I I v r;. 2-, '5 ,R. t_ J&J11J15 Hs5 ' 'l 1 \
s , A. fZ.. \, ) l 2..\ t S Ii) l 4 \Lt\O 5 .itA,JZJ,J I 2..-j I{.. 11 ( u.-*ei :-> I ) -"f A. it.. lf', 2_ J s -SA (<_.., ) i?-1 f1 h> 1 :S D I I < -b A. (l< 'I ,3 tvh1 \ 2--i°O ,ll ... ,, -.J ,, *7 7 ./ TAT Requested: Normal: /Rush: Specify: to Surcharge) I Fax Results:/ Yes J No Circle Deliverable: C of A I QC Summary I Level 1 I Level2 I Level 3 1 Remarks: Are there any known hazards applicable lo these samples? If so, please list the hazards SamnlA Cdllection Time Zone -_/ -Nr {LN_,-1\j ,...J 1+'1V'rr1.tJ > . V'L ei7 .$ '(_ j-fci-;. (> P'dtl.. ro Te&Vrt Pr'--Fuf(....Titf/2., l1N A '-'1SLS , c Eastern/ Pacific Central Other ---Mountain *******-*** Chain of Custody Signatures *Sample Shipping and*Delivery*Details* ******-*****-****** ****-*-*-**** ... 1.Rel;/,f q/:t;,6 Time Received by (signed) Date Time X> GEL PM: 1 Melhod of Shipment: Date Shiooed: { I v 2/ Airbill#: 2 3 3 Airbill 11: I.) Chain of Custody Number= Client Dctennined For Lab Receiving Use Only 2.) QC Codes: N = Normol Sample, TB= Trip Blank, FD= Field Ouplicatc, EB= Equipment Blank. MS= Matrix Spike Somplc, MSD = Mairix Spike Duplicate Sample, G =Grab, C =Composite J.) Field Fillcrcd: For liquid matrices, indicate with a -Y -for yes the sample was field filtered or -N -for sample was nol field fihcred. Custody Seal Intact? 4.) Matrix Codes: DW=Drinking Waler. GW=Groundwntcr. SW=Surface Water, WW=Wastc Water. W=Waler. SO=Soil. SD=Sediment, SL=Sludge, SS=Solid Waste, O=Oil, F=Filler, P=Wipe, U=Urine, F=fecAI, N=Nasal YES NO S.) Sample Analysis Requesied: Analytical method requested (i.e. 82608. 60JOB/7470A) and numbcrof coniainers provided for each (i.e. 82608
3, 60/0817470A -I). Cooler Temp: 6.) Premvaiive Type: HA =Hydrochloric Acid, NI = Nitric Acid, SH =Sodium Hydroxide, SA = Sulfuric Acid, AA = Ascorbic Acid, HX = Hexane, ST= Sodium Thiosulfatc, If no preservative is added =leave lie Id blank c WHITE= LABORATORY YELLOW = FILE PINK = CLIENT Appendix C-Analytical Methodology Analytical Parameter Method MDC Units Standard Analysis Page 12 of 5809' Page: I of '=< GEL Laboratories, LLC J'JJA -Project#: GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#; /VJ/} Charleston, SC 29407 COC Number <ll: N'Kt?alJA--3) GEL Work Order Number: Phone: (843) 556-8171 PO Number: ........ .. ...... ...... , . . ........... '"' -------*-*-------*-* -----*-* **---*---.. ------. --. --...... ---* ----*------*---** ----****-* ---**--Fax:.(843) . .766-.U 78 .. ----Client Name: NlJvV '&z....11 Ct§ Phone#: 716 .3Tl .)3() &> Sample Analysis Requested <SJ (Fill in the number of containers for each test) Project/Site Name: "' J N Fax#: 116 .31':? .s*-:;.o/-Should this .... <--Preservative Type ( 6) ... c sample be *; Address: 2..o-r-Roc-r5 < * , 5 (,) 1 'f'Z::. 'oo 1 o 1.-E .irrJ .. I\) I 11-7-60 considered: = 0 " ... Comments 0 "' Collected by: µ t) li"J Send Results To: t'..AVA.-L£ J-oS>"7i; '1 .... Note: extra sample *is ] ... ..Q .!! E < required for sample *Time
Uate Collected co "' <: Sample ID Collected QC Code Field Sample .::: c specific QC (Military) '" Filtered Ill Matrix CJ> .5! < -; ..,.. (mm-dd-yy) "' (.J 0 *For composites -indicate start and stop date/time (hhmm) Q! .... '\J Lt' . .) 8 JZ
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c; I l ' rz. , "Z.. * '-t I c_ )-z.. fJ .> '50q-¥ ii ,'J' ... c:;-' TAT Requested: Nonna!: VRush: Speci!Y: (Subject to Surcharge) I Fax Results: Jes I No Circle Deliverable: C of A I QC Summary I Level I I Level2 I Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sam11le Collection Time Zonf!"---.J JC 114 (i v\i ,_) HA'?.P\-Flt').J. p L He> -,,o R'otZ f' L-Y::: v IOl\tatL A -& '-1 £l-5 Eastern Pacific '> Central Other Mountain ***-*-*-Chai_n o.fCustody . .. Sample and_ Delivery Details . Relinquished By (Signed) Date Time Received by (signed) Date Time .. 7/-v/16 GEL PM: I .i-100 q /1< Ii (;p jo Method ofShioment: Date Shioped: v // _.._../ Airbill#: 2 2 3 3 Airbill 11: I.) Chain of Custody Number= Client Determined For lab Receiving Use Only 2.) QC Codes: N =Normal Sample. TB =Trip Blank, FD = Field Duplica1e, EB = Equipment Blank. MS = Matrix Spike Sample, MSD =Matrix Spike Duplicate Sample. G = Grab, C = Composite 3.) Field Filtered: For liquid matrices. indica1e with a -Y
for yes the sample was field filtered or* N
for sample was not field filtered. Custody Seal Intact? 4.) Matrix Codes: DW=Drinking Waler, GW=Groundwater, SW=Surface Water, WW=Wnste Water, W=Watcr. SO=Soil, SD=Sediment, SL=Sludge, SS=Solid Waste. O=Oil, F=Filler, P=Wipe. U=Urinc, F=Fecal, N=Nasal YES NO S.) Sample Analysis Requested: Analytical method requested (i.e. 82608. 60tOBn470A) and number of containers provided for each (i.e. 81608
3, 60/0Bl7470A -1). Cooler Temp: 6.) Preservaiive Type: HA= Hydrochloric Acid, NI =Nitric Acid, SH =Sodium Hydroxide, SA = Sulfuric Acid, AA = Ascorbic Acid, HX = Hexane. ST= Sodium Thiosulfate, If no preserva1ivc is added= leave field blank c WHITE= LABORATORY YELLOW= FILE PINK =CLIENT Page: 2-. of '3 GEL Laboratories, LLC Project#: J'\) I J\ GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#: rV l/J Charleston, SC 29407 COC Number <ll: /l/ tJIJ GEL Work Order Number: Phone: (843) 556-8171 PO Number: /VJ A-*--_____ --*. --*---*------**-----*---. *---**-*---**--*---*--*--**--------*--Client Name: IC.;\ L-.;.z:/(,v IC r Phone #:7 /-b 372 Sample Analysis Requested <5l (Fill in the number of containers for each test) Project/Site Name: /\J 1 <:" CCYLO A Fax#: 716 .)7'2 _s;.-::?£17 J <--Preservative Type (6) Should this "' = sample be *; Address: "1.tf'::;, llOo TS 7 1 s,.u 1nt00 / 0£...Zt}rV I 1\1"1. f't-760 considered: = 0 " ... Comments 0 Collected by: µ ci fi/t Send Results To: t.,.-1:,-v tU £ t.-0$ Z.( ... Note: extra sample *is "' d ,.Q *Time :; e required for sample *Dale Collected .. "' Sample ID Collected QC Code Field Sample = specific QC (Mi111ary) Pl Filtered Ill Matrix 1"J .:? < ")('.. (mm-dd*yy) "" u
For composites -indicate start and stop date/time (hhmm) .:2 0 '\}-.I ... 5 JA. /, 7-.. fL.) lb 11 s l'l2b (\) iJrJ S.d A/ tJ . l ' v"' )
J A * (2._. I v s I z./16{1:; 12-3) t 1 $"',1!3trZ, 2 'l_ I -z, \ I'-\\\ 5 'L c;
2 * '):') I fl ( \. "'L 12.}1'"1\1s* 13tCJ '"2-* .) . 7-1A,fl... \ _) J 1..-J 1 't Ii <; . 1 '71.) 5* _z ,A* r2, \ I t.t n ... Jil-J-\u i 5?..5 (_ -* J"(, 1?-IJrtJiS ?_ 5. l A 1-,50 5* .rz. A I fl. 'Z. I '2...{1trf IC:. t Lf. c:o 2 5 -(. f\,Yl,&,(__ 1"2-/11'1 f I l?, (!) I l 5.2-A,c +."L 1t./11l1s r&'Z-*7 ,, v 'I l 'I! ..-* TAT Requested: Nonna!: Rush: Soecifv: (Subjcc110 Surcharge) IF ax Results: I No Circle Deliverable: CofA I QC Summarv I Level I I Level 2 I Level 3 4 \. Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Sam12le Collection Time Zone ---.._; r.J.;:, f i::.l\Jo .v rJ 2 , PL E"IH:"t:.. H--01.,p Fo ii< fo T'Er.r1{)L /JrVftL--'-ISII) Eastern Pacific Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details . Relinquished By (Signed) Date Time Received by (signed) Date Time 4lv)j{, .?; /u/,u GEL PM: l I -? -J et:30 Method of Shipment: Date Shipped: 2 (_)I/ 2 J Airbill#: 3 3 Airbill #: I.) Chain ofCus1ody Number=Clicn1 De1crmined For lab Receiving Use Only 2.) QC Codes: N =Normal Sample, TB= Trip Blank, FD= Field Duplicate, EB= Equipment Blank. MS= Ma1rix Spike Sample, MSD =Matrix Spike Duplica1e Sample, G =Grab, C =Composite J.) Field Fihercd: For liquid ma1riccs, indicn1e with a -Y
for yes the sample was field m1cred or -N -for sample was not field filtered. Custody Seal Intact? 4.) Malrix Codes: DW=Drinking Water, GW=Groundwntcr. SW=Surface Wo1er, WW=Wastc Waler, W=Wa1er, SO=Soil. SIFSedimcnt, SL=Sludgc, SS=Solid Waste, O=Oil, F=Filter, P=Wipe. U=Urine, F=fccal. N=Nasal YE.S NO S.) Sample Analysis Requcs1cd: Analytieal method rcqucsled (i.e. 8260B, 6010Bn470A) and number or containers provided for each (i.e. 82608 -3, 60/08!7470A -I). Cooler Temp: 6.) Presc,.,,niive Type: HA= Hydrochloric Acid, NI= Nitric Acid. SH= Sodium Hydroxide, SA= Sulfuric Acid, AA= Ascorbic Acid, HX =Hexane, ST= Sodium Thiosulfatc, If no preserva1ive is added= leave field blank c WHITE= LABORATORY YELLOW = FILE PINK = CLIENT

....... Vl 0 H') Vl 00 0 \0 Page; --"-G_,,..'----.*of Project#: AJ) Ir GEL Quote #: rJJ .lL GEL Chain of Custody and Analytical Request GEL Work Order Number: GEL Laboratories, LLC 2040 Savage Road Charleston, SC 29407 Phone: (843) 556-8171 COC Number <ll; j\)l.j £. P:U /) .4 -3'0 F'O Number; N) A-!'ax: (843)]66:Jl78 .. __ ------------ICA Phone#: 7163-rz .5300 Sam Analysis Requested <5> (Fill in the number of containers for each test) Project/Site Name: Should this N"-( s;;:. 'E,n_ tJ-4 Fax#: 716 7'2--5?:J::77 sample be Address: z_4-3> t2oO /5'r 1 J Sv, rE fCJo, / Collected by: [__o I.) f2.L--J Send Results To:L::J-u/2t fi=. l.-0 9f::;-*--v/ *Date Collected Sample ID *For composites* indicate start and Sf Op date/time (mm*dd-yy) ,. ,.2, @, f2, J .'-r 1 dn Ii< *rime Collected (Military) (hhmm) QC Code Field Sample m Filtered IJJ Matrix ,.,, i-&1 D ,_, \ \ considered: .. > " " " :;; Ql .. c *; c: e "' ... e .. " ,Q E! ::i c J 'i i I, <--Preservative Type ( 6) Comments Note: extra sample is required for sample specific QC TAT Reouested: Normal: Specify: (Subject 10 Surcharge) I Fax Results:

I No Circle Deliverable: C of A I OC Summary I Level 1 I Level 2 I Level Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Samnle Collection Time Zone r.J }t-1\'V\ Cl0.1 . }\-OL.0 \)GY\CCl"\A-L f=u<2°H-t""'ciJl-_AAJ 4L-"1$1_5 _ ( Eastern acific Other __ _ c;emral Mountain Chain of Custody Signatures Sample Shipping and Delivery Details .. . GELPM: 1 * / q}'"t..-j/6 l--'foe.J l _.c...--:3c.J MethodofShinment: DateShipoed: Airbillll: 3 3 Airbill II: I.) Chain of Custody Number= Client Determined 2.) QC Codes: N =Normal Sample. TB =*Trip Blank; FD= Field Duplicate, EB = Equipment Blank. MS= Matrix Spike Sample. MSD = Matrix Spike Duplicate Sample. G =Grab, C = Composite 3.) field Filtered: For liquid matrices. indicate with*. Y
lllr yes the sample was field fillercd or* N
tbr sample was not field filtered. 4.) Matri< Codes: DW=Drinking Woter, GW=Groundwater. SW=Surface Water. WW=Waste Water, W=Water. SO=Soil. SD=Sediment, SL=Sludge, SS=Solid Waste. O=Oil, F=Filter, P=Wipe. U=Urine, F=Fecal, N=Nasal S.) Sample Analysis Requested: Anoly1ical method requested (i.e. 82608. 601 OBJ7470A) and number of containers provided for each (i.e. 82608
J. 60/0B/7470A -I). 6.) Prcservaiivc Type: HA= Hydrochloric Acid. NI= Nitric Acid. SH= Sodium Hydroxide. SA= Sulfuric Acid, AA= Ascorbic Acid, HX =Hexane. ST= Sodium Thiosulfatc. lfno preservative is added= leave field blonk WHITE= LABORATORY YELLOW= FILE PINK = CLIENT For lab Receiving Use Only Custody Seal intact? YES NO Cop/er Temp: c Appendix C-Analytical Methodology Analytical Parameter Method 'MDC Units Page 16of5809 Page: /. of :::> GEL Laboratories, LLC Project#: IV/A GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#: di A Charleston, SC 29407 COC Number 11>: /'J't'.i.,-C;4-ZO°i4 0 GEL Work Order Number: Phone: (843) 556-8171 ** * -**---*** .. --.---* -.,. .*..*.. . '* --... ---* ---*-... ----******--... ---*-**--*.. ---*-,.,, .... -***-*---*-**-*** ,-.---*-----******-*'"* .. -* ------.. Fax:*(843P66CI 11s-*-------*----*-*-----------*-*------*----. Client Name: /V\j w J Ge, rtN I c ;<J L5 E:Jt LI I C.E-S Phone #:7 I b .31'2 .S 3()() Samp°ie Requested <5l (Fill in the number of for each test) Project/Site Name: -fV Vf .S¥L.04 Fax#: l:! ./ <--Preservative Type (6) Should this ... " sample be *; Address: VI-? Mor-S. l' .. 5u (Tf_ 1Co, 0 J-!Z./'rrV
f\J 't considered: = 0 CJ *" ... Comments 0 Collected by: LtfU ttr/\t r<-'1 Send Results To: L4vtt. I£. 1-0SE.{ .,, ... \J Note: extra sample *is .. "" -2 *Time .. ;; e ! required for sample 'Dole Collecled "i .. = Sample ID Collecled QC Code Field Somple " specific QC (Military) .,, Filtered OI Ma1rix r.1i < !! (mm-dd*yy) '6 u
For composiles
indicole star/ and stop date/time (hhmm) " a: .t.J-., 2 .£?IR I IL.. I Zf8}!_5 15 ?,.R /\} t\Jo 50 ."} rJ 'l v( ' q-. z_ c '11..... I, 3 t2fg{15 101) I £Y. 2-C, rz, I '1t-I '2..-/t< 11 5 l 0 t'9. 4--3 I Ar? i 1Lj_*z.::,f 1j . + .. ?, g It'<_' i . *3 11 1'2.?/ lf 11\0 1-3.A ,<<.2 -L., 11h::>\*s* l 't¥-f tt ' 3.!'3 vz \ °\ ,"?_ I\ l2e--\d t"l.S Lf-' °"?) B.-R .. \l\l--7\\5 I \Lf-S"' ti-. *:s (:3' (( '3d--11 l't)\ 'S \t'S3 ' . ..tr-.3 ,B. \'Z, \. '-r '\ \-z_ ">,\\ 5 ... ... ..... , \T \ \ 't_(J TAT Requested: Nonna!: r /Rush: SoecitV: (Subject 10 Surcharge) I Fax Results: i:.,...-Yes I No Circle Deliverable: C of A I QCSummarv I Level I I Leve12 I Level 3 <J Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Samnlp "oller.tion Time Zone -"' () /Cl\Jtl N ,.; 11 /)Z. rvi ;t-oL-0 Fait PO'l9"vTY 1-) t._ 117:,e_ 1'.N I\ L '15\.S. J ( Pacific I Other Mountain **-*** Chain of.Custody.Signatures .. . Sample Shipping and Deliver.y. Details . . ... , .. . Relinquished By (Signed) Dale Time Received by (signed) Date Time IF'\&-q/w/U.P GEL PM: '1/ vf /h L "/-CJC1 Method ofShioment: Date Shiooed: 2V v 2/ Airbill #: 3 3 Airbill #: I.) Chnin of Custody Number= Client Determined For Lab Receiving Use Only 2.) QC Codes: N =Normal Sample, TB= Trip Blank, FD= Field Duplicate, EB= Equipment Blnnk. MS= Motrix Spike Sample, MSD = Motrix Spike Duplicate Sample. G =Grab, C =Composite 3.) Field Filtered: For liquid matrices, indicate with a -Y -for yes the sample was field filtered or -N
for sample was not field filter<d. Custody Seal Intact? 4.) Matrix Codes: DW=Drinking Water, GW=Groundwoter. SW=Surfacc Waier. WW=Waste Water, W=Walcr. SO=Soil. SD=Sedimenl, SL=Sludge, SS=Solid Waste. O=Oil. F=Filter, P=Wipc. U=Urine, F=Fccal, N=Nasol YES NO S.) Sample Analysis Requesied: Analytical method requested (i.e. 82608, 6010Bn470A) and number ol"contoincrs provided for each (i.e. 81608
3, 60/0Bl7470A
I). Cooler Temp: 6.) Prcmvaiive Type: HA= Hydrochloric Acid. NI= Nilric Acid, SH =Sodium Hydroxide, SA =Sulfuric Acid. AA = Ascorbic Acid, HX = Hexane, ST= Sodium Thiosulfate, If no preservative is added = leave field blnnk c WHITE= LABORATORY YELLOW= FILE PINK =CLIENT

...... 00 0 ......, VI 00 0 \0 Page: "£ of * "'? GEL Laboratories, LLC Project#: /JI A GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#: NJA Charleston, SC 29407 COC Number Cl>: .IV 'I §f: fl,/) 1+.o 0 GEL Work Order Number: Phone: (843) 556-8171 I'O.Number:. _____ A)f--A, ...... --*-----.. -. -* . -*** v ** -,. *---*** -_, ______ *---, .. -... --**-*------*-***** ____ ***--**------.. --------------*--*---**-*------*-*-------Fax: (843)"766;n7g** **-*------**-*--------*--**----------* Client Name: N\J IN "ffetj Iv') C4 L <$£;-z,v Phone #: 1 { 6 Jf2 -Sample Analysis Requested <5> (Fill in the number of containers for each test) Project/Site Name: N'1 .04-* Fax#: 71.G S3D/ Should this <--Preservative Type (6) "' c sample be *; ' c Address: 2--Pr?:, f'la tPT 5 '"t. , £ U 1T"Z,.1m OL.<f1'l\J ,IV'1 /Jt-l 6 0 considered: 0 ' u , .... Comments 0 Collected by: L6 o ft£/'\J fL'1 Send Results To: 1-lt,v te.l z. J..-c;.9',?;: ( il .. C) Note: extra sample -is "' -;; "" 7-;; e required for sample *Date Collected *Time .. = [ Sample ID Collected QC Code Field Sample Ji: c specific QC " Oi (Military) 111 Filtered ll) Mntrix'"J 0 < x (mm-dd*yy) :;; u *For composites-indicate start and stop date/time (hhmm) .>! \N R I *2 .) n l*2?f 1> '\ }() .:[, rJ tJr> _>) fl) N -I v t-I J\-z.. ) li_5 1 \ '\ t-t-i <:3 if\.,2, 11\L._ v +-. R..-Z.t'.f Ii \?als 5 fl\ 4. tt.4( . !<_ ' I . ?7 £7!15 I O*"to t-t-. t.rl I tZ.. ' 1 £-\-\ l \3 " lj 1 0 4-) 1", L.\-,f) I fZ_ I 1*3 JI l o'ltf "f:) '2.-;, 4 j), y<.-.2.:;, -n \s o\tJ i-y-* .l\-D . e , 1-. faf ll \ f I J 13 . 11b,o\1) ... ... ... .1 ...,if ,, ii )")5D TAT Reauested: Nonna!: Speci!Y: (Subject 10 Surcharge) I Fax I No Circle Deliverable: C of A I QC Summary I Level I I Level2 I Level4) Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards Samnle rrinection Time Zone ('.) c) 1.:::: l\tP V\I rJ \-\tr iA (LO .5 , r 1-eA-*.ct_ M-G i. o f=O fl_ P }"'l L r U 1ZT\-\-e,fC. f\rV 4t-"-I £'.JS . .__ Eastern Pacific .. Other ---Mountain .. ...*. .. Chain .of C.us.toiJy Signatures Sample Shipping and Delivery Details ... -. Relinquished By (Signed) Date Time Received by (signed) Date Time 1k GEL PM: 11-'60 q*"> I I -._:x.-, Method of Shipment: Date Shipped: 2 //{/ 2J Airbill#: 3 3 Airbill#: 1.) Chain of Custody Number= Client Determined For lab Receiving Use Only 2.) QC Codes: N =Normal Sample, TB =Trip Blank, FD= Field Duplicate, EB = Equipment Blank, MS= Matrix Spike Sample, MSD = Matrix Spike Duplicate Sample. G = Grab, C =Composite 3.) Field Filtered: For liquid matrices, indicate with a -Y -for yes the sample was field filtered or -N

for sumple was not lield filtered. Custody Seal Intact? 4.) Matrix Codes: DW=Drinking Water, GW=Groundwater. SW=Surfacc Water. WW=Waste Water, W=Wnter, SO=Soil. SL=Sludge, SS=Solid Waste. O=Oil. F=Filtcr, P=Wipe, U=Urine, F=Fccnl, N=Nasal YES NO S.) Sample Analysis Requested: Analytical method requested (i.e. 8260B, 60IOBn470A) and number of containers provided for each (i.e. 82608
3, 60/081747o,t *I). Cooler Temp: 6.) Pn:servaiivc Type: HA= Hydrochloric Acid, NI= Nitric Acid. SH= Sodium Hydroxide, SA= Sulfuric Acid, AA= Ascorbic Acid. HX =Hexane, ST= Sodium Thiosulfatc, IJ'no preservative is added= leave field blank c WHITE= LABORATORY YELLOW= FILE PINK= CLIENT Page: 3 of GEL Laboratories, LLC Project#: GEL Chain of Custody and Analytical Request 2040 Savage Road GEL Quote#: Charleston, SC 29407 COCNumber<ll: Noi">P/l..IJil -'30 GEL Work Order Number: Phone: (843) 556-8171 PO Number: /VJ A-**-*-*-"-* . *---*---*" -. -***-*--.. -... . ---'** *-*********---. .. -. *****-*----**-----.. -** ---------.. .. ---*-****--*--Fax:-'(s43Y166:r*11s .. ----*---------------------------*'*-----**-*** --****** -'"' -Client Name: MJ IN 7fel-f/VI CE;.f Phone#:/ f 6 -37'2 -5 30 e> Sample Analysis Requested <5! (Fill in the number of containers for each test) Project/Site Name: Nwf S£rl0/-}-Fax #:71-6 37'2 .s;;.a/ ::: r L-------" Should this .. <--Preservative Type (6) = sample be *; Address: ? t!f-3;. floor:;;< . 1_Sv 1'T"£I Cc>i () £--'6') rl , Ni considered: c .. " ... Comments .. <:;:::, Collected by: 11-0 CJ rtcN >/L ( Send Results To: .. Note: extra sample 1s .. 2 .c *Time .. -; s required for sample *Date Collected *S "" "' Sample ID Collec!ed QC Code Field Sample = specific QC " J (Mili1ary) m Filtered <<lJ Matrix < !'! *For composites* indicate s1art and stop date/time (mm*dd-yy) "' u 0 (hhmm) Cl !-tt _ 11::-. 'b J'Z. <; .( I\ ha/i f 'ILfl s pJ Ao SD IN l'\J i v *.SA. t<-11-i'J \ ** I I I ,:-:) tJ Io 02._ .tr, .c; A-(?__ ' ' ' i n::.1*1 \ tj to f 6 1/ 1-J. S' I t.-I 1 /. I_) , 31 '= ,, 'V '\) [-../' i"I/ ,, fS d< . \. 'L_ _/ TAT Reouested: Nonna!: /iush: $pecifv: (Subjec1 to Surcharge) !Fax Results:V Yes I No Circle Deliverable: CofA I QC Summary I Level I I Level2 I Level 3 45"* Remarks: Are there any known hazards applicable to these samples? If so, please list the hazards "*<'ollection Time Zone -Ne, lc;-uu-"1.J fV 1-tA-'2A-fl0>. r l-'2 Pis tC-i-lcn...O !f=-o it. Ponc'.-/ll"l'I _s _ c_ Pacific l Other ---Mountain Chain of Custody Signatures -Sample Shipping-and-Delivery-Details ---********-***** . -***** ... -. Relinquished By (Signed} Dale Time Received by (signed) Date Time q /1;eftc,, GEL PM: I "1Jv/t6 I 'to C) I k.-... ,L 0;*30 Method of Shipment: Date Shipped: d /{/ Airbill #: 2 3v 3 Airbill#: I.) Chain of Custody Numbor =Client Detennined For lab Receiving Use Only 2.) QC Codes: N =Nonna! Sample. TB =Trip Blank, FD= Field Duplicate, EB = Equipment Blank. MS = Matrix Spike Sample, MSD = Mnirix Spike Duplica1c Sample, G =Grab. C =Composite J.) Field Filtered: For liquid matrices, indicate with a
Y -for yes 1hc sample was field filtered or -N -for snmple was not field filtered. Custody Seal Intact? 4.) Matrix Codes: DW=Drinking Water. GW=Groundwater. SW=Surface Water. WW=Waste Water, W=Water, SO=Soil, SD=Scdiment, SL=Sludge,SS=Solid Waste. O=Oil. F=Filter, P=Wipc, U=Urine, F=Fecal, N=Nasal YES NO S.) Sample Analysis Requested: Analytical method requested (i.e. 82608. 6010817470A) and nuniber or containers provided for each (i.e. 82608 -3, 60/0817470A -J). Co.oler Temp: 6.) Prcservaiive Type: HA= Hydrochloric Acid. NJ= Nitric Acid, SH= Sodium Hydroxide. SA= Sulfuric Acid. AA= Ascorbic Acid, HX = ST= Sodium Thiosulfate. lfno preservative is added= leave field blank c WHITE= LABORATORY YELLOW= FILE PINK =CLIENT Appendix C -Analytical Methodology Analytical Method 'MDC Units Page 20 of 5809' I Laboratories LLC SAMPLE RECEIPT & REVIEW FORM Client: ! ;vi J f/J G-SDG/AR/COC/Work Order: <,--. q/ /ii Ip -Received By: Date Received: Hazard Information 0 *If Net Counts> IOOcpm on samples not marked "radioactive", contact the Radiation Safety Group for further ; z investigation. COC/Satilples marked as radioactive? / Maximum Net Counts Observed* (Observed Counts -Area Background Counts): O Cf' vv. Classified Radioactive lI or m by RSO? ,/ If yes, Were swipes taken of sample containers <action levels? COC/Samples marked containing PCBs? ./ PJ!ckage, ;coc; a!l<L'or Samples* maiked as" / '*" If )'CS'. sample8 are to be as Safe!}' Samples; and cioen6ii deL *. beiylliurrl or asbesios c0ntainfog? .. ..* .. Shinned lis a DOT Hazardous? ..... Hazard Class Shipped: UN#: Samples identified as Foreign Soil? / ;> ' -\ Sa.i_nple Receipt Criteria ., < 0 .. Comments/Qualifiers (Required for Non-Conforming Items) :>< z z Shipping containers received intact and v"" Circle Applicable: Seals broken Damaged container Leaking container Othc,r (describe) 1 seal¢? saniples requiring cold preservation Preservation Method: lee bags Blue ice Dry ice 6jY Olher(doscribe) 2/"l 2 within (0 6 deg. C)'?* ,/ *all temperatures arc recorded in Celsius Daily check performed and passed on IR Temperature Device Serial #: 2a I , i/ Secondary Temperature Device Serial #(If Applicable): teml?erature gun? 3 of custody documents included / with' shipment? ' Circle Applicable: Seals broken Damaged container Leaking container Olher 4 Sample containers intact and sealed? ./ Samples requiring chemical preservation Sample !D's, containers affected and observed pH: 5 at pH? / . rr ..... ,, ... ,, , .... u. 6 Do !:ow Level Perchlorate samples have ./ Sample !D's and containers affected: headspace as required? 7 vials contain acid preservation? v' (If unknown, select No) VOA vials free of headspace (defined as s/ Sample !D's and containers affected: 8 < 6ni,m bubble)? .. 9 Are Encore containers present? v yes, immediately deliver to Volatiles laboratory) received within holding time? ID's and tests affected:
10 .,/ Sample ID's on COC match ID's on . Sample !D's and containers affected:
11 bottles? . ./ time on COC match date & time Sample !D's affected: 12 on bottles? ' Number of containers received match Sample ID's affected: 13 num1'er indicated on COC? / 14 Are sample containers identifiable as ,/ GEL brovided? . 15 COC/orm is properly signed in / relinquished/received sections? ) Circle Applicable: FedEx Air FedEx Ground UPS Field Services Courier Other ' ?-l:Z.. 0 I <'1 'i?D 7 16 Carrier and tracking number. I .. 201G-y1 qq I (e{,Lf J Z by V1 3 IQ Zl/'/ ' i I z o Yl-'13 oi C/SH ' Comments (Use Continuation Form if needed): ' ! i I PM (or PMA) review: Initials 4rL-Date (} ] /17 / I { Page _l_ ofL..-I I GL-CHL-SR-001 Rev 3 Page 21 of 5809 Page 22 of 5809 Data Review Qualifier Definitions Data Review Qualifier Definitions Qualifier Explanation ** < > A quality control analyte recovery is outside of specified acceptance criteria Analyte is a surrogate compound Result is less than value reported Result is greater than value reported RPD of sample and duplicate evaluated using +/-RL. Concentrations are <SX the RL A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank B Metals-Either presence of analyte detected in the associated blank, or MDL/IDL < sample value < PQL BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample d 5-day BOD-The 2:1 depletion requirement was not met for this sample E Organics-Concentration of the target analyte exceeds the instrument calibration range E Metals-%difference of sample and SD is >10%. Sample concentration must meet flagging criteria H Analytical holding time was exceeded h Preparation or preservation holding time was exceeded J Value is estimated N Metals-The Matrix spike sample recovery is not within specified control limits N Organics-Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC) . Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the reporting limit UI Gamma Spectroscopy-Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC.Samples were not spiked with this compound Z Paint Filter Test-Particulates passed through the filter, however no free liquids were observed. Page 23 of 5809 P Organics-The concentrations between the primary and confirmation columns/detectors is >40% difference. For HPLC, the difference is >70%. u Analyte was analyzed for, but not detected above the MDL, MDA, or LOD. Page 24 of 5809 Radiological Analysis Page 25 of 5809 Case Narrative Page 26 of 5809 Radiochemistry Technical Case Narrative MJW Technical Services (MJWC) SDG #: 405235 Product: Alphaspec Th229 + 228,230,232 Solid Analytical Method: DOE EML HASL-300, Th-01-RC Modified Analytical Procedure: GL-RAD-A-038 REV# 17 Analytical Batch: 1596388 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621688 1203621689 1203621690 Client Sample Identification 4.1.B.R. l.2 4.1.B.R. l .3 4.1.B.R.l .4 4.1.B.R.7.2 4.1.C.R. l.3 4.1.C.R.1.4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.l.3 4.1.D.R.l .4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.1.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Page 27of5809 Refer to Miscellaneous Information section. Recounts Sample 405235013 (4.2A.R.2.3) was recounted due to high MDC. The recount is reported. Samples 405235010 (4.l.D.R.1.4) and 405235014 (4.2A.R.l.3) were recounted due to a peak shift. The recounts are reported. Samples 405235001 (4. l.B.R.1.2) and 405235012 (4.l.D.R.2.4) were recounted due to a suspected false positive. The recounts are reported. Miscellaneous Information I. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203621689 were received and analyzed out of holding. 1. Reporting results. Product: ASP Uranium Isotopic, Solid Analytical Method: DOE EML HASL-300, U-02-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1596389 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621691 1203621692 1203621693 Client Sample Identification 4.1.B.R.1.2 4.1.B.R. l .3 4.1.B.R.1.4 4.1.B.R.7.2 4.1.C.R. I .3 4.1.C.R. I .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.l.3 4.1.D.R.l.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) .The samples in this SDG were analyzed on a "dry weight" basis. Page 28 of 5809 Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203621692 (4. l.B.R. l.2DUP) and 405235001 ( 4.1.B.R. l.2), did not meet theU-233/234 relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of2.98. Technical Information Holding Time Refer to Miscellaneous Infonnation section. Miscellaneous Information 1. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203621692 were received and analyzed out of holding. 1. Reporting results. Product: Am241, Cm Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011REV#26 Analytical Batch: 1596390 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 .405235009 405235010 405235011 405235012 405235013 405235014 405235015 Page 29 of 5809 Client Sample Identification 4.1.B.R. l .2 4.1.B.R. l.3 4.1.B.R. l .4 4.1.B.R.7.2 4.1.C.R. l .3 4.1.C.R. l .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.l.3 4.1.D.R. l .4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 405235016 405235017 405235018 405235019 405235020 1203621694 1203621695 1203621696 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Samples 405235011 (4.l.D.R.3.2), 405235015 (4.2A.R. l.4) and 405235016 (4.2A.R.2.4) were recounted due to a peak shift. The recounts are reported. Miscellaneous Information 1. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203621695 were received and analyzed out of holding. 1. Reporting results. Qualifier Information Qualifier Reason The Cm-245/246 Result may be biased X high due to tailing from the Am-243 ROI into the Cm-245/246 ROI Product: Alphaspec Np237, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 21 Page 30 of 5809 Analyte Curium-245/246 Sample Client Sample 405235005 4.1.C.R. l.3 405235012 4.1.D.R.2.4 405235018 4.2A.R.4.2 405235019 4.2B.R.2.4 Analytical Batch: 1596392 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227
The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621697 1203621698 1203621699 Client Sample Identification 4.1.B.R. l.2 4.1.B.R.l.3 4.1.B.R. l.4 4.1.B.R.7.2 4.1.C.R.l.3 4.1.C.R.l.4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.l.3 4.1.D.R. l.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235018, 405235019, 405235020, and 1203621698 were received and analyzed out of holding. I. Reporting results. Page 31 of 5809 Product: ASP Plutonium Isotopic, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1596393 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621700 1203621701 1203621702 Client Sample Identification 4.1.B.R.l.2 4.1.B.R.1.3 4.1.B.R.1.4 4.1.B.R.7.2 4.1.C.R.l.3 4.1.C.R.l .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R. l.3 4.1.D.R.1.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.1.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the acceptance limits with the following exceptions: Refer to Miscellaneous Information section. Technical Information Holding Time Refer to Miscellaneous Information section. Page 32 of 5809 Recounts Sample 1203621702 (LCS) was recounted due to a peak shift. The recount is reported. Miscellaneous Information 1. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203621701 were received and analyzed out of holding. 2. Sample 1203621701 does not meet the resolution requirement of having a full width half maximum of 100 keV or less for the Pu-242 tracer. I. Reporting results. 2. The sample does meet the tracer yield requirement, the detection limits, and its tracer peak is within the Pu-242 region of interest. Reporting results. Product: Alphaspec Th229 + 228,230,232 Solid Analytical Method: DOE EML HASL-300, Th-01-RC Modified Analytical Procedure: GL-RAD-A-038 REV# 17 Analytical Batch: 1596395 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203621706 1203621707 1203621708 Client Sample Identification 4.2B.R.2.3 4.2B.R.1.3 4.2B.R.1 I .2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.1.3 4.2C.R.1.4 4.3.ARl.3 4.3.B.R.1.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.l.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.1.3 4.4C.R.1.4 4.4D.R.1.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Page 33of5809 Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 1203621707 (4.2B.R.2.3DUP) was recounted due to high MDC. The recount is reported. Sample 405235039 (4.4C.R. l .4) was recounted due to a peak shift. The recount is reported. Sample 405235035 (4.3B.R.2.3) was recounted due to detector error. The recount is reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, and 1203621707 were received and analyzed outside of the holding time. 1. Reporting results. Product: ASP Uranium Isotopic, Solid Analytical Method: DOE EML HASL-300, U-02-RC Modified Analytical Procedure: GL-RAD-A-011REV#26 Analytical Batch: 1596396 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 Page 34 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R. l l .2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 405235038 405235039 405235040 1203621709 1203621710 1203621711 4.4C.R.1.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.28.R.2.3) Sample Duplicate (DUP) Laboratoi:y Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203621710 (4.2B.R.2.3DUP) and 405235021 (4.2B.R.2.3), did not meet the U-233/234 and U-238 relative percent difference requirements; however, they do meet the relative error ratio requirements with the values of0.901 and 1.99. respectively. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts The U-232 traced portion of samples 1203621710 (4.2B.R.2.3DUP), 405235022 (4.2B.R.1.3) and 405235023 (4.2B.R.11.2) and the U-236 traced portion of 1203621710 were recounted due to peak shifts. The recounts are reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, and 1203621710 were received and analyzed outside of the holding time. 1. 1. Reporting results. Product: Alphaspec Np237, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 21 Analytical Batch: 1596399 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Sample Identification Page 35 of 5809 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203621715 1203621716 1203621717 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.l l.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.1.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts The batch was recounted due to analyst error. The recounts are reported with the exception of samples 405235026(4.2C.R.l.3) and 1203621716(4.2B.R.2.3). Sample 405235026(4.2C.R.l.3) was recounted due to a high MDA and the third count is reported. Sample 1203621716(4.2B.R.2.3) was recounted due to a peak shift and the third count is reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, and 1203621716 were received and analyzed out of holding. 1. Reporting results. Product: ASP Plutonium Isotopic, Solid Analytical Method: DOE EML _HASL-300, Pu-11-RC Modified Page 36 of 5809 Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1596400 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203621718 1203621719 1203621720 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.l l.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples. in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 405235039 (4.4C.R.l.4) was recounted due to a peak shift. The recount is reported. Sample 405235037 (4.4C.R.2.4) was recounted due to poor resolution. The recount is reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235039,.405235040, and 1203621719 were received and_ analyzed out of holding. I. Reporting Page 37 of 5809 results. Product: Alphaspec Th229 + 228,230,232 Solid Analytical Method: DOE EML HASL-300, Th-01-RC Modified Analytical Procedure: GL-RAD-A-038 REV# 17 Analytical Batch: 1596407 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621736 1203621737 1203621738 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.SB.R.1.2 4.5B.R.l.3 4.SB.R.1.4 4.5B.R.2.3 4.SB.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041 ( 4.4D.R. l .4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Page 38 of 5809 Samples 405235049 (4.5B.R.l.3) and 405235050 (4.5B.R.1.4) were recounted due to a peak shift. The recounts are reported. Samples 405235043 (4.4D.R.2.4), 405235051 (4.5B.R.2.3) and 405235058 (4.5C.R.2.4) were recounted due to a suspected false positive. The recounts are reported. Sample 405235041 ( 4.4D.R.1.4) was recounted to verify results and then recounted again due to a peak shift. The third count is reported. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203621737 were received and analyzed out of holding. 1. Reporting results. Product: ASP Uranium Isotopic, Solid Analytical Method: DOE EML HASL-300, U-02-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1596408 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621739 1203621740 1203621741 Client Sample Identification 4.4D.R.1.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.l.4 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.IA.R.1.2 5.IA.R.l.3 Method Blank (MB) 405235041 ( 4.4D.R.1.4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and < . Page 39 of 5809 procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203621740 (4.4D.R.l.4DUP) and 405235041 (4.4D.R.l.4), did not meet the U-233/234 relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of 1.41. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts The U-232 traced portion of samples 1203621740 (4.4D.R.1.4DUP), 1203621741 (LCS) and 405235055 ( 4.5C.R. l .4) were recounted due to peak shifts. The recounts are reported. The U-236 traced portion of sample 405235041 ( 4.4D.R. I .4) was recounted due to poor resolution. The recount is reported. Miscellaneous Information I. I. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203621740 were received and analyzed out of holding. I. Reporting results. Product: Am241, Cm Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1596410 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 Page 40 of 5809 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.SA.R.1.3 4.5A.R.l.4 4.SB.R.1.2 4.SB.R.1.3 4.SB.R.1.4 4.SB.R.2.3 4.5B.R.2.4 4.5C.R.5.2 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621745 1203621746 1203621747 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Samples 1203621746 (4.4D.R.l.4DUP), 405235042 (4.4D.R.2.3), 405235048 (4.5B.R.l.2), 405235049 (4.5B.R.1.3) and 405235050 (4.5B.R.l.4) were recounted due to a peak shift. The recounts are reported. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203621746 were received and analyzed out of holding. 1. Reporting results. Product: Alphaspec Np237, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 21 Analytical Batch: 1596411 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 Page 41of5809 Client Sample Identification 4.4D.R.1.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621748 1203621749 1203621750 4.5A.R.l.3 4.5A.R.1.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.l.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Samples 405235051 (4.5B.R.2.3) and 405235056 (4.5C.R.2.2) were recounted due to high MDCs. The recounts are reported. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203621749 were received and analyzed out of holding. 1. Reporting results. Product: ASP Plutonium Isotopic, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011REV#26 . Analytical Batch: 1596412 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 Page 42. of 5809 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621751 1203621752 1203621753 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.1.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.1.3 4.5B.R.1.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.IA.R.1.3 Method Blank (MB) 405235041 ( 4.4D.R. l .4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information l.Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203621752 were received and analyzed out of holding. 2. The Pu-242 tracer peak centroid for sample 405235047 is greater than 50 keV from the expected energy value of 4890 keV. 1. Reporting results. 2. The sample does meet the tracer yield requirement, the detection limits, and its tracer peak is within the Pu-242 region of interest. Reporting results. Product: Alphaspec Th229 + 228,230,232 Solid Analytical Method: DOE EML HASL-300, Th-01-RC Modified Analytical Procedure: GL-RAD-A-038 REV# 17 Page 43 of 5809 Analytical Batch: 1596417 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 . . The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203621757 1203621758 1203621759 Client Sample Identification 5.lB.R.2.2 5.2.A.R.l.2 5 .2 .A.R.1.3 5.2.A.R.l.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R. l .4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Samples 1203621757 (MB), 1203621759 (LCS) and 405235077 (5.5A.R.1.3) were recounted due to a peak shift. The recounts are reported. Miscellaneous Information 1. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203621758 were received and analyzed out of holding. 1. Reporting results. Page 44 of 5809 Product: ASP Uranium Isotopic, Solid Analytical Method: DOE EML HASL-300, U-02-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1596418 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203621760 1203621761 1203621762 Client Sample Identification 5.lB.R.2.2 5 .2.A.R.1.2 5.2.A.R. l .3 5 .2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.1.3 5.4A.R.1.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts The U-232 traced portion of sample 405235064 (5.2.A.R. l .4) was recounted due to a peak shift. The recount is reported. Miscellaneous Information Manual Integration Page 45 of 5809 Manual integrations of alpha spectroscopy spectra 405235067 (5.2A.R.6.2), 405235070 (5.2.B.R.3.2), 405235072 (5.2.B.R.2.4) and 405235077 (5.5A.R. l .3) were performed to fully separate counts in Regions of Interest which would have been biased. 1. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203621761 were received and analyzed out of holding. 1. Reporting results. Product: Alphaspec Np237, Solid Analytical Method: ASTM C 1475-00 Modified Analytical Procedure: GL-RAD-A-032 REV# 21 Analytical Batch: 1596420 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203621766 1203621767 1203621768 Client Sample Identification 5.IB.R.2.2 5 .2.A.R.1.2 5 .2.A.R.1.3 5 .2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5 .2.B.R.1.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R. l .3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.IB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Page 46 of 5809 Holding Time Refer to Miscellaneous Information section. Miscellaneous Information l.Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203621767 were received and analyzed out of holding. 1. Reporting results. Product: ASP Plutonium Isotopic, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-011REV#26 Analytical Batch: 1596421 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203621769 1203621770 1203621771 Client Sample Identification 5.lB.R.2.2 5 .2.A.R.1.2 5 .2.A.R.1.3 5.2.A.R. l .4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R. l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Page 47 of 5809 Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Sall1ples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203621770 were analyzed outside ofholding. 1. Reporting results. Product: Am241, Cm Solid Analytical Method: DOE EML HASL-300, All1-05-RC Modified Analytical Procedure: GL-RAD-A-011REV#26 Analytical Batch: 1599981 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596246 The following sall1ples were analyzed using the above ll1ethods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203630763 1203630764 1203630765 Client Sample Identification 5.lB.R.2.2 5.2.A.R. l .2 5.2.A.R. l .3 5.2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.1.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.1.3 5.4A.R.1.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sall1ple Duplicate (DUP) Laboratory Control Sall1ple (LCS) The sall1ples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sall1ple data provided in this report ll1et the acceptance criteria specified in the analytical ll1ethods and procedures for initial calibration, continuing calibration, instrull1ent controls and process controls where applicable, with the following exceptions. Page 48 of 5809 Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The Cm-245/246 blank result is greater than the MDC but less than the detection limit. Technical Information Holding Time Refer to Miscellaneous Information section. Sample Re-prep/Re-analysis Samples were reprepped due to low carrier/tracer yield. The re-analysis is being reported. Miscellaneous Information 1. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203630764 were received and analyzed out of holding. 1. Reporting results. Qualifier Information Qualifier Reason The Cm-245/246 result may be biased X high due to tailing from the Am-243 ROI. Product: ASP Uranium Isotopic, Solid Analyte Curium-245/246 Analytical Method: DOE EML HASL-300, U-02-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1601257 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 Sample 405235062 405235064 405235068 405235077 1203630763 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235051 1203633742 1203633743 Page 49 of 5809 Client Sample Identification 4.SB.R.2.3 Method Blank (MB) 405235051(4.5B.R.2.3) Sample Duplicate (DUP) Client Sample 5.2.A.R.l.2 5.2.A.R.1.4 5.2A.R.4.2 5.5A.R.l.3 MB for batch 1599981 1203633744 Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: . . All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203633743 (4.5B.R.2.3DUP) and 405235051 (4.5B.R.2.3), did not meet the U-233/234 relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of 1.22. The U-233/234, U-235/235, and U-238 blank activities are greater than the MDC but is less than five percent of the lowest activity in the batch. Technical Information Holding Time Refer to Miscellaneous Information section. Sample Re-prep/Re-analysis Sample 405235051 (4.5B.R.2.3) was reprepped due to low carrier/tracer yield. The re-analysis is being reported. Miscellaneous Information 1. Samples 405235051 and 1203633743 were received and analyzed out of holding. 1. Reporting results. Product: Am241, Cm Solid Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Procedure: GL-RAD-A-011 REV# 26 Analytical Batch: 1602285 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 Page 50 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R. l l .2 4.2B.R.2.2 . 4.2B.R. l .2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARl.3 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203636290 1203636291 1203636292 4.3 .B.R.1.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.l.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The Cm-245/246 blank result is greater than the MDC but less than the detection limit. Technical Information Holding Time Refer to Miscellaneous Information section. Sample Re-prep/Re-analysis Samples were reprepped due to low carrier/tracer yield. The re-analysis is being reported. Recounts Sample 405235037 (4.4C.R.2.4) was recounted due to a peak shift. The recount is reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,40523531,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, and 1203636291 were received and analyzed out of holding. 1. Reporting results. Qualifier Information Qualifier Reason Page 51of5809 Analyte Sample Client Sample x The Cm-245/246 Result may be biased high due to tailing from the Am-243 ROI into the Cm-245/246 ROI Curium-245/246 405235021 Product: Dry Weight Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596227 405235025 405235028 405235031 405235036 1203636290 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621316 Client Sample Identification 4.1.B.R. l .2 4.1.B.R.1.3 4.1.B.R. l.4 4.1.B.R.7.2 4.1.C.R. l.3 4.1.C.R.1.4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.1.3 4.1.D.R.1.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.1.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.1.4 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) The samples in this SDG were analyzed on an "as received" basis. Data Summary: 4.2B.R.2.3 4.2B.R.l.2 4.3.ARl.3 4.3.BR19.2 4.3B.R.2.4 MB for batch 1602285 There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Page 52 of 5809 Product: Dry Weight Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203621317 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.l l.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.1.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 405235021(4.2B.R.2.3) Sample Duplicate (DUP) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Dry Weight Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 Page 53 of 5809 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621322 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.l.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.IA.R.1.3 405235041(4.4D.R.l.4) Sample Duplicate (DUP) The samples in this SDG were analyzed on an "as received" basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Dry Weight Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 Page 54 of 5809 Client Sample Identification 5.IB.R.2.2 5.2.A.R.l.2 5 .2.A.R.1.3 5 .2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.l.3 5.4A.R.l.3 405235076 405235077 405235078 1203621353 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 405235061(5.lB.R.2.2) Sample Duplicate (DUP) The samples in this SDG were analyzed on an "as received". basis. Data Summary: There are no exceptions, anomalies or deviations from the specified methods. All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable. Product: Gammaspec, Gamma, Solid Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 25 Analytical Batch: 1596247 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621350 1203621351 1203621352 Client Sample Identification 4.1.B.R. l .2 4.1.B.R. l .3 4.1.B.R.l .4 4.1.B.R.7.2 4.1.C.R.l.3 4.1.C.R. l .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R. l.3 4.1.D.R.l.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Page 55 of 5809 Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203621351 (4.l.B.R.l.2DUP) and 405235001 (4.l.B.R.1.2), did not meet the Cs-137 and Tl-208 relative percent difference requirement; however, they do meet the relative error ratio requirement with a values of 1.46 and 2.08 respectively. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Samples 405235 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013, 014, 015, 016, 017, 018, 019, 020, and 1203621351 (duplicate) were received outside of the holding period. Samples were analyzed in a timely manner upon receipt. Reporting results. Qualifier Information Qualifier UI UI Page 56 of 5809 Reason Data rejected due to high peak-width. Data rejected due to interference. Analyte Bismuth-212 Cesium-137 Protactinium-231 Sample 405235020 405235002 405235002 405235004 405235005 405235006 405235007 405235009 405235011 405235013 405235014 405235015 405235017 Client Sample 4.2B.R.l.4 4.1.B.R.l.3 4.1.B.R. l.3 4.l.B.R.7.2 4.1.C.R. l.3 4.1.C.R.l.4 4.1.C.R.2.3 4.1.D.R. l.3 4.1.D.R.3.2 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.3.2 405235018 4.2A.R.4.2 405235019 4.2B.R.2.4 Tin-126 405235002 4.1.B.R. l.3 405235003 4.1.B.R.l .4 405235004 4.1.B.R.7.2 405235005 4.1.C.R.l.3 405235006 4.1.C.R.1.4 405235009 4.1.D.R.1.3 405235011 4.1.D.R.3.2 405235012 4.1.D.R.2.4 405235013 4.2A.R.2.3 405235015 4.2A.R.1.4 405235017 4.2A.R.3.2 405235018 4.2A.R.4.2 405235020 4.2B.R.1.4 1203621351 4.1.B.R.1.2(405235001DUP) UI Data rejected due to Antimony-125 1203621351 4.1.B.R.1.2( 40523500 lDUP) low abundance. Bismuth-212 405235001 4.1.B.R.l.2 405235002 4.1.B.R. l.3 405235004 4.1.B.R.7.2 405235005 4.1.C.R.l.3 405235007 4.1.C.R.2.3 405235009 4.1.D.R. l.3 405235010 4.1.D.R. l.4 405235011 4.1.D.R.3.2 405235012 4.1.D.R.2.4 405235013 4.2A.R.2.3 405235014 4.2A.R.l.3 405235015 4.2A.R.1.4 405235016 4.2A.R.2.4 405235018 4.2A.R.4.2 405235019 4.2B.R.2.4 Page 57 of 5809 Cobalt-60 Protactinium-231 Tin-126 Product: Gammaspec, Gamma, Solid Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 25 Analytical Batch: 1596249 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 405235020 4.2B.R.1.4 405235006 4.1.C.R.1.4 405235007 4.1.C.R.2.3 405235010 4.1.D.R.1.4 405235015 4.2A.R.1.4 405235003 4.1.B.R.l.4 405235001 4.1.B.R.l.2 405235010 4.1.D.R.1.4 405235014 4.2A.R.1.3 405235016 4.2A.R.2.4 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203621354 1203621355 1203621356 Page 58 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.l l.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.1.4 4.4D.R.l.3 Method Blank (MB) 405235038( 4.4C.R. l .3) Sample Duplicate (DUP) Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls.and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203621355 (4.4C.R.l.3DUP) and 405235038 (4.4C.R.l.3), did not meet the Bi-214/Ra-226 and Pb-214 relative percent difference requirement; however, they do meet the relative error ratio requirement with a values of 1.78 and 2.36 respectively. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Samples 405235 021, 022, 023, 024, 025, 026, 027, 028, 029, 030, 031, 032, 033, 034, 035, 036, 037, 038, 039, 040, and 1203621355 (duplicate) were received outside of the holding period. Samples were analyzed in a timely manner upon receipt. Reporting results. Qualifier Information Qualifier UI UI UI Page 59 of 5809 Reason Data rejected due to high counting uncertainty. Data rejected due to high peak-width. Data rejected due to interference. Analyte Cesium-137 Bismuth-212 Protactinium-231 Sample Client Sample 1203621355 4.4C.R.l.3(405235038DUP) 405235023 4.2B.R. l l .2 405235021 4.2B.R.2.3 405235022 4.2B.R.l.3 405235023 4.2B.R. l l .2 405235024 4.2B.R.2.2 405235025 4.2B.R.l.2 405235026 4.2C.R.l.3 405235027 4.2C.R.l.4 405235028 4.3.ARl.3 405235029 4.3 .B.R.1.3 405235030 4.3A.R.2.3 405235032 4.3B.R.3.3 405235033 4.3B.R.3.4 405235034 4.3.B.R.1.4 405235035 4.3B.R.2.3 405235036 4.3B.R.2.4 405235037 4.4C.R.2.4 405235038 4.4C.R.1.3 405235039 4.4C.R.1.4 1203621355 4.4C.R. l .3( 405235038DUP) Tin-126 405235021 4.2B.R.2.3 405235022 4.2B.R.l.3 405235023 4.2B.R. l l.2 405235024 4.2B.R.2.2 405235026 4.2C.R.1.3 405235027 4.2C.R.l.4 405235029 4.3.B.R.l.3 405235030 4.3A.R.2.3 405235031 4.3.BR19.2 405235032 4.3B.R.3.3 405235033 4.3B.R.3.4 405235035 4.3B.R.2.3 405235036 4.3B.R.2.4 405235037 4.4C.R.2.4 405235038 4.4C.R.l.3 UI Data rejected due to low Actinium-227 405235023 4.2B.R.l 1.2 abundance. Bismuth-212 405235022 4.2B.R.1.3 405235024 4.2B.R.2.2 405235025 *4.2B.R.1.2 405235026 4.2C.R.l.3 405235027 4.2C.R.l.4 Page 60 of 5809 Cesium-137 Europium-154 Protactinium-231 Tin-126 Product: Gammaspec, Gamma, Solid Analytical Method: DOE HASL 300, 4.5.2.3/Ga-01-R Analytical Procedure: GL-RAD-A-013 REV# 25 Analytical Batch: 1596252 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 405235030 405235033 405235034 405235036 405235037 405235038 405235039 1203621355 405235027 405235039 405235022 405235029 405235040 405235025 4.3A.R.2.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.1.4 4.4C.R.l.3(405235038DUP) 4.2C.R.l.4 4.4C.R.l.4 4.2B.R.l.3 4.3.B.R.l.3 4.4D.R.l.3 4.2B.R.l.2 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 Page 61 of 5809 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.1.2 4.5B.R.l.3 4.5B.R.1.4 4.SB.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.1.3 4.5C.R.l.4 4.SC.R.2.2 405235057 405235058 405235059 405235060 1203621361 1203621362 1203621363 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) S&mple Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Sample received out of holding for sample 405235041, sample 405235042, sample 405235043, sample 405235044, sample 405235045, sample 405235046, sample 405235047, sample 405235048, sample 405235049, sample 405235050, sample 405235051, sample 405235052, sample 405235053, sample 405235054, sample 405235055, sample 405235056, sample 405235057, sample 405235058, sample 405235059, sample 405235060 and DUP 1203621362 Samples were analyzed as soon as possible. Reporting results. Qualifier Information Qualifier Reason Analyte Sample Client Sample Data rejected due to UI high counting Cesium-137 405235041 4.4D.R.l.4 uncertainty. 1203621362 4.4D.R.l.4(405235041DUP) Protactinium-231 405235042 4.4D.R.2.3 405235046 4.5A.R.l.3 405235051 4.5B.R.2.3 405235052 4.5B.R.2.4 405235053 4.5C.R.5.2 Tin-126 405235045 4.4D.R.5.2 405235058 4.5C.R.2.4 UI Data rejected due to Antimony-125 405235050 4.5B.R.l.4 high peak-width. Page 62 of 5809 Bismuth-212 405235053 4.5C.R.5.2 Protactinium-231 405235056 4.5C.R.2.2 Tin-126 405235047 4.5A.R.l.4 405235048 4.5B.R.l.2 405235049 4.5B.R.l.3 UI Data rejected due to Protactinium-231 405235041 4.4D.R.l.4 interference. 405235043 4.4D.R.2.4 405235047 4.5A.R.l.4 405235049 4.5B.R.l.3 Tin-126 405235043 4.4D.R.2.4 405235046 4.5A.R.l.3 405235050 4.5B.R.l.4 405235051 4.5B.R.2.3 405235052 4.5B.R.2.4 405235053 4.5C.R.5.2 405235054 4.5C.R.l.3 405235055 4.5C.R.l.4 405235056 4.5C.R.2.2 405235057 4.5C.R.2.3 405235059 5.IA.R.1.2 405235060 5.IA.R.1.3 1203621362 4.4D.R. I .4( 40523504 IDUP) UI Data rejected due to low Antimony-125 405235048 4.5B.R.l.2 abundance. 405235054 4.5C.R.l.3 Bismuth-212 405235041 4.4D.R.l.4 405235042 4.4D.R.2.3 405235044 4.4D.R.4.2 405235047 4.5A.R.l.4 405235048 4.5B.R.l.2 405235049 4.5B.R.l.3 405235050 4.5B.R.l.4 Page 63 of 5809 UI Data rejected due to no valid peak. Product: Gammaspec, Gamma, Solid Cesium-137 Europium-154 Protactinium-231 Radium-228 Tin-126 Cesium-137 Analytical Method: DOE HASL 300, 4.5.2.3/Ga-Ol-R Analytical Procedure: GL-RAD-A-013 REV# 25 Analytical Batch: 1596254 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596246 405235051 4.5B.R.2.3 405235052 4.5B.R.2.4 405235054 4.5C.R.l.3 405235055 4.5C.R.l.4 405235056 4.5C.R.2.2 405235057 4.5C.R.2.3 405235059 5.lA.R.1.2 405235060 5.lA.R.1.3 1203621362 4.4D.R.l.4(405235041DUP) 405235047 4.5A.R.l.4 405235058 4.5C.R.2.4 405235058 4.5C.R.2.4 405235044 4.4D.R.4.2 405235045 4.4D.R.5.2 405235055 4.5C.R.l.4 405235042 4.4D.R.2.3 405235051 4.5B.R.2.3 405235044 4.4D.R.4.2 405235050 4.5B.R.l.4 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 Page 64 of 5809 Client Sample Identification 5.lB.R.2.2 5.2.A.R.l.2 5.2.A.R.l.3 5.2.A.R.l.4 5.2A.R.2.3 5.2.A.R.2.4 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203621364 1203621365 1203621366 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R. l.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.IB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate 1203621365 (5.1B.R.2.2DUP) and 405235061 (5.IB.R.2.2) did not meet the relative' percent difference requirement for Bi-214/Ra-226; however, they do meet the relative error ratio requirement(0-3) with a value of 2.02. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Sample received and analyzed out of holding: 405235061,062,063,064,065,066,067,068,069, 070,071,072,073,074,075,076,077,078, 1203621365DUP 1. Reporting Results Qualifier Information Page 65 of 5809 Qualifier Reason Data rejected due to UI higl;t counting uncertainty. Analyte Bismuth-212 Cesium-137 Sample 405235069 405235071 405235068 Client Sample 5.2.B.R.4.2 5.2A.R.4.2 405235070 5.2.B.R.3.2 Protactinium-231 405235067 5.2A.R.6.2 405235071 5.2.B.R.4.2 1203621365 5.1B.R.2.2(405235061DUP) Tin-126 405235063 5.2.A.R.1.3 405235064 5 .2.A.R.1.4 405235065 5.2A.R.2.3 405235066 5.2.A.R.2.4 405235067 5.2A.R.6.2 405235068 5.2A.R.4.2 405235071 5.2.B.R.4.2 405235073 5.2.B.R.8.2 405235077 5.5A.R.1.3 UI Data rejected due to Cesium-137 405235071 5.2.B.R.4.2 high peak-width. 405235076 5.4A.R.4.2 Protactinium-231 405235074 5.3.A.R.1.3 Tin-126 405235078 5.6A.R.1.3 UI Data rejected due to Protactinium-231 405235061 5.lB.R.2.2 interference. 405235063 5.2.A.R.1.3 405235064 5.2.A.R.1.4 405235065 5.2A.R.2.3 405235066 5.2.A.R.2.4 405235069 5.2.B.R.1.4 405235076 5.4A.R.4.2 UI Data rejected due to low Bismuth-212 405235061 5.lB.R.2.2 abundance. 405235063 5.2.A.R.1.3 405235064 5.2.A.R.1.4 405235065 5.2A.R.2.3 405235066 5.2.A.R.2.4 405235067 5.2A.R.6.2 405235070 5.2.B.R.3.2 Page 66 of 5809 UI Data rejected due to no valid peak. Product: Gamma 1129, Solid Cesium-137 Europium-154 Radium-228 Tin-126 Cesium-137 Analytical Method: DOE EML HASL-300,1-01 Modified Analytical Procedure: GL-RAD-A-006 REV# 21 Analytical Batch: 1598618 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596227 405235072 405235073 405235074 405235076 405235077 405235078 1203621365 405235066 1203621365 405235061 405235073 1203621364 405235072 1203621365 405235062 405235067 1203621364 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R. l .3 5.4A.R.4.2 5.5A.R.1.3 5.6A.R.1.3 5 .1B.R.2.2(40523506 lDUP) 5.2.A.R.2.4 5 .1B.R.2.2(40523506 lDUP) 5.lB.R.2.2 5.2.B.R.8.2 MB for batch 1596254 5.2.B.R.2.4 5.1B.R.2.2(405235061DUP) 5.2.A.R.l.2 5.2A.R.6.2 MB for batch 1596254 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 Page 67 of 5809 Client Sample Identification 4.1.B.R. l.2 4.1.B.R.l.3 4.1.B.R. l.4 4.1.B.R.7.2 4.1.C.R.l.3 4.1.C.R.l .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R. l.3 4.1.D.R.l.4 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203627430 1203627431 1203627432 1203627433 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.1.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.1.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) 405235001(4.1.B.R.l.2) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Samples received out of holding: 405235 001,002,003,004,005,006,007,008,009, 010,0l l,012,013,014,015,016,017,018, 019,020 QC 1203627431DUP,1203627432MS Samples were counting in a timely manner upon receipt. Reporting results. Qualifier Information Qualifier Reason UI Data rejected due to high counting uncertainty. UI Data rejected due to low abundance. Product: Gamma 1129, Solid Analytical Method: DOE EML HASL-300,1-01 Modified Analytical Procedure: GL-RAD-A-006 REV# 21 Analytical Batch: 1598620 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Page 68 of 5809 Analyte Sample Client Sample Iodine-129 405235017 4.2A.R.3.2 405235015 4.2A.R.1.4 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203627437 1203627438 1203627439 1203627440 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R. l l.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.28.R.2.3) Sample Duplicate (DUP) 405235021(4.28.R.2.3) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Sample received out of holding: 405235 021,022,023,024,025,026,027,028,029, 030,031,032,033,034,035,036,037,038, 039,040 QC 1203627438DUP,1203627439MS Samples were analyzed in a timely manner upon receipt. Reporting results. Qualifier Information Qualifier Reason Analyte Sample Client Sample Page 69 of 5809 UI Data rejected due to low abundance. Iodine-129 405235034 4.3.B.R.l.4 Product: Gamma 1129, Solid Analytical Method: DOE EML HASL-300,1-01 Modified Analytical Procedure: GL-RAD-A-006 REV# 21 Analytical Batch: 1598647 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203627502 1203627503 1203627504 1203627505 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.l.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.SC.R.1.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.IA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) Sample Duplicate (DUP) 405235041(4.4D.R.1.4) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Page 70 of 5809 Recounts Sample 1203627505 (LCS) was recounted due to high recovery. The recount is reported. Miscellaneous Information Sample received out of holding: 405235 041,042,043,044,045,046,047,048,049, 050,051,052,053,054,055,056,057,058, 059,060 QC 1203627503DUP,1203627504MS Samples analyzed in a timely manner upon receipt. Reporting results. Product: Gamma 1129, Solid Analytical Method: DOE EML HASL-300,1-01 Modified Analytical Procedure: GL-RAD-A-006 REV# 21 Analytical Batch: 1598663 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068. 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203627531 1203627532 1203627533 1203627534 Client Sample Identification 5.IB.R.2.2 5.2.A.R. l .2 5.2.A.R. l .3 5.2.A.R.l.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l .4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R. l .3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.IB.R.2.2) Sample Duplicate (DUP) 405235061(5.IB.R.2.2) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Page 71 of 5809 Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information Sample received out of holding: 405235 061,062,063,064,065,066,067,068,069, 070,071,072,073,074,075,076,077,078, QC 1203627532DUP,1203627533MS Samples were analyzed in a timely manner upon receipt. Reporting results. Qualifier Information Qualifier Reason Analyte UI Data rejected due to high counting lodine-129 uncertainty. Product: GFPC, Sr90, solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. I Modified Analytical Procedure: GL-RAD-A-004 REV# 17 Analytical Batch: 1597795 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 Sample 405235061 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 ' 405235015 405235016. 405235017 405235018 405235019 Page 72 of 5809 Client Sample Identification 4.1.B.R. l.2 4.1.B.R. l.3 4.1.B.R. I .4 4.l.B.R.7.2 4. l.C.R.1.3 4.1.C.R. I .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.1.3 4.1.D.R. l .4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 Client Sample 5.lB.R.2.2 405235020 1203625398 1203625399 1203625400 4.2B.R.l.4 Method Blank (MB) 405235005(4.1.C.R. l .3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG wer.e analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 405235002 (4.1.B.R. l .3) was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information I. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203625399 were received and analyzed out of holding. 1. Reporting results Product: GFPC, Sr90, solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 17 Analytical Batch: 1597796 Preparation Method: ASTM D 22.16 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 Page 73 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.1 l .2 4.2B.R.2.2 4.2B.R.1.2 4.2C.R.l.3 4.2C.R.1.4 4.3.ARl.3 4.3 .B.R.1.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203625401 1203625402 1203625403 4.3B.R.3.4 4.3.B.R.l .4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.1.4 4.4D.R.1.3 Method Blank (MB) 405235025( 4.2B.R. l .2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous I11formation section. Recounts Samples 405235025 (4.2B.R.l.2) and 405235033 (4.3B.R.3.4) were recounted due to results more negative than the three sigma TPU. The second counts are reported. Sample 405235024 (4.2B.R.2.2) was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, and 12036254402 were received and analyzed out of holding. I. Reporting results Product: GFPC, Sr90, solid Analytical Method: EPA 905.0 Modified/DOE RP501Rev.1 Modified Analytical Procedure: GL-RAD-A-004 REV# 17 Analytical Batch: 1597803 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 Page 74 of 5809 Client Sample ldentificatiOn 4.4D.R.1.4 4.4D.R.2.3 4.4D.R.2.4 405235044 405235045 405235046 405235047 405235048 40,5235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203625408 1203625409 1203625410 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.l.2 4.SB.R.1.3 4.5B.R.1.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.1.3 4.5C.R.1.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235045(4.4D.R.5.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical mefuods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 405235053 (4.5C.R.5.2) was recounted due to high MDC. The recount is reported. Samples 405235057 (4.5C.R.2.3) and 405235058 (4.5C.R.2.4) were recounted due to results more negative than the three sigma TPU. The second counts are reported. Sample 405235044 (4.4D.R.4.2) was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203625409 were received and analyzed out of holding. 1. Reporting results Product: GFPC, Sr90, solid Analytical Method: EPA 905.0 Modified/DOE RP501 Rev. 1 Modified Analytical Procedure: GL-RAD-A-004 REV# 17 Analytical Batch: 1597804 Page 75 of 5809 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203625412 1203625413 1203625414 Client Sample Identification 5.IB.R.2.2 5 .2.A.R.1.2 5 .2.A.R.1.3 5 .2.A.R.1.4 5.2A.R.2.3 5 .2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l .4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.1.3 Method Blank (MB) 405235065(5.2A.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 1203625414 (LCS) was recounted due to low recovery. The recount is reported. Samples 405235063 (5.2.A.R.l.3), 405235064 (5.2.A.R.l.4), 405235066 (5.2.A.R.2.4), 405235067 (5.2A.R.6.2), 405235070 (5.2.B.R.3.2), 405235074 (5.3.A.R. l.3) and 405235076 (5.4A.R.4.2) were recounted due to results more negative than the three sigma TPU. The second counts are reported. Sample 1203625413 (5.2A.R.2.3DUP) was recounted due to a suspected false positive. The recount is reported. Miscellaneous Information. I. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, and 405235078 were received and analyzed out of holding. I. Reporting results Page 76 of 5809 Product: GFPC, Gross A/B, solid Analytical Method: EPA 900.0/SW846 931 O/SM 711 OB Modified Analytical Procedure: GL-RAD-A-OOIB REV# 17 Analytical Batch: 1597811 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203625435 1203625436 1203625437 1203625438 1203625439 Client Sample Identification 4.2B.R.2.3 4.2B.R.1.3 4.2B.R.1 l.2 4.2B.R.2.2 4.2B.R.1.2 4.2C.R.l.3 4.2C.R.1.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.1.4 4.4D.R.1.3 Method Blank (MB) 405235033(4.3B.R.3.4) Sample Duplicate (DUP) 405235033(4.38.R.3.4) Matrix Spike (MS) 405235033(4.38.R.3.4) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions . . Technical Information Holding Time

Refer to Miscellaneous Information section. Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture Page 77 of 5809 absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes ofcarbon, hydrogen, technetium, polonium and cesium may be lost during sample heating. Miscellaneous Information l.Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, 1203625436, 1203625437, and 1203625438 were received and analyzed out of holding. I. Reporting results Product: GFPC, Gross A/B, solid Analytical Method: EPA 900. O/SW846 931 O/SM 711 OB Modified Analytical Procedure: GL-RAD-A-OOIB REV# 17 Analytical Batch: f597816 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203625449 1203625450 1203625451 1203625452 1203625453 Client Sample Identification 4.1.B.R.l.2 4.1.B.R.l.3 4.1.B.R.1.4 4.1.B.R.7.2 4.1.C.R.l .3 4.1.C.R.l.4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R. l.3 4.1.D.R.1.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.1.3 4.2A.R.1.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235013(4.2A.R.2.3) Sample Duplicate (DUP) 405235013(4.2A.R.2.3) Matrix Spike (MS) 405235013(4.2A.R.2.3) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS)
The samples in this SDG were analyzed on a "dry weight" basis. Page 78 of 5809 Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating. Recounts Samples 1203625451 (4.2A.R.2.3MS) and 1203625452 (4.2A.R.2.3MSD) were recounted due to high recovery. The recounts are reported. Samples 1203625450 (4.2A.R.2.3DUP) and 405235013 (4.2A.R.2.3) were recounted due to high relative percent difference/relative error ratio. The recounts are reported. Miscellaneous Information 1. Samples 405235001, 405235002, 405235003, 405235004, 405235005, 405235006, 405235007, 405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, 1203625450, 1203625451, and 1203625452 were received and analyzed out of holding. 1. Reporting results Product: GFPC, Gross A/B, solid Analytical Method: EPA 900.0/SW846 931 O/SM 711 OB Modified Analytical Procedure: GL-RAD-A-OOIB REV# 17 Analytical Batch: 1597817 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 Page 79 of 5809 Client Sample Identification 5.IB.R.2.2 5.2.A.R.1.2 5 .2.A.R.1.3 5.2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5 .2.B.R.1.4 5.2.B.R.3.2 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203625459 1203625460 1203625461 1203625462 1203625463 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R. l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.1.3 5.6A.R.l.3 Method Blank (MB) 405235073(5.2.B.R.8.2) Sample Duplicate (DUP) 405235073(5.2.B.R.8.2) Matrix Spike (MS) 405235073(5.2.B.R.8.2) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: The sample and the duplicate, 1203625460 (5.2.B.R.8.2DUP) and 405235073 (5.2.B.R.8.2), did not meet the alpha relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of 1.5705. The sample and the duplicate, 1203625460 (5.2.B.R.8.2DUP) and 405235073 (5.2.B.R.8.2), did not meet the beta relative percent difference requirement; however, they do meet the relative error ratio requirement with a value of2.7267. Technical Information Holding Time Refer to Miscellaneous Information section. Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating. Recounts Sample 1203625461 (5.2.B.R.8.2MS) was recounted due to low recovery. The recount is reported. Miscellaneous Information 1. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, 1203625460, 1203625461, and 1203625462 were received and analyzed out of holding. I. Reporting results Page 80 of 5809 Product: GFPC, Gross A/B, solid Analytical Method: EPA 900.0/SW846 93 IO/SM 71 IOB Modified Analytical Procedure: GL-RAD-A-OOIB REV# 17 Analytical Batch: 1602427 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203636653 1203636654 1203636655 1203636656 1203636657 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.SA.R.1.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.l.4 4.SB.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.SC.R.1.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.IA.R.1.2 5.IA.R.1.3 Method Blank (MB) 405235045(4.4D.R.5.2) Sample Duplicate (DUP) 405235045(4.4D.R.5.2) Matrix Spike (MS) 405235045(4.4D.R.5.2) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Sample Re-prep/Re-analysis Samples were reprepped due to low recovery. The re-analysis is being reported. Page 81of5809 Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating. Recounts Samples 1203636655 (4.4D.R.5.2MS) and 1203636656 (4.4D.R.5.2MSD) were recounted due to high recovery. The recounts are reported. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, and 405235060 were received and analyzed out of holding. 1. Reporting results Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 17 Analytical Batch: 1596394 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203621703 1203621704 1203621705 Page 82of5809 Client Sample Identification 4.1.B.R. l .2 4.1.B.R. l .3 4.1.B.R.l.4 4.1.B.R.7.2 4.1.C.R. l .3 4.1.C.R.1.4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.1.3 4.1.D.R.1.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.1.3 4.2A.R.1.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.1.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS)

The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this rep_ort met the acceptance criteria specified in the analytical methods and. procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Samples 1203621704 (4. l .B.R. l .2DUP), 405235003 ( 4.1.B.R. l .4), 405235004 ( 4.1.B.R. 7 .2) and 405235011 (4.l.D.R.3.2) were recounted due to high MDCs. The recounts are reported. Samples 405235006 (4.l.C.R.1.4) and 405235018 (4.2A.R.4.2) were recounted due to results more negative than the three sigma TPU. The second counts are reported. Miscellaneous Information 1. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203621704 were received and analyzed out of holding. 2. Sample 1203621704 does not meet the resolution requirement of having a full width half maximum of 100 keV or less for the Pu-242 tracer. 1. Reporting results. 2. The sample does meet the tracer yield requirement, the detection limits, and its tracer peak is within the Pu-242 region of interest. Reporting results. Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 17 Analytical Batch: 1596402 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 Page 83 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R. l 1.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.1.4 4.3.ARl.3 4.3.B.R. l.3 4.3A.R.2.3 4.3.BR19.2 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203621725 1203621726 1203621727 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.l.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where . applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 1203 621726 ( 4.2B .R.2.3DUP) was recounted due to results more negative than the three sigma TPU. The second count is reported. Samples 405235023 (4.2B.R.l l.2), 405235024 (4.2B.R.2.2), 405235025 ( 4.2B.R. l .2) and 405235039 ( 4.4C.R. l .4) were recounted due to a suspected false positive. The recounts are reported. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, and 1203621726 were received and analyzed out of holding. I. Reporting results. Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 17 Analytical Batch: 1596414 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 Page 84 of 5809 Client Sample Identification 4.4D.R.l.4 405235042 405235043 405235044 405235045 405235046 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203621754 1203621755 1203621756 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.1.2 4.5B.R.l.3 4.5B.R.l.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, and 1203621752 were received and analyzed out of holding. 2. The Pu-242 tracer peak centroid for sample 405235047 is greater than 50 keV from the expected energy value of 4890 keV. 1. Reporting results. 2. The sample does meet the tracer yield requirement, the detection limits, and its tracer peak is within the Pu-242 region of interest. Reporting results. Product: Liquid Scint Pu241, Solid Analytical Method: DOE EML HASL-300, Pu-11-RC Modified Analytical Procedure: GL-RAD-A-035 REV# 17 Analytical Batch: 1596422 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Page 85 of 5809 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203621772 1203621773 1203621774 Client Sample Identification 5.lB.R.2.2 5 .2.A.R.1.2 5.2.A.R.l.3 5.2.A.R.l.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l.4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.1.3 5.4A.R.l.3 5.4A.R.4.2 5.SA.R.1.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Quality Control (QC) Information QC Information All of the QC samples meet the required acceptance limits with the following exceptions: Refer to Miscellaneous Information section. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 405235069,405235070,40523507l,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203621773 were received and analyzed out of holding. 2. Sample 1203621774 does not meet the resolution requirement of having a full width half maximum of 100 ke V or less for the Pu-242 tracer. 1. Reporting results. 2. The sample does meet the tracer yield requirement, the detection limits, and its tracer peak is within the Pu-242 region of interest. Reporting results. Page 86 of 5809 Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 4 Analytical Batch: 1597412 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 ' 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203624301 1203624302 1203624303 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R. l 1.2 4.2B.R.2.2 4.2B.R.1.2 4.2C.R.1.3 4.2C.R.1.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.l.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.1.3 4.4C.R.1.4 4.4D.R.1.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, Page 87 of 5809 405235038, 405235039, 405235040 and 1203624302 were received and analyzed out of the method specified hold time. 1. Reporting results. Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 4 Analytical Batch: 1597414 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203624304 1203624305 1203624306 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.SA.R.1.3 4.5A.R.1.4 4.5B.R.l.2 4.SB.R.1.3 4.5B.R.1.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.1.4) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Page 88 of 5809 Miscellaneous Information I. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060 and 1203624305 were received and analyzed out of the method specified hold time. I. Reporting r(lsults. Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 4 Analytical Batch: 1597416 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203624308 1203624309 1203624310 Client Sample Identification 4.1.B.R. l.2 4.1.B.R.l.3 4.1.B.R.l.4 4.1.B.R.7.2 4.1.C.R.l.3 4.1.C.R. l .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.l.3 4.1.D.R.l.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Page 89 of 5809 Holding Time Refer to Miscellaneous Information section. Recounts Sample 405235015 (4.2A.R.l .4) was recounted due to the quench number being outside the calibration range. The recount is reported. Miscellaneous Information 1. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, and 1203624309 were received and analyzed out of the method specified hold time. 1. Reporting results. Product: Liquid Scint Tc99, Solid Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Procedure: GL-RAD-A-059 REV# 4 Analytical Batch: 1597417 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203624311 1203624312 1203624313 Client Sample Identification 5.lB.R.2.2 5.2.A.R.l.2 5.2.A.R. l.3 5.2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R. l .4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sample Duplicate (DUP) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Page 90 of 5809 Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, and 1203624312 were received and analyzed out of method specified hold time. l. Reporting results. Product: LSC, Tritium Dist, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 21 Analytical Batch: 1598072 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203626094 1203626095 Page 91 of 5809 Client Sample Identification 4.1.B.R.1.2 4.1.B.R. l .3 4.1.B.R.1.4 4.1.B.R.7.2 4.1.C.R.1.3 4.1.C.R. l.4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R.1.3 4.1.D.R.l.4 4.1.D.R.3.2 4.1.D.R.2.4 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) 1203626096 1203626097 405235001(4.1.B.R.l.2) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information I. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, 1203626095 and 1203626096 were received and analyzed out of the method specified hold time. 1. Reporting results. Product: LSC, Tritium Dist, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 21 Analytical Batch: 1598075 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235021 405235022 405235023 405235024 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 Page 92 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.l l.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.l.4 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 . 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 405235038 405235039 405235040 1203626098 1203626099 1203626100 1203626101 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) 405235021(4.28.R.2.3) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235038, 405235039, 405235040, 1203626099, and 1203626100 were received and analyzed out of the method specified hold time. 1. Reporting results. Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 15 Analytical Batch: 1598078 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596227 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 Page 93 of 5809 Client Sample Identification 4.1.B.R. l .2 4.1.B.R. l.3 4.1.B.R.1.4 4.1.B.R.7.2 4.1.C.R.l.3 4.1.C.R.l .4 4.1.C.R.2.3 4.1.C.R.2.4 4.1.D.R. l .3 4.1.D.R.1.4 4.1.D.R.3.2 4.1.D.R.2.4 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203626105 1203626106 1203626107 1203626108 4.2A.R.2.3 4.2A.R.l.3 4.2A.R.l.4 4.2A.R.2.4 4.2A.R.3.2 4.2A.R.4.2 4.2B.R.2.4 4.2B.R.l.4 Method Blank (MB) 405235001(4.1.B.R.l.2) Sample Duplicate (DUP) 405235001(4.1.B.R.l.2) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information I. Samples405235001,405235002,405235003,405235004,405235005,405235006,405235007,405235008, 405235009,405235010,405235011,405235012,405235013,405235014,405235015,405235016,405235017, 405235018, 405235019, 405235020, 1203626106, and 1203626107 were received and analyzed out of the method specified hold time. 1. Reporting results. Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 15 Analytical Batch: 1598080 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596228 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# ' 405235021 405235022 405235023 405235024 405235025 405235026 405235027 Page 94 of 5809 Client Sample Identification 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.1 l .2 4.2B.R.2.2 4.2B.R.1.2 4.2C.R.l.3 4.2C.R.1.4 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203626126 1203626127 1203626128 1203626129 4.3.ARI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3 .B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.l.4 4.4D.R.l.3 Method Blank (MB) 405235021(4.2B.R.2.3) Sample Duplicate (DUP) 405235021(4.2B.R.2.3) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary:-All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information l.Samples405235021,405235022,405235023,405235024,405235025,405235026,405235027,405235028, 405235029,405235030,405235031,405235032,405235033,405235034,405235035,405235036,405235037, 405235038, 405235039, 405235040, 1203626127, and 1203626128 were received and analyzed outside of the method specified hold time. 1. Reporting results. Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 15 Analytical Batch: 1598081 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 Page 95 of 5809 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203626109 1203626110 1203626111 1203626112 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.1.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.1.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.1.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) Sample Duplicate (DUP) 405235041(4.4D.R.l.4) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235041,405235042,405235043,405235044,405235045,405235046,405235047,405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, 1203626110, and 1203626111 were received and analyzed out of the method specified hold time. 1. Reporting results. Product: Liquid Scint C14, Solid Analytical Method: EPA EERF C-01 Modified Analytical Procedure: GL-RAD-A-003 REV# 15 Analytical Batch: 1598082 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596246 Page 96 of 5809 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 .405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203626113 1203626114 1203626115 1203626116 Client Sample Identification 5.lB.R.2.2 5 .2.A.R.1.2 5.2.A.R.1.3 . 5.2.A.R.1.4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l .4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.1.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.1.3 5.6A.R.1.3 Method Blank (MB) 405235061(5.lB.R.2.2) Sample Duplicate (DUP) 405235061(5.lB.R.2.2) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Miscellaneous Information 1. Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, 1203626114, and 1203626115 were received and analyzed out of method specified hold time. 1. Reporting results. Product: LSC, Tritium Dist, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 21 Analytical Batch: 1598092 Preparation Method: ASTM D 2216 (Modified) Page 97 of 5809 Preparation Procedure: GL-RAD-A-021REV#20 Preparation Batch: 1596233 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203626144 1203626145 1203626146 1203626147 Client Sample Identification 4.4D.R.l.4 4.4D.R.2.3 4.4D.R.2.4 4.4D.R.4.2 4.4D.R.5.2 4.5A.R.l.3 4.5A.R.l.4 4.5B.R.l.2 4.5B.R.l.3 4.5B.R.l.4 4.5B.R.2.3 4.5B.R.2.4 4.5C.R.5.2 4.5C.R.l.3 4.5C.R.l.4 4.5C.R.2.2 4.5C.R.2.3 4.5C.R.2.4 5.lA.R.1.2 5.lA.R.1.3 Method Blank (MB) 405235041(4.4D.R.l.4) Sample Duplicate (DUP) 405235041(4.4D.R.l.4) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 405235059 (5. lA.R.1.2) was recounted due to high MDC. The recount is reported. Miscellaneous Information 1. Samples 405235041, 405235042, 405235043, 405235044, 405235045, 405235046, 405235047, 405235048, 405235049,405235050,405235051,405235052,405235053,405235054,405235055,405235056,405235057, 405235058, 405235059, 405235060, 1203626145, and 1203626146 were received and analyzed out of the method specified hold time. 1. Reporting results. Page 98 of 5809 Product: LSC, Tritium Dist, Solid Analytical Method: EPA 906.0 Modified Analytical Procedure: GL-RAD-A-002 REV# 21 Analytical Batch: 1598096 Preparation Method: ASTM D 2216 (Modified) Preparation Procedure: GL-RAD-A-021 REV# 20 Preparation Batch: 1596246 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203626152 1203626153 1203626154 1203626155 Client Sample Identification 5.IB.R.2.2 5 .2.A.R.1.2 5.2.A.R. l .3 5.2.A.R.l .4 5.2A.R.2.3 5.2.A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2.B.R.l .4 5.2.B.R.3.2 5.2.B.R.4.2 5.2.B.R.2.4 5.2.B.R.8.2 5.3.A.R.l.3 5.4A.R.l.3 5.4A.R.4.2 5.5A.R.l.3 5.6A.R.l.3 Method Blank (MB) 405235061(5.IB.R.2.2) Sample Duplicate (DUP) 405235061(5.IB.R.2.2) Matrix Spike (MS) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on a "dry weight" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Holding Time Refer to Miscellaneous Information section. Recounts Sample 1203626155 (LCS) was recounted due to low recovery. The recount is reported. Miscellaneous Information l.Samples405235061,405235062,405235063,405235064,405235065,405235066,405235067,405235068, Page 99 of 5809 405235069,405235070,405235071,405235072,405235073,405235074,405235075,405235076,405235077, 405235078, 1203626153, and 1203626154 were received and analyzed out of the method specified hold time. I. Reporting results. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 100 of 5809 GEL LABORATORIES LLC 2040 Savage R_oad Charleston SC 29407 -(843) 556-8171 -www.gel.com* Qualifier Definition Report for MJWCOOl MJW Technical Services Client SDG: 405235 GEL Work Order: 405235 The Qualifiers in this report are defined as follows:

A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a Tracer compound H Analytical holding time was exceeded U Analyte was analyzed for, but not detected above the Le. UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier h Preparation or preservation holding time was exceeded ReviewN alidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: t7{ 0 G.1J.AJ (.:1 * /"-{ < ... ( (I tr Date: 04 OCT 2016 Page 101 of 5809 Name: Heather McCarty Title: Analyst II Sample Data Summary Page 102 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: MJW Technical Services Address: 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Report Date: October 4, 2016 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R. l.2 Project: MJWC00115 Sample ID: 405235001 Client ID: MJWCOOl Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.4% Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 19.4 percent LYTI 09/08/16 0806 1596227 I Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0364 +/-0.0647 0.105 0.0312 +/-0.0649 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 Plutonium-239/240 HUh -0.00621 +/-0.0429 0.104 0.031 +/-0.0429 1.00 pCi/g ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0134 +/-0.0454 0.118 0.0371 +/-0.0455 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 Uranium-233/234 Hh 0.798 +/-0.232 0.128 0.0392 +/-0.268 1.00 pCi/g Uranium-235/236 Hh 0.0583 +/-0.0739 0.0918 0.021 +/-0.0745 1.00 pCi/g Uranium-238 Hh 1.00 +/-0.255 0.0792 0.0148 +/-0.306 1.00 pCi/g Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0857 +/-0.259 0.727 0.185 +/-0.259 1.00 pCi/g JXH2 09/30/16 0859 1596392 4 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 2.13 +/-1.25 1.06 0.283 +/-1.33 1.00 pCi/g JXH2 10/01/16 1254 1596388 5 Thorium-229 Hh 0.301 +/-0.488 0.691 0.161 +/-0.492 1.00 pCi/g Thorium-230 Hh 1.46 +/-0.868 0.529 0.0803 +/-0.916 1.00 pCi/g Thorium-232 Hh 0.962 +/-0.721 0.527 0.080 +/-0.746 1.00 pCi/g Am241, Cm Solid "Dry Weight Corrected" Americium-24 I HUh -0.0138 +/-0.0417 0.117 0.0298 +/-0.0418 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 Curium-242 Hh 0.00 +/-0.133 0.199 0.00 +/-0.134 1.00 pCi/g Curium-243/244 HUh 0.0101 +/-0.0563 0.108 0.0247 +/-0.0563 1.00 pCi/g Curium-245/246 Hh 0.00 +/-0.0442 0.0658 0.00 +/-0.0443 1.00 pCi/g Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-24 I HUh -4.14 +/-7.71 13.5 6.57 +/-7.71 15.0 pCi/g JXH2 09/30/16 0539 1596394 7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.016 +/-0.176 0.372 0.138 +/-0.177 1.00 pCi/g MJHl 09/27/16 1226 1598618 8 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0104 +/-0.258 0.498 0.231 +/-0.258 pCi/g MXRI 10/03/16 0756 1596247 9 Antimony-125 HUh -0.0487 +/-0.122 0.219 0.0991 +/-0.124 pCi/g Bismuth-212 HU!h 0.00 +/-0.761 1.46 0.672 +l-0.995 pCi/g Bismuth-214 Hh 1.03 +/-0.229 0.135 0.0601 +/-0.233 pCi/g Cesium-137 Hh 0.562 +/-0.104 0.0892 0.0403 +/-0.107 0.100 pCi/g Cobalt-60 HUh -0.0365 +/-0.0504 0.0729 0.0295 +/-0.0531 pCi/g Europium-I 54 HUh 0.0457 +/-0.126 0.257 0.110 +/-0.128 pCi/g Lead-212 Hh 1.20 +/-0.144 0.107 0.050 +/-0.158 pCi/g Page 103 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R. l.2 Sample ID: 405235001 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Lead-214 Hh 1.22 +/-0.220 Potassium-40 Hh 16.9 +/-1.81 Protactinium-231 HUh 0.0574 +/-0.533 Radium-226 Hh 1.03 +/-0.229 Radium-228 Hh 1.04 +/-0.294 Thallium-208 Hh 0.422 +/-0.0952 Tin-126 HUih 0.00 +/-0.103 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.1 +/-3.68 Beta Hh 19.7 +/-2.86 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.296 +/-0.340 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.0866 +/-1.90 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.321 +/-0.636 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.43 +/-1.28 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.146 0.592 1.02 0.135 0.256 0.0725 0.202 3.94 3.33 0.779 3.30 1.11 2.37 2 3 4 5 6 7 8 9 10 11 12 13 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified Page 104 of 5809 0.0669 +/-0.226 pCi/g 0.232 +/-2.02 pCi/g 0.474 +/-0.534 pCi/g 0.0601 +/-0.233 pCi/g 0.110 +/-0.299 pCi/g 0.0324 +/-0.0969 pCi/g 0.0966 +/-0.122 pCi/g 1.69 +/-4.50 4.00 pCi/g JXC9 09/16/16 1057 1597816 10 1.58 +/-4.11 10.0 pCi/g 0.334 +/-0.340 2.00 pCi/g KSDI 09117/16 1550 1597795 II 1.59 +/-1.90 6.00 pCi/g AEA 09/19/16 1326 1598072 12 0.542 +/-0.636 2.00 pCi/g AEA 09/22/16 003 8 1598078 13 1.13 +/-1.28 5.00 pCi/g GXRl 09/20/16 0440 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.l.2 Sample ID: 405235001 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. 14 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer Recovery Test Plutonium-242 Tracer ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Uranium-232 Tracer ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-235/236 Tracer ASP Uranium Isotopic, Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np237, Solid "Dry Weight Corrected" Actinium-227 Tracer Alphaspec Th229 + 228,230,232 Solid "Dry Weight Americium-243 Tracer Am241, Cm Solid "Dry Weight Corrected" Plutonium-242 Tracer Liquid Scint Pu24 l, Solid "Dry Weight Corrected" Strontium Carrier GFPC, Sr90, solid "Dry Weight Corrected" Technetium-99m Tracer Liquid Scint Tc99, Solid "Dry Weight Corrected" Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidenq: level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 105 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 78.4 (15%-125%) 1596389 85.7 (15%-125%) 1596389 104 (15%-125%) 1596392 61.2 (15%-125%) 1596388 92.3 (15%-125%) 1596390 79.7 (15%-125%) 1596394 78.4 (15%-125%) 1597795 100 (25%-125%) 1597416 91.8 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.l.3 Sample ID: 405235002 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 22.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 22.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0194 +/-0.0533 0.0924 Plutonium-239/240 HUh -0.00661 +/-0.0457 0.111 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 Hh 0.0524 +/-0.0754 0.091 Uranium-233/234 Hh 1.13 +/-0.257 0.097 Uranium-235/236 Hh 0.0337 +/-0.0595 0.0902 Uranium-238 Hh 1.17 +/-0.262 0.103 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0214 +/-0.184 0.427 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.89 +/-0.555 0.432 Thorium-229 Hh 0.178 +/-0.170 0.218 Thorium-230 Hh 0.969 +/-0.334 0.218 Thorium-232 Hh 1.23 +/-0.363 0.0817 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.00606 +/-0.0634 0.132 Curium-242 Hh 0.00 +/-0.151 0.224 Curium-243/244 HUh 0,0114 +/-0.0635 0.122 Curium-245/246 HUh 0.0188 +/-0.0706 0.119 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -9.2 +/-7.64 13.7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.109 +/-0.278 0.598 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0188 +/-0.238 0.428 Antimony-125 HUh 0.0438 +/-0.115 0.212 Bismuth-212 HUih 0.00 +/-0.812 1.33 Bismuth-214 Hh 0.915 +/-0.178 0.0819 Cesium-137 HUih 0.00 +/-0.0883 0.0595 Cobalt-60 HUh -0.0144 +/-0.0498 0.0911 Europium-154 HUh 0.0466 +/-0.120 0.256 Lead-212 Hh 1.45 +/-0.143 0.0964 Lead-214 Hh 1.12 +/-0.207 0.116 Page 106 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0235 +/-0.0534 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.033 +/-0.0457 1.00 pCi/g 0.017 +/-0.076 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0264 +/-0.320 1.00 pCi/g 0.0229 +/-0.0598 1.00 pCi/g 0.0295 +/-0.328 1.00 pCi/g 0.0799 +/-0.185 1.00 pCi/g JXH2 09/30/16 0859 1596392 4 0.161 +/-0.598 1.00 pCi/g JXH2 09/28/16 1405 1596388 5 0.068 +/-0.171 1.00 pCi/g 0.0678 +/-0.353 1.00 pCi/g 0.00 +/-0.390 1.00 pCi/g 0.0337 +/-0.0635 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.151 1.00 pCi/g 0.0279 +/-0.0636 1.00 pCi/g 0.0222 +/-0.0707 1.00 pCi/g 6.65 +/-7.64 15.0 pCi/g JXH2 09/30/16 0641 1596394 7 0.252 +/-0.283 1.00 pCi/g MJHl 09/27/16 1227 1598618 8 0.197 +/-0.238 pCi/g MXRl 10/03/16 0757 1596247 9 0.0961 +/-0.117 pCi/g 0.613 +/-1.30 pCi/g 0.0342 +/-0.192 pCi/g 0.0259 +/-0.0888 0.100 pCi/g 0.0391 +/-0.0502 pCi/g 0.111 +/-0.122 pCi/g 0.0446 +/-0.186 pCi/g 0.052 +/-0.227 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.l.3 Sample ID: 405235002 Parameter Qualifier Result Uncertainty Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 17.8 +/-1.78 Protactinium-231 HUih 0.00 +/-0.777 Radium-226 Hh 0.915 +/-0.178 Radium-228 Hh 1.30 +/-0.343 Thallium-208 Hh 0.249 +/-0.0673 Tin-126 HUih 0.00 +/-0.126 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 32.3 +/-7.65 Beta Hh 20.I +/-3.65 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.462 +/-0.472 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.12 +/-1.97 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.024 +/-0.636 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.822 +/-1.21 The following Prep Methods were performed Method Description Diy Soil Prep Diy Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-OI-R MDC 0.667 0.803 0.0819 0.207 0.0645 0.118 3.92 2.74 0.991 3.36 I.IO 2.19 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 107 of 5809 Report Date: Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst 0.275 +/-2.39 pCi/g 0.367 +/-0.793 pCi/g 0.0342 +/-0.192 pCi/g 0.0872 +/-0.388 pCi/g 0.0288 +/-0.0703 pCi/g 0.0553 +/-0.128 pCi/g 1.28 +/-9.68 4.00 pCi/g JXC9 1.17 +/-4.63 10.0 pCi/g 0.445 +/-0.472 2.00 pCi/g KSDI 1.62 +/-1.97 6.00 pCi/g AEA 0.534 +/-0.636 2.00 pCi/g AEA 1.05 +/-1.21 5.00 pCi/g GXRI Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 October 4, 2016 Date Time Batch Mtd. 09/16/16 1057 1597816 10 09/19/16 1155 1597795 II 09/19/16 1459 1598072 12 09/22/16 0125 1598078 13 09/20/16 0456 1597416 14 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R. l.3 Sample ID: 405235002 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 108 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 76.4 (15%-125%) 1596389 79.2 (15%-125%) 1596389 78.9 (15%-125%) 1596392 76 (15%-125%) 1596388 90.7 (15%-125%) 1596390 66.5 (15%-125%) 1596394 76.4 (15%-125%) 1597795 103 (25%-125%) 1597416 91.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.l.4 SamI?le ID: 405235003 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 17.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh 0.000753 +/-0.0558 0.124 Plutonium-239/240 HUh 0.000748 +l-0.0555 0.123 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00505 +/-0.0759 0.177 Uranium-233/234 Hh 1.03 +/-0.255 0.0978 Uranium-235/236 Hh 0.0488 +/-0.0724 0.106 Uranium-238 Hh 0.845 +/-0.231 0.0768 Alphaspec Np237, Solid Dry Weight Corrected" Neptunium-237 Hh 0.00 +/-0.354 0.526 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.51 +/-0.530 0.441 Thorium-229 Hh 0.0762 +/-0.148 0.244 Thorium-230 Hh 0.733 +/-0.344 0.369 Thorium-232 Hh 1.25 +/-0.396 0.215 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0141 +/-0.0625 0.163 Curium-242 Hh 0.00 +/-0.205 0.305 Curium-243/244 HUh -0.0143 +/-0.0634 0.165 Curium-245/246 Hh 0.0673 +/-0.115 0.101 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 0.249 +/-6.97 11.9 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.238 +/-0.233 0.714 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0619 +/-0.261 0.517 Antimony-125 HUh -0.0547 +/-0.118 0.212 Bismuth-212 Hh 1.18 +/-1.20 I.OJ Bismuth-214 Hh 0.730 +/-0.212 0.173 Cesium-137 HUh 0.00714 +/-0.0487 0.0919 Cobalt-60 HUh 0.00486 +/-0.0565 0.111 Europium-154 HUh -0.0771 +/-0.149 0.261 Lead-i12 Hh 1.22 +/-0.151 0.110 Lead-214 Hh 1.01 +/-0.246 0.160 Page 109 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.0338 +l-0.0559 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.0336 +/-0.0555 1.00 pCi/g 0.0507 +/-0.076 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0249 +/-0.315 1.00 pCi/g 0.0288 +/-0.0729 1.00 pCi/g 0.0144 +/-0.276 1.00 pCi/g 0.00 +/-0.354 1.00 pCi/g JXH2 09/30/16 0859 1596392 4 0.159 +/-0.561 1.00 pCi/g JXH2 09/28/16 1405 1596388 5 0.0762 +/-0.148 1.00 pCi/g 0.139 +/-0.354 1.00 pCi/g 0.0619 +/-0.423 1.00 pCi/g 0.0373 +/-0.0627 . 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.205 1.00 pCi/g 0.0379 +/-0.0636 1.00 pCi/g 0.00 +/-0.116 1.00 pCi/g 5.85 +/-6.97 15.0 pCi/g JXH2 10/01/16 1708 1596394 7 0.277 +/-0.258 1.00 pCi/g MJHI 09/27/16 1227 1598618 8 0.239 +/-0.263 pCi/g MXRI 10/03/16 0801 1596247 9 0.0943 +/-0.121 pCi/g 0.440 +/-1.20 pCi/g 0.0783 +/-0.214 pCi/g 0.0411 +/-0.0488 0.100 pCi/g 0.0479 +l-0.0565 pCi/g 0.110 +/-0.153 pCi/g 0.0508 +1-0:164 pCi/g 0.0733 +/-0.249 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.l.4 Sample ID: 405235003 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.5 +/-1.70 Protactinium-231 HUih 0.00 +l-0.595 Radium-226 Hh 0.730 +/-0.212 Radium-228 Hh 0.987 +/-0.335 Thallium-208 Hh 0.394 +/-0.103 Tin-126 HUih 0.00 +/-0.196 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 12.3 +/-3.18 Beta Hh 21.7 +/-2.16 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.424 +/-0.636 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.534 +/-1.89 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.31 +/-0.650 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.375 +/-1.05 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-0.5-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 0.817 1.26 0.173 0.311 0.0656 0.190 3.97 2.24 1.30 3.32 1.14 1.87 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 110of5809 0.338 +/-1.86 pCi/g 0.590 +/-0.740 pCi/g 0.0783 +/-0.214 pCi/g 0.135 +/-0.339 pCi/g 0.0285 +/-0.104 pCi/g 0.0902 +/-0.196 pCi/g 1.81 +/-3.98 4.00 pCi/g JXC9 09/16/16 1058 1597816 10 1.07 +/-3.89 10.0 pCi/g 0.581 +/-0.636 2.00 pCi/g KSDI 09/17/16 1551 1597795 11 1.60 +/-1.89 6.00 pCi/g AEA 09/19/16 1632 1598072 12 0.554 +/-0.650 2.00 pCi/g AEA 09/22/16 0211 1598078 13 0.897 +/-1.05 5.00 pCi/g GXRl 09/20/16 0512 1597416 14 Analyst Date Time Prep Batch LYTl 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.1.4 Sample ID: 405235003 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result U!Icertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 111 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 59.5 (15%-125%) 1596389 75.5 (15%-125%) 1596389 55.8 (15%-125%) 1596392 36.7 (15%-125%) 1596388 84.8 (15%-125%) 1596390 50.7 (15%-125%) 1596394 59.5 (15%-125%) 1597795 102 (25%-125%) 1597416 91.4 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.l.B.R.7.2 Sample ID: 405235004 Matrix: Soil Collect Date: 09-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 19.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh -0.0229 +/-0.0783 0.194 Plutonium-239/240 HUh 0.0106 +/-0.0588 0.113 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00835 +/-0.0577 0.140 Uranium-233/234 Hh 0.855 +/-0.261 0.150 Uranium-235/236 Hh 0.0728 +/-0.0858 0.0928 Uranium-238 Hh 1.11 +/-0.291 0.107 Alphaspec Np237, Solid Dry Weight Corrected" Neptunium-23 7 HUh 0.181 +/-0.537 0.951 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.43 +/-0.656 0.667 Thorium-229 Hh 0.203 +/-0.225 0.265 Thorium-230 Hh 1.15 +/-0.462 0.264 Thorium-232 Hh 0.784 +/-0.388 0.263 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.028 +/-0.0635 0.109 Curium-242 Hh 0.00 +/-0.109 0.162 . Curium-243/244 HUh -0.00757 +/-0.0335 0.0874 Curium-245/246 HUh 0.0135 +l-0.0506 0.0852 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-24 I HUh -5.99 +/-7.28 12.7 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0259 +/-0.221 0.512 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0833 +/-0.234 0.418 Antimony-125 HUh -0.0294 +/-0.0997 0.193 Bismuth-212 HUlh 0.00 +/-1.06 1.39 Bismuth-214 Hh 0.880 +/-0.205 0.109 Cesium-137 Hh 0.209 +/-0.0662 0.0653 Cobalt-60 HUh -0.0229 +/-0.027 0.0451 Europium-I 54 HUh 0.0654 +/-0.0936 0.219 Lead-212 Hh 1.17 +/-0.132 0.0916 Lead-214 Hh 1.16 +/-0.217 0.351 Page 112 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0806 1596227 I 0.0662 +/-0.0783 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.0258 +/-0.0588 1.00 pCi/g 0.0417 +/-0.0578 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0458 +/-0.304 1.00 pCi/g 0.0174 +/-0.0868 1.00 pCi/g 0.0245 +/-0.355 1.00 pCi/g 0.301 +/-0.538 1.00 pCi/g JXH2 10/01/16 1254 1596392 4 0.243 +/-0.684 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0646 +/-0.227 1.00 pCi/g 0.0645 +/-0.486 1.00 pCi/g 0.0643 +/-0.402 1.00 pCi/g 0.0312 +/-0.0636 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.109 1.00 pCi/g 0.020 +/-0.0336 1.00 pCi/g 0.0159 +/-0.0507 1.00 pCi/g 6.22 +/-7.28 15.0 pCi/g JXH2 10/01/16 1909 1596394 7 0.181 +/-0.221 1.00 pCi/g MJHl 09/27/16 1227 1598618 8 0.193 +/-0.237 pCi/g MXRl 10/03/16 0801 1596247 9 0.0871 +/-0.101 pCi/g 0.641 +/-1.42 pCi/g 0.0477 +/-0.208 pCi/g 0.0288 +/-0.0668 0.100 pCi/g 0.0164 +/-0.0289 pCi/g 0.093 +/-0.0982 pCi/g 0.0424 +/-0.145 pCi/g 0.170 +/-0.222 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.7.2 Sample ID: 405235004 Certificate of Analysis Repprt Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.0 +/-1.60 Protactinium-23 I HUih 0.00 +/-0.649 Radium-226 Hh 0.880 +/-0.205 Radium-228 Hh 1.06 +/-0.255 ThaIIium-208 Hh 0.388 +/-0.084 Tin-126 HUih 0.00 +/-0.168 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 20.6 +/-3.58 Beta Hh 25.9 +/-2.14 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.282 +/-0.639 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 1.73 +/-1.94 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.251 +/-0.701 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.25 +/-1.25 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.576 0.723 0.109 0.239 0.0599 0.127 3.98 2.00 1.14 3.27 1.20 2.31 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Mpdified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 113of5809 0.232 +/-1.76 pCi/g 0.329 +/-0.663 pCi/g 0.0477 +/-0.208 pCi/g 0.103 +/-0.261 pCi/g 0.0265 +/-0.0856 pCi/g 0.0594 +/-0.169 pCi/g 1.84 +/-5.41 4.00 pCi/g JXC9 09/16/16 1058 1597816 10 0.954 +/-4.34 10.0 pCi/g 0.502 +/-0.641 2.00 pCi/g KSDI 09/17/16 1551 1597795 II 1.58 +/-1.94 6.00 pCi/g AEA 09/19/16 1805 1598072 12 0.582 +/-0.702 2.00 pCi/g AEA 09/22/16 0410 1598078 13 1.10 +/-1.25 5.00 pCi/g GXRI 09/20/16 0528 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.B.R.7.2 Sample ID: 405235004 Certificate of Analysis Report Date: Project: MJWCOOl15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 114of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 56.3 (15%-125%) 1596389 63.4 (15%-125%) 1596389 76.2 (15%-125%) 1596392 J9.5 (15%-125%) 1596388 73.8 (15%-125%) 1596390 95.4 (15%-125%) 1596394 56.3 (15%-125%) 1597795 92.3 (25%-125%) 1597416 92.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.l.C.R.1.3 Sample ID: 405235005 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 20.4% Parameter Qualifier , Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 20.4 Rad Alpha Spec Analysis ASP Plutonium'/sotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0468 +/-0.0651 0.0972 Plutonium-239/240 HUh 0.00679 +/-0.0377 0.0723 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0134 +/-0.0452 0.117 Uranium-233/234 Hh 0.922 +/-0.227 0.0983 Uranium-235/236 Hh 0.0495 +/-0.0627 0.0779 Uranium-238 Hh 0.754 +/-0.204 0.0672 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.143 +/-0.201 0.658 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.44 +!-0.609 0.352 Thorium-229 Hh 0.162 +/-0.213 0.272 Thorium-230 Hh 1.20 +/-0.511 0.464 Thorium-232 Hh 0.853 +/-0.424 0.368 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0225 +/-0.0594 0.107 Curium-242 Hh 0.00 +/-0.100 0.150 Curium-243/244 Hh 0.00 +/-0.0296 0.044 Curium-245/246 HXh 0.0495 +/-0.0652 0.0495 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -3.76 +/-6.42 11.3 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.129 +/-0.275 0.734 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 H0h -0.000521 +/-0.227 0.439 Antimony-125 HUh -0.0172 +/-0.104 0.194 Bismuth-212 HD!h 0.00 +/-1.04 1.31 Bismuth-214 Hh 0.907 +/-0.175 0.120 Cesium-137 Hh 0.155 +/-0.0586 0.0573 Cobalt-60 HUh 0.00143 +/-0.0329 0.0673 HUh 0.0099 +/-0.109 0.217 Lead-212 Hh 0.950 +/-0.129 0.0948 Lead-214 Hh 1.03 +/-0.201 0.135 Page 115of5809 Report Date: October4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units

PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.0289 +/-0.0654 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.0166 +/-0.0377 1.00 pCi/g 0.0369 +/-0.0452 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0281 +/-0.272 1.00 pCi/g 0.0178 +/-0.0632 1.00 pCi/g 0.0126 +/-0.238 1.00 pCi/g 0.202 +/-0.201 1.00 pCi/g JXH2 09/30/16 0859 1596392 4 0.0835 +/-0.641 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0665 +/-0.215 1.00 pCi/g 0.163 +/-0.537 1.00 pCi/g 0.115 +/-0.440 1.00 pCi/g 0.0318 +/-0.0595 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.101 1.00 pCi/g 0.00 +/-0.0296 1.00 pCi/g 0.00 +/-0.0655 1.00 pCi/g 5.48 +/-6.42 15.0 pCi/g JXH2 09/30/16 0944 1596394 7 0.275 +/-0.281 1.00 pCi/g MJHI 09/27/16 151 I 1598618 8 0.204 +/-0.227 pCi/g MXRI 10/03/16 0802 1596247 9 0.0881 +/-0.104 pCi/g 0.604 +/-1.22 pCi/g 0.0537 +/-0.180 pCi/g 0.025 +/-0.059 0.100 pCi/g 0.0278 +/-0.0329 pCi/g 0.0931 +/-0.109 pCi/g 0.0443 +/-0.138 pCi/g 0.0624 +/-0.205 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms, Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.l.3 Sample ID: 405235005 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.6 +/-1.48 0.672 Protactinium-231 HUih *0.00 +/-0.784 0.824 Radium-226 Hh 0.907 +/-0.175 0.120 Radium-228 Hh 1.08 +/-0.322 0.258 Thallium-208 Hh 0.321 +/-0.081 0.0577 Tin-126 HUih 0.00 +/-0.169 0.135 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid Dry Weight Corrected" Alpha Hh 13.5 +/-3.31 3.93 Beta Hh 18.4 +/-2.38 2.93 GFPC, Sr90, solid Dry Weight Corrected" Strontium-9Q HUh -0.135 +/-0.565 1.10 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.04 +/-1.85 3.14 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.188 +/-0.608 1.06 Liquid Scint Tc99, Solid Dry Weight Corrected" Technetium-99 HUh -0.599 +/-1.32 2.36 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 .6 7 8 9 10 II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 116of5809 0.284 +/-1.67 pCi/g 0.381 +/-0.806 pCi/g 0.0537 +/-0.180 pCi/g 0.114 +/-0.327 pCi/g 0.0256 +/-0.0821 pCi/g 0.0643 +/-0.170 pCi/g 1.78 +/-4.24 4.00 pCi/g JXC9 09/16/16 1058 1597816 10 1.40 +/-3.62 10.0 pCi/g 0.489 +/-0.565 2.00 pCi/g KSDI 09/17/16 1551 1597795 11 1.52 +/-1.85 6.00 pCi/g AEA 09/19/16 1938 1598072 12 0.515 +/-0.608 2.00 pCi/g AEA 09/22/16 0456 1598078 13 1.13 +/-1.32 5.00 pCi/g GXRl 09/20/16 0544 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.l.3 Sample ID: 405235005 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 117 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 93.2 (15%-125%) 1596389 78.4 (15%-125%) 1596389 100 (15%-125%) 1596392 83.9 (15%-125%) 1596388 75.5 (15%-125%) 1596390 102 (15%-125%) 1596394 93.2 (15%-125%) 1597795 89.6 (25%-125%) 1597416 87.1 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.l.4 Sample ID: 405235006 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 19.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 19.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0283 +/-0.0449 0.0621 Plutonium-239/240 HUh 0.00847 +/-0.0318 0.0535 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0147 +/-0.0501 0.0929 Uranium-233/234 Hh 0.762 +/-0.223 0.128 Uranium-235/236 Hh 0.0718 +/-0.0774 0.088 Uranium-238 Hh 0.923 +/-0.241 0.0968 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00979 +/-0.450 0.989 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.90 +l-0.599 0.333 Thorium-229 HUh 0.0681 +/-0.169 0.300 Thorium-230 Hh 0.909 +/-0.368 0.273 Thorium-232 Hh 0.941 +/-0.364 0.201 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.00585 +/-0.0612 0.128 Curium-242 Hh 0.00 +/-0.145 0.216 Curium-243/244 Hh 0.00 +/-0.0428 0.0636 Curium-245/246 Hh 0.00 +/-0.0482 0.0717 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.24 +/-4.20 7.24 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" lodine-129 HUh 0.433 +/-0.424 1.30 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0195 +/-0.198 0.393 Antimony-125 HUh 0.0559 +/-0.082 0.173 Bismuth-212 Hh 1.06 +/-0.592 0.698 Bismuth-214 Hh 0.770 +/-0.168 0.114 Cesium-137 HUh 0.0344 +/-0.0386 0.0791 Cobalt-60 HU!h 0.00 +/-0.0282 0.0722 Europium-154 HUh -0.0518 +/-0.0803 0.144 Lead-212 Hh I.I I +/-0.140 0.085 Lead-214 Hh 1.08 +/-0.170 0.108 Page 118 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.0142 +/-0.0451 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.010 +/-0.0318 1.00 pCi/g 0.0253 +/-0.0502 1.00 pCi/g JXH2 09129116 0913 1596389 3 0.0402 +/-0.257 1.00 pCi/g 0.0202 +/-0.0783 1.00 pCi/g 0.0246 +/-0.286 1.00 pCi/g 0.311 +/-0.450 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.0979 +/-0.644 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0986 +/-0.169 1.00 pCi/g 0.0852 +/-0.384 1.00 pCi/g 0.0491 +/-0.381 1.00 pCi/g 0.0325 +/-0.0613 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.146 1.00 pCi/g 0.00 +/-0.0429 1.00 pCi/g 0.00 +/-0.0483 1.00 pCi/g 3.55 +/-4.20 15.0 pCi/g JXH2 10/01/16 2110 1596394 7 0.503 +/-0.469 1.00 pCi/g MJHI 09/27/16 1511 1598618 8 0.183 +/-0.199 pCi/g MXRI 10/03/16 0802 °1596247 9 0.0784 +/-0.0858 pCi/g 0.305 +l-0.594 pCi/g 0.0516 +/-0.171 pCi/g 0.0363 +/-0.0417 0.100 pCi/g 0.031 +/-0.0335 pCi/g 0.0582 +/-0.0837 pCi/g 0.0397 +/-0.152 pCi/g 0.0495 +/-0.176 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.l.4 Sample ID: 405235006 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 16.0 +/-1.44 Protactinium-231 HUlh 0.00 ' +/-0.730 Radium-226 Hh 0.770 +/-0.168 Radium-228 Hh 1.41 +/-0.299 Thallium-208 Hh 0.366 +/-0.0864 Tin-126 HUlh 0.00 +/-0.118 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 12.0 +/-4.38 Beta Hh 21.2 +/-3.32 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.107 +/-0.733 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.621 +/-1.94 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.0922 +/-0.709 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.909 +/-1.05 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300,_Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.371 0.611 0.114 0.158 0.0537 0.114 3.90 2.68 1.33 3.34 1.22 1.92 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 9Q6.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 119 of 5809 0.138 +/-1.66 pCi/g 0.278 +/-0.771 pCi/g 0.0516 +/-0.171 pCi/g 0.0655 +/-0.307 pCi/g 0.024 +/-0.0878 pCi/g 0.0541 +/-0.119 pCi/g 1.42 +/-4.98 4.00 pCi/g JXC9 09/16/16 1058 1597816 10 1.18 +/-4.61 10.0 pCi/g 0.606 +/-0.734 2.00 pCi/g KSDI 09/17/16 1551 1597795 11 1.61 +/-1.94 6.00 pCi/g AEA 09/19/16 2111 1598072 12 0.593 +/-0.709 2.00 pCi/g AEA 09/22/16 0542 1598078 13 0.918 +/-1.05 5.00 pCi/g GXRI 09/20/16 0601 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.l.C.R.1.4 Sample ID: 405235006 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 120 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 97.3 (15%-125%) 1596389 72.5 (15%-125%) 1596389 101 (15%-125%) 1596392 57.3 (15%-125%) 1596388 95.6 (15%-125%) 1596390 67.9 (15%-125%) 1596394 97.3 (15%-125%) 1597795 89.6 (25%-125%) 1597416 94.3 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.2.3 Sample ID: 405235007 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 21.2% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 21.2 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.000504 +/-0.0373 0.083 Plutonium-239/240 HUh 0.0005 +/-0.0371 0.0824 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0199 +/-0.0549 0.0952 Uranium-233/234 Hh 0.729 +/-0.191 0.0828 Uranium-235/236 Hh 0.0852 +/-0.0703 0.0604 Uranium-238 Hh 0.929 +/-0.213 0.0377 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.230 +/-0.371 0.575 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.19 +/-0.546 0.621 Thorium-229 HUh 0.0163 +/-0.132 0.268 Thorium-230 Hh 0.790 +/-0.333 0.197 Thorium-232 Hh 0.569 +/-0.292 0.236 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0419 +/-0.0679 0.105 Curium-242 HUh -0.0124 +/-0.107 0.248 Curium-243/244 Hh 0.00 +/-0.0306 0.0456 Curium-245/246 Hh 0.0342 +/-0.0587 0.0514 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -8.65 +/-7.14 12.8 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.276 +l-0.459 0.604 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-2i7 HUh -0.0788 +/-0.249 0.471 Antimony-125 HUh -0.0108 +/-0.0993 0.190 Bismuth-212 HUih 0.00 +/-0.945 1.37 Bismuth-214 Hh 0.846 +/-0.188 0.125 Cesium-137 Hh 0.267 +/-0.104 0.0762 Cobalt-60 HUih 0.00 +/-0.0439 0.084 Europium-154 HUh -0.00743 +/-0.0993 0.201 Lead-212 Hh 1.05 +/-0.135 0.103 Lead-214 Hh 1.12 +/-0.199 0.128 Page 121 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU

RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.0226 +/-0.0374 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.0225 +/-0.0371 1.00 pCi/g 0.0242 +!-0.055 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0225 +/-0.223 1.00 pCi/g 0.0113 +/-0.0716 1.00 pCi/g 0.00 +/-0.259 1.00 pCi/g 0.164 +/-0.372 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.243 +/-0.566 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0837 +/-0.132 1.00 pCi/g 0.0482 +/-0.346 1.00 pCi/g 0.068 +/-0.300 1.00 pCi/g 0.0301 +/-0.0681 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.0464 +/-0.107 1.00 pCi/g 0.00 +/-0.0307 1.00 pCi/g 0.00 +/-0.0589 1.00 pCi/g 6.21 +/-7.14 15.0 pCi/g JXH2 09/30/16 1146 1596394 7 0.155 +/-0.476 1.00 pCi/g MJHI 09/27/16 1512 1598618 8 0.219 +t-0.251 pCi/g MXRI 10/03/16 0802 1596247 9 0.0856 +/-0.0995 pCi/g 0.635 +/-1.14 pCi/g 0.056 +/-0.191 pCi/g 0.0342 +/-0.105 0.100 pCi/g 0.0358 +/-0.0535 pCi/g 0.0839 +/-0.0994 pCi/g 0.0479 +/-0.146 pCi/g 0.0585 +/-0.204 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.2.3 Sample ID: 405235007 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.5 +/-1.59 Protactinium-231 HUih 0.00 +/-0.687 Radium-226 Hh 0.846 +/-0.188 Radium-228 Hh 1.23 +/-0.276 Thallium-208 Hh 0.368 +/-0.0928 Tin-126 HUh 0.024 +/-0.144 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 13.6 +/-3.46 Beta Hh 15.9 +/-2.37 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 Hh 0.276 +/-0.239 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Dry Weight Corrected" Tritium HUh -0.257 +/-2.05 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.207 +/-0.709 Liquid Scint Tc99, Solid Dry Weight Corrected" Technetium-99 HUh -0.418 +/-1.28 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.542 0.874 0.125 0.263 0.0546 0.167 3.85 2.81 0.383 3.58 1.23 2.27 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 122 of 5809 0.215 +/-1.78 pCi/g 0.405 +/-0.700 pCi/g 0.056 +/-0.191 pCi/g 0.116 +/-0.283 pCi/g 0.0238 +/-0.0941 pCi/g 0.0793 +/-0.145 pCi/g 1.70 +/-4.38 4.00 pCi/g JXC9 09/19/16 1241 1597816 10 1.34 +/-3.42. 10.0 pCi/g 0.165 +/-0.244 2.00 pCi/g KSDl 09/17/16 1551 1597795 11 1.73 +/-2.05 6.00 pCi/g AEA 09/19/16 2244 1598072 12 0.600 +/-0.709 2.00 pCi/g AEA 09/22/16 0629 1598078 13 1.09 +/-1.28 5.00 pCi/g GXRl 09/20/16 0617 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.2.3 Sample ID: 405235007 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 123 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 1596389 1596389 1596392 1596388 1596390 1596394 1597795 1597416 82.9 91.4 94.4 85.6 103 96.4 82.9 96.4 87.l (15%-125%) (15%-125%)

(15%-125%) (15%-125%) (15%-125%) (15%-125%) (15%-125%) (25%-125%) (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.2.4 Sample ID: 405235008 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 20.7% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 20.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Corrected" Plutonium-238 Hh 0.0454 +/-0.0575 0.0714 Plutonium-239/240 HUh 0.00666 +/-0.037 0.0709 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0134 +/-0.0311 0.0921 Uranium-233/234 Hh 1.03 +/-0.227 0.105 Uranium-235/236 Hh 0.0256 +/-0.051 0.0828 Uranium-238 Hh 0.808 +/-0.200 0.0694 Alphaspec Np23_7, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0552 +/-0.307 0.588 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.73 +/-0.606 0.313 Thorium-229 HUh 0.0778 +/-0.167 0.276 Thorium-230 Hh 1.07 +/-0.415 0.229 Thorium-232 Hh 0.895 +/-0.376 0.117 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.000756 +/-0.0561 0.125 Curium-242 Hh 0.00 +/-0.132 0.196 Curium-243/244 HUh 0.000767 +/-0.0569 0.126 Curium-245/246 Hh 0.00 +/-0.0436 0.0648 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -8.21 +/-6.61 11.8 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.121 +/-0.196 0.362 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0183 +/-0.247 0.478 Antimony-125 HUh -0.053 +/-0.124 0.226 Bismuth-212 HUh -0.0409 +/-0.638 1.19 Bismuth-214 Hh 0.810 +/-0.211 0.162 Cesium-137 Hh 0.189 +/-0.0961 0.0837 Cobalt-60 HUh -0.00334 +/-0.0418 0.0848 Europium-154 HUh 0.00693 +/-0.141 0.283 Lead-212 Hh 1.24 +/-0.156 0.111 Lead-214 Hh 1.10 +/-0.226 0.371 Page 124 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0164 +/-0.0577 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.0163 +/-0.037 1.00 pCi/g 0.0251 +/-0.0312 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0337 +/-0.278 1.00 pCi/g 0.0226 +/-0.0512 1.00 pCi/g 0.0159 +/-0.237 1.00 pCi/g 0.135 +/-0.307 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.0785 +/-0.646 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0793 +/-0.168 1.00 pCi/g 0.056 +/-0.437 1.00 pCi/g 0.00 +/-0.392 1.00 pCi/g 0.0339 +/-0.0561 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.132 1.00 pCi/g 0.0344 +/-0.057 1.00 pCi/g 0.00 +/-0.0437 1.00 pCi/g 5.76 +/-6.61 15.0 pCi/g JXH2 09/30/16 1247 1596394 7 0.150 +/-0.204 1.00 pCi/g MJHl 09/27/16 1619 1598618 8 0.220 +/-0.247 pCi/g MXRl 10/0J/16 0803 1596247 9 0.102 +/-0.127 pCi/g 0.530 +/-0.638 pCi/g 0.0729 +/-0.214 pCi/g 0.0371 +/-0.0965 0.100 pCi/g 0.0345 +/-0.0418 pCi/g 0.121 +/-0.141 pCi/g 0.0517 +/-0.169 pCi/g 0.179 +/-0.230 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.2.4 Sample ID: 405235008 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.5 +/-1.78 Protactinium-231 HUh 0.269 +/-0.536 Radium-226 Hh 0.810 +/-0.211 Radium-228 Hh 0.805 +/-0.386 Thallium-208 Hh 0.233 +/-0.108 Tin-126 HUh 0.0514 +/-0.117 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 14.6 +/-3.33 Beta Hh 23.5 +/-2.51 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.321 +/-0.473 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.42 +/-2.08 Liquid Scint C/4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.083 +/-0.738 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.332 +/-1.24 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML. HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-OI Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.811 1.07 0.162 0.319 0.0849 0.131 2.99 2.36 0.824 3.53 1.27 2.20 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 125 of 5809 0.334 +/-1.93 pCi/g 0.498 +/-0.552 pCi/g 0.0729 +/-0.214 pCi/g 0.140 +/-0.388 pCi/g 0.0382 +/-0.109 pCi/g 0.0625 +/-0.118 pCi/g 1.26 +/-4.36 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.10 +/-4.14 10.0 pCi/g 0.345 +/-0.477 2.00 pCi/g KSDI 09/17/16 1551 1597795 II 1.70 +/-2.08 6.00 pCi/g AEA 09/20/16 0017 1598072 12 0.617 +/-0.738 2.00 pCi/g AEA 09/22/16 0715 1598078 13 1.05 +/-1.24 5.00 pCi/g GXRl 09/20/16 0633 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.C.R.2.4 Sample ID: 405235008 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 126 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 90.1 (15%-125%) 1596389 89.1 (15%-125%) 1596389 105 (15%-125%) 1596392 65.3 (15%-125%) 1596388 86.4 (15%-125%) 1596390 78.4 (15%-125%) 1596394 90.1 (15%-125%) 1597795 103 (25%-125%) 1597416 90.8 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R. l.3 Sample ID: 405235009 Matrix: Soil Collect Date: 10-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 23.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 23.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00709 +/-0.0458 0.0936 Plutonium-239/240 Hh 0.0191 +l-0.0439 0.0696 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0068 +/-0.047 0.114 Uranium-233/234 Hh 1.23 +/-0.301 0.152 Uranium-235/236 HUh 0.0328 +/-0.0744 0.128 Uranium-238 Hh 0.818 +/-0.245 0.120 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.244 +/-0.540 0.948 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.970 +/-0.460 0.356 Thorium-229 HUh 0.0551 +/-0.163 0.296 Thorium-230 Hh 0.758 +/-0.377 0.392 Thorium-232 Hh 1.29 +/-0.445 0.261 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.023 +/-0.0528 0.0838 Curium-242 Hh 0.00 +/-0.105 0.157 Curium-243/244 HUh -0.00737 +/-0.0326 0.0851 Curium-245/246 Hh 0.0346 +/-0.0593 0.0519 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -6.39 +/-6.93 12.3 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0486 +/-0.219 0.469 Gammaspec, Gamma, Solid Dry Weight Corrected" Actinium-227 HUh -0.157 +/-0.211 0.349 Antimony-125 HUh -0.0387 +/-0.126 0.246 Bismuth-212 HUih 0.00 +/-1.13 1.48 Bismuth-214 Hh 1.11 +/-0.206 0.130 Cesium-137 Hh 1.44 +/-0.141 0.0816 Cobalt-60 HUh 0.0135 +/-0.045 0.093 Europium-154 HUh 0.077 +/-0.142 0.295 Lead-212 Hh 1.23 +/-0.128 0.0876 Lead-214 Hh 1.16 +/-0.204 0.125 Page 127of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0278 +/-0.0458 1.00 pCi/g JXH2 09/29/16 0918 1596393 2 0.016 +/-0.044 1.00 pCi/g 0.034 +/-0.047 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0489 +/-0.370 1.00 pCi/g 0.0366 +/-0.0747 1.00 pCi/g 0.0326 +/-0.284 1.00 pCi/g 0.298 +/-0.541 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.104 +/-0.477 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0922 +/-0.163 1.00 pCi/g 0.141 +/-0.389 1.00 pCi/g 0.0749 +/-0.472 1.00 pCi/g 0.0192 +/-0.0529 1.00 pCi/g JXH2 09/29/16 2150 1596390 6 0.00 +/-0.106 1.00 pCi/g 0.0195 +/-0.0327 1.00 pCi/g 0.00 +/-0.0595 1.00 pCi/g 5.98 +/-6.93 15.0 pCi/g JXH2 09/30/16 1349 1596394 7 0.192 +/-0.220 1.00 pCi/g MJHI 09/27/16 1618 1598618 8 *0.159 +/-O.f23 pCi/g MXRl 10/03/16 0806 1596247 9 0.113 +/-0.127 pCi/g 0.683 +/-1.50 pCi/g 0.0582 +/-0.212 pCi/g 0.0367 +/-0.154 0.100 pCi/g 0.0397 +/-0.0455 pCi/g 0.130 +/-0.147 pCi/g 0.0405 +/-0.144 pCi/g 0.057 +/-0.210 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R. l .3 Sample ID: 405235009 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.7 +/-1.73 Protactinium-231 HU!h 0.00 +/-0.637 Radium-226 Hh 1.11 +/-0.206 Radium-228 Hh 1.23 +/-0.340 Thallium-208 Hh 0.370 +/-0.110 Tin-126 HU!h 0.00 +/-0.0975 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 22.6 +/-4.30 Beta Hh 22.4 +/-2.59 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.735 +/-0.710 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.397 +/-2.08 Liquid Sein! CJ4, Solid "Dry Weight Corrected" Carbon-14 Hh 0.714 +/-0.802 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.944 +/-1.27 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.584 0.638 0.130 0.289 0.0768 0.0827 3.04 2.70 1.47 3.59 1.35 2.32 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 128 of 5809 0.229 +/-1.91 pCi/g 0.286 +/-0.707 pCi/g 0.0582 +/-0.212 pCi/g 0.127 +/-0.345 pCi/g 0.0348 +/-0.111 pCi/g 0.039 +/-0.0994 pCi/g 1.24 +/-6.15 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.27 +/-4.08 10.0 pCi/g 0.666 +/-0.710 2.00 pCi/g KSDl 09/17/16 1551 1597795 11 1.73 +/-2.08 6.00 pCi/g AEA 09/20/16 0150 1598072 12 0.655 +/-0.804 2.00 pCi/g AEA 09/22/16 0801 1598078 13 1.11 +/-1.27 5.00 pCi/g GXRl 09/20/16 0649 1597416 14 Analyst Date Time Prep Batch LYT! 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.l.3 Sample ID: 405235009 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 129 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 87 (15%-125%) 1596389 69.7 (15%-125%) 1596389 98.4 (15%-125%) 1596392 62.2 (15%-125%) 1596388 92.l (15%-125%) 1596390 99.5 (15%-125%) 1596394 87 (15%-125%) 1597795 85.5 (25%-125%) 1597416 89.4 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.l.D.R.1.4 Sample ID: 405235010 Matrix: Soil Collect Date: 1 O-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 20.1 % Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 22I 6 % Moisture "As Received" Moisture 20.1 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid Dry Weight Corrected" Plutonium-238 HUh -0.0211 +/-0.0707 0.170 Plutonium-239/240 HUh 0.00444 +/-0.0465 0.097 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0171 +/-0.0584 0.108 Uranium-233/234 Hh 0.741 +/-0.202 0.0903 Uranium-235/236 Hh 0.0451 +/-0.0616 0.084 Uranium-238 Hh 0.988 +/-0.232 0.0903 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0377 +/-0.167 0.434 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.58 +/-1.06 1.06 Thorium-229 HUh -0.0307 +/-0.225 0.541 Thorium-230 Hh 0.655 +/-0.580 0.480 Thorium-232 Hh 0.430 +/-0.490 0.479 Am24I, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.00982 +/-0.0634 0.130 Curium-242 Hh 0.00 +/-0.122 0.182 Curium-243/244 HUh -0.00427 +/-0.0369 0.0854 Curium-245/246 Hh 0.00 +/-0.0404 0.0602 Liquid Scint Pu24I, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.6 +/-6.58 11.4 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.030 +/-0.155 0.347 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0885 +/-0.226 0.422 Antimony-125 HUh 0.0788 +/-0.103 0.213 Bismuth-212 HUlh 0.00 +/-1.33 1.52 Bismuth-214 Hh 0.774 +/-0.182 0.134 Cesium-137 Hh 0.310 +/-0.0918 0.0698 Cobalt-60 HUlh 0.00 +/-0.0324 0.0816 Europium-154 HUh 0.0481 +/-0.114 0.238 Lead-212 Hh I.I I +/-0.141 0.0996 Lead-214 Hh 1.13 +/-0.213 0.120 Page 130 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst

Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0608 +/-0.0707 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0247 +/-0.0465 1.00 pCi/g 0.0295 +/-0.0585 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0246 +/-0.235 1.00 pCi/g 0.0214 +/-0.0621 1.00 pCi/g 0.0246 +/-0.282 1.00 pCi/g 0.0996 +/-0.167 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.305 +/-1.11 1.00 pCi/g JXH2 10/01/16 1254 1596388 5 0.103 +/-0.226 1.00 pCi/g 0.0726 +/-0.593 1.00 pCi/g 0.0724 +/-0.496 1.00 pCi/g 0.0386 +/-0.0635 1.00 pCi/g JXH2 09/29/16 2151 1596390 6 0.00 +/-0.122 1.00 pCi/g 0.016 +/-0.0369 1.00 pCi/g 0.00 +/-0.0405 1.00 pCi/g 5.57 +/-6.58 15.0 pCi/g JXH2 09/30/16 1450 1596394 7 0.136 +/-0.156 1.00 pCi/g MJHl 09/27/16 1619 1598618 8 0.195 +/-0.229 pCi/g MXRl 10/03/16 0806 1596247 9 0.0971 +/-0.109 pCi/g 0.707 +/-1.49 pCi/g 0.0606 +/-0.185 pCi/g 0.0311 +/-0.0928 0.100 pCi/g 0.0348 +/-0.0434 pCi/g 0.103 +/-0.116 pCi/g 0.0465 +/-0.153 pCi/g 0.0545 +/-0.218 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.l.4 Sample ID: 405235010 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.5 +/-1.65 Protactinium-231 HUh 0.0151 +/-0.546 Radium-226 Hh 0.774 +/-0.182 Radium-228 Hh 1.12 +/-0.275 Thallium-208 Hh 0.428 +/-0.0832 Tin-126 HUih 0.00 +/-0.199 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 15.9 +/-3.91 Beta Hh 23.5 +/-2.58 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.276 +/-0.501 Rad Liquid Scintillation Analysis LSC, Dist, Solid "Dry Weight Corrected" Tritium HUh 0.287 +/-2.03 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.232 +/-0.707 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.3 +/-1.15 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified . DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.779 0.989 0.134 0.194 0.0587 0.181 3.92 2.74 0.880 3.51 1.21 2.13 2 3 4 5 6 7 8 9 IO II 12 13 14 EPA 900.0/SW846 9310/SM 71 JOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 131 of 5809 0.335 +/-1.84 pCi/g 0.462 +/-0.546 pCi/g 0.0606 +/-0.185 pCi/g 0.0816 +/-0.280 pCi/g 0.026 +/-0.0852 pCi/g 0.0868 +/-0.203 pCi/g 1.68 +!-4.99 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.30 +/-4.17 10.0 pCi/g 0.390 +/-0.503 2.00 pCi/g KSDI 09/17/16 1551 1597795 II 1.69 +/-2.03 6.00 pCi/g AEA 09/20/16 0323 1598072 12 0.588 +/-0.708 2.00 pCi/g AEA 09/22/16 0847 1598078 13 1.02 +/-1.15 5.00 pCi/g GXRI 09/20/16 0705 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.l.4 Sample ID: 405235010 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Sein! Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 132 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 93.4 (15%-125%) 1596389 87.9 (15%-125%) 1596389 87.1 (15%-125%) 1596392 90 (15%-125%) 1596388 110 (15%-125%) 1596390 95.8 (15%-125%) 1596394 93.4 (15%-125%) 1597795 93.7 (25%-125%) 1597416 88.3 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.3.2 Sample ID: 405235011 Matnx: Soil Collect Date: 09-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 16.3% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 16.3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0814 +/-0.106 0.150 Plutonium-239/240 HUh 0.0272 +/-0.0749 0.130 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00718 +/-0.0399 0.0765 Uranium-233/234 Hh 0.819 +/-0.232 0.0916 Uranium-235/236 Hh 0.071 +/-0.0812 0.101 Uranium-238 Hh 0.823 +/-0.232 0.0793 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0501 +/-0.278 0.534 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.73 +/-0.653 0.491 Thorium-229 HUh 0.0209 +/-0.131 0.248 Thorium-230 Hh 1.66 +/-0.532 0.247 Thorium-232 Hh 1.07 +/-0.432 0.246 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.00946 +/-0.200 0.458 Curium-242 Hh 0.196 +/-0.545 0.587 Curium-243/244 HUh -0.0386 +/-0.118 0.335 Curium-245/246 HUh -0.00869 +/-0.128 0.275 Liquid Sein! Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -4.75 +/-5.90 10.3 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0943 +/-0.144 0.499 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0188 +/-0.242 0.'399 Antimony-125 HUh -0.00882 +/-0.112 0.217 Bismuth-212 HU!h 0.00 +/-0.762 1.17 Bismuth-214 Hh 1.13 +/-0.188 0.113 Cesium-137 Hh 0.255 +/-0.0833 0.0782 Cobalt-60 HUh -0.00648 +/-0.0355 0.0709 Europium-154 HUh -0.106 +/-0.0981 0.155 Lead-212 Hh 0.962 +/-0.130 0.0886 Lead-214 Hh 1.19 +/-0.193 0.0926 Page 133 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time -Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.043 +/-0.106 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0331 +/-0.0751 1.00 pCi/g 0.0175 +/-0.040 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.021 +/-0.270 1.00 pCi/g 0.0258 +/-0.0821 1.00 pCi/g 0.0148 +/-0.270 1.00 pCi/g 0.122 +/-0.279 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.161 +/-0.693 1.00 pCi/g JXH2 09/28/16 1406 1596388 5 0.0605 +/-0.131 1.00 pCi/g 0.0604 +/-0.574 1.00 pCi/g 0.0602 +/-0.454 1.00 pCi/g 0.145 +/-0.200 1.00 pCi/g JXH2 10/01/16 1323 1596390 6 0.00 +/-0.547 1.00 pCi/g 0.0821 +/-0.118 1.00 pCi/g 0.0414 +/-0.129 1.00 pCi/g 5.04 +/-5.90 15.0 pCi/g JXH2 10/03/16 0828 1596394 7 0.171 +/-0.151 1.00 pCi/g MIBI 09/27/16 1619 1598618 8 0.183 +/-0.242 pCi/g MXRl 10/03/16 0807 1596247 9 0.0988 +/-0.113 pCi/g 0.529 +/-0.871 pCi/g 0.0494 +/-0.194 pCi/g 0.0351 +/-0.084 0.100 pCi/g 0.0291 +/-0.0356 pCi/g 0.0607 +/-0.109 pCi/g 0.0408 +/-0.139 pCi/g 0.0406 +/-0.199 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.3.2 Sample ID: 405235011 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.5 +/-1.61

Protactinium-231 HUih 0.00 +/-0.713 Radium-226 Hh 1.13 +/-0.188 Radium-228 Hh 1.13 +/-0.312 Thallium-208 Hh 0.309 +/-0.0942 Tin-126 HUih 0.00 +/-0.168 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 14.2 +/-3.46 Beta Hh 23.0 +/-2.53 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.237 +/-0.610 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.641 +/-1.82 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0917 +/-0.685 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.654 +/-1.01 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.668 0.700 0.113 0.192 0.0662 0.149 3.42 2.57 1.10 3.11 1.19 1.83 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 134 of 5809 0.276 +/-1.78 pCi/g 0.316 +/-0.718 pCi/g 0.0494 +/-0.194 pCi/g 0.0797 +/-0.317 pCi/g 0.0295 +/-0.0951 pCi/g 0.0702 +/-0.169 pCi/g 1.47 +l-4.45 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.21 +/-4.10 10.0 pCi/g 0.482 +/-0.611 2.00 pCi/g KSDl 09/17/16 1632 1597795 11 1.50 +/-1.82 6.00 pCi/g AEA 09/20/16 0607 1598072 12 0.577 +/-0.685 2.00 pCi/g AEA 09/22/16 0934 1598078 13 0.874 +/-1.01 5.00 pCi/g GXRl 09/20/16 0721 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.3.2 Sample ID: 405235011 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 135 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 67.8 (15%-125%) 1596389 73.8 (15%-125%) 1596389 102 (15%-125%) 1596392 70.3 (15%-125%) 1596388 76 (15%-125%) 1596390 38.4 (15%-125%) 1596394 67.8 (15%-125%) 1597795 82.8 (25%-125%) 1597416 92.7 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.2.4 Sample ID: 405235012 Matrix: Soil Collect Date: lO-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 17% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.0 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00464 +/-0.0485 0.101 Plutonium-239/240 HUh -0.0198 +/-0.0375 0.116 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 Hh 0.0538 +/-0.0681 0.0846 Uranium-233/234 Hh 0.798 +/-0.206 0.0822 Uranium-235/236 Hh 0.0918 +/-0.0809 0.0946 Uranium-238 Hh 0.871 +/-0.214 0.0645 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0255 +/-0.267 0.557 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.17 +/-0.926 0.977 Thorium-229 HUh -0.031 +/-0.225 0.541 Thorium-230 Hh 1.19 +/-0.757 0.540 Thorium-232 Hh 0.887 +/-0.653 0.333 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.00646 +/-0.0446 0.109 Curium-242 Hh 0.00 +/-0.102 0.152 Curium-243/244 HUh 0.00775 +/-0.043 0.0825 Curium-245/246 HXh 0.0503 +/-0.0662 0.0503 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -4.13 +/-6.82 12.0 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.131 +/-0.161 0.521 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.00685 +/-0.243 0.428 Antimony-125 HUh 0.0103 +/-0.121 0.250 Bismuth-212 HU!h 0.00 +/-1.08 1.56 Bismuth-214 Hh 0.847 +/-0.209 0.137 Cesium-137 Hh 0.364 +/-0.102 0.103 Cobalt-60 HUh -0.00745 +/-0.0467 0.0973 Europium-154 HUh -0.11 +/-0.155 0.275 Lead-212 Hh 1.39 +/-0.158 0.0897 Lead-214 Hh I.OJ +/-0.208 0.149 Page 136 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOO 1 Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0258 +/-0.0486 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0331 +/-0.0375 1.00 pCi/g 0.0194 +/-0.0686 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0209 +/-0.243 1.00 pCi/g 0.0271 +/-0.0822 1.00 pCi/g 0.0121 +/-0.256 1.00 pCi/g 0.142 +/-0.267 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.265 +/-0.959 1.00 pCi/g JXH2 10/01/16 1254 1596388 5 0.103 +/-0.226 1.00 pCi/g 0.103 +/-0.791 1.00 pCi/g 0.00 +/-0.675 1.00 pCi/g 0.0323 +/-0.0446 1.00 pCi/g JXH2 09/29/16 2152 1596390 6 0.00 +/-0.102 1.00 pCi/g 0.0189 +/-0.0431 1.00 pCi/g 0.00 +/-0.0666 1.00 pCi/g 5.83 +/-6.82 15.0 pCi/g JXH2 09/30/16 1652 1596394 7 0.191 +/-0.172 1.00 pCi/g MJHl 09/27/16 1620 1598618 8 0.192 +/-0.243 pCi/g MXRl 10/03/16 0807 1596247 9 0.111 +/-0.121 pCi/g 0.696 +/-1.26 pCi/g 0.058 +/-0.213 pCi/g 0.0452 +/-0.103 0.100 pCi/g 0.0383 +/-0.0468 pCi/g 0.110 +/-0.163 pCi/g 0.0403 +/-0.174 pCi/g 0.0665 +/-0.213 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.2.4 Sample ID: 405235012 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.8 +/-1.96 Protactinium-231 HUh 0.324 +/-0.525 Radium-226 Hh 0.847 +/-0.209 Radium-228 Hh 1.01 +/-0.321 Thallium-208 Hh 0.331 +/-0.106 Tin-126 HUih 0.00 +/-0.185 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh I 1.6 +/-3.25 Beta Hh 24.8 +/-2.62 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 0.780 +/-0.883 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.731 +/-1.86 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.321 +/-0.659 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.629 +/-1.08 The following Prep Methods were performed Method . Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-O I Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.908 1.05 0.137 0.298 0.0886 0.164 3.42 2.63 1.48 3.19 1.12 1.96 2 3 4 5 6 7 8 9 IO II 12 13 14 EPA 900.0/SW846 9310/SM 71 JOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 137of5809 0.359 +/-2.09 pCi/g 0.481 +/-0.550 pCi/g 0.058 +/-0.213 pCi/g 0.123 +/-0.325 pCi/g 0.039 +/-0.107 pCi/g 0.0774 +/-0.186 pCi/g 1.45 +/-3.97 4.00 pCi/g JXC9 09119116 1232 1597816 10 1.24 +/-4.33 10.0 pCi/g 0.669 +/-0.894 2.00 pCi/g KSDI 09/17/16 1632 1597795 11 1.54 +/-1.86 6.00 pCi/g AEA 09/20/16 0740 1598072 12 0.545 +/-0.660 2.00 pCi/g AEA 09/22/16 1020 1598078 13 0.936 +/-1.08 5.00 pCi/g GXRI 09/20/16 0738 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.1.D.R.2.4 Sample ID: 405235012 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 138 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 90.6 (15%-125%) 1596389 87.7 (15%-125%) 1596389 108 (15%-125%) 1596392 77.6 (15%-125%) 1596388 101 (15%-125%) 1596390 104 (15%-125%) 1596394 90.6 (15%-125%) 1597795 88.3 (25%-125%) 1597416 94.3 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.2.3 SamI?le ID: 405235013 Matnx: Soil

Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 21.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 21.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.000765 +/-0.0567 0.126 Plutonium-239/240 Hh 0.0388 +/-0.0771 0.125 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0102 +/-0.0383 0.0644 Uranium-233/234 Hh 0.778 +/-0.213 0.111 Uranium-235/236 Hh 0.065 +/-0.070 0.0796 Uranium-238 Hh 0.750 +/-0.209 0.111 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.127 +/-0.437 0.837 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 2.23 +/-1.33 1.06 Thorium-229 HUh -0.0188 +/-0.271 0.584 Thorium-230 Hh 0.658 +/-0.652 0.583 Thorium-232 Hh 1.20 +/-0.838 0.581 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0102 +/-0.0307 0.0864 Curium-242 Hh 0.00 +/-0.0992 0.148 Curium-243/244 HUh O.oJ 15 +/-0.0515 0.101 Curium-245/246 Hh 0.0323 +/-0.0554 0.0485 Liquid Scint Pu24 l, Solid "Dry Weight Corrected" Plutonium-241 HUh -6.24 +/-8.21 14.5 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0471 +/-0.319 0.718 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0235 0.466 Antimony-125 HUh 0.0468 +/-0.134 0.260 Bismuth-212 HUih 0.00 +/-1.02 1.58 Bismuth-214 Hh 0.858 +/-0.186 0.123 Cesium-137 Hh 1.22 +/-0.158 0.0943 Cobalt-60 HUh -0.0363 +/-0.0431 0.0683 Europium-154 HUh 0.0172 +/-0.146 0.294 Lead-212 Hh 1.18 +/-0.136 0.102 Lead-214 Hh 1.03 +/-0.203 0.148 Page 139 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 0.0343 +/-0.0568 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0341 +/-0.0773 1.00 pCi/g 0.0121 +/-0.0384 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.034 +/-0.247 1.00 pCi/g 0.0182 +/-0.0708 1.00 pCi/g 0.034 +/-0.241 1.00 pCi/g 0.278 +/-0.438 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.255 +/-1.42 1.00 pCi/g JXH2 10/01/16 1254 1596388 5 0.0887 +/-0.272 1.00 pCi/g 0.0885 +/-0.666 1.00 pCi/g 0.0882 +/-0.874 1.00 pCi/g 0.022 +/-0.0308 1.00 pCi/g JXH2 09/29/16 2152 1596390 6 0.00 +/-0.0994 1.00 pCi/g 0.0288 +/-0.0515 1.00 pCi/g 0.00 +/-0.0556 1.00 pCi/g 7.05 +/-8.21 15.0 pCi/g JXH2 09/30/16 1753 1596394 7 0.278 +/-0.320 1.00 pCi/g MJHl 09/28/16 0636 1598618 8 0.215 +/-0.246 pCi/g MXRl 10/03/16 0810 1596247 9 0.119 +/-0.136 pCi/g 0.726 +/-1.24 pCi/g 0.0537 +/-0.200 pCi/g 0.0425 +/-0.187 0.100 pCi/g 0.026 +/-0.0462 pCi/g 0.126 +/-0.147 pCi/g 0.0473 +/-0.176 pCi/g 0.0678 +/-0.221 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.2.3 Sample ID: 405235013 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.4 +/-1.78 Protactinium-231 HU!h 0.00 +/-1.09 Radium-226 Hh 0.858 +/-0.186 Radium-228 Hh 0.907 +/-0.350 Thallium-208 Hh 0.329 +/-0.0958 Tin-126 HU!h 0.00 +/-0.108 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 17.1 +/-4.66 Beta Hh 24.3 +/-3.36 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh -0.385 +/-0.682 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Dry Weight Corrected" Tritium HUh 0.645 +/-2.14 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0611 +/-0.626 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.556 +/-1.12 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.742 0.832 0.123 0.278 0.0729 0.106 3.84 3.15 1.36 3.68 1.08 2.01 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 140 of 5809 0.297 +/-2.12 pCi/g 0.379 +/-1.13 pCi/g 0.0537 +/-0.200 pCi/g 0.119 +/-0.367 pCi/g 0.0323 +/-0.0999 pCi/g 0.0502 +/-0.110 pCi/g 1.50 +/-5.72 4.00 pCi/g JXC9 09/20/16 1156 1597816 10 1.45 +/-4.90 10.0 pCi/g 0.612 +/-0.682 2.00 pCi/g KSDI 09/17/16 1632 1597795 II 1.78 +/-2.14 6.00 pCi/g AEA 09/20/16 0913 1598072 12 0.527 +/-0.626 2.00 pCi/g AEA 09/22/16 1106 1598078 13 0.962 +/-1.12 5.00 pCi/g GXRI 09/20/16 0754 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.2.3 Sample ID: 405235013 Certificate of Analysis Report Date: Project: MJWCOO 115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 141of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 75.4 (15%-125%) 1596389 90.2 (15%-125%) 1596389 107 (15%-125%) 1596392 76.1 (15%-125%) 1596388 90.2 (15%-125%) 1596390 109 (15%-125%) 1596394 75.4 (15%-125%) 1597795 95 (25%-125%) 1597416 89.6 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R. l .3 Sample ID: 405235014 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 15.2% Parameter Qualifier* Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 15.2 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid Dry Weight Corrected" Plutonium-238 Hh 0.0265 +l-0.0609 0.0966 Plutonium-239/240 HUh 0.0402 +/-0.0793 0.134 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00397 +/-0.0415 0.0865 Uranium-233/234 Hh 0.886 +/-0.238 0.111 Uranium-235/236 Hh 0.044 +/-0.0633 0.0764 Uranium-238 Hh 1.07 +/-0.259 0.0879 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.150 +/-0.630 1.24 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.94 +/-1.43 1.46 Thorium-229 HUh -0.0914 +/-0.337 0.922 Thorium-230 Hh 1.45 +/-1.02 0.705 Thorium-232 Hh 0.326 +/-0.555 0.489 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.00484 +/-0.0551 0.117 Curium-242 Hh 0.0526 +/-0.148 0.158 Curium-243/244 HUh -0.00368 +/-0.0318 0.0736 Curium-245/246 Hh 0.0173 +/-0.0486 0.0519 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -8.27 +/-7.14 12.8 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0846 +/-0.298 0.592 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0454 +/-0.230 0.451 Antimony-125 HUh 0.0232 +/-0.125 0.215 Bismuth-212 HUih 0.00 +/-0.928 1.31 Bismuth-214 Hh 0.734 +/-0.194 0.140 Cesium-137 Hh 0.651 +/-0.115 0.0842 Cobalt-60 HUh 0.0222 +/-0.043 0.0952 Europium-154 HUh -0.0276 +/-0.114 0.223 Lead-212 Hh 1.15 +/-0.129 0.0938 Lead-214 Hh 0.941 +/-0.177 0.130 Page 142of5809 Report Date: October4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units

PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.0221 +/-0.061 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0411 +/-0.0795 1.00 pCi/g 0.022 +/-0.0415 1.00 pCi/g JXH2 09/29/16 0913 1596389 3 0.0319 +/-0.280 1.00 pCi/g 0.0143 +/-0.0637 1.00 pCi/g 0.0202 +/-0.315 1.00 pCi/g 0.417 +/-0.630 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.402 +/-1.51 1.00 pCi/g JXH2 10/01/16 1254 1596388 5 0.215 +/-0.339 1.00 pCi/g 0.107 +/-1.07 1.00 pCi/g 0.00 +/-0.560 1.00 pCi/g 0.0359 +/-0.0552 1.00 pCi/g JXH2 09/29/16 2152 1596390 6 0.00 +/-0.148 1.00 pCi/g 0.0138 +/-0.0318 1.00 pCi/g 0.00 +/-0.0487 1.00 pCi/g 6.21 +/-7.14 15.0 pCi/g JXH2 09/30/16 1854 1596394 7 0.210 +/-0.301 1.00 pCi/g MJHI 09/28/16 0645 1598618 8 0.209 +/-0.231 pCi/g MXRI 10/03/16 0811 1596247 9 0.0976 +/-0.125 pCi/g 0.598 +/-0.996 pCi/g 0.0629 +/-0.197 pCi/g 0.038 +/-0.118 0.100 pCi/g 0.0408 +/-0.0441 pCi/g 0.0936 +/-0.115 pCi/g 0.0435 +/-0.143 pCi/g 0.0591 +/-0.181 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R. I .3 Sample ID: 405235014 Certificate of Analysis Report Date: Project: MJWCOOll5 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.8 +/-1.64 Protactinium-231 HUih 0.00 +/-0.997 Radium-226 Hh 0.734 +/-0.194 Radium-228 Hh 1.22 +/-0.270 Thallium-208 Hh 0.296 +/-0.105 Tin-126 HUih 0.00 +/-0.0993 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 17.6 +/-4.06 Beta Hh 21.5 +/-2.78 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.0021 +/-0.944 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.668 +/-1.89 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0653 +/-0.648 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.179 +/-1.17 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.686 0.832 0.140 0.266 0.0728 0.196 3.43 3.23 1.72 3.25 1.12 2.03 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 143 of 5809 0.281 +/-1.82 pCi/g 0.383 +/-1.02 pCi/g 0.0629 +/-0.197 pCi/g 0.116 +/-0.277 pCi/g 0.0328 +/-0.106 pCi/g 0.0937 +/-0.135 pCi/g 1.41 +/-5.34 4.00 pCi/g JXC9 09119116 1416 1597816 10 1.54 +/-4.09 10.0 pCi/g 0.792 +/-0.944 2.00 pCi/g KSDI 09/17/16 1632 1597795 11 1.57 +/-1.89 6.00 pCi/g AEA 09/20/16 1046 1598072 12 0.546 +/-0.648 2.00 pCi/g AEA 09/22/16 1152 1598078 13 0.972 +/-1.17 5.00 pCi/g GXRI 09/20/16 0810 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R. l .3 Sample ID: 405235014 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 144 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 86 (15%-125%) 1596389 69.5 (15%-125%) 1596389 101 (15%-125%) 1596392 51.5 (15%-125%) 1596388 72.6 (15%-125%) 1596390 97.5 (15%-125%) 1596394 86 (15%-125%) 1597795 93.7 (25%-125%) 1597416 83.5 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R. l .4 Sample ID: 405235015 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 7.15% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 7.15 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0659 +/-0.0753 0.0941 Plutonium-239/240 HUh -0.0147 +/-0.034 0.101 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00798 +/-0.0745 0.173 Uranium-233/234 Hh 0.674 +/-0.230 0.160 Uranium-235/236 Hh 0.102 +/-0.097 0.102 Uranium-238 Hh 0.881 +/-0.256 0.129 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0721 +/-0.360 0.720 Alphaspec Th229 + 228,23q,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.32 +/-0.551 0.451 Thorium-229 Hh 0.153 +/-0.217 0.336 Thorium-230 Hh 0.516 +/-0.336 0.406 Thorium-232 Hh 0.974 +/-0.393 0.224 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0111 +/-0.0681 0.134 Curium-242 Hh 0.00 +/-0.166 0.253 Curium-243/244 HUh -0.00328 +/-0.0487 0.105 Curium-245/246 Hh 0.106 +/-0.121 0.118 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -7.61 +/-6.12 11.0 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUih 0.00 +/-0.176 0.244 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.376 +/-0.266 0.400 Antimony-125 HUh 0.0241 +/-0.102 0.206 Bismuth-212 HUih 0.00 +/-0.878 1.34 Bismuth-214 Hh 0.879 +/-0.200 0.130 Cesium-137 Hh 0.257 +/-0.0964 0.0799 Cobalt-60 HUih 0.00 +/-0.0531 0.0945 Europium-154 HUh -0.0622 +/-0.139 0.252 Lead-212 Hh 1.07 +/-0.136 0.0919 Lead-214 Hh 1.16 +/-0.195 0.349 Page 145 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0239 +/-0.0759 1.00 pCi/g JXH2 09/29/16 0944 1596393 2 0.0275 +/-0.0341 1.00 pCi/g 0.0566 +/-0.0746 1.00 pCi/g JXH2 09/29/16 0920 1596389 3 0.0523 +/-0.260 1.00 pCi/g 0.0235 +/-0.0987 1.00 pCi/g 0.037 +/-0.301 1.00 pCi/g 0.231 +/-0.360 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.149 +/-0.577 1.00 pCi/g JXH2 09/28/16 1407 1596388 5 0.110 +/-0.217 1.00 pCi/g 0.145 +/-0.343 1.00 pCi/g 0.0548 +/-0.412 1.00 pCi/g 0.0309 +/-0.0682 1.00 pCi/g JXH2 10/01/16 1323 1596390 6 0.00 +/-0.167 1.00 pCi/g 0.0157 +/-0.0488 1.00 pCi/g 0.0176 +/-0.122 1.00 pCi/g 5.33 +/-6.12 15.0 pCi/g JXH2 09/30/16 1955 1596394 7 0.00 +/-0.00 1.00 pCi/g MJHl 09/28/16 0648 1598618 8 0.182 +/-0.319 pCi/g MXRl 10/03/16 0811 1596247 9 0.0924 +/-0.102 pCi/g 0.609 +/-0.940 pCi/g 0.0575 +/-0.203 pCi/g 0.0356 +/-0.0971 0.100 pCi/g 0.0402 +l-0.0565 pCi/g 0.108 +/-0.142 pCi/g 0.0423 +/-0.147 pCi/g 0.168 +/-0.201 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.l.4 Sample ID: 405235015 Parameter Qualifier Result Uncertainty Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dry Weight Corrected" Potassium-40 Hh 17.4 +/-1.80 Protactinium-231 HUih 0.00 +/-0.802 Radium-226 Hh 0.879 +/-0.200 Radium-228 Hh 0.964 +/-0.340 Thallium-208 Hh 0.352 +/-0.0898 Tin-126 HUih 0.00 +/-0.159 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" MDC 0.678 0.825 0.130 0.292 0.0652 0.158 Alpha Hh 19.0 +/-4.27 3.92 Beta Hh 19.4 +/-2.44 2.83 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.139 +/-0.756 1.41 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -J.12 +/-1.71 3.05 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.327 +/-0.617 1.05 Liquid Scint Tc99, Solid Dry Weight Corrected" Technetium-99 HUh -0.265 +/-0.925 1.64 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 JO 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-OJ-RC Modified DOE EML HASL-300, Am-05.-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 JOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 MC?dified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 146of5809 Report Date: Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst 0.275 +/-2.02 pCi/g 0.377 +/-0.812 pCi/g 0.0575 +/-0.203 pCi/g 0.128 +/-0.343 pCi/g 0.0287 +/-0.0911 pCi/g 0.0744 +/-0.159 pCi/g 1.67 +/-5.70 4.00 pCi/g JXC9 1.35 +/-3.63 10.0 pCi/g 0.646 +/-0.756 2.00 pCi/g KSDJ 1.47 +/-1.71 6.00 pCi/g AEA 0.510 +/-0.617 2.00 pCi/g AEA 0.787 +/-0.925 5.00 pCi/g GXRI Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 October 4, 2016 Date Time Batch Mtd. 09/19/16 1232 1597816 JO 09/17/16 1632 1597795 II 09/20/16 1219 1598072 12 09/22/16 1239 1598078 13 09/20/16 1231 1597416 14 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R. l .4 Sample ID: 405235015 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 147of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 97.3 (15%-125%) 1596389 81.7 (15%-125%) 1596389 74 (15%-125%) 1596392 81 (15%-125%) 1596388 88.5 (15%-125%) 1596390 87.4 (15%-125%) 1596394 97.3 (15%-125%) 1597795 96.4 (25%-125%) 1597416 93.8 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.2.4 Sample ID: 405235016 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 20.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 20.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0115 +/-0.0348 Plutonium-239/240 HUh 0.0121 +/-0.0454 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0171 +/-0.0465 Uranium-233/234 Hh 0.764 +/-0.242 Uranium-235/236 Uranium-238 Hh Hh 0.0706 0.689 +/-0.0832 +/-0.230 Alphaspec Np237, Solid "Dry Weight Corrected" 0.0979 0.0763 0.124 0.131 0.090 0.131 Neptunium-237 HUh -0.108 +/-0.204 0.631 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.879 +/-0.681 1.04 Thorium-229 Hh 0.113 +/-0.177 0.266 Thorium-230 Hh 1.31 +/-0.487 0.454 Thorium-232 Hh 1.40 +/-0.470 0.298 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0511 +/-0.0689 0.236 Curium-242 Hh 0.00 +/-0.219 0.332 Curium-243/244 HUh -0.013 +/-0.0652 0.168 Curium-245/246 Hh 0.0361 +/-0.101 0.108 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -8.9 +/-6.01 10.8 Rad Gamma Spec Analysis Gamma IJ 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0336 +/-0.117 0.563 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.157 +/-0.227 0.431 Antimony-125 HUh 0.0581 +/-0.116 0.213 Bismuth-212 HUih 0.00 +/-1.14 1.39 Bismuth-214 Hh 0.734 +/-0.186 0.114 Cesium-137 Hh 0.080 +/-0.089 0.086 Cobalt-60 HUh 0.0157 +/-0.0357 0.079 Eu!opium-154 HUh 0.0746 +/-0.106 0.238 Lead-212 Hh 1.09 +/-0.138 0.0936 Lead-214 Hh 1.02 +/-0.200 0.135 Page 148 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0249 +/-0.0349 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0143 +/-0.0454 1.00 pCi/g 0.0398 +/-0.0465 1.00 pCi/g JXH2 09/29/16 0920 1596389 3 0.0376 +/-0.276 1.00 pCi/g 0.0168 +/-0.0841 1.00 pCi/g 0.0376 +/-0.260 1.00 pCi/g 0.180 +/-0.205 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.445 +/-0.691 1.00 pCi/g JXH2 09/28/16 1407 1596388 5 0.0764 +/-0.178 1.00 pCi/g 0.170 +/-0.515 1.00 pCi/g 0.0931 +/-0.503 1.00 pCi/g 0.0704 +/-0.0691 1.00 pCi/g JXH2 10/01/16 1323 1596390 6 0.00 +/-0.220 1.00 pCi/g 0.0357 +/-0.0654 1.00 pCi/g 0.00 +/-0.101 1.00 pCi/g 5.27 +/-6.01 15.0 pCi/g JXH2 09/30/16 2057 1596394 7 0.139 +/-0.118 1.00 pCi/g MJHI 09/28/16 0655 1598618 8 0.200 +/-0.239 pCi/g MXRl 10/03/16 0815 1596247 9 0.0975 +/-0.119 pCi/g 0.647 +/-1.39 pCi/g 0.0503 +/-0.188 pCi/g 0.0392 +/-0.0891 0.100 pCi/g 0.0335 +/-0.0364 pCi/g 0.103 +/-0.111 pCi/g 0.0436 +/-0.150 pCi/g 0.0623 +/-0.205 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.2.4 Sample ID: 405235016 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.0 +/-1.39 Protactinium-231 HUh -0.259 +/-0.411 Radium-226 Hh 0.734 +/-0.186 Radium-228 Hh 0.899 +/-0.294 Thallium-208 Hh 0.321 +/-0.0818 Tin-126 HU!h 0.00 +/-0.175 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.1 +/-3.81 Beta Hh 23.6 +/-2:65 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.157 +/-0.413 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.501 +/-2.13 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.359 +/-0.742 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.98 +/-1.23 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,l-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.376 0.747 0.114 0.184 0.0556 0.192 3.52 2.83 0.766 3.73 1.26 2.24 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 149 of 5809 0.133 +l-1.55 pCi/g 0.342 +/-0.431 pCi/g 0.0503 +/-0.188 pCi/g 0.0766 +/-0.298 pCi/g 0.0245 +/-0.083 pCi/g 0.0916 +/-0.183 pCi/g 1.49 +/-5.01 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.34 +/-4.26 10.0 pCi/g 0.320 +/-0.414 2.00 pCi/g KSDI 09/17/16 1631 1597795 II 1.80 +/-2.13 6.00 pCi/g AEA 09/20/16 1352 1598072 12 0.614 +/-0.743 2.00 pCi/g .AEA 09/22/16 1325 1598078 13 1.07 +/-1.23 5.00 pCi/g GXRl 09/20/16 0842 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.2.4 Sample ID: 405235016 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry.Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 150of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 98 (15%-125%) 1596389 80 (15%-125%) 1596389 101 (15%-125%) 1596392 76.l (15%-125%) 1596388 87.6 (15%-125%) 1596390 67.6 i,(15%-125%) 1596394 98 (15%-125%) 1597795 95 (25%-125%) 1597416 88.8 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.3.2 Sample ID: 405235017 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 22.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 22.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0101 +/-0.0564 0.108 Plutonium-239/240 HUh 0.0248 +/-0.0683 0.118 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0271 +/-0.0616 0.106 Uranium-233/234 Hh 1.04 +/-0.387 0.196 Uranium-235/236 HUh -0.00851 +/-0.0734 0.170 Uranium-238 Hh 1.35 +/-0.440 0.233 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.152 +/-0.517 0.974 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.59 +/-0.554 0.370 Thorium-229 HUh -0.122 +/-0.270 0.586 Thorium-230 Hh 1.18 +/-0.466 0.511 Thorium-232 Hh 0.739 +/-0.328 0.237 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0671 +/-0.121 0.309 Curium-242 Hh 0.00 +/-0.192 0.285 Curium-243/244 HUh 0.0141 +/-0.0781 0.150 Curium-245/246 HUh -0.0146 +/-0.0646 0.169 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -9.98 +/-8.06 14.4 Rad Gamma Spec Analysis Gamma Il29, Solid "Dry Weight Corrected" Iodine-129 HUih 0.00 +/-0.330 0.676 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.100 +/-0.247 0.496 Antimony-125 HUh 0.019 +/-0.131 0.251 Bismuth-212 Hh 1.65 +/-0.904 0.837 Bismuth-214 Hh 1.13 +/-0.189 0.132 Cesium-137 Hh 3.94 +/-0.228 0.0716 Cobalt-60 HUh -0.011 +/-0.0417 O.D78 HUh 0.0439 +/-0.0997 0.215 Lead-212 Hh 1.19 +/-0.137 0.0944 Lead-214 Hh 1.13 +/-0.234 0.145 Page 151of5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent L YT! 09/08/16 0806 1596227 1 0.0248 +/-0.0564 1.00 pCi/g JXH2 09129116 0923 1596393 2 0.0301 +/-0.0684 1.00 pCi/g 0.0303 +/-0.0619 1.00 pCi/g JXH2 09/29/16 0920 1596389 3 0.0449 +/-0.448 1.00 pCi/g 0.0318 +/-0.0738 1.00 pCi/g 0.0635 +/-0.527 1.00 pCi/g 0.377 +/-0.517 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.117 +/-0.589 1.00 pCi/g JXH2 09/28/16 1407 1596388 5 0.242 +/-0.270 1.00 pCi/g 0.205 +/-0.489 1.00 pCi/g 0.0682 +/-0.340 1.00 pCi/g 0.115 +/-0.121 1.00 pCi/g JXH2 09/29/16 2152 1596390 6 0.00 +/-0.192 1.00 pCi/g 0.0343 +/-0.0783 1.00 pCi/g 0.0386 +/-0.0648 1.00 pCi/g 7.02 +/-8.06 15.0 pCi/g JXH2 09/30/16 2158 1596394 7 0.242 +/-0.333 1.00 pCi/g MJHl 09/28/16 0722 1598618 8 0.233 +/-0.252 pCi!g MXRl 10/03/16 0816 1596247 9 0.116 +/-0.131 pCi/g 0.370 +/-0.908 pCi/g 0.0597 +/-0.195 pCi/g 0.0322 +/-0.284 0.100 pCi/g 0.0331 +/-0.042 pCi/g 0.092 +/-0.102 pCi/g 0.0441 +/-0.151 pCi/g 0.0673 +/-0.238 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.3.2 Sample ID: 405235017 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 16.0 +/-1.58 0.702 Protactinium-231 HU!h 0.00 +/-1.04 0.948 Radium-226 Hh 1.13 +/-0.189 0.132 Radium-228 Hh 0.829 +/-0.336 0.251 Thallium-208 Hh 0.342 +/-0.104 0.0704 Tin-126 HU!h 0.00 +/-0.158 0.145 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 19.4 +/-4.17 3.05 Beta Hh 21.2 +/-2.50 2.73 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 0.570 +/-0.475 0.747 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.921 +/-2.14 3.66 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.168 +/-0.740 1.29 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.03 +/-1.32 2.40 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 IO II 12 13 14 ASTM D 22I6 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL.-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-0I Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 93 IO/SM 711 OB Modified EPA 905.0 Modified/DOE RP50I Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 152 of 5809 0.298 +/-1.79 pCi/g 0.444 +/-1.07 pCi/g 0.0597 +/-0.195 pCi/g 0.111 +/-0.339 pCi/g 0.032 +/-0.105 pCi/g 0.0689 +/-0.158 pCi/g 1.22 +/-5.62 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.29 +/-3.87 10.0 pCi/g 0.317 +/-0.486 2.00 pCi/g KSDI 09/17/16 1634 1597795 II 1.77 +/-2.14 6.00 pCi/g AEA 09/20/I6 1525 I598072 12 0.625 +/-0.740 2.00 pCi/g AEA 09/22/16 1411 1598078 13 1.15 +/-1.32 5.00 pCi/g GXRI 09/20/16 0858 I5974I6 I4 Analyst Date Time Prep Batch LYTI 09/08/I6 0806 I596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.3.2 Sample ID: 405235017 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 153 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 75.8 (15%-125%) 1596389 41.6 (15%-125%) 1596389 102 (15%-125%) 1596392 91.9 (15%-125%) 1596388 100 (15%-125%) 1596390 57.4 (15%-125%) 1596394 75.8 (15%-125%) 1597795 95 (25%-125%) 1597416 87.9 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.4.2 Sample ID: 405235018 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 21.7% Parameter

Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 21.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh 0.0285 +/-0.0752 0.135 Plutonium-239/240 HUh -0.00436 +/-0.0376 0.0871 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 Hh 0.0404 +/-0.0643 0.0889 Uranium-233/234 Hh 0.671 +/-0.244 0.157 Uranium-235/236 HUh 0.0162 +/-0.0608 0.102 Uranium-238 Hh 0.761 +/-0.258 0.149 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0813 +/-0.154 0.475 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.22 +/-0.546 0.438 Thorium-229 Hh 0.143 +/-0.188 0.240 Thorium-230 Hh 0.732 +/-0.402 0.453 Thorium-232 Hh 0.671 +/-0.343 0.239 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0041 +/-0.0428 0.0894 Curium-242 Hh 0.00 +/-0.105 0.157 Curium-243/244 HUh -0.0143 +/-0.0331 0.0979 Curium-245/246 HXh 0.0836 +/-0.0807 0.0502 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.157 +/-5.24 8.99 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.237 +/-0.378 0.630 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.116 +/-0.222 0.448 Antimony-125 HUh 0.046 +/-0.108 0.212 Bismuth-212 HUih 0.00 +/-0.699 1.19 Bismuth-214 Hh 0.578 +/-0.166 0.121 Cesium-137 Hh 2.22 +/-0.163 0.0621 Cobalt-60 HUh 0.0103 +/-0.0236 0.0511 Europium-154 HUh -0.0371 +/-0.0869 0.159 Lead-212 Hh 1.06 +/-0.121 0.085 Lead-214 Hh 1.07 +/-0.177 0.118 Page 154 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 1 0.0402 +/-0.0753 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0163 +/-0.0377 1.00 pCi/g 0.0204 +/-0.0647 1.00 pCi/g JXH2 09/29/16 0920 1596389 3 0.0467 +/-0.273 1.00 pCi/g 0.0191 +/-0.0609 1.00 pCi/g 0.0427 +/-0.293 1.00 pCi/g 0.136 +/-0.154 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.137 +/-0.570 1.00 pCi/g JXH2 09/28/16 1407 1596388 5 0.0586 +/-0.189 1.00 pCi/g 0.165 +/-0.413 1.00 pCi/g 0.0583 +/-0.354 1.00 pCi/g 0.0227 +/-0.0429 1.00 pCi/g JXH2 09/29/16 2152 1596390 6 0.00 +/-0.106 1.00 pCi/g 0.0267 +/-0.0331 1.00 pCi/g 0.00 +/-0.0814 1.00 pCi/g 4.40 +/-5.24 15.0 pCi/g JXH2 10/03/16 1029 1596394 7 0.224 +/-0.394 1.00 pCi/g MJHI 09/28/16 0722 1598618 8 0.211 +/-0.228 pCi/g MXRl 10/03/16 0816 1596247 9 0.0986 +/-0.110 pCi/g 0.553 +/-0.986 pCi/g 0.0553 +/-0.168 pCi/g 0.028 +/-0.189 0.100 pCi/g 0.0207 +/-0.0241 pCi/g 0.0667 +/-0.0885 pCi/g 0.0398 +/-0.134 pCi/g 0.0545 +/-0.182 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.4.2 Sample ID: 405235018 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.2 +/-1.35 Protactinium-231 HU!h 0.00 +/-0.673 Radium-226 Hh 0.578 +/-0.166 Radium-228 Hh 0.974 +/-0.282 Thallium-208 Hh 0.262 +/-0.0775 Tin-126 HUih 0.00 +/-0.110 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 13.3 +/-3.55 Beta Hh 21.0 +/-2.40 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.336 +/-0.801 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.0322 +/-2.18 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.0823 +/-0.648 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.527 +/-1.22 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC: Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.500 0.790 0.121 0.204 0.0598 0.107 4.00 2.39 1.41 3.79 1.11 2.19 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 7110B Modified EPA 905.0 Modified/DOE RP501Rev.1 Modified EPA 906.0 Modifi.ed EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 155 of 5809 0.206 +/-1.51 pCi/g 0.368 +/-0.698 pCi/g 0.0553 +/-0.168 pCi/g 0.0897 +/-0.287 pCi/g 0.0272 +/-0.0783 pCi/g 0.051 +/-0.111 pCi/g 1.76 +/-4.39 4.00 pCi/g JXC9 09/19/16 1232 1597816 10 1.12 +/-3.81 10.0 pCi/g 0.644 +/-0.803 2.00 pCi/g KSDI 09/17/16 1640 1597795 11 1.83 +/-2.18 6.00 pCi/g AEA 09/20/16 1658 1598072 12 0.542 +/-0.648 2.00 pCi/g AEA 09/22/16 1458 1598078 13 1.05 +/-1.22 5.00 pCi/g GXRl 09/20/16 0914 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2A.R.4.2 Sample ID: 405235018 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 156 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 1596389 1596389 1596392 1596388 1596390 1596394 1597795 1597416 80.7 69.6 92.9 97.9 78.2 110 80.7 106 92.3 (15%-125%)

(15%-125%) (15%-125%) (15%-125%) (15%-125%) (15%-125%) (15%-125%) (25%-125%) (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.4 Sample ID: 405235019 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-I 6 Collector: Client Moisture: 17.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00708 +/-0.0489 0.119 Plutonium-239/240 Hh 0.0684 +/-0.0782 0.0977 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00385 +/-0.0577 0.135 Uranium-233/234 Hh 0.738 +/-0.235 0.0567 Uranium-235/236 Hh 0.128 +/-0.106 0.091 Uranium-238 Hh 0.922 +/-0.262 0.0907 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.00 +/-0.470 0.700 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.22 +l-0.456 0.349 Thorium-229 HUh 0.0288 +/-0.110 0.205 Thorium-230 Hh 0.463 +/-0.256 0.253 Thorium-232 Hh 0.679 +/-0.286 0.170 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0148 +/-0.0342 0.101 Curium-242 Hh 0.00 +/-0.108 0.161 Curium-243/244 HUh -0.00749 +/-0.0331 0.0864 Curium-245/246 HXh 0.0527 +l-0.0694 0.0527 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -9.54 +l-6.66 12.0 Rad Gamma Spec Analysis Gamma Il29, Solid "Dry Weight Corrected" lodine-129 HUh 0.152 +/-0.253 0.899 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0607 +/-0.172 0.312 Antimony-125 HUh 0.0623 +/-0.148 0.169 Bismuth-212 HUlh 0.00 +/-0.674 1.12 Bismuth-214 Hh 0.698 +/-0.153 0.102 Cesium-137 Hh 0.0561 +/-0.0482 0.0498 Cobalt-60 HUh -0.0119 +/-0.041 0.0685 HUh -0.0127 +/-0.0837 0.166 Lead-212 Hh 0.927 +/-0.113 0.0823 Lead-214 Hh 0.916 +/-0.156 0.0951 Page 157 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOI Le TPU RL *Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0806 1596227 I 0.0354 +/-0.0489 1.00 pCi/g JXH2 09/29/16 0923 1596393 2 0.0248 +/-0.0788 1.00 pCi/g 0.0386 +/-0.0578 1.00 pCi/g JXH2 09/29/16 0920 1596389 3 0.00 +/-0.270 1.00 pCi/g 0.017 +/-0.108 1.00 pCi/g 0.017 +/-0.311 1.00 pCi/g 0.00 +/-0.471 1.00 pCi/g JXH2 09/30/16 0900 1596392 4 0.116 +/-0.479 1.00 pCi/g JXH2 09/28/16 1407 1596388 5 0.0589 +/-0.111 1.00 pCi/g 0.0831 +/-0.261 1.00 pCi/g 0.0414 +/-0.297 1.00 pCi/g 0.0276 +/-0.0343 1.00 pCi/g JXH2 09/29/16 2152 1596390 6 0.00 +/-0.108 1.00 pCi/g 0.0198 +/-0.0332 1.00 pCi/g 0.00 +/-0.0698 1.00 pCi/g 5.84 +l-6.66 15.0 pCi/g JXH2 10/01/16 0000 1596394 7 0.301 +/-0.263 1.00 pCi/g MJHI 09/28/16 0723 1598618 8 0.143 +/-0.175 pCi/g MXRI 10/03/16 0821 1596247 9 0.0769 +/-0.150 pCi/g 0.517 +/-0.892 pCi/g 0.0458 +/-0.156 pCi/g 0.0218 +/-0.0483 0.100 pCi/g 0.0294 +/-0.0413 pCi/g 0.0703 +/-0.0839 pCi/g 0.0385 +/-0.123 pCi/g 0.0431 +/-0.161 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.4 Sample ID: 405235019 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.1 +/-1.32 Protactinium-231 HU!h 0.00 +/-0.750 Radium-226 Hh 0.698 +/-0.153 Radium-228 Hh 0.828 +/-0.255 Thallium-208 Hh 0.348 +/-0.075 Tin-126 HUh 0.046 +/-0.110 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.1 +/-4.31 Beta Hh 16.3 +/-2.92 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.149 +/-0.454 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Dry Weight Corrected" Tritium HUh 0.271 +/-1.95 Liquid Sein! C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.259 +/-0.665 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.451 +/-1.22 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE.EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.393 0.628 0.102 0.199 0.0507 0.100 3.87 3.15 0.927 3.37 1.13 2.17 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPAEERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 158of5809 0.152 +/-1.49 pCi/g 0.288 +/-0.771 pCi/g 0.0458 +/-0.156 pCi/g 0.0867 +/-0.258 pCi/g 0.0226 +/-0.0765 pCi/g 0.0472 +/-0.111 pCi/g 1.58 +/-5.34 4.00 pCi/g JXC9 09/19/16 1230 1597816 10 1.45 +/-3.72 10.0 pCi/g 0.402 +/-0.454 2.00 pCi/g KSDI 09/17/16 1640 1597795 11 1.63 +/-1.95 6.00 pCi/g AEA 09/20/16 1831 1598072 12 0.551 +l-0.665 2.00 pCi/g AEA 09/22/16 1544 1598078 13 1.04 +/-1.22 5.00 pCi/g GXRl 09/20/16 0931 1597416 14 Analyst Date Time Prep Batch LYTI 09/08/16 0806 1596227 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.4 Sample ID: 405235019 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uraniurn-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 159of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 90.2 (15%-125%) 1596389 77.2 (15%-125%) 1596389 78.3 (15%-125%) 1596392 35.7 (15%-125%) 1596388 112 (15%-125%) 1596390 96.6 (15%-125%) 1596394 90.2 (15%-125%) 1597795 95 (25%-125%) 1597416 90.6 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.1.4 Sample ID: 405235020 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 14.3% Parameter Qualifier Result Uncertainty Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 14.3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0243 +/-0.0668 Plutonium-2391240 HUh -0.0272 +/-0.0438 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0108 +/-0.0756 Uranium-233/234 Hh 0.602 +/-0.223 Uranium-235/236 Hh 0.0564 +/-0.0813 Uranium-238 Hh 0.847 +/-0.266 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0197 +/-0.295 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl MDC Le TPU RL Units PF DF Analyst percent LYTI 0.116 0.0295 +l-0.0669 1.00 pCi/g JXH2 0.139 0.0414 +/-0.0439 1.00 pCi/g 0.155 0.0508 +/-0.0757 1.00 pCi/g JXH2 0.113 0.0259 +/-0.249 1.00 pCi/g 0.098 0.0184 +/-0.082 1.00 pCi/g 0.151 0.0448 +/-0.308 1.00 pCi/g 0.690 0.197 +/-0.295 1.00 pCi/g JXH2 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh I.I I +/-0.464 0.328 0.0964 +/-0.485 1.00 pCi/g JXH2 Thorium-229 Hh 0.135 +/-0.172 0.239 0.0686 +/-0.173 1.00 pCi/g Thorium-230 Hh 0.928 +/-0.368 0.269 0.0838 +/-0.385 1.00 pCi/g Thorium-232 Hh 0.673 +/-0.304 0.101 0.00 +/-0.315 1.00 pCi/g Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0333 +/-0.0589 0.0892 0.0227 +/-0.0591 1.00 pCi/g JXH2 Curium-242 Hh 0.00 +/-0.103 0.153 0.00 +/-0.103 1.00 pCi/g Curium-243/244 HUh -0.00712 +/-0.0315 0.0821 0.0188 +/-0.0315 1.00 pCi/g Curium-245/246 Hh 0.0167 +/-0.047 0.0501 0.00 +/-0.047 1.00 pCi/g Liquid Sein! Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -7.36 +/-8.04 14.3 6.93 +/-8.04 15.0 pCi/g JXH2 Rad Gamma Spec Analysis Gamma I 129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0571 +/-0.291 0.835 0.281 +/-0.292 1.00 pCi/g MJHI Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0243 +/-0.209 0.421 0.195 +/-0.209 pCi/g MXRI Antimony-125 HUh 0.0107 +/-0.0847 0.173 0.077 +/-0.0849 pCi/g Bismuth-212 HU!h 0.00 +/-0.981 0.702 0.298 +/-0.986 pCi/g Bismuth-214 Hh 0.626 +/-0.161 0.134 0.0603 +/-0.164 pCi/g Cesium-137 HU!h 0.00 +/-0.0381 0.0831 0.0376 +/-0.0421 0.100 pCi/g Cobalt-60 HUh -0.0221 +/-0.0298 0.0531 0.0201 +/-0.0314 pCi/g Europium-154 HUh 0.0634 +/-0.108 0.245 0.105 +/-0.112 pCi/g Lead-212 Hh 0.961 +/-0.126 0.0847 0.0391 +/-0.136 pCi/g Lead-214 Hh 1.02 +/-0.181 0.305 0.147 +/-0.186 pCi/g Page 160 of 5809 October 4, 2016 Date Time Batch Mtd. 09/08/16 0806 1596227 I 09129116 0923 1596393 2 09/29/16 0920 1596389 3 09130116 0900 1596392 4 09/28/16 1407 1596388 5 09/29/16 2152 1596390 6 10/01/16 0101 1596394 7 09/28/16 0727 1598618 8 I 0/03/16 0853 1596247 9 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l .4 Sample ID: 405235020 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 10.7 +/-1.41 Protactinium-231 HUh 0.116 +l-0.445 Radium-226 Hh 0.626 +/-0.161 Radium-228 Hh 0.703 +/-0.292 Thallium-208 Hh 0.302 +/-0.0928 Tin-126 HUlh 0.00 +/-0.192 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 12.9 +/-3.42 Beta Hh 21.8 +/-2.67 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.30 +/-0.630 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.266 +/-1.89 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.364 +l-0.649 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.951 +/-1.17 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.546 0.896 0.134 0.258 0.0526 0.157 3.86 3.05 1.26 3.30 1.14 2.14 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 161of5809 0.215 +/-1.52 pCi/g 0.416 +/-0.449 pCi/g 0.0603 +/-0.164 pCi/g 0.113 +/-0.294 pCi/g 0.0228 +/-0.0936 pCi/g 0.0744 +/-0.192 pCi/g 1.70 +/-4.24 4.00 pCi/g JXC9 09/19/16 1416 1597816 10 1.45 +/-4.10 10.0 pCi/g 0.562 +/-0.630 2.00 pCi/g KSDl 09/17/16 1640 1597795 11 1.59 +/-1.89 6.00 pCi/g AEA 09/20/16 2004 1598072 12 0.554 +l-0.649 2.00 pCi/g AEA 09/22/16 1630 1598078 13 1.02 +/-1.17 5.00 pCi/g GXRl 09/20/16 0947 1597416 14 Analyst Date Time Prep Batch LYTl 09/08/16 0806 1596227 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.1.4 Sample ID: 405235020 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 162 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596393 74 (15%-125%) 1596389 79.3 (15%-125%) 1596389 87 (15%-125%) 1596392 69.1 (15%-125%) 1596388 94.8 (15%-125%) 1596390 103 (15%-125%) 1596394 74 (15%-125%) 1597795 91 (25%-125%) 1597416 89.9 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.3 Sample ID: 405235021 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 16.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 16.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0188 +/-0.0726 0.141 Plutonium-239/240 HUh -0.00208 +/-0.0744 0.164 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00834 +/-0.0576 0.140 Uranium-233/234 Hh 0.665 +/-0.200 0.104 Uranium-235/236 Hh 0.0262 +/-0.0515 0.0714 Uranium-238 Hh 0.606 +/-0.192 0.104 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0443 +!-0.400 0.969 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.13 +/-0.629 0.584 Thorium-229 HUh -0.0135 +/-0.117 0.270 Thorium-230 Hh 0.787 +/-0.427 0.169 Thorium-232 Hh 0.645 +/-0.398 0.310 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.000535 +/-0.0397 0.0881 Curium-242 HUh -0.0112 +/-0.0964 0.223 Curium-243/244 HUh -0.00652 +/-0.0288 0.0752 Curium-245/246 HXh 0.122 +/-0.0902 0.0459 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 Hh 9.46 +/-7.66 12.7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.057 +/-0.204 0.456 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0409 +/-0.194 0.383 Antimony-125 HUh -0.0541 +/-0.0882 0.161 Bismuth-212 HUh 0.477 +/-0.931 1.12 Bismuth-214 Hh 0.709 +/-0.165 0.105 Cesium-137 Hh 0.130 +/-0.0708 0.0737 Cobalt-60 HUh 0.0124 +/-0.0304 0.0686 Europium-154 HUh -0.0116 +/-0.0856 0.171 Lead-212 Hh 0.748 +/-0.132 0.103 Lead-214 Hh 0.805 +/-0.188 0.118 Page 163of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 I 0.0442 +/-0.0727 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.056 +/-0.0745 1.00 pCi/g 0.0417 +/-0.0577 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0298 +/-0.230 1.00 pCi/g 0.0134 +/-0.0517 1.00 pCi/g 0.0298 +/-0.218 1.00 pCi/g 0.277 +l-0.400 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.180 +/-0.653 1.00 pCi/g MXS2 09/24/16 1316 1596395 5 0.0505 +/-0.117 1.00 pCi/g 0.00 +/-0.443 1.00 pCi/g 0.0711 +/-0.410 1.00 pCi/g 0.024 +/-0.0397 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.0418 +/-0.0965 1.00 pCi/g 0.0172 +/-0.0289 1.00 pCi/g 0.00 +/-0.0915 1.00 pCi/g 6.17 +/-7.93 15.0 pCi/g MXS2 09/28/16 0520 1596402 7 0.189 +/-0.206 1.00 pCi/g MJHI 09/28/16 0845 1598620 8 0.176 +t-0.195 pCi/g MXRI 10/03/16 0857 1596249 9 0.0714 +/-0.0915 pCi/g 0.511 . +l-0.956 pCi/g 0.0462 +/-0.167 pCi/g 0.0332 +/-0.071 0.100 pCi/g 0.0284 +/-0.0309 pCi/g 0.0703 +/-0.0857 pCi/g 0.0484 +/-0.137 pCi/g 0.0537 +/-0.191 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.3 Sample ID: 405235021 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.5 +/-1.38 Protactinium-231 HUlh 0.00 +/-1.06 Radium-226 Hh 0.709 +/-0.165 Radium-228 Hh 1.02 +/-0.391 Thallium-208 Hh 0.259 +/-0.0824 Tin-126 HUlh 0.00 +/-0.106 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 8.46 +/-3.09 Beta Hh 13.9 +/-2.55 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.281 +/-0.605 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Dry Weight Corrected" Tritium Hh 2.57 +/-2.07 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.211 +/-0.697 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 1.02 +/-1.78 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.602 0.668 0.105 0.201 0.0629 0.119 3.90 3.32 1.08 3.33 1.19 3.01 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 164of5809 0.248 +/-1.50 pCi/g 0.303 +/-1.08 pCi/g 0.0462 +/-0.167 pCi/g 0.0854 +/-0.395 pCi/g 0.0282 +/-0.0832 pCi/g 0.0562 +/-0.106 pCi/g 1.70 +/-3.49 4.00 pCi/g BXFI 09/19/16 1436 1597811 10 1.58 +/-3.26 10.0 pCi/g 0.470 +/-0.607 2.00 pCi/g KSDI 09/17/16 1534 1597796 11 1.48 +/-2.07 6.00 pCi/g TXP3 09/22/16 1503 1598075 12 0.581 +/-0.698 2.00 pCi/g TXJl 09/23/16 0839 1598080 13 1.46 +/-1.78 5.00 pCi/g CXS7 09/20/16 1044 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.3 Sample ID: 405235021 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 165 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 72.2 (15%-125%) 1596396 95.3 ' (15%-125%) 1596396 76.4 (15%-125%) 1596399 93 (15%-125%) 1596395 95.9 (15%-125%) 1602285 85.5 (15%-125%) 1596402 72.2 (15%-125%) 1597796 88.3 (25%-125%) 1597412 92.5 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l .3 Sample ID: 405235022 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 19.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0154 +/-0.0356 0.106 Plutonium-239/240 HUh 0.000637 +/-0.0472 0.105 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.000625 +/-0.0463 0.103 Uranium-233/234 Hh 0.802 +/-0.240 0.0547 Uranium-235/236 Hh 0.060 +/-0.082 0.112 Uranium-238 Hh 0.948 +/-0.260 0.0547 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.227 +/-0.582 1.04 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.07 +/-0.608 0.558 Thorium-229 HUh 0.0426 +/-0.160 0.269 Thorium-230 Hh 0.770 +/-0.426 0.268 Thorium-232 Hh 0.433 +/-0.330 0.268 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0502 +/-0.0592 0.064 Curium-242 HUh -0.0223 +/-0.0986 0.257 Curium-243/244 Hh 0.0374 +/-0.0539 0.065 Curium-245/246 Hh 0.0153 +/-0.0429 0.0458 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 Hh 12.5 +/-8.08 13.3 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.163 +/-0.312 0.734 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.119 +/-0.177 0.327 Antimony-125 HUh -0.0437 +/-0.0837 0.147 Bismuth-212 HUih 0.00 +/-0.652 0.912 Bismuth-214 Hh 0.839 +/-0.166 0.0894 Cesium-137 Hh 0.645 +/-0.0922 0.0604 Cobalt-60 HUh 0.0214 +/-0.0323 0.0612 Europium-154 HUih 0.00 +/-0.0944 0.186 Lead-212 Hh 0.961 +/-0.107 0.0763 Lead-214 Hh 0.997 +/-0.168 0.245 Page 166of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 I 0.0288 +/-0.0357 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0286 +/-0.0473 1.00 pCi/g 0.028 +/-0.0464 1.00 pCi/g MXS2 09/28/16 1755 1596396 3 0.00 +/-0.278 1.00 pCi/g 0.0284 +/-0.0826 1.00 pCi/g 0.00 +/-0.308 1.00 pCi/g 0.303 +/-0.583 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.167 +/-0.630 1.00 pCi/g MXS2 09/24/16 1316 1596395 5 0.0503 +/-0.160 1.00 pCi/g 0.0502 +/-0.441 1.00 pCi/g 0.0501 +/-0.336 1.00 pCi/g 0.012 +l-0.0595 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.059 +/-0.0988 1.00 pCi/g 0.0122 +/-0.0541 1.00 pCi/g 0.00 +/-0.043 1.00 pCi/g 6.44 +/-8.50 15.0 pCi/g MXS2 09/28/16 0607 1596402 7 0.298 +/-0.321 1.00 pCi/g Milli 09/28/16 0845 1598620 8 0.153 +/-0.186 pCi/g MXRI 10/03/16 0858 1596249 9 0.0675 +/-0.086 pCi/g 0.426 +/-0.930 pCi/g 0.0407 +/-0.169 pCi/g 0.0279 +/-0.0962 0.100 pCi/g 0.0272 +/-0.0337 pCi/g 0.0836 +/-0.104 pCi/g 0.0359 +/-0.119 pCi/g 0.119 +/-0.173 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l .3 Sample ID: 405235022 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.1 +/-1.10 Protactinium-231 HUih 0.00 . +/-0.651 Radium-226 Hh 0.839 +/-0.166 Radium-228 Hh 0.593 +/-0.211 Thallium-208 Hh 0.357 +/-0.074 Tin-126 HUih 0.00 +/-0.113 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 7.10 +/-2.95 Beta Hh 16.5 +/-2.16 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.311 +/-0.441 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.14 +/-1.76 Liquid Sein! Cl4, Solid "Dry Weight Corrected" Carbon-14 Hh 0.675 +/-0.682 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.616 +/-1.86 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.381 0.623 0.0894 0.200 0.0449 0.110 3.98 2.09 0.908 3.05 1.14 3.24 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 7110B Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 167of5809 0.159 +/-1.30 pCi/g 0.290 +/-0.667 pCi/g 0.0407 +/-0.169 pCi/g 0.0909 +/-0.213 pCi/g 0.0204 +/-0.0755 pCi/g 0.0519 +/-0.114 pCi/g 1.77 +/-3.29 4.00 pCi/g BXFI 09/19/16 1436 1597811 10 0.965 +/-3.17 10.0 pCi/g 0.405 +/-0.441 2.00 pCi/g KSDI 09/17/16 1534 1597796 II 1.36 +/-1.76 6.00 pCi/g TXP3 09/22/16 1535 1598075 12 0.558 +/-0.684 2.00 pCi/g DUI 09/23/16 0950 1598080 13 1.58 +/-1.86 5.00 pCi/g CXS7 09/20/16 1116 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.1.3 Sample ID: 405235022 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l .96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 168of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 69.9 (15%-125%) 1596396 79.1 (15%-125%) 1596396 94.4 (15%-125%) 1596399 93.4 (15%-125%) 1596395 91 (15%-125%) 1602285 90 (15%-125%) 1596402 69.9 (15%-125%) 1597796 92.3 (25%-125%) 1597412 86.4 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l 1.2 Sample ID: 405235023 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 22.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 22.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.032 +/-0.0637 0.103 Plutonium-239/240 HUh -0.00748 +/-0.0331 0.0863 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00054 +/-0.040 0.0889 Uranium-233/234 Hh 0.949 +/-0.254 0.112 Uranium-235/236 Hh 0.068 +/-0.0749 0.051 Uranium-238 Hh 0.822 +/-0.235 0.0938 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0115 +/-0.4ll 0.948 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.26 +/-0.708 0.642 Thorium-229 Hh 0.0988 +/-0.227 0.360 Thorium-230 Hh 0.910 +/-0.513 0.427 Thorium-232 Hh 0.858 +/-0.494 0.395 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0279 +/-0.0547 0.152 Curium-242 Hh 0.00 +/-0.122 0.182 Curium-243/244 HUh 0.000691 +/-0.0512 0.114 Curium-245/246 Hh 0.0536 +/-0.0773 0.0932 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.13 +/-6.99 12.2 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0562 +/-0.220 0.523 Gammaspec, Gamma, Solid Dry Weight Corrected" Actinium-227 HU!h 0.00 +/-0.201 0.425 Antimony-125 HUh 0.0252 +/-0.0922 0.184 Bismuth-212 HU!h 0.00 +/-0.958 0.739 Bismuth-214 Hh 0.922 +/-0.202 0.113 Cesium-137 Hh 0.349 +/-0.105 0.0611 Cobalt-60 HUh 0.00735 +/-0.0289 0.0633 Europium-154 HUh 0.0261 +/-0.122 0.232 Lead-212 Hh 1.09 +/-0.119 0.0829 Lead-214 Hh 1.19 +/-0.182 0.108 Page 169of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 I 0.0282 +/-0.0638 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0198 +/-0.0332 1.00 pCi/g 0.0242 +/-0.0401 1.00 pCi/g MXS2 09/28/16 1755 1596396 3 0.0304 +/-0.300 1.00 pCi/g 0.00 +/-0.0758 1.00 pCi/g 0.0215 +/-0.273 1.00 pCi/g 0.259 +/-0.411 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.191 +/-0.737 1.00 pCi/g MXS2 09/24/16 1316 1596395 5 0.0825 +/-0.227 1.00 pCi/g 0.116 +/-0.532 1.00 pCi/g 0.100 +/-0.512 1.00 pCi/g 0.0506 +/-0.0547 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.123 1.00 pCi/g 0.031 +/-0.0513 1.00 pCi/g 0.0174 +/-0.0776 1.00 pCi/g 5.90 +/-6.99 15.0 pCi/g MXS2 09129116 1042 1596402 7 0.199 +/-0.221 1.00 pCi/g MJHI 09/28/16 0845 1598620 8 0.198 +/-0.222 pCi/g MXRI 10/03/16 0858 1596249 9 0.0834 +/-0.0929 pCi/g 0.323 +/-0.960 pCi/g 0.0503 +/-0.205 pCi/g 0.0271 +/-0.106 0.100 pCi/g 0.0262 +/-0.029 pCi/g 0.101 +/-0.123 pCi/g 0.0384 +/-0.132 pCi/g 0.0488 +/-0.188 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.1 l .2 Sample ID: 405235023 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.4 +/-1.34 Protactinium-231 HUih 0.00 +/-0.570 Radium-226 Hh 0.922 +/-0.202 Radium-228 Hh 0.733 +/-0.299 Thallium-208 Hh 0.325 +/-0.0773 Tin-126 HU!h 0.00 +/-0.104 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 13.3 +/-3.50 Beta Hh 20.6 +/-2.30 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh -0.402 +/-0.432 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 2.23 +/-2.08 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.518 +/-0.749 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.627 +/-1.89 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 0.483 0.721 0.113 0.245 0.0591 0.0941 3.97 2.01 0.930 3.41 1.26 3.22 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 170 of 5809 0.192 +/-1.49 pCi/g 0.331 +/-0.611 pCi/g 0.0503 +/-0.205 pCi/g 0.108 +/-0.301 pCi/g 0.0264 +/-0.0785 pCi/g 0.0443 +/-0.105 pCi/g 1.75 +/-4.32 4.00 pCi/g BXFl 09/19/16 1441 1597811 10 0.932 +/-3.73 10.0 pCi/g 0.412 +/-0.432 2.00 pCi/g KSDI 09/17/16 1534 1597796 11 1.52 +/-2.08 6.00 pCi/g TXP3 09/22/16 1608 1598075 12 0.618 +/-0.750 2.00 pCi/g TXJl 09/23/16 1102 1598080 13 1.57 +/-1.89 5.00 pCi/g CXS7 09120116 1148 1597412 14 Analyst Date Time Prep Batch LYTl 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l l .2 Sample ID: 405235023 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 171 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 68.9 (15%-125%) 1596396 87.7 (15%-125%) 1596396 92.5 (15%-125%) 1596399 85.3 (15%-125%) 1596395 88.5 (15%-125%) 1602285 64 (15%-125%) 1596402 68.9 (15%-125%) 1597796 97.8 (25%-125%) 1597412 93.5 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.2 Sample ID: 405235024 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 19.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.000735 +/-0.0545 0.121 Plutonium-239/240 HUh 0.00146 +/-0.0671 0.147 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0142 +/-0.0329 0.0975 Uranium-233/234 Hh 0.795 +/-0.258 0.101 Uranium-235/236 Hh 0.0211 +/-0.0594 0.0634 Uranium-238 Hh 0.996 +/-0.290 0.129 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.126 +/-0.360 1.04 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.35 +/-1.07 1.29 Thorium-229 HUh 0.0324 +/-0.338 0.706 Thorium-230 Hh 0.263 +l-0.465 0.705 Thorium-232 Hh 0.805 +/-0.640 0.345 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.012 +/-0.0537 0.105 Curium-242 HUh -0.0626 +/-0.119 0.366 Curium-243/244 Hh 0.0304 +/-0.0521 0.0456 Curium-245/246 Hh 0.0342 +/-0.0587 0.0514 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 3.92 +/-7.32 12.5 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.241 +/-0.272 0.254 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.183 +/-0.227 0.373 Antimony-125 HUh -0.00429 +/-0.106 0.205 Bismuth-212 HU!h 0.00 +/-0.551 1.13 Bismuth-214 Hh 0.954 +/-0.213 0.107 Cesium-137 Hh 0.779 +/-0.117 0.058 Cobalt-60 HUh O.D112 +/-0.0408 0.0813 Europium-154 HUh 0.0166 +/-0.0926 0.187 Lead-212 Hh 1.01 +/-0.125 0.0834 Lead-214 Hh 1.03 +/-0.198 0.128 Page 172 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.033 +/-0.0545 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0463 +/-0.0672 1.00 pCi/g 0.0266 +/-0.033 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0189 +/-0.296 1.00 pCi/g 0.00 +l-0.0595 1.00 pCi/g 0.0327 +/-0.341 1.00 pCi/g 0.259 +/-0.361 1.00 pCi/g MXS2 09126116 1711 1596399 4 0.415 +/-1.10 1.00 pCi/g MXS2 09/24/16 1316 1596395 5 0.180 +/-0.339 1.00 pCi/g 0.179 +/-0.468 1.00 pCi/g 0.00 +/-0.661 1.00 pCi/g 0.0301 +/-0.0537 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.105 +/-0.119 1.00 pCi/g 0.00 +/-0.0523 1.00 pCi/g 0.00 +/-0.0589 1.00 pCi/g 6.02 +/-7.37 15.0 pCi/g MXS2 09/29/16 1128 1596402 7 0.00 +/-0.294 1.00 pCi/g MJHl 09/28/16 0846 1598620 8 0.171 +/-0.243 pCi/g MXRl 10/03/16 0859 1596249 9 0.0939 +/-0.106 pCi/g 0.519 +/-0.783 pCi/g 0.0471 +/-0.217

pCi/g 0.0255 +/-0.122 0.100 pCi/g O.D35 +/-0.0411 pCi/g 0.0788 +/-0.0929 pCi/g 0.0385 +/-0.136 pCi/g 0.0588 +/-0.203 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.2 Sample ID: 405235024 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.0 +/-1.44 Protactinium-231 HU!h 0.00 +/-0.638 Radium-226 Hh 0.954 +/-0.213 Radium-228 Hh 0.912 +/-0.297 Thallium-208 Hh 0.273 +/-0.0921 Tin-126 HU!h 0.00 +/-0.131 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 9.08 +/-3.25 Beta Hh 18.8 +/-2.53 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.234 +/-0.374 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.732 +/-1.92 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 Hh 0.613 +/-0.670 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.62 +/-1.85 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.678 0.840 0.107 0.220 0.0624 0.136 3.99 2.56 0.655 3.44 1.13 3.23 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 173 of 5809 0.288 +/-1.60 pCi/g 0.389 +/-0.663 pCi/g 0.0471 +/-0.217 pCi/g 0.0957 +/-0.301 pCi/g 0.0281 +/-0.0929 pCi/g 0.0645 +/-0.131 pCi/g 1.72 +/-3.69 4.00 pCi/g BXFI 09119116 1437 1597811 10 1.19 +/-3.67 10.0 pCi/g 0.281 +/-0.376 2.00 pCi/g KSDI 09/21/16 1046 1597796 11 1.54 +/-1.92 6.00 pCi/g TXP3 09/22/16 1640 1598075 12 0.550 +/-0.672 2.00 pCi/g TXJI 09/23/16 1213 1598080 13 1.57 +/-1.85 5.00 pCi/g CXS7 09/20/16 1220 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R.2.2 Sample ID: 405235024 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOO 1 October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 174 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 67.1 (15%-125%) 1596396 69.5 (15%-125%) 1596396 92.2 (15%-125%) 1596399 81.8 (15%-125%) 1596395 45 (15%-125%) 1602285 80.8 (15%-125%) 1596402 67.1 (15%-125%) 1597796 95 (25%-125%) 1597412 91.6 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l.2 Sample ID: 405235025 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 21.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 21.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0198 +/-0.062 0.116 Plutonium-239/240 HUh -0.025 +/-0.0353 0.115 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00636 +/-0.0594 0.138 Uranium-233/234 Hh 0.747 +/-0.250 0.142 Uranium-235/236 HUh 0.0155 +/-0.0581 0.0977 Uranium-238 Hh 0.889 +/-0.271 0.142 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.103 +/-0.352 0.982 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.25 +/-0.633 0.569 Thorium-229 HUh 0.0147 +/-0.154 0.321 Thorium-230 Hh 0.922 +/-0.478 0.455 Thorium-232 Hh 0.759 +/-0.412 0.289 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0257 +/-0.0646 0.117 Curium-242 Hh 0.00 +/-0.0979 0.146 Curium-243/244 HUh -0.0323 +/-0.0641 0.162 Curium-245/246 HXh 0.0478 +/-0.063 0.0478 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 0.281 +/-6.48 11.2 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.205 +/-0.277 0.922 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0352 +/-0.297 0.569 Antimony-125 HUh 0.148 +/-0.187 0.361 Bismuth-212 HUih 0.00 +/-0.945 1.53 Bismuth-214 Hh 0.921 +/-0.232 0.165 Cesium-137 Hh 5.38 +/-0.275 0.0889 Cobalt-60 HUh 0.0029 +/-0.050 0.0979 Europium-154 HUh 0.0645 +/-0.130 0.275 Lead-212 Hh 0.953 +/-0.183 0.138 Lead-214 Hh 0.962 +/-0.226 0.191 Page 175 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0356 +/-0.0621 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0354 +/-0.0353 1.00 pCi/g 0.0451 +/-0.0594 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0407 +/-0.284 1.00 pCi/g 0.0183 +/-0.0582 1.00 pCi/g 0.0407 +/-0.315 1.00 pCi/g 0.232 +/-0.353 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.180 +/-0.661 1.00 pCi/g MXS2 09/24/16 1316 1596395 5 0.0817 +/-0.154 1.00 pCi/g 0.149 +/-0.497 1.00 pCi/g 0.0663 +/-0.427 1.00 pCi/g 0.0376 +/-0.0647 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0981 1.00 pCi/g 0.0596 +/-0.0641 1.00 pCi/g 0.00 +/-0.0633 1.00 pCi/g 5.43 +/-6.48 15.0 pCi/g MXS2 09/29/16 1215 1596402 7 0.329 +/-0.293 1.00 pCi/g MJHl 09/28/16 0846 1598620 8 0.267 +/-0.298 pCiig MXRl 10/03/16 0901 1596249 9 0.170 +/-0.199 pCi/g 0.705 +/-1.20 pCi/g 0.0747 +/-0.235 pCi/g 0.040 +/-0.359 0.100 pCi/g 0.0418 +/-0.0501 pCi/g 0.119 +/-0.133 pCi/g 0.0652 +/-0.190 pCi/g 0.0895 +/-0.230 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l .2 Sample ID: 405235025 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.1 +/-1.74 Protactinium-231 HU!h 0.00 +/-0.964 Radium-226 Hh 0.921 +/-0.232 Radium-228 Hh 1.11 +/-0.317 Thallium-208 Hh 0.267 +/-0.114 Tin-126 HU!h 0.00 +/-0.191 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 15.3 +/-4.30 Beta Hh 25.3 +/-3.08 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh 0.106 +/-0.613 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.0983 +/-1.82 Liquid Sein! CJ 4, Solid Dry Weight Corrected" Carbon-14 HUh 0.573 +/-0.730 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.6 +/-1.95 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-390, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.'5.2.3/Ga-01-R 0.733 1.13 0.165 0.323 0.0789 0.194 3.92 2.50 1.11 3.39 1.23 3.46 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 176 of 5809 0.301 +/-1.89 pCi/g 0.526 +/-0.977 pCi/g 0.0747 +/-0.235 pCi/g 0.143 +/-0.322 pCi/g 0.0355 +/-0.114 pCi/g 0.0929 +/-0.197 pCi/g 1.59 +/-5.22 4.00 pCi/g BXFI 09/19/16 1436 1597811 10 1.13 +/-4.79 10.0 pCi/g 0.506 +/-0.614 2.00 pCi/g KSDI 09119116 1154 1597796 II 1.51 +/-1.82 6.00 pCi/g TXP3 09/22/16 1713 1598075 12 0.601 +/-0.732 2.00 pCi/g TXJI 09/23/16 1324 1598080 13 1.68 +/-1.95 5.00 pCi/g CXS7 09/20/16 1324 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2B.R. l .2 Sample ID: 405235025 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOO 1 October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Arn241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 177 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 75.4 (15%-125%) 1596396 71.5 (15%-125%) 1596396 85.5 (15%-125%) 1596399 78.6 (15%-125%) 1596395 96.9 (15%-125%) 1602285 92.9 (15%-125%) 1596402 75.4 (15%-125%) 1597796 103 (25%-125%) 1597412 86.4 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2C.R. l .3 Sample ID: 405235026 Matrix: Soil Collect Date: 08-DEC-l 5 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 16.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 16.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.000592 +/-0.0439 0.0976 Plutonium-239/240 Hh 0.0224 +/-0.0514 0.0815 ASP Uranium Isotopic, Solid Dry Weight Corrected" Uranium-232 HUh -0.0262 +/-0.0329 0.110 Uranium-233/234 Hh 0.633 +/-0.216 0.132 Uranium-235/236 Hh 0.0314 +/-0.0618 0.0856 Uranium-238 Hh 0.530 +/-0.195 0.0854 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00244 +/-0.181 0.403 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.69 +/-0.824 0.601 Thorium-229 Hh 0.194 +/-0.280 0.338 Thorium-230 Hh 0.793 +/-0.501 0.429 Thorium-232 Hh 0.824 +/-0.497 0.336 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0129 +/-0.0441 0.0818 Curium-242 Hh 0.00 +/-0.0871 0.130 Curium-243/244 HUh -0.00302 +/-0.0261 0.0604 Curium-245/246 Hh 0.0675 +/-0.0688 0.068 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 Hh 8.50 +/-6.75 11.2 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0231 +/-0.175 0.400 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.00958 +/-0.210 0.385 Antimony-125 HUh -0.00334 +/-0.0702 0.141 Bismuth-212 HUih 0.00 +/-0.670 1.23 Bismuth-214 Hh 0.660 +/-0.159 0.0941 Cesium-137 Hh 0.153 +/-0.0572 0.0499 Cobalt-60 HUh -0.0265 +/-0.0292 0.0494 Europium-154 HUh 0.0305 +/-0.0757 0.171 Lead-212 Hh 0.920 +/-0.119 0.0844 Lead-214 Hh 0.847 +/-0.170 0.107 Page 178 of5809 Report Date: October4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0266 +/-0.0439 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0187 +/-0.0515 1.00 pCi/g 0.0346 +/-0.033 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0391 +/-0.242 1.00 pCi/g 0.016 +/-0.062 1.00 pCi/g 0.016 +/-0.215 1.00 pCi/g 0.110 +/-0.181 1.00 pCi/g MXS2 09/29/16 1405 1596399 4 0.160 +/-0.871 1.00 pCi/g MXS2 09/24/16 1317 1596395 5 0.0632 +/-0.282 1.00 pCi/g 0.109 +/-0.517 1.00 pCi/g 0.0629 +/-0.515 1.00 pCi/g 0.0223 +/-0.0441 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0872 1.00 pCi/g 0.0113 +/-0.0261 1.00 pCi/g 0.0127 +/-0.0693 1.00 pCi/g 5.43 +/-6.98 15.0 pCi/g MXS2 09/28/16 0915 1596402 7 0.159 +/-0.176 1.00 pCi/g MJHl 09/28/16 0928 1598620 8 0.178 +/-0.210 pCi/g MXRl 10/03/16 0901 1596249 9 . 0.0627 +/-0.0702 pCi/g 0.574 +/-1.17 pCi/g 0.0416 +/-0.168 pCi/g 0.0218 +/-0.0585 0.100 pCi/g 0.0195 +/-0.0316 pCi/g 0.072 +/-0.077 pCi/g 0.0393 +/-0.140 pCi/g 0.0489 +/-0.183 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2C.R. l .3 Sample ID: 405235026 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.5 +/-1.28 Protactinium-231 HU!h 0.00 +/-0.661

Radium-226 Hh 0.660 +/-0.159 Radium-228 Hh 0.966 +/-0.306 Thallium-208 Hh 0.283 +/-0.0683 Tin-126 HU!h 0.00 +/-0.108 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 15.3 +/-4.06 Beta Hh 17.4 +/-2.92 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.601 +/-0.458 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.600 +/-1.85 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.510 +/-0.695 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.392 +/-1.78 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.316 0.589 0.0941 0.196 0.0506 0.101 3.94 3.43 1.00 3.34 1.17 3.10 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 7110B Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 179 of 5809 0.111 +/-1.69 pCi/g 0.266 +/-0.681 pCi/g 0.0416 +/-0.168 pCi/g 0.085 +/-0.335 pCi/g 0.0225 +/-0.0721 pCi/g 0.0476 +/-0.110 pCi/g 1.65 +/-5.04 4.00 pCi/g BXFI 09119116 1441 1597811 10 1.61 +/-3.87 10.0 pCi/g 0.450 +/-0.458 2.00 pCi/g KSDI 09/17/16 1533 1597796 11 1.49 +/-1.85 6.00 pCi/g TXP3 09/22/16 1745 1598075 12 0.573 +/-0.696 2.00 pCi/g TIU! 09/23/16 1435 1598080 13 1.51 +/-1.78 5.00 pCi/g CXS7 09/20/16 1252 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2C.R. l .3 Sample ID: 405235026 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l .96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 180 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 83.6 (15%-125%) 1596396 85.1 (15%-125%) 1596396 93.5 (15%-125%) 1596399 86.3 (15%-125%) 1596395 92 (15%-125%) 1602285 91.4 (15%-125%) 1596402 83.6 (15%-125%) 1597796 97.8 (25%-125%) 1597412 88.5 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2C.R. l .4 Sample ID: 405235027 Matrix: Soil Collect Date: 08-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 18.2% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 18.2 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00984 +/-0.0445 0.112 Plutonium-239/240 HUh 0.00403 +/-0.0421 0.0878 ASP Uranium Isotopic, Solid Dry Weight Corrected" Uranium-232 HUh -0.0321 +/-0.0366 0.125 Uranium-233/234 Hh 0.982 +/-0.280 0.0966 Uranium-235/236 Hh 0.0558 +/-0.0803 0.0969 Uranium-238 Hh 0.968 +/-0.280 0.133 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0716 +/-0.507 1.02 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.721 +/-0.573 0.661 Thorium-229 Hh 0.164 +/-0.261 0.361 Thorium-230 Hh 0.911 +/-0.495 0.195 Thorium-232 Hh 1.10 +/-0.540 0.195 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.024 +/-0.0424 0.0642 Curium-242 Hh 0.00 +/-0.0737 0.110 Curium-243/244 HUh -0.00768 +/-0.0232 0.0651 Curium-245/246 Hh 0.0211 +/-0.0415 0.0576 Liquid Sein/ Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 4.77 +l-6.96. 11.8 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0423 +/-0.247 0.525 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0503 +/-0.233 0.469 Antimony-125 HUh -0.0387 +/-0.108 0.200 Bismuth-212 HU!h 0.00 +/-1.03 1.49 Bismuth-214 Hh 0.854 +/-0.191 0.114 Cesium-137 HUih 0.00 +/-0.0442 0.0921 Cobalt-60 HUh -0.0217 +/-0.0423 0.0754 Europium-154 HUh 0.103 +/-0.106 0.254 Lead-212 Hh 0.963 +/-0.133 0.103 Lead-214 Hh 0.786 +/-0.187 0.126 Page 181of5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0343 +/-0.0445 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0223 +/-0.0421 1.00 pCi/g 0.0401 +/-0.0367 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0181 +/-0.330 1.00 pCi/g 0.0181 +/-0.081 1.00 pCi/g 0.0362 +/-0.329 1.00 pCi/g 0.241 +/-0.507 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.201 +/-0.586 1.00 pCi/g MXS2 09/24/16 1317 1596395 5 0.0828 +/-0.263 1.00 pCi/g 0.00 +/-0.517 1.00 pCi/g 0.00 +/-0.569 1.00 pCi/g 0.0163 +/-0.0424 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0738 1.00 pCi/g 0.0166 +/-0.0232 1.00 pCi/g 0.0108 +/-0.0416 1.00 pCi/g 5.71 +/-7.03 15.0 pCi/g MXS2 09/28/16 1002 1596402 7 0.214 +/-0.248 1.00 pCi/g MJHl 09/28/16 0928 1598620 8 0.217 +/-0.234 pCi/g MXRl 10/03/16 0908 1596249 9 0.0895 +/-0.110 pCi/g 0.684 +/-1.22 pCi/g 0.0497 +/-0.194 pCi/g 0.0417 +/-0.0515 0.100 pCi/g 0.0308 +/-0.0434 pCi/g 0.109 +/-0.116 pCi/g 0.0479 +/-0.143 pCi/g 0.0569 +/-0.189 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2C.R.1.4 Sample ID: 405235027 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.0 +/-1.59 Protactinium-231 HUih

0.00 +/-0.974 Radium-226 Hh 0.854 +/-0.191 Radium-228 Hh 0.865 +/-0.383 Thallium-208 Hh 0.357 +/-0.0944 Tin-126 HUlh 0.00 +/-0.126 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 12.2 +/-4.79 Beta Hh 24.0 +/-3.81 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.0791 +/-0.605 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.19 +/-1.90 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.528 +/-0.674 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.141 +/-1.93 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-OI Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.769 0.862 0.114 0.270 0.0644 0.158 3.89 2.79 1.16 3.29 1.13 3.33 2 3 4 5 6 7 8 9 JO II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 182 of 5809 0.322 +/-1.75 pCi/g 0.395 +/-0.995 pCi/g 0.0497 +/-0.194 pCi/g 0.117 +/-0.385 pCi/g 0.0283 +/-0.0956 pCi/g 0.0746 +/-0.127 pCi/g 1.29 +/-5.36 4.00 pCi/g BXFI 09/19/16 1441 1597811 JO 1.20 +/-5.20 JO.O pCi/g 0.517 +/-0.605 2.00 pCi/g KSDI 09/17/16 1533 1597796 II 1.47 +/-1.90 6.00 pCi/g TXP3 09/22/16 1818 1598075 12 0.555 +/-0.675 2.00 pCi/g TXJI 09/23/16 1547 1598080 13 1.62 +/-1.94 5.00 pCi/g CXS7 09/20/16 1428 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.2C.R. l .4 Sample ID: 405235027 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 183 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 78.8 (15%-125%) 1596396 70.7 (15%-125%) 1596396 95.1 (15%-125%) 1596399 68.4 (15%-125%) 1596395 88.9 (15%-125%) 1602285 105 (15%-125%) 1596402 78.8 (15%-125%) 1597796 100 (25%-125%) 1597412 86.7 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.ARI.3 Sample ID: 405235028 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 22.7% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 22.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00618 +/-0.0273 0.0713 Plutonium-239/240 Hh 0.0292 +/-0.0516 0.0781 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0116 +/-0.0349 0.0981 Uranium-233/234 Hh 0.999 +/-0.242 0.0907 Uranium-235/236 Hh 0.0453 +/-0.0671 . 0.0982 Uranium-238 Hh 0.880 +/-0.228 0.0907 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0874 +/-0.298 0.830 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.22 +/-0.837 0.925 Thorium-229 HUh 0.0633 +/-0.237 0.399 Thorium-230 Hh 1.23 +/-0.653 0.398 Thorium-232 Hh 1.72 +/-0.763 0.397 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0504 +/-0.0708 0.110 Curium-242 Hh 0.00 +/-0.0981 0.146 Curium-243/244 HUh 0.0139 +/-0.0474 0.0879 Curium-245/246 HXh 0.090 +/-0.0781 0.045 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 Hh 11.2 +/-6.89 11.3 Rad Gamma Spec Analysis Gamma I 129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.211 +/-0.243 0.342 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.136 +/-0.253 0.394 Antimony-125 HUh 0.0174 +/-0.113 0.226 Bismuth-212 Hh 1.84 +/-0.908 0.822 Bismuth-214 Hh 1.04 +/-0.178 0.117 Cesium-137 Hh 0.132 +/-0.0782 0.0728 Cobalt-60 HUh -0.00215 +/-0.0369 0.0767 Europium-154 HUh 0.0403 +/-0.114 0.250 Lead-212 Hh 1.19 +/-0.139 0.102 Lead-214 Hh 1.12 +/-0.163 0.364 Page 184 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYT! 09/08/16 0812 1596228 1 0.0163 +/-0.0274 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0199 +/-0.0517 1.00 pCi/g 0.025 +/-0.035 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0231 +/-0.293 1.00 pCi/g 0.0267 +/-0.0676 1.00 pCi/g 0.0231 +/-0.270 1.00 pCi/g 0.196 +/-0.298 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.294 +/-0.865 1.00 pCi/g MXS2 09/24/16 1317 1596395 5 0.0747 +/-0.238 1.00 pCi/g 0.0745 +/-0.686 1.00 pCi/g 0.0743 +/-0.817 1.00 pCi/g 0.0353 +/-0.0711 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0983 1.00 pCi/g 0.0239 +/-0.0475 1.00 pCi/g 0.00 +/-0.079 1.00 pCi/g 5.48 +/-7.26 15.0 pCi/g MXS2 09/28/16 1049 1596402 7 0.108 +/-0.262 1.00 pCi/g MJHl 09/28/16 0929 1598620 8 0.178 +/-0.261 pCi/g MXRl 10/03/16 0908 1S96249 9 0.102 +/-0.113 pCi/g 0.350 +/-0.913 pCi/g 0.0509 +/-0.184 pCi/g 0.0319 +/-0.0784 0.100 pCi/g 0.0311 +/-0.0369 pCi/g 0.106 +/-0.116 pCi/g 0.0471 +/-0.152 pCi/g 0.176 +/-0.169 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.ARl.3 Sample ID: 405235028 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.6 +/-1.63 Protactinium-231 HUih 0.00 +/-0.745 Radium-226 Hh 1.04 +/-0.178 Radium-228 Hh 0.827 +/-0.270 Thallium-208 Hh 0.355 +/-0.0778 Tin-126 HUh 0.0334 +/-0.163 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.1 +/-3.58 Beta Hh 47.8 +/-3.72 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.331 +/-0.532 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.54 +/-1.80 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.394 +/-0.7IO Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.604 +/-1.89 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.578 0.746 0.117 0.270 0.0518 0.157 3.89 2.57 0.931 3.51 1.20 3.24 2 3 4 5 6 7 8 9 IO II I2 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 185of5809 0.223 +/-1.80 pCi/g 0.335 +/-0.753 pCi/g 0.0509 +/-0.184 pCi/g 0.116 +/-0.273 pCi/g 0.0219 +/-0.0792 pCi/g 0.0737 +/-0.163 pCi/g 1.69 +/-4.41 4.00 pCi/g BXFI 09119116 1437 1597811 10 1.19 +/-7.56 10.0 pCi/g 0.400 +/-0.535 2.00 pCi/g KSDI 09/17/16 1533 1597796 11 1.57 +/-1.80 6.00 pCi/g TXP3 09/22/I6 I85I 1598075 12 0.588 +/-0.711 2.00 pCi/g TXJI 09/23/16 1658 1598080 13 1.57 +/-1.90 5.00 pCi/g CXS7 09/20/I 6 1356 I597412 14 Analyst Date Time Prep Batch LYTI . 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.ARl.3 Sample ID: 405235028 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl

October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 186 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 82 (15%-125%) 1596396 94.7 (15%-125%) 1596396 87.3 (15%-125%) 1596399 87.3 (15%-125%) 1596395 80.9 (15%-125%) 1602285 86.1 (15%-125%) 1596402 82 (15%-125%) 1597796 88.3 (25%-125%) 1597412 88 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.B.R.l.3 Sample ID: 405235029 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.3% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 19.3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0475 +/-0.0602 0.0748 Plutonium-239/240 Hh 0.0204 +/-0.0468 0.0743 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00507 +/-0.0708 0.150 Uranium-233/234 Hh 0.716 +/-0.215 0.112 Uranium-235/236 Hh 0.0442 +/-0.0637 0.0768 Uranium-238 Hh 0.635 +/-0.201 0.0766 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.079 +/-0.334 0.890 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.924 +/-0.671 0.558 Thorium-229 HUh 0.0608 +/-0.228 0.383 Thorium-230 Hh 0.762 +/-0.551 0.590 Thorium-232 Hh 1.06 +/-0.608 0.486 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.00423 +/-0.0482 0.102 Curium-242 Hh 0.00 +/-0.0988 0.147 Curium-243/244 HUh -0.0193 +/-0.0312 0.0993 Curium-245/246 Hh 0.0151 +/-0.0425 0.0453 Liquid Scint Pu24 J, Solid "Dry Weight Corrected" Plutonium-241 HUh 4.01 +/-7.21 12.3 Rad Gamma Spec Analysis Gamma ll 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0502 +/-0.218 0.521 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.175 +/-0.417 0.478 Antimony-125 HUh -0.0671 +/-0.122 0.215 Bismuth-212 Hh 1.03 +/-0.964 0.907 Bismuth-214 Hh 0.758 +/-0.185 0.144 Cesium-137 Hh 0.311 +/-0.0801 0.0706 Cobalt-60 HUh 0.00176 +/-0.0368 0.0743 Europium-154 HU!h 0.00 +/-0.146 0.254 Lead-212 Hh 1.07 +/-0.131 0.098 Lead-214 Hh 1.16 +/-0.194 0.327 Page 187 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU

RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0171 +l-0.0605 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.017 +/-0.0469 1.00 pCi/g 0.0576 +/-0.0709 1.00 pCi/g MXS2 09/24/16 1319 1596396 3 0.0321 +/-0.245 1.00 pCi/g 0.0144 +/-0.0641 1.00 pCi/g 0.0143 +/-0.226 1.00 pCi/g 0.198 +/-0.334 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.117 +/-0.691 1.00 pCi/g MXS2 09/24/16 1317 1596395 5 0.0717 +/-0.228 1.00 pCi/g 0.175 +/-0.566 1.00 pCi/g 0.124 +/-0.635 1.00 pCi/g 0.0314 +/-0.0482 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +l-0.099 1.00 pCi/g 0.0295 +/-0.0312 1.00 pCi/g 0.00 +/-0.0425 1.00 pCi/g 5.94 +/-7.26 15.0 pCi/g MXS2 09/28/16 1135 1596402 7 0.165 +/-0.219 1.00 pCi/g MJHl 09/28/16 0929 1598620 8 0.223 pCi/g MXRl 10/03/16 0908 1596249 9 0.0983 +/-0.126 pCi/g 0.402 +(-0.965 pCi/g 0.0654 +/-0.188 pCi/g 0.0315 +/-0.0812 0.100 pCi/g 0.0311 +/-0.0368 pCi/g 0.111 +/-0.167 pCi/g 0.0458 +/-0.143 pCi/g 0.158 +/-0.200 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.B.R.l.3 Sample ID: 405235029 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.2 +l-1.49 Protactinium-231 HU!h 0.00 +/-0.864 Radium-226 Hh 0.758 +/-0.185 Radium-228 Hh 0.859 +/-0.295 Thallium-208 Hh 0.323 +/-0.0806 Tin-126 HU!h 0.00 +/-0.194 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 9.55 +/-3.39 Beta Hh 17.6 +/-2.35 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh 0.278 +/-0.515 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.23 +/-1.94 Liquid Sein/ Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.285 +/-0.621 Liquid Sein/ Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.373 +/-1.92 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-OI Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.502 0.886 0.144 0.274 0.0667 0.137 3.99 2.24 0.919 3.37 1.06 3.29 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 188of5809 0.196 +/-1.66 pCi/g 0.411 +/-0.880 pCi/g 0.0654 +/-0.188 pCi/g 0.121 +/-0.298 pCi/g 0.030 +/-0.0818 pCi/g 0.065 +/-0.194 pCi/g 1.71 +/-3.87 4.00 pCi/g BXF! 09/19/16 1436 1597811 10 1.03 +/-3.37 10.0 pCi/g 0.391 +/-0.518 2.00 pCi/g KSD! 09/17/16 1533 1597796 11 1.50 +/-1.94 6.00 pCi/g TXP3 09/22/16 1923 1598075 12 0.516 +/-0.622 2.00 pCi/g DU! 09/23/16 1809 1598080 13 1.60 +/-1.92 5.00 pCi/g CXS7 09/20/16 1532 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.B.R. l.3 Sample ID: 405235029 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 189 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 78 (15%-125%) 1596396 103 (15%-125%) 1596396 99.4 (15%-125%) 1596399 82 (15%-125%) 1596395 88 (15%-125%) 1602285 86.9 (15%-125%) 1596402 78 (15%-125%) 1597796 93.7 (25%-125%) 1597412 88.4 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3A.R.2.3 Sample ID: 405235030 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 23.9% Parameter Qualifier Result Uncertainty MDC , Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 23.9 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0227 +/-0.0625 0.108 Plutonium-239/240 HUh 0.0183 +/-0.0626 0.116 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00403 +/-0.0422 0.088 Uranium-233/234 Hh 0.972 +/-0.233 0.0429 Uranium-235/236 HUh 0.0109 +/-0.0409 0.0687 Uranium-238 Hh 0.830 +/-0.218 0.0942 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.164 +/-0.405 1.21 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.13 +/-0.680 0.556 Thorium-229 HUh 0.00274 +/-0.203 0.451 Thorium-230 Hh 0.976 +/-0.539 0.417 Thorium-232 Hh 1.21 +/-0.584 0.327 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0222 +/-0.0436 0.0604 Curium-242 Hh 0.00 +/-0.0943 0.140 Curium-243/244 HUh -0.0154 +/-0.0291 0.0899 Curium-245/246 Hh 0.0254 +/-0.0498 0.0691 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 1.02 +/-6.76 11.6 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0659 +/-0.232 0.443 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.158 +/-0.210 0.431 Antimony-125 HUh 0.0273 +/-0.0935 0.186 Bismuth-212 HU!h 0.00 +/-1.02 1.45 Bismuth-214 Hh 0.800 +/-0.189 0.129 Cesium-137 Hh 0.0731 +/-0.0455 0.0548 Cobalt-60 HUh 0.0237 +/-0.036 0,0822 Europium-154 HUh -0.0571 +/-0.0973 0.175 Lead-212 Hh 1.25 +/-0.128 0.089 Lead-214 Hh 0,958 +/-0.163 0.119 Page 190of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0276 +/-0.0626 1.00 pCi/g MXS2 09/24/16 2051 1596400 2 0.0316 +/-0.0627 1.00 pCi/g 0.0224 +/-0.0422 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.00 +/-0.281 1.00 pCi/g 0.0129 +/-0.0409 1.00 pCi/g 0.0257 +/-0.256 1.00 pCi/g 0.312 +/-0.406 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.140 +/-0.705 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.123 +/-0.203 1.00 pCi/g 0.106 +/-0.560 1.00 pCi/g 0.0611 +/-0.613 1.00 pCi/g 0.0113 +/-0.0437 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0944 1.00 pCi/g 0.0257 +/-0.0292 1.00 pCi/g 0.0129 +/-0.0499 1.00 pCi/g 5.65 +/-6.77 15.0 pCi/g MXS2 09/28/16 1222 1596402 7 0.124 +/-0.234 1.00 pCi/g MJHl 09/28/16 0930 1598620 8 0.200 +/-0.223 pCi/g MXRl I0/03il6 0909 1596249 9 0.0838 +/-0,0943 pCi/g 0.672 +/-1.20 pCi/g 0.0581 +/-0.192 pCi/g 0.0236 +/-0.0456 0.100 pCi/g 0.035 +/-0.0376 pCi/g 0.0713 +/-0.101 pCi/g 0.0412 +/-0.144 pCi/g 0.0539 +/-0.168 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3A.R.2.3 Sample ID: 405235030 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.1 +/-1.51 Protactinium-231 HU!h 0.00 +/-0.768 Radium-226 Hh 0.800 +/-0.189 Radium-228 Hh 0.975 +/-0.282 Thallium-208 Hh 0.442 +/-0.0829 Tin-126 HU!h 0.00 +/-0.123 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.9 +/-3.89 Beta Hh 21.5 +/-3.01 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.253 +/-0.522 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.263 +/-1.93 Liquid Scint C/4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.092 +/-0.760 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.298 +/-2.09 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.378 0.724 0.129 0.216 0.0427 0.117 3.93 3.28 1.07 3.56 1.30 3.60 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 191of5809 0.134 +/-1.71 pCi/g 0.330 +/-0.794 pCi/g 0.0581 +/-0.192 pCi/g 0.0922 +/-0.286 pCi/g O.oJ8 +/-0.085 pCi/g 0.0555 +/-0.125 pCi/g 1.65 +/-4.78 4.00 pCi/g BXFl 09/19/16 1437 1597811 10 1.54 +/-4.37 10.0 pCi/g 0.470 +/-0.522 2.00 pCi/g KSDI 09/17/16 1533 1597796 11 1.59 +/-1.93 6.00 pCi/g TXP3 09/22/16 1956 1598075 12 0.636 +/-0.760 2.00 pCi/g TXJI 09/23/16 1920 1598080 13 1.75 +/-2.09 5.00 pCi/g CXS7 09/20/16 1500 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3A.R.2.3 Sample ID: 405235030 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 192of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch 11> Recovery% Acceptable Limits 1596400 80.8 (15%-125%) 1596396 98 (15%-125%) 1596396 82.4 (15%-125%) 1596399 69.6 (15%-125%) 1596395 101 (15%-125%) 1602285 84.3 (15%-125%) 1596402 80.8 (15%-125%) 1597796 100 (25%-125%) 1597412 87.3 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.BR19.2 SamI?le ID: 405235031 Matrix: Soil Collect Date: 26-NOV-15 Receive Date: 06-SEP-l 6 Collectbr: Client Moisture: 22.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 22.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0083 +/-0.0367 0.0958 Plutonium-239/240 HUh -0.00825 +/-0.0365 0.0951 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0215 +/-0.0886 0.192 Uranium-233/234 Hh 0.823 +/-0.220 0.0967 Uranium-235/236 Hh 0.0295 +l-0.0505 0.0442 Uranium-238 Hh 0.790 +/-0.216 0.103 Alphaspec Np23 7, Solid "Dry Weigh{ Corrected" Neptunium-237 HUh -0.0742 +/-0.314 0.837 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.18 +/-0.756 0.883 Thorium-229 HUh 0.0846 +/-0.233 0.404 Thorium-230 Hh 0.841 +/-0.485 0.316 Thorium-232 Hh 0.889 +/-0.502 0.364 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0553 +/-0.0632 0.0789 Curium-242 HUh -0.0227 +/-0.100 0.262 Curium-243/244 HUh 0.00683 +/-0.0379 0.0727 Curium-245/246 HXh 0.0591 +/-0.0651 0.0443 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 3.98 +/-6.37 10.8 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" lodine-129 HUh 0.00 +/-0.263 0.578 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0527 +/-0.229 0.452 Antimony-125 HUh -0.0864 +/-0.112 0.193 Bismuth-212 Hh 0.824 +/-0.649 0.797 Bismuth-214 Hh 0.983 +/-0.202 0.121 Cesium-137 Hh 0.205 +/-0.067 0.0539 Cobalt-60 HUh -0.0189 +/-0.0354 0.0648 Europium-154 HUh 0.0583 +/-0.118 0.257 Lead-212 Hh 1.16 +/-0.140 0.0934 Lead-214 Hh 1.07 +/-0.243 0.138 Page 193of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0812 1596228 1 0.0219 +/-0.0368 1.00 pCi/g MXS2 09/24/16 2051 1596400 2 0.0218 +/-0.0365 1.00 pCi/g 0.0761 +/-0.0886 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.0264 +/-0.257 1.00 pCi/g 0.00 +/-0.0507 1.00 pCi/g 0.0295 +/-0.251 1.00 pCi/g 0.186 +/-0.314 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.308 +/-0.779 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.103 +/-0.233 1.00 pCi/g 0.0592 +/-0.502 1.00 pCi/g 0.0834 +/-0.520 1.00 pCi/g 0.0201 +/-0.0636 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.0601 +/-0.101 1.00 pCi/g 0.0167 +/-0.038 1.00 pCi/g 0.00 +/-0.0655 1.00 pCi/g 5.24 +/-6.43 15.0 pCi/g MXS2 09/28/16 1309 1596402 7 0.230 +/-0.00 1.00 pCi/g MJHI 09/28/16 1017 1598620 8 0.209 +/-0.230 pCi/g MXRI 10/03/16 0909 1596249 9 0.0863 +/-0.118 pCi/g 0.342 +/-0.650 pCi/g 0.0533 +/-0.206 pCi/g 0.0227 +/-0.0676 0.100 pCi/g 0.0256 +/-0.0364 pCi/g 0.111 +/-0.121 pCi/g 0.0431 +/-0.153 pCi/g 0.0631 +/-0.247 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.BR19.2 Sample ID: 405235031 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.0 +/-1.54 Protactinium"23 I HUh 0.0906 +/-0.528 Radium-226 Hh 0.983 +/-0.202 Radium-228 Hh 0.898 +/-0.342 Thallium-208 Hh 0.275 +/-0.0953 Tin-126 HUlh 0.00 +/-0.193 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 15.8 +/-5.45 Beta Hh 16.6 +/-3.36 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.0157 +/-0.569 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 2.12 +/-2.18 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.478 +/-0.721 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.361 +/-2.05 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.749 0.926 0.121 0.273 0.0655 0.178 3.91 2.69 1.07 3.63 1.22 3.51 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 194of5809 0.313 +/-1.70 pCi/g 0.428 +/-0.530 pCi/g 0.0533 +/-0.206 pCi/g 0.119 +/-0.345 pCi/g 0.029 +/-0.096 pCi/g 0.0846 +/-0.194 pCi/g 1.28 +/-6.24 4.00 pCi/g BXF! 09/19/16 1441 159781 I 10 1.14 +/-4.17 10.0 pCi/g 0.475 +l-0.569 2.00 pCi/g KSDI 09/17/16 1533 1597796 11 1.62 +/-2.19 6.00 pCi/g TXP3 09/22/16 2028 1598075 12 0.595 +/-0.722 2.00 pCi/g TXJI 09/23/16 2032 1598080 13 1.71 +/-2.05 5.00 pCi/g CXS7 09/20/16 1604 1597412 14 Analyst Date Time Prep Batch LYT! 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.BR19.2 Sample ID: 405235031 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 195of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 84.I (15%-125%) 1596396 94.6 (15%-125%) 1596396 94.2 (15%-125%) 1596399 88.4 (15%-125%) 1596395 109 (15%-125%) 1602285 82.4 (15%-125%) 1596402 84.1 (15%-125%) 1597796 95 (25%-125%) 1597412 87.7 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com

Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.3.3 Sample ID: 405235032 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 20.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 20.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 Hh 0.0429 +/-0.0759 0.115 Plutonium-239/240 HUh -0.0314 +/-0.0443 0.145 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0376 +/-0.0865 0.157 Uranium-233/234 Hh 0.898 +/-0.292 0.143 Uranium-235/236 Hh 0.0885 +/-0.104 0.113 Uranium-238 Hh 0.616 +/-0.244 0.143 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0581 +/-0.325 0.821 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.53 +/-0.773 0.493 Thorium-229 Hh 0.105 +/-0.240 0.381 Thorium-230 Hh 0.601 +/-0.428 0.329 Thorium-232 Hh 1.16 +/-0.570 0.205 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0257 +/-0.0323 0.108 Curium-242 Hh 0.00 +/-0.100 0.149 Curium-243/244 HUh -0.00978 +/-0.0295 0.083 Curium-245/246 Hh 0.0306 +/-0.0524 0.0458 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 Hh 6.06 +/-7.07 11.9 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0975 +/-0.327 0.752 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0296 +/-0.282 0.548 Antimony-125 HUh -0.0866 +/-0.125 0.218 Bismuth-212 Hh 1.88 +/-1.03 1.12 Bismuth-214 Hh 0.958 +/-0.189 0.144 Cesium-137 Hh 0.206 +/-0.113 0.094 Cobalt-60 HUh 0.00618 +/-0.0448 0.0942 Europium-154 HUh -0.0346 +/-0.178 0.293 Lead-212 Hh 1.19 +/-0.153 0.0997 Lead-214 Hh 0.866 +/-0.237 0.141 Page 196 of 5809 Report Date: October 4, 2016 Project: MJWCOOI 15 Client ID: MJWCOOI Le TPU RL Units PF DF Analyst *Date Time Batch Mtd. percent LYT! 09/08/16 0812 1596228 1 0.0293 +/-0.0762 1.00 pCi/g MXS2 09/24116 2051 1596400 2 0.0444 +/-0.0444 1.00 pCi/g 0.0598 +/-0.0867 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.0365 +/-0.336 1.00 pCi/g 0.0211 +/-0.106 1.00 pCi/g 0.0365 +/-0.270 1.00 pCi/g 0.169 +/-0.326 1.00 pCi/g MXS2 09/26/16 1709 1596399 4 0.107 +/-0.814 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.0873 +/-0.241 1.00 pCi/g 0.0616 +/-0.438 1.00 pCi/g 0.00 +/-0.600 1.00 pCi/g 0.0339 +/-0.0323 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.100 1.00 pCi/g 0.0211 +/-0.0296 1.00 pCi/g 0.00 +/-0.0525 1.00 pCi/g 5.76 +/-7.19 15.0 pCi/g MXS2 09/28/16 1356 1596402 7 0.298 +/-0.331 1.00 pCi/g MJHI 09/28/16 1018 1598620 8 0.255 +/-0.282 pCi/g MxRl 10/03/16 0910 1596249 9 0.0974 +/-0.131 pCi/g 0.495 +/-1.04 pCi/g 0.0635 +/-0.193 pCi/g 0.0422 +/-0.113 0.100 pCi/g 0.0391 +/-0.0448 pCi/g 0.126 +/-0.179 pCi/g 0.0459 +/-0.165 pCi/g 0.0636 +/-0.240 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.3.3 Sample ID: 405235032 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.9 +/-1.78 Protactinium-231 HU!h 0.00 +/-0.887 Radium-226 Hh 0.958 +/-0.189 Radium-228 Hh 1.06 +/-0.350 Thallium-208 Hh 0.279 +/-0.109 Tin-126 HU!h 0.00 +/-0.114 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 10.2 +/-3.66 Beta Hh 18.7 +/-2.95 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.266 +/-0.285 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.33 +/-2.09 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.471 +/-0.673 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.182 +/-1.82 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified . DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.766 0.912 0.144 0.270 0.0719 0.122 3.99 3.23 0.661 3.62 1.14 3.16 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 197of5809 0.311 +/-1.93 pCi/g 0.417 +/-0.899 pCi/g 0.0635 +/-0.193 pCi/g 0.115 +/-0.354 pCi/g 0.0317 +/-0.109 pCi/g 0.0581 +/-0.114 pCi/g 1.63 +/-4.17 4.00 pCi/g BXFl 09/19/16 1442 1597811 10 1.51 +/-4.00 10.0 pCi/g 0.283 +/-0.285 2.00 pCi/g KSDl 09/17/16 1534 1597796 11 1.62 +/-2.09 6.00 pCi/g TXP3 09/22/16 2101 1598075 12 0.555 +/-0.674 2.00 pCi/g TXJI 09/23/16 2143 1598080 13 1.53 +/-1.82 5.00 pCi/g CXS7 09/20/16 1636 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.3.3 Sample ID: 405235032 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 198of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 79.2 (15%-125%) 1596396 62.9 (15%-125%) 1596396 96.3 (15%-125%) 1596399 86.8 (15%-125%) 1596395 91.6 (15%-125%) 1602285 92.2 (15%-125%) 1596402 79.2 (15%-125%) 1597796 110 (25%-125%) 1597412 91.5 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.3.4 Sample ID: 405235033 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 17.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0149 +/-0.045 0.126 Plutonium-239/240 HUh 0.0214 +/-0.073 0.135 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.023 +/-0.102 0.196 Uranium-233/234 Hh 0.633 +/-0.231 0.115 Uranium-235/236 Hh 0.0783 +/-0.0923 0.0998 Uranium-238 Hh 0.981 +/-0.285 0.127 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.128 +/-0.406 0.612 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.674 +/-0.656 0.720 Thorium-229 HUh 0.026 +/-0.272 0.568 Thorium-230 Hh 0.587 +/-0.559 0.719 Thorium-232 Hh 0.788 +/-0.578 0.512 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.00952 +/-0.0287 0.0808 Curium-242 Hh 0.00 +/-0.0989 0.147 Curium-243/244 Hh 0.0237 +/-0.0465 0.0645 Curium-245/246 Hh 0.0302 +/-0.0518 0.0453 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 1.91 +/-7.82 13.4 Rad Gamma Spec Analysis Gamma Il29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0794 +/-0.131 0.465 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.026 +/-0.173 0.318 Antimony-125 HUh -0.0033 +/-0.0849 0.168 Bismuth-212 HUih 0.00 +/-0.525 1.09 Bismuth-214 Hh 0.742 +/-0.158 0.103 Cesium-137 Hh 0.0502 +/-0.043 0.0647 Cobalt-60 HUh -0.029 +/-0.0378 0.0623 Europium-154 HUh 0.021 +/-0.108 0.217 Lead-212 Hb 0.937 +/-0.110 0.0737 Lead-214 Hh 0.954 +/-0.157 0.274 Page 199of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/160812 1596228 1 0.0322 +/-0.0451 1.00 pCi/g MXS2 09/24/16 2051 1596400 2 0.0369 +/-0.0731 1.00 pCi/g 0.0762 +/-0.102 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.0263 +/-0.257 1.00 pCi/g 0.0187 +/-0.0933 1.00 pCi/g 0.0323 +/-0.336 1.00 pCi/g 0.0877 +/-0.407 1.00 pCi/g MXS2 09/26/16 1709 1596399 4 0.172 +/-0.669 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.145 +/-0.273 1.00 pCi/g 0.220 +/-0.569 1.00 pCi/g 0.117 +/-0.595 1.00 pCi/g 0.0206 +/-0.0288 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0991 1.00 pCi/g 0.0121 +/-0.0466 1.00 pCi/g 0.00 +/-0.0519 1.00 pCi/g 6.51 +/-7.84 15.0 pCi/g MXS2 09/28/16 1443 1596402 7 0.156 +/-0.136 1.00 pCi/g MJHl 09/28/16 1018 1598620 8 0.146 +/-0.173 pCi/g MXRl 10/03/16 *0915 1596249 9 0.0759 +/-0.085 pCi/g 0.501 +/-0.585 pCi/g 0.0457 +/-0.162 pCi/g 0.029 +/-0.0431 0.100 pCi/g 0.0255 +/-0.040 pCi/g 0.0938 +/-0.108 pCi/g 0.0342 +/-0.120 pCi/g 0.132 +/-0.162 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.3.4 Sample ID: 405235033 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.5 +/-1.33 Protactinium-23 I HUlh 0.00 +/-0.704 Radium-226 Hh 0.742 +/-0.158 Radium-228 Hh 0.994 +/-0.240 Thallium-208 Hh 0.210 +/-0.074 Tin-126 HUih 0.00 +/-0.114 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 11.6 +/-3.82 Beta Hh 15.8 +/-2.74 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.398 +/-0.450 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.606 +/-1.83 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.116 +l-0.649 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.37 +/-1.92 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-OI-R , 0.511 0.577 0.103 0.190 0.0516 0.0574 4.00 2.75 0.962 3.30 1.1 I 3.39 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 JOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 200 of 5809 0.204 +/-1.48 pCi/g 0.261 +/-0.711 pCi/g 0.0457 +/-0.162 pCi/g 0.0809 +/-0.245 pCi/g 0.0228 +/-0.0746 pCi/g 0.0268 +/-0.116 pCi/g 1.63 +/-4.42 4.00 pCi/g BXFI 09/19/16 1437 1597811 10 1.25 +/-3.54 10.0 pCi/g 0.426 +l-0.450 2.00 pCi/g KSD! 09/19/16 1523 1597796 II 1.47 +/-1.83 6.00 pCi/g TXP3 09/22/16 2133 1598075 12 0.543 +l-0.650 2.00 pCi/g TXJI 09/23/16 2254 1598080 13 1.65 +/-1.92 5.00 pCi/g CXS7 09/20/16 1708 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.3.4 Sample ID: 405235033 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOO l October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 201 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 70.2 (15%-125%) 1596396 71.3 (15%-125%) 1596396 87.4 (15%-125%) 1596399 89.6 (15%-125%) 1596395 74.5 (15%-125%) 1602285 83.3 (15%-125%) 1596402 70.2 (15%-125%) 1597796 95 (25%-125%) 1597412 83.8 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.B.R.1.4 Sample ID: 405235034 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 19.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0116 +/-0.0433 0.0729 Plutonium-239/240 HUh -0.00725 +/-0.0321 0.0837 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0252 +/-0.074 0.138 Uranium-233/234 Hh 0.998 +/-0.329 0.164 Uranium-235/236 Hh 0.0806 +/-0.106 0.0806 Uranium-238 Hh 1.03 +/-0.333 0.164 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.00 +/-0.350 0.532 Alphaspec Th229 + 228,230,232 Solid Dry Weight Corrected" Thorium-228 Hh 1.25 +/-0.716 0.623 Thorium-229 Hh 0.00 +/-0.136 0.202 Thorium-230 Hh 0.470 +/-0.373 0.201 Thorium-232 Hh 0.987 +/-0.526 0.321 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.000508 +/-0.0376 0.0837 Curium-242 Hh 0.0471 +/-0.132 0.141 Curium-243/244 Hh 0.0196 +/-0.0451 0.0715 Curium-245/246 Hh 0.029 +/-0.0497 0.0435 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 3.52 +/-5.71 9.67 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HU!h 0.00 +/-0.198 0.273 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0244 +/-0.193 0.375 Antimony-125 HUh -0.00164 +/-0.0904 0.175 Bismuth-212 HU!h 0.00 +/-0.612 1.32 Bismuth-214 Hh 0.717 +/-0.174 0.109 Cesium-137 Hh 0.111 +/-0.0865 0.0748 Cobalt-60 HUh 0.0135 +/-0.0362 0.0771 Europium-154 HUh -0.114 +/-0.101 0.153 Lead-212 Hh 1.16 +/-0.129 0.0892 Lead-214 Hh 1.06 +/-0.185 0.313 Page 202 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0136 +/-0.0434 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0192 +/-0.0321 1.00 pCi/g 0.0525 +/-0.0741 1.00 pCi/g MXS2 09124116 1320 1596396 3 0.0416 +/-0.381 1.00 pCi/g 0.00 +/-0.107 1.00 pCi/g 0.0416 +/-0.387 1.00 pCi/g 0.00 +/-0.351 1.00 pCi/g MXS2 09126116 1735 1596399 4 0.175 +/-0.747 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.00 +/-0.136 1.00 pCi/g 0.00 +/-0.381 1.00 pCi/g 0.060 +l-0.550 1.00 pCi/g 0.0228 +/-0.0377 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.133 1.00 pCi/g 0.0164 +/-0.0451 1.00 pCi/g 0.00 +/-0.0499 1.00 pCi/g 4.69 +/-5.75 15.0 pCi/g MXS2 09/28/16 1530 1596402 7 0.00 +/-0.00 1.00 pCi/g MJHl 09/28/16 1019 1598620 8 0.172 +/-0.193 pCi/g MXRl 10/03/16 0915 1596249 9 0.0784 +/-0.0904 pCi/g 0.612 +/-0.792 pCi/g 0.0485 +/-0.177 pCi/g 0.0339 +/-0.0866 0.100 pCi/g 0.0329 +/-0.0367 pCi/g 0.0617 +/-0.113 pCi/g 0.0415 +/-0.143 pCi/g 0.151 +/-0.190 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.B.R.l.4 Sample ID: 405235034 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.3 +/-1.48 Protactinium-231* HUih 0.00 +/-0.882 Radium-226 Hh 0.717 +/-0.174 Radium-228 Hh 0.967 +/-0.285 Thallium-208 Hh 0.292 +/-0.0785 Tin-126 HUh 0.0419 +/-0.122 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.5 +/-4.12 Beta Hh 16.3 +/-2.90 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.0669 +/-0.493 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.877 +/-1.93 Liquid Sein! C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.354 +/-0.674 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.28 +/-1.93 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-OI Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.643 0.684 0.109 0.196 0.0461 0.127 3.90 3.06 0.914 3.41 1.14 3.41 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 7110B Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 203 of 5809 0.271 +/-1.64 pCi/g 0.312 +/-0.908 pCi/g 0.0485 +/-0.177 pCi/g 0.0835 +/-0.290 pCi/g 0.0199 +/-0.0795 pCi/g 0.0601 +/-0.123 pCi/g 1.57 +/-4.89 4.00 pCi/g BXFl 09119116 1437 1597811 10 1.39 +/-3.68 10.0 pCi/g 0.406 +/-0.493 2.00 pCi/g KSDI 09/17/16 1534 1597796 11 1.52 +/-1.93 6.00 pCi/g TXP3 09/22/16 2206 1598075 12 0.558 +/-0.675 2.00 pCi/g TIU! 09/24/16 0005 1598080 13 1.66 +/-1.93 5.00 pCi/g CXS7 09/20/16 1740 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3.B.R.l.4 Sample ID: 405235034 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 204 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 96.6 (15%-125%) 1596396 57.5 (15%-125%) 1596396 95 (15%-125%) 1596399 81.7 (15%-125%) 1596395 88.7 (15%-125%) 1602285 82.6 (15%-125%) 1596402 96.6 (15%-125%) 1597796 92.3 (25%-125%) 1597412 84.4 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.2.3 Sample ID: 405235035 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 16.3% Parameter Qualifier Result Uncertainty *MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 16.3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh -0.00871 +/-0.0602 0.146 Plutonium-239/240 HUh -0.0181 +/-0.0612 0.159 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.098 +/-0.225 0.408 Uranium-233/234 Hh 0.933 +/-0.352 0.212 Uranium-235/236 HUh 0.0335 +/-0.115 0.212 Uranium-238 Hh 0.731 +/-0.309 0.154 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0184 +/-0.305 0.646 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.21 +/-0.753 0.731 Thorium-229 Hh 0.00 +/-0.147 0.219 Thorium-230 Hh 1.09 +/-0.572 0.219 Thorium-232 Hh 0.927 +/-0.535 0.348 Am241, Cm Solid "Dry Weight Corrected" Americium-24 I Hh 0.0348 +/-0.0553 0.0764 Curium-242 HUh 0.0389 +/-0.146 0.246 Curium-243/244 Hh 0.014 +/-0.0395 0.0421 Curium-245/246 Hh 0.00 +/-0.0318 0.0473 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 2.11 +/-7.34 12.6 Rad Gamma Spec Analysis Gamma Il29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0528 +/-0.393 0.914 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0482 +/-0.212 0.400 Antimony-125 HUh 0.0602 +/-0.101 0.197 Bismuth-212 Hh 0.839 1.02 Bismuth-2 I 4 Hh 0.668 +/-0.175 0.114 Cesium-137 HUh 0.0251 +/-0.0614 0.0681 Cobalt-60 HUh -0.0136 +/-0.0372 0.0708 Europium-I 54 HUh 0.0382 +/-0.0958 0.210 Lead-212 Hh 0.937 +/-0.124 0.0806 Lead-214 Hh 0.769 +/-0.209 0.113 Page 205 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 I 0.0435 +/-0.0602 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0499 +/-0.0612 1.00 pCi/g 0.156 +/-0.226 1.00 pCi/g MXS2 09/24/16 1320* 1596396 3 0.0577 +/-0.409 1.00 pCi/g 0.0578 +/-0.115 1.00 pCi/g 0.0288 +/-0.350 1.00 pCi/g 0.0926 +/-0.306 1.00 pCi/g MXS2 09/26/16 1709 1596399 4 0.217 +/-0.784 1.00 pCi/g MXS2 09/28/16 1756 1596395 5 0.00 +/-0.148 1.00 pCi/g 0.00 +/-0.598 1.00 pCi/g 0.0652 +/-0.555 1.00 pCi/g 0.0175 +/-0.0554 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.0459 +/-0.146 1.00 pCi/g 0.00 +/-0.0395 1.00 pCi/g 0.00 +/-0.0319 1.00 pCi/g 6.10 +/-7.35 15.0 pCi/g MXS2 09/28/16 1616 1596402 7 0.324 +/-0.394 1.00 pCi/g MJHl 09/28/16 1019 1598620 8 0.185 +/-0.214 pCi/g MXRI 10/03/16 0916 1596249 9 0.0894 +/-0.105 pCi/g 0.460 +/-0.579 pCi/g 0.0507 +/-0.178 pCi/g 0.0304 +/-0.0614 0.100 pCi/g 0.0296 +/-0.0377 pCi/g 0.0897 +/-0.0973 pCi/g 0.0371 +/-0.134 pCi/g 0.0514 +/-0.21 I pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 . Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID:

4.3B.R.2.3 Sample ID: 405235035 Parameter Qualifier Result Uncertainty Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.3 +/-1.37 Protactinium-231 HU!h 0.00 +/-0.650 Radium-226 Hh 0.668 +/-0.175 Radium-228 Thallium-208 Tin-126 Hh Hh HU!h 0.974 0.225 0.00 +/-0.239 +/-0.0773 +/-0.149 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 7.78 +/-3.10 Beta Hh 20.8 +/-2.86 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.472 +/-0.450 Rad Liquid Scintillation_ Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.970 +/-1.89 Liquid Scint Cl 4, Solid Dry Weight Corrected" Carbon-14 HUh 0.342 +/-0.665 Liquid Scint Tc99, Solid Dry Weight Corrected" Technetium-99 HUh -1.35 +/-1.80 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R MDC 0.533 0.717 0.114 0.193 0.0633 0.120 3.91 3.36 0.969 3.32 1.13 3.18 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 !0B Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 206 of 5809 Report Date: Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst 0.215 +/-1.51 pCi/g 0.328 +/-0.666 pCi/g 0.0507 +/-0.178 pCi/g 0.0814 +/-0.244 pCi/g 0.0284 +/-0.0779 pCi/g 0.0562 +/-0.150 pCi/g 1.71 +/-3.52 4.00 pCi/g BXF! 1.59 +/-4.11 10.0 pCi/g 0.432 +l-0.450 2.00 pCi/g KSD! 1.48 +/-1.89 6.00 pCi/g TXP3 0.551 +l-0.665 2.00 pCi/g TXJ! 1.55 +/-1.80 5.00 pCi/g CXS7 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 October 4, 2016 Date Time Batch Mtd. 09/19/16 1437 1597811 10 09/17/16 1536 1597796 11 09/22/16 2238 1598075 12 09/24/16 0229-1598080 13 09/20/16 1812 1597412 14 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.2.3 Sample ID: 405235035 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 207 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 74.6 (15%-125%) 1596396 46.2 (15%-125%) 1596396 35.2 (15%-125%) 1596399 89 (15%-125%) 1596395 95.5 (15%-125%) 1602285 85.2 (15%-125%) 1596402 74.6 (15%-125%) 1597796 113 (25%-125%) 1597412 86.6 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.2.4 Sample ID: 405235036 Matrix: Soil Collect Date: 23-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 17.7% Parameter Qualifier

Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0223 +/-0.0613 0.106 Plutonium-239/240 HUh 0,018 +/-0.0614 0.114 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0193 +/-0.0673 0.128 Uranium-233/234 Hh 0.786 +/-0.374 0.235 Uranium-235/236 Hh 0.075 +/-0.147 0.204 Uranium-238 Hh 1.06 +/-0.425 0.127 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.149 +/-0.366 1.09 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.23 +/-0.706 0.615 Thorium-229 HUh 0.0504 +/-0.189 0.318 Thorium-230 Hh 0.711 +/-0.451 0.317 Thorium-232 Hh 0.709 +/-0.450 0.316 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0192 +/-0.0309 0.0986 Curium-242 Hh 0.00 +/-0.0996 0.148 Curium-243/244 HUh 0.00704 +/-0.0391 0.075 Curium-245/246 HXh 0.0609 +/-0.0671 0.0457 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh 0.212 +/-6.32 10.9 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" lodine-129 HUh 3.93E-05 +/-0.167 0.352 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 Huh -0.0376 +/-0.234 0.439 Antimony-125 HUh 0.121 +/-0.124 0.281 Bismuth-212 HU!h 0.00 +/-0.895 1.62 Bismuth-214 Hh 0.815 +/-0.184 0.136 Cesium-137 HUh 0.0114 +/-0.0402 0.0854 Cobalt-60 HUh -0.028 +/-0.0465 0.0852 Europium-154 HUh 0.0695 +/-0.143 0.308 Lead-212 Hh 0.934 +/-0.135 0.0982 Lead-214 Hh 0.850 +/-0.194 0.117 Page 208 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYT! 09/08/16 0812 1596228 1 0.027 +/-0.0614 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.031 +/-0.0615 1.00 pCi/g 0.0473 +/-0.0674 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.0539 +/-0.415 1.00 pCi/g 0.0382 +/-0.148 1.00 pCi/g 0.00 +/-0.490 1.00 pCi/g 0.282 +/-0.367 1.00 pCi/g MXS2 09/26/16 1709 1596399 4 0.174 +/-0.735 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.0595 +/-0.189 1.00 pCi/g 0.0593 +/-0.465 1.00 pCi/g 0.0591 +/-0.464 1.00 pCi/g 0.0293 +/-0.031 1.00 pCi/g MXS2 09/29/16 2126 1602285 6 0.00 +/-0.0998 1.00 pCi/g 0.0172 +/-0.0392 1.00 pCi/g 0.00 +/-0.0676 1.00 pCi/g 5.30 +/-6.32 15.0 pCi/g MXS2 09/28/16 1703 1596402 7 0.145 +/-0.167 1.00 pCi/g MJHl 09/28/16 1117 1598620 8 0.198 +/-0.235 pCi/g MXRl 10/03/16 0916 1596249 9 0.127 +/-0.136 pCi/g 0.733 +/-1.08 pCi/g 0.0581 +/-0.187 pCi/g 0.0369 +/-0.0405 0.100 pCi/g 0.0326 +/-0.0481 pCi/g 0.128 +/-0.146 pCi/g 0.0447 +/-0.144 pCi/g 0.0507 +/-0. 197 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.2.4 Sample ID: 405235036 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 10.6 +/-1.77 Protactinium-231 HU!h 0.00 +/-0.928 Radium-226 Hh 0.815 +/-0.184 Radium-228 Hh 0.922 +/-0.308 Thallium-208 Hh 0.235 +/-0.111 Tin-126 HUih 0.00 +/-0.146 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 8.65 +/-3.14 Beta Hh 17.3 +/-2.42 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.159 +/-0.339 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 1.79 +/-2.04 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.434 +/-0.690 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.0134 +/-1.77 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-OJ-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-O I Modified DOE HASL 300, 4.5.2.3/Ga-OJ-R 0.713 0.658 0.136 0.249 0.0556 0.131 3.86 2.48 0.727 3.43 1.17 3.05 2 3 4 5 6 7 8 9 JO II 12 13 14 EPA 900.0/SW846 9310/SM 71 JOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 209of5809 0.266 +/-1.86 pCi/g 0.285 +/-0.960 pCi/g 0.0581 +/-0.187 pCi/g 0.0996 +/-0.311 pCi/g 0.0227 +/-0.112 pCi/g 0.0614 +/-0.146 pCi/g 1.67 +/-3.56 4.00 pCi/g BXFI 09/19/16 1437 1597811 JO l.15 +/-3.44 10.0 pCi/g 0.310 +/-0.339 2.00 pCi/g KSDI 09/17/16 1536 1597796 II 1.53 +/-2.04 6.00 pCi/g TXP3 09/22/16 2311 1598075 12 0.570 +/-0.690 2.00 pCi/g TXJJ 09/24/16 0341 1598080 13 1.48 +/-1.77 5.00 pCi/g CXS7 09/20/16 1844 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.3B.R.2.4 Sample ID: 405235036 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 210 of 5 809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 84.6 (15%-125%) 1596396 34.8 (15%-125%) 1596396 99.4 (15%-125%) 1596399 80.6 (15%-125%) 1596395 92.3 (15%-125%) 1602285 81.4 (15%-125%) 1596402 84.6 (15%-125%) 1597796 82.8 (25%-125%) 1597412 91.3 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R.2.4 Sample ID: 405235037 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 6.23% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 6.23 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh -0.016 +/-0.0483 0.136 Plutonium-239/240 HUh -0.0371 +/-0.0523 0.171 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.060 +/-0.102 0.178 Uranium-233/234 Hh 0.295 +/-0.371 0.572 Uranium-235/236 HUh -0.0582 +/-0.135 0.399 Uranium-238 Hh 0.454 +/-0.359 0.334 Alphaspec Np237, Solid Dry Weight Corrected" Neptunium-237 HUh -0.139 +/-0.302 0.930 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.12 +/-0.782 0.683 Thorium-229 HUh 0.0679 +/-0.255 0.428 Thorium-230 Hh 0.224 +/-0.357* 0.493 Thorium-232 Hh 0.558 +/-0.499 0.543 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.00816 +/-0.0669 0.163 Curium-242 Hh 0.00 +/-0.165 0.250 Curium-243/244 HUh -0.0253 +/-0.0494 0.155 Curium-245/246 Hh 0.102 +/-0.116 0.113 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 3.80 +/-8.24 14.0 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0144 +/-0.221 0.437 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0456 +/-0.176 0.342 Antimony-125 HUh 0.0696 +/-0.0879 0.190 Bismuth-212 HUih 0.00 +/-0.766 1.20 Bismuth-214 Hh 0.632 +/-0.169 0.112 Cesium-137 HUh 0.0137 +/-0.0379 0.0798 Cobalt-60 HUh -0.0144 +/-0.0333 0.0619 Europium-154 HUh 0.0683 +/-0.139 0.292 Lead-212 Hh 0.766 +/-0.124 0.0852 Lead-214 Hh 0.827 +/-0.178 0.278 Page 211of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 I 0.0345 +/-0.0484 1.00 pCi/g MXS2 09/26/16 1355 1596400 2 0.0524 +/-0.0524 1.00 pCi/g 0.0692 +/-0.104 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.195 +/-0.379 1.00 pCi/g 0.109 +/-0.136 1.00 pCi/g 0.0766 +/-0.378 1.00 pCi/g 0.247 +/-0.302 1.00 pCi/g MXS2 09/26/16 1709 1596399 4 0.162 +/-0.810 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.0801 +/-0.255 1.00 pCi/g 0.113 +/-0.359 1.00 pCi/g 0.138 +/-0.509 1.00 pCi/g 0.0469 +/-0.067 1.00 pCi/g MXS2 10/01/16 1323 1602285 6 0.00 +/-0.165 1.00 pCi/g 0.0427 +/-0.0496 1.00 pCi/g 0.017 +/-0.117 1.00 pCi/g 6.81 +/-8.28 15.0 pCi/g MXS2 09/28/16 1750 1596402 7 0.179 +/-0.221 1.00 pCi/g MJHI 09/28/16 11I8 1598620 8 0.156 +/-0.177 pCi/g MXRl 10/03/16 0917 1596249 9 0.0856 +/-0.0935 pCi/g 0.548 +/-0.830 pCi/g 0.0493 +/-0.177 pCi/g 0.036 +/-0.0384 0.100 pCi/g 0.0242 +/-0.0339 pCi/g 0.128 +/-0.143 pCi/g 0.0394 +/-0.144 pCi/g 0.134 +/-0.191 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R.2.4 Sample ID: 405235037 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.9 +/-1.42 Protactinium-231 HUlh 0.00 +/-0.889 Radium-226 Hh 0.632 +/-0.169 Radium-228 Hh 0.545 +/-0.228 Thallium-208 Hh. 0.210 +/-0.0801 Tin-126 HU!h 0.00 +/-0.0738 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 8.01 +/-3.21 Beta Hh 15.9 +/-2.27 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh -0.427 +/-0.519 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.19 +/-1.73 Liquid Sein/ CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.0748 +/-0.588 Liquid Sein/ Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.14 +/-1.48 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-.RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Oi-R 0.497 0.681 0.112 0.202 0.0604 0.0866 3.85 2.13 1.11 2.97 I.OJ 2.62 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 905.0 Modified/DOE RP50 I Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 212of5809 0.188 +/-1.75 pCi/g 0.309 +/-0.896 pCi/g 0.0493 +/-0.177 pCi/g 0.0844 +/-0.237 pCi/g 0.0268 +/-0.0821 pCi/g 0.041 +/-0.0754 pCi/g 1.60 +/-3.55 4.00 pCi/g BXFI 09/19/16 1437 1597811 10 0.974 +/-3.16 10.0 pCi/g 0.491 +/-0.520 2.00 pCi/g KSDI 09/17/16 1536 1597796 II 1.33 +/-1.73 6.00 pCi/g TXP3 09/22/16 2344 1598075 12 0.492 +/-0.588 2.00 pCi/g TXJI 09/24/16 0452 1598080 13 1.27 +/-1.48 5.00 pCi/g CXS7 09120116 1915 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R.2.4 Sample ID: 405235037 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 213 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 67.4 (15%-125%) 1596396 25.9 (15%-125%) 1596396 84.8 (15%-125%) 1596399 86.6 (15%-125%) 1596395 70.6 (15%-125%) 1602285 88.9 (15%-125%) 1596402 67.4 (15%-125%) 1597796 97.8 (25%-125%) 1597412 87.1 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R. l .3 Sample ID: 405235038 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 16.3% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 16.3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid Dry Weight Corrected" Plutonium-23 8 Hh 0.0287 +/-0.066 0.105 Plutonium-239/240 HUh -0.00902 +/-0.0399 0.104 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0122 +/-0.074 0.147 Uranium-233/234 Hh 0.572 +/-0.201 0.114 Uranium-235/236 Hh 0.0916 +/-0.0915 0.106 Uranium-238 Hh 0.736 +/-0.225 0.0958 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0866 +/-0.295 0.822 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.30 +/-0.853 0.803 Thorium-229 Hh 0.246 +/-0.355 0.428 Thorium-230 Hh 0.891 +/-0.581 0.267 Thorium-232 Hh 1.33 +/-0.698 0.266 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.016 +/-0.045 0.0481 Curium-242 Hh 0.00 +/-0.116 0.173 Curium-243/244 HUh -0.00781 +/-0.0345 0.0901 Curium-245/246 Hh 0.0366 +/-0.0628 0.0549 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -5.78 +/-7.72 13.7 Rad Gamma Spec Analysis Gamma Il29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0563 +/-0.191 0.434 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.024 +/-0.214 0.373 Antimony-125 HUh -0.0676 +/-0.0977 0.170 Bismuth-212 HUih 0.00 +/-1.34 1.34 Bismuth-214 Hh 0.567 +/-0.155 0.132 Cesium-137 Hh 0.115 +/-0.0596 0.0624 Cobalt-60 HUh 0.0113 +/-0.0424 0.0894 Europium-154 HUh -0.0421 +/-0.122 0.231 Lead-212 Hh 0.937 +/-0.121 0.0868 Lead-214 Hh 0.776 +/-0.168 0.114 Page 214of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent L YT! 09/08/16 0812 1596228 1 0.024 +/-0.0661 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0238 +/-0.040 1.00 pCi/g 0.055 +/-0.074 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.0311 +/-0.223 1.00 pCi/g 0.027 +/-0.0928 1.00 pCi/g 0.022 +/-0.257 1.00 pCi/g 0.195 +/-0.295 1.00 pCi/g MXS2 09/26/16 1709 1596399 4 0.222 +/-0.888 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.0801 +/-0.358 1.00 pCi/g 0.00 +/-0.603 1.00 pCi/g 0.00 +/-0.738 1.00 pCi/g 0.00 +/-0.0451 1.00 pCi/g MXS2 09/29/16 2152 1602285 6 0.00 +/-0.117 1.00 pCi/g 0.0207 +/-0.0346 1.00 pCi/g 0.00 +/-0.063 1.00 pCi/g 6.64 +/-7.72 15.0 pCi/g MXS2 09/28/16 1837 1596402 7 0.172 +/-0.193 1.00 pCi/g MJHl 09/28/16 1118 1598620 8 0.172 +/-0.215 pCi/g MXRl 10/03/16 0917 1596249 9 0.0758 +/-0.102 pCi/g 0.619 +/-1.72 pCi/g 0.0594 +/-0.157 pCi/g 0.0274 +/-0.0598 0.100 pCi/g 0.0385 +/-0.0427 pCi/g 0.0991 +/-0.123 pCi/g 0.0403 +/-0.131 pCi/g 0.0518 +/-0.171 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R. l .3 Sample ID: 405235038 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.4 +/-1.44 Protactinium-231 HU!h 0.00 +/-0.599 Radium-226 Hh 0.567 +/-0.155 Radium-228 Hh 0.819 +/-0.386 Thallium-208 Hh 0.285 +/-0.0667 Tin-126 HU!h 0.00 +/-0.194 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 11.4 +/-3.53 Beta Hh 15.6 +/-2.33 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.784 +/-0.594 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.35 +l-1.95 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 Hh 0.700 +/-0.638 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.739 +/-1.84 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.658 0.740 ' 0.132 0.260 0.0613 0.135 3.90 2.41 1.26 3.36 1.07 3.14 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 215of5809 0.273 +/-1.58 pCi/g 0.340 +/-0.616 pCi/g 0.0594 +/-0.157 pCi/g 0.114 +/-0.388 pCi/g 0.0273 +/-0.0678 pCi/g 0.0635 +/-0.195 pCi/g 1.66 +/-4.14 4.00 pCi/g BXFI 09119116 1437 1597811 10 1.11 +/-3.18 10.0 pCi/g 0.573 +/-0.594 2.00 pCi/g KSDI 09/17/16 1537 1597796 II 1.50 +/-1.95 6.00 pCi/g TXP3 09/23/16 0017 1598075 12 0,521 +/-0.640 2.00 pCi/g TXJI 09/24/16 0603 1598080 13 1.53 +/-1.84 5.00 pCi/g CXS7 09/20/16 1947 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R. l .3 Sample ID: 405235038 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 216of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 76.4 (15%-125%) 1596396 83.8 (15%-125%) 1596396 98.2 (15%-125%) 1596399 86.4 (15%-125%) 1596395 81.5 (15%-125%) 1602285 88.7 (15%-125%) 1596402 76.4 (15%-125%) 1597796 92.3 (25%-125%) 1597412 89.2 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R.1.4 Sample ID: 405235039 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 8.7% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 8.70 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0121 +/-0.0366 0.103 Plutonium-239/240 HUh 0.000668 +/-0.0495 0.110 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00515 +/-0.0614 0.127 Uranium-233/234 Hh 0.627 +/-0.214 0.101 Uranium-235/236 Hh 0.0277 +/-0.0636 0.101 Uranium-238 Hh 0.994 +/-0.267 0.0871 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0332 +/-0.277 0.650 Alphaspec Th229 + 228,230,232 Solid Dry Weight Corrected" Thorium-228 Hh 1.13 +/-0.727 0.789 Thorium-229 HUh 0.123 +/-0.279 0.479 Thorium-230 Hh 0.223 +/-0.305 0.416 Thorium-232 Hh 0.883 +/-0.499 0.204 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.000729 +/-0.0541 0.120 Curium-242 Hh 0.00 +/-0.132 0.197 Curium-243/244 HUh 0.00519 +/-0.0542 0.113 Curium-245/246 Hh 0.0208 +/-0.0586 0.0625 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh 0.788 +/-5.30 9.16 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0138 +/-0.173 0.440 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUii -0.123 +/-0.222 0.350 Antimony-125 HUh -0.0428 +/-0.0855 0.162 Bismuth-212 HU!h 0.00 +/-0.503 1.14 Bismuth-214 Hh 0.787 +/-0.143 0.0513 Cesium-137 HU!h 0.00 +/-0.0333 0.0738 Cobalt-60 HUh -0.00863 +/-0.0359 0.0695 Europium-154 HUh 0.0381 +/-0.097 0.212 Lead-212 Hh 0.726 +/-0.137 0.0813 Lead-214 Hh 1.05 +/-0.168 0.271 Page 217 of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0812 1596228 1 0.0261 +/-0.0366 1.00 pCi/g MXS2 09/26/16 1355 1596400 2 0.030 +/-0.0496 1.00 pCi/g 0.0458 +/-0.0614 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.023 +/-0.239 1.00 pCi/g 0.0231 +/-0.0638 1.00 pCi/g 0.0163 +/-0.316 1.00 pCi/g 0.118 +/-0.277 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.256 +/-0.756 1.00 pCi/g MXS2 09/28/16 1756 1596395 5 0.137 +/-0.280 1.00 pCi/g 0.106 +/-0.307 1.00 pCi/g 0.00 +/-0.519. 1.00 pCi/g 0.0327 +/-0.0541 1.00 pCi/g MXS2 09/29/16 2152 1602285 6 0.00 +/-0.133 1.00 pCi/g 0.0288 +/-0.0543 1.00 pCi/g 0.00 +/-0.0587 1.00 pCi/g 4.42 +/-5.30 15.0 pCi/g MXS2 09/29/16 1301 1596402 7 0.156 +/-0.173 1.00 pCi/g MJHl 09/28/16 1119 1598620 8 0.160 +/-0.230 pC.i/g MXRl 10/03/16 0918 1596249 9 0.0719 +/-0.0877 pCi/g 0.521 +/-0.622 pCi/g 0.0193 +/-0.147 pCi/g 0.0332 +/-0.0369 0.100 pCi/g 0.0288 +/-0.0361 pCi/g 0.0902 +/-0.0985 pCi/g 0.0376 +/-0.142 pCi/g 0.130 +/-0.174 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R. l .4 Sample ID: 405235039 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.3 +/-1.58 0.670 Protactinium-231 HUih 0.00 +/-0.739 0.721 Radium-226 Hh 0.787 +/-0.143 0.0513 Radium-228 Hh 0.666 +/-0.327 0.222 Thallium-208 Hh 0.240 +/-0.0812 0.059 Tin-126 HUh 0.0634 +/-0.134 0.145 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 10.3 +/-3.89 3.94 Beta Hh 17.9 +/-3.34 3.59 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.286 +/-0.620 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.13 +/-1.78 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.201 +/-0.586 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.678 +/-1.82 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R I.I I 3.08 0.998 3.18 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 218of5809 0.281 +/-1.72 pCi/g 0.330 +/-0.761 pCi/g 0.0193 +/-0.147 pCi/g 0.0955 +/-0.329 pCi/g 0.0262 +/-0.0819 pCi/g 0.0687 +/-0.134 pCi/g 1.52 +/-4.38 4.00 pCi/g BXFl 09/19/16 1442 1597811 10 1.64 +/-4.27 10.0 pCi/g 0.485 +/-0.622 2.00 pCi/g KSDl 09/17/16 1537 1597796 11 1.38 +/-1.78 6.00 pCi/g TXP3 09/23/16 0049 1598075 12 0.488 +/-0.586 2.00 pCi/g TXJI 09/24/16 0714 1598080 13 1.54 +/-1.82 5.00 pCi/g CXS7 09/20/16 2019 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4C.R.l.4 Sample ID: 405235039 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 219 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 85.3 (15%-125%) 1596396 77.2 (15%-125%) 1596396 102 (15%-125%) 1596399 95.8 (15%-125%) 1596395 90.4 (15%-125%) 1602285 79.1 (15%-125%) 1596402 85.3 (15%-125%) 1597796 92.3 (25%-125%) 1597412 81.l (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.1.3 Sample ID: 405235040 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 14.8% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 14.8 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00424 +/-0.0636 0.149 Plutonium-239/240 Hh 0.0581 +/-0.0837 0.101 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0248 +/-0.040 0.127 Uranium-233/234 Hh 0.495 +/-0.185 0.103 Uranium-235/236 Hh 0.107 +/-0.0954 0.104 Uranium-238 Hh 0.698 +1:0.218 0.103 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.184 +/-0.615 1.14 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.15 +/-0.721 0.675 Thorium-229 HUh 0.00291 +/-0.216 0.479 Thorium-230 Hh 0.677 +/-0.502 0.562 Thorium-232 Hh 0.417 +/-0.378 0.347 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.00357 +/-0.0308 0.0712 Curium-242 Hh 0.0535 +/-0.150 0.161 Curium-243/244 HUh 0.0115 +/-0.043 0.0724 Curium-245/246 Hh 0.017 +/-0.0478 0.051 Liquid Sein/ Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -6.22 +/-7.91 14.0 Rad Gamma Spec Analysis Gamma IJ 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0767 +/-0.179 0.293 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0811 +/-0.206 0.418 Antimony-125 HUh -0.122 +/-0.113 0.160 Bismuth-212 Hh 0.799 +/-0.910 0.879 Bismuth-214 Hh 0.756 +/-0.194 0.130 Cesium-137 Hh 0.142 +/-0.0717 0.0633 Cobalt-60 HUh -0.00875 +/-0.0349 0.0589 Europium-154 HUh -0.0592 +/-0.0908 0.161 Lead-212 Hh 0.961 +/-0.133 0.0882 Lead-214 Hh 0.784 +/-0.163 0.107 Page 220 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0812 1596228 1 0.0425 +/-0.0637 1.00 pCi/g MXS2 09/24/16 2054 1596400 2 0.0189 +/-0.0842 1.00 pCi/g 0.0378 +/-0.0401 1.00 pCi/g MXS2 09/24/16 1320 1596396 3 0.0263 +/-0.204 1.00 pCi/g 0.0264 +/-0.0971 1.00 pCi/g 0.0263 +/-0.249 1.00 pCi/g 0.302 +/-0.615 1.00 pCi/g MXS2 09/26/16 1711 1596399 4 0.191 +/-0.746 1.00 pCi/g MXS2 09/24/16 1318 1596395 5 0.131 +/-0.216 1.00 pCi/g 0.172 +/-0.514 1.00 pCi/g 0.0649 +/-0.384 1.00 pCi/g 0.0133 +/-0.0308 1.00 pCi/g MXS2 09/29/16 2152 1602285 6 0.00 +/-0.151 1.00 pCi/g 0.0135 +/-0.0431 1.00 pCi/g 0.00 +/-0.0478 1.00 pCi/g 6.81 +/-7.91 15.0 pCi/g MXS2 09/28/16 2010 1596402 7 0.0925 +/-0.183 1.00 pCi/g MJHl 09/28/16 1119 1598620 8 0.194 +/-0.209 pCi/g MXRl 10/03/16 0920 1596249 9° 0.0709 +/-0.126 pCi/g 0.391 +/-0.911 pCi/g 0.0588 +/-0.197 pCi/g 0.0281 +/-0.072 0.100 pCi/g 0.0237 +/-0.0351 pCi/g 0.0655 +/-0.0947 pCi/g 0.041 +/-0.143 pCi/g 0.0483 +/-0.167 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.l.3 Sample ID: 405235040 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.0 +/-1.36 Protactinium-231 HU!h 0.00 +/-0.418 Radium-226 Hh 0.756 +/-0.194 Radium-228 Hh 0.863 +/-0.231 Thallium-208 Hh 0.245 +/-0.0778 Tin-126 HUh 0.0671 +/-0.159 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 10.2 +/-3.65 Beta Hh 13.0 +/-2.34 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.328 +/-0.390 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 1.74 +/-1.98 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.276 +/-0.680 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.152 +/-1.88 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-OJ-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-OI Modified DOE HASL 300, 4.5.2.3/Ga-01-R, 0.462 0.829 0.130 0.202 0.0501 0.182 3.91 2.17 0.926 3.32 1.16 3.24 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 221 of 5809 0.179 +/-1.52 pCi/g 0.384 +/-0.473 pCi/g 0.0588 +/-0.197 pCi/g 0.0862 +/-0.236 pCi/g 0.0218 +/-0.0785 pCi/g 0.0871 +/-0.160 pCi/g 1.59 +/-4.16 4.00 pCi/g BXFI 09119116 1438 1597811 JO 0.961 +/-3.02 10.0 pCi/g 0.389 +/-0.390 2.00 pCi/g KSDI 09/17/16 1537 1597796 II 1.48 +/-1.98 6.00 pCi/g TXP3 09/23/16 0237 1598075 12 0.565 +/-0.680 2.00 pCi/g TXJJ 09/24/16 0826 1598080 13 1.58 +/-1.88 5.00 pCi/g CXS7 09120116 2051 1597412 14 Analyst Date Time Prep Batch LYTI 09/08/16 0812 1596228 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R. l .3 Sample ID: 405235040 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Amerieium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma).

Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 222of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596400 66.9 (15%-125%) 1596396 83.8 (15%-125%) 1596396 88.4 (15%-125%) 1596399 73.5 (15%-125%) 1596395 101 (15%-125%) 1602285 95.7 (15%-125%) 1596402 66.9 (15%-125%) 1597796 91 (25%-125%) 1597412' 86.1 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.l.4 Sample ID: 405235041 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 12% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 12.0 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0701 +/-0.119 0.105 Plutonium-239/240 HUh -0.00872 +/-0.0698 0.165 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0147 +/-0.0865 0.172 Uranium-233/234 Hh 0.802 +/-0.207 0.0934 Uranium-235/236 HUh 0.0181 +l-0.0555 0.103 Uranium-238 Hh 0.704 +/-0.193 0.0739 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0562 +/-0.315 0.795 Alphaspec Th229 + 228,230,232 Solid Dry Weight Corrected" Thorium-228 Hh 1.07 +/-0.620 0.626 Thorium-229 Hh 0.373 +/-0.308 0.265 Thorium-230 Hh 0.445 +/-0.366 0.445 Thorium-232 Hh 0.646 +/-0.390 0.263 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0106 +/-0.0523 0.132 Curium-242 HUh -0.00899 +/-0.124 0.269 Curium-243/244 Hh 0.0154 +/-0.0505 0.0783 Curium-245/246 Hh 0.00 +/-0.0402 0.0609 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh -0.671 +/-7.42 12.8 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.176 +/-0.244 0.817 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0314 +/-0.177 0.361 Antimony-125 HUh -0.0586 +/-0.0781 0.140 Bismuth-212 HUih 0.00 +/-0.700 0.973 Bismuth-214 Hh 0.794 +/-0.159 0.0844 Cesium-137 HUih 0.00 +/-0.049 0.0572 Cobalt-60 HUh 0.0168 +/-0.033 0.0712 Europium-154 HUh -0.00765 +/-0.101 0.196 Lead-212 Hh 0.807 +/-0.113 0.0767 Lead-214 Hh 0.803 +/-0.167 0.252 Page 223 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0827 1596233 I 0.00 +/-0.120 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0304 +/-0.0702 1.00 pCi/g 0.0631 +/-0.0866 1.00 pCi/g HAKB 09/22/16 1000 1596408 3 0.0266 +/-0.244 1.00 pCi/g 0.0316 +/-0.0556 1.00 pCi/g 0.0168 +/-0.224 1.00 pCi/g 0.163 +/-0.315 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.202 +/-0.648 1.00 pCi/g HAKB 09/27/16 1712 1596407 5 0.0496 +/-0.314 1.00 pCi/g 0.140 +/-0.373 1.00 pCi/g 0.0493 +/-0.402 1.00 pCi/g 0.0395 +/-0.0523 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.0415 +/-0.124 1.00 pCi/g 0.0121 +/-0.0506 1.00 pCi/g 0.00 +/-0.0403 1.00 pCi/g 6.25 +/-7.42 15.0 pCi/g HAKB 09/23/16 1325 1596414 7 0.290 +/-0.257 1.00 pCi/g MJHl 09/28/16 1250 1598647 8 0.167 +/-0.177 pCi/g MXRl 10/03/16 0554 1596252 9 0.0622 +/-0.0825 pCi/g 0.446 +/-0.824 pCi/g 0.0369 +/-0.163 pCi/g 0.0256 +/-0.049 0.100 pCi/g 0.0309 +/-0.0339 pCi/g 0.0853 +/-0.101 pCi/g 0.0356 +/-0.121 pCi/g 0.122 +/-0.170 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.1.4 Sample ID: 405235041 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.8 +/-1.23 Protactinium-231 HUih 0.00 +/-0.541 Radium-226 Hh 0.794 +/-0.159 Radium-228 Hh 0.629 +/-0.246 Thallium-208 Hh 0.273 +/-0.0808 Tin-126 HUh 0.0427 +/-0.187 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 17.9 +/-4.49 Beta Hh 19.7 +/-2.89 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 0.653 +/-0.699 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.40 +/-2.36 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0252 +/-0.675 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.325 +/-1.62 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.428 0.642 0.0844 0.204 0.0494 0.128 3.91 2.95 1.16 4.00 1.16 2.84 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 224 of 5809 0.171 +/-1.38 pCi/g 0.295 +/-0.565 pCi/g 0.0369 +/-0.163 pCi/g 0.0896 +/-0.249 pCi/g 0.022 +/-0.0816 pCi/g 0.0606 +/-0.188 pCi/g 1.60 +l-5.60 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.36 +/-3.85 10.0 pCi/g 0.509 +/-0.709 2.00 pCi/g KSDI 09/22/16 1720 1597803 II 1.94 +/-2.36 6.00 pCi/g TXP3 09/23/16 2131 1598092 12 0.567 +/-0.675 2.00 pCi/g TXJI 09/26/16 1633 1598081 13 1.34 +/-1.62 5.00 pCi/g CXS7 09/20/16 1338 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R. l .4 Sample ID: 405235041 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Sein! Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 225 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 69.6 (15%-125%) 1596408 84.9 (15%-125%) 1596408 72.2 (15%-125%) 1596411 82.6 (15%-125%) 1596407 99.9 (15%-125%) 1596410 107 (15%-125%) 1596414 69.6 (15%-125%) 1597803 92.3 (25%-125%) 1597414 98.3 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.2.3 Sample ID: 405235042 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 11% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 11.0 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.00 +/-0.0544 0.0826 Plutonium-239/240 HUh -0.0103 +/-0.0553 0.141 ASP Uranium Isotopic, Solid Dry Weight Corrected" Uranium-232 HUh 0.00324 +/-0.0731 0.160 Uranium-233/234 Hh 0.599 +/-0.246 0.187 Uranium-235/236 Hh 0.0574 +l-0.092 0.129 Uranium-238 Hh 0.636 +/-0.245 0.128 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0409 +/-0.415 0.870 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.65 +/-0.701 0.603 Thorium-229 Hh 0.187 +/-0.243 0.344 Thorium-230 Hh 0.809 +/-0.409 0.271 Thorium-232 Hh 0.623 +/-0.360 0.234 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0056 +/-0.0928 0.196 Curium-242 Hh 0.00 +/-0.322 0.489 Curium-243/244 Hh 0.00 +/-0.0936 0.142 Curium-245/246 Hh 0.047 +/-0.149 0.225 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh 1.61 +/-6.94 11.9 Rad Gamma Spec Analysis Gamma IJ 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0936 +/-0.181 0.355 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0685 +/-0.199 0.389 Antimony-125 HUh 0.0894 +/-0.101 0.218 Bismuth-212 HU!h 0.00 +/-0.930 1.30 Bismuth-214 Hh 0.651 +/-0.198 0.131 Cesium-137 Hh 0.249 +/-0.0842 0.0702 Cobalt-60 HUh 0.00586 +/-0.0368 0.0772 Europium-154 HUh -0.0302 +/-0.0912 0.172 Lead-212 Hh 0.687 +/-0.146 0.101 Lead-214 Hh 0.799 +/-0.221 0.122 Page 226 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.00 +/-0.0546 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0293 +/-0.0555 1.00 pCi/g 0.0418 +/-0.0732 1.00 pCi/g HAKB 09/22/16 1000 1596408 3 0.0589 +/-0.273 1.00 pCi/g 0.0296 +/-0.0927 1.00 pCi/g 0.0295 +/-0.275 1.00 pCi/g 0.216 +/-0.415 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.203 +/-0.744 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.0986 +/-0.244 1.00 pCi/g 0.0622 +/-0.427 1.00 pCi/g 0.0438 +/-0.372 1.00 pCi/g 0.0282 +/-0.0934 1.00 pCi/g HAKB 09/22/16 1614 1596410 6 0.00 +/-0.324 1.00 pCi/g 0.00 +/-0.0941 1.00 pCi/g 0.0322 +/-0.149 1.00 pCi/g 5.79 +/-6.95 15.0 pCi/g HAKB 09/23/16 1426 1596414 7 0.129 +/-0.186 1.00 pCi/g MJHl 09/28/16 1334 1598647 8 0.178 +/-0.202 pCi/g MXRI 10/03/16 0655 °1596252 9 0.0991 +/-0.109 pCi/g 0.598 +/-1.13 pCi/g 0.0587 +/-0.200 pCi/g 0.0311 +/-0.0848 0.100 pCi/g 0.0324 +/-0.0369 pCi/g 0.0697 +/-0.0922 pCi/g 0.0471 +/-0.151 pCi/g 0.0553 +/-0.223 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.2.3 Sample ID: 405235042 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.3 +/-1.42 Protactinium-231 HU!h 0.00' +/-0.703 Radium-226 Hh 0.651 +/-0.198 Radium-228 HU!h 0.00 +/-0.270 Thallium-208 Hh 0.308 +/-0.0737 Tin-126 HUh 0.0374 +/-0.0762 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 17.7 +/-4.03 Beta Hh 21.8 +/-2.57 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.253 +/-0.585 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.0656 +/-2.16 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.159 +/-0.683 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 Hh 1.43 +/-1.62 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300,, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.i.3/Ga-01-R 0.616 0.675 0.131 0.502 0.0631 0.152 3.99 2.47 1.03 3.75 1.16 2.73 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 227 of 5809 0.251 +/-1.56 pCi/g 0.304 +/-0.714 pCi/g 0.0587 +l-0.200 pCi/g 0.235 +/-0.454 pCi/g 0.028 +/-0.0749 pCi/g 0.0718 +/-0.0781 pCi/g 1.75 +/-5.42 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.15 +/-4.01 10.0 pCi/g 0.469 +/-0.587 2.00 pCi/g KSDI 09/22/16 1720 1597803 II 1.81 +/-2.16 6.00 pCi/g TXP3 09/23/16 2314 1598092 12 0.570 +/-0.683 2.00 pCi/g TXJI 09/26/16 1745 1598081 13 1.29 +/-1.63 5.00 pCi/g CXS7 09/20/16 1355 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.2.3 Sample ID: 405235042 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 228 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 79.8 (15%-125%) 1596408 88.9 (15%-125%) 1596408 94 (15%-125%) 1596411 91.9 (15%-125%) 1596407 94.6 (15%-125%) 1596410 64.6 (15%-125%) 1596414 79.8 (15%-125%) 1597803 81.5 (25%-125%) 1597414 97 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.2.4 Sample ID: 405235043 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 14.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 14.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.016 +/-0.0724 0.132 Plutonium-239/240 HUh -0.016 +/-0.0524 0.147 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0233 +/-0.0564 0.169 Uranium-233/234 Hh 0.761 +/-0.284 0.152 Uranium-235/236 Hh 0.0677 +/-0.103 0.135 Uranium-238 Hh 0.739 +/-0.279 0.144 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0399 +l-0.405 0.848 Alphaspec Th229 + 228,230,232 Solid Dry Weight Corrected" Thorium-228 Hh 1.71 +/-0.858 0.785 Thorium-229 Hh 0.243 +/-0.308 0.383 Thorium-230 Hh 0.623 +/-0.454 0.454 Thorium-232 Hh 0.739 +/-0.469 0.329 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0414 +/-0.0794 0.107 Curium-242 Hh 0.00 +/-0.161 0.242 Curium-243/244 Hh 0.0234 +/-0.0656 0.0703 Curium-245/246 Hh 0.0737 +/-0.105 0.122 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 0.786 +/-6.12 10.5 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0904 +/-0.393 0.769 Gammaspec, Gamma, Solid Dry Weight Corrected" Actinium-2'.27 HUh -0.0834 +/-0.187 0.339 Antimony-125 HUh 0.037 +/-0.0842 0.180 Bismuth-212 Hh 1.63 +/-0.684 0.770 Bismuth-214 Hh 0.703 +/-0.135 0.0873 Cesium-137 Hh 0.0694 +/-0.0535 0.0503 Cobalt-60 HUh 0.013 +/-0.0208 0.0545 Europium-154 HUh -0.0759 +/-0.113 0.169 Lead-212 Hh 0.954 +/-0.116 0.0771 Lead-214 Hh 0.876 +/-0.167 0.094 Page 229 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU

RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0827 1596233 1 0.0275 +/-0.0725 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0353 +/-0.0525 1.00 pCi/g 0.0441 +/-0.0567 1.00 pCi/g HAKB 09/22/16 1000 1596408 3 0.0369 +/-0.324 1.00 pCi/g 0.0287 +/-0.104 1.00 pCi/g 0.033 +/-0.318 1.00 pCi/g 0.210 +/-0.405 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.253 +/-0.911 1.00 pCi/g HAKB 09/27/16 1712 1596407 5 0.0877 +/-0.310 1.00 pCi/g 0.124 +/-0.465 1.00 pCi/g 0.0617 +/-0.484 1.00 pCi/g 0.0189 +/-0.0797 1.00 pCi/g HAKB 09/22/16 0956 1596410 .6 0.00 +/-0.162 1.00 pCi/g 0.00 +/-0.0657 1.00 pCi/g 0.0216 +/-0.105 1.00 pCi/g 5.12 +/-6.12 15.0 pCi/g HAKB 09/23/16 1527 1596414 7 0.298 +/-0.395 1.00 pCi/g MJHl 09/28/16 1334 1598647 8 0.155 +!-0.192 pCi/g MXRl 10/03/16 0656 1596252 9 0.0811 +/-0.0859 pCi/g 0.337 t/-0.689 pCi/g 0.0376 +/-0.138 pCi/g 0.0216 +/-0.0536 0.100 pCi/g 0.0216 +/-0.0216 pCi/g 0.0699 +/-0.118 pCi/g 0.0355 +/-0.126 pCi/g 0.0419 +/-0.171 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.2.4 Sample ID: 405235043 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.6 +/-1.43 Protactinium-231 HUlh 0.00 +/-0.611 Radium-226 Hh 0.703 +/-0.135 Radium-228 Hh 0.685 +/-0.232 Thallium-208 Hh 0.298 +/-0.072 Tin-126 HU!h 0.00 +/-0.121 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 11.7 +/-3.97 Beta Hh 20.6 +/-2.63 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -1.14 +/-0.912 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.554 +/-2.33 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.202 +/-0.670 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 Hh 1.57 +/-1.69 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.443 0.580 0.0873 0.216 0.047 0.113 4.35 2.17 1.86 4.00 J.15 2.84 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 230 of 5809 0.171 +/-1.60 pCi/g 0.260 +/-0.635 pCi/g 0.0376 +/-0.138 pCi/g 0.0936 +/-0.234 pCi/g 0.0204 +/-0.0731 pCi/g 0.0528 +/-0.122 pCi/g 1.81 +/-4.58 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 0.981 +/-3.92 10.0 pCi/g 0.857 +/-0.912 2.00 pCi/g KSDI 09/22/16 1721 1597803 II 1.94 +/-2.33 6.00 pCi/g TXP3 09/24/16 0209 1598092 12 0.566 +/-0.670 2.00 pCi/g TICJI 09/26/16 1857 1598081 13 1.34 +/-1.70 5.00 pCi/g CXS7 09/20/16 1411 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.2.4 Sample ID: 405235043 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 20 I 6 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 231 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 88.8 (15%-125%) 1596408 86.3 (15%-125%) 1596408 89.3 (15%-125%) 1596411 98.3 (15%-125%) 1596407 91.l (15%-125%) 1596410 75.5 (15%-125%) 1596414 88.7 (15%-125%) 1597803 96.4 (25%-125%) 1597414 95.3 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.4.2 Sample ID: 405235044 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 24.8% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 24.8 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00373 +/-0.0544 0.117 Plutonium-239/240 HUh 0.0197 +/-0.0761 0.131 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0071 +/-0.0496 0.120 Uranium-233/234 Hh 0.934 +/-0.328 0.180 Uranium-235/236 Hh 0.130 +/-0.137 0.147 Uranium-238 Hh 0.881 +/-0.318 0.173 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0595 +/-0.421 0.848 Alphaspec Th229 + 228,230,232 Solid Dry Weight Corrected" Thorium-228 Hh 1.80 +/-0.674 0.463 Thorium-229 Hh 0.214 +/-0.237 0.312 Thorium-230 Hh 0.924 +/-0.421 0.312 Thorium-232 Hh 0.787 +/-0.380 0.212 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0132 +/-0.0625 0.158 Curium-242 HUh -0.0148 +/-0.147 0.334 Curium-243/244 Hh 0.00 +/-0.042 0.063 Curium-245/246 Hh 0.0661 +/-0.0936 0.110 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.67 +/-7.16 12.4 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.014 +/-0.327 0.751 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0362 +/-0.246 0.465 Antimony-125 HUh 0.0844 +/-0.127 0.256 Bismuth-212 HUih 0.00 +/-0.768 . 1.62 Bismuth-214 Hh 1.05 +/-0.201 0.152 Cesium-137 Hh 0.311 +/-0.106 0.0782 Cobalt-60 HUh -0.0134 +/-0.0451 0.0859 Europium-154 HUh 0.00237 +/-0.120 0.244 Lead-212 Hh 1.16 +/-0.142 0.100 Lead-214 Hh 1.13 +/-0.209 0.150 Page 232 of 5809 Report Date: October 4, 2016 Project: MJWCOO 115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYT! 09/08/16 0827 1596233 1 0.0177 +/-0.0546 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0249 +/-0.0763 1.00 pCi/g 0.0232 +/-0.0499 1.00 pCi/g HAKB 09/22/16 1000 1596408 3 0.0475 +/-0.382 1.00 pCi/g 0.0312 +/-0.139 1.00 pCi/g 0.044 +/-0.368 1.00 pCi/g 0.201 +/-0.422 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.142 +/-0.723 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.0894 +/-0.239 1.00 pCi/g 0.0892 +/-0.441 1.00 pCi/g 0.0398 +/-0.396 1.00 pCi/g 0.0478 +/-0.0626 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.0589 +/-0.148 1.00 pCi/g 0.00 +/-0.0421 1.00 pCi/g 0.0193 +/-0.0941 1.00 pCi/g 6.05 +/-7.16 15.0 pCi/g HAKB 09/23/16 1629 1596414 7 0.273 +/-0.327 1.00 pCi/g MJHl 09/28/16 1335 1598647 8 0.214 +/-0.246 pCi/g MXRl 10/0J/16 0656 1596252 9 0.117 +/-0.132 pCi/g 0.748 +/-0.933 pCi/g 0.0681 +/-0.206 pCi/g 0.0346 +/-0.107 0.100 pCi/g 0.0357 +/-0.0455 pCi/g 0.103 +/-0.120 pCi/g 0.0462 +/-0.155 pCi/g 0.0686 +/-0.214 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.4.2 Sample ID: 405235044 Parameter Qualifier Result Uncertainty Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.3 +/-1.67 Protactinium-231 HU!h 0.00 +/-0.493 Radium-226 Hh 1.05 +/-0.201 Radium-228 Thallium-208 Tin-126 Hh Hh HUih 1.09 +/-0.392 0.319 +/-0.0938 0.00 +/-0.117 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 13.6 +/-3.67 Beta Hh 23.3 +/-3.D4 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.0758 +/-0.786 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.256 +/-2.75 Liquid Scint C/4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.122 +/-0.737 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.319 +/-1.96 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-0 I Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R MDC 0.451 0.974 0.152 0.264 0.0767 0.211 3.96 3.43 1.45 4.74 1.27 3.44 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP50 I Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 233 of 5809 Report Date: Project: MJWC00115 Client ID: MJWCOOI Le TPU RL Units PF DF Analyst 0.160 +/-1.85 pCi/g 0.450 +/-0.571 pCi/g , 0.0681 +/-0.206 pCi/g 0.113 +/-0.396 pCi/g 0.0343 +/-0.0948 pCi/g 0.101 +/-0.138 pCi/g 1.72 +/-4.54 4.00 pCi/g JXC9 1.63 +/-4.50 10.0 pCi/g 0.652 +/-0.786 2.00 pCi/g KSDI 2.30 +/-2.75 6.00 pCi/g TXP3 0.621 +/-0.737 2.00 pCi/g TXJI 1.63 +/-1.96 5.00 pCi/g CXS7 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 October 4, 2016 Date Time Batch Mtd. 09/28/16 1448 1602427 10 09/23/16 1327 1597803 II 09/24/16 0352 1598092 12 09/26/16 2009 1598081 13 09120116 1428 1597414 14 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.4.2 Sample ID: 405235044 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 'f.racer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Sein! Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 234 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 75 (15%-125%) 1596408 76.9 (15%-125%) 1596408 98.2 (15%-125%) 1596411 93 (15%-125%) 1596407 103 (15%-125%) 1596410 88.8 (15%-125%) 1596414 75 (15%-125%) 1597803 92.3 (25%-125%) 1597414 96.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.5.2 Sample ID: 405235045 Matrix: Soil Collect Date: 30-NOV-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 22.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 22.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutoniurn-238 Hh 0.0245 +l-0.0796 0.122 Plutonium-239/240 HUh 0.00119 +/-0.0812 0.182 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0347 +/-0.0839 0.251 Uranium-233/234 Hh 0.893 +/-0.321 0.167 Uranium-235/236 Hh 0.082 +/-0. I 13 0.122 Uranium-238 Hh 0.937 +/-0.326 0.122 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.00579 +/-0.414 0.929 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.88 +/-0.876 0.569 Thorium-229 HUh 0.0407 +/-0.263 0.538 Thorium-230 Hh 0.726 +/-0.473 0.218 Thoriurn-232 Hh 0.778 +/-0.493 0.347 Am241, Cm Solid "Dry Weight Corrected" Americium-24 I HUh 0.0126 +/-0.061 0.113 Curium-242 Hh 0.00 +/-0.149 0.223 Curium-243/244 HUh 0.0128 +/-0.0619 0.115 Curium-245/246 Hh 0.0244 +/-0.0684 0.0732 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutoniurn-241 HUh -1.17 +/-7.47 12.9 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0136 +/-0.241 0.687 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.151 +/-0.326 0.528 Antimony-125 HUh 0.0292 +/-0.128 0.251 . Bismuth-212 HUh 0.616 +/-0.826 1.65 Bismuth-214 Hh 0.712 +/-0.279 0.191 Cesium-137 Hh 0.880 +/-0.160 0.0938 Cobalt-60 HUh 0.0326 +/-0.0533 0.120 Europium-154 HUh 0.112 +/-0.145 0.332 Lead-212 Hh 0.991 +/-0.169 0.137 Lead-214 Hh 1.16 +/-0.281 0.146 Page 235 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.0185 +/-0.0797 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0485 +/-0.0814 1.00 pCi/g 0.0656 +/-0.0844 1.00 pCi/g HAKB 09/22/16 1000 1596408 3 0.0406 +/-0.378 1.00 pCi/g 0.0182 +/-0.114 1.00 pCi/g 0.0182 +/-0.387 1.00 pCi/g 0.247 +/-0.415 1.00 pCi/g HAKB 09/22/16 1555 159641 I 4 0.139 +/-0.927 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.160 +/-0.263 1.00 pCi/g 0.00 +/-0.487 1.00 pCi/g 0.0649 +/-0.509 1.00 pCi/g 0.0247 +/-0.061 I 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.149 1.00 pCi/g 0.0251 +/-0.062 1.00 pCi/g 0.00 +/-0.0685 1.00 pCi/g 6.30 +/-7.47 15.0 pCi/g HAKB 09/23/16 1730 1596414 7 0.217 +/-0.241 1.00 pCi/g Mllil 09/28/16 1335 1598647 8 0.243 +/-0.334 pCi/g MXRl 10/03/16 0657 1596252 9 0.113 +/-0.129 pCi/g 0.752 +/-0.872 pCi/g 0.0865 +/-0.281 pCi/g 0.0415 +/-0.164 0.100 pCi/g 0.0509 +/-0.0553 pCi/g 0.142 +/-0.154 pCi/g 0.0642 +/-0.177 pCi/g 0.0657 +/-0.285 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.5.2 Sample ID: 405235045 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dry Weight Corrected" Potassium-40 Hh 12.5 +/-1.76 Protactinium-231 HUih 0.00 +/-0.622 Radium-226 Hh 0.712 +/-0.279 Radium-228 Hh 1.02 +/-0.490 Thallium-208 Hh 0.420 +/-0.139 Tin-126 HU!h 0.00 +/-0.123 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 15.6 +/-3.57 Beta Hh 20.5 +/-2.55 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 0.742 +/-0.723 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.969 +/-2.54 Liquid Scint CJ4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.104 +/-0.745 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.206 +/-1.72 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-OI Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.966 1.25 0.191 0.375 0.086 0.127 3.94 2.83 1.17 4.46 1.28 3.04 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified BP A 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 236 of 5809 0.402 +/-1.88 pCi/g 0.581 +/-0.720 pCi/g 0.0865 +/-0.281 pCi/g 0.165 +/-0.492 pCi/g 0.0382 +/-0.140 pCi/g 0.0601 +/-0.124 pCi/g 1.76 +/-4.60 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.34 +/-3.71 10.0 pCi/g 0.495 +/-0.737 2.00 pCi/g KSDI 09/22/16 1720 1597803 II 2.16 +/-2.54 6.00 pCi/g TXP3 09/24/16 0536 1598092 12 0.627 +/-0.745 2.00 pCi/g TXJI 09/26/16 2120 1598081 13 1.43 +/-1.72 5.00 pCi/g CXS7 09/20/16 1444 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.4D.R.5.2 Sample ID: 405235045 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np23 7, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 237 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 73 (15%-125%) 1596408 77.2 (15%-125%) 1596408 61.4 (15%-125%) 1596411 91.5 (15%-125%) 1596407 97.l (15%-125%) 1596410 80.l (15%-125%) 1596414 73 (15%-125%) 1597803 91 (25%-125%) 1597414 98.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5A.R. l .3 Sample ID: 405235046 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 18.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 18.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0146 +/-0.0701 0.130 Plutonium-239/240 HUh -0.017 +/-0.051 0.146 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0142 +/-0.0962 0.192 Uranium-233/234 Hh 0.645 +/-0.264 0.146 Uranium-235/236 Hh 0.0459 +/-0.0905 0.127 Uranium-238 Hh 0.787 +/-0.288 0.113 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0797 +/-0.432 0.829 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.10 +/-0.640 0.585 Thorium-229 Hh 0.139 +/-0.246 0.372 Thorium-230 Hh 0.914 +/-0.496 0.401 Thorium-232 Hh 0.485 +/-0.358 0.182 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0228 +/-0.0574 0.096 Curium-242 Hh 0.00 +/-0.112 0.167 Curium-243/244 HUh -0.00342 +/-0.0341 0.0774 Curium-245/246 Hh 0.0188 +/-0.0527 0.0565 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -2.2 +/-6.79 11.8 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.129 +/-0.253 0.239 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.145 +/-0.200 0.415 Antimony-125 HUh -0.00584 +/-0.0839 0.163 Bismuth-212 Hh 1.05 +/-0.648 . 0.631 Bismuth-214 Hh 0.887 +/-0.149 0.0852 Cesium-137 Hh 0.162 +/-0.065 0.0542 Cobalt-60 HUh 0.0143 +/-0.0303 0.0676 Europium-154 HUh -0.0604 +/-0.105 0.189 Lead-212 Hh 1.02 +/-0.115 0.0793 Lead-214 Hh 0.940 +/-0.153 0.107 Page 238 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst

Date Time Batch Mtd. percent L YT! 09/08/16 0827 1596233 I O.Q28 +/-0.0703 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0359 +/-0.0512 1.00 pCi/g 0.0453 +/-0.0965 1.00 pCi/g HAKB 09/22/16 1000 1596408 3 0.0336 +/-0.298 1.00 pCi/g 0.0238 +/-0.0911 1.00 pCi/g 0.0168 +/-0.333. 1.00 pCi/g 0.185 +/-0.433 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.171 +/-0.665 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.0947 +/-0.247 1.00 pCi/g 0.109 +/-0.516 1.00 pCi/g 0.00 +/-0.366 1.00 pCi/g 0.0233 +/-0.0575 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.112 1.00 pCi/g 0.0136 +/-0.0342 1.00 pCi/g 0.00 +/-0.0528 1.00 pCi/g 5.75 +/-6.79 15.0 pCi/g HAKB 09/23/16 1831 1596414 7 0.00 +/-0.260 1.00 pCi/g MJHI 09/28/16 1336 1598647 8 0.194 +/-0.212 pCi/g MxRI 10/03/16 0657 1596252 9 0.0733 +/-0.0839 pCi/g 0.272 +/-0.650 pCi/g 0.037 +/-0.153 pCi/g 0.0239 +/-0.0654 0.100 pCi/g 0.0287 +/-0.031 pCi/g 0.0807 +/-0.108 pCi/g 0.0368 +/-0.127 pCi/g 0.0487 +/-0.158 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5A.R. l.3 Sample ID: 405235046 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.7 +/-1.31 Protactinium-231 HUlh 0.00 +/-0.859 Radium-226 Hh 0.887 +/-0.149 Radium-228 Hh I.I I +/-0.270 Thallium-208 Hh 0.271 +/-0.0819 Tin-126 HUlh 0.00 +/-0.106 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 15.1 +/-3.64 Beta Hh 20.9 +/-2.48 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.382 +/-0.657 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.29 +/-2.45 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.182 +l-0.690 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 Hh 2.30 +/-1.90 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.515 0.652 0.0852 0.183 0.0502 0.123 3.95 2.50 1.16 4.16 1.17 3.13 2 3 4 5 6 7 8 9 IO II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 239 of 5809 0.211 +/-1.47 pCi/g 0.299 +/-0.881 pCi/g 0.037 +/-0.153 pCi/g 0.0781 +/-0.276 pCi/g 0.0222 +/-0.0827 pCi/g 0.0589 +/-0.108 pCi/g 1.75 +/-4.66 4.00 pCi/g JXC9 09/28/16 1448 1602427 IO 1.17 +/-3.88 10.0 pCi/g 0.500 +/-0.660 2.00 pCi/g KSDI 09/22/16 1720 1597803 II 2.02 +/-2.45 6.00 pCi/g TXP3 09/24/16 0719 1598092 12 0.576 +/-0.690 2.00 pCi/g TXJI 09/26/16 2232 1598081 13 1.48 +/-1.92 5.00 pCi/g CXS7 09/20/16 1501 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5A.R. l .3 Sample ID: 405235046 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOO l October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 240 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 77 (15%-125%) 1596408 79.8 (15%-125%) 1596408 69.5 (15%-125%) 1596411 82.9 (15%-125%) 1596407 96.1 (15%-125%) 1596410 106 (15%-125%) 1596414 77 (15%-125%) 1597803 93.7 (25%-125%) 1597414 95.l (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5A.R. l .4 Sample ID: 405235047 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 20.7% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 20.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh -0.00389 +/-0.0565 0.122 Plutonium-239/240 HUh -0.00773 +/-0.0566 0.136 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00909 +/-0.0632 0.153 Uranium-233/234 Hh 0.785 +/-0.284 0.154 Uranium-235/236 Hh 0.069 +/-0.0995 0.121 Uranium-238 Hh 1.05 +/-0.323 0.121 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.118 +/-0.291 0.872 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.16 +/-0.676 0.613 Thorium-229 HUh 0.085 +/-0.267 0.499 Thorium-230 Hh 0.758 +/-0.477 0.450 Thorium-232 Hh 0.704 +/-0.436 0.192 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0135 +/-0.0356 0.104 Curium-242 Hh 0.00 +/-0.112 0.168 Curium-243/244 HUh -0.0103 +/-0.0355 0.0978 Curium-245/246 Hh 0.0189 +/-0.0529 0.0567 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.679 +/-7.35 12.7 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.208 +/-0.187 0.517 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.169 +/-0.200 0:398 Antimony-125 HUh -0.00121 +/-0.0854 0.169 Bismuth-212 HU!h 0.00 +/-0.576 1.16 Bismuth-214 Hh 0.882 +/-0.197 0.120 Cesium-137 HU!h 0.00 +/-0.039 0.0849 Cobalt-60 HUh 0.0341 +/-0.0453 0.0926 Europium-154 HUh 0.0428 +/-0.112 0.234 Lead-212 Hh 1.08 +/-0.121 0.0919 Lead-214 Hh 1.07 +/-0.185 0.120 Page 241 of 5809 Project: Client ID: Le TPU RL Units percent 0.0184 +/-0.0567 1.00 pCi/g 0.0259 +/-0.0569 1.00 pCi/g 0.0297 +/-0.0635 1.00 pCi/g 0.0393 +/-0.327 1.00 pCi/g 0.0227 +/-0.101 1.00 pCi/g 0.0227 +/-0.390 1.00 pCi/g 0.225 +/-0.292 1.00 pCi/g 0.178 +/-0.704 1.00 pCi/g 0.153 +/-0.267 1.00 pCi/g 0.129 +/-0.493 1.00 pCi/g 0.00 +/-0.451 1.00 pCi/g 0.027 +/-0.0357 1.00 pCi/g 0.00 +/-0.112 1.00 pCi/g 0.0237 +/-0.0356 1.00 pCi/g 0.00 +/-0.053 1.00 pCi/g 6.19 +/-7.35 15.0 pCi/g 0.211 +/-0.210 1.00 pCi/g 0.185 +/-0.215 pCi/g 0.0756 +/-0.0854 pCi/g 0.529 +/-0.845 pCi/g 0.0535 +/-0.201 pCi/g 0.0388 +/-0.046 0.100 pCi/g 0.0402 +/-0.0479 pCi/g 0.101 +/-0.113 pCi/g 0.043 +/-0.134 pCi/g 0.0551 +/-0.190 pCi/g Report Date: MJWC00115 MJWCOOl October 4, 2016 PF DF Analyst Date Time *Batch Mtd. LYTI 09/08/16 0827 1596233 1 HAKB 09/22/16 0956 1596412 2 HAKB 09/22/16 1000 1596408 3 HAKB 09/22/16 1555 1596411 4 HAKB 09/22/16 0957 1596407 5 HAKB 09/22/16 0956 1596410 6 HAKB 09/23/16 1932 1596414 7 MJHl 09/28/16 1439 1598647 8 MXRl 10/03/!6 0700 1596252 9 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5A.R. l .4 Sample ID: 405235047 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 16.0 +/-1.57

Protactinium-231 HUih 0.00 +/-0.679 Radium-226 Hh 0.882 +/-0.197 Radium-228 Hh 0.886 +/-0.322 Thallium-208 Hh 0.267 +/-0.0818 Tin-126 HUih 0.00 +/-0.133 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.1 +/-3.83 Beta Hh 16.5 +/-2.64 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh -0.744 +/-0.917 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.418 +/-2.59 Liquid Sein! CJ4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.334 +/-0.725 Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.454 +/-1.77 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.429 0.669 0.120 0.247 0.069 0.0664 3.93 3.34 1.78 4.52 1.25 3.10 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 7110B Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 242 of 5809 0.159 +/-1.78 pCi/g 0.305 +/-0.712 pCi/g 0.0535 +/-0.201 pCi/g 0.108 +/-0.325 pCi/g 0.0313 +/-0.0826 pCi/g 0.0311 +/-0.135 pCi/g 1.71 +/-4.93 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.60 +/-3.61 10.0 pCi/g 0.825 +/-0.917 2.00 pCi/g KSDI 09/22/16 1721 1597803 11 2.19 +/-2.59 6.00 pCi/g TXP3 09/24/16 0903 1598092 12 0.614 +/-0.725 2.00 pCi/g TXJI 09/26/16 2344 1598081 13 1.47 +/-1.77 5.00 pCi/g CXS7 09/20/16 1517 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5A.R.l.4 Sample ID: 405235047 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 243 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 76.4 (15%-125%) 1596408 78.5 (15%-125%) 1596408 74.3 (15%-125%) 1596411 90 (15%-125%) 1596407 89.4 (15%-125%) 1596410 103 (15%-125%) 1596414 76.4 (15%-125%) 1597803 91 (25%-125%) 1597414 92.6 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 * (843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.1.2 Sample ID: 405235048 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 22.9% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture .As Received" Moisture 22.9 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00333 +/-0.0483 0.104 Plutonium-239/240 Hh 0.0448 +/-0.0822 0.103 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0357 +/-0.0658 0.209 Uranium-233/234 Hh 0.933 +/-0.322 0.146 Uranium-235/236 Hh 0.0442 +/-0.0957 0.146 Uranium-238 Hh 0.866 +/-0.313 0.172 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.125 +/-0.308 0.921 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.76 +/-0.896 0.704 Thorium-229 Hh 0.399 +/-0.449 0.634 Thorium-230 Hh 0.846 +/-0.561 0.550 Thorium-232 Hh 1.29 +/-0.653 0.433 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.023 +/-0.0846 0.142 Curium-242 HUh -0.0123 +/-0.204 0.431 Curium-243/244 Hh 0.0772 +/-0.121 0.166 Curium-245/246 HUh -0.00414 +/-0.0687 0.145 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.19 +/-6.48 11.2 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0758 +/-0.343 0.674 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.027 +/-0.250 0.472 Antimony-125 HU!h 0.00 +/-0.223 0.245 Bismuth-212 HU!h 0.00 +/-0.708 1.29 Bismuth-214 Hh 0.974 +/-0.193 0.139 Cesium-137 Hh 1.52 +/-0.161 0.0695 Cobalt-60 HUh 0.0124 +/-0.0388 0.0825 Europium-154 HUh 0.0899 +/-0.120 0.263 Lead-212 Hh 1.16 +/-0.142 0.114 Lead-214 Hh 1.36 +/-0.222 0.360 Page 244of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 1 0.0157 +/-0.0485 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0157 +/-0.0825 1.00 pCi/g 0.0583 +/-0.0661 1.00 pCi/g HAKB 09/22/16 1002 1596408 3 0.0313 +/-0.379 1.00 pCi/g 0.0314 +/-0.0962 1.00 pCi/g 0.0442 +/-0.364 1.00 pCi/g 0.237 +/-0.308 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.196 +/-0.945 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.199 +/-0.454 1.00 pCi/g 0.157 +/-0.578 1.00 pCi/g 0.0991 +/-0.687 1.00 pCi/g 0.0258 +/-0.0848 1.00 pCi/g HAKB 09/22/16 1614 1596410 6 0.0617 +/-0.204 1.00 pCi/g 0.037 +/-0.122 1.00 pCi/g 0.0208 +/-0.0689 1.00 pCi/g 5.47 +/-6.48 15.0 pCi/g HAKB 09/23/16 2033 1596414 7 0.261 +/-0.345 1.00 pCi/g MJHl 09/28/16 1440 1598647 8 0.219 +/-0.250 pCi/g MXRl 10/03/16 0700 1596252 9 0.113 +/-0.237 pCi/g 0.590 +/-0.875 pCi/g 0.0623 +/-0.198 pCi/g 0.0307 +/-0.174 0.100 pCi/g 0.0348 +/-0.0392 pCi/g 0.115 +/-0.126 pCi/g 0.0534 +/-0.155 pCi/g 0.174 +/-0.229 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.1.2 Sample ID: 405235048 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 16.4 +/-1.65 Protactinium-231 HUh 0.195 +/-0.533 Radium-226 Hh 0.974 +/-0.193 Radium-228 Hh 1.07 +/-0.364 Thallium-208 Hh 0.366 +/-0.0776 Tin-126 HU!h 0.00 +/-0.198 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid Dry Weight Corrected" Alpha Hh 24.1 +l-5.05 Beta Hh 27.2 +/-3.07 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.194 +/-0.617 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -o.411 +/-2.59 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.209 +/-0.770 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.72 +/-1.81 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,l-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.666 1.03 0.139 0.274 0.0727 0.159 3.94 2.35 1.13 4.52 1.33 3.41 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 245 of 5809 0.275 +/-1.86 pCi/g 0.481 +/-0.542 pCi/g 0.0623 +/-0.198 pCi/g 0.121 +/-0.368 pCi/g 0.0327 +/-0.0792 pCi/g 0.0757 +/-0.198 pCi/g 1.63 +/-6.80 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.07 +/-4.63 10.0 pCi/g 0.492 +/-0.618 2.00 pCi/g KSDI 09/22/16 1720 1597803 11 2.19 +/-2.59 6.00 pCi/g TXP3 09/24/16 I 046 1598092 12 0.650 +/-0.770 2.00 pCi/g TXJI 09/27/16 0207 1598081 13 1.61 +/-1.81 5.00 pCi/g CXS7 09/20/16 1534 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R. l .2 Sample ID: 405235048 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 246 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 83.1 (15%-125%) 1596408 95.1 (15%-125%) 1596408 88.8 (15%-125%) 1596411 91.8 (15%-125%) 1596407 83.9 (15%-125%) 1596410 100 (15%-125%) 1596414 83.l (15%-125%) 1597803 92.3 (25%-125%) 1597414 92.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R. l.3 Sample ID: 405235049 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 18.8% Parameter Qualifier Result Uncertainty , MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 18.8 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh -0.00337 +/-0.0486 0.105 Plutonium-239/240 Hh 0.0208 +/-0.0676 0.104 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0105 +/-0.0491 0.128 Uranium-233/234 Hh 0.773 +/-0.290 0.186 Uranium-235/236 HUh 0.0118 +/-0.0743 0.147 Uranium-238 Hh 0.746 +/-0.281 0.137 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0222 +/-0.369 0.780 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.44 +/-0.870 0.907 Thorium-229 HUh 0.0416 +/-0.231 0.443 Thorium-230 Hh 1.04 +/-0.586 0.239 Thorium-232 Hh 1.11 +/-0.605 0.239 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0565 +/-0.110 0.151 Curium-242 Hh 0.00 +/-0.215 0.326 Curium-243/244 HUh -0.0117 +/-0.0656 0.166 Curium-245/246 Hh 0.0367 +/-0.102 0.110 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 Hh 6.62 +l-6.96 11.7 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.00955 +/-0.223 0.511 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0667 0.394 Antimony-125 HUh 0.00107 +l-0.0965 0.183 Bismuth-212 HUih 0.00 +/-0.839 1.35 Bismuth-214 Hh I.I I +/-0.183 0.109 Cesium-137 Hh 0.481 +/-0.0908 0.0735 Cobalt-60 HUh 6.07E-05 +/-0.0306 0.059 Europium-154 HUh 0.0647 +/-0.111 0.246 Lead-212 Hh 1.06 +/-0.134 0.100 Lead-214 Hh 0.911 +/-0.179 0.132 Page 247 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.0159 +/-0.0487 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0158 +/-0.0678 1.00 pCi/g 0.028 +/-0.0493 1.00 pCi/g HAKB 09122116 1002 1596408 3 0.0538 +/-0.330 1.00 pCi/g 0.0341 +/-0.0745 1.00 pCi/g 0.0294 +/-0.319 1.00 pCi/g 0.112 +l-0.369 1.00 pCi/g HAKB 09122116 1555 1596411 4 0.294 +/-0.913 1.00 pCi/g HAKB 09126116 1201 1596407 5 0.101 +/-0.231 1.00 pCi/g 0.00 +/-0.614 1.00 pCi/g 0.00 +/-0.636 1.00 pCi/g 0.0274 +/-0.110 1.00 pCi/g HAKB 09/22/16 1614 1596410 6 0.00 +/-0.216 1.00 pCi/g 0.034 +/-0.0659 1.00 pCi/g 0.00 +/-0.102 1.00 pCi/g 5.68 +/-7.13 15.0 pCi/g HAKB 09/23/16 2134 1596414 7 0.186 +/-0.223 1.00 pCi/g MJHI 09/28/16 1440 1598647 8 0.180 +/-0.210 pCi/g MXRI 10103116 0701 1596252 9 0.0819 +/-0.0965 pCi/g 0.623 +/-1.05 pCi/g 0.0477 +/-0.189 pCi/g 0.0327 +/-0.0931 0.100 pCi/g 0.0232 +/-0.0306 pCi/g 0.106 +/-0.115 pCi/g 0.0466 +/-0.145 pCi/g 0.060 +/-0.183 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.SB.R.1.3 Sample ID: 405235049 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.l +/-1.48 Protactinium-231 HUlh 0.00 +/-0.921 Radium-226 Hh I.I I +/-0.183 Radium-228 Hh 1.05 +/-0.289 Thallium-208 Hh 0.323 +/-0.0861 Tin-126 HUlh 0.00 +/-0.211 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 27.8 +/-5.44 Beta Hh 21.9 +/-2.68 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.132 +/-0.636 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.551 +/-2.55 Liquid Scint CJ4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.593 +/-0.721 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.0409 +/-1.78 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.503 0.654 0.109 0.202 0.0606 0.143 3.93 2.19 1.26 4.45 1.25 3.17 2 3 4 5 6 7 8 9 IO II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 248 of 5809 0.194 +/-1.63 pCi/g 0.293 +/-0.957 pCi/g 0.0477 +/-0.189 pCi/g 0.0848 +/-0.294 pCi/g 0.0267 +/-0.0871 pCi/g 0.0673 +/-0.211 pCi/g 1.60 +/-7.72 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.00 +/-4.43 10.0 pCi/g 0.552 +/-0.636 2.00 pCi/g KSDI 09/22/16 1720 1597803 II 2.16 +/-2.55 6.00 pCi/g TXP3 09/24/16 1230 1598092 12 0.615 +/-0.721 2.00 pCi/g TXJI 09/27/16 0319 1598081 13 1.50 +/-1.78 5.00 pCi/g CXS7 09/20/16 1550 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.SB.R. l .3 Sample ID: 405235049 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 249 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 79.6 (15%-125%) 1596408 101 (15%-125%) 1596408 98.2 (15%-125%) 1596411 73.9 (15%-125%) 1596407 71.9 (15%-125%) 1596410 94.8 (15%-125%) 1596414 79.6 (15%-125%) 1597803 93.7 (25%-125%) 1597414 95.2 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R. l .4 Sample ID: 405235050 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 11 % Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 11.0 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid Dry Weight Corrected" Plutonium-238 HUh -0.00592 +/-0.0431 0.104 Plutonium-239/240 HUh -0.0118 +/-0.0436 0.119 ASP Uranium Isotopic, Solid Dry Weight Corrected" Uranium-232 HUh 0.00617 +/-0.064 0.134 Uranium-233/234 Hh 0.565 +/-0.240 0.151 Uranium-235/236 HUh 0.0178 +/-0.0688 0.118 Uranium-238 Hh 0.652 +/-0.253 0.118 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0372 +/-0.310 0.729 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.60 +/-0.922 0.967 Thorium-229 Hh 0.442 +/-0.420 0.444 Thorium-230 Hh 0.764 +/-0.552 0.591 Thorium-232 Hh 0.618 +/-0.471 0.382 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0554 +/-0.108 0.148 Curium-242 HUh -0.0128 +/-0.212 0.449 Curium-243/244 HUh 0.0204 +/-0.0897 0.162 Curium-245/246 Hh 0.00 +/-0.071 0.108 Liquid Sein! Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh 2.12 +/-6.17 10.5 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0874 +/-0.171 0.277 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.132 +/-0.242 0.393 Antimony-125 HU!h 0.00 +/-0.245 0.201 Bismuth-212 . HUlh 0.00 +/-0.769 1.42 Bismuth-214 Hh 0.725 +/-0.191 0.120 Cesium-137 HUlh 0.0702 +/-0.0653 0.089 Cobalt-60 HUh -0.0183 +/-0.0338 0.0645 Europium-154 HUh -0.00145 +/-0.132 0.279 Lead-212 Hh 0.801 +/-0.172 0.114 Lead-214 Hh 0.950 +/-0.184 0.336 Page 250 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units

PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0827 1596233 1 0.0197 +/-0.0432 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0277 +/-0.0437 1.00 pCi/g 0.0336 +/-0.0642 1.00 pCi/g HAKB 09/22/16 1002 1596408 3 0.0388 +/-0.264 1.00 pCi/g 0.0225 +/-0.0689 1.00 pCi/g 0.0224 +/-0.284 1.00 pCi/g 0.132 +/-0.311 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.323 +!-0.966 1.00 pCi/g HAKB 09/26/16 1201 1596407 5 0.102 +/-0.427 1.00 pCi/g 0.176 +l-0.565 1.00 pCi/g 0.0715 +/-0.482 1.00 pCi/g 0.0268 +/-0.108 1.00 pCi/g HAKB 09/22/16 1614 1596410 6 0.0643 +/-0.213 1.00 pCi/g 0.0333 +/-0.0899 1.00 pCi/g 0.00 +/-0.0713 1.00 pCi/g 5.13 +/-6.19 15.0 pCi/g HAKB 09/23/16 2235 1596414 7 0.00 +/-0.176 1.00 pCi/g MJHl 09/28/16 1440 1598647 8 0.176 +/-0.249 pCi/g MXRl 10/03/16 0701 1596252 9 0.0876 +/-0.246 pCi/g 0.634 +/-0.896 pCi/g 0.0504 +/-0.193 pCi/g 0.039 +/-0.0654 0.100 pCi/g 0.0228 +/-0.0348 pCi/g 0.115 +/-0.132 pCi/g 0.0529 +/-0.177 pCi/g 0.161 +/-0.188 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.1.4 Sample ID: 405235050 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.6 +/-1.74 Protactinium-231 HUh 0.291 +!-0.505 Radium-226 Hh 0.725 +/-0.191 Radium-228 Hh 1.05 +/-0.340 Thallium-208 Hh 0.232 +/-0.0865 Tin-126 HU!h 0.00 +/-0.143 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 16.6 +/-4.28 Beta Hh 16.3 +/-2.75 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.545 +/-0.687 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -1.75 +/-2.15 Liquid Seint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.264 +/-0.622 Liquid Seint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.438 +/-1.51 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.822 0.960 0.120 0.271 0.0613 0.112 4.00 3.25 1.46 3.83 1.07 2.73 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 251 of 5809 0.325 +/-1.86 pCi/g 0.438 +/-0.526 pCi/g 0.0504 +/-0.193 pCi/g 0.112 +/-0.344 pCi/g 0.0258 +/-0.087 pCi/g 0.0521 +/-0.144 pCi/g 1.66 +/-5.38 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.53 +/-3.62 10.0 pCi/g 0.645 +/-0.687 2.00 pCi/g KSDI 09/22/16 1720 1597803 II 1.86 +/-2.15 6.00 pCi/g TXP3 09/24/16 1414 1598092 12 0.527 +/-0.622 2.00 pCi/g TXJI 09/27/16 0430 1598081 13 1.29 +/-1.51 5.00 pCi/g CXS7 09/20/ 16 1606 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R. l .4 Sample ID: 405235050 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 252 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 88.3 (15%-125%) 1596408 107 (15%-125%) 1596408 104 (15%-125%) 1596411 80.4 (15%-125%) 1596407 90.8 (15%-125%) 1596410 93.3 (15%-125%) 1596414 88.3 (15%-125%) 1597803 95 (25%-125%) 1597414 95.3 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.2.3 Sample ID: 405235051 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 17.7% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 Hh 0.00 +/-0.0523 0.0793 Plutonium-239/240 HUh -0.0146 +/-0.0539 0.147 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0211 +/-0.228 0.434 Uranium-233/234 Hh 0.741 +/-0.301 0.304 Uranium-235/236 Hh 0.134 +/-0.145 0.196 Uranium-238 Hh 0.988 +/-0.311 0.159 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.406 +/-0.736 0.907 Alphaspec_ Th229 + 228,230,232 Solid Dry Weight Corrected" Thorium-228 Hh 1.67 +/-0.803 0.662 Thorium-229 Hh 0.329 +/-0.346 0.431 Thorium-230 Hh 1.32 +/-0.603 0.398 Thorium-232 Hh 1.15 +/-0.557 0.312 Am241, Cm Solid "Dry Weight Corrected" Arnericium-24 I HUh -0.0206 +/-0.0543 0.158 Curium-242 Hh 0.00 +/-0.171 0.256 Curium-243/244 HUh -0.0262 +/-0.056 0.170 Curium-245/246 HUh -0.0059 +/-0.0587 0.133 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 1.43 +/-7.24 12.4 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0898 +/-0.258 0.462 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.00182 +/-0.236 0.412 Antimony-125 HUh -0.0278 +/-0.116 0.214 Bismuth-212 HUlh .0.00 +/-0.984 1.50 Bismuth-214 Hh 0.829 +/-0.210 0.154 Cesium-137 Hh 0.139 +/-0.0833 0.0784 Cobalt-60 HUh 0.0154 +/-0.0408 0.0906 Europium-I 54 HUh -0.0629 +/-0.142 0.255 Lead-212 Hh 0.909 +/-0.149 0.118 Lead-214 Hh 0.956 +/-0.174 0.327 Page 253 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.00 +/-0.0525 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0343 +/-0.0541 1.00 pCi/g 0.191 +/-0.228 1.00 pCi/g KXB2 09/29/16 1404 1601257 3 0.116 +/-0.314 1.00 pCi/g 0.0622 +/-0.146 1.00 pCi/g 0.0438 +/-0.333 1.00 pCi/g 0.130 +/-0.737 1.00 pCi/g HAKB 09/26/16 1151 159641 I 4 0.200 +/-0.854 1.00 pCi/g HAKB 09/26/16 1201 1596407 5 0.117 +/-0.350 1.00 pCi/g 0.101 +/-0.639 1.00 pCi/g 0.0584 +/-0.587 1.00 pCi/g 0.0412 +/-0.0545 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.171 1.00 pCi/g 0.0467 +/-0.0562 1.00 pCi/g 0.0235 +/-0.0589 1.00 pCi/g 6.04 +/-7.25 15.0 pCi/g HAKB 09/23/16 2336 1596414 7 0.119 +/-0.261 1.00 pCi/g MJHl 09/28/16 1441 1598647 8 0.188 +/-0.236 pCi/g MXRI 10/03/16 0704 1596252 9 0.0965 +/-0.117 pCi/g 0.690 +/-1.28 pCi/g 0.0693 +/-0.222 pCi/g 0.0348 +/-0.0841 0.100 pCi/g 0.0376 +/-0.0414 pCi/g 0.107 +/-0.145 pCi/g 0.0552 +/-0.173 pCi/g 0.157 +/-0.192 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.2.3 Sample ID: 405235051 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.0 +/-1.70 Protactinium-231 HU!h 0.00 +/-0.671 Radium-226 Hh 0.829 +/-0.210 Radium-228 HU!h 0.00 +/-0.367 Thallium-208 Hh 0.336 +/-0.0777 Tin-126 HU!h 0.00 +/-0.102 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.7 +/-4.25 Beta Hh 21.1 +/-2.79 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh -0.384 +/-0.664 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.479 +/-2.45 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.322 +/-0.715 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.139 +/-1.73 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.576 0.808 0.154 0.597 0.0658 0.0935 3.99 2.62 1.36 4.27 1.24 3.08 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 254 of 5809 0.218 +/-2.03 pCi/g 0.369 +/-0.683 pCi/g 0.0693 +/-0.222 pCi/g 0.280 +/-0.548 pCi/g 0.029 +/-0.0829 pCi/g 0.0442 +/-0.104 pCi/g 1.67 +/-5.36 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.21 +/-4.19 10.0 pCi/g 0.604 +/-0.664 2.00 pCi/g KSDI 09122116 1720 1597803 11 2.07 +/-2.45 6.00 pCi/g TXP3 09124116 1557 1598092 12 0.606 +/-0.715 2.00 pCi/g TXJl 09/27116 0542 1598081 13 1.46 +/-1.73 5.00 pCi/g CXS7 09/20/16 1623 1597414 14 Analyst Date Time Prep Batch LYTl 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.2.3 Sample ID: 405235051 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 255 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 74.7 (15%-125%) 1601257 89 (15%-125%) 1601257 100 (15%-125%) 1596411 58.2 (15%-125%) 1596407 91.7 (15%-125%) 1596410 70.3 (15%-125%) 1596414 74.7 (15%-125%) 1597803 92.3 (25%-125%) 1597414 95 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.2.4 Sample ID: 405235052 Matrix: Soil Collect Date: 07-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 15.5% Parameter

Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 15.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0204 +/-0.0608 0.174 Plutonium-239/240 HUh -0.0688 +/-0.0663 0.245 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0158 +/-0.056 0.155 Uranium-233/234 Hh 0.900 +/-0.341 0.209 Uranium-235/236 HUh 0.0183 +/-0.0883 0.164 Uranium-238 Hh 0.699 +/-0.300 0.175 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0771 +/-0.262 0.732 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.596 +/-0.665 0.881 Thorium-229 HUh -0.0908 +/-0.210 0.623 Thorium-230 Hh 1.13 +/-0.668 0.283 Thorium-232 Hh 1.27 +/-0.718 0.521 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0184 +/-0.0393 0.119 Curium-242 HUh -0.0124 +/-0.124 0.281 Curium-243/244 HUh -0.00418 +/-0.054 0.127 Curium-245/246 Hh 0.0205 +/-0.0574 0.0614 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 3.66 +/-7.82 13.3 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0439 +/-0.250 0.532 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.137 +/-0.374 0.398 Antimony-125 HUh -0.0333 +/-0.0969 0.185 Bismuth-212 HUih 0.00 +/-1.02 1.23 Bismuth-214 Hh 0.693 +/-0.165 0.131 Cesium-137 Hh 0.148 +/-0.0611 0.063 Cobalt-60 HUh 0.00693 +/-0.0303 0.0673 Europium-154 HUh -0.00356 +/-0.116 0.205 Lead-212 Hh 0.907 +/-0.127 0.0844 Lead-214 Hh 1.03 +/-0.235 0.319 Page 256 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOI Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.0429 +/-0.061 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0786 +/-0.0666 1.00 pCi/g 0.0365 +/-0.0564 1.00 pCi/g HAKB 09/22/16 1002 1596408 3 0.0576 +/-0.393 1.00 pCi/g 0.0354 +/-0.0885 1.00 pCi/g 0.0407 +/-0.336 1.00 pCi/g 0.173 +/-0.263 1.00 pCi/g HAKB 09/22/16 1555 1596411 4 0.252 +/-0.675 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.170 +/-0.211 1.00 pCi/g 0.00 +/-0.702 1.00 pCi/g 0.119 +/-0.758 1.00 pCi/g 0.0328 +/-0.0394 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.0496 +/-0.124 1.00 pCi/g 0.0364 +/-0.054 1.00 pCi/g 0.00 +/-0.0574 1.00 pCi/g 6.48 +/-7.87 15.0 pCi/g HAKB 09/24/16 0038 1596414 7 0.207 +/-0.250 1.00 pCi/g MJHI 09/28/16 1514 1598647 8 0.183 +/-0.380 pCi/g MXRI 10/03/16 0704 1596252 9 0.083 +/-0.0981 pCi/g 0.560 +/-1.06 pCi/g 0.0587 +/-0.168 pCi/g 0.0276 +/-0.0614 0.100 pCi/g 0.0274 +/-0.0305 pCi/g 0.086 +/-0.116 pCi/g 0.0389 +/-0.135 pCi/g 0.154 +/-0.238 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.2.4 Sample ID: 405235052 Parameter Qualifier Result Uncertainty Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.2 +/-1.56 Protactinium-231 HUlh 0.00 +/-0.615 Radium-226 Hh 0.693 +/-0.165 Radium-228 Hh 0.852 +/-0.276 Thallium-208 Hh 0.198 +/-0.0902 Tin-126 HUlh 0.00 +/-0.154 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 17.6 +/-4.06 Beta Hh 20.3 +/-2.72 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 0.896 +/-0.802 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Dry Weight Corrected" Tritium HUh 1.12 +/-2.40 Liquid Scint Cl4, Solid Dry Weight Corrected" Carbon-14 HUh -0.267 +/-0.635 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.295 +/-2.06 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R MDC 0.599 0.677 0.131 0.247 0.0635 0.142 3.95 3.19 1.30 4.10 1.10 3.51 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 257 of 5809 Report Date: Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst 0.243 +/-1.73 pCi/g 0.307 +/-0.623 pCi/g 0.0587 +/-0.168 pCi/g 0.107 +/-0.280 pCi/g 0.0283 +/-0.0906 pCi/g 0.0668 +/-0.154 pCi/g 1.71 +/-5.39 4.00 pCi/g JXC9 1.52 +/-3.95 10.0 pCi/g 0.576 +/-0.817 2.00 pCi/g KSDI 1.99 +/-2.40 6.00 pCi/g TXP3 0.537 +/-0.635 2.00 pCi/g TXJI 1.73 +/-2.06 5.00 pCi/g CXS7 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 October 4, 2016 Date Time Batch Mtd. 09/28/16 1448 1602427 10 09/22/16 1720 1597803 II 09/24/16 1741 1598092 12 09/27/16 0654 1598081 13 09/20/16 1207 1597414 14 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5B.R.2.4 Sample ID: 405235052 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 258 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 68.6 (15%-125%) 1596408 80.2 (15%-125%) 1596408 88.8 (15%-125%) 1596411 93.5 (15%-125%) 1596407 64.3 (15%-125%) 1596410 96.3 (15%-125%) 1596414 68.6 (15%-125%) 1597803 82.8 (25%-125%) 1597414 42.3 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.5.2 Sample ID: 405235053 Matrix: Soil Collect Date: 01-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 30.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 30.4 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0754 +/-0.117 0.177 Plutonium-239/240 HUh 0.00801 +/-0.0923 0.198 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uraniurn-232 HUh -0.000599 +/-0.0904 0.205 Uranium-233/234 Hh 1.16 +/-0.389 0.199 Uraniurn-235/236 Hh 0.221 +/-0.179 0.139 Uraniurn-238 Hh 1.27 +/-0.403 0.169 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.159 +/-0.529 0.978 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thoriurn-228 Hh 2.20 +/-0.918 0.583 Thorium-229 HUh 0.0356 +/-0.198 0.379 Thorium-230 Hh 1.56 +/-0.658 0.328 Thorium-232 Hh 1.41 +/-0.628 0.327 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0133 +/-0.0673 0.172 Curium-242 Hh 0.00 +/-0.225 0.337 Curiurn-243/244 HUh -0.0337 +/-0.0721 0.219 Curiurn-245/246 Hh 0.037 +/-0.104 0.111 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh 2.18 +/-6.84 11.7 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" lodine-129 HUh 0.193 +/-0.507 1.14 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 m.ih 0.194 +/-0.396 0.700 Antimony-125 HUh 0.0321 +/-0.199 0.387 Bismuth-212 HU!h 0.00 +/-1.40 1.62 Bismuth-214 Hh 1.36 +/-0.320 0.249 Cesiurn-137 Hh 0.258 +/-0.150 0.126 Cobalt-60 HUh -0.00448 +/-0.0858 0.168 Europium-154 HUh -0.103 +/-0.237 0.428 Lead-212 Hh 1.55 +/-0.207 0.151 Lead-214 Hh 1.65 +/-0.339 0.606 Page 259 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units *PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0827 1596233 1 0.049 +/-0.118 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0597 +/-0.0924 1.00 pCi/g 0.0557 +i-0.0907 1.00 pCi/g HAKB 09/22/16 1002 1596408 3 0.0514 +/-0.466 1.00 pCi/g 0.021 +/-0.186 1.00 pCi/g 0.0363 +/-0.492 1.00 pCi/g 0.260 +/-0.529 1.00 pCi/g HAKB 09/22/16 1556 1596411 4 0.154 +/-0.984 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.087 +/-0.198 1.00 pCi/g 0.0613 +/-0.702 1.00 pCi/g 0.0612 +/-0.667 1.00 pCi/g 0.0374 +/-0.0676 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.226 1.00 pCi/g 0.0601 +/-0.0723 1.00 pCi/g 0.00 +/-0.104 1.00 pCi/g 5.68 +/-6.85 15.0 pCi/g HAKB 09/24/16 0139 1596414 7 0.465 +/-0.514 1.00 pCi/g MJHl 09/28/16 1514 1598647 8 0.319 +/-0.407 pCi/g MXRl 10/03/16 0706 1596252 9 0.174 +/-0.200 pCi/g 0.704 +/-1.41 pCi/g 0.111 +/-0.325 pCi/g 0.0552 +/-0.150 0.100 pCi/g 0.0707 +/-0.0858 pCi/g 0.179 +/-0.241 pCi/g 0.069 +/-0.223 pCi/g 0.292 +/-0.346 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.5.2 Sample ID: 405235053 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 18.7 +/-2.58 Protactinium-231 HUih 0.00 +/-1.27 Radium-226 Hh 1.36 +/-0.320 Radium-228 Hh 1.36 +/-0.443 Thallium-208 Hh 0.324 +/-0.148 Tin-126 HUih 0.00 +/-0.124 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 17.1 +/-4.24 Beta Hh 26.3 +/-2.91 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.426 +/-0.604 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -1.02 +/-3.28 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.335 +/-0.860 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 1.06 +/-2.16 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASI.:-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300; 4.5.2.3/Ga-Ol-R 0.973 1.25 0.249 0.427 0.113 0.147 3.91 2.30 1.30 5.75 1.46 3.73 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 260 of 5809 0.367 +/-2.76 pCi/g 0.559 +/-1.28 pCi/g 0.111 +/-0.325 pCi/g 0.180 +/-0.448 pCi/g 0.0495 +/-0.149 pCi/g 0.0689 +/-0.125 pCi/g 1.63 +/-5.38 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.05 +/-4.70 10.0 pCi/g 0.566 +/-0.604 2.00 pCi/g KSDI 09/23/16 1136 1597803 11 2.78 +/-3.28 6.00 pCi/g TXP3 09/24/16 1924 1598092 12 0.716 +/-0.860 2.00 pCi/g TXJl 09/27116 0806 1598081 13 1.76 +/-2.17 5.00 pCi/g CXS7 09/20/16 1639 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.5.2 Sample ID: 405235053 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 261of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 83.8 (15%-125%) 1596408 79.7 (15%-125%) 1596408 81.5 (15%-125%) 1596411 88.5 (15%-125%) 1596407 98 (15%-125%) 1596410 57.4 (15%-125%) 1596414 83.8 (15%-125%) 1597803 82.8 (25%-125%) 1597414 96.6 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R. l .3 Sample ID: 405235054 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 18.2% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 18.2 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00714 +l-0.0509 0.123 Plutonium-239/240 HUh -0.0071 +/-0.0506 0.122 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0174 +/-0.0613 0.169 Uranium-233/234 Hh 0.913 +/-0.341 0.184 Uranium-235/236 Hh 0.0851 +/-0.123 0.151 Uranium-238 Hh 0.948 +/-0.346 0.175 Alphaspec Np237, Solid Dry Weight Corrected" Neptunium-237 HUh -0.0119 +/-0.427 0.985 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh I.17 +/-0.728 0.668 Thorium-229 Hh 0.280 +/-0.364 0.517 Thorium-230 Hh I.16 +/-0.596 0.353 Thorium-232 Hh 0.862 +/-0.521 0.352 Am241, Cm Solid "Dry Weight Corrected" Americium-24 I HUh -0.00405 +/-0.0403 0.0916 Curium-242 Hh 0.00 +/-0.137 0.205 Curium-243/244 HUh 0.0159 +/-0.0567 0.093 Curium-245/246 Hh 0.0226 +/-0.0633 0.0678 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -2.03 +/-7.01 12.2 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.138 +/-0.251 0.435 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0501 +/-0.223 0.419 Antimony-125 HUlh 0.00 +/-0.112 0.236 Bismuth-212 HUlh 0.00 +/-0.741 1.51 Bismuth-214 Hh 0.835 +/-0.220 0.121 Cesium-137 HUh -0.00469 +/-0.043 0.0826 Cobalt-60 HUh 0.00992 +/-0.0397 0.0863 Europium-154 HUh 0.035 +/-0.112 0.243 Lead-212 Hh 1.20 +/-0.130 0.0961 Lead-214 Hh 1.1 I +/-0.189 0.346 Page 262 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0827 1596233 1 0.0236 +/-0.0511 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0234 +/-0.0507 1.00 pCi/g 0.040 +/-0.0616 1.00 pCi/g HAKB 09/22/16 1003 1596408 3 0.0454 +/-0.395 1.00 pCi/g 0.0288 +/-0.125 1.00 pCi/g 0.0406 +/-0.403 1.00 pCi/g 0.269 +/-0.427 1.00 pCi/g HAKB 09/22/16 1556 1596411 4 0.186 +/-0.753 1.00 pCi/g HAKB 09/22/16 0957 1596407 5 0.148 +/-0.367 1.00 pCi/g 0.066 +/-0.625 1.00 pCi/g 0.0658 +/-0.539 1.00 pCi/g 0.0162 +/-0.0404 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.137 1.00 pCi/g 0.0164 +/-0.0568 1.00 pCi/g 0.00 +/-0.0634 1.00 pCi/g 5.93 +/-7.01 15.0 pCi/g HAKB 09/24/16 0352 1596414 7 0.138 +/-0.259 1.00 pCi/g MJHl 09/28/16 1514 1598647 8 0.193 +/-0.224 pCi/g MXRl 10/03/16 0707 1596252 '9 0.108 +/-0.124 pCi/g 0.699. +/-I.15 pCi/g 0.0532 +/-0.223 pCi/g 0.037 +/-0.0431 0.100 pCi/g 0.036 +/-0.0399 pCi/g 0.103 +/-0.l 13 pCi/g 0.0446 +/-0.145 pCi/g 0.167 +/-0.195 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.1.3 Sample ID: 405235054 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.5 +/-1.68 Protactinium-231 HUh 0.334 +/-0.456 Radium-226 Hh 0.835 +/-0.220 Radium-228 Hh 1.30 +/-0.285 Thallium-208 Hh 0.338 +/-0.0819 Tin-126 HUih 0.00 +/-0.141 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.3 +/-3.97 Beta Hh 21.8 +/-2.94 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.599 +/-0.569 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.682 +/-2.51 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.502 +/-0.719 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.447 +/-1.80 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC: Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-O I Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.516 0.924 0.121 0.227 0.0772 0.149 3.97 3.45 1.22 4.31 1.25 3.25 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 263 of 5809 0.193 +/-1.86 pCi/g 0.428 +/-0.485 pCi/g 0.0532 +/-0.223 pCi/g 0.0955 +/-0.293 pCi/g 0.0348 +/-0.0832 pCi/g 0.0697 +/-0.141 pCi/g 1.73 +/-5.20 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.64 +/-4.32 10.0 pCi/g 0.547 +/-0.569 2.00 pCi/g KSDl 09/22/16 1720 1597803 II 2.09 +/-2.51 6.00 pCi/g TXP3 09/24/16 2108 1598092 12 0.612 +/-0.719 2.00 pCi/g TXJI 09/27/16 0917 1598081 13 1.54 +/-1.80 5.00 pCi/g CXS7 09/20/16 1656 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R. l .3 Sample ID: 405235054 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic,. Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Arn241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 264of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 76 (15%-125%) 1596408 90.3 (15%-125%) 1596408 82.8 (15%-125%) 1596411 79.7 (15%-125%) 1596407 93.3 (15%-125%) 1596410 88.5 (15%-125%) 1596414 76 (15%-125%) 1597803 92.3 (25%-125%) 1597414 92.6 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.l .4 Sample ID: 405235055 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.3% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 19 .3 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.02 +/-0.0586 0.168 Plutonium-239/240 HUh -0.0157 +/-0.0823 0.207 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0368 +/-0.0549 0.183 Uranium-233/234 Hh 0.707 +/-0.190 0.0889 Uranium-235/236 Uranium-238 Hh Hh 0.0381 0.947 +/-0.0502 0.0381 +/-0.217 0.0608 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0277 +/-0.494 1.07 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.44 +/-0.687 0.554 Thorium-229 Hh 0.267 +/-0.295 0.390 Thorium-230 Hh 0.710 +/-0.426 0.389 Thorium-232 Hh 0.803 +/-0.436 0.306 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.017 +/-0.0605 0.0991 Curium-242 Hh 0.00 +/-0.148 0.222 Curium-243/244 HUh -0.0134 +/-0.046 0.127 Curium-245/246 Hh 0.00 +/-0.0489 0.0733 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 0.440 +/-8.36 14.4 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0833 +/-0.361 0.865 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0469 +/-0.204 0.363 Antimony-125 HUh 0.00308 +/-0.105 0.205 Bismuth-212 HUih 0.00 +/-0.734 1.20 Bismuth-214 Hh 0.785 +/-0.176 0.112 Cesium-137 HUh -0.00211 +/-0.0311 0.0647 Cobalt-60 HUh 0.00585 +/-0.0396 0.0822 Europium-154 HUh -0.0184 +/-0.0824 0.164 Lead-212 Hh 1.14 +/-0.122 0.0856 Lead-214 Hh 1.08 +/-0.203 0.328 Page 265 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le *TPU RL *Units PF DF Analyst Date Time Batch Mtd. percent L YT! 09/08/16 0827 1596233 I 0.0418 +/-0.0588 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0615 +/-0.0825 1.00 pCi/g 0.0537 +/-0.0551 1.00 pCi/g HAKB 09/22/16 1424 1596408 3 0.0254 +/-0.225 1.00 pCi/g 0.00 +l-0.0506 1.00 pCi/g 0.0114 +/-0.270 1.00 pCi/g 0.277 +/-0.495 1.00 pCi/g HAKB 09/22/16 1556 1596411 4 0.166 +/-0.721 1.00 pCi/g HAKB 09/22/16 1344 1596407 5 0.112 +/-0.298 1.00 pCi/g 0.111 +/-0.439 1.00 pCi/g . 0.0702 +/-0.452 1.00 pCi/g 0.0175 +/-0.0606 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.148 1.00 pCi/g 0.0307 +/-0.0461 1.00 pCi/g 0.00 +/-0.049 1.00 pCi/g 7.01 +/-8.36 15.0 pCi/g HAKB 09/24/16 0453 1596414 7 0.273 +/-0.363 1.00 pCi/g MJHI 09/28/16 1515 1598647 8 0.166 +/-0.205 pCi/g MXRI 10/03/16 0718 1596252 9 0.0932 +/-0.105 pCi/g 0.552 +/-0.819 pCi/g 0.0494 +/-0.180 pCi/g 0.0286 +/-0.0311 0.100 pCi/g 0.0352 +/-0.0397 pCi/g 0.0664 +/-0.0828 pCi/g 0.0396 +/-0.137 pCi/g 0.159 +/-0.208 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R. l.4 Sample ID: 405235055 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.7 +/-1.64 Protactinium-231 HU!h 0.00 +/-0.462 Radium-226 Hh 0.785 +/-0.176 Radium-228 Hh 0.951 +/-0.298 Thallium-208 Hh 0.345 +/-0.0764 Tin-126 HUih 0.00 +/-0.138 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 21.1 +/-4.85 Beta Hh 23.3 +/-2.96 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.797 +/-0.573 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.550 +/-2.56 Liquid Scint C 14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.383 +/-0.679 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.234 +/-1.85 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE.EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.753 0.908 0.112 0.199 0.0678 0.100 3.98 2.74 1.24 4.41 1.18 3.26 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 266 of 5809 0.322 +/-1.83 pCi/g 0.423 +/-0.516 pCi/g 0.0494 +/-0.180 pCi/g 0.0844 +/-0.302 pCi/g 0.0306 +/-0.0778 pCi/g 0.047 +/-0.140 pCi/g 1.64 +/-6.48 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.26 +/-4.44 10.0 pCi/g 0.560 +/-0.573 2.00 pCi/g KSDI 09/22/16 1721 1597803 II 2.14 +l-2.56 6.00 pCi/g TXP3 09/24/16 2252 1598092 12 0.577 +/-0.679 2.00 pCi/g TXJI 09/27/16 1029 1598081 13 1.54 +/-1.85 5.00 pCi/g CXS7 09120116 1745 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.l.4 Sample ID: 405235055 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 267 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 64.1 (15%-125%) 1596408 83.6 (15%-125%) 1596408 98.9 (15%-125%) 1596411 79.9 (15%-125%) 1596407 98.8 (15%-125%) 1596410 81.7 (15%-125%) 1596414 64.1 (15%-125%) 1597803 89.6 (25%-125%) 1597414 90 (15%-125%) GEL LABORATORIES LLC . 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.2 Sample ID: 405235056 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 31.8% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 31.8 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0209 +/-0.0446 0.137 Plutonium-239/240 HUh -0.0178 +/-0.0439 0.131 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00495 +/-0.0717 0.169 Uranium-233/234 Hh 1.14 +/-0.419 0.202 Uranium-235/236 Hh 0.116 +/-0.151 0.116 Uranium-238 Hh 1.44 +/-0.470 0.216 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.00 +/-0.273 0.415 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.13 +/-0.657 0.675 Thorium-229 HUh 0.124 +/-0.297 0.538 Thorium-230 Hh 1.09 +/-0.527 0.408 Thorium-232 Hh 0.887 +/-0.472 0.355 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0122 +/-0.0574 0.145 Curium-242 Hh 0.00 +/-0.131 0.197 Curium-243/244 Hh 0.0193 +/-0.054 0.0578 Curium-245/246 HUh 0.0173 +/-0.0614 0.101 Liquid Sein! Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 1.00 +/-5.49 9.41 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.167 +/-0.262 0.913 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0863 +/-0.361 0.655 Antimony-125 HUh 0.0737 +/-0.151 0.302 Bismuth-212 HU!h 0.00 +/-0.880 1.86 Bismuth-214 Hh 1.48 +/-0.253 0.159 Cesium-137 Hh 0.228 +/-0.100 0.0865 Cobalt-60 HUh 0.0496 +/-0.0626 0.145 Europium-154 HUh 0.0879 +/-0.210 0.358 Lead-212 Hh 1.32 +/-0.162 0.146 Lead-2°14 Hh 1.53 +/-0.274 0.510 Page 268 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.0369 +/-0.0447 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.034 +/-0.044 1.00 pCi/g 0.0476 +/-0.0719 1.00 pCi/g HAKB 09/22/16 1003 1596408 3 0.0435 +!-0.495 1.00 pCi/g 0.00 +/-0.154 1.00 pCi/g 0.0502 +/-0.576 1.00 pCi/g 0.00 +/-0.274 1.00 pCi/g HAKB 09/26/16 1151 1596411 4 0.220 +/-0.683 1.00 pCi/g HAKB 09/22/16 1344 1596407 5 0.181 +/-0.298 1.00 pCi/g 0.117 +/-0.555 1.00 pCi/g 0.0903 +/-0.493 1.00 pCi/g 0.0439 +/-0.0575 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.132 1.00 pCi/g 0.00 +/-0.0541 1.00 pCi/g 0.0178 +/-0.0615 1.00 pCi/g 4.58 +/-5.49 15.0 pCi/g HAKB 09/24/16 0554 1596414 7 0.311 +/-0.273 1.00 pCi/g MJHI 09/28/16 1515 1598647 8 0.303 +/-0.363 pCi/g MXRI 10/03/16 0750 1596252 9 0.136 +/-0.155 pCi/g 0.843 +/-1.01 pCi/g 0.0684 +/-0.261 pCi/g 0.0369 +/-0.101 0.100 pCi/g 0.062 +/-0.0665 pCi/g 0.151 +/-0.214 pCi/g 0.0681 +/-0.177 pCi/g 0.246 +/-0.282 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.2 Sample ID: 405235056 Certificate of Analysis Report Date: Project: MJWCOO 115 Client ID: MJWCOO I October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 19.2 +/-2.25 Protactinium-231 HU!h 0.00 +/-1.28 Radium-226 Hh 1.48 +/-0.253 Radium-228 Hh 1.18 +/-0.484 Thallium-208 Hh 0.354 +/-0.112 Tin-126 HU!h 0.00 +/-0.211 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 18.6 +/-4.44 Beta Hh 31.6 +/-3.63 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.971 +/-0.874 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -2.66 +/-2.87 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.647 +/-0.823 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.739 +/-2.33 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 0.967 1.15 0.159 0.478 0.0842 0.180 3.95 3.23 1.85 5.14 1.43 . 4.06 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 269 of 5809 0.387 +/-2.46 pCi/g 0.524 +/-1.29 pCi/g 0.0684 +/-0.261 pCi/g 0.213 +/-0.488 pCi/g 0.0365 +/-0.113 pCi/g 0.0841 +/-0.212 pCi/g 1.65 +/-5.79 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.50 +/-5.91 10.0 pCi/g 0.835 +/-0.874 2.00 pCi/g KSDI 09/22/16 1719 1597803 11 2.49 +/-2.87 6.00 pCi/g TXP3 09/25/16 0035 1598092 12 0.702 +/-0.823 2.00 pCi/g TXJI 09/27/16 1141 1598081 13 1.92 +/-2.33 5.00 pCi/g CXS7 09/20/16 1729 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.2 Sample ID: 405235056 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 270 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 98.2 (15%-125%) 1596408 63.9 (15%-125%) 1596408 99.5 (15%-125%) 1596411 86.5 (15%-125%) 1596407 97.7 (15%-125%) 1596410 90.l (15%-125%) 1596414 98.2 (15%-125%) 1597803 78.8 (25%-125%) 1597414 91.8 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.3 Saml?le ID: 405235057 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 27.l % Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 27.1 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.0209 +/-0.0515 0.154 Plutonium-239/240 HUh 0.0106 +/-0.0694 0.138 ASP Uranium Isotopic, Solid Dry Weight Corrected" Uranium-232 HUh -0.0184 +l-0.0509 0.148 Uranium-233/234 Hh 0.915 +/-0.356 0.166 Uranium-235/236 Hh 0.0639 +/-0.117 0.148 Uranium-238 Hh 0.666 +/-0.308 0.192 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0314 +/-0.262 0.616 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.29 +/-0.620 0.461 Thorium-229 HUh -0.0206 +/-0.192 0.447 Thorium-230 Hh 1.17 +/-0.519 0.431 Thorium-232 Hh 1.24 +/-0.514 0.313 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0246 +/-0.062 0.104 Curium-242 Hh 0.00 +/-0.123 0.185 Curium-243/244 HUh -0.0333 +/-0.0422 0.143 Curium-245/246 Hh 0.00 +/-0.0407 0.061 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -4.86 +/-6.76 11.9 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0658 +/-0.148 0.356 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0122 +/-0.218 0.390 Antimony-125 HUh 0.00259 +/-0.0957 0.189 Bismuth-212 HU!h 0.00 +/-0.757 1.43 Bismuth-214 Hh I.I I +/-0.196 0.128 Cesium-137 Hh 0.225 +/-0.0798 0.0759 Cobalt-60 HUh -0.00665 +/-0.0424 0.0734 Europium-154 HUh 0.0281 +/-0.129 0.242 Lead-212 Hh 1.16 +/-0.130 0.0951 Lead-214 Hh 1.17 +/-0.203 0.130 Page 271of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYT! 09/08/16 0827 1596233 1 0.0399 +/-0.0517 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0324 +/-0.0695 1.00 pCi/g 0.0373 +/-0.0512 1.00 pCi/g HAKB 09/22/16 1003 1596408 3 0.0317 +/-0.409 1.00 pCi/g 0.0225 +/-0.118 1.00 pCi/g 0.0448 +/-0.341 1.00 pCi/g 0.112 +/-0.262 1.00 pCi/g HAKB 09/22/16 1553 1596411 4 0.127 +/-0.650 1.00 pCi/g HAKB 09/22/16 1344 1596407 5 0.146 +/-0.192 1.00 pCi/g 0.138 +/-0.547 1.00 pCi/g 0.0796 +/-0.545 1.00 pCi/g 0.0252 +/-0.0621 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.123 1.00 pCi/g 0.0443 +/-0.0422 1.00 pCi/g 0.00 +/-0.0408 1.00 pCi/g 5.79 +/-6.76 15.0 pCi/g HAKB 09/24/16 0655 1596414 7 0.144 +/-0.151 1.00 pCi/g MJHI 09/28/16 1548 1598647 8 0.177 '+/-0.218 pCi/g MXRI 10/03/16 0751 1596252 9 0.0836 +/-0.0957 pCi/g 0.654 +/-0.962 pCi/g 0.0563 +/-0.202 pCi/g 0.0336 +/-0.0804 0.100 pCi/g 0.0295 +/-0.0425 pCi/g 0.102 +/-0.130 pCi/g 0.0439 +/-0.144 pCi/g 0.0591 +/-0.209 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.3 Sample ID: 405235057 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 14.8 +/-1.85 Protactinium-231 HUh 0.0304 +/-0.520 Radium-226 Hh I.I I +/-0.196 Radium-228 Hh 1.46 +/-0.347 Thallium-208 Hh 0.322 +/-0.097 Tin-126 HUih 0.00 +/-0.105 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 22.1 +/-4.74 Beta Hh 23.9 +/-2.90 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.749 +/-0.592 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.183 +/-2.78 Liquid Scint CJ4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.286 +/-0.798 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.0999 +/-1.95 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.693 0.853 0.128 0.296 0.0655 0.081 3.98 2.68 1.34 4.82 1.36 3.47 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 !0B Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 272 of 5809 0.281 +/-2.00 pCi/g 0.391 +/-0.520 pCi/g 0.0563 +/-0.202 pCi/g 0.130 +/-0.355 pCi/g 0.0289 +/-0.098 pCi/g 0.0378 +/-0.106 pCi/g 1.66 +/-6.35 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.24 +/-4.46 10.0 pCi/g 0.592 +/-0.593 2.00 pCi/g KSDI 09123/16 1121 1597803 II 2.34 +/-2.78 6.00 pCi/g TXP3 09/25/16 0219 1598092 12 0.665 +/-0.798 2.00 pCi/g TXJl 09/27/16 1253 1598081 13 1.64 +/-1.95 5.00 pCi/g CXS7 09/20/16 1712 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.3 Sample ID: 405235057 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 273 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 78.6 (15%-125%) 1596408 .73.6 (15%-125%) 1596408 94 (15%-125%) 1596411 89.7 (15%-125%) 1596407 109 (15%-125%) 97.5 (15%-125%) 1596414 78.6 (15%-125%) 1597803 91 (25%-125%) 1597414 96.7 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.4 Sample ID: 405235058 Matrix: Soil Collect Date: 02-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 19.8% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 19.8 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0115 +/-0.0761 0.152 Plutonium-239/240 Hh 0.0381 +!-0.0919 0.151 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0251 +/-0.0586 0.176 Uranium-233/234 Hh 0.771 +/-0.313 0.215 Uranium-235/236 Hh 0.156 +/-0.158 0.187 Uranium-238 Hh 0.557 +/-0.279 0.257 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0274 +/-0.395 0.934 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.08 +/-0.624 0.595 Thorium-229 Hh 0.131 +/-0.232 0.351 Thorium-230 Hh 0.878 +/-0.483 0.444 Thorium-232 Hh 0.716 +/-0.422 0.317 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0158 +/-0.0567 0.147 Curium-242 Hh 0.00 +/-0.129 0.193 Curium-243/244 HUh -0.0155 +/-0.0407 0.118 Curium-245/246 HUh -0.0131 +/-0.0451 0.124 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 1.19 +/-7.09 12.2 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.188 +/-0.285 0.478 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0411 +/-0.246 0.455 Antimony-125 HUh -0.0263 +/-0.107 0.204 Bismuth-212 HUh 0.178 +/-0.543 1.08 Bismuth-214 Hh 0.900 +/-0.201 0.146 Cesium-137 HU!h 0.00 +/-0.0407 0.0895 Cobalt-60 HUh -0.0217 +/-0.0423 0.0769 Europium-154 HU!h 0.00 +/-0.192 0.272 Lead-212 Hh 1.11 +/-0.136 0.094 Lead-214 Hh 1.18 +/-0.209 0.363 Page 274 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 I 0.0356 +/-0.0763 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0354 +/-0.0921 1.00 pCi/g 0.0466 +/-0.0589 1.00 pCi/g HAKB 09/22/16 1003 1596408 3 0.0621 +/-0.355 1.00 pCi/g 0.0483 +/-0.162 1.00 pCi/g 0.0834 +/-0.304 1.00 pCi/g 0.261 +/-0.395 1.00 pCi/g HAKB 09/22/16 1553 1596411 4 0.182 +/-0.652 1.00 pCi/g HAKB 09/26/16 1201 1596407 5 0.0893 +/-0.233 1.00 pCi/g 0.136 +/-0.502 1.00 pCi/g 0.0725 +/-0.436 1.00 pCi/g 0.0457 +/-0.0568 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.129 1.00 pCi/g 0.0309 +/-0.0408 1.00 pCi/g 0.0301 +/-0.0452 1.00 pCi/g 5.92 +/-7.09 15.0 pCi/g HAKB 09/24/16 0757 1596414 7 0.196 +/-0.298 1.00 pCi/g MJHl 09/28/16 1549 1598647 8 0.209 +/-0.246 pCi/g 0MXRl 10/03/16 0751 1596252 9 0.0914 +/-0.108 pCi/g 0.479 +/-0.549 pCi/g 0.0657 +/-0.215 pCi/g 0.0404 +/-0.0465 0.100 pCi/g 0.031 +/-0.0434 pCi/g 0.116 +/-0.209 pCi/g 0.0431 +/-0.169 pCi/g 0.175 +/-0.234 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.SC.R.2.4 Sample ID: 405235058 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.8 +/-1.62 Protactinium-231 HUh -0.0493 +/-0.455 Radium-226 Hh 0.900 +/-0.201 Radium-228 Hh 0.576 +/-0.375 Thallium-208 Hh 0.214 +/-0.102 Tin-126 HU!h 0.00 +/-0.128 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.9 +/-4.00 Beta Hh 21.2 +/-2.72 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.0972 +/-0.753 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.869 +/-2.79 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0863 +/-0.716 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.0868 +/-1.74 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.799 0.894 0.146 0.291 0.066 0.127 3.92 2.65 1.40 4.78 1.23 3.09 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 275 of 5809 0.332 +/-1.95 pCi/g 0.410 +/-0.456 pCi/g 0.0657 +/-0.215 pCi/g 0.127 +/-0.383 pCi/g 0.0291 +/-0.104 pCi/g 0.0597 +/-0.129 pCi/g 1.69 +/-5.20 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.23 +/-4.04 10.0 pCi/g 0.640 +/-0.753 2.00 pCi/g KSD! 09/23/16 1121 1597803 11 2.32 +/-2.79 6.00 pCi/g TXP3 09/25/16 0647 1598092 12 0.602 +/-0.716 2.00 pCi/g TXJ! 09127116 1404 1598081 13 1.46 +/-1.74 5.00 pCi/g CXS7 09/20/16 1835 1597414 14 Analyst Date Time Prep Batch LYT! 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 4.5C.R.2.4 Sample ID: 405235058 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l .96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 276 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 76.2 (15%-125%) 1596408 86.8 (15%-125%) 1596408 82.1 (15%-125%) 1596411 91.1 (15%-125%) 1596407 99.8 (15%-125%) 1596410 90.3 (15%-125%) 1596414 76.2 (15%-125%) 1597803 88.3 (25%-125%) 1597414 92.6 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.IA.R.1.2 Sample ID: 405235059 Matrix: Soil Collect Date: 16-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 12% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 12.0 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 HUh 0.0153 +/-0.0758 0.142 Plutonium-239/240 HUh -0.0114 +/-0.0543 0.141 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0334 +/-0.0534 0.175 Uranium-233/234 Hh 0.791 +/-0.303 0.151 Uranium-235/236 Hh 0.111 +/-0.127 0.124 Uranium-238 Hh 0.619 +/-0.270 0.151 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.158 +/-0.343 1.06 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.45 +/-0.774 0.778 Thorium-229 Hh 0.439 +/-0.387 0.452 Thorium-230 Hh 0.726 +/-0.459 0.393 Thorium-232 Hh 0.962 +/-0.504 0.192 Am241, Cm Solid "Dry Weight Corrected" Arnericium-241 HUh 0.0239 +/-0.085 0.139 Curium-242 Hh 0.00 +/-0.196 0.294 Curium-243/244 Hh 0.0663 +/-0.122 0.191 Curium-245/246 Hh 0.0343 +/-0.0961 0.103 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh -4.9 +/-7.29 12.8 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.00576 +/-0.128 0.274 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.00951 +/-0.180 0.364 Antimony-125 HUh -0.000891 +/-0.0924 0.181 Bismuth-212 HU!h 0.00 +/-0.970 .1.26 Bismuth-214 Hh 0.795 +/-0.217 0.100 Cesium-137 Hh 0.072 +/-0.0437 0.055 Cobalt-60 HUh -0.0335 +/-0.0339 0.0522 Europium-154 HUh -0.0301 +/-0.0965 0.183 Lead-212 Hh 0.931 +/-0.118 0.0819 Lead-214 Hh 0.851 +/-0.179 0.112 Page 277of5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 1 0.0309 +/-0.076 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0307 +/-0.0545 1.00 pCi/g 0.0505 +/-0.0536 1.00 pCi/g HAKB 09/22/16 1003 1596408 3 0.0325 +/-0.345 1.00 pCi/g 0.0188 +/-0.129 1.00 pCi/g 0.0325 +/-0.299 1.00 pCi/g 0.281 +/-0.343 1.00 pCi/g HAKB 09/22/16 1553 1596411 4 0.261 +/-0.810 1.00 pCi/g HAKB 09/22/16 1344 1596407 5 0.129 +/-0.393 1.00 pCi/g 0.100 +/-0.473 1.00 pCi/g 0.00 +/-0.527 1.00 pCi/g 0.0246 +/-0.0851 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.197 1.00 pCi/g 0.0498 +/-0.123 1.00 pCi/g 0.00 +/-0.0963 1.00 pCi/g 6.24 +/-7.29 15.0 pCi/g HAKB 09/24/16 0858 1596414 7 0.103 +/-0.129 1.00 pCi/g MJHI 09/28/16 1549 1598647 8 0.166 +/-0.180 pCi/g MXRl 10/03/16 0752 1596252 9 0.0812 +/-0.0924 pCi/g 0.580 +/-1.14 pCi/g 0.0436 +/-0.220 pCi/g 0.0237 +/-0.0438 0.100 pCi/g 0.020 +/-0.0371 pCi/g 0.0756 +/-0.0974 pCi/g 0.0377 +/-0.128 pCi/g 0.0506 +/-0.183 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.lA.R.1.2 Sample ID: 405235059 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier . Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 10.9 +/-1.40

Protactinium-231 HUh 0.0471 +/-0.348 Radium-226 Hh 0.795 +/-0.217 Radium-228 Hh 0.513 +/-0.251 Thallium-208 Hh 0.286 +/-0.0704 Tin-126 HUih 0.00 +/-0.136 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 19.9 +/-3.99 Beta Hh 24.8 +/-3.02 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.292 +/-0.653 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -1.78 +/-2.83 Liquid Scint CJ4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.242 +/-0.688 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.587 +/-1.60 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.548 0.682 0.100 0.194 0.0532 0.124 3.98 3.45 1.16 4.95 1.17 2.77 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 278 of 5809 0.219 +/-1.51 pCi/g . 0.309 +/-0.349 pCi/g 0.0436 +/-0.220 pCi/g 0.0812 +/-0.253 pCi/g 0.0232 +/-0.0714 pCi/g 0.0584 +/-0.137 pCi/g 1.77 +/-5.56 4.00 pCi/g JXC9 09/28/16 1448 1602427 10 1.65 +/-4.86 10.0 pCi/g 0.516 +/-0.655 2.00 pCi/g KSDI 09/22/16 1718 1597803 11 2.42 +/-2.83 6.00 pCi/g TXP3 09/26/16 0950 1598092 12 0.574 +/-0.689 2.00 pCi/g TXJI 09/27/16 1516 1598081 13 1.31 +/-1.60 5.00 pCi/g CXS7 09/20/16 1818 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.IA.R.1.2 Sample ID: 405235059 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 279 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 72.5 (15%-125%) 1596408 90.4 (15%-125%) 1596408 93.8 (15%-125%) 1596411 81.2 (15%-125%) 1596407 94.1 (15%-125%) 1596410 55.1 (15%-125%) 1596414 72.5 (15%-125%) 1597803 92.3 (25%-125%) 1597414 95.9 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.lA.R.1.3 Sample ID: 405235060 Matrix: Soil Collect Date: 16-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 9.64% Parameter Qualifier Result,Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 9.64 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0,0108 +/-0.0389 0.107 Plutonium-239/240 HUh -0.00806 +/-0.0383 0.0997 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0171 +/-0.0587 0.163 Uranium-233/234 Hh 0.262 +/-0.171 0.141 Uranium-235/236 Hh 0.0217 +/-0.0704 0.109 Uranium-238 Hh 0.570 +/-0.241 0.122 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.096 +/-0.412 1.06 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.404 +/-0.528 0.787 Thorium-229 HUh -0.0511 +/-0.231 0.583 Thorium-230 Hh 1.16 +/-0.609 0.415 Thorium-232 Hh 0.748 +/-0.487 0.224 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.00394 +/-0.0507 0.120 Curium-242 Hh 0.00 +/-0.111 0.167 Curium-243/244 HUh -0.0106 +/-0.0367 0.101 Curium-245/246 Hh 0.031 +/-0.0676 0.104 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh 2.74 +/-5.93 10.1 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0572 +/-0.119 0.254 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh +/-0.189 0.362 Antimony-125 HUh 0.0261 +/-0.0828 0.158 Bismuth-212 HU!h 0.00 +/-0.686 0.983 Bismuth-214 Hh 0.855 +/-0.176 0.108 Cesium-137 Hh 0.094 +/-0.0438 0.0505 Cobalt-60 HUh 0.0163 +/-0.0265 0.0568 Europium-154 HUh 0.0611 +/-0.103 0.189 Lead-212 Hh 0.811 +/-0.101 0.0736 Lead-214 Hh 1.07 +/-0.167 0.269 Page 280 of 5809 Report Date: October 4, 2016 Project: MJWCOOI 15 Client ID: MJWCOOI Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0827 1596233 1 0.0252 +/-0.039 1.00 pCi/g HAKB 09/22/16 0956 1596412 2 0.0217 +/-0.0384 1.00 pCi/g 0.0389 +/-0.059 1.00 pCi/g HAKB 09/22/16 1003 1596408 3 0.0329 +/-0.179 1.00 pCi/g 0.0165 +/-0.0706 1.00 pCi/g 0.0233 +/-0.268 1.00 pCi/g 0.318 +/-0.412 1.00 pCi/g HAKB 09/22/16 1553 1596411 4 0.245 +/-0.533 1.00 pCi/g HAKB 09/22/16 1344 1596407 5 0.179 +/-0.232 1.00 pCi/g 0.0952 +/-0.641 1.00 pCi/g 0.00 +/-0.504 1.00 pCi/g 0.0342 +/-0.0507 1.00 pCi/g HAKB 09/22/16 0956 1596410 6 0.00 +/-0.112 1.00 pCi/g 0.0245 +/-0.0367 1.00 pCi/g 0.0226 +/-0.0678 1.00 pCi/g 4.91 +/-5.96 15.0 pCi/g HAKB 09/24/16 0959 1596414 7 0.0668 +/-0.122 1.00 pCi/g MJHI 09/28/16 1550 1598647 8 0.170 +/-0.189 pCi/g MXRl 10/03/16 0752 1596252 9 0.0728 +/-0.0836 pCi/g 0.459 +/-0.878 pCi/g 0.0499 +/-0.180 pCi/g 0.0228 +/-0.044 0.100 pCi/g 0.0248 +/-0.0275 pCi/g 0.0846 +/-0.107 pCi/g 0.0344 +/-0.110 pCi/g 0.131 +/-0.173 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.lA.R.1.3 Sample ID: 405235060 Certificate of Analysis Project: Client ID: Report Date: MJWC00115 MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.6 +/-1.07 Protactinium-231 HUh 0.201 +/-0.376 Radium-226 Hh 0.855 +/-0.176 Radium-228 Hh 0.869 +/-0.259 Thallium-208 Hh 0.220 +/-0.0883 Tin-126 HU!h 0.00 +/-0.104 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 17.4 +/-3.70 Beta Hh 22.6 +/-2.51 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.112 +/-0.508 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -2.08 +/-2.20 Liquid Seint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0157 +/-0.598 Liquid Seint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -1.35 +/-1.41 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R 0.422 0.711 0.108 0.162 0.0472 0.0964 3.92 2.42 0.954 3.94 1.02 2.66 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 281of5809 0.178 +/-1.26 pCi/g 0.333 +/-0:389 pCi/g 0.0499 +/-0.180 pCi/g 0.0711 +/-0.263 pCi/g 0.0214 +/-0.0888 pCi/g 0.0451 +/-0.105 pCi/g 1.75 +/-5.03 4.00 pCi/g JXC9 09/28/16 1449 1602427 10 1.13 +/-4.10 10.0 pCi/g 0.410 +/-0.508 2.00 pCi/g KSDI 09/22/16 1718 1597803 II 1.91 +/-2.20 6.00 pCi/g TXP3 09/25/16 1017 1598092 12 0.502 +/-0.598 2.00 pCi/g TXJI 09/27/16 1628 1598081 13 1.26 +/-1.41 5.00 pCi/g CXS7 09120116 1802 1597414 14 Analyst Date Time Prep Batch LYTI 09/08/16 0827 1596233 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.lA.R.1.3 Sample ID: 405235060 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 282 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596412 92.2 (15%-125%) 1596408 94.7 (15%-125%) 1596408 79.8 (15%-125%) 1596411 85.5 (15%-125%) 1596407 72.5 (15%-125%) 1596410 96.3 (15%-125%) 1596414 92.2 (15%-125%) 1597803 88.3 (25%-125%) 1597414 96.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.lB.R.2.2 Sample ID: 405235061 Matrix: Soil Collect Date: 14-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 17.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 17.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0258 +/-0.0508 0.0704 Plutonium-239/240 Hh 0.0257 +/-0.0505 0.070 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0232 +/-0.0794 0.147 Uranium-233/234 Hh 0.585 +/-0.188 0.0462 Uranium-235/236 Hh 0.0309 +/-0.0529 0.0463 Uranium-238 Hh 0.800 +/-0.220 0.0462 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.102 +/-0.237 0.704 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.491 +l-0.506 0.689 Thorium-229 Hh 0.00 +/-0.130 0.193 Thorium-230 . Hh 0.707 +/-0.437 0.193 Thorium-232 Hh 0.850 +/-0.490 0.391 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.142 +/-0.243 0.213 Curium-242 Hh 0.00 +/-0.470 0.700 Curium-243/244 Hh 0.00 +/-0.145 0.216 Curium-245/246 Hh 0.081 +/-0.228 0.243 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.33 +/-4.61 7.97 Rad Gamma Spec Analysis Gamma /129, Solid "Dry Weight Corrected" Iodine-129 HUih 0.00 +/-0.328 0.449 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.12 +/-0.189 0.350 Antimony-125 HUh 0.068 +/-0.0832 0.178 Bismuth-212 HUih 0.00 +/-0.504 1.12 Bismuth-214 Hh 0.922 +/-0.164 0.114 Cesium-137 HUh 0.0251 +/-0.039 0.0783 Cobalt-60 HUh 0.0224 +/-0.0301 0.0701 Europium-154 HUh 0.0331 +/-0.098 0.208 Lead-212 Hh 0.802 +/-0.112 0.0916 Lead-214 Hh 1.19 +/-0.158 0.102 Page 283 of 5809 Report Date: October 4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 1 0.0132 +/-0.0509 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0131 +l-0.0506 1.00 pCi/g 0.0401 +/-0.0795 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.00 +/-0.214 1.00 pCi/g 0.00 +/-0.0532 1.00 pCi/g 0.00 +/-0.260 1.00 pCi/g 0.192 +/-0.238 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.217 +/-0.514 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.00 +/-0.130 1.00 pCi/g 0.00 +/-0.450 1.00 pCi/g 0.0995 +/-0.507 1.00 pCi/g 0.00 +/-0.244 1.00 pCi/g KXB2 09/22/16 1753 1599981 6 0.00 +/-0.471 1.00 pCi/g 0.00 +/-0.145 1.00 pCi/g 0.00 +/-0.228 1.00 pCi/g 3.89 +/-4.61 15.0 pCi/g KXB2 09/21/16 1435 1596422 7 0.183 +/-0.328 1.00 pCi/g MJHl 09/28/16 1909 1598663 8 0.160 +/-0.197 pCi/g MXRl 10/03/16 0552 1596254 9 0.0804 +/-0.0887 pCi/g 0.513 +/-0.633 pCi/g 0.0512 +/-0.168 pCi/g 0.0357 +/-0.0407 0.100 pCi/g 0.0295 +/-0.0318 pCi/g 0.0895 +/-0.0992 pCi/g 0.0428 +/-0.120 pCi/g 0.0459 +/-0.166 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.IB.R.2.2 Sample ID: 405235061 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 10.5 +/-1.37 0.674 Protactinium-231 HU!h 0.00 +/-0.553 0.521 Radium-226 Hh 0.922 +/-0.164 0.114 Radium-228 HU!h 0.00 +/-0.227 0.497 Thallium-208 Hh 0.264 +/-0.0737 0.0515 Tin-126 HUh 0.0261 +/-0.125 0.109 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 28.5 +/-6.85 3.64 Beta Hh 37.7 +/-4.83 2.94 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.823 +/-0.639 1.42 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.635 +/-2.11 3.63 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0115 +/-0.738 1.27 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.147 +/-0.973 1.72 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 284 of 5809 0.286 +/-1.47 pCi/g 0.231 +/-0.593 pCi/g 0.0512 +/-0.168 pCi/g 0.234 +/-0.465 pCi/g 0.0227 +/-0.0745 pCi/g 0.0517 +/-0.126 pCi/g 1.21 +/-8.71 4.00 pCi/g JXC9 09/22/16 1239 1597817 10 1.26 +/-7.08 10.0 pCi/g 0.634 +/-0.640 2.00 pCi/g BXFI 09/27/16 1539 1597804 II 1.75 +/-2.11 6.00 pCi/g TXP3 09/26/16 1335 1598096 12 0.620 +/-0.738 2.00 pCi/g TIU! 09/29/16 0031 1598082 13 0.808 +/-0.974 5.00 pCi/g CXS7 09/20/16 0558 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.lB.R.2.2 Sample ID: 405235061 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 20 I 6 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 I, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 285 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 88 (15%-125%) 1596418 80.7 (15%-125%) 1596418 64.l (15%-125%) 1596420 62.2 (15%-125%) 1596417 104 (15%-125%) 1599981 94.9 (15%-125%) 1596422 88 (15%-125%) 1597804 95 (25%-125%) 1597417 94.4 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.l.2 Sample ID: 405235062 Matrix: Soil Collect Date: 14-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 19.4% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 22 i 6 % Moisture As Received" Moisture 19.4 Rad Alpha Spec Analysis ASP Plutonium isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00479 +/-0.0501 0.105 Plutonium-239/240 HUh -0.0204 +/-0.0387 0.119 ASP Uranium isotopic, Solid "Dry Weight Corrected" Uranium-232 Hh 0.0327 +/-0.0651 0.106 Uranium-233/234 Hh 0.647 +/-0.236 0.137 Uranium-235/236 Hh 0.0577 +/-0.0831 0.100 Uranium-238 Hh 0.954 +/-0.281 0.100 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.024 +/-0.251 0.524 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.234 +/-0.407 0.646 Thorium-229 Hh 0.176 +/-0.279 0.386 Thorium-230 Hh 0.871 +/-0.513 0.385 Thorium-232 Hh 0.399 +/-0.363 0.333 Am24i, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.037 +/-0.164 0.427 Curium-242 HUh -0.0609 +/-0.525 1.22 Curium-243/244 HUh -0.0375 +/-0.166 0.433 Curium-245/246 HXh 0.529 +/-0.459 0.264 Liquid Scint Pu24i, Solid "Dry Weight Corrected" Plutonium-241 HUh -5.88 +/-4.74 8.38 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" lodine-129 HUh -0.00633 +/-0.128 0.361 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.249 +/-0.253 0.413 Antimony-125 HUh -0.00782 +/-0.0964 0.201 Bismuth-212 HUh 0.507 +/-1.06 1.48 Bismuth-214 Hh 0.881 +/-0.205 0.144 Cesium-137 HUih 0.00 +/-0.0638 0.0743 Cobalt-60 HUh -0.0307 +/-0.0466 0.0834 Europium-154 HUh -0.0193 +/-0.140 0.289 Lead-212 Hh 0.897 +/-0.140 0.0957 Lead-214 Hh 1.02 +/-0.219 0.394 Page 286 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units* PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 1 0.0266 +/-0.0502 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0341 +/-0.0388 1.00 pCi/g 0.0288 +/-0.0654 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0374 +/-0.264 1.00 pCi/g 0.0188 +/-0.0838 1.00 pCi/g 0.0187 +/-0.330 1.00 pCi/g 0.133 +/-0.251 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.185 +/-0.410 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.0885 +/-0.280 1.00 pCi/g 0.0883 +/-0.531 1.00 pCi/g 0.0622 +/-0.368 1.00 pCi/g 0.0978 +/-0.164 1.00 pCi/g KXB2 09/22/16 1753 1599981 6 0.228 +/-0.526 1.00 pCi/g 0.0992 +/-0.166 1.00 pCi/g 0.00 +/-0.465 1.00 pCi/g 4.10 +/-4.74 15.0 pCi/g KXB2 09/21/16 1606 1596422 7 0.108 +/-0.128 1.00 pCi/g MJHl 09/28/16 1909 1598663 8 0.183 +/-0.279 pCi/g MXRl 10/03/16 0553 1596254 9 0.0855 +/-0.0965 pCi/g 0.652 +/-1.09 pCi/g 0.0609 +/-0.208 pCi/g 0.0308 +/-0.0639 0.100 pCi/g 0.0308 +/-0.0486 pCi/g 0.116 +/-0.140 pCi/g 0.0431 +/-0.148 pCi/g 0.189 +/-0.223 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.l.2 Sample ID: 405235062 Certificate of Analysis Report Date: Project: MJWCOO 115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 10.3 +/-1.84 Protactinium-231 HUh 0.259 +/-0.545 Radium-226 Hh 0.881 +/-0.205 Radium-228 Hh 1.03 +/-0.387 Thallium-208 Hh 0.238 +/-0.0747 Tin-126 HUh 0.00635 +/-0.207 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 16.6 +/-3.93 Beta Hh 31.2 +/-3.15 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.0085 +l-0.969 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.14 +/-2.25 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.065 +/-0.756 Liquid Sein! Tc99, Solid Dry Weight Corrected" Technetium-99 HUh 0.0577 +/-1.04 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-O I Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.678 1.07 0.144 0.313 0.0643 0.148 4.00 2.56 1.80 3.84 1.29 1.85 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 287 of 5809 0.239 +/-1.92 pCi/g 0.488 +/-0.560 pCi/g 0.0609 +/-0.208 pCi/g 0.130 +/-0.390 pCi/g 0.0266 +/-0.0754 pCi/g 0.0696 +/-0.207 pCi/g 1.74 +l-5.09 4.00 pCi/g JXC9 09/22/16 1239 1597817 10 1.19 +l-5.59 10.0 pCi/g 0.814 +/-0.969 2.00 pCi/g BXFI 09/27/16 1539 1597804 II 1.85 +/-2.25 6.00 pCi/g TXP3 09/26/16 1510 1598096 12 0.633 +/-0.756 2.00 pCi/g TXJI 09/29/16 0255 1598082 13 0.869 +/-1.04 5.00 pCi/g CXS7 09/20/16 0626 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.1.2 Sample ID: 405235062 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 288 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 83.5 (15%-125%) 1596418 64.8 (15%-125%) 1596418 90.8 (15%-125%) 1596420 83.5 (15%-125%) 1596417 98.5 (15%-125%) 1599981 86.8 (15%-125%) 1596422 83.5 (15%-125%) 1597804 86.9 (25%-125%) 1597417 92.1 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.l.3 Sample ID: 405235063 Matrix: Soil Collect Date: 14-DEC-15 Receive Date: 06-SEP-I 6 Collector: Client Moisture: 10.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 10.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid Dry Weight Corrected" Plutonium-238 Hh 0.0159 +/-0.0448 0.0478 Plutonium-239/240 HUh 0.00823 +/-0.0457 0.0877 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00436 +/-0.0455 0.095 Uranium-233/234 Hh 0.622 +/-0.242 0.170 Uranium-235/236 Hh 0.0335 +/-0.077 0.122 Uranium-238 Hh 0.600 +/-0.233 0.134 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0471 +/-0.262 0.501 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.41 +/-0.660 0.490 Thorium-229 Hh 0.0829 +/-0.190 0.302 Thorium-230 Hh 0.274 +/-0.288 0.359 Thorium-232 Hh 0.380 +/-0.302 0.163 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0585 +/-0.164 0.175 Curium-242 HUh -0.0462 +/-0.398 0.923 Curium-243/244 Hh 0.00 +/-0.119 0.178 Curium-245/246 Hh 0.134 +/-0.229 0.201 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -4.21 +l-5.03 8.81 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0176 +/-0.200 0.416 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 6.032 +/-0.230 0.425 Antimony-125 HUh 0.0909 +/-0.119 0.248 Bismuth-212 HUih 0.00 +/-1.07 1.32 Bismuth-214 Hh 0.860 +/-0.230 0.125 Cesium-137 HUh 0.0309 +/-0.0428 0.0883 Cobalt-60 HUh -0.0124 +/-0.0393 0.0748 Europium-154 HUh 0.0544 +/-0.111 0.245 Lead-212 Hh 0.989 +/-0.132 0.0893 Lead-214 Hh 0.957 +/-0.183 0.133 Page 289 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOI Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 I 0.00 +/-0.0448 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0201 +/-0.0458 1.00 pCi/g 0.0242 +/-0.0456 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0522 +/-0.268 1.00 pCi/g 0.028 +/-0.0772 1.00 pCi/g 0.0342 +/-0.258 1.00 pCi/g 0.115 +/-0.262 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.138 +/-0.697 1.00 pCi/g KXB2 09119116 1803 1596417 5 0.0692 +/-0.191 1.00 pCi/g 0.0977 +/-0.291 1.00 pCi/g 0.00 +/-0.307 1.00 pCi/g 0.00 +/-0.165 1.00 pCi/g KXB2 09/22/16 1753 1599981 6 0.173 +/-0.399 1.00 pCi/g 0.00 +/-0.120 1.00 pCi/g 0.00 +/-0.230 1.00 pCi/g 4.31 +l-5.03 15.0 pCi/g KXB2 09/21/16 1737 1596422 7 0.158 +/-0.201 1.00 pCi/g MJHI 09/28/16 1910 1598663 8 0.195 +/-0.231 pCi/g MXRI 10/03/16 0553 1596254 9 0.113 +/-0.126 pCi/g 0.604 +/-1.13 pCi/g 0.055 +/-0.233 pCi/g 0.0399 +/-0.045 0.100 pCi/g 0.0305 +/-0.0397 pCi/g 0.104 +/-0.114 pCi/g 0.0411 +/-0.142 pCi/g 0.0604 +/-0.188 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.l.3 Sample ID: 405235063 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.6 +/-1.59 0.823 Protactinium-231 HUih 0.00 +/-0.644 0.896 Radium-226 Hh 0.860 +/-0.230 0.125 Radium-228 Hh 1.14 +/-0.396 0.227 Thallium-208 Hh 0.243 +/-0.0819 0.0715 Tin-126 HU!h 0.00 +/-0.133 0.121 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 35.9 +/-5.02 3.93 Beta Hh 39.3 +/-3.20 2.23 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.500 +/-0.924 1.61 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 1.83 +/-2.01 3.37 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.0622 +/-0.657 1.13 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.343 +/-0.880 1.53 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, EPA 900.0/SW846 931 O/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 290 of 5809 0.349 +/-1.70 pCi/g 0.413 +/-0.680 pCi/g 0.055 +/-0.233 pCi/g 0.0957 +/-Q.400 pCi/g 0.0319 +/-0.0825 pCi/g 0.0562 +/-0.134 pCi/g 1.74 +/-8.55 4.00 pCi/g JXC9 09/22/16 1239 1597817 10 1.03 +/-6.59 10.0 pCi/g 0.729 +/-0.928 2.00 pCi/g BXF! 09/28/16 0851 1597804 II 1.62 +/-2.01 6.00 pCi/g TXP3 09/26/16 1643 1598096 12 0.551 +/-0.657 2.00 pCi/g TXJI 09/29/16 0406 1598082 13 0.718 +/-0.880 5.00 pCi/g CXS7 09/20/16 0653 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R. l .3 Sample ID: 405235063 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Uranium-232 Tracer ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-235/236 Tracer ASP Uranium Isotopic, Solid "Dry Weight Corrected" Americium-243 Tracer Alphaspec Np237, Solid "Dry Weight Corrected" Actinium-227 Tracer Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Americium-243 Tracer Am241, Cm Solid "Dry Weight Corrected" Plutonium-242 Tracer Liquid Scint Pu241, Solid "Dry Weight Corrected" Strontium Carrier GFPC, Sr90, solid "Dry Weight Corrected" Technetium-99m Tracer Liquid Scint Tc99, Solid "Dry Weight Corrected" Notes: The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 291of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 1596418 1596418 1596420 1596417 1599981 1596422 1597804 1597417 78.5 60.2 92.5 74.7 110 104 78.5 86.9 92.9 (15%-125%) (15%-125%) (15%-125%) (15%-125%) (15%-125%) (15%-125%) (15%-125%) (25%-125%) (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.1.4 Sample ID: 405235064 Matrix: Soil Collect Date: 14-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 8.16% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 8.16 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0295 +/-0.0587 0.0953 Plutonium-239/240 HUh -0.0173 +/-0.0327 0.101 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.026 +/-0.0755 0.141 Uranium-233/234 Hh 0.700 +/-0.267 0.151 Uranium-235/236 Hh 0.00 +/-0.0501 0.0745 Uranium-238 Hh 0.588 +/-0.243 0.119 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.242 +/-0.481 0.781 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 2.18 +/-1.09 0.768 Thorium-229 Hh 0.147 +/-0.337 0.534 Thorium-230 Hh 0.481 +/-0.464 0.289 Thorium-232 Hh 1.44 +/-0.754 0.288 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.00272 +/-0.202 0.448 Curium-242 Hh 0.00 +/-0.451 0.671 Curium-243/244 HUh -0.0827 +/-0.157 0.483 Curium-245/246 HXh 0.233 +/-0.307 0.233 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -3.29 +/-4.38 7.66 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0487 +/-0.244 0.378 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0385 +/-0.200 0.392 Antimony-125 HUh -0.0366 +/-0.0928 0.172 Bismuth-212 HU!h 0.00 +/-0.935 1.43 Bismuth-214 Hh 0.994 +/-0.171 0.129 Cesium-137 HUh -0.0037 +/-0.0402 0.0763 Cobalt-60 HUh 0.0221 +/-0.0363 0.0756 Europium-154 HUh -0.0397 +/-0.0989 0.180 Lead-212 Hh 1.04 +/-0.133 0.0845 Lead-214 Hh 1.22 +/-0.204 0.314 Page 292 of 5809 Report Date: October 4, 2016 Project: MJWCOO 115 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 1 0.026 +/-0.0589 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0289 +/-0.0328 1.00 pCi/g 0.0461 +/-0.0757 1.00 pCi/g KXB2 09/19/16 1547 1596418 3 0.0385 +/-0.299 1.00 pCi/g 0.00 +/-0.0503 1.00 pCi/g 0.0222 +/-0.268 1.00 pCi/g 0.213 +/-0.482 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.194 +/-1.16 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.122 +/-0.338 1.00 pCi/g 0.00 +/-0.472 1.00 pCi/g 0.00 +/-0.796 1.00 pCi/g 0.122 +/-0.202 1.00 pCi/g KXB2 09/22/16 1753 1599981 6 0.00 +/-0.452 1.00 pCi/g 0.138 +/-0.157 1.00 pCi/g 0.00 +/-0.308 1.00 pCi/g 3.75 +/-4.38 15.0 pCi/g KXB2 09/21/16 1908 1596422 7 0.172 +/-0.245 1.00 pCi/g MJHl 09/29/16 0619 1598663 8 0.181 +/-0.20i pCi/g MXRl 10/03/16 0544 1596254 9 0.0773 +/-0.0943 pCi/g 0.665 +/-1.33 pCi/g 0.0584 +/-0.177 pCi/g 0.0346 +/-0.0403 0.100 pCi/g 0.032 +/-0.0376 pCi/g 0.075 +/-0.101 pCi/g 0.0392 +/-0.144 pCi/g 0.152 +/-0.210 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R. l .4 Sample ID: 405235064 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 20 I 6 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.7 +/-1.48 0.719 Protactinium-231 HU!h 0.00 +/-0.669 0.712 Radium-226 Hh 0.994 +/-0.171 0.129 Radium-228 Hh 0.903 +/-0.293 0.244 Thallium-208 Hh 0.306 +/-0.0844 0.0577 Tin-126 HU!h 0.00 +/-0.143 0.151 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 21.7 +/-4.92 3.99 Beta Hh 31.5 +/-3.80 3.63 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.0966 +/-0.745 1.40 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.00112 +/-1.91 3.32 Liquid Scint CJ4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.222 +/-0.672 1.14 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.016 +/-0.849 1.52 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified . DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 293 of 5809 0.307 +/-1.62 pCi/g 0.326 +/-0.744 pCi/g 0.0584 +/-0.177 pCi/g 0.107 +/-0.297 pCi/g 0.0256 +/-0.0854 pCi/g 0.0718 +/-0.144 pCi/g 1.63 +/-6.51 4.00 pCi/g JXC9 09/22/16 1240 1597817 10 1.69 +/-6.01 10.0 pCi/g 0.614 +/-0.746 2.00 pCi/g BXFl 09/28/16 0851 1597804 11 1.60 +/-1.91 6.00 pCi/g TXP3 09/26/16 1817 1598096 12 0.560 +/-0.673 2.00 pCi/g TXJl 09/29/16 0517 1598082 13 0.712 +/-0.849 5.00 pCi/g CXS7 09120116 0721 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.l.4 Sample ID: 405235064 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 294 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 91 (15%-125%) 1596418 57 (15%-125%) 1596418 98.3 (15%-125%) 1596420 64.9 (15%-125%) 1596417 69.8 (15%-125%) 1599981 107 (15%-125%) 1596422 91 (15%-12.5%) 1597804 80.l (25%-125%) 1597417 91.4 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.2.3 Sample ID: 405235065 Matrix: Soil Collect Date: 14-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 10.1% Parameter Qualifier *Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture IO.I Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0124 +/-0.0349 0.0372 Plutonium-239/240 HUh -0.00888 +/-0.0268 0.0753 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0209 +/-0.0476 0.130 Uranium-233/234 Hh 0.659 +/-0.204 0.0482 Uranium-235/236 Hh 0.0967 +/-0.0839 0.0484 Uranium-238 Hh 0.663 +/-0.207 0.0982 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.641 +/-0.610 0.643 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.14 +/-0.649 0.599 Thorium-229 HUh -0.0292 +/-0.129 0.337 Thorium-230 Hh 0.820 +/-0.463 0.336 Thorium-232 Hh 0.604 +/-0.394 0.181 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0985 +/-0.187 0.575 Curium-242 Hh 0.00 +/-0.544 0.810 Curium-243/244 Hh 0.166 +/-0.285 0.250 Curium-245/246 Hh 0.188 +/-0.321 0.281 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -2.13 +/-4.55 7.90 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0554 +/-0.207 0.417 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.128 +/-0.198 0.338 Antimony-125 HUh -0.0197 +/-0.081 0.156 Bismuth-212 HU!h 0.00 +/-0.858 1.27 Bismuth-214 Hh 0.984 +/-0.194 0.129 Cesium-137 HUh 0.0325 +/-0.0369 0.0774 Cobalt-60 HUh 0.0293 +/-0.0452 0.0909 Europium-154 HUh 0.0228 +/-0.115 0.233 Lead-212 Hh 1.08 +/-0.122 0.0782 Lead-214 Hh 1.31 +/-0.192 0.334 Page 295 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOI Le TPU RL Units *PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 I 0.00 +/-0.0349 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0192 +/-0.0269 1.00 pCi/g 0.0424 +/-0.0476 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.00 +/-0.232 1.00 pCi/g 0.00 +/-0.0855 1.00 pCi/g 0.025 +/-0.235 1.00 pCi/g 0.147 +/-0.614 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.179 +/-0.676 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.0771 +/-0.129 1.00 pCi/g 0.0769 +/-0.479 1.00 pCi/g 0.00 +/-0.405 1.00 pCi/g 0.165 +/-0.187 l.00 pCi/g KXB2 09/22/16 1753 1599981 6 0.00 +/-0.546 1.00 pCi/g 0.00 +/-0.286 l.00 pCi/g 0.00 +/-0.323 l.00 pCi/g 3.86 +/-4.55 15.0 pCi/g KXB2 09/21/16 2039 1596422 7 0.170 +/-0.209 l.00 pCi/g MJHl 09/29/16 0620 1598663 8 0.154 +/-0.207 pCi/g MXRI 10/03/16 0557 1596254 9 0.0691 +/-0.0815 pCi/g 0.584 +/-0.927 pCi/g 0.0581 +/-0.199 pCi/g 0.035 +/-0.0398 0.100 pCi/g 0.0392 +/-0.0471 pCi/g 0.100 +/-0.116 pCi/g 0.0361 +/-0.135 pCi/g 0.162 +/-0.200 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.2.3 Sample ID: 405235065 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dry Weight Corrected" Potassiilm-40 Hh 14.9 +/-1.62 Protactinium-231 HUih *0.00 +/-0.652 Radium-226 Hh 0.984 +/-0.194 Radium-228 Hh 1.17 +/-0.293 Thallium-208 Hh 0.359 +/-0.0862 Tin-126 HUih 0.00 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 16.4 Beta Hh 17.7 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 1.02 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.23 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh -0.30 Liquid Scint Tc99, Solid "Dry Weight Corrected" +/-0.084 +/-5.58 +/-3.85 +l-0.909 +/-2.00 +/-0.640 0.707 0.639 0.129 0.233 0.0502 0.0691 3.56 3.41 1.46 3.40 I.I I Technetium-99 HUh -0.364 +/-0.883 1.63 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 II 12 13 14 ASTM J:? 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 296 of 5809 0.296 +/-1.79 pCi/g 0.290 +/-0.706 pCi/g 0.0581 +/-0.199 pCi/g 0.101 +/-0.300 pCi/g 0.0218 +/-0.0876 pCi/g 0.0324 +/-0.0855 pCi/g 1.08 +/-6.34 4.00 pCi/g JXC9 09/22/16 1240 1597817 10 1.46 +/-4.50 10.0 pCi/g 0.629 +/-0.929 *2.00 pCi/g BXFI 09/27/16 1539 1597804 II 1.64 +/-2.00 6.00 pCi/g TXP3 09126116 1950 1598096 12 0.543 +/-0.640 2.00 pCi/g TXJI 09129116 0629 1598082 13 0.763 +/-0.883 5.00 pCi/g CXS7 09/20/16 0748 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.2.3 Sample ID: 405235065 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Teclmetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 297 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 91.l (15%-125%) 1596418 88.2 (15%-125%) 1596418 99.2 (15%-125%) 1596420 58.7 (15%-125%) 1596417 114 (15%-125%) 1599981 87.5 (15%-125%) 1596422 91.l (15%-125%) 1597804 84.2 (25%-125%) 1597417 89.l (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14 228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.2.4 Sample ID: 405235066 Matrix: Soil Collect Date: 14-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 9.29% Parameter

Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 9.29 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.030 +/-0.053 0.0803 Plutonium-239/240 HUh -0.00261 +/-0.0392 0.0916 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00443 +/-0.0664 0.155 Uranium-233/234 Hh 0.712 +/-0.227 0.130 Uranium-235/236 HUh 0.0225 +/-0.062 0.108 Uranium-238 Hh 0.738 +/-0.229 0.116 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0606 +/-0.274 0.690 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.469 +/-0.591 0.889 Thorium-229 Hh 0.00 +/-0.159 0.237 Thorium-230 Hh 0.515 +/-0.442 0.437 Thorium-232 Hh 0.828 +/-0.538 0.436 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.00 +/-0.144 0.215 Curium-242 Hh 0.00 +/-0.475 0.707 Curium-243/244 Hh 0.00 +/-0.146 0.218 Curium-245/246 Hh 0.0819 +/-0.230 0.246 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh -3.42 +/-4.43 7.75 Rad Gamma Spec Analysis Gamma IJ29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.012 +/-0.292 0.623 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0968 +/-0.220 0.421 Antimony-125 HUh -0.0479 +/-0.0868 0.162 Bismuth-212 HUih 0.00 +/-0.746 1.19 Bismuth-214 Hh 0.903 +/-0.191 0.0939 Cesium-137 HUih 0.00 +/-0.0333 0.0772 Cobalt-60 HUh -0.00205 +/-0.0339 0.0695 Europium-154 HUh 0.0238 +/-0.0922 0.184 Lead-212 Hh 0.792 +/-0.144 0.113 Lead-214 Hh 1.11 +/-0.160 0.116 Page 298 of 5809 Report Date: October4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0846 1596246 1 0.0204 +/-0.0531 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0262 +/-0.0392 1.00 pCi/g 0.0444 +/-0.0666 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0386 +/-0.261 1.00 pCi/g 0.0274 +/-0.0622 1.00 pCi/g 0.0315 +/-0.265 1.00 pCi/g 0.212 +/-0.274 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.288 +/-0.599 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.00 +/-0.160 1.00 pCi/g 0.100 +/-0.450 1.00 pCi/g 0.0999 +/-0.555 1.00 pCi/g 0.00 +/-0.145 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.476 1.00 pCi/g 0.00 +/-0.147 1.00 pCi/g 0.00 +/-0.230 1.00 pCi/g 3.79 +/-4.43 15.0 pCi/g KXB2 09/21/16 2210 1596422 7 0.245 +/-0.292 1.00 pCi/g MJHl 09/29/16 0630 1598663 8 0.194 +/-0.225 pCi/g MXRl 10/03/16 0557 1596254 9 0.0717 +/-0.0895 pCi/g 0.544 +/-0.914 pCi/g 0.0405 +/-0.195 pCi/g 0.0349 +/-0.0403 0.100 pCi/g 0.0288 +/-0.034 pCi/g 0.0765 +/-0.0928 pCi/g 0.0534 +/-0.150 pCi/g 0.0525 +/-0.166 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.2.4 Sample ID: 405235066 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOO 1 October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.6 +/-1.47 Protactinium-231 HU!h 0.00 +/-0.617 Radium-226 Hh 0.903 +/-0.191 Radium-228 Hh 0.861 +/-0.392 Thallium-208 Hh 0.347 +/-0.0826 Tin-126 HU!h 0.00 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 26.5 Beta Hh 28.9 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.452 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.47 Liquid Scint C/4, Solid "Dry Weight Corrected" +/-0.217 +/-6.87 +/-4.26 +/-0.594 +/-1.92 0.590 0.658 0.0939 0.209 0.0529 0.150 3.83 2.69 1.24 3.25 Carbon-14 HUh -0.27 +/-0.641 I.I I Liquid Sein! Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.000319 +/-0.867 1.55 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 299 of 5809 0.241 +/-1.63 pCi/g 0.297 +/-0.634 pCi/g 0.0405 +/-0.195 pCi/g 0.0892 +/-0.395 pCi/g 0.0231 +/-0.0839 pCi/g 0.0709 +/-0.217 pCi/g 1.26 +/-8.56 4.00 pCi/g JXC9 09/22/16 1240 1597817 10 1.14 +/-6.06 10.0 pCi/g 0.552 +/-0.594 2.00 pCi/g BXFl 09/28/16 0851 1597804 II 1.57 +/-1.92 6.00 pCi/g TXP3 09/26/16 2123 1598096 12 0.544 +/-0.641 2.00 pCi/g TXJl 09/29/16 0740 1598082 13 0.727 +/-0.867 5.00 pCi/g CXS7 09/20/16 0816 1597417 14 Analyst Date Time Prep Batch LYTl 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.A.R.2.4 Sample ID: 405235066 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 300 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 90.3 (15%-125%) 1596418 70.9 (15%-125%) 1596418 63.3 (15%-125%) 1596420 74.4 (15%-125%) 1596417 86.6 (15%-125%) 1599981 86 (15%-125%) 1596422 90.3 (15%-125%) 1597804 84.2 (25%-125%) 1597417 94.1 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.6.2 Sample ID: 405235067 Matrix: Soil Collect Date: ll-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 13.9% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 13.9 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0221 +/-0.0435 0.0603 Plutonium-239/240 HUh -0.006 +/-0.0265 0.0693 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0006 +/-0.0445 0.0989 Uranium-233/234 Hh 0.563 +/-0.188 0.142 Uranium-235/236 HUh 0.00459 +/-0.0523 O.l ll Uranium-238 Hh 0.708 +/-0.203 0.106 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.068 +/-0.305 0.596 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.23 +/-0.757 0.870 Thorium-229 HUh -0.0317 +/-0.140 0.366 Thorium-230 Hh 0.990 +/-0.537 0.434 Thorium-232 Hh 0.853 +/-0.482 0.197 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0776 +/-0.214 0.370 Curium-242 Hh 0.00 +/-0.407 0.606 Curium-243/244 Hh 0.00 +/-0.124 0.184 Curium-245/246 Hh 0.00 +/-0.140 0.208 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.892 +/-4.48 7.73 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" lodine-129 HUh -0.0119 +/-0.227 0.508 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.121 +/-0.219 0.403 Antimony-125 HUh -0.0314 +/-0.117 0.216 Bismuth-212 HUlh 0.00 +/-0.888 1.52 Bismuth-214 Hh 0.724 +/-0.186 0.121 Cesium-137 HUih 0.00 +/-0.0428 0.0368 Cobalt-60 HUh -0.0303 +/-0.0431 0.07i5 Europium-154 HUh -0.0476 +/-0.127 0.234 Lead-212 Hh 0.922 +/-0.118 0.0879 Lead-214 Hh 1.01 +/-0.209 0.324 Page 301 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL

Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 I O.oJ 13 +/-0.0436 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0159 +/-0.0266 1.00 pCi/g 0.0269 +/-0.0446 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0497 +/-0.209 1.00 pCi/g 0.034 +/-0.0523 1.00 pCi/g 0.0314 +/-0.234 1.00 pCi/g 0.170 +/-0.305 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.304 +/-0.785 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.0838 +/-0.140. 1.00 pCi/g 0.118 +/-0.558 1.00 pCi/g 0.00 +/-0.500 1.00 pCi/g 0.0943 +/-0.214 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.408 1.00 pCi/g 0.00 +/-0.124 1.00 pCi/g 0.00 +/-0.140 1.00 pCi/g 3.78 +/-4.48 15.0 pCi/g KXB2 09/21/16 2341 1596422 7 0.180 +/-0.227 1.00 pCi/g MJHl 09/29/16 0634 1598663 8 0.184 +/-0.226 pCi/g MXRl 10/03/16 0558 1596254 9 0.0976 +/-0.118 pCi/g 0.702 +/-1.20 pCi/g 0.0532 +/-0.195 pCi/g 0.0141 +/-0.0432 0.100 pCi/g 0.0288 +/-0.0452 pCi/g 0.097 +/-0.129 pCi/g 0.0404 +/-0.147 pCi/g 0.156 +/-0.226 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.6.2 Sample ID: 405235067 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.2 +/-1.46 0.699 Protactinium-231 HU!h 0.00 +/-1.15 0.755 Radium-226 Hh 0.724 +/-0.186 0.121 Radium-228 Hh 0.691 +/-0.281 0.255 Thallium-208 Hh 0.223 +/-0.0744 0.0602 Tin-126 HU!h 0.00 +/-0.0967 0.0947 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 22.7 +/-4.31 3.31 Beta Hh 30.6 +/-2.98 2.70 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.464 +/-0.743 1.52 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.39 +/-2.57 4.37 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.0984 +/-0.678 1.17 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.152 +/-0.867 1.57 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 302 of 5809 0.281 +/-1.74 pCi/g 0.343 +/-1.17 pCi/g 0.0532 +/-0.195 pCi/g 0.109 +/-0.292 pCi/g 0.0263 +/-0.0768 pCi/g 0.0448 +/-0.0982 pCi/g 1.38 +/-6.19 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.27 +/-5.17 10.0 pCi/g 0.678 +/-0.743 2.00 pCi/g BXFl 09/28/16 0850 1597804 II 2.11 +/-2.57 6.00 pCi/g TXP3 09/26/16 2258 1598096 12 0.571 +/-0.678 2.00 pCi/g TXJI 09129116 0851 1598082 13 0.737 +/-0.867 5.00 pCi/g CXS7 09/20/16 0843 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.6.2 Sample ID: 405235067 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 303 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 92 (15%-125%) 1596418 83.9 (15%-125%) 1596418 96.3 (15%-125%) 1596420 81.7 (15%-125%) 1596417 105 (15%-125%) 1599981 118 (15%-125%) 1596422 92 (15%-125%) 1597804 84.2 (25%-125%) 1597417 95 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.4.2 Sample ID: 405235068 Matrix: Soil Collect Date: 11-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 13.9% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 13.9 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00587 +/-0.0506 0.117 Plutonium-239/240 HUh 0.00778 +/-0.0886 0.188 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0294 +/-0.0415 0.136 Uranium-233/234 Hh 0.783 +/-0.224 0.147 Uranium-235/236 Hh 0.073 +/-0.0807 0.107 Uranium-238 Hh I.OJ +/-0.245 0.0839 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.126 +/-0.332 0.598 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.974 +/-0.691 0.702 Thorium-229 HUh 0.0583 +/-0.219 0.368 Thorium-230 Hh 0.958 +/-0.565 0.424 Thorium-232 Hh 0.498 +/-0.428 0.423 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0838 +/-0.159 0.490 Curium-242 Hh 0.00 +/-0.469 0.698 Curium-243/244 HUh -0.034 +/-0.150 0.392 Curium-2451246 HXh 0.239 +/-0.315 0.239 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -7.65 +/-8.52 14.9 Rad Gamma Spec Analysis Gamma IJ 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0393 +/-0.125 0.577 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.105 +/-0.287 0.502 Antimony-125 HUh -0.0441 +/-0.123 0.235 Bismuth-212 HUh 0.594 +/-0.766 1.58 Bismuth-214 Hh 0.862 +/-0.255 0.160 Cesium-137 HUih 0.00 +/-0.0803 0.0907 Cobalt-60 HUh -0.0195 +/-0.0654 0.123 Europium-154 HUh 0.0529 +/-0.132 0.305 Lead-212 Hh 0.892 +/-0.184 0.130 Lead-214 Hh 1.08 +/-0.262 0.158 Page 304 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 I 0.0219 +/-0.0508 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0577 +/-0.0887 1.00 pCi/g 0.0416 +/-0.0416 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0509 +/-0.260 1.00 pCi/g 0.0305 +/-0.0817 1.00 pCi/g 0.0192 +/-0.299 1.00 pCi/g 0.178 +/-0.333 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.199 +/-0.712 1.00 pCi/g KXB2 09/19/16 1742 1596417 5 0.0689 +/-0.219 1.00 pCi/g 0.0972 +/-0.585 1.00 pCi/g 0.0969 +/-0.435 1.00 pCi/g 0.140 +/-0.159 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.470 1.00 pCi/g 0.0898 +/-0.151 1.00 pCi/g 0.00 +/-0.317 1.00 pCi/g 7.31 +/-8.52 15.0 pCi/g KXB2 09/22/16 0225 1596422 7 0.148 +/-0.126 1.00 pCi/g MJHI 09/29/16 0645 1598663 8 0.225 +/-0.292 pCi/g MJ(RI 10/03/16 0605' 1596254 9 0.102 +/-0.125 pCi/g 0.701 +/-0.812 pCi/g 0.0688 +/-0.258 pCi/g 0.0388 +/-0.0805 0.100 pCi/g 0.051 +/-0.066 pCi/g 0.124 +/-0.134 pCi/g 0.0597 +/-0.190 pCi/g 0.0696 +/-0.266 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.4.2 Sample ID: 405235068 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 10.7 +/-1.72 Protactinium-231 HUh 0.479 +/-0.591 Radium-226 Hh 0.862 +/-0.255 Radium-228 Hh 0.598 +/-0.299 Thallium-208 Hh 0.333 +/-0.0999 Tin-126 HUih 0.00 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 23.1 Beta Hh 26.6 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.093 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 1.96 Liquid Scint Cl4, Solid "Dry Weight Corrected" +/-0.132 +/-4.69 +/-3.05 +/-0.975 +/-2.06 0.196 1.26 0.160 0.410 0.0792 0.110 3.78 3.26 1.78 3.45 Carbon-14 HUh 0.00569 +/-0.689 1.18 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.347 +/-0.969 1.78 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 IO II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-30.0, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-0 I Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 305 of 5809 0.00 +/-1.81 pCi/g 0.579 +/-0.637 pCi/g 0.0688 +/-0.258 pCi/g 0.178 +/-0.301 pCi/g 0.0338 +/-0.101 pCi/g 0.051 +/-0.133 pCi/g 1.58 +/-6.59 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.55 +/-4.82 10.0 pCi/g 0.825 +/-0.975 2.00 pCi/g BXFI 09/27/16 1539 1597804 II 1.66 +/-2.06 6.00 pCi/g TXP3 09/27/16 0032 1598096 12 0.578 +/-0.689 2.00 pCi/g TXJ! 09/29/16 1002 1598082 13 0.834 +/-0.969 5.00 pCi/g CXS7 09/20/16 0911 1597417 14 Analyst Date Time Prep Batch LYTl 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2A.R.4.2 Sample ID: 405235068 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (l .96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 306 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 47.7 (15%-125%) 1596418 83.6 (15%-125%) 1596418 87.7 (15%-125%) 1596420 83.7 (15%-125%) 1596417 93.6 (15%-125%) 1599981 100 (15%-125%) 1596422 47.7 (15%-125%) 1597804 89.6 (25%-125%) 1597417 89.5 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R. I .4 Sample ID: 405235069 Matrix: Soil Collect Date: 16-DEC-15 Receive Date: 06-SEP-I 6 Collector: Client Moisture: I 0.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 10.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00999 +/-0.0302 0.0847 Plutonium-239/240 HUh -0.0165 +/-0.0313 0.0967 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0123 +/-0.055 0.107 Uranium-233/234 Hh 0.829 +/-0.206 0.0897 Uranium-235/236 Hh 0.0385 +l-0.0506 0.0385 Uranium-238 Hh 0.816 +/-0.202 0.0613 Alphaspec Np237, Solid Dry Weight Corrected" Neptunium-237 HUh 0.0573 +/-0.215 0.361 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.52 +/-0.758 0.599 Thorium-229 Hh 0.166 +/-0.263 0.364 Thorium-230 Hh 0.889 +/-0.520 0.485 Thorium-232 Hh 0.784 +/-0.463 0.196 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh 0.0373 +/-0.207 0.398 Curium-242 Hh 0.00 +/-0.472 0.703 Curium-243/244 HUh -0.0873 +/-0.165 0.510 Curium-245/246 Hh 0.0821 +/-0.231 0.246 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -5.61 +/-4.94 8.72 Rad Gamma Spec Analysis Gamma Il29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0542 +/-0.386 0.892 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium:227 HUh -0.03 +/-0.228 0.435 Antimony-125 HUh 0.0365 +/-0.0967 0.194 Bismuth-212 HUih 0.00 +/-1.22 0.857 Bismuth-214 Hh 0.993 +/-0.166 0.123 Cesium-137 HUh -0.00406 +/-0.0411 0.0794 Cobalt-60 HUh 0.0163 +/-0.0365 0.0827 Europium-154 HUh 0.020 +/-0.131 0.269 Lead-212 Hh 0.870 +/-0.120 0.094 Lead-214 Hh 1.22 +/-0.202 0.344 Page 307 of 5809 Report Date: October 4, 2016 Project: MJWCOOll5 Client ID: MJWCOOI Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTl 09/08/16 0846 1596246 1 0.0216 +/-0.0302 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0277 +/-0.0314 1.00 pCi/g 0.0308 +l-0.055 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0257 +/-0.244 1.00 pCi/g 0.00 +/-0.051 1.00 pCi/g 0.0115 +/-0.240 1.00 pCi/g 0.0676 +/-0.215 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.170 +/-0.800 1.00 pCi/g KXB2 09/19/16 1742 1596417 5 0.0834 +/-0.264 1.00 pCi/g 0.144 +/-0.539 1.00 pCi/g 0.00 +/-0.479 1.00 pCi/g 0.0911 +/-0.208 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.473 1.00 pCi/g 0.146 +/-0.166 1.00 pCi/g 0.00 +/-0.231 1.00 pCi/g 4.26 +/-4.94 15.0 pCi/g KXB2 09/22/16 0356 1596422 7 0.316 +/-0.386 1.00 pCi/g MJHl 09/29/16 0646 1598663 8 0.201 +/-0.228 pCi/g MXRl 10/03/16 0605 1596254 9 0.0871 +/-0.0981 pCi/g 0.373 +/-1.22 pCi/g 0.0545 +/-0.171 pCi/g 0.0357 +/-0.0412 0.100 pCi/g 0.0347 +/-0.0373 pCi/g 0.117 +/-0.132 pCi/g 0.0437 +/-0.129 pCi/g 0.167 +/-0.208 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.l.4 Sample ID: 405235069 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dry Weight Corrected" Potassium-40 Hh 13.8 +/-1.63 0.635 Protactinium-231 HUlh 0.00 +/-0.851 0.783 Radium-226 Hh 0.993 +/-0.166 0.123 Radium-228 Hh 1.30 +/-0.286 0.224 Thallium-208 Hh 0.305 +/-0.0768 0.061 Tin-126 HUh 0.024 +/-0.150 0.177 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 17.0 +/-4.04 3.77 Beta Hh 21.4 +/-2.76 3.02 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.526 +/-0.831 1.45 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 2.26 +/-2.00 3.33 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.00499 +/-0.674 1.16 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.183 +/-0.879 1.55 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-O!-R EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 308 of 5809 0.256 +/-1.78 pCi/g 0.359 +l-0.905 pCi/g 0.0545 +/-0.171 pCi/g 0.095 +/-0.294 pCi/g 0.0269 +/-0.0179 pCi/g 0.0842 +/-0.151 pCi/g 1.59 +/-5.23 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.42 +/-4.07 10.0 pCi/g 0.626 +/-0.837 2.00 pCi/g BXFI 09/27/16 1539 1597804 II 1.61 +/-2.00 6.00 pCi/g TXP3 09/27/16 0316 1598096 12 0.565 +/-0.674 2.00 pCi/g TXJI 09129116 1114 1598082 13 0.727 +/-0.879 5.00 pCi/g CXS7 09/20/16 0938 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R. l .4 Sample ID: 405235069 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu24 l, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 309 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 80.3 (15%-125%) 1596418 83.8 (15%-125%) 1596418 97.5 (15%-125%) 1596420 89.2 (15%-125%) 1596417 96.3 (15%-125%) 1599981 98.1 (15%-125%) 1596422 80.3 (15%-125%) 1597804 81.5 (25%-125%) 1597417 89.3 (15%-125%) GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: . Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.3.2 Sample ID: 405235070 Matrix: Soil Collect Date: l l-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 18.9% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 18.9 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00372 +/-0.0321 0.0744 Plutonium-239/240 HUh -0.0074 +/-0.0327 0.0854 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0215 +/-0.0346 0.110 Uranium-233/234 Hh 0.602 +/-0.175 0.0778 Uranium-235/236 HUh 0.0133 +/-0.0454 0.0841 Uranium-238 Hh 0.802 +/-0.202 0.0839 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.0843 +/-0.237 0.253 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.794 +/-0.651 0.815 Thorium-229 Hh 0.180 +/-0.286 0.396 Thorium-230 Hh 0.428 +/-0.372 0.214 Thorium-232 Hh 1.28 +/-0.609 0.213 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.00 +/-0.134 0.200 Curium-242 Hh 0.00 +/-0.448 0.667 Curium-243/244 Hh 0.0677 +/-0.190 0.203 Curium-245/246 Hh 0.153 +/-0.261 0.229 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -3.56 +/-5.28 9.21 Rad Gamma Spec Analysis Gamma IJ 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.118 +/-0.181 0.338 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.00526 +/-0.216 0.395 Antimony-125 HUh -0.0182 +/-0.0902 0.157 Bismuth-212 HUih 0.00 +/-0.930 1.28 Bismuth-214 Hh 0.966 +/-0.176 0.105 Cesium-137 HUih 0.00 +/-0.071 0.0657 Cobalt-60 HUh 0.0239 +/-0.0296 0.0753 Europium-154 HUh 0.0236 +/-0.0961 0.204 Lead-212 Hh 0.836 +/-0.110 0.0758 Lead-214 Hh 1.00 +/-0.169 0.100 Page 310 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 1 0.0139 +/-0.0322 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0196 +/-0.0328 1.00 pCi/g 0.0328 +/-0.0347 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0198 +/-0.200 1.00 pCi/g 0.0229 +/-0.0454 1.00 pCi/g 0.0228 +/-0.239 1.00 pCi/g 0.00 +/-0.237 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.266 +/-0.667 1.00 pCi/g KXB2 09/19/16 1742 1596417 5 0.0908 +/-0.288 1.00 pCi/g 0.00 +/-0.378 1.00 pCi/g 0.00 +/-0.642 1.00 pCi/g 0.00 +/-0.135 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.449 1.00 pCi/g 0.00 +/-0.190 1.00 pCi/g 0.00 +/-0.262 1.00 pCi/g 4.50 +/-5.28 15.0 pCi/g KXB2 09/22/16 0527 1596422 7 0.119 +/-0.189 1.00 pCi/g Mllil 09/29/16 0653 1598663 8 0.182 +/-0.216 pCi/g MJffil 10l03/16 0608 1596254 9 0.0694 +/-0.0905 pCi/g 0.591 +/-1.11 pCi/g 0.0461 +/-0.181 pCi/g 0.0292 +/-0.0711 0.100 pCi/g 0.0318 +/-0.0316 pCi/g 0.0866 +/-0.0967 pCi/g 0.0348 +/-0.119 pCi/g 0.045 +/-0.174 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.3.2 Sample ID: 405235070 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.7 +/-1.35 Protactinium-231 HUh -0.0614 +/-0.403 Radium-226 Hh 0.966 +/-0.176 Radium-228 Hh 0.566 +/-0.322 Thallium-208 Hh 0.258 +/-0.0727 Tin-126 Hh 0.101 +/-0.116 Rad Gas Flow Proportional Counting GFPC, Gross A/B, solid "Dry Weight Corrected" Alpha Hh 15.2 +/-3.46 Beta Hh 23.8 +/-2.74 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.589 +/-0.442 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid Dry Weight Corrected" Tritium HUh 1.56 +/-2.30 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.148 +/-0.740 Liquid Scint Tc99, Solid Dry Weight Corrected" Technetium-99 HUh 0.0532 +/-1.00 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE H-:fL HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HA.SL 300, 4.5.2.3/Ga-Ol-R 0.515 0.715 0.105 0.222 0.0577 0.105 3.10 2.70 1.12 3.90 1.27 1.78 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 311 of 5809 0.204 +/-1.48 pCi/g 0.327 +/-0.404 pCi/g 0.0461 +/-0.181 pCi/g 0.0957 +/-0.323 pCi/g 0.0256 +/-0.0735 pCi/g 0.0493 +/-0.117 pCi/g 1.31 +/-4.58 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.26 +/-4.30 10.0 pCi/g 0.477 +/-0.442 2.00 pCi/g BXFl 09/28/16 0850 1597804 II 1.88 +/-2.30 6.00 pCi/g TXP3 09/27/16 0450 1598096 12 0.624 +/-0.740 2.00 pCi/g TXJl 09/29/16 1225 1598082 13 0.836 +/-1.00 5.00 pCi/g CXS7 09/20/16 1006 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.3.2 Sample ID: 405235070 Certificate of Analysis Report Date: Project: MJWCOO 115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer . Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 312 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 78.8 (15%-125%) 1596418 89.3 (15%-125%) 1596418 93.4 (15%-125%) 1596420 81.2 (15%-125%) 1596417 93.6 (15%-125%) 1599981 96.8 (15%-125%) 1596422 78.8 (15%-125%) 1597804 86.9 (25%-125%) 1597417 93.4 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.4.2 Sample ID: 405235071 Matrix: Soil Collect Date: ll-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 16.6% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 22 I 6 % Moisture "As Received" Moisture 16.6 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0511 +/-0.0602 0.0651 Plutonium-239/240 Hh 0.0373 +/-0.0537 0.0647 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00297 +/-0.0446 0.104 Uranium-233/234 Hh 0.531 +/-0.166 0.0891 Uranium-235/236 HUh 0.0168 +/-0.0527 0.0987 Uranium-238 Hh 0.693 +/-0.187 0.0703 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 Hh 0.186 +/-0.366 0.507 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 0.306 +/-0.368 0.515 Thorium-229 HUh -0.0128 +/-0.111 0.256 Thorium-230 Hh 0.307 +/-0.279 0.256 Thorium-232 Hh 0.425 +/-0.313 0.159 Am24I, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0316 +/-0.140 0.365 Curium-242 Hh 0.00 +/-0.443 0.659 Curium-243/244 HUh -0.0481 +/-0.145 0.408 Curium-245/246 Hh 0.151 +/-0.258 0.226 Liquid Sein/ Pu24I, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.832 +/-4.89 8.44 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.283 +/-0.260 0.787 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0687 +/-0.212 0.432 Antimony-125 HUh -0.0358 +/-0.106 0.199 Bismuth-212 HU!h 0.00 +/-0.987 0.994 Bismuth-214 Hh 0.746 +/-0.173 0.107 Cesium-137 HU!h 0.00 +/-0.0625 0.0605 Cobalt-60 HUh 0.0286 +/-0.0363 0.089 Europium-154 HUh -0.0159 +/-0.0894 0.186 Lead-212 Hh 0.775 +/-0.121 0.0929 Lead-214 Hh 1.02 +/-0.192 0.334 Page 313 of 5809 Report Date: October4, 2016 Project: MJWC00115 Client ID: MJWCOOl Le

TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 1 0.0122 +/-0.0606 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0121 +/-0.0539 1.00 pCi/g 0.0298 +/-0.0447 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0255 +/-0.186 1.00 pCi/g 0.0302 +/-0.0528 1.00 pCi/g 0.0161 +/-0.217 1.00 pCi/g 0.0949 +/-0.366 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.152 +/-0.373 1.00 pCi/g KXB2 09/19/16 1750 1596417 5 0.0479 +/-0.111 1.00 pCi/g 0.0478 +/-0.282 1.00 pCi/g 0.00 +/-0.319 1.00 pCi/g 0.0836 +/-0.140 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.444 1.00 pCi/g 0.104 +/-0.146 1.00 pCi/g 0.00 +/-0.259 1.00 pCi/g 4.13 +/-4.89 15.0 pCi/g KXB2 09/22/16 0658 1596422 7 0.309 +/-0.291 1.00 pCi/g MJHl 09/29/16 0704 1598663 8 0.198 +/-0.215 pCi/g MXRl 10/03/16 0645 1596254 9 0.089 +/-0.108 pCi/g 0.437 +/-0.989 pCi/g 0.0461 +/-0.176 pCi/g 0.0258 +/-0.0627 0.100 pCi/g 0.0373 +/-0.0386 pCi/g 0.0741 +/-0.0897 pCi/g 0.0428 +/-0.128 pCi/g 0.161 +/-0.196 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.4.2 Sample ID: 405235071 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.3 +/-1.61 Protactinium-231 HU!h 0.00 +/-1.18 Radium-226 Hh 0.746 +/-0.173 Radium-228 Hh 0.861 +/-0.261 Thallium-208 Hh 0.217 +/-0.0618 Tin-126 HU!h 0.00 +/-0.126 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 14.8 +/-3.76 Beta Hh 19.0 +/-2.60 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.325 +/-0.832 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.231 +/-2.58 Liquid Scint CJ 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.112 +/-0.731 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.444 +/-1.12 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.619 0.846 0.107 0.220 0.0533 0.155 3.43 2.90 1.66 4.50 1.25 1.95 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 931 O/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 314of5809 0.243 +/-1.73 pCi/g 0.387 +l-1.19 pCi/g 0.0461 +/-0.176 pCi/g 0.0917 +/-0.264 pCi/g 0.0227 +/-0.0625 pCi/g 0.0732 +/-0.127 pCi/g 1.42 +/-4.81 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.36 +/-3.72 10.0 pCi/g 0.737 +/-0.832 2.00 pCi/g BXFI 09/27/16 1539 1597804 II 2.17 +/-2.58 6.00 pCi/g TXP3 09/27/16 0625 1598096 12 0.612 +/-0.731 2.00 pCi/g TXJI 09129116 1336 1598082 13 0.917 +/-1.12 5.00 pCi/g CXS7 09/20/16 I 033 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.4.2 Sample ID: 405235071 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 315 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 83.6 (15%-125%) 1596418 ' 86.7 (15%-125%) 1596418 96.7 (15%-125%) 1596420 62 (15%-125%) 1596417 116 (15%-125%) 1599981 91.4 (15%-125%) 1596422 83.6 (15%-125%) 1597804 86.9 (25%-125%) 1597417 90.9 (15%-125%)

GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.2.4 Sample ID: 405235072 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 8 .17% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 8.17 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0,0114 +/-0.0426 0.0717 Plutonium-239/240 HUh 0.0113 +/-0.0424 0.0712 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0085 +/-0.0472 0.0905 Uranium-233/234 Hh 0.939 +/-0.244 0.154 Uranium-235/236 Hh 0.107 +l-0.0905 0.0999 Uranium-238 Hh 0.711 +/-0.208 0.0996 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0837 +/-0.286 0.530 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.09 +/-0.658 0.646 Thorium-229 Hh 0.127 +/-0.218 0.190 Thorium-230 Hh 0.950 +/-0.497 0.190 Thorium-232 Hh 0.679 +/-0.431 0.303 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0148 +/-0.222 0.518 Curium-242 Hh 0.00 +/-0.488 0.726 Curium-2431244 HUh -0.0718 +/-0.166 0.493 Curium-245/246 Hh 0.00 +/-0.170 0.253 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -0.293 +/-5.63 9.68 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" Iodine-129 HUh 0.00515 +/-0.352 0.761 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0734 +/-0.182 0.333 Antimony-125 HUh -0.00985 +/-0.0726 0.145 Bismuth-212 HUih 0.00 . +/-0.603 1.05 Bismuth-214 Hh 0.986 +/-0.149 0.0982 Cesium-137 HUh 0.0159 +/-0.0264 0.0564 Cobalt-60 HUh -0.00332 +/-0.0326 0.0644 Europium-154 HUh 0.00365 +/-0.0927 0.187 Lead-212 Hh 0.929 +/-0.102 0.0758 Lead-214 Hh 1.10 +/-0.150 0.0958 Page 316of5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent L YT! 09/08/16 0846 1596246 1 0.0134 +/-0.0427 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0133 +/-0.0424 1.00 pCi/g 0.0207 +/-0.0473 *1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0542 +/-0.291 1.00 pCi/g 0.0272 +/-0.0923 1.00 pCi/g 0.0271 +/-0.240 1.00 pCi/g 0.144 +/-0.286 1.00 pCi/g KXB2 09/22/16 0959 1596420 4 0.198 +/-0.684 1.00 pCi/g KXB2 09/19/16 1749 1596417 5 0.00 +/-0.218 1.00 pCi/g 0.00 +l-0.519 1.00 pCi/g 0.0566 +/-0.444 1.00 pCi/g 0.148 +/-0.222 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.489 1.00 pCi/g 0.134 +/-0.167 1.00 pCi/g 0.00 +/-0.170 1.00 pCi/g 4.73 +/-5.63 15.0 pCi/g KXB2 09/22/16 0829 1596422 7 0.289 +/-0.352 1.00 pCi/g MJHl 09129/16 0711 1598663 8 0.153 +/-0.185 pCi/g MXRI 10/03/16 0645 1596254 9 0.0648 +/-0.0727 pCi/g 0.483 +/-0.832 pCi/g 0.0437 +/-0.155 pCi/g 0.0251 +/-0.0274 0.100 pCi/g 0.0271 +/-0.0326 pCi/g 0.0802 +/-0.0927 pCi/g 0.0352 +/-0.114 pCi/g 0.0434 +/-0.157 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -WWW.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.2.4 Sample ID: 405235072 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 15.0 +/-1.44 0.374 Protactinium-231 HUh 0.0695 +/-0.409 0.708 Radium-226 Hh 0.986 +/-0.149 0.0982 Radium-228 Hh 1.01 +/-0.239 0.206 Thallium-208 Hh 0.297 +/-0.0609 0.0562 Tin-126 HUih 0.00 +/-0.0488 0.0967 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 18.3 +/-4.04 3.01 Beta Hh 22.9 +/-2.72 2.74 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.264 +/-0.826 1.64 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.772 +/-1.90 3.26 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.384 +/-0.652 1.10 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.0651 +/-0.850 1.53 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I !-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 317 of 5809 0.141 +/-1.64 pCi/g 0.328 +/-0.411 pCi/g 0.0437 +/-0.155 pCi/g 0.0898 +/-0.245 pCi/g 0.0253 +/-0.0622 pCi/g 0.0463 +/-0.0715 pCi/g 1.20 +/-5.37 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.29 +/-4.18 10.0 pCi/g 0.725 +/-0.826 2.00 pCi/g BXFI 09/27/16 1540 1597804 II 1.57 +/-1.90 6.00 pCi/g TXP3 09/27/16 0758 1598096 12 0.540 +/-0.652 2.00 pCi/g TXJI 09/29/16 1447 1598082 13 0.717 +/-0.850 5.00 pCi/g CXS7 09/20/16 1101 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.2.4 Sample ID: 405235072 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 318 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 73.7 (15%-125%) 1596418 73.2 (15%-125%) 1596418 87.4 (15%-125%) 1596420 87.5 (15%-125%) 1596417 97.2 (15%-125%) 1599981 98.9 (15%-125%) 1596422 73.7 (15%-125%) 1597804 86.9 (25%-125%) 1597417 91.l (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.8.2 Sample ID: 405235073 Matrix: Soil Collect Date: ll-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 18.9% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 18.9 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.00657 +/-0.0365 0.070 Plutonium-239/240 Hh 0.0256 +/-0.051 0.0828 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.0192 +/-0.053 0.0918 Uranium-233/234 Hh 0.678 +/-0.202 0.104 Uranium-235/236 Hh 0.0487 +/-0.0666 0.0908 Uranium-238 Hh 0.771 +/-0.214 0.0976 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.111 +/-0.378 0.701 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.21 +/-0.790 0.731 Thorium-229 Hh 0.00 +/-0.170 0.253 Thorium-230 Hh 0.737 +/-0.525 0.404 Thorium-232 Hh 0.671 +/-0.495 0.252 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.147 +/-0.251 0.220 Curium-242 HUh -0.117 +/-0.519 1.35 Curium-243/244 HUh -0.0536 +/-0.162 0.454 Curium-245/246 Hh 0.00 +/-0.169 0.252 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh -5.28 +/-4.68 8.26 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 . HUh -0.115 +/-0.373 0.827 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0814 +/-0.233 0.409 Antimony-125 HUh -0.0602 +/-0.0947 0.173 Bismuth-212 HU!h 0.00 +/-0.513 1.15 Bismuth-214 Hh 0.849 +/-0.157 0.114 Cesium-137 Hh 0.121 +/-0.0558 0.0623 Cobalt-60 HUh -0.033 +/-0.0397 0.066 Europium-154 HUh -0.0381 +/-0.115 0.218 Lead-212 Hh 0.779 +/-0.155 0.116 Lead-214 Hh 1.06 +/-0.169 0.328 Page 319of5809 Project: Client ID: Le TPU RL Units percent 0.016 +/-0.0366 1.00 pCi/g 0.0225 +/-0.0511 1.00 pCi/g 0.0234 +/-0.053 1.00 pCi/g 0.0297 +/-0.231 1.00 pCi/g 0.0231 +/-0.0671 1.00 pCi/g 0.0266 +/-0.249 1.00 pCi/g 0.191 +/-0.378 1.00 pCi/g 0.198 +/-0.823 1.00 pCi/g 0.00 +/-0.171 1.00 pCi/g 0.0755 +/-0.541 1.00 pCi/g 0.00 +l-0.509 1.00 pCi/g 0.00 +/-0.252 1.00 pCi/g 0.310 +/-0.520 1.00 pCi/g 0.116 +/-0.162 1.00 pCi/g 0.00 +l-0.169 1.00 pCi/g 4.04 +/-4.69 15.0 pCi/g 0.278 +/-0.377 1.00 pCi/g 0.186 +/-0.236 pCi/g 0.0763 +/-0.0986 pCi/g 0.518 +/-0.601 pCi/g 0.050 +/-0.173 pCi/g 0.027 +/-0.0567 0.100 pCi/g 0.0259 +/-0.0425 pCi/g 0.0903 +/-0.116 pCi/g 0.0543 +/-0.170 pCi/g 0.158 +/-0.194 pCi/g Report Date: MJWC00115 MJWCOOl October 4, 2016 PF DF Analyst Date Time Batch Mtd. LYTI 09/08/16 0846 1596246 1 KXB2 09/17/16 1142 1596421 2 KXB2 09/17/16 1142 1596418 3 KXB2 09/22/16 0959 1596420 4 KXB2 09/19/16 1749 1596417 5 KXB2 09/22/16 1755 1599981 6 KXB2 09/22/16 1000 1596422 7 MJHl 09/29/16 0718 1598663 8 MXRl 10/03/16 0646 1596254 9 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.8.2 Sample ID: 405235073 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 11.7 +/-1.45 0.355 Protactinium-23 I HUh -0.0449 +/-0.388 0.774 Radium-226 Hh 0.849 +/-0.157 0.114 Radium-228 HUih 0.00 +/-0.334 0.520 Thallium-208 Hh 0.303 +/-0.0843 0.0603 Tin-126 HUih 0.00 +/-0.138 0.123 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 27.6 +/-5.03 3.97 Beta Hh 39.4 +/-3.28 2.74 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.27 +/-0.886 1.66 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.17 +/-2.14 3.64 Liquid Scint C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.547 +/-0.749 1.26 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.381 +/-0.970 1.78 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 IO II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 71 !OB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 320 of 5809 0.112 +/-1.76 pCi/g 0.351 +/-0.389 pCi/g 0.050 +/-0.173 pCi/g 0.242 +/-0.428 pCi/g 0.0265 +/-0.0883 pCi/g 0.0576 +/-0.139 pCi/g 1.68 +/-7.39 4.00 pCi/g JXC9 09/22/16 1357 1597817 IO 1.29 +/-6.39 10.0 pCi/g 0.765 +/-0.886 2.00 pCi/g BXFI 09/27/16 1540 1597804 11 1.75 +/-2.14 6.00 pCi/g TXP3 09/27 /I 6 0932 1598096 12 0.618 +/-0.750 2.00 pCi/g TXJI 09/29/16 1559 1598082 13 0.837 +/-0.970 5.00 pCi/g CXS7 09/20/16 1128 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.2.B.R.8.2 Sample ID: 405235073 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 321of5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 86 (15%-125%) 1596418 83.9 (15%-125%) 1596418 91.7 (15%-125%) 1596420 76 (15%-125%) 1596417 72.1 (15%-125%) 1599981 91.5 (15%-125%) 1596422 86 (15%-125%) 1597804 89.6 (25%-125%) 1597417 89.6 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: Contact: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.3.A.R.l.3 Sample ID: 405235074 Matrix: Soil Collect Date: 15-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 10.7% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 10.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.00 +l-0.050 0.0744 Plutonium-239/240 HUh 0.000986 +/-0.0731 0.162 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00986 +/-0.0298 0.0836 Uranium-233/234 Hh 0.639 +/-0.202 0.120 Uranium-235/236 HUh 0.00434 +/-0.0454 0.0947 Uranium-238 Hh 0.967 +/-0.245 0.114 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0753 +/-0.404 0.810 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh I.IO +/-0.681 0.732 Thorium-229 HUh -0.0456 +/-0.138 0.387 Thorium-230 Hh 1.04 +/-0.528 0.350 Thorium-232 Hh 0.41 I +/-0.353 0.349 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0336 +/-0.148 0.387 Curium-242 HUh -0.055 +/-0.474 I.IO Curium-243/244 HUh 0.0539 +/-0.202 0.340 Curium-245/246 Hh 0.0799 +/-0.225 0.240 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-24 I HUh -7.43 +/-8.81 15.4 Rad Gamma Spec Analysis Gamma Il 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0791 +/-0.278 0.532 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.121 +/-0.180 0.343 Antimony-125 HUh 0.0202 +/-0.0825 0.169 Bismuth-212 HU!h 0.00 +/-0.651 I.IO Bismuth-214 Hh 0.863 +/-0.198 0.115 Cesium-137 HUh 0.00388 +/-0.0311 0.061 Cobalt-60 HUh 0.0162 +/-0.0434 0.0823 Europium-I 54 HUh 0.044 +l-0.099 0.213 Lead-212 Hh 0.992 +/-0.123 0.0771 Lead-214 Hh 1.15 +/-0.193 0.112 Page 322 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent L YT! 09/08116 0846 1596246 I 0.00 +/-0.0501 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0442 +/-0.0732 1.00 pCi/g 0.0213 +/-0.0298 1.00 pCi/g KXB2 09117116 1142 1596418 3 0.0367 +/-0.228 1.00 pCi/g 0.0241 +/-0.0454 1.00 pCi/g 0.034 +/-0.292 1.00 pCi/g 0.277 +/-0.404 1.00 pCi/g KXB2 09/22116 0959 1596420 4 0.241 +/-0.705 1.00 pCi/g KXB2 09/19116 1750 1596417 5 0.0985 +/-0.138 1.00 pCi/g 0.0802 +/-0.551 1.00 pCi/g 0.080 +/-0.359 1.00 pCi/g 0.0887 +/-0.149 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.206 +/-0.475 1.00 pCi/g 0.0636 +/-0.202 1.00 pCi/g 0.00 +/-0.225 1.00 pCi/g 7.55 +/-8.81 15.0 pCi/g KXB2 09/22/16 1132 1596422 7 0.149 +/-0.280 1.00 pCi/g MJHl 09/29/16 0718 1598663 8 0.157 +/-0.189 pCi/g MXRl 10/03/16 0646 1596254 9 0.0759 +/-0.083 pCi/g 0.503 +/-0.802 pCi/g 0.0515 +/-0.201 pCi/g 0.027 +/-0.031 I 0.100 pCi/g 0.0356 +/-0.044 pCi/g 0.092 +/-0.101 pCi/g 0.0356 +/-0.134 pCi/g 0.0509 +/-0.199 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.3.A.R.l.3 Sample ID: 405235074 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 12.9 +/-1.39 0.608 Protactinium-231 HU!h 0.00 +/-0.859 0.758 Radium-226 Hh 0.863 +/-0.198 0.115 Radium-228 Hh 0.568 +/-0.335 0.255 Thallium-208 Hh 0.272 +/-0.0705 0.0556 Tin-126 HUh 0.035 +/-0.127 0.125 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 15.I +/-3.78 2.92 Beta Hh 18.7 +/-2.48 2.72 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.219 +/-0.836 1.52 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 1.82 +/-2.03 3.40 Liquid Sein! C14, Solid "Dry Weight Corrected" Carbon-14 HUh 0.332 +/-0.628 1.06 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.0722 +/-0.825 1.49 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 II 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-0 I-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-01-R EPA 900.0/SW846 9310/SM 711 OB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 323 of 5809 0.253 +/-1.54 pCi/g 0.350 +/-0.873 pCi/g 0.0515 +/-0.201 pCi/g 0.113 +/-0.337 pCi/g 0.0247 +/-0.0714 pCi/g 0.0592 +/-0.128 pCi/g 1.14 +/-4.78 4.00 pCi/g JXC9 09/22/16 1357 1597817 10 1.28 +/-3.57 10.0 pCi/g 0.679 +/-0.837 2.00 pCi/g BXFI 09/28/ 16 0854 1597804 11 1.64 +/-2.03 6.00 pCi/g TXP3 09/27/16 1106 1598096 12 0.521 +/-0.628 2.00 pCi/g TXJI 09/29/16 1710 1598082 13 0.697 +/-0.825 5.00 pCi/g CXS7 09120116 1156 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.3.A.R.l.3 Sample ID: 405235074 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: Test . ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" . ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Sein! Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Sein! Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 324 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 46 .(15%-125%) 1596418 78 (15%-125%) 1596418 104 (15%-125%) 1596420 82.3 (15%-125%) 1596417 106 (15%-125%) 1599981 92.4 (15%-125%) 1596422 46 (15%-125%) 1597804 88.3 (25%-125%) 1597417 88.9 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.4A.R.1.3 Sample ID: 405235075 Matrix: Soil Collect Date: 16-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 10.7% Parameter Qualifier Result Uncertainty* MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 10.7 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh -0.00303 +/-0.0455 0.106 Plutonium-239/240 HUh -0.0464 +/-0.0515 0.157 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0274 +/-0.0442 0.141 Uranium-233/234 Hh 0.590 +/-0.206 0.122 Uranium-235/236 Hh 0.118 +/-0.0978 0.0839 Uranium-238 Hh 0.607 +/-0.206 0.0837 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0657 +/-0.342 0.797 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.23 +/-0.843 0.877 Thorium-229 HUh -0.0432 +/-0.191 0.499 Thorium-230 Hh 0.518 +/-0.470 0.431 Thorium-232 Hh 0.426 +/-0.434 0.430 Am241, Cm Solid "Dry Weight Corrected" Americium-241 Hh 0.0986 +/-0.227 0.359 Curium-242 HUh -0.0508 +/-0.438 1.02 Curium-243/244 HUh 0.0184 +/-0.192 0.402 Curium-245/246 Hh 0.205 +/-0.295 0.356 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh -2.47 +/-5.69 9.88 Rad Gamma Spec Analysis Gamma 1129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.176 +/-0.240 0.576 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.088 +t-0.189 0.312 Antimony-125 HUh 0.00 +/-0.0907 0.150 Bismuth-212 HUh 0.00 . +/-0.481 0.968 Bismuth-214 HUh 0.00 +/-0.154 0.270 Cesium-137 HUh 0.00254 +/-0.0268 0.0519 Cobalt-60 HUh -0.00243 +/-0.0319 0.0547 Europium-154 HUh 0.0297 +/-0.0833 0.168 Lead-212 Hh 0.745 +/-0.0993 0.0717 Lead-214 Hh 1.01 +/-0.160 0.101 Page 325 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Uate Time Batch Mtd. percent LYTl 09/08/16 0846 1596246 I 0.0304 +/-0.0456 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0558 +/-0.0515 1.00 pCi/g 0.0418 +/-0.0443 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.035 +/-0.231 1.00 pCi/g 0.0157 +/-0.100 1.00 pCi/g 0.0157 +/-0.232 1.00 pCi/g 0.281 +/-0.342 1.00 pCi/g KXB2 09/22/16 1000 1596420 4 0.261 +/-0.874 1.00 pCi/g KXB2 09/19/16 1750 1596417 5 0.114 +/-0.192 1.00 pCi/g 0.0806 +/-0.478 1.00 pCi/g 0.0804 +/-0.441 1.00 pCi/g 0.0823 +/-0.227 1.00 pCi/g KXB2 09122116 1755 1599981 6 0.190 +/-0.439 1.00 pCi/g 0.102 +/-0.193 1.00 pCi/g 0.0666 +/-0.296 1.00 pCi/g 4.83 +l-5.69 15.0 pCi/g KXB2 09/22/16 1303 1596422 7 0.237 +/-0.254 1.00 pCi/g MJHI 09/29/16 0724 1598663 8 0.144 +/-0.193 pCi/g MXRl 10/03/16 0647 1596254 9 0.0687 +/-0.0997 pCi/g 0.451 +/-0.730 pCi/g 0.131 +/-0.443 pCi/g 0.0235 +/-0.0269 0.100 pCi/g 0.0237 +/-0.0319 pCi/g 0.0742 +/-0.0844 pCi/g 0.0334 +/-0.107 pCi/g 0.0467 +/-0.166 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.4A.R. l.3 Sample ID: 405235075 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.6 +/-1.12 0.404 Protactinium-231 HUh 0.00 +/-0.650 *0.596 Radium-226 HUh 0.00 +/-0.154 0.270 Radium-228 HUh 0.00 +/-0.253 0.454 Thallium-208 Hh 0.274 +/-0.0698 0.0428 Tin-126 HUh 0.00 +/-0.126 0.115 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 9.45 +/-4.22 3.42 Beta Hh 18.1 +/-3.82 3.37 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh 0.362 +/-0.940 1.69 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh -0.0471 +/-1.96 3.42 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.179 +/-0.616 1.06 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh -0.0553 +/-0.840 1.51 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 9 10 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modi.tied DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,I-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 9310/SM 71 lOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified

EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 326 of 5809 0.169 +/-1.32 pCi/g 0.275 +/-0.667 pCi/g 0.131 +/-0.443 pCi/g 0.217 +/-0.530 pCi/g 0.0192 +/-0.0707 pCi/g 0.0544 +/-0.127 pCi/g 1.04 +/-4.56 4.00 pCi/g JXC9 09/22/16 1400 1597817 10 1.44 +/-4.47 10.0 pCi/g 0.749 +/-0.943 2.00 pCi/g BXFI 09/27/16 1538 1597804 II 1.65 +/-1.96 6.00 pCi/g TXP3 09/27/16 1239 1598096 12 0.521 +/-0.616 2.00 pCi/g TXJI 09/29/16 1821 1598082 13 0.708 +/-0.840 5.00 pCi/g CXS7 09/20/16 1223 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.4A.R.l.3 Sample ID: 405235075 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americ\um-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 327 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 76.7 (15%-125%) 1596418 68.7 (15%-125%) 1596418 75.8 (15%-125%) 1596420 88.4 (15%-125%) 1596417 87.7 (15%-125%) 1599981 104 (15%-125%) 1596422 76.7 (15%-125%) 1597804 88.3 (25%-125%) 1597417 95.4 (15%-125%)

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.4A.R.4.2 Sample ID: 405235076 Matrix: Soil Collect Date: l l-DEC-15 Receive Date: 06-SEP-l 6 Collector: Client Moisture: 20.5% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture As Received" Moisture 20.5 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-23 8 Hh 0.0353 +/-0.0448 0.0556 Plutonium-239/240 HUh 0.0104 +/-0.0355 0.0658 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh 0.00935 +/-0.0604 0.124 Uranium-233/234 Hh 0.837 +/-0.207 0.0848 Uranium-235/236 Hh 0.0196 +/-0.0451 0.0715 Uranium-238 Hh 0.769 +/-0.197 0.0617 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0735 +/-0.248 0.645 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.33 +/-0.790 0.756 Thorium-229 HUh 0.0424 +/-0.274 0.561 Thorium-230 Hh 0.856 +/-0.564 0.586 Thorium-232 Hh 0.905 +/-0.534 0.226 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0335 +/-0.148 0.386 Curium-242 Hh 0.00 +/-0.469 0.698 Curium-243/244 HUh -0.034 +/-0.150 0.392 Curium-245/246 Hh 0.160 +/-0.273 0.239 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.12 +/-4.00 6.92 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh -0.101 +/-0.349 0.554 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.157 +/-0.200 0.369 Antimony-125 HUh -0.0336 +/-0.0908 0.169 Bismuth-212 HUih 0.00 +/-0.702 1.08 Bismuth-214 Hh 0.867 +/-0.167 0.106 Cesium-137 HUih 0.00 +/-0.0553 0.0518 Cobalt-60 HUh 0.0204 +/-0.0296 0.0693 Europium-154 HUh -0.0324 +/-0.109 0.206 Lead-212 Hh 0.807 +/-0.107 0.0865 Lead-214 Hh 1.07 +/-0.163 0.106 Page 328 of 5809 Report Date: October4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 I 0.0127 +/-0.0449 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0179 +/-0.0355 1.00 pCi/g 0.0367 +/-0.0604 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0231 +/-0.247 1.00 pCi/g 0.0164 +/-0.0452 1.00 pCi/g 0.0115 +/-0.233 1.00 pCi/g 0.203 +/-0.249 1.00 pCi/g KXB2 09/22/16 1000 1596420 4 0.228 +/-0.824 1.00 pCi/g KXB2 09/19/16 1750 1596417 5 0.167 +/-0.274 1.00 pCi/g 0.180 +/-0.581 1.00 pCi/g 0.00 +/-0.555 1.00 pCi/g 0.0886 +/-0.148 1.00 pCi/g KXB2 09/22/16 1755 1599981 6 0.00 +/-0.470 1.00 pCi/g 0.0898 +/-0.150 1.00 pCi/g 0.00 +/-0.274 1.00 pCi/g 3.38 +/-4.00 15.0 pCi/g KXB2 09/22/16 1434 1596422 7 0.250 +/-0.352 1.00 pCi/g MJHI 09/29/16 0801 1598663 8 0.170 +/-0.213 pCi/g MXRI 10/03/16 0647 1596254 9 0.0761 +/-0.092 pCi/g 0.497 +/-0.779 pCi/g 0.0471 +/-0.171 pCi/g 0.0225 +/-0.0554 0.100 pCi/g 0.0293 +/-0.031 pCi/g 0.0886 +/-0.110 pCi/g 0.0403 +/-0.115 pCi/g 0.0479 +/-0.169 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.4A.R.4.2 Sample ID: 405235076 Certificate of Analysis Report Date: Project: MJWCOOl 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid Dry Weight Corrected" Potassium-40 Hh 11.5 +/-1.31 Protactinium-231 HUih 0.00 +/-0.535 Radium-226 Hh 0.867 +/-0.167 Radium-228 Hh 0.734 +/-0.264 Thallium-208 Hh 0.219 +/-0.0714 Tin-126 HUh 0.0254 +/-0.111 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 8.56 +/-3.96 Beta Hh 16.5 +/-3.53 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 Hh 0.629 +/-0.706 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium Hh 3.03 +/-2.39 Liquid Scint Cl4, Solid "Dry Weight Corrected" Carbon-14 HUh -0.000296 +/-0.705 Liquid Scini Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.0528 +/-1.01 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-01 Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.509 . 0.609 0.106 0.199 0.0497 0.112 3.55 3.04 1.18 3.96 1.21 1.79 2 3 4 5 6 7 8 9 10 11 12 13 14 EPA 900.0/SW846 9310/SM 71108 Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 329 of 5809 0.206 +/-1.44 pCi/g 0.276 +/-0.565 pCi/g 0.0471 +/-0.171 pCi/g 0.0855 +/-0.267 pCi/g 0.0218 +/-0.072 pCi/g 0.0534 +/-0.112 pCi/g 1.14 +/-4.31 4.00 pCi/g JXC9 09/22/16 1400 1597817 10 1.29 +/-4.31 10.0 pCi/g 0.525 +/-0.715 2.00 pCi/g BXFl 09/28/16 0854 1597804 11 1.91 +/-2.39 6.00 pCi/g TXP3 09/27/16 1413 1598096 12 0.592 +/-0.705 2.00 pCi/g TXJl 09/29/16 1932 1598082 13 0.842 +/-1.01 5.00 pCi/g CXS7 09/20/16 1251 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.4A.R.4.2 Sample ID: 405235076 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am24 l, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 330 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 104 (15%-125%) 1596418 90.5 (15%-125%) 1596418 87.5 (15%-125%) 1596420 89.9 (15%-125%) 1596417 87.6 (15%-125%) 1599981 103 (15%-125%) 1596422 104 (15%-125%) 1597804 84.2 (25%-125%) 1597417 94.6 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.5A.R.l.3 Sample ID: 405235077 Matrix: Soil Collect Date: 17-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 9.92% Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 9.92 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 Hh 0.0324 +/-0.0555 0.0486 Plutonium-239/240 HUh 0.00516 +/-0.0587 0.125 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.00832 +/-0.0368 0.096 Uranium-233/234 Hh 0.688 +/-0.173 0.0801 Uranium-235/236 HUh -0.00521 +/-0.0231 0.0602 Uranium-238 Hh 0.677 +/-0.170 0.060 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh -0.0683 +/-0.231 0.599 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.69 +/-0.836 0.739 Thorium-229 HUh 0.0358 +/-0.199 0.381 Thorium-230 Hh 0.602 +/-0.428 0.329 Thorium-232 Hh 0.721 +/-0.468 0.379 Am241, Cm Solid "Dry Weight Corrected" Americium-241 HUh -0.0178 +/-0.153 0.355 Curium-242 Hh 0.00 +/-0.485 0.722 Curium-243/244 HUh -0.036 +/-0.159 0.416 Curium-245/246 HXh 0.593 +/-0.471 0.254 Liquid Scint Pu241, Solid Dry Weight Corrected" Plutonium-241 HUh -1.51 +/-6.32 10.9 Rad Gamma Spec Analysis Gamma I129, Solid "Dry Weight Corrected" Iodine-129 HUh 0.0882 +/-0.302 0.663 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh 0.0556 +/-0.190 0.363 Antimony-125 HUh 0.00686 +/-0.0746 0.152 Bismuth-212 HU!h 0.00 +/-0.820 1.03 Bismuth-214 Hh 0.869 +/-0.160 0.101 Cesium-137 HUh -0.00906 +/-0.0273 0.0515 Cobalt-60 HUh -0.016 +/-0.031 0.0533 Europium-154 HUh -0.0737 +/-0.0876 0.139 Lead-212 Hh 0.859 +/-0.112 0.080 Lead-214 Hh 1.22 +/-0.168 0.296 Page 331 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF, Analyst Date Time Batch Mtd. percent LYTI 09/08/16 0846 1596246 I 0.00 +/-0.0557 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0382 +/-0.0588 1.00 pCi/g 0.022 +/-0.0369 1.00 pCi/g KXB2 09/17/16 1142 1596418 3 0.0238 +/-0.204 1.00 pCi/g 0.0138 +/-0.0231 1.00 pCi/g 0.0137 +/-0.200 1.00 pCi/g 0.188 +/-0.231 1.00 pCi/g KXB2 09/22/16 1030 1596420 4 0.234 +/-0.886 1.00 pCi/g KXB2 09/20/16 1128 1596417 5 0.0874 +/-0.199 1.00 pCi/g 0.0617 +/-0.439 1.00 pCi/g 0.0869 +/-0.483 1.00 pCi/g 0.0665 +/-0.154 1.00 pCi/g KXB2 09/22/16 1756 1599981 6 0.00 +/-0.486 1.00 pCi/g 0.0953 +/-0.160 1.00 pCi/g 0.00 +/-0.478 1.00 pCi/g 5.33 +/-6.32 15.0 pCi/g KXB2 09/22/16 1605 1596422 7 0.275 +/-0.304 1.00 pCi/g MJHI 09/29/16 0802 1598663 8 0.169 +/-0.192 pCi/g MXRI 10/03/16 0647 1596254 9 0.0689 +/-0.0747 pCi/g 0.474 +/-0.979 pCi/g 0.0456 +/-0.164 pCi/g 0.0229 +1-0:0216 0.100 pCi/g 0.0221 +/-0.0319 pCi/g 0.0573 +/-0.0938 pCi/g 0.0374 +/-0.121 pCi/g 0.144 +/-0.176 pCi/g GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.5A.R.l.3 Sample ID: 405235077 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 13.0 +/-1.25 0.441 Protactinium-231 HUh -0.00486 +/-0.389 0.711 Radium-226 Hh 0.869 +/-0.160 0.101 Radium-228 Hh 1.15 +/-0.240 0.175 Thallium-208 Hh 0.273 +/-0.0575 0.048 Tin-126 HUih 0.00 +/-0.157 0.119 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid "Dry Weight Corrected" Alpha Hh 17.3 +/-5.81 3.91 Beta Hh 17.0 +/-3.65 2.90 GFPC, Sr90, solid Dry Weight Corrected" Strontium-90 HUh -0.967 +/-0.744 1.66 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 0.818 +/-1.94 3.33 Liquid Scint Cl 4, Solid "Dry Weight Corrected" Carbon-14 HUh 0.240 +/-0.653 1.11 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.153 +/-0.883 1.56 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description 2 3 4 5 6 7 8 9 10 11 12 13 14 ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-.05-RC Modified DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300,I-Ol Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R EPA 900.0/SW846 931 O/SM 711 OB Modified EPA 905.0 Modified/DOE RP501 Rev. 1 Modified EPA 906.0 Modified EPA EERF C-01 Modified DOE EML HASL-300, Tc-02-RC Modified Page 332 of 5809 0.179 +/-1.43 pCi/g 0.330 +/-0.389 pCi/g 0.0456 +/-0.164 pCi/g 0.0754 +/-0.248 pCi/g 0.0214 +/-0.0587 pCi/g 0.0567 +/-0.158 pCi/g 1.24 +/-6.70 4.00 pCi/g JXC9 09/22/16 1400 1597817 10 1.21 +/-4.46 10.0 pCi/g 0.741 +/-0.744 2.00 pCi/g BXFl 09/27/16 1538 1597804 11 1.60 +/-1.94 6.00 pCi/g TXP3 09/27/16 1547 1598096 12 0.544 +/-0.653 2.00 pCi/g TXJl 09/29/16 2044 1598082 13 0.732 +/-0.883 5.00 pCi/g CXS7 09/20/16 1318 1597417 14 Analyst Date Time Prep Batch LYT! 09/08/16 0846 1596246 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.5A.R. l.3 Sample ID: 405235077 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 333 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 65.9 (15%-125%) 1596418 99.3 (15%-125%) 1596418 83.1 (15%-125%) 1596420 86 (15%-125%) 1596417 88 (15%-125%) 1599981 97.1 (15%-125%) 1596422 65.9 (15%-125%) 1597804 82.8 (25%-125%) 1597417 90.9 (15%-125%) GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.6A.R. l.3 Sample ID: 405235078 Matrix: Soil Collect Date: 17-DEC-15 Receive Date: 06-SEP-16 Collector: Client Moisture: 16.1 % Parameter Qualifier Result Uncertainty MDC Gravimetric Solids ASTM D 2216 % Moisture "As Received" Moisture 16.1 Rad Alpha Spec Analysis ASP Plutonium Isotopic, Solid "Dry Weight Corrected" Plutonium-238 HUh 0.0181 +/-0.0567 0.106 Plutonium-239/240 HUh -0.00599 +/-0.0414 0.101 ASP Uranium Isotopic, Solid "Dry Weight Corrected" Uranium-232 HUh -0.0365 +/-0.252 0.614 Uranium-233/234 Hh 0.624 +/-0.197 0.0946 Uranium-235/236 HUh 0.00435 +/-0.0455 0.0949 Uranium-238 Hh 0.566 +/-0.190 0.115 Alphaspec Np237, Solid "Dry Weight Corrected" Neptunium-237 HUh 0.0981 +/-0.270 0.468 Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Thorium-228 Hh 1.25 +/-0.685 0.615 Thorium-229 HUh 0.0325 +/-0.181 0.346 Thorium-230 Hh 0.359 +/-0.326 0.299 Thorium-232 Hh 0.855 +/-0.474 0.298

Am241, Cm Solid "Dry Weight Corrected" Americium-24 I HUh 0.0272 +/-0.15 I 0.290 Curium-242 Hh 0.00 +/-0.343 0.510 Curium-243/244 HUh -0.0509 +/-0.118 0.349 Curium-245/246 Hh 0.00 +/-0.121 0.179 Liquid Scint Pu241, Solid "Dry Weight Corrected" Plutonium-241 HUh -1.21 +/-4.93 8.50 Rad Gamma Spec Analysis Gamma II 29, Solid "Dry Weight Corrected" Iodine-129 HUh -0.0983 +/-0.302 0.576 Gammaspec, Gamma, Solid "Dry Weight Corrected" Actinium-227 HUh -0.0194 +/-0.162 0.298 Antimony-125 HUh -0.0269 +/-0.0729 0.141 Bismuth-212 HU!h 0.00 +/-0.768 0.978 Bismuth-214 Hh 0.634 +/-0.148 0.0849 Cesium-137 HUh 0.012 +/-0.0204 0.0458 Cobalt-60 HUh 0.00665 +/-0.0194 0.0479 Europium-154 HUh -0.00848 +/-0.0693 0.145 Lead-212 Hh 0.649 +/-0.103 0.074 Lead-214 Hh 0.805 +/-0.157 0.097 Page 334 of 5809 Report Date: October 4, 2016 Project: MJWCOOl 15 Client ID: MJWCOOl Le TPU RL Units PF DF Analyst Date Time Batch Mtd. percent LYT! 09/08/16 0846 1596246 1 0.0325 +/-0.0568 1.00 pCi/g KXB2 09/17/16 1142 1596421 2 0.0299 +/-0.0414 1.00 pCi/g 0.183 +/-0.253 1.00 pCi/g KXB2 09/17/16 1144 1596418 3 0.0241 +/-0.245 1.00 pCi/g 0.0241 +/-0.0456 1.00 pCi/g 0.034 +/-0.232 1.00 pCi/g 0.119 +/-0.270 1.00 pCi/g KXB2 09/22/16 1000 1596420 4 0.185 +/-0.715 1.00 pCi/g KXB2 09/19/16 1741 1596417 5 0.0793 +/-0.18 I 1.00 pCi/g 0.056 +/-0.330 1.00 pCi/g 0.0558 +/-0.491 1.00 pCi/g 0.0664 +/-0.15 I 1.00 pCi/g KXB2 09/22/16 1752 1599981 6 0.00 +/-0.343 1.00 pCi/g 0.0951 +/-0.118 1.00 pCi/g 0.00 +/-0.121 1.00 pCi/g 4.16 +/-4.93 15.0 pCi/g KXB2 09/22/16 1736 1596422 7 0.219 +/-0.305 1.00 pCi/g MJHl 09/29/16 0802 1598663 8 0.135 +/-0.163 pCi/g MXRl 10/03/16 0648 1596254 9 0.0624 +/-0.0739 pCi/g 0.447 +/-0.874 pCi/g 0.037 +/-0.157 pCi/g 0.0198 +/-0.02II 0.100 pCi/g 0.0188 +/-0.0197 pCi/g 0.0587 +/-0.0694 pCi/g 0.0341 +/-0.116 pCi/g 0.0438 +/-0.170 pCi/g GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.6A.R.l.3 Sample ID: 405235078 Certificate of Analysis Report Date: Project: MJWCOOI 15 Client ID: MJWCOOI October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Rad Gamma Spec Analysis Gammaspec, Gamma, Solid "Dry Weight Corrected" Potassium-40 Hh 9.82 +/-1.23 Protactinium-231 HUh 0.0133 +/-0.325 Radium-226 Hh 0.634 +/-0.148 Radium-228 Hh 0.618 +/-0.175 Thallium-208 Hh 0.214 +/-0.067 Tin-126 HU!h 0.00 +/-0.151 Rad Gas Flow Proportional Counting GFPC, Gross AIB, solid Dry Weight Corrected" Alpha Hh 30.8 +/-6.68 Beta Hh 35.2 +l-5.09 GFPC, Sr90, solid "Dry Weight Corrected" Strontium-90 HUh -0.473 +/-0.668 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid "Dry Weight Corrected" Tritium HUh 1.10 +/-2.20 Liquid Scint C14, "Dry Weight Corrected" Carbon-14 HUh 0.277 +/-0.699 Liquid Scint Tc99, Solid "Dry Weight Corrected" Technetium-99 HUh 0.829 +/-1.10 The following Prep Methods were performed Method Description Dry Soil Prep Dry Soil Prep GL-RAD-A-021 The following Analytical Methods were performed Method Description ASTM D 2216 (Modified) DOE EML HASL-300, Pu-11-RC Modified DOE EML HASL-300, U-02-RC Modified ASTM C 1475-00 Modified DOE EML HASL-300, Th-01-RC Modified DOE EML HASL-300, Am-05-RC Modified. DOE EML HASL-300, Pu-I I-RC Modified DOE EML HASL-300,1-0 I Modified DOE HASL 300, 4.5.2.3/Ga-Ol-R 0.562 0.602 0.0849 0.202 0.0438 0.0835 3.94 4.66 1.44 3.75 1.19 1.86 2 3 4 5 6 7 8 9 10 II 12 13 14 EPA 900.0/SW846 9310/SM 71 IOB Modified EPA 905.0 Modified/DOE RP501 Rev. I Modified EPA 906.0 Modified EPA EERF C-0 I Modified DOE EML HASL-300, Tc-02-RC Modified Page 335 of 5809 0.234 +/-1.51 pCi/g 0.273 +/-0.325 pCi/g 0.037 +/-0.157 pCi/g 0.0877 +/-0.195 pCi/g 0.0191 +/-0.0693 pCi/g 0.0389 +/-0.153 pCi/g 1.44 +/-8.94 4.00 pCi/g JXC9 09/22/16 1400 1597817 10 2.12 +/-7.15 10.0 pCi/g 0.628 +/-0.668 2.00 pCi/g BXFI 09/27/16 1538 1597804 II 1.81 +/-2.20 6.00 pCi/g TXP3 09/27/16 1721 1598096 12 0.581 +l-0.699 2.00 pCi/g TXJI 09/29/16 2155 1598082 13 0.873 +/-1.10 5.00 pCi/g CXS7 09/20/16 1346 1597417 14 Analyst Date Time Prep Batch LYTI 09/08/16 0846 1596246 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: MJW Technical Services 15 Hazelwood Drive Suite 112 Buffalo, New York 14228 Contact: Ms. Laurie Losey Project: Soil Radioisotopes Client Sample ID: 5.6A.R.l.3 Sample ID: 405235078 Certificate of Analysis Report Date: Project: MJWC00115 Client ID: MJWCOOl October 4, 2016 Parameter Qualifier Result Uncertainty MDC Le TPU RL Units PF DF Analyst Date Time Batch Mtd. Surrogate/Tracer Recovery Test Plutonium-242 Tracer Uranium-232 Tracer Uranium-235/236 Tracer Americium-243 Tracer Actinium-227 Tracer Americium-243 Tracer Plutonium-242 Tracer Strontium Carrier Technetium-99m Tracer Notes: ASP Plutonium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" ASP Uranium Isotopic, Solid "Dry Weight Corrected" Alphaspec Np237, Solid "Dry Weight Corrected" Alphaspec Th229 + 228,230,232 Solid "Dry Weight Corrected" Am241, Cm Solid "Dry Weight Corrected" Liquid Scint Pu241, Solid "Dry Weight Corrected" GFPC, Sr90, solid "Dry Weight Corrected" Liquid Scint Tc99, Solid "Dry Weight Corrected" The MDC is a sample specific MDC. TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit Le/LC: Critical Level MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 336 of 5809 Mtd.: Method PF: Prep Factor RL: Reporting Limit TPU: Total Propagated Uncertainty Batch ID Recovery% Acceptable Limits 1596421 82.8 (15%-125%) 1596418 97.9 (15%-125%) 1596418 17.9 (15%-125%) 1596420 92.6 (15%-125%) 1596417 106 (15%-125%) 1599981 102 (15%-125%) 1596422 82.8 (15%-125%) 1597804 84.2 (25%-125%) 1597417 86.2 (15%-125%)

Page 337 of 5809 Quality Control Summary GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Report Date: October 4, 2016 Client: MJW Technical Services Page 1 of 39 15 Hazelwood Drive Suite 112 Buffalo, New York Contact: Ms. Laurie Losey Workorder: 405235 Parmname NOM SamJ:!le Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596388 QCl203621689 405235001 DUP Thorium-228 Hh 2.13 H 1.16 pCilg 58.6 (0% -100%) JXH2 09/2811614:07 Uncert: +l-1.25 +l-0.588 TPU: +l-1.33 +l-0.606 Thorium-229 Hh 0.301 HU 0.142 pCilg 0 NIA Uncert: +l-0.488 +l-0.309 TPU: +l-0.492 +l-0.310 Thorium-230 Hh 1.46 H 0.740 pCilg 65.2 (0%-100%) Uncert: +l-0.868 +l-0.427 TPU: +l-0.916 +l-0.437 Thorium-232 Hh 0.962 H 0.484 pCilg 45.4 (0%-100%) Uncert: +l-0.721 +l-0.402 TPU: +l-0.746 +l-0.406 QC1203621690 LCS Thorium-228 u -0.0115 pCilg JXH2 0912811614:07 Uncert: +l-0.118 TPU: +l-0.119 Thorium-229 u 0.0374 pCilg Uncert: +l-0.172 TPU: +l-0.172 Thorium-230 19.2 20.6 pCilg 107 (75%-125%) Uncert: +l-1.74 TPU: +l-3.16 Thorium-232 0.133 pCi/g (75%-125%) Uncert: +l-0.175 TPU: +l-0.176 QCl203621688 MB Thorium-228 u 0.0793 pCilg JXH2 0912811614:05 Uncert: +l-0.155 TPU: +l-0.156 Thorium-229 0.0689 pCi/g Uncert: +l-0.115 TPU: +l-0.115 Thorium-230 u -0.0139 pCilg Uncert: +l-0.0663 TPU: +l-0.0664 Thorium-232 0.0411 pCilg Uncert: +l-0.101 TPU: +l-0.101 Batch 1596389 QCl203621692 405235001 DUP Uranium-232 HUh -0.0134 HU -0.0295 pCilg 0 NIA JXH2 09129116 09:20 Page 338 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summarl'.: Workorder: 405235 Page 2 of 39 Parmname NOM Qual QC

Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596389 Uncert: +l-0.0454 +l-0.0476 TPU: +l-0.0455 +l-0.0478 Uranium-2331234 Hh 0.798 H 1.58 pCi/g 65.9* (0%-20%) Uncert: +l-0.232 +l-0.338 TPU: +l-0.268 +l-0.441 Uranium-2351236 Hh 0.0583 H 0.092 pCilg .246 (0%-100%) Uncert: +l-0.0739 +l-0.0888 TPU: +l-0.0745 +l-0.0903 Uranium-238 Hh 1.00 H . 1.08 pCi/g 7.53 (0%-20%) Uncert: +l-0.255 +l-0.279 TPU: +l-0.306 +l-0.340 QC1203621693 LCS Uranium-232 u -0.0213 pCilg JXH2 0912911609:20 Uncert: +l-0.0577 TPU: +l-0.0578 Uranium-2331234 5.38 pCilg Uncert: +l-0.648 TPU: +l-1.18 Uranium-2351236 0.379 pCi/g Uncert: +l-0.178 TPU: +l-0.191 Uranium-238 5.29 6.27 pCilg 118 (75%-125%) Uncert: +l-0.698 TPU: +l-1.34 QC1203621691 MB Uranium-232 u -0.0183 pCilg JXH2 0912911609:13 Uncert: +l-0.0815 TPU: +l-0.0815 Uranium-2331234 u -0.00641 pCilg Uncert: +l-0.0598 TPU: +l-0.0599 Uranium-2351236 u 0.00514 pCilg Uncert: +l-0.0586 TPU: +l-0.0586 Uranium-238 u 0.0211 pCi/g Uncert: +l-0.0663 TPU: +l-0.0664 Batch 1596390 QCl20362!695 405235001 DUP Americium-241 HUh -0.0138 HU -0.0228 pCilg 0 NIA JXH2 0912911621:52 Uncert: +l-0.0417 +l-0.0688 TPU: +l-0.0418 +l-0.069 Curium-242 Hh 0.00 H 0.00 pCilg 0 NIA Uncert: +l-0.133 +l-0.220 TPU: +l-0.134 +l-0.221 Curium-2431244 HUh 0.0101 HU -0.0077 pCi/g 0 NIA Page 339 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y: Workorder: 405235 Page 3 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596390 Uncert: +/-0.0563 +/-0.0664 TPU: +/-0.0563 +/-0.0667 Curium-245/246 Hh 0.00 H 0.00 pCi/g 0 NIA Uncert: +/-0.0442 +/-0.0729 TPU: +/-0.0443 +/-0.0732 QC1203621696 LCS Americium-241 3.87 3.64 pCi/g 94.2 (75%-125%) JXH2 09/29/1621 :52 Uncert: +/-0.592 TPU: +/-0.838 Curium-242 0.00 pCi/g Uncert: +/-0.049 TPU: +/-0.0492 Curium-243/244 5.11 5.30 pCi/g 104 (75%-125%) Uncert: +/-0.700 TPU: +/-1.11 Curium-245/246 0.0766 pCi/g Uncert: +/-0.110 TPU: +/-0.111 QC1203621694 MB Americium-241 u 0.00305 pCi/g JXH2 09/29/1621 :26 Uncert: +/-0.0319 TPU: +/-0.032 Curium-242 u -0.00262 pCi/g Uncert: +/-0.0226 TPU: +/-0.0227 Curium-243/244 u -0.0103 pCi/g Uncert: +/-0.0239 TPU: +/-0.024 Curium-245/246 u -0.003 pCi/g Uncert: +/-0.0258 TPU: +/-0.0259 Batch 1596392 QC1203621698 405235001 DUP Neptunium-237 HUh -0.0857 H 0.00 pCi/g 0 NIA JXH2 09/30/1609:00 Uncert: +/-0.259 +/-0.358 TPU: +/-0.259 +/-0.359 QC1203621699 LCS Neptunium-237 41.0 42.2 pCi/g 103 (75%-125%) JXH2 09/30/1609:00 Uncert: +/-3.94 TPU: +/-6.20 QC1203621697 MB Neptunium-237 u -0.0165 pCi/g JXH2 09/30/1609:00 Uncert: +/-0.142 TPU: +/-0.142 Batch 1596393 QC1203621701 405235001 DUP Page 340 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Workorder: 405235 Page 4 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596393 Plutonium-238 Hh 0.0364 HU 0.0338 pCilg 0 NIA JXH2 09129116 09:23 Uncert: +l-0.0647 +l-0.093 TPU: +l-0.0649 +l-0.0932 Plutonium-2391240 HUh -0.00621 HU 0.0483 pCi/g 0 NIA Uncert: +l-0.0429 +l-0.121 TPU: +l-0.0429 +l-0.122 QC1203621702 LCS Plutonium-238 0.0899 pCilg (75%-125%) JXH2 0912911614: 16 Uncert: +l-0.114 TPU: +l-0.115 Plutonium-2391240 3.88 4.32 pCilg Ill (75%-125%) Uncert: +l-0.653 TPU: +l-0.978 QC1203621700 MB Plutonium-238 u -0.0183 pCilg JXH2 09129116 09:24 Uncert: +l-0.0347 TPU: +l-0.0347 Plutonium-239/240 0.0586 pCilg Uncert: +l-0.0823 TPU: +l-0.0827 Batch 1596394 QC1203621704 405235001 DUP Plutonium-241 HUh -4.14 HU -4.08 pCi/g 0 NIA JXH2 10103/1612:30 Uncert: +l-7.71 +l-7.44 TPU: +l-7.71 +l-7.44 QC1203621705 LCS Plutonium-241 150 154 pCilg 103 (75%-125%) JXH2 10101/1604:05 Uncert: +l-14.7 TPU: +l-39.3 QC1203621703 MB Plutonium-241 u -1.94 pCilg JXH2 10101116 02:02 Uncert: +l-6.44 TPU: +l-6.44 Batch 1596395 QC1203621707 405235021 DUP Thorium-228 Hh 1.13 H 1.10 pCi/g 3.48 (0%-100%) MXS2 0912811617:56 Uncert: +l-0.629 +l-0.529 TPU: +/-0.653 +l-0.551 Thorium-229 HUh -0.0135 H 0.107 pCi/g 0 NIA Uncert: +l-0.117 +l-0.190 TPU: +l-0.117 +l-0.191 Thorium-230 Hh 0.787 H 0.682 pCilg 14.2 (0%-100%) Un cert: +l-0.427 +l-0.329 TPU: +l-0.443 +l-0.339 Thorium-232 Hh 0.645 H 0.448 pCilg 36.2 (0%-100%) Page 341of5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Workorder: 405235 Page 5 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596395 Uncert: +/-0.398 +/-0.267 TPU: +/-0.410 +/-0.273 QC1203621708 LCS Thorium-228 u 0.0211 pCi/g MXS2 09/24/1613:18 Uncert: +/-0.294 TPU: +/-0.295 Thorium-229 u 0.00 pCi/g Uncert: +/-0.582 TPU: +/-0.582 Thorium-230 17.2 19.3 pCi/g 112 (75%-125%) Uncert: +/-2.79 TPU: +/-4.88 Thorium-232 u -0.0486 pCi/g (75%-125%) Uncert: +/-0.215 TPU: +/-0.216 QC1203621706 MB Thorium-228 u -0.0414 pCi/g MXS2 09/24/1613:16 Uncert: +/-0.145 TPU: +/-0.145 Thorium-229 u 0.0617 pCi/g Uncert: +/-0.170 TPU: +/-0.170 Thorium-230 u -0.0212 pCi/g Uncert: +/-0.146 TPU: +/-0.146 Thorium-232 u -0.0115 pCi/g Uncert: +/-0.0993 TPU: +/-0.0995 Batch 1596396 QC1203621710 405235021 DUP Uranium-232 HUh -0.00834 HU -0.00399 pCi/g 0 N/AMXS2 09/28/1617:55 Uncert: +/-0.0576 +/-0.0344 TPU: +/-0.0577 +/-0.0345 Uranium-233/234 Hh 0.665 H 0.520 pCi/g 24.6* (0%-20%) Uncert: +/-0.200 +/-0.198 TPU: +/-0.230 +/-0.218 Uranium-235/236 Hh 0.0262 H 0.0509 pCi/g 0 NIA Uncert: +/-0.0515 +/-0.0733 TPU: +/-0.0517 +/-0.0738 Uranium-238 Hh 0.606 H 1.00 pCi/g 49.2* (0%-20%) Uncert: +/-0.192 +/-0.270 TPU: +/-0.218 +/-0.323 QC120362171 l LCS Uranium-232 u 0.00859 pCi/g MXS2 09/24/1613:20 Uncert: +/-0.0554 TPU: +/-0.0555 Page 342 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y: Workorder: 405235 Page 6 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596396 Uranium-233/234 4.78 pCi/g Uncert: +/-0.521 TPU: +/-0.950 Uranium-235/236 0.295 pCi/g Uncert: +/-0.133 TPU: +/-0.141 Uranium-238 5.20 5.04 pCi/g 96.9 (75%-125%) Uncert: +/-0.535 TPU: +/-0.993 QC1203621709 MB Uranium-232 0.0297 pCi/g MXS2 09/24/1613:49 Uncert: +/-0.059 TPU: +/-0.0592 Uranium-233/234 u -0.0113 pCi/g Uncert: +/-0.0342 TPU: +/-0.0343 Uranium-235/236 u 0.00821 pCi/g Uncert: +/-0.0456 TPU: +/-0.0457 Uranium-238 0.0239 pCi/g Uncert: +/-0.055 TPU: +/-0.0551 Batch 1596399 QC1203621716 405235021 DUP Neptunium-237 HUh -0.0443 HU 0.0446 pCi/g 0 N/AMXS2 09/29/1614:05 Uncert: +/-0.400 +/-0.467 TPU: +/-0.400 +/-0.467 QC1203621717 LCS Neptunium-237 38.2 41.4 pCi/g 108 (75%-125%) MXS2 09/26/1611 :53 Uncert: +/-4.43 TPU: +/-6.36 QC1203621715 MB Neptunium-237 u -0.0347 pCi/g MXS2 09/26/1617:11 Uncert: +/-0.289 TPU: +/-0.290 Batch 1596400 QC1203621719 405235021 DUP Plutonium-238 HUh 0.0188 HU 0.0047 pCi/g 0 N/AMXS2 09/24/1620:54 Uncert: +/-0.0726 +/-0.0491 TPU: +/-0.0727 +/-0.0492 Plutonium-239/240 HUh -0.00208 HU 0.026 pCi/g 0 NIA Un cert: +/-0.0744. +/-0.0686 TPU: +/-0.0745 +/-0.0687 QC1203621720 LCS Plutonium-238 u -0.0109 pCi/g (75%-125%) MXS2 09/24/1620:54 Uncert: +/-0.0329 Page 343 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235 Page 7 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596400 TPU: +/-0.033 Plutonium-239/240 3.81 3.65 pCi/g 95.5 (75%-125%) Uncert: +/-0.463 TPU: +/-0.677 QCl203621718 MB Plutonium-238 u -0.0483 pCi/g MXS2 09/24/1620:54 Uncert: +/-0.0801 TPU: +/-0.0801 Plutonium-239/240 0.0441 pCi/g Un cert: +/-0.0701 TPU: +/-0.0704 Batch 1596402 QC1203621726 405235021 DUP Plutonium-241 Hh 9.46 HU 3.29 pCi/g 0 N/AMXS2 09/29/1613:48 Uncert: +/-7.66 +/-5.23 TPU: +/-7.93 +/-5.28 QC1203621727 LCS Plutonium-241 147 146 pCi/g 99.4 (75%-125%) MXS2 09/28/1623:41 Un cert: +/-9.96 TPU: +/-32.9 QC1203621725 MB Plutonium-241 u -5.12 pCi/g MXS2 09/28/1622:08 Uncert: +/-5.93 TPU: +/-5.93 Batch 1596407 QC1203621737 405235041 DUP Thorium-228 Hh 1.07 H 1.21 pCi/g 12.4 (0% -100%) HAKB 09/22/1614:25 Uncert: +/-0.620 +/-0.702 TPU: +/-0.648 +/-0.731 Thorium-229 Hh 0.373 H 0.0642 pCi/g 63.9 (0% -100%) Uncert: +/-0.308 +/-0.180 TPU: +/-0.314 +/-0.181 Thorium-230 Hh 0.445 H 0.225 pCi/g 22.7 NIA Uncert: +/-0.366 +/-0.285 TPU: +/-0.373 +/-0.288 Thorium-232 Hh 0.646 H 0.863 pCi/g 28.8 (0%-100%) Uncert: +/-0.390 +/-0.487 TPU: +/-0.402 +/-0.508 QC1203621738 LCS* Thorium-228 u 0.00462 pCi/g HAKB 09/22/1614:25 Uncert: +/-0.413 TPU: +/-0.413 Thorium-229 0.148 pCi/g Uncert: +/-0.340 TPU: +/-0.341 Page 344 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y: Workorder: 405235 Page 8 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596407 Thorium-230 16.4 16.5 pCi/g 101 (75%-125%) Uncert: +/-2.50 TPU: +/-4.14 Thorium-232 0.0969 pCi/g (75%-125%) Uncert: +/-0.272 TPU: +/-0.273 QC1203621736 MB Thorium-228 0.303 pCi/g HAKB 09/22/1613:44 Uncert: +/-0.350 TPU: +/-0.354 Thorium-229 u 0.0371 pCi/g Uncert: +/-0.239 TPU: +/-0.240 Thorium-230 0.100 pCi/g Uncert: +/-0.231 TPU: +/-0.231 Thorium-232 u -0.0158 pCi/g Uncert: +/-0.136 TPU: +/-0.137 Batch 1596408 QCl203621740 405235041 DUP Uranium-232 HUh 0.0147 HU -0.0419 pCi/g 0 N/AHAKB 09/22/1614:24 Uncert: +/-0.0865 +/-0.0482 TPU: +/-0.0866 +/-0.0483 Uranium-233/234 Rh 0.802 H 0.572 pCi/g 33.5* (0%-20%) Uncert: +/-0.207 +/-0.181 TPU: +/-0.244 +/-0.205 Uranium-235/236 HUh 0.0181 H 0.0433 pCi/g 0 NIA Uncert: +/-0.0555 +/-0.0641 TPU: +/-0.0556 +/-0.0646 Uranium-238 Rh 0.704 H 0.781 pCi/g 10.4 (0%-20%) Uncert: +/-0.193 +/-0.210 TPU: +/-0.224 +/-0.249 QC1203621741 LCS Uranium-232 u -0.00759 pCi/g HAKB 09/22/1614:24 Uncert: +/-0.0511 TPU: +/-0.0513 Uranium-233/234 5.05 pCi/g Uncert: +/-0.482 TPU: +/-0.980 Uranium-235/236 0.303 pCi/g Uncert: +/-0.125 TPU: +/-0.135 Uranium-238 5.23 5.38 pCi/g 103 (75%-125%) Uncert: +/-0.497 TPU: +/-1.04 Page 345 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summarl: Workorder: 405235 Page 9 of 39 Parmname NOM Sam(!le Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596408 QC1203621739 MB Uranium-232 u 0.0439 pCilg HAKB 0912211610:03 Uncert: +l-0.139 TPU: +l-0.140 Uranium-2331234 0.072 pCi/g Uncert: +l-0.104 TPU: +l-0.106 Uranium-2351236 0.0722 pCi/g Uncert: +l-0.105 TPU: +l-0.106 Uranium-238 0.0757 pCi/g Uncert: +l-0.104 TPU: +l-0.106 Batch 1596410 QC1203621746 405235041 DUP Americium-241 HUh -0.0106 HU -0.00367 pCilg 0 NIAHAKB 0912211616: 14 Uncert: +l-0.0523 +l-0.0608 TPU: +l-0.0523 +l-0.0611 Curium-242 HUh -0.00899 HU -0.0128 pCilg 0 NIA Uncert: +l-0.124 +l-0.212 TPU: +l-0.124 +l-0.213 Curium-2431244 Hh 0.0154 HU -0.00745 pCilg 0 NIA Uncert: +l-0.0505 +l-0.0622 TPU: +l-0.0506 +l-0.0624 Curium-2451246 Hh 0.00 HU -0.0042 pCilg 0 NIA Uncert: +l-0.0402 +l-0.0695 TPU: +l-0.0403 +/-0.0698 QC1203621747 LCS Americium-241 3.82 4.02 pCi/g 105 (75%-125%) HAKB 09122116 09:56 Uncert: +l-0.497 TPU: +l-0.743 Curium-242 0.0158 pCilg Uncert: +l-0.0443 TPU: +l-0.0443 Curium-2431244 5.06 5.37 pCi/g 106 (75%-125%) Uncert: +l-0.569 TPU: +l-0.931 Curium-2451246 0.145 pCilg Uncert: +/-0.107 TPU: +l-0.109 QC1203621745 MB Americium-241 u 0.00652 pCilg HAKB 0912211609:56 Uncert: +l-0.049 TPU: +l-0.049 Curium-242 0.00 pCi/g Uncert: +l-0.0338 TPU: +l-0.0339 Page 346 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -WWW.gel.com QC Workorde'r: 405235 Page 10 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596410 Curium-243/244 0.00 pCi/g Uncert: +/-0.0335 TPU: +/-0.0335 Curium-245/246 u -0.00398 pCi/g Un cert: +/-0.0396 TPU: +/-0.0397 Batch 1596411 QC1203621749 405235041 DUP Neptunium-237 HUh -0.0562 HU 0.147 pCi/g 0 NIA HAKE 09/22/1615:54 Uncert: +/-0.315 +/-0.542 TPU: +/-0.315 +/-0.543 QC1203621750 LCS Neptunium-237 36.6 42.3 pCi/g 116 (75%-125%) HAKE 09/22/1615:54 Uncert: +/-4.57 TPU: +/-6.51 QC1203621748 MB Neptunium-237 0.229 pCi/g HAKE 09/22/1615:54 Uncert: +/-0.444 TPU: +/-0.445 Batch 1596412 QC1203621752 405235041 DUP Plutonium-238 Hh 0.0701 HU -0.00713 pCi/g 0 N/AHAKE 09/22/1609:56 Uncert: +/-0.119 +/-0.0497 TPU: +/-0.120 +/-0.0499 Plutonium-239/240 HUh -0.00872 HU -0.00354 pCi/g 0 NIA Uncert: +/-0.0698 +/-0.0489 TPU: +/-0.0702 +/-0.0491 QC1203621753 LCS Plutonium-238 0.0726 pCi/g (75%-125%) HAKE 09/22/1609:56 Uncert: +/-0.106 TPU: +/-0.107 Plutonium-239/240 3.84 4.34 pCi/g 113 (75%-125%) Uncert: +/-0.673 TPU: +/-1.01 QC1203621751 MB Plutonium-238 u 0.0086 pCi/g HAKE 09/22/1609:56 Uncert: +/-0.057 TPU: +/-0.0571 Plutonium-239/240 u -0.00573 pCi/g Uncert: +/-0.0405 TPU: +/-0.0406 Batch 1596414 QC1203621755 405235041 DUP Plutonium-241 HUh -0.671 HU -4.08 pCi/g 0 NIA HAKE 09/24/1612:0 l Uncert: +/-7.42 +/-7.14 Page 347of5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Workorder: 405235 Page 11 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596414 TPU: +/-7.42 +/-7.14 QC1203621756 LCS Plutonium-241 148 172 pCi/g 116 (75%-125%) HAKE 09/24/1613:02 Un cert: +/-12.2 TPU: +/-43.3 QC1203621754 MB Plutonium-241 u 2.09 pCi/g HAKE 09/24/1611:00 Uncert: +/-6.03 TPU: +/-6.04 Batch 1596417 QC1203621758 405235061 DUP Thorium-228 Hh 0.491 H 1.40 pCi/g 67.9 (0%-100%) KXB2 09/19/1617:56 Uncert: +/-0.506 +/-0.764 TPU: +/-0.514 +/-0.799 Thorium-229 Hh 0.00 H 0.198 pCi/g 0 NIA Uncert: +/-0.130 +/-0.285 TPU: +/-0.130 +/-0.287 Thorium-230 Hh 0.707 H 0.323 pCi/g 56.3 (0%-100%) Uncert: +/-0.437 +/-0.348 TPU: +/-0.450 +/-0.352 Thorium-232 Hh 0.850 H 0.625 pCi/g 30.6 (0%-100%) Uncert: +/-0.490 +/-0.445 TPU: +/-0.507 +/-0.455 QC1203621759 LCS Thorium-228 u 0.0682 pCi/g KXB2 09/20/1611:29 Uncert: +/-0.276 TPU: +/-0.277 Thorium-229 u -0.0821 pCi/g Uncert: +/-0.156 TPU: +/-0.156 Thorium-230 17.7 18.3 pCi/g 103 (75%-125%) Uncert: +/-2.20 TPU: +/-3.69 Thorium-232 0.120 pCi/g (75%-125%) Uncert: +/-0.236 TPU: +/-0.236 QC1203621757 MB Thorium-228 u 0.0778 pCi/g KXB2 09/20/1611 :28 Uncert: +/-0.263 TPU: +/-0.265 Thorium-229 0.0999 pCi/g Uncert: +/-0.230 TPU: +/-0.230 Thorium-230 u -0.0157 pCi/g Uncert: +/-0.136 TPU: +/-0.136 Page 348 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -WWW.gel.com QC Summar.Y Workorder: 405235 Page 12 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596417 Thorium-232 u -0.0157 pCi/g Uncert: +/-0.135 TPU: +/-0.136 Batch 1596418 QCl203621761 405235061 DUP Uranium-232 HUh 0.0232 H 0.0725 pCi/g 0 N/AKXB2 09/17/1611 :44 Uncert: +/-0.0794 +/-0.0881 TPU: +/-0.0795 +/-0.089 Uranium-233/234 Hh 0.585 H 0.630 pCi/g 7.39 (0%-20%) Uncert: +/-0.188 +/-0.215 TPU: +/-0.214 +/-0.241 Uranium-235/236 Hh 0.0309 H 0.0352 pCi/g 0 NIA Uncert: +/-0.0529 +/-0.070 TPU: +/-0.0532 +/-0.0703 Uranium-238 Hh 0.800 H 0.676 pCi/g 16.9 (0%-20%) Uncert: +/-0.220 +/-0.216 TPU: +/-0.260 +/-0.246 QC1203621762 LCS Uranium-232 0.0338 pCi/g KXB2 09/17/1611:44 Uncert: +/-0.0777 TPU: +/-0.0779 Uranium-233/234 5.07 pCi/g Uncert: +/-0.550 TPU: +/-1.05 Uranium-235/236 0.332 pCi/g Uncert: +/-0.146 TPU: +/-0.157 Uranium-238 5.20 5.61 pCi/g 108 (75%-125%) Uncert: +/-0.577 TPU: +/-1.14 QC1203621760 MB Uranium-232 u -0.0885 pCi/g KXB2 09/17/1611 :42 Uncert: +/-0.0663 TPU: +/-0.0663 Uranium-233/234 u -0.0104 pCi/g Uncert: +/-0.0353 TPU: +/-0.0353 Uranium-235/236 u -0.00546 pCi/g Uncert: +/-Q.0242 TPU: +/-0.0242 Uranium-238 u -0.0136 pCi/g Uncert: +/-0.0258 TPU: +/-0.0259 Batch 1596420 QC1203621767 405235061 DUP Neptunium-237 HUh -0.102 HU -0.0527 pCi/g 0 N/AKXB2 09/22/1610:00 Page 349 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235 Page 13 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1596420 Uncert: +/-0.237 +/-0.233 TPU: +/-0.238 +/-0.234 QC1203621768 LCS Neptunium-237 40.6 45.4 pCi/g 112 (75%-125%) KXB2 09/22/1610:00 Uncert: +/-3.76 TPU: +/-6.33 QC1203621766 MB Neptunium-237 u 0.183 pCi/g KXB2 09/22/1610:00 Uncert: +/-0.625 TPU: +/-0.625 Batch 1596421 QC1203621770 405235061 DUP Plutonium-23 8 Hh 0.0258 H 0.0228 pCi/g 0 N/AKXB2 09/17/1611 :42 Uncert: +/-0.0508 +/-0.0447 TPU: +/-0.0509 +/-0.0448 Plutonium-239/240 Hh 0.0257 HU -0.0185 pCi/g 0 NIA Uncert: +l-0.0505 +/-0.0298 TPU: +/-0.0506 +/-0.0299 QC1203621771 LCS Plutonium-238 u -0.0103 pCi/g (75%-125%) KXB2 09/17 /1611:44 Uncert: +/-0.0713 TPU: +/-0.0714 Plutonium-239/240 3.81 3.99 pCi/g 105 (75%-125%) Uncert: +/-0.602 TPU: +/-0.889 QCl203621769 MB Plutonium-23 8 0.0566 pCi/g KXB2 09/17/1611 :42 Uncert: +/-0.0689 TPU: +/-0.0693 Plutonium-239/240 u 0.00056 pCi/g Uncert: +/-0.0415 TPU: +/-0.0416 Batch 1596422 QCl203621773 405235061 DUP Plutonium-241 HUh -1.33 HU -1.42 pCi/g 0 N/AKXB2 09/22/1620:39 Uncert: +/-4.61 +/-4.49 TPU: +/-4.61 +/-4.49 QC1203621774 LCS 147 177 pCi/g 120 (75%-125%) KXB2 09/22/1622:10 ' Uncert: +/-9.48 TPU: +l-4) .0 QCl203621772 MB Plutonium-241 u -2.3 pCi/g KXB2 09/22/1619:07 Uncert: +/-4.71 TPU: +/-4.71 Page 350 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Workorder: 405235 QC Summar:y Page 14 of 39 Parm name NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1599981 QCl203630764 405235061 DUP Americium-241 Hh 0.142* H 0.0535 pCilg 0 NIAKXB2 0912211617:52 Un cert: +l-0.243 +l-0.150 TPU: +l-0.244 +l-0.150 Curium-242 Hh 0.00 H 0.00 pCi/g 0 NIA Uncert: +l-0.470 +l-0.355 TPU: +l-0.471 +l-0.355 Curium-2431244 Hh 0.00 HU -0.013 pCilg 0 NIA Uncert: +l-0.145 +l-0.112 TPU: :+l-0.145 +l-0.112 Curium-2451246 Hh 0.081 H 0.0611 pCi/g 0 NIA Uncert: +l-0.228 +l-0.172 TPU: +l-0.228 +l-0.172 QC1203630765 LCS Americium-241 16.1 16.5 pCilg 102 (75%-125%) KXB2 0912211617:52 Uncert: +l-1.70 TPU: +l-2.61 Curium-242 u 0.0342 pCilg Uncert: +l-0.128 TPU: +l-0.128 Curium-2431244 21.3 20.7 pCilg 97 (75%-125%) Uncert: +l-1.89 TPU: +l-3.12 Curium-2451246 0.622 pCilg Uncert: +l-0.367 TPU: +l-0.374 QCI203630763 MB Americium-241 u -0.0329 pCilg KXB2 0912211617:52 Uncert: +l-0.0993 TPU: +l-0.0994 Curium-242 0.00 pCilg Uncert: +l-0.0914 TPU: +l-0.0915 Curium-2431244 0.045 pCilg Uncert: +l-0.126 TPU: +l-0.127 Curium-2451246 x 0.341 pCilg Uncert: +l-0.293 TPU: +l-0.296 Batch 1601257 QC1203633743 405235051 DUP Uranium-232 HUh -0.0211 HU -0.172 pCilg 0 NIAKXB2 09/29/1614:04 Uncert: +l-0.228 +l-0.189 TPU: +l-0.228 +l-0.189 Uranium-2331234 Hh 0.741 H 1.02 pCilg 31.3* (0%-20%) Uncert: +l-0.301 +l-0.289 TPU: +l-0.314 +l-0.312 Page 351 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Workorder: 405235 Page 15 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1601257 Uranium-2351236 Hh 0.134 H 0.266 pCilg 30 (0%-100%) Uncert: +l-0.145 +l-0.164 TPU: +l-0.146 +l-0.167 Uranium-238 Hh 0.988 H 1.04 pCilg 5.17 (0%-20%) Uncert: +l-0.311 +l-0.296 TPU: +l-0.333 +l-0.319 QC1203633744 LCS Uranium-232 u 0.0707 pCi/g KXB2 09129/1614:04 Uncert: +l-0.176 TPU: +l-0.176 Uranium-2331234 24.9 pCilg Uncert: +l-1.51 TPU: +l-3.36 Uranium-2351236 1.50 pCilg Uncert: +l-0.376 TPU: +l-0.417 Uranium-238 24.3 25.0 pCilg 103 (75%-125%) Uncert: +l-1.51 TPU: +l-3.37 QC1203633742 MB Uranium-232 u -0.036 pCi/g KXB2 0912911614:04 Uncert: +l-0.224 TPU: +l-0.224 Uranium-2331234 0.344 pCilg Uncert: +l-0.175 TPU: +l-0.180 Uranium-2351236 0.460 pCilg Uncert: +l-0.202 TPU: +l-0.208 Uranium-238 0.370 pCilg Uncert: +l-0.172 TPU: +l-0.177 Batch 1602285 QC1203636291 405235021 DUP Americium-241 HUh 0.000535 HU -0.0107 pCilg 0 NIAMXS2 0912911621:52 Uncert: +l-0.0397 +l-0.0322 TPU: +l-0.0397 +l-0.0322 Curium-242 HUh -0.0112 H 0.00 pCilg 0 NIA Un cert: +l-0.0964 +l-0.104 TPU: +l-0.0965 +l-0.104 Curium-2431244 HUh -0.00652 HU 0.00781 pCilg 0 NIA Uncert: +l-0.0288 +l-0.0434 TPU: +l-0.0289 +l-0.0435 Curium-2451246 HXh 0.122 H 0.00 pCi/g 82.7 (0%-100%) Uncert: +l-0.0902 +l-0.0341 TPU: +l-0.0915 +l-0.0342 Page 352 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com j QC *workorder: 405235 Page 16 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 1602285 QCl203636292 LCS Americium-241 3.82 4.56 pCilg 119 (75%-125%) MXS2 0912911621:52 Uncert: +l-0.588 TPU: +l-0.899 Curium-242 0.0195 pCilg Uncert: +l-0.055 TPU: +l-0.055 Curium-2431244 5.04 6.01 pCilg 119 (75%-125%) Un cert: +l-0.670 TPU: +l-1.12 Curium-2451246 0.157 pCilg Uncert: +l-0.125 TPU: +l-0.127 QC1203636290 MB Americium-241 0.0346 pCilg MXS2 0912911621 :26 Uncert: +l-0.0549 TPU: +l-0.0551 Curium-242 u -0.00657 pCilg Uncert: +l-0.0291 TPU: +l-0.0291 Curium-2431244 u 0.00703 pCi/g Uncert: +l-0.0391 TPU: +l-0.0391 Curium-2451246 x 0.149 pCi/g Uncert: +l-0.103 TPU: +l-0.105 Rad Gamma Spec Batch 1596247 QC1203621351 405235001 DUP Actinium-227 HUh 0.0104 HU 0.0262 pCi/g 0 NIAMXRl 1010311608:53 Uncert: +l-0.258 +l-0.199 TPU: +l-0.258 +l-0.199 Antimony-125 HUh -0.0487 HUI 0.00 pCi/g 0 NIA Uncert: +l-0.122 +l-0.164 TPU: +l-0.124 +l-0.173 Bismuth-212 HUih 0.00 H 1.80 pCilg 20.5 (0%-100%) Uncert: +l-0.761 +l-1.02 TPU: +l-0.995 +l-1.02 Bismuth-214 Hh 1.03 H 0.864 pCilg 17.1 (0%-20%) Uncert: +l-0.229 +l-0.147 TPU: +l-0.233 +l-0.151 Cesium-137 Hh 0.562 H 0.441 pCilg 24.2* (0%-20%) Uncert: +l-0.104 +l-0.122 TPU: +l-0.107 +l-0.123 Cobalt-60 HUh -0.0365 HU 0.00612 pCi/g 0 NIA Uncert: +l-0.0504 +l-0.0347 TPU: +l-0.0531 +l-0.0348 Page 353 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y: Workorder: 405235 Page 17 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596247 Europium-154 HUh 0.0457 HU -0.0186 pCilg 0 NIA Uncert: +l-0.126 +l-0.0993 TPU: +l-0.128 +l-0.0997 Lead-212 Hh 1.20 H 1.19 pCi/g .669 (0%-20%) Uncert: +l-0.144 +l-0.123 TPU: +l-0.158 +l-0.139 Lead-214 Hh 1.22 H 1.07 pCilg 13.2 (0%-20%) Uncert: +l-0.220 +l-0.186 TPU: +l-0.226 +l-0.191 Potassium-40 Hh 16.9 H 18.1 pCilg 6.99 (0%-20%) Uncert: +l-1.81 +l-1.67 TPU: +l-2.02 +l-1.92 Protactinium-231 HUh 0.0574 HU -0.134 pCilg 0 NIA Uncert: +l-0.533 +l-0.449 TPU: +l-0.534 +l-0.454 Radium-226 Hh 1.03 H 0.864 pCilg 17.1 (0%-20%) Uncert: +l-0.229 +l-0.147 TPU: +l-0.233 +l-0.151 Radium-228 Hh 1.04 H 1.24 pCi/g 17.1 (0%-20%) Uncert: +l-0.294 +l-0.285 TPU: +l-0.299 +l-0.292 Thallium-208 Hh 0.422 H 0.287 pCilg 38.1 * (0%-20%) Uncert: +l-0.0952 +l-0.0816 TPU: +l-0.0969 +l-0.0825 Tin-126 HUih 0.00 HUI 0.00 pCilg 0 NIA Uncert: +l-0.103 +l-0.0976 TPU: +l-0.122 +l-0.0992 QC1203621352 LCS Americium-241 489 541 pCilg 111 (75%-125%) MXRl 10103/1608:54 Uncert: +l-10.I TPU: +l-43.1 Actinium-227 u -0.853 pCilg Uncert: +l-3.70 TPU: +l-3.72 Antimony-125 u -0.647 pCilg Uncert: +l-1.68 TPU: +l-1.71 Bismuth-212 u 0.995 pCilg Uncert: +l-7.92 TPU: +l-7.94 Bismuth-214 u -0.329 pCi/g Uncert: +l-1.08 TPU: +l-1.09 Cesium-137 179 176 pCi/g 98.3 (75%-125%) Uncert: +l-3.51 TPU: +l-15.0 Page 354 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235 Page 18 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596247 Cobalt-60 162 153 pCi/g 94.3 (75%-125%) Un cert: +/-3.86 TPU: +/-12.5 Europium-154 u -0.798 pCi/g Uncert: +/-1.02 TPU: +/-1.09 Lead-212 u 0.273 pCi/g Uncert: +/-0.801 TPU: . +/-0.811 Lead-214 u -0.396 pCi/g Uncert: +/-1.12 TPU: +/-1.13 Potassium-40 u -0.439 pCi/g Uncert: +/-2.34 TPU: +/-2.35 Protactinium-231 u -7.97 pCi/g Uncert: +/-6.63 TPU: +/-7.76 Radium-226 u -0.329 pCi/g Uncert: +/-1.08 TPU: +/-1.09 Radium-228 u 0.270 pCi/g Uncert: +/-3.17 TPU: +/-3.17 Thallium-208 u -0.0447 pCi/g Uncert: +/-0.557 TPU: +/-0.558 Tin-126 38.3 pCi/g Uncert: +/-2.70 TPU: +/-4.16 QC1203621350 MB Actinium-227 u -0.00211 pCi/g MXRl 10/03/1608:50 Uncert: +/-0.166 TPU: +/-0.166 Antimony-125 u -0.0111 pCi/g Uncert: +/-0.0665 TPU: +/-0.0667 Bismuth-212 u -0.012 pCi/g Uncert: +/-0.304 TPU: +/-0.304 Bismuth-214 u 0.0133 pCi/g Uncert: +/-0.0896 TPU: +/-0.0896 Cesium-137 u 0.028 pCi/g Uncert: +/-0.0253 TPU: +/-0.0283 Page 355 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Workorder: 405235 Page 19 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596247 Cobalt-60 u -0.0144 pCi/g Uncert: +/-0.0349 TPU: +/-0.0355 Europium-154 u -0.00702 pCi/g Uncert: +/-0.0946 TPU: +/-0.0947 Lead-212 u -0.0294 pCi/g Uncert: +/-0.0457 TPU: +/-0.0476 Lead-214 u 0.00584 pCi/g Uncert: +/-0.0668 TPU: +/-0.0668 Potassium-40 u -0.307 pCi/g Uncert: +/-0.401 TPU: +/-0.425 Protactinium-231 u -0.0946 pCi/g Uncert: +/-0.290 TPU: +/-0.294 Radium-226 u 0.0133 pCi/g Uncert: +/-0.0896 TPU: +/-0.0896 Radium-228 u 0.0959 pCi/g Uncert: +/-0.141 TPU: +/-0.148 Thallium-208 u 0.0174 pCi/g Uncert: +/-0.0327 TPU: +/-0.0337 Tin-126 u -0.00222 pCi/g Uncert: +/-0.0316 TPU: +/-0.0316 Batch 1596249 QC1203621355 405235038 DUP Actinium-227 HUh -0.024 HU 0.0379 pCi/g 0 N/AMXRI I 0/03/16 09:21 Uncert: +/-0.214 +/-0.177 TPU: +/-0.215 +/-0.178 Antimony-125 HUh -0.0676 HU 0.0181 pCi/g 0 NIA Uncert: +/-0.0977 +/-0.0746 TPU: +/-0.102 +/-0.0751 Bismuth-212 HUih 0.00 HUI 0.00 pCi/g 0 NIA Uncert: +/-1.34 +/-0.873 TPU: +/-1.72 +/-I.OJ
Bismuth-214 Hh 0.567 H 0.774 pCi/g 30.8* (0%-20%) Uncert: +/-0.155 +/-0.162 TPU: +/-0.157 +/-0.166 Cesium-137 Hh 0.115 HUI 0.00 pCi/g 74.7 (0%-100%) Uncert: +/-0.0596 +/-0.0694 Page 356 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Workorder: 405235 Page 20 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596249 TPU: +l-0.0598 +l-0.0694 Cobalt-60 HUh 0.0113 HU 0.00345 pCilg 0 NIA Uncert: +l-0.0424 +l-0.0252 TPU: +l-0.0427 +l-0.0252 Europium-154 HUh -0.0421 HU 0.0338 pCi/g 0 NIA Uncert: +l-0.122 +l-0.0842 TPU: +l-0.123 +l-0.0856 Lead-il2 Hh 0.937 H 0.876 pCilg 6.71 (0%-20%) Uncert: +l-0.121 +l-0.135 TPU: +l-0.131 +l-0.143 Lead-214 Hh 0.776 H 1.07 pCilg 31.8* (0%-20%) Un cert: +l-0.168 +l-0.167 TPU: +l-0.171 +l-0.173 Potassium-40 Hh 12.4 H 12.0 pCilg 2.95 (0%-20%) Un cert: +l-1.44 +l-1.20 TPU: +l-1.58 +l-1.35 Protactinium-231 HUlh 0.00 HUI 0.00 pCi/g 0 NIA Uncert: +l-0.599 +l-0.581 TPU: +l-0.616 +l-0.626 Radium-226 Hh 0.567 H 0.774 pCilg 30.8* (0%-20%) Uncert: +l-0.155 +l-0.162 TPU: +l-0.157 +l-0.166 Radium-228 Hh 0.819 H 0.779 pCilg 5.09 (0%-100%) Uncert: +l-0.386 +l-0.284 TPU: +l-0.388 +l-0.287 Thallium-208 Hh 0.285 H 0.308 pCilg 8.03 (0%-20%) Un cert: +l-0.0667 +l-0.0765 TPU: +l-0.0678 +l-0.0776 Tin-126 HUih 0.00 HU 0.0281 pCilg 0 NIA Uncert: +l-0.194 +l-0.113 TPU: +l-0.195 +l-0.114 QC1203621356 LCS Americium-241 489 550 pCilg 112 (75%-125%) MXRI 1010311609:11 Un cert: +l-12.2 TPU: +l-44.3 Actinium-227 u 0.0258 pCilg Uncert: +l-3.69 TPU: +l-3.69 Antimony-125 u -0.919 pCilg Uncert: +l-1.65 TPU: +l-1.70 Bismuth-212 u 3.24 pCilg Uncert: +l-8.15 TPU: +l-8.29 Bismuth-214 u -0.366 pCilg Uncert: +l-1.10 Page 357 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summarl:'. Workorder: 405235 Page 21 of 39 Parmname NOM Qua! QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596249 TPU: +/-1.11 Cesiurn-13 7 179 175 pCi/g 97.8 (75%-125%) Uncert: +/-3.45 TPU: +/-14.9 Cobalt-60 162 153 pCi/g 94.4 (75%-125%) Uncert: +/-3.77 TPU: +/-12.5 Europiurn-154 u 0.318 pCi/g Uncert: +/-1.14 TPU: +/-1.15 Lead-212 u 0.185 pCi/g Uncert: +/-0.774 TPU: +/-0.778 Lead-214 u 0.861 pCi/g Uncert: +/-1.11 TPU: +/-1.18 Potassiurn-40 u 0.257 pCi/g Un cert: +/-2.57 TPU: +/-2.57 Protactinium-231 u -1.17 pCi/g Uncert: +/-6.68 TPU: +/-6.70 Radiurn-226 u -0.366 pCi/g Uncert: +/-1.10 TPU: +/-1.11 Radiurn-228 u 1.60 pCi/g Uncert: +/-3.24 TPU: +/-3.32 Thallium-208 u -0.126 pCi/g Uncert: +/-0.551 TPU: +/-0.554 Tin-126 35.4 pCi/g Uncert: +/-2.38 TPU: +/-3.77 QC1203621354 MB Actiniurn-227 u 0.0024 pCi/g MXRl 10/03/16 09:20 Uncert: +/-0.109 TPU: +/-0.109 Antimony-125 u 0.0346 pCi/g Uncert: +/-0.0376 TPU: +/-0.0407 Bismuth-212 u 0.00283 pCi/g Uncert: +/-0.222 TPU: +/-0.222 Bisrnuth-214 u 0.0218 pCi/g Uncert: +/-0.043 Page 358 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Workorder: 405235 QC Summar:r Page 22 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596249 TPU: +l-0.0442 Cesium-137 u -0.0156 pCilg Uncert: +l-0.020 TPU: +l-0.0212 Cobalt-60 u 0.00355 pCilg Uncert: +l-0.0145 TPU: +l-0.0146 Europium-154 u -0.00923 pCilg Uncert: +l-0.039 TPU: +l-0.0393 Lead-212 u -0.0403 pCilg Uncert: +l-0.0274 TPU: +l-0.0329 Lead-214 u 0.020 pCilg Uncert: +l-0.0382 TPU: +l-0.0393 Potassium-40 u 0.120 pCilg Uncert: +l-0.322 TPU: +l-0.323 Protactinium-231 u 0.0281 pCi/g Uncert: +l-0.180 TPU: +l-0.180 Radium-226 u 0.0218 pCi/g Uncert: +l-0.043 TPU: +l-0.0442 Radium-228 u -0.043 pCilg Uncert: +l-0.066 TPU: +l-0.0689 Thallium-208 u 0.00107 pCilg Uncert: +l-0.0148 TPU: +l-0.0148 Tin-126 u 0.00835 pCi/g Uncert: +l-0.0266 TPU: +l-0.0269 Batch 1596252 QC1203621362 405235041 DUP Actinium-227 HUh 0.0314 HU 0.0461 pCi/g 0 NIAMXRl 1010311607:54 Uncert: +l-0.177 +l-0.164 TPU: +l-0.177 +l-0.166 Antimony-125 HUh -0.0586 HU 0.00169 pCi/g 0 NIA Uncert: +l-0.0781 +l-0.0712 TPU: +l-0.0825 +l-0.0712 Bismuth-212 HUih 0.00 HUI 0.00 pCi/g 0 NIA Uncert: +l-0.700 +l-0.892 TPU: +l-0.824 +l-0.959 Bismuth-214 Hh 0.794 H 0.654 pCi/g 19.3 (0%-20%) Page 359 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Workorder: 405235 QC Summar:y Page 23 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596252 Uncert: +l-0.159 +l-0.138 TPU: +l-0.163 +l-0.141 Cesium-137 HUih 0.00 HUI 0.0546 pCilg 4.56 (0%-100%) Uncert: +l-0.049 +l-0.0611 TPU: +l-0.049 +l-0.0612 Cobalt-60 HUh 0.0168 HU -0.00701 pCi/g 0 NIA Uncert: +l-0.033 +l-0.0329 TPU: +l-0.0339 +l-0.033 Europium-154 HUh -0.00765 HU -0.0325 pCilg 0 NIA Uncert: +l-0.101 +l-0.0702 TPU: +l-0.101 +l-0.0717 Lead-212 Hh 0.807 H 0.736 pCi/g 9.17 (0%-20%) Uncert: +l-0.113 +l-0.102 TPU: +l-0.121 +l-0.109 Lead-214
Hh 0.803 H 0.934 pCilg 15.1 (0%-20%) Uncert: +l-0.167 +l-0.157 TPU: +l-0.170 +l-0.162 Potassium-40 Hh 11.8 H 13.4 pCi/g 12.4 (0%-20%) Uncert: +l-1.23 +l-1.28 TPU: +l-1.38 +l-1.46 Protactinium-231 HUih 0.00 HU -0.182 pCilg 23.5 NIA Uncert: +l-0.541 +l-0.342 TPU: +l-0.565 +l-0.354 Radium-226 Hh 0.794 H 0.654 pCi/g 19.3 (0%-20%) Uncert: +l-0.159 +l-0.138 TPU: +l-0.163 +l-0.141 Radium-228 Hh 0.629 H 0.529 pCi/g 17.2 (0%-100%) Uncert: +l-0.246 +l-0.228 TPU: +l-0.249 +l-0.230 Thallium-208 Hh 0.273 H 0.230 pCilg 17.3 (0%-20%) Uncert: +l-0.0808 +l-0.0708 TPU: +/-0.0816 +l-0.0715 Tin-126 HUh 0.0427 HUI 0.00 pCi/g 14.1 NIA Uncert: +l-0.187 +l-0.102 TPU: +l-0.188 +l-0.103 QCl203621363 LCS Americium-241 489 544 pCi/g 111 (75%-125%) MXRl 1010311605:45 Uncert: +l-7.77 TPU: +l-40.8 Actinium-227 u 1.33 pCi/g Uncert: +l-3.42 TPU: +l-3.48 Antimony-125 u 0.557 pCi/g Uncert: +l-1.53 TPU: +l-1.55 Bismuth-212 u -1.37 pCi/g Page 360 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar,Y Workorder: 405235 Page 24 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596252 Uncert: +/-7.06 TPU: +/-7.09 Bisrnuth-214 u 0.115 pCi/g Uncert: +/-0.961 TPU: +/-0.962 Cesiurn-13 7 179 189 pCi/g 105 (75%-125%) Uncert: +/-3.32 TPU: +/-8.75 Cobalt-60 162 157 pCi/g 97.2 (75%-125%) Uncert: +/-3.49 TPU: +/-6.75 Europiurn-154 u -0.324 pCi/g Uncert: +/-0.939 TPU: +/-0.950 Lead-212 u -0.0245 pCi/g Uncert: +/-0.707 TPU: +/-0.707 Lead-214 1.37 pCi/g Uncert: +/-1.68 TPU: +/-1.79 Potassiurn-40 u -1.01 pCi/g Uncert: +/-2.19 TPU: +/-2.24 Protactiniurn-231 u -0.788 pCi/g Uncert: +/-6.41 TPU: +/-6.42 Radiurn-226 u 0.115 pCi/g Uncert: +/-0.961 TPU: +/-0.962 Radium-228 u -2.57 pCi/g Uncert: +/-2.82 TPU: +/-3.05 Thalliurn-208 u -0.432 pCi/g Uncert: +/-0.509 TPU: +/-0.545 Tin-126 40.7 pCi/g Uncert: +/-2.18 TPU: +/-3.34 QC1203621361 MB Actiniurn-227 u -0.028 pCi/g 'MXRl 10/03/16 07:53 Uncert: +/-0.0998 TPU: +/-0.101 Antirnony-125 u -0.0423 pCi/g Uncert: +/-0.037 TPU: +/-0.0417 Bisrnuth-212 u 0.0179 pCi/g Page 361 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Workorder: 405235 Page 25 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596252 Uncert: +/-0.238 TPU: +/-0.238 Bismuth-214 u 0.011 pCi/g Uncert: +/-0.0391 TPU: +/-0.0394 Cesium-137 u 0.00281 pCi/g Uncert: +/-0.0144 TPU: +/-0.0144 Cobalt-60 u 0.0143 pCi/g Uncert: +/-0.0147 TPU: +/-0.0161 Europium-154 u 0.00394 pCi/g Uncert: +/-0.0315 TPU: +/-0.0315 Lead-212 u 0.00468 pCi/g Uncert: +/-0.0237 TPU: +/-0.0238 Lead-214 u -0.00503 pCi/g Uncert: +/-0.035 TPU: +/-0.0351 Potassium-40 u -0.109 pCi/g Uncert: +/-0.171 TPU: +/-0.178 Protactinium-231 u 0.0246 pCi/g Uncert: +/-0.174 TPU: +/-0.174 Radium-226 u 0.011 pCi/g Uncert: +/-0.0391 TPU: +/-0.0394 Radium-228 u 0.00265 pCi/g Uncert: +/-0.0623 TPU: +/-0.0623 Thallium-208 u 0.011 pCi/g Uncert: +/-0.0203 TPU: +/-0.0209 Tin-126 u 0.0098 pCi/g Uncert: +/-0.0201 TPU: +/-0.0206 Batch 1596254 QCI203621365 405235061 DUP Actinium-227 HUh -0.12 HU -0.0297 pCi/g 0 N/AMXRl 10/03/1606:55 Uncert: +/-0.189 +/-0.227 TPU: +/-0.197 +/-0.227 Antimony-125 HUh 0.068 HU 0.0819 pCi/g 0 NIA Uncert: +/-0.0832 +/-0.107 TPU: +/-0.0887 +/-0.113 Page 362 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Sum.marI Workorder: 405235 Page 26 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596254 Bismuth-212 HUih 0.00 HUI 0.00 pCi/g 0 NIA Uncert: +l-0.504 +l-0.911 TPU: +l-0.633 +l-1.09 Bismuth-214 Hh 0.922 H 1.18 pCi/g 24.8* (0%-20%) Uncert: +l-0.164 +l-0.181
TPU: +l-0.168 +l-0.188 Cesium-137 HUh 0.0251 H 0.161 pCilg 68.8 (0%-100%) Uncert: +l-0.039 +l-0.0673 TPU: +l-0.0407 +l-0.0676 Cobalt-60 HUh 0.0224 HU -0.0228 pCi/g 0 NIA Uncert: +l-0.0301 +l-0.0348 TPU: +l-0.0318 +l-0.0363 Europium-154 HUh 0.0331 HUI 0.00 pCi/g 0 NIA Uncert: +l-0.098 +l-0.117 TPU: +l-0.0992 +l-0.130 Lead-212 Hh 0.802 H 0.931 pCi/g 14.9 (0%-20%) Uncert: +l-0.112 +l-0.126 TPU: +l-0.120 +l-0.135 Lead-214 Hh 1.19 H 1.34 pCilg 11.9 (0%-20%) Un cert: +l-0.158 +l-0.206 TPU: +l-0.166 +l-0.213 Potassium-40 Hh 10.5 H 11.9 pCi/g 12.4 (0%-20%) Uncert: +l-1.37 +l-1.40 TPU: +l-1.47 +l-1.53 Protactinium-231 HUih 0.00 HUI 0.00 pCilg 14.9 NIA Uncert: +l-0.553 +l-0.780 TPU: +l-0.593 +l-0.785 Radium-226 Hh 0.922 H 1.18 pCilg 24.8* (0%-20%) Uncert: +l-0.164 +l-0.181 TPU: +l-0.168 +l-0.188 Radium-228 HUih 0.00 H 0.741 pCilg 18.7 (0%-100%) Uncert: +l-0.227 +l-0.368 TPU: +l-0.465 +l-0.370 Thallium-208 Hh 0.264 H 0.231 pCi/g 13.6 (0%-20%) Uncert: +l-0.0737 +l-0.0777 TPU: +l-0.0745 +l-0.0784 Tin-126 HUh 0.0261 HUI 0.00 pCi/g 56.9 NIA Uncert: +l-0.125 +l-0.0789 TPU: +l-0.126 +l-0.119 QC120362!366 LCS Americium-241 489 562 pCilg 115 (75%-125%) MXRl 1010311605:28 Uncert: +l-9.26 TPU: +l-42.4 Actinium-227 u -0.721 pCilg Un cert: +l-3.25 TPU: +l-3.26 Page 363 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Workorder: 405235 QC Summar:y Page 27 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596254 Antimony-125 u 0.821 pCi/g Uncert: +l-1.55 TPU: +/-1.59 Bismuth-212 u -1.2 pCi/g Uncert: +/-7.37 TPU: +/-7.39 Bismuth-214 u 0.183 pCi/g Uncert: +/-0.955 TPU: +/-0.959 Cesium-137 179 195 pCi/g 108 (75%-125%) Uncert: +/-3.39 TPU: +/-9.01 Cobalt-60 162 160 pCi/g 98.8 (75%-125%) Uncert: +/-3.46 TPU: +/-6.82 Europium-154 u 0.0867 pCi/g Uncert: +/-0.929 TPU: +/-0.930 Lead-212 u -0.0738 pCi/g Uncert: +/-0.686 TPU: +/-0.686 Lead-214 u 0.372 pCi/g Uncert: +/-1.00 TPU: +/-1.01 Potassium-40 u 0.749 pCi/g Uncert: +/-2.54 TPU: +/-2.56 Protactinium-231 u -2.71 pCi/g Uncert: +/-6.49 TPU: +/-6.63 Radium-226 u 0.183 pCi/g Uncert: +/-0.955 TPU: +/-0.959 Radium-228 u -1.64 pCi/g Uncert: +/-2.91 TPU: +/-3.00 Thallium-208 u 0.0682 pCi/g Uncert: +/-0.498 TPU: +/-0.499 Tin-126 39.8 pCi/g Uncert: +/-2.19 TPU: +/-3.30 QCl203621364 MB Actinium-227 u 0.109 pCi/g MXRl 10/03/16 06:55 Uncert: +/-0.136 TPU: +/-0.145 Page 364of5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235 Page 28 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1596254 Antimony-125 u -0.0541 pCi/g Uncert: +/-0.0598 TPU: +/-0.0646 Bismuth-212 u -0.00482 pCi/g Uncert: +/-0.343 TPU: +/-0.343 Bismuth-214 u -0.014 pCi/g Uncert: +/-0.060 TPU: +/-0.0604 Cesium-137 UI 0.00 pCi/g Uncert: +/-0.0248 TPU: +/-0.0248 Cobalt-60 u -0.00794 pCi/g Uncert: +/-0.0197 TPU: +/-0.020 Europium-154 u -0.0127 pCi/g Uncert: +/-0.0476 TPU: +/-0.0479 Lead-212 u 0.0243 pCi/g Uncert: +/-0.0666 TPU: +/-0.0675 Lead-214 u -0.0308 pCi/g Uncert: +/-0.0485 TPU: +!-0.0505 Potassium-40 u 0.0557 pCi/g Uncert: +/-0.284 TPU: +/-0.284 Protactinium-231 u -0.142 pCi/g Uncert: +/-0.262 TPU: +/-0.271 Radium-226 u -0.014 pCi/g Uncert: +/-0.060 TPU: +/-0.0604 Radium-228 UI 0.00 pCi/g Uncert: +/-0.109 TPU: +/-0.132 Thallium-208 u 0.00626 pCi/g Uncert: +/-0.0281 TPU: +/-0.0282 Tirt-126 u . 0.000999 pCi/g Uncert: +/-0.0457 TPU: +/-0.0457 Batch 1598618 QC1203627431 405235001 DUP Iodine-129 HUh -0.016 HU 0.087 pCi/g 0 N/AMllil 09/28/1608:03 Uncert: +/-0.176 +/-0.366 Page 365 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y: Workorder: 405235 Page 29 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1598618 TPU: +/-0.177 +/-0.368 QC1203627433 LCS Iodine-129 12.5 10.5 pCi/g 84.3 (75%-125%) MJHl 09/28/1608:11 Uncert: +/-1.50 TPU: +/-1.82 QC1203627430 MB Iodine-129 u -0.011 pCi/g MJHl 09/28/1607:39 Uncert: +/-0.173 TPU: +/-0.173 . QC1203627432 405235001 MS Iodine-129 16.3 HUh -0.016 H 13.0 pCi/g 79.8 (75%-125%) MJHl 09/28/1608:04 Uncert: +/-0.176 +/-2.16 TPU: +/-0.177 +/-2.52 Batch 1598620 QC1203627438 405235021 DUP Iodine-129 HUh 0.057 HU 0.243 pCi/g 0 N/AMJHl 09/28/1612:51 Uncert: +/-0.204 +/-0.267 TPU: +/-0.206 +/-0.289 QC1203627440 LCS Iodine-129 11.8 13.2 pCi/g 112 (75%-125%) MJHl 09/28/1612:52 Uncert: +/-1.91 TPU: +/-2.31 QC1203627437 MB Iodine-129 u 0.0472 pCi/g MJHl 09/28/1612:50 Uncert: +/-0.190 TPU: +/-0.191 QC1203627439 405235021 MS Iodine-129 14.2 HUh 0.057 H 12.0 pCi/g 84.6 (75%-125%) MJHl 09/28/1612:52 Uncert: +/-0.204 +/-1.68 TPU: +/-0.206 +/-2.06 Batch 1598647 QC1203627503 405235041 DUP Iodine-129 HUh 0.176 HU -0.153 pCi/g 0 NIA MJHl 09/28/1619:04 Uncert: +/-0.244 +/-0.323 TPU: +/-0.257 +/-0.330 QC1203627505 LCS Iodine-129 11.2 10.4 pCi/g 92.4 (75%-125%) MJHl 09/29/1609: 10 Uncert: +/-1.03 TPU: +/-1.47 QC1203627502 MB Iodine-129 u -0.153 pCi/g MJHl 09/28/1615:50 Uncert: +/-0.195 TPU: +/-0.207 QC1203627504 405235041 MS Iodine-129 13.1 HUh 0.176 H 14.l pCi/g 107 (75%-125%) MJHl 09/28/1619:05 Page 366 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235° Page 30 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1598647 Uncert: +/-0.244 +/-1.36 TPU: +/-0.257 +/-1.95 Batch 1598663 QC1203627532 405235061 DUP Iodine-129 HUih 0.00 HU 0.034 pCi/g 0 N/AMJHl 09/29/1608:03 Uncert: +/-0.328 +/-0.118 TPU: +/-0.328 +/-0.119 QCl203627534 LCS Iodine-129 9.84 10.0 pCi/g 102 (75%-125%) MJHl 09/29/1608:33 Un cert: +/-1.44 TPU: +/-1.74 QC1203627531 MB Iodine-129 u 0.00336 pCi/g MJHl 09/29/1608:03 Uncert: +/-0.230 TPU: +/-0.230 QC1203627533 405235061 MS Iodine-129 14.0 HUih 0.00 H 12.1 pCi/g 86.9 (75%-125%) MJHl 09/29/1608:04 Uncert: +/-0.328 +/-2.48 TPU: +/-0.328 +/-2.76 Rad Gas Flow Batch 1597795 QC!203625399 405235005 DUP Strontium-90 HUh -0.135 HU -0.662 pCi/g 0 N/AKSDl 09/17/1616:39 Uncert: +/-0.565 +/-0.742 TPU: +/-0.565 +/-0.742 QC 1203625400 LCS Strontium-90 25.9 26.7 pCi/g 103 (75%-125%) KSDl 09/17 /1616:39 Uncert: +/-1.40 TPU: +/-4.98 QC1203625398 MB Strontium-90 u -0.169 pCi/g KSDl 09/17/1616:40 Uncert: +/-0.211 TPU: +/-0.211 Batch 1597796 QC1203625402 405235025 DUP Strontium-90 HUh 0.106 HU 0.0519 pCi/g 0 N/AKSDl 09/17/1615:45 Uncert: +/-0.613 +/-0.715 +/-0.614 +/-0.715 QC!203625403 LCS Strontium-90 46.1 45.9 pCi/g 99.4 (75%-125%) KSDl 09/17/1615:45 Uncert: +/-2.35 TPU: +/-8.52 QC1203625401 MB Strontium-90 u -0.0178 pCi/g KSDl 09/17/1615:37 Un cert: +/-0.356 Page 367 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summarl: Workorder: 405235 Page 31 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gas Flow Batch 1597796 TPU: +/-0.356 Batch 1597803 QC1203625409 405235045 DUP Strontium-90 Hh 0.742 HU -1.02 pCi/g 0 N/AKSDl 09/22/1617:18 Uncert: +/-0.723 +/-0.730 TPU: +/-0.737 +/-0.730 QC1203625410 LCS Strontium-90 37.9 43.6 pCi/g 115 (75%-125%) ,KSDI 09/22/1617: 18 Uncert: +/-2.41 TPU: +/-8.33 QC1203625408 MB Strontium-90 u 0.054 pCi/g KSDI 09/22/1617:18 Uncert: +/-0.342 TPU: +/-0.342 Batch 1597804 QC1203625413 405235065 DUP Strontium-90 Hh 1.02 HU 0.278 pCi/g 0 NIA BXFl 09/28/1608:54 Uncert: +/-0.909 +/-0.577 TPU: +/-0.929 +/-0.579 QC1203625414 LCS Strontium-90 58.2 61.6 pCi/g 106 (75%-125%) BXFl 09/28/1608:54 Uncert: +/-3.25 TPU: +/-11.9 QC1203625412 MB Strontium-90 u -0.289 pCi/g BXFl 09/27/1615:37 Uncert: +/-0.526 TPU: +/-0.526 Batch 1597811 QCJ203625436 405235033 DUP Alpha Hh 11.6 H 12.l pCi/g 4.49 (0% -100%) BXFl 09/19/1614:36 Uncert: +/-3.82 +/-3.36 TPU: +/-4.42 +/-4.13 Beta Hh 15.8 H 15.9 pCi/g .634 (0%-20%) Uncert: +/-2.74 +/-2.28 TPU: +/-3.54 +/-3.21 QC1203625439 LCS Alpha 95.l 88.9 pCi/g 93.4 (75%-125%) BXFl 09/19/1616:05 Uncert: +/-8.60 TPU: +/-19.4 Beta 346 380 pCi/g 110 (75%-125%) Uncert: +/-13.7 TPU: +/-55.8 QCJ203625435 MB Alpha u 0.190 pCi/g BXFI 09/19/1614:36 Uncert: +/-1.62 Page 368 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Summar,Y Workorderi 405235 Page 32 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gas Flow Batch 1597811 TPU: +/-1.62 Beta u 0.538 pCi/g Uncert: +/-1.45 TPU: +/-1.46 QC1203625437 405235033 MS Alpha 113 Hh 11.6 H 129 pCi/g 104 (75%-125%) BXFl 09/19/1616:05 Uncert: +/-3.82 +/-15.l TPU: +/-4.42 +/-29.l Beta 411 Hh 15.8 H 440 pCi/g 103 (75%-125%) Uncert: +/-2.74 +/-16.0 TPU: +/-3.54 +/-64.0 QC1203625438 405235033 MSD Alpha 113 Hh 11.6 H 142 pCi/g 9.51 116 (0%-20%) BXFl 09/19/1616:05 Uncert: +/-3.82 +/-16.1 TPU: +/-4.42 +/-31.9 Beta 411 Hh 15.8 H 438 pCi/g .51 103 (0%-20%) Uncert: +/-2.74 +/-16.8 TPU:' +/-3.54 +/-64.7 Batch 1597816 QC1203625450 405235013 DUP Alpha Hh 17.1 H 19.8 pCi/g 14.5 (0%-20%) JXC9 09/20/1611 :56 Uncert: +/-4.66 +/-4.36 TPU: +/-5.72 +/-5.82 Beta Hh 24.3 H 20.1 pCi/g 18.9 (0%-20%) Uncert: +/-3.36 +/-2.88 TPU: +/-4.90 +/-4.12 QC1203625453 LCS Alpha 109 105 pCi/g 96.5 (75%-125%) JXC9 09/19/1612:37 Uncert: +/-10.3 TPU: +/-23.7 Beta 396 410 pCi/g 104 (75%-125%) Un cert: +/-15.0 TPU: +/-58.3 QC1203625449 MB Alpha u 0.0336 pCi/g JXC9 09/19/1612:20 Uncert: +/-1.85 TPU: +/-1.85 Beta u -0.87 pCi/g Uncert: +/-1.81 TPU: +/-1.81 QC1203625451 405235013 MS Alpha 109 Hh 17.l H 109 pCi/g 83.9 (75%-125%) JXC9 09/20/1611 :56 Uncert: +/-4.66 +/-14.2 TPU: +/-5.72 +/-25.6 Beta 396 Hh 24.3 H 428 pCi/g 102 (75%-125%) Uncert: +/-3.36 +/-15.8 Page 369 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar.Y
Workorder: 405235 Page 33 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gas Flow Batch 1597816 TPU: +/-4.90 +/-63.2 QC1203625452 405235013 MSD Alpha 110 Hh 17.1 H 116 pCi/g 6.65 90 (0%-20%) JXC9 09/20/1611 :56 Un cert: +/-4.66 +/-15.6 TPU: +/-5.72 +/-27.4 Beta 400 Hh 24.3 H 452 pCi/g 5.3 107 (0%-20%) Uncert: +/-3.36 +/-16.4 TPU: +/-4.90 +/-65.4 Batch 1597817 QC 1203625460 405235073 DUP Alpha Hh 27.6 H 20.0 pCi/g 32* (0%-20%) JXC9 09/22/1614:00 Uncert: +/-5.03 +/-4.54 TPU: +/-7.39 +/-5.94 Beta Hh 39.4 H 27.9 pCi/g 34.3* (0%-20%) Uncert: +/-3.28 +/-3.51 TPU: +/-6.39 +/-5.27 QC1203625463 LCS Alpha 108 108 pCi/g 100 (75%-125%) JXC9 09/22/1613:58 Uncert: +/-10.4 TPU: +/-24.1 Beta 392 436 pCi/g 111 (75%-125%) Uncert: +/-15.5 TPU: +/-62.0 QC1203625459 MB Alpha u -1.29 pCi/g JXC9 09/22/1614:00 Uncert: +/-1.11 TPU: +/-1.11 Beta u -0.444 pCi/g Uncert: +/-1.41 TPU: +/-1.41 QCJ203625461 405235073 MS Alpha 116 Hh 27.6 H 118 pCi/g 77.4 (75%-125%) JXC9 09/23/1613:24 Uncert: +/-5.03 +/-13.3 TPU: +/-7.39 +/-26.8 Beta 423 Hh 39.4 H 359 pCi/g 75.7 (75%-125%) Uncert: +/-3.28 +/-14.5 TPU: +/-6.39 +/-52.3 QC1203625462 405235073 MSD Alpha 113 Hh 27.6 H 141 pCi/g 18.2 100 (0%-20%) JXC9 09/2211613:58 Uncert: +/-5.03 +/-15.6 TPU: +/-7.39 +/-31.9 Beta 411 Hh 39.4 H 389 pCi/g 7.96 85.1 (0%-20%) Uncert: +/-3.28 +/-15.9 TPU: +/-6.39 +/-57.0 Batch 1602427 QC1203636654 405235045 DUP Page 370 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summarl'.: Workorder: 405235 Page 34 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Gas Flow Batch 1602427 Alpha Hh 15.6 H 19.2 pCi/g 20.8 (0% -100%) JXC9 09/28/1614:47 Uncert: +/-3.57 +/-3.82 TPU: +/-4.60 +/-5.36 Beta Hh 20.5 H 24.4 pCi/g 17.2 (0%-20%) Uncert: +/-2.55 +/-2.37 TPU: +/-3.71 +/-4.16 QC1203636657 LCS Alpha 107 113 pCi/g 106 (75%-125%) JXC9 09/28/1614:47 Uncert: +/-10.8 TPU: +/-24.3 Beta 389 441 pCi/g 113 (75%-125%) Uncert: +/-15.8 TPU: +/-63.3 QC1203636653 MB Alpha u 0.070 pCi/g JXC9 09/28/1614:4 7 Uncert: +/-1.26 TPU: +/-1.26 Beta u -2.93 pCi/g Uncert: +/-2.07 TPU: +/-2.07 QC1203636655 405235045 MS Alpha 115 Hh 15.6 H 155 pCi/g 121 (75%-125%) JXC9 09/29/1613:04 Uncert: +/-3.57 +/-16.2 TPU: +/-4.60 +/-34.9 Beta 419 Hh 20.5 H 443 pCi/g 101 (75%-125%) Uncert: +/-2.55 +/-15.9 TPU: +/-3.71 +/-63.6 QC1203636656 405235045 MSD Alpha 120 Hh 15.6 H 161 pCi/g 3.41 121 (0%-20%) JXC9 09/29/1613:04 Uncert: +/-3.57 +/-16.5 TPU: * +/-4.60 +/-34.5 Beta 435 Hh 20.5 H 488 pCi/g 9.74 108 (0%-20%) Uncert: +/-2.55 +/-17.1 TPU: +/-3.71 +/-63.8 Rad Liquid Scintillation Batch 1597412 QC1203624302 405235021 DUP Technetium-99 HUh 1.02 H 1.66 pCi/g 0 NIA CXS7 09/20/1621:55 Uncert: +/-1.78 +/-1.88 TPU: +/-1.78 +/-1.89 QC1203624303 LCS Technetium-99 67.5 77.5 pCi/g 115 (75%-125%) CXS1 09/20/1622:27 Uncert: +/-2.99 TPU: +/-9.39 QC1203624301 MB Technetium-99 u -1.36 pCi/g CXS7 09/20/16 21 :23 Page 371 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235 Page 35 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1597412 Uncert: +l-1.38 TPU: +l-1.38 Batch 1597414 QC1203624305 405235041 DUP Technetium-99 HUh 0.325 HU 0.594 pCilg 0 NIA CXS7 0912011619:08 Uncert: +l-1.62 +l-1.66 TPU: +l-1.62 +l-1.66 QC1203624306 LCS Technetium-99 74.5 81.1 pCi/g 109 (75%-125%) CXS7 0912011619:24 Uncert: +l-4.23 TPU: +l-10.2 QC1203624304 MB Technetium-99 u 0.445 pCilg CXS7 0912011618:51 Uncert: +l-1.51 TPU: +l-1.51 Batch 1597416 QC1203624309 405235001 DUP Technetium-99 HUh -1.43 HU -0.522 pCi/g 0 NIAGXRl 0912011610: 19 Uncert: +l-1.28 +l-1.18 TPU: +l-1.28 +l-1.18 QC1203624310 LCS Technetium-99 40.3 39.9 pCi/g 99.1 (75%-125%) GXRl 0912011610:35 Uncert: +l-2.06 TPU: +l-5.03 QC1203624308 MB Technetium-99 u 0.212 pCi/g GXRl 0912011610:03 Uncert: +l-0.938 TPU: +l-0.939 Batch 1597417 QC1203624312 405235061 DUP Technetium-99 HUh 0.147 HU -0.0928 pCilg 0 NIA CXS7 0912011614:41 Uncert: +l-0.973 +l-0.978 TPU: +l-0.974 +l-0.978 QC1203624313 LCS Technetium-99 71.2 73.0 pCilg 103 (75%-125%) CXS7 0912011615:09 Uncert: +l-2.93 TPU: +l-8.88 QC1203624311 MB Technetium-99 u -0.31 pCilg CXS7 09120/1614:13 Uncert: +l-0.742 TPU: +l-0.742 Batch 1598072 QC1203626095 405235001 DUP Tritium HUh 0.0866 HU 0.210 pCilg 0 NIA AEA 0912011623:10 Uncert: +l-1.90 +l-2.48 Page 372 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Workorder: 405235 Page 36 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1598072 TPU: +l-l.90 +l-2.48 QC1203626097 LCS Tritium 33.0 33.8 pCilg 102 (75%-125%) AEA 0912111600:58 Uncert: +l-5.98 TPU: +l-6.00 QC1203626094 MB Tritium u -0.953 pCilg AEA 0912011621:37 Uncert: +l-l.64 TPU: +l-l.64 QC1203626096 405235001 MS Tritium 38.7 HUh 0.0866 H 37.0 pCilg 95.6 (75%-125%) AEA 09121/1600:42 Uncert: +l-l.90 +l-6.91 TPU: +l-l.90 +l-6.94 Batch 1598075 QC!203626099 405235021 DUP Tritium Hh 2.57 H 2.22 pCi/g 0 NIA TXP3 09/2311603:42 Uncert: +l-2.07 +l-2.14 TPU: +l-2.07 +l-2.14 QC!203626101 LCS Tritium 35.6 32.1 pCilg 90.2 (75%-125%) TXP3 09123/1604:32 Uncert: +l-5.28 TPU: +l-5.31 QC1203626098 MB Tritium 1.40 pCi/g TXP3 0912311603: 10 Uncert: +l-1.61 TPU: +l-1.61 QC1203626100 405235021 MS Tritium 43.5 Hh 2.57 H 39.8 pCi/g 91.5 (75%-125%) TXP3 0912311604:15 Uncert: +l-2.07 +l-6.50 TPU: +l-2.07 +l-6.53 Batch 1598078 QC!203626 l 06 405235001 DUP Carbon-14 HUh -0.321 HU -0.248 pCilg 0 NIA AEA 09122/1618:03 Uncert: +l-0.636 +l-0.603 TPU: +l-0.636 +l-0.603 QC!203626108 LCS Carbon-14 49.9 47.8 pCi/g 95.6 (75%-125%) AEA 0912211619:06 Uncert: +l-2.46 TPU: +l-4.26 QC1203626105 MB Carbon-14 u -0.226 pCilg AEA 0912211617: 16 Uncert: +l-0.595 TPU: +l-0.595 QC1203626107 405235001 MS Carbon-14 55.9 HUh -0.321 H 56.3 pCi/g 101 (75%-125%) AJ;:A 0912211618:50 Page 373 of 5809 GEL LABO RA TORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC SummarI Workorder: 0405235 Page 37 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1598078 Uncert: +l-0.636 +l-2.80 TPU: +l-0.636 +l-4.98 Batch 1598080 QC1203626127 405235021 DUP Carbon-14 HUh 0.211 HU -0.163 pCilg 0 NIA TXJI 09124/1610:48 Uncert: +l-0.697 +l-0.649 TPU: +l-0.698 +l-0.649 QC1203626129 LCS Carbon-14 61.0 62.l pCi/g 102 (75%-125%) TXJI 0912411613:11 Uncert: +l-1.46 TPU: +l-4.76 QC1203626126 MB Carbon-14 u 0.300 pCilg TXJI 0912411609:3 7 Uncert: +l-0.588 TPU: +l-0.588 QC1203626128 405235021 MS Carbon-14 70.5 HUh 0.211 H 71.3 pCi/g 101 (75%-125%) TXJI 09124/1611:59 Uncert: +l-0.697 +l-1.68 TPU: +l-0.698 +l-5.48 Batch 1598081 QC12036261 IO 405235041 DUP Carbon-14 HUh -0.0252 HU 0.194 pCi/g 0 NIA TXJI 0912711618:52 Uncert: +l-0.675 +l-0.672 TPU: +l-0.675 +l-0.672 QC1203626112 LCS Carbon-14 59.9 59.2 pCi/g 98.9 (75%-125%) TXJI 09/2711621:15 Uncert: +l-1.36 TPU: +l-4.53 QC1203626109 MB Carbon-14 u -0.233 pCilg TXJI 0912711617:40 Uncert: +l-0.594 TPU: +l-0.594 QC12036261 I I 405235041 MS Carbon-14 61.8 HUh -0.0252 H 59.8 pCilg 96.7 (75%-125%) TXJI 0912711620:03 Uncert: +l-0.675 +l-1.39 TPU: +l-0.675 +l-4.58 Batch 1598082 QC1203626114 405235061 DUP Carbon-14 HUh -0.0115 H 0.915 pCilg 0 NIA TXJI 0913011600:17 Uncert: +l-0.738 +l-0.715 TPU: +l-0.738 +l-0.718 QCl203626116 LCS Carbon-14 61.4 62.3 pCilg 101 (75%-125%) TXJI 0913011602:40 Uncert: +l-1.48 TPU: +l-4.78 Page 374 of 5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summar:y Workorder: 405235 Page 38 of 39 Parmname NOM Qual QC Units RPD% REC% Range Anlst Date Time Rad Liquid Scintillation Batch 1598082 QC1203626113 MB Carbon-14 u 0.310 pCilg TXJl 0912911623:06 Uncert: +l-0.626 TPU: +l-0.627 QC1203626115 405235061 MS Carbon-14 70.2 HUh -0.0115 H 68.7 pCilg 97.9 (75%-125%) TXJl 0913011601:29 Uncert: +l-0.738 +l-1.66 TPU: +l-0.738 +l-5.29 Batch 1598092 QC1203626145 405235041 DUP Tritium HUh 1.40 HU 0.374 pCilg 0 NIA TXP3 0912511613:44 Uncert: +l-2.36 +l-2.31 TPU: +l-2.36 +l-2.31 QC1203626147 LCS Tritium 37.7 32.8 pCi/g 87 (75%-125%) TXP3 0912511617: 12 Uncert: +l-3.03 TPU: +l-3.07 QC1203626144 MB Tritium u 0.339 pCilg TXP3 0912511612:01 Uncert: +l-2.16 TPU: +l-2.16 QC1203626146 405235041 MS Tritium 41.4 HUh 1.40 H 35.4 pCilg 85.4 (75%-125%) TXP3 0912511615:28 Un cert: +l-2.36 +l-3.36 TPU: +l-2.36 +l-3.41 Batch 1598096 QC1203626153 405235061 DUP Tritium HUh 0.635 HU 1.55 pCilg 0 NIA TXP3 09/2711620:28 Uncert: +l-2.11 +l-2.14 TPU: +l-2.11 +l-2.14 QC1203626155 LCS Tritium 36.9 36.2 pCi/g 98.2 (75%-125%) TXP3 0912911608:14 Uncert: +l-6.79 TPU: +l-6.82 QC1203626152 MB Tritium u 0.402 pCilg TXP3 0912711618:54 Uncert: +l-1.82 TPU: +l-1.82 QC1203626154 405235061 MS Tritium 42.4 HUh 0.635 H 35.0 pCi/g 82.5 (75%-125%) TXP3 0912711621:59' Uncert: +l-2.11 +l-7.00 TPU: +/-2.11 +l-7.03 Notes: TPU and Counting Uncertainty are calculated at the 95% confidence level (1.96-sigma). The Qualifiers in this report are defined as follows: Page 375of5809 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 405235 Parmname NOM Sample Qua! QC Units RPD% REC% ** Analyte is a Tracer compound < > BD FA H J K L M M NIA NI ND NJ Q Result is less than value reported Result is greater than value reported Results are either below the MDC or tracer recovery is low Failed analysis. Analytical holding time was exceeded Value is estimated Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD REMP Result> MDC/CL and< RDL RPD or %Recovery limits do not apply. See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the Le. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Page 39 of 39 Range Anlst R u UI UJ UL x y Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Other specific qualifiers were required to properly define the results. Consult case narrative. A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. ** Indicates analyte is a surrogate/tracer compound. A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+!-the RL is used to evaluate the DUP result. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 376 of 5809 Page 377of5809 Alpha. Spectroscopy Raw Data Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 19-Sep-2016 Batch#-+-1 Product: __ \.,\ _____ _ Criteria: Yes No Comments Sam Die Solids are less than or eauat to 100 mci for GAB. Ll b-Samples have been blank corrected (If required). ill-Blank correction reoorted Included (If renulred). [f activity less than lOx MDA/MDC, error Is less than or eaual to 150% of sample activity. [f greater than 10* MDA/ MDC, error Is 40% or less. /' [f S.ftlnu* *S.n .. nA I Mnl"'. erro* I<: Instrument source check Is within limits. Inctrument bkn ,.heck Is within llmlts. ../ Method RDL/ LLD has been met. ./ If duollcate activities are: /' Less than 5* MDA/ MDC, then RPD Is 100% or less, [f greater 5* MDA/ MDC, then RPD 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reaulred RER acceotance criteria. Tracer vleld Is 15-125%
carrier yield 25*1250/o. / {Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. ./ Tf < 50/o nf ln..,nr* :.r*l .. l>v\ Samole was run within hold time. v Samele was correctlv oreserved If reauired. tJld-Smears Taken for Radioactive batches. f\X;. Method Spike and LCS are within 75*125% (or m ..... ., the rll<>nt's cont*"<+ acc<>nt,.nce crlt .. rla \. ../" No blank spaces on data forms. / Ali line outs Initialed and dated. INn -----,. ... ,.. Aux data is correct. Client Soeclal reauirements oane has been checked. ./ Raw Data and I or soectrum are included and oroaerlv statused. / MS. LCS. and Duolicate RPD/RER values uploaded to UMS and / u"I""" VArlf;.,rl l-41t *-(If l}>,....-. A"trh Antnrn-' lntn r'"rn " .,,, ..... Batch Data Exceotion Reoorts <DER\ comnleted If anollcable. ,/' j)"@j Batch Data Exception Reports (DER) second reviewed. v Disaositlon verified to be comnleted. Ali"""t 1"'.nrrertion rnmoleted If n>nulred .o-Jd--Review sample historical results If available / (If REMP, results above MDC have been verified bv historical results. recount or re-analvsls.\ Primary Review Performed By: __ ____ _ Secondary Review Performed By:___ 09/30/16 @ 'bf-5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER ' ' DATA EXCEPTION REPORi ' Mo.Day Yr. Division: Quality Criteria: 20-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER HASL-300, U-02-RC Solid Batch ID:
Sample Numbers: 1596418 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements -DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075,405235076,405235077,405235078, and 1203621761were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 20-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 379 of 5809 DER Report No.: 1559386 Revision No.: 1 Type: Process Client Code: MJWC Uranium Que Sheet 07-SEP-16 Batch#: 1596418 Analyst: KXB2 First Client Due Date:04-0CT-16 Internal Due Date:30-SEP-16 Tracer LCS Isotope: U-238 Tracer Code: \C{lO '* l5utl-l"xpiration Date: \\'1-'!>-\U LCS Code: I LPOO-G-Expiration Date: J * \"2..-1] Spike Isotope: U-238 Spike Code:_______ Expiration Date: ____ _ Prep Date: q \C::> -U., Initials: Pipet ID: \<01.\00L.=t:. Balance ID: Hazard Sample ID Client Description Type Code MinCRDL Matrix -----405235061-1 5.lB.R.2.2 SAMPLE 1 pCi/g SOIL 405235062-1 5.2A.R.1.2 SAMPLE 1 pCi/g SOIL 405235063-1 5.2A.R.1.3 SAMPLE 1 pCi/g SOIL 405235064-1 5.2AJU.4 SAMPLE 1 pCi/g SOIL 405235065-1 5.2A.R.2.3 SAl\iPLE 1 pCi/g SOIL 405235066-1 5.2A.R.2.4 SAMPLE 1 pCi/g SOIL 405235067-1 5.2A.R.6.2 SAMPLE 1 pCi/g SOIL 405235068-1 5.2A.R.4.2 SAMPLE 1 pCi/g SOIL 405235069-1 5.2B.R.I.4 SAMPLE 1 pCi/g SOIL 405235070-1 5.2B.R.3.2 SAl\iPLE 1 pCi/g SOIL 405235071-1 5.2B.R.4.2 SAMPLE 1 pCi/g SOIL 405235072-1 5.2B.R.2.4 SAMPLE 1 pCi/g SOIL 405235073-1 5.2B.R.8.2 SAMPLE 1 pCilg SOIL 405235074-1 5.3A.R.1.3 SAMPLE 1 pCi/g SOIL 405235075-1 5.4A.R.1.3 SAMPLE 1 pCi/g SOIL 405235076-1 5.4A.R.4.2 SAl\iPLE 1 pCi/g SOIL 405235077-1 5.SA.R.1.3 SAIVIPLE 1 pCi/g SOIL 405235078-1 5.6A.R.1.3 SAMPLE 1 pCi/g SOIL 1203621760-1 MB for batch 1596418 MB 1 pCi/g SOIL 1203621761-1 5.1B.R.2.2(405235061DUP) DUP l pCi/g SOIL 1203621762-1 LCS for batch 1596418 LCS 1 pCi/g SOIL Choose SOP GEL Laboratories LLC, Radiochemistry Divisio11 Vol: -Client MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl l\'UWCOOl MJWCOOl l\UWCOOl l\UWCOOl l\>UWCOOl MJWCOOl MJWCOOl MJWCOOl l\>UWCOOl MJWCOOI MJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Analyzed Sequentially with Pu Analyzed Sequentially with: Pu-236 ID: Pu: \C:Plu=t 2-\ Vol.: Am: \CAU'-\ \C\ ... --/ :/1¥/ Collection Date 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-lS 14-DEC-lS 14-DEC-15 11-DEC-15 ll-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 ll-DEC-15 15-DEC-15 16-DEC-15 11-DEC-15 --17-DEC-15 17-DEC-15 14-DEC-15 Pos. 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 Weti@ Label Aliquot # ti:Jllf) Det# u Data Reviewed °IJ1 qj1i.-Page 1 of 1 0 H') Vi 00 0 \0 Uranium Que Sheet Batch #: 1596418 Analyst: KXB2 First Client Due Date:04-0CT-16 Internal Due Date:30-SEP-16 f / \ -\2-1 M-sEP-16 Tracer Isotope: U-232.@ Tracer Code: \'?\0*.E, Expiration Date: Vol:__Q,__l_ Analyzed Sequentially with Pu Analyzed Sequentially with: LCS Isotope: U-238 LCS Code: ______ _ Expiration Date:. ____ _ Vol:_::_ Vol: -Pu-236 ID: ,_ Pu: __ _ Spike Isotope: U-238 Spike Code:_______ Expiration Date:. ____ _ Prep Date: q * \CQ \ \.1 Initials: ¥b Pipet ID: \92\.:\ 001.a:. Balance ID: Sample ID 405235061-1 405235062-1 405235063-1 405235064-1 405235065-1 405235066-1 405235067-1 405235068-1 405235069-1 405235070-1 405235071-1 405235072-1 405235073-1 405235074-1 405235075-1 405235076-1 405235077-1 405235078-1 1203621760-1 1203621761-1 1203621762-1 Client Description 5.lB.R.2.2 5.2A.R.1.2 5.2A.R.1.3 5.2A.R.1.4 5.2A.R.2.3 5.2A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2B.R.l.4 5.2B.R.3.2 5.2B.R.4.2 5.2B.R.2.4 5.2B.R.8.2 5.3A.R.1.3 5.4A.R.l.3 5.4A.R.4.2 5.SA.R.1.3 5.6A.R.1.3 rvm for batch 1596418 5.1B.R.2.2(405235061DUPJ LCS for batch 1596418 Choose SOP Type SAMPLE SAMPLE SA..1\fl>LE SAMPLE SAMPLE SAl'vlPLE SAl\-IPLE SAMPLE SAMPLE SAl\-fPLE SAMPLE SAl\-IPLE SAMPLE SAMPLE SAIVIPLE SAMPLE SA?vIPLE SAMPLE MB DUP LCS GE,L Laboratories LLC, Radiochemistry Division Hazard Code MinCRDL 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g lpCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g lpCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Client MJWCOOl MJWCOOl MJWCOOl !HJWCOOl MJWCOOl 1\-UWCOOl 1\-UWCOOl MJWCOOl MJWCOO! lVUWCOOl lVUWCOOl MJWCOOl MJWCOOl 1\-UWCOOl l\fJWCOOl lVUWCOOl IVUWCOOl l'vUWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Solid Sample Dissolution by: LEA CH Circle One Vol.: ___ _ Collection Date 14-DEC-15 14-DEC-15 l4-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 11-DEC-15 11-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 11-DEC-15 15-DEC-15 16-DEC-15 11-DEC-15 17-DEC-15 17-DEC-15 14-DEC-15 Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 '---* _,_,_lf6,__* _,_,;o=-. S[;i... I <3+-J ! 11'.l '.D.bt] Ii j olO I ,. 1 l 'to , !I .:7 I 1_, I '"7 _ I '-"-11 i.J i N"""_j Page 1 of 1 BATCH NUMBER : 1596418 SAMPLE ID : T0405235067 _uu SAMPLE QTY : 0.508 G +/-0.197 "lo GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 122 DETECTOR S/N : 75546 AVERAGE %EFFICIENCY : 25.9617 AVERAGE %EFF ERROR : 0.5030 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B122.CNF;1170 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED "lo YIELD : 83.4 +/-8.115 "lo COUNT DATE : 17-Sep-2016 11 :44:56 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W122.CNF;334 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.504 G +/-0.198 "lo TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0744E+01 dpm --r----* TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 667.45 0.04 PEAKNET2 0.32 289.48 RECOVERY YIELD CORR. NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 71 ,--U*238:3974.,.284 keV I U*235: 431o-4581 keV 64 L lJ.3'4: 4592-4865 keV I U-232: sooo-sssa keV 57 ! 50 r-43 36L 5 29 0 I 151 i 8r PEAK ENERGY 5251.42 4783.25 4494.61 4190.49 1 2382 2781 3183 3589 3 Energy (keV) PEAK FWHM 4.959 27.272 34.400 78.098 j i I ... uH, 1 i I 099 M13 11.1230 dpm 4494.61 4490.61 4.6535 dpm 5251.42 5340.45 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 1.000 0.040 0.960 0.9798 100.000 43.000 39.400 3.600 1.8974 100.000 2.000 0.320 1.680 1.2961 99.700 51.000 49.560 1.440 1.2000 100.000 . 11, . i ' i I I i 48. 0 5251 5676 6105 6537 6974 ACTIVITY pCi/G 6.00E-04 5.62E-01 4.58E-03 7.07E-01 I 741 4 96.307 NIA 84.111 1.0079 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.46E-02 9.89E-02 2.69E-02 4.45E-02 2.09E-01 1.42E-01 4.95E-02 1.87E-01 5.22E-02 1.11 E-01 3.40E-02 5.21 E-02 2.33E-01 1.05E-01 3.13E-02 2.02E-01 NOTES:

Results are a compilation of 80405235067 _UU and T0405235067 _UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000) DO NOT REPORT GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-011 ...... CHAMBER . : . 011 *** LIB FILE : U236 BATCH NUMBER : 1596418 SAMPLE ID : S0405235067 UU SAMPLE QTY : 0.508 G -+/-0.197 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 84.1 +/-6.731 % TRACER ID : 1564-1 NUCLIDE : U-232 NOMINAL : 4.6535E+OO dpm RESULTS : 3.9142E+OO dpm DETECTOR S/N : 72531 BKG FILE : B011.CNF;1833 AVERAGE %EFFICIENCY : 31.0555 BKG DATE : 16-Sep-2016 AVERAGE %EFF ERROR : 0.5992 BKG LIVE TIME(SEC) : 59999.99 COUNT DATE : 17-Sep-201611:42:40 EFF FILE : W011.CNF;511 ELAPSED LIVETIME{SEC) : 14400.00 CAL DATE : 27-Aug-2016 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM U-232 5302.10 5340.45 36.661 U-3/4 4763.02 4787.66 52.176 U-235 4391.00 4490.61 129.198 U-238 4184.73 4203.59 62.943 34 31 28 lJ.238* 3974-4284 keV l U-235:4310-4581 keV L.. U-314: 4592...is55 keV L U-232: 5000-5398 keV i 25 22 r r-i en 19 I-16 z :) 13 0 £ 10 .::-7 *;; 4 <i:: 1 ' r I t L 1-' f-I ' i I I l I I , I i 23 88 2788 3192 3601 4 i430 Energy {keV) AREA AREA AREA St Dev pCi/G 295.000 289.480 5.520 2.3495 100.000 4.13E+OO 43.000 39.400 3.600 1.8974 100.000 5.57E-01 2.000 0.320 1.680 1.2961 99.700 4.54E-03 51.000 49.560 1.440 1.2000 100.000 7.01E-01 485 2 527, 5707 6141 6580 7023 7470 pCi/G pCi/G pCi/G 7.44E-01 1.65E-01 6.13E-02 2.01E-01 1.41 E-01 4.92E-02 5.18E-02 1.10E-01 3.37E-02 2.23E-01 1.05E-01 3.11E-02 pCi/G 4.82E-01 1.86E-01 5.17E-02 2.01E-01 BATCHNUMBEF! : 1596418 SAMPLE ID : T0405235070_UU SAMPLE QTY : 0.509 G +/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 127 DETECTOR SIN : 78770 AVERAGE %EFFICIENCY : 26.6218 AVERAGE %EFF ERROR : 0.5155 Instrument SOP: GL-RAD-1-009 Analytical SOP: LIB FILE : U236 BKG FILE : B127.CNF;1165 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 88.0 +/-7.889 % COUNT DATE : 17-Sep-201611:45:04 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W127.CNF;322 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.510 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0422E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 663.86 -1.44 PEAKNET2 1.04 321.20 RECOVERY YIELD CORR. 11.1230dpm 4486.14 4545.16 4.6535 dpm 5198.55 5334.16 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5198.55 0.000 0.000 -1.440 1.440 1.2000 100.000 U-3/4 4763.02 4764.95 59.086 48.000 47.280 0.720 0.8485 100.000 U-235 4391.00 4486.14 59.322 2.000 1.040 0.960 0.9798 99.700 U-238 4184.73 4202.83 14.521 64.000 63.040 0.960 0.9798 100.000 ------61 ,-U-238: 3974-4284 keV j U-235: 431Q..4581 keV j U-314: 4592-4865 keV 55 r-U*232: 5000*5398 keV 49 43 37 $ i I-31 z I 6 25r £ 19 13 f--I t5 7 f--<C 1 ,.__; ,--', ,-"-i ,.-4'--,"'-, ,--', _.;--, .,-,---,u-,...t 2382 2781 3183 3590 4 00 Energy (keV) l .. i 414 48 :, -,-I I I 3 5255 5681 6111 6545 6982 :, ACTIVITY pCi/G -2.15E-02 6.06E-01 1.34E-02 8.08E-01 7424 1.96-sigma TPU pCi/G 3.47E-02 2.01E-01 4.58E-02 2.40E-01 NOTES: MDA pCi/G 1.10E-01 7.83E-02 8.47E-02 8.45E-02 93.413 NIA 88.668 1.0078 Le pCi/G 3.28E-02 1.99E-02 2.31E-02 2.30E-02 1.96-sigma cnt Unc pCi/G 3.46E-02 1.76E-01 4.57E-02 2.03E-01
Results are a compilation of S0405235070_UU and T0405235070_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

AIJ>ho Spectroscopy Software VO!Slon 3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596418 ..... SAMPLE JD : S0405235070_UU GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-011 CHAMBER: 014

DETECTOR SIN : 83289 BKG FILE : 8014.CNF;l814 SAMPLE QTY : 0.509 G +/-0.196 % AVERAGE %EFFICIENCY : 32.6875 I BKG DATE : 16-Sep-2016 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 88.7 +/-6.451 % TRACER ID : 1564-1 NUCLIDE : U-232 NOMINAL : 4.6535E+OO dpm RESULTS : 4.1262E+OO dpm NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 r u.ias: 3974-1284 keV 41 r-U*235: 4310-4581 keV I lJ.314: 4592-4885 keV 37 t-U-232: 5000-5398 keV 33 29 j 25 [-0' 21 Z I :::> 17 o I 13/ I 1 PEAK ENERGY 5334.16 4772.03 4545.16 4218.40 ' ' 2378 2773 3173 3578 Energy (keV) PEAK FWHM 18.176 67.576 9.829 30.716 AVERAGE %EFF ERROR : 0.6302 I BKG LIVE TIME(SEC) : 59999.99 COUNT DATE : 17-Sep-2016 11:42:41 ! EFF FILE : W014.CNF;523 ELAPSED LIVE TIME(SEC) : 14399.99 I CAL DATE : 27-Aug-2016 I NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Uno AREA AREA AREA St Dev pCi/G pCi/G pCi/G pCi/G pCi/G 326.000 321.200 4.800 2.1909 100.000 4.12E+OO 7.09E-01 1.41 E-01 5.15E-02 4.55E-01 48.000 47.280 o.720 0.8485 100.000 6.02E-01 1.92E-01 7.77E-02 1.98E-02 1.75E-01 2.000 1.040 0.960 0.9798 99.700 1.33E-02 4.54E-02 8.41E-02 2.29E-02 4.54E-02 64.000 63.040 0.960 0.9798 100.000 8.02E-01 2.28E-01 8.38E-02 2.28E-02 2.01E-01 DO NbiREPORT --, NOT REPORT I ' ' I !j \i I . , I 5672 6104 6542 6983 7430 BATCH NUMBER : 1596418 SAMPLE ID : T0405235072 UU SAMPLE QTY : 0.513 G -+/-0.195 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 129 DETECTOR S/N : 76227 AVERAGE %EFFICIENCY : 26.3145 AVERAGE %EFF ERROR : 0.5097 Instrument SOP: GL-RAD-1-009 ....... AnaJytical SOP: GL-R_f\D-A:011. LIB FILE : U236 BKG FILE : B129.CNF;1168 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED 0io YIELD : 71.4 +/-8.366 % COUNT DATE : 17-Sep-201611:45:08 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W129.CNF;343 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.7493E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 _ U-23B: 3974-4284 keV 64 f-U-235: 4310-4581 keV I U-3'4: 4592-4805 keV 57 f-U-232: 5000-5398 keV 50 43 i & 36 J-* t-I § 29 o 22 ! 15 ;-8 L I I 3177 2379 2776 Energy (keV) ID 1570-E 1564-1 PEAK ENERGY 5321.84 4774.35 4489.30 4204.51 I 3582 3f NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 613.87 0.52 PEAKNET2 7.04 266.96 RECOVERY YIELD CORR. PEAK FWHM 4.932 26.715 51.608 62.267 i I I I I I ' ff 1& 11 I I 'lk. I * )!. I 91 404 11.1230 dpm 4489.30 4451.07 4.6530 dpm 5321.84 5332.80 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 1.000 0.520 0.480 0.6928 100.000 66.000 62.160 3.840 1.9596 100.000 8.000 7.040 0.960 0.9798 99.700 48.000 47.040 0.960 0.9798 100.000 . J I ACTIVITY pCi/G 8.50E-03 9.53E-01 1.08E-01 7.21E-01 87.387 NIA 72.083 1.0098 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.73E-02 9.06E-02 2.08E-02 4.72E-02 2.95E-01 1.56E-01 5.51E-02 2.48E-01 9.37E-02 1.01E-01 2.76E-02 9.19E-02 2.43E-01 1.01 E-01 2.75E-02 2.11 E-01 NOTES: *Results are a compilation of S0405235072_UU and T0405235072_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000) 5242 5668 6097 6531 6969 7411 Alpha Spectros.c::opy Software Version 3.5.3 effccti\.'e date: 02*P..'lar*2015 BATCH NUMBER : 1596418 SAMPLE ID : S0405235072_UU SAMPLE QTY : 0.513 G +/-0.195 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 016 DETECTOR S/N : 78774 A VERA GE %EFFICIENCY : 33.4185 AVERAGE %EFF ERROR : 0.6439 Instrument SOP: GL-RAD-1-009 Analytical.SOP: .. ' i LIB FILE : U236 I BKG FILE : B016.CNF;1809 !I BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 72.1 +/-6.949 % COUNT DATE : 17-Sep-2016 11 :42:41 ELAPSED LIVE TIME(SEC) : 14399.99 ! EFF FILE : W016.CNF;494 CAL DATE : 27-Aug-2016 TRACER ID : 1564-1 NUCLIDE : U-232 NOMINAL : 4.6530E+OO dpm RES UL TS : 3.3540E+OO dpm NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 _ U-238: 3974-4284 keV 23 j_ U-235:-1310-4581 keV I U-314: 4592-48BS keV 21 l U-232: 5000-5398 keV 19 !-17 ! 15 !--z 11 f-PEAK ENERGY 5332.80 4783.92 4451.07 4215.06 PEAK GROSS FWHM AREA 46.059 272.000 11.531 66.000 19.581 8.000 30.024 48.000 B 9 f-I 5 Ii I u 3 L !1i1 <( 1 --2399 2793 3192 3596 Energy (keV) 4( 04 48' 5 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G 266.960 5.040 2.2450 100.000 4.09E+OO 7.62E-01 1.72E-01 6.29E-02 4.97E-01 62.160 3.840 1.9596 100.000 9.44E-01 2.79E-01 1.55E-01 5.45E-02 2.45E-01 7.040 0.960 0.9798 99.700 1.07E-01 9.23E-02 1.00E-01 2.73E-02 9.10E-02 47.040 0.960 0.9798 100.000 7.14E-01 2.32E-01 1.00E-01 2.73E-02 2.09E-01 . ! . I
I ' I , 5685 6118 6555 6997 7443 BATCH NUMBER : 1596418 SAMPLE ID : T0405235077 UU SAMPLE QTY : 0.510 G -+/-0.196 % SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 92.2 +/-7.848 % SECONDARY QTY : 0.510 G +/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 134 DETECTOR S/N : 76230 AVERAGE %EFFICIENCY : 25.7389 AVERAGE %EFF ERROR : 0.4988 COUNT DATE : 17-Sep-201611:45:20 ELAPSED LIVE TIME(SEC) : 14400.00 --7---*---TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.2687E+OO dpm Instrument SOP: GL-RAD-1-009 Analytical SOP: LIB FILE : U236 BKG FILE : 8134.CNF;1149 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W134.CNF;336 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 ID 1570-E 1564-1 PEAK ENERGY 5198.58 4765.90 4490.69 4204.31 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 570.84 -0.48 PEAKNET2 -0.48 354.92 PEAK FWHM 0.000 66.549 41.660 53.735 11.1230 dpm 4490.69 4445.41 4.6528 dpm 5198.58 5336.26
NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -8.32E-03 65.000 63.560 1.440 1.2000 100.000 7.36E-01 0.000 -0.480 0.480 0.6928 99.700 -5.57E-03 62.000 61.520 0.480 0.6928 100.000 7.12E-01 1.96-sigma TPU pCi/G 3.69E-02 2.19E-01 2.47E-02 2.13E-01 MDA pCi/G 9.60E-02 8.56E-02 6.43E-02 6.41E-02 RECOVERY YIELD CORR. 83.080 N/A 92.894 1.0076 Le pCi/G 2.20E-02 2.55E-02 1.47E-02 1.47E-02 1.96-sigma cnt Unc pCi/G 3.68E-02 1.85E-01 2.47E-02 1.80E-01 U-238: 3974-4284 keV 46 U-235: "310-45!!1 keV I U-314: 45S2-4865 keV 41 L U-232: 5000-5398 keV ! 36 ! 31 f-l en 26 i-1-I z 21 r-:;) I 0 16 f-I 11 t; el-<( I 1 -. >_I -, -, --'-:I-, _,,, § I: I ' ' ! ... ! j ' ** ' l .... J 2387. 2786 3188 3594 4 04 417 48 4 5255 5679 6107 6539 6974 7413 Energy (keV) NOTES:
Results are a compilation of 80405235077 _UU and T0405235077 _UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 {0.009 +/-0.000) DO 'NOT REPORT Ai<>ha_ Spectroscopy Softwnte Ve:slon 3.5.3
etfectve dale: 02*Mar*2015 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596418 SAMPLE ID : S0405235077 UU SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 024 DETECTOR S/N : 76542 AVERAGE %EFFICIENCY : 34.4760 AVERAGE %EFF ERROR : 0.6639 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.9 +/-6.201 % TRACER ID : 1564-1 NUCLIDE : U-232 NOMINAL : 4.6528E+OO dpm RES UL TS : 4.3221 E+OO dpm COUNT DATE : 17-Sep-2016 11 :42:42 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 ...-U*238: 3974-4284 keV j U*235: "310-4581 keV 25 r IJ.314: 4592-4865 keV I U*232: 5000-5398 keV 22 i 19 r-1 16 l-0' 13 L I 7 r-1 PEAK ENERGY 5336.26 4786.44 4445.41 4226.59 :,..... 2399 2793 Energy (keV) PEAK GROSS FWHM AREA 80.219 359.000 83.477 65.000 0.000 0.000 42.814 62.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 354.920 4.080 2.0199 100.000 4.11E+OO 63.560 1.440 1.2000 100.000 7.30E-01 -0.480 0.480 0.6928 99.700 -5.53E-03 61.520 0.480 0.6928 100.000 7.07E-01 ii! I I! l i .. I . ! ' 5680 6111 6548 6989 7435 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B024.CNF;1824 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W024.CNF;517
CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.78E-01 1.20E-01 4.28E-02 2.06E-01 8.50E-02 2.53E-02 2.45E-02 6.38E-02 1.46E-02 2.00E-01 6.36E-02 1.46E-02 1.96-sigma cnt Unc pCi/G 4.31E-01 1.84E-01 2.45E-02 1.79E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235061_UU SAMPLE QTY : 0.514 G +/-0.195 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 79.6 +/-8.702 % SECONDARY QTY : 0.511 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 7.1485E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 116 DETECTOR S/N : 80004 AVERAGE %EFFICIENCY : 25.8624 AVERAGE %EFF ERROR : 0.5011 COUNTDATE: 17-Sep-201611:44:41 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B116.CNF;1159 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W116.CNF;295 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4493.71 4428.18 4.6532 dpm 5351.04 5338.87 PEAK NET 1 442.37 1.04 PEAKNET2 2.00 266.52 RECOVERY YIELD CORR. 64.075 NIA 80.712 1.0134 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5351.04 14.817 2.000 U-3/4 4763.02 4777.62 34.574 38.000 U-235 4391.00 4493.71 32.475 2.000 U-238 4184.73 4194.40 30.869 52.000 46 U.238*3974-4284keV U-235:4310-4581 keV U-3/4:4592-4565keV 41 U-232:5000-5398keV 36 31 (jJ 26 I-z 21 :J 0 16 S?.. 11 *;; n 6 <( " ..... J_ I I I I 23 81 2778 3179 3584 3rn3 48:4 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN AREA AREA StDev 1.040 0.960 0.9798 100.000 38.000 0.000 0.0000 100.000 2.000 0.000 0.0000 99.700 52.000 0.000 0.0000 100.000 I I I I I I 5245 5670 6100 6533 6970 -ACTIVITY pCi/G 2.32E-02 5.85E-01 3.09E-02 8.00E-01 I 7411 1.96-sigma TPU pCi/G 7.95E-02 2.14E-01 5.32E-02 2.60E-01 NOTES: MDA pCi/G 1.47E-01 4.62E-02 4.63E-02 4.62E-02 Le pCi/G 4.01E-02 O.OOE+OO O.OOE+OO O.OOE+OO 1.96-sigma cnt Unc pCi/G 7.94E-02 1.88E-01 5.29E-02 2.20E-01 *Results are a compilation of S0405235061_UU and T0405235061_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.007 +/-0.000) 0 ....., V\ 00 0 '° BATCH NUMBER : 1596418 SAMPLE ID : S0405235061_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 001 DETECTOR S/N : 79451 AVERAGE %EFFICIENCY : 29.7966 AVERAGE %EFF ERROR : 0.5755 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 80.7 +/-6.897 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6532E+OO dpm 3.7556E+OO dpm NUCLIDE LIBRARY PEAK '(j) I-z ::l 0 *:;; u <i: ENERGY ENERGY U-232 5302.10 5338.87 U-3/4 4763.02 4788.47 U-235 4391.00 4428.18 U-238 4184.73 4226.11 U-238: 3974-4284 keV 31 U-235: 43104581 keV U-314:4592-4865keV 28 U-232:5000-5398keV 25 22 19 16 13 10 7 4 2371 2771 3175 3583 Energy (keV) PEAK FWHM 31.548 28.019 9.962 24.906 COUNT DATE : 17-Sep-2016 11 :42:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 267.000 266.520 0.480 0.6928 100.000 4.08E+OO 38.000 38.000 0.000 0.0000 100.000 5.77E-01 2.000 2.000 0.000 0.0000 99.700 3.05E-02 52.000 52.000 0.000 0.0000 100.000 7.90E-01 6108 6542 6979 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B001.CNF;1858 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W001.CNF;565 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.54E-01 8.47E-02 1.94E-02 2.03E-01 4.56E-02 O.OOE+OO 5.24E-02 4.57E-02 O.OOE+OO 2.43E-01 4.56E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.91E-01 1.86E-01 5.22E-02 2.17E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235062 UU SAMPLE QTY : 0.515 G -+/-0.194 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 63.8 +/-9.083 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0132E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 117 DETECTOR S/N : 80003 AVERAGE %EFFICIENCY : 25.8068 AVERAGE %EFF ERROR : 0:5001 COUNT DATE: 17-Sep-201611:44:44 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B117.CNF;1162 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W117.CNF;308 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4492.84 4446.11 4.6532 dpm 5252.28 5333.07 PEAK NET 1 625.67 2.04 PEAKNET2 2.76 196.76 RECOVERY YIELD CORR. 90.819 N/A 64.781 1.0157 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5252.28 103.522 3.000 U-3/4 4763.02 4775.28 31.632 32.000 U-235 4391.00 4492.84 62.961 3.000 U-238 4184.73 4202.98 28.961 46.000 55 U*238:3974-4264keV U-235:431D-4581 keV U-3/4:4592-4865keV 49 lJ..232:5000.5398keV 43 37 en 31 I-z 25 ::i 0 19 8 .?;-13 *:;; ti 7 <l'. 1 2390 2787 3187 3592 4 00 Energy (keV) l/ NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G 2.040 0.960 0.9798 100.000 3.27E-02 31.040 0.960 0.9798 100.000 6.47E-01 2.760 0.240 0.4899 99.700 5.77E-02 45.760 0.240 0.4899 100.000 9.54E-01 5673 6101 6533 6970 7410 1.96-sigma TPU pCi/G 6.54E-02 2.64E-01 8.38E-02 3.30E-01
NOTES: MDA pCi/G 1.06E-01 1.37E-01 1.00E-01 1.00E-01 Le pCi/G 2.88E-02 3.74E-02 1.88E-02 1.87E-02 1.96-sigma en! Unc pCi/G 6.51E-02 2.36E,01 8.31E-02 2.81E-01.
Results are a compilation of S0405235062_UU and T0405235062_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235062 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 002 DETECTOR S/N : 79452 SAMPLE QTY : 0.515 G -+/-0.194 % AVERAGE %EFFICIENCY : 27.4069 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 64.8 +/-7.811 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE U-232 U-3/4 U-235 U-238 1564-1 U-232 4.6532E+OO dpm 3.0144E+OO dpm LIBRARY PEAK ENERGY ENERGY 5302.10 5333.07 4763.02 4776.86 4391.00 4446.11 4184.73 4219.51 PEAK' FWHM 62.129 51.709 190.157 34.278 AVERAGE %EFF ERROR : 0.5303 COUNTDATE: 17-Sep-201611:42:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 197.000 196.760 0.240 0.4899 100.000 4.07E+OO 32.000 31.040 0.960 0.9798 100.000 6.37E-01 3.000 2.760 0.240 0.4899 99.700 5.68E-02 46.000 45.760 0.240 0.4899 100.000 9.39E-01 8 U-238:3974-4284keV 25 U-235:431G-4581 keV U-Jf4:4S92-4a65keV U-232:5000-5398keV 22 19 16 en 13 I-z '.::) 10 0 £ 7 *:;; 4 u <( 2358 2760 3166 3576 3 89 406 48 6 5251 5679 6110 6545 6984 7427 Energy (keV) ii Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B002.CNF;1843 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W002.CNF;518 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.59E-01 9.92E-02 1.86E-02 2.53E-01 1.35E-01 3.68E-02 8.23E-02 9.87E-02 1.85E-02 3.13E-01 9.84E-02 1.84E-02 1.96-sigma cnt Unc pCi/G 5.71E-01 2.32E-01 8.19E-02 2.76E-01 '"O (1) ..,, \0 Alpha Spectroscopy Software Version 3.5.3 effective date: 02-Mar-2015 0 ....., BATCH NUMBER : 1596418 SAMPLE ID : T0405235063 UU SAMPLE QTY : 0.518 G -+/-0.193 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 59.7 +/-9.292 % SECONDARY QTY : 0.513 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0325E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 118 DETECTOR S/N : 80061 AVERAGE %EFFICIENCY : 25.6062 AVERAGE %EFF ERROR : 0.4962 COUNT DATE : 17-Sep-201611:44:46 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B118.CNF;1171 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W118.CNF;318 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4488.59 4497.89 4.6532 dpm 5236.31 5331.41 PEAK NET 1 632.60 0.28 PEAK NET 2 1.52 184.32 RECOVERY YIELD CORR. 92.544 N/A 60.208 1.0088 NUCLIDE LIBRARY PEAK Ui I-z ::J 0 *::; u <{ ENERGY ENERGY U-232 5302.10 5236.31 U-3/4 4763.02 4761.02 U-235 4391.00 4488.59 U-238 4184.73 4189.02 lJ.238: 3974-4284 keV 51 U-235:4310-4581 keV U-3/4:4592-4865keV 46 U-232:5000-5398keV 41 36 31 26 21 16 11 6 2384 2782 3183 3589 Energy (keV) PEAK GROSS FWHM AREA 4.952 1.000 53.237 30.000 39.068 2.000 71.808 28.000 !:S

8 :; NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G 0.280 0.720 0.8485 100.000 4.36E-03 28.320 1.680 1.2961 100.000 6.22E-01 1.520 0.480 0.6928 99.700 3.35E-02 27.280 0.720 0.8485 100.000 6.00E-01 5671 6098 6529 6964 7402 1.96-sigma TPU pCi/G 4.56E-02 2.68E-01 7.72E-02 2.58E-01 NOTES: MDA pCi/G 9.50E-02 1.70E-01 1.22E-01 1.34E-01 Le pCi/G 2.42E-02 5.22E-02 2.80E-02 3.42E-02 1.96-sigma en! Une pCi/G 4.55E-02 2.42E-01 7.70E-02 2.33E-01
Results are a compilation of S0405235063_UU and T0405235063_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235063 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 003 DETECTOR S/N : 79453 AVERAGE %EFFICIENCY : 27.6246 AVERAGE %EFF ERROR : 0.5344 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 60.2 +/-8.063 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6532E+OO dpm 2.8015E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5331.41 U-3/4 4763.02 4780.29 U-235 4391.00 4497.89 U-238 4184.73 4205.49 25 U-236: 39744284 keV lJ.235:4310-4581 kaV 23 U-3/4:4592-4865keV U-232:5000-S398keV 21 19 17 15 Ui 13 1--z 11 :J 0 9 s 7 0 "> 5 u 3 <l'. 1 2377 2775 3177 3582 Energy (keV) PEAK FWHM 23.035 39.635 123.861 21.139 3 92 :<l COUNT DATE : 17-Sep-201611:42:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 186.000 184.320 1.680 1.2961 100.000 4.05E+OO 30.000 28.320 1.680 1.2961 100.000 6.17E-01 2.000 1.520 0.480 0.6928 99.700 3.32E-02 28.000 27.280 0.720 0.8485 100.000 5.94E-01 >> ! g m :;l 5665 6093 6524 6959 7398 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B003.CNF;1841 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W003.CNF;535 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.83E-01 1.70E-01 5.21E-02 2.60E-01 1.69E-01 5.17E-02 7.65E-02 1.21E-01 2.77E-02 2.50E-01 1.33E-01 3.39E-02 1.96-sigma cnt Unc pCi/G 5.89E-01 2.39E-01 7.63E-02 2.31E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235064 UU SAMPLE QTY : 0.517 G -+/-0.193 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 56.2 +/-9.663 % SECONDARY QTY : 0.507 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0963E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 119 DETECTOR S/N : 79450 AVERAGE %EFFICIENCY : 23.3886 AVERAGE %EFF ERROR : 0.4544 COUNTDATE: 17-Sep-201611:44:49 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B119.CNF;1176 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W119.CNF;315 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4491.91 4445.46 4.6532 dpm 5291.61 5314.15 PEAK NET 1 613.52 1.60 PEAK NET2 0.00 164:80 RECOVERY YIELD CORR. 98.264 N/A 56.952 1.0142 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5291.61 0.000 4.000 U-3/4 ' 4763.02 4763.46 54.467 29.000 U-235 4391.00 4491.91 54.542 0.000 U-238 4184.73 4205.43 16.092 24.000 U 238* 3974-4284 keV 55 U-235: 4310-4581 keV U-314:4592-4865keV U-23Z:S000-5398keV 49 43 37 -Ci) 31 I-z 25 ::J I 0 19 f2. c 13 *:;; t5 7 <l'. " J J,i ... I I I I 23 87 2785 3187 3592 41 02 415 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN AREA AREA StDev 1.600 2.400 1.5492 100.000 28.280 0.720 0.8485 100.000 0.000 0.000 0.0000 99.700 23.760 0.240 0.4899 100.000 I I I I I 5253 5678 6107 6539 6975 -ACTIVITY pCi/G 2.60E-02 7.00E-01 O.OOE+OO 5.88E-01 I 7415 1.96-sigma TPU pCi/G 7.57E-02 2.99E-01 5.03E-02 2.68E-01 NOTES: MDA pCi/G 1.41E-01 1.51E-01 7.45E-02 1.19E-01 Le pCi/G 4.61E-02 3.85E-02 O.OOE+OO 2.22E-02 1.96-sigma cnt Unc pCi/G 7.55E-02 2.67E-01 5.01E-02 2.43E-01

Results are a compilation of S0405235064 UU and T0405235064_UU. -*The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

AlphaSpectroscopySoftwareVerslonJ.5.3 effedlvedate:02-Mar*2015 BATCH NUMBER : 1596418 SAMPLE ID : S0405235064 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.517 G -+/-0.193 % CHAMBER : 154 DETECTOR S/N : 76224 AVERAGE %EFFICIENCY : 26.1126 AVERAGE %EFF ERROR : 0.5058 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 57.0 +/-8.453 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6532E+OO dpm 2.6501 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5314.15 U-3/4 4763.02 4762.64 U-235 4391.00 4445.46 U-238 4184.73 4197.23 lJ.238:3974-4284keV 23 U-235: 431Q-4581 keV U.3/4:4592-4865keV 21 U-232:500Q..539BkeV 19 17 15 Ui I-13 z 11 ::i 9 0 s 7 1' 5 *:;; t5 3 <i: 1 2372 2768 3169 Energy (keV) PEAK FWHM 25.045 32.091 0.000 25.509 COUNT DATE : 19-Sep-2016 15:47:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 166.000 164.800 1.200 1.0954 100.000 4.05E+OO 29.000 28.280 0.720 0.8485 100.000 6.90E-01 0.000 0.000 0.000 0.0000 99.700 O.OOE+OO 24.000 23.760 0.240 0.4899 100.000 5.80E-01 6081 6513 6948 7387 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B154.CNF;1097 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W154.CNF;304 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.30E-01 1.73E-01 4.94E-02 2.88E-01 1.49E-01 3.79E-02 4.95E-02 7.35E-02 O.OOE+OO 2.59E-01 1.17E-01 2.19E-02 1.96-sigma cnt Unc pCi/G 6.24E-01 2.63E-01 4.94E-02 2.40E-01 '"t:I ro ...,, 3.5.3 0 ...., BATCH NUMBER : 1596418 SAMPLE ID : T0405235065 UU g SAMPLE QTY : 0.507 G -+/-0.197 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 87.5 +/-8.339 % SECONDARY QTY : 0.509 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1062E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 120 DETECTOR S/N : 74430 AVERAGE %EFFICIENCY : 25.0593 AVERAGE %EFF ERROR : 0.4860 COUNTDATE: 17-Sep-201611:44:52 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B120.CNF;1186 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W120.CNF;351 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4490.86 4429.67 4.6532 dpm 5382.69 5335.27 PEAK NET 1 663.30 -1.40 PEAK NET2 6.00 257.28 RECOVERY YIELD CORR. 99.154 N/A 88.195 1.0077 NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5382.69 4.951 U-3/4 4763.02 4768.20 54.462 U-235 4391.00 4490.86 51.923 U-238 4184.73 4200.31 12.378 61 U*238:3974-4284keV U-235:4310-4581 keV lJ..3i'4:4592-485SkeV 55 U*232:5000-S398keV 49 43 37 Ui 31 I-z ::> 25 0 £ 19 13 *:;: :g 7 <I.'. 1 2372 2770 3172 3578 3 88 Energy (keV) NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -1.400 2.400 1.5492 100.000 -2.09E-02 41.000 41.000 0.000 0.0000 100.000 6.59E-01 6.000 6.000 0.000 0.0000 99.700 9.67E-02 42.000 41.280 0.720 0.8485 100.000 6.63E-01 401 48 9 5240 5665 6094 6526 6963 7403 1.96-sigma TPU pCi/G 4.76E-02 2.32E-01 8.55E-02 2.35E-01 NOTES: MDA pCi/G 1.30E-01 4.82E-02 4.84E-02 9.82E-02 Le pCi/G 4.24E-02 O.OOE+OO O.OOE+OO 2.50E-02 1.96-sigma cnt Unc pCi/G 4.76E-02 2.04E-01 8.39E-02 2.07E-01

Results are a compilation of S0405235065_UU and T0405235065_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235065 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 006 DETECTOR S/N : 79455 SAMPLE QTY : 0.507 G -+/-0.197 % AVERAGE %EFFICIENCY : 26.3231 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 88.2 +/-7.000 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6532E+OO dpm 4.1038E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5335.27 U-3/4 4763.02 4786.10 U-235 4391.00 4429.67 U-238 4184.73 4222.09 U-238: 3974-4284 keV 23 U-235: 4310-4581 keV U-3/4:4592-4865keV 21 U-2J2:5000-5398keV 19 17 15 en I-13 z 11 ::::> 9 0 7 .?;-5 *:;: :g 3 <l'. 1 2381 2782 3187 3594 Energy (keV) PEAK FWHM 64.310 53.696 7.492 31.635 4 05 AVERAGE %EFF ERROR : 0.5098 COUNTDATE: 17-Sep-201611:42:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 258.000 257.280 0.720 0.8485 100.000 4.13E+OO 41.000 41.000 0.000 0.0000 100.000 6.54E-01 6.000 6.000 0.000 0.0000 99.700 9.60E-02 42.000 41.280 0.720 0.8485 100.000 6.58E-01 :g m 5681 6107 6537 6971 7407 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B006.CNF;1837 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W006.CNF;571 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.77E-01 9.82E-02 2.50E-02 2.23E-01 4.78E-02 O.OOE+OO 8.44E-02 4.80E-02 O.OOE+OO 2.26E-01 9.74E-02 2.48E-02 1.96-sigma cnt Unc pCi/G 5.07E-01 2.03E-01 8.33E-02 2.05E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235066 UU SAMPLE QTY : 0.509 G -+/-0.196 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 70.3 +/-9.068 % SECONDARY QTY : 0.515 G +/-0.194 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 7.0621E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 121 DETECTOR S/N : 75545 AVERAGE %EFFICIENCY : 26.2144 AVERAGE %EFF ERROR : 0.5077 COUNTDATE: 17-Sep-201611:44:54 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B121.CNF;1158 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W121.CNF;322 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4519.65 4412.67 4.6532 dpm 5302.73 5323.47 PEAK NET 1 442.98 -0.20 PEAK NET2 1.28 234.52 RECOVERY YIELD CORR. 63.301 N/A 70.870 1.0077 NUCLIDE LIBRARY PEAK (ii I-z :::> 0 .?;-*:;: t5 <i: ENERGY ENERGY U-232 5302.10 5302.73 U-3/4 4763.02 4793.84 U-235 4391.00 4519.65 U-238 4184.73 4226.86 U-238: 3974.4264 keV 41 U-235:4311J..4581 keV U-3/4:4592-4865keV 37 U-232:5000-5398keV 33 29 25 21 17 13 9 5 2424 2819 3217 3620 Energy (keV) PEAK GROSS FWHM AREA 4.909 1.000 34.159 42.000 47.618 2.000 41.727 43.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.200 1.200 1.0954 100.000 -4.43E-03 40.560 1.440 1.2000 100.000 7.12E-01 1.280 0.720 0.8485 99.700 2.25E-02 42.040 0.960 0.9798 100.000 7.38E-01 5694 6121 6551 6986 7425 1.96-sigma TPU pCi/G 6.66E-02 2.61E-01 6.22E-02 2.65E-01 NOTES: MDA pCi/G 1.55E-01 1.30E-01 1.08E-01 1.16E-01 Le pCi/G 4.44E-02 3.86E-02 2.74E-02 3.15E-02 1.96-sigma cnt Unc pCi/G 6.64E-02 2.27E-01 6.20E-02 2.29E-01

Results are a compilation of S0405235066_UU and T0405235066_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.007 +/-0.000) 0 ...., ..,, 00 0 \0 BATCH NUMBER : 1596418 SAMPLE ID : S0405235066 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 010 DETECTOR S/N : 72529 AVERAGE %EFFICIENCY : 29.8601 AVERAGE %EFF ERROR : 0.5768 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 70.9 +/-7.356 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6532E+OO dpm 3.2977E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5323.47 U-3/4 4763.02 4778.58 U-235 4391.00 4412.67 U-238 4184.73 4202.35 U-238: 3974-4284 keV U-235;431D-4581 keV 28 U-3/4:4592-4865keV U-232:5000.5398keV 25 22 19 0' 16 z 13 :J 0 10 c 7 *:;: u 4 <( PEAK FWHM 24.469 22.101 49.114 72.852 COUNT DATE : 17-Sep-2016 11 :42:40 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA SIDev pCi/G 241.000 234.520 6.480 2.5456 100.000 4.12E+OO 42.000 40.560 1.440 1.2000 100.000 7.07E-01 2.000 1.280 0.720 0.8485 99.700 2.24E-02 43.000 42.040 0.960 0.9798 100.000 7.33E-01 i 2405 2800 3199 3602 4 09 420 48 6 5255 5678 6106 6537 6973 7412 Energy (keV) ::i Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B010.CNF;1841 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W010.CNF;511 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.16E-01 2.16E-01 8.19E-02 2.48E-01 1.29E-01 3.83E-02 6.17E-02 1.07E-01 2.72E-02 2.52E-01 1.15E-01 3.13E-02 1.96-sigma cnt Unc pCi/G 5.37E-01 2.25E-01 6.16E-02 2.27E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235067 UU SAMPLE QTY : 0.508 G -+/-0.197 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 83.2 +/-8.127 % SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0744E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 122 DETECTOR S/N : 75546 AVERAGE %EFFICIENCY : 25.9617 AVERAGE %EFF ERROR : 0.5030 COUNTDATE: 17-Sep-201611:44:56 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B122.CNF;1170 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W122.CNF;334 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4494.61 4490.61 TRACER2 1564-1 U-232 4.6535 dpm 5251.42 5340.45 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5251.42 4.959 1.000 0.040 0.960 0.9798 100.000 U-3/4 4763.02 4783.25 27.272 43.000 39.400 3.600 1.8974 100.000 U-235 4391.00 4494.61 34.400 2.000 0.320 1.680 1.2961 99.700 U-238 4184.73 4190.49 78.098 51.000 49.560 1.440 1.2000 100.000 U.238'3974-4284keV 71 U.235:43104581 keV 64 U-314:4592-4865keV -U-232:5000-5398keV 57 43 -Yi 36 1--z :::> 29 0 s 22 15 *:;; u 8 <( -.I ... ui, Ill I I I I I I I I I I I 23 82 2781 3183 3589 3 99 413 48 0 5251 5676 6105 6537 6974 Energy (keV) ACTIVITY pCi/G 6.00E-04 5.63E-01 4.59E-03 7.08E-01 I 7414 667.45 0.32 96.307 N/A 0.04 288.76 83.902 1.0079 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.46E-02 9.89E-02 2.69E-02 4.45E-02 2.09E-01 1.42E-01 4.97E-02 1.88E-01 5.23E-02 1.11E-01 3.40E-02 5.23E-02 2.34E-01 1.06E-01 3.14E-02 2.03E-01 NOTES:
Results are a compilation of S0405235067 _UU and T0405235067 _UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235067 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 011 DETECTOR S/N : 72531 AVERAGE %EFFICIENCY : 31.0555 AVERAGE %EFF ERROR : 0.5992 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.9 +/-6.745 % TRACER , ID 1564-1 NUCLIDE NOMINAL RESULTS U-232 4.6535E+OO dpm 3.9044E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5340.45 U-3/4 4763.02 4787.66 U-235 4391.00 4490.61 U-238 4184.73 4203.59 34 U*238:3974-4284keV lJ.235:43104581 keV 31 U-314: 45924865 keV U-232: 5000-5406 keV 28 25 22 0' 19 z 16 :J 13 0 10 c 7 *::; u 4 <i:: 1 2388 2788 3192 3601 Energy (keV) PEAK FWHM 36.661 52.176 129.198 62.943 COUNT DATE : 17-Sep-2016 11 :42:40 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 295.000 288.760 6.240 2.4980 100.000 4.13E+OO 43.000 39.400 3.600 1.8974 100.000 5.59E-01 2.000 0.320 1.680 1.2961 99.700 4.55E-03 51.000 49.560 1.440 1.2000 100.000 7.03E-01 7470 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B011.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W011.CNF;511 CAL DATE : 27-Aug-2016 1.96-sigma TPU pCi/G 7.45E-01 2.02E-01 5.19E-02 2.23E-01 NOTES: MDA pCi/G 1.74E-01 1.41E-01 1.10E-01 1.05E-01 Le pCi/G 6.54E-02 4.93E-02 3.38E-02 3.12E-02

Regions have been manually adjusted 1.96-sigma cnt Unc pCi/G 4.83E-01 1.86E-01 5.19E-02 2.01E-01 Alpha$peclrcscopySoftwareVersion3.5.3 effeclivedate:02-Mar-2015 BATCH NUMBER : 1596418 SAMPLE ID : T0405235068 UU SAMPLE QTY : 0.509 G -+/-0.196 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 82.9 +/-8.410 % SECONDARY QTY : 0.502 G +/-0.199 % TRACER . ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.7825E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 124 DETECTOR S/N : 80053 AVERAGE %EFFICIENCY : 24.5380 AVERAGE %EFF ERROR : 0.4761 COUNT DATE : 17-Sep-2016 11 :44:59 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD"A-011 LIB FILE : U236 BKG FILE : B124.CNF;1158 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W124.CNF;300 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4490.35 4414.65 4.6535 dpm 5198.58 5327.34 PEAKNET1 574.37 -1.68 PEAK NET2 4.80 271.76 RECOVERY YIELD CORR. 87.685 N/A 83.585 1.0078 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.58 0.000 0.000 U-3/4 4763.02 4758.87 64.409 55.000 U-235 4391.00 4490.35 51.747 6.000 U-238 4184.73 4209.68 72.047 67.000 !:; 55 U-238:3974-4284keV U-235:431()-4581 keV U-314: 4592-4865 keV 49 U-232:5000-5398keV 43 37 (ii 31 I-z 25 ::> 0 19 13 *:;; n 7 <x: 1 2377 2775 3177 3583 3 92 Energy (keV) ; NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -1.680 1.680 1.2961 100.000 -2.94E-02 51.640 3.360 1.8330 100.000 7.83E-01 4.800 1.200 1.0954 99.700 7.30E-02 66.520 0.480 0.6928 100.000 1.01E+OO > 5665 6092 6523 6958 7396 1.96-sigma TPU pCi/G 4.16E-02 2.60E-01 8.17E-02 2.99E-01 NOTES: MDA pCi/G 1.36E-01 1.47E-01 1.07E-01 8.39E-02 Le pCi/G 4.16E-02 5.09E-02 3.05E-02 1.92E-02 1.96-sigma cnt Unc pCi/G 4.15E-02 2.24E-01 8.07E-02 2.45E-01
Results are a compilation of S0405235068_UU and T0405235068_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

AlphaSpeclroscopySoftwareVersion3.5.3 effectivedate:02-Mar*2015 BATCH NUMBER : 1596418 SAMPLE ID : S0405235068 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 012 DETECTOR S/N : 80054 AVERAGE %EFFICIENCY : 29.3381 AVERAGE %EFF ERROR : 0.5668 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.6 +/-6.915 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6535E+OO dpm 3.8896E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5327.34 U-3/4 4763.02 4784.80 U-235 4391.00 4414.65 U-238 4184.73 4204.44 28 U-238: 3974-4284 keV U-235:4310-4581 keV 25 U-314:45924865keV U-232:5000-5398keV 22 19 Ci) 16 I-13 z :::) 0 10 8 z. 7 *s; u 4 <( 1 2402 2797 3196 3599 Energy (keV) PEAK FWHM 63.348 34.777 4.910 58.507 *COUNT DATE : 17-Sep-201611:42:40 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 278.000 271.760 6.240 2.4980 100.000 4.12E+OO 55.000 51.640 3.360 1.8330 100.000 7.77E-01 6.000 4.800 1.200 1.0954 99.700 7.24E-02 67.000 66.520 0.480 0.6928 100.000 1.00E+OO 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B012.CNF;1837 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W012.CNF;494 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 7.64E-01 1.84E-01 6.93E-02 2.48E-01 1.46E-01 5.05E-02 8.08E-02 1.06E-01 3.03E-02 2.81E-01 8.33E-02 1.91E-02 1.96-sigma cnt Unc pCi/G 4.97E-01 2.22E-01 8.01E-02 2.43E-01 Alpha Spactrosoopy Sottware Version 3.5.3 effedivedate:OZ-Mar-2015 BATCH NUMBER : 1596418 SAMPLE ID : T0405235069 UU SAMPLE QTY : 0.505 G -+/-0.198 % SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 83.0 +/-7.875 % SECONDARY QTY : 0.505 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0875E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 126 DETECTOR S/N : 75548 AVERAGE %EFFICIENCY : 25.0653 AVERAGE %EFF ERROR : 0.4861 COUNT DATE : 17-Sep-2016 11 :45:01 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B126.CNF;1162 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W126.CNF;338 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4491. 76 4429. 79 4.6529 dpm 5250.62 5329.42 PEAK NET 1 652.24 0.80 PEAKNET2 3.00 325.44 RECOVERY YIELD CORR. 97.477 N/A 83.834 1.0106 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5250.62 144.136 2.000 U-3/4 4763.02 4779.86 41.004 66.000 U-235 4391.00 4491.76 35.405 3.000 U-238 4184.73 4190.90 46.388 64.000 U-238:3974*4284keV 64 U-235:4310-4581 keV U-314:4592-4865keV 57 U-232:5000-5398keV 50 43 00 36 I-z 29 :J 0 22 15 *::; 8 <( 1 2389 2788 3192 3599 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA Stoev pCi/G 0.800 1.200 1.0954 100.000 1.23E-02 64.800 1.200 1.0954 100.000 8.29E-01 3.000 0.000 0.0000 99.700 3.85E-02 63.760 0.240 0.4899 100.000 8.16E-01 5693 6123 6558 6996 7438 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 5.50E-02 1.07E-01 3.08E-02 5.50E-02 2.44E-01 8.97E-02 2.57E-02 2.06E-01 5.10E-02 3.85E-02 O.OOE+OO 5.06E-02 2.40E-01 6.13E-02 1.15E-02 2.02E-01 NOTES: *Results are a compilation of S0405235069_UU and T0405235069_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235069 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 013 DETECTOR S/N : 78790 AVERAGE %EFFICIENCY : 35.0288 AVERAGE %EFF ERROR : 0.6744 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.8 +/-6.41!j % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6529E+OO dpm 3.9007E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5329.42 U-3/4 4763.02 4783.77 U-235 4391.00 4429.79 U-238 4184.73 4203.45 U-238:3974-4284keV 31 U-235:4310-4581 keV U-314: 4592-4865 keV U-232:5000.5398keV 28 25 22 Ci) 19 I-16 z :l 13 0 8. 10 .2:-7 *:;; n 4 <t: 2395 Energy (keV) PEAK FWHM 52.927 21.468 198.168 65.643 COUNT DATE : 17-Sep-201611:42:41 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 330.000 325.440 4.560 2.1354 100.000 4.15E+OO 66.000 64.800 1.200 1.0954 100.000 8.20E-01 3.000 3.000 0.000 0.0000 99.700 3.81E-02 64.000 63.760 0.240 0.4899 100.000 8.07E-01 7467* Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B013.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W013.CNF;513 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.10E-01 1.38E-01 4.99E-02 2.30E-01 8.88E-02 2.54E-02 5.04E-02 3.81E-02 O.OOE+OO 2.26E-01 6.07E-02 1.14E-02 1.96-sigma cnt Unc pCi/G 4.56E-01 2.04E-01 5.01E-02 2.00E-01 "' ("O """ Version 3.5.3 0 '"" BATCH NUMBER : 1596418 SAMPLE ID : T0405235070 UU @ SAMPLE QTY : 0.509 G -+/-0.196 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 88.6 +/-7.887 % SECONDARY QTY : 0.510 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0422E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 127 DETECTOR S/N : 78770 AVERAGE %EFFICIENCY : 26.6218 AVERAGE %EFF ERROR : 0.5155 COUNT DATE : 17-Sep-201611:45:04 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B127.CNF;1165 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W127.CNF;322 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4486.14 4545.16 TRACER2 1564-1 U-232 4.6535 dpm 5198.55 5335.00 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G U-232 5302.10 5198.55 0.000 0.000 -1.440 1.440 1.2000 100.000 -2.15E-02 U-3/4 4763.02 4764.95 59.086 48.000 47.280 0.720 0.8485 100.000 6.02E-01 U-235 4391.00 4486.14 59.322 2.000 1.040 0.960 0.9798 99.700 1.33E-02 U-238 4184.73 4202.83 14.521 64.000 63.040 0.960 0.9798 100.000 8.02E-01 >> .=.: ii 61 U-238:3974-4284keV U-235:4310-4581 keV 55 U-3/4:4592-4865keV U*232:SOOQ.5398keV 49 43 37 (ii 31 I-z :::> 25 0 s 19 13 *:;: 7 2382 2781 3183 3590 4 00 5681 6111 6545 6982 7424 Energy (keV) 663.87 1.04 93.414 N/A -1.44 323.52 89.309 1.0078 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 3.47E-02 1.10E-01 3.28E-02 3.46E-02 2.00E-01 7.78E-02 1.98E-02 1.75E-01 4.54E-02 8.41E-02 2.29E-02 4.54E-02 2.39E-01 8.39E-02 2.28E-02 2.02E-01 NOTES:

Results are a compilation of S0405235070_UU and T0405235070_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235070 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 014 DETECTOR S/N : 83289 AVERAGE %EFFICIENCY : 32.6875 AVERAGE %EFF ERROR : 0.6302 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 89.3 +/-6.449 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6535E+OO dpm 4.1560E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5335.00 U-3/4 4763.02 4772.03 U-235 4391.00 4545.16 U-238 4184.73 4218.40 U*238:3974-4284keV 41 U-235:431Cl-4581 keV U-314:4592-486SkeV 37 U-232:500CJ..5414keV 33 29 (j) 25 I-21 z ::> 17 0 13 .2!-9 *s: t5 5 <( 1 2378 2773 3173 3578 Energy (keV) PEAK FWHM 18.176 67.576 9.829 30.716 COUNT DATE: 17-Sep-201611:42:41 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 330.000 323.520 6.480 2.5456 100.000 4.12E+OO 48.000 47.280 0.720 0.8485 100.000 5.97E-01 2.000 1.040 0.960 0.9798 99.700 1.32E-02 64.000 63.040 0.960 0.9798 100.000 7.96E-01 6542 6983 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B014.CNF;1814 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W014.CNF;523 CAL DATE : 27-Aug-2016 1.96-sigma TPU pCi/G 7.09E-01 1.91E-01 4.51E-02 2.26E-01 NOTES: MDA pCi/G 1.57E-01 7.72E-02 8.35E-02 8.32E-02 Le pCi/G 5.94E-02 1.96E-02 2.27E-02 2.27E-02

Regions have been manually adjusted 1.96-sigma cnt Unc pCi/G 4.55E-01 1.74E-01 4.50E-02 2.00E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235071_UU SAMPLE QTY : 0.515 G +/-0.194 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 128 DETECTOR S/N : 75549 AVERAGE %EFFICIENCY : 26.0039 AVERAGE %EFF ERROR : 0.5038 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B128.CNF;1169 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 86.0 +/-7.881 % COUNT DATE : 17-Sep-2016 11 :45:06 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W128.CNF;324 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.506 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0790E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 671.38 -0.20 PEAK NET2 1.32 320.44 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5326.22 U-3/4 4763.02 4787.82 U-235 4391.00 4495.17 U-238 4184.73 4197.52 U-238* 3974-4284 keV U.235:43104581 keV 55 C-U-3J4:4592-4865keV U-232:5000-5398keV 49 f-43 f-37 f-Ci) 31 1--f-z 25 :::i f-0 19 f-13 *:;; f-n 7 <( f-1 f-I I I 24 00 2797 3198 3603 Energy (keV) 11.1230 dpm 4495.17 4396.18 4.6535 dpm 5326.22 5331.81 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA StDev 4.935 1.000 -0.200 1.200 1.0954 100.000 31.253 43.000 41.800 1.200 1.0954 100.000 53.430 3.000 1.320 1.680 1.2961 99.700 43.589 55.000 54.520 0.480 0.6928 100.000 ,.j .1 .. 11 ' I I ' I 4 12 425 5263 5688 6117 6550 6987 -ACTIVITY pCi/G -2.97E-03 5.31E-01 1.68E-02 6.93E-01 I 7429 1.96-sigma TPU pCi/G 4.47E-02 1.86E-01 5.28E-02 2.17E-01 NOTES: MDA pCi/G 1.04E-01 8.91E-02 9.87E-02 7.03E-02 96.716 NIA 86.654 1.0078 Le pCi/G 2.98E-02 2.55E-02 3.02E-02 1.61E-02 1.96-sigma cnt Unc pCi/G 4.46E-02 1.66E-01 5.27E-02 1.87E-01
Results are a compilation of S0405235071_UU and T0405235071_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000) 0 ....., Vl 00 0 \0 BATCH NUMBER : 1596418 SAMPLE ID : S0405235071_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 015 DETECTOR S/N : 80055 SAMPLE QTY : 0.515 G +/-0.194 % AVERAGE %EFFICIENCY : 33.3682 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.7 +/-6.455 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6535E+OO dpm 4.0325E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5331.81 U-3/4 4763.02 4791.00 U-235 4391.00 4396.18 U-238 4184.73 4220.26 37 U-238:3974-4284keV lJ.235:4310-4581 keV U-314:45924865keV 33 U*232:5000-5398keV 29 25 (j) 21 I-z 17 :J 0 13 s 9 *:;: t5 5 <( PEAK FWHM 23.884 52.861 4.917 46.714 ;i;s AVERAGE %EFF ERROR : 0.6430 COUNTDATE: 17-Sep-201611:42:41 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 325.000 320.440 4.560 2.1354 100.000 4.07E+OO 43.000 41.800 1.200 1.0954 100.000 5.27E-01 3.000 1.320 1.680 1.2961 99.700 1.67E-02 55.000 54.520 0.480 0.6928 100.000 6.87E-01 > 2386 2781 3182 3587 3 96 410 48 9 5252 5680 6112 6549 6990 7436 Energy (keV) 2: ' Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B015.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W015.CNF;530 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.01E-01 1.37E-01 4.97E-02 1.79E-01 8.84E-02 2.53E-02 5.24E-02 9.80E-02 3.00E-02 2.06E-01 6.98E-02 1.60E-02 1.96-sigma cnt Unc pCi/G 4.50E-01 1.65E-01 5.23E-02 1.85E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235072 UU SAMPLE QTY : 0.513 G -+/-0.195 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 129 DETECTOR S/N : 76227 AVERAGE %EFFICIENCY : 26.3145 AVERAGE %EFF ERROR : 0.5097 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B129.CNF;1168 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 72.5 +/-8.340 % COUNT DATE : 17-Sep-2016 11:45:08 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W129.CNF;343 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.7508E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 613.96 0.52 PEAK NET2 7.04 271.00 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5321.84 4.932 U-3/4 4763.02 4774.35 26.715 U-235 4391.00 4489.30 51.608 U-238 4184.73 4204.51 62.267 ll lJ.238* 39744284 keV 64 lJ.235:4310-4581 keV U-3/4:4592-4865keV 57 U*232:5000-5398keV 50 43 u; 36 I-z 29 ::::> 0 22 s 15 *:;; u 8 <l'. I.I I I I I 23 79 2776 3177 3582 3! 91 404 Energy (keV) 11.1230 dpm 4489.30 4451.07 4.6530 dpm 5321.84 5334.22 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA S!Dev 1.000 0.520 0.480 0.6928 100.000 66.000 62.160 3.840 1.9596 100.000 8.000 7.040 0.960 0.9798 99.700 48.000 47.040 0.960 0.9798 100.000 ll i JI I I I I I I 48 1 5242 5668 6097 6531 6969 -ACTIVITY pCi/G 8.50E-03 9.39E-01 1.07E-01 i11E-01 I 7411 1.96-sigma TPU pCi/G 4.73E-02 2.91E-01 9.23E-02 2.40E-01 NOTES: MDA pCi/G 9.05E-02 1.54E-01 9.99E-02 9.96E-02 87.401 N/A 73.174 1.0098 Le pCi/G 2.07E-02 5.42E-02 2.72E-02 2.71E-02 1.96-sigma cnt Unc pCi/G 4.72E-02 2.44E-01 9.05E-02 2.08E-01
Results are a compilation of S0405235072_UU and T0405235072_UU.
The following nuclide *results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235072 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.513 G -+/-0.195 % CHAMBER : 016 DETECTOR S/N : 78774 AVERAGE %EFFICIENCY : 33.4185 AVERAGE %EFF ERROR : 0.6439 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 73.2 +/-6.918 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6530E+OO dpm 3.4048E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5334.22 U-3/4 4763.02 4783.92 U-235 4391.00 4451.07 U-238 4184.73 4215.06 U-238:3974-4284keV 23 U-235:4310-4581 keV lJ..3/4:4592-4865keV 21 U-232: 4998-5428 keV 19 17 15 Ul I-13 z 11 :::::> 9 0 7 5 *:;; :g 3 <l:'. 1 2399 2793 3192 3596 Energy (keV) PEAK FWHM 46.059 11.531 19.581 30.024 4 04 COUNT DATE: 17-Sep-201611:42:41 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 277.000 271.000 6.000 2.4495 100.000 4.09E+OO 66.000 62.160 3.840 1.9596 100.000 9.30E-01 8.000 7.040 0.960 0.9798 99.700 1.06E-01 48.000 47.040 0.960 0.9798 100.000 7.04E-01 7443 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B016.CNF;1809 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W016.CNF;494 CAL DATE : 27-Aug-2016 1.96-sigma TPU pCi/G 7.58E-01 2.75E-01 9.09E-02 2.28E-01 NOTES: MDA pCi/G 1.81E-01 1.52E-01 9.89E-02 9.86E-02 Le pCi/G 6.76E-02 5.37E-02 2.69E-02 2.69E-02

Regions have been manually adjusted 1.96-sigma cnt Unc pCi/G 4.94E-01 2.42E-01 8.96E-02 2.06E-01

..., 3.5.3 0 ....., BATCH NUMBER : 1596418 SAMPLE ID : T0405235073 UU g SAMPLE QTY : 0.505 G -+/-0.198 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 82.9 +/-8.205 % SECONDARY QTY : 0.515 G +/-0.194 % TRACER ID NUCLIDE : NOMINAL: RESULTS : 1570-E U-235 1.1123E+01 dpm 1.0232E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 130 DETECTOR S/N : 76228 AVERAGE %EFFICIENCY : 26.6411 AVERAGE %EFF ERROR : 0.5158 COUNTDATE: 17-Sep-201611:45:10 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B130.CNF;1165 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W130.CNF;349 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4483.54 4372.84 4.6535 dpm 5185.30 5321.59 PEAK NET 1 652.26 1.28 PEAK NET2 3.28 281.52 RECOVERY YIELD CORR. 91.715 N/A 83.933 1.0124 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5185.30 319.016 2.000 U-3/4 4763.02 4757.44 12.270 47.000 U-235 4391.00 4483.54 36.673 4.000 U-238 4184.73 4181.37 50.920 53.000 U2J8*3974-4284keV 61 U-2J5;4310-4581keV U-3/4:4592-4865keV U*232:500Q..5398keV 55 49 43 0: 37 z 31 ;:) 25 0 19 .?;-13 *s; n 7 <i: .11.l J'I .1 .. I I I 23 98 2793 3192 3596 4 04 416 48l3 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN AREA AREA StDev 1.280 0.720 0.8485 100.000 45.800 1.200 1.0954 100.000 3.280 0.720 0.8485 99.700 52.040 0.960 0.9798 100.000 I I I I 5254 5679 6109 6544 6982 ACTIVITY pCi/G 1.92E-02 6.78E-01 4.87E-02 7.71E-01 I 7425 1.96-sigma TPU pCi/G 5.30E-02 2.31E-01 6.71E-02 2.49E-01 NOTES: MDA pCi/G 9.18E-02 1.04E-01 9.08E-02 9.76E-02 Le pCi/G 2.34E-02 2.97E-02 2.31E-02 2.66E-02 1.96-sigma cnt Unc pCi/G 5.30E-02 2.02E-01 6.66E-02 2.14E-01

Results are a compilation of S0405235073_UU and T0405235073_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: (0.010 +1-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235073 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 017 DETECTOR S/N : 78791 SAMPLE QTY : 0.505 G -+/-0.198 % AVERAGE %EFFICIENCY : 30.2659 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.9 +/-6.818 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6535E+OO dpm 3.9058E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5321.59 U-3/4 4763.02 4777.29 U-235 4391.00 4372.84 U-238 4184.73 4197.99 31 U-238:3974-4284keV U-235:4310-4581keV 28 U-314:4592-4865keV U.232:5000-5398keV 25 22 19 rn 16 I-z 13 :::> 0 s 10 a 7 *::; 4 2382 2779 3181 3587 Energy (keV) PEAK FWHM 63.674 14.661 88.809 53.655 AVERAGE %EFF ERROR : 0.5843 COUNTDATE: 17-Sep-201611:42:41 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 288.000 281.520 6.480 2.5456 100.000 4.15E+OO 47.000 45.800 1.200 1.0954 100.000 6.70E-01 4.000 3.280 0.720 0.8485 99.700 4.81E-02 53.000 52.040 0.960 0.9798 100.000 7.61E-01 6553 6994 7440 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B017.CNF;2655 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W017.CNF;1450 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.58E-01 1.82E-01 6.88E-02 2.20E-01 1.03E-01 2.94E-02 6.61E-02 8.96E-02 2.28E-02 2.36E-01 9.64E-02 2.63E-02 1.96-sigma cnt Unc pCi/G 4.93E-01 1.99E-01 6.58E-02 2.11E-01 Alpha Spectroscopy Software Varsion 3.5.3 affactlvadate:02-Mar*2015 BATCH NUMBER : 1596418 SAMPLE ID : T0405235074 UU SAMPLE QTY : 0.501 G -+/-0.200 % SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 77.4 +/-8.208 % SECONDARY QTY : 0.517 G +/-0.193 % TRACER ID NUCLIDE : NOMINAL: RESULTS : 1570-E U-235 1.1123E+01 dpm 1.1648E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 131 DETECTOR S/N : 80008 AVERAGE %EFFICIENCY : 25.5970 AVERAGE %EFF ERROR : 0.4961 COUNT DATE : 17-Sep-2016 11 :45:13 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B131.CNF;1160 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W131.CNF;319 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4485.87 4446. 79 4.6530 dpm 5198.56 5326.43 PEAK NET 1 713.44 -0.72 PEAKNET2 0.28 270.72 RECOVERY YIELD CORR. 104.409 N/A 77 .972 1.0077 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.56 0.000 0.000 U-3/4 4763.02 4767.10 70.676 43.000 U-235 4391.00 4485.87 31.420 1.000 U-238 4184.73 4187.93 78.942 64.000 >> :s i 81 U.238:3974-4284kaV U.235:43104581 kaV 73 U-3/4:4592-4865keV U-232:5000-5398keV 65 57 49 en 41 1--z ::> 33 0 s 25 17 *:;; ti 9 <t: 2379 2778 3181 3587 3 97 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G -0.720 0.720 0.8485 100.000 -9.86E-03 41.320 1.680 1.2961 100.000 6.39E-01 0.280 0.720 0.8485 99.700 4.34E-03 62.560 1.440 1.2000 100.000 9.67E-01 5678 6108 6542 6979 7421 !:! 1.96-sigma TPU pCi/G 2.98E-02 2.28E-01 4.54E-02 2.92E-01 NOTES: MDA pCi/G 8.36E-02 1.20E-01 9.47E-02 1.14E-01 Le pCi/G 2.13E-02 3.67E-02 2.41E-02 3.40E-02 1.96-sigma en! Une pCi/G 2.98E-02 2.02E-01 4.54E-02 2.45E-01

Results are a compilation of S0405235074_UU and T0405235074_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235074 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 018 DETECTOR SIN : 78782 AVERAGE %EFFICIENCY : 31.3297 AVERAGE %EFF ERROR : 0.6044 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 78.0 +/-6.913 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6530E+OO dpm 3.6281E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5326.43 U-3/4 4763.02 4777.18 U-235 4391.00 4446.79 U-238 4184.73 4197.13 34 U-238:3974-42S4keV U-235:43104581 keV 31 lJ..3.14:4592-4865keV U-232:5000-5398keV 28 25 22 (ii 19 I-16 z :::> 13 0 s 10 7 *:;; t5 4 <t: 1 2380 2776 3176 3581 Energy (keV) PEAK FWHM 28.662 49.790 4.918 27.398 COUNT DATE : 17-Sep-201611 :42:41 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 276.000 270.720 5.280 2.2978 100.000 4.18E+OO 43.000 41.320 1.680 1.2961 100.000 6.34E-01 1.000 0.280 0.720 0.8485 99.700 4.31E-03 64.000 62.560 1.440 1.2000 100.000 9.59E-01 > 5675 6108 6545 6987 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B018.CNF;1810 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W018.CNF;484 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.76E-01 1.76E-01 6.50E-02 2.19E-01 1.19E-01 3.64E-02 4.51E-02 9.40E-02 2.39E-02 2.78E-01 1.13E-01 3.37E-02 1.96-sigma cnt Unc pCi/G 5.05E-01 2.00E-01 4.50E-02 2.43E-01 BATCH NUMBER : 1596418 SAMPLE ID : T0405235075 UU SAMPLE QTY : 0.508 G -+/-0.197 % SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 68.1 +/-8.792 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 8.4573E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 132 DETECTOR S/N : 67579 AVERAGE %EFFICIENCY : 26.0712 AVERAGE %EFF ERROR : 0.5050 COUNTDATE: 17-Sep-201611:45:16 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B132.CNF;1156 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W132.CNF;324 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4492.82 4445.87 TRACER2 1564-1 U-232 4.6529 dpm 5198.57 5317.75 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5198.57 0.000 0.000 -1.440 1.440 1.2000 100.000 U-3/4 4763.02 4769.72 65.455 35.000 33.800 1.200 1.0954 100.000 U-235 4391.00 4492.82 48.535 7.000 6.760 0.240 0.4899 99.700 U-238 4184.73 4192.81 67.513 35.000 34.760 0.240 0.4899 100.000 -U 2J8* 3974-4284 keV U-235:431()-4581 keV 46 1-U-314: 45924865 keV U-232:5000.5398keV 41 >--36 Ui 26 I--z 21 => -0 16 -c 11 *5 >--u 6 <( >---.. JJ1. i.JI .JlJI I I I I' I I I I I 23 82 2780 3180 3585 3!94 406 48 2 5241 5665 6092 6523 6958 -Energy (keV) ACTIVITY pCi/G -2.74E-02 5.90E-01 1.18E-01 6.07E-01 I 7396 527.59 6.76 75.806 N/A -1.44 236.36 68.663 1.0076 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCl/G pCi/G pCi/G pCi/G 4.43E-02 1.41E-01 4.18E-02 4.42E-02 2.31E-01 1.22E-01 3.50E-02 2.06E-01 1.00E-01 8.39E-02 1.57E-02 9.78E-02 2.32E-01 8.37E-02 1.57E-02 2.06E-01 NOTES: *Results are a compilation of S0405235075_UU and T0405235075_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235075 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 020 DETECTOR S/N : 78787 SAMPLE QTY : 0.508 G -+/-0.197 % AVERAGE %EFFICIENCY : 31.0619 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 68.7 +/-7.273 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6529E+OO dpm 3.1948E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5317.75 U-3/4 4763.02 4773.04 U-235 4391.00 4445.87 U-238 4184.73 4206.61 lJ.238: 3974-4284 keV 17 lJ.235:4310-4581 kaV U-31'4:4592'486SkeV lJ..232:S000-5398keV 15 13 11 en 9 1--z ::J 7 0 £ 5 3 0 <t: PEAK FWHM 56.794 81.487 4.939 74.079 AVERAGE %EFF ERROR : 0.5993 COUNTDATE: 17-Sep-201611:42:42 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 239.000 236.360 2.640 1.6248 100.000 4.13E+OO 35.000 33.800 1.200 1.0954 100.000 5.86E-01 7.000 6.760 0.240 0.4899 99.700 1.17E-01 35.000 34.760 0.240 0.4899 100.000 6.02E-01 :g 2401 2798 3198 3602 4 09 420 5673 6098 6526 6958 7393 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B020.CNF;1831 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W020.CNF;560 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.08E-01 1.56E-01 5.20E-02 2.22E-01 1.21E-01 3.48E-02 9.85E-02 8.33E-02 1.56E-02 2.23E-01 8.31E-02 1.55E-02 1.96-sigma cnt Unc pCi/G 5.31E-01 2.05E-01 9.70E-02 2.04E-01 '"C (1) .j:>. N Alpha Spectroscopy Software Verslon 3.5.3 O effectlvedata:OZ-Mar-2015 0 ....., BATCH NUMBER : 1596418 SAMPLE ID : T0405235076 UU SAMPLE QTY : 0.512 G -+/-0.195 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 89.6 +/-7.999 % SECONDARY QTY : 0.507 G +/-0.197 % TRACER .ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.7622E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 133 DETECTOR S/N : 76229 AVERAGE %EFFICIENCY : 25.5293 AVERAGE %EFF ERROR : 0.4948 COUNTDATE: 17-Sep-201611:45:18 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B133.CNF;1153 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W133.CNF;359 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4493.84 4411.76 4.6535 dpm 5356.51 5325.19 PEAK NET 1 596.34 0.56 PEAKNET2 1.52 318.88 RECOVERY YIELD CORR. 87.503 N/A 90.461 1.0101 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5356.51 39.750 2.000 U-3/4 4763.02 4771.77 67.906 66.000 U-235 4391.00 4493.84 38.135 2.000 U-238 4184.73 4201.37 23.187 60.000 >> .:.: * ; 8 55 U-238: 3974-4284 keV U-235:4310-4581 keV U-3/4;4592-4865keV 49 U.232:5000-SJSBkeV 43 37 rn 31 I-z 25 :J 0 19 8 13 *:;; u 7 <1'. 1 2363 2763 3166 3573 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.560 1.440 1.2000 100.000 9.35E-03 65.040 0.960 0.9798 100.000 8.37E-01 1.520 0.480 0.6928 99.700 1.96E-02 59.760 0.240 0.4899 100.000 7.69E-01 5663 6092 6525 6961 7402 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 6.04E-02 1.24E-01 3.67E-02 6.04E-02 2.47E-01 8.48E-02 2.31E-02 2.07E-01 4.52E-02 7.15E-02 1.64E-02 4.51E-02 2.33E-01 6.17E-02 1.15E-02 1.97E-01 NOTES: *Results are a compilation of S0405235076_UU and T0405235076_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S0405235076 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 021 DETECTOR S/N : 795159 AVERAGE %EFFICIENCY : 31.8082 AVERAGE %EFF ERROR : 0.6134 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 90.5 +/-6.454 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6535E+OO dpm 4.2096E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5325.19 U-3/4 4763.02 4792.17 U-235 4391.00 4411.76 U-238 4184.73 4210.78 31 U..238; 3974-4284 keV U*235:4310-4581 keV 28 U-3!4: 45924865 keV lJ..232:5000-5398keV 25 22 19 0' 16 z 13 => 0 i2, 10 7 *:;; :g 4 <l'. 1 2394 2788 3187 3590 Energy (keV) PEAK FWHM 33.881 24.463 39.140 45.011 3 97 ;) COUNT DATE : 17-Sep-2016 11 :42:42 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 322.000 318.880 3.120 1.7664 100.000 4.09E+OO 66.000 65.040 0.960 0.9798 100.000 8.29E-01 2.000 1.520 0.480 0.6928 99.700 1.94E-02 60.000 59.760 0.240 0.4899 100.000 7.61E-01 5673 6104 6539 6978 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B021.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W021.CNF;537 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.05E-01 1.22E-01 4.15E-02 2.32E-01 8.40E-02 2.29E-02 4.47E-02 7.08E-02 1.62E-02 2.20E-01 6.11E-02 1.14E-02 1.96-sigma cnt Unc pCi/G 4.53E-01 2.05E-01 4.46E-02 1.95E-01 AlphaSpectroscopySoftwareVersJonJ.5,3 effeclivedate:02-Mar*2015 BATCH NUMBER : 1596418 SAMPLE ID : T0405235077 UU SAMPLE QTY : 0.510 G -+/-0.196 % SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 98.6 +/-7.735 % SECONDARY QTY : 0.510 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.2684E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 134 DETECTOR S/N : 76230 AVERAGE %EFFICIENCY : 25.7389 AVERAGE %EFF ERROR : 0.4988 COUNT DATE : 17-Sep-2016 11 :45:20 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B134.CNF;1149 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W134.CNF;336 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4490.69 4445.41 TRACER2 1564-1 U-232 4.6528 dpm 5198.58 5341.13 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5198.58 0.000 0.000 -0.480 0.480 0.6928 100.000 U-3/4 4763.02 4765.90 66.549 65.000 63.560 1.440 1.2000 100.000 U-235 4391.00 4490.69 41.660 0.000 -0.480 0.480 0.6928 99.700 U-238 4184.73 4204.31 53.735 63.000 62.520 0.480 0.6928 100.000 i !::::J U-238:3974-4284keV 46 U-235:43104581 keV U-3/4:4592-4865keV 41 U-232:5000-5398keV 36 31 en 26 1--z 21 :J 0 16 £ 11 *:;; 6 2387 2786 3188 3594 4 04 417 48 4 5255 5679 6107 6539 6974 Energy (keV) ACTIVITY pCi/G -8.32E-03 6.88E-01 -5.21E-03 6.77E-01 7413 570.82 -0.48 83.077 N/A -0.48 379.48 99.322 1.0076 1.96-si9ma 1.96-si9ma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 3.69E-02 9.60E-02 2.20E-02 3.68E-02 2.04E-01 8.01E-02 2.38E-02 1.73E-01 2.31E-02 6.02E-02 1.38E-02 2.31E-02 2.00E-01 6.00E-02 1.37E-02 1.70E-01 NOTES:

Results are a compilation of S0405235077 _ UU and T0405235077 _UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

AJphaSpectroscopySoftwareVerslon3.5.3 effeetivedate:02-Mar*2015 BATCH NUMBER : 1596418 SAMPLE ID : S0405235077 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 024 DETECTOR S/N : 76542 AVERAGE %EFFICIENCY : 34.4760 AVERAGE %EFF ERROR : 0.6639 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 99.3 +/-6.058 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6528E+OO dpm 4.6212E+OO dpm NUCLIDE LIBRARY PEAK "Ci) I-z :::i 0 .?;-*:;: ti <l'. ENERGY ENERGY U-232 5302.10 5341.13 U-3/4 4763.02 4786.44 U-235 4391.00 4445.41 U-238 4184.73 4227.59 lJ.238: 3976-4300 keV U-235:4310-4581keV 25 lJ.3/4;4591-4868keV U*232:4999-5445keV 22 19 16 13 10 7 4 2399 2793 3191 3594 Energy (keV) PEAK FWHM 89.042 83.477 0.000 42.814 COUNT DATE : 17-Sep-2016 11 :42:42 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 385.000 379.480 5.520 2.3495 100.000 4.11E+OO 65.000 63.560 1.440 1.2000 100.000 6.83E-01 0.000 -0.480 0.480 0.6928 99.700 -5.17E-03 63.000 62.520 0.480 0.6928 100.000 6.72E-01 6548 6989 7435 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B024.CNF;1824 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W024.CNF;517 CAL DATE : 27-Aug-2016 1.96-sigma TPU pCi/G 6.61E-01 1.92E-01 2.29E-02 1.88E-01 NOTES: MDA pCi/G 1.26E-01 7.95E-02 5.97E-02 5.95E-02 Le pCi/G 4.66E-02 2.36E-02 1.37E-02 1.36E-02

Regions have been manually adjusted 1.96-sigma cnt Unc pCi/G 4.18E-01 1.72E-01 2.29E-02 1.69E-01

'd -!:> Version 3.5.3 0 ...., BATCH NUMBER : 1596418 SAMPLE ID : T0405235078 UU ::E SAMPLE QTY : 0.505 G -+/-0.198 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 139 DETECTOR S/N : 76231 AVERAGE %EFFICIENCY : 24.8887 AVERAGE %EFF ERROR : 0.4828 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B139.CNF;1107 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 97.1 +/-11.797 % COUNT DATE : 17-Sep-201611:45:23 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W139.CNF;334 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.512 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.9940E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 118.75 -0.44 PEAKNET2 0.28 268.08 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5015.77 4.936 U-3/4 4763.02 4755.81 103.662 U-235 4391.00 4470.93 51.420 U-238 4184.73 4169.02 71.576 12 U.238:3974-4284keV lJ.235:4310-4581 keV 11 U-J.14;4592-4665keV U-232:5000-5398keV 10 9 8 0' 7 6 z 5 => 0 4 3 *::; 2 15 <( 2388 2785 3186 3591 4 01 414 Energy (keV) 11.1230 dpm 4470.93 4429.03 4.6528 dpm 5015.77 5321.19 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 1.000 -0.440 1.440 1.2000 100.000 41.000 40.280 0.720 0.8485 100.000 1.000 0.280 0.720 0.8485 99.700 38.000 36.560 1.440 1.2000 100.000 >> !l.= 48 2 5253 5679 6109 6543 6981 ACTIVITY pCilG -3.65E-02 6.24E-01 4.35E-03 5.66E-01 7423 1.96-sigma TPU pCi/G 2.53E-01 2.45E-01 4.56E-02 2.32E-01 NOTES: MDA pCi/G 6.14E-01 9.46E-02 9.49E-02 1.15E-01 17.873 NIA 97 .883 1.0076 Le pCi/G 1.83E-01 2.41E-02 2.41E-02 3.40E-02 1.96-sigma cnt Unc pCi/G 2.52E-01 1.97E-01 4.55E-02 1.90E-01

Results are a compilation of S0405235078_UU and T0405235078_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.002 +f-0.000)

AlphaSpactroscopySoftwaraVarslonJ.5.3 affective data: 02-Mar-2015 BATCH NUMBER : 1596418 SAMPLE ID : S0405235078 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 113 DETECTOR S/N : 80009 AVERAGE %EFFICIENCY : 24.7132 AVERAGE %EFF ERROR : 0.4794 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 97.9 +/-6.902 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6528E+OO dpm 4.5543E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5321.19 U-3/4 4763.02 4780.12 U-235 4391.00 4429.03 U-238 4184.73 4194.96 U-2J6:J974-4284kaV 23 U-235: 431Cl-4581 kaV U-314: 4592-4865 kaV 21 U*232:5000.5396keV 19 17 15 Cii 13 I-z 11 ::::> 9 0 s. 7 5 *:;;: 3 PEAK FWHM 51.836 18.969 4.949 51.960 COUNT DATE : 17-Sep-2016 11 :44:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 270.000 268.080 1.920 1.3856 100.000 4.15E+OO 41.000 40.280 0.720 0.8485 100.000 6.19E-01 1.000 0.280 0.720 0.8485 99.700 4.31E-03 38.000 36.560 1.440 1.2000 100.000 5.62E-01 i 2387 2785 3186 3592 4 01 413 5674 6102 6533 6968 7407 Energy (keV) !l !l Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B113.CNF;1165 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W113.CNF;318 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.68E-01 1.25E-01 3.93E-02 2.14E-01 9.39E-02 2.39E-02 4.52E-02 9.41E-02 2.40E-02 2.05E-01 1.14E-01 3.38E-02 1.96-sigma cnt Unc pCi/G 5.00E-01 1.96E-01 4.51E-02 1.89E-01 BATCH NUMBER : 1596418 SAMPLE ID : T1203621760 UU SAMPLE QTY : 0.518 G -+/-0.193 % SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 107 +/-7.595 % SECONDARY QTY : 0.517 G +/-0.193 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.2820E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 008 DETECTOR S/N : 78788 AVERAGE %EFFICIENCY : 32.5514 AVERAGE %EFF ERROR : 0.6275 COUNTDATE: 17-Sep-201611:42:40 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B008.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W008.CNF;515 CAL DATE : 27-Aug-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4509.62 4445.44 TRACER2 1564-1 U-232 4.6179 dpm 5271.27 5327.73 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5271.27 270.140 3.000 -6.600 9.600 3.0984 100.000 U-3/4 4763.02 4634.86 54.028 1.000 -0.920 1.920 1.3856 100.000 U-235 4391.00 4509.62 40.521 0.000 -0.480 0.480 o.6928 99.700 U-238 4184.73 4148.30 216.112 0.000 -1.200 1.200 1.0954 100.000 U.238 3974-4284keV 64 lJ..235: 4310-4581 keV U-3/4:45924865keV U-232:5000-5398keV 57 50 43 0' 36 z 29 ::i 0 £ 22 a 15 u 8 <( 1 .. ,, . ,J, ll ***' J _, II I I I I I 23 96 2791 3191 3595 4U03 416 48M 5255 5682 6112 6547 6987 '--Energy (keV) ACTIVITY pCi/G -8.85E-02 -1.04E-02 -5.46E-03 -1.36E-02 I 7430 722.97 -0.48 83.199 N/A -6.60 353.80 106.788 1.0001 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 6.63E-02 1.92E-01 7.61E-02 6.63E-02 3.53E-02 9.17E-02 2.88E-02 3.53E-02 2.42E-02 6.30E-02 1.44E-02 2.42E-02 2.59E-02 7.96E-02 2.28E-02 2.58E-02 NOTES: *Results are a compilation of S1203621760_UU and T1203621760_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596418 SAMPLE ID : S1203621760 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 004 DETECTOR S/N : 76389 AVERAGE %EFFICIENCY : 29.8956 AVERAGE %EFF ERROR : 0.5774 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 107 +/-6.188 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6179E+OO dpm 4.9314E+OD dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5327.73 U-3/4 4763.02 4622.89 U-235 4391.00 4445.44 U-238 4184.73 4129.07 41 tJ..238*3974-4284keV -U-235:431Q-4581 keV 37 U*314:4592-4665keV .-U-23Z:5000.5398keV 33 25 -(/) 21 I-f-z :J 17 f-0 s 13 f-9 *;;: f-ti 5 <!'. f-1 f-I I I PEAK FWHM 27.749 4.897 0.000 0.000 I I 24 21 2815 3213 3615 4 )21 Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 355.000 353.800 1.200 1.0954 100.000 4.02E+OO 1.000 -0.920 1.920 1.3856 100.000 -1.04E-02 0.000 -0.480 0.480 0.6928 99.700 -5.46E-03 0.000 -1.200 1.200 1.0954 100.000 -1.36E-02 I 11 "' .I.I I I I I I I 48 5265 5687 6114 6545 6980 7419 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B004.CNF;1844 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W004.CNF;539 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.61E-01 7.96E-02 2.28E-02 3.53E-02 9.17E-02 2.88E-02 2.42E-02 6.30E-02 1.44E-02 2.58E-02 7.96E-02 2.28E-02 1.96-sigma cnt Unc pCi/G 4.20E-01 3.53E-02 2.42E-02 2.58E-02 BATCH NUMBER : 1596418 SAMPLE ID : T1203621761_UU SAMPLE QTY : 0.507 G +/-0.197 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 87.1 +/-8.625 % SECONDARY QTY : 0.502 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.0031 E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 140 DETECTOR SIN : 78771 AVERAGE %EFFICIENCY : 26.0317 AVERAGE %EFF ERROR : 0.5043 COUNTDATE: 17-Sep-201611:45:25 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B140.CNF;1100 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W140.CNF;283 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4498.61 4439.44 4.6532 dpm 5369.55 5323.21 PEAK NET 1 560.79 4.04 PEAK NET2 2.04 244.52 RECOVERY YIELD CORR. 80.698 N/A 89.287 1.0252 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5369.55 4.953 5.000 U-3/4 4763.02 4772.75 35.082 39.000 U-235 4391.00 4498.61 27.741 3.000 U-238 4184.73 4213.87 39.622 40.000 '.;! U.238:3974-4264keV U-235:43104581 keV 64 U-314: 4592-4565 keV U-232:5000-5398keV 57 50 43 en 36 I-z 29 => 0 8 22 15 *:;; 8 <i: 1 2385 2784 3186 3592 4 02 Energy (keV) :'l NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 4.040 0.960 0.9798 100.000 7.25E-02 36.600 2.400 1.5492 100.000 6.30E-01 2.040 0.960 0.9798 99.700 3.52E-02 39.280 0.720 0.8485 100.000 6.76E-01 5681 6110 6543 6981 7422 1.96-sigma TPU pCi/G 8.90E-02 2.41E-01 7.03E-02 2.46E-01 NOTES: MDA pCi/G 1.18E-01 1.49E-01 1.14E-01 1.05E-01 Le pCi/G 3.22E-02 4.88E-02 3.10E-02 2.67E-02 1.96-sigma en! Une pCi/G 8.81E-02 2.15E-01 7.00E-02 2.16E-01 *Results are a compilation of S1203621761_UU and T1203621761_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000)

AlphaSpectroscopySoftwareVersion3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596418 SAMPLE ID : S1203621761_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 114 DETECTOR S/N : 78258 SAMPLE QTY : 0.507 G +/-0.197 % AVERAGE %EFFICIENCY : 24.7116 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 89.3 +/-7.143 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE U-232 U-3/4 U-235 U-238 1564-1 U-232 4.6532E+OO dpm 4.1547E+OO dpm LIBRARY PEAK ENERGY ENERGY 5302.10 5323.21 4763.02 4765.55 4391.00 4439.44 4184.73 4206.52 U-238: 3974-4254 keV 23 21 U-232:5000-5398keV 19 17 15 0' 13 z 11 6 9 £ 7 5 *;;; 3 PEAK FWHM 46.083 75.128 158.513 40.867 AVERAGE %EFF ERROR : 0.4794 COUNTDATE: 17-Sep-201611:44:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 245.000 244.520 0.480 0.6928 100.000 4.13E+OO 39.000 36.600 2.400 1.5492 100.000 6.14E-01 3.000 2.040 0.960 0.9798 99.700 3.43E-02 40.000 39.280 0.720 0.8485 100.000 6.59E-01 1 2390 2788 3190 3595 Energy (keV) 6103 6534 6968 7406 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B114.CNF;1168 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W114.CNF;324 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.94E-01 9.36E-02 2.15E-02 2.28E-01 1.46E-01 4.76E-02 6.85E-02 1.11E-01 3.02E-02 2.32E-01 1.02E-01 2.61E-02 1.96-sigma cnt Unc pCi/G 5.20E-01 2.10E-01 6.83E-02 2.11E-01 BATCH NUMBER : 1596418 SAMPLE ID : T1203621762 UU SAMPLE QTY : 0.518 G -+/-0.193 % SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 93.3 +/-8.747 % SECONDARY QTY : 0.517 G +/-0.193 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 6.8612E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 142 DETECTOR S/N : 42285 AVERAGE %EFFICIENCY : 26.5347 AVERAGE %EFF ERROR : 0.5139 COUNTDATE: 17-Sep-201611:45:28 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID NUCLIDE NOMINAL (pCi/G) % RECOVERY 1600-E U-238 5.1996E+OO 107.879 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B142.CNF;1100 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W142.CNF;306 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4498.41 4424.04 4.6179 dpm 5299.02 5310.25 PEAK NET 1 435.63 1.52 PEAKNET2 21.52 263.16 RECOVERY YIELD CORR. 61.500 N/A 94.122 1.0085 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5299.02 14.833 2.000 U-3/4 4763.02 4728.18 0.000 331.000 U-235 4391.00 4498.41 49.675 22.000 U-238 4184.73 4137.78 4.944 365.000 >> .:.!l 8 U-238:3974-4264keV 37 U-235:4310-4581keV U*3/4;45924665keV U-232;5000-5398keV 33 29 25 0' 21 z 17 :::> 0 13 i2, $ 9 *s; :g <( 5 1 2382 2780 3181 3586 3 94 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 1.520 0.480 0.6928 100.000 3.38E-02 329.560 1.440 1.2000 100.000 5.07E+OO 21.520 0.480 0.6928 99.700 3.32E-01 364.520 0.480 0.6928 100.000 5.61E+OO 5664 6091 6521 6955 7393 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.79E-02 1.23E-01 2.82E-02 7.77E-02 1.05E+OO 1.14E-01 3.38E-02 5.50E-01 1.57E-01 8.55E-02 1.96E-02 1.46E-01 1.14E+OO 8.52E-02 1.95E-02 5.77E-01 NOTES: *Results are a compilation of S1203621762_UU and T1203621762_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.007 +/-0.000) 0 ....., Vi 00 0 \0 BATCH NUMBER : 1596418 SAMPLE ID : S1203621762 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 115 DETECTOR S/N : 79995 SAMPLE QTY : 0.518 G -+/-0.193 % AVERAGE %EFFICIENCY : 25.2291 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 94.1 +/-6.978 % TRACER ID 1564-1 NUCLIDE U-232 NOMINAL 4.6179E+OO dpm RESULTS 4.3465E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5310.25 27.370 U-3/4 4763.02 4765.96 35.256 U-235 4391.00 4424.04 7.465 U-238 4184.73 4199.07 39.900 U238*3974-4284keV 37 -. U-235: 4310-4581 keV U-314:4592-4865keV 33 U-232:5000..5398keV 29 >--25 UJ 21 -I-z 17 -:J 0 13 *;;; 5 -AVERAGE %EFF ERROR : 0.4892 COUNTDATE: 17-Sep-201611:44:39 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 1600-E NUCLIDE U-238 NOMINAL (pCi/G) 5.1996E+OO % RECOVERY 106.971 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 267.000 263.160 3.840 1.9596 100.000 4.02E+OO 331.000 329.560 1.440 1.2000 100.000 5.03E+OO 22.000 21.520 0.480 0.6928 99.700 3.29E-01 365.000 364.520 0.480 0.6928 100.000 5.56E+OO n <l: 11 .., 111ll 1,1L 1, I ,,1.,11' u I I I I I I I I I I I 23 82 2782 3186 3593 4 04 418 48 6 5257 5682 6111 6543 6978 7417 Energy {keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B115.CNF;1177 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W115.CNF;335 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.52E-01 1.55E-01 5.48E-02 8.98E-01 1.13E-01 3.35E-02 1.52E-01 8.48E-02 1.94E-02 9.75E-01 8.45E-02 1.94E-02 1.96-sigma cnt Unc pCi/G 4.91E-01 5.45E-01 1.44E-01 5.72E-01 Effective 3/25/201 O Radiochemistry Balch Checklist Revision 1 Effective March 2010 30-Sep-2016 Product: ___ \,l _____ _ Date: Criteria: Yes No Comments Samele Solids are less than or equal to 100 mq for GAB. ili Samples have been blank corrected (If required). tJg Blank correction reoorted Included Cif reoulredl. lf activity Jess than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. lf greater than 10* MDA/ MDC, error Is 40% or less. "' If *hA MDA/ MDC. nrrnr I" nlr"u Instrument source check is within limits. Tnstrumnnt bka check Is within limits. ./ Method RDL/ LLD has been met. / lf duollcate activities are: Less than 5* MDA/ MDC, then RPD Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, Qu...t. lf below the MDA/ MDC, the RPO Is 0%, v Or meets the client's reaulred RER acceatance criteria. Tracer yield Is 15-125%
Carrier yield 25-125%. (Or meets the client's contract acceptance criteria}. i/ Method blank Is less than the RDL/ LLD. / !(If.,, .. < !iD/n nf lnwPc:t :.dlvltvl Samale was run within hold time. .r ../ ()Ell.Jk Samele was correctlv oreserved If reoulred. Smears Taken for Radioactive batches. k'Vr Method Spike and LCS are within 75-125% ./' Ir or meet-: the client'<= cnntr"r-t-ac"e""'"'"e ,.riteria l No blank spaces on data forms. ./ All line outs initialed and dated * .. " """ Aux data Is correct. klo-Client Sneclal reoulrements oaae has been checked. v Raw Data and I or soectrum are Included and orooerlv statused. ./ MS, LCS, and DUPiicate RPD/RER values uploaded to UMS and / u"luac uarlllArl ..... *-(if l h-A"trh AntArn.t *-*-r---/ Batch Data Exceotlon Reoorts fDERl comoleted if aoollcable. ,/ 1st,3y37 Batch Data Exception Reports (DER) second reviewed. 11' Dlsoositlon verified to be comnleted. Allm*ot Correctinn If reauirPd. \.-,ft-Review sample historical results if available (If REMP, results above MDC have been verified ./ bv historical results recount or re-analvsls.) Primary Review Performed __ I_,!,,"'--____ _ Secondary Review Performed By:_ 10/02/16 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER
DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 30-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, U-02-RC Solid . Batch ID: Sample Numbers: 1596389 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203621692 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 30-SEP-16 Jessica Davis 02-0CT-16 Page 1 Page 433 of 5809 DER Report No.: 1563433 Revision No.: Type: Process Client Code: MJWC '

Uranium Que Sheet 07-SEP-16 ------======-----------*-------------------*-------*---------================== Batch#: 1596389 Analyst: JXH2 Tracer Code: \ 5 Cott * --X:: First Client Due Date:04-0CT-16 Expiration Date: \\*7..'3-1(., Expiration Date: 7-1"2-1'1 Internal Due Date:30-SEP-16 LCS Code: \l,co Vol: 01\,....L. Vol: o.\ML. Spike Isotope: U-238 Prep Date: '\-Z..1.::-1 u. Spike Code: Initials: ..l f \.\ Sample ID Client Description -----405235001-1 4.1.B.R.1.2 405235002-1 4.1.B.R.1.3 405235003-1 4.1.B.R.1.4 405235004-1 4.1.B.R.7.2 405235005-1 4.1.C.R.1.3 405235006-1 4.1.C.R.l.4 405235007 -1 4.1.C.R.2.3 405235008-1 4-1-C.R.2.4 405235009-1 4.1.D.R.1.3 405235010-1 4.1.D.R.1.4 405235011-1 4.1.D.R.3.2 405235012-1 4.1.D.R.2.4 405235013-1 4.2A.R.2.3 405235014-1 4.2A.R.1.3 405235015-1 4.2A.R.l.4 405235016-1 4.2A.R.2.4 405235017-1 4.2A.R.3.2 405235018-1 4.2A.R.4.2 405235019-1 4.2B.R.2.4 405235020-1 4.2B.R.l.4 1203621691-1 MB for batch 1596389 1203621692-1 4.1.B.R.1.2(405235001DUP) 1203621693-1 LCS for batch 1596389 ,,__.. Expiration Date: Vol:-==-PipetID: Balance ID: \\.o\0'7C.. £.. 1.. Hazard Type Code MinCRDL Matrix Client SAMPLE 1 pCi/g SOIL 1\-UWCOOl SAMPLE 1 pCi/g SOIL l\UWCOOl SAMPLE 1 pCi/g SOIL l'>UWCOOl SAMPLE 1 pCi/g SOIL l'>UWCOOI SA!\-IPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL l'>UWCOOl SAMPLE 1 pCi/g SOIL MJWCOOI SAMPLE l pCi/g SOIL l\UWCOOI SAMPLE 1 pCi/g SOIL l'>UWCOOl SAl'vIPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL l'>UWCOOl SAMPLE 1 pCi/g SOIL M.JWCOOl SAIVIPLE 1 pCi/g SOIL l\UWCOOl SAMPLE 1 pCi/g SOIL r.uwcoo1 SAMPLE 1 pCi/g SOIL l'>UWCOOl SAMPLE 1 pCi/g SOIL M.JWCOOl SAl\IPLE 1 pCilg SOIL MJWCOOl SAMPLE 1 pCi/g SOIL l'>UWCOOl SAMPLE 1 pCi/g SOIL M'JWCOOl SAMPLE 1 pCi/g SOIL l'>UWCOOl l'vIB 1 pCi/g SOIL QC ACCOUNT DUP 1 pCi/g SOIL QC ACCOU.!'.'T LCS 1 pCi/g SOIL QC ACCOUNT Analyzed Sequentially with Pu Analyzed Sequentially with: Pu-236 ID: Pu: \S'i<.dcn Vol.: Am: \sc-\<.. 3'lC Witness: ¥"0 C\-'l.li r H 1 Collection Label Ali quo u Date Pos. # @/lit) Det# 10-DEC-15 1 l \ ! o.5oi I ! ! 10-DEC-15 2 ! z. i a.Sos ! E" i 10-DEC-15 3 r----;-----+---j \_l ___ 5o \ ! 2 _ _j 09-DEC-15 4 i l\ l 0. SDZ. l f i) I 10-DEC-15 5 ID, 5C'3 i L3 I 10-DEC-15 6 ! <o !o. St>\ r2fi 10-DEC-15 7 i _J_lQ_._S 6 \ ;.:J 10-DEC-15 8 l 8 lo, So) I !& I 10-DEC-15 9 ; I SOL{ 17 [_3 __ i0..i.=:.:: 10-DEC-15 10 ' I s r& ! '-D lQ1 C\ 09-DEC-15 11 ;.\ ! 'LJ, Sot;, 1.B 10-DEC-15 12 I \?..-:c.scc.,,

Zt 08-DEC-15 13 \ ?:> iei. soo 'Z3 08-DEC-15 14 il.\. lo.50-z. ?...':{_ 08-DEC-15 15 IS lo. So'\ L[3 08-DEC-15 16 ! \6 i ('.).Sc\ rl:i' 02-DEC-15 17 ! \I !a*. so\ LL& i 02-DEC-15 18 i 18 iD. S"oo rr? 08-DEC-15 19 i \q i l),50(, (_{8_ I 08-DEC-15 20 i "tc !D,56'2. 21 i *z..\ ! o. So<t 1/ 10-DEC-15 22 i 2.2. lo.soc f Zf 23 I io. 5i>'l rZ2_j i '2. ') Choose SOP used: GL-RAD-A-011 Solid Sample Dissolution by: LEACH. Circle One GEL Laboratories LLC, Radiochemistry Division Page 1 of 1

--l --l""'VV'l. Uranium Que Sheet 07-SEP-16 -------------------====================================================================-=-=--==-=-== Batch#: 1596389 Analyst: JXH2 First Client Due Date.f4fCT-16 Internal Due Date:30-SEP-16 Tracer Isotope: Code: \'Z:'i5>6.;r Date: "7-1:\.jJ?"" Vol: O, \rL x..i.:e.v Analyzed Sequentially with Pu Analyzed Sequentially with: LCS Isotope: U-238 LCS Code: -Expiration Date: Vol:-==-Pu-236 ID: Pu: ..-Spike Isotope: U-238 Spike Code: fa."Piration Date: Vol:_::::_ Vol.: ___ _ PrepDate: '\-Z..Co-\lo Initials: PipetID: BalanceID:\\.t.\Oll.>(.,1..-C\*i>.J-\\J. Hazard Sample ID Client Description Type Code Min.CRDL 405235001-1 4.1.B.R.1.2 SAMPLE 1 pCi/g 405235002-1 4.1.B.R.1.3 SAMPLE 1 pCi/g 405235003-1 4.1.B.R.1.4 SAMPLE 1 pCi/g 405235004-1 4.1.B.R.7.2 SA!'vlPLE 1 pCi/g 405235005-1 4.1.C.R.1.3 SA!\IPLE 1 pCi/g 405235006-1 4.1.C.R.1.4 SA!'vlPLE 1 pCi/g 4052..l5007-l 4.1.C.R.2.3 SAMPLE 1 pCi/g 405235008-1 4.1.C.R.2.4 SA!'vlPLE 1 pCi/g 405235009-1 4.1.D.R.l.3 SAMPLE 1 pCi/g 405235010-1 4.1.D.R.1.4 SAMPLE 1 pCi/g 405235011-1 SAMPLE 1 pCi/g 405235012-1 4.1.D.R.2.4 SA!l-IPLE 1 pCi/g 405235013-1 4.2A.R.2.3 SAMPLE 1 pCi/g 405235014-1 4.2A.R.1.3 SAMPLE 1 pCi/g 405235015-1 4.2A.R.1.4 SAMPLE 1 pCi/g 405235016-1 4.2A.R.2.4 SA!'vlPLE 1 pCi/g 405235017-1 4.2A.R.3.2 SAMPLE 1 pCi/g 405235018-1 4.2A.R.4.2 SAMPLE 1 pCi/g 405235019-1 4.2B.R.2.4 SA!\IPLE 1 pCi/g 405235020-1 4.2B.R.1.4 SAMPLE 1 pCi/g 1203621691-1 11-IB for batch 1596389 l\IB 1 pCi/g 1203621692-1 4.l.B.R.1.2(405235001DUP) DUP 1 pCilg 1203621693-1 LCS for batch 1596389 LCS 1 pCi/g Matrix Client SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWC001 SOIL MJWCOOl SOIL MJWCOOl. SOIL MJWCOOl SOIL MJWC001 SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL QC ACCOUNT Collection Date 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 02-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 10-DEC-15 Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Am: Witness: q-Ue-tu. wet@?i> u Label Aliquot # i10 Det# "Z-\ !o. Soq 12 ! Choose SOP used: G@;\D-A-OIU Solid Sample Dissolution by: LEACH Circle One Data Reviewed By: 1 A1l 'l/3d1 i,. GEL Laboratories LLC, Radwchemistry Division Page 1 of 1 BATCH NUMBER : 1596389 SAMPLE ID : T0405235001_UU SAMPLE QTY : 0.501 G +/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 124 DETECTOR S/N : 80053 AVERAGE %EFFICIENCY : 24.5380 AVERAGE %EFF ERROR : 0.4761 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B124.CNF;1160 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 85.0 +/-8.354 % COUNT DATE : 29-Sep-2016 09:20:35 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W124.CNF;300 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.507 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1620E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 682.27 -0.92 PEAK NET2 3.52 253.28 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5325.56 4.955 U-3/4 4763.02 4761.15 19.818 U-235 4391.00 4483.59 49.669 U-238 4184.73 4194.27 57.803 IJ-2J8*3974-4Z84keV 61 U-235:431Q-4581keV U-3/4:4592-4865keV 55 U-23Z:S000..539BkeV 49 43 rii 37 I-31 z ;::) 25 0 19 .0 13 *:;; u 7 <{ l I I 23 77 2775 3177 3583 3!92 405 Energy (keV) 11.1230 dpm 4483.59 4408.48 4.6537 dpm 5325.56 5326.36 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 1.000 -0.920 1.920 1.3856 100.000 50.000 48.320 1.680 1.2961 100.000 4.000 3.520 0.480 0.6928 99.700 61.000 60.760 0.240 0.4899 100.000 .J I I I I I I 48: 1 5241 5665 6092 6523 6958 ACTIVITY pCi/G -1.34E-02 7.98E-01 5.83E-02 1.00E+OO I 7396 1.96-sigma TPU pCi/G 4.55E-02 2.68E-01 7.45E-02 3.06E-01 NOTES: MDA pCi/G 1.18E-01 1.28E-01 9.18E-02 7.92E-02 104.156 N/A 85.741 1.0081 Le pCi/G 3.71E-02 3.92E-02 2.10E-02 1.48E-02 1.96-sigma cnt Unc pCi/G 4.54E-02 2.32E-01 7.39E-02 2.55E-01 *Results are a compilation of S0405235001_UU and T0405235001_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235001_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G +/-0.200 % CHAMBER : 007 DETECTOR S/N : 50-066Z1 AVERAGE %EFFICIENCY : 26.6641 AVERAGE %EFF ERROR : 0.5164 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 85.7 +/-7.045 % TRACER .1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.9901 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5326.36 U-3/4 4763.02 4777.74 U-235 4391.00 4408.48 U-238 4184.73 4216.76 -U 230* 3974-4284 keV U-235; 431G4581 keV 28 -u-3/4:4592-4865kaV U-232: 5000-5398 keV 25 19 -Cii 16 I-r z 13 :J -0 10 s c-7 -*:;; u 4 c-<( 1 c-I I I I 23 74 2774 3179 3587 Energy (keV) PEAK FWHM 39.141 16.368 139.483 20.549 I 3! 98 II I I 414 COUNT DATE : 29-Sep-2016 09:13:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 254.000 253.280 0.720 0.8485 100.000 4.18E+OO 50.000 48.320 1.680 1.2961 100.000 7.92E-01 4.000 3.520 0.480 0.6928 99.700 5.79E-02 61.000 60.760 0.240 0.4899 100.000 9.96E-01 11 I I I I I I I 48 3 5256 5682 6113 6547 6985 7427 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B007.CNF;1847 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W007.CNF;505 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.92E-01 1.01E-01 2.57E-02 2.57E-01 1.27E-01 3.89E-02 7.37E-02 9.10E-02 2.09E-02 2.91E-01 7.86E-02 1.47E-02 1.96-sigma cnt Unc pCi/G 5.17E-01 2.30E-01 7.33E-02 2.53E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235002 UU SAMPLE QTY : 0.505 G -+/-0.198 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 77.6 +/-8.399 % SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 8.8071 E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 126 DETECTOR S/N : 75548 AVERAGE %EFFICIENCY : 25.0653 AVERAGE %EFF ERROR : 0.4861 COUNT DATE : 29-Sep-2016 09:20:38 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B126.CNF;1164 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W126.CNF;338 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4489.35 4515.40 4.6537 dpm 5255.93 5315.21 PEAKNET1 528.22 2.76 PEAKNET2 2.28 285.56 RECOVERY YIELD CORR. 78.942 N/A 79.190 1.0208 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5255.93 124.255 3.000 U-3/4 4763.02 4770.13 32.306 78.000 U-235 4391.00 4489.35 51.240 3.000 U-238 4184.73 4204.97 34.791 81.000 >> >> 8 U-238:3974-4284keV 55 U-235:43104581 keV U-3/4:45924865keV lJ.232:5000.5398keV 49 43 37 Yi 31 1--z 25 :::> 0 19 8 13 *:;: ti 7 <( 1 2389 2788 3192 3599 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 2.760 0.240 0.4899 100.000 5.24E-02 77.040 0.960 0.9798 100.000 1.13E+OO 2.280 0.720 0.8485 99.700 3.37E-02 79.800 1.200 1.0954 100.000 1.17E+OO 5693 6123 6558 6996 7438 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.60E-02 9.10E-02 1.70E-02 7.54E-02 3.20E-01 9.70E-02 2.64E-02 2.57E-01 5.98E-02 9.02E-02 2.29E-02 5.95E-02 3.28E-01 1.03E-01 2.95E-02 2.62E-01 NOTES: *Results are a compilation of S0405235002_UU and T0405235002_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235002 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 008 DETECTOR S/N : 78788 AVERAGE %EFFICIENCY : 32.5495 AVERAGE %EFF ERROR : 0.6275 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 79.2 +/-6.789 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.6852E+OO dpm NUCLIDE LIBRARY PEAK 'ii) I-z :J 0 *:;; ti <( ENERGY ENERGY U-232 5302.10 5315.21 U-3/4 4763.02 4768.55 U-235 4391.00 4515.40 U-238 4184.73 4194.83 U-238:3974-4284keV 33 V-235:4310-4581 keV U-3f4:4S92-4865keV lJ.232;5000-5398keV 29 25 21 17 13 9 5 2399 2792 3190 3593 Energy (keV) PEAK FWHM 34.785 53.702 141.579 67.942 COUNT DATE : 29-Sep-2016 09:13:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 293.000 285.560 7.440 2.7276 100.000 4.15E+OO 78.000 77.040 0.960 0.9798 100.000 1.11E+OO 3.000 2.280 0.720 0.8485 99.700 3.30E-02 81.000 79.800 1.200 1.0954 100.000 1.15E+OO 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B008.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W008.CNF;517 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.55E-01 1.89E-01 7.26E-02 2.95E-01 9.50E-02 2.59E-02 5.85E-02 8.83E-02 2.25E-02 3.02E-01 1.01E-01 2.89E-02 1.96-sigma cnt Unc pCi/G 4.90E-01 2.52E-01 5.83E-02 2.56E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235003 UU SAMPLE QTY : 0.501 G -+/-0.200 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 74.9 +/-8.894 % SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 6.2257E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 127 DETECTOR S/N : 78770 AVERAGE %EFFICIENCY : 26.6218 AVERAGE %EFF ERROR : 0.5155 COUNT DATE : 29-Sep-2016 09:20:41 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B127.CNF;1167 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W127.CNF;322 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4484.28 4420.30 TRACER2 1564-1 U-232 4.6537 dpm 5392.81 5324.92 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY ENERGY FWHM AREA AREA AREA S!Dev pCi/G U-232 5302.10 5392.81 4.958 1.000 -0.200 1.200 1.0954 100.000 -5.05E-03 U-3/4 4763.02 4762.91 52.888 65.000 64.280 0.720 0.8485 100.000 1.03E+OO U-235 4391.00 4484.28 28.510 4.000 3.040 0.960 0.9798 99.700 4.88E-02 U-238 4184.73 4194.26 5.757 53.000 52.760 0.240 0.4899 100.000 8.45E-01 ll ;t 46 U-238:3974-4284keV U-235:4310-4581 keV U-3/4:4592-4865keV 41 lJ.232:5000-5398keV 36 31 (ii 26 I-z 21 :J 0 16 8 11 *:;; u <( 6 2382 2781 3183 3590 4 00 414 5681 6111 6545 6982 7424 Energy (keV) 396.58 3.04 55.803 N/A -0.20 261.28 75.465 1.0081 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.60E-02 1.77E-01 5.07E-02 7.59E-02 3.15E-01 9.78E-02 2.49E-02 2.55E-01 7.29E-02 1.06E-01 2.88E-02 7.24E-02 2.76E-01 7.68E-02 1.44E-02 2.31E-01 NOTES:

Results are a compilation of S0405235003_UU and T0405235003_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000) 0 ...., Vl 00 0 \0 BATCH NUMBER : 1596389 SAMPLE ID : S0405235003 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 009 DETECTOR S/N : 72528 AVERAGE %EFFICIENCY : 31.2521 AVERAGE %EFF ERROR : 0.6030 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 75.5 +/-6.955 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.5119E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5324.92 U-3/4 4763.02 4766.09 U-235 4391.00 4420.30 U-238 4184.73 4210.95 45 U-238:3974-4264kaV U-235:431D-4581keV 41 U-3/4:4592-4865keV U-232:5000.5398keV 37 33 29 25 z 21 ::i 17 0 13 9 *;;; :g 5 <( 1 2383 2779 3180 3585 Energy (keV) PEAK FWHM 15.969 51.326 68.983 26.690 COUNT DATE : 29-Sep-2016 09:13:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 262.000 261.280 0.720 0.8485 100.000 4.18E+OO 65.000 64.280 0.720 0.8485 100.000 1.02E+OO 4.000 3.040 0.960 0.9798 99.700 4.84E-02 53.000 52.760 0.240 0.4899 100.000 8.38E-01 >> 8 5673 6104 6539 6978 7422 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B009.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W009.CNF;516 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.81E-01 9.78E-02 2.49E-02 2.92E-01 9.70E-02 2.47E-02 7.21E-02 1.05E-01 2.86E-02 2.58E-01 7.62E-02 1.43E-02 1.96-sigma cnt Unc pCi/G 5.09E-01 2.53E-01 7.18E-02 2.29E-01

"" ('1> 0 '"" BATCH NUMBER : 1596389 SAMPLE ID : T0405235004 UU g SAMPLE QTY : 0.502 G -+/-0.199 % SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 62.9 +/-9.119 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 8.5003E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 128 DETECTOR S/N : 75549 AVERAGE %EFFICIENCY : 26.0039 AVERAGE %EFF ERROR : 0.5038 COUNT DATE : 29-Sep-2016 09:20:43 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B128.CNF;1171 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W128.CNF;324 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4492.37 4533.08 4.6538 dpm 5283.87 5320.97 PEAK NET 1 528.91 -0.44 PEAKNET2 3.76 216.40 RECOVERY YIELD CORR. 76.192 N/A 63.379 1.0082 NUCLIDE LIBRARY PEAK ii> I-z :J 0 8 *:;: n <t: ENERGY ENERGY U-232 5302.10 5283.87 U-3/4 4763.02 4772.96 U-235 4391.00 4492.37 U-238 4184.73 4190.26 51 U*238: 3974-4284 keV U-235:4310-4581 keV U-3/4:4592-4a6SkeV 46 lJ..232:5000-SJSSkeV 41 36 31 26 21 16 11 6 2400 2797 3198 3603 Energy (keV) PEAK GROSS FWHM AREA 4.935 1.000 6.854 46.000 36.050 4.000 36.640 58.000 >> ::! i 8 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G -0.440 1.440 1.2000 100.000 -8.35E-03 44.320 1.680 1.2961 100.000 8.55E-01 3.760 0.240 0.4899 99.700 7.28E-02 57.520 0.480 0.6928 100.000 1.11E+OO 6117 6550 6987 7429 1.96-sigma 1.96-sigma TPU MDA Le en! Une pCi/G pCi/G pCi/G pCi/G 5.78E-02 1.40E-01 4.17E-02 5.77E-02 3.04E-01 1.50E-01 4.58E-02 2.61E-01 8.68E-02 9.28E-02 1.74E-02 8.58E-02 3.55E-01 1.07E-01 2.45E-02 2.91E-01 NOTES:

Results are a compilation of S0405235004_UU and T0405235004_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235004 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 010 DETECTOR S/N : 72529 AVERAGE %EFFICIENCY : 30.8196 AVERAGE %EFF ERROR : 0.5949 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 63.4 +/-7.668 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6538E+OO dpm 2.9495E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5320.97 U-3/4 4763.02 4769.50 U-235 4391.00 4533.08 U-238 4184.73 4187.60 23 U-238: 3974-4284 keV U-235:431CJ.4581keV 21 U-3/4:4592-4865keV U-232:5000-5398keV 19 17 15 en 13 I-11 z :::> 9 0 7 5 u 3 <( 2411 2807 3206 Energy (keV) PEAK FWHM 49.721 60.854 83.598 36.062 COUNT DATE : 29-Sep-2016 09:13:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 226.000 216.400 9.600 3.0984 100.000 4.18E+OO 46.000 44.320 1.680 1.2961 100.000 8.48E-01 4.000 3.760 0.240 0.4899 99.700 7.22E-02 58.000 57.520 0.480 0.6928 100.000 1.10E+OO 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B010.CNF;1843 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W01 O.CNF;513 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.64E-01 2.77E-01 1.10E-01 2.90E-01 1.48E-01 4.54E-02 8.58E-02 9.21E-02 1.72E-02 3.35E-01 1.06E-01 2.43E-02 1.96-sigma cnt Unc pCi/G 5.73E-01 2.58E-01 8.51E-02 2.89E-01 AlphaSpeetroscopySoftwareVersion3.5.3 effectivedate:02-Mar*2015 BATCH NUMBER : 1596389 SAMPLE ID : T0405235005 UU SAMPLE QTY : 0.503 G -+/-0.199 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 77.8 +/-8.038 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1177E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 131 DETECTOR S/N : 80008 AVERAGE %EFFICIENCY : 25.5970 AVERAGE %EFF ERROR : 0.4961 COUNT DATE : 29-Sep-2016 09:41 :50 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B131.CNF;1162 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W131.CNF;319 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAK NETZ RECOVERY YIELD CORR. TRACER 1 TRACER2 NUCLIDE LIBRARY 0' z ::> 0 s c *:;; U-232 U-3/4 U-235 U-238 64 57 50 43 36 29 22 15 8 1 23 ENERGY 5302.10 4763.02 4391.00 4184.73 lJ.238* 3974-4284 keV U-235:43104581 keV lJ.3/4:4592-4865keV U-232:5000-5398keV --

I 79 2778 3181 Energy (keV) 1570-E U-235 11.1230 dpm 4482.43 4471.19 1564-1 U-232 4.6537 dpm 5374.11 5314.87 NUCLIDE ACTIVITY SUMMARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY FWHM AREA AREA AREA S!Dev 5374.11 4.960 1.000 -0.920 1.920 1.3856 100.000 4763.59 37.198 67.000 65.800 1.200 1.0954 100.000 4482.43 42.948 4.000 3.520 0.480 0.6928 99.700 4190.71 57.243 54.000 53.760 0.240 0.4899 100.000 ,,Jj, .** I I I I I I 3587 3!97 412 48 0 5252 5678 6108 6542 6979 -ACTIVITY pCi/G -1.34E-02 9.22E-01 4.95E-02 7.54E-01 I 7421 684.57 3.52 100.184 N/A -0.92 297.28 78.406 1.0081 1.96-sigma 1.96-sigma TPU MDA Le en! Unc pCi/G pCi/G pCi/G pCi/G 4.52E-02 1.17E-01 3.69E-02 4.52E-02 2.72E-01 9.83E-02 2.81E-02 2.27E-01 6.32E-02 7.79E-02 1.78E-02 6.27E-02 2.38E-01 6.72E-02 1.26E-02 2.04E-01 NOTES: *Results are a compilation of S0405235005_UU and T0405235005_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235005 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 013 DETECTOR S/N : 78790 AVERAGE %EFFICIENCY : 34.2243 AVERAGE %EFF ERROR : 0.6594 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 78.4 +/-6.671 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.6487E+OO dpm NUCLIDE LIBRARY PEAK Cii 1--z :J 0 *::; t5 <I: ENERGY ENERGY U-232 5302.10 5314.87 U-3/4 4763.02 4767.88 U-235 4391.00 4471.19 U-238 4184.73 4196.71 U-238: 3974-4264 keV 37 U-235:4310-4581 keV U-314:4592-4865keV lJ.232:5000-5398keV 33 29 25 21 17 13 9 5 2388 2785 3187 3593 Energy (keV) PEAK FWHM 21.172 41.162 143.242 42.973 COUNT DATE : 29-Sep-2016 09:13:19 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 304.000 297.280 6.720 2.5923 100.000 4.17E+OO 67.000 65.800 1.200 1.0954 100.000 9.15E-01 4.000 3.520 0.480 0.6928 99.700 4.91E-02 54.000 53.760 0.240 0.4899 100.000 7.48E-01 6555 6995 7440 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B013.CNF;1815 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W013.CNF;515 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.44E-01 1.75E-01 6.66E-02 2.57E-01 9.75E-02 2.79E-02 6.25E-02 7.72E-02 1.77E-02 2.26E-01 6.67E-02 1.25E-02 1.96-sigma cnt Unc pCi/G 4.81E-01 2.25E-01 6.22E-02 2.02E-01 AlphaSpeclroscopySoltwa!eVersion3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596389 SAMPLE ID : T0405235006 UU SAMPLE QTY : 0.501 G -+/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 132 DETECTOR S/N : 67579 AVERAGE %EFFICIENCY : 26.0712 AVERAGE %EFF ERROR : 0.5050 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B132.CNF;1158 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 71.7 +/-8.282 % COUNT DATE : 29-Sep-2016 09:20:46 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W132.CNF;324 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1304E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 705.20 1.04 PEAK NET2 4.52 265.04 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5309.95 163.020 U-3/4 4763.02 4774.19 65.043 U-235 4391.00 4493.00 42.607 U-238 4184.73 4199.98 41.743 64 U 238* 3974-4284 keV =U-235:4310-45B1keV U-3/4:4592-4865keV 57 _U-232:500G-539BkeV 50 (ii 36 I-z 29 :::i 0 22 8 15 *:;; ts 8 <l: I "j ,,,j I ' I 23 82 2780 3180 3585 3!94 406 Energy (keV) . ' 11.1230 dpm 4493.00 4418.23 4.6537 dpm 5309.95 5317.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 2.000 1.040 0.960 0.9798 100.000 50.000 48.080 1.920 1.3856 100.000 5.000 4.520 0.480 0.6928 99.700 59.000 58.280 0.720 0.8485 100.000 8 ,ii ' I 48 2 5241 5665 6092 6523 6958 -ACTIVITY pCi/G 1.47E-02 7.62E-01 7.18E-02 9.23E-01 ' 7396 1.96-sigma TPU pCi/G 5.02E-02 2.57E-01 7.83E-02 2.86E-01 NOTES: MDA pCi/G 9.29E-02 1.28E-01 8.80E-02 9.68E-02 101.326 N/A 72.537 1.0116 Le pCi/G 2.53E-02 4.02E-02 2.02E-02 2.46E-02 1.96-sigma cnt Unc pCi/G 5.01E-02 2.23E-01 7.74E-02 2.41E-01 *Results are a compilation of S0405235006_UU and T0405235006_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235006 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 014 DETECTOR S/N : 83289 AVERAGE %EFFICIENCY : 32.9813 AVERAGE %EFF ERROR : 0.6357 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 . % YIELD : 72.5 +/-6.994 % TRACER 1564-1 ' ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.3756E+OO dpm NUCLIDE LIBRARY PEAK Ui I-z => 0 *:;; ENERGY ENERGY U-232 5302.10 5317.00 U-3/4 4763.02 4768.91 U-235 4391.00 4418.23 U-238 4184.73 4202.89 lJ..238:3974-4284keV 31 lJ..235:4310-4581keV U*314:4592-4B65keV U-232: 5000-5398 keV 28 25 22 19 16 13 10 7 4 2374 2771 3173 3578 Energy (keV) PEAK FWHM 53.769 23.029 54.283 29.198 COUNT DATE : 29-Sep-2016 09:13:19 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 272.000 265.040 6.960 2.6382 100.000 4.18E+OO 50.000 48.080 1.920 1.3856 100.000 7.53E-01 5.000 4.520 0.480 0.6928 99.700 7.10E-02 59.000 58.280 0.720 0.8485 100.000 9.13E-01 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B014.CNF;1816 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W014.CNF;525 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.86E-01 2.00E-01 7.63E-02 2.45E-01 1.26E-01 3.97E-02 7.71E-02 8.70E-02 1.99E-02 2.71E-01 9.57E-02 2.43E-02 1.96-sigma cnt Unc pCi/G 5.13E-01 2.20E-01 7.65E-02 2.38E-01 Alpha Spectroscopy Software Version 3,5,3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596389 SAMPLE ID : T0405235007 UU SAMPLE QTY : 0.501 G -+/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 133 DETECTOR S/N : 76229 AVERAGE %EFFICIENCY : 25.5293 AVERAGE %EFF ERROR : 0.4948 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B133.CNF;1155 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 90.3 +/-7.833 % COUNT DATE : 29-Sep-2016 09:20:48 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W133.CNF;359 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0530E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 643.27 1.28 PEAKNET2 6.76 334.72 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5213.40 218.623 U-3/4 4763.02 4754.46 51.550 U-235 4391.00 4477.41 61.122 U-238 4184.73 4175.58 39.750 ll ;z e lJ.238: 3974-4284 keV 55 U-235:4310-4581 keV U*314:4592-4865keV U-232:5000-5398keV 49 43 37 (jJ 31 I-z 25 ::i 0 19 .?;> 13 *:;; u 7 <( 2363 2763 3166 3573 3 83 397 Energy (keV) 11.1230 dpm 4477.41 4492.86 4.6537 dpm 5213.40 5309.66 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA S!Dev 2.000 1.280 0.720 0.8485 100.000 59.000 58.040 0.960 0.9798 100.000 7.000 6.760 0.240 0.4899 99.700 74.000 74.000 0.000 0.0000 100.000 > 8 48 5 5237 5663 6092 6525 6961 ACTIVITY pCi/G 1.99E-02 7.29E-01 8.52E-02 9.29E-01 7402 1.96-sigma TPU pCi/G 5.50E-02 2.23E-01 7.16E-02 2.59E-01 NOTES: MDA pCi/G 9.52E-02 8.28E-02 6.04E-02 3.77E-02 94.389 N/A 91.448 1.0129 Le pCi/G 2.42E-02 2.25E-02 1.13E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.49E-02 1.91E-01 7.03E-02 2.13E-01

Results are a compilation of S0405235007 _UU and T0405235007 _UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

Alpha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar*2015 BATCH NUMBER : 1596389 SAMPLE ID : S0405235007 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 015 DETECTOR S/N : 80055 AVERAGE %EFFICIENCY : 33.0386 AVERAGE %EFF ERROR : 0.6369 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 91.4 +/-6.353 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 4.2557E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5309.66 U-3/4 4763.02 4753.74 U-235 4391.00 4492.86 U-238 4184.73 4185.41 lJ.238:3974-4284keV 37 U-235:4310-4561 keV lJ.31'4:4592-4865keV 33 U-232:5000-539BkeV 29 25 Ci) 21 I-z 17 :J 0 13 S?.. 9 *s: ti 5 <( 1 2387 2783 3184 3589 Energy (keV) PEAK FWHM 21.461 57.136 0.000 126.833 COUNT DATE : 29-Sep-2016 09:13:19 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 340.000 334.720 5.280 2.2978 100.000 4.18E+OO 59.000 58.040 0.960 0.9798 100.000 7.20E-01 7.000 6.760 0.240 0.4899 99.700 8.41E-02 74.000 74.000 0.000 0.0000 100.000 9.18E-01 7438 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B015.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W015.CNF;532 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.09E-01 1.43E-01 5.26E-02 2.11E-01 8.17E-02 2.23E-02 7.03E-02 5.96E-02 1.12E-02 2.42E-01 3.72E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.53E-01 1.89E-01 6.94E-02 2.11E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235008 UU SAMPLE QTY : 0.503 G -+/-0.199 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 88.4 +/-7.767 % SECONDARY QTY : 0.502 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1689E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 134 DETECTOR S/N : 76230 AVERAGE %EFFICIENCY : 25.7389 AVERAGE %EFF ERROR : 0.4988 COUNT DATE : 29-Sep-2016 09:20:50 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B134.CNF;1151 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W134.CNF;336 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4488.82 4424.15 4.6537 dpm 5198.58 5311.51 PEAKNET1 719.92 -0.96 PEAK NET2 2.04 332.60 RECOVERY YIELD CORR. 104.776 N/A 89.095 1.0081 NUCLIDE LIBRARY PEAK en I-z :J 0 s *:;: u <{ ENERGY ENERGY U-232 5302.10 5198.58 U-3/4 4763.02 4762.28 U-235 4391.00 4488.82 U-238 4184.73 4199.23 U-238:3974-4284keV 64 U-235: 4310-4581 keV U-3/4:4592-486SkeV 57 U-232:5000-5398keV 50 43 36 29 22 15 8 2387 2786 3188 3594 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 57.042 84.000 47.503 3.000 69.856 65.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.960 0.960 0.9798 100.000 -1.34E-02 81.840 2.160 1.4697 100.000 1.03E+OO 2.040 0.960 0.9798 99.700 2.56E-02 64.520 0.480 0.6928 100.000 8.08E-01 5679 6107 6539 6974 7413 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 3.12E-02 9.21E-02 2.51E-02 3.11E-02 2.78E-01 1.05E-01 3.37E-02 2.27E-01 5.12E-02 8.28E-02 2.26E-02 5.10E-02 2.37E-01 6.94E-02 1.59E-02 2.00E-01 NOTES:

Results are a compilation of S0405235008_UU and T0405235008_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000) 0 ...,, u. 00 0 \0 AlphaSpectrcscopySoflwareVerslon3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596389 SAMPLE ID : S0405235008 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 016 DETECTOR S/N : 78774 AVERAGE %EFFICIENCY : 33.6964 AVERAGE %EFF ERROR : 0.6491 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 89.1 +/-6.396 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 4.1462E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5311.51 U-3/4 4763.02 4764.93 U-235 4391.00 4424.15 U-238 4184.73 4185.76 34 U-238: 3974-4284 keV U-235:431D-4581 keV 31 U-3/4:4592-4865keV U-232:5()()().5398keV 28 25 22 0' 19 z 16 => 13 0 10 .?;> 7 u 4 <i:: 2401 2795 3194 3598 Energy (keV) PEAK FWHM 54.054 16.327 14.694 56.328 COUNT DATE : 29-Sep-2016 09:13:19 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA S!Dev pCi/G 341.000 332.600 8.400 2.8983 100.000 4.17E+OO 84.000 81.840 2.160 1.4697 100.000 1.02E+OO 3.000 2.040 0.960 0.9798 99.700 2.54E-02 65.000 64.520 0.480 0.6928 100.000 8.02E-01 7441 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B016.CNF;1811 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W016.CNF;496 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.11E-01 1.71E-01 6.65E-02 2.62E-01 1.04E-01 3.35E-02 5.07E-02 8.21E-02 2.24E-02 2.24E-01 6.88E-02 1.58E-02 1.96-sigma cnt Unc pCi/G 4.56E-01 2.25E-01 5.06E-02 1.98E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235009 UU SAMPLE QTY : 0.504 G -+/-0.198 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 69.1 +/-8.715 % SECONDARY QTY : 0.500 G +/-0.200 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0975E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 139 DETECTOR S/N : 76231 AVERAGE %EFFICIENCY : 24.8887 AVERAGE %EFF ERROR : 0.4828 COUNT DATE : 29-Sep-2016 09:20:52 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B139.CNF;1109 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W139.CNF;334 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4490.43 4379.56 4.6537 dpm 5253.47 5307.67 PEAK NET 1 653.63 -0.44 PEAKNET2 1.80 229.00 RECOVERY YIELD CORR. 98.378 N/A 69.702 1.0081 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5253.47 4.936 1.000 U-3/4 4763.02 4774.42 46.484 70.000 U-235 4391.00 4490.43 37.177 3.000 U-238 4184.73 4207.00 24.682 46.000 > .ll 8 U-238;3974-4284keV 71 U-235: 43104561 keV U-3/4:4592-4865keV 64 U-232:5000-5398keV 57 50 (j) 43 1--36 z ::i 29 0 22 15 *:;; u 8 <l'. 2388 2785 3186 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.440 1.440 1.2000 100.000 -6.80E-03 67.840 2.160 1.4697 100.000 1.23E+OO 1.800 1.200 1.0954 99.700 3.28E-02 45.040 0.960 0.9798 100.000 8.18E-01 5679 6109 6543 6981 7423 1.96-sigma TPU pCi/G 4.70E-02 3.70E-01 7.47E-02 2.84E-01 NOTES: MDA pCi/G 1.14E-01 1.52E-01 1.28E-01 1.20E-01 Le pCi/G 3.40E-02 4.89E-02 3.66E-02 3.26E-02 1.96-sigma cnt Unc pCi/G 4.70E-02 3.01E-01 7.44E-02 2.45E-01
Results are a compilation of S0405235009_UU and T0405235009_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235009 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 017 DETECTOR S/N : 78791 AVERAGE %EFFICIENCY : 29.6554 AVERAGE %EFF ERROR : 0.5728 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 69.7 +/-7.424 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.2437E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5307.67 U-3/4 4763.02 4761.58 U-235 4391.00 4379.56 U-238 4184.73 4182.80 28 U-238: 3974-4284 keV lJ.235:4310-4581 keV 25 U-3/4:4592-4865keV U-232:5000-5398keV 22 19 'Ci) 16 I-13 z => 0 10 £ 7 4 0 <l'. PEAK FWHM 54.660 28.429 64.273 30.159 COUNT DATE : 29-Sep-2016 09:13:19 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 235.000 229.000 6.000 2.4495 100.000 4.16E+OO 70.000 67.840 2.160 1.4697 100.000 1.22E+OO 3.000 1.800 1.200 1.0954 99.700 3.25E-02 46.000 45.040 0.960 0.9798 100.000 8.11E-01 > ! ; 2381 2779 3181 3587 3 98 413 48 2 5255 5682 6114 6550 6990 7435 Energy (keV) !l; !l; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B017.CNF;2657 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W017.CNF;1452 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.32E-01 2.17E-01 8.15E-02 3.51E-01 1.51E-01 4.85E-02 7.40E-02 1.27E-01 3.63E-02 2.72E-01 1.19E-01 3.23E-02 1.96-sigma cnt Unc pCi/G 5.49E-01 2.99E-01 7.38E-02 2.43E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235010 UU SAMPLE QTY : 0.501 G -+/-0.200 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 86.8 +/-8.074 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.7129E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 140 DETECTOR S/N : 78771 AVERAGE %EFFICIENCY : 26.0317 AVERAGE %EFF ERROR : 0.5043 COUNT DATE : 29-Sep-2016 09:20:55 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B140.CNF;1102 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W140.CNF;283 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4495.55 4384.79 4.6537 dpm 5361.06 5306.47 PEAK NET 1 605.00 1.04 PEAKNET2 3.28 306.44 RECOVERY YIELD CORR. 87.061 NIA 87.881 1.0122 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5361.06 44.575 2.000 U-3/4 4763.02 4767.70 58.608 55.000 U-235 4391.00 4495.55 30.407 4.000 U-238 4184.73 4199.51 58.608 73.000 ll ll ii 71 U-238;3974-4284keV U-235: 431o-4581 keV 64 U.3/4:4592-4865keV U-232:5000.5398keV 57 50 43 36 z :::i 29 0 22 c 15 *;;: t5 8 <!'. 1 2385 2784 3186 3592 4 02 Energy (keV) ll NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G 1.040 0.960 0.9798 100.000 1.71E-02 54.040 0.960 0.9798 100.000 7.41E-01 3.280 0.720 0.8485 99.700 4.51E-02 72.040 0.960 0.9798 100.000 9.88E-01 6110 6543 6981 7422 1.96-sigma TPU pCi/G 5.85E-02 2.35E-01 6.21E-02 2.82E-01 NOTES: MDA pCi/G 1.08E-01 9.03E-02 8.40E-02 9.03E-02 Le pCi/G 2.95E-02 2.46E-02 2.14E-02 2.46E-02 1.96-sigma en! Une pCi/G 5.84E-02 2.02E-01 6.16E-02 2.32E-01 *Results are a compilation of S0405235010_UU and T0405235010_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235010 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 018 DETECTOR S/N : 78782 AVERAGE %EFFICIENCY : 31.4751 AVERAGE %EFF ERROR : 0.6072 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 87.9 +/-6.569 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 4.0897E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5306.47 U-3/4 4763.02 4758.01 U-23S 4391.00 4384.79 U-238 4184.73 4194.40 31 U-238: 39744284 keV IJ.235:4310-4581keV 28 U-3J4:4592-4865keV U-232:5000..5398keV 25 22 19 & 16 1--z 13 ::i 0 10 7 *s; <l'. 4 1 2380 2776 3177 3582 Energy (keV) PEAK FWHM 66.176 44.286 4.921 41.006 COUNT DATE : 29-Sep-2016 09:13:19 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 311.000 306.440 4.560 2.1354 100.000 4.18E+OO 55.000 54.040 0.960 0.9798 100.000 7.32E-01 4.000 3.280 0.720 0.8485 99.700 4.46E-02 73.000 72.040 0.960 0.9798 100.000 9.76E-01 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B018.CNF;1812 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W018.CNF;486 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.35E-01 1.48E-01 5.34E-02 2.22E-01 8.92E-02 2.43E-02 6.12E-02 8.30E-02 2.11E-02 2.64E-01 8.92E-02 2.43E-02 1.96-sigma cnt Unc pCi/G 4.74E-01 1.99E-01 6.09E-02 2.29E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235011_UU SAMPLE QTY : 0.500 G +/-0.200 % SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 73.1 +/-8.368 % SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1432E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 142 DETECTOR S/N : 42285 AVERAGE %EFFICIENCY : 26.5347 AVERAGE %EFF ERROR : 0.5139 COUNT DATE : 29-Sep-2016 09:20:58 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B142.CNF;1102 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W142.CNF;306 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4493.76 4497.15 4.6538 dpm 5283.21 5316.88 PEAK NET 1 725.87 0.52 PEAKNET2 4.28 253.80 RECOVERY YIELD CORR. 102.474 N/A 73.813 1.0099 NUCLIDE LIBRARY PEAK Ui I-z :J 0 s 1:-*;;; t5 <I: ENERGY ENERGY U-232 5302.10 5283.21 U-3/4 4763.02 4778.35 U-235 4391.00 4493.76 U-238 4184.73 4208.58 U-238:3974-4284keV U-235:4310-4581 keV 55 U-3r'4: 45924865 keV U-232:5000-539akeV 49 43 37 31 25 19 13 7 2382 2780 3181 3586 Energy (keV) PEAK GROSS FWHM AREA 4.944 1.000 66.747 50.000 59.692 5.000 49.796 50.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.520 0.480 0.6928 100.000 7.18E-03 49.520 0.480 0.6928 100.000 8.19E-01 4.280 0.720 0.8485 99.700 7.10E-02 49.760 0.240 0.4899 100.000 8.23E-01 5664 6091 6521 6955 7393 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCVG pCVG pCVG pCi/G 4.00E-02 7.65E-02 1.75E-02 3.99E-02 2.70E-01 9.16E-02 2.10E-02 2.32E-01 8.21E-02 1.01E-01 2.58E-02 8.12E-02 2.70E-01 7.93E-02 1.48E-02 2.32E-01 NOTES: *Results are a compilation of S0405235011_UU and T0405235011_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235011_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G +/-0.200 % CHAMBER : 020 DETECTOR S/N : 78787 AVERAGE %EFFICIENCY : 31.0365 AVERAGE %EFF ERROR : 0.5989 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 73.8 +/-7.125 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6538E+OO dpm 3.4351 E+OO dpm NUCLIDE LIBRARY PEAK ii) f-z ::i 0 .2:-*:; <l'. ENERGY ENERGY U-232 5302.10 5316.88 U-3/4 4763.02 4768.48 U-235 4391.00 4497.15 U-238 4184.73 4201.17 U-238: 3974-4284 keV 21 U-235: 4310-4SB1 keV U-3/4:4592-4865keV 19 lJ..232:5000-5398keV 17 15 13 11 9 7 5 3 2407 2804 3204 3608 Energy (keV) PEAK FWHM 66.928 7.611 4.933 69.066 COUNT DATE : 29-Sep-2016 09:13:20 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 261.000 253.800 7.200 2.6833 100.000 4.19E+OO 50.000 49.520 0.480 0.6928 100.000 8.11E-01 5.000 4.280 0.720 0.8485 99.700 7.03E-02 50.000 49.760 0.240 0.4899 100.000 8.15E-01 7410 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B020.CNF;1833 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W020.CNF;562 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.03E-01 2.12E-01 8.12E-02 2.58E-01 9.07E-02 2.08E-02 8.10E-02 1.00E-01 2.55E-02 2.58E-01 7.86E-02 1.47E-02 1.96-sigma cnt Unc pCi/G 5.26E-01 2.30E-01 8.04E-02 2.30E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235012 UU SAMPLE QTY : 0.506 G -+/-0.198 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 85.9 +/-7.945 % SECONDARY QTY : 0.505 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.201 OE+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 143 DETECTOR SIN : 65882 AVERAGE %EFFICIENCY : 22.7820 AVERAGE %EFF ERROR : 0.4430 COUNT DATE : 29-Sep-2016 09:21:00 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B143.CNF;1098 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W143.CNF;291 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4496.13 4452.21 4.6537 dpm 5232.76 5299.44 PEAKNET1 654.72 3.52 PEAKNET2 6.80 311.88 RECOVERY YIELD CORR. 107.655 N/A 87.718 1.0211 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5232.76 285.047 4.000 U-3/4 4763.02 4786.60 18.722 60.000 U-235 4391.00 4496.13 52.385 8.000 U-238 4184.73 4208.30 46.279 65.000 61 lJ.238:3974-4284keV U-235:4310-4581 keV 55 lJ.3/4:4592-4865keV U-232:5000-5398keV 49 43 37 (ii 31 I-z ::::> 25 0 S?. 19 13 *s: 7 2372 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 3.520 0.480 0.6928 100.000 5.38E-02 59.280 0.720 0.8485 100.000 7.98E-01 6.800 1.200 1.0954 99.700 9.18E-02 64.760 0.240 0.4899 100.000 8.71E-01 5629 6051 6478 6907 7340 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 6.86E-02 8.46E-02 1.94E-02 6.81E-02 2.43E-01 8.22E-02 2.09E-02 2.06E-01 8.22E-02 9.46E-02 2.71E-02 8.09E-02 2.56E-01 6.45E-02 1.21E-02 2.14E-01 NOTES: *Results are a compilation of S0405235012_UU and T0405235012_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235012 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 021 DETECTOR SIN : 795159 AVERAGE %EFFICIENCY : 32.0933 AVERAGE %EFF ERROR : 0.6189 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 87.7 +/-6.510 % TRACER ,1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 4.0821 E+OO dpm NUCLIDE LIBRARY PEAK Ui f-z ::::> 0 s *:;; ti <( ENERGY ENERGY U-232 5302.10 5299.44 U-3/4 4763.02 4759.82 U-235 4391.00 4452.21 U-238 4184.73 4184.97 28 U-238:3974-4284keV U-235:4310-4581keV 25 U-3/4:4592-4865keV U-232: 5000.5398 keV 22 19 16 13 10 7 4 2395 2789 3188 3591 Energy (keV) PEAK FWHM 64.241 29.407 220.556 26.140 COUNT DATE : 29-Sep-2016 09:13:20 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 315.000 311.880 3.120 1.7664 100.000 4.14E+OO 60.000 59.280 0.720 0.8485 100.000 7.81E-01 8.000 6.800 1.200 1.0954 99.700 8.99E-02 65.000 64.760 0.240 0.4899 100,000 8.53E-01 7416 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B021.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W021.CNF;539 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.20E-01 1.26E-01, 4.30E-02 2.27E-01 8.05E-02 2.05E-02 8.01E-02 9.27E-02 2.65E-02 2.39E-01 6.32E-02 1.18E-02 1.96-sigma cnt Unc pCi/G 4.63E-01 2.02E-01 7.92E-02 2.10E-01 'i:I (1) -l>-0\ Alpha Spectroscopy Softwafe Version 3.5.3 O effecllvedate:02-Mar-2015 0 ....., BATCH NUMBER : 1596389 SAMPLE ID : T0405235013 UU g SAMPLE QTY : 0.500 G -+/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 144 DETECTOR S/N : 75551 AVERAGE %EFFICIENCY : 26.3153 AVERAGE %EFF ERROR : 0.5097 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B144.CNF;1103 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 89.2 +/-7.944 % COUNT DATE : 29-Sep-2016 09:21 :03 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W144.CNF;297 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.502 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1893E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U-238: 3974-4254 keV 64 U-2JS:431o-4581keV U-3/4:4592-4865keV U-232:5000.5398keV 57 50 43 en 36 I-z 29 => 0 £ 22 a 15 0 8 <( 2389 2784 3183 Energy (keV) ID 1570-E 1564-1 PEAK ENERGY 5310.72 4762.56 4485.04 4193.61 3586 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 748.90 0.76 PEAKNET2 4.52 293.32 RECOVERY YIELD CORR. 11.1230 dpm 4485.04 4432.63 4.6539 dpm 5310.72 5313.74 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA StDev 4.914 1.000 0.760 0.240 0.4899 100.000 56.678 56.000 54.320 1.680 1.2961 100.000 47.987 5.000 4.520 0.480 0.6928 99.700 51.437 54.000 52.320 1.680 1.2961 100.000 :! 8 m 48 8 5237 5660 6086 6517 6951 :l ACTIVITY pCi/G 1.02E-02 7.78E-01 6.50E-02 7.50E-01 7389 1.96-sigma TPU pCi/G 3.84E-02 2.47E-01 7.08E-02 2.41E-01 NOTES: MDA pCi/G 6.44E-02 1.11E-01 7.96E-02 1.11E-01 106.607 N/A 90.160 1.0106 Le pCi/G 1.21E-02 3.40E-02 1.82E-02 3.40E-02 1.96-sigma cnt Unc pCi/G 3.83E-02 2.13E-01 7.00E-02 2.09E-01 *Results are a compilation of S0405235013_UU and T0405235013_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235013 UU SAMPLE QTY : 0.500 G -+/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 023 DETECTOR S/N : 78264 AVERAGE %EFFICIENCY : 29.3659 AVERAGE %EFF ERROR : 0.5674 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.2 +/-6.654 % COUNT DATE : 29-Sep-2016 09:13:20 ELAPSED LIVE TIME(SEC) : 14399.99 TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 4.1960E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5313.74 U-3/4 4763.02 4767.78 U-235 4391.00 4432.63 U-238 4184.73 4206.23 U 238* 3974-4284 keV 33 lJ.235:4310-4581keV ._U-3/4:45924865keV U-232:SOQ0..5398keV 29 r 25 r Ci) 21 r I-17 z r :::> 0 13 r £ c 9 r *;;: ti 5 I-<( r I Ill I I I I I I 23 80 2777 3179 3586 Energy (keV) PEAK GROSS FWHM AREA 55.353 295.000 14.110 56.000 163.146 5.000 34.298 54.000 I j 111 I ,,,,I I 31 97 412 48 1 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 293.320 1.680 1.2961 100.000 4.19E+OO 54.320 1.680 1.2961 100.000 7.70E-01 4.520 0.480 0.6928 99.700 6.43E-02 52.320 1.680 1.2961 100.000 7.42E-01 g I 1 .... 1 I I I I I I 5255 5683 6116 6553 6994 7440 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B023.CNF;1854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W023.CNF;546 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.46E-01 1.11E-01 3.39E-02 2.35E-01 1.10E-01 3.37E-02 6.98E-02 7.88E-02 1.80E-02 2.30E-01 1.10E-01 3.37E-02 1.96-sigma cnt Unc pCi/G 4.82E-01 2.11E-01 6.92E-02 2.07E-01 "" 0 .!>. Rj Version 3.5.3 0 '"" BATCH NUMBER : 1596389 SAMPLE ID : T0405235014 UU SAMPLE QTY : 0.502 G -+/-0.199 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 68.8 +/-8.281 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1237E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 145 DETECTOR S/N : 72526 AVERAGE %EFFICIENCY : 26.3634 AVERAGE %EFF ERROR : 0.5106 COUNT DATE : 29-Sep-2016 09:21 :05 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B145.CNF;1121 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W145.CNF;365 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4515.14 4427.25 4.6539 dpm 5248.57 5316.91 PEAK NET 1 708.88 0.28 PEAK NET2 2.76 263.24 RECOVERY YIELD CORR. 100.726 N/A 69.468 1.0091 NUCLIDE LIBRARY (ii f-z => 0 s t5 <( ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U-238: 3974-4284 keV U-235:4310-4581 keV 64 U-314:45924865keV U-23Z:S000-5398keV 57 50 43 36 29 22 15 8 2411 2806 3205 Energy (keV) PEAK PEAK GROSS ENERGY FWHM AREA 5248.57 4.914 1.000 4798.98 52.821 57.000 4515.14 47.553 3.000 4212.03 7.207 68.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.280 0.720 0.8485 100.000 3.97E-03 55.800 1.200 1.0954 100.000 8.86E-01 2.760 0.240 0.4899 99.700 4.40E-02 67.520 0.480 0.6928 100.000 1.07E+OO 5682 6108 6539 6973 7411 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.15E-02 8.65E-02 2.20E-02 4.15E-02 2.80E-01 1.11E-01 3.19E-02 2.38E-01 6.37E-02 7.64E-02 1.43E-02 6.33E-02 3.15E-01 8.79E-02 2.02E-02 2.59E-01 NOTES:

Results are a compilation of S0405235014_UU and T0405235014_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235014 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 024 DETECTOR SIN : 76542 AVERAGE %EFFICIENCY : 34.2046 AVERAGE %EFF ERROR : 0.6588 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 69.5 +/-6.998 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.2330E+OO dpm NUCLIDE LIBRARY PEAK (ii I-z :::i 0 !2. 0 <l'. ENERGY ENERGY U-232 5302.10 5316.91 U-3/4 4763.02 4763.80 U-235 4391.00 4427.25 U-238 4184.73 4203.88 U-238: 3974-4264 keV 19 U-235: 431Q-45a1 keV U-3!4:4592-4865keV 17 U-232:5000.5398keV 15 13 11 9 7 5 3 2398 2791 3188 3590 Energy (keV) PEAK FWHM 69.121 151.334 131.807 110.450 COUNT DATE : 29-Sep-2016 09:13:20 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 269.000 263.240 5.760 2.4000 100.000 4.18E+OO 57.000 55.800 1.200 1.0954 100.000 8.78E-01 3.000 2.760 0.240 0.4899 99.700 4.36E-02 68.000 67.520 0.480 0.6928 100.000 1.06E+OO 7416 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B024.CNF;1826 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W024.CNF;519 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.85E-01 1.87E-01 6.97E-02 2.67E-01 1.10E-01 3.16E-02 6.31E-02 7.57E-02 1.42E-02 2.98E-01 8.71E-02 2.00E-02 1.96-sigma cnt Unc pCi/G 5.12E-01 2.36E-01 6.28E-02 2.57E-01 AlphaSpectroscopySoftwareVers!on3.5.3 effectlvedate:02-Mar*2015 BATCH NUMBER : 1596389 SAMPLE ID : T0405235015 UU SAMPLE QTY : 0.509 G -+/-0.196 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 81.0 +/-8.967 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 8.2551E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 146 DETECTOR S/N : 72527 AVERAGE %EFFICIENCY : 25.4962 AVERAGE %EFF ERROR : 0.4943 COUNT DATE : 29-Sep-2016 09:21 :07 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B146.CNF;1123 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W146.CNF;315 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAK NET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4505.61 4473.12 503.62 5.52 73.994 N/A TRACER2 1564-1 U-232 4.6539 dpm 5182.40 5324.79 -0.40 223.56 81.655 1.0082 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G U-232 5302.10 5182.40 19.500 2.000 -0.400 2.400 1.5492 100.000 -7.98E-03 7.46E-02 1.73E-01 5.66E-02 7.45E-02 U-3/4 4763.02 4788.70 31.688 39.000 36.600 2.400 1.5492 100.000 6.74E-01 2.60E-01 1.60E-01 5.23E-02 2.30E-01 U-235 4391.00 4505.61 44.614 6.000 5.520 0.480 0.6928 99.700 1.02E-01 9.87E-02 1.02E-01 2.35E-02 9.70E-02 U-238 4184.73 4204.38 84.908 49.000 47.800 1.200 1.0954 100.000 8.81E-01 3.01E-01 1.29E-01 3.70E-02 2.56E-01 NOTES:

Results are a compilation of S0405235015_UU and T0405235015_UU. :! :! :! *The following nuclide results were quantified from the U-235 traced sample: § U-232 U-238;3974-4264keV
Correction made to the following net area 41 U-235:4310-4581keV U-314: 4592-4865 keV due to tracer impurity: 37 lJ.232:5000-5398keV U-238 (0.008 +/-0.000) 33 29 en 25 I-21 z :::> 17 0 £ 13 a 9 t5 5 <{ 1 2423 2815 3212 3613 5688 6117 6550 6987 7430 Energy (keV) "

BATCH NUMBER : 1596389 SAMPLE ID : S0405235015 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 113 DETECTOR S/N : 80009 AVERAGE %EFFICIENCY : 24.7132 AVERAGE %EFF ERROR : 0.4794 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 81.7 +/-7.426 % 1564-1 TRACER . ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.8001 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5324.79 U-3/4 4763.02 4770.20 U-235 4391.00 4473.12 U-238 4184.73 4204.64 21 lJ.238:3974-4284keV lJ.235:4310-4581 keV 19 U-3/4:4592-4865keV U-232:5000-S398keV 17 15 13 (ii 11 I-z 9 ::J 0 7 .?;> 5 *:;: t5 3 <!'. 2387 2785 3186 3592 Energy (keV) PEAK FWHM 58.110 49.156 7.423 54.434 COUNT DATE : 29-Sep-2016 09:20:16 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 225.000 223.560 1.440 1.2000 100.000 4.12E+OO 39.000 36.600 2.400 1.5492 100.000 6.69E-01 6.000 5.520 0.480 0.6928 99.700 1.01E-01 49.000 47.800 1.200 1.0954 100.000 8.73E-01 5674 6102 6533 6968 7407 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B113.CNF;1167 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W113.CNF;318 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.24E-01 1.36E-01 4.05E-02 2.50E-01 1.59E-01 5.19E-02 9.74E-02 1.02E-01 2.33E-02 2.86E-01 1.28E-01 3.67E-02 1.96-sigma cnt Unc pCi/G 5.43E-01 2.28E-01 9.62E-02 2.54E-01 "';) J',l CJ) .!>. Version 3.5.3 0 ....., BATCH NUMBER : 1596389 SAMPLE ID : T0405235016 UU SAMPLE QTY : 0.501 G -+/-0.200 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 79.3 +/-8.674 % SECONDARY QTY : 0.500 G +/-0.200 % TRACER . ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1236E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 147 DETECTOR S/N : 75550 AVERAGE %EFFICIENCY : 25.4403 AVERAGE %EFF ERROR : 0.4932 COUNT DATE : 29-Sep-2016 09:21 :11 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B147.CNF;1093 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W147.CNF;294 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4497.15 4385.41 TRACER2 1564-1 U-232 4.6539 dpm 5373.12 5302.74 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABLIN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5373.12 4.973 1.000 -1.160 2.160 1.4697 100.000 U-3/4 4763.02 4782.67 39.369 42.000 40.800 1.200 1.0954 100.000 U-235 4391.00 4497.15 39.134 4.000 3.760 0.240 0.4899 99.700 U-238 4184.73 4207.27 47.864 38.000 36.800 1.200 1.0954 100.000 lJ.238* 3974-4284 keV U-235:4310-4581 keV lJ.314:4592-4865keV 64 U-232:S000-5398keV -57 50 en 36 I-z 29 :J 0 22 8 15 .Iii j t5 8 <l'. I I I' I I I I I I 23 90 2790 3193 3600 4010 424 48 1 5262 5687 6115 6546 6981 -Energy (keV) ACTIVITY pCi/G -1.71E-02 7.64E-01 7.06E-02 6.89E-01 I 7420 683.96 3.76 100.710 N/A -1.16 223.56 79.985 1.0082 1.96-sigma 1.96-sigma TPU MDA Le en! Une pCi/G pCi/G pCi/G pCi/G 4.65E-02 1.24E-01 3.98E-02 4.65E-02 2.76E-01 1.31E-01 3.76E-02 2.42E-01 8.41E-02 9.00E-02 1.68E-02 8.32E-02 2.60E-01 1.31E-01 3.76E-02 2.30E-01 NOTES: *Results are a compilation of S0405235016_UU and T0405235016_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235016 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 115 DETECTOR S/N : 79995 AVERAGE %EFFICIENCY : 25.2291 AVERAGE %EFF ERROR : 0.4892 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 80.0 +/-7.426 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.7224E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5302.74 U-3/4 4763.02 4766.56 U-235 4391.00 4385.41 U-238 4184.73 4201.07 U 235* 3974-4284 keV 23 _ U-235: 431Cl-4581 keV U*3/4:4592-4865keV 21 -lJ.232:5()()().5398keV 19 15 -en 13 -I-z 11 -:::J 9 0 -8 7 u 3 <( --II I I I I 23 82 2782 3186 3593 Energy (keV) PEAK FWHM 29.859 46.447 84.599 36.494 I I 4104 1111 I 418 COUNT DATE : 29-Sep-2016 09:20:17 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 225.000 223.560 1.440 1.2000 100.000 4.18E+OO 42.000 40.800 1.200 1.0954 100.000 7.57E-01 4.000 3.760 0.240 0.4899 99.700 7.00E-02 38.000 36.800 1.200 1.0954 100.000 6.83E-01 11j I "" Ill I I I I I I I 48 6 5257 5682 6111 6543 6978 7417 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B115.CNF;1179 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W115.CNF;335 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.37E-01 1.38E-01 4.11E-02 2.65E-01 1.30E-01 3.73E-02 8.32E-02 8.93E-02 1.67E-02 2.50E-01 1.30E-01 3.73E-02 1.96-sigma cnt Unc pCi/G 5.52E-01 2.40E-01 8.25E-02 2.28E-01 "ti <> """ gj Version 3.5.3 0 ......, BATCH NUMBER : 1596389 SAMPLE ID : T0405235017 UU g SAMPLE QTY : 0.501 G -+/-0.200 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 41.0 +/-10.817 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1349E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 148 DETECTOR S/N : 74429 AVERAGE %EFFICIENCY : 24.2876 AVERAGE %EFF ERROR : 0.4715 COUNT DATE : 29-Sep-2016 09:21 :13 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B148.CNF;1094 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W148.CNF;312 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4493.59 4445.45 4.6547 dpm 5309.91 5314.28 PEAK NET 1 659.57 1.80 PEAK NET2 -0.24 119.08 RECOVERY YIELD CORR. 101.728 N/A 41.561 1.0149 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5309.91 0.000 3.000 U-3/4 4763.02 4774.44 21.556 30.000 U-235 4391.00 4493.59 45.448 0.000 U-238 4184.73 4200.78 34.293 39.000 :; > U-238: 3974-4284 keV 61 U-235:4310-4581 kaV U.314: 45924865 keV 55 U-232:5000-S398keV 49 43 Cii 37 I-31 z ::l 25 0 s 19 a 13 *:; ti 7 <( 2410 2804 3202 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 1.800 1.200 1.0954 100.000 2.71E-02 29.520 0.480 0.6928 100.000 1.04E+OO -0.240 0.240 0.4899 99.700 -8.51E-03 38.040 0.960 0.9798 100.000 1.35E+OO 5679 6106 6538 6973 7413 1.96-sigma TPU pCi/G 6.19E-02 4.48E-01 7.38E-02 5.27E-01 NOTES: MDA pCi/G 1.06E-01 1.96E-01 1.70E-01 2.33E-01 Le pCi/G 3.03E-02 4.49E-02 3.18E-02 6.35E-02 1.96-sigma cnt Unc pCi/G 6.16E-02 3.87E-01 7.34E-02 4.40E-01 *Results are a compilation of S0405235017 _UU and T0405235017 _UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

AlphaSpectrt1scopySoftwareVersion3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596389 SAMPLE ID : S0405235017 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 116 DETECTOR S/N : 80004 AVERAGE %EFFICIENCY : 25.8624 AVERAGE %EFF ERROR : 0.5011 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 41.6 +/-9.811 % TRACER 1564-1 . ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 1.9345E+OO dpm NUCLIDE LIBRARY PEAK 'ii) 1--z :::::> 0 u <l'. ENERGY ENERGY U-232 5302.10 5314.28 U-3/4 4763.02 4770.64 U-235 4391.00 4445.45 U-238 4184.73 4207.25 U-238: 3974-4284 keV 15 U-235:431D-4561 keV U-3/4:4592-4865kaV U*232:5()()().5398keV 13 11 9 7 5 3 2381 2778 3179 3584 Energy (keV) PEAK FWHM 25.824 33.545 0.000 19.756 >> COUNT DATE : 29-Sep-2016 09:20:21 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 121.000 119.080 1.920 1.3856 100.000 4.19E+OO 30.000 29.520 0.480 0.6928 100.000 1.03E+OO 0.000 -0.240 0.240 0.4899 99.700 -8.39E-03 39.000 38.040 0.960 0.9798 100.000 1.33E+OO ll ! 5670 6100 6533 6970 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B116.CNF;1161 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W116.CNF;295 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.12E+OO 2.84E-01 8.92E-02 4.31E-01 1.93E-01 4.42E-02 7.27E-02 1.68E-01 3.14E-02 5.06E-01 2.30E-01 6.26E-02 1.96-sigma cnt Unc pCi/G 7.62E-01 3.81E-01 7.24E-02 4.34E-01 BATCH NUMBER : 1596389 SAMPLE ID : T0405235018 UU SAMPLE QTY : 0.500 G -+/-0.200 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 68.4 +/-9.097 % SECONDARY QTY : 0.502 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0367E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 149 DETECTOR S/N : 33449 AVERAGE %EFFICIENCY : 25.2769 AVERAGE %EFF ERROR : 0.4901 COUNT DATE : 29-Sep-2016 09:21 :16 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B149.CNF;1104 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W149.CNF;305 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4485.13 4355.28 4.6547 dpm 5336.73 5321.48 PEAK NET 1 627.02 2.52 PEAK NET2 0.76 199.12 RECOVERY YIELD CORR. 92.924 N/A 69.646 1.0180 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5336.73 43.948 3.000 U-3/4 4763.02 4766.73 39.065 33.000 U-235 4391.00 4485.13 63.856 1.000 U-238 4184.73 4177.10 111.905 37.000 51 U-238: keV lJ.235: 4310-4581 keV 46 U-314:4592-4865keV U-232:5000..5398keV 41 36 31 Ui 26 I-z :J 21 0 8 16 11 *5 6 <!'. 2411 2804 3201 3602 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 2.520 0.480 0.6928 100.000 4.04E-02 31.560 1.440 1.2000 100.000 6.71E-01 0.760 0.240 0.4899 99.700 1.62E-02 35.800 1.200 1.0954 100.000 7.61E-01 5676 6104 6536 6972 7413 1.96-sigma TPU pCi/G 6.47E-02 2.73E-01 6.09E-02 2.93E-01 NOTES: MDA pCi/G 8.89E-02 1.57E-01 1.02E-01 1.49E-01 Le pCi/G 2.04E-02 4.67E-02 1.91E-02 4.27E-02 1.96-sigma en! Une pCi/G 6.43E-02 2.44E-01 6.08E-02 2.58E-01

Results are a compilation of S0405235018_UU and T0405235018_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235018 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 117 DETECTOR S/N : 80003 AVERAGE %EFFICIENCY : 25.8068 AVERAGE %EFF ERROR : 0.5001 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 69.6 +/-7.825 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 3.2418E+OO dpm NUCLIDE LIBRARY PEAK 00 I-z :J 0 *:;: u <i: ENERGY ENERGY U-232 5302.10 5321.48 U-3/4 4763.02 4764.22 U-235 4391.00 4355.28 U-238 4184.73 4185.79 U-238: 3974-4264 keV 17 U-235:431Q-4581 keV U-3/4;4592-486SkeV U-232:5000-5398keV 15 13 11 9 7 5 3 2390 2787 3187 3592 Energy (keV) PEAK FWHM 57.512 13.967 4.930 24.032 COUNT DATE : 29-Sep-2016 09:20:23 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA S!Dev pCi/G 202.000 199.120 2.880 1.6971 100.000 4.19E+OO 33.000 31.560 1.440 1.2000 100.000 6.59E-01 1.000 0.760 0.240 0.4899 99.700 1.59E-02 37.000 35.800 1.200 1.0954 100.000 7.48E-01 g 5673 6101 6533 6970 7410 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B117.CNF;1164 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W117.CNF;308 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.87E-01 1.94E-01 6.55E-02 2.62E-01 1.54E-01 4.59E-02 5.98E-02 1.00E-01 1.88E-02 2.80E-01 1.46E-01 4.19E-02 1.96-sigma cnt Unc pCi/G 5.89E-01 2.40E-01 5.97E-02 2.53E-01 ..., <> """' tj Version 3.5.3 0 ....., BATCH NUMBER : 1596389 SAMPLE ID : T0405235019 UU g SAMPLE QTY : 0.506 G -+/-0.198 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 76.6 +/-8.977 % SECONDARY QTY : 0.506 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 8.7346E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 150 DETECTOR S/N : 75552 AVERAGE %EFFICIENCY : 24.8352 AVERAGE %EFF ERROR : 0.4817 COUNT DATE : 29-Sep-2016 09:21 :17 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B150.CNF;1102 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W150.CNF;296 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4496.47 4406.78 TRACER2 1564-1 U-232 4.6539 dpm 5337.91 5307.70 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5337.91 4.978 1.000 -0.200 1.200 1.0954 100.000 U-3/4 4763.02 4768.72 44.803 39.000 39.000 0.000 0.0000 100.000 U-235 4391.00 4496.47 27.468 7.000 6.760 0.240 0.4899 99.700 U-238 4184.73 4192.11 34.017 49.000 48.760 0.240 0.4899 100.000 u 238 3974-4284 k v r" ' 61 U-235:43104581kaV f-U-3/4:4592-4865keV U-232: 5000-5398 keV 55 r 49 r 43 f-Ci) 37 ,... I-31 z ,... ;:;) 25 0 19 f-0 13 *;;: f-:g 7 <t: r .. ..il I I I I I I I 23 90 2790 3193 3601 4 11 425 48 3 5264 5688 6117 6548 6983 Energy (keV) ACTIVITY pCi/G -3.85E-03 7.38E-01 1.28E-01 9.22E-01 I 7422 519.06 6.76 78.292 N/A -0.20 219.04 77.214 1.0082 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 5.78E-02 1.35E-01 3.86E-02 5.77E-02 2.70E-01 5.67E-02 O.OOE+OO 2.35E-01 1.08E-01 9.10E-02 1.?0E-02 1.06E-01 3.11E-01 9.07E-02 1.70E-02 2.62E-01 NOTES:

Results are a compilation of S0405235019_UU and T0405235019_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235019 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 118 DETECTOR S/N : 80061 AVERAGE %EFFICIENCY : 25.6062 AVERAGE %EFF ERROR : 0.4962 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 77.2 +/-7.481 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.5935E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5307.70 U-3/4 4763.02 4770.44 U-235 4391.00 4406.78 U-238 4184.73 4195.25 25 lJ.238: 39744284 keV U-235: 4310-4581 keV 23 lJ..3/4:4592""486SkeV U-232:S000-539SkeV 21 19 17 0' 15 13 z 11 ::i 0 9 s 7 *;; 5 ti 3 <i: 2384 2782 3183 3589 Energy (keV) PEAK FWHM 28.785 19.809 4.952 58.189 3 98 410 COUNT DATE : 29-Sep-2016 09:20:26 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 220.000 219.040 0.960 0.9798 100.000 4.14E+OO 39.000 39.000 0.000 0.0000 100.000 7.32E-01 7.000 6.760 0.240 0.4899 99.700 1.27E-01 49.000 48.760 0.240 0.4899 100.000 9.15E-01 5671 6098 6529 6964 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B118.CNF;1173 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W118.CNF;318 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.36E-01 1.25E-01 3.39E-02 2.58E-01 5.63E-02 O.OOE+OO 1.07E-01 9.02E-02 1.69E-02 2.95E-01 9.00E-02 1.68E-02 1.96-sigma cnt Unc pCi/G 5.51E-01 2.33E-01 1.05E-01 2.60E-01 '"O """ 0 ....., BATCH NUMBER : 1596389 SAMPLE ID : T0405235020 UU g SAMPLE QTY : 0.502 G -+/-0.199 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 78.4 +/-9.102 % SECONDARY QTY : 0.500 G +/-0.200 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.7019E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 152 DETECTOR S/N : 76222 AVERAGE %EFFICIENCY : 24.2896 AVERAGE %EFF ERROR : 0.4714 COUNT DATE : 29-Sep-2016 09:21 :21 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B152.CNF;1088 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W152.CNF;285 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4488.89 4403.16 4.6539 dpm 5061.99 5317.48 PEAK NET 1 563.87 0.60 PEAK NET2 2.76 205.36 RECOVERY YIELD CORR. 86.962 N/A 79.255 1.0108 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5061.99 48.668 3.000 U-3/4 4763.02 4747.81 96.525 30.000 U-235 4391.00 4488.89 52.650 3.000 U-238 4184.73 4208.03 20.684 43.000 U-Z38; 3974-4284 keV 46 U-235:4310-4581 keV U-314: 4592-4865 keV 41 U-232:5000-5398keV 36 31 Vi 26 I-z 21 ;:;) 0 16 s c 11 *:;; u 6 <{ 2406 2798 3194 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.600 2.400 1.5492 100.000 1.08E-02 29.520 0.480 0.6928 100.000 6.02E-01 2.760 0.240 0.4899 99.700 5.64E-02 41.560 1.440 1.2000 100.000 8.47E-01 5660 6086 6517 6952 7391 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.57E-02 1.55E-01 5.08E-02 7.56E-02 2.49E-01 1.13E-01 2.59E-02 2.23E-01 8.20E-02 9.80E-02 1.84E-02 8.13E-02 3.08E-01 1.51E-01 4.48E-02 2.66E-01 NOTES: *Results are a compilation of S0405235020_UU and T0405235020_UU. 1

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S0405235020 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 119 DETECTOR SIN : 79450 AVERAGE %EFFICIENCY : 23.3886 AVERAGE %EFF ERROR : 0.4544 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 79.3 +/-7.719 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.6885E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5317.48 U-3/4 4763.02 4770.61 U-235 4391.00 4403.16 U-238 4184.73 4203.10 19 U-238;3974-4284keV U-235:431o-4581 keV 17 lJ..314;4592-4865keV U-232: 5000-5398 keV 15 13 0' 11 z 9 ::> 0 7 5 u 3 <( 1 2387 2785 3187 3592 Energy (keV) PEAK FWHM 63.804 17.330 54.467 49.515 4 02 415 COUNT DATE : 29-Sep-2016 09:20:28 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 208.000 205.360 2.640 1.6248 100.000 4.18E+OO 30.000 29.520 0.480 0.6928 100.000 5.95E-01 3.000 2.760 0.240 0.4899 99.700 5.58E-02 43.000 41.560 1.440 1.2000 100.000 8.38E-01 5678 6107 6539 6975 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B119.CNF;1182 BKG DATE : 24-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W119.CNF;315 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.71E-01 1.82E-01 6.05E-02 2.39E-01 1.12E-01 2.56E-02 8.09E-02 9.70E-02 1.82E-02 2.94E-01 1.49E-01 4.43E-02 1.96-sigma en! Une pCi/G 5.77E-01 2.21E-01 8.04E-02 2.63E-01 BATCH NUMBER : 1596389 SAMPLE ID : T1203621691_UU SAMPLE QTY : 0.509 G +/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 012 DETECTOR S/N : 80054 AVERAGE %EFFICIENCY : 29.2738 AVERAGE %EFF ERROR : 0.5658 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B012.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 74.3 +/-8.329 % COUNT DATE : 29-Sep-2016 09:13:18 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W012.CNF;496 CAL DATE : 27-Sep-2016 SECONDARY QTY : 0.509 G +/-0.196 % TRACER ID : , 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0731 E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 751.65 -1.40 PEAKNET2 0.32 255.04 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5295.22 345.512 U-3/4 4763.02 4637.55 54.295 U-235 4391.00 4492.76 30.147 U-238 4184.73 4096.71 187.564 U238 39744284k V ' U*235:431G4581 keV 82 U-314: 45924865 keV U-232:5000-5398keV 73 64 55 'iii 46 1--z ::::> 37 0 s 28 19 *::; I n 10 <( I I 23 99 2796 3197 3601 4 09 i421 Energy (keV) 11.1230 dpm 4492. 76 4386.49 4.6165 dpm 5295.22 5318.39 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA S!Dev 7.000 -1.400 8.400 2.8983 100.000 2.000 -0.400 2.400 1.5492 100.000 2.000 0.320 1.680 1.2961 99.700 3.000 1.320 1.680 1.2961 100.000 ,, J,

I I I I I 48l7 5257 5680 6107 6538 6973 ACTIVITY pCi/G -1.83E-02 -6.41E-03 5.14E-03 2.11E-02 I 7412 96.184 N/A 74.267 1.0001 1.96-sigma 1.96-sigma TPU MDA Le en! Une pCi/G pCi/G pCi/G pCi/G 8.15E-02 1.78E-01 6.95E-02 8.15E-02 5.99E-02 1.39E-01 4.55E-02 5.98E-02 5.86E-02 1.24E-01 3.81E-02 5.86E-02 6.64E-02 1.24E-01 3.80E-02 6.63E-02 NOTES: *Results are a compilation of S1203621691_UU and T1203621691_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S1203621691_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 011 DETECTOR S/N : 72531 AVERAGE %EFFICIENCY : 30.9977 AVERAGE %EFF ERROR : 0.5982 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 74.3 +/-7.107 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6165E+OO dpm 3.4285E+OO dpm NUCLIDE LIBRARY PEAK z :::> 0 .;:. *:;: <t: ENERGY ENERGY U-232 5302.10 5318.39 U-3/4 4763.02 4765.12 U-235 4391.00 4386.49 U-238 4184.73 4077.40 28 U-238:3974-4284keV U-235: 431Q-45B1 keV 25 U-J/4:4592-486SkeV U-232:5000.5398keV 22 19 16 13 10 7 4 1 2393 2791 3193 3600 Energy (keV) PEAK FWHM 27.491 162.895 83.916 162.895 COUNT DATE : 29-Sep-2016 09:13:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 262.000 255.040 6.960 2.6382 100.000 4.09E+OO 2.000 -0.400 2.400 1.5492 100.000 -6.41E-03 2.000 0.320 1.680 1.2961. 99.700 5.14E-03 3.000 1.320 1.680 1.2961 100.000 2.11E-02 7479 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B011.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W011.CNF;515 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.80E-01 2.03E-01 7.74E-02 5.99E-02 1.39E-01 4.55E-02 5.86E-02 1.24E-01 3.81E-02 6.64E-02 1.24E-01 3.80E-02 1.96-sigma cnt Unc pCi/G 5.11E-01 5.98E-02 5.86E-02 6.63E-02 '"d .j:>. 0 ...., BATCH NUMBER : 1596389 SAMPLE ID : T1203621692 UU SAMPLE QTY : 0.500 G -+/-0.200 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 CORRECTED % YIELD : 78.1 +/-8.958 % SECONDARY QTY : 0.509 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 7.7426E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 154 DETECTOR S/N : 76224 AVERAGE %EFFICIENCY : 26.1126 AVERAGE %EFF ERROR : 0.5058 COUNT DATE : 29-Sep-2016 09:21 :23 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B154.CNF;1099 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W154.CNF;304 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4484.14 4468.67 4.6537 dpm 5198.56 5340.29 PEAK NET 1 483.77 -1.44 PEAKNET2 5.00 228.56 RECOVERY YIELD CORR. 69.400 N/A 78.700 1.0081 NUCLIDE LIBRARY PEAK 00 I-z :J 0 *::; u <( ENERGY ENERGY U-232 5302.10 5198.56 U-3/4 4763.02 4764.08 U-235 4391.00 4484.14 U-238 4184.73 4191.98 U-238:3974-4284keV 46 U-235:4310-4581keV U-3/4:4592-4865keV 41 U.232:5000-5398keV 36 31 26 21 16 11 6 2372 2768 3169 3574 3 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 58.629 87.000 42.530 5.000 35.736 59.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -1.440 1.440 1.2000 100.000 -2.95E-02 86.280 0.720 0.8485 100.000 1.58E+OO 5.000 0.000 0.0000 99.700 9.20E-02 59.000 0.000 0.0000 100.000 1.08E+OO 5230 5654 6081 6513 6948 7387 1.96-sigma TPU pCi/G 4.78E-02 4.41E-01 9.03E-02 3.40E-01 NOTES: MDA pCi/G 1.52E-01 1.12E-01 5.52E-02 5.50E-02 Le pCi/G 4.51E-02 2.85E-02 O.OOE+OO O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.76E-02 3.38E-01 8.88E-02 2.79E'.01 *Results are a compilation of S1203621692_UU and T1203621692_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.007 +/-0.000)

BATCH NUMBER : 1596389 SAMPLE ID : S1203621692 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 121 DETECTOR S/N : 75545 AVERAGE %EFFICIENCY : 26.2144 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 78.7 +/-7.358 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6537E+OO dpm 3.6624E+OO dpm NUCLIDE LIBRARY PEAK (ii I-z :::i 0 S?.. *s: u <t: ENERGY ENERGY U-232 5302.10 5340.29 U-3/4 4763.02 4801.39 U-235 4391.00 4468.67 U-238 4184.73 4232.01 U-238: 3974-4284 keV 19 U-235: 43104581 keV U-3/4:4592-4865keV 17 U-232:5000.5398keV 15 13 11 9 7 5 3 1 2424 2819 3217 3620 Energy (keV) PEAK FWHM 66.272 34.568 112.909 67.745 COUNT DATE : 29-Sep-2016 09:20:31 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 230.000 228.560 1.440 1.2000 100.000 4.19E+OO 87.000 86.280 0.720 0.8485 100.000 1.57E+OO 5.000 5.000 0.000 0.0000 99.700 9.12E-02 59.000 59.000 0.000 0.0000 100.000 1.07E+OO 5694 6121 6551 6986 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B121.CNF;1160 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W121.CNF;322 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.31E-01 1.36E-01 4.03E-02 4.09E-01 1.11E-01 2.83E-02 8.91E-02 5.47E-02 O.OOE+OO 3.19E-01 5.46E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.47E-01 3.35E-01 8.80E-02 2.76E-01 '"d (l) .j:>. 00 Alpha Spectroscopy Software Version 3.5.3 O effectivedate:OZ-Mar-2015 0 ....., BATCH NUMBER : 1596389 SAMPLE ID : T1203621693 UU SAMPLE QTY : 0.509 G -+/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 155 DETECTOR S/N : 75553 AVERAGE %EFFICIENCY : 26.3876 AVERAGE %EFF ERROR : 0.5110 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B155.CNF;1101 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 CORRECTED% YIELD : 70.5 +/-9.127 % COUNT DATE : 29-Sep-2016 09:21 :25 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W155.CNF;289 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.509 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 8.5034E+OO dpm LCS ID NUCLIDE NOMINAL (pCi/G) % RECOVERY 1600-E U-238 5.2915E+OO 118.401 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 536.91 -1.16 PEAK NET2 18.76 202.80 RECOVERY YIELD CORR. 11.1230 dpm 4488.36 4431.18 4.6165 dpm 5256.88 5318.73 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5256.88 4.930 1.000 -1.160 2.160 1.4697 100.000 U-3/4 4763.02 4752.09 162.697 268.000 267.280 0.720 0.8485 100.000 U-235 4391.00 4488.36 58.366 19.000 18.760 0.240 0.4899 99.700 U-238 4184.73 4186.09 182.418 311.000 311.000 0.000 0.0000 100.000 ii U 238* 39744284 keV 51 U-235:4310-4581 keV -lJ.3!4:4592-4865keV 46 U-232:5000-5398keV 36 -'Ci) 31 1--26 z :::> 21 0 16 .2:-11 *:;; 6 --I I I 11 I I I I I I 23 95 2792 3192 3597 4i06 419 48.6 5257 5682 6111 6545 6982 -Energy (keV) ACTIVITY pCi/G -2.13E-02 5.38E+OO 3.79E-01 6.27E+OO I 7424 76.219 N/A 70.510 1.0001 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 5.78E-02 1.54E-01 4.94E-02 5.77E-02 1.18E+OO 1.23E-01 3.13E-02 6.48E-01 1.91E-01 9.69E-02 1.81E-02 1.78E-01 1.34E+OO 6.04E-02 O.OOE+OO 6.98E-01 NOTES: *Results are a compilation of S1203621693_UU and T1203621693_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000) 0 ....., V\ 00 0 ID AlphaSpectroscopySoftwareVersion35.3 effecllvedate:02-Mar-2015 BATCH NUMBER : 1596389 SAMPLE ID : S1203621693 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 122 DETECTOR S/N : 75546 AVERAGE %EFFICIENCY : 25.9617 AVERAGE %EFF ERROR : 0.5030 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 70.5 +/-7.731 % TRACER ID 1564-1 NUCLIDE U-232 NOMINAL 4.6165E+OO dpm RESULTS 3.2551 E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5318.73 37.071 U-3/4 4763.02 4769.36 60.743 U-235 4391.00 4431.18 29.751 U-238 4184.73 4205.12 40.889 U z:ia* 3974-4284 keV 37 U:235; 4310-4581 keV U-3/4:4592-4865keV 33 1-U-232:5000-5398keV 29 25 Ui 21 f-t-z 17 :::> f-0 13 8 9 u 5 f-<( IT I I I I I .. .rl I I I I 23 82 2781 3183 3589 3 99 Energy (keV) nil I 413 COUNT DATE : 29-Sep-2016 09:20:33 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID . 1600-E NUCLIDE U-238 NOMINAL (pCi/G) 5.2915E+OO % RECOVERY 118.390 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 204.000 202.800 1.200 1.0954 100.000 4.09E+OO 268.000 267.280 0.720 0.8485 100.000 5.38E+OO 19.000 18.760 0.240 0.4899 99.700 3.79E-01 311.000 311.000 0.000 0.0000 100.000 6.26E+OO .I I I I I I I 48 0 5251 5676 6105 6537 6974 7414 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B122.CNF;1172 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W122,CNF;334 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.53E-01 1.41E-01 4.04E-02 1.06E+OO 1.23E-01 3.13E-02 1.87E-01 9.69E-02 1.81E-02 1.20E+OO 6.04E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.66E-01 6.48E-01 1.78E-01 6.97E-01 Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 30-Sep-2016 Criteria: Yes No Comments Samole Solids are less than or eoual to 100 mo for GAB. i\}o Samples have been blank corrected (If required). l\.b--Blank correction reoorted Included (If reoulred'. [f activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. lf greater than 10* MDA/ MDC, error Is 40% or less. [f holn.., *ho Mn A I Mnr lc ni.,,.u / . Instrument source check is within limits. Instrument bkn che,.,k is within ,/ Method RDL/ LLD has been met. \/' If duolicate activities are: Less than 5* M DA/ MDC, then RPO Is 100% or less, ./ Cai-i. . .U'\.Clh-!'.Jlvc If greater 5* MDA/ MDC, then RPD 20% or less, [f below the MDA/ MDC, the RPO is 0%, Or meets the client's reaulred RER accentance criteria. Tracer yield is 15-125%
Carrier yield 25-1250/o. {Or meets the client's contract acceptance criteria). v Method blank is less than the RDL/ LLD. /' C\lU1_. Yl.QW'o.h1te_ (If"""' < nf ln..,oc* :.rlivltv' Samole was run within hold time. v ,)(:'.4Lll* \ 'Slc.?J?J)!J Samele was correctlv oreserved If reoulred. Smears Taken for Radioactive batches. Method Spike and LCS are within 75-125% or mPets the client's contr,.,.. acrPnt:.nce criteria). ./ w No blank spaces on data forms. / Ali line outs Initialed and dated. Nn n**n*c Aux data Is correct. Client Soeclal reoulrements oaae has been checked. ,/ Raw Data and I or soectrum are included and orooerlv st:.*used. _,,,,,--MS, LCS, and Duolicate RPD/RER values uploaded to UMS and ,.,,.-.. k,,.luoc uorl<in..t : ..... flf *\ tJ?-!R,.trh ontn*n..t ln+n r,.co ./ Batch Data Exceotlon Reoorts fDERl comoleted if aoollcable. .,.,... 1Y.iLlt* Batch Data Exception Reports (DER) second reviewed. ....---l'Slc3'0S) Disoositlon verified to be comnleted. IAliouot Co**nrtlnn d If .... nulred. /Vo-Review sample historical results If available / {If REMP, results above MDC have been verified bv historical results-recount or re-analvsls.\ Primary Review Performed By:. __ ___ 1_12>0_)_1_L,. ____ _ . Secondary Review Performed By:__ 10/02/16 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 30-SEP-16 Instrument Type: ALPHA SPECTROMETER Batch ID: 1601257 ' DATA EXCl::PTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: HASL-300, U-02-RC Solid .. Sample Numbers: See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235051 and 1203633743 were received and analyzed out 1. Reporting results. of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 30-SEP-16 Jessica Davis 02-0CT-16 Page 1 Page 483 of 5809 DER Report No.: 1563353 Revision No.: 1 J Type: Process Client Code: MJWC Uranium Que Sheet 22-SEP-16 Batch#: 1601257 Analyst: KXB2 First Client Due Date:04-0CT-16 Internal Due Date:Ol-OCT-16 Tracer Tracer Code: \ SU\..\.-:L Expiration Date: \ l-* l V Vol:-52.:....l-Analyzed Sequentially with Pu Analyzed Sequentially with: LCS Isotope: U-238 -LCS Code: \I oOO-f; Expiration Date: 1-\"2--1/ Vol:--12.:_L Pu-236 ID: Pu: ___ _ Spike Isotope: U-238 Spike Code:_______ Expiration Date: Vol:-=-Prep Date:"\-1.\ -\V Initials: ??f--, Pipet ID:\ ioU.oO-Z....f;; Balance ID: \\.e\0] \ rlf 7,.. Sample ID Client Description '1 Type --------------405235051-2 4.5B.R.2.3 SAMPLE 1203633742-1 MB for batch 1601257 MB 1203633743-2 4.SB.R.2.3(405235051DUP) DUP 1203633744-1 LCS for batch 1601257 LCS Choose SOP used: GL-RAD-A-011 GEL Laboratories LLC, Radiochemistry Division Hazard Code MinCRDL Matrix Client 1 pCi/g SOIL MJ\YCOOI UCF pCi/g to pCil SOIL QCACCOUJl;T 1 pCi/g SOIL QC ACCOUNT UCF pCi/g to pCil SOIL QC ACCOUNT Solid Sample Dissolution by: LEACH Circle One Vol.: ___ _ Am: ___ _ Witness: .Jf,l-\ '1.*7..i*/tg weti@ Collection Label Aliquot u Date Pos. Det# # 07-DEC-15 1 I o. \lLl 7 l I 2 *i. (L\\\ i 9 ! 07-DEC-15 3 I 3 o. 4 1 10 I Data Reviewed By: t..O'\ fr.a.,Jll1J-.. &i /.:PJ1 i.. Page 1 of 1 ../

Uranium Que Sheet 22-SEP-16 Batch#: 1601257 Analyst: KXB2 First Client Due Date:04-0CT-16 Expiration Date: \*\0 '\] Internal Due Date:Ol-OCT-16 Tracer Isotope: Code: \C?-'\0-f. LCS Isotope: U-238 LCS Code: -Vol: Q.\ Expiration Date: ____ _ Vol:_:::::__ Spike Isotope: U-238 Spike Code: -Prep Date: 0\.-1.... "1* \ V Initials: a:> Pipet ID: Date:_____ \faL-\00211:. Balance ID: \\.et 01 l.2\.0..-Hazard Sample ID Client Description Type Code MinCRDL Matrix Client ---405235051-2 4.SB.R.2.3 SAMPLE 1 pCi/g SOIL MJWCOOl 1203633742-1 MB for batch 1601257 J\IB UCF pCi/g to pCit SOIL QC ACCOUNT 1203633743-2 4.5B.R.2.3(405235051DUP) DUP 1 pCilg SOIL QCACCOUNT. 1203633744-1 LCS for batch 1601257 LCS UCF pCi/g to pCiJ SOIL QC ACCOUNT Choose SOP used: GL-RAD-A-011 GEL Laboratories LLC, Radiochemistry Division Analyzed Sequentially with Pu Analyzed Sequentially with: Pu-236 ID: Pu: ___ _ Vol.: ___ _ Am: Witness: "'i*Z"'l--/l'f wet8 u Label Aliquot Pos. # @110 Det# Collection Date 1 \ Io. \1.2 I /?_ 2 '2.. Io, n.i. I 11 I 07-DEC-15 3 3 10. \\U i ?fJ 4 g 0. ... :z.,..j 07-DEC-15 Data Reviewed By: *--'Nt, k 9 Page 1 of 1 BATCH NUMBER : 1601257 SAMPLE ID : T0405235051_UU SAMPLE QTY : 0.111 G +/-0.901 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 012 DETECTOR SIN : 80054 AVERAGE %EFFICIENCY : 29.2738 AVERAGE %EFF ERROR : 0.5658 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B012.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 88.3 +/-5.690 % COUNT DATE : 29-Sep-201614:04:46 ELAPSED LIVE TIME(SEC) : 43200.00 EFF FILE : W012.CNF;496 CAL DATE : 27-Sep-2016 SECONDARY QTY : 0.122 G +/-0.820 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.1185E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 2350.50 -1.20 PEAKNET2 5.56 788.84 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5281.19 U-3/4 4763.02 4751.18 U-235 4391.00 4487.35 U-238 4184.73 4149.67 201 U238*3974-4284keV i:::U:235;4310-4581 keV U*314:4592-4865keV 181 l--U-232:S000-5398keV 161 f--141 f--<ii 121 f--I-101 z f--:::> 81 0 f--s 61 f--.c 41 *::; f--u 21 <!'. f--I I I 1 23 99 2796 3197 3601 Energy (keV) PEAK FWHM 56.763 122.163 50.730 213.477 **"* *I I 4 09 11.1230 dpm 4487.35 4415.19 4.6540 dpm 5281.19 5320.37 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 24.000 -1.200 25.200 5.0200 100.000 36.000 30.960 5.040 2.2450 100.000 7.000 5.560 1.440 1.2000 99.700 42.000 41.280 0.720 0.8485 100.000 lo>J .. I .. I I I I I 48i7 5257 5680 6107 6538 6973 ACTIVITY pCi/G -2.11E-02 7.41E-01 1.34E-01 9.88E-01 I 7412 1.96-sigma TPU pCi/G 2.28E-01 3.14E-01 1.46E-01 3.33E-01 NOTES: MDA pCi/G 4.34E-01 3.04E-01 1.96E-01 1.59E-01 100.260 N/A 89.015 1.0082 Le pCi/G 1.91 E-01 1.16E-01 6.22E-02 4.38E-02 1.96-sigma cnt Unc pCi/G 2.28E-01 3.01E-01 1.45E-01 3.11E-01 *Results are a compilation of S0405235051_UU and T0405235051_UU.

The following nuclide results were quantified from the U-235 traced sample: L!-232
Correction made to the following net area due to tracer impurity: U-238 (0.035 +/-0.001)

AlphaSpectn:iso:ipySoftwareVersion3.5.3 effecliveda!e:02*Mar*2015 BATCH NUMBER : 1601257 SAMPLE ID : S0405235051_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.111 G +/-0.901 % CHAMBER : 007 DETECTOR S/N : 50-06621 AVERAGE %EFFICIENCY : 26.6641 AVERAGE %EFF ERROR : 0.5164 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 89.0 +/-4.754 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 4.1428E+OO dpm NUCLIDE U-232 U-3/4 U-235 U-238 73 65 57 49 41 z => 33 0 s 25 17 9 -- ---LIBRARY PEAK ENERGY ENERGY 5302.10 5320.37 4763.02 4769.46 4391.00 4415.19 4184.73 4193.16 U238'3974-4284kaV U*235:431G-4581keV lJ..3/4:4592-4865keV U*232:50()(}..5398keV I 1 2 374 2774 3179 3587 Energy (keV) PEAK FWHM 35.142 28.229 174.353 56.457 ,,iij, 3!98 I 414 COUNT DATE : 29-Sep-2016 14:04:46 ELAPSED LIVE TIME(SEC) : 43200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 791.000 788.840 2.160 1.4697 100.000 1.89E+01 36.000 30.960 5.040 2.2450 100.000 7.35E-01 7.000 5.560 1.440 1.2000 99.700 1.32E-01 42.000 41.280 0.720 0.8485 100.000 9.80E-01 ,,I, I I I I I I I 48 3 5256 5682 6113 6547 6985 7427 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B007.CNF;1847 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W007.CNF;505 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.34E+OO 2.24E-01 7.59E-02 3.08E-01 3.01E-01 1.15E-01 1.45E-01 1.95E-01 6.17E-02 3.25E-01 1.58E-01 4.35E-02 1.96-sigma cnt Unc pCi/G 1.32E+OO 2.99E-01 1.44E-01 3.09E-01 "'C c§ .p. 00 Alpha Spectroscopy Software Version 3.5.3 00 effecllvedate:OZ-Mar-2015 0 ,...., BATCH NUMBER : 1601257 SAMPLE ID : T1203633742 UU SAMPLE QTY : 0.111 G -+/-0.901 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 011 DETECTOR S/N : 72531 AVERAGE %EFFICIENCY : 30.9977 AVERAGE %EFF ERROR : 0.5982 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B011.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 27-Sep-2016 00:00:00 ANALYST : KXB2 CORRECTED % YIELD : 98.9 +/-5.454 % SECONDARY QTY : 0.122 G +/-0.820 % COUNT DATE : 29-Sep-2016 14:04:46 ELAPSED LIVE TIME(SEC) : 43200.00 EFF FILE : W011.CNF;515 CAL DATE : 27-Sep-2016 TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.6489E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U238*3974-4284keV U-235:4310-4581 keV 154 i--lJ..3/4:4592-4865keV U-232:5000-539BkeV 137 f-120 f-103 f-Ui I-86 f-z => 69 0 f-8 52 f-c 35 *:;; f-u 18 <! f-1 I I ID 1570-E 1564-1 PEAK ENERGY 5245.29 4761.34 4486.25 4152.91 I NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 2147.00 -1.88 PEAK NET2 25.12 1026.84 RECOVERY YIELD CORR. 11.1230 dpm 4486.25 4449.26 4.6164 dpm 5245.29 5310.19 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABLIN FWHM AREA AREA AREA Stoev 76.511 19.000 -1.880 20.880 4.5695 100.000 54.298 21.000 18.840 2.160 1.4697 100.000 59.355 28.000 25.120 2.880 1.6971 99.700 207.321 21.000 20.280 0.720 0.8485 100.000 .Ji :,, * .IL .. .. II I I I I I ACTIVITY pCi/G -3.60E-02 3.44E-01 4.60E-01 3.70E-01 I 1.96-sigma TPU pCi/G 2.24E-01 1.80E-01 2.08E-01 1.77E-01 NOTES: MDA pCi/G 4.35E-01 1.70E-01 1.89E-01 1.22E-01 86.487 N/A 98.860 1.0001 Le pCi/G 1.89E-01 5.78E-02 6.?0E-02 3.34E-02 1.96-sigma en! Unc pCi/G 2.24E-01 1.75E-01 2.02E-01 1.72E-01 *Results are a compilation of S1203633742_UU and T1203633742_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.033 +/-0.001) 23 93 2791 3193 3600 4428 4850 527E 5707 6143 6584 7029 7479 Energy (keV)

BATCH NUMBER : 1601257 SAMPLE ID : S1203633742 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLEQTY:0.111G -+/-0.901% CHAMBER : 009 DETECTOR SIN : 72528 AVERAGE %EFFICIENCY : 31.2521 AVERAGE %EFF ERROR : 0.6030 SAMPLE DATE : 27-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 98.9 +/-4.427 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6164E+OO dpm 4.5638E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5310.19 U-3/4 4763.02 4710.26 U-235 4391.00 4449.26 U-238 4184.73 4140.51 U*238:3974-4284keV 91 U-235:4310-4581 keV U-314: 4592-4865 keV U-232: SOQ0..5398 keV 81 71 61 en 51 I-z 41 ::::> 0 s 31 ;:. 21 *;; :g 11 <( 2383 2779 3180 3585 Energy (keV) PEAK FWHM 32.632 183.543 0.000 83.765 is 3 94 COUNT DATE : 29-Sep-2016 14:04:46 ELAPSED LIVE TIME(SEC) : 43200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET* BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 1029.000 1026.840 2.160 1.4697 100.000 1.87E+01 21.000 18.840 2.160 1.4697 100.000 3.44E-01 28.000 25.120 2.880 1.6971 99.700 4.60E-01 21.000 20.280 0.720 0.8485 100.000 3.70E-01 ll > i! 5673 6104 6539 6978 7422 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B009.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W009.CNF;516 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.14E+OO 1.70E-01 5.78E-02 1.79E-01 1.70E-01 5.78E-02 2.06E-01 1.89E-01 6.70E-02 1.75E-01 1.22E-01 3.34E-02 1.96-sigma cnt Unc pCi/G 1.15E+OO 1.75E-01 2.02E-01 1.72E-01 "1:1 0 .!:>. 0 ...., BATCH NUMBER : 1601257 SAMPLE ID : T1203633743 UU SAMPLE QTY : 0.106 G -+/-0.943 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 020 DETECTOR S/N : 78787 AVERAGE %EFFICIENCY : 31.0365 AVERAGE %EFF ERROR : 0.5989 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B020.CNF;1833 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 94.8 +/-5.428 % COUNT DATE : 29-Sep-2016 14:04:55 ELAPSED LIVE TIME(SEC) : 43199.99 EFF FILE : W020.CNF;562 CAL DATE : 27-Sep-2016 SECONDARY QTY : 0.116 G +/-0.862 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0911 E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 2430.94 -9.60 PEAKNET2 13.84 1033.68 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5275.55 4.933 U-3/4 4763.02 4760.03 54.266 U-235 4391.00 4474.39 64.379 U-238 4184.73 4181.73 0.000 U238'397442B4keV -. U-235:43104581 keV 145 1-U-3!4:4592-4865keV U-232:5()()().5398keV 129 >-113 r 97 r UJ 81 I-r z ::J 65 r 0 49 >-33 r 17 >-" ... I I I I 24 07 2804 3204 3608 4015 i427 Energy (keV) 11.1230 dpm 4474.39 4444.39 4.6540 dpm 5275.55 5306.73 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 12.000 -9.600 21.600 4.6476 100.000 56.000 53.120 2.880 1.6971 100.000 16.000 13.840 2.160 1.4697 99.700 58.000 54.400 3.600 1.8974 100.000 " ... .. I I I I I 48 2 5261 5683 6109 6539 6973 ACTIVITY pCi/G -1.72E-01 1.02E+OO 2.66E-01 1.04E+OO I 7410 1.96-sigma TPU pCi/G 1.89E-01 3.12E-01 1.67E-01 3.19E-01 NOTES: MDA pCi/G 4.13E-01 1.98E-01 1.79E-01 2.14E-01 97.802 N/A 95.552 1.0082 Le pCi/G 1.80E-01 7.01E-02 6.08E-02 7.83E-02 1.96-sigma cnt Unc pCi/G 1.89E-01 2.89E-01 1.64E-01 2.96E-01 *Results are a compilation of S1203633743_UU and T1203633743_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.037 +/-0.001) 0 ...., Vi 00 0 \0 BATCH NUMBER : 1601257 SAMPLE ID : S1203633743 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 008 DETECTOR S/N : 78788 AVERAGE %EFFICIENCY : 32.5495 AVERAGE %EFF ERROR : 0.6275 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 95.6 +/-4.456 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 4.4470E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5306.73 U-3/4 4763.02 4746.68 U-235 4391.00 4444.39 U-238 4184.73 4177.09 U-238:39744284kaV 82 U-235:4310-4581 keV U-Jf4:4592-4865keV 73 U-232:5000-5398keV 64 55 'Ci) 46 I-z 37 :::i 0 28 19 *:;; u 10 <( 1 PEAK FWHM 40.123 78.113 141.579 53.702 >> !!!1 2399 2792 3190 3593 4 00 412 Energy (keV) COUNT DATE : 29-Sep-2016 14:04:46 ELAPSED LIVE TIME(SEC) : 43200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA S!Dev pCi/G 1056.000 1033.680 22.320 4.7244 100.000 1.98E+01 56.000 53.120 2.880 1.6971 100.000 1.01E+OO 16.000 13.840 2.160 1.4697 99.700 2.63E-01 58.000 54.400 3.600 1.8974 100.000 1.03E+OO m 48 8 5250 5676 6107 6542 6983 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B008.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W008.CNF;517 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.28E+OO 4.47E-01 1.95E-01 3.03E-01 1.96E-01 6.95E-02 1.65E-01 1.78E-01 6.04E-02 3.10E-01 2.12E-01 7.77E-02 1.96-sigma cnt Unc pCi/G 1.23E+OO 2.87E-01 1.63E-01 2.93E-01 BATCH NUMBER : 1601257 SAMPLE ID : T1203633744 UU SAMPLE QTY : 0.111 G -+/-0.901 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 021 DETECTOR S/N : 795159 AVERAGE %EFFICIENCY : 32.0933 AVERAGE %EFF ERROR : 0.6189 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B021.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 27-Sep-2016 00:00:00 ANALYST : KXB2 CORRECTED% YIELD : 77.6 +/-5.765 % COUNT DATE : 29-Sep-2016 14:04:55 ELAPSED LIVE TIME(SEC) : 43199.99 EFF FILE : W021.CNF;539 CAL DATE : 27-Sep-2016 SECONDARY QTY : 0.122 G +/-0.820 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.1790E+OO dpm LCS .ID NUCLIDE NOMINAL (pCi/G) % RECOVERY 1600-E U-238 2.4265E+01 103.164 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 2114.64 3.64 PEAKNET2 63.28 798.20 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5282.36 77.195 U-3/4 4763.02 4669.77 142.136 U-235 4391.00 4473.72 44.683 U-238 4184.73 4139.53 274.470 201 U.238* 3974-4264 keV lJ.235:4310-4581keV 181 U-3/4;4592-4865keV r-U*232:5000.5398keV 161 f-141 f-121 f-Ci) 101 I-f-z ::J 81 0 f-f2.. 61 f-41 *:;; f-ti 21 <( f-1 l.J I I I II 23 95 2789 3188 3591 3!98 410 Energy (keV) ,. 11.1230 dpm 4473.72 4437.62 4.6164 dpm 5282.36 5305.41 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 13.000 3.640 9.360 3.0594 100.000 1064.000 1058.960 5.040 2.2450 100.000 64.000 63.280 0.720 0.8485 99.700 1064.000 1062.560 1.440 1.2000 100.000 *" I I I I I I 48 6 5247 5672 6101 6535 6973 ACTIVITY pCi/G 7.07E-02 2.49E+01 1.50E+OO 2.50E+01 I 7416 82.275 N/A 77.926 1.0039 1.96-sigma 1.96-sigma TPU MDA Le en! Unc pCi/G pCi/G pCi/G pCi/G 1.76E-01 3.15E-01 1.28E-01 1.76E-01 3.36E+OO 2.99E-01 1.14E-01 1.51E+OO 4.17E-01 1.57E-01 4.33E-02 3.76E-01 3.37E+OO 1.93E-01 6.10E-02 1.51E+OO NOTES: *Results are a compilation of S1203633744_UU and T1203633744_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.033 +/-0.001)

BATCH NUMBER : 1601257 SAMPLE ID : S1203633744 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.111 G -+/-0.901 % CHAMBER : 010 DETECTOR S/N : 72529 AVERAGE %EFFICIENCY : 30.8196 AVERAGE %EFF ERROR : 0.5949 SAMPLE DATE : 27-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 77.9 +/-4.811 % TRACER ID 1564-1 NUCLIDE U-232 NOMINAL 4.6164E+OO dpm RESULTS 3.5974E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5305.41 42.918 U-3/4 4763.02 4762.11 65.372 U-235 4391.00 4437.62 190.144 U-238 4184.73 4191.08 54.093 91 U-238: 39744284 keV U-235:43104581keV 82 U-3!4:4592-4865keV U-232:5000-5398keV 73 64 55 en 46 1--z ::i 37 0 s 28 19 *:;; 10 1 2411 Energy (keV) COUNT DATE : 29-Sep-2016 14:04:46 ELAPSED LIVE TIME(SEC) : 43200.00 LCS ID 1600-E NUCLIDE U-238 NOMINAL (pCi/G) 2.4265E+01 % RECOVERY 102.768 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 827.000 798.200 28.800 5.3666 100.000 1.87E+01 1064.000 1058.960 5.040 2.2450 100.000 2.49E+01 64.000 63.280 0.720 0.8485 99.700 1.49E+OO 1064.000 1062.560 1.440 1.2000 100.000 2.49E+01 6122 6555 6992 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B010.CNF;1843 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W010.CNF;513 CAL DATE : 27-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.35E+OO 6.14E-01 2.72E-01 2.97E+OO 2.98E-01 1.14E-01 4.05E-01 1.57E-01 4.31E-02 2.98E+OO 1.92E-01 6.08E-02 1.96-sigma cnt Unc pCi/G 1.34E+OO 1.50E+OO 3.75E-01 1.50E+OO Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 satch#_l'5_q_lP_L_-l_0_'6'_ Product: ____ Date:_9 I . ' Criteria: Yes No Comments Sample SPlids are less than or equal to 100 mq for GAB. Ud-Samples have been blank corrected (If required). 1-Jd. Blank correction renorted Included flf reouiredl. If actiVitv less than lOx MDA/MDC, error is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. v IIf hnlnm *ha MDA/ Mnr n*rn* I<: Instrument source check Is within limits. Instrument hkn ch,,..,k lo:: within .... ,/ Method RDL/ LLD has been met. / If duplicate activities are: Less than 5* MDA/ MDC, the11 RPD Is 100% or less, / If greater 5* MDA/ MDC, then RPD 20% or less, fuM_ (ill_rraf1ut) If below the MDA/ MDC, the RPD Is 0%, Or meets the client's reoulred RER accentance criteria. Tracer Yield Is 15-125%. Carrier yield 25-125%. i/ (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. v < 50/n of lnmne* actlvltvl Samole was run within hold time. v Samnle was correctlv nreserved If reoulred. . LW--Smears Taken for Radioactive batches. MO--Method Spike and LCS are within 75-125% ./" (or me<>t" the client's cont=l!f' acc .. nt;,nre rrlt .. rlal. No blank spaces on data forms. / All line outs lnltlaled and dated. '"'" llCllPPr.Pll"! ....... ,...,, .. a.,, .. Aux data Is correct. fl..'lB-Client Sneclal renulrements naae has been checked. ,,,... Raw Data and/ or soectrum are Included and orooerlv statused. .,,..--. MS, LCS, and Duplicate RPD/RER values uploaded to UMS and v* Hit-(If ,, U?-. n_ .. _..., .... _ ............ .a lntn ,. __ .... ** **,.n .,-Batch Data Exception Reoorts mERl completed If aPPlicable. .... n l1l1..U.. 1 Batch Data Exception Reports (DER) second reviewed. ...... 1-'BL< Dlsoosltlon verified to be comoleted. Ali""° Corr0,...ion If l IP\-Review sample historical results If available / (If REMP, results above MDC have been verified bv historical results. recount or re-analvsls. \ Primary Review Pertor:med sy: __ _____ --+J_1>/;. ___ ____ _ Secondary Review Performed By:__ 09/30/16 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 29-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER HASL-300, U-02-RC Solid Batch ID: Sample Numbers: 1596408 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. 1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, and 1203621740 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 29-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 495 of 5809 DER Report No.: 1562825 Revision No.: Type: Process Client Code: MJWC Uranium Que Sheet ==================---------------Batch #: 1596408 Tracer Isotopt@u-236 LCS Isotope: U-238 Analyst: HAKB Tracer Code: \ '5k'1 -.J:. LCS Code: \ Spike Isotope: U-23 Spike Code: ______ _ Prep Date:_._......,,,""'-'-'-\(..,"""---Initials: Pipet ID: 07-SEP-16 First Client Due Date:04-0CT-16 Internal Due Date:30-SEP-16 Expiration Analyzed Sequentially with Pu Analyzed Sequentially with: Expiration Pu-236 Pu: _lf59 laY.1 2.... Date: -Vol: -Am: I SC? (o 4 t (:) . \f(lf Balance ID: I l. \ o-i \,, I.., L.... Witness: '1/aalf,1 i , Wet!@ Hazard Collection Date Label Aliquot # @)'I!f) u Det# Sample ID Client Description Type Code MinCRDL 405235041-1 4.4D.R.1.4 SAMPLE 1 pCi/g 405235042-1 4.4D.R.2.3 SAMPLE 1 pCi/g 405235043-1 4.4D.R.2.4 SAMPLE 1 pCi/g 405235044-1 4.4D.R.4.2 SAl\IPLE lpCi/g 405235045-1 4.4D.R.5.2 SAMPLE 1 pCi/g 405235046-1 4.5A.R.l.3 SAMPLE lpCi/g 4052.15047-1 4.5A.R.l.4 SAMPLE 1 pCi/g 405235048-1 4.;,"B.R.1.2 SAMPLE 1 pCi/g 405235049-1 4.5B.R.1.3 SAMPLE lpCi/g 405235050-1 4.SB.R.1.4 SAl\IPLE 1 pCi/g 40.illSQSJ I "SB Ro SAHl?l.li: 1 pCUg 405235052-1 4.SB.R.2.4 SAMPLE 1 pCi/g 405235053-1 4.5C.R.5.2 SAMPLE lpCi/g 405235054-1 4.5C.R.1.3 SAMPLE 1 pCi/g 405235055-1 4.5C.R.1.4 SAMPLE 1 pCi/g 405235056-1 4.5C.R.2.2 SAMPLE 1 pCi/g 405235057-1 4.SC.R.2.3 SAMPLE 1 pCi/g 405235058-1 4.5C.R.2.4 SAMPLE 1 pCi/g 405235059-1 S.lA.R.1.2 SAl\*IPLE 1 pCi/g 405235060-1 5.lA.R.1.3 SAMPLE 1 pCi/g 1203621739-1 l\-IB for batch 1596408 l\IB lpCi/g 1203621740-1 4.4D.R.1.4(405235041DUP) DUP 1 pCi/g 1203621741-1 LCS for batch 1596408 LCS 1 pCi/g Choose SOP used: GL-RAD-A-011 Solid Sample Dissolution by: GEL Uiboratories LLC, Radiochemistry Division Matrix Client SOIL MJWCOOl SOIL MJWCOOl SOIL l\UWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL-l\UWCOOl SOIL MJWCOOl son MJ1(;001 SOIL M.JWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL J\JJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL QC ACCOUNT LEACH o\:..m.GESTi@ Circle One 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 91'*BEC*15 07-DEC-15 01-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 16*DEC-15 16-DEC-15 30-NOV-15 Pos. 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Page 1 of 1 Uranium Que Sheet \f'.-07-SEP-16 Batch#: 1596408 Analyst: HAKB First Client Due Date:04-0CT-16 Internal Due Date:30-SEP-16 Tracer Isotope: Tracer Code: \ziJ O -t: Expiration Date: 7 \ iS \ l=j-*) Analyzed Sequentially with Pu Analyzed Sequentially with: LCS Isotope: U-238 LCS Code: -Expiration Date: --Vol:--==--. Pu-236 ID: __/ Pu: Spike Isotope: U-238 Spike Code:_______ Expiration Date: --Vol:--===_ Vol.: Prep Date: orh--0 \ \ '9 Initials:d.ftW..h Pipet ID: Q:-7,., Balance ID: jla\'D:J Co (0 > ,, Witness: :5-t-n q/a c IJ{? \I , Wet!@> Aliquot Hazard Sample ID Client Description Type Code MinCRDL 405235041-1 4.4D.R.1.4 SAMPLE 1 pCi/g 405235042-1 4.4D.R.2.3 SAMPLE 1 pCi/g 405235043-1 4.4D.R.2.4 SAMPLE 1 pCi/g 405235044*1 4.4D.R.4.2 SAMPLE 1 pCi/g 405235045-1 4.4D.R.S.2 SAMPLE 1 pCi/g 405235046-1 4.SA.R.1.3 SAMPLE 1 pCi/g 405235047-1 4.SA.R.1.4 SAMPLE 1 pCi/g 405235048-1 4.SB.R.1.2 SAMPLE 1 pCi/g 405235049-1 4.5B.R.1.3 SAMPL;E lpCi/g 405235050-1 4.sB.IU.4 SAMPLE 1 pCi/g 4i!!::!:SSUSl-1 SAMPLE 1 pCilg 405235052-1 4.SB.R.2.4 SAMPLE 1 pCi/g 405235053-1 4.SC.R.S.2 SAMPLE 1 pCi/g 405235054-1 4.SC.R.q SAMPLE l pCifg 405235055-1 4.5C.R.1.4 SA-'"\fPLE l pCi/g 405235056-1 4.5C.R.2.2 SAMPLE l pCi/g 405235057-1 4.SC.R.2.3 SAMPLE 1 pCi/g 405235058-1 4.SC.R.2.4 SAMPLE I pCi/g 405235059-1 S.lA.R.1.2 SAMPLE 1 pCi/g 405235060-1 5.lA.R.1.3 SAi"\fPLE 1 pCifg 1203621739-1 l'vIB for batch 1596408 IVIB 1 pCifg 1203621740-1 4.4D.R.1.4(405235041DUP) DUP 1 pCi/g 1203621741-1 LCS for batch 1596408 LCS I pCi/g Choose SOP used: GL-RAD*A-011 Solid Sample Dissolution by: GEL Laboratories LLC, Radiochemistry Divisio11 Matrix Client SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl sou lltJV1'C66l SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL 1\UWCOOl SOIL .lVUWCOOl SOIL MJWC001 SOIL MJWC001 SOIL MJWCOOl SOIL MJWCOOl SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL QC ACCOUNT LEACH orQ?ffi"ESTI28> Circle One Collection Date 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 97BEC15 07-DEC-15 01-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 16-DEC-15 16-DEC-15 30-NOV-15 Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Label # <fi) I/ f) u Det# sc3 i ' 4 ,I 14Y J ! ! I i ____ . i n ¢.so"]-! flf..* Page 1 of 1 Alpha Spectroscopy Software Version 3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596408 SAMPLE ID : T0405235041_UU SAMPLE QTY : 0.509 G +/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 016 DETECTOR S/N : 78774 AVERAGE %EFFICIENCY : 33.4185 AVERAGE %EFF ERROR : 0.6439 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B016.CNF;1809 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 83.9 +/-7.998 % COUNT DATE : 22-Sep-2016 14:24:56 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W016.CNF;494 CAL DATE : 27-Aug-2016 SECONDARYQTY: 0.511G +/-0.196% TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 8.0518E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY en I-z => 0 s *s; ts <! ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U.238:3974-4284keV U-235: 4310-4581 keV 37 U-Jf4:4592-486SkeV U-232:5000-5398keV 33 29 25 21 17 13 9 5 2399 2793 3192 Energy (keV) ID 1570-E 1564-1 PEAK ENERGY 5251.75 4739.26 4451.57 4166.24 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 643.85 0.96 PEAK NET2 1.35 308.52 RECOVERY YIELD CORR. 11.1230 dpm 4451.57 4496.89 4.6549 dpm 5251.75 5306.36 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA StDev 0.000 6.000 0.960 5.040 2.2450 100.000 60.781 61.000 59.821 1.179 1.0860 100.000 80.309 3.000 1.349 1.651 1.2849 99.700 5.711 53.000 52.528 0.472 0.6868 100.000 ACTIVITY pCi/G 1.47E-02 8.02E-01 1.81E-02 7.04E-01 7443 1.96-sigma TPU pCi/G 8.66E-02 2.44E-01 5.56E-02 2.24E-01 NOTES: MDA pCi/G 1.72E-01 9.34E-02 1.03E-01 7.39E-02 72.172 N/A 84.905 1.0118 Le pCi/G 6.31E-02 2.66E-02 3.16E-02 1.68E-02 1.96-sigma cnt Unc pCi/G 8.65E-02 2.07E-01 5.55E-02 1.93E-01 *Results are a compilation of S0405235041_UU and T0405235041_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235041_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 015 DETECTOR S/N : 80055 AVERAGE %EFFICIENCY : 33.3682 AVERAGE %EFF ERROR : 0.6430 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 84.9 +/-6.550 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.9523E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5306.36 U-3/4 4763.02 4752.50 U-235 4391.00 4496.89 U-238 4184.73 4189.58 31 U-238: 3974-4284 keV U-235: 4310-4581 keV 28 U-314:4592-4665keV U-232:5000-5398keV 25 22 19 16 z 13 => 0 s 10 7 *::; 4 2386 2781 Energy (keV) PEAK FWHM 33.296 24.340 211.442 20.489 COUNT DATE : 22-Sep-2016 10:00:17 ELAPSED LIVE TIME(SEC) : 14151.84 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 313.000 308.519 4.481 2.1169 100.000 4.12E+OO 61.000 59.821 1.179 1.0860 100.000 7.92E-01 3.000 1.349 1.651 1.2849 99.700 1.79E-02 53.000 52.528 0.472 0.6868 100.000 6.96E-01 6549 6990 7436 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B015.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W015.CNF;530 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.21E-01 1.43E-01 5.17E-02 2.31E-01 9.23E-02 2.63E-02 5.49E-02 1.02E-01 3.12E-02 2.13E-01 7.30E-02 1.66E-02 1.96-sigma cnt Unc pCi/G 4.65E-01 2.05E-01 5.49E-02 1.91E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235042 UU SAMPLE QTY : 0.500 G -+/-0.200 % SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 88.1 +/-9.851 % SECONDARY QTY : 0.501 G +/-0.200 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0487E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 132 DETECTOR S/N : 67579 AVERAGE %EFFICIENCY : 26.0712 AVERAGE %EFF ERROR : 0.5050 COUNT DATE : 22-Sep-2016 10:03:28 ELAPSED LIVE TIME(SEC) : 8725.74 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B132.CNF;1156 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W132.CNF;324 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230dpm 4481.52 4484.88 4.6549dpm 5172.94 5307.10 PEAK NET 1 396.42 0.13 PEAKNET2 2.47 181.23 RECOVERY YIELD CORR. 93.999 N/A 88.926 1.0090 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5172.94 4.940 1.000 U-3/4 4763.02 4771.65 32.933 28.000 U-235 4391.00 4481.52 37.393 3.000 U-238 4184.73 4187.91 39.520 28.000 37 U-238:3974-4264keV U-235: 43104581 keV U-3/4:4592-4865keV 33 U-232:5000-5398keV 29 25 00 21 I-17 z => 0 13 !:2. .?;-9 *:;; :g 5 <( 2382 2780 3180 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.127 0.873 0.9341 100.000 3.24E-03 25.887 2.113 1.4537 100.000 5.99E-01 2.472 0.528 0.7269 99.700 5.74E-02 27.472 0.528 0.7269 100.000 6.36E-01 5665 6092 6523 6958 7396 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.32E-02 1.60E-01 4.18E-02 7.31E-02 2.73E-01 1.87E-01 5.89E-02 2.46E-01 9.27E-02 1.29E-01 2.96E-02 9.20E-02 2.75E-01 1.28E-01 2.95E-02 2.45E-01 NOTES: *Results are a compilation of S0405235042_UU and T0405235042_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235042 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 016 DETECTOR S/N : 78774 AVERAGE %EFFICIENCY : 33.4185 AVERAGE %EFF ERROR : 0.6439 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 88.9 +/-8.139 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 4.1395E+OO dpm NUCLIDE LIBRARY PEAK 00 I-z ::i 0 .?;-u <!'. ENERGY ENERGY U-232 5302.10 5307.10 U-3/4 4763.02 4749.95 U-235 4391.00 4484.88 U-238 4184.73 4201.81 lJ.238:3974-4284keV 15 U-235:4310-4581 keV U-314: 45924865 keV U-232:5000-S398keV 13 11 9 7 5 3 2399 2793 3192 3596 Energy (keV) PEAK FWHM 33.042 117.484 171.330 29.371 COUNT DATE : 22-Sep-2016 10:00:17 ELAPSED LIVE TIME(SEC) : 7925.02 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 184.000 181.226 2.774 1.6655 100.000 4.19E+OO 28.000 25.887 2.113 1.4537 100.000 5.94E-01 3.000 2.472 0.528 0.7269 99.700 5.69E-02 28.000 27.472 0.528 0.7269 100.000 6.31E-01 6555 6997 7443 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B016.CNF;1809 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W016.CNF;494 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.24E-01 2.04E-01 6.75E-02 2.62E-01 1.86E-01 5.84E-02 9.17E-02 1.28E-01 2.93E-02 2.64E-01 1.27E-01 2.92E-02 1.96-sigma cnt Unc pCi/G 6.18E-01 2.43E-01 9.12E-02 2.43E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235043 UU SAMPLE QTY : 0.507 G -+/-0.197 % SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 85.6 +/-10.358 % SECONDARY QTY : 0.513 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.9608E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 133 DETECTOR S/N : 76229 AVERAGE %EFFICIENCY : 25.5293 AVERAGE %EFF ERROR : 0.4948 COUNT DATE : 22-Sep-2016 10:03:29 ELAPSED LIVE TIME(SEC) : 8665.95 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B133.CNF;1153 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W133.CNF;359 CAL DATE : 08-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4485.26 4394.55 TRACER2 1564-1 U-232 4.6549 dpm 5198.57 5305.58 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5198.57 0.000 0.000 -0.867 0.867 0.9309 100.000 U-3/4 4763.02 4765.31 30.640 30.000 29.339 0.661 0.8128 100.000 U-235 4391.00 4485.26 25.416 3.000 2.604 0.396 0.6296 99.700 U-238 4184.73 4189.07 26.500 29.000 28.471 0.529 0.7270 100.000 U-238*3974-4Z84k v 41 -. U-235:431o-4581 keV 37 U-3/4:4592-4865keV "'""U-232:5000.5398keV 33 I-29 I-25 I-Ui 21 I-I-z :J 17 -0 s 13 I-9 *:;; I-u 5 <( I-J.il j I-I I I I I 23 63 2763 3166 3573 3rn3 397 48 5 5237 5663 6092 6525 6961 -Energy {keV) ACTIVITY pCi/G -2.33E-02 7.61E-01 6.77E-02 7.39E-01 I 7402 366.18 2.60 89.283 N/A -0.87 159.43 86.341 1.0082 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCl/G pCi/G pCi/G 5.67E-02 1.69E-01 4.41E-02 5.64E-02 3.24E-01 1.52E-01 3.69E-02 2.84E-01 1.04E-01 1.35E-01 2.87E-02 1.03E-01 3.18E-01 1.44E-01 3.30E-02 2.79E-01 NOTES:

Results are a compilation of S0405235043_UU and T0405235043_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235043 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 017 DETECTOR S/N : 78791 AVERAGE %EFFICIENCY :*30.2659 AVERAGE %EFF ERROR : 0.5843 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 86.3 +/-8.633 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 4.0191 E+OO dpm NUCLIDE LIBRARY en I-z ::i 0 8 *:;; ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U*238: 3974-4284 keV 15 U-235: 4310-4581 keV U-J/4:4592-486SkeV U*232:5000-5398keV 13 11 9 7 5 3 2382 2779 3181 Energy (keV) PEAK ENERGY 5305.58 4752.58 4394.55 4188.23 PEAK FWHM 47.283 17.268 152.949 34.537 COUNT DATE : 22-Sep-201610:00:17 ELAPSED LIVE TIME(SEC) : 7928.65 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 163.000 159.432 3.568 1.8889 100.000 4.14E+OO 30.000 29.339 0.661 0.8128 100.000 7.55E-01 3.000 2.604 0.396 0.6296 99.700 6.72E-02 29.000 28.471 0.529 0.7270 100.000 7.33E-01 6553 6994 7440 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B017.CNF;2655 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W017.CNF;1450 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.69E-01 2.49E-01 8.58E-02 3.10E-01 1.50E-01 3.66E-02 1.03E-01 1.34E-01 2.84E-02 3.04E-01 1.43E-01 3.27E-02 1.96-sigma cnt Unc pCi/G 6.52E-01 2.81E-01 1.02E-01 2.77E-01 "'Cl Lil 0 AlphaSpectroscopySoftwareVersionJ.5.3 .J:::.. effectlvedate:02-Mar-2015 0 ....., BATCH NUMBER : 1596408 SAMPLE ID : T0405235044 UU SAMPLE QTY : 0.505 G -+/-0.198 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 134 DETECTOR S/N : 76230 AVERAGE %EFFICIENCY : 25.7389 AVERAGE %EFF ERROR : 0.4988 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B134.CNF;1149 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 76.3 +/-10.474 % COUNT DATE : 22-Sep-2016 10:03:32 ELAPSED LIVE TIME(SEC) : 8669.78 EFF FILE : W134.CNF;336 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.506 G +/-0.198 % TRACER ID : 1570"E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0959E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 34 U-238: 3974-4284 keV U-235: 43104581 keV 31 U-314:4592-4865keV U-232:5000-5398keV 28 25 22 (j) 19 1--16 z :J 13 0 f2. 10 .;:. 7 *;; u 4 <( Energy (keV) ID 1570-E 1564-1 PEAK ENERGY 5198.58 4778.84 4489.44 4198.30 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 406.38 -0.29 PEAKNET2 4.60 147.09 RECOVERY YIELD CORR. 11.1230 dpm 4489.44 4431.16 4.6549 dpm 5198.58 5301.90 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA SIDev 0.000 0.000 -0.289 0.289 0.5376 100.000 27.281 34.000 33.075 0.925 0.9620 100.000 52.082 5.000 4.603 0.397 0.6298 99.700 40.177 32.000 31.207 0.793 0.8907 100.000 5679 6107 6539 6974 ;\ ;\ ACTIVITY pCi/G -7.10E-03 9.34E-01 1.30E-01 8.81E-01 7413 1.96-sigma TPU pCi/G 4.99E-02 3.82E-01 1.39E-01 3.68E-01 NOTES: MDA pCi/G 1.20E-01 1.80E-01 1.47E-01 1.73E-01 98.234 N/A 76.913 1.0082 Le pCi/G 2.32E-02 4.75E-02 3.12E-02 4.40E-02 1.96-sigma en! Unc pCi/G 4.96E-02 3.28E-01 1.37E-01 3.18E-01 *Results are a compilation of S0405235044_UU and T0405235044_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235044 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 018 DETECTOR S/N : 78782 AVERAGE %EFFICIENCY : 31.3297 AVERAGE %EFF ERROR : 0.6044 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 76.9 +/-8.932 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.5802E+OO dpm NUCLIDE LIBRARY PEAK Ci) 1--z ::i. 0 *:;: ENERGY ENERGY U-232 5302.10 5301.90 U-3/4 4763.02 4762.96 U-235 4391.00 4431.16 U-238 4184.73 4191.79 19 lJ.238: 3974-4284 keV lJ.235: 4311>-4581 keV 17 U*314:4592-4865keV U-232:5000-5398keV 15 13 11 9 7 5 3 2380 2776 3176 3581 Energy (keV) PEAK FWHM 61.367 45.897 172.113 31.144 COUNT DATE : 22-Sep-2016 10:00:17 ELAPSED LIVE TIME(SEC) : 7932.85 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 150.000 147.091 2.909 1.7055 100.000 4.15E+OO 34.000 33.075 0.925 0.9620 100.000 9.26E-01 5.000 4.603 0.397 0.6298 99.700 1.29E-01 32.000 31.207 0.793 0.8907 100.000 8.74E-01 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B018.CNF;1810 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W018.CNF;484 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.01E+OO 2.53E-01 8.43E-02 3.65E-01 1.78E-01 4.71E-02 1.38E-01 1.46E-01 3.10E-02 3.52E-01 1.71E-01 4.36E-02 1.96-sigma cnt Unc pCi/G 6.81E-01 3.25E-01 1.36E-01 3.16E-01 'i:I Jq C\) U\ 0 '""" BATCH NUMBER : 1596408 SAMPLE ID : T0405235045 UU g SAMPLE QTY : 0.502 G -+/-0.199 % SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 76.5 +/-11.199 % SECONDARY QTY : 0.513 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 6.8523E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 139 DETECTOR S/N : 76231 AVERAGE %EFFICIENCY : 24.8887 AVERAGE %EFF ERROR : 0.4828 COUNT DATE : 22-Sep-2016 10:03:34 ELAPSED LIVE TIME(SEC) : 8688.31 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B139.CNF;1107 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W139.CNF;334 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAK NET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4477.49 4476.83 246.22 2.87 61.420 N/A TRACER2 1564-1 U-232 4.6549 dpm 5198.53 5301.23 -0.87 146.54 77.154 1.0082 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G U-232 5302.10 5198.53 0.000 0.000 -0.869 0.869 0.9321 100.000 -3.47E-02 8.44E-02 2.51E-01 6.56E-02 8.39E-02 U-3/4 4763.02 4749.55 46.895 32.000 31.338 0.662 0.8138 100.000 8.93E-01 3.78E-01 1.67E-01 4.06E-02 3.21E-01 U-235 4391.00 4477.49 67.566 3.000 2.868 0.132 0.3639 99.700 8.20E-02 1.14E-01 1.22E-01 1.82E-02 1.13E-01 U-238 4184.73 4195.38 32.086 33.000 32.868 0.132 0.3639 100.000 9.37E-01 3.87E-01 1.22E-01 1.82E-02 3.26E-01 NOTES: *Results are a compilation of S0405235045_UU and T0405235045_UU. >

The following nuclide results were quantified from the U-235 traced sample: U-232 21 U-238:3974-4284keV
Correction made to the following net area U-235:431D-4581keV 19 U-3/4:4592-4665keV due to tracer impurity: U-232:5000.-5398keV U-238 (0.004 +/-0.000) 17 15 13 Ci) 11 I-z 9 ::::> 0 7 5 *::; t5 3 <( 2388 2785 3186 3591 5679 6109 6543 6981 7423 Energy (keV) 1'l ;) ;)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235045 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 020 DETECTOR S/N : 78787 AVERAGE %EFFICIENCY : 31.0619 AVERAGE %EFF ERROR : 0.5993 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 77.2 +/-8.905 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.5915E+OO dpm NUCLIDE LIBRARY PEAK z => 0 8 u <( ENERGY ENERGY U-232 5302.10 5301.23 U-3/4 4763.02 4748.95 U-235 4391.00 4476.83 U-238 4184.73 4185.77 13 U-238: 3974-4284 keV U-235:431Cl-4581 keV 12 U-314:4592-4865keV U.232:5000-5398keV 11 10 9 8 7 6 5 4 3 2 1 2401 2798 3198 3602 Energy (keV) PEAK FWHM 63.056 8.643 158.036 30.455 COUNT DATE : 22-Sep-2016 10:00:19 ELAPSED LIVE TIME(SEC) : 7946.44 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 148.000 146.543 1.457 1.2070 100.000 4.18E+OO 32.000 31.338 0.662 0.8138 100.000 8.86E-01 3.000 2.868 0.132 0.3639 99.700 8.13E-02 33.000 32.868 0.132 0.3639 100.000 9.29E-01 6526 6958 7393 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B020.CNF;1831 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W020.CNF;560 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.01E+OO 2.06E-01 6.02E-02 3.56E-01 1.65E-01 4.03E-02 1.13E-01 1.21E-01 1.81E-02 3.63E-01 1.21E-01 1.80E-02 1.96-sigma cnt Unc pCi/G 6.82E-01 3.19E-01 1.12E-01 3.23E-01 '"i;1 (1) U\ 0 AlphaSpectroscopySoftwareVerslon3.5.3 00 effectlvedate:02--Mar*2015 0 ...., BATCH NUMBER : 1596408 SAMPLE ID : T0405235046 UU SAMPLE QTY : 0.514 G -+/-0.195 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 78.9 +/-10.736 % SECONDARY QTY : 0.512 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 7.7532E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 140 DETECTOR S/N : 78771 AVERAGE %EFFICIENCY : 26.0317 AVERAGE %EFF ERROR : 0.5043 COUNT DATE : 22-Sep-2016 10:03:37 ELAPSED LIVE TIME(SEC) : 8691.66 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B140.CNF;1100 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W140.CNF;283 CAL DA TE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4493.36 4409.17 4.6540 dpm 5255.03 5280.18 PEAK NET 1 291.49 0.42 PEAK NET 2 1.73 155.28 RECOVERY YIELD CORR. 69.495 N/A 79.798 1.0115 NUCLIDE LIBRARY PEAK en I-z :J 0 s a *;;: t5 <( ENERGY' ENERGY U-232 5302.10 5255.03 U-3/4 4763.02 4759.31 U-235 4391.00 4493.36 U-238 4184.73 4209.65 U-238:3974-42841wV 33 U-235:4310-4581 keV U-314: 45924865 keV U-232:S000-5398keV 29 25 21 17 13 9 5 2385 2784 3186 3592 Energy (keV) PEAK GROSS FWHM AREA 4.953 1.000 64.386 25.000 34.422 2.000 24.764 30.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.421 0.579 0.7612 100.000 1.42E-02 24.470 0.530 0.7280 100.000 6.45E-01 1.735 0.265 0.5148 99.700 4.59E-02 29.867 0.133 0.3640 100.000 7.87E-01 5681 6110 6543 6981 7422 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 9.65E-02 1.92E-01 4.53E-02 9.62E-02 2.98E-01 1.46E-01 3.36E-02 2.64E-01 9.11E-02 1.27E-01 2.38E-02 9.05E-02 3.33E-01 1.13E-01 1.68E-02 2.88E-01 NOTES: *Results are a compilation of S0405235046_UU and T0405235046_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.004 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235046 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G -+/-0.195 % CHAMBER : 021 DETECTOR S/N : 795159 AVERAGE %EFFICIENCY : 31.8082 AVERAGE %EFF ERROR : 0.6134 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 79.8 +/-8.686 % TRACER . ID 1564-1 NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 3.7138E+OO dpm NUCLIDE LIBRARY PEAK 0' z :::> 0 s. 0 *::; u .:i;: ENERGY ENERGY U-232 5302.10 5280.18 U-3/4 4763.02 4742.59 U-235 4391.00 4409.17 U-238 4184.73 4185.02 17 U-238:3974-4284keV lJ.235:4310-4581keV U-3/4:4592-4S65keV 15 U-232:50Q0..5398keV 13 11 9 7 5 3 2394 2788 3187 3590 Energy (keV) PEAK FWHM 63.836 72.165 83.173 13.862 COUNT DATE : 22-Sep-2016 10:00:19 ELAPSED LIVE TIME(SEC) : 7950.06 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 157.000 155.277 1.723 1.3124 100.000 4.08E+OO 25.000 24.470 0.530 0.7280 100.000 6.38E-01 2.000 1.735 0.265 0.5148 99.700 4.53E-02 30.000 29.867 0.133 0.3640 100.000 7.78E-01 > ! 5673 6104 6539 6978 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B021.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W021.CNF;537 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.62E-01 1.99E-01 6.03E-02 2.84E-01 1.45E-01 3.32E-02 8.99E-02 1.26E-01 2.36E-02 3.15E-01 1.11E-01 1.66E-02 1.96-sigma cnt Unc pCi/G 6.48E-01 2.61E-01 8.95E-02 2.85E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235047 UU SAMPLE QTY : 0.503 G -+/-0.199 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 77.9 +/-10.406 % SECONDARY QTY : 0.507 G +/-0.197 % TRACER . ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 8.2865E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 142 DETECTOR S/N : 42285 AVERAGE %EFFICIENCY : 26.5347 AVERAGE %EFF ERROR : 0.5139 COUNT DATE : 22-Sep-2016 10:03:39 ELAPSED LIVE TIME(SEC) : 8717.12 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B142.CNF;1100 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W142.CNF;306 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4492.37 4443.19 4.6540 dpm 5198.58 5301.65 PEAKNET1 318.49 -0.29 PEAKNET2 2.73 165.75 RECOVERY YIELD CORR. 74.275 N/A 78.525 1.0080 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.58 0.000 0.000 U-3/4 4763.02 4770.27 24.721 32.000 U-235 4391.00 4492.37 48.206 3.000 U-238 4184.73 4182.66 5.768 42.000 28 U-238:3974-4284keV U-235:4310-4581 keV 25 U*314:45924865keV U-232:5000-5398keV 22 19 (ii 16 I-13 z ::> 0 10 s c 7 *s; 4 <( 1 2382 2780 3181 3586 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY. AREA AREA StDev pCi/G -0.291 0.291 0.5390 100.000 -9.09E-03 31.204 0.796 0.8920 100.000 7.85E-01 2.735 0.265 0.5150 99.700 6.90E-02 41.735 0.265 0.5150 100.000 1.05E+OO 5664 6091 6521 6955 7393 1.96-sigma TPU pCi/G 6.35E-02 3.27E-01 1.01E-01 3.90E-01 NOTES: MDA pCi/G 1.53E-01 1.54E-01 1.21E-01 1.21E-01 Le pCi/G 2.97E-02 3.93E-02 2.27E-02 2.27E-02 1.96-sigma cnt Unc pCi/G 6.32E-02 2.84E-01 9.95E-02 3.23E-01

Results are a compilation of S0405235047 _UU and T0405235047 _UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.005 +/-0.000) 0 ....., Vi 00 0 '° BATCH NUMBER : 1596408 SAMPLE ID : S0405235047 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 024 DETECTOR S/N : 76542 AVERAGE %EFFICIENCY : 34.4760 AVERAGE %EFF ERROR : 0.6639 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 78.5 +/-8.452 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 3.6546E+OO dpm NUCLIDE LIBRARY PEAK (ii 1--z :J 0 .?;-*:; n <( ENERGY ENERGY U-232 5302.10 5301.65 U-3/4 4763.02 4757.02 U-235 4391.00 4443.19 U-238 4184.73 4188.06 12 U-238: 39744284 keV lJ.235:4310-4581 keV 11 U-314:4592-4865keV U-232:5000-5398keV 10 9 8 7 6 5 4 3 2 1 2399 2793 3191 3594 Energy (keV) PEAK FWHM 65.152 78.183 185.685 80.626 COUNT DATE : 22-Sep-2016 10:00:19 ELAPSED LIVE TIME(SEC) : 7956.34 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 168.000 165.746 2.254 1.5014 100.000 4.17E+OO 32.000 31.204 0.796 0.8920 100.000 7.78E-01 3.000 2.735 0.265 0.5150 99.700 6.84E-02 42.000 41.735 0.265 0.5150 100.000 1.04E+OO !! 6989 7435 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B024.CNF;1824 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W024.CNF;517 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.55E-01 2.08E-01 6.61E-02 3.11E-01 1.53E-01 3.90E-02 9.94E-02 1.20E-01 2.26E-02 3.66E-01 1.20E-01 2.25E-02 1.96-sigma cnt Unc pCi/G 6.41E-01 2.81E-01 9.87E-02 3.21E-01

"' U1 .....,.. AlphaSpectroscopySof\wateVerslon3.S.3 N effectlvedate:02*Mar*2015 0 '"" BATCH NUMBER : 1596408 SAMPLE ID : T0405235048 UU SAMPLE QTY : 0.507 G -+/-0.197 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST: HAKB CORRECTED% YIELD : 94.3 +/-10.687 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.9022E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 143 DETECTOR S/N : 65882 AVERAGE %EFFICIENCY : 22.7820 AVERAGE %EFF ERROR : 0.4430 COUNT DATE : 22-Sep-2016 10:03:42 ELAPSED LIVE TIME(SEC) : 8707.51 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B143.CNF;1096 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W143.CNF;291 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4496. 76 4483.50 4.6540 dpm 5198.59 5317.91 PEAK NET 1 326.41 -1.16 PEAK NET2 1.59 148.90 RECOVERY YIELD CORR. 88.758 N/A 95.056 1.0080 NUCLIDE LIBRARY PEAK z => 0 (2. *:;; u <t: ENERGY ENERGY U-232 5302.10 5198.59 U-3/4 4763.02 4775.14 U-235 4391.00 4496.76 U-238 4184.73 4209.68 U-238:3974-4284keV 31 U-235: 4310-4581 keV lJ.3/4:4592-4865keV U-232:S000-5398keV 28 25 22 19 16 13 10 7 4 2372 2767 3165 3567 3 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 83.548 34.000 26.014 2.000 31.945 32.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -1.161 1.161 1.0775 100.000 -3.57E-02 33.588 0.412 0.6418 100.000 9.33E-01 1.588 0.412 0.6418 99.700 4.42E-02 31.176 0.824 0.9076 100.000 8.66E-01 6907 7340 1.96-sigma TPU pCi/G 6.61E-02 3.79E-01 9.62E-02 3.64E-01 NOTES: MDA pCi/G 2.09E-01 1.46E-01 1.46E-01 1.72E-01 Le pCi/G 5.83E-02 3.13E-02 3.14E-02 4.42E-02 1.96-sigma cnt Unc pCi/G 6.58E-02 3.22E-01 9.57E-02 3.13E-01

Results are a compilation of S0405235048_UU and T0405235048_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.005 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235048 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 113 DETECTOR S/N : 80009 AVERAGE %EFFICIENCY : 24.7132 AVERAGE %EFF ERROR : 0.4794 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 95.1 +/-8.834 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 4.4240E+OO dpm NUCLIDE LIBRARY PEAK 'iii I-z :::> 0 *;; t5 <t: ENERGY ENERGY U-232 5302.10 5317.91 U-3/4 4763.02 4785.38 U-235 4391.00 4483.50 U-238 4184.73 4214.70 lJ.238:3974-4284keV 15 U.235: 43104581 keV U-Jf4:4592-4665keV lJ..232:5000-5398kaV 13 11 9 7 5 3 2387 2785 3186 3592 Energy (keV) PEAK FWHM 41.533 21.031 0.000 20.413 >> COUNT DATE : 22-Sep-2016 10:02:46 ELAPSED LIVE TIME(SEC) : 8237.28 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 150.000 148.902 1.098 1.0480 100.000 4.13E+OO 34.000 33.588 0.412 0.6418 100.000 9.25E-01 2.000 1.588 0.412 0.6418 99.700 4.39E-02 32.000 31.176 0.824 0.9076 100.000 8.59E-01 >> > > !l!l 5674 6102 6533 6968 7407 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B113.CNF;1165 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W113.CNF;318 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.93E-01 1.85E-01 5.11E-02 3.59E-01 1.45E-01 3.10E-02 9.53E-02 1.45E-01 3.11E-02 3.46E-01 1.70E-01 4.39E-02 1.96-sigma cnt Unc pCi/G 6.69E-01 3.20E-01 9.50E-02 3.11E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235049 UU SAMPLE QTY : 0.506 G -+/-0.198 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 100 +/-10.145 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0953E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 144 DETECTOR S/N : 75551 AVERAGE %EFFICIENCY : 26.3153 AVERAGE %EFF ERROR : 0.5097 COUNT DATE : 22-Sep-2016 10:03:44 ELAPSED LIVE TIME(SEC) : 8714.54 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B144.CNF;1101 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W144.CNF;297 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4488.87 4551.85 4.6540 dpm 5198.55 5291.92 PEAKNET1 417.36 -0.44 PEAK NET2 0.45 158.72 RECOVERY YIELD CORR. 98.173 N/A 100.989 1.0080 NUCLIDE LIBRARY PEAK 00 I-z :J 0 ;:. *:;: n <t: ENERGY ENERGY U-232 5302.10 5198.55 U-3/4 4763.02 4768.52 U-235 4391.00 4488.87 U-238 4184.73 4182.70 37 U-238:3974-4284kaV U-235:4310-4581 keV U.3/4:45924865keV 33 U-232:5000-5396keV 29 25 21 17 13 9 5 2389 2784 3183 3586 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 49.143 31.000 54.769 1.000 7.167 29.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.436 0.436 0.6601 100.000 -1.05E-02 29.622 1.378 1.1737 100.000 7.73E-01 0.449 0.551 0.7423 99.700 1.18E-02 28.587 0.413 0.6429 100.000 7.46E-01 5660 6086 6517 6951 7389 1.96-sigma TPU pCi/G 4.93E-02 3.30E-01 7.45E-02 3.19E-01 NOTES: MDA pCi/G 1.28E-01 1.86E-01 1.47E-01 1.37E-01 Le pCi/G 2.80E-02 5.38E-02 3.41E-02 2.94E-02 1.96-sigma cnt Unc pCi/G 4.91E-02 2.90E-01 7.43E-02 2.81E-01 *Results are a compilation of S0405235049_UU and T0405235049_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235049 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 114 DETECTOR S/N : 78258 AVERAGE %EFFICIENCY : 24.7116 AVERAGE %EFF ERROR : 0.4794 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST: HAKB % YIELD : 101 +/-8.566 % TRACER ID : 1564-1 NUCLIDE : U-232 NOMINAL : 4.6540E+OO dpm RESULTS : 4.7001 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5291.92 U-3/4 4763.02 4748.12 U-235 4391.00 4551.85 U-238 4184.73 4178.97 U-238:3974-4284keV 15 lJ.235:4310-4581 keV U-lr'4:4592-4865keV lJ..232:5000-5398keV 13 11 Ui 9 I-z 7 :l 0 !2. 5 *5 3 u <x: PEAK FWHM 53.498 7.430 4.954 28.483 COUNT DATE : 22-Sep-2016 10:02:49 ELAPSED LIVE TIME(SEC) : 8265.39 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 159.000 158.724 0.276 0.5249 100.000 4.14E+OO 31.000 29.622 1.378 1.1737 100.000 7.67E-01 1.000 0.449 0.551 0.7423 99.700 1.17E-02 29.000 28.587 0.413 0.6429 100.000 7.40E-01 > i§ a 2390 2788 3190 3595 4 04 417 48 3 5253 5676 6103 6534 6968 7406 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B114.CNF;1168 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W114.CNF;324 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.63E-01 1.26E-01 2.40E-02 3.17E-01 1.84E-01 5.33E-02 7.38E-02 1.46E-01 3.38E-02 3.06E-01 1.36E-01 2.92E-02 1.96-sigma cnt Unc pCi/G 6.47E-01 2.88E-01 7.37E-02 2.78E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235050 UU SAMPLE QTY : 0.504 G -+/-0.198 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 106 +/-9.889 % SECONDARY QTY : 0.510 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1602E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 145 DETECTOR S/N : 72526 AVERAGE %EFFICIENCY : 26.3634 AVERAGE %EFF ERROR : 0.5106 COUNT DATE : 22-Sep-2016 10:03:47 ELAPSED LIVE TIME(SEC) : 8694.70 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B145.CNF;1119 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W145.CNF;365 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4514.21 4402.30 441.91 0.73 103.995 N/A TRACER2 1564-1 U-232 4.6540 dpm 5369.63 5313.33 0.28 170.81 106.979 1.0095 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G U-232 5302.10 5369.63 4.914 1.000 0.275 0.725 0.8512 100.000 6.17E-03 6.42E-02 1.34E-01 3.36E-02 6.40E-02 U-3/4 4763.02 4804.32 78.618 24.000 23.178 0.822 0.9069 100.000 5.65E-01 2.64E-01 1.51E-01 3.88E-02 2.40E-01 U-235 4391.00 4514.21 59.100 1.000 0.726 0.274 0.5236 99.700 1.78E-02 6.89E-02 1.18E-01 2.25E-02 6.88E-02 U-238 4184.73 4215.68 76.161 27.000 26.726 0.274 0.5236 100.000 6.52E-01 2.84E-01 1.18E-01 2.24E-02 2.53E-01 NOTES: *Results are a compilation of S0405235050_UU and T0405235050_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232 !Q!:;J U-238:3974-4284keV
Correction made to the following net area 41 U-235: 431D4581 keV U-3/4:4592-4865keV due to tracer impurity: 37 U-232:5000-5398keV U-238 (0.007 +/-0.000) 33 29 en 25 I-21 z :J 17 0 s 13 9 *;; :g 5 <i: 1 2411 2806 3205 3608 5682 6108 6539 6973 7411 Energy (keV) :'l '"

BATCH NUMBER : 1596408 SAMPLE ID : S0405235050 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 115 DETECTOR S/N : 79995 AVERAGE %EFFICIENCY : 25.2291 AVERAGE %EFF ERROR : 0.4892 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 107 +/-8.343 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 4.9789E+OO dpm NUCLIDE LIBRARY PEAK z :::> 0 s *:;; u ENERGY ENERGY U-232 5302.10 5313.33 U-3/4 4763.02 4763.63 U-235 4391.00 4402.30 U-238 4184.73 4206.69 15 U-238: 3974-4284 keV U-235:431()-4581 keV U-3/4:4592-4865keV 13 V.232:5000-5398keV 11 9 7 5 3 2382 2782 3186 3593 Energy (keV) PEAK FWHM 46.613 8.294 4.976 8.709 COUNT DATE : 22-Sep-2016 10:02:51 ELAPSED LIVE TIME(SEC) : 8224.29 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 173.000 170.807 2.193 1.4809 100.000 4.16E+OO 24.000 23.178 0.822 0.9069 100.000 5.60E-01 1.000 0.726 0.274 0.5236 99.700 1.76E-02 27.000 26.726 0.274 0.5236 100.000 6.46E-01 6111 6543 6978 7417 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B115.CNF;1177 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W115.CNF;335 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.41E-01 2.00E-01 6.33E-02 2.55E-01 1.49E-01 3.84E-02 6.82E-02 1.17E-01 2.23E-02 2.73E-01 1.17E-01 2.22E-02 1.96-sigma cnt Unc pCi/G 6.30E-01 2.37E-01 6.81E-02 2.51E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235052 UU SAMPLE QTY : 0.508 G -+/-0.197 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 79.6 +/-10.921 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.9077E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 147 DETECTOR S/N : 75550 AVERAGE %EFFICIENCY : 25.4403 AVERAGE %EFF ERROR : 0.4932 COUNT DATE : 22-Sep-2016 10:03:52 ELAPSED LIVE TIME(SEC) : 8729.03 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B147.CNF;1091 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W147.CNF;294 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4499.39 4375.98 TRACER2 1564-1 U-232 4.6540 dpm 5198.59 5313.61 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA S!Dev U-232 5302.10 5198.59 0.000 0.000 -0.582 0.582 0.7628 100.000 U-3/4 4763.02 4773.91 50.558 30.000 28.892 1.108 1.0528 100.000 U-235 4391.00 4499.39 31.081 1.000 0.584 0.416* 0.6447 99.700 U-238 4184.73 4202.43 10.567 23.000 22.446 0.554 0.7444 100.000 U-238* 3974-4284 keV U-235:4310-4581 keV 37 -U-3/4; 4592-4865 keV U-232:5000-S398keV 33 29 if) 21 I-z 17 => -0 13 9 *::; -u 5 <( 1 -.. Ji -' ..J ' ' I' ' ' I I I 23 90 2790 3193 3600 41110 424 48 1 5262 5687 6115 6546 6981 -Energy (keV) ACTIVITY pCi/G -1.58E-02 9.00E-01 1.83E-02 6.99E-01 ' 7420 365.60 0.58 88.807 N/A -0.58 132.45 80.231 1.0080 1.96-sigma 1.96-sigma TPU MDA Le en! Unc pCi/G pCi/G pCi/G pCi/G 5.64E-02 1.55E-01 3.65E-02 5.60E-02 3.93E-01 2.09E-01 5.76E-02 3.41E-01 8.85E-02 1.64E-01 3.54E-02 8.83E-02 3.36E-01 1.75E-01 4.07E-02 3.00E-01 NOTES:

Results are a compilation of S0405235052_UU and T0405235052_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235052 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 117 DETECTOR S/N : 80003 AVERAGE %EFFICIENCY : 25.8068 AVERAGE %EFF ERROR : 0.5001 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 80.2 +/-9.289 % TRACER *.1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6540E+OO dpm 3.7340E+OO dpm NUCLIDE LIBRARY PEAK UJ I-z :::> 0 u <l: ENERGY ENERGY U-232 5302.10 5313.61 U-3/4 4763.02 4765.45 U-235 4391.00 4375.98 U-238 4184.73 4177.78 12 U-238: 3974-4284 keV U-235:43104581 keV 11 U-3/4:4592-4665keV U.232:5000-5398keV 10 9 8 7 6 5 4 3 2 1 2390 2787 3187 3592 Energy (keV) PEAK FWHM 39.437 67.782 4.930 55.458 >> .:l!l 1! is COUNT DATE : 22-Sep-2016 10:02:56 ELAPSED LIVE TIME(SEC) : 8312.94 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 133.000 132.446 0.554 0.7444 100.000 4.13E+OO 30.000 28.892 1.108 1.0528 100.000 8.93E-01 1.000 0.584 0.416 0.6447 99.700 1.81E-02 23.000 22.446 0.554 0.7444 100.000 6.94E-01 ]] > 5673 6101 6533 6970 7410 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B117.CNF;1162 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W117.CNF;308 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.04E+OO 1.75E-01 4.07E-02 3.77E-01 2.07E-01 5.71E-02 8.78E-02 1.63E-01 3.51E-02 3.24E-01 1.74E-01 4.04E-02 1.96-sigma cnt Unc pCi/G 7.07E-01 3.38E-01 8.76E-02 2.97E-01 "tl ._,, 3.5.3 0 '"" BATCH NUMBER : 1596408 SAMPLE ID : T0405235053 UU g SAMPLE QTY : 0.500 G -+/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 148 DETECTOR S/N : 74429 AVERAGE %EFFICIENCY : 24.2876 AVERAGE %EFF ERROR : 0.4715 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B148.CNF;1092 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 79.0 +/-11.113 % COUNT DATE : 22-Sep-2016 10:03:54 ELAPSED LIVE TIME(SEC) : 8735.45 EFF FILE : W148.CNF;312 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.0943E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 31 U-238:3974-42S4keV U-235:431D-4581 keV 28 lJ.3/4:4592-4865keV U-232:5000-5398keV 25 22 19 UJ 16 I-z 13 ;::) 0 s 10 ;:. 7 *:;; 4 2410 2804 3202 Energy {keV) ID 1570-E 1564-1 PEAK ENERGY 5250.22 4771.61 4493.89 4201.60 3604 4 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 320.62 -0.02 PEAKNET2 6.86 130.58 RECOVERY YIELD CORR. 11.1230 dpm 4493.89 4448.99 4.6548 dpm 5250.22 5301.43 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABLIN FWHM AREA AREA AREA StDev 4.899 1.000 -0.019 1.019 1.0095 100.000 13.064 37.000 36.168 0.832 0.9119 100.000 52.429 7.000 6.861 0.139 0.3723 99.700 79.609 40.000 39.584 0.416 0.6448 100.000 > : 11 422 48 6 5255 5679 6106 6538 6973 ACTIVITY pCi/G -5.99E-04 1.16E+OO 2.21E-01 1.27E+OO 7413 1.96-sigma TPU pCi/G 9.07E-02 4.66E-01 1.86E-01 4.92E-01 NOTES: MDA pCi/G 2.05E-01 1.99E-01 1.39E-01 1.69E-01 81.517 N/A 79.697 1.0082 Le pCl/G 5.57E-02 5.14E-02 2.10E-02 3.63E-02 1.96-sigma en! Une pCi/G 9.04E-02 3.89E-01 1.79E-01 4.03E-01

Results are a compilation of S0405235053_UU and T0405235053_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.005 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235053 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 118 DETECTOR S/N : 80061 AVERAGE %EFFICIENCY : 25.6062 AVERAGE %EFF ERROR : 0.4962 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 79.7 +/-9.343 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6548E+OO dpm 3.7097E+OO dpm NUCLIDE LIBRARY PEAK z => 0 0 *s: u <( ENERGY ENERGY U-232 5302.10 5301.43 U-3/4 4763.02 4751.17 U-235 4391.00 4448.99 U-238 4184.73 4188.46 10 U-238: 3974-4284 keV U-235:431()-4581 keV 9 lJ..314:4592-4865keV U-232:5000-5398keV 8 7 6 5 4 3 2 2384 2782 3183 3589 Energy (keV) PEAK FWHM 51.504 84.188 4.952 51.999 COUNT DATE : 22-Sep-2016 10:02:58 ELAPSED LIVE TIME(SEC) : 8315.75 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 131.000 130.584 0.416 0.6448 100.000 4.19E+OO 37.000 36.168 0.832 0.9119 100.000 1.15E+OO 7.000 6.861 0.139 0.3723 99.700 2.19E-01 40.000 39.584 0.416 0.6448 100.000 1.26E+OO 5671 6098 6529 6964 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B118.CNF;1171 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W118.CNF;318 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.07E+OO 1.69E-01 3.63E-02 4.42E-01 1.98E-01 5.10E-02 1.82E-01 1.38E-01 2.09E-02 4.64E-01 1.68E-01 3.61E-02 1.96-sigma cnt Unc pCi/G 7.23E-01 3.86E-01 1.78E-01 4.00E-01 "t:I Ul N AlphaSpectrtlsc:opySoftwareVersion3.5.3 N effedlvedate:02*Mat*2015 0 ....., BATCH NUMBER : 1596408 SAMPLE ID : T0405235054 UU g SAMPLE QTY : 0.500 G -+/-0.200 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 89.6 +/-10.974 % SECONDARY QTY : 0.500 G +/-0.200 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.2392E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 149 DETECTOR S/N : 33449 AVERAGE %EFFICIENCY : 25.2769 AVERAGE %EFF ERROR : 0.4901 COUNT DATE : 22-Sep-2016 10:03:57 ELAPSED LIVE TIME(SEC) : 8757.15 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B149.CNF;1102 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W149.CNF;305 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4481.90 4411.81 4.6547 dpm 5198.50 5314.76 PEAKNET1 339.83 -0.58 PEAKNET2 2.72 134.62 RECOVERY YIELD CORR. 82.815 N/A 90.321 1.0082 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.50 0.000 0.000 U-3/4 4763.02 4759.70 96.442 30.000 U-235 4391.00 4481.90 80.175 3.000 U-238 4184.73 4177.90 37.437 31.000 U-238: 3974-4284 keV U-235: 4310-4581 keV 28 U-3/4:4592-4865keV U-232:5000-5398keV 25 22 19 'iii 16 I-z 13 ::J 0 10 8 7 u 4 <( 1 2411 2804 3201 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G -0.584 0.584 0.7641 100.000 -1.74E-02 29.310 0.690 0.8307 100.000 9.13E-01 2.724 0.276 0.5254 99.700 8.51E-02 30.448 0.552 0.7430 100.000 9.48E-01 5676 6104 6536 6972 7413 1.96-sigma TPU pCi/G 6.16E-02 3.95E-01 1.25E-01 4.03E-01 NOTES: MDA pCi/G 1.69E-01 1.84E-01 1.51E-01 1.75E-01 Le pCi/G 4.00E-02 4.54E-02 2.88E-02 4.06E-02 1.96-sigma cnt Unc pCi/G 6.13E-02 3.41E-01 1.23E-01 3.46E-01

Results are a compilation of S0405235054_UU and T0405235054_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.005 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235054 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 119 DETECTOR S/N : 79450 AVERAGE %EFFICIENCY : 23.3886 AVERAGE %EFF ERROR : 0.4544 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 90.3 +/-9.251 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 4.2042E+OO dpm NUCLIDE LIBRARY PEAK 'Cii I-z =i 0 f2. c *s: u <{ ENERGY ENERGY U-232 5302.10 5314.76 U-3/4 4763.02 4770.78 U-235 4391.00 4411.81 U-238 4184.73 4205.64 14 U-238: 3974-4284 keV U-235:4310-4581 keV 13 U-314:45924865 keV 12 U-232:5000-5398keV 11 10 9 8 7 6 5 4 3 2 1 2387 2785 3187 3592 Energy (keV) PEAK FWHM 49.162 37.962 7.427 71.797 COUNT DATE : 22-Sep-2016 10:03:00 ELAPSED LIVE TIME(SEC) : 8281.53 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 136.000 134.620 1.380 1.1748 100.000 4.19E+OO 30.000 29.310 0.690 0.8307 100.000 9.06E-01 3.000 2.724 0.276 0.5254 99.700 8.44E-02 31.000 30.448 0.552 0.7430 100.000 9.41E-01 5678 6107 6539 6975 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B119.CNF;1176 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 . EFF FILE : W119.CNF;315 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.06E+OO 2.22E-01 6.42E-02 3.??E-01 1.83E-01 4.50E-02 1.23E-01 1.50E-01 2.86E-02 3.85E-01 1.73E-01 4.03E-02 1.96-sigma cnt Unc pCi/G 7.15E-01 3.38E-01 1.22E-01 3.43E-01 '"t:I (1) VI Version 3.5.3 0 '"" BATCH NUMBER : 1596408 SAMPLE ID : T0405235055 UU SAMPLE QTY : 0.510 G -+/-0.196 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 82.9 +/-8.476 % SECONDARY QTY : 0.502 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1037E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 150 DETECTOR S/N : 75552 AVERAGE %EFFICIENCY : 24.8352 AVERAGE %EFF ERROR : 0.4817 COUNT DATE : 22-Sep-201610:03:59 ELAPSED LIVE TIME(SEC) : 8764.54 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B150.CNF;1100 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W150.CNF;296 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230dpm 4494.59 4475.13 399.19 3.00 98.926 N/A TRACER2 1564-1 U-232 4.6547 dpm 5198.60 5309.33 -1.46 324.44 83.588 1.0082 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le en! Une ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G U-232 5302.10 5198.60 0.000 0.000 -1.461 1.461 1.2086 100.000 -3.68E-02 5.51E-02 1.83E-01 5.37E-02 5.49E-02 U-3/4 4763.02 4771.11 19.166 57.000 55.800 1.200 1.0954 100.000 7.07E-01 2.25E-01 8.89E-02 2.54E-02 1.90E-01 U-235 4391.00 4494.59 39.517 3.000 3.000 0.000 0.0000 99.700 3.81E-02 5.06E-02 3.81E-02 O.OOE+OO 5.02E-02 U-238 4184.73 4201.37 87.117 75.000 74.760 0.240 0.4899 100.000 9.47E-01 2.70E-01 6.08E-02 1.14E-02 2.17E-01 NOTES: *Results are a compilation of S0405235055_UU and T0405235055_UU. '! '! '! '! *The following nuclide results were quantified from the U-235 traced sample: i ;i; i ffi U-232 U-238:3974-4284keV

Correction made to the following net area 41 U-235:4310-4581 keV U-314:4592-4865keV due to tracer impurity: 37 U-232:5000-5398keV U-238 (0.006 +/-0.000) 33 29 'Ci) 25 I-21 z :::i 17 0 13 1:-9 *;; u 5 <( 1 2390 2790 3193 5264 5688 6117 6548 6983 7422 Energy (keV)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235055 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 013 DETECTOR S/N : 78790 AVERAGE %EFFICIENCY : 35.0288 AVERAGE %EFF ERROR : 0.6744 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 83.6 +/-6.423 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 3.8908E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5309.33 U-3/4 4763.02 4759.22 U-235 4391.00 4475.13 U-238 4184.73 4191.13 U-238: 3974-4284 keV U-235:4311l-4581keV 28 U.3/4:4592-4865keV U-232:SOOQ..5398keV 25 22 19 'iii 16 1--z 13 ::::> 0 10 7 *:; t5 4 <( 1 2395 2793 3196 3604 Energy (keV) PEAK FWHM 41.698 52.019 113.947 57.799 i; COUNT DATE : 22-Sep-2016 14:24:56 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 329.000 324.440 4.560 2.1354 100.000 4.11E+OO 57.000 55.800 1.200 1.0954 100.000 7.01E-01 3.000 3.000 0.000 0.0000 99.700 3.78E-02 75.000 74.760 0.240 0.4899 100.000 9.40E-01 >> i 7020 7467 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B013.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W013.CNF;513 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.05E-01 1.37E-01 4.96E-02 2.10E-01 8.81E-02 2.52E-02 5.00E-02 3.78E-02 O.OOE+OO 2.48E-01 6.03E-02 1.13E-02 1.96-sigma cnt Unc pCi/G 4.52E-01 1.88E-01 4.98E-02 2.15E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235056 UU SAMPLE QTY : 0.509 G -+/-0.196 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 63.4 +/-11.609 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER . ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.11 OOE+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 152 DETECTOR S/N : 76222 AVERAGE %EFFICIENCY : 24.2896 AVERAGE %EFF ERROR : 0.4714 COUNT DATE : 22-Sep-2016 10:04:02 ELAPSED LIVE TIME(SEC) : 9007.66 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B152.CNF;1086 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W152.CNF;285 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230dpm 4485.29 4547.91 4.6547 dpm 5332.78 5335.19 PEAK NET 1 403.54 -0.20 PEAKNET2 3.00 107.31 RECOVERY YIELD CORR. 99.491 N/A 63.878 1.0082 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5332.78 4.867 1.000 U-3/4 4763.02 4755.53 55.563 30.000 U-235 4391.00 4485.29 47.046 3.000 U-238 4184.73 4186.41 35.690 38.000 >> > .!.!l lJ..238:39744284keV 31 U-235:4310-4581 keV lJ..J.14:4592-4865keV 28 U-232:5000-5398keV 25 22 en 19 I-16 z :J 13 0 S?. 10 .a 7 *:;; n 4 <i:: 2406 2798 3194 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.201 1.201 1.0959 100.000 -4.95E-03 29.584 0.416 0.6453 100.000 1.14E+OO 3.000 0.000 0.0000 99.700 1.16E-01 37.445 0.555 0.7451 100.000 1.44E+OO 5660 6086 6517 6952 7391 1.96-sigma TPU pCi/G 7.19E-02 4.95E-01 1.54E-01 5.76E-01 NOTES: MDA pCi/G 1.69E-01 2.02E-01 1.16E-01 2.16E-01 Le pCi/G 4.76E-02 4.35E-02 O.OOE+OO 5.02E-02 1.96-sigma cnt Unc pCi/G 7.17E-02 4.19E-01 1.51E-01 4.70E-01

Results are a compilation of S0405235056_UU and T0405235056_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235056 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 121 DETECTOR S/N : 75545 AVERAGE %EFFICIENCY : 26.2144 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : +/-10.228 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 2.9733E+OO dpm NUCLIDE LIBRARY PEAK Vi 1--z ::J 0 .2:-*:;; ENERGY ENERGY U-232 5302.10 5335.19 U-3/4 4763.02 4787.37 U-235 4391.00 4547.91 U-238 4184.73 4235.07 12 U.238:3974-4284keV U-235:431()-4581 keV 11 U*314:4592-4865keV U-232:5000.5398keV 10 9 8 7 6 5 4 3 2 1 2424 2819 3217 3620 Energy (keV) PEAK FWHM 57.272 34.363 0.000 9.818 COUNT DATE : 22-Sep-2016 10:03:06 ELAPSED LIVE TIME(SEC) : 8327.71 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA S!Dev pCi/G 108.000 107.306 0.694 0.8331 100.000 4.12E+OO 30.000 29.584 0.416 0.6453 100.000 1.13E+OO 3.000 3.000 0.000 0.0000 99.700 1.15E-01 38.000 37.445 0.555 0.7451 100.000 1.43E+OO 5694 6121 6551 6986 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B121.CNF;1158 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W121.CNF;322 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.15E+OO 2.27E-01 5.61E-02 4.75E-01 2.00E-01 4.31E-02 1.52E-01 1.15E-01 O.OOE+OO 5.50E-01 2.14E-01 4.98E-02 1.96-sigma cnt Unc pCi/G 7.86E-01 4.16E-01 1.50E-01 4.67E-01 "tl Jii (1) Vt Version 3.5.J 0 '""" BATCH NUMBER : 1596408 SAMPLE ID : T0405235057 UU SAMPLE QTY : 0.500 G -+/-0.200 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 73.0 +/-11.062 % SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0489E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 154 DETECTOR S/N : 76224 AVERAGE %EFFICIENCY : 26.1126 AVERAGE %EFF ERROR : 0.5058 COUNT DATE : 22-Sep-2016 10:04:04 ELAPSED LIVE TIME(SEC) : 9038.90 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B154.CNF;1097 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W154.CNF;304 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 44 79.40 4410.26 4.6547 dpm 5198.56 5317.59 PEAK NET 1 411.36 -0.75 PEAKNET2 1.86 122.44 RECOVERY YIELD CORR. 94.013 N/A . 73.570 1.0082 NUCLIDE LIBRARY PEAK Ui I-z => 0 *:;; ENERGY ENERGY U-232 5302.10 5198.56 U-3/4 4763.02 4751.14 U-235 4391.00 4479.40 U-238 4184.73 4197.90 U-238: 3974-4284 keV 37 U-235: 4310-4581 keV U-3/4:4592-4865keV 33 U-232:5000-5398keV 29 25 21 17 13 9 5 2372 2768 3169 3574 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 46.903 27.000 51.017 2.000 13.166 20.000 l >> .:.: NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABLIN ACTIVITY AREA AREA StDev pCi/G -0.753 0.753 0.8679 100.000 -1.84E-02 26.722 0.278 0.5270 100.000 9.15E-01 1.861 0.139 0.3726 99.700 6.39E-02 19.445 0.555 0.7453 100.000 6.66E-01 l l 5654 6081 6513 6948 7387 1.96-sigma TPU pCi/G 5.12E-02 4.09E-01 1.18E-01 3.41E-01 NOTES: MDA pCi/G 1.48E-01 1.66E-01 1.48E-01 1.92E-01 Le pCi/G 3.73E-02 3.17E-02 2.25E-02 4.48E-02 1.96-sigma cnt Unc pCi/G 5.09E-02 3.56E-01 1.17E-01 3.08E-01

Results are a compilation of S0405235057 _UU and T0405235057 _UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235057 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 122 DETECTOR S/N : 75546 AVERAGE %EFFICIENCY : 25.9617 AVERAGE %EFF ERROR : 0.5030 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 73.6 +/-9.624 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 3.4244E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5317.59 U-3/4 4763.02 4762.18 U-235 4391.00 4410.26 U-238 4184.73 4207.64 14 U-238:39T4-4284kaV U*235:431o-4581 keN 13 U-3/4:4592-4865keV 12 U-232:50Q0..5398keV 11 10 9 en 8 I-7 z 6 ::::> 0 5 s 4 3 *:;: ti 2 <l'. 1 2382 2781 3183 3589 Energy (keV) PEAK FWHM 69.310 9.917 9.917 30.165 COUNT DATE : 22-Sep-2016 10:03:08 ELAPSED LIVE TIME(SEC) : 8331.10 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 123.000 122.445 0.555 0.7453 100.000 4.19E+OO 27.000 26.722 0.278 0.5270 100.000 9.08E-01 2.000 1.861 0.139 0.3726 99.700 6.34E-02 20.000 19.445 0.555 0.7453 100.000 6.61E-01 5676 6105 6537 6974 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B122.CNF;1170 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W122.CNF;334 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCiJG pCi/G 1.10E+OO 1.92E-01 4.48E-02 3.94E-01 1.65E-01 3.14E-02 1.17E-01 1.47E-01 2.23E-02 3.31E-01 1.91E-01 4.44E-02 1.96-sigma cnt Unc pCiJG 7.48E-01 3.53E-01 1.16E-01 3.06E-01 'i::l <> \.J\ W A!phaSpecil'OscopySoftwareVersloo3.5.3 O effective date: 02*Mar*2015 0 ....., BATCH NUMBER : 1596408 SAMPLE ID : T0405235058 UU g SAMPLE QTY : 0.512 G -+/-0.195 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 86.1 +/-10.828 % SECONDARY QTY : 0.501 G +/-0.200 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.1613E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 155 DETECTOR S/N : 75553 AVERAGE %EFFICIENCY : 26.3876 AVERAGE %EFF ERROR : 0.5110 COUNT DATE : 22-Sep-2016 10:04:06 ELAPSED LIVE TIME(SEC) : 9041.49 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B155.CNF;1099 . BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W155.CNF;289 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4483.92 4410.61 4.6547 dpm 5198.53 5309.09 PEAKNET1 363.20 -0.90 PEAK NET2 5.17 136.03 RECOVERY YIELD CORR. 82.117 N/A 86.802 1.0082 NUCLIDE LIBRARY PEAK Ui 1--z :J 0 a *s: n <l'. ENERGY ENERGY U-232 5302.10 5198.53 U-3/4 4763.02 4759.81 U-235 4391.00 4483.92 U-238 4184.73 4193.31 U-238: 3974-4284 keV U*235:43104581keV 33 U-3/4:4592-4865keV lJ.232:5000-5398keV 29 25 21 17 13 9 5 2395 2792 3192 3597 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 45.605 27.000 59.370 6.000 6.163 21.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.904 0.904 0.9509 100.000 -2.51E-02 25.617 1.383 1.1761 100.000 7.71E-01 5.170 0.830 0.9110 99.700 1.56E-01 18.510 2.490 1.5779 100.000 5.57E-01 5682 6111 6545 6982 7 424 1.96-sigma TPU pCi/G 5.89E-02 3.55E-01 1.62E-01 3.04E-01 NOTES: MDA pCi/G 1.76E-01 2.15E-01 1.87E-01 2.57E-01 Le pCi/G 4.66E-02 6.21E-02 4.83E-02 8.34E-02 1.96-sigma cnt Unc pCi/G 5.86E-02 3.13E-01 1.58E-01 2.79E-01

Results are a compilation of S0405235058_UU and T0405235058_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000) 0 ...,, V\ 00 0 \0 BATCH NUMBER : 1596408 SAMPLE ID : S0405235058 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 124 DETECTOR S/N : 80053 AVERAGE %EFFICIENCY : 24.5380 AVERAGE %EFF ERROR : 0.4761 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST: HAKB % YIELD : 86.8 +/-9.193 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 4.0404E+OO dpm NUCLIDE LIBRARY PEAK Ci) I-z :J 0 8 *:;; t5 <t'. ENERGY ENERGY U-232 5302.10 5309.09 U-3/4 4763.02 4763.73 U-235 4391.00 4410.61 U-238 4184.73 4202.13 14 lJ.238:3974-4284keV U-235: 4310-4581 keV 13 U*314:4592-4865keV 12 U-232:S000-5398keV 11 10 9 8 7 6 5 4 3 2 1 2377 2775 3177 3583 Energy (keV) PEAK FWHM 36.058 57.803 133.772 8.258 COUNT DATE : 22-Sep-2016 10:03:10 ELAPSED LIVE TIME(SEC) : 8299.73 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 137.000 136.032 0.968 0.9840 100.000 4.10E+OO 27.000 25.617 1.383 1.1761 100.000 7.65E-01 6.000 5.170 0.830 0.9110 99.700 1.55E-01 21.000 18.510 2.490 1.5779 100.000 5.53E-01 5665 6092 6523 6958 7396 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B124.CNF;1158 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W124.CNF;300 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.02E+OO 1.94E-01 5.20E-02 3.41E-01 2.13E-01 6.16E-02 1.59E-01 1.86E-01 4.79E-02 2.95E-01 2.55E-01 8.27E-02 1.96-sigma cnt Unc pCi/G 6.94E-01 3.11E-01 1.57E-01 2.77E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235059 UU SAMPLE QTY : 0.503 G -+/-0.199 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 156 DETECTOR S/N : 75554 AVERAGE %EFFICIENCY : 25.9446 AVERAGE %EFF ERROR : 0.5027 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B156.CNF;1098 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 89.7 +/-10.459 % COUNT DATE : 22-Sep-2016 10:04:10 ELAPSED LIVE TIME(SEC) : 9043.93 EFF FILE : W156.CNF;299 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0469E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U-238:3974-4284keV U-235:4310-4581 keV 33 U-3/4:4592-4865keV U-232: 5000-5398 keV 29 25 if) 21 I-17 z :J 0 13 8. 9 *:;: ts 5 <I: Energy (keV) ID 1570-E 1564-1 PEAK ENERGY 5198.55 4759.84 4486.35 4183.35 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 408.16 -1.36 PEAK NET2 3.86 145.31 RECOVERY YIELD CORR. 11.1230 dpm 4486.35 4456.35 4.6529 dpm 5198.55 5305.56 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA S!Dev 0.000 0.000 -1.357 1.357 1.1647 100.000 70.310 28.000 27.583 0.417 0.6455 100.000 47.695 4.000 3.861 0.139 0.3727 99.700 43.584 22.000 21.583 0.417 0.6455 100.000 5678 6107 6539 6975 :<! ;\ ACTIVITY pCi/G -3.34E-02 7.91E-01 1.11E-01 6.19E-01 7415 1.96-sigma TPU pCi/G 5.36E-02 3.45E-01 1.29E-01 2.99E-01 NOTES: MDA pCi/G 1.75E-01 1.51E-01 1.24E-01 1.51E-01 93.834 N/A 90.390 1.0078 Le pCi/G 5.05E-02 3.25E-02 1.88E-02 3.25E-02 1.96-sigma cnt Unc pCi/G 5.34E-02 3.03E-01 1.27E-01 2.70E-01 *Results are a compilation of S0405235059_UU and T0405235059_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S0405235059 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 126 DETECTOR S/N : 75548 AVERAGE %EFFICIENCY : 25.0653 AVERAGE %EFF ERROR : 0.4861 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 90.4 +/-8.918 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6529E+OO dpm 4.2058E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5305.56 U-3/4 4763.02 4763.56 U-235 4391.00 4456.35 U-238 4184.73 4193.53 17 U-238: 39744284 keV U-235: 4310-4581 keV U-3/4:4592-4665keV 15 U-232:5000-5398keV 13 11 0' 9 z => 7 0 8 5 3 :g <( 2389 2788 3192 Energy (keV) PEAK FWHM 45.042 54.672 119.285 5.799 COUNT DATE : 22-Sep-201610:03:12 ELAPSED LIVE TIME(SEC) : 8334.57 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 146.000 145.305 0.695 0.8334 100.000 4.17E+OO 28.000 27.583 0.417 0.6455 100.000 7.85E-01 4.000 3.861 0.139 0.3727 99.700 1.10E-01 22.000 21.583 0.417 0.6455 100.000 6.14E-01 5693 6123 6558 6996 7438 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B126.CNF;1162 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W126.CNF;338 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.01E+OO 1.70E-01 4.20E-02 3.32E-01 1.50E-01 3.22E-02 1.27E-01 1.23E-01 1.87E-02 2.90E-01 1.50E-01 3.22E-02 1.96-sigma cnt Unc pCi/G 6.82E-01 3.01E-01 1.26E-01 2.68E-01 BATCH NUMBER : 1596408 SAMPLE ID : T0405235060 UU SAMPLE QTY : 0.515 G -+/-0.194 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 157 DETECTOR S/N : 75555 AVERAGE %EFFICIENCY : 26.0007 AVERAGE %EFF ERROR : 0.5038 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B157.CNF;1098 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB CORRECTED% YIELD : 94.0 +/-10.326 % COUNT DATE : 22-Sep-2016 10:04:12 ELAPSED LIVE TIME(SEC) : 9024.81 EFF FILE : W157.CNF;284 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.512 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 8.9054E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 347.23 -0.60 PEAKNET2 0.86 162.16 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5198.56 0.000 U-3/4 4763.02 4766.10 25.572 U-235 4391.00 4481.60 46.071 U-238 4184.73 4193.00 40.420 U-238:3974-4284keV 37 U.235:43104581 keV U-3/4:4592-4865keV U-232:5000..5398keV 33 29 25 Ci) 21 I-z 17 :J 0 13 9 *:;: t5 < 5 2383 2781 3182 3588 3 97 410 Energy (keV) 11.1230 dpm 4481.60 4555.13 4.6529 dpm 5198.56 5297.33 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA S!Dev 0.000 -0.602 0.602 0.7757 100.000 11.000 10.443 0.557 0.7464 100.000 1.000 0.861 0.139 0.3732 99.700 23.000 22.721 0.279 0.5278 100.000 Il 48 7 5248 5672 6101 6533 6969 ;; " ACTIVITY pCi/G -1.71E-02 2.62E-01 2.17E-02 5.70E-01 7408 1.96-sigma TPU pCi/G 5.90E-02 1.79E-01 7.06E-02 2.68E-01 NOTES: MDA pCi/G 1.63E-01 1.41E-01 1.09E-01 1.22E-01 79.823 N/A 94.733 1.0078 Le pCi/G 3.89E-02 3.29E-02 1.65E-02 2.33E-02 1.96-sigma cnt Unc pCi/G 5.87E-02 1.71E-01 7.04E-02 2.41E-01 *Results are a compilation of S0405235060_UU and T0405235060_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.005 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : 80405235060 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 127 DETECTOR S/N : 78770 AVERAGE %EFFICIENCY : 26.6218 AVERAGE %EFF ERROR : 0.5155 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 94.7 +/-8.500 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6529E+OO dpm 4.4078E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5297.33 U-3/4 4763.02 4759.64 U-235 4391.00 4555.13 U-238 4184.73 4183.58 U-238: 3974-4284 keV 15 U-235: 431o-45B1 keV U-314:4592-4865keV U-232:5000-5398keV 13 11 (ii 9 f-z 7 :J 0 s 5 *:;; 3 t5 <( PEAK FWHM 49.748 9.916 4.958 6.611 >> .!Ill COUNT DATE : 22-Sep-2016 10:03:15 ELAPSED LIVE TIME(SEC) : 8356.29 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 163.000 162.164 0.836 0.9141 100.000 4.07E+OO 11.000 10.443 0.557 0.7464 100.000 2.60E-01 1.000 0.861 0.139 0.3732 99.700 2.15E-02 23.000 22.721 0.279 0.5278 100.000 5.66E-01 >> > .:.: 2382 2781 3183 3590 4 00 414 48 3 5255 5681 6111 6545 6982 7424 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B127.CNF;1165 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W127.CNF;322 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.39E-01 1.56E-01 4.03E-02 1.75E-01 1.40E-01 3.26E-02 7.00E-02 1.08E-01 1.64E-02 2.58E-01 1.21E-01 2.31E-02 1.96-sigma en! Une pCi/G 6.30E-01 1.70E-01 6.99E-02 2.39E-01 BATCH NUMBER : 1596408 SAMPLE ID : T1203621739 UU SAMPLE QTY : 0.515 G -+/-0.194 % SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 91.2 +/-11.038 % SECONDARY QTY : 0.513 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 6.4377E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 158 DETECTOR S/N : 80007 AVERAGE %EFFICIENCY : 25.2718 AVERAGE %EFF ERROR : 0.4900 COUNT DATE : 22-Sep-2016 10:04:13 ELAPSED LIVE TIME(SEC) : 9027.47 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B158.CNF;1103 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W158.CNF;286 CAL DATE : 09-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAK NET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4494.41 4450.56 TRACER2 1564-1 U-232 4.6173 dpm 5149.19 5308.18 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5149.19 4.944 2.000 1.097 0.903 0.9501 100.000 U-3/4 4763.02 4728.16 0.000 3.000 2.721 0.279 0.5280 100.000 U-235 4391.00 4494.41 40.926 3.000 2.721 0.279 0.5280 99.700 U-238 4184.73 4114.61 202.689 3.000 2.861 0.139 0.3733 100.000 lJ.2J8*3974-4284keV lJ.235:4310-4581keV 25 U-3/4:4S92-4865keV U-232:5000-5398kaV 22 19 Ui 16 I-13 z ,__ => 0 10 8 7 u 4 <( "l I I ,I, I I II I I I I I I I I I I 23 86 2784 3186 3591 4( 01 48 3 5255 5681 6111 6546 6984 -Energy (keV) ACTIVITY pCi/G 4.39E-02 7.20E-02 7.22E-02 7.57E-02 I 7426 244.05 2.72 57.704 N/A 1.10 154.30 92.218 1.0109 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 1.40E-01 2.54E-01 6.71E-02 1.39E-01 1.06E-01 1.28E-01 2.45E-02 1.04E-01 1.06E-01 1.29E-01 2.46E-02 1.05E-01 1.06E-01 1.14E-01 1.73E-02 1.04E-01 NOTES: *Results are a compilation of S1203621739_UU and T1203621739_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.004 +/-0.000)

BATCH NUMBER : 1596408 SAMPLE ID : S1203621739 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 128 DETECTOR S/N : 75549 AVERAGE %EFFICIENCY : 26.0039 AVERAGE %EFF ERROR : 0.5038 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 92.2 +/-8.684 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6173E+OO dpm 4.2579E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5308.18 U-3/4 4763.02 4709.15 U-235 4391.00 4450.56 U-238 4184.73 4102.48 -U 238* 3974-4284 keV 15 lJ.235:4310-4581keV U-J/4: 4592-4865 keV lJ..232:SOQ0..5398keV 13 ,_ 11 r 'Ci) 9 r-1--z 7 :J r 0 s 5 r-*:;; 3 ts r PEAK FWHM 58.229 123.366 182.582 217.125 <I'. r I I I I I I I I I 11 I 24 00 2797 3198 3603 4 12 Energy (keV) COUNT DATE : 22-Sep-2016 10:03:17 ELAPSED LIVE TIME(SEC) : 8362.11 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 155.000 154.303 0.697 0.8348 100.000 4.04E+OO 3.000 2.721 0.279 0.5280 100.000 7.12E-02 3.000 2.721 0.279 0.5280 99.700 7.14E-02 3.000 2.861 0.139 0.3733 100.000 7.49E-02 111 I 1 I 1 I I I I I 48 2 5263 5688 6117 6550 6987 7429 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B128.CNF;1169 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W128.CNF;324 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.52E-01 1.55E-01 3.84E-02 1.04E-01 1.27E-01 2.43E-02 1.04E-01 1.27E-01 2.43E-02 1.04E-01 1.13E-01 1.72E-02 1.96-sigma cnt Unc pCi/G 6.41E-01 1.03E-01 1.04E-01 1.03E-01 AlphaSpedn:lsoopySoflwareVersionJ.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596408 SAMPLE ID : T1203621740 UU SAMPLE QTY : 0.511 G -+/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 159 DETECTOR SIN : 76225 AVERAGE %EFFICIENCY : 25.5501 AVERAGE %EFF ERROR : 0.4952 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B159.CNF;1072 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 79.2 +/-8.502 % COUNT DATE : 22-Sep-2016 10:04:16 ELAPSED LIVE TIME(SEC) : 9014.70 EFF FILE : W159.CNF;278 CAL DATE : 09-Sep-2016 SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.2119E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 463.82 -1.95 PEAKNET2 3.04 289.20 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5198.48 0.000 U-3/4 4763.02 4757.52 14.636 U-235 4391.00 4484.70 43.827 U-238 4184.73 4182.94 38.419 46 U 2J8* 3974-4284 keV -U-235:431o-4581keV lJ..3/4:4592-4865keV 41 r-u.232:sooo...sJ98keV 36 31 (j) 26 -I-z 21 -::::> 0 16 s *::; 6 <l'. 1 --l.1JI I I I I 23 94 2786 3183 3585 3rn1 402 Energy (keV) 11.1230 dpm 4484. 70 44 73.39 4.6549 dpm 5198.48 5311.68 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA S!Dev 0.000 -1.953 1.953 1.3976 100.000 41.000 40.280 0.720 0.8485 100.000 4.000 3.040 0.960 0.9798 99.700 56.000 55.040 0.960 0.9798 100.000 ".! I I I I I 4817 5237 5661 6090 6523 6960 -ACTIVITY pCi/G -4.19E-02 5.72E-01 4.33E-02 7.81E-01 I 7403 108.627 N/A 79.846 1.0082 1.96-sigma 1.96-sigma TPU MDA Le en! Unc pCi/G pCi/G pCi/G pCi/G 4.83E-02 1.70E-01 5.29E-02 4.82E-02 2.05E-01 8.67E-02 2.21E-02 1.81E-01 6.46E-02 9.38E-02 2.55E-02 6.41E-02 2.49E-01 9.35E-02 2.55E-02 2.10E-01 NOTES: *Results are a compilation of S1203621740_UU and T1203621740_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.007 +/-0.000)

AlphaSpectroscopySoftwareVerslon3.S.3 effectivedate:02*Mar-2015 BATCH NUMBER : 1596408 SAMPLE ID : S1203621740 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.511 G -+/-0.196 % CHAMBER : 014 DETECTOR S/N : 83289 AVERAGE %EFFICIENCY : 32.6875 AVERAGE %EFF ERROR : 0.6302 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 79.8 +/-6.725 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.7168E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5311.68 U-3/4 4763.02 4762.35 U-235 4391.00 4473.39 U-238 4184.73 4180.73 25 U-238:3974-4284keV U-235:4310-4581 keV 23 U-3/4:4592-4865keV U-232:5000-5398keV 21 19 17 15 en 13 I-z 11 :J 0 9 s 7 *::; 5 t5 3 <!'. 2378 Energy (keV) PEAK FWHM 66.910 52.832 230.986 50.989 COUNT DATE : 22-Sep-2016 14:24:56 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 294.000 289.200 4.800 2.1909 100.000 4.10E+OO 41.000 40.280 0.720 0.8485 100.000 5.67E-01 4.000 3.040 0.960 0.9798 99.700 4.29E-02 56.000 55.040 0.960 0.9798 100.000 7.75E-01 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B014.CNF;1814 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W014.CNF;523 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.39E-01 1.56E-01 5.69E-02 1.95E-01 8.60E-02 2.19E-02 6.39E-02 9.30E-02 2.53E-02 2.34E-01 9.27E-02 2.53E-02 1.96-sigma cnt Unc pCi/G 4.79E-01 1.79E-01 6.36E-02 2.09E-01 AlphaSpectrosoopySoftwareVersio113.5.3 eftectlvedate:02-Mar-2015 BATCH NUMBER : 1596408 SAMPLE ID : T1203621741_UU SAMPLE QTY : 0.515 G +/-0.194 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 160 DETECTOR S/N : 79994 AVERAGE %EFFICIENCY : 25.3966 AVERAGE %EFF ERROR : 0.4923 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B160.CNF;1074 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB CORRECTED % YIELD : 91.5 +/-8.404 % SECONDARY QTY : 0.513 G +/-0.195 % COUNT DATE : 22-Sep-201610:04:19 ELAPSED LIVE TIME(SEC) : 9017.69 EFF FILE : W160.CNF;308 CAL DATE : 09-Sep-2016 TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0166E+01 dpm LCS ID NUCLIDE NOMINAL (pCi/G) % RECOVERY 1600-E U-238 5.2299E+OO 102.794 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 386.88 -0.30 PEAKNET2 25.32 338.44 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5198.56 0.000 U-3/4 4763.02 4796.23 4.950 U-235 4391.00 4487.00 83.454 U-238 4184.73 4007.33 4.950 34 U-238*3974-4284keV U-235:43111-4581 keV 31 U-3/4;4592-4865keV U-232:5000-5398keV 28 25 22 'iii 19 f--16 z :J 13 0 8 10 7 *::; u 4 <( I I I I Ill I 11111 I I I 23 82 2780 3182 3588 31 97 Energy (keV) 11.1230 dpm 4487.00 4465.41 4.6173 dpm 5198.56 5301.22 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 0.000 -0.301 0.301 0.5483 100.000 424.000 422.800 1.200 1.0954 100.000 27.000 25.320 1.680 1.2961 99.700 451.000 450.520 0.480 0.6928 100.000 I I I I I I I I 48 8 5249 5674 6103 6535 6972 -ACTIVITY pCi/G -7.59E-03 5.05E+OO 3.03E-01 5.38E+OO I 7412 91.125 N/A 91.534 1.0001 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 5.13E-02 1.25E-01 2.44E-02 5.11E-02 9.80E-01 8.37E-02 2.39E-02 4.82E-01 1.35E-01 9.27E-02 2.84E-02 1.25E-01 1.04E+OO 6.61E-02 1.51E-02 4.97E-01 NOTES: *Results are a compilation of S1203621741 UU and T1203621741_UU. -* The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.006 +/-0.000) 0 ...., "' 00 0 '° BATCH NUMBER : 1596408 SAMPLE ID : S1203621741_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G +/-0.194 % CHAMBER : 015 DETECTOR S/N : 80055 AVERAGE %EFFICIENCY : 33.3682 AVERAGE %EFF ERROR : 0.6430 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 91.5 +/-6.319 % TRACER ID 1564-1 NUCLIDE U-232 NOMINAL 4.6173E+OO dpm RESULTS 4.2264E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5301.22 49.173 U-3/4 4763.02 4758.19 48.295 U-235 4391.00 4465.41 0.000 U-238 4184.73 4182.75 62.695 >> !l!l U*238:39744284keV 37 lJ.235: 4310-4581 keV U-3/4:4592-4865keV U-232:S000-5398keV 33 29 25 en 21 I-z 17 => 0 13 9 u <( 5 COUNT DATE : 22-Sep-2016 14:24:56 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID . 1600-E NUCLIDE U-238 NOMINAL (pCi/G) 5.2299E+OO % RECOVERY 102.786 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 343.000 338.440 4.560 2.1354 100.000 4.04E+OO 424.000 422.800 1.200 1.0954 100.000 5.04E+OO 27.000 25.320 1.680 1.2961 99.700 3.03E-01 451.000 450.520 0.480 0.6928 100.000 5.38E+OO 2386 2781 3182 3587 3 96 410 48 9 5252 5680 6112 6549 6990 7436 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B015.CNF;1833 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W015.CNF;530 CAL DATE : 27-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.80E-01 1.29E-01 4.67E-02 8.12E-01 8.37E-02 2.39E-02 1.31E-01 9.27E-02 2.84E-02 8.56E-01 6.61E-02 1.51E-02 1.96-sigma cnt Unc pCi/G 4.35E-01 4.82E-01 1.25E-01 4.97E-01 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Batch#___._.\ 5 ....... CJ ....... "---(h Product: _______ _ Date: Criteria: Yes Na Comments Sample Solids are less than or eauat to 100 m11 for GAB. ill Samples have been blank corrected (If required). Blank correction reaorted Included flf r"°ulred\. If activity less than lOx MDA/MDC, error Is less than or equal to lSOO/o of sample activity. lf greater than 10* MDA/ MDC, error Is 400/o or less. ./ [f *hn MnA I Mnt' nPPnr I<: ... Instrument source check Is within limits. .,/" Ino;tr"-"'"* him .-h .. .-k lo:: within flmlt... Method RDL/ LLD has been met. ...-tf duplicate activities are: Less than 5* MDA/ MDC, then RPD is 1000/o or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MOA/ MDC, the RPD Is 0%, Or meets the client's reaulred RER acceotance criteria. / -Tracer yield Is 15-1250/o
Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). \,/ Method blank is less than the RDL/ LLD. ./ lrTf *-" r--nln-4' o;;O/n nf lnounr* --*lulh,\ Sample was run within hold time. v Sample was correctlv areserved if reauired. Smears Taken for Radioactive batches. {\fr Method Spike and LCS are within 75-1250/o ..,/"' 'or me"'tc the client's cnntract ,,..,...,n.,.nce criteria\. No blank spaces on data forms. All tine outs initialed and dated. .,/"' Mn nrrnrr -*n Aux data Is correct. Client Saeclal reaulrements aaae has been checked. / Raw Data and I or snectrum are Included and nronerlv statu<:ed. ..,,,..... MS, LCS, and Duplicate RPD/RER values uploaded to UMS and v ""'"'""'" lu1* *-rlf . }J?--ln-*.-h "'" ........ ln*n ..,--Batch Data Exceatlon Reaorts fDER\ comaleted if anallcabie. ./ 17)\:;il-ll-2B:,c, Batch Data Exception Reports (DER) second reviewed. 1.-/ [bbfl;.U Dlsaositlon verified to be completed. Aliauot Correctinn comaleted If renulred, A.lb.. Review sample historical results If available ./ (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. \ Primary Review Performed By:. __ ___ ___ c_J_/2_q_, Secondary Review Performed By:___ 09/30/16 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCcPTION REPORT Mo.Day Yr. Division: Quality Criteria: 29-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER EML HASL-300, Th-01-RC Solid Batch ID: Sample Numbers: 1596407 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, and 1203621737 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 29-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 543 of 5809 DER Report No.: 1562839 Revision No.: 1 Type: Process Client Code: MJWC

/ Thorium (Ac-227 Tracer) Queue Sheet 07-SEP-16 Batch#: 1596407 Analyst: HAKB First Client Due Date:04-0CT-16 Internal Due Date30-SEP-16 Tracer Isotope: Ac"227 Tracer Code: O :281-P, -t.t Oaxpiration Ac-227 Separation Datetrime: 121J11 .. @. LCS LCS Code: -H Expiration Spike Isotope: Th-230, Th-23:.!ipike Code: -Expiration Date: Vol:---==--Prep Date: ':>J } 2...o \ } Y. Initials: cU4-i::t3 Pipet ID: lg I.{ oo a....z::., Balance ID: i 1,, Io :r 6 Witness: /'JW!U,1 Sample ID Client Description 405235041-1 4.4D.R.1.4 405235042-1 4.4D.R.2.3 405235043-1 4.4D.R.2.4 405235044-1 4.41>.R.4.2 4052351145-1 4.4D.R.5.2 4052351146-1 4.SA.R.1.3 4052351147-1 4.SA.R.1.4 405235048*1 4.5B.R.l.2 405235049-1 4.5B.R.l.3 405235050-1 4.5B.R.1.4 405235051-1 4.5B.R.2.3 405235052-1 4.5B.R.2.4 405"..35053-1 4.SC.R.5.2 405235054-1 4.SC.R.1.3 405235055-1 4.SC.R.lA 405235056-1 4.SC.R.2.2 405235057-1 4.SC.R.2.3 405235058-1 4.SC.R.2A 405235059-1 5.lA.R.1.2 405235060-1 S.lA.R.1.3 -1203621736-1 11-m for batch 1596407 1203621737-1 4.4D.R.1.4(405235041DUP) LCS for batch 1596407 Choose SOP Used: GL-RAD-A-038/ GL-R-'\D-A-032 Type SAMPLE SAMPLE SAMPLE SAMPLE SA.1\.1PLE SAMPLE SAfl.1PLE SAMPLE SM1PLE SAMPLE SAA1PLE SA.l\1PLE SAA1PLE SAMPLE SAJl.1PLE SAMPLE SAJ\.1PLE SA.'\1PLE SAJl.IPLE SM1PLE l\IB DUP LCS GEL Laboratories LLC, Radiochemistry Division Hazard Min Code CRDL 1 pCi/g l pCi/g lpCi/g 1 pCi!g 1 pCi/g 1 pCi/g lpCi/g 1 pCi/g 1 pCl/g lpCi/g 1 pCi/g 1 pCi!g 1 pCi/g l pCi/g 1 pCi!g lpCUg 1 pCI/g lpCUg 1 pCi/g l pCi/g 1 pCI/g 1 pCi/g lpCUg Collection Label Matrix Client Date Pos. # SOIL MJWCOOl 30-NOV-15 1 SOIL .MJWCOOl .JO-NOV-15 2 SOIL MJWCOOl 30-NOV-15 3 SOIL MJWCOOI 30-NOV-15 4 SOIL J\.1.JWCOOl 30-NOV-15 5 SOIL 11-JJWCOOl 07-DEC-15 6 SOIL MJWCOOl 07-DEC-15 7 SOIL MJWCOOl 07-DEC-15 8 SOIL MJWCOOl 07-DEC-15 9 SOIL 1\-JJWCOOl 07-DEC-15 10 SOIL MJWCOOl 07-DEC*lS 11 SOIL MJWCOOl 07-DEC*lS 12 SOIL Jl.fJWCOOl 01-DEC-15 13 SOIL MJWCOOl 02-DEC-15 14 SOIL Jl.fJWCOOl 02-DEC-15 15 SOIL M.JWCOOl 02-DEC*l5 16 SOIL l\IJWCOOl 02-DEC-15 17 SOIL MJWCOOl 02-DEC-lS 18 SOIL 11-JJWCOOl 16-DEC-15 19 SOIL MJWCOOl 16-DEC-lS 20 SOIL QC ACCOUNT 21 SOIL QC ACCOUNT 30-NOV-15 22 SOIL QC ACCOUNT 23 Th Det# Page 1 oil Alph<1SpectrcscopySoftwareVers1on3.5.3 effectlvedate:02-Mar*2015 BATCH NUMBER : 1596407 SAMPLE ID : S0405235041 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.128 G -+/-0.781 % CHAMBER : 188 DETECTOR S/N : 68621 AVERAGE %EFFICIENCY : 26.7276 AVERAGE %EFF ERROR : 0.5175 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 99.9 +/-7.512 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2593E+OO dpm 3.2557E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5838.40 5849.25 TH-228 5363.00 5383.55 TH-229 4900.00 4970.22 TH-230 4671.39 4669.57 TH-232 3972.00 4007.90 8 TH-232:3796-408SkeV TH*23ll: 4495-4745 keV TH-229: 4n5-5142 keV 7 TH-228: 5211*5493 keV AC.227: 5510.0128 keV 6 5 (ii 4 I-z :::> 3 0 (2. 2 u <1'. 2429 2820 3215 3615 Energy (keV) PEAK FWHM 330.929 29.164 272.197 4.861 7.291 > COUNT DATE : 27-Sep-2016 17:12:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 211.000 208.840 2.160 1.4697 100.000 1.45E+01 17.000 14.384 0.480 0.6928 99.940 1.07E+OO 7.000 6.760 0.240 0.4899 99.469 3.73E-01 10.000 8.080 1.920 1.3856 99.700 4.45E-01 12.000 11.760 0.240 0.4899 100.000 6.46E-01 > >> .:.: iii Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B188.CNF;854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W188.CNF;233 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.98E+OO 6.48E-01 3.14E-01 3.73E-01 4.02E-01 NOTES: MDA pCi/G 5.84E-01 6.26E-01 2.65E-01 4.45E-01 2.63E-01 Le pCi/G 1.88E-01 2.02E-01 4.96E-02 1.40E-01 4.93E-02 1.96-sigma cnt Unc pCi/G 1.99E+OO 6.20E-01 3.08E-01 3.66E-01 3.90E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 8.3874E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (2.136 +/-0.014)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235042 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.125 G -+/-0.800 % CHAMBER : 040 DETECTOR S/N : 78773 AVERAGE %EFFICIENCY : 32.4791 AVERAGE %EFF ERROR : 0.6262 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 94.6 +/-7.308 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER . ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 2.9655E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5883.53 TH-228 5363.00 5395.86 TH-229 4900.00 4991.07 TH-230 4671.39 4653.33 TH-232 3972.00 4005.98 15 TH-232:3796-40a5keV TH-230: 4495-4745 keV TH-229: 4nS-5142 keV 13 TH-228: 5211-5493 keV AC-227:5510-6128keV 11 & 9 I-7 z :J 0 5 3 2382 2778 3178 Energy (keV) PEAK FWHM 267.791 83.586 285.176 79.898 49.168 COUNT DATE : 22-Sep-2016 09:57:38 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 241.000 231.160 9.840 3.1369 100.000 1.18E+01 28.000 25.052 2.400 1.5492 99.940 1.65E+OO 5.000 3.800 1.200 1.0954 99.469 1.87E-01 17.000 16.520 0.480 0.6928 99.700 8.09E-01 13.000 12.760 0.240 0.4899 100.000 6.23E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B040.CNF;1827 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W040.CNF;485 CAL DATE : 29-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.35E+OO 7.38E-01 2.92E-01 7.44E-01 6.03E-01 2.03E-01 2.44E-01 3.44E-01 9.86E-02 4.27E-01 2.71E-01 6.22E-02 3.72E-01 2.34E-01 4.38E-02 NOTES: 1.96-sigma cnt Unc pCi/G 1.56E+OO 7.01E-01 2.43E-01 4.09E-01 3.60E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8692E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.548 +/-0.004)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235043 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.118G -+/-0.847% CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 91.1 +/-7.998 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2593E+OO dpm 2.9699E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5838.40 5856.79 TH-228 5363.00 5404.84 TH-229 4900.00 4918.49 TH-230 4671.39 4668.42 TH-232 3972.00 3974.42 7 TH-232: 37964085 keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 6 TH-228:5211-5493keV AC-227: 't<sV 5 4 z 3 :::> 0 c 2 *:;; ti <l: 2416 2810 3209 3612 Energy (keV) PEAK FWHM 420.922 74.822 171.722 7.359 44.157 COUNT DATE : 27-Sep-2016 17:12:39 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 183.000 181.080 1.920 1.3856 100.000 1.58E+01 21.000 18.428 0.720 0.8485 99.940 1.71E+OO 4.000 3.520 0.480 0.6928 99.469 2.43E-01 10.000 9.040 0.960 0.9798 99.700 6.23E-01 11.000 10.760 0.240 0.4899 100.000 7.39E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B189.CNF;855 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.45E+OO 9.11E-01 3.10E-01 4.65E-01 4.84E-01 NOTES: MDA pCi/G 7.04E-01 7.85E-01 3.83E-01 4.54E-01 3.29E-01 Le pCi/G 2.21E-01 2.53E-01 8.77E-02 1.24E-01 6.17E-02 1.96-sigma en! Une pCl/G 2.32E+OO 8.58E-01 3.08E-01 4.54E-01 4.69E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 8.3874E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.852 +/-0.012)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235044 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.123 G -+/-0.813 % CHAMBER : 042 DETECTOR S/N : 78793 AVERAGE %EFFICIENCY : 33.3976 AVERAGE %EFF ERROR : 0.6435 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 103 +/-6.974 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 3.2313E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5901.30 TH-228 5363.00 5406.88 TH-229 4900.00 4952.43 TH-230 4671.39 4663.80 TH-232 3972.00 4005.91 15 TH-232: 37964085 keV TH-+230: 4495-4745 keV TH-229: 4775-5142 keV 13 TH-228: 5211-5493 keV AC-227: 551o-6128 keV 11 Ui 9 1--7 z => 0 5 8 3 *s; :g <t: 2383 Energy (keV) PEAK FWHM 276.100 47.060 4.911 9.003 66.294 ::; 3 COUNT DATE : 22-Sep-2016 09:57:38 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 271.000 259.000 12.000 3.4641 100.000 1.20E+01 32.000 30.186 1.200 1.0954 99.940 1.80E+OO 6.000 4.800 1.200 1.0954 99.469 2.14E-01 22.000 20.800 1.200 1.0954 99.700 9.24E-01 18.000 17.760 0.240 0.4899 100.000 7.87E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B042.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W042.CNF;490 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.27E+OO 7.23E-01 2.39E-01 4.41E-01 3.96E-01 NOTES: MDA pCi/G 7.24E-01 4.63E-01 3.12E-01 3.12E-01 2.12E-01 Le pCi/G 2.93E-01 1.42E-01 8.94E-02 8.92E-02 3.98E-02 1.96-sigma cnt Unc pCi/G 1.50E+OO 6.74E-01 2.37E-01 4.21E-01 3.BOE-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8692E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.614 +/-0.004)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235045 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 199 DETECTOR S/N : 78896 AVERAGE %EFFICIENCY : 26.2038 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 97.1 +/-7.799 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 3.0422E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5911.65 TH-228 5363.00 5390.81 TH-229 4900.00 5066.37 TH-230 4671.39 4682.92 TH-232 3972.00 3999.24 9 TH-232:37964085keV TH-230: 4495-4745 keV TH-229:4n5-5142keV 8 TH-228:5211-S493keV AC-227: 551o-6128 keV 7 6 Ui 5 1--z 4 :::> 0 3 8 2 ti <( 2377 2776 3178 3585 Energy (keV) PEAK FWHM 324.158 5.789 29.770 19.846 4.962 COUNT DATE : 22-Sep-2016 09:57:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 193.000 191.320 1.680 1.2961 100.000 1.44E+01 20.000 19.307 0.240 0.4899 99.940 1.88E+OO 2.000 0.560 1.440 1.2000 99.469 4.07E-02 10.000 10.000 0.000 0.0000 99.700 7.26E-01 11.000 10.760 0.240 0.4899 100.000 7.78E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B199.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W199.CNF;222 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.08E+OO 9.27E-01 2.63E-01 4.87E-01 5.09E-01 NOTES: MDA pCi/G 5.84E-01 5.69E-01 5.38E-01 2.18E-01 3.47E-01 Le pCi/G 1.79E-01 1.39E-01 1.60E-01 O.OOE+OO 6.49E-02 1.96-sigma cnt Unc pCi/G 2.06E+OO 8.76E-01 2.63E-01 4.73E-01 4.93E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8692E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.453 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235046 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.119 G -+/-0.840 % CHAMBER : 200 DETECTOR S/N : 78900 AVERAGE %EFFICIENCY : 27.0654 AVERAGE %EFF ERROR : 0.5238 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 96.1 +/-7.776 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 3.0125E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5879.57 TH-228 5363.00 5408.18 TH-229 4900.00 5048.33 TH-230 4671.39 4672.01 TH-232 3972.00 4012.46 9 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4n5-5142 kev 8 TH-22B:5211*5493keV AC-227;5510-6128keV 7 6 en 5 I-z 4 ::l 0 3 8 .2:-2 *:;; 2394 2791 3191 3596 Energy (keV) PEAK FWHM 343.877 86.277 0.000 4.930 4.930 COUNT DATE : 22-Sep-2016 09:57:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 200.000 195.680 4.320 2.0785 100.000 1.24E+01 15.000 13.576 0.960 0.9798 99.940 1.10E+OO 3.000 2.280 0.720 0.8485 99.469 1.39E-01 16.000 15.040 0.960 0.9798 99.700 9.14E-01 8.000 8.000 0.000 0.0000 100.000 4.85E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B200.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W200.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.63E+OO 6.65E-01 2.47E-01 5.16E-01 3.66E-01 NOTES: MDA pCi/G 6.70E-01 5.85E-01 3.72E-01 4.01E-01 1.82E-01 Le pCi/G 2.40E-01 1.71E-01 9.47E-02 1.09E-01 O.OOE+OO 1.96-sigma en! Une pCi/G 1.76E+OO 6.40E-01 2.46E-01 4.96E-01 3.58E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8692E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.464 +/-0.003) 0 ....., Vi 00 0 \0 AlphaSpecttoscopySaftwareVersian3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596407 SAMPLE ID : S0405235047 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.125 G -+/-0.800 % CHAMBER : 201 DETECTOR S/N : 78902 AVERAGE %EFFICIENCY : 26.2326 AVERAGE %EFF ERROR : 0.5081 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 89.4 +/-8.111 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 2.8012E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5890.97 TH-228 5363.00 5388.73 TH-229 4900.00 4924.47 TH-230 4671.39 4676.91 TH-232 3972.00 4007.04 8 TH-232: 3796-4085 keV TH-230; 4495-4745 kaV TH-229; 4nS-5142 keV 7 TH-228: 5211*5493 keV AC-227:5510-6128keV 6 5 (ii 4 I-z :::> 3 0 s 2 *;;;; ti <i: 2375 2773 3175 3582 Energy (keV) PEAK FWHM 341.355 61.929 94.133 24.772 7.432 COUNT DATE : 22-Sep-2016 09:57:40 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 179.000 176.360 2.640 1.6248 100.000 1.18E+01 15.000 13.622 0.960 0.9798 99.940 1.16E+OO 3.000 1.320 1.680 1.2961 99.469 8.50E-02 13.000 11.800 1.200 1.0954 99.700 7.58E-01 11.000 11.000 0.000 0.0000 100.000 7.04E-01 g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B201.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W201.CNF;224 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.61E+OO 7.04E-01 2.67E-01 4.93E-01 4.51E-01 NOTES: MDA pCi/G 5.97E-01 6.13E-01 4.99E-01 4.50E-01 , 1.92E-01 Le pCi/G 1.99E-01 1.78E-01 1.53E-01 1.29E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.76E+OO 6.76E-01 2.67E-01 4.77E-01 4.36E-01
Ac-227 results are decay corrected to separation date/time. *
Ac-227 Tracer nominal includes 1.8693E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.418 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235048 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 202 DETECTOR S/N : 78903 AVERAGE %EFFICIENCY : 27.2753 AVERAGE %EFF ERROR : 0.5278 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 83.9 +/-8.183 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 2.6287E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5894.59 TH-228 5363.00 5372.55 TH-229 4900.00 5010.64 TH-230 4671.39 4658.47 TH-232 3972.00 3992.64 7 TH-232:3796-40a5keV TH-230: 4495-4745 keV TH-229: 4nS-5142 keV 6 TH-228:5211*5493keV AC-227:5510-6128keV 5 en 4 I-z 3 :J 0 s 2 *;;; ti <!'. 2378 2777 3180 Energy (keV) PEAK FWHM 340.010 181.041 193.441 48.360 85.561 COUNT DATE : 22-Sep-2016 09:57:43 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA S!Dev pCi/G 174.000 172.080 1.920 1.3856 100.000 1.40E+01 18.000 16.872 0.720 0.8485 99.940 1.76E+OO 7.000 5.080 1.920 1.3856 99.469 3.99E-01 12.000 10.800 1.200 1.0954 99.700 8.46E-01 17.000 16.520 0.480 0.6928 100.000 1.29E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B202.CNF;797 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W202.CNF;226 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.14E+OO 9.45E-01 4.54E-01 5.78E-01 6.87E-01 NOTES: MDA pCi/G 6.57E-01 7.04E-01 6.34E-01 5.50E-01 4.33E-01 Le pCi/G 2.07E-01 1.96E-01 1.99E-01 1.57E-01 9.91E-02 1.96-sigma cnt Unc pCi/G 2.11E+OO 8.96E-01 4.49E-01 5.61E-01 6.53E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8693E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.408 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235049 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.123 G -+/-0.813 % CHAMBER : 162 DETECTOR S/N : 70323 AVERAGE %EFFICIENCY : 26.6669 AVERAGE %EFF ERROR : 0.5165 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 71.9 +/-8.694 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2531E+OO dpm 2.3406E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5843.45 5857.66 TH-228 5363.00 5428.05 TH-229 4900.00 4912.17 TH-230 4671.39 4678.27 TH-232 3972.00 4016.32 8 TH-232:3796-4065keV TH-230; 4495-4745 keV TH-229:4nS-5142keV 7 TH-228:5211-5493keV AC-227:5510-6128keV 6 5 4 z ::::> 3 0 2 u <l: 2383 2782 3184 3590 Energy (keV) PEAK FWHM 351.396 24.804 4.961 69.452 24.804 399 441 COUNT DATE : 26-Sep-2016 12:01:33 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 151.000 149.800 1.200 1.0954 100.000 1.44E+01 16.000 13.481 1.200 1.0954 99.940 1.44E+OO 1.000 0.520 0.480 0.6928 99.469 4.16E-02 13.000 13.000 0.000 0.0000 99.700 1.04E+OO 14.000 14.000 0.000 0.0000 100.000 1.11E+OO > i;i :rn I 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B162.CNF;862 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W162.CNF;260 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.44E+OO 9.13E-01 2.31E-01 6.14E-01 6.36E-01 NOTES: MDA pCi/G 6.76E-01 9.07E-01 4.43E-01 2.39E-01 2.39E-01 Le pCi/G 1.93E-01 2.94E-01 1.01E-01 O.OOE+OO O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.33E+OO 8.70E-01 2.31E-01 5.86E-01 6.05E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.2086E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.319 +/-0.009)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235050 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 163 DETECTOR S/N : 80056 AVERAGE %EFFICIENCY : 25.6920 AVERAGE %EFF ERROR : 0.4979 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 90.8 +/-8.000 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2531E+OO dpm 2.9536E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5843.45 5856.68 TH-228 5363.00 5422.98 TH-229 4900.00 4941.81 TH-230 4671.39 4627.91 TH-232 3972.00 4010.09 9 TH-232:3796-4085keV TH-230; 44954745 keV TH-229: 4n5-5142 keV 8 TH-228:5211*5493keV AC-227:5510-6128keV 7 6 en 5 I-z 4 => 0 3 8 2 *:;; ti 1 <i: 2375 2774 3176 Energy (keV) PEAK FWHM 320.356 32.221 0.000 18.589 7.436 ::; F > COUNT DATE : 26-Sep-2016 12:01 :36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 185.000 182.120 2.880 1.6971 100.000 1.76E+01 18.000 14.956 1.440 1.2000 99.940 1.60E+OO 6.000 5.520 0.480 0.6928 99.469 4.42E-01 11.000 9.560 1.440 1.2000 99.700 7.64E-01 8.000 7.760 0.240 0.4899 100.000 6.18E-01 g g F ;!; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B163.CNF;908 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W163.CNF;238 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.86E+OO 8.90E-01 3.00E-01 9.66E-01 9.67E-01 3.23E-01 4.27E-01 4.44E-01 1.02E-01 5.65E-01 5.91E-01 1.76E-01 4.82E-01 3.82E-01 7.15E-02 NOTES: 1.96-sigma cnt Unc pCi/G 2.59E+OO 9.22E-01 4.20E-01 5.52E-01 4.71E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.2087E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.604 +/-0.010)

"i:l l/\ l/\ l/\ 0 ..... l/\ 00 0 \0 BATCH NUMBER : 1596407 SAMPLE ID : S0405235051 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT .SAMPLE QTY : 0.120 G -+/-0.833 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 91.7 +/-7.853 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2531E+OO dpm 2.9834E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5843.45 5897.33 TH-228 5363.00 5435.79 TH-229 4900.00 4902.26 TH-230 4671.39 4678.06 TH-232 3972.00 4040.34 7 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4nS-5142 keV 6 TH-228:5211-5493keV AC-227:5510-6128keV 5 (ii 4 I-z 3 :J 0 s 2 u <{ 2402 2798 3198 3603 Energy (keV) PEAK FWHM 347.714 48.060 157.734 32.040 70.241 COUNT DATE : 26-Sep-201612:01:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 189.000 187.800 1.200 1.0954 100.000 1.48E+01 21.000 19.106 0.240 0.4899 99.940 1.67E+OO 6.000 5.040 0.960 0.9798 99.469 3.29E-01 21.000 20.280 0.720 0.8485 99.700 1.32E+OO 18.000 17.760 0.240 0.4899 100.000 1.15E+OO 7413 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B169.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DA TE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.18E+OO 8.54E-01 3.50E-01 6.39E-01 5.87E-01 NOTES: MDA pCi/G 5.53E-01 6.62E-01 4.31E-01 3.98E-01 3.12E-01 Le pCi/G 1.58E-01 2.00E-01 1.17E-01 1.01E-01 5.84E-02 1.96-sigma cnt Unc pCi/G 2.13E+OO 8.03E-01 3.46E-01 6.03E-01 5.57E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.2087E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.654 +/-0.011)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235052 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.120 G -+/-0.833 % CHAMBER : 206 DETECTOR S/N : 78909 AVERAGE %EFFICIENCY : 25.8407 AVERAGE %EFF ERROR : 0.5007 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 64.3 +/-9.440 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 2.0162E+OO dpm NUCLIDE LIBRARY PEAK en f-z => 0 *:.; t5 <l'. ENERGY ENERGY AC-227 5870.91 5861.87 TH-228 5363.00 5406.36 TH-229 4900.00 4958.10 TH-230 4671.39 4660.20 TH-232 3972.00 3999.66 6 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV TH-228:5211-5493keV 5 AC-227: 5511Hi126 keV 4 3 2 2381 2779 3182 3588 Energy (keV) PEAK FWHM 322.991 19.800 0.000 29.700 18.769 COUNT DATE : 22-Sep-2016 09:57:53 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 126.000 125.040 0.960 0.9798 100.000 1.23E+01 6.000 4.744 0.960 0.9798 99.940 5.96E-01 0.000 -0.960 0.960 0.9798 99.469 -9.08E-02 12.000 12.000 0.000 0.0000 99.700 1.13E+OO 14.000 13.520 0.480 0.6928 100.000 1.27E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B206.CNF;798 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W206.CNF;226 CAL DATE : 15-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.18E+OO 6.46E-01 1.76E-01 6.75E-01 8.81E-01 2.52E-01 2.11E-01 6.23E-01 1.70E-01 7.02E-01 2.83E-01 O.OOE+OO 7.58E-01 5.21E-01 1.19E-01 NOTES: 1.96-sigma cnt Unc pCi/G 2.17E+OO 6.65E-01 2.10E-01 6.68E-01 7.18E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8695E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.296 +/-0.002)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235053 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 207 DETECTOR S/N : 78910 AVERAGE %EFFICIENCY : 26.0138 AVERAGE %EFF ERROR : 0.5040 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 98.0 +/-7.780 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 3.0721E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5895.52 TH-228 5363.00 5401.24 TH-229 4900.00 4928.26 TH-230 4671.39 4677.22 TH-232 3972.00 4008.97 8 TH-232: 3796-4085 keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 7 TH-228: 5211-5493 keV AC.227:S510-6128keV 6 5 0' z 4 => 3 0 2 *:;;: t5 <t: 2375 2773 3175 Energy (keV) PEAK FWHM 326.706 112.700 4.954 5.367 33.645 1i COUNT DATE : 22-Sep-2016 09:57:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 193.000 191.800 1.200 1.0954 100.000 1.36E+01 25.000 24.065 0.480 0.6928 99.940 2.20E+OO 1.000 0.520 0.480 0.6928 99.469 3.56E-02 23.000 22.760 0.240 0.4899 99.700 1.56E+OO 21.000 20.760 0.240 0.4899 100.000 1.41E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B207.CNF;809 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W207.CNF;228 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.90E+OO 9.84E-01 1.98E-01 7.02E-01 6.67E-01 NOTES: MDA pCi/G 4.98E-01 5.83E-01 3.79E-01 3.28E-01 3.27E-01 Le pCi/G 1.42E-01 1.54E-01 8.70E-02 6.13E-02 6.12E-02 1.96-sigma cnt Unc pCi/G 1.94E+OO 9.18E-01 1.98E-01 6.58E-01 6.28E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8696E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.455 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235054 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 208 DETECTOR S/N : 78911 AVERAGE %EFFICIENCY : 26.1198 AVERAGE %EFF ERROR : 0.5060 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 93.3 +/-7.949 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1337E+OO dpm 2.9243E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5870.91 5895.15 TH-228 5363.00 5407.57 TH-229 4900.00 4937.89 TH-230 4671.39 4662.63 TH-232 3972.00 4011.46 9 TH-232:3796-4085keV TH-230; 4495-4745 keV TH-229: 4775-5142 keV 8 TH-228:5211-5493keV AC-227:5510.0128keV 7 6 en 5 I-z 4 ::J 0 3 8 c 2 *:;: u <( 2383 2780 3181 Energy (keV) PEAK FWHM 308.970 5.763 237.099 6.586 7.409 COUNT DATE : 22-Sep-2016 09:57:57 ELAPSED LIVE TIME(SEC) : 14400.00 GROSS AREA 185.000 13.000 5.000 16.000 12.000 NUCLIDE ACTIVITY SUMMARY NET AREA 183.320 11.845 3.800 15.760 11.760 > > *

BKG AREA 1.680 0.720 1.200 0.240 0.240 BKG %ABUN ACTIVITY S!Dev pCi/G 1.2961 100.000 1.40E+01 0.8485 99.940 1.17E+OO 1.0954 99.469 2.80E-01 0.4899 99.700 1.16E+OO 0.4899 100.000 8.62E-01 6970 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: *GL-RAD-A-038 LIB FILE : AC BKG FILE : B208.CNF;805 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W208.CNF;253 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.05E+OO 7.53E-01 3.67E-01 6.25E-01 5.39E-01 NOTES: MDA pCi/G 5.92E-01 6.68E-01 5.17E-01 3.53E-01 3.52E-01 Le pCi/G 1.81E-01 1.86E-01 1.48E-01 6.60E-02 6.58E-02 1.96-sigma cnt Unc pCi/G 2.04E+OO 7.28E-01 3.64E-01 5.96E-01 5.21E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8696E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.435 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235055 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 026 DETECTOR S/N : 80017 AVERAGE %EFFICIENCY : 32.6942 AVERAGE %EFF ERROR : 0.6303 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 98.8 +/-7.217 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1416E+OO dpm 3.1050E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.42 5900.99 TH-228 5363.00 5415.49 TH-229 4900.00 4908.09 TH-230 4671.39 4671.32 TH-232 3972.00 4017.29 10 TH-232:3796-4085keV TH-230: 4495-4745 keV 9 TH-229: 4775-5142 k&V TH--228: 5211-5493 keV AC-227;5510-6128keV 8 7 6 Ui 5 I-z ::> 4 0 s. 3 a 2 *:;; 2395 2793 3194 Energy (keV) PEAK FWHM 340.302 24.685 177.733 22.217 9.874 '£ ! COUNT DATE : 22-Sep-2016 13:44:15 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 259.000 243.640 15.360 3.9192 100.000 1.41E+01 21.000 19.387 0.960 0.9798 99.940 1.44E+OO 6.000 4.800 1.200 1.0954 99.469 2.67E-01 14.000 12.800 1.200 1.0954 99.700 7.10E-01 15.000 14.520 0.480 0.6928 100.000 8.03E-01 &i Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B026.CNF;1838 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W026.CNF;495 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.78E+OO 7.21E-01 2.98E-01 4.39E-01 4.52E-01 NOTES: MDA pCi/G 1.01E+OO 5.54E-01 3.90E-01 3.89E-01 3.06E-01 Le pCi/G 4.16E-01 1.66E-01 1.12E-01 1.11E-01 7.02E-02 1.96-sigma cnt Unc pCi/G 1.85E+OO 6.87E-01 2.95E-01 4.26E-01 4.36E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1197E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.653 +/-0.004)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235056 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY.: 0.113 G -+/-0.885 % CHAMBER : 028 DETECTOR S/N : 78792 AVERAGE %EFFICIENCY : 29.2888 AVERAGE %EFF ERROR : 0.5659 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 97.7 +/-7.760 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1416E+OO dpm 3.0683E+OO dpm NUCLIDE LIBRARY PEAK z => 0 s *:;; :g <l'. ENERGY ENERGY AC-227 5869.42 5902.85 TH-228 5363.00 5408.75 TH-229 4900.00 4997.75 TH-230 4671.39 4668.50 TH-232 3972.00 4034.79 10 TH-232: 37964085 keV TH-230: 4495-4745 keV 9 TH-229: 4nS.5142 keV TH-228:5211-5493keV AC-227:5510-0128keV 8 7 6 5 4 3 2 2364 2765 3170 3580 Energy (keV) PEAK FWHM 329.931 7.479 0.000 34.902 64.818 . COUNT DATE : 22-Sep-2016 13:44:15 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 238.000 215.680 22.320 4.7244 100.000 1.31E+01 17.000 14.502 1.920 1.3856 99.940 1.13E+OO 5.000 2.120 2.880 1.6971 99.469 1.24E-01 20.000 18.800 1.200 1.0954 99.700 1.09E+OO 16.000 15.280 0.720 0.8485 100.000 8.87E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B028.CNF;1842 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W028.CNF;507 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.79E+OO 6.83E-01 2.98E-01 5.55E-01 4.93E-01 NOTES: MDA pCi/G 1.24E+OO 6.75E-01 5.38E-01 4.08E-01 3.55E-01 Le pCi/G 5.27E-01 2.20E-01 1.81E-01 1.17E-01 9.03E-02 1.96-sigma cnt Unc pCi/G 1.86E+OO 6.57E-01 2.97E-01 5.27E-01 4.72E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1197E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.578 +/-0.004)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235057 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.110 G -+/-0.909 % CHAMBER : 029 DETECTOR S/N : 33454 AVERAGE %EFFICIENCY : 30.7100 AVERAGE %EFF ERROR : 0.5928 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 109 +/-7.163 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1416E+OO dpm 3.4093E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.42 5878.40 TH-228 5363.00 5402.17 TH-229 4900.00 4881.53 TH-230 4671.39 4666.84 TH-232 3972.00 4021.06 10 TH*232:3796-4085keV TH-230: 44954745 keV 9 TH-229: 4775-5142 keV TH-228: 5211-5493 keV AC-227:5510.0128keV 8 7 0' 6 5 z => 4 0 3 c 2 *;;; ti <( 2401 Energy (keV) PEAK FWHM 343.443 128.206 192.309 38.626 43.146 '1 COUNT DATE : 22-Sep-2016 13:44:15 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 270.000 251.280 18.720 4.3267 100.000 1.35E+01 20.000 18.846 0.480 0.6928 99.940 1.29E+OO 2.000 -0.400 2.400 1.5492 99.469 -2.06E-02 25.000 22.840 2.160 1.4697 99.700 1.17E+OO 25.000 24.280 0.720 0.8485 100.000 1.24E+OO g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B029.CNF;1830 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W029.CNF;544 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.64E+OO 6.SOE-01 1.92E-01 5.47E-01 5.45E-01 NOTES: MDA pCi/G 1.01E+OO 4.61E-01 4.47E-01 4.31E-01 3.13E-01 Le pCi/G 4.25E-01 1.27E-01 1.46E-01 1.38E-01 7.96E-02 1.96-sigma cnt Unc pCi/G 1.75E+OO 6.20E-01 1.92E-01 5.19E-01 5.14E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1197E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.674 +/-0.004)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235058 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.128 G -+/-0.781 % CHAMBER : 176 DETECTOR S/N : 74434 AVERAGE %EFFICIENCY : 25.6995 AVERAGE %EFF ERROR : 0.4981 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 99.8 +/-7.642 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2531E+OO dpm 3.2478E+OO dpm NUCLIDE LIBRARY PEAK 00 1--z :::i 0 s _;:. *:;: n <( ENERGY ENERGY AC-227 5843.45 5872.04 TH-228 5363.00 5386.79 TH-229 4900.00 4834.42 TH-230 4671.39 4676.80 TH-232 3972.00 4031.57 8 TH-232:3796-40B5keV TH-230: 44954745 keV TH-229: 4n5-S142 keV 7 TH-228:5211*5493keV AC.227:5510-612BkeV 6 5 4 3 2 2379 2776 3177 3582 Energy (keV) PEAK FWHM 347.078 83.891 64.152 24.674 45.646 COUNT DATE : 26-Sep-201612:01:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 202.000 200.320 1.680 1.2961 100.000 1.39E+01 16.000 13.996 0.240 0.4899 99.940 1.08E+OO 3.000 2.280 0.720 0.8485 99.469 1.31E-01 17.000 15.320 1.680 1.2961 99.700 8.78E-01 13.000 12.520 0.480 0.6928 100.000 7.16E-01 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B176.CNF;865 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.90E+OO 6.52E-01 2.33E-01 5.02E-01 4.36E-01 NOTES: MDA pCi/G 5.37E-01 5.95E-01 3.51E-01 4.44E-01 3.17E-01 Le pCi/G 1.64E-01 1.82E-01 8.93E-02 1.36E-01 7.25E-02 1.96-sigma cnt Unc pCi/G 1.94E+OO 6.24E-01 2.32E-01 4.83E-01 4.22E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.2087E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.764 +/-0.011)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235059 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.112 G -+/-0.893 % CHAMBER : 032 DETECTOR S/N : 67041 AVERAGE %EFFICIENCY : 27.7435 AVERAGE %EFF ERROR : 0.5367 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 94.1 +/-7.872 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1416E+OO dpm 2.9574E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.42 5887.58 TH-228 5363.00 5405.45 TH-229 4900.00 4926.91 TH-230 4671.39 4652.96 TH-232 3972.00 3998.87 10 TH-232:3796-40B5keV TH-230: 4495-4745 keV 9 TH-229: 4775-5142 keV TH-228: 5211-5493 keV AC-227:5510-6128keV 8 7 6 en 5 I-z => 4 0 8 3 2 *:;: t5 <( 4353 2756 3163 3574 Energy (keV) PEAK FWHM 337.206 113.932 5.008 145.232 87.640 COUNT DATE : 22-Sep-2016 13:44:16 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 207.000 196.920 10.080 3.1749 100.000 1.32E+01 20.000 17.072 2.400 1.5492 99.940 1.45E+OO 8.000 6.800 1.200 1.0954 99.469 4.39E-01 12.000 11.280 0.720 0.8485 99.700 7.26E-01 15.000 15.000 . 0.000 0.0000 100.000 9.62E-01 >> g i:i Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B032.CNF;1838 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W032.CNF;509 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.85E+OO 8.10E-01 3.93E-01 4.73E-01 5.27E-01 NOTES: MDA pCi/G 9.84E-01 7.78E-01 4.52E-01 3.93E-01 1.92E-01 Le pCi/G 3.91E-01 2.61E-01 1.29E-01 1.00E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.91E+OO 7.74E-01 3.87E-01 4.59E-01 5.04E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracernominal includes 2.1197E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.528 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S0405235060 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 033 DETECTOR S/N : 83293 AVERAGE %EFFICIENCY : 32.6568 AVERAGE %EFF ERROR : 0.6295. SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 72.5 +/-8.438 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1416E+OO dpm 2.2777E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.42 5916.77 TH-228 5363.00 5382.75 TH-229 4900.00 4842.99 TH-230 4671.39 4676.69 TH-232 3972.00 4018.46 11 TH-232:3796-408SkeV TH-230: 4495-4745 keV 10 TH-229:4n5-5142keV TH-228: 5211*5493 keV 9 AC-'12.7:5510-6128keV 8 7 Cii 6 I-z 5 ::i 0 4 s 3 *;;: 2 u <!'. 1 2377 2776 3179 Energy (keV) PEAK FWHM 287.162 4.964 4.964 59.567 34.747 ': > * ': COUNT DATE : 22-Sep-2016 13:44:16 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 197.000 178.520 18.480 4.2988 100.000 1.40E+01 6.000 4.081 1.440 1.2000 99.940 4.04E-01 1.000 -0.680 1.680 1.2961 99.469 -5.11E-02 16.000 15.520 0.480 0.6928 99.700 1.16E+OO 10.000 10.000 0.000 0.0000 100.000 7.48E-01 >

g g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B033.CNF;1823 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W033.CNF;546 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 3.24E+OO 5.33E-01 2.32E-01 6.41E-01 5.04E-01 NOTES: MDA pCi/G 1.47E+OO 7.87E-01 5.83E-01 4.15E-01 2.24E-01 Le pCi/G 6.17E-01 2.45E-01 1.79E-01 9.52E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.19E+OO 5.28E-01 2.31E-01 6.09E-01 4.87E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1197E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.479 +/-0.003)

AlphaSpeciroscopySoftwareVers!on3.5.3 effeetivedate:02-Mar-2015 BATCH NUMBER : 1596407 SAMPLE ID : S1203621736 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.128 G -+/-0.781 % CHAMBER : 034 DETECTOR S/N : 61586 AVERAGE %EFFICIENCY : 32.5970 AVERAGE %EFF ERROR : 0.6285 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 68.3 +/-8.641 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-8-402 AC-227 3.1416E+OO dpm 2.1464E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.42 5898.89 TH-228 5363.00 5353.47 TH-229 4900.00 5071.38 TH-230 4671.39 4711.04 TH-232 3972.00 3940.43 7 TH*232: 37964085 keV TH-230: 4495-4745 keV TH-229: 4775-5142 keV 6 TH-228: 5211-5493 keV AC-227: 551D-6128 keV 5 'iii' 4 I-z 3 :::J 0 2 *::; <{ 2371 2771 3176 3584 Energy (keV) PEAK FWHM 337.132 4.973 119.353 0.000 0.000 399 COUNT DATE : 22-Sep-201613:44:16 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 184.000 167.920 16.080 4.0100 100.000 1.16E+01 6.000 4.590 0.960 0.9798 99.940 3.03E-01 2.000 0.560 1.440 1.2000 99.469 3.71E-02 2.000 1.520 0.480 0.6928 99.700 1.00E-01 0.000 -0.240 0.240 0.4899 100.000 -1.58E-02 g :;::g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B034.CNF;1836 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W034.CNF;481 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.74E+OO 3.54E-01 2.40E-01 2.31E-01 1.37E-01 NOTES: MDA pCi/G 1.22E+OO 4.77E-01 4.90E-01 3.66E-01 3.16E-01 Le pCi/G 5.07E-01 1.39E-01 1.45E-01 8.38E-02 5.91E-02 1.96-sigma cnt Unc pCi/G 1.86E+OO 3.50E-01 2.39E-01 2.31E-01 1.36E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1197E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.450 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S1203621737 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.128 G -+/-0.781 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 87.6 +/-8.151 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1430E+OO dpm 2.7534E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.15 5920.96 TH-228 5363.00 5406.73 TH-229 4900.00 4790.89 TH-230 4671.39 4656.83 TH-232 3972.00 4011.17 9 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4775-5142 keV 8 TH-228: 5211-5493 keV AC-227: 551CHi128 keV 7 6 en 5 I-z 4 ::i 0 3 s 2 *:;; :g 1 <l'. 2402 2798 3198 3603 Energy (keV) PEAK FWHM 334.199 9.858 4.929 128.159 55.453 COUNT DATE : 22-Sep-2016 14:25:33 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 175.000 173.320 1.680 1.2961 100.000 1.16E+01 16.000 14.086 1.440 1.2000 99.940 1.21E+OO 1.000 1.000 0.000 0.0000 99.469 6.42E-02 4.000 3.520 0.480 0.6928 99.700 2.25E-01 14.000 13.520 0.480 0.6928 100.000 8.63E-01 ] ] t;t; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B169.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.59E+OO 5.19E-01 1.59E-01 7.31E-01 6.82E-01 2.12E-01 1.B1E-01 1.92E-01 O.OOE+OO 2.8BE-01 3.54E-01 8.12E-02 5.08E-01 3.53E-01 8.10E-02 NOTES: 1.96-sigma cnt Unc pCi/G 1.74E+OO 7.02E-01 1.BOE-01 2.B5E-01 4.B7E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1649E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.474 +/-0.003)

BATCH NUMBER : 1596407 SAMPLE ID : S1203621738 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.128 G -+/-0.781 % CHAMBER : 170 DETECTOR S/N : 72549 AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 58.8 +/-9.988 % AC-227 SEP. : 21-Sep-2016 09:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1430E+OO dpm 1.8486E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.15 TH-228 5363.00 TH-229 4900.00 TH-230 4671.39 TH-232 3972.00 13 12 11 10 9 8 7 6 5 4 3 2 TH-229: 4n5-5142 keV TH-228:5211-5493keV AC-227:551Q-6128keV 2386 2785 3187 Energy (keV) 5913.02 5353.12 4882.97 4669.80 4055.13 PEAK FWHM 299.789 89.193 203.163 61.011 4.955 > COUNT DATE : 22-Sep-2016 14:25:35 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 1242-H NUCLIDE TH-230 NOMINAL (pCi/G) 1.6352E+01 % RECOVERY 101.057 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 118.000 114.160 3.840 1.9596 100.000 1.16E+01 3.000 0.048 2.640 1.6248 99.940 4.62E-03 2.000 1.520 0.480 0.6928 99.469 1.48E-01 171.000 170.040 0.960 0.9798 99.700 1.65E+01 1.000 1.000 0.000 0.0000 100.000 9.69E-02 6985 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B170.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.19E+OO 4.13E-01 3.41E-01 4.14E+OO 2.73E-01 NOTES: MDA pCi/G 1.03E+OO 8.97E-01 5.39E-01 6.40E-01 2.91E-01 Le pCi/G 3.65E-01 3.03E-01 1.24E-01 1.74E-01 0.00E+OO 1.96-sigma cnt Unc pCi/G 2.18E+OO 4.13E-01 3.40E-01 2.50E+OO 2.72E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1650E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.312 +/-0.002)

Effective 3/25/201 O Revision 1 Effective March 2010 Batch# Product:lh Criteria: SamDle Solids are less than or equal to 100 mo for GAB. Samples have been blank corrected (If required). Blank correction renorted included (Jf reoulredl. lf activity less than 10x MDA/ MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error ls,40% or less. lrf hn(-*** *'--MD4 / .,,..,. "rrn* I,; nk"'" Instrument source check Is within limits. Inctrument bko check Is within limits. Method RDL/ LLD has been met. If duDllcate activities are: Less than 5* MDA/ M.DC, then RPD Is 100% or less, lf greater 5* MDA/ MDC, then RPD 20% or less, If below the MDA/ MDC, the RPD Is 0%, Or meets the client's reouired RER acceotance criteria. Tracer yield Is 15-125%

Carrier yield 25-125%. {Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. 1 ......... < 50/n nf lftouM* "l'.tivitvl Radiochemistry Batch Checklist 27-Sep-2016 Yes No Comments N.rF\ f\Jf\ " !'---'-N -'-.......... "" N ......... i--' ...... I 6 )6/\.,-W-Samole was run within hold time. Samnle was correctlv nreserved If renulred. (V>f-'\ Smears Taken for Radioactive batches. (W'\ ........ f--J Method Spike and LCS are within 75-1250/o ltor the clhmt'.: arcentanr-A r-ritPri"'* ., !'--No blank spaces on data forms. All line outs Initialed and dated. IN-------..... Aux data Is correct. f'Y1"'\ ........ I'-' Client Sneclal reouirements nane has been checked. Raw Data and I or soectrum are Included and orooerlv statused. r--. MS. LCS, and Duplicate RPD/RER values uploaded to UMS and """ ""'I nae uarlna,f " UI> llf ,N..>f n-a.-1.. __ ., ___ ..,. 1 ..... .-r---N:lll--a.: .. -.... I Batch Data Exceotlon Reoorts lDERl comoleted If aoollcable. '-... :--.> \..A.-I 'c>L1 YI J lo Batch Data Exception Reports {DER) second reviewed. 'I'--()::fl \h ) s /; '-l ) J {[) Dlsnositlon verified to be comnleted. All-.. -t Cnrr<>rtlnn rnmn(1>ted If --ulrel'I. N'J0, Review sample historical results Ir available ....r--..i (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. \ Primary Review Performed By: _ --/-"---'-"'"\ _J a-"'-) __,_4 j_J lo 10/04/16 C Page 568 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 04-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, Th-01-RC Solid .. Batch ID: Sample Numbers: 1596395 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, and 1203621707 were received and analyzed outside of the holding time. Originator's Name: Data Validator/Group Leader: Jessica Downey 04-0CT-16 Jessica Davis 04-0CT-16 Page 1 Page 569 of 5809 DER Report No.: 1564126 Revision No.: ' Type: Process Client Code: MJWC Thorium (Ac-227 Tracer) Queue Sheet Batch#: 1596395 Analyst: MXS2 Tracer Tracer Code: B -1../0-Z.... LCS Isotope: , Th-232 LCS Code: /Z...<-/7..' H First Client Due Date:04-0CT-16 Expiration Date: )-3J-II Expiration Date: 'Z-I /-f7 Internal Due Date30-SEP-16 Vol:_Qj_ Ac-227 Separation Dateffime: Vol:_Q}_ Vol:-=-Spike Isotope: Th-230, Th-23'.!ipike Code:._______ Expiration Date: ____ _ Prep Date: C, ** ZA .-1 lP Initials: .ti'-)]) Pipet ID: i Balance ID:. _ _,_,.,'"""""-'--"'-'-'= 1 lol o I Cq Ce'.2-__ _ Sample ID Client Description Type 405235021-1 4.2B.R.2.3 SAMPLE 405235022-1 4.2B.R.1.3 SAMPLE 405235023-1 4.2B.R.11.2 SAMPLE 405235024-1 4.2B.R.2.2 SAMPLE 405235025-1 4.2B.R.1.2 SAMPLE 405235026-1 4.2C.R.1.3 SAMPLE 405235027-1 4.2C.R.1.4

SAMPLE 405235028-1 4.3.ARl.3 SA.l\ll'LE 405235029-1 4.3.B.R.1-1 SAMPLE 405235030-1 4.3A.R.2.3 SAMPLE 405235031-1 4.3.BR19.2 SA.'\f.PLE 405235032-1 4.3B.R.3.3 SAMPLE 405235033-1 4.3B.R.3.4 SAMPLE 405235034-1 4.3.B.R.1.4 SAMPLE 405235035-1 4.3B.R.2.3 SAMPLE 405235036-1 4.3B.R.2.4 SAi'\ll'LE 405235037-1 4.4C.R.2.4 SAMPLE 405235038-1 4.4C.R.1.3 SA:MPLE 405235039-1 4.4C.R.l.4 SAMPLE 405235040-1 4.4D.R.1.3 SA:MPLE 1203621706-1 l\1B for batch 1596395 MB 1203621707-1 4.2B.R.2.3(405235021DUP) DUP 1203621708-1 LCS for batch 1596395 LCS Choose SOP Used: GL-RAD-A-038/ GL-RAD-A-032 GEL Laboratories LLC, Radiochemistry Division Hazard Min Code CRDL Matrix 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL lpCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL l pCi/g SOIL 1 pCi/g SOIL Solid Sample Dissolution by: Client MJWCOOl MJWCOOl M.JWCOOl M.JWCOOl M.JWCOOl MJWCOOl M.JWCOOl l\lJWCOOl l\lJWCOOl M.JWCOOl MJWCOOl MJWCOOl M.JWCOOl MJWCOOl M.JWCOOl l\lJWCOOl l\UWCOOl MJWCOOl M.JWCOOl .MJWCOOl QCACCOUNf QC ACCOUNT QCACCOUNf e Collection Date 08-DEC-15 08-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 23-NOV-15 23-NOV-15 23-NOV-15 26-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 08-DEC-15 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 (5'lp Y} / y Ji 0 07-SEP-16 Page 1 oil '

BATCH NUMBER : 1596395 SAMPLE ID : S0405235021 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.107 G -+/-0.935 % CHAMBER : 033 DETECTOR S/N : 83293 AVERAGE %EFFICIENCY : 32.6568 AVERAGE %EFF ERROR : 0.6295 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 95.9 +/-7.329 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 3.0132E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.21 5887.44 TH-228 5363.00 5405.61 TH-229 4900.00 4958.10 TH-230 4671.39 4685.22 TH-232 3972.00 3987.89 13 TH-232:3796-4085keV TH-230: 44954745 keV 12 TH-229: 4nS-5142 keV TH-228:5211*5493keV 11 AC.227:5510-6128keV 10 9 8 UJ 7 I-6 z :::i 5 0 4 3 *s: 2 2377 2776 3179 3587 Energy (keV) PEAK FWHM 302.008 67.013 0.000 54.603 119.134 COUNT DATE : 24-Sep-2016 13:16:16 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 252.000 236.160 15.840 3.9799 100.000 1.39E+01 17.000 15.157 1.200 1.0954 99.940 1.13E+OO 0.000 -0.240 0.240 0.4899 99.469 -1.35E-02 14.000 14.000 0.000 0.0000 99.700 7.87E-01 12.000 11.520 0.480 0.6928 100.000 6.45E-01 g 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B033.CNF;1825 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W033.CNF;546 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.78E+OO 6.53E-01 1.17E-01 4.43E-01 4.10E-01 NOTES: MDA pCi/G 1.03E+OO 5.84E-01 2.70E-01 1.69E-01 3.10E-01 Le pCi/G 4.28E-01 1.80E-01 5.05E-02 O.OOE+OO 7.11E-02 1.96-sigma cnt Unc pCi/G 1.85E+OO 6.29E-01 1.17E-01 4.27E-01 3.98E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1544E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.643 +/-0.004)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235022 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 038 DETECTOR S/N : 72532 AVERAGE %EFFICIENCY : 35.8983 AVERAGE %EFF ERROR : 0.6908 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 91.0 +/-7.143 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.8585E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.21 5887.91 TH-228 5363.00 5435.76 TH-229 4900.00 5135.18 TH-230 4671.39 4635.78 TH-232 3972.00 4009.24 11 TH-232:3796-4085keV TH-230: 4495-4745 keV 10 TH-229: 4nS-S142 keV TH-228:5211-5493keV 9 AC-227:5510-6128keV 8 7 00 6 I-z 5 ::> 0 4 3 *::; 2 u 1 <l'. 2401 2799 3200 3606 Energy (keV) PEAK FWHM 329.431 33.331 4.938 27.159 153.076 COUNT DATE : 24-Sep-2016 13:16:17 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 259.000 246.280 12.720 3.5665 100.000 1.44E+01 16.000 14.369 0.960 0.9798 99.940 1.07E+OO 1.000 0.760 0.240 0.4899 99.469 4.26E-02 14.000 13.760 0.240 0.4899 99.700 7.70E-01 8.000 7.760 0.240 0.4899 100.000 4.33E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B038.CNF;1826 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W038.CNF;499 CAL DATE : 29-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCl/G pCi/G 2.81E+OO 9.40E-01 3.82E-01 6.30E-01 5.58E-01 1.67E-01 1.60E-01 2.69E-01 5.03E-02 4.41E-01 2.68E-01 5.02E-02 3.36E-01 2.68E-01 5.01E-02 NOTES: 1.96-sigma en! Une pCi/G 1.86E+OO 6.08E-01 1.60E-01 4.26E-01 3.30E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1544E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.671 +/-0.004)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235023 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 040 DETECTOR S/N : 78773 AVERAGE %EFFICIENCY : 32.4791 AVERAGE %EFF ERROR : 0.6262 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.5 +/-7.582 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.7813E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.21 5882.40 TH-228 5363.00 5399.56 TH-229 4900.00 4942.20 TH-230 4671.39 4673.00 TH-232 3972.00 4009.96 11 TH-232: 3796-4085 keV TH-+230: 4495-4745 keV 10 TH-229: 4775-5142 keV TH-22B:5211-5493keV 9 AC-227: 551D-6128 keV 8 7 00 6 I-z 5 ::J 0 4 f2. 3 *:;; 2 n <t: 2382 2778 3178 3582 Energy (keV) PEAK FWHM 309.760 137.671 78.669 9.014 34.418 COUNT DATE : 24-Sep-2016 13:16:17 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 230.000 216.800 13.200 3.6332 100.000 1.47E+01 16.000 14.449 0.960 0.9798 99.940 1.26E+OO 2.000 1.520 0.480 0.6928 99.469 9.88E-02 15.000 14.040 0.960 0.9798 99.700 9.10E-01 14.000 13.280 0.720 0.8485 100.000 8.58E-01 g ii Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B040.CNF;1829 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W040.CNF;485 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 3.05E+OO 7.37E-01 2.27E-01 5.32E-01 5.12E-01 NOTES: MDA pCi/G 1.11E+OO 6.42E-01 3.60E-01 4.27E-01 3.95E-01 Le pCi/G 4.51E-01 1.91E-01 8.25E-02 1.16E-01 1.00E-01 1.96-sigma cnt Unc pCi/G 2.03E+OO 7.08E-01 2.27E-01 5.13E-01 4.94E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1544E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.591 +/-0.004)

AlphaSpeclft:lscopySoftwareVerslon3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235024 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 041 DETECTOR SIN : 78205 AVERAGE %EFFICIENCY : 34.2140 AVERAGE %EFF ERROR : 0.6590 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 45.0 +/-10.404 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387"B-402 AC-227 3.1422E+OO dpm 1.4141 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.21 5907.13 TH-228 5363.00 5429.29 TH-229 4900.00 4835.49 TH-230 4671.39 4686.95 TH-232 3972.00 4012.95 7 TH-232: 37964085 keV TH-230:4495-4745keV TH-229: 4n5-5142 keV 6 TH-228:52t1-5493keV AC-227: 5510-6128 keV 5 (ii 4 I-z 3 => 0 2 *;;; t5 <i: 2408 2801 3199 3602 Energy (keV) PEAK FWHM 312.061 6.099 4.879 117.099 7.319 COUNT DATE : 24-Sep-2016 13:16:17 ELAPSED LIVE TIME(SEC) : 14399.99

NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 131.000 116.120 14.880 3.8575 100.000 1.40E+01 11.000 8.764 1.920 1.3856 99.940 1.35E+OO 1.000 0.280 0.720 0.8485 99.469 3.24E-02 3.000 2.280 0.720 0.8485 99.700 2.63E-01 7.000 7.000 0.000 0.0000 100.000 8.05E-01 ii g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B041.CNF;1825 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W041.CNF;529 CAL DATE : 29-Aug-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.01E+OO 2.07E+OO 8.52E-01 1.10E+OO 1.29E+OO 4.15E-01 3.39E-01 7.06E-01 1.80E-01 4.68E-01 7.05E-01 1.79E-01 6.61E-01 3.45E-01 O.OOE+OO NOTES: 1.96-sigma cnt Unc pCi/G 2.75E+OO 1.07E+OO 3.38E-01 4.65E-01 6.40E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1544E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.316 +/-0.002)

AlphaSpeclroscopySoftwareVerslon3.5.3 effeetivedate:02-Mar-2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235025 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.111 G -+/-0.901 % CHAMBER : 042 DETECTOR S/N : 78793 AVERAGE %EFFICIENCY : 33.3976 AVERAGE %EFF ERROR : 0.6435 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 96.9 +/-7.177 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 3.0446E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.21 5907.34 TH-228 5363.00 5404.64 TH-229 4900.00 4952.43 TH-230 4671.39 4655.51 TH-232 3972.00 4003.11 11 TH-232:3795-4005keV TH-230:4495-4745keV 10 TH-229: 4775-5142 keV TH-228:5211-5493keV 9 AC.227:5510-6128keV 8 7 U) I-6 z 5 ::> 0 4 s 3 2 ti <( 2383 2778 3178 3583 Energy (keV) PEAK FWHM 65.241 54.017 4.911 34.374 24.553 COUNT DATE : 24-Sep-2016 13:16:17 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 257.000 244.040 12.960 3.6000 100.000 1.34E+01 20.000 17.895 1.440 1.2000 99.940 1.25E+OO 1.000 0.280 0.720 0.8485 99.469 1.47E-02 20.000 17.600 2.400 1.5492 99.700 9.22E-01 15.000 14.520 0.480 0.6928 100.000 7.59E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B042.CNF;1823 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W042.CNF;490 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.62E+OO 6.61E-01 1.54E-01 4.97E-01 4.27E-01 NOTES: MDA pCi/G 8.87E-01 5.69E-01 3.21E-01 4.55E-01 2.89E-01 Le pCi/G 3.61E-01 1.80E-01 8.17E-02 1.49E-01 6.63E-02 1.96-sigma cnt Unc pCi/G 1.74E+OO 6.33E-01 1.54E-01 4.78E-01 4.12E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1544E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.665 +/-0.004)

Alpha Spectmsoopy Software Version 3.5.3 effedivedate:02-Mar*2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235026 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.113 G -+/-0.885 % CHAMBER : 161 DETECTOR S/N : 70321 AVERAGE %EFFICIENCY : 25.7727 AVERAGE %EFF ERROR : 0.4995 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 92.0 +/-8.026 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.8907E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5840.46 TH-228 5363.00 5390.77 TH-229 4900.00 5022.99 TH-230 4671.39 4641.67 TH-232 3972.00 3992.00 7 TH*232: 37964085 keV TH-230: 4495-4745 keV TH-229: 4nS.5142 keV 6 TH-228:5211-5493keV AC-227: S51o-6128 keV 5 (ii 4 f-z 3 => 0 2 *::; u <( 2394 2792 3193 3599 Energy (keV) PEAK FWHM 346.083 64.272 113.713 4.944 54.384 :i i!i 400 COUNT DATE : 24-Sep-2016 13:17:52 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 180.000 178.800 1.200 1.0954 100.000 1.31E+01 19.000 18.032 0.480 0.6928 99.940 1.69E+OO 3.000 2.760 0.240 0.4899 99.469 1.94E-01 12.000 11.280 0.720 0.8485 99.700 7.93E-01 12.000 11.760 0.240 0.4899 100.000 8.24E-01 :i :i :i g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B161.CNF;860 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W161.CNF;261 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.89E+OO 8.71E-01 2.82E-01 5.17E-01 5.15E-01 NOTES: MDA pCi/G 5.15E-01 6.01E-01 3.38E-01 4.29E-01 3.36E-01 Le pCi/G 1.47E-01 1.60E-01 6.32E-02 1.09E-01 6.29E-02 1.96-sigma cnt Unc pCi/G 1.94E+OO 8.24E-01 2.80E-01 5.01E-01 4.97E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1562E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.488 +/-0.003)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235027 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 162 DETECTOR S/N : 70323 AVERAGE %EFFICIENCY : 26.6669 AVERAGE %EFF ERROR : 0.5165 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.9 +/-8.026 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.7937E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5916.65 TH-228 5363.00 5431.76 TH-229 4900.00 5031.01 TH-230 4671.39 4664.41 TH-232 3972.00 4020.23 8 TH-232;3796-4085keV TH-230: 4495-4745 keV TH-229: 4nS.5142 keV 7 TH-228: 5211-5493 keV AC-227:551D-612BkeV 6 5 'iii 4 I-z :J 3 0 s ;::. 2 *:;; u <( 2383 2782 3184 Energy (keV) PEAK FWHM 337.694 9.922 74.413 7.441 58.290 COUNT DATE : 24-Sep-2016 13:17:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 180.000 178.800 1.200 1.0954 100.000 1.22E+01 10.000 8.312 1.200 1.0954 99.940 7.21E-01 3.000 2.520 0.480 0.6928 99.469 1.64E-01 14.000 14.000 0.000 0.0000 99.700 9.11E-01 17.000 17.000 0.000 0.0000 100.000 1.10E+OO 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B162.CNF;862 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W162.CNF;260 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.67E+OO 5.86E-01 2.63E-01 5.17E-01 5.69E-01 NOTES: MDA pCi/G 4.77E-01 6.61E-01 3.61E-01 1.95E-01 1.95E-01 Le pCi/G 1.37E-01 2.01E-01 8.28E-02 O.OOE+OO O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.80E+OO 5.73E-01 2.61E-01 4.95E-01 5.40E-01

Ac-227 results are decay corrected to separation date/time.
Tracer nominal includes 2.1562E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.488 +/-0.003)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235028 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 80.9 +/-8.371 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.5423E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5891.35 TH-228 5363.00 5412.74 TH-229 4900.00 4963.98 TH-230 4671.39 4693.71 TH-232 3972.00 4030.07 7 TH-232:37!IB-408SkeV TH-230: 4495-4745 keV TH-229: 4n5-S142 keV 6 TH-228:5211*5493keV AC-227:5510.0128keV 5 w 4 I-z 3 :J 0 s 2 *:;; 2383 2781 3184 3590 Energy (keV) PEAK FWHM 335.562 81.724 4.953 59.435 23.733 400 COUNT DATE : 24-Sep-2016 13:17:57 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 164.000 162.800 1.200 1.0954 100.000 1.41E+01 13.000 10.876 1.680 1.2961 99.940 1.22E+OO 1.000 0.760 0.240 0.4899 99.469 6.33E-02 15.000 14.760 0.240 0.4899 99.700 1.23E+OO 21.000 20.760 0.240 0.4899 100.000 1.72E+OO a Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B166.CNF;891 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.24E+OO 6.09E-01 1.74E-01 8.65E-01 9.25E-01 2.94E-01 2.38E-01 3.99E-01 7.47E-02 6.86E-01 3.98E-01 7.45E-02 8.17E-01 3.97E-01 7.43E-02 NOTES: 1.96-sigma cnt Unc pCi/G 2.19E+OO 8.37E-01 2.37E-01 6.53E-01 7.63E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1562E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.444 +/-0.003)

"d Vt -..J '° 0 ...., Vt 00 0 '° AlphaSpectroscopySoftwareVersionJ.5.3 effecUvedate:02-Mar-2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235029 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.111 G -+/-0.901 % CHAMBER : 167 DETECTOR S/N : 72546 AVERAGE %EFFICIENCY : 24.1606 AVERAGE %EFF ERROR : 0.4690 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.0 +/-8.471 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.7655E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5888.57 TH-228 5363.00 5391.80 TH-229 4900.00 4955.26 TH-230 4671.39 4692.14 TH-232 3972.00 4006.65 8 TH-232:3796-40a5keV TH-230: 4495-4745 keV TH-229: 4775-5142 keV 7 TH-228: 5211-5493 keV AC-227:5510-6128keV 6 5 en 4 I-z :J 3 0 s c 2 *:;; f5 <!'. 2378 2780 3185 3594 Energy (keV) PEAK FWHM 323.837 7.502 5.001 15.004 73.770 400 COUNT DATE : 24-Sep-2016 13:17:59 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 163.000 160.360 2.640 1.6248 100.000 1.34E+01 9.000 8.563 0.000 0.0000 99.940 9.24E-01 1.000 0.760 0.240 0.4899 99.469 6.08E-02 11.000 9.560 1.440 1.2000 99.700 7.62E-01 14.000 13.280 0.720 0.8485 100.000 1.06E+OO f:j Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B167.CNF;886 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W167.CNF;246 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.11E+OO 6.91E-01 2.28E-01 5.66E-01 6.35E-01 NOTES: MDA pCi/G 7.47E-01 5.58E-01 3.83E-01 5.90E-01 4.86E-01 Le pCi/G 2.48E-01 1.17E-01 7.17E-02 1.75E-01 1.24E-01 1.96-sigma cnt Unc pCi/G 2.10E+OO 6.71E-01 2.28E-01 5.51E-01 6.08E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1563E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.437 +/-0.003)

>'!;) Cl> V1 00 0 0 ....., V1 00 0 "' BATCH NUMBER : 1596395 SAMPLE ID : S0405235030 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 101 +/-7.641 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER , ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 3.1741E+OO dpm NUCLIDE LIBRARY PEAK w 1--z ::> 0 8 *s: ti <( ENERGY ENERGY AC-227 5869.20 5910.36 TH-228 5363.00 5450.22 TH-229 4900.00 4863.95 TH-230 4671.39 4679.10 TH-232 3972.00 4031.79 10 TH-232:3796-4085keV TH-230: 4495-4745 keV 9 TH-229: 4nS.5142 keV TH-228: 5211-5493 keV AC-227:5510-0126keV 8 7 6 5 4 3 2 1 2402 2798 3198 3603 Energy (keV) PEAK FWHM 305.610 8.215 4.929 52.989 9.858 COUNT DATE : 24-Sep-2016 13:18:02 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 201.000 199.800 1.200 1.0954 100.000 1.43E+01 13.000 12.215 0.240 0.4899 99.940 1.13E+OO 1.000 0.040 0.960 0.9798 99.469 2.74E-03 15.000 14.280 0.720 0.8485 99.700 9.76E-01 18.000 17.760 0.240 0.4899 100.000 1.21E+OO > Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B169.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.98E+OO 7.05E-01 2.03E-01 5.60E-01 6.13E-01 NOTES: MDA pCi/G 5.01E-01 5.56E-01 4.51E-01 4.17E-01 3.27E-01 Le pCi/G 1.43E-01 1.40E-01 1.23E-01 1.06E-01 6.11E-02 1.96-sigma cnt Unc pCi/G 1.99E+OO 6.80E-01 2.03E-01 5.39E-01 5.84E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1563E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.545 +/-0.004) 0 ....., V\ 00 0 "' A!phaSpectroscopySoftwareVerslon3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235031 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 170 DETECTOR S/N : 72549 AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 109 +/-7.490 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 3.4188E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5896.34 TH-228 5363.00 5418.75 TH-229 4900.00 4972.40 TH-230 4671.39 4645.90 TH-232 3972.00 4008.73 9 TH-232: 3796-4085 keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 8 TH-228: 5211-5493 keV AC-227:551D-6128keV 7 6 (j) 5 I-z 4 => 0 3 .?;-2 *;; n 2386 2785 3187 Energy (keV) PEAK FWHM 329.726 63.179 24.776 81.761 14.866 COUNT DATE : 24-Sep-2016 13:18:04 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 214.000 211.120 2.880 1.6971 100.000 1.46E+01 17.000 13.304 3.120 1.7664 99.940 1.18E+OO 2.000 1.280 0.720 0.8485 99.469 8.46E-02 13.000 12.760 0.240 0.4899 99.700 8.41E-01 14.000 13.520 0.480 0.6928 100.000 8.89E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B170.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.98E+OO 7.79E-01 2.33E-01 5.02E-01 5.20E-01 NOTES: MDA pCi/G 6.35E-01 8.83E-01 4.04E-01 3.16E-01 3.64E-01 Le pCi/G 2.14E-01 3.08E-01 1.03E-01 5.92E-02 8.34E-02 1.96-sigma cnt Unc pCi/G 1.98E+OO 7.56E-01 2.33E-01 4.85E-01 5.02E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1564E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.576 +/-0.004)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235032 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLEQTY: 0.114G -+/-0.877% CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 91.6 +/-7.977 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.8796E+OO dpm NUCLIDE LIBRARY PEAK en 1--z :::> 0 s *:;; t5 <I'. ENERGY ENERGY AC-227 5869.20 5875.01 TH-228 5363.00 5388.83 TH-229 4900.00 4997.36 TH-230 4671.39 4652.19 TH-232 3972.00 3995.29 10 TH-232: 3796-4065 keV TH-230: 4495-4745 keV 9 TH-229: 4nS-5142 kaV TH-228: 5211-5493 keV AC-227:5510.0128keV 8 7 6 5 4 3 2 2363 2764 3168 3575 Energy (keV) PEAK FWHM 311.902 112.106 194.316 7.474 32.386 ¥ COUNT DATE : 24-Sep-201613:18:06 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 183.000 181.560 1.440 1.2000 100.000 1.30E+01 17.000 16.505 0.000 0.0000 99.940 1.53E+OO 2.000 1.520 0.480 0.6928 99.469 1.05E-01 9.000 8.760 0.240 0.4899 99.700 6.01E-01 17.000 17.000 0.000 0.0000 100.000 1.16E+OO >> ]! !l.: Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B175.CNF;870 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.84E+OO 8.14E-01 2.41E-01 4.38E-01 6.00E-01 NOTES: MDA pCi/G 5.30E-01 4.93E-01 3.81E-01 3.29E-01 2.05E-01 Le pCi/G 1.58E-01 1.07E-01 8.73E-02 6.16E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.91E+OO 7.73E-01 2.40E-01 4.28E-01 5.70E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1564E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.495 +/-0.003)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235033 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 176 DETECTOR S/N : 74434 AVERAGE %EFFICIENCY : 25.6995 AVERAGE %EFF ERROR : 0.4981 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 74.5 +/-8.860 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.3399E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5897.69 TH-228 5363.00 5396.86 TH-229 4900.00 5127.49 TH-230 4671.39 4671.00 TH-232 3972.00 4007.78 7 TH-232: 3796-4085 keV TH-230: 4495-4745 keV TH*229; 4n5-5142 keV 6 TH-228: 5211-5493 keV AC-227: 5510-6128 keV 5 UJ 4 I-z 3 =i 0 .?;-2 *:;; t5 < 2379 2776 3177 3582 Energy (keV) PEAK FWHM 326.064 7.402 4.935 39.478 9.870 COUNT DATE : 24-Sep-2016 13:18:08 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 146.000 144.320 1.680 1.2961 100.000 1.40E+01 6.000 5.366 0.240 0.4899 99.940 6.74E-01 1.000 0.280 0.720 0.8485 99.469 2.60E-02 8.000 6.320 1.680 1.2961 99.700 5.87E-01 9.000 8.520 0.480 0.6928 100.000 7.88E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B176.CNF;865 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.41E+OO 6.69E-01 2.73E-01 5.69E-01 5.95E-01 NOTES: MDA pCi/G 7.52E-01 7.20E-01 5.68E-01 7.19E-01 5.12E-01 Le pCi/G 2.30E-01 1.72E-01 1.45E-01 2.20E-01 1.17E-01 1.96-sigma cnt Unc pCi/G 2.31E+OO 6.56E-01 2.72E-01 5.59E-01 5.78E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1564E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.394 +/-0.003)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235034 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.119 G -+/-0.840 % CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.7 +/-8.069 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.7864E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5878.51 TH-228 5363.00 5416.46 TH-229 4900.00 4958.09 TH-230 4671.39 4641.34 TH-232 3972.00 4011.69 8 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 7 TH-228:5211-5493keV AC.227:551o.6128keV 6 5 Vi 4 I-z ::i 3 0 8 2 *5 2375 2774 3177 3583 Energy (keV) PEAK FWHM 315.896 33.448 0.000 4.955 40.881 399 i COUNT DATE : 24-Sep-2016 13:18:10 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 180.000 177.840 2.160 1.4697 100.000 1.25E+01 15.000 13.795 0.720 0.8485 99.940 1.25E+OO 0.000 0.000 0.000 0.0000 99.469 O.OOE+OO 7.000 7.000 0.000 0.0000 99.700 4.70E-01 15.000 14.760 0.240 0.4899 100.000 9.87E-01 >> ii 6989 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B177.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.76E+OO 7.47E-01 1.36E-01 3.81E-01 5.50E-01 NOTES: MDA pCi/G 5.88E-01 6.23E-01 2.02E-01 2.01E-01 3.21E-01 Le pCi/G 1.89E-01 1.75E-01 O.OOE+OO O.OOE+OO 6.00E-02 1.96-sigma cnt Unc pCi/G 1.85E+OO 7.16E-01 1.36E-01 3.73E-01 5.26E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1565E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.485 +/-0.003)

"' Vi 00 Vi 0 ....., Vi 00 0 "' BATCH NUMBER : 1596395 SAMPLE ID : S0405235035 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 207 DETECTOR S/N : 78910 AVERAGE %EFFICIENCY : 26.0138 AVERAGE %EFF ERROR : 0.5040 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 95.5 +/-7.735 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID : 0387-B-402 NUCLIDE : AC-227 NOMINAL : 3.2551E+OO dpm RES UL TS : 3.1080E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5842.16 5856.49 TH-228 5363.00 5411.21 TH-229 4900.00 4958.12 TH-230 4671.39 4657.72 TH-232 3972.00 3980.47 7 TH-23Z:3796-4085keV TH-230; 4495-4745 keV TH-229: 4ns-s14z keV 6 TH-228:5211*5493keV AC-227: 5510-6128 keV 5 4 z 3 :J 0 s 2 *:;; n <l'. 2375 2773 3175 3582 Energy (keV) PEAK FWHM 359.979 73.069 0.000 86.692 17.338 399 li COUNT DATE : 28-Sep-2016 17:56:50 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 195.000 194.040 0.960 0.9798 100.000 1.73E+01 14.000 12.223 0.000 0.0000 99.940 1.21E+OO 0.000 0.000 0.000 0.0000 99.469 O.OOE+OO 15.000 15.000 0.000 0.0000 99.700 1.09E+OO 13.000 12.760 0.240 0.4899 100.000 9.27E-01 ': >> g :;: Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B207.CNF;811 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W207.CNF;228 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.66E+OO 7.84E-01 1.48E-01 5.98E-01 5.55E-01 NOTES: MDA pCi/G 5.87E-01 7.31E-01 2.19E-01 2.19E-01 3.48E-01 Le pCi/G 1.60E-01 2.17E-01 O.OOE+OO O.OOE+OO 6.52E-02 1.96-sigma cnt Unc pCi/G 2.44E+OO 7.53E-01 1.47E-01 5.72E-01 5.35E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.5020E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.777 +/-0.012)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235036 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.117 G -+/-0.855 % CHAMBER : 179 DETECTOR S/N : 74437 AVERAGE %EFFICIENCY : 26.3751 AVERAGE %EFF ERROR : 0.5108 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 92.3 +/-7.938 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.8998E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5898.09 TH-228 5363.00 5395.28 TH-229 4900.00 4977.84 TH-230 4671.39 4659.12 TH-232 3972.00 4000.35 9 TH-232: 3796-4085 keV TH-230: 4495-4745 keV TH-229: 4ns-5142 keV 8 TH-228: 5211-5493 keV AC-227:5510-612BkeV 7 6 0' 5 z 4 => 0 3 c 2 *::; u <{ 2377 2775 3176 3582 Energy (keV) PEAK FWHM 316.014 34.587 4.941 7.411 28.410 {;; 399 COUNT DATE : 24-Sep-2016 13:18:15 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 185.000 183.560 1.440 1.2000 100.000 1.27E+01 15.000 13.779 0.720 0.8485 99.940 1.23E+OO 1.000 0.760 0.240 0.4899 99.469 5.04E-02 11.000 10.760 0.240 0.4899 99.700 7.11E-01 11.000 10.760 0.240 0.4899 100.000 7.09E-01 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B179.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W179.CNF;254 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.76E+OO 5.11E-01 1.52E-01 7.35E-01 6.15E-01 1.74E-01 1.89E-01 3.18E-01 5.95E-02 4.65E-01 3.17E-01 5.93E-02 4.64E-01 3.16E-01 5.91E-02 NOTES: 1.96-sigma cnt Unc pCi/G 1.85E+OO 7.06E-01 1.89E-01 4.51E-01 4.50E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1566E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.501 +/-0.003)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235037 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.114 G -+/-0.877 % CHAMBER : 180 DETECTOR S/N : 83295 AVERAGE %EFFICIENCY : 26.2740 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 70.6 +/-8.974 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.2170E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5880.51 TH-228 5363.00 5404.13 TH-229 4900.00 4859.41 TH-230 4671.39 4670.48 TH-232 3972.00 3974.53 7 TH-232:379S-4085keV TH*230: 4495-4745 keV TH-229: 4n5-5142 keV 6 TH-228:5211-5493keV AC-227:551a.£128keV 5 en 4 I-z 3 ;::) 0 2 .?;-*s: u <l'. 2377 2777 3181 Energy (keV) PEAK FWHM 332.873 67.197 4.978 39.820 4.978 COUNT DATE : 24-Sep-2016 13:18:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 141.000 139.800 1.200 1.0954 100.000 1.30E+01 10.000 9.379 0.240 0.4899 99.940 1.12E+OO 1.000 0.760 0.240 0.4899 99.469 6.79E-02 3.000 2.520 0.480 0.6928 99.700 2.24E-01 7.000 6.280 0.720 0.8485 100.000 5.58E-01 g :; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B180.CNF;879 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W180.CNF;230 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.21E+OO 6.53E-01 1.87E-01 8.10E-01 6.83E-01 1.62E-01 2.55E-01 4.28E-01 8.01E-02 3.59E-01 4.93E-01 1.13E-01 5.09E-01 5.43E-01 1.38E-01 NOTES: 1.96-sigma cnt Unc pCi/G 2.18E+OO 7.82E-01 2.55E-01 3.57E-01 4.99E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1566E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.381 +/-0.002)

Alpha Spedrosoopy Software Version 3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235038 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.115 G -+/-0.870 % CHAMBER : 182 DETECTOR S/N : 74440 AVERAGE %EFFICIENCY : 22.5384 AVERAGE %EFF ERROR : 0.4383 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 81.5 +/-9.021 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 2.5615E+OO dpm NUCLIDE LIBRARY PEAK (ii 1--z ::i 0 $ *:;; n <( ENERGY ENERGY AC-227 5869.20 5913.35 TH-228 5363.00 5441.12 TH-229 4900.00 4941.17 TH-230 4671.39 4676.07 TH-232 3972.00 4013.94 8 TH-232: 37964085 keV TH--230: 4495-4745 keV TH-229: 4775-5142 keV 7 TH-228: 5211-5493 keV AC-'Z1.7:5510-6128keV 6 5 4 3 2 2373 2774 3178 3585 Energy (keV) PEAK FWHM 262.671 29.906 179.434 54.827 5.483 COUNT DATE : 24-Sep-2016 13:18:20 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 140.000 138.560 1.440 1.2000 100.000 1.29E+01 12.000 10.902 0.720 0.8485 99.940 1.30E+OO 3.000 2.760 0.240 0.4899 99.469 2.46E-01 10.000 10.000 0.000 0.0000 99.700 8.91E-01 15.000 15.000 0.000 0.0000 100.000 1.33E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B182.CNF;320 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W182.CNF;95 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.20E+OO 6.89E-01 2.05E-01 8.88E-01 8.03E-01 2.22E-01 3.58E-01 4.28E-01 8.01E-02 6.03E-01 2.67E-01 O.OOE+OO 7.38E-01 2.66E-01 O.OOE+OO NOTES: 1.96-sigma en! Une pCl/G 2.17E+OO 8.53E-01 3.55E-01 5.81E-01 6.98E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1567E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.378 +/-0.002)

BATCH NUMBER : 1596395 SAMPLE ID : S0405235039 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.117 G -+/-0.855 % CHAMBER : 208 DETECTOR S/N : 78911 AVERAGE %EFFICIENCY : 26.1198 AVERAGE %EFF ERROR : 0.5060 SAMPLE DATE : '30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 90.4 +/-7.919 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2551E+OO dpm 2.9441E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5842.16 5852.22 TH-228 5363.00 5405.88 TH-229 4900.00 4930.54 TH-230 4671.39 4649.26 TH-232 3972.00 3996.80 8 TH*232:3796-4085keV TH-230: 44954745 keV TH-229: 4n5-5142 keV 7 TH-228; 5211*5493 keV AC-227:5510-e1:ZSkeV 6 5 en 4 1--z :::> 3 0 2 t5 <l'. 2383 2780 3181 3587 Energy (keV) PEAK FWHM 359.847 69.154 123.489 118.549 32.107 > COUNT DATE : 28-Sep-2016 17:56:52 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 186.000 184.560 1.440 1.2000 100.000 1.54E+01 15.000 12.350 0.960 0.9798 99.940 1.13E+OO 3.000 1.800 1.200 1.0954 99.469 1.23E-01 4.000 3.280 0.720 0.8485 99.700 2.23E-01 13.000 13.000 0.000 0.0000 100.000 8.83E-01 g 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B208.CNF;807 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W208.CNF;253 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.33E+OO 7.56E-01 2.80E-01 3.07E-01 5.19E-01 NOTES: MDA pCi/G 6.15E-01 7.89E-01 4.79E-01 4.16E-01 2.04E-01 Le pCi/G 1.83E-01 2.56E-01 1.37E-01 1.06E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.23E+OO 7.27E-01 2.79E-01 3.05E-01 4.99E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.5021E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.690 +/-0.011)

AlphaSpeciroscopySoftwareVersion3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596395 SAMPLE ID : S0405235040 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 185 DETECTOR S/N : 68615 AVERAGE %EFFICIENCY : 25.3535 AVERAGE %EFF ERROR : 0.4915 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 101 +/-7.793 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 3.1823E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5897.47 TH-228 5363.00 5424.50 TH-229 4900.00 4776.37 TH-230 4671.39 4690.56 TH-232 3972.00 4020.23 12 TH-232; 37964085 keV TH-230; 44954745 keV 11 TH-229: 4n5-5142 keV TH-228: 5211-5493 keV 10 AC-227: keV 9 8 Vi 7 I-6 z 5 :::> 0 4 s 3 *:;; 2 ti -<( 1 2380 2781 3186 3594 Energy (keV) PEAK FWHM 306.513 18.715 0.000 29.944 7.486 j COUNT DATE : 24-Sep-2016 13:18:25 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 197.000 193.640 3.360 1.8330 100.000 1.47E+01 13.000 11.752 0.720 0.8485 99.940 1.15E+OO 1.000 0.040 0.960 0.9798 99.469 2.91E-03 11.000 9.320 1.680 1.2961 99.700 6.77E-01 6.000 5.760 0.240 0.4899 100.000 4.17E-01 j j >> j 6986 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B185.CNF;859 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W185.CNF;237 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.14E+OO 7.46E-01 2.16E-01 5.14E-01 3.84E-01 NOTES: MDA pCi/G 7.37E-01 6.75E-01 4.79E-01 5.62E-01 3.47E-01 Le pCi/G 2.55E-01 1.91E-01 1.31E-01 1.72E-01 6.49E-02 1.96-sigma cnt Unc pCi/G 2.10E+OO 7.21E-01 2.16E-01 5.02E-01 3.78E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1568E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.528 +/-0.003) 0 ...., Vl 00 0 ID BATCH NUMBER : 1596395 SAMPLE ID : S1203621706 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 034 DETECTOR SIN : 61586 AVERAGE %EFFICIENCY : 32.5970 AVERAGE %EFF ERROR : 0.6285 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 98.4 +/-7.238 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1422E+OO dpm 3.0918E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.21 5912.72 TH-228 5363.00 5319.56 TH-229 4900.00 4919.98 TH-230 4671.39 4734.79 TH-232 3972.00 3940.43 11 TH-232: 3796-4085 keV TH-230: 44954745 keV 10 TH-229: 4nS-5142 keV TH*228:5211*5493keV 9 AC.227: 5510-6128 keV 8 7 00 I-6 z 5 :J 0 4 8 3 2 u 1 <( 2371 2771 3176 3584 Energy (keV) PEAK FWHM 337.546 4.973 114.380 4.973 0.000 COUNT DATE : 24-Sep-2016 13:16:16 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 257.000 241.880 15.120 3.8884 100.000 1.22E+01 1.000 -0.859 1.200 1.0954 99.940 -4.14E-02 2.000 1.280 0.720 0.8485 99.469 6.17E-02 1.000 -0.440 1.440 1.2000 99.700 -2.12E-02 0.000 -0.240 0.240 0.4899 100.000 -1.15E-02 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B034.CNF;1838 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W034.CNF;481 CAL DATE : 29-Aug-2016 1.96-sigma TPU pCi/G 2.40E+OO 1.45E-01 1.70E-01 1.46E-01 9.95E-02 NOTES: MDA pCi/G 8.67E-01 3.77E-01 2.95E-01 3.56E-01 2.30E-01 Le pCi/G 3.58E-01 1.16E-01 7.50E-02 1.06E-01 4.30E-02 1.96-sigma cnt Unc pCi/G 1.59E+OO 1.45E-01 1.70E-01 1.46E-01 9.93E-02
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1544E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.659 +/-0.004)

BATCH NUMBER : 1596395 SAMPLE ID : S1203621707 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 201 DETECTOR S/N : 78902 AVERAGE %EFFICIENCY : 26.2326 AVERAGE %EFF ERROR : 0.5081 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 92.2 +/-5.760 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2557E+OO dpm 3.0004E+OO dpm NUCLIDE LIBRARY PEAK en I-z 0 s. *:;: t5 <{ ENERGY ENERGY AC-227 5841.76 5849.42 TH-228 5363.00 5408.31 TH-229 4900.00 4941.32 TH-230 4671.39 4653.90 TH-232 3972.00 4030.12 TH-232: 37964085 keV 15 TH-+230: 4495-4745 keV TH-229; 4775-5142 keV TH-228: 5211-5493 keV 13 AC-227; 551D-612B keV 11 9 7 5 3 2375 2773 3175 3582 Energy (keV) PEAK FWHM 331.941 9.909 237.809 78.031 33.442 COUNT DATE : 28-Sep-2016 17:56:47 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 400.000 397.475 2.525 1.5890 100.000 1.75E+01 29.000 22.791 2.525 1.5890 99.940 1.10E+OO 5.000 2.980 2.020 1.4213 99.469 1.07E-01 20.000 18.990 1.010 1.0050 99.700 6.82E-01 13.000 12.495 0.505 0.7106 100.000 4.48E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B201.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W201.CNF;224 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.73E+OO 5.51E-01 1.91E-01 3.39E-01 2.73E-01 NOTES: MDA pCi/G 4.15E-01 5.77E-01 3.15E-01 2.54E-01 2.10E-01 Le pCi/G 1.41E-01 2.16E-01 1.03E-01 7.29E-02 5.14E-02 1.96-sigma cnt Unc pCi/G 1.73E+OO 5.29E-01 1.90E-01 3.29E-01 2.67E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 7.5940E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (3.684 +/-0.024)

BATCH NUMBER : 1596395 SAMPLE ID : S1203621708 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 187 DETECTOR S/N : 68620 AVERAGE %EFFICIENCY : 25.2519 AVERAGE %EFF ERROR : 0.4896 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 60.1 +/-10.374 % AC-227 SEP. : 23-Sep-2016 08:30:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1423E+OO dpm 1.8896E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5869.20 5907.97 TH-228 5363.00 5455.82 TH-229 4900.00 4827.54 TH-230 4671.39 4690.45 TH-232 3972.00 3940.45 19 TH-232: 37964085 keV TH-230: 4495-4745 keV 17 TH-229: 4n5-5142 keV TH-228:5211-5493keV AC'22.7: SSHl-6128 keV 15 13 Ui 11 I-9 z ::i 0 7 s 5 *s: 3 2387 2786 3188 3593 Energy (keV) PEAK FWHM 284.503 4.955 158.562 74.945 0.000 ill :l 400 COUNT DATE : 24-Sep-201613:18:31 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 1242-H NUCLIDE TH-230 NOMINAL (pCi/G) 1.7156E+01 % RECOVERY 112.347 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 127.000 114.520 12.480 3.5327 100.000 1.22E+01 1.000 0.208 0.480 0.6928 99.940 2.11E-02 6.000 0.000 6.000 2.4495 99.469 O.OOE+OO 194.000 189.680 4.320 2.0785 99.700 1.93E+01 0.000 -0.480 0.480 0.6928 100.000 -4.86E-02 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B187.CNF;854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W187.CNF;238 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCilG 3.47E+OO 2.95E-01 5.82E-01 4.88E+OO 2.16E-01 NOTES: MDA pCi/G 1.69E+OO 6.24E-01 1.22E+OO 1.08E+OO 5.61E-01 Le pCilG 6.88E-01 1.59E-01 4.57E-01 3.87E-01 1.29E-01 1.96-sigma cnt Unc pCi/G 2.38E+OO 2.94E-01 5.82E-01 2.79E+OO 2.15E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 2.1569E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.312 +/-0.002)

Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 30-Sep-2016 Batch#----'-1 ...... _ Product:. __ Date: Criteria: Yes No Comments Samole Solids are less than or eaual to 100 mr:i for GAB. Samples have been blank corrected (If required). lli Blank correction renorted Included rlf r"'1ulred). If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 400/o or less. v llf "'"'""' ..... MnA I unc I<: """' Instrument source check Is within llmlts. Instrument blm ch..,.k Is within limits. ,/ Method RDL/ LLD has been met. y If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 1000/o or less, If greater 5* MDA/ MDC, then RPD 200/o or less, If below the MDA/ MDC, the RPO is 0%, / Or meets the client's reaulred RER acceatance criteria. Tracer yield Is 15-125%. Carrier yleld 25-1250/o. v (Or meets the client's contract acceptance criteria), Method blank Is less than the RDL/ LLD. v'-jlJ\1 \11.o lfTf <! CDI-nf Samale was run within hold time. v 1 iu Samnle was carrectlv oreserved If reaulred. t\}C\ Smears Taken for Radioactive batches. IU'J-Method Spike and LCS are within 75-1250/o v ( nr meets the "lient's rnn*r".+ criteria\. No blank soaces on data forms. All line outs Initialed and dated. v Nn <>rrnrc 2ra Aux data Is correct. '1-Y>--Client Saeclal reauirements oaae has been checked. / Raw Data and I or snectrum are Included and nronerlv statused. / MS. LCS, and Duollcate RPD/RER values uoloaded to UMS and / fu,.hlPC vnrl<la..I 1 .. 1.-rnmnlete (if kir ID-*rk ln*n / Batch Data Exceotlon Reoorts COERl comoleted If aoollcable. v' lcl}O Batch Data Exception Reports (DER) second reviewed. v l"f{lo3LID Dlsoosltlon verified to be comoleted. Alinuot rnrr..,,tlon cnmnf,,ted If rl!auired. A"'/..'"::. Review sample historical results If available ../ (If REMP, results above MDC have been verified bv historical results. recount or re-analvsls. \ Primary Review Performed By:. __ ___ [.O_j _I _}_I\..-______ _ Secondary Review Performed By:__ 10/02/16 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 01-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER HASL-300, Th-01-RC Solid Batch ID: Sample Numbers: 1596388 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and, Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203621689 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 01-0CT-16 Jessica Davis 02-0CT-16 Page 1 Page 595 of 5809 DER Report No.: 1563610 Revision No.: 2 Type: Process Client Code: MJWC Thorium (Ac-227 Tracer) Queue Sheet 07-SEP-16 Batch#: 1596388 Analyst: JXH2 First Client Due Date:04-0CT-16 Internal Due Date30-SEP-16 Tracer Tracer Code: & 1-B* 1-/oz. Exi)iration Date: 5-3i-l/ Vol: O,\,..,L Ac-227 Separation Date/Time: <f-Z 7-l(o i b 15 LCS LCS Code: \"Z. 4. 'Z.-1-J Expiration Date: 2.-1{-17 Vol: O,\.,.,L Spike Isotope: Th-230, Th-23'.Epike Code:______ Expiration Date: Vol:-==-._ PrepDate: '\-'2.6-\1...> -Initials: PipetID:\&'\OO'Z..1: BalancelD: \1..\011.ot.,*z._ Sample ID 405235001-l 405235002-1 405235003-1 40!>"235004-1 405235005-1 405235006-1 405235007-1 405235008-1 405235009-1 405235010-1 405235011-1 405235012-1 405"'..35013-1 405235014-1 405235015-1 405"'..35016-1 405235017-1 405235018-1 405235019-1 405235020-1 U03621688-1 1203621689-1 1203621690-1 Oient Description 4.1.B.R.l.2 4.1.B.R.1.3 4.1.B.R.1.4 4.1.B.R. 7.2 4.1.C.R.1.3 4.1.C.R.lA 4.1.C.R.2.3 4.1.CR.2.4 4.1.D.R.l.3 4.1.D.R.lA 4.1.D.R.3.2 4.1.D.R.2.4 4.2AJU.3 4.2A.IU.3 4.2A.R.l.4 4.1.A.R.2.4 4.1.A.R.3.2 4.2A.R.4.2 4.2B.R.2A 4.2B.R.1.4 l\IB for batch 1596388 4.t.B.R.1.zc4os:i._;soomUP> LCS for batch 1596388 Type SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAJ\.IPLE SAJ\IPLE SA..l'dPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SA?.IPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE l\IB DUP LCS Hazard Min Code CRDL 1 pC"i/g lpCi/g lpCi/g lpCUg 1 pC"i/g lpCi/g 1 pC"i/g 1 pCi/g lpCi/g lpCi/g 1 pCi/g 1 pCi/g 1 pCi/g l pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pC"i/g 1 pCi/g I pCi/g l pCi/g l pCi/g 1 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Client MJWCOOl .MJWCOOl MJWCOOl J'l.fJWCOOl MJWCOOl 1\-IJWCOOl l\-1JWC001 MJWCOOl }.fJWCOOl MJWCOOl MJWCOOl :MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl l\-1JWC001 MJWCOOl l'vfJWCOOl QCACCOW;T QC ACCOUNT QC ACCOUNT Collection Date 10-DEC-15 10-DEC-15 lO-DEC-15 09-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 OS-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 02-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 10-DEC-15 Label Aliquot Th @110 Det# Pos. 1 \ o, to ':;19"' I'"]!'? 2 2-41 3 3 i '" I £>3 J Lj.'2. 4 L\ i O*ll>i j lU(ti 5 5 i O* iC 0 tU.c 6 (c !o i0'-1 1 7 i o. 100 no 8 8 10.iol _ 9 C\ I "* ioz. i nv i 10 \v \ o -iot.. ! 1'"11 11 \\ lc-ioi:;. !' i 12 !-; 13 tB') 14 '"' <f ;;x>-::r 1s \::. 1S'5' 16 lb l 1£${i, 17 \ "1 L 81 18 \g ! 0. I 05 t SS 19 \<\ 1 a .\&l\ r£>q i 20 ! 1..-c i !!* l 0" l., ..;-1 21 ! 7.\ 22 ! -z£.. lO* 161 1'17 . 23 1 7.) !o.\Cf\ ( c;q Choose SOP Used: GL-RAD-A-03v GL-RAD-A-032 Solid Sample Dissolution by: LEACH Data Reviewed _ __.J..l_\o_\_, l_1t.P __ _ Circle One 'Tl-Pr 1 ;:; J ) /lo GEL laboratories LLC, Radiochemistry Division Page 1 oil BATCH NUMBER : 1596388 SAMPLE ID : S0405235001 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 92.3 +/-10.004 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER . ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2316E+OO dpm 2.9827E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5850.01 5857.42 TH-228 5363.00 5401.87 TH-229 4900.00 4924.02 TH-230 4671.39 4663.01 TH-232 3972.00 3991.89 7 TH*232:3796-4065keV TH-230: 4495-4745 keV TH-229: 4775-5142 keV 6 TH-226: 5211*5493 keV AC-227:551o.6128keV 5 Ui 4 I-z 3 => 0 s 2 *::; t5 <I: 2375 2774 3177 3583 Energy (keV) PEAK FWHM 343.769 34.687 163.522 12.388 7.433 COUNT DATE : 01-0ct-201612:54:07 ELAPSED LIVE TIME(SEC) : 8333.38 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 111.000 110.167 0.833 0.9129 100.000 1.56E+01 14.000 12.940 0.278 0.5270 99.940 2.13E+OO 3.000 2.444 0.556 0.7454 99.469 3.01E-01 12.000 11.861 0.139 0.3727 99.700 1.46E+OO 8.000 7.861 0.139 0.3727 100.000 9.62E-01 ]] l :;l:2 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B177.CNF;879 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 4.29E+OO 1.33E+OO 4.92E-01 9.16E-01 7.46E-01 NOTES: MDA pCi/G 8.78E-01 1.06E+OO 6.91E-01 5.29E-01 5.27E-01 Le pCi/G 2.27E-01 2.83E-01 1.61E-01 8.03E-02 8.00E-02 1.96-sigma cnt Unc pCi/G 2.94E+OO 1.25E+OO 4.88E-01 8.68E-01 7.21E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7763E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.783 +/-0.005)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235002 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 041 DETECTOR S/N : 78205 AVERAGE %EFFICIENCY : 34.0563 AVERAGE %EFF ERROR : 0.6560 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.7 +/-5.490 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER 0387-B-402 AC-227 ID NUCLIDE NOMINAL RESULTS 3.1311 E+OO dpm 2.8415E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.08 5894.24 TH-228 5363.00 5404.46 TH-229 4900.00 4947.48 TH-230 4671.39 4668.19 TH-232 3972.00 4013.75 TH-232: 37964085 keV 17 TH-+230: 4495-4745 keV TH-229: 4nS.S142 keV TH-228: 5211-5493 keV 15 AC-227: 5510-6126 keV 13 11 Ui 9 I-z :J 7 0 s 5 *:; 3 t5 <i: 2407 Energy (keV) PEAK FWHM 339.495 21.055 303.587 5.386 29.869 COUNT DATE : 28-Sep-2016 14:05:07 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 520.000 488.690 31.310 5.5955 100.000 1.39E+01 57.000 51.819 4.040 2.0100 99.940 1.89E+OO 8.000 6.485 1.515 1.2309 99.469 1.78E-01 37.000 35.485 1.515 1.2309 99.700 9.69E-01 45.000 45.000 0.000 0.0000 100.000 1.23E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B041.CNF;1825 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W041.CNF;531 CAL DATE : 28-Sep-2016 1.96-sigma TPU pCi/G 2.05E+OO 5.98E-01 1.71E-01 3.53E-01 3.90E-01 NOTES: MDA pCi/G 7.25E-01 4.32E-01 2.18E-01 2.18E-01 8.17E-02 Le pCi/G 3.20E-01 1.61E-01 6.80E-02 6.78E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.29E+OO 5.55E-01 1.70E-01 3.34E-01 3.63E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8403E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.141 +/-0.007)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235003 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 042 DETECTOR S/N : 78793 AVERAGE %EFFICIENCY : 33.4532 AVERAGE %EFF ERROR : 0.6446 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 84.8 +/-5.661 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1311E+OOdpm 2.6562E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.08 5886.73 TH-228 5363.00 5416.11 TH-229 4900.00 5055.16 TH-230 4671.39 4667.87 TH-232 3972.00 4008.06 19 TH-232:3796-4085keV TH*230: 4495-4745 keV 17 TH-229: 4775-5142 keV TH-2Z8:5211-5493keV AC-227:551o-6128keV 15 13 (ii 11 1--9 z => 0 7 s 5 .?;-3 0 <( 2382 2779 3180 3585 Energy (keV) PEAK FWHM 312.011 31.823 157.676 19.710 44.962 COUNT DATE : 28-Sep-2016 14:05:07 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 476.000 448.730 27.270 5.2221 100.000 1.43E+01 41 .. 000 36.922 3.030 1.7407 99.940 1.51E+OO 4.000 2.485 1.515 1.2309 99.469 7.62E-02 29.000 23.950 5.050 2.2472 99.700 7.33E-01 42.000 40.990 1.010 1.0050 100.000 1.25E+OO ]] Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B042.CNF;1823 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W042.CNF;492 CAL DATE : 28-Sep-2016 1.96-sigma TPU pCi/G 2.18E+OO 5.61E-01 1.48E-01 3.54E-01 4.23E-01 NOTES: MDA pCi/G 7.65E-01 4.41E-01 2.44E-01 3.69E-01 2.15E-01 Le pCi/G 3.35E-01 1.59E-01 7.62E-02 1.39E-01 6.19E-02 1.96-sigma cnt Unc pCi/G 1.38E+OO 5.30E-01 1.48E-01 3.44E-01 3.96E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8403E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.048 +/-0.007)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235004 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 73.8 +/-6.350 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.3116E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.07 5913.54 TH-228 5363.00 5417.20 TH-229 4900.00 4905.03 TH-230 4671.39 4679.84 TH-232 3972.00 4008.43 14 TH-232:3796-4085keV TH-230;4495-4745keV 13 TH-229: 4775-5142 keV 12 TH-228:5211-5493keV AC-227:5510-6128keV 11 10 9 en 8 I-7 z 6 ::::> 0 5 f2. 4 a 3 *:;; u 2 <{ 1 2383 Energy (keV) PEAK FWHM 322.649 18.780 163.447 14.240 9.906 § F COUNT DATE : 28-Sep-2016 14:06:35 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 314.000 311.475 2.525 1.5890 100.000 1.45E+01 28.000 23.737 3.535 1.8802 99.940 1.43E+OO 5.000 4.495 0.505 0.7106 99.469 2.03E-01 26.000 25.495 0.505 0.7106 99.700 1.15E+OO 18.000 17.495 0.505 0.7106 100.000 7.84E-01 >> .:.: Ii Ii ;E ;E <l < Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B166.CNF;891 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.51E+OO 6.84E-01 2.27E-01 4.86E-01 4.02E-01 NOTES: MDA pCi/G 4.39E-01 6.67E-01 2.65E-01 2.64E-01 2.63E-01 Le pCi/G 1.50E-01 2.43E-01 6.46E-02 6.45E-02 6.43E-02 1.96-sigma cnt Unc pCi/G 1.63E+OO 6.56E-01 2.25E-01 4.62E-01 3.88E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8420E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.728 +/-0.005)

AlphaSpectroscopySoflwateVersion3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596388 SAMPLE ID : S0405235005 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 167 DETECTOR S/N : 72546 AVERAGE %EFFICIENCY : 24.1606 AVERAGE %EFF ERROR : 0.4690 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 75.5 +/-6.598 % AC-227 SEP. : 27-Sep-201616:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.3641 E+OO dpm NUCLIDE LIBRARY ENERGY AC-227 5871.07 TH-228 5363.00 TH-229 4900.00 TH-230 4671.39 TH-232 3972.00 14 13 TH-229: 4775-5142 keV 12 11 10 g 8 7 6 5 4 3 2 1 TH-228: 5211-5493 keV AC.227: 5510-6128 keV 2378 2780 Energy (keV) PEAK ENERGY 5898.71 5406.99 5010.58 4676.17 4019.25 PEAK FWHM 345.926 147.540 165.044 133.786 26.257 COUNT DATE : 28-Sep-2016 14:06:38 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 294.000 288.445 5.555 2.3569 100.000 1.39E+01 24.000 23.326 0.000 0.0000 99.940 1.44E+OO 4.000 3.495 0.505 0.7106 99.469 1.62E-01 29.000 25.970 3.030 1.7407 99.700 1.20E+OO 20.000 18.485 1.515 1.2309 100.000 8.53E-01 '.i Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B167.CNF;886 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W167.CNF;246 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.49E+OO 6.41E-01 2.15E-01 5.37E-01 4.40E-01 NOTES: MDA pCi/G 6.01E-01 3.52E-01 2.72E-01 4.64E-01 3.68E-01 Le pCi/G 2.28E-01 8.35E-02 6.65E-02 1.63E-01 1.15E-01 1.96-sigma cnt Unc pCi/G 1.63E+OO 6.09E-01 2.13E-01 5.11E-01 4.24E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8420E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.674 +/-0.004)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235006 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 95.6 +/-5.766 % AC-227 SEP. : 27-Sep-201616:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.9933E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.07 5907.41 TH-228 5363.00 5425.24 TH-229 4900.00 4998.63 TH-230 4671.39 4702.53 TH-232 3972.00 4045.22 TH-Z32:3796-4085keV 15 TH-230; 4495-4745 keV TH-229: 4n5-5142 keV TH-228:5211*5493keV 13 AC.'22.7:551Q..6128keV 11 0' 9 z 7 =i 0 s 5 .?;> *::; 3 u <( 2402 2798 3198 3603 Energy (key) PEAK FWHM 332.721 82.153 4.929 19.717 8.626 COUNT DATE : 28-Sep-2016 14:06:41 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 399.000 396.475 2.525 1.5890 100.000 1.41E+01 43.000 41.568 0.505 0.7106 99.940 1.90E+OO 4.000 1.980 2.020 1.4213 99.469 6.81E-02 28.000 26.485 1.515 1.2309 99.700 9.09E-01 28.000 27.495 0.505 0.7106 100.000 9.41E-01 g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B169.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.20E+OO 6.44E-01 1.69E-01 3.84E-01 3.81E-01 NOTES: MDA pCi/G 3.35E-01 3.33E-01 3.00E-01 2.73E-01 2.01E-01 Le pCi/G 1.14E-01 9.79E-02 9.86E-02 8.52E-02 4.91E-02 1.96-sigma cnt Unc pCi/G 1.40E+OO 5.99E-01 1.69E-01 3.68E-01 3.64E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8421 E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.927 +/-0.006)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235007 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLEQTY: 0.100G -+/-1.000% CHAMBER : 170 DETECTOR S/N : 72549 AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 103 +/-5.661 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 3.2395E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.07 5919.97 TH-228 5363.00 5411.40 TH-229 4900.00 5064.64 TH-230 4671.39 4665.84 TH-232 3972.00 4000.72 15 TH-232: 37964085 keV TH-230: 4495-4745 keV TH-229: 4nS-5142 keV 13 TH-228: 5211-5493 keV AC.227:551o.6128keV 11 Ci) 9 I-7 z ;::) 0 5 -2:-3 *;;; ti 2386 Energy (keV) PEAK FWHM 327.042 25.602 39.641 86.716 69.373 COUNT DATE : 28-Sep-2016 14:06:43 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 427.000 420.940 6.060 2.4617 100.000 1.47E+01 34.000 26.451 6.565 2.5622 99.940 1.19E+OO 2.000 0.485 1.515 1.2309 99.469 1.63E-02 24.000 23.495 0.505 0.7106 99.700 7.90E-01 18.000 16.990 1.010 1.0050 100.000 5.69E-01 <l < Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B170.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.25E+OO 5.66E-01 1.32E-01 3.46E-01 3.00E-01 NOTES: MDA pCi/G 4.51E-01 6.21E-01 2.68E-01 1.97E-01 2.36E-01 Le pCi/G 1.73E-01 2.43E-01 8.37E-02 4.82E-02 6.80E-02 1.96-sigma cnt Unc pCi/G 1.42E+OO 5.46E-01 1.32E-01 3.33E-01 2.92E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227Tracernominal includes 1.8421E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.984 +/-0.006)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235008 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 1 O-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 86.4 +/-6.000 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.7057E+OO dpm NUCLIDE LIBRARY PEAK (ii 1--z ::J 0 a *:;; t5 <i: ENERGY ENERGY AC-227 5871.07 5907.95 TH-228 5363.00 5402.25 TH-229 4900.00 4918.44 TH-230 4671.39 4685.78 TH-232 3972.00 4014.23 17 TH-232:3796-4085kaV TH-230: 4495-4745 keV TH-229: 4TI5-5142 keV 15 TH-228: 5211-5493 keV AC-227:551G-6128keV 13 11 9 7 5 3 2363 2764 3168 3575 Energy {keV) PEAK FWHM 328.324 20.345 298.948 17.439 23.252 COUNT DATE : 28-Sep-2016 14:06:45 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 362.000 358.970 3.030 1.7407 100.000 1.45E+01 34.000 33.161 0.000 0.0000 99.940 1.73E+OO 3.000 1.990 1.010 1.0050 99.469 7.78E-02 28.000 27.495 0.505 0.7106 99.700 1.07E+OO 23.000 23.000 0.000 0.0000 100.000 8.95E-01 7400 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B175.CNF;870 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.37E+OO 6.46E-01 1.68E-01 4.37E-01 3.92E-01 NOTES: MDA pCi/G 4.06E-01 3.13E-01 2.76E-01 2.29E-01 1.17E-01 Le pCi/G 1.42E-01 7.85E-02 7.93E-02 5.60E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.52E+OO 6.06E-01 1.67E-01 4.15E-01 3.76E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8422E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0 .839 +/-0 .005)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235009 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 176 DETECTOR S/N : 74434 AVERAGE %EFFICIENCY : 25.6995 AVERAGE %EFF ERROR : 0.4981 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 92.1 +/-5.905 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.8853E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5913.30 TH-228 5363.00 5415.73 TH-229 4900.00 4972.81 TH-230 4671.39 4681.45 TH-232 3972.00 4011.64 TH-232: 37964085 keV 17 TH-230: 44954745 keV TH-229: 4n5-5142 keV TH-228: 5211-5493 keV 15 AC-227:5510-012BkeV 13 11 Ui 9 I-z :::i 7 0 5 c *:;; 3 u <( 2379 2776 3177 3582 Energy (keV) PEAK FWHM 297.495 10.486 187.521 9.870 64.974 399 COUNT DATE : 28-Sep-2016 14:06:48 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 378.000 374.465 3.535 1.8802 100.000 1.44E+01 21.000 19.619 0.505 0.7106 99.940 9.70E-01 3.000 1.485 1.515 1.2309 99.469 5.51E-02 24.000 20.465 3.535 1.8802 99.700 7.58E-01 36.000 34.990 1.010 1.0050 100.000 1.29E+OO >> > > .ll Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B176.CNF;865 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.31E+OO 4.77E-01 1.63E-01 3.89E-01 4.72E-01 NOTES: MDA pCi/G 4.07E-01 3.56E-01 2.96E-01 3.92E-01 2.61E-01 Le pCi/G 1.46E-01 1.04E-01 9.22E-02 1.41E-01 7.49E-02 1.96-sigma cnt Unc pCi/G 1.47E+OO 4.60E-01 1.63E-01 3.77E-01 4.45E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8422E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.876 +/-0.006)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235010 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 179 DETECTOR S/N : 74437 AVERAGE %EFFICIENCY : 26.3751 AVERAGE %EFF ERROR : 0.5108 SAMPLE DATE : 1 O-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 110 +/-9.356 % AC-227 SEP. : 27-Sep-201616:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2316E+OO dpm 3.5405E+OO dpm NUCLIDE LIBRARY PEAK "(j) I-z :::> 0 *s: u <t: ENERGY ENERGY AC-227 5850.01 5868.28 TH-228 5363.00 5434.46 TH-229 4900.00 4958.09 TH-230 4671.39 4630.17 TH-232 3972.00 4007.84 8 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 7 TH-228:5211-5493keV AC-.227:5510-0128keV 6 5 4 3 2 2377 2775 3176 3582 Energy (keV) PEAK FWHM 292.338 13.588 0.000 187.755 54.350 COUNT DATE : 01-0ct-201612:54:09 ELAPSED LIVE TIME(SEC) : 8238.20 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 130.000 128.215 1.785 1.3360 100.000 1.65E+01 12.000 10.540 0.549 0.7411 99.940 1.58E+OO 0.000 -0.275 0.275 0.5240 99.469 -3.07E-02 6.000 5.863 0.137 0.3705 99.700 6.55E-01 4.000 3.863 0.137 0.3705 100.000 4.30E-01 !! Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B179.CNF;879 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W179.CNF;254 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.24E+OO 9.89E-01 3.02E-01 1.11E+OO 1.06E+OO 3.05E-01 2.26E-01 5.41E-01 1.03E-01 5.93E-01 4.80E-01 7.26E-02 4.96E-01 4.79E-01 7.24E-02 NOTES: 1.96-sigma cnt Unc pCi/G 2.89E+OO 1.06E+OO 2.25E-01 5.80E-01 4.90E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7757E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.911 +/-0.006)

AlphaSpectroscopySof!wareVersJonJ.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596388 SAMPLE ID : S0405235011 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 179 DETECTOR S/N : 74437 AVERAGE %EFFICIENCY : 26.3751 AVERAGE %EFF ERROR : 0.5108 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 76.0 +/-6.310 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS . 0387-B-402 AC-227 3.1312E+OO dpm 2.3798E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5890.11 TH-228 5363.00 5418.02 TH-229 4900.00 5041.20 TH-230 4671.39 4664.15 TH-232 3972.00 4010.82 19 TH*232:3796-4085keV TH-230; 4495-4745 keV 17 TH-229:4nS.5142keV TH-226:5211*5493keV AC.227:551CHl128keV 15 13 (ii 11 I-9 z => 0 7 8 5 a *:;; 3 u <i:: 1 2377 2775 3176 3582 Energy (keV) PEAK FWHM 274.280 27.999 4.941 29.646 7.411 > ! . ; COUNT DATE : 28-Sep-2016 14:06:53 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 320.000 316.970 3.030 1.7407 100.000 1.39E+01 33.000 30.744 1.515 1.2309 99.940 1.73E+OO 1.000 0.495 0.505 0.7106 99.469 2.09E-02 40.000 39.495 0.505 0.7106 99.700 1.66E+OO 26.000 25.495 0.505 0.7106 100.000 1.07E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B179.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W179.CNF;254 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.38E+OO 6.93E-01 1.31E-01 5.74E-01 4.54E-01 NOTES: MDA pCi/G 4.38E-01 4.91E-01 2.48E-01 2.47E-01 2.46E-01 Le pCi/G 1.54E-01 1.61E-01 6.05E-02 6.04E-02 6.02E-02 1.96-sigma cnt Unc pCi/G 1.54E+OO 6.53E-01 1.31E-01 5.32E-01 4.32E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8423E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.741 +/-0.005)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235012 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 205 DETECTOR S/N : 78908 AVERAGE %EFFICIENCY : 26.6171 AVERAGE %EFF ERROR : 0.5154 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 101 +/-9.584 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2316E+OO dpm 3.2504E+OO dpm NUCLIDE LIBRARY PEAK '(j) I-z ::J 0 8 .?;> *:;;: :g <i: ENERGY ENERGY AC-227 5850.01 5865.48 TH-228 5363.00 5409.62 TH-229 4900.00 4958.12 TH-230 4671.39 4660.70 TH-232 3972.00 4017.72 6 TH-232: 3795-4085 keV TH-230:4495-4745keV TH-229:4775-5142keV TH-228:5211-5493keV 5 AC-227:5510-6128kaV 4 3 2 2378 2775 3177 3582 Energy (keV) PEAK FWHM 303.314 7.418 0.000 61.817 7.418 COUNT DATE : 01-0ct-201612:54:11 ELAPSED LIVE TIME(SEC) : 8352.94 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 121.000 120.443 0.557 0.7462 100.000 1.54E+01 9.000 7.866 0.278 0.5277 99.940 1.17E+OO 0.000 -0.278 0.278 0.5277 99.469 -3.10E-02 11.000 10.722 0.278 0.5277 99.700 1.19E+OO 8.000 8.000 0.000 0.0000 100.000 8.87E-01 ]! > > .. .. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B205.CNF;805 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W205.CNF;223 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.07E+OO 9.59E-01 2.26E-01 7.91E-01 6.75E-01 NOTES: MDA pCi/G 7.20E-01 9.77E-01 5.41E-01 5.40E-01 3.33E-01 Le pCi/G 1.68E-01 2.65E-01 1.03E-01 1.03E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.78E+OO 9.26E-01 2.25E-01 7.57E-01 6.53E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7765E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrow1h from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrow1h from tracer. (0.856 +/-0.006)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235013 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.2 +/-10.360 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE AC-227 TH-228 TH-229 TH-230 TH-232 0387-B-402 AC-227 3.2316E+OO dpm 2.9137E+OO dpm LIBRARY PEAK ENERGY ENERGY 5850.01 5885.18 5363.00 5412.38 4900.00 4958.08 4671.39 4679.86 3972.00 4041.13 TH-229: 4nS.5142 keV TH-228: 5211-5493 keV AC-227:5510--012BkeV 4 3 2 2416 2810 3209 3612 Energy (keV) PEAK FWHM 343.034 80.954 b.000 4.906 29.438 COUNT DATE : 01-0ct-2016 12:54:14 ELAPSED LIVE TIME(SEC) : 8328.62 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 104.000 102.751 1.249 1.1177 100.000 1.60E+01 13.000 12.270 0.000 0.0000 99.940 2.23E+OO 0.000 -0.139 0.139 0.3726 99.469 -1.88E-02 5.000 4.861 0.139 0.3726 99.700 6.58E-01 9.000 8.861 0.139 0.3726 100.000 1.20E+OO 7429 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B189.CNF;857 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.57E+OO 1.42E+OO 2.72E-01 6.66E-01 8.74E-01 NOTES: MDA pCi/G 1.08E+OO 1.06E+OO 5.84E-01 5.83E-01 5.81E-01 Le pCi/G 3.06E-01 2.55E-01 8.87E-02 8.85E-02 8.82E-02 1.96-sigma cnt Unc pCi/G 3.14E+OO 1.33E+OO 2.71E-01 6.52E-01 8.38E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7764E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.730 +/-0.005)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235014 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 207 DETECTOR S/N : 78910 AVERAGE %EFFICIENCY : 26.0138 AVERAGE %EFF ERROR : 0.5040 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 72.6 +/-11.325 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER , ID NUCLIDE NOMINAL RESULTS NUCLIDE AC-227 TH-228 TH-229 TH-230 TH-232 0387-B-402 AC-227 3.2316E+OO dpm 2.3449E+OO dpm LIBRARY PEAK ENERGY ENERGY 5850.01 5872.06 5363.00 5428.98 4900.00 4958.12 4671.39 4692.81 3972.00 4001.85 TH-229; 4nS-S142 keV TH-228: 5211-5493 keV AC-227: 5510-6128 keV 4 3 2 2375 2773 3175 3582 Energy (keV) PEAK FWHM 78.023 29.723 0.000 7.431 54.492 COUNT DATE : 01-0ct-201612:54:17 ELAPSED LIVE TIME(SEC) : 8363.20 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 86.000 85.024 0.976 0.9878 100.000 1.60E+01 10.000 8.838 0.558 0.7467 99.940 1.94E+OO 0.000 -0.558 0.558 0.7467 99.469 -9.14E-02 9.000 8.861 0.139 0.3733 99.700 1.45E+OO 2.000 2.000 0.000 0.0000 100.000 3.26E-01 ]] > 6533 6970 7412 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B207.CNF;813 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W207.CNF;228 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 5.00E+OO 1.51E+OO 3.39E-01 1.07E+OO 5.60E-01 NOTES: MDA pCi/G 1.22E+OO 1.46E+OO 9.22E-01 7.05E-01 4.89E-01 Le pCi/G 3.27E-01 4.02E-01 2.15E-01 1.07E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.45E+OO 1.43E+OO 3.37E-01 1.02E+OO 5.55E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7767E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.604 0 ....., Ul 00 0 '° BATCH NUMBER : 1596388 SAMPLE ID : S0405235015 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 185 DETECTOR S/N : 68615 AVERAGE %EFFICIENCY : 25.3535 AVERAGE %EFF ERROR*: 0.4915 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 88.5 +/-6.068 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-8-402 AC-227 3.1312E+OO dpm 2.7721E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5895.90 TH-228 5363.00 5421.20 TH-229 4900.00 4870.94 TH-230 4671.39 4697.40 TH-232 3972.00 4029.64 15 TH-2J2:3796-4085keV TH-230: 4495-4745 keV TH-+229: 4775-5142 keV 13 TH-228:5211-5493keV AC-227:5510.U128keV 11 'Cii 9 I-7 z :::> 0 5 .?;-3 *:;: :g <x: 2380 2781 Energy (keV) PEAK FWHM 330.760 106.053 4.991 9.981 7.985 COUNT DATE : 28-Sep-2016 14:07:01 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 362.000 354.930 7.070 2.6589 100.000 1.41E+01 28.000 25.655 1.515 1.2309 99.940 1.32E+OO 6.000 3.980 2.020 1.4213 99.469 1.53E-01 17.000 13.465 3.535 1.8802 99.700 5.16E-01 26.000 25.495 0.505 0.7106 100.000 9.74E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B185.CNF;859 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W185.CNF;237 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.33E+OO 5.77E-01 2.17E-01 3.43E-01 4.12E-01 NOTES: MDA pCi/G 5.46E-01 4.51E-01 3.36E-01 4.06E-01 2.24E-01 Le pCi/G 2.13E-01 1.49E-01 1.10E-01 1.45E-01 5.48E-02 1.96-sigma cnt Unc pCi/G 1.49E+OO 5.51E-01 2.17E-01 3.36E-01 3.93E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8425E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.830 +/-0.005)

Alpha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar*2015 BATCH NUMBER : 1596388 SAMPLE ID : S0405235016 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.107 G -+/-0.935 % CHAMBER : 186 DETECTOR SIN : 68616 AVERAGE %EFFICIENCY : 25.3981 AVERAGE %EFF ERROR : 0.4924 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 87.6 +/-6.140 % AC-227 SEP. : 27-Sep-201616:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.7435E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5928.76 TH-228 5363.00 5437.94 TH-229 4900.00 4881.50 TH-230 4671.39 4696.53 TH-232 3972.00 4027.08 TH-232:3796-4085keV 17 TH-230: 4495-4745 keV TH-229: 4775-5142 keV TH-228: 5211-5493 keV 15 AC-227:551CHi128keV 13 11 Cii 9 1--z :J 7 0 5 z. *::; 3 ti <( 2395 Energy (keV) PEAK FWHM 321.944 23.541 0.000 18.650 62.996 COUNT DATE : 28-Sep-2016 14:07:03 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 364.000 351.880 12.120 3.4814 100.000 1.37E+01 37.000 17.492 18.685 4.3226 99.940 8.79E-01 4.000 2.990 1.010 1.0050 99.469 1.13E-01 40.000 34.950 5.050 2.2472 99.700 1.31E+OO 39.000 37.485 1.515 1.2309 100.000 1.40E+OO >> g g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B186.CNF;819 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W186.CNF;28 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.29E+OO 6.91E-01 1.78E-01 5.15E-01 5.03E-01 NOTES: MDA pCi/G 6.65E-01 1.04E+OO 2.66E-01 4.54E-01 2.98E-01 Le pCi/G 2.74E-01 4.45E-01 7.64E-02 1.70E-01 9.31E-02 1.96-sigma cnt Unc pCi/G 1.47E+OO 6.81E-01 1.77E-01 4.87E-01 4.70E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8425E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.823 +/-0.005)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235017 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 187 DETECTOR S/N : 68620 AVERAGE %EFFICIENCY : 25.2519 AVERAGE %EFF ERROR : 0.4896 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 1 OD +/-5.939 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 3.1347E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5904.66 TH-228 5363.00 5425.57 TH-229 4900.00 4837.73 TH-230 4671.39 4682.12 TH-232 3972.00 4031.52 TH-23Z:3795-4085keV 17 TH-230:4495-4745keV TH-229: 4n5-S142 keV TH-228: 5211-5493 keV 15 AC-227:5510-6128keV 13 11 Ui 9 I-z ::> 7 0 s 5 .?;-*:;; 3 n <t: 2387 Energy (keV) PEAK FWHM 345.698 28.987 14.865 16.517 24.775 COUNT DATE : 28-Sep-2016 14:07:06 ELAPSED LIVE TIME(SEC) : 30300.00 GROSS AREA 426.000 37.000 9.000 44.000 23.000 NUCLIDE ACTIVITY SUMMARY NET AREA 399.740 35.055 -3.625 34.910 21.990 :; BKG AREA 26.260 1.010 12.625 9.090 1.010 BKG %ABUN StDev 5.1245 100.000 1.0050 99.940 3.5532 99.469 3.0150 99.700 1.0050 100.000 ACTIVITY pCi/G 1.40E+01 1.59E+OO -1.22E-01 1.18E+OO 7.39E-01 7416 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B187.CNF;854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W187.CNF;238 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.25E+OO 5.89E-01 2.70E-01 4.89E-01 3.40E-01 NOTES: MDA pCi/G 8.29E-01 3.70E-01 5.86E-01 5.11E-01 2.37E-01 Le pCi/G 3.62E-01 1.17E-01 2.42E-01 2.05E-01 6.82E-02 1.96-sigma cnt Unc pCi/G 1.44E+OO 5.54E-01 2.70E-01 4.66E-01 3.28E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8425E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.935 +/-0.006)

Alpha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar*2015 BATCH NUMBER : 1596388 SAMPLE ID : S0405235018 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 188 DETECTOR S/N : 68621 AVERAGE %EFFICIENCY : 26.7276 AVERAGE %EFF ERROR : 0.5175 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 78.2 +/-6.221 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS AC-227 3.1312E+OO dpm 2.4483E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5907.08 TH-228 5363.00 5425.71 TH-229 4900.00 4987.89 TH-230 4671.39 4688.41 TH-232 3972.00 4043.84 14 TH*232: 37964085 keV TH-230: 44954745 keV 13 TH-229: 4775-5142 keV 12 TH-228: 5211-5493 keV AC.227: 551o.6128 keV 11 10 9 Ui 8 1--7 z 6 => 0 5 8 4 3 *:;; u 2 <( 1 2429 2820 3215 3615 Energy (keV) PEAK FWHM 304.601 12.962 311.082 71.695 57.113 > COUNT DATE : 28-Sep-2016 14:07:08 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 335.000 330.455 4.545 2.1319 100.000 1.40E+01 24.000 22.217 1.010 1.0050 99.940 1.22E+OO 4.000 3.495 0.505 0.7106 99.469 1.43E-01 22.000 17.960 4.040 2.0100 99.700 7.32E-01 17.000 16.495 0.505 0.7106 100.000 6.71E-01 !! g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B188.CNF;854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W188.CNF;233 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.36E+OO 5.70E-01 1.89E-01 4.13E-01 3.54E-01 NOTES: MDA pCi/G 4.91E-01 4.38E-01 2.40E-01 4.53E-01 2.39E-01 Le pCi/G 1.82E-01 1.37E-01 5.86E-02 1.65E-01 5.83E-02 1.96-sigma cnt Unc pCi/G 1.53E+OO 5.46E-01 1.88E-01 4.02E-01 3.43E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8426E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.773 +/-0.005)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235019 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 112 +/-5.513 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 3.4916E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5921.13 TH-228 5363.00 5438.08 TH-229 4900.00 5056.02 TH-230 4671.39 4686.22 TH-232 3972.00 4025.70 TH-232:3796-40S5keV 15 TH-230; 4495-4745 keV TH-229: 4n5-S142 keV TH-228: 5211-5493 keV 13 AC-227;5510-6128keV 11 Ui 9 I-z 7 :J 0 S?, 5 *s; 3 u <( 2416 Energy (keV) PEAK FWHM 325.044 115.299 122.658 87.087 25.349 COUNT DATE : 28-Sep-2016 14:07:11 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 452.000 447.960 4.040 2.0100 100.000 1.35E+01 34.000 31.437 1.515 1.2309 99.940 1.22E+OO 2.000 0.990 1.010 1.0050 99.469 2.88E-02 18.000 15.980 2.020 1.4213 99.700 4.63E-01 24.000 23.495 0.505 0.7106 100.000 6.79E-01 > > g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B189.CNF;855 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.01E+OO 4.79E-01 1.11E-01 2.61E-01 2.97E-01 NOTES: MDA pCl/G 3.34E-01 3.49E-01 2.05E-01 2.53E-01 1.70E-01 Le pCi/G 1.22E-01 1.16E-01 5.89E-02 8.31E-02 4.14E-02 1.96-sigma cnt Unc pCi/G 1.26E+OO 4.56E-01 1.10E-01 2.56E-01 2.86E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8426E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.048 +/-0.007)

BATCH NUMBER : 1596388 SAMPLE ID : S0405235020 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 195 DETECTOR S/N : 78786 AVERAGE %EFFICIENCY : 26.3844 AVERAGE %EFF ERROR : 0.5110 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 94.8 +/-5.771 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.9681 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5916.79 TH-228 5363.00 5409.27 TH-229 4900.00 4888.43 TH-230 4671.39 4694.96 TH-232 3972.00 4025.45 TH+232:3796-4065't<<N 23 TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 21 TH-228:5211*5493keV AC-227: 5510-6128 keV 19 17 15 (jJ 13 I-z 11 :::l 9 0 !:2. 7 .;::-5 *::; u 3 <t: 1 2393 Energy (keV) PEAK FWHM 53.080 15.709 4.961 44.646 52.088 COUNT DATE : 28-Sep-2016 14:07:13 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 398.000 395.475 2.525 1.5890 100.000 1.39E+01 26.000 24.570 0.505 0.7106 99.940 1.11E+OO 5.000 3.990 1.010 1.0050 99.469 1.35E-01 29.000 27.485 1.515 1.2309 99.700 9.28E-01 20.000 20.000 0.000 0.0000 100.000 6.73E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B195.CNF;880 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W195.CNF;259 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.16E+OO 4.85E-01 1.73E-01 3.85E-01 3.15E-01 NOTES: MDA pCi/G 3.30E-01 3.28E-01 2.39E-01 2.69E-01 1.01E-01 Le pCi/G 1.12E-01 9.64E-02 6.86E-02 8.38E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.37E+OO 4.64E-01 1.72E-01 3.68E-01 3.04E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8427E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.925 +/-0.006)

BATCH NUMBER : 1596388 SAMPLE ID : S1203621688 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 038 DETECTOR S/N : 72532 AVERAGE %EFFICIENCY : 36.0700 AVERAGE %EFF ERROR : 0.6941 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 82.6 +/-5.544 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1311E+00dpm 2.5870E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.08 5905.18 TH-228 5363.00 5384.47 TH-229 4900.00 4903.00 TH-230 4671.39 4619.86 TH-232 3972.00 3911.38 TH*232: 3796-4085 keV 19 TH-230; 44954745 keV TH-229: 4n5-5142 keV 17 TH-22B:S211-5493keV AC-227:5510-6128keV 15 13 en 11 I-z 9 ::i 0 7 .?;> 5 *s: 3 :g <{ 2407 2802 3202 3607 Energy (keV) PEAK FWHM 284.762 132.562 68.736 0.000 98.194 COUNT DATE : 28-Sep-2016 14:05:07 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 498.000 471.235 26.765 5.1735 100.000 1.35E+01 6.000 2.879 2.020 1.4213 99.940 7.93E-02 3.000 2.495 0.505 0.7106 99.469 6.89E-02 0.000 -0.505 0.505 0.7106 99.700 -1.39E-02 2.000 1.495 0.505 0.7106 100.000 4.11E-02 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B038.CNF;1826 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W038.CNF;501 CAL DATE : 28-Sep-2016 1.96-sigma TPU pCi/G 2.02E+OO 1.56E-01 1.15E-01 6.64E-02 1.01E-01 NOTES: MDA pCl/G 6.83E-01 2.67E-01 1.62E-01 1.62E-01 1.61E-01 Le pCi/G 2.98E-01 9.22E-02 3.96E-02 3.95E-02 3.94E-02 1.96-sigma en! Une pCl/G 1.27E+OO 1.55E-01 1.15E-01 6.63E-02 1.01E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8403E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.101 +/-0.007)

BATCH NUMBER : 1596388 SAMPLE ID : S1203621689 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 197 DETECTOR S/N : 78894 AVERAGE %EFFICIENCY : 26.0674 AVERAGE %EFF ERROR : 0.5050 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 93.7 +/-5.954 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.9347E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5815.81 TH-228 5363.00 5348.69 TH-229 4900.00 4996.37 TH-230 4671.39 4603.98 TH-232 3972.00 3958.62 TH-232:3796-4085keV 15 TH-230: 4495-4745 keV TH-229: 4n5-5142 keV TH-228: 5211-5493 keV 13 AC-227: 551CHl128 keV 11 en 9 1--z 7 :J 0 s. 5 .?;-*::; 3 t5 <( Energy (keV) PEAK FWHM 307.675 21.465 0.000 16.924 116.404 :: COUNT DATE : 28-Sep-2016 14:07:15 ELAPSED LIVE TIME(SEC) : 30300.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 404.000 386.325 17.675 4.2042 100.000 1.45E+01 33.000 24.017 8.080 2.8425 99.940 1.16E+OO 13.000 3.910 9.090 3.0150 99.469 1.42E-01 30.000 20.405 9.595 3.0976 99.700 7.40E-01 25.000 13.385 11.615 3.4081 100.000 4.84E-01 :: g iii ;= ;= Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B197.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W197.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.35E+OO 6.06E-01 3.10E-01 4.37E-01 4.06E-01 NOTES: MDA pCi/G 7.52E-01 7.21E-01 5.51E-01 5.62E-01 6.06E-01 Le pCi/G 3.19E-01 2.88E-01 2.21E-01 2.27E-01 2.49E-01 1.96-sigma cnt Unc pCi/G 1.50E+OO 5.88E-01 3.09E-01 4.27E-01 4.02E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8427E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.903 +/-0.006)

BATCH NUMBER : 1596388 SAMPLE ID : S1203621690 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 199 DETECTOR S/N : 78896 AVERAGE %EFFICIENCY : 26.2038 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 82.2 +/-6.156 % AC-227 SEP. : 27-Sep-2016 16:15:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.1312E+OO dpm 2.5727E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5871.06 5894.57 TH-228 5363.00 5445.02 TH-229 4900.00 5105.95 TH-230 4671.39 4674.48 TH-232 3972.00 3943.53 51 TH-232: 3796-4085 keV TH-230:4495-474SkeV TH-229: 4775-5142 keV 46 TH-228: 5211-5493 keV AC-227:5510-6128keV 41 36 0' 31 26 z :::i 21 0 8 16 0 11 0 6 <I'. 2377 2776 3178 3585 Energy {keV) PEAK FWHM 336.577 4.962 54.578 37.021 243.119 > ! COUNT DATE : 28-Sep-2016 14:07:18 ELAPSED LIVE TIME(SEC) : 30300.00 LCS ID 1242-H NUCLIDE TH-230 NOMINAL (pCi/G) 1.9202E+01 % RECOVERY 107.307 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 346.000 340.445 5.555 2.3569 100.000 1.35E+01 1.000 -0.301 0.505 0.7106 99.940 -1.15E-02 3.000 0.980 2.020 1.4213 99.469 3.74E-02 542.000 540.485 1.515 1.2309 99.700 2.06E+01 4.000 3.495 0.505 0.7106 100.000 1.33E-01 >> .:.: iii Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B199.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W199.CNF;222 CAL DATE : 15-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.25E+OO 4.95E-01 1.88E-01 1.19E-01 2.71E-01 7.83E-02 1.72E-01 3.34E-01 1.10E-01 3.16E+OO 3.04E-01 9.47E-02 1.76E-01 2.23E-01 5.45E-02 NOTES: 1.96-sigma cnt Unc pCi/G 1.45E+OO 1.18E-01 1.72E-01 1.74E+OO 1.75E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 1.8428E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.796 +/-0.005)

Effective 3(25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 02-Sep-2016 Batch# Product:, ___ f_\l ___ _ Date: Criteria: Yes No Comments Sample Solids are less than or equal to 100 mq for GAB. ()/(f\ Samples have been blank corrected (If required). (V¥\. Blank correction reoorted Included (If required). If activity less than 10x MDA/MDC, error Is less ........ than or equal to 150% of sample activity, N If qreater than 10* MDA/ MDC, error Is 40% or less. lrf'--*-w ..... **"A I Mnr orrnr [s ni.,.u ' Instrument source check Is within llmlts. "r-.. hlm rhort.. h; ... r*hln ' Method RDL/ LLD has been met. If duollcate activities are: ....... I'-.> Less than 5* MDA/ MDC, then RPD Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, If below the MDA/ MDC, the RPD Is 0%, Or meets the client's renulred RER accentance criteria. Tracer yield Is 15-125%

Carrier yield 25-1250/o. ..........._ :-..) (Or meets the contract acceptance criteria). Method blank Is less than the RDL/ LLD. lrlf <: !;O/n nf ln ... ad[vltvl -........_ i-' GL-CHL-RAD-013 Rev 1 Page 1 of 1 Samole was run within hold time. fJ{J ,(,\\,,.,,) f....:> l)6M l c;srq u. q '\\ fY>I-\ Sama le was correctlv areserved if reaulred. Smears Taken far Radioactive batches. ' (\J 'f'v "1--:l Method Spike and LCS are within 75-12S% lrnr ---*-*ko criteria)_ " No blank spaces on data forms. N All line outs initialed and dated. ***------mrA I Aux data is correct. {\Iv-\ ..... Client Snecial reaulrements naae has been checked. ..... t---> Raw Data and I or soectrum are Included anti nronerlv statused. ' MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and N vmlUAS ver"'-" .... (If /\f If-\ I ..... N 11.atl:hJl"*---.t ln*n n Batch Data Excention Renorts fDERl comnleted if aonllcable. 'N /\ "Jj\ D;V\J C' 1cbs yg !./ '-\ Batch Data Exception Reports (DER) second reviewed. --..___ 1f\ {Xj\J) )':::>S l\ Disnositlon verified to be comoleted. Aliauot Correctlnn comnleted if reauired. N¥\ Review sample historical results if avallable "'-.:> (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l -Primary Review Performed By: D;iA tf /; q / ru {/ --., f\!\3W c__ Page 620 of 5809 GEL Laboratories LLC Form GEL-DER DATA EXCEPllON REPORT Mo.Day Yr. Division: Quality Criteria: 19-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER HASL-300, Pu-11-RC Solid Batch ID: Sample Numbers: 1596421 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: . Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075,405235076,405235077,405235078,and 1203621770were analyzed outside of holding. Originator's Name: Data Validator/Group Leader: Jessica Downey 19-SEP-16 Melanie Aycock 21-SEP-16 Page 1 Page 621 of 5809 DER Report No.: 1558949 Revision No.: I Type: Process Client Code: MJWC Plutonium Queue Sheet 07-SEP-16 Batch#: 1596421 Analyst: KXB2 First Client Due Date:04-0CT-16 Internal Due Date:30-SEP-16 Tracer Tracer Code: \110'/\ Expiration Date: 'b -?;-\1 Vol: 0. i Analyzed Sequentially with: LCSCode: O'l:IY(rMM Expiration Date: 1 ... 1.0-\1 Vol: O. \ U: Spike Isotope(s): Pu-239/Pu-238 Spike Code: Expiration Date: Vol:-=--Am: \'Sq\p4\C\ Prep Date: q-\'?-\\J. Initials: 'ff, PipetID: \<Qt.\001-=t:. Balance ID: \te[O'JC<.:({12.,.... CJ J/:J.1} b I ---------------Sample ID ___ C_li_e_n_t __ _ 405235061-1 405235062-1 405235063-1 405235064-1 405235065-1 405235066-1 405235067-1 405235068-1 405235069-1 405235070-1 405235071-1 405235072-1 405235073-1 40523507 4-1 405235075-1 405235076-1 405235077-1 405235078-1 1203621769-1 1203621770-1 1203621771-1 5.lB.R.2.2 5.2A.R.1.2 5.2A.R.1.3 5.2A.R.1.4 5.2A.R.2.3 5.2A.R.2.4 5.2A.R.6.2 5.2A.R.4.2 5.2B.R.1.4 5.2B.R.3.2 5.2B.R.4.2 5.2B.R.2;4 5.2B.R.8.'2 5.3A.R.1.3 5.4A.R.1.3 5.4A.R.4;2 5.SA.R.1.3 5.6A.R.l.3 r.m for batch 1596421 5.1B.R.2.2(40523506IDUP) LCS for batch 1596421 Type Hazard Code Min CRDL Matrix Client wet@ Collection Label Aliquot Pu Date Pos. # @119 Det# =========================================== SAMPLE 1 pCUg SOIL MJWCOOl 14-DEC-15 1 \ !D.S-]4 ! u5 l SAMPLE 1 pCUg SOIL MJWCOOl 14-DEC-15 2 ?_ !D-§l& [ l, !,e __ ! SAMPLE 1 pCUg SOIL r.uwcoo1 14-DEC-15 3 2 1D. i _ta_::z_ _ _i SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP LCS 1 pCUg SOIL r.DWCOOl 14-DEC-15 4 I 4 10-.-£12. ! 1.,,£, i I &" 1&-£07 ieq I I G : -zo I lpCUg 1 pCUg lpCUg lpCUg lpCUg 1 pCUg lpCUg lpCUg lpCUg 1 pCUg lpCUg 1 pCUg lpCUg lpCUg lpCUg lpCUg lpCUg SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL r.uwcoo1 r.DWCOOl r.uwcoo1 r.uwcoo1 MJWCOOl MJWCOOl r.DWCOOl MJWCOOl l\:fJWCOOl MJWCOOl r.DWCOOl r.DWCOOl r.uwcoo1 r.uwcoo1 QC ACCOUNT QC ACCOUNT QC ACCOUNT 14-DEC-15 14-DEC-15 11-DEC-15 11-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 11-DEC-15 15-DEC-15 16-DEC-15 11-DEC-15 17-DEC-15 17-DEC-15 14-DEC-15 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 I 7 rn C I ! ' \..). ;:,,<!) '* 71 i I §i I 9 ID--rD!" I 73 I I to I q ID.S-l& i 7'1 i I ( !? 1D .. ,S-C%: I So i LLLJQ__ l i I ti: I IP-, n 1U.:-s-1p I '8-'f 1 10.so.s: i I ft ID-SJ 9, 8Cb I W Jt\ sfn I' I I '},:I IO.T(8 l Ha<\ Choose SOP Solid Sample Dissolution by: LEACH Page: 1 of 1 GEL Laboratories LLC, , Radiochemistry Division BATCH NUMBER : 1596421 SAMPLE ID : S0405235061_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 065 DETECTOR S/N : 72194 AVERAGE %EFFICIENCY : 28.4758 AVERAGE %EFF ERROR : 0.5506 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 88.0 +/-6.490 % 1770-A TRACER . ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.8559E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5748.94 PU-238 5486.00 5415.55 PU-239 5155.00 5169.13 PU-242 4890.00 4909.38 PU-244 4589.00 4523.95 PU-244* 4497-4597 keV 25 r-PU-242: 4654-4995 keV PLJ.239:5011*5227keV PU-2Ja:S375-5566keV 22 f-PU-236: 5582*5843 keV 19 0' 13 -z :J 10 0 *;:;: 4 -I I I I I PEAK FWHM 4.939 0.000 44.452 39.064 4.939 I I II I 11 I 24 03 2801 3202 3607 4017 4430 COUNT DATE: 17-Sep-201611:42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.520 0.480 0.6928 100.000 9.12E-03 2.000 1.760 0.240 0.4899 99.900 2.58E-02 2.000 1.760 0.240 0.4899 99.900 2.57E-02 264.000 263.520 0.480 0.6928 100.000 3.84E+OO 1.000 1.000 0.000 0.0000 99.900 1.46E-02 l1111J II I I I I I I I I 4848 5 71 J695 6125 6559 6997 7439 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B065.CNF;2658 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W065.CNF;489 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.07E-02 9.71E-02 2.23E-02 5.09E-02 7.04E-02 1.32E-02 5.06E-02 7.00E-02 1.31E-02 6.90E-01 8.07E-02 1.85E-02 4.11E-02 4.38E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.07E-02 5.08E-02 5.05E-02 4.65E-01 4.10E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235062 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 066 DETECTOR S/N : 46-089C1 AVERAGE %EFFICIENCY : 25.6702 AVERAGE %EFF ERROR : 0.4975 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.5 +/-6.972 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6605E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5747.65 PU-238 5486.00 5453.18 PU-239 5155.00 5118.70 PU-242 4890.00 4904.86 PU-244 4589.00 4535.62 25 PU 244* 4497-4597 keV PU-242:4654-4995 keV 23 1-PU-239: 5011-5227 keV PU-238:537S.5566keV 21 1-pU-236:5582-5843keV 19 f-17 f-15 (ii 13 I-f-f-z 11 ::::i f-0 9 7 *s: 5 f-f-f-u 3 <{ f->-I I I I PEAK FWHM 30.175 5.029 0.000 50.501 5.029 I I I 23 75 2779 3188 3600 4016 Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.760 0.240 0.4899 100.000 3.60E-02 1.000 0.280 0.720 0.8485 99.900 4.79E-03 0.000 -1.200 1.200 1.0954 99.900 -2.04E-02 226.000 225.520 0.480 0.6928 100.000 3.83E+OO 1.000 0.760 0.240 0.4899 99.900 1.29E-02 "'" I II I I I I I I 485E p71E 6153 6592 7035 7482 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B066.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W066.CNF;487 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.09E-02 9.81E-02 1.84E-02 5.02E-02 1.05E-01 2.66E-02 3.88E-02 1.19E-01 3.41E-02 7.40E-01 9.41E-02 2.16E-02 4.86E-02 8.16E-02 1.53E-02 1.96-sigma cnt Unc pCi/G 7.08E-02 5.01E-02 3.87E-02 5.02E-01 4.85E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235063 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 067 DETECTOR S/N : 78780 AVERAGE %EFFICIENCY : 29.1959 AVERAGE %EFF ERROR : 0.5641 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 78.5 +/-6.767 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4400E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5522.37 PU-239 5155.00 5198.11 PU-242 4890.00 4907.93 PU-244 4589.00 4598.66 PU 244*4497-4597 keV 25 -PU-242: 46544995 keV PlJ.239: 5011-5227 keV PU-238:537S.5566keV 22 -pu.2Js:sss2-sa43keV 19 (ii 13 I-z -:::> 10 0 *;;; 4 -PEAK FWHM 0.000 4.935 4.935 48.359 0.000 -I I I Ill Ill I I I I I 23 79 2776 3177 3583 3992 440 S COUNT DATE : 17-Sep-201611:42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -2.28E-02 1.000 1.000 0.000 0.0000 99.900 1.59E-02 1.000 0.520 0.480 0.6928 99.900 8.23E-03 242.000 241.040 0.960 0.9798 100.000 3.81E+OO 1.000 1.000 0.000 0.0000 99.900 1.58E-02 lil1l I I I I I I I 4824 5 4E 672 6102 6537 6976 7419 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B067.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W067.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.33E-02 1.33E-01 3.82E-02 4.48E-02 4.78E-02 O.OOE+OO 4.58E-02 8.77E-02 2.01E-02 7.14E-01 1.04E-01 2.84E-02 4.46E-02 4.75E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.33E-02 4.48E-02 4.57E-02 4.83E-01 4.45E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235064 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.517 G -+/-0.193 % CHAMBER : 068 DETECTOR S/N : 78794 AVERAGE %EFFICIENCY : 27.7658 AVERAGE %EFF ERROR : 0.5371 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 91.0 +/-6.474 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.9887E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5497.56 PU-239 5155.00 5118.68 PU-242 4890.00 4902.87 PU-244 4589.00 4546.97 PU-244* 4497-4597 keV 28 f-PU-242: 46544995 keV PU-239:5011-5227keV 25 f-PU-23B:5375-5566keV PU-236: 5582-5843 keV 22 f-19 f-Ci) 16 f-I-z 13 :J f-0 10 £ f-7 f-*s; t5 4 f-<( PEAK FWHM 0.000 49.420 0.000 43.536 0.000 1 f-I 111 Ill I I I I I ' COUNT DATE : 17-Sep-2016 11 :42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.66E-02 3.000 2.040 0.960 0.9798 99.900 2.95E-02 0.000 -1.200 1.200 1.0954 99.900 -1.73E-02 267.000 265.800 1.200 1.0954 100.000 3.82E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO >> :! :! :! llli I II I I ' 23 78 2776 3178 3584 3995 4410 4830 5 5, 682 6115 6552 6993 7439 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B068.CNF;1804 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W068.CNF;453 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.85E-02 1.14E-01 3.10E-02 5.89E-02 9.53E-02 2.60E-02 3.28E-02 1.01E-01 2.89E-02 6.85E-01 1.01E-01 2.88E-02 2.91E-02 4.31E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.85E-02 5.87E-02 3.27E-02 4.61E-01 2.90E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235065 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 069 DETECTOR S/N : 78795 AVERAGE %EFFICIENCY : 32.9662 AVERAGE %EFF ERROR : 0.6355 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 91.1 +/-5.981 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE PU-236 PU-238 PU-239 1770-A PU-242 4.3831E+OO dpm 3.9945E+OO dpm LIBRARY PEAK ENERGY ENERGY 5749.00 5723.58 5486.00 5502.78 5155.00 5118.68 PEAK FWHM 4.959 4.959 0.000 COUNT DATE : 17-Sep-201611:42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 7.71E-03 1.000 1.000 0.000 0.0000 99.900 1.24E-02 0.000 -0.720 0.720 0.8485 99.900 -8.88E-03 PU-242 4890.00 4938.75 48.654 317.000 316.040 0.960 0.9798 100.000 3.89E+OO PU-244 4589.00 4546.97 0.000 0.000 -0.240 0.240 0.4899 99.900 -2.96E-03 >> > a 34 PU-244*4497-4597k V . PU-242:4654-4995keV 31 PU*239;5011*52Z7keV PU-238: 5375-5566 keV 28 PU-236: 5582-5843 keV 25 22 -(ii 19 -I-16 z -::::> 13 0 -s. 10 -7 *s: -u 4 <l'. -, .. il -I "" I I I I I I I I I I I I I I I I I 24 04 2802 3206 3614 4026 44< 2 486" 571* 6152 6591 7034 7481 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B069.CNF;1819 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W069.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 4.29E-02 8.21E-02 1.88E-02 3.49E-02 3.72E-02 O.OOE+OO 2.69E-02 7.53E-02 1.92E-02 6.45E-01 8.12E-02 2.21E-02 2.56E-02 5.91E-02 1.11E-02 1.96-sigma cnt Unc pCl/G 4.28E-02 3.49E-02 2.68E-02 4.31E-01 2.55E-02 "t:l Cl> 0\ N 00 0 ,..., U\ 00 0 "' BATCH NUMBER : 1596421 SAMPLE ID : S0405235066 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 070 DETECTOR S/N : 78262 AVERAGE %EFFICIENCY : 31.2964 AVERAGE %EFF ERROR : 0.6038 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 90.3 +/-6.146 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.9579E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5541.00 PU-239 5155.00 5176.90 PU-242 4890.00 4913.24 PU-244 4589.00 4546.97 PU.244; 4497-4597 keV 31 PU*242: 46544995 keV PU-239: 5011-5227 keV 28 PU-238:5375-5566keV PU-236: 5582-5843 keV 25 22 Vi 19 I-16 z :l 13 0 s 10 7 *:;: 4 2381 2775 3175 3578 Energy (keV) PEAK FWHM 0.000 24.500 4.900 38.792 0.000 COUNT DATE : 17-Sep-2016 11 :42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -1.440 1.440 1.2000 100.000 -2.26E-02 3.000 2.280 0.720 0.8485 99.900 3.00E-02 1.000 -0.200 1.200 1.0954 99.900 -2.61E-03 298.000 297.280 0.720 0.8485 100.000 3.88E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 'i 6100 6537 6978 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B070.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W070.CNF;500 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.65E-02 1.16E-01 3.45E-02 5.31E-02 8.03E-02 2.04E-02 3.92E-02 9.16E-02 2.62E-02 6.60E-01 7.97E-02 2.03E-02 2.64E-02 3.92E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.64E-02 5.30E-02 3.92E-02 4.42E-01 2.63E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235067 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 071 DETECTOR S/N : 80020 AVERAGE %EFFICIENCY : 32.1394 AVERAGE %EFF ERROR : 0.6198 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.0 +/-6.024 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.0324E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5717.08 PU-238 5486.00 5445.38 PU-239 5155.00 5118.68 PU-242 4890.00 4893.79 PU-244 4589.00 4546.97 23 PU 244* 4497-4597 kaV PU-242: 4654-4995 keV 21 1-PU-239: 5011-5227 keV PU-238:5375-5566keV 19 t-PU-236: 5582-5643 keV 17 >-15 >-Ui 13 >-1--11 z -:J 9 0 >-7 -.?;-5 *:;: -:g 3 <i: 1 --I I I I PEAK FWHM 4.953 69.348 0.000 62.153 0.000 I II I I I 23 99 2798 3201 3608 4020 -Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 7.83E-03 2.000 1.760 0.240 0.4899 99.900 2.21E-02 0.000 -0.480 0.480 0.6928 99.900 -6.00E-03 312.000 311.040 0.960 0.9798 100.000 3.89E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO > Ji I 111 I I I I I I I 4857 5?8 571:< 6146 6584 7027 7474 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B071.CNF;1814 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W071.CNF;464 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.36E-02 8.34E-02 1.91E-02 4.36E-02 6.03E-02 1.13E-02 2.66E-02 6.93E-02 1.59E-02 6.48E-01 8.23E-02 2.24E-02 2.53E-02 3.75E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.35E-02 4.35E-02 2.65E-02 4.33E-01 2.52E-02 Alpha Spectroscopy Software Version 3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596421 SAMPLE ID : S0405235068 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 072 DETECTOR S/N : 67584 AVERAGE %EFFICIENCY : 31.8335 AVERAGE %EFF ERROR : 0.6139 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 47.7 +/-8.215 % TRACER ID NUCLIDE NOMINAL RESULTS 1770-A PU-242 4.3831E+OO dpm 2.0916E+OO dpm COUNT DATE : 17-Sep-2016 11 :42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY ENERGY FWHM AREA AREA AREA S!Dev pCi/G PU-236 5749.00 5712.26 0.000 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO PU-238 5486.00 5470.35 0.000 0.000 -0.240 0.240 0.4899 99.900 -5.87E-03 PU-239 5155.00 5109.06 10.008 2.000 0.320 1.680 1.2961 99.900 7.78E-03 PU-242 4890.00 4892.73 49.920 161.000 159.800 1.200 1.0954 100.000 3.88E+OO PU-244 4589.00 4556.86 35.028 3.000 3.000 0.000 0.0000 99.900 7.29E-02 :ll -PU-244'44974597 keV 17 PU-242: 46544995 keV f-PU-239:5011-5227keV PU-238: 5375-5566 keV 15 r-PU-236: 5582-5843 keV 13 f-11 f-Ci) 9 I--z ::::> 7 0 -5 1:--*:;: 3 n <l'. -l1 -I I I I I I I I I I I I I I I I I I 23 77 2780 3187 3597 4013 443? 4856 528 571! 6152 6592 7037 7486 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B072.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W072.CNF;475 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.92E-02 8.78E-02 O.OOE+OO 5.08E-02 1.17E-01 2.19E-02 8.87E-02 1.88E-01 5.77E-02 8.83E-01 1.70E-01 4.87E-02 9.67E-02 7.29E-02 O.OOE+OO 1.96-sigma en! Une pCi/G 5.90E-02 5.06E-02 8.86E-02 6.06E-01 9.59E-02 0 ...., Ul 00 0 ID BATCH NUMBER : 1596421 SAMPLE ID : S0405235069 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 073 DETECTOR S/N : 78775 AVERAGE %EFFICIENCY : 33.5965 AVERAGE %EFF ERROR : 0.6474 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 80.3 +/-6.293 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.5202E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5718.81 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4889.55 PU-244 4589.00 4541.25 PU-244* 4497-4597 keV 23 PU-239: 5011-5227 keV 21 t-PU-238: 5375-5566 keV PU-236: 5582-5843 keV 19 >-17 r 15 r 'iii 13 I-z 11 :::> 9 0 7 5 *;;; 3 1 T I I L L I PEAK FWHM 84.102 0.000 0.000 58.916 54.419 I Ill I L COUNT DATE : 17-Sep-2016 11 :42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 0.320 1.680 1.2961 100.000 5.30E-03 0.000 -0.720 0.720 0.8485 99.900 -9.99E-03 0.000 -1.200 1.200 1.0954 99.900 -1.65E-02 286.000 283.840 2.160 1.4697 100.000 3.91E+OO 2.000 1.520 0.480 0.6928 99.900 2.10E-02 >> > !lll I I I rl! I I I I II L L L I L L 23 84 2783 3185 3593 4004 4842 5)6 5697 6132 6571 7015 7463 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B073.CNF;1820 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W073.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.04E-02 1.28E-01 3.93E-02 3.02E-02 8.47E-02 2.16E-02 3.14E-02 9.67E-02 2.77E-02 6.81E-01 1.15E-01 3.71E-02 4.82E-02 7.64E-02 1.75E-02 1.96-sigma en! Unc pCi/G 6.03E-02 3.02E-02 3.13E-02 4.58E-01 4.81E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235070 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 074 DETECTOR S/N : 83296 AVERAGE %EFFICIENCY : 30.3767 AVERAGE %EFF ERROR : 0.5864 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 78.8 +/-6.649 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4544E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5752.09 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4897.81 PU-244 4589.00 4566.43 PU-244: 4497-4597 keV PU-242;4654.4995keV 25 PU-239: 5011-5227 keV PU-238: 5375-5566 keV 22 PU-236: 5582-5843 keV 19 Ui 16 I-13 z ::::> 0 10 7 *s: 4 ti 2383 2784 3189 3599 Energy (keV) PEAK FWHM 4.988 0.000 0.000 44.581 0.000 4012 COUNT DATE : 17-Sep-2016 11 :42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 4.000 1.840 2.160 1.4697 100.000 3.42E-02 0.000 -0.240 0.240 0.4899 99.900 -3.72E-03 0.000 -0.480 0.480 0.6928 99.900 -7.40E-03 254.000 251.840 2.160 1.4697 100.000 3.88E+OO 2.000 2.000 0.000 0.0000 99.900 3.08E-02 6142 6580 7022 7469 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B074.CNF;1838 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W074.CNF;511 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.61E-02 1.56E-01 5.00E-02 3.22E-02 7.44E-02 1.39E-02 3.28E-02 8.54E-02 1.96E-02 7.14E-01 1.29E-01 4.15E-02 5.30E-02 4.63E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 8.59E-02 3.21E-02 3.27E-02 4.83E-01 5.28E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235071_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 075 DETECTOR S/N : 80010 SAMPLE QTY : 0.515 G +/-0.194 % AVERAGE %EFFICIENCY : 32.3452 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.6 +/-6.282 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE 1770-A PU-242 4.3831E+OO dpm 3.6626E+OO dpm LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5711.01 PU-238 5486.00 5470.55 PU-239 5155.00 5107.51 PU-242 4890.00 4883.78 PU-244 4589.00 4546.97 31 PU 244' 4497-4597 keV PlJ.242: 40544995 keV 28 f-PU-239: 5011-5227 keV PU-238:5375-5566keV 25 f-PU-236: 5582-5B43 keV 22 f-19 f-Ui 16 I-f-z 13 ::::> f-0 s 10 f-7 *:;; f-u <l: 4 f-1 f-I I II I I PEAK FWHM 78.677 122.933 118.016 34.421 0.000 I I I 23 79 2775 3175 3580 3990 440p AVERAGE %EFF ERROR : 0.6238 COUNTDATE: 17-Sep-201611:42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 0.320 1.680 1.2961 100.000 5.20E-03 4.000 3.760 0.240 0.4899 99.900 5.11E-02 3.000 2.760 0.240 0.4899 99.900 3.73E-02 286.000 284.320 1.680 1.2961 100.000 3.83E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO ffi II I Ill I I II I I I I I 4824 5;4E 676 6109 6547 6989 7437 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B075.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W075.CNF;478 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.93E-02 1.26E-01 3.86E-02 6.06E-02 6.51E-02 1.22E-02 5.39E-02 6.47E-02 1.21E-02 6.67E-01 1.04E-01 3.20E-02 2.73E-02 4.05E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.93E-02 6.02E-02 5.37E-02 4.48E-01 2.72E-02 AlphaSpectrosoopySoftwareVersion3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596421 SAMPLE ID : S0405235072 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.513 G -+/-0.195 % CHAMBER : 078 DETECTOR S/N : 38633 AVERAGE %EFFICIENCY : 33.4433 AVERAGE %EFF ERROR : 0.6444 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 73.7 +/-6.539 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.2303E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5791.39 PU-238 5486.00 5491.03 PU-239 5155.00 5102.49 PU-242 4890.00 4888.52 PU-244 4589.00 4591.43 23 PU 244* 4497-4597 keV PU-242:4654-4995keV 21 1-PU-239;5011-5227keV PU-23B:5375-5566keV 19 I-PU-236:5582-5B43keV 17 f-15 f-en 13 f-I-11 z f-:J 9 0 f-7 f-z. 5 *:;; f-t5 3 f-<l'. 1 f-I I PEAK FWHM 4.964 4.964 4.964 53.358 4.964 I I I I 23 88 2787 3190 3597 4009 442 Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 -0.200 1.200 1.0954 100.000 -3.57E-03 1.000 0.760 0.240 0.4899 99.900 1.14E-02 1.000 0.760 0.240 0.4899 99.900 1.13E-02 260.000 259.280 0.720 0.8485 100.000 3.85E+OO 1.000 0.760 0.240 0.4899 99.900 1.13E-02 ]] I I 111111 I I I I 4844 5 61 0695 6126 6562 7002 7445 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B078.CNF;1726 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W078.CNF;447 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.36E-02 1.25E-01 3.58E-02 4.27E-02 7.17E-02 1.34E-02 4.24E-02 7.12E-02 1.33E-02 6.97E-01 9.07E-02 2.31E-02 4.24E-02 7.12E-02 1.33E-02 1.96-sigma cnt Unc pCi/G 5.36E-02 4.26E-02 4.24E-02 4.70E-01 4.24E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235073 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY :. 0.505 G -+/-0.198 % CHAMBER : 080 DETECTOR SIN : 78197 AVERAGE %EFFICIENCY : 34.4422 AVERAGE %EFF ERROR : 0.6633 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.0 +/-6.014 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.7686E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5505.30 PU-239 5155.00 5143.01 PU-242 4890.00 4888.02 PU-244 4589.00 4590.46 -PU-244* 4497-4597 keV PU*242:4654-4995keV 28 ,_ PU-239: 5011-5227 keV PU-238: 5375-5566 keV 25 ...._ PU-236: 5582-5843 keV 22 Ui 16 I-,_ z 13 => -0 10 8 ,_ 7 -4 ,_ -I I II I I I PEAK FWHM 0.000 4.969 4.969 39.117 0.000 I II I I I I I 23 86 2786 3190 3598 4011 Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.240 0.240 0.4899 100.000 -3.63E-03 1.000 0.520 0.480 0.6928 99.900 6.57E-03 3.000 2.040 0.960 0.9798 99.900 2.56E-02 312.000 311.520 0.480 0.6928 100.000 3.91E+OO 2.000 1.520 0.480 0.6928 99.900 1.91E-02 >> !l!l ,,1,llJ rl I I I I I I I I I 4849 5)7, p705 6139 6578 7021 7468 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B080.CNF;1728 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W080.CNF;446 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.14E-02 7.25E-02 1.36E-02 3.66E-02 7.00E-02 1.60E-02 5.11E-02 8.28E-02 2.25E-02 6.51E-01 6.95E-02 1.59E-02 4.39E-02 6.96E-02 1.59E-02 1.96-sigma cnt Unc pCi/G 3.13E-02 3.65E-02 5.10E-02 4.35E-01 4.39E-02 AlphaSpectroscopySoftwareVersion3.5.3 effectlvedate:02*Mar-2015 BATCH NUMBER : 1596421 SAMPLE ID : S0405235074 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 081 DETECTOR S/N : 79996 AVERAGE %EFFICIENCY : 33.0506 AVERAGE %EFF ERROR : 0.6369 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 46.0 +/-8.229 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.0181 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.23 PU-238 5486.00 5470.33 PU-239 5155.00 5044.07 PU-242 4890.00 4880.83 PU-244 4589.00 4597.20 15 PU-244: 4497-4597 keV PlJ.242:4654-4995keV PU-239:5011-5227keV 13 PlJ.238: 5375-5566 keV PU-236:5582-5843keV 11 (j) 9 I-7 z :::i 0 5 .2:-3 *:;; n <t: 2384 2779 3178 3582 Energy (keV) PEAK FWHM 0.000 0.000 4.901 67.881 0.000 3991 COUNT DATE : 17-Sep-2016 11 :42:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.240 0.240 0.4899 100.000 -7.10E-03 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 1.000 0.040 0.960 0.9798 99.900 9.86E-04 162.000 160.080 1.920 1.3856 100.000 3.94E+OO 1.000 0.520 0.480 0.6928 99.900 1.28E-02 673 6106 6543 6985 7432 ; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B081.CNF;1734 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W081.CNF;446 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.15E-02 1.42E-01 2.66E-02 5.01E-02 7.44E-02 O.OOE+OO 7.32E-02 1.62E-01 4.42E-02 8.98E-01 1.99E-01 6.25E-02 7.13E-02 1.36E-01 3.13E-02 1.96-sigma cnt Unc pCi/G 6.13E-02 5.00E-02 7.31E-02 6.17E-01 7.12E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235075 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 082 DETECTOR S/N : 79997 SAMPLE QTY : 0.508 G -+/-0.197 % AVERAGE %EFFICIENCY : 31.9848 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 76.7 +/-6.584 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3625E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.23 PU-238 5486.00 5525.58 PU-239 5155.00 5189.96 PU-242 4890.00 4891.83 PU-244 4589.00 4546.96 PU 244* 4497-4597 keV 23 I-PU-242: 4054-4995 keV PU-239:5011*5227keV 21 t-PU-238: 5375-5566 keV PU-236:5SS2*5843keV 19 f-17 15 f-'Ci) 13 1--z 11 f-::::> 9 0 7 1:-5 *s: 3 PEAK FWHM 0.000 4.883 4.883 54.322 0.000 1 Ir I I I II 11 I I I I I I 23 94 2787 3185 3588 3996 440 Energy (keV) AVERAGE %EFF ERROR : 0.6168 COUNTDATE: 17-Sep-201611:42:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.30E-02 1.000 -0.200 1.200 1.0954 99.900 -3.03E-03 1.000 -3.080 4.080 2.0199 99.900 -4.64E-02 261.000 258.120 2.880 1.6971 100.000 3.89E+OO 0.000 -0.240 0.240 0.4899 99.900 -3.62E-03 111 I Ill I I I I I I 4826 5:4S 676 6108 6545 6987 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B082.CNF;1724 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W082.CNF;423 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.94E-02 1.11E-01 2.81E-02 4.56E-02 1.06E-01 3.04E-02 5.15E-02 1.57E-01 5.58E-02 7.09E-01 1.39E-01 4.68E-02 3.13E-02 7.23E-02 1.35E-02 1.96-sigma en! Une pCi/G 3.93E-02 4.55E-02 5.15E-02 4.78E-01 3.12E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235076 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 083 DETECTOR S/N : 78785 SAMPLE QTY : 0.512 G -+/-0.195 % AVERAGE %EFFICIENCY : 35.3477 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 104 +/-5.477 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.5599E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5747.57 PU-238 5486.00 5487.40 PU-239 5155.00 5122.63 PU-242 4890.00 4901.61 PU-244 4589.00 4525.17 -PU 244* 4497-4597 keV PU-242: 46544995 keV 33 _ PU-239: 5011-5227 keV PU-236:5375-5566keV PlJ.236:5582-5843keV 29 Ui 21 -I-17 z -::i 0 13 8 -c 9 -*s; t5 5 -<( -I I I I I PEAK FWHM 24.717 79.093 74.150 56.848 49.433 I "' I 23 92 2790 3192 3598 4009 4423 -Energy (keV) AVERAGE %EFF ERROR : 0.6805 COUNTDATE: 17-Sep-201611:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.520 0.480 0.6928 100.000 1.83E-02 4.000 3.520 0.480 0.6928 99.900 3.53E-02 2.000 1.040 0.960 0.9798 99.900 1.04E-02 389.000 386.840 2.160 1.4697 100.000 3.86E+OO 4.000 3.520 0.480 0.6928 99.900 3.51E-02 .JLJ "' " I' I I I I I 4843 5 6 i694 6126 6562 7003 7448 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B083.CNF;1740 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W083.CNF;485 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.20E-02 6.66E-02 1.53E-02 4.49E-02 5.56E-02 1.27E-02 3.55E-02 6.58E-02 1.79E-02 5.85E-01 8.36E-02 2.68E-02 4.47E-02 5.53E-02 1.27E-02 1.96-sigma cnt Unc pCi/G 4.20E-02 4.48E-02 3.55E-02 3.86E-01 4.45E-02 AlphaSpectroscopySoftwareVerslon3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596421 SAMPLE ID : S0405235077 PU SAMPLE QTY : 0.510 G -+/-0.196 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 084 DETECTOR S/N : 78265 AVERAGE %EFFICIENCY : 34.7248 AVERAGE %EFF ERROR : 0.6686 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 65.9 +/-6.779 % COUNT DATE : 17-Sep-201611:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.8865E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5529.44 PU-239 5155.00 5164.30 PU-242 4890.00 4899.77 PU-244 4589.00 4543.42 21 PlJ..244*4497-4597keV PU-242: 46544995 keV 19 1-PU-239: 5011-5227 keV PlJ..238; 537S.5566 keV 17 f-PU-236:5582-5843keV 15 -13 f-11 z 9 :J 0 7 5 *:;; :g 3 <( *1 I I I I 24 02 2799 3200 3606 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 54.265 2.000 29.599 2.000 54.182 242.000 4.933 5.000 >> ::i I I 1111 I I I 1!1 l1W I I 4016 4850 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABLIN ACTIVITY AREA AREA StDev pCi/G -0.720 0.720 0.8485 100.000 -1.39E-02 2.000 0.000 0.0000 99.900 3.24E-02 0.320 1.680 1.2961 99.900 5.16E-03 240.560 1.440 1.2000 100.000 3.87E+OO 4.760 0.240 0.4899 99.900 7.67E-02 >> II I I I I I I I I 5701 6133 6570 7011 7457 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B084.CNF;1729 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W084.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.21E-02 1.18E-01 3.00E-02 5.57E-02 4.86E-02 O.OOE+OO 5.88E-02 1.25E-01 3.82E-02 7.27E-01 1.19E-01 3.54E-02 7.88E-02 7.72E-02 1.45E-02 1.96-sigma cnt Unc pCi/G 4.20E-02 5.55E-02 5.87E-02 4.92E-01 7.81E-02 BATCH NUMBER : 1596421 SAMPLE ID : S0405235078 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 085 DETECTOR S/N : 78776 AVERAGE %EFFICIENCY : 32.9780 AVERAGE %EFF ERROR : 0.6356 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 82.8 +/-6.241 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6297E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5428.03 PU-239 5155.00 5215.97 PU-242 4890.00 4894.63 PU-244 4589.00 4546.97 PU 244*4497-4597 keV 21 _ PU-242: 4654-4995 keV PU-239:5011-5227keV 19 ..._ PU-238: 5375-5566 keV PU-236: 5582-5843 kaV 17 -15 (ii 13 I-11 -z :::i 9 0 -7 5 *;:; -:g 3 -<I'. 1 -I I I PEAK FWHM 0.000 49.309 4.931 73.141 0.000 I 11 I I 23 85 2782 3182 3587 3996 COUNT DATE : 17-Sep-2016 11 :42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -1.96E-02 3.000 1.320 1.680 1.2961 99.900 1.81E-02 1.000 -0.440 1.440 1.2000 99.900 -5.99E-03 288.000 287.280 0.720 0.8485 100.000 3.91E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO >> i I 111111 I Ill II I I I I I I 4826 5 4E 673 6103 6537 6974 7416 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B085.CNF;1732 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W085.CNF;479 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 3.72E-02 1.15E-01 3.28E-02 5.68E-02 1.06E-01 3.25E-02 4.14E-02 1.01E-01 2.99E-02 6.76E-01 8.31E-02 2.12E-02 2.75E-02 4.09E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.72E-02 5.67E-02 4.14E-02 4.54E-01 2.75E-02 0 ...., Ul 00 0 '° BATCH NUMBER : 1596421 SAMPLE ID : S1203621769 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 086 DETECTOR S/N : 78198 AVERAGE %EFFICIENCY : 31.1951 AVERAGE %EFF ERROR : 0.6019 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 83.0 +/-6.420 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6379E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5437.23 PU-239 5155.00 5017.21 PU-242 4890.00 4898.93 PU-244 4589.00 4559.45 PU..244' 44974597 keV 37 f-PU-242: 46544995 keV PU-239: 5011-5227 keV PU..238:5375-5566keV 33 f-PU-236: 5582-5843 keV 29 f-25 f-0' 21 f-z 17 ::::> f-0 s 13 f-c 9 *:;; f-u <( 5 f-1 f-I I I PEAK FWHM 0.000 118.750 4.948 19.527 4.948 I 23 81 2779 3181 3587 3998 4416 COUNT DATE : 17-Sep-2016 11 :42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.01E-02 5.000 4.040 0.960 0.9798 99.900 5.66E-02 1.000 0.040 0.960 0.9798 99.900 5.60E-04 275.000 272.360 2.640 1.6248 100.000 3.81E+OO 1.000 0.520 0.480 0.6928 99.900 7.28E-03 .L " I I I I I I 4832 5 5E 6116 6552 6992 7437 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B086.CNF;1733 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W086.CNF;455 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.05E-02 8.56E-02 2.18E-02 6.93E-02 9.23E-02 2.51E-02 4.16E-02 9.23E-02 2.51E-02 6.78E-01 1.25E-01 4.17E-02 4.05E-02 7.76E-02 1.78E-02 1.96-sigma cnt Unc pCi/G 3.05E-02 6.89E-02 4.15E-02 4.56E-01 4.05E-02 BATCH NUMBER : 1596421 SAMPLE ID : S1203621770 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 088 DETECTOR SIN : 83291 AVERAGE %EFFICIENCY : 31.2191 AVERAGE %EFF ERROR : 0.6024 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.4 +/-6.111 % TRACER 1770-A PU-242 ID NUCLIDE NOMINAL RESULTS 4.3831 E+OO dpm 4.0488E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5798.83 PU-238 5486.00 5485.03 PU-239 5155.00 5118.68 PU-242 4890.00 4892.91 PU-244 4589.00 4589.29 37 PU 244' 4497-4597 keV -PU-242: 4654-4995 keV PU-239:5011-5227keV 33 t-PU-236: 537S.5566 keV PlJ.236: 5582-5843 keV 29 t--25 t--Vi 21 t--1--z 17 t--::J 0 13 t--.?;-9 t--*:;: t5 5 t--<( t--I I I PEAK FWHM 4.923 9.845 0.000 36.398 4.923 I I I 23 87 2783 3184 3589 3998 4411> COUNT DATE : 17-Sep-201611:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.520 0.480 0.6928 100.000 8.03E-03 2.000 1.760 0.240 0.4899 99.900 2.28E-02 0.000 -1.440 1.440 1.2000 99.900 -1.85E-02 306.000 303.360 2.640 1.6248 100.000 3.89E+OO 1.000 1.000 0.000 0.0000 99.900 1.28E-02 >> 1.L I I I I I 4830 5 5: 681 6112 6549 6989 7434 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B088.CNF;1728 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W088.CNF;463 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.47E-02 8.55E-02 1.96E-02 4.48E-02 6.20E-02 1.16E-02 2.99E-02 9.50E-02 2.82E-02 6.59E-01 1.15E-01 3.82E-02 3.62E-02 3.85E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.46E-02 4.47E-02 2.98E-02 4.41E-01 3.61E-02 BATCH NUMBER : 1596421 SAMPLE ID : S1203621771_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G +/-0.193 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 58.9 +/-8.130 % TRACER ID 1770-A NUCLIDE PU-242 NOMINAL 4.3831E+OO dpm RESULTS 2.5818E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5773.82 78.867 PU-238 5486.00 5521.49 4.929 PU-239 5155.00 5151.24 69.009 PU-242 4890.00 4895.23 73.938 PU-244 4589.00 4551.68 4.929 12 PlJ..244: 4497-4597 keV PU-242: 4654-4995 keV 11 PU-239:5011*5227keV PU-238: 5375-5566 keV 10 PU-236: 5582-5643 keV 9 8 'iii 7 I-6 z 5 :J 0 4 3 *::; 2 t5 <t: 2402 2798 3198 Energy (keV) COUNT DATE : 17-Sep-201611:44:20 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0338-MM NUCLIDE PU-239 NOMINAL (pCi/G) 3.8148E+OO % RECOVERY 104.617 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 4.000 3.040 0.960 0.9798 100.000 7.14E-02 1.000 -0.440 1.440 1.2000 99.900 -1.03E-02 170.000 170.000 0.000 0.0000 99.900 3.99E+OO 163.000 162.520 0.480 0.6928 100.000 3.81E+OO 1.000 1.000 0.000 0.0000 99.900 2.35E-02 >> > 6974 7413 ; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B169.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.07E-01 1.55E-01 4.22E-02 7.14E-02 1.74E-01 5.16E-02 8.89E-01 7.04E-02 O.OOE+OO 8.58E-01 1.30E-01 2.98E-02 6.61E-02 7.04E-02 O.OOE+OO 1.96-sigma en! Unc pCi/G 1.06E-01 7.13E-02 6.02E-01 5.89E-01 6.60E-02 Effective 3/25/2010 Radiochemistry Batch Checklist Revision 1 Effective March 2010 21-Sep-2016 Batch# \ SC)LoL/f 1_ Product: __ _,&'-':....;;:=----Date: Criteria: Yes No Comments Samole Solids are less tha*n or eaual to 100 ma for GAB. 1\-b Samples have been blank corrected (If required). l}j?.. Blank correction reoorted included flf reaulredl. If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. , If greater than 10* MDA/ MDC, error Is 40% or less. " If h1>ln ... +hn Un A./ unf' Arrnr 1 .. n ... .. Instrument source check Is within limits. hkn r:h,.ck I.: within limits. / Method RDL/ LLD has been met. /' If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, ./ If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reauired RER acceotance criteria. Tracer yield Is 15-125%

Carrier yleld 25-125%. ,,.,,, (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. v (Tf _,, ----<' o;O/n nf ln* .. ne+ :>rtiulru\ Sample was run within hold time. ii' t S,o(J;"'b I Samole was correc:tlv oreserved If reaulred. f\.Jfq--Smears Taken for Radioactive batches. (VI!}-Method Spike and LCS are within 75-125% lror meets the cll<>nt's contract acc .. n*ance criteria), ,/ No blank saaces on data forms. All line outs Initialed and dated. v ll\Jn nrrnre :>rn Aux data Is correct. v' Client Soeclal reoulrements naae has been checked. V' Raw Data and/ or soectrum are Included and orooerlv statused. ,,,,.,.. MS, LCS, and Duplicate RPD/RER values uploaded to UMS and v ...__ u:>luae VPrfflnA ..... -*-(if U'O-IR:>trh <>ntnrafl lntn r:>e<> <..---' Batch Data Exceotlon Reoorts fDERl comoleted If aoollcable. ./ Batch Data Exception Reports (DER) second reviewed. ./ OllU\=-1"Sbf)c;'3 I Dlsoosltlon verified to be comoleted. Allnuot Corr,,ctlnn comoleted If r"nulred llYL Review sample historical results If available ./ (If REMP, results above MDC have been verified bv historical results. recount or re-anatvsls. l Primary Review Performed By:. __ __ -'----Secondary Review Performed By:__ 09/30/16 Gi0 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DER Report No.: 1560531 Revision No.: DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: Type: 22-SEP-16 Radiochemistry Specifications Process Instrument Type: Test I Method: Matrix Type: Client Code: ALPHA SPECTROMETER DOE EML HASL-300, Pu-11-RC Solid MJWC I Batch ID: Sample Numbers: 1596412 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Peak Centroid Values Off Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, and 1203621752 were received and analyzed out of holding. 2. The Pu-242 tracer peak centroid for sample 405235047 is greater than 2. The sample does meet the tracer yield requirement, the detection limits, 50 keV from the expected energy value of 4890 keV. and its tracer peak is within the Pu-242 region of interest. Reporting results. Originator's Name: Data Validator/Group Leader: Melanie Aycock 22-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 645 of 5809 Plutonium Queue Sheet 07-SEP-16 ----------============================================================================== Batch#: 1596412 Analyst: HAKB First Client Due Date:04-0CT-16 Tracer Isotope(s) Pu-24 u-236 Tracer Code: \']:Jo -A Expiration LCS Isotope(s) Pu-23 u-238 LCS Code: M,g Expiration Spike Isotope(s): Pu-239/Pu-238 Spike Code: -Expiration Date: ____ _ Internal Due Date:30-SEP-16 Analyzed Sequentially with: Vo!.;tZS-\ U: 'tog Vol:_:__ Am: l'G°"'ll:.q 1 t> q\:Bo' lb Initials: PipetID: \g\fco;l..=l,. Balance ID: Wet/@) Hazard Min Collection Label Aliquot Sample ID Client Description Code CRDL Matrix Client Date Pos. # _{!jJ__ l / t) Det # Pu Type =40=5=23=5=04=1-=1=====4=.4=n=.R=.=1.=4===================s=Al=MP==L=E==========1=p=c=ilg========so=1=L==========1,u==w=c=o=o1=======30=_N=o=v=-=l:l=-=====1==:::::;::===1 == !-¢-.QJ---9-:--zrd--i 405235042-1 4.4D.R.2.3 SAMPLE 1 pCi/g SOIL l\UWCOOl 30-NOV-15 2 )... tt>_._:S'"O Di (tL_j 405235043-1 4.4D.R.2.4 SAMPLE 1 pCi/g SOIL MJWCOOl 30-NOV-15 3 7o ! 405235044-1 4.4D.R.4.2 SAMPLE 1 pCi/g SOIL MJWCOOl 30-NOV-15 4 / ( 405235045-1 4.4D.R.5.2 SAi"1PLE 1 pCi/g SOIL l\UWCOOl 30-NOV-15 5 I s-!<P' s:o 2J 7Z.. 405235046-1 4.SA.R.1.3 sA.l\1PLE 1 pCi/g so IL MJWC001 o017:DnEEcc:11;,5* 6 I rll; 3 405235047-1 4.SA.R.1.4 SAMPLE 1 pCi/g SOIL MJWCOOl 7 '::7-/Lf ! 405235048-1 4.SB.R.1.2 SAi'\.1PLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 8 Ci;; 12. S-0 :t-!. /!f" /,: 405235049-1 4.SB.R.1.3 SAMPLE 1 pCi/g SOIL 1\-fJWCOOl 07-DEC-15 9 °l ip$, S:Q b: "78 : 405235050-1 4.SB.R.1.4 SAMPLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 10 , I "ti 405235051-1 4.SB.R.2.3 SAMPLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 11 Ll\_fOLSQ_2d __ <6_\___J 405235052-1 4.SB.R.2.4 SAMPLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 12 ! 1..., . r 0 l a,-z_, l ,__-__ I"'--'-LLL.Q__I 405235053-1 4.SC.R.5.2 SAMPLE 1 pCi/g SOIL MJWCOOl 01-DEC-15 13 I l3 , ;:Q 0 i 't> 'I i 405235054-1 4.SC.R.1.3 SAMPLE 1 pCi/g SOIL MJWCOOl 02-DEC-15 14 j I I./ .S::O_Q; CJD j 405235055-1 4.SC.R.1.4 SAMPLE 1 pCi/g SOIL MJWCOOl 02-DEC-15 15 l I ...-ios r--l t> I '9 t i 405235056-1 4.5C.R.2.2 SAMPLE 1 pCi/g SOIL .MJWCOOI 02-DEC-15 16 z_ i 405235051.1 4.sc.R.2.3 sAi'\fPLE 1 pCi/g sOIL MJwcoo1 02-nEc-15 11 I I "::J.. ti s-o-p_! __ 93 ! 405235058-1 4.SC.R.2.4 SAMPLE 1 pCi/g SOIL MJWCOOl 02-DEC-15 18 j ( , ( U 7 !(" j 405235059-1 5.lA.R.1.2 SAMPLE 1 pCi/g SOIL l\.fJWCOOl 16-DEC-15 19 I i 4 I&. s-031 . 14> ! 405235060-1 5.lA.R.1.3 SAJ\.!PLE 1 pCi/g SOIL MJWCOOl 16-DEC-15 20 I ").-0 ' 5' 1203621751-1 MB for batch 1596412 J.\oIB 1 pCi/g SOIL QC ACCOUNT 21 i 1--\ ( s.1__! ___ _j_1J_jj_J 1203621752-1 4.4D.R.1.4(405235041DUP) DUP 1 pCi/g SOIL QC ACCOUNT 30-NOV-15 22 ! 2-"2.-!p:-'--s;-{ 1203621753-1 LCS for batch 1596412 LCS 1 pCi/g SOIL QC ACCOUNT 23 J !¢Sf!;:'! f_b_'-U Choose SOP Used: @AD-A-Of\ GL-RAD-A-036, Solid Sample Dissolution by: LEACH oGiiGEST GL-RAD-A-053 Circle One GEL Laboratories LLC, , Radiochemistry Divisio11 Data Reviewed By: \"A..\tc, Page: 1 of 1 BATCH NUMBER : 1596412 SAMPLE ID : S0405235041_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 067 DETECTOR S/N : 78780 AVERAGE %EFFICIENCY : 29.1959 AVERAGE %EFF ERROR : 0.5641 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 69.6 +/-9.741 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.0510E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5634.56 PU-238 5486.00 5461.05 PU-239 5155.00 5118.69 PU-242 4890.00 4862.17 PU-244 4589.00 4556.91 8 PU-244: 4497-4597 kaV PU-242: 46544995 keV PlJ..239:5011-5227kaV 7 PU-238: 5375-5566 keV PU-236: 5582-5843 keV 6 5 Cii 4 I-z :::> 3 0 !2.. 2 *::; PEAK FWHM 4.935 19.738 0.000 92.935 4.935 2379 2776 3177 3583 3992 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:19 ELAPSED LIVE TIME(SEC) : 7510.30 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.374 0.626 0.7911 100.000 1.59E-02 2.000 2.000 0.000 0.0000 99.900 7.01E-02 0.000 -0.250 0.250 0.5003 99.900 -8.72E-03 112.000 111.499 0.501 0.7076 100.000 3.88E+OO 1.000 1.000 0.000 0.0000 99.900 3.48E-02 6102 6537 6976 7419 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B067.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W067.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.20E-01 2.44E-01 5.85E-02 1.20E-01 1.05E-01 O.OOE+OO 7.02E-02 1.65E-01 3.04E-02 1.05E+OO 1.90E-01 4.30E-02 9.71E-02 1.04E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.20E-01 1.19E-01 6.98E-02 7.25E-01 9.69E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235042 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 069 DETECTOR S/N : 78795 AVERAGE %EFFICIENCY : 32.9662 AVERAGE %EFF ERROR : 0.6355 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 79.8 +/-8.595 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4981E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4905.23 PU-244 4589.00 4546.97 12 PlJ.244:4497-4597 keV PU-242:4654-4995keV 11 PU-239:5011-5227keV PU-238:5375-5566keV 10 PU-236: 5582-5843 keV 9 8 en 7 I-6 z 5 ::J 0 4 3 *:;: 2 t5 <i: 1 2404 2802 3206 Energy (keV) PEAK FWHM 0.000 0.000 0.000 69.971 0.000 COUNT DATE : 22-Sep-2016 09:56:19 ELAPSED LIVE TIME(SEC) : 7518.12 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.251 0.251 0.5006 100.000 -8.34E-03 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 0.000 -0.376 0.376 0.6131 99.900 -1.03E-02 145.000 144.499 0.501 0.7080 100.000 3.95E+OO 0.000 -0.125 0.125 0.3540 99.900 -3.43E-03 >> S;l;; ;i; § 6152 6591 7034 7481 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B069.CNF;1819 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W069.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.70E-02 1.58E-01 2.91E-02 5.46E-02 8.26E-02 0.00E+OO 5.55E-02 1.41E-01 2.93E-02 9.40E-01 1.50E-01 3.38E-02 5.47E-02 1.16E-01 1.69E-02 1.96-sigma cnt Unc pCi/G 6.68E-02 5.44E-02 5.53E-02 6.47E-01 5.45E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235043 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 070 DETECTOR S/N : 78262 AVERAGE %EFFICIENCY : 31.2964 AVERAGE %EFF ERROR : 0.6038 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 88.8 +/-8.370 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.8901 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5464.34 PU-239 5155.00 5118.67 PU-242 4890.00 4871.68 PU-244 4589.00 4545.79 14 PU-244: 4497-4597 keV PU.242: 46544995 keV 13 PU-2J9:5011-5227keV 12 PlJ..238:537S-5566keV PU-236: 5582-5843 keV 11 10 9 Ui 8 I-7 z 6 '.:) 0 5 8 4 3 *::; n 2 <t: 1 2381 2775 3175 Energy (keV) PEAK FWHM 0.000 4.900 0.000 53.083 4.900 COUNT DATE : 22-Sep-2016 09:56:19 ELAPSED LIVE TIME(SEC) : 7521.69 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.752 0.752 0.8673 100.000 -2.34E-02 1.000 0.624 0.376 0.6133 99.900 1.60E-02 0.000 -0.627 0.627 0.7917 99.900 -1.60E-02 153.000 152.624 0.376 0.6133 100.000 3.89E+OO 1.000 1.000 0.000 0.0000 99.900 2.55E-02 ll > > >> .:ii .:ii a 5 41 668 6100 6537 6978 7424 ; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B070.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W070.CNF;500 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.44E-02 1.87E-01 4.70E-02 7.25E-02 1.32E-01 2.75E-02 5.25E-02 1.47E-01 3.53E-02 9.03E-01 1.31E-01 2.73E-02 7.12E-02 7.66E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.42E-02 7.24E-02 5.24E-02 6.21E-01 7.11E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235044 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 071 DETECTOR S/N : 80020 AVERAGE %EFFICIENCY : 32.1394 AVERAGE %EFF ERROR : 0.6198 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 75.0 +/-8.598 % TRACER 1770-A .ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.2855E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749,00 5712.25 PU-238 5486.00 5470.34 PU-239 5155.00 5127.52 PU-242 4890.00 4893.28 PU-244 4589.00 4514.88 14 PU-244: 4497-4597 keV PU-242: 46544995 keV 13 PU-239:5011-5227keV 12 PU-238:5375-5566keV PU-236: 5582-5843 keV 11 10 9 Ui 8 1--7 z 6 ::::> 0 5 8 4 3 *:;; ti 2 <( 1 2399 2798 3201 3608 Energy (keV) PEAK FWHM 0.000 0.000 4.953 47.057 4.953 COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8207.94 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.274 0.274 0.5231 100.000 -9.02E-03 0.000 -0.137 0.137 0.3699 99.900 -3.73E-03 1.000 0.726 0.274 0.5231 99.900 1.97E-02 145.000 144.453 0.547 0.7397 100.000 3.91E+OO 1.000 1.000 0.000 0.0000 99.900 2.71E-02 r; a :£:2 6146 6584 7027 7474 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B071.CNF;1814 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W071.CNF;464 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.67E-02 1.59E-01 3.03E-02 5.46E-02 1.17E-01 1.77E-02 7.63E-02 1.31E-01 2.49E-02 9.31E-01 1.51E-01 3.51E-02 7.56E-02 8.13E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.64E-02 5.44E-02 7.61E-02 6.41E-01 7.54E-02 0 ....., Vi 00 0 \.() BATCH NUMBER : 1596412 SAMPLE ID : S0405235045 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 072 DETECTOR S/N : 67584 AVERAGE %EFFICIENCY : 31.8335 AVERAGE %EFF ERROR : 0.6139 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 73.0 +/-8.753 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.1977E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5407.13 PU-239 5155.00 5122.44 PU-242 4890.00 4867.99 PU-244 4589.00 4546.97 15 PU244*4497-4597k V ' PU-242: 45544995 keV PU-239: 5011-5227 keV 13 I-PU.238: 5375-5566 keV PlJ.236: 5582-5843 keV 11 -'Ci) 9 -I-7 z f-::i 0 5 !2, 0 <t: I I I I PEAK FWHM 0.000 5.004 5.004 58.484 0.000 II I I COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8211.60 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.863 0.137 0.3699 99.900 2.45E-02 1.000 0.042 0.958 0.9788 99.900 1.19E-03 140.000 139.316 0.684 0.8272 100.000 3.93E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO ll 11\111 I II I I I I I 23 77 2780 3187 3597 4013 443(2 4856 528 571! 6152 6592 7037 7486 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B072.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W072.CNF;475 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.83E-02 1.03E-01 O.OOE+OO 7.97E-02 1.22E-01 1.85E-02 8.14E-02 1.82E-01 4.85E-02 9.54E-01 1.67E-01 4.10E-02 5.61E-02 B.48E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.80E-02 7.96E-02 8.12E-02 6.57E-01 5.59E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235046 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G -+/-0.195 % CHAMBER : 073 DETECTOR SIN : 78775 AVERAGE %EFFICIENCY : 33.5965 AVERAGE %EFF ERROR : 0.6474 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 77.0 +/-8.313 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3753E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5659.37 PU-238 5486.00 5438.60 PU-239 5155.00 5118.68 PU-242 4890.00 4861.75 PU-244 4589.00 4546.97 13 PU.244: 4497-4597 keV PU*242: 46544995 keV 12 PU-239:5011*5227keV PU-238: 5375-5566 keV 11 PU-236; 5582-5843 keV 10 9 8 0' 7 z 6 => 5 0 8 4 3 *:;; 2 u <( 1 2384 2783 3185 Energy (keV) PEAK FWHM 4.947 4.947 0.000 55.965 0.000 COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8241.52 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 1.000 0.038 0.962 0.9806 100.000 1.15E-03 1.000 0.588 0.412 0.6419 99.900 1.46E-02 0.000 -0.687 0.687 0.8287 99.900 -1.70E-02 157.000 155.764 1.236 1.1119 100.000 3.84E+OO 0.000 -0.275 0.275 0.5241 99.900 -6.78E-03 ffi 6132 6571 7015 7463 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B073.CNF;1820 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W073.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.61E-02 1.93E-01 5.14E-02 7.03E-02 1.30E-01 2.80E-02 5.12E-02 1.46E-01 3.59E-02 8.85E-01 1.70E-01 4.81E-02 4.99E-02 1.19E-01 2.27E-02 1.96-sigma cnt Unc pCi/G 8.60E-02 7.01E-02 5.10E-02 6.08E-01 4.97E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235047 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 074 DETECTOR S/N : 83296 AVERAGE %EFFICIENCY : 30.3767 AVERAGE %EFF ERROR : 0.5864 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 76.4 +/-8.758 % TRACER ID NUCLIDE NOMINAL RESULTS 1770-A . PU-242 4.3831E+OO dpm 3.3481 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5777.78 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4834.56 PU-244 4589.00 4557.66 10 PU-244: 4497-4597 keV PlJ.242:4654-4995keV 9 PU-239: 5011+5227keV PU-238: 5375-5566 keV PU-236: 5582-5843 keV 8 7 en 6 I-5 z ::J 4 0 8 3 2 *::; u <{ 2383 2784 3189 Energy (keV) PEAK FWHM 4.988 0.000 0.000 93.942 64.845 COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8245.21 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 1.000 -0.237 1.237 1.1121 100.000 -8.06E-03 0.000 -0.137 0.137 0.3707 99.900 -3.89E-03 0.000 -0.275 0.275 0.5243 99.900 -7.73E-03 141.000 139.763 1.237 1.1121 100.000 3.93E+OO 3.000 3.000 0.000 0.0000 99.900 8.43E-02 6142 6580 7022 7469 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B074.CNF;1838 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W074.CNF;511 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.89E-02 2.35E-01 6.65E-02 5.67E-02 1.22E-01 1.84E-02 5.69E-02 1.36E-01 2.59E-02 9.52E-01 1.94E-01 5.48E-02 1.11E-01 8.43E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 9.88E-02 5.65E-02 5.66E-02 6.56E-01 1.10E-01 BATCH NUMBER : 1596412 SAMPLE ID : S0405235048 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 075 DETECTOR S/N : 80010 AVERAGE %EFFICIENCY : 32.3452 AVERAGE %EFF ERROR : 0.6238 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 83.1 +/-8.150 % TRACER 1770-A PU-242 ID NUCLIDE NOMINAL RESULTS 4.3831 E+OO dpm 3.6436E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5470.34 PU-239 5155.00 5154.42 PU-242 4890.00 4853.22 PU-244 4589.00 4522.01 13 PlJ.244: 4497-4597 keV PU*242: 4654-4995 keV 12 PU-239:5011*5227keV PlJ..238:5375-5566keV 11 PU-236: 5582-5843 keV 10 9 8 00 7 1--6 z => 5 0 4 3 *;;; 2 u <l'. 2379 2775 3175 3580 Energy {keV) PEAK FWHM 0.000 0.000 29.504 90.151 19.669 3990 COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8249.61 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.962 0.962 0.9810 100.000 -2.81E-02 0.000 -0.137 0.137 0.3708 99.900 -3.33E-03 2.000 1.863 0.137 0.3708 99.900 4.48E-02 163.000 162.038 0.962 0.9810 100.000 3.89E+OO 2.000 2.000 0.000 0.0000 99.900 4.81E-02 a $N 6109 6547 6989 7437 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B075.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W075.CNF;478 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.15E-02 1.88E-01 5.02E-02 4.85E-02 1.04E-01 1.57E-02 8.25E-02 1.03E-01 1.57E-02 8.79E-01 1.55E-01 4.14E-02 8.23E-02 7.22E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.13E-02 4.83E-02 8.22E-02 6.04E-01 8.19E-02 AlphaSpectroscopySoftwaraVers!on3.5.3 effeetivedate:02-Mar-2015 BATCH NUMBER : 1596412 SAMPLE ID : S0405235049 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 078 DETECTOR S/N : 38633 AVERAGE %EFFICIENCY : 33.4433 AVERAGE %EFF ERROR : 0.6444 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 79.6 +/-8.146 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4906E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.27 PU-238 5486.00 5470.35 PU-239 5155.00 5134.30 PU-242 4890.00 4863.39 PU-244 4589.00 4546.97 11 PU-244: 4497-4597 keV PU-242:4654-4995keV 10 PU-239: 5011-5227 kaV PU-238:5375-5566keV 9 PU-236: 5582-5843 keV 8 7 6 z 5 :::i 0 4 8 3 c *:;; 2 2388 2787 3190 Energy (keV) PEAK FWHM 0.000 0.000 4.964 78.589 0.000 COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8305.06 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 0.000 -0.692 0.692 0.8319 100.000 -2.03E-02 0.000 -0.138 0.138 0.3720 99.900 -3.37E-03 1.000 0.862 0.138 0.3720 99.900 2.08E-02 162.000 161.585 0.415 'o.6444 100.000 3.90E+OO 0.000 -0.138 0.138 0.3720 99.900 -3.35E-03 !;: a 6126 6562 7002 7445 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B078.CNF;1726 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W078.CNF;447 CAL DA TE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.08E-02 1.73E-01 4.28E-02 4.87E-02 1.05E-01 1.59E-02 6.78E-02 1.04E-01 1.58E-02 8.81E-01 1.27E-01 2.73E-02 4.84E-02 1.04E-01 1.58E-02 1.96-sigma en! Unc pCi/G 6.06E-02 4.86E-02 6.76E-02 6.04E-01 4.83E-02 AlphaSpeclrcscopySoftwareVerslon3.5.3 effeciivedate:02-Mar-2015 BATCH NUMBER : 1596412 SAMPLE ID : S0405235050 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 080 DETECTORS/N : 78197 AVERAGE %EFFICIENCY : 34.4422 AVERAGE %EFF ERROR : 0.6633 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 88.3 +/-7.644 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.8723E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4873.72 PU-244 4589.00 4585.20 PU-244: 44974597 keV 17 PU-242:4654-4995keV PU-239: 5011-5227 keV PU-238: 5375-5566 keV 15 PU-236:5582-5843keV 13 11 Ul 9 I-z :J 7 0 5 c *:;; 3 n <{ PEAK FWHM 0.000 0.000 0.000 47.164 4.969 2386 2786 3190 3598 4011 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8310.24 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.139 0.139 0.3722 100.000 -3.56E-03 0.000 -0.277 0.277 0.5263 99.900 -5.92E-03 0.000 -0.554 0.554 0.7443 99.900 -1.18E-02 185.000 184.723 0.277 0.5263 100.000 3.92E+OO 1.000 0.723 0.277 0.5263 99.900 1.53E-02 6139 6578 7021 7468 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B080.CNF;1728 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W080.CNF;446 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.15E-02 1.11E-01 1.68E-02 4.32E-02 1.04E-01 1.97E-02 4.37E-02 1.19E-01 2.77E-02 8.29E-01 1.03E-01 1.96E-02 5.98E-02 1.03E-01 1.96E-02 1.96-sigma cnt Unc pCi/G 5.14E-02 4.31E-02 4.36E-02 5.67E-01 5.97E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235051_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G +/-0.199 % CHAMBER : 081 DETECTOR S/N : 79996 AVERAGE %EFFICIENCY : 33.0506 AVERAGE %EFF ERROR : 0.6369 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 74.7 +/-8.464 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.2730E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.23 PU-238 5486.00 5470.33 PU-239 5155.00 5118.67 PU-242 4890.00 4864.26 PU-244 4589.00 4546.97 13 PU.244* 4497-4597 keV -PtJ..242: 4654-4995 keV 12 f-PU-239:5011-5227kaV PU-238: 5375-5566 keV 11 !--PU-236: 5582-5843 keV 10 8 -Ul 7 I-6 z --::i 5 0 -s. 4 -1:-3 *::; 2 1 ---I I I I PEAK FWHM 0.000 0.000 0.000 77.280 0.000 , Ill 111 I II I 23 84 2779 3178 3582 3991 440 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8313.82 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.139 0.139 0.3722 100.000 -4.41E-03 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 0.000 -0.554 0.554 0.7445 99.900 -1.46E-02 151.000 149.891 1.109 1.0529 100.000 3.93E+OO 0.000 -0.277 0.277 0.5264 99.900 -7.28E-03 111\1 I I I I I 4823 5: 46 673 6106 6543 6985 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B081.CNF;1734 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W081.CNF;446 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.38E-02 1.37E-01 2.08E-02 5.25E-02 7.93E-02 O.OOE+OO 5.41E-02 1.47E-01 3.43E-02 9.22E-01 1.76E-01 4.85E-02 5.31E-02 1.27E-01 2.43E-02 1.96-sigma cnt Unc pCi/G 6.36E-02 5.23E-02 5.39E-02 6.34E-01 5.29E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235052 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 082 DETECTOR S/N : 79997 AVERAGE %EFFICIENCY : 31.9848 AVERAGE %EFF ERROR : 0.6168 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 68.6 +/-8.975 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.0072E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5821.05 PU-238 5486.00 5470.33 PU-239 5155.00 5118.67 PU-242 4890.00 4861.94 PU-244 4589.00 4501.82 13 PlJ.244: 44974597 keV PlJ.242:4654-4995keV 12 PU-239:5011-5227keV PU-238:5375-5566keV 11 PU-236: 5582-5843 keV 10 9 8 (ii 7 I-6 z :J 5 0 4 2:-3 *:; 2 n <t: 1 2394 2787 3185 3588 Energy (keV) PEAK FWHM 4.883 0.000 0.000 51.270 4.883 3996 440 COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8317.64 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.584 0.416 0.6449 100.000 2.06E-02 0.000 -0.693 0.693 0.8325 99.900 -2.04E-02 0.000 -2.357 2.357 1.5351 99.900 -6.88E-02 135.000 133.336 1.664 1.2898 100.000 3.89E+OO 1.000 0.861 0.139 0.3723 99.900 2.51E-02 ll ! 4826 5 4 676 6108 6545 6987 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B082.CNF;1724 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W082.CNF;423 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.00E-01 1.86E-01 4.00E-02 6.10E-02 1.74E-01 4.29E-02 6.66E-02 2.45E-01 7.86E-02 9.66E-01 2.19E-01 6.60E-02 8.18E-02 1.26E-01 1.91E-02 1.96-sigma cnt Unc pCi/G 9.98E-02 6.08E-02 6.63E-02 6.67E-01 8.16E-02

>-1:) 0\ Vl \0 0 ...., Vl 00 0 \0 BATCH NUMBER : 1596412 SAMPLE ID : S0405235053 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 089 DETECTOR S/N : 79988 AVERAGE %EFFICIENCY : 29.2461 AVERAGE %EFF ERROR : 0.5651 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 83.8 +/-8.522 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.671 OE+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5689.75 PU-238 5486.00 5464.90 PU-239 5155.00 5111.91 PU-242 4890.00 4887.02 PU-244 4589.00 4538.81 12 PU-244: 4497-4597 keV PU-242: 45544995 keV 11 PU-239:5011-5227keV PU-238:5375-S566keV 10 PU.236: ssaz-5843 1tev 9 8 7 6 z 5 ::> 0 4 s 3 *:;: 2 2394 2791 3193 3598 Energy (keV) PEAK FWHM 158.029 103.707 118.522 76.957 83.953 COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8465.80 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 -2.092 4.092 2.0228 100.000 -6.64E-02 4.000 2.871 1.129 1.0624 99.900 7.54E-02 2.000 0.307 1.693 1.3012 99.900 8.01E-03 156.000 151.485 4.515 2.1249 100.000 3.95E+OO 3.000 2.012 0.988 0.9938 99.900 5.25E-02 >> 'i 'i 'i ll 6110 6543 6980 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B089.CNF;1433 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W089.CNF;384 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.18E-01 3.21E-01 1.13E-01 1.18E-01 1.77E-01 4.90E-02 9.24E-02 1.98E-01 5.97E-02 9.32E-01 2.73E-01 9.73E-02 1.05E-01 1.69E-01 4.56E-02 1.96-sigma cnt Unc pCi/G 1.18E-01 1.17E-01 9.23E-02 6.42E-01 1.04E-01 BATCH NUMBER : 1596412 SAMPLE ID : S0405235054 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 090 DETECTOR S/N : 78263 AVERAGE %EFFICIENCY : 33.4344 AVERAGE %EFF ERROR : 0.6443 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 76.0 +/-8.237 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3314E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4876.09 PU-244 4589.00 4565.61 12 PU-244: 4497-4597 keV PU-242: 4654-4995 keV 11. PU-2J9:5011*5227keV PU-238: 5375-5566 keV 10 PU-236:5582-5843keV 9 8 en 7 I-6 z 5 :J 0 4 3 *:;: 2 t5 <!'. 1 2398 2796 3199 Energy (keV) PEAK FWHM 0.000 0.000 0.000 89.071 4.948 COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8495.79 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.425 0.425 0.6518 100.000 -1.29E-02 0.000 -0.283 0.283 0.5322 99.900 -7.14E-03 0.000 -0.283 0.283 0.5322 99.900 -7.10E-03 158.000 157.717 0.283 0.5322 100.000 3.95E+OO 1.000 0.858 0.142 0.3763 99.900 2.15E-02 >> > 6145 6584 7028 7476 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B090.CNF;1438 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) :

60000.00 EFF FILE : W090.CNF;374 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.23E-02 1.61E-01 3.49E-02 5.11E-02 1.23E-01 2.36E-02 5.07E-02 1.22E-01 2.34E-02 9.01E-01 1.22E-01 2.34E-02 7.03E-02 1.08E-01 1.66E-02 1.96-sigma cnt Unc pCi/G 6.21E-02 5.09E-02 5.06E-02 6.19E-01 7.02E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235055 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 091 DETECTOR S/N : 78259 AVERAGE %EFFICIENCY : 34.7245 AVERAGE %EFF ERROR : 0.6687 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST: HAKB % YIELD : 64.1 +/-8.794 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.8085E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5470.34 PU-239 5155.00 5180.03 PU-242 4890.00 4864.81 PU-244 4589.00 4583.70 14 PU-244: 4497-4597 keV PU-242: 45544995 keV 13 PU-239:5011-5227keV 12 PlJ.238:537S-5566keV PlJ.236: 5582-5843 keV 11 10 9 'iii 8 1--7 z 6 ::i 0 5 s 4 3 *;;; ti 2 <t: 1 2382 2779 3180 Energy (keV) PEAK FWHM 0.000 0.000 4.930 40.262 4.930 COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8499.46 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.708 0.708 0.8416 100.000 -2.42E-02 0.000 -0.708 0.708 0.8416 99.900 -2.00E-02 1.000 -0.558 1.558 1.2483 99.900 -1.57E-02 139.000 138.150 0.850 0.9219 100.000 3.87E+OO 1.000 0.858 0.142 0.3764 99.900 2.41E-02 ! !! !! > S;S;;?; 683 6116 6553 6996 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B091.CNF;1436 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W091.CNF;363 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.10E-02 2.03E-01 5.04E-02 5.88E-02 1.68E-01 4.18E-02 8.25E-02 2.07E-01 6.15E-02 9.43E-01 1.75E-01 4.54E-02 7.87E-02 1.21E-01 1.86E-02 1.96-sigma cnt Unc pCi/G 7.07E-02 5.86E-02 8.23E-02 6.50E-01 7.85E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235056 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 092 DETECTOR S/N : 80063 AVERAGE %EFFICIENCY : 30.3421 AVERAGE %EFF ERROR : 0.5858 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 98.2 +/-7.671 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.3056E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5708.47 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4876.40 PU-244 4589.00 4528.02 15 PU-244:4497-4597 keV PU-242; 4654-4995 keV PU-239: 5011-5227 keV 13 PlJ.236: 5375-5566 keV PlJ..236: 5582-5843 keV 11 UJ 9 I-7 z :::J 0 5 3 *:;; 2406 Energy (keV) PEAK FWHM 4.922 0.000 0.000 50.204 4.922 COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8503.81 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 1.000 0.000 0.0000 100.000 2.55E-02 0.000 -0.992 0.992 0.9960 99.900 -2.09E-02 0.000 -0.850 0.850 0.9222 99.900 -1.78E-02 187.000 185.158 1.842 1.3574 100.000 3.88E+OO 4.000 3.717 0.283 0.5324 99.900 7.79E-02 ni :;;:;; § :111 :2::l 6129 6565 7005 7449 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B092.CNF;1440 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W092.CNF;414 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.11E-02 7.65E-02 O.OOE+OO 4.47E-02 1.37E-01 3.69E-02 4.40E-02 1.31E-01 3.40E-02 8.24E-01 1.63E-01 5.00E-02 9.32E-02 1.02E-01 1.96E-02 1.96-sigma cnt Unc pCi/G 7.10E-02 4.46E-02 4.39E-02 5.63E-01 9.25E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235057 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 093 DETECTOR S/N : 33206 AVERAGE %EFFICIENCY : 33.0892 AVERAGE %EFF ERROR : 0.6377 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 78.6 +/-8.140 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4468E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 14 PU244*44974597keV PU-242:4654-4995keV 13 12 11 10 9 8 7 6 5 4 3 2 1 --------PlJ.239:5011*5227keV PU-238:5375-5566keV PU*236: 5582*5843 keV I I PEAK ENERGY 5708.26 5470.35 5164.40 4914.26 4496.21 I I I PEAK FWHM 0.000 0.000 4.969 58.384 0.000 I II I 24 07 2806 3210 3617 4029 44*4 -Energy (keV) COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8507.47 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.291 0.709 0.8420 100.000 3.84E-02 0.000 -0.851 0.851 0.9224 99.900 -2.09E-02 1.000 0.433 0.567 0.7531 99.900 1.06E-02 162.000 161.716 0.284 0.5325 100.000 3.95E+OO 2.000 1.858 0.142 0.3766 99.900 4.54E-02 ': 111!1 I I I I 4863 Et28B 6145 6580 7019 7462 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B093.CNF;1429 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W093.CNF;379 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.03E-01 1.77E-01 4.40E-02 5.17E-02 1.54E-01 3.99E-02 6.95E-02 1.38E-01 3.24E-02 8.90E-01 1.19E-01 2.29E-02 8.39E-02 1.06E-01 1.62E-02 1.96-sigma cnt Unc pCi/G 1.03E-01 5.15E-02 6.94E-02 6.11E-01 8.35E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235058 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 095 DETECTOR S/N : 38626 AVERAGE %EFFICIENCY : 30.4247 AVERAGE %EFF ERROR : 0.5873 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 76.2 +/-8.565 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3404E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5725.89 PU-238 5486.00 5436.95 PU-239 5155.00 5144.38 PU-242 4890.00 4871.52 PU-244 4589.00 4517.34 PU*244: 4497-4597 keV 15 PU*242:4654-4995keV PU-239:5011*5227keV PlJ..238:537S-S566keV 13 PU-236: S58Z-584J keV 11 UJ 9 I-z 7 ::i 0 5 *:;; 3 2380 2781 3186 Energy (keV) PEAK FWHM 4.993 4.993 4.993 74.066 4.993 COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8560.38 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.144 0.856 0.9252 100.000 4.66E-03 1.000 0.429 0.571 0.7554 99.900 1.15E-02 2.000 1.429 0.571 0.7554 99.900 3.81E-02 145.000 145.000 0.000 0.0000 100.000 3.86E+OO 1.000 1.000 0.000 0.0000 99.900 2.66E-02 l ll > ll 6125 6559 6997 7439 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B095.CNF;1405 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W095.CNF;408 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.30E-02 2.02E-01 5.26E-02 7.63E-02 1.52E-01 3.56E-02 9.21E-02 1.51E-01 3.54E-02 9.15E-01 7.98E-02 O.OOE+OO 7.43E-02 7.99E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 9.28E-02 7.61E-02 9.19E-02 6.30E-01 7.42E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235059 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 096 DETECTOR S/N : 80016 AVERAGE %EFFICIENCY : 32.5188 AVERAGE %EFF ERROR : 0.6269 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 72.5 +/-8.515 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.1763E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 13 12 PU.239:5011-5227keV PU-238: 5375-5566 keV 11 PU-236: 5582-5843 keV 10 9 8 7 6 5 4 3 2 2391 2788 3189 Energy (keV) 5756.61 5414.05 5118.69 4878.73 4517.50 PEAK FWHM 4.934 4.934 0.000 70.307 4.934 COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8564.06 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 1.000 0.286 0.714 0.8448 100.000 9.19E-03 1.000 0.572 0.428 0.6544 99.900 1.53E-02 0.000 -0.428 0.428 0.6544 99.900 -1.14E-02 148.000 147.429 0.571 0.7556 100.000 3.93E+OO 1.000 0.429 0.571 0.7556 99.900 1.14E-02 ll ii 687 6118 6554 6994 7438 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B096.CNF;1397 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W096.CNF;357 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.18E-02 1.92E-01 4.77E-02 7.60E-02 1.42E-01 3.09E-02 5.45E-02 1.41E-01 3.07E-02 9.26E-01 1.51E-01 3.54E-02 7.59E-02 1.51E-01 3.54E-02 1.96-sigma cnt Unc pCi/G 9.16E-02 7.58E-02 5.43E-02 6.37E-01 7.57E-02 BATCH NUMBER : 1596412 SAMPLE ID : S0405235060 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 097 DETECTOR S/N : 83288 AVERAGE %EFFICIENCY : 35.3557 AVERAGE %EFF ERROR : 0.6805 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 92.2 +/-7.310 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.0407E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4882.92 PU-244 4589.00 4546.97 PU-244: 4497-4597 keV 17 PU-242: 46544995 keV PU-239:5011-S227keV PU-238:5375-5566keV 15 PU-236:5582-5843keV 13 11 0' 9 z :J 7 0 5 .?;-*:;: 3 t5 <i: 2402 2798 3198 3603 Energy (keV) PEAK FWHM 0.000 0.000 0.000 59.932 0.000 4012 COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8567.84 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.286 0.286 0.5344 100.000 -6.47E-03 0.000 -0.571 0.571 0.7558 99.900 -1.08E-02 0.000 -0.428 0.428 0.6545 99.900 -8.06E-03 205.000 204.000 1.000 0.9998 100.000 3.83E+OO 0.000 -0.143 0.143 0.3779 99.900 -2.69E-03 i 3'1 ::si:g 5 6 688 6118 6551 6989 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B097.CNF;1394 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W097.CNF;381 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.59E-02 1.11E-01 2.13E-02 3.90E-02 1.07E-01 2.52E-02 3.84E-02 9.97E-02 2.17E-02 7.76E-01 1.22E-01 3.30E-02 3.77E-02 8.14E-02 1.25E-02 1.96-sigma cnt Unc pCi/G 4.57E-02 3.89E-02 3.83E-02 5.29E-01 3.76E-02 BATCH NUMBER : 1596412 SAMPLE ID : S1203621751_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G +/-0.194 % CHAMBER : 099 DETECTOR S/N : 80059 AVERAGE %EFFICIENCY : 35.6284 AVERAGE %EFF ERROR : 0.6858 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 85.7 +/-7.528 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.7576E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5413.43 PU-239 5155.00 5118.67 PU-242 4890.00 4878.90 PU-244 4589.00 4511.04 17 PU 244* 44974597 keV PU-242:4654-4995keV PU-239:5011-5227keV 15 -PU-238: 5375-5566 keV PU-236; 5582*5843 keV 13 g r z => 7 r 0 8 5 r *:;; 3 t5 f-<( f-I I I PEAK FWHM 0.000 4.881 0.000 61.418 24.405 1111 II I I 24 02 2795 3193 3595 4001 4413 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8572.83 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.857 0.857 0.9259 100.000 -1.72E-02 1.000 0.428 0.572 0.7560 99.900 8.60E-03 0.000 -0.286 0.286 0.5346 99.900 -5.73E-03 192.000 191.286 0.714 0.8452 100.000 3.83E+OO 2.000 2.000 0.000 0.0000 99.900 4.01E-02 11111 II I I I I I I 4829 5 4£ 674 6104 6539 6978 7421 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B099.CNF;1397 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W099.CNF;383 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.22E-02 1.26E-01 3.27E-02 5.71E-02 1.14E-01 2.67E-02 4.06E-02 9.79E-02 1.89E-02 7.99E-01 1.20E-01 2.98E-02 6.86E-02 6.02E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.21E-02 5.70E-02 4.05E-02 5.46E-01 6.83E-02 BATCH NUMBER : 1596412 SAMPLE ID : S1203621752 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.511 G -+/-0.196 % CHAMBER : 103 DETECTOR S/N : 79461 AVERAGE %EFFICIENCY : 33.8848 AVERAGE %EFF ERROR : 0.6527 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 73.5 +/-8.243 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.2203E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4851.52 PU-244 4589.00 4546.97 14 PU*244: 4497-4597 keV PU.242:4654-4995keV 13 PU-239: 5011*5227 keV 12 PU*238;5375-5566keV PU-236: 5582-5843 keV 11 10 9 en 8 I-7 z 6 :::> 0 5 8 4 .?;-3 *:;: 2 1 2380 2779 3182 3590 Energy (keV) PEAK FWHM 0.000 0.000 0.000 78.116 0.000 COUNT DATE : 22-Sep-2016 09:56:16 ELAPSED LIVE TIME(SEC) : 8694.85 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.290 0.290 0.5384 100.000 -8.63E-03 0.000 -0.290 0.290 0.5384 99.900 -7.13E-03 0.000 -0.145 0.145 0.3807 99.900 -3.54E-03 159.000 158.131 0.869 0.9325 100.000 3.86E+OO 0.000 -0.145 0.145 0.3807 99.900 -3.54E-03 6123 6560 7001 7446 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B103.CNF;1412 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W103.CNF;395 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.04E-02 1.46E-01 2.82E-02 4.99E-02 1.21E-01 2.33E-02 4.91E-02 1.06E-01 1.64E-02 8.82E-01 1.54E-01 4.01E-02 4.91E-02 1.06E-01 1.64E-02 1.96-sigma cnt Unc pCi/G 6.02E-02 4.97E-02 4.89E-02 6.06E-01 4.89E-02 BATCH NUMBER : 1596412 SAMPLE ID : S1203621753 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 104 DETECTOR S/N : 80011 AVERAGE %EFFICIENCY : 32.4069 AVERAGE %EFF ERROR : 0.6248 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 69.6 +/-8.637 % TRACER ID 1770-A NUCLIDE PU-242 NOMINAL 4.3831E+OO dpm RESULTS 3.0494E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5467.79 PU-239 5155.00 5125.46 PU-242 4890.00 4858.49 PU-244 4589.00 4549.30 15 PlJ.244: 4497-4597 keV PlJ.242:4854-4995keV PU-239: 5011-5227 keV 13 PU-238:5375-5566keV PU-236; 5582-5843 keV 11 en 9 I-7 z ::::> 0 5 s 3 *:; n <i: 2380 2776 3176 3581 Energy (keV) PEAK FWHM 0.000 127.893 41.304 72.555 73.784 COUNT DATE : 22-Sep-2016 09:56:16 ELAPSED LIVE TIME(SEC) : 8698.89 LCS JD 0338-MM NUCLIDE PU-239 NOMINAL (pCi/G) 3.8370E+OO % RECOVERY 113.176 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.580 0.580 0.7615 100.000 -1.55E-02 3.000 2.710 0.290 0.5385 99.900 7.26E-02 163.000 162.130 0.870 0.9327 99.900 4.34E+OO 144.000 143.275 0.725 0.8514 100.000 3.83E+OO 4.000 3.710 0.290 0.5385 99.900 9.94E-02 m; 6110 6548 6991 7438 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B104.CNF;1397 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W104.CNF;386 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.54E-02 1.52E-01 3.59E-02 1.07E-01 1.31E-01 2.54E-02 1.01E+OO 1.68E-01 4.40E-02 9.17E-01 1.60E-01 4.01E-02 1.19E-01 1.31E-01 2.54E-02 1.96-sigma cnt Unc pCi/G 5.52E-02 1.06E-01 6.73E-01 6.32E-01 1.18E-01 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Product: ___ ___ _ Date: Criteria: Yes No Comments sample Solids are less than or eaual to 100 mq for GAB. u:.r Samples have been blank corrected (If required). Blank correction reoorted Included Clf reaulredl. If activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. ./ If greater than 10* MDA/ MDC, error Is 40% or less. :If h1>ln..., thA Mn.a I Mnr <>rrnr Is""'"' Instrument source check Is within limits. Instr"""'nt bkn check Is within limits. v Method RDL/ LLD has been met. v If duplicate activities are: Less than 5"' MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, / If below the MDA/ MDC, the RPO Is 0%, Or meets the client's renulred RER acceotance criteria. Tracer yield Is 15-1250/o
Carrier yield 25-125%. ,/ (Or meets the client's contract acceptance criteria). Method blank is less than the RDL/ LLD. f' frf _., ----*--.,. 11;;01. of*-.. **-* ,..-tlvltv\ Sample was run within hold time. ...,,r 1:)0l% \ Samele was correctlv oreserved if reouired. w--Smears Taken for Radioactive batches. i\P--Method Spike and LCS are within 75-125% v lfnr -nn*e th" client'" cont.,.,... "C"entance "rlterlal. No blank spaces on data forms. All line outs Initialed and dated. ./ INn <>rrnre "n Aux data Is correct. j\JQ, Client Soeclai reouirements oaoe has been checked. ../ Raw Data and/ or spectrum are included and orooerlv statused. ,/ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and .,/ -values v<>rjfl<>rl Hit (If-*\ D*>-h *-*--.I I->* r---,/ Batch Data Exception Reports (DER) comoleted if aoPlicable. ,/ 'J)._-Q\\-\ SL,?.:> "l \1..-Batch Data Exception Reports (Dl'R) second reviewed. v lS DisPosltion verified to be comoleted. 'Aliouot Corr<>,.,.lnn comole><>rl If reoulred. l\..Q---Review sample historical results if available / (If Rl'MP, results above MDC have been verified bv historical results recount or re-analvsls. l Primary Review Performed By: __ _____ _ Secondary Review Performed By:_ 09/30/16 @ Page ffiso9 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 30-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER ASTM C 1475-00 Modified Solid Batch ID: Sample Numbers: 1596399 See Below Potentially affected work order(s)(SDG):405235 Application Issues: RDL less than MDA Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, and 1203621716 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 30-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 671 of 5809 DER Report No.: 1563212 Revision No.: Type: Process Client Code: MJWC '

Neptunium Queue Sheet -------------------* Batch #: 1596399 Analyst: MXS2 First Client Due Date:04-0CT-16 Internal One nate30-SEP-16 Tracer Isotope: Am-243 (Np-239) LCS Isotope: Np-237 Spike Isotope: Np-237 Prep Date: 9-?,.,l-ftr Initials: Tracer Code: l.ftl?-t/lr z, '.111f:xpiration Date: 'f-30-1 V. Vol: O* I LCS Code: 05 )g-S Expiration Date: /-1g-17 Vol: o. J Spike Code: Y..51> Pipet ID: Expiration Date: 1 'iSt1 Q)Z,.1;-_-____ Vol: -Balance ID: llPt07eo(fQ...,-Np Separation Dateffime: 07-SEP-16 Routine#:. r-REF #: "12-93 BKG#: '71 q-z.z..-((p /z,o *. cS I __ _ Hazard Min Sample ID Client Description 1Jr_pc Code CRDL Matrix we@ GFPC Collection <;:lient __ __Date ___ Label# N11Det# 405235021-1 4.2B.R.2.3 405235022-1 4.2B.R.1.3 405235023-1 4.2B.R.l 1.2 405235024-1 4.2B.R.2.2 405235025-1 4.2B.R.1.2 405235026-1 4.2C.R.1.3 405235027-1 4.2C.R.1A 405235028-1 4.3.ARl.3 405235029-1 4.3.B.R.1.3 405235030-1 4.JA.R.2.3 405235031-1 4.3.BR19.2 405235032-1 4.JB.R.3.3 405235033-1 4.38.R.3.4 405235034-1 4.3.B.R.1.4 405235035-1 4.JB.R.2.3 405235036-1 4.JB.R.2.4 405235037-1 4.4C.R.2A 405235038-1 4.4C.R.l.3 405235039-1 MC.R.1.4 405235040-1 4AD.R.1.3 1203621715-1 MB for batch 1596399 1203621716-1 4.2B.R.2.3(405235021DUP) 1203621717-1 LCS for batch 1596399 SAMPLE 1 pCilg SOIL l'rUWCOOl SAMPLE 1 pCilg SOIL MJWCOOI SAMPLE 1 pCi/g SOIL M.TWCOOl SAMPLE 1 pCilg SOIL MJWCOOl SAMPLE 1 pCilg SOIL M.TWCOOl SAi'\fl>LE 1 pCilg SOIL 1\UWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCilg SOIL MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCilg SOIL MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL :MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL l\>UWCOOl SAl'rfPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL MJWCOOl SAMPLE 1 pCi/g SOIL l\IJWCOOl l'rIB 1 pCi/g SOIL QC ACCOUNT DUP 1 pCi/g SOIL QC ACCOUNT LCS 1 pCilg SOIL QCACCOID<'T Solid Sample Dissolmion by: DIGESTION Circle One GEL Laboratories LLC, Radiochemistry Division 08-DEC-15 1 z.; 08-DEC-15 2 'Z.{; 02-DEC-15 3 08-DEC-15 4 08-DEC-15 5 OS-DEC-15 6 08-DEC-15 7 23-NOV-15 s 23-NOV-15 9 23-NOV-15 10 26-NOV-15 11 23-NOV-15 12 23-NOV-15 13 23-NOV-15 14 23-NOV-15 15 23-NOV-15 16 30-NOV-15 17 30-NOV-15 18 30-NOV-15 19 30-NOV-15 20 21 08-DEC-15 22 23 Data By: Page 1 of 1 NP1596399 Pago 1 Page 673 of 5809 BATCH NUMBER : 1596399 SAMPLE ID : S0405235021_NP SAMPLE QTY : 0.115 G +/-0.870 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 93.0 +/-5.215 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 185 DETECTOR S/N : 68615 AVERAGE %EFFICIENCY : 25.3535 AVERAGE %EFF ERROR : 0.4915 COUNTDATE: 26-Sep-201617:11:18 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 4.1513E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4781.62 1 NP 237' 4430-4922 keV 23 80 2781 3186 3594 Energy (keV) PEAK FWHM 4.991 I 4006 44'1 GROSS AREA 1.000 I NUCLIDE ACTIVITY SUMMARY NET AREA -0.320 I 5262 BKG AREA 1.320 I 5687 BKG StDev 1.1489 %ABUN 100.000 I I 6117 6549 6986 ACTIVITY pCi/G -4.43E-02 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B185.CNF;859 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W185.CNF;237 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.00E-01 MDA pCi/G 9.69E-01 Le pCi/G 2.77E-01 1.96-sigma cnt Unc pCi/G 4.00E-01 AlphaSpectroscopySoftwareVerslon3.5.3 effedlvedate:02-Mar-2015 BATCH NUMBER : 1596399 SAMPLE ID : S0405235022 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 186 DETECTOR S/N : 68616 AVERAGE %EFFICIENCY : 25.3981 AVERAGE %EFF ERROR : 0.4924 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 93.4 +/-5.215 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-201617:11:20 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 4.1660E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4742.00 2 NP 237* 4430-4922 keV -I I I 23 95 2794 3198 3604 Energy (keV) PEAK FWHM 144.228 I 4014 44J8 GROSS AREA 3.000 I 484p NUCLIDE ACTIVITY SUMMARY NET AREA 1.560 I 5265 BKG AREA 1.440 I 5689 BKG StDev 1.2000 I %ABUN 100.000 I 6117 6548 6982 ACTIVITY pCi/G 2.27E-01 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B186.CNF;819 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W186.CNF;28 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 5.83E-01 MDA pCi/G 1.04E+OO Le pCi/G 3.03E-01 1.96-sigma cnt Unc pCi/G 5.82E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235023 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.115 G -+/-0.870 % CHAMBER : 188 DETECTOR S/N : 68621 AVERAGE %EFFICIENCY : 26.7276 AVERAGE %EFF ERROR : 0.5175 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 85.3 +/-5.253 % TRACER . ID 445-96-2-111 COUNT DATE : 26-Sep-2016 17:11 :23 ELAPSED LIVE TIME(SEC) : 7200.00 NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.8055E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4613.29 1 ....-NP 237* 4430-4922 keV PEAK FWHM 4.861 GROSS AREA 1.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.080 BKG AREA 1.080 BKG StDev 1.0392 %ABUN 100.000 ACTIVITY pCi/G -1.15E-02 I I I I I I I I I I I 2429 2820 3215 3615 4019 484 5258 5680 6106 6537 6972 7411 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B188.CNF;854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W188.CNF;233 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.11E-01 MDA pCi/G 9.48E-01 Le pCi/G 2.59E-01 1.96-sigma cnt Unc pCi/G 4.11E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235024 NP SAMPLE QTY : 0.103 G -+/-0.971 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 81.8 +/-5.272 % COUNT DATE : 26-Sep-2016 17:11 :25 ELAPSED LIVE TIME(SEC) : 7200.00 TRACER ID NUCLIDE NOMINAL RESULTS 445-96-2-111 . AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.6512E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.26 1 NP 237* 4430-4922 keV I 24 16 2810 3209 3612 Energy (keV) PEAK FWHM 0.000 4020 44t31 GROSS AREA 0.000 I 48417 NUCLIDE ACTIVITY SUMMARY NET AREA -0.720 5266 BKG AREA 0.720 I 5691 BKG StDev 0.8485 I 6119 6551 %ABUN 100.000 6988 ACTIVITY pCi/G -1.26E-01 7429 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B189.CNF;855 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.61E-01 MDA pCi/G 1.04E+OO Le pCi/G 2.59E-01 1.96-sigma en! Une pCi/G 3.60E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235025 NP SAMPLE QTY : 0.105 G -+/-0.952 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 78.6 +/-5.292 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 195 DETECTOR S/N : 78786 AVERAGE %EFFICIENCY : 26.3844 AVERAGE %EFF ERROR : 0.5110 COUNTDATE: 26-Sep-201617:11:27 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.5079E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.33 1 NP 237* 4430-4922 keV I I 23 93 2792 3195 3601 Energy (keV) I PEAK FWHM 0.000 4012 GROSS AREA 0.000 I 484i NUCLIDE ACTIVITY SUMMARY NET AREA -0.600 I 5266 BKG AREA 0.600 I 5692 BKG S!Dev 0.7746 6122 6556 %ABUN 100.000 I 6993 ACTIVITY pCi/G -1.03E-01 I 7435 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B195.CNF;880 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W195.CNF;259 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.53E-01 MDA pCl/G 9.82E-01 Le pCi/G 2.32E-01 1.96-sigma cnt Unc pCi/G 3.52E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235026 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 069 DETECTOR S/N : 78795 AVERAGE %EFFICIENCY : 32.9662 AVERAGE %EFF ERROR : 0.6355 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 86.3 +/-5.252 % TRACER 445-96-2-111 COUNT DATE : 29-Sep-2016 14:05:23 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 4.4615E+02 dpm 3.8483E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4762.78 r-N?-2: 7:443Q-4922ke I I I 24 04 2802 3206 3614 Energy (keV) PEAK FWHM 4.959 I 4026 4*42 GROSS AREA 1.000 I NUCLIDE ACTIVITY SUMMARY NET AREA 0.040 I 5288 BKG AREA 0.960 I 5718 BKG StDev 0.9798 I I 6152 6591 %ABUN 100.000 I 7034 ACTIVITY pCi/G 2.44E-03 I 7481 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B069.CNF;1823 BKG DATE : 25-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W069.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU pCi/G 1.81E-01 MDA pCi/G 4.03E-01 Le pCi/G 1.10E-01 1.96-sigma cnt Unc pCi/G 1.81E-01 AlphaSpectrosoopySoftwareVersion3.5,3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596399 SAMPLE ID : S0405235027 NP SAMPLE QTY : 0.117 G -+/-0.855 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 199 DETECTOR S/N : 78896 AVERAGE %EFFICIENCY : 26.2038 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 68.4 +/-5.364 % COUNT DATE: 26-Sep-201617:11:32 ELAPSED LIVE TIME(SEC) : 7200.00 TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE NP-237 445-96-2-111 ' AM-243 BETA %EFF.: 48.42148 4.4615E+02 dpm 3.0506E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4497.59 PEAK FWHM 4.962 GROSS AREA 1.000 1 -NP 237: 4430-4922 keV NUCLIDE ACTIVITY SUMMARY NET AREA 0.400 BKG AREA 0.600 BKG S!Dev 0.7746 %ABUN 100.000 I I I I I I I I I ACTIVITY pCi/G 7.16E-02 2377 2776 3178 3585 3995 44 19 482 5249 5674 6103 6537 6974 7414 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B199.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W199.CNF;222 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 5.07E-01 MDA pCi/G 1.02E+OO Le pCi/G 2.41E-01 1.96-sigma cnt Unc pCi/G 5.07E-01 0 ....., u, 00 0 \0 BATCH NUMBER : 1596399 SAMPLE ID : S0405235028 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 200 DETECTOR S/N : 78900 AVERAGE %EFFICIENCY : 27.0654 AVERAGE %EFF ERROR : 0.5238 SAMPLE DATE : 23-Nov-2015*00:00:00 ANALYST : MXS2 % YIELD : 87.3 +/-5.250 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:11 :35 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.8965E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.29 1 _ NP-237: 4430-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.600 BKG AREA 0.600 BKG Stoev 0.7746 %ABUN 100.000 ACTIVITY pCi/G -8.74E-02 I I I I I I I I I I I 2394 2791 3191 3596 4005 44 8 483 p 5256 5681 6111 6544 6982 7423 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B200.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W200.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.98E-01 MDA pCi/G 8.30E-01 Le pCi/G 1.96E-01 1.96-sigma cnt Unc pCi/G 2.98E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235029 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 201 DETECTOR SIN : 78902 AVERAGE %EFFICIENCY : 26.2326 AVERAGE %EFF ERROR : 0.5081 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 82.0 +/-5.278 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:11 :37 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 4.4615E+02 dpm 3.6607E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4675.31 1 NP 237* 4430-4922 keV I I I 23 75 2773 3175 3582 Energy {keV) I PEAK FWHM 0.000 I 3992 44 6 GROSS AREA 0.000 I 482: NUCLIDE ACTIVITY SUMMARY NET AREA -0.480 I 5247 BKG AREA 0.480 I 5673 BKG StDev 0.6928 %ABUN 100.000 I I 6103 6537 6975 ACTIVITY pCi/G -7.90E-02 7417 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B201.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W201.CNF;224 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.34E-01 MDA pCi/G 8.90E-01 Le pCi/G 1.98E-01 1.96-sigma cnt Unc pCi/G 3.34E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235030 NP SAMPLE QTY : 0.101 G -+/-0.990 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 69.6 +/-5.359 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 202 DETECTOR S/N : 78903 AVERAGE %EFFICIENCY : 27.2753 AVERAGE %EFF ERROR : 0.5278 COUNT DATE : 26-Sep-201617:11:40 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.1054E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.30 -1 NP 237* 4430-4922 keV I I I 23 78 2777 3180 3587 Energy (keV) I PEAK FWHM 0.000 3998 44 M GROSS AREA 0.000 I 483 p NUCLIDE ACTIVITY SUMMARY NET AREA -0.840 I 5256 BKG AREA 0.840 I 5683 BKG StDev 0.9165 I I %ABUN 100.000 I 6115 6550 6990 ACTIVITY pCi/G -1.64E-01 I 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B202.CNF;799 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W202.CNF;226 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.06E-01 MDA pCi/G 1.21E+OO Le pCi/G 3.12E-01 1.96-sigma cnt Unc pCl/G 4.05E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235031_NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G +/-0.943 % CHAMBER : 203 DETECTOR S/N : 78905 AVERAGE %EFFICIENCY : 25.9071 AVERAGE %EFF ERROR : 0.5020 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.4 +/-5.248 % TRACER 445-96-2-111 . COUNT DATE : 26-Sep-201617:11:43 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 4.4615E+02 dpm 3.9455E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4675.31 -1 NP rn*4430-4922keV I I I 23 69 2767 3170 3576 Energy (keV) I PEAK FWHM 0.000 3987 44 GROSS AREA 0.000 I 482( NUCLIDE ACTIVITY SUMMARY NET AREA -0.480 I 5242 BKG AREA 0.480 I 5668 BKG S!Dev 0.6928 I I 6099 6533 %ABUN 100.000 I 6972 ACTIVITY pCi/G -7.42E-02 I 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B203.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W203.CNF;229 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.14E-01 MDA pCi/G 8.37E-01 Le pCi/G 1.86E-01 1.96-sigma cnt Unc pCi/G 3.14E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235032 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 161 DETECTOR S/N : 70321 AVERAGE %EFFICIENCY : 25.7727 AVERAGE %EFF ERROR : 0.4995 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 86.8 +/-5.258 % TRACER .445-96-2-111 COUNT DATE : 26-Sep-2016 17:09:37 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.8709E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.31 1 _ NP 237* 4430-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.360 BKG AREA 0.360 BKG S!Dev 0.6000 %ABUN 100.000 ACTIVITY pCi/G -5.81E-02 I I I I I I I I I I I 2394 2792 3193 3599 4008 4122 5261 5686 6115 6548 6986 7427 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B161.CNF;860 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W161.CNF;261 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.26E-01 MDA pCi/G 8.21E-01 Le pCi/G 1.69E-01 1.96-sigma cnt Unc pCi/G 3.25E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235033 NP SAMPLE QTY : 0.108 G -. +/-0.926 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 89.6 +/-5.246 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 162 DETECTOR S/N : 70323 AVERAGE %EFFICIENCY : 26.6669 AVERAGE %EFF ERROR : 0.5165 COUNT DATE : 26-Sep-2016 17:09:39 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.9965E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4838.90 1 NP 237* 4430-4922 keV I I I 23 83 2782 3184 3590 Energy (keV) I PEAK FWHM 4.961 3999 44 2 GROSS AREA 1.000 482 NUCLIDE ACTIVITY SUMMARY NET AREA 0.880 I 5248 BKG AREA 0.120 I 5672 BKG StDev 0.3464 I I %ABUN 100.000 I 6099 6530 6964 ACTIVITY pCi/G 1.28E-01 I 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B162.CNF;862 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W162.CNF;260 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 4.07E-01 MDA pCi/G 6.12E-01 Le pCi/G 8.77E-02 1.96-sigma cnt Unc pCi/G 4.06E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235034 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.115G -+/-0.870% CHAMBER : 182 DETECTOR S/N : 74440 AVERAGE %EFFICIENCY : 22.5384 AVERAGE %EFF ERROR : 0.4383 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 81.7 +/-5.287 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:35:29 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.6433E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.39 1 NP 237 4430-4922 k V -' I I I 23 73 2774 3178 3585 Energy (keV) PEAK FWHM 0.000 I 3996 44 1 GROSS AREA 0.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 0.000 I 5251 BKG AREA 0.000 I 5676 BKG StDev 0.0000 I I %ABUN 100.000 I 6104 6537 6972 ACTIVITY pCi/G O.OOE+OO I 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B182.CNF;320 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W182.CNF;95 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.51E-01 MDA pCi/G 5.32E-01 Le pCi/G O.OOE+OO 1.96-sigma en! Une pCi/G 3.50E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235035 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 89.0 +/-5.251 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:09:43 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 4.4615E+02 dpm 3.9690E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4675.31 1 NP 237* 4430-4922 keV I I I 23 83 2781 3184 3590 Energy (keV) I PEAK FWHM 0.000 4000 44n4 GROSS AREA 0.000 I 483 NUCLIDE ACTIVITY SUMMARY NET AREA -0.120 I 5255 BKG AREA 0.120 I 5681 BKG StDev 0.3464 I I %ABUN 100.000 I 6111 6545 6983 ACTIVITY pCi/G -1.84E-02 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B166.CNF;891 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.06E-01 MDA pCi/G 6.46E-01 Le pCi/G 9.26E-02 1.96-sigma cnt Unc pCi/G 3.05E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235036 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 167 DETECTOR S/N : 72546 AVERAGE %EFFICIENCY : 24.1606 AVERAGE %EFF ERROR : 0.4690 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 80.6 +/-5.296 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:09:46 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.5958E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.42 1 NP 237* 44304922 keV I I I 23 78 2780 3185 3594 Energy (keV) PEAK FWHM 0.000 I 4006 GROSS AREA 0.000 I 484D NUCLIDE ACTIVITY SUMMARY NET AREA -0.840 I 5262 BKG AREA 0.840 I 5687 BKG S!Dev 0.9165 I 6116 %ABUN 100.000 I I 6548 6983 ACTIVITY pCilG -1.49E-01 I 7422 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B167.CNF;886 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W167.CNF;246 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCilG 3.67E-01 MDA pCilG 1.09E+OO Le pCilG 2.82E-01 1.96-sigma cnt Unc pCilG 3.66E-01 Npha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596399 SAMPLE ID : S0405235037 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.114 G -+/-0.877 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 86.6 +/-5.265 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:09:48 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.8632E+02 dpm LIBRARY PEAK ENERGY ENERGY 4 788.00 4675.32 1 NP 237 4430-4922 k V . . I I I 24 02 2798 3198 3603 Energy (keV) I PEAK FWHM 0.000 4010 44 22 GROSS AREA 0.000 I NUCLIDE ACTIVITY SUMMARY NET AREA -0.960 I 5257 BKG AREA 0.960 I 5681 BKG StDev 0.9798 6108 6539 %ABUN 100.000 6974 ACTIVITY pCi/G -1.39E-01 I 7413 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B169.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.02E-01 MDA pCi/G 9.30E-01 Le pCi/G 2.47E-01 1.96-sigma cnt Unc pCi/G 3.02E-01 0 ....., Vl 00 0 "' BATCH NUMBER : 1596399 SAMPLE ID : S0405235038 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 170 . DETECTOR S/N : 72549 SAMPLEQTY: 0.117G -+/-0.855% AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 86.4 +/-5.268 % 445-96-2-111 COUNT DATE : 26-Sep-2016 17:09:51 ELAPSED LIVE TIME(SEC) : 7200.00 TRACER , ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.8559E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.32 1 NP 237* 4430-4922 keV -I I I 23 86 2785 3187 3593 Energy (keV) PEAK FWHM 0.000 4004 44 8 GROSS AREA 0.000 I 4831> NUCLIDE ACTIVITY SUMMARY NET AREA -0.600 I 5258 BKG AREA 0.600 I 5683 BKG S!Dev 0.7746 I I %ABUN 100.000 I 6113 6547 6985 ACTIVITY pCi/G -8.66E-02 I 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B170.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.95E-01 MDA pCi/G 8.22E-01 Le pCi/G 1.95E-01 1.96-sigma cnt Unc pCi/G 2.95E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235039 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 95.8 +/-5.226 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:11 :OB ELAPSED LIVE TIME(SEC) : 7200.00 . ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 4.2732E+02 dpm LIBRARY PEAK ENERGY ENERGY 4 788.00 4675.39 1 NP 237* 4430-4922 keV I I I 23 63 2764 3168 3575 Energy (keV) PEAK FWHM 0.000 I I 3986 44 1 GROSS AREA 0.000 I 481! NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 I 5240 BKG AREA 0.240 I 5665 BKG StDev 0.4899 I I %ABUN 100.000 I 6094 6526 6961 ACTIVITY pCi/G -3.32E-02 I 7400 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B175.CNF;870 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.77E-01 MDA pCi/G 6.50E-01 Le pCi/G 1.18E-01 1.96-sigma cnt Unc pCi/G 2.77E-01 BATCH NUMBER : 1596399 SAMPLE ID : S0405235040 NP SAMPLE QTY : 0.112 G -+/-0.893 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 176 DETECTOR S/N : 74434 AVERAGE %EFFICIENCY : 25.6995 AVERAGE %EFF ERROR : 0.4981 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 73.5 +/-5.347 % COUNT DATE : 26-Sep-2016 17:11 :10 ELAPSED LIVE TIME(SEC) : 7200.00 TRACER ID NUCLIDE NOMINAL RESULTS 445-96-2-111 ' AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.2810E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4493.02 1 NP 237* 4430-4922 keV -I 23 79 2776 3177 3582 Energy (keV) PEAK FWHM 83.891 I 3991 44( 5 GROSS AREA 2.000 I 482' NUCLIDE ACTIVITY SUMMARY NET AREA 1.040 5244 BKG AREA 0.960 5670 BKG StDev 0.9798 I %ABUN 100.000 I 6100 6534 6972 ACTIVITY pCi/G 1.84E-01 I 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B176.CNF;865 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 6.15E-01 MDA pCi/G 1.14E+OO Le pCi/G 3.02E-01 1.96-sigma cnt Unc pCi/G 6.15E-01 BATCH NUMBER : 1596399 SAMPLE ID : S1203621715 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.117 G -+/-0.855 % CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 83.4 +/-5.288 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 17:11:13 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 3.7224E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.28 3 NP 237* 4430-4922 k V ' 2 -I I 23 75 2774 3177 3583 Energy (keV) I PEAK FWHM 0.000 I 3994 44 0 GROSS AREA 0.000 I 4829 NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 5253 BKG AREA 0.240 I 5680 I BKG StDev 0.4899 I 6112 6548 %ABUN 100.000 I 6989 ACTIVITY pCi/G -3.47E-02 I 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B177.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.90E-01 MDA pCi/G 6.80E-01 Le pCi/G 1.23E-01 1.96-sigma cnt Unc pCi/G . 2.89E-01 BATCH NUMBER : 1596399 SAMPLE ID : S1203621716 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 070 DETECTOR S/N : 78262 AVERAGE %EFFICIENCY : 31.2964 AVERAGE %EFF ERROR : 0.6038 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 36.9 +/-5.839 % TRACER 445-96"2-lll COUNT DATE : 29-Sep-2016 14:05:23 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 1.6454E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4681.64 1 NP 237* 44304922 keV I I I 23 81 2775 3175 3578 Energy (keV) I PEAK FWHM 4.900 I 3987 441 0 GROSS AREA 1.000 I 4811 NUCLIDE ACTIVITY SUMMARY NET AREA 0.280 I 5241 BKG AREA 0.720 I 5668 BKG StDev 0.8485 I I %ABUN 100.000 I 6100 6537 6978 ACTIVITY pCi/G 4.46E-02 I 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B070.CNF;1825 BKG DATE : 25-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W070.CNF;500 CAL DATE : 03-Sep-2016 1.96-sigma TPU pCi/G 4.67E-01 MDA pCi/G 9.74E-01 Le pCi/G 2.48E-01 1.96-sigma cnt Unc pCl/G 4.67E-01 AlphaSpectrcscopySoftwareVersion3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596399 SAMPLE ID : S1203621717 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.117 G -+/-0.855 % CHAMBER : 180 DETECTOR S/N : 83295 AVERAGE %EFFICIENCY : 26.2740 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 99.3 +/-5.216 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 11 :53:52 ELAPSED LIVE TIME(SEC) : 7200.00 LCS ID 0518-S ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.42148 NUCLIDE NP-237 4.4615E+02 dpm 4.4316E+02 dpm NUCLIDE LIBRARY PEAK c;;-I-z :i 0 c *:;; n <( NP-237 31 28 25 22 19 16 13 10 7 4 ENERGY ENERGY 4788.00 4779.66 NP-237: 44304922 keV 2377 2777 3181 3588 Energy {keV) PEAK FWHM 26.460 4000 44 5 NOMINAL (pCi/G) 3.8166E+01 % RECOVERY 108.434 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 337.000 336.640 0.360 0.6000 100.000 483 5255 5681 6111 6545 6982 ACTIVITY pCi/G 4.14E+01 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B180.CNF;879 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W180.CNF;230 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 6.36E+OO MDA pCi/G 6.26E-01 Le pCi/G 1.28E-01 1.96-sigma cnt Unc pCi/G 4.43E+OO Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 30-Sep-2016 Batch# Product: Criteria: I Yes No Sample Solids are less than or equal to 100 mq for GAB. f\b-Samples have been blank corrected (If required). f\b-Blank correction reoorted lnduded flf reoulred). [f activity less than 10x MDA/MDC, error Is less than or equal to 150o/o of sample activity. [f greater than 10* MDA/ MDC, error Is 40% or less. v [f hAlnU1 th .. Mn.a I Mnt" """r Is okav. Instrument source check Is within limits. Instrument bko check Is within limits. v Method RDL/ LLD has been met. / [f duplicate activities are: Less than 5* MDA/ MDC, then RPD Is ;J.00% or less, [f greater 5* MDA/ MDC, then RPD 200/o or less, [f below the MDA/ MDC, the RPO Is 0%, ./' Or meets the client's reoulred RER acceotance criteria. Tracer yield Is 15-125%

Carrier yield 25*125%. [Or meets the client's contract acceptance criteria). ../ Method blank Is less than the RDL/ LLD. .._/ irrf < 50/n nf '"ma.,* "ctlvltv) Sa mole was run within hold time. ../ \'Jt§L-lt l'."1/ Samnle was correctlv nreserved If reoulred. k \;).. Smears Taken for Radioactive batches. w-Method Spike and LCS are within 75-125% y r nr meets the client's contract a criteria l. No blank spaces on data forms. v-All line outs lnltlaled and dated. ,.,..,. DPPnPe Aux data Is correct. l\h-Client Sneclal renulrements nane has been checked. ,/ Raw Data and/ or soectrum are Included and orooerlv st,.t11sed. ..,,,-MS, LCS, and Duplicate RPD/RER values uploaded to UM5 and ,,/ ""lues UDPlflaA Hit .. rlf Mr R"trh --*---' *-*-*-,,,,.,. ** ...-11)\ 1\\v Batch Data Exception Reports CDERl comoleted If aoolicable. v 19... o'l L,,lJ Batch Data Exception Reports (DER) second reviewed. tf \ \ :!.-> Dlsnosition V"rlfled tn be completed. I.an ... **-* t"orrection romnl"t .. ..t If renulred. Review sample historical results If available ,,,,.,. [If REMP. results above MDC have been verified bv historical results recount or re-analvsls. l Primary Review Performed By: __ __ J_o_J_i_/_1_L,. ___ _ Secondary Review Performed By: __ @ fh '(J.)0 Page' 697 of 5809 10/03/16 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 01-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, Am-05-RC Solid . Batch ID: Sample Numbers: 1602285 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,40523531,405235032,405235033,405235034,405235035, 405235036,405235037,405235038,405235039,405235040, and 1203636291 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 01-0CT-16 Jessica Davis 03-0CT-16 Page 1 Page 698 of 5809 DER Report No.: 1563613 Revision No.: 1 Type: Process Client Code: MJWC Am/Cm Queue Sheet 27-SEP-16 -*------------*------Analyst: MXS2 First Client Due Date: 04-0CT-16 Internal Due Date:Ol-OCT-16 Tracer(s

m243 . Tracer Code: \1SZ.-(, Expiration Date: . 5-L.L:>** I='] _ LCS Code(s): 0$33-C< I 12..-1( .. o -& Expiration Date: 4-Z..1-17 I q-:p-1r,.,;. Spike Isotope(s): Am241/Cm244 Spike Code(s): . I Expiration Date: I -PrepDate:CJ .... z.1-1t..,., Initials: [v'\.S)) PipetID: \qlO 7&C(f2..,,-Witness:-11'1'"'-A-,__ __ Sample ID Client 405235021*2 4.2B.R.2.3 405235022-2 4.2B.R.1.3 405235023-2 4.2B.R.U.2 405235024-2 4.ZB.R.2.2 405235025-2 4.2B.R.1.2 405235026-2 4.2C.R.1.3 405235027-2 4.2C.R.1.4 405235028-2 4.3.ARl.3 405235029-2 4.3.B.R.1.3 405235030-2 4.3A.R.2.3 405235031-2 4.3.BR19.2 405235032-2 4.3B.R.3.3 405235033-2 4.3B.R.3.4 405235034-2 4.3.B.R.1.4 405235035-2 4.3B.R.2.3 405235036-2 4.3B.R.2.4 405235037-2 *4.4C.R.2.4 405235038*2 4.4C.R.1.3 405235039-2 4.4C.R.1.4 405235040-2 4.4D.R.l.3 1203636290-1 l\'IB for batch 1602285 1203636291-2 4.2B.R.2.3(405235021DUP) 1203636292-1 LCS for batch 1602285 Type SAMPLE SAt"\fi'LE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAt"\fi'LE SAMPLE SAMPLE SAl\1PLE SAMPLE SAt"\fi'LE SAMPLE SAMPLE SAMPLE SAl\1PLE MB DUP LCS Hazard Min Code CRDL 1 pCi/g lpCi/g 1 pCi/g 1 pCi/g 1 pCi/g lpCilg 1 pCilg 1 pCilg 1 pCilg 1 pCi/g 1 pCi!g 1 pCilg 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g lpCilg 1 pCilg 1 pCi/g 1 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL UCF pCilg to pCi!SOIL lpCilg SOIL UCF pCilg to pCi/SOIL Client l\1.JWCOOl l\1JWC001 1\1.JWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl !VlJWCOOl MJWCOOI l'vUWCOOl MJWCOOl MJWCOOl l\1.JWCOOl MJWCOOl MJWCOOl MJWCOOl l\UWCOOI MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Collection Date 08-DEC-15 08-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 23-NOV-15 23-NOV-15 23-NOV-15 26-NOV-15 23-NOV-15 23-NOV-15 . 23-NOV-15 23-NOV-15 23-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 08-DEC-15 Comments: Vol: Ori Vol(s): O* I I 0. / Vol(s): -I -Analyzed Sequentially with U: Pu: ___ _ wet4@ Label Aliquot Am/Cm Pos. Det# Choose SOP GL-RAD-A-036 Solid Sample Dissolution DIGESTION Circle One Data Reviewed By: vf11./2ovajD.L.,,..L 1cJ 1 )11,.. GEL Laboratories LLC, Radiochemistry Division Page 1 ofl /

BATCH NUMBER : 1602285 SAMPLE ID : S0405235021_AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G +/-0.198 % CHAMBER : 069 DETECTOR S/N : 78795 AVERAGE %EFFICIENCY : 32.9662 AVERAGE o/oEFF ERROR : 0.6355 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 85.5 +/-6.219 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.0558E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5545.77 AM-243 5269.50 5294.26 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5387.45 CM-247 4946.00 4911.66 CM-248 5078.60 5077.03 28 CM-247: 4n5-4987 keV CM-248: 5009-5105 keV 25 fl.M.243:5131-5366keV CM-5/6:5372-539BkeV AM-241: 5404-5613 keV 22 CM-314: 5646-5a78 keV CM-242: 5975-6198 keV 19 Vi 16 I-13 z '.:) 0 10 8 7 *:; 4 <( PEAK FWHM 4.959 50.247 0.000 0.000 24.793 7.438 0.000 2404 2802 3206 3614 4026 4442 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.040 0.960 0.9798 98.525 5.35E-04 322.000 320.800 1.200 1.0954 99.980 4.22E+OO 0.000 -0.240 0.240 0.4899 100.000 -1.12E-02 0.000 -0.480 0.480 0.6928 100.000 -6.52E-03 8.000 8.000 0.000 0.0000 86.090 1.22E-01 6.000 5.280 0.720 0.8485 79.300 8.76E-02 3.000 2.280 0.7.20 0.8485 91.000 3.30E-02 6591 7034 7481 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B069.CNF;1823 BKG DATE : 25-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W069.CNF;495 CAL DA TE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.97E-02 8.81E-02 2.40E-02 7.11E-01 9.23E-02 2.64E-02 9.65E-02 2.23E-01 4.18E-02 2.89E-02 7.52E-02 1.72E-02 9.15E-02 4.59E-02 O.OOE+OO 8.82E-02 1.01E-01 2.58E-02 5.85E-02 8.84E-02 2.25E-02 1.96-sigma cnt Unc pCi/G 3.97E-02 4.64E-01 9.64E-02 2.88E-02 9.02E-02 8.75E-02 5.83E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235022 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 070 DETECTOR S/N : 78262 AVERAGE %EFFICIENCY : 31.2964 AVERAGE %EFF ERROR : 0.6038 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 90.0 +/-6.211 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.2716E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5475.03 AM-243 5269.50 5270.60 CM-242 6102.00 6086.56 CM-3/4 5795.02 5721.65 CM-5/6 5386.00 5373.62 CM-247 4946.00 4887.83 CM-248 5078.60 5070.02 28 CM-247: 4n5-4987 keV CM-248: 5009-5105 keV 25 AM-243: 5131*5366 keV CM-5!6:S372-5J98keV AM-241:5404-5613keV 22 CM-3/4: 5646-5878 keV CM-242:5975-6198keV 19 0' 16 z 13 :J 0 10 8 7 ti 4 <l'. 2381 2775 3175 3578 Energy (keV) PEAK FWHM 88.200 42.467 0.000 58.800 0.000 0.000 14.700 3987 4400 COUNT DATE : 29-Sep-2016 21 :26:39 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 4.000 3.760 0.240 0.4899 98.525 5.02E-02 321.000 320.760 0.240 0.4899 99.980 4.22E+OO 0.000 -0.480 0.480 0.6928 100.000 -2.23E-02 3.000 2.760 0.240 0.4899 100.000 3.74E-02 1.000 1.000 0.000 0.0000 86.090 1.53E-02 7.000 7.000 0.000 0.0000 79.300 1.16E-01 11.000 11.000 0.000 0.0000 91.000 1.59E-01 >'>> >> = .: = * = 6537 6978 7424 " " u u u u Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B070.CNF;1825 BKG DATE : 25-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W070.CNF;500 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCl/G pCi/G 5.95E-02 6.40E-02 1.20E-02 7.09E-01 6.30E-02 1.18E-02 9.88E-02 2.57E-01 5.90E-02 5.41E-02 6.50E-02 1.22E-02 4.30E-02 4.58E-02 0.00E+OO 9.33E-02 4.97E-02 O.OOE+OO 1.00E-01 4.33E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.92E-02 4.62E-01 9.86E-02 5.39E-02 4.29E-02 9.22E-02 9.83E-02 AlphaSpactroscopySoflwareVerslon3.5.3 effectlvedata:02*Mar*2015 BATCH NUMBER : 1602285 SAMPLE ID : S0405235023 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 084 DETECTOR S/N : 78265 AVERAGE %EFFICIENCY : 34.7248 AVERAGE %EFF ERROR : 0.6686 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 64.0 +/-6.897 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.0352E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5481.28 AM-243 5269.50 5273.73 CM-242 6102.00 6086.57 CM-3/4 5795.02 5652.77 CM-5/6 5386.00 5372.68 CM-247 4946.00 4893.67 CM-248 5078.60 5039.12 21 CM-247: 4775-4987 keV CM-248: 5009-5105 keV 19 AM-243: 5131-5366 keV CM-516: 5372-5398 keV 17 AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV CM-242: 5975-0198 keV 15 13 0' 11 z 9 => 0 7 5 u 3 <( 1 PEAK FWHM 4.933 52.740 0.000 4.933 0.000 4.933 0.000 2402 2799 3200 3606 4016 4431 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -1.640 2.640 1.6248 98.525 -2.79E-02 256.000 252.880 3.120 1.7664 99.980 4.23E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.040 0.960 0.9798 100.000 6.91E-04 3.000 2.760 0.240 0.4899 86.090 5.36E-02 3.000 2.520 0.480 0.6928 79.300 5.32E-02 8.000 7.760 0.240 0.4899 91.000 1.43E-01 =i = 6570 7011 7457 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B084.CNF;1733 BKG DATE : 25-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W084.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.47E-02 1.52E-01 5.06E-02 7.94E-01 1.58E-01 5.41E-02 1.23E-01 1.82E-01 O.OOE+OO 5.13E-02 1.14E-01 3.10E-02 7.76E-02 9.32E-02 1.74E-02 8.48E-02 1.17E-01 2.68E-02 1.11E-01 8.81E-02 1.65E-02 1.96-sigma cnt Unc pCi/G 5.47E-02 5.27E-01 1.22E-01 5.12E-02 7.73E-02 8.45E-02 1.09E-01 BATCH NUMBER : 1602285 SAMPLE ID : S0405235024 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 088 DETECTOR S/N : 83291 AVERAGE %EFFICIENCY : 31.2191 AVERAGE %EFF ERROR : 0.6024 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 80.8 +/-6.521 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.8326E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5509.09 AM-243 5269.50 5272.74 CM-242 6102.00 6086.57 CM-3/4 5795.02 5702.02 CM-5/6 5386.00 5372.97 CM-247 4946.00 4949.25 CM-248 5078.60 5066.38 CM-247: 47754987 keV 21 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 19 CM-SJ6:5372-5398keV AM-241; 5404-5613 keV 17 CM-314: 5646-5878 keV CM-242: 5975-6198 keV 15 13 11 z => 9 0 i2. 7 5 3 0 <l'. PEAK FWHM 24.614 46.766 0.000 14.768 0.000 4.923 4.923 2387 2783 3184 3589 3998 4412 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 2.000 0.800 1.200 1.0954 98.525 1.20E-02 289.000 287.080 1.920 1.3856 99.980 4.23E+OO 0.000 -1.200 1.200 1.0954 100.000 -6.26E-02 2.000 2.000 0.000 0.0000 100.000 3.04E-02 2.000 2.000 0.000 0.0000 86.090 3.42E-02 7.000 5.800 1.200 1.0954 79.300 1.08E-01 8.000 7.520 0.480 0.6928 91.000 1.22E-01 6549 6989 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B088.CNF;1732 BKG DATE : 25-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W088.CNF;463 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.37E-02 1.05E-01 3.01E-02 7.49E-01 1.19E-01 3.74E-02 1.19E-01 3.66E-01 1.05E-01 5.23E-02 4.56E-02 O.OOE+OO 5.89E-02 5.14E-02 O.OOE+OO 1.06E-01 1.30E-01 3.73E-02 9.75E-02 8.97E-02 2.06E-02 1.96-sigma cnt Unc pCi/G 5.37E-02 4.92E-01 1.19E-01 5.21E-02 5.87E-02 1.05E-01 9.61E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235025 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 089 DETECTOR S/N : 79988 AVERAGE %EFFICIENCY : 29.2461 AVERAGE %EFF ERROR : 0.5651 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 92.9 +/-6.329 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE 1752-C AM-243 4.7442E+OO dpm 4.4086E+OO dpm LIBRARY PEAK ENERGY ENERGY PEAK FWHM AM-241 5480.15 5523.34 108.645 AM-243 5269.50 5275.98 48.595 CM-242 6102.00 6086.58 0.000 CM-3/4 5795.02 5770.74 172.844 CM-5/6 5386.00 5378.72 4.938 CM-247 4946.00 4811.79 7.408 CM-248 5078.60 5067.82 7.408 25 CM-247* 4n5-4987 keV -CM-248: 5009-5105 keV 23 f-AM-243: 5131*5366 keV CM-516: 5372*5398 keV 21 f-AM-241: 5404*5613 keV CM-314: 5646-5876 keV 19 "-CM-242:5975-619BkeV 17 15 (ii 13 I--z 11 :J -0 9 7 $ *:;; 5 ---u 3 4'. --I I II I I I I I I I I 23 94 2791 3193 3598 4006 4419 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:42 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 4.000 1.840 2.160 1.4697 98.525 2.57E-02 312.000 309.360 2.640 1.6248 99.980 4.25E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 3.000 -2.280 5.280 2.2978 100.000 -3.23E-02 3.000 3.000 0.000 0.0000 86.090 4.78E-02 6.000 3.120 2.880 1.6971 79.300 5.40E-02 8.000 6.560 1.440 1.2000 91.000 9.90E-02 i 111111 II 1111 II I I I I I 525 E 82 611) 6543 6980 7420 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B089.CNF;1435 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W089.CNF;384 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.47E-02 1.17E-01 3.76E-02 7.29E-01 1.23E-01 4.09E-02 9.81E-02 1.46E-01 O.OOE+OO 6.41E-02 1.62E-01 5.96E-02 6.33E-02 4.78E-02 O.OOE+OO 9.47E-02 1.60E-01 5.38E-02 9.16E-02 1.12E-01 3.32E-02 1.96-sigma cnt Unc pCi/G 6.46E-02 4.77E-01 9.79E-02 6.41E-02 6.30E-02 9.45E-02 9.07E-02 AtphaSpectrcscopySoftwaruVerslon3.5.3 effectivedate:02-Mar*2015 BATCH NUMBER : 1602285 SAMPLE ID : S0405235026 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 090 DETECTOR S/N : 78263 AVERAGE %EFFICIENCY : 33.4344 AVERAGE %EFF ERROR : 0.6443 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 91.4 +/-6.011 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.3351 E+OO dpm NUCLIDE LIBRARY ENERGY AM-241 5480.15 AM-243 5269.50 CM-242 6102.00 CM-3/4 5795.02 CM-5/6 5386.00 CM-247 4946.00 CM-248 5078.60 CM-247: 4n54957 keV CM-248: 5009-5105 keV 28 AM-243:5131*5366keV CM-516: 5372*5396 keV 25 AM-241:5404-5613keV CM-3/4: 5646-5876 keV 22 CM-242: 5975-6198 keV 19 16 5 13 0 £ 10 0 *;;: 7 4 PEAK ENERGY 5538.23 5270.72 6086.56 5761.59 5377.16 4900.41 5067.97 PEAK FWHM 84.122 41.443 0.000 0.000 0.000 0.000 29.690 COUNT DATE : 29-Sep-2016 21 :26:42 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.040 0.960 0.9798 98.525 . 1.29E-02 348.000 347.760 0.240 0.4899 99.980 4.25E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.240 0.240 0.4899 100.000 -3.02E-03 5.000 4.760 0.240 0.4899 86.090 6.75E-02 8.000 8.000 0.000 0.0000 79.300 1.23E-01 13.000 12.520 0.480 0.6928 91.000 1.68E-01 >>>> s = * = 1 2398 2796 3199 3606 4018 4435 Energy (keV) 6584 7028 7476 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B090.CNF;1440 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W090.CNF;374 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.41E-02 8.18E-02 2.23E-02 6.90E-01 5.86E-02 1.10E-02 8.72E-02 1.30E-01 O.OOE+OO 2.61E-02 6.04E-02 1.13E-02 6.93E-02 6.80E-02 1.27E-02 9.21E-02 4.62E-02 O.OOE+OO 1.01E-01 7.43E-02 1.70E-02 1.96-sigma cnt Unc pCi/G 4.41E-02 4.47E-01 8.71E-02 2.61E-02 6.88E-02 9.09E-02 9.90E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235027 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 091 DETECTOR S/N : 78259 AVERAGE %EFFICIENCY : 34.7245 AVERAGE %EFF ERROR : 0.6687 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 105 +/-5.624 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.9609E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5539.67 AM-243 5269.50 5260.76 CM-242 6102.00 6086.56 CM-3/4 5795.02 5761.59 CM-5/6 5386.00 5374.59 CM-247 4946.00 4887.33 CM-248 5078.60 5072.20 CM-247: 4n5-4987 keV 28 CM-246;5009-51D5keV AM-243: 5131-5366 keV 25 CM-516: 5372-5398 keV AM-241: 54G4-5613 keV CM-314:5646-5878keV 22 CM-242: 5975-6198 kaV 19 Vi 16 I-z 13 :J 0 10 s. 7 *;;; t5 4 <( PEAK FWHM 108.461 70.109 0.000 0.000 0.000 167.622 56.696 2382 2779 3180 3586 3996 4411 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:42 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 3.000 2.280 0.720 0.8485 98.525 2.40E-02 415.000 413.320 1.680 1.2961 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.720 0.720 0.8485 100.000 -7.68E-03 2.000 1.760 0.240 0.4899 86.090 2.11E-02 4.000 2.800 1.200 1.0954 79.300 3.65E-02 13.000 *13.000 0.000 0.0000 91.000 1.48E-01 6553 6996 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B091.CNF;1438 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W091.CNF;363 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.24E-02 6.42E-02 1.63E-02 6.48E-01 8.01E-02 2.46E-02 7.38E-02 1.10E-01 O.OOE+OO 2.32E-02 6.51E-02 1.66E-02 4.16E-02 5.76E-02 1.08E-02 5.92E-02 9.14E-02 2.62E-02 8.52E-02 3.41E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.24E-02 4.14E-01 7.37E-02 2.32E-02 4.15E-02 5.91E-02 8.35E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235028 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 093 DETECTOR S/N : 33206 AVERAGE %EFFICIENCY : 33.0892 AVERAGE %EFF ERROR : 0.6377 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 86.1 +/-6.205 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.0856E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5478.20 AM-243 5269.50 5296.39 CM-242 6102.00 6086.58 CM-3/4 5795.02 5804.90 CM-5/6 5386.00 5379.57 CM-247 4946.00 4881.20 CM-248 5078.60 5095.54 CM-247: 4n5-4987 keV CM-248:5009-510SkeV 28 AM-243: 5131-5366 keV CM-516: 5372-5398 keV 25 AM-241: 5404-5613 keV CM-314: 5646-5878 keV 22 CM-242:597S.0198keV 19 Ui 16 I-z 13 :::> 0 10 £ 7 t5 4 <( PEAK FWHM 0.000 40.579 0.000 104.345 0.000 0.000 4.969 2407 2806 3210 3617 4029 4444 Energy (keV) COUNT DATE : 29-Sep-2016 21:26:42 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 6.000 3.840 2.160 1.4697 98.525 5.04E-02 327.000 324.360 2.640 1.6248 99.980 4.19E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 2.000 1.040 0.960 0.9798 100.000 1.39E-02 6.000 6.000 0.000 0.0000 86.090 9.00E-02 0.000 -0.960 0.960 0.9798 79.300 -1.56E-02 1.000 1.000 0.000 0.0000 91.000 1.42E-02 6580 7019 7462 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B093.CNF;1431 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W093.CNF;379 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.11E-02 1.10E-01 3.53E-02 7.04E-01 1.16E-01 3.84E-02 9.83E-02 1.46E-01 O.OOE+OO 4.75E-02 8.79E-02 2.39E-02 7.90E-02 4.50E-02 O.OOE+OO 3.63E-02 1.07E-01 2.92E-02 3.99E-02 4.26E-02 0.00E+OO 1.96-sigma cnt Unc pCi/G 7.08E-02 4.59E-01 9.81E-02 4.74E-02 7.81E-02 3.62E-02 3.99E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235029 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.511 G -+/-0.196 % CHAMBER : 096 DETECTOR S/N : 80016 AVERAGE %EFFICIENCY : 32.5188 AVERAGE %EFF ERROR : 0.6269 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 86.9 +/-6.225 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.1218E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5483.41 AM-243 5269.50 5267.45 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5387.40 CM-247 4946.00 4900.63 CM-248 5078.60 5061.23 CM-247: 4n5-4987 keV 23 CM-248: 5009-5105 keV A.M.243:5131-5366keV 21 CM-5/6:5372*539BkeV P.M.241:5404-5613keV 19 CM-3/4: 5646-5878 keV CM-242:5975-6198keV 17 15 0' 13 z 11 :J 9 0 8 7 c 5 *5 u 3 <{ 1 PEAK FWHM 44.404 50.435 0.000 0.000 4.934 197.353 76.474 2391 2788 3189 3595 4004 4419 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:43 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 0.320 1.680 1.2961 98.525 4.23E-03 324.000 321.600 2.400 1.5492 99.980 4.18E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.440 1.440 1.2000 100.000 -1.93E-02 1.000 1.000 0.000 0.0000 86.090 1.51E-02 10.000 9.280 0.720 0.8485 79.300 1.52E-01 13.000 13.000 0.000 0.0000 91.000 1.86E-01 6554 6994 7438 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B096.CNF;1399 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W096.CNF;357 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.82E-02 1.02E-01 3.14E-02 7.05E-01 1.13E-01 3.69E-02 9.90E-02 1.47E-01 O.OOE+OO 3.12E-02 9.93E-02 2.95E-02 4.25E-02 4.53E-02 O.OOE+OO 1.09E-01 1.00E-01 2.55E-02 1.08E-01 4.29E-02 O.OOE+OO 1.96-sigma en! Une pCi/G 4.82E-02 4.60E-01 9.88E-02 3.12E-02 4.25E-02 1.08E-01 1.05E-01 BATCH NUMBER : 1602285 SAMPLE ID : S0405235030 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 097 DETECTOR S/N : 83288 AVERAGE %EFFICIENCY : 35.3557 AVERAGE %EFF ERROR : 0.6805 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 84.3 +/-6.086 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.9972E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5485.52 AM-243 5269.50 5267.55 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5373.98 CM-247 4946.00 4935.18 CM-248 5078.60 5083.20 CM-247: 4n5-4987 keV 25 CM-248: 5009-5105 keV AM-243: 5131-5366 keV CM-5/6: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-314: 5646-5878 keV 19 CM-242:5975-e198keV 16 Ui 13 I-z :::> 10 0 (:2. 7 4 PEAK FWHM 73.888 54.185 0.000 0.000 0.000 4.926 0.000 2402 2798 3198 3603 4012 4424 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:43 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.760 0.240 0.4899 98.525 2.22E-02 341.000 339.080 1.920 1.3856 99.980 4.21E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.200 1.200 1.0954 100.000 -1.54E-02 2.000 1.760 0.240 0.4899 86.090 2.54E-02 7.000 6.520 0.480 0.6928 79.300 1.02E-01 3.000 3.000 0.000 0.0000 91.000 4.09E-02 6551 6989 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B097.CNF;1396 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W097.CNF;381 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.37E-02 6.04E-02 1.13E-02 6.93E-01 1.00E-01 3.15E-02 9.44E-02 1.40E-01 0.00E+OO 2.92E-02 8.99E-02 2.57E-02 4.99E-02 6.91E-02 1.29E-02 8.86E-02 8.66E-02 1.98E-02 5.41E-02 4.09E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.36E-02 4.50E-01 9.43E-02 2.91E-02 4.98E-02 8.76E-02 5.38E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235031 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER ; 099 DETECTOR S/N : 80059 AVERAGE %EFFICIENCY : 35.6284 AVERAGE %EFF ERROR : 0.6858 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 82.4 +/-6.115 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.9076E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5516.55 AM-243 5269.50 5264.45 CM-242 6102.00 6086.56 CM-3/4 5795.02 5851.15 CM-5/6 5386.00 5376.28 CM-247 4946.00 4930.19 CM-248 5078.60 5081.86 CM-247: 4775-4987 keV CM-248: 5009-5105 keV 25 AM-243; 5131-5366 keV CM-516: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-3/4: 5645-5878 keV CM-242:5975-0198keV 19 Yi 16 1--13 z :J 10 0 7 .?;-*:;; 4 PEAK FWHM 151.309 56.436 0.000 4.881 4.881 0.000 5.694 2402 2795 3193 3595 4001 4413 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:43 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 5.000 4.280 0.720 0.8485 98.525 5.53E-02 335.000 334.040 0.960 0.9798 99.980 4.25E+OO 0.000 -0.480 0.480 0.6928 100.000 -2.27E-02 1.000 0.520 0.480 0.6928 100.000 6.83E-03 4.000 4.000 0.000 0.0000 86.090 5.91E-02 5.000 4.280 0.720 0.8485 79.300 6.86E-02 11.000 10.760 0.240 0.4899 91.000 1.50E-01 6539 6978 7421 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B099.CNF;1399 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W099.CNF;383 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.36E-02 7.89E-02 2.01E-02 7.03E-01 8.38E-02 2.28E-02 1.01E-01 2.62E-01 6.01E-02 3.80E-02 7.27E-02 1.67E-02 6.55E-02 4.43E-02 O.OOE+OO 7.B9E-02 9.79E-02 2.49E-02 9.72E-02 6.70E-02 1.25E-02 1.96-sigma cnt Unc pCi/G 6.32E-02 4.57E-01 1.00E-01 3.79E-02 6.51E-02 7.84E-02 9.53E-02 0 ....., Ul 00 0 '° BATCH NUMBER : 1602285 SAMPLE ID : S0405235032 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 107 DETECTOR SIN : 67578 AVERAGE %EFFICIENCY : 30.7195 AVERAGE %EFF ERROR : 0.5929 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 92.2 +/-6.204 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.3725E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.48 AM-243 5269.50 5270.07 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5374.65 CM-247 4946.00 4885.31 CM-248 5078.60 5076.70 CM-247: 4775-4987 keV 23 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 21 CM-516:5372-5398keV AM-241: 5404-5613 keV 19 CM-3!4: 5646-5678 keV CM-242: 5975-6198 keV 17 15 (jJ 1--13 z 11 :::) 9 0 s 7 a 5 *:;; 3 2399 2794 3194 3597 Energy (keV) PEAK FWHM 0.000 50.093 0.000 0.000 0.000 127.845 0.000 4005 4417 COUNT DATE : 29-Sep-2016 21 :26:44 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.920 1.920 1.3856 98.525 -2.57E-02 323.000 322.280 0.720 0.8485 99.980 4.24E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.720 0.720 0.8485 100.000 -9.78E-03 2.000 2.000 0.000 0.0000 86.090 3.06E-02 4.000 3.520 0.480 0.6928 79.300 5.84E-02 8.000 8.000 0.000 0.0000 91.000 1.16E-01 :m > § i::!I! = 6538 6975 7415 ::; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B107.CNF;1439 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W107.CNF;426 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.23E-02 1.08E-01 3.39E-02 7.12E-01 8.04E-02 2.04E-02 1.00E-01 1.49E-01 O.OOE+OO 2.96E-02 8.30E-02 2.11E-02 5.25E-02 4.58E-02 o,ooE+oo 7.43E-02 9.19E-02 2.10E-02 8.65E-02 4.34E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.23E-02 4.64E-01 1.00E-01 2.95E-02 5.24E-02 7.39E-02 8.53E-02 AlphaSpectroscopySoftwareVersJon3.5.3 effecllvedate:02-Mat-2015 BATCH NUMBER : 1602285 SAMPLE ID : S0405235033 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 108 DETECTOR S/N : 78778 AVERAGE %EFFICIENCY : 34.5578 AVERAGE %EFF ERROR : 0.6655 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 83.3 +/-6.156 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.9529E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.48 AM-243 5269.50 5270.77 CM-242 6102.00 6086.57 CM-3/4 5795.02 5759.00 CM-5/6 5386.00 5370.99 CM-247 4946.00 4939.29 CM-248 5078.60 5075.70 CM-247: 4n5-4987 keV 23 CM-248;5009-5105keV AM-243:5131*5366keV 21 CM-516: 5372-5398 keV AM-241:5404-5613keV 19 CM-314: 5646-5878 keV CM-242:597&-S198keV 17 15 (j) 13 I-z 11 ::J 9 0 7 5 *:;; t5 3 <I'. 2397 2792 3191 3594 Energy (keV) PEAK FWHM 0.000 76.717 0.000 142.421 0.000 88.399 58.933 4002 4414 COUNT DATE : 29-Sep-2016 21 :26:44 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 98.525 -9.52E-03 328.000 327.760 0.240 0.4899 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 2.000 1.760 0.240 0.4899 100.000 2.37E-02 2.000 2.000 0.000 0.0000 86.090 3.02E-02 3.000 2.040 0.960 0.9798 79.300 3.35E-02 3.000 3.000 0.000 0.0000 91.000 4.29E-02 B n = a = 6535 6971 7412 >:\ i :! ii " " Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B108.CNF;1433 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W108.CNF;430 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.88E-02 8.08E-02 2.06E-02 7.11E-01 6.24E-02 1.17E-02 9.91E-02 1.47E-01 O.OOE+OO 4.66E-02 6.45E-02 1.21E-02 5.19E-02 4.53E-02 O.OOE+OO 6.67E-02 1.08E-01 2.94E-02 5.67E-02 4.29E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.87E-02 4.63E-01 9.89E-02 4.65E-02 5.18E-02 6.66E-02 5.64E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235034 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 109 DETECTOR S/N : 79463 AVERAGE %EFFICIENCY : 36.1703 AVERAGE %EFF ERROR : 0.6959 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 82.6 +/-6.070 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.9182E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5519.34 AM-243 5269.50 5260.40 CM-242 6102.00 6172.15 CM-3/4 5795.02 5704.38 CM-5/6 5386.00 5372.47 CM-247 4946.00 4897.72 CM-248 5078.60 5066.35 28 CM-247; 4n&4987 keV CM-248:5009-5105keV 25 AM-243: 5131-5366 keV CM-516: 5372-5398 keV AM-241:5404-5613keV 22 CM-3/4: 5646-5878 keV CM-242:5975-6198keV 19 (ii 16 I-13 z :::> 0 10 .?;-7 *:;; :g 4 <( 1 2401 2796 3196 Energy (keV) PEAK FWHM 4.905 43.094 4.905 9.810 0.000 19.620 24.525 COUNT DATE : 29-Sep-2016 21 :26:44 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA. AREA AREA StDev pCi/G 1.000 0.040 0.960 0.9798 98.525 5.08E-04 341.000 340.040 0.960 0.9798 99.980 4.25E+OO 1.000 1.000 0.000 0.0000 100.000 4.71E-02 2.000 1.520 0.480 0.6928 100.000 1.96E-02 2.000 2.000 0.000 0.0000 86.090 2.90E-02 9.000 8.280 0.720 0.8485 79.300 1.30E-01 13.000 12.520 0.480 0.6928 91.000 1.72E-01 >>>> !l.ll!l = 6560 7002 7448 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B109.CNF;1431 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W109.CNF;420 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.77E-02 8.37E-02 2.28E-02 6.98E-01 8.23E-02 2.24E-02 1.33E-01 1.41E-01 O.OOE+OO 4.51E-02 7.15E-02 1.64E-02 4.99E-02 4.35E-02 O.OOE+OO 1.00E-01 9.62E-02 2.45E-02 1.04E-01 7.60E-02 1.74E-02 1.96-sigma cnt Unc pCi/G 3.76E-02 4.53E-01 1.32E-01 4.51E-02 4.97E-02 9.87E-02 1.01E-01 BATCH NUMBER : 1602285 SAMPLE ID : S0405235035 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 110 DETECTOR S/N : 83292 AVERAGE %EFFICIENCY : 32.3669 AVERAGE %EFF ERROR : 0.6241 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 85.2 +/-6.262 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.0433E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5446.02 AM-243 5269.50 5253.99 CM-242 6102.00 6122.26 CM-3/4 5795.02 5667.79 CM-5/6 5386.00 5385.09 CM-247 4946.00 4858.26 CM-248 5078.60 5064.74 CM-247: 47754987 keV 21 CM-248: 5009-5105 keV AM-243:5131*5366keV 19 CM-5!6: 5372-5398 keV AM-241: 5404-5613 keV 17 CM-314: 5646-5878 keV CM-242:597S-6198keV 15 0' 13 11 z ::i 9 0 8 7 5 u 3 <( 1 PEAK FWHM 83.679 68.009 4.922 4.922 0.000 132.901 61.528 2376 2772 3173 3578 3988 4402 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:44 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 3.000 2.520 0.480 0.6928 98.525 3.48E-02 314.000 314.000 0.000 0.0000 99.980 4.27E+OO 1.000, 0.760 0.240 0.4899 100.000 3.89E-02 1.000 1.000 0.000 0.0000 100.000 1.40E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 5.000 4.520 0.480 0.6928 79.300 7.74E-02 15.000 14.760 0.240 0.4899 91.000 2.20E-01 6543 6985 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B11 O.CNF;1440 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W110.CNF;441 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.54E-02 7.64E-02 1.75E-02 7.24E-01 4.08E-02 0.00E+OO 1.46E-01 2.46E-01 4.59E-02 3.95E-02 4.21E-02 O.OOE+OO 3.19E-02 4.73E-02 O.OOE+OO 8.40E-02 9.48E-02 2.17E-02 1.21E-01 7.16E-02 1.34E-02 1.96-sigma cnt Unc pCi/G 5.53E-02 4.73E-01 1.46E-01 3.95E-02 3.18E-02 8.34E-02 1.17E-01 Version 3.5.3 BATCH NUMBER : 1602285 SAMPLE ID : S0405235036 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.516 G -+/-0.194 % CHAMBER : 112 DETECTOR S/N : 78261 AVERAGE %EFFICIENCY : 34.0722 AVERAGE %EFF ERROR : 0.6563 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 81.4 +/-6.259 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.8630E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.47 AM-243 5269.50 5258.15 CM-242 6102.00 6086.56 CM-3/4 5795.02 5718.22 CM-5/6 5386.00 5379.20 CM-247 4946.00 4904.27 CM-248 5078.60 5063.61 23 CM-247: 47754987 keV CM-248: 5009-5105 keV 21 AM-243: 5131-5366 keV CM-516: 5372-5398 keV 19 AM-241:5404-5613keV CM-Jf4:5646-5878keV 17 CM-242:5975-6198keV 15 13 z 11 :::i 9 0 7 5 "> t5 3 <i:: PEAK FWHM 0.000 71.073 0.000 4.902 0.000 4.902 0.000 2398 2792 3191 3595 4003 4416 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:44 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.440 1.440 1.2000 98.525 -1.92E-02 317.000 315.800 1.200 1.0954 99.980 4.14E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.520 0.480 0.6928 100.000 7.04E-03 4.000 4.000 0.000 0.0000 86.090 6.09E-02 8.000 6.320 1.680 1.2961 79.300 1.04E-01 10.000 9.760 0.240 0.4899 91.000 1.41E-01 6547 6987 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B112.CNF;1443 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W112.CNF;451 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.10E-02 9.86E-02 2.93E-02 7.02E-01 9.20E-02 2.63E-02 9.98E-02 1.48E-01 O.OOE+OO 3.92E-02 7.50E-02 1.72E-02 6.76E-02 4.57E-02 O.OOE+OO 1.01E-01 1.28E-01 3.93E-02 9.59E-02 6.91E-02 1.29E-02 1.96-sigma cnt Unc pCi/G 3.09E-02 4.59E-01 9.96E-02 3.91E-02 6.71E-02 9.97E-02 9.41E-02 AlphaSpectrcscopySoflwareVersJon3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1602285 SAMPLE ID : S0405235037 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 069 DETECTOR S/N : 78795 AVERAGE %EFFICIENCY : 32.4474 AVERAGE %EFF ERROR : 0.6257 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.9 +/-7.852 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.2199E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5414.29 AM-243 5269.50 5289.04 CM-242 6102.00 6086.56 CM-3/4 5795.02 5761.59 CM-5/6 5386.00 5379.48 CM-247 4946.00 4966.75 CM-248 5078.60 5059.58 14 CM-247: 4n5-4987 keV CM-248:50Q9..5105keV 13 AM-243: 5131-5366 keV 12 CM-5f6: 5372-5398 keV AM-241: 5404-5613 keV 11 CM-314: 5646-5878 keV CM-242: keV 10 9 UJ 8 I-7 z 6 ::::> 0 5 4 3 *:;; n 2 <( 1 2406 2804 3206 3613 Energy {keV) PEAK FWHM 4.946 78.529 0.000 0.000 0.000 14.837 49.455 4024 4440 COUNT DATE : 01-0ct-2016 13:23:25 ELAPSED LIVE TIME(SEC) : 8129.05 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 -0.355 1.355 1.1640 98.525 -8.16E-03 186.000 185.458 0.542 0.7362 99.980 4.20E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.084 1.084 1.0411 100.000 -2.53E-02 4.000 3.865 0.135 0.3681 86.090 1.02E-01 2.000 1.323 0.677 0.8231 79.300 3.77E-02 4.000 3.458 0.542 0.7362 91.000 8.60E-02 m = 6588 7031 7478 1i ill ;!; " 5 " " u u u Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B069.CNF;1825 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W069.CNF;497 CAL DATE : 30-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.70E-02 1.63E-01 4.69E-02 9.01E-01 1.26E-01 2.92E-02 1.65E-01 2.50E-01 O.OOE+OO 4.96E-02 1.55E-01 4.27E-02 1.17E-01 1.13E-01 1.70E-02 9.88E-02 1.68E-01 4.12E-02 1.11E-01 1.39E-01 3.21E-02 1.96-sigma cnt Unc pCi/G 6.69E-02 6.07E-01 1.65E-01 4.94E-02 1.16E-01 9.87E-02 1.10E-01 BATCH NUMBER : 1602285 SAMPLE ID : S0405235038 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 250 DETECTOR S/N : 87938 AVERAGE %EFFICIENCY : 26.3779 AVERAGE %EFF ERROR : 0.5108 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 88.7 +/-6.718 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.2073E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5433.92 AM-243 5269.50 5262.36 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5378.12 CM-247 4946.00 4926.16 CM-248 5078.60 5089.53 CM-247: 4775-4987 keV CM-246: SOOS-5105 keV 25 AM-243; 5131-5366 keV CM-516: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-3/4: 5646-5676 keV CM-242:5975-619BkeV 19 en 16 I-13 z ::::> 0 10 s 7 .?;-*:;: 4 n <!'. PEAK FWHM 4.968 53.230 0.000 0.000 9.936 4.968 24.841 2374 2773 3176 3583 3994 4408 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:33 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 1.000 0.000 0.0000 98.525 1.60E-02 267.000 266.280 0.720 0.8485 99.980 4.20E+OO 0.000 0.000 0.000 o.booo 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -7.81E-03 2.000 2.000 0.000 0.0000 86.090 3.66E-02 1.000 0.520 0.480 0.6928 79.300 1.03E-02 2.000 2.000 0.000 0.0000 91.000 3.46E-02 6536 6973 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B250.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W250.CNF;115 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.51E-02 4.81E-02 O.OOE+OO 7.66E-01 9.63E-02 2.45E-02 1.17E-01 1.73E-01 O.OOE+OO 3.46E-02 9.01E-02 2.07E-02 6.30E-02 5.49E-02 O.OOE+OO 5.75E-02 1.10E-01 2.52E-02 5.96E-02 5.20E-02 O.OOE+OO 1.96-sigma en! Une pCi/G 4.50E-02 5.06E-01 1.16E-01 3.45E-02 6.28E-02 5.74E-02 5.94E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235039 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.511 G -+/-0.196 % CHAMBER : 251 DETECTOR S/N : 87939 AVERAGE %EFFICIENCY : 25.8839 AVERAGE %EFF ERROR : 0.5015 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 79.1 +/-7.115 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.7524E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5581.74 AM-243 5269.50 5250.19 CM-242 6102.00 6086.58 CM-3/4 5795.02 5710.21 CM-5/6 5386.00 5373.72 CM-247 4946.00 4828.83 CM-248 5078.60 5055.51 CM 247* 4n54987 keV 23 I-CM-248: 5009-5105 keV AM-243: 5131*5366 keV 21 t-CM-5!6: 5372-5398 keV AM-241: 5404-5613 keV 19 1-CM-314: 5646-5878 keV CM-242: 597!Hi198 keV 17 r 15 r 0' 13 z 11 r r ::> 9 0 r 2-7 r 5 *;;: r ti 3 <l: r I I I PEAK FWHM 4.963 29.778 0.000 4.963 0.000 4.963 69.481 I I I 23 70 2769 3172 3579 3990 4405 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.040 0.960 0.9798 98.525 7.29E-04 234.000 233.040 0.960 0.9798 99.980 4.18E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.280 0.720 0.8485 100.000 5.19E-03 1.000 1.000 0.000 0.0000 86.090 2.08E-02 1.000 0.520 0.480 0.6928 79.300 1.18E-02 5.000 4.760 0.240 0.4899 91.000 9.38E-02 I 111 I I I I I II I I I I 4S24 p24! 5 73 610' 6538 6976 7418 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B251.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W251.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.41E-02 1.20E-01 3.27E-02 8.10E-01 1.18E-01 3.22E-02 1.33E-01 1.97E-01 O.OOE+OO 5.43E-02 1.13E-01 2.88E-02 5.87E-02 6.25E-02 0.00E+OO 6.54E-02 1.25E-01 2.87E-02 9.65E-02 9.45E-02 1.77E-02 1.96-sigma cnt Unc pCi/G 5.41E-02 5.40E-01 1.32E-01 5.42E-02 5.86E-02 6.54E-02 9.56E-02 BATCH NUMBER : 1602285 SAMPLE ID : S0405235040 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 252 DETECTOR S/N : 87940 AVERAGE %EFFICIENCY : 26.3006 AVERAGE %EFF ERROR : 0.5094 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 95.7 +/-6.512 % TRACER 1752cC ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5405E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY. AM-241 5480.15 5508.49 AM-243 5269.50 5261.64 CM-242 6102.00 6089.58 CM-3/4 5795.02 5659.67 CM-5/6 5386.00 5398.26 CM-247 4946.00 4895.57 CM-248 5078.60 5053.72 25 CM-247: 47754987 keV CM-248: 5009-5105 keV 23 AM-243: 5131-5366 keV CM-5!6: 5372-5398 keV 21 AM-241: 5404-5613 keV (;M.314: 564&5878 keV 19 CM-242:5975-6198keV 17 15 Vi 13 I-z 11 ::::> 0 9 S?.. 7 *s: 5 3 1 2384 2783 3187 3594 Energy (keV) PEAK FWHM 0.000 52.973 4.966 4.966 0.000 144.020 0.000 4004 4419 COUNT DATE : 29-Sep-2016 21:52:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.240 0.240 0.4899 98.525 -3.57E-03 287.000 286.520 0.480 0.6928 99.980 4.19E+OO 1.000 1.000 0.000 0.0000 100.000 5.35E-02 1.000 0.760 0.240 0.4899 100.000 1.15E-02 1.000 1.000 0.000 0.0000 86.090 1.70E-02 2.000 1.520 0.480 0.6928 79.300 2.80E-02 3.000 3.000 0.000 0.0000 91.000 4.82E-02 >>> > m > > .:.:!U! :::::! = 6551 6988 7430 u u u Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B252.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W252.CNF;127 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCl/G pCl/G 3.08E-02 7.12E-02 1.33E-02 7.41E-01 8.10E-02 1.86E-02 1.51E-01 1.61E-01 O.OOE+OO 4.31E-02 7.24E-02 1.35E-02 4.78E-02 5.10E-02 O.OOE+OO 6.45E-02 1.02E-01 2.34E-02 6.38E-02 4.82E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.08E-02 4.87E-01 1.50E-01 4.30E-02 4.78E-02 6.44E-02 6.34E-02 BATCH NUMBER : 1602285 SAMPLE ID : S1203636290 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.516 G -+/-0.194 % CHAMBER : 092 DETECTOR S/N : 80063 AVERAGE %EFFICIENCY : 30.3421 AVERAGE %EFF ERROR : 0.5858 SAMPLE DATE : 27-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 88.7 +/-6.345 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7439E+OO dpm 4.2073E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5482.00 AM-243 5269.50 5282.42 CM-242 6102.00 6086.57 CM-3/4 5795.02 5703.11 CM-5/6 5386.00 5375.07 CM-247 4946.00 4904.98 CM-248 5078.60 5046.82 CM-247: 4n5-4987 keV 25 CM-248; 5009-5105 keV AM-243: 5131*5366 keV CM-5/6: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-314: 5646-5878 keV 19 CM-242:5975-6198keV 16 en 13 1--z ::::> 10 0 7 .?;-*::; 4 n <( PEAK FWHM 103.362 52.337 0.000 4.922 0.000 182.114 4.922 2406 2802 3203 3608 4017 4430 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:42 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 3.000 2.520 0.480 0.6928 98.525 3.46E-02 308.000 306.320 1.680 1.2961 99.980 4.14E+OO 0.000 -0.480 0.480 0.6928 100.000 -6.57E-03 1.000 0.520 0.480 0.6928 100.000 7.03E-03 10.000 9.520 0.480 0.6928 86.090 1.49E-01 4.000 2.560 1.440 1.2000 79.300 4.36E-02 6.000 5.040 0.960 0.9798 91.000 7.49E-02 6565 7005 7449 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B092.CNF;1442 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W092.CNF;414 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.51E-02 7.60E-02 1.74E-02 7.12E-01 1.05E-01 3.21E-02 2.91E-02 7.58E-02 1.74E-02 3.91E-02 7.49E-02 1.72E-02 1.05E-01 8.70E-02 1.99E-02 7.79E-02 1.26E-01 3.75E-02 7.92E-02 9.79E-02 2.67E-02 1.96-sigma cnt Unc pCi/G 5.49E-02 4.66E-01 2.91E-02 3.91E-02 1.03E-01 7.77E-02 7.86E-02 0 ....., Vi 00 0 ID BATCH NUMBER : 1602285 SAMPLE ID : S1203636291 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 253 DETECTOR S/N : 87941 AVERAGE %EFFICIENCY : 25.6727 AVERAGE %EFF ERROR : 0.4975 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 100 +/-6.462 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.7534E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5251.79 CM-242 6102.00 6086.59 CM-3/4 5795.02 5697.36 CM-5/6 5386.00 5385.09 CM-247 4946.00 4916.53 CM-248 5078.60 5074.29 CM-247; 4775-4987 keV 21 CM-248:5009-5105keV AM-243: 5131-5366 keV 19 CM-Sl6:5372-5398keV AM-241: 54G4-5613 keV 17 CM-314: 5646-5878 Jr;eV CM-242: 5975-6198 keV 15 13 11 z :J 9 0 s. 7 5 *:;; u 3 <( 2368 2769 3173 3581 Energy (keV) PEAK FWHM 0.000 60.055 0.000 4.985 0.000 104.681 0.000 COUNT DATE : 29-Sep-2016 21:52:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 98.525 -1.07E-02 294.000 292.800 1.200 1.0954 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 0.00E+OO 1.000 0.520 0.480 0.6928 100.000 7.81E-03 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 2.000 1.760 0.240 0.4899 79.300 3.23E-02 9.000 8.520 0.480 0.6928 91.000 1.36E-01 m = = 6540 6977 7418 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B253.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W253.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.22E-02 9.04E-02 2.30E-02 7.48E-01 1.02E-01 2.92E-02 1.04E-01 1.55E-01 O.OOE+OO 4.35E-02 8.32E-02 1.91E-02 3.42E-02 5.08E-02 0.00E+OO 6.37E-02 8.81E-02 1.65E-02 1.02E-01 8.86E-02 2.03E-02 1.96-sigma cnt Unc pCi/G 3.22E-02 4.91E-01 1.04E-01 4.34E-02 3.41E-02 6.35E-02 1.00E-01 BATCH NUMBER : 1602285 SAMPLE ID : S1203636292 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.516 G -+/-0.194 % CHAMBER : 254 DETECTOR S/N : 87942 AVERAGE %EFFICIENCY : 25.1642 AVERAGE %EFF ERROR : 0.4879 SAMPLE DATE : 27-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 74.9 +/-7.368 % TRACER ID 1752-C NUCLIDE AM-243 NOMINAL 4.7439E+OO dpm RESULTS 3.5527E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM AM-241 5480.15 5498.98 48.957 AM-243 5269.50 5284.39 41.459 CM-242 6102.00 6081.71 4.975 CM-3/4 5795.02 5812.67 49.544 CM-5/6 5386.00 5379.30 14.925 CM-247 4946.00 4906.49 109.453 CM-248 5078.60 5058.10 54.726 CM-247: 47754987 keV CM-248: 5009-5105 keV 25 AM-243: 5131-5366 keV CM-516: 5372-5398 keV 22 AM-241:5404-5613keV CM-3/4: 5646-5878 keV CM-242:5975-619BkeV 19 (/) 16 I-13 z :l 0 10 s 7 ..>--*::; 4 ts <{ 2385 2785 3188 3596 4007 4422 Energy (keV) COUNT DATE : 29-Sep-2016 21:52:42 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0533-CC 1216-G NUCLIDE AM-241 CM-3/4 NOMINAL (pCi/G) 3.8166E+OO 5.0427E+OO % RECOVERY 119.347 119.178 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 233.000 232.520 0.480 0.6928 98.525 4.56E+OO 215.000 214.520 0.480 0.6928 99.980 4.14E+OO 1.000 1.000 0.000 0.0000 100.000 1.95E-02 312.000 311.280 0.720 0.8485 100.000 6.01E+OO 7.000 7.000 0.000 0.0000 86.090 1.57E-01 2.000 1.520 0.480 0.6928 79.300 3.70E-02 4.000 3.760 0.240 0.4899 91.000 7.97E-02 ] :: > = 6553 6991 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B254.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W254.CNF;116 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.99E-01 1.08E-01 2.49E-02 8.32E-01 1.07E-01 2.45E-02 5.50E-02 5.86E-02 O.OOE+OO 1.12E+OO 1.18E-01 3.00E-02 1.27E-01 6.73E-02 O.OOE+OO 8.52E-02 1.35E-01 3.09E-02 9.48E-02 1.02E-01 1.90E-02 1.96-sigma cnt Unc pCi/G 5.88E-01 5.56E-01 5.50E-02 6.70E-01 1.25E-01 8.50E-02 9.40E-02 Effective 3/25/201 O Revision 1 Effective March 2010 Batch# \ $ q (ogq D Product: Criteria: Samole Solids are less than or equal to 100 m11 for GAB. Samples have been blank corrected (If required). Blank correction renorted Included (If reaulredl. If activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. rf hnlnu* *hn unA t Mnr "rror Is ok"" Instrument source check Is within limits. Instrument bka check is within limits. Method RDL/ LLD has been met. If duplicate activities are: Less than 5* MDA/ MDC, then RPO is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, If below the M DA/ MDC, the RPD is 0%, Or meets the client's reauired RER acceotance criteria. Tracer yield Is 15-125%

Carrier yield 25*125%. (Or meets the client's contract acceptance criteria). Method blank is less than the RDL/ LLD. 1n..,.,1 _. l<Oln nf ln .. onr* "'"tlvltv\ Samole was run within hold time. Samole was correctlv areserved if reoulred. Smears Taken for Radioactive batches. Method Spike and LCS are within 75*125% or menho *hn client'" .. nn....,.... e rrltnrb\ No blank soaces on data forms. All line outs Initialed and dated. Nn nrrnr" "rn Aux data' is correct. Client Soeclal reouirements oaae has been checked. Radiochemistry Batch Checklist 30-Sep-2016 oate:_I Yes No Comments AX>J lb-/ / .,/' v v ../ t i:<c,:i.,(.., ... \\..\'J-..,,.--..,,,,...-t\jl)-,,,.,. Raw Data and I or soectrum are included and nronerlv statuscd * .,,..-MS, LCS. and Duplicate RPD/RER values uploaded to UMS and ./ 1v,.1o,,.., ""'r"'n"' Mit -(If 1-..n-"' :,.. .. r. nn*nrn .. ln*n ,,./ Batch Data Exceotlon Reoorts fDERl completed. If aonllcable. / MU-1S1d':k:i11,,,, Batch Data Exception Reports (DER} second reviewed. L:i::<JJI, \5l_o.?Aol6 Dlsoosltian verified to be comoleted. All-.. -* rorrn-fnn if rnnufred. Review sample historical results if available v (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l Primary Review Performed By: __ _ _i;.J..-_...;l_D_._\ ._I .... I _,,_I'-'=--"------Secondary Review Performed By: __ 10/02/16 , GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 01-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, Am-05-RC Solid Batch ID: Sample Numbers: 1596390 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203621695 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 01-0CT-16 Jessica Davis 03-0CT-16 Page 1 Page 724 of 5809 DER Report No.: 1563616 Revision No.: 1 Type: Process Client Code: MJWC Choose SOP GL-RAD-A-036 GEL Laboratories LLC, Radioclzemistry Division Solid Sample Dissolution by: LEACH Circ'ifOne ="' U'fiJ1v Data Reviewed J Page 1 ofl BATCH NUMBER : 1596390 SAMPLE ID : S0405235001 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 213 DETECTOR S/N : 87901 AVERAGE %EFFICIENCY : 24.8786 AVERAGE %EFF ERROR : 0.4826 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 79.7 +/-7.233 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.7834E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5279.38 CM-242 6102.00 6086.59 CM-3/4 5795.02 5781.22 CM-5/6 5386.00 5385.09 CM-247 4946.00 4844.10 CM-248 5078.60 5062.86 -CM 247* 47754987 keV 17 CM-248:5009-5105keV 1-AM-243: 5131-5366 keV CM-+516: 5372-5398 keV 15 i--AM-241: 5404-5613 keV CM-314: 5646-5878 keV 13 CM-242:5975-6198keV 11 Ui 9 I-f-z ::J 7 0 f-5 f-3 u f-<!'. f-I I I I PEAK FWHM 0.000 56.423 0.000 4.987 0.000 69.816 0.000 I I I 23 77 2778 3182 3590 4002 4417 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:31 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 0.000 -0.720 0.720 0.8485 98.525 -1.38E-02 228.000 225.840 2.160 1.4697 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.520 0.480 0.6928 100.000 1.01E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 2.000 1.040 0.960 0.9798 79.300 2.48E-02 2.000 2.000 0.000 0.0000 91.000 4.15E-02 I I 11! I I I I I I I 4g35 525! ! )85 611 p 6548 6985 7426 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B213.CNF;469 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W213.CNF;152 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.18E-02 1.17E-01 2.98E-02 8.41E-01 1.58E-01 5.08E-02 1.34E-01 1.99E-01 O.OOE+OO 5.63E-02 1.08E-01 2.47E-02 4.43E-02 6.58E-02 O.OOE+OO 8.47E-02 1.57E-01 4.27E-02 7.14E-02 6.22E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.17E-02 5.61E-01 1.33E-01 5.63E-02 4.42E-02 8.46E-02 7.11E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235002 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 214 DETECTOR S/N : 87902 AVERAGE %EFFICIENCY : 26.2230 AVERAGE %EFF ERROR : 0.5080 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 66.5 +/-7.622 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.1552E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5576.87 AM-243 5269.50 5281.92 CM-242 6102.00 6086.58 CM-3/4 5795.02 5807.25 CM-5/6 5386.00 5384.87 CM-247 4946.00 4881.19 CM-248 5078.60 5019.13 21 CM-247: 47754987 keV CM-24B:5009-5105keV 19 AM-243; 5131-5366 keV CM-516: 5372-5398 keV 17 AM-241:54D4-5613keV CM-314: 5646-5878 keV CM-242:5975-6198keV 15 13 Ul 11 I-z 9 ::J 0 7 s .?;-5 *5 t5 3 <!'. 1 PEAK FWHM 4.958 56.323 0.000 4.958 4.958 0.000 4.958 2373 2771 3174 3581 3991 4406 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.280 0.720 0.8485 98.525 6.06E-03 199.000 198.520 0.480 0.6928 99.980 4.23E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.520 0.480 0.6928 100.000 1.14E-02 1.000 0.760 0.240 0.4899 86.090 1.88E-02 0.000 -0.960 0.960 0.9798 79.300 -2.58E-02 1.000 0.520 0.480 0.6928 91.000 1.22E-02 6538 6976 7419 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B214.CNF;456 BKG DATE : 23"Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W214.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.35E-02 1.32E-01 3.37E-02 8.80E-01 1.18E-01 2.71E-02 1.51E-01 2.24E-01 O.OOE+OO 6.36E-02 1.22E-01 2.79E-02 7.07E-02 1.19E-01 2.22E-02 5.99E-02 1.77E-01 4.82E-02 6.78E-02 1.30E-01 2.97E-02 1.96-sigma cnt Unc pCi/G 6.34E-02 5.91E-01 1.51E-01 6.35E-02 7.06E-02 5.98E-02 6.77E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235003 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 221 DETECTOR S/N : 87909 AVERAGE %EFFICIENCY : 25.5264 AVERAGE %EFF ERROR : 0.4948 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 50.7 +/-8.724 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 2.4047E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.51 AM-243 5269.50 5288.54 CM-242 6102.00 6086.60 CM-3/4 5795.02 5761.63 CM-5/6 5386.00 5372.39 CM-247 4946.00 4881.21 CM-248 5078.60 5056.59 CM-247* 4775-4987 keV 19 ,_ CM-248: 5009-5105 keV AM-243:5131-S366keV 17 CM-5f6:5372*5398keV I-AM-241: 5404-5613 keV CM-314:5646-5878keV 15 i-CM-242:5975-6198keV 13 c-Ui 11 -I-z 9 ::> -0 7 s . ,. 3 ti -<( c-I I I I I PEAK FWHM 0.000 17.199 0.000 0.000 0.000 0.000 0.000 I I 23 82 2784 3190 3599 4011 4427 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 98.525 -1.41E-02 148.000 147.280 0.720 0.8485 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -1.43E-02 2.000 2.000 0.000 0.0000 86.090 6.73E-02 0.000 -0.480 0.480 0.6928 79.300 -1.75E-02 0.000 -0.480 0.480 0.6928 91.000 -1.53E-02 I I . I I I I I 4846 026! ! )95 612 6557 6993 7433 ---Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B221.CNF;467 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W221.CNF;128 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 6.27E-02 1.63E-01 3.73E-02 1.02E+OO 1.77E-01 4.50E-02 2.05E-01 3.05E-01 O.OOE+OO 6.36E-02 1.65E-01 3.79E-02 1.16E-01 1.01E-01 O.OOE+OO 7.78E-02 2.02E-01 4.63E-02 6.78E-02 1.76E-01 4.04E-02 1.96-sigma cnt Unc pCi/G 6.25E-02 6.93E-01 2.05E-01 6.34E-02 1.15E-01 7.75E-02 6.75E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235004 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 223 DETECTOR S/N : 87911 AVERAGE %EFFICIENCY : 25.6333 AVERAGE %EFF ERROR : 0.4968 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 95.4 +/-6.595 % TRACER , ID 1752-C NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5247E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5510.30 AM-243 5269.50 5277.36 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5398.92 CM-247 4946.00 4905.16 CM-248 5078.60 5029.45 CM-247: 4775-4987 keV CM-248: 5009-5105 keV 25 AM-243: 5131*5366 keV CM-516: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-3!4: 5646-5878 keV CM-242:5975-5198keV 19 Cii 16 I-13 z :J 0 10 e. 7 4 0 <!'. PEAK FWHM 64.534 42.981 0.000 0.000 0.000 119.140 4.964 2377 2776 3178 3584 3994 4408 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:45 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 3.000 1.800 1.200 . 1.0954 98.525 2.80E-02 279.000 278.280 0.720 0.8485 99.980 4.26E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -7.57E-03 1.000 0.760 0.240 0.4899 86.090 1.35E-02 3.000 2.760 0.240 0.4899 79.300 5.32E-02 1.000 1.000 0.000 0.0000 91.000 1.68E-02 6529 6965 7403 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B223.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W223.CNF;114 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.36E-02 1.09E-01 3.12E-02 7.62E-01 9.34E-02 2.38E-02 1.09E-01 1.62E-01 O.OOE+OO 3.36E-02 8.74E-02 2.00E-02 5.07E-02 8.52E-02 1.59E-02 7.70E-02 9.25E-02 1.73E-02 4.73E-02 5.04E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.35E-02 5.02E-01 1.09E-01 3.35E-02 5.06E-02 7.67E-02 4.73E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235005 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 224 DETECTOR S/N : 87912 AVERAGE %EFFICIENCY : 25.7363 AVERAGE %EFF ERROR : 0.4987 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 102 +/-6.407 % TRACER .1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.8389E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5481.72 AM-243 5269.50 5284.24 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5387.92 CM-247 4946.00 4870.40 CM-248 5078.60 5064.71 28 CM-247: 4n5-4987 keV CM*248:500S-5105keV 25 AM-243: 5131*5366 keV CM-Sf6:5372*5396keV AM-241:54Q4.5613keV 22 CM-3f4:5646-SB78keV CM*242:5975-6198keV 19 (j) 16 1--13 z ::i 0 10 7 *:;; u 4 <{ PEAK FWHM 78.719 48.529 0.000 0.000 19.680 78.719 19.680 2399 2795 3195 3599 4007 4420 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:48 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 3.000 1.560 1.440 1.2000 98.525 2.25E-02 300.000 298.800 1.200 1.0954 99.980 4.25E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 3.000 3.000 0.000 0.0000 86.090 4.95E-02 2.000 1.280 0.720 0.8485 79.300 2.29E-02 2.000 1.520 0.480 0.6928 91.000 2.37E-02 > = = = 6545 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B224.CNF;471 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W224.CNF;150 CAL DA TE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.95E-02 1.07E-01 3.18E-02 7.38E-01 9.97E-02 2.85E-02 1.01E-01 1.50E-01 O.OOE+OO 2.96E-02 4.40E-02 O.OOE+OO 6.55E-02 4.95E-02 0.00E+OO 6.32E-02 1.10E-01 2.79E-02 5.46E-02 8.65E-02 1.98E-02 1.96-sigma cnt Unc pCi/G 5.94E-02 4.84E-01 1.00E-01 2.96E-02 6.52E-02 6.31E-02 5.45E-02 Alpha Spectroscopy Software Version 3.5.3 eft"ectlvedate:02*Mar-2015 BATCH NUMBER : 1596390 SAMPLE ID : S0405235006 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 226 DETECTOR S/N : 87914 AVERAGE %EFFICIENCY : 26.8347 AVERAGE %EFF ERROR : 0.5195 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 67.9 +/-7.501 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.2200E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5569.98 AM-243 5269.50 5267.31 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5385.09 CM-247 4946.00 4881.20 CM-248 5078.60 5053.89 CM-247* 4n5-4987 kBV 21 ._ CM-248: 5009-5105 keV AM-243: 5131*5366 keV 19 1-CM-516: 5372*5398 keV AM-241: 54Q4.5613 keV 17 CM-314:5646--5878keV I-CM-242: 5975-6198 keV 15 >-Ci) 13 I-11 z '.:) 9 0 >-£ 7 >-.?;-5 *:;;: u 3 <l: I I I I PEAK FWHM 4.984 43.500 0.000 0.000 0.000 0.000 44.853 I I I 23 72 2772 3177 3585 3997 4413 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:50 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.280 0.720 0.8485 98.525 5.85E-03 209.000 207.320 1.680 1.2961 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 0.000 -0.240 0.240 0.4899 79.300 -6.23E-03 2.000 1.760 0.240 0.4899 91.000 3.98E-02 I I I I I I 4B32 525 E 82 611 6548 6986 7428 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B226.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W226.CNF;122 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.13E-02 1.28E-01 3.25E-02 8.73E-01 1.59E-01 4.88E-02 1.46E-01 2.16E-01 O.OOE+OO 4.29E-02 6.36E-02 O.OOE+OO 4.83E-02 7.17E-02 O.OOE+OO 5.38E-02 1.24E-01 2.33E-02 7.84E-02 1.08E-01 2.03E-02 1.96-sigma cnt Unc pCi/G 6.12E-02 5.85E-01 1.45E-01 *4.28E-02 4.82E-02 5.37E-02 7.82E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235007 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 227 DETECTOR S/N : 87915 AVERAGE %EFFICIENCY : 26.3665 AVERAGE %EFF ERROR : 0.5107 SAMPLE DATE : 1 O-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 96.4 +/-6.499 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5734E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5499.71 AM-243 5269.50 5267.49 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5381.39 CM-247 4946.00 4881.19 CM-248 5078.60 5013.89 23 CM-247: 4n5-4987 keV CM-248: 5009-5105 keV 21 AM-243:5131-5366keV CM*S/6: 5372-5398 keV 19 AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV 17 CM-242:5975-6198keV 15 Vi 13 I-11 z 9 0 7 5 u <I: 3 PEAK FWHM 4.922 56.257 0.000 0.000 0.000 0.000 4.922 2375 2771 3171 3576 3984 4397 Energy (keV) COUNT DATE : 29-Sep-2016 21 :50:52 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 4.000 2.800 1.200 1.0954 98.525 4.19E-02 291.000 289.320 1.680 1.2961 99.980 4.27E+OO 0.000 -0.240 0.240 0.4899 100.000 -1.24E-02 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 2.000 2.000 0.000 0.0000 86.090 3.42E-02 0.000 -1.200 1.200 1.0954 79.300 -2.23E-02 1.000 0.040 0.960 0.9798 91.000 6.48E-04 6525 6963 7405 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B227.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W227.CNF;120 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.81E-02 1.05E-01 3.01E-02 7.52E-01 1.14E-01 3.50E-02 1.07E-01 2.48E-01 4.64E-02 3.07E-02 4.56E-02 O.OOE+OO 5.89E-02 5.14E-02 O.OOE+OO 4.23E-02 1.30E-01 3.73E-02 4.81E-02 1.07E-01 2.91E-02 1.96-sigma cnt Unc pCi/G 6.79E-02 4.94E-01 1.07E-01 3.06E-02 5.87E-02 4.23E-02 4.80E-02 AlphaSpectroscopySoftwareVerslon3.5.3 effec:tivedate:02-Mar*2015 BATCH NUMBER : 1596390 SAMPLE ID : S0405235008 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 228 DETECTOR S/N : 87916 AVERAGE %EFFICIENCY : 25.5769 AVERAGE %EFF ERROR : 0.4958 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 78.4 +/-7.191 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.7205E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5496.58 AM-243 5269.50 5257.74 CM-242 6102.00 6086.59 CM-3/4 5795.02 5747.18 CM-5/6 5386.00 5385.09 CM-247 4946.00 4878.24 CM-248 5078.60 5059.76 21 CM*247: 47754987 keV CM*248: 5009-5105 keV 19 AM-243: 5131*5366 keV CM*S/5;5372*5398keV 17 AM-241: 5404-5613 keV CM+3/4:5646-5878keV CM-242:5975-6198keV 15 13 'iii 11 1--z 9 :J 0 7 5 *::; t5 3 <i: 2369 2768 3171 3578 Energy (keV) PEAK FWHM 4.970 43.071 0.000 4.970 0.000 4.970 0.000 3989 4403 COUNT DATE : 29-Sep-2016 21 :50:56 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.040 0.960 0.9798 98.525 7.56E-04 230.000 228.320 1.680 1.2961 99.980 4.25E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.040 0.960 0.9798 100.000 7.67E-04 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 1.000 -1.160 2.160 1.4697 79.300 -2.72E-02 2.000 1.520 0.480 0.6928 91.000 3.11E-02 > !!! ! m ::::l! :::ll;l 6528 6964 7404 :! u u Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B228.CNF;457 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W228.CNF;117 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.61E-02 1.25E-01 3.39E-02 8.32E-01 1.44E-01 4.42E-02 1.32E-01 1.96E-01 O.OOE+OO 5.70E-02 1.26E-01 3.44E-02 4.37E-02 6.48E-02 O.OOE+OO 7.39E-02 1.97E-01 6.32E-02 7.15E-02 1.13E-01 2.59E-02 1.96-sigma cnt Unc pCi/G 5.61E-02 5.55E-01 1.32E-01 5.69E-02 4.36E-02 7.38E-02 7.14E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235009 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 218 DETECTOR S/N : 87906 AVERAGE %EFFICIENCY : 25.1171 AVERAGE %EFF ERROR : 0.4871 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 99.5 +/-6.553 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.7225E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5464.70 AM-243 5269.50 5275.95 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5374.01 CM-247 4946.00 4921.26 CM-248 5078.60 5060.53 CM-247:4n5-4987keV 31 CM-248:5009-5105keV AM-243:5131*5366keV 28 CM-516: 5372-5398 keV AM-241: 5404-5613 keV 25 CM-314: 5646-5878 keV CM-242:5975-6198keV 22 Ui 19 1--16 z :> 13 0 s 10 a 7 *s; :g 4 <( 1 2369 2770 3176 3585 Energy (keV) PEAK FWHM 14.989 41.684 0.000 0.000 0.000 109.919 74.945 COUNT DATE : 29-Sep-2016 21 :50:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.520 0.480 0.6928 98.525 2.30E-02 287.000 284.600 2.400 1.5492 99.980 4.24E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -7.37E-03 2.000 2.000 0.000 0.0000 86.090 3.46E-02 3.000 2.520 0.480 0.6928 79.300 4.73E-02 2.000 1.280 0.720 0.8485 91.000 2.10E-02 6550 6988 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B218.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W218.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.29E-02 8.38E-02 1.92E-02 7.54E-01 1.29E-01 4.23E-02 1.06E-01 1.57E-01 O.OOE+OO 3.27E-02 8.51E-02 1.95E-02 5.95E-02 5.19E-02 O.OOE+OO 7.55E-02 1.04E-01 2.38E-02 5.77E-02 1.00E-01 2.54E-02 1.96-sigma cnt Unc pCi/G 5.28E-02 4.96E-01 1.05E-01 3.26E-02 5.93E-02 7.52E-02 5.77E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235010 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 231 DETECTOR S/N : 87919 AVERAGE %EFFICIENCY : 22.6542 AVERAGE %EFF ERROR : 0.4405 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 95.8 +/-6.941 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5449E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5465.56 AM-243 5269.50 5268.52 CM-242 6102.00 6086.60 CM-3/4 5795.02 5761.63 CM-5/6 5386.00 5385.09 CM-247 4946.00 4881.21 CM-248 5078.60 5056.59 -CM-247* 47754987 keV CM-248: 50()9.5105 keV 25 AM-243: 5131*5366 keV CM-5f6: 5372-5398 keV 22 _ AM-241: 5404-5613 keV CM-3/4:5646-5878keV CM-24:Z:S975-6198keV 19 -(j) 16 -I-13 z r :J 0 10 r s 7 r *::; 4 t5 r <i: 1 r I I ., I I PEAK FWHM 89.629 35.769 0.000 0.000 0.000 0.000 0.000 I I I I 23 78 2778 3181 3588 3999 4413 Energy (keV) COUNT DATE : 29-Sep-2016 21 :51 :01 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 2.000 0.560 1.440 1.2000 98.525 9.82E-03 248.000 247.040 0.960 0.9798 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.240 0.240 0.4899 100.000 -4.27E-03 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 0.000 0.000 0.000 0.0000 79.300 O.OOE+OO 0.000 -0.720 0.720 0.8485 91.000 -1.37E-02 Jr I I I I I I I 4l30 p25 76 6535 6969 7408 -"':; n Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B231.CNF;423 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W231.CNF;109 CAL DA TE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.35E-02 1.30E-01 3.86E-02 8.06E-01 1.14E-01 3.10E-02 1.22E-01 1.82E-01 O.OOE+OO 3.69E-02 8.54E-02 1.60E-02 4.05E-02 6.02E-02 O.OOE+OO 4.40E-02 6.53E-02 O.OOE+OO 4.13E-02 1.16E-01 2.95E-02 1.96-sigma cnt Unc pCi/G 6.34E-02 5.34E-01 1.22E-01 3.69E-02 4.04E-02 4.39E-02 4.12E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235011_AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G +/-0.200 % CHAMBER : 070 DETECTOR S/N : 78262 AVERAGE %EFFICIENCY : 31.3847 AVERAGE %EFF ERROR : 0.6055 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 38.4 +/-11.794 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 1.8213E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5529.73 AM-243 5269.50 5294.42 CM-242 6102.00 6109.03 CM-3/4 5795.02 5761.59 CM-5/6 5386.00 5385.09 CM-247 4946.00 4887.40 CM-248 5078.60 5016.63 12 CM-247: 4n5-4987 keV CM-248: 5009-5105 keV 11 AM-<243: 5131*5366 keV CM-516: 5372-5398 keV 10 AM-241: 5404-5613 keV CM-3!4: 5646-5878 keV 9 CM-242;5975-6198keV 8 en 7 I-6 z 5 :l 0 4 3 *s; 2 :g <I.'. PEAK FWHM 49.198 30.749 4.920 0.000 0.000 49.198 4.920 2384 2780 3180 3585 3995 4409 Energy (keV) COUNT DATE : 01-0ct-2016 13:23:25 ELAPSED LIVE TIME(SEC) : 8132.68 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 -0.169 2.169 1.4727 98.525 -9.46E-03 78.000 77.458 0.542 0.7363 99.980 4.27E+OO 1.000 1.000 0.000 0.0000 100.000 1.96E-01 0.000 -0.678 0.678 0.8232 100.000 -3.86E-02 0.000 -0.136 0.136 0.3682 86.090 -8.69E-03 2.000 1.593 0.407 0.6377 79.300 1.11E-01 1.000 0.864 0.136 0.3682 91.000 5.24E-02 6545 6986 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B070.CNF;1827 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W070.CNF;502 CAL DATE : 30-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.00E-01 4.58E-01 1.45E-01 1.39E+OO 3.08E-01 7.12E-02 5.47E-01 5.87E-01 O.OOE+OO 1.18E-01 3.35E-01 8.21E-02 1.29E-01 2.75E-01 4.14E-02 2.40E-01 3.64E-01 7.78E-02 1.70E-01 2.60E-01 3.91E-02 1.96-sigma cnt Unc pCi/G 2.00E-01 9.62E-01 5.45E-01 1.18E-01 1.28E-01 2.39E-01 1.70E-01 Alpha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596390 SAMPLE ID : S0405235012 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 234 DETECTOR S/N : 87922 AVERAGE %EFFICIENCY : 24.8037 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 104 +/-6.482 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.9126E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5603.54 AM-243 5269.50 5275.14 CM-242 6102.00 6086.60 CM-3/4 5795.02 5790.25 CM-5/6 5386.00 5378.57 CM-247 4946.00 4922.71 CM-248 5078.60 5100.01 23 CM-247: 4775-4987 keV CM-248; 5009-5105 keV 21 AM-243: 5131-5366 keV CM-516: 5372-5398 keV 19 AM-241:5404-5613keV CM-3!4:5646-5878keV 17 CM-242: 5975-6198 keV 15 en 13 f-11 z :J 9 0 8 7 5 *::; u <( 3 2388 2790 3194 3603 Energy (keV) PEAK FWHM 4.996 61.205 0.000 4.996 4.996 134.901 4.996 4014 4429 COUNT DATE : 29-Sep-2016 21 :52:02 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 1.000 -0.440 1.440 1.2000 98.525 -6.46E-03 295.000 292.360 2.640 1.6248 99.980 4.22E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.520 0.480 0.6928 100.000 7.75E-03 3.000 3.000 0.000 0.0000 86.090 5.03E-02 3.000 3.000 0.000 0.0000 79.300 5.46E-02 1.000 0.520 0.480 0.6928 91.000 8.25E-03 >><> !* = = a = 6554 6990 7428 :! " ii u u u Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B234.CNF;454 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W234.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.46E-02 1.09E-01 3.23E-02 7.43E-01 1.29E-01 4.30E-02 1.02E-01 1.52E-01 O.OOE+OO 4.31E-02 8.25E-02 1.89E-02 6.66E-02 5.03E-02 O.OOE+OO 7.23E-02 5.46E-02 O.OOE+OO 4.59E-02 8.79E-02 2.01E-02 1.96-sigma cnt Unc pCi/G 4.46E-02 4.88E-01 1.02E-01 4.30E-02 6.62E-02 7.19E-02 4.59E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235013 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 235 DETECTOR S/N : 87923 AVERAGE %EFFICIENCY : 24.7991 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 109 +/-6.334 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 5.1602E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5272.08 CM-242 6102.00 6086.58 CM-3/4 5795.02 5730.37 CM-5/6 5386.00 5380.27 CM-247 4946.00 4987.82 CM-248 5078.60 5056.58 28 CM-247: 4775-4967 keV CM-248: 5009-5105 keV 25 AM-243:5131-5366keV CM-516: 5372-5398 keV AM-241: 5404-5613 keV 22 CM-3/4: 5646-5878 keV CM-242:5975-6198keV 19 (ii 16 I-13 z :J 0 10 8 7 u 4 <( 1 2392 2792 3196 3604 Energy (keV) PEAK FWHM 0.000 58.786 0.000 29.867 0.000 0.000 0.000 4016 4431 COUNT DATE : 29-Sep-2016 21 :52:04 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 98.525 -1.02E-02 308.000 307.040 0.960 0.9798 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 2.000 0.800 1.200 1.0954 100.000 1.15E-02 2.000 2.000 0.000 0.0000 86.090 3.23E-02 1.000 0.280 0.720 0.8485 79.300 4.91E-03 0.000 0.000 0.000 0.0000 91.000 O.OOE+OO 6566 7005 7447 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B235.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W235.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.08E-02 8.64E-02 2.20E-02 7.34E-01 9.17E-02 2.50E-02 9.94E-02 1.48E-01 O.OOE+OO 5.15E-02 1.01E-01 2.88E-02 5.56E-02 4.85E-02 O.OOE+OO 5.14E-02 1.07E-01 2.73E-02 3.09E-02 4.59E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.07E-02 4.80E-01 9.92E-02 5.15E-02 5.54E-02 5.14E-02 3.08E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235014 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 236 DETECTOR S/N : 87924 AVERAGE %EFFICIENCY : 25.7707 AVERAGE %EFF ERROR : 0.4994 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 97.5 +/-6.511 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.6254E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5470.89 AM-243 5269.50 5264.88 CM-242 6102.00 6108.33 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5380.52 CM-247 4946.00 4881.20 CM-248 5078.60 5056.58 CM-247: 4n5-4987 keV 23 CM*248:5009-5105keV AM-243:5131-5366 keV 21 CM-5!6: 5372*5398 keV AM-241: 5404*5613 keV 19 CM-.:J/4:5646-5878keV CM-242:5975-6198keV 17 15 if) f-13 z 11 ::> 9 0 7 5 *;;; ts 3 <( 1 PEAK FWHM 44.650 53.084 4.961 0.000 4.961 0.000 0.000 2386 2785 3188 3594 4004 4419 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:07 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 0.320 1.680 1.2961 98.525 4.84E-03 286.000 286.000 0.000 0.0000 99.980 4.26E+OO 1.000 1.000 0.000 0.0000 100.000 5.26E-02 0.000 -0.240 0.240 0.4899 100.000 -3.68E-03 1.000 1.000 0.000 0.0000 86.090 1.73E-02 0.000 -0.960 0.960 0.9798 79.300 -1.80E-02 0.000 -0.480 0.480 0.6928 91.000 -7.85E-03 6547 6984 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B236.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W236.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.52E-02 1.17E-01 3.59E-02 7.52E-01 4.47E-02 O.OOE+OO 1.48E-01 1.58E-01 O.OOE+OO 3.18E-02 7.36E-02 1.38E-02 4.87E-02 5.19E-02 O.OOE+OO 4.18E-02 1.24E-01 3.37E-02 3.48E-02 9.06E-02 2.08E-02 1.96-sigma cnt Unc pCi/G 5.51E-02 4.94E-01 1.48E-01 3.18E-02 4.86E-02 4.17E-02 3.47E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235015 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 071 DETECTOR S/N : 80020 AVERAGE %EFFICIENCY : 31.8394 AVERAGE %EFF ERROR : 0.6142 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 87.4 +/-8.003 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.1464E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5585.42 AM-243 5269.50 5289.14 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5379.20 CM-247 4946.00 4881.19 CM-248 5078.60 5056.58 CM-247: 4nS-4987 kaV 17 CM-248: 5009-5105 keV AM-243: 5131-5366 keV CM--5/6:5372*5398keV 15 AM-241: 5404-5613 keV CM-3/4: 5646-5876 keV 13 CM-242:5975-6198keV 11 Ci) 9 1--z :J 7 0 5 *::; 3 u <t: PEAK FWHM 4.963 38.053 0.000 0.000 4.963 0.000 0.000 2403 2802 3205 3613 4025 4441 Energy (keV) COUNT DATE : 01-0ct-201613:23:22 ELAPSED LIVE TIME(SEC) : 8073.70 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.462 0.538 0.7337 98.525 1.11E-02 178.000 177.596 0.404 0.6354 99.980 4.20E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.135 0.135 0.3668 100.000 -3.28E-03 4.000 3.865 0.135 0.3668 86.090 1.06E-01 0.000 -0.538 0.538 0.7337 79.300 -1.60E-02 0.000 -0.673 0.673 0.8202 91.000 -1.75E-02 6584 7026 7471 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B071.CNF;1818 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W071.CNF;466 CAL DATE : 30-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.82E-02 1.34E-01 3.09E-02 9.18E-01 1.24E-01 2.63E-02 1.67E-01 2.53E-01 O.OOE+OO 4.88E-02 1.05E-01 1.57E-02 1.22E-01 1.18E-01 1.76E-02 6.12E-02 1.66E-01 3.83E-02 5.38E-02 1.53E-01 3.73E-02 1.96-sigma cnt Unc pCi/G 6.81E-02 6.20E-01 1.66E-01 4.87E-02 1.21E-01 6.10E-02 5.36E-02 0 ...., Ul 00 0 \0 BATCH NUMBER : 1596390 SAMPLE ID : S0405235016 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 072 DETECTOR S/N : 67584 AVERAGE %EFFICIENCY : 31.7314 AVERAGE %EFF ERROR : 0.6121 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 67.6 +/-9.019 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.2094E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.48 AM-243 5269.50 5286.69 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5380.68 CM-247 4946.00 4906.57 CM-248 5078.60 5092.38 14 CM-247: 4175-4987 keV CM-248: 5009-5105 keV 13 AM-243: 5131-5366 keV 12 CM-516: 5372-5398 keV AM-241: 5404-5613 keV 11 CM-3/4: 5646-5878 keV CM-242: 5975-6198 keV 10 9 (j) 8 1--7 z 6 0 5 4 3 *:;; t5 2 <!'. 1 PEAK FWHM 0.000 40.120 0.000 0.000 4.963 4.963 4.963 2367 2766 3170 3578 3990 4406 Energy (keV) COUNT DATE : 01-0ct-2016 13:23:22 ELAPSED LIVE TIME(SEC) : 8077.28 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -1.615 1.615 1.2710 98.525 -5.11E-02 138.000 137.058 0.942 0.9707 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.404 0.404 0.6355 100.000 -1.30E-02 1.000 1.000 0.000 0.0000 86.090 3.61E-02 1.000 0.731 0.269 0.5189 79.300 2.87E-02 1.000 0.865 0.135 0.3669 91.000 2.96E-02 6553 6996 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B072.CNF;1825 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W072.CNF;477 CAL DATE : 30-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.91E-02 2.36E-01 7.04E-02 1.05E+OO 1.99E-01 5.29E-02 2.20E-01 3.32E-01 0.00E+OO 6.54E-02 1.68E-01 3.57E-02 1.01E-01 1.08E-01 O.OOE+OO 1.10E-01 1.89E-01 3.57E-02 9.58E-02 1.47E-01 2.20E-02 1.96-sigma en! Une pCi/G 6.89E-02 7.20E-01 2.19E-01 6.52E-02 1.01E-01 1.10E-01 9.56E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235017 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 243 DETECTOR S/N : 87931 AVERAGE %EFFICIENCY : 24.8977 AVERAGE %EFF ERROR : 0.4829 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 57.4 +/-8.348 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 2.7252E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5471.52 AM-243 5269.50 5276.40 CM-242 6102.00 6086.59 CM-3/4 5795.02 5721.73 CM-5/6 5386.00 5385.09 CM-247 4946.00 4801.50 CM-248 5078.60 5056.59 17 CM-247* 4775-4967 keV CM-248: 5009+5105 keV AM-243: 5131-5366 keV 15 1-CM-516: 5372-5398 keV AM-241: 5404-5613 keV 13 CM-3/4: 5646-5878 keV CM-242:5975-0198keV 11 en 9 I-z ::J 7 0 5 *s: 3 t5 <( f--I I I I PEAK FWHM 29.884 40.952 0.000 4.981 0.000 4.981 0.000 I I 23 89 2789 3193 3600 4011 4426 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:14 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 3.000 -2.520 5.520 2.3495 98.525 -6.71E-02 164.000 162.800 1.200 1.0954 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.520 0.480 0.6928 100.000 1.41E-02 0.000 -0.480 0.480 0.6928 86.090 -1.46E-02 1.000 -0.440 1.440 1.2000 79.300 -1.45E-02 0.000 0.000 0.000 0.0000 91.000 O.OOE+OO II II I I I I I I I I ! B90 611 B 6550 6986 7424 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B243.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W243.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.21E-01 3.09E-01 1.15E-01 9.75E-01 1.84E-01 5.26E-02 1.92E-01 2.85E-01 O.OOE+OO 7.83E-02 1.50E-01 3.43E-02 6.48E-02 1.69E-01 3.86E-02 1.01E-01 2.44E-01 7.26E-02 5.82E-02 8.64E-02 O.OOE+OO 1.96-sigma en! Unc pCi/G 1.21E-01 6.60E-01 1.92E-01 7.81E-02 6.46E-02 1.00E-01 5.80E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235018 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 244 DETECTOR S/N : 87932 AVERAGE %EFFICIENCY : 23.7184 AVERAGE %EFF ERROR : 0.4607 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 110 +/-6.427 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 5.2154E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY , AM-241 5480.15 5428.84 AM-243 5269.50 5277.59 CM-242 6102.00 6086.60 CM-3/4 5795.02 5761.63 CM-5/6 5386.00 5381.08 CM-247 4946.00 4880.55 CM-248 5078.60 5063.74 34 CM-247: 4775-4987 keV CM-248: 5009-5105keV 31 AM-243: 5131*5366 keV CM-516: 5372-5398 keV 28 AM-241:541J4.5613keV CM-314: 5645-5878 keV 25 CM-242:5975-6198keV 22 19 z 16 ::> 13 0 10 7 u 4 <( 1 PEAK FWHM 4.999 32.718 0.000 0.000 22.493 129.962 54.984 2378 2779 3184 3592 4004 4419 Energy (keV) COUNT DATE: 29-Sep-201621:52:17 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.280 0.720 0.8485 98.525 4.10E-03 298.000 296.800 1.200 1.0954 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.960 0.960 0.9798 100.000 -1.43E-02 5.000 5.000 0.000 0.0000 86.090 8.36E-02 5.000 3.800 1.200 1.0954 79.300 6.90E-02 3.000 2.040 0.960 0.9798 91.000 3.23E-02 6545 6980 7418 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B244.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W244.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.29E-02 8.94E-02 2.27E-02 7.45E-01 1.01E-01 2.89E-02 1.06E-01 1.57E-01 O.OOE+OO 3.31E-02 9.79E-02 2.67E-02 8.14E-02 5.02E-02 O.OOE+OO 9.01E-02 1.27E-01 3.64E-02 6.44E-02 1.04E-01 2.84E-02 1.96-sigma cnt Unc pCi/G 4.28E-02 4.88E-01 1.05E-01 3.31E-02 8.07E-02 8.96E-02 6.42E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235019 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 245 DETECTOR S/N : 87933 AVERAGE %EFFICIENCY : 25.3775 AVERAGE %EFF ERROR : 0.4920 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 96.6 +/-6.590 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5827E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5272.42 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5371.40 CM-247 4946.00 4979.93 CM-248 5078.60 5056.59 34 CM-247: 4n5-4987 keV CM-248: 5009-5105 keV 31 AM-243: 5131-5366 keV CM-5/6: 5372-5398 keV 28 AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV 25 CM-242:597&-019BkeV 22 (ii 19 I-16 z => 13 0 10 c 7 *:;; n 4 <x: 1 PEAK FWHM 0.000 28.048 0.000 0.000 0.000 4.986 0.000 2375 2776 3180 3588 3999 4414 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:20 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.960 0.960 0.9798 98.525 -1.48E-02 280.000 279.040 0.960 0.9798 99.980 4.22E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -7.49E-03 3.000 3.000 0.000 0.0000 86.090 5.27E-02 1.000 0.760 0.240 0.4899 79.300 1.45E-02 0.000 0.000 0.000 0.0000 91.000 O.OOE+OO 6542 6979 7419 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B245.CNF;457 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W245.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.43E-02 1.01E-01 2.76E-02 7.56E-01 9.97E-02 2.72E-02 1.08E-01 1.61E-01 O.OOE+OO 3.32E-02 8.64E-02 1.98E-02 6.98E-02 5.27E-02 O.OOE+OO 5.45E-02 9.15E-02 1.71E-02 3.36E-02 4.99E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.42E-02 4.98E-01 1.08E-01 3.31E-02 6.94E-02 5.44E-02 3.35E-02 BATCH NUMBER : 1596390 SAMPLE ID : S0405235020 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 246 DETECTOR S/N : 87949 AVERAGE %EFFICIENCY : 25.1972 AVERAGE %EFF ERROR : 0.4886 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 103 +/-6.430 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.8967E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5483.90 AM-243 5269.50 5278.72 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5374.08 CM-247 4946.00 4881.21 CM-248 5078.60 5056.59 CM 247* 4775-4987 keV 31 CM-248: 5009-5105 keV AM-243:5131-5366keV CM-516: 5372*5398 keV 28 -AM-241: 5404*5613 keV 25 CM-3f4:5546-5878keV -CM-242: 5975-ti198keV 22 0' 19 z 16 --:::i 13 0 a *:; 7 -t5 4 <( I I I PEAK FWHM 4.979 54.154 0.000 0.000 0.000 0.000 0.000 I I I 23 75 2775 3179 3587 3998 4412 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:22 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 3.000 2.280 0.720 0.8485 98.525 3.33E-02 297.000 296.040 0.960 0.9798 99.980 4.26E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -7.12E-03 1.000 1.000 0.000 0.0000 86.090 1.67E-02 0.000 -0.480 0.480 0.6928 79.300 -8.70E-03 0.000 0.000 0.000 0.0000 91.000 0.00E+OO Iii ii I 11 I I I I p25: f D78 610 6539 6975 7415 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B246.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W246.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.91E-02 8.92E-02 2.27E-02 7.42E-01 9.48E-02 2.58E-02 1.03E-01 1.53E-01 O.OOE+OO 3.15E-02 8.21E-02 1.88E-02 4.70E-02 5.01E-02 O.OOE+OO 3.86E-02 1.00E-01 2.30E-02 3.19E-02 4.74E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.89E-02 4.87E-01 1.03E-01 3.15E-02 4.70E-02 3.85E-02 3.18E-02 BATCH NUMBER : 1596390 SAMPLE ID : S1203621694 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 095 DETECTOR S/N : 38626 AVERAGE %EFFICIENCY : 30.4247 AVERAGE %EFF ERROR : 0.5873 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 113 +/-5.744 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7439E+OO dpm 5.3493E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5463.63 AM-243 5269.50 5277.02 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5385.09 CM-247 4946.00 4898.38 CM-248 5078.60 5054.30 CM-247: 4775-4967 keV 37 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 33 CM-5!6:5372-5398keV AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV 29 CM-242:597!Hi198keV 25 en 21 I-z 17 :J 0 13 9 *:;; ti <( 5 PEAK FWHM 4.993 35.808 0.000 0.000 0.000 39.946 64.912 2380 2781 3186 3595 4007 4423 Energy (keV) COUNT DATE : 29-Sep-2016 21 :26:43 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.280 0.720 0.8485 98.525 3.05E-03 391.000 390.520 0.480 0.6928 99.980 4.20E+OO 0.000 -0.240 0.240 0.4899 100.000 -2.62E-03 0.000 -0.960 0.960 0.9798 100.000 -1.03E-02 0.000 -0.240 0.240 0.4899 86.090 -3.00E-03 2.000 1.280 0.720 0.8485 79.300 1.73E-02 2.000 2.000 0.000 0.0000 91.000 2.36E-02 6559 6997 7439 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B095.CNF;1407 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W095.CNF;408 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.20E-02 6.66E-02 1.70E-02 6.50E-01 5.95E-02 1.36E-02 2.27E-02 5.24E-02 9.81E-03 2.40E-02 7.09E-02 1.93E-02 2.59E-02 5.99E-02 1.12E-02 4.78E-02 8.28E-02 2.11E-02 4.06E-02 3.54E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.19E-02 4.17E-01 2.26E-02 2.39E-02 2.58E-02 4.77E-02 4.05E-02 BATCH NUMBER : 1596390 SAMPLE ID : S1203621695 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 247 DETECTOR S/N : 87935 AVERAGE %EFFICIENCY : 26.2005 AVERAGE %EFF ERROR : 0.5076 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 46.0 +/-9.010 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 2.1838E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5264.19 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5385.09 CM-247 4946.00 4892.29 CM-248 5078.60 5056.59 17 CM 247' 47754987 keV -CM-248: 5009-5105 keV AM-243: 5131*5366 keV 15 -CM-516: 5372-5398 keV AM-241: 5404-5613 keV 13 CM-3/4: 5646-5878 keV -CM-242: 5975--6198 keV 11 -en 9 I-z :::i 7 -0 s 5 -*::; 3 -r ' ' PEAK FWHM 0.000 30.147 0.000 0.000 0.000 4.984 0.000 I ' ' 23 81 2781 3186 3594 4005 4421 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:25 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA Stoev pCi/G 0.000 -0.720 0.720 0.8485 98.525 -2.28E-02 138.000 137.280 0.720 0.8485 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.240 0.240 0.4899 100.000 -7.70E-03 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 1.000 0.280 0.720 0.8485 79.300 1.10E-02 0.000 -0.480 0.480 0.6928 91.000 -1.64E-02 I I ' 'L I I I I 840 526 89 6552 6990 7431 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B247.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W247.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.90E-02 1.93E-01 4.92E-02 1.06E+OO 1.90E-01 4.84E-02 2.21E-01 3.28E-01 O.OOE+OO 6.67E-02 1.54E-01 2.88E-02 7.32E-02 1.08E-01 O.OOE+OO 1.15E-01 2.40E-01 6.10E-02 7.29E-02 1.89E-01 4.34E-02 1.96-sigma cnt Unc pCi/G 6.88E-02 7.20E-01 2.20E-01 6.64E-02 7.29E-02 1.15E-01 7.26E-02 Alpha Spectrosccpy Software Version 3.5.3 effectiveda!e:02-Mar-2015 BATCH NUMBER : 1596390 SAMPLE ID : S1203621696 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 248 DETECTOR S/N : 87936 AVERAGE %EFFICIENCY : 26.0532 AVERAGE %EFF ERROR : 0.5047 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 59.2 +/-8.074 % TRACER ID 1752-C NUCLIDE AM-243 NOMINAL 4.7439E+OO dpm RESULTS 2.8083E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM AM-241 5480.15 5496.32 30.998 AM-243 5269.50 5278.36 30.308 CM-242 6102.00 6086.58 0.000 CM-3/4 5795.02 5807.03 55.086 CM-5/6 5386.00 5387.36 0.000 CM-247 4946.00 4881.20 0.000 CM-248 5078.60 5044.90 4.963 CM-247; 4775-4987 kaV 21 CM-248: 5009-5105 keV AM-243:5131-5366keV 19 CM-516: 5372-5398 keV AM-241:5404-5613kaV 17 CM-3f4:5646-5878keV CM*242:5975-6198keV 15 13 11 z =i 9 0 7 5 *:;; u 3 <l.'. 1 2383 2782 3184 3591 4002 4416 Energy (keV) COUNT DATE : 29-Sep-2016 21 :52:28 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0533-CC 1216-G NUCLIDE AM-241 CM-3/4 NOMINAL (pCi/G) 3.8691E+OO 5.1126E+OO % RECOVERY 94.153 103.746 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 153.000 150.120 2.880 1.6971 98.525 3.64E+OO 177.000 175.560 1.440 1.2000 99.980 4.20E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 222.000 221.760 0.240 0.4899 100.000 5.30E+OO 3.000 2.760 0.240 0.4899 86.090 7.66E-02 0.000 -0.960 0.960 0.9798 79.300 -2.89E-02 1.000 0.280 0.720 0.8485 91.000 7.36E-03 6546 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B248.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W248.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.38E-01 2.24E-01 7.54E-02 9.27E-01 1.77E-01 5.26E-02 4.92E-02 7.30E-02 O.OOE+OO 1.11E+OO 1.15E-01 2.15E-02 1.11E-01 1.33E-01 2.49E-02 6.72E-02 1.99E-01 5.41E-02 7.70E-02 1.60E-01 4.08E-02 1.96-sigma cnt Unc pCi/G 5.92E-01 6.26E-01 4.90E-02 7.00E-01 1.10E-01 6.71E-02 7.69E-02 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 23-Sep-2016 Product: ,>1\ty1Joro ' Date: Criteria: Yes No Comments Sample Solids are less than or eoual to 100 mo for GAB. Samples have been blank corrected (If required}. A.\').--Blank correction renorted Included (If reouiredl. If activity less than 10x MDA/MDC, error is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. .,,.. If be(nw th .. MnA I Mnr nrrnr i,; nk"u Instrument source check Is within limits. / Instrument him check Is within limits. Method RDL/ LLD has been met. ./ If duplicate activities are: Less than 5* MDA/ MDC, then RPD Is 100% or less, If greater S* MDA/ MDC, then RPD 20% or less, If below the MDA/ MDC, the RPD Is 0%, v Or meets the client's renuired RER accentance criteria. Tracer yleld Is 15-125%

Carrier yield 25-125%, (Or meets the client's contract acceptance criteria}. v Method blank Is less than the RDL/ LLD. v ()(,}tu J'\.rtt ;rr. h,"ho (lf .. C"mnlAC < 50/n nf )nouAct Samnle was run within hold time. ,/ 1\1.:0-\:b-1 l'{1:i.1 Samnle was correctly preserved If rcnulred. Smears Taken for Radioactive batches. ,V;y-Method Spike and LCS arc within 75-125% J 'or meets th" cll<'nt's cnntrart ac,,entance criteria\. No blank spaces on data forms. All line outs Initialed and dated. / Nn Arrnrc "rA Aux data Is correct. Client Soecial renulrements oane has been checked. / Raw Data and/ or snectrum :tre lnch*ded and nronerlv statused. ./ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / l"""'"""""m"rl 1 ..... rnmnlAto (If NG-nntnrn.I ln+n ...,..... Batch Data Excentlon Renorts fDER\ completed If aPPlicable. v-* IC60 Batch Data Exception Reports (DER) second reviewed. 1/ *tx:J'L4\:: i 8'D Dlsnosltlon verified to be comnleted. Alinuot Corrertlon comnleted If renuired. Li+ Review sample historical results If available v (If REMP, results above MDC have been verified bv historical results recount or re-analvsis. l Primary Review Performed _ Secondary Review Performed By:__ @ m 11 (_)( Page 749 of5809 10/02/16 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 25-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER HASL-300, Am-05-RC Solid Batch ID: Sample Numbers: 1599981 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075, 405235076, 405235077, 405235078, and 1203630764 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 25-SEP-16 Jessica Davis 02-0CT-16 Page 1 Page 750 of 5809 DER Report No.: 1561180 Revision No.: Type: Process Client Code: MJWC 0 >-+, Vl 00 0 '° Am/Cm Queue Sheet 19-SEP-16 ---*---*-----------------*--------------*---*-***--------* -------------------------Batch#: 1599981 Analyst: KXB2 First Client Due Date: 04-0CT-16 Internal Due Date:Ol-OCT-16 Comments: Tracer Code: \lSl-"_ 0 Expiration Date: Q *\l Vol: O. l *Analyzed Sequentially with U: ...... I \L...\\v*C:zi ExpirationDate:l-\-1.-\-\"l I "1*60-\VVol(s): 0-l t 0.\ Spike Isotope(s): Am241/Cm244 Spike Code(s): -I -Expiration Date: I -Vol(s): ! __ _ Prep ID: Witness: 9/U J J Pu: ___ _ Sample ID .Client Description 405235061-2 5.lB.R.2.2 4052.l5062-2 5.2.A.R.1.2 405235063-2 5.2.A.R.1.3 405235064-2 5.2.A.R.lA 405235065-2 5.2A.R.2.3 405235066-2 5.2.A.R.2A 405235067-2 5.2A.R.6.2 405235068-2 5.2A.R.4.2 405235069-2 5.2.B.R.1.4 405235070..2 5.2.B.R.3.2 405235071-2 5.2.B.R.4.2 405235072-2 5.2.B.R.2.4 405235073-2 5.2.B.R.8.2 405235074-2 5.3.A.R.l.3 405235075-2 5.4A.R.1.3 405235076-2 5.4A.R.4.2 405235077-2 5.5A.R.l.3 405235078-2 5.6A.R.1.3 1203630763-1 MB for batch 1599981 1203630764-2 5.1B.R.2.2(405235061DUP) 1203630765-1 _LCS for batch 1599981-Choose SOP GEL Laboratories LLC, Radiochemistry Division Type SAMPLE SAMPLE SAMPLE SAJMPLE SAMPLE SAMPLE SAl\fPLE SAMPLE SA!\.fPLE SA!\.fPLE SAMPLE SAl\fPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SA!\.fPLE MB DUP LCS Hazard Min Code CRDL Matrix 1 pCi/g SOIL lpCi/g SOIL lpCi/g SOIL lpCi/g SOIL lpCi/g SOIL lpCi/g SOIL 1 pCi/g SOIL lpCi/g SOIL 1 pCi/g SOIL lpCi/g SOIL lpCi/g SOIL lpCi/g SOIL 1 pCi/g SOIL lpCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL lpCi/g SOIL 1 pCJ/g SOIL UCF pCi/g to pCi/SOIL 1 pCi/g SOIL UCF pCi/g to pCi/SOIL Client l\fJWCOOl MJWCOOl MJWCOOl MJWCOOl lMJWCOOl l\fJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl l\fJWCOOl MJWCOOl MJWC001 QC ACCOUNT QC ACCOUNT QC ACCOUNT Solid Sample Dissolution DIGESTION Circle One Collection Date 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 11-DEC-15 11-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 11-DEC-15 15-DEC-15 16-DEC-15 11-DEC-15 17-DEC-15 17-DEC-15 14-DEC-15 Wet@ Label Aliquot Pos. # &YI/ f) Am/Cm Det# 1 2 3 4 5 6 7 8 9 17 18 116 \!)_ 10 L__J!_ __ i 19 I t9 l 'L _J_i-9_1 20 L2P ID-los ! °&'i I 21 I 1-Tl!) _ \CJ./}_ _l __ Data Reviewed By: <-J11j)qv,i)L,..£ "I /.:z_5 ) IL Page 1 ofl BATCH NUMBER : 1599981 SAMPLE ID : S0405235061_AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.111 G +/-0.901 % CHAMBER : 240 DETECTOR S/N : 87928 AVERAGE %EFFICIENCY : 25.5516 AVERAGE %EFF ERROR : 0.4953 SAMPLE DATE 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 94.9 +/-6.609 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5019E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5506.72 AM-243 5269.50 5272.21 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5371.03 CM-247 4946.00 4881.20 CM-248 5078.60 5087.60 CM-247* 4ns.4987 keV 25 1-CM-248: 5009-5105 keV 5131*5366 keV CM-516:5372-5398keV 22 1-AM-241! 54G4>5613 keV CM-314:5646-5878keV 19 r CM-242:5975-6198keV 16 r en 13 1--r z 10 0 r !2. 7 r *:;: 4 ti r <l'. f-I I I PEAK FWHM 79.495 40.933 0.000 0.000 0.000 0.000 29.811 I I I 23 84 2783 3187 3594 4004 4419 Energy (keV) COUNT DATE : 22-Sep-2016 17:53:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA* AREA AREA StDev pCi/G 2.000 2.000 0.000 0.0000 98.525 1.42E-01 276.000 276.000 0.000 0.0000 99.980 1.93E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 1.000 0.000 0.0000 86.090 8.10E-02 0.000 -0.480 0.480 0.6928 79.300 -4.22E-02 2.000 2.000 0.000 0.0000 91.000 1.53E-01 I I I I I I I I 4837 p26( E 86 611 p 6549 6986 7427 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B240.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W240.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.44E-01 2.13E-01 O.OOE+OO 3.47E+OO 2.09E-01 O.OOE+OO 4.71E-01 7.00E-01 O.OOE+OO 1.45E-01 2.16E-01 O.OOE+OO 2.28E-01 2.43E-01 O.OOE+OO 1.87E-01 4.87E-01 1.12E-01 2.63E-01 2.30E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.43E-01 2.28E+OO 4.70E-01 1.45E-01 2.28E-01 1.87E-01 2.63E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235062 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.110 G -+/-0.909 % CHAMBER : 241 DETECTOR S/N : 87963 AVERAGE %EFFICIENCY : 25.9137 AVERAGE %EFF ERROR : 0.5022 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.8 +/-6.834 % TRACER 1752-C. ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.1180E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5295.98 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5383.56 CM-247 4946.00 4973.08 CM-248 5078.60 5038.02 CM*247: 4n5-4987 keV 28 CM-248: 5009-5105 keV AM-243: 5131*5366 keV 25 CM-516: 5372-5398 keV AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV 22 CM-242:5975-619BkeV 19 0' 16 z 13 => 0 10 c 7 *:;; u 4 <( 1 PEAK FWHM 0.000 37.371 0.000 0.000 7.447 4.964 49.645 2406 2805 3208 3615 4025 4439 Energy (keV) COUNT DATE : 22-Sep-2016 17:53:42 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 98.525 -3.70E-02 257.000 256.040 0.960 0.9798 99.980 1.94E+01 0.000 -0.240 0.240 0.4899 100.000 -6.09E-02 0.000 -0.480 0.480 0.6928 100.000 -3.75E-02 6.000 6.000 0.000 0.0000 86.090 5.29E-01 1.000 0.760 0.240 0.4899 79.300 7.27E-02 3.000 2.760 0.240 0.4899 91.000 2.30E-01 6567 7004 7445 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B241.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W241.CNF;131 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.64E-01 4.27E-01 9.78E-02 3.63E+OO 5.00E-01 1.36E-01 5.26E-01 1.22E+OO 2.28E-01 1.66E-01 4.33E-01 9.92E-02 4.65E-01 2.64E-01 O.OOE+OO 2.73E-01 4.59E-01 8.58E-02 3.33E-01 4.00E-01 7.48E-02 1.96-sigma en! Une pCi/G 1.64E-01 2.39E+OO 5.25E-01 1.66E-01 4.59E-01 2.73E-01 3.31E-01 AfphaSpectroscopySoftwareVerslon3.5.3 effeclivedate:02-Mar-2015 BATCH NUMBER 1599981 SAMPLE ID S0405235063 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY 0.119 G -+/-0.840 % CHAMBER 242 DETECTOR S/N : 87930 AVERAGE %EFFICIENCY : 26.4545 AVERAGE %EFF ERROR : 0.5124 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 104 +/-6.282 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.9154E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5449.14 AM-243 5269.50 5265.21 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5369.37 CM-247 4946.00 4909.34 CM-248 5078.60 5051.63 31 CM-247; 4775-4987 keV CM-248: 5009-5105 keV 28 AM-243:5131*5366keV CM-516: 5372*5398 keV 25 AM-241: 5404-5613 keV CM-314:564S-5878keV CM-242: 597S-6198 keV 22 19 Ci) 16 I-z 13 ::> 0 s 10 0 7 *:;; ti 4 <( 1 PEAK FWHM 4.968 55.538 0.000 0.000 0.000 4.968 74.519 2377 2777 3180 3587 3998 4412 Energy (keV) COUNT DATE : 22-Sep-2016 17:53:46 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 1.000 0.000 0.0000 98.525 5.85E-02 312.000 312.000 0.000 0.0000 99.980 1.80E+01 0.000 -0.240 0.240 0.4899 100.000 -4.62E-02 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 2.000 2.000 0.000 0.0000 86.090 1.34E-01 1.000 1.000 0.000 0.0000 79.300 7.26E-02 2.000 2.000 0.000 0.0000 91.000 1.26E-01 > >>> = = 6542 6979 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B242.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W242.CNF;128 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.65E-01 1.75E-01 O.OOE+OO 3.07E+OO 1.73E-01 O.OOE+OO 3.99E-01 9.23E-01 1.73E-01 1.20E-01 1.78E-01 O.OOE+OO 2.30E-01 2.01E-01 O.OOE+OO 2.04E-01 2.18E-01 O.OOE+OO 2.17E-01 1.90E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.64E-01 2.00E+OO 3.98E-01 1.19E-01 2.29E-01 2.04E-01 2.17E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235064 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 243 DETECTOR S/N : 87931 AVERAGE %EFFICIENCY : 24.8977 AVERAGE %EFF ERROR : 0.4829 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 107 +/-6.369 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 5.0902E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5471.52 AM-243 5269.50 5282.63 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.63 CM-5/6 5386.00 5372.48 CM-247 4946.00 4980.01 CM-248 5078.60 5074.77 28 CM-247: 4775-4987 keV CM-248: 5009-5105 keV 25 AM-243: 5131-5366 keV CM-Sf6:5372-5398keV AM-241: 5404-5613 keV 22 CM-3f4:5646-5878keV CM-242:5975-6198keV 19 (ii 16 1--13 z :J 0 10 7 *:;: ti 4 <( PEAK FWHM 4.981 52.297 0.000 0.000 0.000 4.981 4.981 2389 2789 3193 3600 4011 4426 Energy (keV) COUNT DATE : 22-Sep-2016 17:53:48 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.040 0.960 0.9798 98.525 2.72E-03 306.000 304.080 1.920 1.3856 99.980 2.04E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.200 1.200 1.0954 100.000 -8.27E-02 3.000 3.000 0.000 0.0000 86.090 2.33E-01 1.000 0.520 0.480 0.6928 79.300 4.39E-02 1.000 0.760 0.240 0.4899 91.000 5.59E-02 > = = 6550 6986 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B243.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) .: 60000.00 EFF FILE : W243.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.02E-01 4.48E-01 1.22E-01 3.53E+OO 5.41E-01 1.70E-01 4.52E-01 6.71E-01 O.OOE+OO 1.57E-01 4.83E-01 1.38E-01 3.08E-01 2.33E-01 O.OOE+OO 2.44E-01 4.67E-01 1.07E-01 2.10E-01 3.53E-01 6.60E-02 1.96-sigma cnt Unc pCi/G 2.02E-01 2.30E+OO 4.51E-01 1.57E-01 3.07E-01 2.44E-01 2.10E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235065 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.112 G -+/-0.893 % CHAMBER : 244 DETECTOR S/N : 87932 AVERAGE %EFFICIENCY : 23.7184 AVERAGE %EFF ERROR : 0.4607 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 87.5 +/-7.070 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.1519E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.51 AM-243 5269.50 5283.93 CM-242 6102.00 6086.60 CM-3/4 5795.02 5726.99 CM-5/6 5386.00 5370.47 CM-247 4946.00 4890.01 CM-248 5078.60 5032.11 CM-247: 4n5-4987 keV 28 CM-248: 5009-5105 keV AM-243: 5131*5366 keV 25 CM-516: 5372*5398 keV AM-241: 54()4.5613 keV CM-3/4:5646-5878keV 22 CM*242:5975-6198keV 19 Ui 16 1--z 13 :::> 0 10 2:-7 *;;: n 4 <t: PEAK FWHM 0.000 24.993 0.000 64.981 0.000 104.969 4.999 2378 2779 3184 3592 4004 Energy (keV) COUNT DATE : 22-Sep-2016 17:53:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -1.200 1.200 1.0954 98.525 -9.85E-02 237.000 236.280 0.720 0.8485 99.980 1.91E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 2.000 2.000 0.000 0.0000 100.000 1.66E-01 2.000 2.000 0.000 0.0000 86.090 1.88E-01 2.000 -0.160 2.160 1.4697 79.300 -1.63E-02 1.000 -0.200 1.200 1.0954 91.000 -1.77E-02 6545 6980 7418 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B244.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W244.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.87E-01 5.75E-01 1.65E-01 3.69E+OO 4.93E-01 1.26E-01 5.46E-01 8.10E-01 O.OOE+OO 2.86E-01 2.50E-01 O.OOE+OO 3.23E-01 2.81E-01 O.OOE+OO 3.78E-01 8.54E-01 2.74E-01 2.67E-01 6.22E-01 1.78E-01 1.96-sigma cnt Unc pCi/G 1.87E-01 2.44E+OO 5.44E-01 2.85E-01 3.21E-01 3.77E-01 2.66E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235066 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 245 DETECTOR S/N : 87933 AVERAGE %EFFICIENCY : 25.3775 AVERAGE %EFF ERROR : 0.4920 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.0 +/-6.915 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.0815E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5270.53 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5376.71 CM-247 4946.00 4881 .21 CM-248 5078.60 5056.40 CM-247: 4n5-4987 keV 23 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 21 CM-515: 5372-5398 keV AM-241: 5404-5613 keV 19 CM-314: 5646-5878 keV CM-242: 5975-6198 keV 17 15 en I-13 z 11 ::::> 9 0 7 5 *:;; u 3 cl:: 1 PEAK FWHM 0.000 57.840 0.000 0.000 4.986 0.000 39.890 2375 2776 3180 3588 3999 4414 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 98.525 O.OOE+OO 249.000 248.520 0.480 0.6928 99.980 1.75E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 1.000 0.000 0.0000 86.090 8.19E-02 0.000 -0.240 0.240 0.4899 79.300 -2.13E-02 2.000 1.760 0.240 0.4899 91.000 1.36E-01 6542 6979 7419 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B245.CNF;455 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W245.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.45E-01 2.15E-01 0.00E+OO 3.31E+OO 3.90E-01 8.95E-02 4.76E-01 7.07E-01 O.OOE+OO 1.47E-01 2.18E-01 O.OOE+OO 2.30E-01 2.46E-01 O.OOE+OO 1.84E-01 4.26E-01 7.97E-02 2.69E-01 3.71E-01 6.95E-02 1.96-sigma cnt Unc pCi/G 1.44E-01 2.19E+OO 4.75E-01 1.46E-01 2.30E-01 1.84E-01 2.68E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235067 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 246 DETECTOR S/N : 87949 AVERAGE %EFFICIENCY : 25.1972 AVERAGE %EFF ERROR : 0.4886 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 118 +/-6.085 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 5.5868E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5498.98 AM-243 5269.50 5272.17 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5385.09 CM-247 4946.00 4911.78 CM-248 5078.60 5066.28 28 CM-247: 4775-4987 keV CM-248:5009-5105keV 25 AM-243: 5131-5366 keV CM*Sf6:53n-5398keV AM-241:S404-5613keV 22 CM-3/4: 5640-5878 keV CM-242:5975-6198keV 19 0' 16 z 13 ::::> 0 10 S2. 7 *:;; u 4 <( 1 PEAK FWHM 49.791 69.791 0.000 0.000 0.000 89.624 0.000 2375 2775 3179 3587 3998 4412 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.280 0.720 0.8485 98.525 7.76E-02 338.000 337.760 0.240 0.4899 99.980 2.02E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 2.000 2.000 0.000 0.0000 79.300 1.50E-01 6.000 6.000 0.000 0.0000 91.000 3.93E-01 6539 6975 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B246.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W246.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.14E-01 3.70E-01 9.43E-02 3.34E+OO 2.86E-01 5.36E-02 4.08E-01 6.06E-01 O.OOE+OO 1.24E-01 1.84E-01 O.OOE+OO 1.40E-01 2.08E-01 O.OOE+OO 2.59E-01 2.26E-01 O.OOE+OO 3.45E-01 1.97E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.14E-01 2.15E+OO 4.07E-01 1.24E-01 1.40E-01 2.58E-01 3.41E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235068 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 247 DETECTOR S/N : 87935 AVERAGE %EFFICIENCY : 26.2005 AVERAGE %EFF ERROR : 0.5076 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 100 +/-6.402 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.7569E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5275.06 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5375.68 CM-247 4946.00 4888.78 CM-248 5078.60 5061.11 CM 247' 4775-4987 keV 31 -CM-248: 5009-5105 keV AM-243: 5131-5366 keV 28 i-CM-516: 5372-5398 keV AM-241:5404-5613keV 25 f-CM-314:5646-5878keV CM-242:5975-6198keV 22 r en 19 I-16 f--f--z :::> 13 0 r 8 10 r 7 *::; ,__ ti 4 <( r r I I PEAK FWHM 0.000 40.288 0.000 0.000 0.000 139.555 0.000 I I 23 81 2781 3186 3594 4005 4421 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:39 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -1.200 1.200 1.0954 98.525 -8.38E-02 300.000 299.040 0.960 0.9798 99.980 2.05E+01 0.000 0.000 0.000 0.0000 100.000 0.00E+OO 0.000 -0.480 0.480 0.6928 100.000 -3.40E-02 3.000 3.000 0.000 0.0000 86.090 2.39E-01 3.000 2.280 0.720 0.8485 79.300 1.98E-01 3.000 2.520 0.480 0.6928 91.000 1.90E-01 m > ii=! a = II ,,1..*11 I I I' I I £ 840 526 p89 61n 6552 6990 7431 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B247.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W247.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.59E-01 4.90E-01 1.40E-01 3.59E+OO 4.53E-01 1.23E-01 4.70E-01 6.98E-01 O.OOE+OO 1.51E-01 3.92E-01 8.98E-02 3.17E-01 2.39E-01 O.OOE+OO 3.50E-01 5.29E-01 1.35E-01 3.03E-01 4.18E-01 9.58E-02 1.96-sigma cnt Unc pCi/G 1.59E-01 2.34E+OO 4.69E-01 1.50E-01 3.15E-01 3.49E-01 3.02E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235069 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 248 DETECTOR S/N : 87936 AVERAGE %EFFICIENCY : 26.0532 AVERAGE %EFF ERROR : 0.5047 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 98.1 +/-6.480 % TRACER .1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.6520E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5410.40 AM-243 5269.50 5279.31 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5373.19 CM-247 4946.00 4921.07 CM-248 5078.60 5058.09 31 CM-247: 4775-4987 keV CM-248:5009--5105keV 28 AM-243; 5131-5366 keV CM-5/6: 5372-5398 keV 25 AM-241: 5404-5613 keV CM-314: 5646-5878 keV CM-242: 5975-ti198 keV 22 19 (ii 16 I-z 13 ::i 0 10 7 *:;; t5 <l'. 4 1 PEAK FWHM 4.963 50.661 0.000 0.000 0.000 89.329 0.000 2383 2782 3184 3591 4002 Energy (keV) COUNT DATE : 22-Sep-201617:55:43 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.520 0.480 0.6928 98.525 3.73E-02 292.000 290.800 1.200 1.0954 99.980 2.05E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.200 1.200 1.0954 100.000 -8.73E-02 1.000 1.000 0.000 0.0000 86.090 8.21E-02 2.000 1.520 0.480 0.6928 79.300 1.35E-01 4.000 3.520 0.480 0.6928 91.000 2.73E-01 = = 6546 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B248.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W248.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.08E-01 3.98E-01 9.11E-02 3.63E+OO 4.96E-01 1.42E-01 4.73E-01 7.03E-01 O.OOE+OO 1.66E-01 5.10E-01 1.46E-01 2.31E-01 2.46E-01 O.OOE+OO 3.12E-01 4.93E-01 1.13E-01 3.48E-01 4.30E-01 9.85E-02 1.96-sigma cnt Unc pCi/G 2.07E-01 2.37E+OO 4.72E-01 1.65E-01 2.31E-01 3.11E-01 3.46E-01 0 ...., "' 00 0 '° BATCH NUMBER : 1599981 SAMPLE ID : S0405235070 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.113 G -+/-0.885 % CHAMBER : 249 DETECTOR S/N : 87937 AVERAGE %EFFICIENCY : 26.1419 AVERAGE %EFF ERROR : 0.5065 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 96.8 +/-6.492 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5916E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5265.02 CM-242 6102.00 6086.58 CM:3/4 5795.02 5736.69 CM-5/6 5386.00 5373.96 CM-247 4946.00 4961.38 CM-248 5078.60 5087.93 CM-247: 4775-4987 keV 31 CM-248: 5009-5105 keV AM-243*. 5131-5366 keV 28 CM-Sl6:53n-5398keV AM-241: 54(14.5613 keV 25 CM-3/4: 5646-5878 keV CM-242: 5975-0198 keV 22 en 19 I-16 z ::> 13 0 s 10 7 *:;; t5 4 <( PEAK FWHM 0.000 34.045 0.000 4.955 0.000 4.955 4.955 2375 2774 3176 3582 3993 4407 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:45 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 98.525 O.OOE+OO 288.000 288.000 0.000 0.0000 99.980 1.89E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 1.000 0.000 0.0000 100.000 6.77E-02 2.000 2.000 0.000 0.0000 86.090 1.53E-01 1.000 0.280 0.720 0.8485 79.300 2.32E-02 1.000 1.000 0.000 0.0000 91.000 7.21E-02 6536 6974 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B249.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W249.CNF;128 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.35E-01 2.00E-01 0.00E+OO 3.35E+OO 1.97E-01 O.OOE+OO 4.49E-01 6.67E-01 O.OOE+OO 1.90E-01 2.03E-01 O.OOE+OO 2.62E-01 2.29E-01 O.OOE+OO 2.43E-01 5.06E-01 1.29E-01 2.03E-01 2.16E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.34E-01 2.19E+OO 4.48E-01 1.90E-01 2.61E-01 2.42E-01 2.03E-01 1599981 S0405235071 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER SAMPLE ID SAMPLE QTY SAMPLE DATE ANALYST % YIELD 0.120 G -+/-0.833 % CHAMBER : 250 DETECTOR S/N : 87938 AVERAGE %EFFICIENCY : 26.3779 AVERAGE %EFF ERROR : 0.5108 11-Dec-2015 00:00:00 KXB2 91.4 +/-6.629 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.3375E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5275.36 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5380.77 CM-247 4946.00 4910.38 CM-248 5078.60 5057.87 37 CM-247* 47754987 keV CM-248: 5009-5105 keV AM-243: 5131*5366 keV 33 f-CM-516:5372-5398keV AM-241: 5404-5613 keV 29 i-CM-314: 5646-5878 keV CM-242: 597fKj198 keV 25 r 'iii 21 f-I-z 17 f-::i 0 13 f-9 f-*::; u 5 f-<( r I I I 23 74 2773 3176 3583 Energy (keV) PEAK FWHM 0.000 18.744 0.000 0.000 0.000 4.968 4.968 I 3994 4408 COUNT DATE : 22-Sep-2016 17:55:47 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 98.525 -3.16E-02 275.000 274.520 0.480 0.6928 99.980 1.78E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.720 0.720 0.8485 100.000 -4.81E-02 2.000 2.000 0.000 0.0000 86.090 1.51E-01 1.000 0.280 0.720 0.8485 79.300 2.29E-02 1.000 0.280 0.720 0.8485 91.000 2.00E-02 .11 I I I 4826 J24E 5 74 610 6536 6973 7414 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B250.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W250.CNF;115 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.40E-01 3.65E-01 8.36E-02 3.22E+OO 3.59E-01 8.23E-02 4.44E-01 6.59E-01 O.OOE+OO 1.46E-01 4.08E-01 1.04E-01 2.59E-01 2.26E-01 O.OOE+OO 2.40E-01 5.00E-01 1.27E-01 2.09E-01 4.35E-01 1.11E-01 1.96-sigma cnt Unc pCi/G 1.40E-01 2.11E+OO 4.43E-01 1.45E-01 2.58E-01 2.39E-01 2.09E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235072 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 251 DETECTOR S/N : 87939 AVERAGE %EFFICIENCY : 25.8839 AVERAGE %EFF ERROR : 0.5015 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 98.9 +/-6.470 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.6902E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5512.29 AM-243 5269.50 5263.64 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5385.09 CM-247 4946.00 4907.77 CM-248 5078.60 5021.17 CM 247* 4775-4987 keV CM-248: 5009-5105 keV 28 AM-243: 5131-5366 keV CM-516: 5372-5398 keV 25 AM-241: 5404-5613 keV CM-3/4: 5645-5878 keV 22 I-CM-242: 5975-6198 keV 19 Ui 16 I--z 13 :::> 0 10 s -.c *:;; 7 u 4 <t: -I I I PEAK FWHM 4.963 40.696 0.000 0.000 0.000 44.666 0.000 I I I 23 70 2769 3172 3579 3990 4405 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:50 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 -0.200 1.200 1.0954 98.525 -1.48E-02 292.000 291.280 0.720 0.8485 99.980 2.12E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.960 0.960 0.9798 100.000 -7.18E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 3.000 3.000 0.000 0.0000 79.300 2.75E-01 2.000 1.520 0.480 0.6928 91.000 1.21E-01 I II I I I II I I I I 4S24 p24E 5 73 610' 6538 6976 7418 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B251.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W251.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.22E-01 5.18E-01 1.48E-01 3.74E+OO 4.44E-01 1.13E-01 4.89E-01 7.26E-01 O.OOE+OO 1.67E-01 4.93E-01 1.34E-01 1.70E-01 2.53E-01 O.OOE+OO 3.63E-01 2.75E-01 0.00E+OO 2.79E-01 4.42E-01 1.01E-01 1.96-sigma cnt Unc pCi/G 2.22E-01 2.44E+OO 4.88E-01 1.66E-01 1.70E-01 3.62E-01 2.79E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235073 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 252 DETECTOR S/N : 87940 AVERAGE %EFFICIENCY : 26.3006 AVERAGE %EFF ERROR : 0.5094 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 91.5 +/-6.640 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.3427E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5504.79 AM-243 5269.50 5240.74 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5385.09 CM-247 4946.00 4900.83 CM-248 5078.60 5085.42 21 CM-247: 4775-4987 keV CM-248: 5009-5105 keV 19 AM-243: 5131-5366 keV CM-Sib: 5372-5398 keV 17 AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV CM-+242: keV 15 13 en 11 I-z 9 :::i 0 7 5 *s: u 3 <t: PEAK FWHM 54.628 62.905 0.000 0.000 0.000 34.763 0.000 2384 2783 3187 3594 4004 4419 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:53 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 2.000 0.000 0.0000 98.525 1.47E-01 275.000 274.040 0.960 0.9798 99.980 1.98E+01 0.000 -0.480 0.480 0.6928 100.000 -1.17E-01 0.000 -0.720 0.720 0.8485 100.000 -5.36E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 2.000 1.520 0.480 0.6928 79.300 1.38E-01 4.000 3.760 0.240 0.4899 91.000 2.98E-01 6551 6988 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B252.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W252.CNF;127 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCl/G pCi/G 2.52E-01 2.20E-01 O.OOE+OO 3.59E+OO 4.76E-01 1.30E-01 5.20E-01 1.35E+OO 3.10E-01 1.62E-01 4.54E-01 1.16E-01 1.69E-01 2.52E-01 O.OOE+OO 3.18E-01 5.04E-01 1.16E-01 3.54E-01 3.80E-01 7.12E-02 1.96-sigma cnt Unc pCi/G 2.51E-01 2.35E+OO 5.19E-01 1.62E-01 1.69E-01 3.18E-01 3.52E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235074 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.115 G -+/-0.870 % CHAMBER : 253 DETECTOR SIN : 87941 AVERAGE %EFFICIENCY : 25.6727 AVERAGE %EFF ERROR : 0.4975 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.4 +/-6.681 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.3839E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5273.86 CM-242 6102.00 6086.59 CM-3/4 5795.02 5729.49 CM-5/6 5386.00 5371.84 CM-247 4946.00 4855.09 CM-248 5078.60 5070.91 -CM-247* 4775-4987 k V . CM-248; 5009-5105 keV 25 AM-243: 5131*5366 keV CM-516: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-3/4:564S-5878keV CM-242: 5975-6198 keV 19 -0' 16 z 13 --::> 0 10 -8 7 -*:; 4 n -<!'. 11 I I I PEAK FWHM 0.000 49.136 0.000 4.985 0.000 64.803 39.878 I I I I 23 68 2769 3173 3581 3993 4408 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA SIDev pCi/G 0.000 -0.480 0.480 0.6928 98.525 * -3.36E-02 271.000 270.040 0.960 0.9798 99.980 1.86E+01 0.000 -0.240 0.240 0.4899 100.000 -5.50E-02 1.000 0.760 0.240 0.4899 100.000 5.39E-02 1.000 1.000 0.000 0.0000 86.090 7.99E-02 3.000 2.280 0.720 0.8485 79.300 1.98E-01 4.000 3.760 0.240 0.4899 91.000 2.84E-01 Ill Ill 1U I I I I I I I p25( 5 76 p10 6540 6977 7418 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B253.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W253.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.49E-01 3.87E-01 8.87E-02 3.39E+OO 4.53E-01 1.24E-01 4.75E-01 1.10E+OO 2.06E-01 2.02E-01 3.40E-01 6.36E-02 2.25E-01 2.40E-01 O.OOE+OO 3.51E-01 5.30E-01 1.35E-01 3.37E-01 3.62E-01 6.78E-02 1.96-sigma cnt Unc pCl/G 1.48E-01 2.23E+OO 4.74E-01 2.02E-01 2.25E-01 3.50E-01 3.35E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235075 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.112 G -+/-0.893 % CHAMBER : 254 DETECTOR S/N : 87942 AVERAGE %EFFICIENCY : 25.1642 AVERAGE %EFF ERROR : 0.4879 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 104 +/-6.398 % 1752-C TRACER , ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.9482E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5473.21 AM-243 5269.50 5281.41 CM-242 6102.00 6086.59 CM-3/4 5795.02 5801.99 CM-5/6 5386.00 5376.52 CM-247 4946.00 4793.43 CM-248 5078.60 5104.34 CM-247: 4n5-4987 keV 28 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 25 CM-516: 5372-5398 keV AM-241: 5404-5613 keV CM-314:5646-5878keV 22 CM-242:5975-6198keV 19 Ui 16 I-z 13 ::> 0 10 c 7 *:;: u 4 <! PEAK FWHM 79.602 27.541 0.000 4.975 0.000 4.975 0.000 2385 2785 3188 3596 4007 4422 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:56 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.520 0.480 0.6928 98.525 9.86E-02 299.000 298.760 0.240 0.4899 99.980 1.91E+01 0.000 -0.240 0.240 0.4899 100.000 -5.08E-02 1.000 0.280 0.720 0.8485 100.000 1.84E-02 3.000 2.760 0.240 0.4899 86.090 2.05E-01 1.000 0.520 0.480 0.6928 79.300 4.19E-02 1.000 0.760 0.240 0.4899 91.000 5.33E-02 > .l1 = 6553 6991 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B254.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W254.CNF;116 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.27E-01 3.59E-01 8.23E-02 3.33E+OO 3.06E-01 5.73E-02 4.39E-01 1.02E+OO 1.90E-01 1.93E-01 4.02E-01 1.02E-01 2.96E-01 3.56E-01 6.66E-02 2.33E-01 4.46E-01 1.02E-01 2.00E-01 3.36E-01 6.30E-02 1.96-sigma cnt Unc pCi/G 2.27E-01 2.17E+OO 4.38E-01 1.92E-01 2.95E-01 2.33E-01 2.00E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235076 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 255 DETECTOR S/N : 87943 AVERAGE %EFFICIENCY : 24.9747 AVERAGE %EFF ERROR : 0.4844 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 103 +/-6.447 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.8983E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5277.11 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5369.33 CM-247 4946.00 4881.20 CM-248 5078.60 5065.47 31 CMZ47*4775-4987keV CM-248; 5009-5105 keV AM-243: 5131-5366 keV 28 CM>S/6: 5372-5398 keV AM-241: 5404-5613 keV 25 -CM-3'4: 5646-5878 keV CM*242:5975-0198keV 22 -en 19 1--16 --z :J 13 0 f-S?. 10 f-0 7 *;;; -u 4 <( -f-I I PEAK FWHM 0.000 33.145 0.000 0.000 0.000 0.000 0.000 I I 23 77 2776 3180 3588 3999 4415 Energy (keV) COUNT DATE : 22-Sep-2016 17:55:59 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 98.525 -3.35E-02 294.000 293.520 0.480 0.6928 99.980 2.02E+Ci1 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -3.40E-02 2.000 2.000 0.000 0.0000 86.090 1.60E-01 0.000 -0.240 0.240 0.4899 79.300 -2.08E-02 5.000 4.280 0.720 0.8485 91.000 3.23E-01 >>>> 'i ]!!l!l!l = = I I I "' 'IU I II I I I I p251 ' 85 611 s 6551 6990 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B255.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W255.CNF;120 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.48E-01 3.86E-01 8.86E-02 3.54E+OO 3.80E-01 B.72E-02 4.70E-01 6.98E-01 O.OOE+OO 1.50E-01 3.92E-01 8.98E-02 2.74E-01 2.39E-01 O.OOE+OO 1.BOE-01 4.15E-01 7.77E-02 3.72E-01 4.61E-01 1.17E-01 1.96-sigma cnt Unc pCi!G 1.48E-01 2.31E+OO 4.69E-01 1.50E-01 2.73E-01 1.79E-01 3.69E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235077 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 256 DETECTOR S/N : 87944 AVERAGE %EFFICIENCY : 25.7507 AVERAGE %EFF ERROR : 0.4991 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 97.1 +/-6.542 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.6057E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5280.15 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5370.73 CM-247 4946.00 4986.00 CM-248 5078.60 5075.57 CM-247: 4n5-4987 keV 28 CM-248: 5009-5105 keV AM-243: 5131*5366 keV 25 CM-516: 5372-5398 keV AM-241: 54Q4.5613 keV CM-3/4: 5646-5878 keV 22 CM*242:5975-6198keV 19 w 16 I-z 13 ::J 0 10 2-.?;> 7 *s; u 4 <t: 1 PEAK FWHM 0.000 34.631 0.000 0.000 0.000 0.000 19.821 COUNT DATE : 22-Sep-2016 17:56:01 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.240 0.240 0.4899 98.525 -1.78E-02 286.000 284.560 1.440 1.2000 99.980 2.07E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.480 0.480 0.6928 100.000 -3.60E-02 7.000 7.000 0.000 0.0000 86.090 5.93E-01 2.000 0.800 1.200 1.0954 79.300 7.35E-02 2.000 1.520 0.480 0.6928 91.000 1.22E-01 2372 2771 3173 3579 3989 4403 4 20 6530 6967 7407 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B256.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W256.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.54E-01 3.55E-01 6.65E-02 3.70E+OO 5.39E-01 1.60E-01 4.86E-01 7.22E-01 O.OOE+OO 1.60E-01 4.16E-01 9.53E-02 4.78E-01 2.54E-01 O.OOE+OO 3.30E-01 6.45E-01 1.84E-01 2.80E-01 4.44E-01 1.02E-01 1.96-sigma cnt Unc pCi/G 1.53E-01 2.42E+OO 4.85E-01 1.59E-01 4.71E-01 3.30E-01 2.80E-01 BATCH NUMBER : 1599981 SAMPLE ID : S0405235078 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.107 G -+/-0.935 % CHAMBER : 078 DETECTOR S/N : 38633 AVERAGE %EFFICIENCY : 33.4433 AVERAGE %EFF ERROR : 0.6444 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 102 +/-5.754 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.8354E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5501.73 AM-243 5269.50 5259.96 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5385.09 CM-247 4946.00 4954.35 CM-248 5078.60 5053.64 -CM 247* 4n5-4987 keV CM-248: 5009-5105 keV 33 1-AM-243: 5131-5366 keV CM-Sf6:5372-5398keV AM-241:5404-5613keV 29 1-CM-3(4: 5646-5878 keV CM-242:597s.£198keV 25 Ci) 21 1--17 z :::i 0 13 s 9 *:;; 5 . , I I PEAK FWHM 4.964 51.786 0.000 0.000 0.000 24.818 7.445 I 23 88 2787 3190 3597 4009 4424 Energy (keV) COUNT DATE : 22-Sep-2016 17:52:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 1.000 0.520 0.480 0.6928 98.525 2.72E-02 388.000 388.000 0.000 0.0000 99.980 2.00E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.960 0.960 0.9798 100.000 -5.09E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 2.000 1.520 0.480 0.6928 79.300 9.86E-02 9.000 8.760 0.240 0.4899 91.000 4.95E-01 ..I

I I I I 026 l p95 6126 6562 7002 7445 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B078.CNF;1726 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W078.CNF;447 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.51E-01 2.90E-01 6.64E-02 3.12E+OO 1.54E-01 O.OOE+OO 3.43E-01 5.10E-01 0.00E+OO 1.18E-01 3.49E-01 9.51E-02 1.21E-01 1.79E-01 O.OOE+OO 2.27E-01 3.59E-01 8.24E-02 3.58E-01 2.71E-01 5.07E-02 1.96-sigma cnt Unc pCi/G 1.51E-01 1.99E+OO 3.43E-01 1.18E-01 1.21E-01 2.27E-01 3.53E-01 BATCH NUMBER : 1599981 SAMPLE ID : S1203630763 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 080 DETECTORS/N : 78197 AVERAGE %EFFICIENCY : 34.4422 AVERAGE %EFF ERROR : 0.6633 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 99.3 +/-5.757 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7439E+OO dpm 4.7108E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.48 AM-243 5269.50 5276.94 CM-242 6102.00 6086.57 CM-3/4 5795.02 5645.33 CM-5/6 5386.00 5376.45 CM-247 4946.00 4889.30 CM-248 5078.60 5064.00 CM-247: 4775-4987 keV CM-248: SOOS-5105 keV 33 AM-243: 5131-5366 keV CM-5/6;5J72*5398keV Mf..241:5404-5613keV 29 CM-J/4; 5646-5876 keV CM-242:597S-6198keV 25 'Ci) 21 1--17 z ::::> 0 13 s 9 *s: u 5 <t: PEAK FWHM 0.000 42.115 0.000 0.000 0.000 4.969 0.000 2386 2786 3190 3598 4011 Energy (keV) COUNT DATE : 22-Sep-2016 17:52:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 98.525 -3.29E-02 391.000 389.320 1.680 1.2961 99.980 1.75E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 1.000 0.000 0.0000 100.000 4.50E-02 7.000 6.520 0.480 0.6928 86.090 3.41E-01 5.000 4.760 0.240 0.4899 79.300 2.70E-01 10.000 9.760 0.240 0.4899 91.000 4.82E-01 6578 7021 7468 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B080.CNF;1728 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W080.CNF;446 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.94E-02 2.79E-01 7.10E-02 2.73E+OO 3.49E-01 1.07E-01 9.15E-02 1.36E-01 O.OOE+OO 1.27E-01 1.35E-01 O.OOE+OO 2.96E-01 2.89E-01 6.63E-02 2.77E-01 2.72E-01 5.09E-02 3.28E-01 2.37E-01 4.44E-02 1.96-sigma cnt Unc pCi/G 9.93E-02 1.75E+OO 9.14E-02 1.26E-01 2.93E-01 2.75E-01 3.23E-01 BATCH NUMBER : 1599981 SAMPLE ID : S1203630764 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 081 DETECTOR S/N : 79996 AVERAGE %EFFICIENCY : 33.0506 AVERAGE %EFF ERROR : 0.6369 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 103 +/-5.769 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.8777E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5448.15 AM-243 5269.50 5263.62 CM-242 6102.00 6086.56 CM-3/4 5795.02 5761.58 CM-5/6 5386.00 5378.72 CM-247 4946.00 4916.47 CM-248 5078.60 5065.23 CM-247: 4775-4967 keV CM-248: 5009-5105 keV 33 AM-243: 5131-5366 keV CM-516: 5372-5398 keV AM-241: 5404-5613 keV 29 CM-3/4: 564S-587B keV CM-242: 597!Hi198 keV 25 Ui 21 t-17 z => 0 13 f2, 9 *:;; n 5 <x: PEAK FWHM 4.901 41.462 0.000 0.000 4.901 0.000 17.154 2384 2779 3178 3582 3991 4404 Energy (keV) COUNT DATE : 22-Sep-2016 17:52:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 1.000 0.000 0.0000 98.525 5.35E-02 388.000 386.800 1.200 1.0954 99.980 2.04E+01 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.240 0.240 0.4899 100.000 -1.30E-02 1.000 1.000 0.000 0.0000 86.090 6.11E-02 6.000 4.560 1.440 1.2000 79.300 3.02E-01 9.000 8.280 0.720 0.8485 91.000 4.79E-01 6543 6985 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B081.CNF;1734 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W081.CNF;446 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.50E-01 1.60E-01 O.OOE+OO 3.19E+OO 3.69E-01 1.06E-01 3.55E-01. 5.28E-01 O.OOE+OO 1.12E-01 2.60E-01 4.86E-02 1.72E-01 1.83E-01 O.OOE+OO 3.56E-01 4.91E-01 1.46E-01 3.67E-01 3.53E-01 8.99E-02 1.96-sigma cnt Unc pCi/G 1.50E-01 2.03E+OO 3.55E-01 1.12E-01 1.72E-01 3.54E-01 3.62E-01 BATCH NUMBER : 1599981 SAMPLE ID : S1203630765 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 082 DETECTOR S/N : 79997 AVERAGE %EFFICIENCY : 31.9848 AVERAGE %EFF ERROR : 0.6168 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 108 +/-5.757 % TRACER ID 1752-C NUCLIDE AM-243 NOMINAL 4.7439E+OO dpm RESULTS 5.1165E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM AM-241 5480.15 5490.15 48.584 AM-243 5269.50 5265.96 47.608 CM-242 6102.00 6146.02 4.883 CM-3/4 5795.02 5798.79 58.576 CM-5/6 5386.00 5387.15 9.766 CM-247 4946.00 4921.16 7.324 CM-248 5078.60 5064.02 48.015 37 CM-+247: 4775-4987 keV CM-248: 5009-5105 keV AM-243: 5131*5356 keV 33 CM-5/6: 5372-5398 keV AM-241:5404-5613keV 29 CM+314:5646-5878keV CM-242: keV 25 Ui 21 I-z 17 :J 0 13 f2, 9 *:;; u 5 <( 2394 2787 3185 3588 Energy (keV) COUNT DATE : 22-Sep-2016 17:52:55 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0533-CC 1216-G NUCLIDE AM-241 CM-3/4 NOMINAL (pCi/G) 1.6143E+01 2.1342E+01 % RECOVERY 102.288 96.985 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 366.000 364.800 1.200 1.0954 98.525 1.65E+01 397.000 392.680 4.320 2.0785 99.980 1.75E+01 1.000 0.760 0.240 0.4899 100.000 3.42E-02 465.000 464.040 0.960 0.9798 100.000 2.07E+01 12.000 12.000 0.000 0.0000 86.090 6.22E-01 8.000 5.840 2.160 1.4697 79.300 3.28E-01 19.000 18.520 0.480 0.6928 91.000 9.08E-01 'ffi :;l:';I $ :g 6545 6987 7434 , ; u u u u Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B082.CNF;1724 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W082.CNF;423 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.61E+OO 3.17E-01 9.08E-02 2.73E+OO 4.73E-01 1.70E-01 1.28E-01 2.15E-01 4.03E-02 3.12E+OO 2.94E-01 8.01E-02 3.74E-01 1.55E-01 O.OOE+OO 3.43E-01 4.72E-01 1.51E-01 4.45E-01 2.71E-01 6.22E-02 1.96-sigma cnt Unc pCi/G 1.70E+OO 1.75E+OO 1.28E-01 1.89E+OO 3.67E-01 3.41E-01 4.31E-01 Effective 3/25/201 O Revision 1 Effective March 201 O Radiochemistry Batch Checklist 23-Sep-2016 Batch#_! Product:_-"-e_1_,,_l __ Date: q/81 )I \fl Criteria: Yes No Comments Sam11lc Solids are less than or e11ual to lOD mil for GAD. 11f>A Samples have been blank corrected (If required). IV{\ Blank correction renorted Included rrr reoulredl. [f activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. ........ !-'> If areater than 10* MDA/ MDC, error Is 40% or less. 'rt..,-*-*** .... _ uro.A. / ..... ,. error Is nllav. Im;trument source check Is within limits. '-... ..._;, Ins*rumnnt bkn check Is within limits. Method RDL/ LLD has been met. .......... [f duplicate activities arc: Less than 5* MDA/ MDC, then RPO Is 100% or less, 'to-" Xf greater 5* MDA/ MDC, then RPD 20% or less, If below the MDA/ MDC, the RPO Is 00/o, Or meets the client's reoulred RER acceotance criteria. Tracer yield Is 15-125%
Carrier vleld 25*125%, "' I'. (Or meets the client's contract acceptance criteria). " Method blank Is less than the RDL/ LLD
l/Tr--.a ---.-0:01-nf *-***--* "ctlvllv\ \ £1-:Yl# IS L I G I Samnfe was run within hold time. ,..,. ' Samolc was correctlv orcservcd If reoulred. ('--1--J. PM Smears Taken for Radioactive batches. '\\ v (\ff'"'\ Method Spike and LCS are within 75-125% " !.....> ltnr meets the client's contract acccntance criteria\. No blank spaces on data forms. . ....... N All llne outs Initialed and dated. I**---------I Aux data Is correct. ' rJtt\ 1---..:. Client Sneclal reoulrements oaoe has been checked. ' 1---.. Raw Data and I or snectrum are Included and nronerlu statused * -MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ... "-..... .. v--*n-.a -Ult -/IF f\f Y-1 n nn*n*n.I "---W Batch Data Excentlon Renorts IDER\ completed. If applfcable. .. __ {)?/\ :Ii I s l* I 6 / .S Batch Data Exception Reports (DER) second reviewed. '--....._. Ot:l\ft l$L? }G/....S Dlsnosltlon verified to be comnleted. Alinnot CorTec*lon rnn'\nh>ted If reaulrnd. (y)f\ . ........... Review sample hlstorlcal results If avallable !'--> (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. \ Primary Review Performed By: Ll>>I 1'!Jh /1X1hv 09/29/16 f[OWC Page 773 of 5809 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 27-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, Pu-11-RC Solid . Batch ID: Sample Numbers: 1596400 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, and 1203621719 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Jessica Downey 27-SEP-16 Jessica Davis 29-SEP-16 Page 1 Page 774 of 5809 DER Report No.: 1561615 Revision No.: 1 Type: Process Client Code: MJWC Plutonium Queue Sheet --------*------Batch #:

1596400 Analyst: .MXS2 First Client Due Date:04-0CT-16 Expiration Date: 'i?-3-/7 Expiration Date: 7* z.a -17 Tracer Tracer __ LCS Isotope(s): LCS Code:. __ *-Spike Isotope(s): Pu-239/Pu-238 Spike Code: ______ _ Expiration Date:-07-SEP-16 Internal Due Date:30-SEP-16 Vol:.i2.:l_ Analyzed Sequentially with: Vol: o. / U: Am: Prep Date: q -Z.J 11...p Initials: ,A/ZS b PipetID: Balance ID: , Cc l01Cf Ct2_., Witness:....,jJ,<.>e+k-'-----Hazard Min Sample ID Client Description Type Code CRDL Matrix 405235021-1 4.2B.R.2.3 SAMPLE 1 pCi/g SOIL 405235022-1 4.2B.R.1.3 SAMPLE 1 pCI/g SOIL 405235023-1 4.2B.R.11.2 SAMPLE lpCi/g SOIL 405235024-1 4.2B.R.2.2 SAl\fPLE 1 pCi/g SOIL 405235025-1 4.2B.R.1.2 SAMPLE 1 pCI/g SOIL 405235026-1 4.2C.R.U SAMPLE 1 pCI/g SOIL 405235027-1 4.2C.R.l.4 SAMPLE 1 pCi/g SOIL 405235028-1 4.3.ARl-l SM:IPLE 1 pCi/g SOIL 405235029-1 4.3.B.R.1.3 SAMPLE l pCi/g SOIL 405235030-1 4.3A.R.2-l SAMPLE 1 pCi/g SOIL 405235031-1 4.3.BR19.2 SAMPLE 1 pCi/g SOIL 405235032-1 4.3B.R.3.3 SAMPLE 1 pCi/g SOIL 405235033-1 4.3B.R.3.4 SMfPLE 1 pCi/g SOIL 405235034-1 4.3.B.R.1.4 SA!l-1PLE 1 pCi/g SOIL 405235035-1 4.3B.R.2.3 SAMPLE 1 pCi/g SOIL 405235036-1 4.3B.R.2.4 SAMPLE 1 pCI/g SOIL 405235037-1 4.4C.R.2.4 SAl\fPLE lpCi/g SOIL 405235038-1 4.4C.R.l.3 SAMPLE 1 pCI/g SOIL 405235039-1 4.4C.R.l.4 SAtW>LE 1 pCI/g SOIL 405235040-1 4.4D.R.1.3 SAMPLE 1 pCi/g SOIL 1203621718-1 1"IB for batch 1596400 MB 1 pCi/g SOIL 1203621719-1 4.2B.R.2.3(405235021DUP) DUP 1 pCi/g SOIL 1203621720-1 LCS for batch 1596400 LCS 1 pCi/g SOIL Choose SOP Solid Sample Dissolution by: LEACH ' GEL Laboratories LLC, , Radiochemistry Divisio11 Client MJWC001 MJWCOOl l\:fJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWC001 MJWCOOl MJWCOOl lHJWCOOl MJWCOOl MJWCOOl MJWCOOl l\UWCOOl MJWC001 MJWCOOl MJWCOOl MJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Collection Date 08-DEC-15 08-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 23-NOV-15 23-NOV-15 23-NOV-15 26-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 08-DEC-15 -** .... Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Label # Aliquot I If) Pu Det# Page: 1 of l BATCH NUMBER : 1596400 SAMPLE ID : S0405235021_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 089 DETECTOR S/N : 79988 AVERAGE %EFFICIENCY : 29.2461 AVERAGE %EFF ERROR : 0.5651 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 72.2 +/-7.136 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.1634E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5744.73 PU-238 5486.00 5484.82 PU-239 5155.00 5195.39 PU-242 4890.00 4876.70 PU-244 4589.00 4554.41 PU-244: 4497-4597 keV 15 PU-242: 4654-4995 keV PU-239: 5011-5227 keV PU-238: 5375-5566 keV 13 PU-236: 5582-5843 keV 11 (j) 9 I-z 7 :::i 0 s 5 a *:;; ti 3 <( 2394 2791 3193 Energy (keV) PEAK FWHM 192.598 123.460 24.692 75.558 74.076 COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 5.000 -1.240 6.240 2.4980 100.000 -2.60E-02 3.000 1.080 1.920 1.3856 99.900 1.88E-02 3.000 -0.120 3.120 1.7664 99.900 -2.08E-03 229.000 222.040 6.960 2.6382 100.000 3.84E+OO 3.000 1.320 1.680 1.2961 99.900 2.29E-02 >> :g:g 6110 6543 6980 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B089.CNF;1435 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W089.CNF;384 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.13E-01 2.55E-01 9.61E-02 7.27E-02 1.41E-01 4.42E-02 7.45E-02 1.64E-01 5.60E-02 7.59E-01 2.19E-01 8.36E-02 7.18E-02 1.34E-01 4.11E-02 1.96-sigma cnt Unc pCi/G 1.13E-01 7.26E-02 7.44E-02 5.16E-01 7.17E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235022 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 090 DETECTOR S/N : 78263 AVERAGE %EFFICIENCY : 33.4344 AVERAGE %EFF ERROR : 0.6443 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 69.9 +/-6.695 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.0627E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5643.27 PU-238 5486.00 5470.34 PU-239 5155.00 5110.12 PU-242 4890.00 4872.46 PU-244 4589.00 4518.38 PU-244: 4497-4597 keV 17 PU-242: 4654-4995 keV PlJ.239;5011*5227keV PU-238: 5375-5566 keV 15 PU-236: 5582-5843 keV 13 11 Ci) 9 I-z :J 7 0 5 c *;;; 3 t5 <l.'. PEAK FWHM 39.587 0.000 4.948 57.731 4.948 2398 2796 3199 3606 4018 Energy {keV) COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.520 0.480 0.6928 100.000 2.94E-02 0.000 -0.960 0.960 0.9798 99.900 -1.54E-02 1.000 0.040 0.960 0.9798 99.900 6.37E-04 246.000 245.760 0.240 0.4899 100.000 3.91E+OO 1.000 0.520 0.480 0.6928 99.900 8.28E-03 > 6145 6584 7028 7476 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B090.CNF;1440 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W090.CNF;374 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.75E-02 1.07E-01 2.45E-02 3.57E-02 1.06E-01 2.88E-02 4.73E-02 1.05E-01 2.86E-02 7.25E-01 7.63E-02 1.43E-02 4.61E-02 8.82E-02 2.02E-02 1.96-sigma cnt Unc pCi/G 6.74E-02 3.56E-02 4.72E-02 4.90E-01 4.60E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235023 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 091 DETECTOR S/N : 78259 AVERAGE %EFFICIENCY : 34.7245 AVERAGE %EFF ERROR : 0.6687 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 68.9 +/-6.641 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.0185E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5704.53 PU-238 5486.00 5498.56 PU-239 5155.00 5118.68 PU-242 4890.00 4856.68 PU-244 4589.00 4510.45 17 PU-244: 4497-4597 keV PU-242:4654-4995keV PU-239:5011-5227keV 15 PU-238:5375-5566keV PU-236: 5582-5843 keV 13 11 'iii 9 1--z ::i 7 0 !2-5 ;:. *:;: 3 u <l'. 2382 2779 3180 Energy (keV) PEAK FWHM 4.930 83.811 0.000 68.610 14.790 COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.280 0.720 0.8485 100.000 5.31E-03 3.000 2.040 0.960 0.9798 99.900 3.20E-02 0.000 -0.480 0.480 0.6928 99.900 -7.48E-03 253.000 251.560 1.440 1.2000 100.000 3.92E+OO 3.000 2.760 0.240 0.4899 99.900 4.30E-02 >> > ] ] .:!l l! 6116 6553 6996 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B091.CNF;1438 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W091.CNF;363 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 5.56E-02 1.16E-01 2.95E-02 6.38E-02 1.03E-01 2.82E-02 3.32E-02 8.63E-02 1.98E-02 7.20E-01 1.15E-01 3.42E-02 6.23E-02 7.47E-02 1.40E-02 1.96-sigma cnt Unc pCi/G 5.56E-02 6.37E-02 3.31E-02 4.87E-01 6.20E-02 AlphaSpectroscopySoftwareVerslon3.5.3 effectlvedate:02-Mar*2015 BATCH NUMBER : 1596400 SAMPLE ID : S0405235024 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 092 DETECTOR S/N : 80063 AVERAGE %EFFICIENCY : 30.3421 AVERAGE %EFF ERROR : 0.5858 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 67.1 +/-7.160 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.9431E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5430.46 PU-239 5155.00 5119.91 PU-242 4890.00 4873.62 PU-244 4589.00 4552.77 -PU 244*4497-4597 keV 17 PU.242:4SS4-4995keV t-PU-239: 5011-5227 keV PU-238:5375-5566keV 15 PU-236: 5582-5843 keV 13 11 (ii 9 I-z -::l 7 0 5 .;:. *:;; 3 -PEAK FWHM 0.000 4.922 118.128 74.814 59.064 -I 111 II I I I I I 24 06 2802 3203 3608 4017 443D Energy (keV) COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.06E-02 1.000 0.040 0.960 0.9798 99.900 7.35E-04 2.000 0.080 1.920 1.3856 99.900 1.46E-03 216.000 214.320 1.680 1.2961 100.000 3.91E+OO 2.000 1.520 0.480 0.6928 99.900 2.78E-02 II I I I I I I I I 4848 5>7 J698 6129 6565 7005 7449 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B092.CNF;1442 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W092.CNF;414 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.71E-02 1.23E-01 2.81E-02 5.45E-02 1.21E-01 3.30E-02 6.72E-02 1.47E-01 4.63E-02 7.75E-01 1.41E-01 4.33E-02 6.39E-02 1.01E-01 2.32E-02 1.96-sigma cnt Unc pCi/G 4.70E-02 5.45E-02 6.71E-02 5.27E-01 6.38E-02

'"ti Jil (\) -.J 00 0 0 ...., Ui 00 0 \0 BATCH NUMBER : 1596400 SAMPLE ID : S0405235025 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 093 DETECTOR S/N : 33206 AVERAGE %EFFICIENCY : 33.0892 AVERAGE %EFF ERROR : 0.6377 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 75.4 +/-6.518 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3032E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.27 PU-238 5486.00 5446.19 PU-239 5155.00 5118.70 PU-242 4890.00 4889.29 PU-244 4589.00 4558.92 PU-244: 4497-4597 keV 15 PU-242: 46544995 keV PU-239: 5011-5227 keV PlJ.238:537S.-5566keV 13 PU-236: 5582-5843 keV 11 en 9 I-z 7 ;::) 0 s 5 a "> 3 2407 2806 3210 Energy {keV) PEAK FWHM 0.000 0.000 0.000 80.246 0.000 COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -2.17E-02 3.000 1.320 1.680 1.2961 99.900 1.98E-02 0.000 -1.680 1.680 1.2961 99.900 -2.50E-02 264.000 262.320 1.680 1.2961 100.000 3.90E+OO 6.000 6.000 0.000 0.0000 99.900 8.93E-02 6145 6580 7019 7462 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B093.CNF;1431 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W093.CNF;379 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.11E-02 1.27E-01 3.62E-02 6.21E-02 1.16E-01 3.56E-02 3.53E-02 1.15E-01 3.54E-02 7.04E-01 1.15E-01 3.53E-02 7.84E-02 4.47E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.11 E-02 6.20E-02 3.53E-02 4.75E-01 7.75E-02 0 ...., Vl 00 0 \0 BATCH NUMBER : 1596400 SAMPLE ID : S0405235026 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 095 DETECTOR S/N : 38626 AVERAGE %EFFICIENCY : 30.4247 AVERAGE %EFF ERROR : 0.5873 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 83.6 +/-6.457 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6642E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 PU-244: 4497-4597 keV 17 PU-24Z:4654-4995keV PLJ.239:5011-5227 keV PU-238:5375-5566keV 15 PU-236: 5582-5843 keV 13 11 en 9 I-z ::l 7 0 5 *:;: 3 t5 <( 2380 2781 3186 Energy (keV) 5712.28 5527.73 5141.73 4870.78 4548.76 PEAK FWHM 0.000 4.993 89.878 77.811 44.939 COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.71E-02 1.000 0.040 0.960 0.9798 99.900 5.92E-04 2.000 1.520 0.480 0.6928 99.900 2.24E-02 269.000 267.560 1.440 1.2000 100.000 3.93E+OO 2.000 2.000 0.000 0.0000 99.900 2.94E-02 694 6125 6559 6997 7439 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B095.CNF;1407 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W095.CNF;408 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.98E-02 1.18E-01 3.20E-02 4.39E-02 9.76E-02 2.66E-02 5.15E-02 8.15E-02 1.87E-02 7.03E-01 1.09E-01 3.23E-02 5.06E-02 4.41E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.97E-02 4.39E-02 5.14E-02 4.74E-01 5.04E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235027 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 096 DETECTOR S/N : 80016 AVERAGE %EFFICIENCY : 32.5188 AVERAGE %EFF ERROR : 0.6269 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 78.8 +/-6.434 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4539E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5728.41 PU-238 5486.00 5419.38 PU-239 5155.00 5137.74 PU-242 4890.00 4870.70 PU-244 4589.00 4561.87 PU-244: 4497-4597 keV 21 PU-242:4654-4995keV PU-239; 5011-5227 keV 19 PU-238: 537S.5566 keV PU-236: 5582-5843 keV 17 15 00 13 I-11 z :J 9 0 7 .?;> 5 *s: u 3 <i: 1 2391 2788 3189 Energy (keV) PEAK FWHM 162.816 4.934 4.934 41.526 19.735 COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 4.000 2.560 1.440 1.2000 100.000 4.46E-02 1.000 -0.680 1.680 1.2961 99.900 -9.84E-03 1.000 0.280 0.720 0.8485 99.900 4.03E-03 271.000 269.560 1.440 1.2000 100.000 3.87E+OO 2.000 1.040 0.960 0.9798 99.900 1.50E-02 I t;;S; 6118 6554 6994 7438 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B096.CNF;1399 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W096.CNF;357 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.96E-02 1.29E-01 3.83E-02 4.45E-02 1.12E-01 3.43E-02 4.21E-02 8.78E-02 2.23E-02 6.90E-01 1.06E-01 3.16E-02 5.11E-02 9.47E-02 2.58E-02 1.96-sigma cnt Unc pCi/G 7.94E-02 4.45E-02 4.21E-02 4.65E-01 5.11E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235028 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 097 DETECTOR S/N : 83288 AVERAGE %EFFICIENCY : 35.3557 AVERAGE %EFF ERROR : 0.6805 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 82.0 +/-6.081 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.5921 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.14 PU-238 5486.00 5470.35 PU-239 5155.00 5142.96 PU-242 4890.00 4869.37 PU-244 4589.00 4542.65 23 PU-244: 4497-4597 keV PU-242:4654-4995keV 21 PU-239:5011*5227keV PU-238:5375-5566keV 19 PU-236; 5582-5843 keV 17 15 13 z 11 ::> 9 0 s 7 5 *:;; t5 3 <( 2402 Energy (keV) PEAK FWHM 236.442 0.000 68.962 54.431 4.926 COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 0.560 1.440 1.2000 100.000 8.77E-03 0.000 -0.480 0.480 0.6928 99.900 -6.18E-03 3.000 2.280 0.720 0.8485 99.900 2.92E-02 306.000 304.800 1.200 1.0954 100.000 3.89E+OO 4.000 4.000 0.000 0.0000 99.900 5.12E-02 n! 'i 'i 'i a $N 6118 6551 6989 7431 3 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B097.CNF;1396 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W097.CNF;381 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.67E-02 1.16E-01 3.44E-02 2.74E-02 7.13E-02 1.63E-02 5.17E-02 7.81E-02 1.99E-02 6.56E-01 8.96E-02 2.56E-02 5.67E-02 3.84E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.66E-02 2.73E-02 5.16E-02 4.39E-01 5.64E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235029 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 099 DETECTOR S/N : 80059 AVERAGE %EFFICIENCY : 35.6284 AVERAGE %EFF ERROR : 0.6858 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 78.0 +/-6.192 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4182E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5781.43 PU-238 5486.00 5483.83 PU-239 5155.00 5154.17 PU-242 4890.00 4871.59 PU-244 4589.00 4578.50 21 PU-244: 4497-4597 keV PU-242:4654-4995keV 19 PU-239:5011*5227keV PU-238:537S-5566keV 17 PU.236: 5582*5843 keV 15 13 en 11 t-z 9 => 0 7 8 5 *:;; :g 3 <( 2402 2795 3193 Energy (keV) PEAK FWHM 4.881 4.881 112.262 57.642 0.000 COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.040 0.960 0.9798 100.000 6.57E-04 4.000 3.520 0.480 0.6928 99.900 4.75E-02 2.000 1.520 0.480 0.6928 99.900 2.04E-02 293.000 292.280 0.720 0.8485 100.000 ' 3.92E+OO 2.000 1.280 0.720 0.8485 99.900 1.72E-02 l! ll 6104 6539 6978 7421 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B099.CNF;1399 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W099.CNF;383 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.88E-02 1.08E-01 2.95E-02 6.05E-02 7.48E-02 1.71E-02 4.69E-02 7.43E-02 1.70E-02 6.72E-01 8.19E-02 2.08E-02 4.73E-02 8.20E-02 2.09E-02 1.96-sigma cnt Unc pCi/G 4.87E-02 6.02E-02 4.68E-02 4.51E-01 4.73E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235030 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G -+/-0.195 % CHAMBER : 253 DETECTOR S/N : 87941 AVERAGE %EFFICIENCY : 25.6727 AVERAGE %EFF ERROR : 0.4975 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 80.8 +/-7.083 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.5427E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 PU*244: 4497-4597 keV 15 PU-242:4654-4995keV PU-239: 5011-5227 keV PU-238: 5375-5566 keV 13 PU-236: 5582-5843 keV 11 00 9 I-z :J 0 s .?;-*;:; <( 7 5 3 2368 2769 3173 Energy (keV) 5783.09 5451.69 5135.71 4855.64 4533.36 PEAK FWHM 4.985 104.681 89.727 58.156 54.833 COUNT DATE : 24-Sep-2016 20:51 :04 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 1.12E-02 2.000 1.280 0.720 0.8485 99.900 2.27E-02 2.000 1.040 0.960 0.9798 99.900 1.83E-02 219.000 218.280 0.720 0.8485 100.000 3.84E+OO 3.000 2.520 0.480 0.6928 99.900 4.44E-02 6106 6540 6977 7418 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B253.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W253.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.24E-02 1.19E-01 2.74E-02 6.26E-02 1.08E-01 2.76E-02 6.27E-02 1.16E-01 3.16E-02 7.54E-01 1.07E-01 2.74E-02 7.08E-02 9.76E-02 2.24E-02 1.96-sigma cnt Unc pCi/G 6.23E-02 6.25E-02 6.26E-02 5.12E-01 7.05E-02 Alpha Spectroscopy Software Version 3.5.3 effectivedate:OZ-Mat-2015 BATCH NUMBER : 1596400 SAMPLE ID : S0405235031_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.517 G +/-0.193 % CHAMBER : 254 DETECTOR S/N : 87942 AVERAGE %EFFICIENCY : 25.1642 AVERAGE %EFF ERROR : 0.4879 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 84.1 +/-7.016 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6845E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5772.49 PU-238 5486.00 5470.36 PU-239 5155.00 5118.70 PU-242 4890.00 4886.46 PU-244 4589.00 4549.83 r PU 244* 4497-4597 k V 19 "°""PU-242:4654-4995keV PU-239:5011-5227keV 17 PU-238:5375-5566keV r-PU-236: 5582-5843 keV 15 r 13 -en 11 -I-z 9 :::> -0 7 s *:; 3 :g I-<l'. -II I I I PEAK FWHM 29.851 0.000 0.000 55.224 9.950 I I I 'I I I I 23 85 2785 3188 3596 4007 COUNT DATE : 24-Sep-2016 20:51 :06 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.280 0.720 0.8485 100.000 2.69E-02 0.000 -0.480 0.480 0.6928 99.900 -8.30E-03 0.000 -0.480 0.480 0.6928 99.900 -8.25E-03 223.000 222.520 0.480 0.6928 100.000 3.82E+OO 2.000 1.760 0.240 0.4899 99.900 3.02E-02 Ill II I I I I I I I I 4841 5 6 1689 6119 6553 6991 7432 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B254.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W254.CNF;116 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.41E-02 1.28E-01 3.26E-02 3.68E-02 9.58E-02 2.19E-02 3.65E-02 9.51E-02 2.18E-02 7.42E-01 9.50E-02 2.18E-02 5.96E-02 8.24E-02 1.54E-02 1.96-sigma cnt Unc pCi/G 7.40E-02 3.67E-02 3.65E-02 5.04E-01 5.94E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235032 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 255 DETECTOR SIN : 87943 AVERAGE %EFFICIENCY : 24.9747 AVERAGE %EFF ERROR : 0.4844 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 79.2 +/-7.248 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4709E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.27 PU-238 5486.00 5468.93 PU-239 5155.00 5118.70 PU-242 4890.00 4874.01 PU-244 4589.00 4498.27 19 PU 244*4497-4597 keV PU-242: 4654-4995 keV 17 PU-239: 5011-5227 keV PU-238: 5375-5566 keV PU-236: 5582-5843 keV 15 13 Ui 11 -9 z -:l 0 7 -s 5 c -*:;; 3 ti -<t: f-I II 11 I I I PEAK FWHM 0.000 84.520 0.000 53.447 0.000 I I I I I I COUNT DATE : 24-Sep-2016 20:51 :08 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.10E-02 3.000 2.280 0.720 0.8485 99.900 4.29E-02 0.000 -1.680 1.680 1.2961 99.900 -3.14E-02 209.000 208.040 0.960 0.9798 100.000 3.89E+OO 1.000 0.040 0.960 0.9798 99.900 7.48E-04 1111 111 I' I I I I I 23 77 2776 3180 3588 3999 441 p 4834 5 51 )685 6116 6551 6990 7434 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B255.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W255.CNF;120 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.87E-02 1.27E-01 2.91E-02 7.62E-02 1.15E-01 2.93E-02 4.44E-02 1.45E-01 4.44E-02 7.80E-01 1.23E-01 3.35E-02 5.55E-02 1.23E-01 3.36E-02 1.96-sigma cnt Unc pCi/G 4.86E-02 7.59E-02 4.43E-02 5.31E-01 5.54E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235033 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 256 DETECTOR S/N : 87944 AVERAGE %EFFICIENCY : 25.7507 AVERAGE %EFF ERROR : 0.4991 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 70.2 +/-7.583 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.0757E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.27 PU-238 5486.00 5470.36 PU-239 5155.00 5167.96 PU-242 4890.00 4863.70 PU-244 4589.00 4506.88 15 PU 244 4497-4597 k V . PU-242: 4654-4995 keV PU-239:5011*5227keV 13 t-PU-238: 5375-5566 keV PU-236: 5582-5843 keV 11 >--UJ 9 >--I-7 z >--::i 0 5 >--3 *:;; >--u <( >--I I I II I I I PEAK FWHM 0.000 0.000 14.866 92.169 4.955 11 I I I II I COUNT DATE : 24-Sep-2016 20:51 :11 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.21E-02 0.000 -0.720 0.720 0.8485 99.900 -1.49E-02 2.000 1.040 0.960 0.9798 99.900 2.14E-02 192.000 190.080 1.920 1.3856 100.000 3.90E+OO 1.000 0.520 0.480 0.6928 99.900 1.07E-02 i Ifni II I I I I I 23 72 2771 3173 3579 3989 440B 4820 5 4. 667 6097 6530 6967 7407 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B256.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W256.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.39E-01 3.19E-02 4.51E-02 1.26E-01 3.22E-02 7.31E-02 1.35E-01 3.69E-02 8.20E-01 1.66E-01 5.21E-02 5.95E-02 1.14E-01 2.61E-02 1.96-sigma cnt Unc pCi/G 5.34E-02 4.50E-02 7.30E-02 5.60E-01 5.94E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235034 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 233 DETECTOR S/N : 87921 AVERAGE %EFFICIENCY : 25.2931 AVERAGE %EFF ERROR : 0.4905 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 96.6 +/-6.572 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.2344E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5512.84 PU-239 5155.00 5118.71 PU-242 4890.00 4869.83 PU-244 4589.00 4532.12 PU z44* 4497-4597 keV 19 ._ PU-242: 46544995 keV PU-239: 5011-5227 keV 17 PU-238: 5375-5566 keV I-PU-236: 5582-5843 keV 15 13 (j) 11 I-z 9 :l 0 7 8 5 *s: 3 :g f-<( I I I I I PEAK FWHM 0.000 4.971 0.000 71.772 0.000 II 11 11 I I I 23 96 2795 3198 3605 4016 4433 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:08 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.760 0.240 0.4899 99.900 1.16E-02 0.000 -0.480 0.480 0.6928 99.900 -7.25E-03 258.000 257.040 0.960 0.9798 100.000 3.88E+OO 3.000 3.000 0.000 0.0000 99.900 4.53E-02 l l >> l :R:: i Iii I I I I I I 4848 5 694 6123 6555 6991 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B233.CNF;454 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W233.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.74E-02 5.55E-02 0.00E+OO 4.34E-02 7.29E-02 1.36E-02 3.21E-02 8.37E-02 1.92E-02 7.06E-01 9.94E-02 2.71E-02 5.99E-02 4.53E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.73E-02 4.33E-02 3.21E-02 4.76E-01 5.96E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235035 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.516 G -+/-0.194 % . CHAMBER : 234 DETECTOR S/N : 87922 AVERAGE %EFFICIENCY : 24.8037 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 74.6 +/-7.460 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.2717E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.30 PU-238 5486.00 5465.26 PU-239 5155.00 5226.77 PU-242 4890.00 4870.16 PU-244 4589.00 4562.94 PU-244: 4497-4597 keV 15 PU-242: 4654-4995 keV PU-239:5011-5227keV PU-238: 5375-5566 keV 13 PU-236:5582-5843keV 11 0' 9 z 7 => 0 8 5 c *:;: 3 t5 <I: 2388 Energy (keV) PEAK FWHM 0.000 4.996 0.000 59.123 4.996 COUNT DATE : 24-Sep-2016 20:54:11 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.16E-02 1.000 -0.440 1.440 1.2000 99.900 -8.71E-03 1.000 -0.920 1.920 1.3856 99.900 -1.81E-02 195.000 194.760 0.240 0.4899 100.000 3.83E+OO 3.000 3.000 0.000 0.0000 99.900 5.90E-02 >> > r: !l 6123 6554 6990 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B234.CNF;454 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W234.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.13E-02 1.33E-01 3.06E-02 6.02E-02 1.46E-01 4.35E-02 6.12E-02 1.59E-01 4.99E-02 7.91E-01 9.42E-02 1.76E-02 7.82E-02 5.90E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.11E-02 6.02E-02 6.12E-02 5.39E-01 7.76E-02 0 ...., Ul 00 0 ID BATCH NUMBER : 1596400 SAMPLE ID : S0405235036 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 235 DETECTOR S/N : 87923 AVERAGE %EFFICIENCY : 24.7991 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 84.6 +/-7.054 % 1770-A TRACER . ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.7098E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5805.53 PU-238 5486.00 5433.55 PU-239 5155.00 5146.52 PU-242 4890.00 4871.68 PU-244 4589.00 4546.97 PU 244'4497-4597 keV . 15 PlJ.242: 46544995 keV -PU-239; 5011*5227 keV PlJ.238:537S-5566keV 13 PU-236: 5582-5843 keV 11 0' 9 z 7 ::> 0 s 5 c *:;; 3 t5 -PEAK FWHM 29.867 14.933 64.712 70.163 0.000 <!'. 1 I I 11 Ill 1111 I I I I I I 23 92 2792 3196 3604 4016 443, Energy (keV) COUNT DATE : 24-Sep-2016 20:54:13 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 0.800 1.200 1.0954 . 100.000 1.69E-02 2.000 1.280 0.720 0.8485 99.900 2.23E-02 2.000 1.040 0.960 0.9798 99.900 1.80E-02 222.000 220.800 1.200 1.0954 100.000 3.81E+OO 0.000 -0.240 0.240 0.4899 99.900 -4.15E-03 >> !!!! a *i 11111111 11 I I I 4851 5 7 D701 6132 6566 7005 7447 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B235.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W235.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.59E-02 1.48E-01 4.25E-02 6.14E-02 1.06E-01 2.70E-02 6.15E-02 1.14E-01 3.10E-02 7.45E-01 1.21E-01 3.46E-02 3.59E-02 8.29E-02 1.55E-02 1.96-sigma cnt Unc pCi/G 7.59E-02 6.13E-02 6.14E-02 5.06E-01 3.58E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235037 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 255 DETECTOR S/N : 87943 AVERAGE %EFFICIENCY : 24.9747 AVERAGE %EFF ERROR : 0.4844 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 67.4 +/-7.820 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.9537E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 14 PU 244' 4497-4597 keV -PU*242:4654-4995keV 13 12 11 10 9 8 7 6 5 4 3 2 1 r-PU-239: 5011-5227 keV PlJ..238; 5375-5566 keV f-PU-236: 5582-5843 keV f---f-------f--f--f--I I PEAK ENERGY 5695.60 5470.35 5118.70 4866.83 4546.97 II I I PEAK FWHM 4.972 0.000 0.000 49.244 0.000 I I I 23 77 2776 3180 3588 3999 441 5 Energy (keV) COUNT DATE : 26-Sep-2016 13:55:05 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.520 0.480 0.6928 100.000 1.40E-02 0.000 -0.720 0.720 0.8485 99.900 -1.60E-02 0.000 -1.680 1.680 1.2961 99.900 -3.71E-02 178.000 177.040 0.960 0.9798 100.000 3.90E+OO 0.000 -0.960 0.960 0.9798 99.900 -2.12E-02 1111j I I I I I 4834 5 5! )685 6116 6551 6990 7434 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B255.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W255.CNF;120 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.79E-02 1.49E-01 3.42E-02 4.84E-02 1.36E-01 3.45E-02 5.24E-02 1.71E-01 5.24E-02 8.45E-01 1.45E-01 3.96E-02 4.92E-02 1.45E-01 3.96E-02 1.96-sigma en! Une pCi/G 7.78E-02 4.83E-02 5.23E-02 5.78E-01 4.91E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235038 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 238 DETECTOR S/N : 87926 AVERAGE %EFFICIENCY : 26.1325 AVERAGE %EFF ERROR : 0.5062 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 76.4 +/-7.215 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3490E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5490.86 PU-239 5155.00 5118.69 PU-242 4890.00 4867.80 PU-244 4589.00 4525.12 17 PU-244: 4497-4597 keV PU-242: 4654-4995 keV PU-239:5011-5227keV 15 PU-238;5375-5566keV PU-236: 5582-5843 keV 13 11 en 9 I-z :J 7 0 5 3 u <( 2386 2784 3187 Energy (keV) PEAK FWHM 0.000 39.647 0.000 59.058 4.956 COUNT DATE : 24-Sep-2016 20:54:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.240 0.240 0.4899 100.000 -5.50E-03 2.000 1.520 0.480 0.6928 99.900 2.87E-02 0.000 -0.480 0.480 0.6928 99.900 -9.02E-03 211.000 210.040 0.960 0.9798 100.000 3.94E+OO 1.000 1.000 0.000 0.0000 99.900 1.88E-02 l l >> JU! a $N 6124 6561 7001 7446 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B238.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W238.CNF;125 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.75E-02 1.10E-01 2.05E-02 6.61E-02 1.05E-01 2.40E-02 4.00E-02 1.04E-01 2.38E-02 7.88E-01 1.24E-01 3.37E-02 5.29E-02 5.63E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.74E-02 6.60E-02 3.99E-02 5.36E-01 5.28E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235039 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 256 DETECTOR S/N : 87944 AVERAGE %EFFICIENCY : 25.7507 AVERAGE %EFF ERROR : 0.4991 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 85.3 +/-6.918 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.7391 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5646.01 PU-238 5486.00 5470.36 PU-239 5155.00 5109.87 PU-242 4890.00 4854.54 PU-244 4589.00 4572.03 15 PU-244*44974597 keV -PU-242: 46544995 keV PU-239; 5011-5227 keV 13 i-PU-238:5375-5566keV PU-236: 5582-5843 keV 11 I-if) 9 I-7 z -:J 0 5 -3 *;; -u <t: -I I I I I I PEAK FWHM 4.955 0.000 4.955 83.332 19.821 I I II I I 23 72 2771 3173 3579 3989 440 Energy (keV) COUNT DATE : 26-Sep-2016 13:55:07 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.520 0.480 0.6928 100.000 1.06E-02 0.000 -0.720 0.720 0.8485 99.900 -1.21E-02 1.000 0.040 0.960 0.9798 99.900 6.68E-04 233.000 231.080 1.920 1.3856 100.000 3.86E+OO 2.000 1.520 0.480 0.6928 99.900 2.54E-02 Ii: I I I I I I I 4820 5 4:; 667 6097 6530 6967 7407 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B256.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W256.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.90E-02 1.13E-01 2.59E-02 3.66E-02 1.03E-01 2.61E-02 4.96E-02 1.10E-01 3.00E-02 7.39E-01 1.35E-01 4.24E-02 5.84E-02 9.25E-02 2.12E-02 1.96-sigma cnt Unc pCi/G 5.89E-02 3.66E-02 4.95E-02 5.01E-01 5.83E-02 BATCH NUMBER : 1596400 SAMPLE ID : S0405235040 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 241 DETECTOR S/N : 87963 AVERAGE %EFFICIENCY : 25.9137 AVERAGE %EFF ERROR : 0.5022 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 66.9 +/-7.707 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.9309E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5539.52 PU-239 5155.00 5101.30 PU-242 4890.00 4891.22 PU-244 4589.00 4546.97 14 PU-244: 4497.-4597 keV PU-242: 46544995 keV 13 PU-239: 5011-5227 keV 12 PU-238:5375-5566keV PU-236: 5582-5843 keV 11 10 9 0' 8 7 z 6 ::::> 0 5 s 4 3 *:;; u 2 < 1 2406 2805 3208 Energy (keV) PEAK FWHM 0.000 4.964 94.325 79.018 0.000 COUNT DATE : 24-Sep-2016 20:54:22 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 -0.200 1.200 1.0954 99.900 -4.24E-03 3.000 2.760 0.240 0.4899 99.900 5.81E-02 183.000 182.280 0.720 0.8485 100.000 3.83E+OO 0.000 -0.240 0.240 0.4899 99.900 -5.05E-03 ll > 6134 6567 7004 7445 ; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B241.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W241.CNF;131 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.19E-02 7.70E-02 O.OOE+OO 6.37E-02 1.49E-01 4.25E-02 8.42E-02 1.01E-01 1.89E-02 8.18E-01 1.28E-01 3.27E-02 4.37E-02 1.01E-01 1.89E-02 1.96-sigma en! Une pCi/G 5.17E-02 6.36E-02 8.37E-02 5.60E-01 4.36E-02 BATCH NUMBER : 1596400 SAMPLE ID : S1203621718 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 243 DETECTOR S/N : 87931 AVERAGE %EFFICIENCY : 24.8977 AVERAGE %EFF ERROR : 0.4829 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 83.2 +/-7.117 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6456E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.29 PU-238 5486.00 5526.42 PU-239 5155.00 5167.95 PU-242 4890.00 4887.31 PU-244 4589.00 4548.84 PU.244*4497-4597 keV 17 _ PlJ..242: 46544995 keV PU-239: 5011-5227 keV PU-238:5375-5566keV 15 -PU-236: 5582-5843 keV 13 (j) 9 I--z ::i 0 7 -8 5 -*::; 3 -I I I I PEAK FWHM 0.000 0.000 84.671 73.049 64.748 I I I II I 23 89 2789 3193 3600 4011 44213 COUNT DATE : 24-Sep-2016 20:54:24 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.68E-02 3.000 -2.760 5.760 2.4000 99.900 -4.83E-02 3.000 2.520 0.480 0.6928 99.900 4.41E-02 220.000 217.840 2.160 1.4697 100.000 3.81E+OO 3.000 2.760 0.240 0.4899 99.900 4.83E-02 >> i II II II I I I I I I 4843 5 61 J690 6118 6550 6986 7424 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B243.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W243.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 3.91E-02 1.16E-01 3.15E-02 8.01E-02 2.07E-01 7.70E-02 7.04E-02 9.?0E-02 2.22E-02 7.51E-01 1.47E-01 4.71E-02 7.00E-02 8.40E-02 1.57E-02 1.96-sigma cnt Unc pCi/G 3.90E-02 8.01E-02 7.01E-02 5.10E-01 6.96E-02 BATCH NUMBER : 1596400 SAMPLE ID : S1203621719 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 244 DETECTOR S/N : 87932 AVERAGE %EFFICIENCY : 23.7184 AVERAGE %EFF ERROR : 0.4607 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 93.5 +/-6.885 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.0988E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5759.03 PU-238 5486.00 5497.91 PU-239 5155.00 5088.35 PU-242 4890.00 4886.10 PU-244 4589.00 4528.60 PU 244' 4497-4597 keV 19 1-PU*242:4654-4995keV PU-2J9:5011-5227keV 17 PU-238;537S-5566keV l-PU-236;SS82-SB43keV 15 13 Ci) 11 f-I-z 9 :::i 0 7 8 f-5 u 3 f-I I I I I PEAK FWHM 4.999 4.999 74.978 64.386 4.999 I I II 23 78 2779 3184 3592 4004 COUNT DATE : 24-Sep-2016 20:54:26 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.200 1.200 1.0954 100.000 -4.04E-03 1.000 0.280 0.720 0.8485 99.900 4.70E-03 3.000 1.560 1.440 1.2000 99.900 2.60E-02 235.000 233.320 1.680 1.2961 100.000 3.89E+OO 1.000 1.000 0.000 0.0000 99.900 1.67E-02 a Ill I I I I I I 4837 5: p684 6113 6545 6980 7418 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B244.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W244.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.08E-02 1.42E-01 4.06E-02 4.92E-02 1.03E-01 2.61E-02 6.87E-02 1.23E-01 3.67E-02 7.41E-01 1.29E-01 3.95E-02 4.69E-02 5.00E-02 0.00E+OO 1.96-sigma cnt Unc pCi/G 6.07E-02 4.91E-02 6.86E-02 5.02E-01 4.69E-02 BATCH NUMBER : 1596400 SAMPLE ID : S1203621720 PU SAMPLE QTY : 0.518 G -+/-0.193 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 226 DETECTOR SIN : 87914 AVERAGE %EFFICIENCY : 26.8347 AVERAGE %EFF ERROR : 0.5195 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 89.2 +/-6.637 % COUNT DATE : 24-Sep-2016 20:54:04 ELAPSED LIVE TIME(SEC) : 14400.00 TRACER LCS ID 1770-A ID 0338-MM NUCLIDE PU-242 NUCLIDE PU-239 NOMINAL 4.3831E+OO dpm NOMINAL (pCi/G) 3.8148E+OO RESULTS 3.9097E+OO dpm % RECOVERY 95.550 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY ENERGY FWHM AREA AREA AREA S!Dev pCi/G PU-236 5749.00 5712.28 0.000 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO PU-238 5486.00 5470.36 0.000 0.000 -0.720 0.720 0.8485 99.900 -1.09E-02 PU-239 5155.00 5132.53 63.008 242.000 240.560 1.440 1.2000 99.900 3.65E+OO PU-242 4890.00 4873.48 55.319 253.000 251.800 1.200 1.0954 100.000 3.81E+OO PU-244 4589.00 4577.39 9.967 2.000 1.760 0.240 0.4899 99.900 2.67E-02 PU 244*4497-4597 keV 23 I-PU-242: 4654-4995 keV PU-239:5011*5227keV 21 1-PU-238:5375-5566keV PlJ.236: 5582*5643 keV 19 r-17 r-15 r-I Ui 13 -z 11 -:::i 9 0 5 *:;: -ti 3 <l'. -111 Ill -1 11 1 I I I 11111111 I 1 I Ill I I I I I ,, I I I I I 23 72 2772 3177 3585 3997 4832 5 5! 682 6113 6548 6986 7428 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B226.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W226.CNF;122 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.07E-02 4.55E-02 O.OOE+OO 3.30E-02 9.26E-02 2.36E-02 6.77E-01 1.12E-01 3.33E-02 7.01E-01 1.06E-01 3.04E-02 5.25E-02 7.27E-02 1.36E-02 1.96-sigma en! Une pCi/G 3.06E-02 3.29E-02 4.63E-01 4.73E-01 5.24E-02 Effective 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Product:. __ Date: C\ \ (J)\ I l,,. Criteria: Yes No Comments Sample Solids are less than or equal to 100 mq for GAB. Samples have been blank corrected (If required). [\)3'-Blank correction renorted Included (If reouiredl. If activity less than 10x MDA/MDC, error Is less than or equal to 150%.ofsample activity. If greater than 10* MDA/ MDC, error Is 400/o or less. If hAln*u *ha Uni\ I Mnr a*rnr le Instrument source check Is within limits. .,/ *--nt hkn rnerk Is within llmltc. Method RDL/ LLD has been met. ./ If dupllcate activities are: Less than 5* MDA/ MDC, then .RPD Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, I' If below the MDA/ MDC, the RPD Is 0%, Or meets the client's reoulred RER acceotance criteria. Tracer yield Is -15*125%

Carrier yleld 25-125%. / C Or meets the cllent's contract acceptance criteria). Method blank Is less than the RDL/ LLD. v Uf c:1mnlae < §0/n of lnmae* actlvltv\ Sample was run within hold time. v \ Samole was correctlv oreserved If reouired. smears Taken for Radioactive batches. l\.J(&-Method Spike and LCS are within 75-125% ./ 'or meets the dlent's rnntr:1.+ accen.,,nce rrt*nrla\. No blank spaces on data forms. i\11 llne outs Initialed and dated. ./ Nn ------..... Aux data Is correct. Client Soeclal reouirements naoe has been checked. _/ ' Raw Data and I or snectrum are Included and nronerlv statused. ,,r MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / u:11**-" uertnn.t .... (If nn*n*a.I ln*n r .. .,ft ./' Batch Data Exceotlon Reoorts fDER\ comnleted, If annllcable. v lJtJli Batch Data Exception Reports (DER) second reviewed. .,/"'" D.:;t-1\.-Dlsnosltlon verified to be comnleted. Altnun* CnrPe**lnn <"nmnln*n.1 If reDUi'""..t Review sample historical results If available (If REMP, results above MDC have been verified / bv historical results recount or re-analvsls. l Primary Review Performed By: __ __ 1-'h'---o_J....l./_,_1,. _____ _ -...:.... Secondary Review Performed By:_-_ O 10/02/16 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DER Report No.: 1563222 Revision No.: 1 DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: Type: 30-SEP-16 Radiochemistry Specifications Process Instrument Type: Test I Method: Matrix Type: Client Code: ALPHA SPECTROMETER DOE EML HASL-300, Pu-11-RC Solid MJWC .. *-Batch ID: Sample Numbers: 1596393 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Other Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203621701 were received and analyzed out of holding. 2 .. Sample 1203621701 does not meet the resolution requirement of 2. The sample does meet the tracer yield requirement, the detection limits, having a full width half maximum of 100 keV or less for the Pu-242 and its tracer peak is within the Pu-242 region of interest. Reporting tracer. results. Originator's Name: Data Validator/Group Leader: Melanie Aycock 30-SEP-16 Jessica Davis 02-0CT-16 Page 1 Page 800 of 5809 0 '""+) Vo 00 0 \0 f J Plutonium Queue Sheet 07-SEP-16 ---------Batch #: 1596393 Analyst: JXH2 Tracer Code: \ First Client Due Date:04-0CT-16 Expiration Date: 8 l'1 Expiration Date: "7-Zo**li LCS Code: 0'133-Mf'\ Internal Due Date:30-SEP-16 Vol: 0' \"" L Analyzed Sequentially with: Vol:01\...,L U: 38'\ Spike Code: .-Expiration Date: Vol:-==-Am: \ ?C, (,, 3'10 Pipet ID: \gL\.OCZ-2:_ BalanceID: \(o\07!'.:.(..,-Z.. Sample ID Client Description -------* 405235001-1 4.1.B.R;l.2 405235002-1 4.1.B.R.1.3 405235003-1 4.1.B.R.1.4 405235004-1 4.1.B.R.7.2 405235005-1 4.1.C.R.1.3 405235006-1 4.1.C.R.1.4 405235007-1 4.1.C.R.2.3 405235008-1 4.1.C.R.2.4 405235009-1 4.1.D.R.1.3 405235010-1 4.1.D.R.l.4 405235011-1 4.1.D.R.3.2 405235012-1 4.1.D.R.2.4 405235013-1 4.2A.R.2.3 405235014-1 4.2A.R.1.3 405235015-1 4.2A.R.1.4 405235016-1 4.2A.R.2.4 405235017-1 4.2A.R.3.2 405235018-1 4.2A.R.4.2 405235019-1 4.2B.R.2.4 405235020-1 4.2B.R.l.4 1203621700-1 MB for batch 1596393 1203621701-1 4.1.B.R.l.2(405235001DUP) 1203621702-1 LCS for batch 1596393 Type SAMPLE SAMPLE SAMPLE S.L'\1PLE SAMPLE SAMPLE SA.l'vlPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAJ\.fPLE SAMPLE MB DUP LCS Hazard Code Min CRDL 1 pCifg 1 pCifg 1 pCifg 1 pCi/g 1 pCifg 1 pCi/g 1 pCifg 1 pCifg 1 pCi/g 1 pCifg 1 pCifg 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCilg 1 pCi/g 1 pCifg 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Choose SOP Used: Solid Sample Dissolution by: LEACH GL-RAD-A-053 Circle One GEL Laboratories LLC, , Radiochemistry Division Client MJWCOOl l'vUWCOOl MJWCOOl MJWCOOl MJWCOOl l\'UWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl l\UWCOOl l\UWCOOl MJWCOOl MJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Collection Date 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 02-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 10-DEC-15 Witness: \'.'..-6 q '2-lt*iU Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Label # WetlJ Aliquot @uo Pu Det# Z. /c.5i'.i5 /O<{ j 3 10,?c\ I (o ! o_. _s_c_\ 1 l I l(),5o\ ID'i l i 8 !o,5{j3 lf'D i C\ i \ci i D. 50\ ZIO j \1... !o.5o(.o Zld i jo.Sco ZtL qf lf }t, 1 \\,, io, so1 7zo I J 2.c io.5az. Z7¥ i '"l-\ !o. Scf*=,. 1-1 "2.-'l.--Jb, Soo I ZZB rz.3 /o.Sif\ ! !rn Data Reviewed 1.4., Page: 1 of 1

"" (1) 00 0 N 0 ....., Vl 00 0 '° BATCH NUMBER : 1596393 SAMPLE ID : S0405235001_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G +/-0.200 % CHAMBER : 103 DETECTOR S/N : 79461 AVERAGE %EFFICIENCY : 33.8848 AVERAGE %EFF ERROR : 0.6527 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 78.4 +/-6.316 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.4371 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5450.04 PU-239 5155.00 5033.19 PU-242 4890.00 4865.40 PU-244 4589.00 4590.17 PU-244: 4497-4597 keV 19 PU-242: 46544995 keV PU-239: 5011-5227 keV 17 PU.238: 5375-5566 keV PU-236: 5582-5843 keV 15 13 (ii 11 I-z 9 => 0 7 5 u 3 <l: 2380 Energy {keV) PEAK FWHM 0.000 64.506 4.962 77.502 4.962 COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.65E-02 4.000 2.560 1.440 1.2000 99.900 3.64E-02 1.000 -0.440 1.440 1.2000 99.900 -6.21E-03 280.000 279.520 0.480 0.6928 100.000 3.94E+OO 1.000 1.000 0.000 0.0000 99.900 1.41E-02 !;;!;; i 6123 6560 7001 7446 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B103.CNF;1414 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W103.CNF;395 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.82E-02 1.13E-01 3.08E-02 6.49E-02 1.05E-01 3.12E-02 4.29E-02 1.04E-01 3.10E-02 6.89E-01 7.81E-02 1.79E-02 3.97E-02 4.23E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.81E-02 6.47E-02 4.29E-02 4.63E-01 3.97E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235002 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 104 DETECTOR S/N : 80011 AVERAGE %EFFICIENCY : 32.4069 AVERAGE %EFF ERROR : 0.6248 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 76.4 +/-6.541 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE 1770-A PU-242 4.3831E+OO dpm 3.3470E+OO dpm LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5763.53 PU-238 5486.00 5430.31 PU-239 5155.00 5158.31 PU-242 4890.00 4865.77 PU-244 4589.00 4546.97 23 PU 244* 4497-4597 k V PU-242: 46544995 keV 21 _ PU-239: 5011-5227 keV PlJ.238:5375-5566keV 19 PlJ..236: 5582-5843 keV 17 15 13 z 11 --:J 9 0 -f2, 7 -5 *:;; -u 3 -<( 1 I I I I PEAK FWHM 4.919 14.757 4.919 43.943 0.000 I I I I I 23 80 2776 3176 3581 3991 4403 COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA. AREA AREA S!Dev pCi/G 1.000 0.280 0.720 0.8485 100.000 5.11E-03 2.000 1.280 0.720 0.8485 99.900 1.94E-02 1.000. -0.440 1.440 1.2000 99.900 -6.61E-03 262.000 260.320 1.680 1.2961 100.000 3.91E+OO 0.000 -0.720 0.720 0.8485 99.900 -1.08E-02 >> l !!!l a I ,J,I I I I I I I I I I I 4825 5 677 6110 6548 6991 7438 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B104.CNF;1399 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W104.CNF;386 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.35E-02 1.12E-01 2.84E-02 5.34E-02 9.24E-02 2.35E-02 4.57E-02 1.11E-01 3.30E-02 7.08E-01 1.16E-01 3.57E-02 3.27E-02 9.18E-02 2.34E-02 1.96-sigma en! Unc pCi/G 5.35E-02 5.33E-02 4.57E-02 4.78E-01 3.27E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235003 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 105 DETECTOR S/N : 78777 AVERAGE %EFFICIENCY : 33.6886 AVERAGE %EFF ERROR : 0.6490 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 59.5 +/-7.223 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.6077E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5767.11 PU-238 5486.00 5417.13 PU-239 5155.00 5213.95 PU-242 4890.00 4861.02 PU-244 4589.00 4568.67 -PU 244* 4497-4597 keV PU.242: 46544995 keV 25 f-PU-239:5011-5227keV PU-2J8:537&-5566keV 22 I-PU-236: 5582-5843 keV 19 f--en 16 I-13 z -:J 0 10 -s 7 -*s: 4 t5 -<( 11 11 I I I PEAK FWHM 4.933 4.933 4.933 18.714 4.933 I I 23 75 2772 3174 3580 3991 4403 COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.680 1.680 1.2961 100.000 -1.55E-02 1.000 0.040 0.960 0.9798 99.900 7.53E-04 1.000 0.040 0.960 0.9798 99.900 7.48E-04 213.000 210.840 2.160 1.4697 100.000 3.94E+OO 1.000 0.040 0.960 0.9798 99.900 7.48E-04 mm 1 IJ I I I' I I I I I 4827 5: 51 681 6115 6553 6997 7444 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B105.CNF;1398 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W105.CNF;364 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.00E-02 1.76E-01 5.40E-02 5.59E-02 1.24E-01 3.38E-02 5.55E-02 1.23E-01 3.36E-02 7.88E-01 1.57E-01 5.03E-02 5.55E-02 1.23E-01 3.36E-02 1.96-sigma cnt Unc pCi/G 6.99E-02 5.58E-02 5.55E-02 5.37E-01 5.55E-02 BATCHNUMBER : 1596393 SAMPLE ID : S0405235004 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 106 DETECTOR S/N : 80012 AVERAGE %EFFICIENCY : 32.6615 AVERAGE %EFF ERROR : 0.6296 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 56.3 +/-7.505 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.4693E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5705.53 PU-238 5486.00 5459.31 PU-239 5155.00 5140.44 PU-242 4890.00 4854.84 PU-244 4589.00 4570.39 -PU-244* 44974597 keV 17 PU*242: 46544995 keV -PlJ.239: 5011-5227 keV PU-238: 5375-5566 keV 15 -PU*236: 5582-5843 keV 13 0' 9 r z ::> 7 0 r £ 5 .c r *s; 3 u -<t: Ir I I I I I PEAK FWHM 4.904 24.521 4.904 23.663 29.425 I 11 I COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.760 0.240 0.4899 100.000 1.88E-02 2.000 -1.120 3.120 1.7664 99.900 -2.29E-02 1.000 0.520 0.480 0.6928 99.900 1.06E-02 195.000 193.560 1.440 1.2000 100.000 3.93E+OO 2.000 1.760 0.240 0.4899 99.900 3.58E-02 > }} I rll! I II I I I I I I 23 87 2782 3181 3585 3993 440 3 4824 5.4* 673 6105 6541 6982 7427 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B106.CNF;1398 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W106.CNF;363 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.06E-02 1.19E-01 2.22E-02 7.83E-02 1.94E-01 6.62E-02 5.88E-02 1.13E-01 2.58E-02 8.18E-01 1.50E-01 4.47E-02 7.06E-02 9.75E-02 1.83E-02 1.96-sigma cnt Unc pCi/G 7.05E-02 7.83E-02 5.88E-02 5.58E-01 7.04E-02 3.5.3 BATCH NUMBER : 1596393 SAMPLE ID : 80405235005 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 107 DETECTOR S/N : 67578 AVERAGE %EFFICIENCY : 30.7195 AVERAGE %EFF ERROR : 0.5929 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 93.2 +/-6.114 % TRACER 1770-A ,ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.0832E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5767.98 PU-238 5486.00 5439.25 PU-239 5155.00 5116.13 PU-242 4890.00 4868.26 PU-244 4589.00 4515.46 PU-244: 4497-4597 keV 19 PU-242: 4654-4995 keV PU-239:5011-5227keV 17 PU-238:537S.5566keV PU-236: 5582-5843 keV 15 13 (ii 11 I-z 9 ::::i 0 7 2-5 *:.;: 3 t5 <!'. 1 PEAK FWHM 4.917 157.348 4.917 64.578 0.000 2399 2794 3194 3597 4005 Energy (keV) COUNT DATE : 29-Sep-2016 09:18:30 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.200 1.200 1.0954 100.000 -3.17E-03 5.000 3.560 1.440 1.2000 99.900 4.68E-02 1.000 0.520 0.480 0.6928 99.900 6.79E-03 302.000 301.040 0.960 0.9798 100.000 3.93E+OO 3.000 2.760 0.240 0.4899 99.900 3.60E-02 >> !!..:! a mm 6106 6538 6975 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B107.CNF;1439 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W107.CNF;426 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.76E-02 1.11E-01 3.18E-02 6.54E-02 9.72E-02 2.89E-02 3.77E-02 7.23E-02 1.66E-02 6.65E-01 8.59E-02 2.34E-02 5.21E-02 6.26E-02 1.17E-02 1.96-sigma cnt Unc pCi/G 4.76E-02 6.51E-02 3.77E-02 4.45E-01 5.19E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235006 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 108 DETECTOR S/N : 78778 AVERAGE %EFFICIENCY : 34.5578 AVERAGE %EFF ERROR : 0.6655 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 97.3 +/-5.689 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.2658E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5432.77 PU-239 5155.00 5049.43 PU-242 4890.00 4860.01 PU-244 4589.00 4571.63 23 PU-244: 4497-4597 keV PU-242: 4654-4995 keV 21 PlJ..239: 5011-5227 keV PU.238: 537$.5566 keV 19 PlJ.235:5582-5843keV 17 15 'iii 13 f-11 z ::J 9 0 7 5 t5 3 <t: 1 2397 2792 3191 Energy (keV) PEAK FWHM 0.000 63.844 4.911 70.528 9.822 COUNT DATE : 29-Sep-2016 09:18:30 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -6.50E-03 3.000 2.520 0.480 0.6928 99.900 2.83E-02 1.000 0.760 0.240 0.4899 99.900 8.47E-03 355.000 353.800 1.200 1.0954 100.000 3.94E+OO 2.000 2.000 0.000 0.0000 99.900 2.23E-02 *g 6102 6535 6971 7412 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B108.CNF;1433 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W108.CNF;430 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.88E-02 7.50E-02 1.72E-02 4.51E-02 6.21E-02 1.42E-02 3.18E-02 5.35E-02 1.00E-02 6.21E-01 7.81E-02 2.24E-02 3.83E-02 3.34E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.87E-02 4.49E-02 3.18E-02 4.12E-01 3.82E-02 '"d 00 0 00 0 ....., lll 00 0 \0 BATCH NUMBER : 1596393 SAMPLE ID : S0405235007 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 109 DETECTOR S/N : 79463 AVERAGE %EFFICIENCY : 36.1703 AVERAGE %EFF ERROR : 0.6959 SAMPLE DATE : 1 O-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 82.9 +/-5.993 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.6324E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5690.95 PU-238 5486.00 5492.60 PU-239 5155.00 5204.92 PU-242 4890.00 4857.44 PU-244 4589.00 4552.40 PU-244: 4497-4597 keV 21 PU-242: 46544995 keV PU-239:5011-5227keV 19 PU-238:5375-5566keV PU-236: 5582-5843 keV 17 15 Ci) 13 I-11 z ::J 9 0 7 p 5 *;;; ti 3 <( 1 2401 2796 3196 3600 Energy (keV) PEAK FWHM 4.905 4.905 4.905 80.162 4.905 COUNT DATE : 29-Sep-2016 09:18:30 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 7.90E-03 1.000 0.040 0.960 0.9798 99.900 5.04E-04 1.000 0.040 0.960 0.9798 99.900 5.00E-04 317.000 315.320 1.680 1.2961 100.000 3.94E+OO 1.000 0.520 0.480 0.6928 99.900 6.51E-03 :;:;; 6123 6560 7002 7448 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B109.CNF;1431 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W109.CNF;420 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.39E-02 8.42E-02 1.93E-02 3.74E-02 8.30E-02 2.26E-02 3.71E-02 8.24E-02 2.25E-02 6.54E-01 9.68E-02 2.97E-02 3.62E-02 6.93E-02 1.59E-02 1.96-sigma cnt Unc pCi/G 4.39E-02 3.73E-02 3.71E-02 4.37E-01 3.61E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235008 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 110 DETECTOR S/N : 83292 AVERAGE %EFFICIENCY : 32.3669 AVERAGE %EFF ERROR : 0.6241 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.1 +/-6.064 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.9495E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5461.18 PU-239 5155.00 5218.37 PU-242 4890.00 4858.84 PU-244 4589.00 4546.97 21 PU-244: 4497-4597 keV PU*242:4654-4995keV 19 PU-2J9:5011*5227keV PU-238:5375-5566keV 17 PU-236: 5582-5843 keV 15 13 Ui 11 I-z 9 :J 0 7 0 5 *::; ti 3 ct: PEAK FWHM 0.000 113.212 4.922 71.373 0.000 2376 2772 3173 3578 3988 Energy (keV) COUNT DATE : 29-Sep-2016 09:18:30 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 4.000 3.520 0.480 0.6928 99.900 4.54E-02 1.000 0.520 0.480 0.6928 99.900 6.66E-03 308.000 306.800 1.200 1.0954 100.000 3.93E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 6106 6543 6985 7432 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B11 O.CNF;1440 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W110.CNF;441 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.14E-02 4.67E-02 O.OOE+OO 5.77E-02 7.14E-02 1.64E-02 3.70E-02 7.09E-02 1.63E-02 6.59E-01 8.97E-02 2.57E-02 2.59E-02 3.84E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.14E-02 5.75E-02 3.70E-02 4.41E-01 2.58E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235009 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 112 DETECTOR S/N : 78261 AVERAGE %EFFICIENCY : 34.0722 AVERAGE %EFF ERROR : 0.6563 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 87.0 +/-6.029 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.8135E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5429.74 PU-239 5155.00 5119.56 PU-242 4890.00 4857.86 PU-244 4589.00 4524.68 PU-244: 4497-4597 keV 17 PU-242:46S4-4995keV PU-239:5011-52Z7keV PlJ.23B:5375-5566keV 15 PlJ.236: 5582-5843 keV 13 11 en 9 I-z :l 7 0 s 5 *:;; 3 <I.'. 2398 2792 3191 3595 Energy (keV) PEAK FWHM 0.000 83.327 117.638 94.356 4.902 COUNT DATE : 29-Sep-2016 09:18:30 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -7.33E-03 2.000 0.560 1.440 1.2000 99.900 7.09E-03 2.000 1.520 0.480 0.6928 99.900 1.91E-02 314.000 311.840 2.160 1.4697 100.000 3.92E+OO 1.000 0.760 0.240 0.4899 99.900 9.56E-03 ll > >> l!l! :gtg 6111 6547 6987 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B112.CNF;1443 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W112.CNF;451 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.25E-02 8.46E-02 1.94E-02 4.58E-02 9.36E-02 2.78E-02 4.40E-02 6.96E-02 1.60E-02 6.54E-01 1.05E-01 3.38E-02 3.59E-02 6.03E-02 1.13E-02 1.96-sigma cnt Unc pCi/G 3.24E-02 4.58E-02 4.39E-02 4.37E-01 3.58E-02 AlphaSpectroseopySoftwareVersion3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596393 SAMPLE ID : S0405235010 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 210 DETECTOR S/N : 87898 AVERAGE %EFFICIENCY : 25.3042 AVERAGE %EFF ERROR : 0.4906 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 93.4 +/-6.681 % TRACER 1770-A PU-242 ID NUCLIDE NOMINAL RESULTS 4.3831 E+OO dpm 4.0929E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5728.05 PU-238 5486.00 5530.79 PU-239 5155.00 5117.29 PU-242 4890.00 4874.31 PU-244 4589.00 4518.61 17 PU-244: 4497-4597 keV PU-242: 4654-4995 keV PU-239: 5011-5227 keV 15 PU-238: 5375-5566 keV PU-236: 5582-5843 keV 13 11 (jJ 9 I-z ;:) 7 0 5 *;;; 3 ts <( PEAK FWHM 65.062 15.014 5.005 85.080 0.000 2381 2783 3189 3597 4009 Energy (keV) COUNT DATE : 29-Sep-2016 09:23:32 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.760 0.240 0.4899 100.000 3.39E-02 3.000 -1.320 4.320 2.0785 99.900 -2.11E-02 1.000 0.280 0.720 0.8485 99.900 4.44E-03 250.000 248.560 1.440 1.2000 100.000 3.94E+OO 2.000 2.000 0.000 0.0000 99.900 3.17E-02 ! :g:g 6119 6551 6987 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B210.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W210.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.69E-02 9.24E-02 1.73E-02 7.07E-02 1.70E-01 6.08E-02 4.65E-02 9.70E-02 2.47E-02 7.29E-01 1.17E-01 3.49E-02 5.46E-02 4.76E-02 O.OOE+OO 1.96-sigma en! Une pCi/G 6.67E-02 7.07E-02 4.65E-02 4.93E-01 5.44E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235011_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G +/-0.200 % CHAMBER : 212 DETECTOR S/N : 87900 AVERAGE %EFFICIENCY : 26.0378 AVERAGE %EFF ERROR : 0.5045 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 67.8 +/-7.649 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.9732E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5439.10 PU-239 5155.00 5132.78 PU-242 4890.00 4851.76 PU-244 4589.00 4590.71 17 PU 244* 4497-4597 keV PU-242: 4654-4995 keV PU-239: 5011-5227 keV 15 PU-238: 5375-5566 keV PU-236:5562-5643keV 13 11 UJ 9 f-z :J 7 0 5 c 3 u <1'. I I I PEAK FWHM 0.000 0.000 19.941 40.619 0.000 I I 23 76 2776 3181 3589 4000 4416 COUNT DATE : 29-Sep-2016 09:23:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.86E-02 5.000 3.800 1.200 1.0954 99.900 8.14E-02 2.000 1.280 0.720 0.8485 99.900 2.72E-02 187.000 185.800 1.200 1.0954 100.000 3.95E+OO 2.000 1.520 0.480 0.6928 99.900 3.23E-02 >> !!l! a II 1111 II I I 4835 5 5, 684 6114 6547 6984 7425 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B212.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W212.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.64E-02 1.58E-01 4.02E-02 1.06E-01 1.50E-01 4.30E-02 7.51E-02 1.30E-01 3.31E-02 8.37E-01 1.49E-01 4.26E-02 7.44E-02 1.18E-01 2.70E-02 1.96-sigma cnt Unc pCi/G 5.62E-02 1.06E-01 7.49E-02 5.72E-01 7.43E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235012 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 213 DETECTOR S/N : 87901 AVERAGE %EFFICIENCY : 24.8786 AVERAGE %EFF ERROR : 0.4826 . SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.6 +/-6.822 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.9699E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5455.35 PU-239 5155.00 5118.71 PU-242 4890.00 4873.06 PU-244 4589.00 4568.76 17 PU-244* 4497-4597 k V . PU-242:4654-4995keV PU-239:5011*5227keV 15 1--PU-238: 5375-5566 keV PU-236: 5582-5843 keV 13 en 9 I-,._ z :::> 7 ,._ 0 £ 5 ,._ 3 u <l: I I I PEAK FWHM 0.000 4.987 0.000 73.853 4.987 I I I I 23 77 2778 3182 3590 4002 441 Energy (keV) COUNT DATE : 29-Sep-2016 09:23:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -9.61E-03 1.000 0.280 0.720 0.8485 99.900 4.64E-03 0.000 -1.200 1.200 1.0954 99.900 -1.98E-02 238.000 237.040 0.960 0.9798 100.000 3.90E+OO 1.000 0.520 0.480 0.6928 99.900 8.57E-03 N I II I II I I I I I 4836 5 5! 6115 6548 6985 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B213.CNF;469 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W213.CNF;152 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.26E-02 1.11E-01 2.54E-02 4.86E-02 1.01E-01 2.58E-02 3.75E-02 1.16E-01 3.31E-02 7.37E-01 1.08E-01 2.95E-02 4.77E-02 9.13E-02 2.09E-02 1.96-sigma cnt Unc pCi/G 4.25E-02 4.85E-02 3.75E-02 4.99E-01 4.76E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235013 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 214 DETECTOR S/N : 87902 AVERAGE %EFFICIENCY : 26.2230 AVERAGE %EFF ERROR : 0.5080 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 75.4 +/-7.266 % TRACER 1770-A PU-242 ID NUCLIDE NOMINAL RESULTS 4.3831 E+OO dpm 3.3063E+OO dpm NUCLIDE LIBRARY UJ I-z ::::> 0 £ *:; ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 PU*244: 4497-4597 keV 17 PU-242: 46544995 keV PU-239: 5011-5227 keV PU-238: 5375-5566 keV 15 PU-236: 5582-5843 keV 13 11 9 7 5 3 2373 2771 3174 Energy (keV) PEAK ENERGY 5624.99 5448.78 5167.19 4873.06 4546.97 PEAK FWHM 4.958 4.958 44.618 51.228 0.000 COUNT DATE : 29-Sep-2016 09:23:39 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 1.20E-02 1.000 0.040 0.960 0.9798 99.900 7.65E-04 3.000 2.040 0.960 0.9798 99.900 3.88E-02 210.000 208.080 1.920 1.3856 100.000 3.95E+OO 0.000 -0.480 0.480 0.6928 99.900 -9.12E-03 6104 6538 6976 7419 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B214.CNF;456 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W214.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.68E-02 1.28E-01 2.93E-02 5.68E-02 1.26E-01 3.43E-02 7.73E-02 1.25E-01 3.41E-02 7.95E-01 1.53E-01 4.82E-02 4.04E-02 1.05E-01 2.41E-02 1.96-sigma cnt Unc pCi/G 6.68E-02 5.67E-02 7.71E-02 5.41E-01 4.03E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235014 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 218 DETECTOR S/N : 87906 AVERAGE %EFFICIENCY : 25.1171 AVERAGE %EFF ERROR : 0.4871 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 86.0 +/-6.952 % TRACER ID. 1770-A NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.7703E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5451.35 PU-239 5155.00 5120.15 PU-242 4890.00 4869.65 PU-244 4589.00 4591.42 PU-244: 4497-4597 keV 15 PU-242:4654-4995keV PU-239:5011..S227keV PlJ.238: 5375-5566 keV 13 PU-236:55a2-5843keV 11 0' 9 z 7 => 0 8 5 *;; 3 ti <t: PEAK FWHM 0.000 69.949 169.875 59.956 4.996 2369 2770 3176 3585 3997 Energy (keV) COUNT DATE : 29-Sep-2016 09:23:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.480 . 0.480 0.6928 100.000 -1.01E-02 2.000 1.520 0.480 0.6928 99.900 2.65E-02 4.000 2.320 1.680 1.2961 99.900 4.02E-02 228.000 227.280 0.720 0.8485 100.000 3.93E+OO 1.000 0.520 0.480 0.6928 99.900 9.01E-03 >> .:!! 6115 6550 6988 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B218.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W218.CNF;126 CAL DA TE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCl/G pCi/G 4.48E-02 1.17E-01 2.67E-02 6.10E-02 9.66E-02 2.21E-02 7.95E-02 1.34E-01 4.11E-02 7.57E-01 1.06E-01 2.69E-02 5.01E-02 9.59E-02 2.20E-02 1.96-sigma cnt Unc pCi/G 4.47E-02 6.09E-02 7.93E-02 5.14E-01 5.00E-02 BATCH NUMBER : 1596393 SAMPLE ID : S0405235015 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 235 DETECTOR S/N : 87923 AVERAGE %EFFICIENCY : 24.7991 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 97.3 +/-6.614 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.2643E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5750.94 PU-238 5486.00 5465.55 PU-239 5155.00 5118.70 PU-242 4890.00 4868.08 PU-244 4589.00 4546.97 17 PU-244: 4497-4597 keV PU-242: 4654-4995 keV PU-239: 5011-5227 keV 15 PU-238:537S.5566keV PlJ.236: 5582-5843 keV 13 11 Ui 9 I-z => 7 0 5 -2:-*:;; 3 <( PEAK FWHM 109.512 149.334 0.000 70.934 0.000 2392 2792 3196 3604 4016 Energy (keV) COUNT DATE : 09:44:15 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 3.000 1.800 1.200 1.0954 100.000 3.35E-02 5.000 4.280 0.720 0.8485 99.900 6.59E-02 0.000 -0.960 0.960 0.9798 99.900 -1.47E-02 255.000 253.800 1.200 1.0954 100.000 3.88E+OO 0.000 -0.240 0.240 0.4899 99.900 -3.67E-03 >> > u 6132 6566 7005 7447 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B235.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W235.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.62E-02 1.31E-01 3.73E-02 7.59E-02 9.41E-02 2.39E-02 3.41E-02 1.01E-01 2.75E-02 7.11E-01 1.07E-01 3.07E-02 3.17E-02 7.34E-02 1.37E-02 1.96-sigma cnt Unc pCi/G 7.60E-02 7.53E-02 3.40E-02 4.80E-01 3.17E-02 "d 00 --...J 0 ...., Vi 00 0 \0 BATCH NUMBER : 1596393 SAMPLE ID : S0405235016 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 220 DETECTOR S/N : 87908 AVERAGE %EFFICIENCY : 24.0361 AVERAGE %EFF ERROR : 0.4668 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 98.0 +/-6.688 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.2956E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.29 PU-238 5486.00 5470.36 PU-239 5155.00 5071.69 PU-242 4890.00 4882.99 PU-244 4589.00 4526.96 PlJ..244* 4497-4597 k V . 19 PU*242: 45544995 keV PlJ.239:5011*5227keV 17 PU-238: 5375-5566 keV PU-236: 5582-5843 keV 15 13 0' 11 -z 9 :::> -0 7 *:;; 3 t5 -<( 1 -11 I I I PEAK FWHM 0.000 0.000 4.978 73.840 4.978 I I I Ill I 23 77 2777 3181 3588 3998 441 D COUNT DATE : 29-Sep-2016 09:23:45 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.39E-02 0.000 -0.720 0.720 0.8485 99.900 -1.15E-02 1.000 0.760 0.240 0.4899 99.900 1.21E-02 249.000 247.800 1.200 1.0954 100.000 3.94E+OO 1.000 0.760 0.240 0.4899 99.900 1.21E-02 >> a I 1111Jl1 I I I I I I 4830 5 51 676 6104 6535 6970 7409 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B220.CNF;458 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W220.CNF;142 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.22E-02 1.18E-01 3.01E-02 3.49E-02 9.79E-02 2.49E-02 4.54E-02 7.63E-02 1.43E-02 7.30E-01 1.12E-01 3.19E-02 4.54E-02 7.63E-02 1.43E-02 1.96-sigma cnt Unc pCi/G 4.21E-02 3.48E-02 4.54E-02. 4.93E-01 4.54E-02 "t:I 00 ...... 00 0 ...., V\ 00 0 \0 BATCH NUMBER : 1596393 SAMPLE ID : S0405235017 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 221 DETECTOR S/N : 87909 AVERAGE %EFFICIENCY : 25.5264 AVERAGE %EFF ERROR : 0.4948 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 75.8 +/-7.313 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.3221 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.29 PU-238 5486.00 5444.18 PU-239 5155.00 5162.88 PU-242 4890.00 4871.18 PU-244 4589.00 4581.20 14 PU-244: 4497-4597 keV PlJ.242:4654-4995keV 13 PU-239: 5011-5227 keV 12 PU-238:5375-5566keV PU-236: 5582-5843 keV 11 10 9 <ii 8 I-7 z 6 ::> 0 5 4 3 *:;; u 2 <( 1 2382 2784 3190 3599 Energy (keV) PEAK FWHM 0.000 5.006 45.052 69.899 0.000 4011 COUNT DATE : 29-Sep-2016 09:23:48 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.70E-02 1.000 0.520 0.480 0.6928 99.900 1.01E-02 2.000 1.280 0.720 0.8485 99.900 2.48E-02 204.000 203.520 0.480 0.6928 100.000 3.94E+OO 2.000 1.760 0.240 0.4899 99.900 3.41E-02 l l I &'! a 6124 6557 6993 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B221.CNF;467 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W221.CNF;128 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.16E-02 1.45E-01 3.68E-02 5.64E-02 1.08E-01 2.48E-02 6.84E-02 1.18E-01 3.01E-02 7.98E-01 1.07E-01 2.46E-02 6.72E-02 9.29E-02 1.74E-02 1.96-sigma cnt Unc pCi/G 5.15E-02 5.64E-02 6.83E-02 5.44E-01 6.71E-02 "ti (1) 00 -"' 0 ...., Ul 00 0 "' BATCH NUMBER : 1596393 SAMPLE ID : S0405235018 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 223 DETECTOR S/N : 87911 AVERAGE %EFFICIENCY : 25.6333 AVERAGE %EFF ERROR : 0.4968 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 80.7 +/-7.090 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.5358E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5691.16 PU-238 5486.00 5476.68 PU-239 5155.00 5118.71 PU-242 4890.00 4875.08 PU-244 4589.00 4546.97 15 PU-244: 4497-4597 keV PU-242: 4654-4995 keV PU-239: 5011-5227 keV 13 PV-238: 5375-5566 keV PU-236: 5582-5843 kaV 11 Ui 9 I-7 z :::> 0 5 8 3 <l'. PEAK FWHM 24.821 49.642 0.000 61.981 0.000 COUNT DATE : 29-Sep-2016 09:23:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.520 0.480 0.6928 100.000 3.37E-02 3.000 1.560 1.440 1.2000 99.900 2.85E-02 0.000 -0.240 0.240 0.4899 99.900 -4.36E-03 218.000 217.520 0.480 0.6928 100.000 3.95E+OO 0.000 -0.240 0.240 0.4899 99.900 -4.36E-03 > ! a 2377 2776 3178 3584 3994 440 4825 6098 6529 6965 7403 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B223.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W223.CNF;114 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.76E-02 1.23E-01 2.82E-02 7.53E-02 1.35E-01 4.02E-02 3.77E-02 8.71E-02 1.63E-02 7.75E-01 1.01E-01 2.30E-02 3.77E-02 8.71E-02 1.63E-02 1.96-sigma cnt Unc pCi/G 7.75E-02 7.52E-02 3.76E-02 5.27E-01 3.76E-02 "'Cl ('1) 00 N 0 0 ....., V\ 00 0 '° BATCH NUMBER : 1596393 SAMPLE ID : S0405235019 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 224 DETECTOR S/N : 87912 AVERAGE %EFFICIENCY : 25.7363 AVERAGE %EFF ERROR : 0.4987 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.2 +/-6.738 % TRACER 1770-A JD NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.9555E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5458.69 PU-239 5155.00 5183.32 PU-242 4890.00 4876.19 PU-244 4589.00 4546.97 PU 244* 4497-4597 keV 23 PU-242: 4654-4995 keV 21 .-PU*239:5011-5227keV PU-238: 5375-5566 keV 19 t-PU-236: 5582-5843 keV 17 r 15 r (ii 13 r I-11 z f-=> 9 0 f-£ 7 f-£ 5 > r t5 3 r <( r I 11 I I I PEAK FWHM 0.000 4.920 0.000 66.419 0.000 I I 23 99 2795 3195 3599 4007 442D Energy (keV) COUNT DATE : 29-Sep-2016 09:23:52 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 -0.440 1.440 1.2000 99.900 -7.08E-03 5.000 4.280 0.720 0.8485 99.900 6.84E-02 246.000 244.320 1.680 1.2961 100.000 3.90E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO a l111ll II I I I I I I I I 4836 5 5, 682 6112 6545 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B224.CNF;471 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W224.CNF;150 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.93E-02 5.83E-02 O.OOE+OO 4.89E-02 1.19E-01 3.54E-02 7.88E-02 9.77E-02 2.48E-02 7.28E-01 1.24E-01 3.79E-02 3.23E-02 4.80E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.92E-02 4.89E-02 7.82E-02 4.92E-01 3.22E-02 Alpha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar.2015 BATCH NUMBER : 1596393 SAMPLE ID : S0405235020 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 226 DETECTOR S/N : 87914 AVERAGE %EFFICIENCY : 26.8347 AVERAGE %EFF ERROR : 0.5195 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 74.0 +/-7.240 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 3.2421E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5661.00 PU-238 5486.00 5447.11 PU-239 5155.00 5118.70 PU-242 4890.00 4861.53 PU-244 4589.00 4535.50 15 PU 244' 4497-4597 keV -. PLJ.242:4654-4995keV PlJ.239:5011-5227keV 13 _ pu.23a: 5375-5566 keV PU*236: 5582-5643 keV 11 -en 9 -I-7 z -::::> 0 5 -3 *;; r ti <( rl I I PEAK FWHM 4.984 54.821 0.000 50.564 0.000 II I 23 72 2772 3177 3585 3997 441 COUNT DATE : 29-Sep-2016 09:23:54 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 1.000 0.000 0.0000 100.000 2.29E-02 2.000 1.280 0.720 0.8485 99.900 2.43E-02 0.000 -1.440 1.440 1.2000 99.900 -2.72E-02 210.000 208.800 1.200 1.0954 100.000 3.93E+OO 4.000 3.760 0.240 0.4899 99.900 7.09E-02 i I I 11 I I I I 4832 5 5t 682 6113 6548 6986 7428 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B226.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W226.CNF;122 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.46E-02 6.88E-02 O.OOE+OO 6.69E-02 1.16E-01 2.95E-02 4.39E-02 1.39E-01 4.14E-02 7.89E-01 1.32E-01 3.78E-02 8.42E-02 9.04E-02 1.69E-02 1.96-sigma cnt Unc pCi/G 6.45E-02 6.68E-02 4.38E-02 5.37E-01 8.36E-02 BATCH NUMBER : 1596393 SAMPLE ID : S1203621700 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 227 DETECTOR S/N : 87915 AVERAGE %EFFICIENCY : 26.3665 AVERAGE %EFF ERROR : 0.5107 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 91.8 +/-6.608 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 4.0228E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5151.00 PU-242 4890.00 4857.07 PU-244 4589.00 4546.97 PU-244: 4497-4597 keV 17 PU-242:4654-4995keV PU-239:5011*5227keV PU-238:5375-5566keV 15 PU-236: 5582-5843 keV 13 11 fj) 9 I-z ::J 7 0 S?. 5 c *s; 3 :g <( 2375 2771 3171 3576 Energy (keV) PEAK FWHM 0.000 0.000 54.147 64.520 0.000 3984 COUNT DATE : 29-Sep-2016 09:24:00 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.200 1.200 1.0954 99.900 -1.83E-02 6.000 3.840 2.160 1.4697 99.900 5.86E-02 256.000 254.560 1.440 1.2000 100.000 3.88E+OO 0.000 -0.240 0.240 0.4899 99.900 -3.66E-03 ni > 6091 6525 6963 7405 ; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B227.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W227.CNF;120 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.09E-02 4.58E-02 O.OOE+OO 3.47E-02 1.07E-01 3.06E-02 8.27E-02 1.28E-01 4.11E-02 7.10E-01 1.13E-01 3.35E-02 3.16E-02 7.31E-02 1.37E-02 1.96-sigma cnt Unc pCi/G 3.0BE-02 3.47E-02 8.23E-02 4.79E-01 3.16E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596393 SAMPLE ID : S1203621701_PU SAMPLE QTY : 0.500 G +/-0.200 % CHAMBER : 228 DETECTOR S/N : 87916 AVERAGE %EFFICIENCY : 25.5769 AVERAGE %EFF ERROR : 0.4958 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 56.0 +/-8.523 % TRACER 1770-A ID NUCLIDE NOMINAL RESULTS PU-242 4.3831E+OO dpm 2.4540E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5387.67 PU-239 5155.00 5149.45 PU-242 4890.00 4853.01 PU-244 4589.00 4546.97 10 PU-244: 4497-4597 keV PU-242: 46544995 keV 9 PlJ.239:5011-5227keV PU-238:5375-5566keV 8 PU*236:5582-584JkeV 7 6 5 z ::i 4 0 f2, 3 2 u <i:: 2369 Energy (keV) PEAK FWHM 0.000 9.940 114.305 101.632 0.000 COUNT DATE : 29-Sep-2016 09:23:57 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -3.82E-02 2.000 1.280 0.720 0.8485 99.900 3.38E-02 4.000 1.840 2.160 1.4697 99.900 4.83E-02 154.000 150.640 3.360 1.8330 100.000 3.95E+OO 0.000 -0.720 0.720 0.8485 99.900 -1.89E-02 6096 6528 6964 7404 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B228.CNF;457 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W228.CNF;117 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.27E-02 2.24E-01 6.40E-02 9.32E-02 1.61E-01 4.10E-02 1.22E-01 2.20E-01 7.06E-02 9.32E-01 2.55E-01 8.80E-02 5.72E-02 1.60E-01 4.08E-02 1.96-sigma cnt Unc pCi/G 7.25E-02 9.30E-02 1.21E-01 6.41E-01 5.70E-02 AlphaSpectroscopySoftwareVersion3.5.3 effectivedate:02+Mar-2015 BATCH NUMBER : 1596393 SAMPLE ID : S1203621702 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 54.3 +/-8.378 % TRACER ID 1770-A NUCLIDE PU-242 NOMINAL 4.3831E+OO dpm RESULTS 2.3815E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5669.61 4.955 PU-238 5486.00 5480.68 138.746 PU-239 5155.00 5132.07 56.572 PU-242 4890.00 4870.35 54.817 PU-244 4589.00 4546.97 0.000 15 PU-244: 4497-4597 keV PU-242:4654-4995keV PU-239:5011*5227keV 13 PU-238: 5375-5566 keV PU.236: 5582-5843 keV 11 Ui 9 1--7 z ::J 0 5 8 c 3 *:;; ti <( 2375 2774 3177 3583 3994 Energy (keV) COUNT DATE : 29-Sep-2016 14:16:08 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0338-MM NUCLIDE PU-239 NOMINAL (pCi/G) 3.8823E+OO % RECOVERY 111.200 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA .AREA AREA StDev pCi/G 1.000 -0.200 1.200 1.0954 100.000 -5.12E-03 4.000 3.520 0.480 0.6928 99.900 8.99E-02 169.000 169.000 0.000 0.0000 99.900 4.32E+OO 152.000 152.000 0.000 0.0000 100.000 3.88E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO ll >> > !!.!! jl ::\ a ;* 6112 6548 6989 7433 ; Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : PU BKG FILE : B177.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 7.69E-02 1.79E-01 5.13E-02 1.15E-01 1.41E-01 3.24E-02 9.78E-01 7.66E-02 0.00E+OO 9.00E-01 7.66E-02 O.OOE+OO 5.17E-02 7.66E-02 O.OOE+OO 1.96-sigma cnt Unc pCl/G 7.68E-02 1.14E-01 6.53E-01 6.19E-01 5.15E-02 Effective 3/25/2010 Revision 1 Effective March 2010 Criteria: sample Solids are less than or eaual to 100 mil for GAB. Samples have been blank corrected (If required). Blank correction renorted Included I If reauired). If activity less than lOx MDA/MDC, error Is less than or equal to 1500/o of sample activity. If areater than 10* MDA/ MDC, error Is 40% or less. If holnm tho un.& / unr nrrnr '" Instrument source check Is within limits. hka check 1 .. within limits Method RDL/ LLD has been met. If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's renulred RER accentance criteria. Tracer yield ls 15-125%

Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. (Tf <:' <;O/n nf "rtlultv\ Radiochemistry Batch Checklist 23-Sep-2016 oate: 9 /:7-S} 1 Yes No Comments f\)& NA / / v/ / \/'" / Samnle was run within hold time. v f l q \ Samnle was correctlv nreserved If reoulred. Smears Taken for Radioactive batches. \...hr Method Spike and LCS are within 75-125% 'r or me""" the client's cnntr"rt acc1>nbnce criteria l. / No blank spaces on data forms. All line outs Initialed and dated. \,/"" Nn nrrnrr Aux data Is correct. f..)?* Client Soeclal reaulrements naae has been checked. Raw Data and/ or spectrum are Included and orooerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ...,..... """""' v1>rlflarl ,..,,. flf l.M ...... !n .... *-1-. ............... __ ... 1 .......... ,...,. ....... ,,, Batch Data Exceotlon Reoorts {DER) comoleted. If aoollcable. ,/ l "5Lo \ l q I Batch Data Exception Reports (DER) second reviewed. ../ l\toll°tl Disposition verified to be comoleted. Allnnnt Correction comoleted If ronulred. ,..:.,Y,1-Review sample historical results If available / {If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l vr f} ,uS,jO<.,,. Q , ,, r1 Primary Review Performed By:, ___ 1 /_IYJ), ____ __ _ Secondary Review Performed By:__ 09/30/16 @ 809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 25-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, Am-05-RC Solid Batch ID: Sample Numbers: 1596410 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060,and1203621746 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 25-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 826 of 5809 DER Report No.: 1561191 Revision No.: 1 Type: Process Client Code: MJWC Am/Cm Queue Sheet Batch#: 1596410 Analyst: HAKB First Client Due Date: 04-0CT-16 Internal Due Date:30-SEP-16 Tracer Code: \ '15.1 -C... Expiration Date: I lJ\,U; . LCS LCS Code(s): D S.3 3 -CC.. I t4. \I..., -

o l \lo Spike lsotope(s): Am241/Cm244 Spike Code(s): -I Expiration Date: -I -Prep Date: ti\ b..a \ \I. Pipet ID: \<b'Icx1$ Balance ID: \ o"1 L. k '2.-Witness: JJ.t> I I Sample ID Client Description 405235041-1 4.4D.R.1.4 405235042-1 4.4D.R.2.3 405235043-1 4.40.R.2.4 405235044*1 4.4DJU.2 405235045-1 4.4D.R.S.2 41b"235046-1 4.SA.IU.3 40:>"235047-1 4.SA.R.1.4 405"-35648*1 4.SB.R.1.2 405235049-I 4.SB.R.1.3 405235050..1 4.SB.R.1.4 405'-35051-1 4.5B.R.2.3 405235052-1 4.SB.R.2.4 405235053-1 4.SC.R.5.2 405235054-1 4.SC.R.1.3 405235055-1 4.SC.R.1.4 405235056-1 4.SC.R.2.2 405235057-1 4.Sc.R.2.3 405235058-1 4.SC.R.2.4 405235059-1 5.lA.R.1.2 405235066-1 5.lA.R.1.3 1203621745-1 MB for batch 1596410 1203621746-1 4.4D.R..l.4{405235041DUP) 1203621747-1 LCS for batch 1596410 Choose SOP Used: GL-RAD-A-011 GL-RAD-A-036 GEL Laboratories LLC, RaJ!wcllemistry Divisioll Type SAMPLE SAMPLE SAMPLE SAMPLE SAi\fi'LE SAMPLE SAMPLE SAJ\ll'LE SAMPLE SAi'\.IPLE SAJ\IPLE SAJ\:IPLE SAMPLE SAMPLE SAMPLE SAl\fPLE SAMPLE SAMPLE SA.T\fi>LE SAMPLE :r.m DlJP LCS Hazard Min Code CRDL lpCi/g lpCi/g lpCi/g lpCilg 1 pC'i/g 1 pCi/g l_pCi/g lpCi/g 1 pCi/g 1 pCifg 1 pC'v'g lpCi/g 1 pCi/g l pCilg l pCifg 1 pCi/g lpC'v'g 1 pC'r/g lpC'v'g 1 pC'v'g lpCVg 1 pCi/g 1 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Client l\fJWCOOl MJWCOOl MJWCOOl 1\-!JWCOOI l.'.tJWCOOl M'JWCOOl MJWCOOl MJWCOOl MJWCOOl J\.tJWCOOI MJWCOOl MJWCOOl l\fJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOI MJWCOOl QC ACCOUl'\'T QC ACCOUNT QC ACCOUNT Solid Sample Dissolution by: LEACH or@GESTI@ Circle One Collection Date 30.NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 01-DEC-15 DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 16-DEC-15 16-DEC-15 30-N0\'-15 Comments: Vol: ...e * \ Vol(s))¢.-t-/ .J'!S * \ Vol(s): -I SEP-16 Analyzed Sequentiallv with U: I S<j l.lf Dg Pu: IS9 k4 I 2-Wet/f!fj Label Aliquot Am/Cm Pos. # @,'Y l/ f) Det # Page loft "ti 00 N 00 0 ...., Vl 00 0 \0 BATCH NUMBER : 1596410 SAMPLE ID : S0405235041 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 106 DETECTOR S/N : 80012 AVERAGE %EFFICIENCY : 32.6615 AVERAGE %EFF ERROR : 0.6296 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 107 +/-7.018 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 5.0683E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5421.98 AM-243 5269.50 5258.18 CM-242 6102.00 6086.56 CM-3/4 5795.02 5737.76 CM-5/6 5386.00 5385.09 CM-247 4946.00 4855.67 CM-248 5078.60 5066.41 CM-247: 47754987 keV 17 CM-248: 5009-5105 keV AM-243:5131-5366keV CM-516: 5372-5398 keV 15 AM-241: 54Q4..5613 keV CM-3f4:5646-5878keV 13 CM-242:5975-6198keV 11 if) 9 I-z ::::> 7 0 £ 5 *:;; 3 t5 <{ PEAK FWHM 4.904 69.150 0.000 4.904 0.000 102.989 39.234 2387 2782 3181 3585 3993 4406 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:16 ELAPSED LIVE TIME(SEC) : 8706.02 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.596 1.596 1.2634 98.525 -1.06E-02 241.000 240.129 0.871 0.9331 99.980 4.20E+OO 0.000 -0.145 0.145 0.3809 100.000 -8.99E-03 1.000 0.855 0.145 0.3809 100.000 1.54E-02 0.000 0.000 0.000 0.0000 86.090 0.00E+OO 6.000 4.839 1.161 1.0774 79.300 1.07E-01 5.000 4.855 0.145 0.3809 91.000 9.33E-02 6541 6982 7427 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B106.CNF;1396 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W106.CNF;363 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.23E-02 1.32E-01 3.95E-02 8.02E-01 1.10E-01 2.87E-02 1.24E-01 2.69E-01 4.15E-02 5.06E-02 7.83E-02 1.21E-02 4.03E-02 6.09E-02 O.OOE+OO 1.17E-01 1.50E-01 4.18E-02 9.35E-02 8.34E-02 1.29E-02 1.96-sigma cnt Unc pCi/G 5.23E-02 5.33E-01 1.24E-01 5.05E-02 4.02E-02 1.16E-01 9.25E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235042 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 233 DETECTOR S/N : 87921 AVERAGE %EFFICIENCY : 25.2931 AVERAGE %EFF ERROR : 0.4905 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 64.6 +/-10.771 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.0649E+OO dpm NUCLIDE LIBRARY ENERGY AM-241 5480.15 AM-243 5269.50 CM-242 6102.00 CM-3/4 5795.02 CM-5/6 5386.00 CM-247 4946.00 CM-248 5078.60 14 CM-247* 4775-4987 keV CM-248: 5009-5105 keV 13 12 11 10 9 8 7 6 5 4 3 2 1 "-AM-243: 5131-5366 keV CM-5!6: 5372*5398 keV i-AM-241:5404-5613keV f-CM-3!4: 5646-5878 keV CM-242:5975-6198keV f-f-f-f-f-I PEAK ENERGY 5508.50 5284.20 6086.59 5761.62 5369.51 4881.20 5056.59 I PEAK FWHM 0.000 25.060 0.000 0.000 0.000 0.000 0.000 I I I I 23 96 2795 3198 3605 4016 4430 Energy (keV) COUNT DATE : 22-Sep-2016 16:14:38 ELAPSED LIVE TIME(SEC) : 7200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.120 0.120 0.3464 98.525 -5.60E-03 93.000 93.000 0.000 0.0000 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.880 0.120 0.3464 86.090 4.70E-02 0.000 -0.480 0.480 0.6928 79.300 -2.78E-02 0.000 -0.120 0.120 0.3464 91.000 -6.06E-03 I I I I I I I L 848 526 E B94 612B 6555 6991 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B233.CNF;452 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W233.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.34E-02 1.96E-01 2.82E-02 1.27E+OO 1.38E-01 O.OOE+OO 3.24E-01 4.89E-01 O.OOE+OO 9.41E-02 1.42E-01 0.00E+OO 1.49E-01 2.25E-01 3.22E-02 1.18E-01 3.14E-01 6.99E-02 1.01E-01 2.12E-01 3.04E-02 1.96-sigma cnt Unc pCi/G 9.28E-02 8.73E-01 3.22E-01 9.36E-02 1.49E-01 1.18E-01 1.00E-01 Alpha Spectroscopy Software Version 3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596410 SAMPLE ID : S0405235043 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 210 DETECTOR S/N : 87898 AVERAGE %EFFICIENCY : 25.3042 AVERAGE %EFF ERROR : 0.4906 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 75.5 +/-7.897 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.5824E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5474.95 AM-243 5269.50 5284.72 CM-242 6102.00 6086.60 CM-3/4 5795.02 5781.48 CM-5/6 5386.00 5371.38 CM-247 4946.00 4916.98 CM-248 5078.60 5056.59 CM-247:4775-4987keV 21 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 19 CM-5!6:5372-5398keV AM-241: 5404-5613 keV 17 CM-3/4: 5646-5878 keV CM-242:597!Hi198keV 15 Yi 13 f-11 z ::> 9 0 i2. 7 5 *s: t5 3 <!'. PEAK FWHM 70.066 42.540 0.000 5.005 0.000 0.000 0.000 2381 2783 3189 3597 4009 4425 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:00 ELAPSED LIVE TIME(SEC) : 12284.26 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.795 0.205 0.4525 98.525 4.14E-02 188.000 185.543 2.457 1.5674 99.980 4.22E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 1.000 0.000 0.0000 100.000 2.34E-02 3.000 2.795 0.205 0.4525 86.090 7.37E-02 2.000 1.795 0.205 0.4525 79.300 5.14E-02 0.000 -0.409 0.409 0.6399 91.000 -1.02E-02 6551 6987 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B210.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W210.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.97E-02 1.07E-01 1.89E-02 9.10E-01 1.97E-01 6.43E-02 1.62E-01 2.42E-01 O.OOE+OO 6.57E-02 7.03E-02 O.OOE+OO 1.05E-01 1.22E-01 2.16E-02 9.89E-02 1.33E-01 2.34E-02 5.21E-02 1.33E-01 2.88E-02 1.96-sigma en! Unc pCi/G 7.94E-02 6.13E-01 1.61E-01 6.56E-02 1.05E-01 9.86E-02 5.19E-02 0 ...., Vi 00 0 \0 BATCH NUMBER : 1596410 SAMPLE ID : S0405235044 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 211 DETECTOR S/N : 87899 AVERAGE %EFFICIENCY : 24.1091 AVERAGE %EFF ERROR : 0.4680 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 88.8 +/-7.498 % TRACER 1752-C . ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.2117E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5426.05 AM-243 5269.50 5278.75 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5373.02 CM-247 4946.00 4945.50 CM-248 5078.60 5050.71 CM-247: 4775-4987 keV 23 CM-248: 5009-5105 keV AM-243: 5131-5366 keV 21 CM-5/6:5372-5398keV AM-241: 5404-5613 keV 19 CM-3/4: 5646-5878 keV CM-242: 5975-6198 keV 17 15 (ii 13 I-z 11 :J 9 0 £ 7 c 5 *;; ts 3 <( 1 PEAK FWHM 4.967 36.836 0.000 0.000 0.000 4.967 4.967 2375 2774 3177 3583 3993 4407 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:03 ELAPSED LIVE TIME(SEC) : 12291.35 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 -0.639 1.639 1.2802 98.525 -1.32E-02 210.000 207.951 2.049 1.4313 99.980 4.23E+OO 0.000 -0.205 0.205 0.4526 100.000 -1.48E-02 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 3.000 2.795 0.205 0.4526 86.090 6.61E-02 1.000 0.385 0.615 0.7839 79.300 9.89E-03 1.000 -0.229 1.229 1.1087 91.000 -5.12E-03 >>>> >!>-> >> = !l 6531 6967 7407 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B211.CNF;454 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W211.CNF;131 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.26E-02 1.58E-01 4.78E-02 8.66E-01 1.66E-01 5.26E-02 1.48E-01 3.34E-01 5.89E-02 4.21E-02 6.30E-02 O.OOE+OO 9.41E-02 1.10E-01 1.93E-02 7.41E-02 1.50E-01 3.63E-02 6.65E-02 1.57E-01 4.48E-02 1.96-sigma cnt Unc pCi/G 6.25E-02 5.80E-01 1.47E-01 4.20E-02 9.36E-02 7.40E-02 6.64E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235045 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 212 DETECTOR S/N : 87900 AVERAGE %EFFICIENCY : 26.0378 AVERAGE %EFF ERROR : 0.5045 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 80.1 +/-7.552 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.7985E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5443.36 AM-243 5269.50 5277.70 CM-242 6102.00 6086.59 CM-3/4 5795.02 5710.36 CM-5/6 5386.00 5384.81 CM-247 4946.00 4939.99 CM-248 5078.60 5040.26 CM-247: 4n54987 keV 23 CM-248: 5009-5105 keV AM-243: 5131*5366 keV 21 CM-516: 5372-5398 keV AM-241: 5404-5613 keV 19 CM-3/4:5645-5878keV CM-242:5975-6198keV 17 15 Ul 13 1--11 z :::> 9 0 7 .;::. 5 *:;; 3 1 PEAK FWHM 4.985 28.915 0.000 4.985 4.985 4.985 4.985 2376 2776 3181 3589 4000 4416 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:06 ELAPSED LIVE TIME(SEC) : 12293.51 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.590 0.410 0.6401 98.525 1.26E-02 203.000 202.590 0.410 0.6401 99.980 4.26E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.590 0.410 0.6401 100.000 1.28E-02 1.000 1.000 0.000 0.0000 86.090 2.44E-02 1.000 -0.024 1.024 1.0122 79.300 -6.48E-04 1.000 1.000 0.000 0.0000 91.000 2.31E-02 6547 6984 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B212.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W212.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.11E-02 1.13E-01 2.47E-02 8.77E-01 1.12E-01 2.43E-02 1.49E-01 2.23E-01 O.OOE+OO 6.20E-02 1.15E-01 2.51E-02 6.85E-02 7.32E-02 O.OOE+OO 7.80E-02 1.76E-01 4.84E-02 6.48E-02 6.93E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.10E-02 5.88E-01 1.49E-01 6.19E-02 6.84E-02 7.79E-02 6.47E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235046 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G -+/-0.195 % CHAMBER : 213 DETECTOR S/N : 87901 AVERAGE %EFFICIENCY : 24.8786 AVERAGE %EFF ERROR : 0.4826 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 106 +/-6.834 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 5.0354E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5455.35 AM-243 5269.50 5279.63 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5370.23 CM-247 4946.00 4920.43 CM-248 5078.60 5056.59 34 CM-247* 4n5-4987 keV CM-248: 5009-5105 keV 31 f--AM-243:5131-5366keV CM--5f6:5372-5398keV 28 AM-241: 5404-5613 keV CM-3/4; 5646-5878 keV 25 22 r-(ii 19 r I-16 z r =i 13 0 r i2, 10 r 0 *;;; 7 r t5 4 <t: r-I I I 23 77 2778 3182 3590 Energy (keV) PEAK FWHM 4.987 37.402 0.000 0.000 0.000 4.987 0.000 4002 4417 COUNT DATE : 22-Sep-2016 09:56:08 ELAPSED LIVE TIME(SEC) : 12291.75 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.385 0.615 0.7840 98.525 2.28E-02 258.000 256.566 1.434 1.1975 99.980 4.16E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.205 0.205 0.4526 100.000 -3.42E-03 1.000 1.000 0.000 0.0000 86.090 1.88E-02 1.000 0.385 0.615 0.7840 79.300 7.87E-03 0.000 -0.205 0.205 0.4526 91.000 -3.65E-03 Ufi = H = fu I I I I I 4836 ti25! ! BBS 611 ' 6548 6985 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B213.CNF;467 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W213.CNF;152 CAL DA TE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.75E-02 9.60E-02 2.33E-02 7.73E-01 1.19E-01 3.50E-02 1.12E-01 1.67E-01 O.OOE+OO 3.42E-02 7.74E-02 1.36E-02 5.28E-02 5.65E-02 O.OOE+OO 5.90E-02 1.19E-01 2.89E-02 3.64E-02 8.25E-02 1.45E-02 1.96-sigma cnt Unc pCi/G 5.74E-02 5.11E-01 1.12E-01 3.41E-02 5.27E-02 5.90E-02 3.63E-02 AlphaSpectroscopySoftwareVerslon3.5.3 affectiveda!e:02-Mar-2015 BATCH NUMBER : 1596410 SAMPLE ID : S0405235047 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 214 DETECTOR S/N : 87902 AVERAGE %EFFICIENCY : 26.2230 AVERAGE %EFF ERROR : 0.5080 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 103 +/-6.774 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.8629E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5279.08 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5374.23 CM-247 4946.00 4924.20 CM-248 5078.60 5056.58 CM-247' 4775-4987 keV 31 CM-248: 5009-5105 keV AM-243: 5131-5366 keV CM-516: 5372-5398 kaV 28 AM-241: 5404-5613 keV CM.314: 564S.5878keV 25 CM-242: 5975-£198 keV 22 (ii 19 I-16 z :l 13 0 10 7 *:;; ti 4 <i: 1 I I I PEAK FWHM 0.000 32.307 0.000 0.000 0.000 4.958 0.000 I I 23 73 2771 3174 3581 3991 4406 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:10 ELAPSED LIVE TIME(SEC) : 12292.20 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.819 0.819 0.9053 98.525 -1.35E-02 262.000 261.181 0.819 0.9053 99.980 4.25E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.615 0.615 0.7840 100.000 -1.03E-02 1.000 1.000 0.000 0.0000 86.090 1.89E-02 1.000 -0.639 1.639 1.2802 79.300 -1.31E-02 0.000 -0.410 0.410 0.6401 91.000 -7.32E-03 I i I I I I I 4324 241 5 73 610 6538 6976 7419 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B214.CNF;454 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W214.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.57E-02 1.04E-01 2.70E-02 7.82E-01 1.02E-01 2.66E-02 1.12E-01 1.68E-01 O.OOE+OO 3.56E-02 9.78E-02 2.37E-02 5.30E-02 5.67E-02 O.OOE+OO 6.20E-02 1.56E-01 4.74E-02 3.72E-02 9.49E-02 2.07E-02 1.96-sigma cnt Unc pCi/G 3.56E-02 5.17E-01 1.12E-01 3.55E-02 5.29E-02 6.20E-02 3.72E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235048 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 234 DETECTOR S/N : 87922 AVERAGE %EFFICIENCY : 24.8037 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 100 +/-8.859 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.7640E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5481.20 AM-243 5269.50 5278.86 CM-242 6102.00 6086.60 CM-3/4 5795.02 5704.82 CM-5/6 5386.00 5385.09 CM-247 4946.00 4896.43 CM-248 5078.60 5056.59 15 CM*247: 4n5-4987 keV CM-248: 5009-5105 keV AM-243: 5131*5366 keV 13 CM-516: 5372*5398 keV AM-241:5404-5613keV CM-3/4:5646-5876keV 11 CM-242:597s.6198keV en 9 1--7 z ::i 0 5 3 *:;; PEAK FWHM 4.996 49.131 0.000 89.934 0.000 124.908 0.000 2388 2790 3194 3603 4014 4429 Energy (keV) COUNT DATE : 22-Sep-2016 16:14:39 ELAPSED LIVE TIME(SEC) : 7200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.760 0.240 0.4899 98.525 2.30E-02 142.000 141.760 0.240 0.4899 99.980 4.22E+OO 0.000 -0.120 0.120 0.3464 100.000 -1.23E-02 3.000 2.520 0.480 0.6928 100.000 7.72E-02 0.000 -0.120 0.120 0.3464 86.090 -4.14E-03 3.000 2.760 0.240 0.4899 79.300 1.03E-01 0.000 -0.120 0.120 0.3464 91.000 -3.92E-03 m :a:a = = 6554 6990 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B234.CNF;452 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W234.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.48E-02 1.42E-01 2.58E-02 1.02E+OO 1.40E-01 2.54E-02 2.04E-01 4.31E-01 6.17E-02 1.22E-01 1.66E-01 3.70E-02 6.89E-02 1.45E-01 2.08E-02 1.49E-01 1.76E-01 3.20E-02 6.52E-02 1.37E-01 1.97E-02 1.96-sigma cnt Unc pCi/G 8.46E-02 6.97E-01 2.04E-01 1.21E-01 6.87E-02 1.48E-01 6.49E-02 Alpha Spectn:iscopy Software Version 3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596410 SAMPLE ID : S0405235049 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 235 DETECTOR S/N : 87923 AVERAGE %EFFICIENCY : 24.7991 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 94.8 +/-9.099 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.4960E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5524.27 AM-243 5269.50 5277.33 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5369.62 CM-247 4946.00 4881.20 CM-248 5078.60 5056.58 15 CM-247* 4775-4957 keV CM-245: 5009-5105 keV AM-243: 5131-5366 keV 13 _ CM-516: 5372-5395 keV AM-241: 5404-5613 keV CM-3/4:5646-SS78keV 11 _ CM-242: 5975-6195 keV 9 7 z ::> 0 5 -3 *:;; u <( I I I I PEAK FWHM 114.490 39.822 0.000 0.000 0.000 0.000 0.000 I I 23 92 2792 3196 3604 4016 4431 Energy (keV) COUNT DATE : 22-Sep-2016 16:14:41 ELAPSED LIVE TIME(SEC) : 7200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 2.000 1.760 0.240 0.4899 98.525 5.65E-02 134.000 133.760 0.240 0.4899 99.980 4.22E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.360 0.360 0.6000 100.000 -1.17E-02 1.000 1.000 0.000 0.0000 86.090 3.67E-02 0.000 -0.840 0.840 0.9165 79.300 -3.34E-02 0.000 -0.240 0.240 0.4899 91.000 -8.33E-03 i II I I I I I I I '851 527 ! 701 6132 6566 7005 7447 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B235.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W235.CNF;118 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.10E-01 1.51E-01 2.74E-02 1.05E+OO 1.49E-01 2.69E-02 2.16E-01 3.26E-01 O.OOE+OO 6.59E-02 1.66E-01 3.40E-02 1.02E-01 1.10E-01 O.OOE+OO 8.27E-02 2.46E-01 6.35E-02 6.97E-02 1.63E-01 2.96E-02 1.96-sigma cnt Unc pCi/G 1.10E-01 7.19E-01 2.15E-01 6.56E-02 1.02E-01 8.24E-02 6.94E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235050 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 236 DETECTOR S/N : 87924 AVERAGE %EFFICIENCY : 25.7707 AVERAGE %EFF ERROR : 0.4994 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 93.3 +/-9.029 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.4287E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5510.82 AM-243 5269.50 5279.99 CM-242 6102.00 6086.58 CM-3/4 5795.02 5726.99 CM-516 5386.00 5385.09 CM-247 4946.00 4815.69 CM-248 5078.60 5056.58 13 CM-247: 4775-4987 keV CM-248: 5009-5105 keV 12 AM-243: 5131*5366 keV CM-5'6: 5372*5398 keV 11 AM-241: 5404-5613 keV 10 CM*314:5646-SB78keV CM-242:5975-6198keV 9 8 en 7 I-6 z ::::> 5 0 4 3 *:;; 2 t5 <i: 1 PEAK FWHM 79.378 62.634 0.000 4.961 0.000 4.961 0.000 2386 2785 3188 3594 4004 4419 Energy (keV) COUNT DATE : 22-Sep-2016 16:14:43 ELAPSED LIVE TIME(SEC) : 7200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 2.000 1.760 0.240 0.4899 98.525 5.54E-02 138.000 136.920 1.080 1.0392 99.980 4.24E+OO 0.000 -0.120 0.120 0.3464 100.000 -1.28E-02 1.000 0.640 0.360 0.6000 100.000 2.04E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 1.000 0.400 0.600 0.7746 79.300 1.56E-02 0.000 0.000 0.000 0.0000 91.000 O.OOE+OO 6547 6984 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B236.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W236.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.08E-01 1.48E-01 2.68E-02 1.05E+OO 2.05E-01 5.60E-02 2.13E-01 4.49E-01 6.43E-02 8.99E-02 1.62E-01 3.33E-02 7.13E-02 1.08E-01 O.OOE+OO 1.11E-01 2.22E-01 5.26E-02 6.74E-02 1.02E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.08E-01 7.16E-01 2.12E-01 8.97E-02 7.10E-02 1.11E-01 6.72E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235051 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 218 DETECTOR S/N : 87906 AVERAGE %EFFICIENCY : 25.1171 AVERAGE %EFF ERROR : 0.4871 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 70.3 +/-8.174 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.3366E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5277.39 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5385.09 CM-247 4946.00 4881.20 CM-248 5078.60 5056.59 CM-247: 4775-4987 keV 17 CM-248:500!J..5105keV AM-243:5131-5365keV CM-5/6:5372-5398keV 15 AM-241:5404-5613keV CM-3f4:5646-5878keV 13 CM-242: 5975-6198 keV 11 Ui 9 I-z :::> 7 0 s 5 *:; 3 u <{ PEAK FWHM 0.000 44.134 0.000 0.000 0.000 0.000 0.000 2369 2770 3176 3585 3997 4413 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:21 ELAPSED LIVE TIME(SEC) : 12299.48 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.820 0.820 0.9055 98.525 -2.06E-02 174.000 171.745 2.255 1.5016 99.980 4.26E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.025 1.025 1.0124 100.000 -2.62E-02 0.000 -0.205 0.205 0.4528 86.090 -5.90E-03 0.000 -1.025 1.025 1.0124 79.300 -3.20E-02 0.000 -1.230 1.230 1.1090 91.000 -3.35E-02 6550 6988 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B218.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W218.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.45E-02 1.58E-01 4.12E-02 9.52E-01 2.09E-01 6.72E-02 1.71E-01 2.56E-01 O.OOE+OO 5.62E-02 1.70E-01 4.67E-02 5.89E-02 1.33E-01 2.35E-02 6.87E-02 2.08E-01 5.71E-02 6.09E-02 1.91E-01 5.45E-02 1.96-sigma en! Unc pCi/G 5.43E-02 6.44E-01 1.71E-01 5.60E-02 5.87E-02 6.85E-02 6.07E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235052 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 219 DETECTOR S/N : 87907 AVERAGE %EFFICIENCY : 25.4729 AVERAGE %EFF ERROR : 0.4938 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 96.3 +/-7.050 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5702E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.49 AM-243 5269.50 5251.22 CM-242 6102.00 6086.58 CM-3/4 5795.02 5715.29 CM-5/6 5386.00 5378.63 CM-247 4946.00 4881.19 CM-248 5078.60 5092.08 17 CM-247* 4n5-4987 keV -CM-248:5009-510SkeV AM-243:5131*5366 keV 15 1-CM-5/6: 5372*5398 keV AM-241: 5404-5613 keV 13 CM.J/4:564S-5878keV 1-CM-242: 5975-6198 keV 11 f-Ui 9 I-z => 7 0 5 f-3 u <1: I I I I PEAK FWHM 0.000 64.123 0.000 4.952 4.952 0.000 4.952 I I 23 88 2787 3189 3595 4006 4420 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 12298.88 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.025 1.025 1.0124 98.525 -1.84E-02 240.000 238.565 1.435 1.1979 99.980 4.21E+OO 0.000 -0.205 0.205 0.4527 100.000 -1.24E-02 1.000 -0.230 1.230 1.1090 100.000 -4.18E-03 1.000 1.000 0.000 0.0000 86.090 2.05E-02 0.000 -1.025 1.025 1.0124 79.300 -2.28E-02 1.000 -0.230 1.230 1.1090 91.000 -4.45E-03 I I I I I I I I 4339 p26' ! >88 6119 6554 6993 7437 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B219.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W219.CNF;132 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.94E-02 1.19E-01 3.28E-02 8.07E-01 1.29E-01 3.81E-02 1.24E-01 2.81E-01 4.96E-02 5.40E-02 1.27E-01 3.64E-02 5.74E-02 6.14E-02 O.OOE+OO 4.89E-02 1.48E-01 4.06E-02 5.76E-02 1.36E-01 3.88E-02 1.96-sigma cnt Unc pCi/G 3.93E-02 5.37E-01 1.24E-01 5.40E-02 5.74E-02 4.88E-02 5.75E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235053 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 220 DETECTOR SIN : 87908 AVERAGE %EFFICIENCY : 24.0361 AVERAGE %EFF ERROR : 0.4668 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 57.4 +/-9.147 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 2.7234E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.50 AM-243 5269.50 5283.44 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.63 CM-5/6 5386.00 5372.75 CM-247 4946.00 4881.21 CM-248 5078.60 5040.10 17 CM-247* 4775-4987 keV -CM-248: 5009-5105 keV AM-243: 5131-5366 keV 15 1-CM-5/6: 5372-5398 keV AM-241: 5404-5613 keV 13 CM-3/4: 5646-5878 keV 1-CM-242: 597&-6198 keV 11 f-Ci) 9 I-f-z :::::> 7 f-0 8 5 f-.?;> *:;: 3 t5 <( I I I I I PEAK FWHM 0.000 30.283 0.000 0.000 0.000 0.000 4.978 I I 23 77 2777 3181 3588 3998 4412 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:27 ELAPSED LIVE TIME(SEC) : 12300.10 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.410 0.410 0.6403 98.525 -1.33E-02 136.000 134.155 1.845 1.3583 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.025 1.025 1.0124 100.000 -3.37E-02 1.000 1.000 0.000 0.0000 86.090 3.70E-02 0.000 -0.410 0.410 0.6403 79.300 -1.65E-02 1.000 1.000 0.000 0.0000 91.000 3.50E-02 I II 11 I I' I I I 525' H76 '310 6535 6970 7409 --Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B220.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W220.CNF;142 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.76E-02 1.72E-01 3.74E-02 1.07E+OO 2.52E-01 7.81E-02 2.26E-01 3.37E-01 O.OOE+OO 7.23E-02 2.19E-01 6.01E-02 1.04E-01 1.11E-01 O.OOE+OO 8.39E-02 2.13E-01 4.64E-02 9.82E-02 1.05E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.73E-02 7.32E-01 2.25E-01 7.21E-02 1.04E-01 8.35E-02 9.80E-02 0 ....., Vt 00 0 '° BATCH NUMBER : 1596410 SAMPLE ID : S0405235054 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 221 DETECTOR S/N : 87909 AVERAGE %EFFICIENCY : 25.5264 AVERAGE %EFF ERROR : 0.4948 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 88.5 +/-7.303 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.1985E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.51 AM-243 5269.50 5282.09 CM-242 6102.00 6086.60 CM-3/4 5795.02 5726.98 CM-5/6 5386.00 5375.05 CM-247 4946.00 4930.49 CM-248 5078.60 5056.59 21 CM-247: 4n54987 keV CM-248: 5009-5105 keV 19 AM-243: 5131-5366 keV CM-5!6:5372-5398keV 17 AM-241:5404-5613keV CM-3/4:5646-5878keV CM-242: 5975-6198 keV 15 13 0' 11 z 9 ::> 0 7 5 *:;; t5 3 <( 1 PEAK FWHM 0.000 40.335 0.000 5.006 5.006 5.006 0.000 COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 12307.16 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 0.000 -0.205 0.205 0.4529 98.525 -4.05E-03 221.000 219.769 1.231 1.1094 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.795 0.205 0.4529 100.000 1.59E-02 1.000 1.000 0.000 0.0000 86.090 2.26E-02 1.000 0.795 0.205 0.4529 79.300 1.95E-02 0.000 -0.410 0.410 0.6405 91.000 -8.76E-03 2382 2784 3190 3599 4011 4427 6557 6993 7433 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B221.CNF;465 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W221.CNF;128 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.04E-02 9.16E-02 1.62E-02 8.51E-01 1.36E-01 3.90E-02 1.37E-01 2.05E-01 O.OOE+OO 5.68E-02 9.30E-02 1.64E-02 6.34E-02 6.78E-02 O.OOE+OO 6.95E-02 1.14E-01 2.01E-02 4.46E-02 1.14E-01 2.47E-02 1.96-sigma cnt Unc pCi/G 4.03E-02 5.68E-01 1.37E-01 5.67E-02 6.33E-02 6.94E-02 4.44E-02 Alpha Spectroscopy Software Version 3.5.3 effedivedate:02-Mar-2015 BATCH NUMBER : 1596410 SAMPLE ID : S0405235055 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 222 DETECTOR S/N : 87910 AVERAGE %EFFICIENCY : 25.0479 AVERAGE %EFF ERROR : 0.4857 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 81.7 +/-7.617 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 3.8773E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 AM-243 5269.50 CM-242 6102.00 CM-3/4 5795.02 CM-5/6 5386.00 CM-247 4946.00 CM-248 5078.60 15 CM-247: 4775-4987 keV CM-248:5009-5105keV AM-243: 5131-5366 keV 13 CM-5!6: 5372-5398 keV AM-241: 5404-5613 keV CM-314: 5646-5878 keV 11 CM-242: 5975-0198 keV 9 (ii I-7 z 0 5 f2. 3 *:;; t5 <( 2379 2779 3182 Energy (keV) 5500.89 5246.25 6086.59 5761.62 5385.09 4860.25 5085.87 PEAK FWHM 4.973 59.992 0.000 0.000 0.000 179.044 0.000 COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 12308.89 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.795 0.205 0.4529 98.525 1.70E-02 200.000 199.179 0.821 0.9059 99.980 4.19E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.615 0.615 0.7845 100.000 -1.34E-02 0.000 . 0.000 0.000 0.0000 86.090 O.OOE+OO 6.000 4.974 1.026 1.0128 79.300 1.32E-01 5.000 4.179 0.821 0.9059 91.000 9.66E-02 6546 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B222.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W222.CNF;125 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.06E-02 9.91E-02 1.75E-02 8.71E-01 1.32E-01 3.44E-02 1.48E-01 2.22E-01 O.OOE+OO 4.61E-02 1.27E-01 3.07E-02 4.90E-02 7.33E-02 O.OOE+OO 1.41E-01 1.77E-01 4.85E-02 1.14E-01 1.45E-01 3.78E-02 1.96-sigma cnt Unc pCi/G 6.05E-02 5.85E-01 1.48E-01 4.60E-02 4.89E-02 1.40E-01 1.13E-01 BATCH NUMBER : 1596410 SAMPLE ID : S0405235056 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 223 DETECTOR S/N : 87911 AVERAGE %EFFICIENCY : 25.6333 AVERAGE %EFF ERROR : 0.4968 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 90.1 +/-7.220 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.2737E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5425.41 AM-243 5269.50 5279.44 CM-242 6102.00 6086.59 CM-3/4 5795.02 5691.16 CM-5/6 5386.00 5372.43 CM-247 4946.00 4921.77 CM-248 5078.60 5071.53 CM-247: 4775-4987 keV 25 CM-24B:5009-5105keV AM-243:5131-5366keV CM-S/6:5372-539BkeV 22 AM-241: 5404-5613 keV CM-3/4:5646-5a78keV 19 CM-242: 5975-6198 keV 16 'iii 13 1--z :::i 10 0 f2.. 7 .?;-*:;; 4 u <( PEAK FWHM 4.964 35.990 0.000 4.964 0.000 19.857 4.964 2377 2776 3178 3584 3994 4408 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:35 ELAPSED LIVE TIME(SEC) : 12304.18 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.641 1.641 1.2808 98.525 -1.22E-02 225.000 224.590 0.410 0.6404 99.980 4.20E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 1.000 0.000 0.0000 100.000 1.93E-02 1.000 0.795 0.205 0.4528 86.090 1.73E-02 2.000 1.795 0.205 0.4528 79.300 4.23E-02 4.000 3.385 0.615 0.7844 91.000 6.95E-02 6529 6965 7403 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM , BKG FILE : B223.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W223.CNF;114 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.75E-02 1.45E-01 4.39E-02 8.26E-01 9.93E-02 2.16E-02 1.32E-01 1.97E-01 O.OOE+OO 5.41E-02 5.78E-02 O.OOE+OO 6.15E-02 1.01E-01 1.78E-02 8.14E-02 1.09E-01 1.93E-02 9.21E-02 1.20E-01 2.91E-02 1.96-sigma en! Unc pCi/G 5.74E-02 5.51E-01 1.31E-01 5.40E-02 6.14E-02 8.11E-02 9.15E-02 Alpha SpecUtlscopy Software Version 3.5.3 effectlvedate:02-Mar*2015 BATCH NUMBER : 1596410 SAMPLE ID : S0405235057 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 224 DETECTOR S/N : 87912 AVERAGE %EFFICIENCY : 25.7363 AVERAGE %EFF ERROR : 0.4987 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 97.5 +/-6.971 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.6273E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5490.58 AM-243 5269.50 5283.71 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5385.09 CM-247 4946.00 4893.98 CM-248 5078.60 5025.25 CM-247: 4n5-4987 keV 25 CM-24S:5009-5105keV AM-243: 5131-5366 keV CM-515: 5372-5398 keV 22 AM-241: 5404-5613 keV CM-3/4:5646-5878keV 19 CM-242:597S-6198keV 16 en 13 I-z ::J 10 0 £ 7 4 u <i:: PEAK FWHM 44.280 40.077 0.000 0.000 0.000 132.839 4.920 2399 2795 3195 3599 4007 4420 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:37 ELAPSED LIVE TIME(SEC) : 12305.60 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.385 0.615 0.7844 98.525 2.46E-02 245.000 244.180 0.820 0.9057 99.980 4.27E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.846 1.846 1.3586 100.000 -3.33E-02 0.000 0.000 0.000 0.0000 86.090 O.OOE+OO 2.000 0.564 1.436 1.1982 79.300 1.25E-02 1.000 0.590 0.410 0.6405 91.000 1.13E-02 6545 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B224.CNF;469 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W224.CNF;150 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCUG 6.21E-02 1.04E-01 2.52E-02 8.11E-01 1.10E-01 2.86E-02 1.23E-01 1.85E-01 O.OOE+OO 4.22E-02 1.43E-01 4.43E-02 4.08E-02 6.10E-02 O.OOE+OO 7.91E-02 1.62E-01 4.77E-02 5.50E-02 1.02E-01 2.22E-02 1.96-sigma en! Une pCi/G 6.20E-02 5.38E-01 1.23E-01 4.22E-02 4.07E-02 7.90E-02 5.50E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235058 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 225 DETECTOR S/N : 87913 AVERAGE %EFFICIENCY : 25.9298 AVERAGE %EFF ERROR : 0.5025 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 90.3 +/-7.184 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.2856E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5404.04 AM-243 5269.50 5250.41 CM-242 6102.00 6086.58 CM-3/4 5795.02 5761.61 CM-5/6 5386.00 5385.09 CM-247 4946.00 4881.19 CM-248 5078.60 5074.76 21 CM-247: 4n5-4987 keV CM-248: 5009-5105 keV 19 AM-243: 5131*5366 keV CM-516:5372*5398keV 17 AM-241:5404--5613keV CM-3/4: 5646-SB78 keV CM-242:5975-6198keV 15 13 (ii 11 1--z 9 :J 0 7 s .?;-5 *:;; ti 3 <I'. PEAK FWHM 0.000 54.094 0.000 0.000 0.000 0.000 0.000 2388 2787 3190 3597 4008 4423 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:40 ELAPSED LIVE TIME(SEC) : 12312.47 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.847 1.847 1.3590 98.525 -1.58E-02 229.000 227.974 1.026 1.0129 99.980 4.17E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.821 0.821 0.9060 100.000 -1.55E-02 0.000 -0.616 0.616 0.7846 86.090 -1.31E-02 0.000 -0.821 0.821 0.9060 79.300 -1.89E-02 3.000 2.179 0.821 0.9060 91.000 4.38E-02 6559 6998 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B225.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W225.CNF;124 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.68E-02 1.47E-01 4.57E-02 8.17E-01 1.22E-01 3.35E-02 1.29E-01 1.93E-01 O.OOE+OO 4.08E-02 1.18E-01 3.09E-02 4.52E-02 1.24E-01 3.01E-02 4.99E-02 1.45E-01 3.78E-02 8.11E-02 1.26E-01 3.29E-02 1.96-sigma cnt Unc pCi/G 5.67E-02 5.45E-01 1.29E-01 4.07E-02 4.51E-02 4.98E-02 8.09E-02 BATCH NUMBER : 1596410 SAMPLE ID : S0405235059 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 226 DETECTOR S/N : 87914 AVERAGE %EFFICIENCY : 26.8347 AVERAGE %EFF ERROR : 0.5195 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 55.1 +/-8.836 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 2.6117E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5473.79 AM-243 5269.50 5279.57 CM-242 6102.00 6086.59 CM-3/4 5795.02 5741.45 CM-5/6 5386.00 5399.11 CM-247 4946.00 4881.20 CM-248 5078.60 5096.25 CM-247:4775-49B7keV 15 CM-248:5009-5105keV AM-243: 5131*5366 keV CM-516: 5372-5398 keV 13 AM-241: 5404-5613 keV CM-3/4: 5646-5878 keV CM-242: 5975-6198 keV 11 Ci) 9 1--z 7 :::i 0 5 "> 3 u <l'. PEAK FWHM 4.984 35.716 0.000 64.788 0.000 0.000 0.000 2372 2772 3177 3585 3997 4413 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:43 ELAPSED LIVE TIME(SEC) : 12311.39 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 1.000 0.795 0.205 0.4530 98.525 2.39E-02 145.000 143.769 1.231 1.1096 99.980 4.25E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 3.000 2.179 0.821 0.9060 100.000 6.63E-02 1.000 1.000 0.000 0.0000 86.090 3.43E-02 0.000 -0.821 0.821 0.9060 79.300 -3.06E-02 2.000 2.000 0.000 0.0000 91.000 6.49E-02 6548 6986 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B226.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W226.CNF;122 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.51E-02 1.39E-01 2.46E-02 1.03E+OO 2.07E-01 5.92E-02 1.97E-01 2.94E-01 O.OOE+OO 1.23E-01 1.91E-01 4.98E-02 9.63E-02 1.03E-01 O.OOE+OO 8.06E-02 2.34E-01 6.10E-02 1.12E-01 9.74E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 8.50E-02 7.01E-01 1.96E-01 1.22E-01 9.61E-02 8.03E-02 1.11E-01 BATCH NUMBER : 1596410 SAMPLE ID : S0405235060 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 227 DETECTOR S/N : 87915 AVERAGE %EFFICIENCY : 26.3665 AVERAGE %EFF ERROR : 0.5107 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 96.3 +/-6.940 % TRACER . ID 1752-C NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.5666E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5511.69 AM-243 5269.50 5273.36 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5376.08 CM-247 4946.00 4879.86 CM-248 5078.60 5056.03 CM 247* 4775-4987 keV 23 CM-248: keV AM-243: 5131-5366 keV 21 CM-516:5372*5398keV AM-241: 5404-5613 keV 19 CM-3/4:5646-5878keV CM-242: 5975-0198 keV 17 15 0' 13 z 11 ::i 9 0 7 5 u 3 <I: -I I I PEAK FWHM 4.922 35.942 0.000 0.000 0.000 177.209 4.922 I I 23 75 2771 3171 3576 3984 4397 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:45 ELAPSED LIVE TIME(SEC) : 12310.57 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.231 1.231 1.1095 98.525 -3.94E-03 248.000 246.974 1.026 1.0129 99.980 4.15E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.616 0.616 0.7846 100.000 -1.06E-02 2.000 1.590 0.410 0.6406 86.090 3.10E-02 2.000 0.564 1.436 1.1984 79.300 1.19E-02 1.000 0.179 0.821 0.9059 91.000 3.31E-03 II I I I II I I I I 4114 5 61 509 6525 6963 7405 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B227.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W227.CNF;120 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.07E-02 1.20E-01 3.42E-02 7.84E-01 1.12E-01 3.07E-02 1.12E-01 1.67E-01 O.OOE+OO 3.67E-02 1.01E-01 2.45E-02 6.78E-02 1.04E-01 2.26E-02 7.59E-02 1.55E-01 4.58E-02 5.39E-02 1.16E-01 3.02E-02 1.96-sigr'na cnt Unc pCi/G 5.07E-02 5.20E-01 1.11E-01 3.67E-02 6.76E-02 7.58E-02 5.38E-02 BATCH NUMBER : 1596410 SAMPLE ID : S1203621745 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 228 DETECTOR S/N : 87916 AVERAGE %EFFICIENCY : 25.5769 AVERAGE %EFF ERROR : 0.4958 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 99.7 +/-6.923 % TRACER ID NUCLIDE NOMINAL RESULTS 1752-C . AM-243 4.7439E+OO dpm 4.7302E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5464.68 AM-243 5269.50 5270.24 CM-242 6102.00 6086.59 CM-3/4 5795.02 5761.62 CM-5/6 5386.00 5385.09 CM-247 4946.00 4841.49 CM-248 5078.60 5056.59 CM 247* 4775-4987 keV 25 :.-CM-248: 5009-5105 keV AM-243:5131-5366keV CM-5f6: 5372-5398 keV 22 :-AM-241:5404-5613keV CM-3!4: 5646-5878 keV 19 -CM-242:5975-6198keV 16 en 13 I--z ::::> 10 0 -s 7 c -*::; 4 u -<( n I PEAK FWHM 4.970 47.075 0.000 0.000 0.000 74.547 0.000 I II I I COUNT DATE : 22-Sep-2016 09:56:47 ELAPSED LIVE TIME(SEC) : 12310.50 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.384 0.616 0.7846 98.525 6.52E-03 249.000 248.179 0.821 0.9059 99.980 4.15E+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -0.205 0.205 0.4530 86.090 -3.98E-03 2.000 0.153 1.847 1.3589 79.300 3.23E-03 0.000 -0.410 0.410 0.6406 91.000 -7.54E-03 II II I ni I I I I I 23 69 2768 3171 3578 3989 4403 4B21 >242 5 67 3091 6528 6964 7404 -Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B228.CNF;455 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W228.CNF;117 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.90E-02 9.90E-02 2.40E-02 7.82E-01 1.05E-01 2.74E-02 3.39E-02 5.07E-02 O.OOE+OO 3.35E-02 5.02E-02 O.OOE+OO 3.97E-02 9.00E-02 1.59E-02 7.65E-02 1.67E-01 5.17E-02 3.83E-02 9.76E-02 2.12E-02 1.96-sigma cnt Unc pCi/G 4.90E-02 5.18E-01 3.38E-02 3.35E-02 3.96E-02 7.64E-02 3.82E-02 BATCH NUMBER : 1596410 SAMPLE ID : S1203621746 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.511 G -+/-0.196 % CHAMBER : 238 DETECTOR S/N : 87926 AVERAGE %EFFICIENCY : 26.1325 AVERAGE %EFF ERROR : 0.5062 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 93.4 +/-8.939 % TRACER 1752-C ID NUCLIDE NOMINAL RESULTS AM-243 4.7442E+OO dpm 4.4299E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AM-241 5480.15 5508.48 AM-243 5269.50 5269.14 CM-242 6102.00 6086.57 CM-3/4 5795.02 5761.60 CM-5/6 5386.00 5385.09 CM-247 4946.00 4829.67 CM-248 5078.60 5030.40 19 CM-247: 4775-4987 k&V CM-246: 5009--5105 keV 17 AM-243: 5131-5366 keV CM-516: 5372-5398 keV AM-241: 5404-5613 keV 15 CM-314: 564S.5878 keV CM-242: 5975-6198 keV 13 'iii 11 I-9 z :J 0 7 s 5 .?;> *:;; 3 ti <( PEAK FWHM 0.000 41.072 0.000 0.000 0.000 4.956 4.956 2386 2784 3187 3594 4005 4421 Energy (keV) COUNT DATE : 22-Sep-2016 16:14:46 ELAPSED LIVE TIME(SEC) : 7200.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.120 0.120 0.3464 98.525 -3.67E-03 139.000 138.880 0.120 0.3464 99.980 4.18E+OO 0.000 -0.120 0.120 0.3464 100.000 -1.28E-02 0.000 -0.240 0.240 0.4899 100.000 -7.45E-03 0.000 -0.120 0.120 0.3464 86.090 -4.20E-03 1.000 0.880 0.120 0.3464 79.300 3.34E-02 1.000 0.880 0.120 0.3464 91.000 2.91E-02 m = 6561 7001 7446 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B238.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W238.CNF;125 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.11E-02 1.29E-01 1.85E-02 1.02E+OO 1.27E-01 1.82E-02 2.13E-01 4.49E-01 6.44E-02 6.24E-02 1.46E-01 2.65E-02 6.98E-02 1.47E-01 2.11E-02 1.06E-01 1.60E-01 2.29E-02 9.25E-02 1.39E-01 2.00E-02 1.96-sigma cnt Unc pCi/G 6.08E-02 6.98E-01 2.12E-01 6.22E-02 6.95E-02 1.06E-01 9.24E-02 BATCH NUMBER : 1596410 SAMPLE ID : S1203621747 AM GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 230 DETECTOR S/N : 87918 AVERAGE %EFFICIENCY : 25.1072 AVERAGE %EFF ERROR : 0.4868 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 101 +/-6.732 % TRACER ID 1752-C NUCLIDE AM-243 NOMINAL 4.7439E+OO dpm RESULTS 4.8057E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM AM-241 5480.15 5486.31 45.098 AM-243 5269.50 5271.48 34.336 CM-242 6102.00 5975.15 0.000 CM-3/4 5795.02 5801.52 31.328 CM-5/6 5386.00 5386.59 0.000 CM-247 4946.00 4877.52 4.979 CM-248 5078.60 5064.01 59.751 CM-247: 47754987 keV 37 CM-248: 5009-5105 keV AM-243: 5131-5366 keV CM-5f6: 5372-5398 keV 33 AM-241:5404-5613keV CM-314: 5646-5878 keV 29 CM*242:5975-0198keV 25 Ci) 21 I-z 17 ::i 0 13 9 *;;: n <l'. 5 2377 2777 3181 3589 4001 4416 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:52 ELAPSED LIVE TIME(SEC) : 13214.12 LCS ID 0533-CC 1216-G NUCLIDE AM-241 CM-3/4 NOMINAL (pCi/G) 3.8242E+OO 5.0562E+OO % RECOVERY 105.132 106.193 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 255.000 253.679 1.321 1.1495 98.525 4.02E+OO 267.000 265.679 1.321 1.1495 99.980 4.15E+OO 1.000 1.000 0.000 0.0000 100.000 1.58E-02 344.000 343.780 0.220 0.4693 100.000 5.37E+OO 8.000 8.000 0.000 0.0000 86.090 1.45E-01 1.000 -0.321 1.321 1.1495 79.300 -6.33E-03 3.000 1.899 1.101 1.0494 91.000 3.26E-02 6550 6988 7429 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : AM BKG FILE : B230.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W230.CNF;114 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.43E-01 1.14E-01 3.31E-02 7.59E-01 1.12E-01 3.26E-02 4.43E-02 4.73E-02 O.OOE+OO 9.31E-01 7.35E-02 1.33E-02 1.09E-01 5.44E-02 0.00E+OO 5.91E-02 1.41E-01 4.11E-02 6.98E-02 1.17E-01 3.27E-02 1.96-sigma cnt Unc pCi/G 4.97E-01 5.01E-01 4.43E-02 5.69E-01 1.07E-01 5.90E-02 6.97E-02 Effective 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 04-0ct-2016 GL-CHL-RAD-013 Rev 1 Page 1 of 1 Batch# Product: __ _____ _ Date: Criteria: 'yes No Comments Samole Solids are less than or eaual to 100 m11 for GAB. Ni' Samples have been blank corrected (If required). (\()f\ Blank correction reoorted Included (if reaulredl. If activity less than 10x MDA/MDC, error Is less "' than or equal to 150% of sample activity. !-.; If greater than 10"' MDA/ MDC, error Is 40% or less. If hAlnw the MOA/ MDC. error I<: nr..3v Instrument source check Is within limits. " !'--. Instrument bka check is within lfmltc, " Method RDL/ LLD has been met. ['... If duollcate activities are: "' Less than 5* MDA/ MDC, then RPD Is 100% or less, -.I If greater 5* MDA/ MDC, then RPD 20% or less, If below the MOA/ MDC, the RPO is 0%, Or meets the client's reauired RER acceotance criteria. Tracer vleld Is 15-125%

Carrier vield 25-125%. '-... I'-> (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. " r---fyt r3,.f C3mnlae <('. 50/n nf ln ... ae* .. ctlvltvl ' ' Samele was run within hold time. n IS&tl)t\S Samole was correctlv oreserved if reauired. Mf\ Smears Taken for Radioactive batches. f\/)(\ Method Spike and LCS are within 75-125% ......... ....... lfor meet<: thn client's cnntr"ct ac.,entance criteria'. No blank spaces on data forms. ......, All line outs Initialed and dated. N Nn nrrnre ... Aux data Is correct. NY"'\ Client Sneclal reouirements naae has been checked. -r-. Raw Data and I or snectrum are Included and nronerlv statused. MS, LCS, and Duollcate RPD/RER values uploaded to UMS and.'-............ .. ..,. .. IMlt -(if NA l .\q .. ln*n ** '-.._ t\-'tf> \I.)' 'I Batch Data Excentlon Reports (DERl completed If aoollcable. ............... J_)6f\Jt. I ld'-1 \ \.\ S Batch Data Exception Reports (DER) second reviewed. 'I'---> I SG \.\l'--\..S Dlsnnsltion verified to be comnleted. Alln .. nt Cnrrertlon <0omnl,,.ted if r<'n11lr""* r/JA Review sample historical results If available ......... N (If REMP, results above MDC have been verified bv historical results, recount or re-analvsls. \ Primary Review Performed By: . 10/04/16 rlloLJ G Page 851 of 5809 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 04-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, U-02-RC Solid .. *-Batch ID: Sample Numbers: 1596396 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, and 1203621710 were received and analyzed outside of the holding time. Originator's Name: Data Validator/Group Leader: Jessica Downey 04-0CT-16 Jessica Davis 04-0CT-16 Page 1 Page 852 of 5809 DER Report No.: 1564145 Revision No.: Type: Process Client Code: MJWC Uranium Que Sheet S-f4.l 0 07-SEP-16 *-----*-----------------*-----Batch #: 1596396 Analyst: MXS2 Tracer Code: > S(pLf-I First Client Due Date:04-0CT-16 Expiration Date: lf<Z 3-1 (ti Expiration Date: 1-l'l--If Internal Due Date:30-SEP-16 Tracer LCS Isotope: U-238 LCS Code: 1 <4DO--& Vol: ().) Spike Isotope: U-238 Spike Code:_______ Expiration Date: -Vol: __. Initials:J"'-S Pipet ID: Balance ID: f C;, ( r:::n Prep Date: <<4--Z..kll,P Sample ID Client Description ----* 405235021-1 405235022-1 405235023-1 405235024-1 405235025-1 405235026-1 405235027-1 405235028-1 405235029-1 405235030-1 405235031-1 405235032-1 405235033-1 405235034-1 405235035-1 405235036-1 405235037-1 405235038-1 405235039-1 405235040-1 1203621709-1 1203621710-1 1203621711-1 4.2B.R.2.3 4.2B.R.l.3 4.2B.R.11.2 4.2B.R.2.2 4.2B.R.l.2 4.2C.R.l.3 4.2C.R.1.4 4.3.ARl.3 4.3.B.R.l.3 4_.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.1.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.l.3 4.4C.R.1.4 4.4D.R.1.3 rvm for batch 1596396 4.2B.R.2.3(405235021DUP) LCS for batch 1596396 Type SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAJ\.1PLE SAJ\.1PLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP LCS Hazard Code Min CRDL l pCi/g lpCilg 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCilg 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g l pCi/g 1 pCi/g l pCi/g 1 pCi/g 1 pCi/g 1 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Client l'YlJWCOOl l\1JWC001 l'<UWCOOl MJWCOOl MJWCOOl l\>f.JWCOOl MJWCOOl MJWCOOl l.VIJWCOOl MJWCOOl MJWCOOl l'<f.JWCOOl MJWCOOl MJWCOOl MJWCOOl l'<UWCOOl l\UWCOOl MJWCOOl l'<UWCOOl l'<UWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Analyzed Sequentially with Pu Analyzed Sequentially with: Pu-236 ID: Pu: I 5"? Vol.: =-=== Am: j Collection Date 08-DEC-15 08-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 23-NOV-15 23-NOV-15 23-NOV-15 26-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-lS 08-DEC-15 Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 _____ _ wet6> Label Aliquot # u Det# Choose SOP used: GL-RAD-A-011 Solid Sample Dissolution by: LEACH Circle One GEL Laboratories LLC, Radiochemistry Division Page l of 1 Uranium Que Sheet Batch#: 1596396 Analyst: MXS2 Tracer Isotope: U-232,:a::TIOracer __ LCS Isotope: U-238 LCS Code: Spike Isotope: U-238 Spike First Client Due Date:04-0CT-16 Expiration Date: 7-I 8-l 7 Expiration Date: --Expiration Date: \-ikJJ 07-SEP-16 -----Internal Due Date:30-SEP-16 Vol:-2:...L Analyzed Sequentially with Pu Analyzed Sequentially with: v 01:____::::__ -Vol: __ Pu-236 ID: --==---Pu: --:;* Vol.:____ Am: ___ _ Prep Date: CJ*..-zJ .--1(.p Initials: JA.51) PipetID: Balance ID: l&.\ \) 7& Qiiz_. Hazard Sample ID Client Description Type Code MinCRDL 405235021-1 4.2B.R.2.3 SAMPLE 1 pCi/g 405235022-1 4.2B.R.1.3 SAMPLE 1 pCi/g 405235023-1 4.2B.R.ll.2 SAMPLE 1 pCilg 405235024-1 4.2B.R.2.2 SAMPLE 1 pCilg 405235025-1 4.2B.R.1.2 SAMPLE 1 pCi/g 405235026-1 4.2C.R.1.3 SAMPLE 1 pCilg 405235027-1 4.2C.R.1.4 SAMPLE 1 pCilg 405235028-1 4.3.ARl.3 SAMPLE 1 pCi/g 405235029-1 4.3.B.R.1.3 SAMPLE 1 pCilg 405235030-1 43A.R.2.3 SAJ\IPLE 1 pCi/g 405235031-1 43.BR19.2 SAJ\IPLE 1 pCi/g 405235032-1 43B.R3.3 SAi'\IPLE 1 pCi/g 405235033-1 4.3B.R.3.4 SAMPLE 1 pCilg 405235034-1 4.3.B.R.1.4 SAMPLE lpCi/g 405235035-1 4.3B.R.2.3 SAl\fPLE 1 pCi/g 405235036-1 4.3B.R.2.4 SAMPLE 1 pCi/g 405235037-1 4.4C.R.2.4 SAMPLE 1 pCi/g 405235038-1 4.4C.R.1.3 SAMPLE l pCi/g 405235039-1 4.4C.R.1.4 SAJ\IPLE 1 pCi/g 405235040-1 4.4D.R.1.3 SAJ\.'IPLE 1 pCi/g 1203621709-1 MB for batch 1596396 J\.'IB 1 pCi/g 1203621710-1 4.2B.R.2.3(405235021DUP) DUP 1 pCi/g 1203621711-1 LCS for batch 1596396 LCS 1 pCi/g Choose SOP used: GL-RAD-A-011 Solid Sample Dissolution by: GEL Laboratories LLC, Radiochemistry Division Collection Matrix Client Date SOIL l\UWCOOl 08-DEC-15 SOIL MJWCOOl 08-DEC-15 SOIL MJWCOOl 02-DEC-15 SOIL MJWCOOl 08-DEC-15 SOIL MJWCOOl 08-DEC-15 SOIL l\JJWCOOl 08-DEC-15 SOIL MJWCOOl 08-DEC-15 SOIL MJWCOOl 23-NOV-15 SOIL MJWCOOl 23-NOV-15 SOIL MJWCOOl 23-NOV-15 SOIL l'vIJWCOOl 26-NOV-15 SOIL MJWCOOl 23-NOV-15 SOIL MJWCOOl 23-NOV-15 SOIL 1\-fJWCOOl 23-NOV-15 SOIL l'vIJWCOOl 23-NOV-15 SOIL l\fJWCOOl 23-NOV-15 SOIL MJWCOOl 30-NOV-15 SOIL MJWCOOl 30-NOV-15 SOIL l\fJWCOOl 30-NOV-15 SOIL l'vUWCOOl 30-NOV-15 SOIL QC ACCOUNT SOIL QC ACCOUNT 08-DEC-15 SOIL QC ACCOUNT LEACH or Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 Label Aliquot # Det# u Page 1 of 1 BATCH NUMBER : 1596396 SAMPLE ID : T0405235021_UU SAMPLE QTY : 0.514 G +/-0.195 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 94.5 +/-8.448 % SECONDARY QTY : 0.511 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 8.5280E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 159 DETECTOR S/N : 76225 AVERAGE %EFFICIENCY : 25.5501 AVERAGE %EFF ERROR : 0.4952 COUNT DATE : 24-Sep-2016 13:20:33 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B159.CNF;1074 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W159.CNF;278 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4487.77 4494.71 4.6539 dpm 5141.84 5313.71 PEAKNET1 521.37 -0.44 PEAK NET2 1.76 274.56 RECOVERY YIELD CORR. 76.440 N/A 95.292 1.0081 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5141.84 4.879 1.000 U-3/4 4763.02 4765.21 55.291 46.000 U-235 4391.00 4487.77 31.072 2.000 U-238 4184.73 4190.18 95.947 42.000 U*238;3974-4284keV 46 U-235:431Cl-4581keV U-3/4:4592-4865keV U-232:5000-5398keV 41 36 31 '(ii 26 I-z 21 :J 0 16 (:2. 11 u 6 <( 1 2394 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.440 1.440 1.2000 100.000 -8.34E-03 44.800 1.200 1.0954 100.000 6.65E-01 1.760 0.240 0.4899 99.700 2.62E-02 40.800 1.200 1.0954 100.000 6.06E-01 5237 5661 6090 6523 6960 7403 1.96-sigma TPU pCi/G 5.77E-02 2.30E-01 5.17E-02 2.18E-01 NOTES: MDA pCi/G 1.40E-01 1.04E-01 7.14E-02 1.04E-01 Le pCi/G 4.17E-02 2.98E-02 1.34E-02 2.98E-02 1.96-sigma cnt Unc pCi/G 5.76E-02 2.00E-01 5.15E-02 1.92E-01

Results are a compilation of S0405235021_UU and T0405235021_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.008 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235021_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 128 DETECTOR S/N : 75549 AVERAGE %EFFICIENCY : 26.0039 AVERAGE %EFF ERROR : 0.5038 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 95.3 +/-6.829 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 4.4348E+OO dpm NUCLIDE LIBRARY PEAK en 1--z :J 0 8 *:;; ti <( ENERGY ENERGY U-232 5302.10 5313.71 U-3/4 4763.02 4775.53 U-235 4391.00 4494.71 U-238 4184.73 4195.37 25 U*238:3974-4284keV U-235: 431o-4581 keV 23 lJ.3/4:4592-4865keV U-232:5000-539B't<<!JV 21 19 17 15 13 11 9 7 5 3 2400 2797 3198 3603 Energy (keV) PEAK FWHM 56.625 81.011 39.477 37.010 COUNT DATE : 24-Sep-2016 13:19:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA Stoev pCi/G 276.000 274.560 1.440 1.2000 100.000 4.08E+OO 46.000 44.800 1.200 1.0954 100.000 6.60E-01 2.000 1.760 0.240 0.4899 99.700 2.60E-02 42.000 40.800 1.200 1.0954 100.000 6.01E-01 5688 6117 6550 6987 7429 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B128.CNF;1171 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W128.CNF;324 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.47E-01 1.10E-01 3.27E-02 2.19E-01 1.03E-01 2.96E-02 5.13E-02 7.09E-02 1.33E-02 2.08E-01 1.03E-01 2.96E-02 1.96-sigma en! Une pCi/G 4.85E-01 1.99E-01 5.11E-02 1.90E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235022 UU SAMPLE QTY : 0.505 G -+/-0.198 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 78.4 +/-8.667 % SECONDARY QTY : 0.505 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0534E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 160 DETECTOR S/N : 79994 AVERAGE %EFFICIENCY : 25.3966 AVERAGE %EFF ERROR : 0.4923 COUNT DATE : 24-Sep-2016 13:20:35 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B160.CNF;1076 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W160.CNF;308 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4488.09

4431.09 4.6539 dpm 5322.84 5308.78 PEAK NET 1 640.14 0.04 PEAK NET2 3.28 227.76 RECOVERY YIELD CORR. 94.421 N/A 79.068 1.0083 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5322.84 4.950 1.000 U-3/4 4763.02 4762.31 54.445 44.000 U-235 4391.00 4488.09 46.270 4.000 U-238 4184.73 4201.50 16.086 52.000 U-238:3974-4284keV U-235:431D-4581 keV 55 U-J/4:4592-486SkeV U-232:S000-5398keV 49 43 37 UJ 31 I-z 25 => 0 s 19 13 *:;; u 7 <l: 1 2382 2780 3182 3588 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.040 0.960 0.9798 100.000 6.25E-04 44.000 0.000 0.0000 100.000 8.02E-01 3.280 0.720 0.8485 99.700 6.00E-02 52.000 0.000 0.0000 100.000 9.48E-01 5674 6103 6535 6972 7412 1.96-sigma TPU pCi/G 4.64E-02 2.78E-01 8.26E-02 3.08E-01 NOTES: MDA pCi/G 1.03E-01 5.47E-02 1.12E-01 5.47E-02 Le pCi/G 2.BOE-02 O.OOE+OO 2.84E-02 0.00E+OO 1.96-sigma cnt Unc pCi/G 4.63E-02 2.40E-01 8.20E-02 2.60E-01
Results are a compilation of S0405235022_UU and T0405235022_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235022 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 157 DETECTOR S/N : 75555 AVERAGE %EFFICIENCY : 26.0007 AVERAGE %EFF ERROR : 0.5038 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 79.1 +/-7.349 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.6798E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5308.78 U-3/4 4763.02 4761.59 U-235 4391.00 4431.09 U-238 4184.73 4195.68 23 U-238:3974-4Z84keV U-235:431Q-4581keV 21 U-3/4:4592-4865keV U-232:5000.5398keV 19 17 15 U) 13 I-11 z :J 9 0 !:2. 7 .2:-5 *s: 3 2383 2781 3182 3588 Energy (keV) PEAK FWHM 33.099 32.584 188.077 44.132 COUNT DATE : 28-Sep-2016 17:55:25 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 228.000 227.760 0.240 0.4899 100.000 4.15E+OO 44.000 44.000 0.000 0.0000 100.000 7.95E-01 4.000 3.280 0.720 0.8485 99.700 5.95E-02 52.000 52.000 0.000 0.0000 100.000 9.40E-01 5672 6101 6533 6969 7408 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B157.CNF;1100 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W157.CNF;284 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.22E-01 8.74E-02 1.64E-02 2.66E-01 5.42E-02 O.OOE+OO 8.18E-02 1.11E-01 2.82E-02 2.94E-01 5.42E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.41E-01 2.38E-01 8.13E-02 2.58E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235023 UU SAMPLE QTY : 0.504 G -+/-0.198 % SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 87.0 +/-8.384 % SECONDARY QTY : 0.509 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0315E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 001 DETECTOR S/N : 79451 AVERAGE %EFFICIENCY : 29.7966 AVERAGE %EFF ERROR : 0.5755 COUNT DATE : 25-Sep-2016 15:53:59 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B001.CNF;1860 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W001.CNF;565 CAL DATE : 27-Aug-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4501.70 4444.99 TRACER2 1564-1 U-232 4.6547 dpm 5177.29 5309.60 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY ENERGY FWHM AREA AREA AREA S!Dev pCi/G U-232 5302.10 5177.29 4.981 1.000 0.040 0.960 0.9798 100.000 5.40E-04 U-3/4 4763.02 4784.42 49.812 57.000 56.040 0.960 0.9798 100.000 9.49E-01 U-235 4391.00 4501.70 30.702 4.000 4.000 0.000 0.0000 99.700 6.80E-02 U-238 4184.73 4209.66 72.725 49.000 48.520 0.480 0.6928 100.000 8.22E-01 U-238:3974-4284keV 81 U-235: 4310-4581 keV U-314:4592"4865keV 73 U-232:5000-5398keV 65 57 en 49 I-41 z ::i 33 0 25 c 17 *:;; u 9 <( 1 2371 2771 3175 3583 5678 6108 6542 6979 7420 Energy (keV) 735.46 4.00 92.461 N/A 0.04 245.60 87.720 1.0085 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.01E-02 8.89E-02 2.42E-02 4.00E-02 3.00E-01 1.12E-01 3.04E-02 2.54E-01 7.58E-02 5.10E-02 O.OOE+OO 7.49E-02 2.73E-01 9.38E-02 2.15E-02 2.35E-01 NOTES: *Results are a compilation of S0405235023_UU and T0405235023_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235023 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 158 DETECTOR S/N : 80007 AVERAGE %EFFICIENCY : 25.2718 AVERAGE %EFF ERROR : 0.4900 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 87.7 +/-7.158 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6547E+OO dpm 4.0831 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5309.60 U-3/4 4763.02 4765.49 U-235 4391.00 4444.99 U-238 4184.73 4188.42 25 U-238:39744284keV lJ.235:4310-4581keV 23 U-3/4:4592-4865keV U-232:5000-5398keV 21 19 17 15 00 13 I-z 11 ::> 0 9 f:2. 7 *:;: 5 ti 3 <t: 1 2386 2784 3186 3591 Energy (keV) PEAK FWHM 50.102 74.360 212.576 82.394 > >> !l!l COUNT DATE : 28-Sep-2016 17:55:27 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 248.000 245.600 2.400 1.5492 100.000 4.16E+OO 57.000 q6.040 0.960 0.9798 100.000 9.41E-01 4.000 4.000 0.000 0.0000 99.700 6.74E-02 49.000 48.520 0.480 0.6928 100.000 8.15E-01 5681 6111 6546 6984 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B158.CNF;1105 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W158.CNF;286 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.01E-01 1.47E-01 4.81E-02 2.86E-01 1.11E-01 3.01E-02 7.49E-02 5.05E-02 O.OOE+OO 2.62E-01 9.30E-02 2.13E-02 1.96-sigma cnt Unc pCi/G 5.25E-01 2.51E-01 7.43E-02 2.33E-01 0 ....., Vi 00 0 IO BATCH NUMBER : 1596396 SAMPLE ID : T0405235024 UU SAMPLE QTY : 0.505 G -+/-0.198 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 002 DETECTOR S/N : 79452 AVERAGE %EFFICIENCY : 27.4069 AVERAGE %EFF ERROR : 0.5303 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B002.CNF;1845 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 68.9 +/-9.046 % SECONDARY QTY : 0.506 G +/-0.198 % COUNT DATE : 25-Sep-2016 15:53:59 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W002.CNF;518 CAL DATE : 27-Aug-2016 TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0286E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U238'3974-4284keV 91 U-235:431Cl-4581 keV U-314:4592-4865keV 81 -U-232:5CJ00.5398keV 71 61 Vi 51 I--z 41 :::> -0 31 8 -21 *:;: -I I ID 1570-E 1564-1 PEAK ENERGY 5198.58 4773.73 4493.91 4199.01 I NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 674.57 -0.96 PEAKNET2 1.00 197.08 RECOVERY YIELD CORR. 11.1230 dpm 4493.91 4443.00 4.6539 dpm 5198.58 5302.91 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA StDev 0.000 0.000 -0.960 0.960 0.9798 100.000 30.025 38.000 37.760 0.240 0.4899 100.000 23.658 1.000 1.000 0.000 0.0000 99.700 58.382 48.000 47.280 0.720 0.8485 100.000 >> :i .:.: ie i ,Jl ..J ** I I I I I I I ACTIVITY pCi/G -1.42E-02 7.95E-01 2.11E-02 9.96E-01 I 1.96-sigma TPU pCi/G 3.30E-02 2.96E-01 5.95E-02 3.41E-01 NOTES: MDA pCi/G 9.75E-02 1.01E-01 6.34E-02 1.29E-01 92.200 N/A 69.488 1.0081 Le pCi/G 2.66E-02 1.89E-02 O.OOE+OO 3.27E-02 1.96-sigma en! Une pCi/G 3.29E-02 2.58E-01 5.94E-02 2.90E-01 *Results are a compilation of S0405235024_UU and T0405235024_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000) 23 58 2760 3166 3576 3! 89 406 48 6 5251 5679 6110 6545 6984 7427 -Energy (keV)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235024 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 131 DETECTOR S/N : 80008 AVERAGE %EFFICIENCY : 25.5970 AVERAGE %EFF ERROR : 0.4961 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 69.5 +/-7.840 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.2339E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5302.91 U-3/4 4763.02 4760.64 U-235 4391.00 4443.00 U-238 4184.73 4196.58 19 U-238: 39744284 keV U-235:4310-4581keV 17 U+314:4592-486SkeV U-232:5000-5398keV 15 13 0' 11 z 9 ::J 0 7 5 *::; 3 ti <{ 2379 2778 3181 3587 Energy (keV) PEAK FWHM 46.559 31.411 4.960 37.404 COUNT DATE : 24-Sep-2016 13:19:46 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 199.000 197.080 1.920 1.3856 100.000 4.15E+OO 38.000 37.760 0.240 0.4899 100.000 7.89E-01 1.000 1.000 0.000 0.0000 99.700 2.10E-02 48.000 47.280 0.720 0.8485 100.000 9.88E-01 6108 6542 6979 7421 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B131.CNF;1162 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W131.CNF;319 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.80E-01 1.70E-01 5.35E-02 2.85E-01 1.00E-01 1.88E-02 5.90E-02 6.29E-02 O.OOE+OO 3.27E-01 1.28E-01 3.25E-02 1.96-sigma cnt Unc pCi/G 5.85E-01 2.56E-01 5.89E-02 2.87E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235025 UU SAMPLE QTY : 0.506 G -+/-0.198 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 71.0 +/-8.988 % SECONDARY QTY : 0.504 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.5428E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 003 DETECTOR S/N : 79453 AVERAGE %EFFICIENCY : 27.6246 AVERAGE %EFF ERROR : 0.5344 COUNT DATE : 25-Sep-2016 15:53:59 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B003.CNF;1843 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W003.CNF;535 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4492.31 4412.05 4.6539 dpm 5072.78 5318.80 PEAK NET 1 630.78 -0.40 PEAK NET 2 0.76 204.04 RECOVERY YIELD CORR. 85.536 N/A 71.546 1.0081 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5072.78 14.863 2.000 U-3/4 4763.02 4774.67 41.122 38.000 U-235 4391.00 4492.31 40.379 1.000 U-238 4184.73 4200.67 24.206 45.000 U*238:3974-4284keV 64 U-235:4310-4581 keV IJ..3/4:4592-4865keV lJ..232:S000-5398keV 57 50 43 0' 36 z 29 :::> 0 s 22 )!-15 *s: u 8 <l'. 1 2377 2775 3177 3582 3 92 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -o.400 2.400 1.5492 100.000 -6.36E-03 36.800 1.200 1.0954 100.000 7.47E-01 0.760 0.240 0.4899 99.700 1.55E-02 43.800 1.200 1.0954 100.000 8.89E-01 5665 6093 6524 6959 7398 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 5.94E-02 1.38E-01 4.51E-02 5.94E-02 2.84E-01 1.42E-01 4.07E-02 2.50E-01 5.82E-02 9.77E-02 1.83E-02 5.81E-02 3.15E-01 1.42E-01 4.07E-02 2.71E-01 NOTES:

Results are a compilation of S0405235025_UU and T0405235025_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235025 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 134 DETECTOR S/N : 76230 AVERAGE %EFFICIENCY : 25.7389 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 71.5 +/-7.707 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.3297E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5318.80 U-3/4 4763.02 4760.74 U-235 4391.00 4412.05 U-238 4184.73 4205.40 U-238: 3974-4284 keV 17 U-235:431o-4581keV U-3/4:4592-4865keV U-232:5000.5398keV 15 13 11 9 z :::> 7 0 5 ;:-*;;: 3 n <t: 2387 2786 3188 Energy (keV) PEAK FWHM 69.443 61.589 4.960 11.532 COUNT DATE : 24-Sep-2016 13:19:49 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 205.000 204.040 0.960 0.9798 100.000 4.14E+OO 38.000 36.800 1.200 1.0954 100.000 7.41E-01 1.000 0.760 0.240 0.4899 99.700 1.54E-02 45.000 43.800 1.200 1.0954 100.000 8.82E-01 5679 6107 6539 6974 7413 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B134.CNF;1151 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W134.CNF;336 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.62E-01 1.34E-01 3.64E-02 2.73E-01 1.41E-01 4.04E-02 5.77E-02 9.69E-02 1.81E-02 3.02E-01 1.41E-01 4.04E-02 1.96-sigma cnt Unc pCi/G 5.72E-01 2.48E-01 5.76E-02 2.69E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235026 UU SAMPLE QTY : 0.502 G -+/-0.199 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 84.4 +/-8.505 % SECONDARY QTY : 0.512 G +/-0.195 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0432E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 005 DETECTOR S/N : 79454 AVERAGE %EFFICIENCY : 28.9835 AVERAGE %EFF ERROR : 0.5602 COUNT DATE : 25-Sep-2016 15:53:59 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B005.CNF;1828 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W005.CNF;575 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4517.94 4448.01 4.6539 dpm 5198.64 5320.94 PEAK NET 1 723.44 -1.92 PEAKNET2 1.76 234.56 RECOVERY YIELD CORR. 93.502 N/A 85.057 1.0081 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.64 0.000 0.000 U-3/4 4763.02 4793.51 58.931 37.000 U-235 4391.00 4517.94 31.064 2.000 U-238 4184.73 4223.88 28.839 30.000 U*238: 3974-4284 keV 73 lJ.235:4310-4581 keV U-J/4: 4592-4865 keV U-232:S000-5398keV 65 57 49 en 41 I-z 33 :J 0 £ 25 1' 17 *;;; 9 1 2382 2785 3191 Energy {keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -1.920 1.920 1.3856 100.000 -2.62E-02 35.560 1.440 1.2000 100.000 6.33E-01 1.760 0.240 0.4899 99.700 3.14E-02 29.760 0.240 0.4899 100.000 5.30E-01 5693 6121 6552 6986 7424 1.96-sigma TPU pCi/G 3.30E-02 2.42E-01 6.20E-02 2.15E-01 NOTES: MDA pCi/G 1.10E-01 1.32E-01 8.56E-02 8.54E-02 Le pCi/G 3.46E-02 3.91E-02 1.60E-02 1.60E-02 1.96-sigma cnt Unc pCi/G 3.29E-02 2.16E-01 6.18E-02 1.95E-01 *Results are a compilation of S0405235026_UU and T0405235026_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

Alpha Spectrosoopy Software Version 3.5.3 effedlvedate:02*Mar-2015 BATCH NUMBER : 1596396 SAMPLE ID : S0405235026 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 139 DETECTOR S/N : 76231 AVERAGE %EFFICIENCY : 24.8887 AVERAGE %EFF ERROR : 0.4828 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 85.1 +/-7.280 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.9585E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5320.94 U-3/4 4763.02 4781.50 U-235 4391.00 4448.01 U-238 4184.73 4204.42 U*238:3974-4284keV 31 U-235:43104581 keV U-J/4:4592-4865keV U*232:5000-5398keV 28 25 22 Ui 19 I-16 z => 13 0 10 7 *::;: t5 4 <( 1 2388 2785 3186 3591 Energy (keV) PEAK FWHM 27.542 20.979 49.363 16.043 >> 4 01 :!l COUNT DATE : 24-Sep-2016 13:19:52 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 236.000 234.560 1.440 1.2000 100.000 4.18E+OO 37.000 35.560 1.440 1.2000 100.000 6.28E-01 2.000 1.760 0.240 0.4899 99.700 3.12E-02 30.000 29.760 0.240 0.4899 100.000 5.26E-01 5679 6109 6543 6981 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B139.CNF;1109 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W139.CNF;334 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.18E-01 1.32E-01 3.91E-02 2.34E-01 1.31E-01 3.BBE-02 6.15E-02 8.49E-02 1.59E-02 2.0BE-01 8.47E-02 1.58E-02 1.96-sigma cnt Unc pCi/G 5.38E-01 2.15E-01 6.13E-02 1.93E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235027 UU SAMPLE QTY : 0.510 G -+/-0.196 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 70.2 +/-8.935 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0609E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 006 DETECTOR S/N : 79455 AVERAGE %EFFICIENCY : 26.3231 AVERAGE %EFF ERROR : 0.5098 COUNT DATE : 25-Sep-2016 15:53:59 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B006.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W006.CNF;571 CAL DATE : 27-Aug-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAK NET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4505.72 4453.76 TRACER2 1564-1 U-232 4.6539 dpm 5198.63 5318.10 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5198.63 0.000 0.000 -2.160 2.160 1.4697 100.000 U-3/4 4763.02 4779.29 56.194 49.000 48.760 0.240 0.4899 100.000 U-235 4391.00 4505.72 37.689 3.000 2.760 0.240 0.4899 99.700 U-238 4184.73 4201.03 6.327 49.000 48.040 0.960 0.9798 100.000 U 238*3974-4284keV U-235: 4310-4581 keV 64 I-U-314: 4592-4865 keV lJ.232:5000-5398keV 57 -50 t-43 (ii 36 I-z 29 '.'.) 0 s 22 .?;> 15 *;;; n 8 <!'. 1 -j , .11 I I I I I I I I 23 81 2782 3187 3594 4 05 419 5257 5681 6107 6537 6971 --Energy (keV) ACTIVITY pCi/G -3.21E-02 9.82E-01 5.58E-02 9.68E-01 I 7407 668.23 2.76 95.095 N/A -2.16 204.04 70.741 1.0081 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 3.67E-02 1.25E-01 4.01E-02 3.66E-02 3.30E-01 9.66E-02 1.81E-02 2.80E-01 8.10E-02 9.69E-02 1.81E-02 8.03E-02 3.29E-01 1.33E-01 3.62E-02 2.80E-01 NOTES:

Results are a compilation of S0405235027 _UU and T0405235027 _UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235027 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 140 DETECTOR S/N : 78771 AVERAGE %EFFICIENCY : 26.0317 AVERAGE %EFF ERROR : 0.5043 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 70.7 +/-7.707 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.2922E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5318.10 U-3/4 4763.02 4770.79 U-235 4391.00 4453.76 U-238 4184.73 4196.61 U238'3974-4284keV 28 U.235;431Q-4581kaV U-3/4:4592-4865keV 25 U.232:5000.5396keV 22 19 (jJ 16 I-z 13 ::i 0 10 s 7 *:;;: 4 I I I I I PEAK FWHM 22.288 7.243 84.197 24.104 llJ 111 I 23 85 2784 3186 3592 41 02 Energy (keV) COUNT DATE : 24-Sep-2016 13:19:54 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 205.000 204.040 0.960 0.9798 100.000 4.11E+OO 49.000 48.760 0.240 0.4899 100.000 9.74E-01 3.000 2.760 0.240 0.4899 99.700 5.53E-02 49.000 48.040 0.960 0.9798 100.000 9.60E-01 I j I ,,/ 1l1 I I II 111 I I I 48 3 5255 5681 6110 6543 6981 7422 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B140.CNF;1102 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W140.CNF;283 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.55E-01 1.33E-01 3.62E-02 3.16E-01 9.58E-02 1.79E-02 8.02E-02 9.61E-02 1.80E-02 3.15E-01 1.32E-01 3.59E-02 1.96-sigma cnt Unc pCi/G 5.67E-01 2.77E-01 7.97E-02 2.78E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235028 UU SAMPLE QTY : 0.507 G -+/-0.197 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 007 DETECTOR S/N : 50-066Z1 AVERAGE %EFFICIENCY : 26.6444 AVERAGE %EFF ERROR : 0.5159 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B007.CNF;1847 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 93.9 +/-8.221 % COUNT DATE : 25-Sep-2016 15:54:03 ELAPSED LIVE TIME(SEC) : 14399.99 EFF FILE : W007.CNF;503 CAL DATE : 23-Sep-2016 SECONDARY QTY : 0.507 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+O 1 dpm RESULTS : 9.7355E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 620.68 -0.72 PEAK NET2 3.04 278.52 RECOVERY YIELD CORR. 11.1230 dpm 4494.36 4408.61 4.6558 dpm 5198.60 5317.20 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev U-232 5302.10 5198.60 0.000 0.000 -0.720 0.720 0.8485 100.000 U-3/4 4763.02 4777.66 27.466 68.000 67.280 0.720 0.8485 100.000 U-235 4391.00 4494.36 29.551 4.000 3.040 0.960 0.9798 99.700 U-238 4184.73 4202.66 43.994 60.000 59.280 0.720 0.8485 100.000 }} >> i 73 U238*3974-4284keV U-314: 45924865 keV 65 l-U.232:5000-5398keV 57 >-49 -(j) 41 I-z 33 :::i -0 s 25 >-c 17 *;;; ti 9 <i: -,.,.J .iJ ,J I I I I I I 23 69 2771 3176 3584 31 95 48 9 5251 5677 6106 6538 6974 '----Energy (keV) ACTIVITY pCi/G -1.16E-02 9.99E-01 4.53E-02 8.80E-01 I 7413 87.264 N/A 94. 733 1.0085 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 3.50E-02 9.81E-02 2.50E-02 3.49E-02 2.93E-01 9.07E-02 2.31E-02 2.42E-01 6.76E-02 9.82E-02 2.67E-02 6.71E-02 2.70E-01 9.07E-02 2.31E-02 2.28E-01 NOTES:

Results are a compilation of S0405235028_UU and T0405235028_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235028 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 142 DETECTOR S/N : 42285 AVERAGE %EFFICIENCY : 26.5347 AVERAGE %EFF ERROR : 0.5139 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 94.7 +/-6.779 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 4.4106E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5317.20 U-3/4 4763.02 4773.24 U-235 4391.00 4408.61 U-238 4184.73 4201.61 28 U-238:3974-4284keV U-235:4310-4581keV 25 U*314:4592-4565keV U-232:5000.S398keV 22 19 en 16 I-13 z :J 0 10 7 *:;;: f5 4 <!'. 1 PEAK FWHM 49.649 53.151 192.826 46.806 ]] 2382 2780 3181 3586 3 94 406 Energy (keV) :'! COUNT DATE : 24-Sep-2016 13:19:57 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 279.000 278.520 0.480 0.6928 100.000 4.14E+OO 68.000 67.280 0.720 0.8485 100.000 9.91E-01 4.000 3.040 0.960 0.9798 99.700 4.49E-02 60.000 59.280 0.720 0.8485 100.000 8.73E-01 § 5664 6091 6521 6955 7393 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B142.CNF;1102 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W142.CNF;306 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.51E-01 8.23E-02 1.88E-02 2.76E-01 9.00E-02 2.29E-02 6.69E-02 9.73E-02 2.65E-02 2.56E-01 9.00E-02 2.29E-02 1.96-sigma cnt Unc pCi/G 4.87E-01 2.40E-01 6.66E-02 2.26E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235029 UU SAMPLE QTY : 0.504 G -+/-0.198 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 102 +/-8.097 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1085E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 008 DETECTOR S/N : 78788 AVERAGE %EFFICIENCY : 32.5514 AVERAGE %EFF ERROR : 0.6275 COUNT DATE : 25-Sep-2016 15:54:03 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B008.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W008.CNF;515 CAL DATE : 27-Aug-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAK NET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4489.20 4453.04 TRACER2 1564-1 U-232 4.6558 dpm 5363.01 5324.01 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G U-232 5302.10 5363.01 7.367 7.000 -0.440 7.440 2.7276 100.000 -5.07E-03 U-3/4 4763.02 4770.57 68.763 46.000 44.800 1.200 1.0954 100.000 7.16E-01 U-235 4391.00 4489.20 42.155 3.000 2.760 0.240 0.4899 99.700 4.42E-02 U-238 4184.73 4186.56 46.661 40.000 39.760 0.240 0.4899 100.000 6.35E-01 > .l1 -:;i g U*238:3974-4284keV 73 U-235:43104581 keV U-314: 45924865 keV U-232:5000-5398keV 65 57 49 Ci) 41 I-z 33 => 0 25 8 .o 17 0 9 <( 2396 2791 3191 3595 4 03 5682 6112 6547 6987 7430 Energy (keV) 863.42 2.76 99.362 N/A -0.44 260.52 103.207 1.0085 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.09E-02 1.50E-01 5.76E-02 7.08E-02 2.45E-01 1.12E-01 3.21E-02 2.15E-01 6.41E-02 7.68E-02 1.44E-02 6.37E-02 2.26E-01 7.66E-02 1.43E-02 2.01E-01 NOTES: *Results are a compilation of S0405235029_UU and T0405235029_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.013 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235029 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 143 DETECTOR S/N : 65882 AVERAGE %EFFICIENCY : 22.7820 AVERAGE %EFF ERROR : 0.4430 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 103 +/-6.964 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 4.8051 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5324.01 U-3/4 4763.02 4781.65 U-235 4391.00 4453.04 U-238 4184.73 4213.08 U-238:3974-4284keV 23 U-235:431o-4581 keV U-314:4592-4865keV 21 U-232:5000.5398keV 19 17 15 Ci) 13 I-z 11 ::J 9 0 7 5 *:;: u 3 <( 1 2372 2767 3165 Energy (keV) PEAK FWHM 76.995 21.133 176.926 58.975 COUNT DATE : 24-Sep-2016 13:19:59 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 261.000 260.520 0.480 0.6928 100.000 4.16E+OO 46.000 44.800 1.200 1.0954 100.000 7.10E-01 3.000 2.760 0.240 0.4899 99.700 4.38E-02 40.000 39.760 0.240 0.4899 100.000 6.30E-01 6051 6478 6907 7340 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B143.CNF;1098 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W143.CNF;291 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.78E-01 8.85E-02 2.03E-02 2.36E-01 1.11E-01 3.18E-02 6.35E-02 7.62E-02 1.43E-02 2.18E-01 7.59E-02 1.42E-02 1.96-sigma cnt Unc pCi/G 5.07E-01 2.14E-01 6.32E-02 1.99E-01 "t1 00 Version 3.5.3 0 ...., BATCH NUMBER : 1596396 SAMPLE ID : T0405235030 UU g SAMPLE QTY : 0.514 G -+/-0.195 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 97.1 +/-8.055 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.1979E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 009 DETECTOR S/N : 72528 AVERAGE %EFFICIENCY : 31.6819 AVERAGE %EFF ERROR : 0.6111 COUNT DATE : 25-Sep-2016 15:54:03 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B009.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W009.CNF;514 CAL DATE : 23-Sep-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E TRACER2 1564-1 NUCLIDE LIBRARY PEAK (ii I-z :J 0 <t: ENERGY ENERGY U-232 5302.10 5242.83 U-3/4 4763.02 4764.83 U-235 4391.00 4498.23 U-238 4184.73 4213.36 U-236: 39744284 keV U-235:4310-4581 keV 73 U-3/4:4592-4S65keV U-232:5000-S398keV 65 57 49 41 33 25 17 9 2380 2778 3179 3585 Energy (keV) U-235 11.1230 dpm 4498.23 4393.23 U-232 4.6558 dpm 5242.83 5310.35 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN ACTIVITY FWHM AREA AREA AREA StDev pCi/G 4.938 1.000 0.280 0.720 0.8485 100.000 4.03E-03 57.614 68.000 68.000 0.000 0.0000 100.000 9.72E-01 27.054 1.000 0.760 0.240 0.4899 99.700 1.09E-02 26.808 59.000 58.040 0.960 0.9798 100.000 8.30E-01 g i§ i 5674 6105 6539 6978 7421 697.28 0.76 82.445 N/A 0.28 285.76 98.006 1.0095 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.22E-02 8.80E-02 2.24E-02 4.22E-02 2.81E-01 4.29E-02 O.OOE+OO 2.33E-01 4.09E-02 6.87E-02 1.29E-02 4.09E-02 2.56E-01 9.42E-02 2.57E-02 2.18E-01 NOTES:

Results are a compilation of S0405235030_UU and T0405235030_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235030 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G -+/-0.195 % CHAMBER : 144 DETECTOR S/N : 75551 AVERAGE %EFFICIENCY : 26.3153 AVERAGE %EFF ERROR : 0.5097 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 98.0 +/-6.708 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 4.5630E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5310.35 U-3/4 4763.02 4771.24 U-235 4391.00 4393.23 U-238 4184.73 4190.92 U-238:3974-4284keV 23 U-235:4310-4581 keV LJ..3/4:4592-4865keV 21 U-232:SOCJ0..5396keV 19 17 15 0' 13 z 11 :::> 9 0 7 5 *:;; :g 3 <( 2389 Energy (keV) PEAK FWHM 76.757 35.629 4.914 39.315 COUNT DATE : 24-Sep-2016 13:20:01 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 286.000 285.760 0.240 0.4899 100.000 4.08E+OO 68.000 68.000 0.000 0.0000 100.000 9.63E-01 1.000 0.760 0.240 0.4899 99.700 1.08E-02 59.000 58.040 0.960 0.9798 100.000 8.22E-01 5660 6086 6517 6951 7389 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B144.CNF;1103 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W144.CNF;297 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.33E-01 6.85E-02 1.28E-02 2.66E-01 4.25E-02 O.OOE+OO 4.05E-02 6.81E-02 1.27E-02 2.43E-01 9.33E-02 2.54E-02 1.96-sigma cnt Unc pCi/G 4.74E-01 2.31E-01 4.05E-02 2.15E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235031_UU SAMPLE QTY : 0.517 G +/-0.193 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 010 DETECTOR SIN : 72529 AVERAGE %EFFICIENCY : 29.8601 AVERAGE %EFF ERROR : 0.5768 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B010.CNF;1843 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 93.8 +/-8.070 % COUNT DATE : 25-Sep-2016 15:54:03 ELAPSED LIVE TIME(SEC) : 14399.99 EFF FILE : W010.CNF;511 CAL DATE : 27-Aug-2016 SECONDARY QTY : 0.502 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0505E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 750.55 -1.60 PEAK NET2 2.00 276.28 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5190.52 U-3/4 4763.02 4751.08 U-235 4391.00 4478.00 U-238 4184.73 4184.19 U-238: 3974-4284 keV U-235:4310-4Sl31 keV 64 U-314:45924865keV U*232:S000-5398keV 57 50 43 (ii 36 I-z 29 :J 0 s. 22 .?:-15 t5 8 <t: 2405 2800 3199 3602 Energy (keV) 11.1230 dpm 4478.00 4518.69 4.6555 dpm 5190.52 5340.26 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA S!Dev 4.911 8.000 -1.600 9.600 3.0984 100.000 8.595 57.000 56.040 0.960 0.9798 100.000 49.114 2.000 2.000 0.000 0.0000 99.700 52.797 55.000 53.800 1.200 1.0954 100.000 > Ji ! 4 09 420 48 6 5255 5678 6106 6537 6973 :>! ACTIVITY pCi/G -2.15E-02 8.23E-01 2.95E-02 7.90E-01 7412 1.96-sigma TPU pCi/G 8.86E-02 2.57E-01 5.07E-02 2.51E-01 NOTES: MDA pCi/G 1.92E-01 9.67E-02 4.42E-02 1.03E-01 94.158 N/A 94.582 1.0084 Le pCi/G 7.61E-02 2.64E-02 O.OOE+OO 2.95E-02 1.96-sigma cnt Unc pCi/G 8.86E-02 2.20E-01 5.05E-02 2.16E-01

Results are a compilation of S0405235031_UU and T0405235031_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235031_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.517 G +/-0.193 % CHAMBER : 145 DETECTOR S/N : 72526 AVERAGE %EFFICIENCY : 26.3634 AVERAGE %EFF ERROR : 0.5106 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 94.6 +/-6.804 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6555E+OO dpm 4.4032E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5340.26 U-3/4 4763.02 4793.86 U-235 4391.00 4518.69 U-238 4184.73 4233.28 U-238: 39744284 keV 31 U.235:4310-4581keV U-314:45924865keV lJ..232:5000-5398keV 28 25 22 'Ci) 19 I-16 z ::J 13 0 £ 10 7 u 4 <l.'. 1 2411 2806 3205 Energy (keV) PEAK FWHM 27.551 14.741 44.222 11.512 COUNT DATE : 24-Sep-2016 13:20:04 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 277.000 276.280 0.720 0.8485 100.000 4.06E+OO 57.000 56.040 0.960 0.9798 100.000 8.16E-01 2.000 2.000 0.000 0.0000 99.700 2.92E-02 55.000 53.800 1.200 1.0954 100.000 7.83E-01 5682 6108 6539 6973 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B145.CNF;1121 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W145.CNF;365 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.40E-01 8.97E-02 2.28E-02 2.46E-01 9.59E-02 2.61E-02 5.02E-02 4.38E-02 O.OOE+OO 2.40E-01 1.02E-01 2.92E-02 1.96-sigma cnt Unc pCi/G 4.80E-01 2.18E-01 5.00E-02 2.14E-01 "' 00 ::j 3.5.3 0 '"" BATCH NUMBER : 1596396 SAMPLE ID : T0405235032 UU SAMPLE QTY : 0.508 G -+/-0.197 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 61.8 +/-9.242 % SECONDARY QTY : 0.512 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0741E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 011 DETECTOR S/N : 72531 AVERAGE %EFFICIENCY : 31.0555 AVERAGE %EFF ERROR : 0.5992 COUNT DATE : 25-Sep-2016 15:54:03 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B011.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W011.CNF;511 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4491.87 4503.11 4.6558 dpm 5280.99 5313.39 PEAK NET 1 798.13 3.04 PEAKNET2 3.76 177.60 RECOVERY YIELD CORR. 96.273 NIA 62.867 1.0176 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5280.99 0.000 10.000 U-3/4 4763.02 4776.82 60.251 39.000 U-235 4391.00 4491.87 40.463 4.000 U-238 4184.73 4181.89 53.418 27.000 > U-238:3974-4264keV 73 U-235:4310-4581 keV U-J.14:4592-486SkeV U-232:5000-5398keV 65 57 49 41 z 33 ::J 0 25 17 *:;; ti 9 <( 1 2388 2788 3192 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 3.040 6.960 2.6382 100.000 3.76E-02 38.280 0.720 0.8485 100.000 8.98E-01 3.760 0.240 0.4899 99.700 8.85E-02 26.280 0.720 0.8485 100.000 6.16E-01 6580 7023 7470 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 8.67E-02 1.57E-01 5.98E-02 8.65E-02 3.36E-01 1.43E-01 3.65E-02 2.92E-01 1.06E-01 1.13E-01 2.11E-02 1.04E-01 2.70E-01 1.43E-01 3.65E-02 2.44E-01 NOTES: *Results are a compilation of S0405235032_UU and T0405235032_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.012 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235032 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 146 DETECTOR S/N : 72527 AVERAGE %EFFICIENCY : 25.4962 AVERAGE %EFF ERROR : 0.4943 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 62.9 +/-8.212 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 2.9270E+OO dpm NUCLIDE LIBRARY PEAK Vi I-z :::> 0 s *;;: <1'. ENERGY ENERGY U-232 5302.10 5313.39 U-3/4 4763.02 4780.77 U-235 4391.00 4503.11 U-238 4184.73 4212.70 19 U*238:3974-4264keV lJ.235:431Cl-4581 keV 17 U-314:4592-4865keV U-232:5000-5398keV 15 13 11 9 7 5 3 2423 2815 3212 3613 Energy (keV) PEAK FWHM 19.378 36.563 4.875 9.750 COUNT DATE : 24-Sep-2016 13:20:06 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 180.000 177.600 2.400 1.5492 100.000 4.13E+OO 39.000 38.280 0.720 0.8485 100.000 8.82E-01 4.000 3.760 0.240 0.4899 99.700 8.69E-02 27.000 26.280 0.720 0.8485 100.000 6.06E-01 > i 6550 6987 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B146.CNF;1123 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W146.CNF;315 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.18E-01 2.02E-01 6.60E-02 3.22E-01 1.41E-01 3.58E-02 1.03E-01 1.11E-01 2.07E-02 2.60E-01 1.41E-01 3.58E-02 1.96-sigma cnt Unc pCi/G 6.14E-01 2.87E-01 1.02E-01 2.40E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235033 UU SAMPLE QTY : 0.506 G -+/-0.198 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 70.3 +/-8.979 % SECONDARY QTY : 0.514 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 9.7516E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 012 DETECTOR S/N : 80054 AVERAGE %EFFICIENCY : 29.3381 AVERAGE %EFF ERROR : 0.5668 COUNT DATE : 25-Sep-2016 15:54:03 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B012.CNF;1839 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W012.CNF;494 CAL DATE : 27-Aug-2016 TRACER CORRECTION ID NUCLIDE NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 PEAKNET2 RECOVERY YIELD CORR. TRACER 1 1570-E U-235 11.1230 dpm 4492.84 4396.40 684.56 3.76 87.407 N/A TRACER2 1564-1 U-232 4.6558 dpm 5305.56 5319.98 1.60 200.84 71.250 1.0140 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le en! Unc ENERGY ENERGY FWHM AREA AREA AREA S!Dev pCi/G pCi/G pCi/G pCi/G pCi/G U-232 5302.10 5305.56 4.910 10.000 1.600 8.400 2.8983 100.000 2.30E-02 1.02E-01 1.96E-01 7.62E-02 1.02E-01 U-3/4 4763.02 4772.27 40.505 31.000 30.520 0.480 0.6928 100.000 6.33E-01 2.57E-01 1.15E-01 2.63E-02 2.31E-01 U-235 4391.00 4492.84 32.753 4.000 3.760 0.240 0.4899 99.700 7.83E-02 9.33E-02 9.98E-02 1.87E-02 9.23E-02 U-238 4184.73 4178.81 18.820 48.000 47.280 0.720 0.8485 100.000 9.81E-01 3.36E-01 1.27E-01 3.23E-02 2.85E-01 NOTES: *Results are a compilation of S0405235033_UU and T0405235033_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232 U-238:3974-4264keV

Correction made to the following net area 64 U-235:431Cl-4581keV lJ.3r'4:4592-4865keV due to tracer impurity: 57 U-232:5Q00.5398keV U-238 (0.010 +/-0.000) 50 43 'iii 36 I-z 29 ::i 0 22 c 15 *:;: t5 8 <!'. 1 2402 2797 3196 3599 4 07 419 5680 6109 6542 6979 7420 Energy (keV)

"d 00 00 0 0 ...., Ul 00 0 \D BATCH NUMBER : 1596396 SAMPLE ID : S0405235033 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 147 DETECTOR S/N : 75550 AVERAGE %EFFICIENCY : 25.4403 AVERAGE %EFF ERROR : 0.4932 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 71.3 +/-7.782 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 3.3173E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5319.98 U-3/4 4763.02 4782.63 U-235 4391.00 4396.40 U-238 4184.73 4208.75 19 U*238;3974-42841wV U-235:43104581 keV 17 U-314: 4592-4865 keV U*232:5000-539BkeV 15 13 if) 11 I-9 z ::> 0 7 8 5 c *;;: 3 t5 <( 2390 2790 3193 Energy (keV) PEAK FWHM 66.305 16.162 129.295 50.765 COUNT DATE : 24-Sep-2016 13:20:09 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 203.000 200.840 2.160 1.4697 100.000 4.14E+OO 31.000 30.520 0.480 0.6928 100.000 6.25E-01 4.000 3.760 0.240 0.4899 99.700 7.72E-02 48.000 47.280 0.720 0.8485 100.000 9.68E-01 6546 6981 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B147.CNF;1093 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W147.CNF;294 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.71E-01 1.73E-01 5.56E-02 2.48E-01 1.13E-01 2.60E-02 9.18E-02 9.84E-02 1.84E-02 3.20E-01 1.25E-01 3.18E-02 1.96-sigma cnt Unc pCi/G 5.79E-01 2.27E-01 9.10E-02 2.81E-01 0 ....., U> 00 0 \0 BATCH NUMBER : 1596396 SAMPLE ID : T0405235034 UU SAMPLE QTY : 0.509 G -+/-0.196 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 56.7 +/-9.602 % SECONDARY QTY : 0.515 G +/-0.194 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0597E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER.: 013 DETECTOR S/N : 78790 AVERAGE %EFFICIENCY : 35.0288 AVERAGE %EFF ERROR : 0.6744 COUNT DATE : 25-Sep-2016 15:54:08 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B013.CNF;1815 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W013.CNF;513 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4486.89 4421.61 4.6558 dpm 5327.26 5314.34 PEAK NET 1 888.19 2.28 PEAKNET2 3.00 154.80 RECOVERY YIELD CORR. 94.983 N/A 57.523 1.0146 NUCLIDE LIBRARY PEAK z :::i 0 !2-c *s: ti <l'. ENERGY ENERGY U-232 5302.10 5327.26 U-3/4 4763.02 4766.35 U-235 4391.00 4486.89 U-238 4184.73 4191.02 U*238:3974-4284keV U-235:431Cl-4581keV 73 U.314: 45924865 keV U-232:5Q00..5398keV 65 57 49 41 33 25 17 9 2395 2793 3196 3604 Energy (keV) PEAK GROSS FWHM AREA 165.966 9.000 21.881 38.000 55.625 3.000 44.863 39.000 i NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G 2.280 6.720 2.5923 100.000 2.52E-02 37.280 0.720 0.8485 100.000 9.98E-01 3.000 0.000 0.0000 99.700 8.06E-02 38.280 0.720 0.8485 100.000 1.03E+OO 5706 6140 6578 7020 7467 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 7.41E-02 1.38E-01 5.25E-02 7.40E-02 3.81E-01 1.64E-01 4.16E-02 3.29E-01 1.07E-01 8.06E-02 O.OOE+OO 1.06E-01 3.87E-01 1.64E-01 4.16E-02 3.33E-01 NOTES:

Results are a compilation of S0405235034_UU and T0405235034_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.013 +/-0.000)

A!phaSpectroscopySoflwateVersionJ.5.3 effeclivedate:02-Mar-2015 BATCH NUMBER : 1596396 SAMPLE ID : S0405235034 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 148 DETECTOR S/N : 74429 AVERAGE %EFFICIENCY : 24.2876 AVERAGE %EFF ERROR : 0.4715 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 57.5 +/-8.690 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 2.6782E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5314.34 U-3/4 4763.02 4771.78 U-235 4391.00 4421.61 U-238 4184.73 4218.77 15 U-238: 3974-4284 keV U-235:431D-4Sa1 keV U-314:4592-4865keV 13 U-232:5000-5398keV 11 (ii 9 I-7 z :::i 0 5 .?;> 3 *:;: n <i: PEAK FWHM 66.688 26.128 215.558 57.564 i ::! COUNT DATE : 24-Sep-2016 13:20:11 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 156.000 154.800 1.200 1.0954 100.000 4.12E+OO 38.000 37.280 0.720 0.8485 100.000 9.84E-01 3.000 3.000 0.000 0.0000 99.700 7.94E-02 39.000 38.280 0.720 0.8485 100.000 1.01E+OO 2410 2804 3202 3604 4 11 422 5679 6106 6538 6973 7413 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B148.CNF;1094 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W148.CNF;312 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCl/G 9.72E-01 1.87E-01 5.34E-02 3.67E-01 1.61E-01 4.10E-02 1.05E-01 7.94E-02 O.OOE+OO 3.73E-01 1.61E-01 4.10E-02 1.96-sigma cnt Unc pCl/G 6.54E-01 3.24E-01 1.05E-01 3.28E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235035 UU SAMPLE QTY : 0.516 G -+/-0.194 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 44.8 +/-11.231 % SECONDARY QTY : 0.510 G +/-0.196 % TRACER ID : 1570-E NUCLIDE : NOMINAL : 1.1123E+01 dpm RESULTS : 3.9312E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 014 DETECTOR S/N : 83289 AVERAGE %EFFICIENCY : 32.6875 AVERAGE %EFF ERROR : 0.6302 COUNT DATE : 25-Sep-2016 15:54:08 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B014.CNF;1816 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W014.CNF;523 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK.ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4492.23 4472.87 4.6558 dpm 5303.43 5320.42 PEAK NET 1 307.47 3.04 PEAKNET2 1.04 129.52 RECOVERY YIELD CORR. 35.237 N/A 46.246 1.0326 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5303.43 245.730 10.000 U-3/4 4763.02 4773.30 7.372 30.000 U-235 4391.00 4492.23 25.041 2.000 U-238 4184.73 4191.92 18.430 23.000 U-238: 39744284 keV 37 U-235:43104581 keV lJ..314:4592-4865keV 33 U-232:5000..5398keV 29 25 if) 21 I-z 17 ::::> 0 13 s 9 *::; u 5 <l: 1 2378 2773 3173 3578 3 88 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 3.040 6.960 2.6382 100.000 9.80E-02 29.040 0.960 0.9798 100.000 9.33E-01 1.040 0.960 0.9798 99.700 3.35E-02 22.760 0.240 0.4899 100.000 7.31E-01 5672 6104 6542 6983 7430 ::! 1.96-sigma TPU pCi/G 2.26E-01 4.09E-01 1.15E-01 3.50E-01 NOTES: MDA pCi/G 4.08E-01 2.12E-01 2.12E-01 1.54E-01 Le pCi/G 1.56E-01 5.77E-02 5.78E-02 2.88E-02 1.96-sigma cnt Unc pCi/G 2.25E-01 3.52E*01 1.15E-01 3.09E-01 *Results are a compilation of S0405235035_UU and T0405235035_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.005 +/-0.000)

"" Cl> 00 00 """ 0 ....., Vl 00 0 "' BATCH NUMBER : 1596396 SAMPLE ID : S0405235035 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.516 G -+/-0.194 % CHAMBER : 149 DETECTOR S/N : 33449 AVERAGE %EFFICIENCY : 25.2769 AVERAGE %EFF ERROR : 0.4901 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 46.2 +/-9.383 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 2.1531E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5320.42 U-3/4 4763.02 4776.09 U-235 4391.00 4472.87 U-238 4184.73 4175.77 U*238:3974-4284keV 15 lJ..235: 4310-4581 keV U-314: 4592-4865 keV lJ..232:5000.5398keV 13 11 'Ci) 9 I-z 7 ::i 0 5 *::; 3 u <t: 2411 2804 3201 3602 Energy (keV) PEAK FWHM 26.695 62.260 117.195 90.338 COUNT DATE : 24-Sep-2016 13:20:13 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 130.000 129.520 0.480 0.6928 100.000 4.06E+OO 30.000 29.040 0.960 0.9798 100.000 9.04E-01 2.000 1.040 0.960 0.9798 99.700 3.25E-02 23.000 22.760 0.240 0.4899 100.000 7.08E-01 5676 6104 6536 6972 7413 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B149.CNF;1104 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W149.CNF;305 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.04E+OO 1.74E-01 3.98E-02 3.81E-01 2.05E-01 5.58E-02 1.11E-01 2.06E-01 5.60E-02 3.28E-01 1.49E-01 2.79E-02 1.96-sigma en! Une pCi/G 7.04E-01 3.41E-01 1.11E-01 2.99E-01 "O (l> 00 00 Vl 0 ....., Vl 00 0 \0 BATCH NUMBER : 1596396 SAMPLE ID : T0405235036 UU SAMPLE QTY : 0.518 G -+/-0.193 % SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 34.4 +/-11.565 % SECONDARY QTY : 0.508 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1085E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 015 DETECTOR S/N : 80055 AVERAGE %EFFICIENCY : 33.3682 AVERAGE %EFF ERROR : 0.6430 COUNT DATE : 25-Sep-2016 15:54:08 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B015.CNF;1835 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W015.CNF;530 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4481.54 4456.36 4.6558 dpm 5302.79 5322.85 PEAK NET 1 885.05 1.72 PEAK NET2 1.76 95.80 RECOVERY YIELD CORR. 99.359 N/A 34.814 1.0133 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5302.79 240.946 7.000 U-3/4 4763.02 4757.74 62.080 19.000 U-235 4391.00 4481.54 36.907 2.000 U-238 4184.73 4180.69 27.045 25.000 g i§ U-238:3974-4264keV 81 U-235:431()-4581 keV U-314: 45924865 keV 73 U-232:500Q..5398keV 65 57 en 49 I-41 z => 33 0 25 17 :g 9 <X'. 2386 2781 3182 3587 3 96 410 48 9 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA S!Dev pCi/G 1.720 5.280 2.2978 100.000 1.93E-02 18.520 0.480 0.6928 100.000 7.86E-01 1.760 0.240 0.4899 99.700 7.50E-02 25.000 0.000 0.0000 100.000 1.06E+OO g 5252 5680 6112 6549 6990 7436 1.96-sigma TPU pCi/G 6.74E-02 4.15E-01 1.48E-01 4.90E-01 NOTES: MDA pCi/G 1.28E-01 2.35E-01 2.04E-01 1.27E-01 Le pCi/G 4.73E-02 5.39E-02 3.82E-02 0.00E+OO 1.96-sigma en! Une pCi/G 6.73E-02 3.74E-01 1.47E-01 4.25E-01

Results are a compilation of S0405235036_UU and T0405235036_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.013 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235036 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 150 DETECTOR S/N : 75552 AVERAGE %EFFICIENCY : 24.8352 AVERAGE %EFF ERROR : 0.4817 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 34.8 +/-10.817 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6558E+OO dpm 1.6209E+OO dpm NUCLIDE LIBRARY PEAK 00 I-z ::J 0 *;;: n <l'. ENERGY ENERGY U-232 5302.10 5322.85 U-3/4 4763.02 4770.52 U-235 4391.00 4456.36 U-238 4184.73 4204.23 14 U*238: 3974-4284 keV U*235:431o-4581 keV 13 U-314: 4592-4865 keV 12 U*232:5000.5398keV 11 10 9 8 7 6 5 4 3 2 1 2390 2790 3193 3601 Energy (keV) PEAK FWHM 29.335 69.693 174.233 17.423 COUNT DATE : 24-Sep-2016 13:20:16 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 97.000 95.800 1.200 1.0954 100.000 4.05E+OO 19.000 18.520 0.480 0.6928 100.000 7.76E-01 2.000 1.760 0.240 0.4899 99.700 7.40E-02 25.000 25.000 0.000 0.0000 100.000 1.05E+OO 5688 6117 6548 6983 7422 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKGFILE: B150.CNF;1102 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W150.CNF;296 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.20E+OO 2.96E-01 8.48E-02 4.05E-01 2.32E-01 5.32E-02 1.46E-01 2.02E-01 3.77E-02 4.76E-01 1.26E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 8.21E-01 3.69E-01 1.45E-01 4.19E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235037 UU SAMPLE QTY : 0.506 G -+/-0.198 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 016 DETECTOR S/N : 78774 AVERAGE %EFFICIENCY : 33.4185 AVERAGE %EFF ERROR : 0.6439 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B016.CNF;1811 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 25.3 +/-13.443 % COUNT DATE : 25-Sep-2016 15:54:08 ELAPSED LIVE TIME(SEC) : 14399.99 EFF FILE : W016.CNF;494 CAL DATE : 27-Aug-2016 SECONDARY QTY : 0.512 G +/-0.195 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.4608E+OO dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 756.52 4.60 PEAK NET 2 -0.96 69.60 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5309.48 U-3/4 4763.02 4775.94 U-235 4391.00 4481.94 U-238 4184.73 4189.93 U-238:3974-4284keV 73 U-235:4310-4581keV lJ..314:4592-4865keV U-232:5000-S398keV 65 57 49 "Ci) 41 I-z 33 :::i 0 25 8 0 17 *;:; t5 9 2399 2793 3192 3596 Energy (keV) 11.1230 dpm 4481.94 4445.43 4.6549 dpm 5309.48 5319.42 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA StDev 9.790 13.000 4.600 8.400 2.8983 100.000 45.362 8.000 4.880 3.120 1.7664 100.000 47.664 0.000 -0.960 0.960 0.9798 99.700 33.246 8.000 7.520 0.480 0.6928 100.000 > i§ 4 04 417 48 5 5258 5685 6118 6555 6997 i'l 2: ACTIVITY pCi/G 6.00E-02 2.95E-01 -5.82E-02 4.54E-01 7443 1.96-sigma TPU pCi/G 1.04E-01 3.79E-01 1.36E-01 3.78E-01 NOTES: MDA pCi/G 1.78E-01 5.72E-01 3.99E-01 3.34E-01 84.802 N/A 25.861 1.0228 Le pCi/G 6.92E-02 1.95E-01 1.09E-01 7.66E-02 1.96-sigma cnt Unc pCi/G 1.02E-01 3.71E-01 1.35E-01 3.59E-01 *Results are a compilation of S0405235037 _UU and T0405235037 _UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.011 +/-0.000)

'i:I 00 00 00 0 ....., V\ 00 0 \0 BATCH NUMBER : 1596396 SAMPLE ID : S0405235037 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 152 DETECTOR S/N : 76222 AVERAGE %EFFICIENCY : 24.2896 AVERAGE %EFF ERROR : 0.4714 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 25.9 +/-12.722 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 1.2038E+OO dpm NUCLIDE LIBRARY PEAK en I-z ::::> 0 s *:;: t5 <i: ENERGY ENERGY U-232 5302.10 5319.42 U-3/4 4763.02 4771.39 U-235 4391.00 4445.43 U-238 4184.73 4208.22 10 U-238: 3974-4284 keV U-235:43104581 keV 9 U-:Y4:4592-486SkeV U-232:5000-5398keV 8 7 6 5 4 3 2 1 2406 2798 3194 3594 Energy (keV) PEAK FWHM 32.608 7.300 0.000 46.235 COUNT DATE : 24-Sep-2016 13:20:18 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 72.000 69.600 2.400 1.5492 100.000 4.14E+OO 8.000 4.880 3.120 1.7664 100.000 2.88E-01 0.000 -0.960 0.960 0.9798 99.700 -5.69E-02 8.000 7.520 0.480 0.6928 100.000 4.44E-01 8 6517 6952 7391 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B152.CNF;1088 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W152.CNF;285 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.45E+OO 5.17E-01 1.69E-01 3.70E-01 5.59E-01 1.91E-01 1.33E-01 3.90E-01 1.06E-01 3.68E-01 3.27E-01 7.49E-02 1.96-sigma cnt Unc pCi/G 1.00E+OO 3.62E-01 1.32E-01 3.51E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235038 UU SAMPLE QTY : 0.501 G -+/-0.200 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 017 DETECTOR S/N : 78791 AVERAGE %EFFICIENCY : 30.2659 AVERAGE %EFF ERROR : 0.5843 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B017.CNF;2657 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 82.9 +/-8.343 % COUNT DATE : 25-Sep-2016 15:54:08 ELAPSED LIVE TIME(SEC) : 14399.99 EFF FILE : W017.CNF;1450 CAL DATE : 27-Aug-2016 SECONDARY QTY : 0.520 G +/-0.192 % TRACER . ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0954E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAKNET1 793.28 1.00 PEAKNET2 5.28 242.56 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5217.63 U-3/4 4763.02 4761.08 U-235 4391.00 4478.19 U-238 4184.73 4166.73 -lJ.238* 3974-4284 keV lJ..235;4310-4581keV 82 t-lJ..314: 45924865 keV U-232:S000-5398keV 73 f-64 f-55 f-en 46 I-z :::> 37 0 28 19 *;; u 10 <!'. 1 I I 23 82 2779 3181 3587 Energy (keV) 11.1230 dpm 4478.19 4412.47 4.6549 dpm 5217.63 5310.83 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA S!Dev 296.030 7.000 1.000 6.000 2.4495 100.000 40.910 34.000 33.040 0.960 0.9798 100.000 30.769 6.000 5.280 0.720 0.8485 99.700 44.199 43.000 42.520 0.480 0.6928 100.000 'i >> 'i !!!! U .. I, I I I I I 3!97 412 48 1 5255 5683 6116 6553 6994 -ACTIVITY pCi/G 1.22E-02 5.72E-01 9.16E-02 7.36E-01 I 7440 1.96-sigma TPU pCi/G 7.40E-02 2.23E-01 9.28E-02 2.57E-01 NOTES: MDA pCi/G 1.47E-01 1.14E-01 1.06E-01 9.58E-02 98.184 N/A 83.836 1.0112 Le pCi/G 5.50E-02 3.11E-02 2.70E-02 2.20E-02 1.96-sigma en! Une pCi/G 7.40E-02 2.01E-01 9.15E-02 2.25E-01

Results are a compilation of S0405235038_UU and T0405235038_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.012 +/-0.000)

A!phaSpectroscopySoftwareVersion3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596396 SAMPLE ID : S0405235038 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 154 DETECTOR S/N : 76224 AVERAGE %EFFICIENCY : 26.1126 AVERAGE %EFF ERROR : 0.5058 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 83.8 +/-7.180 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.9025E+OO dpm NUCLIDE LIBRARY PEAK (ii I-z :J 0 £ *:;; u <( ENERGY ENERGY U-232 5302.10 5310.83 U-3/4 4763.02 4754.77 U-235 4391.00 4412.47 U-238 4184.73 4192.33 U-23B:3974-4284keV U-235:431o-45B1keV 25 U-3/4:4592-4865keV U-232:5000-539BkeV 22 19 16 13 10 7 4 2372 2768 3169 3574 Energy (keV) PEAK FWHM 33.017 47.726 4.937 52.663 COUNT DATE : 24-Sep-2016 13:20:21 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 244.000 242.560 1.440 1.2000 100.000 4.19E+OO 34.000 33.040 0.960 0.9798 100.000 5.65E-01 6.000 5.280 0.720 0.8485 99.700 9.06E-02 43.000 42.520 0.480 0.6928 100.000 7.28E-01 6081 6513 6948 7387 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B154.CNF;1099 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W154.CNF;304 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.08E-01 1.28E-01 3.79E-02 2.16E-01 1.13E-01 3.07E-02 9.14E-02 1.05E-01 2.67E-02 2.47E-01 9.48E-02 2.17E-02 1.96-sigma cnt Unc pCi/G 5.30E-01 1.99E-01 9.05E-02 2.23E-01 0 ....., V\ 00 0 '° AlphaSpectroscopySoftwareVersion3.5.3 effectivedate:OZ-Mar-2015 BATCH NUMBER : 1596396 SAMPLE ID : T0405235039 UU SAMPLE QTY : 0.512 G -+/-0.195 % SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 76.5 +/-8.492 % SECONDARY QTY : 0.507 G +/-0.197 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.1351E+01 dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 018 DETECTOR S/N : 78782 AVERAGE %EFFICIENCY : 31.3297 AVERAGE %EFF ERROR : 0.6044 COUNT DATE : 25-Sep-2016 15:54:08 ELAPSED LIVE TIME(SEC) : 14399.99 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B018.CNF;1812 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W018.CNF;484 CAL DATE : 27-Aug-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4482.13 4398.10 4.6549 dpm 5236.66 5308.15 PEAK NET 1 850.90 0.44 PEAK NET2 1.52 225.84 RECOVERY YIELD CORR. 101.740 N/A 77.243 1.0095 NUCLIDE LIBRARY PEAK ENERGY ENERGY 'iii I-z :J 0 S2. u -ct: U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U-238:3974-4284keV U-235: 4310-4581 keV 73 U-3/4:4592-4865keV U-232:5000-S39BkeV 65 57 49 41 33 25 17 9 2380 2776 3176 Energy (keV) 5236.66 4753.92 4482.13 4175.10 PEAK GROSS FWHM AREA 290.134 5.000 83.598 35.000 56.335 2.000 42.291 55.000 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.440 4.560 2.1354 100.000 5.15E-03 34.520 0.480 0.6928 100.000 6.27E-01 1.520 0.480 0.6928 99.700 2.77E-02 54.760 0.240 0.4899 100.000 9.94E-01 5675 6108 6545 6987 7433 1.96-sigma TPU pCi/G 6.14E-02 2.39E-01 6.38E-02 3.16E-01 NOTES: MDA pCi/G 1.27E-01 1.01E-01 1.01E-01 8.71E-02 Le pCi/G 4.58E-02 2.30E-02 2.31E-02 1.63E-02 1.96-sigma en! Unc pCi/G 6.14E-02 2.14E-01 6.36E-02 2.67E-01

Results are a compilation of S0405235039_UU and T0405235039_UU.
The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.013 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235039 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 155 DETECTOR SIN : 75553 AVERAGE %EFFICIENCY : 26.3876 AVERAGE %EFF ERROR : 0.5110 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 77.2 +/-7.406 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.5956E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5308.15 U-3/4 4763.02 4761.95 U-235 4391.00 4398.10 U-238 4184.73 4180.74 U-238:3974-4284keV 23 U-235:4310-4581 keV lJ.3/4:4592-4865keV 21 U-232:5000-5398keV 19 17 15 0' 13 z 11 => 9 0 £ 7 5 *:;: 3 1 2395 2792 3192 Energy (keV) PEAK FWHM 39.442 39.442 93.674 81.965 COUNT DATE : 24-Sep-2016 13:20:22 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 228.000 225.840 2.160 1.4697 100.000 4.10E+OO 35.000 34.520 0.480 0.6928 100.000 6.21E-01 2.000 1.520 0.480 0.6928 99.700 2.74E-02 55.000 54.760 0.240 0.4899 100.000 9.85E-01 5682 6111 6545 6982 7 424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B155.CNF;1101 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 . EFF FILE : W155.CNF;289 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.17E-01 1.52E-01 4.88E-02 2.32E-01 9.96E-02 2.28E-02 6.31E-02 9.99E-02 2.29E-02 3.03E-01 8.62E-02 1.61E-02 1.96-sigma cnt Unc pCi/G 5.39E-01 2.12E-01 6.30E-02 2.64E-01 BATCH NUMBER : 1596396 SAMPLE ID : T0405235040 UU SAMPLE QTY : 0.515 G -+/-0.194 % SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 83.1 +/-8.624 % SECONDARY QTY : 0.503 G +/-0.199 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.8641 E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 113 DETECTOR S/N : 80009 AVERAGE %EFFICIENCY : 24.7132 AVERAGE %EFF ERROR : 0.4794 COUNT DATE : 25-Sep-2016 15:54:41 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B113.CNF;1167 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W113.CNF;318 CAL DATE : 08-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4496.66 4488.99 4.6549 dpm 5198.57 5308.13 PEAK NET 1 583.30 -1.44 PEAKNET2 6.28 240.80 RECOVERY YIELD CORR. 88.416 N/A 83. 766 1.0083 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.57 0.000 0.000 U-3/4 4763.02 4767.89 81.651 30.000 U-235 4391.00 4496.66 44.729 7.000 U-238 4184.73 4205.69 29.691 42.000 55 U-238:3974-4284keV U-235:4310-4581 keV U-314:4592-4865keV 49 U-232:5000-5398keV 43 37 (j) 31 I-z 25 :::l 0 19 2-13 *:;; t5 7 <i: 2387 2785 3186 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -1.440 1.440 1.2000 100.000 -2.48E-02 29.280 0.720 0.8485 100.000 4.95E-01 6.280 0.720 0.8485 99.700 1.07E-01 41.280 0.720 0.8485 100.000 6.98E-01 5674 6102 6533 6968 7407 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 4.01E-02 1.27E-01 3.78E-02 4.00E-02 2.04E-01 1.03E-01 2.63E-02 1.85E-01 9.71E-02 1.04E-01 2.64E-02 9.54E-02 2.49E-01 1.03E-01 2.63E-02 2.18E-01 NOTES:

Results are a compilation of S0405235040_UU and T0405235040_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

BATCH NUMBER : 1596396 SAMPLE ID : S0405235040 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 156 DETECTOR S/N : 75554 AVERAGE %EFFICIENCY : 25.9446 AVERAGE %EFF ERROR : 0.5027 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 83.8 +/-7.198 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6549E+OO dpm 3.8993E+OO dpm NUCLIDE LIBRARY PEAK en I-z :J 0 s. *:;; ENERGY ENERGY U-232 5302.10 5308.13 U-3/4 4763.02 4751.40 U-235 4391.00 4488.99 U-238 4184.73 4190.48 23 U-238:3974-4284keV U-235: 4310-4581 keV 21 U.314:45924865keV U-232:5000-5398keV 19 17 15 13 11 9 7 5 3 2394 2791 3191 3596 Energy (keV) PEAK FWHM 65.992 67.843 177.624 23.437 COUNT DATE : 24-Sep-2016 13:20:25 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 242.000 240.800 1.200 1.0954 100.000 4.07E+OO 30.000 29.280 0.720 0.8485 100.000 4.91E-01 7.000 6.280 0.720 0.8485 99.700 1.06E-01 42.000 41.280 0.720 0.8485 100.000 6.92E-01 6107 6539 6975 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B156.CNF;1100 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W156.CNF;299 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.88E-01 1.19E-01 3.39E-02 1.97E-01 1.02E-01 2.61E-02 9.58E-02 1.03E-01 2.61E-02 2.39E-01 1.02E-01 2.61E-02 1.96-sigma cnt Unc pCi/G 5.17E-01 1.84E-01 9.46E-02 2.16E-01 BATCH NUMBER : 1596396 SAMPLE ID : T1203621709 UU SAMPLE QTY : 0.518 G -+/-0.193 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 132 DETECTOR S/N : 67579 AVERAGE %EFFICIENCY : 26.0712 AVERAGE %EFF ERROR : 0.5050 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B132.CNF;1158 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 CORRECTED% YIELD : 86.4 +/-8.358 % COUNT DATE : 24-Sep-2016 13:49:58 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W132.CNF;324 CAL DATE : 08-Sep-2016 SECONDARY QTY : 0.520 G +/-0.192 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 1.0624E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 662.76 2.04 PEAK NETZ 0.52 256.80 RECOVERY YIELD CORR. NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5313.47 133.380 U-3/4 4763.02 4597.65 4.940 U-235 4391.00 4492.36 44.712 U-238 4184.73 4080.83 4.940 u 238* 3974-4284 k v -* . 64 _ U-235:4310-4581 keV U-314: 45924865 keV 57 -U*232;5000-539SkeV 50 r;J 36 1--f-z 29 :::> r 0 22 8. f-.2:-15 *;;; f-n 8 <!'. 1 r JI .. I I I 23 82 2780 3180 3585 3! 94 1406 Energy (keV) 11.1230 dpm 4492.36 4357.21 4.6171 dpm 5313.47 5307.13 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 3.000 2.040 0.960 0.9798 100.000 0.000 -0.720 0.720 0.8485 100.000 1.000 0.520 0.480 0.6928 99.700 2.000 1.520 0.480 0.6928 100.000 I I I I 48 2 5241 5665 6092 6523 6958 '--ACTIVITY pCi/G 2.97E-02 -1.13E-02 8.21E-03 2.39E-02 7396 1.96-sigma TPU pCi/G 5.92E-02 3.43E-02 4.57E-02 5.51E-02 NOTES: MDA pCi/G 9.58E-02 9.62E-02 8.75E-02 8.72E-02 95.227 N/A 87.060 1.0075 Le pCi/G 2.61E-02 2.45E-02 2.00E-02 2.00E-02 1.96-sigma cnt Unc pCi/G 5.90E-02 3.42E-02 4.56E-02 5.50E-02 *Results are a compilation of S1203621709_UU and T1203621709_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000)

Alpha Spectroscopy Software Version 3.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596396 SAMPLE ID : S1203621709 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 127 DETECTOR S/N : 78770 AVERAGE %EFFICIENCY : 26.6218 AVERAGE %EFF ERROR : 0.5155 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 87.1 +/-7.012 % TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE U-232 U-3/4 U-235 1564-1 U-232 4.6171E+OO dpm 4.0197E+OO dpm LIBRARY PEAK ENERGY ENERGY 5302.10 5307.13 4763.02 4728.17 4391.00 4357.21 PEAK FWHM 34.811 0.000 4.958 U-238 4184.73 4098.15 163.622 U 238* 3974-4284 keV 28 -u-235:4310-4581keV U-3/4;4592-4865keV 25 1-U-232: 5000-5398 keV 22 >--19 >--00 16 -I-z 13 :::> >--0 10 *:;; u 4 >--<I'. -I I I I I I I I II I 23 82 2781 3183 3590 4(00 414 Energy (keV) COUNT DATE : 24-Sep-2016 13:49:22 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 258.000 256.800 1.200 1.0954 100.000 4.02E+OO 0.000 -0.720 0.720 0.8485 100.000 -1.13E-02 1.000 0.520 0.480 0.6928 99.700 8.15E-03 2.000 1.520 0.480 0.6928 100.000 2.38E-02 ill,I I I I I I 48 3 5255 5681 6111 6545 6982 7424 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B127.CNF;1167 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W127.CNF;322 CAL DATE : 08-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.56E-01 1.10E-01 3.14E-02 3.41E-02 9.55E-02 2.43E-02 4.54E-02 8.68E-02 1.99E-02 5.47E-02 8.66E-02 1.98E-02 1.96-sigma cnt Unc pCi/G 4.94E-01 3.40E-02 4.53E-02 5.46E-02 BATCH NUMBER : 1596396 SAMPLE ID : T1203621710 UU SAMPLE QTY : 0.508 G -+/-0.197 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 78.7 +/-8.778 % SECONDARY QTY : 0.505 G +/-0.198 % TRACER ID : 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RES UL TS : 9.6794E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 157 DETECTOR SIN : 75555 AVERAGE %EFFICIENCY : 26.0007 AVERAGE %EFF ERROR : 0.5038 COUNT DATE : 29-Sep-2016 14:04:04 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B157.CNF;1100 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W157.CNF;284 CAL DATE : 09-Sep-2016 TRACER CORRECTION TRACER 1 TRACER2 ID 1570-E 1564-1 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 11.1230 dpm 4482.78 4469.01 4.6539 dpm 5198.56 5292.21 PEAK NET 1 602.20 -0.24 PEAKNET2 2.76 224.56 RECOVERY YIELD CORR. 86.761 N/A 79.332 1.0082 NUCLIDE LIBRARY PEAK PEAK GROSS ENERGY ENERGY FWHM AREA U-232 5302.10 5198.56 0.000 0.000 U-3/4 4763.02 4768.06 69.292 29.000 U-235 4391.00 4482.78 47.868 3.000 U-238 4184.73 4187.62 32.666 55.000 55 U-238:3974-42114keV U-235:431Cl-4581 keV U-314:4592-4865keV 49 U-232:5000-5398keV 43 37 0' 31 z 25 ::l 0 19 s .?;-13 *;;; u <l: 7 2383 2781 3182 3588 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -0.240 0.240 0.4899 100.000 -3.99E-03 28.280 0.720 0.8485 100.000 5.20E-01 2.760 0.240 0.4899 99.700 5.09E-02 54.520 0.480 0.6928 100.000 1.00E+OO 5672 6101 6533 6969 7408 1.96-sigma TPU pCi/G 3.45E-02 2.18E-01 7.38E-02 3.23E-01 NOTES: MDA pCi/G 7.96E-02 1.12E-01 8.84E-02 1.02E-01 Le pCi/G 1.49E-02 2.86E-02 1.65E-02 2.33E-02 1.96-sigma cnt Unc pCi/G 3.44E-02 1.98E-01 7.33E-02 2.70E-01 *Results are a compilation of S1203621710_UU and T1203621710_UU. *The following nuclide results were quantified from the U-235 traced sample: U-232

Correction made to the following net area due to tracer impurity: U-238 (0.009 +/-0.000)

AlphaSpectroscopySoftwareVerslonJ.5.3 effectivedate:02-Mar-2015 BATCH NUMBER : 1596396 SAMPLE ID : S1203621710 UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 159 DETECTOR S/N : 76225 AVERAGE %EFFICIENCY : 25.5501 AVERAGE %EFF ERROR : 0.4952 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 79.3 +/-7.412 % TRACER 1564-1 ID NUCLIDE NOMINAL RESULTS U-232 4.6539E+OO dpm 3.6920E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY U-232 5302.10 5292.21 U-3/4 4763.02 4756.78 U-235 4391.00 4469.01 U-238 4184.73 4189.53 U-238:3974-4284keV 15 U-235;4310-4581 keV U-J/4:4592-4865keV U-232:5000-539BkeV 13 11 Cii 9 I-z 7 :J 0 8 5 *s; 3 t5 <( PEAK FWHM 84.447 92.694 82.937 16.262 'i >> .... 2394 2786 3183 3585 3 91 402 Energy (keV) COUNT DATE : 28-Sep-2016 17:55:29 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 226.000 224.560 1.440 1.2000 100.000 4.13E+OO 29.000 28.280 0.720 0.8485 100.000 5.15E-01 3.000 2.760 0.240 0.4899 99.700 5.05E-02 55.000 54.520 0.480 0.6928 100.000 9.94E-01 'i 'i i 4817 5237 5661 6090 6523 6960 7403 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B159.CNF;1074 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W159.CNF;278 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.24E-01 1.36E-01 4.04E-02 2.11E-01 1.11E-01 2.83E-02 7.31E-02 8.77E-02 1.64E-02 3.07E-01 1.01E-01 2.31E-02 1.96-sigma cnt Unc pCi/G 5.43E-01 1.96E-01 7.27E-02 2.68E-01 BATCH NUMBER : 1596396 SAMPLE ID : T1203621711_UU SAMPLE QTY : 0.518 G +/-0.193 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 115 DETECTOR S/N : 79995 AVERAGE %EFFICIENCY : 25.2291 AVERAGE %EFF ERROR : 0.4892 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B115.CNF;1179 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 CORRECTED % YIELD : 97.5 +/-8.244 % SECONDARY QTY : 0.520 G +/-0.192 % COUNT DATE : 25-Sep-2016 15:54:46 ELAPSED LIVE TIME(SEC) : 14400.00 EFF FILE : W115.CNF;335 CAL DATE : 08-Sep-2016 TRACER ID 1570-E NUCLIDE : U-235 NOMINAL : 1.1123E+01 dpm RESULTS : 1.0412E+01 dpm TRACER CORRECTION TRACER 1 TRACER2 NUCLIDE LIBRARY ENERGY U-232 5302.10 U-3/4 4763.02 U-235 4391.00 U-238 4184.73 U 238* 3974-4284 keV 64 U-235:4310-4581 keV U-314:4592-4865keV 57 _U-232:S000-5398keV 50 43 Cii 36 -z 29 :l -0 22 s. f-a 15 f-0 8 <( -1 I I ID 1570-E 1564-1 PEAK ENERGY 5355.02 4728.19 4491.00 4087.52 LCS ID NUCLIDE NOMINAL (pCi/G) % RECOVERY 1600-E U-238 5.1996E+OO 96.877 NUCLIDE U-235 U-232 NOMINAL PEAK ENERGY 1 PEAK ENERGY 2 PEAK NET 1 628.57 0.56 PEAK NET2 20.00 273.60 RECOVERY YIELD CORR. 11.1230 dpm 4491.00 4452. 79 4.6171 dpm 5355.02 5313.00 NUCLIDE ACTIVITY SUMMARY PEAK GROSS NET BKG BKG %ABUN FWHM AREA AREA AREA S!Dev 59.717 2.000 0.560 1.440 1.2000 100.000 0.000 326.000 325.040 0.960 0.9798 100.000 48.894 20.000 20.000 0.000 0.0000 99.700 159.246 343.000 342.520 0.480 0.6928 100.000 ,11 I' I I I I I I I ACTIVITY pCi/G 8.59E-03 4.78E+OO 2.95E-01 5.04E+OO I 1.96-sigma TPU pCi/G 5.55E-02 9.50E-01 1.41E-01 9.93E-01 NOTES: MDA pCi/G 1.13E-01 9.69E-02 4.43E-02 8.14E-02 93.330 N/A 97.710 1.0022 Le pCi/G 3.37E-02 2.64E-02 O.OOE+OO 1.87E-02 1.96-sigma cnt Unc pCi/G 5.54E-02 5.21E-01 1.33E-01 5.35E-01 *Results are a compilation of S1203621711_UU and T1203621711_UU.

The following nuclide results were quantified from the U-235 traced sample: U-232
Correction made to the following net area due to tracer impurity: U-238 (0.010 +/-0.000) 23 82 2782 3186 3593 4004 418 48 6 5257 5682 6111 6543 6978 7417 -Energy (keV)

BATCH NUMBER : 1596396 SAMPLE ID : S1203621711_UU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G +/-0.193 % CHAMBER : 158 DETECTOR SIN : 80007 AVERAGE %EFFICIENCY : 25.2718 AVERAGE %EFF ERROR : 0.4900 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 97.7 +/-6.851 % TRACER ID 1564-1 NUCLIDE U-232 NOMINAL 4.6171 E+OO dpm RESULTS 4.5114E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM U-232 5302.10 5313.00 20.214 U-3/4 4763.02 4767.13 51.908 U-235 4391.00 4452.79 158.196 U-238 4184.73 4196.02 40.476 U-238 3974-42S4k v 34 lJ.235;431Q-4581keV 31 t-U-314: 4592-4865 keV U-232:50Q0..5398keV 28 25 22 en 19 r-1--16 z -:::> 13 0 -f2, 10 -a *:;: 7 -u 4 <t: r-J h ""I n I ' ' I ' 23 86 2784 3186 3591 4( 01 415 Energy (keV) COUNT DATE : 24-Sep-2016 13:20:30 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 1600-E NUCLIDE U-238 NOMINAL (pCi/G) 5.1996E+OO % RECOVERY 96.661 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 276.000 273.600 2.400 1.5492 100.000 4.02E+OO 326.000 325.040 0.960 0.9798 100.000 4.77E+OO 20.000 20.000 0.000 0.0000 99.700 2.94E-01 343.000 342.520 0.480 0.6928 100.000 5.03E+OO ,I.I ',,ii ' '" I I I I I I 48 3 5255 5681 6111 6546 6984 7426 -Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-011 LIB FILE : U236 BKG FILE : B158.CNF;1105 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W158.CNF;286 CAL DATE : 09-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.37E-01 1.27E-01 4.16E-02 8.45E-01 9.67E-02 2.63E-02 1.39E-01 4.42E-02 O.OOE+OO 8.81E-01 8.13E-02 1.86E-02 1.96-sigma cnt Unc pCi/G 4.79E-01 5.20E-01 1.32E-01 5.34E-01 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 19-Sep-2016 Batch# 1 Sq lplf.(--;r Product: -"lh Date: Criteria: Yes No Comments Samole Solids are less than or eaual to 100 mo for GAB. l\j;}. Samples have been blank corrected (if required). f\Jr Blank correction reoorted Included flf reoulred). If activity less than lOx MDA/MDC, error Is less than or eaual to 150% of samole activity. If greater than 10* MDA/ MDC, error Is 400/o or less. rf hnlnw *ha Mntt,/ Mnr Mrnr le nll:.u ./ Instrument source check Is within limits. In.:trument hko char" Is within limits. ./ Method RDL/ LLD has been met. .,/ If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, ./ Or meets the client's reaulred RER accentance criteria. Tracer yield Is 15-1250/o

carrier yield 25-125%. (Or meets the client's contract acceptance criteria). v Method blank is less than the RDL/ LLD. -../ llf ----*--< '10/,, nf ln ... .. vltv\ Samale was run within hold time. x ,/ I\. t... 'P-Sam1>le was correctlv Preserved If reoulred. Smears Taken for Radioactive batches. /\..&-Method Spike and LCS are within 75-125% v Ir or mo*>>c the client's contract arrontance criteria\ No blank spaces on data forms. All tine outs Initialed and dated. r **-Aux data Is correct. k-0.. Client Soeclal reaulrements oaoe has been checked. v Raw Data and/ orsoectrum are Included and orooerlv statused. /" MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ../ verified IUI* .. (If ,, kb, ln-*rh --*-*--' ln*n v Batch Data Exceotlon Reoorts <DER\ comoleted If aoollcable. . ,,... Batch Data Exception Reports (DER) second reviewed. v Dlsoosltlon verified to be comoleted. Alfnnn* Corrnr*ion comoln*od If r"""lr.,d. Review sample historical results If available / (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. \ Primary Review Performed By: __ ___ _,_i.J;-___ 1_l_tt_l_l_i,.. __ '----Secondary Review Performed By:__ 09/30/16 Q.\ GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA .EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER DOE EML HASL-300, Th-01-RC Solid Batch ID: Sample Numbers: 1596417 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075,405235076,405235077,405235078, and 1203621758were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 21-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 902 of 5809 DER Report No.: 1559853 Revision No.: 1 Type: Process Client Code: MJWC I Thorium (Ac-227 Tracer) Queue Sheet 07-SEP-16 Batch#: 1596417 Analyst: KXB2 First Client Due Date:04-0CT-16 Internal Due Date.30-SEP-16 . c,.*\u* iv Tracer Isotope: Ac-227 Tracer Code:03<Q'1* Pr'=\01.-Expiration Date: TS-:O\-\ 1 LCS Isotope: LCS Code: "\1.1.\J..-H Expiration Date: 1.,.-\\-\l Ac-227 Separation Date/I'ime: C\ /I \J ( i U I LI 00 Vol:__Qj_ Vol: Spike Th-23::Spike Code:. _. Expiration Date: -Prep Date: q .. \\j) Initials: ¥f, Pipet ID: \<()'-\001..9;;. Balance ID:.____.."""'1-""-'"===-I tot D1<otv'!L< Hazard Sample ID Client Description Type Code --------405235061-1 5.lB.R.2.2 SAl'tfi'LE 405235062-1 5.2A.R.l.2 SAMPLE 405235063-1 5.2A.R.1.3 SAMPLE 405235064-1 5.2A.R.1.4 SAMPLE 405235065-1 5.2A.R.2.3 SAMPLE 405235066-1 5.2A.R.2.4 SAMPLE 405235067-1 5.2A.R.6.2 SAMPLE 405235068-1 5.2A.R.4.2 SAJ\.IPLE 405235069-1 5.2B.R.1.4 SAMPLE 405235070-1 5.2B.R.3.2 SAMPLE 405235071-1 5.2B.R.4.2 SAMPLE 405235072-1 5.2B.R.2.4 SAMPLE 405235073-1 5.2B.R.8.2 SAMPLE 405235074-1 5.3A.R.1.3 SAMPLE 405235075-1 5.4A.R.l.3 SMIPLE 405235076-1 5.4A.R.4.2 SAJ\<IPLE 405235077-1 5.SA.R.1.3 SAMPLE 405235078-1 5.6A.R.1.3 SAMPLE 1203621757-1 l'vIB for batch 1596417 MB 1203621758-1 5.1B.R.2.2(405235061DUP) DUP 1203621759-1 LCS for batch 1596417 LCS GEL Laboratories LLC,. Radiochemistry Division Min CRDL Matrix 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCilg SOIL I pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL 1 pCi/g SOIL Client MJWCOOl MJWCOOl MJWCOOl MJWCOOl JVJJWCOOl MJWCOOl MJWCOOI MJWCOOl MJWCOOl l'vJJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl 1\1.JWCOOl MJ\'l'COOl MJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Collection Date 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 11-DEC-15 11-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 ll-DEC-15 15-DEC-15 16-DEC-15 11-DEC-15 17-DEC-15 17-DEC-15 14-DEC-15 1 2 3 4 5 6 7 8 9 IO 11 12 13 14 15 16 17 18 19 20 21 Page 1 ofi BATCH NUMBER : 1596417 SAMPLE ID : S0405235061 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 161 DETECTOR SIN : 70321 AVERAGE %EFFICIENCY : 25.7727 AVERAGE %EFF ERROR : 0.4995 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 104 +/-7.501 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.3550E+OO dpm NUCLIDE LIBRARY PEAK en I-z :l 0 c *;; :g <{ ENERGY ENERGY AC-227 5854.62 5858.99 TH-228 5363.00 5401.63 TH-229 4900.00 4958.11 TH-230 4671.39 4668.84 TH-232 3972.00 3989.92 11 TH*232:3796-4085keV TH-230: 4495-4745 keV 10 TH-229: 4n5-5142 keV TH-228:5211-5493keV 9 AC-227: 5510-S128 keV 8 7 6 5 4 3 2 1 2394 2792 3193 3599 Energy (keV) PEAK FWHM 271.304 153.265 0.000 9.888 4.944 COUNT DATE : 19-Sep-2016 17:41:44 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 208.000 207.520 0.480 0.6928 100.000 1.49E+01 8.000 5.799 0.960 0.9798 99.940 4.91E-01 0.000 0.000 0.000 0.0000 99.469 O.OOE+OO 11.000 11.000 0.000 0.0000 99.700 7.07E-01 14.000 13.280 0.720 0.8485 100.000 8.50E-01 ll ll g f;l Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B161.CNF;858 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W161.CNF;261 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.06E+OO 5.14E-01 1.30E-01 4.50E-01 5.07E-01 NOTES: MDA pCi/G 3.99E-01 6.89E-01 1.93E-01 1.93E-01 3.91E-01 Le pCi/G 9.14E-02 2.17E-01 O.OOE+OO O.OOE+OO 9.95E-02 1.96-sigma cnt Unc pCi/G 2.04E+OO 5.06E-01 1.30E-01 4.37E-01 4.90E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8401 E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.241 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235062 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 162 DETECTOR S/N : 70323 AVERAGE %EFFICIENCY : 26.6669 AVERAGE %EFF ERROR : 0.5165 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 98.5 +/-7.591 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.1687E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5863.03 TH-228 5363.00 5412.18 TH-229 4900.00 4980.29 TH-230 4671.39 4662.63 TH-232 3972.00 4027.34 7 TH-232: 37964085 keV TH-230: 4495-4745 bV TH-229: 4n5-S142 keV 6 TH-228:5211-549JkeV AC.227: 5510-6126 keV 5 en 4 1--z 3 ::i 0 s c 2 0 <( 2383 2782 3184 3590 Energy (keV) PEAK FWHM 354.910 4.961 213.318 24.804 4.961 i COUNT DATE: 19-Sep-201617:41:46 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCifG 204.000 202.800 1.200 1.0954 100.000 1.58E+01 4.000 2.547 0.240 0.4899 99.940 2.34E-01 3.000 2.520 0.480 0.6928 99.469 1.76E-01 13.000 12.520 0.480 0.6928 99.700 8.71E-01 6.000 5.760 0.240 0.4899 100.000 3.99E-01 'i 'i g :;i Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B162.CNF;860 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W162.CNF;260 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCifG 3.28E+OO 4.10E-01 2.80E-01 5.31E-01 3.68E-01 NOTES: MDA pCifG 5.47E-01 6.46E-01 3.86E-01 3.85E-01 3.33E-01 Le pCifG 1.56E-01 1.85E-01 8.85E-02 8.83E-02 6.22E-02 1.96-sigma cnt Unc pCifG 2.19E+OO 4.07E-01 2.79E-01 5.13E-01 3.63E-01

Ac-227 results are decay corrected to separation dateftime.
Ac-227 Tracer nominal includes 4.8402E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.213 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235063 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.118G -+/-0.847% CHAMBER : 188 DETECTOR S/N : 68621 AVERAGE %EFFICIENCY : 26.7276 AVERAGE %EFF ERROR : 0.5175 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 110 +/-7.230 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2164E+OO dpm 3.5276E+OO dpm NUCLIDE LIBRARY PEAK 00 I-z :::> 0 -2:-*:;: u <( ENERGY ENERGY AC-227 5854.52 5868.29 TH-228 5363.00 5429.85 TH-229 4900.00 4879.94 TH-230 4671.39 4689.90 TH-232 3972.00 4001.92 7 TH-232: 3796-4085 keV TH-230: 4495-4745 keV TH-229: 4IT5-5142 keV 6 TH-228:5211-5493keV AC-227:551o-6128kaV 5 4 3 2 2429 2820 3215 3615 Energy (keV) PEAK FWHM 389.460 38.885 126.377 4.861 131.238 :i ¥ COUNT DATE : 19-Sep-2016 18:03:46 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 227.000 226.280 0.720 0.8485 100.000 1.38E+01 21.000 19.641 0.000 0.0000 99.940 1.41E+OO 2.000 1.520 0.480 0.6928 99.469 8.29E-02 6.000 5.040 0.960 0.9798 99.700 2.74E-01 7.000 7.000 0.000 0.0000 100.000 3.80E-01 :i :i :i a 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B188.CNF;852 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W188.CNF;233 CAL DATE : 15-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCl/G pCi/G 2.72E+OO 3.73E-01 9.49E-02 6.97E-01 4.90E-01 1.38E-01 1.91E-01 3.02E-01 6.92E-02 2.91E-01 3.59E-01 9.77E-02 3.07E-01 1.63E-01 O.OOE+OO NOTES: 1.96-sigma cnt Unc pCi/G 1.81E+OO 6.60E-01 1.90E-01 2.88E-01 3.02E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8600E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.359 +/-0.009)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235064 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 69.8 +/-8.827 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 2.2449E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5898.94 TH-228 5363.00 5413.38 TH-229 4900.00 4971.89 TH-230 4671.39 4671.02 TH-232 3972.00 4022.46 7 TH-232:3795-4085keV TH-230:44954745keV TH-229: 4nS-5142 keV 6 TH-228: 5211-5493 keV AC-227: 5510-0128 keV 5 (ii 4 I-z 3 ::::> 0 2 a t) <!'. PEAK FWHM 321.570 81.724 9.906 99.059 89.153 2383 2781 3184 3590 400 441 Energy (keV) COUNT DATE : 19-Sep-201617:41:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 144.000 143.760 0.240 0.4899 100.000 1.55E+01 18.000 17.140 0.000 0.0000 99.940 2.18E+OO 2.000 1.520 0.480 0.6928 99.469 1.47E-01 5.000 5.000 0.000 0.0000 99.700 4.81E-01 15.000 15.000 0.000 0.0000 100.000 1.44E+OO Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B166.CNF;889 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.76E+OO 1.16E+OO 3.38E-01 4.72E-01 7.96E-01 NOTES: MDA pCi/G 5.17E-01 7.68E-01 5.34E-01 2.89E-01 2.88E-01 Le pCi/G 9.68E-02 1.94E-01 1.22E-01 O.OOE+OO O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.55E+OO 1.09E+OO 3.37E-01 4.64E-01 7.54E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8403E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.860 +/-0.006)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235065 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 167 DETECTOR S/N : 72546 SAMPLE QTY : 0.113 G -+/-0.885 % AVERAGE %EFFICIENCY : 24.1606 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 114 +/-7.458 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.6575E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5875.10 TH-228 5363.00 5395.49 TH-229 4900.00 4958.17 TH-230 4671.39 4647.35 TH-232 3972.00 4012.27 8 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 7 TH-228:5211-5493keV AC.227: 5510-6128 keV 6 5 0' 4 z => 3 0 8 2 *s; u <( 2378 2780 3185 3594 Energy (keV) PEAK FWHM 365.098 107.529 0.000 5.001 17.505 AVERAGE %EFF ERROR : 0.4690 COUNTDATE: 19-Sep-201617:41:54 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 214.000 212.080 1.920 1.3856 100.000 1.44E+01 16.000 14.252 0.480 0.6928 99.940 1.14E+OO 0.000 -0.480 0.480 0.6928 99.469 -2.92E-02 14.000 13.520 0.480 0.6928 99.700 8.20E-01 10.000 10.000 0.000 0.0000 100.000 6.04E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B167.CNF;884 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W167.CNF;246 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.94E+OO 6.76E-01 1.29E-01 4.79E-01 4.05E-01 NOTES: MDA pCi/G 5.49E-01 5.99E-01 3.37E-01 3.36E-01 1.81E-01 Le pCi/G 1.72E-01 1.79E-01 7.71E-02 7.69E-02 O.OOE+OO 1.96-sigma en! Unc pCl/G 1.96E+OO 6.49E-01 1.29E-01 4.63E-01 3.94E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8403E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.268 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235066 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.6 +/-8.109 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER . ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 2.7852E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5893.07 TH-228 5363.00 5456.44 TH-229 4900.00 4958.11 TH-230 4671.39 4709.77 TH-232 3972.00 4038.86 6 TH-232: 37964085 keV TH-230: 44954745 keV TH-229:4n5-5142keV TH-228:5211-5493keV 5 AC:,'12.7: 5510-6128 keV 4 (ii 3 1--z ::> 0 2 f2. *:;;: u <( 2402 2798 3198 3603 Energy (keV) PEAK FWHM 423.911 14.788 0.000 0.000 17.252 !!; 401 442 ; COUNT DATE : 19-Sep-2016 17:41:55 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 177.000 175.320 1.680 1.2961 100.000 1.55E+01 7.000 4.511 1.440 1.2000 99.940 4.69E-01 0.000 0.000 0.000 0.0000 99.469 O.OOE+OO 7.000 6.520 0.480 0.6928 99.700 5.15E-01 11.000 10.520 0.480 0.6928 100.000 8.28E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B169.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.45E+OO 5.99E-01 1.60E-01 4.50E-01 5.55E-01 NOTES: MDA pCi/G 6.85E-01 8.89E-01 2.37E-01 4.37E-01 4.36E-01 Le pCi/G 2.10E-01 2.88E-01 O.OOE+OO 1.00E-01 9.99E-02 1.96-sigma cnt Unc pCi/G 2.32E+OO 5.91E-01 1.59E-01 4.42E-01 . 5.38E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8403E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.049 +/-0.007)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235067 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 170 DETECTOR S/N : 72549 SAMPLE QTY : 0.106 G -+/-0.943 % AVERAGE %EFFICIENCY : 25.7306 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 105 +/-7.555 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.3708E+OO dpm NUCLIDE LIBRARY PEAK (j) I-z =i 0 c t5 <{ ENERGY ENERGY AC-227 5854.62 5879.23 TH-228 5363.00 5418.06 TH-229 4900.00 4958.11 TH-230 4671.39 4674.56 TH-232 3972.00 4000.80 9 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4nS..5142 keV 8 TH-228: 5211-5493 keV AC-227:5510-6128keV 7 6 5 4 3 2 2386 2785 3187 3593 Energy (keV) PEAK FWHM 324.977 56.985 0.000 69.373 42.119 AVERAGE o/oEFF ERROR : 0.4988 COUNTDATE: 19-Sep-201617:41:58 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 212.000 208.160 3.840 1.9596 100.000 1.54E+01 18.000 14.115 2.640 1.6248 99.940 1.23E+OO 0.000 -0.480 0.480 0.6928 99.469 -3.17E-02 16.000 15.040 0.960 0.9798 99.700 9.90E-01 13.000 13.000 0.000 0.0000 100.000 8.53E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B170.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.17E+OO 7.85E-01 1.40E-01 5.58E-01 5.00E-01 NOTES: MDA pCi/G 7.51E-01 8.70E-01 3.66E-01 4.34E-01 1.97E-01 Le pCi/G 2.65E-01 3.04E-01 8.38E-02 1.18E-01 O.OOE+OO 1.96-sigma cnt Unc pCl/G 2.12E+OO 7.57E-01 1.40E-01 5.37E-01 4.82E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8404E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.245 +/-0.008) 0 ....., V\ 00 0 \0 Alpha Speciltlscopy Software Version 3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596417 SAMPLE ID : S0405235068 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.100 G -+/-1.000 % CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 93.6 +/-7.816 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.0103E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5888.19 TH-228 5363.00 5389.48 TH-229 4900.00 5055.31 TH-230 4671.39 4652.23 TH-232 3972.00 3980.29' 9 TH-232:37964085keV TH-230: 4495-4745 keV TH-229: 477S.5142 keV 8 TH-228: 5211-5493 keV AC-227:551()..6128keV 7 6 5 z 4 :::i 0 3 s 2 *:;: u 1 <( 2363 2764 3168 3575 Energy (keV) PEAK FWHM 338.808 4.982 4.982 6.643 7.474 'li COUNT DATE : 19-Sep-2016 17:42:00 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA Stoev pCi/G 191.000 189.800 1.200 1.0954 100.000 1.63E+01 11.000 9.625 0.240 0.4899 99.940 9.74E-01 1.000 0.760 0.240 0.4899 99.469 5.83E-02 13.000 12.520 0.480 0.6928 99.700 9.58E-01 7.000 6.520 0.480 0.6928 100.000 4.98E-01 ll 'li 'li 'li Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B175.CNF;868 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DA TE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.49E+OO 7.12E-01 2.19E-01 5.85E-01 4.35E-01 NOTES: MDA pCi/G 6.02E-01 7.02E-01 3.68E-01 4.24E-01 4.23E-01 Le pCi/G 1.72E-01 1.99E-01 6.89E-02 9.72E-02 9.69E-02 1.96-sigma cnt Unc pCi/G 2.33E+OO 6.91E-01 2.19E-01 5.65E-01 4.28E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8404E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.135 +/-0.007)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235069 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.116 G -+/-0.862 % CHAMBER : 176 DETECTOR S/N : 74434 AVERAGE %EFFICIENCY : 25.6995 AVERAGE %EFF ERROR : 0.4981 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 96.3 +/-7.788 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.0973E+OO dpm NUCLIDE LIBRARY PEAK '(ii I-z :::> 0 s *:;; ENERGY ENERGY AC-227 5854.62 5878.01 TH-228 5363.00 5386.00 TH-229 4900.00 5011.43 TH-230 4671.39 4659.20 TH-232 3972.00 4009.64 7 TH*232: 37964085 keV TH-230:4495-4745keV TH-229:4nS.5142keV 6 TH-228: 5211-5493 keV AC-227: 5510-6128 keV 5 4 3 2 2379 2776 3177 3582 Energy {keV) PEAK FWHM 371.340 148.043 0.000 56.750 5.757 COUNT DATE : 19-Sep-2016 17:42:03 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 192.000 191.040 0.960 0.9798 100.000 1.40E+01 19.000 17.617 0.240 0.4899 99.940 1.52E+OO 3.000 2.520 0.480 0.6928 99.469 1.66E-01 15.000 13.560 1.440 1.2000 99.700 8.89E-01 12.000 12.000 0.000 0.0000 100.000 7.84E-01 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B176.CNF;863 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.99E+OO 8.00E-01 2.64E-01 5.39E-01 4.79E-01 NOTES: MDA pCi/G 4.84E-01 5.99E-01 3.64E-01 4.85E-01 1.96E-01 Le pCi/G 1.32E-01 1.?0E-01 8.34E-02 1.44E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.00E+OO 7.58E-01 2.63E-01 5.20E-01 4.63E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8404E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.143 +/-0.007)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235070 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 93.6 +/-7.790 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2160E+OO dpm 3.0095E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5896.17 TH-228 5363.00 5406.23 TH-229 4900.00 4999.77 TH-230 4671.39 4657.33 TH-232 3972.00 4005.09 9 TH-232:3796-4065keV TH-230; 4495-4745 keV TH-229: 4n5-S142 keV 8 TH-228: 5211-5493 keV AC.227;551().6128keV 7 6 0' 5 z 4 :::J 0 3 2 *:;; ti <t: 2375 2774 3177 3583 Energy (keV) PEAK FWHM 279.454 9.910 153.612 104.060 70.612 399 COUNT DATE : 19-Sep-2016 17:42:05 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 194.000* 192.080 1.920 1.3856 100.000 1.54E+01 11.000 8.411 1.440 1.2000 99.940 7.94E-01 3.000 2.520 0.480 0.6928 99.469 1.80E-01 6.000 6.000 0.000 0.0000 99.700 4.28E-01 18.000 18.000 0.000 0.0000 100.000 1.28E+OO >> l!.: Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B177.CNF;875 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.28E+OO 6.67E-01 2.88E-01 3.78E-01 6.42E-01 NOTES: MDA pCi/G 6.46E-01 8.15E-01 3.96E-01 2.14E-01 2.13E-01 Le pCi/G 2.03E-01 2.66E-01 9.08E-02 O.OOE+OO O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.19E+OO 6.51E-01 2.86E-01 3.72E-01 6.09E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8405E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.149 +/-0.007)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235071 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.115 G -+/-0.870 % CHAMBER : 195 DETECTOR S/N : 78786 AVERAGE %EFFICIENCY : 26.3844 AVERAGE o/oEFF ERROR : 0.5110 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 %YIELD: 116 +/-7.105% AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 ' AC-227 3.2161E+OO dpm 3.7440E+OO dpm NUCLIDE LIBRARY PEAK en I-z :::i 0 2.. u <! ENERGY ENERGY AC-227 5854.58 5891.29 TH-228 5363.00 5388.42 TH-229 4900.00 4958.12 TH-230 4671.39 4685.28 TH-232 3972.00 4030.48 15 TH-232:3796-408SkeV TH-230: 44954745 keV TH-229: 4775-5142 keV 13 TH*228:5211*5493keV AC.227:5510-0128keV 11 9 7 5 3 2393 2792 3195 3601 Energy (keV) PEAK FWHM 262.298 4.961 0.000 0.000 7.441 COUNT DATE : 19-Sep-2016 17:50:08 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 239.000 237.080 1.920 1.3856 100.000 1.42E+01 6.000 4.340 0.240 0.4899 99.940 3.06E-01 0.000 -0.240 0.240 0.4899 99.469 -1.28E-02 6.000 5.760 0.240 0.4899 99.700 3.07E-01 8.000 8.000 0.000 0.0000 100.000 4.25E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B195.CNF;878 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W195.CNF;259 CAL DATE : 15-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 2.75E+OO 4.83E-01 1.52E-01 3.73E-01 5.15E-01 1.52E-01 1.11E-01 2.56E-01 4.79E-02 2.82E-01 2.56E-01 4.78E-02 3.19E-01 1.59E-01 0.00E+OO NOTES: 1.96-sigma cnt Unc pCi/G 1.82E+OO 3.68E-01 1.11E-01 2.79E-01 3.13E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8477E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.420 +/-0.009)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235072 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.116 G -+/-0.862 % CHAMBER : 179 DETECTOR S/N : 74437 AVERAGE %EFFICIENCY : 26.3751 AVERAGE %EFF ERROR : 0.5108 *SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 97.2 +/-7.694 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2161E+OO dpm 3.1254E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.58 5888.05 TH-228 5363.00 5388.53 TH-229 4900.00 5096.72 TH-230 4671.39 4665.59 TH-232 3972.00 3988.17 9 TH-232:3796-4085keV TH*230: 4495-4745 keV TH-229: 4ns.5142 keV 8 TH-228; 5211-5493 keV AC-227;5510-6126keV 7 6 en 5 I-z 4 :l 0 3 s .;:. 2 *:;: n <i:: 2377 2775 3176 3582 Energy (keV) PEAK FWHM 287.562 71.643 49.409 44.468 4.941 ; COUNT DATE : 19-Sep-201617:49:57 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 200.000 197.840 2.160 1.4697 100.000 1.40E+01 15.000 13.095 0.720 0.8485 99.940 1.09E+OO 2.000 2.000 0.000 0.0000 99.469 1.27E-01 15.000 15.000 0.000 0.0000 99.700 9.50E-01 11.000 10.760 0.240 0.4899 100.000 6.79E-01 l Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B179.CNF;875 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W179.CNF;254 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.95E+OO 6.84E-01 2.18E-01 5.19E-01 4.44E-01 NOTES: MDA pCi/G 5.95E-01 6.46E-01 1.90E-01 1.90E-01 3.03E-01 Le pCi/G 1.91E-01 1.98E-01 O.OOE+OO O.OOE+OO 5.66E-02 1.96-sigma cnt Unc pCi/G 1.98E+OO 6.58E-01 2.18E-01 4.97E-01 4.31E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8476E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.185 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235073 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.118 G -. +/-0.847 % CHAMBER : 180 DETECTOR S/N : 83295 AVERAGE %EFFICIENCY : 26.2740 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 72.1 +/-8.804 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2161E+OO dpm 2.3204E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.58 5882.36 TH-228 5363.00 5408.12 TH-229 4900.00 4958.13 TH-230 4671.39 4662.91 TH-232 3972.00 3999.60 7 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4n5-5142 keV 6 TH-228:5211-5493keV AC.227: 5511J.6128 keV 5 en 4 1--z 3 :J 0 !2. .?;-2 *;; :g <I'. 2377 2777 3181 3588 Energy (keV) PEAK FWHM 333.121 24.888 0.000 34.843 4.978 COUNT DATE : 19-Sep-2016 17:49:59 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 148.000 146.320 1.680 1.2961 100.000 1.38E+01 12.000 10.884 0.240 0.4899 99.940 1.21E+OO 0.000 0.000 0.000 0.0000 99.469 O.OOE+OO 9.000 8.760 0.240 0.4899 99.700 7.37E-01 8.000 8.000 0.000 0.0000 100.000 6.71E-01 > Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B180.CNF;877 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W180.CNF;230 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.33E+OO 8.23E-01 1.71E-01 5.41E-01 5.09E-01 NOTES: MDA pCi/G 7.31E-01 7.31E-01 2.53E-01 4.04E-01 2.52E-01 Le pCi/G 2.24E-01 1.98E-01 O.OOE+OO 7.55E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.26E+OO 7.90E-01 1.70E-01 5.25E-01 4.95E-01

Ac-227 results a*re decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8476E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.876 +/-0.006)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235074 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 181 DETECTOR S/N : 74439 AVERAGE %EFFICIENCY : 26.6415 AVERAGE %EFF ERROR : 0.5158 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 106 +/-7.376 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2161E+OO dpm 3.4232E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.58 5882.18 TH-228 5363.00 5420.70 TH-229 4900.00 4958.09 TH-230 4671.39 4658.47 TH-232 3972.00 3982.31 8 TH-232:3796-4085keV TH-230: 4495-4745 keV TH-229: 4775-5142 keV 7 TH-226: 5211-5493 keV AC.227:5510-6128keV 6 5 4 z => 3 0 s. c 2 *::; ti <t: 2376 2775 3177 Energy (keV) PEAK FWHM 328.306 49.493 0.000 71.765 4.949 i > COUNT DATE : 19-Sep-2016 17:50:00 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 222.000 218.880 3.120 1.7664 100.000 1.55E+01 16.000 13.249 1.440 1.2000 99.940 1.10E+OO 0.000 -0.720 0.720 0.8485 99.469 -4.56E-02 17.000 16.520 0.480 0.6928 99.700 1.04E+OO 7.000 6.520 0.480 0.6928 100.000 4.11E-01 i >> 52 5679 61 1 6547 6987 7431 ;!; ;!; < Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B181.CNF;317 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W181.CNF;89 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.13E+OO 7.05E-01 1.38E-01 5.51E-01 3.59E-01 NOTES: MDA pCi/G 6.71E-01 7.32E-01 3.87E-01 3.50E-01 3.49E-01 Le pCl/G 2.29E-01 2.41E-01 9.85E-02 8.02E-02 8.00E-02 1.96-sigma cnt Unc pCi/G 2.08E+OO 6.81E-01 1.38E-01 5.28E-01 3.53E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8476E-01 dpm ingrowth from Ra-223. ,
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.311 +/-0.009)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235075 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G -+/-0.943 % CHAMBER : 182 DETECTOR S/N : 74440 AVERAGE %EFFICIENCY : 22.5384 AVERAGE %EFF ERROR : 0.4383 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 87.7 +/-8.631 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2161E+OO dpm 2.8204E+OO dpm NUCLIDE LIBRARY PEAK (ii f-z => 0 £ c *s: <{ ENERGY ENERGY AC-227 5854.58 5872.30 TH-228 5363.00 5405.72 TH-229 4900.00 4958.15 TH-230 4671.39 4688.45 TH-232 3972.00 3997.42 8 TH-232: 37964085 keV TH-230; 4495-4745 keV TH-229: 4775-5142 keV 7 TH-228:5211-5493keV AC-227:5510-0128keV 6 5 4 3 2 2373 2774 3178 3585 Energy (keV) PEAK FWHM 305.702 4.984 0.000 49.843 109.654 COUNT DATE : 19-Sep-2016 17:50:04 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 154.000 152.560 1.440 1.2000 100.000 1.54E+01 12.000 10.366 0.720 0.8485 99.940 1.23E+OO 0.000 -0.480 0.480 0.6928 99.469 -4.32E-02 6.000 5.760 0.240 0.4899 99.700 5.18E-01 5.000 4.760 0.240 0.4899 100.000 4.26E-01 > > *

g 6537 6972 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B182.CNF;318 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W182.CNF;95 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.64E+OO 8.74E-01 1.92E-01 4.78E-01 4.41E-01 NOTES: MDA pCi/G 7.45E-01 8.77E-01 4.99E-01 4.31E-01 4.30E-01 Le pCi/G 2.21E-01 2.61E-01 1.14E-01 8.06E-02 8.04E-02 1.96-sigma cnt Unc pCi/G 2.46E+OO 8.43E-01 1.91E-01 4.70E-01 4.34E-01
Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8477E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223 .
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (0.914 +/-0.006)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235076 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.112 G -+/-0.893 % CHAMBER : 184 DETECTOR S/N : 74442 AVERAGE %EFFICIENCY : 25.3797 AVERAGE %EFF ERROR : 0.4920 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 87.6 +/-8.183 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2161E+OO dpm 2.8166E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.58 5838.99 TH-228 5363.00 5379.75 TH-229 4900.00 4994.81 TH-230 4671.39 4650.56 TH-232 3972.00 3970.59 7 TH-232:3796-408SkeV TH-230: 4495-4745 keV TH-229: 4nS-5142 keV 6 TH-228:5211-5493kaV AC-227: 5510-6128 kaV 5 0' 4 z 3 :::> 0 s 2 *s: 2360 2763 3169 Energy (keV) PEAK FWHM 360.530 58.836 215.316 5.842 46.318 ': COUNT DATE : 19-Sep-2016 17:50:05 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 173.000 171.560 1.440 1.2000 100.000 1.45E+01 15.000 13.252 0.720 0.8485 99.940 1.33E+OO 2.000 0.560 1.440 1.2000 99.469 4.24E-02 13.000 11.320 1.680 1.2961 99.700 8.56E-01 12.000 12.000 0.000 0.0000 100.000 9.05E-01 ': ': ': g Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B184.CNF;295 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W184.CNF;85 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.26E+OO 8.24E-01 2.74E-01 5.81E-01 5.55E-01 NOTES: MDA pCi/G 6.27E-01 7.56E-01 5.61E-01 5.86E-01 2.26E-01 Le pCi/G 1.86E-01 2.28E-01 1.67E-01 1.80E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.19E+OO 7.90E-01 2.74E-01 5.64E-01 5.34E-01

Ac-227 results are decay corrected to separation date/time. /
Ac-227 Tracer nominal includes 4.8477E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.028 +/-0.007)

A!phaSpectrosc:opySoftwareVersion3.5.3 effectivedate:02--Mar-2015 BATCH NUMBER : 1596417 SAMPLE ID : S0405235077 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.117 G -+/-0.855 % CHAMBER : 205 DETECTOR S/N : 78908 AVERAGE %EFFICIENCY : 26.6171 AVERAGE %EFF ERROR : 0.5154 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 88.0 +/-7.967 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2344E+OO dpm 2.8459E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5850.09 5849.40 TH-228 5363.00 5407.10 TH-229 4900.00 5046.95 TH-230 4671.39 4643.63 TH-232 3972.00 3999.32 8 TH-232: 37964085 keV TH-230: 44954745 keV TH-229: 4nS...5142 keV 7 TH-228:5211*5493keV AC-227: 5510-6128 keV 6 5 en 4 1--z ::> 3 0 s 2 *:;: ts <( 2378 2775 3177 3582 Energy {keV) PEAK FWHM 310.732 64.289 4.945 7.418 56.871 399 440 ! COUNT DATE : 20-Sep-2016 11 :28:57 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 183.000 181.800 1.200 1.0954 100.000 1.44E+01 21.000 18.752 0.960 0.9798 99.940 1.69E+OO 1.000 0.520 0.480 0.6928 99.469 3.58E-02 9.000 8.760 0.240 0.4899 99.700 6.02E-01 11.000 10.520 0.480 0.6928 100.000 7.21E-01 ll H * ;: ;: Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B205.CNF;801 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W205.CNF;223 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.14E+OO 8.86E-01 1.99E-01 4.39E-01 4.83E-01 NOTES: MDA pCi/G 5.55E-01 7.39E-01 3.81E-01 3.29E-01 3.79E-01 Le pCi/G 1.59E-01 2.34E-01 8.74E-02 6.17E-02 8.69E-02 1.96-sigma cnt Unc pCi/G 2.11E+OO 8.36E-01 1.99E-01 4.28E-01 4.68E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7655E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.288 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S0405235078 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 207 DETECTOR S/N : 78910 AVERAGE %EFFICIENCY : 26.0138 AVERAGE %EFF ERROR : 0.5040 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 106 +/-7.418 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2159E+OO dpm 3.4245E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.62 5861.43 TH-228 5363.00 5409.00 TH-229 4900.00 4865.20 TH-230 4671.39 4593.82 TH-232 3972.00 3968.02 7 TH-232:3796-4085keV TH-230; 4495-4745 keV TH-229: 4775-5142 keV 6 TH-228: 5211-5493 keV AC.227:551o-6128keV 5 'iii 4 1--z 3 :::> 0 S?. 2 15 <l'. 2375 2773 3175 3582 Energy (keV) PEAK FWHM 356.677 63.162 4.954 104.031 23.531 COUNT DATE : 19-Sep-2016 17:41 :01 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 215.000 213.800 1.200 1.0954 100.000 1.49E+01 17.000 15.241 0.480 0.6928 99.940 1.25E+OO 1.000 0.520 0.480 0.6928 99.469 3.25E-02 6.000 5.760 0.240 0.4899 99.700 3.59E-01 14.000 13.760 0.240 0.4899 100.000 8.55E-01 :;: ::rn 7412 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B207.CNF;809 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W207.CNF;228 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.03E+OO 7.15E-01 1.81E-01 3.30E-01 4.91E-01 NOTES: MDA pCi/G 4.90E-01 6.15E-01 3.46E-01 2.99E-01 2.98E-01 Le pCi/G 1.40E-01 1.85E-01 7.93E-02 5.60E-02 5.58E-02 1.96-sigma en! Une pCi/G 2.01E+OO 6.85E-01 1.81E-01 3.26E-01 4.74E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8395E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.279 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S1203621757 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.118G -+/-0.847% CHAMBER : 207 DETECTOR S/N : 78910 AVERAGE %EFFICIENCY : 26.0138 AVERAGE %EFF ERROR : 0.5040 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 93.5 +/-7.834 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2344E+OO dpm 3.0240E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5850.09 5866.59 TH-228 5363.00 5315.53 TH-229 4900.00 5033.55 TH-230 4671.39 4619.90 TH-232 3972.00 3940.45 7 TH*232: 3796-4085 keV TH-230: 44954745 keV TH-229: 4n5-5142 keV 6 TH-228: 5211-5493 keV AC-227:5510-6128keV 5 en 4 I-z 3 ::J 0 8 2 *s: 2375 2773 3175 3582 Energy (keV) PEAK FWHM 337.894 178.338 54.492 0.000 0.000 :;; 399 COUNT DATE : 20-Sep-2016 11 :28:59 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA S!Dev pCi/G 190.000 188.800 1.200 1.0954 100.000 1.43E+01 3.000 1.183 0.480 0.6928 99.940 7.78E-02 2.000 1.520 0.480 0.6928 99.469 9.99E-02 0.000 -0.240 0.240 0.4899 99.700 -1.57E-02 0.000 -0.240 0.240 0.4899 100.000 -1.57E-02 7412 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B207.CNF;809 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W207.CNF;228 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.06E+OO 2.65E-01 2.30E-01 1.36E-01 1.36E-01 NOTES: MDA pCi/G 5.30E-01 4.98E-01 3.64E-01 3.15E-01 3.14E-01 Le pCi/G 1.52E-01 1.50E-01 8.34E-02 5.89E-02 5.87E-02 1.96-sigma cnt Unc pCi/G 2.05E+OO 2.63E-01 2.30E-01 1.36E-01 1.35E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7656E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.337 +/-0.009)

BATCH NUMBER : 1596417 SAMPLE ID : S1203621758 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 102 +/-7.668 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2163E+OO dpm 3.2651E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5854.55 5839.03 TH-228 5363.00 5402.50 TH-229 4900.00 4991.35 TH-230 4671.39 4676.74 TH-232 3972.00 4009.86 9 TH*232: 37964085 keV TH-230: 44954745 keV TH-229:4n5-5142keV 8 TH-228:5211-5493keV AC.22.7:5510-S128keV 7 6 5 z 4 ::> 0 3 f2.. 1:-2 *:;; u <t: 2416 2810 3209 3612 Energy (keV) PEAK FWHM 357.549 61.329 63.782 4.906 7.359 COUNT DATE : 19-Sep-201617:56:38 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 201.000 199.080 1.920 1.3856 *100.000 1.60E+01 16.000 14.806 0.000 0.0000 99.940 1.40E+OO 3.000 2.760 0.240 0.4899 99.469 1.98E-01 5.000 4.520 0.480 0.6928 99.700 3.23E-01 9.000 8.760 0.240 0.4899 100.000 6.25E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B189.CNF;853 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.35E+OO 7.99E-01 2.87E-01 3.52E-01 4.55E-01 NOTES: MDA pCi/G 6.48E-01 6.22E-01 3.44E-01 3.96E-01 3.42E-01 Le pCi/G 2.04E-01 1.70E-01 6.44E-02 9.08E-02 6.40E-02 1.96-sigma cnt Unc pCi/G 2.24E+OO 7.64E-01 2.85E-01 3.48E-01 4.45E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 4.8536E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.194 +/-0.008)

BATCH NUMBER : 1596417 SAMPLE ID : S1203621759 TH GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.118 G -+/-0.847 % CHAMBER : 208 DETECTOR S/N : 78911 AVERAGE %EFFICIENCY : 26.1198 AVERAGE %EFF ERROR : 0.5060 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 89.4 +/-7.988 % AC-227 SEP. : 16-Sep-2016 16:00:00 TRACER ID NUCLIDE NOMINAL RESULTS 0387-B-402 AC-227 3.2344E+OO dpm 2.8924E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY AC-227 5850.09 5803.95 TH-228 5363.00 5401.99 TH-229 4900.00 4958.11 TH-230 4671.39 4610.78 TH-232 3972.00 4018.74 TH-232:379S-40B5keV 21 TH-230: 4495-4745 keV TH-229:4775-5142 keV 19 TH-228:5211*5493keV AC.22.7:5510-6128keV 17 15 'Ci) 13 I-11 z :::i 9 0 7 .?;-5 *s; n 3 <t: 2383 2780 3181 3587 Energy (keV) PEAK FWHM 319.219 118.549 0.000 54.829 29.637 COUNT DATE : 20-Sep-2016 11 :29:02 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 1242-H NUCLIDE TH-230 NOMINAL (pCi/G) 1.7737E+01 % RECOVERY 103.103 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 183.000 181.320 1.680 1.2961 100.000 1.43E+01 3.000 0.996 0.720 0.8485 99.940 6.82E-02 0.000 -1.200 1.200 1.0954 99.469 -8.21E-02 268.000 267.760 0.240 0.4899 99.700 1.83E+01 2.000 1.760 0.240 0.4899 100.000 1.20E-01 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-038 LIB FILE : AC BKG FILE : B208.CNF;805 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W208.CNF;253 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.12E+OO 2.77E-01 1.56E-01 3.69E+OO 2.36E-01 NOTES: MDA pCi/G 6.10E-01 5.38E-01 4.80E-01 3.27E-01 3.26E-01 Le pCi/G 1.87E-01 1.66E-01 1.37E-01 6.13E-02 6.11E-02 1.96-sigma cnt Unc pCi/G 2.09E+OO 2.76E-01 1.56E-01 2.20E+OO 2.36E-01

Ac-227 results are decay corrected to separation date/time.
Ac-227 Tracer nominal includes 5.7656E-01 dpm ingrowth from Ra-223.
Ac-227 Library Energy adjusted to compensate for ingrowth from Ra-223.
Corrections were made to Th-228 net area due to Ra-223 ingrowth from tracer. (1.284 +/-0.008)

Effective 31251201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 30-Sep-2016 Batch# Product:_--'-*f\_J-F,P'----Date: ' Criteria: Yes No Comments Sam Die Solids are less than or eciual to 100 mci for GAB. Samples have been blank corrected (if required). Blank correction reoorted included flf reauired\. If activity less than 10x MDA/MDC, error is less than or equal to 1500/o of sample activity. lf greater than 10" MDA/ MDC, error is 400/o or less. ,j-If tho Mnll I MDC: I<: Instrument source check Is within limits. In<:trumant bkn che"k I!:: within limits. v--Method RDL/ LLD has been met. v If duDllcate activities are: Less than 5* MDA/ MDC, then RPO Is 1000/o or less, If greater s* M DA/ MDC, then RPO 20% or less, v If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reaulred RER acceotance criteria. Tracer yield is 15*1250/o , Carrier yleld 25-1250/o. (Or meets the client's contract acceDtance criteria). v Method blank is less than the RDL/ LLD, v !rrf *"" ----*--.-50/n nf ,. ... 1 .. 1+u\ SamDle was run within hold time. / Samole was correctlv oreserved If reaulred. .Y j\j';\ f\)\>l I'-w Smears Taken for Radioactive batches. Method Spike and LCS are within 75-1250/o v or meak the client's con..,.ct arrnntance criteria\. No blank spaces on data forms. All line outs initialed and dated. v **------,. . ., Aux data is correct. >XI* Client Saeclal reauirements oaae has been checked. \/ Raw Data and I or are lnclutled and nronerlv statuo::ed. v MS, LCS, and Duplicate RPD/RER values uploaded to UMS and v VPrjfln .. Ult ,M (if 1\..'rr i>.,.t,.h nntnrn.t ln+n v -Batch Data Exceotion Reoorts fDER\ comoleted if aaolicable. V' 1)£.\l-I l/ Batch Data Exception Reports (DER) second reviewed. v \:::i)l*' Is i.;1;tL/lf Dlsoosition verified to be comaleted. IAUnunt C:nrrnrHnn ,.nmnletetl if -n**l*n" Review sample historical results If available ./' (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.l Primary Review Performed _J_[)_....\ _o_\_\_lo ___ _ Secondary Review Performed By:__ 10/03/16 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 03-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER ASTM C 1475-00 Modified Solid Batch ID: Sample Numbers: 1596392 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203621698 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 03-0CT-16 Jessica Davis 03-0CT-16 Page 1 Page 926 of 5809 DER Report No.: 1563744 Revision No.: 1 Type: Process Client Code: MJWC Neptunium Queue Sheet 07-SEP-16 ------*-----*---------*------------'--------Batch #: 1596392 Tracer Isotope: Am-243 (Np-239) LCS Isotope: Np-237 Spike Isotope: Np-237 Analyst: JXH2 First Client Due Date:04-0CT-16 Tracer Code: L\L\ 5-%-2.-j]TExpiration Date: C\-3tH{o Internal One nate30-SEP-16 Vol: (l,\ML Routine#: -*=b __ REF#: CJz.5i;-BKG#: <ii LCSCode: oSI 8-.S Expiration Date: l-la>-17 Vol: 01\.....,L Spike Code: Expiration Date:. _____ Vol:. __ _ NpSeparationDate/Time: lo )(oOO Prep Date: q

L 6 -\ L. Initials: ..)b\.\ Pipet ID: \ S l\ D01.'l: Balance ID: \ (o l 01 lo (o -Z.. Witness: t?b c\ *W-\U Hazard Min Sample D::es::cn=*p::ti::on=========:::::T::y:=pe==C=o=d=e====C=RD==L=========M=a=tri=*x:::* Dct# 405235001-1 4.1.B.R.1.2 405235002-1 4.1.B.R.l.3 4052..l5003-1 4.1.B.R.l.4 405235004-1 4.1.B.R.7.2 405235005-1 4.1.C.R.1.3 405235006-1 4.1.C.R.l.4 405235007-1 4.1.C.R.2.3 405235008-1 4.1.C.R.2.4 405235009-1 4.1.D.R.1.3 405235010-1 4.1.D.R.1.4 405235011-1 4.1.D.R.3.2 405235012-1 4.1.D.R.2.4 405235013-1 4.2A.R.2.3 405235014-1 4.2A.R.1.3 405235015-1 4.2A.R.1.4 405235016-1 4.2A.R.2.4 405235017-1 4.2A.R.3.2 405235018-1 4.2A.R.4.2 405235019-1 4.2B.R.2.4 405235020-1 4.2B.R.l.4 1203621697-1 for batch 1596392 1203621698-1 4.1.B.R.1.2(405235001DUP) 1203621699-1 LCS for batch 1596392 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SA1'\1PLE SAMPLE SAMPLE SAMPLE SAJ.\.IPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP LCS 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCilg 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g lpCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g l pCilg SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl 1\-UWCOOl MJWCOOl 1\-UWCOOl MJWCOOl MJWCOOl l\UWCOOl MJWCOOl MJWCOOl MJWCOOl l\UWCOOl MJWCOOl MJWCOOl MJWCOOl l'>'IJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Solid Sample Dissolution DIGESTION ircle One GEL l.Aboratories LLC, Radiochemistry Division 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 IO-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 02-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 10-DEC-15 2 3 4 5 6 7 8 9 10 11 \ f). 100 Z.1 I Co i 0. ) " '2. ___ ..:)k _ _j 9 1 !O-l6'-I '13 i no a '"' 1"4 i ns Y, i. o.;oo I ..,,,. 1 1 I :n I \11f> I \.C i o. 1 o o j __ .3.LffiJ_j \\ l o . ; as ! -31 i l ! 12 \7... i c. 10 i I ji t6D I 13 I \3 i Q. jO"I :f1 CB".5 I 14 I \I\ ia.161 Y't i__LS!e l 15 I \'5 i 0. l pl l\\ I [ iolOI 16 i , 6 ! o . 1c '1 _--':fz..._J_ 1qs-I 11 I \"1 ir:1.10.1 I c.g ! f'f1 i 18 __ tiW c=rUz 19 I \"\ i 0-\DO I 4".l l t&. 20 I 'Z-c I v. I 0 i.. ! i 2,QQ___) 21 I *z.\ l D, \ O'\ i 41 I fVilP i 22 -..is 1-z-'9=fl 23 l "2..'":> i o ,,e::L I \.\'\ i 1 ?A Data Reviewed By: Y.Jl f r /u .. 1 of 1 NP1596392 Pago 1 Page 928 of 5809 BATCH NUMBER*: 1596392 SAMPLE ID : S0405235001_NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.100 G +/-1.000 % CHAMBER : 161 DETECTOR S/N : 70321 AVERAGE %EFFICIENCY : 25.7727 AVERAGE %EFF ERROR : 0.4995 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 61.2 +/-5.414 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 08:59:52 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 2.7288E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.31 1 NP 237' 4430-4922 keV -I I I 23 94 2792 3193 3599 Energy (keV) PEAK FWHM 0.000 I 4008 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.720 I 5261 BKG AREA 0.720 I 5686 BKG StDev 0.8485 I I %ABUN 100.000 6115 6548 6986 ACTIVITY pCi/G -8.57E-02 ' I 7427 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B161.CNF;860 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W161.CNF;261 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.59E-01 MDA pCi/G 7.27E-01 Le pCi/G 1.85E-01 1.96-sigma cnt Unc pCi/G 2.59E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235002 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 162 DETECTOR S/N : 70323 AVERAGE %EFFICIENCY : 26.6669 AVERAGE %EFF ERROR : 0.5165 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 76.0 +/-5.293 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 08:59:54 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.3895E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.38 1 NP 237* 4430-4922 keV I I I 23 83 2782 3184 3590 Energy (keV) I PEAK FWHM 0.000 3999 44 2 GROSS AREA 0.000 I 482B NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 I 5248 BKG AREA 0.240 I 5672 I BKG S!Dev 0.4899 I 6099 6530 %ABUN 100.000 I 6964 ACTIVITY pCi/G -2.14E-02 I 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B162.CNF;862 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W162.CNF;260 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 1.85E-01 MDA pCi/G 4.27E-01 Le pCi/G 7.99E-02 1.96-sigma cnt Unc pCi/G 1.84E-01 0 ...., Ul 00 0 \0 BATCH NUMBER : 1596392 SAMPLE ID : S0405235003 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 178 DETECTOR S/N : 74436 AVERAGE %EFFICIENCY : 27.7549 AVERAGE %EFF ERROR : 0.5369 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 36.7 +/-5.821 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 08:59:57 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 1.6381 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.25 1 NP* 37: 4430-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA 0.000 BKG AREA 0.000 BKG S!Dev 0.0000 %ABUN 100.000 ACTIVITY pCi/G O.OOE+OO I I I I I I I I I I I 2399 2793 3192 3594 4001 44 3 482 5248 5672 6100 6533 6970 7411 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B178.CNF;874 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W178.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.54E-01 MDA pCi/G 5.26E-01 Le pCi/G 0.00E+OO 1.96-sigma cnt Unc pCi/G 3.54E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235004 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 19.5 +/-6.639 % TRACER 445-96-2-111 COUNT DATE : 01-0ct-201612:54:30 ELAPSED LIVE TIME(SEC) : 43200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 8.7006E+01 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4616.18 1 NP 237* 4430-4922 keV I I I 23 63 2764 3168 3575 Energy (keV) PEAK FWHM 184.351 I I 3986 44 1 GROSS AREA 3.000 I 481! NUCLIDE ACTIVITY SUMMARY NET AREA 1.560 I 5240 BKG AREA 1.440 I 5665 I BKG S!Dev 1.2000 6094 6526 %ABUN 100.000 6961 ACTIVITY pCi/G 1.81E-01 I 7400 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B175.CNF;872 BKG DATE : 30-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 5.38E-01 MDA pCi/G 9.51E-01 Le pCi/G 3.01E-01 1.96-sigma cnt Unc pCi/G 5.37E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235005 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 167 DETECTOR S/N : 72546 AVERAGE %EFFICIENCY : 24.1606 AVERAGE %EFF ERROR : 0.4690 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 83.9 +/-5.249 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 08:59:59 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.7442E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.42 NP* 37: 4430-4922 ke I I I 23 78 2780 3185 3594 Energy (keV) PEAK FWHM 0.000 I 4006 4421 GROSS AREA 0.000 I 484D NUCLIDE ACTIVITY SUMMARY NET AREA -1.680 I 5262 BKG AREA 1.680 I 5687 BKG S!Dev 1.2961 I 6116 %ABUN 100.000 I I 6548 6983 ACTIVITY pCi/G -1.43E-01 I 7422 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B167.CNF;886 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W167.CNF;246 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.01E-01 MDA pCi/G 6.58E-01 Le pCi/G 2.02E-01 1.96-sigma cnt Unc pCi/G 2.01E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235006 NP SAMPLE QTY : 0.102 G -+/-0.980 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 57.3 +/-5.466 % TRACER 445-96-2-111 ' GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 169 DETECTOR S/N : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 COUNT DATE : 30-Sep-2016 09:00:01 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 2.5567E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4746.59 1 NP 237* 4430-4922 kaV I I I 24 02 2798 3198 3603 Energy (keV) PEAK FWHM 305.610 I 4010 44 ?2 GROSS AREA 2.000 I 4833 NUCLIDE ACTIVITY SUMMARY NET AREA 0.080 I 5257 BKG AREA 1.920 5681 I BKG Stoev 1.3856 I 6108 6539 %ABUN 100.000 I 6974 ACTIVITY pCi/G 9.79E-03 I 7413 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B169.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 4.50E-01 MDA pCi/G 9.89E-01 Le pCl/G 3.11E-01 1.96-sigma cnt Unc pCl/G 4.50E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235007 NP SAMPLE QTY : 0.104 G -+/-0.962 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 85.6 +/-5.243 % TRACER . ID 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 170 DETECTOR S/N : 72549 AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 COUNT DATE : 30-Sep-2016 09:00:03 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.8176E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4762.26 2 NP Z37' 443().4922 keV >-I I I 23 86 2785 3187 3593 Energy (keV) PEAK FWHM 188.297 I 4004 44 8 GROSS AREA 4.000 I 483) NUCLIDE ACTIVITY SUMMARY NET AREA 2.800 5258 BKG AREA 1.200 5683 BKG StDev 1.0954 I %ABUN 100.000 I 6113 6547 6985 ACTIVITY pCi/G 2.30E-01 I 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B170.CNF;876 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DA TE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.72E-01 MDA pCi/G 5.75E-01 Le pCi/G 1.64E-01 1.96-sigma cnt Unc pCi/G 3.71E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235008 NP SAMPLE QTY : 0.103 G -+/-0.971 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 65.3 +/-5.387 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 COUNT DATE : 30-Sep-2016 09:00:05 ELAPSED LIVE TIME(SEC) : 14400.00 ,ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 2.9152E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4708.58 1 NP 237* 44304922 keV I 23 63 2764 3168 3575 Energy (keV) I PEAK FWHM 4.982 I 3986 4411 GROSS AREA 1.000 I 481! NUCLIDE ACTIVITY SUMMARY NET AREA 0.520 I 5240 BKG AREA 0.480 5665 BKG StDev 0.6928 I %ABUN 100.000 I 6094 6526 6961 ACTIVITY pCi/G 5.52E-02 I 7400 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B175.CNF;870 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.07E-01 MDA pCi/G 5.88E-01 Le pCi/G 1.35E-01 1.96-sigma cnt Unc pCi/G 3.07E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235009 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.100 G -+/-1.000 % CHAMBER : 176 DETECTOR SIN : 74434 AVERAGE %EFFICIENCY : 25.6995 AVERAGE %EFF ERROR : 0.4981 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 62.2 +/-5.419 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:08 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 2.7758E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4722.64 -2 NP 237* 443G-4922 keV r I I I 23 79 2776 3177 3582 Energy (keV) I PEAK FWHM 4.935 I 3991 44 5 GROSS AREA 4.000 482 NUCLIDE ACTIVITY SUMMARY NET AREA 2.080 I 5244 BKG AREA 1.920 I 5670 I BKG Stoev 1.3856 I %ABUN 100.000 I 6100 6534 6972 ACTIVITY pCi/G 2.44E-01 I 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B176.CNF;865 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 5.41E-01 MDA pCi/G 9.48E-01 Le pCi/G 2.98E-01 1.96-sigma cnt Unc pCi/G 5.40E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235010 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.100G -+/-1.000% CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.0 +/-5.224 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:10 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 4.0138E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.28 1 _ NP-237* 443()-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.480 BKG AREA 0.480 BKG S!Dev 0.6928 %ABUN 100.000 ACTIVITY pCi/G -3.77E-02 I I I I I I I I 2375 277 4 3177 3583 3994 44 0 482 I 5253 5680 6112 6548 6989 7 433 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B177.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 1.67E-01 MDA pCi/G 4.34E-01 Le pCi/G 9.96E-02 1.96-sigma en! Une pCi/G 1.67E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235011_NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G +/-0.952 % CHAMBER : 179 DETECTOR S/N : 74437 AVERAGE %EFFICIENCY : 26.3751 AVERAGE %EFF ERROR : 0.5108 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 70.3 +/-5.350 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:13 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.1371 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4646.74 2 NP 237* 443G-4922 keV -I I 23 77 2775 3176 3582 Energy (keV) PEAK FWHM 4.941 I I 3992 44 7 GROSS AREA 1.000 482 NUCLIDE ACTIVITY SUMMARY NET AREA 0.520 5248 BKG AREA 0.480 5675 BKG Stoev 0.6928 I 6106 6541 %ABUN 100.000 6981 ACTIVITY pCi/G 5.01E-02 I 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B179.CNF;877 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W179.CNF;254 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.79E-01 MDA pCi/G 5.34E-01 Le pCi/G 1.22E-01 1.96-sigma cnt Unc pCi/G 2.78E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235012 NP SAMPLE QTY : 0.101 G -+/-0.990 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 77.6 +/-5.298 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 180 DETECTOR S/N : 83295 AVERAGE %EFFICIENCY : 26.2740 AVERAGE %EFF ERROR : 0.5089 COUNT DATE : 30-Sep-2016 09:00:16 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.4637E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4775.35 _ NP*237: 443D4 22keV I I I 23 77 2777 3181 3588 Energy (keV) PEAK FWHM 4.978 I 4000 44 5 GROSS AREA 1.000 I NUCLIDE ACTIVITY SUMMARY NET AREA 0.280 I 5255 BKG AREA 0.720 5681 BKG S!Dev 0.8485 I I %ABUN 100.000 I 6111 6545 6982 ACTIVITY pCi/G 2.55E-02 I 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B180.CNF;879 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W180.CNF;230 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.67E-01 MDA pCi/G 5.57E-01 Le pCi/G 1.42E-01 1.96-sigma cnt Unc pCi/G 2.67E-01 0 ...., "' 00 0 'D BATCH NUMBER : 1596392 SAMPLE ID : S0405235013 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 185 DETECTOR S/N : 68615 AVERAGE %EFFICIENCY : 25.3535 AVERAGE %EFF ERROR : 0.4915 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 76.1 +/-5.310 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:18 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.3956E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4738.33 2 NP 237* 44304922 kaV -I I 23 80 2781 3186 3594 Energy (keV) PEAK FWHM 304.433 I 4006 44D1 GROSS AREA 4.000 483} NUCLIDE ACTIVITY SUMMARY NET AREA 1.360 I 5262 BKG AREA 2.640 I 5687 BKG StDev 1.6248 I I %ABUN 100.000 I 6117 6549 6986 ACTIVITY pCi/G 1.27E-01 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B185.CNF;859 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W185.CNF;237 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.38E-01 MDA pCi/G 8.37E-01 Le pCi/G 2.78E-01 1.96-sigma cnt Unc pCi/G 4.37E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235014 NP SAMPLE QTY : 0.107 G -+/-0.935 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 51.5 +/-5.559 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 186 DETECTOR S/N : 68616 AVERAGE %EFFICIENCY : 25.3981 AVERAGE %EFF ERROR : 0.4924 COUNT DATE : 30-Sep-2016 09:00:20 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 4.4615E+02 dpm 2.2991 E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4703.71 2 NP 237* 4430-4922 keV --I I I 23 95 2794 3198 3604 Energy (keV) PEAK FWHM 164.122 I 4014 44)8 GROSS AREA 4.000 I 484p NUCLIDE ACTIVITY SUMMARY NET AREA 1.120 5265 BKG AREA 2.880 5689 BKG StDev 1.6971 I 6117 6548 %ABUN 100.000 I 6982 ACTIVITY pCi/G 1.SOE-01 I 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B186.CNF;819 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W186.CNF;28 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 6.30E-01 MDA pCi/G 1.24E+OO Le pCi/G 4.17E-01 1.96-sigma cnt Unc pCi/G 6.30E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235015 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 188 DETECTOR S/N : 68621 AVERAGE %EFFICIENCY : 26.7276 AVERAGE %EFF ERROR : 0.5175 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 81.0 +/-5.282 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:22 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.6118E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4585.78 1 NP 237 4430-4922 keV I I I 24 29 2820 3215 3615 Energy (keV) PEAK FWHM 379.131 I 4019 GROSS AREA 3.000 484 NUCLIDE ACTIVITY SUMMARY NET AREA 0.840 I 5258 BKG AREA 2.160 I 5680 BKG StDev 1.4697 I 6106 6537 %ABUN 100.000 I 6972 ACTIVITY pCi/G 7.21E-02 I 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B188.CNF;854 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W188.CNF;233 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.60E-01 MDA pCi/G 7.20E-01 Le pCi/G 2.31E-01 1.96-sigma cnt Unc pCi/G 3.60E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235016 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 195 DETECTOR S/N : 78786 AVERAGE %EFFICIENCY : 26.3844 AVERAGE %EFF ERROR : 0.5110 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 76.1 +/-5.316 % TRACER 445-96-2-111 ' COUNT DATE : 30-Sep-2016 09:00:25 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.3935E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.33 NP-237: 4430-4922 k V I I I 23 93 2792 3195 3601 Energy (keV) I PEAK FWHM 0.000 4012 44 26 GROSS AREA 0.000 I 4844 NUCLIDE ACTIVITY SUMMARY NET AREA -1.200 5266 BKG AREA 1.200 I 5692 I BKG S!Dev 1.0954 I 6122 6556 %ABUN 100.000 I 6993 ACTIVITY pCi/G -1.08E-01 I 7435 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B195.CNF;880 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W195.CNF;259 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.05E-01 MDA pCi/G 6.31E-01 Le pCi/G 1.80E-01 1.96-sigma cnt Unc pCi/G 2.04E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235017 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.107 G -+/-0.935 % CHAMBER : 197 DETECTOR S/N : 78894 AVERAGE %EFFICIENCY : 26.0674 AVERAGE %EFF ERROR : 0.5050 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 91.9 +/-5.225 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:27 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 4.1010E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4703.08 PEAK FWHM 0.000 2 _ NP-237: 443o-49Z2 keV I I GROSS AREA 10.000 2372 2770 3172 3578 3988 44 2 481 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET AREA 2.080 BKG AREA 7.920 BKG S!Dev 2.8142 %ABLIN 100.000 ACTIVITY pCi/G 1.52E-01 I I I I I 5241 5666 6095 6528 6965 7406 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B197.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W197.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 5.17E-01 MDA pCi/G 9.74E-01 Le pCi/G 3.77E-01 1.96-sigma cnt Unc pCi/G 5.17E-01 AlphaSpectroscopySoflwaroVers!on3.5.3 effectivodato:02-Maf*2015 BATCH NUMBER : 1596392 SAMPLE ID : S0405235018 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 199 DETECTOR S/N : 78896 AVERAGE %EFFICIENCY : 26.2038 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 97.9 +/-5.198 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:30 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 4.3679E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.34 . 1 NP 237* 443()-4922 keV I I I 23 77 2776 3178 3585 Energy (keV) I PEAK FWHM 0.000 3995 44 9 GROSS AREA 0.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA -1.200 I 5249 BKG AREA 1.200 I 5674 I BKG StDev 1.0954 I %ABUN 100.000 I 6103 6537 6974 ACTIVITY pCi/G -8.13E-02 I 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B199.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W199.CNF;222 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 1.54E-01 MDA pCi/G 4.75E-01 Le pCi/G 1.36E-01 1.96-sigma cnt Unc pCi/G 1.54E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235019 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.100 G -+/-1.000 % CHAMBER : 182 DETECTOR S/N : 74440 AVERAGE %EFFICIENCY : 22.5384 AVERAGE %EFF ERROR : 0.4383 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 35.7 +/-5.900 % TRACER 445-96-2-111 . COUNT DATE : 30-Sep-2016 09:00:32 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 1.5921 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.39 1 NP-237; 4430-4.922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA 0.000 BKG AREA 0.000 BKG StDev 0.0000 %ABUN 100.000 ACTIVITY pCi/G O.OOE+OO I I I I I I I I I I I 2373 2774 3178 3585 3996 44 1 482 l 5251 5676 6104 6537 6972 7411 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B182.CNF;320 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W182.CNF;95 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 4.71E-01 MDA pCi/G 7.00E-01 Le pCi/G O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.70E-01 BATCH NUMBER : 1596392 SAMPLE ID : S0405235020 NP SAMPLE QTY : 0.102 G -+/-0.980 % SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 69.1 +/-5.376 % TRACER 445-96-2-111 . GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 200 DETECTOR S/N : 78900 AVERAGE %EFFICIENCY : 27.0654 AVERAGE %EFF ERROR : 0.5238 COUNT DATE : 30-Sep-2016 09:00:34 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.0847E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4745.79 1 NP 237* 44304922 keV I I I 23 94 2791 3191 3596 Energy (keV) I PEAK FWHM 4.930 4005 44 8 GROSS AREA 1.000 I 483 NUCLIDE ACTIVITY SUMMARY NET AREA -0.200 5256 BKG AREA 1.200 I 5681 I BKG S!Dev 1.0954 I %ABLIN 100.000 I 6111 6544 6982 ACTIVITY pCi/G -1.97E-02 I 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B200.CNF;801 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W200.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.95E-01 MDA pCi/G 6.90E-01 Le pCi/G 1.97E-01 1.96-sigma cnt Unc pCi/G 2.95E-01 Alpha Spectroscopy Software Version 3.5.3 effectlvedate:02-Mar-2015 BATCH NUMBER : 1596392 SAMPLE ID : S1203621697 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 93.9 +/-5.220 % TRACER ID. 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.04044 4.4615E+02 dpm 4.1914E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4675.31 .--r P-237: 14304922keV I I 23 83 2781 3184 3590 Energy (keV) PEAK FWHM 0.000 I 4000 44 M GROSS AREA 0.000 I 483 NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 5255 BKG AREA 0.240 I 5681 BKG StDev 0.4899 I I %ABUN 100.000 I 6111 6545 6983 ACTIVITY pCi/G -1.65E-02 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B166.CNF;891 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 1.42E-01 MDA pCi/G 3.29E-01 Le pCi/G 6.16E-02 1.96-sigma cnt Unc pCi/G 1.42E-01 BATCH NUMBER : 1596392 SAMPLE ID : S1203621698 NP SAMPLE QTY : 0.109 G -+/-0.917 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 39.1 +/-5.818 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 234 DETECTOR S/N : 87922 AVERAGE %EFFICIENCY : 24.8037 AVERAGE %EFF ERROR : 0.4811 COUNT DATE : 30-Sep-2016 09:00:39 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 1.7425E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.42 -1 NP 237* 443Cl-4922 keV I I I 23 88 2790 3194 3603 Energy (keV) PEAK FWHM 0.000 I 4014 4A 29 GROSS AREA 0.000 I 48417 NUCLIDE ACTIVITY SUMMARY NET AREA 0.000 5269 BKG AREA 0.000 I 5694 BKG StDev 0.0000 %ABUN 100.000 I 6123 6554 6990 ACTIVITY pCi/G O.OOE+OO I 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B234.CNF;454 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W234.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU pCi/G 3.59E-01 MDA pCi/G 5.33E-01 Le pCi/G O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.58E-01 0 ,...., Vi 00 0 \0 BATCH NUMBER : 1596392 SAMPLE ID : S1203621699 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 71.2 +/-5.365 % TRACER 445-96-2-111 COUNT DATE : 30-Sep-2016 09:00:42 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0518-S ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.04044 NUCLIDE NP-237 4.4615E+02 dpm 3.1759E+02 dpm NUCLIDE LIBRARY PEAK NP-237 25 22 19 16 'Ci) 13 I-z :::> 10 0 7 -2:-*:;; 4 ti <( ENERGY ENERGY 4788.00 4794.02 NP-237: 4430-4922 keV 2416 2810 3209 Energy (keV) PEAK FWHM 59.040 NOMINAL (pCi/G) 4.0967E+01 % RECOVERY 103.092 NUCLIDE ACTIVITY SUMMARY GROSS NET AREA AREA 445.000 443.560 BKG AREA 1.440 BKG StDev 1.2000 %ABUN 100.000 ACTIVITY pCi/G 4.22E+01 5691 6119 6551. 6988 7429 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B189.CNF;855 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 6.20E+OO MDA pCi/G 7.04E-01 Le pCi/G 2.09E-01 1.96-sigma cnt Unc pCi/G 3.94E+OO Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 23-Sep-2016 Batch#_, Product:. __ _.{0-""-IP----Date: Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma ror GAB. /V{;t* Samples have been blank corrected (If required). kr-r-Blank correction reoorted Included (if reouired). If activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. / If h<>lnu. th<> MDA/ MOC. orrnr l<l Instrument source check Is within limits. / I bko check I" within llml"-"* Method RDL/ LLD has been met. / If duplicate activities are: Less than 5"' MDA/ MDC, then RPO Is 100% or less, / lf greater 5* MDA/ MDC, then RPO 20% or less, lf below the MDA/ MDC, the RPO Is 0%, Or meets the client's reoulred RER accentance criteria. Tracer yield Is 15-125%
Carrier yield 25-1250/o. (Or meets the client's contract acceptance criteria). v* Method blank is less than the RDL/ LLD. ./ lfTf < !;;0/n nf ln ... od .......... , Samole was run within hold time. v Sample was correctlv oreserved If reauired. fl-.\;.)-Smears Taken for Radioactive batches. Lh Method Spike and LCS are within 75-1250/o ,/" If nr meets the client's rnntract acceotance criteria). No blank spaces on data forms. All line outs Initialed and dated. ./ Nn --Aux data Is correct. AJ?-Client Sneclal renulrements nane has been checked. ...v Raw Data and/ or soectrum are Included and orooerlv statused. ./ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and _,/ vorlflo,f 'UI* *-.. (If . 11 fv :A;;trh <>nt<>r<>ll ln*n .._,/' Batch Data Exceotlon Reoorts CDER) comoleted if aoollcable. v l) {'S?_p \18""1* Batch Data Exception Reports (DER) second reviewed. ,/ l)JL-tt I '51.o \ \ 8 :r Disoosition verified to be comoleted. Aliouot C<>rrectlnn If renulr<>d. lVJ Review sample historical results if available / Clf REMP, results above MDC have been verified bv historical results. recount or re-analvsls.) Primary Review Performed By:. __ W. ..... _ Secondary Review Performed By:__ 09/30/16 @0 Pagr952' o{ 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 25-SEP-16 Radiochemistry Specifications Instrument Type: ' Test I Method: Matrix Type: ALPHA SPECTROMETER ASTM C 1475-00 Modified Solid Batch ID: Sample Numbers: 1596420 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075, 405235076, 405235077, 405235078, and 1203621767 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 25-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 953 of 5809 DER Report No.: 1561187 Revision No.: Type: Process Client Code: MJWC Neptunium Queue Sheet 15-SEP-16 Batch#: 1596420 Analyst: KXB2 First Client Due Date:04-0CT-16 Tracer Isotope: Am-243 (Np-239) Tracer Code: ji.\S-%'2:Jil'.. Expiration Date: -\l9 Internal Dne Date.30-SEP-16 Routine#: REF#: ?'v-7,£ Les I t N 237 Les Code.. Qr"-\<l.' <; Expiration Date: 1-l<b *\] v I O \ so ope: p-"J_ v o: . O. \ Vol: BKG#: 91 Spike Isotope: Np-Z37 Spike Code:_____ Expiration Date:, _____ Vol:, __ _ Np Separation Dateffime: C\ lW l \\.J \5200 C\-'10-\U Initials:,_--tb-"'=---PipetID:W21.\0075l BalanceID: ltet07C.:-CR1-weUJfJ Sal'flple ID Oient Description Hazard Code Min CRDL Collection GFPC =====l\=fa=tnx:'.':'.* :':::. ___ P"-'os,,,,_.,__ Label# N...111M.L 405235061-1 5.lB.R.2.2 405235062-1 5.2A.R.l.2 405235063*1 5.2A.R.1.3 405235064-1 5.2A.R.1.4 405235065-1 5.2A.R.2.3 405235066-1 5.2A.R.2.4 405235067-1 5.2A.R.6.2 405235068-1 5.2A.R.4.2 405235069*1 5.2B.R.1.4 405235070-1 5.2B.R.3.2 405235071-1 5.2B.R.4.2 405235072-1 5.2B.R.2.4 405235073-1 5.2B.R.8.2 405235074-1 S.3A.R.I.3 405235075-1 5.4A.R.1.3 405235076-1 5.4A.R.4.2 405235077-1 5.5A.R.1.3 405235078-1 5.6A.R.1.3 1203621766-1 MB for batch 1596420 1203621767-1 5.IB.R.2.2(405235061DUP) 1203621768-1 LCS for batch 1596420 SAMPLE SAi.'\fPLE SAMPLE SAi\'1PLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAi\'1PLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAl\'fPLE SAMPLE SAl\'fPLE MB DUP LCS 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi!g 1 pCi/g 1 pCi/g 1 pCi/g I pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g 1 pCi/g SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOI MJWCOOl MJWCOOl MJWCOOl l\'UWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Solid Sample Dissolution by@i or DIGESTION Circle One GEL Laboratories LLC, Radiochemistry Division 14-DEC-15 14-DEC-15 14-DEC-15 14*DEC-15 14-DEC-15 14-DEC-15 11-DEC-15 11-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 11-DEC-15 15-DEC-15 16-DEC-15 11-DEC-15 17-DEC-15 17-DEC-15 14-DEC-15 ll lo-\ efe l l<.e-Z ! ! 2. b-!D'Z-i-1-1 2 L£. P-lLde-J I '+ ()_lo\ z..1 ! .S .D-I OS-z,) i LS'._ o* ll D i<:> nu 3 4 5 6 , 1 o. to3 1A '5 ' I 0-\0 '!? i-5 ntr 1 er 0. \OS" 1 z,.9 111 1 7 8 9 10 1 fl+/- ! $q __ l _j_Ji_J 11 i U f' -I lf-1 I n ! 1e:0_J 12 !-lZ.. t)_ I ]i-I 53j_J! 13 ' I n 1.r-1* rf? l ? U* 2_ 7Z i 14 l_l'f:_l0_,,t0S' l_r< i tSLJ 15 Llb !B: 1e7 I 5 __ J 16 Ltk !O-I ! t "Blf : 17 !OJ]) I 11 i ( 18 Li S IC5Lf i 1 f 1'1 19 LJ3_ ID-I fO Ii t'fl -I 20 i 2-b iO. lo! t? rq!:J---: 21 1.0 1 t t 17 J . /j <11'1 l ' Data Reviewed By: °I ,..;< S} Ito Page 1 of 1 NP1596420 Page1 Page 955 of 5809 BATCH NUMBER : 1596420 SAMPLE ID : S0405235061_NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.106 G +/-0.943 % CHAMBER : 162 DETECTOR S/N : 70323 AVERAGE %EFFICIENCY : 26.6669 AVERAGE %EFF ERROR : 0.5165 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 62.2 +/-5.408 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:26 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 2.7746E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.38 r-NP-237: 443Q-4922 k V I I 23 83 2782 3184 3590 Energy (keV) PEAK FWHM 0.000 I 3999 44 2 GROSS AREA 0.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA -0.960 5248 BKG AREA 0.960 I 5672 BKG S!Dev 0.9798 I I %ABUN 100.000 I 6099 6530 6964 ACTIVITY pCi/G -1.02E-01 I 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B162.CNF;860 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W162.CNF;260 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.38E-01 MDA pCi/G 7.04E-01 Le pCi/G 1.92E-01 1.96-sigma cnt Unc pCi/G 2.37E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235062 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.102 G -+/-0.980 % CHAMBER : 163 DETECTOR S/N : 80056 AVERAGE %EFFICIENCY : 25.6920 AVERAGE %EFF ERROR : 0.4979 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.5 +/-5.259 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:28 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.7256E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4709.20 _NP-237:4' 0-4922keV I I 23 75 2774 3176 3583 Energy (keV) I PEAK FWHM 4.957 I 3993 44 7 GROSS AREA 1.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 0.280 5246 BKG AREA 0.720 I 5672 BKG StDev 0.8485 I %ABUN 100.000 I 6101 6534 6971 ACTIVITY pCi/G 2.40E-02 I 7412 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B163.CNF;905 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W163.CNF;238 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.51E-01 MDA pCi/G 5.24E-01 Le pCi/G 1.33E-01 1.96-sigma cnt Unc pCi/G 2.51E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235063 NP SAMPLE QTY : 0.104 G -+/-0.962 % SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 74.7 +/-5.313 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 COUNT DATE : 22-Sep-2016 09:59:30 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.3327E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4696.15 1 NP 237* 4430-4922 k V -. . I I I 23 83 2781 3184 3590 Energy {keV) PEAK FWHM 4.953 4000 44 4 GROSS AREA 1.000 483 NUCLIDE ACTIVITY SUMMARY. NET AREA 0.520 I 5255 BKG AREA 0.480 I 5681 I BKG S!Dev 0.6928 I 6111 6545 %ABUN 100.000 I 6983 ACTIVITY pCi/G 4.71E-02 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B166.CNF;889 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.62E-01 MDA pCi/G 5.01E-01 Le pCi/G 1.15E-01 1.96-sigma en\ Unc pCi/G 2.62E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235064 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 167 DETECTOR S/N : 72546 AVERAGE %EFFICIENCY : 24.1606 AVERAGE %EFF ERROR : 0.4690 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 64.9 +/-5.389 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:33 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 2.8971 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4636.75 -.. 1 NP 237* 44Jo-4922 keV I 23 78 2780 3185 3594 Energy (keV) PEAK FWHM 120.032 4006 GROSS AREA 3.000 I 484) NUCLIDE ACTIVITY SUMMARY NET AREA 2.040 5262 BKG AREA 0.960 5687 BKG StDev 0.9798 6116 %ABUN 100.000 I I 6548 6983 ACTIVITY pCi/G 2.42E-01 I 7422 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B167.CNF;884 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W167.CNF;246 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 4.82E-01 MDA pCi/G 7.81E-01 Le pCi/G 2.13E-01 1.96-sigma cnt Unc pCi/G 4.81E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235065 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 169 DETECTOR SIN : 72548 AVERAGE %EFFICIENCY : 26.2282 AVERAGE %EFF ERROR : 0.5082 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 58.7 +/-5.451 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:35 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 2.6183E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4714.48 1 NP 237* 4430-4922 keV -I I 24 02 2798 3198 3603 Energy (keV) PEAK FWHM 103.513 I 4010 44 22 GROSS AREA 6.000 I 4833 NUCLIDE ACTIVITY SUMMARY NET AREA 5.520 I 5257 BKG AREA 0.480 I 5681 BKG StDev 0.6928 %ABUN 100.000 6108 6539 6974 ACTIVITY pCi/G 6.41E-01 7413 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B169.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W169.CNF;259 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 6.14E-01 MDA pCi/G 6.43E-01 Le pCi/G 1.47E-01 1.96-sigma cnt Unc pCi/G 6.10E-01 0 ,..., "' 00 0 'Cl BATCH NUMBER : 1596420 SAMPLE ID : S0405235066 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.110 G -+/-0.909 % CHAMBER : 170 DETECTOR S/N : 72549 AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 74.4 +/-5.319 % TRACER 445-96-2-111 ' COUNT DATE : 22-Sep-2016 09:59:38 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.3202E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4610.53 NP-237: 443()492 keV I I I 23 86 2785 3187 3593 Energy (keV) PEAK FWHM 4.955 4004 44 h8 GROSS AREA 1.000 I 483B NUCLIDE ACTIVITY SUMMARY NET AREA -0.680 I 5258 BKG AREA 1.680 5683 I BKG S!Dev 1.2961 6113 %ABUN 100.000 I I 6547 6985 ACTIVITY pCi/G -6.06E-02 I 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B170.CNF;874 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.74E-01 MDA pCi/G 6.90E-01 Le pCi/G 2.12E-01 1.96-sigma cnt Unc pCi/G 2.74E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235067 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 175 DETECTOR S/N : 74433 AVERAGE %EFFICIENCY : 26.2713 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 81.7 +/-5.276 % TRACER 445-96-2-111 ' COUNT DATE : 22-Sep-2016 09:59:40 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 4.4615E+02 dpm 3.6432E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4682.41 1 NP 237* 4430-4922 keV -I I I 23 63 2764 3168 3575 Energy (keV) PEAK FWHM 14.947 I I 3986 44 1 GROSS AREA 2.000 I 481! NUCLIDE ACTIVITY SUMMARY NET AREA 0.800 I 5240 BKG AREA 1.200 5665 I BKG StDev 1.0954 I %ABUN 100.000 I 6094 6526 6961 ACTIVITY pCi/G 6.80E-02 I 7400 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B175.CNF;868 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W175.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.0SE-01 MDA pCi/G 5.96E-01 Le pCi/G 1.70E-01 1.96-sigma cnt Unc pCi/G 3.0SE-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235068 NP SAMPLE QTY : 0.108 G -+/-0.926 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.7 +/-5.266 % TRACER . 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 176 DETECTOR S/N : 74434 AVERAGE %EFFICIENCY : *25.6995 AVERAGE %EFF ERROR : 0.4981 COUNT DATE : 22-Sep-2016 09:59:42 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 _N 23 79 4.4615E+02 dpm 3.7343E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4755.80 *237: 4430-4922 kaV l l I 2776 3177 3582 Energy (keV) PEAK FWHM 133.238 l 3991 441 5 GROSS AREA 3.000 482 NUCLIDE ACTIVITY SUMMARY NET AREA 1.560 5244 BKG AREA 1.440 5670 l BKG S!Dev 1.2000 %ABUN 100.000 l 6100 6534 6972 ACTIVITY pCi/G 1.26E-01 I 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B176.CNF;863 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W176.CNF;237 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.33E-01 MDA pCi/G 5.98E-01 Le pCi/G 1.78E-01 1.96-sigma cnt Unc pCi/G 3.32E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235069 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 177 DETECTOR S/N : 74435 AVERAGE %EFFICIENCY : 26.5935 AVERAGE %EFF ERROR : 0.5150 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 89.2 +/-5.239 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:45 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.9807E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4865.98 ;l2keV ,.... NP*237; 4430-49 I I I 23 75 2774 3177 3583 Energy (keV) I PEAK FWHM 4.955 3994 44 0 GROSS AREA 1.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 0.760 5253 BKG AREA 0.240 I 5680 I BKG S!Dev 0.4899 I %ABUN 100.000 I 6112 6548 6989 ACTIVITY pCi/G 5.73E-02 I 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B177.CNF;875 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W177.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.15E-01 MDA pCi/G 3.61E-01 Le pCi/G 6.76E-02 1.96-sigma cnt Unc pCi/G 2.15E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235070 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % CHAMBER : 179 DETECTOR S/N : 74437 AVERAGE %EFFICIENCY : 26.3751 AVERAGE %EFF ERROR : 0.5108 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 81.2 +/-5.283 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:48 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.6224E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4578.75 NP-237:44 D-4922keV I I 23 77 2775 3176 3582 Energy (keV) PEAK FWHM 4.941 I 3992 44 7 GROSS AREA 1.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 1.000 5248 BKG AREA 0.000 I 5675 BKG Stoev 0.0000 I 6106 6541 %ABLIN 100.000 6981 ACTIVITY pCi/G 8.43E-02 I 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B179.CNF;875 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W179.CNF;254 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.37E-01 MDA pCi/G 2.53E-01 Le pCi/G O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.37E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235071_NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G +/-0.917 % CHAMBER : 180 DETECTOR S/N : 83295 AVERAGE %EFFICIENCY : 26.2740 AVERAGE %EFF ERROR : 0.5089 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 62.0 +/-5.429 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:50 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 2.7646E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4665.24 1 NP '237* 4430-4922 keV I I I 23 77 2777 3181 3588 Energy (keV) PEAK FWHM 214.034 I 4000 44 n5 GROSS AREA 2.000 I 483 NUCLIDE ACTIVITY SUMMARY NET AREA 1.760 5255 BKG AREA 0.240 I 5681 BKG S!Dev 0.4899 I I %ABUN 100.000 I 6111 6545 6982 ACTIVITY pCi/G 1.86E-01 I 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B180.CNF;877 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W180.CNF;230 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.66E-01 MDA pCi/G 5.07E-01 Le pCi/G 9.49E-02 1.96-sigma cnt Unc pCi/G 3.66E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235072 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.100 G -+/-1.000 % CHAMBER : 181 DETECTOR S/N : 74439 AVERAGE %EFFICIENCY : 26.6415 AVERAGE %EFF ERROR : 0.5158 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 87.5 +/-5.252 % TRACER 445-96-2-111 . COUNT DATE : 22-Sep-2016 09:59:52 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.9053E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4707.24 1 NP 237* 4430-4922 keV I I I 23 76 2775 3177 3583 Energy (keV) PEAK FWHM 44.544 I 3994 44 9 GROSS AREA 2.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 1.040 5252 BKG AREA 0.960 I 5679 I BKG StDev 0.9798 I %ABUN 100.000 I 6111 6547 6987 ACTIVITY pCi/G 8.37E-02 I 7431 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B181.CNF;317 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W181.CNF;89 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.86E-01 MDA pCi/G 5.30E-01 Le pCi/G 1.44E-01 1.96-sigma cnt Unc pCi/G 2.86E-01 AJphaSpectroscopySot\wareVerslon3.5.3 effectlvedate:02-Mar*2015 BATCH NUMBER : 1596420 SAMPLE ID : S0405235073 NP SAMPLE QTY : 0.103 G -+/-0.971 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 76.0 +/-5.320 % TRACER 445-96-2-111 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 182 DETECTOR S/N : 74440 AVERAGE %EFFICIENCY : 22.5384 AVERAGE %EFF ERROR : 0.4383 COUNT DATE : 22-Sep-2016 09:59:55 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.3903E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4551.69 _ NP-237: 4430-49 koV I I I 23 73 2774 3178 3585 Energy (keV) PEAK FWHM 104.670 I 3996 44 1 GROSS AREA 2.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 1.040 5251 BKG AREA 0.960 I 5676 BKG StDev 0.9798 I I %ABLIN 100.000 I 6104 6537 6972 ACTIVITY pCi/G 1.11E-01 I 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B182.CNF;318 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W182.CNF;95 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 3.78E-01 MDA pCi/G 7.01E-01 Le pCi/G 1.91E-01 1.96-sigma cnt Unc pCi/G 3.78E-01 AlpllaSpectroscopySoftwareVersion3.5.3 effectivedate:02*Mar*2015 BATCH NUMBER : 1596420 SAMPLE ID : S0405235074 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.105 G -+/-0.952 % CHAMBER : 184 DETECTOR S/N : 74442 AVERAGE %EFFICIENCY : 25.3797 AVERAGE %EFF ERROR : 0.4920 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 82.3 +/-5.282 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 09:59:57 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.6735E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4664.38 2 NP 237* 4430-4922 keV I I I 23 60 2763 3169 3578 Energy (keV) PEAK FWHM 215.316 I 3990 44 7 GROSS AREA 4.000 4821 NUCLIDE ACTIVITY SUMMARY NET AREA 0.880 5249 BKG AREA 3.120 5675 BKG StDev 1.7664 I I %ABUN 100.000 l 6105 6538 6975 ACTIVITY pCi/G 7.53E-02 I 7415 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B184.CNF;295 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W184.CNF;85 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 4.04E-01 MDA pCi/G 8.10E-01 Le pCi/G 2.77E-01 1.96-sigma cnt Unc pCi/G 4.04E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235075 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.107 G -+/-0.935 % CHAMBER : 185 DETECTOR S/N : 68615 AVERAGE %EFFICIENCY : 25.3535 AVERAGE %EFF ERROR : 0.4915 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 88.4 +/-5.252 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 10:00:00 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.9440E+02 dpm LIBRARY PEAK ENERGY ENERGY 4 788.00 '4643.58 1 NP 237* 4430-4922 keV I I I 23 80 2781 3186 3594 Energy (keV) PEAK FWHM 319.406 I 4006 44D1 GROSS AREA 3.000 I 483l NUCLIDE ACTIVITY SUMMARY NET AREA -0.840 I 5262 BKG AREA 3.840 I 5687 I BKG S!Dev 1.9596 I %ABLIN 100.000 I 6117 6549 6986 ACTIVITY pCi/G -6.57E-02 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B185.CNF;857 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W185.CNF;237 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.42E-01 MDA pCi/G 7.97E-01 Le pCi/G 2.81E-01 1.96-sigma cnt Unc pCi/G 3.42E-01 0 ...., "' 00 0 '° BATCH NUMBER : 1596420 SAMPLE ID : S0405235076 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 186 DETECTOR S/N : 68616 AVERAGE %EFFICIENCY : 25.3981 AVERAGE %EFF ERROR : 0.4924 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 89.9 +/-5.246 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 10:00:02 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 4.0091 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4630.69 1 NP 237* 44304922 keV I I I 23 95 2794 3198 3604 Energy (keV) PEAK FWHM 4.973 I 4014 4428 GROSS AREA 1.000 I 484p NUCLIDE ACTIVITY SUMMARY NET AREA -0.920 5265 BKG AREA 1.920 5689 BKG StDev 1.3856 I %ABUN 100.000 I 6117 6548 6982 ACTIVITY pCi/G -7.35E-02 I 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B186.CNF;817 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W186.CNF;28 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.49E-01 MDA pCi/G 6.45E-01 Le pCi/G 2.03E-01 1.96-sigma cnt Unc pCi/G 2.48E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235077 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.110 G -+/-0.909 % CHAMBER : 188 DETECTOR S/N : 68621 AVERAGE %EFFICIENCY : 26.7276 AVERAGE %EFF ERROR : 0.5175 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.0 +/-5.275 % TRACER 445-96-2-111 ' COUNT DATE : 22-Sep-2016 10:30:55 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.8381E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.26 -1 NP 237* 4430-4922 keV I I I 24 29 2820 3215 3615 Energy (keV) I PEAK FWHM 4.861 4019 44 ?8 GROSS AREA 1.000 I 484 NUCLIDE ACTIVITY SUMMARY NET AREA -0.920 I 5258 BKG AREA 1.920 I 5680 I BKG StDev 1.3856 I 6106 6537 %ABUN 100.000 I 6972 ACTIVITY pCi/G -6.83E-02 I 7411 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B188.CNF;852 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W188.CNF;233 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.31E-01 MDA pCi/G 5.99E-01 Le pCi/G 1.88E-01 1.96-sigma cnt Unc pCi/G 2.31E-01 BATCH NUMBER : 1596420 SAMPLE ID : S0405235078 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.104 G -+/-0.962 % . CHAMBER : 189 DETECTOR S/N : 68622 AVERAGE %EFFICIENCY : 25.4050 AVERAGE %EFF ERROR : 0.4925 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.6 +/-5.243 % TRACER 445-96-2-111 COUNT DATE*: 22-Sep-2016 10:00:04 ELAPSED LIVE TIME(SEC) : 14400.00 ,ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 _NP* 24 16 4.4615E+02 dpm 4.1333E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4760.55 µ1: 44304922 keV I I I 2810 3209 3612 Energy (keV) PEAK FWHM 274.755 I 4020 GROSS AREA 2.000 I 4847 NUCLIDE ACTIVITY SUMMARY NET AREA 1.280 I 5266 BKG AREA 0.720 I 5691 I BKG StDev 0.8485 I 6119 6551 %ABUN 100.000 I 6988 ACTIVITY pCi/G 9.81E-02 I 7429 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B189.CNF;853 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W189.CNF;231 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.70E-01 MDA pCi/G 4.68E-01 Le pCi/G 1.19E-01 1.96-sigma cnt Unc pCi/G 2.70E-01 BATCH NUMBER : 1596420 SAMPLE ID : S1203621766 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.110 G -+/-0.909 % CHAMBER : 191 DETECTOR S/N : 68624 AVERAGE %EFFICIENCY : 24.3087 AVERAGE %EFF ERROR : 0.4718 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 39.9 +/-5.794 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 10:00:10 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 4.4615E+02 dpm 1.7807E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4443.11 NP-23 :4430-4922keV r r r 23 74 2773 3175 3581 Energy {keV) r PEAK FWHM 0.000 r 3991 GROSS AREA 2.000 r 482 NUCLIDE ACTIVITY SUMMARY NET AREA 1.040 r 5242 BKG AREA 0.960 r 5667 BKG StDev 0.9798 r r %ABUN 100.000 r 6095 6527 6963 ACTIVITY pCi/G 1.83E-01 r 7402 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B191.CNF;864 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W191.CNF;260 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 6.25E-01 MDA pCi/G 1.16E+OO Le pCi/G 3.16E-01 1.96-sigma en\ Une pCi/G 6.25E-01 BATCH NUMBER : 1596420 SAMPLE ID : S1203621767 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 195 DETECTOR S/N : 78786 AVERAGE %EFFICIENCY : 26.3844 AVERAGE %EFF ERROR : 0.5110 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 64.1 +/-5.437 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 10:00:12 ELAPSED LIVE TIME(SEC) : 14400.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 2.8603E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.33 1 NP 237* 443D-4922 keV I I I 23 93 2792 3195 3601 Energy (keV) I PEAK FWHM 0.000 4012 4AR6 GROSS AREA 0.000 I 4844 NUCLIDE ACTIVITY SUMMARY NET AREA -0.480 I 5266 BKG AREA 0.480 5692 BKG StDev 0.6928 I I %ABUN 100.000 I 6122 6556 6993 ACTIVITY pCi/G -5.27E-02 7435 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B195.CNF;878 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W195.CNF;259 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.34E-01 MDA pCi/G 6.08E-01 Le pCVG 1.39E-01 1.96-sigma cnt Unc pCi/G 2.33E-01 BATCH NUMBER : 1596420 SAMPLE ID : S1203621768 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.110 G -+/-0.909 % CHAMBER : 197 DETECTOR S/N : 78894 AVERAGE %EFFICIENCY : 26.0674 AVERAGE %EFF ERROR : 0.5050 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 82.6 +/-5.300 % TRACER 445-96-2-111 ' COUNT DATE : 22-Sep-2016 10:00:14 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID 0518-S ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 48.63157 NUCLIDE NP-237 4.4615E+02 dpm 3.6853E+02 dpm NUCLIDE LIBRARY PEAK en I-z :J 0 .?;-*:;; n <( NP-237 37 33 29 25 21 17 13 9 5 ENERGY ENERGY 4788.00 4758.41 NP-237: 4430-4922 keV 2372 2770 3172 3578 Energy (keV) PEAK FWHM 61.504 § 3988 44 2 NOMINAL (pCi/G) 4.0595E+01 % RECOVERY 111.921 NUCLIDE ACTl:-JITY SUMMARY GROSS NET AREA AREA 582.000 573.360 > 481 5241 BKG AREA 8.640 5666 BKG StDev 2.9394 %ABUN 100.000 6095 6528 6965 ACTIVITY pCi/G 4.54E+01 7406 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B197.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W197.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 6.33E+OO MDA pCi/G 1.09E+OO Le pCi/G 4.27E-01 1.96-sigma cnt Unc pCi/G 3.76E+OO Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Batch#_.._\ 5)......_0...._, l,.,.o __ lf_,_L"-l'--Product: __ __ _ Date: Criteria: Yes No Comments Samole Solids are less than or eaual to 100 mq ror GAB. 1\YJ* Samples have been blank corrected (If required). f\jf)-Blank correction reoorted Included ((f reauiredl. If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 400/o or less. ,/ [f hPIO'W th .. MnA I Mnr error Is ni.,.u Instrument source check is within limits. rnstrument bka check Is within limits. Method RDL/ LLD has been met. ./ tf duplicate activities are: Less than 5* MDA/ MDC, then RPD is 1000/o or less, [f greater 5* MDA/ MDC, then RPD 200/o or less, lf below the MDA/ MDC, the RPD Is 0%1 ,/ Or meets the client's reaulred RER acceotance criteria. Tracer yield Is 15*125%

Carrier yield 25-125%. ,,, C Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. v 'frf rad ----*--<! o;:O/n nf *-***--* ,.,-tlultu\ Samole was run within hold time. ./ l'lt.:i_it Samnle was correctlv oreserved If reaulred. \:\_ Smears Taken far Radioactive batches. 'IJd> Method Spike and LCS are within 75-125% ...--'or meatc thP. dirmt'<: "C'"""°"n<"" critarla l. No blank spaces on data forms. All line outs lnltlaled and dated. v ... _ --------Aux data Is correct. Client SPeclal reauirements oaae has been checked. ""' Raw Data and/ or soectrum are Included and orooerlv statused. -MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and v ""honcuorlr.nA Liit -(if i\P.. R"trh ftntoroA lntn r,..,., ,/ .. vslB Batch Data Excentlon Reoorts (DERl comoleted If aoollcable. v Batch Data Exception Reports (DER) second reviewed. /' Disnosltlon verified to be comoleted. 'Alln .. nt Corrortlnn com.,la*erl If r"'n""ir ... rl, Review sample historical results If available / (If REMP, results above MDC have been verified bv historical results. recount or re-analvsls. l Primary Review Performed By: __ }_v_!i_/_tc.. ____ _ I Secondary Review Performed By: __ 09/30/16 @ Pag¥9¥J 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 29-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: ALPHA SPECTROMETER ASTM C 1475-00 Modified Solid Batch ID: Sample Numbers: 1596411 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, and 1203621749 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 29-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 978 of 5809 DER Report No.: 1562818 Revision No.: Type: Process Client Code: MJWC Neptunium Queue Sheet 07-SEP-16 Analyst: HAKB First Client Due Date:04-0CT-16 Internal One Date.30-SEP-16 -T-Batch#: 1596411 Routine#: __ J_ REF#: . 'YZ'-95 BKG#: 'ii Cf/.j, '," @ J'f g;(J {, r-J, Tracerlsotope: Am-243 (Np-239) Tracer Code: tfl.\-5-jlz-;2., Vol;_0. \ LCS Isotope: Np-237 LCS Code: Of', \'b -.S Expiration Vol: ,0'. \ Spike Code: Expiration Date: -Vol: -Np Separation Date!fime: Spike Isotope: Np-237 Prep Date:OJ ')-0 \ \ \,... Initials: @ ¥ ..b Pipet ID: I f? l{Oo..2 .:C-: Balance ID: I lo I OJ (., t. Witness: -:f (. 6 7/ari /lb Hazard Min Collection wei6J GFPC Code CRDL Aliquot Sample ID Client Desctjption Type Matrix Client ___D.ate Pos. Label# :.I.Lt) __ NpDet# 405235041-1 4.4D.R.1.4 SAMPLE 1 pCi/g SOIL MJWCOOl 30-N0\'-15 1 LH-£* i Zl 2 ja 405235042-1 4.4D.R.2.3 SAMPLE 1 pCi/g SOIL MJWCOOl 30-NOV-15 2 ?::7 &ll 405235043-1 4.4D.R.2.4 SAMPLE 1 pCi/g SOIL MJWCOOl 30-NOV-15 3 102>\ "2-3 l\'l,, 405235044-1 >l.4D.R.4.2 SAMPLE 1 pCi/g SOIL MJWCOOl 30-NOV-15 4 : 4 !¢.._J_Qq ! 1J{ 2.-i J 405235045-1 4.40.R.5.2 SAMPLE 1 pCi/g SOIL MJWCOOl 30-NOV-15 5 !¢ l OS! <Le) Z..I '{ 405235046-1 4.SA.R.1.3 SAMPLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 6 ! Zr.,, 2...c I. 40523504 7 -1 4.SA.R.1.4 SA."\:IPLE lpCi/g SOIL MJWCOOl 07-DEC-15 7 n I 405235048-1 4.5B.R.1.2 SAMPLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 8 Zf5 I 'z.( 1 i i ' 4052.15049-1 4.5B.R.1.3 SAMPLE 1 pCi/g SOIL MJWCOOl 07-DEC-15 9 . y I ?.. a., "l'/..D ! 07-DEC-15 10 : 1¢. l l ! 2-2. I I 405235050-1 4.5B.R.1.4 SAMPLE 1 pCi/g SOIL MJWCOOl !ta i 3-Q 405235051-1 4.5B.R.2.3 SAi.\fi'LE 1 pCi/g SOIL MJWCOOl 07-DEC-15 11 ' ' I Lll___L¢._,_JJ 'U-'3 i 405235052-1 4.5B.R.2.4 SAi.\fi'LE 1 pCi/g SOIL MJWCOOl 07-DEC-15 12 L!2 !¢ . I '2. zJ. __.:1_(. l7..) i 405235053*1 4.5C.R.5.2 SAMPLE 1 pCi/g SOIL MJWCOOl 01-DEC-15 13 I 12 I !* Z..:Z.i I ! 405235054-1 4.SC.R.1.3 SAMPLE 1 pCi/g SOIL MJWCOOl 02-DEC-15 14 Lkzi_._12 ... 3t.t l.GS l 405235055-1 4.SC.R.1.4 SA!\<IPLE 1 pCi/g SOIL MJWCOOl 02-DEC-15 15 I '3? I C'Z.(;, i 405235056* 1 4.SC.R.2.2 SAMPLE 1 pCi/g SOIL MJWCOOl 02-DEC-15 16 (p i °3l.:> 1 405235057 -1 4.SC.R.2.3 SAMPLE l pCi/g SOIL l\1JWC001 02-DEC-15 17 I 12.-4 37 r ! 405235058-1 4.5C.R.2.4 SAi.\fi'LE 1 pCi/g SOIL MJWCOOl 02-DEC-15 18 -,¢-*---i 31!, i LO<:> I 405235059-1 5.lA.R.1.2 SAMPLE 1 pCi/g SOIL MJWCOOl 16-DEC-15 19 tE> -....o\ 405235060-1 5.IA.R.1.3 SAMPLE 1 pCi/g SOIL MJWCOOl 16-DEC-15 20 : !¢.11Y; t.fo z,01... 1203621748*1 MB for batch 1596411 * !\<ID 1 pCi/g SOIL QC ACCOUNT 21 'ii 1203621749-1 4.4D.R.1.4(405235041DUP) DUP 1 pCi/g SOIL QC ACCOUNT 30-NOV-15 22 Lit i)i il i I.fl. 7..0?' 1203621750-1 LCS for batch 1596411 LCS 1 pCi/g SOIL QC ACCOUNT 23 \ l.f:5 fl\);1-q ltiJ I\. Solid Sample Dissolution QfilJt or DIGESTION Circle One Data Reviewed By: '=! GEL Laboratories LLC, Radiochemistry Division Page 1 of 1 NP1596411 ----BKG . ___ _JI ____ ------------_____ 2.00!?!JQQ__ ___ __ . Cts= __ __ Ellicloncv..:____. __ __ Efllclen£)1_§rror= _ __ _ __ *-:= Std _____ _____ _§!!£1.2!!ey_ Error= ______ -----*------Rel'!!!!_l)_Co ---------____ ___ ... . ____ _!1,!!_l_I_O ____ --------_____ _gQj___ __ii!!!.".'!!!!!!J.... _flrri*24:i_ ____ 1_,_l§._ ___ ---------*------------->------*------------------________ _Hall-lil_l!_!)!J:!e:239 (dal'.!!J= ___ ._j!.356 _ -----------------------_ -------------*---------*------------* ---*--------v -----**-*-*---f-=:-------*-----, __ , __ _§!l)'_P-10 10 ____ . ..!!*I DalefTJ'!!'L. _ __ ..Q!!lla T (J!!f!!l 405235041.1 2171 15 9/22120168:42 9/211201614:30 2718.09 82.61% 1092.5 2177° Vora/on#: -_______ 2407 _ -.. 3023.og_ __ ______ _J_!!l7:-9 __ :::_ __ _=.._1&.2 _ 405235043.1 2566 15 9/22120169:13 9/21/201614:30 3232.84 96.26% 1123.2 2572 ----4o523so44:1 _____ *-*-242r-------1-5--*-a122i201ti9:2ii ___ --912i12oi6!4::io-----siiswr----93.o3% ____ -*-rr3ii:6'"""--242r-*---------2375 = 9JW20f69i4L =]f!_11201614:ao_:: __ --:... . ____ .__ ____ _ 405235046.1 2145 15 9/22120169:59 91211201614:30 2727.99 82.91% 1169.3 2151 ___ _::::::: -.. --= 405235048.1 2359 15 9/221201610:29 91211201614:30 3019.03 91.76% 1200.0 2365 ' :==-1if.52a!!Q19;L __ -::: .. -==IL ___ 14:°3Q ___ 1;i.90'1'!---= ____ =:::= ____ __________ .1_!L, __ . ...J1.12212Ql!!.1!.!.Q.I? __ 9121120..!§__14:3.L.c----* 2e46.52 ___ _____ E!!0-7 ____ _gQ?_t_ --*--*-*---_____ ____ ______ !L_ .... __ _li.15.87 ______ .. ___ 124E!:l1._. _ 1489 __ _ 405235052.1 2373 15 9/221201611:31 9/21/201614:30 3075.26 93.47% 1261.4 2379 __ 405235057.1 2242 15 9/221201612:46 9121/201614:30 2951.43 89.70% 1330.1 ==1 2248 ==---'!.Q!i235o58.r-= =.=-i2.?1-: -=*15-= =-2999.oo -----*-*91:15% -:::: * *-2277--------___ .,..195235q59.1 _______ ... __ ______ ___!11.25% __ .. ____ ... _ 2024 ____ ---------405235oso.1 211e 15 91221201s 13:34 01211201614:30 2814.55 85.54% 1384.2 2124 --120362Ti4ri.-1-------*2257----*-----*-15---9i22tTo16-\3:49---9i21120i6i4:36-* -----*3009_55----*-91.44% --------:-139g:5---*-**-**------1203sffi49.1 ___ --;559--*----Hr*--*-91221201fi4:04 si21i201614:3o *--2oa4_7_5 __ ---*--* --120362f75iff---22oa-*-*-15-----91221201614:20 --3069.20 ____ -* 93.28% *---,;r:ro.2---22or*--* ---*--------------------* ----------* -------* ---------------------------------------*--* 4os23so51-.1-------* ---*--*--3-1 ------*--55 -----**---f.iooc-*----------*-15-*-----*-1545 ----9t22t1e11:16 ------*-----------*--*-***-405235052-.1---------------32 ------95 ------2379---------,5-------1545" 9122/16 11:31 *-----*---------*--4o52350s3.1'" _____ ------95 2245----------,5 ------,-545 9/22116 11:46 --*---------------===::::-* =:=:=.:::Iqf ===::::.-* -:---9,faifa12.:@. .==::::::: -:::==-== --*-*-::::.:::-_::: ______ _____ I!! ___ ________ !§. _______ _ ___ -----* :_:=--==--=t-? ==---==--===---* =:-----= 405235059.1 ________ ----*-39--*------gg ----20241*-------*-15-*-----. 1545l--912211613:i8 ______ ---------------------___ -----:---------**----------------Pago 1 Page 980 of 5809 0 ...., Vi 00 0 \0 BATCH NUMBER : 1596411 SAMPLE ID : S0405235041_NP SAMPLE QTY : 0.115 G +/-0.870 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 210 DETECTOR S/N : 87898 AVERAGE %EFFICIENCY : 25.3042 AVERAGE %EFF ERROR : 0.4906 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 82.6 +/-5.212 % COUNT DATE : 22-Sep-201615:55:09 ELAPSED LIVE TIME(SEC) : 7200.00 TRACER 445-96-2-111 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.6857E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.43 -1 NP 237' 443Q-4922 keV I I I 23 81 2783 3189 3597 Energy (keV) PEAK FWHM o.ooo* I GROSS AREA 0.000 I 4009 44'5 NUCLIDE ACTIVITY SUMMARY NET AREA -0.360 I 5265 BKG AREA 0.360 I 5691 BKG StDev 0.6000 I 6119 %ABUN 100.000 I I 6551 6987 ACTIVITY pCi/G -5.62E-02 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B21 O.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W210.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 3.15E-01 MDA pCi/G 7.95E-01 Le pCi/G 1.63E-01 1.96-sigma cnt Unc pCi/G 3.15E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235042 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.116 G -+/-0.862 % CHAMBER : 211 DETECTOR S/N : 87899 AVERAGE %EFFICIENCY : 24.1091 AVERAGE %EFF ERROR : 0.4680 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 91.9 +/-5.168 % TRACER 445-96-2-111 ' COUNT DATE : 22-Sep-2016 15:55:11 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0992E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4892.98 1 ,.... NP-237* 4430-4922 keV PEAK FWHM 4.967 GROSS AREA 1.000 NUCLIDE ACTIVITY SUMMARY NET AREA 0.280 BKG AREA 0.720 BKG S!Dev 0.8485 %ABUN 100.000 ACTIVITY pCi/G 4.09E-02 I I I I I I I I I I I I 2375 2774 3177 3583 3993 482D 5246 5671 6099 6531 6967 7407 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B211.CNF;454 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W211.CNF;131 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.15E-01 MDA pCi/G 8.70E-01 Le pCi/G 2.16E-01 1.96-sigma cnt Unc pCi/G 4.15E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235043 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.103 G -+/-0.971 % CHAMBER : 212 DETECTOR S/N : 87900 AVERAGE %EFFICIENCY : 26.0378 AVERAGE %EFF ERROR : 0.5045 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 98.3 +/-5.143 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:55:13 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.3837E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4782.11 1 -NP-237* 4430-4922 keV PEAK FWHM 4.985 GROSS AREA 1.000 NUCLIDE ACTIVITY SUMMARY NET AREA 0.280 BKG AREA 0.720 BKG StDev 0.8485 %ABUN 100.000 ACTIVITY pCi/G 3.99E-02 I I 1 I I I I I I 2376 2776 3181 3589 4000 44 6 483i 5257 5684 6114 6547 6984 7425 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B212.CNF;453 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W212.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.05E-01 MDA pCi/G 8.48E-01 Le pCi/G 2.10E-01 1.96-sigma cnt Unc pCi/G 4.05E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235044 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.109 G -+/-0.917 % CHAMBER : 213 DETECTOR S/N : 87901 AVERAGE %EFFICIENCY : 24.8786 AVERAGE %EFF ERROR : 0.4826 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST: HAKB % YIELD : 93.0 +/-5.166 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:55:16 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 4.4615E+02 dpm 4.1507E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4521.71 1 _ fl -237: 443Cl-4922 keV PEAK FWHM 4.987 GROSS AREA 1.000 NUCLIDE ACTIVITY SUMMARY NET AREA 0.400 BKG AREA 0.600 BKG StDev 0.7746 %ABUN 100.000 ACTIVITY pCi/G 5.95E-02 I I I I I I I I I I I 2377 2778 3182 3590 4002 44 7 4836 5259 5685 6115 6548 6985 7426 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B213.CNF;467 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W213.CNF;152 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.22E-01 MDA pCi/G 8.48E-01 Le pCi/G 2.01E-01 1.96-sigma cnt Unc pCi/G 4.21E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235045 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 214 DETECTOR S/N : 87902 AVERAGE %EFFICIENCY : 26.2230 AVERAGE %EFF ERROR : 0.5080 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 91.5 +/-5.174 % TRACER 445-96-2-111 ' COUNT DATE : 22-Sep-2016 15:55:18 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0829E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4834.74 1 NP 237 443Cl-4922 k V -. . I I I 23 73 2771 3174 3581 Energy {keV) PEAK FWHM 4.958 I I 3991 GROSS AREA 1.000 482* NUCLIDE ACTIVITY SUMMARY NET AREA 0.040 I 5247 BKG AREA 0.960 I 5673 BKG S!Dev 0.9798 I %ABUN 100.000 I 6104 6538 6976 ACTIVITY pCi/G 5.79E-03 I 7419 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B214.CNF;454 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W214.CNF;119 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.15E-01 MDA pCilG 9.29E-01 Le pCi/G 2.47E-01 1.96-sigma cnt Unc pCi/G 4.14E-01 Alpha Spectroscopy Software Version 3.5.3 effedivadate;02-Mar-2015 BATCH NUMBER : 1596411 SAMPLE ID : S0405235046 NP SAMPLE QTY : 0.120 G -+/-0.833 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 82.9 +/-5.218 % TRACER 445-96-2-111 . GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 216 DETECTOR SIN : 87904 AVERAGE %EFFICIENCY : 24.6289 AVERAGE %EFF ERROR : 0.4779 COUNT DATE : 22-Sep-2016 15:55:21 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.6991 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4492.92 1 NP 237* 4430-4922 keV -I I I 23 72 2773 3179 3587 Energy (keV) PEAK FWHM 5.000 I 3999 GROSS AREA 1.000 I 483 NUCLIDE ACTIVITY SUMMARY NET AREA 0.520 I 5256 BKG AREA 0.480 I 5681 BKG S!Dev 0.6928 I I 6111 6543 %ABUN 100.000 I 6979 ACTIVITY pCi/G 7.97E-02 I 7418 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B216.CNF;454 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W216.CNF;128 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.33E-01 MDA pCi/G 8.29E-01 Le pCi/G 1.85E-01 1.96-sigma cnt Unc pCi/G 4.32E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235047 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY: 0.118G -+/-0.847% CHAMBER : 218 DETECTOR S/N : 87906 AVERAGE %EFFICIENCY : 25.1171 AVERAGE %EFF ERROR : 0.4871 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 90.0 +/-5.183 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:55:23 ELAPSED LIVE TIME(SEC) : 7200.00 ID, NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0135E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.37 1 NP 237 4430-4922 k V r-. ; . I I I 23 69 2770 3176 3585 Energy (keV) PEAK FWHM 0.000 I 3997 44 3 GROSS AREA 0.000 I NUCLIDE ACTIVITY SUMMARY NET AREA -0.840 I 5257 BKG AREA 0.840 I 5684 BKG StDev 0.9165 I I %ABUN 100.000 I 6115 6550 6988 ACTIVITY pCi/G -1.18E-01 I 7430 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B218.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W218.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 2.92E-01 MDA pCi/G 8.72E-01 Le pCi/G 2.25E-01 1.96-sigma cnt Unc pCi/G 2.91E-01 BATCH NUMBER : 1596411 SAMPLE JD : S0405235048 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 219 DETECTOR S/N : 87907 AVERAGE %EFFICIENCY : 25.4729 AVERAGE %EFF ERROR : 0.4938 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 91.8 +/-5.176 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:55:26 ELAPSED LIVE TIME(SEC) -: 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0938E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.29 NP-237: 4430 922keV I I ' 23 88 2787 3189 3595 Energy (keV) PEAK FWHM 0.000 4006 44DO GROSS AREA 0.000 I NUCLIDE ACTIVITY SUMMARY NET AREA -0.840 5262 BKG AREA 0.840 I 5688 I BKG StDev 0.9165 I 6119 6554 %ABUN 100.000 I 6993 ACTIVITY pCi/G -1.25E-01 I 7437 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B219.CNF;457 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W219.CNF;132 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 3.08E-01 MDA pCi/G 9.21E-01 Le pCi/G 2.37E-01 1.96-sigma cnt Unc pCi/G 3.08E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235049 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.114 G -+/-0.877 % CHAMBER : 220 DETECTOR S/N : 87908 AVERAGE %EFFICIENCY : 24.0361 AVERAGE %EFF ERROR : 0.4668 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 73.9 +/-5.277 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-201615:55:28 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.2971 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.39 1 ,.... NP-237* 4430-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.120 BKG AREA 0.120 BKG StDev 0.3464 %ABUN 100.000 ACTIVITY pCi/G -2.22E-02 I I I I I I I I I I 2377 2777 3181 3588 3998 44 2 483 5251 5676 6104 6535 6970 7409 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B220.CNF;456 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W220.CNF;142 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 3.69E-01 MDA pCi/G 7.80E-01 Le pCi/G 1.12E-01 1.96-sigma cnt Unc pCi/G 3.69E-01 "C (1) \0 \0 0 0 ....., Vl 00 0 \0 BATCH NUMBER : 1596411 SAMPLE ID : S0405235050 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.118 G -+/-0.847 % CHAMBER : 221 DETECTOR S/N : 87909 AVERAGE %EFFICIENCY : 25.5264 AVERAGE %EFF ERROR : 0.4948 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 80.4 +/-5.237 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:55:56 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 4.4615E+02 dpm 3.5886E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4 788.00 4675.41 P-237: 443D-4922 keV I I I 23 82 2784 3190 3599 Energy (keV) PEAK FWHM 0.000 I 4011 44 GROSS AREA 0.000 I 4845 NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 I 5269 BKG AREA 0.240 I 5695 BKG StDev 0.4899 I %ABUN 100.000 I 6124 6557 6993 ACTIVITY pCi/G -3.72E-02 I 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B221.CNF;465 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W221.CNF;128 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 3.11E-01 MDA pCi/G 7.29E-01 Le pCi/G 1.32E-01 1.96-sigma cnt Unc pCi/G 3.10E-01 0 ....., "' 00 0 '° BATCH NUMBER : 1596411 SAMPLE ID : S0405235051_NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.112 G +/-0.893 % CHAMBER : 166 DETECTOR S/N : 74545 AVERAGE %EFFICIENCY : 26.6822 AVERAGE %EFF ERROR : 0.5167 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 58.2 +/-5.416 % COUNT DATE : 26-Sep-2016 11 :51 :54 ELAPSED LIVE TIME(SEC) : 7200.00 TRACER ID NUCLIDE NOMINAL RESULTS NUCLIDE NP-237 445-96-2-111 ' AM-243 BETA %EFF.: 49.16467 4.4615E+02 dpm 2.5979E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4727.57 PEAK FWHM 0.000 GROSS AREA 2.000 1 ,.... NP-237* 4430-4922 keV I I I I 2383 2781 3184 3590 4000 483 Energy (keV) NUCLIDE ACTIVITY SUMMARY NET AREA 1.880 BKG AREA 0.120 BKG S!Dev 0.3464 %ABUN 100.000 ACTIVITY pCi/G 4.06E-01 I I I I I I 5255 5681 6111 6545 6983 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B166.CNF;891 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W166.CNF;299 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 7.37E-01 MDA pCi/G 9.07E-01 Le pCi/G 1.30E-01 1.96-sigma cnt Unc pCl/G 7.36E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235052 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 223 DETECTOR S/N : 87911 AVERAGE %EFFICIENCY : 25.6333 AVERAGE %EFF ERROR : 0.4968 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 93.5 +/-5.174 % TRACER .445-96-2-111 COUNT DATE : 22-Sep-2016 15:55:59 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.1700E+02 dpm LIBRARY PEAK ENERGY ENERGY 4 788.00 4675.37 1 ,...-NP-237* 44JCl-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.600 BKG AREA 0.600 BKG S!Dev 0.7746 %ABUN 100.000 ACTIVITY pCi/G -7.71E-02 I I I I I I I I I I I 2377 2776 3178 3584 3994 44 J8 482 D 5246 5670 6098 6529 6965 7403 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B223.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W223.CNF;114 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 2.63E-01 MDA pCi/G 7.32E-01 Le pCi/G 1.73E-01 1.96-sigma cnt Unc pCi/G 2.62E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235053 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.108 G -+/-0.926 % CHAMBER : 224 DETECTOR S/N : 87912 AVERAGE %EFFICIENCY : 25.7363 AVERAGE %EFF ERROR : 0.4987 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST: HAKB % YIELD : 88.5 +/-5.198 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:56:03 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.9487E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4768.35 ,__NP-237:443 )-4922keV I I 23 99 2795 3195 3599 Energy (keV) PEAK FWHM 260.757 I 4007 44JO GROSS AREA 2.000 I 4833 NUCLIDE ACTIVITY SUMMARY NET AREA 1.040 I 5257 BKG AREA 0.960 I 5682 BKG StDev 0.9798 I I %ABUN 100.000 I 6112 6545 6983 ACTIVITY pCi/G 1.59E-01 I 7425 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B224.CNF;469 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W224.CNF;150 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 5.29E-01 MDA pCi/G 9.78E-01 Le pCi/G 2.60E-01 1.96-sigma cnt Unc pCi/G 5.29E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235054 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 225 DETECTOR S/N : 87913 AVERAGE %EFFICIENCY : 25.9298 AVERAGE %EFF ERROR : 0.5025 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 79.7 +/-5.248 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:56:05 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.5579E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4679.66 ,NP-237: 4430-4922 keV I I I 23 88 2787 3190 3597 Energy (keV) I PEAK FWHM 4.962 4008 4A 23 GROSS AREA 1.000 484B NUCLIDE ACTIVITY SUMMARY NET AREA -0.080 I 5266 BKG BKG AREA S!Dev 1.080 1.0392 I I 5693 6124 6559 %ABUN 100.000 I 6998 ACTIVITY pCi/G -1.19E-02 I 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B225.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W225.CNF;124 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.27E-01 MDA pCi/G 9.85E-01 Le pCi/G 2.69E-01 1.96-sigma cnt Unc pCi/G 4.27E-01 "tJ "' "' U\ 0 ...., U\ 00 0 "' BATCH NUMBER : 1596411 SAMPLE ID : S0405235055 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.101 G -+/-0.990 % CHAMBER : 226 DETECTOR S/N : 87914 AVERAGE %EFFICIENCY : 26.8347 AVERAGE %EFF ERROR : 0.5195 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 79.9 +/-5.248 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-201615:56:08 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.5638E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4774.25 -1 NP 237* 443()4922 keV I I 23 72 2772 3177 3585 Energy (keV) PEAK FWHM 4.984 I 3997 44 3 GROSS AREA 1.000 I 483) NUCLIDE ACTIVITY SUMMARY NET AREA 0.160 I 5255 BKG AREA 0.840 I 5682 BKG StDev 0.9165 I I %ABUN 100.000 I 6113 6548 6986 ACTIVITY pCi/G 2.77E-02 I 7428 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B226.CNF;458 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W226.CNF;122 CAL DATE : 16-Sep-2016 1.96-sigma TPU pCi/G 4.95E-01 MDA pCi/G 1.07E+OO Le pCi/G 2.77E-01 1.96-sigma cnt Unc pCi/G 4.94E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235056 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.113 G -+/-0.885 % CHAMBER : 178 DETECTOR S/N : 74436 AVERAGE %EFFICIENCY : 27.7549 AVERAGE %EFF ERROR : 0.5369 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 86.5 +/-5.213 % TRACER 445-96-2-111 COUNT DATE : 26-Sep-2016 11 :51 :56 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.8579E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.25 1 _ NP-237* 4430-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA 0.000 BKG AREA 0.000 BKG S!Dev 0.0000 %ABUN 100.000 ACTIVITY pCi/G O.OOE+OO I I I I I I I I I I I 2399 2793 3192 3594 4001 44 3 5248 5672 6100 6533 6970 7411 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B178.CNF;874 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W178.CNF;243 CAL DATE : 13-Sep-2016 1.96-sigma TPU pCi/G 2.74E-01 MDA pCi/G 4.15E-01 Le pCi/G O.OOE+OO 1.96-sigma cnt Unc pCi/G 2.73E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235057 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 199 DETECTOR S/N : 78896 AVERAGE %EFFICIENCY : 26.2038 AVERAGE %EFF ERROR : 0.5077 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 89.7 +/-5.198 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:53:49 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0021 E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.34 1 ,.... NP 237: 4430-4922 keV PEAK FWHM 0.000 GROSS AREA 0.000 NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 BKG AREA 0.240 BKG S!Dev 0.4899 %ABUN 100.000 ACTIVITY pCi/G -3.14E-02 I I I I I I I I I 2377 2776 3178 3585 3995 4409 482 5249 5674 6103 6537 6974 7414 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B199.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W199.CNF;222 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 2.62E-01 MDA pCi/G 6.16E-01 Le pCi/G 1.12E-01 1.96-sigma cnt Unc pCi/G 2.62E-01 BATCH NUMBER : 1596411 SAMPLE ID : S0405235058 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.111 G -+/-0.901 % CHAMBER : 200 DETECTOR S/N : 78900 AVERAGE %EFFICIENCY : 27.0654 AVERAGE %EFF ERROR : 0.5238 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 91.1 +/-5.193 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:53:52 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0666E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4589.24 -. 1 NP 237* 443()..4922 keV I I I 23 94 2791 3191 3596 Energy (keV) I PEAK FWHM 4.930 4005 44 8 GROSS AREA 1.000 I 483p NUCLIDE ACTIVITY SUMMARY NET AREA -0.200 I 5256 BKG AREA 1.200 I 5681 I BKG S!Dev 1.0954 I 6111 6544 %ABUN 100.000 I 6982 ACTIVITY pCi/G -2.74E-02 I 7423 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B200.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W200.CNF;230 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.95E-01 MDA pCi/G 9.34E-01 Le pCi/G 2.61E-01 1.96-sigma cnt Unc pCi/G 3.95E-01 BATCH NUMBER : 1596411 . SAMPLE ID : S0405235059 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.107 G -+/-0.935 % CHAMBER : 201 DETECTOR S/N : 78902 AVERAGE %EFFICIENCY : 26.2326 AVERAGE %EFF ERROR : 0.5081 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 81.2 +/-5.246 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:53:55 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.6249E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.31 1 NP 237* 443()-4922 k V -. I I I 23 75 2773 3175 3582 Energy (keV) I PEAK FWHM 0.000 3992 44 6 GROSS AREA 0.000 I 4821 NUCLIDE ACTIVITY SUMMARY NET AREA -0.960 I 5247 BKG AREA 0.960 5673 BKG S!Dev 0.9798 I I %ABUN 100.000 I 6103 6537 6975 ACTIVITY pCi/G -1.58E-01 I 7417 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B201.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W201.CNF;224 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 3.43E-01 MDA pCi/G 1.06E+OO Le pCi/G 2.81E-01 1.96-sigma cnt Unc pCi/G 3.43E-01

-0 0 0 0 ....... Vt 00 0 'D AlphaSpeciltlscopySoftwareVersionJ.5.3 effectiwdate:02-Mar-2015 BATCH NUMBER : 1596411 SAMPLE ID : S0405235060 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.114 G -+/-0.877 % CHAMBER : 202 DETECTOR S/N : 78903 AVERAGE %EFFICIENCY : 27.2753 AVERAGE %EFF ERROR : 0.5278 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 85.5 +/-5.223 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:53:57 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 3.8165E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4669.83 -1 NP 237* 4430-4922 keV I I I 23 78 2777 3180 3587 Energy (keV) I PEAK FWHM 4.960 3998 44 n4 GROSS AREA 1.000 I 483 NUCLIDE ACTIVITY SUMMARY NET AREA -0.680 I 5256 BKG AREA 1.680 I 5683 I BKG S!Dev 1.2961 I 6115 6550 %ABUN 100.000 I 6990 ACTIVITY pCi/G -9.60E-02 I 7433 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B202.CNF;797 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W202.CNF;226 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.12E-01 MDA pCi/G 1.06E+OO Le pCi/G 3.18E-01 1.96-sigma cnt Unc pCi/G 4.12E-01 -0 0 -0 ...,, Vi 00 0 \0 BATCH NUMBER : 1596411 SAMPLE ID : S1203621748 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 203 DETECTOR S/N : 78905 AVERAGE %EFFICIENCY : 25.9071 AVERAGE %EFF ERROR : 0.5020 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 91.4 +/-5.195 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:54:00 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.0797E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4675.22 -1 NP 237* 4430-4922 keV I I I 23 69 2767 3170 3576 Energy (keV) PEAK FWHM 9.911 3987 4401 GROSS AREA 2.000 I 4821 NUCLIDE ACTIVITY SUMMARY NET AREA 1.760 5242 BKG AREA 0.240 5668 BKG S!Dev 0.4899 I %ABUN 100.000 6099 6533 6972 ACTIVITY pCi/G 2.29E-01 I 7414 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B203.CNF;799 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W203.CNF;229 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 4.45E-01 MDA pCi/G 6.11E-01 Le pCi/G 1.11E-01 1.96-sigma cnt Unc pCi/G 4.44E-01 BATCH NUMBER : 1596411 SAMPLE ID : S1203621749 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.115 G -+/-0.870 % CHAMBER : 205 DETECTOR S/N : 78908 AVERAGE %EFFICIENCY : 26.6171 AVERAGE %EFF ERROR : 0.5154 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 63.4 +/-5.385 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:54:02 ELAPSED LIVE TIME(SEC) : 7200.00 ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF. : 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 2.8269E+02 dpm LIBRARY PEAK ENERGY ENERGY 4788.00 4617.57 -1 NP 237* 4430-4922 keV I I I 23 78 2775 3177 3582 Energy (keV) I PEAK FWHM 4.945 3991 44M GROSS AREA 1.000 I 482 NUCLIDE ACTIVITY SUMMARY NET AREA 0.760 I 5242 BKG AREA 0.240 I 5667 BKG StDev 0.4899 I I %ABUN 100.000 I 6095 6527 6964 ACTIVITY pCi/G 1.47E-01 I 7404 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B205.CNF;801 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W205.CNF;223 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 5.43E-01 MDA pCi/G 9.11E-01 Le pCi/G 1.65E-01 1.96-sigma cnt Unc pCi/G 5.42E-01 -0 0 w 0 ...., V\ 00 0 \0 BATCH NUMBER : 1596411 SAMPLE ID : S1203621750 NP GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.122 G -+/-0.820 % CHAMBER : 206 DETECTOR S/N : 78909 AVERAGE %EFFICIENCY : 25.8407 AVERAGE %EFF ERROR : 0.5007 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 93.3 +/-5.189 % TRACER 445-96-2-111 COUNT DATE : 22-Sep-2016 15:54:05 ELAPSED LIVE TIME(SEC) : 7200.00 LCS ID 0518-S ID NUCLIDE NOMINAL RESULTS AM-243 BETA %EFF.: 49.16467 NUCLIDE NP-237 4.4615E+02 dpm 4.1618E+02 dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY NP-237 4788.00 4772.71 28 NP-237: 4430-4922 keV 25 22 19 0' 16 z 13 ::> 0 10 7 u 4 <i:: 2381 2779 3182 3588 Energy (keV) PEAK FWHM 35.697 ; 3998 44 2 NOMINAL (pCi/G) 3.6602E+01 % RECOVERY 115.531 NUCLIDE ACTIVITY SUMMARY GROSS NET AREA AREA 332.000 331.280 483 5252 BKG AREA 0.720 5679 BKG StDev 0.8485 %ABUN 100.000 6109 6543 6981 ACTIVITY pCi/G 4.23E+01 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-032 LIB FILE : NP BKG FILE : B206.CNF;798 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W206.CNF;226 CAL DATE : 15-Sep-2016 1.96-sigma TPU pCi/G 6.51E+OO MDA pCi/G 7.60E-01 Le pCi/G 1.89E-01 1.96-sigma cnt Unc pCi/G 4.57E+OO Page 1004 of 5809 Continuing Calibration Data Review of Alpha Spectrometer QA results (Daily checks) 17-SEP-2016 10:25:53.34 Bank 1 through bank 29 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2Q16 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 17-SEP-2016 Page 1005 of 5809 Detector 19 19 19 19 22 32 36 36 37 37 37 37 39 39 77 77 77 77 79 79 94 94 98 98 100 101 101 102 111 111 125 137 Parameter PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSENERGY-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSFWHM-5000 Flag Below Above Above Below Above Below Below Below Below Below Below Below Above Above Below Below Below Below Below Below Below Below Above Above Above Above Above Above Above Above Above Above 17-SEP-2016 183 PSFWHM-5000 Below 17-SEP-2016 183 PSCENTRD-5000 Below 17-SEP-2016 183 PSCTSS-5000 Below 17-SEP-2016 192 PSENERGY-:5000 Above 17-SEP-2016 198 PSFWHM-5000 Below 17-SEP-2016 198 PSCTSS-5000 Below 17-SEP-2016 237 PSENERGY-5000 Above 17-SEP-2016 237 PSCENTRD-5000 Above 17-SEP-2016 240 PSFWHM-5000 Above 17-SEP-2016 242 PSFWHM-5000 Above The following detectors that may not have properly transfered to the QA file 163 may not have run since 17-SEP-2016 164 may not have run since 17-SEP-2016 171 may not have run since 17-SEP-2016 172 may not have run since 17-SEP-2016 APPROVAL DATE: APPROVAL TIME: r(rzfrC l 0 tf.(' PROCEDURE # GL-RAD-I-009 Report completed at 17-SEP-2016 10:30:04.90 Page 1006 of 5809 Review of Alpha Spectrometer QA results (Daily checks) 19-SEP-2016 17:27:58.24 Bank 1 through_ bank 29 {detectors 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS Detector Parameter Flag 19-SEP-2016 19 PSFWHM-5000 Below 19-SEP-2016 19 PSENERGY-5000 Above 19-SEP-2016 19 PSCENTRD-5000 Above 19-SEP-2016 19 PSCTSS-5000 Below 19-SEP-2016 22 PSENERGY-5000 Above 19-SEP-2016 25 PSFWHM-5000 Above 19-SEP-2016 37 PSFWHM-5000 Below 19-SEP-2016 37 PSENERGY-5000 Below 19-SEP-2016 37 PSCENTRD-5000 Below 19-SEP-2016 37 PSCTSS-5000 Below .19-SEP-2016 39 PSENERGY-5000 Above 19-SEP-2016 48 PSFWHM-5000 Below 19-SEP-2016 48 PSENERGY-5000 Below 19-SEP-2016 48 PSCENTRD-5000 Below 19-SEP-2016 48 PSCTSS-5000 Below 19-SEP-2016 77 PSFWHM-5000 Below 19-SEP-2016 77 PSENERGY-5000 Below 19-SEP-2016 77 PSCENTRD-5000 Below 19-SEP-2016 77 PSCTSS-5000 Below 19-SEP-2016 79 PSFWHM-5000 Below 19-SEP-2016 79 PSCTSS-5000 Below 19-SEP-2016 94 PSFWHM-5000 Below 19-SEP-2016 94 PSCTSS-5000 Below 19-SEP-2016 98 PSENERGY-5000 Above 19-SEP-2016 98 PSCENTRD-5000 Above 19-SEP-2016 100 PSFWHM-5000 Above 19-SEP-2016 101 PSENERGY-5000 Above 19-SEP-2016 101 PSCENTRD-5000 Above 19-SEP-2016 102 PSFWHM-5000 Above 19-SEP-2016 111 PSENERGY-5000 Above 19-SEP-2016 ill PSCENTRD-5000 Above 19-SEP-2016 111 PSCTSS-5000 Below 19-SEP-2016 123 PSFWHM-5000 Above Page 1007of5809 19-SEP-2016 178 PSFWHM-5000 Above 19-SEP-2016 183 PSFWHM-5000 Below 19-SEP-2016 183 PSCENTRD-5000 Below 19-SEP-2016 183 PSCTSS-5000 Below 19-SEP-2016 192 PSENERGY-5000 Above 19-SEP-2016 193 PSFWHM-5000 Above 19-SEP-2016 198 PSFWHM-5000 Below 19-SEP-2016 198 PSCTSS-5000 Below 19-SEP-2016 237 PSENERGY-5000 Above 19-SEP-2016 237 PSCENTRD-5000 Above The following detectors that may not have properly transfered 171 may not have run. since .19-SEP-2016 172 may not have run since 19-SEP-2016 r f) I(., APPROVAL DATE =r* 1 APPROVAL TIME: /3') 5. PROCEDURE # GL-RAD-I-009 Report completed at 19-SEP-2016 17:30:48.77 Page 1008 of 5809 to the QA file Review of Alpha Spectrometer QA results (Daily checks) 20-SEP-2016 14:19:04.43 Bank 1 through bank 29 (detectors 1 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 20-SEP-2016 Page 1009 of 5809 Detector 19 19 19 19 22 37 37 37 37 39 46 67 77 77 77 77 79 79 87 94 94 98 98 98 100 101 101 102 111 111 138 Parameter PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSENERGY-5000 PSENERGY-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 Flag Below Above Above Below Above Below Below Below Below Above Below Below Below Below Below Below Below Below Above Below Below Below Below Below Above Above Above Above Above Above Above 20-SEP-2016 178 PSFWHM-5000 Above 20-SEP-2016 183 PSFWHM-5000 Below 20-SEP-2016 183 PSCENTRD-5000 Below 20-SEP-2016 183 PSCTSS-5000 Below 20-SEP.-2016 192 PSENERGY-5000 Above 20-SEP-2016 198 PSFWHM-5000 Below 20-SEP-2016 198 PSCTSS-5000 Below 20-SEP-2016 237 PSFWHM-5000 Above 20-SEP-2016 237 PSENERGY-5000 Above 20-SEP-2016 237 PSCENTRD-5000 Above The following detectors that may not have properly transfered to the QA file 7 may not have run since 20-SEP-2016 8 may not have run since 20-SEP-2016 i_,pr--Jlr 9 may not have run since 20-SEP-2016 10 may not have run since 20-SEP-2016 11 may not have run since 20-SEP-2016 12 may not have run since 20-SEP-2016 APPROVAL DATE: APPROVAL TIME: '7 r'l.o f APPR°J:;lc4 PROCEDURE # GL-RAD-I-009 Report completed at 20-SEP-2016 14:21:38.35 Page 1010of5809 Review of Alpha Spectrometer QA results (Daily checks) 22-SEP-2016 16:59:01.26 Bank 1 through bank 29 (detectors 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS Detector Parameter Flag 22-SEP-2016 19 PSFWHM-5000 Below 22-SEP-2016 19 PSENERGY-5000 Above 22-SEP-2016 19 PSCENTRD-5000 Above 22-SEP-2016 19 PSCTSS-5000 Below 22-SEP-2016 22 PSENERGY-5000 Above 22-SEP-2016 37 PSFWHM-5000 Below 22-SEP-2016 37 PSENERGY-5000 Below 22-SEP-2016 37 PSCENTRD-5000 Below 22-SEP-2016 37 PSCTSS-5000 Below 22-SEP-2016 39 PSENERGY-5000 Above 22-SEP-2016 46 PSENERGY-5000 Below 22-SEP-2016 77 PSFWHM-5000 Below 22-SEP-2016 77 PSENERGY-5000 Below 22-SEP-2016 77 PSCENTRD-5000 Below 22-SEP-2016 77 PSCTSS-5000 Below 22-SEP-2016 79 PSFWHM-5000 Below 22-SEP-2016 79 PSCTSS-5000 Below 22-SEP-2016 94 PSFWHM-5000 Below 22-SEP-2016 94 PSCTSS-5000 Below 22-SEP-2016 98 PSENERGY-5000 Above 22-SEP-2016 98 PSCENTRD-5000 Above 22-SEP-2016 100 PSFWHM-5000 Above 22-SEP-2016 101 PSENERGY-5000 Above 22-SEP-2016 101 PSCENTRD-5000 Above 22-SEP-2016 102 PSFWHM-5000 Above 22-SEP-2016 111 PSENERGY-5000 Above 22-SEP-2016 111 PSCENTRD-5000 Above 22-SEP-2016 138 PSFWHM-5000 Above 22-SEP-2016 183 PSFWHM-5000 Below 22-SEP-2016 183 PSCENTRD-5000 Below 22-SEP-2016 183 PSCTSS-5000 Below 22-SEP-2016 192 PSENERGY-5000 Above Page 1011 of 5809 22-SEP-2016 198 PSFWHM-5000 Below 22-SEP-2016 198 PSCTSS-5000 Below 22-SEP-2016 237 PSENERGY-5000 Above 22-SEP-2016 237 P 5 0 0.0 Above All QA parameters have been transfered since 22-SEP-2016 APPROVAL DATE: APPROVAL TIME: 'i\-i.-t-\LG )710 APPROp;'L4 PROCEDURE # GL-RAD-I-009 Report completed at 22-SEP-2016 17:01:37.19 Page 1012 of 5809 Review of Alpha Spectrometer QA results (Daily checks) 24-SEP-2016 11:50:37.75 Bank 1 bank 29 (detectors 1 through DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS Detector Parameter Flag -------------------------------------24-SEP-2016 19 PSFWHM-5000 Below 24-SEP-2016 19 PSENERGY-5000 Above 24-SEP-2016 19 PSCENTRD-5000 Above 24-SEP-2016 19 PSCTSS-5000 Below 24-SEP-2016 22 PSENERGY-5000 Above 24-SEP-2016 37 PSENERGY-5000 Below 24-SEP-2016 37 PSCTSS-5000 Below 24-SEP-2016 39 PSENERGY-5000 Above 24-SEP-2016 46 PSENERGY-5000 Below 24-SEP-2016 67 PSENERGY-5000 Below 24-SEP-2016 77 PSFWHM-5000 Below 24-SEP-2016 77 PSENERGY-5000 Below 24-SEP-2016 77 PSCENTRD-5000 Below 24-SEP-2016 77 PSCTSS-5000 Below 24-SEP-2016 79 PSFWHM-5000 Below 24-SEP-2016 79 PSCTSS-5000 Below 24-SEP-2016 94 PSFWHM-5000 Below 24-SEP-2016 94 PSCTSS-5000 Below 24-SEP-2016 98 PSENERGY-5000 Above 24-SEP-2016 98 PSCENTRD-5000 Above 24-SEP-2016 100 PSFWHM-5000 Above 24-SEP-2016 101 PSENERGY-5000 Above 24-SEP-2016 101 PSCENTRD-5000 Above 24-SEP-2016 102 PSFWHM-5000 Above 24-SEP-2016 111 PSENERGY-5000 Above 24-SEP-2016 133 *psFWHM-5000 Above 24-SEP-2016 138 PSFWHM-5000 Above 24-SEP-2016 183 PSFWHM-5000 Below 24-SEP-2016 183 PSCENTRD-5000 Below 24-SEP-2016 183 PSCTSS-5000 Below Page 1013 of 5809 24-SEP-2016 192 PSENERGY-5000 Above 24-SEP-2016 198 PSFWHM-5000 Below 24-SEP-2016 198 PSCTSS-5000 Below 24-SEP-2016 215 PSFWHM-5000 Above 24-SEP-2016 225 PSFWHM-5000 Above 24-SEP-2016 237 PSENERGY-5000 Above 24-SEP-2016 237 PSCENTRD-5000 Above 24-SEP-2016 242 PSENERGY-5000 Below The following detectors that may not have properly transfered to the QA file 163 may not have run since 24-SEP-2016 164 may not have run since 24-SEP-2016 171 may not have run since 24-SEP-2016 172 may not have run since 24-SEP-2016 APPROVAL DATE :1 9 r11-t reo APPROVAL TIME: t PROCEDURE # GL-RAD-I-009 Report completed at 24-SEP-2016 11:57:47.46 Page 1014of5809 Review of Alpha Spectrometer QA results (Daily checks) 25-SEP-2016 15:22:51.14 Bank 1 through bank 29 (detectors 1 through 256) DETECTORS NOT LISTED:HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS 24-SEP-2016 24-SEP-2016 24-SEP-2016 24-SEP-2016 24-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 25-SEP-2016 Page 1015of5809 Detector 19 19 19 19 22 36 36 37 37 37 37 39 46 67 77 77 77 77 79 79 91 91 91 91 94 94 98 98 100 101 101 102 Parameter PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSENERGY-5000 Flag Below Above Above Below Above Below Below Below Below Below Below Above Below Second Check Required for D PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-s*ooo PSFWHM-5000 Below Below Below Below Below Below Below Below Below Below Below Below Above Above Above Above Above Above 25-SEP-2016 111 PSENERGY-5000 Above 25-SEP-2016 123 PSFWHM-5000 Above 25-SEP-2016 133 PSFWHM-5000 Above :25-SEP-2016 138 PSFWHM-5000 Above 25-SEP-2016 168 PSFWHM-5000 Above 25-SEP-2016 183 PSFWHM-5000 Below 25-SEP-2016 183 PSCENTRD-5000 Below 25-SEP-2016 183 PSCTSS-5000 Below 25-SEP-2016 192 PSENERGY-5000 Above 25-SEP-2016 198 PSFWHM-5000 Below 25-SEP-2016 198 PSCTSS-5000 Below 25-SEP-2016 .204 PSFWHM-5000 Above 25-SEP-2016 215 PSFWHM-5000 Above 25-SEP-2016 216 PSFWHM-5000 Above 25-SEP-2016 237 PSENERGY-5000 Above 25-SEP-2016 237 PSCENTRD-5000 Above The following detectors that may not have properly transfered to the QA file 19 may not have run since 25-SEP-2016} 20 may not have run since 25-SEP-2016 21 may not have run since 25-SEP-2016 ) ll Y1 J .S 22 may not have run since 25-SEP-2016 23 may not have run since 25-SEP-2016 24 may not have run since 25-SEP-2016 163 may not have run since 25-SEP-2016 Df s-trv 1.C-4. 164 may not have run since 25-SEP-2016 171 may not have run since 25-SEP-2016 172 may not have run since 25-SEP-2016 APPROVAL DATE: *q' g_s \ APPROVAL TIME: 1 s: )() APPROVED BY: PROCEDURE # GL-RAD-I-009 Report completed at 25-SEP-2016 15:26:08.15 Page 1016of5809 Review of Alpha Spectrometer QA. results (Daily checks) 26-SEP-2016 10:59:23.05 Bank 1 through bapk 29 (detectors 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 26-SEP-2016 Page 1017 of 5809 Detector 19 19 19 36 36 37 37 37 37 39 46 77 77 77 77 79 79 83 83 94 94 98 98 100 101 101 101 102 111 114 123 Parameter PSFWHM-5000 PSENERGY-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSENERGY-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSFWHM-5000 PSENERGY:-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSFWHM-5000 PSFWHM-5000 Flag Below Above Below Below Below Below Below Below Below Above Below Below Below Below Below Below Below Below Below Below Below Above Above Above Above Above Above Above Above Above Above 26-SEP-2016 130 PSFWHM-5000 Above 26-SEP-2016 138 PSFWHM-5000 Above 26-SEP-2016 168 PSFWHM-5000 Above 26-SEP-2016 183 PSFWHM-5000 Below 26-SEP-2016 183 PSCENTRD-5000 Below 26-SEP-2016 183 PSCTSS-5000 Below 26-SEP-2016 192 PSENERGY-5000 Above 26-SEP-2016 198 PSFWHM-5000 Below 26-SEP-2016 198 PSCTSS-5000 Below 26-SEP-2016 215 PSFWHM-5000 Above 26-SEP-2016 216 PSENERGY-5000 Above 26.-SEP-2016 237 PSENERGY-5000 Above 26-SEP-2016 237 PSCENTRD-5000 Above The following detectors that may not have properly transfered to the QA file APPROVAL DATE: APPROVED Page 1018of5809 171 172 may not have run since 26-SEP-2016 I @tlf \Jf .. .may not have run since 26-SEP-2016 ) APPROVAL TIME: PROCEDURE # GL-RAD-I-009 Report completed at 26-SEP-2016 11:02:39.49 Review of Alpha Spectrometer QA results (Daily checks) 27-SEP-2016 11:50:04.75 BaD;k 1 through bank 2 9 (detectors 1 2 5 6) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS Detector Parameter Flag 27-SEP-2016 19 PSFWHM-5000 Below 27-SEP-2016 19 PSENERGY-5000 Below 27-SEP-2016 19 PSCTSS-5000 Below 27-SEP-2016 22 PSENERGY-5000 Above 27-SEP-2016 36 PSFWHM-5000 Below 27-SEP-2016 36 PSCTSS-5000 Below 27-SEP-2016 37 PSFWHM-5000 Below 27-SEP-2016 37 PSENERGY-5000 Below 27-SEP-2016 37 PSCENTRD-5000 Below 27-SEP-2016 37 PSCTSS-5000 Below 27-SEP-2016 39 PSENERGY-5000 Above 27-SEP-2016 46 PSENERGY-5000 Below 27-SEP-2016 77 PSFWHM-5000 Below 2 7-SEP-2 0"16 77 PSENERGY-5000 Below 27-SEP-2016 77 PSCENTRD-5000 Below 27-SEP-2016 77 PSCTSS-5000 Below 27-SEP-2016 79 PSFWHM-5000 Below 27-SEP-2016 79 PSCTSS-5000 Below 27-SEP-2016 94 PSFWHM-5000 Below 27-SEP-2016 94 PSCTSS-5000 Below 27-SEP-2016 98 PSENERGY-5000 Above 27-SEP-2016 98 PSCENTRD-5000 Above 27-SEP-2016 100 PSFWHM-5000 Above 27-SEP-2016 101 PSFWHM-5000 Above 27-SEP-2016 101 PSENERGY-5000 Above 27-SEP-2016 101. PSCENTRD-5000 Above 27-SEP-2016 102 PSFWHM-5000 Above 27-SEP-2016 111 PSENERGY-5000 Above 27-SEP-2016 114 PSFWHM-5000 Above 27-SEP-2016 130 PSFWHM-5000 Above 27-SEP-2016 138 PSFWHM-5000 Above Page 1019of5809 27-SEP-2016 183 PSFWHM-5000 Below 27-SEP-2016 183 PSCENTRD-5000 Below 27-SEP-2016 183 PSCTSS-5000 Below 27-SEP-2016 192 PSENERGY-5000 Abo ye 27-SEP-2016 198 PSFWHM-5000 Below 27-SEP-2016 198 PSCTSS-5000 Below 27-SEP-2016 215 PSFWHM-5000 Above 27-SEP-2016 216 PSENERGY-5000 Above 27-SEP-2016 237 PSENERGY-5000 Above 27-SEP-2016 237 PSCENTRD-5000 Above 27-SEP-2016 240 PSFWHM-5000 Above All QA parameters have been transfered since 27-SEP-2016 APPROVAL DATE: 'tf'\.,'l APPROVAL TIME: JI 5) PROCEDURE # GL-RAD-I-009 Report completed at 27-SEP-2016 11:53:21.22 Page 1020 of 5809 Review of Alpha Spectrometer QA results (Daily checks) 28-SEP-2016 15:27:27.78 Bank 1 through bank 29 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE. PARAMETERS 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP.-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 28-SEP-2016 Page 1021of5809 Detector 19 19 19 36 36 37 37 37 37 39 46 77 77 77 77 79 79 94 94 98 98 100 101 101 101 102 111 114 123 130 138 Parameter PSFWHM-5000 PSENERGY-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSENERGY-5000 PSENERGY-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSFWHM-5000 PSFWHM-5000 PSFWHM-5000 PSFWHM-5000 Flag Below Above Below Below Below Below Below Below Below Above Below Below Below Below Below Below Below Below Below Above Above Above Above Above Above .Above Above Above Above Above Above 28-SEP-2016 168 PSFWHM-5000 Above 28-SEP-2016 183 PSFWHM-5000 Below 28-SEP-2016 183 PSCENTRD-5000 Below 28-SEP-2016 183 PSCTSS-5000 Below 28-SEP-2016 192 PSENERGY-5000 Above 28-SEP-2016 198 PSFWHM-5000 Below 28-SEP-2016 198 PSCTSS-5000 Below 28-SEP-2016 211 PSFWHM-5000 Above 28-SEP-2016 215 PSFWHM-5000 Above 28-SEP-2016 216 PSENERGY-5000 Above 28-SEP-2016 237 PSENERGY-5000 Above 28-SEP-2016 237 PSCENTRD-5000 Above 28-SEP-2016 240 PSFWHM-5000 Above The following_ detectors that may not have properly transfered to the QA file 171 may not have run since 28-SEP-2016 172 may not have run since 28-SEP-2016 APPROVAL TIME: noo PROCEDURE # GL-RAD-I-009 Report completed at 28-SEP-2016 15:30:48.31 Page 1022 of 5809 Review of Alpha Spectrometer QA results (Daily checks) 29-SEP-2016 11:28:28.67 Bank 1 through bank 29 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016

29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 2'9-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 2 9 -SEP*-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 29-SEP-2016 Page 1023 of 5809 Detector 19 19 19 27 27 29 36 36 37 37 43 44 45 45 46 46 47 47 77 77 77 77 79 79 94 94 98 98 100 101 101 101 Parameter PSFWHM-5000 PSENERGY-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSENERGY-5000 PSFWHM-5000 PSCTSS-5000 PSENERGY-5000 PSCTSS-5000 PSENERGY-5000 PSENERGY-5000 PSENERGY-5000 PSCENTRD-5000 PSENERGY-5000 PSCENTRD-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSCTSS-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 PSFWHM-5000 PSENERGY-5000 PSCENTRD-5000 Flag Below Above Below Below Below Above Below Below Below Below Above Above Above Above Above Above Above Above Below Below Below Below Below Below Below Below Above Above Above Above Above Above 29-SEP-2016 102 PSFWHM-5000 Above 29-SEP-2016 111 PSENERGY-5000 Above 29-SEP-2016 114 PSFWHM-5000 Above 29-SEP-2016 130 PSFWHM-5000 Above 29-SEP-2016 137 PSFWHM-5000 Above 29-SEP-2016 138 PSFWHM-5000 Above 29-SEP-2016 183 PSFWHM-5000 Below 29-SEP-2016 183 PSCENTRD-5000 Below 29-SEP-2016 183 PSCTSS-5000 Below 29-SEP-2016 184 PSFWHM-5000 Above 29-SEP-2016 192 PSENERGY-5000 Above 29-SEP-2016 198 PSFWHM-5000 Below 29-SEP-2016 198 PSCTSS-5000 Below 29-SEP-2016 211 PSFWHM-5000 Above 29-SEP-2016 215 PSFWHM-5000 Above 29-SEP-2016 216 PSENERGY-5000 Above 29-SEP-2016 219 PSFWHM-5000 Above 29-SEP-2016 237 PSENERGY-5000 Above 29-SEP-2016 237 PSCENTRD-5000 Above 29-SEP-2016 240 PSFWHM-5000 Above The following detectors that may not have properly transfered to the QA file 171 may not have run since 29-SEP-2016 172 may not have run since 29-SEP-2016 APPROVAL APPROVAL TIME: (,-Z,6 {) APPROVED PROCEDURE.# GL-RAD-I-009 Report completed at 29-SEP-2016 11:31:49.21 Page 1024 of 5809 Review of Alpha Spectrometer QA results (Daily checks) 30-SEP-2016 14:13:56.36 Bank 1 through 29 (detectors 1 through 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS Detector Parameter Flag 30-SEP-2016 19 PSFWHM-5000 Below 30-SEP-2016 19 PSENERGY-5000 Above 30-SEP-2016 19 PSCTSS-5000 Below 30-SEP-2016 27 PSENERGY-5000 Below 30-SEP-2016 27 PSCENTRD-5000 Below 30-SEP-2016 29 PSENERGY-5000 Above 30-SEP-2016 36 PSFWHM-5000 Below .30-SEP-2016 36 PSCTSS-5000 Below 30-SEP-2016 37 PSFWHM-5000 Below 30-SEP-2016 37 PSENERGY-5000 Below 30-SEP-2016 37 PSCENTRD-5000 Below 30-SEP-2016 37 PSCTSS-5000 Below 30-SEP-2016 43 PSENERGY-5000 Above 30-SEP-2016 44 PSENERGY-5000 Above 30-SEP-2016 45 PSENERGY-5000 Above 30-SEP-2016 45 PSCENTRD-5000 Above 30-SEP-2016 46 PSENERGY-5000 Above 30-SEP-2016 46 PSCENTRD-5000 Above 30-SEP-2016 47 PSENERGY-5000 Above 30-SEP-2016 47 PSCENTRD-5000 Above 30-SEP-2016 77 PSFWHM-5000 Below 30-SEP-2016 77 PSENERGY-5000 Below 30-SEP-2016 77 PSCENTRD-5000 Below 30-SEP-2016 77 PSCTSS-5000 Below 30-SEP-2016 79 PSFWHM-5000 Below 30-SEP-2016 79 PSCTSS-5000 Below 30-SEP-2016 94 PSFWHM-5000 Below 30-SEP-2016 94 PSCTSS-5000 Below 30-SEP-2016 98 PSFWHM-5000 Below 30-SEP-2016 98 PSENERGY-5000 Below 30-SEP-2016 . 98 PSCTSS-5000 Below 30-SEP-2016 100 PSFWHM-5000 Above Page 1025 of 5809 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 30-SEP-2016 101 101 102 111 114 129 130 138 183 183 183 184 192 198 198 215 216 237 237 240 PSENERG.Y-5000 PSCENTRD-5000 PSFWHM-5000 PSENERGY-5000 PSFWHM-5000 PSFWHM-5000 PSFWHM-5000 PSFWHM-5000 PSFWHM-5000 PSCENTRD-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSFWHM-5000 PSCTSS-5000 PSFWHM-5000 PSENERGY-5000 PSENERGY-5000 PSCENTRD-5000 PSFWHM-5000 Above Above Above Above Above Above Above Above Below Below Below Above Above Below Below Above Above Above Above Above The following detectors that may not have properly transfered to the QA file Page 1026 of 5809 171 may not have run since 30-SEP-2016 172 may not have run since 30-SEP-2016 APPROVAL TIME: PROCEDURE # GL-RAD-I-009 Report completed at 30-SEP-2016 14:17:13.17 Review of Alpha Spectrometer QA results (Daily checks) 1-0CT-2016 12:15:45.37 Bank 1 through bank 29 (detectors 1 thrc;mgh 256) DETECTORS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS . Detector Parameter Flag -------------------------------------1-0CT-2016 19 PSFWHM-5000 Below 1-0CT-2016 19 PSENERGY-5000 Above 1-0CT-2016 19 PSCENTRD-5000 Above 1-0CT-2016 19 PSCTSS-5000 Below 1-0CT-2016 27 PSFWHM-5000 Above 1-0CT-2016 27 PSENERGY-5000 Below 1-0CT-2016 27 PSCENTRD-5000 Below l-OCT-2016 29 PSFWHM-5000 Above l-OCT-2016 36 PSFWHM-5000 Below 1-0CT-2016 36 PSCTSS-5000 Below 1-0CT-2016 37 PSFWHM-5000 Below l-OCT-2016 37 PSENERGY-5000 Below 1-0CT-2016 37 PSCENTRD-5000 Below 1-0CT-2016 37 PSCTSS-5000 Below 1-0CT-2016 43 PSENERGY-5000 Above l-OCT-2016 44 PSFWHM-5000 Below 1-0CT-2016 44 PSCTSS-5000 Below l-OCT-2016 45 PSFWHM-5000 Below 1-0CT-2016 45 PSENERGY-5000 Above 1 -OCT-2.016 45 PSCTSS-5000 Below l-OCT-2016 46 PSFWHM-5000 Below l-OCT-2016 46 PSENERGY-5000 Above 1-0CT-2016 46 PSCENTRD-5000 Above 1-0CT-2016 46 PSCTSS-5000 Below l-OCT-2016 47 PSFWHM-5000 Below 1-0CT-2016 47 PSENERGY-5000 Above 1-0CT-2016 47 PSCTSS-5000 Below 1-0CT-2016 48 PSFWHM-5000 Below 1-0CT-2016 48 PSENERGY-5000 Below l-OCT-2016 48 PSCENTRD-5000 Below 1-0CT-2016 48 PSCTSS-5000 Below 1-0CT-2016 66 PSFWHM-5000 Below 1-0CT-2016 66 PSENERGY-5000 Below 1-0CT-2016 66 PSCTSS-5000 Below 1-0CT-2016 78 PSENERGY-5000 Above Page 1027 of 5809 1-0CT-2016 79 PSFWHM-5000 Above 1-0CT-2016 87 PSENERGY-5000 Below 1-0CT-2016 87 PSCENTRD-5000 Below 1-0CT-2016 94 PSFWHM-5000 Below 1-0CT-2016 94 PSCTSS-5000 Below l-OCT-2016 98 PSENERGY-5000 Above 1-0CT-2016 98 PSCENTRD-5000 Above 1-0CT-2016 100 PSFWHM-5000 Above l-OCT-2016 101 PSENERGY-5000 Above l-OCT-2016 101 PSCENTRD-5000 Above 1-0CT-2016 102 PSFWHM-5000 Above 1-0CT-2016 111 PSENERGY-5000 Above 1-0CT-2016 114 PSFWHM-5000 Above l-OCT-2016 129 PSFWHM-5000 Above 1-0CT-2016 138 PSFWHM-5000 Above 1-0CT-2016 161 PSFWHM-5000 Above 1-0CT-2016 183 PSFWHM-5000 Below 1-0CT-2016 183 PSCENTRD-5000 Below 1-0CT-2016 183 PSCTSS-5000 Below l-OCT-2016 184 PSFWHM-5000 Above 1-0CT-2016 192 PSENERGY-5000 Above l-OCT-2016 198 PSFWHM-5000 Below 1-0CT-2016 198 PSCTSS-5000 Below 1-0CT-2016 211 PSFWHM-5000 Above l-OCT-2016 215 PSFWHM-5000 Above l-OCT-2016 216 PSENERGY-5000 Above l-OCT-2016 232 PSFWHM-5000 Above l-OCT-2016 233 PSFWHM-5000 Above l-OCT-2016 237 PSENERGY-5000 Above l-OCT-2016 237 PSCENTRD-5000 Above l-OCT-2016 240 PSFWHM-5000 Above The following detectors that may not have properly transfered to the QA file 171 may not have run since 1-0CT-2016 J OLN--t J 5,.(JYIJ\'cA 172 may not have run since 1-0CT-2016 Page 1028 of 5809 APPROVAL DATE: ID I J l J LP APPROVAL TIME: JI) *. l Q APPROVED BY, PROCEDURE # GL-RAD-I-009 Report completed at 1-0CT-2016 12:19:29.45 Page 1029of5809 Page 1030 of 5809 Background and Efficiency Data

-0 w -QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W001.QAF;12 AVRGEFF (Average Efficiency) 4-AUG-2016 14:49:25 through 12:00: 00 0.285426 through 0.303082 . . . . . . . . 3 ........................... ' ............................................... . (J c Q) *ri (J *ri 4-4-LU Q) -0.0 ill Q) > cr: . 295 . . . . . . . x . . . . . . . ............................................................................ . . . . . . . x x x . . . . . . . . 29 ............................................................................ . . . . . . . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurer.-.ent Date/Tir.-.e UP LOW _. 0 V.l N 0 ....., Vl 00 0 \0 QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W001.QAF;12 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-AUG-2016 14:49:25 through 28-SEP-2016 12:00:00 184.000 through 204. 000 200 ........................................ * .......... .' ................... : ........ . I CJ )-1--H > H 1--u a: w CJ H __J u x ::i z x 190 o o o o ' o o 0 "o I o o o o I o o .. o o 0 I o o o o I 'o o 0 0 I o o o I o' o o ' 0 I o o o o *, o 0 o o o I o o o' I I o 0 o I o o o : o o 0 o I o I I o x x 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 MeasureMent Date/Tirrie UP LOW -0 (.;..) (.;..) 0 ....., Vl 00 0 \0 QA filena!Y'le Para!Y'leter Na!Y'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W001.QAF;12 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-AUG-2016 14:49: 25 through 28-SEP-2016 12:00:00 5.00000 through 100.000 80 ......... * .................... * .......... * ......... * .......... * ......... : ........ . ..... I 0 z D H :=i ....I D en w. 0:: :::..::: a: w 0... . . . . . . . 60 ..................... ' ......... ' ........................................... . . . . . . . . x x 40 .......................................................... ' ................ . . . . . . . . . 20 ......... " ........ ' ................... '* ......... , ................... ' ........ . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measure!Y'lent Date/Ti!Y'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W001.QAF;12 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-AUG-2016 14: 49:25 through 28-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . . ............................................................................ ro "'" ""'"" I D C!:I )-C!:I 0::: x x LLJ 3180 z . ' . . . . o o o o o o o o o o o o o o o o I o 0 o o 0 I o o o o I o o o I o o o o o o o o 0 o o o ' o o I I o o o o I o o o ' I o ' 0 o o o o o o o o o o o o I 0 . . . . . . . LLJ :..!* <I: LLJ 0.. 3160 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 LOW MeasureMent Date/TiMe -0 \jJ Vt 0 ....., Vt 00 0 \0 QA filenafYle ParafYleter Narrie Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B001.QAF;5 BACKRATE (Background Rate) 4-MAR-2016 16:29: 27 through 28-SEP-2016 12:00:00 O.OOOOOOE+OO through 2. OOOOOOE-02 . . . '01 ............................................................................ . . . . . . 0 x x x x x x x x *x x *xxxxx xx 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenaMe ParaMeter Narrie 5 tart I En*d Da*tes Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W002.QAF;8 AVRGEFF (Average Efficiency) 4-AUG-2016 14:49:25 through 28-5EP-2016 12:00:00 0.262337 through 0. 278564 I 275 ' ' ' * * ' ' ' ',' ' o ' o o ' ' o ', o o ' ' ' o o 1 ',' ' o ' ' ' ' ' 1 1o' ' ' ' ' ' ' ' '.' o ' ' ' ' ' ' ' ',' I O ' ' ' ' o o: o o o o o o o , o >>" (..) c I}) *r-1 (..) *r-1 4-4-LU . 27 x x x x x x x o o I o o o o . 265 ............................................................................ . . . . . . . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurerrient Date/TiMe UP LOW -0 w -....) 0 Hi Vt 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.W]W002.QAF;8 ParaMeter NaMe NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 4-AUG-2016 14:49:25 through 28-5EP-2016 12: 00:00 Lower/Upper LMts: 184.000 through 204.000 UP 200 0 I 0 I o I I o o o o o o o o I I o o o o I I o o o I I o o o I I o o o o

o o o o I o o o o o I o o
I o o o o I I o o o o I 0 o o I o o Io o 0 I I . . . . . . . I 0 (!) )-I-H > H I-u a: x w D H _J u :J z
x x 190 . . . . . . . I I o o o I o o 0 0 o 0 o o o o o o o o o I I o o o o I o o o I I o o o o o o o o o I o o o o o I 0 o o o o 0 ' I I I o o 0 ' 0 o o o o I Io o o o I o x 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 LOW MeasureMent Date/TiMe

-0 w 00 0 H) Vl 00 0 ID QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W002.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14:49:25 through 28-5EP-2016 12:00: 00 5. 00000 through 100.000 ...... I Cl (!) z 0 H ::::::i ....I 0 ff) w O:'. ::..! a: w 0... 100 80 ......... * .................... * .......... * ......... * .......... * ......... : ........ . . . . . . . . 60 ............................................................................ . . . . . . .

40 x x . . . . . . . . X . . . . . . . :. . . . . . . . .. : . . . . . . . . . :. .. >:-. . . . . .: . . . . . . . .. :. . . . . . . . . .: . . . . . . . . . . . . . . . *X . 20 ................... ' .............................. , ............................ . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W002.QAF;8 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-AUG-2016 14:49:25 through 28-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . . 3200 ' ' ' o 0 o I o I 0 0 I 0 o o o I o o o o 0 I o I I o I o o o I o o o o o o o o o o I o o 0 o o 0 o o 0 I I o o o o I 0 o o o I o o o o o o 0 o o I 0 o . . co v ..-! I D (!) )-" (!) 0::: Jj'¢( x x x w 3180 z . . . . . . . I I 0 o o o o o o o I I o o o I I o o o o I o o o o
o 0 o I o 0 o
o o I o 0 o o I o o *
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o
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o I 0 0 o I I o
o o o *
0 o r o o . . . . . . . w ::...:: a: w CL 3160 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B002.QAF;2 ParaMeter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:27 through 28-5EP-2016 12: 00:00 Lower/Upper Lmts: O.OOOOOOE+OO through 2.000000E-02 UP . . . . .01 ............................................................................ . . . . . . LOW Measurement Date/TiMe 0 ...., Vl 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: '275 :>, (.) c ID *r-f (.) *.-1 4-4-UJ DKA100: [ENV_ALPHA.QA.W]W003.QAF;9 AVRGEFF (Average Efficiency) 10-AUG-2016 10:56:03 through 28-SEP-2016 12:00:00 0. 263000 through 0.279270 x ID "OJ) . 27 . . . . . . . . . . *. . ::<. . . . . . . . . . . . . . . . . . . .. . . . . . . . ... *. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : . ((i J-ID > a: x x x x* I 265 1 1
1 1 1 1 1 1 ',' 1 ' ' 1 o 1 ' 1 ' ',' ' ' ' ' o ' 1' ' 11' 1 1 1 1 1 ' o o 1 .' ' o 1 ' ' 1 ' ' ' ',' ' ' 1 1 1 1 o ' 1 11 o' 'o 1 ' o' ' 1 ', o x UP 8-10 8-17 8-24 8-31 9-07 9-14 9-21 9-28 LOW Measurerrient Date/Tirrie

-0 N 0 >--+) Vl 00 0 \0 QA filenaf"l'le Paraf"l'le ter Naf"l'le Start/End Dates Lower/Upper Lf"l'lts: DKA100: [ENV_ALPHA.QA.W]W003.QAF;9 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 10-AUG-2016 10:56: 03 through 28-SEP-2016 12:00:00 184. 000 through 204. 000 200 ' ' o ' o I 0 o o 0 o o o o o o o o o o o o 0 o 0 o o ' o o o o o o o o 0 o o o o o o o o o e o o 0 o 0 0 ' o o o o o o o o 0 I 0 o o o o o o o o o o o I Cl (!) H > H u a: llJ Cl H ....I u ::i z . . . . . . . x x*

190 >:: ......... * ........... * ........... * .......... * .................................... . UP 8-10 8-17 8-24 8-31 9-07 9-14 9-21 9'-28 LOW Measuref"l'lent Date/Tif"l'le QA filenaMe DKA100: [ENV_ALPHA.QA.W]W003.QAF;9 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Date8 10-AUG-2016 10:56: 03 through 28-SEP-2016 12: 00:00 Lower/Upper LMt8: 5.00000 through 100. 000 ..-i I 0 (.') z 0 H 1-::J ....I 0 (J) l.LJ O'.: ::..::: a:* l.LJ 0... 100 80 . . . . . . . . . . *. . . . . . . . . . . . . . . . . . . . . . ,* . . . . . ..... *. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : . . . . . . . . 60 o o o o o o I o o ' 0 o 0 o o o o 0 o o o o o o o o o o o o o o O o o o o o o o o o I 0
o o o o o o o o o o o o o o o o o I I O O o o o o o o o o o o . . . . . . . x x x* . . . . . 40 ............................................................................ . . . . . . . 20 ............................................. , .......... " ......... " .......... '. UP 8-10 8-17 8-24 8-31 9-07 *9-14 9-21 9-28 LOW MeaBureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.W]W003.QAF;9 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 10-AUG-2016 10:66:03 through 28-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . . ............................................................................ . . co ""'" ...; I D (!:) )-(!:) O:'. x x x: x w 3180 z . . . . . . . ............................................................................ . . . . . . . w ::..:: a: w CL 3160 8-10 8-17 8-24 8-31 9-07 9-14 9-21 9-28 LOW MeasureMent Date/TiMe

-0 Vl 0 Vl 00 0 l.O QA filenaMe DKA100: [ENV_ALPHA.QA.B]B003.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 5-AUG-2016 14:06:41 through 28-SEP-2016 12:00:00 O.OOOOOOE+OO through 2. OOOOOOE-02 . . . . . . 01 ............................................................................ o xxx 8-05 . . . . . . . x :x *x 8-12 8-19 :x 8-26 :x 9-02 :x 9-09 MeasureMent Date/TiMe :x *x 9-16 9-23 UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W004.QAF;11 AYRGEFF (Average Efficiency) 4-AUG-2016 14: 49:25 through 28-SEP-2016 12:00:00 0. 281866 through 0.299302 x . 295 ......... * .................... * .......... * ......... * .......... * ......... : ........ . (j c I])* *.-i (j *.-i 4-4-UJ ID "0.0 l(i I-I]) > a: x x . . . . . . . x . 29 ............................................................................ . . . . . . . x I 285 *

0 0 0
0 0 0 ,* 0
0 0 0 0 0 0 *, 0 0
0 0 0 0 * * ,* 0 0 *
0 0 0 0 *, 0 0 0 0 0 0 0 0 0 ."
0 0 0
0 0 0 00 0 0 0 0 0
0 0 0 : 0
0 0 0 0 0
0 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Parar.-.e ter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W004.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-AUG-2016 14: 49:25 through 28-5EP-2016 12: 00:00 184. 000 through 204. 000 200 ' ' ' o o ' o o ' o o I ' o 0 0 o 0 0 0 o 0 I 0 0 o o I o o 0 o o o 0 o o o o o 0 o o 0 o o o I 0 o 0 ' 0 I o o o I I 0 0 o I o o o o o 0 0 o o o I I o I 0 C!:I )-I-H > H I-u a: w 0 H _J u ::i z x x< x . . . . . . . x x 190 . . :x:* . . . . . :* . . . . . . . . *: . . . . . . . . . :* . . . . . . . . *: . . . . . .... : . . . . . . . . *: . . . . . . . . . : . . . . . . . . . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurer.-.ent Date/Tir.-.e UP LOW

...... 0 +:>. 00 0 ....., Vl 00 0 ID QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W004.QAF;11 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 4-AUG-2016 14:49:25 through 28-5EP-2016 12: 00:00 5. 00000 through 100.000 ""'"" I Cl (!) z 0 H 1-:J 0 en l.LJ O:'. cr: l.LJ 0... 100 80 . . . . . . . ............................................................................ . . . . . . . 0 0 o ' 0 o I o o o o o o o o o I o o o o I o o o 0 o 0 o 0 0 I 0 0 o o o o I o o o o I o o o o 0 0 o o I I o o o o o o o o 0 I 0 o 'o o o o o o o o o -. . . . . . . x x . . . . . 40 o o o o o o o o o o o o o o 0 I ' o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ' o 0 I o o o I I o o o o I o o o o I I o . . . . . . . 20 ......... *' ........ ' ................... '* ......... , ................... ' ........ . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 MeasureMent Date/Tirrie UP LOW QA filenaMe ParaMeter Nafl'le Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W004.QAF;11 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-AUG-2016 14:49:25 through 28-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . . 3200 I I O O O I 1 O O O O 1 o o O 1 1 o o o o 1 o o o o 1 1 o O o 1 1 o o o o I O o O O O O O o o I I o o o I o o o o o o o o o I o o o o 0 I o 0 0 0 I 0 0 . . . . . . co v ..-I I D )-0:: x x w. 3180 z . . . . . . . .......... ' ' ............................................................... . 0 I I 0 o o o w :. 0 c 11) *r-1 x x 0 *r-1 4-4-UJ . 29 * * * * * * * * *:-* * * * * * * *: * * * * * * * * * :-* *x* * * * * *: * * * * * * * * *: * * * * * * * * -:* * * * * * * * *: * * * * * * * *

x x x . . . . .285 I I o o o o o I o o 0 o 0 o o 0 0 o o o o I o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o o 0 I 0 0 o 0 0 0 o I 0 I 0 0 Io 0 0 o . . . . . . . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 MeasurefY'tent Date/TifY'le UP LOW QA filenarrie Pararrie te*r NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W005.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-AUG-2016 14:49:25 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ........ *.* ........ * ........... * ........ * .................... * .......... : ........ . I D (!) )-I-H > H I-u a: w D H __. u ::i z 190 o o o o o o o O o *, o I O o o I O o .. o O o I o O o I I 1o o O O o o o o I 1° o o o o o o o o o 01 o 0 0 0 0 0 o 0 o' I I o o 0 I I o o: o o o o o o o I o x x x 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 MeasureMent Oate/Tirrie UP LOW QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W005.QAF;11 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 4-AUG-2016 14: 49:25 through 28-SEP-2016 12:00:00 5.00000 through 100.000 ..-i I Cl (.') z 0 H 1-::J _J 0 en w ct: a: w 0... 100 * . 80 .. X ...... * ......... ' ......... * .. *X* ..... * ......... * .......... * ......... : ........ . x . . . . . . . x x . . . . . . . 60 . . . . . . . ...... ' ............................. ' ...................................... . . . . . . . . . . . . . 40 o I 0 o o 0 o o o o I I o o o I I o o o o I I o o o o I o o o o I o o o 0 0 o o o o I o o o o o o o o o o o o o o I I o o o O o o o o o o o o o o I o o o I I ' o o I 20 ...... ' ..... ' .... ' . ' ................... '* ......... , ................... ' ........ . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 MeasureMent Date/TifY'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,W]W005.QAF;11 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 4-AUG-2016 14: 49:25 through 28-5EP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . . o I 'e o ' ' o o o I I o o o o ' o o o o I 0 o o o o o o o o o 0 o o o o o o o o o I o o o o I o I 0 o I o o I o I I o o o I I o o o o I o I 0 o I o I . . . . . . . co ""'" ..-I I D (!) )-C) Q'. x x w 3180 z . . . . . . . ............................................................................ . . . . . . . w ::..:: -+, Vi 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B005.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:27 through 28-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2. OOOOOOE-02 . 01 ......................................................................... : .. . . . . . . :x X X x X X X X* X X X X X X x X X X X x: x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-0 Vl 0\ 0 ....., Vl 00 0 ID QA filenal'le Paral'leter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W006.QAF;8 AVRGEFF (Average Efficiency) 4-AUG-2016 14:49:25 through 28-5EP-2016 12:00:00 0.261500 through 0. 280200 '28 o ' 0 o o 0 o 0 0 o' I o o 0 o I o 0 ', o o o o o o o o o ,' o o o o o o o o ', o o o o o o o o o .. I o o o o o o o ', o o o o o o o o o: o o o o o o I o 0 '275 :::-, 0 c Q) -r-1 u -r-1 4-4-LU Q) '27 Wl ill x Q) > a: x '265 . . . . . . . 0 0 o o o 0 o o o o o 0 o o o I I o
o o o o o 0 o o 0 o o 0 ' o o

0 I I o 0 o o 0 o I o o ' I o o o I o o o o o o o o o o I o o o o I o o o 0 I I

x x 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurer.-.ent Date/Tir.-.e UP LOl.i.J QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W006.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-AUG-2016 14:49: 25 through 28-SEP-2016 12: 00: 00 184. 000 through 204. 000 200 .......... * ........ * ........... * ........ * .................... * .......... : ........ . I 0 )-I-H > H I-u a: w 0 H ...J u :J z x

x x x 190 ........ * .................... * .......... * ......... * .......... * ......... : ........ . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 Measurerrient Date/Tirrie UP LOW
-0 Vl 00 0 ......, Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W006.QAF;8 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 4-AUG-2016 14:49:25 through 28-SEP-2016 12:00: 00 Lower/Upper LMts: 5.00000 through 100.000 I Cl (!) z D H 1-::i ....I D (f) w O:'. :::.! a: w 0.. 100 80 ......... * .................... * .......... * ......... * .......... * ......... : ........ . .;{-: : : x : : : : 6 0 . . ;x. . . . . . . . . . . . . . . . : . . . . . . . . . *. . . . . . . . . : . . . . . . . . . *. . . . . . . . . . . . . . . . . . . . : . . . . . . ,:x; . x . . . . . . . x . . . 40 ............................................................................ . . . . . . . 20 ................... ' .............................. , ............................ . 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 MeasureMent Date/TiMe UP LOW -0 Vl \0 0 ......, Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W006.QAF;8 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Date8 4-AUG-2016 14:49:25 through 28-SEP-2016 12:00:00 Lower/Upper LMt8: 3143.00 through 3223.00 UP 3220 3200 o I o 0 I I I ' o I I I 0 ' I I I o I I I I o I o o o o o I o o I I I o o o o o o o o I o I I o I I o o I I I o I o I o o I o o I I o I I I I I I Io o o I 0 o o I 0 . . . . . . co tj" ..i I D }-et:: f@< x x x UJ 3180 z . . . . . . . ............................................................................ . . . . . . . UJ :,.,,:* a: UJ 0.. 3160 8-04 8-11 8-18 8-25 9-01 9-08 9-15 9-22 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B006.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Datea 4-MAR-2016 16:29:27 through 28-SEP-2016 12:00:00 Lower/Upper LMtB: O.OOOOOOE+OO through 2. OOOOOOE-02 UP . . .01 ............................................................................ . . . . . . LOW MeaaureMent Date/TiMe ...... 0 0\ ...... 0 ....., VI 00 0 \0 QA filenafY'le ParafY'leter NafY'le Start/ En*d Da*tes Lower/Upper LMts: .275 DKA100: [ENV_ALPHA.QA.W]W007.QAF;7 AVRGEFF (Average Efficiency) 30-AUG-2016 10:09: 38 through 28-SEP-2016 12:00:00 0.260930 through 0.277070 . . . . u c J1) *r-1 u *r-1 4-4-LU '27 ........................................................................... J1) 'OIJ ((i Q) > a: x: X* x x :x I 265 *
o * * ' * * * * * ' * * * *

I * * * ' * * * * * * * * * * * *

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8-30 9-06 9-13 9-20 9-27 MeasureMent Date/TifY'le UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W007.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 30-AUG-2016 10:09:38 through 28-SEP-2016 12: 00:00 184.000 through 204.000 200 o o O O o I O o O o o o o o o o o o O o O O O o o o o o o o o o o o O O O I o o o o o o 0 o o I O o O o o o o o o 0 I 0 0 0 I I o o o o o o 0 0 o I 0 o I 0 (!)" )-1-H > H 1-u a: LLJ 0 H ....I u ::i z . . . . x X* x 190 . . . . . . . . . . . . . . . . . : . . . . . . . . . . . . . . . .><: ; . . . . . . . . . . . . . . . . . : . . . . . . . . . . . ...... ; ?<. . . x 8-30 I 9-06 9-13 9-20 9-27 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W007.QAF;7 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 30-AUG-2016 10:09:38 through 28-SEP-2016 12:00:00 Lower/Upper 1LMts: 5. 00000 through 100. 000 ...i I Cl z 0 H ::J _J 0 ([) w Ct'. :...:: a: w 0... 100 80 60 40 o o o o o o o o o o o o o o o O I : O o O O I I o o o I o o o I o o o: o o o o 0 I I 0 0 0 o I I 0 0 0 I : 0 o o I I o I I I I o o I o I o o: I I o I . . . . O I o o O o I o o o o I I o o o I *o o o o I o o o o I I o o o 0 o o 0 0 I I 0 0 o 0 I I 0 0 o 0 I o I o I I o I o 0 I o I o o o 0 0 o o o o o o I I I o x x . . . . . x* x: x :x 1 o o o o O o o o O O I O O O I I O O O o I O o o o o o o o o I I o 0 o I I 0 0 0 o I I 0 0 0 I I 0 0 I I I 0 0 0 I I o 0 0 I I o o o o I o I o I I I o . . . . 20 ................. ' ................. ' ................. ' ................. ' . : .. 8-30 9-06 9-13 9-20 9-27 MeasureMent Date/TiMe UP LOW
...... 0 0\ ..j:>. 0 ......, Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W007.QAF;7 P5ENERGY-GD148 (PEAK ENERGY GD-148) 30-AUG-2016 10:09:38 through 28-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . 3200 o o o o o ' ' o o o o ' o o 0 o I o 0 0 o I I 0 0 0 I I 0 o O I O O o o I I o o o o o o o 0 o I I O O O I o o o o O I o o o I I o o o o o o o o o o o o . . . co v ..-! I D (!) }-(!) et:: x: x .x LLJ 3180 z . . . . o o o o o o o o o o I o o o o o o o o o o I 0 o o 0 o I 0 o o I I o o o O o o o o o I o o o o I O O O O I O O o o I O o o O I o o o o o o o o o o o o o . . . . LLJ a: LLJ 0.. 3160 8-30 9-06 9-13 9-20 9-27 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B007.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16: 29:28 through 28-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 x 400 . . . . . . ............................................................................ . . 300 200 . . . . . . . ............................................................................ . . . . . 100 .......... * ....................... ' ........... * ...................... ' ......... . UP MeasureMent Date/TiMe -0 0\ 0\ 0 >-+, Vt 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W008.QAF;6 AVRGEFF (Average Efficiency) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 0.318710 through 0. 338420 . . . . . '335 o o o o o I I o 0 o I I o o I I I o o o o
I o o o o o o o o o o o o o I I 0 0 I o I o 0 I 0 o o I o o o I o ' o ' I o I ' I I 0 o 0 o 0 0 o 1 0 I 1 o >, 0 c ID *.-! 0 *.-! 4-4-LL.J ID "0.0 (lj ID > <I: . . . .. . .33 *x . . . . x . x '325 ............ * ............. * ............. * .......... X .. * ............. * ........... . x: x I 32 * *

0 * * *

0 * * * ,* 0 * * * * * * * * * * * ,* * * * * * * * * * * * *,

0

0 0 * * * * * * * *, 0

0 0 0 0 0

0 0 0 * *, 0 0 0 0 0 0 0 0 0 *

0 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W008.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:48:19 through 28-5EP-2016 12: 00: 00 184.000 through 204.000 200 o ' o o o 0 ' o o o 0 0 o o o o o o o o o o 0 o 0 0 0 o o o o o o o o o o I e' o o 0 o o o o o o o o o o ' o o o 0 I o o o o o o o o o o o o o o o o o . . . . . I D )-I-H > H I-u <I: w D *X x x H _J x: u ::i x z 190 . . . . . ......................................................... ' ................. . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
,_. 0 °' 00 0 ....., Vl 00 0 \0 QA f i lenaMe
ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W008.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00: 00 6.00000 through 100.000 80 ............ * ............. * ............. * ............. * ............ ,* ........... . ,,-! I D C) z 0 H ::i ....I 0 (J) w 0::: :::..::: a: w 0.. . . . . . 60 ............................................................................ . . . . . x: :x x x x x . . 40 o o o o o o o o o o o o o o o o o o o o o o o o 0 o I o o o o I o o o o o o o o o o o o 0 o o I o o o_o o o o o o o o o o o o o o o o o o o o I o I 0 0 . . . . . 20 ....................................... " .......................... " ........... . 4-16 6-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-0 0\ \0 0 ......, Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W008.QAF;6 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 1-APR-2016 08:48:19 through 28-SEP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . ' . I o o o o I I o o o I o I o o I o o o o o I 0 o 0 o I o o o o I o o o o ' 0 0 o o o o o o o o o o o o o 0 I o o o o o o o o 0 o o o o o I ' 0 o o I I o . . . ro tj" -.-I I 0 (!) )-(!) 0::: :x x: x x x w 3180 z . . . . o o o o o ' o o o o o 0 o o o o o o o o o o I o o 0 0 o o o o o o o o o o o 'o o o o o o o o o o o o ' I 0 o 0 o o o o o o o o o o o o o o o' o I o o . . . . . w ::...:: a: w a... 3160 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ...... 0 -.J 0 0 ...., V'I 00 0 \0 .. QA filenaMe DKA100: [ENV_ALPHA.QA.B]B008.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16: 29:28 through 28-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . 01 ............................................................................ . . . . . . x x x x X-x x x x x x x x x x *x x x x: x x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenarrre Pararrreter Narrre 5tart/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W009.QAF;7 AVRGEFF (Average Efficiency) 30-AUG-2016 10:09: 38 through 28-5EP-2016 12: 00: 00 0.308850 through 0.327950 . . . . .325 ............................................................................ >:. u c ID *r-1 u *r-1 4-4-LLI ID 'OIJ ((i i:-ID > <I: . . . . . 32 ' o o o o 0 0 o o o o o o o o I I o o 0 o o I o o o 0 0 I o o I 0 o 0 0 0 I 0 o o o 0 o o 0 o o 0 o o o o I o o o o o o o o o o o o o o o o o o o o o o x x .315 .31 8-30 9-06 x: x* 9-13 Date/Tirrre 9-20 x *X 9-27 UP LOW ...... 0 -...1 N 0 ......, Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W009.QAF;.7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 30-AUG-2016 10:09:38 through 28-SEP-2016 12:00: 00 184.000 through 204.000 200 I I I I I I I I I I I I I I I I I I I I I o I I I I 0 I I O O O I I o I I I o o o o I o o o o 1 o o o o I I I o o O I o I o I I o o o o 1 o o o o 1 1 o I Cl (!) H > H 1-u a: LlJ Cl H ...J u =i z . . . . .x x; x x 190 ?< ................ : ......*.......... : ................. : ......*.......... : ... . x* 8-30 9-06 9-13 9-20 9-27 Measurer.-.ent Date/Tir.-.e UP LOW ..l V.l 0 ....., VI 00 0 \0 QA filenaMe ParaMeter NaMe 5fart/End Dates Lower/Upper LMts: 1DO DKA100: [ENV_ALPHA.QA.W]W009.QAF;7 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 30-AUG-2016 10:09:38 through 28-5EP-2016 12: DO: OD 5.00000 through 100.DOO 80 0 o. *
0 0 I o o o o o o o o o o : o o o o ' o o o o o o o o o o o o : o o o o o 0 o o o 0 o 0 0 o o o 0 : o o o I o o o o o o o o o o ' o o : o o o o .-I I Cl 8 z 0 H ::i ....I 0 en w 0::: ::..:::. c.I w 0... . . . . 60 o o o o o o o o I o o o o o o o o o o o I o o o o o o 0 o o 0 I 0 o o o ' o 0 o o o o o o I o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o . . . . x *X . . 40 ............................................................................ . . . . 20 ................. ' ................. ' ................. ' ................. ' ... . 8-30 9-06 9-13 9-20 9-27 MeasureMent Date/TiMe UP LOW
,_. 0 0 ......, Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W009.QAF;7 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 30-AUG-2016 10:09:38 through 28-SEP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . .......................................... ' ................... ' ............ . . . co '<it ...... I D (!) )-(!) et:: x :x l.J.J 3180 z . . . . ............................................................................ . . . . l.J.J :::.! a: l.J.J 3160 8-30 9-06 9-13 9-20 9-27 LOW MeasureMent Date/TiMe QA filenaf'l"le Paraf'l"leter Naf'l"le Start/End Dates Lower/Upper DKA100: [ENV_ALPHA.QA.B]B009.QAF;2 BACKRATE (Background Rate) 31-AUG-2016 12:42:17 through 28-SEP-2016 12:00:00 O.OOOOOOE+OO through 2. OOOOOOE-02 '01 ............................................................................ 0 x 8-31 . . . . . . . . . x x. x x x . x 9-03 9-06 9-09 x 9-12 9-15 9-18 MeasureMent Date/Tif'l"le 9-21 x* 9-24 9-27 UP LOW ....J 0\ 0 ,....., Ul 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W010.QAF;8 AVRGEFF (Average Efficiency) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 0.298500 through 0. 316960 I 315 ' O o o o ' o o o o o 'o' o o O o o o o o o o o o ,' ' o o o o I o o o o o ', o o o o I O " o o o o o ', o o I o 0 O I o o o o o ', o o O O o o o o O o o o >.. u c. Q) *r-1 u *r-1 4-4-LU Q) 'QI) Ill Q) > cr: . 31 x x* x . . . . . . 305 ............................................................................ . . . . . *x I 3 ' ' o o o 1 ' o o o o 1 o' 0 o o ' o o o o ' ' o o *' ' ' o o o ' 1 o o o ' o, o o o o ' o o o o ' ' 0 o, o 1 ' o o o ' ' o o o ' '* o o o o o ' o o o 1 1 o 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W010.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ............. * ............. * ........... * ............. * ............. * ............ . I 0 (!) )-I-H > H I-u x cr: w 0 H ...J x u z 190 ........... *:* ........... *:* .......... x*:* ........... *:* ........... *:* .......... . :x x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ..) 00 0 ......, Vl 00 0 ID QA filenaMe DKA100: [ENV_ALPHA.QA.W]W010.QAF;8 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Date8 1-APR-2016 08:48:19 through 28-SEP-2016 12:00: 00 Lower/Upper LMt8: 5. 00000 through 100.000 ..-i I D C) z D H ::i ....I D (f) w 0::: 100 80 o o o o o o o o o o o o 0o o o o
o o o o I I o o'o o 0 o o o o o o o o o o0 o o o o o o o 0 o I o o o' o o

o o o o o o o o o o' o o o o o o o o o o o o . . . . . 60 o ,* o o o I I o o o o I o o o o I o 0 o o 0 I o 0 0 o o o o o I o o o o o I o o o o ' o o o o o I o o o I I o o o o o o o o o o o o o o o o o o o I I o . . . . . x x x x: *X x . . . . 40 ............................................................................ . . . . . 20 ................................................................................ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W010.QAF;8 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 1-APR-2016 08:48:19 through 28-SEP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . o o o o o o o o o o o I o

o O o o o o o o o o o o o 0 0 o o o o o o o o 0 o o o 0 I o o o o o o o o o o I o o o 0 o o o o o I o o o o o o o o o 0 0 o co ¢ ..,..-! I D )-0:: x: :x x x x 3180 z . . . . . ............................................................................ . . . . . I.LI :...: 0: I.LI CL 3160 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
>-o (l) ...... 0 00 0 0 ......, Vl 00 0 \0 filenaMe DKA100: [ENV_ALPHA.QA.B]B010.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 16:29:28 through 28-5EP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2. OOOOOOE-02 . . . . . 01 ...................... : .......... : ........... * .......... : .......... : ......... . x x x x x x x x x X* x x x x x x x :x x x ?< x x x X *X X x x x* x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 ......, Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W011.QAF;8 AVRGEFF (Average Efficiency) 1-APR-2016 08: 48:19 through 28-SEP-2016 12:00:00 0.306149 through 0.325087 .325 ************:************:************.************************************** UP . 32 . . . . . ............................................................................ . . . . u c J1) *r-1 u *r-1 4-4-UJ J1) '315 o o 0 o I ............................................................................ . . . ' ' "o.O l(i I-J1) *x x > a: x: . . . . x . . 31 ........... -:* ........... *:* ........... *:* ......... ):(. *:* ........... *:* ......... *>:: 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe -0 00 N 0 ......, Vt 00 0 \0 QA filenarrre Pararrre ter Na.rrre Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA,W]W011.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12: 00: 00 184.000 through 204. 000 200 ............. * ............. * ........... * ............. * ............. * ............ . I Cl )-I-H > H I-x* (j a: x ll.J x Cl H _J *x x (j ::i x z 190 ............ * ............. * ............. * ............. * ............. * ........... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... 0 00 (.;.) 0 ......, VI 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W011.QAF;8 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:48:19 through 28-5EP-2016 12: 00:00 5, 00000 through 100. 000 100 UP ...-4 I D C) z 0 H 1-:J ....I 0 ({) w Ct'. 80 ............ * ............. " . ' .......... " ............ " ............ " ........... . . . . . . 60 ........... *.* ........... *.* ........... ',' ........... *.* ......... x *.* .......... . x x x: :x x 40 ' ' o o o ' ' o o o o ' o o o ' ' o o o o ' o o o o ' o o o o ' ' o o o ' ' o o o o o o o o 0 o 0 o 0 0 I 0 o 0 o I I o o o I I o o o o I o o o o o o o . . . . . 20 ............ " ............ " ........... " ............ " ............ " ........... . 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurer.-.ent Date/Tir.-.e -0 00 0 ....., Vl 00 0 \0 QA filenar.-.e ParaMeter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W011.QAF;8 P5ENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08:48:19 through 28-5EP-2016 12:00:00 3143.00 through 3223.00 . . . . . 3200 o 0 0 o o o o o o o o o o o o 0 o o o o o o o o o o o o o o ' I 0 0 o o o o o o o o I o o o o o I o o 0 I I o o o I ' o o o I I 0 0 o o I o o o o o I o . . . . ro "'1" "'""" I D )-0::: :x x: x x x LLJ 3180 z . . . . . o o 0 o
o 0 o o o I o o o o o 0 o o o 0 I I 0 o o o I o o o o I o o o I ' o o o o I o o o o 0 o o o o I I o o o I I o o o I o o o o o I o o o o I I o . . . . . LLJ ::...: a: LLJ 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
-0 00 Vl 0 I-+) Vl 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B011.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:28 through 28-SEP-2016 12:00:00 L6wer/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP '01 ............................................................................ . . . . . . x *.x x x x x X X X
X X X X" X X X X X X X X X x: X X X X *X X 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenafY"te Parameter NafY"te 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA,W]W012.QAF;7 AVRGEFF (Average Efficiency) 1-APR-2016 08: 48:19 through 28-5EP-2016 12: 00: 00 0.285746 through 0.303420 . . . . . . 3 o o o o o o o o o o o o o 0 0 0 0 o o o o o o o o o ' o o o o o o o o o o I 0 0 o o I o o o o o o o o o o I o 0 ' 0 I o o o o o o o o o I o o o o o I o tl c 0) *r-1 tl *r-la 4-. 295 4-. . . . . I 0 0 I o 0 I I I o 0 o o o o I I o o I o o o o o o o o o o o 0 o o o ' I o o o o o o o o o o 0 o 0 ' I o I o I o I I o o o o o o ' ' o o o o o o o o o . . . . . UJ 0) '0.0 x x x (lj !-x 0) > a: :x x: . 2"9 . . . . . .. -......................................................................... . . -* . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY"le UP LOW
....... 0 00 -..J 0 ....., Vt 00 0 "' QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA.QA.W]W012.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12: 00:00 184.000 through 204.000 200 ............. * ............. * ........... * ............. * ............. * .......... : .. I D (!) )-f-H > H f-u a: w D H ....J u x ::i z x 190 ............ :* ............ ?< ........... *: ............ *: ............ *: ........... . X* x 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/Ti!Yle UP LOW ..... 0 00 00 0 >..;., Vl 00 0 "° QA filenaMe Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W012.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 5.00000 through 100.000 80 ............ * ............. * ............. * ............. * ............. * ........... . ..... I Cl z 0 H 1-:J ....I 0 ({) w (}'.'. ::..::: a: w 0... . . . . . 60 I I o o 0 I o o o o o o ,' o o o o o o o o o o o o ,' o o o o o o o o o o o ', o o 0 0 I o 0 o o o o o ', o 0 o o o o o o o o e o ', o o o 0 0 o o 0 o '* o e x: *x x x x . . . . . 40 o o o o o o o o o e I I o o o I I o o o o I I o o o I I o o o o o o o o I I 0 e o e 0 o o o o I o o o o I o o o o o I o o e o o 0 o o o I o o 0 o I o o . . . . . 20 ................................................................................ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ,_. 0 00 ID 0 ....., Vl 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W012.QAF;7 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . 3200 .......................................................... ' ................ . ro ""'" ........ I D (!:I )-(!:I O:'. :x x: x x x LL.J 3180 z . . . . . ............................................................................ . . . . . LL.J . ::,.:: a: LL.J 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... 0 \0 0 0 ......., Vi 00 0 ID QA filenaMe DKA100: [ENV_ALPHA.QA.B]B012.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:28 through 28-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . 01 ................................................. -......................... . . . . . . . x x x x x x x x x x x :x x x x x x x* x x X X X *X X X X x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe 0 ....., Vl 00 0 \0 QA filenarrie Pararrieter Name Start I End Da.tes Lower/Upper Lmts: ::::-, u r: DKA100: [ENV_ALPHA.QA.W]W013.QAF;4 AVRGEFF (Average Efficiency) 1-APR-2016 08:48:19 through 28-SEP-2016 12: 00: 00 0.338564 through 0.359506 x. ?< Q) *r-1 u *r-1 4-4-LU . 35 ............ * ............. * ........................... * ........... x .............. . .x x x . 34 ..................... ' ..................................................... . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW -0 '° N 0 ....., Vi 00 0 '° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W013.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ............. * ............. * ........... * ............. * ............. * ............ . I o. (!;I >-..... H > H ..... u a: x. w 0 H ....I u ::i :x x z 190 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . x x 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W013.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:48:19 through 28-5EP-2016 12:00: 00 5.00000 through 100. 000 . . . . . 80 ............................................................................ ..-1 I D C) z 0 H 1-=i ....I 0 (f) w O:'. . . . . . 60 ...... ' ........................................... ,* ........................ . . . . . . *X x x x x. 40 x I ' o o o o o o o o o 0 o o 0 I I o 0 o o I 0 0 o o I I 0 o 0 I o 0 o 0 I o o o o o o o o o o o o o o o o o o o o I I o 0 o 0 o o o o ' 0 o o o o 0 o o . . . . . 20 ....................................... '* .......................... '* ........... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W013.QAF;4 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 1-APR-2016 08: 48:19 through 28-SEP-2016 12:00:00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . o o o o o o o o o o o o o o o o I o o o o O I O O O O I O o O O O O o o I I o o o o O o o o o o o o o o o o o o 0 o I o 0 0 I I o 0 o o 0
0 o 0 o I o . . . . . ro v "<""I I D )-0:: :x x: x x x w 3180 z . . . . . ............................................................................ . . . . . w lo.:: <I: w 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
...... 0 \0 Vl 0 H) Vl 00 0 'Cl QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: ID .lo) J1j O:'. -a c-DKA100: [ENV_ALPHA.QA.B]B013.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 16:29: 29 through 28-5EP-2016 12:00: 00 0, OOOOOOE+OO through 2.000000E-02 ::J ' 01 .......... * ........... : .......... : ........... * .......... : .......... : ......... . 0 5-'0.0 (.) J1j [I) 4-16 5-16 x x x . x x x x x x x* x x x x *x .x x . . x x 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW -0 "° 0\ 0 ....., Vl 00 0 "° QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W014.QAF;8 AVRGEFF (Average Efficiency) 1-APR-2*016 08:48:19 through 28-SEP-2016 12:00:00 0.320100 through 0.339600 . 335 ' ' o o o ' ' o o o o ' o o o o ' o o o o ' ' o o o ' ' o o o o o o o o ' ' o o o ' ' o o ' o I 0 0 o o I 0 0 o o 0 o o o o o o o o o o o o o o o I I o . . . . . . . . . . . 33 * * * * * * * * * * * *:X ........... *:* ........... *: ............ *: ............ *:* ......... *x x x: x . 325 . . . . . . . . . . . . : . . . . . . . . . . . . . :. . . . . . . . . . . . .: . . . . . . . . . . >.< . .: . . . . . . . . . . . . . : . . . . . . . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -0 \,Q -.) 0 ......, Vt 00 0 '° QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W014.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:48:19 through 28-5EP-2016 12:00:00 184.000 through 204.000 200 ............. * ..*.......... * ........... * ............. * ............. " ........... . I 0 )-I-H > H I-u a: :x w 0 H ....I u ::i x x X* z 190 . . . . . . . . . . . . . . . . . * ............. * ............. * ............. * .......... x ............. . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Paraf"l'le ter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA,W]W014.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12: 00:00 5.00000 through 100. 000 80 ............ * ............. * ............. * ............. * ............. * ........... . ....... I 0 (!) z D H 1-::i .....I D (f) w O:'. ::.! a: w CL. . . . . . 60 ............................................................................ . . . . . x *X x x* x x . . 40 o ' o o o o o 0 o o o o o o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o I o 0 o 0 o o o o o o o o o o I o o o o 0 o o o o o o o o o o o o o . . . . . 20 ................................................................................ . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ....... 0 \0 \0 0 ....., Vo 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W014.QAF;8 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . ' 3200 o 0 o o o 0 0 o o o o o o o o I I o o o o 0 0 0 0 o I o o o o o I o o o o I o o o o I o o o o o I o o o I o o o o ' o o o o o o o I o o o o o o o I o 0 . . co '<T ""'"" I D (.') )-(.') Ct: :x x: x x x LLJ 3180 z . . . . . I I o o o I I o
o I I o 0 o 0 I o o o o I I 0 0 0 I I o I I o o o o o I I o o o 0 o o o o o I o o o o o I o o o o o o o o o I o o o o o o o o o I o o . . . . . LLJ a: LLJ 3160 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... ...... 0 0 0 Hi VI 00 0 'Cl QA filenaMe DKA100: [ENV_ALPHA.QA.B]B014.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:29 through 28-SEP-2016 12:00: 00 LMts: O.OOOOOOE+OO through 2.000000E-02 . . .01 ................................................... -....................... . x x 0 3-16 x . . . . . . x *x x x x x x x x x x x x: x x :x x x x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....-0 ....-QA filena!Yle Pararrieter Na!Yle Start/End Dates Lower/Upper Lrrits: . 335 DKA100: [ENV_ALPHA.QA.W]W015.QAF;6 AVRGEFF (Average Efficiency) 1-APR-2016 08: 48:19 through 28-SEP-2016 12: 00:00 0.319700 through 0.339450 x :x x: x . . . . . x 0 l]f *r-1 0 *r-1 4-4-UJ . 33 0 I o o o 0 0 o o o ' o o o o o o o o o o 0 I 0 o o 0 o o o o I I o o o o o o o o o 0 0 0 0 o I I o o o I o o o o o I o o o o o o o o o o o 0 o 0 0 o o . . . . . .325 . . . . . I 32 ° 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 -, 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ' 0 0 0 0 1 0 0 0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Ylent Date/Ti!Yle UP LOW ,_. ,_. 0 N 0 ......., Vl 00 0 l,C) QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W015.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ............. * ............. * ........... * ............. * ............. * ............ . I 0 (!) )-1--H > H I-u <r: w 0 H _J x* x x u ::i z 190 . . . . . . . . . . . . . . . . . *X .......................... * .......... X .. * ......................... . x 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOuJ QA filenaMe Pararrieter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W015.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12: 00: 00 5.00000 through 100.000 .-I I Cl z 0 H ::i ....I 0 (j') w Ct'. :::..::: a: w 0.. 100 80 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . -. . . . . 60 o o o o o o o o o o o O o o o o o o o o o o o o o o o o o o o o o o 0 o 0 o 0 o 0 0 I 0 o 0 0 I 0 0 o o I I 0 0 o I I 0 0 o o I 0 0 o o 0 o 0 o o 0 o 0 . . . . . :x x x x x x: 40 ......................................................... ' ................. . . . . . . 20 ................................................................... '* ........... . 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/TiMe UP LOW --0 .j::.. 0 ....... Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W015.QAF;6 PSENERGY-00148 (PEAK ENERGY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 *3143.00 through 3223.00 12:00:00 3220 ................................. * ............................................... . 3200 . . . . ' ............................................................... ' ........... . . . . . . co v """' I D )-Ct: :x x: x x x LLJ 3180 z . . . . . .................................................... ' ...................... . . . . . . LLJ ::..:: a: LLJ Q. 3160 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ..... ..... 0 Vi 0 ......, Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B015.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:29 through 28-SEP-2016 12:00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP .01 ............................................................................ . . . . . . x x X X* X x x x x x x x x x x x x .x x x x x X *x x x x x x 4-16 8-16 0 3-16 9-16 LOW 5-16 6-16 7-16 MeasureMent Date/TiMe ....... ....... 0 O"I 0 ....., Vi 00 0 \0 QA filenaMe Pararrieter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 1-APR-2016 08: 48:19 through 28-5EP-2016 12: 00: 00 0.329763 through 0.350160 . 35 ............................................................................ . . . . . . . . >., (J c Q) *r-i (J *r-i 4-4-LU '34 ............. * ............. * ........... * ............. * ............. * ............ . x . .x *X x. x . . . I 33 * * * * * * * *
0 *

0 * * * * * * * * * * * * * * * * * * * * * * * * *

0 *

0

0 0 0 0 0 *

0 * * * * * * * * * * * * *

0 0

0 * * * * *

4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
--0 -.l 0 ......, Vl 00 0 '° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W016.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 184.000 through 204. 000 200 ............. * ............. * ........... * ............. * ............. * ............ . I Cl CJ )-I-H > H x I-u CI Ll.J Cl H *x x x x ....I u ::i z 190 o 0 0 0 I ............ * ............. * ........... X.* ............. * ............. * ........... . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW --0 00 0 ....., Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W016.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 6.00000 through 100.000 . . . . . 80 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . -........ I D z 0 H =i ...J 0 en w fl'. ::..::: a: w 0.. . . . . . 60 ............................................................................ . . . . . x x x *X x X* . . . . . 40 ............................................................................ . . . . . 20 ....................................... " ............ " ............ " ........... . 4-16 6-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW --0 "° 0 ....., Vl 00 0 "° QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: 3220 DKA100: [ENV_ALPHA.QA.W]W016.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . 320.0 ............................................................................ . . ro "'" ..-I I D )-Q'. :x x: x x x LLJ 3180 z o o 0 I ...................... ' .............................. ' ..................... . o o o 0 I LLJ :::.! a: LLJ CL. 3160 4-16. 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW ..... ..... ..... 0 0 ....., Vt 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B016.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:29 through 28-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000DOOE-02 '01 ............. -............................................................. . . . . . . . x x xx Xx. x x x 0 3-16 4-16 x 5-16 X X X *X X x x x . x x x x x x x x: x x 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe x x UP LOW

0 H) Vl 00 0 ID QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W017.QAF;6 AVRGEFF (Average Efficiency) 1-APR-2016 08:48:19 through 28-SEP-2016 12: 00:00 0.290113 through 0.320651 . . . . . . 3-2 o ' o o o o ' o o o ' o o o o o ' o o o o ' ' ' o o o ' o 0 ' I 0 o 0 0 0 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ::>, (.) c Q) *ri (.) .,;-4-4-UJ Q) "OJ) i(j s.... Q) > a: . 31 0 o o o 0 0 o 0 I 0 o 0 o 0 o 0 o o o o o o o o o o o o o o o o ' o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o . . . . . x .3 ........... *:* ........... *:* ........... *:* ........ *x* *: ............ *:* .......... . x. .x x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafYle ParafYleter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W017.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-201608:48:19 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ....................................... '. .......................... " ........... . I D )-I-H > H. I-u x: x x Cl: :x w D H x ....I u ::i z 190 ............ * ............. * ............. * ............. * ............ ,* ........... . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW

...... ...... ...... w 0 ....., v. 00 0 \0 QA filenaMe DKA100: ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 1-APR-2016 08:48:19 through 28-SEP-2016 12: 00: 00 Lower/Upper LMts: 5.00000 through 100. 000 .,-! I D z 0 H 1-::i 0 ({) w O:'. :::..! <I w 0.. 100 80 . . . . . ............................................................................ . . . . . 60 ............................................................................ . . . . . 40 . . . . x . . v . x . . x ............. ?<* ........... (" .......... X* ............. * ............. * ........... . 20 ....................................... '* .......................... '* ........... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ---0 ....., Vl 00 0 "° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W017.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . 3200 o ' o o o ' o o o o ' ' o o o ' o o o o o ' ' o 0 o 0 o 0 o 0 I 0 0 o 0 I I o o o 0 I o 0 o o 0 ' o o o o 0 o o o 0 ' o o o ' 0 o o o o I 0 0 o 0 I I 0 . . . . . co v ...-! I D (!) )-(!) 0:: :x x: x x x LLJ 3180 z . . . . . o o o o o o o o o o o o o o o o o o 0 o o o 0 o 0 0 o I 0 0 0 I I o 0 0 I 0 o 0 0 0 I 0 0 o 0 I 0 o 0 o I I 0 0 0 I I 0 0 0 0 0 0 o 0 o o o o o o o o o o o 0 I I LLJ ::..::: a: LLJ 0... 3160 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ....... ....... ....... Vl 0 ....., Vl 00 0 \0 QA filename DKA100: Parameter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16: 29:29 through 28-SEP-2016 12:00:00 Lower/Upper Lmts: O.OOOOOOE+OO through 2. OOOOOOE-02 .01 ............................................................................ . . . . . . x ..,. x x x x x x x. x x x x *x x x x X X X X X X X X *X X X X 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW QA filena!Yle Paraf'leter Na!Yle Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W018.QAF;5 AVRGEFF (Average Efficiency) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00:00 0.307005 through 0.325995 I 325 o ' o o o ' ' o o o ' '*' o O O O O O e o o I O o o' I O o o o 1 1 o o o 1 1' o o O e I O O O o ' o o 'o o 1 O o O o 1 ' o o o I 11 o o o o o o o o o o o o .32 >, 0 c 11) *r-1 0 *r-1 x* 4-4-*x UJ Q) 'QJ) . 315 llj ........... *:* ........... *:* ........... *:* ........... *:* ........... *:* ......... *x Q) a: x x I 31 I I 0 0 0 I I 0 0 0 0 o 00 0 0 I I 0 o o o I I o o 00 I o o o o 1 1 o o o o o0 o o o o I O O O O o I o o, o I I o o o 1 1 o o o 1 1, 0 0 0 O 1 0 0 0 0 I O 0 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Ylent Date/Ti!Yle UP LOW

..J 0 ......, Vi 00 0 \0 QA filenal"'le Paral"'le ter Nal"'le Start/ End Da_tes Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W018.QAF;5 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00: 00 184.000 through 204.000 200 ............. * ............. * ...... *-.... * ............. * ............. * ............ . I (!) )-1-H > H u a: w Cl H ...J u =i z x: x x :x x x 190 0 o o o 0 0 o 0 o 0 o I 00 0 o 0 I o o o 0 I I 0 0 'o I I 0 0 0 0 0 o 0 0 I o' o 0 o 0 I 0 0 0 0 I I 0 o' 0 I I o o o 0 I o o' o I 1° o o o o I o o o o o I o 4-16 5-16 6-16 7-16 8-16 9-16 Measurel"'lent Date/Til"'le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper lMts: 100 DKA100: [ENY_ALPHA.QA.W]W018.QAF;5 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:48:19 through 28-SEP-2016 12:00: 00 5.00000 through 100.000 . . . . . 80 ' ' o o o 0 0 o o o o o o o o 0 o o o o o o o o o ' o 0 o o o o o o o o 0 o o o o o o o o 0 o o o o o o I ' o o o o o o o 0 o o o o o o o o o' 0 o 0 o -M I D (!). z 0 H :J _J 0 Cf) w O::'. . . . . . 60 ............................................................................ . . . . . *x x: x x . . . . . x 40 ' o o o o o o o o o 0 I o o o o o o o o o o I 0 0 o 0 o o o o o o o ' o I I o o o o o 0 o 0 0 o o o o o I o o o I I 0 o o o o o o o 0 0 0 0 o o o o o o . . . . . 20 ............ *' ............ *' ........... '* .......................... '* ........... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W018.QAF;5 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08: 48:19 through 28-SEP-2016 12: 00:00 3143. 00 through 3223.00 . . . . . 3200 . ' ......................................................................... . . . . ro """" ..-I I D )-Cl:'. :x x: x x x I.LI 3180 z . . . . . ............................................................................ . . . . . I.LI :..::: <J: I.LI 0.. 3160 ................................................................................ . 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW

--N 0 0 ......., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B018.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29: 29 through 28-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 . . . 01 ............................................................................ x x 0 3-16 . . . . . . x x x x x x x x*. x x x x x x x x x x x x x: .x x {< :x x x x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... ....... N ....... 0 ....., Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: '315 DKA100: [ENV_ALPHA.QA.W]W020.QAF;6 AVRGEFF (Average Efficiency) 1-APR-2016 08:54:43 through 28-SEP-2016 12: 00:00 0.300920 through 0.319530 . 31 ............ : ............. : ............. : .......... x .. : ........... x .. : ........... X: x. :x . . . . . 305 * * * * * * * * * * * *.* * * * * * * * * * * * *x_* * * * * * * * * * * .. * * * * * * * * * * * * *. * * * * * * * * * * * * *.* * * * * * * * * * *
4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
. QA filename DKA100: [ENV_ALPHA.QA.W]W020.QAF;6 Parameter Name NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 1-APR-2016 08:54:43 through 28-SEP-2016 12: 00: 00 Lower/Upper Lmts: 184.000 through 204.000 UP 200 ............. * ............. * ........... * ............. *.-* ........... " ........... . I D r r H > H r u x: x x w D x H u :x z 190 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ' ........................... . 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurement Date/Time --N w 0 ......., Vl 00 0 \0 QA filenal""le Paral""le ter Nal""le Start/End Dates Lower/Upper Ll""lts: 100 DKA100: [ENV_ALPHA.QA.W]W020.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:54: 43 through 28-SEP-2016 12:00: 00 5.00000 through 100. 000 80 ' 0 o o o ' o o o o ' , o o o ' o o o o ' o o o ', ' ' o o o ' ' o o o ' ,' o o o o o o o o o ' ' o ,* o ' ' o o o I 0 o o o 0 1 o o o o o o o o o o o '<'i I D (.') z 0 H ::J _J 0 en w O:'. a: w 0.. 60 *
X* *

X ............................................... *x* ......................... . : x : : x : .x 40 ...... ' .................................................................... . . . . ' . 20 ................................................................................ . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe _ DKA100: [ENV_ALPHA.QA.W]W020.QAF;6 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 1-APR-2016 08:54:43 through 28-5EP-2016 12:00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . .

O o o o o o o o o o o o o o o I o o o o O O o O o I o o o o o o o o o o O o o o O o o o o o o o o O o o o o I o o o o o o I I O O o o o o o I o o o o co ""'" ..-l I D )-et:: :x x: x x x LLJ 3180 z . . . . . ............................................................................ . . . . . LLJ :::4 a: LLJ 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
...-N VI 0 ......., VI 00 0 \0 QA filename DKA100: [ENV_ALPHA.QA.B]B020.QAF;3 Parameter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:30 through 28-SEP-2016 12: 00:00 Lqwer/Upper Lmts: 0. OOOOOOE+OO through 2.000000E-02 . . . 01 ...................... : .......... : ........... * .......... : .......... : ......... . x xx xx xx xx x x:x xx xx xx x: X X X X *X X X X 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W021.QAF;10 AVRGEFF (Average Efficiency) 1-APR-2016 08: 54:43 through 28-SEP-2016 12:00: 00 0.311665 through 0.330943 .33 ............................................................................ . . . . . . . . . . . . . . . 325 o o o o o o o o o o o I 0 o o I 0 0 0 0 0 I o 0 o o I o o o o o o o o o o o 0 0 0 o I o 0 o o o o o o o I 0 0 0 0 I I o o o o o o o o o o o o o o o o o . . . . . >:. u c Q) *r-1 u *r-1 4-4-UJ :x x Q) "Q.Q .32 iti x . ............ * ............. * ...... ,. .... x.* ............. * ............. * ........... . . . . . So-Q) > <I: x '315 4-16-5-16. 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW ...... ...... N -..J 0 ....., Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W021.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:54:43 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ............. * ............. * ........... * ............. * ............. * ............ . I D >-. I-H > x: H I-u a: x x x w D .x H _J u ::i z 190 o I Io o I O I o o I I 0o o o I I o o o o I I o o 0o o I o o 0 I I I o I I o' o I o I I o o o o I o I o' o I o o o o I I o I o I o' I o o o o o o o o o I o 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW --N 00 0 ....., Ul 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W021.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016 08:54:43 through 28-5EP-2016 12:00:00 5.00000 through 100.000 80 ............ * ............. * ............. * ............. * ............. * ........... . ..-1 I D C) z o. H 1-::i _J D (J) w O:'. . . . . . 60 ............................................................................ . . . . . , x: x .x x x 40 o ' e o o o o o o o o o o e o o o o 0 o o o o 0 o o o o o o o o o o o o o o o o o o o o e o o I 0 o 0 o o o o o o o o o o o o o o o o e o o o o o I o o . . . . . 20 ....................................... '* ....................................... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --N \0 0 ....., VI 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W021.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08:54: 43 through 28-SEP-2016 12:00: 00 3143.00 through 3223.00 . . . . . 3200 . ' .......................................................................... . . . . ro ""'" ..-I I D (!) )-(!) 0:: w 3180 z :x x x: x . x . x ..... ' ..................... ' ................... ' ........................... . . . . . . w ::..::: a: w 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOU.I ..... ..... V.l 0 0 .-+, UI 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B021.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29: 30 through 28-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . . . ' 01 .......... * ........... : .......... : ........... * .......... : .......... : ......... . x x x *.x X X X X X X X X X X . X X X X X X X X X* X X X X X X X 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe 0 ....... Vl 00 0 \0 QA. filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: x DKA100: AVRGEFF (Average Efficiency) 30-AUG-2016 10:09:39 through 28-SEP-2016 12: 00: 00 0.289160 through 0.307050 . . . . .305 ' ' e o 0 0 o o o o o o o o o o o o o o 0 0 o o o o o o o o o o o o o o o 0 o o o o o 0 o o o 0 o o o o o o o o o o o o o o 0 o 0 0 o o o o o o o I o o >.. u i:: Q) *n u *n 4-4-UJ Q) "QI) ((i" Q) > a: x .3 '295 ................. : ................. : ................. : ................. : x .. . x x I 29 ' 1 0 0 0 1 1 0 0 0 0 1 0 0 0 1 1 : 0 0 0 0 1 0 0 0 0 o o 0 0 0 0 0 0 : 1 1 0 0 0 0 0 0 0 0 0 1 o o '. 0 1 : 0 0 0 o 1 0 0 0 1 1 0 0 0 0 1 0 0: 0 1 1 1 8-30 9-06 9-13 9-20 9-27 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W023.QAF;6 PqraMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 30-AUG-2016 10:09:39 through 28-SEP-2016 12:00:00 Lower/Upper LMts: 184.000 through 204.000 UP 200 ' 0 '0 o 0 0 o e o o o o e o o o o o o o o 0 o 0 0 0 0 0 o o o ' o o o o o o o 0 0 I o o o o o o o o o o 0 o o 0 I I 0 o o o o o o o o o o o o o o o o . . . . I 0 r H > H u *x w 0 H. x x u z 190 ................. : ................. : ................. : .................. : ... . 8-30 9-06 9-13 9-20 9-27 LOW MeasureMent Date/TiMe ..... ..... w VJ 0 ......., V'I 00 0 \0 QA filenar.-.e Parar.-.eter NaMe Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W}W023.QAF;6 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 30-AUG-2016 10:09:39 through 28-SEP-2016 12:00:00 5.00000 through 100.000 . . . . . 80 ' 0 o o o ' ' o o o ' 0 0 o o I 0 o o o 0 0 0 o o o o 0 0 o 0 0 0 0 0 0 I I 0 o o 0 I o o 0 0 I I 0 0 o I 0 ' o 0 0 I 0 o 0 0 0 o o 0 0 0 o 0 o o I I 0 ..-I I Cl (!:I z 0 H 1-:J _J 0 en w O:'. ::.! a: w 0.. 60 40 . . . . 0 I o o 0 I I o 0 0 0 0 0 0 o I I 0 o 0 0 o o 0 o o I 0 o o 0 I 0 o o o o 0 o o o o I o o o o I I o o o I 0 o o o I I 0 0 0 o 0 0 0 0 0 I o 0 0 0 I I 0 x x . . . . x : ,(< . . . . I I o o o I I o o 0 I I o 0 o I I 0 o 0 0 0 0 0 0 0 0 0 0 o 0 I I 0 o 0 I I 0 0 o 0 I 0 0 0 0 I I 0 o 0 I I o 0 o o I o o o I o o o o o o o o o o I I o . . . . 20 ................. ' ................. ' ................. ' ................. ' ... . 8-30 9-06 9-13 9-20 9-27 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W023.QAF;6 ParaMeter *NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Date8 30-AUG-2016 10:09:39 through 28-SEP-2016 12: 00: 00 Lower/Upper LMt8: 3143.00 through 3223.00 UP 3220 3200 . . . . o ' ' o o ' ' o o o ' I o o o 0 o ' o o o o o o o o o o o o o ' o o ' o I o o o o o o o o o o o o ' o o o o o o o o o o o o o 0 o o o o 0 '
o o ' o o . . . v "<""I I D (!) )-(!) 0:: x : )X( LJ..I 3180 z . . . . ............................................................................ . . . . LJ..I :::..::: a: IJJ 0.. 3160 8-30 9-06 9-13. 9-20 9-27 LOW Mea8ureMent Date/TiMe
--V-l Ul 0 ....., Ul 00 0 "° QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B023.QAF;4 BACKRATE (Background Rate) 31-AUG-2016 12:42:18 through 28-SEP-2016 12:00:00 O.OOOOOOE+OO through 2.000000E-02 . . . ' . . . . . ' 01 ....... : ....... : ....... : ....... : ....... : ....... : ....... : ....... : ....... : ... . *X X* x x x *x x x x: x 0 ;8-31 9-03 9-06. 9-09 9-12 9-15 9-18 9-21 9-24 9-27 MeasureMent Date/Tiriie UP LOW --\.;.) O'I 0 ......., Vt 00 0 \0 QA filenafY'le Pararrieter NafY'le Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W024.QAF;4 AVRGEFF (Average Efficiency) 1-APR-2016 08: 54: 43 through 28-SEP-2016 12: 00:00 0.332785 through 0.353369 I 35 * * * * * * * * * * * * *" * *
0 0 0 0 *

0 0

00 0 0 0 0 0 0 0 0 0

0 00 0 0 0 0 0 0 0 0 0 0 0 0 *, 0 0 0 0 0 0 0 0

0 0 0 00 0 0 0 0 0 0 0 0 0 0 0 0 (..) c Q) *r-1 (..) *r-1 4-4-LlJ x x x :x x* x . . . . . . 34 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TifY'le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W024.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 1-APR-2016 08:54:43 through 28-SEP-2016 12:00:00 184.000 through 204.000 200 ............. * ............. * ........... * ............. * ............. * ............ . I 0 )-I-H > H-I-u a: )( w *X x 0 H --' u x. x x =i z 190 ' ' * *

I I o 0 0 0 I 'o I o I 0 0 0 0 o 0 I 0 0 'o o I o o 0 I o o 0 o o o0 o

o o o o o o o o o o o0 o o o o o o I O O O O I 11 O o O O o o o o o o o, o 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... ...... w 00 0 ....., Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W024.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 1-APR-2016-08:54:43 through 28-SEP-2016 12:00:00 5.00000 through 100.000 . . . . . 80 0 0 o o o o o o o o o o o o o
I o o o o o I o o o 0 o

o o o o o o o o o o I o o

o o o o o o o o o o o o o o I I o o o o o o o o o I o o o o o o o ..-! I D C) z 0 H 1-::J __J" 0 01 w O:'. a: w 0... X* x x x x *X . . . . . 60 ............................................................................ . . . . . . . . . . 40 ............................................................................ . . . . . 20 ................................................................................ . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Oate/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W024.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 1-APR-2016 08:54:43 through 28-SEP-2016 12:00:00 3143. 00 through 3223. 00 . . . . . 3200 ............................................................................ ro "<T .,.; I D (!) )-(!) Q'. :x X* x x x x LlJ 3180 z ............................................................................. . . . . . LlJ ::...:: <C LlJ 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B024.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:29:30 through 28-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . . . 01 ............................................................................ . . . . . . x X X X X X X X X X X* x X X X -X X X X x x x x x x x x x *x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
--.j:>. -0 ....., VI 00 0 \0 QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W026.QAF;7 AVRGEFF (Average Efficiency) 3-MAR-2016 08:11:44 through 29-5EP-2016 12:00: 00 0.312549 through 0.331881 . 33 ...................... * ........... * ........... * ........... * ........... * .......... . :::-, 0 c I]) -ri 0 -ri 4-4-UJ . 325 x x: x o o o o O O O o o o
o o o o I O o o o o oo o o o o o o o o o O"' o O O O O o o o o ooo o o o I o O O o I o oo o o o o o o o I I o oo o o o o o o o o I o :x x x *x I]) '0.0 a::i s... I])

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I 0 o o o o o o o o o o o o o o o o 0 . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
--.i::. N 0 ....., Vl 00 0 '° QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENY_ALPHA.QA.W]W026.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:44 through 29-SEP-2016 12: 00:00 184.000 through 204. 000 200 .......... * ............ * ..................... *.* ........... * ........... * ......... . I 0 (!) )-f-H > H f-u a: w 0 x H x __J u ::i ZL 190 x : :x : x : : .......... .-.......... * ........... * ........... * ........... * ......... *X** ......... . *x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW --"""' w 0 ......., Vl 00 0 "° QA filenar.-.e Pararrieter Nar.-.e Start/End Dates Lower/Upper -Lr.-.ts: 100 OKA100: [ENV_ALPHA.QA.W]W026.QAF;7 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11:44 through 29-SEP-201£ 12:00:00 5,00000 through 100.000 80 ...................... * ........... * ............ * ........... * ........... * .......... . ..--! I 0.. z 0 H 1-:J ....I 0 01 w O:'. :::..: <I: w 0.. . . . . . . 60 I 0 o o o o o o o o o o o 0 o I I 0 0 o o o I o o o o I o o o o I o o 0 0 0 0 0 o I o o o o I I o o o I I e o o 0 0 o o o I I o o o o o o o 0 o I o o . . . . . . :x x .x x x >< x: 40 I I e o o o o o o O I I e 0 o I o o o o o I o o o o I I o,
e. 0 I o 0 o I I o o o o o o o o O I 0 0 0 0 o I o o o I I e o O I O 0 o o o I o o o O I I O . . . . . . 20 .......... ' ...................... , ................................... " ......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe Pararieter NaMe 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W026.QAF;7 P5ENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 08:11:44 through 29-5EP-2016 12:00: 00 3143.00 through 3223. 00 . . . . . . 3200 o ' o o ' o ' 0 o o I I o o o o o o o o o o 0 0 0 0 I o o o o o o o o o 0 0 o o o o o o o 0 o I o o o o I o o o o I 0 0 o o I o o o o o I o o 0 o 0 o o . . . . . CD ""'" """"" I

D (!:I )-(!) Ct:: x :x :x x: x. x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ :::.£ a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOU.I QA filename DKA100: [ENV_ALPHA.QA.B]B026.QAF;2 Parameter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:49:26 through 29-SEP-2016 12:00:00 Lower/Upper Lmts: O.OOOOOOE+OO through*2,000000E-02 ID .µ ITj O:'. "O c :::::; . 01 .......... * ........... : .......... : ......... *.* ........... * .......... : ......... . 0 "OJ) .::.::: u ITj m x x x x 0 3-16 x x x x 4-16 x x x 5-16 *X x x x 6-16 x x 7-16 x x x x x* 8-16 Measurement Date/Time :x x x x x x x 9-16 UP LOW
--0\ 0 ....., Vl 00 0 \0 QA filenafYle DKA100: [ENV_ALPHA.QA.W]W028.QAF;8 ParafYJeter NafYle AVRGEFF (Average Efficiency) Start/End Dates 3-MAR-2016 08:11:44 through 29-SEP-2016 12:00: 00 Lower/Upper LMts: 0.279800 through 0.297100 UP . . . . '295 o o o o o o o O O O I I o o o o o o o o o o o o o O I I o o o o o o o o o o O O o o o o o o o O o O O o I O o o o o o o o o I I O O o o o o o o o o o o . . . . . . X* >, 0 c J1) '2.9 *r-1 0 *r-1 4-4-LU Q) "OJ) Ill x x J1) > a: .x :x '285 .......... .-.......... * ........... * ........... * ........... * ........... * .......... . x '28 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ......................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasurefYlent Date/TifYle QA filenarrre Pararrreter Narrre 5tart/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W028.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:44 through 29-5EP-2016 12: 00: 00 184.000 through 204.000 200 I 0 I I I I I I o o o 0 I I I 0 I I o 0 I o I o I I o o I I I I I I I I I o I o o I I I I I o I I I o' I I ' I I I I I I I o o o I I I I o I I I 0 I 0 o . . . . . . I Cl C!J )-f-H > H f-u a:. w Cl H *x x ...J u x* ::i z x *x 190 . . . . -. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW --.+::.. 00 0 ......, Vt 00 0 \0 QA. filenafYte ParafY'leter NafYte Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W028.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11: 44 through 29-SEP-2016 12:00:00 5.00000 through 100.000 80 .......... : .......... * ........... * ........... * ........... * ........... * .......... . <C w 0... . . . . . . 60 ..................................................... ' ..................... . . . . . . . x :x x x: .x x *X x . . . 40 o I o 0 0 I I o o o o I o o o I I o o o ' 0 I o o o 0 o o o o I I o o o 0 0 o o o o o o o o o I I o 0 o I o o o o I I o o o o I o 0 o o o o o o o I ' o . . . . . . . 20 .......... ' ...................... , ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --.j:::.. \0 0 ......, Ul 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.W]W028.QAF;8 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 3-MAR-2016 08:11:44 through 29-SEP-2016 12: 00: 00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . ............................................................................ . . . ro "'" ...; I 0 (!) )-(!) et:: :x x .x x x: x l.J.J 3180 z . . . . . ............................................................................ . . . . . . l.J.J ::..::: a: l.J.J CL 3160 .......... -...................... -............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe --Vi 0 0 ......, Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B028.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:49:26 through 29-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 . . . . 01 .......... * ............ * .......... : ......... *.* ........... * ........... * ......... . x x x x 0 3-16 x 4-16 x x x x x x 5-16 x :x x x x x x ?< x x x x x. x x x x x 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --Ul -0 >-+, Ul 00 0 "° QA filenal'le DKA100: [ENV_ALPHA.QA,W]W029.QAF;11 Paral'leter Nal'le AVRGEFF (Average Efficiency) 5tart/End Dates 3-MAR-2016 14:39:28 through 29-5EP-2016 12: 00: 00 Lower/Upper Ll'lts: 0.292500 through 0.323350 UP . 32 ;:., (J c I]) *r-1 (J .31 *r-1 4-*x x x 4-Ll.J *x x X* I]) *X 'OfJ ill I-: I]) > a: x .3 . . . . . . o o o 0 o o o o o o o o o o o o o o o o o o ' o o o o o o o o 0 I ' o o o o o o o o o o o o 0 o 0 o o o I I o o o o I o o o o 0 o o o o o o o o o o I o . . . . . . 3-16* 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurel'lent Date/Til'le QA filena(Y']e Para(Y']eter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W029.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 14:39:28 through 29-SEP-2016 12:00:00 184.0UO through 204.000 200 ........... ' ......................... ' .............. ' ...................... . . . . . . . I Cl (!) )-I-H > H f-u a: w Cl *X H ....I u *X =i z x 190 x * * * * * * * * * *: x* * * * * * * * * :* * * * * * * * * * * :* * * * * * * * * * * * * * * * * *
x * :* * * * .... *

1<.:* .... , ..... 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
--Ul w 0 ......, Ul 00 0 "° QA filename Parameter Name 5tart/ End Dates Lower/Upper Lmts: 100 DKA100: [ENV_ALPHA.QA.W]W029.QAF;11 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 14:39:28 through 29-5EP-2016 12:00:00 5.00000 through 100. 000 x* 80 .......... ::?< ......... * ........... * .......... ......... ........... * .......... :X: .,-! I Cl z H 1-::::i _J D U') w
n= :::..! a: w 0... *X 60 .......... *: ......... *:-.......... :*x* ........ *:* ......... *:* ......... *:-......... . . . 40 ' ' ' ' o ' ' ' ' ' ' ' o o * ' I o o ' o 0 o o o o I o o o o I I o o o I o o o o o I o o 0

o 0 o o I I o o o o o o o o o 0 0 o o o o o o o o o o I o . . . . . . 20 .......... ' ...................... , ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Time UP LOW
..... ..... Vl 0 ....., Vl 00 0 l.O QA filenaMe Pararrie ter Naf'l"le Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W029.QAF;11 PSENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 14:39:28 through 29-SEP-2016 12:00:0d 3143.00 through 3223.00 . . . . . . 3200 0 I 0 0 0 0 I 0 0 o 0 I o 0 0 I I o 0 o o 0 0 o o o o o o o o o o o o o o o 0 o o o 0 o o 0 o I o 0 0 0 o I o 0 0 0 0 0 0 0 0 0 0 o 0 0 0 o o o o I o o co v ..-I I D (!) (!) 0:: x :x x* x :x :x x x LJ..I 3180 z . . . . . ' ............... ' ................ ' ........................................ , .. . . . . . . LJ..I ;:,..:; 0: LJ..I CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TiMe UP LOW ,_. ,_. Vo Vo 0 ......., Vo 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B029.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:49:26 through 29-SEP-2016 12: 00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 2. OOOOOOE-02 . . . . 01 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . x . . . . . x x x 4-16 x x x x *x x x 5-16 6-16 x x x x x 7-16 Date/TiMe x x x: x x x ;x 8-16 9-16 x x x UP LOW --Vt 0\ 0 ......., Vt 00 0 ID QA filenarrie Pararrie ter Narrie 5tart/End Date8 Lower/Upper LrritB: ::>, (j c I}) *r-1 (j *r-1 4-4-UJ . 285 .28 DKA100: [ENV_ALPHA.QA.W]W032.QAF;7 AVRGEFF (Average Efficiency) 3-MAR-2016 08:11:46 through 29-5EP-2016 12: 00:00 0.268707 through 0.285329 *X :x :x x: x* x . 275 .......... : .......... : ........... : .......... : ......... <<. : ........... : .......... . x . 27 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:46 through 29-SEP-2016 12:00:00 184.000 through 204.000 200 .......... * ............ * .......... .' ......... *.* ........... * ........... * ......... . I CJ (!) )-I-H > H I-u a: w x x o* *x ....I u *X x ::i z x: 190 I o o
I I I I I I : I I I I I I I I I I 01 I 0 0 0 I I I

I 0 11 I I 0 0 0 I I I I 0 1 I I I I I I I I I 0 I 11 0 I I 0 I I I 0 0 I 11 I I I I I I 0 I o 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
....... ....... Vl 00 0 ....... Vl 00 0 \0 QA filenalY'Je Pararleter Narle Start/End Dates Lower/Upper LIY'lts: 100 DKA100: [ENV_ALPHA.QA.W]W032.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-201608:11:46 through 29-SEP-2016 12: 00:00 5.00000 through 100. 000 80 ' ' ,*, o o 0 0 o 0 o' 0 o o o o o o o o o 'o o o o o o 0 o 0 o o *, 0 o o o o e o o o o'o o 0 o 0 0 o o o o o e o o o o o o 0 I 0 ', o o o o o o o o 0 o T"I I D (!) 2 0 H ::J ...J 0 en w O:'. ::..:: c:r:* w 0... . . . . . . 60 ............................................................................ . . . . . . x *x *x x x x X* . . . 40 ................................ ' .......................................... . . . . . . . 20 .......... ' .......... *' .......... , ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --lJl '° 0 ......, lJl 00 0 '° QA filenaMe Pararleter NaMe 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W032.QAF;7 P5ENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 08:11:46 through 29-5EP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ . . . . roA ""'" "<""i I 0 (!) )-(!) Ct'. x :x :x x X* x LU 3180 z . . . . . o o 0 0 o I o 0 o o o o o 0 o 0 o 0 o o o o o o o o o o o o o o o o o o o o o o o o 0 o o 0 o I I o 0 o I I 0 0 o 0 0 o o 0 o 0 o o o o o o o o o I I o . . . . . . LU :,.::: a: LU CL 3160 **********-**********************-********************************************** 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --0\ 0 0 ....., Vl 00 0 \0 QA filenafY'le ParafY'Jeter NafY'le Start/End Dates Lower/Upper DKA100: [ENV_ALPHA. QA. B]B032. QAF; 3 BACKRATE (Background Rate) 4-MAR-2016 12:49:34 through 29-SEP-2016 12: 00:00 O.OOOOOOE+OO through 2.000000E-02 .01 ............................................................................ . . . . . . x x .X X X x; x .x x x x x x x x x x x x* x x x x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW --0\ -0 ....., Vl 00 0 \0 QA filename Parameter Name Start/End Dates Lower/Upper Lmts: DKA100: [ENV_ALPHA.QA.W]W033.QAF;7 AVRGEFF (Average Efficiency) 3-MAR-2016 08:11:46 through 29-SEP-2016 12: 00: 00 0.314090 through 0.333520 I 33 ' ' ' o * ' ' ' ' ' ',' ' ' ' o ' 0 ' o ',' ' o o o 1 1 o 0 o o .. o o ' ' ' ' ' 0 ' ',' ' ' ' 1 ' ' ' ' ' 1 ,* * ' ' ' ' o o *
o 0o o o o o o o o 0 1 0 x *X .x :::-, u :x x X* c Q) *r-1 x u . 325 *r-1 . . . . . . ................................................... -........................ . . . . 4-4-UJ x Q) "OJ) iU s.... Q) > . 32 I 315 1 0 0 0 0 0 1 0 0 0 00 0 0 0 0 ' 1 0 0 0 0 ,* ' 0 0

o 1 o 0 0 1 .' 0 0 0 1 0 0 0 0 0 000 0 0 0 1 1 0 0 0 0 1 00 0 0 0 1 0 0 0 ' o 0 ,* 0 0 0 0 0 0 0 0 0 0 3-16 4-16 5-16 . 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW
,_. ,_. 0\ N 0 ......, Vi 00 0 \0 QA filenarrie Pararrreter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W033.QAF;7 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:46 through 29-SEP-2016 12:00: 00 184.000 through 204.000 200 ..... ' ' ... *.' ... ' ' ..... * ' ... ' ' ... '.' .... ' .... *.* ... ' ' ... ' '.* ........... * ......... . I D (!) )-f-H > H x f-u a: X* w D H x ....I u *x ::i z 190 . . . . . . x ...................... *.X ......... * ........... * ........... * ........... * .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW --0\ VJ 0 ......, Vl 00 0 \,() QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W033.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11: 46 through 29-5EP-2016 12:00: 00 5.00000 through 100.000 80 ' o o o o ' o 0 o o o' o o 0 o o o o o o o 0o o o o o o o o 0 o o ', 0 o o I o o o o o o0o o o o o o o o 0 0 o 0o o 0 I I o
o o 0 o 'o o o o o o o o ; o o "<"i I D C) z 0 H 1-::i. ...J 0 01 w O:'. . . . . . . 60 0 I o o o o o o o o o I o o o o I o 0 0 0 I 0 o o o o o o o o o o o o o I 0 0 0 o o I o 0 o o o o o o o o o o o o 0 o o o o I I O o o O O o o o O I I o . . . . . . x *X :x x X* x >< x 40 o o o o o o I 0 o o o o o e o o o o o o o o o o o o 0 I o o o o o o o o o o e o o o o o o o o o ' o 0 0 I o e o o o o o o o o o o o o o o o o o o o o o . . . . . . 20 .......... ' ...................... ' ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,W]W033.QAF;7 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 3-MAR-201608:11:46 through 29-5EP-2016 12: 00:00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . . ............... ' .......................... ' ...... ,; ......................... . . . . . co """ I D (!) )-(!) 0::: :x :x x: :x x x x LL.I. 3180 z . . . . . . ......................................................................... ' .. . . . . . . LL.I :>.::: ([ LL.I Cl.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B033.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12: 49:34 through 29-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2. OOOOOOE-02 UP . . . . '01 .......... " ........... * .......... : ......... *.* ........... * ........... * ......... . :x x x x x *x x x x x x x x x x x ?< x x x x x x: x x x x x x x 0 LOW 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe
....... ....... 0\ 0\ 0 ......., Vl 00 0 \0 QA f i lena.rt'le
Parart'leter Nart'le Start/End Dates Lower/Upper Lmts: .6 DKA100: [ENV_ALPHA.QA.W]W034.QAF;7 AVRGEFF (Average Efficiency) 3-MAR-2016 08:11:46 through 29-SEP-2016 12: 00:00 -0.216325 through 0. 647405 . . . . . . .4 0 o o o o ' ' o 0

o o o o o o o o o o o o o o o o o o o 0 o 0 o o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o I I o o o o o o o o o 0 o o :>> 0 c x *x *X *X x X* x Q). *r't 0 *r't 4-4-LU .2 . . . . ............................................................................ . . . . . . Q) "0.0 l1j f.-Q) > a: 0 -.2 ...................... * ........... * ........... * ........... * ........... * .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W034.QAf;7 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 3-MAR-2016 08:11:46 through 29-SEP-2016 12:00:00 Lower/Upper LMts: 184.000 through 204.000 UP 200 o o o o o o o o o o o o o o o o o o o o o 0 I o o 0 I o o 0 0 o o o 0 o I 0 0 0 o 0 o o o o o I o o o o 0 o o o I I 0 0 o I I o o o o o o o o o I o o . . . . . . I Cl )-I-H > .' H I-u <I: w *x D H .....I x .x u ::i z* x .x 190 * * * * * * * * * * .. * * * * * * * * * *** * * * * * * * * * * *. * * * * * * * * *x* * * * * * * * *x*** * * * * * * * * * .*. * * * * * * * * *

X* 3-16 4-16 5-16 *6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
...... ...... 0\ 00 0 ......, Vi 00 0 l.O QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA,W]W034.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11:46 through 29-SEP-2016 12:00: 00 5.00000 through 100.000 .,.-! I Cl (!) z 0 H =:i --' 0 en LLJ O:'. 0: LLJ 0.. 100 80 . . . . . . ............................................................................ . . . . . . 60 ............................................................................ . . . . . . :x *x x. 40 x . . -x . . . x .......... : .......... * ........... * .......... ):: ......... * ........... * .......... . . . . . . . 20 .......... ' .......... *' .......... , ............................................. . 3-16" 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 08:11:46 through 29-SEP-2016 12: 00:00 3143. 00 through 3223.00 . . . . . . 3200 ' ' o o o ' 0 o o o o o 0 o o 0 o 0 o o 0 I I 0 o o I I o o o 0 o o o o I ' o o o o o o o o o o o o o o o I o o o 0 0 0 o o 0 I o o o o I o o o o I o o . . co "<;f" ..-i 1
D )-Ct:: x *X :x x x x x. x LIJ 3180 z . . . . . . ............................................... ' ........................... . . . . . . . LIJ ::..::: a: LIJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
....... --..} 0 0 ......, Vl 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B034.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12: 49:34 through 29-SEP-2016 12: 00:00 Lower/Upper O.OOOOOOE+OO through 2.000000E-02 UP . . . . . . . 01 ************************************************************************* t ** . . . . . . *X x x x x x x x *X X X X x x x x x: x x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ---.i -QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W038.QAF;6 AVRGEFF (Average Efficiency} 3-MAR-2016 08:11: 48 through 29-SEP-2016 12: 00: 00 0.350000 through O. 371670 . 37 ...................... * ........... * ........... * ........... * ........... * .......... . 0 c I]) *r-1 0 *r-1 4-4-UJ x x x . 36 .......... * ............ * ..................... *.* ........... * ........... * ......... . *X x* x *x 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: [ENV_ALPHA.QA.W]W038.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12: 00:00 184.000 through 204. 000 200 .......... * ............ * .......... .' ......... *.* ........... * ........... * ......... . I Cl )-..... H > H ..... u 0:: w :x Cl H ...J u x x: X* x ::i. x z 190 .......... '.x* ....... *:* .......... :x* ........ *:* ......... *:* ......... *:* ......... . . . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ---.J VJ 0 ......, Vi 00 0 \0 QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper *LIY'lts: 100 DKA100: [ENV_ALPHA.QA.W]W038.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12: 00: 00 6.00000 through 100.000 80 ...................... * ........... * ........... * ........... * ........... * .......... . ..-! I er z o H ::i ...J o (() w O:'. :...::: a: w 0... . . . . . . 60 o I o o 0 I I o o o 00 I o o o o o o o o o 1 o I 0 o 0 0 I o o o o : o o o o o o o o o I 0 o o o 0 I I O o o I O 0 o o o I I o o o I I o 1 o o o o o o o o o o x >< x X* *X *X x x . . . 40 ..... ' ..................................................................... . . . . . . ' 20 .......... ' ...................... , ......... '*' .......... *' .......... *' ......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Y'lent Date/TilY'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W038.QAF;6 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 3-MAR-201608:11: 48 through 29-SEP-2016 12:00:00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 o o 0 0 o I I ' I o o o o o I o I I o o 0 0 I I I o 0 I I 0 I o I o 0 o o I o o o o I I o o I I o 0 0 0 0 I o o o o I o o o o I I o o o o I o o o o 1 o o o O I O O . . . . . ro "'" ..-i I
D )-Cl:'. :x :x :x x: x x x x LL.I 3180 z . . . . . . o I o ' o I o o o o o 0 0 0 o 0 o o 0 o o o I o 0 o o o I o o o o o I o o I o o o o I o o o o I I o o ' o o o ' ' o o ' ' o o 0 0 o ' ' o o ' o ' o . . . . . . LL.I :..::: >( x x x x x x:x x x x x x x x x x x x X* x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W040.QAF;6 ParaMeter NaMe AVRGEFF (Average Efficiency) Start/End Dates 3-MAR-2016 08:11:48 through 29-SEP-2016 12:00:00 Lower/Upper LMts: 0.319060 through 0.338800 UP . 336 . . . . . . . o o o o 0 I I o o o I I o o o I o o o o o o I o o o I I o o o o I o o o I I o o o o I o o

0 O O o o o o o o o o o o o o o 0 I o O o o O o o o o o o o >, 0 c Q) *r-1 0 '33 *r-1 x ......... * ......... -.. * ..................... *.* ........... * ........... * ......... . 4-4-LLJ *X Q) "OJ) iU I-Q) :x > x x a: '326 .......... *: .......... :* .......... :* .......... : ........... :* ......... x: :* ......... . I 32 1 1 o o o f I O o O 10' o o o o I o 1 o o o' 1 o o o 1 o 1 o o 1 .. o o o O I O o o o 'o' o o o 1 o o o O I Io' o o 1 o o o o 1 o o o' o o 1 o o o o 1 1 o 3-16 4-16 6-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W040.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12:00:00 184.000 through 204. 000 200 .......... * ............ * .......... .' ......... *.* ........... * ........... * ......... . I D )-I-H > H I-u <J:* x x *x w *x x D H ...J u X* x z 190 ' o

o o ' ' o o o ,"' o o o I I o o o o *, I o 0 0 0 I o o 0 I 'o 0 o o o o o o o o ,*, o o o I I o o o I o 'o o o I I o o o I I o 'o o o I o o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... ...... -.l 00 0 ......, Vl 00 0 \0 Qf'.l filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W040.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12:00:00 5.00000 through *100.000 80 ' o o ' ' I 0 0 o o ," o o o o o I o e o 0 'o I o o o o o o o o o 'o o 0 o I o o o o o o'o 0 e o o o o o o 0 o 'o o 0 0 o o o o o I o 'o 0 0 I o 0 o o o o o .n I Cl z 0 H ::i ....I 0 ({) w* -O:'. . . . . . . 60 ................ ' .......................................................... . . . . . . . x .x :x x x X* x X* . . . . . . 40 o o o o o o o o o o o o o o e I I 0 e o o o o o o o o o o o o I 0 0 o 0 I o o o o o I 0 0 0 0 I I o o o o I o o 0 0 0 o 0 0 o o o o o e o e o 0 o I 0 0 . . . . . . 20 .......... ' ...................... , ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ,_. ,_. -..J \0 0 ....., Vl 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W040.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12: 00:00 3143. 00 through 3223.00 3220 .......... , ...................... ' ............................................. . 3200 . . . . . . I I o o o 1 1 o o o o I o o o 1 o o o o o O I o o o o I o o o I o o O
O o o o o o I o o o 0 I o I o o o o o o o o 0 0 o 0 o o o o I o o o o o o I I 0 . . . . co ""'" .... I 0 )-0::: x :x :x x x: x l.J.J 3180 z . . . . . o o o o o I o 0 o o I I o o o I o o o o

0 I o o o o I o 0 o I I

o o o I o o o o 0 o o o o I I o o o I o o o o o o o o 0 I I o o o o I o o o o o I o . . . . . . l.J.J lo.:: a: l.J.J a. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B040.QAF;2 ParaMeter Name BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 12: 49:42 through 29-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . . . 01 ............................................................................ . . . . . . :x x x x x x x x x x x x x x x x x x: x x x :x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
...... ...... 00 ...... QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W041.QAF;8 AVRGEFF (Average Efficiency) 3-MAR-2016 through 12:00:00 0. 332337 through 0.352787 . . . . . . '35 ............................................................................ :>.. 0 c ID *r-1 0 *r-1 4-4-LU *X *X x. x '34 . . . . x . . ... '* ................................... ,, ................................... . . . . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W041.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12: 00:00 184.000 through 204.000 200 .......... * ............ * .......... .' ......... *.* ........... * ........... * ......... . I CJ )-I-H > *x H x I-u <I: x x w x CJ H _J u x :x X* =i z 190 ...................... * ........... * ........... * ........... * ........... * .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ....... ....... 00 w 0 H) VI 00 0 \0 QA filenarrre Pararrre ter Narrre Start/End Dates Lower/Upper Lrrrts: 100 DKA100: [ENV_ALPHA.QA.W]W041.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11:48 through 29-SEP-2016 12: 00:00 5. 00000 through 100. 000 80 ...................... * ........... * ........... * ........... * ........... * .......... . ..-I I D z. 0 H ::i _J 0 tr) w O:'. 60 . . . . . . ' I o o o o o o o o o 0 o o o o o o o 0 o I o o I I 0 o o o o I 0 o o o o 0 o o o 0 I o o o o o o o o o I I 0 o o 0 0 o 0 o o I 0 o o o o o 0 o o ' o o . . . . . . x x x* *x *X x .x x . . :..:: a: w 0.. 40 .......................................................................... ' . . . . . . . 20 .......... ' ...................... , ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW --00 .;:.. 0 >-+, VI 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W041.QAF;8 PSENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 08:11: 48 through 29-SEP-2016 12: 00:00 3143.00 through 3223.00 322n * *. * * * * * * * *, * * * * * * * * * * ** * * * * * * * * * * -* * * * * * * * * *** * * * * * * * * * * ** * * * * * * * * * * ** * * * * * * * * *
3200 . . . . . . o ' o o o ' ' o o o ' o o o o ' ' o o o o ' ' o o o ' ' o o o ' o o o 0 I 0 o o o o I o o o o o o o o o o I o o o o o 0 o 0 o I o 0 o o I o o o o o o o . . . . . . co tj" ...... I D )-0:: x *X x x x. x *X x w 3180 z . . . . . . . ............................................................................ . . . . . . w ::..::: a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... ...... 00 Vl 0 >-+, Vl 00 0 l.O QA filenaMe OKA100: [ENV_ALPHA.QA.B]B041.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:49:42 through 29-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 2. OOOOOOE-02 .01 ............................................................................ x x x x x . . . . . . x x x x x x x x x *x x x x x x x.xxxx x x x x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --00 °' 0 ,...., Vl 00 0 '° QA filenarrie Pararrie ter Narrie 5tart/End Dates Lower/Upper Lrrits: >., 0 c Q) *r-1 DKA100: [ENV_ALPHA.QA.W]W042.QAF;8 AVRGEFF (Average Efficiency) 3-MAR-2016 08:11:48 through 29-5EP-2016 12:00:00 0.328730 through 0.349060 . 34 .......... * ............ * ..................... *.* ........... * ........... * ......... . 4-4-UJ *x *X *X x x x: x x I 33 ' ' 0 0
0 0

0 0 'w' 0 0 0 ' 0 0 0 0 0 *' ' 0 0 0 ' 0 0 0 0 'J' 0 0 0 0 0 0 0 ' ' '* 0 0 0 ' '

0 0 ' 0 *' 0 0 '

0 0 0 ' ' 0 ,* 0 o ' 0 0 0 0 ' ' 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
...... ...... 00 -.) 0 >-+, VI 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W042.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 3-MAR-2016 08:11: 48 through 29-SEP-2016 12: 00: 00 184.000 through 204. 000 200 .......... * ............ * .......... .' ......... *.* ........... * ..................... . I D (!) )-I-H > H x* I-u a: w o. H x :x x :x x --' u ::i z 190 . . . . . . . . . . : . . . . . . . ... *. . . . . . . . . . . *. . . . . . . . . . . . . . . . . . . . . . . *. . . . . . . . . . . *. . . . . . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ........ ........ 00 00 0 >-+, Vi 00 0 \0 QA filenarrie Pararrieter Narrie St'.art/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W042.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 3-MAR-2016 08:11: 48 through 29-SEP-2016 12: 00:00 5.00000 through 100. 000 . . . . . . 80 . * .......................................................................... . I D C) z 0 H 1-:J ....I 0 (f) w O:'. 60 . . . . . . ............................................................................ . . . . . . x .x :x :x x x :x; x. :i..:. a: w 0.. 40 ............................................................................ . . . . . . 20 .......... ' ...................... ' ............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW --00 ID 0 ,...., Vi 00 0 ID QA filenaMe DKA100: [ENV_ALPHA.QA.W]W042.QAF;8 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 3-MAR-2016 08:11: 48 through 29-SEP-2016 12: 00: 00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . ............................................................................ co v '<""I I D (!) )-(!) a:: :x :x x: x x x LI.I 3180 z . . . . . . ............................................................................ . . . . . . LI.I a: LI.I CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent ..... ..... \0 0 0 ......, Vl 00 0 \0 QA filenarrie DKA100: Pararrieter Narrie BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:49:42 through 29-SEP-2016 12:00:00 Lower/Upper lrrits: O.OOOOOOE+OO through 2.000000E-02 Q) .io l1j Ct'. lJ c :::i 0 'OJ) . 01 ............................................................................ .::t. (.) llj co x x x . . . . . . x x x .x x x x x x x x x x x x x x x. x x x x x x x 0 3 -16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W065.QAF;8 AVRGEFF (Average Efficiency) 4-MAR-2016 13: 27:07 through 1-0CT-2016 12:00: 00 0.267564 through 0.295728 I 29 ' I I I I I I I I 1 I I I I I 0 I I I I I ,o I I I I ' I I I I 111 I I 0 I I I I I I .. I I 0 I I I I I I I .. O O o 1 1 o o o 1 I 'I. o o o I Io I I I I I >, u c Q) *r-1 u *r-1 4-4-UJ Q) "OJ) l1j Q) > a: :x *x . 28 :X" ........ : ..................... *.* ......... " .......... * ........... *, .......... . *x x x . . . . . 27 o I I I o I I I o o I I ' I o I I I o o I I o I I I I o o I I I I o o o I o o o o ' 0 I I 0 o ' I I I o o o I I I I o I I o o I o I o I I I Io o I I o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW --\0 N 0 ....., Vl 00 0 \0 QA filenafYle ParafYleter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W065.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 184.000 through 204.000 200 ' ' o ' ' I 0 o o o 0 o o o o 0 o 0 o o o o o o 0 o o ' o ' ' 0 0 o o o I 0 ' ' o o 0 o ' o o 0 0 o o e I o o o o 0 0 o o o o o o o o e o o 0 e o I o o . . . . . . I D )-f-H > H f-u a: x w D H ....I u *x =i z 190 .......... : .......... * ........... * .......... .................................. . *x x x *x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOld QA filenaMe DKA100: [ENV_ALPHA.QA.W]W065.QAF;8 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 4-MAR-2016 13:27: 07 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 5.00000 through 100. 000 ,,...j I D z 0 H :J* _J 0 01 w tY :,,,::: a: w 0... 100 80 . . . . . . ............................................................................ . . . . . . 60 ............................................................................ x . x . :x x x: :x :x x 40 ............................................................................ . . . . . . 20 .......... ' .......... *' ..................... ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... ...... \0 +:-0 H) Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W065.QAF;8 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13: 27:07 through 1-0CT-2016 12:00: 00 3143. 00 through 3223.00 . . . . . . 3200 ' o o o o ' ' o o o o I o 0 0 0 0 o o 0 o o o o o o o o o o o o o o o o o o 0 o o 0 I o o o o o o o o o o o o o 0 o 0 0 o o o o o o o o o o o o o o o o ro """ ...... I D (!) )-(!) O:'. x x :x *X x :x LLJL 3180 z . . . ...................... ' .................................................... . . . . . . . LLJ ::..:: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B065.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:36 through 1-0CT-2016 12:00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 2.000000E-02 Q) .µ. l1j (t'. lJ c ::; 0 1-"0.I) . 0,1 ............................................................................ .::£. u l1j co . . . . . . X* 0 x x x x x x x x 3-16 4-16 5-16 x x *x x x x x x 6-16 7-16 MeasureMent Date/TiMe x x* x x x x x x 8-16 9-16 x UP LOW ..... ..... '° 0\ 0 ......, Vl 00 0 '° QA f i lenarrie
DKA100: [ENV_ALPHA.QA.W]W066.QAF;8 Pararrieter Narrie AVRGEFF (Average Efficiency) Start/End Dates 24-AUG-2016 10:44:17 through 1-0CT-2016 12:00:00 Lower/Upper Lrrits: 0.253080 through 0.268734 UP . 265 ............................................................................ . . . . . >, 0 x c Q) *r-1

0 *r-1 4-4-UJ x Q) '26 '0.0 ... x .......... : .............. : .............. : .............. : ............. ; ...... . llj l-x Q) > <I: x x I 255 ' o o o o ' o ' ' 0 o 1 o 10 o o 1 o o o o ' ' ' ' ' ',' ' o o ' ' ' ' ' ' ' ' ' ',' ' o ' o ' ' ' o o ' o ' *,' o 1 ' ' o o ' 0 o o o 0 : o ' o o ' ' o 8-24 8-31 9-07 9-14 9-21 9-28 LOW Measurerrient Date/Tirrie QA filenafY'le ParaMeter NafY'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W066.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 24-AUG-2016 10:44:17 through 1-0CT-2016 12:00:00 184.000 through 204.0DO 200 0 I 0 o 0 I 0 I 0 0 I 0 I 0 0 o I o o o o I I o o 0 I I o 0 o I o o o o o I o o o o I o I o o I o o o o o I o o o I I o o o o o o o o O O o o o o I o o I D )-I-H > H I-u <I: w D H ...J u ::r* z x x x x x . . . . . x x . . . . . 190 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-24 8-31 9-07 9-14 9-21 9-28 MeasureMent Date/TifY'le UP LOW
....... ....... \0 00 0 ......, VI 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W066.QAF;8 PSFWHM-G0148 (PEAK RESOLUTION GD-148) 24-AUG-2016 10:44:17 through 1-0CT-2016 12:00:00 5.00000 through 100.000 80
0 o o o ' ' o o 0 0 I o 'o o o I o o o o 0 I o 0 o o 01 o o o o 0 0 0 0 I o o o o'o I o 0 o o I o o o 0 I I .. o o o I o 0 0 o I o o o o : o 0 0 o I o o ..-1 I 0 (!) z 0 H 1-::i _J 0 01 w O:'. :::.! <I: w 0... 60 40 . . . . . . I I I o o o I o o o I 0 0 0 0 0 I o o o o I I o o 0 I I 0 o O I I o o o I I o O O O I o o o o o I o O o O O O o o I O O O O o I o o o o 1 o O O o I o o xx x >i< . . . . . x . . . . . x 0 I o o o o o o o o o 0 0 0 o 0 I o o o o I o o o 0 I I 0 o O I I o o o I o o o O o I o o o o o o o o O I I o o o o o o o o O I o o o o o o o o o o o o I 0 o o I 20 ............................ *' ............ '* ............. ' .................... . 8-24 31 9-07. 9-14 9-21 9-28 Measurerrient Date/Tirrie UP LOW
--\0 \0 0 ......, VI 00 0 \0 QA filenarrie ParaMeter Narrie 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W066.QAF;8 P5ENERGY-GD148 (PEAK ENERGY GD-148) 24-AUG-2016 10:44:17 through 1-0CT-2016 12:00:00 3143.00 through 3223. 00 . . . . . 3200 ' o o ' ' o o ' ' o ' ' o o o ' o o o o o I I o o o o o o o o o o e e o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o 0 o I o 0 . . . . co ""'" ..-i. I D (.!) )-(.!) a: x x Li.I 3180 z I o 0 I 0 ............................................................... ' ............ . . . . . . Li.I lo.:: ([ Li.I 0.. 3160 8-24 8-31 9-07 9-14 9-21 9-28 Measurerrient Date/Tirrie UP LOW ....... N 0 0 0 ......, VI 00 0 \0 QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.B]B066.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 16:21:36 through 1-0CT-2016 12: 00: 00 O.OOOOOOE+OO through 2.000000E-02 . . . '01 ............................................................................ . . . . . . x x x x x x x x x X X X X . X X X X X X X X X* X X X X . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe x x x UP LOW 0 Hi v. 00 0 '° QA filenarrre Pararrreter Narrre 5tart/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W067.QAF;8 AVRGEFF (Average Efficiency) 24-AUG-2016 10: 44:17 through 1-0CT-2016 12:00:00 0.284161 through 0.301737 ' . . . . .3 .............................................................. ' ............ . u c (I) *r-1 u *r-1 4-4-LU (I) "0.0 iO 1-(1) > cr: . . . . '295 ............ *:* ............ *:* ............ *:* ............ *: ............. : .... x .. xi: xx x . . . . . . 29 ............................................................................ . . . . . '285 ............... * .............. * ............ * .............. * .............. : ...... . 8-24 8-31 9-07 9-14 9-21 9-28 Measurerrrent Date/Tirrre UP LOU.I -N 0 N 0 >-+, Vl 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W067.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 24-AUG-2016 10:44:17 through 1-0CT-2016 12: 00:00 184. 000 through 204.000 200 ............................................................................ I Cl )-t-H > H t-u a: w Cl H ....I u =i z x x x . . . . . x . . . x 190 . **-* ........ *:* ............ *:* ............ *:* ............ *:* ............ : ...... . 8-24 8-31 9-07 9-14 9-21 9-28 MeasureMent Date/TiMe UP LOW -N 0 l;.l 0 Hi v. 00 0 "° QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W067.QAF;8 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 24-AUG-201610:44:17 through 1-0CT-2016 12:00: 00 5.00000 through 100. 000 100 UP .-I I Cl z 0 H ::J ....J 0 w O:'. a: w 0... 80 ............. * .............. * .............. * ......... * .... : ............. : ...... . . . . . . 60 o o 0 0 o I I I 0
o o o o o o o o o o o o o 0 I 0 o 0 I o o o O o o o o o o o o o o o o 0 I I O o o o O *' o o o o o o o o o o o o o o o o o o o o o o ' . . . . x x x 0 I o o o o o o o o o o o o I o o o o o o 0 o o o o o o o o I o o o o o o o I o o o I e o o o o o o o I ' o I o o o o I o o I 0 Io ' 0 0 o o o o o I o . . . . . 40 2.0 .......................................... '* ............. ' .................... . 8-24 8-31 9-07 9-14 9-21 9-28 LOW Measurer.-.ent Date/Tir.-.e QA filenaMe DKA100: [ENV_ALPHA.QA.W]W067.QAF;8 ParaMeter NaMe PSENERGY-80148 (PEAK ENERGY GD-148) Start/End Oates 24-AUG-2016 10: 44:17 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . ............... ' ........... ' ......................... ' ..................... . . . co ""'" .,-j I D )-0::: x x l.J.J 3180 z . . . . . o o o o o 0 ' o o o o o o 0 o o 0 o o o o o 0 ' 0 0 I 0 o o o o 0 0 0 o o o o o o o o o o o o o o o o o o 0 o o o o o 0 ' o I I o ' o o o

o o ' 0 ' o . . . . ' l.J.J :,,:: a: l.J.J 0... 3160 8-24 8-31 9-07 9-14 9-21 9-28 LOW MeasureMent Oate/TiMe
-N 0 Vo 0 ......, Vo 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B067.QAF;2 ParaMeter Na.Me BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:36 through 1-0CT-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 X* ' . . . . '01 .......... : ........... * ......... *.* ......... * ........... * ........... * ........... . x x x x :?< 0 3-16 4-16 x x x X X X x X *X X X X x x x x* x x x x x 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ..... N 0 O'I 0 ....., VI 00 0 \0 QA filenarrie Pararrie ter Narrie Start I End Da-tes Lower/Upper LMts: . 285 DKA100: [ENV_ALPHA.QA.W]W068.QAF;8 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 0.268440 through 0.285qso . 28 .......... : .......... * ........... * ...................... .-.......... : .......... . o* c Q.) *r-1 x x 0 *r-1 .x 4-4-UJ Q.) "0.0 l'(i I-. 275 Q.) . *_ ........ : *x ....... *:* ....... :. *:* ......... '. .......... *: .......... *: .......... . > <I: *x *X x .. 27 .......... : . ,* ........ * .......... ,*, ......... .-........... * ...................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tirrie UP LOW -N 0 -l 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W068.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27: 07 through 1-0CT-2016 12:00:0D 184.000 through 204. 000 200 o I I I o ' 0 o I o o I o o o o I o o o o 0 o o o o I
o o o o o 0 I 0 I I o o o I I o o o I o o o I o I I I o I I I o o o I I o o o o o o o o o 0 o I . . . . . . I D (!) )-I-H > H I-u a: w *x *X D H x ....J u ::i *X z 190 .......... : ......... *:* ......... *:* ......... *: .......... *: .......... *: ......... *x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... N 0 00 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W068.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 5.00000 through 100.000 . . . . . -. 80 ' o o 0 0 0 I o 0 o o o o 0 o o I o o o o o I o o o o I o o 0 0 0 0 o o I o o o o o I 0 0 0 0 I 0 o o o I I o o o I 0 0 0 0 I I o 0 o o o o o o o I o o I D (!) z 0 H ::i ....I 0 (f) ll.J Ct: . . . . . . 60 o I o o o I I o o o o I 0 0 0 I I 0 0 0 o 0 o o o o o o o o o I I o o o o o o o o o 0 o o o o I I o o*o o o o o 0 o 0 0 o o o I o 0 o o I o o o o I I o . . . . . . x x *x x *x *x x . . . . . . 40 I I o o o o o o o o I o o o o o o o o o o I I 0 0 0 I I 0 o o I o o o o I I o o o o I 0 0 0 0 O I o o o o I o o o I I o o o I I O O o O I O o o O I I o I I o o o o 20 .......... ' .......... " ......... " .......... ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -N 0 \0 0 >-+, Vl 00 0 \0 QA filenaMe DKA100: ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . o ' o o ' o o o o o o I o 0 o I I o o o e I I o o I I I o 0 o 0 I 0 o o o o o o o o o o o o o I I o o 0 I I 0 o o o o o o 0 o o o o o o o o o o o o o o co -.;j-...-1 I D (!) )-(!) et:: :x :x x x .x x x LI.I 3180 :z . . . . . ..... ' ..................................................................... . . . . . . . LI.I ::...::: <C LI.I 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ,_. N ,_. 0 0 >-+, VI 00 0 '-Cl QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.B]B068.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 16:21:36 through 1-0CT-2016 12:00:00 O.OOOOOOE+OO through 2.000000E-02 . . . . . . x '06 o o o o o o o o o o o o o o O o O o o o O I I O O o I
O o o I o o o o o o o o o o o o o o o I o 0 0 0 I o 0 o o I I o o o o o o o o o I o o o o I o 0 Q) """' aj O:'. 1J C* :J 0 5-"0.0 .::L. (.) aj co . . . . . . '04 .......... : ........... * ......... *.* ......... * ........... * ........... * ........... . '02 0 x x 3-t6 Measurerrient Date/Tirrie UP LOW
...... N ...... ...... QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W069.QAF;11 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 0.318777 through 0.338495 *x x '335 X ......... : .......... * ........... * .......... : .......... : .......... : .......... . . . . . . . u c Q) *ri u '33 *ri *X 4-4-LU Q) "0.0 ({j I-)( Q) > a: :x . . . . . ' '325 . ' .... ' ........ ' ........................................................... . . . . . . . x .32 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... N ...... N 0 ......, Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W069.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:-00 184.000 through 204,*ooo 200 .......... : ........... * ......... *.* ......... " .......... * ........... * ........... . I Cl )-..... H >* H ..... u a: L1J :x Cl H ....I u x .x :J z 190 o ' o ' ' ' o ' o o : ' ' o ' ' I*' o ' e 'o 0 o 0 o 0 I o o o o'o o o o I I o 0 o o .. o o o o o I o o o o o' o 0 0 0 cl o o o I I .. o o o I o o o o I o o :x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW -N -w 0 ......, Ul 00 *o \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W069.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 5.00000 through 100.000 '<'i I Cl z 0 H 1-::i ....I 0 f3* O:'. ::..:::* a: w 0... 100 so x . . . . x . *_X * .
X * *x X . , ........ ' .......... -.X ........ **X* ........ .-.......... .-... " ...... .-.......... . . . . . . . 60 I 0 ' ' ' ' ' ' ' o * * 'o 0 * * * * ' I 0 0 0 ' I 0 o 0 0 I o 'o o o o o o o o o o o 0 o I 0 o 0 I 0 I 0 0 0 I I I 0 0 o I O I o o I O o O o I o o . . . . . . . . . . 40 .......... ' ......................... ' ...................................... . . . . . . . 20 .......... ' ..................... '*' ......... ' .......... ' .......... ' .......... . 3-16 4-16 .5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Time. UP LOW
-N -.j:::.. 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W069.QAF;11 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-MAR-2016 13: 27: 07 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 ' I o I I 0 ............................................................................ CD '<;f" "<"i I D )-Ct:: LLJ 3180 z :x :x x x *x x x . . . I o o I I ' o o o I o o I o o I I I o I I 0 o 0 0 I I I o o 0 0 I o o o o o o o o o o e o o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o . . . . . . LLJ :::..: a: LLJ Cl.." 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ,_. N ,_. VI 0 ....., VI 00 0 ID QA filenaMe DKA100: [ENV_ALPHA.QA.B]B069.QAF;5 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16: 21:36 through 1-0CT-2016 12:00: 00 Lower/Upper iMts: O.OOOOOOE+OO through 2. OOOOOOE-02 '01 ............................................................................ . . . . . . X X X X X X X >( X X X X . X X X X X X X X X* X X X X 'X X X >)< 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -N -0\ 0 ....., Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Oates Lower I Upper _Lr.-. ts: DKA100: [ENV_ALPHA.QA.W]W070.QAF;10 AVRGEFF (Average Efficiency) 25-AUG-2016 08:42:44 through 1-0CT-2016 12:00:00 0.308333 through 0.327405 I 325 I 1 1 1 1 1 O 1 1 1 o 1 1 .. 1 1 O o I 1 1 1 1 1 1 1 1 I, I 1 1 1 1 1 1 1 O I 1 1 1 101 1 1 I 1 1 1 1 1 1 1 I I 1 01 1 1 1 1 1 O I 1 1 1 1 1 1 .I' 1 1 I I 1 )( x x >.. u C* Q) -r-1 u -r-1 ....... ....... LLJ . 32 I 0
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I I I x x . . . . . I 31 I o I I I I I i I I 0 I I ', I I I I I I I I I I o I I ',I I I o o I 0 I I I I I o ',' I I o I o o I I I 0 I I I,' I o I I I I I I I I I o I : o o I 0 I 8-25 9-01 9-08 9-15 9-22 9-29 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W070.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY 08:42:44 through 1-0CT-2016 184.000 through 204.000 . . . 200 ............. * ............ '* . * .............. *.* .......... -.... * .............. : .... . I D )-I-H > H I-u <I: w D H ...J u x x x z 190 ................. ' ........... * .............. * .............. * .............. * ..... . x 8-25 9-01 9-:08 9-15 9-22 9-29 Measurer.-.ent Date/Tir.-.e UP .LOW
....... N ....... 00 0 ......., Vl 00 0 \0 QA filenar.-.e Pararrieter Narrie Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W070.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 25-AUG-2016 08:42: 44 through 1-0CT-2016 12: 00:00 5.00000 through 100. 000 ..-f I D z 0 H 1-=i ....! 0 O") w O:'. <* ....*..* : *.*....*.....* : .............* : .....*........ : .. *x .. x . . . . . . . . . . 40 ............................................................................ . . . . . 20 ............. ' ............. " .............. *' ............................ , .... . 8-25 9-01 9-08 9-15 9-22 9-29 Measurerrient Date/Tir.-.e UP LOLI.I ,_. N ,_. "° 0 ....., Ul 00 0 "° QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W070.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 25-AUG-2016 08:42:44 through 1-0CT-2016 12:00:00 3143.00 through 3223. 00 . . . . . 3200 o o o o o o I o o O O O 0 o 0 I I 0 o o o o o e o o o o o o o o o o o o 0 o o o o 0 I o o o 0 o o o o o o o o o o o o o o o I I 0 o o o o o o o o o 0 o . . . . ro """" ..-I I D (!) )-(!) et::. x x LL.I 3180 z . . . . . ............................................................................ . . . . . LL.I ::..::: a: LL.I CL 3160 *************-***********************************************************-***** 8-25 9-01 9-08 9-15 9-22 9-29 Measurerrrent Date/Tirrre UP LOW -N N 0 0 ....., Vl 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B070.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) .Start/End Dates 4-MAR-2016 16:21:36 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 I]) """' tlj O:'. lJ c ::::; 0 'OIJ ::L. (.) tlj co . . . . '01 .......... : ........... * ......... *.* ......... * ........... * ........... * ........... . x x x x 0 x x x x x x x x *x x x x x x x x* x x x x .x x x >x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... N N ...... QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W071.QAF;10 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 0.312000 through 0.332340 . 33 .......... : .... ' ..... * ........... * .......... : .......... : ...................... . ::;.., 0 c Q) *ri 0 *ri 4-4-UJ Q) "OJ) J'(i O) > a: x :x . 32 .......... : .......... * ........... * .......... ; .......... ; .......... : .......... . . . . . . x *x x :x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W071.QAF;10 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 Lower/Upper LMts:. 184.000 through 204.000 UP 200 .......... : ........... * ......... *.* ......... * ........... * ........... * ........... . I D r H > H u w D H *X .x u x z 190 :x . . . . . . . . . . : . >:: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . ;<. . . . . . . . . . .. . . . . . . . . . * .. x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ...... N N w 0 ...., Ul 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.W]W071.QAF;10 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 LMts: 5.00000 through 100.000 ...... I 0 C) z 0 H :::J ....I 0 en w O:'. 100 80 . . . . . . o 0 0 o o o o o o o o o o o o o I o o o o o I o o o o I o 0 o 0 0 o o 0 I o 0 o 0 o I 0 0 0 o I o o 0 o 0 o o 0 o o o o o o o o o o o o I o o o o o o o . . . . . . 60 o 0 0 o o o o o o o ,-, o o o o o o o o o o o o o o o o o o o o I o o o o o o o o 0 I o o o 0 I o o o o 0 I 0 o o I I e 0 0 I I 0 0 o 0 0 o o o o o o o . ' . . . . x :x x x x *X *X . . . . 40 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 0 o o o o I o o o o I 0 o 0 0 I I 0 0 e e o o o o o o o o . . . . . . 20 ..................... " ......... '*' ......... ' .......... ' .......... ' .......... . 3-1'6 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -N N .j::. 0 ......, VI 00 0 '-0 QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]WOi1.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 3143. oo through 3223.00 . . . . . . 3200 o o o o o o o o o o o O o o o o o o o o o o o o o o I O O o o o o o ,o o O I O O o O O o o o O I I o o o I I o o 0 I I 0 o 0 I I o o o o o o 0 0 0 I I o . . . . . . co "¢ "<"i I D C) )-Cl c::r: x : ,x :x :x *X x x LLJ 3180 z . . . . . . 0 I 0 o o I o o o o o I 0 0 0 I I 0 0 o o I I o o o o I 0 o 0 I *, o o o I I o o o 0 0 o o o o o I o o 0 0 o o o o I o o o o I I o o o o o o o o o I o o . . . . . . Ll.J :..: a: Ll.J Ci.. 3160 3-16. 4-16 5-16 6-16 7-16 8-16 9-:-16 MeasureMent Date/Tirrie UP LOW -N N Vl 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B071.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:38 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 0, OOOOOOE+OO through 2.000000E-02 . . . . 01 .......... : ........... * ......................................................... . . -x x x x x x x x x x x x x . x x x x x x x x: x x x x .x x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaf'l"le Pararrie ter Narrie 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W072.QAF;10 AYRGEFF (Average Efficiency) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 0.313679 through 0.333081 . . . . . . .33 ............................................................................. >, (j c Q) *r-1 (j -r-1* ........ ........ UJ . . . . . . . 325 . . . . . . . . . . : . . . . . . . ... *. . . . . . . . . . . . . . . . . . . . . . : . . . . . . . . . . .* . . . . . . . . . . .. . . . . . . . . . . . :x .32 . . . . . . . . . . : . . . . . . .... : . . . . . . . . . . . : . . . . . . . ... X.: . . . . . . . . . . x* . . . . . . . . . . . . . . . . . . . . :x :x x . . . . ' . 315 x o o o o o o I 0 o o o o o o o o o o o o o o I o o o o I o o o o I o o o o o o o o o o 0 0 0 o o o o o o o o o o o o o o o 0 0 I o o o o o o o o o o o o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W072.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13: 27:07 through 1-0CT-2016 12:00:00 184. 000 through 204.000 200 .......... : ........... * ......... *.* ......... * ........... * ........... * ......... : .. I D )-I-H > H I-u a: ll.J D H ...J x *X x u ::i z 190 . :x . . x . . . ' x ......... : .......... * ........... * .... ' ................. x ... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifYle UP LOW QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper Lrrits: 100 x DKA100: [ENV_ALPHA.QA.W]W072.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 5.00000 through 100.000 :x . . . . . . 80 ............................................................................ ..-l I D (!) z 0 H ::i ....I 0 (j') w O:'. a: w 0... . . . . . . 60 o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o o o o o o o o I o o o o o o o o o o 0 o o o ' o o o o o o o o o o o o o o o o o o . . . . . . *X :x x . . 40 o o o o o o ' o o o o o o o o o o o o o o o 0 ' o 0 I o o o o o o o o o o o o o o 0 I o o o 0 o o o o o o o o o o o o o 0 o o 0 o o o o o o o o o o o o ' . . . . . 20 .......... ' .......... *' ......... '*' ......... ' .......... ' .......... ' .......... . 3-16 4-16. 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW -N N \0 0 ......, Ul 00 0 "' QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper 3220 DKA100: [ENV_ALPHA.QA.W]W072.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 3143,00 through 3223. 00 . . . . . . 3200 o 0 0 '0 I 0 ' a' o ' ' ' ' ' I ' ' ' ' I o 0 0 ' I 0 0 o 0 I 0 o 0 o I 0 o o ,o o I o o o o o I o o o 0 I 0 0 o o 0 o o o o o o I o o o o O o O I I o . . . . . co v -n I D )-(t'. x x *X *X :x x LLJ 3180 z . . . . . . .......... : .... ' ' ..... * ....... " .. *.* ......... * ........... * ........... * ........... . LLJ :::..::* a: LLJ a. 3160 ............................................ -.......... -.......... -.......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW -N VJ 0 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B072.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21: 38 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2. OOOOOOE-02 Q) irj O:'. lJ c ::i 0 s.... "O.(I ::£. u irj. co '01 .............................................................................. . . . . . . 0 x x x x x x x 3-16 4-16 x X" x x 5-16 x *x x x x x x x x x x x x x x x 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -N I.;.) -0 ......, VI 00 0 \Cl QA filenafYle Pararrieter NaMe Start/End Dates Lower/Upper LMts: *: DKA100: [ENV_ALPHA.QA.W]W073.QAF;14 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:07 through 1-0CT-2016 0.325020 through 0.345130 12:00:00 o o 0 o o I '34 ' I o o o I ' o I o o I o o o I I o o o o I *1 o o o '° I 0 o 0 0 I 0 I o 0 0 0 o 0 0 I o o o o I I o o I o I o o o I 0 0 o 0 I I 0 0 0 0 I o o I o o I o . . . . . ' ::., u c I].) -r-1 u -r-1. x .x x x *x 4-4-x LU 11) "0.0 (fj .: x I-I].) > <I: .33 * * * * * ' * * *
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-N VJ 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W073.QAF;14 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-MAR-2016 13:27:07 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . o I 0 0 0 o I o 0 o o o o o o o I o o o o I o o o 0 I 0 o o o I I o o o o o o o o o o o I I 0 I I o o o o I o o o o I 0 0 o I I o O o o I o o o o I I o . . co """" ..,-t I D (!:I )-(!:I a::: x :x :x :x x x LLJ 3180 z . . . . . ..................... ' ..................................................... . . . . . . . LLJ :..::: 0: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ....... N w Vl 0 ,...., Vl 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B073.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:38 through 1-0CT-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 '01 ............................................................................ . . . . . . x X X X X *X X X X X X X 0 X* X X X X "X X X X 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafYle ParafYleter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W074.QAF;10 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 0.299700 through 0.318290 . . . . -. . .315 ............................................................................ . . . . . . >, u c Q) *l"'I u . 31 *l"'I 4-o ' o o o o o o o o '. o o o o o o o o o e :* I o o o 0 I 0 o o *:x* o o I I o o e o : o o 0 o 0 0 o 0 o I : e o o o I o o o I o : o o 0 I o o 0 I I I o 4-Ll.J. *x Q) 'OIJ x x (lj Q) > a: . 305 x :x x I o o o o o . 3 .___*_*_*_*_*_*_*_*_*_*_._* _*_*_*_*_*_*_*_*_*_*...._* _*_*_*_*_*_*_*_*_*_*........_* 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifYle UP LOW -N VJ -.l 0 ....., VI 00 0 l.O QA filenaMe ParaMe ter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W074.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12:00:00 184.000 through 204. 000 200 .......... : ........... * ......... *.* ......... * ........... * ........... * ........... . I D )-I-H > H I-u x ;> * * * * . . ** * * . : * * * . . * * * * . * * * . * * * * * . * >.. u c* 1rr *ri u *ri x 4-. 325 4-. . . . . . ............................................................................. I I o 0 o I UJ Q) "0.0 iU :x x :x I-Q) > Cl: x x . 32 :x . 315 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ......... . 3-16 4-16 5-16 6-16 7-:-16 8-16 9-16 Measure!Ylent Date/Tifl'le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W075.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13: 27:07 through 1-0CT-2016 12:00: 00 184.000 through 204. 000 200 ............................................................................ . . . . . . I Cl )-I-H > H I-u a: x w Cl *X H -I :x u ::i z 190 x . . . . x . . x*_ ........ : ......... *.* ......... *.* ......... * ........... * ........... ........ . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W075.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27: 07 through 1-0CT-2016 12:00:00 5. 00000 through 100.000 80 .......... : .......... * .......... ,*, ......... .-.......... .-.......... .' .......... . ..-t I D C) z 0 H 1-::i --' 0 f.f) w O:'. :::.::: a: w 0.. . . . . . . 60 o o o o o o O O I o o O 0 e o I o o o o o I o o o O I I O 0 0 I o o o o I I o o o o I o o o O I I 0 0 0 I I o o o I I o o O I I 0 0 o o I o o o o I I o . . . . . . x x x :x x .x :x 40 ............................................................................ . . . . . . 20 ............................................ ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W075.QAF;11 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13:27:07 through 1-0CT-2016 12: 00: 00 3143.00 through 3223.00 . . . . . . 3200 o o o o o I o 0 0 0 0 I o O o I I o o o o o
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-Vi 0 ,..., Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B075.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 16:21:38 through 1-0CT-2016 12:00:00 O.OOOOOOE+OO through 2.000000E-02 . 01 ............................................................................ . . . . . . x x x x x x x x x x x x x. x *X x x x x :x x x x x x x x x x x 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOU.I Qfi filenar.-.e DKA100: [ENV_ALPHA.QA.W]W078.QAF;11 Parar.-.eter Nar.-.e AVRGEFF (Average Efficiency) Start/End Dates 4-MAR-2016 13:27:08 through 1-0CT-2016 12:00:00 Lower/Upper Lr.-.ts: 0.325057 through 0.345163 UP . 34 ' o '
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0 0 '*' 0 0 0 ' ' 0 0 0 0 .. 0 0 0 * ' 0 0 0 0 0 .. 0 0 0 0 ' 0 0 0 ' 0 .. 0 0 0 ' 0 0 0 0 0 ' 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper Lmts: DKA100: [ENV_ALPHA.QA.W]W080.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13: 27:08 through 1-0CT-2016 12:00:00 184. 000 through 204.000 200 .......... : ........... * ......... *.* ......... ' .......... * ........... * ........... . I 0 (!) )-..... H > H* ..... u :x x <I w 0 x *x x H* ....I u x :x x =i z 190 .......... : .......... * ........... * .......... : .................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW
....... N Vl VJ a; Vl 00 0 \0 QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W080.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:08 through 1-0CT-2016 12:00:00 5.00000 through 100. 000 . . . . . . 80 o 0 0
0 0 o 0 o o ' 0 o 0 o 0 0

0 o o 0 I o o o o o ' o ' 0 o 0 o 0 o 0 o ' o 0 ' o 0 0 " 0 0 o o o 0 o o ' 0 0 o ' o o o o o o o 0 o o o o o o o o ..-1 I 0 (.!) z 0 H ::i ....I 0 (J) w Ct'. ),..! a: w 0... . . . . . . 60 ............................................................................ . . . . . . x x *x :x x :x x x 40 ............................................................................ . . . . . . 20 .......... ' .......... " ..................... ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W080.QAF;10 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-MAR-2016 13:27:08 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . o I o o o 0 I o 0 o o I o o o o o o o o o o o o 0 o 0 I 0 o o o o o o o o o o o o o I o o o o I o o o

I I o o o I I o o o I I o o o o I o 0 0

I I o co v ""'"" I D )-et:: :x :x X_ .x x x x LLJ 3180 z . . . . . . ......................................................................... ' .. . . . . . . LLJ :::..::: <I: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
...... N Vi . Vi 0 ,....., Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B080.QAF;3 PqraMeter NaMe BACKRATE (Background Rate) Start/End DateB 4-MAR-2016 16:21:42 through 1-0CT-2016 12:00:00 Lower/Upper LMtB: O.OOOOOOE+OO through 2.000000E-02 ID .._;. llj O:'. 1J c :J 0 5-'0.0 _y_* .01 ............................................................................ u llj* co . . . . . . 0 x x x x x x x x x x x
x x x x x x x_ x* x x x x *x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeaBureMent Date/TiMe x x x UP LOW
-N Vi 0\ 0 ......, Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W081.QAF;9 AYRGEFF (Average Efficiency) 4-MAR-2016 13: 27:08 through 1-0CT-2016 12: 00: 00 0.324850 through 0.344947 . 34 o I o o o O o o o o : O o o o o O O o o o 1o O o o o O O I o o 111 o o o o o o o o o .. o o o o o o o o o I .. o I 0 0 0 o 0 o ' I .. 0 I o I I I I 0 I I o ), (..) c Q) *r-1 (..) *r-1 4-4-x LU Q) 'OJ) l1j x I-Q) x >. a: *x . . . . . 33 ............................................................................ . . . . . . *x :x x 3-16 4-16 5-16 6-16 7-16 . 8-16 9-16 Measurerrient Date/Tirrie UP LOW -N Vl -....) 0 ......, Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/ End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W081.QAF;9 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27:08 through 1-0CT-2016 12: 00: 00 184.000 through 204.000 200 o ' o o o o ' o o o ' ' o o o ' o o o o o o ' o ' o ' o o o o o o e o o 0 0 o o o o o o o o o I o o o o o o o o o 0 I 0 I o 0 I o o o o o o o o o I o o . . . . . . I o* (!) )-I-H > H I-u a: w x x :x *X 0 H ....I *x x u :J z 190 .......... : .......... * ........... * .............................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW -N Vl 00 0 ....., Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End DateB Lower/Upper Lr.-.tB: 100 DKA100: [ENV_ALPHA.QA.W]W081.QAF;9 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:08 through 1-0CT-2016 12:00:00 5.00000 through 100.000 80 . . . . . . . . . . : . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : . . . . . . . . . . .. . . . . . . . . . . .. . . . . . . . . . .. I o. z 0 H =i -' 0 Cf) w O:'. a: w 0... . . . . . . 60 0 I e o 0 o 0 o o ' o o o o o o o o o o o ' o o o o o o o o o o I o o o o o o 0 0 o I 0 ' o o o o o o o o o o o o o o o o o 0 I 0 0 ' o 0 o ' o o o 0 0 . . . . . . x x x *x *x :x x x 40 ............................................................................ . . . . . . 20 ..................... " ..................... ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tir.-.e UP LOW ...... N Vl \0 0 ....., Vl 00 0 \0 QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W081.QAF;9 P5ENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13:27:08 through 1-0CT-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ............... ' ........................................................... . . . . . . . co ""'" ..-I I D 8 )-8 et:: x x :x .x x :x LLJ 3180 z ' . . . . o o o o o o o o o o o o o o o o o o 0 o o I I 0 0 0 0 0 o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o I o o . . . . . . w ::...:: a: w CL 3160 ********************************************-**********-**********-*********** 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW ....... N 0\ 0 0 ....., Ul 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B081.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16: 21: 42 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . . . . 01 ............................................................................ . . . . . . x 0 x x x x x x x x x x x . x x x x x x x x x: x x x x :x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ..... N 0\ ..... 0 H, Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W082.QAF;9 AVRGEFF (Average Efficiency) 4-MAR-2016 13: 27:08 through 1-0CT-2016 12: 00: 00 0.312914 through 0.332270 . . . . . . . 33 ................................. -......................................... . >, u c Q) *r-i u *r-i 4-4-UJ* Q) "0.0 i(i Q) > a: .325 x . . . . . . . 32 .......... : ........... * ..................... * ........... ;;(* ......... *. x ......... . . . . . . . x x x *x :x . . . . . . .315 o o o o o o 0 o o o o o o o o ' o o o o o o o o o ,o o o o o o o o
o o o 0 o o o o o o o

0 0 0 o o" 0 I o o o

o o o o o I o o o o o o o o o o o o o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W082.QAF;9 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13: 27:08 through 1-0CT-2016 12:00:00. 184.000 through 204. 000 200 ..................................... ' ............. -........................ . . . . . . . I Cl (!) )-I-H > H I-u a:. x *X w Cl H x *X .x x _J u =i z 190 .......... : .......... * ........... * ............................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-N °' VJ 0 ......, Vt 00 0 \0 QA filenal'le Paral'le ter Nal'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W082.QAF;9 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:08 through 1-0CT-2016 12:00:00 5.00000 through 100.000 80 .......... : ' ......... * ........... * ....................... * ...................... . ..-I I D (!) z D H 1-::J ...J D (f) LlJ O:'. . . . . . . 60 o o o o o o I o o o o I o o o o I e o o o o I o o o o I o o o I o o o o o o o o 0 o I 0 0 o o I I o o o I o o o o o o o o o 0 I 0 0 ' o o o o o o o I o . . . . . . x x :x .x *x x x 40 .......................................................... ' ................ . . . . . . . 20 .......... ' ................................. ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til'le UP LOW QA f i lena!Y'le . Para!Y'leter Na!Y'le 5tart/End Dates Lower/Upper LIY'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W082.QAF;9 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13:27:08 through 1-0CT-2016 12: 00:00 3143.00 through 3223.00 3200 .......... : .......... * ........... * ........ * .. : .......... : .......... : .......... . ro ""'" I. D (!) )-(!) et:: x x *x x :x .x LLJ 3180 z . . . . . . o 0 o o o 0 o o o o o I o o o o o o o o o o o o o o o o o o o o 0 o o ' 0 o o o o o o o o o o o o o o o o o o o o o o ' 0 o I 0 o o o e o o o o o o o o . . . . . . LLJ :,..::: a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Y'lent Date/TilY'le UP LOli.I QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B082.QAF;3 BACKRATE (Background Rate) 4-MAR-2016 16:21:42 through 1-0CT-2016 12: 00: 00 O.OOOOOOE+OO through 2.000000E-02 x . 04 .......... : ........... * ......... *.* ......... * ........... * ........... * ........... . ID .f.) l1j O:'. 1J c :J 0 s.... 'O.(l .::L. (J l1j co . 02 X-X X X X X X X X X X x x x* x x x x *x x x 3-16 4-16 5-16 6-16 8-16 9-16 MeasureMent Date/TiMe UP LOU.I QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: >i u c I]) *r-1 u *r-1 4-4-LU I]) 'OJ) iU I]) > a: '36 x DKA100: [ENV_ALPHA.QA.W]W083.QAF;10 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:09 through 1-0CT-2016 12:00:00 0.347305 through 0. 368790 x *X *x . . . *X '35 ............................................................................ . . . . . . x 3-16* 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaf'le Paraf'leter Naf'le Start/End Dates Lower/Upper Lf'lts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27: 09 through 1-0CT-2016 12:00: 00 184.000 through 204.000 200 I I I I I o I I I I I o I I I I I I I I I o I I I I o o o I I I I I I I o o I I I I 0 o I I I I I I I I o I I I I I I I I I o I I I I I I I I I I o I I . . . . . . I D C!:I )-. I-H > H I-u a: w D H x x :x x x ....! u x x ::i z 190 .......... : .......... ......... * ................................... :0 ......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measuref'lent Date/Tif'le UP LOW ...... N 0\ 00 0 ....., Vl 00 0 "° QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W083.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 t3:27: 09 through 1-0CT-2016 12:00:00 5.00000 through 100. 000 80 . . . . . . ' . . . : . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . .. . . . . . . . . . . : . . . ' . . . . . . . ..-l I D C) z o* H ::. ....I 0 U') l.LJ Ct'. a: l.LJ Q. . . . . . . 60 o o o o o o I o o o o o o o o o I o o o o O o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o
0 0 I 0 o

o I 0 0 o o o o o o o o o o . . . . . . x *X :x x .x x x . . . 40 ............................................................................ . . . . . . 20 .......... ' .......... *' ......... '*' ......... ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W083.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13:27:09 through 1-0CT-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 o ' ' ' 0 0 I 0 I I o o o o o o o 0 o 0 0 I I 0 o 0 I I o o o I o o o o I I o o o o I o o o o O o o o o I o o o o O O O o O I o O O o o I o o O O O I O . . . . . . co v "<"i I D )-0:: x x :x x :x *X LU 3180 z . . . . . . ' 0 0 o o 0 o o o I o o o o o I I o o 0 0 0 I o I 0 o o 0 o o I I o o o o I o o o o o o o o o o I o o o I I o o o I I O o O I O O o Io O o o O o 1 1 o . . . . . . LU ::..: a: LU CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B083.QAF;4 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:44 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 2.000000E-02 UP . 01 ............................................................................ . . . . . . 0 x x x x x x x x x x x x . x x x x x x x x x* x x x x :x x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenarrie Parafl'le ter NaMe Start/End Date8 Lower/Upper Lrrit8: >> (.) c ID *r-1 (.) *r-1 4-4-Ll.J .35 DKA100: [ENV_ALPHA.QA,W]W084.QAF;9 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:09 through 1-0CT-2016 12:00: 00 0. 337400 through 0.358200 x :x x *x x *X x . 34 ............................................................................ -. . . . . . x x 3".""16 4-16 5-16 6-16 7-16 8-16 9-16 Mea8ureMent Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W084.QAF;9 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) -: 4-MAR-2016 13:27: 09 through 1-0CT-2016 12:00:00 184.000 through 204. 000 200 0 I o o I I o o o o I I o o o I o o I I 1 I o I o o o o o o 1 I I o o o o o o o O O I o o o o 1 o o o o I o o o o o o I o O I I o o o o O o O o o o o o I D (!) >-1-H > H 1-u a: w D H* ....I u ::i z . . . . . . .x x x :x *x x 190 o o o o o o o o o e : I o o o I o o o 0 o *, I o o o o I o o o o'o o o o I I 0 o o o ," o o o o o o o o o I ," o o o I I o o 0 I I .. o o o I 0 o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W084.QAF;9 ParaMeter Name PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 4-MAR-2016 13:27:09 through 1-0CT-2016 12:00:00 Lower/Upper Lmts: 5.00000 through 100. 000 .,-j I 0 z 0 H :J ...J 0 01 w O:'. :::..!: a: w CL. 100 80 .......... : .......... * ..... ' ..... * .......... : .................................. . 60 ' . . . . . . I I o o o o o o o o o I o o o I I o 0 o 0 I 0 o o o o o e 0 0 o o o 0 o I o 0 I I 0 I o o o o I I o o o o ' o I o I I o o o 0 I I I o I I 0 0 0 0 ' 0 I . . . . . . :x x x x .x *X x . . . 40 o o o o o I o o o o o o o ' o I I o o o o o I o o o I o e o o I I o o o I I o o o o o o o o o o o o o o o I o o o o o o o I I o o o o o o o o o o 0 I I . . . . . . 20 .......... ' .......... *' ......... '*' ......... ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W084.QAF;9 ParaMeter NaMe PSENERGY-GD148 (PEAK_ ENERGY GD-148) Start/End Dates 4-MAR-2016 13:27:09 through 1-0CT-2016 12:00:00 Lower/Upper LMts: 3143.00 through_ 3223.00 UP 3220 3200 . . . . . . o o o e o ' 0 o o o 0 ' o o o ' ' o o o o ' 0 0 0 0 ' 0 0 0 0 I I 0 o o I I o o o o ' o o o o I I o o o I 0 0 0 0 0 0 0 o 0 I I o o o o o o o o o o I 0 . . co -.;t -M I D )-et:: :x :x :x x x x LLJ 3180 z . . . . . I o o o o I o o o o I o o o o I I o o o o I I o o 0 I I 0 O O I I O o O I o o o o o I o o o o o o o o O o I o O O 1 O o O O I o o o o o 1 o o o o 1 1 o . . . . . . LLJ :..: 0: LLJ a.. 3160 3-16 _4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
-N -...] Vl 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B084.QAF;3 ParaMeter NaMe (Background Rate) Start/End Dates 4-MAR-2016 16:21:44 through 1-0CT-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 '01 ............................................................................ . . . . . . O X X X X X X X X X X X X : X X X X X X X X X* X X X X *X X X X:< 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOliJ ...... N -..l °' 0 ......, Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA,W]W085.QAF;10 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:09 through 4-SEP-2016 12:00:00 0.319702 through 0. 339500 . 335 ............ * ............ * ... ' ......... * ............ * .... ' ....... * ............. * .. ::>, (..) c I]) *r-1 (..) *r-1 4-" 4-UJ . . . . . . . 33 * * * * * * * * * * * *.* * * * * * * * * * * * .* * * * * * * * * * * * *. * * * * * * * * * * * )( * * * * * * * * * *
x* * * * * * * * * * * ***x

x * *x * *

x x x .325 . . . . UP , ........ ........ ........ ........ ........ ........ LOW Measurerrient Date/Tirrie QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W085.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13: 27:09 through 4-SEP-2016 12: 00: 00 184.000 through 204.000 200 ........... *.* .......... *.* ........... * ............ * .......................... *.* . I Cl (!) )-f-H > x H f-u <J: x :x *x w Cl H _J u ::i x z 190 ' I 0 0 o ' I o o o I o0o o o I I o o o o I 0 o 0o o o I o o o I o o o o 11 I o o o o I O o o o I 1' o O " o I o O O 1 I o o 1o I ,1 o o o o 1 o o e o 1'0 o UP 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurer.-.ent Date/Tir.-.e
-N -..l 00 0 ......, Vl 00 0 l.Q QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA,W]W085.QAF;10 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13: 27:09 through 4-5EP-2016 12:00: 00 5. 00000 through 100.000 . . . . . . 80 ...................... ' .................................................... . ""'"" I Cl z 0 H f-* ::l ...J 0 en L1J O:'. :::..::: a: L1J CL . . . . . . 60 o ' o o o I I 0 o o I I 0 0 0 0 I o o 0 o
o o o o o o o o o o o o o o I I 0 o o o o o o o o o o o o o o I 0 o o o I o o o o o o o o o o o o o o I I 0 . . . . . . x *X .x .x x . . . . . . 40 o o o o o o o o o o o I o o o 0 I 0 o o o 0 o o o o o o o o o o o o o o I 0 0 o o o o o o o o o o o o o o o o 0 0 o I o o o o o o o o o o o o o o o o I . . . . . . 20 ...................................... " ........... '* ............ ' ........... '*' . UP 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurer.-.ent Date/Tir.-.e QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA,W]W085.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13: 27:09 through 4-SEP-2016 12: 00: 00 3143.00 through 3223.00 . . . . . . 3200 o I o o I o I o o o I o o o o o o o o I o o o o o o o I 0 o o I o o o o o o o o I I I o 0 o o o o o o o o 0 o 0 o

o o o o I I o o o o I 0 o o o 0 I o . . . . . . ro tj-..-I I D (!) )-x x (!) O:'. x :x :x . . . ' . . w 3180 ................ ' ............................... ' .......................... . z 0 o o I 0 o w :::..c* a: w CL 3160 UP 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurement Date/Tir.-.e
..... N 00 0 0 ....., Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B085.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:44 through 4-SEP-2016 12:00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 UP . 01 ............................................................................. . . . . . . x x x x x x x. x x x x : x x x x x x x x: x x x x *x 0 3 -16 4-16 5-16 6-16 7-16-8-16 9-16 x x LOW MeasureMent Date/TiMe -N 00 -0 ....., Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/ End Da*tes Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W086.QAF;9 AYRGEFF (Average Efficiency) 4-MAR-2016 13:27:09 through 4-SEP-2016 12:00: 00 0.300722 through 0.319324 . . . . . . . 315 ............................................................................ (j c I]) *r-1 (j *r-1 4-4-UJ I]) -0.0 i(j l-1]) > (( . . . . . . **X :x . 31 o ' 0 ' o o o o o o o o
o o o 0 o o o o ' 0 I o ,' o o o o o o o o o o o ', o o o o o o o o o o o o' ' o o 0 o o o o I 0 ' ' .. o o 0 o o 0 I o o o o o' o o x x x . 305 3-16 4-16 5-16 x x 6-16 7-16 Measurerrient Date/Tirrie 8-16 9-16 UP LOW
,_. N 00 N 0 >-+) Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper DKA100: [ENV_ALPHA.QA.W]W086.QAF;9 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27:09 through 4-SEP-2016 12:00:00 184.000 through 204. 000 200 o ' ' ' ' ' I o o o I I o o e 0 0 o o o 0 o o o o o I o o o o o o o o o 0 I o 0 0 0 0 o o o o o o o o o o o o o o o I 0 0 o I I o o o o o o o o o o I o . . . . . . I 0 (!)* >-I-H > H x I-u a: w x 0 H __. u :J x :x :x z 190 ............ * ............ * ............ ,* ............ * ............ * ............ ,*, . UP 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurer.-.ent Date/Tir.-.e -N 00 {.,.) 0 ......, Vi 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W086.QAF;9 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:09 through 4-SEP-2016 12: 00: 00 5.00000 through 100.000 80 ............ * ............ * ............. * ............ * ............ * ....... ' ..... * .. '<'i I D z 0 H 1-=:J _J 0 (f) w O:'. ::...::: a: w 0... . . . . . . 60 ............................................................................ . . . . . . *x x x x :x x 40 ............................................................................ . . . . . . 20 ................................................................. ' .............. . UP 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.W]W086.QAF;9 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-MAR-2016 13:27:09 through 4-SEP-2016 12:00: 00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . . . ' ......................................................................... . co """" ..-I I 0 )-et:: x :x :x x x LLJ 3180 z . . . . . . ............................................................................. . . . . . . LLJ :::..::: a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe filenaMe DKA100: [ENV_ALPHA.QA.B]B086.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:21:44 through 4-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2. OOOOOOE-02 UP . 01 ............................................................................ . . . . . . x x x x x. x x x x x x x x x x x : x x x x x: x x x x :x 0 3 -16 9-16 LOW 4-16 6-16 6-16 7-16 8-16 MeasureMent Date/TiMe ....... N 00 0\ 0 ....., v. 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: '32 DKA100: [ENV_ALPHA.QA.W]W088.QAF;11 AVRGEFF (Average Efficiency) 4-MAR-2016 13:27:09 through 1-0CT-2016 12: 00: 00 0.301414 through 0. 320060 . . . . . . .315 ............................................................................ . . . . . . u c Q) *r-1 u :x x *r-1 4-4-UJ x *X Q) '31 "0.0 .......... , ......... *:*x* ....... *.* ......... * ........... * ........... * ........... . '° l-Q) > a: x '305 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Oate/Tir.-.e UP LOW -N 00 -..J 0 ......., Vl 00 0 \0 QA filenafYle ParaTY1eter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA.QA.W]W088.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAR-2016 13:27: 09 through 1-0CT-2016 12:00:00 184.000 through 204.000 200 .......... : .......... " ......... *.* ......... * ........... * ........... * ........... . I 0 )-I-H > H I-u :x x a: w x *X x 0 H __J u ::i z x *x 190 .......... : ......... *:* ......... *:* ... * ...... *: .......... ......... *: .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW ...... N 00 00 0 ......, VI 00 0 \0 QA f i lenafYle
ParafYleter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W088.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAR-2016 13:27:09 through 1-0CT-2016 12100:00 5. 00000 through 100.000 . . . . . . 80 ......................................................... ' ................. . ...i I Cl z* 0 H 1-::i ....I 0 (.f) w Ct'. ;:,..: a: w 0.. 60 40 . . . . . . ............................................................................ x I I o o o I *x x *X x x x *x x I I o o o I o o o o o I o o o ' I o o o o o I o o o o o o o o I I o o o o o o o o o ' o o o o o I o o o o o o o 0 o I o o o I 0 o o 'o I 0 o o 0 I 0 o . . . . -. ' 20 ............................................ ' .......... ' .......... ' .......... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... N 00 \0 0 ....., Vl 00 0 \0 QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W088.QAF;11 P5ENERGY-GD148 (PEAK ENERGY GD-148) 4-MAR-2016 13: 27:09 through 1-0CT-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ' I o o o o o o o o o o o o o o I o o o o o o o o o o o o o o 0 0 0 0 o o o 0 o 0 o o o o e o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 I 0 . . co ""'" -rl I D )-Cl:'. x x :x .x x .x w 3180 z . . . . . . ............................................................................ . . . . . . w ::.::: q: w CL. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW -N \0 0 0 ......, Vt 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B088.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16: 21:44 through 1-0CT-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 2.000000E-02 . . . . . 01 ............................................................................ . . . . . . x x x x x x x x x: x x x x : x x x x x x x x x: x x x x :x x x >>< 0 3-16" 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafY'le Pararrreter NafY'le Start/End Dates Lqwer/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W089.QAF;10 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54: 00 through 7-SEP-2016 12:00:00 0.281646 through 0.311292 . . . . . ' '31 I I 0 o 0 0 0 o o o I I o o o o o o o o o I I 0 0 o 0 o o o o o o o o o 0 o o o o o o o o o o o I o o o o I o o o 0 I o o o I I o o o o I o o o o I o o . . . . . . . :>, (J c .3 Q)" . . . . . . I o o o o o o o o 0 0 I I 0 o 0 o o o o o I I o o o I I o 0 o 0 I 0 o o I I o o 0 o I 0 0 I o I o o o o o 0 o o o o o o o o I I o o o 0 0 0 o o o o I I . . *r-1 (J *r-1 4-4-UJ x x ID "O,I) x x l1j I-ID > x x x a: . 29 ........... ,* ............ * ............ * ............ * ............ : ............ * .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA.QA.W]W089.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 184.000 through 204.000 200 .......................................................... ' ................ . . . . . . . I 0 (!) )-f-H > H f-u cr: w 0 H --' x u ::i z x : x . . . . x . . x 190 ..................................... *x* ................................... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenaMe Parameter Name Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W089.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:00 through 7-SEP-2016 12: 00:00 5. 00000 through 100.000 ..-1 I 0 (!) z D H 1-::l ....! D ti) w O:'. CI w 0... 100 80 . . . . . . ............................................................................ x x x x 60 ............ *:* .x ....... * *:* * * * * * * * * * * *:* *X * * * * * * * * *:* **x* * * * * * ... : ........... *: .. . . . . . 40 ............................................................................ . . . . . . 20 ........... '* ........... '* ............ *' ........... *' ........................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W089.QAF;10 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . 0 I o o o o I o o o o I o o o I I o o o o o o o I o o o o 0 0 o o e o o I o I o ' 0 I o o o o I I I o o o o ' o I I I o o o 0 I 0 o o o o o I o o I o o . . . . co """ "'""' I D (!) )-(!) 0::: x x x x x x x w 3180 z . . . . . ........... * ............ * .............. * ............ * .. -......... : ........... * ... . w ::..::: a: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Oate/TiMe ........ N \0 Vi 0 ......, Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA,B]B089.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12: 51:34 through 7-SEP-2016 12: 00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' ' ' ' ' ' ' ', * ' ' ' ' ' ' ' ' ' ' ',' ' ' ' ' ' ' ' ' ' ' ',' 1 o o o ' ' o ' ' o ',' ' ' ' ' o o o o o 1 ' : ' ' ' ' ' ' ' ',' ' ' . . . . . . '06 I o o 0 o I o 0 o 0 0 I
o 0 I 0 o 0 0 0 I I o o 0 0 o o o o o o o

o o o o o o o o o 0 0 o 0 o o o o o o o o o o o o o o I I 0 o 0 0 I o o o o o o ' . . '04 . . . . '02 ........... " ........... * ............. " ............ * ........... : ........... " .. . 0 x 3-16 x x x x x 4-16 x x 5-16 x x x *x x 6-16 x x x x 7-16 MeasureMent Date/TiMe x x* x x 8-16 x x *x 9-16 UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W090.QAF;9 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 0.320935 through 0.354717 . . . . . . . 35 I 0 o o o I o o o o o 0 o o o o I o o o o o o o o o o o o o o

o o o o I I O o o o I o o o I I O o o o I I o I o O I o o o I 0 o o o e o o o o o I I o . . . . . ' >i u c Q) *r-1 u . 34 *r-1 ........... ,* ............ * ............ * ............ * ............ : ........... *' .. . 4-4-LU x Q) -0.0 I'll I-. Q) x x x > a: x .33 x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-N l.O -.l 0 ......, Vi 00 0 l.O QA filenafY'le ParafY'leter Naffle Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W090.QAF;9 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54: 00 through 7-SEP-2016 12:00:00 184.000 through 204. 000 200 ........... * ............ * .............. * ............ * ........... : ........... * ... . I Cl )-I-H > H I-u a: w Cl H x _J u x x x x ::i z 190 ............ * ............ * ............ * ............ * ............ , ............ *. *x* x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW -N ID 00 0 ....., Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W090.QAF;9 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End oa*tes 7-MAR-2016 09: 54: 00 through 7-SEP-2016 12: 00: 00 Lower/Upper LMts: 5.00000 through 100.000 ....... I. Cl Cl 2 0 H ::i __J 0 en w O:'. ::..::: a: w 0.. 100 80 ............ * ............ * ............ * ............ * ............ : ............ * .. . . . . . . . 60 o o o o o o o o o o o I o O o O o o o o o o o o o o o 0 o O O I O o o o o o o o o o I 0 o o 0 o o o o o o o o o 0 0 0 0 o 0 o o o o o o o o o o o I I o . . . . . . x x x x x x x 40 o o* o o o o o o o o o o o o o 0 0 0 0 0 o o o o o o o o o o o o o o o o o I o 0 0 o I o o o o o o o o o o o o o o I I o o o o o o o o o o o o o o I 0 0 . . . . . . 20 ........... '* ........... '* ......................... *' ........... ' ............... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -N \0 \0 0 ....., Vt 00 0 \0 QA filenarl"Je Pararl"Je ter Narl"Je Start/End Dates Lower/Upper LP"lts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 o o o o o o o o o o O O o o o o o o o o o o o o o o o o o o o o I o o o o o o o o o I o O o o o o o o o I O I o o I I o o o I I IO O o o I o o o I I o . . co "<:!" ...... I D )-(!) Ct: x x x x x x x LLJ 3180 z . . . . . o o o o I I I I o I I o o o 0 I I o 0 o I 0 I I 0 o I o o o o I o o o o I I o I 0 I 0 o I o o o I o o o I I o I I I o o o I I o o o o o I o o 0
I o o . . . . . . LLJ <C w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerl"Jent Date/TiP"le UP LOW
...... w 0 0 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B090.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:34 through 7-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 .08 ............................................... ' ........................... . . . . . . . . 06 . . . . . . ............................................................................ . . .04 . . . . 02 .............................................................................. . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 '"-+-> VI 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W091.QAF;9 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:00 through 7-SEP-2016 12: 00:00 0.332363 through 0.352921 . . . . 35 o o o 0 o 0 o o o 0 I 0 0 0 0 0 o' o o o o o o o o o o o o 0 0 0 I 0 0 0 0 o o o o o o o o 0 0 o o o o o o o o o o o I o o o o o o o o o o o o 0 o I 0 o ), u c JI) *r-1 u *r-1. 4--UJ . . . . . . x x x x . , . . . . . '34 ..................... ' ' .................................................. ' .. . . ' . . . x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW -\.>.) 0 N 0 ......, Va 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA,W]W091.QAF;9
NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54: 00 through 7-5EP-2016 12:00:00 184.000 through 204. 000 200 ........... * ............ * .............. * ............ * ........... : ........... * ... . I Cl )-1--H > H 1--* u cr: LLJ Cl H x ...J u ::i x x x x x z 190 ........... *:* .......... *:* .......... *:* .......... *:* ........... : ........... *:* *x* 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
........ VJ 0 VJ 0 ....., Ul 00 0 \0 QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09: 54:00 through 7-SEP-2016 12: 00:00 5,00000 through 100.000 80 ' 0 'o o 0 0 o o o 0 ,' o o o o 0 o o o 0 o I o' o o 0 o o o o
0 0 0 o '1 0 o o o o o o o o o o *, o o 0 o I o 0 0 I I o : o o o o o o o o o o o o' o o o -M I D (!) z 0 H 1-::i _J 0 (f) w O::'. :..::: a: w 0... . . . . . . 60 O O O o O I o O o o o O o o O o I o o o o o o o o o o o o o O I o o O O I o O o o O I o o o o o o o o o o .o o 0 0 I 0 0 o o o o o I o o o o o o o o o o . . . . . . x x x x x x x . . . . . 40 ............................................................................. . . . . . . 20 ........... '* ........... '* ............ *' ........... *' ........................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenarrre DKA100: [ENV_ALPHA.QA.W]W091.QAF;9 Pararrreter Narrre PSENERGY-G0148 (PEAK ENERGY GD-148) Start/End Dates 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 Lower/Upper Lrrrts: 3143.00 through 3223 .. 00 UP 3220 3200 . . . . . ' *********************************.************** ' ************************* l ** . . . . . . co ...;t '<""I I D )-0:: x x x x x x x LLJ 3180 z . . . . . ' . 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 0 o o o o o o 0 I o o o 0 0 o 0 o o o I o 0 o 0 0 0 o o 0 o 0 0 0 I 0 o 0 o 0 0 0 o o o I I 0 o o I o o I LLJ ::...:: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurerrrent Date/Tirrre QA filenaMe DKA100: [ENV_ALPHA.QA.B]B091.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:34 through 7-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I o.s I I I I 1 I 1 1 1 1 1 'o 1 1 1 1 1 1 1 1 1 o I 11 1 1 1 o 1 1 1 1 1 1 1 1 01 1 1 I I O I I I 1 I I 01 1 1 1 1 1 1 1 1 1 1 1 : 1 1 1 1 1 1 1 1 I 1 I', I 1 I . . . . . . . 06 ............................................................................ . . . 04 . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 5.,....16 7-16. 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter Narrie Start/End Dates Ldwer/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W092.QAF;10 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 O. 291600 through 0.309620 .305 o o e o o o O o o o I 10 I O O I I O O o O I I o0 O O o I o o O I I o o O 0o o o o o o

o o o o I 0o o o o o o o o o o o o : o o o o o o o 0 o o o o0 I o 0 x u c I]) x *r-1 u *r-1 4-x 4-UJ x . . . . . . rJ) .3 o I o o o I 0 o o o o I o o o I o o o o o o o o o o o o o o o I I o o o o o o o o o o o o o o o o o o o I o o o o I I o o o I ' o o o o o o o o o I I o . . . . . . "Of! 1(1 I-I]) > <J:. x x x '295 o I 0 o o o o o o o I ,* o o o I I o o o o I I ,' o o I I 0 o ' I I 0 o o '1 I I o 0 o I o o o o o ', o o o I I o o o I I o: o o o o o o o I o o o o' I o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TiMe UP LOW QA filenafY'le ParafY'leter NaMe Start/End Dates Lower/Upper DKA100: [ENV_ALPHA.QA.W]W092.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54: 00 through 7-SEP-2016 12:00: 00 184. 000 through 204. 000 200 I 0 I I o ' o 0 I I I I I I I I I I I I I o o I I I o o o o I o I I I I I I o I o I I I I I I I I ' o I 0 I o o o 0 I I I 0 o o o o o o o o o o o o o o . . . . . . I Cl >-I-H > H I-u a: w x Cl H _J u x x x ::i z x x 190 ........... *:* .......... *:* .......... *:* *x* ....... *:* ........... : ........... *:* .. 3-16 4-16 5-16 6-16 7-16 8-16 . 9-16 MeasureMent Date/TiMe UP LOW QA filena!"le Paral"le ter Na!"le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W092.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:00 through 7-SEP-2016 12:00:00 5.00000 through 100.000 80 ' ' 0 o 0 I 0 0 0 o 0 o' o o o o o o 0 o 0 0 0 o' o o o o o o o o 0 0 0 0 '1 0 o o o o o o o 0 o 0 'o o o o o I o o o I I 0 : o I I o o o o I o 0 o o' I 0 o ...... I D C!l. z 0 H 1-::i --' 0 en L1J O:'. a: L1J 0.. . . . . . . 60 ........... *.* .......... *.* .......... *.* .......... *.* ........... : ........... *.* x x x x x x x . . . . . . 40 I I o o o o o o o o 0 0 O o O I O O O O o I I o o o I I o O O I O O o O I o o o o o I o o 0 O I O O O o o I o o o I 0 0 0 0 I I o o o o I o o o o 0 I 0 . . ' . . . 20 ........... '* ........... '* ...................................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!"lent Date/Ti!"le UP LOW
-w 0 \0 0 ......, Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W092.QAF;10 Parameter Name P5ENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 7-MAR-2016 09:54: 00 through 7-SEP-2016 12:00:00 Lower/Upper Lmts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . ............................................................................ . . ro """ rl I D )-0: x x x x x x x w 3180 :z . . . . . . ............................................................................. I 0 o o o o w :::..:: a: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurement Date/Time ..... VJ ..... 0 0 ......, Vi 00 0 \0 QA filenaMe -DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:34 through 7-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' o o o o o ' ' ' ' o ', O o ' o I o O ' o I I 00 0 0 I I 0 ' 0 I I o o 0 00 I" o o o o o o o o o I 00 0 o 0 I I 0 O O I I O : O o o o o o o 1 o o o o0 1 o o . . . . . . O 1 o o o O o o o o 1 1 o o o I I o O o o O I O o O O I O o O O I O o o o I o o o o o o o o o I o o o o I 0 o 0 0 I 0 0 0 o I I o o o o I o o o o o I o . . . 04 . . . . . 02 ........... * ............ * .............. * ............ * ........... : ........... * ... . 0 . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -w --QA filenal'le Pararrle ter Narrle Start/End Dates Lower/Upper Ll'lts: DKA100: [ENV_ALPHA.QA.W]W093.QAF;10 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:00 through 7-SEP-2016 12: 00:00 0.292468 through 0.375000 I 36 o O o o 0 o I o o o o ', o o o o 1 o o o o o o 'o o o 1 1 o o o O o 0 o o o' o o o e 1 I o o o o 1 o' o '-0 O I o o o o o o : o o o o o o o o o o o ',' 0 o (.) . . . . c I]) *r-1 (.) *r-1 . 34 ' o o o o ' ' o o o o I 0 o o I o o o o o o o o 0 0 o o 0 o o o o o o o I I 0 o o o o o ' o 0 I 0 o o o ' I 0 o o 0 I o o o 0 I 0 0 o o I o o o o I o o 4-4-LU . . . . . . x x x x x x x I e I o o o .32 ............................................................................. I 0 I 0 o o .3 . . . . . . .................................................. *-........................ . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrlent Date/Til'le UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W093.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:00 through 7-5EP-2016 12:00:00 184. 000 through 204. 000 200 o o e o o I o 0 o o I o o I 0 0 I 0 0 o o I o o o I o I o o o I I o 0 o 0 I o o o o o o o o o o I I o o I ' o o o I I o I o I I o o o o I I I o I I o I . . . . . . I 0 >-I-H > H I-u a: w* 0 H x x ...J u ::i x x : . x x z x 190 ............ * ............ * ............ * ............ *, ........... : ............ *' .. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA f i lenaMe
ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 x DKA100: [ENV_ALPHA.QA.W]W093.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:00 through 7-SEP-2016 12100:00 5.00000 through 100.000 x x 80 ............ * ............ * ............ * ............ * ............ : ............ * .. x. ..-I I Cl z D H =i ....I D U') w O:'. x x x 60 . . . . . , . o I o O o o o o o o o O o o o o I o o o o o O o o o o O o I I O O o O O I I O o o O I o o o o o o o o o I I o 0 0 I 0 o 0 o ' o o o o o

o o o o o o o . . . . . . . . . . 40 .................................................. *-........................ . . . . . . . 20 ................................................................................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... w ....... .J::>. 0 ......, Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W093.QAF;10 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 7-MAR-2016 09:64:00 through 7-5EP-2016 12:00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 I I 0 I I I ............................................................................ . . ro ¢ """""" I D (!) )-(!) 0::: x x x x x x x w 3180 z . . . . ......................................................................... ' .. . . . . . . w ::...::: <C w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ....... w ....... Vl 0 H, Vl 00 0 \0 QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:34 through 7-SEP-2016 12:00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' ' ' * ' ' ' ',' ' ' ' o ' ' ' * ' ' ',' * ' ' ' o ' ' ' o o ',' ' ' o o o o o o o o ',' o o o ' 1 o o o 1 1 o : o ' ' o 'o ' ' o o o 0 ' ' . . . . . . . 06 0 0 o o o o 0 o o o I o o o o ' o o o o o o o o o o o o e o o o o o o o o I 0 0 0 0 o o 0 o o o o o o e o o o 0 0 0 o o 0 o o 0 o o o o o o o o o o o o . . . 04 . . . '02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -VJ -O'I 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W095.QAF;11 AVRGEFF (Average Efficiency) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00:00 0.295600 through 0.313900 . . . . .31 o o o o o o o o o o o o o o o o o o o o 0 o I o o o I o o o 0 0 I 0 o 0 I o o o o o I o o o o I o o o o 0 o o 0 0 o o o o o 0 I o o o 0 0 o o o o o I o :>, 0 c ID *n 0 *n 4-4-LU . . . . x x x . 3 0 5 .................... :x:* ...................................................... . . . . . x x x x x . . . . .3 ............................................................................ . . . . p-16 6-16 7-16 8-16 9-16 MeasureMent* Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W095.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00:00 184.000 through 204.000 200 o I o I o o ' o o I I o I o o o I o 0 o o 0 I o o o o o o o I o I o o o o I o o o o I e o o o o I o I o I o o o o o I o o o I I o o o o I o o o o I ' o I Cl )-1-. H > H I-u a: w Cl H ....I u ::i z x x . . . . x . x . x . . x 190 .... :x ............ : ................. * .................. * .................. : ... . x x 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00: 00 5.00000 through 100.000 . . . . 80 ' ' e o ' ' ' ' o ' ' ' ' o ' o o o o o o ' ' o o o ' ' o o ' ' ' o o o ' ' o o o o ' o o o o ' ' o o o 0 ' o o o ' ' o o o o o o o o ' 0 o 0 o o I o 0 ........ I Cl z 0 H* 1-=i ....I 0 ({) w O:'. ::..::: a: w 0... 60 40 x x . . . . o o o o o o o o o o o o 0 o o I o 0 o o 0 I 0 o 0 0 o 0 o o 0 0 0 0 o o 0 o o o o 0 I 0 0 o o I 0 o o o 0 0 o o o o o o o o o I o o o o o o o o o o o o x x x . . . . x x x x .................................... ' ............... ' ...................... . . . . . 20 ................. ' .................................... ' ................. ' ... . 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -l;.) -\0 0 >-+, Ul 00 0 \0 QA filenal"'le Para!"'le ter Na!"'le Start/End Dates Lower/Upper Ll"'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W095.QAF;11 P5ENERGY-GD148 (PEAK ENERGY GD-148) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . 3200 ............................................................................ CD v """" I D (!) )-(!) et:: LLJ z LLJ ::...: <r: LLJ a.. x xx* x x . . . x x 3180 ............................................................................ . . . . 3160 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til"'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.8]8095.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAY-2016 15:23:40 through 7-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' 0 ' 1 ' 0 ' 1 ' ' ' 1 1 0 ', 0 1 0 0 ' 0 0 0 0 1 0 o 0 1 1
0 00 1 1 ' 0 o o 1 0 o 0 o 0 0 0 0 0 0 .' 0 0 0 0 ' 0 0 0 0 0 0 0 0 0 0 0 0 ', 0 0 ' 0 . . . . .06 ............... ' .......... ' ................................................ . . . .04 .oz ............................................................................ 0 5-16 . . . . 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
,_. !,;.) N ,_. 0 ....... I.Ji 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W096.QAF;10 AVRGEFF (Average Efficiency) 4-MAY-2016 14:17:17 through 7-SEP-2016 12: 00: 00 0.314971 through 0.334453 . 33 o o o e o o o o o O o O o o o o o .. o o o o o o o o o I o o o I o o o 'o o o o o o o o o o o o 1 1 o o o I 01 o o o I I o o o o I o o o o o o o .. o I o o 0 c Q) *r-1 0 *r-1 4-4-LU . 325 . 32 x x x x x x . X . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . :. . . . . . . . . . . . . . . . . . : . . . . . . . . . . . . . . . . . . . X . . . . . . . . . ............................................................................ . . . . . 315 -..... .......... ......... ..................... ........ ..................... ......... ........................................ ............................ ......... ............................ ..................... 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W096.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAY-2016 14:17:17 through 7-5EP-2016 12:00:00 184.000 through 204.000 200 ................. * ................... * ................. : ................. * .... . I Cl )-I-H > H I-u .;,I w Cl H ...J. u =r x x x x x z 190 O o o o o o o o o o o o O o o O O .. o O o o o o o o o o o O O I O o o 0o o o o o *o o I 0 o o o o o o o o o 00 o o 0 I I o o o I I o o 0 0 I 0 o .. o : I o 5-16 6-16 7-16 *8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie 5tart/End Dales Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W096.QAF;10 P5FWHM-GD148 (PEAK GD-148) 4-MAY-2016 14:17:17 through 7-5EP-2016 12:00:00 5. 00000 through 100.000 80 .................................... * .................. * ....................... . ....... I 0 (:) z 0 H 1-::1 --' 0 (f) w O:'. ::,,.::: a: w (L. . . . . 60 ............................................................................ . . . . x x x x . . . . 40 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 0 o o 0 0 o o o o o o o o o o o o 0 o o I o o o o o o o o o o o o o o o o o o o o o o o . . . . 20 ................. ' .................................... , ................. ' ... . 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie .UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W096.QAF;10 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Dates 4-MAY-201614:17:17 through 7-SEP-2016 12: 00: 00 Lower/Upper lMts: 3143.00 through 3223.00 UP 3220 3200 . . . . .......................................... ' ................................ . co ¢ ..-l I D (!) )-(!) et:: x x x x LL.I 3180 :z . . . . o 0 0 0 o I o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o *' o o o I o o o o o o o o ' o 0 0 o o I o o o o o o 0 0 o I o ' . . . . LL.I a: LL.I CL 3160 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAY-2016 15:23:40 through 7-SEP-2016 12:00:00 Lower/Upper LMts: O. OOOOOOE+OO through 0.100000 I 08 ' I ' ' O I 1 o o 1 1 1 o o o 1 o 10 o O o I I O I o o 1 o o o 1 1 o o ,' ' o o o o 1 o o 1 o o 1 I o O 1 o 01 I O O O I o o o O O o o 1 o 1 o o ', o 1 1 o . . . . .06 I I o 0 I I o o o o I I o o 0 I I 0 0 o 0 0 I I o o I o o I o o I o o o I o o I o o I o o o o I I o o o I o o o o I I 0 o 0 I I o o I I I 0 o 0 I I I 0 .04 . . . 02 ................. * ..................................... : ................. * .... . 0 5-16 6-16 7-16 MeasureMent Date/TiMe 8-16 9-16 UP LOW -VJ N °' 0 ......, Ul 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W097.QAF;10 AYRGEFF (Average Efficiency) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00:00 0.348290 through 0.369834 . . . . >.. u c ID *r-i u *r-i 4-4-UJ . 36 ................................................... -........................ . . . . . x x x x x x x x x . 35 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ...... VJ N -..} 0 ....., Vt 00 0 \0 QA filenafY'le Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W097.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAY-2016 14:17:17 through 7-5EP-2016 12:00:00 184.000 through 204.000 200 I I o o o o I o o o o I o o o o I 0 o 0 o I I o 0 o o o 0 o o I I o o o o o o o o o o o o o o o o o o o I 0 o 0 0 I I 0 0 o I I 0 o o 0 I o o 0 o I o o I Cl )-I-H > H 1-* u a: LLJ Cl H ....I u ::i z x x
x . . . . x x x x 190 .................................... *. ' ..... ' .......... * ....................... . 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-(.;.) N 00 0 H-i VI 00 0 \0 QA filenarrie Parafl'le ter Nafl'le Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W097.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00: 00 5.00000 through 100.000 80 o o o o o o o e o o o o o o o o O .. o o O O I o O o O O o o o o o o o 'o o o o o o o o o o o o o o o o o o 'o o o 0 o I o o 0 o I o o o o I o o .. o I o o I D C) z 0 H 1-::i ....I 0 r.n w Ct'. ::..:C a: w 0... . . . . 60 I I 0 o o I I 0 o o o I 0 o e o I o 0 o o o I o 0 0 o I o 0 0 0 o 0 0 0 I I 0 0 o o I o o o o I o o o o o I o o o I I o o o I o o o ' o 0 o o o o 0 I 0 . . . . x x x x x x 40 ............................................................................ . . . . 20 ................. ' .................................... ' ................. ' ... . 5-16 6-16 7-16 8-16 9-16 Measurefl'lent Date/Tifl'le UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W097.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 4-MAY-20i6 14:17:17 through 7-SEP-2016 12:00: 00 3143.00 through 3223.00 . . . . . 3200 o ' o ' 0 I I o o o I o o o o I I o o 0 o 0 I o o 0 o o o o o I o o o o o o o o o o o e o o o I I o o o o o o o o O I O o o I I e O o o I O O O O I I O . . . . co v ""'"" I D (!) )-(!) ct:: x x x x LU 3180 z I o o 0 I 0 0 0 o 0 o 0 o
I I 0 o o 0 I 0 0 0 0 I 0 o o 0 I I o o o o o o o o I I o o o O I o o o o I I o o o O o o o o I O O o O 'I O O O o O I o O O o I o O . . . . LU a: LU 0.. 3160 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B097.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAY-2016 15: 23:40 through 7-SEP-2016 12:00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' ' 0 ' o o o o 0 0 0 0 0 0 00 0 o o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ,' 0 0 o 0 0 0 0 0 0 0 0 o 1 0 0 0 0 .' 0 0 o 1 1 0 0 0 1 1 0 0 0 0 0 0 0 ', 0 0 0 0 .06 . . . . o o o o o I o e o o I o o o o o o o o o o I I o o o o o o o o o I 0 e o I o o o o o o o 0 o o o o o o o o o o 0 o 0 0 o o o o o 0 o 0 0 I o o o o o o o .04 . . . . .02 ............................................................................ . . . . LOW MeasureMent Date/TiMe 0 ......, Vi 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W099.QAF;11 AVRGEFF (Average Efficiency) 4-MAY-2016. 14: 17: 17 through 7-SEP-2016 12: 00: 00 0.310091 through 0.375000 ' . . . . . . . . 36 . .............. : ................. * ................ -.. * .................. : ... . :>, u c ID *r-1 u *r-1 4-4-UJ x x x x x ID , 34 ................. * ........ ' ......... ** ................. ' ................. * .... . "OJ) i(i ID > a:* . 32 5-16 6-16 7-16 8-16 "9-16 Measurerrient Date/Tirrie UP LOW QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LIY'lts: DKA100: [ENV_ALPHA.QA.W]W099.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 4-MAY-2016 14:17:17 through 7-SEP-2016 12: 00:00 184. 000 through 204.000 200 ........... ' ............................................................... . . . . . I 0 (!:I )-I-H > H I-u a: x Ll.J x 0 H _J u x x :J z x 190 ................. *: ................ *:* ................. :*. *x .............. *: ... . 5-16 6-16 7-16 8-16 9-16 Measure!Y'lent Date/Ti!Y'le UP LOW
-VJ VJ VJ 0 ....., Vl 00 0 \0 QA filenarrie Parameter Name Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENY_ALPHA.QA.W]W099.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 4-MAY-2016 14:17:17 through 7-SEP-2016 12:00: 00 5.00000 through 100.000 80 ' 0 o o o o o o o o ' ' o o o o ' .. o o o ' ' o o o ' 0 e 0 0 ' ' 0 0 'o 0 o o o o o o o o o o o o o o o o ', o 0 0 0 I o 0 o o o o o o o o o o .. o o o e """" I Cl z 0 H =i ....J 0 01 w 0::: . . . . 60 ............................................................................ . . . . x x x x 40 ............................................................................ . . . . 20 ................. ' .................................... , ................. ' ... . 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W099.QAF;11 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 4-MAY-2016 14:17:17 through 7-5EP-2016 12:00:00 Lower/Upper LMts: 3143. 00 through 3223. 00 UP 3220 3200 . . . . ............................................................................ . . co "'" "<""I I o* )-i:::t:: x x x x LLJ 3180 z . . . ............................................................................ . . . . LLJ ::..:: ([ LLJ CL 3160 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B099.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Date8 4-MAY-2016 15:23:40 through 7-SEP-2016 12: 00: 00 Lower/Upper LMt8: O.OOOOOOE+OO through 0.100000 UP .08 ' I ' I 0 0 0 o
o o o o o o I I o o o o o o o o o o o 0 o o I 0 o

o o I o o 0 o 0 e 0 0 o 0 0 o 0 o 0 o o o o I I 0 0 o I I 0 o o 0 0 o 0 0 o 0 I o . . . . . . . . I o o o o I I o 0 o I I o 0 0 I 0 o 0 o 0 0 I I o o o o o o o o I o o o I I o o o o I o o 0 0 0 o o 0 o I 0 o o o I o o o o I o o o o o o I o o o o o o .04 . . .02 ............................................................................ . . . . LOW -MeasureMent Date/TiMe
-w w O'I 0 ......., Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W103.QAF;12 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:02 through 7-SEP-2016 12:00:00 0.322108 through 0.342032 >.. 0 c Q) *.-! 0 *.-! 4-4-UJ Q) "0.0 iJj Q) > a: . . . . . . .34 I 0 0 0 0 I I o o o I I o o 0 I 0 I 0 0 0 I o o o o I o o 0 0 I 0 0 o o 0 o o o 0 o 0 0 0 o o o o o o o o 0 o 0 o 0 0 o o o o o 0 0 o o I o o o o o o o . . . . . . : x x x x . . . . . . . 335 ......................................... x ........ '*' ........................... . x x .33 . . . . . . 0 I o o I I I o o o I I o o o I I I 0 I 0 I 0 I o o I o o o o I o o o o I 0 0 I o o o o o o o o o o 0 0 I 0 0 o o I I 0 I o I o Io 0 0 I 0 0 I I I 0 o . . . . . . . 325 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW Qfi filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W103.QAF;12 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54: 02 through 7-SEP-2016 12:00:00 184.000 through 204.000 200 ........... * ............ * .............. * ............ * ........... : ........... * ... . I D (!) )-I-H > x H I-u a: x x x w x D H ...J u ::i x z 190 ............ * ............ * ............ * ............ * ............ : ............ * .. . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW -l;.l l;.l 00 0 ....., Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W103.QAF;12 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:02 through 7-SEP-2016 12:00:00 5,00000 through 100. 000 . . . . . . 80 ............................................................................ ...... I D z 0 H ::. ....! 0 (.!) w O:'.* :...::: a: w 0... . . . . . . 60 o o o o o o I o o 0 0 0 0 0 0 o I o o o 0 o I o o o o o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o . . . . . . x x x x x x x 40 o o o o o I I 0 o 0 I 0 0 0 o I I 0 o o 0 o 0 0 o o I o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o o o o o o o o o o o . . . . . . 20 ................................................... *' ....................... '* .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA f i len_arrie Pararrie ter Na-rrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 7-MAR-2016 09:54l02 through 7-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 I 0 o o o o o o o o 0 I o o o o o o o o o I o o o o I I o o o o o 0 0 0 I I o o o o I o o o o I o 0 o 0 I I o o o o o o o o o o o o o o I o 0 0 0 I I o . . . . . . (D ""'" "<"i I D )-x ct: x x x x x x . . . . . . LL.I 3180 o o o o o ' o o o o ' o o o o o o *, o o o o I o 0 0 o 0 0 O O I*, O O o I o o o o o o o o o O I I O O o I I O o o I o o o o I I O O O o I O o O o I I o z . . . . . ' LL.I ::..: a: LL.I a.. 3160 ................................................................................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,B]B103.QAF;4 ParaMeter NaMe BACKRATE (Background Rate) Start/End Da-tes 4-MAR-2016 12: 51: 39 through 7-SEP-2016 12: 00: 00 Lciwer/Upper LMts: O.OOOOOOE+OO through 0.100000 . 08 ' .......................................................................... . . . . . . . .06 o o o o o o o o o o o ,' o o o ' o o o o o o I ,* o o 0 ' o o o o I o o o ', I o o o o I o o o o o ', o o o o o o o o o o o : o I o o o o 0 0 o o o ,' o o o . . . 04 . . . . . 02 ........... * ............ * .............. * ............ * ........... : ........... * ... . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 ......., Vl 00 0 ID QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: . 335 DKA100: [ENV_ALPHA.QA,W]W104.QAF;10 AVRGEFF (Average Efficiency) 7-MAR-2016 09: 54:02 through 7-SEP-2016 12:00:00 0.317853 through 0.337513 x . . . . . . u c Q) -ri u -ri 4-4-UJ .33 o o o o o o o o o o o o o o o o 0 o ' ' o 0 I o o o o o o o o o o o o o o 0 o o o o o o o o o o I o '* o o o o o o o 0 o o o o o o o o o o o o o o I 0 ' . . . . . x x x x .325 x x . . . . . . . 32 o o 0 0 o I o o I o 0 I o o o o o o o o o o o o o o o o 0 o o I I o o o I I o o 0 o I o o o 0 I I o o o o o o I
o I o o o I I o o o o 0 I 0 o I I I o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW
-w """ N 0 H) Vl 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Date:s Lower/Upper LMt:s: DKA100: [ENV_ALPHA.QA.W]W104.QAF;10 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54: 02 through 7-SEP-2016 12:00: 00 184.000 through 204.000 200 ........... * ............ * .............. * ............ * ........... : ........... * ... . I 0 (!) )-1--H > x H 1--u 0:: x x x x x w 0 x H ....I u =:i z 190 0 0 0 o o o 0 o o o o o' o o o o I o o o 0 0 I o' o 0 0 I o o I o
o o o 'o I I o o I I o o o o o 0o 0 o I I I o o I I I o : o 0 I I 0 o o ' I o I 01 o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Mea:sureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 10_0 .

DKA100: [ENV_ALPHA.QA.W]W104.QAF;10 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:02 through 7-SEP-2016 5.00000 through 100.000 12:00:00 80 0 *

0 0 0 I 0 0 0 0 1' 0 0 o I 0 o 0 o 0 I I o' 0 I I I 0 o o I I o o o 01 o o o o o o 0 0 0 0 I 00 o o o I I o o o 0 I o : 0 0 0 o o o 0 I o o o o' 1 o o ..-1* I Cl (!:I z 0 H" 1-:J ....I 0 en w 0::: a: w 0... . . . . . . 60 1 o o o o 1 1 o o o o 1 o o o o 1 o o o o o o o o o 1 o o o o 1 o ,o o o o 1 I O O O I o o o o o o o o o I o o o o I I o 0 0 I o 0 0 o o I o o o o I I o I o I o o I x x x x x x x . . . . 40 I I o o O I O o o O O o o O o I I O o O o o I o O O O o o o o I I o o o I o o o o o I o o 0 0 I I 0 o o 0 I o o o I I o o o I I o o 0 0 0 0 0 0 o I 0 0 . . . . . . 20 ........... '* ......................... *' ........................ ' ............... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W104.QAF;10 PSENERGY-GD148 (PEAK ENERGY GD-148) 7-MAR-2016 09:54: 02 through 7-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 ............................................................................ co "'" "'""' I D (.') )-(.') 0::: x x x x x x x LU 3180 z o o o o o I I o o o o I o o o o o o o o o I o o o o o I 0 o 0 0 I I o 0 0 I I o I 0 o o o o o o o o o o o o o o o o I I o o o I o o o o I o 0 o 0 o o o 0 o o 0 o o I 0 o o o I LU :..::: a: LU CL 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA. QA. 8]8104. QAF; 3 BACKRATE (Background Rate) 4-MAR-2016 12:51:39 through 7-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 . 08 ' ' ' ' ' a ' o o o o 0 o o o ' ' o o o 0 0 I o 0 o o o e o o I I 0 o o o o o o 0 0 I o o o o o o 0 0 o o o o o o 0 I o o o o o e o o o o o o o o o o o . . . . . . . 06 . . . . . . ................................ ' .......................................... . . 04 ................................................................ -................ . . . . . . . 02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: x DKA100: [ENV_ALPHA.QA.W]W105.QAF;12 AVRGEFF (Average Efficiency) 7-MAR-2016 09: 54:02 through 7-SEP-2016 12:00:00 0. 324335 through 0.344400 x . 34 o 0 0 o o I 0 o o o 0 o o o o o o o o o o 0 o 0 I 0 I o 0 o o o o o o o I o 0 0 o 0 o o o o o o o o o 0 o I 0 o o o I o o o o o o o o o o 0 0 o 0 I I o :::-, 0 c I}) *r-1 0 *r-1 4-4-UJ . . . . . . x x x x x .33 ............ * ............ * ............ * ............ * ............ : ............ * .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA;QA.W]W105.QAF;12 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:02 through 7-SEP-2016 12:00:00 184.000 through 204.000 20*0 . '. ......... * ............ * ............. " ............ * .. " ........ ' ........... * ... . I Cl )-I-H > H x I-u a: x x x x w* Cl x H ..J" x u =i z 190 . . . . . . ' ' o

o ' o o o o o o o o o o 0 o o o 0 o I 0 o 0 I I o o o o o o o o o o o o o o 0 0 0 0 o o o o o o o I o 0 0 I I 0 o o I o o o o o I 0 0 0 0 0 I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
....... VJ 00 0 ......, Vo 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W105.QAF;12 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54: 02 through 7-SEP-2016 12:00:00 5.00000 through 100.000 80 I I O o o I o o o o I o' o o o I I O e O O O I o0 o o o I o o o O O O o o 'o I o o o o o o 0 0 o I 11 o o o o o o o e I I o : 0 o I o o o o I o o o o' I 0 0 ..-! I 0 (!) z 0 H :J ...J 0 en w O'.'. 60 . . . . . . o 0 e o 0 ' I 0 o o I 0 0 0 o o I o o o o o I o o o o 0 o o o I I o o o I I o o o o I 0 o o o I I o o o I 0 o o o 0 I 0 o o I o o o o o I 0 0 0 e I I o . . . . . . x x . x x x x . . . x . . 40 o o o o o I 0 o o 0 0 I O e O O o o o o o I o o o o I o o O O I I O O O o o o o o o 0 0 0 0 e O I O e O I I o o o o I 0 e 0 0 0 o o o o I o o o o I 0 0 ' . . . . . 20 ................................................................................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filename DKA100: [ENV_ALPHA.QA.W]W105.QAF;12 Parameter Name PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 7-MAR-2016 09:54:02 through 7-SEP-2016 12: 00:00 Lower/Upper Lmts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : . . . . . ." . . . . . . . . . oo. v ..-l I D (!:I )-(!:I et:: x x x x x x x LLI 318.0 z . . . . . . o 0 0 o o 0 o o o o o 0 o o o o o o 0 o o I 0 o o o o 0 0 o o o 0 'o o I I o o o o I o o o o I o o o o I 0 o o o o o o o o o o o o o o o o o o o I o o . . . . . . LLI <C LLI CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurement Date/Time QA filenaMe DKA100: [ENV_ALPHA.QA.B]B105.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:39 through 7-SEP-2016 12:00:00 Lower/Upper O.OOOOOOE+OO through 0.100000 UP .08 I 0 0 0 I 0 I 0 I I 0 0 o o o o I o o o o I I o o o I I I O O I I o I I I o o o o o I o o o o I O I I O I I Io o I I O o o o o o o o I o o O I o I I I . . . . . . .06 . . . . . . I I I I I o o I I o I 0 o I I I I I o 0 I I I I 0 I I 0 I o I I I I o o I I I I I I o I I I o 0 I o I I o I o I I I o o I I 0 I o o 0 I I o o o o 0 I I . . . . 04 . . . . . . 02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe 0 ......, Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W106.QAF;11 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:02 through 7-SEP-2016 12:00:00 0.323416 through 0.343420 . 34 ............ * ............ * ............ * ............ * ............ : ............ * .. . >> u c Q) *r-i u *r-i 4-4-UJ . 33 * * * * * * * * * * * ... * * * * * * * * * * "* *x* * * * * * * * * ... * * * * * * * * * * ... * * * * * * * * * * *' * * * * * * * * * * * "* *
x x x x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
-w Vi N 0 ....., Vi 00 0 "° QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W106.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:02 through 7-SEP-2016 12:00:00 184.000 through 204. 000 200 ............................................................................ . . . . . . I Cl (!) )-I-H x > H I-u 0: x x . x x w Cl x x H _J u ::i z 190 o I 0 0 0 I o 0 0 0 o 1' O O o O o o o o o o o o0 o o o o o o o O O o O O 'o I o o o o o o o o o o 0o o o o o I o O o I I o : o o o o o o o o o o o o' I o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: PSFWHM-GD148 (PfAK RESOLUTION GD-148) 7-MAR-2016 09:54:02 through 12:00:00 5. 00000 through 100.000 80 ............ * ............. * ............ * ............ * .... ,, ....... : .... ** ....... * .. . I er z 0 H 1-=i -4. 0 en w Ct'. :::.:: a: w 0.. . . . . . . 60 o o o o o I o o o o o I o o o o o 0 0 0 o o 0 0 0 0 o 0 o 0 0 I I 0 0 o I 0 0 0 o 0 I 0 o o o 0 I o o o I I o o o I I o o o o I o o o o o o o o o I o o . . . . . . x x x x x x x . . 40 I I 0 0 0 I I 0 0 o o o o o o o o o o o o o o o o ,o I o o o o O O o o O o o o o o o o o O o o o o o o o 01 o o o o o o o o o o o o o o o o o o o o o o o . . . . . . 20 ................................................................................ . 3-16 4-*16 5-16 6-16 7-16 8-16 9-16 MeasureMent UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W106.QAF;11 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 7-MAR-2016 09:54: 02 through 7-SEP-2016 12:00:00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . . ............................................................................ . . . . . . co "<;!" ..-I I 0 (!) >-(!) et: x x x x x x x LLJ 3180 Z* . . . . . . ............................................................................ . . . . . . LLJ :;,..:: <r: LLJ a.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B106.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:39 through 7-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' ' o ' ' o o ' ', o o o ' ' o o o o o ' ', o o ' ' o o o ' ' o o o ,' ' '.' o o ' O o o o O ,' O O o ' o o o o ' ' o : e o o o o o o O o o o 'o I I o .06 . . . . . . ............................................................................ . 04 . . . . 02 ............................................................................ . . . . . . 0 3-16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe QA filenarrie DKA100: [ENV_ALPHA.QA.W]W107.QAF;11 Pararrieter Narrie AVRGEFF (Average Efficiency) Start/End Dates 7-MAR-2016 09: 54:03 through 7-SEP-2016 12:00: 00 Lower/Upper Lrrits: 0.306300 through 0.325260 . 325 UP .32 >.. u c Q) *r-1 u *r-1 4-x 4-Ll.J Q) . 315 -0.0 ...................................................... x* ........................ . i{j I-Q) > a: x . . . . . . . 31 .............. *X* ............................................... , ............... . . . x . . . . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurerrient Date/Tirrie -w Vl -:i 0 ......, Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lrrits: DKA100: [ENV_ALPHA.QA.W]W107.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12: 00: 00 184.000 through 204.000 200 ........... * ............ * .............. * ............ * ........... : ........... * ... . I Cl (!) )-I-H > H I-u a: w Cl H x x x x x _J u ::i x x z. 190 . . . . . . I I 0 0 o I o o 0 o I I o o o I I o o o o I I o o o o I o o O I I o o o o I o o o o o o
o o I I o o o I I o o o I I o o o I o o o o I I 0 o o o I o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W107.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09: 54:03 through 7-SEP-2016 12: 00:00 5.00000 through 100.000 80 ........... ,* ............ * ............ * ............ * ............ : ............ * .. . ....... I Cl (!) z 0 H =i ...J 0 r.f) lJ.J 0::: ;:,,.! a: lJ.J 0.. . . . . . . 60 o ' o o o o o o o o o o o o o 0 I o 0 0 o ' o o o o o o o o o o o 0 0 0 0 o o o o o o o o o o o o o o 0 I 0 o o o o o o o o I o o 0 o o I o o o o o o o . . . . . . x x x x x x x 40 I I 0 0 0 I I o 0 0 0 I o o o o o o o o o o o o o 0 o 0 o O O I I O o o o o o o o o o o o 0 0 I I O O o I o o o o o o o o o I I O o o o I o o o o o o o . . . . . . 20 ................................................................................ . 16. 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W107.QAF;11 PSENERGY-GD148 (PEAK ENERGY GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12:DO:OO 3143. 00 through 3223.00 I o 0

o I 3200 I I o o o o I e o I I I I 0 I I o I o o o I I o o I I I o I o 0 I 0 I o I I o o e o I o 0 o o I o o o o I I o ' o o I o o o o I o o o o ' I 0 o o I o o . . co v ..-i I o* (!) )-(!) 0::: x x x x x x x LLJ 3180 z . . . . . o o o o o 0 I o o I I I 0 0 e o I o o o o I I o o o I o o o o I I o o e o o o o o I I o o o o I I o o o I o o o o o o o o o I o o I o o o o o e o I I o . . . . . . LLJ <I: LLJ CL 3160 ...................................................... * .......................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B107.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:41 through 7-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' * * * * ' * * * ' ',' ' ' o ' ' o o o ' ' ', o o ' ' o o o ' ' o o o 01 1 o o o o ' o o o o ',' ' o 0 o ' o o o ' ' o : o ' ' o o o o 1 ' o o o, 1 ' o .06 . . . . . . ............................................................................ . . .04 . . . . 02 ............................................................................ . . . . . . 0 ........... ......... ......... _..,__......._ 3-16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe
-v.> 0\ -0 ....., Vl 00 0 ID QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: :>, (.) i:: ID *n (.) *n 4-4-UJ . 35 x DKA100: [ENV_ALPHA.QA.W]W108.QAF;11 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:03 through 7-SEP-2016 12: 00:00 0. 337380 through 0.358250 x x x x x . 34 ............................................................................ . . . . . . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... \.;..) O'\ N 0 ......, VI 00 0 "° QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W108.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12:00:00 184. 000 through 204.000 200 ............................................................................ . . . . . . I D )-I-' H > H I-x x u x cl: LLJ x D x H _J x u ::i z x 190 . . . . . . o o o o o o o o o o o o o o o o 0 o o o 0 0 I o o o o I o o o o o o o o o o o o o o I 0 o o o o o o o o o o o o o o o o 0 o I I o o o o I o o o o I o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe -* ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W108.QAF;11 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:03 through 7-5EP-2016 12:00:00 5.00000 through 100.000 80 ........... ,* ............ * ............ * ............ * ............ : ............ * .. . ...-I I D C) z a H 1-::i ....I a (!). Ll.J o::* . . . . . . 60 ' .......................................................................... . . . . . . . x x x x x x x . . 40 o o o o o I I o o o I I o o o o o o o o o I o o o o o o o O O I I O o I o o o o o o o o o e o o o o o o o O o o I O o o o o o o o o o o o o o o o o o o . . . . . . 20 ...................................... *' ........................ ' ............... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrre ter Narrre Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W108.QAF;11 PSENERGY-GD148 (PEAK ENERGY GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 o o o o o I I o 0 o I o o o o o o o o o o o o o o 0 o 0 0 o o o o o o o o o o o o o I o 0 o o o o o o o o o o o o 0 o o o o o o o o o o o o 0 o o I o o ro """ I D (!) )-x x x (!) 0::: x x x x . . . . . . ........... * ............ * .............. * ............ * ........... : ........... * ... . w 3180 z w ::..::: <I: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B108.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:41 through 7-SEP-2016 12:00: 00 Lower/Upper LMts: 0.000000£+00 through 0.100000 . 08 ' o o o * ' I o 0 0 I I 0 0 0 0 I 0 0 o 0 I I o o 0 I I o 0 o o o o o o o I o 0 o o 0 0 o o o I I 0 0 o
I o o o I I 0 o 0 o I o o o o I o o o o I o o . . . . . . . 06 . . . . . . ....................................................... ' ................... . . 04 . . . . . . 02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Da.tes Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W109.QAF;11 AVRGEFF (Average Efficiency) 7-MAR-2016 09: 54:03 through 7-SEP-2016 12:00: 00 0.355179 through 0.377149 . . . . . . '37 ............................................................................ u c Q.) *ri u *ri 4-4-UJ x x x x x x x . 36 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-VJ 0\ -.l 0 H; VI 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W109.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:03 through 7-5EP-2016 12:00:0D 184.000 through 204.000 200 o ' o I o I o I o o o I o
o 0 I o 0 o 0 I 0 o o o o o o o o o o o o o o o o o o o o o o o o 0 o o o 0 o I o o o 0 I 0 0 o 0 0 o o

0 0 0 o o o I o o . . . . . . I D (!:I )-f-H *> x x H f-x u a: x LLJ D x H ....I u x x =:i z 190 ............ * ............ * ............ * ............ * ............ : ............ * .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
,_. V.l 0\ 00 0 ....., Vl 00 0 \0 QA filenafY'le ParafY'leter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA,W]W109.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12:00:00 5.00000 through 100. 000 80 ............ * ............ * ............ * ............ *, ........... : ............ * .. . -M I Cl z 0 H ::J 0 (f) w O:'. ::..:: a: w Q.. . . . . . . 60 ............................................................................ . . . . . . x x x x x x x 40 o o o o o o o o o o o o e o o o I o o 0 0 0 o o o o 0 o o o o o o o o e o o o 0 0 0 ' o 0 o 0 o 0 o o o o o o o o o I o 0 0 o I o I o o o o o o o I o o . . . . . . 20 ........... '* ........... '* ............ *' ........................................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW QA filenafYle Para1Y1eter NafYle Start/End Dates Lower/Upper LfYlts: 322_0 DKA100: [ENV_ALPHA.QA.W]W109.QAF;11 PSENERGY-GD148 (PEAK ENERGY GD-148) 09:54:03 through 7-SEP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 o 0 o o o o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o o o I o o o o o o o o o o o o 0 o o 0 o o o o o o o o o o o o o o o o o ro .,,,. ...-! I D )-. 0:: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . . LLJ :::...:: a: LLJ 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW .... \>) -...] 0 0 ......, Vl 00 0 "° QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B109.QAF;3 BACKRATE (Background Rate) 4-MAR-2016 12:61:41 through 7-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 . 08 .................................................... ' ' ..................... . Q) .µ iti a:: 1J c :J. 0 1-"0.Q .Y. u iti co . 06 . 04 . 0.2 . . . . . . . . . . . . ............................................................................ . . ............................................................................ . . . . . . 4-16 6-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tir'le UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: AVRGEFF (Average Efficiency) 7-MAR-2016 09:54: 03 through 7-SEP-2016 12:00:00 0.308266 through 0.327334 :::-, u c I]) -ri u -ri UJ I]) 'QI) Jtj I]) > a: x . . . . '325 o ' o ' ' ' ' ' o o ' ' ' o ' ' o o o o o ' ' o ' o ' ' o 0 o o ' o o o I I 0 o 0 o 0 o o o o o o o o o o I o o 0 I I 0 o 0 I I o o o o I o o o o I I o . . . . . . x x I 0 I 0 o I '32 ........... *.* *x ........ *.* ....................... *.* ........... : *x ......... *.* .. x . . . . . . x . . . . . . '315 ............................................................................ . . ' . . . '31 . . . . . . ............................................................................ . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Oate/Tirrie UP LOW -\;.) -....) N 0 ........ Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W110.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12: 00: 00 184. 000 through 204.000 200 ........... * ............ * .............. * ............ * ........... ' ........... * ... . I 0 (!:I )-t--H > H t--u a: w 0 H x x x ...J u x ::) z 190 . x . . . . . ........... *:* .......... *:* .......... *:* .......... *:*. x ......... : *x ......... *:* .. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W110.QAF;11 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12: 00: 00 5.00000 through 100. 000 . . . . . . 8.0 ' '
o * ' ' o o * ' o o

o 0 o " o o 0 o I 0 o 0 o 0 0 0 0 0 I 0 o 0 0 0 o 0 o o 0 o o o o I I o o o o I o o o I I o o o I I o o o o I o o o o I o o ...... I D z 0 H 1-=i 0 (/') w O:'. :>.! a:. w 0.. . . . . . . 60 o o o o o o o o o o o o o o o I I o o O o I o O O I O I o o O I O o o e o o o O o O I o o o o o o o o o o o o o o o o o o o 0 0 I o o o o o 0 0 o I I 0 . . . . . . x x x x x x x 40 ................................................ ' .......................... . . . . . . . 20 ................................................................................ . 3-16 4-16 5-16 6-16 7-16. 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W110.QAF;11 ParaMeter NaMe PSENERGY-80148 (PEAK ENERGY GD-148) Start/End Dates 7-MAR-2016 09: 54:03 through 7-SEP-2016 12:00:00 Lqwer/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . o o e' o o o o o o o I o o o o I e o o o o o o o o I o ' o o I o o o o 0 I o o o o o o o o o I 0 o o o I I e o o o 0 0 o o I I e o o o I o 0 o o I o o . . CD "<;t "i:""I I D )-0::: x x x x x x x w 3180 z . . . . . . ............................................................................ . . . . . . w <I: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower I Upper .Lr.-. ts: DKA100: [ ENV_ALPHA. QA, BJ B110. QAF; 3 BACKRATE (Background Rate) 4-MAR-2016 12:51:41 through 7-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' ' ' ' ' ' o ',' ' o ' o o ' ' * ' ' ',' o 1 1 ' ' o 1 1 ' o o ,' ' o ' o ' ' ' ' ' ' 1 ,' * ' o 1 ' ' 0 ' 1 1 o : o 1 1 ' ' ' ' ',' ' ' . . . . . . . 06 o o o o o I o o o o o I o o o I o o o o o I I o e o I I o o o o o o I o o o 0 0 o o o o o o o I o o o o o o o o o I o o o o I 0 0 o o 0 I o o o o I o o '04 . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: DKA100: [ENV_ALPHA.QA.W]W112.QAF;11 AVRGEFF (Average Efficiency) 7-MAR-2016 09:54:03 through 7-SEP-2016 12: 00: 00 0. 333084 through 0.353688 . . . . . . .35 o O o o o o o o o o o 0 O o O O o o o o o o o o o 0 I I 0 o o o o o o o o o o o 0 0 0 o 0 o o o o o o o o I 0 o o 0 o o o o o 0 o 0 o 0 I o o o o o o o ::>, (.) c ID *r-1 (.) *r-1 4-4-LU . . . . . . x x x x x x . 34 . . ' . . . ............................................................................ . ' . . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW QA filenafY'le ParafYJeter NafY'le Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W112.QAF;11 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-MAR-2016 09:54: 03 through 7-SEP-2016 12:00:00 184.000 through 204. 000 200 . : ......... " ......................... " ........... .' ........... : ............... . I D )-I-H > H I-u x a: x x w D x x H . ....I u x ::i z x 190 o 0 o o o o o o o o o o' o o e 0 o

o 0 o o o o' 0 0 0 o o o o o o o o o *, o o e o o o o o o o o 'o o o o o o o o o o o o: o t 0 0 0 o o I 0 o o o' o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12:00:00 5.oooao through 100.000 . . . . . . 80 ............................................................................ .,-! I Cl (!) . . . . . . z 0 H ::i _J 60 ............................................................................ 0 (f) w 0::: ::...: a:* w 0.. . . . . . . x x x x x x x . . . . . . 40 ............................................................................ . . . . . . 20 ...................................... *' ........... *' ........................... . 3-16 4-16 5-16 6-16 7-16 16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/ End Da.tes Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W112.QAF;11 P5ENERGY-GD148 (PEAK ENERGY GD-148) 7-MAR-2016 09:54:03 through 7-SEP-2016 12:00:00 3143. 00 through 3223. 00 . . . . . . 3200 I I o o O o O o O O O O o O O I O o O o o o I O O o o o O O o O I o o O ' o o o o O o o o o o o o o o o o o o o o o 0 o o o I 0 0 o 0 o I o

0 o I I o . . co -.:;t ...-i I D )-et:: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ o o o o 0 I LLJ lo.::: 0: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B112.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:51:41 through 7-SEP-2016 12:00:00 Lower/Upper O.OOOOOOE+OO through 0.100000 . 08 ' ' ' o o ' ' o o o ' ' o o 0 I o o 0 o o o o o o o o o o o o o o o 0 0 0 o o o o o o o o o o o o o o o I 0 0 o e o I o o o I I o o o o I o o 0 o 0 I o . . . . . . . 06 . . . . . . ............................................................................ . . . . . 04 . . . '02 ............................................................................. . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... w 00 ...... 0 Hi VI 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W113.QAF;6 AYRGEFF (Average Efficiency) 8-MAR-2016 08: 21:15 through 9-SEP-2016 12:00: 00 0.237837 through 0.252549 . . . . . . '25 ............................................................................ >:. u c Q) *ri u *ri 4-4-UJ . . . . . . x x x x x x . 245 ............ * ........... : ............ *. ....... : ............ * ............ * ... . . . . . . . . . . . . 24 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Parar.-.eter Name Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W113.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-201608:21:15 through 9-SEP-2016 12:00:00 184.000 through 204.000 200 ' ' o o o ' ' o o o ' o 0 0 o I I o o o o I o o o o I o o 0 0 I I o o o o I o o o o o 0 o 0 0 I I o o o I I o o o o o o o o ' I o o o o I, o o o o I I o . . . . . . I 0 (!) )-I-H > H I-u a: LL.I x 0 H ....I x x u ::i z x x x 190 I I 0 ' o 0 o o 0 o 0 ,' o o o I o o o o o I I : o o o I o o o o o o o 0° I 0 o o o o I o I o o ," o o o o o I 0 0 o I I 1° o o I o o o o o o o o o'o o I o x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W113.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 through 9-SEP-2016 12:00:00 5.00000 through 100.000 80 . . . . . . ,* . . . . ,* . . . . . . . . . . . : . . . . . . . . . . .. * . . . . . . . .... : . . . . . . . . . . . .* . . . . . . . . . . . . . . . . . '<'i I CJ z D H :l _f D 01 w O:'. ::..::: a: w O..* x x 60 ........... -: ... X. *. *. * * *: *
X* * * * * * * * **: * * * * * * * * * * *: * * * * * * * * * * * *: * * * * * * * * * * * *:* * *

x x x . . . 40 o o o o o o o e o o o o o o o o 0 o 0 0 o 0 o o o o o o o o o o o o 0 o I o o o o o o e o 0 o o o o o o o o o 0 I I o o o o o o o o o o 0 o o o o o o . . . . . . 20 ........... " ............ ' ........... " ........... ' ........... " ........... '*' .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W113.QAF;6 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 8-MAR-2016 08: 21:15 through 9-SEP-2016 12:00: 00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . ' ............................................................................ co ""'" "<"'i I D (!) )-(!) 0:: x x x x x x x IJJ. 3180 z . . . . . . o o o ' o 0 o o ' ' ' ', o 0 o o o o o o o o o : o o o ' o ' 0 o o o o ', o o o o o o o o o o o ', o o o o o o o o o o o ', o o I o o o o o o o o ',' o o o IJJ ::...! a: IJJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenafY'le ParafY'leter NafY'le Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.B]B113.QAF;3 BACKRATE (Background Rate) 4-MAR-2016 12:30: 40 through 9-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 ° 0

0 0 ' 0 0 0 * ' ', 0 0 0 0 ' 0 0 0 0 ' ' : o 0 ' ' 0 0 0 0 ' 0 0 ',' ' 0 0 0 0 ' 0 0 0 0 *. o o o 0 o 1 0 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 ',' 0 0 0 . . . . . . .06 ............................................................................ . 04 . 02 ...................................................... -.................... . 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW QA f i lenaMe . ParaMeter NaMe Start/End Dates Lower/Upper LMts: . 255 >, u c ID *r-1 u *r-1 4-4-UJ ID x "0.0 iU s.... DKA100: [ENV_ALPHA.QA.W]W114.QAF;6 AVRGEFF (Average Efficiency) 8-MAR-2016 08:21:20 through 9-SEP-2016 12: 00: 00 0. 244425 through 0.259545 x x x . . . . ID . 25 I I o 0 I 0 I o *

I I o I o o o o o o o o o o o o o o o o o O o o O O O I I I o o o o o o o o o o o o o I o o o o O o O I o O o o o o o o o o o o o o > cr: . . . . . . x x x ......... -.. * ........... : ............ * ......................... * ............ * ... . .245 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... (,,.) 00 --.J 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W114.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:21:20 through 9-SEP-2016 12:00:00 184.000 through 204. 000 200 * ' * * * * ' * * * ' ,* * * * ' ' * * * * ' ' : * * ' ' * * * ' * * * ,*' ' * *
o ' * * * * ,"' * * * ' ' * * ' ' ' ,*' * ' ' * * * * ' * * ,', I '

x x x x x x 150 . . . . . . o I 0 0 o 0 0 o o 0 o o O o o o o o o o o o o o o o o o 0 o O I O I o o o o o o o o I o o o o o o o o o o o o 0 o * ' o o o o ' o o o o o o 0 o o o I o . . I Cl (!) )-I-H > H I-u a: . . . . . . w 100 ............................................................................ . . . . . . Cl H _J u ::i z* . . . . 50 o I o o o o I o o o 0 I o o 0 0 0 o o o o o o o o o I I o o o o ' o o o I I o o o o I o o o o o o o 0 o I I o o o I I o 0 o I 0 o o o o I o o o o o I o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W114.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:21:20 through 9-SEP-2016 12:00:00 5. 00000 through 100.000 x . . . . 150 ............................................................................ . . . . . . T"I I Cl C) z 0 100 H f-::i _J 0 if) w O:'. ::.::: a: w 0... x x x x x 50 ........................... *X* .................... , ............................. . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W114.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:21:20 through 9-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 o ' o o o o ' o o o ' ' o o o ' ' o o o o I 0 0 0 o I o o o o o I o o o o o 0 o o o o o o o o o I 0 o o I o o o o o o o o o 0 o o I o o o o o o o I I o co ""'" ...-1' I* D 0::: LL.J z LL.J . . . x x x x x x 3150 ............ * ........... : ............ * ......................... * ............ * ... . 3100 I I o o o o I o o o I 1' o o o o I o o 0 o 0 I : o o o o o o o I o o o ,o o 0 o o o o I o o o o too o o o I o o o o I I o' o 0 I o o o o o o 0 o o'o I < o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B114.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:30:44 through 9-SEP-2016 12: 00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' * ' ' ' o ' ' ', o ' ' ' ' ' ' o ' 1 1 : ' ' 1 1 ' o o o ' o o 0' 1 1 o o o o 1 o o o o 1' 1 o o o o 1 o o o 1 1 ', o ' 1 1 ' ' 1 ' 1 ',' 1 1 ' .06 . . . . . . ............................................................................ . . . . .04 . . . . .02 ............................................................................ . . . . . . 0 ......... ____ ....._ __ .,.__ _______ .......... ___. ......... __ __,,..,..__.... __ __ 3 -16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe 0 ....., Vi 00 0 \0 QA filenarrie DKA100: [ENV_ALPHA.QA.W]W115.QAF;6 Pararrieter Narrie AVRGEFF (Average Efficiency) 5tart/End Dates 8-MAR-2016 08:21: 23 through 9-5EP-2016 12:00:00 Lower/Upper Lrrits: 0.246238 through 0.261470 '26 ............ * ........... : ............ * ......................... * ............ * ... . (J c Q) *r-1 '255 (J ............................................................................ -. . . . . . *r-1 4-4-w Q) -0.0 x '° s.... Q) x x x > -t-H > H t-u <I: w x 0 H ....I u =i x x x x z 190 ............ * ........... : ............ *' ........................ * ............ * ... . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafYle ParafYleter Narrie 5tart/End Dates Lower/Upper LfYlts: 100 DKA100: [ENV_ALPHA.QA.W]W115.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:21:23 through 9-5EP-2016 12: 00:00 5.00000 through 100.000 80 ............ * ........... : ............ * ........... : ............ * ........ ' ... * ... . ..-! I D (!:) z 0 H :J ....I 0 01 w. 0:: ::..::: a: w 0.. . . . . . . 60 o o '*' o o o o o o o o I o o o I o o o o I o o o o I I o o 0 0 o o 0 0 0 I o o o o I o o o o o o o 0 o I 0 0 o o I o o o o I I o o o o I 0 0 0 I 0 I o . . . . . . x x x x x x x . . . 40 ............................................................................ . . . . . . . 20 ........... * ..................................... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenaMe DKA100: ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 8-MAR-2016 08:21:23 through 9-5EP-2016 12: 00: 00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . ............................................................................ CD v .,-I I 0 (!) )-(!) O:'. x x x x x x x I.LI 3180 z . . . . o o o o o o o o o o o o o o o o o o o o o 0 I o o 0 I o 0 o o o o o o o o o o o o o o o o o o 0 I o o o o o o o o o o o o o I 0 o 0 o o I o o o o o o o . . . . . . I.LI ::..:::* a: I.LI 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B115.QAF;2 ParaMeter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:30: 48 through 9-SEP-2016 12:00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP . 08 o 0 o o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 I I o o o o o o o o o I I 0 0 o I o o o o o o o o o I 0 o o o o I o o o o ' I o . . . . . . . 06 . . . . . . I o o o o o o o o o I I o 0 0 I 0 o o 0 o o I o o o I I o o o I I 0 0 o 0 I o I o o I o o 0 o I 0 o 1 o o o 1 o o I 1 O O o ' 1 o o o O 1 o o O O I I o . OA . . . 02 ............................................................................ . . . . . . 0 ......... ---"-'--"""'----'-"--......... __.....__ .......... __.....__-""----"->--_._,_ ......... .__ 3-16 LOW 5-16 8-16 9-16 Measurement Date/TiMe
....... . V.l IO O'I 0 ......, VI 00 0 IO QA filenar.-.e Parar.-.eter Nar.-.e St:art/ En*d Da-tes Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W116.QAF;7 AVRGEFF (Average Efficiency) 8-MAR-2016 08:21:27 through 9-SEP-2016 12:00:00 0.250100 through 0.265570 . 265 * * * * * * * * * * * *" * * * ' * * * * * *
I * * * * * * * ,, ' ' * ,o * * * * * * * * * *

_,' * * * * * * * * * * * * ' ' * * * * * * * *'* * ' ' x :>,-u . 26 c o o o o o o o o o o o o' o 0 o 0 o 0 0 o o o"o : o o o o o o o I 0 o o o' o o o o 0 o 0 0 0 0 0 .. o o o o o 0 o 0 0 0 0 o' o o o o o o o o 0 o 0 o'o o o o I}) *r-1 u *r-1 x 4-4-UJ I]) "0.0 i1j x S-I}) x > a: . 255 .. x ......... * ........... : ........... : ........... : ........... : ............ * ... . . . . . . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measu.rer.-.ent Date/Tir.-.e UP LOW QA filenafl"le Parafl"le ter Nafl"le Start/End Dates Lower/Upper Lfl"lts: DKA100: [ENV_ALPHA.QA.W]W116.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:21:27 through 9-SEP-2016 12:00:00 184.000 through 204.000 200 ........... '. ........... : ........... " ........... '. ........................ *.* .. . I 0 )-I-H > H I-u <I: x x w 0 H _J x x x u ::i x x z 190 ........... ,* ........... : ............ * ......................... * ............ * ... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl"lent Date/Tifl"le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W116.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:21:27 through 9-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... ,* ........... : .. ' ......... * ............ *' .* .......... * ............ * ... . -M I Cl (!) z 0 H ::i ....J 0 ti) LU O:'. ::..:: a: LU 0... . . . . . . 60 o o o o o O o o o o o O o o o O O e O O e o o o o O I o o o o o o .o o o I o 0 o ,0 0 I 0 0 0 0 I I e o o 0 0 o o o I I o o o I I 0 0 e 0 I o 0 0 o I I o . . . . . . . x x x x x x x . . . . . 40 0 I o o o I 0 e o o o I o o o I o o o o o I 0 o o 0 I 0 o O O I I O O O O O o o o o o o o o o o I o o o I O O O O I O O o O O O o o o o o o o e o I o o . . . . . . 20 ........... '* .................................... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMen t Date/ T iMe UP LOW QA filenarrie Pq.rarrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W116.QAF;7 PSENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:21:27 through 9-SEP-2016 12:00:00 3143.00 through . . ' . . . 3200 0 I o o 0 o I o 0 o 0 o 0 I o 0 I 0 0 0 0 0 I 0 0 o 0 0 o o o I o o o o I o o o o o I o o I o 0 I 0 o 0 0 I 0 o o 0 I 0 o o I o o o o o I o o o o o I o . . . co ""'" . ..n I D (!) )-" .(!) et:: x x x x x x x UJ 3180 z . . . . . . o o o o o I I o o o I I o o o I I o 0 o o o I 0 0 o 0 o o o 0 I I o o o I o o o o o o o o o o o I 0 o 0 o. 0 I 0 0 I I 0 0 0 I I o 0 o o o o o o 0 0 I o . -. ' . . . UJ :..:: 0: UJ a.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW
-0 0 0 >-!) Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B116.QAF;4 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 12:30:52 through 9-5EP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 *'* ' ' ' ' ' * *' ' ',' ' ' ' ' ' ' ' ' 1 ' : o ' ' o o 0 0 1 1 ' ' ',' ' ' ' ' ' 0 o ' ' o ', 1 ' o o 1 1 ' 0 0 1 1 ',' o ' ' o ' ' o ' ',' 1 1 ' . . . . . . . 06 ............................................................................ . 04 ............................................................................ 0 x 3-16 . . . . . . . MeasureMent Date/TiMe x x 9-16 UP LOW -.p.. 0 -0 ....., Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W117.QAF;6 AVRGEFF (Average Efficiency) 8-MAR-2016 11:51:37 through 9-SEP-2016 12: 00: 00 0.250782 through 0.266290 . . . . . . '265 ......... -................................................................. . . . . . . ' x >, 0 c ID .26 *r-1 .. x . . . . . . . . .: . . . . . . . . . . . . . . . . . . . . . .. : . . )5 . . . . . . . . . . . . . . . . . . . .: . . . . . . . . . . .. : . . . . 0 *r-1 4-x 4-LLJ x ID Wl Ill I-ID x > c,I x '255 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W117.QAF;6 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 8-MAR-2016 11:51:37 through 9-5EP-2016 12: 00: 00 Lower/Upper LMts: 184.000 through 204.000 UP 200 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . I 0 r H > H u x w 0 x x H x x x u z 190 0 0 ' 0 0 I o 0 0 0 I 1' o 0 o ' o o o 0 o o o : o o o o o o o I I
o o' I o o o o o o o o o o ," o o 0 o 0 o 0 o o o o o' o o o o o o o o o 0 o ,', 0 o o x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W117.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 11: 51:37 through 9-SEP-2016 12: 00: 00 5. 00000 through 100.000 80 . . . . . . . . . . . .* . . . . . . . . . . . : . . . . . . . . . . .. * . . . . . . . . . . . : . . . . . . . . . . . .* . . . . . . . . . . . . . . . . . .,.... I D z 0 H 1-::i _J 0 en w Cl:'. a:* w 0.. . . . . . . 60 . ')<' ....... * ... x' ....... : .. x' ....... * ............ * ... x* ....... * ............ *.*. *x* x x . . . . 40 ............................................................................ . . . . . . 20 ........... '* .................................... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Y'lent Date/TifY'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W117.QAF;6 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 8-MAR-2016 11:51:37 through 9-5EP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . o ' o o o ' o o o o ' I o o o 0 o o o o o o o o o o o o o o o I 0 o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o o ' o o o o o o o o o I o o co v """"" I D )-0::: x x x x x x x LL.I 3180 z . . . . . . o o 0 0 o I o 0 o o o 0 0 0 o o o o o o o o o o o o o o o o o o 0 o o 0 I 0 o o o o o o o o o o o o o o 0 o o o o 0 o o o o o o o o o o o o o o o 0 o o . . ' . . . LL.I ::..::: <L LL.I 0.... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B117.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:30: 56 through 9-SEP-2016 12:00:00 Lower/Upper Lmts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' ' ' ' ' ' ' ' ',' * ' ' ' ' ' ' ' 1 1 : ' ' o o ' ' o o o ' ' ', 1 1 ' ' ' ' 1 ' ' o O ', O ' o o o o o o o o o o0 o o o o 0 0 0 0 1 0 0 ',' 1 1 0 .06 . . . . . . ............................................................................ . 04 . . . . 02 ............................................................................ . . . . . . o """""".__""-'-____...__.........___.._=----..:....:....---"-.__ .......... 3_16 5-16 6-16 8-16 9-16 LOW Measurement Date/TiMe
,_. 0 O"I 0 ....., Vl 00 0 \0 QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W118.QAF;9 AVRGEFF (Average Efficiency) 8-MAR-2016 08:21:36 through 9-SEP-2016 12: 00: 00 0. 248236 through 0.263590 . . . . . . . 26 ...................... ' .................................................... . u c Q)" *r-1 u *r-1 4-4-UJ . . . . . . x x x x x . 2 5 5 . . x . . . . . . . . *: . . . . . . . . . . . : . . . . . . . . . . . *: . . . . . . . . . . . : . . x. . . . . . . . *: . . . . . . . . . ... : . . . . . 25 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Oate/TifY'le UP LOW -.j::.. 0 ....:i 0 Vl 00 0 l,O QA filenaMe DKA100: [ENV_ALPHA.QA.W]W118.QAF;9 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 8-MAR-2016 08:21:36 through 9-SEP-2016 12:00:00 Lower/Upper LMts: 184.000 through 204.000 200 ............................................................................ . . . . . . I 0 (!) )-I-H > H I-x u a: w x 0 H ...J x x x u ::i z 190 . . . x . . . .. >!'. .*....... * *.*......*. : ...**....... * ......................... * ............ * ... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... .j:>. 0 00 0 H') Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W118.QAF;9 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 8-MAR-2016 08:21: 36 through 9-SEP-2016 12:00:00 Lower/Upper LMts: 5. 00000 through 100.000 ....... I D z 0 H =i ...J 0 en w O:'. ::..::: ([ w 0.. 100 80 ...... ' ..... * ......... ' . : ....... ' .... * ......................... * ............ *. ' .. x 60 . . . . . . .............................................................................. . . . . . . x x x x x x . . . . . . 40 0 I 0 o 0 0 0 o o o o o o o o o 0 o o o o 0 o o o o o o o o 0 I I 0 o 0 ' o o o o o o o o o o o o o e o o o o 0 o 0 I o o o o o o o o 0 I 0 o o o o o o . . . . . . 20 ........................ ' ........................ ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W118.QAF;9 P5ENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:21:36 through 9-SEP-2016 12: 00:00 3143.00 through 3223. 00 . . . . . . 3200 ' ' o o o ' 0 o o 0 I 0 o o 0 0 I o o o o I o o o o I I o 0 o ' ' o o o I 0 o o o o I o 0 0 0 0 0 0 o o 0 I 0 o o I I 0 o o I o o o o o ' o o o o o o o . . . co ""'" .....! I 0 (!) )-(!) Cl:'. x x x x x x x IJ.J. 3180 z . . . . . . ............................................... ' ' ........ ' .... ' ............ . . . . . . . w :ii.: , u c ID *ri u *ri 4-4-UJ . 24 . . . . . . x x x x x . . . . . . . 235 ' ......................................................... ' ................ . . . . . . . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW -.j::.. -N 0 ....., Vl 00 0 \D QA filenal'le Parafl"le te*r NafY'le 5tart/End Dates Lower/Upper Lfl"lts: DKA100: [ENV_ALPHA.QA.W]W119.QAF;7 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:21:40 through 9-5EP-2016 12: 00: 00 184. 000 through 204.000 200 ........... * ............ : ........... * ............ ' ............ * ............ *.* .. . I D (!) )-I-H > H I-u a: Ll.J D H ...J .x x x x u ::i z x x x 190 I 0 0 I I I o I I I I 01 o o o I o o o o o I I : o o I I o o 1 I O o o o' I o o o o o I o o o o ," o o o o o O o o o I I o1 o o o o o o o o o o o 111 O o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/Til'le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W119.QAF;7 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:21: 40 through 9-SEP-2016 12:00: 00 5. 00000 through 100. 000 80 ............ * ........... : ............ * ......................... * ............ * ... . -M I D C) . . . . . . z D H 1-::i ...J D tr) lJJ Ct'. 60 ........... *.* .......... : ........... *.* *; ........ * .. *x* ....... *.* .......... *.*. *x ::..! a: lJJ 0.. x x x x 40 o I 0 o 0 0 o o
o I I o o o o o o o I o I I o o o I I o o o I I o o o o o 0 o o 0 I o 0 o o I I o o o I o o o o ' o o o o o o o o o o o o o o o o o o . . . . . . 20 ........... '* ........... ' ........................ ' ............................. . 3-16' 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W119.QAF;7 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 8-MAR-2016 08:21:40 through 9-SEP-2016 12: 00: 00 Lower/Upper LMts: 3143.GO through 3223.00 UP 3220 3200 . . . . . . ............................................................................ co """" "<""i I D (!) )-(!) O:'. x x x x x x x w 3180 z . . . . . . o o o o o I 0 o ' o o o o o o o o o o o

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o o o o o o o o o o o o o o o o o o I o o . . . . . . w :..::: a: w 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOlll MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B119.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Datee 4-MAR-2016 12:31:09 through 9-SEP-2016 12:00: 00 Lower/Upper LMte: O.OOOOOOE+OO through 0.100000 I 08 o ' a o o ' o o ' o o ', o 0 o ' o o o o o ' ' : o o o o o o 0 o o o o 'o I o o o o o o o o o o ', o o o o o o o o o o I ', o o o o o o o o ' o o *,O I o o . . . . . . . 06 o o o o o o o o O o I O o o 0 o o o o o o o o o o o o o o o 0 0 I 0 0 o 0 0 o 0 o 0 0 I 0 0 o 0 o 0 o o 0 0 o 0 o I o o 0 o 0 I o o o o o o o o o o o o . . . . 04 . 02 ............................................................................ 0 3-16 . . . . . . x x x x x 4-16 5-16 6-16 8-16 9-16 MeaeureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W120.QAF;7 AVRGEFF (Average Efficiency) 8-MAR-2016 08: 21:44 through 9-5EP-2016 12:00:00 0.247350 through 0.262650 . . . . . . . 26 o o o o o o o o o o o o o o o o O o o o o I I 1 o O I I o O O I I o o O o o O O o o o o o o o o I o o o I I o o o o o o 0 o I I 0 I 0 o I 0 0 0 0 I I o u c Q) *r-1 u *r-1. 4-4-LU Q) 'O,I) nj Q) > a: . . . . . . 255 ............................................................................ . . . . . . x x x x x x x . 25 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:21: 44 through 9-5EP-2016 12:00: 00 184.000 through 204.000 200 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . x I CJ (!) )-f-H > H f-u x a: x w CJ H _J x u x ::i z 190 ........... *:*. x* ....... : ........... *:* .......... *: ........... *:* .......... *:* .. . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenafY'le Pa raffle ter NafY'le 5tart/End Dates Lower/Upper LMts: x 100 .-1 I D (!) z 0 H I-::i ....I 0 ({) w [( :::..::: a: DKA100: [ENV_ALPHA.QA.W]W120.QAF;7 P5FWHM-GD148 (PEAK RE50LUTION GD-148) 8-MAR-2016 08:21:44 through 9-5EP-2016 12:00:00 5.00000 through 100.000 x x w 50 I I 0 o o 0 o o o o o 1' o o o 0 I o o o 0 I I : o o I o o o o o o o 0 o' I I o ' o o o o o o o ," o o o o o I o o o I o o' o o o I o o o o I o o o'o I I I 0... x x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW
-..j::.. -\0 0 ......, Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W120.QAF;7 P5ENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:21:44 through 9-SEP-2016 12:00:00 3143.00 through 3223.00 3220 ........... '* ........... ' ........................ ' ............................. . 3200 ........... * ............ : ........... * ............ * ............. * ............ *.* .. . ro '<t" -..-! I 0 (!) )-3180 (!) x x x x x x . . ............................................................................ o o o o o I 0::: LL.I z LL.I ::..:::* a: LL.I CL 3160 ............ * ........... : ............ * ........... ; ............ * ............ * ... . . . . . 3140 o o o o o o 0 o 0 o o ,o o o o o o o o o o o I : o 0 o 0 0 0 o o o o o o' o o o o o o o o o o o .. o o o o o o o o o o o o' o o o I o o o o 0 o o o'o 0 I 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Oate/Tirrie UP LOW ...... .+::-. N 0 0 Hi Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B120.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:31:13 through 9-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 1 0 1 ' ' 1 1 ' ' ' 1 ',' 1 o 1 0 o 0 0 0 0 1 : 0 0 0 0 0 0 0 0 0 0 0 ', 0 0 0 o 0 0 0 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 ', 0 0 1 0 o 0 0 0 0 0 0 ',' 0 o o . . . . . . . 06 o ' ' e o o o o o o o o o o o ' o o o o o 0 o o o o o o o o o o I o o o o I o o o o o o o o o o I o ' o o o o o o o o o o o o o o o o o o o o o o o o o . 04 . 02 ............................................................................ 0 3-16 x . . . . x . . x x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 ......, Vi 00 0 \0 QA filenaMe Parameter Name 5tart/ End oa-tes Lmi..1er I Upper Lmts: DKA100: [ENV_ALPHA.QA.W]W121.QAF;7 AVRGEFF (Average Efficiency) 8-MAR-2016 08:21:48 through 9-5EP-2016 12:00:00 0.248969 through 0.264369 x x x x .26 . . . . . . . . . . . .* . . . . . . . . . . . : . . . . . . . . . . .. * . . . . . . . . . . . .. . . . . . . . . . . . .* . . . . . . . . . . . . . . . .. ::>, (.) c ID *r-1 (.) *r-1 4-4-UJ x ID "QI) x (lj . . . . . . I-' 25.5 ' ' o o o ' 0 o I o o o o o o I o 0 0 o 0 I o o o o o o o o o 0 I o 0 o o I o o o o o o o o o o o o o o I 0 0 o o 0 I o o o o o o o o o o o o o o ' 0 0 ID . . . . . . > a: x '25 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/TiMe UP LOW QA filena!l1e Para!l1eter Na!l1e Start/End Dates Lower/Upper Lfl1ts: DKA100: [ENV_ALPHA.QA.W]W121.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:21:48 through 9-SEP-2016 12:00: 00 184.000 through 204.000 200 I I I I o 0 I Io o 0 I I o 0 I I o I o 0 I 0 0 0 I 0 I o 0 I I I I I I I I 0 I I I I 0 Io o I I I 0 o I 0 o o I I I 0 o 0 I I o o Io I o 0 o o I I o . . . . . . I Cl (!)" >-I-H > H I-u a: x w Cl H _J x . ' x x x u x ::i z 190 . . . ' ............ * ........... : .. x ......... * ......................... * ............ * ... . . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl1ent Date/Ti!l1e UP LOW QA filenal'le Paral'leter Name Start/End Dates Lower/Upper Lmts: 100 x DKA100: [ENV_ALPHA.QA.W]W121.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:21:48 through 9-SEP-2016 12:00:00 5. 00000 through 100.000 x x x x 80 ' I o o o o o o o o o *,' o o o o o o o o o o I : o o 0 o o o o o I 0 o ,* o o o o o o o o o o o ," o o o o o o o o 0 o I ,' o o I I 0 o o o 0 o o ,', I 0 o ........ I 0 (!) z 0 H :=J _J 0 (J) L1.J O:'. :..::: a: L1.J 0... x x . . . . . . 60 ........................... ' ................................................ . . . . . . . 40 I I 0 o o o o o o o o o o o o o o o o o e o o o o o I O O o o I I o o O O O o O o o o o O o O o o o o I O
o o o o o o o o o o o o o o o o o o o o o o . . . . . . 20 ........... '* ....................... '* ........... ' ........... '* ........... '*' .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Til'le UP LOW QA filenafY'le Pa raffle ter NafY'le 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W121.QAF;7 P5ENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:21: 48 through 9-5EP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ........... ' ............................................................... . . . . . co """" ........ I D )-O:'. x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ ::..:: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW
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o . . . . . . . 06 . . . . . . I I I o o I 0 o o o I I o o o o o o o o o o o o I o I o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o o e o o I o o o I 0 I o o I o o I o . . . 04 . . . . . . 02 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0 3-16 4-16 6-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
..... ..j:::.. N 0\ 0 ....., Vo 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: >i (.) c 11) *r-1 (.) *r-1 4-4-UJ .27 x DKA100:[ENV_ALPHA.QA.W]W122.QAF;7 AVRGEFF (Average Efficiency) 8-MAR-2016 08:21:53 through 9-SEP-2016 12:00:00 0.257670 through 0.273610 x . 2 6 5 . . . . . . . . . . . *: .. x. . . . . . . . : . . . . . . . . . . . *: . . . . . . . . . . . : . . . . . . . . . . . *: . . . . . . . . . . .. : . . . . a:i s... 11) > a: x . 26 . . . . . . . . . . . : . . . . . . . . . . . : . . . . . . . . . . . : . . .' . . . . . ._ . . : . . . . . . . . . . . : . . x* . . . . . . . . . . . . . . . . . . . x 3-16 *. 4-16 5-16, 6-16 7-16 8-16 9-16
Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W122.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:21:53 through 9-SEP-2016 12:00:00 184.000 through 204.000 200 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . I 0 (!) )-I-H > H I-u 'X a: x x w 0 x H ....I x x u ::i z x 190 ............ * ........... , .. x* ........ * ......................... * ............ * ... . .3-16 4-16 .5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe. DKA100: [ENV_ALPHA.QA.W]W122.QAF;7 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Oates 8-MAR-2016 08:21:53 through 9-5EP-2016 12: 00: 00 Lower/Upper LMts: 5.00000 through 100.000 ..,.... I D (!) z 0 H ::i __J 0 U') w O:'. ::..::: a: w CL 100 80 60 40 . . . . . . ............................................................................ . . . . . . o o o o o o o o o o o o o 0 o o f o 0 0 o o o o o o 0 o o o o o o o o o o o o o 0 o I ' 0 o o 0 o o o o I o o o o o o o o o 0 0 0 0 ' 0 ' o o o o ' o o *x . . . . . ' x x x x x x . . . x o I o o o ' o o o o I o o o o I I o o o o o I o o I o I o 0 0 I I 0 o 0 o o o o o o o o o o o o o o 0 0 0 o 0 I I o o 0 I I o o o o o o o o o o o 0 o o I o ' o 20 ........... '* .................................... ' ........... '* ................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafY'le ParafY'leter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W122.QAF;7 PSENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:21:53 through 9-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ' .......................... ' ............................................... . . . co ""'" .....! I D (!) )-(!) 0::: x x x x x x LL.I 3180 z . . . . . . ...................................................................... ' ..... . . . . . . LL.I :ii.: H I-u x <I: w D H x ....I x u ::i z x x x . . . . . . 190 o o o o o ' ' o o o ' ' o o o I I o o o 0 o o o o o 0 o o o o o o o o o o o 0 0 o 0 0 o o o o o o o o o o 0 o o o I I o o o o o o o o o o o 0 o o I o o x 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W124.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016. 08:22:01 through 9-SEP-2016 12:00:00 5.DOOOO through 100.000 . . . . . . 80 o o o o o o 0 o o 0 I 0

0 o 0 I o 0 o o I I o o o I I o o o o o o o o I I 0 o 0 o I 0 0 0 0 I 0 o 0 o 0 o o o o I I o o o I I o o o o I o o o o I o o I Cl z 0 H ::i ...J 0 01 w O:'. a: w 0.. . ' ......... -:* .......... : ............ -: ........... *: ........... *:*. ....... *:* .. . x x x x x x . . . . . 40 I I o 0 o I I o o o I o o o o 0 I 0 0 0 o 0 0 0 0 0 o I o

o o o o o o o o o o 0 o I 0 o 0 0 0 o 0 0 o I 0 o 0 0 I I 0 0 0 0 0 0 0 o 0 0 o o o o 0 I o . . . . . . 20 ........... '* ........... ' ........................ ' ............................. . *. 3-16 4-16 5-16 6-16 7-16 8-:1:6 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W124.QAF;8 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 8-MAR-2016 08:22:01 through 9-5EP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 ........................ ' ........................ , ........................... ' .. 3200 . . . . . . 0 I o o o o I o o o o o o o o I o 0 o 0 o o o o o o o o o o 0 I ' o o o o o o o o o o o o o o o o o o o o 0 ' o o o o o o o o ' o 0 o o ' o o o o o o o . . co """'" I 0 (!) )-(!) et:: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . ' . . . LLJ ::..:: :. (.) c Q) *ri (.) . . . . . . *ri x 4-4-UJ

255 ................................................. ' ............................. . Q) -of! iU. Q) > a: x x x x x x . 25 0 0 o o o I o o o o I o' o o o o I o o o o o I : o o I I o o o o O o o o1 O o o o o o o o o o o ," o o o o o o o o o I I o' o o I I o o o o o o o o1o I I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrre Pararrre ter Na*rrre 5tart/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W126.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:22:09 through 9-5EP-2016 12:00:00 184. 000 through 204.000 200 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . I Cl )-I-H > H I-u a: x w Cl H *X x x x _J u ::i x x z 190 . . . . . . 0 o 0 o o 0 o o o o o o o 0 o I o o o o o o o o o o ' o o ' 0 I o o o o o o o o o o o o o o o o o o o o I o o o o 0 0 o o o I o o o o o o o o o o o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW
-(.,.) 00 0 ....., Vi 00 0 \0 QA filenaMe Parafl'le ter NaMe Start/End Dates Lriwer/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W126.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:22: 09 through 9-SEP-2016 12:00:00 5. 00000 through 100.000 . . . . . . 80 ............................................................................ .n* I D (!) z D H 1-::i _J D (f) w ::..::: a: w 0... . . . . . . 60 0 I 0 0 o o I o o
o o o o o o o o o o o o o o o 0 o o o o 0 I 0 o o o o o o o o o o o o ' o o o o o o o o o o o o o o o o I 0 0 o o o ' o o o o ' o o . . . . . . x x x x x x x 40 ..................................... ' ..................................... . . . . . . . 20 ........... '* ........... ' ........... " ........... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenal'le Paral'leter Name Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W126.QAF;6 P5ENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:22:09 through 9-SEP-2016 12: 00: 00 3143.00 through 3223.00 o o I I

f 3200 I I I I I 0 0 I o o I o I I o I I I I I I o I I I I o o o o I 0 0 I I I I I o o I I I ' 0 o I 0 I I o I I I I o I 0 0 0 o I I I Io Io I o 0 o ' o I I . . . ro ""'" ..i I D (.') )-(.') Cl:'. x x x x x x x LL.I 3180 z . . . . . ............................................................................ . . . . . . LL.I ::..:: a: LL.I CL 3160 .3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-201613:43:13 through 9-SEP-2016 12: 00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' 0 ' 0 ' ' ' ' ',' ' * ' ' 0 ' 0 o o o : o 0 0 ' 0 0 0 0 0 0 0 ',' 0 0 0 0

0 o 0 o 0 '* o 0 0 0 0 0 0 0 0 0 0 ', 0 0 1 o o o 0 0 1 1 0 ',' 0 ' 0 .06 . . . . . . .................................................................... ' ...... . . . . . .04 . . . . '02 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Oate/TiMe 0 ....., Vi 00 0 \C) QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 8-MAR-2016 08:22:12 12:00:00 0. 258380 through 0.274360 . . . . . . .27 O o o o o o I o o o I o o o I I O O o O o O o o o o I o o o o o I o o o o I o o o o I o o o o I 0 0 0 o 0 o o o o o I o o o I I o o o o o o o o o 0 I o . . . . . . >> 0 c I]) *r-1 0 *r-1* 4-4-UJ x x x I]) -0.0 Ill . 265 I-............ * ........... : .. *X* ........ * ........... ' ............ * ............ * ... . . . . . . x . I]) > x <I: x :x I 26 ' o o o o ' o o o o 1 10 0 o o 1 o o o o o 1 1 I o o 1 1 o o o o o o o '* 1 0 o o o o 1 o o o o 'w o o o o ' 1 o o o 1 1 '* o o 1 1 o o o o 1 e o o,o o 1 1 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenal'le Paral'leter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W127.QAF;8 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:22:12 through 9-SEP-2016 12: 00: 00 184.000 through 204. 000 200 ............................................................................ . . . . . . I Cl (!) )-I-H > H 1--* u x a: w Cl. .xx H -' u x x '.:) x z 190 ........... *:* .......... : ........... *: ........... *: .. x* ....... *:* .......... *:* .. . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W127.QAF;8 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:22:12 through 9-SEP-2016 12: 00: 00 5.00000 through 100.000 80 ............ * ........... : ....... ' .... * ......................... * ............ * ... . ..... I D C) z 0 H =i ....J 0 rJ) w O:'. 60 . . . . . . o ' o o o o o o o o 0 o 0 o o ' I o o o o o o o o o 0 o o o o I 0 o o o I I 0 0 o 0 I 0 o 0 0 0 I 0 0 o I 0 o o o 0 I o o o 0 0 0 o o o o o o o o o o o x . . . . . . x x . . . x x *x x 40 0 0 0 o o o o o o o o o o o o 0 I o o o o o o o o o o o o o o o 0 o o 0 o 0 0 o o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o . . . . . . 20 ..................... " ........................... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENY_ALPHA.QA.W]W127.QAF;8 PSENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:22:12 through 9-SEP-2016 12:00:00 3143.00 through 3223.00 3220 * * * * * * * * * * * *" * * * *' * * * * * *

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3200 . . . . . . . ..................................................... ' ..................... . . . . . . . co "'3" """" I D )-Ct'. x x x :xx x x x LLJ 3180 2 o o o o 0 I ............................................................................ . . . . . . LLJ a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-t Ul 0 >-+, Ul 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B127.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:43:18 through 9-SEP-2016 12:00: 00 O.OOOOOOE+OO through 0.100000 . 0-8 . ' .......... * ............ : ........... * ............ * ............ * ............ *.* .. . . 06 . . . . . . o 0 0 0 o 0 o o o o o o o 0 o ' I o o o o o o o o o 0 0 0 o 0 o o o o o o o o o o o I o o o o o o o o o I o 0 0 0 I I o o o o o o o o o I o o o 0 0 o o . . . 04 '02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafl"le Parafl"leter Nafl"le Start/End Dates Lower/Upper Lfl"lts: DKA100: [ENV_ALPHA.QA.W]W128.QAF;6 AVRGEFF (Average Efficiency) 8-MAR-2016 08:22:17 through 9-SEP-2016 12:00: 00 0.252400 through 0.267960 .265 ............ * ........... : ............ * ......................... * ............ * ... . >.. (.) c Q) *r-1 (.) *r-1 4-4-UJ x , 2 6 . . . . . . . . . . . .: . . . . . . . . . . . . . X" . . . . . . . .: . . . . . . . . . . . .: . . X . . . . . . . . .: . . ?<. . . . . . . . . : . . *X* x x '255 . . . . . . o o o 0 o I o 0 o o o I o o 0 I 0 0 o 0 0 I o o o o I o o o o o o o o o o o o o o o o 0 0 0 0 o 0 o o o o o o o o o o o o o I 0 0 o 0 0 0 0 0 0 0 I 0 o . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl"Jent Date/Tifl"le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W128.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:22:17 through 12:00:00 184.000 through 204.000 200 ............................................................................ . . . . . . I o. (!) )-x f-H > H x f-u a: x x w 0 H x x _J x u ::i z 190 o o o o o o ' o o o o ,' o 0 o 0 o ' ' 0 ' 0 0 : o o o ' ' ' o 0 I ' o o' o o o o o o o o o o o .-I o o o I o o o o 0 o o' o 0 o o o o o o I o o o'o I I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA. QA. W]W128. QAF; 6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-201608:22:17 through 9-SEP-2016 12: 00: 00 5. 00000 through 100.000 80 ............ * ........... : ............ * ......................... * ............ * ... . ...... I 0 C). z 0 H 1-::i ....I 0 (j') w O:'. a: w 0... . . . . . . 60 o o o o o o o o o o o 0 0 0 o 0 o o o o o o o o o o o o o o o o o o o 0 0 o o o o o o o o o o o o o o o I I o I o I o I o o I o o o o 0 I 0 0 o I I o o o o o e o I x x x x x x x 40 I I o o o I o I o o I o o o o o o e o o o 0 I o o o 0 I o o o o o o o o o o o o o o I o o o o o o o o I I I o o o I I o I o o o o o o o o o o o o '*I o . . . . . . 20 ........................ ' ........................ ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenafYle ParafYleter NafYle 5tart/End Dates Lower/Upper LfYlts: 3220 DKA100: [ENV_ALPHA.QA.W]W128.QAF;6 P5ENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:22:17 through 9-5EP-2016 12:00: 00 3143. 00 through 3223.00 . . . . . . . 3200 ............................................................................ ro q-..-I I D )-(!:I Ct'. x x x x x x x w 3180 z o o I o o I ............................................................................ . . . . . . w :i:..: <C w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW -QA filenaMe DKA100: [ENV_ALPHA.QA.B]B128.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) . 5tart/End Dates 4-MAR-2016 13:43:22 through 9-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 1 1 0 0 0 0 1 0 0 0 0 1' 0 0 0 0 0 0 0 0 o 0 0 : 0 0 0 0 0 0 0 0 0 ' ' ',' ' ' ' ' ' ' ' ' ' ' '*' ' ' ' ' ' ' ' ' ' ' *, * * *
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o o o *,* o o o .06 . . . . . . ............................................................................ . 04 . . . . . . .02 ............................................................................ . . . . . . 0 ........ __ ___ __....._......___....._....._____.,___.,.._....__ ___ ___..__ ........ 3-16 LOW 4-16 6-16 5-16 7-16 8-16 9-16 MeasureMent Date/TiMe 0 ....., Vi 00 0 \0 QA filenar'le Parar'leter Nar'le Start/End Dates Lower/Upper Lr'lts: DKA100: [ENV_ALPHA.QA.W]W129.QAF;7 AVRGEFF (Average Efficiency) 8-MAR-2016 08:22:21 through 9-SEP-2016 12: 00: 00 0.254891 through 0.270657 . . . . . . . 27 ............................................................................ ::>, (.) c Q) *r-1 (.) *r-1 4-4-LU. Q) "O.(I i'(i Q) > a: .265 x x x x x x '26 x . 255 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .......................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer'lent Date/Tir'le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper.LMts: DKA100: [ENV_ALPHA.QA.W]W129.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:22:21 through 9-SEP-2016 12:00:00 184.000 through 204.000 200 o 0 o 0 o 0 0 o o o ' o o o o o o o o o o o I 0 0 0 I o o o o o o o o o o o 0 0 o 0 0 o o o o o o o o o o I o 0 0 0 o o o o o o o o o o 0 o o 0 0 0 o o I D (!) H > H 1-u a: LLJ D H ...J u z . . . . . . x x x x x x x 190 . . . . . . 0 0 0 0 ,o I I o 0 o o o e o o o o o o o o o I 0 0 0 o I 0 o o O I o o o o o 0 o 0 0 I 0 0 o o o o o o o o o o 0 0 I I 0 0 0 o o o o o o o o 0 0 o I 0 o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA,W]W129.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:22:21 through 9-SEP-2016 12l 00: 00 5.00000 through 100. 000 80 ' ' o o o ' ' o o o ' , o o o I o o o

0 I : o ' ' I o o o o o o o ,'I o o o o o o ' o o o ," o o o o I I o 0 o I 0 , o I I o o o o I I o o'o o o ' T"'I I Cl (!) z 0 H ::i ....I 0 (f) w O:'. . . . . . . 60 ............................................................................ . . . . . . x x x x x . . . x . x 40 ........... * ............ : ........... * ............ * .... * ........ * ... ' ........ *.* .. . 20 ................................................. ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenpMe DKA100: [ENV_ALPHA.QA.W]W129.QAF;7 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 8-MAR-2016 08:22:21 through 9-SEP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . .......................................... ' ................................ . . . . . ID v ..-I I D (!) )-(!) 0:: x x x x x x x LI.I 3180 z . . . o o o 0 o I 0 o o 0 o o o o o o o o o o o o 0 0 o 0 o o o o o o o o o o 0 o o o o o o o o o o 0 I o o o 0 o o o o o o o o 0 ' o o o o o ' o o o o 0 0 o . . . . . . LI.I a: LI.I 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B129.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:43:26 through 9-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 . 08 ............................................................................ . . . . . . .06 . . . . . . o o 0 0 o I I o o o o I o o o o o o o o o I I o O O I I O o O I I o I o o I O o O e O O O I o O I O O O O O O O o I o o O o I I O o O O I o o O o O o o . 04 . . . . . . 02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: . 275 DKA100: [ENV_ALPHA.QA.W]W130.QAF;7 AYRGEFF (Average Efficiency) "8-MAR-2016 08:22:25 through 9-SEP-2016 12:00: 00 0.259030 through 0.275050 . " . 27 O O O O * * * * * * * '* * * * * * * * * * *

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O :>, x (.) c Q) x x x *r-1 (.) :x x *r-1 4-4-lJJ x Q) x "0.0 iti Q) . 265 > . . . . . . o 0 o o 0 o I o o 0 0 0 0 0 0 0 I 0 o o 0 I I 0 0 0 0 o o 0 o I 0 0 0 0 I o 0 0 0 0 0 0 o 0 o I o o o 0 I I o 0 o o I o o o I I 0 0 o o 0 0 0 0 0 I I o . . . . . . a: . 26 3-16_ 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W130.QAF;7 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:22:25-through 9-SEP-2016 12:00:00 184.000 through 204.000 200 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . I D (!) )-I-* H > H x I-u a: x x x w *X D H ....! x x x u ::::i z 19_0 ............ * ........... : ............ * ......................... * ............ * . .' .. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 8-MAR-2016 08:22:25 through 9-SEP-2016 12:00:00 Lower/Upper LMts: 5. 00000 through 100.000 ........ I D (!) z 0 H" 1-::i _J 0 (!) LLJ O:'. :..::: a: LLJ 0... 10_0 80 ............ * ........... : ............ * ......................... * ... ' ........ * ... . . . . . . . 60 ............................................................................ . . . . . . x x x x x x .x x 40 ............................................................................ . . . . . . 20 ........... '* .................................... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W130.QAF;7 ParaMeter NaMe (PEAK ENERGY GD-148) Start/End Dates 8-MAR-2016 08:22:25 through 9-SEP-2016 12:00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 o o I 0 o o I I o o o I I I 0 0 I I 0 0 o 0 I o o o o I o o o o I I o o o o o I o I I I o o I o I o o o o o I o o o I I o o o I I o o o I I o o o o I o o o o I o o co ..,. ....... I D (!) )-(!) x .xx x x x x x UJ 3180 z 0 o I o 0 I I I I o 0 0 0 0 0 0 0 I o 0 o 0 I o o o I I I o o I I I o o o o o o o o o I o o o o I o o o o I o o o o 0 0 I o o I I 0 o o I 0 0 o o 0 I 0 0 0 0 0 I 0 . . . . . . UJ <I: UJ a.. 3160 3-16 4-16 5-16. 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B130.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 13: 43:30 through 9-5EP-2016 12:00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 1 o o o 1 1 o 1 1 1 1 10 1 1 o 1 o o o o 1 1 ' : 1 1 1 ' 1 1 o 1 1 1 1 10 1 1 1 1 1 o 1 1 1 1 1 10 1 1 1 1 1 o 1 1 1 1 ' 10 1 1 1 1 1 1 1 1 1 1 1 '*' 1 1 0 .06 . . . . . . o o o o o 0 o o 0 ' 0 o o o o ' o o o o o o o o o ' 0 o o o o o o o 0 o o I ' o o o o o o o o o o o o o I o o o o o o o o o o 0 o o o o o o o o o o o o .04 .02 ............................................................................ . . . . . . 0 ......... ......... ......... 3-16 LOW 4-16 8-16 9-16 5-16 6-16 7-16 MeasureMent Date/TiMe
-.j:>. 0\ -QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W131.QAF;7 AVRGEFF (Average Efficiency) 8-MAR-2016 08:22:28 through 9-SEP-2016 12: 00: 00 0.250957 through 0.266481 '265 ............ * ........... : ............ * ......................... * ............ * ... . ), 0 c x I]) *n '26 0 I I o o 0 0 0 o o o 0 *' 0 0 0 I 0 o 0 o 0 0 I : o o o 0 o 0 0 I I 0 o o' 0 I 0 o 0 0 0 o 0 o o ," 0 o o o o o o o o o o o0 o o o o o o o o o o 0 o'o I 0 o *n 4-x 4-UJ I]) "0.0 Ill* x x 1, .. : I]) > a: x x x '255 . . . . . . o o o o o o 0 o o 0 I I 0 0 0 0 I o o o 0 I 0 0 0 0 o o o 0 o I o o o o 0 I o 0 0 0 I 0 0 o 0 o I 0 o o 0 o o o o o o o o o o o o o o o o o o o o o o o . . . . . . 3-16 5-16 6-16 7-16 8-16 9-16 _Mea:surer.-.ent Date/ Tir.-.e UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W131.QAF;7 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08:22:28 through 9-SEP-2016 12:00: 00 184.000 through 204.000 20-0 . *-......... * ............ : ........... * ............ * ............ * ............ *.* .. . I 0 (!) )-1-H > H 1-u a: w 0 H _J" u =r z x x x x x x x 190 ' o o o o ' o o o 0 0 ,* o o o ' o o o o o ' o : o o o o o o o ' ' o 0 o' I o o o o o o o o 0 0 .-I o o o I o o 0 o I o o' o o o o o 0 o o o o o o'o o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.ete_r Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W131.QAF;7 PSFWHM-80148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:22:28 through 9-SEP-2016 12:00: 00 5.00000 through 100.000 80 ............ * ........... : ............ * ......................... * ............ * ... . ...i I D CJ z 0 H :::::i ...J 0 (!) L1J Cl:'. 60 . . . . . . .............................................................. ' ............ . . . . . . . x x x x x x x :::.:: a: 40 ...... ' .................................................................... . L1J 0.. . . . . . . 20 ........... '* ....................... " ........... ' ........... " ........... '*' .. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,W]W131.QAF;7 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Oates 8-MAR-2016 08:22: 28 through 9-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 o o 0 0 o I ............................................................................ . . co . ..,,. ..-I I D (!) >-(!) er: x x x x x x x LL.I 3180 z . . . . . ............................................................................ . . . . . ' LL.I ::..::: a: LL.I 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:23: 28 through 9-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' * ' 0 0 ' 0 0 0 ' 00 0 0 0 ' ' 0 0 0 0 ' ' : 0 0 ' 0 0 0 0 0 o 0 0 '*' 0 0 0 0 0 0 0 0 0 0 '. 0 0 0 0 0 0 0 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 ',' 0 0 0 . . . . . . . 06 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 0 o I o 0 o 0 I 0 o o o o o o o o o o o 0 o I 0 o o o I o o o o o o o o o o o o o o o o 0 0 . 04 . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W132.QAF;6 AVRGEFF (Average Efficiency) 8-MAR-2016 08:22:33 through 9-SEP-2016 12: 00: 00 0.253891 through 0.269595 . . . . 265 ............................................................................ . . . . . . :::>, (.) c Q) *r-1 (.) *r-1 4-x x 4-LJ.J Q) "0.0 ((j x x x x . 26 Q) ........................ : ........................ ". *x* .................... *.* .. . > a: . . . . . . . 255 o o o o o o o o o o o I o o 0 I I 0 o 0 0 0 ' o o o ' o o o o o o o 0 o I 0 O o O O o o o o o o o o o o o I o O O I O o o O o o o o o o o o o o o ' o O . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W132.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 D8:22:33 through 9-SEP-2016 12:00:00 184.000 through 204.000 200 ........... * ............ : ........... * ............ * ............ * ............ *.* .. . I 0 (!) )-I-H > H I-x u cr: w x x 0 x x H ....I x u =i x z 190 0 o e e 0 0 o o e o 0 o' o ' ' o o o o o o o o : o o o o o o o o o ' o o' o o 0 o e' I o o e o ," o e o o o I o o o 0 o o' o o o o o o o o 0 o o o'o 0 0 o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W132.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:22:33 through 9-SEP-2016 12:00:00 5.00000 through 100.000 . . . . . . 80 0 I o o o o I o ' o I o o o o o o o o ' o o ' o o o o o o o o o o o o o o o o o o o ' o o o o o o o o o 0 0 o o o I o o o o o o o o o o o o o o o o o o .-1 I D z 0 H 1-::i ...J. 0 (!') lJ.J a: . . . . . . 60 I I o o 0 I I o 0 o I 0 o 0 I o I 0 0 o 0 I o o 0 0 0 o o o 0 I o o o o o o I o o o o o o o o o o o o o o o o o o o ' o o o o o o o o o 0 o 0 o o I 0 o . . . . . . x x x x x x x 40 0 0 o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o o o o 0 o o o o o 0 I o 0 0 0 I I o 0 o 0 I o o 0 o o o o o o o o o o o o o o . . . . . . 20 ........... '* .................................... ' ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W132.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:22:33 through 9-SEP-2016 12: 00: 00 3143.00 through 3223.00 . . . . . . 3200 o o o o o I o o o o o o o 0 o o 0 o o o o o o o 0 0 o o o o o o o o o o o o o o o 0 I o o o I o o o o I* o o o o o o o o o 0 o I o o o o ' I o o o o o o . . . co """ -n I D (!) )-(!) et:: x x x x x x x w 3180 z . . . ' o o o o I I I I 0 o o o o o o o I I o o o o o o o I o o o o I I o o o o o I o o o o o o o o o o o o o I o 0 o o I 0 0 I o I o o o I o o o I o o 0 I 0 . . . . . . w ::..::: a: w 0.. 3160 . . . . . . . . . . . .. . . . . . . . . . . . . *' . . . . . . . . . . .. . . . . . . . . . . . -. . . . . . . . . . . .. . . . . . . . . . . . . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B132.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:23:31 through 9-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 o ' o o o ' O o o o 1 ', o o o 1 1 o o o o 1 I : o O I I O o O I I O o ',I I o o o o 1 o o o o ', 1 o o o 1 1 o O o I I o, O O O o O o o o o o o ',' o I o . . . . . . . 06 ............................................................................ . . . . . . 04 . . . . 02 ........... * ............ : ........... * ............ : ........... * ............ *.* .. . 0 3-16 4-16 x x x *x x x x x x 5-16 6-16 7-16 MeasureMent Date/TiMe x x* x x x x x 8-16 9-16 UP LOW -.j:>. -..J -0 >-+, Vl 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: '26 ::>, DKA100: [ENV_ALPHA.QA.W]W133.QAF;6 AVRGEFF (Average Efficiency) 8-MAR-2016 08:22:37 through 9-SEP-2016 12:00:00 0.245373 through 0.260550 (.) '255 c . . . . . . x ........... *:* .......... ; .. X* ....... *: ........... *: ........... *:* .......... *:* .. . ID *ri (.) x *ri 4-4-UJ x x x ID '0.0 ((i x I-ID > a: .25 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... -..J N 0 ......, VI 00 0 \0 QA filenaMe ParaMeter Narrie Start/End Dates Lqwer/Upper Lrrits: DKA100: [ENV_ALPHA.QA,W]W133.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 8-MAR-2016 08: 22:37 through 9-SEP-2016 12:00:00 184.000 through 204. 000 200 ........... " ........... : ........... " ........... " ........... " ........... *.* .. . I D )-I-x H > H I-(....) a: x x x x w D H _J (....) x x ::i z. 190 . . . . . . ..... ' ..................................................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 8-MAR-2016 08:22: 37 through 9-SEP-2016 12:00: 00 5.00000 through 100. 000 80 ............ * ........... : ............ * ......................... * ............ * ... . -M I Cl (!)* z D H 1-::i _J D (f) Ll.J O:'. ::..: a: Ll.J 0.. . . . . . . 60 o o o o o o o o o o o o o o o o o o o 0 o I o o o 0 0 0 o o o 0 o o I o o I o o o o o o o o o o o o o o 0 I 0 o e I ' o o o I o o o o o ' o o o o ' o o . . . . . . x x 40 . . x . . . . . . . . .: . . . . . . . . . . . . . ,.,., . . . . . . .. : . . . . . . . . . . .: . . . . . . . . . . . _: . . ?<. . . . . . . .. : . . . .
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20 ...... ' .......................................... ' ........... '* ................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e up* LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W133.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 8-MAR-2016 08:22:37 through 9-SEP-2016 12:00:00 3143. 00 through 3223. 00 . ;, . . . . 3200 ........................................................... ' ................ . . . . . . co v "<"i I o* )-c:: x x x x x x x LU 3180 z . . ., . . . o o 0 o o I I o o o I I o o o o 0 o o o ' I 0 o o o I o o o o o I o o o I o o o o o I o o o 0 0 0 o 0 o I I o o o I o o o o 0 0 o o o o I o 0 o o 0 I 0 . . . . . . LU ::...::: ([ LU 0... 3160 ................................................. -.. *.* ......................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B133.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:43:43 through 9-SEP-2016 12: 00: 00 Lower/Upper LM£s: O.OOOOOOE+OO through 0.100000 I 08 0 I ** 0 0 I

o o o ', o o o o o o I I 0 0 I : o o o o o o o o o o o 1, I I o o o o o o o o o 1, 0 o o o 0 I I I o I I 1, 0 0 0 I o 0 0 0 o Io 0,0 I o o . . . . . . '0-6 I 0 I I o o o o o I o o o I 0 I 0 0 0 o I o I o o o o o o o o I o o o o o o o o o o I o o o o I I o o o o I I I o I I O o O o I IO I I I O o O O O o I '04 . . . . . I 02 ° 0 0 0 0 *

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0 0 3-16 4-16 5-16 6-16 7-16 9-16 MeasureMe.nt Date/TiMe UP LOU.I QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: >.. (.) c ID *r-1 (.) *r-1 4-4-UJ . 26 x x x DKA100: [ENV_ALPHA.QA.W]W134.QAF;6 AVRGEFF (Average Efficiency) 7-JUL-2016 14:05:23 through 9-5EP-2016 12: 00:00 0.249513 through 0.264950 x x . . . . . . . . . . 255 ...... ' .................................................................... . . . . . . . . . . . I 25 ° 0 0 0 0 ' 0 00 0 0 0 0 0 0 0 ',' 0 0 0 0 0 0 0 ,' 0 0 0 0 0 0 0 : 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 01 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 : 0 0 0 0 0 0 0 00 0 0 7-07 7-14 7-21 7-28 8-04 8-11 8-18 8-25 9-01 9-08 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENY_ALPHA.QA.W]W134.QAF;6 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 7-JUL-2016 14: 05:23 through 9-SEP-2016 12: 00: 00 184. 000 through 204. 000 200 ................ *.* ................ : ................ " .. _ ....... * ....... .' ....... '. .. I 0 (!) )-f-H > H f-u a: w 0 H ....I u ::i z xx x x x 190 . . . . . . . .* . . . . . . . . . . . . . . . . . *. . . . . . . . : . . . . . . . .. . . . . . . . . . . . . . . . . . . . . . . . . . . *. . . . . . . . .. .. 7-07 7-14 7-21 7-28 8-04 8-11 8-18 8-25 9-01 9-08 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W134.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 7-JUL-2016 14:05:23 through 9-SEP-2016 12:00: 00 5.00000 through 100.000 ..-1 I Cl C) z 0 H 1-:J ....I 0 Cf) LU Ct'. a: LU 0... 100 80 ........ * ........ * ........ * ........ : ................. * ........ * ........ * ........... . . . . . . . . . . 60 0 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o o o o 0 o 0 I 0 o o I I 0 o o 0 I 0 o o o I 0 I o o I o o o o o o o . . . . . . . . . *X 40 I I o o o o o o o o o o o o o o o o o o o o o o o o o o e o o o o o o o o o o o o o o o o o o o o o o o o I o 0 o o o o 0 o 0 I 0 0 o 0 I 0 o o o I I o . . . . . . . . . 2 0 ........................................... ' ....... '* ................. , ....... ' .. 7-07 7-14 7-21 7-28 8-04 8-11 8-18 8-25 9-01 9-08 MeasureMent Date/TiMe UP LOW QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 7-JUL-2016 14:05:23 through 9-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . . . . 3200 o o o o o o I ' o o I I o o o o o o o o o I o o o o 0 o 0 o o o o o o o o o o o o o I o o o o I 0 o o o o o o o o o o o o o o o o 0 o o o o 0 o o o o o . . . . . . co """" ...i I D (!:I )-(!:I et:: xx LLJ 3180 z . . . . . . . . . o o o o o o I 0 o o o o o o o 0 I o o o o o o o o 0 I 0 o o o o o o o o o o o o o 0 I o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o 0 o I o o . . . . . . . . . LLJ :..::: a: LLJ 0... 3160 7-07 7-14 7-21 7-28 8-04 8-11 8-18 8-25 9-01 9-08 Measurerrrent Date/Tirrre UP LOW
....... .j::.. 00 0 0 ......, Vl 00 0 \0 QA filename DKA100: [ENV_ALPHA.QA.B]B134.QAF;2 Parameter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:43: 47 through 9-SEP-2016 12: 00:00 Lower/Upper Lmts: O.OOOOOOE+OO through 0.100000 . 08 0 ' o 0 o o o o o o o ' o o o o o o o o o o o o 0 o o o o o o o o o o o 0 0 o 0 o 0 o o o o o o o o o o o 0 o 0
I I 0 0 o o o o o o o o o o o o 0 0 o . . . . . . . 06 . . . . . . ............................................................................. . . . 04 . . .02 ............................................................................ . . . . . . 0 x x x 3-16 x x x x x x x x *x x 4-16 5-16 6-16 Measurement Date/Time UP LOW
-.j:::.. 00 QA filenal'te Paral'le ter Nal'te 5tart/End Dates Lower/Upper Ll'lts: .255 :>, u c IJ.) *r-1 u *r-1 4-4-LLJ* IJ.) "OIJ l(i S-IJ.) x DKA100: [ENV_ALPHA.QA.W]W139.QAF;6 AVRGEFF (Average Efficiency) 9-MAR-2016 08: 43:08 through 10-5EP-2016 12:00:00 0.244640 through 0.259770 x x . . . . . . > . 25 ............................................................................ a: . . . . . . x x x x . 245 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'tent Date/Til'te UP LOU.I ....... +>-00 N 0 >-+, Vl 00 0 \0 QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W139.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:43: 08 through 10-SEP-2016 12: 00: 00 184. 000 through 204.000 200 ' ' ' ' o ' o 0 o o o o o o o o o o o o o o o o o 0 o I 0 o o o o o o o I I o o o o I 0 o I o I o o o-o o I o ' o I I 0 o o I o o o o o I o o o o 0 I ' . . . . . . I 0 (!:I >-I-H > H I-u a: Ll.J x 0 H _J u x x ::i z 190 * * * * * * * * * * * .: . . . . . . . . . . . :. . . *x . . . . . . . -: . . >!. . . . . . . . . . . . . . . . . . . . '. . . x. . . . . . . . .: . . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LfY'lts: 100 DKA100: [ENV_ALPHA.QA.W]W139.QAF;6 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08: 43:08 through 10-SEP-2016 12:00:00 5.00000 through 100.000 . . . . . . 80 .................................................... ' ...................... . I 0 z 0 H =:i ....I 0 en LLJ O:'. :::..:: a: LLJ 0... . . . . . . 60 ............................................................................ . . . . . . x x x x x .x x 40 ............................................................................ . . . . . . 20 ° 0 0 0 0 0 1 0 0 0 0 ._ 0 0 0 0 0 0 0 0 0 0 0 .. 0 0 0 0 0 0 0 0 0 0 0 ._ 0 0 0 0 0 0 0 0 0 1 0 ,/ 0 0 0 0 1 0 0 0 0 1 0 I 0 0 0 1 0 0 0 0 0 0 0 .. 0 0 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/TifY'le UP LOW ....... ..j::. 00 ..j::. 0 ......., VI 00 0 \0 QA f i lenal'le . Paral'leter Narrie Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W139.QAF;6 PSENERGY-GD148 (PEAK ENERGY GD-148) 9-MAR-2016 08:43:08 through 10-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ............................................................................ . . . co """ "<"""I I D (.!) )-x x (.!) O:'. x x x x x . . . . . . o 0 o o o I o o
o o .. o o o I o o o o o I I : o o I I o o o o o o o ', I I o ' o ' o ' o o o : I o o o I I o o o I I : ' o I ' o ' o o o o o ', o o o o Ll...I 3180 z Ll...I ;:,..:: <r: Ll...I CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
....... 00 Vl 0 ......, Vl 00 0 ID QA filenarrie Pararrie te_r Narrie Start/End Dates Lawer/Upper Lrrits: DKA100: [ENV_ALPHA. QA, B]B139. QAF; 3 BACKRATE (Background Rate) 4-MAR-2016 12:35:59 through 10-SEP-2016 12: 00:00 O.OOOOOOE+OO through 0.100000 . 08 0 I o 0 * ' o o o o ' ' o o o ' ' o o o o o o o o o I 0 I o o 0 o o o o o o 0 o o o o e o I o o o o o o o o o o o o o o o o o o o o o o o o o e o o o o . . . . . . . . . . . . . 06 o o o o o 0 0 0 o 0 I I o o o o o o o o o o o o o o I o o o o 0 o o o o I o 0 o o o I o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o '04 . . . . '02 ............ -......................................... -.................... . -o 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Oate/Tirrie UP LOW QA filenafY'le ParafY'leter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ ENV_ALPHA. QA. W] W140. QAF; 3 AVRGEFF (Average Efficiency) 9-MAR-2016 08:43:14 through 10-SEP-2016 12:00:00 0.254850 through 0.270613 . 27 0 0 0 , 0 0 0 0 0 0 0 ," o 0 o o , o o o o o o 'o o o o o o o , I o o o .. o o o o o o o o o o O ', o o o o o o o o o o o : o o I I o 0 I o o o o .. o I I o :>i u c Q) *r-i u *r-i 4-4-LU . 265 x x . . . . . . x . 26 ........... '. ... x* ...... '. .. *X ....... '. ........... '. ........... : ........... '. ... . x x I 255 ° 0 0 0 0 1 0 0 0 0 0 0 0 0 1 0 0 0 0
0 1 0 0 0 1 0 0 0 1 0 0 0 ' 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 3-16-4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W140.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:43:14 through 10-SEP-2016 12: 00: 00 184. 000 through 204. 000 200 o ' o

o o ' * * * ' o o o o o I e o o o o 0 0 0 o 0 o o o o o o o o o o o o o 0 o o o o o o o o o o

0 I o I o 0 I o o o I I o o o o 0 o o o 0 o o o . . . . . . I Cl (!) )-. I-H > H I-u a: x x w Cl x H _J u x x x x :=i z 190 . . . . . . o o o o o o o o o o o o o o o o 0 o o o o o I o 0 o 0 o o o o o o o o o o o 0 o o 0 I o o o e o o o e o o 0 o 0 o I o o o o o o o o o o 0 o 0 o o I 0 o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW
...... +:>. 00 00 0 ....., Vt 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W140.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08: 43:14 through 10-SEP-2016 12:00:00 5. 00000 through 100.000 . . . . . . 80 ............................................................................ ..-t I Cl z O* H 1-::a _J a (/) l.J..J O:'. a: l.J..J 0.. . . . . . . 60 ............................................................................ . . . . . . x x x x x x x 40 ..... ' ......................... ' ' ............... ' .......................... . . . . . . . 20 o o o o o ' o o
o ' ... o o o o o

o o o I ',/' o o I ' o o o I I o o .. o o o o o o ' o o o o ,/' o o o o ' ' o o o ' ' I o o ' ' o o o o ' o ' .. o ' ' o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-.j::>. 00 \0 0 ....., Vl 00 0 \0 QA filenarrle Pararrie ter Narrie Start/End Dates Lower/Upper Lrrlts: 3220 DKA100: [ENV_ALPHA.QA.W]W140.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 9-MAR-2016 08: 43:14 through 10-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 O O o O o I I o O o O O O o o O o o o o o o o o o o I o o o o o o o o o o o o o o o I 0 o o o 0 I o o o I I o o o I I 0 o o o I o o o o o o o o o I I I . . ro v ..-l I 0 C) )-C) 0::: x x x x x x x LLJ 3180 z . . . . . . . . . . . . . . . . *. *. . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . .. : . . . . . . . . . . . : . . ' . . . . . . . . *. . . . . LLJ :...::: a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B140.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 12:36: 04 through 10-5EP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 I I 1 I I ' I I I I I 11 I I I I I I I I I I I .. I I I I I 1 o o o o O 11 I o o o o o o o o I I 1o o o o o 1 I o o o I I : o o , 1 1 1 1 O I 1 1 00 1 1 0 1 . . . . . . . 06 .......................................................................... ' . . . . . . 04 . . . . '02 ............................................................................ 0 x x 3-16 . . . . . . x x x 6-16 MeasureMent Date/TiMe x *x 9-16 UP LOliJ 0 Hi Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W142.QAF;5 AVRGEFF (Average Efficiency) 24-AUG-201614:10:42 through 10-SEP-2016 12:00:00 0.258101 through 0.274067 . . . . . . . . 27 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 I o 0 o o o o o o o o o o o o o o o o o o o o o o o o o (..) c (!) *r-i (..) *r-i 4-4-UJ (!) "O.ll. iO 1--(!) > a: x x x . . . . . . . . x , x . 265 .... *x* *:* ....... *:* ....... : ....... *:* ....... *:* ....... : ....... *:* ....... *:* ..... . ' 2"6 . *-............................................................................... . 8-24 8-26 8-28 8-30 9-01 9-03 9-05 9-07 9-09 MeasureMent Date/TiMe UP LOW -.j::.. \0 N 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/End OateB Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W142.QAF;5 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 24-AUG-2016 14:10:42 through 10-5EP-2016 12: 00:00 184.000 through 204.000 200 ............................................................................ . . . . . . . . I D (!) )-I-H > H I-u a: x Ll.J D x H-_J x u ::i xx z 190 . . . . . . . . ............................................................................ x 8-24 8-26 8-28 8-30 9-01 9-03 9-05 9-07 9-09 MeaBureMent Date/TiMe UP LOW ...... +:>. \0 w 0 ......, VI 00 0 \0 QA filenarrie Pararrieter NafYte Start/End Dates Lower/Upper Lrrits: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTiON GD-148) 24-AUG-2016 14:10:42 through 10-SEP-2016 12:00: 00 5.00000 through 100. 000 80 ........ * ......... * ........ : ........ * ......... * ........ : ........ * ......... * ...... . ..-! I D C) z 0 H 1-::J _J 0 (f) w O:'. ::..::: a: w 0.. x . . . . . . . . 60 .. ..... *:*** ..... : ....... *:** ...... *:*** .... *: ....... *>**. *****:*x** .. . . . . . . 40 ............................................................... ' ........... . . . . . . . . . 20 ........ *' ....... '* .......................... '* .................................. . 8-24 8-26 8-28 8-30 9-01 9-03 9-05 9-07 9-09 MeasurefYlent Date/Tirrie UP LOW QA filenafY'le ParaMe ter NafY'le Start/ End Da-tes Lower/Upper LfY'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W142.QAF;5 P5ENERGY-GD148 (PEAK ENERGY GD-148) 24-AUG-2016 14:10:42 through 10-SEP-2016 12: 00: 00 3143. 00 through 3223. 00 o 0 o o o o o I 3200 ............... ' ........................................................... . . . co ""'" """"' I 0 (.') )-(.') a::: x )Ol( x x w 3180 z o o o I I I I o I o I I o o o I I I o I I I o o o o I o o I o o o o o I o I ' o o I I I o I o o o I I o o I o o o o o I o I o I o o 0 o I o o o I o o I I 0 o I I I . . . . . . . . w :::..,: <C w a.. 3160 8-24 8-26 8-28 8-30 9-01 9-03 9-05 9-07 9-09 MeasurefY'lent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B142.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 12:36:13 through 10-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' ' 0 0 ' o o o o ' ', o ' ' ' ' ' ' ' ' ' o .. ' ' ' o o o ' ' o ' ' ', ' ' ' o o ' ' o o o o .' ' ' o o ' ' o o o ' ' : o o o 1 o o o o 1 o o ', o 1 1 o .06 . . . . . . o o o o o o o o o o o o o o o o 0 o o o o I 0 o 0 ' 0 0 o o o o o o o o o o o o o o I 0 o o e o o o o o o o o 0 o 0 0 o o o o o o o o o o o o o o o o o .04 . . .02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent -.j::.. \0 0\ 0 ......, VI 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: .235 (..) c 11)-*.-i (..) *.-i 4-4-UJ ID -0.0 f(i x I-ID > a: ' .*. :. I! .... ,, . ';* DKA100: [ENV_ALPHA.QA,W]W143.QAF;4 AVRGEFF (Average Efficiency) 9-MAR-2016 08: 43:32 through 10-5EP-2016 12:00:00 0.225440 through x x x . 23 ' . --. . . . -. . : .. -. . -. . . . . -. . . . . . . . . . : . . -. . . . . . .. : . . )( . . --. . . : --. . . . . . . .. : . . .. x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W143.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:43:32 through 10-SEP-2016 12: 00: 00 184.000 through 204. 000 200 ........... * ......................... * ......................... : ........... * .. : .. I 0 (!) )-I-H > H I-u a: x x x w 0 H x x -I u ::i z x x 190 . . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . . .. . . . . . . . . . . . *, . . . . . . . . . . ' : . . . . . . . . . ... * . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW -.+::-. \0 00 0 ......, Vl 00 0 \0 QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W143.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08: 43:32 through 10-SEP-2016 12:00:00 6.00000 through 100. 000 -M I Cl (!) z 0 H 1-::i ....I 0 (.{) w Ct'. ::..::: a: w 0... 100 80 ' o ' ' o o ' o o o ' .-o o o 0 o ' o o o o o ', o o o * ' o o o o o o .. o o o ' o o o o o o o ', o " o o o o o o o o o : ' o o o o o o o o o o .. o I o o . . . . . . 60 ........... " ... x' ...... : ........... * ............ : ........... : .. x* ....... ". * .. . .X . . X . . X . . X x 40 o I o o o o o o o o o o o o o I I o o o o I o o o 0 o I o o o I I o o o o o o o o o ' o 0 o e I I o o o o ' 0 o o o 0 o o o o o o o o 0 I 0 o e o o o o . . . . . . 20 I o o o o ' I o ' o ' .. o o o ' ' o o o o o 'I' o o ' ' o o o ' o o o "o o ' ' o o o ' o o o o I' ' o o o o ' o o o o o I o o o ' o o o o I o o .. o ' o o 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurement Date/Tirrre UP LOW QA filenarrre Pararrreter Narrre 5tart/ End D-ates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W143.QAF;4 P5ENERGY-GD148 (PEAK ENERGY GD-148) 9-MAR-2016 08:43:32 through 10-5EP-2016 12: 00:00 3143. 00 through 3223.00 . . . . . . 3200 0 I ' ' 0 o ' ' ' ' ' ' o ' o ' ' o o ' o o ' o ' ' o o o o ' ' o o o o o 0 o o o o o o o o o o o o o 0 0 0 0 o o o o o o o o ' o o o o o o o '0 0 0 o co q-...-! I D (!) )-(!) 0::: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ ::..::: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW -Ul 0 0 0 ......, Ul 00 0 "° QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-201612:36:17 through 10-SEP-2016 12: 00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 ' 0-S . '* ......... * ......................... * ......................... : ........... " ... . '06 . . . . . . . . . . . ; . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . .. : . . . . '04 . . . . 02 ............................................................................ . . . . . . 0 x x 3-16 4-16 5-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... Vl 0 ...... 0 ......, Vl 00 0 ID QA filenal'le Paral'teter NaMe Start/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 9-JUL-2016 09:35:58 through 10-SEP-2016 12:00: 00 0.253789 through 0.269487 '265 . . . . . . . .* . . . . . . . . *. . . . . . . . .. . . . . . . . . . . . . . . . .. *. . . . . . . . .' . . . . . . . . . . . . . . . . . *. . . . . . . . .* . x (.) c Q) *r-1 x: (.) *r-1 4-4-x UJ x Q) '0.0 x ((i I-'2-6 Q) . . . . . . . . . o o o o 0 0 I o o o o o o o o o I o o o o o o o o o o 0 o o o o o o o o o I o o o o I 0 0 o o o o o o 0 I o o o o o I 0 o o o o o o o o I o 0 o o o o 0 > a: '255 UP 7-09 7-16 7-23 7-30 8-06 8-13 8-20 8-27 9-03 9-1G LOW MeasureMent Date/TiMe ...... Ul 0 N 0 ....., Ul 00 0 \0 QA filenafYle Pararrieter NafYle Start/ End Da_tes Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W144.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-JUL-2016 09:36:58 through 10-SEP-2016 12:00:00 184.000 through 204.000 200 0 0 o 0 0 ' 0 o o o o o o o o o 0 o o o o o I o o o I I o o o I I o o 0 I o I o o o I o o 0 0 0 0 o o o I I o o o I 0 o o 0 ' o o o o o o o o o o o I 0 . . . . . . . . . I Cl >-I-H > H I-x u <J: w x. Cl H _J u :J z xx 190 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ' ................... ' ................................ . x UP 7-09 7-16 7-23 7-30 8-06 8-13 8-20 8-27 9-03 9-1G LOW MeasureMent Date/TiMe -VI 0 (.;.) 0 H) VI 00 0 \0 QA filenafY'le ParafY'leter NafY'le Start/End Dates Lower/Upper Lmts: 100 DKA100: [ENV_ALPHA.QA.W]W144.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-JUL-2016 09:35:58 through 10-SEP-2016 12:00:00 5. 00000 through 100.000 80 ........ * ........ * .................. * ........ * .................. * ........ * ......... *. ..-! I D z 0 H ...J 0 (j) LLJ Q'. ::.:: a: LLJ (I... . . . . . . . . . . 60 ....... * ........................... *.* ................ " ....... *.* ............... *x*. x x xx . . . . . 40 ......................................................... ' ................. . . . . . . . . . . 20 .......................... ' ................. ' ....... ' ................. ' ......... . UP 7-09 7-16 7-23 7-30 8-06 8-13 8-20 8-27 9-03 9-1G LOW MeasurefY'lent Date/TifY'le -Vl 0 0 ......., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W144.QAF;3 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 9-JUL-2016 09:35:58 through 10-5EP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . . . . ............................................................................ co .,-I I D (!) )-(!) ct: x xx x: LLJ 3180 z . . . . . . . . . o o o o o I 0 o o
0 I o o o o o o o o o o o o o o o o 0 O O o I o o o o o o o o o o o o o o o I o o o o o o o o o o o o o I I o o o o o o o o o o o o . . . . . . . . . LLJ a: LLJ Cl.. 3160 7-09 7-16 7-23 7-30 8-06 8-13 8-20 8-27 9-03 9-1G LOW MeasureMent Date/TiMe
....... Vl 0 Vl 0 ,....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B144.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Date8 4-MAR-2016 12:36:22 through 10-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' '
0 0 ' '

0 * ' '. * * * ' 0 0

0 0 ' '." 0 ' ' ' 0 0 ' ' ' ' 0 '*' 1 0 0 ' ' ' ' ' ' '.' ' ' ' ' ' ' ' ' ' ' ' ! ' ' ' ' ' ' * * * *, * * * * . 06 . . . . . . o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ' o o o o I o O o O I o O o o o o o o o o o o o o o o o o o I I 0 o 0 0 I 0 o o 0 0 I o . 04 '02 ............................................................................ -. . . . . 0 ._._..__""-'-___._..__.._.__,_.__.._._ .......... .......... 3-16 4-16 5-16' 6-16 7-16 8-16 9-16 Mea8ureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: >, (..) c Q) *ri (..) *ri 4-" 4-UJ '265 '26 x '255 3-16 DKA100: [ENV_ALPHA.QA.W]W145.QAF;7 AVRGEFF (Average Efficiency) 9-MAR-2016 14:48: 03 through 10-5EP-2016 12: 00:00 0.252879 through 0. 268521 x x x x 4-16 5-16 6-16 7-16 Measurerrient Date/Tirrie UP x x 8-16 9-16 LOW
..... Vl 0 -..J 0 ......, Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W145.QAF;7 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 14:48: 03 through 10-SEP-2016 12:00:00 184.000 through 204.000 200 ........... * ......................... * ......................... : ........... * .... . I D (!) )-f-H > H f-u a: w x D H x _J u ::i z x x x x 190 ........................ * ......................... * ............ : ................ . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ...... Vl 0 00 0 ....., Vl 00 0 "° QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W145.QAF;7 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 14:48:03 through 10-SEP-2016 12: 00:00 5.00000 through 100.000 x x x x 80 * * * * * * * * * * * *: * * * * * * * * * * * :* * * * * * * * * * * * *: * * * * * * * * * * *: * * * * * * * * * * *: *
x* * * * * * * * *: * * * * ...i I D x z 0 H 1-::i _J 0 (() w O:'. ::..::: a: w Q.. . . . . . . 60 .......................... ' ................................................ . . . . . . . x . . . 40 o o o o o o o o 0 o 0 o o o o o o o o o o I 0 o o o o o o o o o I 0 o o I o o o o o I

0 o o o o o o o o 0 o o o o o o o o t I O o o o o o o o o o o o . . . . . . 20 ' o o o o ' I o o o ' .. o o o ' o o o o o ' o ,/' o o ' ' o ' o I o o o .. ' ' o o o o I o o o o ,/' ' o o o o o o o o o ' I o o I ' o o o o ' o o .. o ' o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16. Measure!Y'lent Date/Ti!Y'le UP LOW
-Vl 0 \0 0 ,...., Vl 00 0 \0 QA filenaMe DKAioo: [ENV_ALPHA.QA.W]W145.QAF;7 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 9-MAR-2016 14: 48:03 through 10-5EP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . ............................................................................ CD ""'" I D (!) )-(!) 0::: x x x x x LLJ 3180 z w ............ : ........... : ............. : .. x ........ : ............ ............ : ... . x :..::* a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ....... Vl ....... 0 0 ....., Vl 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B145.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:36:25 through 10-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 . 08 ............................................................................ . . . . . . . 06 . . . . . . . . . . ' : . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . ' .. : . . .. . 04 . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 ....., Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper DKA100: [ENV_ALPHA.QA.W]W146.QAF;5 AVRGEFF (Average Efficiency) 9-MAR-2016 08:43:50 through 10-5EP-2016 12: 00:00 0.250993 through 0.266519 . . . . . . .265 ............................... ' ............... ' ........................... . ::;..; 0 c Q) *r-1 . 26 0 . . . . . . ............................................................................ *r-1 4-4-LU x Q) WJ x l'O Q) > a: x x x . 255 ........... *: ........... :* ........... *: ........... :* ........... : ........... *:., *x* x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW -Vi -N 0 ......, Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W146.QAF;5 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08: 43:50 through 10-SEP-2016 12:00:00 184.000 through 204.000 200 I o
I o 0 ' o ' o o 0 o o ' 0 0 ' o o o o o o 0 o I o 0 o o o I o o 0 o o o o o I o o o o o o I o o o o o o o I o t o o o o o o o o o o o o o o o' o o . . . . . . I D )-I-H > H I-u a: w D x x H ....I u :) x x x x z 190 . . . . . . ................................................ ' .......................... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-!.Ji -!.;.) 0 ....., !.Ji 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W146.QAF;5 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08:43:50 through 10-SEP-2016 12:00:00 5.00000 through 100.000 80 . . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . . .. . . . . . . . .... *. . . . . . . . . . . . : . . . . . . . . . . . .. . . .. ...... I CJ z 0 H 1-::J ...J 0 (f) w 0::: ::.::: a: w 0.. x x x x x x x . . . . . . 60 I 0 o o 0 I I o I o 0 I o o o O o o o o o O o o o I I o o o o o o o o o o o o o o o O o o I o I o o o o o o o o e o o o o O I o o o o o o o o o o o o o . . . . . . . . . . 40 ............................................................................ . . . . . . 20 ' I o o o o o o o o ' .. ' o o ' ' o o o o ' o" o ' ' o o o o o I o ' .. o I o o o o ' o o o o" o ' o o I ' o o o ' o I o o ' ' I o o o ' o o .. o ' I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 9-MAR-2016 08:43:50 through 10-SEP-2016 12: 00: 00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . . ............................................................................ . . ro ""'" ..-I I D (!) )-(!) Ct:: x x x x x x x LLl 3180 z . . . . . . ............................................................................ . . . . . . LLl )o.:; <r: LLl 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ....... Vi ....... Vi 0 ....., Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B146.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:36:29 through 10-SEP-2016 12: 00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 . 08 ........... ' ........................................................ ' ...... . . . . . . . . . 06 . . . . . . I o o o o 0 o ' o o o o o o o o o o o o 0 0 I o o o I I o o o 0 I o o o o o o o 0 o 0 o o o o o I o o o ' o o o 0 I I o
o o o o o o o I o o o o o o o . 04 . . . . . . . 02 ................. -........... -.................... -........................ . . . . . . . 0 x 3-16 x x 4-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper LMts: .26 ::., u c Q) *r-1 u *r-1 4-4-x LU Q) "Of! iO DKA100: [ENV_ALPHA.QA.W]W147.QAF;4 AVRGEFF (Average Efficiency) 9-MAR-2016 08:43:57 through 10-SEP-2016 12:00:00 0.248902 through 0.264298 x x x x . 255 o o o o o o o

o o o ," o o o o o o e o o o o *, o o 0 o o o o o o o o .-I 0 o o o o o o o o o 0o I o o o o o o o o o I : o o o o o o o o o 'o o' o o o o Q) > .x a: x . . . . . . . 25 o o e o o O O e o o o o o o o o o o o o o I I o o o o o o o o o o O o O I o o o o o o o o 0 e I I o o o o o o o o o 0 o o 0 ' o o o o o o o o 0 0 o I o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-Ul --..J 0 ....... Ul 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W147.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:43:57 through 10-SEP-2016 12:00:00 184.000 through 204.000 200 ' 0 * *
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0 I o o o o I I o o o o o I o o e o I o o o I I o O e O O O o o o o o o o o I O O O o I I o O o I I o o o I I O O o O O O o o o I o o . . . . . . I D (!) >-f-H > H f-u a: x LL.I D .x x x H ....I x u =i z x 190 0 I 0 ' 0 I I 0 0 o I o' 0 0 o I I o o o 0 0 I 00 0 0 I I o o O I I o O .. o I e o o o I o o o o 0o o o O o 1 I O o o I I : o o o O o o e o 1 o o : o 1 1 o x .. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/ TiMe* UP LOW
....... Vi ....... 00 0 H') Vi 00 0 "° QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W147.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08:43: 57 through 10-SEP-2016 12:00: 00 5.00000 through 100.000 ...... I 0 C) z 0 H ::i ....J 0 ({) w O:'. :::..::: a: w 0.. 100 80 . . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . .. : . . . . 60 x x x ........... : ... ...... * ............ : ........... * ... x* ....... : ........... : ... . X 0 A 0 * * * * . . . x . . . . . . . 40 ............................................................................ . . . . . . 20' 0 0 0 0 0 0 0 0 0 0 0 .. 0 0 0 0 0 0 0 0 0 0 0 .I 0 0 0 0 0 0 0 0 1 0 0 ._ 0 0 0 0 0 0 0 0 0 0 0,,,. 0 0 0 0 0 1 0 0 0 0 0 I 0 0 ' 0 0 0 0 0 0 0 0 ._ 0 ' 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW ...... Vl ...... \0 0 H) Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W147.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 9-MAR-2016 08:43:57 through 10-SEP-2016 12:00:00 3143.00 through 3223.00 3200 o ' o o o o o o o o ' : o o o ' ' o o o o o I ', o o o o o 0 0 I I 0 0 : I o o o o o 0 o o o o ', I e" 0 0 0 0 o o o o I : o o I I o o o 0 I o o : 0 I 0 o . . . . . . co v "<"i I D (!) )-(!) 0::: x x x x x x x LL.I 3180 z . . . . . . I o o o o ' o o o o I o o o o I I o o o o I I o o o o I o o o I I o o o o 0 o o 0 0 I 0 0 o ,, I O o o o I o o o 0 o o o o o I 1 o o O o o o O O o I I O . . . . . . LL.I ::...::: a: LL.I a.. 3160 *3-16. 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -Vl N 0 0 ......, Vl 00 0 "° QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B147.QAF;4 BACKRATE (Background Rate) 4-MAR-2016 12:36:34 through 10-5EP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 ' 1 0 0 0 0 0 0 0 0 o '* 0 0 0 0 0 0 0 0 0 o o ." 0 0 0 0 0 0 0 0 o o 0 ', 0 0 0 0 0 * ' 0 0 0 0 .' 0 0 0 0 0 1 0 0 0 0 0 : 0 0 1 0 0 0 0 0 0 0 0 ', 0 1 1 0 . . . . . . .06 ............................................................................ . . . . 04 . . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 6-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 ......, Vl 00 0 '° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.WlW148.QAF;5 AVRGEFF (Average Efficiency) 9-MAR-2016 08:44: 04 through 10-SEP-2016 12: 00:00 0.237420 through 0.252100 '25 ........................... ,, ............................................... . :::-, (.) c Q) *r-1 (.) *r-1 4-4-UJ . . . . . . x x x x '245 x x x I 24 ' ' 0 0 0 0 ' 0 0 0 ' .. 0 0 0 0 ' 0 0 0 0 0 ',/' 0 0 ' 0 0 0 0 0 *' 0 0 .. o o o 0 0 0 o 0 0 0 0 J' 0 0 0 0 0 ' 0 0 o 0 o I 0 0 0 0 0 0 0 0 0 0 0 .. 0 0 o 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter Naf'le 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W148.QAF;5 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:44:04 through 10-5EP-2016 12:00:00 184. 000 through 204. 000 200 ........... * ............ .' ........... " ........... .' ........... : ........... * .... . 1
0 (!) )-1--H > H 1--u .< . . . . . * . . . . . . * . . * * . . . . . . . . . . . . . . . . . . . . x . . . . . 40 ............................................................................ . . . . . . 20 ' ' o o o ' o o ' .. o o o ' I o o o o o ',/' o o o ' o o o ' ' o o ... I o o o o o ' o o o o ,/ I o o o I o o o o ' ' I o o I o o o o o ' o o .. o ' o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Mea8ureMent Date/TiMe UP LOW QA filenarrre Pararrreter Narrre 5tart/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W148.QAF;5 P5ENERGY-GD148 (PEAK ENERGY GD-148) 9-MAR-2016 08:44:04 through 10-5EP-2016 12: 00:00 3143.00 through 3223. 00 . . . . . . 3200 .......................................... ' ................................ . co ""'" ..-I I D (!:I )-(!:I CJ::: x x x x x x x LLJ 3180 z . . . . . . ..................................................... ' ..................... . . . . . . . LLJ ::..: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOlll QA filenaMe DKA100: [ENV_ALPHA.QA.B]B148.QAF;3 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 12:36:38 through 10-SEP-2016 12: OO:OO Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 . 08 ............................................... ' ........................... . . . . . . . . . 06 . . . . . . ............................................................................ '04 '02 ....................................................... -................... . . . . . . . 0 3-16 4-16 x 6-16 MeasureMent Date/TiMe UP LOW
,__ Vi N °' 0 I-+) Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W149.QAF;* AVRGEFF (Average Efficiency) 9-MAR-201608:44:10 through 10-5EP-2016 12: 00: 00 O. 249000 through 0. 264407 o o o I o * ' . 26 ' ' o o o ' o o o o o o o o o o o o o o o I I o o o I o o o o I o o o o o
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-Vl N 00 0 H) Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W149.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08:44:10 through 10-SEP-2016 12:00:00 5.00000 through 100.000 80 . . . . . . . . . . . .* . . . . . . . . . . . *. . . . . . . . . . . . .. . . . . . . . .... *. . . . . . . . . . . . : . . . . . . . . . .. : . . .. ...... I D C) z 0 H 1-::l _J 0 (J) w 0:: :::..:: a: w 0. 60 ........... *: ........... :* ........... *:. *X* ...... *:* ........... : ........... *:*. X x x x x x 40 ............................................................................ . . . . . . 20 ' o o o o ' o o o o o .. o ' o o ' o o o o o '" o o ' ' o o o I ' o o .. ' ' o o o o ' o o o o ,/ ' o o o o I o o o o o I o o ' ' o o o o ' o o .. o I I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W149.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148). 9-MAR-2016 08:44:10 10-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 O o o o o o o o o o I O O O O O O O o O o o o o o o o o o O O I O o, O O O *I o o o o o o o o o I o o o o o o o o 0 I I 0 o o o o o o o 0 I 0 0 o o I o o . . co v """" I D (!) }-(!) O:'. x x x x x x x LLJ 3180 Z. . . . . . I I 0 0 0 I 0 o o o I I o o o o o o o o 0 0 I 0 0 0 0 o o O o o o o o o 0 0 0 o o 0 o o o o o I I o o o I 0 o o 0 0 I 0 o 0 I o o o o o 0 0 0 0 0 0 0 0 . . -. . . . LLJ a:. LLJ 0.. 3160 16. 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B149.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:44: 33 through 10-SEP-2016 12: 00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 UP .08 O o o o o I O o o o o o o o o o o o o o o o o o o o o o o o e o o o o o o o o o o o o o o o o o o o o o o I o o o o o o o o 0 o 0 0 0 o o 0 0 o o I I 0 . . . . . . .06 . . . . . . o o o o
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0 o 0 o 0 I o o o 0 o o o o I o o o 0 o o o o o o o o o o o o o o o o o o .04 .02 ............................................................................ . . . . . . 0 ......... 3-16 LOW 4-16 8-16 9-16 5-16 6-16 7-16 MeasureMent Date/TiMe 0 ,...., Vl 00 0 \D QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W150.QAF;4 AVRGEFF (Average Efficiency) 9-MAR-2016 08:44:16 through 10-SEP-2016 12: 00: 00 0.246282 through 0.261516 . . . . . . . 26 ............... ' .................................. *-........................ . (j c I}) *r-1 . 255 (j *r-1 4-4-LlJ I}) "OJ) ill x I-I}) > x a: x . 25 . ,* ...................... * ......................... * ............ : ................ . x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W150.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:44:16 through 10-SEP-2016 12:00:00 184.000 through 204. 000 200 I I I I I o 0 I I I I 0 I I 0 0 I I I I o o o o I 0 I o I I I I I o o o I o o o o o I o o I O I o o o o I I o o o o I I o o o 1 O o o O o o o o o o 1 1 I 0 (!) H > H u a: w 0 H _J u ::i z . . . . . . x x x x x x . . . . . . 190 .. '*' .................... * ......................... * ... x ........ : ................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Oate/Tir.-.e UP LOliJ QA filenarvle Pararvleter Nar.-.e Start/End Oates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W150.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08:44:16 through 10-SEP-2016 12:00:00 5.00000 through 100.000 80 o o

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0 0 0 0 0 0 0 J' 0 0 0 0 1 0 0 0 0 0 0 I 0 0 1 1 0 0 0

0 0 0 'w 0 0 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-Vl Vl \0 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W157.QAF;3 ParaMeter NaMe PSENERGY-G0148 (PEAK ENERGY GD-148) Start/End Dates 9-MAR-2016 08:45: 04 through 10-SEP-2016 12:00: 00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . ............................................................................ . . . . co ""'" ..,-! I D C!J )-C!J O:'. x x x x x x -X Ll.J 3180 z . . . . . . I 0 o o o o o o o o o o o o o o o o 0 0 o o o o o o o o o 0 0 0 I o o o o o o o o 0 o o o o o o o o 0 0 I o o o o o o 0 o o I o o o o o o o o o o 0 I o . . . . . . Ll.J :,..c:: a: Ll.J 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOliJ MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B157.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 16:22:59 through 10-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0. 100000 I 08 1 1 1 1 1 1 1 1 1 1 1 11 1 1 1 1 o 1 1 1 1 1 ' ." 1 o o ' 1 1 1 1 1 1 1 10 ' 1 1 1 1 1 1 1 1 1 1 .' 1 1 1 1 1 ' 1 1 1 ' 1 : 1 o 1 ' 1 1 1 1 1 1 1 10 1 1 1 1 '06 . . . . . . . . . . . : . . . . . . . . . . . *. . . ' . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . .. : . . . . '04 . . . '02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16-MeasureMent Date/TiMe UP LOW -Vi O'\ -0 ....., Vi 00 0 \0 QA filenar.-.e Parar.-.eter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W158.QAF;4 AVRGEFF (Average Efficiency) 9-MAR-2016 08:45:10 through 10-SEP-2016 12: 00: 00 0.244300 through 0. 259410 . . . . 255 ............................................................................ . . . . . . :>, (..) c Q) x x x *r-1 (..) *r-1 x x 4-x 4-UJ x ID* "O,I) (lj S-Q) . 25 > -. . . . . ................ ' .............. ' ........................................... . a: I 24*5 o .. o o o o I o o o I 'o o o o I o o O O o o o .. o o o o o o o o o o o 'o o o o o o o o o o o o .. I o o o o I o o o o o : o o O I o o o O I o o 'o O I I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W168.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08: 45:10 through 10-SEP-2016 12:00:00 184. 000 through 204. 000 200 o o o o o o ' o o ' ' o 0 0 o I I 0 0 0 o ' o o o o ' ' o o o I I o 0 o 0 I o o o o o o o o o o o o o ' I o o o o o 0 o o o o o o o ' o o o o o o o o o . . . . . . I 0 (!) )-f-H > H f-x u <I: x x w o* x H ...J x x u x ::J z 190 ' o o o o o o o o o o ," o o o o I o o o 0 o I 00
0 I I 0 o o o o o o : o o o o o o o o o o o 'o o o O o O o o o o o o : o o o o o o o o I O O : o I o o 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOLI.I QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper 100 DKA100: [ENV_ALPHA.QA.W]W158.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08:45:10 through 10-5EP-2016 12:00:00 5,00000 through 100.00D 80 ' 0 o * ' o 0 o o o o ," o o o o o o 0 o o o I ', o o I o o o o o I 0 0 .. I I o o o 0 0 o o o o ', o o o e o I o o o o o : o o I o o o o o I ' o : o o o o ..-l I Cl (') z 0 H ::i ....I 0 en w a: ::..::: a: w 0... . . . . . . 60 .......................................... ' ................................ . . . . . . . x x x x x x x . . . 40 o o o O o I I O o o o o o o o o o o o o o o o o o O I I o o o o o o e o o I O o o e o o o e o o I o o o o o o o o 0 0 o o 0 o o o o o o o o o 0 o I I o . . . . . . 20 *, ' o o o ' ' o o o ' .. o o o o I

o o o ' '.!' o o ' ' o o o ' ' ' I .. ' I o o o ' ' o o o o .I o ' o o o ' o o o o ' I o o ' ' o o o o I o ' .. o o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
-Vl 0\ 0 ,...., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W158.QAF;4 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 9-MAR-2016 08:45:10 through 10-SEP-2016 12: 00:00 Lower/Upper LMts: 3143. 00 through 3223. 00 UP 3220 3200 . . . . . . ' I o o o ' ' ' ' ' o ' o o ' o o 0
o o ' ' o o o ' ' o o 0 0 0 o o o ' ' o o o o I o ' o o o o o o o 0 0 ' o o I o o o o I I o o o o o o o o o o o o . . . . . co ""'" ..-i I D )-Ct'. x x x x x x x LiJ 3180 z . . . . . . . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . .. : . . . . . . . . . . . : . . . . . . . . . .. *. . . . . LiJ ::..::: a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B158.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 16:23:03 through 10-SEP-2016 12: 00: 00 O.OOOOOOE+OO through 0.100000 I 08 1 0 0 0 0

0 0 0 0 0 '* 0 0 0 ' 0

0 0 0 ' 1 / 0 o 0 ' 0 0 0 0 1 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 .' o 0 0 0 0 0

0 0 0 0 : 0 0 0 0 o 0 0 0 0 0 0 ',

0 0 0 . . . . . . o r o o e o o o o o o o o e o o o o o o o o o o o o o o o o o o o o o o o o o o o

I o o I o I o o o o o I I o o 0 o o I o o o o o o I o o o I I o I o '04 . . . . 02 ........... * ............ : ........... * ............ : ........... : ........... * .... . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TilY'le UP LOW QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Date8 Lower/Upper Lr.-.t8: DKA100: [ENV_ALPHA.QA.W]W159.QAF;3 AVRGEFF (Average Efficiency) 9-MAR-2016 08:45:15 through 10-5EP-2016 12:00:00 0. 251623 through 0.267187 . 265 o o o " 0 0 I o 0 o I o o o o I I o o o o o o 0 o o I I 0 o o o

e o o I o o o

0 o 0 I o o o o o o o o I o 0 o o 0 o o o o o o o o o o o o 0 o 0 I o ::>, u c ID *r-1 u *r-1 4-4-UJ . . . . . . . . . . . . . 26 ............................................................................ . . . . . . x x x x x x x I 255 ° 1 0 0 0 ' ' 0 0 0 1 ', 0 0 0 1 0

0 0 0 ' 1 ." o 1 o 0 0 0 0 0 0 0 0 ', 0 1 0 0 0 0 o 0 0 0 0 .' ' 0 0 0 1 1 0 0 0 1 1 : 0 o 0 1 0 0 0 0 1 0 0 ', 1 1 1 o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Mea8urer.-.ent Oate/Tir.-.e UP LOW QA filenafl'le Pararieter Nafl'le Start/End Dates Lower/Upper LMts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-2016 08:45:15 through 10-SEP-2016 12:00:00 184. 000 through 204. 000 200 ........... * ......................... * ................. -........ : ........... * .... . I D (!:I )-I-H >" H I-u x x x x x a: w x D x H ....I u ::i z 190 . . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . . : . . ' . . . . . . . . .. . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl'lent Date/Tifl'le UP LOW
-VI 0\ 00 0 ....., VI 00 0 \0 QA filenar.-.e Pararieter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W159.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 08:45:15 through 10-5EP-2016 12:00:00 5.00000 through 100. 000 80 I o I I I o I
I o o ," o o o o I o o o o I I*, o o I I o o o o I o o .-I

o o o o o e o I 1 'o o O o o o I o o o o o : o o o I 1 o o I O o O : o o o o -M I CJ (!) z D H 1-. :l _J D (f) w O:'. . . . . . . 60 ......................................................................... ' .. . . . . . . x x x x x x x . . . . . 40 o o o o o 0 ' o I o I I o I 0 o 0 o 0 I 0 I I o I I I I o o o o o o o o o o I o o o o I o o o I I O o o I I o o o I o o o o o o o o o o o o o o o o I I . . . . . . . 20 o ' o ' o o o ' ' ' ' .. o ' ' ' ' ' ' ' ' ' ',/' ' ' ' ' ' ' ' ' o o ' ._' ' ' ' ' ' ' ' ' ' '.I o ' ' ' ' ' ' * ' ' o I o o ' o ' ' ' .. ' ' ' ' 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA f i lenaMe . ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W169.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 9-MAR-2016 08:46:16 through 10-SEP-2016 12: 00:00 3143.00 through 3223. 00 . . . . . . 3200 .......... ' ................................................................ . ro "'" "'""" I D (!) :r x x (!) a: x x x x x LL.I . . . . . . 3180 ............................................................................ z . . . . . . LL.I a: LL.I 0.. 3160 3-16 4-16 6-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... Vl -..J 0 0 ....., Vl 00 0 \0 QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.B]B169.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13: 46:09 through 10-5EP-2016 12:00:00 0. OOOOOOE+OO through 0. 100000 . 08 o o o o o I o o o o O O o o o o I o o o o o I o o o I I o o o I o o 0 o I 0 o o I o I o o o o I I o o o
I o 0 o 0 I 0 0 o I I o o o o o o o o o I I I . . . . . . . 06 . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . .. *. . . . . . . . . . . . : . . . . . . . . . .. : . . . . . 04 . . . . . 02 ........... * ............ : ........... * ............ : ........... : ........... * .... . 0 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW 0 >-+, Vi 00 0 \0 QA filenar.-.e DKA100: [ENV_ALPHA.QA.W]W160.QAF;3 Parar.-.eter Nar.-.e AVRGEFF (Average Efficiency) Start/End Dates 9-MAR-2016 11:00:19 through 10-SEP-2016 12:00:00 Lower/Upper Lr.-.ts: 0, 248170 through 0.263520 . . . . . . . 26 ' ' ......................................................................... . u c I}) *r-1 u *r-1 4-4-UJ x x x . . . . 0 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o o 0 I o o o o I o o o I I o o o o I o o o o I I o . . . . . . . 255 x x x x I 2 5 ° 0 0 0 0 1 0 0 0 0 0 ._ 0 0 0 0 1 0 0 0 0 0 0 ,/' 0 0 0 0 0 0 0 0 0 0 0 ._ 0 0 0 0 0 0 1 0 0 0 0 #' 0 0 0 0 1 0 0 0 0 0 0 I 0 0 0 0 0 0 0 0 0 0 0 .. 0 0 0 0 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filena!'le Para!'leter Nal'le Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W160.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 9-MAR-201611:00:19 through 10-SEP-2016 12: 00:00 184.000 through 204.000 200 ........... " ........................ * ......................... : ........... " ... . I D (!:I )-x I-H > H x x I-x u cI x w D H ...J x x U. ::i z 190 o I 0

O o o o o o o ," o o o O I o o o o 1 o 'o I I O o o o o 1 1 o I .. o o o o o o O o o o o 01 1 o o o 1 O o o o o o : o o I I o o o o 1 o o o" 1 1 o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW
..... Vl -J w 0 ....., Vl 00 0 \0 QA filena!Yle Para!Yleter Na!Yle Start/End Dates Lower/Upper LIYlts: 100 DKA100: [ENV_ALPHA.QA,W]W160.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 9-MAR-2016 11: 00:19 through 10-SEP-2016 12:00: 00 5, 00000 through 100, 000 80 ' ' o
o ' I ' o o o : ' o o o o 0 o o o I I 'o o o o o o ' I o o o 0 .. I o o o o o I o o o o 'o I o o o o o o o o o I : o o o I o o o o I o o: o 0 o e ..-1 I* D z 0 H :::::i ....J 0 (f) w [!'.'. :..::: a: w 0.. . . . . . . 60 .......................................... ' ................................ . . . . . . . x x x *x x x x 40 ' ' o o o o I o o o o o o o o o o o o o o I I o o o I O o o o o O o o o o o O o o o o o O o o o o o o O o o o o o I o o o o I I 0 o o o o o o o o o I O . . . . . . 20 1 0 0 0 0 1 0 0 0 0 0 ._ 0 0 0 0 0 0 0 0 0 0 0 .!' 0 0 0 0 0 0 0 0 0 0 0 .. 0 0 0 0 0 0 1 0 0 0 0 .I 0 0 0

0 0 0 0 0 0 0 I 0 0 0 ' 0 0 0 0 0 0 0 ._ 0 0 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Ylent Date/Ti!Yle UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W160.QAF;3 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 9-MAR-2016 11:00:19 through 10-5EP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . . : . . . . . . . . . .. *. . . . . . . . . . . . : . . . . . . . . . . . : . . . . . . co ""'" ..i* I D >-ct:: x x x x x x x LL.I 3180 z . . . . . . * * * * * * * * * * * ** * * * * * * * * * * * : * * * * * * * * * * * ** * * * * * * * * * * * : * * * * * * * * * * * : * * * * * * * * * * * * ** .r *

LL.I :::.::: <L LL.I Q.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B160.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-201613:45:13 through 10-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' 1 0 0 0 0 '

0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 .' 0 0 0 0 0 0 0 ' ' 0 0 ', 0 0 0 0 0

0 0 0 0 0 *' o 0 0 0 0 0

0 0 0 0 : 0 0 0 0 0 0 0 0 0 0 0 ', 0 0 0 0 .06 . . . . . . o o o 0 o o o o o o o ' o 0 0 0 o o o o o I I o o I I o o o o 0 I 0 I o I o o o o 0 I o o o o o o 0 o o I I o o ' I I I I I o I o o o o o o o o o o I o . . . . 04 . . . . . . .02 ............................................................................ . . . . . . 0 3-16 LOW 4-16 5-16 7-16 6-16 8-16 9-16 MeasureMent Date/TiMe
-Vi -..J 0\ 0 ......, Vi 00 0 "° QA filenal'le ParaMeter Nal'le Start/End Dates Lower/Upper Ll'lts: DKA100: [ENV_ALPHA.QA.W]W161.QAF;4 AVRGEFF (Average Efficiency) 13-JUL-2016 12:44:02 through 14-SEP-2016 12:00:00 0.245186 through 0.260352 . . . . . . . . . . 26 ............................................................................ x x x :>, . 255 (..) c Q) *r-i (..) *r-i 4-4-LU Q) '0.0 iU s-Q) > a: . 25 . . . . . . . . . ' I o 0 o ' ' o o o ' o o 0 0 I ' o o o o o o o o 0 0 I 0 o o o o o o o I 0 o I o o o o o o o I 0 o 0 o o o o o o o I o o o o o o o o 0 0 0 o o o o o o . . . UP 7-13 7-20 7-27 8-03 8-10 8-17 8-24 8-31 9-07 9-14 LOW Measurel'lent Date/Til'le -Vl -.l -.l 0 >-+, Vl 00 0 \0 QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W161.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 13-JUL-2016 12:44: 02 through 14-SEP-2016 12: 00:00 184.000 through 204.000 200 ....... * .......... * ....... * ........ *.* ................ * ........ *.* ................ * .. I D )-t--H > H t--U* a: LLJ D H __J x (j ::i z* .x: 190 ........ * .. ' ..... * .................. * ........ * ................. ,*, ....... * ......... *. x UP 7-13 7-20 7-27 8-03 8-10 8-17 8-24 8-31 9-07 9-14 LOW Measurerrrent Date/Tirrre QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W161.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 13-JUL-2016 12:44: 02 through 14-SEP-2016 12: 00:00 5.00000 through 100. 000 80 o o o o o o o o' o o o o o o o o 'o o O o O O I o : o o o o o o o o 0 o o o o o o o o 1o o e o o o 0 o .. o o 0 0 o o 0 I 0 o o o o I I o o 10 o I o o o o I o' o T"I I D (!) z 0 H ::i _J 0 (f)" w O:'. a: w 0... x . . . . . . . . . 60 ......................................... ' ................................ . . . . . . . . . . X* . . . . . . 40 .......... ' ................................................... ' ............ . . . . . . . . . . 20 .......................... ' ................. , ....... ' ................. , ......... . UP 7-13 7-20 7-27 8-03 8-10 8-17 8-24 8-31 9-07 9-14 LOW MeasureMent Date/TiMe -Vl -..J \0 0 ....., Vl 00 0 \0 QA filenafYJe ParaMeter Nartle Start/End Dates Lower/Upper LMts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 13-JUL-2016 12:44:02 through 14-SEP-2016 12: 00:00 3143.00 through 3223.00 o o o o I I o 0 o 3200 0 0 0 0 o I o o o o 0 o 0 0 o o I o o o o I o 0 o 0 I o o o I o o o o o I o o o o o I o o 0 o 0 o o o o I I o o o I I o o o I I o 0 o o 0 o o 0 o I ' o . . . . . . . . . ro tj" ""'"" I D CJ )-CJ O:'. x X* x LLJ 3180 z . . . . . . . . . ............................................................................ . . . . . . . . . LLJ ::..:: a: LLJ 0.. 3160 UP 7-13 7-20 7-27 8-03 8-10 8-17 8-24 8-31 9-07 9-14 LOW MeasureMent Date/TifYle QA filenaMe DKA100: [ENV_ALPHA.QA.B]B161.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:04:23 through 14-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 UP I 08 ' 0 0 *
0 ' 0

0 ' .' 0 ' ' ' 0 ' ' ' 0 ' '* 0 0 0 0 ' 0 0 0 0 0 * *, 0 0 0 0 0 0 0 0 0 0 0 : 0 0 0 0 0 0 0 0 o o 0 01 0 0 0 0 0 0 0

o 1 0 00 0 0 0 0 0 .06 . . . . . . ............................................................................ . 04 .02 ............................................................................ . . . . . . x x x. 0 3 -16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe
-VI 00 0 ......, VI 00 0 \0 QA filenafYle ParafYle ter NafYle Start/End Dates Lqwer/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 18-AUG-2016 12:26:31 through 14-SEP-2016 12:00:00 0.259705 through 0.275769 (.) c Q) *r-1 (.) *r-1 4-4-LU Q) "0.0 ill Q) > a: . 275 . 27 . 265 . 26 . . . . . . . . ............................................................................ . . . . . . . . . o o. 0 o o o o o' o 0 o o o o o o'o o o o o o I o 'o o o o o o o I .. o o o o o 0 o o'o o o o o o o 0 'o o o o o o o o : I o o o o o o o' o o I o o o o o'o o x x x x x x o o o o o o o *, o o o I o o o 'o' 0 o 0 o o o o .. o 0 o o o o o 'o o o o o o o o 'o o I o 0 o o o o o' o o I o 0 0 o : o o o o 0 I o 'o o o o o o o o 1,1 o . . . . . . .. * . . . . . . . . . . . . . . . . . *. . . . . . . . .. . . . . . . .. * . . . . . . . . *. . . . . . . . : . . . . . . . .* . . . ....... . 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 MeasurefYlent Date/TifYle UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Oates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W162.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 18-AUG-2016 12:26:31 through 14-SEP-2016 12: 00:00 184.000 through 204.000 20 0 ....... * .......... * ................ * ........ * .......... * ....... : ....... " ....... *.* . I D )-I-H > H I-u cr: L1J D H ....I u :J z 190 x x x x . . . . . . . . . ' o o o o ' o o o o ' o o o ' I I o o 0 o o o o o o o o o o o ' o o o o I o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 0 o o o o o o x x UP 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 LOW MeasureMent Date/Tir.-.e ...... Vl 00 VJ 0 Hi Vl 00 0 \0 QA filenal'Je Parameter Name Start/End Dates Lower/Upper Lmts: DKA100: [ENV_ALPHA.QA.W]W162.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 18-AUG-2016 12:26:31 through 14-SEP-2016 12:00:00 5. 00000 through 100. 000 "<"i I 0 z* 0 H ::i _J 0 U') LLJ O:'. a: LLJ 0.. 100 80 60 40 . . . . . . . . . .......................... ' ................................................ . . . . . . . . . . ............................................................................ . . . . . . . . . x x x . . . . . . . . *. ............................................................................ . . . . . . . . . 20 ................ '*' ....... ' ....... ' ....... '*' ....... *' ....... ' ................ '*' . 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 Measurel'lent Date/Til'le UP LOW -Vl 00 ""'" 0 ....., Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W162.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 18-AUG-2016 12:26:31 through 14-SEP-2016 12: 00: 00 3143. 00 through 3223. 00 o o o ' o o I 0 o 3200 .......................................................... ' ................ . co v ...-1 I D (!:I. )-(!:I Ct:: LLJ 3180 2 LLJ ::..:: a: LLJ 0.. 3160 x ::00:: . . . x . . . . . . . . . ............................................................................ . . . . . . . . . UP 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 LOW MeasureMent Date/Til'l"Je ...... Vi 00 Vi 0 >-+, Vi 00 C> \D QA filenaMe DKA100: [ENV_ALPHA.QA.B]B162.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:04:27 through 14-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 .08 ' ' 0 o o ' ' o o o ' ' o o o ' 0 o o o 0 o
o 0 o o o o o o o I o o o I I o o o 0 I o o o o I I o o o I I 0 o o o o o o o I 0 o o o 0 o o o o o o I o . . . . . . .06 . . . . . . ................................ ' .......................................... . . 04 .02 ............................................................................ . . . . . . 0 3 -16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA f i len*arrie

Pararrie ter Narrie Start/End Date8 Lower/Upper LrritB: DKA100: [ENV_ALPHA.QA.W]W163.QAF;4 AVRGEFF (Average Efficiency) 14-MAR-2016 10: 47:13 through 14-SEP-2016 12:00:00 0. 251924 through 0.267506 . . . . . 265 0 0 o o o o o o o o o o o o o I I o o 0 o o o o o o o o o 0 0 I I o o o o o o o o o I 0 o o o o o o o o ' o o I 0 I I o o o o o o o o o o o o o o o I o >.. (J . . . . . . c Q) -ri (J -ri 4-4-* 26 ....................... * ............ * .......................... * ............ * .... . UJ x x x x x x x . 255 o I o o o I o o o o I o o o o I I o o o o I I o o 0 o I 0 o o o ' o o o I I o o o o I o o o o o o o o o I 0 0 o o o o o o o I I o o o o 0 o o o o ' I o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeaBurerrient Oate/Tirrie UP LOW QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W163.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 10:47:13 through 14-SEP-2016 12:00:00 184.000 through 204. 000 200 ........... : .......... * ............ * ............ : ............ * ............ * .... . I D )-I-H > H x I-u <I: w x x x D H ....I u :::) x x z 190 ........... * ............ * ............ * ........... * ............ * ............ * ..... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW QA filenarrie Pq.rarrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W163.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10:47:13 through 14-SEP-2016 12:00: 00 5. 00000 through 100.000 . . . . . . 80 ...................... ' .................................................... . ..-l I 0 z 0 H ::i ....I 0 (.{) w O::'. . . . . . . 60 o ' o o o I I o o o o I o o o o I o o o I o I o I 0 o 0 o o o 0 0 o o o I I o o o o I o o o o I o o o o o I o o o 0 I 0 o 0 o I o o o o o o o o o o o o . . . . . . x x x x x x x 40 ' o o o o o I o o o I o o 0 o I 0 o o 0 o I I o o o I o o o o o o o o o I o o o o o I o o o 0 0 0 0 0 o I I o o o I o I o I o o o o o o o o o o 0 ' 0 0 . . . . . . 20 ........... ' .......... '* ........................ ' ........... *' ................. . 3-16' 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W163.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10:47:13 through 14-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 o ' o o o o I o o o 0 0 o o o I o o o o o o o o o o 0 I o o o I o o o o I o o o o 0 0 o o o 0 o o o o o I o o o o o o o o ' 0 o o o o o o o o o o o o o . . ro v ..,..., I D (!) )-C) 0::: x x x x x x x w 3180 z . . . . . . ............................................................................ . . . . . . w ;:,.:: <r w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B163.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:04: 31 through 14-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' 0 0 ' 0 0 0 0 .' 0 0 0 ' ' 0 0 0 0 ' ', 0 0 0 ' 0 0 0 0 ' 1 0 ', 0 0 0 0 0 0 * ' o 0 0 ." 0 0 0 0 0 0 ' 0 0 0 0 .' 0 0 o 0 0 0 0 0 0 0 0 ,* 0 0 o 0 0 . . . . . . . 06 ............... ' ........................................................... . . 04 '02 ............................................................................ 0 x 3-16 . . . . -. . 4-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW 0 ......, Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: . 275 ), 0 c DKA100: AYRGEFF (Average Efficiency) 18-AUG-2016 15: 05:24 through 14-5EP-2016 12: 00: 00 0.260389 through 0.276500 X* . . . . . . . . . Q) . 2} ' o o o 0 I I o o o 0 0 o o o I 0 o o o o I I o o o o o o 0 0 o o o o o I I o o o o o o 0 0 o I o o o o I I 0 o o o o o o o I I o o o o o o 0 0 o o o o *ri . . . . . . . . . 0 x *ri 4-4-LU Q) "OJ) X* i(i I-x Q) x > q: '265 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W166.QAF;6 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 18-AUG-2016 15: 05:24 through 14-5EP-2016 12:00:00 184.000 through 204.000 200 0 I I o o ' I o o 0 0 I e o o o 0 o 0 0 o I ' o o o I I 0 o o o o o o 0 I I o o I o I I o o o I I o I 0 I 0 I o o o I 0 0 I I I o I o I I 0 o o I o I I . . . . . . . . . I 0 (!) )-t-H > H t-u x a: . 24 . . . . . . . . . . . . . . . . ............................................................... ' ........... . x x x x x. I o o o o I I o' o o 0 I o o o o'o o o o o o o o 1o o o o o o o o .. o o o o o o o o' O I o O o o o o 1o o o o o o o o : o o o o o o o o' o o o o I o o o'o o x* UP 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 LOW MeasurefYlent Date/TifYle QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA. QA. W]W167. QAF; 4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 18-AUG-2016 14:53:57 through 14-SEP-2016 12:00:00 184.000 through 204.000 200 ....... * ........ *.* ................ * ........ * .......... * ....... : ....... * ........ *.* . I Cl (!) )-I-H > H I-u a: w Cl H ...J U* ::i z x x x x x x: 190 . ' ...... * ........ * ........ * ........ : ........ * ........ * ........ : ........ * ........ * .. 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 Measurerrient Date/Tirrie UP LOW
....... Vt \0 00 0 H) Vt 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W167.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 18-AUG-2016 14:53:57 through 14-SEP-2016 12:00:00 5.00000 through 100.000 80 ......... * ........ * ........ * .................. * ........ * ........ : ........ * ........ * .. -M I D (!) z D H 1-=:i ....I D en w O:'. ::..::: a: w o..* 60 40 . . . . . . . . . I I 0 0 0 0 0 0 0 o I I O O O I I o o O o I o O o O o o o O o I o O O O O O O O O O I e O o o o o o o o o O o o O O O O O O I O o o o o o o o o o I o O x x . . . . . . -. . . . x x x: x . . . . . . . . . I I o o o I o o o o I I 0 0 e I I & 0 0 0 0 I o o 0 I I o o o o o o o o 0 o o o 0 0 I o e o O o o O O o o o o o o o o o o o I I O O o e O O O o o o o e . . . . . . . . . 20 .......................... .! ******* ' .......................... ' ******************** UP 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 LOW Measurerrient Date/Tirrie QA filenarrre Pararrreter Narrre Start/End Dates lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA.QA.W]W167.QAF;4 P5ENERGY-GD148 (PEAK ENERGY GD-i48) 18-AUG-2016 14: 53:57 through 14-5EP-2016 12:00:00 3143.00 through 3223.00 . . . . . . . . . . 3200 o o o o o o o o o o o o o 0 o o o 0 o o o o o 0 o o o I 0 0 o o o o o o o o o 0 o o ' o o o ' I I o o o o 0 o o o o I o ' o I o o o ' o I o o o o I I o . . . . . ro tj" . .-I I. D (!) )-(!) et: x: x LLJ 3180 z . . . . . . . . .* .............................................................. ' ............ . . . . . . . . . . LLJ ::,..::: a: LLJ 0.. *. 3160 8-18 8-21 8-24 8-27 8-30 9-02 9-05 9-08 9-11 9-14 Measurerrrent Date/Tirrre UP LOW QB filena!Yle Para!Yleter Na!Yle Start/End Dates Lower/Upper L!Ylts: DKA100: [ENV_ALPHA.QA.B]B167.QAF;2 BACKRATE (Background Rate) 19-AUG-2016 12:55:14 through 14-SEP-2016 12:00:00 0. OOOOOOE+OO through 0.100000 .08 I I I I I I I I I I I I I I I o I I I I I I I I I o I I I o O o o I I I I I I o I I I I I I I I I I I I I I I I I I I I I o I 0 I I I I o I I I 1 O o o . . . . . . . . . 06 . . . . . . . . ............................................................................ '04 . . . . . 02 . *-......................................................................... . . . . . . . . . 8-22 8-26 8-28 8-31 9-03 9-06 9-09 9-12 MeasureMent Date/Ti!Yle UP LOU.I 0 ....... VI 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 14-MAR-2016 10: 47:36 through 14-SEP-2016 12:00:00 0.258364 through 0. 274346 . . . . . . . 27 ...... ' .................................................................... . . . . . . . >.. _u i:::: I]) *r-i u *r-i 4-4-LU ID "OJ) i{j . 265 I-I]) ........... * ............ * ............ * ........... '* ........... * ............ * ..... . x x > a: x x x x -X . . . . . . . 26 ........... .' .......... " ........... * ............ .' ... *><: ...... " ........... " .... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... 0\ 0 N 0 ......, Vi 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W169.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 10:47:36 through 14-5EP-2016 12: 00: 00 184.000 through 204.000 200 ' ' ' o o ' ' o o o I 0 o o e o o o o o o o o o 0 0 0 0 0 o o o o o o o o I o o o o o o o o o o o o o 0 0 I o o o o o o o o I 0 o o o I o o o o o I I o . . . . . . I D (!) )-I-H > H I-u a: x x llJ D H x _J u ::i z x x 190 ' o o e o o o o o o o 'o o o o I I o o o o 0 o' o o o ' o o o o I I e o'o I ' o o o o o o o o ', I I o o o 0 I o o o I 'o o o o I I o o o o o o 'o o o I I o x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -O'I 0 v.> 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W169.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10:47:36 through 14-SEP-2016 12:00:00 5.00000 through 100.000 ..-! I Cl CJ z 0 H 1-:l ....I 0 (/) w O:'. a: w CL 100 x 80 ........... * ............ * ....... x .... * ........... * .... *X ...... * ............ * .... *x . x . x . . x . . x . 60 . . . . . . o I ' 0 o o o o o o 0 0 o o o o o e 0 o o
o o o o O O I 0 o o o o o o O O O O O o ' o o o o o o O o o I I o o o o o o o o o o O o o o o o o o o o I o . . . . . . . . . . . . 40 ............................................................................ . . . . . . 20 ........... , .......... '* ........... '* ........... , ............ *' ........... *' .... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 14-MAR-2016 10: 47:36 through 14-SEP-2016 12:00:00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . . . ' ......................................................................... . . . CD ""'" "<""i I D (!) )-(!) 0::: x x x x x x x x w 3180 z . . . . . . ............................................................................ . . . . . ' W. :i.:: a: w CL. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
-0\ 0 VI 0 ....... VI 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B169.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:04: 56 through 14-SEP-2016 00 O.OOOOOOE+OO through 0.100000 . 08 .......................................................... ' ................ . . . . . . . . 06 . . . . . . ............................................................................ . 04 . . . . . 02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ,_. 0\ 0 0\ 0 ......, Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: . 265 ::>, u c (I) *r-1 u *r-1 4-4-lJJ (I) x "OJ) '26 l{j I-(I) > a: DKA100: AVRGEFF (Average Efficiency) 14-MAR-2016 10:47:40 through 14-SEP-2016 12:00: 00 0. 253400 through 0.269100 x x x x x x I 255 O O O o O I I o o o o ,/' o o o I I o o o o o o, o o o o o o o o o o o o, o 1 o o o o o o o o o ,/' o o o o o o o o o o 1 *' o o o o o o o o o o o ,o o o o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -0\ 0 -...] 0 ....., Vl 00 0 \0 QA filenafYle ParafYleter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W170.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 through 14-SEP-2016 12:00:00 184.000 through 2n4.000 200 ........... .' .......... * ............ * ............ .' ............ * ............ * .... . I D )-1--H > H 1--u a: x w D x x H ....J u ::i x x x z 190 I o o o o 0 o o o 0 , o o o 0 0 o o 0 0 o 1' o o 0 0 o o o o 0 I o o' o I I 0 0 o o 0 o 0 e 'o o o o o o o I o o o 0 '1 o o o o o 0 0 0 o I o 'o 0 0 I I o x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TifYle UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W170.QAF;4 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Date8 14-MAR-2016 10:47: 40 through 14-SEP-2016 12: 00:00 Lower/Upper LMt8: 5.00000 through 100.000 I CJ z D H 1-:l ....J D r.n lJJ O:'. :::..::: a: lJJ 0.. 100 80 ........... * ............ * ............ * ........... * ...... ' ..... * ............ * ..... . x x 60 . . . . . x . ..... x******.-***********.****x********.***********:***********:***********:***** x x . . . 40 ............................................................................ . . . . . . 20 ........... , .......... " ........................ , .............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -0\ 0 \0 0 ....., VI 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10:47:40 through 14-SEP-2016 12: 00:00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ ro ""'" I 0 )-0:: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ ;:,..::: G: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B170.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 13:05:00 through 14-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 Q) ..,Jo l1j [t'. C :J 0 -0.0 .::£. u l1j co I 08 ' o * ' ' ' o ' e ' o: ' o o ' I o o o 0 0 o, 0 o 0 I I 0 o o o I o ', 0 I o o o o o o o o o .. o o o o o o o o 0 0 o ,1 I o o ' o o o o o o o ,' I o o I o . 06 ........... * ............ * ............ * ........... * ............ * ............ * ..... . . . . . 04 . . . . . 02 ........... : .......... * ............ * ............ : ............ * ............ * .... . 0 x x x 3-16 x x 4-16 5-16 6-16 7-16 MeasureMent Date/TiMe x x 8-16 9-16 UP LOW 0 >-+, Vl 00 0 \0 QA filenar.-.e
Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W175.QAF;3 AVRGEFF (Average Efficiency) 14-MAR-2016 10: 48:01 through 14-SEP-2016 12:00:00 0.260448 through 0.276590 . . . . . . .275 .................................................................... ' ...... . >i 0 c ID . 27 *r-1 0 *r-1 4-4-x UJ ID "O,I) (lj I-x ID > a: x x . 265 0 0 0 o o o 0 o o o o 0o o o o o o

o 0 o I o' o o o I o o 0 0 I I o o' o o o o o o o O o o o 0o I 0 0 0 o o o o o o o 01 o o O I o o 0

o o o 0o o o o o o x x .x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W175.QAF;3 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 14-MAR-2016 10:48:01 through 14-SEP-2016 12:00: 00 Lower/Upper LMts: 184. 000 through 204.000 UP 200 ....................... * ............ * .......................... * ............ * .... . I 0 r r H > H r u x w 0 H x x u x x x z 190 . . . . . . o o o o o o o o o o o o o o o o o o o o o o 0 0 0 0 0 o o o o o o o o o o o o o o o I 0 o o o o o o o o o o o o o 0 o o 0 0 o o o o o o o o o o o o o 0 x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenarrre Pararrre ter Narrre Start/End Dates Lower/Upper Lrrrts: 100 DKA100: [ENV_ALPHA.QA.W]W175.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10: 48:01 through 14-SEP-2016 12: 00: 00 5.00000 through 100.000 80 ........... * ............ * ............ * ........... * ............ * ............ * ..... . -M I D (!) z 0 H ::i _J 0 en w O:'. ::..::: a: w 0... 60 . . . . . . o o o o o o o o o o o o 0 o o o o o o o o I o 0 0 o o o o o o 0 o o 0 o o o o o o o I o o o o 0 0 o o o o o o e o o 0 0 o o o o o o o o o o 0 o o o o o . . . . . . x x x 40 . . . . ::< . . . . . . :. . . . . . . . . . . .: . . . .x. . . . . . . .: . . . . . . . . . . . :. . . . . . . . . . . :. . . . . . . . . . . :. . . . . . 20 ........... , .................................... , .............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW
-0\ -.j:>. 0 ......, VI 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA,W]W175.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10:48:01 through 14-5EP-2016 12: 00:00 3143.00 through 3223. 00 . . . . . . 3200 .......................... ' ................................................ . . . . CD tj" .n I D )-a::: x x x x x x x LlJ 3180 z . . . . . . .............................................................. ' ............ . . . . . . . LlJ ::..::: a: w* 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ,_. 0\ ,_. Vi 0 ......, Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B175.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:05:20 through 14-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' ' 1 ' ' ' ' .' ' ' ' 1 ' ' ' o o ' 1 ' ' 1 1 o o o 1 1 o *, o 1 1 o o o o ' o o o : 1 1 o o o 1 1 o o o o 01 o ' o 1 1 o o o o 1 o *' o o o 1 o . . . . . . . 06 O o o o o o I o O O o o o o o I O o o o o I I O o o o o o O o I I o O o o o o o o O I O O O o o o o o o o o O 0 0 I o o o o I o o o I 0 I o o o o o I I . . . '04 . . I 02 ° 0 0
0 0 0 0 0 0 0 : 0 0 0 0 0 0 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 ', 0 0 0 0 0 0

0 0 0 0 ." 0 0 0 *. 0 0 0 0 0 0 0 ,' 0 0 0 0 0

0 0 0 0 0 '0 0 " 0 0 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA,W]W176.QAF;3 AVRGEFF (Average Efficiency) 14-MAR-2016 10: 48:05 through 14-SEP-2016 12: 00:00 0. 250874 through 0.266392 I 265 * ' * * * * ' * * * *"' * * * * * * * * * * ., 0 0 0 * ' *

0 0 0 0 "* * * * * * *

0 * * *"' 0 0 0 0

0 * * * * * *' * * * *

0 * * * *

00 0 0 0 0

x (..). c I]) *ri . 26 (..) *ri 4-4-UJ I]) x "o.O (lj I]) x x > a: x . 255 ........... ........... : ............ : ........... ........... : .... x ....... : ..... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W176.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 10:48:05 through 14-SEP-2016 184. 000 through 204. 000 200 ............................... ' ........................................... . . . . . . . I D )-I-H > H x I-u x cr: w D H x x ...J u :=i x x z 190 ........... :* .......... *:* .......... *:* .......... :* .......... *:* .. *x ...... *:* .... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
...... 0\ ...... 00 0 >-+, Vl 00 0 l.O QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10:48:05 trrough 14-SEP-2016 12:00:00 5. 00000 through 100.000 . . . . . . 80 .................................................................... ' ...... . .,-1 I Cl z 0 H ::i ...J 0 (f) LLJ O:'. ::..::: a: LLJ 0.. . . . . . . 60 ' 0 o o 0 o 0 o o o o o o o o 0 ' o o o o o o o o o o o o 0 o I o o o 0 0 o 0 o o o I o o o o o o o o o o I o o 0 0 I o 0 0 o o o 0 o o o o o o o o o o . . . . . . x x x x x x x 40 ' < o o 0 o 0 o o o o o o o o o o o o o o o o o o o o o o o o I o o o o 0 o o o o o o o o o o o o o o o o I o 0 o 0 I o o o o o o o o o o o o o o I o o . . . . . . 20 ........... , .................................... , .............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W176.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10:48:05 through 14-5EP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 ............................................................................ CD tj" "<""I I D C!:I >-C!:I 0::: x x x x x x x LU 3180 z . . . . . ............................................................................ . . . . . . . LU ::..::: ([ LU ll. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B176.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13: 05:25 through 14-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP . 0*8 ' ' o o o I ' 0 o o I I o o o I I o o o o I o o o 0 0 0 0 o o I I o e o I I o o 0 o I o o o o I I o o I I ' o o I I I o o o I I o o 'o 0 o I o o o I o . . . . . . .06 . . . . . . o o o o o o o o o o I I o o O I o o o o O o o o o I o o o o O o I o o e o o o o o I o o o o
o I o o o o o o o o o o o o o I I o o o o o o o o o o o o . . .04 .02 ............................................................................ . . . . . . 0 ......... ......... ___ ......... .,__ .......... _.,...---__ --;.,,__ __ ........ ____,,,..,__.......__, _______ .,__.....----"-"'--....,__ 3-16 LOW 4-16 5-16 6-16 7-16 8-16 MeasureMent Date/TiMe QA filenalY'le ParalY'le ter NalY'le start I End oa*tes Lower/Upper LMts: x DKA100: [ENV_ALPHA.QA.W]W177.QAF;3 AVRGEFF (Average Efficiency) 14-MAR-2016 10: 48:09 through 14-SEP-2016 12:00:00 0.258414 through 0. 274398 x x .27 o' o o o o o 0 I .. o o o o o o o o 0' 'o' o o o o o o o 0 I 0 'o' I I 'X' e o o o o ," o o o o o o o o o ** o,o 0 o o I Io o o o o ',' o o o Io x x :::-, (..) c ID *ri (..) *ri 4-4-UJ ID x x "0.0 i(i . 265 . . . . . . o o o o" I o o o o o I o o 0 0 o o o o o o o o o o 0 o e o o o o o o o o o e 0 0 0 I 0 o o o o o o o o o o o o o o I o o o I I o o o o o o o o o I I 0 ID > a: . 26 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... °' N N 0 ......, VI 00 0 ID QA filena!Y'le Para!Y'le ter Na!Y'le Start/End Dates Lower/Upper LMte: DKA100: [ENV_ALPHA.QA,W]W177.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 10:48:09 through 14-SEP-2016 12: 00: 00 184.000 through 204.000 200 ........... .' .......... " ........... " ........... ' ............ * ............ * .. : .. I D CJ )-t-H > H t-u a: w D H ....I u ::i z x x x x x x x . . . . . . 190 ............................................................................ x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeaeureMent Date/Ti!Y'le UP LOW QA filenaMe ParaMe ter Name Start/End Dates Lower/Upper Lmts: DKA100: [ENY-ALPHA.QA.W]W177.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10:48:09 through 14-SEP-2016 12:00:00 5, 00000 through 100.000 100 UP o:-1 I D z 0 :::) _J 0 (f) w 0::: a: w 0.. 80 ........... * ............ * ............ * ........... * .... *-....... * ............ * ..... . 60 . . . . . . ............................................................................ . . . . . . x x x x x x 40 x . . . . . . . ....................... * .... *x* ...... * .......................... * ................. . 2.0 o o o o o o ' o o 0 o I' o o o I o o o 0 0 o 1, o o o I o o o o o I 0 'o o o o o o 0 0 I o o o I' o I 0 o o o o o o o I ,o o o o o I o o o o o o o' 0 o o ' o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurement Date/TiMe QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W177.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10: 48:09 through 14-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 .......................................... ' ................................ . . . . co ""'" .....! x I D (!) )-(!). O:'. LLJ 3180 z x x x x x . . . . x . ............................................................................ . . . . . . x LLJ ::...::: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW ...... 0\ N Ul 0 ....., Ul 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.8]8177.QAF;2 ParaMeter Na-Me BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13: 05:29 through 14-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 . 08 ' ' ' o o o ' o o o ' o o o o ' ' o o o o 0 0 o o o 0 0 o o o o 0 o o o o I o o o o o o o o o o I o o o o o o o o 0 o o o o I o o o o 0 o o o o o I 0 o . . . . . . . 06 . . . . . . o o 0 0 o o I 0 o o o o '
o I 0 o o o o I I o o o o o o o o 0 I o o o I I o o o o o 0 o o o o 0 0 o o o o o I o o I o 0 o o o o o 0 o o o o o o o o o . 04 . . . . . . . 02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-0\ N 0\ 0 ....., Vl 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/ End Da-tes Lower/Upper LMts: DKA100: [ENV_ALPHA.QA,W]W178.QAF;3 AVRGEFF (Average Efficiency) 14-MAR-201610:48:13 through 14-5EP-2016 12: 00: 00 0.266941 through 0.283453 . 28 ........... * ............ * ............ * ........... * ............ * ............ * ..... . 0 c Q) *r-1 0 *r-1 4-4-UJ Q) "O.Q l(i I]) > a: x x x x x . 275 . . . . . . ......... -................................................................. . x x . 27 . . . . . . ............................................................................ . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W178.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 10:48:13 through 14-5EP-2016 12:00:00 184. 000 through 204.000 200 ........... .' .......... * ............ *.* .......... .' ............ * ............ * .... . I 0 )-I-H > H I-u x x a: x w 0 H ...J u x x x x ::i z 190 ........... * ............ * ............ * ........... * ............ * ............ * ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... °' N 00 0 >-+, Ul 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W178.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10:48:13 through 14-SEP-2016 12:00:00 5.00000 through 100.000 x . . . . . . 80 o o o o o o ' o o o ' ' o o o o o o o 0 o o o o o o o o o o o o o o o 0 I 0 o o o o o o o o o o o o o o 0 o o o o o o o o o o o o o 0 0 I o o o o o o o o:-1 I 0 (!:I z 0 H ::i ....I 0 (.f) w O:'. ::..::: a: w. 0... x x . . . . . . 60 0 I 0 o 0 o o o o o o o o o o o o o o o o o o o o o o o o 0 o I I 0 o o 0 0 0 o o o o o o o o o o o ,-, o I o o o o o o o o o o o o o o o o o o o I o o . . . . . . x x x x . . 40 o 0 0 o 0 0 0 o o o o o o o o o o o o o o o o o o o o o o 0 o 0 0 o o o I o o o o o o o o o o o o o o 0 0 I o o 0 I 0 o o o o o o o o o o o o 0 o ' 0 o . . . . . . 20 ........... , .......... " ........................ , .............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W178.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10: 48:13 through 14-SEP-2016 12:00: 00 3143.00 through 3223.00 322'0 .. * ......... ' .................................... ' .............................. . 3200 . . . . . . o I 0 o o o o o o o o I o o o 0 I o o o o o o O o o I O O 0 o 0 o o o o I o o o o O I o o O o I I 0 0 o o o o o o o o o o o o o o 0 o o I 0 0 0 o o o o . . . . . . co v* T"i I D (!:I x }-(!:I 0:: LL.I 3180 z x x x x x . . . . . x . I I 0 o 0 0 o 0 o o o I o 0 0 0 I o 0 o o o o o o o O o O o 0 0 0 o o 0 I I o o o o o o o o o o o o o o o o o o o I I o 0 o I I 0 o 0 o o o o o o o o o . . . . . . . LL.I <I: LL.I 0... 3160 .. 3-.:16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B178.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Date8 4-MAR-2016 13: 05:33 through 14-SEP-2016 12: 00:00 Lower/Upper LMt8: O.OOOOOOE+OO through 0.100000 UP .08 ............................................................................ . . . . . . .06 . . . . . . ............................................................................ . 04 .02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe Pararrieter NaMe Start/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 10-MAR-2016 08:08:34 through 14-SEP-2016 12: 00: 00 0.258303 through 0. 274280 . . . . . . . 27 ............................................................................ . . . . . . ::., u c Q) *r-i u *r-i 4-4-UJ x Q) "O!) . 265 '° S-Q) > a: x x x x x . . . . 26 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ,._.. O'I \.;J N 0 ......, VI 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W179,QAF;5 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 10-MAR-2016 08:08:34 through 14-SEP-2016 12: 00:00 184.000 through 204, 000 200 0 0 o 0
o I o o o o o o o o o o e o o o o 0 o 0 o o o o o o o o o o o ' o o o o 0 0 o o o o o o o o o o o o 0 0 0 I 0 o 0 o o o o o o o o o 0 o I 0 o . . . . . . I D )-I-H > H I-u x x x x x a: x LU D x x H _J (j ::i z 190 0 0 o 0 I 0 0 o o 0 I 'o o 0 o I o e o 0 o o ... o o o o o o o o o I o o' 0 I I o o o o I o o o ', o o o o o o 0 o 0 o I '1 o o o o o o o o o o o 'o o o 0 o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
-0\ w w 0 H) Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 10-MAR-2016 08:08:34 through 14-SEP-2016 12: 00:00 5.00000 through 100.000 100 UP .,-! I D (!) z 0 H :J _J O* U') w 0::: ::..! a: w 0.. 8*o * .. * * * * * * * * * *. * * * * * * * * * * ** * * * * * * * * * * * *** * * * * * * * * * * *. * * * * * * * * * * * *. * * * * * * * * * * * *. * * * *
60 . . . . . . o ' o o o o o o o o o o o o o 0 0 o o o o o o o 0 0 o o o o o o o o o o I o 0 o o o o o o o o o o o o o 0 o o o o 0 I o o o o o o o o o 0 o o o o o o o . . . . . . x x x x x x . . . . . . 40 .................................................................... ' ...... . . . . . . . 20 ........... , .......... '* ........... '* ........... ' ........... *' ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW Measurer.-.ent Date/Tir.-.e QA filenal'le Paral'leter Name Start/End Dates Lower/Upper Lmts: 3220 DKA100: [ENV_ALPHA.QA.W]W179.QAF;5 P5ENERGY-GD148 (PEAK ENERGY GD-148) 10-MAR-2016 08: 08:34 through 14-5EP-2016 12:00:00 3143.00 through 3223.00 3200 ........ : .. * ............ * ............ * ........... * ............ * ............ * ..... . . . . ro ""'" I D (!) )-(!) et:: xx x x x x x x LlJ 3180 z . . . . . . o o o o o ' o o o o o o

o o o o o o o o o 0 o o o o o o o o o o o" ' 0 o o o o o o o ' o ' o o o o o o 0 o o o o o o o o I 0 o o o o o o o o o I o o . . . . . . Ll.J" :..:: a: LlJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW
....... 0\ VJ VI 0 ....., VI 00 Cl \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B179.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:05:37 through 14-SEP-2016 12:00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 .08 ............................................................................. . . . . . . .06 . . . . . . o o o o o 0 o o o o o ' 0 o o ' o o 0 o 0 I o o o o I 0 o o o o I 0 o o o I o o o o I o 0 0 o o o o o o I I 0 0 o I o o o o I 0 0 o o I I o o 0 0 0 o I .04 .02 ............................................................................ . . . . . . 0 ............ __....__,..,._....., ____ ........ .__.__ ......... __,...._ .......... 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... 0\ VJ O"I 0 ......., Vt 00 0 \0 QA filenafY'le ParafY'leter NafY'le Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W180.QAF;3 AVRGEFF (Average Efficiency) 10-MAR-2016 08: 08:37 through 14-SEP-2016 12:00:00 0.256445 through 0.272307 I 27 ' ' ' 0 o 1 0 0 0 0 0 .. 0 0 0 0 0 0 0 o 0 0 '* 0 0 o 0 1 0
0 0 0 0 '* 0 ' 0 0 0 0 0 0 0 0 o /' 0 0 0 0 0 0 o 0 0 0 o 00 0 0 0 o o o 0 0 0 0 0 00 0 0 o 0 o :::>, 0 c I}) -r-1 0 -r-1 4-4-UJ x . . . . . . .265 ***********:***********.************.****x******:***********:***********:***** . . . . x x x x x x . 26 . . . . . . .......................................... ' ................................ . . . . . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W180.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 10-MAR-2016 08:08:37 through 14-SEP-2016 12: 00: 00 184.000 through 204. 000 200 ............................................................................ . . . . . . I 0 (!) )-I-H > H x I-x u a: x w 0 H x _J x x u ::i x z 190 ... *x* ..... :* .......... *:* .......... *:* .......... :* .......... *:* .......... *:* .... . . . x . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOli.J
-O'I \;.) 00 0 ......, Vt 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W180.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 10-MAR-2016 08:08:37 through 14-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ............ * ........... * ............ * ............ * ... ' .. ..-! I Cl z Cl H 1-:J ....I Cl (f) w O:'. :::.! a: w 0.. . . . . . . 60 ............................................................................. . . . . . . x x x x x x x x x 40 o o I o 0 0 0 0 *
0 I o 0

o I o o o I I I I I o o o o 0 0 0 o o o o 0 o 0 0 o o I I o

o I 0 0 0 o I 0 0 0 I I I o o 0 o I o o o o o o Io o o I o . . . . . . 20 ........... , .................................... , .............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOl.i.J QA filena!Yle Para!Yleter Na!Yle Start/End Dates Lower/Upper LIYlts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 10-MAR-2016 08: 08:37 through 14-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ..................... ' ..................................................... . . . . co """ ...-! I D. )-(t'. xx x x x x x x x LLJ 3180 z . . . . . . o o o o 0 o o o o o 0 0 o o o o o o 0 o o o o o o o o o o o o 0 o o o o 0 o o 0 o o o o o o o o I o o o I I o o o ' o o o I ' o o o 0 o o I o o o 0 I o o o o I o I LLJ ::,..:: > u c ID *r-1 u *r-1 4-4-w . . . . . . x o I 0 I o I . 26 o I o o 0 I I o o o I I 0 0 o o o o O o 0 o o o o o O o o o o I I o O o o o o o o O I O O O o 0 o o o o I o O o o I I o o o I I 0 o o o o I o o I I I o 0 0 o I ........... * ............ * ............ * ........... * ............ * ............ * ..... . '255 3-16 4-16 5-16 6-16 7-16 8-16 9-16 . MeasureMent Date/TiMe UP LOW
-°' .j:::.. N 0 ......, Vi 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W181.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 10-MAR-2016 08:08: 42 through 14-SEP-2016 12: 00: 00 184.000 through 204. 000 200 ........... .' .......... * ............ * .......................... * ............ * .... . I D )-1--H > H 1--u <I w D H ...J (j ::i z -x x x x x x x x 190 ........... * ........... ,* ............ * ........... * ............ * ............ * ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 10-MAR-2016 08:08:42 through 14-SEP-2016 12:00:00 5. 00000 through 100.000 80 I I I o o o o o o o I', o o o o o ' 0 o I o o' o o o o 0 0 0 o o o o o' o o o 0 o 0 o o I o o 'o o o o o o o o 0 e o 0 ', o o o o o o o o o I o 'o o o ' o o -M I D (!) z 0 H 1-::J ...J 0 O") w 0:::. . . . . . . 60 ..... ' ..................................................................... . . . . . . . x x x x x x . . . . . . 40 ........................................................... ' ................ . . . . ' . . 20 ........... , .......... '* ........................ , ........... *' ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Oates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W181.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 10-MAR-2016 08:08:42 through 14-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 ............................................................................ co "'" "<""i I D )-et:: xx x x x x x x L1J 3180 z 0 o I o o ............................................................... ' ............ . . . . . . . L1J ::...::: a:. L1J 0.. 3160 3-16. 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... Vl 0 ......., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.8]8181.QAF;1 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:05:44 through 14-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 .08 ............................................................................ . . . . . . .06 . . . . . . I o o o o o 0 o o o ' o o o o o o o 0 o o o o o o o o o o o o o I o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o 0 o o o o o o o .04 . . . . . . . 02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 x x x *x x 9-16 MeasureMent Date/TiMe UP LOW QA filenal'le Paral'leter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W182.QAF;3 AVRGEFF (Average Efficiency) 10-MAR-2016 08:08:46 through 14-SEP-2016 12:00:00 0. 215980 through 0. 229340 . . . . . . x '225 ............................................................................ >, u* . . x . c Q) *r-1 x u *r-1 4-x 4-UJ Q) "OJ) (lj I-Q) > x a: x '22 ........... * ............ * ............ *. ' ......... * ............ * ............ * ..... . x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til'le UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W182.QAF;3 NLACTVTY-GD148 (NUCLIDE GD-148) 10-MAR-2016 08: 08:46 through 14-SEP-2016 12:00:00 184.000 through 204.000 200 ........... .' .......... " ........... * ............ .' ............ * ............ * .... . I D (!:I )-x I-H x > H I-u xx x x a: w D H x x x ...J u ::i z 190 ........... * ............ * ............ * ........... * ............ *, ........... * ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenafY'le ParafY'leter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W182.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 10-MAR-2016 08:08:46 through 14-SEP-2016 12:00:00 5.00000 through 100.000 . . . . . . 80 0 I 0 o 0 0 I o o o 0 o o o o o I o o o o 0 I I 0 0 o o o o o o o o o o o o o I o *
o o o o o o o o o o o o o 0 I 0 o o o o o o o o o o o *

o 0 0 o ..-1 I Cl C) z 0 H :J ....J 0 U') w Ct'. ::,,,::; a: w 0... . . . . . . 60 I I o o o I I I o o I I 0 0 o 0 I o 0 I o 0 o o o o o o o o o o o o I o I o 0 I 0 o I o 0 o o o o o o o o o o o o I I 0 0 o o 0 O o o o o o o o o o o I . . . . . . x x x x x x x x x . . . 40 0 I 0 o o 0 0 0 o o I o o 0 o o I o o o o o o o o o o o o o o I o o 0 0 0 o o o o o o o o o o o o o o o o 0 o I 0 I I o o o o o o o o o o o o Io I 0 0 . . . . . . 20 ........... , ....................... '* ........... ' ........... *' ........... " .... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W182.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 10-MAR-2016 08:08:46 through 14-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 o o o o o I o o o o o o o o 0 I 0 o o o o o o 0 o o o o o o o 0 I 0 o o o o o o o o I o 0 0 o 0 o o o o ' o o o o 0 0 o o o o o o o o o 0 o 0 o o o o o . . *xx x x x x x c.o tj" ........ I D (!) )-(!)* 0:: LLJ 3100 z . . . . . . ............................................................................ LLJ a: LLJ CL x 3000 . . . . . . o o o o O I o o o o o o o o o o o o o o o O o o o o o o o o o O o o o o o o o O o o o o o o o o o o o o

I o 0 o o o o o o o o o 0 I 0 I o o o o o I o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B182.QAF;1 ParaMeter NaMe BACKRATE (Background Rate) Start/End Date8 4-MAR-2016 13:05: 49 through 14-SEP-2016 12: 00:00 Lower/Upper LMt8: O.OOOOOOE+OO through 0.100000 . o-s . ** ..................... * ............ * .......................... * ............ * .... . . . . . . . . 06 ' ' o o o o o o o o ' ' o o o I o o o o o I o o o o ' o o o o o I o o o 0 I o o o o I o 0 o o I o o o o o ' 0 o o o o o o o I I o o o o I o o 0 o o o o . 04 . . . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Mea8ureMent Date/TiMe UP LOW 0 Hi U'i 00 0 \0 QA filenar.-.e Parar.-.e ter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: . 26 :::-, DKA100: [ENV_ALPHA.QA.W]W184.QAF;3 AVRGEFF (Average Efficiency) 14-MAR-2016 10:48:38 through 14-5EP-2016 12: 00:00 0.245385 through 0. 260560 x . . . . . . 0 . 255 o o ' 0 o o o o o 0 0 o o o o o o o o o o o o 0 0 o o o o o o 0 0 0 o o o o o o o o I 0 o o o o o o o o 0 I o o o o o o o o o o o o o o o o o' o o o o c . . . . . . . ID *r-i x x 0 *r-i x 4-4-LU [I "OJ) l1j x l-ID > <C .25 x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafYle ParafYleter NafYle Start/ End Da_tes Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W184.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 14-MAR-2016 10:48:38 through 14-SEP-2016 12: 00: 00 184. 000 through 204.000 200 ........... .' .......... " ........... " ........... ,' ........... " ............ * .... . I D (!) )--I-H > H I-u a: x LL.J x D x H __J x x u ::r x z 190 ..... ' ..... * ............ * ............ * ........... * ............ * ............ * ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifYle UP LOli.I
...... O'I Vl w 0 ......, Vl 00 0 "° QA filena!Yle Para!Yleter Na!Yle Start/End Dates Ldwer/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W184.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 14-MAR-2016 10:48:38 through 14-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ............ * ........... * ........... '* ............ * ..... . I D (!:! z 0 H ::i -I 0 ([) LLJ O:'. :::.::: a: LLJ* 0... . . . . . . . 60 o o o o o o o o o o o 0 o o o o I o o o o 0 I o o o 0 0 o o o o I 0 o o o o 0 o o o o o 0 o o I o o o o I I o o
o o o

o o o 0 o o o o o o o o o o o . . . . . . x x x x x x . . . 40 ............................................................................ . . . . . . 20 ........... , .......... " ........................ , ........... " ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Ylent Date/Ti!Yle UP LOW QA filena!Y'le Para!Y'leter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 14-MAR-2016 10:48:38 through 14-SEP-2016 12: 00:00 3143. 00 through 3223. 00 . . . . . . 3200 0 0 0 o o I I o o o 0 o o o o o I o o o o 0 0 o o o 0 o o 0 0 0 o 0 o 0 I 0 o 0 o o I ' o o ' 0 0 o o o 0 ' o o o 0 0 o o o o o o o o o o o o o o o ' o co ¢ T""I I D (!) )-(!) 0:: x x x x x x LU 3180 z . . . . . . ............................................................................ . . . . . . LU <I: LU 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-0\ Vl Vl 0 ....., Vl 00 0 \0 QA filenar.-.e Pararrieter Narrie Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.B]B184.QAF;1 BACKRATE (Background Rate) 4-MAR-2016 13:05: 57 through 14-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 x 400 ........... * ............ * ............ * ........... * ............ * ............. * ..... . ID r'(i O:'. "D c :J 0 '0.0 ::t. 0 l1j co . . . . . . 300 ............................................................................ . . . . . . 200 . . . . . . . . . . . .. . . . . . . . . . . . . . . . . .. -. . . . *. . . . . . . . . ... : . . . . . . . . . . . .* . . . . . . ...... * .. : . . 100 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TiMe UP QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W185.QAF;3 AVRGEFF (Average Efficiency) 19-APR-2016 15:41:25 through 16-SEP-2016 12:00:00 0. 246814 through 0.262080 I 2*6 ' '_' ' ' I 0 ' 0 ' ' ' 011 o
I o I o o o o o o o 001 o o o I o o o o I I O O : o I o o I o 1 I o o o o 1 .. o o o I o o o 1 o 0 0 o 0 .' I o o o 1 1 0 >> u c Q) *r-1* u *.-! 4-4-LU Q) "0.0 Ill Q) . 25 x x x x x x UP > LOW a: I 24 ° 1 0 0 0 0 0 0 0 0 0 * *'* 0

0 0 0 0 0 0 0 0 0 0 *'* 0 0 0 ' ' 0 0 0 0 0 0 0 I 0 ' 0 0 ' 0 ' ' ' 0 ' ' ' ... ' ' ' ' ' ' ' ' ' * * * * .. '* * * * *

4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifYle QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W185.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 19-APR-2016 15:41:25 through 16-5EP-2016 12: 00: 00 184.000 through 204.000 200 ............ *.* ............ *.* ............ : ............. .' ............. .' ...... . I D (!) )-I-H > H I-x u a: w x x D H _J u ::i z x 190 ............ *:* .......... x *:* ............ : ............. :* ..... *x ...... :* ...... . . . x . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tir.-.e UP LOW QA filena!Yle Para!Yleter NaMe Start/End Dates Lower/Upper LMta: 100 I CJ (!) z 0 H DKA100: [ENV_ALPHA.QA.W]W185.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION G0-148) 19-APR-2016 15:41:25 through 16-SEP-2016 12:00:00 5.00000 through 100. 000 I-=i 50 : : : x : x : x ......................... _x_ ::< ..... x ...... : ............. * .............. * ....... . _J 0 U') w O:'. :::..::: a: w 0.. 0 4-16 5-16 6-16 7-16 8-16 9-16 MeaaureMent Date/TiMe UP LOW QA filenaMe ParaMeter NafYle Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA,W]W185.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 19-APR-2016 15:41:25 through 16-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . . 3200 ............................................................................ . . co ""'" ...i I D (!:I }-(!:I et:: xx x x x x LLJ 3180 z. . . . . . ............................................................................ . . . . . LLJ x ::..:: a: LLJ 0.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.8]8185.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:16:31 through 16-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0. 100000 I 08 ' '

1

o o ' 1 * '01 o 1 ' o 1 1 ' ' ' o 10' 1 ' 1 1 o 0 o o 1 ' : ' 1 ' o o ' ' 1 1 ' ', o 1 1 0 o ' 1 1 ' o ' 10 1 ' ' o 1 1 o 0 o o 1 : o o o o 1 o . . . . . . . 06 o o o o I o o o o o o o o e o I 0 o I o 0 0 0 o o o 0 o o o o o o o e o o o o o o o I 0 0 o o o o o o o o o o o o o o o o o I 0 o o o o o o o o o o o o . 04 . . . . .02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... 0\ 0\ ....... 0 ....., Vl 00 0 "° QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper lMts: DKA100: [ENV_ALPHA.QA.W]W186.QAF;4 AVRGEFF (Average Efficiency) 12-MAY-2016 09:14:47 through 16-5EP-2016 12: 00: 00 0.247066 through o. 273072 . . . . .27 ............................................................................ >.. (..) c ID *r-1 (..) *r-1 4-4-UJ
26 ................................ '* ............................................ . ID "OI) Ill Q) > (( x x x)< x x x x x I 25 *

0 0 0

0 0 0 0 0 0 0 0 0 0 : 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ,' 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 .* 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ,* 0 0 0 0 0 0 0 0 0 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W186.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 12-MAY-2016 09:14:47 through 16-SEP-2016 12:00: 00 184.000 through 204.000 200 ................ : ............... " ................ * ................. * ......... . I 0 )-I-H > H I-u <I: w 0 H ...J u :J z x x x x x x 190 ................ : ............... "* ...... *X* ........ * ................. * ........ . . . . . . 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenal'Ie Paral'Ieter Nal'Ie 5tart/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W186.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 12-MAY-201609:14:47 through 16-5EP-2016 12:00:00 5. 00000 through 100. 000 . . . . 80 o o o

o 0 0 o o o o o o 0 o o o o o O 0 I 0 o o o O I o o o I I o O O I o o o o o I o O o o 0 I o 0 o I o o o o I 0 0 o o o o o o o o 0 o o o o I o o ........ I Cl C) z 0 H ::i __J 0 (f) w O::'. ::..::: a: w 0.. 60 40 . . . . 0 I 0 o o o o o 0 o o o o o o I I o o o o I o o o o o o o o 0 0 o o o o o o o 0 o o o o o o o o o o 0 o o o o o o o ' 0 0 o o o o o o o 0 0 o o o o o o x . . . . x x x x x ' o o o o o o o o o I 0 0 o o o I 0 0 o o o o o 0 0 I o o o o o I o o o o o o o o o I 0 o o o o o o o o I 0 o o o o o o o 0 I I o o o o ' 0 0 o o o o o . . . . 20 .............................................................................. . 5-16 6-16 7-16 8-16 9-16 Measurel'Ient Date/Til'Ie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 12-MAY-2016 09:14:47 through 16-SEP-2016 12:00:00 3143.00 through 3223.00 . ' . . 3200 I I ' I I I I I I o I I I I o I I I o o o I I o o 0 0 o 0 o 0 I o o o o o I o o o o 0 o ' o ' I I o e o I o o o o o 0 0 0 ' I I o o o o o o o o o I 0 o co """" "<"i I D )-et: x x x x LLJ 3180 z . . . . ............................................................................ . . . . LLJ ::..::: <I: LLJ 0.. 3160 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA. QA. 8]8186. 2 BACKRATE (Background Rate) 20-APR-2016 12:57:24 through 16-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 I I I I I I I 0 I I I I 111 0 I I o o o I I o o I o 111 o o o 1 o o I o I 1 I o : o 1 o o o o o o o I, o 1 I .. 1 1 1 1 1 1 1 O O O I 1 1 .' 1 1 1 I I I 0 . . . . . . 06 I I o o I I I I o I o I I o o I 0 I o o I I o I I I I o I o o I I I I I I I o o I I o I I I I o o I I I I I o I I I o o o I o o I I I I I o o o o o I I '04 . . . '02 ............................................................................ 0 4-16 . . . . . Xx X* X X X X *X X X X X X X X X* X X X X *x X 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
.... O'I O'I O'I 0 ......, VI 00 0 l.O QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W187.QAF;4 AVRGEFF (Average Efficiency) 15-MAR-2016 14:48:31 through 16-SEP-2016 12:00:00 0.248323 through 0. 263683 . 26 1 o
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o ' * ' ' ' ' ' ' ' ' ' I ' ' ' ' ' ' ::., 0 c Q) *.-i 0 *.-i 4-4-" UJ Q) -0.0 . 255 JU I-x x Q) x > a: x x x x .25 -. . . . . . I I o O O I O o o o I o o O o I o I o I I O o o O o I I o o o o I o o o o o o o o o o o o o o o o o o o 0 I o I o o I o I 0 I I 0 I I I I I 0 I I I I I . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W187.QAF;4 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 15-MAR-2016 14:48:31 through 16-SEP-2016 12:00:00 Lower/Upper LMts: 184. 000 through 204.000 UP 200 ' '

o o o o o o o o ' o o o o o o o o o o O o o o o o O o o o o o o o o o o O O o o o e o o o o o o o 0 I o o o o I 0 o o o o 0 0 o o o O 0 o o o O o . . . . . . I 0 (!) )-I-H > H I-u <I: x x w 0 x H ....I x u ::r z 190 .... *x .... *:* .......... *:* .......... : ... *x* .... *:* .......... *:* .......... : ..... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
,_. 0\ 0\ 00 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter Nal'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W187.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 14:48:31 through 16-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ........... : ........... * ............ *' .......... : ..... . ..-! I Cl z 0 H :J ....I 0 (f) LLJ O:'. ::..: a: LLJ 0... . . . . . . 60 I I o o 0 o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o O O I I O o o o O o o o o o o o o o o O o o O o O O o o o o o o o o o o o o o o o o . . . . . . x x x x x x x . . 40 o ' o o o o o o o o o o o o o o o o o o o o 0 0 o ' o I 0 o o 0 0 0 o o o o o o o o o o o o o o o o o o o 0 o o 0 I I o o o o 0 o o o o o o o o o o o o . . . . . . 20 ............................................................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W187.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 14: 48:31 through 16-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ co "'1" "' I 0 )-0::: x x x x x* x x LL.I 3180 z . . . . . . ............................................................................. . . . . . . LL.I ::...:: a:* LL.I CL 3160 3-16-4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B187.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:16:35 through 16-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 o 1 o o 1 1 o ' ' 1 1 01 ' o 1 1 ' o o o ' 1 10 1 o 1 o ' o ' o 1 1 o : ' ' ' o o ' 1 1 o o *, 0 1 o o o o 1 1 o o o 10 o o o o 1 1 o 1 o o 1 : o o o 1 1 o . 06 ........... * ............ * ........... : ........... * ............ * ........... : ..... . . -. . . 04 . . . . . I 02 ' 0 0 0 0 0
0 0 0 0 00 0 0 0 0 0 0 0 0 0 * ', 0 0 0 0 0 0 0 0 *

0 : 0 *

0 0 0 0

0 0 ', 0 *

0 0 0 0

0 0 0 00

0 0 0 *

0 0 0 0 * : 0 0 0

0 0 O X X X X X X X X X* X X X X *X X X X X X 3-16 4-16 5-16 6-16 7-16 x x* x x x x -x x 8-16 9-16 LOW MeasureMent Date/TiMe
-°' -..J -QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W188.QAF;3 AVRGEFF (Average Efficiency) 15-MAR-2016 08:38:24 through 16-SEP-2016 12: 00:00 0. 257260 through 0.273174 I 27 ' ' ' o o ' O ' o o o ,' o o o o o o o o o O 1' o o e 1 1 O o o o o o : o o o o 0 o o o o o ', o o O o 0 O 1 o o o o 1' O o o o I 1 o o o o o : o o o 1 1 o >.. 0 c IJ) *n 0 *n 4-4-UJ x . 265 ........... * ............ * ........... : ........... * ............ * ........... : ... ':' .. . . x x x x x x . 26 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W188.QAF;3 NLACTVTY-GD148 (N_UCLIDE ACTIVITY GD-148) 15-MAR-2016 08:38:24 through 16-SEP-2016 12: 00:00 184.000 through 204.000 200 ............ * .......... * ............ : .......... * ............ * ............ : ..... . I Cl (!) )-I-H > H I-u a: x LLJ Cl H ....I u x x :J z x x 190 o ' o o o ' ' o 0 o 0 'o o o o o ' o o o o o o' 0 0 o ' o o o o o o o: 0 0 0 o o o o o o o o' o 0 0 o o o o o o o o 1' I o o 0 o o o o o 0 0 : o o o I o o x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tir.-.e UP LOW QA filenaf"l"Je ParafYleter NafYle Start/End Dates Lower/Upper LfYlta: 100 DKA100: [ENV_ALPHA.QA.W]W188.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:38:24 through 16-SEP-2016 12: 00:00 6. 00000 through 100.000 80 ........... * ............ * ......... ' . : ........... * ............ * ........... : ..... . ""'"" I D z 0 H 1-:J ....I 0 ({) Ll.J 0:: ::>.! a: Ll.J 0... x x x x x x 60 . . . . x . . o o o 0 o o o o 0 o o o o o o o o o o 0 o o o o o 0 o o o o o I o o o o o 0 0 o o o ' o o o ' o o o o o o I o o o o o 0 0 o o o o o' ' o o o o o o o o . . . . . . . . . 40 o o o o o o o o o o o o o o o o o o o o o o o o o o o o ' o o o o o o o o o o o o o o o o o o o o o o o ' o o o o o o o o 0 0 0 o o o o I o o o o o I o . . . . . . 20 ............................................................................... . 3-16 4-16 6-16 6-16 7-16 8-16 9-16 MeaaureMent Date/TifYle UP LOW QA filenafY'le ParafY'leter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W188.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 08:38:24 through 16-SEP-2016 12: 00:00 3143. 00 through 3223.00 3200 ........... * ........... : ........... : ........... * ............ * ........... : ..... . co ""'" "<""I I D >-CJ:: x x x x x x x LiJ 3180 z . . . . . ........... : .......... * ............ : .......... * ............ * ............ : ..... . LiJ ::..:: q: LiJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B188.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:16: 39 through 16-SEP-2016 12: 00: 00 0. OOOOOOE+OO through 0. 100000 I 08 ' .. o o o ' ' o o o O o' o o o ' ' O O o o ' ', o o o O I O o o o o o: O O I O o o o 1 o o 1, o I O o O o 1 1 o o o 10 I 1 1 0 0 0 ;, o o o I : o I
I o o . . . . . . . 06 ............................................................................ . . .04 . . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: AVRGEFF (Average Efficiency) 15-MAR-2016 08:38:28 through 16-SEP-2016 12: 00:00. 0. 250152 through 0.265626 . 265 o ' o 0 o I o o o o o 'o o 0 0 0 0 o o o o o o' o o o o o o o o o o o : o o o o o ' ' I 0 o o' o I I o o o I I o o o o' I o o I 0 ' o 0 o o I : o o e I o o ij .26 c . . . . . . ............................................................................ . . . . . . Q) -rt ij -rt 4-x x x 4-UJ Q). "O.l) x iU f.-Q) > a: . 255 ........... : ............ : ........... ; .... x* ..... : ............ : .... *X ..... '. ... .. x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenafYle ParafYleter Nar.-.e Start I End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W189.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 08:38:28 through 16-SEP-2016 12: 00:00 184. 000 through 204.000 200 ............ * .......... * ............ : .......... * ............ * ............ : ..... . I 0 (9 )-I-H > H I-u a: w 0 H x x ...J u ::i x x x z x 190 I I I I I I o o I I I*, I I I I I I I I I o ,'I 0 o I I o o o o 0 o : o o o o o I o I o o o' o o o o o o 0 o I 0 0 ,' o o o o o o o o o o o : o o o o 0 o x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/TifYle UP LOW
.... 0\ -..J 00 0 ......, Vi 00 0 \0 QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA,W]W189.QAF;3 P5FWHM-GD148 (PEAK RE50LUTION GD-148) 15-MAR-2016 08:38: 28 through 16-SEP-2016 12:00: 00 5.00000 through 100. 000 80 ........... * ............ * ........... : ........... * ............ * ........... : ..... . "'""' I Cl C) z 0 H =:i ...J 0 ti) w l:.::: a: w 0.. x x x x 60 * * * * * * * * * * <* * * *
x. * * * * *> * * * * * * * * * * : * * * * * * * * * * *> * * * * * * * * * * *> * * * * * * * * * * : * * * : *x x 40 ........... : .......... * ............ : .......... * .... * ........ * ............ : ..... . 20 ....................... '* ........... ' ....... ,* ............... '* ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W189.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 08:38:28 through 16-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 0 ' o o o ' I o 0 o o I o o o I 0 o o o o I I o o o I O O o o o o o o o O O O o O o O o o o o o I o o o o O o O o o o o o o o o o I o o O o O o o o o o co '<T '<'i I D (!) )-(!) Ct: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ :..::: <C LLJ 0.. 3160 ............................................................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
..... 0\ 00 0 0 ....., Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B189.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-201613:16:43 through 16-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' * * * ' o ' ' o o 01 ' o ' ' ' ' o ' o 1 10' ' ' ' ' ' o ' ' 1 o : o ' ' o o o ' 1 o o ',' ' ' ' ' 0 ' ' ' ' ' ',' ' ' ' o ' ' ' : ' ' o ' ' ' . 06 ............ * ............ * ........... : ........... * ............ * ........... : ..... . . 04 . . . . . . 02 ............ * .......... " ........... : .......... * ............ * ............ : ..... . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/TiMe UP LOU.I QA filenarrre Pararrreter Narrre 5tart/End Dates Lower/Upper Lrrrts: x DKA100: [ENV_ALPHA.QA.W]W191.QAF;4 AVRGEFF (Average Efficiency) 15-MAR-2016 10:10:22 through 16-5EP-2016 12: 00:00 0.237611 through 0.252309 . . . . . . ' 25 ........... : .......... * ............ : .......... * ...... _ ...... * ............ : ..... . (..) c I]) ...... (..) *r-1 4-4-LlJ I]) "0.0 Ill I]) > a: . . . . . . '245 o ' o o o ' ' o o o I o o o o o I o ' o o I o o o o 0 0 o o o o o o o o 0 0 o o o o o o o o o 0 0 o o o o o o o o o I o o o I o o o o o o o 0 0 o o o o . . . . . . x x x x x x . . . . . . .24 o ' o o o o o o o o o o o 0 0 o o o o o o 0 0 o o o o o o o 0 I 0 o o o I I o o o o 0 0 o o o I o o o o 0 I o o o 0 I o o o ' I o o o o I o o o o I 0 o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW ..... 0\ 00 N 0 ......, Vl 00 0 '° QA filenaMe DKA100: ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 15-MAR-2016 10:10: 22 through 16-SEP-2016 12: 00:00 Lower/Upper LMts: 184.000 through 204. 000
UP 200 ***********.************.***********:**********-.*************.***********:****** I 0 C!:I )-I-H >" H I-u a: LLJ 0 H x _J u ::i x x x z 190 ........... * ........... " ... ,x; ...... : ........... * ........... " ........... : ..... . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W191.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 10:10:22 through 16-SEP-2016 12:00:00 5. 00000 through 100. 000 80 ........... * ............. * ........... : ........... * ........... ,* ..... ' .... ' : ..... . ..-! I 0 (!) z 0 H 1-:J ...J 0 (J) w Ct'. ::..::: a: w 0... . . . . . . 60 I 0 o o o I 0 o o o I I o o o 0 I o e 0 o I o o 0 o o o o o o I o o o o I o o o 0 o I o o o o o o o o o I I o o o o o o o o I 0 o o o o o o o o o o 0 o . . . . . . x x x x x x x . . . . . . 40 I o o o o I I o o o I I o o o o I o o o o I o o 0 o I I o o o o I o o o I I o o o o I o o o o o o o o o o o o o o 0 o o o o I I o o o o I o o o o I I o . . . . . . 20 ........... *' .................................................................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA f i lenar.-.e -Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W191.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 10:10:22 through 16-SEP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 ............................................................................ co 'OJ" """"" I D )-Ct:: x x x x x x x U.J 3180 z . . . . ..................................................... ' ..................... . . . . . . . U.J a: U.J 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tir.-.e UP LOl.d
-O'I 00 Vl 0 ....., Vl 00 0 '° QA filena!Yle Para!Yleter Na!Yle Start/End Dates Lower/Upper LIYlts: DKA100: [ENV_ALPHA.QA.B]B191.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:16:52 through 16-SEP-2016 12: 00: 00 O.OOOOOOE+OO through 0.100000 . 08 ............................................................................ l[I .µ llj O:'. 1J c :J 0 '0.0 .::£.. U. llj co . . . . . . . . . . . . . 06 ............................................................................ '04 . . . . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Ylent Date/Ti!Yle UP LOW -°' 00 °' 0 ......, Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W195.QAF;4 AVRGEFF (Average Efficiency) 15-MAR-2016 08:38:54 through 16-SEP-2016 12:00:00 0.256857 through 0.272745 . 27 ........... * ............ * ........... : ........... * ............ * ........... : ..... . >.. (.) c Q) *r-1 (.) *r-1 4-4-UJ . 265 x x x x x x x . 26 *' * * * * * * * * * :. * * * * * * * * * * .: * * * * * * * * * * *; * * *
X* * * * * .:. * * * * * * * * * * .: * * * * * * * * * * *; * * * * *

3-16* 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W195.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016.08:38:54 through 16-SEP-2016 12:00:00 184.000 through 204.000 200 ............ * .......... * ............ : .......... * ............ * ............ : ..... . I Cl (!) )-f--H > H f--u x a: LLJ x Cl H __J u x x x x ::r z x 190 . * ......... *:* .......... *:* .......... : ... *x* .... *:* .......... *:* .......... : ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-0\ 00 00 0 ....., Vl 00 0 \0 QA filenarrre Pararrreter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W195.QAF;4 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:38:54 through 16-5EP-2016 12:00:00 5. 00000 through 100.000 I* 0 (!) z D H 1-=:i ....I D r.n w O:'. ::...! H t-U* a: x w 0 x H _J x x u ::i x z 190 ............ *:* ............ *:* .... x ...... : ............. :* ............. : ...... . 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filena!Y'le Para!Y'le ter Nafl'le Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W197.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-APR-2016 10:36:28 through 16-SEP-2016 12:00:00 5.00000 through 100.000 . . . . . 80 0 I o o o o I o ' o I I o o o o 0 o o 0 o o I o 0 I I I o o o o 0 o o o o o o o o 0 o o o o ' I o o o ' o I o o o I I o ' o I I o o o o o o o I o o ...... I Cl z 0 H :J ....I 0 ([') w O:'. ::..:: a: w 0.. 60 ..... *X* ..... <* ............ <* ............ ; ............. :* ............. :* ...... . x x x x x 40 ............................................................................ . . . . . 20 .......................................... , ............. , ............. , ...... . 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Y'lent Date/TilY'le UP LOW QA filenarrie Pararrieter Narrie Start I End Da-tes Lower/Upper Lmts: 3220 DKA100: [ENV_ALPHA.QA.W]W197.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD--148) 15-APR-2016 10:36:28 through 16-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . 3200 ' ' o o o o o o o o o o o o 0 o I 0 0 0 o 0 *O 0 0 0 0 o o o o 0 o o o o o o o o o o o o o o o o o o o o 0 I o o o o I 0 o o o I o o o o o o o o o *o I o . . . . . co '<:t "<""I I D (!)* )-(!) Ct'. x x x x x x . . . . ._ " . I O o o O I I O o O I O o 1 O o I I O o o o I I o o o I 0 1, o O I o I o o o o I o o : o I o o o o o o 0 o 0 o I : o 0 0 I o o o
o o o o o : o o o o I o o I.LI 3180 z I.LI ::...:: <r I.LI a.. 3160 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrieht Date/Tirrie UP LOW
-0\ '-0 Vt 0 ,...., Vt 00 0 '-0 QA filenaMe ParaMeter NaMe Dates Lower/Upper LMts: DKA100: BACKRATE (Background Rate) 4-MAR-2016 13:17:18 through 16-SEP-2016 12:00:00 0. OOOOOOE+OO through 0.100000 I 08 ' 1 1 1
1 '

0 1 0 01 0 0 0 0 1 0 0 0 0 1 ', 0 0 0 1 1 0 0 0 1 1 0 : 0 1 1 0 *

0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 ', 1 0 0 0 0 0 0 0 0 0 0 : 0 0 o 0 1 0 . 06 . . . . . . 0 o o o o 0 o o o o I 0 o o 0 0 o o o 0 0 I I o I I o I o I o 0 I o o o 0 0 0 I o o I I 0 0 o I o o '* o I o o o o I I o o o I o Io o I I o I 0 I I I e '04 . . . . '02 ............................................................................ . . . . . . . X X X X X X X X X* X X X X : X x X X X X X X X

X X X X *X X 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
........ O'I \0 0\ 0 ....., VI 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lqwer/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W199.QAF;3 AVRGEFF (Average Efficiency) 08:39:06 16-SEP-2016 12: 00:00 0.258679 through 0. 274679 '27 ............................................................................ . . . . . . u c ID *r-1 u *r-1 4-4-LU ID "OJ) ill I-'265 ID . . . . . . ' ' o o o ' ' o o 0 0 ' o o o ' o o o 0 0 0 o o o o o o o o o 0 o o o o o o 0 o 0 o o o o o o 0 0 o o o o o o o o 0 I I o o I 0 0 o o o I o o o o I I I > a: x x x x x .26 x 1 1 ' ' ' ' ' ' ' ' ',o * * ' ' ' ' ' ' * * *, * * ' ' ' ' * * * *
I ' ' ' * * * * * ' ' '* * * * * * ' * ' ' * * *, * * * * ' ' * * * *

I * ' ' * *

x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
....... 0\ \0 -..J 0 ......, Vi 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W199.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 08:39:06 through 16-SEP-2016 12:00:00 184. 000 through 204.000 200 '
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o o o o o o o o o o o o o o O o o o o O o o o o O o O o o o o O O o o o o o o o o o o o 0 I o o o I I 0 0 o o o 0 o 0 o o O o o o o o o . . . . . . I D )-I-H > H I-u a: w D x H _J u x x x ::i z x x x 190 ........... * ............ * ........... : ........... * ............ * ........... : ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOli.I
.... 0\ \0 00 0 Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ ENV_ALPHA. QA. W] W199. QAF; 3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:39:06 through 16-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ........... ; ........... * ............ * ........... : ..... . I D (.!) z Cl H ::. ....I Cl en w Ct'. ::..::: a: w 0.. . . . . . . 60 I I o o I I I o o o o I o o o o I o o o o I 0 I 0 o 0 0 o o o o o o o o I o 0 0 o 0 I o o o o o o o e o I I o I o 0 I 0 o o I I o o o o 0 o o 0 0 o 0 o . . . . . . x x x x x x x 40 ' o o I o I o 0 I I 0 I o o o I I o o o o I I o o o I I o o I I 0 0 o o I o o o o o I o o 0 0 o o 0 o I o I I o o I o e o o 0 0 o o o o I o o o o o I o . . . . . . 20 ........... *' .......... '* ........... ' ....................... '* ........... ' ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ...... 0\ \0 \0 0 ......, v. 00 0 \0 QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W199.QAF;3 P5ENERGY-GD14B (PEAK ENERGY GD-148) 15-MAR-2016 08:39:06 through 16-5EP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 ............................................................................ ro """ ........ I D (!) )-(!) x x x x x x x w 3180 z . . . . . . ..................................... ' ..................................... . . . . . . . w ::.::: a: w 0... 3160 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ..... -.l 0 0 0 ....., Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B199.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:17:22 through 16-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 . 08 .......................................................... ' ................ . . . . . . . .06 . . . . . . ............................................................................ . 04 . 02 ............................................................................. . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --..J 0 -QA filenafYJe ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA. QA. W]W200. QAF; 4 AVRGEFF (Average Efficiency) 15-MAR-2016 08: 39:09 through 16-SEP-2016 12:00:00 0.259942 through 0.276020 . . . . . . '275 ............................................................................ . . . . . . ::::-, x x 0 '27 c 0) ..................................................... *x ........................ . "M 0 x x "M 4-4-UJ x O)* '(\I) ill 0) x > a: . . . . . . .265 . ' .... ' .................................................................... . . . . . . . '26 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYJent Date/Tiffie UP LOW ...... -..! 0 N 0 >-+, Vl 00 0 \0 QF=! filenar.-.e Parar.-.eter NaMe Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W200.QAF;4 (NUCLIDE .ACTIVITY GD-148) 15-MAR-2016 08:39:09 through 16-SEP-2016 12:00:00 184.000 through 204.000 200 ............ * .......... * ............ : .......... * ............ * ............ : ..... . I 0 (!:I )-I-H > H I-x u a: x x LLJ x o* H _J x x u ::i x z 190 . . . . . . o ' o o ' ' ' ' o ' ' ' ' o 0 ' 0' o 0 0 0 0 ' o o o o ' o o o ' ' o 0 o 0 0 o o o o ' o o o o ' ' 0 0 0 I o 0 o o o o o o o, I I 0 0 0 o I o o o o I I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW .... -..l 0 w 0 ......., Vi 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower I Up-per -Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W200.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:39:09 through 16-SEP-2016 12:00:00 5.00000 through 100.000 80 0 o *
o ' ' o o 0 I', o o, o o I o 0 o ' o ,' o o o ' I o o o o o o: .o I o 0 o o o o o ,,,' o o o o 0 o o o o o o ,' o o o 0 o 0 o o o o o : o o o 0 0 0 -:-! I 0 z 0 H =i 0 01 w tt:: a: w 0.. 60 .......... *:* .......... -:* .......... : .......... *:* ... *x ..... *:* .......... : ... : .. x x x x x x . . 40 o o o o o o o o o o 0 0 0 o o o o 0 0 o 0 o o o o o I 0 o o o o o o o 0 0 o o o o o o o o o 0 0 I o o o o o o o 0 I I 0 o o o o o o o o I 0 o o o o o o . -. . . . . 20 ........... *' ........... '* ............ ' ........................ '* ........... ' ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA,W]W200,QAF;4 P5ENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 08:39: 09 through 16-5EP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 ............................................................................ co """" ""'"" I D )-0::: x x x x x x x w 3180 z . . . . . ............................................................................ . . . . . . w :::..:: a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B200.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:17:26 through 16-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ° ' ' 0

0 ' ' 0 ' ',' 0 0 0 ' ' ' 0 0 0 ' ', 0 0 0 0 0 0 0 * ' ' 0 : 0 ' ' 0 0 0 0 ' 0 0 00 0 0 ' 0 0 0 ' ' 0 0 o ',' 0 0 0 1 0 0 0 0 0 0 : 0 0 0 0 ' 0 . 06 -. . . . . . o o o o o o o

0 o o o o o o I 0 o o o 0 o o o o o O O o o o O O o o O o o o o o o o o o o o o o o O o o o O 0 o o O o o o o O 0 o o o I o o o O 0 o o . 04 . 02 ............................................................................ . . . . . . 0 x x x 3-16 MeasureMent Date/TiMe UP LOld QA filenafYle ParafYleter NafYle 5tart/End Dates Lower/Upper LfYlts: '27 >:. (.) c Q) *r-i (.) *r-i 4-4-LU DKA100: [ENV_ALPHA.QA.W]W201.QAF;4 AVRGEFF (Average Efficiency) 15-MAR-2016 10:07:54 through 16-5EP-2016 12:00:00 0.257911 through 0.273865 . . . . . x . Q) '265 W) i'(i .... *x* .... *.* ........................ = .**....... *.* **. *x .................. = *..... x Q) x x > H x x I-u x a: x w D H _J x (_) x x ::i z 190 ........... * ............ * ........... : ........... * ............ * ........... : ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W201.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 10:07:54 through 16-SEP-2016 12: 00:00 5. 00000 through 100.000 80 ........... * ........... ,* ........... : ........... * ...... ' ..... * ........... : ..... . .,-! I Cl C) z 0 H f-* :l _J 0 (f) w O'. cr: w 0.. . . . . . . 60 ............................................................................ . . . . . . x x x x x x x . . . . . 40 *********** : ********** * ************ : ********** * ************ * ************ : *** t '

20 .................................... ' .................................... ' ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOltl
--..J 0 \0 0 ....... VI 00 0 \0 QA f i len-arrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W201.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 10:07:54 through 16-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 ...... ' ...................................................... * .............. . . . co v ..-i I D (!) )-(!) 0::: x x x x x x x LLJ 3180 z . . . . O o o o o o O o o o o o o o o o O o o o o o o O O O o o o o O o O o o o o o o o o o o o o o o I I o o o I I o o o o 0 o I o I I o o o o I o o 0 o I o o . . . . . . LLJ ::...:: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B201.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-201613:17:30 through 16-SEP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 o ' * * * ' ' ' ' ' 1 ,* ' ' ' o ' ' o ' ' ' 10 o ' o ' ' ' o o ' ' o : ' ' ' o o o o ' ' o ', o ' ' o o o ' ' o ' ' ',' o o o ' ' o o o o ' : o o o ' ' ' . 06 ........... * ............ * ........... : ........... * ............ * ........... : ..... . . . . . '02 ............ * .......... * ............ : .......... * ............ * ............ : ..... . 0 ........ 3 -16 LOW 4-16 6-16 8-16 9-16 7-16 MeasureMent Date/TiMe ...... -....l ...... ...... 0 ....., Vl 00 0 "° QA filenafYle Pq.rafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA.QA.W]W202.QAF;3 AVRGEFF (Average Efficiency) 15-MAR-2016 10:07:31 through 16-SEP-2016 12: 00: 00 0.262756 through 0. 279008 . 275 ........... *, ........... * ........... : ........... * ............ * ........... : ..... . (..) c ID "M (..) x x x "M 4-x 4-UJ x ID . 27 "Oil i{j . . . . . . ............... ' .................... ' ...................................... . . . . . . . x x I-. ID > <I: x I 265 ° 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 '* 0 0 0 0 0 0 0 0 0 0 0 I 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0 I 0 0 0 0 0 0 3-16" 4-16 5-16 6-16 7-16 8-16 9-16 Measure£YJent Date/TifYle UP LOW QA filenarrre Pararie ter Narie Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W202.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 10: 07:31 through 16-SEP-2016 12:00:00 184.000 through 204.000 200 o o o o o ' ' o ' ' o ' o ' o ' ' o o o o ' o o o o ' o o 0 o ' I 0 o o 0 0 o o o 0 I o o o o o I o o o I o o o o ' o o o o I I o o o o o o o o o 0 o o . . . . . . I Cl x )-t-H > x x H t-u <I x x w Cl H x x x ....I U* ::i z 190 . . . . . . ' o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o o I o o o o o o o o o 0 o 0 o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerient Date/Tirrre UP LOW QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: 100 DKA100: [ENV_ALPHA.QA.W]W202.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 10:07:31 through 16-SEP-2016 12:00:00 5. 00000 through 100.000 80 ........... * ............ * ........... : ........... * ............ * ........... : ..... . .-I 1
D z D H 1-:=i _J D (J) w Ct'. ::..:: a: w 0.. 60 . . . . . . ............................................................................ . . . . . . x x x x x x x x . . . . . . 40 o o o o 0 o o o o o o o o o o I I o o o o 0 o o o o I I o o o o o ' o o o o o 0 o 0 0 o o o 0 o 0 o o o o o o o o o o o o 0 o o o o o o o o o o o o ' o . . . . . . 20 ............................................................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W202.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 10:07: 31 through 16-SEP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 o 0 0 o 0 I o o o o o o o o o 0 o o o o o o o o o 0 o o o o o o o o o o 0 I o o o o o o o 0 o o o o o o o 0 o o o o o o o o I I o I o o o o o o o I o o . . . . . . co ""'" "<"-I I D (.') )-(.') Ct'. x x x x x x x x LLI 3180 z . . . . . . . . . . . : . . . . . . . . . . . . : . . . . . . . . . . . . . . . . . . . . . . : . . . . . . . . . . . . : . . . . . . . . . . . ; . . . : . . LLI ::..: a: LLI CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
...... -l ...... Vl 0 ......, Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B202.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:17:35 through 16-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 .08 ' 0 0 0 o o 0 o o o o I 0 o o o o o o o o I 0 0 o o o 0 o o o o I 0 o o o o o o o o o o o o o I 0 o o o ' I ' ' o ' o o 0 o I o o o o ' o o o o o I o o . . . . . . .06 . . . . . . I o o 0 o o 0 0 o o o I o o o I o o o o o I 0 o o o I o o o o I I o o o I 0 o o o o I o 0 o o I o 0 0 0 I I o o 0 o o o o o I 0 o o o o 0 o o o 0 0 o o . 04 . . . . . . . 02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 xxxxxx xx 6-16 7-16 x x* x x x *x x 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W203.QAF;3 ParaMeter NaMe AVRGEFF (Average Efficiency) Start/End Dates 15-MAR-2016 08:39:21 through 16-SEP-2016 12:00:00 Lower/Upper LMts: 0.255187 through 0.270971 UP . 27 . . . . . . ' ' o 0 o I I o o o o o o o o o o o o o 0 0 0 o o o 0 o o o o o o o o o o 0 o o o o o o o o o o I o 0 o I I o o o I I o 0 o o o o o o o o o o 0 0 I I o . . . . . >:. u c . 265 Q) ........... * ............ * ........... : ........... * ............ * ........... : ..... . *ri u *ri 4-4-UJ Q) "0.0 i(j I-Q) > x x a: .26 x x x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenar.-.e ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA,W]W203.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 08:39:21 through 16-5EP-2016 12: 00:00 184.000 through 204.000 200 .............................................................. ' ............ . . . . . . . I D (!) )-f-H > x H f-x u* a: x x x x w D *H ....I x u ::i z 190 ........... * ............ * ........... : ........... * ............ * ........... : ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Oates Lower/Upper LMts: 100 OKA100: [ENV_ALPHA.QA.W]W203.QAF;3 PSFWHM-G0148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:39: 21 through 16-SEP-2016 12: 00:00 5.00000 through 100. 000 80 ........... * ............ * ........... : ........... * ............ * ........... : ..... . .-I I Cl C) z D H 1-:::::i ....I D en w O:'. ::..::: a: w o_ . . . . . . 60 ............................................................................ . . . . . . x x x x x x x 40 0 I 0 o o I o o o o o 0 0 o o o o o o o 0 I o 0 o o o o o o 0 I I o o o 0 0 0 0 o 0 0 o 0 o o o o o o o I o o o o o o o o o o o o o o o o o o o o o o o . . . . . . 20 ........... *' ............................................... '* ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Oate/TiMe UP LOW --.l -"° 0 ...., Vl 00 0 "° QA filenal'le Paral'leter Nal'le Start/ End Da*tes Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W203.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 08:39:21 through 16-SEP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 ....... '* ................... ** ............................................... . ro """ -.-( I D (!) )-(!) et:: x x x x x x x . . . . . . ..... ' ..................................................................... . . . . . . . w 3180 z w ::,..:: a: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B203.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:17: 39 through 16-SEP-2016 12:00: 00 Lower/Upper 0. OOOOOOE+OO through 0.100000 UP .08 ............................................................................ . . . . . . .06 . . . . . . ............................................................................ . 04 .02 ............................................................................ . . . . . . 4-16 5-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W205.QAF;3 AVRGEFF (Average Efficiency) 15-MAR-2016 08:39:30 through 16-SEP-2016 12:00:00 0.256250 through 0.272000 I 27 ° ' * *
1 ' 0 0 0 0 *' 0 0 0 ' 1 0 0 0 0 1 '* 0 0 * ' 0 0 0 0 0 0 0 I 0 0 0 0 0 0 0 0 0 0 '* 0 ' 0 0 0 0 1 ' ' 0 0 '* 0 0 0 o 1 1 0 0' o 0 I 0 0 0 0 ' 0 :>, u c IJ) *r-i u *r-i 4-4-LU IJ) "0.0 Ill IJ) > <r: x x x x . . . . . . . 2 6 5 * * *

x * * * * * .* * * * * * * * * * * *. * * * * * * * * * * * = * * * * * * * * * * *. * * * * * * * * * * * *. * * *

x* * * * * * = * * * * * * . . . x . . . . . . 26 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,W]W205.QAF;3 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 15-MAR-2016 08: 39:30 through 16-SEP-2016 12:00:00 Lower/Upper LMts: 184.000 through 204.000 UP 200 ............ * .......... " ........... : .......... * ............ * ............ : ..... . I 0 r H > H x u x x x x x w 0 H x u z 190 . . . . . . ............................................................................. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W205.QAF;3 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:39:30 through 16-5EP-2016 12: 00: 00 5.00000 through 100.000 80 ........... * ............ * ........... : ........... * ............ * ........... : ..... . I Cl C) z 0 H _J 0 01 w 0:: a: w 0.. . . . . . . 60 ............................................................................ . . . . . . x x x x x x x 40 ............................................................................ . . . . . . 20 ............................................................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W205.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 08:39:30 through 16-SEP-2016 12: 00: 00 3143.00 through 3223.00 . . . . . . 3200 ............................................................................ . . . . . co ""'" ...-l I D )-0::: x x x x x x x LLJ 3180 2 . . . . . . ............................................................................ . . . . . . LLJ ::...: <I: LLJ a.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til'Je UP LOW
...... -..J N Vl 0 ....., Vl 00 C> \D QA filenaMe DKA100: [ENV_ALPHA.QA.B]B205.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:17: 47 through 16-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' I I o ' ' I,' I 0 o I I o o o o 0 10 o o I o o 0 0 0 I I o : o I I o 0 o o I o 0 o0 o o I o o o I I O o o 10 o o o o I I o o o o o : o o o I I o .06 . . . . . . I o o o o I I 0 o o I o o o 0 o o o e O 0 0 o o o o I o o o o o o o o o I I o o o o o o o o o I I 0 o o o o o o o I 0 o o o o o I o I 0 I o o o O o I o .04 . . . . . . .02 o ' o * * * ' * * * * * ' * * ' ' ' * * * *
o '* ' ' * * * ' o * * * * * * ' o ' * * ' ' ' * *

o o ' o * ' * * * * * ' o * * * * * * * ' I ' * . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W206.QAF;4 AVRGEFF (Average Efficiency) 15-MAR-2016 08:39:33 through 16-SEP-2016 12:00: 00 0.248420 through 0.263785 x .26 o o * ' ' I o o o o I', o o o I ' o o o o o ,' o o o o I o o o I I o : o ' I 0 0 o 0 o I o o' o o I o o o I I o o o ,'I o I o I ' o o o 0 0 : o o 0 I I o >i u x c Q) *r-1 u *r-1 4-4-x UJ x x Q) "QJ) . 255 iti . . . .. . . ............................................................................ . . . . . . I-Q) > x <I: x . 25 ......................................................................... ' .. . . . . . 16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe ParaMeter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 08:39:33 through 16-SEP-2016 12: 00:00 184.000 through 204.000 200 ............ * .......... * ............ : .......... * ............ * ............ : ..... . I D CJ. )-I-H > H I-u x a: w x x x D H x x ...J u ::J x z 190 0 o o o o o o 0 o o o 'o o o o I I o o o o o ,' 0 o o o o o o o o I o : o o o o o o o I o o o'o o o o o o I I o o o 1' 0 o e e I I o o o o 0 : o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/TiMe UP LOW
...... -.J N 00 0 >-+, Vi 00 0 ID QA filenaf"l"le Paraf"l"leter Narrie Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W206.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08: 39:33 through 16-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ........... : ........... * ............ * ........... : ... ' .. I Cl z 0 H 1-::J ....I 0 en w Ct'. :::..::: a: w 0.. . . . . . . 60 .......................... ' ' ............................................... . . . x . . x . . x x x x x 40 I I 0 0 o I I o o 0 I o 0 0 0 I I o 0 o 0 I I 0 0 0 I o 0 o 0 0 0 o o o 0 0 o 0 o o I o o o 0 o I 0 o o I I o o o o I o
o I I o o o o I o o o o o o o . . . . . . 20 ........... *' ............................................... '* ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tif"l"le UP LOW
..... .....:i N \0 0 ......, Vo 00 0 \0 QA filenarrie Pararrieter Narrre Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W206.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 08:39:33 through 16-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 ' ' o 0 0 0 ' o o o I I o o o I I 0 0 o o o I o 0 0 o I o o o I I o 0 o o o o o 0 0 I 0 0 0 o I I o o o I 0 0 0 o o o o o o I I 0 o o o I o 0 o 0 0 I o . . . . . . co """ ..-! I D (!) )-(!) Ct:: x x x x x x x LLJ 3180 z . . . . . . I o o o 0 0 I o o o I 0 o o o I I 0 0 o 0 o I o 0 0 o* *O o o o I I o 0 0 o 0 o o o o o o o 0 0 0 I o o o I o o o o o 0 o o o I o o o o o I o o o o 0 I 0 . . . . . . LLJ ::..: <I: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B206.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 13:17:51 through 16-5EP-2016 12:00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 I 08 o o o o o 1 ' o o o o ,' o o o 1 ' o o o o o '* o o o 1 1 o o o ' o o : o 1 1 o o o o 1 o o ', o 1 ' o o o o 1 o o o 1' 1 o o o 1 1 o ' o o o : ' 1 ' ' ' ' . 06 ........... * ............ * ........... : ........... * ............ * ........... : ..... . . . . 04 . . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Oate/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W207.QAF;3 AVRGEFF (Average 15-MAR-2016 08:39:37 through 16-SEP-2016 12:00:00 0 .,256618 through O. 272492 . . . . . . '27 .............................. "' ............................................ . >.. (.) c ID *r-1 (.) *r-1 . . . . *' . . '265 .. * ...................... * ... , ....... : ...................................... : ..... . UJ '26 x . . . . . . . . . . . :* . . . . . . . . *: . . . *:x: . . . . .. : . . . . . . . . : . *: . . . . . . . . . . . *: . . .. . . . . . : . . . . .x x x* 3-16 4-16 5-16 6-1_6 7-16 8-16 9-16 *MeasureMent Date/TiMe UP LOW ....... -.l w N 0 ......, Vo 00 0 l.O QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA,W]W207.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 08: 39:37 through 16-SEP-2016 12: 00:00 184.000 through 204.000 200 . ' ................... ' ..................................................... . . . . . . . I D )-t-H x > H t-x u a: x x W* D H x x x ...J u ::i z 190 . . . . . . I o o o I o o o o ' o o o o o o o o o o 0 I I o I o I o o o o o ' o o o o o o o o 0 I o o o o o o o o o o 0 I 0 o 0 o I e o o o o o o o 0 0 o o o o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrre Pararrre ter Narrre Start/End Dates Lower/Upper Lrrrts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 15-MAR-2016 08:39:37 through 16-SEP-2016 12:00: 00 5.00000 through 100.000 80 ........... * ............ * ........... : ............ * ............ * ........... : ..... . .,..i I Cl z 0 H :J ....I 0 ({) L1J Ct'. :..::: a: L1J 0.. . . . . . . 60 o o o o o o o o o o o o 0 o 0 o I o o o o o o 0 0 0 o o o o o o 0 o o o o o o o o o o o o o o o o 0 0 o I 0 o o o o o o o o o o 0 0 o o o o o o o ; o o . . . . . . x x x x x x x . . . . . . 40 ................................ ' .......................................... . . . . . . . 20 ............................................... '* .............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOliJ QA filenaMe DKA100: [ENV_ALPHA.QA.W]W207.QAF;3 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY G0-148) Start/End Dates 15-MAR-2016 08: 39:37 through 16-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223. 00 UP 3220 3200 . . . . . . ............................................................................ . . . co ""1" ""'"" I D )-Q'. x x x x x x x LU 3180 2 . . . . . ' o ' ' o 0 o o ' ' o o ' o o ' ' ' o o o o ' o o o o ' o o o ' ' o o o ' I o o o o o o o o o o o o o o o o o o 0 o 0 o o 0 0 o o o o o o o o o o ' o o . . . . . . LU ::...! a: LU ll.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOii.i MeasureMent Date/TiMe QA filenaMe DKA100: [ENV_ALPHA.QA.B]B207.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:17:55 through 16-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through O.lOOOpO UP I 08 ' 1 1 0 0 0 0 0 0 o 0 00 0 0 0 0 0 o 0 0 o 0 ', 0 0 0 0 0 1 1 0 0 0 0 : 0 0 0 0 0 0 o 1 0 1 O, 1 1 0 0 0 0 0 0 0 0 0 '* 1 1 o 0 1 0 0 0 0 0 0 : 0 0 1 0 0 0 .06 . . . . . . ........................... ** ............................................... . . ' .04 ' . . . . . . 02 ................................................ -........................... . . . . . . . 4-16 5-16 6-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W208.QAF;3 AVRGEFF (Average Efficiency) 15-MAR-201616:11:10 through 16-5EP-2016 12: 00: 00 0.254591 through 0.272100 . . . . . . .27 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 I 0 0 , o o o o o o o o o o o o o o o o o o o o o o I o o o o I o o o o 0 I o o ' I I o ' ' ' ' 'o ' ' I o 0 o' I I o . . . . . . >i ij c Q) .265 *r-1 . . . ............................................................................ . . . . . . ij *r-1 4-4-w Q) x "0.0 i(i x x x Q) x x > a: . . . . . . . 26 * * * * *X * * * * ... * * *
X* * * * * ... * * * * * * * * * * * * * * * * * * * * * *** * * * * * * * * * * *** * * * * * * * * * * * * * * * *

I 256 ° ' 0 0 0 0 1 0 0 0 1 00 0 0 0 0 1 0 0 0 0 1 0 1 0 1 0 0 0 0 0 0 0 0 0 ' 0 0 o 0 0 1 0 0 0 0 1 0 0 0 1 1 0 0 0 00' ' 0 o ' ' o 0 0 0 1 0 0 0 1 1 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Pararrieter Narrie Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W208.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 15-MAR-2016 16:11:10 through 16-SEP-2016 12: 00: 00 184.000 through 204.000 200 ...... ' ........................................ ' ........................... . I Cl (!) )-I-H" > H I-u a: w Cl H -I u :=i z x . . . . . . x x x x x x x 190 o o o o o 0 o o o o o 'o o o o ' I o o o o o o' o o o o o o o o o o o : o I I o o ' o I o o o' o o o o o o o o o o o o' I 0 o o I o o o o o o : o o o I I 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
...... -.J w 00 0 ......, VI 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W208.QAF;3 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 15-MAR-201616:11:10 through 16-SEP-2016 12:00:00 Lower/Upper LMts: 5.00000 through 100.000 100 UP -M I 0 80 ........... * ............ * ........... : ........... * .... *-* ...... * ........... : ..... . (.!) x z a H 1-:J _J a CJ') w O:'. 60 40 . . . . . . ............................................................................ . . . . . . x x x x x x . . . . . x I o o o o I o o o o o I o o o o 0 o o o 0 I 0 0 0 0 I o 0 o o o o o o o o o o o o o o o o o o I o o O O I I O o o o I o o o o o o o o o o o o o o o I o # * * * * *
2_0 ' ' * * * ' ' * * * '*' ' ' * ' ' ' * * * ' '*' ' ' ' ' * * ' ' ' o I ' ' ' ' ' ' ' ' * ' '* * ' ' * * * ' ' ' ' * '*' * ' * ' ' ,.,

o ' I ' ' ' ' ' ' 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe LOW QA filenafY'le ParafY'le ter Na!Y'le Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W208.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 15-MAR-2016 16:11:10 through 16-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 I I o o I I I o o o o I 0 o 0 I o o o o 0 I I o o O I 1 o o o I O O O o 1 1 o o O O I o o o o o I o O o 1 1 o o o I

O o o 1 o o o o I I 1 o o o o I o . . . . ro ""'" -rl I D (!) )-(!) 0:: LLJ 318.0 z LLJ x x x x x x x . . . . . . ............................................................................ . . . . . . x LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B208.QAF;2 ParaMeter BACKRATE (Background Rate) 5tart/End Dates 4-MAR-201613:18:00 through 16-5EP-2016 12: 00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' ' ' 0 0 0 0 0 ,' 0 0 0 ' ' o

o 0 ' ', 0 ' 0 ' 1 o ' ' ' ' ' : ' ' 1 ' ' ' ' ' ' ' ',' ' ' ' ' ' ' 1 ' ' ' ',' o * * ' * * * *

o : o o o o , o . 06 ........... * ............ * ........... : ........... * ............ * ........... : ..... . . . .04 . . . . . . 02 ............................................................................ . . . . . . 4-16 6-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe 0 ....., Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W210.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:35:29 through 17-SEP-2016 12:00:00 0. thfough 0.261915 *. I 26 * * *

0 ' * *

0 ',* *

0 * ' * * *

0 ':. 0 *

0 * *

0 0 0 * ."

0 0 0 0 0 0 0 0 0 *, 0 0 0 0 0 0 0 0 0 0 0 ." 0 0 0 0 0 0 0 0 0 0 0 ,' 0 0 0 0 0 0 (.) c Q) *r-1 (.) *r-1 4-4-UJ . 255 o o o o o I o o o o o ', o o o o o o o o o o .. 0 0 o o o o o o ' 0 o 'o o o o o 0 o o o o o .. o o I o o o o, o o o o o, 0 o o o o o o o o o o 'o o o o o ' 0 x x x x x x x . . . . 25 ............................................................... ** ............ . . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,W]W210.QAF;3 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 16-MAR-2016 08:35: 29 through 17-SEP-2016 12:00: 00 Lower/Upper LMts: 184. 000 through 204. 000 UP 200 ............................................................................ . . . . . . I a )-I-H > H I-u a: x LLJ a H x -' x u ::i z 190 ........... :* .......... *: ..... X* .... :* .... *x .... *: ........... :* .......... *:* ..... . . . . . . . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenafl'le Paraf"l'le ter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ EN_V_ALPHA. QA, W] W210. QAF; 3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:35:29 through 17-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ........... * ............ * ........... * ............ * ...... . .,-t. I D z 0 H 1-:=i --' 0 ({) w Q'. 0:: w 0... . . . . . . 60 I 0 o o 0 o o o o o o 0 0 o o o o o o o o o o o o 0 o I o o o o 0 o o o o o o o o o I o o o o o o o o 0 o o o o e o o I o o o o o o o o 0 o o o o o I o . . . . . . x *X x x x x x . . . . . . 40 o o o o o o o o o o o 0 o e o o o o o o o o o o o o o o o o o I I o o o o o o o o o o o o o o o I o o o I o o o o I o o o o o I o o o o o o o o 0 o I o . . . . . . 20 ....................... ' ........... ' .......... ' ........... , .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tifl'le UP LOW QA filenal'le Paral'leter Nal'le 5tart/End Dates Lower/Upper Ll'lts: DKA100: [ENV_ALPHA.QA.W]W210.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08:35:29 through 17-SEP-2016 12:00:00 3143.00 through 3223.00 3 2 io * ** * * * * * * * * * ** * * * * * * * * * * , * * * * * * * * * * * , * * * * * * * * * * , * * * * * * * * * * * , * * * * * * * * * * * * * * * * * *

3200 . . . . . . .......................................................... ' ................ . ro ¢* ...-I I D (!:I )-(!:I 0::: x x x x x x x LL.I 3180 z o I o 0 o ............................................................................ . . . . . . LL.I :::..::: ([ LL.I 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B210.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) . Start/End Dates 4-MAR-2016 13:31: 04 through 17-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' ' 1 1 ' ' ' ',' 1 1 ' ' 1 ' ' ' ' 1 10' ' 1 o o 1 ' ' ' o '," ' ' ' ' ' ' ' ' 1 ' ',' 1 o o ' 1 1 1 '

1 '1 1 o o o 1 1 o o 1 o 1 ,o o o o : 1 1 .06 . . . . . . ............................................................................ . . .04 . . . . .02 ............................................................................ . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 16-MAR-2016 08:35:34 through 17-SEP-2016 12: 00: 00 0.238175 through 0. 252907 . . . . I 25 * ' * * * * * * * * * ,' * * * '

0 * * * * ', * * * ' * * * * * * * ," 0 0 0 * * *

0 *

00 0 0 0 * *

0 0

0 0: 0 * * * '

0 0 *

0 00

0

0 * * >, 0 c I]) *r-1 0 *r-1 4-4-UJ . . . . . . 245 ***********.-***********.***********:***********.*****_******:*****x***** .. ****** . . . . . . x x x x . x x . . . . . 24 ........... : .......... * ............ : ....................... : ............ * ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarie Pararieter Narie Start/End Dates Lower/Upper Lrits: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:35:34 through 17-SEP-2016 12: 00:00 184.000 through 204.000 200 ............ * .......... " ........... ,' .......... * ............ ,' ............ ' ..... . I er >-I-H > H 1--. u a: x w er x H x x ....I (j =i x .x z 190 .......... *:* .. : ....... *: ........... :* .......... *: .... *x ..... :* .......... *:* ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerient Date/Tirie UP LOW
....... -..) .i::. 00 0 ....., Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W211.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:35:34 through 17-SEP-2016 12:00:00 5. 00000 through 100.000 ...-I I D (!) z 0 H 1-::J _J o* 01 w 0::: ::,..: a: w 0.. 100 80 -. . . . . . ............................................................................ . . . . . . 60 ............................................................................ . . . . . . x x x x x x x 40 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ' o o o o o o o o o 0 o o o o o o 0 o o o 0 I o . . . . . . 20 ....................... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOU.I QA filenar.-.e Parar.-.eter Nar.-.e Start/ End oa:tes Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W211.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08.: 35: 34 through 17-SEP-2016 12: 00: 00 3143. 00 through 3223.00 3220 ************************'***********'**********-***********'******************* 3200 . . . . . . .......... ' ................................................................ . . . . . ro """ """" I D )-0::: LL.I 3180 z x . x. x . x . x . x . x o o o o 0 0 o o o o o o o o o 0 0 o o o o o 0 o o o o o 0 0 o o o o 0 0 0 I o o o o o o 0 0 o o o o o o I 0 o 0 o I o o o 0 I, 0 o o o o o o ' o o I 0 o . . . .. . . LL.I :::..:: a: LL.I 0... *. 3160 ....................... -........... -.......... -........... -.................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B211.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13: 31:08 through 17-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' 0 0 ' ' ' ' ' 0 ',' 0 0 o o 0 0 0 0 0 0 ', 0 0 0 0 o o 0 0 0 0 0 ." 0 0 0 0 0 0 0 ' 0 0 ',' ' ' 0 0 ' ' ' ' ' '.' ' ' ' ' ' ' ' ' * ,'
o

o * * .06 . . . . . . . . . . . *. . . . . . . . . . . ; . . . . . . . . . . . *. . . . . . . . . .. : . . . . . . . . . .. *. . . . . . . . . . . . . . . . . . . . . . . . 04 .02 ............................................................................ . . . . . . 0 .......... ......... 3-16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe 0 ....., Vi 00 0 ID QA filenafl"le Parafl"le ter Nafl"le 5tart/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 16-MAR-2016 08:35:38 through 17-5EP-2016 12: 00:00 0.250992 through 0. 266518 o o I I 0 o '265 o I o o o o I o o o I I o o o I I ' o o o I o o o o I o o o o I I 0 0 o I ' o o o o I I o o o o I o o o o I o o o 0 I 0 o I I o o o o I I o I o o ! o I x x :::-, 0 c I}) *r-1 '26 0 x x ........... * ........... : ........... * ...... x .... : ............ * ............ * ...... . . . . . . . *r-1 4-4-UJ x x I]) "Of) ill l-I}) > a:. '255 . . . . . . ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl"lent Date/Tifl"le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W212.QAF;3 NaMe (NUCLIDE ACTIVITY GD-148) Start/End Dates 16-MAR-2016 08:35:38 through 17-SEP-2016 12:00:00 Lower/Upper LMts: 184.000 through 204. 000 UP 200 ............ * .......... * ............ .' .......... * .......................... * ..... . I a r H > H x u x w a x H u x x x x z 190

0 o o o ' o o o o '01 0 0 o o I o o o 0 0 1' 0 0 0 o I o o o 0 I 0 'o 0 I I o o o o I 0 0 .. o I o o o o I I 0 O o 01 I o o o I I O O o o o 0o o o 0 O I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W212.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:35:38 through 17-SEP-2016 12:00:00 5. 00000 through 100.000 80 . . . . . . . . . . . *, . . . . . . . . . . ,* . . . . . . . . . . . *. . . . . . . . . . . : . . . . . . . . . .. *. . . . . . . . .... *. . . . . . . I 0 (!) z 0 H ::i ....I 0 (f) w O::'. :>.! a: w 0... . . . . . . 60 ............................................................................ . . . . . . x x x x x x x . . . . . 40 ...... ' .................................................................... . . . . . . . 20 ........... *' .......... ' ........... ' .......... ' ........... , ........... *' ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 16-MAR-2016 08:35:38 through 17-SEP-2016 12: 00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 o o I I o I ............................................... ' ........................... . ro """" ..-I I 0. (!) )-(!) O:'. x x x x x x x w 3180 z . . . . . . ............................................................................ . . . . . . w ::..::: a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
--.I Vl Vl 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B212.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:31:12 through 17-SEP-2016 12: 00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 I 08 ° ' 0 * * ' '
0 0 0 ,' 0 0 0

0 0 0 0 0 ' 10 0 0 0 0 0 0 0 0 0 0 0 ." 0 0 o 0 0 0 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 0 .' 0 0 0 0 0 0 0 0 0 0 0 ,' 0 o 0 0 0 0 . . . . . . . 06 0 o o o o 0 o o o o 0 0 o o o I 0 o o o o o 0 o o o 0 o o o o o o o o o o o o o o 0 I 0 o o o o o o o o o o o o o 0 o o o o o o o o o o o o o o 0 o o o . . . . 04 . . . . '02 ............................................................................ 0 3-16 . . . . . . x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: OKA100: [ENV_ALPHA.QA.W]W213.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08: 35:43 through 17-5EP-2016 12:00:00 0. 243562 through 0.258628 . 255 ........... : ........... : ........... ; .... *x .... : ........... ; ..... x ..... : ...... . . . . . . . x >, x (.) c Q) -r-1 (.) x x -r-1 4-4-UJ Q) "Q.Q '25 in . . . . . . ............................................................................ . . . . . . s... Q) > a: x . 245 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W213.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08: 35:43 through 17-SEP-2016 12: 00: 00 184. 000 through 204. 000 200 ...................... ' .................................................... . . . . . . . I 0 (!) )-t-H > H t-u <I: w* x 0 H _J u ::i x x x x x x z 190 . . . . . . . . . . . *. . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . .. . . . . . . . . . .. *. . . . . . . . . . . . *. . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
--.) Vi 00 0 ....., Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W213.QAF;3 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:35:43 through 17-5EP-2016 12:00:00 5. 00000 through 100.000 . . . . . . 80 ............................................................... ' ......... ' .. .,..... I Cl z D H 1-:J ...J D en w O:'.. ::..::: <I: w 0... . . . . . . 60 ' ' ......................................................................... . . . . . . . x x x x x x x 40 o o o o o 0 I 0 o o Io' 0 e o I 0 0 0 o 0 I ', 0 I 0 I o o o 0 I I o: o o o o 0 0 o ' ' o ', o o 0 o o,o o 0 o o o: o o 0 o I I 0 o o' 0 ,' o o o I I 0 2 0 ....................... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ...... -..J Vl \0 0 ....., Vl 00 0 \0 QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W213.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08:35:43 through 17-SEP-2016 12:00:00 3143. 00 through 3223.00 . . ' . . . 3200 ................... , ........................................................ . co '<t" ...-I I D (!:I )-(!) O:'. x x x x x x x LLJ 3180 z . . . . 0 0 0 0 o o o o o 0 o o o o o o I o o o o o o o 0 0 o o o o o o o o o o 0 o o o o o o o o o ' I o o o o o o o o o ' o o o o 0 o o o o o o o 0 o o o o o . . . . . . LLJ :::..:: a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --....) 0\ 0 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B213.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:31:17 through 17-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 . 08 o ' ' ' ' o I ' o ' I,' ' e 0 0 I 0 0 0 o I ', o o o I I o e 0 I I 0 .. o I o o o 0 o 0 e 0 'o o o o o o o I I o 0 0 .. 0 0 0 0 o I o o o o I ,o 0 0 e I o o . . . . . . . 06 I I o 0 0 I 0 o o o o I o e o I o o o o o I I 0 0 o o o o o o o I o o o o I 0 0 o o I o o o o I I o 0 0 0 o o o o I I o o o 0 I o o o o I o e o o o I o .04 .02 ............................................................................. 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOU.I 0 ..,.., Ul 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W214.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:35:47 through 17-SEP-2V16 12:00:00 0.254982 through 0.270754 . . . . . . . 27 ............................................................................ . . . . . . ::;:., u . 265 c . . . . . . .................................................................. -........ . . . . . . . Jl) *r-1 u *r-1 4-4-UJ Jl) x "0.0 (lj x Jl) > a: x x x .26 . . . . . . I I o o o o o o 0 o I o o o o I I 0 o o o o o o o o I O o o o o o o o o o o I O O o I o o o o o o o o o I o o O o I o o o o o o o o o o O O O o o o o o x . 255 ......... 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW --...J O'I N 0 ......, Vt 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W214.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:35:47 through 17-SEP-2016 12:00:00 184. 000 through 204. 000 200 ........... " .......... " ........... .' ....................... .' .................. . I 0 (!) )-I-H > H I-u cJ: x Ll.J x 0 H ...J x x x x u =i x z 190 ........... * ........................ * ........... .-........... * ............ * ...... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W214.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08: 35:47 through 17-SEP-2016 12:00:00 5.00000 through 100.000 x 80 ........... *, .......... ,* ........... * ............ * ..... -...... * ............ * ...... . T"'I I D C) z D ::i _J D 01 w 0::: ::...::: a: w 0... . . . . . . 60 ............................................................................ . . . . . . x x x x x x .X . . 40 o o o o o o o o o o o o o o o o o o o o o o o 0 o o o O o o o o o o o o o o o O O o o o o o o o o o o o I 0 o o o I I o o o o o 0 o o o o o o o o o O o . . . . . . 2.0 ........... *' ....................... I' ....................... ,, **** ' ************** 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W214.QAF;3 PSENERGY-GD148 (PEAK ENERGY G0-148) 16-MAR-2016 08:35:47 through 17-SEP-2016 12:00:00 3143. 00 through 3223.00 o o I 0 0 o 3200 0 0 0 0 0 0 o 0 o o o I 0 0 0 I I o o o o o 0 0 0 0 0 0 o 0 0 I 0 0 0 0 0 I 0 0 0 0 0 0 0 0 0 0 I 0 0 o I 0 o o 0 0 0 0 o 0 I I o o o o I o o o o I I o . . . . . co v "<"i I D )-O:'. x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ lo.! -+, VI 00 0 \0 QA filenaMe ParaMeter NafYle Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B214.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:31:21 through 17-SEP-2016 12: 00:00 O.OOOOOOE+OO through 0.100000 I 08 1 1 * *
1 o ' ' ' o 01 1 1 ' 1 o 1 ' ' ' 1 10 ' 1 ' 1 1 o 1 o 1 1 o ,* 1 1 1 o o o o ' o o ', o 1 1 o o 1 o 1 o o o .' 1 1 o 0 1 1 o 1 o o '01 o o 1 ' 1 o . . . . . . . 06 .......... ' ................................................................ . '04 . . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifYle x UP LOW
...... -.J 0\ 0\ 0 ....., Vt 00 0 ID QA filenafYle ParafYle ter NafYle Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA,W]W216.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:35:56 through 17-SEP-2016 12:00:00 0.240458 through 0.255332 . . . . . . . 255 ' ' o o o o ' o o o ' 0 o o o 0 o o o o o o o o o o o o o o o 0 0 0 o o o o o o o o o o o o o I I o o o o I o o I 0 I 0 o o 0 I o o o o o 0 0 o o o I o >-> 0 . 25 c Q) *r-1 0 *r-1 4-4-UJ Q) "0.0 l1j ID > a: x . 245 . . . . . . . . . . . :. . . . . . . . . . . : . . . . . :x: . . . . . . . . . . x . . . . : . . . . . . . . . . . . . . . . . . . . . . . : . . . . . . . . x . . . x . . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW QA filenafl"Je Parafileter Nafl"Je Start/End Dates Lower/Upper Lfl'lts: DKA100: [ENV_ALPHA.QA.W]W216.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:35:56 through 17-SEP-2016 12:00:00 184.000 through 204.000 200 ' 0 0 o o o 0 0 o o o 0 o o o o o o o o o 0 ' o o o o ' o o o o 0 0 o o o o o 0 0 o o o o o o o o o o o o I 0 o o o I I 0 o I I o o o o I o o o I I o o . . . . . . I. D (!) )-I-H > H I-u <I: w D H x x x -1. u ::i z 190 . . . . . x . ..... x ..... :* .......... *: ........... :* ..... >s .... *: ........... :* ........... :* ..... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl"Jent Date/Tifl"Je UP LOW --..J O'I 00 0 H) Vl 00 0 \C QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W216.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08: 35:56 through 17-SEP-2016 12:00:00 5.00000 through 100.000 80 . . . . . . . . . . . *. . . . . . . . . . . .-. . . . . . . . . . . *. . . . . . . . . .. : . . . . . . . . . . . *. . . . . . . . .... *. . . . . . . .,..j I D z 0 H 1-::J ...J 0 U') w Ct'. ::..::: <C W* 0... . . . . . . 60 ........................... ' ............................................... . . . . . . . x x x x x x x 40 0 0 0 0 0 o I 0 o 0 0 0 0 0 o 0 0 0 0 o o I 0 o 0 o I o 0 e o o 0 o o o o o o o o o o e o o o o o o o o o 0 o o o o o o o o 0 I 0 o o o 0 o o o o o o o . . . . . . 2 0 ....................... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W216.QAF;3 PSENERGY-GD148* (PEAK ENERGY GD-148) 16-MAR-2016 08:35:56 through 17-SEP-2016 12:00:00 3143.00 through 3223.00 o o I I o I 3200 I I 0 I I o I I I I I I o I I I 1 I o I o I 1 I O I 1 1 o o 1 1 o 1 1 O 1 1 1 1 1 1 o 1 1 1 I I I o 1 1 O I 1 o 1 o I O o o 1 o O o o o 1 o O O o o I o co "=:!" ....... I 0 )-0::: x x x x x x x w 3180 z . . . . . . I I I I o I o o I o I I o I o o I I o o I o I o o I o o o 0 o I I o o I I o o o I I I I I o o o I I o o o 0 I I o 0 ' o o o I I o o I I o o I I I 0 I o . . . . . . w ([ w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B216.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:31:29 through 17-SEP-2016 12:00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP .08 ............................... ' .......................................... ' . . . . . . . .06 . . . . . . ............................................................................ . . . . 04 .02 ............................................................................ . . . . . . 0 _____ ......... ........ ......... 3-16 LOW 4-16 5-16 7-16 6-16 8-16 9-16 MeasureMent Date/TiMe ...... -....) -....) ...... 0 Hi Ul 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W218.QAF;3 AYRGEFF (Average Efficiency) 16-MAR-2016 09: 48:51 through 17-5EP-2016 12:00:00 0.246780 through 0. 262040 . 26 o * *
o ' ' o o ' I ', o o o o o o

o ' o .. o o o I ' ' o o I I o ', o 0 I o o o o o o o .. o o 0 o o 0 o o o o o 'o o o o o 0 o o o o o o 'o o o o o o o :>, u c 0) *r-i u *r-i ........ ........ UJ x . 25-5 * * * * * * * * * * * :. * * * * * * * * * * .: * * * * * * * * * * * :. * * * * *x * * * * -: * * * * * * * * * * * :. * * * * * * * * * * *> * * * * *

x . 25 3-16 4-16 5-16 6-16 7-16 MeasureMent Date/TiMe x x x 8-16 9-16 UP LOW
--.J -.J N 0 ......, Vl 00 0 '° QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W218.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 09:48:51 through 17-SEP-2016 12:00:00 184.000 through 204. 000 200 ............ * .......... * ........................ * .......................... * ..... . I Cl (!) H > H u a: w Cl H ...J u =i z x x x x 190 o o o o o I ' o I I o o I * ' 0 o
o o 0 1' I 0 o ' I o I o o ' o ', o I I o o o o o o o .. o I I o o I o I I o o 'o o 0 0 0 o o o o o o o 'o o o o o I I x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W218.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 09:48:51 through 17-SEP-2016 12:00:00 5. 00000 through 100.000 80 . : ......... * ........................ * ........................ * ............ * ...... . ..-1 I D Q) z 0 H :J ...J o* 01 l.LJ O:'. a: l.LJ 0.. . . . . . . 60 0 0 o o o 0 I o o o I 0 o o o I I o o o o 0 I o o o 0 0 o o o o 0 0 o o o o o 0 o o o o o o 0 I 0 o o o o I 0 o o o o 0 o o I o o o o o 0 o o o 0 I o o . . . . . ' . x x x x . . . . 40 I o o o o I o o o o o o o o o o o o o o o o o o e o o o o o o o o o o o o o o o o e o o 0 ' o o o o o o 0 0 o o o o I o o o o o o 0 ' o o o o o o 0 o o . . ' . . . 20 ........... *' .......... ' ........... ' .......... ' ........... ' ........... *' ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Oate/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W218.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 09:48:51 through 17-5EP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ co """ ..i I D )-(!) 0:: x x x x LLJ 3180 Z. . . . . . . ............................................................................ . . . . . . LLJ ::..::: a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.8]8218.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:31:37 through 17-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP . 08 o ' o o 0 o ' o o o 0 0 o o o o o 0 o o o o o o o o o o o o o o I o 0 o o o o o o o o o o ' o o o o o o ' I o o o o o o o o o o o o o o o o o o o 0 o o . . . . . . . 06 . . . . . . I o o o o o 0 o o o o o o o o ' o o 0 o 0 o o o o 0 0 o o o o o I 0 0 o o o o o o 0 0 0 o o o o o o o o 0 0 o o o o o o o o I o o o o o o o o o e o o o . 04 . . . . . 02 ............................................................................ . . . . . . LOW MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W219.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:36:12 through 17-SEP-2016 12:00:00 0.251970 through 0. 267550 I 265

0 0

0 0 0 0

0 0 *' 0 0 0 0 0 0 0 0 0 0 .. 0 0 0 0 ' 0 0 0 ' 0 0 ,/' 0 0 0 0 0 0 0 0 0 0 ... 0 0 ' 0 0 0 ' 0 0 0 0 ,/' 0 0 0 0 ' 0 0 0 0 0 0 00 0 0 0 0 0 0 u c Q) *r-1 u *r-1 4-4-.26 ....................... , ........... , .......... , ........... , .................. . UJ x x x x x x . 255 x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... -J -J -J 0 ....., Ul 00 0 \0 QA filename DKA100: [ENV_ALPHA.QA.W]W219.QAF;3 Parameter Name NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 16-MAR-2016 08:36:12 through 17-SEP-2016 12: 00: 00 Lower/Upper Lmts: 184.000 through 204.000 200 ............................................................................ . . . . . . x x x x x. x x . . . . . . ............................................................................ 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time UP LOW ....... -..J -.J 00 0 Hi Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W219.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:36:12 through 17-SEP-2016 12: 00:00 5.00000 through 100. 000 80 . . . . . . . . . . . *, . . . . . . . . . . .. . . . . . . . . . . . *. . . . . . . . . . . : . . . . . . . ' ... *. . . . . . . . . . . . *. . . . . .. ..-i I CJ z 0 H ::J _J 0 f,J) w O:'. <J: w 0... x x x x x x . . . . . . 60 ........... : .......... * ............ : .......... * ............ : ..... x ...... * ..... . 40 I I o o 0 0 0 o o o I I o o o I o o o o e I o 0 0 o I o o o o I I o o o I o
o o

0 o o o o I I o o o o I o o o I I o o o o o o o o 0 I

o o o I I o . . . . . . 20 ....................... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Oate/Tirrie UP LOW
--.l -.l \0 0 ....., Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W219.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08:36:12 through 17-SEP-2016 12: 00:00 3143.00 through 3223.00 . . . . . . 3200 ............................................................................ o:::r tj" .-I I D* (!) )-(!) Cl:'. x x x x x x x LL.I 3180 z . . . . . . ..................................................... ' ..................... . . . . . . . LL.I a: LU CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B219.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:31:42 through 17-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' I I 1 1 I O 1 1 1 I 11 1 1 1 1 o 1 1 1 1 o 11 1 1 1 1 1 1 1 1 1 1 1 .. O I I 1 1 I 1 1 1 1 11 1 o 1 1 o_o 1 1 1 1 1 .' 1 I O 1 1 o I 1 1 1 1 *1 1 1 1 o 1 1 .06 . . . . . . o I I o o o o o o I I o I I o I o I o I I I I o o I 0 o I o o I I I o I o I I o I I o o I I o o I 0 o o 0 o o I I o o o I I I o o I o o o o o 0 o 0 I o . . .04 . . . . 0 2 ............ * .......... * ............ ; .......... * ............ : ............ * ..... . 0 ........ __ .__ ........ ___, __ __ "--........ ...................... 3-16 LOW 4-16 5-16 9-16 6-16 7-16 8-16 MeasureMent Date/TiMe

1 00 -QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W220.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 11:11:34 through 17-SEP-2016 12:00:00 0.234900 through 0.249440 . 245 ' ' 0 0 o ' 0 0 0 o o ', 0 0 o ' o o 0 o o ' ,' 0 0 o ' o o 0 0 ' 0 o ', 0 ' ' o o 0 0 I 0 o : o o I 0 0 0 I o o o 0 'o I o o 0 I 0 0 o o o I o 0 0 0 o : 0 0 . . u c ID *r-1 u *r-1 4-4-UJ ID x "0.0 '° I-ID x x x > . 24 a: . . . . . . I o o 0 0 I o o o o I I o 0 0 o I o 0 o o I I 0 0 0 o o o o o I I o O 0 o o o o o 0 I 0 o o o o I 0 o o I I o o o I I o o 0 I I o o o 0 I o o o 0 I I o . . . . . . . 235 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ................ . 3-16 4-16 5-16 6-16 7-16: 8-16 9-16 MeasureMent Date/Tir.-.e UP LOW

-.....:i 00 N 0 Vt 00 0 \0 QA filenaMe. DKA100: ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 16-MAR-2016 11:11:34 through 17-SEP-2016 12: 00:00 Lower/Upper LMts: 184. 000 through 204. 000 200 . ' ......................................................................... . . . . . . . I D (!:I )-I-H > H I-u <I w D H ....I u ::i z 190 . . x . . . x . . ' ......... * ........................ * ........................ *. x .... ' ' ........... . x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW --.I 00 w 0 ......., Vl 00 0 "° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W220.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 11:11:34 through 17-SEP-2016 12:00:00 5.00000 through 100. 000 80 ........... * ........................ * ........... .-........... * ............ * ...... . """" I D (.!) z D H ::i ....I D rJ) w (I:'.. ::..::: a: w 0.. . . . . . . 60 I o o o o o o o o o 0 I o o o o o o o o o I o o 0 0 o o o o o o o o o o o o o o o o I 0 0 o o 0 0 0 0 o 0 I o o o o o o o o o o o o o o o o o o o o 0 o . . . . . . x x x x . . . . 40 . ' ......................................................................... . . . ' . . . 20 ........... *' .......... ' ........... ' .......... ' ........... ' ........... *' ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOl.iJ QA filenaMe DKA100: [ENV_ALPHA.QA.W]W220.QAF;3 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 16-MAR-2016 11:11:34 through 17-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 320*0 . . . . . . o O O O O O O O O O I O o O O O I O O O O I I O O O I o O o o I o o o o I I o o 0 0 I o 0 0 0 I 0 0 0 o I I 0 o o I I o o o o o
o o o I o 0 0 o I 0 0 . . . . . . co ""'" ...-l I D (!) )-(!) 0:: :x x x x x LLJ 3180 z . . . . . . o I o o 0 I 0 0 0 o o 0 o o o I 0 o o o o 0 o o 0 0 0 0 0 o 0 0 o o o o o o o o o o o o o o o I I o o o I o o o o o o o o o I I o o 0 0 0 o 0 0 o I 0 o . . . . . . LLJ ::..:: <I* LLJ CL 3160 ***********************-***********-**********-***********-******************* 3-16-4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:31:46 through 17-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 0 8 1 ' * ' 0 0 0 0 0 0 ' ,' 0 0 0 0 0 0 0 0 0 0 ', 0 0 0 ' 0 0 0 0 0 ' 0 ." 0 0 ' 0 0 0 1 0 0 0 ', 0 ' ' 0 0 0 0 0 0 0 0 .' ' 0 0 0 0 0 0 0 0 0 ,* 0 0 0 ' 0 0 .06 * * * ,I * * ............................................................................ . 04 . . .02 ............................................................................ . . . . . . LOW MeasureMent Date/TiMe
--.J 00 0\ 0 ......, Ut 00 0 \0 QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA.QA.W]W221.QAF;3 AYRGEFF (Average Efficiency) 16-AUG-2016 08:46:48 through 17-SEP-2016 12:00:00 0.249939 through 0.265399 . . . . .265 ' ,* o 0 o I 0 o o o I o o o 0 I o o o o o o 0 0 0 o 0 I o o o o I 0 o o o I o o 0 0 I o o o o o o o o o o o o o o I I o o o o 0 o o o o I o o 0 0 I I o :::-,. u i:::: Q) *r-1 u *r-1 4-4-UJ . . . . . . . . . 26 ............................................................................ . . . . x .255 x x x . 25 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ......................... . 8-16 8-23 8-30 9-06 9-13 MeasurefYlent Date/TifYle UP LOW .... -...! 00 -...! 0 ......, Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-AUG-2016 08: 46:48 through 17-SEP-2016 12: 00:00 184. 000 through 204. 000 . . . 200 ......................................................................... : .. . . . . I 0 (!) )-I-H > H I-u 0:: x w 0 H -I x u =i z 190 ................ * ................ * ................ : ................ * .......... . x 8-16 8-23 9-06 9-13 Measurer.-.ent Date/Tir.-.e UP LOW ...... -.l 00 00 0 ....., Vl 00 0 ID QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W221.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-AUG-2016 08: 46:48 through 17-SEP-2016 12:00:00 5.00000 through 100.000 I Cl z 0 H 1-::i ....I 0 tr) w O:'. ::..::: a: w 0... 100 80 .................... * ................ * ................ : ................ * .......... . . . . . 60 ............................................................................ . . . . x 40 x . . . . ... x .>ff: ......... .: ................ :. ............... ; ................ : .......... . 20 ............... '* ................ *' ............... ' ............... '* .......... . 8-16 8-23 8-30 9-06 9-13 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: PSENERGY-GD148 (PEAK ENERGY GD-148) 16-AUG-2016 08:46:48 through 17-SEP-2016 12: 00:00 3143.00 through 3223.00 . . . . 3200 ............................................................................. . . . . ro """ ...... I D (!) )-(!)" et:: x x :$: x LLJ 3180 z . . . . ........... ' . ' ............................ ' ................................ . . ' . . LLJ :..:: q; LLJ CL 3160 .............................................................................. . 8-16 8-23 8-30 9-06 9-13 MeasureMent Date/TiMe UP LOW QA filename Parameter Name 5tart/End Dates Lower/Upper Lmts: DKA100: [ENV_ALPHA.QA.B]B221.QAF;2 BACKRATE (Background Rate) 11-AUG-2016 15: 56:48 through 17-5EP-2016 12:00: 00 O.OOOOOOE+OO through 0.100000 I 0 8 ' ( ' o ' 1 ' ' ' ' 1 1 o ', o ' o ' o o ' 1 ' o 1 o o 00' ' ' 1 1 ' o ' ' 1 ' ' ' '0 1 ' ' '
1 1 o o ' 1 o ' ','

1 o ' ' 1 1 ' ' ' ' 1 ' ." ' ' o 1 ' . 06 . . . . . ............................................................................ . . . 04 .02 ............................................................................ . . . . . 0 ................. ......... 8-11 8-18 8-25 9-01 9-08 9-15 Measurement Date/Time UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: '255 u c ID *r-1 u *r-1 4-4-UJ x ID "0.0 l(i I-DKA100: [ENV_ALPHA.QA.W]W222.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:36:25 through 17-5EP-2016 12: 00: 00 0.244366 through 0.259480 x x x x . -. . . . x ID .25 o ' o o 0 0 o o o o 0 I o o o o 0 o o o o I o o o o I I o ' o I I o o o I I o I o o I 0 I o o o I o o o 0 I o o o I I o o o I o o o o o I o o o 0 I ' o > . . . . . . <r x '245 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W222.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:36:25 through 17-SEP-2016 12:00:00 184.000 through 204.000 200 ........... " .......... * ........................ * .......................... * ..... . I Cl (!) )-I-H > H I-u a: x x x w Cl x x x H ....I u ::i z x 190 . . . . . . o ' o o o o o o o 0 I ' 0 0 o I 0 0 o o 0 0

0 0 0 I 0 o o 0 I I 0 0 o 0 0 0 0 0 0 t 0 o 0 0 I I o o o o 0 0 0 o I 0 o o 0 o o o o o o 0 0 o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W222.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:36:25 through 17-SEP'-2016 12:00:00 5.00000 through 100.000 80 ........... * ............ * ........... * ........................ *, ........... * ...... . ..-i I 0 z D H 1-::i _J D (J) w O:'. :::..::: a: w* 0... 60 . . . . . . o o o 0 o o o o o o 0 0 o o o o o o o o 0 I o o o o o o o o 0 I o o o o o o o o o 0 I o o o o I o o o o I I o o o 0 0 o o o o o o o o o o o o o o o o o . . . . . . x x x x x x x . . . . 40 ............................................................................ . . . . . . 20 ........... " .......... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W222.QAF;3 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) 5tart/End Dates 16-MAR-2016 08:36:25 through 17-5EP-2016 12:00:00 LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . ' 0 0 0 0 ' I o o

0 o o o o o o o o o o o o o o o o o o o o o o o 0 o I I 0 o o 0 I o o o o I o o o o o I o o o I I o ' o o o o o o o o o o I o I o o . . . co "=:!" """"" I D )-Ct'. x x x x x x x w 3180 z . . . . . . ......................................................................... ' .. . . . . . . w a: w 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
--.) \0 Vl 0 ......, Vl 00 0 \0 QA filenal'Je Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: DKA100: [ENV_ALPHA.QA.B]B222.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:31:54 through 17-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' 1 o ' ' ' 1 ,' ' ' ' 1 1 o o o o 1 1' o ' o 1 1 o o o o ' o ." o 1 1 o o o o 1 o ' o, o 1 o o o o 1 1 o o o .' ' ' ' ' ' 1 ' ' ',' ' 1 1 ' . . . . . . '06 o o o o o o O O O I I I o o o o o o o O o o o o o O o o o 0 o I I o o o o o o o o o o o o o o I I o o o o I o o o I 0
o 0 I I o o 0 0 I o o o o o I o '04 . . . '02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOW QA filenar<le Para1T1eter Nar<le Start/End Dates Lower/Upper Lr<lts: DKA100: [ENV_ALPHA.QA.W]W223.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:36:30 through 17-SEP-2016 12:00:00 0.246039 through 0.277420 .27 ' ' o o o o o o o o o o o o o o o o o o o ' ' o o o o o o 0 o 0 ' e 0 o I I 0 0 o 0 I 0 0 o o 0 0 o o o 0 o o o o o o o o o o o o o o o o o o o o o o o >, u c I}) *r-1" u *r-1 4-4-UJ . . . . . . . . . . . . .26 .......... *.* .......... * ........................ * .................. *x* ... *.* ..... . x x x x x x . . . . . . . 25 I I o o o o ' o o o o o o o o o I o ' o ' o o o 0 o 0 I o o o o 0 o o o o o o o o o o o o o o o o o o o o I o o o I I 0 o 0 o o o o o o o o o o o o o o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tir<le UP LOU.I QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:36:30 through 17-SEP-2016 12:00:00 184.000 through 204.000 200 ............ * .......... ' ....................... * .......................... * ..... . I D .>-I-H > H I-u a: w D H ....I x x x x u :J x x z x 190 ' ' o ' o ' o ' o 0 0 'o 0 0 o ' o o o 0 o 0 1' o 0 0 o I 0 o o o o o ', o o o o o o o o o o : o o o o o o 0 I o 0 e '1 I 0 0 0 I o o o o o o 'o o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
--..l \0 00 0 ......, Vl 00 0 \0 QA*filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W223.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:36:30 through 17-SEP-2016 12: 00:00 5.00000 through 100.000 80 ' .......... * ........................ * ........... .-........... * ............ * ...... . '0-i I Cl z 0 H 1-::i ....I 0 (J) w O:'. :>.:: a: w 0... . . . . . . 60 o o o o o o o o o o o o o o o o I o o o o o o o o o o 0 o 0 0 f o o o 0 I I 0 o o o I o o o o o o o o o o o o o o o o o o o 0 0 0 o o 0 0 o o o o I I o . . . . . . x x x x x x x 40 ............................................................................ . . . . . . 20 ........... *' .......... ' ........... , .......... ' ........... , .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKAlOO: [ENV_ALPHA.QA.W]W223.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08:36:30 through 17-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200
I o o o I o o o o I I o o o I I o o o O I O o o o o o o o o I o o O o I O o o o o o o o o o I o o o o O O o o o o o o o o o o o o o o o o o I o O o o ro v "<"i I D )-0::: x x x x x x x LL! 3180 z. . . . . . . I I o o o I o o o o I o o o o 0 I o o o o I o o o o o I o o I o o o o o I I o o o 0 0 o o o o o I o o o I I o o o I 0 I o o I o o o o o o o I o o 0 o o . . . . . . LL! loo! a: LL! 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent UP LOU.I QA filenaMe DKA100: [ENV_ALPHA.QA.B]B223.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 13:31:57 through 17-5EP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ° ' 0 0 0 ' ' o

0 ',* 0 0 0 ' ' 0 0 o 0 0 ', 0 0 0 ' ' 0 0 0 0 ' 0 ." 0 ' ' 0 ' 0 0 1 0 0 ', 0 0 0 0 o 0 o 0 0 0 0 .' 0 0 o 0 0 0 0 0 0 0 0 00 o 0 0 0 0 0 .06 . . . . . . ............................................................................ . . . . .04 . . . . . . 02 ............ * .......... * ............ ; .......... * ............ ; ............ * ..... . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
-00 0 -QA filenarrie Paraf"l'le ter Naf"l'le Start/End Dates Lower/Upper DKA100: [ENV_ALPHA.QA.W]W224.QAF;4 AYRGEFF (Average Efficiency) 16-AUG-2016 08: 47:00 through 17-SEP-2016 12: 00: 00 0. 250168 through 0.265640 . . . . .265 ............................................................................ x u . 26 c . . . . .............................................. -............................ . . . . . Q) *.-f u *.-f x 4-x 4-UJ Q) "OJ) x x (rj s-Q) > a: . 255 x . ............................................................................ . . . . 8-16 8-23 .8-30 9-06 9-13 Measuref"l'lent Oate/Tirrie UP LOW -00 0 N 0 ......, Vl 00 0 l.O QA filenaJYJe ParaJYJe ter Name Start/End Dates Lower/Upper Lmts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-AUG-2016 08:47:00 through 17-SEP-2016 12: 00:00 184.000 through 204.000 200 ............... * .................. * ............... : ............... * ......... ' .. I 0 )-f-H > H f-u a: w 0 H ....I u ::i z x x xx x x 190 ................ * ................ * ................ : ................ * .......... . 8-16 8-23 8-30 9-06 9-13 Measurement Date/TiJYJe UP LOW -00 0 l;.l 0 ....., Ul 00 0 '° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W224.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-AUG-2016 08: 47:00 through 17-SEP-2016 12:00:00 5. 00000 through 100.000 80 ' ' ' o o ' o o o o 0 o o 0 o ,' 0 o o o o I I o o o o o 0 0 o o 'o o o o I o ' o o
o o 0 o o I : o o o I I o o o I I o o o I o o' o o o I o o' o 0 I I ..-I I D (!) z 0 H 1-=i --' 0 en w O:'. a: w 0.. . . . . 60 I 0 o o o I I o 0 o 0 I o o o o ' o o o o I I o o o I I o o o o 0 o o o I I o o o o I o o o o I I o ' o I I o o o 0 I o o o o I o o o o I o o o o ' I o . . . . x x 40 ............................................................................ . . . . 20 ............... '* ................................. ' ........................... . 8-16 8-23 8-30 9-06 9-13 Measurerrient Date/Tirrie UP LOW
........ 00 0 0 ......, Vl 00 0 ID QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LIY'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W224.QAF;4 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-AUG-2016 08:47:00 through 17-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . 3200 I I o 0 0 I 0 o 0 0 I I 0 0 0 0 0 o 0 o o 0 0 o o 0 o 0 0 0 0 I o o
0 I o 0 0 0 0 I o o 0 o 0 0 0 0 o I o o o o o I 0 o 0 I I o o o o I

o 0 0 I I 0 . . . . co v ....... I D C) )-C) Cl:: x x :m: x LL.J 3180 z 0 I I 0 o o o o o I I o o o o o o o o I o o o o o o o o o 0 o o o o 0 o 0 o '0 0 0 o 0 o 0 0 0 o 0 0 o I 0 o o 0 o o 0 o 0 0 0 o 0 I 0 0 0 o o I 'o o o I I 0 . . . . LL.J a: LL.J Cl.. 3160 8-16 8-23 8-30 9-06 9-13 MeasurefY'lent Date/TifY'le UP LOW QA filenaf'l"le Paraf'l"leter Naf'l"le Start/End Dates Lower/Upper Lf'l"lts: DKA100: [ENV_ALPHA. QA. 8]8224. 2 BACKRATE (Background Rate) 11-AUG-2016 15:56:52 through 17-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 '08 ' o

o

0 o *

o I I o 0 0 0 I o o o o o o o o o o 0 o o o o o o o o o o o o o o o o o o o o I 0 0 o I I 0 o 0 0 I 0 0 o o I 0

o o I 0 o

o I I 0 . . . . . . . . . . '06 o o o o 0 I 0 o o 0 I I o e o o o o o o o o o o o o I o o o o o I I o o I I o o o o I o o o o I o o o o o o o o o o O o o o o o o o o o I o o o o o I o '04 . . '02 ............................................................................ 0 8-11 . . . . . 8-18 8-25 9-01 9-08 9-15 MeasureMent Date/Tif'l"le UP LOW
...... 00 0 0\ 0 I-+) Vo 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: . 265 u c Q) *r-1 x u *r-1 4-. 4-UJ Q) "OJ) . 26 ({j Q) > a: DKA100: [ENV_ALPHA.QA.W]W225.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:36:41 through 17-SEP-2016 12:00:00 0.253380 through 0.269055 x x x x x x x I 255
1 0 ' ' 0 1 0 0 0 ',* 0 0 0 1 0 0 0 0 0 1 *, 0 0 0 '* 1 0 0 0 1 1 0 ," 0 0 0 0 0 0 0 0 0 0 *, 0 ' 1 0 0 0 1 0 0 0 0 : 0 0 0 0 0 0 0 0 0 0 1 00 0 1 0 1 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-00 0 -....] 0 ....., Ul 00 0 \0 QA f i lenarrie -Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W225.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:36:41 through 17-5EP-2016 12:00:00 184.000 through 204.000 200 ............ * .......... * ............ : .......... * ............ : ............ * ..... . I 0 )-f-H > H f-x u cr: w 0 H ...J x x x x u :J x z 190 ........... * ....... x ................ * ........... : ........... * ............ * ...... . x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ...... 00 0 00 0 ....... Vl 00 0 \0 QA filenartle Parartleter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W225.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:36:41 through 17-SEP-2016 12: 00:00 5.00000 through 100.000 80 . . . . . . . . . . . *. . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . .-. . . . . . . . . .. *. . . . . . . . . . . . *. . . . . . . -M I D (!) z 0 H 1-:l _J 0 ({) w Ct'. :::..:: a: w 0... . . . . . . 60 o o o o o o o o o o O o o o o o o o o o o O O O O o I o o o o o o o o o I o o o o o o o o o o I I O o o o o o o o o I o o o o o o o o o o o o o o o o o . . . . . . x x x x x x x x . . . . . . 40 I o o o o o o o o o o I o o 0 I I 0 o o o o o o o o o o o o o 0 0 o o o o o o o 0 0 I o 0 o o o o o o o I I o o o o o o o o 0 I o o o o o o o o o I ' o . . . . . . 20 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tiffie UP LOW ...... 00 0 \0 0 ....., Vl 00 0 l.O QA filenafl"le Parafl"le ter Nafl"le Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W225.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08:36:41 through 17-SEP-2016 12: 00: 00 3143.00 through 3223.00 . . . . . . 3200 ' o ' o 0 o I o o o 0 0 o o 0 o 0 o o o o o I o o o I I o o o o o o o o I I o o o o I o o o o I 0 o o o o I o o 0 o I o o o I 0 o o o o o o o o o o ' o ro ""'" ...-! I D )-0::: x x x x x x x x LL.I 3180 z . . . . . . o o o o o o o o o o o I o 0 o o I o o o o I 0 o o o o o o o o o I o o o o o o o o o I o o o o ' I o o o o 0 o o o o o o o o I o o o o o o o o o o o I o . . . . . . LL.I ::..::: a:* LL.I 0.. 3160 "3-16* 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl"lent Date/Tifl"le UP LOW ....... 00 ....... C> 0 ......, Vi 00 C> ID QA filenaMe DKA100: [ENV_ALPHA.QA.B]B225.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Dates 4-MAR-2016 13:32:05 through 17-5EP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 .08 o 0 0 0 o ' 0 o o o ' o o o o ' I o 0 0 o o o o o o o o o o o 0 I 0 o o o o o o o o o o o o 0 0 o o o o o o o o o o o o o 0 o o o o o o o o o o o I ' o . . . . . . .06 . . . . . . . . .... *. . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . . . : . . . . . -. . . . . . *. . . . . . . . . . . . . . . . . . . . . . .04 .02 ............................................................................ . . . . . . . x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... 00 ....... ....... 0 >-+, VI 00 0 \0 QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W226.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-201615:11:24 through 17-SEP-2016 12: 00: 00 0.259485 through 0.275535 I 275 ' ' ' ' 0 ' ' ' 0 ' '*' ' ' ' ' ' 0 0 ' 0 ' .. *' **' ' ' 0 ' o 0 0 I' 0 o 0 0 0 0 0 0 0 0 .. 0 0 ' 0 0 0 0 0 o 0 0 I' 0 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 (..) c I}) *r-1 (..) *r-1 4-4-UJ x x . . . . . . .27 *****x*****:******x****.*****x*****:***********.***********:***********.******* . . . x . . x . x . 265 . . . . . . ............................................................................ . . . . . . '26 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... 00 ...... N 0 ......, Vl 00 0 '° QA filena!Yle Para1Y1eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 200 x I D )-I-H > DKA100: [ENV_ALPHA.QA.W]W226.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 15:11:24 through 17-5EP-2016 12: 00:00 184. 000 through 204.000 x x x x H 150 . . . . . . . . . . . *. . . . . . . . . . . : . . . . . . . . . . . *. . . . . . . . . .. : . . . . . . . . . .. *. . . . . . . . . . . . . . . . . . . . I-. . . . . . u a: w D H ...J u ::i z 100 ........... " .......... ' ........... ' .......... ' ........... ' .................. . 3-16. 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ,_. 00 ,_. l;.l 0 H-, Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 ..-I I 0 z 0 H I-DKA100: [ENV_ALPHA.QA.W]W226.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 15:11:24 through 17-SEP-2016 12: 00:00 5. 00000 through 100.000 =i 50 ............................................................................ _J 0 01 w Ct'. ::..:: a: w 0.. x . . . . . . x x x x x x 0 3-16 4-16 5-16. 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenafYle ParafYte ter NafYle Start/End Dates Lower/Upper LMts: 3200 x ro tj" ........ DKA100: [ENV_ALPHA.QA.W]W226.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 15:11:24 through 17-SEP-2016 12:00: 00 3143.00 through 3223.00 x x x x I 3100 ............ * .......... * ........................ * ............ .' ............ * ..... . D )-et: LLJ z LLJ :t.::: a: LLJ 0... . . . . . 3000 ............................................................................ . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYte UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.B]B226.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:32:09 through 17-SEP-2016 12:00: 00 O.OOOOOOE+OO through 0.100000 '08 ............................................................................ . . . . . . . . . . . . '06 ............................................................................ . 04 '02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W227.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 08:36:54 through 17-SEP-2016 12:00:00 0.255004 through 0.270778 . 27 ............................................................................ . . . . . . >.. (.) . 265 c . . . . . o o o o o o o 0 0 o 0 o o o o o I o 0 0 0 0 o o o o 0 0 o o o 0 o o o o 0 0 o 0 o o o o o o 0 I 0 o o o o I 0 0 0 0 o o o o 0 0 0 0 o o o o 0 0 0 I 0 o . . . . . . I}) *n (.) *n x 4-4-UJ I})" "o.Q ({j I-I}) > x (J: . 26 . x . . . . . .......... *:* ..... *; ... *: .... *x* .... :* .... *x .... *: ........... :* .......... *:* ... : .. x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ,_. 00 ,_. -.l 0 ......, Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start I End Da*tes Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W227.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:36:54 through 17-SEP-2016 12:00:00 184. 000 through 204.000 200 .......................................................... ' ................ . . . . . . . I Cl )-t-H > x x x H t-u a: w x x x D x x H ....I u :J x z 190 . . . . . . I I 0 o o I o o o o I 0 o o o I o o o e o I I o o o o I o o o I ' o o o I I o o o o I o o o o I o o o o o I o o o o o o o e o I o o o o I o o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW 00 0 ....., !.Ji 00 0 '° QA filenarrte Pararrte ter Narrte Start/End Dates Lrrtts: 100 DKA100: [ENV_ALPHA.QA.W]W227.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08:36:54 through 17-SEP-2016 12: 00:00 5.00000 through 100. 000 80 I I I I I I I I I I I 'o I I I o I I I I I I .. I I I I o I I I 0 o o '1 o o o o I o I o o I .. I I o I o I o o o o o 'o I o o I o o o o o o 0 '1 I I I o o 0 ..-I I 0 (!) z D H 1-:J ....I D (f) LLJ Q'. :..::: a: LLJ o_ . . . . . . 60 ' I o o I o o o o o o 0 o o o I o o o o o o o o o I 0 o o o o o o o o 0 I o o o o o ' o o I I o o o o o o 0 I o o o ' o o o I 0 o Io o o o o I 0 I I o . . . . . . . x x x x x x x 40 x .......... *.* ...... .... : ........... : ............ : ........... : ............ :. ..... . 20 ....................... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrtent Date/Tirrte UP LOW ID 0 ....., Vi 00 0 ID QA filena!Y'le ParafY'le ter Na!Y'le Start/End Dates Lqwer/Upper LIY'lts: 3220 DKA100: [ENV_ALPHA.QA,W]W227.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08:36:54 through 17-SEP-2016 12:00:00 3143. 00 through 3223. 00 . . . . . . 3200 ' ' o o 0 ' ' 0 o o o o o o o I I o o o o I I o o o 0 0 0 0 0 I I o o o o o o o o 0 ' o 0 0 ' I 0 o o o I I o o o o I o o o o I 0 0 ' 0 0 o o o o o o o . . . . . . ro tj" ..-I I D )-0: x x x x x x x LL.I 3180 z . . . . . . o o o o o I o o o o I o o o o I I o o o o o I o 0 0 o o o o o I I o o o o I ' 0 o o o o o o o I o o o o I I o o o I 0 o o o I o o o o e I o o o o o I o . . . . . . LL.I :::..! a: LL.I 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Y'lent Date/TifY'le UP LOW ,_.. 00 N 0 0 ......, Vi 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B227.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Dates 4-MAR-2016 13:32:14 through 17-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 '08 0 o o o o 0 o o *
o 0 o

0 I 0 o o '

0 0 0 0 o 0 0 0 o o o I o o 0 I I o o o o I o o o o I I o o o o ' o o o I I o o o I I o o o o o o o o o o I I . . . . . . '06 -. . . . . . ............................................................................ '04 .02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-00 N -0 ....., Vt 00 0 \0 QA filenafYle ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: AVRGEFF (Average Efficiency) 16-MAR-2016 08:36: 59 through 17-SEP-2016 12:00:00 0.250600 through 0.266100 . 2 fr5 . . . . . . . . . . . .. . . . . . . . . . . ' . . . . . . . . . . . ' . . . . . . . . . . ' . . . . . . . . . . . ' . . . . . . . . . . . . . . . . . . . x ::.-, 0 c ID . 26 *ri 0 *ri 4-4-UJ ID x "0.0 l1j x S-x ID > x a: x x . 255 .... *x ..... :* .......... : ........... : .......... : ........... : ........... :* ..... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefYlent Date/TifYle UP LOW ,_. 00 N N 0 ....., Vl 00 0 ID QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 16-MAR-2016 08:36:59 through 17-5EP-2016 12:00:00 184.000 through 204.000 200 ............ * .......... * ............ .' .......... * .......................... * ..... . I 0 (!) >-1-H. > H 1-u a: w 0 H ....I u :J z x x x x x x x x 190 ' '
o o o o o o * ' 01 o o o I 0 o o 0 o o ," o o o o o o o 0 I 0 o *, 0 0 o o o o o I o o .. o o o 0 0 o o I o o o 0o o o o o I I 0 o 0 o I 00 o o o o I I 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenarrre Pararrreter Narrre 5tart/End Dates Lower/Upper Lrrrts: 100 DKA100: [ENV_ALPHA.QA.W]W228.QAF;3 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 16-MAR-2016 08: 36:59 through 17-5EP-2016 12:00: 00 5.00000 through 100.000 80 ........... * ........................ * ........... .-........... * ............ * ...... . -M I D (!) z 0 H 1-::J .....I 0 (!) LLJ :...:: a: LLJ 0... . . . . . . 60 ............................................................................ . . . . . . x x x x x x x x . . . . 40 ............................................................................ . . . . . . 20 ' .......... " .......... ' ............ , .......... ' ........... , .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Oate/Tirrre UP LOW QA filen-arrie -Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W228.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 08: 36:59 through 17-5EP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ . . . co ¢ ..; I D (!) )-(!) CJ:: x x x x x x x x . . . . . . I 0 o o 0 I 0 o ' o 0 ,' o 0 o I I o 0 0 o o ', o o o o o o o o o o o; o o o o o o o o o o 'o o o o o o ' o 0 ... o o: o o o o o o o o o o o ,' o o o o o o w 3180 z w ::..:: a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
-00 N Vi 0 ....., Vi 00 0 \0 08 filenaMe DKA100: [ENV_ALPHA.QA.B]B228.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:32:17 through 17-SEP-2016 12: 00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 . 08 ' ' ' 0 ' ' ' ' e ' o o o ' o ' ' o o o o o o o o 0 ' ' o o o ' ' o o o 0 0 o o o o o o o o o o o o o o o o o o o ' I o 0 o I o o o o o o o o o o o 0 0 . . . . . . . 06 . . . . . . o o 0 o o I 0 o o o I I o 0 o I 0 o 0 I o I I o o o O I O 0 0 0 o o o o o o o o o o I o O e o I I 0 0 0 I 0 o o o o o o o o o o o o o I I o o 0 o I o o '04 '02 ........................................... -............................... . . . . . . . 0 x* x x 3-16 x x x x % x x x
x x x x x x x x* x x 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMe ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W230.QAF;3 AVRGEFF (Average Efficiency) 16-MAR-2016 11:01:29 through 17-SEP-2016 12: 00: 00 0.244269 through 0.269380 . . . . . . .255 ......................................................................... ' .. . . . . . . >> (..) c ID. *n (..) *n x 4-4-x LU ID -x x x x "Q.I) ilj !-... x ID . 25 > H I-u a: x x x x w x CJ H x ....J u ::i z x 190 . . . . . . 0 0 0 0 0 0 0 o o o o o o o o o o o o o o o o o o o o o o o 0 0 I 0 o o o o o o o o I o 'o o I I o o o I 0 o 0 0 I I o o o I o o o o o o 0 0 0 0 o o o 3-16 4-16 5-16. 6-16 7-16 8-16 9-16 MeasureMent DateiTiMe UP LOW
...... 00 N 00 0 ......, VI 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W230.QAF;3 ParaMeter NaMe P5FWHM-GD148 (PEAK RESOLUTION GD-148) 5tart/End Dates 16-MAR-2016 11:01:29 through 17-5EP-2016 12:00:00 Lower/Upper LMts: 5. 00000 through 100. 000 ..-! I 0 (.!) z 0 H ::i _J 0 (f) w 0:: ::..::: a: w 0.. 100 80 ........... * ........................ * ........................ * ............ * ...... . . . . . . . 60 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o 0 0 o o 0 o 0 I o 0 o o o o o o o o o o o o o o o o o o o 0 o o 0 I o 0 o 0 I 0 o . . . . . . x x x x x x x . . . . 40 ............................................................................ . . . . . . 20 ....................... ' ........... ' .......... ' ........... ' .................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... 00 N \0 0 ....., Vi 00 0 \0 QA filena[l"Je Para[l"Je ter Na[l"Je Start/End Dates Lower/Upper L[l"Jts: 3220 DKA100: [ENV_ALPHA.QA.W]W230.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 16-MAR-2016 11:01:29 through 17-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 ' o o 0 o ' I o o o o ' o o o 0 0 0 o o o o I o o o I o o 0 o 0 I o o o I I o o o o I o o o o I o o o o 0 0 o o o o o o o o o o o o o o o o o o o 0 o o . . ro "'" """" I 0 (!) )-(!) Cl::: x x x x x x x LU 3180 z* . . . . . o o o o o o 0 o o 0 o o o o o o o o 0 ' ' o I o o o o o o o o o I o o o o o o o o o o o o o o o I o o o I ' o o o o o o o o o o o o o o o o o 0 o I o o . . . . . . LU :::..::: a: LU 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure[l"Jent Date/Ti[l"Je UP LOuJ QA filename DKA100: [ENV_ALPHA.QA.B]B230.QAF;2 Parameter Name BACKRATE. (Backgfound Rate) Start/End Dates 4-MAR-2016 13:32:25 through 17-SEP-2016 Lower/Upper Lmts: O.OOOOOOE+OO through 0.100000 UP I 08 I I I I 1 1 1 o o o 1 01 o o O I 1 1 o o o 1 'o o O O O O o o o 1 o o ," o I I o o o o 1 o o 10 o I O o o 1 o 1 o O I.' I I o o 1 1 1 o O O O ,' 1 o o 1 1 o '06 . . . . . . I 0 o o o* o o o o I I I I o 0 I I o Io o o I o o I I I I I 0 I I I o o o I o I 0 I I o o o o I I o o ' 0 I o o I I o o I o I 0 o o o o o o o Io o o o . . . . . . '04 . . . . . . 02 ............................................................................. . . . . . . 0 3-16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Time ...... 00 w ...... 0 ......, Vl 00 0 '° QA filenal'le Paral'leter Nal'le Start/End Dates -Ll'lts: DKA100: AVRGEFF (Average Efficiency) 10-AUG-2016 13:30:04 through 17-SEP-2016 12:00:00 0.220210 through 0. 233830 . 23 ' ' ' ' ' ' ' ' ' ' ' ' * ' ' ' * ' ' ' ' ' ' ' ' * * ' ' ' ' ' ' ' ' ' ' ' * ,*' ' ' ' ' ' ' ' ' o * .I' * ' ' ' ' ' ' ' ' ' I o ' ' ' ' ' ' >:. (.) c ID *r-1 x* (.) *r-1 4-x 4-LU X* ID x "0.0 (lj s... ID x > . 22.5 a: . . . . . ........... *x.-............ *.* ............ *.* ............ * .............. : ...... . 8-10 8-17 24 8-31 9-07 9-14 Measurel'lent Date/Til'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W231.QAF;3 ParaMeter NaMe NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) Start/End Dates 10-AUG-2016 13:30: 04 through 17-5EP-2016 12: 00: 00 Lower/Upper LMts: 184.000 through 204.000 UP 200 .............. * .............. * ............ * .............. * .............. : ...... . I 0 r H > H u w 0 H x x x u z X* ' '*' ' ' ' ' ' ' ' ' ' * ', o ' ' * *
o ' ' o o o o ',

o 0 I I o 0 0 0 0 o 0 o' 0 I o o o o o o o o o o I .. 0 o o 0 0 0 o I 0 o o o o : O O o o o o o 8-10 8-17 8-24 8-31 9-07 9-14 LOW MeasureMent Date/TiMe QA filenafYle ParaMeter NafYle Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W231.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 10-AUG-2016 13: 30:04 through 17-SEP-2016 12: 00:00 5. 00000 through 100.000 80 ............. * .............. * .............. * ............. : ............. : ...... . .,-i I Cl (!:I z D H =:i _J D 01 w O:'. 60 . . . . . ..................................................... ' ..................... . . . . . . x x . x. x . . . . . 40 I I 0 0 I I o I I o I 0 o I o o I o 0 0 o I O' I 0 o o I 0 o I 0 0 I o o I o o o o o o o o o o o

o I 0 ' 0 0 o o o 0 o o o o o o o o I o o o o o o o o . . . . . 20 ............................ *' ........................... ' .................... . 8-10 8-17 8-24 8-31 . 9-07 9-14 MeasureMent Date/TifYle UP LOW
-00 w .j:::.. 0 ,......, Vl 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.W]W231.QAF;3 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 10-AUG-2016 13:30:04 through 17-SEP-2016 12:00:00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . ' . ............................................................................ . . CD 'OJ" ..-i I D )-0::: X),ii{ x x LLJ 3180 z . . . . . ' o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o 0 0 0 I 0 0 o 0 o o o o o o o o o o o I o o o I I o o o o o o o o I 0 o o o o o o o o o o I o . . . . . LLJ ::...:: a: LLJ CL 3160 8-10 8-17 8-24 8-31 9-07 9-14 LOW MeasureMent Date/TiMe .... 00 w Vl 0 ......, Vl 00 0 '° QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.B]B231.QAF;2 BACKRATE (Background Rate) 10-AUG-2016 15:47:19 through 17-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 . 08 ' ' o o o ' ' o o o ' o o o o o o o o o o 0 0 o o o o o o o e o o o o o o o o o o ' o o e o o o o o o o o I o o o o 0 o o o o o o o o o o o 0 o 0 o o o . . . . . . 06 . . . . . I I 0 0 o I 0 0 o 0 I I 0 o o I o 0 o 0 o I I o o o o o o o o o I o 0
o I 0 0 o 0 0 o o o o I I ' o o 0 I 0 o o o o o o o O 1 o o o o I o I O O I I o . 04 . 02 ............................................................................ . . . . . 0 8-10 8-17 8-24 8-31 9-07 9-14 Measurerrient Date/Tirrie UP LOW
...... 00 w 0\ 0 ......, Vl 00 0 \C) QA filenafY'le ParafY'leter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W233.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 12:17:05 through 20-SEP-2016 12:00: 00 0.247620 through 0. 262936 . ' . . . . '26 ......................................... -................................. . :>.. (.) c Q) *r-1 (.) *r-1 4-* 4-UJ Q) "OJ) Ill Q) > a: . . . . . . .255 ***********.***********.-***********.***********.***********:******x****.******** x x x x x x . 25 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TifY'le UP LOW QA f i len-afYle ParafYleter NafYle Start/End Dates Lower/Upper LfYlts: DKA100: [ENV_ALPHA.QA.W]W233.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 12:17:05 through 20-SEP-2016 12:00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I 0 (!) )-f-H > H f-u -+) Ul 00 0 ID QA filenafY'le ParafY'leter Narrie Start/End Dates Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W233.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 12:17:05 through 20-SEP-2016 12: 00: 00 5.00000 through 100.000 80 o 0 o
o o o o o o ,*, o o ' 0 o o o o o o 'o o o o o o ' o o o o o' o o o o o o o o o o o'o o 0 0 o o o o o o o : 0 I o o o o o o o 0 o 'o o o o o o o 0 ..-j I Cl (!) z a H ::J ...J a if) w Cl:'. ::..::: a: w 0.. . . . . . . 60 .......... *:* ......... *> .......... *:* ......... *:* ..... 0 .... : ..... *X* .. *:* ..... *X x x x x . . 40 .......... ' ................................................................ . . . . . . ' 20 ............................................................ ' ........... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
...... 00 V.l \0 0 ....... Vl 00 0 \0 QA filenarrie Pararieter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W233.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-201612:17:05 through 20-SEP-2016 12: 00: 00 3143.00 through 3223.00 . . . ' . . 320"0 0 L 0 0 0 0 0 0 0 0 0 0 0 0 0 I 0 0 0 O 0 0 0 O O O O O O O O O O O O O O O O O O O 0 O O O O 0 0 O O O 0 0 O 0 O 0 I 0 O o I o 0 o o o o o o o o o I o . . co "'" ..-l I D (!) )-(!) 0::: x x x x x x x LlJ 3180 z . . . . . . .......... ' ................................................................ . . . . . . . LlJ ::...!. i" (j c Q) *r-1 (j *r-1 4-4-LU '255 DKA100: AVRGEFF (Average Efficiency) 17-MAR-2016 12:17:09 through 20-SEP-2016 12: 00: 00 0.243320 through 0.258370 x x . . . . . . '25 ..... x* ... *:* .......... :* .......... *: .......... *:* .... *x .... : .......... *:* ...... . x x x '245 . . . . . . O o O O o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o O O O o I o o o o o o o o o o o o o o o o o 0 o 0 o o o 0 0 o 0
0 I I 0 o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W234.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 12:17:09 through 20-SEP-2016 12: 00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I 0 (!)_ )-I-H > H I-u a: x w 0 H x x ....I u :J x z x 190 ........... * ........... * ............ * ..... *x* .... * ........... = ***** *x* ... * ....... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
-00 .j:::.. w 0 ....., Vl 00 0 \0 QA filenaMe ParaMe ter NaMe 5tart/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W234.QAF;3 P5FWHM-GD148 (PEAK RE50LUTION GD-148) 17-MAR-2016 12:17:09 through 20-5EP-2016 12:00:00 5.00000 through 100.000 80 ........... * ........... * ............ * ........... * ........... : ........... *, ...... . ..-! I Cl (!) z D H ::i _J D en w (t'. ::..:: a: w 0.. . . . . . . 60 0 I o o o o o o e o o o 0 0 o o o o o o o o o o o o 0 I o o 0 o o o o o o o o o e o o o o o o 0 o o o o I I o o o 0 0 0 o o I I o o o o o o o o o o o o . . . . . . x x x x x x x . . . 40 o I o o O I o o o o o o o o o o o O o o o o o o o o o o e o o o I O o O I O o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I 0 0 0 o 0 o 0 . . . . . . 20 ............................................................. ' ................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ..... 00 t 0 H, Vi 00 0 \0 QA filenarrre Pararrreter NaMe 5tart/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W234.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-201612:17:09 through 20-5EP-2016 12:00: 00 3143.00 through 3223.00 . . . . . . 3200 .......... ' ................................................................ . . . . . . . ID v ""'"" I D )-et:: x x x x x x x LLJ 3180 z . . . . . . .............................................................................. . . . . . ' LLJ :...::: ([ LLJ 0.. 3160 3-16 4-16 5-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B234.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:35:19 through 20-SEP-2016 12:00:00 0. OOOOOOE+OO through 0.100000 .. oa * * * * * * * * * * *.* * * * * * * * * * * .* * * * * * * * * * * *. * * * * * * * .. * *.* .......... = ***********. * ******* . . . . . . . 06 o o o 0 o o o o o o o I o o o I o o o o 0 o I o o o o o o 0 o I I 0 o o o I 0 o o o o o o o o o o o o o o I 0 o o I I 0 o o o o o o o o o o o o o o o o .04 . . . . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ..... 00 0\ 0 ....., Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper Lmts: . 26 DKA100: [ENV_ALPHA.QA.W]W235.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-201609:06:18 through 20-SEP-2016 12: 00:00 0, 245103 through 0.260263 x o ' o I o o >i . 255 I I o o o I o o o o I o o o o I o o o o o I I o o o o o o o o I I o 0 o 0 0 0 0 o o o o o o o I I o o o I I o o o o I o o o I I 0 o 0 o I o o o 0 I I o 0 . . . . . . c Q) *ri 0 *ri 4-4-LU Q) -0.0 i(i !-Q) > a: . 25 x x x x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... 00 ..j:::. -...J 0 I-+) VI 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/ End oa-tes Lower/Upper Lr.-.ts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:06:18 through 20-SEP-2016 12:00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I 0 (!) )-I-H > H I-u a: x w x 0 H x x x -' u =i z x x 190 . . . . . . 0 o 0 0 o o o o o o o o o 0 0 I I o o o o o o o O O O O O 0 o o o o o o .o o o o o o o o o o o I I o 0 0 o I 0 o o o o o o o o o o o o o o o o o 0 I o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ....... 00 .j:>.. 00 0 ......., Vl 00 0 "° QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W235.QAF;3 P5FWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09:06:18 through 20-5EP-2016 12:00: 00 5.00000 through 100.000 80 ........... * ........... * ............ * ........... * ........... : ........... * ....... . ...i I 0 z 0 H :J _J 0 (f) LLJ O:'. a: LLJ 0... 60 . . . . . . ............................................................................ . . . . . . x x x x x x x . . . . . 40 o o o o o o o o o o o I 0 e o o o o o o o o o 0 0 o I o e o o o o o o o 0 0 o o o o ' o o o o 0 o o o o o ' o o 0 o o o o o o o o o o o 0 o o o e o o o o o o I o 0 20 ............................................................ ' ................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W235.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:06:18 through 20-SEP-2016 12:00:00 3143.00 through 3223.00 0 I o I o o 3200 o O I O O I I O O O I O O O O 1 O o o o o O I o o I o o o O o o o o o o o o o O O O I O O I o I I o o o I o o o o o I o o o 0 o o o o o 0 o I o 0 I o o . . . . . . co v '<"i I D )-et:: x x x x x x x LL.J 3180 z . ' . . . . o I 0 0 o I o o o o I I o o o o I o o o o o o o o o o o o o o I I o o o o o o o o o o o o o o I I o o o o 0 o o ';_ o o 0 0 0 I I 0 o 0 0 I I 0 0 o 0 I o 0 o o I o I LL.J :l:.<: a: LL.J 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ...... 00 Vi 0 0 ........ Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B235.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:35:23 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 .08 ' ' ' o ' ' ' ' ' o ' ' ' o o ' ' ' ' ' o ' ' ' ' o o ' ' 0 o ' o o o o I I 0 0 o 0 I o 0 o 0 I 0 o 0 o o I o o o I I o o o I I o o o o I o o o o o I o . . . . . . '06 . . . . . . ............................................................................ '04 .02 ............................................................................ . . . . . . 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOl.i.J 0 ....., Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Date8 Lower/Upper LrritB: DKA100: [ENV_ALPHA.QA.W]W236.QAF;3 AYRGEFF (Average Efficiency) 17-MAR-2016 14:51:08 through 20-SEP-2016 12:00:00 0.251250 through 0.266790 . 265 ........... * ........... * ............ * ........... * ........... : ........... * ....... . >, x u c x Q). *r-i u .26 *r-i . . . . . . ............................................................................ . . 4-4-UJ x x Q) "0.0 i(i x x I-Q) x > a: . 255 . . . . . . o o o o o o o o o o o I 0 o o o o o o o o o o o o o o o o o o I I 0 0 ' 0 0 o 0 0 o 0 o o o 0 o I o o 0 I I 0 0 o I o 0 0 o 0 0 o 0 o o I 0 o o o I o o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeaBurerrient Date/Tirrie UP LOW ....... 00 Vl N 0 ....., Vl 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W236.QAF;3 Parameter NaMe (NUCLIDE ACTIVITY GD-148) Start/End Dates 17-MAR-2016 14:51:08 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 184. 000 through 204. 000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I 0 (!) )-I-H* > H I-u a: x w 0 H x x x x x ....J u ::i x z 190 .... '* ...... * ........... * ............ * ........... * ........... : ........... * ..... ,, .. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Time UP LOW ....... 00 Vl w 0 Hi Vl 00 0 '° QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W236.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 14:51: 08 through 20-SEP-2016 12:00:00 5.00000 through 100.000 80 ........... * ........... * ............ * ........... * ........... : ........... * ....... . ..-! I Cl z 0 H 1-::::i ....I 0 (f) Li.] O:'. a: Li.] 0.. . . . . . . 60 o o o e 0 0 I o 0 o o I 0 o o o o o o o o o o e o o o o o o o o 0 o o o o o o o e o I o o o o o o o o o I o o o o o o o o o o o o o o o o o o o 0 o o o . . . . . . x x x x x x x 40 ............................................................................ . ' . . . . 20 .......... '*' .......... *' ............................................... *' ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA f i lenar.-.e
Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W236.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 14:51:08 through 20-SEP-2016 12: 00:00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ . . . . . . co "'" """' I D )-0:: x x x x x x x LJ..I 318_0 z . . . . . .......... ' ......................... ' ...................................... . . . . . . . LJ..I ::..::: a: LJ..I 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
....... 00 Vl Vl 0 ....., Vl 00 C> \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B236.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 13:35:28 through 20-5EP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP .08 ............................................................................ . . . . . . .06 . . . . . . ............................................................................ . 04 .02 ............................................................................ . . . . . . 0 ................. ........... ___.."'"-_,,.__-;.:;,__,.._ .................... ...,__ ........... __,."'"-*-.......... ----;;.;,-..........._ 3-16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: .265 :>, u !: Q) *r-1 u *r-1 4-4-UJ I]) 'QI) i{j DKA100: [ENV_ALPHA.QA.W]W238.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 09:06:30 through 20-SEP-2016 12:00: 00 0.254020 through 0.269732 x x '26 Q) > .............................. x* ................................................ . <I: x x x x I 255 1 1 1 o o 1 ' o
1 101 ' 1 o 1 1 o o o o 1 11 o o o ' ' o o o ' 1 'o 1 o o 1 1 o 1 o 1 1 '*' o ' ' o o o 1 ' 1 o I o ' 1 o o ' ' 1 1 o o 11 1 o o o ' ' o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... 00 Vl -.l 0 ......, Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W238.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:06:30 through 20-SEP-2016 12:00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I CJ )-I-H x > H I-u a: w x D H x ....! x x u =i z 19-0 o ,r o o o o 0 o 0 0 o'o o o o o o ' ' 0 0 o 'o o o o o o o o 0 0 0 o' 0 o o o o o o o o o o'o o o 0 o o o 0 0 0 o : 0 o o o o o o o o o o 'o 0 o o o I o o x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ...... 00 Vi 00 0 ,....., Vi 00 0 \C) QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W238.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09:06:30 through 20-SEP-2016 12: 00:00 5. 00000 through 100.000 80 ........... * ........... * ............ * ........... * ........... : ........... * ....... . "'""'* I D C) z 0 H :J ...J 0 en w O:'. a: w 0.. . . . . . . 60 o o o o o 0 o 0 o o o I o o o I o o o o o o o o o o o o o o 0 I o o o o o o o o o o o o o 0 o o 0 0 o o o o o o o o o o o o f ' 0 0 o o o o o o o o o o . . . ' . . x x x x x x x 40 ............................................................................ . . . . . . 20 ................................................................................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW ....... 00 Vl \0 0 ........ Vl 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W238.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:06: 30 through 20-SEP-2016 12:00:00 3143.00 through 3223. 00
i * * * * . 3200 ............................................................................ co tj" """"" I D (!) )-(!) 0::: x x -x x x x x LLI 3180 :z o o o I o I ..... ' ..................................................................... . 0 o o o o I LLI ::...:: <I: LLI 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
..... 00 0\ 0 0 H) Vl 00 0 \0 QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.B]B238.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:35:38 through 20-SEP-2016 12: 00:00 O.OOOOOOE+OO through 0.100000 I 08 ° 0 * * * ' 0 ' ' 0 ',' ' ' ' ' ' ' ' ' ' 1 01 o 0 0 1 1 o 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 ',' 0 0 0 0 o 0 0 1 0 0 : 1 ' o 0 o 0 0 0 0 0 0 ,' 0 0 0 0 0 ' 0 .06 . . . . . . o 0 o o o I o 0 o o 0 I o ' 0 I o o o o o o o o o o o I o o o I o o I o o I o o o o I o o o o o o o o o 0 o o o o I o o o o I I o o o o o o o o o o o ' . . '04 . . . . 02 ............................................................................ . . . . . . 4-16 6-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -00 0\ -QA filenaMe DKA100: [ENV_ALPHA.QA.W]W240.QAF;3 ParaMeter NaMe AVRGEFF (Average Efficiency) Start/End Dates 17-MAR-2016 12:17:27 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 0.248737 through 0.264123 UP . 26 . . . . . . ' ' o '
I 0 o o o o o o o o ' o o o o o o o o o o o o o o 0 o o o o o o o o o

o o o o o o o o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o . . . . . . :>.. u c ID *.-! u *r-1 4-" 4-UJ x ID "OJ) x aj . 255 ............................................................................ . . . . . . ID > x a: x x x x I 25 ° ' 0 0 0 o 0 0 0 o '*' 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 '*' 0 0 0 0 0 0 o 0 0 0 I 0 0 0 0 0 0 0 0 0 0 '*' 0 0 0 0 0 0 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
-00 O'\ N 0 ....., Vl 00 0 \0 QA filenarrie Pararrieter NaP"te Start/End Dates Lower/Upper LP"lts: DKA100: [ENV_ALPHA.QA.WJW240.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 12:17:27 through 20-SEP-2016 12:00:00 184.000 through 204. 000 200 ............................................................................ . . . . . . I a >-I-H > H I-u a: x w x a H ....I u ::i z x x x x *x 190 . . . . . . o o 0 o o I o o o o o I o o o I o o o o o o o o o o o I o o o o o o o o I I o o o o I o o o o I o o o o o I o o o I I o o o o o o o o o ' o o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureP"tent Date/Tirrie UP LOLI.I QA filena!Y'le Pararrie ter Na*!Y'le Start/End Dates Lower/Upper LIY'lts: 100 DKA100: PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 12:17:27 through 20-SEP-2016 12:00:00 5.00000 through 100.000 80 ' ' o o o o ' o ' ' o'o " ' o ' o ' 0 o o I 'o o o o o o o o o o o ,' o o o o I o 0 o o o ,*, o o o o o o o o o o ; I o o o e I I o o o o ', o o '* o o o ..-I I Cl (!) z 0 H =i ...J 0 ({) w 0:: :::..:: a: w 0.. . . . . . . 60 ............................................................................ . . . . . . x x x x x x x . . . . . 40 ................ ' .......................................................... . . . . . . . 20 .......... '*' ............................................... ' ........... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W240.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 12:17:27 through 20-SEP-2016 12:00:00 3143.00 through 3223. 00 . . . . . . 3200 ............................................................................ . . . CD """ ..-I I D (!:I )-(!:I 0:: x x x x x x x . . . . . . ............................................................................ . . . . . . LLJ 3180 z LLJ :;,..::: a: LLJ CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ...... 00 °' VI 0 ......, VI 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B240.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:35: 47 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 Q) .i-' (lj O:'. 7J c :::; 0 5--0.0 .::L. u l1j co. I 0 8 ° ' ' ' ' ' 0 ' ' * '0' 0 o 0 0 ' 0
0 0 0 ,' 0 0 0 ' 0 o 0 0 ' ' ', 0 0 ' ' 0 0 0 0 '

0' 0 0 ' o 0 0 0 0 0 0 0 o 1 0 0 0 0 0 0 0 0 0 ,' 0 0 0 0 0 0 0 . . . . . . . 06 ..... ' ..................................................................... . . 04 . . . . . . . 02 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . 0 .3:-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOU.I
,_. 00 O'\ O'\ 0 ....., Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W241.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 12:17:36 through 20-SEP-2016 12:00:00 0.251040 through 0.266570 . . . . . ' . 265 0 I o o 0 I o 0 0 0 I I O o o I o o o o o o o o o o o I o o o I I o o o o o o o o o o o o 0 O I I o o o o o o o o o o o o o I I o O o o O o o o o o o o . . . . . . . ::>, (.) c Q) -r-1 . 26 (.) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . -r-1 4-4-x x x x LU x Q) "OJ) x n:1 l--Q) x > a: .255 o o o o o o o o o o 00o o o o o I o o o
0 00 o o o 0 o o o o o o o0 o o o o o o o o o o o0o O I I o o o o o o o : o o o o o o I o o O O 11 o o o o o o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Paraf"l'le ter Naf"l'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W241.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-201612:17:36 through 20-SEP-2016 12: 00: 00 184. 000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ........... " ...... . I Cl )-I-H > H I-u a: w Cl H ....I u :J x x x z 190 .......... *:* ......... *:* ..... :x* ... *:* ......... *:* .......... : .......... *:* ...... . x x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measuref"l'lent Date/Tirrie UP LOW
...... 00 0\ 00 0 ......, Vl 00 0 \C) QA filenarrre Parafile ter Narrre Start/End Dates Lower/Upper Lrrrts: 100 DKA100: [ENV_ALPHA.QA.W]W241.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-201612:17:36 through 20-SEP-2016 12: 00:00 5. 00000 through 100.000 x 8 0 ........... : ........... :* ..... x .... *: ..... x .... : ...... x .... : ........... :* ...... . ..-! I D z 0 H 1-=i 0 en w Q'. a: w 0.. x x x . . . . . . 60 ............ *' .............................................................. . . . . . . . 40 I I o o o o I o o o I o o o o o 0 o 0 o o I I o 0 o I I o o o o o o o o o o o o o o I o 0 o o o I O o o o o o o o o o o o o I I o o o o O o o o o o o o . . . . . . 20 ................................................................................ . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenal'le Paral'le ter Nal'le Start/End Dates Lower/Upper Ll'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W241.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 12:17:36 through 20-SEP-2016 12:00:00 3143. 00 through 3223. 00 . . . . . . 3200 ............................................................................ co v ..-f I D (!) )-(!) et:: LL.I 3180 z x x x x x x . . . . . . . . . . . : . . . . . . >.<. . . . :. . . . . . . . . . . .: . . . . . . . . . .. : . . . . . . . . . . . . . . . . . . . ... :. . . . . . . . LL.I ::..::: ([ LL.I CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurel'lent Date/Til'le UP LOU.I QA filenaMe DKA100: [ENV_ALPHA.QA.B}B241.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:35: 51 through 20-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.1GODOO UP .08 o '
0 0 0 0 o 0 0 0 I o 0 o 0 o 0 e 0 o I I 0 0 0 I I 0 o e o 0 0 o 0 0 0 o 0 o 0

o 0 o 0 I I 0 o I I o o o I I 0 o 0 o o o o o o I o o o o I 0 o . . . . . . . 06 . " . . . . . I I o 0 0 0 o 0 o o I 0 o o o I 0 o o o o I I o o o I I o o o I I o o o o o o o o o o o o o o 0 I o o, o I o o o o I o o o o I 0, 0 o 0 0 I o o 0 o I I 0 . . . . . . x '* 04 . . . . . 02 ............................................................................. . . ,. . . . x 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ..] -0 ....., Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: AVRGEFF (Average Efficiency) 17-MAR-2016 12:17: 40 through 20-SEP-2016 12:00:00 0.256891 through 0.272781 . . . . . . . 27 ...................... ' .................................................... . >.. 0 c I]) *ri 0 *ri 4-4-UJ I]) "0.0 l(j I]) > a: . . . x x . 265 x x x . 26 * * * * * * * * * * *** * * * * *x* * * ... * * * * * * * * * * *** * * * * * * * * * *** * * * * *x* * * * * * * * * * * * * * * ... * * * * * *

x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
...... 00 -..J N 0 >--+) Vl 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W242.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 12:17: 40 through 20-SEP-2016 12:00:00 184.000 through 204. 000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I Cl (!) )-I-H > H f-u <I: W* Cl x x H _J u x x x x ;:) z x 190 . . . . . . o ' ' ' ' ' ' o ' ' ' ' o ' o ' ' ' o o o ' ' o o o o ' o 0 o 0 0 o 0 o I ' o 0 o 0 I 0 0 o 0 o 0 o o o 0 o o o o o o o o o o o o o o o ' o o o o o o o x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW ..l V.l 0 ......, Vl 00 0 "° QA filenar.-.e Parar.-.eter Nar.-.e Start/ En_d Datea Lower/Upper lr.-.ta: 100 DKA100: [ENV_ALPHA.QA.W]W242.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 12:17:40 through 20-SEP-2016 12:00: 00 5.00000 through 100.000 80 o ' ' o o o ' o o 0 1'1 o o o I o o o o o I 'o o o 0 o o o o o o o ,* o o o o o o o o o o ,*, o 0 o o o o o o o 0 : I o o o o o o o o o 0 'o o o o o o o e ....... I CJ C) z 0 H 1-=:i ....I 0 01 w O:'. :::..::: a: w CL . . . . . . 60 o o e e o o o o o o o o o O o O O o o O o o o o o o o o o o O I I o o o o o o o o o I 0 o
o o o o o o I I o o o I o o o o 0 o o o o o I o o o o : 0 o . . . . . . x x x x x x x x . . . . 40 o o o o o o o o o o o I o O o O o o o o o o o o o o o I o O O o I o o o o o o o 0 0 0 o o o o o o o o 0 I o o o o o I o o o I I o o o o o o o o o o I o . . . . . . 20 ........................................................................ " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeaaureMent Date/TiMe UP LOW ..J 0 ......, Vi 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.W]W242.QAF;3 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 17-MAR-2016 12:17:40 through 20-SEP-2016 12: 00: 00 Lower/Upper LMts: 3143. 00 through 3223.00 UP 3220 3200 . . . . . . 0 o o o o o 0 o o o o o o o o o I o o o o o 0 o I o o o o o o o o o o o o o 0 o 0 o I o o o o I I o o o I o o o o o o o ' o I o o o o o I o o o o ' I o . . . ro v ..-i I D )-Ct: x x x x x x xx LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ :::..:: ([ LLJ a.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe
,_. 00 -.....) Vi 0 ....., Vi 00 0 "° QA filenaMe DKA100: [ENV_ALPHA.QA.B]B242.QAF;2 P*araMeter NaMe BACKRATE _(Background Ra.te) Start/End Dates 4-MAR-2016 13:35:54 through 20-SEP-2016 12:00:00 Lower/Upper Lrrits:. O.OOOOOOE+OO th:rough 0.100000 Q) +) l'lj O:'. lJ !: :i 0 1-"0J) .Y. 0 l'lj co . 08 ' ' 0 0 o 0 0 o o 0 o o o o o o o o o o o o 0 o 0 o 0 o o o o' o o o o o o o 0 o 0 o o e o o o o 0 0 o 0 o o o o o o ,0 o o 0 0 o o o o o o o o o 0 I o . . . . . . . 06 . . . . . . . 0 I o o o o o o o o o o o o o o o o o o o I I e o 0 I o 0 o o *o o o o o o 0 o 0 o 0 o o o o o o o 0 0 o I o o o o o o o o o 0 I o 0 0 o o o o o o o o o . . . . . 04 . . . . . . . 02 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . 4-16 5-16 6-16 7-16 8-16 9-16 Date/TiMe UP LOW ....... 00 -..J 0\ 0 >-+, Vl 00 0 \0 QA filenarrre Pararrre ter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: AVRGEFF (Average Efficiency) 17-MAR-2016 09: 06:51 through 20-SEP-2016 12:00: 00 0.243130 through 0.258200 . . . . . . . 255 ............................................................................ u c I]) *ri u *ri 4-4-UJ . 25 .... *x* ......................................................................... . x x x x x x . 245 .............................................................................. . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW ....) -....) 0 ......, Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W243.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09: 06:51 through 20-SEP-2016 12:00:00 184. 000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I 0 (!) )-f-H' > H f-u a: x x w 0 H x x x ....I u :::::i x x z 190 ........... * ........... * ............ * ........... * ........... : ........... * ....... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW .J 00 0 ....., Vi 00 0 \0 QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W243.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09: 06:51 through 20-SEP-2016 12: 00:00 5. 00000 through 100.000 ........ I Cl z 0 H ::i _J 0 (f) w O:'. ::..::: a: w 0.. 100 80 ........... * ........... * ............ * ........... * ..... *-* .... ; ........... * ....... . 60 . . x . . . . x : x : : x : : x : ........................................................................... X x 40 o I 0 0 o 0 0 o o o o 0 o 0 o 0 0 o o o o o I o o 0 o I o 0 o 0 I 0 I o I 0 I I *
I o 0 o o o I I o o I o o o o I o Io I o I Io o o I o o o o o o o . . . . . . 2,0 ' ' o o o o I o o o 1,0 o o o o I o o o o o o' I o o ' I o o o I I '* o o o I o o o o I o '*' o ' I o o o o ' o o I ' ' o o o ' ' o o o o *' o o o o ' ' o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: 3220 DKA100: [ENV_ALPHA.QA.W]W243.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:06:51 through 20-SEP-2016 12: 00:00 3143.00 through 3223.00 . ' . . . . 3200 ............................................................................ . . . . ro ""'" "'"""" I D (!) )-(!) 0::: x x x x x x x LL.I 3180 z . . . . . . ............................................................................ . . . . . . LL.I ::,..::: <I: LL.I CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measure!'lent Date/Til'le UP LOW
...... 00 00 C> 0 Hi Vl 00 C> \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B243.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) 5tart/End Dates 4-MAR-2016 13:35:59 through 20-5EP-2016 12: 00:00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 I 08 ° 0 0
0 ' ' * ' ' ',' * ' 0 ' ' ' ' ' ' 1 01 0 0 o 1 o 0 0 0 0 ' ', 0 0 0 ' 0 0 0 0 0 0 ',' 0 0 0 0 0 0 0 1 0 0 : 0 ' o 0 0 0 0 0 0 0 0 ,' 0 0 0 0 0 ' 0 .06 . . . . . . o o o o o o o o o o o 0 o o o I o o o o 0 0 o o o o 0 o ' o o o o o o o o o o o o o ' o o o o o o o o o 0 0 0 o o 0 o o o o o o o o o o o o o o o o ' o . . .04 . . .02 ............................................................................ . . . . . . 0 ......... 3_16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... 00 00 ....... 0 ......, Vi 00 0 \0 QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W244.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 09:06:55 through 20-SEP-2016 12:00:00 0.236059 through 0.250661 . . . . . . . '25 I I o o I I I o I o I I I 0 o o o o o o o I I o o o o I o o o 0 0 I o o I I o o o o I o o O I 0 I o o o o o o o o O o o o O o O I o o o o o o o o o O I . . . . . . :>i 0 c '245 ID I I o o I I I I o o o I o 0 0 I I o o o o I o O O O O o o o o o I o o O I I O o o o o o o o o I I I o O I O O o o o o o o o o o o Io O I O o o o o o o . . . . . . *r-f 0 *r-f 4-4-UJ ID "O!) l1j 5, .. : ID > a: x x '24 x .......... *:* .......... *:* ........... *:* .......... *:* .... *x.* ... : ..... *x* .. *:* ...... . x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW ....... 00 00 N 0 H) Ul 00 0 \0 QA f*i lenarrie Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: DKA100: [ENV_ALPHA.QA.W]W244.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:06:55 through 20-SEP-2016 12:00:00 184. 000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* ........ * .. : ........... " ...... . I 0 (!) )-I-H > H I-u a: LLI 0 H x x .....I u x ::i z 190 ........... * ........... " ........... : ........... * ........... : ........... * ....... x . . . . . . x x x I 3-16 4-16 5-16 6-16 7-16 8-16 Measurerrient. Date/ Tirrie UP LOW -00 00 l>.l 0 H) Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W244.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION 17-MAR-2016 09:06:55 through 12: 00: 00 5. 00000 through 100.000 80 ........... * ........... * .......... ' .* ........... * ........... : ........... * ....... . ..-!* I D C) z 0 H ::i ....I 0 en w O:'. ::..::: a: w 0.. . . . . . . 60 ........... ' ............................................................... . . . . . . . x x x x x *. x x . . . . . 40 ............................................................................ . . . . . . 20 ................................................... , ............................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -00 00 .j::. 0 ......., Vl 00 0 \0 -QA filenaMe DKA100: [ENV_ALPHA.QA.W]W244.QAF;3 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 17-MAR-2016 09:06:55 through 20-SEP-2016 12: 00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . ' . . . . I 0 0 o 0 I 0 o o o I o o o o o o o o o o I o o o o I I o o o o o o o o I 0 o o o o o o o o o o o o o o I I o o o I I o o o 0 ' o o o o o o o o o I I o . . . . . . co tj-* o:-1 I 0 (!) )-(!) 0:: x x x x x x x w 3180 z . . . . . . ......................................................... ' ................. . . . . . . . w ::..:: a: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ...... 00 00 VI 0 ......, VI 00 C> \0 QA filename DKA100: [ENV_ALPHA.QA.B]B244.QAF;2 Parameter Name BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:36:03 through 20-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' I I 0 o I 0 0 0 O' 0,1 0 I 0 I 0 0 0 I o I,' I I o I I o o o o I '1' 0 I I o o Io I o 'o' o I o I I I 0 I o I: I I o o o I 0 0 0 I 0 ,' o o o o : o o .06 . . . . . . ..... ' ......... ' ............................... ' ........................... . . . . . . . .04 . . . . . . ' 02 .......... *.* .......... : ...................... *.* .......... : ............ * ...... . 0 ......... __ ......._ ____ ____ ...._ __ __."'--.......... .................... .,__""'--......... --'.,__....._ ......... ___.._ 3-16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Time QA filenafY'te ParafY'teter Narrie Start/End Dates Lower/Upper Lrrits: . 265 ::;., u c ID *r-1 . 26 u *r-1 4-4-UJ ID "OJ) a:i ID > cr: x DKA100: [ENV_ALPHA.QA.W]W245.QAF;3 AYRGEFF (Average Efficiency) 17-MAR-2016 09: 06:59 through 20-SEP-2016 12:00:00 0.250917 through 0.266437 x x x x .255 o o o 0 o I
0 o 0 o'o o o o o o o o o o o ', o o o o I 0 o o o o 1' o o I I o o o o I o o'o o I o o o o o I o o : I I o o o I o o o o o 'o o o o o I I I x x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TifY'te UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA1DO: [ENV_ALPHA.QA.W]W245.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY.GD-148) 17-MAR-2016 09:06:S9 through 20-SEP-2016 12:00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........ ' .. *.* .......... : ............ * ..... ' . I Cl (!) )-....., H > H f-,. u a: w Cl x H ....I x u =i .x z 190 ........... * ...... * ..... * ...... ?< ..... * ............ * ...... ':< .... : ........... * ....... . x x 3-16 4-16 5-16 6-16 7-16 8-16* 9-16 Date/Tir.-.e UP LOW
"'C (I) ...... 00 00 00 0 ......, v.. 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W245.QAF;3 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 17-MAR-2016 09:06:59 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 5. 00000 through 100. 000 ..-I I 0 (!) z D H ::i ...J o* (J') w O:'. :,.:: a: w 0... 100 80 . . . . . . . ............................................................................ . . . . . . 60 o o o o o o o 0 0 o I 0 0 o o I o o o o o o o o o o o o o o 0 I ' 0 o o o o o o o o o o o o o o 0 o o o I I o o o o o o o o o o 0 0 o o I o o o o o o o . . . . . . x x x x x x x 40 I I 0 o 0 I I o o o o o o o o o o o o o o o o o o o o o o O o o o o o o o o o o o o o o o o o o o o o o O o o o o o o o o o o o o o o O I O o o I o I o . . . . . . 20 .......... '*' .......... " .......... '* ....................... ' ........... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -00 00 ID 0 ......, Ui 00 0 ID QA filenaMe ParaMeter NaMe 5tart/ End Da.tes Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W245.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:06:59 through 20-5EP-2016 12:00:00 3143.00 through 3223.00 o ' ' I ' ' 3200 I ' o o I I ' o 0 o I I 0 0 0 0 I o 0 0 0 I I 0 0 0 I o 0 o o I o o o o I o o o o o I 0 0 0 o o I o o o o I o o o I I 0 0 o I t o o o I o o o o o o o o co "'" I D )-0: x x x x x x x 0 o o 0 o I ' .......................................................................... . . . . . . . w 3180 z w ::...::: a: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.B]B245.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13: 36:07 through 20-SEP-2016 12:00:00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' * * * ' ' ' ' ' ',' ' o ' ' ' ' o ' ' '01 o o o o ' o o o ' o ', o o ' ' o o o o ' o ',' o 1 ' o o o 1 1 o o : ' 1 o o o ' ' ' ' ' '*' ' ' o' ' ' o . 06 ....................... * ........... : ....................... : ........... * ....... . . . .04 . . . . .02 ............................................................................. . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe -00 \0 -QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper Lrrits: u c Q) *r-1 u *r-1 '26 DKA100: [ENV_ALPHA.QA.W]W246.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 09:07:03 through 20-SEP-2016 12: 00:00 0.247020 through 0.262301 0 I I I
o

4-4-UJ '255 o I O I O I O o o O O I I I o O I o O o O I I O o o 1 O o o I O I I o O O o o o o o o o o o o o o o o o I o o I o 0 I I I 0 I I I I o o o o o I I o I o . . . . . . x x x x x x x I 25 I o o o o o ' o o I o,o o o o ' o o o o o o ,o o o o ' ' o o o ' o '* o o I I o o o o ' o '*' o ' ' o o o ' ' o o I o o o o o I I I o 'o ,o o o o o I o o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW
....... 00 \0 N 0 ....., VI 00 0 \0 QA filenaMe ParaMeter NaMe 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W246.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:07:03 through 20-5EP-2016 12:00:00 184. 000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I 0 >-f-H > H f-u a: x x w 0 x x x H ....I u x x ::i z 190 ........... * ........... *, ........... * .. ' ........ * ........... : ........... * ....... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... 00 ID w 0 H') Vl 00 0 ID QA filenar.-.e Parar.-.eter Nar.-.e 5tart/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W246.QAF;3 P5FWHM-GD148 (PEAK RE50LUTION GD-148) 17-MAR-2016 09:07:03 through 20-5EP-2016 12:00:00 5. 00000 through 100.000 . . . . . . 80 o ' o o o ' ' o o o ' o o o o o o o o o o I I o 0 0 0 o o o o I o o o o I o o o
0 I o o I o I o o o o I o o o o 0 I o o o I o o o o 0 I

o o 0 o o o ""'"" I D (!)_ z 0 H 1-=i ....I 0 Cf) w Ct'. . . . . . 60 I I o o o I I o o o o I I o o o I o o o o o o o o o o I 0 O O I I o o o I I o o o o 0 o 0 0 O I o o o o I I o o o 0 I e 0 0 o I o o o o I o o o o 0 I 0 o o o I o I x x x x x x *x . . . . . 40 ............................................................................ . . . . . . 20 .......... '*' .......... " ................................... ' ........... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
-00 \0 0 ....., Vo 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W246.QAF;3 ParaMeter NaMe P5ENERGY-GD148 (PEAK ENERGY G0-148) Start/End Dates 17-MAR-2016 09: 07:03 through ZO-SEP-2016 12:00:00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . ............................................................................ . . co ""'" "<"i I o. (!) )-(!) (t'. x x x x x x x w 3180 z . . . . . ....................... : .......... * ................ ' ....... : ............ * ...... . w :..::: a: w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.8]8246.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13:36:11 through 20-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' ' 1 * ' ' ',' ' ' ' ' ' * ' ' ' ',' o o o 1 o o o o ' ' ', o o ' ' o o o o ' o ',' o 1 1 o o o ' ' o o : o 1 o ' ' ' ' o o o o ,' o ' o o ' ' o . . . . . . . 06 ............... ' ........................................................... . . . . . 04 '02 ............................. -............................................. . 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W247.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 09: 07:07 through 20-SEP-2016 12:00:00 0.258845 through 0.274486 . . . . . . . 27 0 I 0 o 0 o 0 o o o I o o o o o 0 0 o 0 0 o o o o o o o o 0 0 0 0 0 o o o o o o 0 0 I o 0 o o o o o o 0 o I 0 o o o I o o o o 0 0 0 o o o o o o o I o 0 . . . ::::-, (.) c Q) *n (.) *n 4-4-UJ Q) Wl l(j I-.265 Q) > . . . . . . ............................................................................ . . x ([ x x x x x x . 26 . . . . . . ............................................................................ 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA,W]W247.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:07:07 through 20-SEP-2016 12:00: 00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ................... . I 0 (!) )-I-H > H I-u a: w* x x 0 H __J u x x ::i z x x x 190 ........... * ........... * ............ * ........... * ........ ' .. : ........... * ....... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -00 \0 00 0 H) !Ji 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.W]W247.QAF;3 ParaMeter NaMe PSFWHM-G0148 (PEAK RESOLUTION GD-148) Start/End Dates 17-MAR-2016 09: 07:07 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 5.00000 through 100.000 ..-! I Cl (!) z 0 H 1-=i _J 0 (!) lJJ O:'.. ::..:: a: lJJ 0.. 100 80 . . . . . . ............................................................................ . . . . . . 60 ............................................................................ . . . . . . x x x x x x x . . 40 .................................... ' ...................................... . . . . . . . 20 .......... '*' ...................... '* ........................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenarrie Pararrieter Narrie 5tart/End Dates Lower/Upper Lrrits: 3220 DKA100: [ENV_ALPHA.QA.W]W247.QAF;3 P5ENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09: 07:07 through 20-5EP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 ' ' o o o ' 0 o 0 0 I I 0 o o o o o o o o ' ' o o o 0 o o o o o ' o o o ' o o o o o 0 o o o o 0 o o o o o o o o o o I o o o o o o o o o o o o o o ' ' ' ro ""'" .,-I I D )-0::: x x x x x x x w 3180 z . . . . . ' o o o o ' o o o o I o o o 0 o o I o o o o o : o o o o o o o o o o ', o 0 o o o o o 0 o o o o o o o o o o o o o o o : o o o o 0 I o 0 o o o 0 o o o o o I o w :..: ([ w 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW -\0 0 0 0 ......, Vi 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B247.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 5-MAR-2016 18: 03:24 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 0, OOOOOOE+OO through 0.100000 I 08 ' ' ' ' ' ' ' 0 * * ','
0 0 ' ' 0 0 0 0 '*' o ' 0 0 ' 0 0 0 ' ' ', 0 0 ' ' 0 0 0 * ' 0 ',' 0 ' ' 0 ' 0 ' ' 0 0 : o 1 0 0 0 0 0 0 0 0 o ,' 0 0 0 0 0 0 0 . . . . . . . 06 ................................ ' .......................................... . . . . . 04 . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
....... '° 0 ....... 0 Hi Vl 00 0 '° QA filenari1e DKA100: [ENV_ALPHA.QA.W]W248.QAF;3 Parari1eter Nari1e AVRGEFF (Average Efficiency) Start/End Dates 17-MAR-2016 09:07:11 through 20-SEP-2016 12:00:00 Lower/Upper Lri1ts: 0.251863 through 0.267443 . . . . . . .265 ............................................................................ ::.-, 0 c Q) *r-1 0 *r-1 4-4-UJ . . . . . . . x x x . . . . . . . 26 o o o o o o o o o o o o o o o o o o o o o o 0 o o o o o o o o o I 0 0 0 o o o o o o o o o o o 0 o 0 0 o I I o o 0 o o o o o o o o o 0 0 I 0 0 o o o o o . . . . " . . x x x x . . . . . . . 255 o o o o o o o o o o o I o o o o o o o o o 0 I 0 o 0 o I o o o o o o o o O o o o o o o o o o o o I o O o o o o o o o o o o o I o o o o o o o o o O o o o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tiri1e UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Lower/Upper LMts: DKA100: NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:07:11 through 20-SEP-2016 12: 00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ........... .' ...... . I 0 (!) )-1-H > H 1-u a: w 0 H -I u ::i z x x x x x x 190 o o o o o o o o o o o'o o O o O o o o o o o 0o o o o o o o o O I I o' o o I o o o o o I o o'o O o 1 o o o I o o o : o o o o o I 0 o I o o 'o o o o o I I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/TiMe UP LOW ...... \0 0 w 0 H') Vl 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W248.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09:07:11 through 20-SEP-2016 12: 00: 00 5.00000 through 100.000 80 ........... * ........... *, ........... * ........... * ...... -..... : ............ * ....... . "<"i I D z 0 H* =:i ....I 0 en w O:'. ::...!: a: w 0.. . . . . . . 60 ............................................................................ . . . . . . x x x x x x x . . . 40 ............................................................... ' ........... . . . . . . . 20 .......... '*' ...................... '* .......... '*' ...................... *' ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -'° 0 .j::. 0 ...., Vl 00 0 '° QA filenaMe DKA100: [ENV_ALPHA.QA.W]W248.QAF;3 ParaMeter NaMe PSENERGY-GD148 (PEAK ENERGY GD-148) Start/End Dates 17-MAR-2016 09:07:11 through 20-SEP-2016 12:00: 00 Lower/Upper LMts: 3143.00 through 3223.00 UP 3220 3200 . . . . . . o ' o o o I o 0 o o o o o o 0 o 0 o o o o o I o o 0 o 0 o o 0 0 I 0 0 0 o o o o o o o o o o o o o o o o o o o o o o ' o o o I o 0 o o o o o o 0 o I I o ro .q ..-I I D (!) )-(!)* Q'. x x x x x x x w 3180 z . . . ' . . o O O o o I o o o o o o o o o o o o o o o o O o o o o O o o O O I o o o O o o o o O o o o o o o o o o o o o o o o o o o o o I o o o o o o o o 0 o I o o . . . . . . w ::..::: a: w 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe ....... \0 0 VI 0 ......, VI 00 0 \0 QA filenaMe DKA100: [ENV_ALPHA.QA.B]B248.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:36:18 through 20-5EP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' 'o o ' ' o o o ',' o o e ' ' e o o o '*' o o o ' ' o o o I I ', o o I I o o o o o o 'o' o I o o o o 1 1 o o : 1 o o o o o o o o o o 01 o o o o ' ' o . . . . . . . 06 I I o o o I I o 0 o I o o O o o o o e o o I o o o o I I o O o 1 I o O o O I I o o o o o o o o o I O O o I o o o o o o o o o I I I O O o o o o o O o o o . 04 . 02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Pararieter Narie Start/End Dates Lower/Upper Lr.-.ts: u c I}) *r-1 u *r-1 4-4-LU . 27 .265 . 26 x DKA100: [ENV_ALPHA.QA.W]W249.QAF;3 AYRGEFF (Average Efficiency) 17-MAR-201612:17:44 through 20-SEP-2016 12:00: 00 0.254827 through 0.270589 x x x x x x . 255 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ................. . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOl..1.J QA filenart'le Parart'leter Name Start/End Dates Lower/Upper Lrt'tts: DKA100: [ENV_ALPHA.QA.W]W249.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 12:17:44 through 20-SEP-2016 12: 00: 00 184. 000 through 204.000 200 ............................................... ' ........................... . . . . . . . I D (!) >-t-H > H t-u <I: w x x D H _J_ x u ::i z x x x x 190 ........... * ........... * ............ * .. ' ........ * ........... : ........... * ....... . 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tirt'le UP LOW -\0 0 00 0 ......, Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W249.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-201612:17:44 through 20-SEP-2016 12:00:00 5. 00000 through 100.000 80 ........... * ........... * ............ * ........... * ........... : ........... * ....... . ..-! I Cl 8 z 0 H 1-=i ...J 0 (f) l.LJ O:'. ::,.::: a: l.LJ* 0.. . . . . . . . 60 ' o o o o o o o o o o I o 0 o I 0 o o 0 o 0 o o o o o o o o o o o o o o 0 o o o o 0 I o o o o o o o o o o I o o o 0 0 0 o o o o o o o o o o o o o ' I 0 . . . . . . x x x x x x x . . . 40 ............... ' ........................................................... . . . . . . . 20 .......... '*' .......... " ............................................... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -\C) 0 \C) 0 ......, Vl 00 0 \C) QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W249.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 12:17:44 through 20-SEP-2016 12: 00: 00 3143.00 through 3223.00 . . . . . . 3200 ............................... ' ........................................... . . . . . ro ""'" ""'"" I D (!) )-(!) 0::: x x x x x x x LU 3180 z . . . . . . I o o o o 0 o o o o o I o o o o I o 0 o 0 0 I o 0 o 0 o o o o o o o o o o o o o o o 0 o o
o o o o o o o o o o o o o o I 0 ' 0 o o o o o o o o o o o o o I o I o o LU ::..::: <I: LU 0... 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenaMe DKA100: NaMe BACKRATE (Background Rate) Start/End Dates 4-MAR-2016 13:36:23 through 20-SEP-2016 12:00:00 Lower/Upper *LMts: 0, OOOOOOE+OO through 0.10DOOO UP I 08 o o o o o ' 0 0 o o 1,1 o o o I I o o o 0 I,' 0 0 0 I I 0 o o o o 'o 0 0 I I o 0 o o '* o o,o o I I 0 0 o I o o o : I I 0 0 0 o o o o o o o' o 0 0 0 I I o .06 . . . . . . o o o o o I o o o o I I o o O I I O O O O o o o o o o I o O O O I O o O I I o o o o I o o 0 O O I o o o o I o o o o I o 0 0 I I o o o o I o *' 0 o I I o .04 ................................................................................... . . . . 02 ............................................................................ . . . . . . 0 ........ _______ ........ .......... __ ................. __ ___,,....... __ __...,__ ......... __ .--......... ___ ........... ____ _........,_ ........ _.,..,,........,,.._ ___ 3-16 LOW 4-16 9-16 5-16 6-16 7-16 8-16 MeasureMent Date/TiMe 0 H) Vo 00 0 \0 QA filenar.-.e DKA100: [ENV_ALPHA.QA.W]W260.QAF;3 Parar.-.eter Nar.-.e AVRGEFF (Average Efficiency) Start/End Dates 17-MAR-2016 09:07:19 through 20-SEP-2016 12:00:00 Lower/Upper Lr.-.ts: 0.266448 through 0.271248 . 27 . . . . . . ............................................................................ . . . . u i::: 0) . 266 *r-1 u x *r-1 4-x 4-UJ x 0) "OJ) l(j x x x I-0) x > a: . 26 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W250.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:07:19 through 20-SEP-2016 12:00:00 184.000 through 204.000 200 ............................................................................ . . . . . . I 0 C) )-I-H > H x x I-u x x a: x w 0 x x H -I u ::i z 190 ........... * ........... * ............ * ........ ' .. * ........... : ........... * ....... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tir.-.e UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W250.QAF;3 PSFWHM-GD148 (PEAK*RESOLUTION GD-148) 09:07:19 through 20-SEP-2016 12:00:00 5.00000 through 100.000 80 . : ......... * .......... '* ............ * ........... * ........... : ........... * ....... . """' I Cl C) z D H ::J ....J o* (f) LLJ O:'. a: LLJ 0.. . . . . . . 60 I I o o o o 0 0 o o o 0 o o o I I e 0 o o o o o o o o I o o 0 I o o o o I o o o o o O o o o I I 0 0 0 0 0 I o o o I I o o o I o o o o I I 0 0 0 o I o o . . . . . . x x x x x x x 40 I I 0 0 o I I o o o I 1 O 0 o o o o o o' o o I 1o O O o o o o o o o o : o O O I O O e e O o o '., o o *, o o o o I o o : O I O O o I o o o o o 0 o o I o I O I O . . . . . . 20 .......................... ; .................................. ' ................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
...... \0 ...... .j:>.. 0 ....., Vi 00 0 \0 QA filenaMe ParaMe ter NaMe ::Hart/ End Dates Lower/Upper LMts: 3220 DKA100: [ ENV_ALPHA. QA. W] W250. QAF; 3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:07:19 through 20-SEP-2016 12:00: 00 3143. 00 through 3223.00 . . . . . . 3200 ............................................................................ . . . co ""'" ...t I D CJ )-CJ Cl:: x x x x x x x LLJ 3180 z. . . . . . ....................... : .......... * ........................ : ................... . LLJ ::..! a: LLJ 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ...... \0 ...... Vl 0 ....., Vl 00 C> \0 QA filenaMe DKA100: ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 5-MAR-2016 18:03:28 through 20-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 UP I 08 ' ' ' ' ' ' ' * ' o '*' ' ' ' ' ' ' ' ' ' ',' ' o ' ' 1 o ' ' 1 1 ',' ' 1 1 ' ' ' ' ' ' ',' ' 1 1 ' ' ' ' 1 ' ' : 1 1 o ' o 1 1 ' o ,' ' ' o 1 o .06 . . . . . . I o o O o o o o o o o I o o o o o o O o o o o o o o o o o e o o o o o o o o o o o o I o o O 0 0 I 0 o o 0 o 0 I 0 0 o e o o I 0 0 o o o I o o o o o o o .04 . . . . 02 ............................................................................ . . . . . . 0 .......... ........ 3-16 LOW 4-16 6-16 7-16 8-16 9-16 5-16 MeasureMent Date/TiMe -'° -0\ 0 ......, Vl 00 0 '° QA filenarrre Pararrre ter Narrre Start/End Dates Lower/Upper Lrrrts: DKA100: [ENV_ALPHA.QA.W]W251.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 09:07:23 through 20-SEP-2016 12:00:00 0.252760 through 0.268394 . . . . 265 ............................................................................ :>i 0 c I]) *r-1 0 *r-1 4-4-UJ I}) "OJ) ilj I}) > a: . . . . . . x x x x . . . . '26 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o o ' o o o o o o o o 0 I o o ' o o o o o o o o o o o o o o o o o o o o o o o o o o o ' o o . . . . . . x x x . . . . . . '255 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o ' o o o o o o I 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o 0 o 0 o 0 . . . . . . 3-16 4-16 5-16 6-16 '7-16 8-16 9-16 Measurerrrent Date/Tirrre UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W251.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:07:23 through 20-SEP-2016 12:00:00 184.000 through 204.000 200 ' ' ' o o ' o o o o ' o o o o o o 0 o 0
0 I o o o o o o 0 o o o o o o o o o o o o o o o o o 0 o o o o 0 0 o o 0 0 I 0 0 0 I I o

o o o o o o 0 I I o . . . . . . x x x x x x x . . . . . . .................................... ' ...................................... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W251.QAF;3 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Start/End Dates 17-MAR-2016 09:07:23 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 5. 00000 through 100. 000 ""'"" I 0 z 0 H 1-::J ...J 0 en w O:'. ::..::: a: w 0.. 100 80 ........... * ........... * ............ * ........... * ........... : ........... *, ...... . . . . . . . 60 .......................................................................... ' . 0 I o I o o 40 . x . . . x . x . x x . . . x . . . .............................. x* ... " .......... " ........... : ............ * ...... . 2 0 .......... " ........... " ............................................... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
..... l.O ..... l.O 0 ,...., Ul 00 0 l.O QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W251.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:07: 23 through 20-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . ' 3200 ............................................................................ . . ro v ..-i I D* (.!:) )-(.!:) et:: x x x x x x x w 3180 z . . . . ............................................................................ o I o I o o w <I: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,B]B251.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates-5-MAR-2016 18: 03:32 through 20-SEP-2016 12: 00: 00 Lower/Upper LMts: 0. OOOOOOE+OO through 0.100000 UP I 0 8 I I I O 1 ' o O o o O 0 I O o O I O 1 I 1 o o o' I O o o I O o o 1 ' ', o o 1 1 o o 1 o 1 o o 'o 1 1 o o O ' O O 1 : I I I o 1 1 1 o o o o ,' o o 1 o 1 1 o . 06 ........... * ........... * ............ * ........... * ...... *' .... : ........... * ....... . . . .04 .02 ............................................................................ . . . . . . 0 ........... ................... __ .,...___..,.............,...,__ __ ......... 3 -16 LOW 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ...... \0 N ...... QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: '27 DKA100: [ENV_ALPHA.QA.W]W252.QAF;3 AVRGEFF (Average Efficiency) 17-MAR-2016 12:17:49 through 20-SEP-2016 12: 00: 00 0.254300 through 0.270020 .265 .......... *:* .......... :* .......... *:* ......... *:* .......... : ..... .. *:* ...... . x x x x x x '26 I 255 * * * *
0 0 0 0 0 "*" 0 0 0 * ' 0 0 0 0 0 10 0 0 0 0 0 0 0 0 0 0 '* 0 0 0 0 0 0 0 0 0 0 010 0 0 0 0 0 0 0 0 0 0 I 0 0 0 0 0 0 0 0 0 0 0 10 0 0 0 0 0 0 0 3-16. 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW
-\0 N N 0 >-+., Vl 00 0 \0 QA f i lenar.-.e . Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W262.QAF;3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 12:17: 49 through 20-SEP-2016 12: 00:00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I CJ (!) )-x I-H > H I-u a: w x x x x CJ H ....I x x u ::J z 190 ' I 0 o o I o o I o 0'1 o I o I o o I o o o '1 o 0 0 o o o o o I I o' o o o o o 0 o o ' o o'o o o I I o o o o o o : o I o o o 0 o 0 0 o o 'o o o I o I I o 3-16 4-16 6-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenar.-.e Pararrieter Narrie Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA:QA.W]W252.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 12:17:49 through 20-SEP-2016 12:00:00 5.00000 through 100. 000 80 ........... * ........... * ............ * ........... * ........... : ........... *, ...... . ...... I Cl (:) z 0 H ::J ...J 0 ({) w Q'.. :::.::: a: w 0... 60 . . . . . . . ................ ' .......................................................... . . . . . . . x x x x x x x 40 .......... ' ' ............................................................... . . . . . . . 20 ............................................................ ' ........... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 3220 DKA100: [ENV_ALPHA.QA.W]W252.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 12:17:49 through 20-SEP-2016 12:00: 00 3143. 00 through 3223.00 . . . . . . 3200 ' o o o o 0 I o o o o o o o o o o o o o o I o o o o o o o o o 0 I 0 o o o o o o o o I ' o o ' o o o o o o 0 o o o o o o o o I 0 0 o o o o o o o o o o 0 . . . . . . ro ""'" """""" I D (!) >-(!) Ct: x x x x x x x LLJ 3180 z . . . . . . ............................................................................ . . . . . . LLJ :..::: a:* LLJ 0.. 3160 3-16* 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenafY'le ParafY'leter NafY'le Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.B]B252.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13: 36:35 through 20-5EP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 '08 ............................................................................ . . . . . . .06 . . . . . . o o o o o o o o o o I o o o o I O o O O O O o o o O O O o o I O I O o O O o o o o o o o o o o o o o o o o o o o o o o o o o I I 0 0 0 0 I 0
0 0 I I o '04 '02 ............................................................................ . . . . . . MeasurefY'lent Date/TifY'le UP LOW
-\0 N 0\ 0 ....., Vl 00 0 \0 QA filenal'le Paral'leter Nal'le Start/End Dates Lower/Upper Ll'lts: DKA100: AVRGEFF (Average Efficiency) 17-MAR-2016 09: 07:31 through 20-SEP-2016 12:00:00 0.250199 through 0.265675 . . . . . . . 265 ........... ' ................................................................ . . . . . . . ::>,. u .26 c . . . . . . ............................................................................ . . . . . . (I) *r-i u *r-i 4-4-LLJ x x (I) x "Of) ill x x x (I) > a: . 255 o ' o o o o o o o o o o o o o o I o ' o 0 0 o o o o o o o o o o o o o o I 0 0 0 o o 0 o o o o o o o o o o 0 0 o o o I o o o o o o o o 0 I 0 o o o o o o . . . . . . x 3-16 4-16 5-16 6-16 7-16 8-16 MeasureMent Date/TiMe UP LOW ...... \0 N -..J 0 ....., Vi 00 0 \0 QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ ENV_ALPHA. QA. W] W253. QAF; 3 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 09:07: 31 through 20-SEP-2016 12: 00:00 184.000 through 204.000 . . . . . 200 .......... *.* ........... * .......... " .......... *.* .......... : ............ * .... ' .. I 0 (!) )-1--x H > H 1--x x u a: x x w D x H ...J x u ::i z 190 0 0 o ' 0 0 o 0 0 o o'o o o o I I o o o 0 o 'o 0 o 0 o 0 o o 0 0 0 o' o o o o e o o o o o o'o o o o 0 o o 0 o o o : o o o o o o o o o o o 'o o o o o I o 0 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW -\0 N 00 0 ......, VI 00 0 '° QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: 100 DKA100: [ENV_ALPHA.QA.W]W253.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09:07:31 through 20-SEP-2016 12:00: 00 5.00000 through 100. 000 80 o o o o O o I o o o 0°1 o o o o 1 o o o o I', o o o I I o o o o I o' o o I o o o o o I o 0'1 O o I o o o I I o o ; 0 I o o o o I o o o o 0o o o o o I 0 0 I Cl C) z 0 H 1-:J ....J 0 01 w [t'.* <I: w Cl.. . . . . . . 60 ' .......................................................................... . . . . . . . x x 40 : : x : x : : x : ..... x ..................................................................... . . x . . . . . . . . . 20 .......... '*' .......... " ............................................... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW ....... \0 N \0 0 ....., Vl 00 0 \0 QA filenarrre Pararrreter Narrre Start/End Dates Lower/Upper Lrrrts: 3220 DKA100: [ENV_ALPHA. QA. W]W253. QAF; 3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:07:31 through 20-SEP-2016 12:00:00 3143. 00 through 3223.00 . . . . . . 3200 o o o o o o o o o o o 0 o o o 0 I o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o o o o o o o I o O o o o o O o O I O o . . . . . . co tj-I D (!:I )-(!:I 0:: x x x x x x x . . . . . . o 0 0 o 0 I o o o o o I o o o o I ' o 0 o o 0 o o o I I o o o o o o o o I I o o o o I o o o o o I o o o I o o o o o o o o o I o o o o o 0 o o o o I o o . . . . . ' w 3180 z w ::..::: a: . . . . . . x x x x . . . . . . '245 o o o o o o o o o o o o o o o o I o o 0 o o o 0
o 0 o I o 0 0 I 0 o o 0 ' o o o o o o o o 0 o o o o o o o o o o o o o o o o o o o o o o o o o o o o o . . . . . . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurefl"Jent Date/Tifl"Je UP LOW QA filenaMe ParaMeter Narrie 5tart/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W254.QAF;3 NLACTYTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09: 07:35 through 20-5EP-2016 12:00:00 184. 000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* .......... : ............ * ...... . I D )-I-H > H I-u <I x w x D H _J x x x u ::i z x 190 .......... *:* ......... *:* ..... x* ... *:* ......... *:* .......... : .......... *:* ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurement Date/Tirrie UP LOW QA filenaMe Pararrieter NaMe Start/End Dates Lower/Upper Lrrits: 100 DKA100: [ENV_ALPHA.QA.W]W254.QAF;3 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09:07:35 through 20-SEP-2016 12:00:00 5.00000 through 100. 000 80 . ' ......... * ............ * ............ * ........... * ........... : ' .......... *_ ....... . '<""I I Cl z 0 H" 1-::J _J 0 ({) w O:'. :::..: a: w 0.. 60 . . . . . . o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o o 0 I 0 o o 0 I o o o o I o o I o I 0 0 o o 0 0 o o o o I o o o I I ' o . . . . . . x x x x x x x . . . . 40 o I o o o I I o o o I o o o o I o I o o I I I o 0 o I I o o o o I o 0 o o o o o o o I o o o o o o o o o 0 I o 0 o I o o o o I o o o o o 0 0 o' o I o o . . . . . . 2*0 . * ............................................................................. ' .. 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 3220 DKA100: [ENV_ALPHA.QA.W]W254.QAF;3 PSENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:07:35 through 20-SEP-2016 12: 00:00 3143.00 through 3223. 00 . . . . . . 3200 o o o o o ' ' o o o o o o o o ' ' o o o o ' o o 0 o o o o o o ' o o o o ' 0 0 o o o I o o o o o I o 0 o o o o o o o o o o o I I 0 0 o o o o o o o o o o . . . . . ro v ""'"" I D >-. et:: x x x x x x x LL.I 3180 z . . . . . . ............................................................................ o o o I o I LL.I 0:: LL.I CL. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA f i lenarrie . Pararrieter Narrie Start/End Date8 Lower/Upper LMt8: DKA100: [ENV_ALPHA.QA.B]B254.QAF;2 BACKRATE (Background Rate) 4-MAR-2016 13: 36:44 through 20-SEP-2016 12:00:00 O.OOOOOOE+OO through 0.100000 I 08 ' 0 ' ' ' ' 0 ' ' ' ',' ' 0 ' 0 ' ' ' ' ' ',' ' ' ' ' 0 o o 0 1 ' 00 0 o 1 1 0 0 0 0 0 0 ',' 0 0 0 o 0 0 1 ' 0 0 : 0 0 0 0 0 0 0 0 0 0 0 ,' 0 0 o 0 ' ' 0 I]) llj O:'. 1J c :J 0 1-"0.IJ ::t. (..) llj co . . . . . . .06 o o o o o o o o o o I o o o o I o O o o o o o o o o I o o o o o o o o o o o o 0 o 0 0 o o o o o o o o o o o o 0 o I 0 o o o o o o o o o o o o o o I o 0 . . . '04 . . . . '02 ............................................................................ 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: . 26 (j c DKA100: [ENV_ALPHA.QA.W]W255.QAF;4 AVRGEFF (Average Efficiency) 17-MAR-2016 09:07:39 through 20-SEP-2016 12:00: 00 0.245940 through 0.261150 x ID . 255 *r-1 ........... : ...... x .... : ............ : ........... : ........... ........... : ....... . (j *r-1 4-x 4-UJ IJ.) x x "0.0 l'lj s... ID > x CI .25 x 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW
...... \0 w -..J 0 ....., Vl 00 0 \0 QA filenafY'le ParafY'le ter NafY'le Start/End Dates Lower/Upper LfY'lts: DKA100: [ENV_ALPHA.QA.W]W255.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY 17-MAR-2016 09:07:39 through 20-SEP-2016 12:00:00 184. 000 through 204.000 200 o o I I I 0 I I o 0 o 0 o I I I I o o o I I o o o o I I o I I o o o o o I I o o o 0 I I I I o o I o I o I o o o I I I o o o o o o o I I I Io I I I o o . . . . . . I Cl )-I-H > H f-u x x a: x w x Cl H x x _J" u =i z x 190 . . . . . . o I 0
o 0 o o o o o I o o o o I o I o o I o o o o o I o o O o I o o o O o o o o o o I o o o o o o o o o o o o o o o I o o I o o I I o o o I o o I I I 3-16-4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA.W]W255.QAF;4 ParaMeter NaMe PSFWHM-GD148 (PEAK RESOLUTION GD-148) Dates 17-MAR-2016 09:07: 39 through 20-SEP-2016 12:00:00 Lower/Upper LMts: 5. 00000 through 100.000 ...i I D (!) z D H 1-::i ....I D (j') Ll.J O:'. a:. Ll.J 0.. 100 80 ........... * ........... * ............ * ........... * ........... : ........... * ....... . 60 . . . . . . ........................................................... ' ............... . . . . . . . x x x x x 40 ........... : ........... :. ..... x ..... : ........... : ........... ; ...... x .... :. ...... . 20 .......... '*' .......... " ................................... ' ........... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.e ter Nar.-.e Start/End Dates Lower/Upper LMts: 3220 : .DKA100: [ENV_ALPHA.QA.W]W255.QAF;4 : PSENERGY-GD148 (PEAK ENERGY GD-148) : 17-MAR-2016 09:07:39 through 20-SEP-2016 12:00:00 3143.00 through 3223.00 . . . . . . 3200 0 0 0 0 o I I o o o I o o o o I I o o o o 0 I 0 0 0 I I 0 0 0 I I o o o 0 o o 0 0 o 0 o 0 0 o 0 0 0 0 o I 0 o 0 o o 0 0 0 o I I o 0 o o 0 o 0 o o I o o . . . . . . CO* """ "<"i I D )-ct:: x x x x x x *X LU 3180 z . . . . . . I o o o o I o o o o 0 I o 0 0 o I o o o o o I o 0 o o o o I I I I 0 0 o I 0 0 0 o 0 0

0 o o I 0 o 0

I I o 0 o I o o 0 o I I 0 0 0 o 0 o 0 o o o o o . . . . . . LU <I: LU 0.. 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe DKA100: [ENV_ALPHA.QA,B]B255.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 5-MAR-2016 18:03:39 through 20-SEP-2016 12:00:00 Lower/Upper LMts: O,OOOOOOE+OO through 0.100000 UP I 08 ' 0 0 o 0 ' 1 0 0 0 ',' 0 0 0 0 o ' o 0 0 0 ,' 0 0 0 0 1 o 0 0 0 0 ', 0 0 0 0 0 0 0 0 0 0 ',' 0 0 1 0 0 0 0 0 0 0 : 1 1 0 0 0 0 0 0 0 0 o 01 0 0 0 0 0 0 0 .06 . . . . . . ............................................................................ . . . . 04 . . . . 02 ............................................................................ . . . . . . 0 ......... "'-......... ......... ..........,.,.__ .......... 3-16 LOW 4-16 7-16 9-16 8-16 5-16 6-16 MeasureMent Date/TiMe 0 ......, Ul 00 0 ID QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [ENV_ALPHA.QA.W]W256.QAF;4 AVRGEFF (Average Efficiency) 17-MAR-2016 09:07:43 through 20-SEP-2016 12:00:00 0.252440 through 0.2£8050 . . . . . . '265 o ' o o o o I 0 0 o I I o o o o I o o o o I I o O O O I O O o o O o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o I o o o o o o o (.) c Q) *ri (.) *ri 4-4-LL.I . . . . . . '26 . . . . . . .......... *.* ..... x .... : .......... * ........... *.* .......... : ........... ,' ...... . x x x x x x

255 . ' . . . . ............................................................................ . . . . . . 3-16 4-16 5-:-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenarrie Pararrie ter NaMe Start/End Dates Lower/Upper LMts: DKA100: [ENV_ALPHA.QA.W]W256.QAF;4 NLACTVTY-GD148 (NUCLIDE ACTIVITY GD-148) 17-MAR-2016 09:07:43 through 20-SEP-2016 12: 00: 00 184.000 through 204.000 200 .......... *.* ........... * .......... * ........... *.* ....... " .. : ............ * ...... . I 0 (!) )-I-H > H x I-u x a: x x w 0 .. x H ....I x u ::i x z 190 . . . . . . ' o o o o ' o o o o ' 0 o 0 o 0 o o o o o o o o o o o I 0 o o o o o o o o o o 0 o 0 I o o o o o o o o o o I o o o o I o o o o o o o 0 o I 0 o o o o I o 3-16 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: 100 DKA100: [ENV_ALPHA.QA.W]W256.QAF;4 PSFWHM-GD148 (PEAK RESOLUTION GD-148) 17-MAR-2016 09:07:43 through 20-SEP-2016 12: 00:00 5.00000 through 100. 000 80 ........... * ........... * ............ * ........... * ........... : ........... * ....... . .-I I D C) z 0 H ::i _J. 0 en w 0.:: :::.,:: a: w n. . . . . . . 60 0 I o o o o o o o o o o o o o o o o o o o o o o o o o o o o o o O o o o o o o o o o o o o 0 0 I I 0 0 o 0 I o o o o o o o o o o 0 o o 0 I 0 0 0 0 I I o . ' . . . . x x x x x x x . . . . 40 I o o o ' 0 o o o o o o o o o o o o o o o I 0

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o o o o o o o o o o 0 I o o o o 0 I 0 0 o I I o o 0 o 0 o o I o o o o o o o o o o o o I o . . . . . . 20 ....................... " ............................................... " ...... . 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenart1e Parart1e ter Nart1e Start/End Dates Lower/Upper Lrt1ts: 3220 DKA100: [ENV_ALPHA.QA.W]W256.QAF;4 P5ENERGY-GD148 (PEAK ENERGY GD-148) 17-MAR-2016 09:07:43 through 20-SEP-2016 12:00:00 3143. 00 through 3223. 00 . . . . . . 3200 ............................................................................ . . . co "<T ..-I I D )-et:: X* x x x x x x w 3180 z* . . . . . ............................................................................. . . . . . . w ::..:: a: w CL 3160 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurert1ent Date/Tirt1e UP LOl.i.I QA filenaMe DKA100: [ENV_ALPHA.QA.B]B256.QAF;2 ParaMeter NaMe BACKRATE (Background Rate) Start/End Dates 5-MAR-2016 18:03:43 through 20-SEP-2016 12: 00: 00 Lower/Upper LMts: O.OOOOOOE+OO through 0.100000 I 08 ' ' ' ' * ' ' *

o ',' ' o o ' ' o o o o ',' ' o o ' ' o o o o ' 0* o o ' 1 o o o ' ' o ',' ' ' ' ' ' ' ' ' ' ' : ' ' ' ' ' ' ' ' ',' ' ' ' ' ' . . . . . . '06 ' ' * ' ' ' * ' * ' ' ' ' ' * ' ' *

o ' ' ' ' * ' ' ' ' ' ' ' ' ' ' ' ' ' ' * * ' ' o o ' * ' ' ' ' * ' ' * ' ' ' ' ' ' * ' ' ' ' ' ' *' ' I ' o . . '04 . . '02 ............................................................................. 0 3-16 . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW Page 1946 of 5809 RAD Standards Traceability
.... j Page 1947 of 5809 ANALYTICS CERTIFICATE OF. CALIBRATION Standard Radionuclide Source 61762-278 Ac-227 s mL Liquid in Flame sealed Vial 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318
U.S.A. Phone (404) 352-8677 Fax (404) 352-2837 This standard radionuclide source was prepared gravimetrically from a calibrated master solution. The master solution was calibrated using a germanium gamma spectrometer system. Radionuclide purity p.nd calibration were checked by alpha spectroscopy. The nuclear decay rate and assay date for this source are given below. Analytics maintains traceability to the National Institute of standards and Technology through participation in a Measurements Assurance Program as described in USNRC Reg. Guide 4.15, Revision 1, February 1979. ISOTOPE: ACTIVITY ( dps) : HALF-LIFE: Ac-227 2.085 ES 21. 77 years CALIBRATION DATE: June 8, 2001 12:00 EST TOTAL UNCERTAINTY*: 5.0% SYSTEMATIC: 2.0% RANDOM: 3. 0% *99% Confidence Level Impurities:

y-impurities (other than: decay products) <0 .1% a-impurities <0.3% 5.3136 grams 2M HN03 solution, carrier free. p 0 NUMBER 2533RD, Item 2 SOURCE PREPARED BY: Manager Q A APPROVED:
!4 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Actinium-22 7 Parent Code: 0387 Prepared By: Angela Johnson Prepared By: Angela Johnson Prep Date: 07/17/2001 Carrier Cone: 2MHN03 Verification Date: 08/02/2011 Reference Date: 06/08/2001 Expiration Date: 07/31/2012 Ampoule Mass (g): 5.3136 g Primary Code: 0387-A Uncertainty: +/-5 % Dilution(mL): lOOmL LogBookNo: RC S 034-049a Mass of Parent(g): 4.7794 g Density(g/mL): 1.0370 Balance ID: Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) * (Parm Activity (dps)) *(conversion dpm to dps) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (dps)) *(conversion dpm to dps) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (4.7794 g) * (208500 dps) * (60 dpm/dps) I (5.3136 g
100 mL) = 112523.1369 dpm/mL (4.7794 g) * (208500 dps) * (60 dpm/dps) I ( 1.0370 g/mL)/ (5.3136 g

100 mL) = 108511.1539 dpm/g Prep Date Preparer 07/17/2001 Lonnie Morris 07/17/2001 Lonnie Morris 05/12/2011 Ashley Drochter 08/01/2011 Ashley Drochter GEL Laboratories LLC Version 1.0 9/18/2000 Page 1948of5809 Secondary Standards Mass Dilution Code Primary (mL) .4684 1000 0387-B-102 .4684 1000 0387-B-202 .4605 1000 0387-B-302 .4603 1000 0387-B-402 Cone Verification Expiration dpm/mL Date Date 50.8266 07/22/2010 07/22/2011 dpm/mL 50.827 07/11/2004 07/11/2005 dpm/mL 49.9694 05/12/2011 05/12/2012 dpm/mL 49.9477 05/31/2016 05/31/2017 dpm/mL Verification for Ac-227 Standard 0387-8-402 v1.2 Analyst TC1 Tracer Information Verification Prep Date 5/31/2016 Isotope Th-230 Serial Number 1242-H Amount of Std. (ml) 0.5 Exoiration Date 2/11/2017 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dom/mll Amount of Std. (ml) Standard Prep Date Ac-227 0387-B-402 21.7730 y 6/8/2001 49.9477 0.5 8/1/2011 Verification Rules Std# 1 2 3 Count Date 5/31/2016 5/31/2016 5/31/2016 Mean Value= Stdev= pCi dpm/ml Certificate Value* = 6.9829 7.280 32.32 Two sigma= 0.3606 7.530 33.43 10% of Mean= 0.7330 7.180 31.88 Rule A (Pass/Fail) Pass % Recovery 104.97% 7.330 32.545 Rule B (Pass/Fail) Pass 0.180277564 0.800432383 Expiration Date 5/31/2017 Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value.

Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Ac-227 standard 0387-8-402 using 0.5 ml for each source. Each standard was combined with 0.5*ml of Th-230 standard 1242-H and was diluted in a 50 ml plastic centrifuge tube containing 1 O ml of BM HN03. The verification sources were then passed through an AG 1 x8 column and eluted with 20ml 9M HCI. The elution was cooked dry, wet ashed and then dissolved in 5ml 2M HCI. The 2M HCI solution was transferred to a disposable centrifuge tube using deionized water and was analyzed following SOP Gl-RAD-A-038. 100 micrograms of neodynium and five ml of 48% HF was added to precipitate neodymium (and Actinium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Ac-227 were calculated by comparison to Th 230 certified values. dpm/ml 31.0043 1.6009 3.2545 *pass 104.97% Pass -r-t. r I 11 ANALYTICS CERTIFICATE OF CALIBRATION Standard Radionuclide Source 65338-278 Am-241 5 mL Liquid in Flame Sealed Vial 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318

U.S.A. Phone (404) 352-8677 Fax (404) 352-2837 This standard radionuclide source was prepared g:tavimetrically from a calibrated master solution.

The master solution was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and assay date for this source are given below. ANALYTICS maintains traceability to the National Inst;i.tute of Standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision 1. ISOTOPE: ACTIVITY {dps) : HALF-LIFE: CALIBRATION DATE: TOTAL UNCERTAINTY*: .SYSTEMATIC: RANDOM: *99% confidence 5.10649 grams lM HCl solution. Impurities: y-impurities <0.1% a-impurities <0.1% P 0 NUMBER 3213 RD, *Item 1 Arn-241 3.920 E4 4.322 E2 years January 15, 2003 12:00 EST 3.2% 2.2% 1. 0% \ SOURCE PREPARED BY: a...e..i/.o!..._ M. Taskaeva, Radiochemist QA APPROVED: I -H;-o5 Standard Traceability Log Rad A Solution Material Info Source Material Info' Isotope: Americium-241 Parent Code: 0533 Prepared By: Angela Johnson Prepared By: Angela Johnson Prep Date: 02/05/2003 Carrier Cone: lMHCL Verification Date: 01/22/2016 Reference Date: 01/15/2003 Expiration Date: 01/22/2017 Ampoule Mass (g): 5.10649 g Primary Code: 0533-A Uncertainty: +/-1.24 % Dilution( mL): lOOmL LogBookNo: RCS 035 048 Mass of Parent(g): 4.8225 g Density(g/mL): 1.0139 Balance ID: Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (dps)) *(conversion dpm to dps) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (dps)) *(conversion dpm to dps) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (4.8225 g) * (39200 dps) * (60 dprn/dps) I (5.10649 g

100 mL) = 22211.9695 dprn/mL (4.8225 g) * (39200 dps) * (60 dprn/dps) I ( 1.0139 g/mL)/ (5.10649 g

100 mL) = 21907.2185 dprn/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone Verification Expiration Primary (mL) dpm/mL Date Date 02/20/2003 Angela 1.0151 100 0533-B 222.38 03/01/2006 03/01/2007 Johnson dpm/mL 01/16/2015 Christina .005081 500 0533-BB .22263 01/14/2016 01/14/2017 Kimball dpm/mL 02/20/2003 Angela .6819 250 0533-C 59.754 02/20/2004 02/20/2005 Johnson dpm/mL 05/04/2015 Tim 1.02 500 0533-CC 44.6907 04/21/2016 04/21/2017 Chandler dpm/mL 05/07/2003 Tim .1245 100 0533-D 27.2745 05/03/2004 05/03/2005 Chandler dpm/mL 01/22/2016 Christina .103 500 0533-DD 4.51289 01/22/2016 01/22/2017 Kimball dpm/mL 09/10/2004 Amanda .6933 250 0533-E 60.753 09/10/2005 0911012006 Fehr dpm/mL 12117/2004 *Brenda .0093 100 0533-F 2.0374 12/20/2004 12/20/2005 Burke dpm/mL Page 1951of5809 12/21/2004 Brenda .009273 100 0533-G 2.0315 12/07/2005 12/07/2006 Burke dpm/mL 04/28/2005 Brenda .1347 100 0533-H 29.4598 04/27/2006 04/27/2007 Burke dpm/mL 10/19/2005 Mary Aders .6948 . 250 0533-1 60.7831 10/18/2006 10/18/2007 dpm/mL 05/08/2006 Julie Strock .0711 100 0533-J 15.576 05/10/2008 05/10/2009 dpm/mL 05/11/2006 Brenda .00092601 100 0533-K .20286 08/02/2007 07/28/2007 Burke dpm/mL 11/15/2006 Tara Sides .132 1000 0533-L 2.88586 09/15/2015 09/15/2016 dpm/mL 06/12/2007 Julie Strock .000979 100 0533-M .21448 05/20/2009 05/20/2010 dpm/mL 08/03/2007 Daniel Roy .7042 250 0533-N 61.7083 08/02/2008 08/02/2009 dpm/ml 09/25/2008 Daniel Roy 1.4561 500 0533-0 63.7982 09/07/2010 09/07/2011 dpm/ml 09/29/2008 Tara Sides .1004 100 0533-P 21.9948 09/07/2010 09/07/2011 dpm/mL 06/03/2009 Julie Strock .0009751 100 0533-Q .2136 06/01/2010 06/01/2011 dpm/mL 11/08/2010 Ashley 1.4675 500 0533-R 64.2977 11/08/2010 11/08/2011. Drochter dpm/mL 11/09/2010 Ashley .7295 500 0533-S 31.9626 10/31/2011 10/31/2012 Drochter dpm/mL 01/03/2011 Christina .097 100 0533-T 21.25 01/03/2011 01/03/2012 Kimball dpm/mL 01/05/2011 Christina .1009 100 0533-U 22.10438 12/18/2013 12/18/2014 Kimball dpm/mL 05/23/2011 Christina .001008999 100 0533-V .2210438 05/11/2012 05/11/2013 Kimball dpm/mL 05/11/2012 Christina .001016 100 0533-W .222676 05/01/2014 05/01/2015 Kimball dpm/mL 06/13/2012 Ashley .728 500 0533-X 31.8969 06/02/2014 06/02/2015 Drochter dpm/mL 01/23/2013 Salina 2 500 1641 .1498555 12119/2013 12/01/2038 Pizarro dpm/mL 07/16/2013 Julie Strock 1 500 1641-A .07492775 07/16/2038 07/16/2039 dpm/mL 03/17/2014 Christina .1013 100 0533-Y 22.19201 03/14/2016 03/14/2017 Kimball dpm/mL 05/05/2014 Christina .00101595 100 0533-Z .222567 05/05/2014 05/05/2015 Kimball dpm/mL Page 1952 of 5809 GEL Laboratories LLC Version 1.0 9/18/2000 Page 1953of5809 Verification for Am-241 Standard 0533-CC v1.2 Analyst TC1 Tracer Information Verification Prep Date 4/21/2016 Isotope Am-243 Serial Number 1752-B Amount of Std. (ml) 0.5 Expiration Date 11/23/2016 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife

Reference Date Ref. Act. (dpm/ml) Amount of Std. (ml) Standard Prep Date Am-241 0533-CC -432.6000 y 1/15/2003 44.6907 0.5 5/4/2015 Verification Rules Std# 1 2 3 Count Date 4/21/2016 4/21/2016 4/21/2016 Mean Value= Stdev = pCi dpm/mL Certificate Value"' = 9.8538 9.430 41.87 Two sigma= 0.4762 9.520 42.27 10 % of Mean= 0.9610 9.880 43.87 Rule A (Pass/Fail) Pass %.Recovery 97.53% 9.610 42.668 Rule B (Pass/Fail) Pass 0.238117618 1.057242224 Expiration Date 4/21/2017 Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value. "' Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Am-241 standard 0533-CC using 0.5 ml for each source. Each standard was combined with 0.5 ml of Am-243 standard 1752-B and was diluted in a 50 ml plastic centrifuge tube containing 10 ml of 1 M HCI. 100 micrograms of neodymium carrier and five ml of 48% HF was added to precipitate neodymium (and Americium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Am-241 were calculated by comparison to Am-243 certified values. dpm/ml 43.7509 2.1145 4.2668 Pass 97.53% Pass
. 1!f* Eckert & Ziegler Analytics CERTIFICATE OF CALIBRATl.QN Standard Reference Source 101294 Am-243 6 mL Liquid in Flame Sealed Vial Customer: GEL Laboratories, LLC P.O. No.: GEL1511998, Item l Product Code: 8243 1380 Seaboard Industrial Blvd. Atlanta, Georgia 3031 B Tel 404*352*8677 Fax 404*352*2837 www.ezag.com This standard radionuclide source was prepared gravimetrically from a master solution calibrated by Eckert & Ziegler Analytics, using a germanium gamma spectrometer system. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry, liquid scintillation counting, and/or alpha spectrometry, as applicable. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 2, July 2007, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST." Uncertainty* , % Half-Life, Activity Type Reference Date Isotope Days (Bq) UA UB u (12:00 PM EST) Am-243 2.692E+06 3.809E+04 0.5 1.8 3.7 09/01/2015 *Uncertainty: U*-Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results." Comments: Impurities: y-impurities (other than decay products)<O. l %. 5.10528 g lM HCI solution, carrier free. Source Prepared by: _____ Z. Dimitrova, Radiochemist QC Approved: Single Isotope Certificate Rev 7, 3 November 2014 Page 1955of5809 Corporate Office G L.-le 'i1-CY 15'" Page 1 of 1 Laboratory Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Americium-243 Parent Code: 1752 Prepared By: Tim Chandler Prepared By: Gregory Ramsay Prep Date: 11/23/2015 Carrier Cone: lMHCl Verification Date: 05/26/2016 Reference Date: 09/01/2015 Expiration Date: 05/26/2017 Ampoule Mass (g): 5.10528 g Primary Code: 1752-A Uncertainty: +/-1.85 1 Dilution(mL): lOOmL LogBookNo: GL-CED-297-045 Mass of Parent(g): 5.0826 g Density(g/mL): 1.0282 Balance ID: C31514 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (5.0826 g) * (38090 Bq) * (60 dpm/Bq) I (5.10528 g
100 mL) = 22752.4720 dprn/mL (5.0826 g) * (38090 Bq) * (60 dpm/Bq) I ( 1.0282 g/mL)/ (5.10528 g

100 mL) = 22128.4498 dprn/g Prep Date Preparer 11/23/2015 Tim Chandler 05/26/2016 Tim Chandler GEL Laboratories LLC Version 1.0 9/18/2000 Page 1956 of 5809 Mass Primary 1.0432 1.072 Secondary Standards Dilution Code Cone Verification Expiration (mL) dpm/mL Date Date 500 1752-B 46.1688 11/24/2015 11123/2016 dprn/mL 500 1752-C 47.4434 05/26/2016 05/26/2017 dprn/mL Verification for Am ... 243 Standard 1752.,.C V1.2 Analyst TC1 Tracer Information Verification Prep Date 5/26/2016. Isotope Am*241 Serial Number 0533,CC Amount of Std. (mL) 0.5 Exolratlon Date 4/21/2017 Standard Information Activity Standard pCt 11).6847 0.4000 1.0900 Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dpm/mL) Amount of Std. lmL) Standard Prep Pate Am-243 Std# 1752-C 1 7.3700E+03 Y. 2 9/1/2015 3 47.4434 0.5 5/26/2016 Verification Rules Count Date 5/27/2016 5/26/2016 5/26/2016 Mean Value= Stdev= pCi 11.100 10.900 10.700 ---10;900 0.2 di::>m/mL 49.28 48.40 47.51 48;396 0.888 Certificate Value* a Two sigma ... 10%ofMean:;; Rule A (Paas/rail) % Recovery Rule B (Pase/Fall) Expiration Date Pass 102.01% Pass 5/26/2017 Rule A= The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of. the certificate value.

Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Am-243 standard 1752*C using 0.5 mL for each aouroe. Each standard was combined with 0.5 mL of Am-241 standard 053S*CC and was diluted In a 50 mL plastlc centrifuge tube containing 15 mL of 1 M HCI. 100 micrograms of neodymium carrier and five mL of 48°/o HF was added to precipitate neodymium (and Americium) fluoride. After 30 minutes, each sample was 1lltered followlng routlnfil procedures for alpha spectroscopy source preparation. Each source was counted .using routine alpha spec procedures. DPM vah . .1es for Am-243 were calculated by comparison to Am-241 certified values. df}m/mL 41.4401 1.7760 4.13396 Pass. Pass CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION Radionuclide Half Life; Catalog No.: .Ani.-243 7380 +/- 40 years 7243 445-96-2 Customer: P.O.No.: GENERAL ENGINEE!UNG LABS 9290-RAD Reference Date: January 1 1994 12:00 PST. Source No.: Contained Radioactivity: 101.2 µ.Ci Contained Radioactivity: (Am-243) 3750 kBq Description of Solution a. Mass of solution: b. Chemical fonn: c. Carrier content: S.3739 g (in a 5 ml Flame Sealed Am(N03)3 in 2N HN03 None added d. Density: 1.0651 g/ml @ 20°c. Radioimpurities Radioactive Daughters Radionuclide Concentration Method of Calibration None detected Np-239 (beta active) in equilibrium (Am-243) 18.84 µ.Ci/g Weighed aliquots of the solution were assayed using gamma spectrometxy for Np-239: Energy peak.(s) intergrated UDder:

228, 278 keV. Branching ratio(s) used: 0.108, 0.1420 gamma rays per decay. Uncertainty of Measurement a. Systematic uncertainty in inst1UIDent calibration: b. RandOm uncertainty in assay: c. Random uncenainty in weigbing(s): d. Total uncertainty at the 99% confidence level: +/-3.0% +/-0.4% +/-0.0% +/-3.0% NIST Traceability This calibration is implicitly traceable to the National Institute of Standards and Technology. Leak Test(s) See reverse side for Leak Test(s) applied to this source. Notes 1958of5809 1. Nuclear data were taken from "Table of lladioactive Isotopes*, edited by Vii-ginia S. Shirley, 1986. 2. IPL participali:s in an NIST measurement assurance program i0 establish and maintain implicit ttaceability for a numb.:r of nuclides, balled on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15). ISOT9PEPRODUCTSLABORATORIF.S 1800 North Keystone Street Burbank, California 91504 818 843 -7000 QUALITY CONTROL J J 121 "I ll-s-M-? 2. """I* 11.1 etl.J THE LEAK TEST(S) INDICATED BY THE CHECKED BOX(ES) WAS(WERE) APPLIED TO DETERMINE THE INTEGRllY OF THE SOURCE DESCRIBED ON THE FRONT SIDE 1. STANDARD WIPE TEST The source is wiped over its entire surface with a moistened filter paper disk. After drying, the disk is checked for activity using a windowless proportional counter or end-window G.M. tu.be. Activity levels exceeding O.OOl 11Ci beta-gamma or 0.0001 µCi alpha are cause for rejection of the source. 0 2. SOAK TEST The somce is immersed in distilled water and maintained at 50 :1: 10° C for a minimum of four hours. After removal of the source, the liquid is a) checked for activity using a liquid scintillation counter, orb) evaporated in a planchet and the residue is checked for activity using a windowless proportional counter or end-window GM. tube. Activity levels exceeding 0 .001 µCi beta-gamma or 0.0001 µCi alpha are cause for rejection of the somce. 0 3. SOAK TEST*-BERYLLIUM WINDOW . The source is immersed in distilled water and maintained at 50 :!: l 0° C for 20 minutes. The entire surface of the source is then wiped with a moistened cotton swab or filter paper disk. After dl)'ing, the swab or disk is checked for activity using a windowless proportional counter or end-window G.M tube. Activity levels exceeding 0.001 µCi beta-gamma or 0.0001 µCi alpha are cause for rejection of the source.

0 4. GAS SOURCE TEST (Radioactive Gas) The source is placed in a vacuum desiccator and maintained at a pressure of less than l mm Hg for not less than 12 hours. The activity is checked by introducing air into the desiccator and monitoring the air with an end-window G.M. tu.be. Activity levels exceeding 1000 cpm are cause for rejection of the source. 5. OTHER LEAK TEST The ampoule is kept in an inverted position on a filter paper disk for a minimum of 16 hours. The filter paper disk is then checked for activity usfug a windowless proportional counter or end.window G.}4. tube. Activity levels exceeding 0.001 µ.Ci beta-gllUllllll. or 0.0001 µCi alpha are cause for rejection of the source. 0 6. LEAK TEST NOT APPLICABLE

The active area of this source is uncovered or is protected by a very thin coating. Although the deposit is adherent, it is not Page 1959 of 5809 designed or certified to pass a standard leak test The inactive portions of the source have been checked using the standard wipe test. Levels of removable activity did not 0.001 µCi beta-gamma or Q.0001 µCi alpha at the time of shipment. -. .. -I , I
!4 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Americiuin-243 Parent Code: 445-96-2 Prepared By: Angela Johnson Prepared By: Genie Bost Prep Date: 01/05/1994 Carrier Cone: 2MHN03 Verification Date: 08/01/2016 Reference Date: 01/01/1994 Expiration Date: 08/01/2017 Ampoule Mass (g): 5.3739 g Primary Code: 445-96-2-A Uncertainty: +/-3 % Dilution(mL): lOOmL LogBookNo: RCS 005 032 Mass of Parent(g): 5.3419 g Density(g/mL): 1.0785 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLjdpm/g (Mass ofparent(g)) *(Parm Activity (uCi/g)) *(conversion dpm to uCi) I (Dilution Vol)= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (uCi/g)) *(conversion dpm to uCi) I Density (g/mL)/ (Dilution Vol)= Parent Activity (dpm/g) (5.3419 g) * (18.8317609 uCi/g) * (2220000 dpm/uCi) I (100 mL) = 2233261.9148 dpm/mL (5.3419 g) * (18.8317609 uCi/g) * (2220000 dpm/uCi) I ( 1.0785 g/mL) I (100 mL) = 2070711.0942 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone Verification Expiration Primary (mL) dpm/mL Date Date 01/05/1994 Genie Bost .0058 100 445-96-2-B 120.l 01/05/1995 0110511996 dpm/ml 09/10/2004 Amanda .0325 1000 445-96-2-BB 67.328 09/10/2005 09/10/2006 Fehr dpm/mL 06/29/2011 Christina .0010549 500 445-96-2-BBB 4.37074 06/29/2011 06/29/2012 Kimball dpm/mL 01/05/1994 Genie Bost .0025 100 445-96-2-C 51.77 01/05/1995 01/05/1996 dpm/ml 05/27/2005 Brenda .000246 100 445-96-2-CC 5.10613 05/31/2005 05/31/2006 Burke dpm/mL 05/07/2012 Christina .001059 500 445-96-2-CCC 4.38535 05/01/2013 05/01/2014 Kimball dpm/mL 03/25/1994 Genie Bost .0064 100 445-96-2-D 132.53 01/05/1995 01/05/1996 dpm/ml 08/16/2005 Brenda .001224 500 445-96-2-DD 5.07144 08/18/2007 08118/2008 Burke dpm/mL Page 1960 of 5809 06/13/2012 Christina .00001105 100 445-96-2-DDD .2288308 07/29/2016 07/29/2017 Kimball dpm/mL 08/04/1994 Genie Bost .0094 100 445-96-2-E 194.65 01/05/1995 01/05/1996 dpm/ml 10/13/2005 Brenda .0017 5(')0 445-96-2-EE 7.0435 11/15/2005 11/15/2006 Burke dpm/mL 11/15/2012 Ashley 2.0992 1000 445-96-2-EEE 4346.8367 11/21/2014 11/21/2015 Drochter dpm/mL 03/21/2015 Christina .00106557 500 445-96-2-GGG 4.41297 03/17/2016 03/17/2017 Kimball dpm/mL 07/20/2015 Christina .00631239 500 445-96-2-HHH 26.14226 07/18/2016 07/18/2017 Kimball dpm/mL 08/04/1994 Genie Bost .0046 100 445-96-2-F 95.25 01/05/1995 01/05/1996 dpm/ml 10/14/2005 Mary Aders .0141 500 445-96-2-FF 58.4196 10/14/2005 10/14/2006 dpm/mL 09/01/1994 Genie Bost .0031 100 445-96-2-G 64.19 01/05/1995 01/05/1996 dpm/ml 05/10/2006 Mary Aders 2.0753 1000 445-96-2-GG 4299.227 09/30/2008 09/30/2009 dpm/mL 10/17/1994 Genie Bost .0969 100 445-96-2-H 2006.52 01/05/1995 01/05/1996 dpm/ml 06/07/2006 Mary Aders .0365 1000 445-96-2-HH 75.614 06/19/2006 06/19/2007 dpm/mL 02/06/1995 Genie Bost .0043 100 445-96-2-1 89.04 01/05/1995 01/05/1996 dpm/ml 05/11/2006 'Brenda .000009739 100 445-96-2-11 .201761 07/26/2006 07/26/2007 Burke dpm/mL 09/30/2015 Tim 1.0796 500 445-96-2-III 4471.0794 09/21/2016 09/21/2017 Chandler dpm/mL 07/20/1995 Theresa .0041 100 445-96-2-J 84.9 01/05/1995 01/05/1996 Austin dpm/ml 05/01/2007 Daniel Roy .0352 1000 445-96-2-JJ 72.9209 04/30/2008 04/30/2009 dpm/ml 05/31/2016 Christina .0010641 500 445-96-2-JJJ 4.40688 05/31/2016 05/31/2017 Kimball dpm/mL 08/10/1995 Garret Ray .0952 100 445-96-2-K 1971.32 01/05/1995 01/05/1996 dpm/ml 06/12/2007 Julie Strock .01038 250 445-96-2-KK 22.1496 05/28/2008 05/28/2009 dpm/mL 08/01/2016 Christina .0057457 100 445-96-2-KKK .23521 08/01/2016 08/01/2017 Kimball dpm/mL 09/11/1995 Theresa 1.0525 100 445-96-2-L 21794.23 01/05/1995 01/05/1996 Austin dpm/ml Page 1961of5809 09/11/1995 Theresa .5107 100 445-96-2-L-1 111.3 01/05/1995 01105/1996 Austin dpm/ml 04/28/1998 Richard .1264 100 445-96-2-M 2617.4 04/28/1998 04/28/1999 Kinney dpm/ml 1110112007 Eric .001274' 500. 445-96-2-MM 5.27945 04/06/2008 04/06/2010 Williamson dpm/mL 10/12/1998 Gregory .1348 100 445-96-2-N 2791.32 01/05/1995 01/05/1996 Smith dpm/mL 01/25/1999 Gregory 1.9382 100 445-96-2-N-1 50.16 01/05/1995 01/05/1996 Smith dpm/ml 04/19/2008 Daniel Roy .0424 1000 445-96-2-NN 87.8366 04/16/2009 04/16/2010 dpm/ml 04/2111999 Greg Smith .1645 100 445-96-2-0 3406.32 04/21/1999 0412112000 dpm/mL 07/27/1999 Gregory 1.567 100 445-96-2-0-2 50.56 05/13/1999 05/13/2000 Smith dpm/ml 10/12/1999 Richard 1.5589 100 445-96-2-0-3 50.31 05/13/1999 05/13/2000 Kinney dpm/mL 04/21/1999 Greg Smith 1.5309 100 445-96-2-0-1 49.4 04/2111999 04/21/2000 dpm/mL 02/23/2011 Christina .0005294 250 445-96-2-00 4.3866 02/23/2011 02/23/2012 Kimball dpm/mL 1111,0/1999 Joe Davis .1809 100 445-96-2-P 3745.92 05/13/1999 05/13/2000 dpm/mL 01/04/2008 Julie Strock .00001005 100 445-96-2-PP .20819 12/29/2008 12/29/2009 dpm/mL 01/28/2000 Angela .0354 1000 445-96-2-Q 73.3 02/08/2001 02/08/2002 Johnson dpm/mL 09/29/2008 Tara Sides .0025219 250 445-96-2-QQ 20.8977 09/14/2009 09/14/2010 dpm/mL 04/18/2000 Robert .429 250 445-96-2-R 3553.34 04/18/2000 04/18/2001 Timm dpm/mL 04/23/2009 Tina .001251 500 445-96-2-RR 4.8075 04/09/2010 04/09/2011 Schoneman dpm/mL 04/13/2001 Angela .1869 100 445-96-2-S 3870.16 04/13/2001 04/13/2002 Johnson dpm/mL 05/08/2009 Mary Aders .0141 1000 445-96-2-SS 29.2098 05/11/2009 05/1112010 dpm/ml 07/03/2001 Lonnie 2.0057 1000 445-96-2-T-103 4153.225 07/03/2002 07/03/2003 Morris dpm/mL 07/03/2001 Lonnie 2.0057 1000 445-96-2-T-203 4153.225 07/03/2002 07/03/2003 Morris dpm/mL 07/03/2001 Lonnie 2.0057 1000 445-96-2-T-303 :;i153.225 07/03/2002 07/03/2003 Morris dpm/mL Page 1962of5809 06/03/2009 Julie Strock 08/23/2001 Angela Johnson 08/23/2001 Angela Johnson 08/23/2001 Angela Johnson 06/02/2009 Mary Aders 08/27/2001 Angela Johnson 08/27/2001 Angela Johnson 08/27/2001 Angela Johnson 03/09/2010 Ashley Drochter 09/06/2013 Christina Kimball 03/17/2003 Angela Johnson 03/23/2010 Ashley Drochter 04/14/2003 Lonnie Morris 09/13/2010 Julie Strock 05/03/2003 Tim Chandler 10/20/2010 Ashley Drochter 05/05/2003 Eric Williamson 11/23/2010 Ashley Drochter GEL Laboratories LLC Version 1.0 9/18/2000 Page 1963 of 5809 .00000927 100 .0194 500 .0194 500 .0194 500 2.1177 1000 .0394 1000 .0394 1000 .0394 1000 .011 1000 .0010458 500 2.1108 1000 .0163 1000 .0315 1000 .00049678 250 .0103 1000 .0146 1000 .011 1000 2.1175 1000 445-96-2-TT .1923 06/02/2011 06/02/2012 dpm/mL 445-96-2-U-103 80.34 08/23/2001 08/23/2002 dpm/mL 445-96-2-U-203 80.34 08/23/2001 08/23/2002 dpm/mL 445-96-2-U-303 80.34 08/23/2001 08/23/2002 dpm/ml 445-96-2-UU 4387.0634 05/18/2011 05/18/2012 dpm/ml 445-96-2-V-103 81.586 08/27/2002 08/27/2003 dpm/mL 445-96-2-V-203 81.586 08/27/2002 08/27/2003 dpm/mL 445-96-2-V-303 81.586 08/27/2002 08/27/2003 dpm/mL 445-96-2-VV 22.7878 02/06/2015 02/06/2016 dpm/mL 445-96-2-FFF 4.33111 08/30/2014 08/30/2015 dpm/mL 445-96-2-W 4370.857 03/14/2006 03/14/2007 dpm/mL 445-96-2-WW 33.7674 03/23/2010 03/23/2011 dpm/mL 445-96-2-X 65.2559 04/14/2004 04/14/2005 dpm/mL 445-96-2-XX 4.1166 09/13/2010 09/13/2011 dpm/mL 445-96-2-Y 21.3376 05/05/2003 05/05/2004 dpm/mL 445-96-2-YY 30.2456 10/20/2010 10/20/2011 dpm/mL 445-96-2-Z 22.7877 04/03/2007 04/03/2008 dpm/mL 445-96-2-ZZ 4386.6491 06/14/2012 06/14/2013 dpm/mL Verification for Am-243 Standard 445-96-2-111 v1.2 Analyst TC1 Tracer Information Verification Prep Date 9/21/2016 Isotope Cm-244 Serial Number 1216-G Amount of Std. (ml) 0,2 Exoiration Date 9/30/2016 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dpm/ml) Amount of Std. (ml) Standard Prep Date Am-243 Std# Count Date pCi dpm/ml Certificate Value* = 10.0485 445-96-2-111 1 9/21/2016 9.660 4289.04 Two sigma= 0.3355 7.3700E+03 Y 2 9/21/2016 9.640 4280.16 10%ofMean = 0.9553 1/1/1994 3 9/21/2016 9.360 4155.84 Rule A (Pass/Fail) Pass 4471.0794 % Recovery 95.07% 0.0 Mean Value = 9.553 4241 .680 Rule B (Pass/Fail) Pass 9/30/2015 Stdev = 0.167729942 74.4720941 Expiration Date 9/21/2017 Verification Rules Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value;
Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Am-243 standard 445"96-2-111 using 0.005 ml for each source. Each standard was combined with 0.2 ml of Cm-244 standard.1216-G and was diluted in a 50 ml plastic centrifuge tube containing 20 ml of 1 M HCI, 100 micrograms of neodymium carrier and five ml of 48% HF was added to precipitate neodymium (and Americium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Am-243 were calculated by comparison to Cm-244 certified values. dpm/ml 4461.5351 148.9442 424.1680 Pass 95.07% Pass I ........._ 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 J . : Eckert & Ziegler Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com I -' I ' I _f *-' ' I I -I I *-' Analytics CERTIFICATE OF CALIBRATION Standard Radionuclide Source 77573-278 Cm-244 S mL Liquid in Flame Sealed Vial Customer: General Engineering Labs P.O. No.: 7308 RD, Item 9 This standard radionuclide source was prepared gravimetrically from a calibrated master liquid radionuclide solution source. The master source was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and assay date for this source are given below. ANALYTICS maintains traceability to the National Institute of Standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision l. Comments: Impurities: ISOTOPE: ACTIVITY (Bq): HALF-LIFE: CAI.lBRATION DATE: :RELATIVE EXPANDED Cm-244 l.950E4 l.810 El years June 19, 2008 12:00 EST UNCERTAINTY (k=2): 2.0% y-impurities <0.1 % Pu-238 <41 Bq Pu-240 -59 Bq 5.03182 grams IM HCl solution. ----Source Prepared By: .4?'?M=z?<2 g..,.<fl---M. I. Taskaeva, Radiochemist QA Approved: 1.rn? A D. :oJf Manager Date: ,.., ';).IJ-a f Page 1965 of 5809 7 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Curium-244 Parent Code: 1216 Prepared By: Daniel Roy Prepared By: Daniel Roy Prep Date: 06/24/2008 Carrier Cone: lMHCL Verification Date: 09/24/2014 Reference Date: 06/19/2008 Expiration Date: 09/24/2015 Ampoule Mass (g): 5.03182 g Primary Code: 1216-A Uncertainty: +/-1 % Dilution(mL): lOOmL LogBookNo: RC-S-048-097 Mass of Parent(g): 4.882 g Density(g/mL): 1.0153 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (4.882 g) * (19500 Bq) * (60 dpm/Bq) I (5.03182 g

100 mL) = 11351.6382 dpm/mL (4.882 g) * (19500 Bq) * (60 dpm/Bq) I ( 1.0153 g/mL)/ (5.03182 g

100 mL) = 11181.0599 dprn/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone Verification Expiration Primary (mL) dpm/mL Date Date 06/28/2008 Daniel Roy 7.0442 1000 1216-B 78.7616 06/07/2011 06/07/2012 dpm/ml 10/05/2009 Tara Sides 9.9307 100 1216-C 1110.36 11117/2011 11117/2012 dpm/mL 12/14/2011 Julie Strock 1 ASCS2012-001 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-002 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-004 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-005 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-007 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-008 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-009 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-016 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-017 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-018 1110.36 dpm 12/14/2020 12/14/2021 Page 1966 of 5809 12/14/2011 Julie Strock 1 ASCS2012-019 1110.36 dpm 12/14/2020 12/14/2021 12114/2011 Julie Strock 1 ASCS2012-020 1110.36 dpm 12/14/2020 12/14/2021 12114/2011 Julie Strock 1 ASCS2012-021 1110.36 dpm 12/14/2020 12/14/2021 12/14/2011 Julie Strock 1 ASCS2012-023 1110.36 dpm 12/14/2020 12114/2021 12/23/2011 Julie Strock 1 ASCS2012-025 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-026 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-027 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-028 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-029 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-030 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-031 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-032 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-033 1110.36 dpm 12/23/2020 12/23/2021 12/23/2011 Julie Strock 1 ASCS2012-034 1110.36 dpm 12/23/2020 12/23/2021 03/13/2012 Julie Strock .5 7 1110.36 dpm 03/1312021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-038 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-039 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-040 1110.36 dpm 03/1312021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-041 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-042 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-043 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-044 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-045 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-046 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-047 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-048 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-049 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-050 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-051 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-052 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-053 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-054 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-055 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-056 1110.36 dpm 03/1312021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-057 1110.36 dpm 03/1312021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2Ql2-058 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-059 1110.36 dpm 03/13/2021 03/13/2022 03/13/2012 Julie Strock .5 ASCS2012-060 1110.36 dpm 03/13/2021 03/13/2022 Page 1967of5809 10/05/2009 Tara Sides 01/03/2011 Christina Kimball 01/05/2011 Christina Kimball 10/31/2011 Ashley Drochter 06/08/2016 Christina Kimball 03/08/2012 Christina Kimball 04/30/2012 Christina Kimball 05/21/2012 Christina Kimball 09/24/2014 Christina Kimball GEL Laboratories LLC Version 1.0 9/18/2000 Page 1968of5809 .0496535 100 .044 100 .0508 100 7.0911 1000 .0513 100 .009948 250 .00535 250 .0501 100 .0513 100 1216-D 5.5518 09/13/2010 09/13/2011 dpm/mL 1216-E 4.9197 01/03/2011 01/03/2012 dpm/mL 1216-F 5.67998 12/21/2012 12/21/20'13 dpm/mL 1216-G 79.2860138 09/21/2016 09/21/2017 dpm/mL 2416618 5.73588 01/22/2016 01/22/2017 dpm/mL 1216-H .4449 03/08/2012 03/08/2013 dpm/mL 1216-I .239466 04/25/2016 04/25/2017 dpm/mL 1216-J 5.601711 12/12/2014 12/12/2015 dpm/mL 1216-K 5.73588 01/22/2016 01/22/2017 dpm/mL
...... "' 0\ "' 0 ....., Ut 00 0 "' Verification for Cm-244 Standard 1216-G v1.2 Analyst TC1 Tracer Information Verification Prep Date 9/21/2016 Isotope Am-243 Serial Number 1752-C Amount of Std. (ml) 0.5 Exoiration Date 5/26/2017 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dam/ml) Amount of Std. (ml) Standard Prep Date Cm-244 1216-G 18.1100 y 6/19/2008 79.2860138 0.2 10/31/2011 Verification Rules Std# 1 2 3 Count Date 9/22/2016 9/22/2016 9/22/2016 Mean Value= Stdev = pCi dpm/ml Certificate Value* = 5.2074 5.050 56.06 Two sigma= 0.4015 5.450 60.50 10 % of Mean= 0.5260 5.280 58.61 Rule A (Pass/Fail) Pass % Recovery 101.01% 5.260 58.386 Rule 8 (Pass/Fail) Pass 0.200748599 2.228309449 Expiration Date 9/21/2017 Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule 8 =The determined mean value shall be within 5% of the certificate value.
Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Cm-244 standard 1216-G.using 0.2 ml for each source. Each standard was combined with 0.5 ml of Am-243 standard 1752-C and was diluted in a 50 ml plastic centrifuge tube containing 20 ml of 1 M HCI, 100 micrograms of neodymium carrier and five ml of 48% HF was added to precipitate neodymium (and Curium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Cm-244 were calculated by comparison to Am-243 certified values. dpm/ml 57.8017 4.4566 5.8386 Pass 101.01% Pass Amersham pie The Grove Centre Amersham pk Radiation &: Radioactivity Calibration Laboratory The Grove Centre White Lion Road Amersham

Buckinghamshire HPi'.9LL -----*-------------. . Principal radionuclide: Neptunium-237 Daughter radionuclide: Protactinium-233 easurement Reference time: Radioactive concentration of neptunium-23 7: . ' which is equivalent to: .

Mass of solution: Total activity ofneptunium-237: which is equivalent to: Method of measurement used: ISSUED FOR: AEA Technology plc lsotrak 329 Harwell Didcot Oxfordshire OXllOQJ Product code: Solution number: NGZ44 SS/31/100 1200 GMT on 27 November 1995 45.86 kilobecquerels per gram of solution 1.240 microcuries per gram of solution 5.0201 grams 230.2 kilobecquerels 6.22 microcuries 41t coincidence and anticoincidence counting using a gas flow proportional counter. *Calibration date(s): 25 November 1995 to 1 December 1995 . The calibration date is provided for added infonuation only, and must not be confused with the reference date. It is the reference date that must be useu in all calculations relating to ifa. values of at:!ivity. Expanded uncertainty in the radioactive concentration quoted above: :l: 1.79 % ("..Combined Type A uncertainty: :I: 0.24 % . \ 'Combined Type B uncertainty:+/- 0.87 % Date of issue UKAS ACCREDITED CALIBRATION LAB ORA TORY No. 0146 Radionuclidic The estimated activities of any radioactive impurities found by high-resolution gamma ray or in any urity other.examination of the solution; are listed below expressed as percentages oftb.e activity of the principal radionuclide at the reference time. Plutonium-23-8 0.14(2)% O. lM HCl containing 1.8i milligrams ofneptunium per ml. Recommended half life: * (2.14 +/- 0.01) x 106 years (1 year= 365.25 days) This measurement was on the following assumptions about the decay scheme neptunium-237 and protactinium-233: Neptunium-237: .100% alpha particle emission followed by prompt L X-rays of Protactinium-233. Protacfu:rium-233: 100% beta particle emission. Half life 27.0 days. This product meets the quality a5surance requirements for achieving traceability to NIST as defined in ANSI N42.22-1995. Nuclear data quoted on this certificate are taken from the Joint European File, Version 2.2. The daughter nuclide protactinium-233 was chemically separated from the neptunium-23 7 at 0814 GMT on 22 November 1995. At any time t days from the time of separation, the ratio actiyi.1y of Pa-233 activity ofNp-237 in the ampoule is given by (l-e-4*025671) There can be no guarantee that the protactiniwn will remain in solution. xpression of The reported expanded uncertainty is based on a standard uncertainty multiplied by a coverage factor k = 2.00,. Jncertainties which for at-distribution with Vetr"" co effective degrees of freedom corresponds to a coverage probability of approximately 95 %. The uncertamty evaluation has been carried out in accordance with UK.AS requirements. ('\Unless all other uncertainties are expressed at the confidence level associated with one standard * *Scertamty. . The format used for the un?Crtainties in the values ofradionuclidic purity is illustrated in the following examples; 6.5(21) 6.54(21) fi *W\(?.1' = = 6.5

2.1 6.54+/-0.21 (i_l:j4i+/-0.021 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Neptunium-237 Parent Code: 0518 Prepared By: Angela Johnson Prepared By: Penet Melton Prep Date: 12/20/2002 Carrier Cone: 0.1 MHCL Verification Date: 07/24/2015 Reference Date: 11/27/1995 Expiration Date: 07/24/2016 Ampoule Mass (g): 5.02014 g Primary Code: 0518-A Uncertainty: +/-1.79 % Dilution(mL): lOOmL LogBookNo: RCS 035 033 Mass of Parent(g): 3.003 g Density(g/mL): 0.9992 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLJdpm/g (Mass ofparent(g)) *(Parm Activity (kBq/g)) *(conversion dpm to kBq) I (Dilution Vol)= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (kBq/g)) *(conversion dpm to kBq) I Density (g/mL)/ (Dilution Vol)= Parent Activity (dpm/g) (3.003 g) * (45.86 kBq/g) * (60000 dpm/kBq) I (100 mL) = 82630.5480 dprn/mL (3.003 g) * (45.86 kBq/g) * (60000 dpm/kBq) I ( 0.9992 g/mL) I (100 mL) = 82693.3120 dprn/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone Verification Expiration Primary (mL) dpm/mL Date Date 09/05/2003 Amanda .1004 100 0518-B 83.0241 09/10/2004 09/10/2005 Fehr dprn/mL 01/19/2004 Tim .1612 250 0518-C 53.3206 01/18/2004 01/18/2005 Chandler dprn/mL 11/23/2004 Amanda .25 250 0518-D 82.69 11/30/2007 11/29/2008 Fehr dprn/mL 04/16/2008 Daniel Roy .1312 100 0518-E 108.4936 08/23/2008 04/16/2009 dprn/ml 12/05/2008 Julie Strock .096 250 0518-F 31.7542 12/05/2008 12/05/2009 dprn/mL 12/05/2008 Julie Strock .0060406148 250 0518-G .02555 12/05/2008 12/05/2009 dprn/rnL 10/14/2008 Daniel Roy .2195 250 0518-H 72.6047 10/14/2008 10/14/2009 dprn/ml 02/02/2009 Christina .001312 500 0518-1 .216872 03/17/2016 03/17/2017 Kimball dprn/mL Page 1972of5809 02/1112009 Tina .0569 250 0518-J 18.821 02/11/2009 02/11/2010 Schoneman dpm/mL 07/10/2009 Mary Aders .2642 250 0518-K 87.3903 07/13/2010 07/13/2011 dpm/mL 10/06/2009 Robert 1.5146 100 0518-L 1252.47 03/21/2015 03/21/2016 Timm dpm/mL 03/21/2015 Christina .006099 100 0518-R 5.04428 03/21/2016 03/21/2017 Kimball dpm/mL 12/14/2011 Julie Strock .5 ASCS2012-001 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-002 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-004 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-005 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-007 626.235 12114/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-008 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-009 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-016 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-017 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-018 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-019 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-020 626.235 12/14/2020 12/14/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-021 626.235 12/14/2020 12114/2021 dpm 12/14/2011 Julie Strock .5 ASCS2012-023 626.235 12/14/2020 12/14/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-025 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-026 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-027 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-028 626.235 12/23/2020 12/23/2021 dpm Page 1973of5809 12/23/2011 Julie Strock .5 ASCS2012-029 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-030 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-031 626.235 12/23/2020 . 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-032 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-033 626.235 12/23/2020 12/23/2021 dpm 12/23/2011 Julie Strock .5 ASCS2012-034 626.235 12/23/2020 12/23/2021 dpm 03/13/2012 Julie Strock .25 ASCS2012-037 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-038 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-039 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-040 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-041 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-042 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-043 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-044 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-045 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-046 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-04 7 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-048 626.235 03/13/2021 03/1312022 dpm 03/13/2012 Julie Strock .25 ASCS2012-049 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-050 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-051 626.235 03/13/2021 03/13/2022 dpm 03/13/2012 Julie Strock .25 ASCS2012-052 626.235 03/13/2021 03/13/2022 dpm Page 1974of5809 03/13/2012 Julie Strock 03/13/2012 Julie Strock . 03/13/2012 Julie Strock 03/13/2012 Julie Strock 03/13/2012 Julie Strock 03/13/2012 Julie Strock 03/13/2012 Julie Strock 03/13/2012 Julie Strock 03/02/2010 Julie Strock 03/17/2010 Ashley Drochter 06/03/2010 Julie Strock 08/16/2011 Ashley Drochter 02/14/2012 Christina Kimball 07/24/2015 Tim Chandler GEL Laboratories LLC Version 1.0 9/18/2000 Page 1975of5809 .25 .25 .25 .25 .25 .25 .25 .25 .095 250 .2751 250 .00532519 100 .2893 250 .00174 500 .2997 250 ASCS2012-053 626.235 03/13/2021 03/13/2022 dpm ASCS2012-054 626.235 03/13/2021 03/13/2022 dpm ASCS2012-055 626.235 03/13/2021 03/13/2022 dpm ASCS2012-056 626.235 03/13/2021 03/13/2022 dpm ASCS2012-057 626.235 03/13/2021 03/13/2022 dpm ASCS2012-058 626.235 03/13/2021 03/13/2022 dpm ASCS2012-059 626.235 03/13/2021 03/13/2022 dpm ASCS2012-060 626.235 03/13/2021 03/13/2022 dpm 0518-M 31.4235 03/02/2010 03/02/2011 dpm/mL 0518-N 90.9957 01/23/2013 01/23/2014 dpm/mL 0518-0 4.4036 05/23/2014 05/23/2015 dpm/mL 0518-P 95.6927 08/03/2015 08/03/2016 dpm/mL 0518-Q .287518 03/26/2012 03/26/2013 dpm/mL 0518-S 99.1327 07/18/2016 07/18/2017 dpm/mL Verification for Np-237 Standard 0518-S v1.2 Analyst TC1 Tracer Information Verification Prep Date 7/18/2016 Isotope Cm-244 Serial Number 1216-G Amount of Std. (ml) 0.2 Exoiration Date 9/30/2016 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dom/ml) Amount of Std. (ml) Standard Prep Date Np-237 0518-S 2.1400E+06 Y 11/27/1995 99.1327 0.2 7/24/2015 Verification Rules Std# 1 2 3 Count Date 7/18/2016 7/18/2016 7/18/2016 Mean Value= Stdev= pCi dpm/ml Certificate Value*= 8.9308 8.770 97.35 Two sigma= 0.8492 9.520 105.67 10 % of Mean= 0.9030 8.800 97.68 Rule A (Pass/Fail) Pass % Recovery 101.11% 9.030 100.233 Rule B (Pass/Fail) Pass 0.424617475 4.713253972 Expiration Date 7/18/2017 Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value. *Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Np-237 standard 0518-S using 0.2 ml for each source. Each standard was combined with 0.2 ml of Cm-244 standard 1216-G and w_as diluted in a 50 ml plastic centrifuge tube containing 15 ml of 1M HCI. To each source, 0.5 ml of H202, 100 micrograms of neodymium carrier and five ml of 48% HF was added to precipitate neodymium (and Neptunium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Np-237 were calculated by comparison to Cm-244 certified values. dpm/ml 99.1320 9.4265 10.0233 Pass 101.11% Pass 1 c, I ] -..... -L ..... ,\! ANALYTICS 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318

U.S.A. CERTIFICATE OF CALIBRATION Standard Radionuclide Source 60513-278 Pu-239 S mL Liquid in Flame Sealed Vial Phone (404) 352-asn Fax (404) 352-2837 This standard radionuclide source was prepared using an aliquot measured gravimetrically from a master radionuclide solution standard.

The master radionuclide solution standard was ca.librated by the Department Des Applications Et De La Metrologie Des *Rayonnements Ionisants (DAMRI), Paris, France, as Number 24148. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. *The nuclear decay rate and assay date for this source are given below. ANALYTICS maintains traceability to the National Institute of standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision 1. ISOTOPE: ACTIVITY (dps): HALF-LIFE: CALIBRATION DATE: TOTAL UNCERTAINTY*: *99% confidence level. PU-239 3.674 E4 24131 years October 30, 2000 12:00 EST . 5.0% 5.45541 grams 3M HN03 solution. detected (activity in dps/vial on Oct. 30, 2000): Am-241 297.28 Pu-240 1208.8 Pu-241 2010.'1 Pu-242 0.17 See reverse side for additional information. P 0 NUMBER 2528RD, Item 1 PREPARED BY: M. Taskaeva, Radiochemist Q A APPROVED:* of 5809 t.c __ 5 -1 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Plutonium-239 Parent Code: 0338 Prepared By: Perret Melton Prepared By: Perret Melton Prep Date: 12/01/2000 Carrier Cone: 3 MHN03 Verification Date: 07/27/2015 Reference Date: 10/30/2000 Expiration Date: 05/31/2017 Ampoule Mass (g): 5.45541 g Primary Code: 0338-A Uncertainty: +/-1.953 % Dilution(mL): lOOmL LogBookNo: RC-S-029-134 Mass of Parent(g): 5.1674 g Density(g/mL): 1.0121 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLjdpm/g (Mass ofparent(g)) *(Parm Activity (dps)) *(conversion dpm to dps) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (dps)) *(conversion dpm to dps) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (5.1674 g) * (36740 dps) * (60 dpm/dps) I (5.45541g*100 mL) = 20880.2208 dpm/mL (5.1674 g) * (36740 dps) * (60 dpm/dps) I ( 1.0121 g/mL)/ (5.45541 g

100 mL) = 20630.6111 dpm/g (5.1674 g) * (37948.8 dps) * (60 dpm/dps) I (5.45541 g

100 mL) = 21567.2108 dpm/mL (5.1674 g) * (37948.8 dps) * (60 dpm/dps) I ( 1.0121 g/mL)/ (5.45541 g

100 mL) = 21309.3885 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone Verification Expiration Primary (mL) dpm/mL Date Date 06/23/2009 Mary Aders .591 250 0338-BB 50.3753 06/23/2009 06/23/2010 dpm/mL 03/09/2010 Ashley .5127 250 0338-CC 43.7013 03/09/2010 03/09/2011 Drochter dpm/mL 01/12/2011 Ashley .5302 250 0338-DD 45.193 01/06/2012 01/06/2013 Drochter dpm/mL 1012912001 Tim Chandler .3032 250 0338-E 10/16/2003 10/1612004 04/18/2011 Ashley .528 250 0338-EE 45.0054 03/29/2012 03/29/2013 Drochter dpm/mL 05/17/2011 Christina .101 500 0338-FF 4.3045 09/19/2016 09/19/2017 Kimball dpm/mL 05/15/2012 Christina .256 250 0338-GG 21.82081 09/27/2016 09/27/2017 Kimball dpm/mL Page 1978of5809 09/04/2012 Ashley Drochter 12/30/2002 Tim Chandler 01/22/2013 Christina .Kimball 01/07/2015 Christina Kimball 08/12/2003 Amanda Fehr 01/07/2015 Christina Kimball 12/09/2003 Amanda Fehr 01/07/2015 Christina Kimball 03/18/2004 Tim Chandler 07/24/2015 Tim Chandler 04/26/2004 Amanda Fehr 05/31/2016 Christina Kimball 05/26/2004 Eric Williamson 12/20/2004 Brenda Burke 03/16/2005 Julie Strock 07/19/2005 Amanda Fehr 05/11/2006 Brenda Burke 01/04/2007 Julie Strock 01/05/2007 Daniel Roy 03/16/2007 Julie Strock 05/15/2007 Eric Williamson 07/31/2007 Julie Strock 12/10/2008 Daniel Roy 09/29/2008 Tara Sides GEL Laboratories LLC Version 1.0 9/18/2000 Page 1979of5809 1.0264 10.0252 .248 .119 .2282 .0052 .2409 .052 10.0192 1.0298 .643 .005109 .355 .01957 10.0395 .677 .0009935 .050286 .7285 .010175 .253 .0010045 .7715 .0504 ' 500 0338-HH 43.7439 07/22/2016 07/22/2017 dpm/mL 100 0338-1 10/24/2003 10/24/2004 250 0338-11 21.1389 01/22/2013 09/11/2013 dpm/mL 500 0338-JJ 5.0716 01/07/2015 01/07/2016 dpm/mL 100 0338-K 08/12/2003 08/12/2004 500 0338-KK .22166 01/04/2016 01/04/2017 dpm/mL 100 0338-L 12/09/2003 12/09/2004 500 0338-LL 2.2162 01/04/2016 01/04/2017 dpm/mL 500 0338-M 03/18/2004 03/18/2005 500 0338-MM 42.8888 07/20/2016 07/20/2017 dpm/mL 250 0338-N 04/26/2005 04/26/2006 500 0338-NN .21776 05/31/2016 05/31/2017 dpm/mL 250 0338-0 30.2619 05/17/2007 05/17/2008 dpm/mL 100 0338-P 4.16992 12/19/2006 12/19/2007 dpm/mL 100 0338-Q 2139.558 06/12/2008 06/12/2009 dpm/mL 250 0338-R 07/10/2006 07/10/2007 100 0338-S .21172 07/30/2007 07/28/2007 dpm/mL 250 0338-T 4.2887 12/31/2007 12/31/2008 dpm/mL 250 0338-U 01/05/2008 01/05/2009 1000 0338-V .216847 03/21/2015 03/21/2016 dpm/mL 250 0338-W 21.567 05/02/2012 05/05/2013 dpm/mL 100 0338-X .21379 12/31/2007 12/31/2008 dpm/mL 250 0338-Y 12/10/2008 12/10/2009 250 0338-Z 4.29599 09/01/2010 09/01/2011 dpm/mL Verification for Pu-239 Standard 0338-MM V1.2 Analyst TC1 Tracer Information Verification Prep Date 7/20/2016 Isotope Pu-242 Serial Number 1769-A Amount of Std. (ml) 0.2 Exoiration Date 5/2/2017 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dom/mU Amount of Std. (ml) Standard Prep Date Pu-239 0338-MM 2.4131E+04 Y 11/15/2011 43.8888 0.2 7/24/2015 Verification Rules Std# 1 2 3 Count Date 7/20/2016 7/20/2016 7/20/2016 Mean Value= Stdev= pCi dpm/ml Certificate Value* = 3.9534 3.990 44.29 Two sigma= 0.1510 4.140 45.95 10%of Mean= 0.4060 4.050 44.96 Rule A (Pass/Fail) Pass % Recovery 102.70% 4.060 45.066 Ru_le B (Pass/Fail) Pass 0.075498344 0.83803162? Expiration Date 7/20/2017 Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value.

Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Pu-239 standard 0338-MM using 0.2 ml for each source. Each standard was combined with 0.2 ml of Pu-242 standard 1769-A and was diluted in a 50 ml plastic centrifuge tube containing 15 ml of 1 M HCI. To each source, 6 drops of 25% hydrazine dichloride, 100 micrograms of neodymium carrier and five ml of 48% HF was added to precipitate neodymium (and Plutonium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Pu-239 were calculated by comparison to Pu-242 certified values. dpm/ml 43.8829 1.6761 4.5066 Pass 102.70% Pass
. . : \J!') & W:edµwln£t! '411!8 di *.*. ' . . . .' *: '*' .*
qiertif ica:f.e Standard Reference Material 43341 1110 Plutonium-242 Radioactivity Standard This Standard Reference Material;(SRM) consists of a solutibil of a standardized and certified quantity of radioactive plutonium-242 in a suitably stable and matrix. It is intended primarily for* the calibration of instruments that are used to measure radioactivity and for the monitoring of radiochemical procedures. A unit consists of a solution, whose composition is specified in Table 1, contained in a flame-sealed 5 mL borosilicate-glass ampoule (see Note l)". The certified Plutonium-242 massic activity value, at a Reference Time of 1200 EST, 01January2010, is: (26.77 +/- 0.18) Bq*g*1* Additional physical, chemical, and radiological properties for this SRM, as well as details on the standardization method, are given in Table 1. Uncertainties for the certified quantities are expanded (k = 2). The uncertainties are calculated according to the ISO Guide (see Note 2). Table 2 contains a specification of the components that comprise the uncertainty analyses. , ,., , . , ; \. Expiration of Certification: The certification of SRM 43341 is valid indefinitely provided the SRM is handled and . and that no evaporation or change in composition has occurred. The solution matrix, in an unopened ampoule, is homogeneous *ahd stable within its half-life-dependent useful lifetime provided the SRM is handled in accordanc'e with instructions given in 'this certificate (see "Instructions for Storage and Handling"). The certification is nullified if the SRM is damaged, contaminated, or otherwise modified. Maintenance of Certification: NIST will monitor this SRM over the period of its certification. If substantive technical changes occur that affect the certification before the expiration of this certificate, NIST will nptify the purchaser. Registration (see attached sheet) wili facilitate notification. This SRM may represent a radiological hazard and a chemical hazard. Consult the Material Safety Data Sheet (MSDS), enclosed with the SRM shipment, for details. ' * ' This Standard Reference Materiiil was prepared in the Physics Laboratory, Ionizing Radiation Division, Radioactivity Group, M.P. Unterweger, Group Leader. The overall technical direction and physical measurement leading to certification were provided by L. Lucas of the NIST Radioactivity Group. Support aspects involved in the issuance of this SRM were coordinated through the NIST Measurement Services Division. INSTRUCTIONS FOR STORAGE AND HANDLING Storage: SRM 43341 should be stored and used at a temperature between 5 °C and 65 °C. The ampoule (or any subsequent container) should always be clearly marked as containing radioactive material. Handling: If the ampoule is transported, it should be packed, marked, labeled, and shipped in accordance with the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous good (hazardous material) because of both the radioactivity and the strong acid. The ampoule should be opened only by persons qualified to handle both radioactive material and alkaline and/or acidic solutions. Appropriate shielding and/or distance should be used to minimize personnel exposure. Refer to MSDS for further infonnation. Gaithersburg, MD 20899 Certificate Issue Date: 30 June 20 l 0

Notes and.,references may be found on pages 4 and 5. SRM4334I Page 1981of5809 Lisa R. Karam, Chief Ionizing Radiation Division Robert L. Watters, Jr., Chief Measurement Services Division l 'Page 1of5 Table 1. Properties of SRM 43341 Certified values Radionuclide Plutonium-242 Reference time 1200 EST; 1 January 2010 (See Note 3)

Massie activity of the solution 26.77 Bq*g*1. ,. .. Relative expanded uncertainty (k = 2) 0.68 % (see Note 2) Uncertified infonnation Source description Liquid in a 5 mL borosilicate-glass {see Note 1) Solution composition 3.2 mol I:1 HN03 Solution density (1.105 +/- 0.002) g 'niL1at22 °C (see Note 4) ***:* Solution mass Approximately 5.5 g Alpha-particle-emitting 241Am: (0.00f6 +/- 0.0003) Bq g1 (See Note 3,. 5 and. 6)

impurities Beta-particle-emitting 241Pu : (0.044 +/- 0.009) Bq g1 (see 4) impurities . Phpfon-emitting .. ** .. *

impuritie.s -None detected (see Note 7) -l..* ,242Pu: (373 500 +/- 1100) a (see Note 8) [l] 241Pu: (14.290 +/- 0.006) a Half-lifes used 240Pu: (6 561 +/- 7) a 239Pu: (24 110 +/- 30) a ,. 238Pu: (87.7 +/- 0.1) a

241 Am: { 432.6 +/- 0.6) a Calibration methods (and The certified massic activity for 242Pu was obtained by 4mx liquid scintillation (LS) instruments) spectrometry using four commercial LS counters, a calibrated gennanium detector system, and a silicon surface-barrier detector. ,.

Notes and reforences may be found on pages 4 and 5. SRM43341 Page 1982of5809 I' . Page2 of5 Tabfo'2; Uncertainfy'evaluation for the massieactivify ofSRM 4334! *' Relative standard ... '-'*' '*' .. tin certainty UncertaintY component. Assessment Typet contribution on ., " ;. massic activity of 242pu (%) Massie alpha-particle emission rate, for packground and decay. I Standard deviation of the mean for 180 4m:x A 0.06 . measurements. .. 2 Halflife of242Pu; standard uncertainty of the halflife B 3 x 10-6 3 Decay-scheme data; standard uncertainty'of the probability of decay by B 0.001 alpha-particle emission 4 Extrapolation of the alpha-particle-count-rate-versus-energy to zero energy B 0.25 " . ' 5 Gravimetric measurements B .. 0.10 6 Live time :'.,I fL

B J. 0.10 .. 7 Alpha-particle detection efficiency of scintillators B OJO 8 241Pu detection efficiency of scintillators' * . : .......... *. If 0.04 9 Alpha-particle limit of detection B 0.10 IO 241Pu impurity i B 0.02 .. ... 11 Photon emitting impurities; limit of detection

B 0.10 Relative combined standard uncertairify* *-* 0.34 Relative expanded uncertainty (k = 2) * ' 0.68 T= (A) denotes evaluation by statistical methods, (B) denotes evaluation by other methods. > *. ' : ... * ': ... : : .. '! . -. . : **:**. *: . :*-r . ,., .. -* .': ; -::: ! . : SRM4334I Page3of5 Page 1983of5809 Note 1. Refer to http://physics.nist.gov/Divisions/Div846/snn.html (accessed Jun 2010) for assistance and instructions on how to properly open an ampoule. Infonnation on additional storage and handling requirements is also included on the website. This SRM is contained in a generic borosilicate-glass ampoule and not in the standard NIST ampoule. Note 2. The uncertainties on certified values are expanded uncertainties, U = kuc. The quantity Uc is the combined standard uncertainty calculated according to the ISO Guides [2-3]. The combined standard uncertainty is multiplied by a coverage factor of k = 2 and was chosen to obtain an approximate 9 5 % level of confidence. Note 3. The 242Pu was chemically purified 07 June 1994 at the Lawrence Livennore National Laboratory (LLNL). Americiurp.-241, the daughter of241Pu, was removed but has been growing in since that time. * .. Note 4. The stated uncertainty is two times the standard uncertainty. See reference 3. Note 5. The estimated limits of detection for alpha-particle-emitting impurities, as massic alpha-particle emission: rates of alpha-particles emission rates second per gram), are: . 6.003 s*1 gi, for energies less than 3.1 MeV, 0:03 s"1. g1 for energies between 3.1 MeV and 4.4 keV; and 0.003 s*1 g1 for energies greater than 5.0 MeV Note 6. The 242Pu was chemically purified 07 June 1994. The relative massic activities ofradionuclidic impurities after purification foliow; *-** * * . * * * * .

ll . Radionuclide Relative Activity As Determined By LLNL NIST :t4"Pu 1 ' 1 ,. :mpu --(3.5 +/- 0.4) x 10-3 {a) ""uPu + "'YPu < 10-0 (b) (2.0 +/- 2.1) x 10-s (c) "'"Pu+ i41Am < 1.6 x (b) (9 +/- 16) x I0-6 (c) 241Am --assumed 0 (a) ' (a) The stated uncertainty is the standard uncertainty. The 241Pu activity was calculated from a gamma-ray measurement of the 241Am ingrowth as of 25 November 1998, assuming was completely removed at the time of chemical purification. (b} Using alpha-particle spectrometry. The value shown is an estimated upper limit based upon background and counting statistics. Measurements were made at the Lawrence Livennore National Laboratory (LLNL) in July of 1994. * ( c) Using alpha-particle spectrometry. The stated uncertainty is the standard uncertainty. Measurements were made at the National Institute of Standards and Technology (NIST) in June and July 1999. Note 7. The estimated limits of detection for photon-emitting impurities, expressed as massic photon emission rates (numbers of photons per second per gram), are: 5 x 10-s s*1 g1 for energies between 19 keV and 39 keV, 7 x 10-s s"1 g1 for energies between 49 keV and 92 keV, 2 x 10-s s"1 g1 for energies between 106 keV and 507 keV, 1 x 10-5 s"1 g1 for energies between 515 keV and 1456 keV, and 5 x 10*6 s"1 g1 for energies between 1465 keV and 2750 keV. . provided that the photons are separated in energy by 4 ke more from photons emitted in the decay of242Pu, 241Pu, or 241Am. Note 8. The stated uncertainty is the standard uncertainty. See reference 2. SRM4334I Page 4 of5 Page 1984of5809 REFERENCES [l] Evaluated Nuclear Structure Data File (ENSDF), online database, National Nuclear Center, Brookhaven National Laboratory (Upton, NY), accessed November 2009. Refer to http://www.nndc.bnl.gov/nudat2/ Jun 2010). [2] JCGM 100:2008; Evaluation of Measurement Data-Guide to the Expression of Uncertainty in Measurement GUM 1995 with Minor Corrections); Joint Committee for Guides in Metrology (2008); available at http://www.bipm.org/utils/common/documents/jcgm/JCGM_l 00_2008_E.pdf (accessed May 201 O); see also Taylor, B.N.; Kuyatt, C.E.; Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results; NIST Technical Note 1297; U.S. Government Printing Office: Washington, DC (1994); available at http://www.nist.gov/physlab/pubs/index.cfin (accessed Jun 2010). [3] Thompson, A.; Taylor, B.N.; Guide for the Use of the International System of Units (SI); NIST Special Publication 811; U.S. Government Printing Office: Washington, DC (2008); available at: http://ts.nist.gov/WeightsAndMeasures/Metric/mpo_pubs.cfm (accessed Jun 2010). Users of this SRM should ensure that the Certificate in their possession is current. This can be accomplished by contacting the SRM Program: telephone (301) 975-2200; fax (301) 926-4751; e-mail srminfo@nist.gov; or via the Internet at http://www.nist.gov/srm. SRM4334I Page 5 of5 Page 1985of5809 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Plutoniuin-242 Parent Code: 1770 Prepared By: Tim Chandler Prepared By: Gregory Ram:say Prep Date: 08/03/2016 Carrier Cone: 3.2MHN03 Verification Date: 08/03/2016 Reference Date: 01/01/2010 Expiration Date: 08/03/2017 Ampoule Mass (g): 5.5 g Primary Code: 1770-A Uncertainty: +/-.34 % Dilution(mL): 200mL LogBookNo: GL-CED-297-063 Mass of Parent(g): 5.4578 g Density(g/mL): 1.0312 Balance ID: C31514 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq/g)) *(conversion dpm to Bq) I (Dilution Vol)= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq/g)) *(conversion dpm to Bq) I Density (g/mL)/ (Dilution Vol)= Parent Activity (dpm/g) (5.4578 g) * (26.77 Bq/g) * (60 dpm/Bq) I (200 mL) = 43.8316 dpm/mL (5.4578 g) * (26.77 Bq/g) * (60 dpm/Bq) I ( 1.0312 g/mL) I (200 mL) = 42.5054 dpm/g Prep Preparer Date GEL Laboratories LLC Version 1.0 9/18/2000 Page 1986 of 5809 Mass Primary Secondary Standards Dilution Code Cone Verification Expiration (mL). dpm/mL Date Date Verification for Pu-242 Standard 1770-A v1.2 Analyst TC1 Tracer Information Verification Pre Date 8/3/2016 Isotope Pu-239 Serial Number 0338-MM Amount of Std. (ml) 0.5 Expiration Date 7/20/2017 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dpm/ml) Amount of Std. (ml) Standard Prep Date Pu-242 1770-A 3.7350E+05 Y 1/1/2010 43.8316 0.5 8/3/2016 Verification Rules Std# 1 2 3 Count Date 8/4/2016 8/4/2016 8/4/2016 Mean Value= Stdev= pCi dpm/mL Certificate Value*= 9.8719 9.460 42.00 Two sigma= 0.4392 9.440 41.91 10 %of Mean= 0.9577 9.830 43.65 Rule A (Pass/Fail) Pass % Recovery 97.01% 9.577 42,520 Rule B (Pass/Fail) Pass 0.219620885 0.975116731 Expiration Date 8/3/2017 Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value . ... Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Pu-242 standard 1770-A using 0.5 ml for each source. Each standard was combined with 0.5 ml of Pu-239 standard 0338-MM and was diluted in a 50 ml plastic centrifuge tube containing 1 o ml of 2M HCI. Five drops of 25% hydrazine dichloride, 100 micrograms of neodymium carrier and three ml of 48% HF was added to precipitate neodymium {and Plutonium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Pu-242 were calculated by comparison to Pu-239 certified values. dpm/ml 43.8311 1.9502 4.2520 Pass 97.01% .Pass
' j I ' .-i
D ! *' : Eckert & Ziegler Analytics CERTIFICATE OF CALIBRATION Standard Radionuclide Source 78148-278 Th-230 6 mL Liquid in Flame Sealed Vial Customer: General Engineerings Labs P.O. No.: 7311RD, Item l 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com This standard radionuclide source was prepared gravimetrically from a calibrated master solution. The master solution was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and assay date for this source are given below. ANALYTICS maintains traceability to the National Institute of Standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision 1. Isotope: Activity (Bq): Half-Life: Calibration Date: Relative Expanded Uncertainty (k=2): Comments: Impurities: y-impurities <0.1 %, a-impurities <0.04% 5.07467 grams 0.5M HN03 solution. ---Source Prepared By: #q M. I. Taskaeva, Radiochemist QA Approved: D. Th-230 4.021 E4 7 .538 E4 years August 25, 2008 12:00EST 2.0% Date: End of Certificate 988 of 5809 Cornorate Office I .:ahnr:1f'1uu Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Thorium-230 Parent Code: 1242 Prepared By: Ashley Drochter Prepared By: Daniel Roy Prep Date: 11/10/2009 Carrier Cone: 0.5MHN03 Verification Date: 06/24/2015 Reference Date: 08/25/2008 Expiration Date: 06/24/2016 Ampoule Mass (g): 5.07467 g Primary Code: 1242-A Uncertainty: +/-2 % Dilution(mL): lOOmL LogBookNo: RC-S-048-123 Mass of Parent(g): 4.8836 g Density(g/mL): 1.0597 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLJdpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (4.8836 g) * (40210 Bq) * (60 dpm/Bq) I (5.07467 g

100 mL) = 23217.6149 dpm/mL (4.8836 g) * (40210 Bq) * (60 dpm/Bq) I ( 1.0597 g/mL)/ (5.07467 g

100 mL) = 21908.6601 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone dpm/mL Verification Expiration Primary (mL) Date Date 12/01/2009 Bethany Fiem 6.3855 500 1242-B 279.79548 12/02/2009 12/02/2010 dpm/mL 08/03/2010 Gregory 12.8745 1000 1242-C 282.063 07/30/2013 07/30/2014 -Ramsay dpm/mL 07/05/2011 Bethany Fiem 12.1975 1000 1242-D 267.2309 06/22/2012 06/22/2013 dpm/mL 01/12/2012 Christina .105 500 1242-E 4.6008 01/13/2015 01/13/2016 Kimball dpm/mL 01/08/2013 Bethany Fiem 12.5093 1000 1242-F 274.062 01/07/2014 01/07/2015 dpm/mL 08/26/2013 Christina .012512 100 1242-G 2.74129 08125/2014 08/25/2015 Kimball dpm/mL 02/17/2014 Tim Chandler .2121 100 1242-H 46.46827 02/11/2016 02/11/2017 dpm/mL 08/11/2014 Gregory 6.16 500 1242-I 269.9147 08/06/2015 08/06/2016 Ramsay dpm/mL Page 1989of5809 GEL Laboratories LLC Version 1.0 9/18/2000 Page 1990 of 5809
(!) -\0 \0 -0 1-+i VI 00 0 \0 Verification for Th-230 Standard 1242-H v1.0.2 Instrument GREEN Analyst TC1 Verification Prep Date 2/11/2016 Standard Information Quench Gross Bkg dpm/ml 46.36 1.369658179 Isotope Serial Number lsotooe Halflife Reference Date Ref. Act. (DPM/ml) Amount of Std. CmU Standard Prep Date Th-230 Std# Count Date 1242-H 1 2/11/2016 7.5380E+04 Y 2 2/11/2016 8/25/2008 3 2/11/2016 46.46827 1.0 Net 11/10/2009 Std# cpm 1 47.72 2 45.42 3 47.92 Verification Rules Number cpm 117.00 95.32 117.00 93.02 117.00 95.52 Calculated Standard Avg. Eff. dpm/ml 1.014300 47.05 1.014300 44.78 1.014300 47.24 cpm 47.60 47.60 47.60 Measured dpm 47.05 44.78 47.24 Mean Value= Stdev= Certificate Value*= Two sigma= 10 %of Mean= Rule A (Pass/Fail) % Recovery Rule B (Pass/Fail) Expiration Date Rule A =The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value.
Certificate Value is decay corrected to Count Date. 46.5 2.739 4.636 Pass 99.77% Pass 2111/2017 The analyst prepared three standard verification sources for Th-230 source 1242-H by transferring t ml portions of the standard into glass liquid scintillation vials. 15 ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 15 ml of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and background source were dark adapted for at least two hours and counted on lSCGREEN for Th-230 source standard verification. The Th-230 efficiency calibration which was used for verification calculations was performed on 2/11/2016 using Th-230 source 1493-A. Standard results for each verification source was calculated as follows: RAD-M-001 Source dprn/ml = (A -B)/(C)(D) where: A = 8 = c = D Ver. source cpm, BKGcpm, System efficiency (cpm/dpm), and volume used for standard verification.
! Eckert & Ziegler Analytics CERTIFICATE OF CAUBRATION Standard Radionuclide Source 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352 .. 8677 Fax 404*352*2837 www.an a lyticsinc .. :o m 85621-278 5 mL Liquid in Flame Sealed Vial Customer: P.O. No.: General Engineering Labs/Charleston, SC 936814RD, Item 1 This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by the Department Des Applications Et De La Metrologie Des Rayonnements Ionisants (DAMRI), Paris, France. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February, 1979, and compliance*with ANSI N42.22-1996, "Traceability ofRadioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in accordance with the HPS accreditation requirements. Customers may report any concerns with the accreditation program tc* the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101. Isotope U-232 Half-Life, Days 2.517E+04 Activity (Bq) 3.393E+04 Uncertainty* , % Type u 0.5 2.4 4.9 Reference Date (12:00 PM EST) 09/12/2011 *Uncertainty: U -Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating an:l Expressin9 the Uncertainty of NIST Measurement Results." Comments: Impurities: y-impurities (other than decay products)< 0.1 %, U-233 < l.20E2 Bq, Arn-241 < 5.BEI Bq. 5.06048 grams 2M HN03 _.-.-Source Prepared by: 1 .t?e O-M. I. Taskaeva, Radiochemist ]. D. McCorvey, QA Manager Alternate Date: --* QA Approved: Single Isotope Certificate, Rev 1 9/28/2009 Corporate Office Laboratory Page 1992 Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30:118 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Uranium-232 Parent Code: 1564 Prepared By: Ashley Drochter Prepared By: Ashley Drochter Prep Date: 11/15/2012 Carrier Cone: 2MHN03 Verification Date: 09/21/2016 Reference Date: 09/12/2011 Expiration Date: 09/2112017 Ampoule Mass (g): 5.06048 g Primary Code: 1564-A Uncertainty: +/-2.45 % Dilution( mL): lOOmL LogBookNo: RC-S-060-109 Mass of Parent(g): 4.9067 g Density(g/mL): 1.0615 Bahmce ID: 38080204 Calculations Converting parent activity to dpm/mLJdpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) * (conversion dpm to Bq) I Density I (Ampoule Mass (g) * (Dilution Vol))= Parent Activity (dpm/g) (4.9067 g) * (33930 Bq) * (60 dpm/Bq) I (5.06048 g
100 mL) = 19739.3525 dpm/mL (4.9067 g) * (33930 Bq) * (60 dpm/Bq) I ( 1.0615 g/mL)/ (5.06048 g

100 mL) = 18595.7160 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone Verification Expiration Primary (mL) dpm/mL Date Date 11/16/2012 Ashley 2.6179 1000 1564-B 48.6817 11/13/2013 11/13/2014 Drochter dpm/mL 01/15/2013 Christina .265 250 1564-C 19.7115 01/13/2014 01/13/2015 Kimball dpm/mL 02/18/2013 Christina .116 500 1564-D 4.31421 02/16/2015 02/13/2016 Kimball dpm/mL 01/02/2014 Gregory 2.6936 1000 1564-E 50.08942 12/10/2014 12/10/2015 Ramsay dpm/mL 03/17/2014 Christina .266 250 1564-F 19.78584 03/25/2015 03/25/2016 Kimball dpm/mL 12/10/2014 Tim Chandler 2.6312 1000 1564-G 48.929 12/10/2014 12/10/2015 dpm/mL 07/20/2015 Christina .266 250 1564-H 19.78584 07/25/2016 07/25/2017 Kimball dpm/mL 11/23/2015 Tim Chandler 2.6117 1000 1564-1 48.5664 11/23/2015 11/23/2016 dpm/mL Page 1993 of 5809 01/05/2016 Christina Kimball 0912012016 Tim Chandler GEL Laboratories LLC Version 1.0 9/18/2000 Page 1994of5809 .119 2.6389 500 1564-J 4.4258 01/05/2016 01/05/2017 dpm/mL 1000 1564-K 49.0722 09/2112016 09/21/2017 dpm/mL Verification for U-23.2 Standard 1564-1 v1.2 Analyst TC1 Tracer Information *. *:o*.:o-:" .. -:::::,,* 0cverification*:prepcDate**" .: ... -::.:.:*.1**1123/2015 :;.-.... =* ......... * .. ,,,,_: :-'.*.-. .. -: .. ::::: ... *.*U-238: .. ::.::*:.:. * ....... : :.:.-:::_ .. : .. ::.: .. -.... :c .. *-... ::.::,: . .-0:: .. .-*. .. :.:c-;:.: ... .--..:.:*.;:.:.:.-:-::::: .. :.:::.= .. :"-=.:,:::.'-:.==.::::::.:.:::::.:=c.:*.::: Serial Number 1600-E Amount of Std. (ml) 0.5 Expiration Date 7/24/2016 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dpm/ml) Amount of Std. (mL) Standard Prep Date U-232 1564-1 68.9000 y 9/12/2011 48.5664 0.5 11/23/2015 Verification Rules Std# 1 2 3 Count Date 11/23/2015 11/23/2015 11/23/2015 Mean Value= Stdev= pCI dpm/mL Certificate Value* = 10.4861 10.100 44.84 Two sigma= 0.5774 10.600 47.06 10 % of Mean= 1.0433 10.600 47.06 Rule A (Pass/Fail) Pass % Recovery 99.50% 10.433 46.324 Rule B (Pass/Fail) Pass 0.288675135 1.281717598 Expiration Date 11/23/2016 Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value. *Certificate Value is decay corrected Verification Prep Date. The analyst prepared three standard verification sources for U-232 standard 1564-1 using 0.5 ml for each source. Each standard was combined with 0.5 mL of U-238 standard 1600-E and was diluted in a 50 ml plastic centrifuge tube containing 15 ml of 1 M HCI, 1 ml of TiCl3. 100 micrograms of neodymium carrier and five mL of 48% HF was added to precipitate neodymium (and Uranium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for U-232 were calculated by comparison to U-238 certified values. dpm/mL 46.5584 2.5634 4.6324 Pass 99.50% Pass
-. _. Eckert & Ziegler Isotope Products 24937 Avenue Tibbitts Valencia, California 91355 Tel 661*309*1010 Fax 661 *257*8303 IS10 CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION Radionuclide: U-236 Customer: Half-life: (2.342 +/- 0.003)E+07 years P.O. No.: Catalog No.: 7336 Source No.: 1555-47 Physical
Description:
A. Mass of solution: 8. Chemical form: C. Carrier content: D. Density: Radioimpurities: See Technical Data Sheet Radionuclide Concentration: Method of Calibration: 20.07 Reference Date: Contained Radioactivity: 5.00824 g in 5 ml flame-sealed ampoule U02(N03h in 0.1 M HN03 None 1.0016 g/ml@2d°C nCi/g, 742.6 Bq/g GENERAL ENGINEERING LABS. 936817RD 15-Nov-11 12:00 PST 100.5 nCi 3719 Bq This source was prepared from a weighed aliquot of solution whose activity in µCi/g was determined using a liquid scintillation counter. -4' Uncertainty of Measurement: A. Type A (random) uncertainty: +/- 1.3 % 8. Type B (systematic) uncertainty: +/- 3.0 % f . C. Uncertainty in aliquot weighing: +/- 0.1 % D. Total uncertainty at the 99% confidence level: +/- 3.3 % ... Notes: -See reverse side for leak test(s) performed on this source. -EZIP participates in a NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference !"laterials (as in NRC Regulatory Guide 4.15). . -Nuclear data was taken from "Table of Radioactive Isotopes", edited by Virginia Shirley, 1986. -This solution has a working life of 5 years. ll/-Oc.T-I I Date EZIP Re.f. No.: 1555-47 tl,..'(;-OfP 0-11 ----------------....---1509001 CERTIFIED------...,_:-.....;;.....----.........::----Medical Imaging Laboratory Industrial Gauging Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank, California 91504 a e 1996 of 5809 § Eckert & Ziegler Isotope Products 24937 Avenue Tibbitts Valencia, California 91355 Tel 661*309*1010 Fax 661*257*8303 U-236 Technical Data The U-236 used to prepare your order was taken from Isotope Products Laboratories Lot #30130.01 and had the following composition as of 8 Jul 05: Nuclide U-235 U-236 U-238 Mass% 0.046 99.657 0.297 Activity% 0.0015 99.997 0.0015 Isotopic composition provided by Techsnabexport Co. Ltd. If you have any question, please cpntact IPL Technical Service: (661) 309-1010. -----'--------------ISO 9001 CERTIFIED ---------'-.:::>1<..-=-__;;...;;;;...._--:...=..==-.. Ml!dical Imaging Laboratory 24937 Avenue Tibbitts Valencia, California 91355 a e 1997 of 5809. _ . . . . Industrial Gauging Laboratory 1800 North Keystone Street Burbank, California 91504 't Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Uranium-236 Parent Code: 1570 Prepared By: Jesse Craig Prepared By: Ashley Drochter Prep Date: 10/31/2011 Carrier Cone: 0.1MHN03 Verification Date: 10/03/2016 Reference Date: 11/15/2011 Expiration Date: 10/03/2017 Ampoule Mass (g): 5.00824 g Primary Code: 1570-A Uncertainty: +/-1.289 % Dilution(mL): lOOmL LogBookNo: RC-S-060-115 Mass of Parent(g): 4.852 g Density(g/mL): 0.9993 Balance ID: 1113021018 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq/g)) *(conversion dpm to Bq) I (Dilution Vol)= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq/g)) *(conversion dpm to Bq) I Density (g/mL)/ (Dilution Vol)= Parent Activity (dpm/g) (4.852 g) * (742.6 Bq/g) * (60 dpm/Bq) I (100 mL) = 2161.8571 dprn/mL (4.852 g) * (742.6 Bq/g) * (60 dpm/Bq) I ( 0.9993 g/mL) I (100 mL) = 2163.3715 dprn/g Secondary Standards Prep Date Preparer Mass Dilution code Cone Verification Expiration Primary (mL) dpm/mL Date Date 11/29/2011 Ashley 10.2782 200 1570-B 111.1778 11/13/2013 11/13/2014 Drochter dprn/mL 03/06/2012 Christina .2059854 100 1570-C 4.4562 02/19/2016 02/19/2017 Kimball dprn/mL 03/27/2014 Tim 5.0353 100 1570-D 108.9322 03/18/2015 03/18/2016 Chandler dprn/mL 07/24/2015 Tim 5.1415 100 1570-E 111.2297 07/18/2016 07/18/2017 Chandler dprn/mL 10/03/2016 Tim 12.8711 250 1570-F 111.3799 10/03/2016 10/03/2017 Chandler dprn/mL 10/31/2011 Paul Boyd 6.64 10 IMSl21016-0l 10 mg/L 07/28/2016 07/28/2017 10/16/2012 Paul Boyd .05 50 WMS121016-100 10 ug/L 10/17/2011 10/17/2012 11/10/2012 Paul Boyd .05 50 WMSl211 I0-100 10 ug/L 11/11/2011 11/11/2012 11/10/2012 Paul Boyd 5 50 WMS121110-100a 1 ug/L 11/11/2011 11/1112012 11/10/2012 Paul Boyd .025 50 WMSl21110-104 5ug/L 11/11/2011 11/11/2012 11/11/2012 Paul Boyd .05 50 WMS1211l1-100 10 ug/L 11/12/2011 11/12/2012 Page 1998of5809 11111/2012 Paul Boyd 5 50 \Vl\1Sl21111-100a 1 ug/L 11112/2011 11/12/2012 11/1112012 Paul Boyd .025 50 \Vl\1Sl21111-104 5ug/L 11112/2011 11/12/2012 11112/2012 Paul Boyd .05 50 \Vl\1S 121112-100 10 ug/L 11/13/2011 11/13/2012 11/12/2012 Paul Boyd 5 50 \Vl\1S121112-100a 1 ug/L 11113/2011 11113/2012 11112/2012 Paul Boyd .025 50 \Vl\1S121112-104 5 ug/L 11113/2011 11113/2012 11113/2012 Paul Boyd .05 50 \Vl\1Sl21113-100 10 ug/L 11/14/2011 11114/2012 11113/2012 Paul Boyd 5 50 \Vl\1Sl21113-100a 1 ug/L 11114/2011 11114/2012 11113/2012 Paul Boyd .025 50 \Vl\1S 121113-104 5 ug/L 11114/2011 11114/2012 11114/2012 Paul Boyd .05 50 \Vl\1Sl21114-100 10 ug/L 11115/2011 11/15/2012 11114/2012 Paul Boyd 5 50 \Vl\1Sl21114-100a 1 ug/L 11115/2011 11115/2012 11114/2012 Paul Boyd .025 50 \Vl\1Sl21114-104 5 ug/L 11115/2011 11/15/2012 11115/2012 Paul Boyd .05 50 \Vl\1Sl21115-100 10 ug/L 11116/2011 11116/2012 11115/2012 Paul Boyd 5 50 \Vl\1Sl21115-100a 1 ug/L 11/16/2011 11116/2012 11/15/2012 Paul Boyd .025 50 \Vl\1Sl21l15-104 5 ug/L 11/16/2011 11116/2012 11/16/2012 Paul Boyd .05 50 \Vl\1Sl21116-100 10 ug/L 11/17/2011 11117/2012 11/16/2012 Paul Boyd 5 50 \Vl\1Sl21116-100a 1 ug/L 11117/2011 11/17/2012 11116/2012 Paul Boyd .025 50 \Vl\1Sl21l16-104 5ug/L 11117/2011 11117/2012 11117/2012 Paul Boyd .05 50 \Vl\1Sl21117-100 10 ug/L 11118/2011 11/18/2012 11117/2012 Paul Boyd 5 50 \Vl\1Sl21117-100a 1 ug/L 11118/2011 11/18/2012 11117/2012 Paul Boyd .025 50 \Vl\1Sl21117-104 5ug/L 11118/2011 11/18/2012 11118/2012 Paul Boyd .05 50 \Vl\1Sl21118-100 10 ug/L 11119/2011 11/19/2012 11118/2012 Paul Boyd 5 50 \Vl\1Sl21118-100a 1 ug/L 11119/2011 11119/2012 11118/2012 Paul Boyd .025 50 \Vl\1Sl21118-104 5ug/L 11119/2011 11/19/2012 11/19/2012 Paul Boyd .05 50 \Vl\1Sl21119-100 10 ug/L 11120/2011 11120/2012 11/19/2012 Paul Boyd 5 50 \Vl\1Sl21119-100a 1 ug/L 11120/2011 11120/2012 11/19/2012 Paul Boyd .025 50 \Vl\1S 121119-104 5ug/L 11120/2011 11120/2012 11/20/2012 Paul Boyd .05 50 \Vl\1Sl21120-100 10 ug/L 11121/2011 11121/2012 11/20/2012 Paul Boyd 5 50 \Vl\1Sl21120-100a 1 ug/L 1112112011 11121/2012 11/20/2012 Paul Boyd .025 50 \Vl\1S121120-104 5ug/L 11121/2011 1 l/21/2012 12/3112012 Elizabeth .05 .50 \Vl\1Sl21231-100 10 ug/L 01101/2012 01101/2013 Janssen 12/3112012 Elizabeth 5 50 \Vl\1Sl21231-100a 1 ug/L 0110112012 0110112013 Janssen 12/3112012 Elizabeth .025 50 \Vl\1Sl21231-104 5ug/L 0110112012 01/01/2013 Janssen Ol/03/2013 Elizabeth .05 50 \Vl\1Sl30103-100 10 ug/L 01/04/2012 01104/2013 Janssen 01103/2013 Elizabeth 5 50 \Vl\1Sl30103-100a 1 ug/L 01104/2012 01/04/2013 Janssen Page 1999of5809 01/03/2013 Elizabeth .025 50 WMS130103-104 5ug/L 01/04/2012 01104/2013 Janssen 01107/2013 Paul Boyd .05 50 WMS130107-100 10 ug/L 01108/2012 01/08/2013 01107/2013 Paul Boyd 5 50 WMS130107-100a 1 ug/L 01108/2012 01/08/2013 01107/2013 Paul Boyd .025 50 WMS130107-104 5ug/L 01/08/2012 01/08/2013 01/08/2013 Paul Boyd .05 50 WMS130108-100 10 ug/L 01/09/2012 01/09/2013 01/08/2013 Paul Boyd 5 50 WMS130108-100a 1 ug/L 01/09/2012 01/09/2013 01/08/2013 Paul Boyd .025 50 WMS130108-104 5ug/L 01/09/2012 01/09/2013 01109/2013 Paul Boyd .05 50 WMS 130109-100 10 ug/L 01110/2012 01110/2013 01/09/2013 Paul Boyd 5 50 WMS 130109-lOOa 1 ug/L 01110/2012 01110/2013 01109/2013 Paul Boyd .025 50 WMS 130109-104 5ug/L 01/10/2012 01/10/2013 01110/2013 Paul Boyd .05 50 WMS130110-100 10 ug/L 01111/2012 0111112013 01/10/2013 Paul Boyd 5 50 WMS130110-100a 1 ug/L 01111/2012 01/1112013 01/10/2013 Paul Boyd .025 50 WMS130110-104 5ug/L 01/11/2012 01/1112013 02/05/2013 Paul Boyd .05 50 WMS130205-100 10 ug/L 02/06/2012 02/06/2013 02/05/2013 Paul Boyd 5 50 WMS130205-100a 1 ug/L 02/06/2012 02/06/2013 02/05/2013 Paul Boyd .025 50 WMS130205-104 5 ug/L 02/06/2012 02/06/2013 02/06/2013 Paul Boyd .05 50 WMS 130206-100 10 ug/L 02/07/2012 02/07/2013 02/06/2013 Paul Boyd 5 50 WMS130206-100a 1 ug/L 02/07/2012 02/07/2013 02/06/2013 Paul Boyd .025 50 WMS130206-104 5ug/L 02/07/2012 02/07/2013 02/25/2013 Paul Boyd .05 50 WMS 130225-100 10 ug/L 02/26/2012 02/26/2013 02/25/2013 Paul Boyd 5 50 WMS130225-100a 1 ug/L 02/26/2012 02/26/2013 02/25/2013 Paul Boyd .025 50 WMS130225-104 5 ug/L 02/26/2012 02/26/2013 04/03/2013 Paul Boyd .05 50 WMS130403-100 10 ug/L 04/04/2012 04/04/2013 04/03/2013 Paul Boyd 5 50 WMS130403-100a l ug/L 04/04/2012 04/04/2013 04/03/2013 Paul Boyd .025 50 WMS130403-104 5ug/L 04/04/2012 04/04/2013 04/05/2013 Elizabeth .05 50 WMS130405-100 10 ug/L 04/06/2012 04/06/2013 Janssen 04/05/2013 Elizabeth 5 50 WMS130405-100a 1 ug/L 04/06/2012 04/06/2013 Janssen 04/05/2013 Elizabeth .025 50 WMS130405-104 5ug/L 04/06/2012 04/06/2013 Janssen 04/09/2013 Paul Boyd .05 50 WMS 130409-100 10 ug/L 04/10/2012 04/10/2013 04/09/2013 Paul Boyd 5 50 WMS130409-100a 1 ug/L 04/10/2012 04/10/2013 04/09/2013 Paul Boyd .025 50 WMS 130409-104 5ug/L 04/10/2012 04/10/2013 04/10/2013 Paul Boyd .05 50 WMS 130410-100 10 ug/L 04/11/2012 04/11/2013 04/10/2013 Paul Boyd 5 50 WMS 130410-1 OOa 1 ug/L 04/11/2012 04/1112013 04/10/2013 Paul Boyd .025 50 WMS130410-104 5ug/L 04/11/2012 04/11/2013 04/11/2013 Paul Boyd .05 50 WMS130411-100 10 ug/L 04/12/2012 04/12/2013 Page 2000 of 5809 04/11/2013 Paul Boyd 5 50 \Vl\18130411-IOOa I ug/L 04/12/2012 04/12/2013 04/11/2013 Paul Boyd .025 50 \Vl\1813 04 l l -I04 5ug/L 04/1212012 04/12/2013 04/15/2013 Paul Boyd .05 50 \Vl\18130415-IOO IO ug/L 04/I6/20I2 04/16/2013 04/15/2013 Paul Boyd 5 50 \Vl'v18I304I5-IOOa I ug/L 04/I6/20I2 04/16/2013 04/15/2013 Paul Boyd .025 50 \Vl\18130415-I 04 5ug/L 04/I6/20I2 04/16/2013 04/I6/2013 Paul Boyd .05 50 \Vl\181304 I 6-IOO IO ug/L 04/I7/20I2 04/I7/2013 04/I6/20I3 Paul Boyd 5 50 \Vl\18I30416-I00a I ug/L 04/I7/2012 04/17/2013 04/16/2013 Paul Boyd .025 50 \Vl\1813 04 I 6-I04 5ug/L 04/I7/20I2 04/17/2013 04/17/2013 Paul Boyd .05 50 \Vl\181304 I 7-IOO 10 ug/L 04/I8/20I2 04/I8/2013 04/17/2013 Paul Boyd 5 50 \Vl\18130417-IOOa I ug/L 04/18/20I2 04/18/2013 04/17/2013 Paul Boyd .025 50 \Vl\181304 I 7-I04 5ug/L 04/18/2012 04/18/2013 05/28/2013 Paul Boyd .05 50 \Vl\18130528-IOO IO ug/L 05/29/2012 05/29/2013 05/28/2013 Paul Boyd 5 50 \Vl\18130528-IOOa 1 ug/L 05/2912012 05/29/2013 05/28/2013 Paul Boyd .025 50 \Vl\18130528-104 5ug/L 05/2912012 05/29/2013 05/29/2013 Paul Boyd .05 50 \Vl\18130529-100 IO ug/L 05/30/2012 05/30/2013 05/29/2013 Paul Boyd 5 50 \Vl\18130529-IOOa I ug/L 05/3012012 05/30/2013 05/29/2013 Paul Boyd .025 50 \Vl\18130529-I04 5ug/L 05/3012012 05/30/2013 07/08/2013 Elizabeth .05 50 \Vl\18130708-IOO IO ug/L 07/0912012 07/09/2013 Janssen 07/08/2013 Elizabeth 5 50 \Vl\18130708-IOOa I ug/L 07/09/2012 07/09/2013 Janssen 07/08/2013 Elizabeth .025 50 \Vl\1813 0708-I04 5ug/L 07/09/2012 07/09/2013 Janssen 07/10/2013 Elizabeth .05 50 \Vl\1813 0710-IOO IO ug/L 07/11/2012 07/11/2013 Janssen 07/I0/2013 Elizabeth 5 50 \Vl\18130710-IOOa I ug/L 07111/2012 07111/2013 Janssen 07/I0/2013 Elizabeth .025 50 \Vl\1813 07 IO-I04 5ug/L 07/11/2012 07/11/2013 Janssen 07111/2013 Paul Boyd .05 50 \Vl\1813 0711-IOO 10 ug/L 07/12/2012 07/12/2013 07/11/2013 Paul Boyd 5 50 \Vl\18130711-IOOa 1 ug/L 07/12/2012 07/12/2013 07/11/2013 Paul Boyd .025 50 \Vl'v1813071 l-I04 5ug/L 07/1212012 07/12/2013 08/01/2013 Paul Boyd .05 50 \Vl\18130801-100 IO ug/L 08/02/2012 08/02/2013 08/01/2013 Paul Boyd 5 50 \Vl'v18I30801-100a I ug/L 08/02/2012 08/02/2013 08/01/2013 Paul Boyd .025 50 \Vl'v18130801-I04 5 ug/L 08/0212012 08/02/2013 I0/11/2013 Paul Boyd .05 50 \Vl\181310 l I-IOO IO ug/L 10/12/20I2 I0/12/2013 10/I 112013 Paul Boyd 5 50 \Vl'v18I31011-IOOa I ug/L 10/12/2012 10/12/2013 I0/11/2013 Paul Boyd .025 50 \Vl\18 13 IO 11-I 04 5 ug/L I0/12/2012 IO/I2/2013 I0/14/2013 Paul Boyd .05 50 \Vl\1813 IO 14-100 IO ug/L 10/15/20I2 I0/15/2013 I0/14/2013 Paul Boyd 5 50 \Vl'v18I31014-100a I ug/L I0/15/20I2 I0/15/2013 Page 2001 of 5809 10/14/2013 Paul Boyd .025 50 WMS 131014-104 5 ug/L 10/15/2012 10/15/2013 10/15/2013 Paul Boyd .05 50 WMS131015-IOO IO ug/L 10/16/2012 10/16/2013 10/15/2013 Paul Boyd 5 50 WMS131015-100a 1 ug/L 10/16/2012 10/16/2013 I0/15/2013 Paul Boyd .025 50 WMS131015-104 5ug/L 10/16/2012 10/16/2013 10/16/2013 Paul Boyd .05 50 WMS 131016-IOO 10 ug/L I0/17/2012 10/17/2013 I0/16/2013 Paul Boyd 5 50 WMS131016-100a 1 ug/L I0/17/2012 10/17/2013 10/16/2013 Paul Boyd .025 50 WMS131016-I04 5ug/L 10/17/2012 .10/17/2013 10/17/2013 Paul Boyd .05 50 WMS 131017-100 IO ug/L I0/18/2012 I0/18/2013 10/17/2013 Paul Boyd 5 50 WMS131017-100a 1 ug/L 10/18/2012 I0/18/2013 10/17/2013 Paul Boyd .025 50 WMS131017-104 5 ug/L 10/18/2012 I0/18/2013 11105/2013 Paul Boyd .05 50 WMS131105-IOO 10 ug/L 11106/2012 11/06/2013 11/05/2013 Paul Boyd 5 50 WMS131105-100a 1 ug/L 11/06/2012 11/06/2013 11/05/2013 Paul Boyd .025 50 WMS 131105-104 5ug/L 1110612012 11/06/2013 1110612013 Paul Boyd .05 50 WMS 131106-IOO 10 ug/L 11/07/2012 11107/2013 11106/2013 Paul Boyd 5 50 WMS131106-100a 1 ug/L 11/07/2012 11107/2013 11/06/2013 Paul Boyd .025 50 WMS 131106-104 5 ug/L 11107/2012 11107/2013 12117/2013 Paul Boyd .05 50 WMS131217-100 IO ug/L 12/18/2012 12/18/2013 12/17/2013 Paul Boyd 5 50 WMS131217-100a 1 ug/L 12/18/2012 12/18/2013 12/17/2013 Paul Boyd .025 50 WMS131217-104 5 ug/L 12/18/2012 12/18/2013 01/08/2014 Paul Boyd .05 50 WMS140108-IOO 10 ug/L 0110912013 01/09/2014 01108/2014 Paul Boyd 5 50 WMS140108-100a 1 ug/L 0110912013 01/09/2014 01108/2014 Paul Boyd .025 50 WMS140108-I04 5ug/L 01/09/2013 0110912014 01109/2014 Paul Boyd .05 50 WMS140109-100 10 ug/L 01/10/2013 01110/2014 0110912014 Paul Boyd 5 50 WMS140109-100a 1 ug/L 01/10/2013 01110/2014 01/09/2014 Paul Boyd .025 50 WMS 140109-104 5 ug/L 01/10/2013 01110/2014 01/10/2014 Paul Boyd .05 50 WMS140110-IOO 10 ug/L 01110/2013 01110/2014 01/I0/2014 Paul Boyd 5 50 WMS 140110-IOOa 1 ug/L 01110/2013 01110/2014 01/10/2014 Paul Boyd .025 50 WMS140110-104 5 ug/L 01110/2013 Ol/I0/2014 01/14/2014 Paul Boyd .05 50 WMS140114-100 IO ug/L 0111512013 01115/2014 01/14/2014 Paul Boyd 5 50 WMS140114-100a 1 ug/L 01115/2013 01/15/2014 01/14/2014 Paul Boyd .025 50 WMS140114-104 5ug/L 01115/2013 01/15/2014 01115/2014 Paul Boyd .05 50 WMS140115-100 10 ug/L 01116/2013 01/16/2014 01115/2014 Paul Boyd 5 50 WMS140115-100a 1 ug/L 0111612013 01/16/2014 01115/2014 Paul Boyd .025 50 WMS140115-104 5ug/L 01116/2013 01/16/2014 01/16/2014 Paul Boyd .05 50 WMS140116-IOO 10 ug/L 01117/2013 01/17/2014 01116/2014 Paul Boyd 5 50 WMS1401J6-100a 1 ug/L 01/17/2013 0111712014 01/16/2014 Paul Boyd .025 50 WMS140116-104 5ug/L 01/17/2013 01/17/2014 01117/2014 Paul Boyd .05 50 WMS140117-100 10 ug/L Ol/18/2013 01118/2014 Page 2002 of 5809 01117/2014 Paul Boyd 5 50 Wl\1S140117-100a 1 ug/L 01118/2013 01/18/2014 01117/2014 Paul Boyd .025 50 Wl\1S140117-104 5 ug/L 01118/2013 01/18/2014 01/28/2014 Paul Boyd .05 50 Wl\1Sl40128-100 10 ug/L 01129/2013 01/29/2014 01/28/2014 Paul Boyd 5 50 Wl\1Sl40128-100a 1 ug/L 01129/2013 01/29/2014 01/28/2014 Paul Boyd .025 50 Wl\1Sl40128-104 5 ug/L 01/29/2013 01/29/2014 01/30/2014 Paul Boyd .05 50 Wl\1S140130-100 10 ug/L 01/31/2013 0113112014 01130/2014 Paul Boyd 5 50 Wl\1Sl40130-100a 1 ug/L 01/3112013 0113112014 01130/2014 Paul Boyd .025 50 Wl\1S140130-104 5 ug/L 0113112013 0113112014 0113112014 Paul Boyd .05 50 Wl\1S 140131-100 10 ug/L 02/0112013 02/0112014 01/3112014 Paul Boyd 5 50 Wl\1Sl40131-100a 1 ug/L 02/0112013 02/0112014 0113112014 Paul Boyd .025 50 Wl\1S 140131-104 5 ug/L 02/0112013 02/01/2014 02/03/2014 Paul Boyd .05 50 Wl\1Sl40203-100 10 ug/L 02/04/2013 02/04/2014 02/03/2014 Paul Boyd 5 50 Wl\1S140203-100a 1 ug/L 02/04/2013 02/04/2014 02/03/2014 Paul Boyd .025 50 Wl\1Sl40203-104 5 ug/L 02/04/2013 02/04/2014 02/21/2014 Paul Boyd .05 50 Wl\1S 140221-100 10 ug/L 02/22/2013 02/22/2014 02/2112014 Paul Boyd 5 50 Wl\1Sl40221-100a 1 ug/L 02/22/2013 02/22/2014 02/2112014 Paul Boyd .025 50 Wl\1S 5 ug/L 02/22/2013 02/22/2014 02/24/2014 Paul Boyd .05 50 Wl\1S 140224-100 10 ug/L 02/25/2013 02/25/20.14 02/24/2014 Paul Boyd 5 50 Wl\1Sl40224-100a 1 ug/L 02/25/2013 02/25/2014 02/24/2014 Paul Boyd .025 50 Wl\18140224-104 5ug/L 02/25/2013 02/25/2014 04/07/2014 Paul Boyd .05 50 Wl\1S 140407-100 10 ug/L 04/08/2013 04/08/2014 04/07/2014 Paul Boyd 5 50 Wl\1Sl40407-100a 1 ug/L 04/08/2013 04/08/2014 04/07/2014 Paul Boyd .025 50 Wl\1Sl40407-104 5ug/L 04/08/2013 04/08/2014 04/08/2014 Paul Boyd .05 50 Wl\1S 140408-100 10 ug/L 04/09/2013 04/09/2014 04/08/2014 Paul Boyd 5 50 Wl\1Sl40408-100a 1 ug/L 04/09/2013 04/09/2014 04/08/2014 Paul Boyd .025 50 Wl\1S 140408-104 5ug/L 04/09/2013 04/09/2014 04/09/2014 Paul Boyd .05 50 Wl\1S 140409-100 10 ug/L 04/10/2013 04/10/2014 04/09/2014 Paul Boyd 5 50 Wl\1Sl40409-100a 1 ug/L 04/10/2013 04/10/2014 04/09/2014 Paul Boyd .025 50 Wl\1S 140409-104 5ug/L 04/10/2013 04/10/2014 04/10/2014 Paul Boyd .05 50 Wl\1S 140410-100 10 ug/L 04/11/2013 04/11/2014 04/10/2014 Paul Boyd 5 50 Wl\1S 140410-1 OOa 1 ug/L 04/11/2013 04/11/2014 04/10/2014 Paul Boyd .025 50 Wl\1S 140410-104 5 ug/L 04/11/2013 04/11/2014 04/1112014 Paul Boyd .05 50 Wl\1Sl40411-100 10 ug/L 04/12/2013 04/12/2014 04/1112014 Paul Boyd 5 50 Wl\1Sl40411-100a 1 ug/L 04/12/2013 04/12/2014 04/11/2014 Paul Boyd .025 50 Wl\1S 140411-104 5ug/L 04/12/2013 04/12/2014 04/14/2014 Paul Boyd .Q5 50 Wl\1S 140414-100 10 ug/L 04/15/2013 04/15/2014 04/14/2014 Paul Boyd 5 50 Wl\1S140414-100a 1 ug/L 04/15/2013 04/15/2014 04/14/2014 P<!ul Boyd .025 50 Wl\1S 140414-104 5ug/L 04/15/2013 04/15/2014 Page 2003 of 5809 04/15/2014 Paul Boyd .05 50 WMS140415-100 10 ug/L 04/16/2013 04/16/2014 04/15/2014 Paul Boyd 5 50 WMS140415-100a 1 ug/L 04/16/2013 04/16/2014 04/15/2014 Paul Boyd .025 50 WMS140415-104 5ug/L 04/16/2013 04/16/2014 04/16/2014 Paul Boyd .05 50 WMS140416-100 10 ug/L 04/17/2013 04/17/2014 04/16/2014 Paul Boyd 5 50 WMS140416-100a 1 ug/L 04/17/2013 04/17/2014 04/16/2014 Paul Boyd .025 50 WMS140416-104 5ug/L 04/17/2013 04/17/2014 04/17/2014 Paul Boyd .05 50 WMS140417-100 10 ug/L 04/18/2013 04/18/2014 04/17/2014 Paul Boyd 5 50 WMS140417-100a 1 ug/L 04/18/2013 04/18/2014 04/17/2014 Paul Boyd .025 50 WMS140417-104 5ug/L 04/18/2013 04/18/2014 06/05/2014 Paul Boyd .05 50 WMS 140605-100 10 ug/L 06/06/2013 06/06/2014 06/05/2014 Paul Boyd 5 50 WMS140605-100a 1 ug/L 06/06/2013 06/06/2014 06/05/2014 Paul Boyd .025 50 WMS140605-104 5ug/L 06/06/2013 06/06/2014 06/14/2014 Paul Boyd .05 50 WMS140614-100 10 ug/L 06/15/2013 06/15/2014 06/14/2014 Paul Boyd 5 50 WMS140614-100a 1 ug/L 06/15/2013 06/15/2014 06/14/2014 Paul Boyd .025 50 WMS140614-104 5ug/L 06/15/2013 06/15/2014 06/20/2014 Paul Boyd .05 50 WMS 140620-100 10 ug/L 06/21/2013 06/21/2014 06/20/2014 Paul Boyd 5 50 WMS 140620-1 OOa 1 ug/L 06/21/2013 06/21/2014 06/20/2014 Paul Boyd .025 50 WMS140620-104 5ug/L 06/21/2013 06/21/2014 07/01/2014 Paul Boyd .05 50 WMS140701-100 10 ug/L 07/02/2013 07/02/2014 07/01/2014 Paul Boyd 5 50 WMS140701-100a 1 ug/L 07/02/2013 07/02/2014 07/01/2014 Paul Boyd .025 50 WMS140701-104 5ug/L 07/02/2013 07/02/2014 07/02/2014 Paul Boyd .05 50 WMS140702-100 10 ug/L 07/03/2013 07/03/2014 07/02/2014 Paul Boyd 5 50 WMS140702-100a 1 ug/L 07/03/2013 07/03/2014 07/02/2014 Paul Boyd .025 50 WMS 140702-104 5ug/L 07/03/2013 07/03/2014 07/03/2014 Paul Boyd .05 50 WMS140703-100 10 ug/L 07/04/2013 07/04/2014 07/03/2014 Paul Boyd 5 50 WMS140703-100a 1 ug/L 07/04/2013 07/04/2014 07/03/2014 Paul Boyd .025 50 WMS140703-104 5ug/L 07/04/2013 07/04/2014 07/05/2014 Elizabeth .05 50 WMS 140705-100 10 ug/L 07/06/2013 07/06/2014 Janssen 07/05/2014 Elizabeth 5 50 WMS140705-100a 1 ug/L 07/06/2013 07/06/2014 Janssen 07/05/2014 Elizabeth .025 50 WMS140705-104 5 ug/L 07/06/2013 07/06/2014 Janssen 07/08/2014 Elizabeth .05 50 WMS140708-100 10 ug/L 07/09/2013 07/09/2014 Janssen 07/08/2014 Elizabeth 5 50 WMS140708-100a 1 ug/L 07/09/2013 07/09/2014 Janssen 07/09/2014 Bryan 5 50 WMS 140709-1 OOa 1 ug/L 07/09/2013 07/09/2014 Davis Page 2004 of 5809 07/08/2014 Elizabeth .025 50 WMSl40708-104 5ug/L 07/09/2013 07/09/2014 Janssen 07/09/2014 Bryan .05 50 WMSl40709-100 10 ug/L 07/10/2013 07/10/2014 Davis 07/09/2014 Bryan .025 50 WMSl40709-104 5ug/L 07/10/2013 07/10/2014 Davis 07110/2014 Bryan .05 50 WMSl40710-IOO 10 ug/L 07111/2013 07/11/2014 Davis 07/10/2014 Bryan .025 50 WMSl40710-104 5ug/L 07/11/2013 07111/2014 Davis 07/14/2014 Bryan .05 50 WMSl40714-100 10 ug/L 07115/2013 07/15/2014 Davis 07/14/2014 Bryan .025 50 WMS140714-104 5ug/L 07/15/2013 07/15/2014 Davis 07/15/2014 Bryan .05 50 WMS140715-100 10 ug/L 07/16/2013 07/16/2014 Davis 07/15/2014 Bryan .025 50 WMS140715-104 5ug/L 07/16/2013 07/16/2014 Davis 07/16/2014 Bryan .05 50 WMSl40716-100 10 ug/L 07/17/2013 07/17/2014 Davis 07116/2014 Bryan .025 50 WMS140716-104 5ug/L 07117/2013 07/17/2014 Davis 07/17/2014 Bryan .05 50 WMS 140717-100 10 ug/L 07118/2013 07/18/2014 Davis 07117/2014 Bryan .025 50 WMS140717-104 5ug/L 07118/2013 07/18/4014 Davis 07118/2014 Bryan .05 50 WMS140718-100 10 ug/L 07/19/2013 07/19/2014 Davis 07/18/2014 Bryan .025 50 WMS140718-104 5ug/L 07/19/2013 07/19/2014 Davis 07/19/2014 Elizabeth .05 50 WMS140719-IOO 10 ug/L 07/20/2013 07/20/2014 Janssen 07/19/2014 Elizabeth 5 50 WMSl40719-100a I ug/L 07/20/2013 07/20/2014 Janssen 07/19/2014 Elizabeth .025 50 WMSl40719-104 5 ug/L 07/20/2013 07/20/2014 Janssen 08/28/2014 Bryan .05 50 WMS 140828-100 10 ug/L 08/29/2013 08/29/2014 Davis 08/28/2014 Bryan 5 50 WMS140828-100a I ug/L 08/29/2013 08/29/2014 Davis 08/28/2014 Bryan .025 50 WMS140828-104 5ug/L 08/29/2013 08/29/2014 Davis 09/26/2014 Paul Boyd .05 50 WMS140926-100 10 ug/L 09/27/2013 09/27/2014 09/26/2014 Paul Boyd 5 50 WMS140926-100a 1 ug/L 09/27/2013 09/27/2014 09/26/2014 Paul Boyd .025 50 WMS 140926-104 5ug/L 09/27/2013 09/27/2014 Page 2005 of 5809 I0/13/2014 Samantha .05 50 WMS141013-100 IO ug/L I0/14/2013 I0/14/2014 Jacobs 10/13/2014 Samantha 5 50 WMS141013-100a 1 ug/L I0/14/2013 I0/14/2014 Jacobs I0/13/2014 Samantha .025 50 WMS141013-104 5ug/L I0/14/2013 I0/14/2014 Jacobs I0/14/2014 Samantha .05 50 WMS141014-IOO 10 ug/L I0/15/2013 10/15/2014 Jacobs 10/14/2014 Samantha 5 50 WMSl4IOl4-I00a 1 ug/L I0/15/2013 I0/15/2014 Jacobs I0/14/2014 Samantha .025 50 WMS141014-I04 5ug/L I0/15/2013 I0/15/2014 Jacobs I0/15/2014 Samantha .05 50 WMS14IOl5-IOO IO ug/L I0/16/2013 I0/16/2014 Jacobs I0/15/2014 Samantha 5 50 WMSl41015-100a 1 ug/L I0/16/2013 I0/16/2014 Jacobs 10/15/2014 Samantha .025 50 WMS14I015-104 5 ug/L I0/16/2013 I0/16/2014 Jacobs I0/16/2014 Samantha .05 50 WMS141016-IOO 10 ug/L I0/17/2013 I0/17/2014 Jacobs 10/16/2014 Samantha 5 50 WMSl4IOl6-I00a 1 ug/L I0/17/2013 10/17/2014 Jacobs I0/16/2014 Samantha .025 50 WMS 141016-104 5 ug/L I0/17/2013 10/17/2014 Jacobs 10/17/2014 Samantha .05 50 WMSl41017-IOO IO ug/L I0/18/2013 10/18/2014 Jacobs I0/17/2014 Samantha 5 50 WMS141017-100a 1 ug/L I0/18/2013 10/18/2014 Jacobs ' Samantha 10/17/2014 Jacobs .025 50 WMS141017-I04 5 ug/L 10/18/2013 I0/18/2014 I0/21/2014 Samantha .05 50 WMS 141021-IOO IO ug/L 10/22/2013 10/22/2014 Jacobs 10/21/2014 Samantha 5 50 WMS14I021-100a I ug/L 10/22/2013 10/22/2014 Jacobs I0/21/2014 Samantha .025 50 WMS 141021-104 5 ug/L 10/22/2013 10/22/2014 Jacobs 10/22/2014 Samantha .05 50 WMSl41022-IOO 10 ug/L 10/23/2013 I0/23/2014 Jacobs 10/22/2014 Samantha 5 50 WMSl41022-100a 1 ug/L 10/23/2013 I0/23/2014 Jacobs 10/22/2014 Samantha .025 50 WMS141022-104 5ug/L 10/23/2013 10/23/2014 Jacobs I0/23/2014 Samantha .05 50 WMS141023-IOO 10 ug/L I0/24/2013 I0/24/2014 Jacobs Page 2006 of 5809 10/23/2014 Samantha 5 50 WMS141023-100a 1 ug/L 10/24/2013 10/24/2014 Jacobs 10/23/2014 Samantha .025 50 WMS141023-104 5ug/L 10/24/2013 10/24/2014 Jacobs 10/24/2014 Samantha .05 50 WMS141024-100 10 ug/L 10/25/2013 10/25/2014 Jacobs 10/24/2014 Samantha 5 50 WMS141024-100a 1 ug/L 10/25/2013 I0/25/2014 Jacobs I0/24/2014 Samantha .025 50 WMS141024-104 5ug/L 10/25/2013 10/25/2014 Jacobs 10/27/2014 Samantha .05 50 WMS141027-100 10 ug/L I0/28/2013 10/28/2014 Jacobs 10/27/2014 Samantha 5 50 WMS141027-100a 1 ug/L I0/28/2013 10/28/2014 Jacobs I0/27/2014 Samantha .025 50 WMS141027-104 5ug/L I0/28/2013 10/28/2014 Jacobs 11/03/2014 Samantha .05 50 \VMS141103-IOO IO ug/L 11/04/2013 11/04/2014 Jacobs 11/03/2014 Samantha 5 50 WMS141103-100a 1 ug/L 11/04/2013 11/04/2014 Jacobs 11/03/2014 Samantha .025 50 \VMS141 I03-I04 5ug/L 11/04/2013 11/04/2014 Jacobs 11/04/2014 Samantha .05 50 WMS141104-IOO IO ug/L 11/05/2013 11/05/2014 Jacobs 11/04/2014 Samantha 5 50 WMS141104-100a 1 ug/L 11/05/2013 11/05/2014 Jacobs 11/04/2014 Samantha .025 50 WMS141104-I04 5 ug/L 11/05/2013 11/05/2014 Jacobs 11/06/2014 Samantha .05 50 \VMS141 I06-100 10 ug/L 11107/2013 11/07/2014 Jacobs 11/06/2014 Samantha 5 50 \VMS141106-100a 1 ug/L 11/07/2013 11/07/2014 Jacobs 11/06/2014 Samantha .025 50 \VMS l 4 l I06-I04 5ug/L 11/07/2013 11/07/2014 Jacobs 11/12/2014 Samantha .05 50 WMS141l12-IOO 10 ug/L 11/13/2013 11/13/2014 Jacobs 11/12/2014 Samantha 5 50 \VMS141112-100a 1 ug/L 11/13/2013 11/13/2014 Jacobs 11/12/2014 Samantha .025 50 WMS141l12-I04 5 ug/L 11/13/2013 11/13/2014 Jacobs 02/27/2015 Samantha .05 50 \VMS 150227-100 IO ug/L 02/28/2014 02/28/2015 Jacobs 02/27/2015 Samantha 5 50 \VMS150227-100a 1 ug/L 02/28/2014 02/28/2015 Jacobs Page 2007of5809 02/27/2015 Samantha .025 50 WMS150227-104 5ug/L 02/28/2014 02/28/2015 Jacobs 03/12/2015 Samantha .05 50 WMS 150312-100 10 ug/L 03/13/2014 03/13/2015 Jacobs 03/12/2015 Samantha ' 5 50 WMS150312-100a 1 ug/L 03/13/2014 . 03/13/2015 Jacobs 03/12/2015 Samantha .025 50 WMS150312-104 5 ug/L 03/13/2014 03/13/2015 Jacobs 04/13/2015 Samantha .05 50 WMS150413-100 10 ug/L 04/14/2014 04/14/2015 Jacobs 04/13/2015 Samantha 5 50 WMS150413-100a 1 ug/L 04/14/2014 04/14/2015 Jacobs 04/13/2015 Samantha .025 50 WMS150413-104 5ug/L 04/14/2014 04/14/2015 Jacobs 0610912015 Paul Boyd .05 50 WMS150609-100 10 ug/L 06/10/2014 06/10/2015 06/09/2015 Paul Boyd 5 50 WMS150609-100a 1 ug/L 06/10/2014 06/10/2015 06/09/2015 Paul Boyd .025 50 WMS 150609-104 5ug/L 06/10/2014 06/10/2015 06/10/2015 Paul Boyd .05 50 WMS150610-100 10 ug/L 06/11/2014 06/11/2015 06/10/2015 Paul Boyd 5 50 WMS150610-100a 1 ug/L 06/11/2014 06/11/2015 06/10/2015 Paul Boyd .025 50 WMS150610-104 5 ug/L 06/11/2014 06/11/2015 06/11/2015 Paul Boyd .05 50 WMS15061 l-100 10 ug/L 06/12/2014 06/12/2015 06/11/2015 Paul Boyd 5 50 WMS150611-100a 1 ug/L 06/12/2014 0611212015 06/11/2015 Paul Boyd .025 50 WMS150611-104 5 ug/L 06/12/2014 06/12/2015 06/18/2015 Paul Boyd .05 50 WMS150618-100 10 ug/L 06/19/2014 06/19/2015 06/18/2015 Paul Boyd 5 50 WMS150618-100a 1 ug/L 06/19/2014 06/19/2015 06/18/2015 Paul Boyd .025 50 WMS150618-104 5 ug/L 06/19/2014 06/19/2015 06/25/2015 Paul Boyd .05 50 WMS 150625-100 10 ug/L 06/26/2014 06/26/2015 06/25/2015 Paul Boyd 5 50 WMS150625-100a 1 ug/L 06/26/2014 06/26/2015 06/25/2015 Paul Boyd .025 50 WMS 150625-104 5 ug/L 06/26/2014 06/26/2015 07/01/2015 Paul Boyd .05 50 WMS150701-100 10 ug/L 07/02/2014 07/02/2015 07/01/2015 Paul Boyd 5 50 WMS150701-100a 1 ug/L 07/02/2014 07/02/2015 07/01/2015 Paul Boyd .025 50 WMS150701-104 5 ug/L 07/02/2014 07/02/2015 07/08/2015 Paul Boyd .05 50 WMS 150708-100 10 ug/L 07/09/2014 07/09/2015 07/08/2015 Paul Boyd 5 50 WMS150708-100a 1 ug/L 07/09/2014 07/09/2015 07/08/2015 Paul Boyd .025 50 WMS150708-104 5 ug/L 07/09/2014 07/09/2015 07/09/2015 Paul Boyd .05 50 WMS 150709-100 10 ug/L 07/10/2014 07/10/2015 07/09/2015 Paul Boyd, 5 50 \VMS150709-100a 1 ug/L 07110/2014 07/10/2015 07/09/2015 Paul Boyd .025 50 WMS 150709-104 5ug/L 07/10/2014 07/10/2015 07/10/2015 Paul Boyd .05 50 WMS 150710-100 10 ug/L 07/11/2014 07111/2015 07/10/2015 Paul Boyd 5 50 WMS150710-100a 1 ug/L 07/11/2014 07111/2015 Page 2008 of 5809 07/10/2015 Paul Boyd .025 50 WMS150710-104 5ug/L 07/11/2014 07/11/2015 07/13/2015 Paul Boyd .05 50 WMS150713-100 10 ug/L 07/14/2014 07/14/2015 07/13/2015 Paul Boyd 5 50 WMS150713-100a 1 ug/L 07/14/2014 07/14/2015 07/13/2015 Paul Boyd .025 50 WMS150713-104 5ug/L 07/14/2014 07114/2015 07/14/2015 Paul Boyd .05 50 WMS150714-100 10 ug/L 07/15/2014 07/15/2015 07/14/2015 Paul Boyd 5 50 \Vl\1S150714-100a I ug/L 07115/2014 07/15/2015 07/14/2015 Paul Boyd .025 50 WMS150714-104 5ug/L 07/15/2014 07/15/2015 07/15/2015 Paul Boyd .05 50 \Vl\1Sl50715-100 10 ug/L 07/16/2014 07/16/2015 07/15/2015 Paul Boyd 5 50 WMS150715-100a 1 ug/L 07/16/2014 07/16/2015 07/15/2015 Paul Boyd .025 50 \Vl\1Sl50715-104 5ug/L 07/16/2014 07/16/2015 07/16/2015 Paul Boyd .05 50 \Vl\1S 150716-100 10 ug/L 07/17/2014 07/17/2015 07/16/2015 Paul Boyd 5 50 WMS150716-100a I ug/L 07/17/2014 07/17/2015 07/16/2015 Paul Boyd .025 50 \Vl\1S 150716-104 5ug/L 07/17/2014 07/17/2015 07117/2015 Paul Boyd '.05 50 \Vl\1Sl50717-100 10 ug/L 07/18/2014 07/18/2015 07/17/2015 Paul Boyd 5 50 WMS150717-100a 1 ug/L 07/18/2014 07/18/2015 07/17/2015 Paul Boyd .025 50 \Vl\1Sl 50717-104 5ug/L 07/18/2014 07/18/2015 07/28/2015 Paul Boyd .05 50 WMS 150728-100 10 ug/L 07/29/2014 07/29/2015 07/28/2015 Paul Boyd 5 50 WMS150728-100a 1 ug/L 07/29/2014 07/29/2015 07/28/2015 Paul Boyd .025 50 \Vl\1S 150728-104 5ug/L 07/29/2014 07/29/2015 10/09/2015 Paul Boyd .05 50 WMS151009-100 10 ug/L 10/10/2014 10/10/2015 10/09/2015 Paul Boyd 5 50 \Vl\1Sl51009-100a 1 ug/L 10/10/2014 10/10/2015 10/09/2015 Paul Boyd .025 50 \Vl\1Sl51009-104 5ug/L 10/10/2014 10/10/2015 10/10/2015 Paul Boyd .05 50 \Vl\1S 1510 I 0-100 10 ug/L 10/11/2014 10/11/2015 10/10/2015 Paul Boyd 5 50 \Vl\1Sl51010-100a 1 ug/L 10/11/2014 10/11/2015 10/10/2015 Paul Boyd .025 50 \Vl\1S 151010-104 5 ug/L 10/11/2014 10/11/2015 10/12/2015 Paul Boyd .05 50 WMS151012-100 IO ug/L 10/13/2014 10/13/2015 10/12/2015 Paul Boyd 5 50 \Vl\1Sl51012-100a 1 ug/L 10/13/2014 10/13/2015 10/12/2015 Paul Boyd .025 50 \Vl\1S 151012-104 5ug/L 10/13/2014 10/13/2015 10/13/2015 Paul Boyd .05 50 \Vl\1Sl 51013-100 10 ug/L 10/14/2014 10/14/2015 10/13/2015 Paul Boyd 5 50 \Vl\1Sl51013-100a I ug/L 10/14/2014 10/14/2015 10/13/2015 Paul Boyd .025 50 \Vl\1Sl51013-104 5ug/L 10/14/2014 10/14/2015 10/14/2015 Paul Boyd .05 50 \Vl\1S 151014-100 10 ug/L 10/15/2014 10/15/2015 10/14/2015 Paul Boyd 5 50 WMS151014-100a I ug/L 10/15/2014 10/15/2015 10/14/2015 Paul Boyd .025 50 \Vl\1Sl51014-104 5 ug/L 10/15/2014 10/15/2015 1011512015 Paul Boyd .05 50 \Vl\1Sl51015-100 10 ug/L 10/16/2014 10/16/2015 10/15/2015 PaulBqyd 5 50 \Vl\1Sl51015-100a 1 ug/L 10/16/2014 10/16/2015 10/15/2015 Paul Boyd .025 50 \Vl\1Sl51015-104 5ug/L 10/16/2014 10/16/2015 10/22/2015 Paul Boyd .05 50 \Vl\1Sl51022-100 10 ug/L 10/23/2014 10/23/2015 Page 2009 of 5809 10/22/2015 Paul Boyd 5 50 \Vl\18151022-lOOa 1 ug/L 10/23/2014 10/23/2015 10/22/2015 Paul Boyd .025 50 \Vl\18151022-104 5 ug/L 10/23/2014 10/23/2015 12/04/2015 Paul Boyd .05 50 \Vl\18151204-100 10 ug/L 12/05/2014 12/05/2015 12/04/2015 Paul Boyd 5 50 \Vl\18151204-lOOa 1 ug/L 12/05/2014 12/05/2015 . . 12/04/2015 Paul Boyd .025 50 \Vl\18151204-104 5 ug/L 12/05/2014 12/05/2015 01/11/2016 Paul Boyd .05 50 \Vl\18160111-100 10 ug/L 01/12/2015 01/12/2016 01/11/2016 Paul Boyd 5 50 \Vl\18160111-lOOa 1 ug/L 01/12/2015 01/12/2016 0111112016 Paul Boyd .01 50 \Vl\18160111-104 5ug/L 01/12/2015 01/12/2016 01/12/2016 Paul Boyd .05 50 \Vl\18160112-100 10 ug/L 01/13/2015 01/13/2016 01/12/2016 Paul Boyd 5 50 \Vl\18160112-lOOa 1 ug/L 01/13/2015 01/13/2016 01/12/2016 Paul Boyd .01 50 \Vl\18160112-104 5ug/L 01/13/2015 01/13/2016 02/12/2016 Paul Boyd .05 50 \Vl\18160212-100 10 ug/L 02/13/2015 02/13/2016 02/12/2016 Paul Boyd 5 50 \Vl\18160212-lOOa 1 ug/L 02/13/2015 02/13/2016 02/12/2016 Paul Boyd .01 50 \Vl\18160212-104 5ug/L 02/13/2015 02/13/2016 02/16/2016 Paul Boyd .05 50 \Vl\18160216-100 10 ug/L 02/17/2015 02/17/2016 02/16/2016 Paul Boyd 5 50 \Vl\18160216-lOOa 1 ug/L 02/17/2015 02/17/2016 02/16/2016 Paul Boyd .01 50 \Vl\18160216-104 5 ug/L 02117/2015 02/17/2016 02/17/2016 Paul Boyd .05 50 \Vl\18160217-100 10 ug/L 02/18/2015 02/18/2016 02/17/2016 Paul Boyd 5 50 \Vl\18160217-lOOa 1 ug/L 02/18/2015 02/18/2016 02/17/2016 Paul Boyd .01 50 \Vl\18160217-104 5 ug/L 02/18/2015 02/18/2016 02/18/2016 Paul Boyd .05 50 \Vl\18160218-100 10 ug/L 02/19/2015 02/19/2016 02/18/2016 Paul Boyd 5 50 \Vl\18160218-lOOa 1 ug/L 02/19/2015 02/19/2016 02/18/2016 Paul Boyd .01 50 \Vl\18160218-104 5 ug/L 02/19/2015 02/19/2016 02/22/2016 Paul Boyd .05 50 \Vl\18160222-100 10 ug/L 02/23/2015 02/23/2016 02/22/2016 Paul Boyd 5 50 \Vl\18160222-lOOa 1 ug/L 02/23/2015 02/23/2016 02/23/2016 Paul Boyd .05 50 \Vl\18160223-100 10 ug/L 02/24/2015 02/24/2016 02/23/2016 Paul Boyd 5 50 \Vl\18160223-lOOa 1 ug/L 02/24/2015 02/24/2016 03/07/2016 Paul Boyd .05 50 \Vl\18160307-100 10 ug/L 03/08/2015 03/08/2016 03/07/2016 Paul Boyd 5 50 \Vl\18160307-lOOa 1 ug/L 03/08/2015 03/08/2016 03/07/2016 Paul Boyd .01 50 \Vl\181603 07-104 5ug/L 03/08/2015 03/08/2016 03/09/2016 Paul Boyd .05 50 \Vl\181603 09-100 10 ug/L 03/10/2015 03/10/2016 03/09/2016 Paul Boyd 5 50 \Vl\18160309-lOOa
l ug/L 03/10/2015 03/10/2016 03/10/2016 Paul Boyd .05 50 \Vl\18160310-100 10 ug/L 03/11/2015 03/11/2016 03/10/2016 Paul Boyd 5 50 \Vl\18160310-lOOa 1 ug/L 03/11/2015 03/11/2016 03/14/2016 Paul Boyd .05 50 \Vl\18160314-100 10 ug/L 03/15/2015 03/15/2016 03/14/2016 Paul Boyd 5 50 \Vl\18160314-lOOa 1 ug/L 03/15/20,15 03/15/2016 03/15/2016 Paul Boyd .05 50 \Vl\18160315-100 10 ug/L 03/16/2015 03/16/2016 03/15/2016 Paul Boyd 5 50 \Vl\18160315-lOOa 1 ug/L 03/16/2015 03/16/2016 Page 2010 of 5809 04/07/2016 Paul Boyd .05 50 WMS160407-100 10 ug/L 04/08/2015 04/08/2016 04/07/2016 Paul Boyd 5 50 WMS160407-100a 1 ug/L 04/08/2015 04/08/2016 04/08/2016 Paul Boyd .05 50 WMS160408-IOO IO ug/L 04/09/2015 04/09/2016 04/08/2016 Paul Boyd 5 50 WMS160408-100a 1 ug/L 04/09/2015 04/09/2016 04/08/2016 Paul Boyd .01 50 WMS 160408-104 5ug/L 04/09/2015 04/09/2016 04/11/2016 Paul Boyd .05 50 WMS 160411-IOO 10 ug/L 04/12/2015 04/12/2016 04/11/2016 Paul Boyd 5 50 WMS160411-100a 1 ug/L 04/12/2015 04/12/2016 0411112016 Paul Boyd .01 50 WMS16041 l-I04 5 ug/L 04/12/2015 04/12/2016 04/12/2016 Paul Boyd .05 50 WMS160412-IOO IO ug/L 04/13/2015 04/13/2016 04/12/2016 Paul Boyd 5 50 WMS160412-100a 1 ug/L 04/13/2015 04/13/2016 04/12/2016 Paul Boyd .01 50 WMS160412-104 5 ug/L 04/13/2015 04/13/2016 04/13/2016 Paul Boyd .05 50 WMS160413-IOO 10 ug/L 04/14/2015 04/14/2016 04/13/2016 Paul Boyd 5 50 WMS160413-100a 1 ug/L 04/14/2015 04/14/2016 04/13/2016 Paul Boyd .01 50 WMS l 60413-I04

5 ug/L 04/14/2015 04/14/2016 04/14/2016 Paul Boyd .05 50 WMS160414-100 10 ug/L 04/15/2015 04/15/2016 04/14/2016 Paul Boyd 5 50 WMS160414-100a 1 ug/L 04/15/2015 04/15/2016 04/14/2016 Paul Boyd .01 50 WMS160414-104 5 ug/L 04/15/2015 04/15/2016 04/15/2016 Paul Boyd .05 50 WMS160415-IOO 10 ug/L 04/16/2015 0411612016 04/15/2016 Paul Boyd 5 50 WMS160415-100a 1 ug/L 04/16/2015 04/16/2016 04/15/2016 Paul Boyd .01 50 WMS 160415-104 5ug/L 04/16/2015 04/16/2016 04/19/2016 Paul Boyd .05 50 WMS160419-100 IO ug/L 04/20/2015 04/20/2016 04/19/2016 Paul Boyd 5 50 WMS160419-100a 1 ug/L 04/20/2015 04/20/2016 04/19/2016 Paul Boyd .01 50 WMS 160419-104 5 ug/L 04/20/2015 04/20/2016 04/20/2016 Paul Boyd .05 50 WMS160420-IOO IO ug/L 04/21/2015 04/21/2016 04/20/2016 Paul Boyd 5 50 WMS160420-100a 1 ug/L 04/21/2015 04/21/2016 04/20/2016 Paul Boyd .01 50 WMS 160420-104 5 ug/L 04/21/2015 04/21/2016 04/21/2016 Paul Boyd .05 50 WMS160421-IOO IO ug/L 04/22/2015 04/22/2016 04/21/2016 Paul Boyd 5 50 WMS160421-100a 1 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06/22/2016 06/22/2016 Paul Boyd .05 50 \Vl\18160622-100 10 ug/L 06/23/2015 06/23/2016 06/22/2016 Paul Boyd 5 50 \Vl\18160622-lOOa I ug/L 06/23/2015 06/23/2016 06/22/2016 Paul Boyd .01 50 \Vl\18160622-104 5ug/L 06/23/2015 06/23/2016 06/23/2016 Paul Boyd .05 50 \Vl\18160623-100 10 ug/L 06/24/2015 06/24/2016 06/23/2016 Paul Boyd 5 50 \Vl\18160623-IOOa I ug/L 06/24/2015 06/24/2016 06/23/2016 Paul Boyd .01 50 \Vl\18160623-104 5 ug/L 06/24/2015 06/24/2016 06/24/2016 Paul Boyd .05 50 \Vl\18160624-100 10 ug/L 06/25/2015 06/25/2016 06/24/2016 Paul Boyd 5 50 \Vl\18160624-lOOa I ug/L . 06/25/2015 06/25/2016 06/24/2016 Paul Boyd .01 50 \Vl\18160624-104 5 ug/L 06/25/2015 06/25/2016 06/27/2016 Paul Boyd .05 50 \Vl\1816062 7-100 10 ug/L 06/28/2015 06/28/2016 06/27/2016 Paul Boyd 5 50 \Vl\18160627-lOOa 1 ug/L 06/28/2015 06/28/2016 06/27/2016 Paul Boyd .01 50 \Vl\18160627-104 5ug/L 06/28/2015 06/28/2016 06/28/2016 Paul Boyd .05 50 \Vl\18160628-100 10 ug/L 06/29/2015 06/29/2016 06/28/2016 Paul Boyd 5 50 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07/15/2016 07/26/2016 Paul Boyd .05 50 \Vl\18160726-100 10 ug/L 07/27/2015 07/27/2016 07/26/2016 Paul Boyd 5 50 \Vl\18160726-lOOa 1 ug/L 07/27/2015 07/27/2_016 07/26/2016 Paul Boyd .01 50 \Vl\18160726-104 5ug/L 07/27/2015 07/27/2016 . 07/27/2016 Paul Boyd .05 50 \Vl\18160727-100 . 10 ug/L 07/27/2015 07/27/2016 07/27/2016 Paul Boyd 5 50 \Vl\18160727-lOOa 1 ug/L 07/27/2015 07/27/2016 07/27/2016 Paul Boyd .01 50 \Vl\18160727-104 5ug/L 07/27/2015 07/27/2016 Page 2012of5809 07/28/2016 Paul Boyd .05 50 WMS 160729-100 10 ug/L 07/29/2015 07/29/2016 07/28/2016 Paul Boyd 5 50 WMS160729-100a 1 ug/L 07/29/2015 07/29/2016 08/09/2016 Paul Boyd .05 50 WMS160809-100 10 ug/L 08/10/2015 08/10/2016 08/09/2016 Paul Boyd 5 50 WMS160809-100a 1 ug/L 08/10/2015 08/10/2016 08/16/2016 Paul Boyd .05 50 WMS 160816-100 10 ug/L 08/17/2015 08/17/2016 08/16/2016 Paul Boyd 5 50 WMS160816-100a 1 ug/L 08/17/2015 08/17/2016 08/17/2016 Paul Boyd .05 50 WMS160817-100 10 ug/L 08/18/2015 08/18/2016 08/17/2016 Paul Boyd 5 50 WMS160817-100a 1 ug/L 08/18/2015 08/18/2016 08/24/2016 Paul Boyd .05 50 WMS 160824-100 10 ug/L 08/25/2015 08/25/2016 08/24/2016 Paul Boyd 5 50 WMS160824-100a 1 ug/L 08/25/2015 08/25/2016 08/25/2016 Paul Boyd .05 50 WMS 160825-100 10 ug/L 08/26/2015 08/26/2016 08/25/2016 Paul Boyd 5 50 WMSl60825-100a I ug/L 08/26/2015 08/26/2016 09/01/2016 Paul Boyd .05 50 WMS160901-100 10 ug/L 09/02/2015 09/02/2016 09/01/2016 Paul Boyd 5 50 WMS160901-100a 1 ug/L 09/02/2015 09/02/2016 09/08/2016 Paul Boyd .05 50 WMS160908-100 10 ug/L 09/09/2015 09/09/2016 09/08/2016 Paul Boyd 5 50 WMS160908-100a 1 ug/L 09/09/2015 09/09/2016 09/09/2016 Paul Boyd .05 50 WMS160909-100 10 ug/L 09/10/2015 09/10/2016 09/09/2016 Paul Boyd 5 50 WMS160909-100a 1 ug/L 09/10/2015 09/10/2016 09/13/2016 Paul Boyd .05 50 WMS160913-100 10 ug/L 09/14/2015 09/14/2016 09/13/2016 Paul Boyd 5 50 WMS160913-100a 1 ug/L 09/14/2015 09/14/2016 09/14/2016 Paul Boyd .05 50 WMS 160914-100 10 ug/L 09/15/2015 09/15/2016 09/14/2016 Paul Boyd 5 50 WMSl60914-100a 1 ug/L 09/15/2015 ' 09/15/2016 09/15/2016 Paul Boyd .05 50 WMS 160915-100 10 ug/L 09/16/2015 09/16/2016 09/15/2016 Paul Boyd 5 50 WMSl60915-100a I ug/L 09/16/2015 09/16/2016 09/16/2016 Paul Boyd 5 50 WMSl60916-100a 1 ug/L 09/16/2015 09/16/2016 09/16/2016 Paul Boyd .05 50 WMS160916-100 10 ug/L 09/17/2015 09/17/2016 09/21/2016 Paul Boyd .05 50 WMS 160921-100 10 ug/L 09/22/2015 09/22/2016 09/21/2016 Paul Boyd 5 50 WMSl60921-100a I ug/L 09/22/2015 09/22/2016 09/22/2016 Paul Boyd .05 50 WMSl60922-100 10 ug/L 09/23/2015 09/23/2016 09/22/2016 Paul Boyd 5 50 WMSl60922-100a I ug/L 09/23/2015 09/23/2016 09/23/2016 Paul Boyd .05 50 WMSl60923-100 10 ug/L 09/24/2015 09/24/2016 09/23/2016 Paul Boyd 5 50 WMSl60923-100a I ug/L 09/24/2015 09/24/2016 09/27/2016 Paul Boyd .05 50 WMSl60927-100 10 ug/L 09/28/2015 09/28/2016 09/27/2016 Paul Boyd 5 50 WMSl60927-100a I ug/L 09/28/2015 09/28/2016 09/28/2016 Paul Boyd .05 50 WMS 160928-100 10 ug/L 09/29/2015 09/29/2016 09/28/2016 Paul Boyd 5 50 WMSl60928-100a 1 ug/L 09/29/2015 09/29/201.6 06/16/2016 Paul Boyd .05 50 WMS2419735-IOO lOug/L 06/17/2015 06/17/2016 06/16/2016 Paul Boyd 5 50 WMS2419737-100a I ug/L 06/17/2015 06/17/2016 Page 2013 of 5809 I 06/16/20161 Paul Boyd I .01 GEL Laboratories LLC Version 1.0 9/18/2000 Page 2014 of 5809 50 I WMS2419743-104 I 5 ug/L 0611112015 I 0611112016 I
'"t:I ('!) N 0 -VI 0 H) VI 00 0 \0 Verification for U-236 Standard 1570-E v1.2 Analyst TC1 Tracer Information Verification Prep Date 7/18/2016 Isotope U-232 Serial Number 1564-1 Amount of Std. (ml) 0.2 Exoiration Date 11/23/2016 Standard Information Activity Standard pCi Isotope Serial Number lsotooe Halflife Reference Date Ref. Act. (dom/ml) Amount of Std. (ml) Standard Prep Date U-236 1570-E 2.3420E+07 Y 11/15/2011 111.2297 0.2 7/24/2015 Verification Rules Std# 1 2 3 Count Date 7/20/2016 7/20/2016 7/20/2016 Mean Value= Stdev= pCi dpm/ml Certificate Value .. = 10.0207 10.700 118.77 Two sigma= 0.8582 9.920 110.11 10%ofMean= 1.0207 10.000 111.00 Rule A (Pass/Fail) Pass "lo Recovery 101.86% 10.207 113"294 Rule B (Pass/Fail) Pass 0.429107601 4.763094372 Expiration Date 7/18/2017 Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value * .. Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for U-236 standard 1570-E using 0.2 ml for each source. Each standard was combined with 0.2 ml of U-232 standard 1564-1 and was diluted in a 50ml plastic centrifuge tube containing 15ml of 1 M HCL. In each source, 0.5ml of TiCl3, 100 micrograms of neodymium carrier and three ml of 48% HF was added to precipitate neodymium (and Uranium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for U-236 were calculated by comparison to U-232 certified values. dpm/ml 111.2297 9.5262 11.3294 Pass 101.86% Pass § Eckert & Ziegler Isotope Products 24937 Avenue Tibbitts Valencia, California 91355 Tel 661*309*1010 Fax 661 *257*8303 CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION Radionuclide: Half-life: Catalog No.: Source No.: U-238 (Nat) (4.468 +/- 0.005)E+09 years 7338 1577-71-2 Physical
Description:
Customer: P.O. No.: Reference Date: Contained Radioactivity: (Total Uranium) GENERAL ENGINEERING LABS. 936823 RD 15-Apr-12 12:00 PST 1.023 µCi 37.85 k.Bq A. Mass of solution: B. Chemical form: 7.05210 g in 10 ml flame-sealed ampoule U02(N03h in dilute HN03 C. Carrier content: None D. Density: Approximately 1.41 g/ml@20°C Radioimpurities: See Technical Data Sheet Radionuclide Concentration: 0.1451 µCi/g, 5.369 kBq/g Method of Calibration: Activity calculations are based upon known specific-activity and mass. Uncertainty of Measurement: A. Type A (random) uncertainty: B. Type B (systematic) uncertainty: C. Uncertainty in aliquot weighing: D. Total uncertainty at the 99% confidence level: Notes: +/- 0.0 % +/- 3.0 % +/- 0.0 % +/- 3.0 % -See reverse side for leak test(s) performed on this source. -EZIP participates in a NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference . Materials (as in NRC Regulatory Guide 4.15). . -Nuclear data was taken from "Table of Radioactive Isotopes", edited by Virginia Shirley, 1986. -This solution has a working life of 5 years. 2-l-:t'AK-/2.. Date EZIP Ref. No.: 1577-71 1'2.-l-s....-o to) t'I ------------------ISO 9001 CERTIFIED------------------Medical Imaging Laboratory Industrial Gauging Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank, California 91504 e Eckert & Ziegler 24937 Avenue Tibbitts Valencia, California 91355 Isotope Products Tel 661*309*1010 Fax 661*257*8303 U-238 Natural Technical Data The U-238 Natural used to prepare your order was taken from Eckert & Ziegler Isotope Products Lot #4550102 It had the following composition as of9 Feb 10: Nuclide U-234 U-235 U-238 At01n % 0.0055 0.7200 99.274 Activity% 49.086 *2.241 48.673 Isotopic composition provided by New Bnmswick Laboratory. If you have any question, please contact Eckert & Ziegler Isotope Products Technical Service: (661) 309-1010 ----------------1509001 CERTIFIED----------------Medical Imaging Laboratory Industrial Gauging Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank, California 91504 Standard Traceability Log Rad A Solution Material Info Isotope: Uranium-238 Source Material Info Parent Code: 1600 Prepared By: Ashley Drochter Prepared By: Ashley Drochter Prep Date: 09/04/2012 CamerConc: U02(N03)2 in dilute HN03 Verification 07/24/2015 Date: Reference Date: 04/15/2012 Expiration Date: 07/24/2016 Ampoule Mass 7.0521 g (g): Primary Code: 1600-A Dilution( mL): IOOmL Uncertainty: +/-1.17 % LogBookNo: RC-S-065-030 Mass of 6.8204 g Parent(g): Density(g/mL): 1.0789 Balance 38080204 ID: Calculations Converting parent activity to dpm/mLJdpm/g (Mass ofparent(g)) *(Parm Activity (kbq)) *(conversion dpm to kbq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (kbq)) *(conversion dpm to kbq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (6.8204 g) * (18.42 kbq) * (60000 dpm/kbq) I (7.0521g*100 mL) = 10688.8814 dpm/mL (6.8204 g) * (18.42 kbq) * (60000 dpm/kbq) I ( 1.0789 g/mL)/ (7.0521g*100 mL) = 9907.0626 dpm/g Prep Date Preparer 09/04/2012 Ashley Drochter 09/11/2012 Ashley Drochter 03/27/2014 Tim Chandler 07/24/2015 Tim Chandler GEL Laboratories LLC Version 1.0 9/18/2000 Page 2018of5809 Mass Primary 1.4579 3.0288 3.0445 3.0177 Secondary Standards Dilution Code Cone Verification Expiration (mL) dpm/mL Date Date 500 1600-B 28.8913 09/04/2012 09/04/2013 dpm/mL 500 1600-C 60.0219 09/04/2013 09/04/2014 dpm/mL 500 1600-D 60.3241 03/18/2015 03/18/2016 dpm/mL 500 1600-E 59.7931 07/12/2016 07/12/2017 dpm/mL Verification for U-238 Standard 1600-E v1.2 Analyst TC1 Tracer Information Verification Prep Date 7/12/2016 Isotope U-232 Serial Number 1564-1 Amount of Std. (ml) 0.2 Exairation Date 11/23/2016 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. ( dom/ml) Amount of Std. lmU Standard Prep Date U-238 Std# 1600-E 1 4.4680E+09 Y 2 4/15/2012 3 59.7931 0.2 7/24/2015 Verification Rules Count Date 7/12/2016 7/12/2016 7/12/2016 -Mean. Value = Stdev= pCi 5.160 5.530 5.420 5.370 0:19 dpm/ml 57.28 61.38 60.16 "59.607 2.109 Certificate Value* = Two sigma= 10 % of Mean= Rule A (Pass/Fail} %Recovery Rule B (Pass/Fail) Expiration Date 5.3868 0.3800 0.5370 .Pass 99.69% Pass 7/12/2017 Rule *A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. * -Rule B = The determined mean_ value shall be within 5% of the certificate value. *Certificate Value is decay corrected to Verification Prep -The analyst prepared three standard sources f9r U-238 standard 1600-E using. 0.2 ml for each source. Each standard was combined with 0.2 ml of U-232 standard 1564-1 and was diluted in a 50ml plastic centrifuge tube containing 15 ml of 1 M HCI. One milliliter-of TiCIS, 100 micrograms of neodymium carrier and five ml of 48% HF was added to precipitate neodymium (and Uranium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for U-238 were calculated by comparison to certified values. dpm/ml 59.7931 4.2180 5.9607 Pass 99.69% Pass Runlogs Page 2020 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Bateh ID: 1596388 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235001 SAMPLE JXH2 1040 SEP-28-16 14:05:07 DUSE 28-SEP-16 13:05 405235002 SAMPLE JXH2 1041 SEP-28-16 14:05:07 DONE 28-SEP-16 13:05 405235003 SAMPLE JXH2 1042 SEP-28-16 14:05:07 DONE 28-SEP-16 13:05 1203621688 MB JXH2 1038 SEP-28-16 14:05:07 DONE 28-SEP-16 13:04 405235004 SAMPLE JXH2 1166 SEP-28-16 14:06:35 DONE 13-SEP-16 11 :30 405235005 SAMPLE JXH2 1167 SEP-28-16 14:06:38 DONE 13-SEP-16 11 :21 405235006 SAMPLE JXH2 1169 SEP-28-16 14:06:41 DONE 13-SEP-16 11 :21 405235007 SAMPLE JXH2 1170 SEP-28-16 14:06:43 DONE 13-SEP-16 11:21 405235008 SAMPLE JXH2 1175 SEP-28-16 14:06:45 DONE 13-SEP-1611:21 405235009 SAMPLE JXH2 1176 SEP-28-16 14:06:48 DONE 13-SEP-1611:22 405235010 SAMPLE JXH2 1178 SEP-28-16 14:06:50 DUSE 13-SEP-16 13:06 405235011-SAMPLE JXH2 1179 SEP-28-1.6 14:06:53 DONE 13-SEP-16 11 :22 405235012 SAMPLE JXH2 1180 SEP-28-16 14:06:55 DUSE 13-SEP-1611:22 405235014 SAMPLE JXH2 1184 SEP-28-16 14:06:58 DUSE 13.:SEP-16 11 :23 405235015 SAMPLE JXH2 1185 SEP-28-16 14:07:01 DONE 15-SEP-16 *12:01 405235016 SAMPLE JXH2 1186 SEP-28-16 14:07:03 DONE 15-SEP-16 17:13 40523501.7 SAMPLE JXH2 1187 SEP-28-16 14:07:06 DONE 15-SEP-16 17:13 405235018 SAMPLE JXH2 1188 SEP-28-16 14:07:08 DONE 15-SEP-16 17:13 405235019 SAMPLE JXH2 1189 SEP-28-16 14:07:11 DONE 15-SEP-16 12:01 405235020 SAMPLE JXH2 1195 SEP-28-16 14:07:13 DONE 15-SEP-16 12:02 1203621689 DUP JXH2 1197 SEP-28-16 14:07:15 DONE 15-SEP-16 13:09 1203621690 LCS JXH2 1199 SEP-28-16 14:07:18 DONE 15-SEP-16 12:02 405235013 SAMPLE JXH2 1182 SEP-28-16 14:27:22 DUSE 14-SEP-16 09:53 405235001 SAMPLE JXH2 1177 OCT-01-16 12:54:07 DONE 13-SEP-16 12:10 405235010 SAMPLE JXH2 1179 OCT-01-16 12:54:09 DONE 13-SEP-1611:22 405235012 SAMPLE JXH2 1205 OCT-01-16 12:54:11 DONE 15-SEP-16 12:03 405235013 SAMPLE JXH2 1189 OCT-01-16 12:54:14 DONE 15-SEP-16 12:01 405235014 SAMPLE JXH2 1207 OCT-01-16 12:54:17 DONE 15-SEP-16 12:04 Page 2021of5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst lnstru'!lent ID Type 405235001 SAMPLE JXH2 1007 405:235002 SAMPLE JXH2 1008 405235003 SAMPLE JXH2 1009 405235004 SAMPLE JXH2 1010 1203621691 MB JXH2 1011 1203621691 MB JXH2 1012 405235005 SAMPLE JXH2 1013 405235006 SAMPLE JXH2 1014 405235007 SAMPLE JXH2 1015 405235008 SAMPLE JXH2 1016 405235009 SAMPLE JXH2 1017 405235010 SAMPLE JXH2 1018 405235011 SAMPLE JXH2 1020 405235012 SAMPLE JXH2 1021 405235013 SAMPLE JXH2 1023 405235014 SAMPLE JXH2 1024 405235015 SAMPLE JXH2 1113 405235016 SAMPLE JXH2 1115 405235017 SAMPLE JXH2 1116 405235018 SAMPLE JXH2 1117 405235019 SAMPLE JXH2 1118-405235020 SAMPLE JXH2 1119 1203621692 DUP JXH2 1121 1203621693 LCS JXH2 1122 405235001 SAMPLE JXH2 1124 405235002 SAMPLE JXH2 1126 405235003 SAMPLE JXH2 1127 405235004 SAMPLE JXH2 1128 405235006 SAMPLE JXH2 1132 405235007 SAMPLE JXH2 1133 405235008 SAMPLE JXH2 1134 405235009 SAMPLE JXH2 1139 405235010 SAMPLE JXH2 1140 405235011 SAMPLE JXH2 1142 405235012 SAMPLE JXH2 1143 405235013 SAMPLE JXH2 1144 405235014 SAMPLE JXH2 1145 ,405235015 SAMPLE JXH2 1146 405235016 SAMPLE JXH2 1147 405235017 SAMPLE JXH2 1148 405235018 SAMPLE JXH2 1149 405235019 SAMPLE JXH2 1150 405235020 SAMPLE JXH2 1152 1203621692 DUP JXH2 1154 Page 2022 of 5809 Run Date Status SEP-29-16 09:13:18 DONE SEP-29-16 09:13:18 DONE SEP-29-16 09:13:18 DONE SEP-29-16 09:13:18 DONE SEP-29-16 09:13:18 DONE SEP-29-16 09:13:18 DONE SEP-29-16 09:13:19 DONE SEP-29-16 09:13:19 DONE SEP-29-16 09:13:19 DONE SEP-29-16 09:13:19 DONE SEP-29-16 09:13:19 DONE SEP-29-16 09:13:19' DONE SEP-29-16 09:13:20 DONE SEP-29-16 09:13:20 DONE SEP-29-16 09:13:20 DONE SEP-29-16 09:13:20 DONE SEP-29-16 09:20:16 DONE SEP-29-16 09:20:17 DONE SEP-29-16 09:20:21 DONE SEP-29-16 09:20:23 DONE SEP-29-16 09:20:26 DONE SEP-29-1.6 09:20:28 DONE SEP-29-16 09:20:31 DONE SEP-29-16 09:20:33 DONE SEP-29-16 09:20:35 DONE SEP-29-16 09:20:38 DONE SEP-29-16 09:20:41 DONE SEP-29-16 09:20:43 DONE SEP-29-16 09:20:46 DONE SEP-29-16 09:20:48 DONE SEP-29-16 09:20:50 DONE SEP-29-16 09:20:52 DONE SEP-29-16 09:20:55 DONE SEP-29-16 09:20:58 DONE SEP-29-16 09:21:00 DONE SEP-29-16 09:21:03 DONE SEP-29-16 09:21:05 DONE SEP-29-16 09,:21:07 DONE SEP-29-16 09:21:11 DONE SEP-29-16 09:21:13 DONE SEP-29-16 09:21:16 DONE SEP-29-16 09:21:17 DONE SEP-29-16 09:21:21 DONE SEP-29-16 09:21:23 DONE Batch ID: 1596389 Geometry Calibration Date 27-SEP-16 14:31 27-SEP-16 14:31 27-SEP-16 14:31 27-SEP-16 14:31 27-SEP-16 17:14 27-SEP-16 14:33 27-SEP-16 14:33 27-SEP-16 14:34 27-SEP-16 14:34 27-SEP-16 14:34 27-SEP-16 14:34 27-SEP-16 14:34 27-SEP-16 14:34 27-SEP-16 14:35 27-SEP-16 17:14 27-SEP-16 14:35 08-SEP-16 11 :00 08-SEP-1611:00 08-SEP-1611:01 08-SEP-16 11 :01 08-SEP-16 12:36 08-SEP-16 12:37 08-SEP-16 12:37 08-SEP-16 11 :01 08-SEP-16 12:37 08-SEP-16 12:37 08-SEP-16 11 :02 08-SEP-16 11 :02 08-SEP-16 12:38 08-SEP-16 11 :03 08-SEP-16 11 :03 09-SEP-16 11 :41 09-SEP-16 11:41 09-SEP-16 11 :42 09-SEP-16 13:32 09-SEP-16 11 :43 09-SEP-16 13:32 09-SEP-16 11 :43 09-SEP-1611:43 09-SEP-16 11 :44 09-SEP-16 11 :44 09-SEP-16 11 :44 09-SEP-16 12:25 09-SEP-16 12:25 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst Instrument ID *Type 1203621693 LCS JXH2 1155 405235005 SAMPLE JXH2 1131 Page 2023 of 5809 Run Date Status SEP-29-16 09:21:25 DONE SEP-29-1609:41:50 DONE Geometry Calibration Date 09-SEP-16 11:44 08-SEP-16 11:02 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596390 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 1203621694 MB JXH2 1095 SEP-29-16 21 :26:43 DONE 06-SEP-16 11 :01 405235001 SAMPLE JXH2 1213 SEP-29-16 21:50:31 DONE 16-SEP-16 12:45 405235002 SAMPLE JXH2 1214 SEP-29-16 21:50:34 DONE 16-SEP-16 12:45 405235009 SAMPLE JXH2 1218 SEP-29-16 21 :50:36 DONE 16-SEP-16 12:46 405235003 SAMPLE JXH2 1221 SEP-29-16 21:50:41 DONE 16-SEP-16 14:16 405235004 SAMPLE JXH2 1223 SEP-29-16 21:50:45 DONE 16-SEP-16 14:05 405235005 SAMPLE JXH2 1224 SEP-29-16 21 :50:48 DONE 16-SEP-16 14:17 405235006 SAMPLE JXH2 1226 SEP-29-16 21:50:50 DONE 16-SEP-16 11 :38 405235007 SAMPLE JXH2 1227 SEP-29-16 21 :50:52 DONE 16-SEP-16 14:05 405235008 SAMPLE JXH2 1228 SEP-29-16 21 :50:56 DONE 16-SEP-16 11:38 405235010 SAMPLE JXH2 1231 SEP-29-16 21 :51 :01 DONE 16-SEP-16 12:46 405235011 SAMPLE JXH2 1233 SEP-29-16 21 :51 :59 DUSE 19-SEP-16 15:36 405235012 SAMPLE JXH2 1234 SEP-29-16 21 :52:02 DONE 19-SEP-16 15:36 405235013 SAMPLE JXH2 1235 SEP-29-16 21 :52:04 DONE 19-SEP-16 15:37 405235014 SAMPLE JXH2 1236 SEP-29-16 21 :52:07 DONE 19-SEP-16 15:37 405235015 SAMPLE JXH2 1241 SEP-29-16 21 :52:09 DUSE 19-SEP-16 15:37 405235016 SAMPLE JXH2 1242 SEP-29-16 21 :52:11 DUSE 19-SEP-16 15:38 405235017 SAMPLE JXH2 1243 SEP-29-16 21 :52: 14 DONE 19-SEP-16 15:38. 405235018 SAMPLE JXH2 1244 SEP-29-16 21:52:17 DONE 19-SEP-16 15:38 405235019 SAMPLE JXH2 1245 SEP-29-16 21 :52:20 DONE 19-SEP-16 15:38 405235020 SAMPLE JXH2 1246 SEP-29-16 21 :52:22 DONE 19-SEP-16 15:38 1203621695 DUP JXH2 1247 SEP-29-16 21 :52:25 DONE 19-SEP-16 15:39 1203621696 LCS JXH2 1248 SEP-29-16 21 :52:28 DONE 19-SEP-16 15:39 405235015 SAMPLE JXH2 1071 OCT-01-16 13:23:22 DONE 30-SEP-16 12:07 405235016 SAMPLE JXH2 1072 OCT-01-16 13:23:22 DONE 30-SEP-16 12:07 405235011 SAMPLE JXH2 1070 OCT-01-16 13:23:25 DONE 30-SEP-16 12:06 Page 2024 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596392 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235001 SAMPLE JXH2 1161 SEP-30-16 08:59:52 DONE 13-SEP-16 13:45 405235002 SAMPLE JXH2 1162 SEP-30-16 08:59:54 DONE 13-SEP-16 11:19 405235003 SAMPLE JXH2 1178 SEP-30-16 08:59:57 DONE 13-SEP-16 13:06 405235005 SAMPLE JXH2 1167 SEP-30-16 08:59:59 DONE 13-SEP-16 11:21 405235006 SAMPLE JXH2 1169 SEP-30-16 09:00:01 DONE 13-SEP-16 11:21 40523Q007 SAMPLE JXH2 1170 SEP-30-16 09:00:03 DONE 13-SEP-1611:21 405235008 SAMPLE JXH2 1175 SEP-30-16 09:00:05 DONE 13-SEP-16 11 :21 405235009 SAMPLE JXH2 1176 SEP-30-16 09:00:08 DONE 13-SEP-1611:22 405235010 SAMPLE JXH2 1177 SEP-30-16 09:00:10 DONE 13-SEP-16 12:10 405235011 SAMPLE JXH2 1179 SEP-30-16 09:00:13 DONE 13-SEP-16 11 :22 405235012 SAMPLE JXH2 1180 SEP-30-16 09:00:16 DONE 13-SEP-16 11 :22 405235013 SAMPLE JXH2 1185 SEP-30-16 09:00:18 DONE 15-SEP-16 12:01 405235014 SAMPLE JXH2 1186 SEP-30-16 09:00:20 DONE *15-SEP-16 17:13 405235015 SAMPLE JXH2 1188 SEP-30-16 09:00:22 DONE 15-SEP-16 17:13 405235016 SAMPLE JXH2 1195 SEP-30-16 09:00:25 .DONE 15-SEP-16 12:02 405235017 SAMPLE JXH2 1197 SEP-30-16 09:00:27 DONE 15-SEP-16 13:09 405235018 SAMPLE JXH2 1199 SEP-30-16 09:00:30 DONE 15-SEP-16 12:02 405235019 SAMPLE JXH2 1182 SEP-30-16 09:00:32 DONE 14-SEP-16 09:53 405235020 SAMPLE JXH2 1200. SEP-30-16 09:00:34 DONE 15-SEP-16 12:03 1203621697 MB JXH2 1166 SEP-30-16 09:00:37 DONE 13-SEP-1611:30 1203621698 DUP JXH2 1234 SEP-30-16 09:00:39 DONE 19-SEP-16 15:36 1203621699 LCS JXH2 1189 SEP-30-16 09:00:42 DONE 15-SEP-16 12:01 405235004 SAMPLE JXH2 1175 OCT-01-16 12:54:30 PONE 13-SEP-16 11:21 Page 2025 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596393 Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235001 SAMPLE JXH2 1103 SEP-29-16 09: 18:29 DONE 06-SEP-16 11 :02 405235002 SAMPLE JXH2 1104 SEP-29-16 09:18:29 DONE 06-SEP-16 11 :02 405235003 SAMPLE JXH2 1105 SEP-29-16 09:18:29 DONE 06-SEP-16 11 :02 405235004 SAMPLE JXH2 1106 SEP-29-16 09:18:29 DONE 06-SEP-16 11 :02 405235005 SAMPLE JXH2 1107 SEP-29-16 09:18:30 DONE 06-SEP-16 11 :02 405235006 SAMPLE JXH2 1108 SEP-29-16 09:18:30 DONE 06-SEP-16 11 :02 405235007 SAMPLE JXH2 1109 SEP-29-16 09:18:30 DONE 06-SEP-16 11 :02 405235008 SAMPLE JXH2 1110 SEP-29-16 09:18:30 DONE 06-SEP-16 11:02
405235009 SAMPLE JXH2 1112 SEP-29-16 09:18:30 DONE 06-SEP-16 11 :03 405235010 SAMPLE JXH2 1210 SEP-29-16 09:23:32 DONE 16-SEP-16 11 :37 405235011 SAMPLE JXH2 1212 SEP-29-16 09:23:34 DONE 16-SEP-16 12:45 405235012 SAMPLE JXH2 1213 SEP-29-16 09:23:37 DONE 16-SEP-16 12:45 405235013 SAMPLE JXH2 1214 SEP-29-16 09:23:39 DONE 16-SEP-16 12:45 405235014 SAMPLE JXH2 1218 SEP-29-16 09:23:41 DONE 16-SEP-16 12:46 405235016 SAMPLE JXH2 1220 SEP-29-16 09:23:45 DONE 16-SEP-16 11:38 405235017 SAMPLE JXH2 1221 SEP-29-16 09:23:48 DONE 16-SEP-16 14:16 405235018 SAMPLE JXH2 1223 SEP-29-16 09:23:51 DONE 16-SEP-16 14:05 405235019 SAMPLE JXH2 1224 SEP-29-16 09:23:52 DONE 16-SEP-16 14:17 405235020 SAMPLE JXH2 1226 SEP-29-16 09:23:54 DONE 16-SEP-16 11:38 1203621701 DUP JXH2 1228 SEP-29-16 09:23:57 DONE 16-SEP-16 11:38 1203621700 MB JXH2 1227 SEP-29-16 09:24:00 DONE 16-SEP-16 14:05 1203621702 LCS JXH2 1233 SEP-29-16 09:24:03 DUSE 19-SEP-16 15:36 405235015 SAMPLE JXH2 1235 SEP-29-16 09:44:15 DONE 19-SEP-16 15:37 1203621702 LCS JXH2 1177 SEP-29.-16 14: 16:08 DONE 13-SEP-16 12:10 Page 2026 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596395 Sample Sample Ana1vst Instrument Run Date Status Geometry Calibration Date ID Type 405235021 SAMPLE MXS2 1033 SEP-24-16 13:16:16 DONE 29-AUG-16 12:37 1203621706 MB MXS2 1034 SEP-24-16 13:16:16 DONE 29-AUG-16 12:37 405235022 SAMPLE MXS2 1038 SEP-24-16 13:16:17 DONE 29-AUG-16 12:38 405235023 SAMPLE MXS2 1040 SEP-24-16 13:16:17 DONE 29-AUG-16 12:38 405235024 SAMPLE MXS2 1041 SEP-24-16 13:16:17 DONE 29-AUG-16 12:38 405235025 SAMPLE MXS2 1042 SEP-24-1613:16:17 DONE 29-AUG-16 12:38 405235026 SAMPLE MXS2 1161 SEP-24-16 13:17:52 DONE 13-SEP-16 13:45 405235027 SAMPLE MXS2 1162 SEP-24-16 13:17:55 DONE 13-SEP-16 11 : 19 405235028 SAMPLE MXS2 1166 SEP-24-16 13:17:57 DONE 13-SEP-16 11 :30 405235029 SAMPLE MXS2 1167 SEP-24-16 13:17:59 DONE 13-SEP-1611:21 405235030 SAMPLE MXS2 1169 SEP-24-16 13:18:02 DONE 13-SEP-16 11:21 405235031 SAMPLE MXS2 1170 SEP-24-'16 13:18:04 DONE 13-SEP-16 11:21' 405235032 SAMPLE MXS2 1175 SEP-24-16 13:18:06 DONE 13-SEP-16 11 :21 405235033 SAMPLE MXS2 1176 SEP-24-16 13:18:08 DONE 13-SEP-1611:22 405235034 SAMPLE MXS2 1177 SEP-24-16 13:18:10 DONE 13-SEP-16 12:10 405235036 SAMPLE MXS2 1179 SEP-24-16 13:18:15 DONE 13-SEP-16 11:22 405235037 SAMPLE MXS2 1180 SEP-24-16 13:18:18 DONE 13-SEP-16 11 :22 405235038 SAMPLE MXS2 1182 SEP-24-16 13:18:20 DONE 14-SEP-16 09:53 405235040 SAMPLE MXS2 1185 SEP-24-16 13:18:25 DONE 15-SEP-16 12:01 1203621708 LCS MXS2 1187 SEP-24-16 13:18:31 DONE 15-SEP-16 17:13 1203621707 DUP MXS2 1201 .SEP-28-16 17:56:47 DONE 15-SEP-16 12:03 405235035 SAMPLE MXS2 1207 SEP-28-16 17:56:50 DONE 15-SEP-16 12:04 405235039 SAMPLE MXS2 1208 SEP-28-16 17:56:52 DONE 15-SEP-16 14:36 Page 2027 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst. Instrument ID Type 405235021 SAMPLE MXS2 1128 405235024 SAMPLE MXS2 1131 405235025 SAMPLE MXS2 1134 405235026 SAMPLE MXS2 1139 405235027 SAMPLE MXS2 1140 405235028 SAMPLE MXS2 1142 405235029 SAMPLE MXS2 1143 405235030 SAMPLE MXS2 1144 405235031 SAMPLE MXS2 1145 405235032 SAMPLE MXS2 1146 405235033 SAMPLE MXS2 1147 405235034 SAMPLE MXS2 1148 405235035 SAMPLE MXS2 1149 405235036 SAMPLE MXS2 1150 405235037 SAMPLE MXS2 1152 405235038 SAMPLE MXS2 1154 405235039 SAMPLE MXS2 1155 405235040 SAMPLE MXS2 1156 1203621711 LCS MXS2 1158 405235021 SAMPLE MXS2 1159 405235022 SAMPLE MXS2 1160 1203621709 MB MXS2 1127 1203621709 MB MXS2 1132 405235023 SAMPLE MXS2 1001 405235024 SAMPLE MXS2 1002 405235025 SAMPLE MXS2 1003 405235026 SAMPLE MXS2 1005 405235027 SAMPLE MXS2 1006 405235028 SAMPLE MXS2 1007 405235029 SAMPLE MXS2 1008 405235030 SAMPLE MXS2 1009 405235031 SAMPLE MXS2 1010 405235032 SAMPLE MXS2 1011 405235033 SAMPLE MXS2 1012 405235034 SAMPLE MXS2 1013 405235035 SAMPLE MXS2 1014 405235036 SAMPLE MXS2 1015 405235037 SAMPLE MXS2 1016 405235038 SAMPLE MXS2 1017 405235039 SAMPLE MXS2 1018 405235040 SAMPLE MXS2 1113 1203621711 LCS MXS2 1115 405235022 SAMPLE MXS2 1157 405235023 SAMPLE MXS2 1158 Page 2028of5809 Run Date Status SEP-24-16 13:19:38 DONE SEP-24-16 13:19:46 DONE SEP-24-16 13:19:49 DONE SEP-24-16 13:19:52 DONE SEP-24-16 13:19:54 DONE SEP-24-16 13:19:57 DONE SEP-24-16 13:19:59 DONE SEP-24-16 13:20:01 DONE SEP-24-16 13:20:04 DONE SEP-24-16 13:20:06 DONE SEP-24-16 13:20:09 DONE SEP-24-16'13:20:11 DONE SEP-24-16 13:20:13 DONE SEP-24-16 13:20:16 DONE SEP-24-16 13:20:18 DONE SEP-24-16 13:20:21 DONE SEP-24-16 13:20:22 DONE SEP-24-16 13:20:25 DONE SEP-24-16 13:20:30 DONE SEP-24-16 13:20:33 DONE SEP-24-16 13:20:35 DONE SEP-24-16 13:49:22 DONE SEP-24-16 13:49:58 DONE SEP-25-16 15:53:59 DONE SEP-25-16 15:53:59 DONE SEP-25-16 15:53:59 DONE SEP-25-16 15:53:59 DONE SEP-25-16 15:53:59 DONE 15:54:03 DONE SEP-25-16 15:54:03 DONE SEP-25-16 15:54:03 DONE SEP-25-16 15:54:03 DONE SEP-25-16 15:54:03 DONE SEP-25-16 15:54:03 DONE SEP-25-16 15:54:08 DONE SEP-25-16 15:54:08 DONE SEP-25-16 15:54:08 DONE 15:54:08 DONE SEP-25-16 15:54:08 DONE SEP-25-16 15:54:08 DONE SEP-25-16 15:54:41 DONE SEP-25-16 15:54:46 DONE SEP-28-16 17:55:25 DONE SEP-28-16 17:55:27 DONE Batch ID: 1596396 Geom Calibration Date 08-SEP-16 11 :02 08-SEP-16 11 :02 08-SEP-16 11 :03 09-SEP-16 11:41 09-SEP-16 11:41 09-SEP-1611:42 09-SEP-16 13:32 09-SEP-1611:43 09-SEP-16 13:32 09-SEP-16 11 :43 09-SEP-1611:43 09-SEP-1611:44 09-SEP-16 11 :44 09-SEP-16 11 :44 09-SEP-16 12:25 09-SEP-16 12:25 09-SEP-16 11 :44 09-SEP-16 11 :44 09-SEP-16 11 :46 09-SEP-16 11 :46 09-SEP-16 11 :46 08-SEP-16 11 :02 08-SEP-16 12:38 27-AUG-16 14:30 27-AUG-16 14:30 28-AUG-16 16:08 27-AUG-16 14:31 27-AUG-16 14:31 23-SEP-16 11 :42 27-AUG-16 14:31 23-SEP-16 11 :42 28-AUG-16 16:08 27-AUG-16 14:32 27-AUG-16 14:32 27-AUG-16 14:32 27-AUG-16 14:32 27-AUG-16 14:32 27-AUG-16 14:32 27-AUG-16 14:32 28-AUG-16 16:08 08-SEP-16 11 :00 08-SEP-16 11 :00 09-SEP-16 11 :46 09-SEP-16 11 :46 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst Instrument ID. Type 1203621710 DUP MXS2 1159 1203621710 DUP MXS2 1157 Page 2029 of 5809 Run Date Status SEP-28-16 17:55:29 DONE SEP-29-16 14:04:04 DONE Geometry Calibration Date 09-SEP-16 11 :46 09-SEP-16 11 :46 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst Instrument ID . Type 405235021 SAMPLE MXS2 1205 405235022 SAMPLE MXS2 1206 405235023 SAMPLE MXS2 1207 405235024 SAMPLE MXS2 1208 405235025 SAMPLE MXS2 1026 405235026 SAMPLE MXS2 1028 405235027 SAMPLE MXS2 1029 405235028 SAMPLE MXS2 1030 405235029 SAMPLE MXS2 1032 405235030 SAMPLE MXS2 1033 405235031 SAMPLE MXS2 1034 405235032 SAMPLE MXS2 1038 405235033 SAMPLE MXS2 1040 405235034 SAMPLE MXS2 1041 405235035 SAMPLE MXS2 1042 405235036 SAMPLE MXS2 1161 405235037 SAMPLE MXS2 1162 405235038 SAMPLE MXS2 1166 405235039 SAMPLE MXS2 1167 405235040 SAMPLE MXS2 1169

1203621715 MB MXS2 1170 1203621716 DUP 1203621717 LCS MXS2 1175 MXS2 1176 1203621717 LCS MXS2 1180 405235032 SAMPLE MXS2 1161 405235033 SAMPLE MXS2 1162 405235035 SAMPLE MXS2 1166 405235036 SAMPLE MXS2 1167 405235037 SAMPLE MXS2 1169 405235038 SAMPLE MXS2 1170 405235039 SAMPLE MXS2 1175 405235040 SAMPLE MXS2 1176 1203621715 MB MXS2 1177 405235021 SAMPLE MXS2 1185 405235022 SAMPLE MXS2 1186 405235023 SAMPLE MXS2 1188 405235024 SAMPLE MXS2 1189 405235025 SAMPLE 1195 405235027 SAMPLE MXS2 1199 405235028 SAMPLE MXS2 1200 405235029 SAMPLE MXS2 1201 405235030 SAMPLE MXS2 1202 405235031 SAMPLE MXS2 1203 405235034 SAMPLE MXS2 1182 Page 2030 of 5809 Run Date Status SEP-24-16 13:14:29 DUSE SEP-24-16 13:14:31 DUSE SEP-24-16 13:14:34 DUSE SEP-24-16 13:14:36 DUSE SEP-25-16 15:53:37 DUSE SEP-25-16 15:53:37 DUSE SEP-25-16 15:53:37 DUSE SEP-25-16 15:53:37 DUSE SEP-25-16 15:53:42 DUSE SEP-25-16 15:53:42 DUSE SEP-25-16 15:53:42 DUSE SEP-25-16 15:53:46 DUSE SEP-25-16 15:53:46 DUSE SEP-25-16 15:53:46 DUSE SEP-25-16 15:53:46 DUSE SEP-25-16 15:54:22 DUSE SEP-25-16 15:54:24 DUSE SEP-25-16 15:54:25 DUSE SEP-25-16 15:54:29 DUSE SEP-25-16 15:54:31 DUSE SEP-25-16 15:54:32 DUSE SEP-25-16 15:54:36 DUSE SEP-25-16 15:54:38 DUSE SEP-26-16 11:53:52 DONE SEP-26-16 17:09:37 DONE SEP-26-16 17:09:39 DONE SEP-26-16 17:09:43 DONE SEP-26-16 17:09:46 DONE SEP-26-16 17:09:48 DONE SEP-26-16 17:09:51 DONE SEP-26-16 17:11:08 DONE SEP-26-16 17:11:10 DONE SEP-26-16 17:11:13

DONE SEP-26-16 17:11:18 DONE SEP-26-16 17:11 :20 DONE SEP-26-16 17:11 :23 DONE SEP-26-16 17:11:25 DONE SEP-26-16 17:11:27 DONE SEP-26-16 17:11:32 DONE SEP-26-16 17:11:35 DONE SEP-26-16 17:11 :37 DONE SEP-26-16 17:11:40 DONE SEP-26-1617:11:43 DONE SEP-26-16 17:35:29 DONE Batch ID: 1596399 Geometry Calibration Date 15-SEP-16 12:03 15-SEP-16 12:03 15-SEP-16 12:04 15-SEP-16 14:36 29-AUG-16 12:35 29-AUG-1612:35 29-AUG-16 16:41 29-AUG-16 16:41 29-AUG-16 12:36 29-AUG-16 12:37 29-AUG-16 12:37 29-AUG-16 12:38 29-AUG-16 12:38 29-AUG-16 12:38 29-AUG-16 12:38 13-SEP-16 13:45 13-SEP-1611:19 13-SEP-16 11 :30 13-SEP-16 11:21 13-SEP-16 11:21 13-SEP-16 11:21 13-SEP-16 11:21 13-SEP-16 11 :22 13-SEP-16 11 :22 13-SEP-16 13:45 13-SEP-1611:1.9 13-SEP-16 11 :30 13-SEP-16 11:21 13-SEP-16 11:21 13-SEP-16 11:21 13-SEP-16 11:21 13-SEP-16 11 :22 13-SEP-16 12:10 15-SEP-16 12:01 15-SEP-16 17:13 15-SEP-16 17:13 15-SEP-16 12:01 15-SEP-16 12:02 15-SEP-16 12:02 15-SEP-16 12:03 15-SEP-16 12:03 15-SEP-16 13:09 15-SEP-16 17:14 14-SEP-16 09:53 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst ID Type 405235026 SAMPLE MXS2 1069 1203621716 DUP MXS2 1070 Page 2031 of 5809 Run Date Status SEP-29-16 14:05:23 DONE SEP-29-16 14:05:23 DONE Geometry Calibration Date 03-SEP-16 15:23 03-SEP-16 15:23 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596400 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235030 SAMPLE MXS2 1253 SEP-24-16 20:51:04 DONE 19-SEP-16 15:40 405235031 SAMPLE MXS2 1254 SEP-24-16 20:51:06 DONE 19-SEP-16 15:40 405235032 SAMPLE MXS2 1255 SEP-24-16 20:51:08 DONE 19-SEP-16 15:40 405235033 SAMPLE MXS2 1256 SEP-24-16 20:51 :11 DONE 19-SEP-16 15:40 1203621720 LCS MXS2 1226 SEP-24-16 20:54:04 DONE 16-SEP-16 11 :38 405235034 SAMPLE MXS2 1233 SEP-24-16 20:54:08 DONE 19-SEP-16 15:36 405235035 SAMPLE MXS2 1234 SEP-24-16 20:54: 11 DONE 19-SEP-16 15:36 405235036 SAMPLE MXS2 1235 SEP-24-16 20:54: 13 DONE

19-SEP-16 15:37 405235037 SAMPLE MXS2 1236 SEP-24-16 20:54:15 DUSE 19-SEP-16 15:37 405235038 SAMPLE MXS2 1238 SEP-24-16 20:54:18 DONE 19-SEP-16 15:37 405235039 SAMPLE MXS2 1240 SEP-24-16 20:54:20 DUSE

19-SEP-16 15:37 405235040 . SAMPLE MXS2 1241 SEP-24-16 20:54:22 "DONE 19-SEP-16 15:37 1203621718 MB MXS2 1243 SEP-24-16 20:54:24 DONE 19-SEP-16 15:38 1203621719 DUP MXS2 1244 SEP-24-16 20:54:26 DONE 19-SEP-16 15:38 405235021 SAMPLE MXS2 1089 SEP-24-16 20:54:51 DONE 06-SEP-16 10:59 405235022 SAMPLE MXS2 1090 SEP-24-16 20:54:51 DONE 06-SEP-16 11 :00 405235023 SAMPLE* MXS2 1091 SEP-24-16 20:54:51 DONE 06-SEP-16 11 :00 405235024 SAMPLE MXS2 1092 SEP-24-16 20:54:51 DONE 06-SEP-16 11 :00 405235025 SAMPLE MXS2 1093 SEP-24-16 20:54:51 DONE 06-SEP-16 11 :00 405235026 SAMPLE MXS2 1095 SEP-24-16 20:54:52 DONE 06-SEP-16 11 :01 405235027 SAMPLE MXS2 1096 SEP-24-16 20:54:52 DONE 06-SEP-16 11:01 405235028 SAMPLE MXS2 1097 SEP-24-16 20:54:52 DONE 06-SEP-16 11 :01 405235029 SAMPLE MXS2 1099 SEP-24-16 20:54:52 DONE 06-SEP-16 11 :01 405235037 SAMPLE MXS2 1255 SEP-26-16" 13:55:05 DONE 19-SEP-16 15:40 405235039 SAMPLE MXS2 1256 SEP-26-16 13:55:07 DONE

19-SEP-16 15:40 Page 2032 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596407 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235045 SAMPLE HAKB 1199 SEP-22-16 09:57:35 DONE 15-SEP-16 12:02 405235041 SAMPLE HAKB 1038 SEP-22-16 09:57:38 DUSE 29-AUG-16 12:38 405235042 SAMPLE HAKB 1040 SEP-22-16 09:57:38 DONE 29-AUG-16 12:38 405235044 SAMPLE HAKB 1042 SEP-22-16 09:57:38 .DONE 29-AUG-16 12:38 405235046 SAMPLE HAKB 1200 SEP-22-16 09:57:38 DONE 15-SEP-16 12:03 405235047 SAMPLE HAKB 1201 SEP-22-16 09:57:40 DONE 15-SEP-16 12:03 405235048 SAMPLE HAKB 1202 SEP-22-16 09:57:43 DONE 15-SEP-16 13:09 405235049 SAMPLE HAKB 1203 SEP-22-16 09:57:45 DUSE 15-SEP-16 17:14 405235050 SAMPLE HAKB 1204 SEP-22-16 09:57:47 DUSE 15MSEP-16 14:00 405235051 SAMPLE HAKB 1205 SEP-22-16 09:57:50 DUSE 15-SEP-16 12:03 405235052 SAMPLE HAKB 1206 SEP-22-16 09:57:53 DONE 15-SEP-16 12:03 405235053 SAMPLE HAKB 1207 'SEP-22-16 09:57:55 DONE 15-SEP.:16 12:04 405235054 SAMPLE HAKB 1208 SEP-22-16 09:57:57 DONE 15-SEP-16 14:36. 405235055 SAMPLE HAKB 1026 SEP-22-16 13:44: 15 . DONE 29-AUG-16 12:35 405235056 .SAMPLE HAKB 1028 SEP-22-16 13:44:15 DONE 29-AUG-16 12:35 '405235057 SAMPLE HAKB 1029 SEP-22-16 13:44:15 DONE 29-AUG-16 16:41 405235058 SAMPLE HAKB 1030 SEP-22-.16 13:44:15 DUSE 29-AUG-16 16:41 405235059 SAMPLE HAKB 1032 SEP-22-16 13:44:16 DONE 29-AUG-16 12:36 405235060 SAMPLE HAKB 1033 SEP-22-16. 13:44:16 DONE 29-AUG-16 12:37 1203621736 MB. HAKB 1034 SEP-22-16 13:44: 16 DONE 29-AUG-16 12:37 1203621737 DUP HAKB 1169 SEP-22-16 14:25:33 DONE 13-SEP-16 11 :21 1203621738 LCS HAKB 1170 . SEP-22-16 14:25:35* DONE 13-SEP-16 11 :21 405235049 SAMPLE HAKB 1162 SEP-26-16 12:01:33 DONE 13-SEP-16 11:19 405235050 SAMPLE HAKB 1163 SEP-26-16 12:01:36 DONE 13-SEP-16 11 :20 405235051 SAMPLE HAKB 1169 SEP-26-1612:01:38 DONE 13-SEP-16 11 :21 405235058 SAMPLE HAKB 1176 SEP-26-16 12:01 :41 DONE 13-SEP-16 11 :22 405235041 SAMPLE HAKB 1188 SEP-27-16 17:12:36 DONE 15-SEP-16 17:13 405235043 SAMPLE HAKB 1189 SE0P-27-16 17:12:39 DONE 15-SEP-16 12:01 Page 2033 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst Instrument ID Type 405235041 SAMPLE HAKB 1015 405235042 SAMPLE HAKB 1016 405235043 SAMPLE HAKB 1017 405235044 SAMPLE HAKB 1018 405235045 SAMPLE HAKB 1020 405235046 SAMPLE HAKB 1021 405235047 SAMPLE HAKB 1024 405235048 SAMPLE HAKB 1113 405235049 SAMPLE HAKB 1114 405235050 SAMPLE HAKB 1115 405235051 SAMPLE HAKB 1116 405235052 SAMPLE HAKB 1117 405235053 SAMPLE HAKB 1118 405235054 SAMPLE HAKB 1119 405235056 SAMPLE HAKB 1121 405235057 SAMPLE HAKB 1122 405235058 SAMPLE HAKB 1124 405235059 SAMPLE HAKB 1126 405235060 SAMPLE HAKB 1127 1203621739 MB HAKB 1128 405235042 SAMPLE HAKB 1132 405235043 SAMPLE HAKB 1133 405235044 SAMPLE HAKB 1134 405235045 SAMPLE HAKB 1139 405235046 SAMPLE HAKB 1140 405235047 SAMPLE HAKB 1142 405235048 SAMPLE HAKB 1143 405235049 SAMPLE HAKB 1144 405235050 SAMPLE HAKB 1145 405235051 SAMPLE HAKB 1146 405235052 SAMPLE HAKB 1147 405235053 SAMPLE HAKB 1148 405235054 SAMPLE HAKB 1149 405235055 SAMPLE HAKB 1150 405235056 SAMPLE HAKB 1152 405235057 SAMPLE HAKB 1154 405235058 SAMPLE HAKB 1155 405235059 SAMPLE HAKB 1156 405235060 SAMPLE HAKB 1157 1203621739 MB HAKB 1158 1203621740 DUP 1203621741 LCS HAKB 1159 HAKB 1160 405235041 SAMPLE HAKB 1016 405235055 SAMPLE HAKB 1013 Page 2034 of 5809 Run Date Status SEP-22-16 10:00:17 DONE SEP-22-16 10:00:17 DONE SEP-22-16 10:00:17 DONE SEP-22-16 10:00:17 DONE SEP-22-16 10:00:19 DONE SEP-22-16 10:00:19 DONE SEP-22-16 10:00:19 DONE SEP-22-16 10:02:46 DONE SEP-22-16 10:02:49 DONE SEP-22-16 10:02:51 DONE SEP-22-16 10:02:54 DUSE SEP-22-16 10:02:56 DONE SEP-22-16 10:02:58 DONE SEP-22-16 10:03:00 DONE SEP-22-16 10:03:06 DONE SEP-22-16 10:03:08 DONE SEP-22-16 10:03:10 DONE SEP-22-16 10:03:12 DONE SEP-22-16 10:03:15 DONE SEP-22-16 10:03:17 DONE SEP-22-16 10:03:28 DONE SEP-22-16 10:03:29 DONE SEP-22-16 10:03:32 DONE 10:03:34 DONE SEP-22-16 10:03:37 DONE SEP-22-16 10:03:39 DONE SEP-22-16 10:03:42 DONE SEP-22-16 10:03:44 DONE SEP-22-16 10:03:47 DONE SEP-22-16 10:03:49 DUSE SEP-22-16 10:03:52 DONE SEP-22-16 10:03:54 DONE SEP-22-16 10:03:57 DONE SEP-22-16 10:03:59 DONE SEP-22-16 10:04:02 DONE SEP-22-16 10:04:04 DONE SEP-22-16 10:04:06 DONE SEP-22-16 10:04:10 DONE SEP-22-16 10:04:12 DONE SEP-22-16 10:04:13 DONE SEP-22-16 10:04:16 DONE SEP-22-16 10:04:19 DONE SEP-22-16 14:24:56 DONE SEP-22:..16 14:24:56 DONE Batch ID: 1596408 Calibration Date 27-AUG-16 14:32 27-AUG-16 14:32 27-AUG-16 14:32 28-AUG-16 16:08 27-AUG-16 14:33 27-AUG-16 14:33 27-AUG-16 14:34 08-SEP-16 11 :00 08-SEP-16 15:33 08-SEP-16 11 :00 08-SEP-16 11 :O 1 08-SEP-16' 11 :01 08-SEP-16 12:36 08-SEP-16 12:37 08-SEP-16 12:37 08-SEP-16 11:01 08-SEP-16 12:37 08-SEP-16 12:37 08-SEP-16 11 :02 08-SEP-1611:02 08-SEP-16 12:38 08-SEP-16 11 :03 08-SEP-16 11 :03 09-SEP-16 11 :41 09-SEP-16 11 :41 09-SEP-16 11 :42 09-SEP-16 13:32 09-SEP-16 11 :43 09-SEP-16 13:32 09-SEP-16 11 :43 09-SEP-16 11 :43 09-SEP-16 11 :44 09-SEP-16 11 :44 09-SEP-16 11 :44 09-SEP-16 12:25 09-SEP-16 12:25 09-SEP-16 11 :44 09-SJ=P-16 11 :44 09-SEP-16 11 :46 09-SEP-16 11 :46 09-SEP-16 11 :46 09-SEP-16 11 :46 27-AUG-16 14:32 27-AUG-16 14:32 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 1203621740 DUP HAKB 1014 SEP-22-16 14:24:56 DONE 27-AUG-16 14:32 1203621741 LCS HAKB 1015 SEP-22-16 14:24:56 DONE 27-AUG-16 14:32 Page 2035 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596410 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235042 SAMPLE HAKB 1209 SEP-22-16 09:55:59 DUSE 16-SEP-16 12:45 405235043 SAMPLE HAKB 1210 SEP-22-16 09:56:00 DONE 16-SEP-16 11:37 405235044 SAMPLE HAKB 1211 SEP-22-16 09:56:03 DONE 16-SEP-16 14:05 405235045 SAMPLE HAKB 1212 SEP-22-16 09:56:06 DONE 16-SEP-16 12:45 405235046 SAMPLE HAKB 1213 SEP-22-16 09:56:08 DONE 16-SEP-16 12:45 405235047 SAMPLE HAKB 1214 SEP-22-16 09:56: 10 DONE 16-SEP-16 12:45 405235048 SAMPLE HAKB 1215 SEP-22-16 09:56: 13 DUSE 16-SEP-16 12:46 405235041 SAMPLE HAKB 1106 SEP-22-16 09:56:16 DONE 06-SEP-16 11 :02 405235049 SAMPLE HAKB 1216 SEP-22-16 09:56:16 DUSE 16-SEP-16 12:46 405235050 SAMPLE HAKB 1217 SEP-22-16 09:56:18 DUSE 16-SEP-16 12:46 405235051 SAMPLE HAKB 1218 SEP-22-16 09:56:21 DONE 16-SEP-16 12:46 405235052 SAMPLE HAKB 1219 SEP-22-16 09:56:24 DONE '16-SEP-16 11 :38 405235053 SAMPLE HAKB 1220 SEP-22-16 09:56:27 DONE 16-SEP-16 11 :38 405235054 SAMPLE HAKB 1221 SEP-22-16 09:56:29 DONE 16-SEP-16 14:16 405235055 SAMPLE HAKB 1222 SEP-22-16 09:56:32 DONE 16-SEP-16 12:49 405235056 SAMPLE HAKB 1223 SEP-22-16 09:56:35 DONE 16-SEP-16 14:05 405235057 SAMPLE HAKB 1224 SEP-22-16 09:56:37 DONE 16-SEP-16 14:17 405235058 SAMPLE HAKB 1225 SEP-22-16 09:56:40 DONE 16-SEP-16 14:05 405235059 SAMPLE HAKB 1226 SEP-22-16 09:56:43 DONE 16-SEP-16 11 :38 405235060 SAMPLE HAKB 1227 SEP-22-16 09:56:45 DONE 16-SEP-16 14:05 1203621745 MB HAKB 1228 SEP-22-16 09:56:47 DONE 16-SEP-1611:38 1203621747 LCS HAKB 1230 SEP-22-16 09:56:52 DONE 16-SEP-16 11 :38 405235042 SAMPLE HAKB 1233 SEP-22-16 16:14:38 DONE 19-SEP-16 15:36 405235048 SAMPLE HAKB 1234 SEP-22-16 16:14:39 DONE 19-SEP-16 15:36 405235049 SAMPLE HAKB 1235 16: 14:41 DONE 19-SEP-16 15:37 405235050 SAMPLE HAKB 1236 SEP-22-16 16:14:43 DONE 19-SEP-16 15:37 1203621746 DUP HAKB 1238 SEP-22-16 16:14:46 DONE 19-SEP-16 15:37 Page 2036 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596411 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235056 SAMPLE HAKB 1197 SEP-22-16 15:53:48 DUSE 15-SEP-16 13:09 405235057 SAMPLE HAKB 1199 SEP-22-16 15:53:49 DONE 15-SEP-16 12:02 405235058 SAMPLE HAKB 1200 SEP-22-16 15:53:52 DONE 15-SEP-16 12:03 405235059 SAMPLE HAKB 1201 SEP-22-16 15:53:55 DONE 15-SEP-16 12:03 405235060 SAMPLE HAKB 1202 SEP-22-16 15:53:57 DONE 15-SEP-16 13:09 1203621748 MB HAKB 1203 SEP-22-16 15:54:00 DONE 15-SEP-16 17:14 1203621749 DUP HAKB 1205 SEP-22-16 15:54:02 DONE 15-SEP-16 12:03 1203621750 LCS HAKB 1206 SEP-22-16 15:54:05 DONE 15-SEP-16 12:03 405235041 SAMPLE HAKB 1210 SEP-22-16 15:55:09 DONE 16-SEP-16 11:37 405235042 SAMPLE HAKB 1211 SEP-22-16 15:55:11 DONE ' 16-SEP-16 14:05 405235043 SAMPLE HAKB 1212 SEP-22-16 15:55:13 DONE 16-SEP-16 12:45 405235044 . SAMPLE HAKB 1213 SEP-22-16 15:55:16 DONE 16-SEP-16 12:45 405235045 SAMPLE HAKB 1214 SEP-22-16 15:55:18 DONE 16-SEP-16 12:45 405235046 SAMPLE HAKB 1216 SEP-22-16 15:55:21 DONE 16-SEP-16 12:46 405235047 SAMPLE HAKB 1218 SEP-22-16 15:55:23 DONE 16-SEP-16 12:46 405235048 SAMPLE HAKB 1219 SEP-22-16 15:55:26 DONE 16-SEP-1611:38 405235049 SAMPLE HAKB 1220 SEP-22-16 15:55:28 DONE 16-SEP-1611:38 405235050 SAMPLE HAKB 1221 SEP-22-16 15:55:56 DONE 16-SEP-16 14:16 405235051 SAMPLE HAKB 1222 SEP-22-16 15:55:58 DUSE 16-SEP-16 12:49 405235052 SAMPLE HAKB 1223 SEP-22-16 15:55:59 DONE 16-SEP-16 14:05 405235053 SAMPLE HAKB 1224 SEP-22-16 15:56:03 DONE 16-SEP-16 14:17 405235054 SAMPLE HAKB 1225 SEP-22-16 15:56:05 DONE 16-SEP-16 14:05 405235055 SAMPLE HAKB 1226 SEP-22-16 15:56:08 DONE 16-SEP-16 11:38 405235051 SAMPLE HAKB 1166 SEP-26-16 11:51:54 DONE 13-SEP-1611:30 405235056 SAMPLE HAKB 1178 SEP-26-16 11 :51 :56 DONE 13-SEP-16 13:06 Page 2037 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596412 Sample Sample Analyst Instrument Run Date Status* Geometry Calibration Date ID Type 1203621752 DUP HAKB 1103 SEP-22-16 09:56:16 DONE 06-SEP-16 11 :02 1203621753 LCS HAKB 1104 SEP-22-16 09:56:16 DONE 06-SEP-16 11 :02 405235041 SAMPLE HAKB 1067 SEP-22-16 09:56:19 DONE 03-SEP-16 15:22 405235042 SAMPLE HAKB 1069 SEP-22-16 09:56:19 DONE 03-SEP-16 15:23 405235043 SAMPLE HAKB 1070 SEP-22-16 09:56:19 DONE 03-SEP-16 15:23 405235044 SAMPLE HAKB 1071 . SEP-22-16 09:56:24 DONE 03-SEP-16 15:23 405235045 SAMPLE HAKB 1072 SEP-22-16 09:56:24 DONE 03-SEP-16 15:23 405235046 SAMPLE HAKB 1073 SEP-22-16 09:56:24 DONE 03-SEP-16 15:23 405235047 SAMPLE HAKB 1074 SEP-22-16 09:56:24 DONE 03-SEP-16 15:23 405235048 SAMPLE HAKB 1075 SEP-22-16 09:56:24 DONE 03-SEP-16 15:24 405235049 SAMPLE HAKB 1078 SEP-22-16 09:56:26 DONE 03-SEP-16 15:24 ., 405235050 SAMPLE HAKB 1080 SEP-22-16 09:56:26 DONE' 03-SEP-16 15:24 405235051 SAMPLE HAKB 1081 SEP-22-16 09:56:26 DONE 03-SEP-16 15:24 405235052 SAMPLE HAKB 1082 SEP-22-16 09:56:26 DONE 03-SEP-16 15:24 405235053 SAMPLE HAKB 1089 SEP-22-16 09:56:29 DONE 06-SEP-16 10:59 405235054 SAMPLE HAKB 1090 SEP-22-16 09:56:29 DONE 06-SEP-16 11 :00 405235055 SAMPLE HAKB 1091 SEP-22-16 09:56:29 DONE 06-SEP-16 11 :00 405235056 SAMPLE HAKB 1092 SEP-22-16 09:56:29 DONE 11 :00 405235057 SAMPLE HAKB 1093 SEP-22-16 09:56:29 DONE 06-SEP-16 11 :00 405235058 SAMPLE HAKB 1095 SEP-22-16 09:56:32 DONE 06-SEP-16 11 :01 405235059 SAMPLE HAKB 1096 SEP-22-16 09:56:32 DONE 06-SEP-16 11 :01 405235060 SAMPLE HAKB 1097 SEP-22-16 09:56:32 DONE 06-SEP-16 11:01 1203621751 MB HAKB 1099 SEP-22-16 09:56:32 DONE 06-SEP-16 11 :01 Page 2038 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596417 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235077 SAMPLE KXB2 1206 SEP-19-16 17:40:59 DUSE 15-SEP-16 12:03 405235078 SAMPLE KXB2 1207 SEP-19-16 17:41:01 DONE 12:04 1203621757 MB KXB2 1208 SEP-19-16 17:41:04 DUSE 15-SEP-16 14:36 405235061 SAMPLE KXB2 1161 SEP-19-16 17:41:44 DONE 13-SEP-16 13:45 405235062 SAMPLE KXB2 1162 SEP-19-16 17:41:46 DONE 13-SEP-16 11:19 405235064 SAMPLE KXB2 1166 SEP-19-16 17:41:51 DONE 13-SEP-16 11 :30 405235065 SAMPLE KXB2 1167 SEP-19-16 17:41:54 DONE 13-SEP-1611:21 405235066 SAMPLE KXB2 1169 SEP-19-16 17:41:55 DONE 13-SEP-1611:21 405235067 SAMPLE KXB2 1170 SEP-19-16 17:41:58 DONE 13-SEP-1611:21 405235068 SAMPLE KXB2 1175 SEP-19-16 17:42:00 DONE 13-SEP-16 11:21 405235069 SAMPLE KXB2 1176 SEP-19-16 17:42:03 DONE 13-SEP-16 11 :22 405235070 SAMPLE KXB2 1177 SEP-19-16 17:42:05 DONE

13-SEP-1612:10 405235072 SAMPLE KXB2 1179 SEP-19-16 17:49:57 DONE 13-SEP-16 11 :22 405235073 SAMPLE KXB2 1180 SEP-19-16 17:49:59 DONE 13-SEP-16 11 :22 405235074 SAMPLE KXB2 1181 SEP-19-16 17:50:00 DONE 13-SEP-16 12:10 405235075 SAMPLE KXB2 1182 SEP-19-1.6 17:50:04 DONE 14-SEP-16 09:53 405235076 SAMPLE KXB2 1184 SEP-19-16 17:50:05 DONE 13-SEP-16 11 :23 405235071 SAMPLE KXB2 1195 SEP-19-16 17:50:08 DONE 15-SEP-16 12:02 1203621758 DUP KXB2 1189 SEP-19-16 17:56:38 DONE 15-SEP-16 12:01 1203621759 LCS KXB2 1191 SEP-19-16 17:56:39 DUSE 15-SEP-16 13:09 405235063 SAMPLE KXB2 1188 SEP-19-16 18:03:46 DONE 15-SEP-16 17:13 405235077 SAMPLE KXB2 1205 SEP-20-16 11 :28:57 DONE 15-SEP-16 12:03 1203621757 MB KXB2 1207 SEP-20-16 11 :28:59 DONE 15-SEP-16 12:04 1203621759 LCS KXB2 1208 SEP-20-16 11 :29:02 DONE 15-SEP-16 14:36 Page 2039 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596418 Sample Sample Instrument Run Date Status Calibration Date ID Type 405235061 SAMPLE KXB2 1001 SEP-17-16 11 :42:39 . DONE 27-AUG-16 14:30 405235062 SAMPLE KXB2 1002 SEP-17-1611:42:39 DONE 27-AUG-16 14:30 405235063 SAMPLE KXB2 1003 SEP-17-16 11 :42:39 DONE 28-AUG-16 16:08 405235065 SAMPLE KXB2 1006 SEP-17-16 11:42:39 DONE 27-AUG-16 14:31 1203621760 MB KXB2 1004 SEP-17-1611:42:39 DONE 27-AUG-16 14:31 405235066 SAMPLE KXB2 1010 SEP-17-1611:42:40 DONE 28-AUG-16 16:08 405235067 SAMPLE KXB2 1011 SEP-17-1611:42:40 DONE 27-AUG-16 14:32 405235068 SAMPLE KXB2 1012

SEP-17-1611:42:40 DONE 27-AUG-16 14:32 1203621760 MB KXB2 1008 SEP-17-1611:42:40 DONE 27-AUG-16 14:31 405235069 SAMPLE KXB2 1013 SEP-17-1611:42:41 DONE 27-AUG-16 14:32 405235070 SAMPLE KXB2 1014 SEP-17-1611:42:41 DONE 27-AUG-1614:32 405235071 SAMPLE KXB2 1015 SEP-17-1611:42:41 DONE 27-AUG-16 14:32 405235072 SAMPLE KXB2 1016 SEP-17-1611:42:41 DONE 27-AUG-16 14:32 405235073 SAMPLE KXB2 1017 SEP-17-1611:42:41 DONE 27-AUG-16 14:32 405235074 SAMPLE KXB2 1018 SEP-17-1611:42:41 DONE 28-AUG-16 16:08 405235075 SAMPLE KXB2 1020 SEP-17-1611:42:42 DONE 27-AUG-16 14:33 405235076 SAMPLE KXB2 1021 SEP-17-1611:42:42 DONE . 27-AUG-16 14:33 405235077 SAMPLE KXB2 1024 SEP-17-16 11:42:42 DONE 27-AUG-16 14:34 405235078 SAMPLE KXB2 1113 SEP-17-1611:44:34 DONE 08-SEP-16 11 :00 1203621761 DUP KXB2 1114 SEP-17-1611:44:37 DONE 08-SEP-16 15:33 1203621762 LCS KXB2 1115 SEP-17-1611:44:39 DONE 08-SEP-16 11 :00 405235061 SAMPLE KXB2 1116 SEP-17-16 11 :44:41 DONE 08-SEP-16 11:01 405235062 SAMPLE KXB2 1117 SEP-17-1611:44:44 DONE 08-SEP-16 11:01 405235063 SAMPLE KXB2 1118 SEP-17-1611:44:46 DONE 08-SEP-16 12:36 405235064 SAMPLE KXB2 1119 SEP-17-16 11 :44:49 DONE 08-SEP-16 12:37 405235065 SAMPLE KXB2 1120 SEP-17-16 11 :44:52 DONE 08-SEP-16 11 :01 405235066 SAMPLE KXB2 1121 SEP-17-1611:44:54 DONE 08-SEP-16 12:37 405235067 SAMPLE KXB2 1122 SEP-17-1611:44:56 DONE 08-SEP-16 11 :01 405235066 SAMPLE KXB2 1124 SEP-17-1611:44:59 DONE 08-SEP-16 12:37 405235069 SAMPLE KXB2 1126 SEP-17-1611:45:01 DONE 08-SEP-16 12:37 405235070 SAMPLE KXB2 1127 SEP-17-16 11:45:04 DONE 08-SEP-16 11 :02 405235071 SAMPLE KXB2 1128 SEP-17-16 11 :45:06 DONE 08-SEP-16 11 :02 405235072 SAMPLE KXB2 1129 SEP-17-16 11:45:08 DONE 08-SEP-16 15:34 405235073 SAMPLE KXB2 1130 SEP-17-1611:45:10 DONE 08-SEP-16 11 :02 405235074 SAMPLE KXB2 1131 SEP-17-16 11:45:13 DONE 08-SEP-16 11 :02 405235075 SAMPLE KXB2 1132 SEP-17-1611:45:16 DONE 08-SEP-16 12:38 405235076 SAMPLE KXB2 1133 SEP-17-1611:45:18 DONE 08-SEP-16 11 :03 405235077 SAMPLE KXB2 1134 SEP-17-1611:45:20 DONE 08-SEP-:16 11 :03 405235078 SAMPLE KXB2 1139 SEP-17-1611:45:23 DONE 09-SEP-16 11:41 1203621761 DUP KXB2 1140 SEP-17-1611:45:25 DONE 09-SEP-1611:41 1203621762 LCS KXB2 1142 SEP-17-1611:45:28 DONE 09-SEP-16 11 :42 405235064 SAMPLE KXB2 1154 SEP-19-16 15:47:38 DONE 09-SEP-16 12:25 Page 2040 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596420 Sample Sample Analyst Instrument Run Date Status Geometry ' Calibration Date 10 Type 405235061 SAMPLE KXB2 1162 SEP-22-16 09:59:26' DONE 13-SEP-1611:19 405235062 SAMPLE KXB2 1163 SEP-22-16 09:59:28 DONE 13-SEP-16 11:20 405235063 SAMPLE KXB2 1166 SEP-22-16 09:59:30 DONE 13-SEP-16 11 :30 405235064 SAMPLE KXB2 1167 SEP-22-16 09:59:33 DONE 13-SEP-1611:21 405235065 SAMPLE KXB2 1169 SEP-22-16 09:59:35 DONE 13-SEP-16 11 :21 405235066 SAMPLE KXB2 1170 SEP-22-16 09:59:38 DONE 13-SEP-16 11:21 405235067 SAMPLE KXB2 1175 SEP-22-16 09:59:40 DONE 13-SEP-16 11 :21 405235068 SAMPLE KXB2 1176 SEP-22-16 09:59:42 DONE 13-SEP-16 11 :22 405235069 SAMPLE KXB2 1177 SEP-22-16 09:59:45 DONE 13-SEP-16 12:10 405235070 SAMPLE KXB2 1179 SEP-22-16 09:59:48 DONE 13-SEP-16 11:22 405235071 SAMPLE KXB2 1180 09:59:50 DONE 13-SEP-1611:22 405235072 SAMPLE KXB2 1181 SEP-22-16 09:59:52 DONE 13-SEP-16 12:10 405235073 SAMPLE KXB2 1182 SEP-22-16 09:59:55 DONE 14-SEP-16 09:53 . 405235074 SAMPLE KXB2 1184 SEP-22-16 09:59:57 DONE 13-SEP-1611:23 405235075 SAMPLE KXB2 1185 SEP-22-16 10:00:00 DONE 15-SEP-16 12:01. 405235076 SAMPLE KXB2 1186 SEP-22-16 10:00:02 DONE 15-SEP-16 17:13 405235078 SAMPLE KXB2 1189 SEP-22-16 10:00:04 DONE 15-SEP-16 12:01 1203621766 MB KXB2 1191 SEP-22-16 10:00:10 DONE 15-SEP-16 13:09 1203621767 DUP KXB2 1195 SEP-22-16 10:00:12 DONE 15-SEP-16 12:02 1203621768 LCS KXB2 1197 SEP-22-16 10:00:14 DONE 15-SEP-16 13:09 405235077 SAMPLE KXB2 1188 SEP-22-16 10:30:55 DONE 15..:SEP-16 17:13 Page 2041of5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1596421 Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235061 SAMPLE KXB2 1065 SEP-17-1611:42:34 DONE 03-SEP-16 15:22 405235062 SAMPLE KXB2 1066 SEP-17-1611:42:34 DONE 03-SEP-16 15:22 405235063 SAMPLE KXB2 1067 SEP-17-16 11 :42:34 DONE 03-SEP-16 15:22 405235064 SAMPLE KXB2 1068 SEP-17-1611:42:34 DONE 03-SEP-16 15:23 405235065 SAMPLE KXB2 1069 SEP-17-1611:42:34 DONE 03-SEP-16 15:23 405235066 SAMPLE KXB2 1070 SEP-17-1611:42:34 DONE 03-SEP-16 15:23 405235067 SAMPLE KXB2 *1071 SEP-17-1611:42:35 DONE 03-SEP-16 15:23 405235068 SAMPLE KXB2 1072 SEP-17-16 11 :42:35 DONE 03-SEP-16 15:23 405235069 SAMPLE KXB2 1073 SEP-17-1611:42:35 DONE 03-SEP-16 15:23 405235070 SAMPLE KXB2 1074 SEP-17-16 11 :42:35 DONE 03-SEP-16 15:23 405235071 SAMPLE KXB2 1075 SEP-17-1611:42:35 DONE 03-SEP-16 15:24 405235072 SAMPLE KXB2' 1078 SEP-17-16 11 :42:36 DONE 03-SEP-16 15:24 405235073 SAMPLE KXB2 1080 SEP-17-16 11 :42:36 DONE 03-SEP-16 15:24 405235074 SAMPLE KXB2 1081 SEP-17-1611:42:36 DONE 03-SEP-16 15:24 405235075 SAMPLE KXB2 1082 SEP-17-16 11:42:36 DONE 03-SEP-16 15:24 405235076 SAMPLE KXB2 1083 SEP-17-16 11 :42:37 DONE 03-SEP-16 15:24 405235077 SAMPLE KXB2 1084 SEP-17-16 11:42:37 DONE 03-SEP-16 15:24 405235078 SAMPLE KXB2 1085 SEP-17-16 11 :42:37 DONE 15:25 1203621769 MB KXB2 1086 SEP-17-16 11:42:37 DONE 03-SEP-16 15:25 1203621770 DUP KXB2 1088 SEP-17-16 11:42:37 DONE 03-SEP-16 15:25 1203621771 LCS KXB2 1169 SEP-17-16 11 :44:20 DONE 11 :21 Page 2042 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1599981 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date \ ID Type 405235078 SAMPLE KXB2 1078 . SEP-22-16 17:52:55 DONE 03-SEP-16 15:24 1203630763 MB KXB2 1080 SEP-22-16 17:52:55 DONE 03-SEP-16 15:24 1203630764 DUP KXB2 1081 SEP-22-16 17:52:55 DONE 03-SEP-16 15:24 1203630765 LCS KXB2 1082 SEP-22-16 17:52:55 DONE 03-SEP-16 15:24 405235061 SAMPLE KXB2 1240 SEP-22-16 17:53:41 DONE 19-SEP-16 15:37 405235062 SAMPLE KXB2 1241 SEP-22-16 17:53:42 DONE 19-SEP-16 15:37 405235063 SAMPLE KXB2 1242 SEP-22-16 17:53:46 DONE 19-SEP-16 15:38 405235064 SAMPLE KXB2 1243 SEP-22-16 17:53:48 DONE 19-SEP-16 15:38 405235065 *SAMPLE KXB2 1244 SEP-22-16 17:53:51 DONE 1'9-SEP-16 15:38 405235066 SAMPLE KXB2 1245 SEP-22-16 17:55:36 DONE 19-SEP-16 15:38 405235067 SAMPLE KXB2 1246 SEP-22-16 17:55:38 DONE 19-SEP-16 15:38 405235068 SAMPLE KXB2 1247 SEP-22-16 17:55:39 DONE 19-SEP-16 15:39 405235069

SAMPLE KXB2 1248 SEP-22-16 17:55:43 DONE 19-SEP-16 15:39 405235070 SAMPLE KXB2 1249 SEP-22-16 17:55:45 DONE 19-SEP.:15 15:39' 405235071 SAMPLE KXB2 1250 SEP-22-16 17:55:47 DONE 19-SEP-16 15:39. 405235072 SAMPLE KXB2 1251 SEP-22-16 17:55:50 DONE 19-SEP-16 15:39 405235073 SAMPLE KXB2 1252 . SEP-22-16 17:55:53 DONE 19-SEP-16 15:40 405235074 SAMPLE KXB2 1253 SEP-22-16 17:55:55 DONE 19-SEP-16 15:40 405235075 SAMPLE KXB2 1254 SEP-22-16 17:55:56 DONE 19-SEP-16 15:40 405235076 SAMPLE KXB2 1255 SEP-22-16 17:55:59 DONE 19-SEP-16 15:40 405235077 SAMPLE KXB2 1256 SEP-22-16 17:56:01 DONE 19-SEP-16 15:40 Page 2043 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1601257 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235051 SAMPLE KXB2 1007 SEP-29-16 14:04:46 DONE 27-SEP-16 14:31 405235051 SAMPLE KXB2 1012 SEP-29-16 14:04:46 DONE 27-SEP-16 14:33 1203633742 MB KXB2 1009 SEP-29-16 14:04:46 DONE 27-SEP-16 14:31 1203633742 MB KXB2 1011 SEP-29-16 14:04:46 DONE 27-SEP-16 17:14 1203633743 DUP KXB2 1008 SEP-29-16 14:04:46 DONE 27-SEP-16 14:31 1203633744 LCS KXB2 1010 SEP-29-16 14:04:46 DONE 27-SEP-16 14:31 1203633743 DUP KXB2 1020 SEP-29-16 14:04:55 DONE 27-SEP-16 14:34 1203633744 LCS KXB2 1021 SEP-29-16 14:04:55 DONE 27-SEP-16 14:35 Page 2044 of 5809 Instrument Run Log Instrument Type: ALPHA SPECTROMETER Batch ID: 1602285 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID *Type 405235021 SAMPLE MXS2 1069 SEP-29-16 21 :26:39 DONE 03-SEP-16 15:23 405235022 SAMPLE MXS2 1070 SEP-29-16 21 :26:39 DONE 03-SEP-16 15:23 405235023 SAMPLE MXS2 1084 SEP-29-16 21:26:41 DONE 03-SEP-16 15:24 405235024 SAMPLE MXS2 1088 SEP-29-16 21 :26:41 DONE 03-SEP-16 15:25 405235025 SAMPLE MXS2 1089 SEP-29-16 21 :26:42 DONE 06-SE;P-16 10:59 405235026 SAMPLE MXS2 1090 SEP-29-16 21 :26:42 DONE 06-SEP-16 11 :00 405235027 SAMPLE MXS2 1091 SEP-29-16 21:26:42 DONE 06-SEP-16 11 :00 405235028 SAMPLE MXS2 1093 SEP-29-16 21:26:42 DONE 06-SE;P-16 11 :00 1203636290 MB MXS2 1092 SEP-29-16 21 :26:42 DONE 06-SEP-16 11 :00 405235029 SAMPLE MXS2 1096 SEP-29-16 21 :26:43 DONE 06-SEP-1611:01 405235030 SAMPLE MXS2 1097 SEP-29-16 21:26:43 DONE 06-SEP-16 11 :01 405235031 SAMPLE MXS2 1099 SEP-29-16 21 :26:43 DONE 11:01 405235032 SAMPLE MXS2 1107 SEP-29-16 21:26:44 DONE 06-SEP-16 11 :02 405235033 SAMPLE MXS2 1108 SEP-29-16 21:26:44 DONE 06-SEP-16 11:02 405235034 SAMPLE MXS2 1109 SEP-29-16 21:26:44 DONE 06-SEP-16 11 :02 405235035 SAMPLE MXS2 1110 SEP-29-16 21:26:44 DONE 06-SEP-16 11 :02 405235036 SAMPLE MXS2 1112 SEP-29-16 21:26:44 DONE 06-SEP-16 11 :03 405235037 SAMPLE MXS2 1249 SEP-29-16 21 :52:30 DUSE* 19-SEP-16 15:39 405235038 SAMPLE MXS2 1250 SEP-29-16 21 :52:33 DONE 19-SEP-16 15:39 405235039 SAMPLE MXS2 1251 SEP-29-16 21 :52:36 DONE 19-SEP-16 15:39 405235040 SAMPLE MXS2 1252 SEP-29-16 21 :52:38 DONE 19-SEP-16 15:40 1203636291 DUP MXS2 1253 SEP-29-16 21 :52:41 DONE 19-SEP-16 15:40 1203636292 LCS MXS2 1254 SEP-29-16 21 :52:42 DONE 19-SEP-16 15:40 405235037 SAMPLE MXS2 1069 OCT-01-16 13:23:25 DONE 30-SEP-16 12:06 Page 2045 of 5809 Page 2046 of 5809 Gamma Spectroscopy Raw Data Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 09/30/16 Batch# __ l_S_9_8_6_4_7 __ Product: 1-129 / MJWC Dato: 09/30/16 Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. n/a Samples have been blank corrected (If required). n/a Blank correction reoorted Included rtr reaulredl. If activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. ./ If greater than 10* MDA/ MDC, error Is 40% or less. If below the MDA/ MDC. error Is Instrument source check Is within limits. h; llmlts ./ Method RDL/ LLD has been met. ./ lf duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or.less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, ./ Or meets the client's reaulred RER acceotance criteria. Tracer yield Is 15-125%. Carrier yield 25-125%. (Or meets the client's contract acceptance criteria), n /,. Method blank Is less than the RDL/ LLD. ./ .. ---" t;O/n nfJow.ejt _ ...... 1 ... \ Sample was run within hold time. I DER Sam ale was correctlv oreserved If reoulred. if Smears Taken for Radioactive batches. n/a Method Spike and LCS are within 75-1250/o ./' llnr meet-" the client's cri*A*lal. No blank spaces on data forms. ./ All line outs lnltlaled and dated. N.Q .. !l:ruwa:lPtlon ereors Aux data is correct. ./ Client Snecial reoulrements oaoe has been checked. ./ Raw Data and/ or soectrum are Included and ProPerlv statused. J MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and ./ ll!iili!..es verfflptf 1 .. 1. "' ./ llilttb....c:ntered Into ./ Batch,Data Exception Reports {DER} comoleted If aoollcable. / DER Batch Data Exception Reports (DER) second reviewed. / Disposition verified to be comnleted. Aliouot Correction comnlcted If rnnnlred n/a Review sample hlstorlcal results if available ./ (If REMP, results above MDC have been verified by historical results recount or re-analvsls.) Primary Review Performed By:. ____ __ /_1_{;, __ _ Secondary Review Performed Page 2047 of 5809 1563266 1563266 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 30-SEP-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1598647 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE EML HASL-300,1-01 Modified Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception
Description:
DER Report No.: 1563266 Revision No.: 1 Type: Process Client Code: MJWC Sample received out of holding: Samples analyzed in a timely manner upon receipt. Reporting results. 405235 041,042,043,044,045,046,047 ,048,049, 050,051,052,053,054,055,056,057,058, 059,060 QC 1203627503DU P, 1203627504MS Originator's Name: Data Validator/Group Leader: Spencer Collins 30-SEP-16 Bryan Williams 30-SEP-16 Page 1 Page 2048of5809 I-129 Queue Sheet 09114/2016 Hatch #: 159864 7 Analyst: MJHl First Client Due Datc:l0/0412016 Internal Due Datc:09/30/2016 Spike Isotope: I-129 Spike Code: )l1/0 -K LCS Isotope: .I-129 LCS Code: P*ilO-K Prep Datc:£/*2."7*lb Sample rn 405235041*1 4052.35().12-1 4051.35043-1 405235044-1 -105235045-1 -105235046-1 405235048-1 405235049-1 ..105235050-1 405235051-1 405235052-1 40523SO:i3*1 405235054-1 405235055-l -105235056-1 405235057-1 405235058-1 -105235059-1 405235060-l i 203627503-1 12036!i504-l 1103627505-l Client Description 4 .. 40.R.l.4 4.40 .. R.2..J 4.4D .. R..2 .. 4 4.40.R.4.? 4 .... m .. R.5 .. 2 4.51\..R.l..J 4.SA.R..l.4 4..SB.R..1.2 4..SB.R.1.3 4..56.R.J.4 4.SS.R..2..J 4.5B .. R.2.4 4.SC.R.5 .. 2 -l.SC .. R .. J..J -l.SC .. R .. 1.-l 4 .. SC .. R.l.2 4.5C.R.l..3 4.5C .. R .. 2.4 5.IA..R.J.2 S.IA.R.l..3 MB for 159S64i 4.4D .R. DUP) 4.40.R.l.4(405235041;\fS) LCS for batd1 1598647 GEL Laboratories LLC, Radiocltemistry Division Expiration Date: 3-3c-11 Expiration Date: 3-3c-n Pipette ID: P-i1'i i 'l t Hazard TyJ>e Code RDL SAMPLE I pCUg SAMPLE l pCifg S,'\J'.-1PLE I pCi/g SAMPLE 1 pCilg SAMPLE I pCi!g, SAMPLE l pCilg SAMPLE I pCi!g SAMPLE 1 pCi/g SAMPLE 1 pCilg SAMPLE l pCi/g SAMPLE I pCi!g SAl\IPLE I pCi/g S,'\J'\1PLE l pCi/g SAMPLE I pCilg SAMPLE I pCi/g SAMPLE I pCUg SAMPLE 1 pCUg SAMPLE l pCi/g SAMPLE 1 pCUg SAMPLE I pCifg MB I pCi/g our t pCifg MS I pCi/g LCS 1 pCifg Vol: 0,1'"'-'-l Vol:o,1 ........ L Nominal Concc11tratio11:_....;Nil...="l..--'------Nominal Conccntration:_.:..;N-\..,,,' :i:-. __ _ Witncss:-.-:...Nh..:.:..' ...;..__ __ fS..\t,>-;Nc.;;:'. i"l'fS'Si-S-6 C!f;J (mLo@ Client We-t . Auswr.ls) Matrix Collect Date MJWCOOI SOIL *; .b'--\ 30-NOV-15 13:27i)j j *:,.le MJWCOOl SOIL ;.E2 30-Z'OV-JS 13:53Dl( '$.<-; 0 MJWCOOl SOIL *-3.0i Z.'57 MJWCOOl SOIL *;.21 30-NOV-1513:50:12-'-ib M.JWCOOl SOIL 'cl , I:;; 30-)>QV-15 14:15 1 ;.12.. MJWCOOI SOlL *;.112.. 07-DEC-15 10:02 Oi.l 3 .. \'9 MJWCOOI SOIL l.l. Oi-DEC-15 10:10 D7i 3-"'!7 MJWCOOl SOIL 07-DEC-15 13:28 vri MJWCOOl SOIL q."'{Lj 07-DEC-IS 13:33 i1t j ; \, l MJWCOOJ SOIL Oi-DEC-1513:42 Dtj 2 _L\ "i MJWCOOJ SOIL J.l.\'.l 07-DEC-15 13:02 ml 3. '{ D MJWCOOt SOIL *3 .. 2(,, 07-DEC-15 IJ: II OiiJ 2..I '5 l\1JWCoOJ SOIL ,3.jO 2.lb MJWCOOl SOIL '"' ... -t:"'..:-02-DEC-1514:51 5. t 5 MJWCOOI SOIL *;. .. !'"1 !l2-DEC-I5 J4:5?p;sj 2, SG MJWCOOI SOIL 3 .1:*5" 02-DEC-15 14:50-oit.! 2. (, z. MJWCOO! SOIL 3 1B 02-DEC-1514:55 Di"( 2. MJWCOOI SOIL 2.'-l 02-DEC-15 15:00 :z, Sq MJWCOOJ SOIL ;.J .1.i J6-DEC-15 l2:26m;/ MJWCOOJ SOIL °3 .15 !6-DEC-1512:331>"'...Lj 3."?.iq QC ACCOl:'l"i"T SOIL Cj-27-lh 'Dld 3.10 QC ACCOUNT SOI!. "';.:; 1 30-:\0V-15 l3:27vz_i, '3 .CO QC ACCOUNT SOIL *3.i.o 30-N'0\1-15 l3:?7cy;i 3 -QC ACCOUNT SOIL CJ-21-16 I .I J D2r.tJ -ic Data ReYicwcd By: q/3 (j I 1 b Detector . YJa 10i; -*1---xn Iv!<; f.:1-jMS X.Ylh.1 'ii.. _&JMS f\1.-/If\& ;< L( I MS 'li;-:1--t.s ltJts ;{l /vi*S "'1..1.. !!V'IS :{i; I !J'..A >Cbll-16 X:I )'!.tj ){ S"'I '/.le\ !AS 5 i;> /(/ 1A" ertvt/!i.. Pnge l of J
Weight/Loss Aliquot Correction Report http://prodsvrOl.gel.com:7778/pls/lims/weight_loss_rpts.show _report Weight/Loss Aliquot Correction Report Select What to Correct Aliquot to <.'.1 Ash Dry Weight *.9,; Dry Weight Wet Weight Batch ID: 1598647 Aliquot Correction to Dry Weight for Batch 1598647 :! Sample Id !Aliquot (G) !sample TypejParcnt Sample Id]Loss (Dcc)*jcorrcctcd Aliquot (G)-'1405235041 :13.64. . jsAMPLE [NA 1.1197 *1i264i368189s69S5t -*1405235042 j 3.82 I SAMPLE INA j .1097 13.400653019479009; 1405235043 [3.01 jsAMPLE INA /.1453 12.5724262064l9619; 1405235044 J 3.27 lsAMPLE --!NA 1.2477 I 2.4s992s899242-99i-1405235045 **14.15 fAMPLE INA [.2237 I 3.221299:2252s7384

1405235046 j 3.92 \sAMPLE INA j.1864 13.189154732989702 .["405235047-14.38 ---\SAMPLE I 3.4l3592139s9415oi '14-05235048 ji83 ...... -* --,SAMPLE jNA 1.2288 -j 1405235049 14.44 .,SAMPLE INA 1.1878 .j 3.6057B73081i8374. 1405235050 13.30 jsAMPLE \NA 1.1103 J 2.935721900620517; f405235051 \NA j.1766 j 3.4006:3251018773*3* J405235052 f3.26 \SAMPLE INA :1.1547 Ii 7ss4s93'1632999a: [405235053 f3.10 JsAMPLE fNA :1.3036 .12.15s7400165647121 1405235054 13.85 --. -jsAMPLE INA f.1820 j 3.149o347.6ns7346 [405235055 13.17 jsAMPLE ___ [NA r1930 I :1405235056 Jiss* ... ,SAMPLE JNA 1.3183 I 2.624s25328os5i27; / 3.28 fNA 1.2713 12.389871233785726 . .... ---1405235058 [3.23 js'AMPLE INA 1.1980 J 2.s90262140976851 1405235059 --\SAMPLE !NA" 1.1201 r 3.70423994954408-i; [405235060 \ 3.75 isAMPLE !NA j .0963 I 3.38S54S931a4719a;* F-203627502r___ 1MB !NA JNA __ , ____ _ Ji2o36275o3f3.41 :lour [405235041 ___ :1.1197 f3:ooi6?76243"52s6Q;-,l12036275o4J :3.60 * !Ms 1405235041 *\ .1191 :\ 3.i68926s24243in:

fLcs--*---*---jNi _______ GEL Laboratories LLC j.'.' qi I of I 9/27/2016 6:25 PM Page 2050 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:20:37.15 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235041.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 30-NOV-2015 13:27:00 Acquisition date : 28-SEP-2016 12:50:10 Sample ID I405235041 Sample quantity 3.20000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK* REPORT No peaks were found Page 2051of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:20:38.16 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235041.CNF;l *

Acquisition date 28-SEP-2016 12:50:10 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Analyst initials: MJHl *

Sample ID I405235041 Sample Quantity 3.2000E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -8.575E-01 5.574E+OO I-129 l.760E-01 2.439E-01 Page 2052 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.189E+Ol 8. l 72E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:20:36.44 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2053 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:20:37.52 Nuclide Line Activity Report Flag: "*" = Keyline Page 2054 of 5809 Summary of Nuclide Activity Sample ID : 1405235041 Acquisition date Page : 2 28-SEP-2016 12:50:10 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2055 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235041 None Flags: "T" Tentatively associated Page 2056 of 5809 Acquisition date Page : 3 28-SEP-2016 12:50:10 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:20:39.69 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235041.CNF;l * *Acquisition date 28-SEP-2016 12:50:10 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Nuclide Library : IODINE *

Sample ID I405235041 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.2000E+OO GRAM *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 * -K Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2057 of 5809 Le (pCi/GRAM 3.685E+OO NOT IDENT. 2.895E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:20:40.78 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA *

* * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235041.CNF;l *

Acquisition date 28-SEP-2016 12:50:10 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Nuclide Library : IODINE *

Sample ID I405235041 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.2000E+OO GRAM *

Quantity Err(%) 3.1250E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff.' Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -8.575E-01 5.574E+OO I-129 1.760E-01 2.446E-01 Page 2058 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.588E+OO 2. 571E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2059 of 5809 MDA COUNTS 1.4157 0.0000 0.0000 0.0000 0.7906 3.3136 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:00.31 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235042.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : Z5-SEP-2016 12:22:54 Sample date 30-NOV-2015 13:53:00 Acquisition date : 28-SEP-2016 13:34:32 Sample ID I405235042 Sample quantity 3.40000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2060 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:01.09 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235042.CNF;l *

Acquisition date 28-SEP-2016 13:34:32 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 30-NOV-2015 13:53:00 Analyst initials: MJHl *

Sample ID I405235042 Sample Quantity 3.4000E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1. 769E+OO 5.068E+OO I-129 -9.360E-02 l.811E-01 Page 2061 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.058E+Ol 3.549E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:04:59.62 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2062 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:00.65 Nuclide Line Activity Report Flag: "*" = Keyline Page 2063 of 5809 Summary of Nuclide Activity Sample ID : 1405235042 Acquisition date Page : 2 28-SEP-2016 13:34:32 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2064 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235042 None Flags: "T" Tentatively associated Page 2065 of 5809 Acquisition date Page : 3 28-SEP-2016 13:34:32 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:02.69 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235042.CNF;l *

Acquisition date 28-SEP-2016 13:34:32 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 30-NOV-2015 13:53:00 Nuclide Library : IODINE *

Sample ID I405235042 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.4000E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2066 of 5809 Le (pCi/GRAM 4.429E+OO NOT IDENT. l.294E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:03.84 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235042.CNF;l *

Acquisition date 28-SEP-2016 13:34:32 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 30-NOV-2015 13:53:00 Nuclide Library : IODINE *

Sample ID I405235042 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.4000E+OO GRAM *

Quantity Err(%) 2.9412E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.769E+OO 5.078E+OO I-129 -9.360E-02 1.814E-01 Page 2067 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 5.140E+OO 1. 862E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2068 of 5809 MDA COUNTS 6.1327 5.0891 3.4625 1. 7970 1.8430 3.8759 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:27.19 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235043.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Configuration Background file Background date : 75-SEP-2016 12:22:59 Sample date 30-NOV-2015 13:59:00 Acquisition date : 28-SEP-2016 13:34:57 Sample ID I405235043 Sample quantity 2.57000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: O 00:30:00.00 Elapsed real time: 0 00:30:00.09 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 16.37* 93.14* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 2 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2 0.37 0 0.29 80.85 465.23 78 461 6 1.38E-03173.7 9 2.61E-03 81.5 Flag: "*" = Peak area was modified by background subtraction Page 2069 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:28.01 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235043.CNF;l *

Acquisition date 28-SEP-2016 13:34:57 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *

Sample date 30-NOV-2015 13:59:00 Analyst initials: MJHl *

Sample ID I405235043 Sample Quantity 2.5700E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery : 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15 *, Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.895E+OO 7.942E+OO I-129 -9.043E-02 3.926E-01 Page 2070 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.152E+Ol 7.694E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:26.52 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 . 2 0 Energy 16.37 93.14 Page 2071 of 5809 Area 10 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2 0.37 80.85 0 0.29 465.23 78 461 6 5.32E-03 42.4 9 7.22E-03 27.7 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:27.54 Nuclide Line Activity Report Flag: "*" = Keyline Page 2072 of 5809 Summary of Nuclide Activity Sample ID : 1405235043 Acquisition date Page : 2 28-SEP-2016 13:34:57 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2073 of 5809 Keyline not fo.und Manually edited "M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235043 Page : 3 Acquisition date : 28-SEP-2016 13:34:57 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 16.37 93.14 2 5 2 0.37 0 0.29 Flags: "T" = Tentatively associated Page 2074 of 5809 80.85 78 6 1.38E-03 **** 3.42E-04 465.23 461 9 2.61E-03 **** 3.15E-08 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:29.44 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235043.CNF;l *

Acquisition date 28-SEP-2016 13:34:57 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *

Sample date 30-NOV-2015 13:59:00 Nuclide Library : IODINE *

Sample ID I405235043 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.5700E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO:'[CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2075 of 5809 Le (pCi/GRAM 8.057E+00 NOT IDENT. 2.976E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:30.50 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235043.CNF;l *

Acquisition date 28-SEP-2016 13:34:57 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *

Sample date 30-NOV-2015 13:59:00 Nuclide Library : IODINE *

Sample ID I405235043 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.5700E+OO GRAM *

Quantity Err(%) 3.8911E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( l. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 3.895E+OO 7.971E+OO I-129 -9.043E-02 3.927E-01 Page 2076 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 8.162E+OO 3.948E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2077 of 5809 MDA COUNTS 1.0519 5.3517 4.3235 2.2015 3.3440 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:51.73 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235044.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : Sample date 30-NOV-2015 13:50:00 Acquisition date : Sample ID I405235044 Sample quantity Detector name : XRAY4 Detector geometry: Elapsed live time: 0 00:30:00.00 Elapsed real time: Energy tolerance 1.00000 keV Analyst Initials Abundance limit 75.00000 Sensitivity Batch ID 1598647 Detector SN# 25-SEP-2016 12:23:10 28-SEP-2016 13:35:27 2.46000E+OO GRAM I129 0 00:30:00.09 0.0% MJHl 3.00000 Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 12.94* 1 3 0.56 64.13 61 6 3.33E-04716.8 2 0 16.27* 5 2 0.47 80.80 78 6 2.64E-03 77.9 3 0 63.21* 6 0 0.23 316.00 312 8 3.18E-03 50.8 Flag: "*" = Peak area was modified by background subtraction Page 2078 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:52.43 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235044.CNF;l *

Acquisition date 28-SEP-2016 13:35:27 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *

Sample date 30-NOV-2015 13:50:00 Analyst initials: MJHl *

Sample ID I405235044 Sample Quantity 2.4600E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 6.477E+OO 6.092E+00 I-129 l.401E-02 3.270E-01 Page 2079 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.849E+Ol 7.505E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:51.01 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 12.94 8 3 0.56 64.13 61 6 4.44E-03 49.2 2 0. 16.27 .8 2 0.47 80.80 78 6 4. 64E-03 .41. 9 3 0 63.21 8 0 0.23 316.00 312 8 4.44E-03 35.4 Page 2080 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:52.04 Nuclide Line Activity Report Flag: "*" = Keyline Page 2081 of 5809 Summary of Nuclide Activity Sample ID : I405235044 Acquisition date Page : 2 28-SEP-2016 13:35:27 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags:. "K" "E" Page 2082 of 5809 Keyline not found Manually edited "M" "A" 3 3 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235044 Acquisition date : 28-SEP-2016 13:35:27 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 12.94 1 3 0.56 64.13 61 6 3.33E-04 **** 2.26E-01 0 16.27 5 2 0.47 80.80 78 6 2.64E-03 **** 1.35E+OO 0 63.21 6 0 0.23 316.00 312 8 3.18E-03 **** 5.21E+OO Flags: "T" = Tentatively associated Page 2083 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:53.91 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* ** * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235044.CNF;l *

Acquisition date 28-SEP-2016 13:35:27 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *

Sample date 30-NOV-2015 13:50:00 Nuclide Library : IODINE *

Sample ID I405235044 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.4600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Critical Level Report Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2084 of 5809 Le (pCi/GRAM 7.230E+OO NOT IDENT. 2.729E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:05:55.57 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235044.CNF;l *

Acquisition date 28-SEP-2016 13:35:27 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *

Sample date 30-NOV-2015 13:50:00 Nuclide Library : IODINE *

Sample ID .I405235044 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.4600E+OO GRAM *

Quantity Err(%) 4.0650E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION *

Eff. Cal. date 17-JUN-2016' 08: 18: 14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 6.477E+00 6.196E+OO I-129 1. 401E-02 3.270E-01 Page 2085 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 6.849E+OO 3. 271E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2086 of 5809 MDA COUNTS 0.0000 2.2178 3.3663 2.2941 3.4934 2.4010 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:16.39 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : Z5-SEP-2016 12:23:15 Sample date 30-NOV-2015 14:15:00 Acquisition date : 28-SEP-2016 13:35:51 Sample ID I405235045 Sample quantity 3.22000E+OO GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.02 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2087 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:17.17 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235045.CNF;l * *Acquisition date 28-SEP-2016 13:35:51 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *

Sample date 30-NOV-2015 14:15:00 Analyst initials: MJHl *

Sample ID I405235045 Sample Quantity 3.2200E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 3.540E+OO I-129 1.357E-02 2.408E-01 Page 2088 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.895E+OO 6.873E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:15.67 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2089 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:16.72 Nuclide Line Activity Report Flag: "*" = Keyline Page 2090 of 5809 Summary of Nuclide Activity Sample ID : 1405235045 Acquisition date Page : 2 28-SEP-2016 13:35:51 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2091 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235045 None Flags: "T" Tentatively associated Page 2092 of 5809 Acquisition date Page : 3 28-SEP-2016 13:35:51 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:18.52 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235045.CNF;l *

Acquisition date 28-SEP-2016 13:35:51 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *

Sample date 30-NOV-2015 14:15:00 Nuclide Library : IODINE *

Sample ID I405235045 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.2200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2093 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. 2.172E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generateq 28-SEP-2016 14:06:19.50 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235045.CNF;l *

Acquisition date 28-SEP-2016 13:35:51 Sensitivity : 3.000 *

Detector ID XRAY5 . Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *

Sample date 30-NOV-2015 14:15:00 Nuclide Library : IODINE *

Sample ID I405235045 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.2200E+OO GRAM *

Quantity Err(%) 3.1056E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. 'date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 0.000Et00 I-129 1.357E-02 2.408E-01 Page 2094 of 5809 TPU ( 1. 96-sigma) TPU ( 1 . 96-sigma ) O.OOOE+OO 2.409E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2095 of 5809 MDA COUNTS 0.0000 0.8547 0.0000 0.9231 0.9543 1.0189 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:40.17 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235046.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 7-DEC-2015 10:02:00. Acquisition date : 28-SEP-2016 13:36:13 Sample ID I405235046 Sample quantity 3.19000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 8.15* 63.26* BACKGROUND CORRECTED* SAMPLE PEAK REPORT Area 4 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 1 0.57 0.43 40.00 315.73 38 313 5 2.40E-03 59.0 6 3.36E-03 58.7 Flag: "*" = Peak area was modified by background subtraction Page 2096 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:40.95 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235046.CNF;l *

Acquisition date 28-SEP-2016 13:36:13 Sensitivity 3.000 * *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 7-DEC-2015 10:02:00 Analyst initials: MJHl *

Sample ID I405235046 Sample Quantity 3.1900E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;'5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -6.563E+OO 7.427E+OO I-129 -1.293E-01 2.534E-01 Page 2097 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.188E+OO 2.392E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:39.33 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 . 0 Page 2098 of 5809 Energy 8.15 63.26 Area 6 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.57 40.00 1 0.43 315.73 38 313 5 3.33E-03 40.8 6 4.86E-03 40.0 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:40.53 Nuclide Line Activity Report Flag: "*" = Keyline Page2099of5809 Summary of Nuclide Activity Sample ID : 1405235046 Acquisition date Page : 2 28-SEP-2016 13:36:13 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2100 of 5809 Keyline not found. Manually edited "M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235046 Page : 3 Acquisition date : 28-SEP-2016 13:36:13 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 8.15 63. 26 4 6 0 0.57 1 0.43 Flags: "T" =.Tentatively associated Page 2101of5809 40.00 38 5 2.40E-03 **** 8.98E-03 315.73 313 6 3.36E-03 **** 3.09E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:42.34 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235046.CNF;l *

Acquisition date 28-SEP-2016 13:36:13 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 7-DEC-2015 10:02:00 Nuclide Library : IODINE *

Sample ID I405235046 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.1900E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2102 of 5809 Le (pCi/GRAM 0.000E+OO NOT IDENT. O.OOOE+OO NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 14:06:43.31 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235046.CNF;l *

Acquisition date 28-SEP-2016 13:36:13 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: O 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 7-DEC-2015 10:02:00 Nuclide Library : IODINE *

Sample ID I405235046 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.1900E+OO GRAM *

Quantity Err(%) 3.1348E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 9 6-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -6.563E+OO 7.449E+OO I-129 -1.293E-01 2.537E-01 Page 2103 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 8.015E+OO 2.603E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2104of5809 MDA COUNTS 4.2472 1.4643 0.0000 1.5445 1.5811 1. 6568 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:08.66 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235047.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : Z5-SEP-2016 12:22:54 Sample date 7-DEC-2015 10:10:00. Acquisition date : 28-SEP-2016 14:39:43 Sample ID I405235047 Sample quantity 3.47000E+00 GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2105 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:09.46 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235047.CNF;l *

Acquisition date 28-SEP-2016 14:39:43 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 7-DEC-2015 10:10:00 Analyst initials: MJHl *

Sample ID I405235047 Sample Quantity 3.4700E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -1.191E+OO 5.034E+OO I-129 2.076E-01 1.872E-01 Page 2106of5809 MDA (pCi/GRAM MDA (pCi/GRAM 9.039E+OO 5.167E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:07.98 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2107of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:08.98 Nuclide Line Activity Report Flag: "*" = Keyline Page 2108 of 5809 Summary of Nuclide Activity Sample ID : 1405235047 Acquisition date Page : 2 28-SEP-2016 14:39:43 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2109of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235047 None Flags: "T" Tentatively associated Page 2110of5809 Acquisition date Page : 3 28-SEP-2016 14:39:43 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:10.90 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235047.CNF;l *

Acquisition date 28-SEP-2016 14:39:43 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 7-DEC-2015 10:10:00 Nuclide Library : IODINE *

Sample ID I405235047 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.4700E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2111 of 5809 Le (pCi/GRAM 3.739E+OO NOT IDENT. 2.113E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:11.96 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235047.CNF;l *

Acquisition date 28-SEP-2016 14:39:43 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 7-DEC-2015 10:10:00 Nuclide Library : IODINE *

Sample ID I405235047 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.4700E+OO GRAM *

Quantity Err(%) 2.8818E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:'39:23 Eff. Geometry : I129 *'

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1 . 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.191E+OO 5.038E+OO I-129 2.076E-01 l.883E-01 . Page 2112 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.067E+OO 2.103E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2113of5809 MDA COUNTS 9.8124 0.8482 6.9250 2.6955 2.7645 7.7519 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:35.16 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235048.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 7-DEC-2015 13:28:00. Acquisition date : 28-SEP-2016 14:40:07 Sample ID I405235048 Sample quantity 2.95000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 6.47 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 22 32 0.45 31. 29 29 6 1.24E-02 45.4 Flag: "*" = Peak area was modified by background subtraction Page 2114 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:35.94 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235048.CNF;l * *Acquisition date 28-SEP-2016 14:40:07 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 7-DEC-2015 13:28:00 Analyst initials: MJHl *

Sample ID I405235048 Sample Quantity 2.9500E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -3.373E+OO 1.037E+Ol I-129 -7.582E-02 3.429E-01 Page 2115of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 969E+Ol 6.737E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:34.48 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2116of5809 Energy 6.47 Area 22 Bkgnd 32 FWHM Channel 0.45 31.29 Left 29 Pw Cts/Sec %Err 6 1. 24E-02 45. 4 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:35.48 Nuclide Line Activity Report Flag: "*" Key line Page 2117 of 5809 Summary of Nuclide Activity Sample ID : 1405235048 Acquisition date Page : 2 28-SEP-2016 14:40:07 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2118of5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235048 Page : 3 Acquisition date : 28-SEP-2016 14:40:07 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 6.47 22 32 0.45 31. 29 29 6 1.24E-02 90.8 1.02E-28 Flags: "T" = Tentatively associated Page 2119of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:37.40 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235048.CNF;l *

Acquisition date 28-SEP-2016 14:40:07 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 7-DEC-2015 13:28:00 Nuclide Library : IODINE *

Sample ID I405235048 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.9500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2120of5809 Le (pCi/GRAM 7.670E+OO NOT IDENT. 2.610E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:38.36 *******************************************************************************
GEL Laboratories LLC * * .2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235048.CNF;l *

Acquisition date 28-SEP-2016 14:40:07 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 7-DEC-2015 13:28:00 Nuclide Library : IODINE *

Sample ID I405235048 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.9500E+OO GRAM *

Quantity Err(%) 3.3898E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -3.373E+OO 1.039E+Ol I-129 -7.582E-02 3.430E-01 Page 2121 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 1.050E+Ol 3.447E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2122of5809 MDA COUNTS 6. 3114 5.3517 4.3235 1.1008 1.1147 3.4302 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:58.63 ********************************************************************************

GEL Laboratories 'LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235049.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 7-DEC-2015 13:33:00. Acquisition date : 28-SEP-2016 14:40:29 Sample ID I405235049 Sample quantity 3.61000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.12 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 76.95 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 0 0.54 384.86 380 8 3.89E-03 37.8 Flag: "*" = Peak area was modified by background subtraction Page 2123of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:59.55 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235049.CNF;l *

Acquisition date 28-SEP-2016 14:40:29 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 7-DEC-2015 13:33:00 Analyst initials: MJHl *

Sample ID I405235049 Sample Quantity 3.6100E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.053E+OO 4.316E+OO I-129 9.547E-03 2.228E-01 Page 2124 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.162E+Ol 5 .114E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:57.94 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2125of5809 Energy 76.95 Area 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.54 384.86 380 8 3.89E-03 37.8 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:10:59.00 Nuclide Line Activity Report Flag: "*" = Keyline Page 2126of5809 Summary of Nuclide Activity Sample ID : 1405235049 Acquisition date Page : 2 28-SEP-2016 14:40:29 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2127 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235049 Page : 3 Acquisition date : 28-SEP-2016 14:40:29 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 76.95 7 0 0.54 384.86 380 8 3.89E-03 75.6 1.88E+OO Flags: "T" = Tentatively associated Page 2128of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:01.79 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235049.CNF;l *

Acquisition date 28-SEP-2016 14:40:29 Sensitivity 3.000 *

Detector ID . XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 7-DEC-2015 13:33:00 Nuclide Library : IODINE *

Sample ID I405235049 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity : 3.6100E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29'.CNF;14

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2129 of 5809 Le (pCi/GRAM 4.544E+OO NOT IDENT. l.859E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:02.88 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235049.CNF;l *

Acquisition date 28-SEP-2016 14:40:29 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 7-DEC-2015 13:33:00 Nuclide Library : IODINE *

Sample ID I405235049 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.6100E+OO GRAM *

Quantity Err(%) 2.7701E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.053E+OO 4.349E+OO I-129 9.547E-03 2.228E-01 Page 2130of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.562E+OO 2.229E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2131 of 5809 MDA COUNTS 1.0858 2.2178 2.2442 3.4411 1.1645 2.4010 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:23.01 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235050.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 7-DEC-2015 13:42:00. Acquisition date : 28-SEP-2016 14:40:52 Sample ID I405235050 Sample quantity 2.94000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2132 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:23.84 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235050.CNF;l *

Acquisition date 28-SEP-2016 14:40:52 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 7-DEC-2015 13:42:00 Analyst initials: MJHl *

Sample ID I405235050 Sample Quantity 2.9400E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 1.564E+OO 3. 311E+OO I-129 -8.741E-02 1. 713E-01 Page 2133 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.280E+Ol 2. 772E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:22.34 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2134of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:23.33 Nuclide Line Activity Report Flag: "*" = Keyline Page 2135 of 5809 Summary of Nuclide Activity Sample ID : 1405235050 Acquisition date Page : 2 28-SEP-2016 14:40:52 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2136of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235050 None Flags: "T" Tentatively associated Page 2137 of 5809 Acquisition date Page : 3 28-SEP-2016 14:40:52 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:25.23 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235050.CNF;l * *Acquisition date 28-SEP-2016 14:40:52 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 7-DEC-2015 13:42:00 Nuclide Library : IODINE *

Sample ID I405235050 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.9400E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA:GAMMA]EFF XRAY5 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2138 of 5809 Le (pCi/GRAM 3.930E+00 NOT IDENT. O.OOOE+OO NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:26.24 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* t *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235050.CNF;l *

Acquisition date 28-SEP-2016 14:40:52 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 7-DEC-2015 13:42:00 Nuclide Library : IODINE *

Sample ID I405235050 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.9400E+OO GRAM *

Quantity Err(%) 3.4014E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.564E+OO 3.322E+OO I-129 -8. 741E-02 l.716E-01 Page 2139of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3. 396E+OO l.760E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2140of5809 MDA COUNTS 0.0000 0.8547 0.0000 0.9231 1.9087 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:47.02 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235051.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 7-DEC-2015 13:02:00. Acquisition date : 28-SEP-2016 14:41:12 Sample ID I405235051 Sample quantity 3.40000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.52* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 4 1 0.59 317.02 314 6 2.22E-03 81.7 Flag: "*" = Peak area was modified by background subtraction Page 2141of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:47.90 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* t * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235051.CNF;l *

Acquisition date 28-SEP-2016 14:41:12 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.07 Half life ratio : ***** *

Sample date 7-DEC-2015 13:02:00 Analyst initials: MJHl *

Sample ID I405235051 Sample Quantity 3.4000E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF';5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -6.022E-01 4.921E+OO I-129 -8.983E-02 2.579E-01 Page 2142of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.066E+Ol 4.618E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:46.24 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2143of5809 Energy 63.52 Area 7 Bkgnd 1 FWHM Channel Left 0.59 317.02 314 Pw Cts/Sec %Err 6 3.72E-03 47.9 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:47.42 Nuclide Line Activity Report Flag: "*" = Keyline Page 2144of5809 Summary of Nuclide Activity Sample ID : 1405235051 Acquisition date Page : 2 28-SEP-2016 14:41:12 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: Keyline not found "E" -Manually edited Page 2145of5809 "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235051 Page : 3 Acquisition date : 28-SEP-2016 14:41:12 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.52 4 1 0.59 317.02 314 6 2.22E-03 **** 3.04E+OO Flags: "T" Tentatively associated Page 2146of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:49.52 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235051.CNF;l *

Acquisition date 28-SEP-2016 14:41:12 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.07 Half life ratio : ***** *

Sample date 7-DEC-2015 13:02:00 Nuclide Library : IODINE *

Sample ID I405235051 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.4000E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA. GAMMA] EFF XRAY6 'Il29. CNF; 5 * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM Non-Identified Nuclides Nuclide I-125 I-129 Page 2147of5809 Le (pCi/GRAM 3.370E+OO NOT IDENT. l.188E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:11:50.68 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

*

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235051.CNF;l *

Acquisition date 28-SEP-2016 14:41:12 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.07 Half life ratio : ***** *

Sample date 7-DEC-2015 13:02:00 Nuclide Library : IODINE *

Sample ID I405235051 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.4000E+OO GRAM *

Quantity Err(%) 2.9412E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 -6.022E-01 4. 921E+OO I-129 -8.983E-02 2.581E-01 Page 2148 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.929E+OO 2.612E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2149of5809 MDA COUNTS 1.4157 1.4643 0.0000 1.5445 0.7906 1.6568 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:27.50 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235052.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 7-DEC-2015 13:11:00. Acquisition date : 28-SEP-2016 15:14:01 Sample ID I405235052 Sample quantity 2.75000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.13 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 27.69 10 2 0.60 138.88 135 7 5.69E-03 37.9 Flag: "*" = Peak area was modified by background subtraction Page 2150of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:28.31 ******************'*************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235052.CNF;l * *Acquisition date 28-SEP-2016 15:14:01 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 7-DEC-2015 13:11:00 Analyst initials: MJHl * *Sample ID I405235052 Sample Quantity 2.7500E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery : 1. 00000 Standard Weight : 0. 00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : 'DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6'

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Activity (pCi/GRAM 7.386E+OO Cnt uncert ( 1. 96-sigma) 5.481E+OO Non-Identified Nuclides Nuclide I-129 Page 2151of5809 Key-Line Activity (pCi/GRAM -4. 391E-02 K.L. Cnt Uncert ( 1. 96-sigma) 2.495E-01 MDA (pCi/GRAM 5.720E+OO MDA (pCi/GRAM 5.319E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:26.77 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2152of5809 Energy 27.69 Area 10 Bkgnd FWHM Channel 2 0.60 138.88 Left 135 Pw Cts/Sec %Err 7 5.69E-03 37.9 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:27.88 Nuclide Line Activity Report Nuclide Type: Nuclide Energy Area I-125 27.34 10 30.97 ------35.49 ------Flag: "*" Key line Page 2153 of 5809 %Abn 114.10* 20.30 6.68 %Eff 2.103E+Ol 2.245E+Ol 2.317E+Ol Uncorrected Decay Corr pCi/GRAM pCi7GRAM 2.332E-01 7.386E+OO ------Line Not Found ------Line Not Found 2-Sigma %Error 75.73 Summary of Nuclide Activity Sample ID : 1405235052 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 15:14:01 Number of lines tentatively identified by NID 1 0 1 100.00% Nuclide Type : Nuclide I-125 Hlife 59.40D Uncorrected Decay pCi/GRAM 31. 7 2. 332E-01 Total Activity 2.332E-01 Grand Total Activity 2.332E-01 Flags: "K" "E" Page 2154of5809 Keyline not found Manually edited Decay Corr pCi7GRAM 7.386E+OO 7.386E+00 7.386E+OO Decay Corr 2-Sigma Error 5.593E+OO Manually accepted 2-Sigma %Error Flags 75.73 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235052 None Flags: "T" Tentatively associated Page 2155of5809 Acquisition date Page : 3 28-SEP-2016 15:14:01 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:29.81 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235052.CNF;l * *Acquisition date 28-SEP-2016 15:14:01 Sensitivity 3.000 *

Detector ID . XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 7-DEC-2015 13:11:00 Nuclide Library : IODINE *

Sample ID I405235052 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity : 2.7500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Le (pCi/GRAM 1.875E+00 ----Non-Identified Nuclides Nuclide I-129 Page 2156 of 5809 Le (pCi/GRAM 2.066E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:30.86 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235052.CNF;l *

Acquisition date 28-SEP-2016 15:14:01 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 7-DEC-2015 13:11:00 Nuclide Library : IODINE *

Sample ID I405235052 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity 2.7500E+00 GRAM *

Quantity Err(%) 3.6364E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 7.386E+OO Act Error ( 1. 96-sigma) 5.598E+OO Non-Identified Nuclides Nuclide I-129 Page 2157of5809 Key-Line Activity (pCi/GRAM -4.391E-02 K.L Act error (1.96-sigma) 2.496E-01 TPU ( 1. 96-sigma) 5.598E+OO TPU (1. 96-sigma) 2.503E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 30.97 33.59 35.49 39.58 Page 2158of5809 MDA COUNTS 1. 22 65 5.0891 4.3281 1. 7970 2.7645 0. 9690 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:55.85 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235053.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : Z5-SEP-2016 12:22:59 Sample date 1-DEC-2015 14:24:00. Acquisition date : 28-SEP-2016 15:14:23 Sample ID I405235053 Sample quantity 2.16000E+00 GRAM Detector name : XRAY2 Detector geometry: Il29 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.13 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 6.83 63.40* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 17 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 23 0 0.27 0.25 33 .11 316.33 31 311 5 9. 24E-03 51. 9 9 3.55E-03 49.4 Flag: "*" = Peak area was modified by background subtraction Page 2159of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:56.59 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235053.CNF;l *

Acquisition date 28-SEP-2016 15:14:23 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 1-DEC-2015 14:24:00 Analyst initials: MJHl *

Sample ID I405235053 Sample Quantity 2.1600E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.573E+OO 8.273E+OO I-129 l.925E-01 5.065E-01 Page 2160 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.600E+Ol 1.136E+OO NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:55.16 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2161of5809 Energy 6.83 63.40 Area 17 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 23 0.27 33.11 0 0.25 316.33 31 311 5 9.24E-03 51.9 9 5.00E-03 33.3 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:56.18 Nuclide Line Activity Report Flag: "*" = Keyline Page 2162 of 5809 Summary of Nuclide Activity Sample ID : 1405235053 Acquisition date Page : 2 28-SEP-2016 15:14:23 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2163of5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235053 Page : 3 Acquisition date : 28-SEP-2016 15:14:23 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 6.83 63.40 17 6 23 0.27 0 0.25 -Flags: "T" = Tentatively associated. Page 2164of5809 33.11 31 5 9.24E-03 **** l.93E-26 316.33 311 9 3.55E-03 98.7 1.69E-02 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:57.94 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235053.CNF;l * *Acquisition date 28-SEP-2016 15:14:23 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 1-DEC-2015 14:24:00 Nuclide Library : IODINE *

Sample ID I405235053 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.1600E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2165of5809 Le (pCi/GRAM 9.820E+OO NOT IDENT. 4.645E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:44:59.07 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235053.CNF;l *

Acquisition date 28-SEP-2016 15:14:23 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date l-DEC-2015 14:24:00 Nuclide Library : IODINE *

Sample ID I405235053 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.1600E+OO GRAM *

Quantity Err(%) 4.6296E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.573E+OO 8.379E+OO I-129 l.925E-01 5.068E-01 Page 2166of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 9.048E+OO 5.142E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2167 of 5809 MDA COUNTS 0.0000 4.2814 8.6471 0.0000 2.2293 4.5736 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:19.29 ********************************************************************************

GEL Laboratoriei LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235054.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 2-DEC-2015 14:51:00. Acquisition date : 28-SEP-2016 15:14:44 Sample ID I405235054 Sample quantity 3.15000E+OO GRAM Detector name : XRAY4 Detector geometry: Il29 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.12 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2168 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:20.08 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235054.CNF;l *

Acquisition date 28-SEP-2016 15:14:44 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 2-DEC-2015 14:51:00 Analyst initials: MJHl *

Sample ID I405235054 Sample Quantity 3.1500E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;14 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -8. 401E-01 4.343E+OO I-129 -1. 375E-01 2.508E-01 Page 2169 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 9.421E+OO 4.349E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:18.58 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2170 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:19.62 Nuclide Line Activity Report Flag: "*" Key line Page 2171of5809 Summary of Nuclide Activity Sample ID : I405235054 Acquisition date Page : 2 28-SEP-2016 15:14:44 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2172of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235054 None Flags: "T" Tentatively associated Page 2173 of 5809 Acquisition date Page : 3 28-SEP-2016 15:14:44 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:21.88 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

*

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235054.CNF;l * *Acquisition date 28-SEP-2016 15:14:44 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 2-DEC-2015 14:51:00 Nuclide Library : IODINE *

Sample ID I405235054 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.1500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2174of5809 Le (pCi/GRAM 3.170E+OO NOT IDENT. l.375E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:23.30 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235054.CNF;l *

Acquisition date 28-SEP-2016 15:14:44 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 2-DEC-2015 14:51:00 Nuclide Library : IODINE *

Sample ID I405235054 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.1500E+OO GRAM *

Quantity Err(%) 3.1746E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 -8. 401E-01 4.346E+OO I-129 -1.375E-01 2.512E-01 Page2175 of5809 TPU ( 1. 96-sigma) TPU * ( 1. 96-sigma) 4.362E+OO 2:587E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2176of5809 MDA COUNTS 2.1715 3.3266 0.0000 2.2941 2.3289 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:44.20 ********************************************************************************

GEL Laboratories L0LC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235055.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 2-DEC-2015 14:59:00. Acquisition date : 28-SEP-2016 15:15:08 Sample ID I405235055 Sample quantity 2.56000E+00 GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 46.53* 63.31* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 5 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2 0 0.33 0.32 231.34 314.92 227 310 7 2.51E-03 75.0 8 4.83E-03 40.9 Flag: "*" = Peak area was modified by background subtraction Page 2177of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:45.00 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235055.CNF;l *

Acquisition date 28-SEP-2016 15:15:08 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 2-DEC-2015 14:59:00 Analyst initials: MJHl *

Sample ID I405235055 Sample Quantity 2.5600E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -5.121E-01 7.176E+OO I-129 -8.332E-02 3.612E-01 Page 2178 of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.822E+Ol 8.645E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:43.30 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2179 of 5809 Energy 46.53 63. 31 Area 7 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2 0.33 231.34 0 0.32 314.92 227 310 7 3. 61E-03 51. 2 8 6.67E-03 28.9 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:44.57 Nuclide Line Activity Report Flag: "*" = Keyline Page 2180of5809 Summary of Nuclide Activity Sample ID : 1405235055 Acquisition date Page : 2 28-SEP-2016 15:15:08 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2181of5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235055 Acquisition date : 28-SEP-2016 15:15:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.53 5 2 0.33 231.34 227 7 2.51E-03 **** 7.90E+OO 0 63.31 9 0 0.32 314.92 310 8 4.83E-03 81. 8 3.20E+OO Flags: "T" = Tentatively associated Page 2182of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:46.58 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235055.CNF;l * *Acquisition date 28-SEP-2016 15:15:08 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 2-DEC-2015 14:59:00 Nuclide Library : IODINE *

Sample ID I405235055 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.5600E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2183 of 5809 Le (pCi/GRAM 6.103E+OO NOT IDENT. 2.732E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:45:47.61 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235055.CNF;l *

Acquisition date 28-SEP-2016 15:15:08 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 2-DEC-2015 14:59:00 Nuclide Library : IODINE *

Sample ID I405235055 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.5600E+OO GRAM *

Quantity Err(%) 3.9063E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -5 .121E-01 7.176E+OO I-129 -8.332E-02 3.612E-01 Page 2184 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 7.180E+OO 3.632E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2185 of 5809 MDA COUNTS 1.6265 1. 7094 0.0000 0.9231 0.9543 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:46:08.22 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235056.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 2-DEC-2015 14:50:00. Acquisition date : 28-SEP-2016 15:15:30 Sample ID I405235056 Sample quantity 2.62000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE* PEAK REPORT No peaks were found Page 2186of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:46:08.99 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235056.CNF;l *

Acquisition date 28-SEP-2016 15:15:30 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 2-DEC-2015 14:50:00 Analyst initials: MJHl * *Sample ID I405235056 Sample Quantity*: 2.6200E+OO GRAM *

Batch Number 1598647 Carrier Weight : 0.00000 *

Recovery 1.00000 Standard Weight : 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1. 796E+OO 3.706E+OO I-129 1.665E-01 2.622E-01 Page 2187 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.419E+Ol 9 .133E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:46:07.39 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2188of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:46:08.58 Nuclide Line Activity Report Flag: "*" = Keyline Page 2189of5809 Summary of Nuclide Activity Sample ID : 1405235056 Acquisition date Page : 2 28-SEP-2016 15:15:30 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2190 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235056 None Flags: "T" Tentatively associated Page 2191of5809 Acquisition date Page : 3 28-SEP-2016 15:15:30 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:46:10.36 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235056.CNF;l *

Acquisition date 28-SEP-2016 15:15:30 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 2-DEC-2015 14:50:00 Nuclide Library : IODINE *

Sample ID I405235056 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.6200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2192of5809 Le (pCi/GRAM 4.399E+OO NOT IDENT. 3.112E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 15:46:11.33 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * .. DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235056.CNF;l *

Acquisition date 28-SEP-2016 15:15:30 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 2-DEC-2015 14:50:00 Nuclide Library : IODINE *

Sample ID I405235056 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.6200E+00 GRAM *

Quantity Err(%) 3.8168E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date :* 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 1. 796E+OO 3. 710E+OO I-129 l.665E-01 2.627E-01 Page 2193of5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 3.797E+OO 2.732E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2194 of 5809 MDA COUNTS 0.0000 0.0000 1. 4921 1.5445 1.5811 3.3136 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:10.89 ******************************************************************************** *

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235057.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Configuration Background file Background date : 25-SEP-2016 12:22:54 Sample date 2-DEC-2015 14:55:00. Acquisition date : 28-SEP-2016 15:48:44 Sample ID I405235057 Sample quantity 2.39000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.21 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 65.19* 109.39* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.29 327.85 3 1.84 550.57 321 543 11 1.67E-03 88.7 14 l.69E-03 93.3 Flag: "*" = Peak area was modified by background subtraction Page 2195of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:11.64 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235057.CNF;l * *Acquisition date 28-SEP-2016 15:48:44 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *

Sample date 2-DEC-2015 14:55:00 Analyst initials: MJHl *

Sample ID I405235057 Sample Quantity 2.3900E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff.' File : DKA100: [CANBERRA. GAMMA] EFF XRAYl Il29. CNF; 6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.848E-01 3.588E+OO I-129 6.578E-02 1.475E-01 Page 2196of5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.038E+OO 3.561E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:10.23 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2197of5809 Energy 65.19 109 .. 39 Area 7 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.29 327.85 3 1.84 550.57 321 11 l.81E-03 80.1 543 14 3.52E-03 42.0 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:11.20 Nuclide Line Activity Report Flag: "*" = Keyline Page 2198 of 5809 Summary of Nuclide Activity Sample ID : 1405235057 Acquisition date Page : 2 28-SEP-2016 15:48:44 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2199 of 5809 Keyline not found Manually edited "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235057 Page : 3 Acquisition date : 28-SEP-2016 15:48:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 65.19 109.39 6 6 6 0.29 3 1. 84 Flags: "T" = Tentatively associated Page 2200 of 5809 327.85 321 11 1.67E-03 **** 1.39E+Ol 550.57 543 14 1.69E-03 **** 3.36E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:13.13 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235057.CNF;l *

Acquisition date 28-SEP-2016 15:48:44 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *

Sample date 2-DEC-2015 14:55:00 Nuclide Library : IODINE *

Sample ID I405235057 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.3900E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2201 of 5809 Le (pCi/GRAM 2.919E+00 NOT IDENT. l.439E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:14.21 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235057.CNF;l *

Acquisition date 28-SEP-2016 15:48:44 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *

Sample date 2-DEC-2015 14:55:00 Nuclide Library : IODINE *

Sample ID I405235057 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.3900E+OO GRAM *

Quantity Err(%) 4.1841E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * * '* Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1 . 96-sigma) I-125 2.848E-01 3.589E+OO I-129 6.578E-02 1.476E-01 Page 2202 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.591E+OO 1. 506E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2203 of 5809 MDA COUNTS 7.3593 3.3927 2.5969 8.0864 4.6075 5.8139 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:43.65 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235058.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 2-DEC-2015 15:00:00. Acquisition date : 28-SEP-2016 15:49:08 Sample ID I405235058 Sample quantity 2.59000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.19 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.08* 11 10 0.73 79.41 75 9 2.93E-03 78.4 2 0 53.73 9 2 0.58 267.90 264 7 2.60E-03 40.0 3 0 64.26* 1 7 0.90 320.62 313 9 3.30E-04475.l 4 0 89.35* 11 12 0.44 446.25 436 16 3.06E-03 78.1 5 0 95.86 6 9 0.53 478.85 474 8 1.64E-03111.1 6 0 141.04 16 3 1. 53 705.09 698 14 4.40E-03 35.3 7 0 147.26 15 9 1. 93 736.23 726 18 4.17E-03 53.5 Flag: "*" = Peak area was modified by background subtraction Page 2204 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:44.45 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235058.CNF;l * *Acquisition date 28-SEP-2016 15:49:08 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 2-DEC-2015 15:00:00 Analyst initials: MJHl *

Sample ID I405235058 Sample Quantity 2.5900E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combine0 Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.117E+Ol 9 .119E+OO I-129 -l.884E-01 2.848E-01 Page 2205 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM l.302E+Ol 4.781E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:42.96 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 13.34 7 24 0.19 65.67 62 8 1. 82E-03135. 7 2 0 16.08 25 10 o .. 73 79.41 75 9 6.88E-03 31. 4 3 0 53.73 9 2 0.58 267.90 264 7 2.60E-03 40.0 4 0 64. 26 6 7 0.90 320.62 313 9 1.78E-03 82.7 5 0 89.35 12 12 0.44 446.25 436 16 3.36E-03 70.2 6 0 95.86 6 9 0.53 478.85 474 8 l.64E-03111.l 7 0 141.04 16 3 1. 53 705.09 698 14 4.40E-03 35.3 8 0 147.26 15 9 1. 93 736.23 726 18 4.17E-03 53.5 Page 2206 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:44.01 Nuclide Line Activity Report Flag: "*" = Keyline Page 2207 of 5809 Summary of Nuclide Activity Sample ID : 1405235058 Acquisition date Page : 2 28-SEP-2016 15:49:08 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2208 of 5809 Keyline not found Manually edited "M" "A" 7 7 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235058 Acquisition date : 28-SEP-2016 15:49:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.08 11 10 0.73 79.41 75 9 2.93E-03 **** 1.94E-04 0 53.73 9 2 0.58 267. 90 2 64 7 2.60E-03 80.l 5.58E-01 0 64.26 1 7 0.90 320.62 313 9 3.30E-04 **** l.21E-02 .o 89.35 11 12 0.44 446.25 .436 16 3.06E-03 **** l.92E-07 0 95.86 6 9 0.53 478.85 474 8 l.64E-03 **** 8.51E-09 0 141.04 16 3 1. 53 705.09 698 14 4.40E-03 70.6 9.62E-19 0 147.26 15 9 1. 93 736.23 726 18 4.17E-03 **** 3.70E-20 Flags: "T" = Tentatively associated Page 2209 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:46.83 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235058.CNF;l * *Acquisition date 28-SEP-2016 15:49:08 Sensitivity 3.000 *

Detector ID : XRAY2 Energy tolerance: 1.000 * *Elapsed live time:* 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 2-DEC-2015 15:00:00 Nuclide Library : IODINE *

Sample ID I405235058 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 2.5900E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2210 of 5809 Le (pCi/GRAM 5.200E+OO NOT IDENT. l.959E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:49:48.36 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235058.CNF;l *

Acquisition date 28-SEP-2016 15:49:08 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 2-DEC-2015 15:00:00 Nuclide Library : IODINE *

Sample ID I405235058 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 2.5900E+OO GRAM *

Quantity Err(%) 3.8610E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.117E+Ol 9.327E+OO I-129 -1.884E-01 2.855E-01 Page 2211 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 1.060E+Ol 2.978E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2212 of 5809 MDA COUNTS 16.8305 12.8441 6.4853 5.5038 7.8027 5.7170 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:08.90 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235059.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 75-SEP-2016 12:23:10 Sample date 16-DEC-2015 12:26:00 Acquisition date : 28-SEP-2016 15:49:42 Sample ID I405235059 Sample quantity 3.70000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.20 0.0% Energy tolerance : 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 10.08* 30 15 1. 29 49.76 44 12 8.37E-03 33.2 2 0 19.09* 5 13 0.45 94.89 89 13 1.41E-03158.7 3 0 97.51 9 0 0.55 487.89 484 8 2.50E-03 33.3 4 0 107.46 4 5 0.55 537.76 532 7 1.16E-03102. 4 5 0 165.55 12 5 0.62 828.89 824 10 3.30E-03 45.7 6 0 238.83 9 0 0.53 1196. 22 1191 10 2.50E-03 33.3 7 0 242.32 10 6 0.39 1213.71 1204 12 2.66E-03 61. 0 8 0 260.16 4 3 0.34 1303.15 1295 10 1.19E-03 84.9 Flag: "*" = Peak area was modified by background subtraction Page 2213 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:09.65 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235059.CNF;l * *Acquisition date 28-SEP-2016 15:49:42 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 16-DEC-2015 12:26:00 Analyst initials: MJHl * *Sample ID 1405235059 Sample Quantity 3.7000E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.003E+OO 2.079E+OO I-129 -5.757E-03 l.284E-01 Page 2214of5809 MDA (pCi/GRAM MDA (pCi/GRAM 3.765E+OO 2.740E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:08.23 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 10.08 37 15 1. 29 49.76 44 12 1. 02E-02 26.8 2 .0 19.09 8 . 13 0.45 94.89 89 .13 2.lOE-03105.4 3 0 97.51 9 0 0.55 487.89 484 8 2.50E-03 33.3 4 0 107.46 4 5 0.55 537.76 532 7 1.16E-03102.4 5 0 165.55 12 5 0. 62 828.89 824 10 3.30E-03 45.7 6 0 238.83 9 0 0.53 1196. 22 1191 10 2.50E-03 33.3 7 0 242.32 10 6 0.39 1213. 71 1204 12 2.66E-03 61. 0 8 0 260.16 4 3 0.34 1303 .15 1295 10 l.19E-03 84.9 Page 2215 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:09.22 Nuclide Line Activity Report Flag: "*" = Keyline Page 2216of5809 Summary of Nuclide Activity Sample ID : 1405235059 Acquisition date Page : 2 28-SEP-2016 15:49:42 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2217of5809 Keyline.not found Manually edited "M" "A" 8 8 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235059 Acquisition date : 28-SEP-2016 15:49:42 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 10.08 30 15 1.29 49.76 44 12 8.37E-03 66.5 1. 59E-02 0 19.09 5 13 0.45 94.89 89 13 1. 41E-03 **** 3.41E+OO 0 97.51 9 0 0.55 487.89 484 8 2.50E-03 66.7 3.36E-01 0 107.46 4 5 0.55 537.76 532 7 1.16E-03 ***** .l.39E-01 0 165.55 12 5 0.62 828.89 824 10 3.30E-03 91. 4 5.85E-04 0 238.83 9 0 0.53 1196. 22 1191 10 2.50E-03 66.7 4.36E-07 0 242.32 10 6 0.39 1213.71 1204 12 2.66E-03 **** 3.08E-07 0 260.16 4 3 0.34 1303.15 1295 10 1.19E-03 **** 5.22E-08 Flags: "T" = Tentatively associated Page 2218of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:11.13 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235059.CNF;l *

Acquisition date 28-SEP-2016 15:49:42 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 16-DEC-2015 12:26:00 Nuclide Library : IODINE *

Sample ID I405235059 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity : 3.7000E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14'

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2219 of 5809 Le (pCi/GRAM 1.325E+OO NOT IDENT. 1.030E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:12.20 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235059.CNF;l * *Acquisition date 28-SEP-2016 15:49:42 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 16-DEC-2015 12:26:00 Nuclide Library : IODINE *

Sample ID I405235059 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity 3.7000E+OO GRAM *

Quantity Err(%) 2.7027E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -1.003E+OO 2.086E+OO I-129 -5.757E-03 1.284E-01 Page 2220 of 5809 TPU (1.96-sigma) TPU (1.96-sigma) 2.135E+00 1.285E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2221of5809 MDA COUNTS 4.3431 3.3266 2.2442 3. 4411 3.4934 4.8019 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:32.94 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235060.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 16-DEC-2015 12:33:00 Acquisition date : 28-SEP-2016 15:50:06 Sample ID I405235060 Sample quantity 3.39000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.05 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 26.17 BACKGROUND CORRECTED SAMPLE PEAK*REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 4 3 0.31 129.90 127 5 1. 23E-03 71. 9 Flag: "*" = Peak area was modified by background subtraction Page 2222 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:33.65 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235060.CNF;l * *Acquisition date 28-SEP-2016 15:50:06 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *

Sample date 16-DEC-2015 12:33:00 Analyst initials: MJHl *

Sample ID I405235060 Sample Quantity 3.3900E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 9.795E-01 2.906E+OO I-129 -5. 724E-02 1.192E-01 Page 2223 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.677E+OO 2.536E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:32.31 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2224 of 5809 Energy 26.17 92.44 Area 4 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 3 0.31 129.90 2 0.57 459.98 127 455 5 1. 23E-03 71. 9 9 2.72E-03 42.2 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:33.25 Nuclide Line Activity Report Flag: "*" = Keyline Page 2225 of 5809 Summary of Nuclide Activity Sample ID : 1405235060 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 15:50:06 Number of lines tentatively identified by **** There are no nuclides meeting summary 1 1 NID 0 criteria 0.00% **** .Flags: "K" "E" Page 2226 of 5809 Keyline not found Manually edited "M" F Manually accepted "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235060 Page : 3 Acquisition date : 28-SEP-2016 15:50:06 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 26 .17 4 3 0.31 129.90 127 5 1.23E-03 **** 7.lOE+OO Flags: "T" = Tentatively associated Page 2227 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:35.20 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235060.CNF;l * *Acquisition date 28-SEP-2016 15:50:06 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *

Sample date 16-DEC-2015 12:33:00 Nuclide Library : IODINE *

Sample ID 1405235060 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.3900E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 * *' Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2228 of 5809 Le (pCi/GRAM 2.874E+00 NOT IDENT. 6.677E-02 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:36.45 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235060.CNF;l * *Acquisition date 28-SEP-2016 15:50:06 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *

Sample date 16-DEC-2015 12:33:00 Nuclide Library : IODINE *

Sample ID I405235060 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.3900E+00 GRAM *

Quantity Err(%) 2.9499E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 9.795E-01 2. 911E+OO I-129 -5.724E-02 l.193E-01 Page 2229 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 2.945E+OO l.221E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2230 of 5809 MDA COUNTS 1.6265 1. 7094 0.0000 4.6154 1.9087 1.0189 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:57.88 ********************************************************************************

GEL LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627502.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 27-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 15:50:32 Sample ID I1203627502 Sample quantity 3.70000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.08 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.64* 2 2 0.28 232.54 230 7 5.49E-04190.6 2 0 66.61 7 1 0.49 332.47 329 6 1.84E-03 48.3 3 0 92.79* 9 6 0.57 463.44 459 8 2.44E-03 69.6 Flag: "*" = Peak area was modified by background subtraction Page 2231 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:58.67 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627502.CNF;l *

Acquisition date 28-SEP-2016 15:50:32 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.08 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Analyst initials: MJHl *

Sample ID Il203627502 Sample Quantity 3.7000E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *

Eff. File' : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 -2.144E-02 l.015E-01 I-129 -l.527E-01 1. 947E-01 Page 2232 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM l.930E-01 2.122E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:57.23 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.64 8 2 0.28 232.54 230 7 2.17E-03 46.3 2 0 66.61 7 1 0.49 332.47 329 6 1. 84E-03 48.3 3 0 92.79 16 6 0.57 463.44 459 8 4.46E-03 36.3 Page 2233 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:50:58.25 Nuclide Line Activity Report Flag: "*" = Keyline Page 2234 of 5809 Summary of Nuclide Activity Sample ID : 11203627502 Acquisition date Page : 2 28-SEP-2016 15:50:32 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2235 of 5809 Keyline not found Manually edited "M" "A" 3 3 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I1203627 502 Acquisition date : 28-SEP-2016 15:50:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.64 2 2 0.28 232.54 230 7 5.49E-04 **** 7.69E+OO 0 66.61 7 1 0.49 332.47 329 6 1.84E-03 96. 7 2.49E+00 0 92.79 9 6 0.57 463.44 459 8 2.44E-03 **** 4.0BE-01 Flags: "T" = Tentatively associated Page 2236 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:51:00.06 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627502.CNF;l *

Acquisition date 28-SEP-2016 15:50:32 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.08 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627502 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity : 3.7000E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Elf. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2237of5809 Le (pCi/GRAM 6.750E-02 NOT IDENT. 5.456E-02 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 16:51:01.02 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627502.CNF;l *

Acquisition date 28-SEP-2016 15:50:32 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.08 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627502 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity 3.7000E+OO GRAM *

Quantity Err(%) 2.7027E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.144E-02 1.016E-01 I-129 -l.527E-01 1.953E-01 Page 2238 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 1.020E-01 2. 071E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2239 of 5809 MDA COUNTS 2.8315 4.3929 0.0000 0.7722 3.1623 2.4852 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:04:52.22 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627503.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;476 Background date : 25-SEP-2016 12:20:17 Sample date 30-NOV-2015 13:27:00 Acquisition date : 28-SEP-2016 19:04:24 Sample ID I1203627503 Sample quantity 3.00000E+OO GRAM Detector name : GAM05 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.33 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 0 2 3 3 0 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 Energy 38.74 49.67 62.67* 65.88 72.21 77.43* 86.72* 92.55* 185.60* 197.79* 202.84 238.07* 241.10* 277.03 352.06 387.13 451.80 570.07 583.32* 620.48 685.86 799.61 878.70 903.81 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 12 11 14 20 7 15 14 18 11 8 8 18 12 14 29 13 7 9 7 9 7 12 9 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 39 31 27 25 31 48 18 52 38 25 21 12 20 12 18 8 18 3 9 3 7 2 0 3 0.74 0.95 1. 09 1.10 1. 01 0.90 1. 03 1. 20 1. 26 1. 28 0.76 1. 50 1. 50 1. 41 1.19 1. 64 3.79 0.94 0.95 1. 30 3.58 2. 65 3.94 0.73 79.32 101.15 127.13 133. 55 146.21 156.64 175.20 186.86 372.82 397.20 407.28 477.69 483.75 555.56 705.52 775.60 904.86 1141. 25 1167.73 1242.00 1372. 67 1600. 02 1758.11 1808.29 75 89 122 122 143 153 173 183 368 392 404 470 470 551 700 770 897 1138 1163 1239 1365 1596 1753 1804 7 3.33E-03 91.8 16 3.lOE-03 87.1 8.55E-01 18 3.98E-03 84.3 9.80E-01 18 5.44E-03 51.3 6 1.90E-03135.2 9 4.20E-03 90.6 6 3.85E-03 58.4 9 4.99E-03 92.0 10 3.02E-03120.6 8 2.24E-03126.1 6 2.31E-03 97.0 21 5.03E-03 51.9 9.88E-01 21 3.37E-03 75.3 8 4.02E-03 48.9 13 8.04E-03 36.3 11 3.56E-03 51.6 13 1.96E-03125.3 6 2.57E-03 43.9 9 1. 97E-03 92. 1 6 2.62E-03 43.1 10 l.82E-03 87.6 8 3.32E-03 35.5 10 2.50E-03 33.3 8 2.12E-03 57.1 Flag: "*" = Peak area was modified by background subtraction Page 2240 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:04:53.07 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627503.CNF;l * *Acquisition date 28-SEP-2016 19:04:24 Sensitivity : 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Analyst initials: MJHl *

Sample ID I1203627503 Sample Quantity 3.0000E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 Il29.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2241of5809 Key-Line Activity (pCi/GRAM -9.645E+OO -1.528E-01 K.L. Cnt Uncert ( 1. 96-s igma) 9.502E+OO 3.226E-01 MDA (pCi/GRAM MDA (pCi/GRAM 1.343E+Ol 4.971E-01 NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:04:51.48 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 38.74 12 39 0.74 79.32 75 7 3.33E-03 91. 8 2 2 45.93 46 35 0.94 .93. 67 89 16 1. 27E-02 26.6 8.55E-01 3 2 49.67 11 31 0.95 101.15 89 16 3.lOE-03 87.1 4 3 62. 67 48 27 1. 09 127.13 122 18 l.32E-02 24.6 9.80E-01 5 3 65.88 20 25 1.10 133.55 122 18 5. 44E-03 51. 3 6 0 72.21 7 31 1. 01 146.21 143 6 1.90E-03135.2 7 0 77.43 25 48 0.90 156.64 153 9 6.81E-03 55.3 8 0 86. 72 18 18 1. 03 175.20 173 6 5.12E-03 42.3 9 0 92.55 70 52 1. 20 186.86 183 9 1.94E-02 23.1 10 0 185.60 33 38 1.26 372.82 368 10 9.19E-03 38.8 11 0 197.79 18 25 1. 28 397.20 392 8 4.96E-03 54.5 12 0 202.84 8 21 0.76 407.28 404 6 2. 31E-03 97.0 13 3 238.07 31 12 1. 50 477.69 470 21 8.63E-03 29.4 9.88E-01 14 3 241.10 16 20 1. 50 483.75 470 21 4.37E-03 57.0 15 0 277.03 14 12 1. 41 555.56 551 8 4.02E-03 48.9 16 0 352.06 29 18 1.19 705.52 700 13 8.04E-03 36.3 17 0 387.13 13 8 1. 64 775.60 770 11 3.56E-03 51.6 18 0 451.80 7 18 3.79 904.86 897 13 l.96E-03125.3 19 0 511.16 81 19 2.78 1023.50 1016 16 2.26E-02 16.5 20 0 570.07 9 3 0.94 1141. 25 1138 6 2.57E-03 43.9 21 0 583.32 11 9 0.95 1167.73 1163 9 2.97E-03 59.3 22 0 620.48 9 3 1. 30 1242.00 1239 6 2.62E-03 43.1 23 0 685.86 7 7 3.58 1372. 67 1365 10 1. 82E-03 87.6 24 0 799.61 12 2 2. 65 1600.02 1596 8 3.32E-03 35.5 25 0 878.70 9 0 3.94 1758.11 1753 10 2.50E-03 33.3 26 0 903.81 8 3 0.73 1808.29 1804 8 2.12E-03 57.1 Page 2242 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:04:52.61 Nuclide Line Activity Report Flag: "*" = Keyline Page 2243 of 5809 Summary of Nuclide Activity Sample ID : 11203627503 Acquisition date Page : 2 28-SEP-2016 19:04:24 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2244 of 5809 Keyline not.found Manually edited "M" "A" 24 23 NID 1 criteria **** 4.17% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 11203627503 Acquisition date : 28-SEP-2016 19:04:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 38.74 12 39 0.74 79.32 75 7 3.33E-03 **** 2.73E+Ol T 2 49.67 11 31 0.95 101.15 89 16 3.lOE-03 **** 3.17E+OO 3 62. 67 14 27 1. 09 127.13 122 18 3.98E-03 **** 5.16E-02 3 .. 65. 88 20 25 1.10 133. 55. 122 1.8 5.44E-03 **** l.60E-02 0 72.21 7 31 1. 01 146.21 143 6 l.90E-03 **** l.41E-03 0 77.43 15 48 0.90 156.64 153 9 4.20E-03 **** l.72E-04 0 86.72 14 18 1. 03 175.20 173 6 3.85E-03 **** 3.45E-06 0 92.55 18 52 1. 20 186.86 183 9 4.99E-03 **** 2. 72E-07 0 185.60 11 38 1. 26 372. 82 368 10 3.02E-03 **** 1. 64E-26 0 197.79 8 25 1. 28 397.20 392 8 2.24E-03 **** 3.94E-29 0 202.84 8 21 0.76 407.28 404 6 2.31E-03 **** 3.23E-30 3 238.07 18 12 1. 50 477.69 470 21 5.03E-03 **** O.OOE+OO 3 241.10 12 20 1. 50 483.75 470 21 3.37E-03 **** O.OOE+OO 0 277.03 14 12 1. 41 555.56 551 8 4.02E-03 97.8 O.OOE+OO 0 352.06 29 18 1.19 705.52 700 13 8.04E-03 72.6 O.OOE+OO 0 387.13 13 8 1. 64 775.60 770 11 3.56E-03 **** O.OOE+OO 0 451.80 7 18 3.79 904.86 897 13 1. 96E-03 **** O.OOE+OO 0 570.07 9 3 0.94 1141. 25 1138 6 2.57E-03 8.7. 8 0.00E+OO 0 583.32 7 9 0.95 1167.73 1163 9 1.97E-03 **** O.OOE+OO 0 620.48 9 3 1. 30 1242.00 1239 6 2.62E-03 86.3 O.OOE+OO 0 685.86 7 7 3.58 1372.67 1365 10 1.82E-03 **** O.OOE+OO 0 799.61 12 2 2.65 1600.02 1596 8 3.32E-03 70.9 O:OOE+OO 0 878.70 9 0 3.94 1758.11 1753 10 2.50E-03 66.7 O.OOE+OO 0 903.81 8 3 0.73 1808.29 1804 8 2.12E-03 **** O.OOE+OO Flags: "T" = Tentatively associated Page 2245 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:04:54.68 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627503.CNF;l *

Acquisition date 28-SEP-2016 19:04:24 Sensitivity 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Nuclide Library : IODINE *

Sample ID I1203627503 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.0000E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 Il29.CNF;l5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2246 of 5809 Le (pCi/GRAM 5.978E+OO NOT IDENT. 2.234E-01 FAIL ABUN VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:04:55.79 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * * " DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627503.CNF;l * *Acquisition date 28-SEP-2016 19:04:24 Sensitivity 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Nuclide Library : IODINE *

Sample ID I1203627503 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.0000E+OO GRAM *

Quantity Err ( % ) 3. 3333E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2247 of 5809 Key-Line Activity . (pCi/GRAM -9.645E+OO -1. 528E-01 K.L Act error ( 1. 96-sigma) 9.649E+OO 3.230E-01 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) l.058E+Ol NOT IDENT. 3.303E-01 FAIL ABUN
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * *

* ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2248 of 5809 MDA COUNTS 39.8805 30.2741 17.4184 27.9341 14.8329 14.0959 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:05:48.51 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627504.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 75-SEP-2016 12:22:54 Sample date 30-NOV-2015 13:27:00 Acquisition date : 28-SEP-2016 19:05:16 Sample ID Il203627504 Sample quantity 3.17000E+OO GRAM Detector name : XRAYl Detector geometry: Il29 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.24 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.69 740 84 0.84 148.92 141 20 2.06E-01 4.9 2 0 33.71 159 24 0.56 169.19 161 16 4.42E-02 10.5 3 0 39.62 99 19 0.66 199.00 194 10 2.74E-02 13.1 4 0 42.88 7 7 0.17 215.40 208 9 1. 99E-03 75.3 5 0 140. 71 7 5 0. 21 708.39 700 12 1. 83E-03 83.2 6 0 163.52* 10 0 0.33 823.38 817 14 2.72E-03 39.7 Flag: "*" = Peak area was modified by background subtraction Page 2249 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:05:49.29 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627504.CNF;l * *Acquisition date 28-SEP-2016 19:05:16 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.24 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Analyst initials: MJHl *

Sample ID I1203627504 Sample Quantity 3.1700E+OO GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM l.408E+Ol Cnt uncert ( 1. 96-sigma) 1.357E+OO Non-Identified Nuclides Nuclide I-125 Page 2250 of 5809 Key-Line Activity (pCi/GRAM 3.274E+OO K.L. Cnt Uncert ( 1. 96-sigma) 7.012E+OO MDA (pCi/GRAM 6.167E-01 MDA (pCi/GRAM 1.189E+Ol NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:05:47.86 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.69 740 84 0.84 148.92 141 20 2.06E-01 4. 9 2 .0 33.71 159 . 24 0.56 169.19 161 16 4.42E-02 10.5 3 0 39.62 99 19 0.66 199.00 194 10 2.74E-02 13.1 4 0 42.88 7 7 0.17 215.40 208 9 1.99E-03 75.3 5 0 140.71 7 5 0.21 708.39 700 12 1.83E-03 83.2 6 0 163.52 13 0 0.33 823.38 817 14 3.61E-03 27.7 Page 2251of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:05:48.86 Nuclide Line Activity Report Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error I-129 29.62 740 56.60* 2.200E+Ol 1.408E+Ol 1.408E+Ol 9.83 33.59 159 10.04 2.304E+Ol 1.628E+Ol 1.628E+Ol 21. 01 39.58 99 7.51 2.288E+Ol 1.360E+Ol 1.360E+Ol 26. 27 Flag: "*" Key line Page 2252 of 5809 Summary of Nuclide Activity Sample ID : I1203627504 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 19:05:16 Number of lines tentatively identified by NID 6 3 3 50.00% Nuclide Type : FISSION Nuclide I-129 Hlif e l.57E+07Y Uncorrected Decay pCi/GRAM 1. 00 1. 408E+Ol Total Activity 1.408E+Ol Grand Total Activity 1.408E+Ol Flags: "K" "E" Page 2253 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM l.408E+Ol l.408E+Ol l.408E+Ol Decay Corr 2-Sigma Error 0.138E+Ol Manually accepted 2-Sigma %Error Flags 9.83 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 11203627504 Acquisition date : 28-SEP-2016 19:05:16 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 42.88 7 7 0.17 215.40 208 9 1.99E-03 **** 2.22E+Ol 0 140.71 7 5 0.21 708.39 700 12 1. 83E-03 **** l.09E+OO 0 163.52 10 0 0.33 823.38 817 14 2. 72E-03 79.4 4.69E-01 . Flags: "T" = Tentatively associated Page 2254 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:05:51.01 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100;[CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627504.CNF;l *

Acquisition date 28-SEP-2016 19:05:16 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.24 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Nuclide Library : IODINE *

Sample ID Il203627504 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity : 3.1700E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl' I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 2.827E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2255 of 5809 Le (pCi/GRAM 5.482E+OO NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:05:52.05 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627504.CNF;l * *Acquisition date 28-SEP-2016 19:05:16 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.24 Half life ratio : ***** *

Sample date 30-NOV-2015 13:27:00 Nuclide Library : IODINE *

Sample ID Il203627504 Analyst initials: MJHl *

Batch Number 1598647 Sample Quantity 3.1700E+00 GRAM *

Quantity Err(%) 3.1546E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry* : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1.408E+Ol Act Error ( 1. 96-sigma) 1.945E+OO Non-Identified Nuclides Nuclide I-125 Page 2256 of 5809 Key-Line Activity (pCi/GRAM 3.274E+OO K.L Act error ( 1. 96-sigma) 7.035E+OO TPU ( 1. 96-sigma) 1.945E+OO TPU ( 1. 96-sigma) 7.188E+OO NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2257 of 5809 MDA COUNTS 37.6141 40.7126 41. 5498 8.0864 4.1467 13. 5658 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 10:10:51.66 ********************************************************************************

GEL LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627505.CNF;2 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 27-SEP-2016 00:00:00 Acquisition date : 29-SEP-2016 09:10:18 Sample ID I1203627505 Sample quantity 3.70000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.29 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598647 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED *SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 9 26. 89 13 21 0.64 134.80 132 27 3. 72E-03 62.4 4.89E+OO 2 9 27.44 35 34 0.66 137.61 132 27 9. 72E-03 36.8 3 9 28.12 23 24 0.49 141.00 132 27 6.30E-03 48.1 4 9 29.59 636 48 1.18 148.42 132 27 1.77E-01 5.0 5 0 33.81 180 39 0.87 169.67 163 16 5.00E-02 11. 3 6 0 39.74 71 26 0.91 199.57 193 14 1.97E-02 19.7 7 0 108.39 11 2 0.58 545.53 540 10 2.93E-03 41. 6 8 0 113. 43 9 3 0.60 570.92 565 11 2.62E-03 47.0 Flag: "*" = Peak area was modified by background subtraction Page 2258 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 10:10:52.54 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627505.CNF;2 * *Acquisition date 29-SEP-2016 09:10:18 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.29 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Analyst initials: MJHl * *Sample ID I1203627505 Sample Quantity 3.7000E+00 GRAM *

Batch Number 1598647 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date : 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File :'DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Activity (pCi/GRAM 3.064E-01 1.039E+Ol Cnt uncert ( 1. 96-sigma) 2.210E-01 1.027E+OO Non-Identified Nuclides Nuclide Page 2259 of 5809 Key-Line Activity (pCi/GRAM K.L. Cnt Uncert (1.96-sigma) MDA (pCi/GRAM 2.103E-01 4.395E-01 MDA (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 10:10:50.90 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 9 26. 89 13 21 0.64 134.80 132 27 3.72E-03 62.4 4.89E+OO 2 .9 27.44 35 34 0.66 137.61 132 27 9. 72E-03 36.8 3 9 28.12 23 24 0.49 141.00 132 27 6.30E-03 48.1 4 9 29.59 636 48 1.18 148.42 132 27 l.77E-01 5.0 5 0 33.81 180 39 0.87 169.67 163 16 5.00E-02 11. 3 6 0 39.74 71 26 0.91 199.57 193 14 l.97E-02 19.7 7 0 108.39 11 2 0.58 545.53 540 10 2.93E-03 41. 6 8 0 113. 43 9 3 0.60 570.92 565 11 2.62E-03 47.0 Page 2260 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 10:10:52.00 Nuclide Line Activity Report Nuclide Type: Nuclide Energy Area I-125 27.34 35 30.97 ------35.49 ------Nuclide Type: FISSION Nuclide I-129 Flag: "*" Page 2261of5809 Energy 29.62 33.59 39.58 Key line Area 636 180 71 %Abn 114 .10* 20.30 6.68 %Abn 56.60* 10.04 7.51 %Eff 2.088E+Ol 2.245E+Ol 2.317E+Ol %Eff 2.195E+Ol 2.305E+Ol 2.286E+Ol Uncorrected Decay Corr pCi/GRAM pCi/GRAM 2.980E-01 3.064E-01 ------Line Not Found ------Line Not Found Uncorrected pCi/GRAM 1.039E+Ol 1.577E+Ol 8.399E+OO Decay Corr pCi/GRAM 1.039E+Ol 1.577E+Ol 8.399E+OO " 2-Sigma %Error 73.58 2-Sigma %Error 10.08 22.53 39.30 Summary of Nuclide Activity Sample ID : I1203627505 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 29-SEP-2016 09:10:18 Number of lines tentatively identified by NID 8 4 4 50.00% Nuclide Type : Nuclide I-125 Hlife 59.40D Decay 1. 03 Total Activity Nuclide Type : FISSION Nuclide Hlife I-129 l.57E+07Y Decay 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 2.980E-01 ---------2.980E-01 Uncorrected pCi/GRAM 1.039E+Ol ---------1.039E+Ol 1. 069E+Ol Flags: '"K" "E" Keyline not found Manually edited Page 2262 of 5809 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 3.064E-01 2.255E-01 73.58 ---------3.064E-01 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 1.039E+Ol 0.105E+Ol 10.08 ---------1.039E+Ol 1.070E+Ol accepted "M" "A" Nuclide specific abn. limit Flags Flags Unidentified Energy Lines Page : 3 Sample ID : 11203627505 Acquisition date : 29-SEP-2016 09:10:18 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 9 26. 89 13 21 0.64 134.80 132 27 3. 72E-03 **** 2.05E+Ol 9 28.12 23 24 0.49 141.00 132 27 6.30E-03 96.1 2.13E+Ol 0 108.39 11 2 0.58 545.53 540 10 2.93E-03 83.3 3.48E+OO 0 113. 43 9 3 0.60 570.92 565 11 2. 62E.-03 93.9 2.92E+OO Flags: "T" = Tentatively associated Page 2263 of 5809 VAX/VMS'Nuclide Identification Report Generated 29-SEP-2016 10:10:54.45 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627505.CNF;2 * *Acquisition date 29-SEP-2016 09:10:18 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.29 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627505 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity : 3.7000E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : 1129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 LC (pCi/GRAM 9.331E-02 1.978E-01 ----Non-Identified Nuclides Nuclide Page 2264 of 5809 Le (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 10:10:55.56 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

* *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627505.CNF;2 * *Acquisition date 29-SEP-2016 09:10:18 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.29 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627505 Analyst initials: MJHl * *Batch Number 1598647 Sample Quantity 3.7000E+00 GRAM *

Quantity Err(%) 2.7027E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11: 39: 23 Eff. Geometry * : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 I-129 3.064E-01 1.039E+Ol Act Error ( 1. 96-sigma) 2.269E-01 1.465E+OO Non-Identified Nuclides Nuclide Page 2265 of 5809 Key-Line Activity (pCi/GRAM K.L Act error ( 1. 96-sigma) TPU ( 1. 96-sigma) 2.269E-01 1.465E+OO TPU ( 1. 96-sigma)

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2266 of 5809 MDA COUNTS 20. 8513 27.1418 27.6999 21.5637 5.5290 13.5658 ENERGY MDA COUNTS ENERGY MDA COUNTS Effective 3/25/2010 Revision 1 Effective March 201 O Radiochemistry Batch Checklist 09/29/16 1598663 Batch# ________ _ 1-129 I MJWC Product:,_--..,. _____ _ Dato: 09/29/16 Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. n/a Samples have been blank corrected (If required). n/a Blank correction reoorted Included flt renulredl. If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. ./ If greater than 10* MDA/ MDC, error Is 400/o or less. If be*ow the MDA' MDC error Is okav llnstrument source check Is within limits. Is within llmltc. ./ Method RDL/ LLD has been met. ./ If dupllcate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, ./ If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reaulred RER acceatance criteria. Tracer yield Is 15-1250/o

Carrier yield 25-125%. (Or meets the cllent's contract acceptance criteria). tn '"' Method blank Is less than the RDL/ LLD. ./ *-***--* --***'" Samole was run within hold time. I DER 1562850 Samnle was correctlv nreserved if renulred. ./ Smears Taken for Radioactive batches. n/a Method Spike and LCS are within 75-1250/o ./ lrn. --ets the -t'c cnntrart ,,rrt .. rl") No blank spaces on data forms. ./ All line outs Initialed and dated. (liqjr:ruw;dJztil!D Aux data Is correct. ./ Client Sneclal renulrements "aoe has been checked. ./ Raw Data and I or soectrum are Included and proPerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ./ uorJfled :u ** "' ./ In-*-'---*-*eJUn>n r---./ Batch Data Exceotlon RePorts COERl completed If annllcable. / DER 1562850 Batch Data Exception Reports (DER) second reviewed. / verlfl!ild to be comoleted. Allnuot Cnrredlnn cnmnlnted If reoulred. n/a Review sample historical results If available ./ (If REMP, results above MDC have been verified bu historical results recount or re*analvsls.) Primary Review Perfonnod By: 4 (2-cr (\-b Soc:ondary Rovlow Performed By: Page 2267 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 29-SEP-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1598663 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE EML HASL-300,1-01 Modified Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception
Description:
DER Report No.: 1562850 Revision No.: 1 Type: Process Client Code: MJWC Sample received out of holding: Samples were analyzed in a timely manner upon receipt. Reporting results. 405235 061,062,063,064,065,066,067,068,069, 070,071,072,073,074,075,076,077,078, QC 1203627532DU P, 1203627533MS Originator's Name: Data Validator/Group Leader: Spencer Collins 29-SEP-16 Bryan Williams 30-SEP-16 Page 1 Page 2268 of 5809 I-129 Queue Sheet 09/27/2016 Batch #:1598663 Analyst: MJHl First Client Due Date:I0/04/2016 Internal Due Datc:09/30/2016 Spike Isotope: I-129 Spike Code: i'-i1 c -i: LCS Isotope: I-129 LCS Code: Jl-n o -i::: Prep Date: q.;17.11, Initials: ..-v..-..-"l'"' Sample TD Client Description 405235061-1 5.!B.R.2.2 405235062-1 5.2.A.R.l.2 -105135063-1 5.?.A.IU.3 40523:506-l-l 5.2.A.R. l .4 4 05235065-1 5.!A.R.2.3 405235066-1 5.2.A.R.2.4 -105235067-1 5.2A.R.6.2 405235068-1 5.2A.R.4.2 -105235069-1 S.2.B.R.1.4 405235070-1 5.2.B.R.3.2 4052350il-l 5.2.B.R.4.2 405235072-1 5.2.B.R.2.4 40523507.3-l 5.2.B.R.8.2 405235074-1 :5.3..A.R.l.3 405235075-1 5.4A.R.1...3 405235076-1 5.4A..R.4.2 -105235077-1 5.5A.R.1.3 -105235078-1 5.6A.R.1.3 1203627531-1 MB for b31th 1598663 120362i53!-1 5.1B.R..?.2(40523506!DUP) 120362i533-1 5.18.R.2.2{405235061:.'lfS) 12036:?i534-l LCS for botch 1598663 GEL Laboratories LLC, Radiodzemisrry Dil-'isio11 Expiration Date: ;;-">::;-n Expiration Date: 3-3:::,-n Pipette ID: /"3y*=-">"t=P Hazard Type Code RDL SA!'lfPLE I pCifg SAi'lllPLE 1 pCilg SAMPLE I pCilg SAMPLE 1 pCilg SAMPLE I pC"tlg SAMPLE I pCilg SAMPLE l pCi!g SAMPLE I pCilg SAMPLE lpCilg SAMPLE I pCi/g SAMPLE I pCilg SAMPLE I pCilg SAMPLE I pCifg SAMPLE 1 pCi!g SAMPLE I pCi/g SAMPLE 1 pCi/g SAMPLE 1 pCi/g SAMPLE I pCifg MB l pCifg our l pCi/g l\IS I pC"t/g LCS l pCi/g Vol: o. 1...._L 1'\omin:il Concentration: ___ "-i4_..*-'----Vol: o.lv.A,L Nominal Concentration: f'.!A ------Witness: 1'-J.,l\ BALANL;!.: n q \, -pr--; ..,_,,, .... (<;) Aliquot Client 1\fatrix Auc.ue--Collcct Date (mL or'g); l\IJWCOOl SOIL ;. ,c 14-DEC-15 13:47 Cl I .)*C"':l' MJWCOiJJ ;.*lb -1 SOIL 14-DEC-I513:10a.:i.l 2.-1.q MJWCOOJ SOIL '.:\.21 14-DEC-15 13:15--i '5. t; 2 ;:::.;>>: MJWCOOl SOIL 14-DEC-1513:25"'" f 2 .'1 ! _., MJWC001 SOIL l-\.16 14-DEC-15 l3:56;;>j 4.1? MJWCOOI SOii. '), '-('l l-l-DEC-1514:00;;:1;, j :> , ::> MJWCOOJ SOIL :;_q5 ll*DEC-1511:30c.--i LJ.<i0 MJWCOOJ SOIL ll-DEC-15 10:27 2.12.. MJWCOOI SOI!. 3 -5C 16-DEC-15 12:45 e'l I MJWCOOI SOIL :.;.ci... 11-DEC-15 10:10 i:itj 3-1.'o MJWCOOI SOIL *3. ,g ll-DEC-15 10:25c_11 j 2.bS MJWCOOl SOIL 3.ci 15-DEC-15 13:35,,.,,.! ..... _, 2.'lb MJWCOOJ SOIL 3.10 l l-DEC-1511:35 3.oo MJWCOOJ SOIL '3.tS .Z.!P MJWCOOl SOIL '.).5b l 6-DEC-15 09:31i;15j 3.IU i" i\IJWCOOI SOIL 3-'-l:S 11-DEC-15 l4:19tJ<:.j 1..11 MJWCOOl SOIL *;,11 li-DEC-15 13:30i!;-ri ! MJWCOOI SOIL *3-M', 17-DEC-1512:40.::.h! 3 .Z? ' ,, ... QC ACCOUl\'T SOI!. 'i-2*(-!l> :: QC ACCOUNT SOIL !4-DEC-15 J.3:4ie.r0, 2. £, 2.. QCACCOU!"T SOIL z... 14-DEC-15 13:-l;ez.1 t l ,C\ {; QC ACCOUNT SOIL ci...--,_;-ll-Czt.j !.i -2:$ ' Detector Page 1 of 1 Weight/Loss Aliquot CotTection Report http://prodsvrOl.gel.com:7778/pls/lims/weight_loss _rpts.show _report I ofl Weight/Loss Aliquot Correction Report Select What to Correct Aliquot to *t1 Ash Dry Weight *i?i Dry. Weight* o Wet Weight Batch ID: 1598663 Aliquot Correction to Dry Weight for Batch 1598663 pie Id !Aliquot (G) I sample Type \Parent Sample Id [Loss (Dec) \corrected Aliquot (G). j Sam [40523 [40523 140523 140523 140523 f4052-3 -5061 13.70 jsA-MPLE-,NA j.1759 5062 13.46 lsAMPLE 14.27 .. jsAMPLE 5063 5064 r3.11 ... ,SAMPLE 5065 f4.7o jsAMPLE 5o66j3.69 ls AMPLE -5067 13."95 [SAMPLE 140523 140523 J4os23 ]40523 14052 14052 14052 J4052 14052 f4o52 f4o52 5068 f3.16.-. ---. lsAMPLE 5069 13."50 5070 J4.02 35071 13.18-35072 I 3"01
35073 13.70 35074 13.65 35075 13.56 35076 13.48 35077 13.17 14052 \1203 35078 13.88 627531 r *[1203-62753213.42 11203 \ 1203 627533 j 3.62 6275341 jsAMPLE lsAMPLE .. jsAMPLE ********. jsAMPLE lsAMPLE lsAMPLE jsAMPLE lsAMPLE lsAMPLE .!SAMPLE [MB JouP -,MS \Les GEL Laboratories LLC INA j .1935 INA 1.1051 !NA j.0816 INA 1.1005 r----NA * \.0929 JNA [.1385 !NA [.1387 INA 1.1061 INA ;j.1885 jNA :j.1655 INA .j.0816 INA j.1890 jNA l1067 !NA---l-1072 INA ---1.2054 F 1.0992 fNA j.1613 \NA fNA 1405235061 1.1759 1405235061 1.1759 INA rw:-j 3.0491146i.64o5934-J *;j .12.911361114365975 :14.2273961761.is3

13.347074883307074: j 3Ao26261s7374366-* f2: 72"15776633i1'98i": 13.128465437949653: 13.261936451874178-.j 2.6534441-53300698; 13.000427282492979 I 3.25032521ss91i29; 13.1781098iii29473-j 2.85539868t9os191: j 3.2540335055s3277: r 12 . .818370807596836'. .12.983187813889049 :I . I Page 2270 of 5809 9/27/2016 6:18 PM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:09:48.81 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235061.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 14-DEC-2015 13:47:00 Acquisition date : 28-SEP-2016 19:09:16 Sample ID I405235061 Sample quantity 3.05000E+00 GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.19 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED *SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.56* 4 14 0.78 82.24 77 9 1.05E-03207.6 2 0 30.56 7 7 0.55 152.38 145 10 1.83E-03 87.1 3 0 92.77* 6 4 0.54 464.14 459 8 1. 69E-03 90.3 4 0 110. 04 13 3 0.23 550.67 546 10 3. 71E-03 35.3 5 7 125.51 9 0 0.93 628.23 627 11 2.63E-03 21. l 4. 91E-01 6 7 126.80 9 0 0.61 634.69 627 11 2.49E-03 33.4 Flag: "*" = Peak area was modified by background subtraction Page 2271 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:09:49.68 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235061.CNF;l * *Acquisition date 28-SEP-2016 19:09:16 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Analyst initials: MJHl *

Sample ID I405235061 Sample Quantity 3.0500E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM I-129 1.919E-01 3.276E-01 4.487E-01 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM I-125 -2.902E-01 2.926E+OO 6.017E+OO FAIL ABUN Page 2272 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:09:47.99 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16. 56 11 14 0.78 82.24 77 9 3.04E-03 67.9 2 .o 30.56 7 7 0.55 152.38 145 10 1.83E-03 87.1 3 0 92.77 14 4 0.54 464.14 459 8 3.89E-03 36.4 4 0 110. 04 13 3 0.23 550.67 546 10 3.71E-03 35.3 5 7 125.51 9 0 0.93 628.23 627 11 2.63E-03 21.1 4.91E-01 6 7 126.80 9 0 0.61 634.69 627 11 2.49E-03 33.4 Page 2273 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:09:49.22 Nuclide Line Activity Report Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 7 56.60* l.489E+Ol l.919E-01 l.919E-01 174.17 33.59 ------10.04 l.626E+Ol ------Line Not Found ------39.58 ------7.51 l.619E+Ol ------Line Not Found ------Flag: "*" Key line Page 2274 of 5809 Summary of Nuclide Activity Sample ID : I405235061 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 19:09:16 Number of lines tentatively identified by NID 6 5 1 16.67% Nuclide Type : FISSION Nuclide Hlife I-129 l.57E+07Y Uncorrected Decay pCi/GRAM 1.00 1.919E-01 Total Activity 1.919E-01 Grand Total Activity l.919E-01 Flags: "K" "E" Page 2275 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM l.919E-01 1.919E-01 1.919E-01 Decay Corr 2-Sigma 2-Sigma Error %Error Flags 3.343E-01 174.17 "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235061 Acquisition date : 28-SEP-2016 19:09:16 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.56 4 14 0.78 82.24 77 9 1. 05E-03 **** 1. 51E+OO 0 92.77 6 4 0.54 464.14 459 8 1. 69E-03 **** 5.07E-01 0 110. 04 13 3 0.23 550.67 546 10 3. 71E-03 70.7 1.lOE-01 7 125.51. 9 0 0.93 .628.23 627 11 2.63E-03 42.2 2.65E-02 7 126. 80 9 0 0.61 634.69 627 11 2.49E-03 66.9 2.35E-02 Flags: "T" = Tentatively associated Page 2276 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:09:51.27 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235061.CNF;l * *Acquisition date 28-SEP-2016 19:09:16 Sensitivity : 3.000 *

Detector ID . XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Nuclide Library : IODINE *

Sample ID I405235061 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.0500E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14 *' Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 1.831E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2277 of 5809 Le (pCi/GRAM 2.316E+OO FAIL ABUN VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:09:52.77 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235061.CNF;l * *Acquisition date 28-SEP-2016 19:09:16 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Nuclide Library : IODINE *

Sample ID I405235061 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.0500E+OO GRAM *

Quantity Err(%) 3.2787E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 l.919E-01 Act Error (1.96-sigma) Non-Identified Nuclides Nuclide I-125 Page 2278 of 5809 Key-Line Activity (pCi/GRAM -2.902E-01 K.L Act error ( 1. 96-sigma) 2.926E+OO TPU ( 1. 96-sigma) 3.281E-01 TPU ( 1. 96-sigma) 2.929E+00 FAIL ABUN

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2279 of 5809 MDA COUNTS 4.3431 6.6533 2.9923 2.2941 10.4803 1.2005 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:13.08 ********************************************************************************

GEL Laboratories *LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235062.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 14-DEC-2015 13:10:00 Acquisition date : 28-SEP-2016 19:09:43 Sample ID I405235062 Sample quantity 2.79000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 35.39 7 0 0.33 175.86 173 6 1.94E-03 37.8 2 0 77.33* 3 3 0.27 384.75 381 7 9. 45E-04119. 3 3 0 90.59 5 5 0.36 450.77 443 9 1. 4 7E-03 84.6 4 0 92.65* 4 6 0.60 461.01 454 11 9.85E-04186.7 Flag: "*" = Peak area was modified by background subtraction Page 2280 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:13.82 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235062.CNF;l *

Acquisition date 28-SEP-2016 19:09:43 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 14-DEC-2015 13:10:00 Analyst initials: MJHl * *Sample ID I405235062 Sample Quantity 2.7900E+00 GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -6.833E-01 2.570E+OO I-129 -6.332E-03 l.280E-01 Page 2281 of 5 809 MDA (pCi/GRAM MDA (pCi/GRAM 6.231E+OO 3.612E-01 FAIL ABUN NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:12.41 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 35.39 7 0 0.33 175.86 173 6 1.94E-03 37.8 2 0 77.33 6 .3 0.27 384.75 381 7 1.70E-03 63.6 3 0 90.59 5 5 0.36 450.77 443 9 l.47E-03 84.6 4 0 92.65 18 6 0.60 461.01 454 11 5.03E-03 34.5 Page 2282 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:13.41 Nuclide Line Activity Report Flag: "*" = Keyline Page 2283 of 5809 Surrunary of Nuclide Activity Sample ID : 1405235062 Acquisition date Page : 2 28-SEP-2016 19:09:43 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting surrunary Flags: "K" "E" Page 2284 of 5809 Keyline not found Manually edited "M" "A" 4 3 NID 1 criteria **** 25.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235062 Acquisition date : 28-SEP-2016 19:09:43 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 35.39 7 0 0.33 175.86 173 6 l.94E-03 75.6 9.99E+OO T 0 77.33 3 3 0.27 384.75 381 7 9.45E-04 **** 1.19E+OO 0 90.59 5 5 0.36 450.77 443 9 1. 4 7E-03 **** 4.23E-01 0 92. 65 4 6. 0.60 4 61. 01 454 11 9.85E-04 **** 3.58E-01 Flags: "T" = Tentatively associated Page 2285 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:15.36 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235062.CNF;l *

Acquisition date 28-SEP-2016 19:09:43 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 14-DEC-2015 13:10:00 Nuclide Library : IODINE *

Sample ID I405235062 Analyst initials: MJHl. * *Batch Number 1598663 Sample Quantity : 2.7900E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************** * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29".CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2286 of 5809 Le (pCi/GRAM 1.913E+OO FAIL ABUN l.076E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:16.53 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235062.CNF;l * *Acquisition date 28-SEP-2016 19:09:43 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 14-DEC-2015 13:10:00 Nuclide Library : IODINE *

Sample ID I405235062 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity 2.7900E+OO GRAM *

Quantity Err(%) 3.5842E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Key-Line Activity (pCi/GRAM -6.833E-01
-6.332E-03 K.L Act error (1.96-sigma) 2.573E+OO 1.280E-01 TPU (1.96-sigma) TPU (1.96-sigma) 2.591E+OO FAIL ABUN 1.280E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2288 of 5809 MDA COUNTS 1.6265 0.8547 1.7568 2.7692 0.9543 3.0566 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:37.27 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235063.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 14-DEC-2015 13:15:00 Acquisition date : 28-SEP-2016 19:10:13 Sample ID I405235063 Sample quantity 3.82000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 19.31 6 0 0.55 95.83 94 5 1. 67E-03 40.8 2 0 63.33* 7 0 0.23 316.08 312 8 1.84E-03 55.7 3 0 92.82* 1 4 0.45 463.59 460 7 3.38E-04380.8 Flag: "*" = Peak area was modified by background subtraction Page 2289 of 5809 VAX/VMS Nµclide Identification Report Generated 28-SEP-2016 20:10:37.97 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235063.CNF;l *

Acquisition date 28-SEP-2016 19:10:13 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 14-DEC-2015 13:15:00 Analyst initials: MJHl *

Sample ID I405235063 Sample Quantity 3.8200E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.529E+OO 2. 861E+OO I-129 1. 760E-02 2.004E-01 Page 2290 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.613E+OO 4.162E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:36.?1 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 19.31 6 0 0.55 95.83 94 5 1. 67E-03 40.8 2. 0 63.33 12 0. 0.23 316.08 312 8 3.33E-03 28.9 3 0 92.82 9 4 0.45 463.59 460 7 2.36E-03 50.1 Page 2291of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:37.58 Nuclide Line Activity Report Flag: "*" = Keyline Page 2292 of 5809 Summary of Nuclide Activity Sample ID : 1405235063 Acquisition date Page : 2 28-SEP-2016 19:10:13 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" Keyline not found "E" = Manually edited Page 2293 of 5809 "M" "A" 3 3 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235063 Acquisition date : 28-SEP-2016 19:10:13 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 19.31 6 0 0.55 95.83 94 5 1. 67E-03 81. 6 3.23E+OO 0 63.33 7 0 0.23 316.08 312 8 1.84E-03 **** 3.08E+OO 0 92.82 1 4 0.45 463.59 460 7 3.38E-04 **** 4.07E-01 Flags: "T" = Tentatively associated Page 2294 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:39.32 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235063.CNF;l *

Acquisition date 28-SEP-2016 19:10:13 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 14-DEC-2015 13:15:00 Nuclide Library : IODINE *

Sample ID I405235063 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.8200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2295 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. l.583E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 20:10:40.43 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* t * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235063.CNF;l *

Acquisition date 28-SEP-2016 19:10:13 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 14-DEC-2015 13:15:00 Nuclide Library : IODINE *

Sample ID I405235063 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.8200E+OO GRAM *

Quantity Err(%) 2.6178E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : 1129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-s igma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -2.529E+OO 2.870E+OO I-129 1. 760E-02 2.004E-01 Page 2296 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 3.088E+OO 2.006E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2297 of 5809 MDA COUNTS 4.2472 2.9286 2.9842 3.0889 1.5811 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:50:09.17 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235064.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;476 Background date : 25-SEP-2016 12:20:17 Sample date 14-DEC-2015 13:25:00 Acquisition date : 29-SEP-2016 06:19:44 Sample ID I405235064 Sample quantity 2.91000E+00 GRAM Detector name : GAM05 Detector geometry: I129 Elapsed live time: 0 01:30:00.00 Elapsed real time: 0 01:30:00.52 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 0 0 0 0 0 0 0 0 0 0 0 0 4 4 0 0 2 2 0 0 0 0 0 0 0 0 0 0 Energy 43.45 46.15* 52.92 62.81* 77.13* 92.74* 179.85 186.62 295.92* 351.79* 395.00 459.39 497.13 500.15 543.86 584.48 608.99* 612.42 712.33 751.65 763.83 822.88 860.44 871.69 886.29 937.91 967.93 1200.60 BACKGROUND CORRECTED SAMPLE*PEAK REPORT Area 14 1 20 0 40 11 20 47 16 29 14 10 17 12 15 9 20 19 10 12 9 9 9 11 6 9 16 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 36 47 64 63 30 98 31 83 40 30 14 13 12 5 8 20 8 10 3 0 10 4 2 0 9 0 3 2 1. 33 0.90 0.91 0.99 1. 62 1. 47 0.79 1. 36 1. 28 0.95 1. 88 1. 09 2.06 1.24 1. 79 0.61 1. 81 1. 82 0.66 1. 97 0.58 1.15 1. 07 0.73 0.82 0.63 3.45 1. 03 88.72 94.13 107.66 127.41 156.03 187.24 361.34 374.86 593.31 704.98 791.35 920.04 995.47 1001.50 1088.87 1170.06 1219.03 1225.90 1425.58 1504.17 1528.50 1646.53 1721. 62 1744.09 1773.28 1876.44 1936.46 2401.50 86 91 105 125 153 182 358 367 587 701 788 916 987 987 1085 1164 1212 1212 1423 1499 1523 1643 1718 1740 1767 1874 1930 2398 5 2.61E-03 69.4 7 1.70E-04***** 7 3. 62E-03 71. 4 6 1.62E-05***** 7 7.39E-03 30.2 11 2.02E-03204.7 6 3.77E-03 49.3 12 8.75E-03 41.4 13 3.05E-03 85.0 10 5.46E-03 42.6 9 2.55E-03 55.6 8 1. 93E-03 68. 4 17 3.17E-03 47.4 17 2.21E-03 38.5 8 2. 78E-03 41. 6 11 1.71E-03 98.0 19 3.68E-03 43.9 19 3.51E-03 41.8 6 1. 81E-03 45. 5 9 2.22E-03 28.9 10 1. 73E-03 71. 2 7 1.57E-03 50.1 7 1.73E-03 40.0 8 2.04E-03 30.2 12 1.12E-03107.4 6 1. 67E-03 33. 3 11 2.98E-03 32.1 7 1.20E-03 51.2 Flag: "*" = Peak area was modified by background subtraction Page 2298 of 5809 Fit 5.13E-01 5.68E-01 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:50:09.98 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235064.CNF;l * *Acquisition date 29-SEP-2016 06:19:44 Sensitivity : 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:30:00.52 Half life ratio : ***** *

Sample date 14-DEC-2015 13:25:00 Analyst initials: MJHl *

Sample ID I405235064 Sample Quantity 2.9100E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File : DKAlOO': [CANBERRA.GAMMA]EFF GAM05 I129.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.670E-01 6.042E+00 I-129 -4.873E-02 2.436E-01 Page 2299 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.004E+Ol 3.776E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:50:08.38 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 43.45 14 36 1. 33 88. 72 86 5 2.61E-03 69.4 2 0 46.15 74 47 0.90 94.13 91 .7 1.37E-02 19.3 3 0 52.92 20 64 0.91 107.66 105 7 3.62E-03 71. 4 4 0 62.81 50 63 0.99 127.41 125 6 9.26E-03 28.8 5 0 77.13 54 30 1. 62 156.03 153 7 9.99E-03 21. 6 6 0 92.74 88 98 1. 47 187.24 182 11 1. 64E-02 24.4 7 0 179.85 20 31 0.79 361. 34 358 6 3.77E-03 49.3 8 0 186.62 47 83 1. 36 374.86 367 12 8.75E-03 41. 4 9 0 295.92 19 40 1. 28 593.31 587 13 3.53E-03 71. 4 10 0 351. 7 9 42 30 0.95 704.98 701 10 7.78E-03 28.9 11 0 395.00 14 14 1. 88 791.35 788 9 2.55E-03 55.6 12 0 459.39 10 13 1. 09 920.04 916 8 1. 93E-03 68.4 13 4 497.13 17 12 2.06 995.47 987 17 3.17E-03 47.4 5.13E-01 14 4 500.15 12 5 1.24 1001.50 987 17 2.21E-03 38.5 15 0 510.64 97 61 2 .11 1022.47 1015 16 1. 80E-02 20.5 16 0 543.86 15 8 1. 79 1088.87 1085 8 2.78E-03 41. 6 17 0 584.48 9 20 0.61 1170.06 1164 11 1.71E-03 98.0 18 2 608.99 27 8 1. 81 1219.03 1212 19 4.93E-03 30.9 5.68E-01 19 2 612.42 19 10 1. 82 1225.90 1212 19 3.51E-03 41. 8 20 0 712.33 10 *3 0.66 1425.58 1423 6 1. 81E-03 45.5 21 0 751. 65 12 0 1. 97 1504.17 1499 9 2.22E-03 28.9 22 0 763.83 9 10 0.58 1528.50 1523 10 1.73E-03 71. 2 23 0 822.88 9 4 1.15 1646.53 1643 7 1.57E-03 50.1 24 0 . 860.44 9 2 1. 07 1721.62 1718 7 1.73E-03 40.0 25 0 871.69 11 0 0.73 1744.09 1740 8 2.04E-03 30.2 26 0 886.29 6 9 0.82 1773.28 1767 12 1.12E-03107.4 27 0 937.91 9 0 0.63 1876.44 1874 6 1. 67E-03 33. 3 28 0 967.93 16 3 3.45 1936.46 1930 11 2.98E-03 32.1 29 0 1200.60 7 2 1. 03 2401. 50 2398 7 1.20E-03 51.2 Page 2300 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:50:09.53 Nuclide Line Activity Report Flag: "*" = Keyline Page 2301 of 5809 Summary of Nuclide Activity Sample ID : 1405235064 Acquisition date Page : 2 29-SEP-2016 06:19:44 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2302 of 5809 Keyline not found Manually edited "M" "A" 28 28 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235064 Acquisition date : 29-SEP-2016 06:19:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 43.45 14 36 1. 33 88.72 86 5 2.61E-03 **** 1. 33E+Ol 0 46.15 1 47 0.90 94.13 91 7 l.70E-04 **** 7.56E+OO 0 52.92 20 64 0.91 107.66 105 7 3.62E-03 **** l.27E+OO 0 77.13 40. 30 1. 62 156.03 153 7 7.39E-03 60 .. 5 1.95E-04 0 92.74 11 98 1. 47 187.24 182 11 2.02E-03 **** 2.50E-07 0 179.85 20 31 0.79 361.34 358 6 3.77E-03 98.5 2.78E-25 0 186.62 47 83 1. 36 374.86 367 12 8.75E-03 82.7 9.89E-27 0 295.92 16 40 1.28 593.31 587 13 3.05E-03 **** O.OOE+OO 0 351. 79 29 30 0.95 704.98 701 10 5.46E-03 85.2 O.OOE+OO 0 395.00 14 14 1. 88 791.35 788 9 2.55E-03 **** O.OOE+OO 0 459.39 10 13 1. 09 920.04 916 8 l.93E-03 **** 0.00E+OO 4 497.13 17 12 2.06 995.47 987 17 3.17E-03 94.8 0.00E+OO 4 500.15 12 5 1. 24 1001.50 987 17 2.21E-03 77.1 0.00E+OO 0 543.86 15 8 1. 79 1088.87 1085 8 2.78E-03 83.3 0.00E+OO 0 584.48 9 20 0.61 1170.06 1164 11 l.71E-03 **** O.OOE+OO 2 608.99 20 8 1. 81 1219.03 1212 19 3.68E-03 87.8 O.OOE+OO 2 612.42 19 10 1. 82 1225.90 1212 19 3.51E-03 83.7 O.OOE+OO 0 712.33 10 3 0.66 1425.58 1423 6 l.81E-03 91.0 O.OOE+OO 0 7 51. 65 12 0 1. 97 1504*.17 1499 9 2.22E-03 57.7 O.OOE+OO 0 763.83 9 10 0.58 1528.50 1523 10 l.73E-03 **** O.OOE+OO 0 822.88 9 4 1.15 1646.53 1643 7 l.57E-03 **** O.OOE+OO 0 860.44 9 2 1. 07 1721.62 1718 7 1.73E-03 80.1 O.OOE+OO 0 871.69 11 0 0.73 1744.09 1740 8 2.04E-03 60.3 O.OOE+OO 0 886.29 6 9 0.82 1773.28 1767 12 1.12E-03 **** O.OOE+OO 0 937.91 9 0 0.63 1876.44 1874 6 1. 67E-03 66. 7 O.OOE+OO 0 967. 93 16 3 3.45 1936.46 1930 11 2.98E-03 64.1 O.OOE+OO 0 1200.60 7 2 1. 03 2401.50 2398 7 1.20E-03 **** O.OOE+OO Flags: "T" = Tentatively associated Page 2303 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:50:12.16 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235064.CNF;l *

Acquisition date 29-SEP-2016 06:19:44 Sensitivity 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:30:00.52 Half life ratio : ***** *

Sample date 14-DEC-2015 13:25:00 Nuclide Library : IODINE *

Sample ID I405235064 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 2.9100E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2304 of 5809 Le (pCi/GRAM 4.587E+00 NOT IDENT. 1.715E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:50:13.32 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235064.CNF;l *

Acquisition date 29-SEP-2016 06:19:44 Sensitivity : 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:30:00.52 Half life ratio : ***** *

Sample date 14-DEC-2015 13:25:00 Nuclide Library : IODINE *

Sample ID I405235064 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 2.9100E+OO GRAM *

Quantity Err(%) 3.4364E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129' *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 I129.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -l.670E-01 6.042E+OO I-129 -4.873E-02 2.437E-01 Page 2305 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 6.042E+OO 2.447E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2306 of 5809 MDA COUNTS 38.4562 30.2741 31.9338 27.9341 40.0489 22.6542 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 06:50:38.27 ******************************************************************************** * 'GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235065.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 14-DEC-2015 13:56:00 Acquisition date : 29-SEP-2016 06:20:10 Sample ID I405235065 Sample quantity 4.23000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.13 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2307 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 06:50:39.14 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235065.CNF;l * *Acquisition date 29-SEP-2016 06:20:10 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 14-DEC-2015 13:56:00 Analyst initials: MJHl *

Sample ID I405235065 Sample Quantity 4.2300E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. 'File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 -1.856E+OO 2.642E+OO I-129 -5.535E-02 2.074E-01 Page 2308 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.009E+OO 4.169E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 06:50:37.31 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2309 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 06:50:38.65 Nuclide Line Activity Report Flag: "*" = Keyline Page 2310 of 5809 Summary of Nuclide Activity Sample ID : 1405235065 Acquisition date Page : 2 29-SEP-2016 06:20:10 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2311 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235065 None Flags: "T" Tentatively associated Page 2312 of 5809 Acquisition date Page : 3 29-SEP-2016 06:20:10 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 06:50:41.01 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235065.CNF;l *

Acquisition date 29-SEP-2016 06:20:10 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 14-DEC-2015 13:56:00 Nuclide Library : IODINE *

Sample ID I405235065 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 4.2300E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2313 of 5809 Le (pCi/GRAM 1.410E+OO NOT IDENT. l.699E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 06:50:42.34 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235065.CNF;l *

Acquisition date 29-SEP-2016 06:20:10 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 14-DEC-2015 13:56:00 Nuclide Library : IODINE *

Sample ID I405235065 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 4.2300E+OO GRAM *

Quantity Err(%) 2.3641E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.856E+OO 2.662E+OO I-129 -5.535E-02 2.075E-01 Page 2314of5809 TPU ( 1 . 96-sigma) TPU ( 1 . 96-sigma ) 2.791E+OO 2.089E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2315of5809 MDA COUNTS 6.1327 8.4818 2.5969 1. 7970 1.8430 0. 9690 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:01:07.53 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235066.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 14-DEC-2015 14:00:00 Acquisition date : 29-SEP-2016 06:30:34 Sample ID I405235066 Sample quantity 3.35000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 16.53* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 5 4 0.64 81.63 77 8 2.93E-03 96.8 Flag: "*" = Peak area was modified by background subtraction Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:01:08.47 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235066.CNF;l *

Acquisition date 29-SEP-2016 06:30:34 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 14-DEC-2015 14:00:00 Analyst initials: MJHl *

Sample ID I405235066 Sample Quantity 3.3500E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.233E+OO 1.016E+Ol I-129 1.204E-02 2.922E-Ol* Page 2317 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.939E+Ol 6.225E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:01:06.77 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2318 of 5809 Energy 16.53 Area 12 Bkgnd 4 FWHM Channel 0.64 81.63 Left 77 Pw Cts/Sec %Err 8 6.87E-03 39.6 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:01:07.95 Nuclide Line Activity Report Flag: "*" = Keyline Page 2319of5809 Summary of Nuclide Activity Sample ID : 1405235066 Acquisition date Page : 2 29-SEP-2016 06:30:34 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2320 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted. Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235066 Page : 3 Acquisition date : 29-SEP-2016 06:30:34 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.53 5 4 0.64 81. 63 77 8 2.93E-03 **** 4.60E-04 Flags: "T" = Tentatively associated Page 2321 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:01:10.12 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235066.CNF;l *

Acquisition date 29-SEP-2016 06:30:34 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 14-DEC-2015 14:00:00 Nuclide Library : IODINE *

Sample ID I405235066 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.3500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : 'DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2322 of 5809 Le (pCi/GRAM 7.918E+OO NOT IDENT. 2.445E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:01:11.26 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235066.CNF;l *

Acquisition date 29-SEP-2016 06:30:34 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live *time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 14-DEC-2015 14:00:00 Nuclide Library : IODINE *

Sample ID I405235066 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.3500E+OO GRAM *

Quantity Err(%) 2.9851E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.233E+OO 1.017E+Ol I-129 l.204E-02 2.922E-01 Page 2323 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 1. 021E+Ol 2.922E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2324 of 5809 MDA COUNTS 8.4152 4.2814 2.1618 3.3023 2.2293 3.4302 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:05:10.87 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235067.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 75-SEP-2016 12:23:10 Sample date 11-DEC-2015 11:30:00 Acquisition date : 29-SEP-2016 06:34:44 Sample ID I405235067 Sample quantity 3.40000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 12.86* BACKGROUND *CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 3 2 0.46 63.72 60 7 1. 61E-0314 6. 8 Flag: "*" = Peak area was modified by background subtraction Page 2325 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:05:11.71 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

* *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235067.CNF;l *

Acquisition date 29-SEP-2016 06:34:44 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date ll-DEC-2015 11:30:00 Analyst initials: MJHl *

Sample ID I405235067 Sample Quantity 3.4000E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.162E+OO 3.999E+OO I-129 -l.192E-02 2.266E-01 Page 2326 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.051E+OO 5.084E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:05:10.10 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2327 of 5809 Energy 12.86 Area 10 Bkgnd 2 FWHM Channel 0.46 63.72 Left 60 Pw Cts/Sec %Err 7 5.72E-03 37.7 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:05:11.21 Nuclide Line Activity Report Flag: "*" = Keyline Page 2328 of 5809 Summary of Nuclide Activity Sample ID : I405235067 Acquisition date Page : 2 29-SEP-2016 06:34:44 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2329 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235067 Page : 3 Acquisition date : 29-SEP-2016 06:34:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 12.86 3 2 0.46 63.72 60 7 1.61E-03 **** 2.14E-01 Flags: "T" = Tentatively associated Page 2330 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:05:13.30 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235067.CNF;l *

Acquisition date 29-SEP-2016 06:34:44 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 11-DEC-2015 11:30:00 Nuclide Library : IODINE *

Sample ID I405235067 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.4000E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2331 of 5809 Le (pCi/GRAM 2.229E+OO NOT IDENT. l.801E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:05:14.52 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235067.CNF;l *

Acquisition date 29-SEP-2016 06:34:44 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date ll-DEC-2015 11:30:00 Nuclide Library : IODINE *

Sample ID I405235067 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.4000E+OO GRAM *

Quantity Err(%) 2.9412E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.162E+00 4.017E+OO I-129 -1.192E-02 2.266E-01 Page 2332 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 4 .134E+OO 2.267E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2333 of 5809 MDA COUNTS 3.2573 2.2178 3.3663 1.1470 1.1645 2.4010 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:15:53.35 ********************************************************************************

GEL0Laboratories LLC * *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235068.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 11-DEC-2015 10:27:00 Acquisition date : 29-SEP-2016 06:45:27 Sample ID I405235068 Sample quantity 2.72000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.05 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 77.18* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 9 4 0.43 385.35 381 8 4.79E-03 54.7 Flag: "*" = Peak area was modified by background subtraction Page 2334 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:15:54.19 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235068.CNF;l *

Acquisition date 29-SEP-2016 06:45:27 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.05 Half life ratio : ***** *

Sample date 11-DEC-2015 10:27:00 Analyst initials: MJHl * *Sample ID I405235068 Sample Quantity 2.7200E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * / Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.469E+OO 4.839E+OO I-129 3.932E-02 1.251E-01 Page 2335 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.726E+OO 5.773E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:15:52.61 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2336 of 5809 Energy 77.18 Area 10 Bkgnd FWHM Channel 4 0.43 385.35 Left 381 Pw Cts/Sec %Err 8 5.79E-03 45.0 Fit VAX/VMS Nuclide Identification Report 'Generated 29-SEP-2016 07:15:53.73 Nuclide Line Activity Report Flag: "*" = Keyline Page 2337 of 5809 Summary of Nuclide Activity Sample ID : 1405235068 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 29-SEP-2016 06:45:27 Number of lines tentatively identified by **** There are no nuclides meeting summary 1 1 NID 0 criteria 0.00% **** Flags: "K" "E" Page 2338 of 5809 Keyline not found Manually edited "M" Manually accepted "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235068 Page : 3 Acquisition date : 29-SEP-2016 06:45:27 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 77.18 9 4 0.43 385.35 381 8 4.79E-03 **** 1.22E+OO Flags: "T" = Tentatively associated Page 2339 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:15:55.86 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND *SAMPLE DATA * * * *

Configuration . DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235068.CNF;l *

Acquisition date 29-SEP-2016 06:45:27 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.05 Half life ratio : ***** *

Sample date ll-DEC-2015 10:27:00 Nuclide Library : IODINE *

Sample ID I405235068 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity : 2.7200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 * * 'Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2340 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. l.484E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:15:57.02 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235068.CNF;l *

Acquisition date 29-SEP-2016 06:45:27 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.05 Half life ratio : ***** *

Sample date ll-DEC-2015 10:27:00 Nuclide Library : IODINE *

Sample ID I405235068 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity 2.7200E+OO GRAM *

Quantity Err(%) 3.6765E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 -2.469E+OO 4.844E+OO I-129 3.932E-02 1. 251E-01 Page 2341of5809 TPU (1.96-sigma) TPU (1. 96-sigma) 4.970E+OO 1.264E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2342 of 5809 MDA COUNTS 1. 4157 0.0000 2.9842 0.7722 0.0000 2.4852 ENERGY MDA COUNTS ENERGY MDA COUNTS VllX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:17:14.24 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235069.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 16-DEC-2015 12:45:00 Acquisition date : 29-SEP-2016 06:46:52 Sample ID I405235069 Sample quantity 3.13000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2343 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:17:15.07 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235069.CNF;l *

Acquisition date 29-SEP-2016 06:46:52 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 16-DEC-2015 12:45:00 Analyst initials: MJHl *

Sample ID I405235069 Sample Quantity 3.1300E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File' : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide {pCi/GRAM ( 1. 96-sigma) I-125 2.889E+OO 4.155E+OO I-129 -5.419E-02 3.855E-01 Page 2344 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 407E+Ol 8. 921E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:17:13.53 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2345 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:17:14.61 Nuclide Line Activity Report Flag: "*" = Keyline Page 2346 of 5809 Summary of Nuclide Activity Sample ID : 1405235069 Acquisition date Page : 2 29-SEP-2016 06:46:52 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2347of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235069 None Flags: "T" Tentatively associated Page 2348 of 5809 Acquisition date Page : 3 29-SEP-2016 06:46:52 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:17:16.86 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235069.CNF;l *

Acquisition date 29-SEP-2Dl6 06:46:52 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 16-DEC-2015 12:45:00 Nuclide Library : IODINE *

Sample ID I405235069 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.1300E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5 * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2349 of 5809 Le (pCi/GRAM 4.932E+OO NOT IDENT. 3.161E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:17:18.18 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235069.CNF;l *

Acquisition date 29-SEP-2016 06:46:52 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 16-DEC-2015 12:45:00 Nuclide Library : IODINE *

Sample ID I405235069 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.1300E+OO GRAM *

Quantity Err(%) 3.1949E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff: Cal. date 30-AUG-2016 11:41:11 Eff. : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1 . 96-sigma ) I-125 2.889E+OO 4.186E+OO I-129 -5.419E-02 3.855E-01 Page 2350 of 5809 TPU (1.96-sigma) TPU (1.96-sigma) 4.384E+OO 3.863E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2351of5809 MDA COUNTS 0.0000 2.5641 2.6352 0.0000 0.0000 2.0378 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:23:38.12 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235070.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 11-DEC-2015 10:10:00 Acquisition date : 29-SEP-2016 06:53:16 Sample ID I405235070 Sample quantity 3.26000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.13 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2352 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:23:39.10 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235070.CNF;l *

Acquisition date 29-SEP-2016 06:53:16 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date 11-DEC-2015 10:10:00 Analyst initials: MJHl *

Sample ID I405235070 Sample Quantity 3.2600E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-s igma) I-125 -l.469E+OO 4.321E+OO I-129 -1. l 79E-01 1. BllE-01 Page 2353 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.672E+OO 3.383E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:23:37.28 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2354 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:23:38.53 Nuclide Line Activity Report Flag: "*" = Keyline Page 2355 of 5809 Summary of Nuclide Activity Sample ID : 1405235070 Acquisition date Page : 2 29-SEP-2016 06:53:16 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2356 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235070 None Flags: "T" Tentatively associated Page 2357 of 5809 Acquisition date Page : 3 29-SEP-2016 06:53:16 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:23:40.98 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235070.CNF;l *

Acquisition date 29-SEP-2016 06:53:16 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date ll-DEC-2015 10:10:00 Nuclide Library : IODINE *

Sample ID I405235070 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.2600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Le (pCi/GRAM 3.037E+00 NOT IDENT. 1.190E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:23:42.24 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * . *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235070.CNF;l * *Acquisition date 29-SEP-2016 06:53:16 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *

Sample date ll-DEC-2015 10:10:00 Nuclide Library : IODINE *

Sample ID I405235070 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.2600E+00 GRAM *

Quantity Err(%) 3.0675E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 -1.469E+OO 4.328E+OO I-129 -1.179E-01 1.815E-01 Page 2359 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 4.379E+00 1.891E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29.62 35.49 39.58 Page 2360 of 5809 MDA COUNTS 7.3593 5.0891 0.0000 0.8985 0.9215 0. 9690 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:34:51.75 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235071.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date ll-DEC-2015 10:25:00 Acquisition date : 29-SEP-2016 07:04:23 Sample ID I405235071 Sample quantity 2.65000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 28.59 165.17 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 7 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.38 3 1.74 142.00 825.94 137 818 9 3.89E-03 37.8 12 3.40E-03 69.4 Flag: "*" = Peak area was modified by background subtraction Page 2361of5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:34:52.56 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235071.CNF;l * *Acquisition date 29-SEP-2016 07:04:23 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 11-DEC-2015 10:25:00 Analyst initials: MJHl *

Sample ID I405235071 Sample Quantity 2.6500E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File . : DKA100: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -9.957E-01 6.309E+OO I-129 2.826E-01 2.604E-01 Page 2362 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 2 68E+Ol 7.869E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:34:51.07 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 28.59 7 0 0.38 142.00 137 9 3.89E-03 37.8 2 0 165.17 6 3 1. 74 825.94 818 12 3. 40E.,.-03 69.4 Page 2363 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:34:52.15 Nuclide Line Activity Report Flag: "*" = Keyline Page 2364 of 5809 Summary of Nuclide Activity Sample ID : 1405235071 Acquisition date Page : 2 29-SEP-2016 07:04:23 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2365 of 5809 Keyline.not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235071 Page : 3 Acquisition date : 29-SEP-2016 07:04:23 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 28.59 165.17 7 6 0 0.38 3 1.74 Flags: "T" = Tentatively associated Page 2366 of 5809 142.00 137 9 3.89E-03 75.6 1.27E+Ol 825.94 818 12 3.40E-03 **** 2.85E-24 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:34:54.25 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

* *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235071.CNF;l * *Acquisition date 29-SEP-2016 07:04:23 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 11-DEC-2015 10:25:00 Nuclide Library : IODINE *

Sample ID I405235071 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity : 2.6500E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF' XRAY2 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2367 of 5809 Le (pCi/GRAM 4.008E+OO NOT IDENT. 3.090E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:34:55.76 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235071.CNF;l *

Acquisition date 29-SEP-2016 07:04:23 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 11-DEC-2015 10:25:00 Nuclide Library : IODINE *

Sample ID I405235071 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 2.6500E+00 GRAM *

Quantity Err(%) 3.7736E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff.' Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -9.957E-01 6. 311E+OO I-129 2.826E-01 2.619E-01 Page 2368 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 6.327E+OO 2.912E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2369 of 5809 MDA COUNTS 1.5779 0.0000 6.4853 3.3023 2.2293 4.5736 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:41:40.11 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235072.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : Z5-SEP-2016 12:23:10 Sample date 15-DEC-2015 13:35:00 Acquisition date : 29-SEP-2016 07:11:09 Sample ID I405235072 Sample quantity 2.76000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 63.31* 73.99 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 4 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.23 316.50 0 0.57 370.00 312 365 7 2.07E-03 68.2 8 3.33E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 2370 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:41:40.85 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235072.CNF;l *

Acquisition date 29-SEP-2016 07:11:09 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 15-DEC-2015 13:35:00 Analyst initials: MJHl * *Sample ID I405235072 Sample Quantity 2.7600E+00 GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.903E+OO 4.387E+OO I-129 5.145E-03 3.520E-01 Page 2371of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.177E+Ol 7.613E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:41:39.39 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 13.83 7 4 0.57 68.55 65 6 3.69E-03 63.5 2 0 63.31 6 0 0.23 316.50 312 7 3.33E-03 40.8 3 0 73.99 6 0 0.57 370.00 365 8 3.33E-03 40.8 Page 2372of5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:41:40.43 Nuclide Line Activity Report Flag: "*" = Keyline Page 2373 of 5809 Summary of Nuclide Activity Sample ID : 1405235072 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 29-SEP-2016 07:11:09 Number of lines tentatively identified by **** There are no nuclides meeting summary 2 2 NID 0 criteria 0.00% **** Flags: "K". "E" Page 2374 of 5809 Keyline not found Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235072 Page : 3 Acquisition date : 29-SEP-2016 07:11:09 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 63.31 73.99 4 6 0 0.23 0 0.57 Flags: . "T" = Tentatively associated Page 2375of5809 316.50 312 7 2.07E-03 **** 5.17E+OO 370.00 365 8 3.33E-03 81.6 2.37E+OO VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:41:42.34 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235072.CNF;l *

Acquisition date 29-SEP-2016 07:11:09 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 15-DEC-2015 13:35:00 Nuclide Library : IODINE *

Sample ID I405235072 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity: 2.7600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2376 of 5809 Le (pCi/GRAM 4.363E+OO NOT IDENT. 2.894E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:41:43.42 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235072.CNF;l *

Acquisition date 29-SEP-2016 07:11:09 Sensitivity 3.000 *

Detector ID . XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 15-DEC-2015 13:35:00 Nuclide Library : IODINE *

Sample ID I405235072 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity 2.7600E+OO GRAM *

Quantity Err(%) 3.6232E-03 % *

Recovery 1.00000 Carrier Weight O.GOOOO *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 1.903E+00 4.400E+OO I-129 5.145E-03 3.520E-01 Page 2377of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.483E+OO 3.520E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2378 of 5809 MDA COUNTS 1.0858 3.3266 2.2442 0.0000 1.1645 6.0024 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:48:50.19 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235073.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date ll-DEC-2015 11:35:00 Acquisition date : 29-SEP-2016 07:18:28 Sample ID I405235073 Sample quantity : 3.00000E+OO GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found VAX/VMS Nuclide Identification Report Generated .29-SEP-2016 07:48:51.01 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235073.CNF;l *

Acquisition date 29-SEP-2016 07:18:28 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 11-DEC-2015 11:35:00 Analyst initials: MJHl *

Sample ID I405235073 Sample Quantity 3.0000E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 l.722E+00 3.375E+OO I-129 -l.148E-01 3.733E-01 Page 2380 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.267E+Ol 8.268E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:48:49.33 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2381of5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:48:50.54 Nuclide Line Activity Report Flag: "*" = Keyline Page 2382 of 5809 Summary of Nuclide Activity Sample ID : 1405235073 Acquisition date Page : 2 29-SEP-2016 07:18:28 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2383 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235073 None Flags: "T" Tentatively associated Page 2384 of 5809 Acquisition date Page : 3 29-SEP-2016 07:18:28 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:48:52.57 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235073.CNF;l * *Acquisition date 29-SEP-2016 07:18:28 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date ll-DEC-2015 11:35:00 Nuclide Library : IODINE *

Sample ID I405235073 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.0000E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *'

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2385 of 5809 Le (pCi/GRAM 4.006E+OO NOT IDENT. 2.777E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:48:53.78 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235073.CNF;l *

Acquisition date 29-SEP-2016 07:18:28 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 11-DEC-2015 11:35:00 Nuclide Library : IODINE *

Sample ID I405235073 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.0000E+OO GRAM *

Quantity Err(%) 3.3333E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 1.722E+OO 3.389E+OO I-129 -l.148E-01 3.734E-01 TPU (1.96-sigma) TPU (1.96-sigma) 3.477E+OO 3.770E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2387 of 5809 MDA COUNTS 0.0000 2.5641 3. 5136 0.0000 0.9543 2.0378 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:49:16.91 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235074.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 15-DEC-2015 14:10:00 Acquisition date : 29-SEP-2016 07:18:54 Sample ID I405235074 Sample quantity 3.26000E+00 GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT* No peaks were found Page 2388 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:49:17.88 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235074.CNF;l * *Acquisition date 29-SEP-2016 07:18:54 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 15-DEC-2015 14:10:00 Analyst initials: MJHl *

Sample ID I405235074 Sample Quantity 3.2600E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 6.738E-01 5. 371E+OO I-129 -7.909E-02 2.779E-01 Page 2389 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 2 65E+Ol 5.317E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:49:16.21 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2390 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:49:17.33 Nuclide Line Activity Report Flag: "*" = Keyline Page 2391 of 5809 Summary of Nuclide Activity Sample ID : 1405235074 Acquisition date Page : 2 29-SEP-2016 07:18:54 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2392 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235074 None Flags: "T" Tentatively associated Page 2393 of 5809 Acquisition date Page : 3 29-SEP-2016 07:18:54 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:49:19.37 *'******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235074.CNF;l * *Acquisition date 29-SEP-2016 07:18:54 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 15-DEC-2015 14:10:00 Nuclide Library : IODINE *

Sample ID I405235074 Analyst initials.: MJHl * *

Batch Number 1598663 Sample Quantity : 3.2600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2394 of 5809 Le (pCi/GRAM 4.448E+00 NOT IDENT. l.489E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:49:20.40 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235074.CNF;l *

Acquisition date 29-SEP-2016 07:18:54 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 15-DEC-2015 14:10:00 Nuclide Library : IODINE *

Sample ID I405235074 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.2600E+00 GRAM *

Quantity Err(%) 3.0675E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016'10:07:09 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 6.738E-01 5.371E+OO I-129 -7.909E-02 2.780E-01 Page 2395 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.380E+OO 2.802E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2396 of 5809 MDA COUNTS 1.4157 1.4643 2.9842 0. 7722 0.0000 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:55:09.41 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235075.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 75-SEP-2016 12:22:54 Sample date 16-DEC-2015 09:31:00 Acquisition date : 29-SEP-2016 07:24:37 Sample ID I405235075 Sample quantity 3.18000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.12 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 25.28 31. 37 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 9 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.39 0 0.63 126.70 157.38 124 153 7 4.72E-03 56.7 9 7.22E-03 27.7 Flag: "*" = Peak area was modified by background subtraction Page 2397 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:55:10.35 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235075.CNF;l *

Acquisition date 29-SEP-2016 07:24:37 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 16-DEC-2015 09:31:00 Analyst initials: MJHl *

Sample ID I405235075 Sample Quantity 3.1800E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 4.425E-01 4.259E+OO I-129 1.760E-01 2.402E-01 Page 2398 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 8.541E+OO 5.760E-01 FAIL ABUN NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:55:08.65 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 25.28 9 6 0.39 126.70 124 7 4.72E-03 56. 7 2 0 31. 37 13 . 0 0.63 157.38 153 9 7.22E-03 27 .. 7 Page 2399 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:55:09.79 Nuclide Line Activity Report Flag: "*" = Keyline Page 2400 of 5809 Summary of Nuclide Activity Sample ID : 1405235075 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 29-SEP-2016 07:24:37 Number of lines tentatively identified by **** There are no nuclides meeting summary 2 1 NID 1 criteria 50.00% **** Flags: "K" Keyline not found "E" = Manually edited Page 2401 of 5809 "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235075 Acquisition date : 29-SEP-2016 07:24:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 25.28 9 6 0.39 126.70 124 7 4.72E-03 **** 1. 94E+Ol 0 31. 37 13 0 0.63 157.38 153 9 7.22E-03 55.5 2.26E+Ol T Flags: "T". = Tentatively associated Page 2402 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:55:12.07 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235075.CNF;l *

Acquisition date 29-SEP-2016 07:24:37 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 16-DEC-2015 09:31:00 Nuclide Library : IODINE *

Sample ID I405235075 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.1800E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYI I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2403 of 5809 Le (pCi/GRAM 3.498E+OO FAIL ABUN 2.367E-01 NOT IDENT. I VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 07:55:13.32 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235075.CNF;l *

Acquisition date 29-SEP-2016 07:24:37 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.12 Half life ratio : ***** *

Sample date 16-DEC-2015 09:31:00 Nuclide Library : IODINE *

Sample ID I405235075 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.1800E+OO GRAM *

Quantity Err(%) 3.1447E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. 'date 9-JUN-2016 11:39:23 Eff. : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2404 of 5809 Key-Line Activity (pCi/GRAM 4.425E-01 1. 760E-01 K.L Act error ( 1. 96-sigma) 4.260E+OO 2.408E-01 TPU (1.96-sigma) TPU (1. 96-sigma) 4.265E+OO FAIL ABUN 2.536E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2405 of 5809 MDA COUNTS 6.1327 2.5445 3.4625 4.4924 5.5290 0. 9690 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:01:54.25 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235076.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;476 Background date : 25-SEP-2016 12:20:17 Sample date ll-DEC-2015 14:19:00 Acquisition date : 29-SEP-2016 08:01:20 Sample ID I405235076 Sample quantity 2.77000E+OO GRAM Detector name : GAM05 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.34 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED' SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.43* 6 62 0.79 94.69 90 10 1. 57E-032 98. 0 2 0 63.42* 11 82 1. 00 128.64 125 11 2.93E-03176.8 3 0 92.32* 14 50 1. 43 186.40 181 9 3. 83E-03112. 6 4 0 177.19 27 23 3.57 356.02 352 10 7.51E-03 38.1 5 0 185.94* 4 39 1.11 373.51 368 10 1.05E-03346.4 6 0 242. 72 9 29 0.60 486.99 482 8 2. 36E-03115. 9 7 0 351.42* 20 19 1. 02 704.24 699 11 5.63E-03 50.7 8 0 511.11* 16 26 2.21 1023.40 1017 17 4.32E-03105.8 9 0 609.20* 15 8 1. 47 1219.45 1215 9 4.20E-03 47.6 10 0 695.53 7 11 0.58 1392.00 1386 11 1. 94E-03 99.2 11 0 776.38 10 2 1.15 1553.60 1549 8 2.84E-03 39.2 12 0 803.21* 1 4 1. 59 1607.21 1602 8 3.65E-04359.2 13 0 998.33 9 0 0.58 1997.22 1993 8 2.50E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 2406 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:01:55.18 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *. * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235076.CNF;l *

Acquisition date 29-SEP-2016 08:01:20 Sensitivity 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *

Sample date ll-DEC-2015 14:19:00 Analyst initials: MJHl * *Sample ID I405235076 Sample Quantity 2.7700E+00 GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File DKAlOO: [CANBERRA.GAMMA]EFF GAM05 I129.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.691E+OO 8.090E+OO I-129 -1.005E-01 3.487E-01 Page 2407 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM l.328E+Ol 5.543E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:01:53.42 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.43 54 62 0.79 94.69 90 10 1. 51E-02 30.3 2 . 0 63.42 44 82 1. 00 128.64 125 11 1.22E-02 41. 9 3 0 92.32 66 50 1. 43 186.40 181 9 1. 82E-02 23.0 4 0 177.19 27 23 3.57 356.02 352 10 7.51E-03 38.1 5 0 185.94 26 39 1.11 373.51 368 10 7.23E-03 49.4 6 0 242. 72 9 29 0.60 486.99 482 8 2.36E-03115.9 7 0 351.42 29 19 1. 02 704.24 699 11 7.95E-03 35.1 8 0 511.11 100 26 2.21 1023.40 1017 17 2.77E-02 15.9 9 0 609.20 20 8 1. 47 1219.45 1215 9 5.46E-03 35.4 10 0 695.53 7 11 0.58 1392.00 1386 11 l.94E-03 99.2 11 0 776.38 10 2 1.15 1553.60 1549 8 2.84E-03 39.2 12 0 803.21 7 4 1. 59 1607.21 1602 8 l.94E-03 62.3 13 0 998.33 9 0 0.58 1997.22 1993 8 2.50E-03 33.3 Page 2408 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:01:54.73 Nuclide Line Activity Report Flag: "*" = Keyline Page 2409 of 5809 Page : 2 Summary of Nuclide Activity Sample ID : 1405235076 Acquisition date 29-SEP-2016 08:01:20 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2410of5809 Keyline not found. Manually edited "M" "A" 13 13 NID 0 criteria **** 0.00% Manually .accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235076 Acquisition date : 29-SEP-2016 08:01:20 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.43 6 62 0.79 94.69 90 10 l.57E-03 **** 7.09E+OO 0 63.42 11 82 1. 00 128.64 125 11 2.93E-03 **** 3.93E-02 0 92.32 14 50 1. 43 186.40 181 9 3.83E-03 **** 3. OlE-07 0 177.19 27 23 3.57 356.02 352 10 7.51E-03 76.3 l.03E_.:24 0 185.94 4 39 1.11 373.51 368 10 l.05E-03 **** 1.38E-26 0 242. 72 9 29 0.60 486.99 482 8 2.36E-03 **** O.OOE+OO 0 351. 42 20 19 1. 02 704.24 699 11 5.63E-03 **** O.OOE+OO 0 511.11 16 26 2.21 1023.40 1017 17 4.32E-03 **** O.OOE+OO 0 609.20 15 8 1. 47 1219.45 1215 9 4.20E-03 95.3 O.OOE+OO 0 695.53 7 11 0.58 1392.00 1386 11 l.94E-03 **** O.OOE+OO 0 776.38 10 2 1.15 1553.60 1549 8 2.84E-03 78.4 O.OOE+OO 0 803.21 1 4 1. 59 1607.21 1602 8 3.65E-04 **** O.OOE+OO 0 998.33 9 0 0.58 1997.22 1993 8 2.50E-03 66.7 O.OOE+OO Flags: "T" = Tentatively associated Page 2411of5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:01:57.31 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235076.CNF;l *

Acquisition date 29-SEP-2016 08:01:20 Sensitivity 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *

Sample date 11-DEC-2015 14:19:00 Nuclide Library : IODINE *

Sample ID I405235076 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity: 2.7700E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2412of5809 Le (pCi/GRAM 5.935E+OO NOT IDENT. 2.499E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:01:58.45 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235076.CNF;l *

Acquisition date 29-SEP-2016 08:01:20 Sensitivity : 3.000 *

Detector ID GAM05 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *

Sample date ll-DEC-2015 14:19:00 Nuclide Library : IODINE *

Sample ID I405235076 Analyst initials: MJHl * *Batch Number 1598663 Sample Quantity 2.7700E+00 GRAM *

Quantity Err(%) 3.6101E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 6-SEP-2016 11:51:40 Eff. Geometry * : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 I129.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 9 6-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.691E+OO 8.095E+OO I-129 -1.005E-01 3.489E-01 Page 2413 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 8 .131E+OO 3.518E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2414of5809 MDA COUNTS 27.0618 28.8325 17.4184 20.5830 22.2494 20.3887 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:32:36.11 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235077.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : Z5-SEP-2016 12:22:54 Sample date 17-DEC-2015 13:30:00 Acquisition date : 29-SEP-2016 08:02:10 Sample ID I405235077 Sample quantity 2.86000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.15 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 24.92 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 9 12 0.25 124.88 121 9 4.89E-03 81.4 Flag: "*" = Peak area was modified by background subtraction Page 2415 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:32:37.37 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235077.CNF;l * *Acquisition date 29-SEP-2016 08:02:10 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.15 Half life ratio : 8.000 *

Sample date 17-DEC-2015 13:30:00 Analyst initials: MJHl *

Sample ID I405235077 Sample Quantity 2.8600E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -8.546E-02 4.302E+OO I-129 8.824E-02 3.016E-01 Page 2416of5809 MDA (pCi/GRAM MDA (pCi/GRAM 9.029E+OO 6.633E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:32:34.86 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2417 of5809 Energy 24.92 Area 9 Bkgnd 12 FWHM Channel Left 0.25 124.88 121 Pw Cts/Sec %Err 9 4.89E-03 81.4 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:32:36.67 Nuclide Line Activity Report Flag: "*" = Keyline Page 2418 of 5809 Summary of Nuclide Activity Sample ID : 1405235077 Acquisition date Page : 2 29-SEP-2016 08:02:10 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" Keyline not found "E" = Manually edited Page 2419of5809 "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235077 Page : 3 Acquisition date : 29-SEP-2016 08:02:10 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 24.92 9 12 0.25 124.88 121 9 4.89E-03 81.4 1.91E+Ol Flags: "T" = Tentatively associated Page 2420 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:32:39.77 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235077.CNF;l *

Acquisition date 29-SEP-2016 08:02:10 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.15 Half life ratio : 8.000 *

Sample date 17-DEC-2015 13:30:00 Nuclide Library : IODINE *

Sample ID I405235077 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 2.8600E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2421 of 5809 Le (pCi/GRAM 3.666E+OO NOT IDENT. 2.746E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:32:41.91 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235077.CNF;l *

Acquisition date 29-SEP-2016 08:02:10 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.15 Half life ratio : 8.000 *

Sample date 17-DEC-2015 13:30:00 Nuclide Library : IODINE *

Sample ID I405235077 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 2.8600E+OO GRAM *

Quantity Err(%) 3.4965E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *'

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 -8.546E-02 4.302E+OO I-129 8.824E-02 3.017E-01 Page 2422of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.302E+OO 3.043E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2423 of 5809 MDA COUNTS 6.4394 5. 7252 0.9738 2.0216 4.1467 4.3604 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:20.95 ********************************************************************************

GEL LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235078.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 75-SEP-2016 12:22:59 Sample date 17-DEC-2015 12:40:00 Acquisition date : 29-SEP-2016 08:02:53 Sample ID I405235078 Sample quantity 3.25000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 13. 37* 63.14* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.25 0 0.60 65.80 315.00 63 311 7 3.09E-03 60.6 7 2.99E-03 55.5 Flag: "*" = Peak area was modified by background subtraction Page 2424 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:21.83 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235078.CNF;l *

Acquisition date 29-SEP-2016 08:02:53 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 17-DEC-2015 12:40:00 Analyst initials: MJHl *

Sample ID I405235078 Sample Quantity 3.2500E+00 GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 * *' Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.105E+OO 6.942E+OO I-129 -9.825E-02 3.019E-01 Page 2425 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.572E+Ol 5.760E-01 NOT IDENT. .NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:20.19 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2426 of 5809 Energy 13.37 63.14 Area 10 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.25 65.80 0 0.60 315.00 63 311 7 5.56E-03 31.6 7 4.44E-03 35.4 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:21.34 Nuclide Line Activity Report Flag: "*" Key line Page 2427 of 5809 Summary of Nuclide Activity Sample ID : 1405235078 Acquisition date Page : 2 29-SEP-2016 08:02:53 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" Keyline not found "E" Manually edited Page 2428 of 5809 "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235078 Page : 3 Acquisition date : 29-SEP-2016 08:02:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 13.37 63.14 6 5 0 0.25 0 0.60 Flags: "T" = Tentatively associated Page 2429 of 5809 65.80 63 7 3.09E-03 **** 2.0lE-07 315.00 311 7 2.99E-03 **** 1.88E-02 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:23.51 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235078.CNF;l *

Acquisition date 29-SEP-2016 08:02:53 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 17-DEC-2015 12:40:00 Nuclide Library : IODINE *

Sample ID I405235078 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 3.2500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2430 of 5809 Le (pCi/GRAM 6.091E+00 NOT IDENT. 2.191E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:24.71 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235078.CNF;l *

Acquisition date 29-SEP-2016 08:02:53 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 17-DEC-2015 12:40:00 Nuclide Library : IODINE *

Sample ID I405235078 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 3.2500E+OO GRAM *

Quantity Err(%) 3.0769E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1,96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.105E+OO 6.945E+OO I-129 -9.825E-02 3.020E-01 Page 2431 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 6.963E+OO 3.053E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29.62 35.49 39.58 Page 2432 of 5809 MDA COUNTS 3.1557 5.3517 2.1618 6.6046 2.2293 3.4302 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:00.09 ********************************************************************************

GEL *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627531.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 75-SEP-2016 12:23:10 Sample date 27-SEP-2016 00:00:00 Acquisition date : 29-SEP-2016 08:03:29 Sample ID I1203627531 Sample quantity 4.23000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 4.49 13.13* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 17 1 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 12 0.58 2 0.29 21. 76 65.07 19 63 7 9.62E-03 42.3 5 6.llE-04346.5 Flag: "*" = Peak area was modified by background subtraction Page 2433 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:00.86 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627531.CNF;l *

Acquisition date 29-SEP-2016 08:03:29 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Analyst initials: MJHl *

Sample ID I1203627531 Sample Quantity 4.2300E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -2.228E-03 7.514E-02 I-129 3.357E-03 2.297E-01 Page2434of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.912E-01 4.967E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:33:59.28 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 4.49 17 12 0.58 21. 76 19 7 9.62E-03 42.3 2 0 13 .13 9 .2 0.29 65.07 63 5 4.72E-03 40.0 Page 2435 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:00.44 Nuclide Line Activity Report Flag: "*" = Keyline Page 2436 of 5809 Summary of Nuclide Activity Sample ID : 11203627531 Acquisition date Page : 2 29-SEP-2016 08:03:29 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2437of5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I1203627531 Page : 3 Acquisition date : 29-SEP-2016 08:03:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 4.49 13 .13 17 1 12 0.58 2 0.29 Flags: "T" = Tentatively associated Page 2438 of 5809 21. 76 65.07 19 7 9.62E-03 84.5 l.76E-09 63 5 6.llE-04 **** 2.58E-01 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:02.40 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627531.CNF;l *

Acquisition date 29-SEP-2016 08:03:29 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627531 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 4.2300E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2439 of 5809 Le (pCi/GRAM 6.042E-02 NOT IDENT. l.888E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:03.59 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627531.CNF;l *

Acquisition date 29-SEP-2016 08:03:29 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627531 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 4.2300E+OO GRAM *

Quantity Err(%) 2.3641E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date

17-JUN-2016 08:18:14 Eff. Geometry : 1129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -2.228E-03 7.514E-02 I-129 3.357E-03 2.297E-01 Page 2440 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 7.515E-02 2.297E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2441of5809 MDA COUNTS 1.0858 3.3266 2.2442 2.2941 1.1645 1.2005 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:28.93 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627532.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 14-DEC-2015 13:47:00 Acquisition date : 29-SEP-2016 08:03:56 Sample ID I1203627532 Sample quantity 2.82000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2442of5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:29.85 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627532.CNF;l * *Acquisition date 29-SEP-2016 08:03:56 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Analyst initials: MJHl *

Sample ID I1203627532 Sample Quantity 2.8200E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1. 768E+OO 3.465E+OO I-129 3.395E-02 l.179E-01 Page 2443 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.301E+Ol 5.687E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:28.05 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2444 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:29.35 Nuclide Line Activity Report Flag: "*" = Keyline Page 2445 of 5809 Summary of Nuclide Activity Sample ID : Il203627532 Acquisition date Page : 2 29-SEP-2016 08:03:56 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2446 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627532 None Flags: "T" Tentatively associated Page 2447 of 5809 Acquisition date Page : 3 29-SEP-2016 08:03:56 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:31.63 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627532.CNF;l *

Acquisition date 29-SEP-2016 08:03:56 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Nuclide Library : IODINE *

Sample ID I1203627532 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 2.8200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA:GAMMA]EFF XRAY5 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2448 of 5809 Le (pCi/GRAM 4.112E+OO NOT IDENT. 1.400E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:32.88 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* '!'"

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627532.CNF;l *

Acquisition date 29-SEP-2016 08:03:56 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Nuclide Library : IODINE *

Sample ID I1203627532 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 2.8200E+00 GRAM *

Quantity Err(%) 3.5461E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOrE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1. 7 68E+OO 3.479E+OO I-129 3.395E-02 l.180E-01 Page 2449 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.569E+OO 1.190E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2450 of 5809 MDA COUNTS 0.0000 0.0000 0.8784 1. 8461 1.9087 1.0189 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:35:01.08 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627533.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 14-DEC-2015 13:47:00 Acquisition date : 29-SEP-2016 08:04:21 Sample ID I1203627533 Sample quantity 2.98000E+00 GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE *PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.69 129 13 0.58 147.75 143 11 7.15E-02 10.4 2 0 34.44 8 4 0.20 171.54 170 5 4.54E-03 52.3 3 0 39.58 23 0 0.43 197.26 194 7 l.28E-02 20.9 Flag: "*" == Peak area was modified by background subtraction Page 2451 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:35:02.32 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627533.CNF;l *

Acquisition date 29-SEP-2016 08:04:21 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time' 0 00:30:00.03 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Analyst initials: MJHl *

Sample ID Il203627533 Sample Quantity 2.9800E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF 'XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 1.213E+Ol Cnt uncert ( 1. 96-sigma) 2.478E+OO Non-Identified Nuclides Nuclide I-125 Page 2452 of 5809 Key-Line Activity (pCi/GRAM -7.798E+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.043E+Ol MDA (pCi/GRAM l.320E+OO MDA (pCi/GRAM 1.426E+Ol NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:34:59.87 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.69 129 13 0.58 147.75 143 11 7.15E-02 10.4 2 0 34.44 8 4 0.20 171. 54 170 .5 4.54E-03 52.3 3 0 39.58 23 0 0.43 197.26 194 7 1.28E-02 20.9 Page 2453 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:35:01.61 Nuclide Line Activity Report Nuclide Type: .FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error I-129 29.62 129 56.60* 9.442E+OO l.213E+Ol 1. 213E+Ol 20.84 33.59 8 10.04 1.026E+Ol 3.995E+OO 3.995E+OO 104.62 39.58 23 7.51 9.700E+OO 1. 591E+Ol 1.591E+Ol 41.70 Flag: "*" Key line Page 2454 of 5809 Summary of Nuclide Activity Sample ID : I1203627533 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 29-SEP-2016 08:04:21 Number of lines tentatively identified by NID 3 0 3 100.00% Nuclide Type : FISSION Nuclide I-129 Hlife l.57E+07Y Uncorrected Decay pCi/GRAM 1.00 1.213E+Ol Total Activity 1.213E+Ol Grand Total Activity 1.213E+Ol Flags: "K" "E" Page 2455 of 5809 Keyline not found Manually edited Decay Corr pCi7GRAM 1.213E+Ol 1.213E+Ol 1. 213E+Ol Decay Corr 2-Sigma Error 0.253E+Ol Manually accepted 2-Sigma %Error Flags 20.84 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : Il203627533 None Flags: "T" Tentatively associated Page 2456 of 5809 Acquisition date Page : 3 29-SEP-2016 08:04:21 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:35:05.87 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627533.CNF;l * *Acquisition date 29-SEP-2016 08:04:21 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Nuclide Library : IODINE *

Sample ID I1203627533 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 2.9800E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 5.321E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2457 of 5809 Le (pCi/GRAM 5.051E+OO NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 08:35:08.07 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627533.CNF;l * *Acquisition date 29-SEP-2016 08:04:21 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 14-DEC-2015 13:47:00 Nuclide Library : IODINE *

Sample ID I1203627533 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 2.9800E+OO GRAM *

Quantity Err(%) 3.3557E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09'Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1.213E+Ol Act Error ( 1. 96-sigma) 2.760E+OO Non-Identified Nuclides Nuclide I-125 Page 2458 of 5809 Key-Line Activity (pCi/GRAM -.7.798E+00 K.L Act error ( 1 . 96-sigma) 1.046E+Ol TPU (1.96-sigma) 2.760E+OO TPU (1.96-sigma) 1.103E+Ol NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2459 of 5809 MDA COUNTS 7.0786. 5.8572 2.9842 2.0593 3.1623 1.6568 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:03:59.48 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627534.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 12:22:54 Sample date 27-SEP-2016 00:00:00 Acquisition date : 29-SEP-2016 08:33:28 Sample ID Il203627534 Sample quantity 4.23000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.16 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598663 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.69 5 15 0.26 123.73 120 7 2.94E-03125.9 2 0 29.77 352 56 1. 06 149.35 .142 16 1.95E-01 7.3 3 0 33.93 91 9 1. 58 170.28 161 18 5.06E-02 13.0 4 0 39.61 54 0 0.83 198.93 194 10 3.00E-02 13. 6 Flag: "*" = Peak area was modified by background subtraction Page 2460 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:04:00.30 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627534.CNF;l *

Acquisition date 29-SEP-2016 08:33:28 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.16 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Analyst initials: MJHl *

Sample ID Il203627534 Sample Quantity 4.2300E+OO GRAM *

Batch Number 1598663 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMAJEFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 1.002E+Ol Cnt uncert ( 1. 96-sigma) 1.438E+OO Non-Identified Nuclides Nuclide I-125 Page 2461 of 5809 Key-Line Activity (pCi/GRAM -6.783E-02 K.L. Cnt Uncert ( 1. 96-sigma) 2.419E-01 MDA (pCi/GRAM 6.886E-01 MDA (pCi/GRAM 3.747E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:03:58.77 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.69 5 15 0.26 123.73 120 7 2.94E-03125.9 2 0 29.77 352 56 1. 06 149.35 142 16 1. 95E-01 7.3 3 0 33.93 91 9 1. 58 170.28 161 18 5.06E-02 13. 0 4 0 39.61 54 0 0.83 198.93 194 10 3.00E-02 13.6 Page 2462 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 _09:03:59.87 Nuclide Line Activity Report Nuclide Type: FISSION Nuclide I-129 Flag: "*" Page 2463 of 5809 Energy 29.62 33.59 39.58 Key line Area 352 91 54 %Abn 56.60* 10.04 7.51 %Eff 2.203E+Ol 2.307E+Ol 2.288E+Ol Uncorrected pCi/GRAM 1.002E+Ol 1.397E+Ol 1.115E+Ol Decay Corr pCi/GRAM 1.002E+Ol l.397E+Ol 1.115E+Ol 2-Sigma %Error 14.65 26. 01 27.22 Summary of Nuclide Activity Sample ID : I1203627534 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 29-SEP-2016 08:33:28 Number of lines tentatively identified by NID 4 1 3 75.00% Nuclide Type : FISSION Nuclide I-129 Hlife 1.57E+07Y Uncorrected Decay pCi/GRAM 1. 00 1. 002E+Ol Total Activity 1.002E+Ol Grand Total Activity 1.002E+Ol Flags: "K" "E" Page 2464 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM 1. 002E+Ol 1. 002E+Ol 1. 002E+Ol Decay Corr 2-Sigma Error 0.147E+Ol Manually accepted 2-Sigma %Error Flags 14.65 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627534 Page : 3 Acquisition date : 29-SEP-2016 08:33:28 It 0 Energy 24.69 Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 15 0.26 123.73 120 7 2.94E-03 **** 1.89E+Ol Flags: "T" = Tentatively associated Page 2465 of 5809 VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:04:01.83 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627534.CNF;l *

Acquisition date 29-SEP-2016 08:33:28 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.16 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627534 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity : 4.2300E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 3.058E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2466 of 5809 Le (pCi/GRAM 1.667E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 29-SEP-2016 09:04:02.91 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Ro-ad *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627534.CNF;l *

Acquisition date 29-SEP-2016 08:33:28 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.16 Half life ratio : ***** *

Sample date 27-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627534 Analyst initials: MJHl *

Batch Number 1598663 Sample Quantity 4.2300E+OO GRAM *

Quantity Err(%) 2.3641E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1.002E+Ol Act Error ( 1. 96-sigma) 1.740E+OO Non-Identified Nuclides Nuclide I-125 Page 2467of5809 Key-Line Activity (pCi/GRAM -6.783E-02 K.L Act error ( 1. 96-sigma) 2.422E-01 TPU ( 1. 96-sigma) 1.740E+OO TPU ( 1. 96-sigma) 2.441E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2468 of 5809 MDA COUNTS 26.1663 21.2045 8.6562 4.4924 1.3822 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS Effective 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 09/28/16 Batch#. __ 1_5_9_8_6_1_8 __ _ Product: 1-129 / MJWC Date: 09/28/16 Criteria: Samele Solids are less than or equal to 100 m11 for GAB. Samples have been blank corrected (If required). Blank correction recorted Included (If reaulred\. [f activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40*/o or less. lf be*ow the MDA/ MDC error Is lrnstrument source check Is within limits. hnstrumeot bkg check Is w**i.*n Method RDL/ LLD has been met. If ducllcate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 00/o, Or meets the client's reaulred RER acceotance criteria. Tracer vleld Is 15-1250/o

Carrier vleld 25*1250/o. {Or meets the cllent's contract acceptance criteria). Method blank Is less than the RDL/ LLD. Uf.rild samole:;. < 50/o of lowe"'" .. *h*' Samole was run within hold time. Samele was correctlv oreserved If reaulred. Smears Taken for Radioactive batches. Method Spike and LCS are within 75*125% Ir nr meets the client'.: cnn .. ac,,entancA crlterl"' Aux data ls correct. Client Snech1I renulrements oaae has been checked. Data and I or snectrum are Included and crooerlv statused. MS, LCS, and Duolicate RPD/RER values uploaded to LIMS and "alue" verified :ur* m Yes No Comments n/a n/a ./ In'"' _,/ !t'J-t-/ Ve-r 11,/ n/a ,/ ,/ ,/ ,/ ./' ,/ J' J' GL-CHL-RAD-013 Rev 1 Page 1 of 1 Batch Data Exceotlon Renorts (DER) completed If annllcable. v i\n/a i)e-y 'It /l':;/,..Z.'IZ I Batch Data Exception Reports (DER) second reviewed. Dlsoosltlon verified to be comcleted. Allnuot Correction comnleted if rO""'red, / ,,/ Review sample historical results If available / (If REMP, results above MDC have been verified .., bv historical results recount or re-analvsls. \ ni\ Primary Revl1;1w Performed b_ Secondary Review Performed cfL ___ C;__ Page 2469 of 5809 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 28-SEP-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1598618 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE EML HASL-300,1-01 Modified Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception
Description:
DER Report No.: 1562421 Revision No.: 1 Type: Process Client Code: MJWC Samples received out of holding: Samples were counting in a timely manner upon receipt. Reporting results. 405235 001,002,003,004,005,006,007,008,009, 010,011,012,013,014,015,016,017,018, 019,020 QC 1203627 431DUP,1203627 432MS Originator's Name: Data Validator/Group Leader: Spencer Collins 28-SEP-16 Bryan Williams 29-SEP-16 Page 1 Page 2470of5809 0 >-+) Vo 00 0 \0 I-129 Queue Sheet 09il4i2016 Batch #:1598618 Analyst: !"1JH1 flrst Client Due Date:l0/04/2016 Internal Due Date:09/30/2016 Spike Isotope: I-129 LCS Isotope: I-129 SpikcCode: il-1/c-K LCS Code: Expiration Date: Expiration Date: Vol: o.l.......l Vol: c;>.l<M-L. Nominal Concentration: NA ------Nominal Concentration: __
Prep Date:CJ-'2.6*-tb Initials: Pipette ID: )J.\2'l5D'3 \Vitness: ----------1:5?-'-1 Aliquot Sample ID Client Description 40523:5001-1 405235002-l -105235003-1 405235004-1 405235005-1 405235006-1 405235007-1 405235008-1 405235009-1 -105235010-1 405235011-1 -105235012-1 405235013-1 -105235014-1 405235015-1 405235016-1 4 052350 I 7-1 405235018-1 -105235019-l 405235020-1 J20.'!6!i430-l 1203627431-i 1203627432-1 1203627433-l 4.l.B.R.1.2 4.J.B.R.1.3 -1.l.B.R.JA 4.1.B.R..7.2 4.J.C.R.1.3 -1.l.C.R.lA 4.1.C.R.:D 4.l.C.R.2.-1 -1.l.D.R.1.J 4.1.D.R.U 4.1.D.!Ll.2 .U.D.R.2.4 4.!A.R.2.3 4.2A.R.l.3 4.2A.R.IA 4.2A.R.3.2 4.2A.RA.2 4.2B.IUA 4.2B.R.l.4 !llB for 1598618 -U.B.R.1.2(405235-00lDUrJ LCS for batch 1598618 GEL Laboratories LLC, Rodioc/iemistry Division Type SAMPLE SA.MP LE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SA:'\IPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAi\IPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE .MB DUP MS I.CS Hazard Code RDL I pCilg 1 pCilg I pCL'g l pCL'g I pCiig 1 pCi/g 1 pCiig l pCiig I pCifg 1 pCi/g lpCL'g 1 pCi/g I pCL'g 1 pCL'g I pCL'g I pCi!g 1 pCiJg I pCilg I pCUg lpCUg l pCi!g 1 pCilg lpCi!g I pCilg ._,Va.T Client Matrix Collect Date (mL 01@ *Detector *:;' '2..0. M.lWCOOI SOIL -4 10-DEC-l:> R Z.cS ;<!;-I.Ah l\1JWCOOI SOIL l0-DEC-15 l-1:30AJ./ z.S\; 'f.:1.,. fvt5 3-CI:: MJWCOOI SOJL 10-DEC-15 14:J5p,;; i 2 . .,;:, I x.c; *:..12 i\1.JWCOOl SOIL 09-DEC-15 14:00A'i i .2 5 2 x:. 6 MS MJWCOOl SOIL 10.DEC-15 13:15;\> i 1.. '"1;, i ){I-( ,.'-\; ;'o.l.lWCOOl SOIL ., MJWCOOI SOIL 10-DEC-1513:25;.t, j 2 i'8 j )(!) p.11.5 IO.DEC-1513:55 A1 j*---2.1.0 j Xb I 1"'15 3 :is MJWCOO! SOIL 3.'-1'-l MJWCOOI SOIL '1-12 l\IJWC-001 SOIL g,,z MJWCOOI SOIL l0-DEC-1514:05M; l.-5o l )<'.j fM..<; IO-DEC-t510:30A'1 f z.b3 '{..1.. p.ttS 10-DEC-1510:35.t>,;ci --* u *1' [*" r }.."J 09-DEC-1510:13,r.11 i '£1)"" 3.-;o MJWCOOI SOIL *-;. ::."3 MJWCOOI SOIL '; .4.'-\ MJWCOOl SOIL MJWCOOJ SOIL 3.:;i i\IJWCOOI SOIL MJWCOOl SOIL '3 .'53 l\1JWC001 SOIL '3.i\ MJWCOOI SOIL 3 *fi MJWCOOI SOIL QC,\CCOUNT SOIL ".:>*\C QC ACCOUNT SOIL ;.1e QC ACCOUNT SOIL QC ACCOUNT SOIL 10-DEC-I5ll:25,1,12/ 2,l'-j )l.h.Jt./i,j OS-DEC-15 11:23.AHi 1.11 AU 1l_t}2. 08-DEC-15 10:49 08-DEC-1s 0_13 (!.% os-nEc-1s 11:29Al:d. 2_.i£i ;(SI n9-___ 02-DEC-1510:02FJ'li _ 3_ 2.1\o Xe.Jilt OS-DEC-JS 14:30M'1) 2.Sfc Xz£! -OS-DEC-15 13:50/\,Z.:\

2 ,"1 { )(Sj if cr-:&-1b A:l.1 l i. Y-t lrl::L.-10-nEc-1s 14:20,IW.:;;;::g *i-, * ., v"') * .t.l-t I " 7 -,Q /'-!-i 2.'5 (; Xlt l "' q_ zt, i b-:U<i! 3 3'1 JL..L j ff D"' R"1ow..i -Pagel of I Weight/Loss Aliquot Correction Report http://prodsvrOl.gel.com:7778/pls/lims/weight_loss _rpts.show _report 1of1 Weight/Loss Aliquot Correction Report Select What to Correct Aliquot to o* Ash Dry Weight '*' Dry Weight *o Wet Weight Batch ID: 1598618 Aliquot Correction to Dry Weight for Batch 1598618 -;;;pie Id jAiiquot-(G)-lsample Type !Parent Sample Id !Loss (Dec) I corrected Aliquot (G) Is f40ill j40 523500 I j3.29 lsAMPLE 5235002 jsAMPLE 140 5235003 13.06 jsAMPLE Jii2' . *****-**1sAMPLE 5235004 5235005 f3.43 jsAMPLE 140 if4052 140 5235006 _[3.45-[SAMPLE 140 5235007 /3.30 -5235008[3.25 \40 .Foills :14 05235009 13.44 :14 ;14.18 05235010 05235011 -13.12 05235012 l3.3o ** 14 '.[4Q 05235013 -13.53 05235014 13.44 jsAMPLE lsAMPLE jsAMPLE -I SAMPLE jsAMPLE

1SAMPLE I SAMPLE jsAMPLE jNA \NA INA jNA JNA jNA \NA-jNA \NA jNA INA [NA INA 14 14! [40s 052350JSj3.37 ____ lsAMPLE -\NA 14 14 0523sol6-J3.Ss 05235017 13.01 05235018 J 3.53 *f4Dm il4 05235019 05235020 li1i j 3.47 I 1 I 1 2036274301 203627431 / 3.10 lsAMPLEjNA lsAMPLE INA -jsAMPLE jNA . ** 1sAMPLE jNA *:1sAMPLE jNA IMB fNA ****/ouP 1405235001 1.1942 .i 2.6s10660266so666; 1-2235 12.360379856739744 . . . . . *f.i736 .j 2:s28?-2s584719417* l.i 938 --.12.sis3:6oi4462366-j.2039 j 2.7305743181i6s59* 1.1950 j.2124 ./ 2.598888698402866: [.2073 :1 /.2364 :/ 2.6267so391974iocii 1.2011 -j.1630 :f2.61i4o!i1.66i8s86:3. *1.1695 12.7404a2o383iso4 1.2159 j 2.767562944111547 j.1517 :[ j.0714 I 3.1292ii4ii8ssl711 1.2043 -1*2.s4aisii2i'2ioi27*** j.2250 j 2.3326564Gso1s990! .* f2167 ,j 2.764182914942685-'j.1752 *I 2.s64ssis-9s7i2oa4 1.1427 j INA I '/.1942 *j 2.497964949i2:in8i i-1-GEL Laboratories LLC Page 2472 of 5809 9/27/2016 11 :28 AM VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:08.82 ********************************************************************************

GEL Laboratories.LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235001.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : Z5-SEP-2016 12:23:10 Sample date 10-DEC-2015 14:20:00 Acquisition date : 27-SEP-2016 12:26:55 Sample ID I405235001 Sample quantity 2.65000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.20 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.23* 0 10 0.27 80.58 78 5 8.63E-05***** 2 0 25.34 6 3 0.25 126.21 123 6 1. 64E-03 62.4 3 0 27.18 7 7 0.74 135.45 131 9 1. 77.6 4 0 42.46 6 4 0.43 212.03 208 8 1. 61E-03 73.1 5 0 71. 46 11 2 0.92 357.31 354 7 3.09E-03 36.1 6 0 113 .16 10 0 1. 37 566.30 561 10 2.78E-03 31. 6 7 0 185.92* 8 2 0.88 930.99 927 8 2.28E-03 56.7 Flag: "*" = Peak area was modified by background subtraction Page 2473 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:09.87 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235001.CNF;l *

Acquisition date 27-SEP-2016 12:26:55 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 10-DEC-2015 14:20:00 *Analyst initials: MJHl *

Sample ID I405235001 Sample Quantity 2.6500E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Activity (pCi/GRAM 4.290E+OO Cnt uncert ( 1. 96-sigma) 6.523E+OO Non-Identified Nuclides Nuclide I-129 Page 2474 of 5809 Key-Line Activity (pCi/GRAM -l.600E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1. 7 63E-01 MDA (pCi/GRAM 8.870E+00 MDA (pCi/GRAM 3.719E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:07.90 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.23 8 10 0.27 80.58 78 5 2.08E-03 72. 4 2 0 25.34 6 3 0.25 126.21 123 6 1. 64E-03 62.4 3 0 27.18 7 7 0.74 135.45 131 9 1. 93E-03 77.6 4 0 42.46 6 4 0.43 212.03 208 8 1. 61E-03 73.l 5 0 71. 46 11 2 0.92 357.31 354 7 3.09E-03 36.1 6 0 113 .16 10 0 1. 37 566.30 561 10 2.78E-03 31. 6 7 0 185.92 13 2 0.88 930.99 927 8 3.66E-03 33.1 Page 2475 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:09.38 Nuclide Line Activity Report Nuclide Type: Nuclide Energy Area I-125 27.34 7 30.97 ------35.49 ------Flag: "*" Key line Page 2476of5809 %Abn 114.10* 20.30 6.68 %Eff 1.216E+Ol 1.514E+Ol 1.660E+Ol Uncorrected Decay Corr pCi/GRAM pCi/GRAM 1.422E-01 4.290E+OO ------Line Not Found ------Line Not Found 2-Sigma %Error 155.15 Summary of Nuclide Activity Sample ID : 1405235001 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 27-SEP-2016 12:26:55 Number of lines tentatively identified by NID 7 6 1 14.29% Nuclide Type : Nuclide I-125 Hlife 59.40D Uncorrected Decay pCi/GRAM 30.2 1.422E-01 Total Activity l.422E-01 Grand Total Activity 1.422E-01 Flags: "K" "E" Page 2477 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM 4.290E+OO 4.290E+OO 4.290E+OO Decay Corr 2-Sigma Error 6.656E+OO Manually accepted 2-Sigma %Error Flags 155.15 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235001 Acquisition date : 27-SEP-2016 12:26:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 25.34 6 3 0.25 126.21 123 6 l.64E-03 **** 1. 02E+Ol 0 42.46 6 4 0.43 212.03 208 8 l.61E-03 **** 1. 52E+Ol 0 71.46 11 2 0.92 357.31 354 7 3.09E-03 72 .1 2.88E+OO 0 113 .16 10 0 1. 37 566.30 561 10 2.78E-03 63.2 8.28E-02 0 185.92 8 2 0.88 930.99 927 8 2.28E-03 **** 8.06E-05 Flags: "T" = Tentatively associated Page 2478 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:11.81 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235001.CNF;l *

Acquisition date 27-SEP-2016 12:26:55 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *

Sample ID I405235001 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.6500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Le (pCi/GRAM 3.613E+OO ----Non-Identified Nuclides Nuclide I-129 ,/ Le (pCi/GRAM 1.384E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:13.05 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235001.CNF;l *

Acquisition date 27-SEP-2016 12:26:55 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE :1

Sample ID I405235001 Analyst initials: MJHl

Batch Number 1598618 Sample Quantity 2.6500E+OO GRAM *

Quantity Err(%) 3.7736E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff. Cal. date* 17-JUN-2016 08:18:14 Eff. Geometry : 'I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 4.290E+OO Act Error (1. 96-sigma) 6. 571E+OO Non-Identified Nuclides Nuclide I-129 Page 2480 of 5809 Key-Line Activity (pCi/GRAM -1.600E-02 K.L Act error ( 1. 96-sigma) 1. 763E-01 TPU ( 1. 96-sigma) 6. 571E+OO TPU ( 1. 96-sigma) l.765E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2481 of 5809 MDA COUNTS 6.5146 3.3266 6.7326 0.0000 2.3289 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:33.97 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235002.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Configuration Background file Background date : 25-SEP-2016 12:22:59 Sample date 10-DEC-2015 14:30:00 Acquisition date : 27-SEP-2016 12:27:18 Sample ID I405235002 Sample quantity 2.36000E+OO GRAM Detector name : XRAY2 Detector geometry: 1129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.19 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 4.99* 22 119 0.42 23.87 22 6 6.08E-03101.3 2 0 21. 91 17 3 1. 63 108.60 103 12 4.67E-03 32.1 3 0 63.35* 16 0 0.64 316.05 310 12 4.38E-03 31.5 4 0 74.97* 8 3 0.29 374.22 369 11 2.13E-03 66.0 5 0 95.89 5 4 0.26 478.98 474 8 1.30E-03 88.4 6 0 113 .15 7 6 1. 54 565.43 557 12 1.94E-03 79.5 7 0 164.06 8 7 1. 84 820.40 809 13 2.08E-03 79.0 8 0 238.95 9 9 0.36 1195. 49 1186 14 2.55E-03 80.7 Flag: "*" = Peak area was modified by background subtraction Page 2482 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:34.85 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA. GAMMA.ARCHIVE. GAMMA] I405235002.*CNF;1 * *Acquisition date 27-SEP-2016 12:27:18 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 10-DEC-2015 14:30:00 Analyst initials: MJHl *

Sample ID I405235002 Sample Quantity 2.3600E+00 GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1. 963E+OO 6. 722E+OO I-129 1.088E-01 2.783E-01 Page 2483 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 462E+Ol 5.982E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:33.24 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 4.99 194 119 0.42 23.87 22 6 5.40E-02 11.1 2 0 . 21. 91 17 3 1. 63 108.60 103. 12 4.67E-03 32.1 3 0 63.35 21 0 0.64 316.05 310 12 5.83E-03 21. 8 4 0 74.97 13 3 0.29 374.22 369 11 3.63E-03 37.2 5 0 92.52 13 6 0.60 462.12 455 11 3.47E-03 46.0 6 0 95.89 5 4 0.26 478.98 474 8 1.30E-03 88.4 7 0 113 .15 7 6 1. 54 565.43 557 12 1.94E-03 79.5 8 0 164.06 8 7 1. 84 820.40 809 13 2.08E-03 79.0 9 0 186.52 9 14 0.37 932.89 920 14 2.50E-03 94.3 10 0 238.95 9 9 0.36 1195.49 1186 14 2.55E-03 80.7 Page 2484 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:34.35 Nuclide Line Activity Report Flag: "*" = Keyline Page 2485 of 5809 Summary of Nuclide Activity Sample ID : 1405235002 Acquisition date Page : 2 27-SEP-2016 12:27:18 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2486 of 5809 Keyline not found Manually edited "M" "A" 8 8 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235002 Acquisition date : 27-SEP-2016 12:27:18 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 4.99 22. 119 0.42 23.87 22 6 6.08E-03 **** O.OOE+OO 0 21. 91 17 3 1. 63 108.60 103 12 4.67E-03 64.1 4.42E-01 0 63.35 16 0 0.64 316.05 310 12 4.38E-03 63.1 1.73E-02 0 74.97 .8 3 0. 29 374.22 369 11 2.13E-03 ':*** l.37E-04 0 95.89 5 4 0 .26 478.98 474 8 l.30E-03 **** 8.41E-09 0 113 .15 7 6 1. 54 565.43 557 12 1. 94E-03 **** 1.64E-12 0 164.06 8 7 1. 84 820.40 809 13 2.08E-03 **** 5.13E-24 0 238.95 9 9 0.36 1195. 49 1186 14 2.55E-03 **** O.OOE+OO Flags: "T" = Tentatively associated Page 2487 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:36.43 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235002.CNF;l * *Acquisition date 27-SEP-2016 12:27:18 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 10-DEC-2015 14:30:00 Nuclide Library : IODINE *

Sample ID I405235002 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.3600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2488 of 5809 Le (pCi/GRAM 6.019E+OO NOT IDENT. 2.517E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:37.57 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235002.CNF;l *

Acquisition date 27-SEP-2016 12:27:18 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.19 Half life ratio : ***** *

Sample date 10-DEC-2015 14:30:00 Nuclide Library : IODINE *

Sample ID I405235002 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.3600E+00 GRAM *

Quantity Err(%) 4.2373E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide {pCi/GRAM (1.96-sigma) I-125 l.963E+OO 6.730E+OO I-129 l.088E-01 2.785E-01 Page2489of5809 TPU (1.96-sigma) TPU (1.96-sigma) 6.788E+00 2.828E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 27.34 5.2595 29.62 6.4220 \ 27.34 8. 6471 29.62 4.4030 35.49 8.9174 39.58 9.1471 Page 2490 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:58.44 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235003.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 10-DEC-2015 14:35:00 Acquisition date : 27-SEP-2016 12:27:38 Sample ID I405235003 Sample quantity 2.53000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.67* BACKGROUND CORRECTED SAMPLE* PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 3 5 0.73 316.68 312 9 7.98E-04179.4 Flag: "*" = Peak area was modified by background subtraction Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:59.28 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235003.CNF;l *

Acquisition date 27-SEP-2016 12:27:38 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 10-DEC-2015 14:35:00 Analyst initials: MJHl *

Sample ID I405235003 Sample Quantity 2.5300E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File . : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.199E+00 3. 231E+OO I-129 2.377E-01 2.329E-01 Page 2492 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 9.382E+OO 7.137E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:57.72 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2493 of 5809 Energy 63. 67 Area 10 Bkgnd FWHM Channel 5 0.73 316.68 Left 312 Pw Cts/Sec %Err 9 2. 64E-03 51. 7 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:28:58.79 Nuclide Line Activity Report Flag: "*" = Keyline Page 2494 of 5809 Summary of Nuclide Activity Sample ID : 1405235003 Acquisition date Page : 2 27-SEP-2016 12:27:38 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2495 of 5809 Keyline. not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% = .Manually accepted = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235003 Page : 3 Acquisition date : 27-SEP-2016 12:27:38 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63. 67 3 5 0.73 316.68 312 9 7.98E-04 **** 3.12E+OO Flags: "T" = Tentatively associated Page 2496 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:00.88 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235003.CNF;l * *Acquisition date 27-SEP-2016 12:27:38 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 10-0EC-2015 14:35:00 Nuclide Library : IODINE *

Sample ID I405235003 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.5300E+OO GRAM *

Recovery 1. 00000 Carrier Weight : 0. 00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2497 of 5809 Le (pCi/GRAM 3.324E+OO NOT IDENT. 2.765E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:02.06 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA *

* *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235003.CNF;l *

Acquisition date 27-SEP-2016 12:27:38 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 10-DEC-2015 14:35:00 Nuclide Library : IODINE *

Sample ID I405235003 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.5300E+OO GRAM *

Quantity Err(%) 3.9526E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. *cal. date 30-AUG-2016 11:41:11 Eff. : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 L 199E+OO 3.237E+OO I-129 2.377E-01 2.342E-01 Page 2498 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.282E+OO 2.575E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2499 of 5809 MDA COUNTS 0.8133 0.0000 0.0000 2. 7 692 1.9087 3.0566 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:21.90 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 9-DEC-2015 14:00:00. Acquisition date : 27-SEP-2016 12:27:59 Sample ID I405235004 Sample quantity 2.52000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 63.36* 81.17* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 4 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.47 316.22 2 0.38 405.30 313 402 7 1.00E-03 89.9 7 1.32E-03 74.3 Flag: "*" = Peak area was modified by background subtraction Page2500of5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:22.80 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l *

Acquisition date 27-SEP-2016 12:27:59 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 9-DEC-2015 14:00:00 Analyst initials: MJHl *

Sample ID I405235004 Sample Quantity 2.5200E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129'.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1. 726E+OO 4.133E+OO I-129 2.594E-02 2.210E-01 Page 2501of5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.935E+OO 5.123E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:21.16 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2502 of 5809 Energy 63.36 81.17 Area 9 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.47 316.22 2 0.38 405.30 313 402 7 2.50E-03 33.3 7 1. 98E-03 48. 8 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:22.26 Nuclide Line Activity Report Flag: "*" = Keyline Page 2503 of 5809 Summary of Nuclide Activity Sample ID : 1405235004 Acquisition date Page : 2 27-SEP-2016 12:27:59 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2504 of 5809 Keyline not f.ound Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235004 Page : 3 Acquisition date : 27-SEP-2016 12:27:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 63.36 81.17 4 5 0 0.47 2 0.38 Flags: = Tentatively associated Page 2505 of 5809 316.22 313 7 1.00E-03 **** 3.07E+OO 405.30 402 7 1.32E-03 **** 9.25E-01 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:24.41 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l *

Acquisition date 27-SEP-2016 12:27:59 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 9-DEC-2015 14:00:00 Nuclide Library : IODINE *

Sample ID I405235004 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.5200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKA100': [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2506 of 5809 Le (pCi/GRAM 2.192E+00 NOT IDENT. l.805E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:25.55 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l *

Acquisition date 27-SEP-2016 12:27:59 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 9-DEC-2015 14:00:00 Nuclide Library : IODINE *

Sample ID I405235004 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.5200E+00 GRAM *

Quantity Err(%) 3.9683E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geome'try : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1. 726E+OO 4.136E+OO I-129 2.594E-02 2.210E-01 Page 2507 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.208E+OO 2.213E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2508 of 5809 MDA COUNTS 2.8315 1.4643 1. 4 921 0.0000 1.5811 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:01.35 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 10-DEC-2015 13:15:00 Acquisition date : 27-SEP-2016 15:11:29 Sample ID I405235005 Sample quantity 2.73000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 44.78 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0 0.29 223.67 220 6 3.33E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 2509 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:02.44 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l *

Acquisition date 27-SEP-2016 15:11:29 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 10-DEC-2015 13:15:00 Analyst initials: MJHl * *Sample ID I405235005 Sample Quantity 2.7300E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File DKA100: [CANBERRA:GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -1.488E+OO 5.457E+OO I-129 1.289E-01 2.748E-01 Page 2510 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.099E+Ol 7.339E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:00.22 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2511of5809 Energy 44.78 Area 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.29 223.67 220 6 3.33E-03 40.8 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:01.84 Nuclide Line Activity Report Flag: "*" = Keyline Page 2512of5809 Summary of Nuclide Activity Sample ID : 1405235005 Acquisition date Page : 2 27-SEP-2016 15:11:29 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2513 of 5809 Keyline not found Manually edited "M" "A" l 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235005 Page : 3 Acquisition date : 27-SEP-2016 15:11:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 44.78 6 0 0.29 223.67 220 6 3.33E-03 81.6 1.41E+Ol Flags: "T" = Tentatively associated Page 2514of5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:04.03 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l *

Acquisition date 27-SEP-2016 15:11:29 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 10-DEC-2015 13:15:00 Nuclide Library : IODINE *

Sample ID I405235005 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7300E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2515of5809 Le (pCi/GRAM 3.893E+OO NOT IDENT. 2.747E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:05.13 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l *

Acquisition date 27-SEP-2016 15:11:29 : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 10-DEC-2015 13:15:00 Nuclide Library : IODINE *

Sample ID I405235005 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7300E+OO GRAM *

Quantity Err(%) 3.6630E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -l.488E+00 5.463E+OO I-129 1.289E-01 2.751E-01 Page 2516of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.504E+OO 2.812E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2517 of 5809 MDA COUNTS 3.2573 1.1089 2.2442 1.1470 0.0000 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:13.53 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 10-DEC-2015 13:25:00 Acquisition date : 27-SEP-2016 15:11:52 Sample ID I405235006 Sample quantity 2.78000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.02 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike IQ : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 131. 03 BACKGROUND CORRECTED SAMPLE PEAK REPORT

Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 0 0.55 652.14 645 12 3.89E-03 37.8 Flag: "*" = Peak area was modified background subtraction Page 2518 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:14.33 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l *

Acquisition date 27-SEP-2016 15:11:52 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *

Sample date 10-DEC-2015 13:25:00 Analyst initials: MJHl * *Sample ID I405235006 Sample Quantity 2.7800E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line , Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.842E+OO 3. 611E+OO I-129 4.326E-01 4.240E-01 Page 2519of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.356E+Ol l.299E+OO NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:12.79 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2520 of 5809 Energy 131.03 Area 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.55 652.14 645 12 3.89E-03 37.8 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:13.87 Nuclide Line Activity Report Flag: "*" = Keyline Page 2521 of 5809 Summary of Nuclide Activity Sample ID : I405235006 Acquisition date Page : 2 27-SEP-2016 15:11:52 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: !'K" "E" Page 2522 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235006 Page .: 3 Acquisition date : 27-SEP-2016 15:11:52 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 131. 03 7 0 0.55 652.14 645 12 3.89E-03 75.6 1.35E-02 Flags: "T" = Tentatively associated Page 2523 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:16.31 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l *

Acquisition date 27-SEP-2016 15:11:52 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *

Sample date 10-DEC-2015 13:25:00 Nuclide Library : IODINE *

Sample ID I405235006 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7800E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2524 of 5809 Le (pCi/GRAM 4.286E+OO NOT IDENT. 5.032E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:17.50 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l *

Acquisition date 27-SEP-2016 15:11:52 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: O 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *

Sample date 10-DEC-2015 13:25:00 Nuclide Library : IODINE *

Sample ID I405235006 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7800E+OO GRAM *

Quantity Err(%) 3.5971E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1. 842E+OO 3.625E+OO I-129 4.326E-01 4.262E-01 Page 2525 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.719E+OO 4.687E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2526 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 0.9231 0.9543 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:38.92 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 10-DEC-2015 13:55:00 Acquisition date : 27-SEP-2016 15:12:14 Sample ID I405235007 Sample quantity 2.60000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2527 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:39.74 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* **

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l *

Acquisition date 27-SEP-2016 15:12:14 Sensitivity 3.000 *

Detector ID . XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 10-DEC-2015 13:55:00 Analyst initials: MJHl *

Sample ID I405235007 Sample Quantity 2.6000E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-s igma) I-125 -2.559E+OO 5.015E+00 I-129 -2.761E-01 4.587E-01 Page 2528 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.898E+OO 6.039E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:38.06 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2529 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:39.28 Nuclide Line Activity Report Flag: "*" = Keyline Page 2530 of 5809 Summary of Nuclide Activity Sample ID : 1405235007 Acquisition date Page : 2 27-SEP-2016 15:12:14 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2531 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235007 None Flags: "T" Tentatively associated Page 2532 of 5809 Acquisition date Page : 3 27-SEP-2016 15:12:14 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:41.27 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l * *Acquisition date 27-SEP-2016 15:12:14 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 10-DEC-2015 13:55:00 Nuclide Library : IODINE *

Sample ID I405235007 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.6000E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6'I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2533 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. 1.553E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:42.27 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l *

Acquisition date 27-SEP-2016 15:12:14 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 10-DEC-2015 13:55:00 Nuclide Library : IODINE *

Sample ID I405235007 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.6000E+OO GRAM *

Quantity Err(%) 3.8462E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 . * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry* : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.559E+OO 5.020E+OO I-129 -2.761E-01 4.595E-01 Page 2534 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.151E+OO 4.761E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2535 of 5809 MDA COUNTS 1. 4157 2.9286 0.0000 0.0000 1. 5811 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:39.41 ********************************************************************************

GEL Laboratories LLC 1 * * -2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 -Sample date 10-DEC-2015 14:05:00 Acquisition date : 27-SEP-2016 16:19:05 Sample ID I405235008 . Sample quantity 2. 58000E+OO GRAM Detector name : XRAYl Detector geometry: I129 . Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.23 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 72. 29 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 11 0 0.63 363.64 360 8 3.06E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 2536 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:40.21 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l *

Acquisition date 27-SEP-2016 16:19:05 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.23 Half life ratio : ***** *

Sample date 10-DEC-2015 14:05:00 Analyst initials: MJHl *

Sample ID I405235008 Sample Quantity 2.5800E+00 GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.033E+OO 3.175E+OO I-129 -l.212E-01 l.964E-01 Page 2537 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.873E+OO 3.623E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:38.71 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2538 of 5809 Energy 72.29 Area 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.63 363.64 360 8 3.06E-03 30.2 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:39.76 Nuclide Line Activity Report Flag: "*" = Keyline Page 2539 of 5809 Summary of Nuclide Activity Sample ID : 1405235008 Acquisition date Page : 2 27-SEP-2016 16:19:05 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2540 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235008 Page : 3 Acquisition date : 27-SEP-2016 16:19:05 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 72.29 11 0 0.63 363.64 360 8 3.06E-03 60.3 1.13E+Ol Flags: "T" = Tentatively associated Page 2541 of 5 809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:41.88 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l *

Acquisition date 27-SEP-2016 16:19:05 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.23 Half life ratio : ***** *

Sample date 10-DEC-2015 14:05:00 Nuclide Library : IODINE *

Sample ID I405235008 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.5800E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2542 of 5809 Le (pCi/GRAM 2.937E+00 NOT IDENT. l.495E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:43.00 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 , * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l *

Acquisition date 27-SEP-2016 16:19:05 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.23 Half life ratio : ***** *

Sample date 10-DEC-2015 14:05:00 Nuclide Library : IODINE *

Sample ID I405235008 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.5800E+OO GRAM *

Quantity Err(%) 3.8760E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.033E+OO 3.195E+OO I-129 -1.212E-01 1. 968E-01 Page 2543 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 3.324E+OO 2.042E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2544 of 5809 MDA COUNTS 6.1327 12. 7227 5.1937 8.9849 6.4505 6.7829 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:13.31 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : Z5-SEP-2016 12:22:59 Sample date 10-DEC-2015 10:30:00 Acquisition date : 27-SEP-2016 16:18:41 Sample ID I405235009 Sample quantity 2.63000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.20 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.81* 7 14 0.43 83.03 77 11 2.0lE-03124.4 2 0 36.66 7 0 0.55 182.43 177 9 1.94E-03 37.8 3 0 41. 39 9 3 1. 36 206.11 200 10 2.62E-03 45.4 4 0 57.90 12 0 0.25 288.75 283 11 3.33E-03 28.9 5 0 63.05* 6 2 0.61 314.55 310 9 1.58E-03 82.0 6 0 64.67 6 2 0.45 322.66 319 7 1.74E-03 53.2 7 2 70.09 12 1 0. 96 349.79 346 13 3.39E-03 34.7 4. 21E-01 8 2 71.29 12 2 0.65 355.82 346 13 3.26E-03 32.l 9 0 93.00* 6 7 1.31 464.51 456 14 1. 7 lE-0312 6. 9 10 0 134.56 9 2 0.28 672.65 668 9 2.44E-03 45.7 11 0 182.13 11 6 0.42 910.91 904 12 3.06E-03 53.8 Flag: "*" = Peak area was modified by background subtraction Page 2545 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:14.37 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l *

Acquisition date 27-SEP-2016 16:18:41 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 10-DEC-2015 10:30:00 Analyst initials: MJHl *

Sample ID I405235009 Sample Quantity 2.6300E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 * '* Eff. File : DKAlOO: [CANBERRA.GAMMA']EFF XRAY2 I129.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.282E+OO 6.193E+OO I-129 4.861E-02 2.191E-01 Page 2546 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.361E+Ol 4.694E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:12.54 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 5.01 166 89 0.41 23.95 22 6 4.60E-02 11. 6 2 0 . 16. 81 21 14 0.43 83.03 .77 11 5.96E-03 39.8 3 0 36.66 7 0 0.55 182.43 177 9 1.94E-03 37.8 4 0 41. 39 9 3 1. 36 206.11 200 10 2.62E-03 45.4 5 0 57.90 12 0 0.25 288.75 283 11 3.33E-03 28.9 6 0 63.05 11 2 0.61 314.55 310 9 3.03E-03 38.9 7 0 64. 67 6 2 0.45 322.66 319 7 1. 74E-03 53.2 8 2 70.09 12 1 0. 96 349.79 346 13 3.39E-03 34.7 4.21E-01 9 2 71. 29 12 2 0.65 355.82 346 13 3.26E-03 32.l 10 0 93.00 23 7 1. 31 464.51 456 14 6.32E-03 32.4 11 0 134. 56 9 2 0.28 672.65 668 9 2.44E-03 45.7 12 0 182.13 11 6 0.42 910.91 904 12 3.06E-03 53.8 Page 254 7 of 5 809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:13.70 Nuclide Line Activity Report Flag: "*" = Keyline Page 2548 of 5809 Summary of Nuclide Activity Sample ID : 1405235009 Acquisition date Page : 2 27-SEP-2016 16:18:41 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2549 of 5809 Keyline not found Manually edited "M" "A" 11 11 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235009 Acquisition date : 27-SEP-2016 16:18:41 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.81 7 14 0.43 83.03 77 11 2.0lE-03 **** 7.68E-04 0 36.66 7 0 0.55 182.43 177 9 l.94E-03 75.6 2.36E+Ol 0 41. 39 9 3 1. 36 206.11 200 10 2.62E-03 90.7 1.34E+Ol 0 57.90 12 0 0.25 .288.75 283 11 3.33E-03 57.7 l.34E-01 0 63.05 6 2 0.61 314.55 310 9 l.58E-03 **** 1.95E-02 0 64.67 6 2 0.45 322.66 319 7 1. 74E-03 **** 1. 03E-02 2 70.09 12 1 0. 96 349.79 346 13 3.39E-03 69.5 1.12E-03 2 71. 29 12 2 0.65 355.82 346 13 3.26E-03 64.3 6. 72E-04 0 93.00 6 7 1. 31 464.51 456 14 1.71E-03 **** 3.38E-08 0 134.56 9 2 0.28 672. 65 668 9 2.44E-03 91. 4 2.81E-17 0 182 .13 11 6 0.42 910.91 904 12 3.06E-03 **** 3.32E-28 Flags: "T" = Tentatively associated Page 2550 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:16.11 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA

k *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l *

Acquisition date 27-SEP-2016 16:18:41 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 10-DEC-2015 10:30:00 Nuclide Library : IODINE *

Sample ID I405235009 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.6300E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15 '* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2551of5809 Le (pCi/GRAM 5.639E+OO NOT IDENT. 1.922E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:17.37 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l * *Acquisition date 27-SEP-2016 16:18:41 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *

Sample date 10-DEC-2015 10:30:00 Nuclide Library : IODINE *

Sample ID I405235009 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.6300E+OO GRAM *

Quantity Err(%) 3.8023E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.282E+OO 6.206E+OO I-129 4. 8 61E-02 2.191E-01 Page 2552 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 6.291E+OO 2.202E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2553 of 5809 MDA COUNTS 5.2595 5.3517 4.3235 5.5038 6.6880 8.5754 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:03.84 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 10-DEC-2015 10:35:00 Acquisition date : 27-SEP-2016 16:19:26 Sample ID I405235010 Sample quantity 3.34000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.21 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.66 3 6 0.32 122.81 119 7 9.57E-04123.8 2 0 27.52 6 6 0.40 137.17 132 8 1.62E-03 90.7 3 0 92.71* 9 3 0.61 463.84 459 11 2.52E-03 62.2 4 0 139.94 12 3 0.75 700.53 693 12 3.28E-03 41.5 5 0 158.54 7 5 1. 36 793.77 788 9 1. 81E-03 70. 7 6 0 185.65* 9 0 0.33 929.64 925 9 2.51E-03 45.1 7 0 202.95 9 0 0.65 1016.33 1012 9 2.50E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 2554 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:04.73 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l *

Acquisition date 27-SEP-2016 16:19:26 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *

Sample date 10-DEC-2015 10:35:00 Analyst initials: MJHl *

Sample ID I405235010 Sample Quantity 3.3400E+00 GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 * * 'Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Activity (pCi/GRAM 2.786E+OO Cnt uncert ( 1. 96-sigma) 4.954E+OO Non-Identified Nuclides Nuclide I-129 Page 2555 of 5809 Key-Line Activity (pCi/GRAM 2.999E-02 K.L. Cnt Uncert (1.96-sigma) l.554E-01 MDA (pCi/GRAM 6.562E+OO MDA (pCi/GRAM 3.474E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:03.10 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 17.21 6 12 0.20 85.51 80 8 1.76E-03102.3 2 0 24.66 3 6 0.32 122.81 119 7 9.57E-04123.8 3 0 27.52 6 6 0.40 137.17 132 8 1.62E-03 90.7 4 0 92.71 17 3 0.61 463.84 459 11 4. 72E-03 30.9 5 0 139.94 12 3 0.75 700.53 693 12 3.28E-03 41. 5 6 0 158.54 7 5 1. 36 793.77 788 9 l.81E-03 70.7 7 0 185.65 14 0 0.33 929.64 925 9 3.89E-03 26.7 8 0 202.95 9 0 0.65 1016.33 1012 9 2.50E-03 33.3 Page 2556 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:04.20 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-125 27.34 6 114 .10* 1.249E+Ol 9.202E-02 2.786E+OO 181.42 30.97 ------20.30 1.514E+Ol ------Line Not Found ------35.49 ------6.68 1.660E+Ol ------Line Not Found ------Flag: "*" Key line Page 2557 of 5809 Summary of Nuclide Activity Sample ID : 1405235010 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 27-SEP-2016 16:19:26 Number of lines tentatively identified by NID 7 6 1 14.29% Nuclide Type : Nuclide I-125 Hlif e 59.40D Uncorrected Decay pCi/GRAM 30.3 9.202E-02 Total Activity 9.202E-02 Grand Total Activity 9.202E-02 Flags: "K" "E" Page 2558 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM 2.786E+OO 2.786E+OO 2.786E+OO Decay Corr 2-Sigma Error 5.055E+OO Manually accepted 2-Sigma %Error Flags 181.42 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235010 Acquisition date : 27-SEP-2016 16:19:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 24.66 3 6 0.32 122.81 119 7 9.57E-04 **** 9.48E+OO 0 92.71 9 3 0.61 463.84 459 11 2.52E-03 **** 5.lOE-01 0 139.94 12 3 0.75 700.53 693 12 3.28E-03 83.0 6.82E-03 0 158.54 7 5 1. 36 793.77 788 9 1.81E-03 **** 1.15E-03 0 185.65 9 0 0.33 929.64 925 9 2.51E-03 90.2 8.28E-05 0 202.95 9 0 0.65 1016.33 1012 9 2.50E-03 66.7 l.52E-05 Flags: "T" = Tentatively associated Page 2559 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:06.35 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l *

Acquisition date 27-SEP-2016 16:19:26 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *

Sample date 10-DEC-2015 10:35:00 Nuclide Library : IODINE *

Sample ID I405235010 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 3.3400E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides".are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Le (pCi/GRAM 2.626E+OO ----Non-Identified Nuclides Nuclide I-129 Page 2560 of 5809 Le (pCi/GRAM l.360E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:07.54 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

* *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l *

Acquisition date 27-SEP-2016 16:19:26 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *

Sample date 10-DEC-2015 10:35:00 Nuclide Library : IODINE *

Sample ID I405235010 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 3.3400E+OO GRAM *

Quantity Err(%) 2.9940E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:'14 Eff. Geometry : 1129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 2.786E+OO Act Error ( 1. 96-sigma) 4.975E+OO Non-Identified Nuclides Nuclide I-129 Page 2561of5809 Key-Line Activity (pCi/GRAM 2.999E-02 K.L Act error ( 1. 96-sigma) 1.554E-01 TPU ( 1. 96-sigma) 4.975E+OO TPU ( 1. 96-sigma) l.560E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2562 of 5809 MDA COUNTS 5.4288 3.3266 4.4884 2.2941 8.1513 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:28.54 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 9-DEC-2015 10:13:00. Acquisition date : 27-SEP-2016 16:19:47 Sample ID I405235011 Sample quantity 2.61000E+00 GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.53* 2 .o 0.20 231. 33 229 5 5.61E-04135.4 2 0 63.38* 6 4 0.32 315.27 311 8 1.77E-03 82.2 3 0 74.74* 6 0 0.53 371. 80 369 6 1. 7 5E-03 53.3 4 0 78.54 9 3 0.20 390.74 383 11 2.47E-03 49.8 5 0 92.69* 3 0 0.70 461.22 457 8 9. 51E-04139. 4 6 0 162.02 8 3 0.39 806.47 800 11 2.35E-03 51. 0 Flag: "*" = Peak area was modified by background subtraction Page 2563 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:29.39 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l *

Acquisition date 27-SEP-2016 16:19:47 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 9-DEC-2015 10:13:00 Analyst initials: MJHl *

Sample ID I405235011 Sample Quantity 2.6100E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -4.152E-01 2.005E+OO I-129 9.429E-02 1.444E-01 Page 2564 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.607E+OO 4.988E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:27.85 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.53 6 0 0.20 231.33 229 5 1. 67E-03 40.8 2 0 63.38 13 4 0.32 315.27 311 8 3.61E-03 38.5 3 0 74.74 10 0 0.53 371. 80 369 6 2.78E-03 31. 6 4 0 78.54 9 3 0.20 390.74 383 11 2.47E-03 49.8 5 0 92. 69 18 0 0.70 461.22 457 8 5.00E-03 23.6 6 0 162.02 8 3 0.39 806.47 800 11 2.35E-03 51. 0 Page 2565 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:28.93 Nuclide Line Activity Report Flag: "*" = Keyline Page 2566 of 5809 Summary of Nuclide Activity Sample ID : 1405235011 Acquisition date Page : 2 27-SEP-2016 16:19:47 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2567 of 5809 Keyline not found Manually edited "M" "A" 6 6 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235011 Acquisition date : 27-SEP-2016 16:19:47 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.53 2 0 0.20 231.33 229 5 5.61E-04 **** 7.90E+OO 0 63.38 6 4 0.32 315.27 311 8 1.77E-03 **** 3.18E+OO 0 74.74 6 0 0.53 371. 80 369 6 1. 7 5E-03 **** 1. 44E+OO 0 78.54 9 3 0.20 390.74 383 11 2.47E-03 .99. 7 1.09E+OO 0 92.69 3 0 0.70 4 61. 22 457 8 9.51E-04 **** 3.57E-01 0 162.02 8 3 0.39 806.47 800 11 2.35E-03 **** 8.37E-04 Flags: "T" = Tentatively associated Page 2568 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:30.94 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l *

Acquisition date 27-SEP-2016 16:19:47 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 9-DEC-2015 10:13:00 Nuclide Library : IODINE *

Sample ID I405235011 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.6100E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2569 of 5809 Le (pCi/GRAM 1.456E+00 NOT IDENT. l.714E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:32.03 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l *

Acquisition date 27-SEP-2016 16:19:47 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *

Sample date 9-DEC-2015 10:13:00 Nuclide Library : IODINE *

Sample ID I405235011 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.6100E+OO GRAM *

Quantity Err(%) 3.8314E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* *

CALIBRATION INFORMATION * * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.152E-01 2.006E+OO I-129 9.429E-02 1.448E-01 Page 2570 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 2.015E+OO l.509E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2571of5809 MDA COUNTS 0. 8133 0.0000 0.8784 3.6923 1.9087 3.0566 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:52.82 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 10-DEC-2015 11:25:00 Acquisition date : 27-SEP-2016 16:20:09 Sample ID I405235012 Sample quantity 2.74000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3,00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2572 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:53.69 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l *

Acquisition date 27-SEP-2016 16:20:09 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 10-DEC-2015 11:25:00 Analyst initials: MJHl * *Sample ID I405235012 Sample Quantity 2.7400E+00 GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.958E+OO 3.614E+OO I-129 1.310E-01 1.608E-01 Page 2573 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.090E+Ol 5.208E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:52.05 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2574 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:53.19 Nuclide Line Activity Report Flag: "*" = Keyline Page 2575 of 5809 Summary of Nuclide Activity Sample ID : I405235012 Acquisition date Page : 2 27-SEP-2016 16:20:09 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2576 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235012 None Flags: "T" Tentatively associated Page 2577 of 5809 Page : 3 Acquisition date 27-SEP-2016 16:20:09 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:55.21 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l *

Acquisition date 27-SEP-2016 16:20:09 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 10-DEC-2015 11:25:00 Nuclide Library : IODINE *

Sample ID I405235012 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7400E+OO GRAM *

Recovery 1. 00000 Carrier Weight : 0. 00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2578 of 5809 Le (pCi/GRAM 4.290E+00 NOT IDENT. l.909E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:56.62 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l *

Acquisition date 27-SEP-2016 16:20:09 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *

Sample date 10-DEC-2015 11:25:00 Nuclide Library : IODINE *

Sample ID I405235012 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7400E+OO GRAM *

Quantity Err(%) 3.6496E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.958E+OO 3. 631E+OO I-129 1.310E-01 1.613E-01 Page 2579 of 5809 TPU (1.96-sigma) TPU (1.96-sigma) 4.046E+OO 1.718E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2580 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 0. 7722 2.3717 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:14.72 ******************************************************************************** *

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235013.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 75-SEP-2016 12:22:59 Sample date 8-DEC-2015 11:23:00. Acquisition date : 28-SEP-2016 06:36:49 Sample ID I405235013 Sample quantity 2.77000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page2581of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:15.62 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235013.CNF;l * *Acquisition date 28-SEP-2016 06:36:49 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 8-DEC-2015 11:23:00 Analyst initials: MJHl * *Sample ID I405235013 Sample Quantity 2.7700E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff: File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.949E+OO 9.129E+OO I-129 4. 713E-02 3.193E-01 Page 2582 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.085E+Ol 7.175E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:13.92 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2583 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:15.10 Nuclide Line Activity Report Flag: "*" = Keyline Page 2584 of 5809 Summary of Nuclide Activity Sample ID : 1405235013 Acquisition date Page : 2 28-SEP-2016 06:36:49 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2585 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235013 None Flags: "T" Tentatively associated Page 2586 of 5809 Acquisition date Page : 3 28-SEP-2016 06:36:49 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:17.47 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * * "

DETECTOR AND SAMPLE' DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235013.CNF;l *

Acquisition date 28-SEP-2016 06:36:49 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 8-DEC-2015 11:23:00 Nuclide Library : IODINE *

Sample ID I405235013 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7700E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : O. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2587 of 5809 Le (pCi/GRAM 8.145E+OO NOT IDENT. 2.780E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:18.62 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235013.CNF;l * *Acquisition date 28-SEP-2016 06:36:49 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 8-DEC-2015 11:23:00 Nuclide Library : IODINE *

Sample ID I405235013 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7700E+OO GRAM *

Quantity Err(%) 3.6101E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.949E+OO 9.136E+OO I-129 4.713E-02 3.193E-01 Page 2588 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 9.178E+OO 3.201E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2589 of 5809 MDA COUNTS 3.1557 3. 2110 2.1618 4.4030 4.4587 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:47.60 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 8-DEC-2015 10:49:00. Acquisition date : 28-SEP-2016 06:45:16 Sample ID I405235014 Sample quantity 2.92000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 14.62 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 13 2 0.34 72.50 69 7 7. 43E-03 31. 8 Flag: "*" = Peak area was modified by background subtraction Page 2590 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:48.45 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * , * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l *

Acquisition date 28-SEP-2016 06:45:16 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 8-DEC-2015 10:49:00 Analyst initials: MJHl *

Sample ID I405235014 Sample Quantity 2.9200E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 3.275E+OO 3.791E+OO I-129 -8.457E-02 2.980E-01 Page2591of5809 MDA (pCi/GRAM MDA (pCi/GRAM l.209E+Ol 5.919E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:46.87 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2592 of 5809 Energy 14.62 Area 13 Bkgnd 2 FWHM Channel 0.34 72.50 Left 69 Pw Cts/Sec %Err 7 7. 43E-03 31. 8 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:47.95 Nuclide Line Activity Report Flag: "*" = Keyline Page 2593 of 5809 Summary of Nuclide Activity Sample ID : 1405235014 Acquisition date Page : 2 28-SEP-2016 06:45:16 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2594 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235014 Page : 3 Acquisition date : 28-SEP-2016 06:45:16 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 14.62 13 2 0.34 72. 50 69 7 7.43E-03 63.6 6.25E-01 Flags: "T" = Tentatively associated Page 2595 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:49.98 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l *

Acquisition date 28-SEP-2016 06:45:16 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 8-DEC-2015 10:49:00 Nuclide Library : IODINE *

Sample ID I405235014 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.9200E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2596 of 5809 Le (pCi/GRAM 4.499E+OO NOT IDENT. 2.097E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:51.11 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l *

Acquisition date 28-SEP-2016 06:45:16 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *

Sample date 8-DEC-2015 10:49:00 Nuclide Library : IODINE *

Sample ID I405235014 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.9200E+OO GRAM *

Quantity Err(%) 3.4247E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.275E+OO 3.834E+OO I-129 -8.457E-02 2.981E-01 Page 2597 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 4.108E+OO 3.005E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2598 of 5809 MDA COUNTS 0.0000 3.3266 1.1221 2.2941 6.9868 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:50.73 ******************************************************************************** *

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23!20 Sample date 8-DEC-2015 10:56:00. Acquisition date : 28-SEP-2016 06:48:23 Sample ID I405235015 Sample quantity 3.13000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K *******************************************'************************************* Pk It 1 0 2 0 Energy 87.30 295.19 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.57 436.00 433 0 0.40 1476.17 1472 6 3.33E-03 40.8 8 3.33E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 2599 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:51.88 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l *

Acquisition date 28-SEP-2016 06:48:23 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 8-DEC-2015 10:56:00 Analyst initials: MJHl *

Sample ID I405235015 Sample Quantity 3.1300E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff.' File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 1.442E+OO 2. 931E+OO I-129 O.OOOE+OO 1. 764E-01 Page 2600 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.116E+Ol 2.438E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:49.84 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 87.30 6 0 0.57 436.00 433 6 3.33E-03 40.8 2 0 295.19 6 0 0.40 1476.17 1472 8 3.33E-03 40.8 Page 2601 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:51.24 Nuclide Line Activity Report Flag: "*" = Keyline Page 2602 of 5809 Summary of Nuclide Activity Sample ID : 1405235015 Acquisition date Page : 2 28-SEP-2016 06:48:23 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2603 of 5809 Keyline not found Manually edited !'M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235015 Acquisition date : 28-SEP-2016 06:48:23 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 87.30 6 0 0.57 436.00 433 6 3.33E-03 81. 6 6.0lE-01 0 295.19 6 0 0.40 1476.17 1472 8 3.33E-03 81. 6 2.29E-06 Flags: "T" = Tentatively associated Page 2604 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:53.71 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l *

Acquisition date 28-SEP-2016 06:48:23 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 8-DEC-2015 10:56:00 Nuclide Library : IODINE *

Sample ID I405235015 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 3.1300E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2605 of 5809 Le (pCi/GRAM 3.479E+OO NOT IDENT. O.OOOE+OO NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:54.91 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l *

Acquisition date 28-SEP-2016 06:48:23 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *

Sample date 8-DEC-2015 10:56:00 Nuclide Library : IODINE *

Sample ID I405235015 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 3.1300E+OO GRAM *

Quantity Err(%) 3.1949E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * * '* Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.442E+OO 2.934E+OO I-129 O.OOOE+OO O.OOOE+OO Page 2606 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.005E+00 O.OOOE+OO NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2607 of 5809 MDA COUNTS 0.0000 0.0000 1.4921 0.0000 0.0000 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:02.09 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 8-DEC-2015 11:29:00. Acquisition date : 28-SEP-2016 06:55:30 Sample ID I405235016 Sample quantity 2.85000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 92.55* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 0 0.55 460.50 456 9 3.73E-03 58.1 Flag: "*" = Peak area was modified by background subtraction Page 2608 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:02.95 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l *

Acquisition date 28-SEP-2016 06:55:30 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 11:29:00 Analyst initials: MJHl *

Sample ID I405235016 Sample Quantity 2.8500E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 4.138E+OO 8.276E+OO I-129 3.359E-02 1.167E-01 Page 2609 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.197E+Ol 5.628E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:01.40 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2610of5809 Energy 92.55 Area 14 Bkgnd FWHM Channel 0 0.55 460.50 Left 456 Pw Cts/Sec %Err 9 7.78E-03 26.7 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:02.47 Nuclide Line Activity Report Flag: "*" = Keyline Page2611of5809 Summary of Nuclide Activity Sample ID : I405235016 Acquisition date Page : 2 28-SEP-2016 06:55:30 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2612of5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235016 Page : 3 Acquisition date : 28-SEP-2016 06:55:30 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.55 7 0 0.55 460.50 456 9 3.73E-03 **** 3.61E-01 Flags: "T" = Tentatively associated Page 2613 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:04.87 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l *

Acquisition date 28-SEP-2016 06:55:30 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 11:29:00 Nuclide Library : IODINE *

Sample ID I405235016 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.8500E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;'5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2614 of 5809 Le (pCi/GRAM 8.477E+OO NOT IDENT. l.385E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:06.07 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l *

Acquisition date 28-SEP-2016 06:55:30 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 11:29:00 Nuclide Library : IODINE *

Sample ID I405235016 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.8500E+OO GRAM *

Quantity Err(%} 3.5088E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : Il29 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 4.138E+OO 8.308E+OO I-129 3.359E-02 1.167E-01 Page 2615 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 8.515E+OO 1.177E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2616of5809 MDA COUNTS 1.6265 0.0000 0.0000 0.9231 0.9543 1.0189 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:55.37 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 2-DEC-2015 10:02:00. Acquisition date : 28-SEP-2016 07:22:16 Sample ID I405235017 Sample quantity 2.33000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 20.58 14 5 1. 35 101.91 95 11 7.51E-03 43.2 2 0 29.78 6 0 0.57 148.00 145 6 3.33E-03 40.8 3 0 34.84 6 0 0.38 173.33 170 6 3.33E-03 40.8 4 0 115. 20 9 0 1. 79 575.67 569 13 5.00E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 2617 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:56.26 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l *

Acquisition date 28-SEP-2016 07:22:16 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 2-DEC-2015 10:02:00 Analyst initials: MJHl *

Sample ID I405235017 Sample Quantity 2.3300E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 4.128E-01 Cnt uncert (1.96-sigma) 3.303E-01 Non-Identified Nuclides Nuclide I-125 Page2618of5809 Key-Line Activity (pCi/GRAM -3.109E+OO K.L. Cnt Uncert (1.96-sigma) 1.290E+Ol MDA (pCi/GRAM 6.757E-01 MDA (pCi/GRAM 2.538E+Ol FAIL ABUN VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:54.64 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 20.58 14 5 1. 35 101.91 95 11 7. 51E-03 43.2 2 .o 29.78 6 0 0. 5.7 148.00 145 6 3.33E-03 40.8 3 0 34.84 6 0 0.38 173.33 170 6 3.33E-03 40.8 4 0 92. 88 7 5 0.65 463.93 457 9 3.98E-03 65.6 5 0 115. 20 9 0 1. 79 575.67 569 13 5.00E-03 33.3 Page 2619of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:55.79 Nuclide Line Activity Report Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 6 56.60* 1.655E+Ol 4.128E-01 4.128E-01 81. 65 33.59 ------10.04 2.487E+Ol ------Line Not Found ------39.58 ------7.51 1.767E+Ol ------Line Not Found ------Flag: "*" Key line Page 2620 of 5809 Summary of Nuclide Activity Sample ID : I405235017 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 07:22:16 Number of lines tentatively identified by NID 4 2 2 50.00% Nuclide Type : FISSION Nuclide I-129 Hlife l.57E+07Y Uncorrected Decay pCi/GRAM 1.00 4.128E-01 Total Activity 4.128E-01 Grand Total Activity 4.128E-01 Flags: "K" "E" Page 2621 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM 4.128E-01 4.128E-01 4.128E-01 Decay Corr 2-Sigma Error 3.370E-01 2-Sigma %Error Flags 81. 65 "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235017 Acquisition date : 28-SEP-2016 07:22:16 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 20.58 14 5 1. 35 101.91 95 11 7.51E-03 86. 4 l.30E-01 0 34.84 6 0 0.38 173.33 170 6 3.33E-03 81. 6 2.52E+Ol T 0 115.20 9 0 1. 79 57 5. 67 569 13 5.00E-03 66.7 5.83E-13 Flags: "T" = Tentatively associated Page 2622 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:57.80 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l * *Acquisition date 28-SEP-2016 07:22:16 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 2-DEC-2015 10:02:00 Nuclide Library : IODINE *

Sample ID I405235017 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.3300E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5'

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 2.417E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2623 of 5809 Le (pCi/GRAM 9.779E+OO FAIL ABUN VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:59.28 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l *

Acquisition date 28-SEP-2016 07:22:16 Sensitivity 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *

Sample date 2-DEC-2015 10:02:00 Nuclide Library : IODINE *

Sample ID I405235017 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.3300E+OO GRAM *

Quantity Err(%) 4.2918E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 4.128E-01 Act Error ( 1. 96-sigma) 3.327E-01 Non-Identified Nuclides Nuclide I-125 Page 2624 of 5809 Key-Line Activity (pCi/GRAM -3.109E+OO K.L Act error ( 1. 96-sigma) 1. 291E+Ol TPU ( 1. 96-sigma) 3.327E-01 TPU ( 1. 96-sigma) l.298E+Ol FAIL ABUN

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2625 of 5809 MDA COUNTS 5.2595 2.1407 1.6213 0.0000 1. 6720 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:07.51 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Configuration Background file Background date : 25-SEP-2016 12:23:10 Sample date 2-DEC-2015 10:19:00. Acquisition date : 28-SEP-2016 07:22:56 Sample ID I405235018 Sample quantity 2.76000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.08 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 10 .11* BACKGROUND CORRECTED SAMPLE PEAK*REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 1 0.58 49.91 48 5 3.22E-03 60.7 Flag: "*" = Peak area was modified by background subtraction Page 2626 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:08.33 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l *

Acquisition date 28-SEP-2016 07:22:56 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *

Sample date 2-DEC-2015 10:19:00 Analyst initials: MJHl * *Sample ID I405235018 Sample Quantity 2.7600E+00 GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.773E+OO 4.336E+OO I-129 -2.368E-01 3.781E-01 Page 2627 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.380E+Ol 6.299E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:06.62 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2628 of 5809 Energy 10 .11 Area 9 Bkgnd 1 FWHM Channel 0.58 49.91 Left 48 Pw Cts/Sec %Err 5 5.06E-03 37.4 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:07.84 Nuclide Line Activity Report Flag: "*" = Keyline Page 2629 of 5809 Summary of Nuclide Activity Sample ID : 1405235018 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 07:22:56 Number of lines tentatively identified by **** There are no nuclides meeting summary 1 1 NID 0 criteria 0.00% **** .Flags: "K" "E" Page 2630 of 5809 Keyline not found Manually edited "M" Manually accepted "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235018 Page : 3 Acquisition date : 28-SEP-2016 07:22:56 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 10 .11 6 1 0.58 49.91 48 5 3.22E-03 **** l.65E-02 Flags: "T" = Tentatively associated Page 2631 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:09.89 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l *

Acquisition date 28-SEP-2016 07:22:56 Sensitivity 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *

Sample date 2-DEC-2015 10:19:00 Nuclide Library : IODINE *

Sample ID I405235018 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.7600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 * *' Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2632 of 5809 Le (pCi/GRAM 5.146E+00 NOT IDENT. 2.237E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:11.00 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l *

Acquisition date 28-SEP-2016 07:22:56 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *

Sample date 2-DEC-2015 10:19:00 Nuclide Library : IODINE *

Sample ID I405235018 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7600E+OO GRAM *

Quantity Err ( % ) 3. 6232E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 3.773E+OO 4.386E+OO I-129 -2.368E-01 3.788E-01 Page 2633 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 4.704E+OO 3.936E-01 NOT IDENT. NOT IDENT.
* * *

GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2634 of 5809 MDA COUNTS 0.0000 5.5444 1.1221 2.2941 0.0000 1.2005 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:32.95 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 8-DEC-2015 14:30:00. Acquisition date : 28-SEP-2016 07:23:18 Sample ID I405235019 Sample quantity 2.56000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2635 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:33.74 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l *

Acquisition date 28-SEP-2016 07:23:18 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 14:30:00 Analyst initials: MJHl *

Sample ID I405235019 Sample Quantity 2.5600E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

Eff. File' : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 3. 711E+00 I-129 1.518E-01 2.533E-01 Page 2636 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.131E+OO 8.990E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:32.19 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2637 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:33.28 Nuclide Line Activity Report Flag: "*" = Key line Page 2638 of 5809 Summary of Nuclide Activity Sample ID : I405235019 Acquisition date Page : 2 28-SEP-2016 07:23:18 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2639 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235019 None Flags: "T" Tentatively associated Page 2640 of 5809 Acquisition date Page : 3 28-SEP-2016 07:23:18 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:35.35 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l *

Acquisition date 28-SEP-2016 07:23:18 Sensitivity : 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 14:30:00 Nuclide Library : IODINE *

Sample ID I405235019 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.5600E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *

E'ff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2641of5809 Le (pCi/GRAM 0.000E+OO NOT IDENT. 3.006E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:36.46 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l *

Acquisition date 28-SEP-2016 07:23:18 Sensitivity 3.000 *

Detector ID XRAY6 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 14:30:00 Nuclide Library : IODINE *

Sample ID I405235019 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.5600E+OO GRAM *

Quantity Err(%) 3.9063E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 26-JAN-2016 10: 07: 09 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 O.OOOE+OO O.OOOE+OO I-129 1.518E-01 2.537E-01 Page 2642 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) O.OOOE+OO 2.628E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29.62 35.49 39.58 Page 2643 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 1.5445 0.7906 2.4852 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:57.75 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 8-DEC-2015 13:50:00. Acquisition date : 28-SEP-2016 07:27:31 Sample ID I405235020 Sample quantity 2.97000E+OO GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.22* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 10 0 0.63 314.46 310 10 5.38E-03 38.1 Flag: "*" = Peak area was modified by background subtraction Page 2644 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:58.58 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l * *Acquisition date 28-SEP-2016 07:27:31 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 13:50:00 Analyst initials: MJHl *

Sample ID I405235020 Sample Quantity 2.9700E+00 GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.322E-01 4.494E+OO I-129 5.711E-02 2.909E-01 Page 2645 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 309E+Ol 8.351E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:57.03 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2646 of 5809 Energy 63.22 Area 13 Bkgnd FWHM Channel 0 0.63 314.46 Left 310 Pw Cts/Sec %Err 10 7.22E-03 27.7 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:58.13 Nuclide Line Activity Report Flag: "*" = Keyline Page 2647 of 5809 Summary of Nuclide Activity Sample ID : I405235020 Acquisition date Page : 2 28-SEP-2016 07:27:31 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2648 of 5809 Keyline not. found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235020 Page : 3 Acquisition date : 28-SEP-2016 07:27:31 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 63.22 10 0 0.63 314.46 310 10 5.38E-03 76.2 3.22E+OO Flags: "T" = Tentatively associated Page 2649 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:58:00.07 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l *

Acquisition date 28-SEP-2016 07:27:31 Sensitivity 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 13:50:00 Nuclide Library : IODINE *

Sample ID I405235020 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.9700E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2650 of 5809 Le (pCi/GRAM 4.138E+00 NOT IDENT. 2.805E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:58:01.14 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l *

Acquisition date 28-SEP-2016 07:27:31 Sensitivity : 3.000 *

Detector ID XRAY5 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *

Sample date 8-DEC-2015 13:50:00 Nuclide Library : IODINE *

Sample ID I405235020 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.9700E+00 GRAM *

Quantity Err(%) 3.3670E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYS I129.CNF;5

Combined Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1 . 96-sigma) I-125 3.322E-01 4.494E+OO I-129 5. 711E-02 2.910E-01 Page 2651of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.497E+OO 2.921E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2652 of 5809 MDA COUNTS 0.8133 0.8547 0.0000 0.0000 1.9087 2.0378 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:57.73 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627430.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : Z5-SEP-2016 12:22:54 Sample date 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 07:39:35 Sample ID I1203627430 Sample quantity 3.34000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2653 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:58.68 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627430.CNF;l *

Acquisition date 28-SEP-2016 07:39:35 Sensitivity : 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *

Sample ID I1203627430 Sample Quantity 3.3400E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7. 411E-02 1.016E-01 I-129 -1.098E-02 1. 731E-01 Page 2654 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.473E-01 3.935E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:56.96 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2655 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:58.17 Nuclide Line Activity Report Flag: "*" = Keyline Page 2656 of 5809 Summary of Nuclide Activity Sample ID : 11203627430 Acquisition date Page : 2 28-SEP-2016 07:39:35 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2657 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627430 None Flags: "T" Tentatively associated Page 2658 of 5809 Acquisition date Page : 3 28-SEP-2016 07:39:35 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:10:00.55 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627430.CNF;l *

Acquisition date 28-SEP-2016 07:39:35 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: O 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627430 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 3.3400E+OO GRAM *

Recovery 1. 00000 Carrier Weight : 0. 00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2659 of 5809 Le (pCi/GRAM 4.734E-02 NOT IDENT. l.478E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:10:02.01 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627430.CNF;l *

Acquisition date 28-SEP-2016 07:39:35 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627430 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 3.3400E+OO GRAM *

Quantity Err(%) 2.9940E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7. 411E-02 1.025E-01 I-129 -l.098E-02 1. 731E-01 Page 2660 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) l.078E-01 1.732E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2661 of 5809 MDA COUNTS 4.9062 3.3927 1. 7312 0.8985 0.9215 3.8759 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:26.86 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627431.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 10-DEC-2015 14:20:00 Acquisition date : 28-SEP-2016 08:03:53 Sample ID I1203627431 Sample quantity 2.50000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.08 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 16.37* 61. 41 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 10 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.58 80.86 4 0.29 306.33 76 300 11 5.78E-03 61.0 8 2.78E-03 82.5 Flag: "*" = Peak area was modified by background subtraction Page 2662 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:27.66 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627431.CNF;l * *Acquisition date 28-SEP-2016 08:03:53 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *

Sample date 10-DEC-2015 14:20:00 Analyst initials: MJHl *

Sample ID I1203627431 Sample Quantity 2.5000E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA:GAMMA]EFF XRAY2 I129.CNF;15 * ***********************************************T*****T************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 1.190E+OO 9.544E+OO I-129 8.699E-02 3.661E-01 Page 2663 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.149E+Ol 8.341E-01 NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:26.16 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2664 of 5809 Energy 16.37 61. 41 Area 18 . 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.58 80.86 4 0.29 306.33 76 11 9.72E-03 35.3 300 8 82.5 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:27.22 Nuclide Line Activity Report Flag: "*" = Keyline Page 2665 of 5809 Summary of Nuclide Activity Sample ID : 11203627431 Acquisition date Page : 2 28-SEP-2016 08:03:53 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2666 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627431 Page : 3 Acquisition date : 28-SEP-2016 08:03:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 16.37 61. 41 10 5 6 0.58 4 0.29 Flags: "T" = Tentatively associated Page 2667 of 5809 80.86 76 11 5.78E-03 **** 3.43E-04 306.33 300 8 2.78E-03 **** 3.66E-02 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:29.53 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA *

* *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627431.CNF;l *

Acquisition date 28-SEP-2016 08:03:53 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *

Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *

Sample ID I1203627431 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.5000E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. 'File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2668 of 5809 Le (pCi/GRAM 8.280E+00 NOT IDENT. 3.276E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:30.88 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * *

DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627431.CNF;l * *Acquisition date 28-SEP-2016 08:03:53 Sensitivity : 3.000 *

Detector ID XRAY2 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *

Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *

Sample ID I1203627431 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.5000E+OO GRAM *

Quantity Err(%) 4. OOOOE-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *

Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.190E+OO 9.546E+OO I-129 8.699E-02 3.662E-01 Page 2669 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 9.561E+OO 3.683E-01 NOT IDENT. NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2670 of 5809 MDA COUNTS 3.1557 3. 2110 3.2426 4.4030 7.8027 5.7170 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:51.76 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627432.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 75-SEP-2016 12:23:10 Sample date 10-DEC-2015 14:20:00 Acquisition date : 28-SEP-2016 08:04:20 Sample ID I1203627432 Sample quantity : 2.56000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT

Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.82* 9 7 0.57 83.56 78 10 4*. 98E-03 70.8 2 4 28.53 12 7 0.48 142.22 131 24 6.47E-03 52.3 1.13E+OO 3 4 29.68 179 7 0.65 147.98 131 24 9.95E-02 8.5 4 6 33.43 38 0 0.81 166.76 164 12 2. llE-02 17.3 3.06E+OO 5 6 34.39 25 0 0.69 171.59 164 12 l.42E-02 30.7 6 0 39.62 24 2 0.29 197.79 194 8 1.33E-02 22.9 Flag: "*" = Peak area was modified by background subtraction Page 2671of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:52.73 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627432.CNF;l *

Acquisition date 28-SEP-2016 08:04:20 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : 8.000 *

Sample date 10-DEC-2015 14:20:00 Analyst initials: MJHl *

Sample ID Il203627432 Sample Quantity 2.5600E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 1. 2 98E+Ol Cnt uncert ( 1. 96-sigma) 2.163E+OO Non-Identified Nuclides Nuclide I-125 Page 2672 of 5809 Key-Line Activity (pCi/GRAM 1.537E+Ol K.L. Cnt Uncert ( 1. 96-sigma) 1.206E+Ol MDA (pCi/GRAM 9.931E-01 MDA (pCi/GRAM 2.819E+Ol NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:50.97 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.82 13 7 0.57 83.56 78 10 6.97E-03 49.6 2 4 28.53 12 7 0.48 142.22 131 24 6.47E-03 5.2. 3 1.13E+OO 3 4 29.68 179 7 0.65 147.98 131 24 9.95E-02 8.5 4 6 33.43 38 0 0.81 166.76 164 12 2. llE-02 17.3 3.06E+OO 5 6 34.39 25 0 0.69 171.59 164 12 l.42E-02 30.7 6 0 39.62 24 2 0.29 197.79 194 8 1. 33E-02 22.9 Page 2673 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:52.17 Nuclide Line Activity Report Nuclide Type: FISSION Uncorrected Decay Corr 1-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 179 56.60* 1.430E+Ol l.298E+Ol 1. 298E+Ol 8.50 33.59 38 10.04 1.621E+Ol 1.369E+Ol 1.369E+Ol 17. 26 39.58 24 7.51 1.618E+Ol l.153E+Ol 1.153E+Ol 22.93 Flag: "*" Key line Page 2674 of 5809 Summary of Nuclide Activity Sample ID : Il203627432 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 08:04:20 Number of lines tentatively identified by NID 6 3 3 50.00% Nuclide Type : FISSION Nuclide I-129 Hlife 1.57E+07Y Uncorrected Decay pCi/GRAM 1. 00 1. 298E+Ol Total Activity 1. 298E+Ol Grand Total Activity 1.298E+Ol Flags: "K" "E" Page 2675 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM 1.298E+Ol l.298E+Ol 1.298E+Ol Decay Corr 1-Sigma Error 0. llOE+Ol Manually accepted 1-Sigma %Error Flags 8.50 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 11203627432 Acquisition date : 28-SEP-2016 08:04:20 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.82 9 7 0.57 83.56 78 10 4.98E-03 70.8 1. 67E+00 4 28.53 12 7 0.48 142.22 131 24 6.47E-03 52.3 1.34E+Ol 6 34.39 25 0 0.69 171.59 164 12 1.42E-02 30.7 1. 65E+Ol Flags: "T" = Tentatively associated Page 2676 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:54.52 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627432.CNF;l * *Acquisition date 28-SEP-2016 08:04:20 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : 8.000 *

Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *

Sample ID I1203627432 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 2.5600E+00 GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * * *

CALIBRATION INFORMATION * *

Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 3.983E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2677 of 5809 Le (pCi/GRAM 1.238E+Ol NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:55.74 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627432.CNF;l *

Acquisition date 28-SEP-2016 08:04:20 Sensitivity : 3.000 *

Detector ID XRAY4 Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.10 Half life ratio : 8.000 *

Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *

Sample ID I1203627432 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 2.5600E+OO GRAM *

Quantity Err(%) 3.9063E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0.00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal: date 17-JUN-2016 08:18:14 Eff. Geometiy : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1.298E+Ol Act Error (1.96-sigma) 2.517E+OO Non-Identified Nuclides Nuclide I-125 Page2678of5809 Key-Line Activity (pCi/GRAM 1.537E+Ol K.L Act error (1.96-sigma) 1.235E+Ol TPU (1.96-sigma) 2.517E+OO TPU (1.96-sigma) l.416E+Ol NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2679 of 5809 MDA COUNTS 5.4288 5.5444 5.0495 3. 4411 6.9868 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:37.28 ********************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627433.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 08:11:05 Sample ID I1203627433 Sample quantity 3.34000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.75 291 33 0.60 149.23 145 12 1.62E-01 7.3 2 0 33.71 90 3 0.48 169.18 164 12 4.98E-02 11. 3 3 0 39.54 49 0 0.80 198.55 193 13 2.72E-02 14.3 Flag: "*" = Peak area was modified by background subtraction Page 2680 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:38.20 *******************************************************************************

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627433.CNF;l *

Acquisition date 28-SEP-2016 08:11:05 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *

Sample ID I1203627433 Sample Quantity 3.3400E+OO GRAM *

Batch Number 1598618 Carrier Weight 0.00000 *

Recovery 1.00000 Standard Weight 0.00000 *

Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File ': DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 1. 051E+Ol Cnt uncert (1.96-sigma) 1.500E+OO Non-Identified Nuclides Nuclide I-125 Page 2681 of 5 809 Key-Line Activity (pCi/GRAM -5.238E-02 K.L. Cnt Uncert (1. 96-sigma) 3.087E-01 MDA (pCi/GRAM 9.173E-01 MDA (pCi/GRAM 5.310E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:36.48 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.75 291 33 0.60 149.23 145 12 1. 62E-01 7.3 2. 0 33.71 90 3 0.48 169.18. 164 12 4.98E-02 11. 3 3 0 39.54 49 0 0.80 198.55 193 13 2.72E-02 14.3 Page 2682 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:37.74 Nuclide Line Activity Report Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 291 56.60* 2.202E+Ol 1.051E+Ol 1. 051E+Ol 14.56 33.59 90 10.04 2.304E+Ol 1.741E+Ol 1.741E+Ol 22.54 39.58 49 7.51 2.289E+Ol 1.281E+Ol 1.281E+Ol 28.57 Flag: "*" Key line Page 2683 of 5809 Summary of Nuclide Activity Sample ID : I1203627433 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 08:11:05 Number of lines tentatively identified by NID 3 0 3 100.00% Nuclide Type : FISSION Nuclide I-129 Hlife l.57E+07Y Uncorrected Decay pCi/GRAM 1.00 1.051E+Ol Total Activity 1.051E+Ol Grand Total Activity 1. 051E+Ol Flags: "K" "E" Page 2684 of 5809 Keyline not found Manually edited Decay Corr pCi/GRAM 1. 051E+Ol 1.051E+Ol 1. 051E+Ol Decay Corr 2-Sigma Error 0.153E+Ol 2-Sigma %Error Flags 14.56 "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627433 None Flags: "T" Tentatively associated Page 2685 of 5809 Acquisition date Page : 3 28-SEP-2016 08:11:05 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:39.73 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* *

DETECTOR AND SAMPLE DATA * * * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627433.CNF;l * *Acquisition date 28-SEP-2016 08:11:05 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627433 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity : 3.3400E+OO GRAM *

Recovery 1.00000 Carrier Weight : 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 4.099E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2686 of 5809 Le (pCi/GRAM 2.393E-01 NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:40.79 *******************************************************************************
GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 * ******************************************************************************* * * *

DETECTOR AND SAMPLE DATA * *

Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627433.CNF;l * *Acquisition date 28-SEP-2016 08:11:05 Sensitivity 3.000 *

Detector ID XRAYl Energy tolerance: 1.000 *

Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *

Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *

Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *

Sample ID I1203627433 Analyst initials: MJHl *

Batch Number 1598618 Sample Quantity 3.3400E+00 GRAM *

Quantity Err(%) 2.9940E-03 % *

Recovery 1.00000 Carrier Weight 0.00000 *

Standard Weight : 0. 00000 * ******************************************************************************* * *

CALIBRATION INFORMATION * * *

Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry* : I129 *

Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6

Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1.051E+Ol Act Error ( 1. 96-sigrna) 1.820E+OO Non-Identified Nuclides Nuclide I-125 Page 2687 of 5809 Key-Line Activity (pCi/GRAM -5.238E-02 K.L Act error ( 1. 96-sigrna) 3.089E-01 TPU ( 1. 96-sigrna) 1.820E+OO TPU ( 1. 96-sigrna) 3.098E-01 NOT IDENT.

GEL Laboratories LLC *

2040 Savage Road *

Charleston, SC 29407 *

GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2688 of 5809 MDA COUNTS 30.6637 23.7490 10.3875 8.0864 9.6757 3.8759 ENERGY MDA COUNTS ENERGY MDA COUNTS Effective 3/25/201 O Revision 1 Effective March 201 O Radiochemistry Batch Checklist 09/29/16 Batch#_1_5_9_8_6_2_0 __ _ Product: 1-129 I MJWC Date: 09/29/16 Criteria: ., Yes No Comments Sample Solids are less than or eoual to 100 mo for GAB. n/a Samples have been blank corrected (If required). Blank correction rooortod Included tlf renulredl. n/a If activity less than 10x MDA/MDC, error Is loss than or equal to 1500/o of sample activity. ../' If greater than 10* MDA/ MDC, error Is 40% or less. [f below the MDAI MDC error Is okav. !Instrument source check Is within limits. bl..n rhACk '"within limit ... ../' Method RDL/ LLD has been met. ../' If duplicate activities are: Less than 5* MDA/ MDC, then RPD Is 100% or less, lf greater 5* MDA/ MDC, then RPO 20% or less, ../' [f below the MOA/ MDC, the RPO Is 0%, Or meets the client's reouired RER acceptance criteria. Tracer yield is 15-1250/o

Carrier yield 25-1250/o. (Or meets the client's contract acceptance criteria). In Method blank Is less than the RDL/ LLD. ,/ Inf __ .. ----*--_, !;D/o nf *-u*nb* ** 1 .. ,\ Sample was run within hold time. I DER 1562566 Samole was correctlv oreserved If reoulred. ../' Smears Taken for Radioactive batches. n/a Method Spike and LCS are within 75-1250/o Ir nr --ets the -*'s contract e criteria\. ../' No blank spaces on data forms. ../' All line outs Initiated and dated. trnOli,Cil!tl!Hl.!"----. Aux data Is correct. ../' Client Sneclal renulrements naae has been checked. ../' Raw Data and / or snectrum are Included and nronerlv statused. ./' MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and ../' **-tuna ve*ifln.I .... --. (If _/ Batch entered ./ Batch Data Excentlon Reoorts (DERl comoleted If annlicable. / DER 1562566 Batch Data Exception Reports (DER) second reviewed * / .Qk;11osltlon verified to be comnleted. ./ "1'l7"""""<i 9/it/,1. 1.a.nnuot Cnrrnctinn com-*e*-"' If r"nulred. I Review sample historical results If avallable ../' (If REMP, results above MDC have been verifled bv historical results recount or re-analvsls. l Primary Rovlow Performed By: Q0-4 /2--Cf. (\.b secondary Revlow Performed Page 2689 of 5809 ' GL-CHL-RAD-013Rev1 Page 1 of 1}}

ML17009A183

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