{{Adams | number = ML16364A246 | issue date = 12/14/2016 | title = Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey, Rev. 1, Appendix G: Data Validation Report 405235, Part 1 of 2 | author name = | author affiliation = State of NY, Energy Research & Development Authority | addressee name = | addressee affiliation = NRC/NMSS, NRC/NRR | docket = 05000201, P00M-032 | license number = | contact person = | package number = ML17006A156 | document type = Environmental Monitoring Report | page count = 1955 }}

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{{#Wiki_filter:1-----------------------------------------------------------------------------------___ ,_ -----------------------------------1 I I I ! I . I I Data Validation Report 405235 , I I L __ -----------------------------------------------------------------_________ _J VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:21.90 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 9-DEC-2015 14:00:00. Acquisition date : 27-SEP-2016 12:27:59 Sample ID .I405235004 Sample quantity 2.52000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND*CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd. FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 63.36* 4 0 0.47 316.22 313 7 1. OOE-03 89.9 2 0 81.17* 5 2 0.38 405.30 402 7 1. 32E-03 74.3 Flag: "*" = Peak area was modified by background subtraction Page 2500 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:22.80 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA' * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l *
Acquisition date 27-SEP-2016 12:27:59 Sensitivity : 3.000 *
Detector ID XRAY6 Energy toler*ance: 1. 000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
Sample date 9-DEC-2015 14:00:00 Analyst initials: MJHl *
Sample ID I405235004 Sample Quantity 2.5200E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1; 96-sigma) "I-125 -1. 726E+OO 4.133E+OO I-129 2.594E-02 2.210E-01 Page 2501of5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.935E+00 5.123E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:21.16 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 63.36 9 0 0.47 316.22 313 7 2.50E-03 33.3 2 0 81.17 7 2 0.38 405 .. 30 402 7 l.98E-03 48.8 Page 2502 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:22.26 Nuclide Line Activity Report Flag: "*" Key line Page 2503 of 5809 Summary of Nuclide Activity Sample ID : 1405235004 Acquisition date Page : 2 27-SEP-2016 12:27:59 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2504 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235004 Page : 3 Acquisition date : 27-SEP-2016 12:27:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 63.36 81.17 4 5 0 0.47 2 0.38 Flags: "T" = Tentatively associated Page 2505 of 5809 316.22 313 7 1.00E-03 **** 3.07E+OO 405.30 402 7 l.32E-03 **** 9.25E-01 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:24.41 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l *
Acquisition date 27-SEP-2016 12:27:59 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
date 9-DEC-2015 14:00:00 Nuclide Library : IODINE *
Sample ID I405235004 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.5200E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date : 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 If29.CNF;5 '
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2506 of 5809 Le (pCi/GRAM 2.192E+00 NOT IDENT. l.805E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 13:29:25.55 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235004.CNF;l *
Acquisition date 27-SEP-2016 12:27:59 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
Sample date 9-DEC-2015 14:00:00 Nuclide Library : IODINE *
Sample ID I405235004 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.5200E+OO GRAM *
Quantity Err(%) 3.9683E--:03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1. 726E+OO 4.136E+OO I-129 2.594E-02 2.210E-01 Page 2507 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.208E+OO 2.213E-01 NOT IDENT. NOT IDENT.
- - - - t*************************************** * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * *
******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2508 of 5809 MDA COUNTS 2.8315 1.4643 1.4921 0.0000 1. 5811 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:01.35 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 10-DEC-2015 13:15:00 Acquisition date : 27-SEP-2016 15:11:29 Sample ID I405235005 Sample quantity 2.73000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 44.78 BACKGROUND C.GRRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0 0.29 223.67 220 6 3.33E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 2509 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:02.44 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l *
Acquisition date 27-SEP-2016 15:11:29 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 10-DEC-2015 13:15:00 Analyst initials: MJHl * *Sample ID I405235005 Sample Quantity 2.7300E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified *Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 -1.488E+OO 5.457E+OO I-129 1.289E-01 2.748E-01 Page 2510of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.099E+Ol 7.339E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:00.22 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2511 of 5809 Energy 44.78 Area 6 Bkgnd FWHM Channel 0 0.29 223.67 Left 220 Pw Cts/Sec %Err 6 3.33E-03 40.8 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:01.84 Nuclide Line Activity Report Flag: "*" = Keyline Page 2512 of 5809 Summary of Nuclide Activity Sample ID : 1405235005 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 27-SEP-2016 15:11:29 Number of lines tentatively identified by **** There are no nuclides meeting summary 1 1 NID 0 criteria 0.00% **** Flags: "K" "E" Page 2513of5809 Keyline not found Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235005 Page : 3 Acquisition date : 27-SEP-2016 15:11:29 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 44.78 6 0 0.29 223.67 220 6 3.33E-03 81.6 1.41E+Ol Flags: "T" = Tentatively associated Page 2514of5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:42:04.03 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l *
Acquisition date 27-SEP-2016 15:11:29 Sensitivity . : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 10-DEC-2015 13:15:00 Nuclide Library : IODINE *
Sample ID I405235005 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7300E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Anal¥sis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2515of5809 Le (pCi/GRAM 3.893E+OO 2.747E-01 NOT* "IDENT. NOT IDENT.

VAX/VMS Nuclide Identf;Eication Report Generated 27-SEP-2016 15:42:05.13_ *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235005.CNF;l *
Acquisition date 27-SEP-2016 15:11:29 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 10-DEC-2015 13:15:00 Nuclide Library : IODINE *
Sample ID I405235005 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7300E+OO GRAM *
Quantity Err(%) 3.6630E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date : 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File :*DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer tb Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -1.488E+OO 5.463E+OO I-129 l.289E-01 2. 751E-01 Pag.e 2516of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.504E+OO 2.812E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2517 of5809 MDA COUNTS 3.2573 1.1089 2.2442 1.1470 0.0000 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:13.53 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 . Background date : 25-SEP-2016 12:23:15 Sample date 10-DEC-2015 13:25:00 Acquisition date : 27-SEP-2016 15:11:52 Sample ID I405235006 Sample quantity 2.78000E+OO GRAM Detector name : XRAY5 . Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.02 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk* It 1 0 Energy 131.03 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 0 0.55 652.14 645 12 3.89E-03 37.8 Flag: "*" = Peak area was modified by background subtraction Page 2518of5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:14.33 *****************'**************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l *
Acquisition date 27-SEP-2016 15:11:52 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00: 30: 00. 02 Half life ratio : ***** *
Sample date 10-DEC-2015 13:25:00 Analyst initials: MJHl * *Sample ID I405235006 Sample Quantity 2.7800E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I-129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5 '* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. * ----Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.842E+OO 3.611E+OO I-129 4.326E-01 4.240E-01 Page 2519of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.356E+Ol 1.299E+OO NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:12.79 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2520 of 5809 Energy 131. 03 Area 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.55 652.14 645 12 3.89E-03 37.8 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:13.87 Nuclide Line Activity Report Flag: "*" = Keyline Page 2521 of 5809 Page : 2 Summary of Nuclide Activity Sample ID : 1405235006 Acquisition date 27-SEP-2016 15:11:52 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2522 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235006 Page : 3 Acquisition date : 27-SEP-2016 15:11:52 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 131. 03 7 0 0.55 652.14 645 12 3.89E-03 75.6 l.35E-02 Flags: "T" = Tentatively associated Page 2523 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:16.31 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CAWBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l *
Acquisitiqn date 27-SEP-2016 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
Sample date 13:25:00 Nuclide Library : IODINE *
Sample ID I405235006 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7800E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5 .
Combined Critical Level Report 'NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide -I-125 I-129 Page 2524 of 5809 Le (pCi/GRAM 4.286E+OO NOT IDENT. 5.032E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:17.50 ******************'*************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *'Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235006.CNF;l *
Acquisition date 277SEP-2016 15:11:52 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 **
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
Sample date 10-DEC-2015 13: 25: 00 Nuclide Libra*ry : IODINE *
Sample ID I405235006 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7800E+00 GRAM *
Quantity Err(%) 3.5971E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * * ** Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error .Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.842E+OO 3.625E+OO I-129 4.326E-01 4.262E-01 Page 2525 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 3.719E+00 4.687E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2526 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 0.9231 0.9543 0.0000 ENERGY MDA COUNTS ENERGY ' MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:38.92 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l Background file DKAlOO: [CANBERRA,GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 10-DEC-2015 13:55:00 Acquisition date : 27-SEP-2016 15:12:14 Sample ID I405235007 Sample quantity GRAM Detector name : XRAY6 Detector I129 Elapsed liye 0 00:30:00.00 Elapsed teal time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch In 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2527 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:39.74 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * *-* *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I4Q5235007.CNF;l * *Acquisition date 27-SEP-2016 15:12:14 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed *live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 10-DEC-2015 13:55:00 Analyst initials: MJHl *
Sample ID I405235007 Sample Quantity 2.6000E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff .. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.559E+OO 5.015E+OO I-129 -2.761E-01 4.587E-01 -Page 2528 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.898E+OO 6.039E-01 NOT IDENT. NOT I.DENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:38.06 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2529 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:39.28 Nuclide Line Activity Report Flag: "*" = Keyline \. Page 2530 of 5809 Summary of Nuclide Activity Sample ID : 1405235007 Acquisition date Page : 2 27-SEP-2016 15:12:14 **** There are no nuclides meeting summary criteria **** Flags: "K" Keyline not found "E" = Manually edited Page 2531 of 5809 "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235007 None Flags: "T" Tentatively associated Page 2532 of 5809 Acquisition date Page : 3 27-SEP-2016 15:12:14 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:41.27 ******************.*************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA ** * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l *
Acquisition date 27-SEP-2016 15:12:14 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 10-DEC-2015 13:55:00 Nuclide Library : IODINE *
Sample ID I405235007 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.6000E+00 GRAM *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
Eff: File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2533 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. l.553E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 15:43:42.27 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************.************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235007.CNF;l *
Acquisition date 27-SEP-2016 15:12:14 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00: 30: 00. 04 Half life ratio : ***** *
Sample date 10-DEC-2015 13:55:00 Nuclide Library : IODINE *
Sample ID I405235007 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.6000E+OO GRAM *
Quantity Err(%) 3.8462E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.559E+OO 5.020E+OO I-129 -2. 761E-01 4.595E-01 Page 2534 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5 .151E+OO 4. 761E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2535 of 5809 MDA COUNTS 1. 4157 2.9286 0.0000 0.0000 1.5811 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:39.41 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 10-DEC-2015 14:05:00 Acquisition date : 27-SEP-2016 16:19:05 Sample ID I405235008 Sample quantity 2.58000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.23 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrii Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 72 .29 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 11 0 0.63 363.64 360 8 3.06E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 2536 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:40.21 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * '******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l *
Acquisition date 27-SEP-2016 16:19:05 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.23 Half life ratio : ***** * .*Sample date 10-DEC-2015 14:05:00 Analyst i_nitials: MJHl *
Sample ID I405235008 Sample Quantity 2.5800E+00 GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * **
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.'CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-I9entified Nuclides Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 2.033E+OO 3.175E+OO I-129 -1.212E-01 1.964E-01 Page 2537of5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.873E+OO 3.623E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:38.71 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Energy 72. 29 Page 2538 of 5809

Area 11 Bkgnd FWHM Channel 0 0.63 363.64 Left 360 Pw Cts/Sec %Err 8 3.06E-03 30.2 Fit VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17.:19:39.76 Nuclide Line Activity Report Flag: "*" Key line Page 2539 of 5809 Summary of Nuclide Activity Sample ID : I405235008 Acquisition date Page : 2 27-SEP-2016 16:19:05 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2540 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235008 Acquisition date Page : 3 27-SEP-2016 16:19:05 It Energy 72. 29 Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 11 0 0.63 363.64 360 8 3.06E-03 60.3 1.13E+Ol Flags: "T" = Tentatively associated Page 2541of5809 VAX/VMS Nuclide Identification Report _Generated 27-SEP-2016 17:19:41.88 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l *
Acquisition 27-SEP-2016 16:19:05 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.23 Half life ratio : ***** *
Sample date 14:05:00 Nuclide Library : IODINE *
Sample ID I405235008 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.5800E+00 GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * . * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKAlOO:'[CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Critical Level Re.port NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2542 of 5809 Le (pCi/GRAM 2.937E+OO NOT IDENT. l.495E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:43.00

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235008.CNF;l *
Acquisition date 27-SEP-2016 16:19:05 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.23 Half life ratio : ***** *
Sample date 10-DEC-2015 14:05:00 Nuclide Library : IODINE *
Sample ID . I405235008 Analyst .initials: MJHl *
Batch Number 1598618 Sample Quantity 2.5800E+OO GRAM *
Quantity Err(%) 3.8760E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************** * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 2.033E+OO 3.195E+OO I-129 -1.212E-01 1.968E-01 Page 2543 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 3. 324E+oo* 2.042E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2544 of 5809 MDA COUNTS 6.1327 12.7227 5.1937 8.9849 6.4505 6.7829 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:13.31 ************************************************************t*******************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 2"5-SEP-2016 12: 22 :.59' Sample date 10-DEC-2015 10:30:00 Acquisition date : 27-SEP-2016 16:18:41 Sample ID I405235009 Sample quantity 2.63000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.20 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.81* 7 14 0.43 83.03 77 11 2.0lE-03124.4 2 0 36.66 7 0 0.55 182.43 177 9 1..94E-03 37.8 3 0 41. 39 9 3 1. 36 206.11 200 10 2.62E-03 45.4 4 0 57.90 12 0 0.25 288.75 283 11 3.33E-03 28.9 5 0 63.05* 6 2 0.61 314.55 310 9 l.58E-03 82.0 6 0 64.67 6 2 0.45 322.66 319 7 1. 74E-03 53.2 7 2 70.09 12 1 0. 96 349.79 346 13 3.39E-03 34.7 4.21E-01 8 2 71. 29 12 2 0.65 355.82 346 13 3.26E-03 32.1 9 0 93.00* 6 7 1. 31 464.51 456 14 1. 71E-03126. 9 10 0 134. 56 9 2 0.28 672. 65 668 9 2.44E-03 45.7 11 0 182 .13 11 6 0.42 910.91 904 12 3.06E-03 53.8 Flag: "*" = Peak area was modified by background subtraction Page 2545 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:14.37 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l *
Acquisition date 27-SEP-2016 16:18:41 Sensitivity 3.000 *
Detector ID XRAY2 . Energy tolerance: 1. 000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
Sample date 10-DEC-2015 10:30:00 Analyst initials: MJHl *
Sample ID I405235009 Sample Quantity 2.6300E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2546 of 5809 Key-Line Activity (pCi/GRAM 2.282E+00 4.861E-02 K.L. Cnt Uncert (1. 96-sigma) 6.193E+OO 2 .191E-01 MDA (pCi/GRAM MDA (pCi/GRAM 1.361E+Ol 4.694E-01 NOT .IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:12.54 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 5.01 166 89 0.41 23.95 22 6 4. 60E-02 11. 6 2 0 16.81 21 14 0.43 83.03 77 11 5.96E-03 39.8 3 0 36.66 7 0 0.55 182.43 177 9 1. 94E-03 37. 8 4 0 41. 39 9 3 1. 36 206 .11 200 10 2.62E-03 45.4 5 o. 57.90 12 0 0.25 288.75 283 11 3.33E-03 28.9 6 0 63.05 11 2 0.61 314.55 310 9 3.03E-03 38.9 7 0 64. 67 6 2 0.45 322.66 319 7 l.74E-03 53.2 8 2 70.09 12 1 0. 96 349.79 346 13 3.39E-03 34.7 4.21E-01 9 2 71. 29 12 2 0.65 355.82 346 13 3.26E-03 32.l 10 0 93.00 23 7 1. 31 464.51 456 14 6. 32E-03 32 .. 4 11 0 134.56 9 2 0.28 672. 65 668 9 2.44E-03 45.7 12 0 182. 13 11 6 0.42 910.91 904 12 3.06E-03 53.8 Page 2547 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:13.70 Nuclide Line Activity Report Flag: "*" = Keyline Page2548of5809 Surrunary of Nuclide Activity Sample ID : 1405235009 Acquisition date Page : 2 27-SEP-2016 16:18:41 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting surrunary Flags: "K" "E" Page 2549 of 5809 Keyline not found Manually edited "M" "A" 11 11 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235009 Acquisition date : 27-SEP-2016 16:18:41 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.81 7 14 .0.43 83.03 77 11 2.0lE-03 **** 7.68E-04 0 36.66 7 0 0.55 182.43 177 9 1. 94E-03 75.6 2.36E+Ol 0 41. 39 9 3 1. 36 206.11 200 10 2.62E-03 90.7 l.34E+Ol 0 57.90 12 0 0.25 288.75 283 11 3.33E-03 57.7 l.34E-01 0 63.05 6 2 0.61 314.55 310 9 l.58E-03 **** l.95E-02 0 64.67 6 2 0.45 322.66 319 7 l.74E-03 **** 1. 03E-02 2 70.09 12 1 0. 96 349.79 346 13 3.39E-03 69.5 l.12E-03 2 71. 29 12 2 0.65 355.82 346 13 3.26E-03 64.3 6. 72E-04 0 93.00 6 7 1. 31 464.51 456 14 1. 71E-03 **** 3.38E-08 0 134.56 9 2 0.28 672.65 66*8 9 2.44E-03 91. 4 2.81E-17 0 182.13 11 6 0.42 910.91 904 12 3.06E-03 **** 3.32E-28 Flags: "T" = Tentatively associated Page 2550 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:16.11 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l *
Acquisition date 27-SEP-2016 16:18:41 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
Sample date 10-DEC-2015 10:30:00 Nuclide Library : IODINE *
Sample ID I405235009 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.6300E+00 GRAM *
Recovery 1.00000 Carrier Weight 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combinyd Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2551 of 5809 Le. (pCi/GRAM 5.639E+OO NOT IDENT. l.922E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:19:17.37 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235009.CNF;l * *Acquisition date 27-SEP-2016 16:18:41 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
Sample date 10-DEC-2015 10:30:00 Nuclide Library : IODINE *
Sample ID I405235009 Analyst initials: MJHl * *.Batch Number 1598618 Sample Quantity 2.6300E+OO GRAM *
Quantity Err(%) 3.8023E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.282E+OO 6.206E+OO I-129 4. 8 61E-02 2 .191E-01 Page 2552 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 6.291E+OO 2.202E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2553 of 5809 MDA COUNTS 5.2595 5.3517 4.3235 5.5038 6.6880 8.5754 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:03.84 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 10-DEC-2015 10:35:00 Acquisition date : 27-SEP-2016 16:19:26 *Sample ID 1405235010 Sample quantity 3.34000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.21 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl . Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.66 3 6 0.32 122.81 119 7 9.57E-04123.8 2 0 27.52 6 6 0.40 137.17 132 8 1.62E-03 90.7 3 0 92.71* 9 3 0.61 463.84 A59 11 2.52E-03 62.2 4 0 139.94 12 3 0.75 700.53 693 12 3.28E-03 41. 5 5 0 158.54 7 5 1. 36 793.77 788 9 1.81E-03 70.7 6 0 185.65* 9 0 0.33 929.64 925 9 2. 51E-03 45.1 7 0 202.95 9 0 0.65 1016.33 1012 9 2.50E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 2554 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:04.73 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA , * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l *
Acquisition date 27-SEP-2016 16:19:26 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *
Sample date 10-DEC-2015 10:35:00 Analyst initials: MJHl *
Sample ID I405235010 Sample Quantity 3.3400E+00 GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 08:18:14 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Nuclide I-125 Activity (pCi/GRAM 2.786E+OO Cnt uncert (1. 96-sigma) 4.954E+OO Non-Identified Nuclides Nuclide I-129 Page 2555 of 5809 Key-Line Activity (pCi/GRAM 2.999E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.554E-01 MDA (pCi/GRAM 6.562E+OO MDA (pCi/GRAM 3.474E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:03.10 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 17. 21 *6 12 0.20 85.51 80 8 1.76E-03102.3 2 0 24.66 3 6 0.32 122.81 119 7 9.57E-04123.8 3 0 27.52 6 6 0.40 137 .17 132 8 1.62E-03 90.7 4 0 92. 71 17 3 0.61 463.84 459 11 4.72E-03 30.9 5 0 139. 94 12 3 0.75 -700.53 693 12 3.28E-03 41. 5 6 0 158.54 7 5 1. 36 793.77 788 9 1.81E-03 70.7 7 0 185.65 14 0 0.33 929.64 925 9 3.89E-03 26. 7 8 0 202.95 9 0 0.65 1016.33 1012 9 2.50E-03 33.3 Page 2556 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:04.20 Nuclide Line Activity Report Nuclide Type: Nuclide Energy Area I-125 27.34 6 30.97 ------35.49 ------Flag: "*" Key line Page 2557 of 5809 %Abn 114 .10* 20.30 6.68 %Eff 1.249E+Ol 1.514E+Ol 1.660E+Ol Uncorrected Decay Corr pCi/GRAM pCi/GRAM 9.202E-02 2.786E+OO ------Line Not Found ------Line Not Found 2-Sigma %Error 181.42 Surrunary of Nuclide Activity Sample ID : 1405235010 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 27-SEP-2016 16:19:26 Number of lines tentatively identified by NID 7 6 1 14.29% Nuclide Type : Nuclide I-125 Hlife 59.40D Uncorrected Decay pCi/GRAM 30.3 9.202E-02 Total Activity 9.202E-02 Grand Total Activity 9.202E-02 Flags: "K" "E" Page 2558 of 5809 Keyline not found Manually edited Decay Corr pCilGRAM . 2.786E+OO 2.786E+OO 2.786E+OO Decay Corr 2-Sigma Error 5.055E+OO Manually accepted 2-Sigma %Error Flags 181.42 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235010 Acquisition date : 27-SEP-2016 16:19:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 24.66 3 6 0.32 122.81 119 7 9.57E-04 **** 9.48E+OO 0 92.71 9 3 0.61 463.84 459 11 2.52E-03 **** 5.lOE-01 0 139.94 12 3 0.75 700.53 693 12 3.28E-03 83.0 6.82E-03 0 158.54 7 5 1. 36 793.77 788 9 1. 81E-03 **** l.15E-03 0 185.65 9 0 0.33 929. 64 925 9 2.51E-03 90.2 8.28E-05 0 202.95 9 0 0.65 1016.33 1012 9 2.50E-03 66.7 l.52E-05 Flags: "T" = Tentatively associated Page 2559 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:06.35 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l *
Acquisition date 27-SEP-2016 16:19:26 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapseq live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.21 Half life ratio : ****** *
Sample date 10-DEC-2015 10:35:00 Nuclide Library : IODINE *
Sample ID I405235010 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 3.3400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 Le (pCi/GRAM 2. 626E+OO ----Non-Identified Nuclides Nuclide I-129 Page 2560 of 5809 Le (pCi/GRAM l.360E-01 NOT IDENT.

VAX/VMS Nuclide Report Generated 27-SEP-2016 17:20:07.54 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235010.CNF;l * *Acquisition date 27-SEP-2016 16:19:26 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.21 Half life ratio : ***** *
Sample date 10-DEC-2015 10:35:00 Nuclide Library : IODINE *
Sample ID I405235010 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 3.3400E+OO GRAM *
Quantity Err(%) 2.9940E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 2.786E+OO Act Error ( 1. 96-sigma) 4.975E+OO Non-Identified Nuclides Nuclide I-129 Page 2561of5809 Key-Line Activity (pCi/GRAM 2.999E-02 K.L Act error. ( 1. 96-sigma) l.554E-01 TPU ( 1 . 96-sigma) 4.975E+OO TPU ( 1. 96-sigma) l.560E-01 NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charlestoni SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2562 of 5809 MDA*COUNTS 5.4288 3.3266 4.4884 2.2941 8.1513 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VM9 Nuclide Identification Report Generated 27-SEP-2016 17:20:28.54 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 9-DEC-2015 10:13:00. Acquisition date : 27-SEP-2016 16:19:47 Sample ID I405235011 Sample quantity 2.61000E+OO GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** *BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy, Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.53* 2 0 0.20 231.33 229 5 5.61E-04135.4 2 0 63.38* 6 4 0.32 315.27 311 8 l.77E-03 82.2 3 0 74.74* 6 0 0.53 371. 80 369 6 1. 75E-03 53.3 4 0 78.54 9 3 0.20 390.74 383 11 2.47E-03 49.8 5 0 92.69* 3 0 0.70 461.22 457 8 9. 51E-04139. 4 6 0 162. 02 8 3 0.39 806.47 800 11 2.35E-03 51. 0 Flag: "*" = Peak area was modified by background subtraction ( Page 2563 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 *17:20:29.39 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l *
Acquisition date 27-SEP-2016 16:19:47 Sensitivity : 3.000 *
Detector ID . XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *
Sample date 9-DEC-2015 10:13:00 Analyst initials: MJHl *
Sample ID I405235011 Sample Quantity 2.6100E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 * .
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNFj5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.152E-01 2.005E+OO I-129 9.429E-02 l.444E-01 Page 2564 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.607E+OO 4.988E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:27.85 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.53 6 0 0.20 231.33 229 5 l.67E-03 40.8 2 0 63.38 13 4 0.32 315.27 311 8 3.61E-03 38.5 3 0 74.74 10 0 0.53 371. 80 369 6 2.78E-03 31. 6 4 0 78.54 9 3 0.20 390.74 383 11 2.47E-03 49.8 5 0 92.69 18 0 0. 7.0 461.22 457 8 5.00E-03 23.6 6 0 162.02 8 3 0.39 806.47 800 11 2.35E-03 51. 0 Page 2565 of 5809 VAX/VMS.Nucliae Identification Report Generated 27-SEP-2016 17:20:28.93 Nuclide Line Activity Report Flag: "*" = Keyline ( Page 2566 of 5809 Summary of Nuclide Activity Sample ID : 1405235011 Acquisition date Total number of lines in spectrum 6 Number of unidentified lines 6 Number of lines tentatively identified by NID 0 **** There are no nuclides meeting summary criteria **** Page : 2 27-SEP-2016 16:19:47 0.00% Flags: "K" "E" Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Page 2567 of 5809 Unidentified Energy Lines Page : 3 Sample ID : 1405235011 Acquisition date : 27-SEP-2016 16:19:47 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.53 2 0 0.20 231.33 229 5 5.61E-04 **** 7.90E+OO 0 63.38 6 4 o,. 32 315.27 311 8 l.77E-03 **** 3.18E+OO 0 74.74 6 0 0.53 371. 80 369 6 1. 7 5E-03 **** 1.44E+OO 0 78.54 9 3 0.20 390.74 383 11 2.47E-03 99.7 1. 09E+OO 0 92.69 .3 0 0.70 461.22 457 8 9.51E-04 **** 3.57E-01 0 162.02 8 3 0.39 806.47 800 11 2.35E-03 **,** 8.37E-04 Flags: "T" = Tentatively associated Page 2568 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:30.94 *********'**********************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Conf'iguration. DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l *
Acquisition date 27-SEP-2016 16:19:47 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance': 1. OOQ *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *
Sample date 9-DEC-2015 10:13:00 Nuclide Library : IODINE *
Sample ID I405235011 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.6100E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : Il29 *
Eff. File' : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2569 of 5809 Le (pCi/GRAM l.456E+OO 1.714E-01 NOT IDENT .. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:32.03 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235011.CNF;l **
Acquisition date 27-SEP-2016 16:19:47 Sensitivity 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.06 Half life ratio : ***** *
Sample date 9-DEC-2015 10:13:00 Nuclide Library : IODINE *
Sample ID I405235011 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.6100E+OO GRAM *
Quantity Err(%) 3.8314E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Pleise refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96--:sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.152E-01 2.006E+OO I-129 9.429E-02 1.448E-01 Page 2570 of 5809 TPU ( 1. 96-sigma) TPD ( 1. 96-sigma) 2.015E+OO l.509E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2571of5809 MDA COUNTS 0. 8133 0.0000 0.8784 3.6923 1.9087 3.0566 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:52.82 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 10-DEC-2015 11:25:00 Acquisition date : 27-SEP-2016 16:20:09 Sample ID I405235012 Sample quantity 2.74000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance : 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2572 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:53.69
GEL Laboratories LLC
i 2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l * *Acquisition date 27-SEP-2016 16:20:09 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
Sample date 10-DEC-2015 11:25:00 Analyst initials: MJHl * *Sample ID I405235012 Sample Quantity 2.7400E+00 GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5'
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Cnt Uncert Activity K.L. Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.958E+OO 3.614E+OO I-129 l.310E-01 1.608E-01 Page 2573 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.090E+Ol 5.208E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:52.05 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2574 of 5809 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:53.19 Nuclide Line Activity Report Flag: "*" = Keyline Page 2575 of 5809 Summary of Nuclide Activity Sample ID : 1405235012 Acquisition date Page : 2 27-SEP-2016 16:20:09 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2576 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235012 None Flags: "T" Tentatively associated Page 2577 of 5809 Acquisition date Page : 3 27-SEP-2016 16:20:09 VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:55.21 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235012.CNF;l *
Acquisition date 27-SEP-2016 16:20:09 Sensitivity 3.000 *
Detector ID . XRAY6 Energy tolerance: 1.000 *
live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed time: 0 01:00:00.07 Half life : ***** *
Sample date 10-DEC-2015 11:25:00 Nuclide Library : IODINE *
Sample ID I405235012 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2578 of 5809 Le (pCi/GRAM 4.290E+00 NOT IDENT. 1.909E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 27-SEP-2016 17:20:56.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA. GAMMA.ARCHIVE. GAMMA] I40523.5012. CNF; 1 *
Acquisition date 27-SEP-2016 16:20:09 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio ***** *
Sample date 10-DEC-2015 11:25:00 Nuclide Library : IODINE *
Sample ID I405235012 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7400E+00 GRAM *
Quantity Err(%) 3.6496E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not ali "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K. L Act *error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.958E+OO 3.631E+OO I-129 1.310E-01 1.613E-01 Page 2579 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 4.046E+OO 1. 718E-0.1 NOT IDENT. NOT IDENT.
GEL Laboratories LLC **
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2580 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 0.7722 2. 3717 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:14.72 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235013.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 75-SEP-2016 12:22:59 Sample date 8-DEC-2015 11:23:00. Acquisition date : 28-SEP-2016 06:36:49 Sample ID I405235013 Sample quantity 2.77000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2581of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:15.62 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA *
* *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235013.CNF;l * *Acquisition date 28-SEP-2016 06:36:49 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *'
Sample date 8-DEC-2015 11:23:00 Analyst initials: MJHl * *Sample ID I405235013 Sample Quantity 2.7700E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 * *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]'EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.949E+OO 9.129E+OO I-129 4.713E-02 3.193E-01 Page 2582 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.085E+Ol 7.175E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 07:07:13.92 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2583 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:15.10 Nuclide Line Activity Report Flag: "*" = Keyline-, Page,2584of5809 Surrunary of Nuclide Activity Sample ID : 1405235013 Acquisition date Page : 2 28-SEP-2016 06:36:49 **** There are no nuclides meeting surrunary criteria **** Flags: "K" "E" Page 2585 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235013 None Flags: "T" Tentatively associated Page 2586 of 5809 Acquisition date Page : 3 28-SEP-2016 06:36:49 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:17.47 *******************************************************************************

GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *' Configuration DKAlOO: [CANBERRA. GAMMA.ARCHIVE. GAMMA] I405235013. CNF; 1 *
Acquisition date 28-SEP-2016 06:36:49 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 8-DEC-2015 11:23:00 Nuclide Library : IODINE *
Sample ID I405235013 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity : 2.7700E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA. GAMMA] EFF XRAY2 Il29 .. CNF; 15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2587 of 5809 Le (pCi/GRAM 8.145E+OO NOT IDENT. 2.780E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:07:18.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]i405235013.CNF;l * *Acquisition date 28-SEP-2016 06:36:49 Sensitivity 3.000 *
Detector ID XRAY2 ' Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 8-DEC-2015 11:23:00 Nuclide Library : IODINE *
Sample ID I405235013 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7700E+OO GRAM *
Quantity Err(%) 3.6101E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : _0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report Not all "Identified Nuclides" are valid. Please refer to Ceitificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM )_ Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.949E+OO 9.136E+OO I-129 4.713E-02 3.193E-01 Page 2588 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 9.178E+OO 3.201E-01 NOT IDENT. NOT IDENT.
- - - - '***********************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29.62 35. 49 39.58 Page 2589 of 5809 MDA COUNTS 3.1557 3. 2110 2.1618 4.4030 4.4587 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:47.60 ******************************************************************************** ** GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 8-DEC-2015 10:49:00. Acquisition date : 28-SEP-2016 06:45:16 Sample ID I405235014 Sample quantity 2.92000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy.tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K Pk It 1 0 Energy 14.62 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 13 2 0.34 72.50 69 7 7. 43E-03 31. 8 Flag: "*" = Peak area was modified by background subtraction Page 2590 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:48.45 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * ' *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l * *Acquisition date 28-SEP-2016 06:45:16 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 8-DEC-2015 10:49:00 Analyst initials: MJHl *
Sample ID I405235014 Sample Quantity 2.9200E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000
Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.275E+00 3. 791E+OO I-129 -8.457E-02 2.980E-01 Page 2591 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.209E+Ol 5.919E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:46.87 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2592 of 5809 Energy 14.62 Area 13 Bkgnd 2 FWHM Channel 0.34 72.50 Left 69 Pw Cts/Sec %Err 7 7.43E-03 31.8 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:i5:47.95 Nuclide Line Actiyity Report Flag:."*" = Keyline Page 2593 of 5809 Surrunary of Nuclide Activity Sample ID : 1405235014 Acquisition date Page : 2 28-SEP-2016 06:45:16 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting surrunary Flags: "K" "E" Page 2594 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235014 Page : 3 Acquisition date : 28-SEP-2016 06:45:16 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 14.62 13 2 0.34 72. 50 69 7 7.43E-03 63.6 6.25E-01 F1ags: "T" , Tentatively associated Page 2595 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:49.98 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l *
Acquisition date 28-SEP-2016 06:45:16 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half 'life ratio : ***** *
Sample date 8-DEC-2015 10:49:00 Nuclide Library : IODINE *
Sample ID I405235014 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.9200E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00006 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Cert'ificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2596 of 5809 Le (pCi/GRAM 4.499E+00 NOT IDENT. 2.097E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:15:51.11 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * * ' ; DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235014.CNF;l * *
Acquisition date 28-SEP-2016 06:45:16 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : ***** *
Sample date 8-DEC-2015 10:49:00 Nuclide Library : IODINE *
Sample ID I405235014 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.9200E+00 GRAM *
Quantity Err(%) 3.4247E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;14
Combined Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.275E+OO 3.834E+OO I-129 -8.457E-02 2. 981E-01 Page 2597of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.108E+OO 3.005E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY* 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2598 of 5809 MDA COUNTS 0.0000 3.3266 1.1221 2.2941 6.9868 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:50.73
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 8-DEC-2015 10:56:00. Acquisition date : 28-SEP-2016 06:48:23 Sample ID I405235015 Sample quantity 3.13000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 real time: 0 . 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN#. Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 87.30 295.19 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0 0.57 436.00 0.40 1476.17 433 1472 6 3.33E-03 40.8 8 40.8 Flag: "*" = Peak area was modified by background subtraction \ Page 2599 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:51.88 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l *
Acquisition date 28-SEP-2016 06:48:23 Sensitivity : 3.000 *
Detector ID . XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 8-DEC-2015 10:56:00 Analyst initials: MJHl *
Sample ID I405235015 Sample Quantity 3.1300E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]'EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-LinE:) Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.442E+OO 2.931E+OO I-129 O.OOOE+OO 1.764E-01 ( Page 2600 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.116E+Ol 2.438E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:49.84 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2601of5809 Energy 87.30 295.19 Area 6 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.57 436.00 433 0 0.40 1476.17 1472 6 3.33E-03 40.8 8 3.33E-03 40.8 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:51.24 Nuclide Line Activity Report Flag: "*" Key line Page 2602 of 5809 Summary of Nuclide Activity Sample ID : 1405235015 Total number of lines in spectrum Number of unidentified lines Acquisition date 2 2 Page : 2 28-SEP-2016 06:48:23 Number of lines tentatively identified by **** There are no nuclides meeting summary NID 0 criteria 0.00% **** Flags: ,;K" "E" Page 2603 of 5809 Keyline not found Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235015 Page : 3 Acquisition date : 28-SEP-2016 06:48:23 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff. Flags 0 0 87.30 295.19 6 6 0 0.57 436.00 433 6 3.33E-03 81.6 6.0lE-01 0 0.40 1476.17 1472 8 3.33E-03 81.6 2.29E-06 Flags: "T" = Tentatively associated Page 2604 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:53.71 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l * *Acquisition date 28-SEP-2016 06:48:23 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 00:30:00.04 Half.life ratio : ***** *
Sample date 8-DEC-2015 10:56:00 Nuclide Library : IODINE *
Sample ID I405235015 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 3.1300E+00 GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 *' Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2605 of5809 Le (pCi/GRAM 3.479E+OO O.OOOE+OO l NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:18:54.91 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 , * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235015.CNF;l * *Acquisition date 28-SEP-2016 06:48:23 Sensitivity 3.000 *
Detector ID . XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 8-DEC-2015 10:56:00 Nuclide Library : IODINE *
Sample ID I405235015 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 3.1300E+OO GRAM *
Quantity Err(%) 3.1949E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.442E+OO 2.934E+OO I-129 O.OOOE+OO O.OOOE+OO Page 2606 of 5809 TPU ( 1. 96-sigma ) TPU ( 1. 96-sigma) 3.005E+OO O.OOOE+OO NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27. 34* 29.62 35.49 39.58 Page 2607 of 5809 MDA COUNTS 0.0000 0.0000 1. 4921 0.0000 0.0000 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:02.09 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 8-DEC-2015 11:29:00. Acquisition date : 28-SEP-2016 06:55:30 Sample ID I405235016 Sample quantity 2.85000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K. LCS ID . : 1470-K ******************************************************************************** Pk It 1 0 Energy 92.55* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err ,7 0 0.55 460.50 456 9 3.73E-03 58.1 Flag: "*" = Peak area was modified by background subtraction Page 2608 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:02.95 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * . *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l *
Acquisition date 28-SEP-2016 06:55:30 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** * .: 1l: 29: OO GRAM :
B'atch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * -* *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Activity-MDA Report NOTE: all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 4.138E+OO 8.276E+OO I-129 3.359E-02 1.167E-01 Page 2609 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.197E+Ol 5.628E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:01.40 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2610of5809 Energy 92.55 Area 14 Bkgnd FWHM Channel 0 0.55 460.50 Left 456 Pw Cts/Sec %Err 9 7.78E-03 26.7 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:02.47 Nuclide Line Activity Re.port Flag: "*" = Keyline Page 2611 of 5809 Summary of Nuclide Activity Sample .ro : 1405235016 Acquisition date Page : 2 28-SEP-2016 06:55:30 Total number of lines.in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2612 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235016 Page : 3 Acquisition date : 28-SEP-2016 06:55:30 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 92.55 7 0 0.55 460.50 456 9 3.73E-03 ***** 3.61E-01 Flags: "T" = Tentatively associated Page 2613of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:04.87 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l *
Acquisition date 28-SEP-2-016 06:55:30 Sensitivity 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 11:29:00 Nuclide Library : *IODINE *
Sample ID I405235016 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.8500E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29'.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2614 of 5809 Le (pCi/GRAM 8.477E+OO NOT IDENT. l.385E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:26:06.07 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235016.CNF;l *
Acquisition date 28-SEP-2016 06:55:30 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 11:29:00 Nuclide Library : IODINE *
Sample ID I405235016 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.8500E+OO GRAM *
Quantity Err(%) 3.5088E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 4 .13*8E+OO 8.308E+00 I-129 3.359E-02 1.167E-01 Page 2615of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 8.515E+OO 1.177E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND .REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2616 of 5809 MDA COUNTS 1. 62 65 0.0000 0.0000 0.9231 0.9543 1. 018 9 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:55.37 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 2-DEC-2015 10:02:00. Acquisition date : 28-SEP-2016 07:22:16 Sample ID I405235017 Sample quantity 2.33000E+00 GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.11 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 159861B Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 20.58 14 5 1. 35 101.91 95 11 7. 51E-03 43.2 2 0 29.78 6 0 0.57 148.00 145 6 3.33E-03 40.8 3 0 34.84 6 0 0.38 173.33 17b 6 3.33E-03 40.8 4 0 115. 20 9 0 1. 79 575.67 569. 13 5.00E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 2617 of 5809 VAX/VMS Nuclide Ide.ntification Report Generated 28-SEP-2016 07: 53: 56. 2 6 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l * *Acquisition date 28-SEP-2016 07:22:16 Sensitivity : 3.000 *
Detector ID . XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *
Sample date 2-DEC-2015 10: 02: 00 Analyst initia*1s: MJHl *
Sample ID I405235017 Sample Quantity 2.3300E+00 GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 27-JUL-2016*12:15:07 Eff. Geometry : Il29 *
Eff. File : DKAl'OO: [CANBERRA.GAMMA]EFF XMY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 4.128E-01 Cnt uncert ( 1. 96-sigma) 3.303E-01 Non-Identified Nuclides Nuclide I-125 Page 2618of5809 Key-Line Activity (pCi/GRAM -3.109E+OO K.L. Cnt Uncert ( 1. 96-sigma) *l.290E+Ol MDA (pCi/GRAM 6.757E-01 MDA (pCi/GRAM 2.538E+Ol FAIL ABUN VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:54.64 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Char:inel Left Pw Cts/Sec %Err Fit 1 0 20.58 14 5 1. 35 101.91 95 11 7.51E-03 43.2 2 0 29.78 6 O* 0.57 148.00 145 6 3.33E-03 40.8 3 0 34.84 6 0 0.38 173.33 170 6 3.33E-03 40.8 4 0 92.88 7 5 0.65 463.93 457 9 3.98E-03 65.6 5 0 115. 20 9 0 1. 79 575.67 569 13 5.00E-03 33.3 Page 2619of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:55.79 Nuclide Line Activity Report Nuclide Type: FISSION Nuclide Energy Area I-129 29.62 6 33.59 ------39.58 ------Flag: "*" Key line Page 2620 of 5809 %Abn %Eff 56.60* 1.655E+Ol 10.04 2.487E+Ol 7.51 1. 7 67E+Ol Uncorrected Decay Corr pCi/GRAM pCi/GRAM 4.128E-01 4.128E-01 ------Line Not Found ------Line Not Found 2-Sigma %Error 81. 65 Summary of Nuclide Activity Sample ID : I40523o017 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 07:22:16 Number of lines tentatively identified by NID 4 2 2 50.00% Nuclide Type : FISSION Nuclide I-129 Hlife l.57E+07Y Uncorrected Decay pCi/GRAM 1.00 4.128E-01 Total Activity 4.128E'-01 Grand Total Activity 4.128E-01 Flags: "K" "E" Page 2621of5809 Keyline not found Manually edited Decay Corr pCi(GRAM 4.128E-01 4.128E-01 4.128E-01 Decay Corr 2-Sigma Error 3.370E-01 Manually accepted 2-Sigma %Error Flags 81. 65 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : !405235017 It Energy Area Bkgnd FWHM 0 20.58 14 5 1. 35 0 34.84 6 0 0.38 0 115.20 9 0 1. 79 Flags: "T" = Tentatively associated Page 2622 of 5809 Page : 3 Acquisition date : 28-SEP-2016 07:22:16 Channel Left Pw Cts/Sec %Err %Eff Flags 101.91 95 11 7.SlE-03 -86.4 1.30E-01 173.33 170 6 3.33E-03 81. 6 2.52E+Ol T 575.67 569 13 5.00E-03 66.7 5.83E-13 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:53:57.80 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l *
Acquisition date 28-SEP-2016 07:22:16 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *
Sample date 2-DEC-2015 10:02:00 Nuclide Library : IODINE *
Sample ID I405235017 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.3300E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : . 0. 00000 * ******************************************************************************* * --; * *
CALIBRATION INFORMATION * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 2.417E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2623 of 5809 Le (pCi/GRAM 9.779E+OO FAIL ABUN VAX/VMS Nuclide Identification Report Generated 07:53:59.28 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * * . DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235017.CNF;l *
Acquisition date 28-SEP-2016 07:22:16 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.11 Half life ratio : ***** *
Sample date 2-DEC-2015 10:02:00 Nuclide Library : IODINE *
Sample ID I405235017 Analyst initials: MJHl * '* Batch Number 1598618 Sample Quantity 2.3300E+OO GRAM *
Quantity Err(%) 4.2918E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 4.128E-01 Act Error ( 1. 96-sigma) 3.327E-01 Non-Identified Nuclides Nuclide I-125 Page 2624 of 5809 Key-Line Activity (pCi/GRAM -3.109E+OO K.L Act error ( 1. 96-sigma) 1 . .291E+Ol TPU ( 1. 96-sigma) 3.327E-01 TPU ( 1. 96-sigma) 1.298E+01 FAIL ABUN
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29.62 35.49 39.58 Page 2625 of 5809 MDA COUNTS 5.2595 2.1407 1. 6213 0.0000 1. 6720 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:07.51 *********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 2-DEC-2015 10:19:00. Acquisition date : 28-SEP-2016 07:22:56 Sample ID I405235018 Sample quantity 2.76000E+00 GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.08 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 10.11* BACKGROUND CORRECTED SAMPLE*PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 1 0.58 49.91 48 5 3.22E-03 60.7 Flag: "*" = Peak area was by background subtraction Page 2626 of 5809 I Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:08.33 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l *
Acquisition date 28-SEP-2016 07:22:56 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *
Sample date 2-DEC-2015 10:19:00 Analyst initials: MJHl * *Sample ID I405235018 Sample Quantity 2.7600E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKA100': [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.773E+OO 4.336E+OO I-129 -2.368E-01 3.781E-01 Page 2627 of 5809 MDA (pCi/GRAM MDA. (pCi/GRAM 1.380E+Ol 6.299E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:06.62 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2628 of 5809 Energy 10.11 Area 9 Bkgnd 1 FWHM Channel 0.58 49.91 Left 48 Pw Cts/Sec %Err 5 5.06E-0'3 37.4 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:07.84 Nuclide Line Activity Report Flag: "*" = Keyline Page 2629 of 5809 Summary of Nuclide Activity Sample ID : I405235018 Acquisition date Page : 2 28-SEP-2016 07:22:56 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2630 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235018 Page : 3 Acquisition date : 28-SEP-2016 07:22:56 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 10 .11 6 1 0.58 49.91 48 5 3.22E-03 **** l.65E-02 Flags: "T" = Tentatively associated Page 2631 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:09.89 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
*
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l *
Acquisition date 28-SEP-2016 07:22:56 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *
Sample date 2-DEC-2015 10:19:00 Nuclide Library : IODINE *
Sample ID I405235018 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity: 2.7600E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date* 17-JUN-2016 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclide I-125 I-129 Page 2632 of 5809 Le (pCi/GRAM 5.146E+OO NOT IDENT. 2.237E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:11.00 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235018.CNF;l *
Acquisition date 28-SEP-2016 07:22:56 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *
Sample date 2-DEC-2015 10:19:00 Nuclide Library : IODINE *
Sample ID I405235018 Analyst initials: MJHl * *Batch Number 1598618 Sample Quantity 2.7600E+OO GRAM *
Quantity Err(%) 3.6232E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date : '17-JUN-2016 08: 18: 14 Eff. Geometry : Il29' *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identi.fied Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.773E+00 4.386E+OO I-129 -2.368E-01 3.788E-01 Page 2633 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.704E+OO 3.936E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2634 of 5809 MDA COUNTS 0.0000 5.5444 1.1221 2.2941 0.0000 1.2005 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:32.95 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 12:23:20 Sample date 8-DEC-2015 14:30:00. Acquisition date : 28-SEP-2016 07:23:18 Sample ID I405235019 Sample quantity 2.56000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2635 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
* *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l *
Acquisition date 28-SEP-2016 07:23:18 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 14:30:00 Analyst initials: MJHl *
Sample ID I405235019 Sample Quantity 2.5600E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2b-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff.'File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K. L'. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 3.711E+OO I-129 1.518E-01 2.533E-01 Page 2636 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.131E+OO 8.990E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:32.19 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2637 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:33.28 Nuclide Line Activity Report Flag: "*" = Keyline Page 2638 of 5809 Summary of Nuclide Activity Sample ID : I405235019 Acquisition date Page : 2 28-SEP-2016 07:23:18 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2639 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235019 None Flags: "T" Tentatively associated Page 2640 of 5809 , Page : 3 Acquisition date 28-SEP-2016 07:23:18 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:35.35 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: *
Acquisition date 28-SEP-2016 07:23:18 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 14:30:00 Nuclide Library : IODINE *
Sample ID I405235019 Analyst initials: MJHl * *' Batch Number 1598618 Sample Quantity : 2. 5600E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * **
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]E.FF XRAY6 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2641 of 5809 Le (pCi/GRAM 0.000E+OO NOT IDENT. 3.006E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:55:36.46 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND .SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235019.CNF;l *
Acquisition date 28-SEP-2016 07:23:18 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 14:30:00 Nuclide Library : IODINE *
Sample ID I405235019 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.5600E+OO GRAM *
Quantity Err(%) 3.9063E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * * '* Eff. Cal. date 26-JAN-2016 10: 07: 09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid: Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-s igma) I-125 0.000E+OO O.OOOE+OO I-129 l.518E-01 2.537E-01 Page 2642 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) O.OOOE+OO 2.628E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2643 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 1.5445 0.7906 2.4852 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:57.75 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ************************t******************************************************* Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 8-DEC-2015 .13:50:00. Acquisition date : 28-SEP-2016 07:27:31 Sample ID I405235020 Sample quantity 2.97000E+OO GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 00-:30:00.00 Elapsed real time: 0 00:30:00.03 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Flag: "*" Page 2644 of 5809 Energy 63.22* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 10 0 0.63 314.46 310 10 5.38E-03 38.1 = Peak area was modified by background subtraction Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:58.58* *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I4052'35020.CNF;l *
Acquisition date 28-SEP-2016 07:27:31 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 13:50:00 Analyst initials: MJHl *
Sample ID I405235020 Sample Quantity 2.9700E+OO GRAM *
Batch Number 15.98618 Carrier Weight 0. 00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File. : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L. Cnt Un cert Nuclide (pCi/GRAM (1.96-sigma) I-125 3.322E-01 4.494E+OO I-129 5. 711E-02 2.909E-01 Page 2645 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.309E+Ol 8.351E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:57.03 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2646 of 5809 Energy 63.22 Area 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.63 314.46 310 10 7.22E-03 27.7 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:57:58.13 Nuclide Line Activity Report Flag: "*" = Keyline Page 2647of5809 Summary of Nuclide Activity Sample ID : 1405235020 Acquisition date Page : 2 28-SEP-2016 07:27:31 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary .Flags: "K" "E" Page 2648 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235020 Page : 3 Acquisition date : 28-SEP-2016 07:27:31 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.22 10 0 0.63 314.46 310 10 5.38E-03 76.2 3.22E+OO Flags: "T" =Tentatively associated Page 2649 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:58:00.07 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ***************************************)**************************************** * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l *
Acquisition date 28-SEP-2016 07:27:31 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 AbuDdance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** * *Sample date 8-DEC-2015 13:50:00 Nuclide Library: IODINE* *
Sample ID I405235020 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.9700E+00 GRAM *
Recovery l.OQOOO Carrier : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : Il29 *
Eff. File : 'DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2650 of 5809 Le (pCi/GRAM 4.138E+00 NOT IDENT. 2.805E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 07:58:01.14 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235020.CNF;l *
Acquisition date 28-SEP-2016 07:27:31 Sensitivity. : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.03 Half life ratio : ***** *
Sample date 8-DEC-2015 13:50:00 Nuclide Library : IODINE *
Sample ID I405235020 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.9700E+OO GRAM *
Quantity Err(%) 3.3670E-03 %* *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Geometry : I129 *
Eff .. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5 ** Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certiftcate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.322E-01 4.494E+00 I-129 5.711E-02 2.910E-01 Page 2651 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 4 .*497E+OO 2. 921E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27. 34 29.62 27.34 29.62 35.49 39.58 Page 2652 of 5809 MDA COUNTS 0.8133 0.8547 0.0000 0.0000 1.9087 2.0378
ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:57.73 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627430.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 75-SEP-2016 12:22:54 Sample 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 07:39:35 Sample ID I1203627430 Sample quantity 3.34000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID . : 1470-K ******************************************************************************** BACKGROUND *CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2653 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:58.68 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627430.CNF;l *
Acquisition date 28-SEP-2016 07:39:35 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed *live time: 0 00:30:00.00 Abundance* limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *
Sample ID Il203627430 Sample Quantity 3.3400E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l . * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Activity-MDA Report NOTE! Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7. 411E-02 l.016E-01 I-129 -l.098E-02 l.73°1E-01 Page 2654 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM l.473E-01 3.935E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:56.96 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2655 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:09:58.17 Nuclide Line Activity Report Flag: "*" = Keyline Page 2656 of 5809 Summary of Nuclide Activity Sample ID : 11203627430 Acquisition date Page : 2 28-SEP-2016 07:39:35 **** There are no nuclides meeting summary criteria **** Fiags: "K" "E" Page 2657 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627430 None Flags: "T" Tentatively associated Page 2658 of 5809 Acquisition date Page : 3 28-SEP-2016 07:39:35 VAX/VMS Nuclide Identification Report 28-SEP-2016 08:10:00.55 *******************************************************************************

GEL Laboratories LLC.
2040 Savage Road *
Charleston, SC 29407 * *******************************************************************************. *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627430.CNF;l * *Acquisition date 28-SEP-2016 07:39:35 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID Il203627430 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 3.3400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2659 of 5809 Le (pCi/GRAM 4.734E-02 NOT IDENT. l.478E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:10:02.01 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627430.CNF;l * *Acquisition date 28-SEP-2016 07:39:35 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID I1203627430 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 3.3400E+OO GRAM *
Quantity Err(%) 2.9940E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-.sigma) I-125 -7. 411E-02 l.025E-01 I-129 -l.098E-02 l.731E-01 Page 2660 of 5809 TPU (1.96-sigma) TPU (1. 96-sigma) 1.078E-01 1. 732E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road **
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2661of5809 MDA COUNTS 4.9062 3.3927 1.7312 0.8985 0.9215 3.8759 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:26.86 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627431.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 10-DEC-2015 14:20:00 Acquisition date : 28-SEP-2016 08:03:53 Sample ID I1203627431 Sample quantity 2.50000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.08 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K , LCS ID : 1470-K ******************************************************************************** Pk It 1 2 0 0 Energy 16.37* 61. 41 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 10 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.58 4 0.29 80.86 306.33 76 300 11 5.78E-03 61.0 8 2.78E-03 82.5 Flag: "*" = Peak area was modified by background subtraction Page 2662 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:27.66 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA] I1203627431.CNF;l * *Acquisition date 28-SEP-2016 08:03:53 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Analyst initials: MJHl *
Sample ID I1203627431 Sample Quantity 2.5000E+00 GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 27-JUL-2016 12: 15: 07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Un cert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.190E+OO 9.544E+OO I-129 8.699E-02 3.661E-01 Page 2663 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 8. 341E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:26.16 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2664 of 5809 Energy 16.37 61. 41 Area 18 5 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.58 80.86 4 0.29 306.33 76 11 9.72E-03 35.3 300 8 2.78E-03 82.5 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:27.22 Nuclide Line Activity Report Flag: 11*11 = Key line Page 2665 of 5809 Summary of Activity Sample ID : 11203627431 Acquisition date Page : 2 28-SEP-2016 08:03:53 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2666 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627431 It 0 0 Energy 16.37 61.41 Area 10 5 Bkgnd FWHM 6 0.58 4 0.29 Flags: "T" = Tentatively associated Page 2667 of 5809 Acquisition Channel Left Pw 80.86 76 11 306.33 300 8 Page : 3 date : 28-SEP-2016 08:03:53 Cts/Sec %Err %Eff Flags 5.78E-03 **** 3.43E-04 2.78E-03 **** 3.66E-02 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:29.53 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627431.CNF;l * *Acquisition date 28-SEP-2016 08:03:53 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance_: 1. 000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *
Sample ID I1203627431 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.5000E+OO GRAM *
Recovery 1.00000 Weight : 0.00000 * -* Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 * * 'Eff. File : DKAlOO: [CANBERRA. GAMMA] EFE XRAY2 1129. CNF; 15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2668 of 5809 Le (pCi/GRAM 8.280E+OO NOT IDENT. 3.276E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:30.88 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627431.CNF;l * *Acquisition date 28-SEP-2016 08:03:53 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.08 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *
Sample ID I1203627431 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.5000E+OO GRAM *
Quantity Err(%) 4.0000E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * *******************************************************'************************ * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129. *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1 . 96-sigma ) I-125 1.190E+OO 9.546E+OO I-129 8.699E-02 3.662E-01 Page 2669 of 5809 . TPU ( 1. 96-sigma) TPU (1.96-sigma) 9.561E+OO 3.683E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2670 of 5809 MDA COUNTS 3.1557 3.2110 3.2426 4.4030 7.8027 5.7170 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:51.76 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627432.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : Z5-SEP-2016 12:23:10 Sample date 10-DEC-2015 14:20:00 Acquisition date : 28-SEP-2016 08:04:20 Sample ID . Il203627432 Sample quantity 2.56000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.10 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 16.82* 9 7 0.57 83.56 78 10 4.98E-03 70.8 2 4 28.53 12 7 0.48 142.22 131 24 6.47E-03 52.3 1.13E+OO 3 4 29.68 179 7 0.65 147.98 131 24 9.95E-02 8.5 4 6 33.43 38 0 0.81 166.76 164 12 2. llE-02 17.3 3.06E+OO 5 6 34.39 25 0 0.69 171.59 164 12 1. 42E-02 30.7 6 0 39.62 24 2 0.29 197.79 194 8 l.33E-02 22.9 Flag: "*" = Peak area was modified by background subtraction Page 2671 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:52.73 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627432.CNF;l *
Acquisition date 28-SEP-2016 08:04:20 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : 8.000 *
Sample date 10-DEC-2015 14:20:00 Analyst initials: MJHl *
Sample ID I1203627432 Sample Quantity 2.5600E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File. : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM 1.298E+Ol Cnt uncert ( 1. 96-sigma) 2.163E+00 Non-Identified Nuclides Nuclide I-125 Page 2672 of 5809 Key-Line Activity (pCi/GRAM 1.537E+Ol K.L. Cnt Uncert ( 1. 96-sigma) 1. 206E+Ol MDA (pCi/GRAM 9.931E-01 MDA (pCi/GRAM 2.819E+Ol NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:50.97 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel .Left Pw Cts/Sec %Err Fit 1 0 16.82 13 7 0.57 83.56 78 10 6.97E-03 49.6 2 4 28.53 12 7 0.48 142.22 131 24 6.47E-03 52.3 1.13E+00 3 4 29.68 179 7 0.65 147.98 131 24 9.95E-02 8.5 4 6 33.43 38 0 0.81 166.76 164 12 2. llE-02 17.3 3.06E+OO 5 6 34.39 25 0 0.69 171. 59 164 12 1.42E-02 30.7 6 0 39.62 24 2 0.29 197.79 .194 8 1. 33E-02 22.9 Page 2673 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:52.17 Nuclide Line Activity Report Nuclide Type: FISSION Nuclide I-129 Energy 29. 62 33.59 39.58 Flag: "*". = Keyline Page 2674 of 5809 Area 179 38 24 %Abn 56.60* 10.04 7.51 %Eff l.430E+Ol 1.621E+Ol 1.618E+Ol Uncorrected pCi/GRAM l.298E+Ol 1.369E+Ol 1.153E+Ol Decay Corr pCi/GRAM l.298E+Ol 1.369E+Ol 1.153E+Ol 1-Sigrna %Error 8.50 17.26 22.93 Summary of Nuclide Activity Sample ID : I1203627432 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 08:04:20 Number of lines tentatively identified by NID 6 3 3 50.00% Nuclide Type : FISSION Nuclide I-129 Hlife 1. 57E+07Y Uncorrected Decay pCi/GRAM 1. 00 1. 298E+Ol Total Activity 1.298E+Ol Grand Total Activity 1.298E+Ol Flags: "K" "E" Page 2675 of 5809 Keyline not found Manually edited Decay Corr pCi7GRAM 1.298E+Ol 1.298E+Ol 1.298E+Ol Decay Corr 1-Sigma Error 0. llOE+Ol 1-Sigma %Error Flags *8.50 "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 11203627432 Acquisition date : 28-SEP-2016 08:04:20 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 16.82 9 7 0.57 83.56 78 10 4.98E-03 70.8 1.67E+OO 4 28.53 12 7 .0.48 142.22 131 24 6.47E-03 52.3 1.34E+Ol 6 34.39 25 0 0.69 171. 59 164 12 l.42E-02 30.7 1.65E+Ol Flags: "T" = Tentatively associated Page 2676 of 5809

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:54.52 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627432.CNF;l *
Acquisition date 28-SEP-2016 08:04:20 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : 8.000 *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *
Sample ID Il203627432 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 2.5600E+OO GRAM *
Recovery 1.00000 Carrier Weight : a.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Le (pCi/GRAM 3.983E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2677 of 5809 Le (pCi/GRAM 1.238E+Ol NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:34:55.74 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAiOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627432.CNF;l *
Acquisition date 28-SEP-2016 08:04:20 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.10 Half life ratio : 8.000 *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : IODINE *
Sample ID I1203627432 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 2.5600E+OO GRAM *
Quantity Err(%) 3.9063E-03 % *
Recovery 1.0000Q Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRAT,ION INFORMATION * * *
Eff: Cal. date 17-JUN-2016 08:18:14 Eff. : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1. 298E+Ol Act Error ( 1. 96-sigma) 2.517E+00 Non-Identified Nuclides Nuclide I-125 Page 2678 of 5809 Key-Line Activity (pCi/GRAM 1.537E+Ol K.L Act error ( 1. 96-sigma) 1.235E+Ol TPU ( 1. 96-sigma) 2.517E+00 TPU (1. 96-sigma) l.416E+Ol 'NOT IDENT.
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2679 of 5809 MDA COUNTS 5.4288 5.5444 5.0495 3.4411 6.9868 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:37.28 *********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627433.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 08:11:05 Sample ID I1203627433 Sample quantity 3.34000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000. Batch ID 1598618 Detector SN# Matrix Spike ID : 1470-K LCS ID , . 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.75 291 33 0.60 149.23 145 12 1.62E-01 7.3 2 0 33. 71 90 3* 0.48 169.18 164 12 4.98E-02 11. 3 3 0 39.54 49 0 0.80 198.55 193 13 2. 72E-02 14.3 Flag: "*" = Peak area was modified by background subtraction Page 2680 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:38.20 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627433.CNF;l * *Acquisition date 28-SEP-2016 08:11:05 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *
Sample ID Il203627433 Sample Quantity 3.3400E+OO GRAM *
Batch Number 1598618 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il2'9.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Pleaie refer to Certificate of Analysis. Identified Nuclides Nuclide I-129 Activity (pCi/GRAM L051E+Ol Cnt uncert (1. 96-sigma) l.500E+OO Non-Identified Nuclides Nuclide I-125 Page 2681of5809 Key-Line Activity (pCi/GRAM -5.238E-02 K.L. Cnt Uncert ( 1. 96-sigma) 3.087E-01 MDA (pCi/GRAM 9.173E-01 MDA (pCi/GRAM 5.310E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:36.48 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd *FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 29.75 291 33 0.60 149.23 145 12 1. 62E-01 7.3 2 0 33.71 90 3 0.48 169.18 164 12 4.98E-02 11. 3 3 0 39.54 49 0 0.80 198.55 193 13 2.72E-02 14.3 Page 2682 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:37.74 Nuclide Line Activity Report Nuclide Type: FISSION Nuclide I-129 Flag: "*" Page 2683 of 5809 Energy 29.62 33.59 39.58 Key line Area 291 90 49 %Abn 56.60* 10.04 7.51 %Eff 2.202E+Ol 2.304E+Ol 2.289E+Ol Uncorrected pCi/GRAM. 1.051E+Ol 1. 741E+Ol 1. 281E+Ol Decay Corr pCi/GRAM 1.051E+Ol 1. 741E+Ol 1.281E+Ol 2-Sigma %Error 14.56 22.54 28.57 Surrunary of Nuclide Activity Sample ID : I1203627433 Total *number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 08:11:05 Number of lines tentatively identified by NID 3 0 3 100.00% Nuclide Type : FISSION. Nuclide I-129 Hlife 1.57E+07Y Uncorrected Decay pCi/GRAM 1. 00 L 051E+Ol Total Activity 1. 051E+Ol Grand Total Activity 1. 051E+Ol Flags: "K" "E" Page 2684 of 5809 Keyline not found Manually edited Decay Corr pCi7GRAM 1.051E+Ol 1.051E+Ol 1. 051E+Ol Decay Corr 2-Sigma Error 0.153E+Ol Manually accepted 2-Sigma %Error Flags 14.56 "M" "A" Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627433 None Flags: "T" Tentatively associated Page 2685 of 5809 Acquisition date Page : 3 28-SEP-2016 08:11:05 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:39.73 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627433.CNF;l * *Acquisition date 28-SEP-2016 08:11:05 Sensitivity 3.000 * *Detector ID XRAYl Energy tolerance: 1.000-*
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID I1203627433 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity : 3.3400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6 * ***********************************************W*****W************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identif iea Nuclides Nuclide I-129* Le (pCi/GRAM 4.099E-01 ----Non-Identified Nuclides Nuclide I-125 Page 2686 of 5809 Le (pCi/GRAM 2.393E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 08:42:40.79 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627433.CNF;l * *Acquisition date 28-SEP-2016 08:11:05 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ****** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID Il203627433 Analyst initials: MJHl *
Batch Number 1598618 Sample Quantity 3.3400E+00 GRAM *
Quantity Err(%) 2.9940E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-129 1. 051E+Ol Act Error ( 1. 96-sigma) l.820E+OO Non-Identified Nuclides Nuclide I-125 Page 2687 of 5809 Key-Line Activity (pCi/GRAM -5.238E-02 K.L Act error ( 1. 96-sigma) 3.089E-01 TPU ( 1. 96-sigma) l.820E+OO TPU ( 1. 96-sigma) 3.098E-01 NOT IDENT.
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2688 of 5809 MDA COUNTS 30.6637 23.7490 10.3875 8.0864 9.6757 3.8759 ENERGY MDA COUNTS ENERGY MDA COUNTS Effective 3/25/201 O Revision 1 Effective March 201 O Radiochemistry Balch Checklist 09/29/16 Batch#_1_5_9_8_6_2_0 __ _ Product: 1-129 / MJWC Date:_0_9_/_2_9/_1,....6_ Criteria: i Yes No Comments S11mple Solids are less than or equal to 100 mQ for GAB. n/a Samples have been blank corrected (If required). n/a Blank correction renorted Included (If renulredl. If activity less than lOx MDA/MDC, error Is less than or equal to 1500/o of sample activity. ,/ If greater than 10* MDA/ MDC, error Is 40%" or less. If b0*nw the MDA/ MDC error Is okav Instrument source check Is within limits. In.:tr"ment bkn rh.,,.k I<: within limits. ,/ Method RDL/ LLD has been met. ,/ If duplicate activities are: Less than 5* MDA/ MDC, then RPD is 1000/o or less, If greater 5* MDA/ MDC, then RPD 200/o or less, If below the MDA/_ MDC, the RPD Is OD/o, ,/ Or meets the client's required RER acceotance criteria. Tracer yield Is 1S-12SD/o
Carrier yield 2S-125D/o. {Or meets the client's contract acceptance criteria). n /:. Method blank Is less than the RDL/ LLD. ,/ lrlf .. ntn:;, li"{o !If lllW!lliit !l!O!;llll .. Sample was run within hold time. I DER 1562566 ,/ ' Samele was correctlv oreserved if reoulred. Smears Taken for Radioactive batches. n/a* Method Spike and LCS are within 75-1250/o . ,/ (Or moots *hA Pllnn*'s contract crlterlal No blank spaces 'on data forms. ,/ All line outs Initialed and dated. INn are Aux data Is correct. ,/ Client Sneclal reoulrements oaoe has been checked. ,/ Raw Data and/ or snectrum are Included and nronerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ,/ .. verlfletl UI* *-. (ff ./ R"t*h antara .. ln*n r,.cn ./ Batch Data Exceetlon Reeorts (DER} comeleted, If aeellcable. / DER 1562566 Batch Data Exception Reports (DER) second reviewed. / Disnosltlon verified to be comnleted. . Allnuat Cnrr.,ctlnn co-n*et"d If renulred. ./ I// 9/z9l #fr/ <l IV /(, I Review sample historical results If available ,/ (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l Primary Rovlew Porformod By: Q0-4 tz.cr. (\-b C/ . Secondary Revlow Performed By: Page 2689 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 29-SEP-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1598620 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE EML HASL-300,1-01 Modified Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1562566 Revision No.: 1 Type: Process Client Code: MJWC Sample received out of holding: Samples were analyzed in .a timely manner upon receipt. Reporting results. 405235 021, 022,023, 024, 025, 026, 027' 028, 029, 030,031,032,033,034,035,036,037,038, 039,040 QC 1203627438DUP, 1203627439MS ' Originator's Name: Data Validator/Group Leader: Spencer Collins 29-SEP-16 Bryan Williams 29-SEP-16 Page 1 Page 2690 of 5809 0 ......., Vo 00 0 ID I-129 Queue Sheet 09/14/2016 Rat ch #:1598620 Analyst: MJHl First Client Due Datc:I0/04/2016 Internal Due Datc:09/30/2016 Spike Isotope: f-129 Spike Code: LCS Isotope: I-129 LCS Code: 141 D-K Prep Date: q...2.h-i b Initials:...-v.A..<) 4-._.v4:1";-21.:.-I;,, Expiration Date:<. o,0 .. Vol: 0. lv..t..{ Nomin:il Concentration: _ ___ _ Expiraiion Date: 3-3 0 -I Vol: o. 1......._L *Nominal Conccntration:._-'-lw.;,""*""* ___ _ Pipette ID: H :zc1303 Witness: N-1\-f3ALl>.Nc.£: i 7 '15"51 Sb Sample TD 405235022-l 405235023-1 405235024-1 405235026-l 4052350!i-l 40523:5028-1 405235029-1 405235030-1 40523:5031-1 405235032-1 405:?35033-1 405235034-1 405235035-1 405235036-1 40523503?-l 405235038-1 405235039-1 40523504Q-1 120362743i-1 1203627438-l 1203627439-l 1203627440-1 Client Description UB.R.2.3 4.2B.R.l-1 4.2B.R.l!.2 4.!B.R.2.2 4.!B.R.1.2 .uc.n.u 4.2C.R.JA 4..3J\RI.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.3.3 4.3B.R.3.4 4.3.B.R.JA 4.3B.R.2.3 4.4C.R.2.4 4.4C.R.I.3 4.-IC.R.IA 4.4D.R.l.3 :-.m for batch 1598620 4.2B.R.2.3(40523502JDUP} 4.2B.R.2.3(40523502li11S) LCS for batch 1598620 GEL Laboratories LLC, Radiochemistry Division Type SAMPLE S,\..\lPLE S.*\.\1PLE SAMPLE SAMPLE SAMPLE SA.,">ll'LE SA;llPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMP!,E SAMPLE. SAMPLE SAMPLE 'SAMPLE SAMPLE )!B DUP *1'1S LCS Hazard Code RDL I pCi/g l pCi!g I pCi/g ** l pCi/g l pCilg I pCUg l pCiig I pCi!g l pCi/g I pCi/g I pCilg I pCilg l pCilg I pCilg I pCi/g 1 pCUg 1 pCUg l pCi!g I pCi/g 1 pCL'g l pCUg l pCil:_? I pCi/g I 1>Cilg Client W<.,. . i\fatrix '°""_.-Collect Date ""DP.'1 AHquot (mLoi@) Detector Page 1 or l Weight/Loss Aliquot Correction Repo1i http://prodsvrOI.gel.com :7778/pls/lims/weight_loss _rpts.show _report Weight/Loss Aliquot Correction Report Select What to Correct Aliquot to < Ash Dry Weight Dry Weight -::i Wet Weight Batch ID: 1598620 Aliquot Correction to Dry Weight for Batch 1598620 I Sample Id I Aliquot (G) I sample Type !Parent Sample Id !Loss (Dec)!lcori;ected Aliquot (G), 1405235021 13.94 isAMPLE !NA ,.1654 :13.2s8i792682897o6 -1405235022 -r 3.23 !SAMPLE [NA

1.1937 12.604187628721362( " 1405235023 J4.18 I SAMPLE !NA 1.2255 .!3.237336122156177! f405235024 li22 -........ !SAMPLE !NA 1.1939 :I 2.s9.s32iii6827s62! [405235025 :13.00 !SAMPLE INA 1.2138 i 2.35B3S8470i324s6: 1405235026 J 3.05 lsAMPLE INA 1.1664 , 2.542323?512?3092_. -[405235027 13.63 *1SAMPLE INA 12.970780G55597255( : 1405235028 j3.38.-. -. ISAMPLE JNA 1.2267 i 1405235029 13.47--I SAMPLE !NA 1.1932 , 2.79956391512922 -f405235030 13.42 --,SAMPLE [NA-1.2389 12.602888768270461---. 1405235031 J 3.57 I SAMPLE INA 1.2258 J 2.763843686790458: [405235032 Jisg* ... .... *1SAMPLE INA 1.2036 12*.85874ii3792i3'386: 1405235033 14.00 :JsAMPLE JNA *1.1762 -I 3.294ss881s75Jso6-f4o5235034 f3.7o * . JsAMPLE .INA 1.1956 J 1405235035 r3.42 lsAMPLE INA 1.1626 '! -....... -. : 2.863609378360937! 1405235036 r3.24 ...... --.... ,SAMPLE INA J.1769 J 2.666ss:7ios6ooso-i; . [405235031 13.03 lsAMPLE INA f:0623 f2.s412161so261s82 J4o5235038 13.37 lsAMPLE INA 1.1634 I 2.s1907o4736ss432-f 405235039-J 3.47 I SAMPLE ---[NA 1.0869 13.168239125791668! -f4o523so40 J 4.15 lsAMPLE INA J.1478 I 3.53632807s496o36 _ ' *112036274371 IMB INA INA I ii 1203627438J 4.ci1 .:Jnur 1405235021 J.1654 I i346s9s6969i4*142* [ **
IMs 1405235021 1.1654 I 2.937662G96s43os7£ ------!NA ------[NA ____ :I GEL Laboratories LLC I of l 9/27/2016 11:25 AM Page 2692 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:56.34 *********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 8-DEC-2015 14:17:00. Acquisition date : 28-SEP-2016 08:45:02 Sample ID I405235021 Sample quantity 3.29000E+00 GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:38:04.89 Elapsed real time: 0 00:38:05.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 59.10 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 0 0.54 297.14 2'94 6 3.06E-03 37.8 Flag: "*" = Peak area was modified by background subtraction Page 2693 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:57.11 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l *
Acquisition date 28-SEP-2016 08:45:02 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:04.89 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:05.06 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Analyst initials: MJHl *
Sample ID I405235021 Sample Quantity 3.2900E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. *File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6 * ***********************************************T*****T************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ) ( 1. 96-sigma) I-125 1.235E+OO 4.824E+OO I-129 5.697E-02 2.039E-01 Page 2694 of 5809 MDA (pCi/GRAM MDA. (pCi/GRAM 9.388E+OO 4.564E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:55.55 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2695 of 5809 Energy 59.10 Area 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.54 297.14 294 6 3.06E-03 37.8 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:56.68 Nuclide Line Activity Report Flag: "*" = Keyline Page 2696 of 5809 Summary of Nuclide Activity Sample ID : 1405235021 Acquisition date Page : 2 28-SEP-2016 08:45:02 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2697 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235021 Page : 3 Acquisition date : 28-SEP-2016 08:45:02 It Energy Area Bkgnd FWHM Channel Pw Cts/Sec %Err %Eff Flags 0 59.10 7 0 0.54 297.14 294 6 3.06E-03 75.6 1.63E+Ol Flags: "T" = Tentatively associated Page 2698 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:58.57 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l * *Acquisition date 28-SEP-2016 08:45:02 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:04.89 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:05.06 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
Sample ID I405235021 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 3.2900E+OO GRAM *
Recovery 1.00000 -Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2699 of 5809 Le (pCi/GRAM 4.057E+OO NOT IDENT. l.892E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:59.61 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l *
Acquiiition date 28-SEP-2016 08:45:02 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:04.89 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:05.06 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
Sample ID I405235021 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.2900E+OO GRAM *
Quantity Err(%) 3.0395E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are Please refer to Certificate of Analysis. ----Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.235E+OO 4.828E+OO I-129 5.697E-02 2.040E-01 Page 2700 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.860E+OO 2.056E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT . * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2701 of 5809 MDA COUNTS 11. 038 9 5.9373 6.0593 6.2894 5.5290 0.9690 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:19.03 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 8-DEC-2015 13:43:00. Acquisition date : 28-SEP-2016 08:45:25 Sample ID I405235022 Sample quantity 2.60000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:37:43.11 Elapsed real time: 0 00:37:43.26 0.0% Energy tolerance 1.00000 keV Analyst Initials*: MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 6.24 27 50 0.49 30.14 28 6 1.20E-02 47.6 2 0 72 .18 6 2 0.48 360.25 356 7 2.76E-03 53.2 3 0 82.04 8 2 0.53 409.63 406 8 3.71E-03 44.5 4 0 92.46* 9 4 0.71 461.84 455 14 3.99E-03 68.1 5 0 132.97 9 0 0.33 664.67 658 12 3.98E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Pag.e 2702 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:19.83 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;) *
Acquisition date 28-SEP-2016 08:45:25 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 * *
Elapsed live time: 0 00:37:43.11 Abundance limit : 75.000 *
Elapsed real time: 0 00:37:43.26 Half life ratio : ***** *
Sample date 8-DEC-2015 13:43:00 Analyst initials: ,MJHl *
Sample ID I405235022 Sample Quantity 2.6000E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 8.869E+00 9.085E+OO I-129 1.625E-01 3 .115E-01 Page 2703 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.302E+Ol 7.337E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:18.36 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 6.24 27 50 0.49 30.14 28 6 1.20E-02 47.6 2 0 72.18 6 2 0.48 360.25 356 7 2.76E-03 53.2 3 0 82.04 8 2 0.53 409.63 406 8 3.71E-03 44.5 4 0 92.46 19 4 0. 71 461.84 455 14 8.61E-03 30.5 5 0 132.97 9 0 0.33 E;64.67 658 12 3.98E-03 33.3 Page 2704 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:19.38 Nuclide Line Activity Report Flag: "*" = Keyline Page 2705 of 5809 Summary of Nuclide Activity Sample ID : 1405235022 Total number of lines in spectrum Number of unidentified lines Acquisition date 5 Page : 2 28-SEP-2016 08:45:25 Number of lines tentatively identified by **** There are no nuclides meeting summary 5 NID 0 criteria 0.00% **** Flags: "K" "E" Page 2706 of 5809 Keyline not found Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235022 Acquisition date : 28-SEP-2016 08:45:25 It Energy Area Bkg_nd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 6.24 27 50 0.49 30.14 28 6 l.20E-02 95.3 2.66E-30 0 72 .18 6 2 0.48 360.25 356 7 2.76E-03 **** 4.60E-04 0 82.04 8 2 0.53 409.63 406 8 3.71E-03 89.1 5.78E-06 0 92.46 9 4 0.71 461.84 455 14 3.99E-03 **** 4.36E-08 0 132.97 9 0 0.33 664.67 658 12 3.98E-03 66.7 6.43E-17 Flags: "T" = Tentatively associated Page 2707 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:21*.69

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;l *
Acquisition date 28-SEP-2016 08:45:25 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:37:43.11 Abundance limit : 75.000 *
Elapsed real time: 0 00:37:43.26 Half life ratio : ***** *
Sample date 8-DEC-2015 13:43:00 Nuclide Library : IODINE *
Sample ID I405235022 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.6000E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2708 .of 5809 Le (pCi/GRAM 9.582E+OO NOT IDENT. 2.984E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:22.73 *******************************************************************************

GEL Laborator1es LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;l *
Acquisition date 28-SEP-2016 08:45:25 Sensitivity : 3.000 *
Detector ID : XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:37:43.11 Abundance limit : 75.000 *
Elapsed real time: 0 00:37:43.26 Half life ratio : ***** *
Sample date . 8-DEC-2015 13:43:00 Nuclide Library : IODINE *
Sample ID I405235022 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.6000E+00 GRAM *
Quantity Err(%) 3.8462E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. date 27-JUL-2016 12:15:07 Eff. Geometty : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 8.869E+OO 9.217E+OO I-129 1.625E-01 3.120E-01 Page 2709 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 1.005E+Ol 3.205E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2710 of 5809 MDA COUNTS 2.1038 3. 2110 3.2426 2.2015 2.2293 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report 28-SEP-2016 09:24:42.35 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235023.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 2-DEC-2015 10:40:00. Acquisition date : 28-SEP-2016 08:45:52 Sample ID I405235023 Sample quantity 3.24000E+00 GRAM Detector name : XRAY4 Detector. geometry: I129 Elapsed live time: 0 00:37:20.59 Elapsed real time: 0 00:37:20.71 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTE*D SAMPLE PEAK REPORT No peaks were found Page 2711of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:43.56 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235023.CNF;l *
Acquisition date 28-SEP-2016 08:45:52 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:37:20.59 Abundance limit : 75.000 * *Elapsed real time: 0 00:37:20.71 Half life ratio : ***** *
Sample date 2-DEC-2015 10:40:00 Analyst initials: MJHl *
Sample ID I405235023 Sample Quantity 3.2400E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 * "* Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -6.749E+OO 5.000E+OO I-129 5.620E-02
2 .196E-01 Page 2712 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.406E+OO 5.229E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:41.52 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2713 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:43.03 Nuclide Line Activity Report Flag: "*" = Keyline Page 2714 of 5809 Summary of Nuclide Activity Sample ID : 1405235023 Acquisition date Page : 2 28-SEP-2016 08:45:52 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2715of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235023 None Flags: "T" Tentatively associated Page 2716of5809 Acquis.i ti on date Page : 3 28-SEP-2016 08:45:52 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:06.50 *********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 8-DEC-2015 14:13:00. Acquisition date : 28-SEP-2016 08:46:16 Sample ID I405235024 Sample quantity 2.60000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:36:58.84 Elapsed real time: 0 00:36:58.88 0.0% Energy tolerance 1.00000 keV Analyst Initials Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2717of5809 VAX/VMS Nuclide Identification Report Generated .28-SEP-2016 09: 25: 07. 39 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l * *Acquisition date 28-SEP-2016 08:46:16 Sensitivity 3.000. *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:36:58.84 Abundance limit : 75.000 *
Elapsed real time: 0 00:36:58.88 Half life ratio : ***** *
Sample date 8-DEC-2015 14:13:00 Analyst initials: MJHl *
Sample ID I405235024 Sample Quantity 2.6000E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 **
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Ejf. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K. L. Cnt un*cert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.080E-01 4.166E+OO I-129 -2.406E-01 2. 722E-01 Page 2718 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1. 214E+Ol 2.542E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:05.65 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2719 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:06.88 Nuclide Line Activity Report Flag: "*" = Keyline Page 2720 of 5809 Summary of Nuclide Activity Sample ID : 1405235024 Acquisition date Page : 2 28-SEP-2016 08:46:16 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2721of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235024 None Flags: "T" Tentatively associated Page 2722 of 5809 Acquisition date Page : 3 28-SEP-2016 08:46:16 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:09.59 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l *
Acquisition date 28-SEP-2016 08:46:16 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:36:58.84 Abundance limit : 75.000 *
Elapsed real time: 0 00:36:58.88 Half life ratio : ***** *
Sample date 8-DEC-2015 14:13:00 Nuclide Library : IODINE *
Sample ID I405235024 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.6000E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Critical Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Le (pCi/GRAM 3.836E+OO NOT IDENT. O.OOOE+OO NOT IDENT.

VAX/VMS Nuclide Identification Generated 28-SEP-2016 09:25:11.02 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l *
Acquisition date 28-SEP-2016 08:46:16 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:36:58.84 Abundance limit : 75.000 *
Elapsed real time: 0 00:36:58.88 Half life ratio : ***** *
Sample date 8-DEC-2015 14:13:00 Nuclide Library : IODINE *
Sample ID I405235024 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.6000E+OO GRAM *
Quantity Err(%) 3.8462E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.080E-01 4.167E+OO I-129 -2.406E-01 2.733E-01 Page 2724 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.169E+OO* 2.940E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2725 of 5809 MDA COUNTS 0.8133 2.5641 1.7568 0.9231 0.0000 2.0378 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:34.51 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 8-DEC-2015 13:38:00. Acquisition date : 28-SEP-2016 08:46:38 Sample ID I405235025 Sample quantity 2.36000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:36:39.40 Elapsed real time: 0 00:36:39.44 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK RE*PORT No peaks were found Page 2726 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:36.40 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l *
Acquisition date 28-SEP-2016 08:46:38 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: .o 00:36:39.40 Abundance limit : 75.000 *
Elapsed real time: 0 00:36:39.44 Half life ratio : ***** *
Sample date 8-DEC-2015 13:38:00 Analyst initials: MJHl *
Sample ID I405235025 Sample Quantity 2.3600E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 '* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM .) (1. 96-sigma) I-125 3.082E+OO 4.463E+OO I-129 2.049E-01 2. 772E-01 Page 2727 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.515E+Ol 9.224E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:32.99 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2728 of 5809 VAX/VMS Nuclide Identifi.cation Report Generated 28-SEP-2016 09: 25: 35. 36 Nuclide Line Activity Report Flag: "*" = Keyline Page 2729 of 5809 Summary of Nuclide Activity Sample ID : 1405235025 Acquisition date Page : 2 28-SEP-2016 08:46:38 **** There are no nuclides meetin9 summary criteria **** Flags: "K" "E" Page 2730 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235025 None Flags: "T" Tentatively associated Page 2731 of 5809 Acquisition date Page : 3 28-SEP-2016 08:46:38 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:39.58 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *'
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l *
Acquisition date 28-SEP-2016 08:46:38 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:36:39.40 Abundance limit : 75.000 *
Elapsed real time: 0 00:36:39.44 Half life ratio : ***** *
Sample date 8-DEC-2015 13:38:00 Nuclide Library : IODINE *
Sample ID I405235025 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.3600E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2732 of 5809 Le (pCi/GRAM . ) 5.298E+OO *NOT IDENT. 3.291E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:41.99 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l *
Acquisition date 28-SEP-2016 08:46:38 Sensitivity 3.000 *
Detector ID XRAY6 . Energy tolerance: 1. 000 *
Elapsed live time: 0 00:36:39.40 Abundance limit : 75.000 *
Elapsed real time: 0 00:36:39.44 Half life ratio : ***** *
Sample date 8-DEC-2015 13:38:00 Nuclide Library : IODINE *
Sample ID I405235025 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.3600E+00 GRAM *
Quantity Err(%) 4.2373E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal., date 10: 07: 09 Eff. Geometry : 1129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-.sigma) *Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.082E+OO 4.472E+OO I-129 2.049E-01 2.780E-01 Page 2733 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.683E+OO 2.929E-01 NOT IDENT. NOT IDENT.
- - - - £**************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2734 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 2.3167 0.0000 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report 28-SEP-2016 10:15:42.48 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 8-DEC-2015 10:15:00. Acquisition date : 28-SEP-2016 09:28:33 Sample ID I405235026 Sample quantity 2.54000E+OO GRAM Detector name : XRAYl Detector geometry: I-129 Elapsed live time: 0 00:46:46.72 Elapsed real time: 0 00:46:46.92 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 95.02 120.45 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 3 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.39 478.17 10 0.30 606.33 474 8 2.14E-03 40.8 598 10 l.07E-03205.5 Flag: "*" = Peak area was modified by background subtraction Page 2735 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:43.29 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l * *Acquisition date 28-SEP-2016 09:28:33 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 00:46:46.72 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:46.92 Half life ratio : ***** *
Sample date . 8-DEC-2015 10: 15: 00 Analyst initials: MJHl *
Sample ID I405235026 Sample Quantity 2.5400E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il2'9.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 7.436E-01 3.805E+00 I-129 2.314E-02 1. 752E-01 Page 2736 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.756E+OO 3. 996E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:40.82 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 2737 of 5809 Energy 95.02 120.45 Area 6 3 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.39 478.17 10 0.30 606.33 474 8 2.14E-03 40.8 598 10 l.07E-03205.5 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:42.85 Nuclide Line Activity Report Flag: "*" = Keyline Page 2738 of 5809 Summary of Nuclide Activity Sample ID : 1405235026 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 09:28:33 Number of lines tentatively identified by **** There are no nuclides meeting summary 2 2 NID 0 criteria 0.00% **** Flags: "K" Keyline not found "E" = Manually edited Page 2739 of 5809 "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235026 Page : 3 Acquisition date : 28-SEP-2016 09:28:33 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 95.02 120.45 6 3 0 0.39 10 0.30 Flags: "T" = Tentatively associated Page 2740 of 5809 478.17 474 8 2.14E-03 81.6 5.50E+OO 606.33 598 10 1.07E-03 **** 2.27E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:44.92 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l *
Acquisition date 28-SEP-2016 09:28:33 Sensitivity : 3.000 *
Detector ID XRAYl *Energy tolerance: 1.000 * *Elapsed live time: 0 00:46:46.72 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:46.92 Half life ratio : ***** *
Sample date 8-DEC-2015 10:15:00 Nuclide Library : IODINE *
Sample ID I405235026 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.5400E+OO GRAM *
Recovery 1.00000 Carrier Weight :
0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION IN.FORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff: File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2741of5809 Le (pCi/GRAM 3.204E+OO NOT IDENT. l.586E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:46.24

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DET.ECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l *
Acquisition date 28-SEP-2016 09:28:33 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 .00:46:46.72 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:46.92 Half life ratio : ***** *
Sample date 8-DEC-2015 10:15:00 Nuclide Library : IODINE *
Sample ID I405235026 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.5400E+OO GRAM *
Quantity Err(%) 3.9370E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) .Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.436E-01 3.807E+OO I-129 2.314E-02 1. 752E:-01 Page 2742 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.822E+OO 1.755E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LL*c *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2743 of 5809 MDA COUNTS 6.1327 4.2409 6.0593 4.4924 4.6075 4.8449 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:06.11
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 8-DEC-2015 10:19:00. Acquisition date : 28-SEP-2016 09:28:55 Sample ID I405235027 Sample quantity 2.97000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 . Elapsed live time: 0 00:46:24.90 Elapsed real time: 0 00:46:25.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd *FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 5'4. 20 6 7 0.71 270.24 263 9 2. 31E-03 82.7 2 0 87.03 9 3 0.99 434.61 430 10 3.28E-03 46.8 3 0 92.83* 9 3 0.82 463.68 458 11 3.41E-03 63.7 4 0 126.22 9 0 0.40 630.89 625 12 3.23E-03 33.3 5 0 129.38 9 3 0.35 646.72 639 13 3.19E-03 53.5 6 0 144.07 11 0 0.56 720.27 716 10 3.95E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 2744 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:06.88 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l * *Acquisition date 09:28:55 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:46:24.90 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:25.06 Half life ratio : *****
Sample date 8-DEC-2015 10:19:00 Analyst initials: MJHl *
Sample ID I405235027 Sample Quantity 2.9700E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l . * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.'CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sfgma) Non-Identified Nqclides Nuclide I-125 .I-129 Page 2745 of 5809 , Key-Line Activity (pCi/GRAM -5.286E-02 4.226E-02 K.L. Cnt Uncert ( 1. 96-sigma) 7.746E+OO 2.471E-01 MDA (pCi/GRAM MDA (pCi/GRAM 1.557E+Ol 5.254E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:05.43 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 13.90 5 27 0.31 68.47 61 10 l.78E-03202.6 2 0 54.20 6 7 0. 71 270.24 263 9 2.31E-03 82.7 3 0 87.03 9 3 0.99 434.61 *430 10 3.28E-03 46.8 4 0 92.83 22 3 0.82 463.68 458 11 8.02E-03 25.5 5 0 126.22 9 0 0.40 630.89 625 12 3.23E-03 33.3 6 0 129.38 9 3 0.35 646.72 639 13 3.19E-03 53.5 7 0 144.07 11 0 0.56 . 720.27 716 10 3.95E-03 30.2 Page 2746 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:06.44 Nuclide Line Activity Report Flag: "*" = Keyline Page 2747of5809 Summary of Nuclide Activity Sample ID : 1405235027 Acquisition date . Page : 2 28-SEP-2016 09:28:55 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuc.lides meeting summary Flags: "K" "E" Page 2748 of 5809 Keyline not found Manually edited "M" "A" 6 6 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235027 Acquisition date : 28-SEP-2016 09:28:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 54.20 6 7 0. 71 270.24 263 9 2.31E-03 **** 4.79E-01 0 87.03 9 3 0.99 434.61 430 10 3.28E-03 93.6 5.73E-07 0 92.83 9 3 0.82 463.68 458 11 3.41E-03 **** 3.66E-08 0 126.22 9 0 0.40 630.89 625 12 3.23E-03 66.7 2.lOE-15 0 129.38 9 3 0.35 646.72 639 13 3.19E-03 **** 4. llE-16 0 144.07 11 0 0.56 720. 27 716 10 3.95E-03 60.3 1. 97E-19 Flags: "T" = Tentatively associated Page 2749 of 5809 VAX/VMS Nuclide Report Generated 28-SEP-2016 10:16:08.39 *******************************************************************************

GEL Laboratories LLC *
2040 Savage.Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l * *Acquisition date 28-SEP-2016 09:28:55 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:46:24.90 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:25.06 Half life ratio : ***** *
Sample date 8-DEC-2015 10:19:00 Nuclide Library : IODINE *
Sample ID I405235027 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.9700E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100 :'[CANBERRA. GAMMA] EFF XRAY2 Il29. CNF; 15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Nuclides Nuclide I-125 I-129 Page 2750 of 5809 Le (pCi/GRAM 6.407E+OO NOT IDENT. 2.140E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:09.44 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, sc* 29407 . * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l * *Acquisition date 28-SEP-2016 09:28:55 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:46:24.90 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:25.06 Half life ratio : ***** *
Sample date 8-DEC-2015 10:19:00 Nuclide Library : IODINE *
Sample ID I405235027 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.9700E+OO GRAM *
Quantity Err(%) 3.3670E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 0'0000 * ********************************************************.*********************** * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate.of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -5.286E-02 7.746E+OO I-129 4.226E-02 2.471E-01 Page 2751of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 7.746E+OO 2.478E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2752 of 5809 MDA COUNTS 7.3633 5.3517 2.1618 3.3023 2.2293 3.4302 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:29.09 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 75-SEP-2016 12:23:10 Sample date 23-NOV-2015 14:50:00 Acquisition date : 28-SEP-2016 09:29:20 Sample ID I405235028' Sample quantity 2.61000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:46:04.82 Elapsed real time: 0 00:46:04.97 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 35.56 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 4 0.60 177.46 173 7 2. 35E-03 61. 8 Flag: "*" = Peak area was modified by background subtraction Page 2753 of 5809 Fit VAX/VMS Nuclide Identijication Report Generated 28-SEP-2016 10:16:29.91 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l * *Acquisition date 28-SEP-2016 09:29:20 Sensi*tivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:46:04.82 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:04.97 Half life ratio : ***** *
Sample date 23-NOV-2015 14:50:00 Analyst initials: MJHl *
Sample ID I405235028 Sample Quantity 2.6100E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.708E+00 4.341E+OO I-129 -2.llOE-01 2.433E-01 Page 2754 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM l.169E+Ol 3.417E-01 FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:28.17 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 35.56 7 4 0.60 177.46 173 7 2.35E-03 61. 8 2 0 92.73 5 7 0.22 463.91 460 6 1.73E-03100.6 Page 2755 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:29.41 Nuclide Line Activity Report Flag: "*" = Keyline Page 2756 of 5809 Summary of Nuclide Activity Sample ID : 1405235028 Acquisition date Page : 2 28-SEP-2016 09:29:20 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2757 of 5809 not found Manually edited "M" "A" 1 0 NID 1 criteria 100.00% **** Manualiy accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235028 Page : 3 Acquisition date : 28-SEP-2016 09:29:20 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 35.56 7 4 0.60 177.46 173 2.35E-03 **** 1.66E+Ol T Flags: "T" = Tentatively associated Page 2758 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:31.48

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *******************************************************************************-* * * ) J DETECTOR*AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l *
Acquisition date 28-SEP-2016 09:29:20 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:46:04.82 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:04.97 Half life ratio : ***** *
Sample date 23-NOV-2015 14:50:00 Nuclide Library : IODINE *
Sample ID I405235028 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.6100E+00 GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Critical Level Report* NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2759 of 5809 Le (pCi/GRAM 4.504E+00 FAIL ABUN l.080E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:32.55 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l *
Acquisition date 28-SEP-2016 09:29:20 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:46:04.82 Abundance limit : 75.000 *
Elapsed real time: 0 00:46:04.97 Half life ratio : ***** *
Sample date 23-NOV-2015 14:50:00 Nuclide Library : IODINE *
Sample ID I405235028 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.6100E+OO GRAM *
Quantity Err(%) 3.8314E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date : '17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1; 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2760 of 5809 Key-Line Activity (pCi/GRAM 2.708E+OO -2. llOE-01 K.L Act error ( 1. 96-sigma) 4.366E+OO 2.442E-01 TPU ( 1. 96-sigma) TPU . ( 1. 96-sigma) 4.534E+00 FAIL ABUN 2.621E-01 NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2761of5809 MDA COUNTS, 1.0858 5.5444 4.4884 1.1470 1.1645 3.6015 ENERGY MDA COUNTS ,ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:52.26 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 23-NOV-2015 11:10:00 Acquisition date : 28-SEP-2016 09:29:56 Sample ID I405235029 Sample quantity 2.80000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:45:30.43 Elapsed real time: 0 00:45:30.47 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.59* BACKGROUND CORRECTED.SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 1 4 0.56 316.31 310 8 2.83E-04569.7 Flag: "*" = Peak area was modified by background subtraction Page 2762 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:53.03 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l *
Acquisition date 28-SEP-2016 09:29:56 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:45:30.43 Abundance limit : 75.000 *
Elapsed real time: 0 Half life ratio : ***** *
Sample date 23-NOV-2015 11:10:00 Analyst initials: MJHl *
Sample* ID I405235029 Sample Quantity 2. 8000E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Ac ti vi ty-MDA Repor,t NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1, 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 -4.832E+OO 4.735E+OO I-129 -5.022E-02 2.177E-01 Page 2763 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.025E+OO 5.210E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:51.60 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2764 of 5809 Energy 63.59 Area 6 Bkgnd FWHM Channel 4 0.56 316.31 Left 310 Pw Cts/Sec %Err 8 2.12E-03 73.1 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:52.59 Nuclide Line Activity Report Flag: "*" = Keyline Page 2765 of 5809 Summary of Nuclide Activity Sample ID : 1405235029 Acquisition date Page : 2 28-SEP-2016 09:29:56 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2766 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235029 Page : 3 Acquisition date : 28-SEP-2016 09:29:56 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.59 1 4 0.56 316.31 310 8 2.83E-04 **** 3.14E+OO Flags: "T" = Tentatively associated Page 2767 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:54.58

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l *
Acquisition date 28-SEP-2016 09:29:56 Sensitivity 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:45:30.43 Abundance limit : 75.000 *
Elapsed real time: 0 00:45:30.47 Half life ratio : ***** *
Sample date 23-NOV-2015 11:10:00 Nuclide Library : IODINE *
Sample ID I405235029 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.8000E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA.JEFF XRAY5 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2768 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. l.647E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:55.66 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l *
Acquisition date 28-SEP-2016 09:29:56 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:45:30.43 Abundance limit : 75.000 *
real time: 0 00:45:30.47 Half life ratio : ***** *
Sample date 23-NOV-2015 11:10:00 Nuclide Library : IODINE *
Sample ID I405235029 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.8000E+00 GRAM *
Quantity Err(%) 3.5714E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 * .* Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides
Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.832E+OO 4.810E+OO I-129 -5.022E-02 2.177E-01 Page 2769 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 5.280E+OO 2.189E-01 NOT IDENT. NOT IDENT.
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2770 of 5809 MDA COUNTS 3.2531 1. 7094 0.8784 4.6154 0.9543 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:15.32 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 23-NOV-2015 14:44:00 Acquisition date : 28-SEP-2016 09:30:21 Sample ID I405235030 Sample quantity 2.60000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:45:07.66 Elapsed real time: 0 00:45:07.72 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 7.43* 10.27 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 4 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err . 2 0. 56 1 0.36 36.37 50.62 34 49 5 1.66E-03 81.4 4 2.68E-03 41.4 Flag: "*" = Peak area was modified by background subtraction Page 2771of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:16.26 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO :. [CANBERRA. GAMMA.ARCHIVE. GAMMA] I405235030. CNF; 1 *
Acquisition date. 28-SEP-2016 09:30:21 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 * *Elapsed live time: 0 00:45:07.66 Abundance limit : 75.000 *
Elapsed real time: 0 00:45:07.72 Half life ratio : ***** *
Sample date 23-NOV-2015 14:44:00 Analyst initials: MJHl *
Sample ID I405235030 Sample Quantity 2.6000E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : *n29 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.092E+00 4.lOlE+OO I-129 *-6.592E-02 2.316E-01 Page 2772 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.005E+OO 4.432E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:14.59 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 7.43 7 2 0.56 36.37 34 5 2.59E-03 49.7 2 0 10 .27 7 1 0.36 50.62 49 4 2.68E-03 41. 4 Page 2773 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:15.71 Nuclide Line Activity Report Flag: "*" = Keyline Page 2774 of 5809 Summary of Nuclide Activity Sample ID : 1405235030 Acquisition date Page : 2 28-SEP-2016 09:30:21 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no meeting summary Flags: "K" Keyline not found "E" = Manually edited Page 2775 of 5809 "M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235030 Page : 3 Acquisition date : 28-SEP-2016 09:30:21 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 7.43 10.27 4 7 2 0.56 1 0.36 Flags: RT" = Tentatively associated Page 2776 of 5809 36.37 50.62 34 5 l.66E-03 **** 3.52E-03 49 4 2.68E-03 82.8 7.lOE-02 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:17.92 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l *
Acquisition date 28-SEP-2016 09:30:21 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 * *Elapsed live time: 0 00:45:07.66 Abundance limit : 75.000 * *Elapsed real . 0 00:45:07.72 Half life ratio : ***** *
Sample date 23-NOV-2015 14:44:00 Nuclide Library : IODINE *
Sample ID I405235030 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.6000E+00 GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 * '* Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5 * .Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of.Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2777 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. l.241E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:19.07 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l * *Acquisition date 28-SEP-2016 09:30:21 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 * *Elapsed li.ve time: 0 00:45:07.66 Abundance limit : 75.000 *
Elapsed real time: 0 00:45:07.72 Half life ratio : ***** *
Sample date 23-NOV-2015 14:44:00 Nuclide Library : IODINE *
Sample ID I405235030 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.6000E+OO GRAM *
Quantity Err(%) 3.8462E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION . * * * * 'Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : 1129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( l. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -2.092E+OO 4.105E+OO I-129 -6.592E-02 2.317E-01 Page 2778 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 4.212E+OO 2.336E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2779 of 5809 MDA COUNTS 1.4157 1.4643 0.0000 0. 7722 0.7906 1.6568 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:30.25 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : Z5-SEP-2016 12:22:54 Sample date 26-NOV-2015 14:25:00 Acquisition date : 28-SEP-2016 10:17:59 Sample ID I405235031 Sample quantity 2.76000E+00 GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 23.69 BACKGROUND*CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 20 '.2 0 0 . 5 6 118 . 7 2 113 11 l.09E-02 53.0 Flag: "*" = Peak area was modified by background subtraction Page 2780 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:31.04
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l *
Acquisition date 28-SEP-2016 10:17:59 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-NOV-2015 14:25:00 Analyst initials: MJHl * *Sample ID I405235031 Sample Quantity 2.7600E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. Fil'e : DKA100: [CANBERRA.GAMMA]EFF XRAYl' I129.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96:-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -9. 311E-01 5.701E+OO I-129 O.OOOE+OO 2.630E-01 Page 2781of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.077E+Ol 5.775E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:29.46 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2782 of 5809 Energy 23.69 Area 20 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 20 0.56 118.72 113 11 1.09E-02 53.0 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:30.59 Nuclide Line Activity Report Flag: "*" = Keyline Page 2783 of 5809 Summary of Nuclide Activity Sample ID : 1405235031 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 10:17:59 Numb.er of lines tentatively identified by **** There are no nuclides meeting summary 1 1 NID 0 criteria 0.00% **** Flags: "K" Keyline not found "E" = Manually edited Page 2784 of 5809 "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235031 Page : 3 Acquisition date : 28-SEP-2016 10:17:59 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 23.69 20 20 0.56 118.72 113 11 1.09E-02 **** 1.80E+Ol Flags:. "T" Tentatively associated Page 2785 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:32.83 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l * *Acquisition date 28-SEP-2016 10:17:59 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-NOV-2015 14:25:00 Nuclide Library : IODINE *
Sample ID I405235031 Analyst initi'als: MJHl * *Batch Number 1598620 Sample Quantity : 2.7600E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * * .CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff: Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2786 of 5809 Le (pCi/GRAM 4.276E+OO NOT IDENT. 2.296E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:33.95 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l * *Acquisition date 28-SEP-2016 10:17:59 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
Sample date 26-NOV-2015 14:25:00 Nuclide Library : IODINE *
Sample ID I405235031 Analyst initials: MJHl * *Batch Number 1598620 Sample Quantity 2.7600E+00 GRAM *
Quantity Err ( % ) 3. 6232E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. 'Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Activity-MDA Report NOTE: Nbt all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -9. 311E-01 5.703E+OO I-129 O.OOOE+OO '2. 630E-01 Page 2787of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.719E+OO O.OOOE+OO NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 .39.58 Page 2788 of 5809 MDA COUNTS 6.1327 5.0891 4.3281 6.2894 8.2934 6.7829 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2019 10:49:03.08 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 23-NOV-2015 11:48:00 Acquisition date : 28-SEP-2016 10:18:25 Sample ID I405235032 Sample quantity 2.86000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: .0 00:30:00.13 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID /1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 185.52* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 13 0 1.80 927.89 920 15 7.44E-03 32.7 Flag: "*" = Peak area was modified by background subtraction Page 2789 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:03.88 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l *
Acquisition date 28-SEP-2016 10:18:25 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *
Sample date 23-NOV-2015 11:48:00 Analyst initials: MJHl *
Sample ID I405235032 Sample Quantity 2.8600E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7.655E-01 1. 096E+Ol I-129 9.754E-02 3.274E-01 Page 2790 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.298E+Ol 7.522E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:02.41 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2791of5809 Energy 185.52 Area 18 Bkgnd FWHM Channel 0 1.80 927.89 Left 920 Pw Cts/Sec %Err 15 1. OOE-02 23. 6 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:03.42 Nuclide Line Activity Report Flag: "*" = Keyline Page 2792 of 5809 Summary of Nuclide Activity Sample : 1405235032 Acquisition date Page : 2 28-SEP-2016 10:18:25 T9tal number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2793 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235032 Page : 3 Acquisition date : 28-SEP-2016 10:18:25 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 185.52 13 0 1. 80 927.89 920 15 7.44E-03 65.3 5.39E-29 Flags: "T" = Tentatively associated Page 2794 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:05.33 , *******************************************************************************

GEL Labbratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
l DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l *
Acquisition date 28-SEP-2016 10:18:25 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *
Sample date 23-NOV-2015 11:48:00 Nuclide Library : IODINE *
Sample ID I405235032 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.8600E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 * '* Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2795 of 5809 Le (pCi/GRAM 8.854E+00 NOT IDENT. 2.979E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:06.55 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l * *Acquisition date 28-SEP-2016 10:18:25 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *
Sample date 23-NOV-2015 11:48:00 Nuclide Library : IODINE *
Sample ID I405235032 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.8600E+OO GRAM *
Quantity Err(%) 3.4965E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * * * 'Eff. Cal. date 27-JUL-2016 12: 15: 07 Eff'. Geometry : Il29 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7.655E-01 1. 096E+Ol I-129 9.754E-02 3.275E-01 Page 2796 of 5809 TPU ( 1. 96-sigma ) TPU ( 1. 96-sigma) l.097E+Ol 3.305E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2797 of 5809 MDA COUNT$ 4.2076 3.2110 5.4044 5.5038 2.2293 2.2868 ENERGY MDA COUNTS ,ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:26.12 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 11: 53: 00 Acquisition date : 28-SEP-2016 10: 18 :-4 7 Sample ID I405235033 Sample quantity 3.29000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.09 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit. 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND*CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2798 of 5809

"\ VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:26.94 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* 1 j * *
DETECTOR AND S:AMPL_E DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l *
Acquisition date 28-SEP-2016 10:18:47 Sensitivity : 3.000 *
Detector ID XRAY4 -Energy tolerance: 1. 000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *
Sample date 23-NOV-2015 11:53:00 Analyst initials: MJHl *
Sample ID I405235033 Sample Quantity 3.2900E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE. NLB; 1 . * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : Il29 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4'Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 5 :241E-01 1.560E+OO I-129 7.937E-02 1.313E-01 Page 2799 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.979E+OO 4.649E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:25.37 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2800 of 5809 VAX/VMS Nuclide *Identification Report Generated 28-SEP-2016 10:49:26.47 Nuclide Line Activity Report Flag: "*" = Keyline Page 2801 of 5809 Summary of Nuclide Activity Sample ID : 1405235033 Acquisition date Page : 2 28-SEP-2016 10:18:47 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2802 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235033 None Flags: "T" Tentatively associated Page 2803 of 5809 Page : 3 Acquisition date 28-SEP-2016 10:18:47 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:29.21 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l *
Acquisition date 2B-SEP-2016 10:18:47 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *
Sample date 23-NOV-2015 11:53:00 Nuclide Library : IODINE *
Sample ID I405235033 Analyst initials: MJHl * *Batch Number 1598620 Sample Quantity*: 3.2900E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 **
Standard Weight : 0 .. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4' * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2804 of 5809 Le (pCi/GRAM l;852E+00 NOT IDENT. l.559E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-20.16 10: 49: 30. 33 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l * *Acquisition date 28-SEP-2016 10:18:47 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *
Sample date 23-NOV-2015 11:53:00 Nuclide Library : IODINE *
Sample ID I405235033 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.2900E+00 GRAM *
Quantity Err(%) 3.0395E-03 % *
Recovery . 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 . * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid; Please refer to Certificate of Analysis. ----Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 5.241E-01 1. 563E+OO I-129 7.937E-02 l.316E-01 Page 2805 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) l.581E+OO 1.364E-01 NOT IDENT. NOT IDENT.
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2806 of 5809 MDA COUNTS 0.0000 0.0000 1.1221 4.5881 2.3289 1.2005 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:51.59 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 23-NOV-2015 11:20:00 Acquisition date : 28-SEP-2016 10:19:14 Sample ID I405235034 Sample quantity 2.98000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.02 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID : 1598620 Detector SN# : Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.33* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0 0.33 315.00 311 7 3.16E-03 54.5 Flag: "*" = Peak area was modified by background subtraction Page 2807 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:52.44 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l *
Acquisition date 28-SEP-2016 10:19:14 Sensitivity 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
Sample date 23-NOV-2015 11:20:00 Analyst initials: MJHl *
Sample ID I405235034 Sample Quantity 2.9800E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library* : IODINE.NLB;l * ******************************************************************************* ** *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MCA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-:Sigma) I-125 -5.212E+OO 7.694E+OO I-129 O.OOOE+OO l.978E-01 Pag*e 2808 of 5809
MDA (pCi/GRAM MDA (pCi/GRAM l.450E+Ol 2.734E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:50.97 .PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2809 of 5809 Energy 63.33 Area 9 Bkgnd FWHM Channel 0 0.33 315.00 Left 311 Pw Cts/Sec %Err 7 5.00E-03 33.3 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:51.95 Nuclide Line Activity Report Flag: "*" = Keyline Page 2810of5809 Summary of Nuclide Activity Sample ID : 1405235034 Acquisition date Page : 2 28-SEP-2016 10:19:14 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2811of5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235034 Page : 3 Acquisition date : 28-SEP-2016 10:19:14 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 63.33 6 0 0.33 315.00 311 7 3.16E-03 **** 3.19E+OO Flags: "T" = Tentatively associated Page 2812of5809 VAX/VMS Nuclide Ide'ntification Report Generated 28-SEP-2016 10: 49: 54. 28 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* ** * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l *
Acquisition date 28-SEP-2016 10:19:14 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
Sample date 23-NOV-2015 11:20:00 Nuclide Library : IODINE *
Sample ID I405235034 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.9800E+00 GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2813of5809 Le (pCi/GRAM 4.383E+OO NOT IDENT. O.OOOE+OO NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:55.54 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * ** * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l * *Acquisition date 28-SEP-2016 10:19:14 Sensitivity . 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
Sample date 11:20:00 Nuclide Library : IODINE *
Sample ID I405235034 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.9800E+OO GRAM *
Quantity Err(%) 3.3557E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -5.212E+OO 7.748E+OO I-129 O.OOOE+OO O.OOOE+OO Page 2814 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 9 Ei-sigma) 8.097E+OO O.OOOE+OO NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2815of5809 MDA COUNTS 3.2531 0.0000 0.0000 0.9231 0.9543 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:15.90 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road. * * . Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 23-NOV-2015 11:06:00 Acquisition date : 28-SEP-2016 10:19:45 Sample ID I405235035 Sample quantity 2.86000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance : 1.00000 keV Analyst Initials MJHl Abundance limit * : 7 5. 00000 Sensi ti vi ty 3. 00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.28* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 9 0 0.35 315.83 312 7 5.17E-03 37.8 Flag: "*" = Peak area was modified by background subtraction Page 2816of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:16.74 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * .
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l * *Acquisition date 28-SEP-2016 10:19:45 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 23-NOV-2015 11:06:00 Analyst initials: MJHl *
Sample ID I405235035 Sample Quantity 2.8600E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * *******"************************************************************************ * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. .File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 '* ***********************************************T*****T************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert. ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line *Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 3. 969E+OO I-129 5.275E-02 3.929E-01 Page 2817 of5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.488E+OO 9.144E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:15.20 PEAK REPORT WITHOUT BACKGROUND. SUBTRACTION Pk It 1 0 Page 2818of5809 Energy 63.28 Area .Bkgnd FWHM Channel Left Pw Cts/Sec %Err 12 0 0.35 315.83 312 7 6.67E-03 28.9 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:16.26 Nuclide Line Activity Report Flag: "*" = Keyline Page 2819of5809 Summary of Nuclide Activity Sample ID : 1405235035 Acquisition date Page : 2 28-SEP-2016 10:19:45 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2820 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide. specific abn. limit Unidentified Energy Lines Sample ID : I405235035 Page : 3 Acquisition date : 28-SEP-2016 10:19:45 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.28 9 0 0.35 315.83 312 7 5.17E-03 75.6 3.09E+OO Flags: "T" = Tentatively associated Page 2821 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:18.32 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l *
Acquisition date 28-SEP-2016 10:19:45 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 23-NOV-2015 11:06:00 Nuclide Library : IODINE *
Sample ID 1405235035 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.8600E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * **********************'********************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2822 of 5809 Le (pCi/GRAM 0.000E+OO NOT IDENT. 3.240E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:19.52 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l *
Acquisition date 28-SEP-2016 10:19:45 Sensitivity : 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
Sample date 23-NOV-2015 11:06:00 Nuclide Library : IODINE *
Sample ID I405235035 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.8600E+OO GRAM *
Quantity Err(%) 3.4965E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date :. 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO O.OOOE+OO I-129 5.275E-02 3.929E-01 Page 2823 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) O.OOOE+OO 3.936E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2824 of 5809 MDA COUNTS 0.0000 1.4643 0.0000 0.0000 0.7906 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:06.75 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA. GAMMA.ARCHIVE. GAMMA] I405.235036. CNF; 1 Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 -Background date : 25-SEP-2016 12:22:54 Sample date 23-NOV-2015 11:12:00 Acquisition date : 28-SEP-2016 11:17:38 Sample ID I405235036 Sample quantity 2.67000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0/01:00:00.00 Elapsed real time: 0 01:00:00.22 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K *************************************************"******************************* Pk It 1 0 2 0 Energy 32.52 108.45 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 15 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.53 163.19 9 0.21 545.85 157 533 12 4. 22E-03 41.1 16 2.35E-03 82.6 Flag: "*" = Peak area was modified by background subtraction Page 2825 of 5809 .Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:07.53 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l *
Acquisition date 28-SEP-2016 11:17:38 Sensitivity 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.22 Half life ratio : ***** *
Sample date 23-NOV-2015 11:12:00 Analyst initials: MJHl *
Sample ID I405235036 Sample Quantity 2.6700E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 * **Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff .. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il2'9.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -2.077E+OO 4.349E+OO I-129 3.934E-05 l.665E-01 Page 2826 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.270E+OO 3.518E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:06.05 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Er*r Fit 1 0 32.52 15 6 0.53 163.19 157 12 4.22E-03 41.1 2 0 108.45 8 9 0.21 545.85 533 16 2.35E-03 82.6 Page 2827 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:07.11 Nuclide Line Activity Report Flag: "*" = Keyline Page 2828 of 5809 Summary of Nuclide Activity Sample ID : 1405235036 Acquisition date Page : 2 28-SEP-2016 11:17:38 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2829 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235036

Page : 3 Acquisition date : 28-SEP-2016 11:17:38 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 32.52 108.45 15 8 6 0.53 9 0.21 Flags: "T" = Tentatively associated Page 2830 of 5809 163.19 157 12 4.22E-03 82.2 2.28E+Ol 545.85 533 16 2.35E-03 **** 3.47E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:09.17 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOQ: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l * *Acquisition date 28-SEP-2016 11:17:38 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.22 Half life ratio : ***** *
Sample date 23-NOV-2015 11:12:00 Nuclide Library : IODINE *
Sample ID I405235036 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.6700E+OO GRAM *
Recovery 1.00000 Carrier. Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2Q16 11:39:23 Eff. Geometry : I129 *
EfL File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Critical\ Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM Non-Identified Nuclides Nuclide I-125 I-129 Page 2831 of 5809 Le (pCi/GRAM 3.040E+OO l.454E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:10.23 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l *
Acquisition date* 28-SEP-2016 11:17:38 Sensitivity *
Detector ID XRAYl Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.22 Half life ratio : ***** *
Sample date 23-NOV-2015 11:12:00 Nuclide Library : IODINE *
Sample ID I405235036 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.6700E+OO GRAM *
Quantity Err ( % ) 3. 7 453E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM .l ( 1. 96-sigma) I-125 -2.077E+OO 4.365E+OO I-129 3.934E-05 1.665E-01 Page 2832 of 5809 TPU (1. 96-sigma) TPU ( 1. 96-sigma) 4.464E+OO 1 .. 665E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT
ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2833 of 5809 MDA COUNTS 13. 4920 7.6336 7.7906 6.7387 3.6860 4.8449 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:32.74. ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : Z5-SEP-2016 12:22:59 Sample date 30-NOV-2015 11:19:00 Acquisition date : 28-SEP-2016 11:18:01 Sample ID I405235037 Sample quantity 2.84000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.20 0.0% Energy tolerance 1.00000 keV Analyst Initials : 'MJHl Abundance limit 75.00000 Sensitivity : 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.46 10 5 0.50 121. 32 114 10 2.65E-03 55.0 2 4 91. 42 12 3 0.79 456.60 454 14 3. 41E-03 27.3 3.05E+OO 3 4 92.50* 19 2 0.86 462.00 454 14 5.23E-03 33.7 4 0 147.24 9 11 1. 41 736.13 723 15 2.45E-03 89.4 5 0 153.65 13 0 0.33 768.23 763 10 3. 61E-03 27.7 6 0 185.93* 20 0 1.14 929.93 920 18 5.49E-03 29.2 Flag: "*" = Peak area was modified by background subtraction Page 2834 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:33.51 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * : Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l * *Acquisition date 28-SEP-2016 11:18:01 Sensitivity 3.000 *
Detector ID XRAY2 . Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
Sample date 30-NOV-2015 11:19:00 Analyst initials: MJHl *
Sample ID I405235037 Sample Quantity 2.8400E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION ** * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.'CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi(GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-;-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.085E-01 5 .. 704E+OO I-129 -l.442E-02 2.213E-01 Page 2835 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.168E+Ol 4.373E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:32.06 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd

FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.46 10 5 0.50 121. 32 114 10 2.65E-03 55.0 2 4 91. 42 12 3 0.79 456.60 454 14 3.41E-03 27.3 3.05E+OO 3 4 92. 50 35 2 0.86 462.00 454 14 9.84E-03 16.4 4 0 147.24 9 11 1. 41 736.13 723 15 2.45E-03 89.4 5 0 153.65 13 0 0.33 768.23 763 10 3. 61E-03 27.7 6 0 185.93 29 0 1.14 929.93 920 18 8.06E-03 18.6 Page 2836 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:33.06 Nuclide Line Activity Report Flag: "*" = Keyline Page 2837 of 5809 Summary of Nuclide Activity Sample ID : 1405235037 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 11:18:01 Number of lines tentatively identified by **** There are no nuclides meeting summary 6 6 NID 0 criteria 0.00% **** Flags: "K" "E" Page 2838 of 5809 Keyline not found Manually edited "M" = Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235037 Acquisition date : 28-SEP-20lq 11:18:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 24.46 10 5 0.50 121.32 114 10 2.65E-03 **** 2.50E+OO 4 91. 42 12 3 0.79 456.60 454 14 3.41E-03 54.7 7.19E-08 4 92.50 19 2 0. 86 462.00 454 14 5.23E-03 67.5 4.30E-08 0 147.24 9 11 1. 41 736.13 723 15 2.45E-03 **** 3.74E-20 0 153.65 13 0 0.33 768.23 763 10 3.61E-03 55.5 l.28E-21 0 185.93 20 0 1.14 929.93 920 18 5. 49E.:..03 58.5 4.33E-29 Flags: "T" = Tentatively associated Page 2839 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:35.14 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100:[CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l *
Acquisition date 28-SEP-2016 11:18:01 Sensitivity 3.000 * *Detector-ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
Sample date 30-NOV-2015 11:19:00 Nuclide Library : IODINE *
Sample ID I405235037 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.8400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKA100:'[.CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Critical Level Report NOTE: Not all Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuciide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2840 of 5809 Le (pCi/GRAM 4.616E+00 NOT IDENT. l.793E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:36.22 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
* *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l * *Acquisition date 28-SEP-2016 11:18:01 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
Sample date 30-NOV-2015 11:19:00 Nuclide Library*: IODINE *
Sample ID I405235037 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.8400E+00 GRAM *
Quantity Err(%) 3.5211E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 * * .Standard Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry .: I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.085E-01 5.704E+OO I-129 -1.442E-02 2.213E-01 Page 2841of5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.707E+OO 2.214E-01 NOT IDENT. NOT IDENT.
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT *
* * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2842 of 5809 MDA COUNTS 5.2595 7.4924 5.4044 5.5038 5.5733 4.5736 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:14.89 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 30-NOV-2015 10:40:00 Acquisition date : 28-SEP-2016 11:18:47 Sample ID I405235038 Sample quantity 2.82000E+OO GRAM Detector name : XRAY4 Detector geometry: Il29 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.18 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 15.84* 8 8 0.55 78.64 75 17. 2. llE-03 83.5 2.83E+OO 2 4 16.51* 1 7 0.38 82.00 75 17 l.55E-04***** 3 4 17.89 8 5 0.57 88.91 75 17 2.20E-03 51. 7 4 0 31. 71 7 2 0.36 158.14 155 6 l.82E-03 56.0 5 0 92.53* 8 0 0.78 462.94 458 9 2.25E-03 55.6 6 0 132.35 8 3 1. 50 662.49 656 10 2. 31E-03 49.9 Flag: "*" Peak area was modified by background subtraction Page 2843 of 5809 VAX/VMS Nuclide Identification Generated 28-SEP-2016 12:19:15.71 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l *
Acquisition date 28-SEP-2016 11:18:47 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
Sample date 30-NOV-2015 10:40:00 Analyst initials: MJHl *
Sample ID I405235038 Sample Quantity 2.8200E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14 .
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) ----Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.595E-01 2.363E+OO I-129 5.630E-02 l.910E-01 Page 2844 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.306E+OO 4.337E-01 FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:13.98 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err

Fit 1 4 15.84 15 8 0.55 78.64 75 17 4.lOE-03 39.6 *2.83E+OO 2 4 16.51 8 7 0.38 82.00 75 17 2.15E-03 75.6 3 4 17.89 8 5 0.57 88.91 75 17 2.20E-03 51. 7 4 0 31. 71 7 2 0.36 158.14 155 6 1.82E-03 56. 0 5 0 92.53 16 0 0.78 462.94 458 9 4.44E-03 25.0 6 0 132. 35 8 3 1. 50 662.49" 656 10 2. 31E-03 49.9 Page 2845 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:15.25 Nuclide Line Activity Report Flag: "*" = Keyline Page 2846 of 5809 Summary of Nuclide Activity Sample ID : I405235038 Acquisition date Page : 2 28-SEP-2016 11:18:47 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2847of5809 Keyline not found Manually edited . "M" "A" 6 5 NID 1 criteria **** 16.67% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235038 Acquisition date : 28-SEP-2016 11:18:47 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 15.84 8 -8 0.55 78.64 75 17 2. llE-03 **** 1.12E+OO 4 16.51 1 7 0.38 82.00 75 17 1.55E-04 **** 1.48E+OO 4 17.89 8 5 0.57 88.91 75 17 2.20E-03 **** 2.41E+OO 0 31.71 7 2 0.36 158.14 155 6 1.82E-03 **** 1.55E+Ol T 0 92.53 8 0 0.78 462.94 458 9 2.25E-03 **** 5.17E-01 0 132.35 8 3 1. 50 662.49 656 10 2.31E-03 99.9 1. 40E-02 Flags: "T" = Tentatively associated Page 2848 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:17.28 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l * *Acquisition date 28-SEP-2016 11:18:47 Sensitivtty : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: O 01:00:00.18 Half life ratio : ***** *
Sample date 30-NOV-2015 10:40:00 Nuclide Library : IODINE *
Sample ID I405235038 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity :. 2. 8200E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : O. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2849 of 5809 Le (pCi/GRAM 2.273E+OO FAIL ABUN l.722E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:18.35 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l *
Acquisition date 28-SEP-2016 11:18:47 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
Sample date 30-NOV-2015, 10:40:00 Nuclide Library : IODINE *
Sample ID I405235038 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.8200E+OO GRAM *
Quantity Err(%) 3.5461E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff, Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-s igma) Non-Identified Nuclides Nuclide *I-125 I-129 Page 28.50 of 5809 Key-Line Activity (pCi/GRAM 7.595E-01 5.630E-02 K.L Act error ( 1. 96-sigma) 2.367E+OO 1. 911E-01 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 2.391E+OO FAIL ABUN l.928E-01 NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2851 of 5809 MDA COUNTS 1.0858 3.3266 1.4961 2.2941 4.6579 4.8019 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:44.16 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 30-NOV-2015 10:43:00 Acquisition date : 28-SEP-2016 11:19:10 Sample ID I405235039 Sample quantity 3.17000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed .live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.05 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.90* 2 4 0.26 233.18 228 7 4.22E-04268.3 2 0 63.52* 9 3 0.60 315.92 312 9 2.46E-03 57.1 3 *o 92.75* 3 2 1. 01 461.54 456 10 8.74E-04176.9 Flag: "*" = Peak area was modified by background subtraction Page 2852 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:44.99 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 . * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l * *Acquisition date 28-SEP-2016 11:19:10 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *
Sample date 30-NOV-2015 10:43:00 Analyst initials: MJHl *
Sample ID I405235039 Sample Quantity 3.1700E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF.;5
Combined Activity-MDA Report 'NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.840E-01 3.302E+OO I-129 1.378E-02 1;*729E-01 Page 2853 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 8.592E+OO 4.404E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:43.46 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.90 6 4 0.26 233.18 228 7 1.53E-03 70.7 2 0 63.52 15 3 0.60 315.92 312 9 4.30E-03 31. 0 3 0 92.75 18 2 1. 01 461. 54 456 10 4.92E-03 28.9 Page 2854 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:44.52 Nuclide Line Activity Report Flag: "*" = Keyline Page 2855 of 5809 Summary of Nuclide Activity Sample ID : 1405235039 Acquisition date Page : 2 28-SEP-2016 11:19:10 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2856 of 5809 Keyline not found Manually edited "M" "A" 3 3 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235039 Acquisition date : 28-SEP-2016 11:19:10 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.90 2 4 0.26 233.18 228 7 4.22E-04 **** 7.78E+OO 0 63.52 9 3 0.60 315.92 312 9 2.46E-03 **** 3.16E+OO 0 92.75 3 2 1. 01 4 61. 54 456 10 8.74E-04 **** 3.55E-01 Flags: "T" = Tentatively associated Page 2857 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:46.90 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l *
Acquisition date 28-SEP-2016 11:19:10 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *
Sample date 30-NOV-2015 10:43:00 Nuclide Library : IODINE *
Sample ID I405235039 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 3.1700E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2858 of 5809 Le .(pCi/GRAM 3.054E+00 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:47.99 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR*AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l *
Acquisition date 28-SEP-2016 11:19:10 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: O 01:00:00.05 Half life ratio : ***** *
Sample date 30-NOV-2015 10:43:00 Nuclide Library : IODINE *
Sample ID I405235039 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.1700E+OO GRAM *
Quantity Err(%) 3.1546E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
E£f. Cal. date 30-AUG-2016 l1:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.840E-01 3.303E+OO I--:129 1.378E-02 1. 729E-01 Page 2859 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.307E+OO 1. 731E-01 NOT IDENT. NOT IDENT.
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2860 of 5809
MDA COUNTS 1.6265 1. 7094 0.0000 1. 8461 3.8174 1.0189 'ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:21.94 *******************************************************************.*************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Configuration Background file Background date : 75-SEP-2016 12:23:20 Sample date 30-NOV-2015 13:23:00 Acquisition date : 28-SEP-2016 11:19:53 Sample ID 1405235040 Sample quantity 3.54000E+00 GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K . LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.27* *BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 3 2 0.54 315.77 312 7 8. 07E-04131. 4 Flag: "*" = Peak area was modified by background subtraction Page 2861 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:22.76 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration .. DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l *
Acquisition date 11:19:53 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 . Half life ratio : ***** *
Sample date 30-NOV-2.015 13: 23: 00 Analyst initials: MJHl *
Sample ID I405235040 Sample Quantity 3.5400E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNFf5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclidesri are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.535E-01 1.477E+OO I-129 -7.671E-02 1. 793E-01 Page 2862 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.546E+OO 2.928E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:21.14 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 63.27 8 2 0.54 315.77 312 7 2.31E-03 43.5 2 0 92. 65 6 3 *0.19 462.75 458 7 1.70E-03 63.6 Pa,ge 2863 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:22.32 Nuclide Line Activity Report Flag: "*" = Keyline Page 2864 of 5809 Summary of Nuclide Activity Sample ID : 1405235040 Acquisition date Page : 2 28-SEP-2016 11:19:53 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" Keyline not found "E" = Manually edited Page 2865 of 5809 "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235040 Page : 3 Acquisition date : 28-SEP-2016 11:19:53 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 63.27 3 2 0.54 315.77 312 7 8.07E-04 **** 3.09E+OO Flags: "T" = Tentatively associated Page 2866 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:24.89 **********************"*********************************************************

GEL Laboratories LLC *
2040 Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Config_uration DKAlOO: [CANBERRA. GAMMA.ARCHIVE. GAMMA] I405235040. CNF; 1 *
Acquisition date 28-SEP-2016 11:19:53 Sensitivity 3.000 *
Detector ID XRAY6 Energy tolerance: 1.000 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
Sample date 30-NOV-2015 13:23:00 Nuclide Library : IODINE *
Sample ID I405235040 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 3.5400E+00 GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. File' : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2867 of 5809 Le (pCi/GRAM 1.753E+OO NOT IDENT. 9.254E-02 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:26.03 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l * *Acquisition date 28-SEP-2016 11:19:53 Sensitivity 3.000 *
Detector ID *XRAY6 Energy tolerance: 1.000 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
Sample date 30-NOV-2015 13:23:00 Nuclide Library : IODINE *
Sample ID I405235040 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.5400E+OO GRAM *
Quantity Err(%) 2.8249E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 0000.0 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
Eff. Pile : DKA100: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.535E-01 1..478E+OO I-129 -7. 671E-02 1. 795E-01 Page 2868 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 1.517E+OO 1.828E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29.62 35.49 39.58 Page 2869 of 5809 .MDA COUNTS 0.0000 2.9286 l. 4921 0.0000 1.5811 3.3136 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:24.89 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627437.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415
Background date : 25-SEP-2016 12:22:54 Sample date 26-SEP-2016 00:00:00 Acquisition date : 12:50:58 Sample ID I1203627437 Sample quantity 3.54000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:40:07.21 Elapsed real time: 0 00:40:07.36 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found / Page 2870 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:25.77 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627437.CNF;l *
Acquisition date 28-SEP-2016 12:50:58 Sensitivity 3.000 *
Detector ID XRAYl Energy toleran.ce: 1. 000 * *Elapsed live time: 0 00:40:07.21 Abundance limit : 75.000 *
Elapsed real time: 0 00:40:07.36 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *
Sample ID I1203627437 Sample Quantity 3.5400E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6'
Combined Activity-MDA NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides ----Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 9 6-sigma) I-125 2.094E-02 l.050E-01 I-129 4.719E-02 1. 896E-01 Page 2871 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.142E-01 4.177E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:24.23 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2872 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:25.31 Nuclide Line Activity Report Flag: "*" = Keyline Page 2873 of_5809 Summary of Nuclide Activity Sample ID : 11203627437 Acquisition date Page : 2 28-SEP-2016 12:50:58 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2874 of 5809 Keyline not found Manually edited-"M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627437 None Flags: "T" Tentatively associated Page 2875 of 5809 Acquisition date Page : 3 28-SEP-2016 12:50:58 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:27.29 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627437.CNF;l *
Acquisition date 28-SEP-2016 12:50:58 Sensitivity 3.000 *
Detector ID XRAYl Energy tolera*nce: 1. 000 *
ElaRsed live time: 0 00:40:07.21 Abundance limit : 75.000 *
Elapsed real time: 0 00:40:07.36 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID I1203627437 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 3.5400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2876 of 5809 Le (pCi/GRAM 8.853E-02 NOT l.744E-01 NOT IDENT.

VAX/VMS Nuclide Identification *Report Generated 28-SEP-2016 13:32:28.31 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627437.CNF;l *
Acquisition date 28-SEP-2016 12:50:58 Sensitivity : 3.000 *
Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 00:40:07.21 Abundance limit : 75.000 *
Elapsed real time: 0 00:40:07.36 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID I1203627437 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.5400E+00 GRAM *
Quantity Err(%) 2.8249E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.094E-02 l.051E-01 I-129 4.719E-02 1. 897E-01 Page 2877 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) l.055E-01 1.909E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2878 of 5809 MDA COUNTS 6.1327 6.7854 4.3281 1.7970 1.8430 10.6588 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:00.80 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627438.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Configuration Bac_kground file Background date : 25-SEP-2016 12:22:59 Sample date 8-DEC-2015 14:17:00. Acquisition date : 28-SEP-2016 12:51:32 Sample ID Il203627438 Sample quantity 3.35000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:39:28.38 Elapsed real time: 0 00:39:28.53 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 92.71* 96.42 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 10 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.94 463.05 3 0.37 481.65 457 11 4.25E-03 48.5 474 12 3.40E-03 55.6 Flag: "*" = Peak area was modified by background subtraction Page 2879 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:01.59 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627438.CNF;l *
Acquisition date 28-SEP-2016 12:51:32 Sensitivity* 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:39:28.38 Abundance limit : 75.000 *
Elapsed real time: 0 00:39:28.53 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Analyst initials: MJHl *
Sample ID I1203627438 Sample Quantity 3.3500E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard .Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]'EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide* (pCi/GRAM (1.96-sigma) I-125 3.393E+OO 7.155E+00 I-129 2.433E-01 2.666E-01 Page 2880 of 5809 MDA (pCi/GRAM MDA (pCi-/GRAM 1.631E+Ol 6.452E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:00.10 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 92. 71 21 0 0.94 463.05 457 11 8.87E-03 21. 8 2 0 96.42 8 3 0.37 481. 65 474 12 3.40E-03 55.6 Page 2881 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:01.13 Nuclide Line Activity Report Flag: "*" = Keyline Page 2882 of 5809 Summary of Nuclide Activity Sample ID : 11203627438 Acquisition date Page : 2 28-SEP-2016 12:51:32 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2883 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 11203627438 Acquisition date : 28-SEP-2016 12:51:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.71 10 0 0.94 463.05 457 11 4.25E-03 97.0 3.89E-08 0 96. 42 8 3 0.37 481. 65 474 12 3.40E-03 **** 6.49E-09 Flags: "T" Tentatively associated Page 2884 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:03.06 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627438.CNF;l * *Acquisition date 28-SEP-2016 12:51:32 Sensitivity 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:39:28.38 Abundance limit : 75.000 *
Elapsed real time: 0 00:39:28.53 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
Sample ID I1203627438 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 3.3500E+00 GRAM *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-0UL-2016 12:15:07 Eff. Geometry : *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2885 of 5809 Le (pCi/GRAM 6.719E+OO NOT IDENT. 2.719E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:04.39 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC *29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627438.CNF;l *
Acquisition date 28-SEP-2016 12:51:32 Sensitivity : 3.000 *
Detector ID XRAY2 Energy tolerance: 1.000 *
Elapsed live time: 0 00:39:28.38 Abundance limit : 75.000 *
Elapsed real time: 0 00:39:28.53 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
Sample ID . I1203627438 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.3500E+OO GRAM *
Quantity Err(%) 2.9851E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM ) Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.393E+OO 7.180E+OO I-129 2.433E-01 2.677E-01 Page 2886 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 7.341E+OO 2.893E-01 NOT IDENT. NOT IDENT.
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2887 of 5809 MDA COUNTS 4.2076 3. 2110 5.4044 7.7053 7.8027 4.5736 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:36.22 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627439.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 75-SEP-2016 12:23:10 Sample date 8-DEC-2015 14:17:00. Acquisition date : 28-SEP-2016 12:52:05 Sample ID Il203627439 Sample quantity 2.94000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:38:50.89 Elapsed real time: 0 00:38:51.04 0.0% Energy tolerance keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID * . 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 27.00 10 22 0.63 134.54 127 32 4.35E-03 77.9 1. 74E+OO 2 4 27.78 19 18 0.53 138.46 127 32 7.98E-03 45.3 3 4 28.69 11 14 0.44 143.00 127 32 4.92E-03 81.1 4 4 29.70 247 13 0.65 148.09 127 32 l.06E-01 7.1 5 0 33.60 23 27 0.36 167. 62 164 8 1. OOE-02 43.2 6 0 39.65 29 9 0.75 197.94 193 9 1.25E-02 26.2 Flag: "*" = Peak area was modified by background subtraction Page 2888 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:37.06 *******************************************************************************
GEL Laboratories LLC *
2040 Savage *Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627439.CNF;l *
Acquisition date 28-SEP-2016 12:52:05 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:50.89 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:51.04 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Analyst initials: MJHl *
Sample ID 11203627439 Sample Quantity 2.9400E+00 GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Librari : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION ** * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Activity (pCi/GRAM 9.138E+OO 1.203E+Ol *cnt uncert ( 1. 96-sigma) 1.395E+Ol 1. 679E+OO Non-Identified Nuclides Nuclide Page 2889 of 5809 Key-Line Activity (pCi/GRAM K.L. Cnt Uncert ( 1. 9 6-s igr:na) MDA (pCi/GRAM 1.362E+Ol 7.659E-01 MDA (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13 : 31 : 3 5 ,. 4 9 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd
FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 27.00 10 22 0.63 134.54 127 32 4.35E-03 77.9 1.74E+OO 2 4 27.78 19 18 0.53 138.46 127 32 7.98E-03 45.3 3 4 28.69 11 14 0.44 143.00 127 32 4.92E-03 81.1 4 4 29.70 247 13 0.65 148.09 127 32 1.06E-01 7.1 5 0 33.60 23 27 0.36 167. 62 164 8 1. OOE-02 43.2 6 0 39.65 29 9 0.75 197.94 193 9 1.25E-02 26. 2 Page 2890 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:36.58 Nuclide Line Activity Report Nuclide Type: Nuclide I-125 Ene:r;:gy 27.34 30.97 35.49 Nuclide Type: Nuclide I-129 Flag: "*" Page 2891 of 5809 Energy 29.62 33.59 39.58 Keyline Area 10 Area 247 23 29 %Abn 114.10* 20.30 6.68 %Abn 56.60* 10.04 7.51 %Eff 1.19BE+Ol l.514E+Ol l.660E+Ol %Eff l.431E+Ol 1.626E+Ol 1.617E+Ol Uncorrected Decay Corr pCi/GRAM pCi/GRAM 2.925E-01 9.138E+OO ------Line Not Found ------Line Not Found Uncorrected pCi/GRAM 1.203E+Ol 5.644E+OO 9.467E+OO Decay Corr pCi/GRAM 1.203E+Ol 5.644E+OO 9.467E+OO 2-Sigma %Error 155.83 2-Sigma %Error 14.24 86.43 52.35 Summary of Nuclide Activity Sample ID : I1203627439 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 12:52:05 Number of lines *tentatively identified by NID 6 2 4 66.67% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi7GRAM 2-Sigma Error %Error Flags I-125 59.40D 31.2 2. 92.5E-01 9 .138E+OO 14.24E+OO 155.83 ------------------Total Activity 2.925E-01 9 .138E+OO Nuclide Type : FISSION . Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags I-129 l.57E+07Y 1. 00 1.203E+Ol 1.203E+Ol 0 .171E+Ol 14.24 ------------------Total Activity 1. 203E+Ol 1.203E+Ol Grand Total Activity 1.232E+Ol 2 .117E+Ol Flags: "K" Key line not found "M" Manually accepted "E" Manually edited "A" Nuclide specific abn. limit Page 2892 of 5809 Unidentified Energy Lines *Page : 3 Sample ID : Il203627439 Acquisition date : 28-SEP-2016 12:52:05 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 27.78 19 18 0.53 138.46 127 32 7.98E-03 90.6 1.27E+Ol 4 28.69 11 14 0.44 143.00 127 32 4.92E-03 **** 1. 35E+Ol Flags: "T" = Tentatively associated Page 2893 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:38.97 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627439.CNF;l *
Acquisition date 28-SEP-2016 12:52:05 Sensitivity 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:50.89 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:51.04 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
Sample ID I1203627439 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 2.9400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 I129'.CNF;14
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Le (pCi/GRAM 5.626E+oo* 3.169E-01 ----Non-Identified Nuclides Nuclide Page 2894 of 5_809 Le (pCi/GRAM VAX/VMS Nuclide Identification Report 28-SEP-2016 13:31:40.16 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627439.CNF;l *
Acquisition date 28-SEP-2016 12:52:05 Sensitivity : 3.000 *
Detector ID XRAY4 Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:50.89 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:51.04 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
Sample ID I1203627439 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 2.9400E+00 GRAM *
Quantity Err(%) 3.4014E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
Eff. File DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 I-129 9 .138E+OO 1.203E+Ol Act Error (1. 96-:-sigma) l.407E+Ol 2.057E+OO Non-Identified Nuclides Nuclide Page 2895 of 5809 Key-Line Activity (pCi/GRAM K.L Act error ( 1. 96-sigma) TPU ( 1. 96-sigma) 1. 407E+Ol 2.057E+OO TPU ( 1. 96-sigma)
- - - - * * *
GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2896 of 5809 MDA COUNTS 7.6004 7.7622 7.8547 17.2054 12.8092 7.2029 ENERGY MDA COUNTS ENERGY MDA*COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:10.80 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627440.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 12:52:43 Sample ID Il203627440 Sample quantity 3.54000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:38:05.93 Elapsed real time: 0 00:38:05.98 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID : 1598620 Detector SN# : Matrix Spike ID : .1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 6 27.21 14 0 0.57 135.07 129 25 6.34E-03 35.9 2.22E+OO 2 6 29.70 198 0 0.61 147.48 129 25 8.66E-02 7.4 3 0 32.46 8 3 0.55 161. 23 157 7 3.34E-03 54.2 4 0 33.67 27 16 0.53 167.29 164 8 1.18E-02 31. 3 5 0 39.64 38 5 0.58 196. 99 192 10 l.68E-02 19.4 6 0 76.98* 4 0 0.58 383.00 380 6 1.87E-03 59.8 Flag: "**" = Peak area was modified by background subtraction Page 2897 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:11.78 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627440.CNF;l *
Acquisition date 28-SEP-2016 12:52:43 Sensitivity 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:05.93 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:05.98 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *
Sample ID I1203627440 Sample Quantity 3.5400E+OO GRAM *
Batch Number 1598620 Carrier Weight 0.00000 *
Recovery 1.00000 Standard Weight 0.00000 *
Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Activity (pCi/GRAM 5.681E-01 1.320E+Ol Cnt uncert ( 1. 96-sigma) 3.992E-01 1.907E+OO Non-Identified Nuclides Nuclide Page 2898 of 5809 Key-Line Activity (pCi/GRAM K.L. Cnt Uncert ( 1. 96-sigma) MDA (pCi/GRAM . 2. 681E-01 4.688E-01 MDA * (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:09.99 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 6 27.21 14 0 0.57 135.07 129 25 6.34E-03 35.9 2.22E+OO 2 6 29.70 198 0 0.61 147.48 129 25 8.66E-02 7.4 3 0 32.46 8 3 0.55 161.23 157 7 3.34E-03 54.2 4 0 33.67 27 16 0.53 167.29 164 8 1.18E-02 31. 3 5 0 39.64 38 5 0.58 196. 99 192 10 1. 68E-02 19.4 6 0 76.98 6 0 0.58 383.00 380 6 2.62E-03 40.8 Page 2899 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:11.25 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pC:i/GRAM) pCi/GRAM %Error I-125 27.34 14 114 .10* 7.693E+OO 5.514E-01 5.681E-01 71.71 30.97 ------20.30 9.289E+OO ------Line Not Found ------35.49 ------6.68 9.988E+OO ------Line Not Found ------Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 198 56.60* 8. 851E+OO 1.320E+Ol 1.320E+Ol 14.75 33.59 27 10.04 9.860E+OO 9.070E+OO 9.070E+OO 62.69 39.58 38 7.51 9.649E+OO 1. 769E+Ol 1. 769E+Ol 38.83 Flag: "*" Keyli_ne Page 2900 of 5809 Summary of Nuclide Activity Sample ID : I1203627440 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 12:52:43 Number of lines tentatively identified by NID 6 2 4 66.67% Nuclide Type : Nuclide I-125 Hlife 59.40D Decay 1. 03 Total Activity Nuclide Type : FISSION Nuclide Hlife I-129 . l.57E+07Y Decay 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 5.514E-01 ---------5.514E-01 Uncorrected pCi/GRAM 1.320E+Ol ---------1.320E+Ol 1.375E+Ol Flags: "K" "E" Keyline not fouhd Manually edited Page 2901of5809 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 5. 681E-01 4.073E-01 71. 71 ---------5. 681E-01 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 1.320E+Ol 0.195E+Ol 14.75 ---------1.320E+Ol 1. 3.76E+Ol Manually accepted "M" "A" Nuclide specific abn. limit Flags Flags Unidentified Energy Lines Sample ID : 11203627440 Page : 3 Acquisition date : 28-SEP-2016 12:52:43 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 32.46 76.98 8 4 3 0.55 0 0.58 Flags: "T" Tentatively associated Page 2902 of 5809 161.23 157 7 3.34E-03 **** 9.66E+00 383.00 380 6 1.87E-03 **** 1.22E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:14.03 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * ; ' ' .. DETECTOR AND' SAMPLE DATA *
* *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627440.CNF;l *
Acquisition date 28-SEP-2016 12:52:43 Sensitivity 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:05.93 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:05.98 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID 11203627440 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity : 3.5400E+OO GRAM *
Recovery 1.00000 Carrier Weight : 0.00000 *
Standard Weight : 0. 00000 * **************************fa**************************************************** * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 'Il29.CNF;5
Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Le (pCi/GRAM 8.148E-02 1.438E-01 Non-Identified Nuclides Nuclide Page 2903 of 5809 Le (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:15.78 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627440.CNF;l *
Acquisition date 28-SEP-2016 12:52:43 Sensitivity : 3.000 *
Detector ID XRAY5 Energy tolerance: 1.000 *
Elapsed live time: 0 00:38:05.93 Abundance limit : 75.000 *
Elapsed real time: 0 00:38:05.98 Half life ratio : ***** *
Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
Sample ID Il203627440 Analyst initials: MJHl *
Batch Number 1598620 Sample Quantity 3.5400E+OO GRAM *
Quantity Err(%) 2.8249E-03 % *
Recovery 1.00000 Carrier Weight 0.00000 *
Standard Weight : 0. 00000 * ******************************************************************************** * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 I-129 5.681E-01 l.320E+Ol Act Error ( 1. 96-sigma) 4.125E-01 2. 311E+OO Non-Identified Nuclides Nuclide Page 2904 of 5809 Key-Line Activity (pCi/GRAM K.L Act error ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.125E-01 2. 311E+OO TPU ( 1. 96-sigma)
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************** ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2905 of 5809 MDA COUNTS 0.8133 0.8547 0.0000 7.3846 6.6804 1.0189 ENERGY )YlDA COUNTS ENERGY MDA COUNTS Effective 3/2512010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 10/03/16 1596247 Batch# _________ _ Gamma Solid MJWC Product: ________ _ Criteria: Yes Sample Solids are less than or equal to 100 mq for GAB. samples have been blank corrected (if required). Blank correction reoorted included Clf reouired). If activity less than 10x MDA/MDC, error is less Date: 10/03/16 No Comments n/a n/a than or equal to 1SO% of sample activity. ./ If greater than 10* MDA/ MDC, error Is 400/o or less. If b!ll2w U!!l MQAL MD!;, 1:rr2t l!i 21rn!t. Instrument source check is within limits. Instrument bka check is within limits. ./ Method RDL/ LLD has been met. ./ If duolicate activities are: Less than 5* MDA/ MDC, then RPO is 100% or less, . see narrative If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO is 0%, ./ Or meets the client's required RER acceotance criteria. Tracer yield is 15-125%
Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). In'" Method blank is less than the RDL/ LLD. ./ (If rad !lilDml!:lio S :Z0lq I!( 12W!:5t Samole was run within hold time. ./ DER 1563869 Samnle was correctlv nreserved If reauired. ./ Smears Taken far Radioactive batches. n/a Method Spike and LCS are within 75-125% ./ or meets the client's contract a"centan"e criterin\, Na blank spaces on data forms. ./ All line outs initialed and dated. i1'2DiJcgat Aux data Is correct. ./ Client Sneclal reouirements oane has been checked. ./ R"W Data and I or sncctrum are included and nronerlv statused. J MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ./ 1 ..... *-* .. (ff ./ lla.Wumteoul.lnm..Casi: tlarrat1**-./ Batch Data Excentlon Reoorts CDERl comoleted if aonllcable. ,/ DER 1563869 Batch Data Exception Reports (DER) second reviewed. ,/ Disoosltion verified to be comoleted. /\liouot Correction comaleted If renulred, n/a Review sample historlcal results If available ./ (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l Primary Review Porformed 3_( _I h ___ _ Secondary Review Performed ... *** .* ;t-I I b Page 2906 of 5809 GL-CHL-RAD-013 Rev 1 Page 1of1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 03-0CT-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1596247 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE HASL 300, 4.5.2.3/Ga-01-R Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1563869 Revision No.: Type: Process Client Code: MJWC Samples 405235 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, Samples were analyzed in a timely manner upon receipt. Reporting 012, 013, 014, 015, 016, 017, 018, 019, 020, and 1203621351 (duplicate) results. were received outside of the holding period. Originator's Name: Data Validator/Group Leader: Spencer Collins 03-0CT-16 Michael Hilton 03-0CT-16 Page 1

Page 2907 of 5809 Gamma Spec Queue Sheet Batch #:1596247 Analyst: MXRl First Client DueDate:l 0/04/2016 Internal Due Date: 09/30/2016 Gamma LCS Isotope: Mixec_l Gamma LCS Code: IS 51a Expiration Date: 4 j 1 \ 31 Vol: t-0 ....
_* __ _ Prep Date:_Cf......,) ....... 12-___,_/ l..,_(o __ _ Library: 'b-DC...J Balance ID: N ) A-Sample JD Client Description I Contain 405235001-1 4.1.B.R.l.2 405235002-1 4.1. B. R.1.3 405235003-1 4.1.B.R.1.4 4052350-04-1 4.1.B.R.7.2 4052350-05-1 4.1.C.R.1.3 405235006-1 4.1.C.R.l.4 405235007-1 4.l.C.R.2.3 405235008-1 4. t.C.R.2.4 4052350-09-1 4.l.D.R.1.3 405235010-1 4.1.D.R.l.4 405235011-1 4.1.D.R.3.2 405235012-1 4.1.D.R.2.4 405235013-1 4.2A.R.2.3 405235014-1 4.2A.R.l.3 405235015-1 4.2A.R.1.4 405235016-1 4.2A.R.2.4 405235017-1 4.2A.R.3.2 405235018-1 4.2A.R.4.2 405235019-1 4.2B.R.2.4 405235020..f 4.2B.R1.4 1203621350-1 MB 1203621351-1 DUP 4.l.B.R.1.2(405235001) 1203621352-1 LCS er ID GEL Laboratories LLC, Radiochemistry Division Type SAl\:IPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAJ\:IPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAl\:IPLE MB DUP LCS Hazard Code Client MJWCOOI MJWCOOl l\fJWCOOl MJWCOOl MJWCOOI MJWCOOl MJWCOOl MJWCO-OI MJWCOOl MJWCO-Ol MJWCOOl MJWCOOl MJWCOOJ MJWCOOI MJWCOO! MJWCOOl MJWCOOI MJWCOOl MJWCOOI MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOU1T Matrix Collect Date SOIL IO-DEC-15 14:20:00 tl\q_ SOIL 10-DEC-15 14:30:00\2.f SOIL IO-DEC-15 14:35:00 SOIL 09-DEC-1514:00:00 ) SOIL 10-DEC-15 13:15:0:m SOIL 10-DEC-1513:25:00 l :--SOIL 10-DEC-15 13:55:00 l1Z.t-SOIL SOIL 10-DEC-15 10:30:0l\-1:f: SOIL SOIL 09-DEC-15 10:13:00 f1.f SOIL l SOIL SOIL 08-DEC-15 10:49:00 ;.. SOIL 08-DEC-15 10:56:00 1 SOIL 08-DEC-15 11:29:00 fl.¥' SOIL 02-DEC-15 1.0:02:00{Lp-SOIL 02-DEC-15 10:19:00 SOIL 08-DEC-t< 14'JO"IO SOIL 08-DEC-15 SOIL q!1'L-/1v *_ SOIL 10-DEC-15 14:20:oolt . I SOIL q lrz.,j1h Wet Ar {:fa Geometry (I ) Detector CAN I 141.921 g 2-. 123.837 g I .3c'i I 140.486 g '8" 148.94 g l 't I 157.331 g l9 I 156.342 g Zaj I 152.523 g '32.. 147.889 g Jq 134.381 g 'LS I 141.695 g I 'Z...<6 146.502 g 'S)I 154.64 g 144.574 g I L\l J I I 153.732 g I 431 145.075 g L{tfi I 163.118 g I n. I 148.561 g I le ' 155.815 g ' 1.71 I 175.975 g \\ 170.763 g l -3\ I .1 I ' {, I 09/16/2016 Sealing Dateffime (if Applicable) lf I 11--lllo I ! . ' ' --Data Reviewed By: te-'5-/b Page 1 of 1 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:57:39.80 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA.]G405235001.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Z-OCT-2016 11:00:01. Sample date : 10-DEC-2015 14:20:00 Acquisition date : 3-0CT-2016 07:56:53. Sample ID : G405235001 Sample quantity : 1.41921E+02 GRAM Detector name : GAM02 Detector geometry: CAN Elapsed live time: a Ol:OD:00.00 Elapsed real time: 0 01:00:00.40 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596247 netector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 3 3 3 4 0 5 0 6 0 7 0 8 0 9 6 Energy 62.77* 74.90* 77.10 92.82* 112. 23* 143.48* 186.02* 208.83 238.54* 241.94 270.65 295.25 338.34*

351.68* 382.01 464.18 510.86* 546.32 548.66 583.19* 609.14* 658.58 661.37 717.42 726.67 755.24 769.00 795.57 808.56 812.22 911.29* 964.76* 969.00* 10 6 11 0 12 0 13 0. 14 0 15 0 16 0 17 0 18 1 19 1 20 0 21 0 22 4 23 4 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 1 33 1 34 0 1023.46 Page 2909 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 30 134 214 107 12 10 77 67 414 115 84 153 102 258 14 18 54 22 18 145 183 16 174 13 33 14 24 28 14 6 79 26 49 12 Bkgnd FWHM Channel Left .Pw Cts/Sec %Err 156 219 173 266 140 140 141 162 71 81 95 83 48 72 39 44 54 18 28 28 49 20 30 19 15 25 40 17 20 12 11 1 5 15 0.99 1.19 1. 25 1. 47 1. 42 1.27 1.10 2. 65 1. 26 2.10 3.65. 1.10 1. 41 1. 53 2.94 0.60 2.48 1. 84 1. 67 1. 34 1. 35 1. 94 1. 79 3.43 1. 28 1. 36 0.88 1. 37 1.21 1. 07 1. 64 2.17 2.17 4.60 125.05 149.28 153.69 185.10 223.88 286.32 371.32 416.92 476.29 483.07 540.43 589.60 675. 71 702.37 7 62. 98 927.18 1020.46 1091.33 1096. 00 1165. 01 1216.87 1315. 69 1321.26 1433.28 1451. 7 5 1508.86 1536.36 1589.45 1615.42 1622.73 1820.74 1927.61 1936.08 2044.92 122 146 146 180 223 283 366 411 471 471 533 585 671 696 756 918 1015 1088 1088 1159 1210 1312 1312 1429 1448 1502 1527 1582 1608 1618 1815 1922 1922 2036 8 8.25E-03 79.1 16 3.72E-02 19.9 16 5.95E-02 13.0 12 2.97E-02 34.l 8 3.36E-03174.4 8 2.92E-03203.7 11 2.13E-02 34.6 13 l.86E-02* 41.0 18 1.15E-01 6.1 18 3.20E-02 19.7 14 2.34E-02 26.8 10 4.26E-02 13.7 10 2.83E-02 16.4 12 7.17E-02 9.2 9 3.79E-03 79.9 13 5.13E-03 78.4 15 37 .4 18 6.19E-03 35.8 18 5.09E-03 58.2 13 4. 04E-02 11. 5 15 5.08E-02 11.4 17 4.55E-03 56.*0 17 4.82E-02 9.5 12 3.65E-03 70.7 8 9.04E-03 27.5 10 3.91E-03 71.6 12 6.74E-03 55.5 15 7.65E"-03 41.3 11 3.75E-03 71.6 9 1.80E-03101.7 11 2.20E-02 14.4 21 7.22E-03 27.6 21 1.36E-02 18.2 15 3.33E-03 76.0 Fit 2.23E+OO l.54E+OO 2.69E+OO 6.25E+OO 6.57E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1099.87 16 18 0.80 2197.65 2188 14 4.35E-03 66.3 36 0 1120.14* 42 12 1. 94 2238.17 2233 15 1. 17E-02 24.3 37 0 1130 .15 18 6 3.23 2258.17 2252 12 5.00E-03 36. 0 38 0 1154. 59 26 10 2.10 2307.01 2300 14 7.16E-03 33.1 39 2 1186.65 15 8 2.55 2371. 09 2361 26 4.09E-03 62.7 1.04E+OO 40 2 1191. 84 14 17 2.55 2381. 47 2361 26 4.0lE-03 52.9 41 0 1195. 72 9 7 1. 37 2389.22 2386 7 2.50E-03 59.1 42 0 1222.52 15 8 1. 55 2442.79 2438 10 4.24E-03 42.3 43 0 1228.78 14 5 2.06 2455.30 2451 9 3. 96E-03 37.8 44 0 1252.82 23 3 *3.01 2503.34 2498 12 6.31E-03 26.0 45 0 1282.31 24 4 5.42 2562.30 2555 16 6.59E-03 28.0 46 0 1325. 72 13 0 2.73 2649.08 2644 12 3. 61E-03 27.7 47 0 1378.42* 14 7 1.11 2754.41 2750 10 3. 91E-03 47.3 48 0 1460.66* 375 8 1. 79 2918.80 2910 15 1.04E-01 5.5 49 0 1729.65* 7 2 0.69 3456.50 3450 11 1. 90E-03 63.9 50 0 1764.48* 33 0 2.63 3526.12 3520 13 9.15E-03 19.8 Flag: "*" = Peak area was modified by background subtraction Page 2910of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:57:42 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl . Sample title Sample date 10-DEC-2015 14:20:00 Acquisition date : 3-0CT-2016 07:56:53 Sample ID G405235001 Sample qu,anti ty 141. 92 GRAM Sample. type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID Sample geometry : GAMMA2 Detector -geometry: 0 01:00:00.00 Elapsed real time: 1.50 keV Half life ratio No Linear 75.00 Systematic Error J;:fficienc:j..es at Interference Report Interfering Interfered Nuclide Line Nuclide Line PB-214 242.00 RA-224 240.99 PB-214 74.82 AM-243 74.66 PB-214 74.82 TH-228 74.82 PB-214 74.82 PB-212 74.82 PB-214 351.93 BI-211 351.06 Page 2911 of 5809 CAN 0 01:00:00.40 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.059E+OO 1.685E+Ol 1.685E+Ol 10.98 OK C0-58 810.76 99.45* 1. 711E+OO 2.038E-02 3. 7 51E-01 203.37 OK BA-137M 661. 66 89.90* 2.016E+OO 5.224E-01 5.323E-01 18.94 OK CS-137 661. 66 85.10* 2.016E+OO 5.519E-01 5.624E-01 18.94 OK TL-208 277.37 6.60 4.173E+OO Line Not Found Absent 583.19 85.00* 2.233E+OO 4.222E-01 4.222E-01 23.00 OK 860.56 12.50 1.634E+OO Line Not Found Absent PB-212 74.82 10.28 3.783E+OO 1.545E+OO 1.545E+OO 59.01 OK 77 .11 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25. 96 OK 238.63 43.60* 4.702E+OO 1.200E+OO 1.200E+OO 12.25 OK 300.09 3.30 3.910E+OO Line Not Found Absent BI-214 609.32 45.49* 2.155E+OO 1.025E+OO 1.026E+OO 22.80 OK 1120.29 14.92 1.323E+OO 1.112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 1.201E+OO l.202E+00 39.68 OK PB-214 74.82 5.80 3.775E+OO Line Not Found <<INT Reject 77 .11 9.70 4.000E+OO 3.579E+00 3.580E+OO 25.96 OK 87.09 3.41 4.837E+OO Line Not Found Absent 242.00 7.25 4.651E+OO Line Not Found <<INT Reject 295.22 18'. 42 3.963E+OO 1.226E+OO 1.226E+OO 27.45 OK 351. 93 35.60* 3.418E+00 1.221E+OO 1.221E+OO 18.38 OK RN-222 609.32 45.49* 2.155E+OO l.025E+00 l.026E+00 22.80 OK 1120.29 14.92 1.323E+OO 1.112E+OO 1.112E+00 48.51 OK 1764.49 15.30 8.931E-01 1.201E+OO 1.202E+OO 39.68 OK RA-224 240.99 4.10* 4.652E+OO 1.414E+OO 1.414E+OO 108.39 OK RA-226 609.32 45.49* 2.155E+OO 1.025E+OO 1.026E+OO 22.80 OK 1120. 29 14.92 1.323E+OO 1.112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 1.201E+OO 1.202E+OO 39.68 OK AC-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO l.479E+OO l.479E+00 32.75 OK 794.95 4.25 1. 739E+OO 1.999E+OO 1.999E+OO 82.62 OK 835.71 1. 61 1.672E+OO -----Line Not Found Absent 911.20 25.80* 1.561E+OO 1.041E+OO 1. 041E+OO 28.80 OK 968.97 15.80 l.487E+OO 1.lOOE+OO l.lOOE+OO 36.32 OK RA-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO 1.479E+OO 1.479E+OO 32.75 OK 794.95 4.25 1.739E+OO 1.999E+OO 1.999E+OO 82. 62 OK 835.71 1. 61 1.672E+OO Line Not Found Absent 911.20 25.80* 1.561E+OO 1.041E+OO 1.041E+OO 28.80 OK 968. 97 15.80 1.487E+OO 1.lOOE+OO 1.lOOE+OO 36.32 OK TH-228 74.82 10.28 3.783E+00 1. 5'45E+OO l.545E+00 59.01 OK 77 .11 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25.96 OK 238.63 43.60* 4.702E+OO 1.200E+OO l.200E+00 12.25 OK 300.09 3.30 3.910E+OO Line Not Found Absent TH-230 609.32 45.49* 2.155E+00 l.025E+00 1.025E+OO 22.80 OK 1120.29 14.92 1.323E+OO 1.112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 1.201E+OO 1. 201E+OO 39.68 OK TH-232 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+00 l.479E+OO 1.479E+OO 32.75 OK 835.71 1. 61 1. 672E+OO Line Not Found Absent Page 2912 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 25.80* 1.561E+OO 1.041E+OO 1.041E+OO 28.80 OK 968. 97 15.80 1.487E+OO 1.lOOE+OO 1.lOOE+OO 36.32 OK TH-234 63.29 3.70* 2.417E+OO 2.186E+OO 2.186E+OO 158.12 OK 92.59 4.23 5.211E+00 3.099E+OO 3.099E+OO 68.16 OK u:...234 609.32 45.49* 2.155E+OO 1.025E+OO 1.025E+OO 22.80 OK 1120.29 14.92 1. 323E+OO 1.112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8. 931E-01 1.201E+OO 1.201E+OO 39.68 OK U-235 89. 96 3.47 5.033E+OO Line Not Found Absent 93.35 5.60 5.211E+00 2.341E+OO 2.341E+OO 68.16 OK 143.76 10.96* 6.129E+OO 9.669E-02 9.669E-02 407.43 OK 163.33 5.08 5.908E+00 Line Not Found* -----Absent 185.72 57.20 5.553E+OO 1.464E-01 1.464E-01 69 .13 OK 205.31 5.01 5.230E+OO Line Not Found Absent U-238 63.29 3.70* 2.417E+OO 2.186E+OO 2.186E+OO 158.12 OK 92.59 4.23 5. 211E+OO 3.099E+OO 3.099E+OO 68.16 OK AM-243 43.53 5.90 2.878E-01 Line Not Found Absent 74.66 67.20* 3.783E+OO 2.363E-01 2.364E-01 59.01 OK ANH-511 511. 00 100.00* 2.491E+OO 1.218E-01 l.218E-01 74.84 OK Flag: "*" = Keyline Page 2913 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:57:43.46 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l *
Acquisition date 3-0CT-2016 07:56:53 'sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1. 5'00 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Analyst initials: MXRl *
Sample ID G405235001 Sample Quantity l.4192E+02 GRAM *
Batch Number 1596247 Wet Weight* 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.685E+Ol 1.814E+OO C0-58 3.751E-01 7.476E-01 BA-137M 5.323E-01 9.881E-02 CS-137 5.624E-01 1.044E-01 TL-208 4.222E-01 9.518E-02 PB-212 1.200E+OO 1.441E-01 BI-214 1. 026E+OO 2.292E-01 PB-214 1.221E+OO 2.199E-01 RN-222 1.026E+OO 2.292E-01 RA-224 l.414E+00 1.502E+OO RA-226 l.026E+OO 2.292E-01 AC-228 1.041E+OO 2.939E-01 RA-228 1.041E+OO 2.939E-01 TH-228 1.200E+OO l.441E-01 TH-230 l.025E+OO 2.291E-01 TH-232 l.041E+OO 2.939E-01 TH-234 2.186E+OO. 3.388E+00 U-234 1.025E+OO 2.291E-01 U-235 9.669E-02 3.860E-01 U-238 2.186E+OO 3.388E+OO AM-243 2.364E-01 1. 367E-01 ANH-511 1.218E-01 8.937E-02 Non-Identified Nuclides Nuclide BE-7 . NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 2914 of 5809 Key-Line Activity (pCi/GRAM -1.033E+Ol 1.975E-02 O.OOOE+OO -1.136E-02 -2.504E-01 O.OOOE+OO O.OOOE+OO 1.886E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.586E+Ol 5.169E-02 1.349E+41 2. 855E.:..02 4.309E-01 l.594E+04 4.612E+02 7.391E-02 MDA (pCi/GRAM 5.916E-01 l.576E-01 8.448E-02 8.924E-02 7.254E-02 l.072E-01 l.350E-01 1.460E-01 1.350E-01 1.149E+OO 1.350E-01 2.560E-01 2.560E-01 1.072E-01 1.350E-01 2.560E-01 2.955E+OO l.350E-01 3.806E-01 2.955E+OO l.249E-01 6.502E-02 MDA (pCi/GRAM 2.726E+Ol l.055E-01 O.OOOE+OO 5.642E-02 7.340E-01 O.OOOE+OO O.OOOE+OO 1. 496E-01 NOT IDENT. NOT IDENT . SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 -3.947E-01 5.563E-01 9.794E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 410E+41 O.OOOE+OO SHORT HLIF C0-57 4.240E-02 5.649E-02 l.081E-01 NOT IDENT. FE-59 1. lllE+Ol 1.443E+Ol 1. 734E+Ol FAIL ABUN C0-60 -3.648E-02 5.042E-02 7.292E-02 NOT IDENT. ZN-65 -4. 372E-03 2.487E-01 4.150E-01 NOT IDENT. GE-68 -5.512E-01 2.709E+OO 5.102E+OO NOT IDENT. AS-73 8.307E+OO 1.268E+Ol 2.537E+Ol NOT IDENT. AS-74 0.000E+OO 7.478E+03 O.OOOE+OO SHORT HLIF SE-75 -1. 7 64E-01 2.576E-01 4.087E-01 NOT IDENT. BR-77 O.OOOE+OO l.407E+37 O.OOOE+OO SHORT HLIF

SR-82 O.OOOE+OO 7 .141E+02 O.OOOE+OO SHORT HLIF RB-83 2. 717E-01 7.858E-01 1. 531E+OO NOT IDENT. KR-85 l.558E+OO 9.643E+OO 1.629E+Ol NOT IDENT. SR-85 1. 601E-Ol 9. 966E-01 l.683E+OO NOT.IDENT. RB-86 0.000E+OO 3.140E+04 O.OOOE+OO SHORT HLIF Y-88 4.653E-02 2.202E-01 5.156E-01 NOT IDENT. Y-91 -1.329E+02 6.400E+02 l.180E+o3 NOT IDENT. NB-94 -1.070E-02 3.508E-02 6.669E-02 NOT IDENT. NB-95 -2.388E-01 1.250E+OO 2.107E+OO NOT IDENT. NB-95M -4.962E-01 2.845E+OO 4.826E+OO NOT IDENT. ZR-95 l.934E+OO 2.712E+OO 3.715E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 097E+41 . 0 .. OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.179E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1.572E+41 O.OOOE+OO SHORT HLIF RH-101 -l.953E-02 4.321E-02 7.469E-02* NOT IDENT. RH-102 1. 531E-02 7.310E-02 l.392E-01 NOT IDENT. RU-103 5.366E+OO 5. 231E+OO 1.151E+Ol FAIL ABUN RH-106 -2.953E-01 6.393E-01 1.102E+OO NOT IDENT. RU-106 -2.953E-01 6.393E-01 1.102E+OO NOT IDENT. AG-108M 3.360E-02 3.703E-02 7.512E-02 NOT IDENT. CQ-109 2.982E+OO 1.609E+OO 3.067E+OO NOT IDENT. AG-llOM 5.130E-02 1.239E-01 2.550E-01 FAIL ABUN SN-113 l.139E-01 2.743E-01 5.386E-01 NOT IDENT. CD-115 O.OOOE+OO 2.020E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1. 017E+05 O.OOOE+OO SHORT HLIF TE-123M 5.067E-02 1.533E_:Ol 3.055E-01 NOT IDENT. SB-124 -6.571E-01 1.707E+OO 3.429E+OO NOT IDENT. SB-125 -4.868E-02 1.220E-01 2.192E-01 FAIL ABUN TE-125M 8.935E+Ol 3.109E+02 5.793E+02 NOT IDENT. I-126 O.OOOE+OO 9.782E+05 O.OOOE+OO SHORT HLIF SB-1.2 6 O.OOOE+OO l.382E+06 O.OOOE+OO SHORT HLIF SN-126 l.453E-01 l.028E-01 2.016E-01 NOT IDENT. SB-127 O.OOOE+OO 1.820E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.953E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF TE-132 0.000E+OO 3 .181E+26 O.OOOE+OO SHORT HLIF BA-133 2.367E-02 4.869E-02 8.874E-02 NOT IDENT. I-133 O.OOOE+OO 7.179E+40 O.OOOE+OO SHORT HLIF CS-134 1.306E-01 l.058E-01 l.338E-01 FAIL ABUN CS-135 2.299E-02 1.592E-01 3.083E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HliIF CS-136 O.OOOE+OO 2.992E+05 O.OOOE+OO SHORT HLIF CE-139 -2.036E-03 1.259E-01 2.457E-01 NOT IDENT. BA-140 O.OOOE+OO 1.537E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.300E+05 0.000E+OO SHORT HLIF CE-141 -5.740E+OO 3.088E+Ol 4.955E+Ol NOT IDENT. CE-143 0. OOOE+OO. 1.042E+41 O.OOOE+OO SHORT HLIF CE-144 -4.306E-02 3:893E-01 6.950E-01 NOT IDENT. PM-144 3.248E-02 6*. 778E-02 l.395E-01 NOT IDENT. PR-144 2.802E+OO 5.879E+OO 1.210E+Ol NOT IDENT. PM-146 l.939E-02 5.429E-02 l.056E-01 NOT IDENT. ND-147 0.000E+OO 3.661E+07 O.OOOE+OO SHORT HLIF PM-147 1. 318E+02 9.980E+02 1. 821E+03 NOT IDENT. PM-149 O.OOOE+OO 2.721E+40 O.OOOE+OO SHORT HLIF EU-150 -4.283E-03 3. 377E-02 5.634E-02 FAIL ABUN EU-152 5.747E-03 1.128E-01 2.144E-01 FAIL ABUN GD-153 -9. 845E-02 . 2.504E-01 4.109E-01 NOT IDENT. EU-154 4.574E-02 1.263E-01 2.570E-01 NOT IDENT. EU-155 7.265E-02 l.258E-01 2.402E-01 NOT IDENT. TB-160 -1.448E+OO 1. 972E+OO 3.443E+OO FAIL ABUN H0-166M 2.139E-02 6.676E-02 l.331E-01 NOT IDENT. TM-171 -2. 711E+OO 3.236E+Ol 6.126E+Ol NOT IDENT. HF-172 -l.167E-02 2.786E-01 4.995E-01 FAIL ABUN LU-172 -3.326E-02 1.334E-01 2.099E-01 FAIL ABUN LU-176 -9.986E-03 2. 611E-02 4.822E-02 NOT IDENT. HF-181 2.255E-01 5.453E+00 1.019E+Ol NOT IDENT. Page 2915 of 5809 TA-182 l.438E+OO l.193E+00 2.312E+OO FAIL ABUN
RE-183 -2.638E+OO 4.377E+OO 7.887E+OO NOT IDENT. RE-184 2.943E+Ol 3.645E+Ol 7.818E+Ol NOT IDENT. W-188 -3.587E+Ol l.423E+02 2.362E+02 FAIL ABUN IR-192 -4.362E-01 5.188E-01 9.087E-01 FAIL ABUN HG-203 4.209E-01 2.751E+00 5.309E+OO NOT IDENT. BI-207 -2.553E-02 5.978E-02 1.077E-01 FAIL ABUN PB-210 -1.184E+OO 5. 916E+OO. 1.104E+Ol NOT IDENT. BI-211 O.OOOE+OO 6.058E-01 9.921E-01 FAIL ABUN PB-211 -3.378E-02 8.026E-01 1.503E+OO NOT IDENT. BI-212 1.412E+OO 7.607E-01 1.461E+OO FAIL ABUN RN-219 -l.153E-01 4.514E-01 8.272E-01 FAIL ABUN RA-223 -2.656E-01 6.892E-01 l.262E+OO FAIL ABUN AC-227 1.042E-02 2.582E-01 4.975E-01 NOT IDENT. TH-227 1. 042E-02 2.582E-01 4.975E-01 NOT IDENT. TH-229 1.264E-01 5.363E-01 1.054E+OO NOT IDENT. PA-231 5.744E-02 5.328E-01 1.019E+OO NOT IDENT. TH-231 -2.656E-01 6.892E-01 l.262E+00 FAIL ABUN PA-233 -8.485E-03 6.648E-02 1.255E-01 NOT IDENT. PA-234 -l.485E-01 3.838E-01 6.989E-01 FAIL ABUN PA-234M -l.313E+OO 5.149E+OO 1. 012E+Ol NOT IDENT. NP-237 -8.485E-03 6.648E-02 1.255E-01 NOT IDENT. NP-238 O.OOOE+OO l.204E+41 O.OOOE+OO SHORT HLIF NP-239 3.933E-01 3.00lE-01 5.656E-01 NOT IDENT. PU-239 2.344E+Ol 3.894E+02 7.001E+02 NOT IDENT. AM-241 2 .139E-01 2.158E-01 4.059E-01 NOT IDENT. CM-243 -1. 051E-02 1.259E-01 2.275E-01 NOT IDENT. BK-247 -6."994E-02 8.734E-02 1.363E-01 NOT IDENT. CM-247 -3.403E-02 4.0SOE-02 6.917E-02 NOT IDENT. CF-249 3.059E-03 4.283E-02 8.169E-02 NOT IDENT. CF-251 -l.555E-02 1.229E-01 2.383E-01 NOT IDENT. Page 2916of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:57:40.93 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 360 10.66* l.059E+OO l.685E+Ol l.685E+Ol 10.98 C0-58 810.76 7 99.45* 1. 711E+OO 2.038E-02 3.751E-01 203.37 BA-137M 661.66 179 89.90* 2.016E+OO 5.224E-01 5.323E-01 18.94 CS-137 661. 66 179 85.10* 2.016E+OO 5.519E-01 5.624E-01 18.94 TL-208 277.37 ------6.60 4.173E+OO ------Lin'e Not Found ------583.19 151 85.00* 2.233E+OO 4.222E__:Ol 4.222E-01 23.00 860.56 ------12.50 l.634E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.574E+OO ------Line Not Found ------351.06 281 12.92* 3.418E+OO 3.364E+OO 3.364E+OO 18.38 PB-212 74.82 164 10.28 3.783E+OO 2.237E+OO 2.237E+OO 39.87 77 .11 262 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25. 96 238.63 465 43.60* 4.702E+OO l'. 200E+OO l.200E+OO 12.25 300.09 ------3.30 3.910E+OO ------Line Not Found ------BI-214 60.9.32 190 45.49* 2.155E+OO l.025E+OO l.026E+OO 22.80 1120.29 41 14.92 l.323E+oo l .112E+OO l.112E+OO 48.51 1764 .'49 31 15.30 8.931E-01 l.201E+OO ' 1. 202E+00 39.68 PB-214 74.82 164 5.80 3.783E+OO 3. 964E+OO 3. 966E+OO 39.87 77 .11 262 9.70 4.000E+OO 3.579E+00 3.580E+OO 25. 96 87.09 ------3.41 4.837E+OO ------Line Not Found ------242.00 129 7.25 4.652E+OO 2.026E+OO 2.027E+OO 39.44 295.22 169 18.42 3. 963E+00 l.226E+OO l.226E+OO 27.45 351. 93 281 35.60* 3.418E+OO l.221E+OO 1. 221E+OO 18.38 RN-222 609.32 190 45.49* 2.155E+OO l.025E+OO l.026E+OO . 22. 80 1120.29 41 14.92 l.323E+OO l .112E+OO l .112E+OO 48.51 1764.49 31 15.30 8. 931E-01 l.201E+OO l.202E+OO 39.68 RA-224 240.99 129 4.10* 4.652E+OO 3.582E+OO 3.582E+OO 39.44 RA-226 609.32 190 45.49* 2.155E+OO l.025E+OO 1. 026E+OO 22.80 1120.29 41 14.92 l.323E+OO l .112E+OO l .112E+OO 48.51 1764.49 31 15.30 8. 931E-01 1. 201E+OO l.202E+OO 39.68 AC-228 105.21 ------1.10 5.776E+OO ------Line.Not Found ------338.32 111 11. 27 3.533E+OO 1. 479E+OO l.479E+OO 32.75 794.95 28 4.25 1. 739E+OO l.999E+OO l.999E+OO 82.62 835.71 ------1. 61 1. 672E+OO ------Line Not Found ------911.20 79 25.80* l.561E+OO 1. 041E+OO l.041E+OO 28.80 968. 97 49 15.80 l.487E+OO 11* lOOE+OO l.lOOE+OO 36.32 RA-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 111 11.27 3.533E+OO 1:479E+OO l.479E+OO 32.75 794.95 28 4.25 1. 739E+OO l.999E+OO l.999E+OO 82.62 835.71 ------1. 61 1. 672E+OO ------Line Not Found ------911.20 79 25.80* l.561E+OO l.041E+OO 1. 041E+OO 28.80 968. 97 49 15.80 l.487E+OO l.lOOE+OO l.lOOE+OO 36.32 TH-228 74.82 164 10.28 3.783E+00 2.237E+OO 2.237E+OO 39.87 77 .11 262 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25.96 238.63 465 43.60* 4.702E+OO l.200E+OO l.200E+OO 12.25 300.09 ------3.30 3.910E+OO ------Line Not Found ------TH-230 609.32 190 45.49* 2.155E+OO l.025E+OO l.025E+OO 22.80 1120.29 41 14.92 l.323E+OO l.112E+00 l .112E+OO 48.51 Page 2917 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 1764.49 31 15.30 8.931E-01 1.201E+OO 1.201E+OO 39.68 TH-232 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 111 11.27 3.533E+OO l.479E+OO 1.479E+OO 32.75 835. 71 ------1. 61 1. 672E+OO ------Line Not Found ------911. 20 79 25.80* 1.561E+OO 1.041E+OO 1.041E+OO 28.80 968. 97 49 15.80 l.487E+OO l.lOOE+OO 1.lOOE+OO 36.32 TH-234 63.29 37 3.70* 2.417E+OO 2.186E+OO 2.186E+OO 15.8 .12 92.59 129 4.23 5. 211E+OO 3.099E+OO 3.099E+OO 68.16 U-234 609.32 190 45. 49.* 2.155E+OO l.025E+OO 1.025E+OO 22.80 1120.29 41 14.92 1.323E+OO l .112E+OO 1.112E+OO 48.51 1764.49 31 15.30 8.931E-01 l.201E+OO 1. 201E+OO 39.68 U-235 89.96 ------3.47 5.033E+OO ------Line Not Found ------93.35 129 5.60 5. 211E+OO 2.341E+OO 2.341E+OO 68.16 143.76 12 10.96* 6.129E+OO 9.669E-02 9.669E-02 407.43 163.33 ------5.08 5. 908E+*oo ------Line Not Found ------185.72 88 5"7.20 5.553E+OO 1.464E-01 1.464E-01 69.13 205.31 ------5.01 5.230E+OO ------Line Not Found ------U-238 63.29 . 37 .3. 70* 2.417E+OO 2.186E+OO 2.186E+OO 158.12 92. 59' 129 4.23 5. 211E+00 3.099E+OO 3'. 099E+OO 68.16 AM-243 43.53 ------5.90 2.878E-01 ------Line Not Found ------74.66 164 67.20* 3.783E+OO 3. 421E-01 3.422E-01 39.87 ANH-511 51,1. 00 57 100.00* 2.491E+OO l.218E-01 1.218E-01 74.84 Flag: "*" Key line Page 2918of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Total number of lines in spectrum 50 Number of unidentified lines 16 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 C0-58 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 . TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlif e 1. 25E+09Y 70.86D 30.08Y 30.08Y 1.41E+10Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+l0Y 1. 41E+l0Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 18.4 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.685E+Ol 2.038E-02 5.224E-01 5.519E-01 4.222E-01 3.364E+OO 1.200E+OO 1. 025E+OO 1.221E+OO 1.025E+OO 3.582E+OO 1.025E+OO 1.041E+OO 1. 041E+OO 1.200E+OO 1. 025E+OO 1. 041E+OO 2.186E+00 1.025E+OO 9.669E-02 2.186E+OO 3.421E-01 1.218E-01 4.212E+Ol 4.212E+Ol Decay Corr pCi/GRAM 1.685E+Ol 3.751E-01 5.323E-01 5.624E-01 4.222E-01 3.364E+OO 1.200E+OO 1.026E+OO 1.221E+OO 1.026E+OO 3.582E+00 1.026E+OO 1. 041E+OO 1.041E+OO 1.200E+OO l.025E+OO 1.041E+OO 2.186E+OO 1.025E+OO 9.669E-02 2.186E+OO 3.422E-01 1.218E-01 4.250E+Ol 4.250E+Ol 68.00% Decay Corr 2-Sigma Error 0.185E+Ol 7.629E-01 l.008E-01 l.065E-01 0.971E-01 0.618E+OO 0.147E+OO 0.234E+00 0.224E+OO 0.234E+OO l.413E+OO 0.234E+OO . 0. 300E+OO 0.300E+OO 0.147E+OO 0.234E+OO 0.300E+OO 3.457E+OO 0.234E+OO 39.39E-02 3.457E+OO 1.364E-01 0.912E-01 "M" Manually accepted 2-Sigma %Error 10.98 203.37 18.94 18.94 23.00 18.38 12.25 22.80 18.38 22.80 39.44 22.80 28.80 28.80 12.25 22.80 28.80 158.12 22.80 407.43 158.12 39.87 74.84 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 2919 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235001 Acquisition date : 3-0CT-2016 07:56:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 112.23 14 167 l. 42 223.88 223 8 3.36E-03 **** 5.97E+OO T 0 208.83 76 184 2.65 416;92 411 13 l.86E-02 82.0 5.17E+OO 0 270.65 94 105 3.65 540.43 533 14 2.34E-02 53.6 4.26E+OO T 0 382.01 15 43 2.94 762.98 756 9 3.79E-03 **** 3.19E+OO 0 464.18 20 46 0.60 927.18 918 13 5.13E-03 **** 2.70E+OO T 1 546.32 23 19 l. 84 1091.33 1088 18 6.19E-03 71. 6 2.36E+OO T 1 548.66 19 29 l. 67 1096.00 1088 18 5.09E-03 **** 2.35E+OO 4 658.58 17 21 l. 94 1315.69 1312 17 4.55E-03 **** 2.02E+OO T 0 717. 42 13 19 3.43 1433.28 1429 12 3.65E-03 **** l.89E+OO 0 726. 67 33 16 l. 28 1451.75 1448 8 9.04E-03 55.0 l.87E+OO .T 0 755.24 14 25 l. 36 1508.86 1502 10 3. 91E-03 **** l.81E+OO T 0 769.00 25 40 0.88 1536.36 1527 12 6.74E-03 **** l.79E+OO 0 808.56 14 20 1.21 1615.42 1608 11 3.75E-03 **** 1.72E+OO T 1 964. 76 26 1 2.17 1927.61 1922 21 7.22E-03 55.2 l.49E+OO T 0 1023.46 12 15 4.60 2044.92 2036 15 3.33E-03 **** 1.42E+OO 0 1099.87 15 18 0.80 2197.65 2188 14 4.35E-03 **** 1.34E+OO T 0 1130 .15 18 6 3.23 2258.17 2252 12 5.00E-03 '72. 0 1. 31E+OO T 0 1154.59 25 10 2.10 2307.01 2300 14 7.16E-03 66.1 1.29E+OO 2 1186.65 14 8 2.55 2371. 09 2361 26 4.09E-03 **** 1.26E+OO 2 1191. 84 14 17 2.55 2381. 47 2361 26 4.0lE-03 **** l.26E+00 0 1195. 72 9 7 l. 37 2389.22 2386 7 2.50E-03 **** 1.25E+OO 0 1222.52 15 8 l. 55 2442.79 2438 10 4.24E-03 84.7 l. 23E+OO T 0 1228.78 14 5 2.06 2455.30 2451 9 3. 96E-03 75.7 l. 23E+OO 0 1252.82 22 3 3.01 2503.34 2498 12 6.31E-03 52.1 l.21E+OO 0 1282.31 23 4 5.42 2562.30 2555 16 6.59E-03 55.9 1.18E+OO 0 1325.72 13 0 2.73 2649.08 2644 12 3. 61E-03 55.5 1.15E+OO 0 1378.42 14 7 1.11 2754.41 2750 10 3.91E-03 94.7 l. llE+OO 0 1729.65 6 2 0.69 3456.50 3450 11 1.90E-03 **** 9.lOE-01 Flags: "T" = Tentatively associated Page 2920 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:58:05.87 *******************************************************************************
GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA ' * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l *
Acquisition date 3-0CT-2016 07:56:53 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
Sample ID G405235001 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4192E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 . * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 BA-137M CS-137 TL-208 PB-212 I BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.322E-01 O.OOOE+OO 3.814E-02 4.029E-02 3.242E-02 4.997E-02 6 .'005E-02 6.692E-02 6.005E-02 5.359E-01 6.005E-02 1.lOOE-01 1.lOOE-01 4.997E-02 6.003E-02 1.lOOE-01 1.395E+OO 6.003E-02 1. 791E-01 l.395E+OO 5.947E-02 2.957E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 2921 of 5809 Le (pCi/GRAM 1.234E+Ol 4.521E-02 O.OOOE+OO 1.999E-02 3.135E-01 O.OOOE+OO O.OOOE+OO 6.639E-02 4.262E-01 NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144' PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 2922 of 5809 O.OOOE+OO 5.099E-02 7.686E+OO 2.947E-02 l.825E-01 2.199E+OO 1.192E+Ol O.OOOE+OO 1. 881E-01 O.OOOE+OO O.OOOE+OO 6.927E-01 7.428E+OO 7.675E-01 O.OOOE+OO 1.997E-01 5.143E+02 2.955E-02 9.515E-01 2.254E+OO 1.672E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.522E-02 6.238E-02 5 .151E+OO 4.904E-01 4.904E-01 3.472E-02 1. 469E+00 1.133E-01 2.474E-01 O.OOOE+OO O.OOOE+OO l.443E-01 1.215E+OO 9.914E-02 2.724E+02 O.OOOE+OO O.OOOE+OO 9.664E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.066E-02 O.OOOE+OO 6.047E-02 1.433E-01 O.OOOE+OO O.OOOE+OO l.157E-01 O.OOOE+OO O.OOOE+OO 2.333E+01 O.OOOE+OO 3.248E-01 6.308E-02 5.470E+OO 4.823E-02 O.OOOE+OO 8.571E+02 O.OOOE+OO 2. 599E-02. 9.888E-02 l.942E-01 1.lOOE-01 l.131E-01 1.461E+OO 5.947E-02 2.873E+Ol 2.351E-01 9.346E-02 2.205E-02 4.643E+OO 1.025E+OO SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 2923 of 5809 3. 711E+OO 3.498E+Ol l.093E+02 4.152E-01 2.471E+OO 4. 672E-02 5.173E+OO 4.796E-01 6.871E-01 6. 722E-01 3.771E-01 5.807E-01 2.312E-01 2.312E-01 4. 961E-01 4.740E-01 5.807E-01 5.767E-02 3.097E-Ol 4.465E+OO 5.767E-02 O.OOOE+OO 2.671E-01 3.308E+02 1.924E-01 l.073E-01 6.243E-02 3.123E-02 3. 729E-02 1.115E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide. Identification Report Generated 03-0CT-2016 08:58:11.72 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l *
Acquisition date 3-0CT-2016 07:56:53 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
Sample ID G405235001 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity 1.4192E+02 GRAM *
Quantity Err(%) 1.4092E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal: date 22-AUG-2016 09:02:05 Eff. Geometiy : CAN *
Eff. File . : DKA100: GAM02 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are. valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.685E+Ol 2.017E+OO 2.017E+00 C0-58 3.751E-01 7.478E-01 7.478E-01 BA-137M 5.323E-01 1.014E-01 l.014E-01 CS-137 5.624E-01 l.071E-01 1. 071E-01 TL-208 4.222E-01 9.686E-02 9.686E-02 PB-212 1. 200E+OO 1. 57 6E-01 l.576E-01 BI-214 1. 026E+OO 2.334E-01 2.334E-01 PB-214 1.221E+OO 2.258E-01 2.258E-01 RN-222 1.026E+OO 2.334E-01 2.334E-01 RA-224 l.414E+00 .1. 511E+OO 1. 511E+OO RA-226 1.026E+OO 2.334E-01 2.334E-01 AC-228 1.041E+OO 2.987E-01 2.987E-01 RA-228 1. 041E+OO 2.987E-01 2.987E-01 TH-228 1.200E+00 1. 57 6E-01 1. 576E-01 TH-230 1. 025E+OO 2.333E-01 2.333E-01 TH-232 1.041E+OO 2.987E-01 2.987E-Ul TH-234 2.186E+00 3.422E+OO 3.422E+OO U-234. 1-. 025E+OO 2.333E-01 2.333E-01 U-235 9.669E-02 3.861E-01 3.861E-01 U-238 2.186E+OO 3.422E+OO 3.422E+OO AM-243 2.364E-01 1. 381E-01 1. 381E-01 ANH-511 1.218E-01 8.951E-02 8. 951E-02 N9n-Identif ied Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 -1.033E+Ol 1.586E+Ol 1.653E+Ol NOT I.DENT. NA-22 l.975E-02 5.170E-02 5.246E-02 NOT IDENT. NA-24 -1.000E+41 1.417E+41 O.OOOE+OO
SHORT HLIF AL-26 -1.136E-02 2.856E-02 2.901E-02 FAIL ABUN SC-46 -2.504E-01 4.310E-01 4.456E-01 FAIL ABUN V-48 l.277E+04 l.595E+04 1. 696E+04 SHORT HLIF CR-51 2.842E+02 4.614E+02 4.789E+02 SHORT HLIF MN-54 l.886E-02 7. 391E-02 7.440E-02 NOT IDENT. Page 2924 of 5809 C0-56 -3.947E-01 5.565E-01 5.843E-01 NOT IDENT. MN-56 -1.000E+41 l.410E+41 O.OOOE+OO SHORT HLIF C0-57 4.240E-02 5. 653E-02. 5. 967E-02 NOT IDENT. FE-59 l. lllE+Ol l.445E+Ol 1.529E+Ol FAIL ABUN C0-60 -3.648E-02 5.044E-02 5.306E-02 NOT *IDENT. ZN-65 -4.372E-03 2.487E-01 2.487E-01 NOT IDENT. GE-68 -5.512E-01 2.709E+OO 2.720E+OO NOT IDENT. AS-73 8.307E+OO 1.279E+Ol 1.333E+Ol NOT IDENT. AS-74 5.670E+03 7.493E+03 7.917E+03 SHORT HLIF SE-75 -l.764E-01 2.577E-01 2.697E-01 NOT IDENT. BR-77 1.172E+38 l.007E+39 O.OOOE+OO SHORT HLIF SR-82 l.438E+02 7.141E+02 7.170E+02 SHORT HLIF RB-83 2. 717E-01 7.867E-01 7.962E-01 NOT IDENT. KR-85 1.558E+OO 9.643E+OO 9.668E+OO NOT IDENT. SR-85 l.601E-01 9. 966E-01 9.992E-01 NOT IDENT. RB-86 -l.205E+04 3.141E+04 3 .187E+04 SHORT HLIF Y-88 4.653E-02 2.202E-01 2.212E-01 NOT IDENT. Y-91 -1. 329E+02 6.400E+02 6.428E+02 NOT IDENT. NB-94 -1. 070E-02 3.508E-02 3.541E-02 NOT IDENT. NB-95 -2.388E-01 1.250E+OO 1.255E+OO NOT IDENT. NB-95M -4.962E-01 2.845E+OO 2.854E+OO NOT IDENT. ZR-95 1.934E+OO 2.714E+OO 2.850E+OO FAIL ABUN NB-97 l.000E+41 1.098E+41 0.000E+OO SHORT HLIF ZR-97 l.000E+41 4.411E+41 O.OOOE+OO SHORT HLIF M0-99 1. 831E+31 l.179E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.576E+41 O.OOOE+OO SHORT HLIF. RH-101 -1.953E-02 4.335E-02 4.424E-02 NOT IDENT. RH-102 l.531E-02 7. 311E-02 7.344E-02 NOT IDENT. RU-103 5.366E+OO 5.237E+OO 5.769E+OO FAIL ABUN RH-106 -2.953E-01 . 6. 396E-01 6.533E-01 NOT IDENT. RU-106 -2.953E-01 6. 396E-01 6.533E-01 NOT IDENT. AG-108M 3.360E-02 3.705E-02 4.003E-02 NOT IDENT. CD-109 2.982E+OO 1.628E+OO 2. lllE+OO NOT IDENT. AG-llOM 5.130E-02 1.239E-01 1.260E-01 FAIL ABUN SN-113 1.139E-01 2.743E-01 2."791E-01 NOT IDENT. CD-115 6.777E+38 2.023E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 2.239E+03 1. 017E+05 l.017E+05 SHORT HLIF TE-123M 5.067E-02 1.533E-01 1.550E-01 NOT IDENT. SB-124 -6.571E-01 1. 707E+OO 1. 733E+OO NOT IDENT. SB-125 -4.868E-02 1. 220E-01 l.239E-01 FAIL ABUN TE-125M 8.935E+Ol 3.109E+02 3.135E+02 NOT IDENT. I-126 l.189E+05 9.783E+05 9.798E+05 SHORT HLIF SB-126 -4.278E+05 l.384E+06 *l. 398E+06 SHORT HLIF SN-126 l.453E-01 l.032E-01 l.222E-01 NOT IDENT. SB-127* -1.412E+22 2. 651E+22 O.OOOE+OO SHORT HLIF I-131 1.886E+09 4.954E+09 5.026E+09 SHORT HLIF I-132 -1. 000E+41 1. 847E+42 O.OOOE+OO SHORT HLIF TE-132 -1.375E+26 3.229E+26 O.OOOE+OO SHORT HLIF BA-133 2.367E-02 4.870E-02 4.985E-02 NOT IDENT. I-133 -1.000E+41 1.935E+41 O.OOOE+OO SHORT HLIF CS-134 1.306E-01 l.059E-01 1.212E-01 FAIL ABUN CS-135 2.299E-02 1. 592E..:.01 1.596E-01 NOT IDENT. I-135 1. OOOE+41 7.696E+41 O.OOOE+OO SHORT HLIF CS-136 2.616E+05 3.005E+05 3.229E+05 SHORT HLIF CE-139 -2.036E-,-03 1.259E-01 1.259E-01 NOT IDENT. . BA-140 l.090E+06 1.538E+06 l.615E+06 SHORT HLIF LA-140 1. 213E+05 5.300E+05 5.328E+05 SHORT HLIF CE-141 -5.740E+OO 3.089E+Ol 3.099E+Ol NOT IDENT. CE-143 1. OOOE+41 . 1.047E+41 O.OOOE+OO SHORT HLIF CE-144 -4.306E-02 3.893E-01 3.898E-01 NOT IDENT. PM-144 3.248E-02 6.781E-02 6.937E-02 NOT IDENT. PR-144 2.802E+OO 5.880E+OO 6.014E+OO NOT IDENT. PM-146 l.939E-02 5.431E-02 5.500E-02 NOT IDENT. ND-147 -2.717E+07 3.664E+07 3.863E+07 SHORT HLIF PM-147 l.318E+02 9.980E+02 9.998E+02 NOT IDENT. PM-149 -9.014E+39 2.728E+40 O.OOOE+OO SHORT HLIF EU-150 -4.283E-03 3.377E-02 3.382E-02 FAIL ABUN EU-152 5.747E-03 l.128E-01 l.128E-01 FAIL ABUN Go-1*53 -9.845E-02 2.505E-01 2.544E-01 NOT IDENT. EU-154 4.574E-02 l.263E-01 l.280E-01 NOT IDENT. EU-155 7.265E-02 l.259E-01 l.301E-01 NOT IDENT. TB-160 -i.448E+OO 1.974E+OO 2.079E+OO FAIL.ABUN H0-166M 2.139E-02 6.677E-02 6.746E-02 NOT IDENT. TM-171 -2. 711E+OO 3.236E+Ol 3.239E+Ol NOT IDENT. HF-172 -l.167E-02 2.786E-01 2.787E-01 FAIL ABUN LU-172 -3.326E-02 1.334E-01 1.342E-01 FAIL ABUN LU-176 -9.986E-03 2.612E-02 2.650E-02 NOT IDENT. HF-181 2.255E-01 5.453E+OO 5.454E+OO NOT IDENT. Page 2925 of 5809 TA-182 l.438E+OO 1.195E+OO 1.359E+OO FAIL ABUN RE-183 -2.638E+00 4.396E+OO 4.554E+OO NOT IDENT. RE-184 2.943E+Ol 3.712E+Ol 3.942E+Ol NOT IDENT. W-188 -3.587E+Ol l.424E+02 1.433E+02 FAIL ABUN IR-192 -4.362E-01 5 .191E-01 5.551E-01 FAIL ABUN HG-203 4.209E-01 2.751E+OO 2.757E+OO NOT IDENT. BI-207 -2.553E-02 5.979E-02 6.088E-02 FAIL ABUN PB-210 -l.184E+OO 5.917E+OO 5.941E+OO NOT IDENT. BI-211 3.364E+OO 6.243E-01 l'. 640E+OO FAIL ABUN PB-211 -3.378E-02 8.026E-01 8.027E-01 NOT IDENT. BI-212 1.412E+OO 7.641E-01 9.945E-01 FAIL ABUN RN-219 -l.153E-01 4.517E-01 4.547E-01 FAIL ABUN -2.656E-01 6.894E-01 6 .. 997E-01 FAIL ABUN AC-227 l.042E-02 2.582E-01 2.583E-01 NOT IDENT. TH-227 l.042E-02 2.582E-01 2.583E-01 NOT IDENT. TH-229 l.264E-01 5.363E-01 5.393E-01 NOT. IDENT. PA-231 5.744E-02 5.329E-01 5.336E-01 NOT IDENT. TH-231 -2.656E-01 6.894E-01 6.997E-01 FAIL ABUN PA-233 -8.485E-03 6.648E-02 6.659E-02 NOT IDENT. PA-234 -1.485E-01 4.197E-01 4.250E-01 FAIL ABUN PA-234M -1.313E+OO 5.149E+OO 5.183E+OO NOT IDENT. NP-237 -8.485E-03 6.648E-02 6.659E-02 NOT IDENT. NP-238 1.000E+41 l.205E+41 O.OOOE+OO SHORT HLIF NP-239 3.933E-01 3.019E-01 3. 501E-01 NOT IDENT. PU-239 2.344E+Ol 3.894E+02 3. 896E+02 NOT IDENT. AM-241 2 .139E-01 2.164E-01 2.369E-01 NOT IDENT. CM-243 -1. 051E-02. l.259E-01 1. 2 60E-01 NOT IDENT. BK-247 -6.994E-02 8.847E-02 9.392E-02 NOT IDENT. CM-247 -3.403E-02 4.090E-02 4.368E-02 NOT IDENT. CF-249 . 3.059E-03 4.283E-02 4.286E-02 NOT IDENT. CF-251 -l.555E-02 1.229E-01 1.231E-01 NOT IDENT. Page 2926 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 78.2704 87.09 134.7812 .136.47 85.0401 45.60 71.5784 87.57 127.0328 140.51 0.0000 46.54 72.7927 88. 03* 103.5126 143.76 85.8807 49.72 0.0000 88.34 141.0985 144.24 85.9352 51. 35 77.8999 88.47 136.6277 145.44 91.8101 51. 87 86.3264 89.96 143.0228 152.43 89.3353 52.39 78.1111 1093.63 137.1702 153.25 0.0000 52.97 63.6255 91.11 0.0000 323.87 90.7811 53.44 65.7908 92.59 114.5844 156.02 0.0000 54.07 78.4481 93.35 114.7400 158.56 0.0000 57.36 0.0000 94.56 114.9858 159.00 89.2407 57.53 88.6213 94.65 115. 0043 162.33 96. 3059 57.98 101.3919 94.67 115. 0082 162.66 0.0000 59.27 69.2175 94.87 115.0482 163.33 90.5537 59.32 69.2258 97.43 100.6885 165.86 88.3075 59.54 81. 9838 98.43 85.9617 176.31 78.3306 60. 96 93.6061 98.44 85. 9634 176.60 0.0000 61.17 86.5572 99.53 97.6068 177.52 75.0288 62. 93 94.0358 100 .11 100.0017 181.07 0.0000 63.29 94 .1133 102.03 93.4072 181.52 80.9379 63.58 94.1761 103.18 94.7418 184.41 77.3337 64.28 102.9014 103.37 94.7718 143.76 77.4463 66.73 100.5944 105.21 73.0336 193.51 78.9761 67.24 103.5850 105.31 73.0456 197.03 85.3722 125.81 111. 2457 106.12 85.9137 198.01 77.6124 67.75 111. 2622 106.47 98.7410 201.83 78.8013 69. 67 100.8815 109.28 75.8505 203.43 72.3545 70.83 144.6296 111. 00 84.2492 205.31 56.6783 72.81 141.2314 111.76 0.0000 210.85 70.2564 72. 87 141.2491 114. 06 99.9395 215.65 63.0488 74.66 130.4477 116. 30 0.0000 222 .11 78.6445 74.82 130.4904 116.74 61.3925 227.09 80.8209 74.97 130.5312 119. 76 83.0230 227.38 80.8429 77 .11 131.1005 121.12 82.0038 228.16 0.0000 78.74 131. 5290 121. 22 82.0159 228.18 86.2988 79.69 131. 77 69 121.78 83.2740 116.74 86.2988 80.12 104.9197 122.06 72.5976 235.69 71. 9757 80.19 0.0000 122.92 95.3308 235. 96 71.9943 80.57 121.2817 123.07 95.3522 238.63 63.5486 81. 00 113.9828 265.00 90.6657 238.98 0.0000 81. 07 113.9984 125.81 87.3586 240.99 63.6874 81. 75 121. 5611 127.23 104.3257 242.00 63.7465 83.79 109.3894 127.91 80.4223 244.70 64.3611 84.00 101.6162 129.30 96.2170 252.40 0.0000 85.43 164.5944 131. 20 86.8293 252.80 53.3366 86.55 138. 0118 l33.02 91.8886 254.15 0.0000 86.79 131.3385 133.52 71. 3841 256.23 57.1884 86.94 134. 7437 136.00 69.2017 260.90 0.0000 Page 2927 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 59.9320 355.39 0.0000 584.27 23.8292 264.80 57.1520 356.01 31.3994 595.83 0.0000 265.00 57.1620 364.49 0.0000 427.87 29.7303 268.22 55.9216 366.42 0.0000 602.52 0.0000 269.46 55.9802 372.51 40.3223 604. 72 32.6505 270.03 56*. 0071 375.05 35.3418 607.14 25.8060 271. 23 56.0645 377.52 40. 9622 609.32 21.8134 273.65 0.0000 356.01 36.5625 610.33 21.8234 276.40 65.3180 388.16 35.6473 614.28 24.1642 277.37 56.3538 388.63 0.0000 618.01 28.8157 277.60 56.3647 391.69 35.7285 620.36 19.6154 278.00 48.8653 264.66 36. 9602 621.93 28.8676 279.20 57.3799 401. 81 40.0696 630.19 0.0000 279.54 60.2188 402.40 43.1672 631. 29 22.0314 279.70 61.1676 404.85 39; 1164 633.25 27.8535 280.46 61. 2060 410.95 37.1990 634.78 0.0000 283.69 45.3184 413.71 35.1925 635.95 25.5628 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 48.2182 423. 72 0.0000 645.85 20.1313 285.90 *o. 0000 . 427.09 39.6552 657.76 29.5620 287.50 55.8767 427.87 36.5424 657.90 0.0000 290.67 56.9690 433.94 33. 5313 661. 66 29.0835 293.27 0.0000 439.40 35.7425 664.57 0.0000 351.93 48.6000 453.88 31. 8048 666.33 0.0000 295.96 48.6291 463.37 27. 7144 666.50 0.0000 879.38 51.5962 468.07 38.4756 667.71 0.0000 299.98 61.6970 473.00 0.0000 677.62 24.8452 300.09 61.7023 475.06 37.5535 685.70 0.0000 300.13 61. 7036 476.78 35.4412 695.00 0.0000 301.36 57.4548 477.60 41. 9041 696.49 23.2531 302.85 54.6447 482.18 34.4701 696. 51 23.2531 256.23 47.0361 487.02 0.0000 697.00 0.0000 304.85 0 .. 0000 492.35 0.0000 697.30 19.6824 306.78 45.1956 497.08 11. 9453 697.49 23.2626 308.46 31.7740 '505.52 27.8164 702.65 24.2084 311. 90 41. 5119 507.63 0.0000 706.68 22.4525 316.51 53.2835 511. 00 33.9141 711. 68 19.5414 319.41 0.0000 514.00 32.8720 720. 70 0.0000 320.08 0.0000 514.00 32.8720 721. 93 0.0000 321.04 47.6322 520.40 2*5.2854 722. 78 14.4634 323.87 51. 6284 520.69 0.0000 722. 91 14.4644 325.23 59.4822 522.65 0.0000 723.31 14.4668 328.76 0.0000 527.90 0.0000 724.19 16.8836 333.37 58.8562 528.26 19.8691 727. 33 11.5918 333.97 50.0496 529.59 34.2430 733.00 18.1537 334.37 50.0641 529.87 0.0000 735.93 18.1744 338.28 40.3619 531. 02 0.0000 333.97 16.3669 338.32 40.3627 537.26 0.0000 739.50 0.0000 311. 90 50.2851 546.56 0.0000 747.24 19.1684 340.48 50.2851 552.55 26.8184 748.06 21. 9133 340.55 0.0000 563.25 34.8233 752.31 24.8766 344.28 46.4664 569.33 38.3067 753.82 0.0000 345.93 50.4802 946.00 38.3095 756.73 16.1240 351.06 40.7289 569.70 39.4405 756.80 14.6587 351.93 40.7531 583.19 23.8173 884.68 23.5188 Page 2928 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:58:47.82 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM30.CNF;300 Background date : Z-OCT-2016 11:01:47. Sample date 10-DEC-2015 14:30:00 Acquisition date : 3-0CT-2016 07:57:26. Sample ID G405235002 Sample.quantity : 1.23837E+02 GRAM Detector name : GAM30 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 2 *2 2 0 0 0 2 2 0 3 3 0 2 2 0 0 5 5 2 2 0 0 3 3 0 0 0 0 0 0 Page 2930 of 5809 Energy 63.20* 72. 96 74.81 77.12* 87.18 89.84 92.75* 105.57 186.31* 209.30 238.71* 241. 88 270.44 295.25* 300.21 331. 7 6* 338.35* 341.35 352.21* 387.36 430.57 433.18 463.17 466.96 511.12* 524.39 583.26* 587.03 609.64* 639.66 660.26. 666.48 727.68 737.36 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 16 37 170 277 96 66 93 39 88 49 530 122 43 185 28 83 112 22 259 19 15 24 38 14 35 15 97 15 186 25 44 31 58 15 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 128 158 155 129 181 141 140 134 173 89 59 62 116 38 59 97 38 51 74 50 7 9 20 18 58 26 18 12 31 28 33 12 12 16 1.12 12 6 .12 1.31 145.65 1.31 149.35 1.10 153.97 1.19 174.09 0.97 179.40 1.23 185.22 1.15 210.87 1.18 372.35 1.00 418.34 1.20 477.15 1.44 483.50 1.50 540.64 1.25. 590.25 1.65 600.18 7.88 663.28 1.45 676.47 1.54 682. 46 1.34 704.19 1.86 774.49 1.54 860.93 1.64 866.14 1.65 926.14 1.50 933.73 1.97 1022.06 1.69 1048.59 1.39 1166.36 1.92 1173.92 1.39" 1219.15 3.74 1279.20 7.52 1320.41 0.67 1332.84 2.21 1455.27 0.78 1474.65 123 142 142 142 169 169 169 207 365 415 471 471 536 585 585 652 672 672 699 767 859 859 919 919 1015 1041 1162 1162 1213 1271 1309 1328 1448 14.71 7 4.52E-03122.3 17 1.03E-02 65.1 1.24E+OO 17 4.72E-02 15.1 17 7.68E-02 *9.3 25 2.66E-02 23.7 2.94E+OO 25 1. 82E-02 30. 4 25 2.59E-02 25.9 10 1. 09E-02 57. 3 14 2.43E-02 34.5 8 1. 37E-02 35. 8 18 l.47E-01 5.0 2.23E+OO 18 3.40E-02 16.6 13 1.20E-02 53.1 27 5.13E-02 9.6 1.17E+OO 27 7.74E-03 54.9 20 2.32E-02 31.4 21 3.12E-02 14.4 3.34E+OO 21 6.02E-03 60.7 13 7.19E-02 9.4 10 5.29E-03 73.1 11 4.04E-03 32.2 7.52E-01 11 6.72E-03 32.8 31 1.05E-02 29.8 1.95E+OO 31 3.98E-03 62.2 17 9.64E-03 60.7 10 4.07E-03 73.5 15 2.70E-02 13.8 2.37E+OO 15 4.llE-03 42.9 14 5.17E-02 9.9 14 7.02E-03 48.6 20 1.22E-02 36.2 12 8.61E-03 28.7 16 1.60E-02 18.8 7 4.27E....:03 49.7 Peak Search Report (continued) Page : 2 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 794.89 31 10 1. 34 1589.74 1585 10 8. 61E-03 26. 2 36 0 851. 32 14 2 0.66 1702.64 1699 8 3.98E-03 31. 2 37 0 860.49 37 14 ,..1. 26 1720.98 1715 12 l.03E-02 26. 4 38 . 0 911. 52 111 27 1. 55 1823.07 1817 14 3.09E-02 13.5 39 0 935.80 26 3 2.68 1871.64 1867 10 7.31E-03 22.6 40 5 964.58* 22 32 2.64 1929.22 1921 27 6.24E-03 63.9 8.74E-01 41 5 969. 20* 50 22 1. 87 1938.48 1921 27 l.39E-02 23.9 42 0 1065.20 8 13 0.77 2130.55 2124 11 2.lOE-03101.3 43 0 1115. 32 11 14 1. 38 2230.82 2223 14 3.06E-03 78.2 44 0 1121.17* 57 7 2.07 2242.53 2236 14 1. 59E-02 16.8 45 0 1167. 01 19 20 5.96 2334.25 2325 16 5.34E-03 56.7 46 0 1212.44 9 14 0.66 2425.14 2420 7 2.59E-03 73.9 47 0 1238.24 21 12 1. 35 2476.76 2469 12 5.83E-03 39.6 48 0 1328.10 6 5 1. 03 2656 .. 58 2652 7 l.64E-03 76.0 49 0 1378.05 16 2 1. 36 2756.53 2751 10 4. 37E-03 31. 3 50 0 1393. 55* 4 4 1. 41 2787.55 2781 8 l.16E-03101.2 51 0 1430.88 6 5 1. 40 2862.25 2855 10 1. 67E-03 80.8 52 0 1461.22* 432 10 1. 91 2922.95 2916 14 l.20E-01 5.1 53 0 1547.80 9 0 0.88 3096. 22 3091 10 2.50E-03 33.3 54 0 1731.15 7 5 0.77 3463.13 3455 10 l.92E-03 71.6 55 0 1765.18* 23 ' 6 3.09 3531.24 3526 11 6.51E-03 30.0 Flag: "*" = Peak area was modified by background subtraction Page 2931 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:58:50 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 10-DEC-2015 14:30:00 G405235002 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:57:26 123.84 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA30 0 01:00:00.00 1.50 keV No Empirical 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 2932 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line-EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 RA-224 240.99 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.45 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.307E+OO 1.784E+Ol l.784E+Ol 10.20 OK ZN-65 1115. 54 50.60* l.652E+OO 7.695E-02 1. 792E-01 156.41 OK CD-109 88.03 3.70* 6.548E+OO l.395E+OO 2.183E+OO 92.25 OK SN-126 64.28 9.60 3.867E+OO 3.007E-01 3.007E-01 244.55 OK 86.94 8.90 6.548E+OO 5.801E-01 5. 801E-01 92.25 OK 87.57 37.00* 6.548E+OO 1.395E-01 1.395E-01 92.25 OK BA-137M 661.66 89.90* 2.546E+OO 1.156E-01 1.178E-01 72.35 OK CS-137 661. 66 85.10* 2.546E+OO l.222E-01 1.245E-01 72. 35 OK EU-155 86.55 30.70 6.548E+OO 1.682E-01 l.894E-01 92.25 OK 105.31 21.10* 7.284E+OO 1.703E-01 l.918E-01 114. 53 OK TL-208 277.37 6.60 4.820E+OO Line Not Found Absent 583.19 85.00* 2.799E+OO 2.485E-01 2.485E-01 27.65 OK 860.56 12.50 2.059E+OO 8.550E-01 8.550E-01 52.88 OK PB-212 74.82 10.28 5.441E+OO l.291E+OO 1.291E+OO 49.80 OK 77 .11 17.10 5.693E+OO 1.928E+00 1.928E+OO 18.63 OK 238.63 43.60* 5.356E+OO 1.449E+OO 1.449E+OO 10.08 OK 300.09 3.30 4.554E+OO 1.169E+OO l.169E+OO 109.89 OK BI-214 609.32 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 OK 1120 .'29 14.92 . 1. 644E+OO 1.366E+OO 1.366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7. 771E-01 59.97 OK PB-214 74.82 5.80 5.442E+OO Line Not Found <<INT Reject 77 .11 9.70 5.693E+OO 3.400E+OO 3.401E+OO 18.63 OK 87.09 3.41 6.542E+OO Line Not Found <<INT Reject 242.00 7.25 5.305E+OO Line Not Found <<INT Reject 295.22 18.42 4.609E+OO 1. 374E+OO 1.375E+OO 19.23 OK 351.93 35.60* 4.058E+OO 1.119E+OO 1.120E+OO 18.84 OK RN-222 609.32 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 OK 1120. 29 14.92 1.644E+OO l.366E+OO 1. 366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7.771E-01 59.97 OK RA-224 240.99 4.10* 5.307E+OO 1.160E+OO 1.160E+OO 110.62 OK RA-226 609.32 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 OK 1120.29 14. 92. l.644E+OO

1. 366E+OO 1. 366E+OO 33.69 OK 1764.49 15.30 -l.121E+OO 7.769E-01 7.771E-01 59.97 OK AC-228 105.21 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 OK 338.32 11. 27 4.178E+OO l.494E+OO 1. 494E+OO 28.78 OK 794.95 4.25 2.197E+OO 1.980E+OO 1.980E+OO 52.41 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO 1.298E+OO 1. 298E+OO 26.93 OK 968. 97 15.80 1.863E+OO 9.990E-Ol 9.990E-01, 47.84 OK RA-228 105.21 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 OK 338.32 11. 27 4.178E+OO 1.494E+OO 1.494E+OO 28.78 OK 794.95 4.25 2.197E+OO l.980E+OO l.980E+OO 52.41 OK 835.71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO 1.298E+OO 1. 298E+OO 26.93 OK 968.97 15.80 1.863E+OO 9.990E-01 9.990E-01 47.84 OK TH-228 74.82 10.28 5.441E+OO 1.291E+OO 1.291E+OO 49.80 OK 77 .11 17.10 5.693E+OO 1.928E+OO 1.928E+OO 18. 63. OK 238.63 43.60* 5.356E+OO 1.449E+OO 1.449E+OO 10.08 OK 300.09 3.30 4.554E+OO 1.169E+OO 1.169E+OO 109.89 OK Page 2933 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status TH-230 609.32 45.49* 2.707E+OO 9.149E-01 9.149E-01 19.80" OK 1120. 29 14.92 1.644E+OO 1.366E+OO 1.366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 OK PA-231 283.69 1. 70 4.743E+OO Line Not Found. Absent 301.36 5.35* 4.554E+OO 7. 211E-01 7.211E-01 *109.89 OK TH-232 105.21 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114.53 *OK 338.32 11. 27 4.178E+OO 1.494E+OO 1.494E+OO 28.78 OK 835.71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO l.298E+00 1. 298E+OO 26.93 OK 968. 97 15.80 1.863E+OO 9.990E-01 9.990E-01 47.84 OK TH-234 63.29 3.70* 3.867E+OO 7.801E-01 7.801E-01 244.55 OK 92.59 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 OK U-234 609.32 45.49* 2.707E+00 9.149E-01 9.149E-01 19.80 OK 1120.29 14.92 1.644E+OO 1.366E+00 1.366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 OK U-235 89. 96 3.47 6.713E+OO l.893E+OO 1.893E+OO 60.80 OK 93.35 5.60 6.868E+OO 1.628E+OO 1. 628E+OO 51. 86 OK 143.76 10.96* 7.121E+OO Line Not Found *-----Absent 163.33 5.08 6.750E+OO Line Not Found Absent 185. 72 57.20 6.287E+OO 1.577E-01 l.577E-01 69.06 OK 205.31 5.01 5.922E+OO Line Not Found Absent U-238 63.29 3.70* 3.867E+OO 7. 801E-01 7.801E-01 244.55 OK 92.59 4.23 6.868E+OO 2.155E+.00 2.155E+OO 51. 86 OK AM-243 43.53 5.90 8.765E-01 Line Not Found Absent 74.66 67.20* 5. 441E+OO 1. 97 5E-.01 1. 975E-01 49.80 OK CF-249 252.80 2.50 5.147E+OO Line Not Found Absent 333.37 14.60 4.223E+OO Line Not Found Absent 388.16 66.00* 3.787E+OO 4.741E-02 4.748E-02 146.17 OK ANH-511 511. 00 100.00* 3.091E+OO 6.875E-02 6 .. 875E-02 121. 32 OK Flag: "*" = Keyline Page 2934 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:58:51.71 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l *
Acquisition date 3-0CT-2016 07:57:26 Sensitivity : 3.000 *
Detector ID GAM30 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
Sample date 10-DEC-2015 14:30:00 Analyst initials: MXRl *
Sample ID G405235002 Sample Quantity 1.2384E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date : ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 9 6-sigma) K-40 1.784E+Ol 1.782E+OO ZN-65 1. 792E-01 2.747E-01 CD-10.9 2.183E+00 1.973E+OO *SN-126 1.395E-01 1.262E-01 BA-137M 1.178E-01 8.354E-02 CS-137 1.245E-01 8.825E-02 EU-155 l.918E-01 2.153E-01 TL-208 2.485E-01 6.732E-02 PB-212 1.449E+OO l.431E-01 BI-214 9.152E-01 1. 775E-01 PB-214 1 .. 120E+OO 2.068E-01 RN-222 9.152E-01 1. 775E-01 RA-224 1.160E+OO 1.258E+OO RA-226 9.152E-01 1.775E-01 AC-228 1.298E+OO 3.426E-01' RA-228 1.298E+OO 3.426E-01 TH-228 1.449E+OO 1. 431E-01 TH-230 9.149E-01 1. 775E-01 PA-231 7. 211E-01 7.766E-01 TH-232 1.298E+OO 3.426E-01 TH-234 7.801E-01 1.870E+OO U-234 9.149E-Ol l.775E-01 U-235 5.447E-02 1. 765E-01 U-238 7.801E-Ol l.870E+OO AM-243 1.975E-Ol 9. 638.E-02 CF-249 4.748E-02 6.802E-02 ANH-511 6.875E-02 8.174E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 2935 of 5809 Key-Line Activity (pCi/GRAM -5.252E+OO 2.002E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.lOlE+Ol 4.927E-02 1. 960E+41 MDA (pCi/GRAM 6.674E-01 2.520E-01 l.831E+OO 1.176E-01 5.633E-02 5. 951E-02 1. 766E-01 *6.449E-02 9.642E-02 8.187E-02 1.155E-01 8.187E-02 1.033E+OO 8.187E-02 2.069E-01 2.069E-01 9.642E-02 8.184E-02 8.034E-01 2.069E-01 1.939E+OO 8.184E-02 3.287E-01 1.939E+OO 7.383E-02 6.705E-02 4.622E-02 MDA (pCi/GRAM l.916E+Ol l.049E-Ol O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 1.369E-03 2.682E-02 6. 071E-02 NOT IDENT. SC-46 1.978E-01 3.668E-01 7.672E-01 FAIL ABUN V-48 O.OOOE+OO l.554E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 3.903E+02 O.OOOE+OO SHORT HLIF MN-54 5.343E-02 6.886E-02 1.437E-01 NOT IDENT. C0-56 2.914E-01 4.921E-01 9.506E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 689E+41 O.OOOE+OO SHORT HLIF C0-57 -5.272E-02 4. 967E-02 8.267E-02 NOT IDENT. C0-58 -2.314E-01 4.909E-01 8.752E-01 NOT IDENT. FE-59 4.032E+OO 6.865E+OO 1.428E+Ol NOT IDENT. C0-60 -1.437E-02 4.976E-02 9.113E-02 NOT IDENT. GE-68 -2.439E+OO 2.787E+OO 4.454E+OO NOT IDENT. AS-73 3.034E+OO 7. 472E+OO 1.464E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.971E+03 0.000E+OO SHORT HLIF SE-75 5.062E-02 2.085E-01 3.827E-01 NOT IDENT. BR-77 O.OOOE+OO l.395E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.441E+02 O.OOOE+OO SHORT HLIF RB-83 -l.OlOE-01 7.256E-01 1.230E+OO NOT IDENT. KR-85 1.877E+OO 6.059E+OO i.224E+Ol NOT IDENT. SR-85 l.922E-01 6.260E-01 1.265E+OO NOT IDENT. RB-86 O.OOOE+OO 3.177E+04 O.OOOE+OO SHORT HLIF Y-88 -7.362E-02 1.373E-01 2.849E-01 NOT IDENT. Y-91 2. 211E+Ol 5.808E+02 1.084E+03 NOT IDENT. NB-94 -3.826E-03 3.251E-02 6.065E-02 NOT IDENT. NB-95 -1.197E+OO 9.999E-01 1.569E+OO NOT IDENT. NB-95M 1.723E+OO 2.489E+OO 4.477E+OO NOT IDENT. ZR-95 9.690E-01 1.418E+OO 2.980E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.281E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1.948E-02 3.571E-02. 6.210E-02 NOT IDENT. RH-102 4.200E-02 5.459E-02 l. l 72E-01 NOT IDENT. RU-103 3.008E+OO 5.206E+OO 1.083E+Ol FAIL ABUN RH-106 3.384E-01 4.781E-01 1. OllE+OO NOT IDENT. RU-106 3.384E-01 4. 781E-01 1. OllE+OO NOT IDENT. AG-108M 4.739E-02 3.046E-02 4.786E-02 FAIL ABUN AG-llOM -8.785E-02 9.486E-02 l.497E-01 NOT IDENT. SN-113 4.570E-02 2.014E-01 4.059E-01 NOT IDENT. CD-115 0.000E+OO l.549E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 8. 813E+04 O.OOOE+OO SHORT HLIF TE-123M 8.256E-02 1.258E-01 2.419E-01 NOT IDENT. SB-124 -7.328E-01 2.022E+OO 3.914E+OO NOT IDENT. SB-125
4.379E-02 1.152E-01 2. ll 7E-01 FAIL ABUN TE-125M 8.068E-01 2.778E+02 4.673E+02 NOT IDENT. I-126 O.OOOE+OO l.080E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.004E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.524E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 4.394E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 5.620E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.627E+26 0.000Et00 SHORT HLIF BA-133 -3.670E-03 4 .171E-02 7.281E-02 NOT IDENT. I-133 O.OOOE+OO 1.130E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.647E-02 l.205E-01 FAIL ABUN CS-135 4.649E-02 1.530E-01 .2. 611E-01 . NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.317E+05 O.OOOE+OO SHORT HLIF CE-139 1. 710E-03 l.169E-01 2.107E-01 NOT IDENT. BA-140 O.OOOE+OO l.067E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.015E+05 O.OOOE+OO SHORT HLIF CE-141 -5.014E+OO 2.309E+Ol 4. lllE+Ol NOT IDENT. CE-143 O.OOOE+OO 1.665E+41 O.OOOE+OO SHORT HLIF CE-144 9.386E-03 3.450E-01 6.333E-01 NOT IDENT. PM-144 2.222E-03 5.523E-02 1.084E-01 NOT IDENT. PR-144 1. 775E-01 4.789E+OO 9.394E+OO NOT IDENT. PM-146 4.628E-02. 4. 510E-.02 9. 611E-02 FAIL ABUN ND-147 O.OOOE+OO 2.628E+07 O.OOOE+OO SHORT HLIF PM-147 1. 446E+03 7.769E+02 1. 641E+03 NOT IDENT. PM-149 O.OOOE+OO 2.674E+40 0.000E+OO SHORT HLIF EU-150 l.870E-02 3.044E-02 5.659E-02 FAIL ABUN EU-152 -1. 7 98E-03 9.207E-02 1.629E-01 FAIL ABUN GD-153 -6.544E-02 1. 732E-01 2.840E-01 NOT IDENT. EU-154 4.660E-02 1.204E-01 2.560E-01 NOT IDENT. TB-160 -3.604E-02 2.009E+OO 3.794E+OO FAIL ABUN H0-166M 8.084E-03 5.809E-02 l.129E-01 NOT IDENT. TM-171 -2.052E-01 1. 746E+Ol 3.327E+Ol NOT IDENT. HF-172 1. 331E-01 2.256E-01 4.322E-01 FAIL ABUN LU-172 3.109E-02 7.343E-02 1.518E-Ql FAIL ABUN Page 2936 of 5809 LU-176 -3.930E-03 2.940E-02 4.668E-02 FAIL ABUN HF-181 1.039E+OO 3.943E+oo* 7.927E+OO NOT IDENT. TA-182 2.800E-02 9.320E-01 1. 866E+OO FAIL ABUN RE-183 -9.476E-02 2.642E+OO 4. 972E+OO NOT IDENT. RE-184 -2.167E+OO 2.852E+Ol 5. 396E+Ol NOT IDENT. W-188 5.014E+Ol 1. 2 68E+02 2.174E+02 FAIL ABUN IR-192 -1.458E-02 4.490E-01 8.747E-01 FAIL ABUN HG-203 -1.183E+OO 2.437E+OO 4. 072E+OO FAIL ABUN BI-207 1. 742E-02 4. 722E-02 9.617E-02 FAIL ABUN PB-210 3.524E-01 2.359E+OO 4.605E+OO NOT IDENT. BI-211 O.OOOE+OO 5.695E-01 8.315E-01 FAIL ABUN PB-211 4.493E-01 6.822E-01 1.403E+OO NOT IDENT. BI-2-12 O.OOOE+OO 8. llSE-01 1.330E+OO FAIL ABUN RN-219 -6.924E-02 3.679E-01 7.0lSE-01 FAIL ABUN RA-223 4.601E-02 6.537E-01 1.159E+OO FAIL ABUN AC-227 1. 881E-02 2.380E-01 4.276E-01 FAIL ABUN TH-227 l.881E-02 2.380E-01 4.276E-01 FAIL ABUN TH-229 2.042E-01 4.583E-01 8.605E-01 FAIL ABUN TH-231 4.601E-02 6.537E-01 1.159E+OO FAIL ABUN PA-233 -1. 265E-02 5.819E-02 1.116E-01 FAIL ABUN PA-234 9.521E-03 2.502E-01 4.885E-01 NOT IDENT. PA-234M -2.099E+OO 4. 725E+OO 8.194E+OO NOT IDENT. NP-237 -1. 265E-02 5.819E-02 1.116E-01 FAIL ABUN NP-238 O.OOOE+OO 1.097E+41 O.OOOE+OO SHORT HLIF NP-239 5.193E-03 2.345E-01 4.312E-01 FAIL ABUN PU-239 3.268E+02 3.267E+02 6.386E+02 NOT IDENT. AM-241 5.439E-02 l.330E-01 2.406E-01 NOT IDENT. CM-243 -1.163E-02 9. 611E-02 l.625E-01 NOT. IDENT. BK-247 -1. 203E-02 7.576E-02 l.324E-01 FAIL ABUN CM-247 -5.026E-03 3.442E-02 6.584E-02 NOT IDENT. CF-251 -1.778E-01 l.232E-01 1.907E-01 NOT IDENT. Page 2937 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:58:48.94 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 410 10.66* 1.307E+OO l.784E+Ol 1. 784E+Ol 10.20 ZN-65 1115. 54 11 50 .. 60* 1.652E+OO 7.695E-02 l.792E-01 156.41 CD-109 88.03 106 3.70* 6.548E+oo* 2.662E+OO 4.163E+OO 47.48 SN-126 64.28 18 '9. 60 3.867E+OO 3.007E-01 3.007E-01 244.55 86.94 106 8.90 6.548E+OO 1.107E+OO l.107E+OO 47.48 87.57 106 37.00* 6.548E+OO 2.662E-01 2.662E-01 47.48 BA-137M 661.66 44 89.90* 2.546E+OO 1.156E-01 1.178E-01 72 .35 CS-137 661.66 44 85.10* 2.546E+OO 1.222E-01 *1. 245E-01 72 .35 EU-155 86.55 106 30.70 6.548E+OO 3.208E-01 3.613E-01 47.48 105.31 43 21.10* 7.284E+OO l.703E-01 l.918E-01 114. 53 TL-208 277.37 ------6.60 4.820E+OO ------Line Not Found ------583.19 98 85.00* 2.799E+OO 2.485E-01 2.485E-01 27.65 860.56 36 12.50 2.059E+OO 8.550E-01 8.550E-01 52.88 BI-211 72.87 41 1.23 5.224E+OO 3.913E+OO 3.913E+OO 130.26 351.06 267 12.92* 4.058E+OO 3.084E+OO 3.084E+OO 18.84 PB-212 74.82 191 10.28 5.441E+OO 2.066E+00 2. 066E+OO' 30.27 77 .11 310 17.10 5.693E+00 1.928E+OO 1.928E+OO 18.63 238.63 558 43.60* 5.356E+OO 1.449E+OO .1.449E+OO 10.08 300.09 29 3.30 4.554E+OO l.169E+OO 1.169E+OO 109.89 BI-214 609.32 186 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 1120.29 55 14.92 1.644E+OO 1.366E+00 l.366E+00 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7.771E-01 59.97 PB-214 74.82 191 5.80 5.441E+OO 3.662E+OO 3.663E+OO 30.27 77 .11 310 9.70 5.693E+OO 3.400E+OO 3.401E+OO 18.63 87.09 106 3.41 6.548E+OO 2.888E+OO 2. 88,9E+OO 47.48 242.00 129 7.25 5.307E+OO 2.030E+OO 2.031E+OO 33.30 295.22 192 18.42 4.609E+00 1.374E+OO 1.375E+OO 19.23 351. 93 267 35. 607\c 4.058E+OO l .119E+OO 1.120E+OO 18.84 .RN-222 609.32 186 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 1120.29 55 14.92 1. 644E+OO 1. 366E+OO l.366E+00 1764.49 22 15.30 1.121E+OO 7.769E-01 7.771E-01 59.97 RA-224 240.99 129 4.10* 5.307E+OO 3.590E+00 3.590E+OO 33.30 RA-226 609.32 186 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 1120.29 55 14.92 1.644E+OO 1.366E+OO 1.366E+OO 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7. 771E-01 59.97 AC-228 105.21 43 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 338.32 116 11.27 4.178E+OO 1.494E+OO 1.494E+00 28.78 794.95 31 4.25 2.197E+OO 1. 980E+OO l.980E+00 52.41 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911.20 108 25.80* 1. 962E+OO 1.298E+OO 1.298E+OO 26.93 968. 97 49 15.80 1. 8 63E+OO 9.990E-01 9.990E-01 47.84 RA-228 105.21 43 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 338.32 116 11. 27 4.178E+OO 1.494E+OO l.494E+OO 28.78 794.95 31 4.25 2.197E+OO l.980E+OO 1.980E+OO 52.41 835.71 ------1. 61 2.109E+00 ------Line Not Found ------911.20 108 25.80* 1. 962E+OO l.298E+OO 1.298E+OO 26. 93 968.97 49 15.80 1.863E+00 9.990E-01 9.990E-01 47.84 Page 2938 of 5809 Nuclide Line Activity Report (contim,ied) Page : 2 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 191 10.28 5.441E+OO 2.066E+OO 2.066E+OO 30.27 77 .11 310 17.10 5.693E+OO 1.928E+OO 1.928E+OO 18.63 238.63 558 43.60* 5.356E+OO 1. 449E+OO 1.449E+OO 10.08 300.09 29 3.30 4.554E+OO 1.169E+OO l.169E+OO 109.89 TH-230 609.32 186 45. 4'9* 2.707E+OO 9.149E-01 9.149E-01 19.80 1120.29 55 14.92 1.644E+OO l.366E+OO 1.366E+OO 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 PA-231 283.69 ------1. 70 4.743E+OO ------Line Not Found ------301.36 29 5.35* 4.554E+OO 7.211E-01 7. 211E-01 109.89 TH-232 105.21 43 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 338.32 116 11. 27 4.178E+OO 1.494E+OO 1.494E+OO 28.78 835. 71 ------1. 61 2.109E+OO ------Line Not Found ------911. 20 108 25.80* 1. 962E+OO 1. 298E+OO l.298E+OO 26.93 968. 97 49 15.80 1. 863E+OO 9.990E-01 9.990E-01 47.84 TH-234 63.29 18 3.70* 3.867E+OO 7. 801E-01 7.801E-01 244.55 92. 59. 103 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 U-234 609.32 186 45.49* 2.707E+OO 9.149E-01 9.149E-01 19.80 1120.29 55 14.92 1.644E+OO 1. 366E+OO 1.366E+OO 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 U-235 89. 96 73 3.47 6.713E+OO 1.893E+OO 1. 893E+00 60.80 93.35 103 5.60 6.868E+OO 1.628E+OO 1.628E+OO 51. 86 143.76 ------10. 96* 7.121E+OO ------Line Not Found ------163.33 ------5.08 6.750E+OO ------Line Not Found ------185.72 94 57.20 6.287E+OO 1.577E-01 1.577E-01 69.06 205.31 ------5.01 5.922E+OO ------Line Not Found ------U-238 63.29 18 3.70* 3.867E+OO 7. 801E-01 7.801E-01 244.55 92.59 103 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 AM-243 43.53 ------5.90 8.765E-01 ------Line Not Found ------74.66 191 67.20* 5.441E+OO 3.161E-01 3.161E-01 30.27 CF-249 252.80 ------2.50 5.147E+OO ------Line Not Found ------333.37 ------.14.60 4. 223E+OO* ------Line Not Found ------388.16 20 66.00* 3.787E+OO 4.741E-02 4.748E-02 146.17 ANH-511 511. 00 35 100.00* 3.091E+OO 6.875E-02 6.875E-02 121. 32 Flag: "*" Key line Page 2939 of 5809 Page : 3 Summary of *Nuclide Activity Sample ID : G405235002 Acquisition date : 3-0CT-2016 07:57:26 Total number of lines in spectrum 55 Number of unidentified lines 17 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 . RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Hlife l.25E+09Y 244.06D 461.40D 2.30E+05Y 30.08Y 30.08Y 4.75Y 1.41E+10Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1: 41E+l0Y . 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 351.00Y l.OOE+09Y Decay 1. 00 2.33 i. 56 1. 00 1. 02 1. 02 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 784E+Ol 7.695E-02 2.662E+OO 2.662E-01 l.156E-01 1.222E-01 1. 703E-01 2.485E-01 3.084E+OO 1.449E+OO 9.149E-01 1.119E+OO 9.149E-01 3.590E+00 9.149E-01 l.298E+OO 1.298E+OO 1.449E+OO 9.149E-01 7.211E-01 l.298E+OO 7. 801E-01 9.149E-01 l.577E-01 7.801E-01 3.161E-01 4.741E-02 6.875E-02 4.353E+Ol 4.353E+Ol Decay Corr pCi/GRAM 1. 784E+Ol l.792E-01 4.163E+OO 2.662E-01 l.178E-01 1.245E-01 1.918E-01 2.485E-01 3.084E+OO 1.449E+OO 9.152E-01 l.120E+OO 9.152E-01 3.590E+OO 9.152E-01 l.298E+00 1.298E+OO l.449E+OO 9.149E-01 7. 211E-01 1.298E+OO 7.801E-01 9.149E-01 1.577E-01 7.801E-01 3.161E-01 4.748E-02 6.875E-02 4.516E+Ol 4.516E+Ol 69.09% Decay Corr 2-Sigma Error 0.182E+Ol 2.803E-01 1.977E+OO 1. 2 64E-01 0.852E-01 0.901E-01 2.197E-01 0.687E-01 0.581E+OO 0.146E+OO 1. 812E-01 0.211E+OO 1.812E-01 1.195E+OO 1.812E-01 '0.350E+OO 0.350E+OO 0.146E+OO 1. 811E-01 7.924E-01 0.350E+OO 19.08E-01 1. 811E-01 1.089E-01 19.08E-01 0.957E-Oi 6. 941E-02 8. 341E-02 "M" Manually accepted 2-Sigma %Error 10.20 156.41 47.48 47.48 .72.35 72.35 114. 53 27.65 18.84 10.08 19.80 18.84 19.80 33.30 19.80 26.93 26.93 10.08 19.80 109.89 26.93 244.55 19.80 69.06 244.55 30.27 146.17 121.32 Flags: "K" Keyline not found "E" = Manually edited "A" = specific abn. limit Page 2940 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235002 Acquisition date : 3-0CT-2016 07:57:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.30 53 94 1. 00 418.34 415 8 1.37E-02 71. 6 5.85E+OO 0 270.44 45 121 1. 50 540.64 536 13 1. 20E-02 **** 4.91E+OO T 0 331..76 86 100 7.88 663.28 652 20 2.32E-02 62.8 4.24E+OO 2 341.35 22 53 1. 54 682.46 672 21 6.02E-03 **** 4.15E+OO T 5 430.57 15 *8 1. 54 860.93 859 11 4.04E-03 64.4 3.51E+OO 5 433.18 25 9 1. 64 866.14 859 11 6.72E-03 65.6 3.49E+OO T 2 463 .17 38 20 1. 65 926.14 919 31 1.05E-02 59.6 3.32E+OO T 2 466.96 15 18 1. 50 933.73 919 31 3.98E-03 **** 3.30E+OO T 0 524.39 15 27 1. 69 1048.59 1041 10 4.07E-03 **** 3.03E+OO 3 587.03 15 12 1. 92 1173.92 1162 15 4. llE-03 85.8 2.79E+OO 0 639.66 25 28 3.74 1279.20 1271 14* 7.02E-'03 97.2 2.61E+OO 0 666.48 31 12 0.67 1332. 84 1328 12 8.61E-03 57.3 2.53E+00 T 0 727.68 57 12 2.21 1455.27 1448 16 l.60E-02 37.7 2.36E+OO T 0 737.36 15 15 0.78 1474.65 1471 7 4.27E-03 99.5 2.33E+OO T 0 851. 32 14 2 0.66 1702.64 1699 8 3.98E-03 62.5 2.08E+OO 0 935.80 26 3 2.68 1871.64 1867 10 7.31E-03 45.1 1. 92E+OO 5 964.58 22 31 2. 64 1929.22 1921 27 6.24E-03 **** 1.87E+OO T 0 1065.20 7 13 0.77 2130.55 2124 11 2.lOE-03 **** 1. 72E+OO 0 1167. 01 *18 19 5. 96 2334.25 2325 16 5.34E-03 **** 1. 59E+OO 0 1212.44 9 13 0.66 2425.14 2420 7 2.59E-03 **** 1.54E+OO 0 1238.24 20 11 1. 35 2476.76 2469 12 5.83E-03 79.1 1. 51E+OO T 0 1328.10 6 5 1. 03 '2656.58 2652 7 1. 64E-03 **** 1.42E+OO 0 1378.05 15 2 1. 36 2756.53 2751 10 4.37E-03 62.6 1. 37E+OO 0 1393.55 4 4 1. 41 2787.55 2781 8 l.16E-03 **** 1.36E+OO 0 1430.88 6 5 1. 40 2 8 62 . 2 5. 2 8 5 5 10 1.67E-03 **** 1. 33E+OO 0 1547.80 9 0 0.88 3096. 22 3091 10 2.50E-03 66.7 l.25E+OO 0 1731.15 6 5 0.77 3463.13 3455 10 1. 92E-03 **** 1.14E+OO Flags: "T" = Tentatively associated Page 2941of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:59:09.04 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l * *Acquisition date 3-0CT-2016 07:57:26 Sensitivity 3.000 *
Detector ID GAM30 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
Sample date 10-DEC-2015 14:30:00 Nuclide Library : SOLID *
Sample ID G405235002 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.2384E+02 GRAM * *Wet wt corr 1.00000 Wet Weight. 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry :. CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7 .
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Le (pCi/GRAM 2,750E-01 1.031E-01 8.616E-01 5.532E-02 2.448E-02 2.586E-02 8.214E-02 2.877E-02 4.464E-02 3.421E-02 5.198E-02 3.421E-02 4.783E-01 3.421E-02 8. 719E-02 8. 719E-02 4.464E-02 3.420E-02 3.674E-01 8.719E-02 9.105E-01 3.420E-02 l.536E-01 9.105E-01 3.459E-02 3.019E-02 2. 043E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 2942 of 5809 Le (pCi/GRAM 8. 396E+00 4.554E-02 O.OOOE+OO 2.292E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-'-56 C0-57 C0-58 FE-59 C0-60 GE.:...68 AS-73 AS-74 SE-75* BR-77. SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132

TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 2943 of 5809 3.354E-01 O.OOOE+OO O.OOOE+OO .6.429E-02 4.182E-01 O.OOOE+OO 3.849E-02 3.670E-01 6.244E+00 3.912E-02 l.906E+OO 6.849E+OO O.OOOE+OO 1. 754E-01 O.OOOE+OO O.OOOE+OO 5.487E-01 5.468E+OO 5.647E-01 0.000E+OO 9.004E-02 4.726E+02 2.692E-02 6. 931E-01 2.082E+00 1.323E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.905E-02 5.209E-02 4.862E+OO 4.509E-01 4.509E-01 2.129E-02 6.200E-02 1.825E-01 O.OOOE+OO O.OOOE+OO 1.127E-01 1.500E+OO 9.613E-02 2.182E+o2 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.289E-02 O.OOOE+OO 5. 451E-02* 1. 200E-01 O.OOOE+OO O.OOOE+OO 9.837E-02 O.OOOE+OO O.OOOE+OO 1.916E+Ol O.OOOE+OO 2.951E-01 4.818E-02 4.177E+OO 4.387E-02 O.OOOE+OO 7.709E+02 O.OOOE+OO 2.621E-02 7.356E-02 l.323E-01 1. llOE-01 1.662E+OO 5. OllE-02 1.549E+Ol 2.024E-01 6.539E-02 2.136E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT I DENT .. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT TDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. . FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 2944 of 5809 3.548E+OO 8.122E-01 2.331E+OO 2.326E+Ol 1.002E+02 3.998E-01 1.857E+OO 4.158E-02 2.139E+OO 4.00lE-01 6.414E-01 6.129E-01 3.167E-01 *5.309E-01 1. 966E-01 1. 966E-01 3.994E-01 5.309E-01 5.091E-02 2.082E-01 3.558E+.00 5. 091E-02 O.OOOE+OO 2.012E-01 3.012E+02 1.131E-01 7.556E-02 6.059E-02 2.979E-02 8.784E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.
VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:59:18.87 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l * *Acquisition date 3-0CT-2016 07:57:26 Sensitivity : 3.000 *
Detector ID GAM30 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
Sample date 10-DEC-2015 14:30:00 Nuclide Library : SOLID *
Sample ID G405235002 Analyst .initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.2384E+02 GRAM *
Quantity Err(%) : 1.6150E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************** * *
CALIBRATION INFORMATION * * *
Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1. 784E+Ol 2.389E+OO 2.389E+OO ZN-65 1. 792E-01 2.770E-01 2.770E-01 CD-109 2.183E+OO 2.007E+OO 2.007E+OO SN-126 l.395E-01 1.281E-01 l.281E-01 BA-137M 1.178E-01 8.405E_:_02 8.405E-02 CS-137 1.245E-01 8.879E-02 8.879E-02 EU-155 1.918E-01 2' .159E-01 2.159E-01 TL-208 2.485E-01 7.033E-02 7.033E-02 PB-212 1.449E+OO l.858E-01 l.858E-01 BI-214 9.152E-01 1.924E-01 1.924E-01 PB-214 1.120E+OO 2.265E-01 2.265E-01 RN-222 9.152E-01 l.924E-01 1.924E-01 RA-224 1.160E+OO l.292E+OO 1.292E+OO RA-226 9.152E-01 l.924E-01 l.924E-01 AC-228 1.298E+OO 3.876E-01 3.876E-01 RA-228 1. 2 98E+OO 3.876E-01 3. 876E-01 TH-228 1.449E+OO 1.858E-01 l.858E-01 TH-230 9.149E-01 l.923E-01 l.923E-01 PA-231 7.211E-01 7.933E-01 7.933E-01 TH-232 1.298E+OO 3.876E-01 3.876E-01 TH-234 7.801E-01 1.878E+OO 1.878E+OO U-234 9.149E-01 1.923E-01 l.923E:-01 5.447E-02 1. 765E-01 1. 765E-01 U-238 7.801E-01 1.878E+OO 1.878E+OO AM-243 1.975E-01 9. 910E-02' 9.910E-02 CF-249 4.748E-02 6.821E-02 6.821E-02 ANH-511 6.875E-02 8.194E-02 8.194E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) BE-7 -5.252E+OO 1.102E+Ol 1.127E+Ol NOT IDENT. NA-22 2.002E-02 4.930E-02 5.012E-02 NOT IDENT. NA-24 1.000E+41 1. 285E+42 O.OOOE+OO SHORT HLIF Page 2945 of 5809 AL-26 1.369E-03 2.682E-02 2.683E-02 NOT IDENT. SC-46. l.978E-01 3.677E-01 3.784E-01 FAIL ABUN V-48 l.221E+04 1.565E+04 l.659E+04 SHORT HLIF CR-51 -2.639E+02 3.909E+02 4.086E+02 SHORT HLIF MN-54 5.343E-02 6.914E-02 7.322E-02 NOT IDENT. C0-56 2.914E-01 4.934E-01 5.106E-01 FAIL ABUN MN-56 1.000E+41 1.693E+41 O.OOOE+OO SHORT HLIF C0-57 -5. 272E-02 *4. 981E-02 5.519E-02 NOT IDENT. .C0-58 -2.314E-Ol 4.916E-01 5.025E-01 NOT IDENT. FE-59 4.032E+OO 6.914E+OO 7.148E+OO NOT IDENT. C0-60 ....:.1. 437E-02 4.977E-02 5.019E-02 NOT IDENT. GE-68 -2.439E+OO 2.823E+OO 3.030E+OO NOT IDENT. AS-73 3.034E+OO 7.498E+OO 7.622E+OO NOT IDENT. AS-74 -2.159E+02 5.971E+03 5. 972E+03 SHORT HLIF SE-75 5.062E-02 2.085E-01 2.098E-01 NOT IDENT. BR-77 1.412E+38 1.214E+39 0.000E+OO SHORT HLIF SR-82 l.989E+02 6.444E+02 6.506E+02 SHORT HLIF RB-83 -1.0lOE-01 7.257E-01 7. 272E-01 NOT IDENT. KR-85 1.877E+OO 6.061E+OO 6.120E+OO NOT IDENT. SR-85 l.922E-01 6.262E-Ol* .. 6. 321E-01 NOT IDENT. RB-86 -2.369E+04 3.208E+04 3.381E+04 SHORT HLIF Y-88 -7.362E-02 1.374E-01 l.414E-01 NOT IDENT. Y-91 2. 211E+Ol 5.808E+02 5.809E+02 NOT IDENT. NB-94 -3.826E-03 3. 251E-02 3.256E-02 NOT IDENT. NB-95 -1.197E+OO l.007E+00 1.143E+OO NOT IDENT. NB-95M 1. 723E+OO 2.495E+OO 2.613E+OO NOT IDENT. ZR-95 9.690E-01 1.421E+OO 1.487E+OO NOT IDENT. NB:....97 1.000E+41 6.207E+41 *o.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1. 229E+42 O.OOOE+OO SHORT HLIF M0-99 -4.789E+31 1. 282E+32 O.OOOE+OO SHORT HLIF
TC-99M -1.000E+41 1. 414E+42 0.000E+OO SHORT HLIF RH-101 -l.948E-02 3.590E-02 3.696E-02 NOT IDENT. RH-102 4.200E-02 5.477E-02 5.795E-02 NOT IDENT. RU-103 3.008E+OO 5.212E+OO 5.386E+OO FAIL ABUN RH-106 3.384E-01 4.791E-01 5.028E-01 NOT IDENT. RU-106 3.384E-01 4.791E-01 5.028E-01 NOT IDENT. AG-108M 4.739E-02 3. 071E-02. 3. 741E-02 FAIL ABUN AG-llOM -8.785E-02 9.557E-02 1.035E-01 NOT IDENT. SN-113 4.570E-02 2.014E-01 2.025E-01 NOT IDENT. CD-115 l.004E+39 1. 561E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 6.973E+03 8.814E+04 8.819E+04 SHORT HLIF TE-123M 8.256E-02 1.259E-01 l.313E-01 NOT IDENT. SB-124 -7.328E-01 2.023E+OO 2.049E+OO NOT IDENT. SB-125 4.379E-02 1.153E-01 1.170E-01 FAIL ABUN TE-125M 8.068E-01 2.778E+02 2.778E+02 NOT IDENT. I-126 1.922E+06 1.118E+06 1. 414E+06 SHORT HLIF SB-126 8. 688E+o4 1.004E+06 1. 005E+o6 SHORT HLIF SB-127 -3. 331E+21 1.591E+22 O.OOOE+OO SHORT HLIF I-131 3.100E+09 4.402E+09 4.618E+09 SHORT HLIF I-132 1.000E+41 1.836E+42 O.OOOE+OO SHORT HLIF TE-132 1. 363E+26 2.685E+26 O:OOOE+OO SHORT HLIF BA-133 -3.670E-03 4 .171E-02 4.174E-02 NOT IDENT. I-133 -l.OOOE+41 2.124E+41 O.OOOE+OO SHORT HLIF CS-134 1.294E-01 6. 790E-"02 8. 951E-02 FAIL ABUN CS-135 4.649E-02 l.530E-01 l.545E-01 NOT IDENT. I-135 -l.000E+41 2.665E+42 O.OOOE+OO SHORT HLIF CS-136 l.536E+04 3.317E+05 3.317E+05 SHORT HLIF CE-139 1. 710E-03 1.169E-01 l.169E-01 NOT IDENT. BA-140 -7.668E+05 l.069E+06 l.124E+06 SHORT HLIF LA-140 -1. 87 5E+05 4.018E+05 4.106E+05 SHORT HLIF CE-141 -5.014E+OO 2.309E+Ol
2. 320E+Ol NOT IDENT. CE-143 1.000E+41 1.669E+41 O.OOOE+OO SHORT HLIF CE-144 9.386E-03 3.450E-01 3.450E-01 NOT IDENT. PM-144. 2.222E-03 5.523E-02 5.524E-02 NOT IDENT. PR-144 1. 775E-01 4.790E+OO 4.790E+OO NOT IDENT. PM-146 4.628E-02 4.534E-02 4.991E-02 FAIL ABUN ND-147 -9.633E+06 2.629E+07 2.665E+07 SHORT HLIF PM-147 1. 446E+03 7.833E+02 1. 01"9E+03 NOT IDENT. PM-149 -3.778E+39 2.675E+40 O.OOOE+OO SHORT HLIF EU-150 1.870E-02 3.048E-02 3.163E-02 FAIL ABUN EU-152 -l.798E-03 9.207E-02 9.208E-02 FAIL ABUN GD-153 -6.544E-02 l.733E-01 1. 758E-01 NOT IDENT. EU-154 4.660E-02 1.205E-01 1.223E-01 NOT IDENT. TB-160 -3.604E-02 2.009E+OO 2.009E+OO FAIL ABUN H0-166M 8.084E-03 5.809E-02 5.821E-02 NOT IDENT. TM-171 -2.052E-01 1. 746E+Ol 1. 746E+Ol NOT IDENT. HF-172 1.331E-01 2.268E-01 2.346E-01 FAIL ABUN LU-172 3.109E-02 7.372E-02 7.504E-02 FAIL ABUN Page 2946 of 5809 LU-176 -3.930E-03 2.940E-02 2.945E-02 FAIL ABUN HF-181 1. 039E+OO 3.944E+OO 3.972E+OO NOT IDENT. TA-182 2.800E-02 9.320E-01 9.321E-01 FAIL ABUN RE-183 -9.476E-02 2.642E+OO 2.642E+OO NOT IDENT. RE-184 -2.167E+00 2.852E+Ol 2.854E+Ol NOT IDENT. W-188 5.014E+Ol l.270E+02 l.290E+02 FAIL ABUN IR-192 -l.458E-02 4.490E-01 4.491E-01 FAIL ABUN HG-203 -l.183E+OO 2.439E+OO 2.496E+OO FAIL ABUN BI-207 l.742E-02 4.733E-02 4.797E-02 FAIL ABUN PB-210 3.524E-01 2.359E+OO 2.364E+OO NOT IDENT. BI-211 3.084E+OO 6.258E-01 l.525E+OO FAIL ABUN PB-211 4.493E-01 6.833E-01 7.127E-01 NOT IDENT. BI-212 2.197E+OO 8.384E-01 1. 298E+OO FAIL ABUN RN-219 -6.924E-02 3.680E-01 3. 693E.-01 FAIL ABUN RA-223 4. 601E-02 6.537E-01 6.540E-01 FAIL ABUN AC-227 l.881E-02 2.380E-01 2.382E-01 FAIL ABUN TH-227 l.881E-02 2.380E-01 2.382E-01 FAIL ABUN TH-229 2.042E-01 4.585E-01 4.677E-01 FAIL ABUN TH-231 4.601E-02 6.537E-01 6.540E-01 FAIL ABUN PA-233 -l.265E-02 5*. 820E-02 5.848E-02 FAIL ABUN PA-234 9.521E-03 2.505E-01 2.505E-01 NOT IDENT. PA-234M -2.099E+OO 4.737E+OO 4.831E+OO NOT IDENT. NP-237 -l.265E-02 5 .,820E-02 5.848E-02 FAIL ABUN NP-238 l.OOOE+41 l.108E+41 O.OOOE+OO SHORT HLIF NP-239 5.193E-03 2.345E-01 2.345E-01 FAIL ABUN PU-239 3. 2 68E+02 3.275E+02 3. 591E+02 NOT IDENT. AM-241 5.439E-02 l.330E-01 l.353E-01 NOT IDENT. CM-243 -l.163E-02 9.612E-02 9.626E-02 NOT IDENT. BK-247 -l.203E-02 7.580E-02 7.600E-02 FAIL ABUN CM-247 -5.026E-03 3.444E-02 3. 451E-02 NOT IDENT .. CF-251 -l.778E-01 l.252E-01 1. 486E-01 NOT IDENT. Page 2947of5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 37.0694 87.09 84.5633 136.47 56.9975 45.60 58. 6698* 87.57 84.6261 140.51 0.0000 46.54 47.5979 88.03 84.6864 143.76 55.3058 49 .72 0.0000 88.34 84.7267 144.24 47.7410 51. 35 64.1478 88.47 84.7440 145.44 67.3612 51. 87 66.1086 89.96 84.9376 152.43 78.8291 52.39 61.4550 1093.63 85.0254 "153.25 0.0000 52.97 57.7443 91.11 0.0000 323.87 63.6234 53.44 61.5921 92.59 85.2760 156.02 0.0000 54.07 59.7763 93.35 85. 3727 158.56 0.0000 57.36 0.0000 94.56 85.5259 159.00 48.5124 57.53 71. 6703 94.65 85.5374 162.33 73.0214 57.98 75.5609 94.67 85.5400 162.66 0.0000 59.27 77.6734 94.87 85.5650 163.33 62.0216 59.32 77.6811 97.43 66.8003 165.86 65.5143 59.54 71. 6383 98.43 70.9922 176.31 .54.9829 60.96 82.1009 98.44 70.9932 176.60 0 ."0000 61.17 82 .1344 99.53 59.4815 177.52 78.6400 62.93 79.1938 100 .11 66. 7154 181.07 0.0000 63.29 79.2483 102.03 63.1232 181.52 85.7122 63.58 79.2917 103.18 61.8507 184.41 55.4151 64.28 76.1693 103.37 61. 8 672 143.76 55.4839 66.73 86.8927 105.21 58.9239 193.51 46.7650 67.24 69.1252 105.31 58.9322 197.03 49.2043 125.81 71.1292 106.12 58.9978 198.01 60.7014 67.75 71.1381 106.47 59.0261 201.83 47.1197 69.67 88.6620 109.28 63.7561 203.43 71. 3554 70.83 69.2471 111. 00 76.0587 205.31 43.0385 72.81 73.7497 111.76 0.0000 210.85 50.9710 72.87 73.7572 114. 06 67.9973 215.65 46.5295 74.66 73.9861 116. 30 0.0000 222 .11 65.4994 74.82 74.0061 116.74 65.0855 227.09 51. 6773 74.97 74.0250 119.76 62.1757 227.38 49.3405 77 .11 74.2945 121.12 40.1141 228.16 0.0000 78.74 76.8147 121. 22 40 .1193 228.18 45.8465 79.69 83.5674 121. 78 59.1646 116.74 45.8465 80.12 87.6086 122.06 86.6646 235.69 39.4251 80.19 0.0000 122.92 66.6554 235. 96 39.4338 80.57 77.0466 123.07 60.3185 238.63 52.1641 81. 00 82.4175 265.00 70.9544 238.98 0.0000 81. 07 82.4270 125.81* 59.4611 240.99 52.2621 81. 75 80.8548 127.23 84.0285 242.00 52.3037 83.79 98.8127 127.91 72.3885 244.70 31. 7668 84.00 96.1743 129.30 62.9135 252.40 0.0000 85.43 84. 3435 131. 20 73.7442 252.80 37.1616 86.55 84.4922 133.02 69.6199 254.15 0.0000 86.79 84.5236 133.52 58.9444 256.23 42.0667 86.94 84.5435 136.00 69.8639 260.90 0.0000 Page 2948 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36 .. 2869 355.39 0.0000 584.27 23.0508 264.80 42.3390 356.01 30.8540 595.83 0.0000 265.00 42.3454 364.49 0.0000 427.87 23.2080 268.22 37.1906 366:42 0.0000 602.52 0.0000 269.46 48.5535 372.51 30.2917 604.72 23.2471 270.03 48:5742 375.05 23.4025 607.14 21. 8161 271.23 48.6169 377.52 30.3800 609.32 8.7341 273.65 0.0000 356.01 24.8285 610.33 8.7378 276.40 40.6667 388.16 27.5093 614.28 14.5862 277.3] 37.8456 388.63 0.0000 618.01 21.4253 277.60 34.1891 391.69 23.6261 620.36 19.4954 278.00 34.1993 264.66 29.9008 62L 93 14.6313 279.20 45.2304 401. 81 31.6802 630.19 0.0000 279.54 45.2417 402.40 32.5707 631.29 12.7276 279.70 41. 5776 404.85 28.2070 633.25 13.2275 280.46 31.8121 410.95 31.8391 634.78 0.0000 283.69 42.9222 413.71 30 .1152 635.95 8.8275 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.1518 423.72 0.00.00 645.85 16.7392 285.90 0.0000 427.09 21. 4106 657.76 14.8383 287.50 38 .1190 427.87 26.7743 657.90 0.0000 290.67 37.7933 433 :94 20.1448 661.66 14.8602 293.27 0.0000 439.40 22.4467 664.57 0.0000 351. 93 38.3243 453.88 21. 7095 666.33 0.0000 295. 96 38.3441 463.37 17.2686 666.50 0.0000 879.38 38.4123 468.07 17.3088 667.71 0.0000 299.98 38.4492 473.00 0.0000 677.62 16.9440 300.09 38.4520 475.06 16.4542 685.70* 0.0000 300 .13 38.4529 476.78 16.4681 695.00 0.0000 301.36 38.4851 477.60 23.0646 696. 49 17.0636 302.85 38.5239 482.18 21. 0978 696. 51 17.0636 256.23 38.5674 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18. 0725 306.78 41. 5334 497.08 18.4774 697.49 18.0740 308.46 43.6592 505.52 20.8699 702.65 21.1256 311. 90 40.0088 507.63 0.0000 706.68 22.1647 316.51 38.4578 511. 00 19.5284 711. 68 19.1770 319.41 0.0000 514.00 19.5551 720.70 0.0000 320.08 0.0000 514.00 19.5551 721. 93 0.0000 321. 04 35.2179 520.40 25.2169 722. 78 16.7202 323.87 39.0622 520.69 0.0000 722. 91 18.2410 325.23 37.8360 522.65 0.0000 723. 31 18.2439 328.76 0.0000 527.90 0.0000 724 .19 13.6873 333.37 40.5684 528.26 15.9340 727. 33 14.2096 333.97 40.5830 529.59 25.3224 733.00 12.2046 334.37 40.5938 529.87 0.0000 735.93 15. 2716 338.28 29.2484 531. 02 0.0000 333.97 16.8075 338.32 29.2491 537.26 0.0000 7"'.39.5o* 0.0000 311. 90 29.2884 546.56 0.0000 747.24 12.2656 340.48 29.2884 552.55 14.2120 748.06 15.3363 340.55 0.0000 563.25 25.7014 752.31 13.3110 344.28 29.3578 569.33 14.3158 753.82 0. 0000, 345.93 37.0536 946.00 16.2260 756.73 13.3317 351. 06 27.3438 569.70 16.2273 756.80 12".3066 351.93 27.3581 583.19 23.0400 884.68 15.4211 Page 2949 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 37.0342 1274.44 16.5686 1620.50 1. 9110 766.42 33.9547 1001.03 19.9087 1621.92 3.8232 766.84 23.6691 1002.74 9.9591 1678.03 0.0000 772.60 0.0000 1004.73 13.2861 1690.97 5.8092 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.9057 778.90 18.5999 1028.54 0.0000 1063.66 8.8391 783.70 0.0000 1037.84 13.4072 1771. 35 4.4905 785:37 5.1778 1038.76 0.0000 1791.20 0.0000 792.07 20.2387 631.29 16.7993 1808.65 2. 9663 794.95 11. 427 9 1048.07 0.0000. 1810.72 0.0000 795.86 15.5884 1049.04 16.8103 1836.06 1.9869 810.06' 17.7498 1050.41 8. 968 8 810.29 16.7070 1063.66 10.1257 344.28 12.5308 1077.00 0.0000 810.76 13.5761 1077.34 20.3247 815.77 0.0000 1085.87 11.3167 1048.07 0.0000 1093.63 9.0716 832.01 18.9280 1099.45 10.2209 834.85 14.7354 1112. 07 1. 7090 835.71 12.6338 1112. 84 3.4187 836.80 0.0000 1115.54 6.8423 846.75 0.0000 1120. 29 15.4138 846.77 '11. 0934 1120.55 15.4149 856.80 0.0000 1221. 41 15.4171 860.56 13.7945 1129. 67 6.8667 871.09 12.7754 1131. 51 0.0000 873.19 17.0449 1147.95 0.0000 875.33 0.0000 1173.23 15.2722 879.38 17.0775 1177.95 13.9004 880.51 18 .1510. 1189.05 13.9375 883.24 9.6174 1204.77 15.1571 884.68 17.1055 1221.41 14.9248 889.28 10.7060 1231. 02 14.0791 894.76 10.7239 1235.36 0.0000 898.04 20.3955 1238.28 10.5776 900. 72 11.8173 1260.41 0.0000 903.28 13.9770 1271.87 14.2139 911. 20 9.6995 1274.44 10.6670 912.08 9.7020 1274.54 10.6670 923.98 0.0000 1291.59 8.0316 926.50 15.1570 1298.22 0.0000 929 .11 6.5007 1312 .11 0.0000 937.49 9.7753 1332:49 15.4395 944 .13 0.0000 1362.66 0.0000 946.00 10.8883 1365.19 6.3502 949.00 15. 2572 1368.63 0.0000 667.71 0.0000 1384.29 7.2876 962. 31 15.3159 1408.01 10.9871 964.08 15.3239 1457.56 0.0000 966 .17 15.3330 1460.82 7.4063 911. 20 15.3450 1489.16 7.4492 968. 97 15.3450 1505.03 0.9341 983.53 0.0000 1584.12 7.5908 984.45 0.0000 1596.21 0.0000 Page 2950 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:01:35.64
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : Z-OCT-2016 11:00:23. Sample date 10-DEC-2015 14:35:00 Acquisition date : 3-0CT-2016 08:01:06. Sample ID G405235003 Sample quantity : 1.40486E+02 GRAM Detector name : GAM08 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.68 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID : 1596247 Detector SN# : Matrix Spike ID : ID. : 1556 ******************************************************************************** Pk It 1 0 2 0 3 2 4 2 5 0 6 0 7 0 8 0 9 0 10 0 11 3 12 3 13 0 14 0 15 0 16 7 17. 7 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 2951of5809 Energy 41.47 63.66* 74.52* 77.bl* 86.98* 92.58* 104.66 129.00 185.88* 209.35 238.59* 241.51 270.63 278.02* 294. 96* 338.25* 342.50 352.04* 367.54 401.74 416.72 463.41 511.20* 517.47 583.39* 596. 95 609.38* 679.31 706.97 727. 97* 781.12 785.41 860.11* 876.69 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 14 67 116 157 51 14 31 18 56 64 371 90 29 15 116 70 33 189 22 16 12 12 42 18 121 14 116 25 9 24 21 25 25 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 99 146 145 119 178 204 88 116 108 112 56 76 77 60 48 52 61 76 30 51 27 30 31 17 33 7 42 17 19 29 2 0 10 7 1. 38 1. 58 1. 30 1.10 1. 03 1. 43 1. 66 0.83 1. 54 3.58 1.15 1. 79 1.12 1. 02 1. 30 1. 72 2.84 1. 25 2.73 4.42 1. 30 1. 33 1. 97 3. 86 1. 36 1. 66 1. 56 3.78 0.98 1. 06 0.90 0.87 0.82 3.30 83.16 127.57 149.30 154.28 174.23 185 . .43 209.61 258.30 372 .11 419.08 477.57 483.42 541.69 556.48 590.38 676.98 685.48 704.59 735.59 804.01 834.00 927.40 1023.03 1035.57 1167.46 1194.59 1219.46 1359.36 1414.71 1456.73 1563.07 1571. 64 1721.09 1754.26 80 122 143 143 171 182 207 253 367 . 413 473 473 535 550 585 672 672 698 731 795 830 923 1015 1030 1161 1191 1213 1350 1411 1448 1558 1568 1714 1748 7 3.94E-03118.8 11 1.87E-02 37.6 16 3.22E-02 20.8 3.53E+OO 16 4.35E-02 14.7 8 1.41E-02 47.8 9 3.85E-03198.0 7 8.75E-03 52.7 9 4. 96E-03111. 6 9 1.55E-02 38.5 14 l.78E-02 37.2 18 l.03E-01 6.3 l.OlE+OO 18 2.51E-02 27.7 10 8.0lE-03 60.0 9 4.25E-03100.0 10 3'. 21E-02 14. 8 20 1.93E-02 23.1 2.33E+OO 20 9.06E-03 53.0 14 5.24E-02 12.4 9 6.12E-03 49.3 15 4.37E-03103.2 8 3.34E-03 81.l 8 3. 45E-03 81. 3 16 1. l 7E-02 40. 9 11 4.86E-03 50.9 12 3.36E-02 13.3 7 3.75E-03 42.l 12 3.23E-02 14.8 17 7.05E-03 42.l 7 2. 61E-03 91. 4 13 6.75E-03 51.9 10 5.72E-03 26.2 8 6.94'E-03 20 . .0 13 6.86E-03 34.3 10 2.16E-03 74.8 Peak Search Report (continued) Page : 2 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 50* 67 13 1. 62 1823.91 1818 14 l.87E-02 17.3 36 0 934.52 9 9 0.92 1869.96 1863 9 2.45E-03 70.0 37 0 963.07* 27 6 0.63 1927.07 1920 13 7.49E-03 28.3 38 0 968. 96* 44 11 2.45 1938.86 1934 10 1. 22E-02 21. 7 39 0 1042.94 18 4 1. 35 2086.86 2082 11 4.90E-03 34.5 40 0 1097.55 11 6 1. 29 2196.11 2192 8 3.14E-03 47.7 41 0 1121.15* 34 10 3.88 2243.33 2236 18 9.40E-03 30.9 42 0 1145.18 9 7 1.18 2291. 40 2287 8 2.40E-03 69.3 43 0 1155. 67 21 7 2.04 2312.38 2304 14 5.79E-03 34.7 44 0 1239.66 11 12 3.50 2480.41 2473 13 3.12E-03 71. 9 45 0 1243.50 10 0 1. 53 2488.10 2485 7 2.78E-03 31. 6 46 0 1310. 84 12 5 1.11 2622.80 2617 12 3.38E-03 48.6 47 0 1408.11 9 2 1. 57 2817.40 2813 9 2.41E-03 46.2 48 0 1430. 72 8 6 0.66 2862.62* 2853 13 2.14E-03 76.8 49 0 1460.85 291 3 1. 90 2922.90 2916 13 8.08E-02 6.0 50 0 1764.80* 17 3 1. 03 3530.91 3525 11 4.68E-03 34.6 Flag: "*" = Peak area was modified by background subtraction Page 2952 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:01:37 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 14:35:00 G405235003 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016.08:01:06 140,49 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors Efficiency type Abundance limit Interference Report SOLID GAMMAS 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 TL-208. 277.37 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 2953 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 87.57 CD-109 88.03 RA-224 2"40.99 CM-247 278.00 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.68 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Nuclide* Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 9.671E-01 1.446E+Ol 1.446E+Ol 12.00 OK CD-109 88.03 3.70* 4.281E+OO 1.lOlE+OO 1.722E+OO 181.21 OK SN-126 64.28 9.60 2.181E+OO 2.125E+OO 2.125E+OO 75.23 OK 86. 94 8.90 4.281E+OO 4.577E-01 4.577E-01 181.21 OK 87.57 37.00* 4.281E+OO 1.lOlE-01 1.lOlE-01 181. 21 OK EU-155 86.55 30.70 4.281E+OO l.327E-01 l.495E-01 181.21 OK 105.31 21.10* 5.121E+OO l.853E-01 2.088E-01 105.38 OK TL-208 277.37 6.60 3.703E+OO 3.695E-01 3.695E-01 199.99 OK 583.19 85.00* 2.006E+OO 3.940E-01 3.940E-01 26.63 OK 860.56 12.50 1.479E+OO 7.179E-01 7.179E-01 68.57 OK BI-212 727.33 6.67* l.684E+OO 1.178E+OO 1.178E+OO 103.81 OK 785.37 1.10 1.587E+OO 7.754E+00 7.754E+OO 40.00 OK 1620.50 1. 47 8.836E-01 Line Not Found Absent PB-212 74.82 10.28 3.291E+OO 1.644E+OO 1.644E+OO 57.64 OK 77 .11 17.10 3.516E+OO 1.694E+OO 1.694E+OO 29.38 OK 238.63 43.60* 4.175E+OO 1.218E+OO 1.218E+OO 12.63 OK 300.09 3.30 3.479E+OO Line Not Found Absent BI-214 609.32 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 OK 1120.29 14.92 1.202E+OO 9.905E-01 9.908E-01 61. 72 . OK 1764.49 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 OK PB-2*14 74.82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3.516E+OO 2. 986E+O.O 2.987E+OO 29.38 OK 87.09 3.41 4.288E+OO Line Not Found <<INT Reject 242.00 7.25 4.130E+OO Line Not Found <<INT Reject 295.22 18.42 3.529E+OQ l.045E+00 1.045E+OO 29.69 OK 351.93 35.60* 3.045E+OO 1.007E+OO l.008E+00 24.88 OK RN-219 271.23 10.80 3.784E+OO 4.176E-01 4.176E-01 120.01 OK 401.81 6.60* 2.725E+OO 5.016E-01 5 ."016E-01 206.32 OK RN-222 609.32 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 OK 1120.29 14.92 l.202E+OO 9.905E-01 9.908E-01 61. 72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.777E-01 69 .13 OK RA-224 240.99 4.10* 4.136E+OO 1.333E+OO 1.333E+OO 138.31 OK RA-226 609.32 45. 49*. 1.938E+OO 7.300E-01 7.303E-01 29.55 OK 1120.29 14.92 1. 202E+OO 9.905E-01 9.908E-01 61. 72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 OK AC-228 105.21 1.10 5.121E+OO 3.555E+OO 3.555E+OO 105.38 OK 338.32 11. 27 3.149E+OO 1.138E+OO 1.138E+OO 46 .11 OK 794.95 4.25 1.572E+OO Line Not Found Absent 835. 71 1. 61 1.512E+OO Line Not Found Absent 911. 20 25.80* l.413E+OO 9.868E-01 .9.868E-01 34.65 OK 968. 97 15. 80 l.348E+OO 1.097E+OO 1.097E+OO 43.42 OK RA-228 105.21 1.10 5.121E+00 3.555E+OO 3.555E+OO 105.38 OK 338.32 11.27 3.149E+OO 1.138E+OO l .138E+OO 46.11 OK 794.95 4.25 1.572E+OO Line Not Found Absent 835. 71 1. 61 1.512E+OO Line Not Found Absent 911.20 25.80* 1.413E+OO 9.868E-01 9.868E-01 34.65 OK 968.97 15.80 1.348E+OO 1.097E+OO 1.097E+OO 43.42 OK TH-228 74.82 10.28 3.291E+00 l.644E+OO 1.644E+OO 57.64 OK 77 .11 17.10 3.516E+OO 1.694E+OO 1.694E+OO 29.38 OK Page 2954 of 5809 Nuclide Line Activity Report (continued) *Page : 3 Sample ID : G405235003 . Acquisition date 3-0CT-2016 08:01:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 4.175E+00 1.218E+OO 1.218E+OO 12.63 OK 300.09 3.30 3.479E+OO Line Not Found Absent TH-230 609.32 45.49* 1.938E+OO 7.301E-01 7. 301E-01 29.55 OK 1120.29 14.92 1.202E+OO 9.905E-01 9.905E-01 61.72 OK' 1764.49 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 OK TH-232 105.21 1.10 5.121E+OO 3.555E+OO 3.555E+OO 105.38 OK 338.32 11. 27 3.149E+OO 1.138E+OO l.138E+OO 46.11 OK 835. 71 1. 61 l.512E+OO Line Not Found Absent 911. 20 25.80* l.413E+OO 9.868E-01 9.868E-01 34.65 OK 968. 97 15.80 1.348E+OO 1.097E+OO 1.097E+OO 43.42 OK TH-234 63.29 3.70* 2.181E+OO 5.514E+OO 5.514E+OO 75.23 OK 92.59 4.23 4.614E+00 4.562E-01 4.562E-01 395.92 OK U-234 609.32 45.49* l.938E+00 7.300E-01 7.301E-01 29.55 OK 1120.29 14.92 l.202E+OO 9.905E-01 9.905E-01 61. 72. OK 1764.49 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 OK U-238 63.29 3.70* 2.181E+OO 5.514E+OO 5.514E+OO 75.23 OK 92. 59 4.23 4.614E+OO 4 .562E-01 4.562E-01 395.92 OK AM-243 43.53 5.90 2.327E-01 Line Not Found Absent 74.66 67.20* 3.291E+OO 2.515E-01 2.515E-01 57.64 OK CM-247 278.00 3.40 3.703E+OO Line Not Found <<INT Reject 287.50 2.00 3.604E+OO Line Not Found Absent 402.40 72. 00* 2. 725E+OO 4.598E-02 4.598E-02 206.32 OK ANH-511 511. 00 100.00* 2.232E+OO l.061E-01 l.061E-01 81. 81 OK Flag: "*" = Keyline Page 2955 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09.:01:38.98 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l *
Acquisition date 3-0CT-2016 08:01:06 Sensitivity : 3.000 * *.Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date* 10-DEC-2015 14:35:00 Analyst initials: MXRl *
Sample ID G405235003 Sample Quantity 1.4049E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
Eff.' File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.446E+Ol 1. 700E+OO 8.167E-01 CD-109 1.722E+OO 3.058E+OO 3.055E+OO SN-126 1.lOlE-01 l.955E-01 l.900E-01 EU-155 2.088E-01 2.156E-01 2.455E-01 TL-208 3.940E-01 l.028E-01 6.557E-02 BI-212 1.178E+OO l.199E+OO 1.0lOE+OO PB-212 l.218E+OO 1.508E-01 1.099E-01 BI-214 7.303E-01 2 .115E-01 1.733E-01 PB-214 1.008E+OO 2.457E-01 l.604E-01 RN-219 5.016E-01 1.014E+OO 8.686E-01 RN-222 7.303E-01 2 .115E-01 l.733E-01 RA-224 l.333E+OO l.807E+00 1.178E+OO RA-226 7.303E-01 2 .115E-01 1.733E-01 AC-228 3.351E-01 3.106E-01 RA-228 9. 8 68E-01 3.351E-01 3.106E-01 TH-228 1.218E+OO l.508E-01 1.099E-01 TH-230 7. 301E-01 2 .114E-01 l.733E-01 TH-232 9.868E-01 3.351E-01 3.106E-01 TH-234 5.514E+OO 4.065E+OO 2.879E+OO U-234 7.301E-01 2 .114E-01 1.733E-01 U-238 5.514E+OO 4.065E+OO 2.879E+00 AM-243 2.515E-01 1. 421E-01 1.162E-01 CM-247 4.598E-02 9.297E-02 7.973E-02 AtjH-511 1. 061E-01 8.509E-02 5.025E-02 Non-Identified Nuclides / Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 3.769E-01 1.220E+Ol 2.376E+Ol NOT IDENT. NA-22 -3.017E-02 6. llOE-02 l.074E-01 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 2.807E-04 1.819E-02 4.928E-02 NOT IDENT. SC-46 -4.138E-02 3.385E-01 6.862E-01 FAIL ABUN V-,-48 O.OOOE+OO l.t:j52E+04 O.OOOE+OO SHORT HLIF Page 2956 of 5809 CR-51 O.OOOE+OO 4.984E+02 O.OOOE+OO SHORT HLIF MN-54 l.168E-02 6.721E-02 l.390E-01 NOT IDENT. C0-56 -3.603E-01 5.812E-01 1.044E+OO FAIL ABUN MN-56 1.603E+41 O.OOOE+OO SHORT HLIF C0-57 3.215E-02 5.676E-02 1.088E-01 NOT IDENT. C0-58 -7.275E-01 6.999E-01 1.167E+OO NOT IDENT. FE-59 2.551E+OO 9.019E+OO 1.654E+Ol NOT IDENT. C0-60 4. 8 61E-03 5.650E-02 1.113E-01 NOT IDENT. ZN-65 9.557E-02 2.044E-01 3.990E-01 NOT IDENT. GE-68 9.350E-01 2.840E+OO 5.888E+OO' NOT IDENT. AS-73 4.679E+OO 1.492E+Ol 2. 911E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.875E+03 O.OOOE+OO . SHORT HLIF SE-75 2.433E-01 2.254E-01 4.693E-01 FAIL ABUN BR-77 O.OOOE+OO l.469E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.886E+02 O.OOOE+OO SHORT HLIF RB-83 -4.842E-01 8.995E-01 1.357E+OO NOT IDENT. KR-85 9.885E+OO 9. 717E+OO l.687E+Ol NOT IDENT. SR-85 1.019E+OO 1.004E+OO 1. 743E+OO NOT IDENT. RB-86 O.OOOE+OO 3.377E+04 O.OOOE+OO SHORT HLIF Y-88 -8.771E-02 2.218E-01 4.392E-01 NOT IDENT. Y-91 -2.454E+02 4. 722E+02 8.419E+02 NOT IDENT. NB-94 9.471E-03 4.610E-02 8.292E-02 NOT IDENT. NB-95 -6.313E-01 1.019E+OO l.846E+OO NOT IDENT. NB-95M -2.326E-01 2.792E+OO 4.837E+OO NOT IDENT. ZR-95 -9.418E-02 1. 968E+00 3.838E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 517E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO I. 217E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE-i-00 SHORT HLIF RH-101 1.169E-02 4.169E-02 7.220E-02 NOT IDENT. RH-102 3. 701E-03 6. 831E-02 1.306E-01 NOT IDENT. RU-103 1. 458E+00 6.553E+OO 1.286E+Ol FAIL ABUN RH-106 -2.142E-01 6.246E-01 1.109E+OO NOT IDENT. RU-106 -2.142E-01 6.246E-01 1.109E+OO NOT IDENT. AG-108M -9.918E-03 3.475E-02 6.372E-02 NOT IDENT. AG-llOM -2.885E-02 9. lOlE-02 l.769E-01 FAIL ABUN SN-113 7.813E-02 2.482E-01 4.970E-01 NOT IDENT. CD-115 O.OOOE+OO 2.060E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.123E+05 O.OOOE+OO SHORT HLIF TE-123M l.883E-01 1. 573E-01 3.123E-01 NOT IDENT. SB-124 -7.623E-01 1.056E+OO 1.104E+OO NOT IDENT. SB-125 -5.468E-02 1. 17 9E-01 2.122E-01 FAIL ABUN TE-125M 1.069E+02 3.419E+02 6. 351E+02 NOT IDENT. I-126 O.OOOE+OO l. ll 7E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.198E+06 O.OOOE+OO SHORT HLIF SB-127 0.000E+OO 1.667E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.195E+09 O.OOOE+OO SHORT HLIF r--132 O.OOOE+OO l.039E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.815E+26 O.OOOE+OO SHORT HLIF BA-133 l.325E-02 5.067E-02 9.088E-02 NOT IDENT. I-133 O.OOOE+OO l.167E+41 O.OOOE+OO SHORT HLIF CS-134 8.258E-02 5.926E-02 l.380E-01 NOT IDENT. CS-135 9.185E-02 1.70/E-01 3.171E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.500E+05 O.OOOE+OO SHORT HLIF BA-137M 6.763E-03 4.608E-02 8.695E-02 NOT IDENT. CS-137 7.144E-03 4.868E-02 9.186E-02 NOT IDENT. CE-139 -4.362E-02 l.406E-01 2.432E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 724E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.627E+05
0. OOOE+OO SHORT HLIF CE-141 3.308E+OO 3.052E+Ol 5.510E+Ol NOT IDENT. CE-143 O.OOOE+OO 8.286E+40
0. OOOE+OO SHORT HLIF CE-144 9.356E-02 .4.746E-01 8.603E-01 NOT IDENT. PM-144 -1.355E-02 6.227E-02 l.212E-01 NOT IDENT. PR-144 -1.232E+OO 5.393E+OO l.048E+Ol NOT IDENT. PM-146 4.955E-03 5.043E-02 9.762E-02 NOT IDENT. ND-147 O.OOOE+OO 4.064E+07 O.OOOE+OO SHORT HLIF PM-147 -9 .139E+02 l.045E+03 l.753E+03 NOT IDENT. PM-149 O.OOOE+OO 2. 372E+40 O.OOOE+OO SHORT HLIF EU-150 -6.881E-03 3.208E-02 5.364E-02 FAIL ABUN EU-152 7.929E-04 1.151E-01 l.992E-01 FAIL ABUN GD-153 -8.738E-02 2.201E-01 3.926E-01 FAIL ABUN EU-154 -7.705E-02 1.494E-01 2.614E-01 NOT IDENT. TB-160 -7. 311E-01 1.832E+OO 2. 961E+OO FAIL ABUN H0-166M 6.388E-02 7.824E-02 l.640E-01 FAIL ABUN TM-171 -1.557E+Ol 3. 878E+Ol. 7.150E+Ol NOT IDENT. HF-172 -9.778E-02 2.939E-01 4.742E-01 FAIL ABUN LU-172 4.333E-02 1.119E-01 2 .119E-01 FAIL ABUN Page 2957 of 5809 LU-176 2.191E-02 2.782E-02 5.780E-02 FAIL ABUN . HF-181 2.207E+OO 4.754E+OO 9. 671E+OO NOT IDENT. TA-182 -8.885E-01 1.158E+00 1.*927E+OO FAIL ABUN RE-183 1.486E-01 4.431E+OO 8.474E+OO NOT IDENT. RE-184 9.336E+OO 3.418E+Ol 7.087E+Ol NOT IDENT. W-188 9.807E+OO 1.247E+02 2.208E+02 FAIL ABUN IR-192 -l.562E-01 5.335E-01 9. 972E-01 FAIL ABUN HG-203 2.509E+OO 4.918E+OO 4.798E+OO FAIL ABUN BI-207 -2.470E-02 6.450E-02 1.176E-01 FAIL ABUN PB-210 4.378E+OO 6.861E+OO 1. 389E+Ol NOT IDENT. BI-211 O.OOOE+OO 6.767E-01 9.852E-01 FAIL ABUN PB-211 -6. 341E-02 7.940E-01 1.350E+OO NOT IDENT. RA-223 -3.459E-01 6.499E-01 l.147E+OO FAIL ABUN AC-227 6.193E-02 2.609E-01 5.171E-01 NOT IDENT. TH-227 6.193E-02 2.609E-01 5.171E-01 NOT IDENT. TH-229 3 .118E-01 5.182E-01 1.061E+OO FAIL ABUN PA-231 8.794E-01 5.953E-01 1.261E+OO NOT IDENT. TH-231 -3.459E-01 6.499E-01 1.147E+OO FAIL ABUN PA-233 -l.557E-02 6.863E-02 1.294E-01 NOT IDENT. PA-234 6. OllE-02 3.615E-01 7.255E-01 NOT IDENT. PA-234M 1.138E+OO 6.167E+00 1.246E+Ol NOT IDENT. U-235 1.168E-01 2.250E-01 4.286E-01 FAIJ;.i ABUN NP-237 -l.557E-02 6.863E-02 l.294E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 4.035E-02 3.200E-01 5.880E-01 FAIL ABUN PU-239 3.234E+02 7. 071E+02 7.300E+02 FAIL ABUN AM-241 l.208E-02 2.140E-01 3.793E-01 NOT IDENT. CM-243 1.908E-01 1.970E-01 2. 313E-01 FAIL ABUN BK-247 3.487E-02 8. 713E-02 l.603E-01 NOT IDENT. CF-249 -2.600E-02 4.139E-02 7.336E-02 NOT IDENT. CF-251 5.720E-02 1.289E-01 2.619E-01 NOT IDENT. Page 2958 of 5809 VAX/VMS Nuclide Identification*Report Generated 3-0CT-2016 09:01:36.41 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 279 10.66* 9. 671E-01 1.446E+Ol l.446E+Ol 12.00 CD-109 88.03 61 3.70* 4.281E+OO 2.064E+OO 3.228E+OO 95.67 SN-126 64.28 83 9.60 2.181E+OO 2.125E+OO 2.125E+OO 75.23 86.94 61 8.90 4.281E+OO 8.580E-01 8.580E-01 95.67 87.57 61 37.00* 4.281E+OO 2.064E-01 2.064E-01 95.67 EU-155 86.55 61 30.70 4.281E+OO 2.487E-01 2.802E-01 95.67 105.31 37 21.10* 5 .121E+OO l.853E-01 2.088E-01 105.38 HG-203 70.83 ------3.69 2.935E+OO ------Line Not Found ------72. 87 ------6.19 3.135E+OO ------Line Not Found ------279.20 17 81.56* 3.703E+OO 2.990E-02 2.509E+OO 199.99 TL-208 277.37 17 6.60 3.703E+OO 3.695E-Oi 3.695E-01 199.99 583.19 126 85.00* 2.006E+OO 3.940E-01 3.940E-01 26.63 8 60. 56 25 12.50 1. 479E+OO 7.179E-01 7.179E-01 68.57 BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 204 12.92* 3.045E+OO 2.776E+00 2.776E+OO 24.88 BI-212 25 6.67* 1.684E+00 1.178E+OO l.178E+OO 103.81 785.37 25 1.10 l.587E+OO 7.754E+OO 7.754E+OO 40.00 1620.50 ------1. 47 8.836E-01 ------Line Not Found ------PB-212 74.82 141 10.28 3.291E+00 2.233E+OO 2.233E+00 41. 69 77 .11 191 17.10 3.516E+OO 1.694E+OO 1.694E+OO 29.38 238 415 43.60* 4.175E+OO 1.218E+OO 1.218E+OO 12.63 300.09 ------3.30 3.479E+OO ------Line Not Found ------BI-214 609.32 120 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 1120.29 33 14.92 l.202E+OO 9.905E-01 9.908E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.777E-01 69 .13 PB-214 74.82 141 5.80 3.291E+OO 3.959E+OO 3. 960E+00 41. 69 77 .11 191 9.70 3.516E+OO 2.986E+OO 2.987E+OO 29.38 87.09 61 3.41 4.281E+OO 2.239E+OO 2.240E+OO 95.67 242.00 101 7.25 4.136E+OO 1. 799E+OO 1.799E+OO 55.34 295.22 127 18.42 3.529E+OO 1.045E+OO 1.045E+OO 29.69 351. 93 204 35.60* 3.045E+OO 1.007E+OO 1.008E+OO 24.88 RN-219 271.23 32 10.80 3.784E+OO 4.176E-01 4.176E-01 120.01 401.81 17 6.60* 2.725E+OO 5.016E-01 5.016E-01 206.32 RN-222 609.32 120 45.49* l.938E+OO 7.300E-01 7.303E-01 29.55 1120.29 33 14.92 l.202E+OO 9.905E-01 9.908E-01 61.72 1764.49 16 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 RA-224 240.99 101 4.10* 4.136E+OO 3.181E+OO 3.181E+00 55.34 RA-226 609.32 120 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 1120.29. 33 14.92 1.202E+OO 9.905E-01 9.908E-01 61.72 1764.49 16 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 AC-228 105.21 37 1.10 5 .121E+OO 3.555E+OO 3.555E+OO 105.38 338.32 76 11. 27 3.149E+OO l.138E+OO l.138E+OO 46.11 794.95 ------4.25 l.572E+OO ------Line Not Found ------835.71 ------1. 61 l.512E+OO ------Line Not Found ------911.20 67 25.80* l.413E+OO 9.868E-01 9.868E-01 34.65 968. 97 44 15.80 l.348E+OO 1.097E+OO l.097E+OO 43.42 RA-228 105.21 37 1.10 5.121E+OO 3.555E+OO 3.555E+OO 105.38 Page 2959 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 338.32 76 11. 27 3.149E+OO 1.138E+OO l.138E+OO 46 .11 794.95 ------4.25 l.572E+OO ------Line Not Found ------835. 71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 67 25.80* 1.413E+OO 9.868E-Oi 9.868E-01 34.65 968. 97 44 15.80 l.348E+OO 1.097E+OO l.097E+OO 43.42 TH-228 74.82 141 10.28 3.291E+OO 2.233E+OO 2.233E+OO 41. 69 77 .11 191 17.10 3.516E+OO l.694E+OO 1.694E+OO 29.38 238.63 415 43.60* 4.175E+OO 1.218E+OO 1.218E+OO 12.63 300.09 ------3.30 3.479E+OO ------Line Not Found ------TH-230 609.32 120 45.49* l.938E+OO 7. 301E-01 7.301E-01 29.55 1120.29 33 14.92 1.202E+OO 9.905E-01 9.905E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 TH-232 105.21 37 1.10 5.121E+OO 3.555E+OO 3.555E+OO 105.38 338.32 76 . 11. 27 3 .14.9E+OO 1.138E+OO 1.138E+OO 46.11 835.71 ------1. 61 1. 512E+OO ------Line Not Found ------911.20 67 25.80* 1. 413E+OO 9.868E-01 9.868E-01 34.65 968.97 44 15.80 1.348E+OO 1.097E+OO 1.097E+OO 43.42 TH-234 63.29 83 3.70* 2.181E+00 5.514E+OO 5.514E+00 .75. 23 92.59 17 4.23 4.614E+OO 4.562E-01 4.562E-01 395.92 U-234 609.32 120 45.49* 1.938E+OO 7.300E-01 7. 301E-01 29.55 1120. 29 33 14.92 1.202E+OO 9.905E-01 9.905E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 U-238 63.29 83 3.70* 2.181E+OO 5.514E+OO 5.514E+OO 75.23 92.59 17 4.23 4.614E+OO 4.562E-01 4.562E-01 395.92 AM-243 43.53 ------5.90 2.327E-01 ------Line Not Found ------74.66 141 67.20* 3.291E+OO 3.417E-01 3.417E-01 41. 69 CM-247 278.00 17 3.40 3.703E+00 7.173E-01 7.173E-01 199.99 287.50 ------2.00 3.604E+OO ------Line Not Found ------402.40 17 72.00* 2. 725E+O.O 4.598E-02 4.598E-02 206.32 ANH-511 511. 00 44 100.00* 2.232E+OO 1.061E-01 1.061E-01 81. 81 Flag: "*" Key line Page 2960 of 5809 Summary of Nuclide Activity Sample ID : G405235003 Acquisition date Page : 3 3-0CT-2016 08:01:06 Total number of lines in spectrum 50 Number of unidentified lines 13 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 EU-155 HG:-203 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 CM-247 ANH-511 Hlif e l.25E+09Y 461.40D 2.30E+05Y 4.75Y 46.59D l.41E+10Y 7.04E+08Y l.41E+l0Y l.41E+10Y 1600.00Y 1600. OOY 7.04E+08Y 1600.00Y l.41E+l0Y 1600. OOY 1.41E+10Y 1. 41E+l0Y 1.41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.56E+07Y l.00E+09Y Decay 1. 00 1. 56 LOO 1.13 83.9 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.446E+Ol 2.064E+OO 2.064E-01 1.853E-01 2.990E-02 3.940E-01 2.776E+OO 1.178E+OO 1. 218E+OO 7.300E-01 1.007E+OO 5.016E-01 7.300E-01 3 .181E+OO 7.300E-01 9.868E-01 9.868E-01 1.218E+OO 7.301E-01 9.868E-01 5.514E+OO 7.300E-01 5.514E+OO 3.417E-01 4.598E-02 1. 061E-01 4.655E+Ol 4.655E+Ol Decay Corr pCi/GRAM l.446E+Ol 3.228E+OO 2.064E-01 2.088E-01 2.509E+OO 3.940E-01 2.776E+OO 1.178E+OO 1.218E+OO 7.303E-01 1.008E+OO 5.016E-01 7.303E-01 3.181E+OO 7.303E-01 9. '8 68E-01 9.868E-01 1.218E+OO 7. 301E-01 9.868E-01 5.514E+OO 7.301E-01 5.514E+OO 3.417E-01 4.598E-02 1.061E-01 5.022E+Ol 5.022E+Ol 74.00% Decay Corr 2-Sigma Error 0.173E+Ol 3.088E+OO 1.974E-01 2.200E-01 5.018E+OO 1.049E-01 0.690E+OO 1.223E+OO 0.154E+OO 2.158E-01 0.251E+OO 10.35E-01 2.158E-01 1. 760E+OO 2.158E-01 3.419E-01 3.419E-01 0.154E+OO 2.157E-01 3.419E-01 4.148E+OO 2.157E-01 4.148E+OO 1.425E-01 9.486E-02 0.868E-01 "M" Manually accepted 2-Sigma %Error 12.00 95.67 95.67 105.38 199.99 26.63 24.88 103.81 12.63 29.55 24.88 206.32 29.55 55.34 29.55 34.65 34.65 12.63 29.55 34.65 75.23 29.55 75.23 41. 69 206.32 81. 81 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 2961of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235003 Acquisition date : 3-0CT-2016 08:01:06 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec. %Err %Eff Flags 0 41. 47 18 126 1. 38 83.16 80 7 3.94E-03 **** 1. 33E-01 0 129.00 21 136 0.83 258.30 253 9 4. 96E-03 **** 5.48E+OO T 0 185.88 64 123 1. 54 372 .11 367 9 1.55E-02 76.9 4.93E+OO T 0 209.35 72 126 3.58 419.08 413 14 1. 78E-02 74.5 4.58E+OO T 7 342.50 35 66 2.84 685.48 672 20 9.06E-03 **** 3.12E+OO 0 367.54 24 32 2.73 735.59 731 9 6.12E-03 98.5 2.94E+OO T 0 416.72 13 29* 1. 30 834.00 830 8 3.34E-03 **** 2.64E+OO 0 463.41 13 31 1. 33 927.40 923 8 3.45E-03 **** *2.42E+OO T 0 517.47 18 17 3.86 1035.57 1030 11 4.86E-03 **** 2.21E+OO 0 596. 95 14 7 1. 66 1194. 59 1191 7 3.75E-03 84.1 1. 97E+OO T 0 679.31 26 17 3.78 1359.36 1350 17 7.05E-03 84.2 1.78E+OO 0 706.97 10 19 0.98 1414. 71 1411 7 2. 61E-03 **** 1. 72E+OO T ,o 781.12 21 2 0.90 1563.07 1558 10 5. 72E-03 52.5 1.59E+OO 0 876.69 8 7 3.30 1754.26 1748 10 2.16E-03 **** 1.46E+00 T 0 934.52 9 9 0.92 1869.96 1863 9 2.45E-03 **** 1.39E+OO 0 963. 07 27 6 0.63 1927.07 1920 13 7.49E-03 56.7 1.35E+OO T 0 1042.94 17 4 1. 35 2086.86 2082 11 4.90E-03 69.1 *1.27E+OO 0 1097.55 11 6 1. 29 2196 .11 2192 8 3.14E-03 95.4 1.22E+00 0 1145 .18 8 7 1.18 2291. 40 2287 8 2.40E-03 **** 1.18E+OO 0 1155.67 20 7 2.04 2312.38 2304 14 5.79E-03 69.5 l.17E+OO 0 1239.66 11 11 3.50 2480.41 2473 13 3.12E-03 **** 1. llE+OO T *o 1243.50 10 0 1. 53 2488.10 2'485 7 2.78E-03 63.2 1. llE+OO 0 "1310.84 12 5 1.11 2622.80 2617 12 3.3BE-03 97.2 1. 06E+OO T 0 1408 .11 8 2 1. 57 2817.40 2813 9 2.41E-03 92.3 9.98E-01 T 0 1430.72 7 6 0.66 2862.62 2853 13 2.14E-03 **** 9.84E-01 Flags: "T" = Tentatively associated Page 2962 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:01:56.09
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l * *Acquisition date 3-0CT-2016 08:01:06 Sensitivity : 3.000 *
Detector ID GAM08 Energy tolerance:. 1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date 14:35:00 Nuclide Library : SOLID *
Sample ID G405235003 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4049E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
Co.mbined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 EU-155 TL-208 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 3.380E-01 1.453E+OO 9.024E-02 1.148E-01 2.846E-02 4.395E-01 5.081E-02 7.832E-02 7.331E-02 3.930E-01 7.832E-02 5.448E-01 7.832E-02 l.353E-01 1.353E-01 5.081E-02 7.829E-02 l.353E-01 1.343E+OO 7.829E-02 1.343E+OO 5.467E-02 3.607E-02 2 .1.BlE:-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 2963 of 5809 Le' (pCi/GRAM l.043E+Ol 4.538E-02 O.OOOE+OO l.558E-02 2.834E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I:--132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149
EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 2964 of 5809 6.013E-02 4.509E-01 O.OOOE+OO 5.090E-02 4. 960E-01 7.178E+OO 4.792E-02 1.717E-01 2.553E+OO l.364E+Ol 0.000E+OO 2.162E-01 O.OOOE+OO 0.000E+OO 5.964E-01 7.628E+OO 7.877E-01 O.OOOE+OO 1.556E-01 3.369E+02 3.721E-02 8.089E-01 2.238E+OO 1. 712E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.369E-02 5. 716E-02 5.748E+OO 4.864E-01 4.864E-01 2.865E-02 7. 251E-02 2.238E-01 O.OOOE+OO O.OOOE+OO 1.466E-01 O.OOOE+OO 9.428E-02 2.980E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.124E-02 O.OOOE+OO 6.184E-02 1.463E-01 O.OOOE+OO O.OOOE+OO 3.888E-0.2 4.108E-02 1.135E-01 O.OOOE+OO O.OOOE+OO 2.591E+Ol O.OOOE+OO 4.045E-01 5.312E-02 4.593E+OO 4.368E-02 O.OOOE+Ob 8.158E+02 O.OOOE+OO 2.434E-02 9.019E-02 1.835E-01 1.102E-01 1.190E+OO 7.409E-02 3.345E+Ol 2.205E-01 9.319E-02 2.657E-02 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN , FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 2965 of 5809 4.324E+OO 8.178E-01 3. 962E+OO 3.085E+Ol l.004E+02 4.542E-01 2.190E+OO 5.0BBE-02 6.513E+OO 4.739E-01 6.025E-01 5.165E-01 2.386E-01 2.386E-01 4.951E-01 5.901E-01 5.165E-01 5.895E-02 3.184E-01 5.567E+OO 2.016E-01 5.895E-02 O.OOOE+OO 2.763E-01 3. 431E+02 1.772E-01 1.084E-01 7.365E-02 3.265E-02 1.223E-01 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:02:07.13 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l *
Acquisition date 3-0CT-2016 08:01:06 Sensitivity : 3.000 *
Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date 10-DEC-2015 14:35:00 Nuclide Library : SOLID *
Sample ID G405235003 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity 1.4049E+02 GRAM *
Quantity Err(%) 1.4236E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal'. date 21-JUL-2016 06: 09: 19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA. GAMMA] EFF GAM08 CAN. CNF; 14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.446E+Ol 1.860E+OO 1.860E+OO CD-109 l.722E+00 3.067E+00 3.067E+OO SN-126 1.lOlE-01 l.960E-01 1. 960E-01 EU-155 2.088E-01 2.161E-01 2.161E-01 TL-208 3.940E-01 1.042E-01 1.042E-01 .BI-212 1.178E+00 1.200E+OO 1.200E+OO PB-212 1.218E+OO l.640E-01 1.640E-01 BI-214 7.303E-01 2 .138E-01 2.138E-01 PB-214 l.008E+00 2.492E-01 2.492E-01 RN-219 5.016E-01 1.016E+OO 1.016E+OO RN-222 7.303E-01 2.138E-01 2.138E-01 RA-224 1.333E+OO 1.812E+OO 1.812E+OO RA-226 7.303E-01 2.138E-01 2.138E-01 AC-228 9.868E-01 3.389E-01 3.389E-01 RA-228 9.868E-01 '3. 389E-01 3.389E-01 TH-228 1.218E+OO 1. 640E-01 1.640E-01 TH-230 7. 301E-01 2.137E-01 2.137E-01 TH-232 9.868E-01 3.389E-01 3.389E-01 TH-234 5.514E+OO 4.245E+OO 4.245E+OO U-234 7. 301E-01 2.137E-01 2.137E-01 U-238 5.514E+OO 4.245E+OO 4.245E+OO AM-243 2.515E-01 1.434E-01 1.434E-01 CM-247 4.598E-02 9.329E-02 9.329E-02 ANH-511 1.061E-01 8.520E-02 8. 5,20E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 3.769E-01 1.220E+Ol 1.220E+Ol NOT IDENT. NA-22 -3.017E-02 6. lllE-02 6.261E-02 NOT IDENT. NA-24 -l.OOOE+41 8.361E+41 O.OOOE+OO SHORT HLIF AL-26-2.807E-04 l.819E-02 l.819E-02 NOT IDENT. SC-46 -4.138E-02 3.385E-01 3.390E-01 FAIL ABUN V-48 -8.087E+03 1.452E+04 1.497E+04 SHORT HLIF Page 2966 of 5809 CR-51 2. 431E+02 4.985E+02 5.104E+02 SHORT HLIF MN-54 l .168E-02 . 6. 721E-02 6.742E-02 NOT IDENT. C0-56 -3.603E-01 5.814E-01 6 .*037E-01 FAIL ABUN MN-56 -1.000E+41 l.604E+41 0.000E+OO SHORT HLIF C0-57 3.215E-02 5.678E-02 5.860E-02 NOT IDENT. C0-58 -7.275E-01 7.006E-01 7.736E-01 NOT IDENT. FE-59 2.551E+OO 9.021E+OO 9.094E+OO NOT IDENT. C0-60 4.861E-03 5.650E-02 5.654E-02 NOT IDENT. ZN-65 9.557E-02 2.045E-01 2.090E-01 NOT IDENT. GE-68 9.350E-01 2.840E+OO 2. 871E+OO NOT IDENT. AS-73' 4.679E+OO l.495E+Ol l.510E+Ol NOT IDENT. AS-74 7.125E+03 5*. 904E+03 6.722E+03 SHORT HLIF SE-75 2.433E-01 2.257E-01 2.509E-01 FAIL ABUN BR-77 l.187E+38 l.020E+39 O.OOOE+OO SHORT HLIF SR-82 -5.075E+Ol 7. 886E+o2 7.890E+02 SHORT HLIF RB-83 -4.842E-01 9.019E-01 9.280E-01 NOT IDENT. KR-85 .9.885E+OO 9. 725E+OO 1.070E+Ol NOT IDENT. SR-85 1.019E+OO 1.00SE+OO l.105E+OO NOT IDENT. RB-86 l.534E+03 3.377E+04 3.378E+04 SHORT HLIF Y-88 -8.771E-02 2.218E-01 2.253E-01 NOT IDENT. Y-91 -2.454E+02 4. 723E+02 4. 851E+02 NOT IDENT. NB-94 9.471E-03 4.610E-02 4.630E-02 NOT IDENT. NB-95 -6. 313E-01 l.019E+OO 1.058E+OO NOT IDENT. NB-95M -2.326E-01 2.792E+OO 2.794E+OO NOT IDENT. ZR-95 -9.418E-02 1. 968E+OO 1. 968E+OO NOT IDENT. NB-97 --1.000E+41 3.976E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.517E+41 O.OOOE+OO SHORT HLIF M0-99 5.623E+30 1.217E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.882E+41 0.000E+OO SHORT HLIF RH-101 1.169E-02 4.175E-02 4.208E-02 NOT IDENT. RH-102 3.701E-03 6. 831E-02 6.833E-02 NOT IDENT. RU-103 1.458E+OO 6.554E+OO 6.586E+OO FAIL ABUN RH-106 -2.142E-01 6.247E-01 6.321E-01 NOT IDENT. RU-106 -2.142E-01 6.247E-01 6.321E-01 NOT IDENT. AG-108M -9.918E-03 3.475E-02 3.504E-02 NOT IDENT. AG-110M -2.885E-02 9.102E-02 9.195E-02 FAIL ABUN SN-113 7.813E-02 2.482E-01 2.507E-01 NOT IDENT. CD-115 -1.298E+39 2.074E+39 O.OOOE+OO SHORT HLIF SN-117M 1.370E+04 l.123E+05 l.125E+05 SHORT HLIF TE-123M 1.883E-01 l.576E-01 1.790E-01 NOT IDENT. SB-124 -7.623E-01 1.057E+OO l .112E+OO NOT IDENT. SB-125 -5.468E-02 l.179E-01 l.205E-01 FAIL ABUN TE-125M 1.069E+02 3.420E+02 3.453E+02 NOT IDENT. I-126 -3.319E+04 l .117E+06 l.117E+06 SHORT HLIF SB-126 5.939E+05 l.203E+06 l.233E+06 SHORT HLIF SB-127 2.057E+21 1.690E+22 O.OOOE+OO SHORT HLIF I-131 -3. 372E+09 5.197E+09 5.415E+09 SHORT HLIF I-132 1.000E+41 l.838E+42 O.OOOE+OO SHORT HLIF TE-132 -l.489E+26 2.879E+26 O.OOOE+OO SHORT HLIF BA-133 1.325E-02 5.067E-02 5.102E-02 NOT IDENT. I-133 l.OOOE+41 2.142E+41 O.OOOE+OO SHORT HLIF CS-134 8.258E-02 5.936E-02 7.007E-02 NOT IDENT. CS-135 9.185E-02 l.708E-01 1. 757E-01 NOT IDENT. I-135 1.000E+41 2.658E+42 O.OOOE+OO SHORT HLIF CS-136 2.261E+05 3.508E+05 3.653E+05 SHORT HLIF BA-137M 6.763E-03 4.608E-02 4.619E-02 NOT IDENT. CS-137 7.144E-03 4.868E-02 4.879E-02 NOT IDENT. CE-139 -4.362E-02 1. 409E-01 l.422E-01 NOT IDENT. BA-140 -4.541E+05 1. 724E+06 l.737E+06 SHORT HLIF LA-140 -7.891E+04 3.627E+05 3.644E+05 SHORT HLIF CE-141 3.308E+OO 3.052E+Ol 3.055E+Ol NOT IDENT. CE-143 1.000E+41 8.31+/-7E+40 O.OOOE+OO SHORT.HLIF CE-144 9.356E-02 4.746E-01 4.765E-01 NOT IDENT. PM-144 -1.355E-02 6.227E-02 6.257E-02 NOT IDENT. PR-144 -1.232E+OO 5.394E+OO 5.422E+OO NOT IDENT. PM-146 4.955E-03 5.043E-02 5.048E-02 NOT IDENT. ND-147 -5.972E+06 4.064E+07 4.073E+07 SHORT HLIF PM-147 -9.139E+02 1.046E+03 l.124E+03 NOT IDENT. PM-149 -6.305E+39 '2. 37 6E+40 O.OOOE+OO SHORT HLIF EU-150 -6.881E-03 3.208E-02 3.223E-02 FAIL ABUN EU-152 7.929E-04 l .151E-01 l.151E-01 FAIL ABUN GD-153 -8.738E-02 2.202E-01 2.237E-01 FAIL ABUN EU-154 -7.705E-02 l.494E-01 l.534E-01 NOT IDENT. TB-160 -7. 311E-01 1.832E+OO 1. 8 62E+OO FAIL ABUN H0-166M 6.388E-02 7. 831E-02 8.344E-02 FAIL ABUN TM-171 -1.557E+Ol 3.880E+Ol 3. 94.3E+Ol NOT IDENT; HF-172 -9.778E-02 2.943E-01 2.976E-01 FAIL ABUN LU-172 4.333E-02 l .119E-Ol l.136E-01 FAIL ABUN Page 2967 of 5809 LU-176 2.191E-02 2.783E-02 2.953E-02 FAIL ABUN HF-181 2.207E+OO 4.755E+OO 4.858E+00 NOT IDENT. TA-182 -8.885E-01 1.159E+OO l.226E+OO FAIL ABUN RE-183 1. 48 6E-01 4.431E+OO 4.431E+OO NOT IDENT. RE-184 9.336E+OO 3.425E+Ol 3.451E+Ol NOT IDENT. W-188 9.807E+OO l.247E+02 1.248E+02 FAIL ABUN IR-192 -1. 562K-01 5.335E-01 5.382E-01 FAIL ABUN HG-203 2.509E+OO 4.919E+OO 5.048E+OO FAIL ABUN BI-207 -2.470E-02 6.451E-02 6.546E-02 FAIL ABUN PB-210 4.378E+OO 6.874E+OO 7 .151E+OO NOT IDENT. BI-211 2.776E+OO 6.879E-01 1.428E+OO FAIL ABUN PB-211 -6.341E-02 7.940E-01 7.945E-01 NOT IDENT. RA-223 -3.459E-01 6.502E-01 6.687E-01 FAIL ABUN AC-227 6.193E-02 2.610E-01 2.625E-01 NOT IDENT. TH-227 6.193E-02 2.610E-01 2.625E-01 NOT IDENT. TH-229 3 .118E-01 5.184E-01 5. 372E-01 FAIL ABUN PA-231 8.794E-01 6.242E-01 7.395E-01 NOT IDENT. TH-231 -3.459E-01 6.502E-01 6.687E-01 FAIL ABUN PA-233 -1.557E-02 6.864E-02 6.900E-02 NOT IDENT. PA-234 6. OllE-02 3.680E-01 3.690E-01 NOT IDENT. PA-234M 1.138E+OO 6.167E+OO 6-.189E+00 NOT IDENT. U-235 1.16.8E-01 2.251E-01 2.311E-01 FAIL ABUN NP-237 -l.557E-02 6.864E-02 6.900E-02 NOT IDENT. NP-238 -9.871E+40 2.386E+41 O.OOOE+OO SHORT HLIF NP-239 4.035E-02 3.200E-01 ' 3.206E-01 FAIL ABUN PU-239 3.234E+02 7.073E+02 7.222E+02 FAIL ABUN AM-241 1.208E-02 2.140E-01 2 .141E-01 NOT IDENT. CM-243 1.908E-01 1.978E_:Ol 2.157E-01 FAIL ABUN BK-247 3.487E-02 8.741E-02 8.881E-02 NOT IDENT. CF-249 -2.600E-02 4.145E-02 4.307E-02 NOT IDENT. CF-251 5. 720E-02 1. 291E-01 1.317E-01 NOT IDENT. Page 2968 of 5809
- - - - ** GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 59.6892 87.09 118.9514 136.47 81.1235 45.60 68.0586 87.57 119.0594 140.51 0.0000 46.54 61.2173 88.03 127.9901 143.76 60.2501 49. 72 0.0000 88.34 128.0645 144.24 72. 3.468 51.35 64.0687 88.47 128.0954 145.44 79.7094 51. 87 70.2679 89. 96 126.2374 152.43 62.1633 52.39 75.4637 1093.63 104.2217 153.25 0.0000 52.97 68.4295 91.11 0.0000 323.87 76.9658 53.44 61.3554 92.59 107.9328 156.02 0.0000 54.07 67.6015 93.35 108.0823 158.56 0.0000 57.36 0.0000 94.56 84.8680 159.00 50.:5948 57.53 66 .1311 94.65 84.8813 162.33 59.2449 57.98 68.2737 94.67 84.8848 162.66 0.0000 59.27 66.4148 94.87 84.9149 163.33 58.0823 59.32 66.4231 97. 43 78.5674 165.86 73.1387 59.54 66.4585 98.43 68.5859 176.31 68.6178 60. 96 63.9081 98.44 68.5873 176. 60 0.0000 61.17 63.9402 99.53 63.0850 177. 52 57.8208 62.93 63.8584 100 .11 75.5524 181.07 0.0000 63.29 63.9123 102.03 63.3568 181.52 64.4029 63.58 63.9555 103.18 64.9917 184.41 64.1930 64.28 64.0596 103.37 66.5246 143.76 64.2881 66.73 70.4041 105.21 70.5224 193.51 52.9009 67.24 76.1237 105.31 70.5343 197.03 70.2344 125.81 87.4877 106.12 71.3888 198.01 53.1602 67.75 86.0897 106.47 68.3908 201.83 68.0136 69.67 72.2842 109.28 62.9815 203.43 53.8135 70.83 89.5185 111. 00 7.5.7883 205.31 55.7348 72.81 83.4790 111.76 0.0000 210.85 47.7999 72.87 83.4897 114.06 70.3898 215.65 69.1703 74.66 83.8069 116. 30 0.0000 222 .11 52.7423 74.82 83.8349 116.74 77.6390 227.09 48.5843. 74.97 83.8611 119.76 68.6882 227.38 50.3655 77 .11 84.2342 121.12 81.6633 228.16 0.0000 78.74 88.1268 121. 22 81.6761 228.18 58.3630 79.69 94.0862 121. 78 65. 3960 116.74 58.3630 80.12 76.7822 122.06 58.4141 235.69 53.4418 80.19 0.0000 122.92 58.4900 ' 235. 96 52 .1194 80.57 58.0013 123.07 59.6730 238.63 50. 9112 81.00 74.0150 265.00 62.0702 238.98 . 0.0000 81. 07 95.7975 125.81 67.3581 240.99 51.0242 81. 75 101. 37 68 127.23 58.0801 242.00 51.0724 83.79 74.4222 127.91 60.1026 244.70 41. 7688 84.00 74.4528 129.30 60.2240 252.40 0.0000 85.43 *112.7193 131.20 77.3620 252.80 40.7217 86.55 118.8295 133.02 68.8573 254.15 0.0000 86.79 118.8831 133.52 74.8471 256.23 43.5703 86.94 118.9177 136.00 77.4940 260.90 0.0000 Page 2969 of 5809 ENERGY MDA COUNT.S ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 27.4353 355.39 0.0000 584.27 10.0789 264.80 26.0664 356.01 27.9886 595.83 0.0000 265.00 35.6762 364.49 0.0000 427.87 8.4644 2 68. 22 37.1522 366.42 0.0000 602.52 0.0000 269.46 42.2425 372.51 20.8590 604.72 27 .1387 270.03 42.2640 375.05 27.8604 607.14 35.6592 271.23 46.9056 377.52 20.9299 609.32 29.4626 273.65 0.0000 356.01 29.0254 610.33 25.5093 276.40 40.6466 388.16 31.1154 614.28 28.9625 277.37 40.6798 388.63 0.0000 618.01 14.7906 277.60 40.6878 391.69 23.1390 620.36 28.4749 278.00 40.2387 264.66 30.3571 621. 93 21.6564 279.20 30.5568 401. 81 30.3796 630.19 0.0000 279.54 30.5656 402.40 30.3906 631.29 16.0251 279.70 30. 5696 404.85 24.3506 633.25 10. 3110 280.46 27.8082 410.95 26.4819 . 634. 78 0.0000 283.69 38.1072 413. 71 33.6700 635.95 13.7646 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 35.3691 423. 72 ' 0.0000 645.85 10.3693 285.90 0.0000 427.09 29.8349 657.76 23.1641 287.50 27.0388 427.87 27.7905 657.90 0.0000 290.67 32.2504 433.94 30.9924 661. 66 22.0437 293.27 439.40 37.3125 664.57 0.0000 351.93 36.5919' 453.88 22.9981 666.33' 0.0000 295. 96 40.8379 463.37 25. 2271 666.50 0.0000 879.38 57.8577 468.07 30.5647 667. 71 0.0000 299.98 52.7427 473.00 0.0000 677.62 11. 3897 300.09 52.7472 475.06 27. 5118 685.70 0.0000 300.13 38.6193 476.78 19.0649 695.00 0.0000 301.36 41.4863 477.60 16.9544 696.49 19.4293 302.85 55.6942 482.18 18.0601 696. 51 19.4299 256.23 56.7126 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.0863 306.78 30.3008 497.08 19.2799 697.49 22.0879 308.46 36.9775 505.52 11. 2981 702.65 22.6672 311. 90 38.9780 507.63 0.0000 706.68 31. 0416 316.51 40.0706 511. 00 14.5688 711. 68 18.2825 319.41 0.0000 514.00 12.9707 720. 70 0.0000 320.08 0.0000 514.00 12.9707 721. 93 0.0000 321.04 31. 5928 520.40 26.0293 722.78 19.9979 323.87 33.5794 520.69 0.0000 722. 91 19.9992 325.23 43.2175 522.65 0.0000 723.31 22.8602 328.76 0.0000 527.90 0.0000 724.19 17.1510 333.37 33.3345 528.26 25.0468 727.33 15.2050 333.97 36.2488 529.59 17.4362 733.00 14.3433 334.37 43. 5114 529.87 0.0000 735.93 17.0529 338.28 29.0912 531.02 0.0000 333.97 12.5730 338.32 29.0918 537.26 0.0000 739.50 0.0000 311. 90 29.1376 546.56 0.0000 747.24 16.2285 340.48 29.1376 552.55 23.1542 748.06 14.4297 340.55 0.0000 563.25 17.7357 752.31 20.7778 344.28 30.6784 569.33 22.2355 753.82 0.0000 345.93 46.8037 946.00 22.2380 756.73 23.5284 351. 06 38.1669 569.70 21.1276 756.80 23.5292 351. 93 38.1907 583.19 14.5509 884.68 19. 9650 Page 2970 of 5809 ENERGY MDJI. COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.5198 1274.44 22.6315 1620.50 2.7681 766.42 21. 8005 1001.03 16.7525 1621.92 5.5377 766.84 19.0787 1002.74 19. 7192 1678.03 0.0000 772.60 0.0000 1004.73 17-.7583 1690.97 1.8724 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.8000 778.90 10.2228 1028.54 0.0000 1063.66 4.7551 783.70 0.0000 1037.84 6.3785 1771.35 2.8538 785.37 8.7838 1038.76 0.0000 1791.20 0.0000 792.07 22.9332 631.29 4.7968 1808.65 0.9581 794.95 12.8563 1048.07 0.0000 1810.72 0.0000 795.86 9.1864 1049.04 14.6676 1836.06 3.8525 810.06 20.3175 1050.41 13.0063 810.29 23.0896 1063.66 18.0802 344.28 23. 0911 1077.00 0.0000. 810.76 22.1697 1077.34 11. 0933 815.77 0.0000 1085.87 8.0884 1048.07 0.0000 1093.63 11. 3490 832.01 7.4478 1099.45 11. 3682 834.85 12 .1153 1112. 07 13.2436 835. 71 17.7122 1112.84 15.2847 836.80 0.0000 1115. 54 8.1582 846.75 0.0000 1120.29 12.2534 846.77 20.5908 1120.55 12. 2'542 856.80 0.0000 1221.41 12. 2571 860.56 15.9894 1129. 67 10.9212 871.09 10.5731 1131. 51 0.0000 873.19 9.0694 1147.95 0.0000 875.33 0.0000 1173.23 10.3638 879.38 9.0888 1177.95 19.7167 880.51 4.5461 1189.05 15.6125 883.24 6.6362 1204.77 9.4076 884.68 9.4849 1221.41 18.8987 889.28 8.5501 1231. 02 16-. 8418 894.76 10.4696 1235.36 0.0000 898.04 10.4814 1238.28 13.4992 900. 72 15.2598 1260.41 0.0000 903.28 12.4093 1271.87 9.5746 911.20 15.3140 1274.44 14.9041 912.08. 15.3184 1274.54 14.9041 923.98 0.0000 1291. 59 13.8998 926.50 9.6204 1298.22 0.0000 929 .11 7.7029 1312 .. 11 0.0000 937.49 10.8141 1332.49 10.8026 944 .13 0.0000 1362.66 0.0000 946.00 15.4922 1365.19 7.6225 949.00 11. 6305 1368.63 0.0000 667. 71 0.0000 1384.29 10.9393 962. 31 15.5742 1408.01 4.4004 964.08 19.4788 1457.56 0.0000 966 .17 15.5938 1460.82 7.7960 911.20 12.4863 1489.16 6.7255 968. 97 12.4863 1505.03 11. 2488 983.53 0.0000 1584.12 10.0719 984.45 0.0000 1596.21 0.0000 Page 2971of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:02:43.73
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 9-DEC-2015 14:00:00. Acquisition date : 3-0CT-2016 08:01:44. Sample ID G405235004 Sample quantity 1.48940E+02 GRAM Detector name : GAM09 Detector geometry: CAN Elapsed live time: 0 Ol:OO:OD.00 Elapsed real time: 0 Dl:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 4 4 0 0 0 0 0 4 4 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 2972 of 5809 Energy 58.87 63.49* 74.93 77.15 83.38* 87.17 185.97* 190.86 209.28 238.68* 241. 57 295.43* 299.56 301.06 327.62 338.35* 352.00* 438.80 462.68 510.90* 582.98* 592.66 609.23* 661.71 701.42 727.52 752. 96 768.41 795.16 808.19 820.39 861.30 872.46 910.79* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 42 24 86 149 16 116 74 16 36 428 116 146 33 25 32 89 264 16 40 32 147 35 173 72 18 53 20 24 28 17 7 11 17 90 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 77 163 189 129 126 153 148 79 89 69 96 58 44 34 54 77 91 24 30 64 24 16 52 17 24 28 33 13 7 3 10 14 19 6 1. 95 0.93 1. 03 0.78 0.99 1.14 0.94 1. 00 0.82 0.93 1. 61 1.10 1.16 1.16 2.41 1. 52 1. 29 0.52 1. 07 2.16 1. 38 3.82 1.10 1. 64 1. 39 1. 63 3.45 0.82 1.15 0.73 0. 62 2.20 0.94 L73 117. 40 126.66 149.54 153.99 166.45 174.03 371. 72 381.50 418.36 477.18 482. 96 590.73 599.00 602.00 655. 13 676.60 703.92 877.59 925.37 1021. 86 1166. 08 1185.46 1218.60 1323.62 1403.06 1455.29 1506.21 1537.12 1590.64 1616.71 1641.13 1722.98 1745.32 1822.02 114 124 146 146 165 170 367 378 415 473 473 585 596 596 651 671 699 874 919 1013 1159 1179 1212 1319 1396 1447 1497 1532 1586 1613 1636 1717 1736 1816 7 1.17E-02 37.9 9 6.78E-03 97.6 16 2.39E-02 25.8 4.15E+OO* 16 4.15E-02 14.1 6 4.36E-03117.2. 8 3.23E-02 20.7 11 2.06E-02 35.4 7 4.57E-03 92.7 7 9.88E-03 47.2 15 l.19E-01 5.8 l.17E+00 15 3.21E-02 21.7 10 4.07E-02 12.9 12 9.24E-03 38.1 2.17E+00 12 7.00E-03 50.4 10 8.75E-03 46.8 .11 2.48E_:_02 22.0 12 7.34E-02 9.5 9 4.36E-03 62.4 12 1.12E-02 31.3 17 8.82E-03 67.1 14 4.09E-02 11.1 13 9.70E-03 29.2 14 4. 82E-02 11. 9 11 1.99E-02 16.2 14 4.99E-03 62.9 16 l.47E-02 26.3 17 5.66E-03 69.0 10 6.56E-03 36.5 10 7.71E-03 26.4 8 4. 63E-03 31. 8 8 1.95E-03 86.5 11 3.02E-03 73.0 16 4.75E-03 67.3 12 2.51E-02 12.2 Peak Search Report (continued) Page : 2 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964.44 21 10 1. 25 1929.37 1926 7 5.86E-03 33.3 36 0 968.67 40 21 1.22 1937.82 1933 10 1. llE-02 26.3 37 0 1120.29 50 11 1. 03 2241. 21 2233 15 l.39E-02 20.3 38 0 1183.15 12 5 1. 27 2367.01 2363 9 3.35E-03 43.2 39 0 1216.65 23 9 2.98 2434.04. 2428 12 6.46E-03 33.0 40 0 1220.72 12 4 i. io 2442.17 2439 7 3.19E-03 40.0 41 1 1224.31 17 3 1. 98 2449.36 2446 19 4.80E-03 24.7 1:13E+OO 42 1 1226.95 18 3 1. 98 2454.64 2446 19 4.99E-03 39.4 43 1 1230.12 23 0 1. 80 2461.00. 2446 19 6.30E-03 21. 6 44 0 1239.21 10 20 0.56 2479.18 2473 9 2.'78E-03 89.8 45 0 1460.26* 352 14 1. 63 2921. 51 2914 14 9.77E-02 5. 9 46 0 1542.51 6 2 1. 20 3086.11 3082 7 1.79E-03 51. 7 47 0 1763.43* --.29 0 1. 85 3528.19 3522 11 7.94E-03 20.2 Flag: "*" = Peak area was modified by background subtraction Page 2973 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:02:46 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID .. 9-DEC-2015 14:00:00 G405235004 SOLID GAMMA9 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:01:44 148.94 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 2974 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.146E+OO 1.398E+Ol 1.398E+Ol 11. 70 OK NB-94 702.65 99.81* 2.061E+OO 4.576E-02 4.576E-02 125.83 OK 871. 09 99.89 1. 740E+OO 5.040E-02 5.040E-02 134.51 OK CD-109 88.03 3.70* 4.855E+OO 3.083E+OO 4.830E+OO 55.48 OK SN-126 64.28 9:60 2.292E+OO 7.198E-01 7.198E-01 195.25 OK 86.94 8.90 4.855E+OO 1.282E+OO 1.282E+OO 55.48 OK 87.57 37.00* .4.855E+OO 3.083E-01 3.083E-01 55.48 OK BA-137M 661. 66 89.90* 2.157E+00 l.943E-01 l.980E-01 32.30 OK CS-137 661. 66 85.10* 2.157E+OO 2.053E-01 2.092E-01 32.30 OK TL-208 277.37 6.60 4.352E+OO Line Not Found Absent 583.19 85.00* 2.382E+OO 3.877E-01 3.877E-01 22.10 OK 860.56 12.50 1. 757E+OO 2.538E-01 2.538E-01 145.96 OK BI-211 72. 87 1.23 3.448E+OO Line Not Found Absent 351.06 12.92* 3.588E+OO l.803E-01 1. 803E-01 546.38 OK PB-212 74.82 10.28 3.682E+OO 8.364E-01 8.364E-01 91. 68 OK 77 .11 17.10 3.923E+OO 1.421E+OO 1. 421E+OO 28.16 OK 238.63 43.60* 4.882E+OO 1.167E+OO 1.167E+OO 11.52 OK 300.09 3.30 4.092E+OO l.399E+OO 1.399E+OO 76.19 OK BI-214 609'. 32 45.49* 2. 301E+OO 8.801E-01 8 .. 804E:.._01 23.73 OK 1120.29 14.92 l.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 OK PB-214 74.82 5.80 3.669E+OO Line Not Found <<INT Reject 77 .11 9.70 3.923E+OO 2.506E+OO 2.507E+OO 28.16 OK 87.09 3.41 4.849E+OO Line Not Found <<INT Reject 242.00 7.25 4.832E+OO Line Not Found <<INT Reject 295*.22 18.42 4 .139E+OO 1.093E+OO 1.093E+OO 25.74 OK 351. 93 35.60* 3.588E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.301E+OO 8. 801E-01 8.804E-01 23.73 OK 1120.29 14.92 1. 429E+OO 1. l 71E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 OK RA-224 240.99 4.10* 4.839E+OO *1.444E+OO 1.444E+OO 106. 96 OK RA-226 609.32 45.49* 2. 301E+OO 8. 801E-01 8.804E-01 23.73 OK 1120.29 14.92 l.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.'49 15.30 9. 661E-01 9.205E-01 9.208E-01 40.3'7 OK AC-228 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11. 27 3.706E+OO 1.201E+OO 1.201E+OO 44.00 OK 794.95 4.25 1. 869E+OO 1.809E+OO 1.809E+00 . 52. 80 OK 835. 71 1. 61 1. 799E+OO Line Not Found Absent 911. 20 25.80* 1.682E+OO 1.062E+OO 1.062E+OO 24.49 OK 968. 97 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 OK RA-228 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11.27 3.706E+OO l.201E+OO 1.201E+OO OK 794.95 4.25 1. 869E+OO 1.809E+OO 1.809E+OO 52.80 OK 835. 71 1. 61 1. 799E+OO Line Not .Found Absent 911. 20 25.80* 1.682E+OO l.062E+OO 1.062E+OO 24.49 OK 968. 97 15.80 l.603E+OO 8.012E-01. 8.012E-01 52.66 OK TH-228 74.82 10.28 3.682E+OO 8.364E-01 8.364E-01 91. 68 OK 77 .11 17.10 3.923E+OO 1.421E+OO 1. 421E+OO 28.16 OK 238.63 43.60* 4.882E+OO l.167E+OO 1.167E+OO 11. 52 OK Page 2975 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.092E+OO 1.399E+OO 1.399E+OO 76.19 OK TH-230 609.32 45.49* 2.301E+OO 8.801E-01 8.801E-01 23.73 OK 1120.29 14.92 1.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.205E-01 40. 3*7 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301. 36 5.35* 4.076E+OO 6.560E-01 6.560E-01 100.87 OK TH-232 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11.27 3.706E+OO 1.201E+OO 1.201E+OO 44.00 OK 835.71 1. 61 1.799E+OO -----'Line Not Found Absent 911.20 25.80* 1.682E+OO 1. 062E+OO 1.062E+OO 24.49 OK 968.97 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 OK U-234 609.32 45.49* 2. 301E+OO 8.801E-01 8. 801E-01 23.73 OK 1120.29 14.92 1.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.205E-01 40.37 OK AM-241 59.54 35.90* 1.701E+OO 4.489E-01 4.495E-01 75.85 OK AM-243 43.53 5.90 1. 969E-01 Line Not Found Absent 74.66 67.20* 3.682E+OO 1. 27 9E-01 1.280E-01 91. 68 OK ANH-511 511. 00 100.00* 2.647E+OO 6.485E-02 6.485E-02 134.22 OK Flag: "*" = Keyline Page 2976 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:02:49.39 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l * *Acquisition date 3-0CT-2016 08:01:44 Sensitivity : 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 9-DEC-2015 14:00:00 Analyst initials: MXRl *
Sample ID G405235004 Sample Quantity 1.4894E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-JUN-2016 07:32:22 Eff. : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.398E+Ol 1.603E+OO 5.756E-01 NB-94 4.576E-02 5.643E-02 5.494E-02 CD-:-109 4.830E+OO 2.626E+OO 2.236E+OO SN-126 3.083E-01 1. 676E-01 1.268E-01 BA-137M l.980E-01 6.270E-02 6.185E-02 CS-137 2.092E-01 6.623E-02 6.534E-02 TL-208 3.877E-01 8.398E-02 5.989E-02 BI-211 1.803E-01 9.657E-01 3.372E-01 PB-212 1.167E+OO 1.317E-01 9.158E-02 BI-214 8.804E-01 2.048E-01 1.088E-01 PB-214 1.159E+OO 2.166E-01 3.SlOE-01 RN-222 8.804E-01 2.048E-01 l.088E-01 RA-224 1.444E+OO 1.514E+OO 9.818E-01 RA-226 8.804E-01 2.048E-01 1.088E-01 AC-228 1.062E+OO 2.549E-01 2.386E-01 RA-228 1.062E+OO 2.549E-01 2.386E-01 TH-228 1.167E+OO l.317E-01 9.158E-02 TH-230 8*. 801E-01 2.047E-01 1.088E-01 PA-231 6.560E-01 6.485E-01 7.231E-01 TH-232 l.062E+OO 2.549E-01 2.386E-01 U-234 8.801E-01 2.047E-01 1.088E-01 AM-241 4.495E-01 3.342E-01 3.277E-01 AM-243 l.280E-01 1.lSOE-01 1.048E-01 ANH-511 6.485E-02 8.530E-02 4.609E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 -1.312E+OO 1.196E+Ol 2.345E+Ol NOT IDENT. NA-22 2.943E-02 3.671E-02 8.789E-02 NOT IDENT. NA-24 O.OOOE+OO 1.883E+41 O.OOOE+OO SHORT HLIF AL-26 -5.207E-03 2.342E-02 4.981E-02 NOT IDENT. SC-46 -7.557E-02 3.229E-01 6.092E-01 FAIL ABUN V-48 0.000E+OO l.251E+04 O.OOOE+OO SHORT HLIF Page 2977 of 5809 CR-51 O.OOOE+OO 4.078E+02 O.OOOE+OO SHORT HLIF MN-54 7.091E-03 6.386E-02 l.250E-01 NOT IDENT. C0-56 -4.387E-02 4.399E-01 8.425E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.608E-02 3.948E-02 7. 496E-02 NOT IDENT. C0-58 l.278E-01 4.763E-01 9.224E-01 NOT IDENT. FE-59 -7.773E+OO 8.275E+OO l.291E+Ol NOT IDENT. C0-60 -2.285E-02 2.699E-02 4.509E-02 NOT IDENT. ZN-65 -8. 201E-03 1.538E-01 2.637E-Ol NOT IDENT. GE-68 -3.959E-01 2.345E+OO 4.453E+OO NOT IDENT. AS-73 7.034E+OO 1.17 9E+Ol 2.556E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.264E+03 O.OOOE+OO SHORT HLIF SE-75 1.159E-01 1.817E-01 3.649E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 731E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.308E+02 O.OOOE+OO SHORT HLIF RB-83 5.138E-01 6.149E-01 1.340E+OO NOT IDENT. KR-85 4. 621E+OO 6.934E+OO 1.360E+Ol NOT IDENT. SR-85 4.825E-01 7.244E-01 1.420E+OO NOT IDENT. RB-86 O.OOOE+OO 2.671E+04 O.OOOE+OO SHORT HLIF Y-88 8.201E-02 1.545E-01 4.203E-01 NOT IDENT. Y-91 3.388E+02 5.518E+02 l.185E+03 NOT IDENT. NB-95 -2.377E-01 8.955E-01 l.468E+OO NOT IDENT. NB-95M 3.039E-01 2.355E+OO 4.109E+OO NOT IDENT. ZR-95 2.840E-01 1.845E+OO 3.234E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.326E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.655E-02 2.779E-02 4.988E-02 NOT IDENT. RH-102 7.622E-03 5.477E-02 l.104E-01 NOT IDENT. RU-l03 4 .191E+OO 5.418E+00 1.168E+Ol FAIL ABUN RH-106 4.606E-02 3.733E-01 7.751E-01 NOT IDENT. RU-106 4.606E-02 3.733E-01 7. 751E-01 NOT IDENT. AG-108M 2.466E-02 2.478E-02 5.507E-02 NOT IDENT. AG-110M -6. 962E-02 8.794E-02 l.452E-01 NOT IDENT. SN-113 -2.848E-02 2.040E-01 4.059E-01 NOT IDENT. CD-115 O.OOOE+OO 2.022E+39 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO 7. 413E+04 O.OOOE+OO SHORT HLIF TE-123M 3. 041E-02 1.078E-01 2.135E-01 NOT IDENT. SB-124 7.987E-01 1.642E+OO 4.128E+OO NOT IDENT. SB-125 -2.940E-02 9. 972E-02 1.932E-01 FAIL ABUN TE-125M 2.234E+02 2.220E+02 4 :761E+02 NOT IDENT. I-126 O.OOOE+OO 7.250E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.274E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.679E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.399E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.933E+26 O.OOOE+OO SHORT HLIF BA-133 1.473E-03 3.922E-02 6.709E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.121E-02 l.158E-01 FAIL ABUN CS-135 -1.026E-01 1.337E-01 2. 271E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 2.525E+05 O.OOOE+OO SHORT HLIF CE-139 -3.435E-04 l.007E-01 l.924E-01 NOT IDENT. BA-140 O.OOOE+OO 1.062E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.202E+05 O.OOOE+OO SHORT HLIF CE--141 6.175E-01 2.076E+Ol 4.018E+Ol NOT IDENT. CE-143 O.OOOE+OO l.514E+41 O.OOOE+OO SHORT HLIF CE-144 -l.473E-01 3. 011E-01 5.628E-01 NOT IDENT. PM-144 5.270E-03 4.419E-02 8.239E-02 NOT IDENT. PR-144 4.725E-01 3.840E+OO 7.163E+OO NOT IDENT. PM-146 1.615E-02 3.930E-Q2 8.246E-02 NOT IDENT. ND-147 O.OOOE+OO 2.882E+07 O.OOOE+OO SHORT HLIF PM-147 -2.104E+02. 6.816E+02 l.307E+03 NOT IDENT. PM-149 O.OOOE+OO 3.252E.f-40 O.OOOE+OO SHORT HLIF EU-150 -1.637E-02 2.736E-02 4.185E-02 FAIL ABUN EU-152 -7.932E-03 8. 013E-02 l.466E-01 FAIL ABUN GD-153 5.437E:...03 1. 603E-01 3.174E-01 NOT IDENT. EU-154 6.543E-02 9.358E-02 2.185E-01 FAIL ABUN EU-155 1.214E-01 9.804E-02 2 .110E-01 FAIL ABUN TB-160 l.399E-01 1.814E+OO 3.562E+OO FAIL ABUN H0-166M 1.280E-02 5.584E-02 1.121E-Ol FAIL ABUN TM-171 6.161E+OO 3.042E+Ol 6.404E+Ol NOT IDENT. HF-172 -6.209E-02 1. 763E-01 3.368E-01 FAIL ABUN LU-172 2.174E-03 8.933E-02 l.675E-01 FAIL ABUN LU-176 2.479E-03 2.245E-02 4.216E-02 FAIL ABUN HF-181 -5.894E-01 3.197E+OO 6.381E+OO FAIL ABUN Page 2978 of 5809 TA-182 9.666E-01 7. 572E-01 1.821E+OO FAIL ABUN RE-183 0.000E+OO 6.730E+OO 7.122E+OO FAIL ABUN RE-184 -8.777E-02 3.088E+Ol 5.919E+Ol NOT IDENT. W-188 8.756E+Ol 8.965E+Ol l.804E+02 FAIL ABUN IR-192 -5.684E-02 4. 725E-01 8.544E-01 FAIL ABUN HG-203 -l.680E+OO 2.336E+OO 3.975E+OO NOT IDENT. BI-207 -8.270E-04 3.599E-02 7.363E-02 FAIL ABUN PB-210
6. 344E-01 6.095E+OO 1.271E+Ol NOT IDENT. PB-211 -1. 763E-01 5.784E-01 1.130E+OO NOT IDENT. BI-212 O.OOOE+OO 1.064E+OO 1.386E+OO FAIL ABUN RN-219 6.745E-02 3.160E-01 6.557E-01 NOT IDENT. RA-223 -4.703E-02 5.77EiE-01 9.710E-01 FAIL ABUN AC-227 -8.334E-02 2.338E-01 4.178E-01 FAIL ABUN TH-227 -8.334E-02 2.338E-01 4.178E_:Ol FAIL ABUN TH-229 2.894E-01 4.550E-01 8.509E-01 FAIL ABUN TH-231 -4.703E-02 5.776E-01 9.710E-01 FAIL ABUN PA-233 -1.322E-02 5.324E-02 9.572E-02 FAIL ABUN PA-234 3.338E-02 2.817E-01 5. 511E-01 NOT IDENT. PA-234M -3.346E-01 4.292E+OO 8.503E+00 NOT IDENT. TH-234 1. 868E+OO 3.573E+00 3.066E+00 FAIL ABUN U-235 * -2;460E-02 1.600E-01 3.047E-01 FAIL 'ABUN NP-237 -1.322E-02 5.324E-02 9. 572E-02 *FAIL ABUN NP-238 O.OOOE+OO 1.898E+41 O.OOOE+OO SHORT HLIF U-238 1. 868E+OO 3.573E+OO 3.066E+OO FAIL ABUN NP-239 -4.922E-02 2.028E-01 3.920E-01 NOT IDENT. PU-239 2.068E+02 2. 724E+02 5.608E+02 NOT IDENT. CM-243 -5.301E-02 8.741E-02 1.649E-01 NOT IDENT. BK-247 2.268E-03 6.609E-02 l.239E-01 FAIL ABUN CM-247 1. 361E-02 2.862E-02 6.109E-02 NOT IDENT. CF-249 -l.180E-02 3. 731E-02 6.494E-02 NOT IDENT. CF-251 5.653E-02 1.029E-01 2.054E-01 NOT *IDENT. Page 2979 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:02:45.10 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 339 10.66* l.146E+OO 1.398E+Ol 1.398E+Ol 11. 70 NB-94 702.65 19 99.81* 2.061E+OO 4.576E-02 4.576E-02 125.83 871.09 17 99.89 1. 740E+OO 5.040E-02 5.040E-02 134.51 CD-109 . 88. 03 146 3.70* 4.855E+OO 4.090E+OO 6.408E+OO 41. 34 SN-126 64.28 31 9.60 2.292E+OO 7.198E-01 7.198E-01 195.25 86.94 14 fr 8.90 4.855E+00 1. 701E+OO 1. 701E+OO 41. 34 87.57 146 37.00* 4.855E+OO 4.090E-01 4.090E-01 41. 34 BA-137M 661.66 75 89.90* 2.157E+OO l.943E-01 1.980E-01 32.30 CS-137 661.66 75 85.10* 2.157E+OO 2.053E-01 2.092E-01 32.30 TL-208 277.37 ------6.60 4.352E+OO ------Line Not Found ------583.19 156 85.00* 2.382E+OO 3.877E-01 3.877E-01 22.10 860.56 11 12.50 1. 757E+00 2.538E-01 2.538E-01 145.96 BI-211 72.87 ------1. 23 3.448E+OO ------Line Not Found ------351.06 293 12.92* 3.588E+OO 3.191E+OO 3.191E+OO 19.07 PB-212 74.82 109 10.28 3.682E+OO 1.453E+OO 1.453E+OO 51. 64 77 .11 189 17.10 3.923E+OO 1.421E+OO 1.421E+OO 28.16 238.63 493 43.60* 4 .. 882E+OO l.167E+00 1.167E+OO 11. 52 300.09 37 3.30 4.092E+OO 1.399E+OO 1.399E+OO 76.19 BI-214 609.32 183 45.49* 2.301E+00 8.801E-01 8.804E-01 23.73 1120.29 50 14.92 1.429E+OO l.171E+OO l.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.208E-01 40. 37. PB-214 74.82 109 5.80 3.682E+OO 2.575E+OO 2.576E+OO 51.64 77 .11 189 9.70 3.923E+OO 2.506E+OO 2.507E+OO 28.16 87.09 146 3.41 4.855E+OO 4.438E+OO 4.440E+OO 41. 34 242.00 133 7.25 4.839E+OO 1.909E+OO 1.910E+OO 43.31 295.22 165 18.42 4 .139E+OO 1.093E+OO 1.093E+OO 25.74 351. 93 293 35.60* 3.588E+OO 1.158E+OO 1.159E+OO 19.07 RN-222 609.32 183 45.49* 2.301E+OO 8. 801E-01 8.804E-01 23.73 1120.29 50 14.92 l.429E+OO l.171E+OO l.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 RA-224 240.99 133 4.10* 4.839E+00 3.376E+OO 3.376E+OO 43.31 RA-226 609.32. 183 45.49* 2.301E+OO 8.801E-01 8.804E-01 23.73 1120.29 50 14.92 l.429E+OO l .171E+OO l.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 AC-228 105.21 ------1.10 5.896E+00 ------Line Not Found ------338.32 100 11. 27 3.706E+OO l.201E+OO 1.201E+OO 44.00 794.95 29 4.25 l.869E+OO 1.809E+OO 1.809E+OO 52.80 835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 91 25.80* 1. 682E+OO 1.062E+OO *1.062E+OO 24.49 968. 97 40 15.80 1.603E+00 8.012E-01 8.012E-01 52.66 RA-228 105.21 ------1.10 5. 896E+OO ------Line Not Found ------338.32 100 11. 27 3.706E+OO l.201E+OO 1.201E+OO 44.00 794.95 29 4.25 1.869E+OO 1.809E+OO 1. 809E+OO 52.80 835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911.20 91 25.80* 1.682E+OO 1.062E+OO 1.062E+OO 24.49 968. 97 40 15.80 1.603E+00 8.012E-01 8.012E-01 52.66 TH:-228 74.82 109 10.28 3.682E+OO 1.453E+OO l.453E+OO 51. 64 Page 2980 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Nuclide Type: Uncorrected De.cay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 189 17.10 3.923E+OO 1.421E+OO 1.421E+OO 28.16 238.63 493 43.60* 4.882E+OO 1.167E+OO 1.167E+OO 11. 52 300.09 37 3.30 4.092E+OO 1.399E+OO l.399E+OO 76.19 TH-230 609.32 183 45.49* 2.301E+OO 8. 801E-01 8.801E-01 23.73 1120.29 50. 14.92 1.429E+OO 1. l 71E+OO 1.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.205E-01 40.37 PA-231 283.69 ------1. 70 4.275E+OO ------Line Not Found ------301.36 28 5.35* 4.076E+OO 6.560E-01 6.560E-01 100.87 TH-232 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 100 11. 27 3.706E+OO 1.201E+OO 1.201E+OO 44.00 835. 71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 91 25.80* 1.682E+OO 1.062E+OO 1.062E+OO 24.49 968. 97 40 15.80 1.603E+OO -8. 012E-01 8:012E-01 52.66 U-234 609.32 183 45.49* 2.301E+OO 8. 801E-01 8.801E-01 23.73 1120.29 50 14.92 1.429E+OO 1.171E+OO 1. l 71E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.205E-01 40.37 AM-241 59.54 54 35.90* 1. 7-0lE+OO 4.489E-01 4.495E-01 75.85 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 109 67.20* 3.682E+OO 2."223E-01 2.223E-01 51. 64 ANH-511 511. 00 34 100.00* 2.647E+OO 6.485E-02 6.485E-02 134.22 Flag: "*" Key line Page 2981of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Total number of lines in spectrum 47 Number of unidentified lines 11 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 NB-94 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-241 AM-243 ANH-511 Hlife l.25E+09Y 20300.00Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1.41E+l0Y 7.04E+08Y l.41E+10Y 1600. DOY 1600. DOY 1600. OOY 1.41E+l0Y 1600.00Y l.41E+l0Y 1. 41E+l0Y l.41E+10Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 2.45E+05Y 432.60Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 00 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.398E+Ol 4.576E-02 4.090E+OO 4.090E-01 1.943E-01 2.053E-01 3.877E-01 3.191E+OO l.167E+00 8.801E-01 l.158E+OO 8. 801E-01 3.376E+OO 8. 801E-01 1.062E+OO 1.062E+OO l.167E+00 8.801E-01 6.560E-01 l.062E+OO 8. 8 OlE-01 4.489E-01 2.223E-01 6.485E-02 3.835E+Ol 3.835E+Ol Decay Corr pCi7GRAM l.398E+Ol 4.576E-02 6.408E+OO 4.090E-01 l.980E-01 2.092E-01 3.877E-01 3.191E+OO 1.167E+OO 8.804E-01 1.159E+OO 8.804E-01 3.376E+OO 8.804E-01 1.062E+OO 1.062E+OO 1.167E+OO 8.801E-01* 6.560E-01 1.062E+OO 8.801E-01 4.495E-01 2*. 223E-01 6.485E-02 4.068E+Ol 4.068E+Ol 76.60% Decay Corr 2-Sigma Error 0.164E+Ol 5.759E-02 2.649E+OO l.691E-01 0.640E-01 0.676E-01 0.857E-01 0.609E+OO 0.134E+OO 2.089E-01 0.221E+OO 2.089E-01 1.462E+OO 2.089E-01 0.260E+OO 0.260E+00 0.134E+OO 2.089E-01 6.617E-01 0.260E+OO 2.089E-01 3.410E-01 1.148E-01 8.704E-02 Manually accepted 2-Sigma %Error 11. 70 125.83 41. 34 41. 34 32.30 32.30 22.10 19.07 11. 52 23.73 19.07 23.73 43.31 23.73 24.49 24.49 11. 52 23.73 100.87 24.49 23.73 75.85 51. 64 134.22 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 2982 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235004 Acquisition date : 3-0CT-2016 08:01:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.38 20 158 0.99 166.45 165 6 4.36E-03 **** 4.53E+OO T 0 185.97 87 174 0.94 371.72 367 11 2.06E-02 70.8 5.74E+OO T 0 190.86 19 92 1. 00 381.50 378 7 4.57E-03 **** 5.66E+OO 0 209.28 41 104 0.82 418.36 415 7 9.88E-03 94.3 5.35E+OO 0 327.62 35 61 2.41 655.13 651 10 8.75E-03 93.5 3.81E+OO T 0 438.80 17 26 0.52 877.59 874 9 4.36E-03 **** 2.99E+OO T 0 462. 68 44 32 1. 07 925.37 919 12 1.12E-02 62.7 2.87E+OO T 0 592.66 37 17 3.82 1185.46 1179 13 9.70E-03 58.4 2.35E+OO 0 727. 52 55 29 1. 63 1455.29 1447 16 1.47E-02 52.6 2.00E+OO T 0 752.96 21 34 3.45 1506.21 1497 17 5.66E-03 **** 1.95E+OO T 0 768.41 24 14 0.82 1537.12 1532 10 6.56E-03 73.1 1.92E+OO 0 808.19 17 3 0.73 1616.71 1613 8 4.63E-03 63.6 1. 85E+OO 0 820.39 7 10 0.62 1641.13 1636 8 1. 95E-03 **** 1.82E+OO 0 964. 44 21 10 1.25 1929.37 1926 7 5.86E-03 66.6 l.61E+OO T 0 1183 .15 12 5 1.27 2367.01 2363 9 3.35E-03 86.4 1.37E+OO 0 1216.65 23 9 2.98 2434.04 2428 12 6.46E-03 66.1 1. 34E+OO 0 1220. 72 11 3 1.10 2442.17 2439 7 3.19E-03 79.9 1.33E+OO T 1 1224.31 17 3 1. 98 2449.36 2446 19 4.80E-03 49.5 1. 33E+OO 1 1226.95 18 3 1. 98 2454.64 2446 19 4.99E-03 78.7 1. 33E+OO 1 1230.12 22 0 1. 80 2461.00 2446 19 6.30E-03 43.2 1.32E+OO T 0 1239.21 10 20 0.56 2479.18 2473 9 2.78E-03 **** 1.32E+OO .T 0 1542.51 6 1 1. 20' 3086.11 3082 7 1. 79E-03 **** 1.09E+OO Flags: "T" = Tentatively associated Page 2983 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:03:14.91 *******************************************************************************
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Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l *
Acquisition date 08:01:44 Sensitivity 1.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 9-DEC-2015 14:00:00 Nuclide Library : SOLID *
Sample ID G405235004 Analyst init'ials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4894E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16 '* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-94 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 B.I-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-241 AM-243 ANH-511 Le (pCi/GRAM 2.316E-01 2.408E-02 1. 056E+OO 5.937E-02 2.726E-02 2.879E-02 2.649E-02 1.534E-01 4.244E-02 4.772E-02 1.700E-01 4.772E-02 4.550E-01 4.772E-02 1.033E-01 1.033E-01 4.244E-02 4.770E-02 3.289E-01 1.033E-01 4.770E-02 1.524E-01 4.944E-02 2.039E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 2984 of 5809 Le (pCi/GRAM 1.054E+Ol 3. 729E-02 O.OOOE+OO 1. 765E-02 2.566E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 . Page 2985 of 5809 5.502E-02 O.OOOE+OO 3.460E-02 3.906E-Ol 5.570E+OO 1.637E-02 1. 096E-01 1.914E+OO l.188E+Ol O.OOOE+OO 1.674E-01' O.OOOE+OO O.OOOE+OO 6.039E-01 6.150E+OO 6.424E-01 O.OOOE+OO 1.586E-01 5.249E+02 6. 418E-,01 1.906E+OO l.450E+00 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 2.'294E-02 4.873E-02 5.282E+OO 3.332E-01 3.332E-01 2. 496E-02 5.990E-02 1.829E-01 O.OOOE+OO O.OOOE+OO 9.882E-02 1.618E+OO 8. 710E-02 2.216E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.016E-02 0.000E+OO 5.216E-02 l.036E-01 O.OOOE+OO O.OOOE+OO 8.953E-02 O.OOOE+OO O.OOOE+OO 1. 871E+Ol O.OOOE+OO 2.602E-01 3.521E-02 3.062E+OO 3. 711E-02 O.OOOE+OO 6.033E+02 O.OOOE+OO 1. 8 92E-02 6.572E-02 l.480E-:-01 9.296E-02 9.894E-02 l.547E+OO 4.973E-02 2.975E+Ol l.547E-01 7.359E-02 l.919E-02 2.773E+OO 7.936E-01 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT .IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT .IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 w....:188 IR_.:.192 HG-203 BI-207 PB-210 PB-211 BI-21*2 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 2986 of 5809 3.301E+OO 2.587E+Ol 8.199E+Ol 3.910E-01 l.816E+OO 3.049E-02 5.892E+OO 5.064E-01 6.410E-01 2.946E-01 4.392E-01 l.927E-01 l.927E-01 3. 965E-01 4.392E-01 4.320E-02 2.402E-01 3.725E+OO i.446E+OO l.419E-01 4.320E-02 O.OOOE+OO l.446E+OO l.813E-01 2.624E+02 7.638E-02 5.670E-02 2. 74;9E-02 2.923E-02 9.565E-02 FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:03:28.23 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l * *Acquisition date 3-0CT-2016 08:01:44 Sensitivity : 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 9-DEC-2015 14:00:00 Nuclide Library : SOLID *
Sample ID G405235004 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4894E+02 GRAM *
Quantity Err ( % ) : 1. 3428E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * * '* Eff. Cal. date 07:32:22 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity_ Act Error TPU Nuclide (pCi/GRAM ) ( 1. 96-s igma) ( 1. 96-sigma) K-40 1.398E+Ol 1. 761E+OO 1. 761E+OO NB-94 4.576E-02 5.647E-02 5.647E-02 CD-109 4.830E+OO 2.663E+OO 2.663E+OO SN-126 3.083E-01 l.692E-01 1.692E-01 BA-137M l.980E-01 6.327E-02 6.327E-02 CS-137 2.092E-01 6.684E-02 6.684E-02 TL-208 3.877E-01 8.558E-02 8.558E-02 BI-211 1.803E-01 9.829E-01 9.829E-01 PB-212 l.167E+00 1.454E-01 l.454E-01 BI-214 8.804E-01 2.082E-01 2.082E-01 PB-214 1.159E+OO 2.218E-01 2.218E-01 RN-222 8.804E-01 2.082E-01 2.082E-01 RA-224 1. 444E+OO 1.521E+OO 1.521E+OO RA-226 8.804E-01 2.082E-01 2.082E-01 AC-228 1.062E+OO 2.606E-01 2.606E-01 RA-228 1. 062E+00 2.606E-01 2.606E-01 TH-228 l.167E+OO 1.454E-01 l.454E-01 TH-230 8.801E-01 2. 081E-01 2.081E-01 PA-231 6.560E-01 6.634E-01
6.634E-01 TH-232 l.062E+OO 2.606E-01 2.606E-01 u-234 8. 801E-01 2. 081E-01 2.081E-01 AM-241 4.495E-01 3.359E-01 3.359E-01 AM-243 1.280E-01 1.159E-01 1:159E-01 ANH-511 6.485E-02 8.534E-02 8.534E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) BE-7 -1.312E+OO 1.196E+Ol 1.198E+Ol NOT IDENT. NA-22 2.943E-02 3.673E-02 3.905E-02 NOT IDENT. NA-24 1.000E+41 1.933E+41 O.OOOE+OO SHORT HLIF AL-26 -5.207E-03 2.343E-02 2;354E-02 NOT SC-46 -7.557E-02 3.229E-01 3.247E-01 FAIL ABUN V-48 1. 07 5E+03 l.251E+04 l.252E+04 SHORT HLIF Page 2987 of 5809 CR-51 -2.238E+02 4.079E+02 4.202E+02 SHORT HLIF MN-54 7.091E-03 6.386E-02 6.394E-02 NOT IDENT. C0-56 -4.387E-02 4.399E-01 4.404E-01 FAIL ABUN MN-56 -1.000E+41 8.989E+41 O.OOOE+OO SHORT HLIF C0-57 -1. 60*8E-02 3.948E-02 4.014E-02 NOT IDENT. C0-58 l.278E-01 4.763E-01 4.798E-01 NOT IDENT. FE-59 -7.773E+OO 8.294E+OO 9.004E+OO NOT IDENT. C0-60 -2.285E-02 2.700E-02 2.890E-02 NOT IDENT. ZN-65 -8.201E-03 1.538E-01 1.539E-01 NOT IDENT. GE-68 -3.959E-Ol 2.345E+OO 2.352E+OO NOT IDENT. AS-73 7.034E+OO 1.188E+Ol l.230E+Ol NOT IDENT. AS-74 1.324E+03 5.265E+03 .5.299E+03 SHORT HLIF SE-75 1.159E-01 1.818E-01 1. 891E-01 NOT IDENT. BR-77 l.533E+38 1.322E+39 O.OOOE+OO SHORT HLIF SR-82 l.195E+02 6.308E+02 6.331E+02 SHORT HLIF RB-83 5 .138E-01 6.189E-01 6.608E-01 NOT IDENT. KR-85 4.621E+00 6.937E+OO 7.243E+OO NOT IDENT. SR-85 4.825E-01 7.246E-01 7.566E-01 NOT IDENT. RB-86 -6.350E+02 2.671E+04 2. 671E+04 SHORT HLIF Y-88 8.201E-02 l.546E-01 l.590E-01 NOT IDENT. Y-91 3.388E+02 5.519E+02 5.726E+02 NOT IDENT. NB-95 -2.377E-01 8.956E-01 9.020E-01 NOT IDENT. NB-95M 3.039E-01 2.355E+OO 2.359E+OO NOT IDENT. ZR-95 2.840E-01 1. S45E+OO l.849E+OO NOT IDENT. NB-97 -l.000E+41 2.193E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 3 .*295E+41 O.OOOE+OO SHORT HLIF M0-99 -4.049E+31 1.327E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 5.879E+41 0.000E+OO SHORT HLIF RH-101 -2.655E-02 2.820E-02 3.063E-02 NOT IDENT. RH-102 7.622E-03 5.477E-02 5.488E-02 NOT IDENT. RU-103 4.191E+00 5.421E+oo* 5.741E+OO FAIL ABUN RH-106 4.606E-02 3.733E-01 3.739E-01 NOT IDENT. RU-106 4.606E-02 3.733E-01 3.739E-01 NOT IDENT. AG-108M 2.466E-02 2.480E....:02 2.718E-02 NOT IDENT. AG-110M -6. 962E-02 8.801E-02 9.344E-02 NOT IDENT. SN-113 -2.848E-02 2.040E-01 2.044E-01 NOT IDENT. CD-115 1. 572E+39 2.042E+39 O.OOOE+OO SHORT HLIF SN-117M 1. 471E+04 7.415E+04 7.445E+04 SHORT HLIF TE-123M 3.041E-02 1.078E-01 1. 086E-01 NOT IDENT. SB-124 7.987E-01 l.643E+OO 1.682E+OO NOT IDENT. SB-125 -2.940E-02 9.972E-02 1.006E-01 FAIL ABUN TE-125M 2.234E+02 2.224E+02 2. 441E+02 NOT IDENT. I-126 7.169E+05 7.315E+05 7.997E+05 SHORT HLIF SB-126 8.367E+05 9.405E+05 l.013E+06 SHORT HLIF SB-127 -3.384E+21 l.742E+22 0.000E+OO SHORT HLIF I-131 2.533E+09 4.401E+09 4.547E+09 SHORT HLIF I-132 -l.000E+41 l.857E+42 O.OOOE+OO SHORT HLIF TE-132 -l.554E+26 3.000E+26 O.OOOE+OO SHORT HLIF BA-133 1.473E-03 3.922E-02 3.922E-02 NOT IDENT. I-133 -1.000E+41 2.884E+41 O.OOOE+OO SHORT HLIF CS-134 1.183E-01 6.141E-02 8 .133E-02 FAIL ABUN CS-135 -1.026E-01 1.338E-01 1.416E-01 NOT IDENT. I-135 1.000E+41 l.184E+42 O.OOOE+OO SHORT HLIF CS-136 -1.122E+05 2.528E+05 2.578E+05 SHORT HLIF CE-139 -3.435E-04 l.007E-01 l.007E-01 NOT IDENT. BA-140 -5.276E+05 1.062E+06 1.088E+06 SHORT HLIF LA-140 l.248E+03 2.202E+05 2.202E+05 SHORT HLIF CE-141 6.175E-01 2.076E+Ol 2.076E+Ol NOT IDENT. CE-143 -1.000E+41 1. 517E+41 O.OOOE+OO SHORT HLIF CE-144 -1. 473E-01 3.012E-01 3.085E-01 NOT IDENT. PM-144 5.270E-03 4.420E-02 4.426E-02 NOT IDENT. PR-144 4. 725E-01 3.840E+OO 3.846E+00 NOT IDENT. PM-146 l.615E-02 3.932E-02 3.999E-02 NOT IDENT. ' ND-147 -2.097E+07 2.884E+07 3.035E+07 SHORT HLIF PM-1.47 -2.104E+02 6.816E+02 6.882E+02 NOT IDENT. PM-149 -l.076E+40 3.261E+40 O.OOOE+OO SHORT HLIF EU-150 -1.637E-02 2.737E-02 2.835E-02 FAIL ABUN EU-152 -7.932E-03 8. 013E-02 8.021E-02 FAIL ABUN GD-153 5.437E-03 l.603E-01 l.603E-01 NOT IDENT. EU-154 6.543E-02 9.362E-02 9.815E-02 FAIL ABUN EU-155 l.214E-01 9.842E-02 1. 12 6E-01 FAIL ABUN TB-160 l.399E-01 1.814E+OO 1. 815E+OO FAIL ABUN H0-166M l.280E-02 5.585E-02 5.615E-02 FAIL ABUN TM-171 6.161E+OO 3.042E+Ol 3.055E+Ol NOT IDENT. HF-172 -6.209E-02 1.766E-01 1. 788E-01 FAIL ABUN LU-172 2.174E-03 8.933E-02 8.933E-02 FAIL ABUN LU-176 2.479E-03 2.245E-02 2.248E-02 FAIL ABUN HF-181 -5.894E-01 3.197E+OO 3.208E+OO FAIL ABUN Page 2988 of 5809 TA-182 9.666E-01 7.581E-01 8.744E-01 FAIL ABUN RE-183 9.053E+OO 6.876E+OO 7.996E+OO FAIL ABUN RE-184 -8.777E-02 3.088E+01 3.088E+Ol NOT IDENT. .w-188 8.756E+Ol 9.018E+Ol 9.844E+Ol FAIL ABUN IR-192 -5.684E-02 4.725E-01 4.732E-01 FAIL ABUN HG-203 -l.680E+OO 2.337E+OO 2.457E+OO NOT IDENT. BI-207 -8.270E-04 3.599E-02 3.599E-02 FAIL ABUN PB-210 6.344E-01 6.095E+OO 6.102E+OO NOT IDENT. PB-211 -l.763E-01 5.785E-01 5.839E-01 NOT IDENT. BI-212 2.064E+OO l.069E+OO 1.417E+OO FAIL ABUN RN-219 6.745E-02 3.162E-01 3.176E-01 NOT IDENT. RA-223 -4.703E-02 5.776E-01 5.780E-01 FAIL ABUN AC-227 -8.334E-02 2.341E-01 2.371E-01 FAIL ABUN TH-227 -8.334E-02 2.341E-01 2.371E-01 FAIL ABUN TH-229 2.894E-01 4.552E-01 4.736E-01 FAIL ABUN TH-231 -4.703E-02 5.776E-01 5.780E-01 FAIL ABUN PA-233 -l.322E-02 5.324E-02 5.358E-02 FAIL ABUN PA-234 3.338E-02 2.843E-01 2.847E-01 NOT IDENT, PA-234M -3.346E-01 4.292E+OO 4.295E+OO NOT IDENT. TH-234 l.868E+OO 3.597E+OO 3.695E+00 FAIL ABUN U-235 -2.460E-02 1.600E-01 l.604E-01 FAIL ABUN NP-237 -1.322E-02 5.324E-02 5. 358E_..:.02 FAIL ABUN NP-238 1.000E+41 1.898E+41 0.000E+OO SHORT HLIF U-238 1.868E+OO 3.597E+OO 3.695E+OO FAIL ABUN NP-239 -4.922E-02 2.029E-01 2.041E-01 NOT IDENT. PU-239 2.068E+02 2. 725E+02 2.880E+02 NOT IDENT. CM-243 -5.301E-02 8.755E-02 9.075E-02 NOT IDENT. BK-247 2.268E-03 6.610E-02 6.610E-02 FAIL ABUN CM-247 1.361E-02 2. 871E-02 2.936E-02 NOT IDENT. CF-249 -l.180E-02 3.732E-02 3.770E-02 NOT IDENT. CF-251 5.653E-02 1.031E-01 1.062E-01 NOT IDENT. Page 2989 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 44.2373 87.09 72. 3018 136:47 63.3131 45.60 48.4640 87.57 72.3787 140.51 0.0000 46.54 43.1295 88.03 94.6541 143.76 59.1933 49. 72 0.0000 88.34 94. 7184 144.24 57.2949 51.35 50.9800 88.47 94.7455 145.44 60.3198 51. 87 47.8720 89. 96 77.4505 152.43 73.7423 52.39 53.5440 1093.63 135 .1493 153.25 0.0000 52.97 51. 2388 91.11 0.0000 323.87 58.1628 53.44 46.5024 92.59 75.2317 156.02 0.0000 54.07 57.8386 93:35 107.2662 158.56 0.0000 57.36 0.0000 94.56 120.8698 159.00 46.6572 57.53 51. 9465 94.65 120.8915 162.33 52.8641 57.98 58.5162 94.67 120. 8967 162.66 0.0000 59.27 58.7348 94.87 104.0505 163.33 55.9359 59.32 58.7433 97.43 58 .1113 165.86 60.1447 59.54 58.7802 98.43 68.9799 176.31 56.9408 60.96 44.2631 98.44 68.9811 176. 60 61.17 44.2893 99.53 61.0528 177.52 49.9039 62.93 69.2328 100 .11 67.4160 181. 07 0.0000 63-. 2 9 69. 3013 102.03 59.5532 181. 52 54.6037 63.58 69.3563 103.18 65 .1143 184.41 57.5492 64.28 69.4888 103.37 65.1385 143.76 57.6466 66.73 75.4984 105.21 56.2930 193.51 48,.5145. 67.24 82.2706 105.31 49.0388 197.03 54.2947 125.81 74.5749 106.12 47.2964 198.01 48.0882 67.75 75.7010 106. 4 7. 53.6992 201.83 52.5131 69.67 74.6816 109.28 41.1764 203.43 69.4513 70.83 90.8935 111. 00 74.3567 205.31 52.0297 72.81 94.7316 111. 76 0.0000 210.85 49.5399 72.87 94.7461 114.06 60.9299 215.65 45.9021 74.66 91. 7 677 116.30 0.0000 222 .11 48.3913 74.82 91. 8040 116.74 55.6604 227.09 42.1724 74.97 91.8377 119.76 45.7012 227.38 47.5946 77 .11 92.3148 121.12 54.2250 228.16 0.0000 78.74 92.6741 121. 22 54.2343 228.18 56.2982 79.69 92.8817 121. 78 56.1594 116.74 56.2982 80.12 68.8708 122.06 56.1868 235.69 52.3938 80.19 0.0000 122.92 41.2653 235.96 50.9534 so.57 67.2193 123.07 45.0282 ' 238.63 53.6536 81. 00 67.2865 265.00 47.8930 238.98 0.0000 81. 07 75.9258 125.81 49.0107 240.99 53.7881 81.75 67.4038 127.23 63.3007 242.00 53.8457 83.79 72. 9277 127.91 54.8609 244.70 41.1415 84.00 72. 9623 129.30 54.0402 252.40 0.0000 85.43 73.1975 131. 20 64.6735 252.80 41.1169 86.55 72. 2154 133.02 59.1439 254.15 0.0000 86.79 72. 2539 133.52 60.1469 256.23 54.6420 86.94 72.2778 136.00 57.5139 260.90 0.0000 Page 2990 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 30.3626 355.39 0.0000 584.27 19.7302 264.80 35.9902 356.01 25.9889 595.83 0.0000 265.00 38.2469 364.49 0.0000 427.87 19.8994 268.22 50.7816 366.42 0.0000 602.52 0.0000 269.46 36.1553 372. 51 28.3773 604. 72 14.2444 270.03 47.4794 375.05 27.1959 607.14 17.1145 271.23 48.6663 377.52 23.5308 609.32 17.1335 273.65 0.0000 356.01 31.1073 610.33 17.1423 276.40 35.2600 388.16 32.4548 614.28 20.0396 277.37 42.1230 388.63 0.0000 618.01 9.5610 277.60 40.9933 391.69 30.0359 620. 36 18.1867 278.00 34.1739 264.66 28.5512 621.93 11. 4956 279.20 51.3199 401.81 23.5316 630.19 0.0000 279.54 36.5059 402.40 21.0195 631.29 17.3240 279.70 39.9336 404.85 29.4786 633.25 15.4141 280.46 38.8207 410.95 43.1392 634.78 0.0000 283.69 30.9221 413.71 23.7298 635.95 14.4702 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 37.8541 423.72 0.0000 645,.85 18.4178 285.90 0.0000 427.09 33.3585 657.76 19.0120 287.50 26.4344 427.87 32.5202 657.90 0.0000 290.67 18.4429 433.94 18 .. 0456 661. 66 18.5593 293.27 0.0000 439.40 26.7359 664.57 0.0000 351. 93 38.5824 453.88 21. 7 667 666.33 0.0000 295.96 38.6078 463.37 14. 0160 666.50 0.0000 879.38 25.5416 468.0:J 14.0576 667.71 0.0000 299.98 34.0984 473.00 0.0000 677.62 13.7790 300.09 34 .1011 475.06 25.5921 685.70 0.0000 300.13 34.1029 476.78 33.5701 695.00 0.0000 301.36 34.1405 477.60 26.5161 696.49 10.4252 302.85 29.5236 482.18 16.8415 696.51 10.4252 256.23 32.6792 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 o.ooob 697.30 11. 9189 306.78 32.7450 497.08 19.6783 697.49 11. 9199 308.46 43.3345 505.52 22.9247 702.65 16.9260 311. 90 32.8920 507.63 0.0000 706.68 16.4584 316.51 41. 2794 511.00 19.8422 711. 68 17.9956 319.41 0.0000 514.00 20.3293 720.70 0.0000 320.08 0.0000 514.00 20.3293 721. 93 0.0000 321.04 27. 2311 520.40 17.2311 722.78 12.0566 323.87 31. 6479 520.69 0.0000 722.91 12.0571 325.23 23.7634 522.65 0.0000 723.31 13.5670 328.76 0.0000 527.90 0.0000 724.19 15.0800 333.37 22.3302 528.26 13.6652 727. 33 16.1081 333.97 41.4904 529.59 22.7926 733.00 0.0000 334.37 39.9078 529.87 0.0000 735.93 15.1587 338.28 33.6302 531. 02 0.0000 333.97 9 .1011 338.32 33. 6311 537.26 0.0000 739.50 0.0000 311. 90 32.0858 546.56. 0.0000 747.24 13.7098 340.48 32.0858 552.55 24.9368 748.06 13. 7148 340.55 0.0000 563.25 17.6509 752.31 20.3556 344.28 26.5527 569.33 24.2343 753.82 0.0000 345.93 22.9620 946.00 24.2364 756.73 22.9431 351.06 33.9772 569.70 19.5773 756.80 22.9440 351. 93 34. 0011 583.19 19.7191 884.68 15.3430 Page 2991 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 19. 9610 1274.44 14.5224 1620.50 4.9722 766.42 19. 9666 1001.03 12.3083 1621. 92 4.9738 766.84 16.8975 1002.74 14.5546 1678.03 0.0000 772.60 0.0000 1004.73 13.4438 1690.97 2.0200 776.52 0.0000 507.63 0.0000 1750.46 0.0000* 739.50 0.0000 1025.87 0.0000 1764.49 1. 6415 778.90 11.3227 1028.54 0.0000 1063.66 5.1361 783.70 0.0000 1037.84 9.0625 1771. 35 3.0822 785.37 10.3210 1038.76 0.0000 1791.20 0.0000 792.07 13.9719 631. 29 7.9525 1808.65 . 1. 0354 794.95 10.3617 1048.07 0.0000 1810.72 0.0000 795.86 10.3658 1049.04 9.0957 1836.06 1. 0411 810.06 4.6917 1050.41 20.4741 810.29 4.6921 1063.66 5.7117 344.28 4.6924 1077.00 0.0000 810.76 7.8217 1077.34 12.6212 815.77 0.0000 1085.87 14.9561 1048.07 0.0000 1093.63 17.2998 832.01 18.9324 1099.45 25. 4196 834.85 16.8477 1112. 07 8.1200 835.71 13.6935 1112.84 6. 9614 836.80 0.0000 1115.54 8.7091 846.75 0.0000 1120.29 13.9551 846.77 14.8106 1120.55 13.9561 856.80 0.0000 1221.41 13.9590 860.56 12.7632 1129. 67 12.8289 871.09 13.8823 1131. 51 0.0000 873.19 13.8934 1147.95 0.0000 875.33 0.0000 1173.23 15.0670 879.38 13.9262 1177.95 5.9167 880.51 7.5019 1189.05 11.1941 883.24 9.6552 1204.77 13.4180 884.68 15.0277 1221. 41 3.5952 889.28 11. 827 6 1231. 02 12.9788 894.76 10.7743 1235.36 0.0000 898.04 14.0241 1238.28 19.8690 900.72 12.9580 1260.41 0.0000 903:28 16.2128 1271. 87 10.0285 911.20 14.0923 1274.44 5.4741 912.08 14.6393 1274.54 4.5618 923.98 0.0000 1291.59 8.2502 926.50 9.8108 1298.22 0.0000 929 .11 10. 9111 1312 .11 0.0000 937.49 15.3216 1332.49 7.4146 944.13 0.0000 1362.66 0.0000 946.00 14.2706 1365.19 12.1534 949.00 17.5827 1368.63 0.0000 667. 71 0.0000 1384.29 6.5766 962. 31 19.8735 1408.01 4.7260 964.08 11. 6002 1457.56 0.0000 966: 17 6.6335 1460.82 5.7466 911.20 13.2798 1489.16 1. 9288 968. 97 13.2798 1505.03 5.8088 983.53 0.0000 1584.12 5.9176 984.45 0.0000 1596.21 0.0000 Page 2992 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:04:17.52 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration .DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM19.CNF;561 Background date : Z-OCT-2016 11:01:07. Sample date 10-DEC-2015 13:15:00 Acquisition date : 3-0CT-2016 08:02:09. Sample ID G405235005 Sample quantity : 1.57331E+02 GRAM Detector name GAM19 Detector geometry: CAN Elapsed' live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.81 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 6 6 5 5 5 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 8 Page 2993 of 5809 Energy 53.91 63.56** 74.83* 77.19* 87.35 90.10 92.75* 185.62* 208.99 238.58* 241.88 270.49 295.09* 300.17. 326.32 338.70 351.79* 463.18 471.99 489.26* 510.87* 561.21 569. 64* 583.12* 609.18* 614.42* 661. 60 665.45 727.26 757.10 763.15* 829.83 911. 02* 948.19 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 3 51 157 221 75 32 100 135 26 364 93 60 166 36 74 125 246 66 13 23 45 18 16 127 186 14 55 25 38 22 17 21 97 16 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 179 190 150 118 256 170 195 164 120 91 111 73 85 70 98 56 84 55 45 17 72 34 24 33 32 30 18 19 35 22 8 7 23 4 1. 51 0.74 1.16 1. 06 1. 56 1. 21 1. 73 1. 38 1. 26 1.14 1. 70 1. 20 1.18 1. 09 5.86 1. 70 1. 35 2.43 0.86 4.22 2.01 1. 39 1.19 1. 57 1. 59 0.83 1. 50 2.40 1. 59 2.86 1. 09 1. 22 2.05 3.21 108.59 127.90 150.45 155.17 175.52 181.00 186.31 372 .14 418.88 478.09 484.71 541. 9'4 591.15 601.33 653. 64 678.41 704.61 927.47 945.12 979.67 1022.91 1123.63 1140.49 1167.46 1219.62 1230.09 1324.50 1332.20 1455.87 1515.57 1527.69 1661.10 1823.55 1897.92 102 123 145 145 170 170 170 365 416 472 472 538 584 598 643 672 698 918 940 974 1014 1118 1136 1161 1213 1226 1320 1329 1448 1509 1523 1656 1817 1894 10 7.37E-04956.6 10 1.43E-02 53.2 17 4.35E-02 15.5 1.19E+OO 17 6.15E-02 10.6 23 2.08E-02 37.1 3.61E+OO 23 9.0lE-03 68.7 23 2.77E-02 31.3 14 3.74E-02 22.4 8 7.22E-03 75.6 18 l.OlE-01 6.9 1.84E+OO 18 2.58E-02 25.2 9 1.68E-02 28.7 13 4.60E-02 14.1 9 9.93E-03 44.9 18 2.07E-02 33.4 15 3.48E-02 15.8 12 6.83E-02 9.9 18 1.83E-02 29.7 10 3.61E-03100.4 11 6. 41E-03 42 .. 2 18 1.26E-02 51.6 11 5.12E-03 64.8 11 4.35E-03 98.9 12 3.52E-02 12.9 13 5.17E-02 9.9 9 3.94E-03 76.8 9 1.54E-02 19.2 9 6.99E-03 36.5 13 1.06E-02 37.0 14 6.24E-03 48.3 8 4.78E-03 38.6 10 5.75E-03 33.0 15 2.68E-02 15.1 15 4.33E-03 32.2 1.63E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 8 951.23 17 9 1. 93 1904.00 1894 15 4.66E-03 38.1 36 2 962. 21 16 2 1. 73 1925.97 1923 12 4.46E-03 33.6 7. 21E-01 37 2 964. 22 26 12 1. 94 1930.00 1923 12 7.24E-03 32.8 38 0 969. 02 58 20 2.28 1939.60 1934 13 l.60E-02 20.6 39 0 1024.33 4 10 0.47 2050.27 2044 8 l.OlE-03160.1 40 0 1120.64 48 12 1.23 2242.97 2236 12 l.33E-02 20.5 41 0 1130.03 22 10 4.80 2261. 75 2253 16 6.00E-03 41. 4 42 0 1197. 83 28 41 8.79 2397.43 2382 28 7.64E-03 69.3 43 5 1212.75 10 3 1. 49 2427.27 2426 11 2.65E-03 32.6 2.29E+OO 44 5 1215.68 17 5 1. 82 2433.14 2426 11 4. 61E-03 30.9 45 0 1376.89 17 6 4.26 2755.69 2749 13 4.79E-03 38.5 46 0 1460.49 391 4 1. 98 2922.98 2916 15 l.09E-01 5.2 47 0 1694.43 7 3 1. 47 3391. 07 3384 10 2.00E-03 56.0 48 0 1764.28* 43 0 2.21 3530.83 3523 15 1.19E-02 16.1 Flag: "*" = Peak area was modified by background subtraction Page 2994 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:04:21 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 13:15:00 G405235005 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:02:09 157.33 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA19 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 2995 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.81 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff . pCi/GRAM pCi7GRAM %Error Status K-40 . 1460.82 10.66* 1.161E+OO l.461E+Ol 1.461E+Ol 10.35 OK AS-73 53.44 10.30* 2.017E+OO 8.281E-02 l.083E+001913.23 OK CD-109 88.03 3.70* 5.494E+OO 1.200E+OO l.876E+OO 143.99 . OK SN-126" 64.28 9.60 3.338E+OO l.024E+OO 1.024E+OO 106.41 OK 86.94 8.90 5.494E+OO 4.987E-01 4.987E-01 143.99 OK 87.57 37.00* 5.494E+OO l.200E-01 l.200E-01 143.99 OK BA-137M 661. 66 89.90* 2.164E+OO l.444E-01 1.471E-01 38.46 OK CS-137 661.66 85.10* 2.164E+OO 1.526E-01 1.554E-01 38.46 OK TL-208 277.37 6.60 4.415E+OO Line Not Found Absent 583.19 85.00* 2.392E+OO 3.206E-01 3.206E-01 25.76 OK 860.56 12.50 1. 763E+00 Line Not Found Absent PB-212 74.82 10.28 4.545E+OO 1.445E+OO 1.445E+OO 47.20 OK 77 .11 17.10 4.754E+OO 1. 710E+OO 1.710E+OO 21.10 OK 238.63 43.60* 4.960E+OO 9.499E-01 9.499E-01 13.81 OK 300.09 3.30 4.141E+OO 1.443E+OO 1.443E+OO 89.83 OK BI-214 609.32 45.49* 2.310E+OO 9.063E-01 9.066E-01 19.71 OK 1120.29 14.92 l.437E+00 l.064E+00 *1. 065E+OO 41. 00 OK 1764.49 15.30 9.862E-01 l.282E+00 . 1. 282E+OO 32.20 OK PB-214 74.82 5.80 4.544E+OO 'Line Not Found <<INT Reject 77 .11 9.70 4.754E+OO 3.015E+OO 3.016E+OO 21.10 OK 87.09 3.41 5.478E+OO Line Not Found <<INT Reject 242.00 7.25 4.908E+OO Line Not Found <<INT Reject 295.22 18.42 4.199E+00 1.183E+OO 1.183E+OO 28.12 OK 351. 93 35.60* 3.630E+OO 1.032E+OO 1.033E+OO 19.83 OK RN-222 609.32 45.49* 2.310E+OO 9.063E-01 9.066E-01 19.71 OK 1120.29 14.92 1.437E+OO 1.064E+OO 1.065E+OO 41. 00 OK 1764.49 15.30 9.862E-01 l.282E+OO 1.282E+00 32.20 OK RA-224 240.99 4.10* 4.910E+OO 5.045E-01 5.045E-01 284.33 OK RA-226 609.32 45.49* 2.310E+OO 9.063E-01 9.066E-01 19. 71 OK 1120. 29 14.92 1.437E+OO l.064E+OO l.065E+00 41. 00 OK 1764.49 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 OK AC-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.747E+OO 1.616E+OO L 616E+OO 31.60 OK 794.95 4.25 1.875E+OO Line Not Found Absent 835.71 1. 61 1.803E+OO -----Line Not Found Absent 911.20 25.80* 1.687E+OO 1.084E+OO 1. 084E+OO 30.29 OK 968. 97 15.80 *l.609E+OO 1.098E+OO 1.098E+OO 41. 21 OK RA-228 105.21 1.10 6.259E+OO Line Not'Found Absent 338.32 11. 27 3.747E+OO 1.616E+OO 1.616E+OO 31. 60 OK 794.95 4.25 l.875E+00 Line Not Found Absent 835.71 1. 61 1.803E+OO Line Not Found Absent 911.20 25.80* 1.687E+OO 1.084E+OO 1.084E+OO 30.29 OK 968.97 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41. 21 OK TH-228 74.82 10.28 4.545E+OO 1.445E+OO l.445E+00 47.20 OK 77 .11 17.10 4.754E+OO 1. 710E+OO 1. 710E+OO 21.10 OK 238.63 43.60* 4. 960E+OO 9.499E-01 9.499E-01 13.81 OK 300.09 3.30 4 .141E+OO 1.443E+OO 1.443E+OO 89.83 OK TH-230 609.32 45.49* 2.310E+OO 9.063E-01 9.063E-01 19. 71 OK 1120.29 14.92 l.437E+OO 1. 064E+OO 1.064E+OO 41.00 OK Page 2996 of 5809 Nuclide Line Activity Report (continued) Page 3 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff, pCi/GRAM pCi7GRAM %Error Status 1764.49 15.30 9.862E-01 1.282E+OO 1. 282E+OO 32.20 OK PA-231 283.69 1. 70 4.336E1-00 Line Not Found Absent 301.36 5.35* 4.141E+OO 8.901E-01 8. 901E-01 89.83 OK TH-232 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 *3.747E+OO 1.616E+OO 1.616E+OO 31. 60 OK 835.71 1. 61 l.803E+OO Line Not Found Absent 911. 20 25.80* l.687E+OO 1.084E+OO 1.084E+OO 30.29 OK 968. 97 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41. 21 OK TH-234 63.29 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 OK 92.59 4.23 5.791E+OO 2.516E+OO 2.516E+OO 62.65 OK U-234 609.32 45.49* 2.310E+OO 9.063E-01 9.063E-01 19.71 OK 1120.29 14.92 1.437E+OO 1.064E+OO 1.064E+OO 41: 00 OK 1764.49 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 OK U-235 89. 96 3.47 5.653E+OO 1.024E+OO 1.024E+OO 137.50 OK 93.35 5.60 5. 7191E+OO 1.900E+OO 1.900E+OO 62.65 OK 143.76 10.96* 6:462E+OO Line Not Found Absent 163.33 5.08 .6. 216E+OO Line Not Found Absent 185.72 57.20 5.848E+OO 2.332E-01 2.332E-01 44.76 OK 205.31 5.01 5.506E+OO Line Not Found Absent U-238 63.29 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 OK 92.59 4.23 5.791E+OO 2.516E+OO 2.516E+OO 62. 65 OK AM-243 43.53 5.90 5.190E-01 Line Not Found Absent 74.66 67.20* 4.545E+OO 2. 211E-01 2. 211E-01 47.20 OK ANH-5ll 511. 00 100.00* 2.662E+OO 8.853E-02 8.853E-02 103.14 OK Flag: "*" = Keyline -----...__ / Page 2997 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:04:23.25

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l * *Acquisition date 3-0CT-2016 08:02:09 Sensitivity : 3.000 *
Detector ID GAM19 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.81 Half life ratio : ***** *
Sample date 10-DEC-2015 13:15:00 Analyst initials: MXRl *
Sample ID G405235005 Sample Quantity 1.5733E+02 GRAM *
Batch Number 1596247 Wet Weight .. 0. 00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
Eff. File : DKA100': [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM K-40 1.461E+Ol 1.481E+OO 6. 721E-01 AS-73 1.083E+OO 2.030E+Ol 1.538E+Ol CD-109 1. 876E+OO 2.648E+OO 2.107E+OO SN-126 1.200E-01 1.693E-01
1. 354E-01 BA-137M 1.471E-01 5.546E-02 5.420E-02 CS-137 1.554E-01 5.858E-02 5.726E-02 TL-208 3.206E-01 8.095E-02 5.774E-02 PB-212 9.499E-01 l.285E-01 9.481E-02 BI-214 9.066E-01 1. 751E-01 l.201E-01 PB-214 1.033E+OO 2.006E-01 1.353E-01 RN-222 9.066E-01 1. 751E-01 1. 201E-Oi RA-224 5.045E-01 1.406E+OO 1.016E+OO RA-226 9.066E-01 1. 751E-01 l.201E-01 AC-228 1.084E+OO 3.219E-01 2.582E-01 RA-228 1.084E+OO 3.219E-01 2.582E-01 TH-228 9.499E-01 l.285E-01 9.481E-02 TH-230 9.063E-01 1. 751E-01 1.201E-01 PA-231 8. 901E-01 7.835E-01 8.240E-01 TH-232 1.084E+OO 3.219E-01 2.582E-01 TH-234 2.657E+OO 2.771E+OO 2.013E+OO U-234 9.063E-01 l.751E-01 1. 201E-01 U-235 -4.374E-02 1.754E-01 3.346E-01 U-238 2.771E+OO 2.013E+OO AM-243 2. 211E-01 1.023E-01 9.013E-02 , ANH-511 8.853E-02 8.948E-02 5.654E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 1. 076E+Ol 1.249E+Ol 2.588E+Ol NOT IDENT. NA-22 4. 948E-03 . 4.450E-02 8.902E-02 NOT IDENT. NA-24 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -3.904E-03 2.083E-02 4.619E-02 FAIL ABUN SC-46 1.237E-01 3.257E-01 6.951E-01 FAIL ABUN Page 2998 of 5809 V-48 O.OOOE+OO 1. 287E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 4.153E+02 0.000E+OO SHORT HLIF MN-54 -8.393E-03 7. 391E-02 1.255E-01 NOT IDENT. C0-56 -1.813E-01 4.386E-01 8.220E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 2.889E-02. 4.520E-02 9.408E-02 NOT IDENT. C0-58 -3.563E-01 5.850E-01 1.064E+OO NOT IDENT. FE-59 -4.730E-02 5*. 995E+OO 1.186E+Ol NOT IDENT. C0-60 1. 4,29E-03 3.289E-02 6.726E-02 NOT IDENT. ZN-65 2.099E-02 l.873E-01 3,293E-Ol NOT IDENT. GE-68 -7. 8'59E-01 l.695E+OO 3.141E+OO NOT IDENT. AS-74 O.OOOE+OO 5.432E+03 O.OOOE+OO SHORT HLIF SE-75 -2.272E-02 2.061E-01 3.943E-01 NOT IDENT. BR-77 O.OOOE+OO l.273E+37 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 6. 671E+02 O.OOOE+OO SHORT HLIF RB-83 -3.352E-01 7.244E-01 l.278E+OO NOT IDENT. KR-85 -2.354E+OO 8.780E+OO 1. 394E+Ol NOT IDENT. SR-85 -2.437E-01 9.080E-01 1.441E+OO NOT IDENT. RB-86 O.OOOE+OO 1. 979E+04 O.OOOE+OO SHORT HLIF Y-88 1. 07 5E-01 1.516E-01 *4.219E-01 NOT IDENT. Y-91 1.331E+02 5. 8 63E+02 1.042E+03 NOT IDENT. NB-94 4.733E-03 3.297E-02 6.606E-02 NOT IDENT. NB-95 l.607E-01 9. 452E-01 . 1.689E+OO NOT IDENT. NB-95M -9.658E-01 2.638E+OO 4.397E+OO NOT IDENT.
ZR-95 2.661E+OO 2.518E+OO 3.235E+00 FAIL ABUN NB-97 O.OOOE+OO 8.289E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.667E+40 O.OOOE+OO SHORT HLIF M0-99 0. O.OOE+OO 1.064E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.643E+41 O.OOOE+OO SHORT HLIF RH-101 2.392E-02 3.357E-02 6. 960E-02 FAIL ABUN RH-102 -l.925E-02 6.311E-02 1.125E-01 NOT IDENT. RU-103 -2.171E+OO 5.207E+00 9.347E+OO FAIL ABUN RH-106 -7.927E-02 5.362E-01 9.786E-01 NOT IDENT. RU-106 -7.927E-02 5.362E-01 9.786E-01 NOT IDENT. AG-108M -7.699E-04 3.053E-02 5.740E-02 FAIL ABUN AG-llOM 2.930E-02 9.489E-02 1.976E-01 FAIL ABUN SN-113 -9.900E-02 2.233E-01 4.050E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 782E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 8.822E+04 O.OOOE+OO SHORT HLIF TE-123M -4.327E-02 l.294E-01 2.495E-01 NOT IDENT. SB-124 l.082E-01 1.674E+OO 3.422E+OO NOT IDENT. SB-125 -l.718E-02 1. 041E-01 1.941E-01 FAIL ABUN TE-125M . -2. 351E+02 2.895E+02 4.908E+02 NOT IDENT. I-126 O.OOOE+OO 1.105E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 2 63E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.380E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.066E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.699E+26 0. OOOE+OO SHORT HLIF BA-133 3.556E-02 4.089E-02 7.893E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.287E-02 5.612E-02 l.184E-01 FAIL ABUN CS-135 7.152E-02 l.535E-01 2.784E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.387E+05 O.OOOE+OO SHORT HLIF CE-139 -7.430E-02 1. 067E-01 2.002E-01 NOT IDENT. BA-140 O.OOOE+OO l.271E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.458E+05 O.OOOE+OO SHORT HLIF CE-141 4.671E+OO 2.202E+Ol 4.422E+Ol NOT IDENT. CE-143 O.OOOE+OO 6.428E+40 O.OOOE+OO SHORT HLIF CE-144 -2.000E-01 3.390E-01 6.502E-01 NOT IDENT. PM-144 -5.629E-02 5.442E-02 9.538E-02 NOT IDENT. PR-144 -4.870E+OO 4.724E+00 8.285E+OO NOT IDENT. PM-146 -4.808E-02 4.381E-02 7.142E-02 NOT IDENT. ND-147 0.000E+OO 3.376E+07 O.OOOE+OO SHORT HLIF PM-147 -1.015E+02 7.754E+02 l.543E+03 NOT IDENT. PM-149 0.000E+OO 2.610E+40 O.OOOE+OO SHORT HLIF EU-150 -8.023E-03 2.560E-02 4.216E-02 FAIL ABUN EU-152 2.626E-03 8.486E-02 l ."484E-01 FAIL ABUN GD-153 -4.lOlE-02 1. 947E-01 3.238E-01 NOT IDENT. EU-154 9.896E-03 1.088E-01 2.170E-01 FAIL ABUN EU-155 -1.051E-02 l.152E-01 2.083E-01 FAIL ABUN TB-160 5.362E-01 1.681E+OO 3.524E+OO FAIL ABUN H0-166M -5 .176E-02 5.397E-02 9.423E-02 FAIL ABUN TM-171 l.322E+Ol 2.074E+Ol 4.122E+Ol NOT IDENT. HF-172 -l.790E-01 2.219E-01 4. 211E-01 FAIL ABUN LU-172 -1. 38 6E-02 7.778E-02 1. 478E-01 FAIL ABUN LU-176 l.804E-02 2.493E-02 5.073E-02 FAIL ABUN Page 2999 of 5809 HF-181 -1. 929E+OO 4.398E+OO 7.850E+OO NOT IDENT. TA-182 -5.309E-01 1. 051E+OO 1. 775E+OO FAIL ABUN RE-183 9.693E-01 *2.792E+OO 5.408E+OO 'NOT IDENT. RE-184 -9.237E+OO 2.423E+Ol 4.590E+Ol NOT IDENT. W-188 -7.491E+Ol 1.312E+02 2.094E+02 FAIL ABUN IR-192 2.868E-01 4.517E-01 9.166E-01 FAIL ABUN HG-203 -5.437E-01 2.322E+OO 4.376E+OO NOT IDENT. BI-207 -7.770E-02 9.420E-02 2.223E-01 FAIL ABUN PB-210 -9.949E-02 3.206E+OO 6.122E+OO NOT IDENT. BI-211 O.OOOE+OO 5.526E-01 8.424E-01 FAIL ABUN PB-211 5.173E-01 6. 65*9E-01 1.367E+OO NOT IDENT. BI-212 O.OOOE+OO 1.037E+OO 1.307E+OO FAIL ABUN RN-219 2.706E-02 3.912E-01 7.474E-01 FAIL ABUN RA-223 2.309E-01 6.365E-01 1. 249E+OO FAIL ABUN AC-227 -5.213E-04 2.273E-01 4.389E-01 FAIL ABUN TH-227 -5.213E-04 2. 273E-0.1 4.389E-01 FAIL ABUN TH-229 4.061E-02 4.873E-01 9.525E-01 FAIL ABUN TH-231 2.309E-01 6.365E-01 1.249E+OO FAIL ABUN PA-233 4.542E-02 6.106E-02 1.244E-01 FAIL ABUN PA-234 -2.884E-02 2.437E-01 4.246E-01 FAIL ABUN PA-234M 6. 096E-01 4.818E+OO 9.595E+OO NOT IDENT. NP-237 4.542E-02 6.106E-02 1.244E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -2.650E-02 2.318E-01 4.623E-01 NOT IDENT. PU-239 2.374E+02 3.222E+02 6.651E+02 NOT IDENT. AM-241 9.053E-02 1.381E-01 2.545E-01 NOT IDENT. CM-243 -8.033E-02 1. 089E-01 1. 866E-01 NOT IDENT. BK-247 -3.373E-02 7.300E-02 1.354E-01 NOT IDENT. CM-247 2.414E-04 3.662E-02 6.939E-02 NOT IDENT. CF-249 -1.809E-02
3. 760E-02 6.786E-02 NOT IDENT. CF-251 -4.791E-03 l .119E-01 2.190E-01 NOT IDENT. Page 3000 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:04:19.07 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 379 10.66* 1.161E+OO 1.461E+Ol 1. 461E+Ol 10.35 AS-73 53.44 4 10.30* 2.017E+OO 8.281E-02 1.083E+OO 1913. 23 CD-109 88.03 98 3.70* 5.494E+OO 2.290E+OO 3.582E+OO 74.24 SN-126 64.28 69 9.60 3.338E+OO 1.024E+OO 1.024E+OO 106.41 86.94 98 8.90 5.494E+OO 9.519E-01 9.519E-01 74.24 87.57 98 37.00* 5.494E+OO 2.290E-01 2.290E-01 74.24 BA-137M 661. 66 59 89.90* 2.164E+OO 1.444E-01 1.471E-01 38.46 CS-137 661. 66 59 85.10* 2.164E+OO 1. 526E-01 1.554E-01 38.46 TL-208 277.37 ------6.60 4.415E+OO ------Line Not Found ------583.19 137 85.00* 2.392E+OO 3.206E-01 3.206E-01 25.76 860.56 ------12.50 1.763E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 4.361E+OO ------Line Not Found ------351.06 280 12.92* 3.630E+OO 2.844E+OO 2.844E+OO 19.83 PB-212 74.82 207 10.28 4.545E+00 2 .113E+OO 2 .113E+OO 31. 05 77 .11 291 17.10 4.754E+OO 1. 710E+OO 1. 710E+OO 21.10 238.63 431 43.60* , 4. 960E+OO 9.499E-01 9.499E-01 13.81 300.09 41 3.30 4.141E+OO 1.443E+OO 1.443E+OO 89.83 , BI-214 609.32 200 .45. 49* 2.310E+OO 9.063E-01 9.066E-01 19.71 1120.29 48 14.92 1.437E+OO 1.064E+OO 1.065E+OO 41. 00 1764.49 41 15.30 9.862E-01 1. 282E+OO 1.282E+OO 32.20 PB-214 74.82 207 5.80 4.545E+OO 3.745E+OO 3.746E+OO 31. 05 77 .11 291 9.70 4.754E+OO 3.015E+00 3.016E+OO 21.10 87.09 98 3.41 5.494E+OO 2.485E+OO 2.485E+OO 74.24 242.00 110 7.25 4.910E+OO 1.468E+OO 1. 469E+OO 50.39 295.22 192 18.42 4.199E+OO l.183E+OO 1.183E+OO 28.12 351. 93 280 35.60* 3.630E+OO 1.032E+OO 1.033E+OO 19.83 RN-222 609.32 200 45.49* 2.310E+OO 9.063E-01 9.066E-01 19.71 1120.29 48 14.92 1.437E+OO l.064E+OO 1.065E+OO 41. 00 1764.49 41 15.30 9.862E-01 l.282E+OO 1.282E+OO 32.20 RA-224 240.99 110 4.10* 4.910E+OO 2.596E+OO 2.596E+00 50.39 RA-226 609.32 200 45.49* 2.310E+OO 9.063E-01 9.066E-01 19.71 1120. 29 48 14.92 l.437E+OO l.064E+OO l.065E+00 41. 00 1764.49 41 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 AC-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 143 11. 27 3.747E+00 1.616E+OO 1.616E+OO 31. 60 794.95 ------4.25 1. 875E+OO ------Line Not Found ------835.71 ------1. 61 1.803E+OO ------Line Not Found ------911. 20 99 25.80* 1.687E+OO 1.084E+OO 1.084E+OO 30.29 968. 97 59 15.80 1.609E+OO 1.098E+OO l.098E+OO 41. 21 RA-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 143 11. 27 3.747E+OO l.616E+OO 1.616E+OO 31. 60 7 94 .. 95 ------4.25 1. 875E+OO ------Line Not Found ------835. 71 ------1. 61 l.803E+OO ------Line Not Found ------911. 20 99 25.80* 1.687E+OO l.084E+OO 1.084E+OO 30.29 968.97 59 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41. 21 TH-228 74.82 207 10.28 4.545E+OO 2 .113E+OO 2 .113E+OO 31. 05 77 .11 291 17 .10' 4.754E+OO 1.710E+OO 1.710E+OO 21.10 Page 3001of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 431 43.60* 4. 960E+OO 9.499E-01 9.499E-01 13. 81 300.09 41 3.30 4.141E+OO 1.443E+OO l.443E+OO 89.83 TH-230 609.32 200 45.49* 2.310E+OO 9.063E-01 9.063E-01 19.71 1120.29 48 14.92 1.437E+OO 1.064E+OO 1.064E+OO 41. 00 1764.49 41 15.30 9.862E-01 1.282E+OO l.282E+OO 32.20 PA-231 283.69 ------1. 70 . 4.336E+OO ------Line Not Found ------301.36 41 5.35* 4.141E+OO 8.901E-01 8. 901E-01 89.83 TH-232 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 143 11. 27 3.747E+OO 1.616E+OO 1.616E+OO 31. 60 835.71 ------1. 61 1. 803E+OO ------Line Not Found ------911. 20 99 25.80* l.687E+00 1.084E+OO 1.084E+OO 30.29 968. 97 59 15.80 1. 609E+OO 1.098E+OO 1.098E+00 41. 21 TH-234 63.29 69 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 92.59 129 4.23 5. 7 91E+OO 2.516E+OO 2.516E+OO 62. 65 U-234 609.32 200 45.49* 2.310E+OO 9.063E-01 9.063E-01 19.71 1120.29 48 14.92 1.437E+OO 1.064E+OO l.064E+00 41.00 1764.49 41 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 U-235 89. 96 42 3.47 5.653E+OO 1.024E+OO 1.024E+OO 137.50 93.35 129 5.60 5'. 791E+OO 1.900E+OO 1.900E+OO 62. 65 143.76 ------10. 96* 6.462E+OO ------Line Not Found ------163.33 ------5.08 6.216E+00 ------Line Not Found ------185.72 163 57.20 5.848E+OO 2.332E-01 2.332E-01 44.76 205.31 ------5.01 5.506E+OO ------Line Not Found ------U-238 63.29 69 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 92.59 129 4.23 5. 791E+OO 2.516E+OO 2.516E+OO 62. 65 AM-243 43.53 ------5.90 5.190E-01 ------Line Not Found ------74.66 207 67.20* 4.545E+OO 3.232E-01 3.232E-01 31. 05 ANH-511 511. 00 49 100.00* 2.662E+OO 8.853E-02 8.853E-02 103.14 Flag: "*" Key line Page 3002 of 5809 Sununary of Nuclide Activity Sample ID : G405235005 Acquisition date Page : 3 3-0CT-2016 08:02.:09 Total number of lines in spectrum 48 Number of unidentified lines 11 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 AS-73 cb-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 80.30D 461.4.0D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+l0Y L 41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47Et09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 13.1 1. 56 1. 00 1. 02 1. 02 1. 00 1. 08 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.461E+Ol 8.281E-02 2.290E+OO 2.290E-01 1.444E-01 1. 526E-01 3.206E-01 2.844E+OO 9.499E-01 9. 063E-01 1.032E+OO 9.063E-01 2. 596E+OO 9.063E-01 1. 084E+OO 1.084E+OO 9.499E-01 9.063E-01 8.901E-01 1. 084E+OO 2.657E+00 9.063E-01 2.332E-01 2.657E+OO 3.232E-01 8.853E-02 4.083E+Ol 4.083E+Ol Decay Corr pCi7GRAM l.461E+Ol 1.083E+OO 3.582E+OO 2.290E-01 1.471E-01 l.554E-01 3.206E-01 2.844E+OO 9.499E-01 9.066E-01 1.033E+OO 9.066E-01 2. 596E+OO 9.066E-01 l.084E+00 1.084E+OO 9.499E-01 9.063E-01 8.901E-01 1.084E+OO 2.657E+OO 9.063E-01 2.332E-01 2.657E+OO 3.232E-01 8.853E-02 4. 313E+Ol 4.313E+Ol 77.08% Decay Corr 2-Sigma Error 0.151E+Ol 20.71E+OO 2.659E+OO l.700E-01 0.566E-01 0.598E-01 0.826E-01 0.564E+OO 1. 311E-01 1. 787E-01 0.205E+OO 1. 787E-01 1.308E+00 l.787E-01 0.328E+00 0.328E+OO 1. 311E-01 1.787E-01 7.995E-01 0.328E+OO 2.827E+OO l.787E-01 1.044E-01 2.827E+OO l.004E-01 9 .131E-02 "M" Manually accepted 2-Sigma %Error 10.35 1913.23 74.24 74.24 38.46 38.46 25.76 19.83 13. 81 19. 71 19.83 19. 71 50.39 19.71 30.29 30.29 13.81 19. 71 89.83 30.29 106.41 19.71 44.76 106.41 31. 05 103.14 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3003 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235005 Acquisition date : 3-0CT-2016 08:02:09 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 208.99 31 144 1.26 418.88 416 8 7.22E-03 **** 5.44E+OO 0 270.49 71 85 1.20 541. 94 538 9 l.68E-02 57.3 4.50E+OO T 0 326.32 85 112 5.86 653.64 643 18 2.07E-02 66.8 3.87E+OO T 0 463.18 73 61 2.43 927: 47 918 18 1. 83E-02 59.4 2.89E+OO T 0 471. 99 14 50 0.86 945.12 940 10 3.61E-03 **** 2.84E+OO T 0 489.26 25 18 4.22 979.67 974 11 6.41E-03 84.3 2.76E+OO 0 561.21 20 36 1. 39 1123. 63 1118 11 5.12E-03 **** 2.47E+OO 0 569.64 17 26 1.19 1140.49 1136 11 4.35E-03 **** 2.44E+OO T 0 614.42 15 32 0.83 1230.09 1226 9 3.94E-03 **** 2.29E+OO T 0 665.45 27 20 2.40 1332.20 1329 9 6.99E-03 73.1 2.15E+OO T 0 727.26 40 37 1. 59 1455.87 1448 13 1. 06E-02 74.0 2.0lE+OO T 0 757.10 23 23 2.86 1515.57 1509 14 6.24E-03 96. 5 1.95E+OO T 0 763.15 18 8 1. 09 1527.69 1523 8 4.78E-03 77.2 1. 93E+OO T 0 829.83 21 8 1. 22 1661.10 1656 10 5.75E-03 66.1 1. 81E+OO 8 948.19 16 4 3.21 1897.92 1894 15 4.33E-03 64.4 1.64E+OO T 8 951. 23 17 9 1. 93 1904.00 1894 15 4.66E-03 76.1 l.63E+OO 2 962. 21 16 2 1. 73 1925.97 1923 12 4.46E-03 67.1 1.62E+OO T 2 964.22 27 12 1. 94 1930.00 1923 12 7.24E-03 65.6 1. 61E+OO T 0 1024.33 4 10 0.47 2050.27 2044 8 l.OlE-03 **** 1. 54E+OO 0 1130. 03 22 10 4.80 2261.75 2253 16 6.00E-03 82.8 1. 43E+OO T 0 1197. 83 27 41 8.79 2397.43 2382 28 7.64E-03 **** l.36E+OO 5 1212.75 9 3 1. 49 2427.27 2426 11 2.65E-03 65.1 1. 35E+OO 5 1215.68 16 4 1. 82 2433.14 2426 11 4. 61E-03 61. 7 1.35E+OO 0 1376.89 17 6 4.26 2755.69 2749 13 4.79E-03 77.0 1. 22E+OO 0 1694.43 7 3 1. 47 3391.07 3384 10 2.00E-03 **** 1.02E+OO Flags: "T" = Tentatively associated Page 3004 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:04:50.15 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETEcroR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l * *Acquisition date 3-0CT-2016 08:02:09 Sensitivity : 3.000 *
Detector ID GAM19 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.81 Half life ratio : ***** * *.Sample date 10-DEC-2015 13:15:00 Nuclide Library : SOLID *
Sample ID G405235005 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5733E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. .. 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
Eff, File* : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234. U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.835E-01 7.232E+OO 1.00lE+OO 6.427E-02 2.362E-02 2.495E-02 2.559E-02 4.426E-02 5.372E-02 6.241E-02 5.372E-02 4.744E-01 5.372E-02 1.140E-01 1.140E-01 4.426E-02 5.371E-02 3.814E-01 1.140E-01 9.491E-01 5.371E-02 1. 576E-01 9.491E-01 4.277E-02 2.576E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3005 of 5809 Le (pCi/GRAM l.184E+Ol 3.825E-02 O.OOOE+OO l.636E-02 3.025E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF CR-51 .MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-l26 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 .GD-153 EU-154 EU-i55 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3006 of 5809 O.OOOE+OO 5.568E-02 3.574E-01 O.OOOE+OO 4.439E-02 4.658E-01 5.106E+OO 2.783E-02 1.437E-01 1.276E+OO O.OOOE+OO 1.831E-01 O.OOOE+OO O.OOOE+OO 5.770E-01 6.356E+OO 6.573E-01 O.OOOE+OO l.634E-01 4.578E+02 2.982E-02 7.580E-01 2. 061E+OO 1. 461E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO ,3.296E-02 '5.012E-02 4.155E+OO 4.380E-01 4.380E-01 2.626E-02 8.678E-02 1.837E-01 O.OOOE+OO 0.000E+OO 1.17 4E-01 1. 301E+OO 8.806E-02 2.306E+02 0.000E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 3.628E-02 O.OOOE+OO 5.380E-02 l.299E-01 O.OOOE+OO O.OOOE+OO 9.388E-02 O.OOOE+OO O.OOOE+OO 2.085E+Ol O.OOOE+OO 3.055E-01 4.203E-02 3.651E+OO 3.181E-02 0.000E+OO 7.255E+02 O.OOOE+OO l.919E-02 6.704E.:_02 1.525E-01 9. 313E-02 9.822E-02 l.542E+00 4 .111E-02 l.948E+Ol 1. 97 9E-01 6.430E-02 2.359E-02 3.537E+OO SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT. I DENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT H:µIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN . NOT I DENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3007 of 5809 7.780E-01 2.554E+OO 1.948E+Ol 9.706E+Ol 4.245E-01 2.029E+OO 1.052E-01 2.874E+OO 4.070E-Ol 6.286E-01 6.042E-01 3.424E-01 5.808E-01 2.043E-01 2.043E-01 4.491E-01 5.808E-01 5.784E-02 1.788E-01 4.299E+OO 5.784E-02 0.000E+OO 2.177E-01 3.158E+02 l.203E-01 8.786E-02 6.275E-02 3.181E-02 3.087E-02 1.029E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT TDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:04:58.76 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l *
Acquisition date 3-0CT-2016 08:02:09 Sensitivity : 3.000 *
Detector ID GAM19 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.81 Half life ratio : ***** *
Sample date 10-DEC-2015 13:15:00 Nuclide Library : SOLID *
Sample ID G405235005 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5733E+02 GRAM *
Quantity Err(%) : 1.2712E-03 % ** *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides*" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM . ) ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.461E+Ol 1.667E+OO l.667E+OO AS-73* 1.083E+OO 2.030E+Ol 2.030E+Ol CD-109
1. 876E+OO 2.661E+OO 2.661E+OO SN-126 l.200E-01 1.700E-01 l.700E-01 BA-137M 1.471E-01 5.582E-02 CS-137 1.554E-01 5.897E-02 5.897E-02 TL-208 3.206E-01 8. 211E-02 8. 211E-02 PB-212 9.499E-01 1.381E-01 1. 381E-01 BI-214 9.066E-01 1. 795E-01 l.795E-01 PB-214 1.033E+OO 2.052E-01 2.052E-01 RN-222 9.066E-01 1. 795E-01 1. 7 95E-01 RA-224 5.045E-01 l.413E+00 1. 413E+OO RA-226 9.066E-01 1. 795E-01 l.795E-01 AC-228 1.084E+OO 3.267E-01 3.267E-01 RA-228 1. 084E+OO 3.267E-01 3.267E-01 TH-228 9.499E-01 1.381E-01 1.381E-01 TH-230 9.063E-01 l.794E-01 l.794E-01 PA-231 8. 901E-01 8.062E-01 8.062E-01 TH-232 1.084E+OO 3.267E-01 3.267E-01 TH-234 2.657E+OO 2.833E+OO 2.833E+OO U-234 9.063E-01 1. 794E-01 1.794E-01 U-235 -4.374E-02 1. 754E-01 1. 754E-01 U-238 2.657E+OO 2.833E+OO 2.833E+OO AM-243 2. 211E-01 l.040E-01 1.040E-01 ANH-511 8.853E-02 8.955E-02 8.955E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1.076E+Ol 1.250E+Ol l.341E+Ol NOT IDENT. NA-22 4.948E-03 4.450E-02 4.456E-02 NOT IDENT. NA-24 -1.000E+41 3.245E+41 0.000E+OO SHORT HLIF AL-26 -3.904E-03 2.083E-02 2.090E-02 FAIL ABUN SC-46 l.237E-01 3.258E-01 3.305E-01 FAIL ABUN Page 3008 of 5809 V-48 6.546E+03 1.287E+04 1.321E+04 SHORT HLIF CR-51 -1.643E+02 4.154E+02 4.219E-i-02 SHORT HLIF MN-54 -8.393E-03 7. 391E-02 7.401E-02 NOT IDENT. C0-56 -1. 813E-01 4.387E-01 4.-462E-01 NOT IDENT. MN-56 -l.OOOE+41 2.420E+41 O.OOOE+OO SHORT HLIF C0-57 2.889E-02 4.522E-02 4.705E-02 NOT IDENT. C0-58 -3.563E-01 5.852E-01 6.069E-01 NOT IDENT. FE-59 -4.730E-02 5.995E+OO 5.995E+OO NOT IDENT. C0-60 1.429E-03 3.289E-02 3.289E-02 NOT IDENT. ZN-65 2.099E-02 1.873E-01 1. 875E-01 NOT IDENT. GE-68 -7.859E-01 1.695E+OO 1.732E+OO NOT IDENT. AS-74 -4.299E+02 5.432E+03 5.436E+03 SHORT HLIF SE-75 -2.272E-02 2.062E-01 2.064E-01 NOT IDENT. BR-77 9.409E+37 8.088E+38 O.OOOE+OO SHORT HLIF SR-82 -7.664E+02 6.681E+02 7. 521E+02 SHORT HLIF RB-83 -3.352E-01 7.258E-01 7.414E-01 NOT IDENT. KR-85 -2.354E+OO 8.781E+OO 8.845E+OO NOT IDENT. SR-85 -2.437E-01 9.080E-01 9.147E-01 NOT IDENT. RB-86 -5.544E+03 1. 979E+04 1. 995E+04 SHORT HLIF Y-88 1. 075E-01 l.518E-01 l.593E-01 NOT IDENT. Y-91 1. 331E+02 5.863E+02 5.894E+02 NOT IDENT. NB-94 4.733E-03 3.297E-02 3.304E-02 NOT IDENT. NB-95 1.607E-01 9.452E-01 9.480E-01 NOT IDENT. NB-95M -9.658E-01 2.639E+OO 2.675E+OO NOT IDENT. ZR-95 2.661E+00 2.520E+OO 2.791E+OO FAIL ABUN NB-97 -l.OOO'E+41 8.300E+40 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 7.678E+40 *O.OOOE+OO SHORT HLIF M0-99 -l.402E+31 l.064E+32 0.000E+OO. SHORT HLIF TC-99M 1.000E+41 1. 646E+41 O.OOOE+OO SHORT HLIF RH-101 2.392E-02 3.385E-02 3.552E-02 FAIL ABUN RH-102 -1.925E-02 6.313E-02 6.373E-02 NOT IDENT. RU-103 -2.171E+OO 5.208E+OO 5.299E+OO FAIL ABUN RH-106 -7.927E-02 5.362E-01 5.374E-01 NOT IDENT. RU--:106 -7.927E-02 5. 362E-01 5.374E-01 NOT IDENT. AG-108M -7.699E-04 3.053E-02 3.053E-02 FAIL ABUN AG-110M 2.930E-02 9.490E-02 9.581E-02 FAIL ABUN SN-113 -9.900E-02 2.233E-01 2.277E-01 NOT IDENT. CD-115 6.419E+38 l.785E+39 O.OOOE+OO SHORT HLIF SN-117M -1.'092E+04
8.823E+04 8.836E+04 SHORT HLIF TE-123M -4.327E-02 1.294E-01 1.309E-01 NOT IDENT. SB-124 1.082E-01 1. 674E+OO 1. 675E+OO NOT IDENT. SB-125 -1.718E-02 l.041E-01 l.044E-01 FAIL ABUN TE-125M -2. 351E+02 2.898E+02 3.086E+02 NOT IDENT. I-126 1. 543E+06 1.124E+06 1.322E+06 SHORT HLIF SB-126 -7.978E+04 1.263E+06 l.264E+06 SHORT HLIF SB-127 -4.045E+21 1.487E+22 O.OOOE+OO SHORT HLIF I-131 1.159E+09 4.067E+09 4.100E+09 SHORT HLIF I-132 -1.000E+41 1. 901E+42 O.OOOE+OO SHORT HLIF TE-132 -3.288E+25 2.703E+26 . 0. OOOE+OO SHORT HLIF BA-133 3.556E-02 4.092E-02 4.394E-02 NOT IDENT. I-133 -l.000E+41 4.526E+41 O.OOOE+OO SHORT HLIF CS-134 4.287E-02 5.615E-02 5.938E-02 FAIL ABUN CS-135 7.152E-02 1.535E-01 1.569E-01 NOT IDENT. I-135 . -1.000E+41 1. 2 98E+42 O.OOOE+OO SHORT HLIF CS-136 -7. '556E+04 2.389E+05 2.413E+05 SHORT HLIF CE-139 -7.430E-02 1.077E-01 1.128E-01 NOT IDENT. BA-140 -3.243E+05 1. 271E+06 l.280E+06 SHORT HLIF LA-140 -2.754E+04 4.458E+05 4.459E+05 SHORT HLIF CE-141 4.671E+00 2.202E+Ol 2.212E+Ol NOT IDENT. CE-143 l.000E+41 6.508E+40 O.OOOE+OO SHORT HLIF CE-144 -2.000E-01 3.391E-01 3.509E-01 . NOT IDENT . PM-144 -5.629E-02 5.453E-02 6.014E-02 NOT IDENT. PR-144 -4.870E+OO 4.729E+OO 5.214E+OO NOT IDENT. PM-146 -4.808E-02 4.395E-02 4.900E-02 NOT IDENT. ND-147 7.985E+06 3.376E+07 3.395E+07 SHORT HLIF PM-147 -l.015E+02 7.754E+02 7.768E+02 NOT IDENT. PM-149 -3.334E+39 2. 611E+40 O.OOOE+OO SHORT HLIF EU-150 -8.023E-03 2.560E-02 2.586E-02 FAIL ABUN EU-152 2. 626E-03' 8.486E-02 8.487E-02 FAIL ABUN GD-153 -4.lOlE-02 l.948E-01 1.956E-01 NOT ID.ENT. EU:-154 9.896E-03 l.088E-01 l.089E-01 FAIL ABUN EU-155 -l.051E-02 1.152E-01 l.153E-01 FAIL ABUN TB-160 5.362E-01 1. 681E+OO 1.698E+OO FAIL ABUN H0-166M -5.176E-02 5.404E-02 5.886E-02 FAIL ABUN TM-171 1.322E+Ol 2.077E+Ol 2.161E+Ol NOT IDENT. HF-172 -1. 7 90E-01 2.238E-01 2.379E-01 FAIL ABUN LU-172 -1.386E-02 7.779E-02 7.804E-02 FAIL ABUN LU-176 1.804E-02 2.494E-02 2.623E-02 FAIL ABUN Page 3009 of 5809 HF-181 -1.929E+OO 4.398E+OO 4.484E+OO NOT IDENT. TA-182 ...:5.309E-01 l.051E+OO 1.078E+OO FAIL ABUN RE-183 9.693E-01 2.796E+OO 2.830E+OO NOT IDENT. RE-184 -9.237E+OO 2.433E+Ol 2.469E+Ol NOT IDENT. W-188 -7.491E+Ol 1.314E+02 1.357E+02 FAIL ABUN IR-192 2.868E-01 4.519E-01 4.700E-01 FAIL ABUN HG-203 -5.437E-01 2.322E+OO 2.335E+OO NOT IDENT. BI-207 -7.770E-02 9.425E-02 l.005E-01 FAIL ABUN PB-210 -9.949E-02 3.206E+00 3.206E+00 NOT IDENT. BI-211 2.844E+OO 5.671E-01 l.402E+OO FAIL ABUN PB-211 5.173E-01 6.664E-01 7.060E-01 NOT IDENT. BI-212 l.431E+OO l.040E+OO l.223E+OO FAIL ABUN RN-219 2.706E-02 3.912E-01 3.914E-01 FAIL ABUN RA-223 2.309E-01 6.366E-01 6.451E-01 FAIL ABUN AC-227 -5. 213E-04 2.273E-01 2.273E-01 FAIL ABUN TH-227 -5.213E-04 2.273E-01 2.273E-01 FAIL ABUN TH-229 4.061E-02 4.873E-01 4.876E-01 FAIL ABUN TH-231 2.309E-01 6.366E-01 6.451E-01 FAIL ABUN PA-233 4.542E-02 6.llOE-02 6.444E-02 FAIL ABUN PA-234 -2.884E-02 2.459E-01 2.463E-01 FAIL ABUN PA-234M 6.096E-01 4.818E+OO 4.826E+OO NOT IDENT. NP-237 4.542E-02 6. llOE-02 6.444E-02 FAIL ABUN NP-238 8.874E+40 2.429E+41 O.OOOE+OO SHORT HLIF NP-239 -2.650E-02 2.318E-01 2.321E-01 NOT IDENT. PU-239 2.374E+02 3.224E+02 3.397E+02 NOT IDENT. AM-241 9.053E-02 1.382E-01 l.441E-01 NOT IDENT. CM-243 -8.033E-02 1.092E-01 l.150E-01 NOT IDENT. BK-247 -3.373E-02 7.332E-02 7.488E-02 NOT IDENT. CM-247 2.414E-04 3.662E-02 3.662E-02 NOT IDENT. CF-249 -1.809E-02 3.763E-02 3.850E-02 NOT IDENT. CF-251 -4.791E-03 1.119E-01 l.120E-01 NOT IDENT. Page 3010of5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, .SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 83.8463 87.09 117.3344 136.47 87.6127 45.60 77.4971 87.57 117.4180 140.51 0.0000 46.54 73.1555 88.03 117.4979 143.76 90.0468 49. 72 0.0000 88.34 117.5512 144.24 80.5642 51. 35 69.7358 88.47 117.5742 145.44 85.0043 51. 87 81. 9514 89. 96 117.8302 152.43 92.6217 52.39 82.0382 1093.63 117 .. 9472 153.25 0.0000 52.97 82.1346 91.11 0.0000 323.87 90.1659 53.44 82.2123 92.59 118.2780 156.02 0.0000 54.07 82.3162 93.35 118.4060 158.56 0.0000 57.36 0.0000 94;56 118. 6095 159.00 93.246.0 57.53 90.9330 94.65 89.6816 162.33 75.0226 57.98 86.4029 94.67 89.6844 162.66 0.0000 59.27 87.7696 94.87 89.7096 163.33 82.1649 59.32 87.7779 97.43 86.7563 165.86 92.9976 59.54 80.1111 98.43 82.3683 176.31 87.6730 60. 96 105.0388 98.44 82.3698 176.60 0.0000 61.17 95.8082 99.53 94.8048 177.52 81.5033 62.93 90.6917 100 .11 104.7377 181.07 0.0000 63. 29 90.7511 102.03 87. 7143 181.52 74.1656 63.58 90.7987 103.18 107.6462 184.41 82.9258 64.28 90.9129 103.37 107.6734 143.76 83.0250 66.73 120.1840 105.21 94.2891 193.51 89.0587 67.24 131.2269 105.31 94.3013 197.03 76.5728 125.81 125.0741 106.12 90.6758 198.01 73.9015 67.75 98.5074 106.47 90.7170 201.83 83.2991 69.67 118. 8364 109.28 104.7680 203.43* 84.3305 70.83 139.8981 111. 00 99.9988 205.31 89.5148 72. 81 127.7457 111. 76 0.0000 210.85 78.8647 72. 87 127.7589 114. 06 99.5492 215.65 63.8993 74.66 115. 0854 116.30 0.0000 222 .11 75.4069 74.82 115 .1150 116.74 89.8089 227.09 75.7076 74.97 115 .1431 119.76 79.1891 227.38 85.0746 77 .11 115.5427 121.12 85.2259 228.16 0.0000 78.74 115.8424 121. 22 85.2362 228.18 83.2573 79.69 119. 6045 121.78 77.6933 116.74 83.2573 80.12 119. 6854 122.06 77.7195 235.69 84.6890 80.19 0.0000 122.92 65 .1148 235. 96 80.4711 80.57 99.0093 123.07 76.9673 238.63 66.0181 81. 00 81. 4976 265.00 94.7979 238.98 0.0000 81. 07 81.5064 125.81 101.8250 240.99 66 .1377 81. 75 135.9875 127.23 87.5446 242.00 66.1883 83.79 154.0664 127.91 91.8677 244.70 52.5851 84.00 154 .1162 129.30 97.9788 252.40 0.0000 85 .43 133. 5342 131. 20 100.7545 252.80 66. 7259 86.55 117.2404 133.02 10.5. 2414 254.15 0.0000 86.79 117.2818 133.52 95.0282 256.23 60.2045 86.94 117.3085 136.00 72.9725 260.90 0.0000 Page 3011 of5809.

ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 58.6495 355.39 0.0000 584.27 22.1938 264.80 59.6172 356.01 27.5284 595.83 0.0000 265.00 63.4716 364.49 0.0000 427.87 27.4951 2 68. 22 53.4969 366.42 0.0000 602.52 0.0000 269.46 53.5432 372. 51 36.0233 604. 72 .24.0975 270.03 63.6985 375.05 42.2587 607.14 20.6748 271.23 63.7522 377.52 37.1565 609.32 24 .1411 273.65 0.0000 356.01 30.0372 610.33 24.1505 276.40 68.8304 388.16 42.5665 614.28 24.1881 277.37 57.2355 388.63 0.0000 618.01 20.7634 277.60 57.2451 391.69 39.5277 620.36 28.8635 278.00 46.5850 264.66 43.9004 621. 93 26.5713 279.20 54.3936 401.81 38.6975 630.19 0.0000 279.54 70.9222 402.40 40.8027 631.29 26.6667 279.70 70.9311 404.85 30.3800 633.25 17.4048 280.46 68.0518 410.95 38.8849 634.78 0.0000 283.69 51.6381 413. 71 35.7840 635.95 19.7455 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 65.3547 423. 72 0.0000 645.85 31. 4791 285.90. 0.0000 427.09 37.0921 657.76 21. 0798 287.50 61. 5401 427.87 34.9860 657.90 0.0000 290.67 61. 6721 433.94 39.3479 661.66 15.4811 293.27 0.0000 439.40 34.1237 664.57 0.0000 351.93 48.6037 453.88 39.7393 666.33 0.0000 295. 96 48.6269 463.37 35.6063 666.50 0.0000 879.38 17.7133 468.07 19.4656 667. 71 0.0000 299.98 47.2783 473.00 0.0000 677.62 17.6953 300.09 47.2822 475.06 35.8057 685.70 0.0000 300.13 47.2832 476.78 35.8346 695.00 0.0000 301.36 51. 7 577 4 77 .*60 24.9855 696.49 29.3967 302.85 66.6101 482.18 34.8372 696. 51 29.3967 256.23 53. 3452* 487.02* 0.0000 697.00 0.0000 304.85. 0.0000 492.35 0.0000 697.30 24.0584 306.78 44.5203 497.08 27.4043 697.49 21.3867 308.46 63.3854 505.52 29.7109 702.65 26.7828 311.90 43.6742 507.63 0.0000 706.68 27.7144 316.51 40.8148 511. 00 35.2995 711.68 27.7636 319.41 0.0000 514.00 41.4215 720.70 0.0000 320.08 0.0000 514.00 41.4215 721. 93 0.0000 321.04 38.9349 520.40 36.5557 722.78 33.0861 323.87 52.0042 520.69 0.0000 722.91 27.3329 325.23 52.0487 522.65 0.0000 723. 31 27.3366 328.76 0.0000 527.90 0.0000 724.19 37.4194 333.37 40.7406 528.26 22.2314 727.33 29.7159 333.97 40.7554 529.59 31:1423 733.00 19.5918 334.37 49.8243 529.87 0.0000 735.93 18. 9665 338.28 40.3573 531.02 0.0000 333.97 23.4943 338.32 40.3589 537.26 0.0000 739.50 0.0000 311. 90 40.4110 546.56 0.0000 .747.24 20.8529 340.48 40.4110 552.55 30.3278 748.06 19.9516 340.55 0.0000 563.25 30.4640 752.31 26.1554 344.28 28.8583 569.33 16.9678 753.82 0.0000 345.93 42.5699 946.00 16. 9690 756.73 14.5527 351.06 47.7822 569.70 16.9702 756.80 14.5527 351. 93 47.8061 583.19 20.4771 884.68 37.9285 Page 3012 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.3547 1274.44 16.6176 1620.50 6.7394 766.42 16. 0596 1001.03 18.5970 1621.92 5.6177 766.84 14.6016 1002.74 23.5012 1678.03 0.0000 772.60 0.0000 1004.73 15.6763 1690.97 3.0340 *776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.7662 778.90 21.0733 1028.54 0.0000 1063.66 11. 9990 783.70 0.0000 1037.84 20.7578 1771.35 3.6926 785.37 24.7909 1038.76 0.0000 1791.20 0.0000 792.07 36.8079 631.29 14.8608 1808.65 2.7872 794.95 21.1842 1048.07 0.0000 1810.72 0.0000 795.86 22 .1111 1049.04 13.8787 1836.06 0.9333 810.0ti 28.6907 1050.41 13.8838 810.29 26.8415 1063.66 9.9512 344.28 26.8432 1077.00 0.0000 810.76 24.0687 1077.34 9.9860 815.77 0.0000 1085.87 14. 0111, 1048.07 0.0000 1093.63 17.0467 832.01 19.3845 1099.45 13.0555 834.85 22.3865 1112. 07 16 .1191 835.71 25.5912 1112.84 13.0992 836.80 0.0000 1115. 54 14.5195 846.75 0.0000 1120.29 13.1230 846.77 19.6599 1120.55 13 .1238 856.80 0.0000 1221.41 14.5406 860.56 23.5039 1129. 67 17.2013 871.09 15.0903 1131. 51 0.0000 873.19 15.1001 1147.95 0.0000 875.33 0.0000 1173.23 22. 4968 879.38 13.2369 1177.95 17.4036 880.51 15.1333 1189.05 13 .1383 883.24 17.0387 1204.77 14.8359 884.68 14.2049 1221.41 23.6398 889.28 11. 3796 1231.02 13.4753 894.76 18.0468 1235.36 0.0000 898.04 10.4582 1238.28 20.7654 900.72 17.1271 1260.41 0.0000 903.28 14.2831 1271. 87 8.3701 911.20 19.0881 1274.44 11.5156 912.08 19.0930 1274.54 11.5156 923.98 0.0000 1291. 59 15.7626 926.50 14.3797 1298.22 0.0000 929 .11 24.9439 1312.11 0.0000 937.49 17.3101 1332.49 7.4221 944.13 0.0000 1362 .-66 *O. 0000 946.00 10.7967 1365.19 4.2712 949.00 10. 6.129 1368.63 0.0000 667.71 0.0000 1384.29 9.6487 962. 31 3.0989 1408.01 3.2324 964.08 7.7512 1457.56 0.0000 966.17 7.7556 1460.82 9.8020 911.20 13. 9711 1489.16 6.5717 968. 97 13. 9711 1505.03 7.6913 983.53 0.0000 1584.12 14.5028 984.45 0.0000 1596.21. 0.0000 Page 3013 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:05:32.50 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date 10-DEC-2015 13:25:00 Acquisition date : 3-0CT-2016 08:02:32. Sample ID G405235006 Sample quantity 1.56342E+02 GRAM Detector name GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:14.99 0.4% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 7 7 0 1 1 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3014of5809 Energy 26.75* 28.24* 63.57* 73.54 76.84 84.32* 87.19 89.95* 92.82* 105.40 121. 3 9 128.75 186.06* 210.28 238.45* 241.57 270.34 295.06* 300.35 338.55* 351.77* 446.92 462.90 511. 01
543.83 583.49* 609.34* 654.51 727.18 786.46 794.94 835.82 911. 38* 957.75 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 15 38 0 51 316 33 83 36 94 42 32 38 63 35 473 80 66 201 53 96 288 39 46 15 64 164 179 26 32 17 29 18 142 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 68 243 190 172 119 181 107 201 147 99 82 164 146 122 84 106 72 61 78 60 30 50 79 30 42 49 14 14 29 7 15 19 11 1.19 53.71 2.00 56.68 0.50 127.29 1.23 147.22 1.24 153.82 0.77 168.76 1.03 174.51 0.96 180.02 1.51 185.76 1.17 210.90 1.33 242.85 1.75 257.57 0.93 372.12 2.42 420.54 1.22 476.85 1.22 483.08 1.48 540.60 0.98 590.03 1.02 600.60 1.14 676.98 1.24 703.41 2.59 893.68 1.74 925.64 1.85 1021.84 5.63 1087:48 1. 32 l166. 82 1.52 1218.53 1.06 1308.89 2.01 1454.27 0.64 1572.89 2.70 1589.85 4.43 1671.64 1. 54. 1822. 85 3.21 1915.67 51 51 123 144 144 166 172 178 178 207 239 255 367 411 471 481 535 584 596 671 698 885 919 1016 1074 1159 1211 1304 1448 1568 1585 1664 1817 1910 16 16 9 16 16 6 7 13 13 10 7 6 11 12 10 7 13 11 11 13 12 15 15 15 30 16 13 10 11 14 9 12 15 9 4.30E-03 69.1 1.05E-02 59.6 l.OlE-04***** 1.42E-02 50.3 8.78E-02 9.5 9.21E-03 56.2 2.29E-02 29.0 1.00E-02 42.8 2.60E-02 30.6 1.17E-02 55.6 8.84E-03 55.2 1. 05E-02 41. 4 1.76E-02 42.8 9.85E-03 70.3 1.31E-01 6.5 2.21E-02 22.5 1. 84E-02 34. 5 5.59E-02 .10.8 1.46E-02 31.8 2.68E-02 21.6 8.0lE-02 8.0 1. 09E-02 34. 4 1.29E-02 36.1 4.17E-03143.3 1.76E-02 28.1 4.55E-02 12.0. 4. 97E-02 11. 1 7-.08E-03 34.5 8.96E-03 28.4 4.75E-03 70.2 8.14E-03 24.4 4.99E-03 49.2 3.95E-02 10.8 3.83E-03 51.5 Fit 2.88E+OO 2.27E+Ol .3. OlE+OO Peak Search Report (continued) Page : 2 Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 1 964. 57 41 10 1. 94 1929.32 1922 22 l.15E_.:02 22.3 2.97E+OO 36 1 969. 00 73 17 1. 87 1938.18 1922 22 2.03E-02 14.7 37 0 1088.96 11 12 1.19 2178.31 2174 9 2.92E-03 65.5 38 0 1095.52 29 11 4.82 2191. 43 2183 17 8.07E-03 33.4 39 0 1104. 64 12 6 3.10 2209.70 2204 11 3.19E-03 49.3 40 0 1108. 77 11 . 4 1.17 2217.95 2214 7 2.92E-03 42.7 41 0 1120.71 33 22 1.18 2241.86 2239 8 9.18E-03 30.1 42 1 1203.69 17 9 1. 87 2408.00 2400 20 4.59E-03 40.0 6.67E-01 43 1 1206.69 14 7 1. 87 2414.00 2400 20 3.77E-03 54.5 44 0 1238.48 27 7 2.23 2477.66 2472 10* 7.42E-03 27.2 45 0 1258.60 11 11 1. 01 2517. 96 2512 9 3.12E-03 61.3 46 0 1288.43 15 7 2.88 2577.68 2572 13 .4.17E-03 43.8 47 0 1334. 20 17 6 1.19 2669.34 2664 12 4.73E-03 37.6 48 0. 1360.53 6 5 0.55 2722.08 2718 6 1.53E-03 74.4 49 0 1377.89 22 5 1. 34 2756.85 2751 11 6.08E-03 29.7 50 0 1416.25 6 9 0.55 2833.68 2823 12 1.74E-03103.4 51 0 1460.92* 480 0 2.16 2923.15 2916 14 l.33E-01 4.6 52 0 1588.20 11 6 4.32 3178.14 3171 12 3.06E-03 53.8 53 0 1630.78 11 0 0.83 3263.45 3257 11 3.06E-03 30.2 54 0 1729.10 13 3 0. 72 3460.47 3453 13 3.67E-03 39.0 55 0 '1764.39 43 0 2.54 3531.19 3525 12 1.19E-02 15.2 Flag: "*" = Peak area was modified by background subtraction Page 3015of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:05:34 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 13:25:00 G405235006 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:02:32 156.34 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA20 0 01:00:00.00 1. 50 keV No Linear 75. 00. Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3016of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109. 88.03 TH-229 88.47' RA-224 240.99 BI-211 72. 87 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:14.99 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error status K-40 1460.82 10.66* 1.312E+OO 1.597E+Ol 1.597E+Ol 9.18 OK MN....:54 834.85 99.98* 2.057E+OO 4.332E-02 8.395E-02 98.38 OK C0-57 122.06 85.60* 7.574E+OO 2. 963E-02 6.333E-02 110.46 OK 136.47 10.68 7.468E+OO Line Not Found Absent Y-91 1204.77 0. 26* 1.543E+OO 1. 960E+Ol 6.675E+02 79. 96 OK CD-109 88.03 3.70* 6.842E+OO 8.453E-01 1.322E+OO 142.57 OK SN-126 64.28 9.60 4.822E+OO 5. 031E-03 5.031E-03******* OK 86.94 8.90 6.842E+OO 3.514E-01 3.514E-01 142.57 OK 87.57 37.00* 6.842E+OO 8.453E-02 8.453E-02 142.57 OK PM-147 121.22 0.00* 7.574E+OO 8.899E+02 l.104E+03 110. 46 OK EU..:.155 86.55 30.70 6.842E+OO l.019E-01 l.147E-01 142.57 OK 105.31 21.10* 7.457E+OO 1.643E-01 1.850E-01 111.18 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.718E+oo 3.661E-01 3.661E-01 24.08 OK 860.56 12.50 2. OllE+OO Line Not Found Absent BI-212 "727.33 6.67* 2.290E+OO 1.064E+OO 1.064E+OO 56.79 OK 785.37 1.10 2.156E+OO 3.600E+OO 3.600E+OO 140.46 OK 1620.50 1. 47 1.197E+OO Line Not Found Absent PB-212 74.82 10.28 5. 996E+'OO Line Not Found <<INT Rej e'ct 77 .11 17.10 6.163E+OO 1.887E+OO 1.887E+OO 19.08 OK 238.63 43.60* 5.555E+OO 1.105E+OO 1.105E+OO 12.91 OK 300.09 3.30 4.643E+OO 1. 896E+OO l.896E+OO 63. 67 OK BI-214 609.32 45.49* 2.627E+OO 7.694E-01 7.696E-01 22.24 OK 1120. 29* 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 OK 1764.49 15.30 1.106E+OO

1.155E+OO l.155E+OO 30.50 OK PB-214 74.82 5.80 5.884E+OO 9.459E-01 9.463E-01 100.67 OK 77 .11 9.70 6.163E+OO 3.326E+OO 3.328E.+00 19.08 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.502E+OO 1.127E+OO l.128E+00 45.00 OK 295.22 18.42 4.710E+OO 1.287E+OO 1.287E+OO 21. 68 OK 351.93 35.60* 4.085E+OO 1.079E+OO 1.080E+OO 16.10 OK RN-222 609.32 45.49* 2.627E+OO 7.694E-01 7. 696E-01 22.24 OK 1120.29 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 OK 1764.49 15.30 l.106E+OO 1.155E+OO 1.155E+00 30.50 OK RA-226 609.32 45.49* 2.627E+OO 7.694E-01 7.696E...:01 22.24 OK 1120.29 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 OK 1764.49 15.30 1.106E+OO 1.155E+OO 1.155E+OO 30.50 OK AC-228 105.21 1.10 7.457E+OO 3 .151E+OO 3.151E+OO 111.18 OK 338.32 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 OK 794.95 4.25 2.138E+OO 1.609E+OO 1.609E+OO 48.85 OK 835. 71 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 OK 911. 20 25.80* 1.923E+OO l.408E+OO l.408E+OO 21. 64 OK 968. 97 15.80 1.834E+OO 1.229E+OO l.229E+OO 29.49 OK RA-228 105.21 1.10 7.457E+OO 3 .151E+OO 3.151E+OO 111.18 OK 338.32 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 OK 794.95 4.25 2.138E+OO l.609E+OO 1.609E+OO 48.85 OK 835. 71 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 OK 911. 20 25.80* 1.923E+OO 1.408E+OO 1.408E+OO 21. 64 OK 968. 97 15.80 1.834E+OO 1.229E+OO 1.229E+OO 29.49 OK Page 3017 of5809 Nuclide Line Activity Report (continued) Sample ID : G405235006 ' Acquisition date Page : 3 Nuclide Type: Nuclide TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Energy 74.82 77.11 238.63 300.09 85.43 88.47 193.51 210.85 609.32 1120.29 1764.49 283.69 301.36 105.21 338.32 835.71 911.20 968. 97 63.29 92.59 609.32 1120.29 1764.49 89. 96 93.35 143.76 163.33 185.72 205.31 63.29 92.59 511. 00 %Abn 10.28 17.10 43.60* 3.30 14.70 24.00 4.41* 2.80 45.49* 14.92 15.30 1. 70 5.35* 1.10 11. 27 1. 61 25.80* 15.80 3.70* 4.23 45.49* 14.92 15.30 3.47 5.60 10. 96* 5.08 57.20 5.01 3.70* 4.23 100.00* Flag: "*" = Keyline Page 3018of5809 %Eff 5. 996E+OO 6.163E+OO 5.555E+OO 4.643E+OO 6.681E+OO 6.842E+OO 6.409E+OO 6.074E+OO 2.627E+OO l.635E+OO l.106E+OO 4.860E+OO 4.643E+OO 7.457E+OO 4.214E+OO 2.057E+OO l.923E+OO l.834E+OO 4.822E+OO' 7.101E+OO 2.627E+OO l.635E+OO l.106E+OO 6.978E+OO 7.101E+OO 7.370E+OO 7.024E+OO 6.562E+OO 6.171E+OO 4.822E+OO 7.101E+OO '3.019E+OO 3-0CT-2016 08:02:32 Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error Status Line Not Found l.887E+OO l.887E+OO l.105E+OO l.105E+OO l.896E+OO l.896E+OO 2.108E-01 2.108E-01 l.303E-01 l.303E-01 Line Not Found l.196E+OO l.196E+OO 7.694E-01 7.694E-01 6.500E-01 6.500E-01 l.155E+OO l.155E+OO 19.08 12.91 63.67 112. 36 142.57 140.62 22.24 60.22 30.50 Line Not Found l.169E+OO l.169E+OO 63.67 3.151E+OO 3.151E+OO 111.18 l.llOE+OO l.llOE+OO 43.25 2.690E+OO 2.690E+00 98.38 l.408E+OO l.408E+OO 21.64 l.229E+OO l.229E+OO 29.49 l.305E-02 l.305E-02******* l.932E+00 l.932E+OO 61.25 7.694E-01 7.694E-01 22.24 6.500E-01 6.500E-01 60.22 l.155E+OO l.155E+OO 30.50 9.241E-01 9.241E-01 85.65 l.459E+OO l.459E+OO 61.25 Line Not Found Line Not Found 9.797E-02 9.797E-02 85.62 Line Not Found l.305E-02 l.305E-02******* l.932E+OO l.932E+OO 61.25 2.603E-02 2.603E-02 286.68 <<INT Reject OK OK OK OK OK Absent OK OK OK OK Absent OK OK OK OK OK OK OK OK OK OK OK OK OK Absent Absent OK Absent OK OK OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:05:35.82 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l *
Acquisition date 3-0CT-2016 08:02:32 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.99 Half life ratio : ***** *
Sample date 10-DEC-2015 13:25:00 Analyst initials: MXRl *
Sample ID G405235006 Sample Quantity 1.5634E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.597E+Ol 1.437E+OO MN-54 8.395E-02 8.094E-02 C0-57 6.333E-02 6.855E-02 Y-91 6.675E+02 5. 2*31E+02 CD-109 1.322E+OO 1. 847E+OO SN-126 8.453E-02 l .181E-01 PM-147 l.104E+03 1.195E+03 EU-155 1.850E-01 2.016E-01 TL-208 3.661E-01 8.638E-02 BI-212 1.064E+OO 5.920E-01 PB-212 1.105E+OO l.398E-01 BI-214 7. 696E-01 1.678E-01 PB-214 1.080E+OO 1.703E-01 RN-222 7. 696E-01 l.678E-01 RA-226 7. 696E-01 1.678E-01 AC-228 l.408E+OO 2.987E-01 RA-228 1.408E+OO 2.987E-01 TH-228 1.105E+OO 1.398E-01 TH-229 7.367E-02 4.123E-01 TH-230 7.694E-01 l.677E-01 PA-231 l.169E+OO 7.297E-Ol TH-232 1.408E+OO 2.987E-01 TH-234 1. 305E-02 2.015E+OO U-234 7.694E-01 l.677E-01 U-235 -2.283E-02 l.683E-01 U-238 1.305E-02 2.015E+OO ANH-511 2.603E-02 7.312E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3019of5809 Key-Line Activity (pCi/GRAM 1.023E+OO -2.495E-02 O.OOOE+OO K.L. Cnt* Uncert ( 1. 96-sigma) 8.808E+OO 3.358E-02 1. 960E+41 MDA (pCi/GRAM 3.706E-01 l.126E-01 7.947E-02 6.999E+02 1. 773E+OO 1.137E-01 1.17 9E+03 l.643E-01 5.374E-02 6.980E-01 8.502E-02 1.143E-01 l.083E-01 1.143E-01 1.143E-01 1. 578E-01 1. 578E-01 8.502E-02 8.250E-01 l.143E-01 6.113E-01 1.578E-01 1.560E+OO l.143E-01 3.042E-01 1.560E+OO 4.614E-02 MDA (pCi/GRAM 1. 761E+Ol 5.855E-02 O.OOOE+OO NOT IDENT. NOT 'IDENT. SHORT HLIF AL-26 O.OOOE+OO 8.732E-03 l.210E-02 NOT IDENT. SC-46 l.332E-01 2.927E-01 6.099E-01 FAIL ABUN V-48 O.OOOE+OO l.052E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.021E+02 O.OOOE+OO SHORT HLIF C0-56 l.650E-01 2.952E-01 6.507E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 789E+41 O.OOOE+OO SHORT HLIF C0-58 -3. 271E-01 4.576E-01 7.628E-01 NOT IDENT. FE-59 4.920E+OO 3.163E+OO 9. 091E+OO NOT IDENT. C0-60 4.019E-02 2.818E-02 7.222E-02 NOT IDENT. ZN-65 -3.067E-02 1. 335E-*01 2.514E-01 NOT IDENT. GE-68 -2.497E-01 l.905E+OO 3.777E+OO NOT IDENT. AS-73 4.709E-02 5.122E+OO 9. 820E+OO NOT IDENT. AS-74 O.OOOE+OO 4.730E+03 O.OOOE+OO SHORT HLIF. SE-75 -6. 351E-02 l.680E-01 3.059E-01 FAIL ABUN BR-77 O.OOOE+OO l.382E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.250E+02 O.OOOE+OO SHORT HLIF RB-83 3.126E-02 5.566E-01 l.083E+OO NOT IDENT. KR-85 1. 789E+OO 6.540E+OO l.171E+Ol NOT IDENT. SR-85 l.852E-01 6.763E-01 l.211E+OO NOT IDENT. RB-86 O.OOOE+OO 2.298E+04 O.OOOE+OO SHORT HLIF Y-88 4.852E-02 7.663E-02 2.677E-01 NOT IDENT. NB-94 2.643E-02 2.816E-02 5. 967E-02 NOT IDENT. NB-95 -4.482E-01 7.824E-01 l.348E+OO NOT IDENT. NB-95M -7.774E-02 2.027E+OO 3.588E+OO NOT IDENT. ZR-95 -l.106E-01 l.356E+OO 2.525E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO 9.017E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 l.017E-02 3.106E-02 5.424E-02 NOT IDENT. RH-102 -l.268E-02 4.314E-02 8.041E-02 NOT IDENT. RU-103 -8.177E-01 4.273E+OO 8.146E+OO FAIL ABUN RH-106 2.870E-01 4.005E-01 8.522E-01 NOT IDENT. RU-106 2.870E-01 4.005E-01 8.522E-01 NOT IDENT. AG-108M -2.404E-02 2.189E-02 3.677E-02 NOT IDENT. AG-llOM -2.067E-02 7.810E-02 l.429E-01 NOT IDENT. SN-113 -l.728E-01 2.027E-01 3.583E-01 NOT IDENT. CD-115 O.OOOE+OO l.463E+39 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.675E+04 O.OOOE+OO SHORT HLIF TE-123M 7.504E-02 l.194E-01 2.273E-01 NOT IDENT. SB-124 l.068E+OO l.509E+OO 3. 831E+OO NOT IDENT. SB-125 5.590E-02 8.202E-02 1. 728E-01 FAIL ABUN TE-125M 3.300E+Ol 2. 511E+02 4.330E+02 NOT IDENT. I-126 O.OOOE+OO 6.554E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.492E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.293E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.417E+09
0. OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.209E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.209E+26 O.OOOE+OO SHORT*HLIF BA-133 -l.606E-03 3.919E-02 7.061E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 5.032E-02 l.OOlE-01 FAIL ABUN CS-135 6.807E-02 l.326E-01 2.466E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.078E+05 O.OOOE+OO SHORT HLIF BA-137M 3.260E-02 3.657E-02 7.489E-02 NOT IDENT. CS-137 3.443E-02 3.863E-02 7. 911E-02 NOT IDENT. CE-139 3.492E-02 9.631E-02 l.800E-01 NOT IDENT. BA-140 O.OOOE+OO 8.021E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.277E+05 O.OOOE+OO SHORT HLIF CE-141 -2.549E+OO 2.069E+Ol 3.738E+Ol NOT IDENT. CE-143 O.OOOE+OO 4.447E+40 O.OOOE+OO' SHORT HLIF CE-144 8.658E-02 3.246E-01 6.052E-01 NOT IDENT. PM-144 9.297E-03 3.994E-02 8.052E-02 NOT IDENT. PR-144 7.690E-01 3.459E+OO 6. 964E+OO NOT IDENT. PM-146 -*4. 613E-03 3.653E-02 6.994E-02 NOT IDENT. ND-147 O.OOOE+OO 2.538E+07 O.OOOE+OO SHORT HLIF PM-149 O.OOOE+OO 1. 938E+40 O.OOOE+OO SHORT HLIF EU-150 -l.374E-02 2.402E-02 3.900E-02 FAIL ABUN EU-152 2.263E-02 8.124E-02 l.563E-01 FAIL ABUN GD-153 3.451E-02 l.485E-01 2. 811E-01 NOT IDENT. EU-154 -5.181E-02 8.030E-02 l.437E-01 NOT IDENT. TB-160 -l.190E+OO l.530E+OO 2.487E+OO FAIL ABUN H0-166M 2.688E-02 4. 531E-02 9.477E-02 NOT IDENT. TM-171 -l.661E+OO l.166E+Ol 2.218E+Ol NOT IDENT. HF-172 2.763E-02 2. 097E*-01 3.599E-01 FAIL. ABUN LU-172 8.659E-02 6.847E-02 l.520E-01 FAILABUN LU-176 3.988E-03 2.147E-02 4.260E-02 FAIL ABUN Page 3020 of 5809 HF-181 1.079E+OO 3.284E+OO 6.687E+OO NOT IDENT. TA-,182 7.436E-01 8.528E-01 1.849E+OO FAIL ABUN RE-183 -2.026E-01 1.829E+OO 3.463E+OO NOT IDENT. RE-184 -2.740E+OO 2.614E+Ol 4.846E+Ol NOT IDENT. W-188 -4.717E+Ol l.004E+02 1. 672E+02 FAIL ABUN IR-192 -1. 267E-01 3.466E-01 6.595E-01 FAIL ABUN HG-203 -7.852E-02 2.006E+OO 3.918E+OO FAIL ABUN BI-207 -l.900E-02 3. 968E-02 7. 421E-02 FAIL ABUN PB-210 -l.283E+OO 1.617E+OO
2. 972E+OO NOT IDENT. BI-211 O.OOOE+OO 4.691E-01 7.832E-01 FAIL ABUN PB-211 3.265E-02 5.032E-01 9.959E-01 NOT IDENT. RN-219 8.218E-02 3.087E-01 . 6 .196E-01 FAIL ABUN RA-223 2.836E-01 4.879E-01 1. 005E+OO FAIL ABUN RA-224 O.OOOE+OO 8.792E-01 1.309E+OO FAIL ABUN AC-227 1.949E-02 1.984E-01 3.929E_..:01 FAIL ABUN TH-227 1.949E-02 1.984E-01 3.929E-01 FAIL ABUN TH-231 2.836E-01 4.879E-01 l.005E+OO FAIL ABUN PA-233 -2.120E-02 5.083E-02 9.575E-02 FAIL ABUN PA-234 1.098E-01 2.475E-01 5.245E-01 NOT IDENT. *PA-234M 2.820E+OO 3.809E+OO 8.419E+OO NOT IDENT. NP-237 -2.120E-02 5.083E-02 9.575E-02 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF NP-239 -1. 976E-01 2.067E-01 3.502E-01 FAIL ABUN PU-239 4.764E+02 3.862E+02 5.310E+02 FAIL ABUN AM-241 2.954E-02 9.556E-02 l.724E-01 NOT IDENT. AM-243 8.165E-02 8.055E-02 1.lOOE-01 FAIL ABUN CM-243 l.654E-02 7.731E-02 1. 368E-01 NOT IDENT. BK-247 -1.296E-02 6.102E-02 1.061E-01 FAIL*ABUN CM-247 -1.052E-02 2.867E-02 5.364E-02 NOT IDENT. CF-249 1. 569E-02-3.256E-02 6.621E-02 NOT IDENT. CF-251 6.862E-02 1.006E-01 2.083E-01 NOT IDENT. Page 3021of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:05:33.27 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 465 10.66* 1.312E+OO 1.597E+Ol 1.597E+Ol 9.18 MN-54 834.85 19 99.98* 2.057E+OO 4.332E-02 8.395E-02 98.38 C0-57 122.06 40 85.60* 7.574E+OO 2. 963E-02 6.333E-02 110. 46 136.47 ------10.68 7.468E+OO ------Line Not Found ------Y-91 1204.77 16 0. 26* 1.543E+OO 1. 960E+Ol 6.675E+02 79. 96 CD-109 88.03 107 3.70* 6.842E+OO 2.031E+OO 3.177E+OO 57.97 SN-126 64.28 0 9.60 4.822E+OO 5. 031E-03 5. 031E-03 15752.45 86.94* 107 8.90 6.842E+OO 8.444E-01 8.444E-01 57.97 87.57 107 37.00* 6.842E+OO 2. 031E-01 2.031E-01 57.97 PM-147 121.22 40 0.00* 7.574E+OO 8.899E+02 1.104E+03 110. 46 EU-155 86.55 107 30.70 6.842E+OO 2.448E-01 2.757E-01 57.97 105.31 54 21.10* 7.457E+OO l.643E-'-01 1.850E-01 111.18 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 176 85.00* 2.718E+OO 3.661E-01 3.661E-01 24.08 860.56 ------12.50 2. 011E+OO ------Line Not Found ------BI-'211 72.87 67 1. 23 5. 884E+o0' 4.460E+OO 4.460E+OO 100.67 351.06 327 12.92* 4.085E+OO 2.974E+OO 2.974E+OO 16.10 BI-212 727. 33 34 6.67* 2.290E+OO l.064E+00 1.064E+OO 56.79 785.37 18 1.10 2.156E+OO 3:600E+OO 3.600E+OO 140.46 1620.50 ------1. 47 l.197E+00 ------Line Not Found ------PB-212 74.82 67 10.28 5.884E+OO 5.337E-01 5.337E-01 100.67 77 .11 414 17.10 6.163E+00 1.887E+OO 1. 887E+OO 19.08 238.63 557 43.60* 5.555E+OO l.105E+OO 1.105E+00 12.91 300.09 60 3.30 4.643E+OO 1.896E+OO 1.896E+OO 63. 67 BI-214 609.32 191 45.49* 2.627E+OO 7.694E-01 7. 696E-01 22.24 1120.29 33 14.92 l.635E+OO 6.500E-01 6.502E-01 60.22 1764.49 41 15.30 1.106E+OO l.155E+OO 1.155E+OO 30.50 PB-214 74.82 67 5.80 5.884E+OO 9.459E-01 9.463E-01 100.67 77 .11 414 9.70 6.163E+OO 3.326E+00 3.328E+OO 19.08 87.09 107 3.41 6.842E+OO 2.204E+OO 2.205E+OO 57.97 242.00 94 7;25 5.502E+00 l.127E+OO 1.128E+OO 45.00 295.22 232 18.42 4.710E+00 l.287E+OO 1.287E+OO 21. 68 351. 93 327 35.60* 4.085E+OO l.079E+00 1.080E+OO 16.10 RN-222 609.32 191 45.49* 2.627E+OO 7.694E-01 7.696E-01 22.24 1120.29 33 14.92 1. 635E+OO 6.500E-01 6.502E-01 60.22 1764.49 41 15.30 l.106E+00 l.155E+OO l.155E+00 30.50 RA-224 240.99 94 4.10* 5.502E+OO 1.994E+OO 1.994E+OO 45.00 RA-226 609.32 191 45.49* 2. 627E+OO* 7.694E-01 7. 696E-01 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 1764.49 41 15.30 1.106E+OO l.155E+OO 1.155E+OO 30.50 AC-228 105.21 54 1.10 7.457E+OO 3 .151E+OO 3.151E+OO 111.18 338.32 110 11. 27 4.214E+OO 1.110E+OO 1.110E+OO 43.25 794.95 30 4.25 2.138E+OO 1.609E+OO 1.609E+OO 48.85 835.71 19 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 911.20 146 25.80* 1.923E+OO 1.408E+OO 1. 408E+OO 21. 64 968. 97 74 15.80 1.834E+OO L 229E+OO 1.229E+OO 29.49 RA-228 105.21 54 1.10 7.457E+OO 3.151E+OO 3 .151E+OO 111.18 Page 3022 of 5809 Nuclide Line Activity Report (continued) Page : 2
Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 338.32 110 11. 27 4.214E+OO 1. llOE+OO 1.llOE+OO 43.25 794.95 30 4.25 2.138E+OO l.609E+OO l.609E+OO 48.85 835. 71 19 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 911. 20 146 25.80* 1.923E+OO l.408E+00 1.408E+OO 21. 64 968. 97 74 15.80 1.834E+OO l.229E+OO l.229E+OO 29.49 TH-228 74.82 67 10.28 5.884E+OO 5.337E-01 5.337E-01 100.67 77 .11 414 17.10 6.163E+OO l.887E+OO 1.887E+OO 19.08 238.63 557 43.60* 5.555E+OO 1.105E+OO 1.105E+OO 12.91 300.09 60 3.30 4.643E+OO 1. 896E+OO 1. 896E+OO 63.67 TH-229 85.43 43 14.70 6. 681E+OO 2.108E-01 2.108E-01 112.36 88.47 107 24.00 6.842E+OO 3.131E-01 3.131E-01 57.97 193.51 ------4.41* 6.409E+OO ------Line Not Found ------210.85 42 2.80 6.074E+OO l .196E+00 l .196E+00 140.62 TH-230 609.32 191 45.49* 2.627E+OO 7.694E-01 7. 694E-01. 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.500E-01 60.22 1764.49 41 15.30 1.106E+OO 1.155E+OO 1.155E+OO 30.50 PA-231 283.69 --*----1. 70 4.860E+OO ------Line Not Found ------301.36 60 5.35* 4.643E+OO 1.169E+OO 1.169E+OO 63.67 TH-232 105.21 54 1.10 7.457E+OO 3.151E+OO 3.151E+OO 111.18 338.32 110 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 835. 71 19 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98. 38 . 911.20 i46 25.80* 1.923E+OO 1.408E+OO 1.408E+OO 21. 64 968. 97 74 15.80 1.834E+OO 1. 229E+OO 1.229E+OO 29.49 TH-234 63.29 0 3.70* 4.822E+OO 1.305E-02 l.305E-02 15752.45 92.59 121 4.23 7 .101E+OO l.932E+00 1.932E+OO 61. 25 U-234 609.32 191 45.49* 2.627E+00 7.694E-01 7.694E-01 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.500E-01 60.22 1764.49 41 15.30 1.106E+OO 1.155E+OO 1.155E+OO 30.50 U-235 89. 96 47 3.47 6.978E+OO 9.241E-01 9. 241E-01 85.65 93.35 121 5.60 7.101E+OO l.459E+00 l.459E+00 61. 25 143.76 ------10. 96* 7.370E+OO ------Line Not Found ------163.33 -------5. 08 7.024E+OO ------Line Not Found ------185. 72 77 57.20 6.562E+OO 9.797E-02 9.797E-02 85.62 205.31 ------5.01 6.171E+OO ------Line Not Found ------U-238 63.29 0 3.70* 4.822E+OO 1.305E-02 1.305E-02 15752.45 92.59 121 4.23 7 .101E+OO 1.932E+00 l.932E+OO 61.25 AM-243 43.53 ------5.90 l.315E+00 ------Line Not Found ------74.66 67 67.20* 5.884E+OO 8.164E-02 8.165E-02 100.67 ANH-511 511. 00 16 100.00* 3.019E+OO 2.603E-02 2.603E-02 286 .. 68 Flag: "*" Keylin.e Page 3023 of 5809 Summary of Nuclide Activity Sample ID : G405235006 Page : 3 Acquisition date 3-0CT-2016 08:02:32 Total number of lines in spectrum 55 Number of unidentified lines 20 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 MN-54 C0-57 Y-91 CD-109 SN-126 PM-147 EU-155 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 312.05D 271.74D 58.51D 461.40D 2.30E+05Y 2.62Y 4.75Y l.41E+l0Y 7.04E+08Y l.41E+l0Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+l0Y l.41E+l0Y l.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 94 2.14 34.1 1. 56 1. 00 1. 24 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.597E+Ol 4.332E-02 2. 963E-02 l.960E+Ol 2. 031E+OO 2. 031E-01 8.899E+02 l.643E-01 3.661E-01 2.974E+00 1. 064E+OO l.105E+OO 7.694E-01 l.079E+OO 7.694E-01 l.994E+OO 7.694E-01 l.408E+OO l.408E+OO l.105E+OO 3 .131E-01 7.694E-01 l.169E+00 l.408E+OO l.305E-02 7.694E-01 9.797E-02 l.305E-02 8.164E-02 2.603E-02 9.474E+02 9.474E+02 Decay Corr pCi/GRAM ' l.597E+Ol 8.395E-02 6.333E-02 6.675E+02 3.177E+OO 2. 031E-01 l.104E+03 l.850E-01 3. 661E-01 2.974E+OO l.064E+OO l.105E+00 7. 696E-01 l.080E+OO 7. 696E-01 l.994E+OO 7.696E-01 l.408E+OO l.408E+00 l.105E+OO 3.131E-01 7.694E-01 l.169E+OO l.408E+OO l.305E-02 7.694E-01 9.797E-02 l.305E-02 8.165E-02 2.603E-02 1. 811E+03 1. 811E+03 63.64% Decay Corr 2-Sigma Error 0.147E+Ol 8.259E-02 6.995E-02 5.337E+02 l.842E+OO l. l 77E-01 l.219E+03 2.057E-01 0. 881E-01 0.479E+OO 0.604E+00 0.143E+OO 1. 712E-01 0.174E+OO 1. 712E-01 0.897E+OO l.712E-01 0.305E+OO 0.305E+OO 0.143E+OO l.815E-01 2-Sigma %Error 9.18 98.38 110.46 79. 96 57.97 57.97 110.46 111.18 24.08 16.10 56.79 12.91 22.24 16.10 22.24 45.00 22.24 21. 64 21. 64 12.91 57.97 22.24 63.67 21. 64 1. 711E-01 0.745E+OO 0.305E+OO 205.6E-02 l.711E-01 8.388E-02 205.6E-02 8.220E-02 7.461E-02 15752.45 22.24 85. 62 15752.45 100.67 286.68 Flags: "K" Keyline not found "E" = Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Page 3024 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235006 Acquisition date : 3-0CT-2016 08:02:32 It Energy Area Bkgnd FWHM *channel Left Pw Cts/Sec %Err %Eff Flags 7 26.75 22 11 1.19 53. 71 51 16 4.30E-03 **** 1. 71E-07 7 28.24 54 98 2.00 56.68 51 16 l.05E-02 **** l.29E-05 0 128.75 47 103 1. 75 257.57 255 6 1. 05E-02 82.7 7.54E+OO T 0 270.34 77 123 1. 48 540.60 535 13 1. 84E-02 69.1 5.05E+OO T 0 446.92 43 33 2.59 893.68 885 15 1. 09E-02 68.8 3.36E+OO 0 462.90 51 55 1. 74 925.64 919 15 l.29E-02 72.2 3.27E+OO T 0 543.83 69 33 5.63 1087.48 1074 30 l.76E-02 56.2 2.87E+OO 0 654.51 27 15 1. 06 1308.89 1304 10 7.08E-03 69.0 2.48E+OO 0 957.75 14 11 3.21 1915.67 1910 ,9 3.83E-03 **** 1. 85E+OO 1 964. 57 42 10 1. 94 1929.32 1922 22 l.15E-02 44.6 l.84E+OO T 0 1088.96 11 12 1.19 2178.31 2174 9 2.92E-03 **** 1. 67E+00 0 1095.52 29 11 4.82 2191. 43 2183 17 8.07E-03 66. 8. 1. 66E+OO 0 1104. 64 12 6 3.10 2209.70 2204 11 3.19E-03 98.6 1. 65E+OO 0 1108. 77 11 4 1.17 2217.95 2214 7 2.92E-03 85.4 1. 65E+OO 1 1206.69 13 7 1. 87 2414.00 2400 20 3.77E-03 **** 1.54E+OO 0 1238.48 26 7 2.23 2477.66 2472 10 7.42E-03 54.4 1.51E+OO T 0 1258.60 11. 11 1. 01 2517.96 2512 9 3.12E-03 **** l.49E+OO 0 1288.43 15 7 2.88 2577.68 2572 13 4.17E-03 87.6 l.46E+OO 0 1334.20 17 6 1.19 2669.34 2664 12 4.73E-03 75.1 l.42E+OO 0 1360.53 5 4 0.55 2722. 08 2718 6 1.53E-03 **** 1.39E+OO 0 1377.89 21 5 1. 34 2756.85 2751 11 6.08E-03 59.3 1.38E+OO 0 1416.25' 6 8 0.55 2833.68 2823 12 l.74E-03 **** 1.35E+OO 0 1588.20 11 6 4.32 3178.14 3171 12 3.06E-03 **** 1.22E+OO 0 1630.78 11 0 0.83 3263.45 3257 11 3.06E-03 60.3 1.19E+OO 0 1729.10 13 3 o. 72 3460.47 3453 13 3.67E-03 78.0 l.13E+OO Flags: "T" = Tentatively associated _Page 3025 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:05:47.73 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l *
Acquisition date 3-0CT-2016 08:02:32 Sensitivity 3.000 *
Detector ID. GAM20 Energy tolerance: 1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.99 Half life ratio : ***** *
Sample date 10-DEC-2015 13:25:00 Nuclide Library : SOLID *
Sample ID G405235006 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5634E+02 GRAM *
Wet wt corr 1.000DO Wet Weight 0.00000 *
Dry Weight : 0.00000 ** ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File . : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 C0-57 Y-91 CD-109 SN-126 PM-147 EU-155 TL-208 BI-212 PB-212 BI-214 PB-214 RN-'222 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Le' (pCi/GRAM l.384E-01 5.004E-02 3.745E-02 2.941E+02 8.436E-01 5. 411E-02 5.496E+02 7.715E-02 2.397E-02 3.053E-01 3. 968E-02 5.156E-02 4.948E-02 5.156E-02 5.156E-02 6.554E--,02 6.554E-02 3.968E-02 3. 8.82E-01 5.154E-02 2.781E-01 6.554E-02. 7.400E-01 5.154E-02 1.435E-01 7.400E-01 2.085E-02 ----Non-Identified Nuelides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3026 of 5809 Le (pCi/GRAM 7.828E+OO 2.373E-02 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48

CR-51 C0-56 MN-56 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110.M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3027 of 5809 2.652E-01 O.OOOE+OO 0.000E+OO 2.781E-01 O.OOOE+OO 3.229E-01 3.818E+OO 3.097E-02 1.072E-01 1. 628E+OO 4.638E+OO O.OOOE+OO l.403E-01 O.OOOE+OO O.OOOE+OO 4.866E-01 5.311E+OO 5.493E-01 O.OOOE+OO 9 .115E-02 2.700E-02 5.977E-01 1. 670E+OO 1.124E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.551E-02 3.477E-02 3.613E+OO 3.807E-01 3.807E-01 1. 621E-02 6.085E-02 l.624E-01 o*. OOOE+OO 0.000E+OO 1. 071E-01 l.548E+00 7.840E-02 2.040E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.246E-02 O.OOOE+OO 4.526E-02 1.149E-01 O.OOOE+OO O.OOOE+OO 3.438E-02 3.632E-02 8.445E-02 O.OOOE+OO O.OOOE+OO 1. 757E+Ol O.OOOE+OO 2.854E-01 3.526E-02 3.048E+OO 3.151E-02 O.OOOE+OO O.OOOE+OO 1. 781E-02 7.175E-02 l.327E-01 5.823E-02 1.050E+OO 4.209E-02 1.044E+Ol l.689E-01 6.752E-02 1.971E-02 2.999E+OO FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT.IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF" SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 RA-224 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3028 of 5809 8.279E-01 l.634E+OO 2. ll 7E+Ol 7.674E+Ol 2.995E-01 1.817E+OO 3.182E-02 l.398E+OO 3.789E-01 4.488E-01 2.8l8E-01 4.637E-01 6.245E-01 l.828E-01 1.828E-01 4.637E-01 4.395E-02 2.327E-01 3.770E+OO 4.395E-02 O.OOOE+OO l.635E-01 2:so9E+o2 8.159E-02 5.328E-02 6.378E-02 4.862E-02 2.425E-02 3,_ 038E-02 9.823E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:05:53.20 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l *
Acquisition date 3-0CT-2016 08:02:32 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.99 Half life ratio : ***** *
Sample date 10-DEC-2015 13:25:00 Nuclide Library : SOLiD *
Sample ID G405235006 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity 1.5634E+02 GRAM *
Quantity Err(%) 1.2792E-03 % *
Wet wt corr . 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date '30-JUN-2016 06:52:39 Eff. Geometry : CAN' *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma). K-40 l.597E+Ol l.661E+OO l.661E+OO MN-54 8.395E-02 8.lOlE-02 8.lOlE-02 C0-57 6.333E-02 6.862E-02 6.862E-02 Y-91 6.675E+02 5.236E+02 5.236E+02 CD-109 1.322E+OO 1. 865E+OO 1. 865E+OO SN-126 8.453E-02 l.191E-01 l.191E-01 PM-147 1.104E+03 l .196E+03 1.196E+03 EU-155 1.850E-01 2.020E-01 2.020E-01 TL-208 3.661E-01 8.776E-02 8.776E-02 BI-212 1. 064E+OO 5.944E-01 5.944E-01 PB-212 1.105E+OO l.515E-01 1.515E-'-01 BI-214 7. 696E-01 1. 710E-01 1. 710E-01 PB-214 1.080E+OO 1. 761E-01 1. 761E-01 RN-222 7.696E-01 1.710E-01 1. 710E-01 RA-22 6 7.696E-01 1. 710E-01 l.710E-01 AC-228 1.408E+OO 3.072E-01 3. 072E-01 RA-228 1.408E+OO 3. 072E-01 3. 072E-01 TH-228 1.105E+OO l.515E-01 l.515E-01 TH-229 7.367E-02 4.123E-01 4.123E-01 TH-230 7.694E-01 1. 709E-01 1.709E-01 PA-231 1.169E+OO 7. 712E-Ol
7. 712E-01 TH-232 l.408E+OO 3.072E-01 3.072E-01 TH-234 l.305E-02 2.015E+OO 2.015E+OO U-234 7.694E-01 1.709E-01 l.709E,-01 U-235 -2 .'283E-02 l.684E-01 l.684E-01 U-238 1.305E-02 2 .. 015E+OO 2.015E+OO ANH-511 2.603E-02 7. 313E-02 7.313E-02 Non-Identified Nuclides Key-Line Activity
K. L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1.023E+OO 8.808E+OO 8.820E+OO NOT IDENT. NA-22 -2.495E-02 3.359E-02 3.542E-02 NOT IDENT. NA-24 *1. 000E+41 3.151E+41 0.000E+OO SHORT HLIF *Page 3029 of 5809 AL-26 O.OOOE+OO O.OOOE+OO O.OOOE+OO NOT IDENT. SC-46 l.332E-01 2.928E-01 2.989E-01 FAIL ABUN V-48 -7.895E+02 l.052E+04 l.053E+04 SHORT HLIF CR-51 -1.589E+02 3.022E+02 3.105E+02 SHORT HLIF C0-56 1.650E-01 2.953E-01 3.045E-01 FAIL ABUN MN-56 l.000E+41 1. 790E+41 O.OOOE+OO SHORT HLIF C0-58 -3.271E-01 4.578E-01 4.809E-01 NOT IDENT. FE-59 4.920E+OO 3.183E+OO 3.880E+OO NOT IDENT. C0-60 4.019E-02 2.82iE-02 3.353E-02 NOT IDENT. ZN-65 -3.067E-02 1.335E-01 l.342E-01 NOT IDENT. GE-68 -2.497E-01 l.905E+OO 1.909E+OO NOT IDENT. AS-73 4.709E-02 5.122E+OO 5.122E+OO NOT IDENT. AS-74 5.866E+02 4.730E+03 4.738E+03 SHORT HLIF SE-75 -6.351E-02 l.681E-01 l.705E-01 FAIL ABUN BR-77 1.092E+38 9.390E+38 O.OOOE+OO SHORT HLIF SR-82 -3.489E+02 6.252E+02 6.447E+02 SHORT HLIF RB-83 3.126E-02 5.566E-01 5.568E-01 NOT IDENT. KR-85 1.789E+OO 6.540E+OO 6.590E+OO NOT IDENT. SR-85 1.852E-01 6.763E-01 6.815E-01 NOT IDENT. RB-86 -8.693E+03 2.298E+04 2. 331E+04 SHORT HLIF Y-88 4.852E-02 7.669E-02 7.975E-02 NOT IDENT. NB-94 2.643E-02 2.818E-02 3.059E-02 NOT IDENT. NB-95 -4.482E-01 7.827E-01 8.083E-01 NOT IDENT. NB-95M -7.774E-02 2 .'027E+OO 2.028E+OO NOT IDENT. ZR-95 -1.106E-01 1. 356E+OO 1. 356E+OO NOT IDENT. NB-97 -1.000E+41 l.063E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.758E+42 O.OOOE+OO SHORT HLIF M0-99 -2.556E+31 9.018E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 4.493E+41 O.OOOE+OO SHORT HLIF RH-101 1.017E-02 3 .111E-02 3.145E-02 NOT IDENT. RH-102 -1. 268E-02 . 4.315E-02 4.353E-02 NOT IDENT. RU-103 -8.177E-01 4.273E+OO 4.289E+00 FAIL ABUN RH-106 2.870E-01 4.009E-01 4.212E-01 NOT IDENT. RU-106 2.870E-01 4.009E-01 4.212E-01 NOT IDENT. AG-108M -2.404E-02 2.191E-02 2.444E-02 NOT IDENT. AG-110M -2.067E-02 7.810E-02 7.866E-02 NOT IDENT. SN-113 -1. 728E-01 2.029E-01 2.173E-01 NOT IDENT. CD-115 -2.604E+38 l.464E+39 O.OOOE+OO SHORT HLIF SN-117M -6.846E+03 8.675E+04 8. 681E+04 SHORT HLIF TE-123M 7.504E-02 1.195E-01 l.242E-01 NOT IDENT. SB-l24 1.068E+OO 1.510E+OO 1.585E+OO NOT IDENT. SB-125 5.590E-02 8.205E-02 8.583E-02 FAIL"ABUN TE-125M 3.300E+Ol 2. 511E+02 2.516E+02 NOT IDENT. I-126 2.407E+04 6.554E+05 6.555E+05 SHORT HLIF SB-126 -2.921E+05 9.508E+05 9.598E+05 SHORT HLIF SB-127 -1.057E+21 l.301E+22 O.OOOE+OO SHORT HLIF I-131 2.058E+09 3.419E+09 3.542E+09 SHORT HLIF I-132 -l;OOOE+41 1.839E+42 O.OOOE+OO SHORT HLIF TE-132 1. 221E+26 2.263E+26 O.OOOE+OO SHORT HLIF BA-133 -l.606E-03 3.919E-02 3.919E-02 NOT IDENT. I-133 -1.000E+41 l.045E+43 O.OOOE+OO SHORT HLIF CS-134 1.051E-01 5.052E-02 6.926E-02 FAIL ABUN CS-135 6.807E-02 1.327E-01 l.362E-01 NOT IDENT. I-135 -l.OOOE+41 2.090E+42 O.OOOE+OO SHORT HLIF CS-136 -4.409E+03 2.078E+05 2.078E+05 SHORT HLIF BA-137M 3.260E-02 3.659E-02 3.943E-02 NOT IDENT. CS-137 3.443E-02 3.866E-02 4.166E-02 NOT IDENT. CE-139 3.492E-02 9.656E-02 9.784E-02 NOT IDENT. BA-140 2.207E+04 8. 021E+05 8.022E+05 SHORT HLIF LA-140 -5. 841E+04 2.277E+05 2.292E+05 SHORT HLIF CE-141 -2.549E+OO 2.069E+Ol 2.072E+Ol NOT IDENT. *cE-143 l.000E+41 4. 561E+40 O.OOOE+OO SHORT HLIF CE-144 8.658E-02 3.247E-01 3.270E-01 NOT IDENT. PM-144 9.297E-03 3.995E-02 4.017E-02 NOT IDENT. PR-144 7.690E-01 3.460E+OO 3.477E+OO NOT IDENT. PM-146 -4. 61°3E-03 3.653E-02 3.659E-02 NOT IDENT. ND-147 -1.414E+07 2.539E+07 2.618E+07 SHORT HLIF PM-149 -1.459E+40 1. 964E+40 *o.OOOE+OO SHORT HLIF EU-150 -1. 37 4E-02 2.403E-02 2.481E-02 FAIL ABUN EU-152 2.263E-02 8.125E-02 8.189E-02 FAIL ABUN GD-153 3.451E-02 l.485E-01 1.493E-01 NOT IDENT. EU-154 -5.181E-02 8.033E-02 8.365E-02 NOT IDENT. TB-160 -l.190E+OO l.532E+00 l.623E+00 FAIL ABUN H0-166M 2.688E-02 4.533E-02 4.692E-02 NOT IDENT. TM-171 -*1. 661E+OO 1.166E+Ol l.168E+Ol NOT IDENT. HF-172 2.763E-02 2.097E-01 2.lOlE-01 FAIL ABUN LU-172 8.659E-02 6.902E-02 7.930E-02 FAIL ABUN LU-176 3.988E-03 2.147E-02 2.154E-02 FAIL ABUN Page 3030 of 5809 HF-181 1.079E+00 3.284E+OO 3.320E+OO NOT IDENT. TA-182 7.436E-01 8.532E-01 9.167E-01 FAIL ABUN RE-183 -2.026E-01 1. 829E+OO 1.832E+OO NOT IDENT. RE-184 -2.740E+00 2.614E+Ol 2.617E+Ol NOT IDENT. W-188 -4.717E+01 l.005E+02 1.027E+02 FAIL ABUN IR-192 -1.267E-01 3.466E-01 3. 513E-01 FAIL ABUN HG-203 -7.852E-02 2.006E+OO 2.007E+OO FAIL ABUN BI-207 -1.900E-02 3. 968E-02 4.060E-02 FAIL ABUN PB-210 -1.283E+OO 1. 621E+OO 1. 721E+OO NOT IDENT. BI-211 2.974E+OO 4.874E-01 l.426E+OO FAIL ABUN PB-211 3.265E-02 5.032E-01 5.034E-01 NOT IDENT. RN-219 8.218E-02 3.089E-01 3. lllE-01 FAIL ABUN RA-223 2.836E-01 4.882E-01 5.047E-01 FAIL ABUN RA-224 1.994E+OO 8.856E-01 1. 262E+OO FAIL ABUN AC-227 1.949E-02 1.984E-01 1. 986E-01 FAIL ABUN TH-227 1.949E-02 1.984E-01 1. 986E-01 FAIL ABUN TH-231 2.836E-01 4.882E-01 5.047E-01 FAIL ABUN PA-233 -2.120E-02 5.084E-02 5.173E-02 °FAIL ABUN PA-234 1. 09.8E-01 2.776E-01 2.820E-01 NOT IDENT. PA-234M 2.820E+OO 3. 811E+OO 4.018E+OO NOT IDENT. NP-237 -2.120E-02° 5.084E-02 5.173E-02 FAIL ABUN NP-238 -2.635E+40 2.010E+41 O.OOOE+OO SHORT HLIF NP-239 -1.-976E-01 2.073E-Oi 2.257E-01 FAIL ABUN PU-239 4.764E+02 3.868E+02 4.424E+02 FAIL ABUN AM-241 2.954E-02 9.558E-02 9. 651E-02 NOT IDENT. AM-243 8.165E-02 8. 071E-02 8.870E-02 FAIL ABUN CM-243 l.654E-02 7.733E-02 7.769E-02 NOT IDENT. BK-2'47 -1. 296E-02 6.107E-02 6'.135E-02 FAIL ABUN CM-247 -1.052E-02 2.873E-02 2. 911E-02 NOT IDENT. CF-249 l.569E-02 3.259E-02 3.335E-02 NOT IDENT. CF-251 6.862E-02 1.009E-01 l.055E-01 NOT IDENT. Page 3031 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 95.6707 87.09 127.8269 136.47 90.6452 45.60 88.5982 87.57 127.9089 140.51 0.0000 46.54 95.1794 88.03 127.9884 143.76 91.3067 49.72 0.0000 88.34 114. 3227 144.24 88.9131 51. 35 100. 3728 88.47 114.3421 145.44 81. 7012 51. 87 99.3889 89. 96 97.7650 152.43 84.7055 52.39 89.7516 1093.63 97.8522 153.25 0.0000 52.97 87.6816 91.11 0.0000 323.87 92.2256 53.44 96.4237 92.59 98.1009 156.02 o. oo*o o 54.07 90.0252 93.35 98.1973 158.56 0.0000 57.36 0.0000 94.56 87.5926 159.00 69.1694 57.53 90.5761 94.65 87.6031 162.33 68.1407 57.98 97.1988 94.67 87.6054 162.66 0.0000 59.27 94.8598 94.87 87.6274 163.33 70.6829 59.32 94.8677 97.43 84.4413 165.86 68.3581 59.54 94.9031 98.43 85.7053 176.31 75.2582 60.96 98.0573 98.44 85.7065 176.60 0.0000 61.17 98.0917 99.53 86.9820 177.52 75.3369 62.93 114.5288 100 .11 70.7961 181.07 0.0000 63.29 114. 5964 102.03 69.7998 181.52 69.2938 63.58 114. 6506 103.18 68.3440 184.41 75.7764 64.28 114.7809 103.37 59.0379 143.76 74.1739 66.73 115.2322 105.21 79.4105 193.51 80.5873 67.24 143.4160 105.31 79.4198 197.03 73.1591 125.81 134.6384 106.12 79.4966 198.01 61. 2971 67.75 134.6532 106.47 79.5298 201.83 64.0450 69.67 129.1194 109.28 84.4868 203.43 67. 9726 70.83 141.2427 111. 00 94.0619 205.31 71. 9260 72.81 118.5529 111.76 0.0000 210.85 77.3932 72.87 118.5634 114. 06 96. 7519 215.65 69.0454 74.66 118.8796 116. 30 0.0000 222 .11 74.5816 74.82 118.9079 116.74 91.1279 227.09 76.5954 74.97 118.9338 119. 76 71. 24 73 227.38 76.6115 77 .11 119.3066 121.12 63.0289 228.16 0.0000 78.74 102.2885 121. 22 63.0358 228.18 63.5898 79.69 100.9205 121. 78 77.7523 116.74 63.5898 80.12 85.9099 122.06 88.8866 235.69 61.7442 80.19 0.0000 122.92 73.0823 235. 96 61.7556 80.57 83.7022 123.07 77.8615 238.63 .65.8218 81. 00 90.5438 265.00 79.5029 238.98 0.0000 81. 07 104.1359 125.81 74.9039 240.99 79.1171 81.75 83. 8411 127.23 75.0167 242.00 62.0188 83.79 93.9259 127.91 76.6682 244.70 37.0166 84.00 84.8608 129.30 78.3799 252.40 0.0000 85.43 93.3780 131.20 88.1520 252.80 46.0850 86.55 93.5194 133.02 83.0999 254.15 0.0000 86.79 93.5494 133.52 84.3480 256.23 57.7399 86.94 127.8013 136. 00 88.1857 260.90 0.0000 Page 3032 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.2377 355.39 o.booo 584.27 22. 9722 264.80 48.2421 356.01 35.3600 595.83 0.0000 265.00 44.2279 364.49 0.0000 427.87 23 .1127 2 68. 22 51.0358 366.42 0.0000 602.52 0.0000 269.46 49.2854 372.51 35.1934 604.72 23.6737 270.03 49.3033 375.05 36.1925 607.14 28.4337 271.23 49.3413 377.52 26.7023 609.32 28.4568 273.65 0.0000 356.01 26.7889 610.33 22.1416 276.40 47.5256 388.16 33.5595 614.28 31. 6760 277.37 51. 3373 388.63 0.0000 618.01 16.9167 277.60 49.5439 391.69 46.1064 620.36 29.6304 278.00 45. 0511 264.66 34.7344 621. 93 14.8232 279.20 55.0045 401.81 29.9272 630.19 0.0000 279.54 52.3100 402.40 35.7301 631.29 16.9980 279.70 55.9239 404.85 27.0715 633.25 12.7573 280.46 60.4625 410.95 35.8799 634.78 0.0000 283.69 43.4043 413.71 33.0150 635.95 22.3467 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 53.4087 423.72 0.0000 645.85 20.2896 285.90 0.0000 427.09 26.3859 657.76 22.5193 287.50 41.6950 427.87 22.4848 657.90 0.0000 290.67 51.7676 433.94 34.3143 661. 66 24.6967 293.27 0.0000 439.40 24.7688 664.57 0.0000 351. 93 28.6879 453.88 29.6832 666.33 0.0000 295. 96 30.0681 463.37 24.8418 666.50 0.0000 879.38 27.3779 468.07 23.8979 667. 71 o*. 0000 299.98. 34.2514 473.00 0.0000 677.62 16.1951 300.09 34.2537 475.06 16.9799 685.70 0.0000 300.13 34.2545 476.78 20.9910 695.00 0.0000 301.36 34.2796 477.60 19.9984 696. 49 14.1251 302.85 39.7998 482.18 21. 0402 696. 51 14.1251 256.23 42. 5872 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 19.5630 306.78 47.6889 497.08 23.1919 697.49 20.6514 308.46 54.1626 505.52 21. 2508 702.65 17.4199 311. 90 49.6736 507.63 0.0000 706.68 19.6238 316.51 38.7393 511. 00 29. 4136 711. 68 14 .1960 319.41 o. o*ooo 514. 00 . 27.4197 720.70 0.0000 320.08 0.0000 514.00 27.4197 721.93 0.0000 321.04 44.3896 520.40 25.4557 722.78 27.9467 323.87 37.0516 520.69 0.0000 722.91 27.9477 325.23 56.5471 522.65 0.0000 723.31 23.0192 328.76 0.0000 527.90 0.0000 724 .19 11. 5130 333.37 51.6857 528.26 26.5586 727.33 16.4636 333.97 48.9090 529.59 20.4411 733.00 19.7922 334.37 53.1128 529.87 0.0000 735.93 13.2075 338.28 40.1550 531.02 0.0000 333.97 17.6185 338.32 40.1559 537.26 0.0000 739.50 0.0000 311. 90 51.8912 546.56 0.0000 747.24 19.8823 340.48 51.8912 552.55 10.8303 748.06 15.4680 340.55 0.0000 563.25 18.6445 752.31 25.4454 344.28 37.1024 569.33 24.9180 753.82 0.0000 345.93 43.8883 946.00 30 .1104 756.73 23.2653 351.06 37.6164 569.70 30.1128 756.80 23.2661 351. 93 37.6343 583.19 22. 9623 884.68 16.6559 Page 3033 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.8861 1274.44 12.4457 1620.50 6.0806 7 66 .. 42 27.7812 1001.03 12.4606 1621.92 4.0547 766.84 18.8933 1002.74 13.3566 1678.03 0.0000 772.60. 0.0000 1004.73 24.0535 1690.97 2.0516 776*. 52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.0000 778.90 11.1552 1028.54 0.0000 1063.66 3 .1183 783.70 0.0000 1037.84 10.7798 1771.35 3 .1190 785.37 15.0892 1038.76 0.0000 1791.20 0.0000 792.07 10.0800 631. 29 14.4043 1808.65 0.0000 794.95 13.4517 1048.07 0.0000 1810.72 0.0000 795.86 18.5014 1049.04 11. 7098 1836.06 0.0000 810.06 19.1430 1050.41 12.6149 810.29 22.5228 1063.66 17.1758 344.28 20.2712 1077.00 0.0000 810.76 18.0208 1077.34 14.5117 815.77 0.0000 1085.87 8. 7252 1048.07 0.0000 1093.63 7.2842 832.01 13.6006 1099.45 0.0000 834.85 21. 5520 1112. 07 8.7791 835. 71 21. 557 5 1112. 84 14.6348 836.80 0.0000 1115. 54 13.5985 846.75 0.0000 1120.29 11. 7281 846.77 6.8293 112.0: 55 16.1272 856.80 0.0000 1221. 41 19.2466 860.56 7.9992 *1129.67 13.7741 871. 09 12.6077 1131.51 0.0000 873.19 11. 4685 1147.95 0.0000 875.33 0.0000 1173.23 20.4048 879.38 18.3815 1177.95 18.5693 880.51 14.9397 1189.05 17.6849 883.24 6.9004 1204.77 9.3402 884.68 13.8066 1221. 41 14.0616 889.28 10.3682 1231.02 15.9697 894.76 17.3065 1235.36 0.0000 898.04 16.1676 1238.28 15.0537 900. 72 13.8682 1260.41 0.0000 903.28 17.3474 1271. 87 7.5815 911.20 8 .112 8 1274.44 11. 3782 912.08 8 .1148 1274.54 12. 3264 923.98 0.0000 1291. 59 7.6128 926.50 12.8020 1298.22 0.0000 929 .11 12.8110 1312 .11 0.0000 937.49 20.1348 1332.49 1.5355 944.13 0.0000 1362.66 0.0000 946.00 15.7934 1365.19 11. 5928 949.00 17.5623 1368.63 0.0000 667. 71 0.0000 1384.29 8. 7275 962.31 7.0496 1408.01 6.2355 964.08 15 .1130 1457.56 0.0000 966 .17 15.1214 1460.82 2.9528 911. 20 15.1324 1489.16 3.9583 968.97 15.1324 1505.03 12.9024 983.53 0.0000 1584.12 6.4441 984.45 0.0000 1596.21 0.0000 Page 3034 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:06:26.57 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Confi.guration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277
Background date : Z-OCT-2016 11:01:57. Sample date 10-DEC-2015 13:55:00 Acquisition date : 3-0CT-2016 08:02:54. Sample ID G405235007 Sample quantity 1.52523E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.63 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID
1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 . ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 0 5 5 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 7 7 0 0 0 0 0 0 0 0 0 0 Energy 62.99* 75.19 77.47 87.49 93.12* 94.77 129.53 186.37* 209.43 239.11* 242 .11 270.47 295.71* 300.59 338.59 352.25* 464.99 511.31* 534.57 583.92* 609.94* 662.17 707.28 710.32 720.76 728.15* 797.49 803.54* 812.25 816.56 861.47* 911.71* 969.39 996.21 Page 3035 of 5809
BACKGROUND CORRECTED SAMPLE PEAK REPORT* Area 45 109 181 38 46 32 31 139 71 381 93 46 168 24 114 255 14 46 24 139 165 91 11 27 14 35 23 19 13 9 20 103 56 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 145 157 135 136 153 84 117 169 76 91 90 61 74 52 63 67 51 53 36 38 38 55 9 15 7 27 26 11 11 15 18 . 8 44 13 1. 34 1. 29 1.14 1. 68 1. 93 1.26 1. 78 1. 23 1. 25 1. 23 1. 62 1. 08 1. 34 1. 45 1. 03 1.13 0.67 1. 96 3.98 1.19 1. 42 1. 77 1. 96 2.00 3.40 0.95 1. 86 0.66 3. 67 1. 70 1. 45 1. 62 1. 73 1.17 127.20 151. 59 156.14 176.20 187.46 190.76 260.27 373. 96 420.08 479.43 485.43 542.17 592.64 602.40 678.40 705.72 931.20 1023.86 1070.37 1169. 08 1221.11 1325.59 1415.81 1421. 88 1442.77 1457.55 1596.23 1608.33 1625.76 1634.38 1724.20 1824.69 1940.04 1993.69 123 147 147 174 184 184 256 368 416 474 537 588 599 673 699 925 1017 1064 1162 1215 1319 1413 1413 1438 1450 1586 1604 1617 1630 1719 1819 1933 1989 9 1. 25E-02 51. 6 13 3.02E-02 23.0 9.54E-01 13 5.02E-02 13.1 6 1. 05E-02 51. 5 10 1.28E-02 51.7 4.56E+OO 10 8.77E-03 57.2 8 8.50E-03 64.0 13 3.85E-02 21.6 8 1. 97E-02 24. 4 17 1.06E-01 6.6 1.54E+OO 17 2.57E-02 25.5 10 1,27E-02 35.6 11 4.66E-02 12.7 8 6.67E-03 55.9 11 3.15E-02 16.5 12 7.08E-02 9.0 11 3.97E-03101.1 14 1. 28E-02 41. 6 13 6.57E-03 56.1 14 3.85E-02 12.8 14 4.59E-02 11.3 13 2.52E-02 19.9 25 3.12E-03 48.2 1.37E+OO 25 7.41E-03 35.6 10 3.86E-03 45.4 12 9.78E-03 34.8 14 6.26E-03 53.8 11 5.25E-03 44.7 13 3.52E-03 64.3 8 2.62E-03 76.6 10 5.62E-03 45.5* 11 2.87E-02 11.5 17 1.56E-02 30.9 12 3.43E-03 63.2 Peak Search Report (continued) Page : '2 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1049.83 19 6 3.87 2100.93 2093 14 5.20E-03 37.6 36 0 1121.18* 38 14 1. 72 2243.64 2238 10 l.05E-02 25.4 37 0 1190. 02 9 7 0.61 2381.31 2378 6 2.57E-03 56.4 38 0 1227.61 16 12 3.52 2456.49 2449 15 4.58E-03 50.8 39 0 1234.03 27 5 2.60 2469.34 2464 10 7.53E-03 24. 6 . 40 0 1239.00 23 6 1. 24 2479.29 2475 11 6.25E-03 29.2 41 0 1245.45 17 3 3. 62 2492.19 2486 11 4.79E-03 30.4 42 0 1250.95 17 15 3.83 2503.18 2497 14 4.77E-03 52.4 43 0 1333.81 15 3 4.00 2668.91 2663 11 4.25E-03 33.0 44 0 1337.86 6 0 1. 50 2677.00 2674 6 1. 67E-03 40.8 45 0 1461.22* 389 3 1. 96 2923.73 2917 14 l.08E-01 5.2 46 0 1544.74 9 2 0.52 3090.77 3086 8 2.58E-03 41. 8 47 0 1765.38* 23 0 1. 50 .3532. 08 3527 10 6.40E-03 22.4 Flag: "*" = Peak area was modified by background subtraction Page 3036 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:06:28 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 13:55:00 G405235007 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:02:54 152.52 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA32 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74. 82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3037 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.63 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.119E+OO 1.552E+Ol 1.552E+Ol 10.42 OK C0-58 810.76 99.45* l.793E+OO 3.603E-02 6.633E-01 128.52 OK CD-109 88.03 3.70* 4.577E+OO. 2.402E-01 3.758E-01 612. 50 OK SN-126 64.28 9.60 2.075E+OO l.451E+OO 1.451E+OO 103.12 OK 86.94 8.90 4.577E+OO 9.988E-02 9.988E-02 612.50 OK 87.57 37.00* 4.577E+OO 2.402E-02 2.402E-02 612.50 OK BA-137M 661.66 89.90* 2.104E+OO 2.484E-01 2.531E-01 39.80 OK CS-137 661.66 85.10* 2.104E+OO 2.624E-01 2. 674E-,01 39.80 OK TL-208 277.37 6.60 4.277E+OO Line Not Found Absent 583.19 85.00* 2.325E+OO 3.684E-01 3.684E-01 25.69 OK 860.56 12.50 1.712E+OO 4.765E-01 4.765E-01 90. 96 OK PB-212 74.82 10.28 3.461E+OO 1.229E+OO 1.229E+OO 73.91 OK 77 .11 17.10 3.693E+OO 1. 813E+OO 1. 813E+OO . 26. 24 OK 238.63 43.60* 4.786E+OO 1.046E+OO 1.046E+OO 13.16 OK 300.09 3.30 4. OllE+OO . 1.017E+OO 1.017E+00 111. 80 OK BI-214 609.32 45.49* 2.246E+00 8.454E-01 8.457E-01 22.62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 OK PB-214 74.82 5.80 3.423E+OO Line Not Found <<INT Reject 77 .11 9.70 3.693E+OO 3 .196E+OO 3.197E+OO 26.24 OK 87.09 3.41 4.545E+OO Line Not Found <<INT Reject 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 18.42 4.064E+OO 1.258E+OO 1.258E+OO 25.48 OK 351.93 35.60* 3.521E+OO 1.122E+OO 1.122E+OO 18.06 OK RN-222 609.32 45.49*. 2.246E+OO 8.454E-01 8.457E-01 22.62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 OK RA-224 240.99 4.10* 4.743E+OO 4.991E-01 4.991E-01 300.41 OK RA-226 609.32 45.49* 2.246E+OO 8.454E-01 8.457E-01 22. 62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 OK AC-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.639E+OO 1.535E+OO 1.535E+OO 32.99 *OK 794.95 4.25 1.823E+OO *-----Line Not Found Absent 835.71 1. 61 1. 753E+OO Line Not Found Absent 911.20 25.80* 1.638E+OO l.226E+00 1.226E+OO 22.98 OK 968. 97 15.80 1. 561E+OO 1.130E+OO l.130E+OO 61. 71 OK RA-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11.27 3.639E+OO 1. 535E+OO 1.535E+OO 32.99 OK 794.95 4.25 1.823E+OO Line Not Found Absent 835. 71 1. 61 1. 753E+OO Line Not Found Absent 911.20 25.80* 1.638E+OO l.226E+OO 1.226E+OO 22.98 OK 968. 97 15.80 1. 561E+OO 1.130E+OO 1.130E+OO 61. 71 OK TH-228 74.82 10.28 3.461E+00 1. 229E+OO 1.229E+OO 73.91 OK 77 .11 17.10 3.693E+OO 1.813E+00 1.813E+OO 26.24 OK 238.63 43.60* 4.786E+00 1.046E+OO 1.046E+OO 13.16 OK 300.09 3.30 4. OllE+OO 1. 017E+00 l.017E+OO 111. 80 OK TH-230 609.32 45.49* 2.246E+OO 8.454E-01 8.455E-01 22.62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.904E-01 50.87 OK Page 3038 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.30 9.459E-01 7.405E-01 7.405E-01 44.75 OK PA-231 283.69 1. 70 4.201E+OO Line Not Found* Absent 301.36 5.35* 4. OllE+OO 6.271E-01 6.271E-01 111.80 OK TH-232 105.21 1.10 5:586E+OO Line Not Found Absent 338.32 11. 27 3.639E+OO 1.535E+OO l.535E+OO 32.99 OK 835.71 1. 61 1. 753E+OO Line Not Found Absent 911. 20 25.80* 1.638E+OO 1. 22 6E+OO l.226E+OO 22.98 OK 968.97 15.80 1.561E+OO 1.130E+OO 1.130E+OO 61. 71 OK TH-234 63.29 3.70* 2.075E+OO 3.764E+OO

3. 764E+OO 103.12 OK 92.59 4.23 4.971E+OO 1.370E+OO 1.370E+OO 103.36 OK U-234 609.32 45.49* 2.246E+OO 8.454E-01 8.454E-01 22.62 OK 1120. 29 14.92 1. 392E+OO 8.904E-01 8.904E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.405E-01 44.75 OK U-238 63.29 3.70* 2.075E+OO 3.764E+OO 3.764E+OO 103.12 OK 92.59 4.23 4.971E+OO 1.370E+OO 1.370E+OO 103.36 OK AM-243 43.53 5.90 1. 701E-01 Line Not Found Ab.sent 74.66 67.20* 3.461E+OO 1.880E-01 1. 880E-01 73.91 OK ANH-511 511. 00 100.00* 2.588E+OO 9.466E-02 9.466E-02 83.19 OK Flag: "*" Key line Page 3039 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:06:29.83 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l *
Acquisition date 3-0CT-2016 08:02:54 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
Sample date 10-DEC-201_5 13: 55: 00 Analyst initials: MXRl *
Sample ID G405235007 Sample Quantity 1.5252E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATI.ON * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM K-40 1.552E+Ol 1.585E+OO 5.415E-01 C0-58 6.633E-01 8.354E-01 8.694E-01 CD-109 3.758E-01 2.256E+OO 2.825E+OO SN-126 2.402E-02 l.442E-01 l.669E-01 BA-137M 2. 531E-01 9.871E-02 7.217E-02 CS-137 2.674E-01 l.043E-01 7.624E-02 TL-208 3.684E-01 9.275E-02 5.456E-02 PB-212 1.046E+OO l.349E-01 1.025E-01 BI-214 8.457E-01 1. 875E-01 1.254E-01 PB-214 1.122E+OO 1.986E-01 l.280E-01 RN-222 8.457E-01 1. 875E-01 1.254E-01 RA-224 4.991E-01 1.470E+OO 1.098E+00 RA-226 8.457E-01 1. 875E-01 1.254E-01 AC-228 1.226E+OO 2.762E-01 2.634E-01 RA-228 l.226E+OO 2.762E-01 2.634E-01 TH-228 1.046E+OO 1.349E-01 l.025E-01 TH-230 8.455E-01 1. 874E-01 1.254E-01 PA-231 6. 271E-01 6.871E-01 8.744E-01 TH-232 1. 226E+OO 2.762E-01 2.634E-01 TH-234 3.764E+OO 3.804E+OO 3.193E+OO U-234 8.454E-01 l.874E-01 l.254E-01 U-238 3.764E+OO 3.804E+OO 3.193E+OO AM-243 1.880E-01 1. 362E-01 1.165E-01 ANH-511 9.466E-02 7. 717E-02 4.992E-02 Non-Identified Nuclides Key-Line Activity K .. L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 2.468E+OO 1. 18 OE+Ol 2.337E+Ol NOT IDENT. NA-22 -l.801E-02 4.318E-02 8.088E-02 NOT IDENT. NA-24 O.OOOE+OO l.523E+41 O.OOOE+OO SHORT HLIF AL-26 2.599E-02 3.510E-02 8.479E-02 NOT IDENT. SC-46 -7.774E-02 4.446E-01 8.057E-01 FAIL ABUN V-48 O.OOOE+OO 1.266E+04 O.OOOE+OO SHORT HLIF Page 3040 of 5809 CR-51 0.000E+OO 4.162E+02 O.OOOE+OO SHORT HLIF MN-54 8.976E-03 6.462E-02 1.236E-01 NOT IDENT. C0-56 -1.060E-02 4.543E-01 8.620E-01 FAIL ABUN MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 3.147E-02 5.427E-02 1. 030E--01 NOT IDENT. FE-59 -3.185E+OO 5.999E+OO l. llOE+Ol NOT IDENT. C0-60 6.774E-02 4.386E-02 8.395E-02 FAIL ABUN ZN-65 -3.150E-02 2.052E-01 3.480E-01 NOT IDENT. GE-68 1. 743E+OO 2.387E+00 5.269E+00 NOT IDENT. AS-73 -3.993E-01 1.505E+Ol 2.858E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.810E+03 O.OOOE+OO SHORT HLIF SE-75 -3.559E-02 2.054E-01 3.949E-01 NOT IDENT. BR-77 O.OOOE+OO l.326E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.736E+02 O.OOOE+OO SHORT HLlF_ RB-S3 -5.887E-01 6.134E-01 l.020E+OO NOT IDENT. KR-85 5. 211E+OO 8.053E+OO 1.500E+Ol NOT IDENT. SR-85 5.350E-01 8.321E-01 1.550E+OO NOT IDENT. RB-86 O.OOOE+OO 2.647E+04 O.OOOE+OO SHORT HLIF Y-88 l.131E-01 l.280E-01 4.065E-01 NOT IDENT. Y-91 -1.149E+Ol 5.321E+02 1.050E+03 NOT IDENT. NB-94 8.328E-03 *3.326E-02 6.198E-02 NOT IDENT. NB-95 4.546E-01 9. 760E-01 -l.920E+OO NOT IDENT. .NB-95M 8.656E-01 2.662E+OO 4.785E+OO NOT IDENT. ZR-95 8. 962E-02 1.322E+OO 2. 572E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.305E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.158E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 5.080E-03 3.847E-02 6.507E-02 NOT IDENT. RH-'-102 3.756E-02 5.752E-02 1.208E-01 NOT IDENT. RU-103 -3.909E+OO 5.lOOE+OO 8.823E+00 FAIL ABUN RH-106 -7.579E-02 4.995E-01 9.362E-01 FAIL ABUN RU-106 -7.579E-02 4.995E-01 9.362E-01 FAIL ABUN AG-108M 1. 727E-02 2.729E-02 5.656E-02 NOT IDENT. AG-llOM -8.523E-02 l.004E-01 1.593E-01 FAIL ABUN SN-113 -2.925E-02 2.040E-01 3.917E-01 NOT IDENT. CD-115 O.OOOE+OO 1.825E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 0.000E+OO 9.374E+04 O.OOOE+OO SHORT HLIF TE-123M 4.718E-03 l.414E-01 2.795E-01 NOT IDENT. SB-124 -1.878E+OO l.637E+OO 1. 776E+OO NOT IDENT. SB-125 -l.082E-02 9.934E-02 1.901E-01 NOT IDENT. TE-125M 6.273E+Ol 3.059E+02 5.674E+02 NOT IDENT . I-126 O.OOOE+OO . 9. 549E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.086E+o6 O.OOOE+OO -SHORT HLIF SB-127 O.OOOE+OO l.598E+22 O.OOOE+OO SHORT HLIF I-131 0. OOOE+OO_ 4. 096E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.430E+26 O.OOOE+OO SHORT HLIF BA-133 2.323E-02 4.307E-02 8.057E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.025E-02 6.329E-02 1. 281E-01 NOT IDENT. CS-135 -6.215E-02 1.478E-01 2.463E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.422E+05 O.OOOE+OO SHORT HLIF CE-139 2.333E-02 1.015E-01 2.050E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 297E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3. 761E+05 O.OOOE+OO SHORT HLIF CE-141 1. OOlE+Ol 2.238E+Ol 4.585E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.576E+41 O.OOOE+OO SHORT HLIF CE-144 6.062E-02 4.104E-01 7.478E-01 NOT IDENT-. PM-144 -2.192E-02 5.275E-02 9.415E-02 NOT IDENT. PR-144 -1.887E+OO 4.579E+OO 8.179E+OO NOT IDENT. PM-146 l.579E-03 4 .119E-02 8.030E-02 NOT IDENT. ND-147 O.OOOE+OO 3.634E+07 O.OOOE+OO SHORT HLIF PM-147 2.177E+02 9.659E+02 1. 781E+o3 NOT IDENT. PM-149 0.000E+OO 2.348E+40 o.-oooE+oo SHORT HLIF EU-150 2.461E-02 2.784E-02 5.355E-02 FAIL ABUN EU-152 -l.533E-02 9.628E-02 1.832E-01 NOT IDENT. GD-153 5.333E-02 2.075E-Ol 3. 610E-01 NOT IDENT. EU-154 -7.429E-03 9.930E-02 2.006E-01 FAIL ABUN EU-155 9.166E-02 1.201E-01 2.338E-01 FAI.L ABUN TB-160 -9.629E-01 2.004E+OO 3.461E+OO FAIL ABUN H0-166M O.OOOE+OO 8.884E-02 1.223E-01 FAIL ABUN TM-171 -1. 473E+Ol 4.019E+Ol 7. 396E+Ol NOT IDENT. HF-172 3.379E-03 2.709E-01 4.519E-01 FAIL ABUN LU-172 7.175E-02 7.846E-02 1. 765E-01 FAIL ABUN LU-176 -l.076E-02 2.381E-02 4.436E-02 FAIL ABUN HF-181 1.271E+OO 3.789E+OO 7.711E+OO NOT IDENT. Page 3041of5809 TA-182 3.677E-01 9.252E-01 1.780E+00 FAIL ABUN RE-183 -1.069E-02 4.879E+OO 9.182E+OO NOT IDENT. RE-184 1.417E+Ol 2.767E+Ol 5.768E+Ol NOT IDENT. W-188 -4.823E+Ol l.084E+02 l.923E+02 FAIL ABUN IR-192 3. 096E-01 4.344E-01 9.031E-01 FAIL ABUN HG-:-203 2.435E+OO 2.341E+OO 4.928E+OO NOT IDENT. BI-207 -4.060E-02 4.397E-02 7.559E-02 FAIL ABUN PB-210 -6. 291E-01 8.393E+OO l .°595E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.470E-01 7.906E-01 FAIL ABUN PB-211 -2.468E-02 6.710E-01 l.289E+OO NOT IDENT. BI-212 O.OOOE+OO 9.448E-01 l.374E+OO *FAIL ABUN RN-219 -3.656E-02 3.732E-01 7.139E-01 FAIL ABUN RA-223 -3.302E-01 5.544E-01 l.015E+OO FAIL ABUN AC-227 -7.881E-02 2.487E-01 4.705E-01 FAIL ABUN TH-227 -7.881E-02 2.487E-01 4.705E-01 FAIL ABUN* TH-229 4.338E-02 4.603E-01 9.108E-01 FAIL ABUN TH-231 -3.302E-01 5.544E-01 l.015E+OO FAIL ABUN PA-233 -6.032E-03 5. 711E-02 l.102E-01 FAIL ABUN PA-234 -9.698E-02 2.745E-01 5.269E-01 FAIL ABUN PA-234M 1.616E+OO 3.597E+00 7.521E+OO NOT IDENT. U-235 -2.144E-02 l.797E-01 3.545E-01 FAIL ABUN NP-237 -6.032E-03 5.711E-02 l.102E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF NP-239 l.792E-02 2.553E-01 4.693E-01 NOT IDENT. PU-239 4.826E+02 6.058E+02 6.983E+02 FAIL ABUN AM-241 -l.091E-01 2.368E-01 3.916E-01 NOT IDENT. CM-243 -l.OlBE-01 1. 076E-01 1. 803E-01 NOT IDENT. BK-247 1. 296E-02 7.448E-02 1.413E-01 NOT IDENT. CM-247 -2.391E-03 3.386E-02 6.502E-02 NOT IDENT. CF-249 l.156E-02 3.690E-02 7.375E-02 NOT IDENT. CF-251 -3.520E-02 l.088E-01 2.104E-01 NOT IDENT. Page 3042 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:06:27.42 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 376 10.66* 1.119E+OO 1.552E+Ol 1.552E+Ol 10.42 C0-58 810.76 13 99.45* 1.793E+OO 3.603E-02 6.633E-01 128.52 CD-109 88.03 48 3.70* 4.577E+OO 1.399E+OO 2.189E+OO 103.01 SN-126 64.28 59 9:60 2.075E+OO 1.451E+OO 1.451E+OO 103.12 86.94 48 8.90 4.577E+OO 5.818E-01 5.818E-01 103.01 87.57 48 37.00* 4.577E+OO 1. 399£:-01 1.400E-01 103.01 BA-137M 661. 66 95 89.90* 2.104E+OO 2.484E-01 2.531E-01 39.80 CS-137 661. 66 95 85.10* 2.104E+OO 2.624E-01 2.674E-01 39.80 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 148 85.00* 2.325E+OO 3.684E-01 3.684E-01 25.69 860.56 21 12.50 1.712E+OO 4.765E-01 4.765E-01 90. 96 BI-211 72.87 ------1.23 3.214E+OO ------Line Not Found ------351.06 286 12.92* 3. 521E+OO 3.091E+OO 3.091E+OO 18.06 PB-212 74.82 140 10.28 3.461E+OO 1.938E+OO 1.938E+OO 45.91 77' 11 233 17.10 3.693E+OO 1. 813E+OO 1.813E+OO 26.24 238.63 443 43.60*' 4.786E+OO 1.046E+OO l.046E+OO 13 .16' 300.09 27 3.30 4. OllE+OO 1. 017E+OO
1. 017E+OO 111.80 BI-214 609.32 175 45.49* 2.246E+OO 8.454E-01 8.457E-01 22. 62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 PB-214 74.82 140 5.80 3.461E+OO 3.436E+OO 3.437E+OO 45.91 77 .11 233 9.70 3.693E+OO 3 .196E+OO 3.197E+OO 26. 24 87.09 48 3.41 4.577E+OO l.519E+OO 1.519E+OO 103.01 242.00 108 7. 25 4.743E+OO 1.540E+OO 1.541E+OO 50.98 295.22 191 18.42 4.064E+OO 1.258E+OO 1.258E+OO 25.48 351.93 286 35.60* 3.521E+OO 1.122E+OO 1.122E+OO 18.06 RN-222 609.32 175 45.49* 2.246E+OO 8.454E-01 8.457E-01 22.62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 RA-224 240.99 108 4.10* 4.743E+OO 2. 723E+OO 2.723E+OO 50.98 609.32 175 45.49* 2.246E+OO 8.454E-01 8.457E-01 22. 62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 AC-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 128 11. 27 3.639E+OO 1.535E+OO l.535E+OO 32.99 794.95 ------4.25 1.823E+OO ------Line Not Found ------83.5. 71 ------1. 61 i. 753E+oo* ------Line Not Found ------911.20 105 25.80* l.638E+OO l.226E+OO l.226E+OO 22.98 968. 97 57 15.80 1. 561E+OO 1.130E+OO 1.130E+OO 61. 71 RA-228 105.21 ------1.1.0 5.586E+OO ------Line* Not Found ------338.32 128 11. 27 3.639E+OO 1.535E+OO 1.535E+OO 32.99 794.95 ------4.25 1.823E+OO ------Line Not Found ------835. 71 ------1. 61. 1. 753E+OO ------Line Not Found ------911.20 105 25.80* 1.638E+OO 1. 226E+OO l.226E+OO 22.98 968. 97 57 15.80 1.561E+OO l.130E+OO l.130E+OO 61. 71 TH-228 74.82 140 10.28 3.461E+OO 1.938E+OO 1.938E+OO 45.91 77 .11 233 17.10 3.693E+OO 1.813E+OO 1.813E+OO 26. 24 Page 3043 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 443 43.60* 4.786E+OO l.046E+OO 1. 046E+OO 13.16 300.09 27 3.30 4. OllE+OO 1.017E+OO 1.017E+OO 111. 80 TH-230 609.32 175 45.49* 2.246E+OO 8.454E-01 8.455E-01 22.62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.904E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.405E-01 44.75 PA-231 283.69 ------1. 70 4.201E+OO ------Line Not Found ------301.36 27 5.35* 4. OllE+OO 6. 271E-01 6.271E-01 111. 80 TH-232 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 128 11. 27 3.639E+OO 1.535E+OO 1.53SE+OO 32.99 835. 71 ------1. 61 1. 753E+OO ------Line Not Found ------911. 20 105 25.80* 1.638E+OO 1.226E+OO 1.226E+OO 22.98 968. 97 57 15.BO 1.561E+OO l.130E+00 1.130E+OO 61.71 TH-234 63.29 59 3.70* 2.075E+OO 3.764E+00 3.764E+OO 103.12 92.59 59 4.23 4.971E+OO 1.370E+OO 1.370E+OO 103.36 U-234 609.32 175 45.49* 2.246E+OO 8.454E-01 8.454E-01 22. 62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.904E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E'-01 7.405E-01 44.75 U-238 63.29 59 3.70* 2.075E+OO 3.764E+00 3.764E+00 103.12 92.59 59 4.23 4.971E+OO 1.370E+OO 1.370E+OO 103.36 AM-243 43.53 ------5.90 1. 701E-01 ------Line Not Found ------74.66 140 67.20* 3.461E+OO 2. 965E-01 2. 965E-01 45.91 ANH-511 511. 00 50 100.00* 2.588E+OO 9.466E-02 9.466E-02 83.19 Flag: "*" =.Keyline Page 3044 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Total number of lines in spectrum 47 Number of unidentified lines 9 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 70.86D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1.41E+10Y l.41E+l0Y l.41E+10Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 18.4 1. 56 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 0.0 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM . 1.552E+Ol 3.603E-02 1.399E+OO 1.399E-01 2.484E-01 2.624E-01 3.684E-01 3.091E+OO 1. 046E+OO 8.454E-01 1.122E+OO 8.454E-01 2. 723E+00 8.454E-01 1.226E+OO 1.226E+OO 1.046E+00 8.454E-01 6.271E-01 l.226E+OO 3.764E+OO 8.454E-01 3.764E+OO 2. 965E-01 9.466E-02 4.345E+Ol 4.345E+Ol Decay Corr pCi/GRAM 1.552E+Ol 6.633E-01 2.189E+OO l.400E-01 2.531E-01 2.674E-01 3. 684E-Ol. 3.091E+OO 1. 046E+OO 8.457E-01 l.122E+OO 8.457E-01 2.723E+OO 8.457E-01 l.226E+OO l.226E+00 l.046E+OO 8.455E-01 6. 271E-01 l.226E+OO 3.764E+00 8.454E-01 3.764E+OO 2.965E-01 9.466E-02 4.488E+Ol 4.488E+Ol 80.85% Decay Corr 2-Sigma Error 0.162E+Ol 8. 5.25E-01 2.255E+OO 1. 442E-01 l.007E-01 l.064E-01 0.946E-01 0.558E+OO 0.138E+OO l.913E-01 0.203E+OO 1. 913E-01 l.388E+OO, l.913E-01 0.282E+OO 0. 282E+OO' 0 .138E+OO l.912E-01 7. OllE-01 0.282E+OO 3.882E+OO l.912E-01 3.882E+OO l.362E-01 7.874E-02 "M" Manually accepted 2-Sigma %Error 10.42 128.52 103.01 103.01 39. 80 39.80* 25.69 18.06 13 .16 22.62 18.06 22.62 50.98 22.62 22.98 22.98 13.16 22.62 111.80 22.98 103.12 22.62 103.12 45.91 83.19 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3045 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235007 ' Acquisition date : 3-0CT-2016 08:02:54 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 94.77 40 106 1. 26 190.76 184 10 8.77E-03 **** 5.07E+OO T 0 129.53 38 145 1. 78 260.27 256 8 8.50E-03 **** 6.09E+OO :r 0 186.37 165 201 1. 23 373. 96 368 13 3.85E-02 43.l 5.60E+OO T 0 209.43 84 90 1. 25 420.08 416 8 l.97E-02 48.7 5.24E+OO T 0 270.47 52 71 1. 08 542.17 537 10 l.27E-02 71. 2 4.36E+OO. T 0 464.99 16 55 0. 67 931.20' 925 11 3.97E-03 **** 2.80E+OO 0 534.57 25 39 -3. 98 1070.37 1064 13 6.57E-03 **** 2.50E+OO 7 707.28 12 9 1. 96 1415.81 1413 25 3.12E-03 96.3 2.00E+OO T 7 710.32 28 16 2.00 1421. 88 1413 25 7. 41E-03 71.1 1.99E+OO T 0 720.76 14 7 3.40 1442.77 1438 10 3.86E-03 90.8 1. 97E+OO T 0 728 .15 37 29 0.95 1457.55 1450 12 9.78E-03 69.5 1. 95E+OO T 0 797.49 23 27 1. 86 1596. 23 1586 14 6.26E-03 **** 1.82E+00 0 803.54 19 12 0.66 1608.33 1604 11 5.25E-03 89.5 1.81E+OO 0 816.56 10 15 1. 70 1634.38 1630 8 2.62E-03 **** 1. 79E+OO T 0 996.21 12 13 1.17 1993.69 1989 12 3.43E-03 **** 1. 53E+OO T 0 1049.83 19 6 3.87 2100.93 2093 14 5.20E-03 75.2 1. 4 7E+OO T 0 1190. 02 9 7 0.61 2381. 31 2378 6 2.57E-03 **** l.33E+OO T 0 1227.61 16 11 3.52 2456.49 2449 15 4.58E-03 **** 1.29E+OO 0 1234.03 27 5 2.60 2469.34 2464 10 7.53E-03 49:2 1.29E+OO T 0 1239.00 22 5 1.24 2479.29 2475 11 6.25E-03 58.4 1.28E+OO T 0 1245.45 17 3 3.62 2492.19 2486 11 4.79E-03 60.9 1.28E+OO 0 1250.95 17 15 3.83 2503.18 2497 14 4.77E-03 ****' l.27E+00 0 1333.81 15 3 4.00 2668.91 2663 11 4.25E-03 66.1 1.21E+OO T 0 1337.86 6 0 1. 50 2677.00 2674 6 1.67E-03 81. 6 1.21E+OO 0 1544.74 9 2 0.52 3090.77 3086 8 2.58E-03 83.5 1.07E+OO Flags: "T" = Tentatively associated Page 3046 of 5809 VAX/VMS Nuclide _Identification Report Generated 03-0CT-2016 09: 06: 43. 93 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l * *.Acquisition date 3-0CT-2016 08:02:54 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
Sample date 10-DEC-2015 13:55:00 Nuclide Library : SOLID *
Sample ID G405235007 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5252E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN * * 'Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid.' Please refer to Certificate of Analysis. Identified Nuclides Le Nuclide (pCi/GRAM ) K-40 2.145E-01 C0-58 3.645E-01 CD-109 1.347E+OO SN-126 7.925E-02 BA-137M 3. 241E-02 CS-137 3.424E-02 TL-208 PB-212 4.791E-02 BI-214 5.602E-02 PB-214 5.848E-02 RN-222 5.602E-02 RA-224 5 .134E-01 RA-226 5.602E-02 AC-228 1.157E-01 RA-228 1.157E-01 TH-228 4.791E-02 TH-230 5.600E-02 PA-231 4.048E-01 TH-232 1.157E-01 TH-234 1.504E+OO U-234 5.600E-02 U-238 1.504E+OO AM-243 5. 511E-02 ANH-511 2.231E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3047 of 5809 Le (pCi/GRAM 1.052E+01 3.377E-02 O.OOOE+OO 3.517E-02 3.552E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133-I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3048 of 5809 5.427E-02 3.743E-01 O.OOOE+OO 4.857E-02 4.676E+OO 3.579E-02 1.518E-01 2.322E+OO 1.334E+Ol O.OOOE+OO l.825E-01 O.OOOE+OO O.OOOE+OO 4.445E-01 6.854E+OO 7.079E-01 O.OOOE+OO 1.522E-01 4.580E+02 2.759E-02 8.686E-01 2.246E+OO 1.120E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.050E-02 5.390E-02 3.863E+OO 4.138E-01 4.138E-01 2.571E-02 6. 691E-02 l.760E-01 O.OOOE+OO O.bOOE+OO l.318E-01 4.471E-01 8.557E-02 2.670E+02 0.000E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.691E-02 O.OOOE+OO 5.834E-02 l.132E-01 O.OOOE+OO O.OOOE+OO 9.582E-02 O.OOOE+OO O.OOOE+OO 2.155E+Ol O.OOOE+OO 3.523E-01 4.108E-02 3.569E+OO 3.604E-02 O.OOOE+OO 8.393E+02 O.OOOE+OO 2.478E-02 8.402E-02 l.694E-01 8.393E-02 1.lOlE-01 l.498E+OO 5.479E-02 3.458E+Ol 2.120E-01 7.807E-02 2.030E-02 3.445E+OO 7.733E-01 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN .FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABON NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-.207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3049 of 5809 4.320E+OO 2. 517E+Ol 8.804E+Ol 4.158E-01 2.296E+OO 3.144E-02 7.468E+OO 3.802E-01 5.862E-01 6.347E-01 3.238E-01 4.613E-01 2.191E-01 2.191E-01 4.264E-01 4.613E-01 5.045E-02 2.280E-01 3.232E+00 1.667E-01 5.045E-02 O.OOOE+OO 2 .*195E-01 3.307E+02 1.837E-01 8.386E-02 6.539E-02 3.364E-02 9.812E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT' IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:06:49.63 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF';l * *Acquisition date 3-0CT-2016 08:02:54 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.63 Half life ratio : ***** * *Sample date. 10-DEC-2015 13:55:00 Nuclide Library: SOLID *
Sample ID G405235007 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5252E+02 GRAM *
Quantity Err(%) : 1.3113E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) K-40 1.552E+Ol 1. 780E+OO 1. 780E+OO C0-58 6.633E-01 8.359E-01 8.359E-01 CD-109 3.758E-01 2.267E+OO 2.267E+OO SN-126 2.402E-02 1. 449E-01 1.449E-01 BA-137M 2. 531E-01 9.931E-02 9.931E-02 CS-137 2.674E-01 1.049E-01 l.049E-01 TL-208 3.684E-01 9.407E-02 9.407E-02 PB-212 1. 046E+00 l.459E-01 l.459E-01 BI-214 8.457E-01 1.909E-01 l.909E-01 PB-214 1.122E+OO 2. 041E-01 2.041E-01 RN-222 8.457E-01 l.909E-01 1.909E-01 RA-224 4.991E-01 l.477E+00 l.477E+OO RA-226 8.457E-01 1.909E-01 l.909E-01 AC-228 l.226E+00 2.832E-01 2.832E-01 RA-228 1.226E+OO 2.832E-01 2. 832E*-01 TH-228 1.046E+OO l.459E-01 l.459E-01 TH-230 8.455E-01 1.909E-01 1.909E-01 PA-231 6.271E-01 7.000E-01 7.000E-01 TH-232 1. 22 6E+OO 2.832E-01 2.832E-01 TH-234 3.764E+OO 3.895E+OO 3.895E+OO U-234 8.454E-01 1.909E-01 1.909E-01 U-238 3.764E+OO 3.895E+OO I 3.895E+OO AM-243 1.880E-01 1.373E-01 1.373E-01 ANH-511 9.466E-02 7.726E-02 7.726E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 2.468E+OO 1.180E+Ol 1.185E+Ol NOT IDENT. NA-22 -l.801E-02 4.319E-02 4.395E-02 NOT IDENT. NA-24 1.000E+41 l.583E+41 O.OOOE+OO SHORT HLIF AL-26 2.599E-02 3.513E-02 3.704E-02 NOT IDENT. SC-46 -7.774E-02 4.446E-01 4.460E-01 FAIL ABUN V-48 7.600E+03 1.266E+04 1.312E+04 SHORT HLIF Page 3050 of 5809 CR-51 6. 530E+Ol
4.162E+02 4.173E+02 SHORT HLIF MN-54 8.976E-03 6.462E-02 6.475E-02 NOT IDENT. C0-56 -l.060E-02 4.543E-01 4.543E-01 FAIL ABUN MN-56 -1.000E+41 4.285E+42 O.OOOE+OO SHORT HLIF C0-57 3.147E-02 5.429E-02 5.612E-02 NOT IDENT. FE-59 -3.185E+OO 6.003E+OO 6.173E+OO NOT IDENT. C0-60 6.774E-02 4.393E-02 5.350E-02 FAIL ABUN ZN-65 -3.150E-02 2.052E-01 2.057E-01 NOT IDENT. GE-68 1. 743E+OO 2.388E+OO 2.514E+OO NOT IDENT. AS-73 -3.993E-01 1.505E+Ol 1.505E+Ol NOT IDENT. AS-74 2.245E+03 5.813E+03 5. 901E+03 SHORT HLIF SE-75 -3.559E-02 2.054E-01 2.060E-01 NOT IDENT. BR-77 l.028E+38 8.832E+38 O.OOOE+OO SHORT HLIF SR-82 -2.144E+02 6.737E+02 6.806E+02 SHORT HLIF RB-83 -5.887E-Ol 6.187E-01 6.732E-01 NOT IDENT. KR-85 5.211E+OO 8.056E+OO 8. 391E+OO NOT IDENT. SR-85 5.350E-Ol 8.324E-01 8.667E-01 NOT IDENT. RB-86 1.804E+04 2.648E+04 2.770E+04 SHORT HLIF Y-88 1.131E-01 1.282E-01 1.380E-01 NOT IDENT. Y-91 -1.149E+Ol 5.321E+02 5.322E+02 NOT IDENT. NB-94 8.328E-03 3.326E-02 3.347E-02 NOT IDENT. NB-95 4.546E-01 9.762E-01 9.975E-01 NOT IDENT. NB-95M 8.656E-01 2.663E+OO 2. 691E+OO NOT IDENT. ZR-95 8. 962E-02 1.322E+OO 1.323E+OO NOT IDENT. NB-97 -l.OOOE+41 2.015E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 l.306E+41 O.OOOE+OO SHORT HLIF M0-99 -6.792E+31 1.159E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 1.054E+42 0. OOOE+OO' SHORT HLIF RH-101 5.080E-03 3.848E-02 *3.854E-02 NOT IDENT. RH-102 3.756E-02 5.760E-02 6.004E-02 NOT IDENT. RU-103 -3.909E+OO 5.104E+OO 5.399E+OO FAIL ABUN RH-106 -7.579E-02 4.995E-01 5.007E-01 *FAIL ABUN RU-106 -7.579E-02 4.995E-01 5.007E-01 FAIL ABUN AG-108M 1.727E-02 2.730E-02 2.839E-02 NOT IDENT. AG-llOM -8.523E-02 l.005E-01 l.076E-01 FAIL ABUN SN-113 -2.925E-02 2.040E-01 2.044E-01 NOT IDENT. CD-115 7.006E+38 l.830E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 4.147E+04 9.386E+04 9.571E+04 SHORT HLIF TE-123M 4.718E-03 l.414E-01 1.414E-01 NOT IDENT. SB-124 -1.878E+OO 1.640E+OO 1.846E+OO NOT IDENT. SB-125 -l.082E-02 9.934E-02 9.946E-02 NOT IDENT. TE-125M 6.273E+Ol 3.059E+02 3.072E+02 NOT IDENT. I-126 4.551E+05 9.569E+05 9.787E+05 SHORT HLIF SB-126 l.220E+06 l .110E+06 1.239E+06 SHORT HLIF SB-127 4.058E+21 1. 691E+22 O.OOOE+OO SHORT HLIF I-131 -3.554E+09 4.099E+09 4. 401E+09 SHORT HLIF I-132 -l.000E+41 l.865E+42 O.OOOE+OO SHORT HLIF TE-132 -3.447E+24 2.430E+26 O.OOOE+OO SHORT HLIF BA-133 2.323E-02 4.308E-02 4.434E-02 NOT IDENT. I-133 1.000E+41 7.821E+41 O.OOOE+OO SHORT HLIF CS-134 5.025E-02 6.332E-02 6.725E-02 NOT IDENT. CS-135 -6.215E-02 1.478E-01 l.505E-01 NOT IDENT. I-135 l.OOOE+41 8.076E+41 O.OOOE+OO SHORT HLIF CS-136 -9.321E+04 2.425E+05 2.461E+05 SHORT HLIF CE-139 2.333E-02 1.016E-01 l.022E-01 NOT IDENT. BA-140 1. 476E+05 l.297E+06 l.299E+06 SHORT HLIF .LA-140 4.078E+04 3.761E+05 3.766E+05 SHORT HLIF CE-141 1.00lE+Ol 2.238E+Ol 2.283E+Ol NOT IDENT. CE-143 l.OOOE+41 l.579E+41 O.OOOE+OO SHORT HLIF CE-144 6.062E-02 4.105E-01 4 .114E-01 NOT IDENT. PM-144 -2.192E-02 5.277E-02 5.368E-02 NOT IDENT. PR-144 -1.887E+OO 4.580E+OO 4.658E+OO NOT IDENT. PM-146 1.579E-03 4 .119E-02 4.120E-02 NOT IDENT. ND-147 -7.968E+06 3.635E+07 3. 652E+07
SHORT HLIF PM-147 2.177E+02 9.659E+02 9.709E+02 NOT IDENT. PM-149 l.655E+40 2.375E+40 O.OOOE+OO SHORT HLIF EU-150 2. 461E-02 2.786E-02 2.999E-02 FAIL ABUN EU-152 -1.533E-02 9.629E-02 9.653E-02 NOT IDENT. GD-153 5.333E-02 2.089E-01 NOT IDENT. EU-154 -7.429E-03 9.930E-02 9.936E-02 FAIL ABUN EU-155 9.166E-02 1.203E-01 l.272E-01 FAIL ABUN TB-160 -9.629E-01 2.005E+OO 2.052E+OO FAIL ABUN H0-166M 1. 27 5E-01 8. 911E-02 1.060E-01 FAIL ABUN TM-171 -1. 473E+Ol 4.021E+Ol 4.076E+Ol NOT IDENT. HF-172 3.379E-03 2.709E-01 2.709E-01 FAIL ABUN LU-172 7.175E-02 7.880E-02 8.518E-02 FAIL ABUN LU-176 -1.076E-02 2.382E-02 2.431E-02 FAIL ABUN HF-181 1. 271E+00 3.789E+OO 3.832E+OO NOT IDENT. Page 3051 of 5809 TA-182 3.677E-01 9.253E-01 9.400E-01 FAIL ABUN RE-183 -1. 069E-02 4.879E+OO 4.879E+OO NOT IDENT. RE-184 1. 417E+Ol 2.788E+Ol 2.860E+Ol NOT IDENT. W-188 -4.823E+Ol 1.085E+02 l.106E+02 FAIL ABUN IR-192 3.096E-01 4.346E-01 4.564E-01 FAIL ABUN HG-203 2.435E+OO 2.344E+OO 2.588E+OO NOT IDENT. BI-207 . -4. 060E-02 4.399E-02 4.765E-02 FAIL ABUN PB-210 -6.291E-01 8 .. 393E+OO
8.398E+OO NOT IDENT. BI-211 3.091E+OO 5.643E-01 1. 503E+OO FAIL ABUN PB-211 -2.468E-02 6.710E-01 6.711E-01 NOT IDENT. BI-212 1.387E+OO 9.474E-01 l.135E+OO FAIL ABUN RN-219 -3.656E-02 3.732E-01 3. 736E-01 . FAIL ABUN RA-223 -3*. 302E-01 5.548E-01 5.744E-01 FAIL ABUN AC-227 -7.881E-02 2.489E-01 2.514E-01 FAIL ABUN TH-227 -7. 881E-02 2.489E-01 2.514E-01 FAIL ABUN TH-229 4.338E-02 4.603E-01 4.607E-01 FAIL ABUN TH-231 -3.302E-01 5.548E-01 5.744E-01 FAIL ABUN PA-233 -6.032E-03 5.711E-02 5. 718E-02 FAIL ABUN PA-234 -9.698E-02 2. 961E-01 2.993E-01 FAIL ABUN PA-234M 1.616E+OO 3.598E+OO 3.671E+OO NOT IDENT. U-235 -2.144E-02 l.797E-01 1. 799E-01 FAIL ABUN NP-237 -6.032E-03 5.711E-02 5.718E-02 FAIL ABUN NP-238 -1.000E+41 1.995E+41 O.OOOE+OO SHORT HLIF NP-239 1. 792E-02 2.553E-01 2.554E-01 NOT IDENT. PU-239 4.826E+02 6.061E+02 6.440E+02 FAIL ABUN AM-241 -1. 091E-01 2.370E-01 2.420E-01 NOT IDENT. CM-243 -1.018E-01 1.080E-01 l.173E-01 NOT IDENT. BK-247 *1. 296E-02 7.453E-02 7.476E-02 NOT IDENT. CM-247 -2.391E-03 3.386E-02 3.388E-02 NOT IDENT. CF-249 l.156E-02 3. 691E-02 3.728E-02 NOT IDENT. CF-251 -3.520E-02 1. 089E-01 l. lOlE-01 NOT IDENT. Page 3652 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 60.1854 87.09 115. 6747 136.47 95.9819 45.60 71. 5991 87.57 117.7241 140.51 0.0000 46.54 68.3569 88.03 141.1892 143.76 85.6973 49. 72 0.0000 88.34 141.2417 144.24 82.3725 35 66.6640 88.47 146.0260 145.44 71.5216 51. 87 72.3762 89. 96 135.9516 152.43 83.8122 52.39 78.0977 1093.63 109.8045 153.25 0.0000 52.97 71. 3746 91.11 0.0000 323.87 84.7890 53.44 66.8942 92.59 105.2728 156.02 0.0000 54.07 82.8521 93.35 105.3661 158.56 0.0000 57.36 0.0000 94.56 105.5151 159.00 91.0932 57.53 73.0383 94.65 105.5259 162.33 83.6625 57.98 84.5096 94.67 105.5286 162.66 0.0000 59.27 76.2866 94.87 105.5527 163.33 79.4602 59.32 99.1800 97.43 70. 5:7 53 165.86 63.3574 59.54 90.0554 98.43 75.8743 176.31 60.4368 60. 96 68.8346 98.44 75.8752 176.60 0.0000 61.17 68.8564 99.53 73.5568 177. 52 70.8641 62.93 88.5981 100 .11 74.8113 181.07 0.0000 63.29 88.6451 102.03 83.4357 181.52 66.3173 63.58 88.6830 103.18 85. 9630 184.41 82.1030 64.28 102.9933 103.37 82.3479 143.76 69.5744 66.73 87.9318 105.21 67.9522 193.51 69.9821 67.24 83.3648 105.31 67.9599 197.03 72.7947 125.81 99.6370 106.12 72.8778 198.01 55.2935 67.75 99.6468 106.47 88.7014 201.83 75.6892 69.67 97.5925 109.28 79.2183 203.43 49.3429 70.83 85.3366 111. 00 90.3512 205.31 55.5851 72.81 99.5703 111. 76 0.0000 210.85 65.1035 72. 87 101.1340 114. 06 77.1663 215.65 79.9850 74.66 102.9377 116. 30 0.0000 222 .11 62.4862 74.82 102.9598 116.74 68.7806 227.09 55.5303 74.97 102.9807 119.76 85.0066 227.38 52.8536 77 .11 103.2727 121.12 82.6551 228.16 0.0000 78.74 106.6284 121. 22 82.6633 228.18 60.0522 79*_ 69 108.3291 121.78 69.1301 116.74 60.0522 80.12 111. 5305 122.06 75.3234 235.69 70.2582 80.19 0.0000 122.92 74.1513 235. 96 70.2701 80.57 73.8726 123.07 74.1623 238.63 68.5874 81. 00 86.4936 265. 00 89.0480 238.98 0.0000 81. 07 86.5015 125.81 76.0139 240.99 68.6918 81.75 97.9888 127.23 71.1540 242.00 68.7358 83.79 106.5255 127.91 81.1361 244.70 62.5130 84.00 113. 6565 129.30 83.3165 252.40 0.0000 85.43 104.3704 131. 20 94.6799 252.80 58.2786 86.55 131. 4335 133.02 93.1784 254.15 0.0000 86.79 131.4724 133.52 84.8983 256.23 68.4406 86.94 115.6539 136. 00 90.9342 260.90 0.0000 Page 3053 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA°COUNTS 264. 66 53.2009 355.39 0.0000 584.27 15.8948 264.80 48.4355 356.01 30.3689 595.83 0.0000 265.00 48.4408 364.49 0.0000 427.87 24.5105 268.22 52.3950 366.42 0.0000 602.52 0.0000 269.46 43.2354 372.51 28.1846 604. 72 24. 0115 270.03 43.2497 375.05 32 .1111 607.14 30.4401 . 271. 23 43.2803 377.52 37.9939 609.32 23.5155 273.65 0.0000 356.01 32.2454 610.33 23.5236 276.40 46.1843 388.16 31.3314 614.28 22.4843 277.37 55.4529 388.63 0.0000 618.01 13.9363 277.60 54.5359 391. 69 28.4407 620.36 26.8219 278.00 49.0006 264.66 24.6195 621.93 21.4689 279.20 41.6336 401.81 33.4999 630.19 0.0000 279.54 58.2986 402.40 32.5233 631.29 15.0755 279.70 58.3037 ' 404.85 34.5329 633.25 16.1627 280.46 50.9224 410.95 31. 6602 634.78 0.0000 283.69 38.0321 413.71 31.6992 635.95 20.4913 284.31 0.0000 414.70 0. 0000' 636.99 0.0000 285.41 42.7123 423. 72 0.0000 645.85 16.2299 285.90 0.0000 427.09 30.8909 657.76 19.5520 287.50 53.9183 427.87 28.9080 657.90 0.0000 290.67 433.94 23.9868 661.66 26.1016 293.27 0.0000 439.40 31.0561 664.57 0.0000 351.93 44.8184 453.88 '25.1994 666.33 0.0000 295. 96 44.8369 463.37 26.3110 . 666.50 0.0000 879.38 36.4832 468.07 34.9808 667. 71 0.0000 299.98 36.5117 473.00 0.0000 677. 62 18.5834 300.09 44.9404 475.06 23.3870 685.70 0.0000 300.13 44.9414 476.78 27.4735 695.00 0.0000 301.36 51. 9985 477.60 24.4292 6.96. 49 20.8926 302.85 36. 5696 482.18 19.3753 696. 51 20.8926 256.23 36.6030 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.6982 306.78 46.9859 497.08 26.6713 697.49 20.8995 308.46 31.9795 505.52 32.4203 702.65 17.1869 311. 90 41.4631 507.63 0.0000 706.68 21.5098 316.51 33.0639 511. 00 23.7225 711. 68 9.9430 319.41 0.0000 514.00 26.3311 720.70 0.0000 320.08 0.0000 514.00 26.3311 721. 93 0.0000 321. 04 36.9315 520.40 27.9492 722.78 13.3022 323.87 43.6257 520.69 0.0000 722.91 13.3027 325.23 48.4019 522.65 0.0000 723.31 13.3042 328.76 0:0000 527.90 0.0000 724 .19 13.3076 333.37 35.7414 528.26 19.9344 727. 33 10.6563 333.97 34.3220 529.59 21.8135 733.00 12.0085 334.37 35.7597 529.87 0.0000 735.93 13.3545 338.28 39.1757 531.02 0.0000 333.97 15.5876 338.32 39.1766 537.26 0.0000 739.50 0.0000 311. 90 31. 5673 546.56 0.0000 747.24 18.9825 340.48 31. 5673 552.55 31.4294 748.06 13.4028 340.55 0.0000 563.25 18.9309 752.31 22.3657 344.28 44.0880 569.33 20.0267 753.82 0.0000 345.93 39.1374 946.00 20.0275 756.73 14.5568 351.06 37.5067 569.70 20.0290 756.80 14.5573 351.93 37.5234 583.19 15.8887 884.68 28.0528 Page 3054 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.5771 1274.44 8.9459 1620.50 1. 0120 766.42 31. 4419 1001.03 5.7320 1621. 92 1. 0123 766.84 35.9375 1002.74 16.7253 1678.03 0.0000 772.60 0.0000 1004.73 12.5499 1690.97 6.1425 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.9714 778.90 9.0156 1028.54 0.0000 1063.66 7.2563 783.70 0.0000 1037.84 7.2271 1771. 35 5.1840 785.37 11.2903 1038.76 0.0000 1791.20 0.0000 792.07 11. 8774 631. 29 10.1384 1808.65 3.1282 794.95 22.6424 1048.07 0.0000 1810.7'2 0.0000 795.86 22.6481 1049.04 12.6807 1836.06 0.0000 810.06 9. 0 9'54 1050.41 12.6849 810.29 9. 0960 1063.66 13.6322 344.28 9. 0964 1077.00 0.0000 810.76 9.0970 1077.34 10.9395 815.77 0.0000 1085.87 6.3937 1048.07 0.0000 1093.63 10.0648 832.01 16.0132 1099.45 14.6582 834.85 14.8810 1112. 07 13.7805 835. 71 18.3197 1112.84 11. 9455 836.80 0.0000 1115. 54 17.6531 846.75 0.0000 1120. 29 14.7256 846.77 14.9292 1120.55 14.7266 856.80 0.0000* 1221. 41 13.2565 860.56 10.3740 1129.67 15.6781 871.09 11. 5588 1131. 51 0.0000 8*73 .19 10.4088 1147.95 0.0000 875.33 0.0000 1173.23 15.8254 879.38 19.6929 1177.95 12 .1145 880.51 15.0635 1189.05' 12.1423 883.24 13. 9150 1204.77 15.9313 884.68 18.5599 1221.41 10.5314 889.28 20.9055 1231.02 7.5376 894.76 15 .1196 1235.36 0.0000 898.04 17.4609 1238.28 0.0000 900.72 17.4725 1260.41 . 0.0000 903.28 10.4905 1271.87 12.3502 911. 20 17.5195 1274.44 9.5050 912.08 17.5238 1274.54 12.3565 923.98 0.0000 1291.59 9.5374 926.50 7.9146 1298.22 0.0000 929 .11 15.8395 1312.11 0.0000 937.49 25.5732 1332.49 12.3055 944 .13 0.0000 1362. 66 0.0000 946.00 17.6740 1365.19 5.8041 949.00 9. 7281 1368. 63 0.0000 667.71 0.0000 1384.29 6.7958 962.31 21. 2944 1408.01 7.8008 964.08 14.202'6 1457.56 0.0000 966.17 17.0520 1460.82 4.9228 911.20 15.1085 1489.16 3.9583 968.97 15*.1085 1505.03 3. 9692 983.53 0.0000 1584.12 4.0237 984.45 0.0000 1596.21 0.0000 Page 3055 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:07:22.76 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;134 Background date : Z-OCT-2016 11:02:13. Sample.date 10-DEC-2015 14:05:00 Acquisition date : 3-0CT-2016 08:03:23. Sample ID G405235008 Sample quantity : l.47889E+02 GRAM Detector name GAM39 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:07.23 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 0 0 0 0 0 0 0 3 3 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3056 of 5809 Energy 46.75* 63.19* 72. 81 74.90* 77.17* 87.21 92.82* 129.55 153.90*

185.18* 209.61 217.41 238.66* 241. 62 270.81* 295.22* 299.64* 338.10* 352.09* 375. 96 411. 7 6 454.53 464. 96 511.52* 534.00 552.45 562. 62 583.26* 595.97 609.56* 663.04 669.35 693.49 808.79 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 50 1. 32 222 272 56 74 49 21 91 31 35 392 77 25 111 24 78 210 9 61 39 74 12 14 21 13 72 9 130 52 14 33 37 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 157 252 141 172 159 169 176 107 107 175 101 79 74 95 64 60 62 89 62 32 34 16 57 82 13 21 34 51 28 49 24 6 24 4 1. 60 1.10 1. 27 1.17 1. 08 1.17 1. 48 0.95 0.61 1. 55 0.98 0.74 1. 20 1. 83 1. 90 1. 56 1. 57 1.12 1. 44 1. 27 6.89 6.16 9.36 1. 73 1. 46 1. 27 1. 79 1. 59 1. 27 1. 22 2.17 1. 24 6.10 4.03 93.34 126.23 145.47 149.65 154.17 174.26 185.47 258.94 307.64 370.20 419.06 434.67 477.17 483.09 541.47 590.28 599.12 676.04 704.03 7 51. 77 823.38 908.93 929.79 1022.92 1067.88 1104. 78 1125.13 1166.40 1191. 82 1219.01 1325.97 1338.59 1386.88 1617.50 89 123 143 143 143 171 183 256 305 364 413 430 472 472 536 586 586 669 698 748 816 902 917 1016 1065 1099 1118 1160 1185 1214 1319 1335 1378 1610 8 1.39E-02 47.5 8 3.42E-04***** 16 8.84E-03 64.2 16 6.17E-02 12.1 16 7.56E-02 9.8 7 1.55E-02 40.8 8 2.05E-02 35.8 8 1.36E-02 39.1 8 5.81E-03 89.8 15 2.53E-02 34.0 10 8.56E-03 "64.0 9 9.66E-03 49.5 17 1.09E-01 6.4 17 2.15E-02 33.2 9 6.87E-03 62.7 21 3.09E-02 16.1 21 6.57E-03 65.0 14 2.15E-02 28.4 12 5.84E-02 10.5 8 2.42E-03115.6 17 1.69E-02 25.4 15 1.09E-02 26.8 28 2.06E-02 30.9 17 3. 24E-03201. 7 6 3.80E-03 50.2 11 5.72E-03 49.2 10 3.61E-03 89.4 12 2.00E-02 23.8 10 2.54E-03112.4 10 3.61E-02 13.3 17 1.45E-02 25.9 8 3.97E-03 39.6 20 9. lOE-03 41. 2 16 1. 03E-02 20. 5 Fit 8.87E-01 1.84E+OO 7. 31E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 860.71 30 14 2.16 1721.35 1715 11 8.40E-03 29.9 36 0 870. 96 14 12 1.14 1741.86 1736 10 3. 96E-03 53.1 37 0 881.92 27 23 8.82 1763.78 1749 23 7.50E-03 50.0 38 0 911.61* 55 26 1.16 1823.17 1816 13 1.52E-02 24.4 39 1 964.70 22 17 2.03 1929.37 1919 26 6.05E-03 42. 6 9.26E-01 40 1 969.17* 51 14 2.03 1938.30 1919 26 l.42E-02 22.5 41 0 1033.58 14 2 1.12 2067.13 2063 8 3.91E-03 31. 7 42 0 1120.49 23 25 1. 73 2241.00 2236 8 6.31E-03 39.4 43 0 1160. 33 18 3 1. 58 2320.67 2315 10 5.lOE-03 28.4 44 0 1175 .. 83 28 9 0.75 2351.69 2343 17 7.64E-03 30.9 45. 0 1228.04 9 7 0.90 2456.12 2453 8 2.39E-03 61. 6 46 0 1384.20 7 5 1. 35 2768.50 2763 10 *1. 94E-03 70.7 47 0 1460.83* 284 4 1. 75 2921. 78 2914 16 7.89E-02 6.3 4.8 0 1509.87 9 2 0.93 3019.90 3014 10 2.39E-03 48.3 49 0 1587.75 13 0 1. 53 3175.69 3170 11 3. 61E-03 27.7 50 0 1764.45 18 0 2. 02 3529.17 3524 10 5.00E-03 23.6 51 0 1887.13 4 3 1. 36 3774.60 3767 10 l.23E-03 82.2 Flag: "*" = Peak area was modified by background subtraction Page 3057 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:07:26 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title* Sample date Sample ID 10-DEC-2015 14:05:00 G405235008 Acquisition date Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:03:23 147.89 GRAM Sample type . Detector name : Elapsed live time: Energy tolerance Errors propagated: Efficiency type Abundance limit SOLID GAMMA39 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide PB-214 PB-214 PB-214 PB-214 'PB-214 PB-214 PB-214 PB-214 Page 3058 of 5809 Line 242.00 87;09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:07.23 10.00 0.00 % Peak Energy 0.2% Nuclide. Line Activity Report Page : 2 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Nuclide Type: Uncorrec'ted Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM . %Error Status K-40 1460.82 10.66* 8.984E-01 1.449E+Ol 1.449E+Ol 12.51 OK CD-109 88.03 3.70* 6.754E+OO 5.138E-01 8.037E-01 232.54 OK SN-126 64.28 9.60 6.932E+00 l.205E-02 1.205E-024690.27 OK 86.94 8.90 6.754E+OO 2.136E-01 2.136E-01 232.54 OK 87.57 37.00* 6.754E+00 5.138E-02 5.138E-02 232.54 OK BA-137M 661.66 89.90* 1.755E+OO 1.757E-01 l.790E-01 51.88 OK CS-137 661.66 85.10* 1.755E+OO l.856E-01 l.891E-01 51. 88 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* l.953E+OO 2.325E-01 2.325E-01 47.52 OK 860.56 12.50 1.416E+OO 8.818E-01 8.818E-01 59.82 OK PB-210 46.54 4.25* 6.842E+OO 1.145E+OO 1.174E+OO 94.92 OK BI-211 72.87 1.23 6.824E+OO 2.436E+OO 2.436E+OO 128.32 OK 351. 06 12.92* 3.013E+OO 3.292E-01 3.292E_:Ol 327.48 OK PB-212 74.82 10.28 6. 811E+OO 1.481E+OO l.481E+OO 35.42 OK 77 .11 17.10 6.799E+OO 1.497E+OO 1.497E+OO 19.65 OK 238.63 43.60* 4.211E+OO 1.242E+OO 1.242E+OO 12.83 OK 300.09 3.30 3.469E+OO 1.178E+OO 1.*178E+OO 130.01 OK BI-214 609.32 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 OK 1120.29 14.92 1. 13 6E:+-o 0 6.735E-01 6.737E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 OK PB-214 74.82 5.80 6.812E+OO Line Not Found <<INT Reject 77 .11 9.70 6.799E+OO 2.640E+OO 2. 641E+OO 19.65 OK 87.09 3.41 6.755E+OO Line Not Found <<INT Reject 242.00 7.25 4.163E+OO Line Not Found <<INT Reject 295.22 18.42 3.514E+OO 9.817E-01 9.821E-01 32.23 OK 351.93 35.60* 3.014E+OO Line Not Found <<J;NT Reject RN-222 609.32 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 OK 1120.29 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 OK RA-224 240.99 4.10* 4.168E+OO 8. 981E-01 8. 981E-01 204.49 OK RA-226 609.32 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 OK 1120.29 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11.27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 . OK 794.95 4.25 1.512E+OO Line Not Found Abserit 835.71 1. 61 1. 451E+OO Line Not Found Absent 911.20 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 OK 968. 97 15.80 1.284E+OO 1.288E+OO 1.288E+OO 44. 9.1 OK RA-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835.71 1. 61 1.451E+OO Line Not Found Absent 911.20 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 OK 968.97 15.80 1.284E+OO l.288E+OO 1. 288E+OO 44.91 OK TH-228 74.82 10.28 6.811E+OO 1.481E+OO L 481E+OO 35.42 OK 77 .11 17.10 6.799E+OO 1.497E+OO 1.497E+OO 19.65 OK 238.63 43.60* 4.211E+OO 1.242E+OO 1.242E+OO 12.83 OK 300.09 3.30 3.469E+OO l.178E+OO 1.178E+OO 130.01 OK Page 3059 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 1.882E+OO 8.lOOE-01 8.lOOE-01 26.57 OK 1120.29 14.92 1.136E+OO 6.735E-01 6.735E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 OK TH-232 105.21 1.10 6.612E+OO Li.ne Not Found Absent 338.32 11.27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 OK 835.71 1. 61 1.451E+OO Line Not Found Absent 911.20 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 OK 968. 97 15.80 1.284E+OO 1.288E+OO 1.288E+OO 44.91 OK TH-234 63.29 3.70* 6.932E+OO 3.126E-02 3.126E-024690.27 OK 92.59 4.23 6. 722E+OO 1.635E+OO 1.635E+OO 71. 63 OK U-234 609.32 45.49* 1.882E+OO 8.lOOE-01 8.lOOE-01 26.57 OK 1120.29 14.92 1.136E+OO 6.735E-01 6.735E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 OK U-238 63.29 3.70* 6.932E+00 3.126E-02 3.126E-024690.27 OK 92.59 4.23 6.722E+OO 1.635E+00 1. 635E+OO 71. 63 OK PU-239 129.30 0.01* 6.237E+OO 7.647E+02 7.647E+02 78.19 OK 375.05 0.00 2.845E+00 1.099E+03 1.099E+03 231.16 OK 413.71 0.00 2.617E+OO Line Not Found Absent AM-243 43.53 5.90 6.236E+OO Line Not Found Absent 74.66 67.20* 6.811E+OO 2.266E-01 2.266E-01 35.42 OK ANH-511 511. 00 100.00* 2 .181E+OO 2.903E-02 2.903E-02 403.36 OK Flag: "*" = Keyline Page 3060 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:07:28.43

GEL Laboratories LLC *
2040 Savage Road * "* Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l * *Acquisition date 3-0CT-2016 08:03:23 Sensitivity : 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit :* 75.000 * *Elapsed real time: 0 01:00:07.23 Half life ratio : ***** *
Sample date 10-DEC-2015 14:05:00 Analyst initials: MXRl *
Sample ID G405235008 Sample Quantity l.4789E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ) ( 1. 96-sigma) (pCi/GRAM ) K-40 1.449E+Ol 1.777E+OO 8 .112E-01 CD-109 8.037E-01. 1.832E+OO 2.195E+OO SN-126 5.138E-02 l. l 71E-01 1.308E-01 BA-137M 1.790E-01 9.lOlE-02 7.925E-02 CS-137 1.891E-01 9.614E-02 8.372E-02 TL-208 2.325E-01 l.083E-01 8.491E-02 PB-210 1.174E+OO 1.092E+OO 9.860E-01 BI-211 3.292E-01 l.057E+OO 4.359E-01 PB-212 l.242E+00 1.561E-01 1. lllE-01 BI-214 8.103E-01 2. llOE-01 1.622E-01 PB-214 1.102E+OO 2.257E-01 3.711E-01 RN-222 8.103E-01 2. llOE-01 l.622E-01 RA-224 8. 981E-01 1. 800E+OO 1.192E+OO RA-226 8.103E-01 2 .. llOE-01 AC-228 8.054E-01 3.855E-01 3 .191E-01 RA-228 8.054E-01 3.855E-01 3 .191E-01 TH-228 l.242E+00 1.561E-01 1. lllE-01 TH-230 8.lOOE-01 2.109E-01 1.621E-01 TH-232 8.054E-01 3.855E-01. 3 .191E-01 TH-234 3.126E-02 1.437E+OO 1.238E+OO U-234 8.lOOE-01 2.109E-01 1. 621E-01 U-238 3.126E-02 1.437E+OO l.238E+OO PU-239 7.647E+02 5.860E+02 6.159E+02 AM-243 2.266E-01 7.864E-02 6.463E-02 ANH-511 2.903E-02 l.147E-01 6.277E-02. Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3061of5809 Key-Line Activity (pCi/GRAM 3.700E+OO 1.582E-03 O.OOOE+OO 8.283E-03 1.544E-01 K.L. Cnt Uncert ( 1. 96-sigma) 1.362E+Ol 5.716E-02 1. 960E+41 3.889E-02 4.379E-01 MDA (pCi/GRAM 2.698E+Ol l.145E-01 O.OOOE+OO 8.760E-02 9. lllE-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.467E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 5.071E+02 O.OOOE+OO SHORT HLIF MN-54 -2.318E-02 7.886E-02 1.514E-01 NOT IDENT. C0-56 -2.644E-01 5.683E-01 1. 066E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 l.366E-02 4.783E-02 8.895E-02 NOT IDENT. C0-58 6.019E-01 6.532E-01 1.490E+OO NOT IDENT. FE-59 2.132E-01 6.512E+OO 1. 349E+Ol NOT IDENT. C0-60 -3.340E-03 4.175E-02 8.481E-02 NOT IDENT. ZN-65 -7.592E-02 2.510E-01 4.065E-01 NOT IDENT. GE-68 1. 875E-01 3. lOlE+OO 6.185E+OO NOT IDENT. AS-73 1.305E-01 2.674E+OO 5.00lE+OO NOT IDENT. AS-74 O.OOOE+OO 1.055E+04 O.OOOE+OO SHORT HLIF SE-75 2.219E-01 2.-432E-01 5.059E-01 NOT IDENT. BR-77 O.OOOE+OO 1.531E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.059E+02 O.OOOE+OO SHORT HLIF RB-83 4.312E-02 7.892E-01 1.517E+OO FAIL ABUN KR-85 4.428E+OO 8.639E+OO 1. 731E+Ol NOT IDENT. SR-85 4.578E-01 8.931E-01 1. 789E+OO NOT IDENT. RB-86 O.OOOE+OO 3.395E+04 O.OOOE+OO SHORT HLIF Y-88 -1.521E-02 2.493E-01 5.313E-01 NOT IDENT. Y-91 6.165E+Ol 6.898E+02 l.360E+03 NOT IDENT. NB-94 7.994E-03 4.165E-02 7.975E-02 FAIL ABUN NB-95 -6.481E-01 1.134E+OO 1.916E+OO NOT IDENT. NB-95M 2.790E+00 2.797E+OO 5.364E+OO NOT IDENT. ZR-95 1.184E+OO 1.798E+OO 3.723E+OO NOT IDENT. NB...:97
O.OOOE+OO l.657E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.439E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.315E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2. 661E-03 4.124E-02 6.760E-02 NOT IDENT. RH-102 3.605E-02 6.848E-02 1.413E-01 NOT IDENT. RU-103 2.292E+OO 6.649E+OO 1.327E+Ol FAIL ABUN RH-106 -7.648E-02 6.488E-01 1.203E+OO NOT IDENT. RU-106 -7.648E-02 6.488E-01 1.203E+OO NOT IDENT. AG-108M -l.319E-02 2.899E-02 5.281E-02 NOT IDENT. AG-llOM 3.183E-02 1.457E-01 2.676E-01 FAIL ABUN SN-113 -2. 081E-02 2.744E-01 5.218E-01 NOT IDENT. CD-115 O.OOOE+OO 2.009E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9. 913E+04 O.OOOE+OO SHORT HLIF TE-123M 5.890E-03 l.393E-01 2.645E-01 NOT IDENT. SB-124 1.653E+OO 2.049E+OO 5.536E+OO NOT IDENT. SB-125 -5.299E-02 1.243E-01 2.259E-01 NOT IDENT. TE-125M -7.003E+Ol 2.762E+02 4.901E+02 NOT IDENT. I-126 O.OOOE+OO 6.358E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.277E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.434E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.927E+09 O.OOOE+OO SHORT HLIF I-132 0 :OOOE+OO 4.267E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.028E+26 O.OOOE+OO SHORT HLIF BA-133 -9.803E-03 5.528E-02 9.266E-02 NOT I DENT.
I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.874E-02 7.077E-02 1.476E-01 FAIL ABUN CS-135 -8.423E-02 1. 764E-01 2.891E-01 NOT IDENT. I-135 O.OOOE+OO 1. 552E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.474E+05 O.OOOE+OO SHORT HLIF CE-139 -8.275E-02 1.131E-01 2.114E-01 NOT IDENT. BA-140 O.OOOE+OO 1.509E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.638E+05 O.OOOE+OO SHORT HLIF CE-141 -1. 571E+Ol 2.454E+Ol 4.663E+Ol NOT IDENT. CE-143. O.OOOE+OO 9.757E+40 O.OOOE+OO SHORT HLIF . CE-144 2.523.E-01 4.242E-01 7.943E-01 NOT IDENT. PM-144 3.898E-03 6.171E-02 l.187E-01 NOT IDENT. PR-144 3.382E-01 5.354E+OO 1.030E+Ol NOT IDENT. PM-146 0.000E+OO 8.015E-02 l.067E-01 FAIL ABUN ND-147 *o.OOOE+OO 3.842E+07 O.OOOE+OO SHORT HLIF PM-147 -4.548E+02 8.518E+02 l.466E+03 NOT IDENT. PM-149 O.OOOE+OO 2.847E+40 O.OOOE+OO SHORT HLIF EU-'-150 -4.633E-03 2.973E-02 5.055E-02 FAIL ABUN EU-152 4.066E-03 1.131E-01 2.089E-01 FAIL ABUN GD-153 -2.382E-01 2.075E-01 3.089E-01 NOT IDENT. EU-154 6.934E-03 l.409E-01 2.832E-01 NOT IDENT. EU-155 3.278E-02 1.168E-01 2.159E-01 FAIL ABUN TB-160 4.738E-01 2.158E+OO 4.395E+OO FAIL ABUN H0-166M 4. 661E-03 6.804E-02 l.301E-01 FAIL ABUN TM-171 -2.266E-01 5.845E+OO 1. 089E+Ol NOT IDENT. HF-172 l.805E-01 2. 778E-01 4.889E-01 FAIL ABUN LU-172 -5. 872E-02 8.580E-02 1.515E-01 FAIL ABUN Page 3062 of 5809 LU-176 -2.576E-02 2.683E-02 4.501E-02 FAIL ABUN HF-181 1.594E+OO 4.821E+00 9.668E+OO NOT IDENT. TA-182 *1. 301E+OO 1.153E+00 *2. 620E+OO FAIL ABUN RE-183 -5.289E-01 1.231E+OO 2.220E+OO NOT IDENT. RE-184 8.884E+OO 3.801E+Ol 7.801E+Ol NOT IDENT. W-188 -l.235E+02 L 4 60E+02 2.257E+02 FAIL ABUN IR-192 -1.293E-01 5.466E-01 l.029E+OO FAIL ABUN HG-203 7.372E-01 2.945E+OO 5.769E+OO FAIL ABUN BI-207 4.104E-02 6.548E-02 1.399E-01 FAIL ABUN PB-211 4.073E-01 7.909E-01 1.548E+OO NOT IDENT. BI-212 -:4.087E-02 6.376E-01 l.190E+OO NOT IDENT. RN-219 1.161E-01 4.444E-01 8.780E-01 FAIL ABUN RA-223 -1.003E-01 7. 311E-01. 1.384E+OO FAIL ABUN AC-227 -l.829E-02 2.469E-01 *4.781E-01 FAIL ABUN TH-227 -1.829E-02 2.469E-01 4. 78 lE-01 FAIL ABUN TH-229 2.750E-02 4.927E-01 9.700E-01 FAILABUN PA-231 2.686E-01 5.359E-01 l.072E+OO NOT IDENT. TH-231 -1.003E-01 7. 311E-01 1.384E+OO FAIL ABUN PA-233 5.629E-04 6. 771E-02 1. 311E-01 FAIL ABUN PA-234 -7.937E-02 3.624E-01 6.983E-01 FAIL ABUN PA-234M -1.304E+OO 5.456E+OO 1.058E+Ol NOT IDENT. U-235 l.313E-02 1.897E-01 3.77-SE-01 FAIL ABUN NP-237 5.629E-04 6.771E-02 1. 311E-01 FAIL ABUN NP-238 O.OOOE+OO 1.900E+41 O.OOOE+OO SHORT HLIF NP-239 -8.397E-02 2.566E-01 4.509E-01 NOT IDENT. AM-241 4.371E-02 7.067E-02 1.263E-01 NOT IDENT. CM-243 -4. 231E-02 1.013E-01 1.776E-01 NOT IDENT . . BK-247 9. 072E-02 8.940E-02 1.808E-01 NOT IDENT. CM-247 -3.040E-02 4.226E-02 7.421E-02 NOT IDENT. CF-249 7.471E-03 4.250E-02 8.354E-02 NOT IDENT. CF-251 l.046E-02 1.315E-01 2.587E-01 NOT IDENT. Page 3063 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:07:24.23 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 273 10.66* 8.984E-01 1.449E+Ol 1.449E+Ol 12.51 CD-109 88.03 70 3.70* 6.754E+OO 1.419E+OO 2.219E+OO 81. 68 SN-126 64.28 2 9.60 6.932E+OO l.205E-02 l.205E-02 4690.27 86.94 70 8.90 6.754E+OO 5.898E-01 5.898E-01 81. 68 87.57 70 37.00* 6.754E+OO l.419E-01 l.419E-01 81. 68 BA-137M 661.66 55 89.90* 1. 755E+00 l.757E-01 l.790E-01 51. 88 CS-137 661.66 55 85.10* 1.755E+OO l.856E-01 1. 891E-01 51. 88 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 76 85.00* 1.953E+OO 2.325E-01 2.325E-01 47.52 860.56 31 12.50 1.416E+OO 8.818E-01 8.818E-01 59.82 PB-210 46.54 66 4.25* 6.842E+OO 1.145E+OO l.174E+OO 94.92 BI-211 72. 87 40 1.23 6.824E+00 2.436E+00 2.436E+OO 128.32 351. 06 233 12.92* 3.013E+OO 3.034E+OO 3.034E+OO 20.91 PB:-212 74.82 281 10.28 6. 811E+OO 2.035E+OO 2.035E+OO 24.24 77 .11 343 17 .10 6.799E+OO 1.497E+OO 1.497E+OO 19.65. 238.63 449 43.60* 4.211E+OO l.242E+00 1.242E+OO 12.83 300.09 27 3.30 3.469E+OO 1.178E+OO 1.178E+00 130.01 BI-214 609.32 137 45.49* l.882E+00 8.lOOE-01 8.103E-01 26.57 1120.29 22 14.92 l.136E+00 6.735E-01 6. 737E-01
78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 PB-214 74.82 281 5 .. 80 6.811E+00 3.607E+OO 3.608E+OO 24.24 77 .11 343 9.70 6.799E+OO 2.640E+OO 2. 641E+OO 19.65 87.09 70 3.41 6.754E+OO 1.539E+OO l.540E+00 81. 68 242.00 89 7.25 4.168E+OO 1.490E+OO 1.490E+OO 66.41 295.22 125 18.42 3.514E+00 9.817E-01 9. 821E-01 32.23 351.93 233 35.60* 3.013E+00 1.101E+OO 1.102E+OO 20.91 RN-222 609.32 137 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 . 1120. 29 22 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 RA-224 240.99 89 4.10* 4.168E+00 2.634E+OO 2.634E+OO 66.41 RA-226 609.32 137 45.49* l.882E+00 8.lOOE-01 8.103E-01 26. 57 1120.29 22 14.92 l.136E+00 6.735E-01 6.737E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 86 11. 27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 794.95 ------4.25 i.512E+OO ------Line Not Found ------835.71 ------1. 61 l.451E+OO ------Line Not Found ------911. 20 55 25.80* 1. 350E+OO 8.054E-01 8.054E-01 48.84 968. 97 51 15.80 1.284E+OO l.288E+OO l.288E+OO 44.91 RA-228 105.21 ------. 1.10 6.612E+00 ------Line Not Found ------338.32 86 11. 27 3.122E+OO . 1. 243E+OO 1.243E+OO 56.75 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 55 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 968.97 51 15.80 1.284E+OO l.288E+OO 1.288E+OO 44.91 TH-228 74.82 281 10.28 6. 811E+OO 2.035E+00 2.035E+OO 24.24 77 .11 343 17.10 6.799E+OO 1.497E+OO 1.497E+OO 19.65 Page 3064 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 449 43.60* 4.211E+OO 1.242E+OO 1.242E+OO 12.83 300.09 27 3.30 3.469E+OO 1.178E+OO 1.178E+OO 130.01 TH-230 609.32 137 45.49* 1.882E+OO 8.lOOE-01 8.lOOE-01 26. 57 1120.29 22 14.92 l.136E+OO 6.735E-01 6.735E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 86 11.27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 835.71 ------1. 61 1. 451E+OO ------Line Not Found ------911. 20 55 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 968. 97 51 15.80 1.284E+OO 1.288E+OO 1.288E+OO 44.91 TH-234 63.29 2 3.70* 6.932E+OO 3.126E-02 3.126E-02 4690.27 92.59 92 4.23 6.722E+OO 1.635E+OO 1.635E+OO 71. 63 U-234 609.32 137 45.49* 1.882E+OO 8.lOOE-01 8.lOOE-01 26. 57 1120.29 22 14.92 1.136E+OO 6.735E-01 6.735E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 U-238 63.29 2 3.70* 6.932E+OO 3.126E-02 3.126E-02 4690.27 92.59 92 4.23 6.722E+OO 1.635E+OO 1.635E+OO 71. 63 PU-239 129.30 59 0.01* 6.237E+OO 7.647E+02 7.647E+02 78.19 375.05 10 0.00 2.845E+OO 1.099E+03 l.099E+03 231.16 413.71 ------0.00 2.617E+OO ------Line Not Found ------AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 281 6. 811E+OO 3 .113E-01 3 .113.E-01 24.24 ANH-511 511. 00 12 100.00* 2.181E+OO 2.903E-02 2.903E-02 403.36 Flag: "*" Key line Page 3065 of 5809 Summary of Nuclide Activity Sample ID : G405235008 Acquisition date Page : 3 3-0CT-2016 08:03:23 Total number of lines in spectrum 51 . Number of unidentified lines 12 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 PU-239 AM-243 ANH-511 Hlif e 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y 1.41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 24110. OOY 7370.00Y l.OOE+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 449E+Ol l.419E+OO 1.419E-01 1. 757E-01 l.856E-01 2.325E-01 l.145E+OO 3.034E+OO l.242E+00 8.lOOE-01 l.101E+OO 8.lOOE-01 2.634E+OO 8.lOOE-01 8.054E-01 8 .'054E-:-01 l.242E+OO 8.lOOE-01 8.054E-01 3.126E-02 8.lOOE-01 3.126E-02 7.647E+02 3 .113E-01 2.903E-02 7.986E+02 7.986E+02 Decay Corr pCi7GRAM 1.449E+Ol 2. 2t9E+OO 1.790E-01 1. 891E-0'1 2.325E-01 l.174E+OO 3.034E+OO 1.242E+OO 8.103E-01 1.102E+OO 8.103E-01 2.634E+OO 8.103E-01 8.054E-01 8.054E-01 1.242E+OO 8.lOOE-01 8.054E-01 3.126E-02 8.lOOE-01 3.126E-02 7.647E+02 3 .113E-01 2.903E-02 7.995E+02 7.995E+02 76.47% Decay Corr 2-Sigma Error 0.181E+Ol 1.812E+OO l.159E-01 0.929E-01 0.981E-01 1.105E-01 1.114E+OO 0.634E+OO 0.159E+00 2.153E-01 0.230E+OO 2.153E-01 1. 749E+00 2.153E-01 3.933E-01 3.933E-01 0.159E+00 2.153E-01 3.933E-01 146.6E-02 2.152E-01 146.6E-02 5.980E+02 0.755E-01 11.71E-02 "M" Manually accepted 2-Sigma %Error 12.51 81. 68 81. 68 51. 88 51. 88 47.52 94.92 20.91 12.83 26.57 20.91 26.57 66.41 26.57' 48.84 48.84 12.83 26.57 48.84 4690.27 26.57 4690.27 78.19 24.24 403.36 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3066 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235008 Acquisition date : 3-0CT-2016 08:03:23 It Energy Area Bkgnd. FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 153.90 25 128 0.61 307.64 305 8 5.81E-03 **** 5.75E+OO T 0 185.18 107 205 1. 55 370.20 364 15 2.53E-02 67.9 5.12E+OO T 0 209.61 36 117 0.98 419.06 413 10 B.56E-03 **** 4.67E+00 T 0 217.41 40 92 0.74 434.67 430 9 9.66E-03 98.9 4.54E+00 0 270.81 28 73 1. 90 541.47 536 9 6.87E-03 **** 3.79E+OO T 0 411.76 67 37 6.89 823.38 816 17 1. 69E-02 50.7 2.63E+OO T 0 454.53 43 17. 6.16 908.93 902 15 1. 09E-02 53.6 2.41E+OO T 0 464. 96 80 61 9.36 929.79 917 28 2.06E-02 61. 8 2.37E+00 0 534.00 15 14 1. 46 1067.88 1065 6 3.80E-03 **** 2.lOE+OO 0 552.45 22 23 1. 27 1104. 78 1099 11 5.72E-03 98.3 2.04E+OO T 0 562.62 14 36 1. 79 1125.13 1118 10 3. 61E-03 **** 2.0lE+OO T 0 595.97 10 29 1.27 1191. 82 1185 10 2.54E-03 **** 1.92E+OO T 0 669.35 15 6 1. 24 1338.59 1335 8 3. 97E-03. 79.1 1. 74E+OO 0 693.49 34 25 6.10 1386.88 1378 20 9.lOE-03 82.3 1. 69E+OO 0 808.79 38 4 4.03 1617.50 1610 16 1.03E-02 40.9 1. 49E+OO T 0 870.96 14 12 1.14 1741.86 1736 10 3. 96E-03 **** 1.40E+OO T 0 881.92 27 23 8.82. 1763.78 1749 23 7.50E-03 **** 1.39E+OO T 1 964.70 22 17 2.03 1929.37 1919 26 6.05E-03 85.2 l.29E+OO T 0 1033.58 14 2 1.12 2067.13 2063 8 3.91E-03 63.5 1.22E+OO 0 1160. 33 18 3 1. 58 2320.67 2315 10 5.lOE-03 56.9 1.lOE+OO 0 1175.83 27 8 0.75 2351.69 2343 17 7.64E-03 61. 8 1. 09E+OO 0 1228.04 8 7 0.90 2456.12 2453 8 2.39E-03 **** 1. 05E+OO 0 1384. 20 7 5 1. 35 2768.50 2763 10 1.94E-03 **** 9.44E-01 T 0 1509.87 8 2 0.93 3019.90 3014 10 2.39E-03 96. 7 8.71E-01 0 1587.75 12 0 1. 53 3175.69 3170 11 3.61E-03 55.5 8.31E-01 0 1887.13 4 2 1. 36 3774.60 3767 10 1.23E-03 **** 6.98E-01 Flags: "T" = Tentatively associated Page 3067 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:07:55.80 *******************************************************************************
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Charlestonf SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l *
Acquisition date 3-0CT-2016 08:03:23 Sensitivity 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:07.23 Half life ratio : ***** *
Sample date 10-DEC-2015 14:05:00 Nuclide Library : SOLID *
Sample ID G405235008 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4789E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA. GAMMA] E.FF GAM39* CAN. CNF; 4 . * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nu.elide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 PU-2'.39 AM-243 ANH-511 Le (pCi/GRAM 3.335E-01 1.052E+OO 6.250E-02 3.510E-02 3.708E-02 3.822E-02 4.668E-01 l.997E-01 5.165E-02 7.288E-02 1.790E-01 7.288E-02 5.541E-01 '7.288E-02 1.396E-01 1. 396E-01 5.165E-02 7.286E-02 1. 396E-01 5.902E-01 7.286E-02 5.902E-01 2.895E+02 3. 072E-02 2.815E-02 ----Non-Identified Nuclides Nu.elide BE-7 NA-22 NA-24 AL-26. SC-46 V-48
Page 3068 of 5809 Le (pCi/GRAM 1.207E+Ol 4.879E-02 0.000E+OO 3.437E-02 3. 961E-01 O.OOOE+OO NOT IDENT. NOT IDENT.
SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M .RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3069 of 5809 O.OOOE+OO 6.639E-02 4.626E-01 O.OOOE+OO 4.162E-02 6.582E-01 5.643E+OO 3.452E-02 L 7 52E-01 2.699E+OO 2.368E+OO O.OOOE+OO 2.353E-01 0.000E+OO O.OOOE+OO 6.784E-01 7.863E+OO 8.129E-01 0 .. OOOE+OO 1. 989E-01 5.950E+02 3.568E-02 8.452E-01 2. 511E+OO 1. 656E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.178E-02 6.266E-02 5. 969E+OO 5.350E-01 5.350E-01 2.328E-02 1.180E-01 2.370E-01 O.OOOE+OO O.OOOE+OO 1. 236E-01 2.197E+OO 1.015E-01 2.301E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.227E-02 O.OOOE+OO 6. 667E-02 . 1.328E-01 O.OOOE+OO O.OOOE+OO 9.834E-02 O.OOOE+OO O.OOOE+OO 2.187E+Ol O.OOOE+OO 3.753E-01 5 .196E-02 4.509E+OO 4.837E-02 0.000E+OO 6.835E+02 O.OOOE+OO 2.289E-02 9.539E-02 l.456E-01 l.208E-01 l.021E-01 1.908E+OO 5. 722E-02 5.146E+OO 2.307E-01 6.289E-02 2.026E-02 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT I DENT .. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. *SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN *NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-..211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3070 of 5809 4.335E+OO 1.162E+OO 1.052E+OO 3.443E+Ol 1.032E+02 4. 718E-01 2.685E+OO 6 .196E-02 7.036E-01 5.302E-01 3.989E-01 6.370E-01 2.200E-01 2.200E-01 4.520E-01 4.976E-01 6.370E-01 6.002E-02 3.048E-01 4.627E+OO 1.777E-01 6.002E-02 O.OOOE+OO 2 .113E-01 6.022E-02 8.343E-02 8.423E-02 3.343E-02 3.787E-02 1.214E-01 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:08:01.36 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA . *' * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l *
Acquisition date 3-0CT-2016 08:03:23 Sensitivity : 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:07.23 Half life ratio : ***** *
Sample date 10-DEC-2015 14:05:00 Nuclide Library SOLID *
Sample ID G405235008 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity 1.4789E+02 GRAM *
Quantity Err(%) l.3524E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN * ** Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) K-40 l.449E+Ol 1. 931E+OO l.931E+OO CD-109 8.037E-01 1. 841E+OO 1. 841E+OO SN-126 5.138E-02 l.177E-01 1.177E-01 BA-137M l.790E-01 9 .134E-02 9.134E-02 CS-137 l.891E-01 9.649E-02 9.649E-02 TL-208 2.325E-01 l.087E-01 l.087E-01 PB-210 l.174E+OO 1. 096E+OO 1. 096E+OO BI-211 3.292E-01 1.070E+OO 1. 070E+OO PB-212 1. 242E+OO 1.694E-01 l.694E-01 BI-214 8.103E-01 2.139E-01 2.139E-01 PB-214 1.102E+OO 2.303E-01 2.303E-01 RN-222 8.103E-01 2 .139E-01 2.139E-01 RA-224 8.981E-01 1.804E+OO 1. 804E+OO 8.103E-01 2.139E-01 2.139E-01 AC:--228 8.054E-01 3.877E-01 3.877E-01 RA-228 8.054E-01 3.877E-01 3.877E-01 TH-228 1.242E+OO l.694E-01 1.694E-01 TH-230 8.lOOE-01 2.138E-01 2.138E-01 TH-232 8.054E-01 3.877E-01 3.877E-01 TH-234 3.126E-02 1.437E+OO 1.437E+OO U-234 8.lOOE-01 2.138E-01 2 .138E-01 U-238 3.126E-02 1.437E+OO 1.437E+OO PU-239 7.647E+02 5.870E+02 5.870E+02 AM-243 2.266E-01 8.058E-02 8.058E-02 ANH-511 1.148E-01 1.148E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma ) (1. 96-sigma) BE-7 3.700E+OO .1. 362E+Ol 1. 372E+Ol NOT IDENT. NA-22 l.582E-03 5. 716E-02 5.717E-02 NOT IDENT. NA-24 l.000E+41 2.556E+43 O.OOOE+OO SHORT HLIF AL-26 8. 283K'-03 3.889E-02 3.907E-02 NOT IDENT. SC-46 1.544E-01 4.379E-01 4.434E-01 FAIL ABUN Page 3071 of 5809 V-48 l.063E+04 l.468E+04 l.544E+04 SHORT HLIF CR-51 -5.832E+Ol 5.071E+02 5.078E+02 SHORT HLIF MN-54 -2.318E-02 7.886E-02 7.955E-02 NOT IDENT. C0-56 -2.644E-01 5.684E-01 5. 80.8E-01 NOT IDENT. MN-56 -l.OOOE+41 2.187E+41 O.OOOE+OO SHORT HLIF C0-57 l.366E-02 4.783E-02 4.822E-02 NOT IDENT. C0-58 6.019E-01 6.537E-01 7.078E-01 NOT IDENT. FE-59 2.132E-01 6.512E+OO 6.513E+OO NOT IDENT. C0-60 -3.340E-03 4.175E-02 4.177E-02 NOT IDENT. ZN-65 -7.592E-02 2.510E-01 2.533E-01 NOT IDENT. GE-68 1. 875E-01 3 .101E+OO 3.102E+OO NOT IDENT. AS-73 l.305E-01 2.674E+OO 2.675E+OO NOT IDENT. AS-74 4.791E+03 1.056E+04 l.078E+04 SHORT HLIF SE-75 2.219E-01 2.434E-01 2.631E-01 NOT IDENT. BR-77 1.218E+38 1.047E+39 O.OOOE+OO SHORT HLIF SR-82 1. 68 9E+02 8.059E+02 8.095E+02 SHORT HLIF RB-83 4.312E-02 7.892E-01 7.894E-01 FAIL ABUN KR-85 4.428E+OO 8. 641E+OO 8.869E+OO NOT IDENT. SR-85 4.578E-01 8.933E-01 9.168E-01 NOT IDENT. RB-86 l.566E+04 3. 396E+04 3.468E+04 SHORT HLIF Y-88 -l.521E-02 2.493E-01 2.494E-01 NOT IDENT. Y-91 6.165E+Ol 6.898E+02 6.903E+02 NOT IDENT. NB-94 7.994E-03 4.165E-02 4.180E-02 FAIL ABUN .NB-95 -6.481E-01 l.134E+00 l .171E+OO NOT IDENT. NB-95M 2.790E+OO 2.806E+OO 3.075E+OO NOT IDENT. ZR-95 1.184E+OO 1. 799E+OO l.877E+OO NOT IDENT. NB-97 1.000E+41 1. 658E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 l.439E+41 O.OOOE+OO SHORT HLIF M0-99 -5.484E+31 1.315E+32 0.000E+OO SHORT HLIF TC-99M -1.000E+41 4.182E+41 O.OOOE+OO SHORT HLIF RH-101 -2.661E-03 4.125E-02 4.126E-02 NOT IDENT. RH-102 3.605E-02 6.854E-02 7.044E-02 NOT IDENT. RU-103 2.292E+OO 6.650E+OO 6.730E+OO FAIL ABUN RH-106 -7.648E-02 6.489E-01 6.498E-01 NOT IDENT. RU-106 -7.648E-02 6.489E-01 6.498E-01 NOT IDENT. AG-108M -l.319E-02 2.900E-02 2. 960E--02 NOT IDENT. AG-llOM 3.183E-02 l.457E-01 1.464E-01 FAIL ABUN SN-113 -2.081E-02 2.744E-01 2.746E-01 NOT IDENT. CD-115 2.413E+38 2.010E+39 O.OOOE+OO SHORT HLIF SN-117M 2.909E+03 9.913E+04 9.913E+04 SHORT HLIF .TE-123M 5.890E-03 1.393E-01 l.394E-01 NOT IDENT. SB-124 l.653E+OO 2. 051E+OO 2.182E+OO NOT IDENT. SB-125 -5.299E-02 1.243E-01 1. 2 66E-01 NOT IDENT. TE-125M -7'.003E+Ol 2.762E+02 2.780E+02 NOT IDENT. I-126 l.392E+06 6.630E+05 9 .130E+05 SHORT HLIF SB-126 -7.973E+05 l.286E+06 l.335E+06 SHORT HLIF SB-127 -3.168E+20 2.434E+22 O.OOOE+OO SHORT HLIF I-131 -2.939E+08 4.927E+09 4.929E+09 SHORT HLIF I-132 l.OOOE+41 1. 836E+42 O.OOOE+OO SHORT HLIF TE-132 2.547E+25 3.029E+26 O.OOOE+OO SHORT HLIF BA-133 -9.803E-03 5.528E-02 5.546E-02 NOT IDENT. I-133 -1. OOOE+41 2.749E+41 O.OOOE+OO SHORT HLIF CS-134 3.874E-02 7.079E-02 7.292E-02 FAIL ABUN CS-135 -8.423E-02 1. 764E-01 1.805E-01 NOT IDENT. I-135 -l.OOOE+41 6.905E+41 O.OOOE+OO SHORT HLIF CS-136 -1.289E+05 3.477E+05 3.525E+05 SHORT HLIF CE-139 -8.275E-02 l.143E-01 l.203E-01 NOT IDENT. BA-140 2.024E+05 l.509E+06 l.512E+o6 SHORT HLIF LA-140 2.085E+05 4.639E+05 4.733E+05 SHORT HLIF CE-141 -l.571E+Ol 2.455E+Ol 2.555E+Ol NOT IDENT.
CE-143 1.000E+41 9.810E+40 O.OOOE+OO SHORT HLIF CE-144 2.523E-01 4.245E-01 4.394E-01 NOT IDENT. PM-144 3.898E-03 6.171E-02 6.173E-02 NOT IDENT. PR-144 3.382E-01 5.354E+OO 5.356E+OO NOT IDENT. PM-146 l.527E-01 8.091E-02 l.062E-01 FAIL ABUN ND-147 -l.0'.39E+06 3.842E+07 3.843E+07 SHORT HLIF PM-147 -4.548E+02 8. 521E+o2 8.764E+02 NOT IDENT. PM-149 -8.392E+39 2.853E+40 0.000E+OO SHORT HLIF EU-150 -4.633E-03 2.973E-02 2. 981E-02 FAIL ABUN EU-152 4.066E-03 l.131E-01 l.132E-01 FAIL ABUN GD-153 -2.382E-01 2.080E-01 2.340E-01 NOT IDENT. EU-154 6.934E-03 1.409E-01 l.410E-01 NOT IDENT. EU-155 3.278E-02 l.169E-01 l.178E-01 FAIL ABUN TB-160 4.738E-01 2.159E+OO 2.169E+OO FAIL ABUN H0-166M 4. 661E-03 6.804E-02 6.808E-02 FAIL ABUN TM-171 -2.266E-01 5.845E+OO 5.846E+OO NOT IDENT. HF-172 1. 805E-01 2.793E-01 2.909E-01 FAIL ABUN LU-172 -5. 872E-02 8.601E-02 8.999E-02 FAIL ABUN Page 3072 of 5809 LU-176 -2.576E-02 2.686E-02 2.926E-02 FAIL ABUN HF-181 1.594E+OO 4.822E+OO 4.875E+OO NOT IDENT. TA-182 l.301E+OO 1.154E+OO 1. 294E+OO FAIL ABUN RE-183 -5.289E-01 1.234E+OO 1.257E+OO NOT IDENT. RE-184 8.884E+00 3.807E+Ol 3.828E+Ol NOT IDENT. W-188 -l.235E+02 1.467E+02 l.569E+02 FAIL ABUN IR-192 -l.293E-01 5.466E-01 5.497E-01 FAIL ABUN HG-203 7.372E-01 2.946E+OO 2. 964E+OO FAIL ABUN BI-207 4.104E-02 6.550E-02 6.806E-02 FAIL ABUN PB-211 4.073E-01 7.912E-01 8.122E-01 NOT IDENT. BI-212 -4.087E-02 6.376E-01 6.379E-01 NOT IDENT. RN-219 l.161E-01 4.446E-01 4.477E-01 FAIL ABUN RA-223 -1.003E-01 7. 311E-01 7.325E-01 FAIL ABUN AC-227 -1.829E-02 2.470E-01 2.471E-01 FAIL ABUN TH-227 -1. 829E-02 2.470E-01 2.471E-01 FAIL ABUN TH-229 2.750E-02 4.927E-01 4.929E-01 FAIL ABUN PA-231 2.686E-01 5.389E-01 5.524E-01 NOT IDENT. TH-231 -l.003E-01 7. 311E-01 7.325E-01 FAIL ABUN PA-233 5.629E-04 6.771E-02 6. 771E-02 FAIL ABUN PA-234 -7.937E-02 3.736E-01 3.753E-01 FAIL ABUN PA-234M -1.304E+OO 5.456E+OO 5.487E+OO NOT IDENT. U-235 1. 313E-02 1. 897E-01 l.898E-01 FAIL ABUN 5.629E-04 6. 771E-02 6. 771E-02 FAIL ABUN N*P-238 l.000E+41 1.900E+41 O.OOOE+OO SHORT HLIF NP-239 -8.397E-02 2.567E-01 2.594E-01 NOT IDENT. AM-241 4.371E-02 7.074E-02 7.343E-02 NOT IDENT. CM-243 -4.231E-02 1.013E-01 1.031E-01 NOT IDENT. BK-247 9.072E-02 9.125E-02 1.000E-01 NOT IDENT. CM-247 -3.040E-02 4.257E-02 4.472E-02 NOT IDENT. CF-249 7.471E-03 4.250E-02 4.264E-02 NOT IDENT. CF-251 l.046E-02 l.315E-01 l.316E-01 NOT IDENT. Page 3073 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 84.9955 87.09 151.3662 136.47 76.0925 45.60 104.8623 87.57 151.4658 140.51 0.0000 46.54 105.0630 88.03 175.2441 143.76 71. 6081 49.72 0.0000 88.34 153.2064 144.24 66.5855 51. 35 101.5943 88.47 15.3. 2330 145.44 79.3240 51. 87 94.9898 89.96 87.8530 152.43 86.6695 52.39 89.4901 1093.63 123.5825 153.25 0.0000 52.97 89.5877 91.11 0.0000 323.87 69.7948 53.44 94.1498 92 .*59 123.9063 156.02 0.0000 54.07 99.8704 93.35 124.0308 158.56 0.0000 57.36 0.0000 94.56 101.9316 159.00 67.7201 57.53 123.0845 94.65 100.3505 162.33 73.7645 57.98 120.9224 94.67 100.3537 162.66 0.0000 59.27 110.2482 94.87 100.3800 163.33 55.8038 59.32 110.2578 97.43 127.8914 165.86 75.7271 59.54 117.8549 98.43 82.8361 176.31 70.3617 60.96 151.4684 98.44 82.8372' 176.60 0.0000 61.17 145.4619 99.53 81. 7502 177.52 76.5238 62.93 140.1993 100 .11 78. 2011 181.07 0.0000 63.29 140.2847 102.03 104.9228 181.52 70.6822 63.58 140.3530 103.18 91. 7883 184.41 62.9854 64.28 138. 6134 103.37 91. 8103 143.76 63.0557 66.73 131.5265 105.21 92.0191 193.51 61. 7072 67.24 134. 6972 105.31 92.0307 197.03 62.7707 125.81 130. 9636 106.12 88.4853 198.01 53.0884 67.75 134.4252 106.47 88.5232 201.83 57.6909 69.67 110.6375 109.28 85.1747 203.43 63.9866 70.83 121.6157 111. 00 87.7879 205.31 57.4073 72. 81 121.6057 111.76 0.0000 210.85 64.3638 72. 87 121.6169 114.06 67.3025 215.65' 69.9885 74.66 121. 9510 116.30 0.0000 222 .11 61.6786 74.82 121.9806 116.74 82.2421 227.09 69.6935 74.97 122.0079 119.76 77.5988 227.38 69.7084 77 .11 122;4012 121.12 76.4844 228.16 0.0000 78.74 143.3419 121. 22 76.4929 228.18 67.0328 79.69 127.9390 121.78 64.1958 116.74 67.0328 80.12 128.0191 122.06 64.2161 235.69 49.1869 80.19 0.0000 122.92 72.9303 235. 96 43.7300 80.57 106.2320 123.07 76.6514 238.63 81. 00 120.3673 265.00 82.8892 238.98 0.0000 '81.07 132.8860 125.81 74.4035 240.99 58.5189 81. 75 129.1043 127.23 84.4547 242.00 58.5612 83.79 116.1403 127.91 82.8603 244.70 38.5047 84.00 116.1745 129.30 82.1548 252.40 0.0000 85.43 125.8472 131.20 86.4805 252.80 54.3984 86.55 151.2529 133. 02 76.6508 254.15 0.0000 86.79 151.3027 133.52 81. 27 58 256.23 46.2097 86.94 151.3350 136.00 80.2344 260.90 0.0000 Page 3074 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.8277 355.39 0.0000 584.27 27.8035 264.80 41.8323 35t:i.Ol 39.7881 595.83 0.0000 265.00 41. 27 99 364.49 0.0000 427.87 18.6519 268.22 53.1082 366.42 0.0000 602.52 0.0000 269.46 43.8273 372.51 20.8154 604.72 26.3730 270.03 43.8435 375.05 17.8660 607.14 26.3965 271.23 46.2129 377.52 32.7966 609.32 26.4180 273.65 0.0000 356.01 28.9174 610.33 31. 3841 276.40 52.4590 388.16 28.9817 614.28 24.8135 277.37 52.4920 388.63 o*. o o o o 618.01 19.8779 277.60 53.4375 391.69 34.0408 620.36 19.8955 278.00 53.4514 264.66 19.1098 621. 93 23.2251 279.20 55.3701 401. 81 29.1847 630.19 0.0000 279.54 55 .. 3821 402.40 39.2603 631.29 14.4266 279.70 55.3881 404.85 25.3994 633.25 15.5478 280.46 53.5372 410.95 31.3406 634.78 0.0000 283.69 57. 4134 413.71 31.3835 635.95 22.2323 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42.4008 423. 72 0.0000 645.85 23.4276 285.90 0.0000 427.09 36.6841 657.76 15.1249 287.50 30.1921 427.87 32.6204 657.90 0.0000 290.67 56.7236 433.94 24.5366 661. 66 20.1943 293.27 0.0000 439.40 28.7007 664.57 0.0000 351. 93 45.5088 4*53. 88 15.4797 666.33 o. o*ooo 295. 96 45.5303 463.37 17.1022 666.50 0.0000 879.38 45.6045 468.07 17.1388 667. 71 0.0000 299.98 45.6436 473.00 0.0000 677.62 21. 4353 300.09 45.6465 475.06 28.7590 685.70 0.0000 300.13 45.6475 476.78 18.7701 695.00 0.0000 301.36 45.6826 477.60 18.7771 696. 49 15.8970 302.85 41. 4379 482.18 20.9062 696.51 15.8970 256.23 24.3156 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.6299 306.78 42.0145 497.08 22.0950 697.49 13.6304 308.46 27.7197 505.52 30.0957 702.65 21.6193 311. 90 39. 2716 507.63 0.0000 706.68 13. 6729 316.51 45.1430 511. 00 25.4028 711. 68 17.1198 319.41 0.0000 514.00 25.4355 720.70 0.0000 320.08 0.0000 514.00 25.4355 721. 93 0.0000 321. 04 49.1168 520.40 23.3786 722.78 18.3288 323.87 47.2694 520.69 0:0000 722.91 18.3294 325.23 52 .1334 522.65 0.0000 723.31 16.0405 328.76 0.0000 527.90 0.0000 724.19 19.4833 333.37 30.5554 528.26 25.5879 727.33 18.3561 333.97 33.4766 529.59 25.6025 733.00 14.9419 334.37 34.9402 529.87 0.0000 735.93 23.0103 338.28 27.2367 531.02 o. o*ooo 333.97 17.2662 338.32 27.2372 537.26 0.0000 739.50 0.0000 311. 90 37.9836 546.56 0.0000 747.24 18.4753 340.48 37.9836 552.55 16.1517 748.06 10.3953 340.55 0.0000 563.25 27.5762 752.31 17.3492 344.28 36.3084 569.33 28.1847 753.82 0.0000 345.93 37.5148 946.00 28.1857 756.73 13.8989 351.06 40.1692 569.70 28.1878 756.80 13.8994 351. 93 40.1884 583.19 27 .2471. 884.68 13.9307 Page 3075 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 26. 7163 1274.44 8.3752 1620.50 4.2529 766.42 27.8838 1001.03 14.9072 1621. 92 2.1270 766.84 20.9158 1002.74 15.8462 1678.03 0.0000 772.60 0.0000 1004.73 14.9219 1690.97 1. 07 64 776.52 0.0000 507.63 0.0000 1750.46 . 0. 0000 739.50 0.0000 1025.87 0.0000 1764.49 1. 7438 778.90 22 .1613 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 12.0383 1771.35 2.1824 785.37 24.5436 1038.76 0.0000 1791.20 0.0000 792.07 30.7425 631.29 12.2534 1808.65 3.2937 794.95 28.1328 1048.07 0.0000 1810.72 0.0000 795.86 21.9849 1049.04 17.9203 1836.06 3.3083 810.06 9 .. 7153 1050.41 15.0957 810.29 9. 7160 1063.66 13. 2523 344 .. 28 9.7166 1077.00 0.0000 810.76 9.7177 1077.34 15 .1963 815.77 0.0000 1085.87 14.2767 1048.07 0.0000 1093.63 14.3033 832.01 15 .1142 1099.45 8.5941 834.85 20.4661 1112. 07 14.3665 835.71 17.8009 1112.84 17.2430 836.80 0.0000 1115.54 16.8706 846.75 0.0000 1120.29 29.1735 846.77 19.6448 1120.55 19.9621 856.80 0.0000 1221.41 15.3584 860.56 16.1378 1129.67 15.3887 871.09 9.5924 1131. 51 0.0000 873.19 7.1987' 1147.95 0.0000 875.33 0.0000 1173.23 14.5743 879.38 12.3624 1177.95 12.4500 880.51 12.3662 1189.05 11. 7012 883.24 12.3758 1204.77 14.6786 884.68 15.8893 1221.41 8.8401 889.28 11. 3641 1231. 02 17.3239 894.76 14.4858 1235.36 0.0000 898.04 19.0300 1238.28 16.7603 900.72 13.6034 1260.41 0.0000 903.28 16.3356 1271.87 5.9590 911. 20 16.3718 1274.44 10.9308 912.08 16.3757 1274.54 10.9308 923.98 0.0000 *1291. 59 9.9731 926.50 12.7875 1298.22 0.0000 929 .11 8.2263 1312 .11 0.0000 937.49 14.6582 1332.49 7.0419 944 .13 0.0000 1362. 66 0.0000 946.00 18.3649 1365 .19 8.1021 949.00 12.8661 1368.63 0.0000 667. 71 0.0000 1384.29 8.1333 962. 31 14.7563 1408.01 5.1077 964.08 14.7637 1457.56 0.0000 966 .17 14.7720 1460.82 7.2252 911.20 14.7827 1489.16 2.0756 968. 97 14.7827 1505.03 4. 99.66 983.53 0.0000 1584.12 3.3801 984.45 0.0000 1596.21 0.0000 Page 3076 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:08:34.60 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 10-DEC-2015 10:30:00 Acquisition date*: 3-0CT-2016 08:06:24. Sample ID G405235009 Sample quantity 1.34381E+02 GRAM .Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.62 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl . Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 3 3 6 6 0 6 6 0 1 1 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3077 of 5809 Energy 46.38* 63.59* 74.85* 77.11* 84.01* 87.39 90.02 92.97* 186.07* 188.01 209.48 238.76* 241. 66 269.95 295.28* 297.40 300.15 304.40 328.57 338.73* 352.20* 359.52 365.92 463.66 481.50 511 .. 58* 583.51* 609.59* 628.56 661.82 728. 64 794.87 861.31 911". 58* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 76 35 252 432 51 137 55 144 118 27 41 481 147 31 218 28 57 28 42 69 269 12 22 56 13 53 138 214 16 477 54 14 30 98 207 307 186 147 199 180 171 168 138 51 94 61 116 95 43 31 32 28 46 94 76 45 53 80 28 51 59 41 20 23 23 21 19 18 1. 01 1. 04 0.99 0.85 1. 42 1. 52 1. 01 1.15 1. 32 0.74 0.60 1. 00 2.04 0.60 1. 36 1.18 1. 36 1. 37 1. 66 1. 29 1. 26 0.89 3.16 2.90 0.66 1. 89 1. 65 1. 36 1. 65 1. 45 2.05 1. 64 1. 07 1. 50 92. 26 126.67 149.20 153.72 167.51 174.27 179.53 185.42 371. 60 375.48 418.42 476.98 482.78 539.36 590.02 594.25 599.75 608.25 656.61 676.91 703.'86 718.50 731.31 926.81 962.48 1022.65 1166. 55 1218.72 1256.67 1323.20 1456.89 1589.39 1722.34 1822.92 88 121 145 145 164 171 177 177 367 367 415 471 471 535 . 583 583 583 583 653 672 698 714 725 917 958 1016 1162 1213 1250 1317 1449 1584 1715 1816 9 2.12E-02 10 9.62E-03 14 6.99E-02 14 1. 20E-01 7 1. 41E-02 7 3.80E-02 12 1.52E-02 12 4.0lE-02 11 3.27E-02 11 7.42E-03 7 l.15E-02 18 1.34E-01 18 4.09E-02 9 8.59E-03 34 6.07E-02 34 7.78E-03 34 1.60E-02 34 7.66E-03 9 1.18E-02 11 1. 91E-02 12 7.48E-02 6 3.43E-03 10 6. OlE-03 18 l.55E-02 7 3.67E-03 16 1.48E-02 14 3.82E-02 14 5.95E-02 10 4.44E-03 12 l.32E-01 17 l.49E-02 9 3.78E-03 15 8.32E-03 15 2.73E-02 36.9 99.1 10.8 9.42E-01 6.6 48.8 18.5 37.8 2.80E+OO 18.6 20.3 2.78E+OO 49.9 41. 9 5.3 2.lOE+OO 21. 4 59.5 8.5 3.16E+OO 48.8 22.6 45.6 32.5 30.5 9.0 90.3 69.4 40.0 71. 8 38.1 15.2 9.5 58.1 5.0 26.6 68.0 36.5 14.l Peak Search Report (continued) Page : 2 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 5 931. 00 10 3 2.15 1861. 77 1859 12 2.79E-03 34.6 3.lOE-01 36 5 934.05 14 3 1. 37 1867.88 1859 12 3.87E-03 33.3 37 0 968.97* 46 18 2.45 1937.76 1934 11 l.27E-02 23.8 38 0 1087.13 12 2 1. 60 2174.21 2168 10 3.33E-03 37.5 39 0 1120 ;99* 25 24 1. 41 2241.97 2235 12 6.92E-03 46.1 40 0 1198. 08 10 20 3.41 2396.26 2385 14 2.87E-03 98. 5 . 41 0 1277.97 15 34 7.78 2556.16 2542 23 4.07E-03107.3 42 0 1294.72 10 2 0.68 2589.68 2585 9 2. 72E-03 42.2 43 . 0 1377.63 11 7 5.07 2755.63 2745 14 2.95E-03 61. 4 44 0 1444.68 7 0 0.99 2889.86 2883 12 1. 94E-03 37.8 45 0 .1460.82* 355 7 1. 99 2922.17 2915 15 9.86E-02 5.6 46 0 1848.28 9 3 1. 79 3697.89 3692 10 2.63E-03 45.2 Flag: "*" = Peak area was modified by background subtraction Page 3078 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:08:37 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 10:30:00 G405235009 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:06:24 134.38 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA25 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3079 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:00.62 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* l.131E+OO 1.571E+Ol 1. 571E+Ol 11. 22 OK CD-109 88.03 3.70* 9.275E+OO l.166E+OO 1.824E+OO 85.38 OK SN-126 64.28 9.60 9.538E+OO 2.527E-01 2.527E-01 198.23 OK 86.94 8.90 9.275E+OO 4.846E-01 4.846E-01 85.38 OK 87.57 37.00* 9.275E+OO 1.166E-01 l.166E-01 85.38 OK BA-137M 661.66 89.90* 2.257E+OO 1.333E+OO 1.359E+OO 10.04 OK CS-137 661.66 85.10* 2.257E+OO 1.409E+OO l.435E+OO 10.04 OK TL-208 277.37 6.60 4.809E+OO .Line Not Found Absent 583.19 85.00* 2.509E+OO 3.698E-01 3.698E-01 30.35 OK 860.56 12.50 1. 809E+OO 7.369E-01 7.369E-01 72.92 OK PB-210 46.54 4.25* 9.109E+OO 1. 34 7E+OO 1.381E+OO 73.81 OK PB-212 74.82 10.28 9.404E+OO 8.358E-01 8.358E-01 47.84 OK 77 .11 17.10 9.383E+OO 1. 775E+OO 1. 775E+OO 13.12* OK 238.63 43.60* 5.476E+OO 1.232E+OO 1.232E+OO 10.64 OK 300.09 3.30 4.485E+OO 2.336E+OO 2.336E+OO 45.10 OK BI-214 609.32 45.49* 2.418E+OO 1. 112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 l.443E+OO 6.310E-01 6.312E-01 92.J,6 OK 1764.49 15.30 9.336E-01 Line Not Found Absent 'PB-214 74.82 5.80 9.405E+OO -----Line Not Found <<INT Reject 77 .11 9.70 9.383E+OO 3 .130E+OO 3 .131E+OO 13 .12 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.551E+OO l.570E+OO 1.570E+OO 17.08 OK 351. 93 35.60* 3.891E+OO 1.155E+OO 1.156E+00 18.02 OK RN-222 60'9. 32 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 l.443E+OO 6.310E-01 6.312E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent 240.99 4.10* 5.420E+OO 1. 27 5E+OO 1. 27 5E+OO 141.00 OK RA-226 609.32 45.49* 2.418E+OO 1.112E+OO l .112E+OO 18.92 OK 1120.29 14.92 1.443E+OO 6.310E-01 6.312E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 OK 794.95 4.25 l.935E+OO 9. 2 64E-01 9.264E-01 135. 94 OK 835.71 1. 61 l.856E+00 Line Not Found Absent 911.20 25.80* 1. 724E+OO 1.225E+OO 1.225E+OO 28.29 OK 968. 97 15.80 l.637E+00 9.749E-01 9.749E-01 47.53 OK RA-228 105.21 1.10 8.977E+00 Line Not Found Absent 338.32 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 OK 794.95 4.25 1. 935E+OO 9.264E-01 9.264E-01 135.94 OK 835.71 1. 61 1. 856E+OO Line Not Found Absent 911.20 25.80* 1. 724E+OO 1.225E+OO 1.225E+OO 28.29 OK 968. 97 15.80 l.637E+00 9.749E-01 9.749E-01 47.53 OK TH-228 74.82 10.28 9.404E+OO 8.358E-01 8.358E-01 47.84 OK 77 .11 17.10 9.383E+OO l.775E+00 1. 775E+OO 13 .12 OK. 238.63 43.60* 5.476E+OO 1.232E+OO 1.232E+OO 10.64 . OK 300.09 3.30 4.485E+OO 2.336E+OO 2.336E+OO 45.10 OK TH-229 85.43 14.70 9.314E+OO 2.437E-01 2.437E-01 97.55 OK 88.47 24.00 9.275E+OO 1. 797E-01 1.797E-01 85.38 OK Page 3080 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 193.51 4.41* 6.496E+OO Line Not Found Absent 210.85 2.80 6.103E+00 1.494E+OO 1. 494E+OO 83.76 OK TH-230 609.32 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 1.443E+00 . 6.310E-01 6.310E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent PA-231 283.69 1. 70 4.715E+OO Line Not Found Absent 301.36 5.35* 4.485E+OO 1.441E+OO 1.441E+OO 45.10 OK Tij-232 105.21 1. io 8.977E+OO Line Not Found Absent 338.32 11. 27 4.029E+OO 9. 021E-01 9. 021E-01 61. 06 OK 835,71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1. 724E+OO 1.225E+OO l.225E+OO 28.29 OK 968. 97 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 OK TH-234 63.29 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 OK 92.59 4.23 9.199E+00 2.418E+OO 2.418E+OO 37.13 OK U-234 609.32 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Foundc Absent U-235 89. 96 3.47 9.241E+OO 1.118E+OO 1.118E+00 75.64 OK 93.35 5. 60' 9.199E+OO 1.827E+OO 1.827E+OO 37.13 OK 143.76 10. 96* 7.922E+OO Line Not Found Absent 163.33 5.08 7.333E+OO Line Not Found Absent 185. 72 57.20 6.691E+OO 1.913E-01 1. 913E-01 40.58 OK 205 .. 31 5.01 6.202E+OO Line Not Found Absent U-238 63.29 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 OK 92.59 4.23 9.199E+OO 2.418E+OO 2.418E+OO 37 .13 OK AM-243 43.53 5.90 8.344E+OO Line Not Found Absent 74.66 67.20* 9.404E+OO 1. 27 9E-01 1.279E-01 47.84 OK ANH-511 511. 00 100. 00* . 2.807E+OO

1. 099E-01 1.099E-01 76.13 OK Flag: "*" Key line Page 3081of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:08:38.16 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l * *Acquisition date 3-0CT-2016 08:06:24 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
Sample date 10-DEC-2015 10:30:00 Analyst initials: MXRl *
Sample ID G405235009 Sample Quantity 1.3438E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.571E+Ol 1.727E+OO CD-109 1.824E+OO 1.526E+OO SN-126 l.166E-01 9.753E-02 BA-137M 1.359E+OO l.336E-01 CS-137 l.435E+OO 1.412E-01 TL-208 3.698E-01 1.lOOE-01 PB-210 1.381E+OO 9.991E-01 PB-212 1.232E+OO 1.284E-01 BI-214 1.112E+OO 2.062E-01 PB-214 1.156E+OO 2.041E-01 RN-222 l .112E+00 2.062E-01 RA-224 1.275E+OO 1. 761E+OO RA-226 l .112E+00 2.062E-01 AC-228 l.225E+OO 3. 396E-01 RA-228 1.225E+OO 3. 396E-01. TH-228 1.232E+OO l.284E-01 TH-229 -3. 296E-01 4.288E-01 TH-230 1.112E+OO 2.061E-01 PA-231 1.441E+OO 6.369E-01 TH-232 1.225E+00 3. 396E-01 TH-234 6.556E-01 1.274E+OO U-234 1.112E+00 2.061E-01 U-235 4.637E-02 1.639E-01 U-238 6.556E-01 1. 274E+OO AM-243 1. 279E-bl 5.995E-02 ANH-511 l.099E-01 8.199E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3082 of 5809 Key-Line Activity (pCi/GRAM 2. 661E+OO 3.162E-02 O.OOOE+OO 6.255E-03 K.L. Cnt Uncert ( 1. 96-sigma) 1.476E+Ol 5.806E-02 1. 960E+41 2.080E-02 MDA (pCi/GRAM 5.843E-01 l.295E+OO 8.267E-02 , 7. 723E-02 8.159E-02 7.677E-02 6.610E-01 8.755E-02 1.304E-01 1.252E-01 1.304E-01 9. 401E-01 1.304E-01 2. 891E-01 2.891E-01 8.755E-02 7.339E-01 l.303E-01 6.375E-01 2.891E-01 8.056E-01 l.303E-01 3.117E-01 8.056E-01 4.413E-02 5.541E-02 MDA (pCi/GRAM 2.592E+Ol 1.205E-01 O.OOOE+OO 5.709E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1.855E-01 4.335E-01 8.997E-01 FAIL ABUN V-48 O.OOOE+OO 1. 611E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4. 361E+02 O.OOOE+OO SHORT HLIF MN-54 1.633E-02 7.268E-02 l.465E-01 NOT IDENT. C0-56 -5.956E-02 4.434E-01 8.743E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.905E-02 3.876E-02 6.981E-02 NOT IDENT. C0-58 3.051E-02 4.858E-01 1.009E+OO NOT IDENT. FE-59 1. 751E+OO 6.862E+OO l.432E+Ol NOT IDENT. C0-60 1.350E-02 4.504E-02 9.302E-02 NOT IDENT. ZN-65 -1.109E-01 2.428E-01 3.679E-01 NOT IDENT. GE-68 8.788E-01 2.899E+OO 5.824E+OO NOT IDENT. AS-73 l.073E+OO 1.691E+00 3.508E+OO NOT IDENT. AS-74 O.OOOE+OO 6.245E+03 O.OOOE+OO SHORT HLIF SE-75 -3.233E-02 l.893E-01 3.366E-01 NOT IDENT. BR-77 O.OOOE+OO 1.317E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.213E+02 O.OOOE+OO SHORT HLIF RB-83 3. 231E-Ol 6.745E-01 1.366E+OO NOT IDENT. KR-85 4.405E+OO 7.677E+OO l.539E+Ol NOT IDENT. SR-85 4.537E-01 7.946E-01 l.592E+OO NOT IDENT. RB-8*6 0.000E+OO 2.881E+04 O.OOOE+OO SHORT HLIF Y-88 -l.335E-01 2.806E-01 5.170E-01 NOT IDENT. Y-91 1.692E+02 5.887E+02 l.181E+03 NOT IDENT. NB-94 7.792E-03 3.280E-02 6.358E-02 NOT IDENT. NB-95 1.508E-01 1. 069E+OO 1. 980E+OO NOT IDENT. NB-95M 7.155E-01 2.422E+OO 4.167E+OO NOT IDENT. ZR-95 -6.851E-03 1.372E+OO 2.599E+OO NOT IDENT. NB-97 O.OOOE+OO 1.852E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.355E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2 969E-02 2.744E-02 4.788E-02 NOT IDENT. RH-102 1.982E-02 5.620E-02 1.052E-01 NOT IDENT. RU-103 -7.399E-01 6.537E+OO 1. 202E+Ol FAIL ABUN RH-106 4.417E-01 5.306E-01 l.087E+OO NOT IDENT. RU-106 4.417E-01 5.306E-01 l.087E+OO NOT IDENT. AG-108M -1.515E-02 2.932E-02 5.325E-02 NOT IDENT. AG-llOM -4.508E-02 l.170E-01 2.178E-01 NOT IDENT. SN-113 1.091E-01 2.420E-01 4.872E-01 NOT IDENT. CD-115 O.OOOE+OO 1.862E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 7.590E+04 O.OOOE+OO SHORT HLIF TE-123M 2.173E-02 1. lllE-01 2 .113E-01 NOT IDENT. SB-124 5.418E-01 1.661E+OO 4.176E+OO NOT IDENT. SB-125 3.870E-02 l.256E-01 2.457E-01 FAIL ABUN TE-125M 2.269E+02 2.014E+02 4.163E+02 NOT IDENT. I-126 O.OOOE+OO 9.701E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.109E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.618E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.383E+09 O.OOOE+OO. SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.480E+26 O.OOOE+OO SHORT HLIF BA-133 -1. 782E-02 5.633E-02 7.376E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.054E-02 8.065E-02 1.199E-01 FAIL ABUN CS-135 3.691E-02 1. 595E-01 2. 701E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.272E+05 O.OOOE+OO SHORT HLIF CE-139 -4.642E-02 9. 727E-02 1.740E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 451E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.369E+05 O.OOOE+OO SHORT HLIF CE-141 -5.909E+OO 2.174E+Ol 3.970E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.509E+40 O.OOOE+OO SHORT HLIF CE-144 -4.959E-02 2.739E-01. 5.136E-01 NOT IDENT. PM-144 -4.640E-03 5.639E-02 1. 046E-01 NOT IDENT. PR-144 -4.345E-01 4.889E+OO 9. 061E+OO NOT IDENT. PM-"146 -6.640E-02 4.803E-02 7.713E-02 NOT IDENT. ND-147 O.OOOE+OO 3.458E+07 O.OOOE+OO SHORT HLIF PM-147 2.122E+02 6.514E+02 l.274E+03 NOT IDENT. PM-'-14 9 O.OOOE+OO 2.676E+40 O.OOOE+OO SHORT HLIF EU-150 2.936E-03 2.949E-02 5.224E-02 FAIL ABUN EU-152 -l.635E-02 l.027E-01 1. 880E-01 FAIL ABUN GD-153 -l.370E-02 1.225E-01 2.330E-01 NOT IDENT. EU-154 7.697E-02 1.424E-01 2.954E-01 NOT IDENT. EU-155 6.138E-02 7.207E-02 1. 484E-01 FAIL ABUN TB-160 -9.744E-01 1. 701E+OO 3.108E+OO FAIL ABUN H0-166M -2*. 2 64E-02 6.623E-02 l.166E-01 NOT IDENT. TM-171 l.070E+OO 3.740E+OO 7.617E+OO NOT IDENT. HF-172 -6.646E-02 l.776E-01 3.291E-01 FAIL ABUN Page 3083 of 5809 LU-172 1.140E-01 9.308E-02 2. 091E-01 FAIL ABUN LU-176 l.849E-02 2.267E-02 4.486E-02 FAIL ABUN HF-181 4.208E+OO 5.925E+OO 9.140E+OO FAIL ABUN TA-182 7.320E-02 9.871E-01 1. 925E+OO FAIL ABUN RE-183 8.592E-02 7.612E-01 1.540E+OO NOT IDENT. RE-184 -2.544E+OO 3. 071E+Ol 6.019E+Ol NOT IDENT. W-188 -8.215E+OO l.243E+02 2.019E+02 FAIL ABUN IR-192 4.411E-01 7.933E-01 FAIL ABUN HG-203 -1. 42.2E+OO 2.615E+OO 4.400E+OO NOT IDENT. BI-207 -6.303E-03 4. 881E-02 9.438E-02 FAIL ABUN BI-211 O.OOOE+OO 5.623E-01 8.326E-01 FAIL ABUN PB-211 1. 501E-01 7.320E-01 1.433E+OO NOT IDENT. BI-212 O.OOOE+OO 1.134E+OO 1.475E+OO FAIL ABUN RN-219 * -3.899E-01 4.248E-01 7.423E-01 FAIL ABUN RA-223 -5.684E-01 6.527E-01 1.117E+OO FAIL ABUN AC-227 -1. 566E-01 2.106E-01 3.488E-01 FAIL ABUN TH-227 -1. 566E-01 2.106E-01 3.488E-01 FAIL ABUN TH-231 -5.684E-01 6.527E-01 1.117E+OO FAIL ABUN PA-233 1.157E-02 '6 .159E-02 l.222E-01 FAIL ABUN PA-234 5 .117E-02 2.771E-01 5.682E-01 NOT I DENT .. PA-234M -l.149E+00 4.204E+OO 8.188E+OO NOT IDENT. NP-237 1.157E-02 6.159E-02 1.222E-01 FAIL ABUN NP-238 0. OOOE+oo* l.960E+41 O.OOOE+OO SHORT HLIF NP-239 -3.652E-02 1.884E-01 3.558E-01 NOT IDENT. pu:....239 2. 896E+Ol 2.737E+02 5.202E+02 NOT IDENT. AM-241 1.940E-02 4.328E-02 8.364E-02 NOT IDENT. CM-243 -1. 32 6E-02 6.780E-02 1.296E-01 NOT IDENT. BK-247 -1.995E-02 6.859E-02 l.199E-01 FAIL ABUN CM-247 -2.568E-02 3.748E-02 6. 723E-02 NOT IDENT. CF-249 -3.489E-04 4.091E-02 7. 876E-02* NOT IDENT. CF-251 -8.440E-03 1.038E-01 1.910E-01 NOT IDENT. Page 3084 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:08:35.47 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 339 10.66* 1.131E+OO 1.571E+Ol 1.571E+Ol 11. 22 CD-109 88.03 160 3.70* 9.275E+OO 2.612E+OO 4.087E+OO 36.90 SN-126 64.28 41 9.60 9.538E+OO 2.527E-01 2.527E-01 198.23 86.94 160 8.90 9.275E+OO l.086E+OO 1.086E+OO 36.90 87.57 160 37.00* 9.275E+OO 2.612E-01 2. 612E*-Ol 36.90 BA-137M 661. 66 484 89.90* 2.257E+OO 1.333E+OO 1.359E+OO 10.04 CS-137 661. 66 484 85.10* 2 *. 257E+OO 1.409E+OO l.435E+OO 10.04 TL-208 277.37 ------6.60 4.809E+OO ------Line Not Found ------583.19 141 85.00* 2.509E+OO 3.698E-01 3.698E-01 30.35 860.56 30 12.50 1.809E+OO 7.369E-01 7.369E-01 72. 92 PB-210 46.54 93 4.25* 9.109E+OO 1. 34 7E+OO 1.381E+OO 73.81 BI-211 72. 87 ------1. 23 9.424E+OO ------Line Not Found ------351.06 286 12.92* 3. 891E+OO 3.183E+OO 3.183E+OO 18.02 PB-212 74.82 2 98 10.28 9.404E+OO 1.722E+OO 1. 722E+OO 21. 50 77 .11 510 17.10 9. 383E+OO 1. 775E+OO 1. 775E+OO 13.12 238.63 527 43. 60*' 5.476E+OO 1.232E+OO 1. 232E+.00 10 .*64' 300.09 62 3.30 *4. 485E+OO 2.336E+OO 2.336E+OO 45.10 BI-214 609.32 219 45.49* 2.418E+00 1.112E+OO 1.112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.312E-01 92.16 1764.49 ------15.30 9. 336E-01 ------Line Not Found ------PB-214 74.82 298 5.80 9.404E+OO 3. 051E+OO 3.052E+OO 21. 50 77 .11 510 9.70 9.383E+OO 3.130E+OO 3 .131E+OO 13.12 87.09 160 3.41 9.275E+OO 2.835E+OO 2.836E+OO 36.90 242.00 161 7.25 5.420E+OO 2. 291E+OO 2.291E+OO 42.80 295.22 236 18.42 4.551E+OO 1.570E+OO 1.570E+OO 17.08 351. 93 286 35.60* 3.891E+OO 1.155E+OO 1.156E+OO 18.02 RN-222 609.32 219 45.49* 2.418E+OO 1.112E+OO l .112E+00 18.92 1120.29 24 14.92 l.443E+OO 6.310E-01 6.312E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------RA-224 240.99 161 4.10* 5.420E+OO 4.050E+OO 4.050E+OO 42.80 RA-226 609.32 219 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 1120.29 24 14.92 l.443E+OO 6.310E-01 6.312E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------AC-228 105.21 ------1.10 8.977E+00 ------Line Not Found ------338.32 73 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 794.95 14 4.25 l.935E+OO 9.264E-01 9.264E-01 135. 94 835.71 ------1. 61. 1.856E+OO ------Line Not Found ------911. 20 98 25.80* 1. 724E+OO 1.225E+OO 1.225E+OO 28.29 968.97 45 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 73 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 794.95 14 4.25 l.935E+OO 9.264E-01 9.264E-01 135.94 835. 71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 98 25.80* 1. 724E+OO 1.225E+OO 1.225E+OO 28.29 968.97 45 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 TH-228 74.82 298 10.28 9.404E+OO 1. 722E+OO 1. 722E+OO 21. 50 77 .11 510 17.10 9.383E+OO 1. 775E+OO 1. 775E+OO 13.12 Page 3085 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 527 43.60* 5.476E+OO l.232E+OO 1.232E+OO 10.64 300.09 62 3.30 4.485E+OO 2.336E+OO 2.336E+OO 45.10 TH-229 85.43 60 14.70 9.314E+OO 2.437E-01 2.437E-01 97.55 88.47 160 24.00 9.275E+OO 4.027E-01 4.028E-01 36.90 193.51 ------4.41* 6.496E+OO ------Line Not Found ------210.85 46 2.80 6.103E+OO l.494E+OO 1.494E+OO 83.76 TH-230 609.32 219 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 4.715E+OO ------Line Not Found ------301.36 62 5.35* 4.485E+00 1.441E+OO l.441E+OO 45.10 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 73 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 835.71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 98 25.80* l.724E+OO 1.225E+OO 1.225E+OO 28.29 968.97 45 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 TH-234 63.29 41 3.70* 9.538E+OO 6.556E-01 6.556E-01 198;23 92.59 168 4.23 9.199E+OO. 2.418E+OO 2.418E+OO 37.13 U-234 609.32 219 45.49* '2. 418E+OO . l.112E+OO 1.112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------U-235 89. 96 64 3.47 9.241E+00 1.118E+OO 1.118E+OO 75.64 ' 93. 35 168 5.60 9.199E+OO 1.827E+OO 1.827E+OO 37.13 143.76 ------10. 96* 7.922E+OO ------Line Not Found ------163.33 ------5.08 7.333E+OO ------Line Not Found ------185.72 131 57.20 6. 691E+OO l.913E-01 1.913E-01 40.58 205.31 ------5.01 6.202E+OO ------Line Not Found ------U-238 63. 29 41. 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 92.59 168 4.23 9.199E+OO 2.418E+OO 2.418E+00 37.13 AM-243 43.53 ------5.90 8.344E+OO ------Line Not Found ------74.66 298 67.20* 9.404E+OO 2.634E-01 2.634E-01 21. 50 ANH-511 511. 00 55 100.00* 2.807E+OO l.099E-01 l.099E-01 76.13 Flag: "*" Key line Page 3086 of 5809 Summary of Nuclide Activity Sample ID : G405235009 . Acquisition date Page : 3 3-0CT-2016 08:06:24 Total number of lines in spectrum 46 Number of unidentified lines 11 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600.00Y 1600. OOY 1.41E+10Y 1600. OOY 1.41E+10Y 1.41E+10Y 1.41E+10Y 7340.00Y 7.54E+04Y . 7. 04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.571E+Ol 2.612E+OO 2.612E-01 1.333E+OO 1.409E+OO 3.698E-01 l.347E+OO 3.183E+OO 1. 232E+OO 1.112E+OO 1.155E+00 1.112E+OO 4.050E+OO 1.112E+OO l.225E+OO. 1.225E+OO 1.232E+OO 4.027E-01 l .112E+OO 1. 441E+OO 1.225E+OO 6.556E-01 1.112E+OO 1. 913E-01 6.556E-01 2.634E-01 1.099E-01 4.685E+Ol 4.685E+Ol Decay Corr pCi/GRAM 1.571E+Ol 4.087E+OO 2.612E-01 l.359E+OO 1.435E+OO 3.698E-01 1.381E+OO 3.183E+OO 1.232E+OO 1.112E+OO l.156E+OO 1.112E+OO 4.050E+OO l .112E+OO 1.225E+OO 1.225E+OO l.232E+00 4.028E-01 1.112E+OO 1.441E+OO 1.225E+OO 6.556E-01 l.112E+OO l.913E-01 6.556E-01 2.634E-01 l.099E-01 4. 841E+Ol 4. 841E+Ol 76.09% Decay Corr 2-Sigma Error 0.176E+Ol 1.508E+OO 0.964E-01 0.136E+00 0.144E+OO 1.122E-01 1.019E+OO 0.574E+OO 0 .131E+OO 0.210E+OO 0.208E+00 0.210E+OO 1.733E+OO 0.210E+00 0:347E+OO 0.347E+OO 0 .131E+OO l.486E-01 0.210E+OO 0.650E+OO 0.347E+OO 13.00E-01 0.210E+OO 0.776E-01 13.00E-01 0.566E-01 0.837E-01 Manually accepted 2-Sigma %Error 11. 22 *36.90 36.90 10.04 10.04 30.35 73.81 18.02 10.64 18.92 18. 02 18.92 42.80 18.92 28.29 28.29 10.64 36.90 18.92 45.10 28.29 198.23 18.92 40.58 198.23 21. 50 76 .13 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 3087 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235009 Acquisition date : 3-0CT-2016 08:06:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 188.01 30 56 0.74 375.48 367 11 7.42E-03 99.8 6.64E+OO 0 269.95 34 103 0.60 539.36 535 9 8.59E-03 **** 4.92E+OO T 1 297.40 30 34 1.18 594.25 583 34 7.78E-03 97.6 4.52E+OO T 1 304.40 30 30 1. 37 608.25 583 34 7.66E-03 91. 2 4.43E+OO T 0 3.28. 57 45 49 1. 66 656.61 653 9 l.18E-02 65.0 4.14E+OO T 0 359.52 13 47 0.89 718. 50 714 6 3.43E-03 **** 3.82E+00 0 365.92 23 57 3.16 731.31 725 10 6.0lE-03 **** 3.76E+OO T 0 463.66 58 84 2.90 926.81 917 18 l.55E-02 80.1 3.06E+OO T 0 481. 50 14 29 0.66 962.48 958 7 3.67E-03 **** 2. 96E+OO T 0 628. 56 16 20 1. 65 1256.67 1250 10 4.44E-03 **** 2.36E+OO 0 728. 64 54 24 2.05 1456.89 1449 17 l.49E-02 53.2 2.08E+OO T 5 931. 00 10 2 2.15 18 61. 77 1859 12 2.79E-03 69.3 1. 69E+00 5 934.05 14 3 1. 37 1867.88 1859 12 3.87E-03 66.6 1. 69E+OO 0 1087.13 12 2 1. 60 2174.21 2168 10 3.33E-03 75.0 1. 48E+OO T 0 1198. 08 10 19 3.41 2396.26 2385 14 2.87E-03 **** 1. 36E+OO 0 1277.97 14 33 7.78 2556.16 2542 23 4.07E-03 **** L28E+OO 0 1294.72 9 2 0.68 2589.68 2585 9 2.72E-03 84.4 l.27E+OO 0 1377.63 10 7 5.07 2755.63 2745 14 2.95E-03 **** l.20E+OO 0 1444.68 7 0 0.99 2889.86 2883 12 l.94E-03 75.6 l.14E+OO 0 1848.28 9 2 1. 79 3697.89 3692 10 2.63E-03 90.3 8.88E-01 Flags: "T" = Tentatively associated Page 3088 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:08:53.03 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA. GAMMA.ARCHIVE. GAMMA] G405235009. CNF ;*1 *
Acquisition date 08:06:24 Sensitivity : 3.000
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
Sample date 10-DEC-2015 10:30:00 Nuclide Library : SOLID *
Sample ID .. G405235009 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : l.3438E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN * *' Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate ot Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.294E-01 6 .115E-01 3.904E-02 3.477E-02 3.673E-02 3.479E-02 3.094E-01 4.052E-02 5.822E-02 5.700E-02 5.822E-02 4.351E-01 5.822E-02 1.274E-01 1.274E-01 4.052E-02 3.397E-01 5.820E-02 2.863E-01 1.274E-01 3.803E-01 5.820E-02 1.468E-01 3.803E-01 2.081E-02 2.497E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3089 of 5809 Le (pCi/GRAM 1.176E+Ol '5. 2 94E-02 O.OOOE+OO 2.023E-02 3.990E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97' ZR-'97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3090 of 5809 O.OOOE+OO 0.000E+OO 6.531E-02 3.768E-01 O.OOOE+OO 3.261E-02 4.299E-01 6.209E+OO 3. 967E-02 l.598E-01 2.574E+OO 1.649E+OO O.OOOE+OO l.535E-01 O.OOOE+OO O.OOOE+OO 6.153E-01 7.026E+OO 7.271E-01 O.OOOE+OO 1. 996E-01 5 .'l 72E+02 2.822E-02 8.934E-01 1. 941E+OO 1.124E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 231E-02 4.582E-02 5.446E+OO 4.870E-01 4.870E-01 2.399E-02 9.534E-02 2.234E-01 O.OOOE+OO O.OOOE+OO 9.859E-02 l.586E+OO l.132E-01 1. 962E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.347E-02 O.OOOE+OO 5.386E-02 1.252E-01 O.OOOE+OO O.OOOE+OO 8. 096E-02 O.OOOE+OO O.OOOE+OO 1.867E+Ol O.OOOE+OO 2.390E-01 4.603E-02 3.985E+OO 3.434E-02* O.OOOE+OO 5. 971E+02 O.OOOE+OO 2.412E-02 8.634E-02 1.095E-01 1.297E-01 6.949E-02 l.306E+00 5.164E-02 3. 572E+00 l.534E-01 9.348E-02 SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-1°81 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3091of5809 2.0SSE-02 4.148E+00 8.349E-01 7.237E-01 2.616E+Ol 9.289E+Ol 3.607E-01 2.033E+OO 4.033E-02 4. OllE-01 6. 572E-01 6.826E-01 3.373E-01 5.120E-01 1.585E-01 1.585E-"-01 5.120E-01 5.648E-02 2.461E-01 3.525E+OO 5.648E-02 O.OOOE+OO 1.665E-01 2.452E+02 3. 951E-02 6.052E-02 5.478E-02 3.051E-02 3.610E-02 8.898E-02 FAIL ABUN F]1.IL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:09:00.45 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l *
Acquisitiori date 3-0CT-2016 08:06:24 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
Sample date 10-DEC-2015 10:30:00 Nuclide Library : SOLID *
Sample ID G405235009 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity l.3438E+02 GRAM *
Quantity Err(%) l.4883E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.571E+Ol l.912E+OO CD-109 l.824E+00 l.559E+00 SN-126 l.166E-01 9.943E-02 BA-137M l.359E+OO l.458E-01 CS-137 l.435E+OO l.540E-01 TL-208 3.698E-01 l. lllE-01 PB-210 1. 381E+OO l.006E+00 PB-212 1. 232E+OO l.440E-01 BI-214 l .112E+OO 2 .117E-01 PB-214 l.156E+OO 2.097E-01 RN-222 l .112E+00 2. ll 7E-01 RA-224 l.275E+OO 1. 772E+OO RA-226 l .112E+00 2. ll 7E-01 AC-228 1.225E+OO 3.453E-01 RA-228 1.225E+OO 3.453E-01 TH-228 1.232E+00 l.440E-01 TH-229 -3. 296E-01 4.291E-01 TH-230 1.112E+OO 2 .116E-01 PA-231 1. 441E+OO 7. 072E-01 TH-232 l.225E+00 3.453E-01 TH-234 6.556E-01 l.282E+OO U-234 1.112E.f-OO 2 .116E-01 U-235 4.637E-02 l.639E-01 U-238 6.556E-01 1.282E+OO AM-243 1. 27 9E-01 6.285E-02 ANH-511 l.099E-01 8. 211E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3092 of 5809 Key-Line Activity (pCi/GRAM 2.661E+OO 3.162E-02 -l.OOOE+41 6.255E-03 K.L Act error ( 1. 96-sigma) l.476E+Ol 5.807E-02 5.479E+41 2.081E-02 TPU ( 1. 96-sigma) l.912E+OO l.559E+OO 9.943E-02 l.458E-01 l.540E-01 l. lllE-01 l.006E+OO l.440E-01 2. ll 7E-01 2.097E-01 2.117E-01 1. 772E+OO 2.117E-01 3.453E-01 3.453E-01 l.440E-01 4.291E-01 2 .116E-01 7.072E-01 3.453E-01 l.282E+OO 2 .116E-01 l.639E-01 l.282E+OO 6.285E-02 8.211E-02 TPU (1.96-sigma) l.481E+Ol *5.980E-02 O.OOOE+OO 2.lOOE-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1.85SE-01 4.335E-01 4.415E-01 FAIL ABUN V-48 -9.990E+02 1. 611E+04 l.612E+04 SHORT HLIF CR-51 3.589E+02 4.363E+02 4.654E+02 SHORT HLIF MN-54 1. 633E-02 7.269E-02 7.306E-02 NOT IDENT. C0-56 -5.956E-02 4.434E-01 4.442E-01 NOT IDENT. MN-56 -l.OOOE+41 8 .191E+41 O.OOOE+OO SHORT HLIF C0-57 -2.905E-02 3.878E-02 4.093E-02 NOT IDENT. C0-58 3.051E-02 4.858E-01 4.860E-01 NOT IDENT. FE-59 1. 751E+OO 6.864E+OO 6.909E+OO NOT IDENT. C0-60 1.350E-02 . 4. 504E-02 4.545E-02 NOT IDENT. ZN-65 -1.109E-01 2.429E-01 2.480E-01 NOT IDENT. GE-68 8.788E-01 2.899E+OO 2.926E+OO NOT IDENT. AS-73 1.073E+OO 1. 706E+OO 1. 773E+OO NOT IDENT. AS-74 4.227E+03 6.254E+03 6.538E+03 SHORT HLIF SE-75 -3.233E-02 1. 893E-01 . l.899E-01 NOT IDENT. BR-77 1. 263E+38 1. 086E+39 O.OOOE+OO SHORT HLIF SR-82 -3.719E+02 8.215E+02 8.384E+02 SHORT HLIF RB-83 3. 231E-01 6.759E-01 6.915E-01 NOT IDENT. KR-85 4.405E+OO 7.679E+OO 7.932E+OO NOT IDENT. SR-85 4.537E-01 7.948E-01 8.207E-01 NOT IDENT. RB-86 2.143E+04 2.883E+o4 3.040E+04 SHORT HLIF Y-88 -1.335E-01 2.808E-01 2. 871E-:-Ol NOT IDENT. Y-91 1.692E+02 5.887E+o2 5.936E+02 NOT IDENT. NB-94 7.792E-03 3.280E-02 3.298E-02 NOT IDENT. NB-95 l.508E-01 1. 069E+OO 1. 071E+OO NOT IDENT. NB-95M 7.155E-01 2.423E+OO 2.444E+OO NOT IDENT. ZR-95 -6. 851E-03

1.372E+OO 1. 372E+OO NOT IDENT. NB-97 -1.000E+41 1.852E+41 0.000E+OO SHORT HLIF ZR-97 -l.OOOE+41 l.019E+43 O.OOOE+OO SHORT HLIF *M0-99 -4.374E+31 1.356E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.210E+42 O.OOOE+OO SHORT HLIF RH-101 -2. 969E-02 2.796E-02 3.lOOE-02 NOT IDENT. RH-102 1.982E-02 5.623E-02 5.693E-02 NOT IDENT. RU-103 -7.399E-01 6.537E+OO 6.546E+OO FAIL ABUN RH-106 4.417E-01 5.313E-01 5.674E-01 NOT IDENT. RU-106 4.417E-01 5.313E-01 5.674E-01 NOT IDENT. AG-108M -1.515E-02 2.932E-02 3. 011E-02 NOT IDENT. AG-110M -4.508E-02 l.171E-01 l.188E-01 NOT IDENT. SN-113 1.091E-01 2.420E-01 2.470E-01 NOT IDENT. CD-115 3.038E+38 1.862E+39 O.OOOE+OO SHORT HLIF SN-117M 2.652E+04 7.597E+04 7.690E+04 SHORT HLIF TE-123M 2.173E-02 1.111E-01 l .115E-01 NOT IDENT. SB-124 5.418E-01 1.662E+OO 1. 679E+OO NOT IDENT. SB-125 3.870E-02 1.256E-01 l.268E-01 FAIL ABUN TE-125M 2.269E+02 2. 018E+02 2.263E+02 NOT IDENT. I-126 8.903E+05 9.775E+05 1. 057E+06 SHORT HLIF SB-126 4.828E+05 1.112E+06 l.134E+06 SHORT HLIF SB-127 8.216E+21 1. 969E+22 0.000E+OO SHORT HLIF I-131 6.167E+09 8. 388E+o9 8.837E+09 SHORT HLIF I-132 -1. 000E+41 l.858E+42 O.OOOE+OO SHORT HLIF TE-132 2.070E+26 2.617E+26 O.OOOE+OO SHORT HLIF BA-133 -1. 782E-02 5.634E-02 5. 691E-02 NOT IDENT. I-133 -1.000E+41 9.416E+41 O.OOOE+OO SHORT HLIF CS-134 6.054E-02 8.069E-02 8.518E-02 FAIL ABUN CS-135 3.691E-02 l.595E-01 1.604E-01 NOT IDENT. I-135 -l.OOOE+41 1. 271E+43 O.OOOE+OO SHORT'HLIF CS-136 3.652E+03 3.272E+05 3. 272E+05 SHORT HLIF CE-139 -4.642E-02 9.772E-02 9.994E-02 NOT IDENT. BA-140 8. 721E+05 1.452E+06 l.504E+06 SHORT HLIF LA-140 -l.823E+05 4.370E+05 4.446E+05 SHORT HLIF CE-141 -5.909E+OO 2.174E+Ol 2.190E+Ol NOT IDENT. CE-143 1.000E+41 "5. 601E+40 O.OOOE+OO SHORT HLIF CE-144 -4.959E-02 2.739E-01 2.748E-01 NOT IDENT. PM-144 -4.640E-03 5.639E-02 5.643E-02 NOT IDENT. PR-144 -4.345E-01 4.889E+OO 4.893E+00 NOT IDENT. PM-146 . -6.640E-02 4.827E-02 5. 68.0E-02 NOT IDENT. ND-147 -l.046E+07 3.458E+07 3.490E+07 SHORT HLIF PM-147 2.122E+02 6.515E+02 6.585E+02 NOT IDENT. PM-149 1.439E+40 2.694E+40 0.000E+OO SHORT HLIF EU-150 2.936E-03 2.949E-02 2.952E-02 FAIL ABUN EU-152 -1.635E-02 1.028E-01 l.030E-01 FAIL ABUN GD-153 -l.370E-02 l.225E-01 l.227E-01 NOT IDENT. EU-154 7.697E-02 1.424E-01 1.466E-01 NOT IDENT. EU-155 6.138E-02 7.220E-02 7.732E-02 FAIL ABUN TB-160 -9.744E-01 1.702E+OO 1. 758E+OO FAIL .ABUN H0-166M -2.264E-02 6.624E-02 6.702E-02 NOT IDENT. TM-171 l.070E+OO 3.741E+OO 3. 772E+OO NOT IDENT. HF-172 -6.646E-02 1.779E-01 l.804E-01 FAIL ABUN Page 3093 of 5809 LU-172 1.140E-01 9.379E-02 1.069E-01 FAIL ABUN LU-176 1.849E-02 2.268E-02 2.416E-02 FAIL ABUN HF-181 4.208E+00 5.928E+OO 6.224E+OO FAIL ABUN TA-182 7.320E-02 9.871E-01 9.877E-01 FAIL ABUN RE-183 8.592E-02 7.614E-01 7.623E-01 NOT IDENT. RE-184 -2.544E+OO 3.071E+Ol 3.073E+Ol NOT IDENT. W-188 -8.215E+OO l.243E+02 l.244E+02 FAIL ABUN IR-192 -4.103E-01 4.415E-01 4.787E-01 FAIL ABUN HG-203 -l.422E+OO 2.616E+OO 2.693E+OO NOT IDENT. BI-207 -6.303E-03 4.881E-02 4.889E-02 FAIL ABUN BI-211 3.183E+OO 5.799E-01 1.548E+OO FAIL ABUN PB-211 l.501E-01 7.320E-01 7.352E-01 NOT IDENT. BI-212 2.176E+OO 1.140E+OO 1.504E+OO FAI-L ABUN RN-219 -3.899E-01 4.276E-01 4.623E-01 FAIL ABUN RA-223 -5.684E-01 6.536E-01 7.021E-01 FAIL ABUN AC-227 -l.566E-01 2 .116E-01 2.231E-01 FAIL ABUN TH-227 -l.566E-01 2 .116E-01 2.231E-01 FAIL ABUN TH-231 -5.684E-01 6.536E-01 7.021E-01 FAIL ABUN PA-233 l.157E-02 6.159E-02 6.181E-02 FAIL ABUN PA-234 5. ll 7E-02 2.832E-01 2.842E-01 NOT IDENT. PA-234M -1.149E+OO 4.204E+OO 4.236E+OO NOT IDENT. NP-237 l.157E-02 6.159E-02 6.181E-02 FAIL ABUN NP-238 -1.000E+41 2.176E+41 O.OOOE+OO SHORT HLIF NP-239 -3.652E-02 l.884E-01 l.892E-01 NOT IDENT. PU-239 2.896E+Ol 2.737E+02 2.740E+02 NOT IDENT. AM-241 1.940E-02 4.331E-02 4.418E-02 NOT IDENT. CM-243 -1.326E-02 6.781E-02 6.808E-02 NOT IDENT. BK-247 '....l. 995E-02 6.871E-02 6.930E-02 . FAIL ABUN CM-247 -2.568E-02 3.773E-02 3.947E-02 NOT IDENT. CF-249 -3.489E-04 4.091E-02 4. 091E-02 NOT IDENT. CF-251 -8.440E-03 1.038E-01 l.039E-01 NOT IDENT. . Page 3094 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 73.4783 87.09 95.5220 136.47 69.6050 45.60 71.3332 87.57 95.6613 140.51 0.0000 46.54 71.6618 88.03 95.7946 143.76 70.6794 49.72 0.0000 88.34 68.4888 144.24 72. 7150 51.35 79.2780 88.47 68.5156 145.44 79.7888 51. 87 76.4654 89. 96 100.9381 152.43 78.9144 52.39 66.8749 1093.63 101.1413 153.25 0.0000 52.97 68.5541 91.11 0.0000 323.87 69.1664 53.44 64.9216 92.59 101. 7205 156.02 0.0000 54.07 71.1566 93.35 101.9443 158.56 0.0000 57.36 0.0000 94.56 66.2623 159.00 60.7004 57.53 80.6626 94.65 69.7675 162.33 64 .1372 57.98 74.6553 94.67 69.7717 162. 66 -0.0000 59.27 99.0366 94.87 69.8114 163.33 56.0969 59.32 80.4835 97.43 79.1071 165.86 70.7056 59.54 80.5557 98.43 79.3275 176.31 61. 6009 60. 96 99. 7124 98.44 79.3295 176.60 0.0000 61.17 99.7959 99.53 71. 6116 177.52 63.8231 62.93 94.9933 100 .11 80.5803 181.07 0.0000 63.29 95 .1262 102.03 63.1992 181.52 71. 6389 63.58 95.2328 103.18 71. 4301 184.41 88.9302 64.28 95.4895 103.37 71. 4667 143.76 74.2714 66.73 88.1461 105.21 54.7595 193.51 68.7832 67.24 91.5053 105.3*1 54.7740 197.03 60. 5271 125.81 89.5226 106.12 72.8871 198.01 62.7861 67.75 87.9466 106.47 74.7552 201.83 72.9674 69.67 115.9398 109.28 62.5981 -203. 43 76.4258 70.83 87.3166 111. 00 91.1186 205.31 81. 0290 72.81 115.0662 111. 76 0.0000 210.85 63.3120 72.87 114.0042 114. 06 91.8175 215.65 55.6122 74.66 91. 7690 116.30 o.ooob 222 .11 48.2818 74.82 91.8186 116.74 75.7864 227.09 66.7216 74.97 91.8656 119.76 64.2358 227.38 64.4868 77 .11 92.5321 121.12 67.2446 228.16 0.0000 78.74 76.4198 121.22 67.2605 228.18 45.3052 79.69 102.2104 121.78 83.2508 116.74 45.3052 80.12 102.3536 122.06 85.1778 235.69 54.9397 80.19 0.0000 122.92 64. 7154 235.96 54. 9602 80.57 90.2466 123.07 62.8616 238.63 51.7140 -81.00 92.0454 265.00 65.7692 238.98 0.0000 81. 07 92.0664 1-25. 81 71. 7579 240.99 51. 8802 81. 75 86.1159 127.23 88.0922 242.00 51.9509 83.79 102.4324 127.91 87.2800 244.70 49.4362 84.00 102.5000 129.30 87.5527 252.40 0.0000 85.43 101.8259 131.20 80.2791 252.80 38.6467 86.55 95.3647 133.02 89.2366 254.15 0.0000 86.79 95.4340 133.52 64.3593 256.23 47.0526 86.94 95.4784 136.00 62.7744 260.90 0.0000 Page 3095 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 39.2358 355.39 0.0000 584.27 31. 4380 264.80 35.6754 356.01 39.4482 595.83 0.0000 265.00 42.8214 364.49 0.0000 427.87 24.3523 268.22 49.3621 366.42 0.0000 602.52 0.0000 269.46 52.6273 372. 51 29.3900 604. 72 19.1067 270.03 52.6649 375.05 38.3870 607.14 35.0813 271.23 62.3324 377.52 38.4753 *609. 32 23.4198 273.65 0.0000 356.01 38.7010 610.33 23.4341 276.40 50.6633 388.16 40.6604 614.28 14.4146 277.37 42.2685 388.63 0.0000 618.01 23.5442 277.60 42.2803 391.69 33.5388 24.6490 278.().Q 45.9263 264.66 43.8584 621.93 14.1598 279.20 58.0957 401.81 49.3912 630.19 0.0000 279.54 61. 7 516 402.40 43.9258 631.29 11. 3271 279.70 61. 7 640 404.85 37.6009 633.25 18.3606 280.46 55.7593 410.95 40. 56.70 634.78 0.0000 283.69 55.9741 413. 71 35.1186 635.95 12.9810 284.31 0.0000 414.70 *o.oooo 636.99 0.0000 285.41 47.5527 423. 72 0.0000 645.85 19.5850 285.90 0.0000 427.09 48.6051 657.76 23.0081 287.50 63.5591 427.87 40.2189 657.90 0.0000 290.67 45.8008 433.94 35. 7216 661.66 27.4516 293.27 0.0000 439.40 31.1604 664.57 0.0000 351.93 25.8982 453.88 43.9448 666.33 0.0000 295. 96 25.9200 463.37 35. 6119 666.50 0.0000 879.38 25.9975 468.07 30.4291 667.71 0.0000 299.98 26.0385 473.00 0.0000 677.62 19.9446 300.09 26.0417 475.06 27.1939 685.70 0.0000 300 .13 26.0430 476.78 32.0916 695.00 0.0000 301.36 26.0789 477.60 29.1925 696.49 19.0337 302.85 26.1225 '482.18 33.6879 696. 51 19.0344 256.23 26.1705 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.6822 306.78 26.2372 497.08 31.5951 697.49 15.6833 308.46 37.5513 505.52 28.3127 702.65 17.9746 311.90 46.0694 507.63 0.0000 706.68 21. 3912 316.51 49.6672 511. 00 27.9259 711. 68 24.8359 319.41 0.0000 514 .*oo 27.9852 720.70 0.0000 320.08 0.0000 514.00 27.9863 721. 93 0.0000 321. 04 42.2963 520.40 21. 0846 722.78 23.8472 323.87 54.9809 520.69 0.0000 722.91 23.8489 325.23 42.0597 522.65 0.0000 723.31 18.7424 .328.76 0.0000 527.90 0.0000 724 .19 25.5698 333.37 50.1306 528.26 28.2689 727.33 13.6597 333.97 46.3030 529.59 27.2834 733.00 13.7007 334.37 43.7482 529.87 0.0000 735.93 13. 7212 338.28 44.7859 531. 02 0.0000 333.97 19.4543 338.32 44.7869 537.26 0.0000 739.50 0.0000 311. 90 42.7274 546.56 0.0000 747.24 23.0029 340.48 42.7274 552.55 22.5819 748.06 20.7114 340.55 0.0000 563.25 22.7430 752.31 19.6037 344.28 45.7521 569.33 29.0618 753.82 0.0000 345.93 45.1329 946.00 21. 7981 756.73 13.8691 351. 06 34.8950 569.70 23.8778 756.80 13.8696 34.9251 583.19 31.4172 884.68 24.3599 Page 3096 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.7042 1274.44 10.6156 1620.50 2.8216 766.42 25.5512 1001.03 12.5695 1621.92 3.7635 766.84 29.0415 1002.74 9.6753 1678.03 0.0000 772.60 0.0000 1004.73 14.5244 1690.97 1.9146 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.9488 778.90 22.7889 1028.54 0.0000 1063.66 16.5883 783.70 0.0000 1037.84 11.7700 1771.35 6.8322 785.37 14.0688 1038.76 0.0000 1791.20 0.0000 792.07 12.7037 631. 29 14.7620 1808.65 0.9846 794.95 16.*9617 1048.07 0.0000 1810.72 0.0000 795.86 14 .1411 1049.04 13.7906 1836.06 6.9354 810.06 14.2383 1050.41 14.7830 810.29 12.4598 1063.66 12.8762 344.28 12.4611 1077.00 0.0000 810.76 10.6824 1077.34 15.9287 815.77 0.0000 1085.87 4.9936 1048.07 0.0000 1093. 63" 10.0153 832.01 18.8826 1099.45 9.0330 834.85 19.8079 1112. 07 10.0830 835.71 19.8160 1112. 84 16.1367 836.80 0.0000 1115. 54 20.9980 846.75 0.0000 1120.29 17.1909 846.77 14.4854 1120.55 17.1930 856.80 0.0000 1221. 41 17.8041 860.56 15.4882 1129. 67 16.2344 871.09 13.7311 1131. 51 0.0000 873.19 11. 9114 1147. 95 0.0000 875.33 0.0000 1173.23 11. 3323 879.38 14.7007 1177.95 16.5098 880.51 10 .1118 1189.05 17.9533 883.24 15.6465 1204.77 13. 5364 884.68 21.1821 1221.41 13. 6118 889.28 15.6880 1231.02 24.1595 894.76 13.8757 1235.36 0.0000 898.04 10.1903 1238.28 20.0054 900.72 15.7668 1260.41 0.0000 903.28 15.7845 1271.87 8;5151 911.20 18.6334 1274.44 11. 7177 912.08 18.6407 1274.54 11. 7184 923.98 0.0000 1291.59 10.2820 926.50 15.0049 1298.22 0.0000 929.11 10.5150 1312 .11 0.0000 937.49 9.0448 1332.49 8.6777 944.13 0.0000 1362.66 0.0000 946.00 12.2918 1365.19 6.5731 949.00 16.0937 1368.63 0.0000 667.71 0.0000 1384.29 8.8140 962. 31 23.7976 1408.01 4.4377 964.08 15.2417 1457.56 0.0000 966.17 9.1529 1460.82 4.5054 911.20 18.1355 1489.16 1. 8164 968". 97 18.1355 1505.03 7.2977 983.53 0.0000 1584.12 15.8387 984.45 0.0000 1596.21 0.0000 Page 3097 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:09:40.98 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date 10-DEC-2015 10:35:00 Acquisition date : 3-0CT-2016 08:06:48. Sample ID G405235010 Sample quantity : 1.41695E+02 GRAM Detector name GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.44 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 1 2 1 3 0 4 7 5 7 6 0 7 0 8 3 9 3 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 1 18 1 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30. 0 31 0 32 0 33 0 34 7 Page 3098 of 5809 Energy 74.87* 77.34 88.10 90.12 92.81* 186.51* 209.46 238.84* 241. 88 270.52 281. 98 295.46 328.59 338.71 352.30* 381.75 415.85 418.05 498.95 511. 08* 537.63* 583. 55*" 609.92* 662.07* 690.92 728.43 777 .17 862.69 880.77 889.35 911. 66* 925.88 957.60 965. 52* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 115 233 29 71 86 91 55 415 91 68 26 172 25 102 263 10 24 23 10 *39 33 167 157 109 10 39 22 35 17 7 98 12 8 23 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 142 145 281 89 163 164 98 101 87 98 149 108 46 61 80 34 11 25 12 53 67 20 47 35 32 58 18 26 9 15 12 15 29 16 1. 22 1.23 1.27 1.17 1. 45 1. 65 2.05 1. 41 1. 80 1. 57 3.65 1. 52 1.14 1. 70 1. 49 0.78 1. 67 1. 67 1. 39 1. 24 7.89 1. 75 1. 67 1. 71 0.91 1. 37 1. 40 1. 64 0.82 0. 72 2.04 5.21 4.25 2.53 149.82 154.78 176.31 180.35 185.73 373.28 419.22 478.01 484 .11 541.41 564.35 591.33 657.65 677.90 705.10 764.04 832.30 836.70 998.62 1022.90 1076.05 1167. 95 1220. 72 1325.10 1382.84 1457.91 1555.47 1726.64 1762.82 1780.00 1824.66 1853 .11 1916.61 1932.45 145 145 169 178 178 368 415 473 473 534 552 584 654 672 698 759 829 829 994 1016 1063 1160 1215 1318 1371 1450 1549 1718 1756 1771 1819 1843 1903 1928 15 3.21E-02 20.5 2.90E+OO 15 6.47E-02 11.1 10 7.99E-03111.2 12 l.98E-02 22.9 l.05E+OO 12 2.39E-02 31.4 12 2. 51E-02 31. 2 9 1. 53E-02 35. 2 16 l.15E-01 6.5 2.08E+OO 16 2.52E-02 23.8 14 l.88E-02 33.4 17 7.25E-03110.1 14 4.77E-02 15.0 7 6.97E-03 48.9 11 2.82E-02 17.9 14 7.32E-02 9.6 7 2.68E-03106.2 13 6.54E-03 31.0 l.76E+OO 13 6.48E-03 46.0 7 2.86E-03 64.0 14 l.08E-02 50.2 23 9.llE-03 68.2 16 4*. 65E-02 9. 9 12 4.36E-02 12.0 13 3.04E-02 15.1 13 2. 82E-03119. 5 16 1.09E-02 45.6 14 6.12E-03 45.6 18 9.81E-03 38.3 12 4.72E-03 42.8 10 l.94E-03110.2 12 2.73E-02 12.5 16 3.23E-03 82.0 15 2.29E-03148.6 18 6.35E-03 39.3 2.09E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 7 969.75 30 25 2.06 1940.92 1928 18 8.40E-03 36.3 36 0 1120.99* 47 6 2.03 2243.64 2237 11 l.30E-02 18.1 37 0 1227.79 6 16 3.42 2457.39 2446 13 1.67E-03143.6 38 0 1331.39 15 0 1. 06 2664.73 2659 12 4.17E-03 25.8 39 0 1362.03 9 7 2.99 2726.06 2721 11 2.57E-03 60.3 40 0 1461.82* 402 15 2.22 2925.80 2918 15 l.12E-01 5.4 Flag: "*" = Peak area was modified by_background subtraction Page 3099 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:09:43 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 10:35:00 G405235010 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:06:48 141.70 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA28 0 01:00:00.00 . 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3100of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies*at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line. 240.99 86.94 87.57 88.03 74: 6'6 74.82 74.82 351. 06 CAN 0 01:00:00.44 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %.Error Status K-40 1460.82 10.66* l.237E+OO l.548E+Ol l.548E+Ol 10.88 OK SC-46 889.28 99.98* 1. 841E-i-OO 2. 023E-02 . 2.379E-01 220.39 OK 1120.55 99.99 l.539E+00 l.584E-01 l.862E+OO 36. 29 OK BA-137M 661. 66 89.90* 2.305E+OO 2.882E-01 2.937E-01 30.20 OK CS-137 661.66 85.10* 2.305E+OO 3.045E-01 3.103E-01 30.20 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2*. 540E+OO 4.280E-01 4.280E-01 19.83 OK 860.56 12.50 l.888E+OO Line Not Found Absent PB-212 74.82 10.28 4.348E+OO 9.762E-01 9.762E-01 73.52 OK 77 .11 17.10 4.595E+OO l.922E+OO l.922E+OO 22.12 OK 238.63 43.60* 5.102E+OO l. llOE+OO l.llOE+OO 13. 00 OK 300.09 3.30 4.295E+OO Line Not Found Absent BI-214 609.32 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 OK 1120.29 14.92 l.539E+OO l.061E+OO l.062E+OO 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.595E+OO 3.388E+OO 3.389E+00 22.12 OK 87.09 3.41 5.480E+OO 9.889E-01 9.893E-01 222.31 OK 242.00 7.25 5.054E+OO Line Not Found <<INT Rej'ect 295.22 18.42 4.348E+OO l.253E+OO l.253E+OO 29.93 OK 351. 93 35.60* 3.782E+00 l.127E+OO 1.128E+OO 19.25 OK RN-222 609.32 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 OK 1120.29 14.92 l.539E+OO 1.061E+OO 1.062E+OO 36.29 OK 1764.49 15.30 l.045E+OO Line Not Found Absent RA-224 240.99 4.10* 5.056E+OO 3.884E-01 3.884E-01 361.47 OK RA-22 6 609.32 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 OK 1120. 29 14.92 1.539E+OO 1.061E+OO 1.062E+00 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.903E+OO l.334E+OO 1.334E+OO 35.71 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 l.930E+OO Line Not Found Absent 911. 20 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 OK 968. 97 15.80 1. 723E+OO 5.862E-01 5.862E-01 72.56 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.903E+OO 1.334E+OO 1.334E+OO 35. 71 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 OK 968. 97 15.80 1.723E+OO 5.862E-01 5.862E-01 72 .56 OK TH-228 74.82 10.28 4.348E+OO 9.762E-01 9.762E-01 73.52 OK 77 .11 17.10 4.595E+OO l.922E+00 l.922E+OO 22.12 OK 238.63 43.60* 5.102E+00 1. llOE+OO l. llOE+OO 13.00 OK 300.09 3.30 4.295E+OO Line Not Found Absent TH-230 609.32 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 OK 1120.29 14.92 l.539E+OO l.061E+OO l.061E+OO 36.29 OK 1764.49 15.30 l.045E+OO Line Not Found Absent TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11.27 3.903E+OO 1.334E+OO 1.334E+OO 35.71 OK Page 3101of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.118E+OO l .118E+OO 25.05 OK 968. 97 15.80 l.723E+OO 5.862E-01 5.862E-01 72 .56 OK U-234 609.32 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 OK 1120.29 14.92 l.539E+OO 1.061E+OO 1.061E+OO 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent U-235 89. 96 3.47 5.613E+OO 2.346E+OO 2.346E+OO 45.73 OK 93.35 5.60 5.774E+OO 1.699E+OO 1.699E+OO 62.79 OK 143.76 10. 96* 6.593E+OO Line Not Found Absent 163.33 5.08 6.352E+OO Line Not Found Absent 185.72 57.20 5. 972E+OO l.607E-01 l.607E-01 62.42 OK 205.31 5.01 5.647E+00 Line Not Found Absent AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.348E+OO l.493E-01 l.493E-01 73.52 OK ANH-511 511. 00 100.00* 2.815E+OO 7.735E-02 7.735E-02 100.37 OK Flag: "*" = Keyline Page 3102of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:09:45.53 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * ' '
DETECTOR AND SAMPLE DATA ' * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l * *Acquisition date 3-0CT-2016 08:06:48 Sensitivity .. 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.44 Half life ratio : ***** *
Sample date 10-DEC-2015 10:35:00 Analyst initials: MXRl *
Sample ID G405235010 Sample Quantity 1.4170E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
_Combined Ac ti vi ty-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 l.548E+Ol 1. 651E+OO 7.790E-01 SC-46 2.379E-01 5 .138E-01 5.677E-01 BA-137M 2.937E-01 8.693E-02 6.608E-02 CS-137 3.103E-01 9.183E-02 6.981E-02 TL-208 4.280E-01 8.316E-02 5. 872E-02 PB-212 l. llOE+OO 1. 414E-01 9.957E-02 BI-214 7.738E-01 l.823E-01 1.343E-01 PB-214 1.128E+OO 2.127E-01 1.199E-01 RN-222 7.738E-01 1.823E-01 l.343E-01 RA-224 3.884E-01 1. 376E+OO 1.067E+OO RA-226 7.738E-01 1.823E-01 l.343E-01 AC-228 1.118E+OO 2.745E-01 1.944E-01 RA-228 1.118E+OO 2.745E-01 1.944E-01 TH-228 1. llOE+OO 1.414E-01 9.957E-02 TH-230 7.735E-01 1.822E-01 1.343E-01 TH-232 l .118E+00 2.745E-01 1.944E-01 U-234 7. 735E-Ol* l.822E-01 l.343E-01 U-235 5.665E-02 2.136E-01 3.889E-01 AM-243 l.493E-01 1.076E-01 1.007E-01 ANH-511 7.735E-02 7.608E-02 5.153E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma) (pCi/GRAM BE-7 1.688E+OO l.184E+Ol 2.292E+Ol NOT IDENT. NA-22 2.246E-02 4.683E-02 9.887E-02 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 -2.222E-02 2.865E-02 4.9i1E-02 NOT IDENT. V-48 O.OOOE+OO l.431E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.367E+02 O.OOOE+OO SHORT HLIF MN-54 5.688E-03 6.780E-02 l.345E-01 NOT IDENT. C0-56 8.791E-02 4.665E-01 9.481E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1. 294E-02 5.206E-02 9.583E-02 NOT IDENT. Page 3103 of 5809 C0-58 -2.229E-01 6.006E-01 l.133E+OO NOT IDENT. FE-59 -4 .196E+OO 7.282E+OO l.292E+Ol NOT IDENT. C0-60 6. 396E:-02 3.237E-02 8.164E-02 FAIL ABUN ZN-65 5.230E-02 2.045E-01 3.667E-01 NOT IDENT. GE-68 -4.752E-01 2.518E+OO 4.891E+OO NOT IDENT. AS-73 2.390E+OO 9.590E+OO l.832E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.002E+03 O.OOOE+OO SHORT HLIF SE-75 -8.366E-02 2.154E-01 3.575E-01 NOT IDENT. BR-77 O.OOOE+OO l.448E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l .191E+03 O.OOOE+OO SHORT HLIF RB-83 -3.177E-02 6.447E-01 l.215E+OO NOT IDENT. KR-85 8.201E+OO 8.453E+OO l.599E+Ol NOT IDENT. SR-85 8.474E-01 8.751E-01 l.655E+OO NOT IDENT. RB-86 O.OOOE+OO 2.899E+04 O.OOOE+OO SHORT HLIF Y-88 4.586E-02 2.072E-01 4.784E-01 NOT IDENT. Y-91 -3.295E+Ol 5.892E+02 l .118E+03 NOT IDENT. NB-94 2.235E-02 3.464E-02 6.927E-02 NOT IDENT. NB-95 -2.932E-01 8.910E-01 l.686E+OO NOT IDENT. NB-95M 2.382E+OO 2.519E+OO 4.765E+OO NOT IDENT. ZR-95 1. 093E+OO l.411E+OO 3. 071E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 511E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.353E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.083E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.385E-02 3.724E-02 6.332E-02 NOT IDENT. RH-102 -4.469E-02 6.196E-02 l.034E-01 NOT IDENT. RU-103 3.193E+OO 4.627E+OO 9.254E+OO FAIL ABUN. RH-106 -4.160E-01 5.095E-01 8.365E-01" NOT IDENT. RU-106 -4.160E-01 5.095E-01 8.365E-01 NOT IDENT. AG-108M 6.887E-03 2.765E-02 5.420E-02 NOT IDENT. CD-109 l.426E+OO 3.106E+OO 2.659E+00 FAIL ABUN AG-llOM 7.324E-03 l.277E-01 l.711E-01 NOT IDENT. SN-113 -1. 7 97E-01 2.263E-01 3.929E-01 NOT "IDENT. CD-115 O.OOOE+OO l.853E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.019E+o5 O.OOOE+OO SHORT HLIF TE-123M 3.932E-02 l.466E-01 2.659E-01 NOT IDENT. SB-124 2.091E-01 1. 723E+OO 3.804E+OO NOT IDENT. SB-125 7.877E-02 1. 031E-01 2.129E-01 NOT IDENT. TE-125M 4 .114E+Ol 2.824E+02 5.199E+02 NOT IDENT. I-126 O.OOOE+OO 8.109E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.774E+05 0.000E+OO SHOR'!'. HLIF SN-126 9 .114E-02 1.986E-01 l.810E-01 FAIL ABUN SB-127 O.OOOE+OO 1.793E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.261E+09 O.OOOE+OO SHORT HLIF I-132 ,0. OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.678E+26 O.OOOE+OO SHORT HLIF BA-133 -2.253E-02 4.414E-02 7.019E-02 NOT* I DENT. I-133 O.OOOE+OO O.OOOE+OO SHORT HLIF CS-134 3.080E-02 5.427E-02 l .132E-01 NOT IDENT. CS-135 6.612E-02 l.343E-01 2.702E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.768E+05 O.OOOE+OO SHORT HLIF CE-139 -1.225E-01 1.030E-01 1.856E-01 NOT IDENT. BA-140 O.OOOE+OO 3.992E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4. 611E+05 O.OOOE+OO SHORT HLIF CE-141 -2.890E+Ol 2.759E+Ol 4.480E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.293E-01 4.016E-01 6.848E-01 NOT IDENT. PM-144 1. 911E-02 5.353E-02 1.055E-01 NOT IDENT. PR-144 1.643E+OO 4.643E+OO 9 .151E+OO NOT IDENT. PM-146 7.738E-04 4.315E-02 8. 231E-02 NOT' IDENT. ND-147 O.OOOE+OO 3.238E+07 O.OOOE+OO SHORT HLIF PM-147 l .114E+02 8.989E+02 1.640E+03 NOT IDENT. PM-149 O.OOOE+OO 2.644E+40 O.OOOE+OO SHORT HLIF EU-150 l.735E-02 2.584E-02 4. 8 61E-02 FAIL ABUN EU-152 -l.553E-02 8.440E-02 1.597E-Ol FAIL ABUN GD-153 -l.236E-01 l.838E-01 3.185E-01 NOT IDENT. EU-154 4.809E-02' l.135E-01 2.383E-01 NOT IDENT. EU-155' 9.599E-02 1.155E-01 2.241E-01 NOT !DENT. TB-160 2.821E+OO 2.367E+OO 3.319E+OO FAIL ABUN H0-166M -l.197E-02 6.195E-02 l .114E-01 NOT IDENT. TM-171 -l.198E+OO 2.291E+Ol 4.280E+Ol NOT IDENT. HF-172 -l.589E-01 2.482E-01 4.226E-01 NOT IDENT. LU-172 -4.140E-02 7.390E-02 l.322E-01 FAIL ABUN LU-176 -2.567E-03 2.640E-02 4.999E-02 FAIL ABUN HF-181 6.322E-01 4.423E+OO 8.501E+OO NOT IDENT. TA-182 -3.562E-01 l.OOOE+OO l.565E+OO FAIL ABUN RE-183 -6.587E-01 3.101E+OO 5.754E+OO NOT IDENT. Page 3104 of 5809 RE-184 1.787E+Ol 3.187E+Ol 6.685E+Ol NOT IDENT. W-188 4.322E+Ol 1.161E+02 2 .112E+02 NOT IDENT. IR-192 -2.023E-01 4.750E-01 8.734E-Ol FAIL ABUN HG-203 2.180E+OO 2.401E+OO 4.943E+OO NOT IDENT. BI-207 3.199E-02 4.675E-02 l.016E-01 FAIL ABUN PB-210 3.202E-01 3. 896E+OO 7.399E+OO NOT IDENT. BI-211 O.OOOE+OO 5.860E-01 8.039E-01 FAIL ABUN PB-211 3.286E-01 6.805E-01 l.358E+OO NOT IDENT. BI-212 l.489E+OO l.330E+,00 l.516E+OO FAIL ABUN RN-219 5.262E-02 3.531E-01 6.889E-01 FAIL ABUN RA-223 5.300E-01 6.662E-01 l.304E+OO FAIL ABUN AC-227 -8.847E-02 2.256E-01 4.217E-01 NOT IDENT. TH-227 -8.847E-02 2.256E-01 4.217E-01 NOT IDENT. TH-229 -2.527E-01 4.570E-01 8.562E-01 FAIL ABUN PA-231 l.510E-02 5.457E-01 9.892E-01 NOT IDENT. TH-231 5.300E-01 6.662E-01 1.304E+OO FAIL ABUN PA-233 -2.707E-02 5.936E-02 1. 091E:..._01 NOT IDENT. PA-234 2.153E-02 3.000E-01 5.934E-01 FAIL ABUN PA-234M -1.253E+OO 4.256E+OO 8.510E+OO NOT IDENT. TH-234 -2. 636E-01 l.457E+OO 2.692E+OO FAIL ABUN NP-237 -2.707E-02 5.936E-02 1. 091E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -2.636E-01 l.457E+OO 2.692E+OO FAIL ABUN NP-239 -1. 749E-0.l 2.651E-01 4. 527E-0*1 NOT IDENT. PU-239 2.404E+02 3.353E+02 6.365E+02 NOT IDENT. AM-241 -9.236E-02 1. 471E-01 2.629E-01 NOT IDENT. CM-243 -l.132E-01 1. 092E-01 1. 817E-01 NOT IDENT. BK-247 8. 431E-03 7. 088E'-02 l.261E-01 NOT IDENT. CM-247 -2. 331E-02 3.432E-02 6.035E-02 NOT IDENT. CF-249 l.601E-02 3.725E-02 7.428E-02 NOT IDENT. CF-251 5.780E-02 1.161E-01 2.343E-01 NOT IDENT. Page 3105 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:09:42.03 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 385 10.66* 1.237E+OO 1. 548E+Ol 1.548E+Ol 10.88 SC-46 889.28 7 99.98* 1.841E+OO 2.023E-02 2.379E-01 220.39 1120.55 46 99.99 1.539E+OO 1. 584E-01 1. 862E+OO 36.29 CD-109 88.03 35 3.70* 5.480E+OO 9.114E-01 1.426E+OO 222.31 SN-126 64.28 ------9.60 3.124E+OO ------Line Not Found ------86.94 35 8.90 5.480E+00 3.789E-01 3.789E-01 222.31 87.57 35 37.00* 5.480E+OO 9 .114E-02 9 .114E-02 222.31 BA-137M 661.66 113 89.90* 2.305E+OO 2.882E-01 2.937E-01 30.20 CS-137 661.66 113 85.10* 2.305E+OO 3.045E-01 3.103E-01 30.20 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 174 85.00* 2.540E+OO 4.280E-01 4.280E-01 19.83 860.56 ------12.50 1.888E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 4.138E+OO ------Line Not Found ------351.06 287 12.92* 3.782E+OO 3.107E+OO 3.107E+OO 19.25 PB-212 74.82 142 10.28 4.348E+OO 1.679E+OO 1.679E+00 40.90 77 .11 285 17.10 4 .'595E+00 1.922E+OO 1.922E+OO 22.12 . 238.63 466 43.60* 5.102E+OO 1. llOE+OO l. llOE+OO 13.00 300.09 ------3.30 4.295E+OO ------Line Not Found ------BI-214 609.32 163 45.49* 2.455E+00 7.735E-01 7.738E-01 24.04 1120.29 46 14.92 1.539E+OO 1.061E+00 1.062E+OO 36.29 1764.49 ------15.30 1.045E+OO ------Line Not Found ------PB-214 74.82 142 5.80 4.348E+OO 2.976E+OO 2.977E+OO 40.90 77 .11 285 9.70 4.595E+OO 3.388E+OO 3.389E+00 22.12 87.09 35 3.41 5.480E+OO 9.889E-01 9.893E-01 222.31 242.00 102 7.25 5.056E+OO 1.472E+OO 1.473E+OO 47.53 295.22 189 18.42 4.348E+00 1.253E+OO 1.253E+OO 29.93 351. 93 287 35.60* 3.782E+OO 1.127E+OO 1.128E+OO 19.25 RN-222 609.32 163 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 1120.29 46 14.92 1.539E+OO 1. 061E+OO 1.062E+OO 36.29 1764.49 ------15.30 l.045E+OO ------Line Not Found ------RA-224 240.99 102 4.10* 5.056E+OO 2.604E+OO 2.604E+OO 47.53 RA-226 609.32 163 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 1120.29 46 14.92 1.539E+OO 1.061E+OO 1.062E+OO 36.29 1764.49 ------15.30 1.045E+OO ------Line Not Found ------AC-228 105.21 .------1.10 6.315E+OO ------Line Not Found ------338.32 111 11. 27 3.903E+OO l.334E+00 l.334E+OO 35.71 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 98 25.80* l.806E+OO 1.118E+OO 1.118E+OO 25.05 968. 97 30 15.80 l.723E+OO 5.862E-01. 5.862E-01 72. 56 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 111 11. 27 3.903E+OO 1.334E+OO 1.334E+OO 35.71 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 98 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 968. 97 30 15.80 1.723E+OO 5.862E-01 5.862E-01 72. 56 TH-228 74.82 142 10.28 4.348E+OO 1.679E+OO 1. 679E+OO 40.90 Page 3106 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM ,pCi/GRAM %Error 77 .11 285 17.10 4.595E+OO 1.922E+OO 1.922E+OO 22.12 238.63 *466 43.60* 5.102E+OO 1. llOE+OO '1.llOE+OO 13.00 300.09 ------3.30 4.295E+OO ------Line :Not Found ------TH-230 609.32 163 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 1120.29 46 14.92 1.539E+OO 1.061E+OO l.061E+OO 36.29 1764.49 ------15.30 1.045E+OO ------Line Not Found ------TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 111 11. 27 3.903E+OO 1.334E+OO 1.334E+OO 35.71 835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 98 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 968.97 30 15.80 1. 723E+OO 5.862E-01 5.862E-01 72. 56 U-234 609.32 163 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 1120.29 46 14.92 1.539E+OO 1.061E+OO 1.061E+OO 36.29 1764.49 ------15.30 1.045E+00 ------Line Not Found ------U-235 89.96 86 3.47 5. 613E+OO 2.346E+OO 2.346E+OO 45.73 93.35 104 5.60 5.774E+OO 1.699E+OO 1.699E+OO 62.79 143.76 ------10. 96* 6.593E+OO ------Line Not Found ------163.33 ------5.08 6.352E+OO ------Line Not Found ------185. 72 104 57.20 5. 972E+OO 1.607E-01 1.607E-01 62.42 205.31 ------5.01 5.647E+OO ------Line Not Found ------AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 142 67.20* 4.348E+OO 2.568E-01 2.568E-01 40.90 ANH-511 511. 00 41 100.00* 2.815E+OO 7.735E-02 7.735E-02 100.37 Flag: "*" Key line Page 3107 of 5809.

Summary of Nuclide Activity Sample ID : G405235010 Acquisition date Page : 3 3-0CT-2016 08:06:48 Total number of lines in spectrum 40 Number of unidentified lines 8 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife l.25E+09Y 83.79D 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+10Y l.41E+10Y 1. 41E+l0Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1. OOE+09Y Decay 1. 00 11. 8 1. 56 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 LOO 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM . l.548E+Ol 2.023E-02 9. 114E-01 9. 114E-02 2.882E-01 3.045E-01 4.280E:-01 3.107E+OO 1.llOE+OO 7.735E-01 1.127E+OO 7.735E-01 2.604E+OO 7.735E-01 1.118E+OO 1.118E+OO 1. llOE+OO 7.735E-01 1.118E+OO 7.735E-01 1.607E-01 2.568E-01 7.735E-02 3.430E+Ol 3.430E+Ol Decay Corr pCi/GRAM 1.548E+Ol 2.379E-01 1.426E+OO 9 .114E-02 2.937E-01 3.103E-01 4.280E-01 3.107E+OO 1.llOE+OO 7.738E-01 1.128E+OO 7.738E-01 2.604E+OO 7.738E-01 1.118E+OO 1.118E+OO l. llOE+OO 7.735E-01 1.118E+OO 7.735E-01 1.607E-01 2.568E-01 7.735E-02 3.504E+Ol 3.504E+Ol 80.00% Decay Corr 2-Sigma Error 0.169E+Ol 5.243E-01 3.170E+OO 20.26E-02 0.887E-01 0.937E-01 0.849E-01 0.598E+OO 0.144E+OO l.860E-01 0.217E+OO 1. 860E-01 1.237E+OO l.860E-01 0.280E+OO 0.280E+OO 0.144E+OO 1.860E-01 0.280E+OO 1.860E-01 1.003E-01 1. 051E-01 7.764E-02 "M" Manually accepted 2-Sigma %Error 10.88 220.39 222.31 222.31 30.20 30.20 19.83 19.25 13.00 24.04 19.25 24.04 47.53 24.04 25.05 '25. 05 13.00 24.04 25.05 24.04 62.42 40.90 100.37 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3108of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235010 Acquisition date : 3-0CT-2016 08:06:48 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.46 62 111 2.05 419.22 415 9 1.S3E-02 70.4 5.58E+OO T 0 270.52 75 109 1. 57 541. 41 534 14 1.88E-02 66.7 4.65E+OO T 0 281. 98 29 165 3.65 564.35 552 17 7.25E-03 **** 4.51E+OO 0 328.59 27 50 1.14 657.65 654 7 6.97E-03 97. 8 . 4.00E+OO T 0 381. 75 10 37 0.78 764.04 759 7 2.68E-03 **** 3.55E+OO 1 415.85 25 12 1. 67 832.30 829 13 6.54E-03 62.0 3.31E+OO T 1 418.05 25 27 1. 67 836.70 829 13 6.48E-03 92.0 3.30E+OO 0 498.95 11 12 1. 39 998.62 994 7 2.86E-03 **** 2.87E+OO 0 537.63 34 70 7.89 1076.05 1063 23 9. llE-03 **** 2.71E+OO T 0 *690.92 10 33 0.91 1382.84 1371 13 2.82E-03 **** 2.23E+OO 0 728.43 40 59 .1. 37 1457.91 1450 16 1.09E-02 91. 2 2.14E+OO T 0 777.17 22 18 1. 40 1555.47 1549 14 6.12E-03 91. 3 2.04E+OO T 0 862.69 36 26 1. 64 1726.64 1718 18 9.81E-03 76.5 1.88E+00 0 880.77 17 9 0.82 1762.82 1756 12 4.72E-03 85.6 1. 85E+00 T 0 925.88 12 15 5.21 1853 .11 1843 16 3.23E-03 **** 1.79E+OO T 0 957.60 8 29 4.25 1916.61 1903 15 2.29E-03 ***** 1.74E+OO 7 965. 52 23 16 2.53 1932.45 1928 18 6.35E-03 78.6 1.73E+OO T 0 1227.79 6 16 3.42 2457.39 2446 13 1.67E-03 **** 1. 43E+OO 0 1331.39 15 0 1. 06 2664.73 2659 12 4.17E-03 51. 6 1. 34E+OO T 0 1362.03 9 7 2.99 2726.06 2721 11 2.57E-03 **** 1. 31E+OO T Flag's: "T" = Tentatively associated Page 3109 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:09:59.02 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
* : DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l
3-0CT-2016 08:06:48 Sensitivity 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.44 Half life ratio : ***** *
Sample date 10-DE.C-2015 10: 35: 00 Nµclide Library : SOLID *
Sample ID G405235010 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4170E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000' *
Dry Weight : . 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff". File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCizGRAM 3.350E-01 2.374E-01 2.945E-02 3. lllE-02 2.597E-02 4.645E-02 6.062E-02 5.448E-02 6.062E-02 4. 978E-0.l 6.062E-02 8.161E-02 8.161E-02 4.645E-02 6.060E-02 8 .161E-02 6.060E-02 1.841E-01 4.776E-02 2.316E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 MN-56
C0-57 C0-58 Page 3110of5809 Le (pCi/GRAM 1. 031E+Ol 4.298E-02 0.000E+Ob 1. 7 52E-02 O.OOOE+OO O.OOOE+OO 5.997E-02 4.189E-01 O.OOOE+OO 4.508E-02 4.980E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT H°LIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181* TA-182 RE-183 RE-184 Page 3111 of 5809 5.610E+00 3.483E-02 1.618E-01 2.142E+OO 8.583E+OO O.OOOE+OO l.638E-01 O.OOOE+OO O.OOOE+OO 5.428E-01 7.361E+00 7.618E-01 O.OOOE+OO 1.895E-01 4.940E+02 3.132E-02 7.544E-01 2.236E+OO 1.374E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 969E-02 4.534E-02 4.087E+00 3. 651E-01 3. 651E-01 2.456E-02 1. 271E+OO 7.322E-02 l.768E-01 O.OOOE+OO O.OOOE+OO 1. 251E-01 l.474E+OO 9.710E-02 2.441E+02 O.OOOE+OO O.OOOE+OO 8.675E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3 .175E-02 0. ,OOOE+OO 5.102E-02 1.252E-01 O.OOOE+OO O.OOOE+OO 8.616E-02 O.OOOE+OO O.OOOE+OO 2.105E+Ol O.OOOE+OO 3.214E-01 4.693E-02 4.069E+OO 3.710E-02 O.OOOE+OO 7.706E+02 O.OOOE+OO 2.232E-02 7.233E-02 1.490E-01 1.033E-01 1*. 057E-Ol 1.434E+OO 4.950E-02 l.998E+Ol l.977E-01 5. 621E-02 2.312E-02 3.846E+OO 6.694E-01 2.692E+OO 2.985E+Ol NOT IDENT.

FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT. I DENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. 'FAIL *ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 ' U-238 NP-239 PU-239 AM-241 CM-243 Bl):-247 CM-247 CF-249 CF-251 Page 3112 of 5809 9.753E+Ol 4. OllE-01 2.303E+OO 4.464E-02 3.470E+OO 3.870E-01 6.215E-01 7.072E-01 3. ll 7E-01 6.062E-01 l.947E-01 1. 947E-01 3.992E-01 4.623E-01 6.062E-01 4.992E-02 2.623E-01 3.742E+OO 1.277E+OO 4.992E-02 O.OOOE+OO 1.277E+OO 2 .119E-01 3.004E+02 1. 229E-01 8.493E-02 5.780E-02 2.716E-02 3.394E-02 1. lOlE-01 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:10:04.79 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l * *Acquisition date 3-0CT-2016 08:06:48 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.44 Half life ratio : ***** *
Sample date 10-DEC-2015 10:35:00 Nuclide Library : SOLID *
Sample ID G405235010 Analyst initials: MXRl *
Batch Number 1596247 *sample Quantity :* 1.4170E+02 GRAM *
Quantity Err(%) : 1.4115E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act* Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1. 548E+Ol 1.840E+OO 1.840E+OO SC-46 2.379E-01 5.139E-01 5 .139E-01 BA-137M 2.937E-01 8.786E-02 8.786E-02 CS-137 3.103E-01 9.281E-02 9.281E-02 TL-208 4. 280E-01* 8.516E-02 8.516E-02 PB-212 1.llOE+OO 1.533E-01 1.533E-01 BI-214 7.738E-01 1.854E-01 1.854E-01 PB-214 1.128E+OO 2.179E-01 2.179E-01 RN-222 7.738E-01 l.854E-01 l.854E-01 RA-224 3.884E-01 1.384E+OO 1.384E+OO RA-226 7.738E-01 l.854E-01 1.854E-01 AC-228 1.118E+OO 2.804E-01 2.804E-01 RA-228 1.118E+OO 2.804E-01 2. 804E,.-01 TH-228 1. llOE+OO 1.533E-01 1.533E-01 TH-230 7.735E-01 1.853E-01 1.853E-01 TH-232 1.118E+OO 2.804E-01 2.804E-01 U-234 7.735E-01 l.853E-01 1.853E-01 U-235 5.665E-02 2.136E-01 2.136E-01 AM-243 l.494E-01 1.088E-01 1.088E-01 ANH-511 7.735E-02 7.615E-02 7.615E-02 Non-Identif{ed Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1. 688E+OO 1.184E+Ol 1.186E+Ol NOT IDENT. NA-22 2.246E-02 4.684E-02 4.792E-02 NOT IDENT. NA-24 -l;OOOE+41 3.866E+41 0.000E+OO SHORT HLIF AL-26 -2.222E-02 2.868E-02 3.038E-02 NOT IDENT. V-48 1.361E+03 1.431E+04 1.432E+04 SHORT HLIF CR-51 2.139E+02 4.368E+02 4.473E+02 SHORT HLIF MN-54 5.688E-03 6.780E-02 6.785E-02 NOT IDENT. C0-56 8.791E-02 4.665E-01 4.682E-01 NOT IDENT. MN-56 1.000E+41 5.403E+41 O.OOOE+OO SHORT HLIF C0-57 1. 294E-02 5.206E-02 5.239E-02 NOT IDENT. Page 3113of5809 C0-58 -2.229E-01 6.007E-01 6. 091E-01 NOT IDENT. FE-59 -4.196E+OO 7.288E+OO 7.530E+oo* NOT IDENT. C0-60 6.396E-02 3.246E-02 4.342E-02 FAIL ABUN ZN-65 5.230E-02 2.045E-01 2.059E-01 NOT IDENT. GE-68 -4.752E-01 2.518E+OO 2.527E+OO NOT IDENT. AS-73 2.390E+OO 9.602E+OO 9.662E+OO NOT IDENT. AS-74 2.106E+03 6 .. 005E+03 6.079E+03 SHORT HLIF SE-75 -8.366E-02 2.154E-01 2.187E-01 NOT IDENT. BR-77 l.137E+38 9.776E+38 O.OOOE+OO SHORT HLIF SR-82 l.331E+03 l.192E+03 l.335E+03 SHORT HLIF RB-83 -3.177E-02 6.447E-01 6.449E-01 NOT IDENT. KR-85 8.201E+OO 8.460E+OO 9.233E+OO NOT IDENT. SR-85 8.474E-01 8.758E-01 9.555E-01 NOT IDENT. RB-86 -l.586E+04 2.900E+04 2.987E+04 SHORT HLIF Y-88 .4.586E-02 2.072E-01 2.082E-01 NOT IDENT. Y-91 -3.295E+Ol 5.892E+02 5.894E+02 NOT IDENT. NB-94 2.235E-02 3.465E-02 3.609E-02 NOT IDENT. NB-95 -2.932E-01 8.910E-01 9.008E-01 NOT IDENT. NB-95M 2.382E+OO 2.526E+OO 2.745E+OO NOT IDENT. ZR-95 l.093E+OO l.412E+OO l.495E+OO NOT IDENT. NB-97 l.OOOE+41 l.512E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 8.363E+40 O.OOOE+OO SHORT HLIF M0-99 -3.736E+30 1. 083E+32 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 1. 363E+42 O.OOOE+OO SHORT HLIF RH-101 -2.385E-02 3.749E-02 3.900E-02 NOT IDENT. RH-102 -4.469E-02 6.207E-02 6.525E-02 NOT IDENT. RU-103 3.193E+OO 4.630E+OO 4.848E+00 FAIL ABUN RH-106 -4 *.160E-01 5.102E-01 5.436E-01 NOT IDENT. RU-106 -4.160E-01 5.102E-01 5.436E-01 NOT IDENT. AG-108M 6.887E-03 2.765E-02 2.782E-02 NOT IDENT. CD-109 l.426E+OO 3.109E+OO 3.174E+OO FAIL ABUN AG-llOM 7.324E-03 1.277E-01 l.278E-01 NOT IDENT. SN-l13 -l.797E-01 2.264E-01 2.404E-01 NOT IDENT. CD-l15 2.208E+38 l.854E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -6.889E+04 1.022E+05 l.068E+05 SHORT HLIF TE-123M 3.932E-02 1.466E-01 l.477E-01 NOT IDENT.
SB-124 2.091E-01 1. 723E+OO l.725E+OO NOT IDENT. SB-125 7.877E-02 1.031E-01 l.090E-01 NOT IDENT. TE-125M 4 .114E+Ol 2.824E+02
2. 830E+02 NOT IDENT. I-126 9.719E+05 8.215E+05 9.310E+05 SHORT HLIF SB-126 5.345E+05 8. 831E+05 9.154E+05 SHORT HLIF SN-126 9 .114E-02 1. 986E-01 2.028E-01 FAIL ABUN SB-127 -4.249E+21 l.884E+22 O.OOOE+OO SHORT HLIF I-131 -l.546E+09 4.262E+09 4.318E+09 SHORT HLIF I-132 l.OOOE+41 1.921E+42 O.OOOE+OO SHORT HLIF TE-132 1.165E+25 2.678E+26 O.OOOE+OO SHORT HLIF BA-133 -2.253E-02 4.415E-02 4.530E-02 NOT IDENT. I-133 -l.OOOE+41 2.154E+41 O.OOOE+OO SHORT HLIF CS-134 3.080E-02 5.429E-02 5.603E-02 NOT IDENT. CS-135 6.612E-02 l.344E-01 1. 376E-01 NOT IDENT. I-135 l.OOOE+41 7. l13E+41-O.OOOE+OO SHORT HLIF CS-136 4. 311E+04 2.769E+05 2.775E+05 SHORT HLIF CE-139 -1.225E-01 l.059E-01 1.195E-01 NOT IDENT. BA-140 2.989E+06 3.994E+06 4.215E+06 SHORT HLIF LA-140 -1.434E+05 4. 6l1E+05 4.656E+05 SHORT HLIF CE-141 -2.890E+Ol 2.762E+Ol 3.054E+Ol NOT IDENT. CE-143 l.OOOE+41 4.669E+41 O.OOOE+OO SHORT HLIF CE-144 -2.293E-01 4.018E-01 4.149E-01 NOT*IDENT. PM-144 l.91iE-02 5.354E-02 5.423E-02 NOT IDENT. PR-144 l.643E+OO 4.643E+OO 4.702E+OO NOT IDENT. PM-146 7.738E-04 4.315E-02 4.315E-02 NOT IDENT. ND-147 -2.366E+06 3.238E+07 3. 23.9E+07 SHORT HLIF PM-147 l .114E+02 8.989E+02 9.003E+02 NOT IDENT. PM-149 6.778E+39 2.648E+40 0.000E+OO SHORT HLIF EU-150 l.735E-02 2.585E-02 2.701E-02 FAIL ABUN EU-152 -l.553E-02 8.440E-02 8.469E-02 FAIL ABUN GD-153 -l.236E-01 1.840E-01 1.922E-01 NOT IDENT. EU-154 4.809E-02 l.136E-01 l.156E-01 NOT IDENT. EU-155 9.599E-02 l.157E-01 l.235E-01 NOT IDENT. TB-160 2.821E+OO 2.373E+OO 2.693E+OO FAIL ABUN H0-166M ..:l.197E-02 6 .196E-02 6.219E-02 NOT IDENT. TM-171 -1.198E+00 2.291E+Ol 2.292E+Ol NOT IDENT. HF-172 -1.589E-01 2.496E-01 2.597E-01 NOT IDENT. LU-172 -4.140E-02 7.402E-02 7.633E-02 FAIL ABUN LU-176 -2.567E-03 2.640E-02 2.643E-02 FAIL ABUN HF-181 6.322E-01 4.424E+OO 4.433E+OO NOT IDENT. TA-182 -3. 562E-0.l 1.000E+OO l.013E+OO FAIL ABUN RE-183 -6.587E-01 3.103E+OO 3 .117E+OO NOT IDENT. Page 3114 of 5809 RE-184 1.787E+Ol 3.215E+Ol 3.315E+Ol NOT IDENT. W-188 4.322E+Ol l.162E+02 l.178E+02 NOT IDENT. IR-192 -2.023E-01 4. 7 51E-01 4.838E-01 FAIL ABUN HG-203 2.180E+OO *2.403E+OO 2.597E+OO NOT IDENT. BI-207 3.199E-02 4.677E-02 4.894E-02 FAIL ABUN PB-210 3.202E-01 3.896E+OO 3.898E+OO NOT IDENT. BI-211 3.107E+OO 6.024E-01 l.525E+OO FAIL ABUN PB-211 3.286E-01 6.807E-01 6. 966E-01 NOT IDENT. BI-212 1.489E+OO 1.333E+OO l.492E+OO FAIL ABUN RN-219 5.262E-02 3.532E-01 3.540E-01 FAIL ABUN RA-223 5.300E-01 6.670E-01 7.085E-01 FAIL ABUN AC-227 -8.847E-02 2.259E-01 2.294E-01 NOT IDENT. TH-227 -8.847E-02 2.259E-01 2.294E-01 NOT IDENT. TH-229 -2.527E-01 4.572E-01 4. 712E-01 FAIL ABUN PA-231 1.510E-02 5.457E-01 5.458E-01 NOT IDENT. TH-231 5.300E-01 6.670E-01 7.085E-01 FAIL ABUN PA-233 -2.707E-02 5.937E-02 6.062E-02 NOT IDENT. PA-234 2.153E-02 3.0lOE-01 3.012E-01 FAIL ABUN PA-234M -1.253E+OO 4.257E+OO 4.294E+OO NOT IDENT. TR-234 -2.636E-01 1.458E+OO 1.463E+OO FAIL ABUN NP-237 -2.707E-02 5.937E-02 6.062E-02 NOT IDENT. NP-238 3.888E+40 2.708E+41 O.OOOE+OO SHORT HLIF U-238 -2.636E-01 1.458E+OO 1.463E+OO FAIL ABUN NP-239 -l.749E-01 2.655E-01 2.769E-01 NOT IDENT. PU-239 2.404E+02 3.355E+02 3.526E+02 NOT IDENT. AM-241 -9.236E-02 l.473E-01 1. 531E-01 NOT IDENT. CM-243 -1.132E-01 l.097E-01 l.210E-01 NOT IDENT. BK-247 8.431E-03 7.090E-02 7.lOOE-02 NOT IDENT. CM-247 -2.331E-02 3.455E-02 3. 611E-02 NOT IDENT. CF-249 l.601E-02 3.727E-02 3.796E-02 NOT IDENT. CF-251 5.780E-02 l.163E-01 l.192E-01 NOT IDENT. Page 3115of5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 54.1856 87.09 145.3838 136.47 79.0660 45.60 74.3617 87.57 145.4961 140.51 0.0000 46.54 69.2816 88.03 145.6035 143.76 89.5680 49.72 0.0000 88.34 68.2860 144.24 85.9352 51. 35 67.9370 88.47 68.3002 145.44 110. 6419 51. 87 64.8281 89. 96 112. 5823 152.43 80.5468 52.39 63.8395 1093.63 91.3812 153.25 0.0000 52.97 73.5099 91.11 0.0000 323.87 74.4983 53.44 63.9880 92.59 91.6608 156.02 0.0000 54.07 61.9405 93.35 91.7688 158.56 0.0000 57.36 0.0000 94.56 81.2139 159.00 77.3884 57.53 62.4014 94.65 81.2247 162.33 82.6783 57.98 75.3828 94.67 81.2274 162.66 0.0000 59.27 77.7448 94.87 81.2522 163.33 71. 8994 59.32 85.3120 97.43 83.1077 165.86 82.1522 59.54 85.3506 98.43 84.3884 176.31 71.1835 60. 96. 81. 2 642 98.44 8'4.3895 176.60 0.0000 61.17 96.4746 99.53 83.3692 177.52 69.5737 62.93 96.8158 .100.11 81.1228 181.07 0.0000 63.29 106.6823 . 102.03 79.0276 181.52 74.1134 63.58 103.4757 103.18 97.7857 184.41 85.8591 64.28 93.8020 103.37 96.6488 143.76 72.7105 66.73 105.2073 105.21 70.0518 193.51 75.8461 67.24 116.2796 105.31 70.0616 197.03 74.3699 125.81 107.5942 106.12 79.4950 198.01 65.7826 67.75 107.6077 106.47 87. 7224 201.83 89. 4712 69.67 113.5081 109.28 75.1533 203.43 8 6. 9'934 70.83 92.7684 111. 00 80.0413 205.31 67. 9723 72.81 115.2734 111.76 0.0000 210.85 61. 7463 72.87 124.1534 114. 06 68.5577 215.65 65. 9691 74.66 111.2091 116. 30 0.0000 222 .11 53.0750 74.82 111.2404 116.74 88.9727 227.09 55.0794 74.97 111. 2701 119.76 89.3297 227.38 58.6476 77.11 111. 6913 121.12 77.5574 228.16 0.0000 78.74 112.0079 121. 22 77.5674 228.18 66.6901 79.69 92.7446 121.78 78.8186 116.74 66.6901 80.12 92.8127 122.06 77.6527 235.69 55.0331 80.19 0.0000 122.92 84.9149 235. 96 64.4429 80.57 92.8839 123.07 78.9505 238.63 . 64. 5857 81. 00 92.9514 265.00 79.0125 238.98 0. 0000 81. 07 92. 9628 125.81 87.6315 240.99 64.7109 81. 75 123.0918 127.23 92.5992 242.00 64.7644 83.79 115.9809 127.91 91. 4755 244.70 59.4983 84.00 116.0217 129.30 74.7546 252.40 0.0000 85.43 144.9912 131.20 100.3128 252.80 46.2753 86.55 145.2559 133.02 86.0026 254.15 0.0000 86.79 145.3125 133.52 93.3268 256.23 56.4086 86.94 145.3477 136.00 81.4518 260.90 0.0000 Page 3116 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.0791 355.39 -0.0000 .584.27 19.7366 264.80 49.4583 356.01 39.4964 595.83 0.0000 265.00 38.4735 364.49 0.0000 427.87 28.7083 268.22 44. 0771 366.42 0.0000 602.52 0.0000 269.46 44 .1191 372.51 38.4192 604. 72 23.2277 270.03 44.1377 375.05 41. 4377 607.14 23.2507 271.23 44.1777 377.52 31.1245 609.32 28.8131 273.65 0.0000 356.01 44.6301 610.33 28.8258 276.40 59.1328 388.16 30.8228 614.28 18.3235 277.37 44.3818 388.63 0.0000 618.01 30.0300 2.77.60 44.3887 391. 69 39.8535 620. 36 14.4727 278.00 44.4023 264.66 29.0431 621. 93 26.7363 279.20 44.4414 401. 81 28.0598 630.19 0.0000 279.54 44.4531 402.40 38.0943 631. 29 26.8389 279.70 44.4580 404.85 31.1198 633.25 16.7877 280.46 44.4834 410.95 27.8021 634.78 0.0000 283.69 43.1955 413.71 33.2927 635.95 29.1305 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.4591 423.72 0.0000 645.85 21. 3727 285.90 0.0000 427.09 31.5064 657.76 11.8672 287.50 45.6434 427.87 24.4023 657.90 0.0000 290.67 36.4117 433.94 27.5427 661. 66 22.6392 293.27 0.0000 439.40 27.6235 664.57 0.0000 351.93 59. 0112 453.88 27.8350 666.33 0.0000 295. 96 59.0420 463.37 31.0797 666.50 0.0000 879.38 77.4596 468.07 30 .1163 667. 71 0.0000 299.98 46.5221 473.00 0.0000 677.62 14.8070 300.09 46.5251 475.06 32.3074 685.70 0.0000 300.13 49.3459 476.78 23.9906 695.00 0.0000 301.36 67.7329 477.60 25.0439 696.49 17.2083 302.85 69.6866 482.18 28.2387 696. 51 17.2083 256.23 49.9689 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.2137 306.78 52.8805 497.08 11.0627 697.49 18.3626-308.46 47.2697 505.52 14.2817 702.65 20.6982 311. 90 47.3806 507.63 0.0000 706.68 26.4871 316.51 50.3819 511. 00 26.5170 711. 68 24.2291 319.41 0.0000 514.00 27.0854 720.70 0.0000 320.08 0.0000 514.00 27.0854 721.93 0.0000 321. 04 48.6281 520.40 24.5039 722.78 10.4268 323.87 42.4154 520.69 0.0000 722.91 10.4271 325.23 48.7640 522.65 0.0000 723.31 10.4286 328.76 0.0000 527.90 0.0000 724.19 13.9092 333.37 49.0255 528.26 32.0801 727.33 10.4440 333.97 30.2926 52.9.59 30.4946 733.00 13.9541 334.37 34.6289 529.87 0.0000 735.93 20.9531 338.28 41.4673. 531.02 0.0000 333.97 17.4707 338.32 41.4682 537.26 0.0000 739.50 0.0000 311.90 39 .1116 546.56 0.0000 747.24 20.1622 340.48 39 .1116 552.55 20.5439 748.06 21. 0447 340.55 0.0000 563.25 19.5564 7 52 .. 31 19.3205 344.28 33.8820 569.33 23. 9658 753.82 0.0000 345.93 46.5156 946.00 25.0570 756.73 14.9528 351.06 33.0558 569.70 25.0599 756.80 14.9533 351. 93 33.0738 583.19 19.7278 884.68 24.6914 Page 3117 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.4725 1274.44 12.3387 1620.50 4.3926 766.42 29.1258 1001.03 15.2065 1621. 92 2.1969 766.84 28.2471 1002.74 10.4595 1678.03 0.0000 772.60 0.0000 1004.73 13. 3198 1690.97 3.3391 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 5.4152 778.90 17.7289 1028.54 0.0000 1063.66 12.6485 783.70 0.0000 1037.84 15.3643 1771.35 7.2293 785.37 15.1033 1038.76 0.0000 1791.20 0.0000 792.07 25.8237 631.29 18.2903 1808.65 6.3680 794.95 22.2839 1048.07 0.0000 1810.72 0.0000 795.86 20.5075 1049.04 15.4121 1836 .. 06 3.6564 810.06 25.0862 1050.41 10.5999 810.29 25.0879 1063.66 10.6381 344.28 22.4007 1077.00 0.0000 810.76 22.4037 1077.34 15. 5313 815.77 0.0000 1085.87 12.6485 1048.07 0.0000 1093.63 16.5746 832.01 17.1474 1099.45 21.4817 834.85 21. 6797 1112. 07 13.7163 835. 71 17.1683 1112. 84 16.6586 836.80 0.0000 1115. 54 15.6895 846.75 0.0000 1120.29 15.7090 846.77 17.2303 1120.55 15.7100 856.80 0.0000 1221.41 17.2842 860.56 12.7529 1129.67 14.7629 871. 09 9.1397 1131. 51 0.0000 873.19 16.4625 1147.95 0.0000 875.33 0.0000 1173.23 17.9143 879.38 14.6621" 1177.95 18.9316 880.51 14.6675 1189.05 15.9863 883.24 11. 0098 1204.77 20.0610 884.68 11. 0149 1221.41 16 .1143. 889.28 8.8245 1231.02 19.3828 894.76 13.8121 1235.36 0.0000 898.04 15.6698 1238.28 23.2597 900.72 21.2179 1260.41 0.0000 903.28 16.6185 1271. 87 12.2329 911.20 9.2551 1274.44 10.2002 912.08 9.2575 1274.54 10.2008 923.98 0.0000 1291. 59 14.3375 926.50 12.0875 1298.22 0.0000 929 .11 11. 9109 1312 .11 0.0000 937.49 21. 4572 1332.49 8.2705 944.13 0.0000 1362.66 0.0000 946.00 18.7054 1365 .19 6.6652 949.00 25.4626 1368.63 0.0000 667.71 0.0000 1384.29 7. 3213 962. 31 16.5408 1408.01 6.3080 964. 08 16.5494 1457.56 0.0000 966 .17 18.8177 1460.82 12.7595 911.20 18.8330 1489.16 3.2087 968.97 18.8330 1505.03 5.3656 983.53 0.0000 1584.12 9. 8135 984.45 0.0000 1596.21 0.0000 Page 3118of5809 VAX/VMS Nuclide Identific9tion Report Gener_ated 3-0CT-2016 09: 10: 36. 59 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 9-DEC-2015 10:13:00. Acquisition date : 3-0CT-2016 08:07:11. *Sample ID G405235011 Sample quantity 1.46502E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.76 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 3 4 3 5. 3 6 0 7 0 8 0 9 2 10 2 11 0 12 1 13 1 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 3119of5809 Energy 63.53* 76.04* 87. 05* 89.79 92.69* 163.14* 185.81* 209.23 238.67* 241.72 253 .11 269.69 271.20 279.74 295.23 300.38 328.33* 338.46* 351.84* 405.09 410.63 462.59 510.76* 583.10* 609.29* 653.95 661.69 726.96 769.04 805.86 825.89 860.69 880.86 894.48 BACKGROUND CORRECTED SAMPLE PEAK* REPORT Area 7 27.!! 70 43 61 15 95 33 343 100 24 31* 28 20 176 15 48 60 263 27 18 48 20 114 215 5 85 23 14 12 12 19 15 24 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 123 283 193 127 148 63 125 73 74 88 48 58 54 108 69 57 48 70 51 28 44 33 52 41 24 29 30 20 19 17 8 18 14 14 0.83 3.34 1. 31 1. 01 1. 37 1. 35 1. 27 1.11 1.18 1. 48 0.65 1. 25 1. 25 2.28 0.97 0.97 1. 22 0.81 1. 05 1. 67 1. 27 4.52 1. 21 1. 20 1. 31 0.84 1. 51 2.41 1. 49 1. 03 1. 28 1. 98 4.75 0.62 127.17 152.16 174.15 179.62 185.41 326.13 371.42 418.20 477.02-483 .11 505.86 539.00 542.00 559.08 590.01 600.32 656.16 676.40 703.14 809.54 820.61 924.45 1020.71 1165. 31 1217.67 1306.93 1322.41 1452.90 1537.04 1610.67 1650.71 1720.32 1760.64 1787.88 124 146 168 168 168 324 367 415 472 472 502 534 534 551 584 596 653 671 697 805 815 917 1015 1158 1210 1298 1317 1447 1533 1605 1646 1713 1753 1779 6 1.85E-03281.l 14 7.61E-02 14.4 24 1.94E-02 34.5 1.69E+OO 24 1.18E-02 44.1 24 1.70E-02 41.6 5 4.03E-03 90.4 11 2.63E-02 26.4 7 9.llE-03 47.0 17 9.52E-02 6.9 l.29E+OO 17 2.78E-02 20.4 8 6.54E-03 55.0 12 8.59E-03 44.7 2.12E+OO 12 7.68E-03 51.3 14* 5.47E-03115.7 12 4.89E-02 12.l 8 4.27E-03 88.1 9 1. 34E-02 30. 9 10 1.65E-02 29.7 12 7.30E-02 8.3 9 7.43E-03 41.1 11 5.00E-03 75.2 15 1.32E-02 30.3 13 5.55E-03 92.7 14 3.16E-02 15.6. 14 5.99E-02 8.5 13 1.44E-03219.5 11 2.35E-02 16.7 10 6.43E-03 41.7 8 3.83E-03 63.6 9 3.19E-03 72.0 9 3.25E-03 54.2 11 5.18E-03 50.8 14 4.05E-03 60.5 18 6.75E-03 40.9 Peak Search Report (continued) Page : 2 Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 34* 93 18 1. 23 1821. 60 .1815 12 2.60E-02 14.0 36 0 934.66 28 8 1. 44 1868.25 1861 15 7.64E-03 28.9 37 0 967. 81 62 23 6.61 1934.54 1924 18 1.73E-02 21. 9 38 0 979.57 12 14 0.94 1958.08 1948 14 3.33E-03 72 .2 39 0 1120.52* 53 16 1.17 2240.03 2234 13 1.48E-02 21. 0 40 0 1166. 35 10 4 0.71 2331.73 2328 8 2.67E-03 53.1 41 0 1195.46 11 9. 1. 38* 2389.97 2386 9 2.99E-03 62.5 42 0 1238.94 17 12 2.42 2476.97 2472 10 4.69E-03 46.0 43 0 1461. 02* 355 9 1. 87 2921.43 2913 17 9.85E-02 5.7 44 0 1592.82* 10 2 1. 63 3185.30 3182 7 2.80E-03 41. 0 45 0 *1765.02* 30 0 1. 72 3530.12 3524 12 8.28E-03 19.5 Flag: "*" = Peak area was modified by background subtraction Page 3120 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:10:39 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 9-DEC-2015 10:13:00 G405235011 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:07:11 146.50 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA33 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-2-14 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 77 .11 PB-214 77 .11 PB-214 77 .11 PB-214 77 .11 PB-214 77 .11 PB-214 351.93 Page 3121of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 TH-228 77 .11 PB-212 77 .11 PB-214 77 .11 AM-243 74.66 TH-228 74.82 PB-212 74.82 TH-228 77 .11 PB-212 77 .11 BI-211 351.06 CAN 0 01:00:00.76 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235011 Acquisition date 3-0CT-2016 D8:07:11 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.133E+OO l.447E+Ol l.447E+Ol 11. 37 OK CD-109 88.03 3.70* 4.889E+OO 1.205E+OO 1.888E+OO 142.57 OK SN-126 64.28 9.60 2.483E+OO l.819E-01 1. 819E-01 562.28 OK 86.94 8.90 4.889E+OO 5.0lOE-01 5.0lOE-01 142.57 OK 87.57 37.00* 4.889E+OO l.205E-01 1.205E-01 142.57 OK CS-135 268.22 16.00* 4.353E+OO 2.570E-01 2.570E-01 89.36 OK BA-137M 661. 66 89.90* 2 .115E+OO 2.371E-01 2.416E-01 33.30 OK CS-137 661. 66 85.10* 2.115E+OO 2.505E-01 2.553E-01 33.30 OK HG-203 70.83 3.69 3.364E+OO Line Not Found Absent 72. 87 6.19 3.591E+OO Line Not Found Absent 279.20 81.56* 4.230E+OO 3.294E-02 2.813E+OO 231.47 OK TL-208 277.37 6.60 4.258E+OO Line Not Found Absent 583.19 85.00* 2.334E+OO 3.090E-01 3.090E-01 31.11 OK 860.56 12.50 1.727E+OO 4.495E-01 4.495E-01 101. 63 OK PB-212 74.82 10.28 3.925E+OO 2.323E+OO 2.323E+OO 56.07 OK 77 .11 17.10 3.925E+OO 1.397E+OO 1.397E+00 56.07 OK 238.63 43.60* 4.775E+OO 9.622E-01 9.622E-01 13.75 OK 300.09 3.30 3. 996E+OO 6.688E-01 6.688E-01 176.29 OK BI-214 609.32 45.49* 2.255E+OO, 1.129E+OO 1.129E+OO 17.00* OK 1120.29 14.92 1.407E+OO 1.289E+OO 1.290E+OO 41. 98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 OK PB-214 '74. 82 5.80 3.800E+OO Line Not Found <<INT Reject* 77 .11 9.70 4.033E+OO Line* Not Found -----<<INT Reject 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4.727E+OO Line Not Found <<INT Reject 295.22 18.42 4.052E+OO 1.353E+OO 1.353E+OO 24.17 OK 351.93 35.60* 3.513E+OO 1.187E+OO 1.187E+OO ' 16. 59 OK RN-222 609.32 45.49* 2.255E+OO 1.129E+OO 1.129E+OO 17.00 OK 1120. 29 14.92 1.407E+OO 1.289E+OO 1.290E+OO 41. 98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 OK RA-224 240.99 4.10* 4.731E+00 6.267E-01 6.267E-01 216.97 OK RA-226 609.32 45.49* 2.255E+00 1.129E+OO 1.129E+OO 17.00 OK 1120.29 14.92 1.407E+OO 1.289E+OO 1.290E+OO 41.98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.627E+OO 8.265E-01 8.265E-01 59.37 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835.71 1. 61 1.766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 OK 968. 97 15.80 l.578E+OO 1.282E+OO 1. 282E+00 43.90 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.627E+OO 8.265E-01 8.265E-01 59.37 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 OK 968. 97 15.80 1. 578E+OO 1.282E+OO 1.282E+OO 43.90 OK TH-228 74.82 10.28 3.925E+OO 2.323E+OO 2.323E+OO 56.07 OK 77 .11 17.10 *3.925E+OO 1.397E+OO 1.397E+OO 56.07 OK 238.63 43.60* 4.775E+00 9.622E-01 9.622E-01 . 13. 75 OK Page 3122 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error ,Status 300.09 3.30 3. 996E+OO 6.688E-01 6.688E-01 176.29 OK TH-230 609.32 45.49* 2.255E+OO 1.129E+OO 1.129E+OO 17.00 OK 1120.29 14.92 1.407E+OO 1.289E+OO 1.289E+OO 41. 98 OK 1764.49 15. 30. 9.589E-Ol 9.830E-01 9.830E-01 38.98 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent 301.36 5.35* 3. 996E+OO 4.125E-01 4.125E-01 176.29 OK TH-232 105.21 1.10 5.839E+OO Line Not Found -----Absent 338.32 11. 27 3.627E+OO 8.265E-01 8.265E-01 59.37 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* l.653E+OO 1.133E+OO 1.133E+OO 28.05 OK 968. 97 15. 80 . l.578E+OO 1.282E+OO 1.282E+00 43.90 OK TH-234 63.29 3.70* 2.483E+OO 4.719E-01 4.719E-01 562.28 OK *92. 59 4.23 5.263E+OO 1. 738E+OO l.738E+OO 83.28 OK U-234 609.32 45.49* 2.255E+OO 1.129E+OO l.129E+OO 17.00 OK 1120.29 14.92 l.407E+OO 1.289E+OO 1.289E+OO 41. 98. OK 1764.49 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 OK U-235 89. 96 3.47 5.080E+OO 1.5'.55E+OO l.535E+00 88.12 OK 93.35 5.60 5.263E+OO 1.312E+OO. 1.312E+OO 83.28 OK 143. 7 6 '10.96* 6.181E+OO Line Not Found -----Absent 163.33 5.08 5.966E+OO 2.895E-01 2.895E-01 180.74 OK 185. 72 57.20 5.616E+OO 1. 761E-01 l.761E-01 52.74 OK 205.31 5.01 5.295E+OO Line Not Found Absent U-238 63.29 3.70* 2.483E+OO 4. 719E-01 4. 719E-01 562.28 OK 92.59 4.23 5.263E+OO 1.738E+OO 1. 738E+OO 83.28 OK AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.925E+OO 3.554E-01 3.555E-01 5'6. 07 OK ANH-511 511. 00 100.00* 2.593E+00 4.207E-02 4.207E-02 185.33 OK Flag: "*" = Keyline Page 3123 of 5809 VAX/VMS Nuclide Identification Report Generated Q3-0CT-2016 09:10:40.68 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l *
Acquisition date 3-0CT-2016 08:07:11 Sensitivity : 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 15.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
Sample date 9-DEC-2015 10:13:00 Analyst initials: MXRl *
Sample ID G405235011 Sample Quantity 1.4650E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File . : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;B
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-s igma) (pCi/GRAM K-40 l.447E+Ol 1.613E+OO 6.678E-01 CD-109 1. 888E+OO 2.638E+OO. 2.312E+OO SN-126 1.205E-01 1.684E-01 l.485E-01 CS-135 2.570E-01 2.250E-01 2.458E-01 BA-137M 2.416E-01 7.886E-02 7.398E-02 CS-137 2.553E-01 8. 331E-02 7.816E-02 HG-203 2.813E+OO 6.381E+OO 4.499E+OO TL-208 3.090E-01 9.423E-02 6.624E-02 PB-212 9.622E-01 1. 297E-01 8.860E-02 BI-214 1.129E+OO 1. 881E-01 1.126E-01 PB-214 1.187E+OO 1. 931E-01 9.264E-02 RN-222 1.129E+OO 1.881E-01 1.126E-01 RA-224 6.267E-01 l.333E+OO 9.496E-01 RA-226 1.129E+OO 1.881E-01 1.126E-01 AC-228 1.133E+OO 3 .115E-01 l.924E-01 RA-228 1.133E+OO 3 .115E-01 l.924E-01 TH-228 9.622E-01 1.297E-01 8.860E-02 TH-230 1.129E+OO 1.880E-01 l.125E-01 PA-231 4.125E-01 7.127E-01 6.999E-01 TH-232 l.133E+00 3 .115E-01 1.924E-01 TH-234 4. 719E-01 2.600E+OO 2.657E+OO U-234 1.129E+OO 1.880E-01 1.125E-01 U-235 6.013E-02 2.029E-01 3.875E-01 U-238 4. 719E-01 2.600E+OO 2.657E+OO AM-243 3*. 555E-01 l.953E-01 9.832E-02 ANH-511 4.207E-02 7. 641E-02 5.558E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -5.945E-01 1.274E+Ol 2.471E+Ol NOT IDENT. NA-22 -4.517E-02 3.949E-02 6.094E-02 NOT IDENT. NA-24 O.OOOE+OO l.335E+41 O.OOOE+OO SHORT HLIF AL-26 -5.270E-03 2.490E-02 5.224E-02 NOT IDENT. Page 3124 of 5809 sc:...46 -6. 396E-02 3.082E-01 5.412E-01 FAIL ABUN V-48 O.OOOE+OO 1.507E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 4.031E+02 0.000E+OO SHORT HLIF MN-54 3.719E-03 6.319E-02 l.223E-01 NOT, I DENT. C0-56 1.604E-02 4.266E-01 8.360E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF C0-57 l.222E-02 4. 696E-02 9.024E-02 NOT IDENT. C0-58 -2.268E-01 4.725E-01 8.438E-01 NOT IDENT. FE-59 -1.039E+OO 5.646E+OO 1.133E+Ol NOT IDENT. C0-60 -6.480E-03 3.547E-02 7.091E-02 NOT IDENT. ZN-65 7.180E-02 1. 755E-01 3.441E-01 NOT IDENT. GE-68 1.522E+OO 2.297E+OO 5. lllE+OO NOT IDENT. AS-73 4.634E+OO 1.069E+Ol 2.202E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.303E+03 O.OOOE+OO SHORT HLIF SE-75 6.535E-02 l.891E-01 3.600E-01 FAIL ABUN BR-77 O.OOOE+OO 1. 785E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.736E+02 0.000E+OO SHORT HLIF RB-83 2.006E-01 5.353E-01 l.129E+OO NOT IDENT. KR-85 1. 45*0E+OO 7.081E+OO l.285E+Ol NOT IDENT. SR-85 1. 517E-01 7.411E-01 1.344E+OO NOT IDENT. RB-86 O.OOOE+OO 2.606E+04 O.OOOE+OO SHORT HLIF Y-88 -8.954E-02 2. 715E-01 5'.115E-01 NOT IDENT. Y-91 -7.957E+Ol 5.157E+02 l.010E+03 NOT IDENT. NB-94 -3.468E-03 2.946E-02 5;606E-02 NOT IDENT. NB-95 -2.194E-01 1.070E+OO 1.748E+OO NOT IDENT. NB-95M -7.068E-01 2.544E+OO 4.077E+OO NOT IDENT. ZR-95 7.376E-01 1. 301E+OO 2.776E+OO NOT IDENT. NB-:-97 O:OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1.345E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.292E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 7 93E+41 0.000E+OO SHORT HLIF RH-101 -3.358E-02 3.564E-02 6 .130E-02 NOT IDENT. RH-102 -1.877E-04 6.083E-02 1.178E-01 NOT IDENT. RU-103 -2.149E+OO 5.258E+OO 9.805E+00 FAIL ABUN RH-106 -l.854E-01 4.052E-01 7.438E-01 NOT IDENT. RU-106 -l.854E-01 4.052E-01 7.438E-01 NOT IDENT. AG-108M 6.948E-03 2. 791E-02 5.626E-02 NOT IDENT. AG-llOM 4. 396E-03 8. 931E-02 1.606E-01 NOT IDENT. SN-113 -l.097E-01 2. 371E-01 4.431E-01 NOT IDENT. CD-115 O.OOOE+OO 2.202E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 9. ll 7E+04 O.OOOE+OO SHORT HLIF TE-123M -l.092E-01 l.297E-01 2.210E-01 NOT IDENT. SB-124 -9. 972E-03 1.333E+OO 3.141E+OO NOT IDENT. SB-125 -8.818E-03 l.124E-01 2.172E-01 FAIL ABUN TE-125M 2.608E+02 2.761E+02 5.574E+02 NOT IDENT. I-126 O.OOOE+OO l.036E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.108E+o6 O.OOOE+oo* SHORT HLIF SB-127 O.OOOE+OO 1. 7B8E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.369E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.099E+26 O.OOOE+OO SHORT HLIF BA-:-133 -1.680E-02 4.204E-02 7.083E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.235E-03 4.819E-02 9.439E-02 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.923E+05 0.000E+OO SHORT HLIF CE-139 2.759E-02 'l.227E-01 2 .131E-01 NOT IDENT. BA-140 O.OOOE+OO l.265E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.156E+05 O.OOOE+OO SHORT HLIF CE-141 -2.715E+OO 2.561E+Ol 4.689E+Ol NOT IDENT. CE-143 O.OOOE+OO l.121E+41 O.OOOE+OO SHORT HLIF. CE-144 -1.632E-01 3.535E-01 6.338E-01 NOT IDENT. PM-144 9.472E-04 5.455E-02 1.054E-01 NOT IDENT. PR-144 1.446E-01 4.746E+OO 9.187E+OO NOT IDENT. PM-146 -3.349E-02 4. 771E-02 8.562E-02 NOT IDENT. ND-147 O.OOOE+OO 2.826E+07' O.OOOE+OO SHORT HLIF PM-147 3.068E+02 8.045E+02 1.564E+03 NOT IDENT. PM-149 O.OOOE+OO 3.366E+40 0.000E+OO SHORT HLIF EU-150 1.228E-02 2.552E-02 4.849E-02 FAIL ABUN EU-152 2.065E-02 9.906E-02 l.979E-01 NOT IDENT. GD-153 -3.455E-02 2.178E-01 3.728E-01 NOT IDENT. EU-154 -l.059E-01 9.805E-02 1. 551E-01 NOT IDENT. EU-155 -3.636E-02 l.082E-01 l.993E-01 FAIL ABUN TB-160 2.603E+OO 3.089E+OO 3.609E+OO FAIL ABUN H0-166M 2.822E-02 5.407E-02 1.130E-01 FAIL ABUN TM-171 -7.373E+OO 2.694E+Ol 5.225E+Ol NOT IDENT. HF-172 7.132E-03 2.314E-01 4.345E-01 FAIL ABUN LU-172 . 8.715E-03 6.365E-02 l.355E-01 FAIL ABUN Page 3125 of 5809 LU-176 4 .116E-03 2.251E-02 4.560E-02 FAIL ABUN HF-181 1. 807E+OO 3.986E+OO 8.302E+OO NOT IDENT. TA-182 -3.295E-01 9.705E-01 1.828E+OO FAIL ABUN RE-183 1. 712E+OO 3.502E+OO 7.147E+OO FAIL ABUN RE-184 1.509E+Ol 2.852E+Ol 6.0lOE+Ol FAIL ABUN W-188 -8.038E-01 l.136E+02 2.040E+02 FAIL ABUN IR-192 -l.862E-01 3.850E-01 7.339E-01 FAIL ABUN BI-207 4. 969E-02 5.131E-02 1.159E-01 FAIL ABUN PB-210 3.479E+OO 5.166E+OO 1.090E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.318E-01 8.701E-01 FAIL ABUN PB-211 1.262E+OO l.016E+OO 1.464E+OO FAIL ABUN BI-212 9.324E-01 7.616E-01 1.165E+OO FAIL ABUN RN-219 l.905E-02 3.799E-01 6.826E-01 FAIL ABUN RA-223 -2.012E-01 6.095E-01 1.112E+OO FAIL ABUN AC-227 -1.880E-02 2.417E-01 3.986E-01 FAIL ABUN TH-227 -1.880E-02 2.417E-01 3.986E-01 FAIL ABUN TH-229 l.531E-01 4.706E-01 8.856E-01 FAIL ABUN TH-'231 -2.012E-01 6.095E-01 l.112E+OO FAIL ABUN PA-233 1.608E-02 5.091E-02 1.053E-01 FAIL ABUN PA-234 -l.947E-02 2.525E-01 4.826E-01 FAIL ABUN PA-234M -2.344E+OO 4.564E+OO 8.080E+00 NOT IDENT. NP-237 1.608E-02 5. 091E-02 l.053E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF NP-239 l.453E-01 2.540E-01 4.982E-01 NOT IDENT. PU-239 5.633E+Ol 3.310E+02 6.237E+02 NOT IDENT. AM-241 -l.OOlE-01 l.674E-01 3.l:i9E-01 NOT IDENT. CM-243 6.895E-02 9.505E-02 1.917E-01 NOT IDENT. -2. 901E-02 7.847E-02 l'.234E-01 NOT IDENT. CM-247 5.343E-03 3.533E-02 6. 431E-02 NOT IDENT. CF-249 2.814E-02 3.785E-02 7. 964E-02 FAIL ABUN CF-251 l.066E-01 l.181E-01 2.335E-01 NOT IDENT. Page 3126 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:10:37.60 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 341 10.66* 1.133E+OO 1. 447E+Ol l.447E+Ol 11. 37 CD-109 88.03 87 3.70* 4.889E+OO 2.452E+OO 3.842E+OO 68.99 SN-126 64.28 8 9.60 2.483E+OO l.819E-01 1.819E-01 562.28 86.94 87 8.90 4.889E+OO 1.019E+OO 1.019E+OO 68.99 87.57 87 37.00* 4.889E+OO 2.452E-01 2.452E-01 68.99 CS-135 268.22 35 16.00* 4.353E+OO 2.570E-01 2.570E-01 89.36. BA-137M 661.66 88 89.90* 2 .115E+OO 2.371E-01 2.416E-01 33.30 CS-137 661.66 88 85.10* 2 .115E+OO 2.505E-01 2.553E-01 33.30 HG-203 70.83 ------3.69 3.364E+OO ------Line Not Found ------72.87 ------6.19 3.591E+OO ------Line Not Found ------279.20 22 81.56* 4.230E+OO 3.294E-02 2.813E+OO 231.47 TL-208 277.37 ------6.60 4.258E+OO ------Line Not Found ------583.19 120 85.00* 2.334E+OO 3.090E-01 3.090E-01 31.11 860.56 19 12.50 1.727E+OO 4.495E-01 4.495E-01 101. 63 BI-211 72. 87 ------1. 23 3.591E+OO ------Line Not Found ------351.06 290 '12.92* 3.513E+OO 3.270E+OO 3.270E+OO 16.59 PB-212 74.82 344 10.28 3.925E+OO 4.363E+OO . 4. 363E+OO 28.70 77 .11 344 17.10 3.925E+OO 2.623E+OO 2.623E+OO 28.70 238.63 391 43.60* 4.775E+OO 9.622E-01 9.622E-01 13*. 75 300.09 17 3.30 3. 996E+OO 6.688E-01 6.688E-01 176.29 BI-214 609.32 226 45.49* 2.255E+OO l.129E+OO 1.129E+OO 17.00 1120.29 53 14.92 1.407E+OO 1. 289E+OO 1.290E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 PB-214 74.82 344 5.80 3.925E+00 7.733E+OO 7.736E+OO 28.70 77 .11 344 9.70 3.925E+OO 4.624E+OO 4.626E+OO 28.70 87.09 87 3.41 4.889E+OO 2.660E+OO 2.661E+OO 68.99 242.00 114 7.25 4. 731E+OO 1. 707E+OO 1. 708E+OO 40.77 295.22 197 18.42 4.052E+OO l.353E+OO 1.353E+OO 24.17 351.93 290 35.60* 3.513E+OO 1.187E+OO 1.187E+OO 16.59 RN-22;2 609.32 226 45.49* 2.255E+OO 1.129E+OO 1.129E+OO 17.00 1120.29 53 14.92 1.407E+OO 1.289E+OO 1. 290E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 RA-224 240.99 114 4.10* 4. 731E+OO 3.019E+OO 3.019E+OO 40.77 RA-226 909.32 226 45.49* 2.255E+OO l.129E+OO l.129E+OO 17.00 1120.29 53 14.92 1.407E+OO 1.289E+OO 1. 290E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 AC-228 . 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 66 11. 27 3.627E+OO 8.265E-01 8.265E-01 59.37 794.95 ------4.25 1.835E+OO ------Line Not Found ------835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911. 20 94 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 968. 97 62 15.80 1.578E+OO 1.282E+OO l.282E+OO 43.90 RA-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 66 11. 27 3.627E+OO 8.265E-01 8.265E-01 59.37 794.95 ------4.25 1.835E+OO ------Line Not Found ------835. 71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 94 25.80* 1.653E+OO 1". 1J3E+OO 1.133E+OO 28.05 Page 3127 of 5809 Nuclide Line Activity Report (continued) Page : 2 .Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 62 15.80 1.578E+OO l.282E+OO 1.282E+OO 43.90 TH-228 74.82 344 10.28 3.925E+OO 4.363E+OO 4.363E+OO 28.70 77 .11 344 17.10 3.925E+OO 2.623E+OO 2.623E+OO 28.70 238.63 391 43.60* 4.775E+OO 9.622E-01 9.622E-01 13.75 300.09 17 3.30 3. 996E+OO 6.688E-01. 6.688E-01 176.29 TH-230 609.32 226 45.49* 2.255E+OO l.129E+OO 1.129E+OO 17.00 1120.29 53 14.92 1.407E+OO l.289E+OO l.289E+00 41.98 1764.49 28 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 PA-231 283.69 ------1. 70 4.183E+00 ------Line Not Found ------301.36 17 5.35* 3. 996E+OO 4.125E-01 4.125E-01 176.29 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 66 11.27 3.627E+OO 8.265E-01 8.265E-01 59.37 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 94 25.80* 1.653E+OO l.133E+OO 1.133E+OO 28.05 968.97 62 15.80 1.578E+OO 1. 282E+OO 1.282E+OO 43.90* TH-234 63.29 8 3.70* 2.483E+OO 4. 719E-01 4.719E-01 562.28 92.59 75 4.23 5.263E+OO *l.738E+OO 1.738E+OO 83.28 U-234 609.32 226 45.49* 2.255E+OO 1.129E+OO 1.129E+OO 17.00 1120.29 53 14. 92. l.407E+00 l.289E+OO 1.289E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 U-235 89. 96 53 3.47 5.080E+OO 1.535E+OO 1.535E+OO 88.12 93.35 75 5.60 5.263E+OO 1.312E+OO 1.312E+OO 83.28 143.76 ------10. 96* 6.181E+OO ------Line Not Found ------163.33 17 5.08 5.966E+OO 2.895E-01 2.895E-01 180.74 185. 72 110 57.20 5.616E+OO l.761E-01 1. 761E-01 52.74 205.31 ------5.01 5.295E+OO ------Line Not Found ------U-238 63.29 8 3.70* 2.483E+OO 4.719E-01 4. 719E-01 562.28 92.59 75 4.23 5.263E+OO 1.738E+OO 1.738E+OO 83.28 AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 344 67.20* 3.925E+OO 6.675E-01 6.675E-01 28.70 ANH-511 511. 00 21 100.00* 2.593E+OO 4.207E-02 . 4. 207E-02 185.33 Flag: "*" Key line Page 3128 of5809 Summary of Nuclide Activity Sample ID : G405235011
Acquisition date Page : 3 3-0CT-2016 08:07:11 Total number of lines in spectrum 45 Number of unidentified lines 10 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137. HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 46.59D l.41E+l0Y 7.04E+08Y 1.41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+l0Y 1.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 00 1. 02 1. 02 85.4 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 . 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.447E+Ol 2.452E+OO 2.452E-01 2.570E-01 2. 371E-01 2.505E-01 3.294E-02 3.090E-01 3.270E+OO 9.622E-01 1.129E+OO l.187E+00 1.129E+OO 3.019E+OO 1.129E+OO 1.133E+OO 1.133E+OO 9.622E-01 1.129E+OO 4.125E-01 1.133E+OO 4.719E-01 1.129E+OO 1.761E-01 4. 719E-01 6.675E-01 4.207E-02 3. 894E+Ol 3.894E+Ol Decay Corr pCi/GRAM 1. 447E+Ol 3.842E+OO 2.452E-01 2.570E-01 2.416E-01 2.553E-01 2.813E+OO 3.090E-01 3.270E+OO 9.622E-01 1.129E+OO 1.187E+OO 1.129E+OO 3.019E+OO 1.129E+OO l.133E+OO l.133E+OO 9.622E-01 1.129E+OO 4.125E-01 1.133E+OO 4. 719E-01 1.129E+OO 1. 761E-01 4.719E-01 6.675E-01 4.207E-02 4.312E+Ol 4.312E+Ol 77.78% Decay Corr 2-Sigma Error 0.165E+Ol 2.650E+OO l.691E-01 2.296E-01 0.805E-01 0.850E-01 0. 961E-01 0.543E+00 1.323E-01 0.192E+OO 0.197E+00 0.192E+OO 1.231E+OO 0.192E+OO 0.318E+OO 0.318E+OO 1.323E-01 0.192E+OO 7.273E-01 0.318E+OO 26.53E-01 0.192E+OO 0.929E-01 26.53E-01 1.916E-01 7. 797E-02 * "M" Manually accepted 2-Sigma %Error 11. 37 68.99 68.99 89.36 33.30 33.30 231. 4 7 31.11 16.59 13.75 17.00 16.59 17.00 40.77 17.00 28.05 28.05 13.75 17. 00 176.29 28.05 562.28 17.00 52.74 562.28 28.70 185.33 Flags: "K" Keyline not found "E" == Manually edited "A" == Nuclide specific abn. limit Page 3129 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235011 Acquisition date : 3-0CT-2016 *08:07:11 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.23 38 84 1.11 418.20 415 7 9. llE-03 94.0 5.23E+OO 0 253 .11 27 55 0.65 505.86 502 8 6.54E-03 **** 4.57E+OO T 1 271.20 31 60 1. 25 542.00 534 12 7.68E-03 **** 4.33E+OO T 0 328.33 53 53 1. 22 656.16 653 9 1.34E-02 61. 8 3.72E+OO T 0 405.09 29 31 1.67 809.54 805 9 7.43E-03 82.2 3.13E+OO T 0 410.63 20 48 1. 27 820.61 815 11 5.00E-03 **** 3.09E+OO T 0 . 462.59 51 36 4.52 924.45 917 15 1.32E-02 60.6 2.81E+OO T 0 653.95 5 30 0.84 1306.93 1298 13 1.44E-03 **** 2 .13E+OO 0 726.96 24 20 2.41 1452.90 1447 10 6.43E-03 83.4 1.97E+OO T 0 769.04 14 20 1. 49 1537.04 1533 8 3.83E-03 **** 1. 88E+OO 0 805.86 12 17 1. 03 1610.67 1605 9 3.19E-03 **** 1.82E+OO 0 825.89 12 8 1. 28 1650.71 1646 9 3.25E-03 **** 1.78E+OO 0 880.86 15 15 4.75 1760.64 1753 14 4.05E-03 **** 1. 70E+OO T 0 894.48 25 14 0.62 1787.88 1779 18 6.75E-03 81. 8 1.68E+OO T 0 934.66 28 8 1. 44 1868.25 1861 15 7.64E-03 57.8 1. 62E+00 0 979.57 12 14 *o.94 1958.08 1948 14 3.33E-03 **** 1.56E+OO 0 1166. 35 9 4 0.71 2331.73 2328 8 2.67E-03 **** 1.36E+OO 0 1195.46 11 9 1. 38 2389.97 2386 9 2.99E-03 **** 1.34E+OO 0 1238.94 17 12 2.42 2476.97 2472 10 4.69E-03 92.0 1 .. 30E+OO T 0 1592.82 10 1 1. 63 3185.30 3182 7 2.80E-03 82.0 1. 05E+OO Flags: "T" = T'entatively associated Page 3130 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:11:03.48 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l * *Acquisition date 3-0CT-2016 08:07:11 Sensitivity 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
Sample date 9-DEC-2015 10:13:00 Nuclide Library : SOLID *
Sample ID G405235011 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : l.4650E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.'GAMMA]EFF GAM33 CAN.CNF;8
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----,Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.762E-01 1.093E+OO 7.021E-02 l.126E-01 3.320E-02 3.507E-02 2. 071E+OO 2.954E-02 4.083E-02 4.936E-02 4.057E-02 4.936E-02 4.376E-01 4.936E-02 7.970E-02 7.970E-02 4.083E-02 4.934E-02 3.161E-01 7.970E-02 l.247E+00 4.934E-02 l.830E-01 1. 24 7E+OO 4.625E-02 2.504E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3131 of5809 Le (pCi/GRAM 1.113E+Ol 2.361E-02 O.OOOE+OO l.870E-02 2.209E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3132 of 5809 O.OOOE+OO O.OOOE+OO 5.340E-02 3.590E-01 O.OOOE+OO 4.215E-02 3.487E-01 4. 7 51E+OO 2. 91°0E-02 l.492E-01 2.233E+OO 1.022E+Ol O.OOOE+OO* 1.643E-01 O.OOOE+OO O.OOOE+OO 4. 960E-01 5.753E+OO 6.020E-01 O.OOOE+OO 2.030E-01 4.349E+02 2.452E-02 7.787E-01 l.885E+OO 1.215E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.859E-02 5.217E-02 4.323E+OO 3.156E-01 3.156E-01 2.546E-02 6.716E-02 2.008E-01 O.OOOE+OO O.OOOE+OO l.023E-01 1.113E+OO 9.876E-02 2.618E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.190E-02 O.OOOE+OO 4.127E-02 O.OOOE+OO O.OOOE+OO 9. 965E-02 O.OOOE+OO O.OOOE+OO 2. 201E+Ol O.OOOE+OO 2.950E-01 4. 651E-02 4.056E+OO 3.854E-02 O.OOOE+OO 7.304E+02 O.OOOE+OO 2.217E-02 9.107E-02 l.755E--:01 6.074E-02 9.292E-02 1.563E+OO 4.993E-02 2.415E+Ol 2.031E-01 5. 724E-02 2.084E-02 SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT I DENT.
NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN r HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3133 of 5809 3. 718E:t-00 7.934E-01 3.338E+OO 2.618E+Ol 9.347E+Ol 3.293E-01 5.145E-02 5.068E+OO 4.194E-01 6.713E-01 5.287E-01 3.068E-01 5.083E-01 1. ,825E-01 1.825E-01 4.128E-01 5.083E-01 4.783E-02 2.048E-01 3.496E+OO 4.783E-02 O.OOOE+OO 2.340E-01 2.932E+02 1.454E-01 8. 965E-02 5.623E-02 2.899E-02 3.647E-02 1.094E-01 NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:11:16.35 *******************************************************************************

CEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l *
Acquisition date 3-0CT-2016 08:07:11 Sensitivity : 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit 75.000 *
Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
Sample date 9-DEC-2015 10:13:00 Nuclide Library : SOLID *
Sample ID G405235011 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity l.4650E+02 GRAM *
Quantity Err(%) 1.3652E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 10:....JUN-2016 07: 00: 49 E"ff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. rdentif ied Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 44 7E+Ol 1. 781E+OO CD-109 1.888E+OO 2.654E+OO SN-126 1.205E-01 l.693E-01 CS-135 2.570E-01 2.257E-01 BA-137M 2.416E-01 7.954E-02 CS-137 2.553E-01 8. 403E-02. HG-203 2.813E+00 6.383E+OO TL-208 3.090E-01 9.513E-02 PB-212 9.622E-01 1.392E-01 BI-214 1.129E+OO l.942E-01 PB-214 1.187E+OO 1.992E-01 RN-222 1.129E+OO l.942E-01 RA-224 6.267E-01 1.342E+OO RA-226 1.129E+OO l.942E-01 AC-228 l.133E+00 3.168E-01 RA-228 1.133E+OO 3.168E-01 TH-228 9.622E-01 1.392E-01 TH-230 1.129E+OO 1.941E-01 PA-231 4.125E-Ol 7 .181E-01 TH-232 l.133E+00 3.168E-01 TH-234 4. 719E-01 2.602E+OO U-234 1.129E+OO 1. 941E-01 U-235 6.013E-02 2.029E-01 U-238 4. 719E-01 2.602E+OO AM-243 3.555E-01 1.987E-01 ANH-511 4.207E-02 7.643E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3134 of 5809 -Key-Line Activity (pCi/GRAM -5.945E-01 -4.517E-02 -1.000E+41 -5.270E-03 K.L Act error (1. 96-sigma) 1.274E+Ol 3.952E-02 1.404E+41 2. 491E-02 TPU (1. 96-sigma) 1. 781E+OO 2.654E+OO l.693E-01 2.257E-01 7.954E-02 8.403E-02 6;383E+OO 9.513E-02 1.392E-01 1.942E-01 l.992E-01 l.942E-01 l.342E+OO l.942E-01 3.168E-01 3.168E-01 1.392E-01 l.941E-01 7 .181E-01 3.168E-01 2.602E+OO 1. 941E-01 2.029E-01 2.602E+OO l.987E-01 7.643E-02 TPU ( 1. 96-sigma) l.274E+Ol 4.446E-02 O.OOOE+OO 2.502E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -6. 396E-02 3.083E-01 3. 096E-01 FAIL ABUN V-48 8.494E+03 l.508E+04 l.556E+04 SHORT HLIF CR-51 -7.144E+01 4.031E+02 4.044E+02 SHORT HLIF MN-54. 3.719E-03 6.319E-02 6.321E-02 NOT IDENT. C0-56 l.604E-02 4.266E-01 4.267E'-01 FAIL ABUN MN-56 l.OOOE+41 2.977E+42 0.000E+OO SHORT HLIF C0-57 l.222E-02 4. 696E-02 4.729E-02 NOT IDENT. C0-58 -2.268E-01 4.726E-01 4.835E-01 NOT IDENT. FE-59 -1.039E+OO 5.647E+OO 5.666E+OO NOT IDENT. C0-60 -6.480E-03 3.547E-02 3.559E-02 NOT IDENT. ZN-65 7.180E-02 1.756E-01 l.785E-01 NOT IDENT. GE-68 l.522E+OO 2.298E+OO 2.398E+OO NOT IDENT. AS-73 4.634E+00 1.073E+Ol l.093E+Ol NOT IDENT. AS-74 7.799E+02 6.303E+03 6.313E+03 SHORT HLIF SE-75 6.535E-02 1.892E-01 l.914E-01 FAIL ABUN BR-77 1. 325E+38 1.143E+39 O.OOOE+OO SHORT HLIF SR-82 6.801E+Ol 8.736E+02 8. 7 41E+02 SHORT HLIF RB-83 2.006E-01 5.360E-01 5.435E-01 NOT IDENT. KR-85 l.450E+OO 7.082E+OO 7 .112E+OO NOT IDENT. SR-85 1. 517E-01 7.411E-01 7.442E-01 NOT IDENT. RB-86 9.534E+03 2.607E+04 2.642E+04 SHORT HLIF Y-88 -8.954E-02 2.716E-01 2.745E-01 NOT IDENT. Y-91 -7.957E+Ol 5.157E+02 5.169E+02 NOT IDENT. NB-94 -3.468E-03 2.946E-02 2.951E-02 NOT IDENT. NB-95 -2.194E-01 1.070E+OO 1. 074E+OO NOT IDENT. NB-95M -7.068E-01 2.544E+OO 2.564E+OO NOT IDENT. ZR-95 7.376E-01 l.301E+OO l.343E+OO NOT IDENT. NB-97 1.000E+41 2.701E+41 0 .'OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.345E+41 O.OOOE+OO SHORT HLIF M0-99 3.932E+30 1.292E+32 0.000E+OO SHORT HLIF TC-99M -1. OOOE+41 1. 796E+41 O.OOOE+OO SHORT HLIF RH-101 -3.358E-02 3.615E-02 3.919E-02 NOT IDENT. RH-102 -1.877E-04 6.083E-02 6.083E-02 NOT IDENT. RU-103 -2.149E+OO 5.259E+OO 5.348E+OO FAIL ABUN RH-106 -l.854E-01 4.054E-01 4.139E-01 NOT IDENT. RU-106 -l.854E-01 4.054E-01 4.139E-01 NOT IDENT. AG-108M 6.948E-03 2.791E-02 2.809E-02 NOT IDENT. AG-llOM 4. 396E-03 8.931E-02 . 8.933E-02 NOT IDENT. SN-113 -l.097E-01 2.372E-01 2.423E-01 NOT IDENT. CD-115 1.272E+38 2.202E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -3.348E+04 9.125E+04 9.249E+04 SHORT HLIF TE-123M -l.092E-01 1.298E-01 1. 38 8E-01 NOT IDENT. SB-124 -9.972E-03 1.333E+OO l.333E+OO NOT IDENT. SB-125 -8.818E-03 l.124E-01 l.125E-01 FAIL ABUN TE-125M 2.608E+02 2.765E+02 3.005E+02 NOT IDENT. I-126 9.615E+05 1.045E+06 l .131E+06 SHORT HLIF SB-126 5.093E+05 1.112E+06 1. U5E+06 SHORT HLIF SB-127 -l.559E+22 2.787E+22 O.OOOE+OO SHORT HLIF I-131 -3. 096E+09 4.371E+09 4.589E+09 SHORT HLIF. I-132 1.000E+41 2.179E+43 O.OOOE+OO SHORT HLIF TE-132 6.791E+25 3 .112E+26 O.OOOE+OO SHORT HLIF BA-133 -1. 680E-02 4.205E-02 4.273E-02 NOT IDENT. I-133 -l.000E+41 4.789E+41 O.OOOE+OO SHORT HLIF CS-'134 5 *. 235E-03 4.819E-02 4.825E-02 NOT IDENT. I-135 -1.000E+41 7.403E+41 O.OOOE+OO SHORT HLIF CS-136 1.611E+05 2.928E+05 3.017E+05 SHORT HLIF CE-139 2.759E-02 l.228E-01 l.235E-01 NOT IDENT. BA-140 8.039E+05 1.266E+06 l.317E+06 SHORT HLIF LA-140 -3.472E+04 2.156E+05 2.162E+05 SHORT HLIF CE-141 -2. 715E+OO 2.561E+Ol 2.564E+Ol NOT IDENT. CE-143 1. OOOE+41 l.126E+41 0.000E+OO SHORT HLIF CE-144 -l.632E-01 3.536E-01 3.612E-01 NOT IDENT. PM-144 9.472E-04 5.455E-02 5.455E-02 NOT IDENT. PR-144 1. 446E-01 4.746E+OO 4.746E+OO NOT IDENT. PM-146 -3.349E-02 4.777E-02 5.0lOE-02 NOT IDENT. ND-147 -l.297E+07 2.827E+07 2.887E+07 SHORT HLIF PM-147 3.068E+02 8.047E+02 8.165E+02 NOT .IDENT. PM-149 -9. 900E+3.9 3.373E+40 O.OOOE+OO SHORT HLIF 'EU-150 l.228E-02 2.552E-02 2. 611E-02 FAIL ABUN EU-152 2.065E-02 9.906E-02 9.950E-02 NOT IDENT. GD-153 -3.455E-02 2.178E-01 2.184E-01 NOT IDENT. EU-154 -l.059E-01 9.814E-02 l.091E-01 NOT IDENT. EU-155 -3.636E-02 1.082E-01 1.095E-01 FAIL ABUN TB-160 2.603E+OO 3.093E+OO 3.308E+OO FAIL ABUN H0-166M 2.822E-02 5.40*9E-02 5.556E-02 FAIL ABUN TM-171 -7.373E+OO 2.695E+Ol 2.715E+Ol NOT IDENT. HF-172 7.132E-03 2.314E-01 . 2. 315E-01 FAIL ABUN LU-172 8. 715E-03 6.365E-02 6.378E-02 FAIL ABUN Page 3135 of 5809 LU-176 4 .116E-03 2.251E-02 2.258E-02 FAIL ABUN HF-181 1.807E+00 3.986E+OO 4.069E+OO NOT IDENT. TA-182 -3.295E-01 9.706E-01 9.819E-01 FAIL ABUN RE-183 1.712E+00 3.512E+OO 3. 596E+OO FAIL ABUN RE-184 1.509E+Ol 2.875E+Ol 2.954E+Ol FAIL ABUN W-188 -8.038E-01 l.136E+02 1.136E+02 *FAIL ABUN IR-192 -1. 8 62E-01 3.851E-01 3.941E-01 FAIL ABUN BI-207 4. 969E-02 5.135E-02 5.602E-02 FAIL ABUN PB-210 3.479E+OO 5.176E+OO 5.408E+OO NOT IDENT. BI-'-211 3.270E+OO 5.514E-01 1 .. 574E+OO FAIL ABUN PB-211 1.262E+OO 1.018E+OO l.166E+OO FAIL ABUN BI-212 9.324E-01 7.631E-01 8.712E-01 FAIL ABUN RN-219 1.905E-02 3.800E-01 3.801E-01 FAIL ABUN RA-223 -2.012E-01 6.097E-01 6.164E-01 FAIL ABUN AC-227 -l.880E-02 2.417E-01 2.419E-01 FAIL ABUN TH-227 -l.880E-02 2.417E-01 2.419E-01 FAIL ABUN TH-229 1. 531E-01 4.707E-01 4.757E-01 FAIL ABUN TH-231 -2.012E-01 6.097E-01 6.164E-01 FAIL ABUN PA-233 1.608E-02 5.092E-02 5.143E-02 FAIL ABUN PA-234 -1.947E-02 2.535E-01 2.537E-01 FAIL ABUN PA-234M -2.344E+OO 4.566E+00 4.686E+OO NOT IDENT. NP-237 1.608E-02 5.092E-02 5.143E-02 FAIL ABUN NP-238 -l.OOOE+41 2.592E+41 O.OOOE+OO SHORT HLIF NP-239 1.453E-01 2.543E-01 2.626E-01 NOT IDENT. PU-239 5.633E+Ol 3.310E+02 3.320E+02 NOT IDENT. AM-241 -1. OOlE-01 1. 675E-01 1.735E-01 NOT IDENT. CM-243 6.895E-02 9.527E-02 l.002E-01 NOT IDENT. BK-24 7 , -2.901E-02 7.869E-02 7. 977E-02 NOT IDENT. CM-247 5.343E-03 3.534E-02 3.542E-02 NOT IDENT. CF-249 2.814E-02 3.792E-02 3.999E-02 FAIL ABUN CF-251 1.066E-01 1.187E-01 1. 281E-01 NOT IDENT. Page 3136 of5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.1871 87.09 100.1593 136.47 54.8256 45.60 63. 9396 87.57 .100. 2393 140.51 0.0000 46.54 45.2391 88.03 100.3156 143.76 73.0133 49.72 0.0000 88.34 100.3668 144.24 78.5901 51. 35 54.3427 88.47 100.3881 145.44 80.9187 51. 87 59.1808 89. 96 100.6333 152.43 63.7006 52.39 55.4288 1093.63 100.7440 153.25 0.0000 52.97 47.8468 91.11 0.0000 323.87 82.8672 53.44 46.9400 92. 59 101.0610 156.02 0.0000 54.07 47.9658 93.35 101.1829 158.56 0.0000 57.36 0.0000 94.56 101.3773 159.00 70.9317 57.53 58. 9665 94.65 101. 3915 162.33 61. 7769 57.98 56.1207 94.67 101.3945 162.66 0.0000 59.27 77.6215 94.87 89.6970 163.33 78.0598 59.32 77.6297 97.43 88.6699 165.86 63.5281 59.54 77.6657 98.43 79.0934 176.31 68.8257. 60.96 70.1079 98.44 79.0946 176.60 0.0000 61.17 70.1386 99.53 77.1419 177.52 53.9809 62. 93 77.2373 100 .11 64.6891 181.07 0.0000 63.29 77.2941 102.03 73.2481 181.52 49.2057 63.58 77.3397 103.18 64.9881 184.41 75.5676 64.28 94 .1155 103.37 53.4731 143.76 56.7505 66.73 78.8135 105.21 68.3380 193.51 56.0229 67.24 89.7399 105.31 71.5024 197.03 64.4120 125.81 89.8170 106.12 65.2707 198.01 48.0619 67.75 93.7780 106.47 62.1442 201.83 57.6492 69.67 80.2560 109.28 53.9365 203.43 65.9847 70.83 84.7363 111. 00 86.9342 205.31 51. 9371 72.81 93.0257 111.76 0.0000 210.85 64.8599 72.87 93.0364 114. 06 77.7262 215.65 57.2007 74.66 84.0096 116. 30 0.0000 222 .11 59.9297 74.82 84.0346 116.74 66.2596 227.09 49.3582 74.97 84.0577 119.76 70.8244 227.38 55.3915 77 .11 84.3845 121.12 60.2037 228.16 0.0000 78.74 84.6300 121.22 58.0614 228.18 44.5851 79.69 88.8090 121. 7 8 63.4847 116.74 44.5851 80.12 71. 3702 122.06 61.3557 235.69 56.5984 80.19 0.0000 122.92 64.6587 235. 96 56. 6115 80.57 70.0787 123.07 64. 6715 238.63 46.2023 81. 00 86.3151 265.00 72.2748 238.98 0.0000 81. 07 86.3255 125.81 68.1507 240.99 46.2939 81. 75 95.8808 127.23 87.7839 242.00 46.3334 83.79 77.2449 127.91 71. 5906 244.70 47.2519 84.00 77. 2722 129.30 78.2380 252.40 0.0000 85.43 99.8819 131. 2 0 87.1436 252.80 38.1355 86.55 100.0696 133. 02 73.1504 254.15 0.0000 86.79 100.1092 133. 52 71. 0114 256.23 41.1194 86.94 100.1346 136.00 48.2183 260.90 0.0000 Page 3137of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31.0463 355.39 0.0000 584.27 22.8821 264.80 43.0562 356.01 34.4305 595.83 0.0000 265.00 43.0625 364.49 0.0000 427.87 26.0518 268.22 39.8496 366.42 0.0000 602.52 0.0000 269.46 39.8887 372. 51 38.3546 604. 72 19.5730 270.03 39.9063 375.05 30.3739 607.14 17.0816 271.23 39.9434 377.52 33.1037 609.32 17.0975 273.65 0.0000 356.01 24.2496 610.33 17.1045 276.40 38.8484 388.16 27.9140 614.28 24.1885 277.37 45.1472 388.63 0.0000 618.01 20.1888 2.77. 60 45.1549 391.69 38.8008 620.36 7.0729 278.00 45.1692 264.66 19.0492 621*. 93 15.1666 279.20 45.2098 401.81 25.8693 630.19 0.0000 279.54 45.2219 402.40 25.8786 631.29 20.3011 279.70 45.2274 404.85 25.9l51 633.25 24.3809 280.46 45.2527 410.95 24.6374 634.78 0.0000 283.69 45.3625 413.71 24.6758 635.95 21.3572 284.31 0.0000 414.70 0.0000 636.99 .0.0000 285.41 45.4208 423. 72 0.0000 645.85 15.3168 285.90 0.0000 427.09 31. 3078 657.76 12.3125 287.50 49.7032 427.87 35.0065 657.90 0.0000 290.67 40.5313 433.94 26.8052 661. 66 25.6917 293.27 0.0000 439.40 20.3954 664.57 0.0000 351.93 33.0411 .453.88 38.3065 666.33 0.0000' 295. 96 33.0586 463.37 21.5967 666.50 0.0000 879.38 30.5735 468.07 33.8862 667.71 0.0000 299.98 34.4298 473.00 0.0000 677.62 14.4785 300.09 34.4331 475.06 32 .1192 685.70 0.0000 300.13 34.4339 476.78 21. 7469 695.00 0.0000 301.36 . 29.3586 477.60 28.3777 696.49 18.7522 302.85 38.3340 482.18 18. 9624 696. 51 18.7522 256.23 40.9375 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.7581 306.78 35.0242 497.08 23.8810 697.49 19. 8017 308.46 31.6448 505.52 17.2661 702.65 17.7519 311. 90 28.2916 507.63 0.0000 706.68 20.9172 316.51 32.6825 511.00 27.8920 711. 68 13.6215 319.41 0.0000 514.00 21. 6714 720.70 0.0000 320.08 0.0000 .514.00 21. 6714 721.93 0.0000 321. 04 37.0983 520.40 13.5260 722.78 17.3614 323.87 43.5668 520.69 0.0000 722. 91 23.6755 325.23 41.5303 522.65 0.0000 723. 31 23.6792 328.76 0.0000 527.90 0.0000 724.19 17.3708 333.37 33.0583 528.26 16.4867 727. 33 15.8099 333.97 30.0254 529.59 19.4084 733.00 12.6743 334.37 36.5620 529.87 0.0000 735.93 15.8600 338.28 39.2752 531.02 0.0000 333.97 16.9271 338.32 39.2761 537.26 0.0000 739.50 0.0000 311. 90 51.1316 546.56 0.0000 747.24 11.6790 340'.48 51.1316 552.55 12.7509 748.06 13.8067 340.55 0.0000 563.25 17.7407 752.31 11. 7005 344.28 41.1824 569.33 22.7314 753.82 0.0000 345.93 29.4725 946.00 22.7333 756.73 10.6539 351.06 16.7209 569.70 20.7582 756.80 10.6543 351. 93 16.7301 583.19 22. 8718 884.68 30.7629 Page 3138 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:11:59.40 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : 2-0CT-2016 11:02:08. Sample date 10-DEC-2015 11:25:00 Acquisition date : 3-0CT-2016 08:07:40. Sample ID G405235012 Sample quantity : 1.54640E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed iive time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.35 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 0 0 8 8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3140of5809 Energy 63.37* 74.74* 77.05* 87.48 93.40* 129.39 186.31* 238.68* 2 41. 61 258.46 277.51 291.35 295.32* 328.80* 338.53 352.01* 450.55 463.41 511.75* 533.47 537.32 545.07 554.96 563.51 583.39* 609.42* 623.55* 633 .11 643.35 661.56 679.66 726.74 772. 05 816.20 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 17 107 181 62 67 47 86 371 107 52 34 11 101 7 51 158 9 35 54 17 11 18 7 10 81 107 11 10 6 79 11 23 21 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 99 127 142 167 162 86 125 31 37 41 38 42 52 37 35 34 22 17 46 9 11 23 11 16 25 17 9 39 11 12 7 13 19 4 0.73 0.99 1.15 1. 42 1. 53 1.16 1.19 1. 20 2.19 2.58 0.73 2.01 0.82 0.65 1. 22 1.12 0.49 1. 48 2.88 2.38 1. 20 3.44 0.72 0.57 1. 60 1. 02 3.28 5.34 0.91 1. 29 1. 08 4.32 4.63 2.17 12 6. 71 149.46 154.07 174.93 186. 78 258.76 372. 60 477.34 483.20 516.90 555.00 582.69 590.62 657.57 677.04 704.00 901. 07 926.78 1023.44 1066.89 1074.59 1090.08 1109.86 1126.95 1166.71 1218.76 1247.01 1266.13 1286.60 1323. 02 1359.22 1453.35 1543.94 1632.23 124 146 146 170 182 255 367 474 474 511 552 577 588 653 673 699 897 921 1014 1062 1072 1081 1108 1119 1162 1214 1242 1256 1282 1317 1354 1446 1533 1628 6 4.70E-03 98.4 19 2.98E-02 19.0 19 5.02E-02 13.5 8 1. 72E-02 38. 4 10 1.85E-02 39.4 8 1. 31E-02 37. 3 13 2.39E-02 29.8 15* 1 . 0 3 E -0 1 5 . 8 15 2.98E-02 19.2 11 1.44E-02 27.8 8 9.35E-03 36.2 8 3.lOE-03105.0 8 2.81E-02 16.1 6 1. 82E-03155. 6 9 1.41E-02 25.5 9 4.40E-02 10.5 8 2.40E-03100.2 11 9.58E-03 28.5 24 1. 51E-02 40. 6 10 4.67E-03 42.5 8 2. 94E-03 61. 3 16 5.00E-03 65.0 6 1.96E-03 85.0 10 2.69E-03 89.9 10 2.25E-02 16.4 11 2.97E-02 12.6 9 3.05E-03 59.1 14 2.90E-03130.0 6 1.54E-03107.0 12 2.20E-02 14.3 10 3.00E-03 56.1 13 6.47E-03 38.0 20 5.83E-03 56.3 8 3.17E-03 42.1 Fit 7.00E-01 l.99E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 905.10* 5 7 1. 39 1809.98 1804 9 1. 28E-03116 .1 36 0 911.73* 53 3 1. 67 1823.23 1817 14 1.46E-02 16.3 37 0 934.67 14 10 0.67 1869.10 1861 14 3.78E-03 57.2 38 0 951. 55 10 1 0.91 1902.84 1900 6 2.69E-03 37.6 39 0 970.47 9 24 0.68 1940.67 1933 12 2.50E-03113.9 40 0 1000.30* 16 4 3.42 2000.31 1993 15 4.55E-03 37.1 41 0 1120.98* 22 6 2.21 2241. 57 2235 11 5.99E-03 31. 0 42 0 1202.26 7 12 1. 35 2404.06 2397 10 l.89E-03104.0 43 0 1208.67 13 9 1. 04 2416.88 2409 12 3.59E-03 54.1 44 0 1377. 98* 10 2 0.64 2755.32 2752 7 2.81E-03 38.3 45 0 1461.19* 205 3 1. 98 2921.64 2916 12 5.68E-02 7.3 46 0 1588. 72 11 0 1. 50 3176.55 3171 10 3.06E-03 30.2 Flag: "*" Peak area was modified by background subtraction . Page 3141 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:12:01 PKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration AnalysE!S by Sample title Sample date Sample ID 10-DEC-2015 11:25:00 G405235012 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:07:40 154.64 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87. 09* PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3142of5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-l26 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.35 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity *Report Page : 2 Sample ID : G405235012 Acquisition date 3-0(::T-2016 08:07:40 Nucl":ide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 6.545E-01 L.377E+Ol 1.377E+Ol 14.53 OK CD-109 88.03 3.70* 4.307E+OO 1.439E+OO 2.252E+OO 131.26 OK SN-126 64.28 9.60 2.480E+OO 4. 564E-01 . 4.564E-01 196.78 OK 86.94 8.90 4.307E+OO 5.984E-01 5.984E-01 131.26 OK 87.57 37.00* 4.307E+OO l.439E-01 1.439E-01 131.26 OK BA-137M 661. 66 89.90* l.335E+OO 3.381E-01 3.445E-01 28.51 OK CS-137 661. 66 85.10* 1.335E+OO 3.572E-01 3.639E-01 28.51 OK TL-208 277.37 6.60 3.040E+OO 9.409E-01 9.409E-01 72.30 OK 583.19 85.00* l.496E+OO 3. 313E-01 3.313E-01 32.72 OK 860.56 12.50 1.058E+OO Line Not Found Absent PB-212 74.82 10.28 3.476E+OO 1.297E+OO 1. 2 97E+OO 57.70 OK 77 .11 17.10 3.651E+OO 1;828E+OO 1.828E+OO 27.04 OK 238.63 43.60* 3.499E+OO 1.385E+OO l.385E+00 11. 62 OK 300.09 3.30 2.819E+OO Line Not Found Absent BI-214 609.32 45.49* 1.437E+OO 8.468E-01 8. 471E-01 25.22 OK 1120. 29 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 OK . 1764.49 15.30 5.419E-01 Line Not Found Absent PB-214 74.82 5.80 3.482E+OO Line Not Found Reject 77 .11 9.70 . 3. 651E+OO 3.222E+OO 3.224E+OO 27.04 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found <<INT Reject 295.22 18.42 2.863E+OO 1.068E+OO 1.069E+OO 32.17 OK 351.93 35.60* 2.414E+OO l.OlOE+OO 1.0lOE+OO 21. 06 OK RN-222 609.32 45.49* 1.437E+OO 8.468E-01 8.471E-01 25.22 OK 1120.29 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent RA-224 240.99 4.10* 3.460E+OO 2.410E+OO 2.410E+OO 73.01 OK RA-226 609.32 45.49* 1.437E+OO 8.468E-01 8. 471E-01 25.22 OK 1120.29 14.92 8 .*367E-01 8.359E-01 8.362E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent AC-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 9.861E-01 9.861E-01 51. 02 OK 794.95 4.25 1.134E+OO Line Not Found Absent 835.71 1. 61 1.085E+OO -----Line Not Found Absent 911. 20 25.80* 1.005E+OO 1.007E+OO 1.. 007E+OO 32.55 OK 968. 97 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 9.861E-01 9. 861E-01 51. 02 OK 794.95 4.25 l.134E+OO Line Not Found Absent 835.71 1. 61 1.085E+OO Line Not Found. Absent 911. 20 25.80* l.005E+OO 1. 00.7E+OO 1.007E+OO 32.55 OK 968.97 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 OK TH-228 74.82 10.28 3.476E+OO 1. 297E+OO 1.297E+OO 57.70 OK 77 .11 17.10 3.651E+OO l.828E+OO 1.828E+OO 27.04 OK 238.63 43.60* 3.499E+OO 1.385E+OO 1.385E+OO 11. 62 OK 300.09 3.30 2.819E+OO Line Not Found Absent TH-230 609.32 45.49* 1.437E+OO 8.468E-Oi 8.469E,-01 25.22 OK 1120.29 14.92 8.367E-01 8.359E-01 8.359E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent Page 3143 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-232 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 9.861E-01 9.861E-01 51. 02 OK 835. 71 1. 61 l.085E+OO Line Not Found Absent 911. 20 25.80* 1.005E+OO 1.007E+OO 1.007E+OO 32.55 OK 968.97 15.80 9.513E-01 2.947E-01 2.947E-01 227. 71 OK TH-234 63.29 3.70* 2.480E+OO 1.184E+OO l.184E+OO 196. 78 OK 92.59 4.23 4.581E+OO 2.132E+OO 2 .132E+OO 78.87 OK U-234 609.32 45.49* l.437E+OO 8.468E-01 8.469E-01 25.22 OK* 1120.29 14.92 8.367E-01 8.359E-01 8.359E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent U-238 63.29 3.70* 2.480E+OO 1.184E+OO l.184E+OO 196.78 OK 92.59 4.23 4.581E+OO 2.132E+OO 2.132E+OO 78.87 OK AM-243 43.53 5.90 5.957E-01 Line Not Found Absent 74.66 67.20* 3.476E+OO 1.984E-01 l.984E-01 57.70 OK ANH-511 511. 00 100.00* l.688E+OO 1.698E-01 1.698E-01 81.23 OK Flag: "*" = Keyline Page 3144of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:02.63 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l *
Acquisition date 3-0CT-2016 08:07:40 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.35 Half life ratio : ***** * *
Sample date 10-DEC-2015 11:25:00 Analyst initials: MXRl * *Sample.ID G405235012 Sample Quantity 1.5464E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 l.377E+Ol 1. 961E+OO 9.078E-01 CD-109 2.252E+OO 2.897E+OO 2. 471E+OO SN-126 1. 439E-01 l.852E-01 l.636E-01 BA-137M 3.445E-01 9.625E-02 9.705E-02 CS-137 3.639E-01 1.017E-01 l.025E-01 TL-208 3.313E-01 1.063E-01 8.861E-02 PB-212 1.385E+OO 1.577E-01 8.974E-02 BI-214 8.471E-01 2.094E-01 1.368E-01 PB-214 l.OlOE+OO 2.084E-01 1.489E-01 RN-222 8. 471E-01 2.094E-01 l.368E-01 RA-224 2.410E+00 1.725E+OO 9.638E-01 RA-22 6 8.471E-01 2.094E-01 1.368E-01 AC-228 1.007E+OO 3.212E-01 2.979E-01 RA-228 1.007E+OO 3.212E-01 2.979E-01 TH-228 1.385E+OO 1.577E-01 8.974E-02 TH-230 8.469E-01 2.093E-01 1. 367E-01 TH-232 1.007E+OO 3.212E-01 2.979E-01 TH-234 1.184E+OO 2.284E+OO 2.343E+00 U-234 8.469E-01 2.093E-01 1.367E-01 U-238 l.184E+OO 2.284E+OO 2.343E+OO AM-243 1.984E-01 l.122E-01 9.921E-02 ANH-511 1.698E-01 l.351E-01 5. 931E-02 . ----Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -l.388E+Ol l.167E+Ol 1.922E+Ol NOT IDENT. NA-22 -4.322E-02 6.347E-02 1.137E-01 NOT IDENT. NA-24 O.OOOE+OO l.309E+41 O.OOOE+OO SHORT HLIF AL-26 -1.009E-02 3.228E-02 6.799E-02 NOT IDENT. SC-46 -2.551E-01 4.008E-01 6.887E-01 FAIL ABUN V-48 O.OOOE+OO 1. 782E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.461E+02 O.OOOE+OO SHORT HLIF MN-54 5.323E-02 7.878E-02 l.761E-01 NOT IDENT. Page 3145 of5809 C0-56 -l.022E-01 5.833E-01 1.126E+OO NOT IDENT. MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 1.567E-02 4.796E-02 9.727E-02 NOT IDENT. C0-58 -5.616E-03 5.973E-01 1.186E+OO NOT IDENT. FE-59 -2.197E+OO 8.186E+OO 1.643E+Ol NOT IDENT. C0-60 -7.445E-03 4.669E-02 9.734E-02 NOT IDENT. ZN-65 6.894E-02 2. 49.8E-01 4.909E-01 NOT IDENT. GE-68 -2.026E+OO 3.020E+OO 4. 966E+OO NOT IDENT. AS-73 8.629E+OO 7.399E+OO 1.691E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.435E+03 O.OOOE+OO SHORT HLIF SE-75 1.056E-01 2.387E-01 4.740E-01 NOT IDENT. BR-77 O.OOOE+OO 1.599E+37 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 7.092E+02 O.OOOE+OO SHORT HLIF RB-83 8.669E-02 8.817E-01 1.657E+OO NOT IDENT. KR-85 8.653E+OO 8.540E+OO l.925E+Ol NOT IDENT. SR-85 8.904E-01 8. 831E-01 1.990E+OO NOT IDENT. RB-86 0.000E+OO 3.260E+04 O.OOOE+OO SHORT HLIF Y-88 -7.223E-02 2.296E-01 4.815E-01 NOT IDENT. Y-91 -3.935E+02 l.253E+03 1.410E+03 NOT IDENT. NB-94 l.658E-02 3.730E-02 8.045E-02 NOT IDENT. NB-95 8. 572E-02 l.014E+00 l.876E+00 NOT IDENT. NB-95M -1.658E-01 2.526E+OO 4.394E+OO NOT IDENT. ZR-95 3.502E-01 1.303E+OO 2. 921E+OO NOT IDENT. NB-97 O.OOOE+OO 1.282E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.705E+41 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO .1.134E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 2.476E-02 3.333E-02 6.615E-02 NOT IDENT. RH-102 -1.754E-03 8.764E-02 l.725E-01 NOT IDENT. RU-103 3.893E+OO 6. 051E+OO 1.359E+Ol FAIL ABUN RH-106 -2.134E-01 6.580E-01 1. 12 9E+OO NOT IDENT. RU-106 -2.134E-01 6.580E-01 1.12 9E+OO NOT IDENT. AG-108M -1.346E-02 3.256E-02 6.309E-02 NOT IDENT. AG-llOM -l.380E-02 l.418E-01 2.742E-01 NOT IDENT. SN-113 -5.246E-02 2.639E-01 5.281E-01 NOT IDENT. CD-115 O.OOOE+OO 2.097E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 0.000E+OO 9.397E+04 O.OOOE+OO SHORT HLIF TE-123M -2.052E-02 1.345E-01 2.575E-01 NOT IDENT. SB-124 1.113E+OO 1.542E+OO 5.188E+OO NOT IDENT. SB-125 l.032E-02 1.210E:...01 2.500E-01 FAIL ABUN TE-125M 1. 784E+02 2.554E+02 5.388E+02 NOT IDENT. I-126 O.OOOE+OO 9.810E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.519E+o6 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 1. 962E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.892E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.348E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.982E+26 0.000E+OO SHORT HLIF BA-133 1.368E-02 4.688E-02 9.169E-02 FAIL ABUN I-133 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 l.758E-02 7.139E-02 1. 451E-01 FAIL ABUN CS-135 -1.049E-01 l.661E-01 2.880E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.804E+05 O.OOOE+OO SHORT HLIF CE-139 -3.431E-02 1.090E-01 2.052E-01 NOT IDENT. BA-140 O.OOOE+OO l.828E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.106E+05 O.OOOE+OO SHORT HLIF CE-141 -1.837E+Ol 2.366E+Ol 4.177E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF
CE-144 2.411E-01 3.828E-01 7.848E-01 NOT IDENT. PM-144 -l.160E-02 6.810E-02 1.324E-01 NOT IDENT. PR-144 -1.054E+OO* 5.901E+OO 1.146E+Ol NOT IDENT. PM-146 3.331E-02 5.304E-02 l.090E-01 FAIL ABUN ND-147 O.OOOE+OO 3.694E+07 0.000E+OO SHORT HLIF PM-147 -l.006E+00 8 .159E+o2 1.615E+03 NOT IDENT. PM-149 O.OOOE+OO 2.955E+40 O.OOOE+OO SHORT.HLIF EU-150 2.220E-02 3.178E-02 6.42QE-02 FAIL ABUN EU-152 -5.809E-02 1.118E-01 l.922E-01 NOT IDENT. GD-153 3.292E-02 1.939E-01 3.679E-01 NOT IDENT. EU-154 -1.lOOE-01 1.548E-01 2.750E-01 NOT IDENT. EU-155 -7.153E-03 1.lOlE-01 2.180E-01 FAIL ABUN TB-160 4.382E-01 2.210E+OO 4.647E+OO FAIL ABUN H0-166M -S.789E-03 6.146E-02 1.223E-01 NOT IDENT. TM-171 -3.869E+OO 1. 748E+Ol 3.616E+Ol NOT IDENT. HF-172 2.282E-02 2.297E-01 4. 271E-01 FAIL ABUN LU-172 3.835E-03 9.394E-02 1. 893E-01 FAIL ABUN LU-176 -l.853E-03 2. 811E-02 5.236E-02 FAIL ABUN HF-181 l.758E-03 5.398E+OO 1. 091E+Ol NOT IDENT. TA-182 -7.022E-01 1.215E+OO 2.238E+OO FAIL ABUN Page 3146of5809 RE-183 9. 966E-01 2. 722E+OO 5.807E+OO NOT IDENT. RE-184 -2.399E-01 4.279E+Ol 7.563E+Ol NOT IDENT. W-188 l.029E+02 2. ll 7E+02 2. 611E+02 FAIL ABUN IR-192 1. 705E-01 5.551E-01 1. 07 9E+OO FAIL ABUN HG-203 2.766E-01 2.749E+OO 4.866E+OO
NOT IDENT. BI-207 5.891E-02 7. 431E-02 1.631E-01 FAIL ABUN PB-210 -1. 426E+OO 2.486E+OO 5.002E+OO NOT IDENT. BI-211 O.OOOE+OO 5.741E-01 9.598E-Ol FAIL ABUN PB-211 -3.359E-01 8.036E-01 l.563E+OO NOT IDENT. BI-212 l.444E+OO l.076E+OO l.556E+OO . FAIL ABUN RN-219 -9.572E-03 4.406E-01 8.983E-01 NOT IDENT. RA-223 -l.789E-01 7.173E-01 l.292E+OO FAIL ABUN AC-227 -6.853E-03 2.432E-01 4.280E-Ol NOT IDENT. TH-227 -6.853E-03 2.432E-01 4.280E-01 NOT IDENT. TH-229 -1. 759E-01 5.134E-01 9.485E-01 FAIL ABUN PA-231 3.236E-01 5.254E-01 1.054E+OO NOT IDENT. TH-231 -1. 789E-01 7.173E-01 l.292E+OO FAIL ABUN PA-233 4.224E-02 6.304E-02 l.309E-01 NOT IDENT. PA-234 7.189E-02 4.086E-01 8.216E-01 FAIL ABUN PA-234M 1. 032E+Ol 7.498E+OO 1.271E+Ol FAIL ABUN U-235 3.330E-02 l.935E-01 3.735E-01 FAIL ABUN NP-237 4.224E-02 6.304E-02 l.309E-01 FAIL ABUN NP-238 o. oo*oE+oo 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -5. 313E-02 2.280E-01 4.446E-01 FAIL ABUN PU-239 O.OOOE+OO 6. 481E+02 7.164E+02 FAIL ABUN AM-241 1.825E-02 1.297E-01 2.712E-01 NOT IDENT. CM-243 5.526E-02 9.585E-02 2.007E-01 FAIL ABUN BK-247 7.357E-03 8.605E-02 1.636E-01 NOT IDENT. CM-247 l.727E-02 3. 941E-02 8.481E-02 FAIL ABUN CF-249 2.069E-02 4.089E-02 8.909E-02 NOT IDENT. CF-251 4.467E-02 l.232E-01 2.449E-01 NOT IDENT. Page 3147of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:12:00.24 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 198 10.66* 6.545E-01 1.377E.+Ol 1.377E+Ol 14.53 CD-109 88.03 80 3.70* 4.307E+OO 2.424E+OO 3.792E+OO 76.83 SN-126 64.28 22 9.60 2.480E+OO 4. 56'4E-01 4.564E-01 196.78 8 6. 94 80 8.90 4.307E+OO 1.008E+OO 1.008E+OO 76.83 87.57 80 37.00* 4.307E+OO 2.424E-01 2.424E-01 76.83 BA-137M 661. 66 84 89.90* 1.335E+OO 3.381E-01 3.445E-01 28.51 CS-137 661. 66 84 85.10* 1.335E+OO 3. 572E-01 3.639E-01 28.51 TL-208 277.37 39 6.60 3.040E+OO 9.409E-01 9.409E-01 72.30 583.19 87 85.00* 1.496E+OO 3.313E-01 3.313E-01 32. 72 860.56 ------12.50 1.058E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.327E+OO ------Line Not Found ------351.06 179 12 .. 92* 2.414E+OO 2.782E+OO 2.782E+OO 21. 06 PB-212 74.82 140 10.28 3.476E+OO 1.899E+OO 1. 899E+OO 38.04 77 .11 235 17.10 3.651E+OO 1.828E+OO 1.828E+OO 27.04 238.63 435 43.60* 3.499E+OO 1.385E+OO 1.385E+00 11. 62 300.09 ------3.30 ------Line Not Found ------BI-214 609.32 114 45.49* 1.437E+OO 8.468E-01 8.471E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.362E-01 62. 02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------PB-214 74.82 140 5.80 3.476E+OO 3.367E+OO 3.368E+OO 38.04 77 .11 235 9.70 3.651E+OO 3.222E+00 3.224E+OO 27.04 87.09 80 3.41 4.307E+OO 2.630E+00 2.631E+OO 76.83 242.00 126 7.25 3.460E+OO 2.432E+OO 2.432E+00 38.41 295.22 116 18.42 2.863E+OO 1.068E+OO 1.069E+OO 32:17 351.93 179 35.60* 2.414E+OO 1.0lOE+OO 1.0lOE+OO 21. 06 RN-222 609.32 114 45.49* l.437E+OO 8.468E-01 8.471E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------RA-224 240.99 126 4.10* 3.460E+OO 4.300E+OO 4.300E+OO 38.41 RA-226 609.32 114 45.49* l.437E+OO 8.468E-01 8.471E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 57 11. 27 2.507E+OO 9.861E-01 9. 8 61E-01 51. 02 794.95 ------4.25 1.134E+OO ------Line Not Found ------835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 54 25.80* 1.005E+OO 1.007E+OO 1.007E+OO 32.55 968. 97 9 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 57 11. 27 2.507E+OO 9. 861E-01 9.861E-01 51. 02 794.95 ------4.25 1.134E+OO ------Line Not Found ------835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 54 25.80* 1.005E+OO l.007E+OO 1.007E+00 32.55 968. 97 9 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 TH-228 74.82 140 10.28 3.476E+OO 1.899E+OO 1.899E+OO 38.04 77 .11 235 17 .10. 3.651E+OO 1.828E+OO l.828E+OO 27.04 238.63 435 43.60* 3.499E+OO 1.385E+OO 1.385E+OO 11. 62 Page 3i48of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Nuclide Type: Uncorrected Decay Corr *2-sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 ------3.30 2.819E+OO ------Line Not Found ------TH-230 609.32 114 45.49* 1.437E+OO 8.468E-01 8.469E-01 25.22 1120. 29 21 14.92 8.367E-Ol 8.359E-01 8.359E-01 62.02 1764.49 ------15.30 5.419E-Ol ------Line Not Found ------TH-232 105.21 ------1.10' 4.933E+OO ------Line Not Found ------338.32 57 11. 27 2.507E+OO 9.861E-01 9.861E-01 51. 02 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 54 25.80* 1.005E+OO 1.007E+OO l.007E+OO 32.55 968. 97 9 15.80 9.513E-01 2.947E-01 2.947E-Ol 227.71 TH-234 63.29 22 3.70* 2.480E+OO 1.184E+OO 1.184E+OO 196.78 92.59 85 4.23 4.581E+OO 2.132E+OO 2.132E+OO 78.87 U-234 609.32 114 45.49* 1.437E+OO 8.468E-01 8.469E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.359E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------U-238 63. 29 22 3.70* 2.480E+OO 1.184E+OO 1.184E+OO 196.78 92.59 85 4.23 4.581E+OO 2.132E+OO 2 .132E+OO 78.87 AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 140 67.20* 3.476E+OO 2.906E-01 2.906E-01 38.04 ANH-511 511.00 59 100.00* 1.688E+OO 1.698E-01 1. 6'98E-01 81. 23 Flag: "*" Key line Page 3149 of 5809 Page : 3 Surrunary of Nuclide Activity Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Total number of lines in spectrum 46 Number of unidentified lines 14 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA.,..226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlif e 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y *1.41E+10Y 1600. OOY 1600. OOY 1600.00Y 1.41E+l0Y 1600. OOY 1. 41E+l0Y l.41E+10Y 1.41E+10Y 7.54E+04Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Uncorrected Decay pCi/GRAM 1.00 1.377E+Ol 1.56
2.424E+OO 1.00 . 2.424E-01 1.02 3.381E-01 1. 02 3. 572E-01 1.00 3.313E-01 1. 00 2. 782E+OO 1.00 1.385E+OO 1.00 8.468E-01 1.00 1.0lOE+OO 1.00 8.468E-01 1.00 4.300E+OO 1.00 8.468E-01 1. 00 1. 007E+OO 1.00 1.007E+OO 1'.00 1.385E+OO 1.00 8.468E-01 1.00 1.007E+OO 1. 00 1.184E+OO 1.00 1. 00 1.184E+OO 1.00 2.90EiE-01
1.00 1.698E-01 Total Activity 3.841E+Ol Grand Total Activity 3.841E+Ol Decay Corr pCi/GRAM 1.377E+Ol 3.792E+OO 2.424E-01 3.445E-01 3.639E-01 3.313E-01 2.782E+OO 1.385E+OO 8.471E-01 1.0lOE+OO 8.471E-01 4.300E+OO 8.471E-01 1. 007E+OO 1.007E+OO 1.385E+Oci 8.469E-01 1.007E+OO 1.184E+OO 8.469E-01 1.184E+OO 2.906E-01 l.698E-01 3.979E+Ol 3.979E+Ol 69.57% Decay Corr 2-Sigma Error 0.200E+Ol 2.914E+OO 1.863E-01 0.982E-01 1.037E-01 1.084E-01 0.586E+OO 0.161E+OO 2.136E-01 0.213E+00 2 .136E-01 1. 651E+OO 2.136E-01 0.328E+OO 0.328E+00 0 .161E+OO 2.136E-01 0.328E+00 2.330E+OO 2.136E-01 2.330E+OO 1.105E-01 1. 379E-01 "M" Manually accepted 2-Sigma %Error 14.53 76.83 76.83 28.51 28.51 32.72 21. 06 11. 62 25.22 21. 06 25.22 38.41 25.22 32.55 32.55 11. 62 25.22 32.55 196.78 25.22 196.78 38.04 Sl. 23 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3150 of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235012 Acquisition date : 3-0CT-2016 08:07:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.39 59 107 1.16 258.76 255 8 1. 31E-02 74.5 5.08E+OO T 0 186.31 103 150 1.19 372.60 367 13 2.39E-02 59.5 4.29E+00 T 0 *258.46 60 48 2.58 516.90 511 11 1. 44E-02 55.6 3.25E+00 0 291.35 13 48 2.01 582.69 577 8 3.lOE-03 **** 2.90E+OO T 0 328.80 7 42 0.65 657.57 653 6 l.82E-03 **** 2.58E+00 T 0 450.55 10 25 0.49 901. 07 8 97 8 2.40E-03 **** 1. 90E+OO 0 463.41 38 18 1. 48 92 6. 78 921 11 9.58E-03 56.9 1.85E+OO T 0 533.47 18 10 2.38 1066.89 1062 10 4.67E-03 85.0 1.62E+00 0 537.32 11 12 1. 20 1074.59 1072 8 2.94E-03 **** 1.61E+OO T 0 545.07 19 25 3.44 1090.08 1081 16 5.00E-03 **** l.59E+00 T 0 554. 96 8 12 o. 72 1109.86 1108 6 1. 96E-03 **** 1.57E+OO 0 563.51 10 18 0.57 1126.95 1119 10 2.69E-03 **** 1.54E+OO T 0 623.55 12 9 3.28 12*47.01 1242 9 3.05E-03 **** 1. 41E+OO 0 633 .11 11 41 5.34 1266.13 1256* 14 2.90E-03 **** 1.39E+OO T 0 643.35 6 12 0.91 1286.60 1282 6 l.54E-03 **** 1.37E+OO 0 679.66 11 8 1. 08 1359.22 1354 10 3.00E-03 **** 1.30E+00 0 726.74 24 13 4.32 1453.35 1446 13 6.47E-03 76.0 l.23E+00 T 0 772.05 22 20 4.63 1543.94 1533 20 5.83E-03 **** 1.16E+OO T 0 816.20 12 4 2.17 1632.23 1628 8 3.17E-03 84.1 1. llE+OO T 0 905.10 5 7 1. 39 1809.98 1804 9 l.28E-03 **** 1.0lE+OO 0 934.67 14 11 0.67 1869.10 1861 14 3.78E-03 **** 9.83E-01 0 951. 55 10 1 0.91 1902.84 1900 6 2. 69E.-03 75.2 9.68E-01 0 1000.30 17 4 3.42 2000.31 1993 15 4.55E-03 74.2 9.26E-01 T 0 1202.26 7 12 1. 35 2404.06 2397 10 1. 89E-03 **** 7.85E-01 0 1208.67 13 9 1. 04 2416.88 2409 12 3.59E-03 **** 7.82E-01 0 1377. 98 10 2 0.64 2755.32 2752 7 2. 81E-03 76.7 6.92E-01 0 1588.72 11 0 1. 50 3176.55 3171 10 3.06E-03 60.3 6.03E-01 Flags: "T" = Tentatively associated Page 3151of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:15.07 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 , * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l *
Acquisition date 3-0CT-2016 08:07:40 Sensitivity 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
Sample date 10-DEC-2015 11:25:00 Nuclide Library : SOLID *
Sample ID G405235012 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5464E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 1-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF'GAM36 CAN.CNF;?
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 *PB-214 RN-222 RA-224 RA-226 . AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.591E-01 1.167E+OO 7.735E-02 4.279E-02 4.521E-02 3.898E-02 4.033E-02 5.802E-02 6.647E-02 5.802E-02 4.332E-01 5.802E-02 1. 231E-01 1.231E-01 4.033E-02 5 . .BOOE-02 1.231E-01 1.093E+OO 5.800E-02 1.093E+OO 4.656E-02 2.563E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 3152 of5809 Le (pCi/GRAM 7.856E+00 4.574E-02 O.OOOE+OO 2.149E-02 2.676E-01 O.OOOE+OO O.OOOE+OO 7.609E-02 4. 723E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-.85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 . PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3153 of5809 O.OOOE+OO 4.519E-02 4.812E-Ol 6.780E+OO 3.833E-02 2.089E-01 1.971E+OO 7.853E+OO O.OOOE+OO 2.163E-01 0.000E+OO O.OOOE+OO 7.287E-01 8.642E+OO 8.932E-01 O.OOOE+OO l.522E-01 5.940E+02 3.489E-02 7. 931E-01 1.999E+00 1.198E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.067E-02 7.618E-02 5. 965E+OO 4.804E-01 4.804E...:01 2.772E-02 1.167E-.01 2.350E-01 O.OOOE+OO O.OOOE+OO 1.188E-01 1.838E+OO 1.109E-01 2.504E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO *O.OOOE+OO 0.000E+OO 0.000E+OO 4. 096E-02 0.000E+OO 6.342E-02 1.302E-01 O.OOOE+OO O.OOOE+OO 9.416E-02 O.OOOE+OO O.OOOE+OO l.920E+Ol O.OOOE+OO 3.666E-01 5.682E-02 4.914E+OO 4.835E-02 O.OOOE+OO 7.476E+02 0.000E+OO 2.924E-02 8.517E-02 1.718E-01 1.103E-01 1.014E-01 1.950E+OO 5. ll 7E-02 1.662E+Ol 1.970E-01 7.791E-02 2.352E-02 4.836E+OO 9.259E-01 2.700E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3154 of 5809 3.189E+Ol l.192E+02 4.885E-01 2.198E+OO 7.120E-02 2.298E+OO 4. 581E-01 6.957E-01 6.956E-01 4.004E-01 5.800E-01 l.918E-01 1.918E-01 4.365E-01 4.813E-01 5.800E-01 5.886E-02 3.535E-01 5. 496E+OO 1. 739E-01 5.886E-02 O.OOOE+OO 2.048E-01 3.363E+02 1. 262E-01 9.330E-02 7.457E-02 3.793E-02 3.981E-02 l.134E-01 NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:20.75 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA *
* *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l *
Acquisition date 3-0CT-2016 08:07:40 Sensitivity : 3.000 *
Detector ID GAM36 Energy-tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
Sample date 10-DEC-2015 11:25:00 Nuclide Library : SOLID *
Sample ID G405235012 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5464E+02 GRAM *
Quantity Err ( % ) : 1. 2 933E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 1-JUN-2016 09:39:12 Eff. Geometry. : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7 .
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.377E+Ol 2 .. 089E+OO 2.089E+OO CD-109 2.252E+OO 2.909E+OO 2.909E+OO SN-126 l.439E-01 1.858E-01 1.858E-01 BA-137M 3.445E-01 9.738E-02 9.738E-02 CS-137 3.639E-01 1.029E-01 1. 029E-01 TL-208 3. 313E-01 1. 072E-01 1.072E-01 PB-212 l.385E+OO 1.738E-01 1. 738E-01 BI-214. 8.471E-01 2.125E-01 2.125E-01 PB-214 1.0lOE+OO 2.126E-01 RN-222 8.471E-01 2.125E-01 2.125E-01 RA-224 2.410E+OO 1. 734E+OO 1. 734E+OO RA-226 8.471E-01 2.125E-01 2.125E-01 AC-228 1.007E+OO 3.253E-01 3.253E-01 RA-228 1.007E+00 3.253E-01 3.253E-01 TH-228 1.385E+OO 1.738E-01 1.738E-01 TH-230 8.469E-01 2.124E-01 2.124E-01 TH-232 1.007E+OO 3.253E-01 TH-234 1.184E+OO 2.299E+OO 2.299E+OO U-234 8.469E-01 2.124E-01 2.124E-01 U-238 1.184E+OO 2.299E+OO 2.299E+OO AM-243 1.984E-01 1.134E-01 1.134E-01 ANH-511 l.698E-01 1.353E-01 1.353E-01 Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.388E+Ol 1.169E+Ol 1.326E+Ol NOT IDENT. NA-22 -4.322E-02 6.349E-02 6.641E-02 NOT IDENT. NA-24 1. OOOE+41 1.379E+41 O.OOOE+OO SHORT HLIF AL-26 -1.009E-02 3.229E-02 3. 2 61E-02 NOT IDENT. SC-46 -2.551E-01 4.0lOE-01 4.171E-01 FAIL ABUN V-48 8.315E+03 1.782E+04 1.821E+04 SHORT HLIF CR-51 -4.712E+02 4.466E+02 4.945E+02 SHORT HLIF MN-54 5.323E-02 7.881E-02 8.238E-02 NOT IDENT. Page 3155of5809 C0-56 -1.022E-01 5.833E-01 5.852E-01 NOT IDENT. MN-56 -1.000E+41 6.027E+41 O.OOOE+OO SHORT HLIF C0-57 1.567E-02 4.796E-02 4.848E-02 NOT IDENT. C0-58 -5.616E-03 5.973E-01 5.973E-01 NOT IDENT. FE-59 -2.197E+OO 8.187E+OO 8.247E+00 NOT IDENT. C0-60 -7.445E-03 4.669E-02 4.681E-02 NOT IDENT. ZN-65 6.894E-02 2.498E-01 2.517E-01 NOT IDENT. GE-68 -2.026E+00 3. 021E+OO 3.157E+OO NOT IDENT. AS-73 8.629E+OO *7.609E+OO 8.546E+OO NOT IDENT. AS-74 3.007E+03 5.441E+03 5.607E+03 SHORT HLIF SE-75 1.056E-01 2.388E-01 2. 435E-0.l NOT IDENT. BR-77 1.404E+38 1.207E+39 O.OOOE+OO SHORT HLIF SR-82 2.194E+02 7.092E+02 7.161E+02 SHORT HLIF RB-83 8.669E-02 8.818E-01 8.827E-01 NOT IDENT. KR-85 8.653E+OO 8.547E+OO 9.395E+OO NOT IDENT. SR-85 8.904E-01 8.838E'-01 9.707E-01 NOT IDENT. RB-86 7 93E+04 3.261E+04 3.360E+04 SHORT HLIF Y-88 -7.223E-02 2.297E-01 2.320E-01 NOT IDENT. Y-91 -3.935E+02* 1.253E+03 l.265E+03 NOT IDENT. NB-94 l.658E-02 3.731E-02 3.805E-02 NOT IDENT. NB-95 8.572E-02 1.014E+OO .1. 015E+OO NOT IDENT. NB-95M -l.658E-01 2.526E+OO 2.527E+OO NOT IDENT. ZR-95 3.502E-01 1.303E+OO 1.313E+OO NOT IDENT. NB-97 1. OOOE+41 l.283E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 1. 705E+41 0.000E+OO SHORT HLIF M0-99 -4*. 920E+30 1.134E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.885E+41 O.OOOE+OO SHORT HLIF RH-101 2.476E-02 3.363E-02 3.543E-02 NOT IDENT. RH-102 8.764E-02 8.765E-02 NOT IDENT. RU-103 3.893E+OO 6.053E+OO 6.303E+OO FAIL ABUN -2 .134E-01 6.581E-01 6.651E-01 NOT IDENT. RU-106 -2.134E-01 6.581E-01 6. 651E-01 NOT IDENT. AG-108M -1. 34 6E-02 3.257E-02* 3.313E-02 NOT IDENT. AG-110M -1.380E-02 l.418E-01 l.420E-01 NOT IDENT. SN-113 -5.246E-02 2.639E-01 2.650E-01 NOT IDENT. CD-115 1.366E+39 2 .111E+39 O.OOOE+OO SHORT HLIF SN-117M -4.365E+04 9. 411E+04 9.615E+04 SHORT HLIF TE-123M -2.052E-02 l.345E-01 l.348E-01 NOT IDENT. SB-124 l .113E+OO 1.543E+OO 1.623E+OO NOT IDENT. SB-125 1.032E-02 1.210E-01 1. 211E-01 FAIL ABUN TE-125M 1. 784E+02 2.556E+02 2.680E+02 NOT IDENT. I-126 l.202E+06 9.944E+05 l.132E+06 SHORT HLIF SB-126 9.405E+05 l.529E+06 l.587E+06 SHORT HLIF SB-127 -5.551E+21 2.103E+22 O.OOOE+OO SHORT HLIF I-131 4.133E+09 4. 896E+09 5.238E+09 SHORT HLIF I-132 -l.000E+41 1. 841E+42 O.OOOE+OO SHORT HLIF TE-132 -1.162E+26 3.019E+26 O.OOOE+OO SHORT HLIF BA-133 1.368E-02 4.689E-02 4.729E-02 FAIL ABUN I-133 :-1.000E+41 4.249E+41 O.OOOE+OO SHORT HLIF CS-134 1. 758E-02 7.139E-02 7.183E-02 FAIL ABUN CS-135 -l.049E-01 1.662E-01 1.728E-01 NOT IDENT. I-135 -1.000E+41 7 .196E+41 O.OOOE+OO SHORT HLIF CS-136 2.513E+05 4.812E+05 4.943E+05 SHORT HLIF CE-139 -3. 431E-02 1.092E-01 l.103E-01 NOT IDENT. BA-140 1.521E+06 l.829E+06 1.953E+06 SHORT HLIF LA-140 9.148E+04 3.107E+05 3.134E+05 SHORT HLIF CE-141 -1.837E+Ol 2.367E+Ol 2.508E+Ol NOT IDENT. CE-143 l.000E+41 2.575E+41 O.OOOE+OO SHORT HLIF CE-144 2. 411E-01 3.830E-01 3. 981E-01 NOT IDENT. PM-144 -l.160E-02 6.811E-02 6.831E-02 NOT IDENT. PR-144 -1. 054E+OO 5. 901E+OO 5:920E+OO NOT IDENT. PM-146 3 . .331E-02 5.310E-02 5.518E-02 FAIL ABUN ND-147 -3.489E+06 3.694E+07 3.697E+07 SHORT HLIF PM-147 -1.006E+OO 8.159E+02 8.159E+02 NOT IDENT. PM-149 -2.189E+40 2.993E+40 O.OOOE+OO SHORT HLIF EU-150 2.220E-02 3.179E-02 3.333E-02 FAIL ABUN EU-152 -5.809E-02 1.118E-01 l.149E-01 NOT IDENT. GD-153 3.292E-02 1. 939.E-01 1.945E-01 NOT IDENT. EU-154 -1.lOOE-01 l.548E-01 1. 62 6E-'01 NOT IDENT. EU-155 -7.153E-03 1.lOlE-01 l.lOlE-01 *FAIL ABUN TB-160 4.382E-01 2. 211E+OO 2.219E+OO FAIL ABUN H0-166M -8.789E-03 6.146E-02 6.159E-02 NOT IDENT. TM-171 -3.869E+OO 1. 748E+Ol 1. 757E+Ol NOT IDENT. HF-172 2.282E-02 *2.298E-01 2.300E-01 FAIL ABUN LU-172 3.835E-03 9.394E-02 9. 396E-02 FAIL ABUN LU-176 -1.853E-03 2.811E-02 2.812E-02 . FAIL ABUN HF-181 1.758E-03 5.398E+OO 5.398E+00 NOT IDENT. TA-182 -7.022E-01 1.216E+OO l.256E+00 FAIL ABUN Page 3156of5809 RE-183 9. 966E-Ol 2.726E+OO 2.763E+OO NOT IDENT. RE-184 -2.399E-Ol 4.279E+Ol 4.279E+Ol NOT IDENT. W-188 1.029E+02 2.120E+02 2.171E+02 FAIL ABUN IR-192 1.705E-Ol 5.552E-01 5.605E-01 FAIL ABUN HG-203 2.766E-Ol 2.749E+OO 2.751E+OO NOT IDENT. BI-207 5.891E-02 7.435E-02 7.895E-02 FAIL ABUN PB-210 -1. 426E+OO 2.489E+OO 2.571E+OO NOT IDENT. BI-211 2.782E+OO 5.873E-01 1.385E+OO FAIL ABUN PB-211 -3.359E-01 8.038E-01 8.179E-01 NOT IDENT. BI-212 l.444E+OO 1.078E+00 1. 259E+OO FAIL ABUN RN-219 -9.572E-03 4.406E-01 4.406E-01 NOT IDENT. RA-223 -1. 789E-01 7.173E-01 7.219E-01 FAIL ABUN AC-227 -6.853E-03 2.432E-01 2.432E-01 NOT IDENT. TH-227 -6.853E-03 2.432E-01 2.432E-01 NOT IDENT. TH-229 -1. 759E-01 5.135E-01 5.195E-01 FAIL ABUN PA-231 3.236E-01 5.299E-01 5.496E-01 NOT IDENT. TH-231 -1. 78 9E-01 7.173E-01 7.219E-01 FAIL ABUN PA-233 I 4.224E-02 6.307E-02 6.589E-02 NOT IDENT. PA-234 7.189E-02 4.168E-01 4.181E-01 FAIL ABUN PA-234M 1.032E+Ol 7.512E+OO 8.835E+OO FAIL ABUN U-235 3.330E-02 1.935E-01 l.941E-01 FAIL ABUN NP-237 4.224E-02 6.307E-02 6.589E-02 FAIL ABU.N NP-238 1.000E+41 2.226E+41 O.OOOE+OO SHORT HLIF NP-239 -5.313E-02 2.280E-01 2.293E-01 FAIL ABUN PU-239 8. 872E+02 6.493E+02 7.626E+02 FAIL ABUN AM-241 1.825E-02 1.297E-01 l.299E-01 NOT IDENT. CM-243 5.526E-02 9.599E-02 9.917E-02 FAIL ABUN BK-247 7.357E-03 8.607E-02' 8.613E-02 NOT IDENT. CM-247 l.727E-02 3.952E-02 4.028E-02 FAIL ABUN CF-249 2.069E-02 4.093E-02 4.198E-02 NOT IDENT. CF-251 4.467E-02 1.233E-01 1.249E-01 NOT IDENT. Page 3157of5809
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 22.6668 87.09 101. 37 52 136.47 51.2710 45.60 47.2366 87.57 101.4831 140.51 0.0000 46.54 46.5986 88.03 95.4023 143.76 55.7815 49.72 0.0000 88.34 95.4673 144.24 49.9471 51. 35 48.1423 88.47 96.6735 145.44 57.8900 51. 87 47.4180 89. 96 81.6125 152.43 64.4565 52.39 47.4955 1093.63 95.9473 153.25 0.0000 52. 97 37.9040 91.11 0.0000 323.87 52.6959 53.44 35.5365 92.59 76.7224 156.02 0.0000 54.07 54.2174 93 .35 76.8464 158.56 0.0000 57.36 0.0000 94.56 77.0425 159.00 51. 0646 57.53 67.8678 94.65 77.0570 162.33 47.2847 57.98 51. 5819 94.67 77.0603 162.66 0.0000 59.27 54.2413 94.87 50.1997 163.33 53.3971 59.32 54.2491 97.43 54.0715 165.86 47.5214 59.54 56.7511 98.43 51.4732 176.31 54.3619 60. 96 67.1668 98.44 51.4745 176.60 0.0000 61.17 53.9858 99.53 56.1137 177.52 45.2038 62. 93 65.6012 100 .11 52.5550 181.07 0.0000 63.29 65.6664 102.03 57.3052 181.52 46.8206 63.58 65. 7190 103.18 48.3192 184.41 37.3217 64.28 68.9016 103.37 47.4253 143.76 37.3848 66.73 62. 92 65 105.21 60.4107 193.51 51.3918 67.24 66. 3724 105.31 60.4228 197.03 46.3499 125.81 63.0850 106.12 '60.5175 198.01 36.9141 67.75 63. 0964* 106.47 61.4763 201.83 .33.9077 69.67 50.7317 109.28 44.2800 203.43 53.0838 70.83 71.2358 111. 00 48.1255 205.31 46.8192 72.81 60.2305 111.76 0.0000 210.85 51.4124 72.87 60. 2396 114. 06 49.3305 215.65 39.8522 74.66 77.9192 116. 30 0.0000 222 .11 41.2326 74.82 77.94971 116.74 50. 5072 227.09 40. 3722 74.97 77.9789 119.76 48.9004 227.38 46.9341 77 .11 78.3864 121.12 45.2476 228.16 0.0000 78.74 78.6933 121.22 51.8554 228.18 41. 5138 79.69 78.8710 121. 78 48.1312 116.74 41. 5138 80.12 78.9509 122.06 50.9875 235.69 35.2471 80.19 0.0000 122.92 50 .1185 235. 96 41.1335 80.57 79.0342 123.07 50.1315 238.63 26.5192 81. 00 79.1140 265.00 51.1317 238.98 0.0000 81.07 79.1265 125.81 45.6176 240.99 26.5858 81.75 71. 9946 127.23 39.3768 242.00 26.6144 83.79 70.0000 127.91 48.3243 244.70 31.1385 84.00 91.0436 129.30 58.3165 252.40 0.0000 85.43 93.6808 131.20 56.2649 252.80 25.7939 86.55 101.2532 133.02 50.0211 254.15 0.0000 8 6. 7 9 .101. 3067 133.52 53.9133 256.23 25.5090 86.94 101.3409 136.00 54.1321 260.90 0.0000 Page 3158 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 29.5087 355.39 0.0000 584.27 18.0336 264.80 29.5126 356.01 19.6787 595.83 0.0000 265.00 34.0594 364.49 0.0000 427.87 8.6158 268.22 41. 0010 366.42 0.0000 602.52 0.0000 269.46 34.2096 372*_51 22.4231 604. 72 17.2683 270.03 33.0870 375.05 12.4814 607.14 8.6448 271.23 21. 7032 377.52 24.1755 609.32 10.5779 273.65 0.0000 356.01 15.9141 610.33 10.5833 276.40 18.3677 388.16 17.6453 614.28 17.3533 277.37 26.4281 388.63 0.0000 618.01 15.0681 277.60 26.4337 391.69 24.4304 620.36 8.7034 278.00 26.4442 264.66 21.1980 621.93 13.0655 279.20 27.6255 401.81 22. 9131 630.19 0.0000 279.54 27.6343 402.40 18.6775 631.29 19.4474 279.70 23.0322 404.85 25.5139 633.25 19.4661 280.46 24.5853 410.95 17.9371 634.78 0.0000 283.69 21.9630 413. 71 23. 9622 635:95 11. 69$3 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 32.4186 423.72 0.0000 645.85 8.8143 285.90 0.0000 427.09 15.5475 657.76 7.3880 287.50 20.1078 427.87 19.8770 657.90 0.0000 290.67 26.7601 433.94 22.5622 661. 66 18.7511 293.27 0.0000 439.40 19.1609 664.57 0.0000 351.93 30.3767 453.88 13.1894 666.33 0.0000 295.96 30.3965 463.37 15.9243 666.50 0.0000 879.38 43.7500 468.07 22.6274 667.71 0.0000 299.98 37.5479 473.00 0.0000 677.62 13.4247 300.09 38. 7253 475.06 12.4779 685.70 0.0000 300.13 38.7263 476.78 16.0602 695.00 0.0000 301.36 27.0205 477.60 17.8536 696. 49 14.0450 302.85 30.5862 482.18 20.5901 696. 51 14.0450 256.23 20.0277 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.0501 306.78 27.1518 497.08 10.8411 697.49 11. 0403 308.46 20.0983 505.52 12.2583 702.65 10.0602 311. 90 17.7873 507.63 0.00.00 706.68 10.0789 316.51 26.1921 511. 00 13.6647 711. 68 10.1017 319.41 0.0000 514.00 13.6890 720.70 0.0000 320.08 0.0000 514.00 13.6890 721. 93 0.0000 321.04 26.2942 520.40 15 .1143 722.78 15.2283 323.87 29.9522 520.69 0.0000 722.91 18.2747 325.23 33.5850 522.65 0.0000 723.31 18.2783 328.76 0.0000 527.90 0.0000 724.19 18.2856 333.37 26.5681 528.26 12.1467 727.33 11.1902 333.97 24.1650 529.59 19.3389 733.00 10.1982 334.37 29.0076 529.87 0.0000 735.93 14.2962 338.28 21.8260 531.02 0.0000 333.97 6.1311 338.32 21.8265 537.26 0.0000 739.50 0.0000 311. 90 29.1533 546.56 0.0000 747.24 14.3669 340.48 29.1533 552.55 8. 3965 748.06 5.1329 340.55 0.0000 563.25 8.4459 752.31 9.2560 344.28 28.0249 569.33 12.2404 753.82 0.0000 345.93 17.0813 946.00 12.2415 756.73 5.1522 351.06 23:2774 569.70 16.0094 756. 80 5.1522 351. 93 23.2937 583.19 18.0236 884.68 10.8529 Page 3159of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 9.3098 1274.44 8.4689 1620.50 2. 0114 766.42 12.4165 1001.03 6.7861 1621.92 2.0120 766.84 12.4185 1002.74 10.1851 1678.03 0.0000 772.60 0.0000 1004.73 5. 0960 1690.97 0.0000 776.52 0.0000 507.63 0.0000 1750.46 0.'0000 739.50 0.0000 1025.87 0.0000 1764.49 3 .1130 778.90 8.7374 1028.54 0.0000 1063.66 3 .1166 783.70 0.0000 1037.84 5. 7255 1771.35 1.0391 785.37 7.3008 1038.76 0.0000 1791.20 0.0000 792.07 15.6885 631. 29 8.0385 1808.65 2.0944 794.95 12.5654 1048.07 0.0000 1810.72 0.0000 795.86 13.6178 1049.04 9.1940 1836.06 2.1061 810.06 2.1073 1050.41 11. 4982 810.29 4.2148 1063.66 8.0835 344.28 5.2690 1077.00 0.0000 810.76 6.3235 1077.34 10.4385 815.77 0.0000 1085.87 5.8150 1048.07 0.0000 1093.63 6.9951 '832. 01 9.5665 1099.45 9.6364 834.85 7.4492 1112. 07 8.7946 835.71 7.4517 1112.84 4.3985 836.80 0.0000 1115. 54 8.4521 846.75 0.0000 1120.29 9.6989 846.77 10.6917 1120.55' 9.6995 856.80 0.0000 1221.41 9.8786 860.56 8.5993 1129. 67 7.9585 871.09 10.7926 1131. 51 0.0000 873.19 7.5608 1147.95 0.0000 875.33 0.0000 1173.23 8. 9600 879.38 7.5788 1177.95 6.2809 880.51 9.7482 1189.05 10.8025 883.24 10.8427 1204.77 14.4697 884.68 11. 9332 1221.41 12.7225 889.28 8.6940 1231. 02 13.6688 894.76 8.7119 1235.36 0.0000 898.04 7.6320 1238.28 10.9578 900.72 4. 9113 1260.41 0.0000 903.28 9.8320 1271.87 6.4523 911.20 7.6694 1274.44 11. 0691 912.08 7.6719 1274.54 11. 0698 923.98 0.0000 1291.59 5.5609 926.50 8.8141 1298.22 0.0000 *929 .11 8.2712 1312 .11 0.0000 937.49 9.9554 1332.49 5.6228 944.13 0.0000 1362.66 0.0000 946.00 11. 0954 1365.19 8.5073 949.00 11.6625 1368.63 0.0000 667. 71 0.0000 1384.29 2.8499 962*. 31 11.1597 1408.01 5.7345 964.08 5.0250 1457.56 0.0000 966 .17 6.7048 1460.82 4.8425 911. 20 11.1857 1489.16 1.9504 968.97 11.1857 1505.03 2.9370 983.53 0.0000 1584.12 4.7874 984.45 0.0000 1596.21 0.0000 Page 3160 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:13:37.83 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;119 Background date : Z-OCT-2016*11:02:18. Sample date 8-DEC-2015 11:23:00. Acquisition date : 3-0CT-2016 08:10:29. Sample ID G405235013 Sample quantity l.44574E+02 GRAM Detector name : GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.06 0.2% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 . ******************************************************************************** Pk It 1 0 2 0 3 3 4 3 5 3 6 3 7 3 8 3 9 0 10 0 11 0 12 0 13 4 14 4 15 5 16 5 17 0 18 0 19 0 20 0 21 0 '22 0 23 0 24 10 25 10 26 10 27 1 28 1 29 0 30 0 31 0 32 . 0 33 0 34 0 Page 3161of5809 Energy 46.50* 63.49* 7 4. 8 6* 77.27* 84.07* 87.32 89.88 92.86* 129.25 135.60 185.77* 209.76 238.91* 241.66 270.18 273.53 295.59 300.37 338.80 352.16* 411. 07 464.00 498.44 511.26* 516.70 519.03 521.78 524.48 583.87* 609.73* 636.18 662.05* 728. 48* 782.60 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 66 .96 289 372 49 113 51 101 46 38 116 95 384 97 49 19 134 43 67 206 20 17 14 84 16 10 16 16 105 142 7 345 32 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 113 0.88 276 0.96 219 1.55 110 . 0.90 212 1. 58 156 1.23 126 0.93 135 1.13 122 0.60 121 2.98 126 0.94 73 2.39 42 1. 03 55 1. 67 61 2.10 44 1. 62 66 0.99 79 1.34 95 0. 96 53 1.13 .36 2.23 39 1. 57 22 0.95 24 4.01 6 1.53 3 1.21 3 1. 51 4 1. 81 33 1. 81 23 1. 24 16 0.49 38 1. 34 20 1. 91 2 1.12 93.30 127.26 149.99 154.81 168.41 174.91 180.04 185.98 258.74 271. 43* 371. 76 419.73 478.00 483.51 540.52 547.23 591.35 600.90 677.74 704.46 822.26 928.10 996. 98 1022.62 1033.49 1038.16 1043.66 1049.06 1167. 83 1219.55 1272. 45 13i4 .18 1457.05 1565.29 90 122 143 143 161 161 161 161 255 267 367 414 470 470 535 535 585 596 672 697 816 924 992 1014 1014 1014 1041 1041 1161 1213 1267 1316 1452 1560 8 1. 84E-02 32. 5 11 2.66E-02 36.5 15 8.03E-02 10.8 8.32E+OO 15 1. 03E-01 6. 8 32 l.37E-02 53.8 l.02E+00 32 3.15E-02 20.1 32 1.41E-02 37.5 32 2.80E-02 25.1 9 1.26E-02 46.1 10 l.06E-02 56.6 11 3.22E-02 21.7 12,2.65E-02 20.8 18 1.07E-01 5.8 1.45E+OO 18 2.70E-02 25.8 16 1.35E-02 34.1 1.73E+OO 16 5.36E-03 64.1 11 3.72E-02 14.6 12 1.21E-02 43.5 12 l.87E-02 31.l 12 5.72E-02 10.1 9 5.52E-03 60.0 7 4.68E-03 67.5 8 3.99E-03 62.2 27 2.34E-02 20.4 2.44E+OO 27 4.40E-03 46.5 27 2.88E-03 42.9 12 4.40E-03 29.0 8.51E-01 12 4.36E-03 32.6 12 2.92E-02 14.9 13 3. 94E-02 11. 1 7 l.93E-03105.6 14 9.59E-02 6.6 12 8.77E-03 34.5 9 3.34E-03 36.3 Peak Search Report (continued) Page : 2 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 8 61. 22 37 0 1. 48 1722.54 1716 14 1.03E-02 16.4 36 0 912.01* 61 17 1. 76 1824.14 1815 14 1. 69E-02 19.7 37 0 935.83 34 7 4. 86 1871. 77 1864 16 9.41E-03 25.2 38 0 952.71 11 10 0.69 1905.55 1899 10 3.06E-03 61. 7 39 0 969. 98* 33 *13 1. 34 1940.09 1935 10 9.22E-03 28.1 40 0 1104 .14 13 21 4.41 2208.47 2198 17 3.55E-03 87.1 41
0 1121. 49 23 17 0.75 2243.17 2239 10 6.41E-03 39.6 42 0 1208.19 13 10 1. 54 2416.62 2411 10 3. 61E-03 53.3 43 0 1211. 03 10 0 1. 24 2422.30 2420 6 2.78E-03 31. 6 44 0 1238.66 30 13 1. 50 2477.57 2470 13 8.33E-03 30.8 45 0 1378.39. 8 4 0.61 2757.12 2752 9 2.18E-03 60.0 46 0 1461. 77* 256 8 1. 76 2923.94 2915 16 7.lOE-02 6.8 47 0 1765.03 28 0 1. 05 3530.75 3524 12 7.78E-03 18.9 Flag: "*" = Peak area was modified by background subtraction Page 3162 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:13:39 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 11:23:00 G405235013 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:10:29 144.57 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA41 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 3163of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:06.06 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.926E-01 l.342E+Ol 1.342E+Ol 13.57 OK RU-103 497.08 91.00* 2.367E+OO 3.686E-02 7.344E+OO 124.44 OK 610.33 5.76 1.970E+OO 6.774E+OO l.350E+03 22.14 OK CD-109 88.03 3.70* 7.449E+OO 1.582E+OO 2.483E+OO 69.50 OK SN-126 64.28 9. 6.0 7.794E+OO -8. 387E-01 8.387E-01 72. 92 OK 86.94 8.90 7.449E+OO 6.579E-01 6.579E-01 69.50 OK 87.57 37.00* 7.449E+OO 1.582E-01 1.582E-01 69.50 OK BA-137M 661.66 89.90* 1. 826E+OO 1.132E+OO 1.154E+OO 13.23 OK CS-137 661.66 85.10* L 826E+OO 1.196E+OO 1.219E+00 13.23 OK TL-208 277.37 6.60 3.907E+OO Line Not Found Absent 583.19 85.00* 2.050E+00 3.288E-01 3.288E-01 29.74 OK 860.56 12.50 1.433E+OO 1.085E+OO 1.085E+OO 32.88 OK

PB-210 46.54 4.25* 7.552E+OO 1.385E+OO 1.421E+OO 64.95 OK PB-212 74.82 10.28 7.683E+OO 1. 726E+OO 1.726E+OO 31.59 OK 77 .11 17.10 7.644E+OO 1.836E+OO 1.836E+00 13.51 OK 238.63 43.60* 4.382E+OO l.184E+OO 1.184E+OO 11. 68 OK 300.09 3.30 3.666E+00 2. 071E+00 2. 071E+OO 86.98 OK BI-214 609.32 45 .. 49* 1.970E+OO 8.578E-01 8.581E-01 22.14 OK 1120.29 14.92 1.127E+oo* 7.033E-01 7.035E-01 79.28 OK 1764.49 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 OK PB-214 74.82 5.80 7.683E+OO Line Not Found <<INT Reject 77 .11 9.70 7.644E+OO 3.237E+OO 3.238E+00 13.51 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3. 714E+OO 1.133E+OO 1.133E+OO 29.15 OK 351. 93 35.60* 3.212E+OO l.026E+OO 1.026E+OO 20.15 OK RN-222 609.32 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 OK 1120.29 14.92 l.127E+OO 7.033E-01 7.035E-01 79.28 OK 1764.49 15.30 7.618E-01 l.177E+OO l.177E+00 37.80 . OK RA-224 240.99 4.10* 4.345E+OO l.202E+OO 1.202E+OO 146.05 OK RA-226 609.32 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 OK 1120.29 14.92 l.127E+00 7.033E-01 7.035E-01 79.28 OK 1764.49 15.30 '7.618E-01 l.177E+OO l.177E+00 37.80 OK AC-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.319E+OO 1. 031E+OO 1.031E+OO 62. 23 OK 794.95 4.25 l.543E+00 Line Not Found Absent 835. 71 1. 61 1.473E+00 Line Not Found Absent 911.20 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 OK 968. 97 15.80 l.285E+OO 8.493E-01 8.493E-01 56.29 OK RA-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32. 11. 27 3.319E+OO 1.031E+OO l.031E+00 62. 23 OK 794.95 4.25 1.543E+OO Line Not Found Absent 835.71 L61 1. 473E+00 Line Not Found Absent 911.20 25.80* l.360E+OO 9.074E-01 9.074E-01 39.40 OK 968. 97 15.80 l.285E+00 8.493E-01 8.493E-01 56.29 OK TH-228 74.82 10.28 7.683E+OO 1.726E+OO 1. 726E+OO 31. 59 OK 77 .11 17.10 7.644E+OO 1.836E+OO l.836E+00 13.51 OK 238.63 43.60* 4.382E+OO l.184E+OO l.184E+00 11. 68 OK 300.09 3.30 3.666E+OO 2.071E+OO 2. 071E+OO 86.98 OK Page 3164of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : .G405235013
Acquisition date 3-0CT-2016 08:10:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-229 85.43 14.70 7.517E+OO 2.864E-Ol 2.864E-01 107.55 OK 88.47 24.00 7.449E+OO 2.440E-Ol 2.440E-01 69.50 OK 193.51 4.41* 5.088E+OO Line Not Found Absent 210.85 2.80 4.815E+OO 4.207E+OO 4.208E+OO 41.60 OK TH-230 609.32 45.49* l.970E+OO 8.578E-01 8.578E-01 22.14 OK 1120.29 14.92 l.127E+OO 7.033E-01 7.033E-01 79.28 OK 1764.49 15.30 7.618E-01 l.177E+OO l.177E+OO 37.80 OK PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.666E+OO 1.277E+OO . l.277E+OO 86.98 OK TH-232 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.319E+OO 1. 031E+OO 1. 031E+OO 62.23 OK 835.71 1. 61 l.473E+OO Line Not Found Absent 911.20 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 OK 968. 97 15 .. 80 1.285E+OO 8.493E-01 8.493E-01 56. 29 OK TH-234 63.29 3.70* 7.794E+OO 2.176E+00 2.176E+00 . 72. 92 OK 92.59 4.23 7.325E+OO 2.067E+OO 2.067E+OO 50.15 OK U-234 609.32 45.49* 1.970E+OO 8.578E-01 8.578E-01 22.14 OK 1120.29 14.92 l.127E+00 7.033E-01 7.033E-01 79.28 OK i764.49 15.30 7.618E-01' 1.177E+OO 1.177E+00 *37. 80 OK U-235 89. 96 3.47 7.393E+OO 1.264E+OO 1.264E+OO 75.02 OK 93.35 5.60 7.325E+OO 1. 562E+OO 1.562E+OO 50.15 OK 143.76 10.96* 6.093E+OO Line Not Found Absent 163.33 5.08 5.667E+OO Line Not Found Absent 185.72 57.20 5.227E+OO 2.333E-01 2.333E-01 43.44 OK 205.31 5.01 4.887E+OO Line Not Found Absent U-238 63.29 3.70* 7.794E+OO 2.176E+OO 2.176E+OO 72.92 OK 92.59 4.23 7.325E+OO 2.067E+OO 2.067E+OO 50.15 OK AM-243 43.53 5.90 7. 421E+OO Line Not.Found Absent. 74.66 67.20* 7.683E+OO 2.640E-01 2. 641E-01 31. 59 OK ANH-511 511. 00 100.00* 2.313E+OO 2.004E-01 2.004E-01 40.73 OK Flag: "*" = Keyline Page 3165 of5809 VAX/VMS Nuclide Identification* Report Generated 03-0CT-2016 09:13:40.80 *******************************************.************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l *
Acquisition date 3-0CT-2016 08:10:29 Sensitivity : 3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.06 Half life ratio : ***** *
Sample date 8-DEC-2015 11:23:00 Analyst initials: MXRl *
Sample ID G405235013 Sample Quantity 1.4457E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date : 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File ': DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;'3 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.342E+Ol 1. 784E+OO RU-103 7.344E+OO 8.956E+OO CD-109 2.483E+00 1.691E+OO SN-126 1.582E-01 1.078E-01 BA-137M l.154E+OO l.497E-01 CS-137 1.219E+OO 1.581E-01 TL-208 3.288E-01 9.584E-02 PB-210 1.421E+OO 9.045E-01 PB-212 l.184E+OO l.355E-01 BI-214 8.581E-01 1. 862E-01 PB-214 l.026E+00 2.026E-01 RN-222 8.581E-01 1. 8 62E-01 RA-224 1.202E+OO 1. 720E+OO RA-226 8.581E-01 1. 8 62E-01 AC-228 9.074E-01 3.503E-01 RA-228 9.074E-01 3.503E-01 TH-228 1.184E+OO 1.355E-01 TH-229 2.255E-01 5.388E-01 TH-230 8.578E-01 1.861E-01 PA-231 1.277E+OO 1.089E+OO TH-232 9.074E-01 3.503E-01 TH-234 2.176E+OO 1.555E+OO U-234 8.578E-01 1.861E-01 U-235 -2.341E-02 2.042E-01 U-238 2.176E+OO 1.555E+OO AM-243 2.641E-01 8.175E-02 ANH-511 2.004E-01 7.998E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3166 of5809 Key-Line Activity (pCi/GRAM 5.147E+00 6.027E-03 0.000E+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.532E+Ol 5.947E-02 9.294E+40 MDA" (pCi/GRAM 7.420E-01 1.390E+Ol 1.662E+OO l.058E-01 8.929E-02 9.433E-02 7.288E-02 7.952E-01 l.022E-01 1.233E-01 l.483E-01 1.233E-01 l.095E+OO 1.233E-01 2.775E-01 2.775E-01 l.022E-01 1.064E+OO 1.233E-01 8.319E-01 2.775E-01 1.053E+OO l.233E-01 3.984E-01 l.053E+OO 6.463E-02 5.635E-02 MDA (pCi/GRAM 2.985E+Ol 1.193E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3 .*212E-02 2.816E-02 l.889E-02 NOT IDENT. SC-46 -3. 272E-Ol 4.132E-01 7.148E-01 FAIL ABUN V-48 O.OOOE+OO 1.692E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 4.497E+02 O.OOOE+OO SHORT HLIF MN-54 -5.825E-04 6. 511E-02 l.318E-01 NOT IDENT. C0-56 -l.375E-02 4.374E-01 8.986E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.237E-02 4.737E-02 9.132E-02 FAIL ABUN C0-58 -7.185E-02 6.447E-01 l.278E+OO NOT IDENT. FE-59 -6.747E-01 9.589E+OO l.633E+Ol NOT IDENT. C0-60 -3.631E-02 4.306E-02 6.830E-02 NOT IDENT. ZN-65 -2.634E-01 2.362E-01 3.465E-01 NOT IDENT. GE-68 -1. 572-E+OO 3. ll 7E+OO 5.598E+OO NOT IDENT. AS-73 1.478E+OO 2.671E+OO 5.057E+OO NOT IDENT. AS-74 O.OOOE+OO 7.205E+03 O.OOOE+OO SHORT HLIF SE-75 l.799E-02 2.404E-01 4.421E-01 FAIL ABUN BR-77 O.OOOE+OO 2.465E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 7.950E+02 O.OOOE+OO SHORT HLIF RB-83 6.204E-01 5.213E-01 l.469E+OO FAIL ABUN KR-85 1.119E+Ol 9.534E+00 1.858E+Ol NOT *I DENT. SR-85 1.178E+OO 1,007E+OO 1. 963E+OO NOT IDENT. RB-86 O.OOOE+OO 3. 688E+o4 O.OOOE+OO SHORT HLIF Y-88 -1.347E-01 2.056E-01 3.668E-01 NOT IDENT. Y-91 -3.063E+02 8.498E+02 1.316E+03 NOT IDENT. NB-94 8.340E-03 3.899E-02 7.890E-02 NOT IDENT. NB-95 l.013E-01 9.653E-01 1.946E+OO NOT IDENT. NB-95M -7.221E-01 2.944E+OO 4.891E+OO NOT IDENT. ZR-95 -9.977E-02 1. 746E+00 3.449E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.945E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1.200E-02 3. 8 61E-02 6.608E-02 NOT IDENT. RH-102 -l.545E-02 7.933E-02 l.354E-01 NOT IDENT. RH-106 1.730E-01 5.784E-01 1.138E+OO NOT IDENT. RU-106 l.730E-01 5.784E-01 1.138E+OO NOT IDENT. AG-108M 2.763E-03 3.302E-02 6.280E-02 NOT IDENT. AG-llOM -7.668E-04 1.217E-01 2.488E-01 NOT IDENT. SN-113 -3.029E-02 2.802E-01 5.205E-01 NOT IDENT. CD-115 O.OOOE+OO 4.226E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 9.991E+04 O.OOOE+OO SHORT HLIF TE-123M 8.356E-02 1.358E-01 2.757E-01 NOT IDENT. SB-124 2.379E+OO 2.789E+OO 6.999E+OO NOT IDENT. SB-125 4.677E-02 1.340E-01 2.598E-01 FAIL ABUN TE-125M 1.899E+02 2.766E+02 5.623E+02 NOT IDENT. I-126 O.OOOE+OO l.277E+06 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO l.384E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.687E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.620E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.346E+26 O.OOOE+OO SHORT HLIF BA-133 4.340E-02 5.521E-02 1. 024E-01 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.339E-02 6.894E-02 1.464E-01 NOT IDENT. CS-135 -2.247E-02 1.666E-01 2.804E-01 NOT IDENT. I-135 O.OOOE+OO l.753E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4 .130E+05 O.OOOE+OO SHORT HLIF CE-139 -5.176E-02 1.197E-01 2.244E-01 NOT IDENT. BA-140
O.OOOE+OO l.443E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 5.563E+05 O.OOOE+OO SHORT HLIF CE-141 5.832E-01 2.697E+Ol 5.232E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 1.757E-01 5.043E-01 7.432E-01 NOT IDENT. PM-144 2.327E-02 5.848E-02 l.240E-01 NOT IDENT. PR-144 3.672E-01 5.332E+OO 1.077E+Ol NOT IDENT. PM-146 -2.107E-02 6.287E-02' l.120E-01 NOT IDENT. ND-147 0.000E+OO 4.209E+07 O.OOOE+OO SHORT HLIF PM-147 2.230E+02 8.008E+02 l.603E+03 NOT IDENT. PM-149 O.OOOE+OO 5.423E+40 O.OOOE+OO SHORT HLIF EU-150 -8 .134E-03 3.563E-02 5.804E-02 FAIL ABUN EU-152 3.350E-03 l .131E-01 2.047E-01 NOT IDENT. GD-153 -4.475E-03 l.671E-01 2.972E-01 NOT IDENT. EU-154 1. 715E-02 1.463E-01 2.940E-01 NOT IDENT. EU-155 7.484E-02 1.040E-01 2.129E-01 FAIL ABUN TB-160 2.176E+OO 2.275E+OO 5.141E+OO FAIL ABUN H0-166M 6.081E-04 5. 596E-02 l.142E-01 FAIL ABUN TM-171 3.640E+OO 5.817E+OO 1. llOE+Ol NOT IDENT. HF-172 1.196E-01 2.625E-Ol
4.800E-01 FAIL ABUN Page 3167of5809 LU-172 8.250E-03 1.091E-01 2.140E-01 FAIL ABUN LU-176 l.038E-02 2.953E-02 5.763E-02 FAIL ABUN HF-181 -1.063E+OO 5.596E+OO l.019E+Ol NOT IDENT. TA-182 9.516E-02 1.177E+OO 2.317E+OO FAIL ABUN RE-183 7.378E-01 1.201E+OO 2.274E+OO NOT IDENT. RE-184 3.078E+Ol 8.280E+Ol NOT IDENT. W-188 -7.409E+Ol 1.425E+02 2.257E+02 FAIL ABUN IR-192 -4.557E-02 5.237E-01 9.865E-01 FAIL ABUN HG-203. 2.099E+OO 2.455E+OO 5.095E+OO NOT IDENT. BI-207 4.081E-04 6.198E-02 1.220E-01 FAIL ABUN BI-2Ll O.OOOE+OO 5.582E-01 8.632E-01 FAIL ABUN PB-211 7.339E-01 7.929E-01 1.593E+OO NOT IDENT. BI-212 1.510E+OO 1.021E+OO 1.580E+OO FAIL ABUN RN-219 -2.732E-01 4.461E-01 7.790E-01 FAIL ABUN RA-223 l.967E-01 6.671E-01 1.302E+OO FAIL ABUN AC-227 -2.352E-02 2.456E-01 *4.663E-01 FAIL ABUN TH-227 -2.352E-02 2.456E-01 4.663E-01 FAIL ABUN TH-231 l.967E-01 6.671E-01 1.302E+OO FAIL ABUN PA-233 2.532E-02 7.518E-02 1.459E-01 FAIL ABUN PA-234 -2*. 915E-02 3.071E-01 5.673E-01 NOT IDENT. PA-234M -2.595E+OO 4.341E+OO 7.673E+OO NOT IDENT. NP-237 2.532E-02 7.518E-02 l.459E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.233E-02 2.332E-01 4.625E-01 NOT IDENT. PU-239 O.OOOE+OO 6.271E+02 6.927E+02 FAIL ABUN AM-241 :-4.753E-02 6.929E-02 1. 089E-01 NOT IDENT. CM-243 -4.333E-02 9.516E-02 l.821E-01 NOT IDENT. BK'....247 5.619E-03 8.955E-02 1.544E-01 FAIL ABUN CM-247 -1. 7 90E-02 4.179E-02 7.468E-02 NOT IDENT. CF-249 4.208E-04 4.683E-02 8.788E-02 NOT IDENT. CF-251 6.306E-02 1.157E-01 2. 341E-01 NOT IDENT. Page 3168of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:13:38.63 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 246 10.66* 8.926E-01 1. 342E+Ol 1.342E+Ol 13. 57 RU-103 497.08 15 91.00* 2.367E+OO 3.686E-02 7.344E+OO 124.44 610.33 148 5.76 1.970E+OO 6.774E+OO 1.350E+03 22.14 CD-109 88.03 139 3.70* 7.449E+OO 2.626E+OO 4.121E+OO 40.24 SN-126 64.28 121 9.60 7.794E+OO 8.387E-01 8.387E-01 72.92 86.94 139 8.90 7.449E+OO 1.092E+OO l.092E+OO 40.24 87.57 139 37.00* 7.449E+OO 2.626E-01 2.626E-01 40.24 BA-137M 661.66 358 89.90* 1.826E+OO 1.132E+OO l.154E+OO 13. 23 CS-137 661.66 358 85.10* 1.826E+OO 1.196E+OO l.219E+OO 13.23 TL-208 277.37 ------6.60 3. 907E+O_O ------Line Not Found ------583.19 110 85.00* 2.050E+OO 3.288E-01 3.288E-01 29.74 860.56 37 12 .50 1.433E+OO 1.085E+OO 1.085E+OO 32.88 PB-210 46.54 86 4.25* 7.552E+OO 1.385E+OO 1.421E+OO 64.95 BI-211 72.87 ------1. 23 7. 711E+OO ------Line Not Found ------351. 06 226 12.92* 3.212E+OO 2.826E+OO 2.826E+OO 20.15 PB-212 74.82 360 10.28 7.683E+OO 2.365E+OO 2.365E+OO 21. 67 77 .11 462 17.10 7.644E+OO 1.836E+OO 1.836E+OO 13.51 238.63 435 43.60* 4.382E+OO 1.184E+OO 1.184E+OO 11. 68 300.09 48 3.30 3.666E+00 2.071E+OO 2. 071E+OO 86.98 BI-214 609.32 148 45.49* 1.970E+OO 8.578E-01 8. 581E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-01 7.035E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO l.177E+OO 37.80 PB-214 74.82 360 5.80 7.683E+OO 4.192E+OO 4.193E+OO 21. 67 77 .11 462 9.70 7.644E+OO 3.237E+OO 3.238E+OO 13. 51 87.09 139 3.41 7.449E+OO 2.849E+OO 2.851E+OO 40.24 242.00 110 7.25 4.345E+OO *l. 812E+OO 1.813E+OO 51. 66 295.22 149 18.42 3.714E+OO 1.133E+OO 1.133E+OO 29.15 351. 93 226 35.60* 3.212E+OO 1. 02 6E+OO 1.026E+OO 20.15 RN-222 609.32 148 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-Ol 7.035E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 RA-224 240.99 110 4.10* 4.345E+OO 3.205E+OO 3.205E+OO 51. 66 RA-226 609.32 148 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 1120 .29 23 14.92 1.127E+OO 7.033E-01 7.035E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 AC-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 74 11. 27 3.319E+OO 1. 031E+OO 1.031E+OO 62.23 794.95 ------4.25 1.543E+OO ------Line Not Found ------835.71 ------1. 61 1.473E+OO ------Line Not Found ------911. 20 61 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 968.97 33 15.80 1.285E+OO 8.493E-01 8.493E-01 56.29 RA-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 74 11. 27 3.319E+OO 1. 031E+OO 1. 031E+OO 62.23 794.95 ------4. 2.5 1.543E+OO ------Line Not Found ------835. 71 ------1. 61 1.473E+OO ------Line Not Found ------911. 20 61 25.80* l.360E+OO 9.074E-01 9. OT4E-01 39.40 968. 97 33 15.80 l.285E+OO 8.493E-01 8.493E-01 56.29 Page 3169 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 360 10.28 7.683E+OO 2.365E+OO 2.365E+OO 21. 67 77 .11 462 17.10 7.644E+OO l.836E+OO 1.836E+OO 13.51 238.63 435 43.60* 4.382E+00 l.184E+OO 1. *184E+OO 11. 68 300.09 48 3.30 3.666E+OO 2.071E+OO 2. 071E+OO 86.98 TH-229 85.43 61 14.70 7.517E+OO 2.864E-01 2.864E-01 107.55 88.47 139 24.00 7.449E+OO 4.049E-01 4.049E-01 40.24 193.51 ------4.41* 5.088E+oo* ------Line Not Found ------210.85 109 4.815E+OO 4.207E+OO 4.208E+OO 41.60 TH-230 609.32 148 45.49* 1.970E+OO 8.578E-01 8.578E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-01 7.033E-01 79.28 1764.49 26 15.30 7.618E-01 l.177E+OO
1.177E+OO 37.80 PA-231 283.69 ------1. 70 3.838E+OO ------Line Not Found ------301.36 48 5.35* 3.666E+OO l.277E+OO 1.277E+OO 86.98 TH-232 105.21 ------1.10 7.028E+00 ------Line Not* Found ------338.32 74 11.27 3.319E+OO 1. 031E+OO 1.031E+OO 62.23 835.71 ------1. 61 l.473E+OO ------Line Not Found ------911.20 61 . 25.80* l.360E+00 9.074E-01 9.074E-01 39.40 968. 97 33 15.80 1.285E+00 8.493E-01 8.493E-01 56.29 TH-234 63. 29 121 *3. 70* 7.794E+OO 2.176E+OO 2.176E+00 *72. 92 92.59 123 4.23 7.325E+OO 2.067E+OO 2.067E+OO 50.15 U-234 609.32 148 45.49* 1.970E+OO 8.578E-01 8.578E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-01 7.033E-01 79.28 1764.49 2.6 15 .. 30 7.618E-01 1.177E+OO 1.177E+OO 37.80 U-235 89. 96 62 3.47 7.393E+OO 1. 264E+OO . 1. 2 64E+OO *75.02 93.35 123 5.60 7.325E+OO 1.562E+OO 1.562E+OO 50.15 143.76 ---...... --10. 96* 6.093E+OO ------Line Not Found ------163.33 ------5.08 5.667E+OO ------Line Not Found ------185.72 134 57.20 5.227E+OO 2.333E-01 2.333E-01 43.44 205.31 ------5.01 4.887E+00 ------Line Not Found ------U-238 *63. 29 121 3.70* 7.794E+OO 2.176E+OO 2.176E+00 72. 92 92.59 123 4.23 7:325E+OO 2.067E+OO 2.067E+00 50.15 AM-243 43.53 ------5.90 7.421E+00 ------Line Not Found ------74.66 360 67.20* 7.683E+OO 3.618E-01 3.618E-01 21. 67 ANH-511 511. 00 89 100.00* 2.313E+00 2.004E-01 2.004E-01 40.73 Flag: "*" Key line Page 3170 of 5809 Summary of Nuclide Activity Sample ID : G405235013 Acquisition date Page : 3 3-0CT-2016 08:10:29 Total number of lines in spectrum 47 Number of unidentified lines 8 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-'214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 39. 26D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1. 41E+10Y 1.41E+10Y 1. 41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 199. 1. 57 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.342E+Ol 3.686E-02 2.626E+OO 2.626E-01 1.132E+OO 1.196E+OO 3.288E-01 l.385E+OO 2.826E+OO 1.184E+OO 8.578E-01 1. 026E+OO 8.578E-01 3.205E+OO 8.578E-01 9.074E-01 9.074E-01 l.184E+OO 4.049E-01 8.578E-01 l.277E+OO 9.074E-01 2.176E+OO 8.578E-01 2.333E-01 2.176E+OO 3.618E-01 2.004E-01 4. 365E+Ol* 4.365E+Ol Decay Corr pCi/GRAM 1.342E+Ol 7.344E+OO 4.121E+OO 2.626E-01 1.154E+OO 1.219E+OO 3.288E-01 1.421E+OO 2.826E+OO 1.184E+OO 8.581E-01 1. 026E+OO 8. 581E-01 3.205E+OO 8. 581E-01 9.074E-01 9.074E-01 1.184E+OO 4.049E-01 8.578E-01 l.277E+OO 9.074E-01 2.176E+00 8.578E-01 2.333E-01 2.176E+OO 3.618E-01 2.004E-01 5.253E+Ol 5.253E+Ol 82.98% Decay Corr 2-Sigma Error 0.182E+Ol 9.139E+OO 1.658E+OO 1.057E-01 0.153E+OO 0.161E+OO 0.978E-01 0.923E+OO 0.570E+OO 0 .138E+OO 1.899E-01 0.207E+00 l.899E-01 1.656E+OO 1. 899E-01 3:575E-01 3.575E-01 0.138E+OO 1. 629E-01 l.899E-01 . 1. lllE+OO 3.575E-01 1.587E+OO 1. 899E-01 1.014E-01 1.587E+OO 0.784E-01 0.816E-01 "M" Manually accepted 2-Sigma %Error 13.57 124.44 40.24 40.24 13. 23 13 .23 29.74 64.95 20.15 11. 68 22.14 20.15 22.14 51. 66 22.14 39.40 39.40 11. 68 40.24 22.14 86.98 39.40 72.92 22.14 43.44 72. 92 21. 67 40.73 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3171 of5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235013 Acquisition date : 3-0CT-2016 08:10:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.25 54 145 0.60 258.74 255 9 1.26E-02 92.2 6.43E+OO T 0 135.60 45 144 2.98 271.43 267 10 1. 06E-02 **** 6.28E+OO T 5 270.18 55 68 2.10 540.52 535 16 1.35E-02 68.2 3.99E+OO T 5 273.53 22 49 1. 62 547.23 535 16 5.36E-03 **** 3.95E+OO T 0 411. 07 22 39 2.23 822.26 816 9 5.52E-03 **** 2.81E+OO T 0 464.00 18 42 1. 57 928.10 924 7 4.68E-03 **** 2.52E+OO T 10 516.70 17 6 1. 53 1033.49 1014 27 4.40E-03 93.1 2.29E+OO 10 519.03 11 3 1.21 1038.16 1014 27 2.88E-03 85.7. 2.28E+OO T 1 521. 78 17 3 1. 51 1043.66 1041 12 4.40E-03 58.0 . 2. 27E+OO T 1 524.48 17 4 1. 81 1049.06 1041 12 4.36E-03 65.1 2.26E+OO 0 636.18 7 17 0.49 1272.45 1267 7 l.93E-03 **** l.89E+OO T 0 728.48 32 21 1. 91 1457.05 1452 12 8.77E-03 69.0 1. 67E+OO T 0 782.60 12 2 1.12 1565.29 1560 9 3.34E-03 72. 6 1.57E+OO T 0 935.83 34 7 4.86 1871. 77 1864 16 9.41E-03 50.4 l.33E+OO 0 952. 71 11 10 0.69 1905.55 1899 10 3.06E-03 **** 1.31E+OO 0 1104 .14 13 21 4.41 2208. 4 7 2198 17 3.55E-03 **** 1.14E+OO 0 1208.19 13 10 1. 54 2416.62 2411 10 3.61E-03 **** 1. 05E+00 0 1211.03 10 0 1. 24 2422.30 2420 6 2.78E-03 63.2 1. 05E+OO 0 1238.66 29 13 1. 50 2477.57 2470 13 8.33E-03 61. 6 1.03E+OO T 0 1378.39 8 4 0.61 2757.12 2752 9 2.18E-03 **** 9.39E-01 Flags: "T" = Tentatively associated Page 3172 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:52.71 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l *
Acquisition date 3-0CT-2016 08:10:29 Sensitivity : .3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.06 Half life ratio : ***** *
Sample date 8-DEC-2015 11:23:00 Nuclide Library : SOLID *
Sample ID G405235013 Analyst initials: MXRl * '* Batch Number *1596247 Sample Quantity : l.4457E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-20l6 06:01:47 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA'. GAMMA] EFF GAM41 CAN. CNF; 3
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 RU-103 CD-109 SN-126 BA-.137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 . RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2. 969E-01 6.283E+OO 7.885E-01 5.018E-02 4.020E-02 4.247E-02 3.232E-02 3.735E-01 4.727E-02 5.365E-02 6.782E-02 5.365E-02 5.067E-01 5.365E-02 l.185E-01 l.185E-01 4.727E-02 4.992E-01 5.364E-02 3.787E-01 1.185E-01 5.007E-01 5.364E-02 1. 882E-01 5.007E-01 3.087E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3173 of 5809 Le (pCi/GRAM 1.353E+Ol 5.087E-02 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 .TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140. CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149* EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3174 of 5809 2. 961E-01 O.OOOE+OO O.OOOE+OO 5.646E-02 3.769E-01 O.OOOE+OO 4.285E-02 5.500E-01 6.995E+OO 2.600E-02 1.442E-01 2.392E+OO 2.403E+OO 0.000E+OO 2.037E-01 O.OOOE+OO O.OOOE+OO 6.561E-01 8.530E+OO 9.009E-01 O.OOOE+OO 1.159E-01 5.6S2E+02 3.530E-02 8.577E-01 2.274E+OO 1.515E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.105E-02 5.988E-02 5.038E-01 5.038E-01 2.841E-02 1.083E-01 2.371E-01 . 0. OOOE+OO O.OOOE+OO 1.291E-01 2.908E+OO 1.189E-01 2.663E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.731E-02 O.OOOE+OO 6.605E-02 l.288E-01 O.OOOE+OO O.OOOE+OO *1. 048E-01 O.OOOE+OO O.OOOE+OO 2.465E+Ol O.OOOE+OO 3.498E-01 5.465E-02 4.747E+OO 5.123E-02 O.OOOE+OO 7.527E+02 O.OOOE+OO 2.673E-02 9.364E-02 l.402E-01 1.255E-01 1.008E-01 2.272E+OO 4.932E-02 5.269E+00 2. 264E-01. 9.378E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NO'T IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. 'NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. . SHORT HLIF FAIL ABUN' NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3175 of 5809 2.666E-02 4.601E+OO l.004E+OO l.082E+OO 3.656E+Ol l.034E+02 4.514E-01 2.348E+OO 5.281E-02 4.143E-01 7:293E-01 7.262E-01 3.512E-Ol 5.983E-01 2.147E-01 2.147E-01 5.983E-01 6.763E-02 2.385E-01 3.158E+OO 6.763E-02 0.000E+OO '2.174E-01 3.282E+02 5.175E-02 8.592E-02 7.120E-02 3.383E_.:.02 4.022E-02 l.091E-01 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:57.96 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l *
Acquisition date 3-0CT-2016 08:10:29 Sensitivity : 3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.06 Half life ratio : ***** * *Sample.date 8-DEC-2015 11:23:00 Nuclide Library: SOLID *
Sample ID G405235013 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity 1.4457E+02 GRAM *
Quantity Err(%) 1.3834E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dty Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM41
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.342E+Ol
2 .119E+OO 2 .119E+OO RU-103 7.344E+OO 8.980E+OO 8.980E+OO CD-109 2.483E+00 1.729E+OO 1. 729E+OO SN-126 1.582E-01 1.099E-01 1.099E-01 BA-137M 1.154E+OO 1. 769E-01 1.769E-01 CS-137 1.219E+OO 1. 868E-01 1.868E-01 TL-208 3.288E-01 9.987E-02 9.987E-02 PB-210 1.421E+OO 9.219E-01 9.219E-01 PB-212 1.184E+OO 1. 759E-01 1. 759E-01 BI-214 8.581E-01 1.998E-01 l.998E-01 PB-214 1. 026E+00 2.207E-01 2.207E-01 RN-222 8.581E-01 1.998E-01 l.998E-01 RA-224 1.202E+OO 1. 743E+OO 1.743E+00 RA-226 8.581E-01 1.998E-01 1.998E-01 AC-228 9.074E-01 3.666E-01 3.666E-01 RA-228 9.074E-01 3.666E-01 3.666E-01 TH-228 1.184E+OO 1. 759E-01 1.759E-01 TH-229 2.255E-01 5.392E-01 5.392E-01 TH-230 8.578E-01 1.997E-01 1.997E-01 PA-231 1.277E+OO 1.126E+OO l.126E+OO TH-232 9.074E-01 3.666E-01 3.666E-01 TH-234 2.176E+OO 1.645E+OO 1.645E+OO U-234 8.578E-01 1.997E-01 1.997E-01 U-235 -2.341E-02 2.042E-01 2.042E-01 U-238 2 .17'6E+OO 1.645E+00 1.645E+OO AM-243 2.641E-01 8.817E-02 8.817E-02 ANH-511 2.004E-01 8.181E-02 8.181E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) BE-7 5.147E+OO 1.533E+Ol 1.550E+Ol NOT IDENT. NA-22 6.027E-03 5.948E-02 5.954E-02 NOT IDENT. NA-24 -1.000E+41 1.029E+41 O.OOOE+OO SHORT HLIF Page 3176of5809 AL-26 -3.212E-02 2.826E-02 3.175E-02 NOT IDENT. SC-46 -3.272E-01 4.148E-01 4.402E-01 FAIL ABUN V-48 1.217E+04 1. 700E+04 l.787E+04 SHORT HLIF CR-51 2.275E+Ol 4.497E+02 4.499E+02 SHORT HLIF MN-54 -5.825E-04 6. 511E-02 6. 511E-02 NOT IDENT. C0-56 -1. 375E-02 4.374E-01 4.375E-01 FAIL ABUN MN-56 -1.000E+41 3.761E+42 0.000E+OO SHORT HLIF C0-57 -1.237E-02 4.739E-02 4.772E-02 FAIL ABUN C0-58 -7.185E-02 6.448E-01 6.456E-01 NOT IDENT. FE-59 -6.747E-01 9.590E+OO 9.595E+OO NOT IDENT. C0-60 -3.631E-02 4.315E-02 4.615E-02 NOT IDENT. ZN-65 -2.634E-01 2.409E-01 2.686E-01 NOT IDENT. GE-68. -1. 572E+OO 3.128E+OO 3.207E+OO NOT IDENT. AS-73 1. 478E+OO 2.692E+OO 2.773E+OO NOT IDENT. AS-74 -3.064E+03 7.213E+03 7.344E+03 SHORT HLIF SE-75 1. 799E-02 2.404E-01 2.405E-01 FAIL ABUN BR-77 2.152E+38 1.863E+39 O.OOOE+OO SHORT HLIF SR-82 -l.024E+02 7.950E+02 7.964E+02 SHORT HLIF RB-83 6.204E-:-Ol 5.302E-01 5.995E-01 FAIL ABUN KR-85 1.119E+Ol 9.582E+00 l.083E+Ol NOT IDENT. SR-85 l.178E+OO 1.012E+OO l.143E+OO NOT I DENT .. RB-86 -2.266E+04 3.708E+04 3.846E+04 SHORT HLIF Y-88 -1. 347E-01 2.058E-01 2.146E-01 NOT IDENT. Y-91 -3.063E+02 8.502E+02 8.613E+02 NOT IDENT. NB-94 8.340E-03 3.900E-02 3.918E-02 NOT IDENT. NB-95 l.013E-01 9.653E-01 9.664E-01 NOT IDENT. NB-95M -7. 221E-01 2.945E+OO .2. 963E+OO NOT IDENT. ZR-95 -9.977E-02 1. 746E+OO 1'. 746E+OO NOT IDENT. NB-97 1.000E+41 2.778E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.000E+41 2.499E+41 O.OOOE+OO SHORT HLIF M0-99 4.076E+31 l.946E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 4.249E+41 O.OOOE+OO SHORT HLIF RH-101 -1.200E-02 3.870E-02 3.907E-02 NOT IDENT. RH-102 -1.545E-02 7.935E-02 7. 966E-02 NOT IDENT. RH-106 1.730E-01 5.786E-01 5.838E-01 NOT IDENT. RU-106 1. 730E-01 5.786E-01 5.838E-01 NOT IDENT. AG-108M 2.763E-03 3.303E-02 3.305E-02 NOT IDENT. AG-llOM -7.668E-04 1. 21*7E-01 l.217E-01 NOT IDENT. SN-113 -3.029E-02 2.802E-01 2.805E-01 NOT IDENT. CD-115 -1.504E+39 4.236E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 1.323E+04 9.993E+04 l.001E+05 SHORT HLIF TE-123M 8.356E-02 1.360E-01 l.411E-01 NOT IDENT. SB-124 2.379E+OO 2.795E+OO 2.994E+OO NOT IDENT. SB-125 4.677E-02 1. 341E-01 1.357E-01 FAIL ABUN TE-125M 1.899E+02 2.774E+02 2.903E+02 NOT IDENT. I-126 1.085E+06 l.288E+06 l.378E+06 SHORT HLIF SB-126 -3.412E+05 1.385E+06 l.394E+06 SHORT HLIF SB-127 4.426E+21 2.755E+22 O.OOOE+OO SHORT HLIF I-131 4.091E+09 5.631E+09 5.925E+09 SHORT HLIF I-132 1.000E+41 l.893E+42 O.OOOE+OO SHORT HLIF TE-132 -1. 311E+26 4.380E+26 O.OOOE+OO SHORT HLIF BA-133 4.340E-02 5.534E-02 5.869E-02 NOT IDENT. I-133 l.000E+41 4.882E+42 O.OOOE+OO SHORT HLIF CS-134 5.339E-02 6.913E-02 7. 321E-02 NOT IDENT. CS-135 -2.247E-02 1.667E-01 1. 670E-01 NOT IDENT. I-135 l.000E+41 6.999E+41 O.OOOE+OO SHORT HLIF CS-136 -3.018E+04 4 .130E+05 4.132E+05 SHORT HLIF CE-139 -5.176E-02 l.202E-01 l.224E-01 NOT IDENT. BA-140 -5.974E+05 1.444E+06 l.469E+06 SHORT HLIF LA-140 -4.657E+05 5.575E+05 5.957E+05 SHORT HLIF. CE-141 5.832E-01 2.697E+Ol 2.697E+Ol NOT IDENT. CE-143 l.OOOE+41 3. 931E+41 0.000E+OO SHORT HLIF CE-144 1.757E-01 5.048E-01 5.109E-01 NOT IDENT. PM-144 2.327E-02 5.853E-02 5.946E-02 NOT IDENT. PR-144 3.672E-01 5.333E+OO 5.335E+OO NOT IDENT. PM-146 -2.107E-02 6.291E-02 6.362E-02 NOT IDENT. ND-147 7.793E+06 4.210E+07 4.224E+07 SHORT HLIF PM-147 2.230E+02 8.012E+02 8.075E+02 NOT IDENT. ' PM-149 1.902E+40 5.441E+40 O.OOOE+OO SHORT HLIF EU-150 -8.134E-03 3.563E-02 3.582E-02 FAIL ABUN EU-152 3.350E-03 l .131E-01 l.132E-01 NOT IDENT. GD-153 -4.475E-03 l.671E-01 l.671E-01 NOT IDENT. EU-154 l.715E-02 1.463E-01 1. 465E-01 NOT IDENT. EU-155 7.484E-02 l.043E-01 1.097E-01 FAIL ABUN TB-160 2.176E+OO 2.289E+OO 2.491E+OO FAIL ABUN H0-166M 6. 081E-04 5. 596E-02 5.596E-02 FAIL ABUN TM-171 3.640E+OO 5.838E+OO 6.064E+OO NOT IDENT. HF-172 l .196E-01 2.635E-01 2.690E-01 FAIL .ABUN Page 3177 of 5809 LU-172 8.250E-03 1. 091E-01 l.091E-01 FAIL ABUN LU-176 1.038E-02 2.955E-02 2.991E-02 FAIL ABUN HF-181 -l.063E+00 5.597E+00 5.618E+OO NOT IDENT. TA-182 9.516E-02 1.177E+OO 1.178E+OO FAIL ABUN RE-183 7.378E-01 1.209E+OO 1.254E+OO NOT IDENT. RE-184 3.078E+Ol 3.824E+Ol 4.067E+Ol NOT IDENT. W-188 -7.409E+Ol *1.429E+02 l.467E+02 FAIL ABUN *IR-192 -4.557E-02 5.237E-01 5.241E-01 FAIL ABUN HG-203 2.099E+OO 2.461E+OO 2.637E+OO NOT IDENT. BI-207 4. 081E-04 6.198E-02 6.198E-02 FAIL ABUN BI-211 2.826E+OO 6.098E-01 1.413E+OO FAIL ABUN PB-211 7.339E-01 7.955E-01 8.616E-01 NOT IDENT. BI-212 1.s10E+oo 1.031E+OO 1.235E+OO FAIL ABUN RN-219 . 732E-01 4.478E-01 4.644E-01 FAIL ABUN RA-223 1. 967E-01 6.673E-01 6.732E-01 FAIL ABUN AC-227 -2.352E-02 2.456E-01 2.458E-01 FAIL ABUN TH-227 -2.352E-02 2.456E-01 2.458E-01 FAIL ABUN TH-231 1. 967E-01 6.673E-01 6.732E-01 FAIL ABUN PA-233 2.532E-02 7.522E-02 7.608E-02 FAIL ABUN PA-234 -2.915E-02 3.090E-:01 3.092E-01 NOT IDENT. PA-234M -2.595E+OO 4.356E+00 4. 511E+OO NOT IDENT. NP-237 2.532E-02 7.522E-02 7.608E-02 FAIL ABUN NP-238 1.000E+41 2.895E+41 O.OOOE+OO SHORT HLIF NP-239 3.233E-02 2.332E-01 2.337E-01 NOT IDENT. PU-239 6.937E+02 6.321E+02 7.053E+02 FAIL ABUN AM-241 -4.7S3E-02 6.959E-02 7.281E-02 NOT IDENT. CM-243 -4.333E-02 9. 531E-02 9.729E-02 NOT IDENT. BK-247' 5.619E-03 8.955E-02 8.959E-02 . FAIL ABUN CM-247 -1. 7 90E-02 4.192E-02 4.269E-02 NOT IDENT. CF-249 4.208E-04 4.683E-02 4.683E-02 NOT IDENT. CF-251 6.306E-02 1.160E-01 l.194E-01 NOT IDENT. Page 3178 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 60.6064 87.09 114.3639 136.47 83.1355 45.60 74.9070 87.57 114. 4384 140.51 0.0000 46.54 79.7381 88.03 114. 5095 143.76 83.7465 49. 72 0.0000 88.34 114.5576 144.24 82.8953 51. 35 130.1865 88.47 114. 5771 145.44 88.3471 51. 87 117.2815 89. 96 114.8056 152.43 88.9463 52.39 93.6784 1093.63 114. 9095 153.25 0.0000 52.97 94. 9655 91.11 0.0000 323.87 65.6973 53.44 98. 6113 92.59 115. 2042 156.02 0.0000 54.07 101.1032 93.35 115. 3178* "158.56 0.0000 57.36 0.0000 94.56 115.4990 159.00 59.6648 57.53 112.4989 94.65 115. 5122 162.33 68.0092 57.98 110.1909 94.67 115. 5150 162.66 0.0000 59.27 105. 6350 . 94.87 84.7611 163.33 73.5167 59.32 129.6541 97.43 92.6535 165.86 76.4147 59.54 148.9184 98.43 88.4496 176.31 70.6969 60. 96 . 136. 4368 98.44 88.4507 176.60 0. 00'00 61.17 136.4847 99.53 78.8997 177.52 52.3886 62.93 123.1975 100 .11 90.8429 181.07 0.0000 63.29 123.2705 102.03 92.7610 181.52 52.5683 63.58 123.3296 103.18 98.8568 184.41 74.8853 64.28 123.4711 103.37 105.6991 143.76 65.7124 66.73 155.5576 105.21 87.1400 193.51 67.9994 67.24 136.2240 105.31 87.1509 197.03 73.7989 125.81 116.8447 106.12 96. 6433 198.01 77. 5964 67.75 116.8572. 106.47 100.9621 201.83 71.2693* 69.67 120.4660 109.28 84 .1300 203.43 69.4819 70.83 159.8222 111. 00 100.6433 205.31 81. 8085 72. 81 150.9000 111.76 0.0000 210.85 57.6076 72. 87 150.9141 114. 06 80.2818 215.65 48.3406 74.66 151.3204 116. 30 0.0000 222 .11 57.1"484 74.82 151.3561 116.74 78.7951 227.09 60.2270 74.97 151. 3899 119.76 79.0622 227.38 62.1521 77 .11 151. 8 685 121.12 73.0903 228.16 0.0000 78.74 118.8120 121. 22 73.0984 228.18 59.3183 79.69 133.8464 121.78 74.8852 116.74 59.3183 80.12 106.6470 122.06 83.6182 235.69 64.9319 80.19 0.0000 122.92 91.5439 235. 96 64.9443 80.57 134.0145 123.07 101.1507 238.63 51.0904 81. 00 142.3745 265.00 85.5117 238.98 0.0000 81. 07 142.3885 125.81 76.0887 240.99 51.1755 81. 75 115. 5944 127.23 89.3429 242.00 51.2122 83.79 115. 9250 127.91 95.9827 244.70 53.7295 84.00 115. 9591 129.30 81. 6389 252.40 0.0000 85.43 116.1876 131.20 73.8871 252.80 44.7820 86.55 114.2803 133.02 71. 3834 254.15 0.0000 86.79 114.3172 133. 52 74.0657 256.23 46.8379 86.94 114. 3409 136.00 83.0953 260.90 0.0000 Page 3179 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.7474 355.39 0.0000 584.27 20.6689 264.80 45.6353 356.01 34.1957 595.83 0.0000 265.00 45.6410 364.49 0.0000 427.87 28.8839 2 68. 22 45.7375 366.42 0.0000 602.52 0.0000 269.46 37.4078 372.51 29.2703 604. 72 17.3572 270.03 37.4217 375.05 34.5428 607.14 27.7959 271. 23 37. 4511 377.52 34. 5872 609.32 15.0683 273.65 0.0000 356.01 36.8037 610.33 15.0741 276.40 41. 5317 388.16 38.9918 614.28 29.6110 277.37 48.9783 388.63 0.0000 618.01 30.2328 277.60 48.9854 391.69 36.9504 620.36 23.2764 278.00 45.1380 264.66 29.6936 . 621. 93 16.3026 279.20 31.6999 401. 81 38.1995 630.19 0.0000 279.54 31. 7070 402.40 38.2104 631.29 22.4336 279.70 34.6831 404.85 24.2296 633.25 25.2554 280.46 32.7167 410.95 27.1799 634.78 0.0000 283.69 45.6986 413.71 27.2167 635.95 21.0667 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 39.7811 423.72 0.0000 645.85 16.7369 285.90 0.0000 427.09 32.2266 657.76 15.5687 287.50 41. 8248 427.87 33.3128 657.90 0.0000 290.67 50.8879 433.94 29.0978 661. 66 27.4590 293.27 0.0000 439.40 22.6898 664.57 0.0000 351. 93 46.5284 453.'88 44.5960 666.33 0. 0000' 295. 96 46.5492 463.37 46.9726 666.50 0.0000 879.38 36.0959 468.07 39.4087 667.71 0.0000 299.98 34.6214 473.00 0.0000 677.62 13. 3598 300.09 34.6235 475.06 47.2176 685.70 0.0000 300.13 34.6249 476.'78 26.3740 695.00 0.0000 301.36 34.6502 477.60 26.3833 696. 49 14.3418 302.85 46.7450 482.18 31.9441 696. 51 17.9272 256.23 52.8290 487.02 0.0000 697.00 0.0060 304.85 0.0000 492.35 0.0000 697.30 20.6219 306.78 44.3366 497.08 29.9331 697.49 22.4167 308.46 56.4853 505.52 21. 6959 702.65 21. 5574 311. 90 47.5039 507.63 0.0000 706.68 17.9883 316.51 40.5387 511.00 21.7459 711. 68 13.5136 319.41 0.0000 514.00 21.7733 720.70 0.0000 320.08 0.0000 514.00 21.7733 721. 93 0.0000 321.04 39.6300 520.40 3.3586 722. 78 16.8779 323.87 37.6594 520.69 0.0000 722.91 17.3613 325.23 45.8377 522.65 0.0000 723.31 18.8106 328.76 0.0000 527.90 0.0000 724.19 18.8157 333.37 35.3058 528.26 18.5323 727.33 21. 7324 333.97 50.6732 529.59 21.3518 733.00 13.0636 334.37 43.0049 529.87 0.0000 735.93 17.2530 338.28 40.0212 531. 02 0.0000 333.97 11. 8106 338.32 40.0220 537.26 0.0000 739.50 0.0000 311. 90 44.6939 546.56 0.0000 747.24 15.4929 340.48 44.6939 552.55 13.6108 748.06 14.5850 3-40. 55 0.0000 563.25 22.7799 752.31 22.8203 344.28 38.3012 569.33 22.8337 753.82 0.0000 345.93 41.7376 946.00 15.9847 756.73 18.2819 351.06 38.2375 569.70 15.9858 756.80 18.2819 351. 93 38.2556 583.19 20.6602 884.68 12.8259 Page 3180 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.4171 1274.44 14.6750 1620.50 4.4641 766.42 15.5868 1001.03 10.7747 1621. 92 4.4653 766.84 14. 6719 1002.74 11. 7 594 1678.03 0.0000 772. 60 0.0000 1004.73 9.8044 1690.97 2.7114 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9150 778.90 10.3086 1028.54 0.0000 1063.66 11. 9063 783.70 0.0000 1037.84 12.8524 1771. 35 3.6643 785.37 10.3291 1038.76 0.0000 1791.20 0.0000 792.07 26.7999 631.29 7.9263 1808.65 4.6082 794.95 10.1745 1048.07 0.0000 1810.72 0.0000 795.86 18.5040 1049.04 11.8967 1836.06 3.7029 810.06 .14.8667 1050.41 15.8682 810.29 13.9384 1063.66 13.9299 344.28 14.8687 1077.00 0.0000 810. 76 13.9407 1077.34 16.9709 815.77 0.0000 1085.87 12.0037 1048.07 0.0000 1093.63 16.0352 832.01 8.4172 1099.45 12.8461 834.85 12.1685 1112. 07 11. 0725 835. 71 13.1075 1112. 84 8.0542 836.80 0.0000 1115. 54 20.7246 846.75 0.0000 1120.29 8.0684 846.77 9.3927 1120.55 8.0688 856.80 0.0000 1221. 41 19.1670 860.56 11.3163 1129. 67 15 .1611 871.09 11. 3503 1131.51 0.0000 873.19 8.5177 1147.95 0.0000 875.33 o. ooo*o 1173.23 7.1465 879.38 9.4809 1177.95 11. 2424 880.51 11. 3804 1189.05 17.4182 883.24 18.0328 1204.77 18.0963 884.68 12.3434 1221.41 13.4158 889.28 15.2114 1231. 02 13.0003 894.76 8.5696 1235.36 0.0000 898.04 10.4834 1238.28 16.5723 900. 72 11. 4448 1260.41 0.0000 903.28 10.4985 1271. 87 8. 3462 911.20 11.4781 1274. "44 10.4382 912.08 11.4807 1274.54 10.4388 923.98 0.0000 1291. 59 6.2860 926.50 8.6446 1298.22 0.0000 92 9. 11 15.3789 1312 .11 0.0000 937.49 6.7434 1332.49 9.5092 944.13 o.ooob 1362.66 0.0000 946.00 10.2992 1365.19 5.3183 949.00 9.2766 1368.63 0.0000 667. 71 0.0000 1384.29 7.4742 962. 31 25.2129 1408.01 2.1455 964.08 18 .1101 1457.56 0.0000 966 .17 13.9781 1460.82 5.4190 911.20 34.1945 1489.16 6.5380 968. 97 34.1.945 1505.03 1. 0929 983.53 0.0000 1584.12 5.5441 984.45 0.0000 1596.21 0.0000 Page 3181of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:14:26.62 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM43.CNF;l51 Background date : Z-OCT-2016 11:02:23. Sample date 8-DEC-2015 10:49:00. Acquisition date : 3-0CT-2016 08:11:15. Sample ID G405235014 Sample quantity 1.53732E+02 GRAM Detector name : GAM43 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.71 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 4 4 0 0 0 3 3 6 6 0 0 0

0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3182of5809 Energy 47.48 62.99* 74.87 76. 92 90.01 . 92.96* 109.22 186.07* 210.28 238.55* 241. 44 266.97 270.06 277.80 295.37* 301.50 337.91 352.00* 434.31 440.31 444.15 463.30 510.77* 583.13* 609.17* 661.58 665.90 695.65 704.04 727.74 754.99 768.76 773.28 794.87 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area-Bkgnd FWHM Channel Left Pw Cts/Sec %Err 53 25 99 173 50 81 21 84 35 415 88 13 26 33 158 36 105 209 20 24 29 31 62 106 136 208 19 17 21 19 54 18 8 28 153 69 168 176 61 149 125 169 153 56 77 30 68 90 77 76 47 50 58 18 22 37 41 -63 46 36 5 23 27 27 20 18 11 6 1. 50 0.84 1. 36 1. 29 0.94 1. 70 1. 34 1. 09 0.58 1. 08 1. 90 1. 36 1. 58 1. 33 1. 26 4.72 1.16 1. 20 4.44 *2. 02 2.03 0.88 2.24 1. 45 1. 43 1. 65 0.61 0.86 0.89 1. 03 8.83 1. 41 1. 41 1. 00 94.74 125.76 149.53 153.64 179.82 185.73 218. 25 372. 01 420.44 476.99 482.76 533.85 540.02 555.51 590.66 602.93 675. 7 6 703.94 868.61 880.60 888.30 926.60 1021.56 1166. 31 1218.40 1323. 25 1331.88 1391. 39 1408.18 1455.59 1510.09 1537.65 1546.69 1589.88 90 124 145 145 178 178 214 366 412 472 472 532 532 549 584 596 670 700 861 876 876 924 1014 1160 1212 1318 1329 1386 1397 1448 1497 1532 1543 1585 13 5 13 13 16 16 9 12 12 18 18 12 12 10 13 13 10 11 16 17 17 8 15 12 13 12 7 12 18 12 27 '11 8 10 l.47E-02 50.3 6.82E-03 56.7 2.74E-02 25.5 4.81E-02 15.3 1. 39E-02 25. 8 2. 24E-02 31. 9 5.70E-03101.0 2.34E-02 33.7 9.81E-03 72.0 1.15E-01 5. 7 2. 43E-02 31. 5 3.68E-03 62.7 7.35E-03 58.9 9.20E-03 56.8 4.40E-02 14.1 9.97E-03 53.3 2.91E-02 15.7 5.80E-02 9.6 5.63E-03 88.1 6.72E-03 42.2 8.07E-03 36.7 8.55E-03 39.5 1. 72E-02 29. 6 2.94E-02 18.1 3.78E-02 13.5 5.79E-02 9.0 5.28E-03 31.7 4.72E-03 62.3 5.95E-03 60.8 5.27E-03 59.4 1.51E-02 26.7 4.98E-03 54.8 2.35E-03 73.9 7.64E-03 26.4 Fit 2.30E+00 1.43E+OO 1. 71E+00 2.44E+00 1.57E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 799.01 9 5 0.56 1598.16 1595 8 2.62E-03 49.7 36 0 821.19 9 12 4.21 1642.52 1635 10 2.46E-03 86.4 37 0 910.92 96 6 1. 79 1822.01 1816 11 2.65E-02 11. 3 38 0 935.10 12 21 0.80 1870.38 1859 14 3.33E-03 86.0 39 0 969. 52 25 44 1. 27 1939.21 1933 14 6.81E-03 61. 6 40 0 1031.64 13 11 0.88 2063.48 2052 15 3.52E-03 64.1 41 0 1050.16 13 9 3.86 2100.52 2094 12 3.59E-03 54.1 42 0 1093.61 31 5 4.87 2187.43 2177 20 8.69E-03. 25.0 43 0 1120.46 40 3 2. 67 2241.12 2235 13 l.lOE-02 18.5 44 0 1155. 98 16 16 0.84 2312.18 2305 13 4.49E-03 56.9 45 0 1197.74 8 13 0.71 2395.70 2387 13 2.32E-03 95.2 46 0 1376.00 20 0 3.21 2752.25 2744 16 5.56E-03 22.4 47 0 1460.53* 335 4 2.38 2921. 30 2913 15 9.30E-02 5.7 48 0 1764.33* 28 0 3.32 3528.90 3522 14 7.82E-03 20.0 49 0 1847.78 9 0 1. 07 3695.78 3692 9 2.50E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 3183 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:14:28 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl . Sample title Sample date Sample ID 8-DEC-2015 10:49:00 G405235014 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:11:15 153.73 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA43 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3184 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.71 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.002E+00 1.481E+Ol l.481E+Ol 11. 33 OK TE-125M 109.28 0.27* 5.555E+OO 8.391E+OO 3 .138E+02 202.05 OK CS-135 268.22 16.00* 4.339E+OO 1. 078E-01 l.078E-01 125.35 OK BA-137M 661.66 89.90* 1. 974E+OO 6.050E-01 6.165E-01 18.01 OK CS-137 661. 66 85.10* 1. 974E+OO 6.391E-01 6.513E-01 18.01 OK PR-144 696. 51 1.34* 1. 892E+OO 3.437E+OO 7 .130E+OO 124.51 OK 1489.16 0.28 9.838E-01 Line Not Found Absent HG-203 70.83 3.69 2.720E+OO Line Not Found Absent 72. 87 6.19 2.941E+OO Line Not Found Absent 279.20 81.56* 4.200E+OO 3.048E-02 2.642E+OO 204.81 OK TL-208 277.37 6.60 4.205E+OO Line Not Found <<INT Reject 583.19 85.00* 2.199E+OO 2.958E-01 2.958E-01 36.14 OK 860.56 12.50 1. 582E+OO Line Not Found Absent PB-210 46.54 4.25* 3.240E-01 2.540E+Ol 2.606E+Ol 100.60 OK PB-212 74*. 82 10.28 3.152E+OO 1.248E+OO 1.248E+OO 80.16 OK 77 .11 17.10 3.363E+OO 1.907E+OO 1.907E+OO 30.68 OK 238.63 43.60* 4.740E+OO 1. 14 7E+OO 1.147E+OO 11. 44 OK 300.09 3.30 3.919E+OO 1.548E+OO 1.548E+OO 106.58 OK BI-214 609.32 45.49*' 2 .118E+OO 7.335E-01 7.337E-01 27.01 OK 1120.29 14.92 1. 2 66E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO l.017E+OO 39.95 OK PB-214 74.82 5.80 3.147E+00 Line Not Found <<INT Reject 77 .11 9.70 3.363E+OO 3.361E+OO 3.362E+OO 30.68 OK 87.09 3.41 4.287E+OO Line Not Found Absent 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.989E+OO 1.205E+OO 1.205E+OO 28 .11 OK 351.93 35.60* 3.425E+OO 9. 411E-01 9.414E-01 19.18 OK RN-222 609.32 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 OK 1120.29 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1. 017E+OO 39.95 OK RA-224 240.99 4.10* 4.697E+OO 4.607E-01 4.607E-01 377.38 OK RA-226 609.32. 45.49* 2.118E+OO 7.335E-Ol 7.337E-01 27.01 OK 1120. 29 14.92 l.266E+OO l.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 l.016E+OO 1. 017E+OO 39.95 OK AC-228 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.550E+OO 1.444E+OO l.444E+00 31. 44 OK 794.95 4.25 1.691E+OO 1.935E+OO 1.935E+OO 52.79 OK 835. 71 1. 61 1. 621E+OO Line Not Found Absent 911. 20 25.80* 1.508E+OO 1.222E+OO 1.222E+OO 22.57 OK 968.97 15.80 1. 431E+OO 5.358E-01 5.358E-01 123.29 OK RA-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.550E+OO 1.444E+OO 1.444E+OO 31. 44 OK 794.95 4.25 1.691E+00 1.935E+OO 1.935E+OO 52.79 OK 835.71 1. 61 1. 621E+OO Line Not Found Absent 911.20 25.80* 1.508E+OO 1.222E+OO 1.222E+OO 22.57 OK 968. 97 15.80 1. 431E+OO 5.358E-01 5.358E-01 123.29 OK TH-228 74.82 10.28 3.152E+OO 1.248E+OO 1.248E+OO 80.16 OK 77 .11 17.10 3.363E+OO 1.907E+OO 1.907E+OO 30.68 OK 238.63 43.60* 4.740E+OO 1.147E+OO 1. 14 7E+OO 11. 44 OK Page 3185of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID G405235014 Acquisition date 3-0CT-2016 08:11:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3.919E+OO 1.548E+OO l.548E+OO 106.58 OK TH-230 609.32 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 OK 1120.29 14.92 l.266E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1.016E+OO 39.95 OK PA-231 283.69 1. 70 4.127E+OO Line Not Found Absent 301.36 5.35* 3.919E+OO 9.549E-01 9.549E-01 106.58 OK TH-232 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.550E+OO 1.444E+OO l.444E+OO 31. 44 OK 835.71 1. 61 l.621E+OO Line Not Found Absent 911.20 25.80* l.508E.f.OO 1.222E+OO 1.222E+OO 22.57 OK 968.97 15.80 l.431E+OO 5.358E-01 5:358E-01 123.29 OK TH-234 63.29 3.70* 1.836E+OO 2.324E+OO 2.324E+00 113. 44 OK 92.59 4.23 4. 722E+OO 2.512E+OO 2.512E+OO 63. 86 OK U-234 609.32 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 OK 1120.29 14.92 1.266E+OO 1. 020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1. 016E+00 1. 016E+00 39.95 OK U-235 89.96 3.47-4.512E+OO 1.994E+OO 1.994E+OO 51. 66 .OK 93.35 5.60 4.722E+OO 1.897E+OO 1.897E+OO 63.86 OK 143.76 10. 96* 6.023E+00 Line Not Found Absent 163.33 5.08 5.876E+OO Line Not Found Absent 185. 72 57.20 5.564E+OO 1.546E-01 1.546E-01 67.36 OK 205.31 5.01 5.260E+OO Line Not Found Absent U-238 63.29 3.70* 1.836E+OO 2.324E+OO 2.324E+OO 113. 44 OK 92.59 4.23 4.722E+OO 2.512E+OO 2.512E+OO 63. 86 OK AM-243 43.53 5.90 l.216E-01 Line Not Found Absent 74.66 67.20* 3.152E+OO 1.910E-01 l.910E-01 80.16 OK ANH-511 511. 00 100.00* 2.466E+OO l.326E-01 1. 32 6E-01 59.16 OK Flag: "*" = Keyline Page 3186of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:14:29.63 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l * *Acquisition date 3-0CT-2016 08:11:15 Sensitivity : 3.00Q *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.71 Half life ratio : ***** *
Sample date 8-DEC-2015 10:49:00 Analyst initials: MXRl *
Sample ID G405235014 Sample Quantity 1.5373E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
Eff. F'ile : DKAlOO: [CANBERRA. GAMMA] EFF GAM43 CAN. CNF; 7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 481E+Ol 1.644E+OO 6.863E-01 TE-125M .3 .138E+02 6.214E+02 5.267E+02 CS-135 l.078E-01 l.324E-01 2. 716E-01 BA-137M 6.165E-01 1.088E-01 7.973E-02 CS-137 6.513E-01 1.150E-01 8.423E-02 PR-144 7 .130E+OO 8.700E+OO 9.976E+OO HG-203 2.642E+OO 5.302E+OO 4.912E+OO TL-208 2.958E-01 l.048E-01 7.283E-02 PB-210 2.606E+Ol 2.569E+Ol 1.890E+Ol PB-212 1.147E+OO l.286E-01 9.376E-02 BI-214 7.337E-01 l.942E-01 l.399E-01 PB-214 9.414E-01 1.770E-01 1.295E-01 RN-222 7.337E-01 *l.942E-01 1.399E-01 RA-224 4.607E-01 1. 704E+OO 1.005E+00 RA-226 7.337E-01 1.942E-01 1.399E-01 AC-228 1.222E+OO 2.702E-01 2.657E-01 RA-228 1.222E+OO 2.702E-01 2.657E-01 TH-228 1.147E+OO
1. 286E-01 9.376E-02 TH-230 7.335E-01 l.942E-01 1.398E-01 PA-231 9.549E-01 9.974E-01 8.322E-01 TH-232 l.222E+OO 2.702E-01 2.657E-01 TH-234 2.324E+OO 2.583E+OO 3.466E+OO U-234 7.335E-01 l.942E:-01 1.398E-01 U-235 -2.352E-02 1. 788E-01 3.515E-01 U-238 2.324E+OO 2.583E+OO 3 .*466E+OO AM-243 1.910E-01 1.500E-01 1.329E-01 ANH-511 1.326E-01 7.689E-02 5.390E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -1.129E+Ol l.462E+Ol 2.444E+Ol NOT IDENT. NA-22 -8.378E-03 4.504E-02 8.932E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF Page 3187of5809 AL-26 -3.236E-02 3.683E-02 5.583E-02 NOT IDENT. SC-46 7.289E-02 3.221E-01 6.806E-01 FAIL ABUN V-48 O.OOOE+OO 1.413E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.006E+02 O.OOOE+OO SHORT HLIF MN-54 -l.942E-02 6.643E-02 l.240E-01 NOT IDENT. C0-56 -9.078E-02 5.059E-01 9.614E-01 NOT I DENT.
MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 3.139E-03 5 .. 206E-02 9.550E-02 NOT IDENT. C0-58 -l.237E-01 5.755E-01 l .101E+OO NOT IDENT. FE-59 4.269E+OO 8.949E+OO 1.651E+Ol NOT IDENT. C0-60 2.219E-02 4. 296E-02 9.516E-02 NOT IDENT. ZN-65 -l.444E-01 2.380E-01 3.342E-01 NOT IDENT. GE-68 5.698E-01 2.104E+OO 4.417E+OO NOT IDENT. AS-73 1.078E+OO 1. 785E+Ol 3.442E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.601E+03 O.OOOE+OO SHORT HLIF SE-75 -1.310E-01 2.388E-01 3.840E-01 NOT IDENT. BR-77 O.OOOE+OO 2.356E+37 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 7.819E+02 0.000E+OO SHORT HLIF RB-83 -1.294E-01 7.147E-01 l.395E+00 NOT IDENT. KR-85 -3.310E+OO 9.208E+OO l.412E+Ol NOT IDENT. SR-85 -3.512E-01 9.735E-01 1.492E+OO NOT IDENT. RB-86 O.OOOE+OO 2.538E+04 O.OOOE+OO SHORT HLIF Y-88 -1.760E-01 1.823E-01 1. 968E-01 NOT IDENT . Y-91 . -2. 612E+02 6.761E+02 1.259E+03 NOT IDENT. NB-94 5.865E-02 6.989E-02 6.659E-02 FAIL ABUN .NB-95 7.046E-01 1.044E+OO 1.992E+OO NOT IDENT. NB-95M -1.012E+OO 2.615E+OO 4.336E+00 NOT IDENT. ZR-95 1.957E+OO 1.629E+OO 3.655E+OO NOT IDENT. NB-97 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 1.583E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.482E+41 O.OOOE+OO SHORT HLIF RH-101 -3.795E-02 4.00lE-02 6.654E-02 NOT IDENT. RH-102 5.154E-02 5.776E-02 1.285E-01 NOT IDENT. RU-103 l.514E+00 5.774E+OO 1.128E+Ol FAIL ABUN RH-106 2. 972E-01 4.719E-01 1.026E+OO FAIL ABUN RU-106 2. 972E-01 4.719E-01 1. 02 6E+00 FAIL ABUN AG-108M 4.241E-02 7.319E-02 6.090E-02 FAIL ABUN CD-109 1.734E+OO 1.563E+OO 2. 901E+O o. NOT IDENT. AG-llOM -l.342E-01 1.085E-01 1.641E-01 NOT IDENT. SN-113 -2.478E-01 2.780E-01 4.697E-01 NOT IDENT. CD-115 O.OOOE+OO 3.293E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 9.876E+04 0.000E+OO SHORT HLIF TE-123M 1.303E-01 1. 351E-01 2.830E-01 NOT IDENT. SB-124 -3.031E-01 2.005E+OO 4 .171E+OO NOT IDENT. SB-125 2.322E-02 1.247E-01 2.148E-01 FAIL ABUN I-126 O.OOOE+OO 9.035E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 1. 424E+06 O.OOOE+OO SHORT HLIF SN-126 O.OOOE+OO 9. 931E-02 1.962E-01 FAIL ABUN SB-127 O.OOOE+OO 2.142E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.700E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.120E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.875E+26 O.OOOE+OO SHORT HLIF BA-133 1.923E-03 4.564E-02 7.799E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.553E-02 l.245E-01 FAIL ABUN I-135 O.OOOE+OO 1.833E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 4.236E+05 O.OOOE+OO SHORT HLIF CE-139 -1.909E-02 1.037E-01 2.027E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 438E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 5.120E+05 O.OOOE+OO SHORT HLIF CE-141 -2.980E+00 2.395E+Ol 4.726E+Ol NOT IDENT. CE-143 O.OOOE+OO 8 .116E+40 0.000E+OO SHORT HLIF CE-144 -8.042E-02 3.852E-01 7.583E-01 NOT IDENT.
PM-144 8.208E-02 l.002E-:-01 l.253E-01 FAIL ABUN PM-146 1. 728E-02 4.907E-02 9.645E-02 NOT IDENT. ND-147 O.OOOE+OO 3.358E+07 O.OOOE+OO SHORT HLIF PM-147 1.955E+02 9.309E+02 1. 727E+03 NOT IDENT. PM-149 .O.OOOE+OO 5.276E+40 O.OOOE+OO SHORT HLIF EU-150 2.285E-03 3.046E-02 5.200E-02 FAIL ABUN EU-152 -6.069E-02 1.084E-01 1. 931E-01 NOT IDENT. GD-153 -8.930E-02 2.365E-01 3.882E-01 NOT IDENT. EU-154 -2.756E-02 1.142E-01 2.231E-01 NOT IDENT. EU-155 2.749E-02 l.236E-01 2.158E-01 NOT IDENT. TB-160 1.175E-01 1.916E+OO 3.810E+OO NOT IDENT. H0-166M -1. 54 7E-02 6.203E-02 1.175E-01 NOT IDENT. TM-171 -1.986E+Ol 4.678E+Ol 7. 968E+Ol NOT IDENT. HF-172 2.189E-01 2.466E-01 4.829E-01 FAIL ABUN Page 3188 of5809 LU-172 O.OOOE+OO 1.244E-01 2. OOlE-01 FAIL ABUN LU-176 -4.830E-03 2.643E-02 4.421E-02 NOT IDENT. HF-181 -l.802E+OO 4.908E+OO 8.702E+OO NOT IDENT. TA-182 9.192E-03 1.077E+OO 2 .130E+OO FAIL ABUN RE-183 3.007E-01 5.700E+OO 1. 096E+Ol NOT IDENT. RE-184 -6 .113E+OO 3.426E+Ol 6*. 457E+Ol NOT IDENT. W-188 -3.102E+Ol 1.259E+02 2.089E+02 FAIL ABUN IR-192 -2.127E-01 4.731E-01 8.620E-01 FAIL ABUN BI-207 1.715E-02 5.288E-02 1. 075E-01 FAIL ABUN BI-211 0.000E+OO 4.875E-01 8.259E-01 FAIL ABUN PB-211 -4.174E-01 6.882E-01 l.202E+OO NOT IDENT. BI-212 7.965E-01 9.276E-01 1.307E+OO FAIL ABUN RN-219 l.993E-01 4.340E-01 8.510E-01 FAIL ABUN RA-223 -2.664E-01 6.167E-01 1.122E+OO FAIL ABUN AC-227 4.542E-02 2.299E-01 4.506E-01 NOT IDENT. TH-227 4.542E-02 2.299E-01 4.506E-01 NOT IDENT. TH-229 6*. 960E-02 4.526E-01' 8.954E-01 FAIL ABUN TH-231 -2.664E-01 6.167E-01 1.122E+OO FAIL ABUN PA-233 2.563E-03 6.297E-02 i.204E-01 FAIL ABUN PA-234 l.054E-01 2.756E-01 5.773E-01 NOT IDENT. PA-234M 1. 875E+OO 5.187E+OO NOT IDENT. NP-237 2.563E-03 6.297E-02 1.204E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 -1.186E-01 2.716E-01 4.776E-01 FAIL ABUN PU-239 1. 003E+02 3.584E+02 6.616E+02 NOT IDENT. AM-241 8.840E-02 2.500E-01 4.899E-01 NOT IDENT. CM-243 3.917E-02 l.137E-01 2.158E-01 FAIL ABUN BK-247 -4.830E-02 8.371E-02. l.341E-01 NOT IDENT. CM-247 1.053E-03 3. 963E-02 7.438E-02 FAIL ABUN CF-249 4.493E-02 4.237E-02 8.790E-02 NOT IDENT. CF-251 5.042E-02 l .112E-01 2.257E-01 NOT IDENT. Page 3189of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:14:27.34 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 324 10.66* l.002E+OO l.481E+Ol 1.481E+Ol 11. 33 TE-125M 109.28 26 0.27* 5.555E+OO 8.391E+OO 3.138E+02 202.05 CS-135 268.22 15 16.00* 4.339E+OO 1.078E-01 l.078E-01 125.35 BA-137M 661.66 220 89.90* 1.974E+OO 6.050E-01 6.165E-01 18.01 CS-137 661.66 220 85.10* l.974E+OO 6.391E-01 6.513E-01 18.01 PR-144 696. 51 18 1. 34* l.892E+00 3.437E+OO 7.130E+OO 124.51 1489.16 ------0.28 9.838E-01 ------Line Not Found ------HG-203 70.83 ------3.69 2.720E+00 ------Line Not Found ------72.87 ------6.19 2.941E+OO ------Line Not Found ------279.20 38 81.56* 4.200E+OO 5.442E-02 4. 716E+OO 113. 61 TL-208 277.37 38 6.60 4.200E+00 6. 725E-01 6.725E-01 113. 61 583.19 113 85.00* 2.199E+OO 2.958E-01 2.958E-01 36.14 860.56 ------12.50 1.582E+OO ------Line Not Found ------PB-210 46.54 72 4.25* 3.240E-01 2.540E+Ol 2.606E+Ol 100.60 BI-211 72. 87 ------1. 23 2.941E+OO ------Line Not Found ------351.06 235 12.92* 3.425E+OO 2.593E+00 2.593E+OO 19.18 PB-212 74.82 128 10.28 3.152E+OO 1.928E+OO 1. 928E+OO 50.94 77 .11 225 17.10 3.363E+OO 1.907E+OO 1.907E+OO 30.68 238.63 486 43.60* 4.740E+00 1.147E+OO 1.147E+OO 11. 44 300.09 41 3.30 3.919E+OO 1.548E+OO 1.548E+OO 106.58 BI-214 609.32 145 45.49* 2 .118Ef00 7.335E-01 7.337E-01 27.01 1120.29 39 14.92 1.266E+OO l.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO 1.017E+OO 39.95 PB-214 74.82 128 5. 80 3.152E+OO 3.418E+OO 3.419E+OO 50.94 77 .11 225 9.70 3.363E+OO 3.361E+OO 3.362E+OO 30.68 87.09 ------3.41 4.287E+OO ------Line Not Found ------242.00 102 7.25 4.697E+OO 1.465E+OO 1.466E+00 62.99 295.22 181 18.42 3.989E+OO 1. 205E+OO 1.205E+OO 28 .11 351. 93 235 35.60* 3.425E+OO 9.411E-01 9.414E-01 19.18 RN-222 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 1120.29 39 14.92 l.266E+OO 1.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 l.016E+OO 1. 017E+OO 39.95 RA-224 240.99 102 4.10* 4.697E+OO 2. 591E+OO 2.591E+OO 62.99 RA-226 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 1120. 29 39 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO l.017E+00 39.95 AC-228 105.21 ------1.10 5.396E+OO ------Line Not Found ------338.32 118 11.27 3.550E+OO 1.444E+OO 1.444E+OO 31. 44 794.95 28 4.25 1. 691E+OO 1.935E+OO 1.935E+OO 52.79 835.71 ------1. 61 1. 621E+OO ------Line Not Found ------911.20 97 25.80* 1.508E+OO 1.222E+OO l.222E+00 22.57 968. 97 25 15.80 1.431E+OO 5.358E-01 5.358E-01 123.29 RA-228 105.21 ------1.10 5 .. 396E+OO ------Line Not Found ------338.32 118 11. 27 3.550E+OO 1.444E+OO 1.444E+OO 31.44 794.95 28 4.25 1.691E+OO 1.935E+OO 1.935E+OO 52.79 835. 71 ------1. 61 1.621E+OO ------Line Not Found ------911.20 97 25.80* l.508E+OO 1.222E+OO l.222E+OO 22.57 Page 3190 of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 25 15.80 1.431E+OO 5.358E-01 5.358E-01 123.29 TH-228 74.82 128 10.28 3.152E+OO 1.928E+OO 1.928E+OO 50.94 77 .11 225 17.10 3.363E+OO 1.907E+OO 1.907E+OO 30.68 238.63 486 43.60* 4 .. 740E+OO 1.147E+OO 1.147E+OO 11. 44 300.09 41 3.30 3.919E+OO 1.548E+00 1.548E+OO 106.58 TH-230 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 1120.29 39 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO 1.016E+OO 39.95 PA-231 283.69 ------1. 70 4.127E+OO ------Line Not Found ------301.36 41 . 5.35* 3.919E+OO 9.549E-01 9.549E-01 106.58 TH-232 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 118 11. 27 3.550E+OO 1.444E+OO 1. 444E+00-31. 44 835. 71 ------1. 61 1. 621E+OO ------Line Not Found ------911. 20 97 25.80* 1.508E+OO 1.222E+OO 1.222E+OO 22.57 968. 97 25 15.80 1. 431E+OO 5.358E-01 5.358E-01 123. 2-9 TH-234 63.29 32 3.70* 1. 836E+OO 2.324E+OO 2.324E+OO 113. 44 92.59 103 4.23 4. 722E+OO 2.512E+OO 2.512E+00 63.86 U-234 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 1120.29 39 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO 1.016E+OO 39.95 U-235 89.96 64 3.47 4.512E+OO 1.994E+OO 1.994E+OO 51. 66 93.35 103 5.60 4.722E+OO 1. 897E+OO 1. 897E+OO 63.86 143.76 ------10.96* 6.023E+OO ------Line Not Found ------163.33 ------5.08 5.876E+OO ------Line Not Found ------185. 72 101 57.20 5.564E+OO l.546E-01 1.546E-01 67. 36 205.31 ------5.01 5.260E+OO ------Line Not Found ------U-238 63.29 32 3.70* 1.836E+OO 2.324E+OO 2.324E+00 113. 44 92.59 103 4.23 4. 722E+OO 2.512E+OO 2.512E+OO 63.86 AM-243 43.53 ------5.90 1.216E-01 ------Line Not Found ------74.66 128 67.20* 3.152E+OO 2.950E-01 2.950E-01 50.94 ANH-511 511. 00 67 100.00* 2.466E+OO 1.326E-01 1.326E-01 59.16 Flag: "*" Key line Page 3191of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Total number of lines in spectrum 49 Number of unidentified lines 10 Number of lines tentatively identified by NID 39 Nuclide Type .. Nuclide K-40 TE-125M CS-135 BA-137M CS-137 PR-144 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222' RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 B-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 57.40D 2.30E+06Y 30.08Y 30.08Y 284.91D 46.59D 1. 41E+10Y 22.20Y 7.04E+08Y 1. 41E+1*oy 1600.00Y 1600. OOY 1600.00Y 1. 41E+l0Y 1600. OOY 1.41E+l0Y 1.41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 37.4 1. 00 1. 02 1. 02 2.07 86.7 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.481E+Ol 8. 391E+OO l.078E-01 6.050E-01 6. 391E-01 3.437E+OO 5.442E-02 2.958E-01 2.540E+Ol 2.593E+OO l.147E+OO 7.335E-01 9.411E-01 7.335E-01 2.591E+OO 7.335E-01 l.222E+OO l.222E+OO l.147E+OO 7.335E-01 9.549E-01 l.222E+OO 2.324E+OO 7.335E-01 l.546E-01 2.324E+OO 2.950E-01 1.326E-01 7.567E+Ol 7.567E+Ol Decay Corr pCi/GRAM l.481E+Ol 3 .138E+02 1. 078E-01 6.165E-01 6.513E-01 7.130E+OO 4. 716E+OO 2.958E-01 2.606E+Ol 2.593E+OO 1.147E+OO 7.337E-01 9.414E-01 7.337E-01 *2. 591E+OO 7.337E-01 1. 222E+OO 1. 222E+OO l.147E+OO 7.335E-01 9.549E-01 l.222E+00 2.324E+OO 7.335E-01 1.546E-01 2.324E+OO 2.950E-01 l.326E-01 3. 901E+02 3.901E+02 79.59% Decay Corr 2-Sigma Error 0.168E+Ol 6.341E+02 l.351E-01 1.llOE-01 l .173E-01. 8.877E+00 5.358E+OO l.069E-01 2. 621E+Ol 0.497E+OO 0 .131E+OO l.982E-01 1. 806E-01 l.982E-01 1.632E+OO l.982E-01 0.276E+OO 0.276E+OO 0.131E+OO 1.981E-01 10.lBE-01 0.276E+OO 2.636E+OO 1. 981E-01 1.041E-01 2.636E+00 1.503E-01 0.785E-01 "M" Manually accepted 2-Sigma %Error 11. 33 202.05 125.35 18.01 18.01 124.51 113.61 36.14 100.60 19.18 11. 44 27.01 19.18 27.01 62.99 27.01 22.57 22.57 11. 44 27.01 106.58 22.57 113. 44 27.01 67.36 113. 44 50.94 59.16 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit . Page 3192of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235014 Acquisition date : 3-0CT-2016 08:11:15 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 210.28 42 181 o.58 420.44 412 12 9. 81E-03 **** 5.18E+OO T 6 270.06 31 78 1. 58 540.02 532 12 7.35E-03 **** 4.30E+OO T 0 434.31 22 64 4.44 868.61 861 16 5.63E-03 **** 2.84E+OO T 2 440.31 27 20 2.02 880.60 876 17 6.72E-03 84.4 2.81E+OO T 2 444.15 32 *24 2.03 888.30 876 17 8.07E-03 73.5 2.79E+OO 0 463.30 34 41 0.88 926.60 924 8 8.55E-03 79.1 2.69E+OO T 0 665.90 20 5 0.61 1331.88 1329 7 5.28E-03 63.4 1. 96E+OO T 0 704.04 22 28 0.89 1408.18 1397 18 5.95E-03 **** 1.87E+OO T 0 727.74 20 28 1. 03 1455.59 1448 12 5.27E-03 **** l.82E+OO T 0 754.99 56 21 8.83 1510.09 1497 27 l.51E-02 53.5 1.77E+OO T 0 768.76 19 19 1. 41 1537.65 1532 11 4.98E-03 **** 1. 74E+OO 0 773.28 9 11 1. 41 1546.69 1543 8 2.35E-03 **** 1.73E+OO T 0 799.01 10 5 0.56 1598.16 1595 8 2.62E-03 99.5 1.68E+OO 0 821.19 9 13 4.21 1642.52 1635 10 2.46E-03 **** 1.65E+OO 0 935.10 12 21 0.80 1870.38 1859 14 3.33E-03 **** 1.48E+OO 0 1031.64 13. 11 0.88 2063.48 2052 15 3.52E-03 **** 1.36E+OO 0 1050.16 13 9 3. 86 2100.52 2094 12 3.59E-03 **** 1. 34E+00 T 0 1093.61 31 5 4.87 2187.43 2177 20 8.69E-03 49.9 1.29E+OO T 0 1155. 98 16 16 0.84 2312.18 2305 13 4.49E-03 **** 1. 23E+OO 0 1197. 74 8 13 0. 71 2395.70 2387 13 2.32E-03 **** 1.20E+00 0 1376.00 19 0 3.21 2752.25 2744 16 5.56E-03 44.7 1. 06E+OO O' 1847.78 8 0 1. 07 3695.78 369'2 9 2.50E-03 66.7 7.98E-01 Flags: "T" == Tentatively associated Page 3193 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:14:41.62 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l *
Acquisition date 3-0CT-2016 Sensitivity 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.71 Half life ratio : ***** *
Sample date 8-DEC-2015 10:49:00 Nuclide Library : SOLID *
Sample ID G405235014 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5373E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************** * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 TE-125M CS-135 BA-137M CS-137 PR-144 HG-203 TL-208 PB-210 PB-2.12 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 . TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.808E-01 2.457E+02 1.258E-01 3.598E-02 3.800E-02 4.433E+OO 2.280E+OO 3.278E-02 8.795E+OO 4.352E-02 6.289E-02 5. 911E-02 6.289E-02 4.667E-01 6.289E-02 1.156E-01 l.156E-01 4.352E-02 6.286E-02 3.832E-01 1.156E-01 1.630E+OO 6.286E-02 1.651E-01 1.630E+00 6.306E-02 2.418E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3194of5809 Le (pCi/GRAM 1.098E+Ol 3.732E-02 O.OOOE+OO 1.978E-02 NOT IDENT. NOT IDENT. SHORT HLJ:F NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99

TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3195of5809 2.880E-01 O.OOOE+OO O.OOOE+OO 5.393E-02 4.186E-01 O.OOOE+OO 4.475E-02 4.739E-01 7.273E+OO 4.076E-02 1.427E-01 1. 866E+00 1.607E+Ol O.OOOE+OO l.767E-01 O.OOOE+OO 0.000E+OO 6.277E-01 6.384E+OO 6.747E-01 O.OOOE+OO 3.998E-02 5.540E+02 2. 968E-02 8. 962E-01 2.017E+OO 1.646E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.121E-02 5.740E-02. 5.046E+OO 4.554E-01 4.554E-01 2.779E-02 1.382E+OO 6.827E-02 2.142E-01 O.OOOE+OO O.OOOE+OO 1.335E-01 1. 580E+OO 9.758E-02 O.OOOE+OO O.OOOE+OO 9.368E-02 O.OOOE+OO O.OOOE+OO O.OOOE+bo O.OOOE+OO 3.554E-02 O.OOOE+OO 5. 611E-02 O.OOOE+OO O.OOOE+OO 9.455E-02 O.OOOE+OO 0.000E+OO 2.218E+Ol O.OOOE+OO 3.573E-01 5.627E-02 4.396E-02 O.OOOE+OO 8 .112E+02 O.OOOE+OO 2.397E-02 8.881E-02 l.825E-01 9.356E-02 l.009E-01 l.650E+OO 5.200E-02 3.695E+Ol 2.273E-01 8.890E-02 FAIL ABUN SHORT HLIF .SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. _NOT I DENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN .FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3196 of 5809 2.019E-02 3.910E+OO 9.356E-01 5.161E+OO 2.816E+Ol 9.609E+Ol 3.939E-01 4.684E-02 3.976E-01 5.410E-01 5.979E-01 3.914E-01 5.141E-01 2.091E-01 2.091E-01 4.187E-01 5.141E-01 5.550E-02 2.503E-01 4.606E+OO 5.550E-02 O.OOOE+OO 2.234E-01 3.122E+02 2.312E-01 l.014E-01 6.175E-02 3.406E-02 4.064E-02 1.058E-01 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:14:46.75 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407' * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l *
Acquisition date 3-0CT-2016 08:11:15 Sensitivity : 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.71 Half life ratio : ***** *
Sample date 8-DEC-2015 10:49:00 Nuclide Library : SOLID *
Sample ID G405235014 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5373E+02 GRAM *
Quantity Err ( % ) : 1. 3010E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. 'date 6-SEP-2016 07: 25: 20 Eff. Geometry' : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activit'y Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.481E+Ol 1.817E+00 1.817E+OO TE-125M 3 .138E+02 6.217E+02 6.217E+02 CS-135 1.078E-01 1.326E-01 1.326E-01 BA-137M 6.165E-01 1.120E-01 1.120E-01 CS-137 6.513E-01 1.183E-01 1.183E-01 PR-144 7.130E+OO 8.705E+OO 8.705E+OO HG-203 2.642E+OO 5.308E+OO 5.308E+OO TL-208 2.958E-01 1.055E-01 1.055E-01 PB-210 2.606E+01 2.580E+Ol 2.580E+Ol PB-212 1.147E+OO l.425E-01 1.425E-01 BI-214 7.337E-01 1. 968E-01 1. 968E-01 PB-214 9.414E-01 1.814E-01 1.814E-01 RN-222 7.337E-01 1. 968E-01 1.968E-01 RA-224 4.607E-01 1.710E+OO 1.710E+OO RA-226 7.337E-01 1. 968E-01 1. 968E-01 AC-228 1.222E+OO 2.774E-01 2.774E-01 RA-228 1.222E+00 2.774E-01 2.774E-01 TH-228 1.147E+OO 1.425E-01 1.425E-01 TH-230 7.335E-01 1. 967E-01 1. 967E-01 PA-231 9.549E-01 l.018E+OO 1.018E+OO TH-232 1.222E+OO 2.774E-01 2.774E-01 TH-234 2.324E+OO 2.635E+00 2.635E+OO U-234 7.335E-01 1. 967E-01 1. 967E-01 U-235 -2.352E-02 1. 788E-01 1. 788E-01 U-238 2. 32'4E+OO 2.635E+OO 2.635E+OO AM-243 1.910E-01 1. 511E-01 l.511E-01 ANH-511 1.326E-01 7.708E-02 7.708E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.129E+01 1.463E+Ol 1.549E+Ol NOT IDENT. NA-22 -8.378E-03 4.504E-02 4.520E-02 NOT IDENT. NA-24 1.000E+41 7.300E+41 O.OOOE+OO SHORT HLIF Page 3197of5809 AL-26 -3.236E-02 3.689E-02 3. 967E-02 NOT IDENT. SC-46 7.289E-02 3.221E-01 3.238E-01 FAIL ABUN V-48 -9.700E+02 1. 413E+04 l.414E+04 SHORT HLIF CR-51 3.430E+02 4.009E+02 4.296E+02 SHORT HLIF MN-54* -1.942E-02 6.643E-02 6.701E-02 NOT IDENT. C0-56 -9.078E-02 5.059E-01 5.076E-01 NOT IDENT. MN-56 -1.000E+41 5.573E+41 O.OOOE+OO SHORT HLIF C0-57 3.139E-03 5.206E-02 5.208E-02 NOT IDENT. C0-58 -1.237E-01 5.755E-01 5.782E-01 NOT IDENT. FE-59 4.269E+OO 8.955E+OO 9.159E+OO NOT IDENT. C0-60 2.219E-02 4. 296E-02 4.411E-02 NOT IDENT. ZN-65 -1.444E-01 2.381E-01 2.468E-01 NOT IDENT. GE-68 5.698E-01 2.104E+00 2.120E+OO NOT IDENT. AS-73 l.078E+OO 1. 786E+Ol 1.786E+Ol NOT IDENT. AS-74 4.392E+03 6. 611E+03 6.902E+03 SHORT HLIF SE-75 -l.310E-01 2.389E-01 2.460E-01 NOT IDENT. BR-77 2.101E+38 l.819E+39 0.000E+OO SHORT HLIF SR-82 4.516E+02 7.822E+02 8.082E+02 SHORT HLIF RB-83 -l.294E-01 7.149E-01 7.173E-01 NOT IDENT. KR-85 -3.310E+OO 9.209E+OO 9.329E+OO NOT IDENT. SR-85 -3.512E-01 9.736E-01 9.864E-01 NOT IDENT. RB-86 6.876E+03 2.538E+04 2.557E+04 SHORT HLIF Y-88 -1. 7 60E-01 l.827E-01 1.992E-01 NOT IDENT. Y-91 -2.612E+02 6.762E+02 6.864E+02 NOT IDENT. NB-94 5.865E-02 6.993E-02 7.476E-02 FAIL ABUN NB-95 7.046E-01 l.044E+OO 1.091E+OO NOT IDENT. NB-95M -1.012E+OO 2.616E+OO 2.656E+OO NOT IDENT. ZR-95 *1. 957E+OO 1.632E+OO 1.855E+OO NOT IDENT. NB-97 1.000E+41 5.763E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 3.376E+41 0.000E+OO SHORT HLIF M0-99 -4.810E+30 1.583E+32 O.OOOE+OO SHORT HLIF TC-99M -1. OOOE+41 l.485E+41 O.OOOE+OO SHORT HLIF RH-101 -3.795E-02 4.059E-02 4.405E-02 NOT IDENT. RH-102 5.154E-02 5.791E-02 6.240E-02 NOT IDENT. RU-103 1.514E+OO 5.775E+OO 5.815E+OO FAIL ABUN RH-106 2.972E-01 4. 723E-01 4.909E-01 FAIL ABUN RU-106 2.972E-01 4. 723E-01 4.909E-01 FAIL ABUN AG-108M 4.241E-02 7.321E-02 7.567E-02 FAIL ABUN CD-109 1. 734E+OO 1. 570E+OO 1.754E+OO NOT IDENT. AG-llOM -l.342E-01 1.087E-01 l.244E-01 NOT IDENT. SN-113 -2.478E-01 2.782E-01 2.997E-01 NOT IDENT. CD-115 3.730E+38 3.293E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 9. 717E+04 9.943E+04 l.087E+05 SHORT HLIF TE-123M 1.303E-01 1.352E-01 1.474E-01 NOT IDENT. SB-124 -3.031E-01 2.005E+OO 2.009E+OO NOT IDENT. SB-125 2.322E,02 l.247E-01 l.251E-01 FAIL ABUN I-126 1.455E+06 9.248E+05 l.134E+06 SHORT HLIF SB-126 -7.524E+05 l.431E+06 l.470E+06 SHORT HLIF SN-126 1.998E-01 1.00lE-01 1.347E-01 FAIL ABUN SB-127 6. 591E+21 2.326E+22 0.000E+OO SHORT HLIF I-131 -3.823E+08 4.700E+09 4.703E+09 SHORT HLIF I-132 l.OOOE+41 l.852E+42 O.OOOE+OO SHORT HLIF TE-132 -1.155E+26 3.904E+26 O.OOOE+OO
SHORT HLIF BA-133 1.923E-03 4.564E-02 4.565E-02 FAIL ABUN I-133 -l.OOOE+41 7.635E+41 O.OOOE+OO SHORT HLIF CS-134 1.267E-01 6.575E-02 8.708E-02 FAIL ABUN I-135 -1.000E+41 7.020E+41 O.OOOE+OO SHORT HLIF CS-136 -1. 299E+04 4.236E+05 4.236E+05 SHORT HLIF CE-139 -l.909E-02 l.037E-01 l.041E-01 NOT IDENT. BA-140 3.127E+05 1.438E+06 l.445E+06 SHORT HLIF LA-140 -6.102E+05 5.128E+05 5.819E+05 SHORT HLIF CE-141 -2.980E+OO 2.395E+Ol 2.399E+Ol NOT IDENT. CE-143 1.000E+41 8.180E+40 O.OOOE+OO SHORT HLIF CE-144 -8.042E-02 3 .. 852E-01 3.870E-01 NOT IDENT. PM-144 8.208E-02 l.003E-01 l.069E-01 FAIL ABUN PM-146 1. 728E-02 4.909E-02 4.970E...:02 NOT IDENT. ND-147 -4.681E+06 3.358E+07 3.364E+07 SHORT HLIF PM-147 l.955E+02 9.309E+02 9.351E+02 NOT IDENT. PM-149 -1.248E+40 5.284E+40 O.OOOE+OO SHORT HLIF* EU-150 2.285E-03 3.046E-02 3.048E-02 FAIL ABUN EU-152 -6.069E-02 l.085E-01 l .119E-01 NOT IDENT. GD-153 -8.930E-02 2.365E-01 2.399E-01 NOT IDENT. EU-154 -2.756E-02 l.142E-01 l.149E-01 NOT IDENT. "EU-155 2.749E-02 1.236E-01 l.242E-01 NOT IDENT. TB-160 1.175E-01 l.916E+OO l.916E+OO NOT IDENT. H0-166M -l.547E-02 6.204E-02 6.243E-02 NOT IDENT. TM-171 -1. 98 6E+Ol 4.682E+Ol 4.767E+Ol NOT IDENT. HF-172 2.189E-01 2.492E-01 2.680E-01 FAIL ABUN Page 3198 of 5809 LU-172 2.541E-01 1.270E-01 1.710E-01 FAIL ABUN LU-176 -4.830E-03 2.643E-02 2.652E-02 NOT IDENT. HF-181 -1.802E+OO 4.908E+OO 4.975E+OO NOT IDENT. TA-182 9.192E-03 1.077E+OO 1.077E+OO FAIL ABUN RE-183 3.007E-01 5.700E+OO s.702E+oo* NOT IDENT. RE-184 -6 .113E+OO 3.429E+Ol 3.440E+Ol NOT IDENT. W-188 -3.102E+Ol 1.259E+02 l.267E+02 FAIL ABUN IR-192 -2.127E-01 4.732E-01 4.828E-01 FAIL ABUN BI-207 l.715E-02 5.288E-02 5.344E-02 FAIL ABUN BI-211 2.593E+OO 5.013E-01 1. 272E+OO FAIL ABUN PB-211 -4.174E-01 6.886E-01 7.138E-01 NOT IDENT. BI-212 7. 965E-01 9.284E-01 9.955E-01 FAIL ABUN RN-219 l.993E-01 4.347E-01 4.439E-01 FAIL ABUN RA-223 -2.664E-01 6.169E-01 6.285E-01 FAIL ABUN AC-227 4.542E-02 2.300E-01 2. 30,9E-01 NOT IDENT. TH-227 4.542E-02 2.300E-01 2.309E-01 NOT IDENT. TH-229 6. 960E-02 4.527E-01 4.537E-01 FAIL ABUN
TH-231 -2.664E-01 6.169E-01 6.285E-01 FAIL ABUN PA-233 2.563E-03 6.297E-02 6.298E-02 FAIL ABUN PA-234 1.054E-01 3.009E-01 3.046E-01 NOT IDENT. PA-234M 1. 875E+00 5.188E+00 5.256E+OO NOT IDENT. NP-237 2.563E-03 6.297E-02 6.298E-02 FAIL ABUN NP-238 -1.000E+41 2.329E+41 O.OOOE+OO SHORT HLIF NP-239 -l.186E-01 2.717E-01 2.770E-01 FAIL ABUN PU-239 l.003E+02 3.585E+02 3.613E+02 NOT IDENT. AM-241 8.840E-02 2.SOlE-01 2.533E-01 NOT IDENT. CM-243 3.917E-02 1.137E-01 1.151E-01 FAIL ABUN BK-247 -4.830E-02 8.428E-02 8.704E-02 NOT IDENT. CM-247 l.053E-03 3. 963E-02 3. 963E-02 FAIL ABUN CF-249 4.493E-02 4.253E-02 4.710E-02 NOT IDENT. CF-251 5.042E-02 l .113E-01 1.136E-01 NOT IDENT. Page 3199of5809
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************** ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 64.4058 87.09 95.1059 136.47 89.5901 45.60 81. 3972 87.57 82.9171 140.51 0.0000 46.54 60.1935 88.03 96.8296 143.76 79.5716 49.72 0.0000 88.34 96.8917 144.24 76.2396 51. 35 58.9820 88.47 96.9174 145.44 81. 4648 51. 87 66.1055 89.96 106.4733 152.43 81. 4309 52.'39 61. 9809 1093.63 82.2839 153.25 0.0000 52.97 64.9081 91.11 0.0000 323.87 *77. 3383 53.44 61.4644 92.59 82.6084 156.02 0.0000 54.07 64.7612 93.35 82.7340 158.56 0.0000 57.36 0.0000 94.56 82.9328 159.00 68.3382 57.53 80.4045 94.65 82.9474 162.33 67.7803 57.98 85.8707 94.67 82.9507 162.66 0.0000 59.27 90.4818 94.87 82.9837 163.33 65.2611 59.32 82.9528 97.43 90.8392 165.86 68.9747 59.54 84.0801 98.43 73.7531 176.31 58.4133 60. 96 83.6789 98.44 '73.7545 176.60 0.0000 61.17 83.7255 99.53 90.8130 177.52 63.8218 62.93 90.2769 100 .11 81.4679 181.07 0.0000 63.29 82.7403 102.03 91. 2436 181.52 74.8339 63.58 81. 3498 103.18 72.4389 184.41 79.5725 64.28 94.5941 103.37 72.4650 143.76 79.7011 66.73 91.1561 105.21 63.5730 193.51 65.9907 67.24 86.8734 105.31 63.5844 197.03 70.8041 125.81 92.4729 106.12 90.7423 198.01 78.1562 67.75 92.4883 106.47 90.8003 201.83 73.0265 69.67 113. 9450 109.28 64.8439 203.43 92.1826 70.83 90.2279 111. 00 77.0874 205.31 83.8582 72.81 98.0849 111.76 0.0000 210.85 58.0999 72.87 98.0990 114. 06 79.9234 215.65 64.9001 74.66 115.3021 116. 30 0.0000 222 .11 72.8267 74.82 115.3446 116.74 81. 5095 227.09 70 .3987 74.97 115.3846 119.76 61.1397 227.38 69.4811 77 .11 115.9520 121.12 74.7598 228.16 0.0000 78.74 100.9369 121. 22 74.7724 228.18 62 .. 0220 79.69 87.5635 121.78 72.3879 116.74 62.0220 80 .. 12 84.6249 122.06 72.4217 235.69 69.6121 80.19 0.0000 122.92 83.5878 235.96 73.8947 80.57 114. 9618 123.07 71.3128 238.63 56:0477 81. 00 122.6412 265.00 78.7690 238.98 0.0000 81. 07 122.6602 125.81 62.9874 240.99 56.1822 81. 75 108.0564 127.23 102.7431 242.00 56.2398 83.79 93.6820 127.91 86.7462 244.70 40.1436 84.00 99.4395 129.30 85. 6962 252.40 0.0000 85.43 173.1168 131. 20 10*8. 3770 252.80 52.0285 86.55 90.7850 133. 02 93.6951 254.15 0.0000 86.79 98.1120 133.52 94.1851 256.23 51. 2351 86.94 98.1432 136.00 92.0359 260.90 0.0000 Page 3200 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 57.0087 355.39 0.0000 584.27 26.1571 264.80 58.4790 356.01 34.7261 595.83 0.0000 265.00 58.4900 364.49 0.0000 427.87 30.2205 268.22 52.8003 366.42 0.0000 602.52 0.0000 269.46 52.8607 372. 51 38.3489 604. 72 33.7700 270.03 52.8893 375.05 42.6880 607.14 32.3404 271.23 61. 7734 377.52 37.4189 609.32 26.6724 273.65 0.0000 356.01 35.4405 610.33 26.6857 276.40 60. 0965 388.16 31.2403 614.28 29.5039 277.37 60.1499 388.63 0.0000 618.01 25.8629 277.60 60.1623 391. 69 52.9159 620.36 24.9681 278.00 62.1579 264.66 40.2068 621.93 13.8817 279.20 56.2996 401.81 35.8883 630.19 0.0000 279.54 54.8349 402.40 39.1663 631.29 13.0152 279.70 54.8428 404.85 37.0526 633.25 26.9848 280.46 68.2293 410.95 32.8290 634.78 0.0000 283.69 56.5280 413.71 51.5277 635.95 13.0443 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 59.5947 423.72 0. 0000* 645.85 18. 7219 285.90 0.0000 427.09 24.3342 657.76 18.0738 287.50 52.7391 427.87 29.8801 657.90' 0.0000 290.67 4.9. 3953 433.94 28.3316 661. 66 28.6688 293.27 0.0000 439.40 6.6897 664.57 0.0000 351. 93 36.0667 453.88 27.0049 666.33 0.0000 295.96 36.0901 463.37 28.8618 666.50 0.0000 879.38 24 .1143 468.07 25. 5396 667. 71 0.0000 299.98 45.2692 473.00 0.0000 677.62 14.2497 300.09 45.2737 475.06 28.4973 685.70 0.0000 300 .13 45.2747 476.78 29.6679 695.00 0.0000 301.36 45.3223 477.60 38.8158 696.49 21. 4601 302.85 34.7913 482.18 32.0537 696. 51 21.4601 256.23 36.3552 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.3340 306.78 40.9787 497.08 20.7872 697.49 15.3354 308.46 45.5960 505.52 26.1108 702.65 16.9077 311. 90 45.7278 507.63 0.0000 706.68 13.8582 316.51 45.9027 511. 00 25.6105 711.68 23.1475 319.41 0.0000 514.00 36.7321 720.70 0.0000 3*20. 08 0.0000 514.00 36.7321 721. 93 0.0000 321.04 34. 8114 520.40 29.8434 722. 78 12.4047 323.87 48.2326 520.69 0.0000 722. 91 12.4055 325.23 48.2852 522.65 0.0000 723. 31 13. 9583 328.76 0.0000 527.90 0.0000 724 .19 15.5151 333.37 40.3282 528.26 24.6846 727. 33 24.2752 333.97 .45.0027 529.59 23.8203 733.00 18.1694 334.37 40.3600 529.87 0.0000 735.93 17,5424 338.28 52.9413 531. 02 0.0000 333.97 17.5540 338.32 52.9434 537.26 0.0000 739.50 0.0000 311. 90 43.6740 546.56 0.0000 747.24 15.6680 340.48 43.6740 552.55 23.2261 748.06 25.0773 340.55 0.0000 563.25 26.9522 752.31 12.7572 344.28 55.2752 569.33 28.8403 753.82 0.0000 345.93 *45. 94 7 0 946.00 28.8428 756.73 12.7806 351.06 44. 0311 569.70 27.0428 756.80 12.7810 351. 93 36. 7168 583.19 27.2324 884.68 15.7769 Page 3201of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 17.3680 1274.44 17.1860 1620.50 5.0767 766.42 22 .1102 1001.03 17.2129 1621.92 4.0625 766.84 20.5347 1002.74 17.2227 1678.03 0.0000 772.60 0.0000 1004.73 20.4652 1690.97 4.1234 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.1403 778.90 14.7397 1028.54 0.0000 1063.66 3.4933 783.70 0.0000 1037.84 11. 97 62 1771.35 1.4975 785.37 14.9203 1038.76 0.0000 1791.20 0.0000 792.07 15.9580 631. 29 17.4688 1808.65 7.3931 794.95 11.1836 1048.07 0.0000 1810.72 0.0000 795.86 0.0000 1049.04 17.4824 1836.06 4.2477 810.06 18.0813 1050.41 17.4902 810.29 18.0829 1063.66 12.0742 344.28 18.0840 1077.00 0.0000 810.76 15.0719 1077.34 7.7165 815.77 0.0000 1085.87 21.2215 1048.07 0.0000 1093.63 15.5107 832.01 13.1702 1099.45 12.4312 834.85 18.2554 1112. 07 13.3696 835.71 18.2615 1112. 84 11.1444 836.80 0.0000 1115. 54 19.6292 846.75 0.0000 1120.29 14.5203 846.77' 17.3201 1120.55 14.5211 856.80 0.0000 1221.41 14.5242 860.56 19.4581 1129. 67 16.8008 871.09 18.5065 1131. 51 0.0000 873.19 15.4340 1147.95 0.0000 875.33 0.0000 1173.23 9.9833 879.38 13.4066 1177.95 19.0846 880.51 13. 4122 1189.05 12.5361 883.24 14.4584 1204.77 *22.8943 884.68 21. 6985 1221.41 17.4813 889.28 8.2800 1231. 02 17.5277 894*. 76 13.4820 1235.36 0.0000 898.04 16.6128 1238.28 11. 0924 900. 72 18.7075 1260.41 0.0000 903.28 17.6843 1271.87 6.5304 911.20 15.0223 1274.44 11.2025 912.08 16.6963 1274.54 10.2690 923.98 0.0000 1291.59 11.2541 926.50 10.0690 1298.22 0.0000 929 .11 10.0784 1312 .11 0.0000 937.49 18. 5313 1332.49 7.5836 944.13 0.0000 1362.66 0.0000 946.00 10.5603 1365.19 8.6036 949.00 19.0278 1368.63 0.0000 667. 71 0.0000 1384.29 5.3366 962. 31 24.2732 1408.01 9.6631 964.08 20.4018 1457.56 0.0000 966 .17 11. 9092 1460.82 6.8517 911.20 22.3516 1489.16 4. 92 72 968.97 22.3516 1505.03 10.8802 983.53 0.0000 1584.12 4.0287 984.45 0.0000 1596.21 0.0000 Page 3202 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:15:15.21 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 8-DEC-2015 10:56:00. Acquisition date': 3-0CT-2016 08:11:39. Sample ID G405235015 Sample quantity 1.45075E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.75 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 .6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 0 0 0 4 4 0 0 2 2 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 Page 3203 of 5809 Energy 62 .. 79* 74.99 77.15* 87.17 93.06* 99.51* 185.90* 209.20 238.73* 241.60 271. 00 284.47 295.41 299.91 321.84 338.37 351.83* 414.86 482.23 511.09* 516.88 525.75 583.28* 609.36* 661.95 669.81 727. 83 738.40 768.61 772.60 794.46 861.16 871. 28 911.36* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 60 79 140 38 58 31 102 26 365 113 23 43 91 21 37 70 241 15 12 64 21 19 120 155 78 10 17 5 27 8 35 37 26 73 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 131 138 118 144 181 187 114 70 63 88 74 79 56 56 40 82 48 37 21 23 4 7 33 35 40 26 25 10 23 13 7 15 13 24 1. 00 1. 07 1. 07 1. 06 1. 03 3. 3'3 0. 96 0.93 1.15 1. 78 1. 46 3. 86 1. 42 1. 56 0.98 1. 05 1.19 2.38 1. 49 2.12 1. 80 1. 81 1. 30 1. 35 1.17 4.82 1. 36 0.89 1. 71 1. 38 1. 26 0.64 6.59 1. 06 126.04 150.43 154.76 174.81 186.60 199.50 372.34 418. 96 478.06 483.80 542.61 569.57 591.47 600.46 644.35 677 .-42 704.35 830.48 965. 28 1023.03 1034.63 1052.37 1167. 51 1219.70 1324.93 1340.67 1456.78 1477.92 1538.38 1546.37 1590.12 1723.62 1743.86 182'4. 08 122 147 147 172 183 193 366 416 472 472 536 562 587 *587 640 673 698 823 959 1015 1031 1031 1162 1213 1319 1330 1451 1474 1529 1543 1584 1714 1734 1819 9 1.68E-02 37.0 13 2.18E-02 25.3 1.29E+OO 13 3.89E-02 15.4 7 l.06E-02 54.1 10 1.60E-02 46.7 12 8.49E-03 92.2 12 2.83E-02 23.7 7 7.09E-03 57.9 19 1.0lE-01 6.5 1.12E+OO 19 3.14E-02 24.2 9 6.29E-03 71.7 15 1.20E-02 47.4 18 2.53E-02 17.9 1.56E+OO 18 5.84E-03 69.0 10 l.03E-02 36.0 11 1. 95E-02 27. 4 11 6.71E-02 8.6 10 4.05E-03 82.7 10 3.27E-03 80.2 16 1.76E-02 25.5 25 5.80E-03 29.6 1.60E+OO 25 5.21E-03 30.7 10 3.33E-02 13.0 15 4.31E-02 11.6 12 2.18E-02 19.2 12 2.80E-03107.3 10 4.66E-03 60.9 6 1.25E-03116.5 13 7.49E-03 41.3 7 2.35E-03 76.9 13 9.79E-03 22.5 20 1.03E-02 30.5 18 7.15E-03 38.8 11 2.02E-02 18.0 Peak Searc.h Report (continued) Page : 2 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Pk It. Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 923.46 11 5 0.59 1848.31 1845 7 3.07E-03 45.4 36 5 964. 70 22 5 2.91 1930.84 1926 18 6.07E-03 27.5 1.67E+OO 37 5 968.96* 44 5 1. 74 1939.36 1926 18 1. 23E-02 20.0 38 0 1005.15 8 12 0.92 2011. 81 2008 8 2.22E-03 82.9 39 *o 1039.30 7 14 0.97 2080.16 2071 11 2.02E-03105.3 40 0 1041. 21 13 1 1. 51 2083.97 2081. 6 3.50E-03 32.0 41 0 1084.19 13 14 0.73 2170.00 2162 14 3.61E-03 67.1 42 0 1095.28 7 7 0.98 2192. 21. 2188 6 l.84E-03 76.1 43 0 1098.49 16 4 3.22 2198.64 2194 10 4.44E-03 35.6 44 0 1120.70 34 30 1. 56 2243.09 2237 15 9.44E-03 39.1 45 0 1154. 44 16 8 2.34 2310.63 2305 11 4.45E-03 42.6 46 0 1223.88 9 11 0.65 2449.62 2444 9 2.51E-03 74.6 47 0 1333.06 9 6 2.33 2668.18 2661 11 2.36E-03 63.5 48 0 1460.73* 384 4 2.05 2923.76 2915 16 1.07E-01 5.3 49 0 1764.90 24 2 2.03 3532. 71 3528 11 6.61E-03 24.4 Flag: "*" = Peak area was modified by backgroun0 subtraction Page 3204 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:15:17 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 10:56:00 G405235015 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:11:39 145.07 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA44 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3205 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 'AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.75 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 030E+OO 1. 738E+Ol 1.738E+Ol 10.57 OK CD-109 88.03 3.70* 4.453E+OO 8.036E-01 1.261E+OO 202.07 OK SN-126 64.28 9.60 1.986E+OO 2.070E+OO 2.070E+OO 73. 96 OK 86.94 8.90 4.453E+OO 3.341E-01 3.341E-01 202.07 OK 87.57 37.00* 4.453E+OO 8.036E-02 8.036E-02 202.07 OK BA-137M 661. 66 89.90* 1. 965E+OO 2.384E-01 2.430E-01 38.33 OK CS-137 661. 66 85.10* 1. 965E+OO 2.519E-01 2.567E-01 38.33 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent 583.19 85.00* 2.178E+OO 3.520E-01 3.520E-01 26.04 OK 860.56 12.50 1. 591E+OO 9.740E-01 9.740E-01 60.95 OK BI-211 72.87 1. 23 3.135E+OO Line Not Found Absent 351.06 12.92* 3.337E+OO 1.150E+OO 1.150E+OO 79.27 OK PB-212 74.82 10.28 3.357E+OO 1.054E+OO 1.054E+OO 71. 86 OK 77 .11 17.10 3.576E+OO 1.473E+OO 1. 473E+OO 30.75 OK 238.63 43.60* 4.584E+OO l.073E+00 1.073E+OO 12.92 OK 300.09 3.30 3.820E+OO 9.620E-01 9.620E-01 137.97 OK BI-214 609.32 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 OK 1120.29 14.92 l.287E+OO 9.041E-01 9.044E-01 78.15 OK 1764.49 15.30 8. 672E-01 8.753E-01 8.756E-01 48.71 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 3.576E+OO 2.597E+OO 2.598E+OO 30.75 OK 87.09 3.41 4.447E+OO Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.868E+OO 7.375E-01 7.378E-01 35.88 OK 351.93 35.60* 3. 336E+oo* Line Not Found <<INT Reject RN-222 609.32 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 OK 1120. 29 14.92 l.287E+OO 9. 041E-01 9.044E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 8.756E-01 48.71 OK RA-224 240.99 4.10* 4.543E+OO 2.256E+OO 2.256E+OO 79.02 OK RA-226 609.32 45.49* 2.102E+00 8.785E-01 8.789E-01 23.19 OK 1120. 29 14.92 l.287E+00 9.041E-01 9.044E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 8.756E-01 .48.71 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11.27 3.450E+OO 1.0JlE+OO 1.031E+OO 54.85 OK 794.95 4. 25. 1.697E+OO 2.579E+OO 2.579E+OO 45.09 OK 835. 71 1. 61 l.630E+OO Line Not Found Absent 911. 20 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 OK 968. 97 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.450E+OO 1. 031E+OO 1.031E+OO 54.85 OK 794.95 4.25 l.697E+00 2.579E+OO 2.579E+OO 45.09 OK 835.71 1. 61 l.630E+OO Line Not Found Absent 911. 20 25.80* 1. 521E+OO 9.637E-01 9.637E-01 35.95 OK 968. 97 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 OK TH-228 74.82 10.28 3.357E+OO 1.054E+OO 1. 054E+OO . 71. 86 OK 77 .11 17.10 3.576E+OO 1. 473E+00 1.473E+OO 30.75 OK 238.63 43.60* 4.584E+OO 1.073E+OO 1.073E+oo* 12.92 OK 300.09 3.30 3.820E+OO 9.620E-01 9.620E-01 137.97 OK TH-230 609.32 45.49* 2.102E+OO 8.785E-01 8.785E-01 23.19 OK Page 3206 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235015 Acquisition date 08:11:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 l.287E+OO 9.041E-Ol 9.041E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 .8.753E-01 48.71 OK PA-231 283.69 1. 70 3. 991E+OO 3.676E+OO 3.676E+00 94.84 OK 301.36 5.35* 3.820E+OO 5.934E-01 5.934E-01 137.97 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.450E+OO 1. 031E+OO 1. 031E+OO 54.85 OK 835. 71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 OK 968. 97 15.80 1.448E+OO 9. 995E-01* 9.995E-01 39.93 OK TH-234 63.29 3.70* 1. 986E+OO 5.371E+OO 5.371E+OO 73. 96 OK 92.59 4.23 4.860E+OO 1. 783E+OO 1. 783E+OO 93.49 OK U-234 609.32 45.49* 2.102E+OO 8.785E-01 8.785E-01 23.19 OK 1120.29 14.92 1.287E+OO 9. 041E-01 9.041E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 8.753E-01 48. 71 OK U-238 63.29 3.70* 1.986E+OO 5.371E+OO 5.371E+OO 73. 96 OK 92.59 4.23 4.860E+OO 1.783E+OO l.783E+00 93.49 OK AM-243 43.53 5.90 1. 573E-01 Line Not Found Absent 74.66 67.20* 3.357E+OO 1.612E-01 l.612E-01 71. 86 OK ANH-511 511. 00 100.00* 2.430E+OO l.437E-01 1.437E-01 . 51. 05 OK Flag: "*" = Keyline Page 3207 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:15:18.10 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l * *Acquisition* date 3-0CT-2016 08:11:39 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
Sample date 8-DEC-2015 10:56:00 Analyst initials: MXRl *
Sample ID G405235015 Sample Quantity 1.4507E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File. : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt unc*ert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.738E+Ol 1. 800E+OO CD-109 1. 261E+OO 2.497E+OO SN-126 8.036E-02 1.591E-01 BA-137M 2.430E-01 9.127E-02 CS-137 2 .'567E-01 9.642E-02 TL-208 3.520E-01 8.982E-02 BI-211 1.150E+OO 8.936E-01 PB-212 l.073E+00 l.359E-01 BI-214 8.789E-01 l.997E-01 PB-214 1.155E+OO l.947E-01 RN-222 8.789E-01 1:997E-01 RA-224 2.256E+OO 1. 7 4 7E+00 RA-226 8.789E-01 l.997E-01 AC-228 9.637E-01 3.395E-01 RA-228 9.637E-01 3.395E-01 TH-228 l.073E+OO l.359E-01 TH-230 8.785E-01 1.997E-01 PA-231 5.934E-01 8.023E-01 TH-232 9.637E-01 3.395E-01 TH-234 5. 371E+OO 3.893E+OO U-234 8.785E-01 1.996E-01 U-238 5. 371E+OO. 3.893E+OO AM-243 1.612E-01 1.135E-01 ANH-511 1.437E-01 7.188E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3208 of 5809 Key-Line Activity (pCi/GRAM' -1.215E+OO -2.426E-02 O.OOOE+OO l.487E-02 -2.499E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.313E+Ol 5.689E-02 1. 960E+41 3.214E-02 3.789E-01 l.677E+04 MDA (pCi/GRAM 6.783E-01 2. 713E+OO l.577E-01 7.562E-02 7.989E-02 6.522E-02 3.333E-01 9 .191E-02 1.300E-01 3.487E-01 1.300E-01 9.855E-01 l.300E-01 2. 92lE-Oi 2. 921E-01 9 .191E-02 1.300E-01 8.249E-01 2.921E-01 2.910E+OO l.300E-01 2.910E+OO 1.148E-01 4.525E-02 MDA (pCi/GRAM 2.278E+Ol l.037E-01 O.OOOE+OO 7.812E-02 6.934E-01 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.430E+02 O.OOOE+OO SHORT HLIF MN-54 -l.210E-02 8.120E-02 1.475E-01 NOT IDENT. C0-56 -1.lOlE-01 4.646E-01 8.533E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 5.235E-02 4.850E-02 9.989E-02 NOT IDENT. C0-58 l.616E-01 5.703E-01 l.163E+OO NOT IDENT. FE-59 1.183E+Ol 8.264E+OO l.373E+Ol FAIL ABUN C0-60 4.267E-02 5. 311E-02 9.449E-02 FAIL ABUN ZN-65 l.012E-01 2.061E-01 4.006E-01 NOT IDENT. GE-68 2.lOlE+OO 2.449E+OO 5. 311E+OO NOT IDENT. AS-73 2.130E+OO 1.516E+Ol 3.040E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.059E+03 O.OOOE+OO SHORT HLIF SE-75 -3.892E-03 2.215E-01 3.990E-01 NOT IDENT. BR-77 O.OOOE+OO 2.486E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9. 496E+02 O.OOOE+OO SHORT HLIF RB-83 3.473E-01 6.642E-01 l.294E+OO NOT IDENT. KR-85 6.488E+OO 5.028E+OO 1.124E+Ol NOT IDENT. SR-85 6.846E-01 5. 313E-01 1.188E+OO NOT IDENT. RB-86 O.OOOE+OO 3.075E+04 O.OOOE+OO SHORT HLIF Y-88 -2.598E-02 2.676E-01 5.665E-01 NOT IDENT. Y-91 2 .110E+02 6.393E+02 1.306E+03 NOT IDENT. NB-94 2.033E-02 3.945E-02 7.873E-02 FAIL ABUN NB-95 l.164E-01 1.067E+OO l.829E+00 NOT IDENT. NB-95M -l.639E+OO 2.828E+OO 4.342E+OO .NOT I DENT. ZR-95 -9.700E-01 1.819E+OO 3.138E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 810E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 1.974E-02 3.565E-02 6.993E-02 NOT IDENT. RH-102 7.340E-03 5.816E-02 l.156E-01 NOT IDENT. RU:..103 -2.265E+OO 6.652E+OO 1.230E+Ol FAIL ABUN RH-106 2.279E-02 5.336E-01 l.037E+OO NOT IDENT. RU-106 2.279E-02 5.336E-01 1.037E+OO NOT IDENT. AG-108M l.552E-02 3.093E-02 6.332E-02 NOT IDENT. AG-llOM -1.230E-01 l.150E-01 1. 947E-01 NOT IDENT. SN-113 -1.381E-01 2.528E-01 4.650E-01 NOT IDENT. CD-115 O.OOOE+OO 2.914E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 0.000E+OO 9.547E+04 O.OOOE+OO SHORT HLIF TE-123M 2.414E-02 1. 261E-01 2.394E-01 NOT IDENT. *SB-124 -9.028E-01 1.943E+OO 3.543E+OO NOT IDENT. SB-125 2.405E-02 1. 017E-01 2.058E-01 FAIL ABUN TE-125M -4.543E+Ol 2.972E+02 5.574E+02 NOT IDENT. I-126 O.OOOE+OO 1. 066E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.128E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.299E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.605E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.228E+26 O.OOOE+OO SHORT HLIF BA-133 5.431E-02 3.986E-02 8.526E-02 NOT IDENT. I-133 O.OOOE+OO 1.388E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 7.462E-02 1.326E-01 FAIL ABUN CS-135 -2.155E-02 l.460E-01 2.585E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O:OOOE+OO SHORT HLIF CS-136 0.000E+OG 3.293E+05 O.OOOE+OO SHORT HLIF CE-139 7.823E-02 l.206E-01 2.342E-01 NOT IDENT. BA-140 0.000E+OO l.205E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.009E+05 O.OOOE+OO SHORT HLIF CE-141 1.041E+OO 2. 691E+Ol 5.0.04E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.331E-01 3.726E-01 6.609E-01 NOT IDENT. PM-144 -7.840E-03 6 .171E-02 1.150E-01 NOT IDENT. PR-144 -6.812E-01 5. 361E+oo* 9.992E+OO NOT IDENT. PM-146 2.362E-02 4.484E-02 9.309E-02 NOT IDENT. ND-147 O.OOOE+OO 3.052E+07 0.000E+OO SHORT HLIF. PM-147 -5.403E+Ol 8.382E+02 l.579E+03 NOT IDENT. PM-149 O.OOOE+OO 9.295E+40 O.OOOE+OO SHORT HLIF EU-150 5.076E-06 2.641E-02 4.717E-02 FAIL ABUN EU-152 2.974E-02 8. 964E-02 l.835E-01 FAIL ABUN GD-153 1.756E-01 1. 968E-01 3.800E-01 NOT IDENT. EU-154 -6.221E-02 1.389E-01 2.524E-01 FAIL ABUN EU-155 -1.454E-02 l.127E-01 2.128E-01 FAIL ABUN TB-160 7.227E-01 1.782E+OO 3.904E+OO FAIL ABUN H0-166M -4.340E-03 5.857E-02 1. lllE-01 FAIL ABUN TM-171 l.593E+OO 3.750E+Ol 7.477E+Ol NOT IDENT. HF-172 -6.872E-02 2.293E-Ol 4.218E-01 FAIL ABUN LU-172 2. 874E-.02 l.066E-01 1.947E-01 FAIL ABUN LU-176 7.255E-03 2.377E-02 4.854E-02 FAIL ABUN Page 3209 of 5809 HF-181 4.271E+OO 6.717E+OO 8.497E+OO FAIL ABUN TA-182 -1. 841E-01 1.190E+OO l.980E+OO FAIL ABUN RE-183 -2 .181E-01 4.547E+OO 8.974E+00 NOT IDENT. RE-184 -8.667E+OO 2.909E+Ol 5.692E+Ol NOT IDENT. W-188 9.675E+OO l.339E+02 2. 221E+02 FAIL ABUN IR-192 1.295E-Ol 4.625E-01 9.399E-01 FAIL ABUN HG-203 -1.257E+OO 2.412E+OO 4. 061E+OO NOT IDENT. BI-207 6.760E-02 5. OllE-02 1.207E-01 FAIL ABUN PB-210 -1.268E-Ol 7.562E+OO 1.525E+Ol NOT IDENT. PB-211 1.792E-01 7.193E-01 1.438E+OO NOT IDENT. BI-212 7.358E-01 8.783E-01 1.335E+OO FAIL ABUN RN-219 -2.098E-01 3.617E-01 6.640E-01 FAIL ABUN RA-223 -4. 391E-Ol 6.307E-01 1. Ol 7E+OO FAIL ABUN AC-227 -3.762E-01 '2.657E-01 3. 996E-01 FAIL ABUN TH-227 -3.762E-01 2.657E-01 3.996E-01 FAIL ABUN TH-229 -7.744E-02 4.848E-01 8.736E-01 FAIL ABUN TH-231 -4.391E-01 6.307E-01 1.017E+OO FAIL ABUN PA-233 5. 431E-02 6.613E-02 1.385E-01 FAIL ABUN PA-234 1. 529E-02 2. 725E-01 5.620E-01 FAIL ABUN PA-234M 3.369E+OO 4.340E+OO 9.184E+OO NOT IDENT. U-235 1. 771E-02 1.940E-01 3.630E-01 FAIL ABUN NP-237 5. 431E-,02 6. 613E-02 1.385E-01 FAIL ABUN NP-238 O.OOOE+OO *l.960E+41. O.OOOE+OO SHORT HLIF NP-239 -l.136E-01 2.437E-01 4.440E-01 FAIL ABUN PU-239 -4.243E+01 3.300E+02 6 .121E+02 FAIL ABUN AM-241 6.568E-02 2.020E-01 3.839E-01 NOT IDENT. CM-243 2.062E-02 l.056E-01 1.915E-01 FAIL ABUN BK-247 l.557E-03 7.712E-02 1.394E-01 NOT IDENT. CM-247 1.930E-02 3.194E-02 6.773E-02 NOT IDENT. CF-249 l.140E-02 3.678E-02 7.492E-02 NOT IDENT. CF-251 -6.705E-02 1.119E-01 l.944E-01 FAIL ABUN Page 3210of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:15:15.97 Nuclide Line Activity Report Nuclide Type: Uncorrected' Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 369 10.66* 1.030E+OO 1.738E+Ol 1.738E+Ol 10.57 CD-109 88.03 47 3.70* 4.453E+OO 1.483E+OO 2.328E+OO 108.23 SN-126 64.28 76 9.60 1. 986E+OO 2.070E+OO 2.070E+OO 73. 96 86.94 47 8.90 4.453E+OO 6.167E-01 6.167E-01 108.23 87.57 47 37.00* 4.453E+OO 1.483E-01 1.483E-01 108.23 661.66 81 89.90* 1. 965E+OO 2.384E-01 2.430E-01 38.33 CS-137 661.66 81 85.10* 1. 965E+OO 2.519E-01 2.567E-01 38 .. 33 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 126 85.00* 2.178E+OO 3.520E-01 3.520E-01 26.04 860.56 37 12.50 1.591E+OO 9.740E-01 9.740E-01 60.95 BI-211 72. 87 ------1. 23 3 .135E+OO ------Line Not Found ------351.06 265 12.92* 3.337E+OO 3.182E+OO 3.182E+OO 17.20 PB-212 74.82 98 10.28 3.357E+OO 1.470E+OO 1. 470E+OO, 50.50 77 .11 174 17.10 3.576E+OO 1.473E+OO 1.473E+OO 30.75 238.63 415 43.60* 4.584E+OO 1.073E+OO 1.073E+OO 12.92 300.09 23 3.30 3.820E+OO 9.620E-01 9.620E-01 137. 97 BI-214 609.32 162 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 1120.29 34 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 1764.49 22 15.30 8. 672E-01 8.753E-01 8.756E-01 48.71 PB-214 74:82 98 5. 80 3.357E+00 2.605E+00 2.606E+OO 50.50 77 .11 174 9.70 3.576E+OO 2.597E+OO 2.598E+OO 30.75 87.09 47 3.41 4.453E+00 l.609E+OO l.610E+OO 108.23 242.00 128 7.25 4.543E+OO 2.013E+OO 2.014E+OO 48.32 295.22 102 18.42 3.868E+OO 7.375E-01 7.378E-01 35.88 351. 93 265 35.60* 3.337E+OO 1.155E+OO 1.155E+OO 17.20 RN-222 609.32 162 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 1120.29 34 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 1764.49 22 15.30 8. 672E-01 8.753E-01 8.756E-01 48'. 71 RA-224 240.99 128 4.10* 4.543E+OO 3.560E+OO 3.560E+OO 48.32 RA-226 609.32 162 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 1120.29 34 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 1764.49 22 15.30 8. 672E-01 8.753E-01 8.756E-01 48.71 AC-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 77 11. 27 3.450E+OO 1. 031E+OO 1. 031E+OO 54.85 794.95 36 4.25 1.697E+OO 2.579E+OO 2.579E+OO 45.09 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 73 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 968. 97 44 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 77 11. 27 3.450E+OO l.031E+00 1.031E+OO 54.85 794.95 36 4.25 1.697E+OO 2.579E+OO 2.579E+OO 45.09 835. 71 ------1. 61 1.630E+OO ------*Line Not Found ------911.20 73 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 968. 97 44 15.80 l.448E+OO 9.995E-01 9.995E-01 39.93 TH-228 74.82 98 10.28 3.357E+OO . 1. 470E+OO 1. 470E+OO 50.50 77 .11 174 17.10 3.576E+OO 1.473E+OO 1.473E+OO 30.75 238.63 415 43.60* 4.584E+OO l;073E+00 l.073E+OO 12.92 Page 3211 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 23 3.30 3.820E+OO 9.620E-01 9.620E-01 137. 97 TH-230 609.32 162 45.49* 2.102E+OO 8.785E-01 8.785E-01 23.19 1120.29 34 14.92 1. 287E+OO 9. 041E-01 9.041E-01 78.15 1764.49 22 15.30 8.672E-01 8.753E-01 8.753E-01 48.71 PA-231 283.69 48 1. 70 3.991E+OO 3.676E+OO 3.676E+OO 94.84 301.36 23 5.35* 3.820E+OO 5.934E-01 5.934E-01 l37.97 TH-232 105.21 ------1.10 5.460E+00 ------Line Not Found ------338.32 77 11. 27 3.450E+OO l.031E+OO 1. 031E+OO 54.85 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 73 25.80* 1. 521E+OO 9.637E-01 9.637E-01 35.95 968. 97 44 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 TH-234 63 .29 76 3.70* 1. 986E+OO 5. 371E+OO 5. 371E+OO 73. 96 92.59 71 4.23 4.860E+OO 1.783E+OO 1.783E+OO 93.49 U-234 609.32 162 45.49* 2.102E+OO 8.785E-01 *8. 785E-01 23.19 1120.29 34 14.92 1.287E+OO 9. 041E-01 9.041E-01 78.15 1764.49 22 15.30 8. 672E-01 8.753E-01 8.753E-01 48. 71 U-238 63.29 76 3.70* 1. 986E+OO 5. 371E+OO 5.371E+00 73. 96 92.59 71 4.23 4.860E+OO 1. 783E+OO. 1.783E+OO 93.49 AM-243 43.53 ------5.90 1.573E-01 ------Line Not Found ------74.66 98 67.20* 3.357E+OO 2.248E-01 2.248E-01 50.50 ANH-511 511.00 67 100.00* 2.430E+OO l.437E-01 l.437E-01 51. 05 Flag: "*" Key line Page 3212 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Total number of lines in spectrum 49 Number of unidentified lines 10 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 *RA-224 ,RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1.41E+l0Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1.41E+l0Y 1.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1 .. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 738E+Ol l.483E+00 l.483E-01 2.384E-01 2.519E-01 3.520E-01 3.182E+OO 1. 073E+OO 8.785E-01 1.155E+OO 8.785E-01 3.560E+00 8.785E-01 9.637E-01 9.637E-01 1.073E+OO 8.785E-01 5.934E-01 9.637E-01 5.371E+OO 8.785E-01 5.371E+OO 2.248E-01 l.437E-01 4.889E+Ol 4.889E+Ol Decay Corr pCi/GRAM 1. 738E+Ol 2.3.28E+OO 1. 483E-01 2.430E-01 2.567E-01 3.520E-01 3.182E+OO 1.073E+OO 8.789E-01 1.155E+OO 8.789E-01 3.560E+OO 8.789E-01 9.637E-01 9.637E-01 1.073E+O'O 8.785E-01 5.934E-01 9.637E-01 5.371E+OO 8.785E-01 5. 371E+OO 2.248E-01 1.437E-01 4.975E+Ol 4.975E+Ol Decay Corr 2-Sigma Error 0.184E+Ol 2.519E+OO 1.605E-01 0.931E-01 0.984E-01 0.917E-01 0.547E+OO 0.139E+00 2.038E-01 0.199E+OO 2.038E-01 1. 720E+00 2.038E-01 3.464E-01 3.464E-01 0.139E+00 2.037E-01 8.186E-01 3.464E-01 3.973E+OO 2.037E-01 3.973E+OO 1.135E-01 0.733E-01 "M" Manually accepted 2-Sigma %Error 10.57 108.23 108.23 38.33 38.33 26.04 17.20 12.92 23.19 17. 20 23.19 48.32 23.19 35.95 35.95 12.92 23.19 137. 97 35.95 73. 96 23.19 73. 96 50.50 51. 05 Flags: "K" not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3213 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235015 Acquisition date : 3-0CT-2016 08:11:39 It Energy Area Bkgnd FWf1M Channel Left Pw Cts/Sec %Err %Eff Flags 0 99.51 37 228 3.33 199.50 193 12 8.49E-03 **** 5.22E+OO T 0 185.90 118 132 0. 96 372.34 366 12 2.83E-02 47.5 5.40E+00 T 0 209.20 29 81 0.93 418. 96 416 7 7.09E-03 **** 5.03E+OO 0 271. 00 25 84 1. 46 542.61 536 9 6.29E-03 **** 4.15E+OO T 0 321. 84 41 44 0.98 644.35 640 10 1. 03E-02 71. 9 3.60E+OO T 0 414.86 16 40 2.38 830.48 823 10 4.05E-03 **** 2.90E+OO T 6 482.23 13 23 1. 49 965.28 959 10 3.27E-03 **** 2.55E+OO T 2 516.88 22 4 1. 80 1034.63 1031 25 5.80E-03 59.2 2.41E+OO 2 525.75 20 7 1. 81 1052.37 1031 25 5.21E-03 61. 4 2.37E+OO 0 669.81 10 27 4.82 1340. 67 1330 12 2.80E-03 **** 1. 95E+OO 0 727.83 17 26 1. 36 1456.78 1451 10 4.66E-03 **** l.82E+OO T 0 738.40 5 10 0.89 1477.92 1474 6 1. 25E-03 **** l.80E+OO T 0 768.61 28 24 1. 71 1538.38 1529 13 7.49E-03 82.6 1. 74E+OO 0 772.60 9 13 1. 38 1546.37 1543 7 2.35E-03 **** 1. 74E+OO T 0 871. 28 26 13 6.59 1743.86 1734 18 7.15E-03 77.6 1. 58E+OO T 0 923.46 11 5 0.59 1848.31 1845 7 3.07E-03 90.7 1. 50E+OO T 5 964.70 22 5 2.91 1930.84 1926 18 6.07E-03 55.0 . 1. 45E+OO T 0 1005.15 8 12 0.92 2011. 81 2008 8 2.22E-03 **** 1. 41E+OO T 0 1039.30 7 14 0.97 2080.16 2071 11 2.02E-03 **** l.37E+OO T 0 1041.21 13 1 1. 51 2083.97 2081 6 3.50E-03 63.9 l.37E+OO 0 1084.19 13 14 0.73 2170.00 2162 14 3.61E-03 **** l.32E+OO 0 1095.28 7 7 0.98 2192.21 2188 6 1. 84E-03 **** l.31E+OO 0. 1098.49 16 4 3.22 2198.64 2194 10 4.44E-03 71. 3 l.31E+OO T 0 1154.44 16 8 2.34 2310.63 2305 11 4.45E-03 85.3 l.26E+OO 0 1223.88 9 11 0.65 2449.62 2444 9 2. 51E-03 **** l.20E+00 0 1333.06 8 5 2.33 2668.18 2661 11 2.36E-03 **** l. llE+OO T Flags: "T" Tentatively associated Page 3214 of 5809 VAX/VMS Nuclide Identification Report Generated 09:15:39.45 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l *
Acquisition date 3-0CT-2016 08:11:39 Sensitivity 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
Sample date 8-DEC-2015 10:56:00 Nuclide Library : SOLID *
Sample ID Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4507E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2. 7 51E-01 1.287E+OO 7.438E-02 3.369E-02 3.559E-02 2.874E-02 l.499E-01 4. 231E-02 5.753E-02 l.683E-01 5.753E-02 4 . .S37E-01 5.753E-02 1.280E-01 1.280E-01 4. 231E-0.2 5,. 751E-02 3.768E-01 1.280E-01 1.356E+OO 5. 7 51E-02 1.356E+OO 5.407E-02 1. 967E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3215of5809 Le (pCi/GRAM l.006E+Ol 4.428E-02 0.000E+OO 3.078E-02 2.919E-01 O.OOOE+OO 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. , FAIL ABUN SHORT HLIF SHORT'HLIF MN-54 C0-56 MN:--56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 *I-133 CS-134 CS-135 I-135 CS-136' CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3216of5809 6.526E-02 3.615E-01 0.000E+OO 4.678E-02 5.009E-01 5.845E+OO 4. 021E-02 l.750E-01 2.300E+OO l.415E+Ol 0.000E+OO 1. 829E-01 O.OOOE+OO 0 .. OOOE+OO 5. 728E-01 4.899E+OO 5.175E-01 O.OOOE+OO 2.239E-01 5.751E+02 3.555E-02 8.093E-01 2.008E+OO 1.378E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.278E-02 5.050E-02 5.518E+OO 4.573E-01 4.573E-01 2.880E-02 8. 291E-02 2.103E-01 O.OOOE+OO 0. OO"OE+OO l .110E-01 1.255E+OO 9.237E-02 2.604E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.890E-02 O.OOOE+OO 5.983E-02 l.184E-01 O.OOOE+OO O.OOOE+OO 1.098E-01 O.OOOE+OO O.OOOE+OO 2.348E+Ol O.OOOE+OO 3. 072E-01 5.076E-02 4.410E+OO 4.197E-02 O.OOOE+OO 7.344E+02 O.OOOE+OO 2.139E-02 8.342E-02 1. 781E-01 1. 07 6E-01 9.915E-02 1.684E+00 4.844E-02 3.475E+Ol 1.959E-01 8.575E-02 2.220E-02 3.776E+00 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT; NOT .I DENT. NOT IDENT. SHORT"HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHO.RT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3217of5809 8.560E-01 4.187E+OO 2.414E+Ol 1.020E+02 4.299E-01 1. 840E+OO 5.319E-02 7.066E+OO 6.545E-01 6.091E-01 2.952E-01 4.577E-01 l.821E-01 1.821E-01 4.054E-01 4.577E-01 6.417E-02 2.410E-01 3.994E+OO 1.702E-01 6.417E-02 O.OOOE+OO 2.059E-01 2.863E+02 1. 789E-01 8. 901E-02 6.398E-02 *3. 049E-02 3.389E-02 8.954E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:15:50.50 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l *
Acquisition date 3-0CT-2016 08:11:39 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
Sample date 8-DEC-2015 10:56:00 Nuclide Library : SOLID *
Sample ID : G405235015 Analyst initials: MXRl *
Batch Number :, 1596247 Sample Quantity l.4507E+02 GRAM *
Quantity Err(%) l.3786E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date' 6-SEP-2016 04:59:25 Eff. Geometry :'CAN -i:
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity* Act Error TPU Nuclide (pCi/GRAM ) ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.738E+Ol 2.015E+OO 2.015E+00 CD-109 l.261E+00 2.503E+OO 2.503E+00 SN-126 8.036E-02 l.594E-01 l.594E-01 BA-137M 2.430E-01 9.187E-02 9.187E-02 CS-137 2.567E-01 9.705E-02 9.705E-02 TL-208 3.520E-01 9.105E-02 9.105E-02 BI-211 l.150E+OO 9.036E-01 9.036E-01 PB-212 l.073E+OO l.473E-01 l.473E-01 BI-214 8.789E-01 2.032E-01 2.032E-01 PB-214 l.155E+00 2.006E-01 2.006E-01 RN-222 8.789E-01 2.032E-01 2.032E-01 RA-224 2.256E+OO 1. 753E+OO 1. 753E+OO RA-226 8.789E.:...01 2.032E-01 2.032E-01 AC-228 9.637E-01 3.430E-01 3.430E-01 RA-228 9.637E-01 3.430E-01 3.430E-01 TH-228 l.073E+OO l.473E-01 l.473E-01 TH-230 8.785E-01 2.032E-01 2.032E-01 PA-231 5.934E-01 8.122E-01 8.122E-01 TH-232 9.637E-01 3.430E-01 3.430E-01 TH-234 5.371E+OO 4.071E+OO 4.071E+OO U-234 8.785E-01 2.032E-01 2.032E-01 U-238 5. 371E+OO 4.071E+OO 4.071E+OO AM-243 l.612E-01 l.142E-01 l.142E-01 ANH-511 l.437E-01 7.212E-02 7.212E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide. (pCi/GRAM (1.96-sigma) ( 1 . 96-sigma ) BE-7 -l.215E+OO 1. 313E+Ol 1. 314E+Ol NOT IDENT. NA-22 -2.426E-02 5.690E-02 5.794E-02 NOT IDENT. NA-24 -l.OOOE+41 4.956E+41 O.OOOE+OO SHORT HLIF AL-26 l.487E-02 3.216E-02 3.285E-02 NOT IDENT. SC-46 -2.499E-01 3.790E-01 3.954E-01 FAIL ABUN V-48 l. ll3E+04 l.678E+04 1. 751E+04 SHORT HLIF Page 3218of5809 CR-51 -1.114E+02 4. 431E+02 4.459E+02 SHORT HLIF MN-54 -1.210E-02 8.120E-02 8 .138E-02 NOT IDENT. C0-56 -1. lOlE-01 4.647E-01 4.673E-01 FAIL ABUN MN-56 -l.000E+41 4.458E+41 O.OOOE+OO SHORT HLIF C0-57 5.235E-02 4.856E-02 5.399E-02 NOT IDENT. C0-58 1.616E-01 5.704E-01 5.750E-01 NOT IDENT. FE-59 l.183E+Ol 8.309E+OO 9.874E+OO FAIL ABUN C0-60 4.267E-02 5.313E-02 5.650E-02 FAIL ABUN ZN-65 1.012E-01 2.061E-01 2. lllE-01 NOT IDENT. GE-68 2 .101E+OO 2.450E+00 2.627E+OO NOT IDENT. AS-73 2.130E+OO 1.516E+Ol 1.519E+Ol NOT IDENT. AS-74 -3.971E+02 6.059E+03 6.062E+03 SHORT HLIF SE-75 -3.892E-03 2.215E-01 2.215E-01 NOT IDENT. BR-77 1. 963E+38 1. 700E+39 O.OOOE+OO SHORT HLIF SR-82 -2.631E+Ol 9.496E+02 9.497E+02 SHORT HLIF RB-83 3.473E-01 6.659E-01 6.841E-01 NOT IDENT. KR-85 6.488E+OO 5.035E+OO 5.823E+OO NOT IDENT. SR-85 6.846E-01 5.321E-01 6.151E-01 NOT IDENT. RB-86 7.865E+03 3.075E+04 3.095E+04 SHORT HLIF Y-88 -2.598E-02 2.676E-01 2.678E-01 NOT IDENT. Y-91 2 .110E+02 6.394E+02 6.464E+02 NOT IDENT. NB-94 2.033E-02 3.946E-02 4.051E-02 FAIL ABUN NB-95 l.164E-01 1.067E+OO l.068E+OO NOT IDENT. NB-95M -1.639E+OO 2. 831E+OO 2.926E+OO NOT IDENT. ZR-95 -9.700E-01 1.820E+OO 1.872E+OO NOT IDENT. NB-97 -1.000E+41 l.940E+42 O.OOOE+OO SHORT HLIF* ZR-97 1.000E+41 3.690E+41 O.OOOE+OO SHORT HLIF M0-99 7.926E+31 1. 811E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 5.547E+41 O.OOOE+OO SHORT HLIF RH-101 1. 974E-02 3.582E-02 3.691E-02 NOT IDENT. RH-102 7.340E-03 5.817E-02 5.826E-02 NOT IDENT. RU-103 -2.265E+OO 6.653E+OO 6.730E+OO FAIL ABUN RH-106 2.279E-02 5.336E-01 5. 337E'-01 NOT IDENT. RU-106 2.279E-02 5.336E-01 5.337E-01 NOT IDENT. AG-108M 1.552E-02 3.094E-02 3.172E-02 NOT IDENT. AG-llOM -1.230E-01 1.151E-01 l.278E-01 NOT IDENT. SN-113 -1.381E-01 2.529E-01 2.604E-01 NOT IDENT. CD-115 l .119E+39 2.921E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -8.680E+03 9.548E+04 9.556E+04 SHORT HLIF TE-123M 2.414E-02 1.261E-01.. 1.266E-01 NOT IDENT. SB-124 -9.028E-01 1.944E+OO 1. 986E+OO NOT IDENT. SB-125 2.405E-02 1. 017E-01 l.023E-01 FAIL ABUN TE-125M -4.543E+Ol 2.972E+02 2.979E+02 NOT IDENT. I-126 2.633E+05 l.066E+06 l.073E+06 SHORT HLIF SB-126 -l.938E+05 9.135E+05 9.177E+05 SHORT HLIF SB-127 1. 037E+22 2.705E+22 O.OOOE+OO SHORT HLIF I-131 7.678E+08 4.605E+09 4.618E+09 SHORT HLIF I-132 1.000E+41 l.933E+42 O.OOOE+OO SHORT HLIF TE-132 3.654E+26 4.481E+26 O.OOOE+OO SHORT HLIF BA-133 5.431E-02 3.992E-02 4.683E-02 NOT IDENT. I-133 -l.000E+41 2.280E+41 O.OOOE+OO SHORT HLIF CS-134 l.689E-01 7.497E-02 1.068E-01 FAIL ABUN CS-135 -2.155E-02 1.460E-01 1.463E-01 NOT IDENT. I-135 l.000E+41 l.052E+42 O.OOOE+OO SHORT HLIF CS-136 -4.493E+04 3.294E+05 3.300E+05 SHORT HLIF CE-139 7.823E-02 1.216E-01 l.266E-01 NOT IDENT. BA-140 -3.078E+05 1.205E+06 l.213E+06 SHORT HLIF LA-140 -3.037E+05 4.012E+05 4.239E+05 SHORT HLIF CE-141 1. 041E+OO 2. 691E+Ol 2.692E+Ol NOT IDENT. CE-143 -1.000E+41 6.679E+41 O.OOOE+OO SHORT HLIF CE-144 -2.331E-01 3. 728E-01 3.873E-01 NOT IDENT. PM-144 -7.840E-03 6. l 71E-02 6.181E-02 NOT IDENT. PR-144 -6.812E-01 5.361E+OO 5.369E+OO NOT IDENT. PM-146 2.362E-02 4.487E-02 4.612E-02 NOT IDENT. ND-147 -8.845E+06 3.053E+07 3.079E+07 SHORT HLIF PM-147 -5.403E+Ol 8.382E+02 8.386E+02 NOT IDENT. PM-149 l.000E+41 9.550E+40 O.OOOE+OO SHORT HLIF EU-150 5.076E-06 2. 641E-02 2.641E-02 FAIL ABUN EU-152 2.974E-02 8. 966E-02 9.065E-02 FAIL ABUN GD-153 1.756E-01 1.971E-01 2.124E-01 NOT IDENT. EU-154 -6.221E-02 l.390E-01 l.418E-01 FAIL ABUN EU-155 -1.454E-02 l.127E-01 1.129E-01 FAIL ABUN TB-160 7.227E-01 1. 783E+OO l.812E+OO FAIL ABUN H0-166M -4.340E-03 5.857E-02 5.860E-02 FAIL ABUN TM-171 1.593E+OO 3.750E+Ol 3.750E+Ol NOT IDENT. HF-172 -6. 872E-02 2.296E-01 2.317E-01 FAIL ABUN LU-172 2.874E-02 l.066E-01 l.074E-01 FAIL ABUN LU-176 7.255E-03 2.377E-02 2.400E-02 FAIL ABUN Page 3219of5809 HF-181 4.271E+OO
6.720E+OO 6.990E+00 FAIL ABUN TA-182 -1. 841E-01 1.190E+OO l.193E+00 FAIL ABUN RE-183 -2.181E-01 4.547E+OO 4.549E+OO NOT I DENT .. RE-184 -8.667E+OO 2.917E+Ol 2.943E+Ol NOT IDENT. W-188 9.675E+OO 1. 339E+02 1.340E+02 FAIL ABUN IR-192 l.295E-01 4.625E-01 4.662E-01 FAIL ABUN HG-203 -1.257E+OO *2.413E+00 2.478E+OO* NOT IDENT. BI-207 6.760E-02 5.018E-02 5.870E-02 FAIL ABUN PB-210 -1.268E-01 7.562E+OO 7.562E+OO NOT IDENT. PB-211 l.792E-01 7.194E-01 7.239E-01 NOT IDENT. BI-212 7.358E-01 8.791E-01 9. 396E-01 FAIL ABUN RN-219 -2.098E-01 3.626E-01 3.747E-01 FAIL ABUN RA-223 -4.391E-01 6.312E-01 6.616E-01 FAIL ABUN AC-227 -3.762E-01 2.703E-01 3.191E-01 FAIL ABUN TH-227 -3.762E-01 2.703E-01 3.191E-01 FAIL ABUN TH-229 -7.744E-02 4.848E-01 4.860E-01 FAIL ABUN TH-231 -4. 391E-01 6.312E-01 6.616E-01 FAIL ABUN PA-233 5.431E-02 6.618E-02 7.056E-02 FAIL ABUN PA-234 1.529E-02 2.731E-01 2.732E-01 FAIL ABUN PA-234M 3.369E+OO 4.343E+OO 4. 601E+OO NOT IDENT. U-235 l.771E-02 l.940E-01 l.942E-01 FAIL ABUN NP-237 5.431E-02 6.618E-02 7.056E-02 FAIL ABUN NP-238 4.718E+40 5.971E+41 O.OOOE+OO SHORT HLIF NP-239 -1.136E-01 2.439E-01 2.492E-01 FAIL ABUN PU-239 -4.243E+Ol 3.300E+02 3.306E+02 FAIL ABUN AM-241 6.568E-02 2.020E-01 2.042E-01 NOT IDENT. CM-243 2.062E-02 l.056E-01 1.060E-01 FAIL ABUN 'BK-247 l.557E-03 7.712E-02 7. 713E-02 NOT IDENT. CM-247 1.930E-02 3.210E-02 3.326E-02 NOT IDENT. CF-249 l.140E-02 3.679E-02 3. 715E-02 NOT IDENT. CF-251 -6.705E-02 l.121E-01 1.161E-01 FAIL ABUN Page 3220 of 5809
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.8048 87.09 91.6306 136.47 51.5515 45.60 55. 0496 87.57 91. 7214 140.51 0.0000 46.54 53.4309 88.03 113 .1961 143.76 *72.7363 49.72 0.0000 88.34 113.2678 144.24 64.0964 51. 35 61.4377 88.47 113.2975 145.44 76.1780 51. 87 57. 9111 89. 96 85.2290 152.43 79.1334 52.39 54.3732 1093.63 85.3452 153.25 0.0000 52.97 49.0174 91.11 0.0000 323.87 60.5977 53.44 54.5368 92.59 92.9816 156.02 0.0000 54.07 56.4552 93.35 93.1204 158.56 0.0000 57.36 0.0000 94.56 93.3405 159.00 51.0144 57.53 57.9169 94.65 93.3568 162.33 57.9263 57.98 66.2709 94.67 93.3604 162.66 0.0000 59.27 65.2685 94.87 93. 3967 163.33 69.1578 59.32 65.2771 97.43 53.6324 165.86 60.4352 59.54 55.4562 98.43 53.7341 176.31 52.1754 60. 96 63.0852 98.44 53.7351 176.60 0.0000 61.17 63. 1197 99.53 53.8456 177.52 57.9345 62. 93 62.4742 100 .11 53.9038 181.07 0.0000 63.29 62.5314 102.03 51.3915 181.52 63.9297 63.58 62.5775 103.18 54.2102 184.41 46.9708 64.28 72.3566 103.37 54.2293 143.76 47.0459 66.73 56.4816 105.21 65.2930 193.51 59.0645 .67. 24 59.3797 105.31 65.3047 197.03 59.3073 125.81 76.4276 106.12 57.2249 198.01 76 .. 8372 67.75 76.4399 106.47 57.2608 201.83 60.8042 69.67 71.1061 109.28 70.9057 203.43 59.7431 70.83 75.1046 111. 00 63.9044 205.31 64.1734 72.81 95.5101 111. 76 0. 0000. 210.85 59.8451 72.87 95.5238 114. 06 56.9886 215.65 65.3049 74.66 87.2842 116. 30 0.0000 222 .11 66.9537 74.82 87.3162 116.74 64.5340 227.09 57.6899 74.97 87.3460 119. 76 65.9051 227.38 43.2806 77 .11 87.7675 121.12 60.8099 228.16 0.0000 78.74 80.0184 121. 22 60.8201 228.18 48.1299 79.69 60.7853 121.78 52.4788 116. 74 48.1299 80.12 55.6641 122.06 49.3527 235.69 64. 6696 80.19 0.0000 122.92 52.5761 235. 96 64.6867 80.57 59.6057 123.07 56.7962 238.63 44.9978 81. 00 53.1765 265.00 56.8522 238.98 0.0000 81. 07 59.6703 125.81 63.3852 240.99 45.1039 81. 75 78.9186 127.23 62.4687 242.00 45.1496 83.79 61. 3217 127.91 71.0157 244.70 44.0469 84.00 58.7384 129.30 73.2946 252.40 0.0000 85.43 79.8615 131.20 68.1855 252.80 48.0954 86.55 91.5291 133.02 65.1709 254.15 0.0000 86.79 91. 5738 133.52 72.7055 256.23 65.5755 86.94 91.6029 136.00 62.2472 260.90 0.0000 Page 3221of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 41.1553 355.39 0.0000 584.27 20.0919 264.80 41.1614 356.01 16.1433 595.83 0.0000 265.00 41.1684 364.49 0.0000 427.87 28.0470 268.22 42.5425 366.42 0.0000 602.52 0.0000 269.46 45.0967 372.51' 32.6785 604. 72 15.6134 270.03 45 .1198 375.05 22.7351 607.14 25.0107 271. 23 42.6608 377.52 26.4187 609.32 19.8218 273.65 0.0000 356.01 35.6881 610.33 19. 8311 276.40 34.4570 388.16 25.6997 614.28 26.6673 277.37 37.0104 388.63 0.0000 618.01 19.9053 277.60 37.0176 391.69 38.6436 620.36 22.0254 278.00 35.3478 264.66 36.1047 621.93 16.7943 279.20 40.4414 401. 81 29.6471 630.19 0.0000 279.54 50.5664 402.40 19.4641 631.29 14.7611 279.70 50.5737 404.85 30.6367 633.25 18. 9961 280.46 44.2819 410.95 32.1606 634.78 0.0000 283.69 29.6060 413.71 36.4221 635.95 16.9069 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 29.6509 423.72 0.0000 645.85 14.8625 285.90 0.0000 427.09 30.1478 657.76 17.6132 287.50 30.5544 427.87 22.6221 657.90 0.0000 290.67 40.8516 433.94 26.4955 661.66 22.4569 293.27 0.0000 439.40 28.4863 664.57 0.0000 351.93 38.4485 453.88 21.0798 666.33 0.0000 295. 96 38.4732 463.37 26.0211 666.50 0.0000 879.38 38.5593 468.07 23.1958 667.71 0.0000 299.98 38.6050 473.00 0.0000 677.62 14.0029 300.09 38.6087 475.06 21. 3519 685.70 0.0000 300 .13 38. 6096 476.78 26.2315 695.00 0.0000 301. 36 37.3616 477.60 20.4121 696.49 20.6375 302.85 39.9884 482.18 15.5944 696. 51 20.6382 256.23 38.2357 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.8184 306.78 33.6497 497.08 30.4765 697.49 21. 7334 308.46 42.3367 505.52 25.1903 702.65 21.7822 311. 90 38.1249 507.63 0.0000 706.68 17.4564 316.51 33.9203 511. 00 14.8639 711. 68 16.4008 319.41 0.0000 514.00 2.9778 720. 70 0.0000 320.08 0.0000 514.00 2.9778 721. 93 0.0000 321.04 30.5524 520.40 13.4478 722.78 6.5918 323.87 39.3713 520.69 0.0000 722.91 8.2401 325.23 44. 6696 522.65 0.0000 723. 31 8.2416 328.76 0.0000 527.90 0.0000 724 .19 6.5957 333.37 27.5031 528.26 10.5047 727. 33 12.1082 333.97 31.7490 529.59 18.0212 733.00 15.4475 334.37 33.0826 529.87 0.0000 735.93 9. 942 6 338.28 30.0862 531.02 0.0000 333.97 .15.4766 338.32 30.0869 537.26 0.0000 739.50 0.0000 311. 90 31.9102 546.56 0.0000 747.24 12.2098 340.48 31.9102 552.55 21. 2854 748.06 16.6553 340.55 0.0000 563.25 23.4436 752.31 23.3584 344.28 28.4473 569.33 20.4500 753.82 0.0000 345.93 29.9072 946.00 20.4517 756.73 24.5155 351.06 26.8066 569.70 20.4541 756.80 24.5164 351. 93 26.8237 583.19 18.5361 884.68 13. 4116 Page 3222 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 18.4551 1274.44 13.6844 1620.50 2.1527 766.42 18.4591 1001.03 7.3098 1621. 92 7.5370 766.84 18.4625 1002.74 13.1647 1678.03 0.0000 772. 60 0.0000 1004. '73 17.3817 1690.97 4.3708 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 8.8750 778.90 11. 2439 1028.54 0.0000 1063.66 7.7750 783.70 0.0000 1037.84 16.2733 1771. 35 2.2219 785.37 16.9098 1038.76 0.0000 1791.20 0.0000 792.07 8.4775 631. 29 9.2712 1808.65 2.2385 794.95 7. 9211 1048.07 0.0000 1810. 72 0.0000 795.86 7.9240 1049.04 15.7736 1836.06 5.4015 810.06 15.9363 1050.41 10. 2111 810.29 15.9380 1063.66 5.5928 344.28 10.2462 1077.00 0.0000 810.76 10.2477 1077.34 5.9906 815.77 0.0000 1085.87 13.5141 1048.07 0.0000 1093.63 15.0518. 832.01 19.5151 1099.45 7.5391 834.85 21. 8342 1112. 07 13. 2438 835.71 18.3932 1112. 84 18.9233 836.80 0.0000 1115. 54 10.6060 846.75 0.0000 1120.29 17.0695 846.77. 12.6982 1120. 55 17.0706 856.80 0.0000 1221.41 17.0739 860.56 10.4429 1129. 67 11. 4111 871.09 10.4832 1131. 51 0.0000 873.19 10.4912 1147.95 0.0000 875.33 0:0000 1173.23 13. 4830 879.38 9.6388 1177.95 13.5010 880.51 4.3831 1189.05 11. 608 9 883.24 18.4269 1204.77 14.5752 884.68 22.8262 1221. 41 15.6191 889.28 15.8291 1231.02 18.5964 894.76 14.0981 1235.36 0.0000 898.04 11. 4678 1238.28 19.6143 900.72 14.1279 1260.41 0.0000 903.28 13.2568 1271. 87 13.8556 911. 20 16.8395 1274.44 15.8457 912.08 16.8448. 1274.54 15.8457 923.98 0.0000 1291.59 8.9539 926.50 12.8312 1298.22 0.0000 929 .11 8.0266 1312 .11 0.0000 937.49 9.8388 1332. 49 8.0444 944.13 0.0000 1362.66 0.0000 946.00 11. 6618 1365.19 5. 0696 949.00 14.3677 1368. 63 0.0000 667. 71 0.0000 1384.29 9.1692 962. 31 11.5461 1408.01 6.1487 964.08 9.0259 1457.56 0.0000 966 .17 9.0323 1460.82 6.2278 911. 20 9.0408 1489.16 5.2246 968. 97 9.0408 1505.03 6. 292 6 983.53 0.0000 1584.12 7.4747 984.45 0.0000 1596.21 0.0000 Page 3223 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:16:33.43 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM12.CNF;467 Background date : Z-OCT-2016 11:00:40. Sample date 8-DEC-2015 11:29:00. Acquisition date : 3-0CT-2016 08:15:34. Sample ID G405235016 Sample quantity : l.63118E+02 GRAM ' Detector name : GAM12 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 9 2 9 3 9 4 .9 5 9 6 0 7 3 8 3 9 0 10 4 11 4 12 0 13 0 14 0 15 0 16 3 17 3 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 2 26 2 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 35.91* 37.68* 40.14 42.83 45.08 64.52* 75.00 77.26* 87.10 90.06 93.09* 154.32 157.46 185.62* 209.26 238.62* 241.60 258.15 271.20 295.06 338.33* . 351. 65* 408.91 432.57 443.52 446.21 462.58 491.73 510.37* 569.42 583.20* 609.25* 662.19 727. 24 Page 3224 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 31 50 72 27 17 14 120 148 30 53 108 31 23 61 29 399 122 13 32 171 76 232 26 10 20 24 29 14 58 39 122 146 28 46 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 8 40 77 145 86 166 192 135 170 68 169 65 92 137 90 86 90 62 112 58 57 75 97 31 7 26 45 17 36 60 26 44 58 35 1.15 1. 86 1. 78 2.60 1.17 0.62 1. 69 1.23 1. 23 1. 04 1. 90 1. 34 1. 37 1. 24 0.89 1. 28 1. 92 1. 41 0.80 1. 30 1.10 1. 38 5.41 1. 27 1. 28 1. 74 3.05 1. 73 1. 35 0.81 1. 31 1. 55 1. 02 1. 52 71. 66 75.20 80 .11 85.49 90.00 128.86 149.83 154.36 174.04 179.95 186.01 308.48 314.75 371.06 418.35 477.07 483.04 516 .13 542.23 589.98 676.52 703.18 817.70 865.05 886.95 892.32 925.07 983.40 1020.67 1138. 82 1166. 38 1218.51 1324.44 1454.59 Ei8 68 68 68 68 124 143 143 171 178 178 306 312 367 415 472 472 512 536 586 672 697 805 861 885 885 918 979 1013 1132 1160 1213 1320 1448 25 8.49E-03 43.5 2.41E+OO 25 1. 39E-02 41. 4 25 2.00E-02 28.2 25 7.47E-03 90.1 25 4.85E-03 81.1 8 3.90E-03163.9 17 3.33E-02 24.8 1.17E+OO 17 4.lOE-02 16.1 8 8.20E-03 78.4 16 1.48E-02 24.7 1.47E+OO 16 3.0lE-02 26.9 6 8.54E-03 45.7 8 6.48E-03 73.6 10 l.70E-02 39.1 8 7.98E-03 60.2 19 1.llE-01 6.5 1.02E+OO 19 3.40E-02 23.9 9 3. 62E-03112. 8 14 8.80E-03 73.9 10 4.75E-02 11.3 10 2.llE-02 22.3 12 6.46E-02 10.0 19 7.34E-03 92.5 8 2.74E-03100.0 17 5.51E-03 28.1 3.17E+OO 17 6.65E-03 45.9 14 8.03E-03 52.9 7 3.94E-03 55.4 16 1. 61E-02 31. 0 16 1.lOE-02 46.6 14 3.40E-02 13.0 15 4.04E-02 12.9 11 7.65E-03 56.8 16 1.27E-02 32.8 Peak Search Report (continued) Page : 2 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 795.02 25 11 1.10 1590.21 1584 11 7.0lE-03 32.3 36 0 862.42 39 30 4.43 1725.08 1717 19 1.08E-02 36.7 37 0 889.39 12 14 3.27 1779.06 1774 11 3.26E-03 68.0 38 0 911. 23* 78 20 1.10 1822.78 1817 13 2.15E-02 16.7 39 0 969.14 66 24 1. 25 1938.66 1932 14 1. 83E-02 20.1 40 0 996 .16 11 2 1. 63 1992.73 1989 7 3.14E-03 35.4 41 0 1104.74 15 2*0 0.53 2210.06 2202 16 4.07E-03 73.2 42 0 1120. 60 50 11 1. 39 2241. 80 2236 14 1.39E-02 19.8 43 0 1161.46 12 0 1. 60 2323.58 2320 7 3.33E-03 28.9 44 0 1181.87 11 27 3.93 2364.44 2352 19 2.97E-03123.2 45 0 1187. 67 16 5 2.39 2376.05 2372 9 4.46E-03 34.8 46 0 1194.48 20 2 3.89 2389.67 2385 11 5.49E-03 27.5 -4 7 0 1239.76 31 7 3.90 2480.31 2473 14 8.73E-03 25.2 48 0 1247*.01 21 7 2.11 2494.83 2488 13 5.69E-03 33.8 49 0 1460.74 336 0 1. 85 2922.71 2915 14 9.33E-02 5.5 50 0 1764.60 35. 7 1. 38 3531.13 3523 13 9.58E-03 22.8 51 0 2042.49 5 5 0.51 4087.70 4081 10 l.39E-03 94.9 Flag: "*" = Peak area was modified by background subtraction Page 3225 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:16:36 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 11:29:00 G405235016 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:15:34 163.12 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA12 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3226 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfere.d Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 .74. 82 74.82 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.082E+00 1.303E+Ol 1.303E+Ol 10.91 OK SC-46 889.28 99.98* 1.620E+OO 3.460E-02 4.135E-01 135. 97 OK 1120.55 99.99 l.350E+00 l.715E-01 2.049E+OO 39.59 OK BA-137M 661. 66 89.90* 2.040E+OO 7.427E-02 7.569E-02 113. 58 OK CS-137 661. 66 85.10* 2.040E+00 7.846E-02 7. 996E-02 113. 58 OK TL-208 277.37 6.60 4.142E+OO Line Not Found Absent 583.19 85.00* 2.256E+00 3.205E-01 3.205E-01 26.05 OK 860.56 12.50 l.662E+OO Line Not Found Absent PB-210 46.54 4.25* 3.130E-01 8.579E+OO 8.802E+OO 162.16 OK PB-212 74.82 10.28 3.186E+OO 1.562E+OO 1.562E+OO 73.17 OK 77 .11 17.10 3.414E+OO l.571E+OO 1.571E+OO 32.23 OK 238.63 43.60* 4.646E+OO 1.093E+OO l.093E+OO 12.91 OK 300.09 3.30 3.888E+OO Line Not Found Absent BI-214 609.32 45.49* 2.179E+OO 7.334E-01 7.336E-01 25. 80. OK 1120. 29 14.92 1.350E+OO 1.149E+OO 1.149E+OO 39.59 OK 1764.49 15.30 9 .121E-01 1.079E+OO 1.079E+OO 45.69 OK PB-214 74.82 5.80 3.167E+OO Line Not Found <<INT Reject 77 .11 9.70 3.414E+OO 2.769E+OO 2.770E+OO 32.23 OK 87.09 . 3. 41 4.297E+OO 1.237E+OO 1.238E+OO 15"6. 88 OK 242.00 7.25 4.599E+00 Line Not Found <<INT Reject 295.22 18.42 3.942E+OO 1.277E+OO 1.278E+OO 22.57 OK 351. 93 35.60* 3. 413E+OO 1. 017E+OO 1.018E+OO 20.10 OK RN-222 609.32 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 OK 1120.29 14.92 L 350E+OO 1.149E+OO 1.149E+OO 39.59 OK 1764.49 15.30 9.121E-01 l.079E+OO 1. 079E+OO 45.69 OK RA-224 240.99 4.10* 4.604E+OO 1.332E+OO 1.332E+OO 134. 55 OK RA-226 609.32 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 OK 1120.29 14.92 1.350E+OO 1.149E+OO 1.149E+OO 39.59 OK 1764.49 15.30 9 .121E-01 1.079E+OO 1.079E+OO 45.69 OK AC-228 105.21 1.10 5.379E+OO -----Line Not Found Absent 338.32 11. 27 3.524E+OO 1.021E+OO 1. 021E+OO 44.67 OK 794.95 4.25 1. 768E+OO 1.623E+OO 1.623E+OO 64.54 OK 835.71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1.589E+OO 8.986E-01 8.986E-01 33.41 OK 968. 97 15.80 1.514E+OO 1.298E+OO 1. 2 98E+OO 40.27 OK RA-228 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.524E+OO 1.021E+OO 1. 021E+OO 44.67 . OK 794.95 4.25 1. 768E+OO *1.623E+OO 1.623E+OO 64.54 OK 835.71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* L 589E+OO 8.986E-01 8.986E-01 33.41 OK 968. 97 *15.80 1.514E+OO l.298E+OO l.298E+OO 40.27 OK TH-228 74.82 10.28 3.186E+OO 1.562E+OO 1.562E+OO 73.17 OK 77 .11 17 _,10 3.414E+00 1. 571E+OO 1.571E+OO 32.23 OK 238.63 43.60* 4.646E+OO 1.093E+OO 1.093E+OO 12.91 OK 300.09 3.30 3.888E+OO Line Not Found Absent TH-230 609.32 4-S. 49* 2.179E+00 7.334E-01 7.334E-01 25.80 OK 1120.29 14.92 1.350E+OO 1.149E+00 1.149E+OO 39.59 OK 1764.49 15.30 9 .121E-01 1. 079E+OO 1. 079E+OO 45.69 OK TH-232 105.21 1.10 5.379E+OO Line Not Found Absent Page 3227 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM . pCi/GRAM %Error Status 338.32 11. 27 3.524E+OO 1.021E+OO 1. 021E+OO 44.67 OK 835. 71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1.589E+OO 8.986E-Ol 8.986E-01 33.41 OK 968. 97 15.80 l.514E+OO 1.298E+OO l.298E+OO 40.27 OK TH-234 63.29 3.70* 2.058E+OO 1.166E+OO *1.166E+OO 327.90 OK 92.59 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53.76 OK U-234 609.32 45.49* 2.179E+OO 7 *. 334E-01 7.334E-01 25.80 OK 1120.29 14.92 1.350E+OO l.149E+OO 1.149E+OO 39.59 OK 1764.49 15.30 9 .121E-01 l.079E+OO 1.079E+OO 45.69 OK U-235 89.96 3.47 4.522E+OO 2.083E+OO 2.083E+OO 49.42 OK 93.35 5.60 4.733E+OO 2.492E+OO 2.492E+OO 53.76 OK 143.76 10. 96* 5.929E+OO Line Not Found Absent 163.33 5.08 5.762E+OO Line Not Found Absent 185. 72 57.20 5.452E+OO 1.120E-01 l.120E-01 78.16 OK 205.31 5.01 5.147E+00 Line Not Found Absent U-238 63.29 3.70* 2.058E+OO 1.166E+OO 1.166E+OO 327.90 OK 92.59 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53. 76 OK AM-243 43.53 5.90 2.032E-01 1.471E+Ol 1.471E+Ol 180.12 OK 74.66 67.20* 3.186E+00 2.389E-01 2.390E-01 73.17 OK ANH-511 511. 00 100.00* 2. 511E+OO 1. l 77E-01 1. l 77E-01 62.00 OK Flag: "*" = Keyline Page 3228 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:16:37.62 *******************************************************************************

GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l *
Acquisition date 3-0CT-2016 08:15:34 Sensitivity : 3.000 *
Detector ID GAM12 . Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 8-DEC-2015 11:29:00 Analyst initials: MXRl *
Sample ID G405235016 Sample Quantity
1.6312E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN * *'Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.303E+Ol 1. 394E+OO SC-46 4.135E-01 5.510E-01 BA-137M 7.569E-02 8.424E-02 CS-137 7.996E-02 8.900E-02 TL-208 3.205E-01 8 .181E-02 PB-210 8.802E+OO 1.399E+Ol PB-212 1.093E+OO l.382E-01 BI-214 7.336E:--01 1.855E-01 PB-214 1.018E+OO 2.004E-01 RN-222 ].336E-01 l.855E-01 RA-'-224 1.332E+OO 1.756E+OO RA-226 7.336E-01 1.855E-01 AC-228 8.986E-01 ,2.943E-01 RA-228 8.986E-01 2 .*943E-01 TH-228 1.093E+OO 1.382E-01 TH-230 7.334E-01 1.855E-01 TH-232 8.986E-01 2.943E-01 TH-234 1.166E+OO 3.747E+OO U-234 7.334E-01 1.855E-01 U-235 4.023E-02 1. 760E-01 U-238 l.166E+OO 3.747E+OO AM-243 2.390E-01 1. 713E-01 ANH-511 l.177E-01 7.154E-02 Non-Identified Nuclides Nuclide BE-7 NA-22* NA-24 AL-26 V-48 CR-51 MN-54 Page 3229 of 5809 Key-Line Activity (pCi/GRAM -5.074E-01 3.326E-02 O.OOOE+OO -1.662E-02 O.OOOE+OO 0.000E+OO 1. 791E-02 K.L. Cnt Uncert ( 1. 96-sigma) l.269E+Ol 4.387E-02 1. 960E+41 2.829E-02 l.393E+04 3.755E+02 5.843E-02 MDA (pCi/GRAM 3.757E-01 7.481E-01 8.137E-02 8. 596E-02 5.564E-02 1.482E+Ol 9.363E-02 1.137E-01 1.354E-01 1.137E-01 1.003E+OO l.137E-01 1.842E-01 1.842E-01 9.363E-02 l.136E-01 1.842E-01 3.551E+OO. 1.136E-01 3.561E-01 3.551E+00 1.220E-01 4.450E-02 MDA (pCi/GRAM 2.412E+Ol 9.885E-02 O.OOOE+OO 4.921E-02 0.000E+OO. O.OOOE+OO l.232E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1. 676E-01 4.422E-01 9.416E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.561E-02 4.717E-02 9.092E-02 NOT IDENT. C0-58 -1. 599E-01 4.577E-01 8.989E-01 NOT IDENT. FE-59 3.785E+OO 5.186E+OO l.151E+Ol NOT IDENT. C0-60 l.572E-02 3.574E-02 7.896E-02 NOT IDENT. ZN-65 -3.473E-02 f.851E-01 3.122E-01 NOT IDENT. GE-68 1. 709E-01 2.145E+OO 4.394E+OO NOT IDENT. AS-73 -9.140E+OO 1.748E+Ol 3.136E+Ol NOT IDENT. AS-74 O.OOOE+OO 6 .114E+03 O.OOOE+OO SHORT HLIF SE-75 -l.278E-02 1.970E-01 3.815E-01 NOT IDENT. BR-77 O.OOOE+OO 2.513E+37 0.000E+OO SHORT HLIF SR-82 0.000E+OO 6.420E+02 O.OOOE+OO SHORT HLIF RB-83 2.473E-01 7.246E-01 l.428E+OO NOT IDENT. KR-85 7.898E+OO 6.575E+00 1.362E+Ol NOT IDENT. SR-85 8.337E-01 6.948E-01 l.439E+OO NOT IDENT. RB-86 O.OOOE+OO 2.513E+04 0. OOOE*+oo SHORT HLIF Y-88 -l.189E-01 1. 34 6E-01 1.009E-01 NOT IDENT. Y-91 l.635E+02 5.205E+02 1.077E+03 NOT IDENT. NB-94 1. 7 64E-02 3.342E-02 6.702E-02 NOT IDENT. NB-95 -2.185E-03 8.650E-01 1. 727E+OO NOT IDENT. NB-95M -1.185E+OO 2.737E+OO 4.532E+OO NOT IDENT. ZR-95 -4.0lOE-01 1.203E+OO 2.179E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 6.b34E+40 O.OOOE+OO SHORT HLIF M0-99 .o. OOOE+OO 1. 711E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1.426E+41 O.OOOE+OO SHORT HLIF RH-101 -2. 472E-02 3.403E-02 6:454E-02 NOT IDENT. RH-102 4.147E-03 6.179E-02 1.181E-01 NOT IDENT. RU-103 7.210E-01 5.736E+OO l .115E+Ol FAIL ABUN RH-106 -4. 231E-04 5 .113E-01 9.706E-01 NOT IDENT. RU-106 -4. 231E-04 5 .113E-01 9.706E-01 NOT IDENT. AG-108M 1. 970E-:-02 3.860E-02 5.205E-02 FAIL ABUN CD-109 1.789E+00 2.751E+00 2.923E+OO FAIL ABUN AG-llOM 6.783E-03 1.103E-01 1.991E-01 NOT IDENT. SN-113 -9.909E-02 2.278E-01 4.167E-01 NOT IDENT. CD-115 O.OOOE+OO 3 .111E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.682E+05 O.OOOE+OO SHORT HLIF TE-123M -3.086E-02 1.478E-01 2.567E-01 NOT IDENT. SB-124 -8.270E-01 2.224E+OO 4.163E+OO NOT IDENT. SB-125 5. BllE-02 1.160E-01 2.134E-01 FAIL ABUN TE-125M l.391E+02 2.888E+02 5. 969E+02 NOT IDENT. I-126 O.OOOE+OO 1.205E+06 0 .. OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.273E+06 O.OOOE+OO SHORT HLIF SN-126 1.140E-01 1.753E-01 l.916E-01 FAIL ABUN SB-127 O.OOOE+OO 2.169E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 4.777E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.871E+26 O.OOOE+OO SHORT HLIF BA-133 1.772E-02 4.090E-02 7. 551E-02 NOT IDENT. I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 l.063E-01 6.721E-02 1.082E-01 FAIL ABUN CS-135 8. OllE-02 l.432E-01 2.662E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.416E+05 O.OOOE+OO SHORT HLIF CE-139 8.136E-03 1.051E-01 2.085E-01 NOT IDENT. BA-140 O.OOOE+OO 1.186E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.593E+05 O.OOOE+OO SHORT HLIF CE-141 -1.706E+Ol 2.422E+Ol 4.565E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.559E+40 0. 00 OE+OO. SHORT HLIF CE-144 8.743E-02 3.465E-01 7. 021E-01 NOT IDENT. PM-144 2.444E-03 4.852E-02 9.377E-02 NOT IDENT. PR-144 -6.480E-01 4.365E+OO 8.130E+OO NOT IDENT. PM-146 -9. 711E-03 3.995E-02 7.109E-02 NOT IDENT. ND-147 O.OOOE+OO 3.585E+07 O.OOOE+OO SHORT HLIF PM-147 -2.014E+02 8.307E+02 1.635E+03 NOT IDENT. PM-149 O.OOOE+OO 4.587E+40 O.OOOE+OO SHORT HLIF EU-150 2.263E-02 2.525E-02 4.915E-02 FAIL ABUN EU-152 -4.763E-03 9.819E-02 l.874E-01 NOT IDENT. GD-153 3.764E-02 l.940E-01 3.607E-01 NOT IDENT. EU-154 7.458E-02 1.061E-01 2.380E-01 FAIL ABUN EU-155 1.808E-02 1.089E-01 2.221E-01 FAIL ABUN TB-160 -1.413E+OO 1.475E+OO 2.526E+OO FAIL ABUN H0-166M 2.079E-02 5.761E-02 1.144E-01 FAIL ABUN TM-171 -3.003E+Ol 4.271E+Ol 7.545E+Ol NOT IDENT. HF-172 -9.750E-02 2.359E-01 4.575E-01 NOT IDENT. LU-172 7.676E-02 5.341E-02 l.409E-01 FAIL ABUN LU-176 -6.849E-03 2.260E-02 4.256E-02 FAIL ABUN Page 3230 of 5809 HF-181 -2.950E+OO 4.400E+00 7.685E+OO NOT IDENT. TA-182 3.397E-02 8.497E-01 1.701E+OO FAIL ABUN RE-183 -3.033E+OO 5.074E+00 8.999E+OO NOT IDENT. RE-184 -9.960E+00 2.832E+Ol 5.441E+Ol NOT IDENT. W-188 1.869E+Ol 1.254E+02 2.204E+02 FAIL ABUN IR-192 -2.217E-01 4.445E-01 7.900E-01 FAIL ABUN HG-203 -5.593E-01 2.547E+00 4. 813E+OO NOT IDENT. BI-207 -1.147E-02 4.946E-02 9.508E-02 FAIL ABUN BI-211 O.OOOE+OO 5.521E-01 8.615E-01 FAIL ABUN PB-211 7.166E-01 6.909E-01 1.458E+OO NOT IDENT. BI-212 O.OOOE+OO 1.137E+OO 1.394E+OO FAIL ABUN RN-219 -2.873E-01 4.540E-01 7.021E-01 FAIL ABUN RA-223 1.044E-01 5 .. 3S7E-01 1. 066E+OO FAIL ABUN AC-227 1. 571E-01 2.269E-01 4.306E-01 NOT IDENT. TH-227 1.571E-01 2.269E-01 4.306E-01 NOT IDENT. TH-229 4.188E-01 4.920E-01 1. OllE+OO FAIL ABUN PA-231 -2.591E-01 4 .113E-01 7.474E-01 NOT IDENT. TH-231 1.044E-01 5.387E-01 1.066E+OO FAIL ABUN PA-233 -2.076E-02 5. 396E-02 l.OOSE-01 NOT IDENT. PA-234 -4.241E-03 1.812E-01 3.856E-01 FAIL ABUN PA-234M -6 .112E-01 3. 785E+OO* 7.418E+OO NOT IDENT. NP-237 -2.076E-02 5.396E-02 1.008E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.730E-02 2.438E-01 4.938E-01 NOT IDENT. PU-239 1.282E+02 3 .112E+02 6.352E+02 NOT IDENT. AM-241 -8.076E-02 2.236E-01 4.049E-01 NOT IDENT. CM-243 -6.819E-02 9.733E-02 l.873E-01 NOT IDENT. BK-247 l.640E-02 6.957E-02 1.328E-01 NOT IDENT. CM-247 1.891E-02 3.598E-02 6.701E-02 NOT IDENT. CF-249 4.479E-02 3. 711E-02 8.006E-02 NOT IDENT. CF-251 7. 996E-02 l.141E-01 2.346E-01 NOT IDENT. Page 3231 of 58Q9 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:16:34.41 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 327 10.66* 1.082E+OO 1.303E+Ol l.303E+Ol 10.91 SC-46 889.28 12 99.98* 1. 620E+OO 3.460E-02 4.135E-01 135.97 1120.55 50 99.99 1.350E+OO 1. 715E-01 2.049E+OO 39.59 CD-109 8.8. 03 39 3.70* 4.297E+OO 1.140E+OO 1. 789E+OO 156.88 SN-126 64.28 19 9.60 2.058E+OO 4.494E-01 4.494E-01 327.90 86.94 39 8.90 4.297E+OO 4.741E-01 4. 741E-01 156.88 87.57 39 37.00* 4.297E+OO l.140E-01 1.140E-01 156.88 BA-137M 661.66 30 89.90* 2.040E+OO 7.427E-02 7.569E-02 113. 58 CS-137 661. 66 30 85.10* 2.040E+OO 7.846E-02 7.996E-02 113.58 TL-208 277.37 ------6.60 4.142E+OO ------Line Not Found ------583.19 134 85.00* 2.256E+OO 3.205E-01 3.205E-01 26. 05 860.56 ------12.50 1.662E+OO ------Line Not Found ------PB-210 46.54 25 4.25* 3.130E-01 8.579E+OO 8.802E+OO 162.16 BI-211 72. 87 ------1.23 2. 964E+Od ------Line Not Found ------351.06 269 12.92* 3.413E+OO 2.803E+OO 2.803E+OO 20.10 PB-212 74.82 162 10*. 28 3.186E+OO 2.282E+OO 2.282E+OO 49.58 77 .11 199 17.10 3.414E+OO

1. 571E+OO 1. 571E+OO 32.23 238.63 481 43.60* 4.646E+OO 1.093E+OO 1.093E+OO 12.91 300.09 ------3.30 3.888E+OO ------Line Not Found ------BI-214' 609.32 158'. 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 1120.29 50 14.92 1.350E+OO l.149E+00 1.149E+OO 39.59 1764.49 33 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 PB-214 74.82 162 5.80 3.186E+OO 4.045E+OO 4.046E+OO 49.58 77 .11 199 9.70 3.414E+OO 2.769E+OO 2.770E+00 32.23 87.09 39 3.41 4.297E+OO 1.237E+OO 1.238E+OO 156.88 242.00 147 7.25 4.604E+OO 2. 031E+OO 2. 031E+OO 47.85 295.22 201 18.42 3.942E+OO 1.277E+OO 1.278E+OO 22.57 351.93 269 35.60* 3.413E+OO 1. 017E+OO 1.018E+OO 20.10 RN-222 609.32 158 45.49* 2.179E+OO 7. 334.E-01 7.336E-01 25.80 1120.29 50 14.92 l.350E+OO l.149E+OO 1.149E+OO 39.59 1764.49 33 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 RA-224 240.99 147 4.10* 4.604E+OO 3.591E+OO 3. 591E+OO 47.85 RA-226 609.32 158 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 1120.29 50 14.92 l.350E+00 1.149E+OO 1.149E+OO 39.59 1764.49 33 15.30 9.121E-01 l.079E+00 1.079E+OO 45.69 AC-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 88 11. 27 3.524E+OO 1.021E+OO 1. 021E+OO 44.67 794.95 26 4.25 1. 768E+OO 1.623E+OO l.623E+OO 64.54 835. 71 ------1. 61 1. 701E+OO ------Line Not Found ------911. 20 80 25.80* 1.589E+OO 8.986E-01 8.986E-01 33.41 968. 97 67 15.80 l.514E+00 1.298E+OO l.298E+OO 40.27 RA-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 88 11. 27 3.524E+OO l.021E+OO 1. 021E+OO 44.67 794.95 26 4.25 1.768E+OO 1.623E+OO l.623E+OO 64.54 835. 71 ------1. 61 1. 701E+OO ------Line Not Found ------911.20 80 25.80* 1.589E+OO 8.986E-01 8.986E-01 33.41 968. 97 67 15.80 1.514E+OO 1.298E+OO l.298E+OO 40.27 Page 3232 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 162 10.28 3.186E+OO 2.282E+OO 2.282E+OO 49.58 77 .11 199 17.10 3.414E+OO 1.571E+OO 1.571E+OO 32.23 238.63 481 43.60* 4.646E+OO 1. 093E+OO . 1. 093E+OO 12.91 300.09 ------3.30 3.888E+OO ------Line Not Found ------TH-230 609.32 158 45.49* 2.179E+OO 7.334E-01 7.334E-01 25.80 1120. 29 50 14.92 l.350E+OO 1.149E+OO 1.149E+OO 39.59 1764.49 33 15.30 9.121E-01 1.079E+OO 1. 079E+OO 45.69 TH-232 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 .88 11. 27 3.524E+OO 1.021E+OO 1.021E+OO 44*_ 67 835.71 ------1. 61 1. 701E+OO ------Line Not Found ------911.20 80 25.80* 1.589E+OO 8.986E-01 8.986E-01 33.41 968. 97 67 15.80 1.514E+OO 1.298E+OO 1.298E+OO 40.27 TH-234 63.29 19 3.70* 2.058E+OO 1.166E+OO 1.166E+OO 327.90 92.59 144 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53.76 U-234 609.32 158 45.49* 2.179E+OO 7.334E-01 7.334E-01 25. 80 1120.29 50 14.92 1.350E+OO 1.149E+OO 1.149E+OO 39.59 1764.49 33 15.30 9.121E-01 1.079E+OO 1. 079E+OO 45.69 U-235 89. 96 71 3.47 4.522E+OO 2.083E+OO 2.083E+OO 49.42 93.35 144 5.60 4.733E+OO 2.492E+OO 2.492E+OO 53.76 143.76 ------10.96* 5.929E+OO ------Line Not Found ------163.33 ------5.08 5.762E+OO ------Line Not Found ------185. 72 76 57.20 5.452E+OO 1.120E-01 1.120E-01 78.16 205.31 ------5.01 5.147E+OO ------Line Not Found ------U-23*3 63.29 19 3.70* 2.058E+OO 1.166E+OO 1.166E+OO 327.90 92.59 144 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53.76 AM-243 43.53 38 5.90 2.032E-01 1.471E+Ol 1. 471E+Ol 180.12 74.66 162 67.20* 3.186E+OO 3.491E-01 3.491E-01 49.58 ANH-511 511. 00 64 100.00* 2. 511'E+OO 1.177E-01 1.177E-01 62.00 Flag: "*" Key line Page 3233 of 5809 Summary of Nuclide Activity Sample ID : G405235016 Acquisition date Page : 3 3-0CT-2016 08:15:34 Total number of lines in spectrum 51 Number of unidentified lines 15 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 83.79D 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+10Y 1600. OOY l.41E+l0Y l.41E+10Y 1.41E+10Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 12.0 1. 57 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.303E+Ol 3.460E-02 l.140E+OO l.140E-Oi 7.427E-02 7.846E-02 3.205E-01 8.579E+OO 2.803E+OO 1.093E+OO, 7.334E-01 1.017E+OO 7.334E-01 3.591E+OO 7.334E-01 8.986E-01 8.986E-01 1.093E+OO 7.334E-01 8.986E-01 1.166E+OO 7.334E-01 1.120E-01 1.166E+OO 3.491E-01 l.177E-01 4.225E+Ol 4.225E+Ol Decay Corr pCi/GRAM l.303E+Ol 4.135E-01 1. 789E+OO 1.140E-01 7.569E-02 7. 996E-02 3.205E-01 8.802E+OO 2.803E+OO 1. 093E+00 7. 33 6E-0-l 1.018E+OO 7.336E-01 3. 591E+OO 7.336E-01 8.986E-01 8.986E-01 1.093E+OO 7.334E-01 8.986E-01 1.166E+OO 7.334E-01 1.120E-01 1.166E+OO 3.491E-01 1.177E-01 4.350E+Ol 4.350E+Ol 70.59% Decay Corr 2-Sigma Error 0.142E+Ol 5.622E-01 2.807E+OO 1. 789E-01 8.596E-02 9.081E-02 0.835E-01 14.27E+OO 0.563E+OO 0.141E+OO 1. 893E-01 0.205E+OO l.893E-01 1.718E+OO 1.893E-01 3.003E-01 3.003E-01 0.141E+OO 1.892E-01 3.003E-01 3.824E+OO 1.892E-01 0.876E-01 3.824E+OO 1. 731E-01 0.730E-01 "M" Manually 2-Sigma %Error 10.91 135.97 156.88 156.88 113. 58 113. 58 26.05 162.16 20.10 12.91 25.80 20.10 25.80 47.85 25.80 33.41 33.41 12.91 25.80 33.41 327.90 25.80 78.16 327.90 49.58 62.00 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3234 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235016 Acquisition date : 3-0CT-2016 08:15:34 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 9 35.91 44 11 1.15 71. 66 68 25 8.49E-03 87.0 2.40E-02 9 37.68 72 58 1. 86 75.20 68 25 1.39E-02 4.91E-02 9 40.14 103 111 1. 78 80 .11 68 25 2. OOE-*02 56. 4 1.06E-01 0 154.32 39 82 1. 34 308.48 306 6 8. 54E-03 91. 3 5.86E+OO T 0 157.46 29 115 1. 37 314.75 312 8 6.48E-03 **** 5.83E+OO T 0 209.26 35 110 0.89 418.35 415 8 7.98E-03 **** 5.09E+OO 0 258.15 16 74 1. 41 516.13 512 9 **** 4.38E+00 0 271. 20 38 133 0.80 542.23 536 14 8.80E-03 **** 4.22E+OO T 0 408.91 30 110 5.41 817.70 805 19 7.34E-03 **** 3.0lE+OO 0 432.57
11 35 1. 27 865.05 861 8 2.74E-03 **** 2.87E+OO T 2 443.52 22 8 1. 28 886.95 885 17 5.51E-03 56.2 2.82E+OO 2 446.21 27 30 1. 74 892.32 885 17 6.65E-03 91.8 2.80E+OO 0 462.58 32 '51 3.05 925.07 918 14 8.03E-03 **** 2. 72E+OO T 0 491. 73 16 19 1. 73 983.40 979 7 3.94E-03 **** 2.59E+OO T 0 569.42 43 65 0.81 1138.82 1132 16 1.lOE-02 93.2 2.30E+OO T 0 727.24 49 38 1. 52 1454.59 1448 16 1.27E-02 65.7 1. 90E+OO T 0 862.42 41 31 4.43 1725.08 1717 19 1.08E-02 73.4 1. 66E+OO 0 996 .16 12 2 1. 63 1992.73 1989 7 3 . 14 E-0 3 .7 0 . 9 1. 48E+OO T 0 1104.74 15 21 0.53 2202 16 4.07E-03 **** 1.37E+OO 0 1161.46 12 0 1. 60 2323.58 2320 7 3.33E-03 57.7 1. 31E+OO 0 1181.87 11 27 3.93 2364.44 2352 19 2.97E-03 **** 1.29E+OO 0 1187. 67 16 5 2.39 2372 9 4.46E-03 69.5 1.29E+OO T 0 1194.48 20 2 3.89 2389.67 2385 11 5.49E-03 55.0 1.28E+OO 0 1239.76 31 7 3.90 2480.31 2473 14 8.73E-03 50.3 l.24E+00 T 0 1247.01 20 6 2.11 2494.83 2488 13 5.69E-03 67.7 l.24E+'OO 0 2042.49 5 5 0. 51. 4087.70 4081 10 1.39E-03 **** 7.90E-01 Flags: "T" = Tentatively associated Page 3235 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:16:51.97 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
*
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l * *Acquisition date 3-0CT-2016 08:15:34 Sensitivity 3.000 *
Detector ID GAM12 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 8-DEC-2015 11:29:00 Nuclide Library : SOLID *
Sample ID G405235016 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.6312E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 22-SEP-2016 11: 41: 01 Eff. Geometry . : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.333E-01 3.270E-01 3.712E-02 3. 921E-02 2.445E-02 6.990E+OO 4.355E-02 5.033E-02 6.229E-02 5.033E-02 4.667E-01 5.033E-02 7.656E-02 7.656E-02 4.355E-02 5.032E-02 7.656E-02 1. 679E+OO 5.032E-02 1. 678E-01 1. 679E+OO 5.778E-02 1. 967E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 Page 3236 of 5809 Le (pCi/GRAM 1.089E+Ol 4.296E-02 O.OOOE+OO 1. 757E-02 O.OOOE+OO O.OOOE+OO 5.428E-02 4.148E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3237 of 5809 O.OOOE+OO 4.257E-02 3.800E-01 4.882E+00 3.348E-02 l.344E-01 1.893E+OO 1.472E+Ol O.OOOE+OO 1. 760E-01 O.OOOE+OO O.OOOE+OO 6.490E-01 6 .181E+OO 6. 531E-01 O.OOOE+OO 0.000E+OO 4. 719E+02 3.021E-02 7.729E-01 2.120E+OO 9.246E-01 O.OOOE+OO 0.000E+OO 0.000E+OO O.OOOE+OO 3.028E-02 5.275E-02 5.023E+OO 4.324E-01 4.324E-01 2.352E-02 1. 396E+OO 8. 716E-02 1.887E-01 O.OOOE+OO O.OOOE+OO 1. 2'05E-01 1.644E+OO 9.747E-02 2.816E+02 O.OOOE+OO O.OOOE+OO 9.158E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.446E-02 O.OOOE+OO 4.854E-02 l.234E-01 O.OOOE+OO O.OOOE+OO 9.768E-02 O.OOOE+OO O.OOOE+OO 2.143E+Ol 0.000E+OO 3.299E-01 4.105E-02 3.558E+OO 3.153E-02 O.OOOE+OO 7.674E+02 O.OOOE+OO 2.263E-02 8. 631E-02 1. 693E-01 l.032E-01 l.043E-01 1.033E+OO. 5.106E-02 3.537E+Ol 2.150E-01 6.052E-02 l.944E-02 3.429E+00 SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN *NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-.211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3238 of 5809 7.361E-01 4.214E+00 2.349E+Ol l.021E+02 3.594E-01 2.237E+OO 4.139E-02 4.161E-01 6. 722E-01 6.466E-01 3.187E-01 4.883E-01 l.995E-01 l.995E-01 4.774E-01 3.420E-01 4.883E-01 4.586E-02 1. 584E-01 3 .196E+OO 4.586E-02 O.OOOE+OO 2. 321E-01 2. 996E+02 1. 899E-01 8.741E-02 6.126E-02 3.054E-02 3.689E-02 l.104E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:16:58.06 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l *
Acquisition date 3-0CT-2016 08:15:34 Sensitivity : 3.000 *
Detector ID GAM12 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed time: 0 01:00:00.56 Half ratio : ***** *
Sample date 8-DEC-2015 11:29:00 Nuclide Library : SOLID *
Sample ID G405235016 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity 1.6312E+02 GRAM' *
Quantity Err(%) 1.2261E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.303E+Ol l.552E+OO SC-46 4.135E-01 5.513E-01 BA-137M 7.569E-02 8. 431E-02 CS-137 7. 996E-02 8.906E-02 TL-208 3.205E-01 8.295E-02 PB-210 8.802E+OO l.404E+Ol PB-212 1.093E+OO l.503E-01 BI-214 7.336E-01 1.882E-01 PB-214 1.018E+00 2.050E-01 RN-222 7.336E-01 l.882E:...01 RA-224 1.332E+OO 1.764E+OO RA-226 . 7. 336E-01 1.882E-01 AC-228 8.986E-01 2.979E-01 RA-228 8.986E-01 2.979E-01 TH-228 1.093E+OO 1.503E-01 TH-230 7.334E-01 1. 881E-01 TH-232 8.986E-01 2.979E-01 TH-234 l.166E+00 3.756E+OO U-234 7.334E-01 1. 881E-01 U-235 4.023E-02 1. 760E-01 U-238 1.166E+OO 3.756E+OO AM-243 2.390E-01 1.726E-01 ANH-511 l.177E-01 7.170E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 Page 3239 of 5809 Key-Line Activity (pCi/GRAM -5.074E-01 3.326E-02 1.000E+41 -1.662E-02 -7.597E+03 4.549E+Ol 1. 791E-02 K.L Act error (1.96-sigma) 1.269E+Ol 4.388E-02 4.275E+41 2. 831E-02* 1.393E+04 3.755E+02 5.844E-02 TPU ( 1 . 96-sigma ) 1.552E+OO 5.513E-01 8. 431E-02 8.906E-02 8.295E-02 1.404E+Ol 1.503E-01 l.882E-01 2.050E-01 1. 882E-01 1. 7 64E+OO 1. 882E-01 2.979E-01 2.979E-01 1.503E-01 1.881E-01 2.979E-01 3.756E+OO 1. 881E-.Ol 1. 760E-01 3.756E+OO 1. 726E-01 7.170E-02 TPU (1. 96-sigma) l.269E+Ol 4.637E-02 O.OOOE+OO 2.929E-02 1.435E+04 3.761E+02 5.899E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1. 67 6E-01 4.423E-01 4.487E-01 FAIL ABUN MN-56 l.OOOE+41 2.640E+41 O.OOOE+OO SHORT HLIF C0-57 -2.561E-02 4.718E-02 4.857E-02 NOT IDENT. C0-58 -1.599E-01 4.578E-01 4.634E-01 NOT IDENT. FE-59 3.785E+OO 5.193E+OO 5.466E+OO NOT IDENT. C0-60 1.572E-02 3.575E-02 3.644E-02 NOT IDENT. ZN-65 -3.473E-02 1.851E-01 1.857E-01 NOT IDENT. GE-68 1. 709E-01 2.145E+OO 2.146E+OO NOT IDENT. AS-73 -9 .140E+OO' 1. 758E+Ol l.806E+Ol NOT IDENT. AS-74 -8.607E+02 6.115E+03 6.127E+03 SHORT HLIF SE-75 -1.278E-02 1.971E-01 1.971E-01 NOT IDENT. BR-77 1.987E+38 1. 720E+39 O.OOOE+OO SHORT HLIF SR-82 l.105E+02 6.420E+02 6.439E+02 SHORT HLIF RB-83 2.473E-01 7.254E-01 7.339E-01 NOT IDENT. KR-85 7.898E+OO 6.583E+OO 7.484E+OO NOT IDENT. SR-85 8.337E-01 6.9S7E-01 7.907E-01 NOT IDENT. RB-86 3.294E+03 2.513E+04 2.517E+04 SHORT HLIF Y-88 -1.189E-01 1.348E-01 1.451E-01 NOT IDENT. Y-91 1.635E+02 5.205E+02 5.257E+02 NOT IDENT. NB-94 1. 764E-02 3.343E-02 3.436E-02 NOT IDENT. NB-95 -2.185E-03 8.650E-01 8.650E-01 NOT IDENT. NB-95M -1.185E+OO 2.739E+OO 2.791E+00 NOT IDENT. ZR-95 -4.0lOE-01 1.203E+OO l.216E+OO NOT IDENT. NB-97 1.000E+41 3.541E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 6.048E+40 0.000E+OO SHORT HLIF M0-99 8.346E+31 1.712E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.430E+41 O.OOOE+OO SHORT HLIF RH-101 -2.472E-02 3.432E-02 3.609E-02 NOT IDENT. RH-102 4.147E-03 6.179E-02 6;182E-02 NOT IDENT. RU-103 7.210E-01 5.736E+OO 5.745E+00 FAIL ABUN RH-106 -4. 231E-04 5 5.113E-01. NOT IDENT. RU-106 -4. 231E-04 5 .113E-01 5 .113E-01 NOT IDENT. AG-108M 1.970E-02 3.860E-02 3. 961E-02 FAIL ABUN CD-109 l.789E+OO 2.755E+OO 2.870E+OO FAIL ABUN AG-llOM 6.783E-03 1.103E-01 1.103E-01 NOT IDENT. SN-113 -9.909E-02 2.279E-01 2.322E-01 NOT IDENT. CD-115 2.004E+39 3.132E+39 O.OOOE+OO SHORT HLIF SN-117M 1.166E+05 1.688E+05 1. 768E+05 SHORT HLIF TE-123M -3.086E-02 l.478E-01 1.485E-01 NOT IDENT. SB-124 -8.270E-01 2.224E+OO 2.255E+OO NOT IDENT. SB-125 5. 811E-02 1.160E-01 1.190E-01 FAIL ABUN TE-125M 1.391E+02 2.889E+02 2.956E+02 NOT IDENT. I-126 2.344E+05 l.205E+06 1.210E+06 SHORT HLIF SB-126 -2.180E+05 1.273E+06 1.277E+06 SHORT HLIF SN-126 1.140E-01 1.755E-01 1.828E-01 FAIL ABUN SB-127 4.336E+21 2.249E+22 O.OOOE+OO SHORT HLIF I-131 -3.454E+09 4.780E+09 5.027E+09 SHORT HLIF I-132 1.000E+41 1. 911E+42 O.OOOE+OO SHORT HLIF TE-132 -l.587E+25 3.871E+26 O.OOOE+OO SHORT HLIF BA-133 1. 772E-02 4.091E-02 4.168E-02 NOT IDENT. I-133 1.000E+41 4.029E+41 0.000E+OO SHORT HLIF CS-134 l.063E-01 6.737E-02 8.266E-02 FAIL ABUN CS-135 8. OllE-02 1.433E-01 l.478E-01 NOT IDENT. I-135 l.OOOE+41 1.016E+42 O.OOOE+OO SHORT HLIF CS-136 -l.033E+04 2.416E+05 2.417E+05 SHORT HLIF CE-139 8.136E-03 1.051E-01 1. 051E-01 NOT IDENT. BA-140 8.733E+05 1.187E+o6 l.250E+06 SHORT HLIF LA-140 -2.688E+05 4.595E+05 4.752E+05 SHORT HLIF CE-141 -l.706E+01 2.423E+Ol 2.542E+Ol NOT IDENT. CE-143 l.OOOE+41 5.652E+40 O.OOOE+OO SHORT HLIF CE-144 8.743E-02 3.466E-01 3.488E-01 NOT IDENT. PM-144 2.444E-03 4.852E-02 4.853E-02 NOT IDENT. PR-144 -6.480E-01 4.365E+OO 4.375E+OO NOT IDENT. PM-146 -9. 711E-03 3.995E-02 4.019E-02 NOT IDENT. ND-147 7.457E+06 3.585E+o7 3. 601E+07 SHORT HLIF PM-'147 -2.014E+02 8.307E+02 8.357E+02 NOT IDENT. PM-149 2.545E+38 4.587E+40 O.OOOE+OO SHORT HLIF EU-150 2.263E-02 2.527E-02 2.725E-02 FAIL ABUN EU...:.152 -4.763E-03 9.819E-02 9.822E-02 NOT IDENT. GD-153 3.764E-02 1.941E-01 1.948E-01 NOT IDENT. EU-154 7.458E-02 l.061E-01 1.113E-01 FAIL ABUN EU-155 1.808E-02 1. 089E-01 1.092E-01 FAIL ABUN TB-160 -l.413E+OO 1.477E+OO l.609E+OO FAIL ABUN H0-166M 2.079E-02 5.762E-02 5.838E-02 FAIL ABUN TM-171 -3.003E+Ol 4.280E+Ol 4.489E+Ol NOT IDENT. HF-172 -9.750E-02 2.365E-01 2.405E-01 NOT IDENT. LU-172 7.676E-02 5.397E-02 6.411E-02 FAIL ABUN LU-176 -6.849E-'03 2.260E-02 2.281E-02 FAIL ABUN Page 3240 of 5809 HF-181 -2.950E+OO 4.402E+OO 4.599E+OO NOT IDENT. TA-182 3.397E-02 8.497E-01 8.498E-01 FAIL ABUN RE-183 -3.033E+OO 5.097E+OO 5.277E+OO NOT IDENT. RE-184 -9.960E+OO 2.842E+Ol 2.877E+Ol NOT IDENT. W-188 1. 8 69E+Ol 1.254E+02 l.257E+02 FAIL ABUN IR-192 -2.217E-01 4.446E-01 4.557E-01 FAIL ABUN HG-203 -5.593E-01 2.547E+OO 2.560E+OO NOT IDENT. BI-207 -1.14 7E-02 4.946E-02 4.973E-02 FAIL ABUN BI-211 2.803E+OO 5.666E-01 1.385E+OO FAIL ABUN PB-211 7.166E-01 6.919E-01 7.636E-01 NOT IDENT. BI-212 1. 766E+OO 1.140E+OO 1. 391E+OO FAIL ABUN RN-219 -2.873E-01 4.555E-01 4.735E-01 FAIL ABUN RA-223 1.044E-01 5.388E-01 5.408E-01 FAIL ABUN AC-227 1.571E-01 2.279E-01 2.386E-01 NOT IDENT. TH-227 1.571E-01 2.279E-01 2.386E-01 NOT IDENT. TH-229 4.188E-01 4.924E-01 5.274E-01 FAIL ABUN PA-231 -2.591E-01 4.150E-01 4.312E-01 NOT IDENT. TH-231 l.044E-01 5.388E-01 5.408E-01 FAIL ABUN PA-233 -2.076E-02 5.397E-02 5.478E-02 NOT IDENT. PA-234 -4.241E-03 1.813E-01 l.813E-01 FAIL ABUN PA-234M -6.112E-01 3.785E+OO 3.795E+OO NOT IDENT. NP-237 -2.076E-02 5.397E-02 5.478E-02 NOT IDENT. NP-238 -l.OOOE+41 2.160E+41 O.OOOE+OO SHORT HLIF NP-239 3.730E-02 2.439E-01 2.444E-01 NOT IDENT. PU-239 1. 282E+02 3 .113E+02 3.166E+02 NOT IDENT. AM-241 -8.076E-02 2.237E-01 2.267E-01 NOT IDENT. CM-243 -6.819E-02 9.754E-02 1.023E-01 NOT IDENT. BK-247 1.640E-02 6 .'965E-02 7.004E-02 NOT IDENT. CM-247 1.891E-02 3.612E-02 3.712E-02 NOT IDENT. CF-249 4.479E-02 3.730E-02 4.241E-02 NOT IDENT. *CF-251 7.996E-02 1.145E-01 l.200E-01 NOT IDENT. Page 3241of5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 43.8354 87.09 136.4134 136.47 78.0933 45.60 91.2ill 87.57 136.4821 140.51 0.0000 46.54 92.9732 88.03 136.5484 143.76 74.0322 49. 72 0.0000 88.34 82.4707 144.24 82.1883 51. 35 92.4033 88.47 82.4819 145.44 95.8253 51. 87 88.7731 89. 96 82.6099 152.43 64.0735 52.39 91.3065 1093.63 83.9597 153.25 0.0000 52.97 95.0859 91.11 0.0000 323.87 87.365'.2 53.44 90.2060 92.59 84.1273 156.02 0.0000 54.07 76.6810 93.35 84.1922 158.56 0.0000 57.36 0.0000 94.56 84.2949 159.00 84.9359 57.53 83.2581 94.65 84.3028 162.33 71. 4095 57.98 88.2817 94. 67 84.3043 162.66 0.0000 59.27 85.9423 94.87 84.:3212 163.33 84.2875 59.32 85.9478 97.43 72. 8314 165.86 71. 5912 59.54 85.9728 98.43 68.9972 176.31 69.3436 60. 96 74.8979 98. 4*4 68 .*9980 176.60 0.0000 61.17 83.2428 99.53 72.9813 177.52 68.4762 62.93 88.8544 100 .11 78.2382 181.07 0.0000 63.29 101.8330 102.03 67.9322 181.52 86.2916 63.58 101.8704 103.18 81.9574 184.41 65.5423 64.28 101.9606 103.37 81.9722 143.76 71.6478 66.73 100.5957 105.21 76.8738 193.51 73.8857 67.24 98.1427 105.31 76.8809 197.03 96. 5510 125.81 100.7135 106.12 69.9451 198.01 76.9142 67.75 100.7220 106.47 71. 7171 201.83 84.6231 69.67 94.6472 109.28 80.6731 203.43 63.0613 70.83 102.3605 111. 00 82.5569 205.31 72.0876 72.81 107.2447 111.76 0.0000 210.85 73.7542 72. 87 107.2525 114.06 79.2632 215.65 76.8159 74.66 107.4760 116. 30 0.0000 222 .11 65.6898 74.82 107.4954 116.74 78.5703 227.09 64.9287 74.97 107.5141 119.76 83.2048 227.38 65.8948 77 .11 107.7770 121.12 84.1890 228.16 78.74 109.6757 121.22 83.3100 228.18 64.0148 79.69 112.3452 121. 78 84.2373 116.74 64. 0148 80.12 109.8443 122.06 85.1445 235.69 82.0462 80.19 0.0000 122.92 85.2075 235. 96 71. 9818 80.57 108.6209 123.07 88.7690 238.63 59.5958 81. 00 108.6728 265.00 73.7167 238.98 0.0000 81. 07 121.4672 125.81 92.5356 240.99 59.6753 81.75 125.3965 127.23 95.3186 242.00 83.79 107. 7211 127.91 90*. 9166 244.70 44.8501 84.00 107.7455 129.30 82.0982 252.40 0.0000 85.43 107.9108 131. 20 98.3156 252.80 56.1934 86.55 124.7601 133.02 69.8195 254.15 0.0000 86.79 136.3697 133.52 75.2209 256.23 39.3118 86. 94 136.3915 136.00 85.2424 260.90 0.0000 Page 3242 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.7539 355.39 0.0000 584.27 17.7370 264.80 47.7828 356.01 29.0410 595.83 0.0000 265.00 43.3016 364.49 0.0000 427.87 22.2843 268.22 42.4964 366.42 0.0000 602.52 0.0000 269.46 49.8555 372.51 25.6571 604.72 31. 7 958 270.03 49.8701 375.05 33.9037 607.14 26.7949 271. 23 . 49.9022 377.52 28.7970 609.32 20.1094 273.65 0.0000 356.01 36.0923 610.33 20 .1160 276.40 54.4510 388.16 25.8265 614 .. 28 30.2102 277.37 49.4720 388.63 0.0000 618.01 19.0427 277.60 49.4782 391. 69 38.2789 620. 36 20.1775 278.00 51.0595 264.66 46.7267 621. 93 22.4300 279.20 62.8815 401.81 45.1904 630.19 0.0000 279.54 69.7707 402.40 26.4971 631.29 22.4927 279.70 69.7765 404.85 29.1239 633.25 . 20.2559 280.46 62.9219 410.95 34.4086 634.78 0.0000 283.69 46.2848 413. 71 31.3153 635.95 28.1555 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 54.2100 423.72 0.0000 645.85 15.8132 285.90 0.0000 427.09 39.8748 657.76 22.1025 287.50 50.3214 427.87 28.3409 657.90 0.0000 290.67 50.4013 433.94 37.8765 661. 66 36.3112 293.27 0.0000 439.40 30.3650 664.57 0.0000 351. 93 53:4869 453.88 24.1707 666.33 0.0000 295. 96 53.5067 463.37 31.9159 666.50 0.0000 879.38 35.7173 468.07 33.5694 667. 71 0.0000 299.98 29.7852 473.00 0.0000 677.62 21.6587 300.09 29.7864 475.06 25.6421 685.70 0.0000 300.13 29.7870 476.78 34.2109 695.00 0.0000 301.36 50.6690 477.60* 29.9431 696. 49 16.0445 302.85 54.6822 482.18 33.2062 696. 51 18.3366 256.23 30.8461 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.1942 306.78 42.8338 497.08 25.8447 697.49 17.1954 308.46. 35.8901 505.52 19.4407 702.65 20.6638 311. 90 40.9424 507.63 0.0000 706.68 26.4328 316.51 41. 0325 511. 00 19.4777 711. 68 18.4134 319.41 0.0000 514.00 14.6234 720.70 0.0000 320.08 0.0000 514.00 14.6234 721.93 0.0000 321.04 44.1289 520.40 28.2249 722.78 24. 2411 323.87 36.1531 520.69 0.0000 722.91 24.2419 325.23 43.2108 522.65 0.0000 723. 31 22.5135 328.76 0.0000 527. 90' 0.0000 724.19 22.5183 333.37 36.3127 528.26 21.7700 727.33 17.3370 333.97 28.7551 529.59 26.1357 733.00 17.3633 334.37 40.8708 529.87 0.0000 735.93 18.5352 338.28 50.5473 531.02 0.0000 333.97 18.5430 338.32 50.5483 537.26 0.0000 739.50 0.0000 311. 90 51.6101 546.56 0.0000 747.24 16.2678 340.48 51.6101 552.55 15.3621 748.06 18.5957 340.55 0.0000 563.25 26.4268 752.31 10.4718 344.28 46.6298 569.33 27.5818 753.82 0.0000 345.93 45.6500 946.00 27.5838 756.73 13.9785 351.06 44.7376 569.70 27.5859 756.80 13.9790 351. 93' 44 .. 7546 583.19 17.7305 884.68 12.2547 Page 3243 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.5214 1274.44 7.4001 1620.50 3.1053 766.42 28.0283 1001.03 11. 6411 1621. 92 1.0353 766.84 27.1553 1002.74 12.0423 1678.03 0.0000 772. 60 0.0000 1004.73 13.9009 1690.97 7.3226 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2 .1146 778.90 19.3326 1028.54 0.0000 1063.66 5.6436 783.70 0.0000 1037.84 9.3329 1771.35 4.2332 785.37 14. 9637 1038.76 0.0000 1791.20 0.0000 792.07 11.2859 631.29 13.0900 1808 .. 65 5.3195 794.95 12.3530 1048.07 0.0000 1810.72 0.0000 795.86 8.4727 1049.04 8.4194 1836.06 3.2040 810.06 11. 5146 1050.41 11. 2288 810.29 11.5154 1063.66 17.8287 344.28 13.2875 1077.00 0.0000 810.76 13.2884 1077.34 12.2327 815.77 0.0000 1085.87 12.2542 1048.07 0.0000 1093.63 1. 8882 832.01 11. 5777 1099.45 4.5372 834.85 15.1505 1112. 07 15.1621 835.71 16.9364 1112. 84 15.1641 836.80 0.0000 1115. 54 15.1729 846.75 0.0000 1120.29 17.0848 846.77 14. 3013 1120. 55 17.0859 856.80 0.0000 1221.41 17.0892 860.56 17.9364 1129. 67 17.1167 871.09 15.4128 1131. 51 0.0000 873.19 12.5935 1147. 95 0.0000 875.33 0.0000 1173.23 7. 672 9 879.38 15.3144 1177.95 *16.8953 880.51 11. 7142 1189.05 7.6958 883.24 10.3048 1204.77 13.5087 884.68 15.8748 1221.41 13.5505 889.28 16.2532 1231.02 12.6057 894.76 23.1453 1235.36 0.0000 898.04 11.7626 1238.28 6.2141 900. 72 19.0127 1260.41 0.0000 903.28 17.2124 1271.87 15.6309 911. 20 8.1683 1274.44 7.8193 912.08 8.1700 1274.54 7.8193 923.98 0.0000 1291.59 8.8242 92 6. 50 10.9292 1298.22 0.0000 929 .11 12.7584 1312 .11 0.0000 937.49 21. 9133 1332.49 6.9133 944 .13 0.0000 1362.66 0.0000 946.00 7.3186 1365 .19 8.9390 949.00 10.9852 1368. 63 0.0000 667. 71 0.0000 1384.29 3.9861 962. 31 22.0356 1408.01 6.0029 964.08 16.1659 1457.56 0.0000 966 .17 23.5250 1460.82 2.0187 911. 20 22.9881 1489.16 4.0562 968. 97 22.9881 1505.03 11.1826 983.53 0.0000 1584.12 8.2349 984.45 0.0000 1596.21 0.0000 Page 3244 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:17:28.73 ********************************************************************************
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2040 Savage Road *
Charleston, SC 29407
Configuration Background'file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM16.CNF;440 Background date : Z-OCT-2016 11:00:50. Sample date 2-DEC-2015 10:02:00. Acquisition date : 3-0CT-2016 08:16:00. Sample ID G405235017 Sample quantity : l.48561E+02 GRAM Detector name : GAM16 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.55 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 3 1 1 1 0 0 0 0 0 0 6 6 0 0 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 Page 3245 of 5809 Energy 43.60 70.29 74.95 77.16 81. 32 87.09 90.10 92.57* 115. 21 144.07* 154.89 186.01* 209.13 228.05 238.69* 241. 61 270.50 295.27* 300.49 328.07 338.67 351. 96* 467.98 511.26* 546.79 551. 54 562. 64 583.38* 609.48* 616.03 646.12 661. 74 685.39 728.12* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 27 31 142 234 43 78 40 75 31 29 28 -91 44 26 468 154 32 173 54 47 88 277 99 14 22 17 30 139 238 24 28 1437 17 45 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 145 189 189 170 71 205 194 183 183 133 180 207 129 123 91 150 155 117 113 89 118 133 201 104 12 21 30 68 38 37 13 68 23 '.?5 0.86 1. 22 1. 32 1. 32 1. 34 1.12 1.12 1.13 1. 66 1. 56 1. 75 1.19 1.18 1. 48 1.11 2.23 1. 06 1.10 3.35 1. 60 1. 00 1. 25 9.84 1.12 1. 7i 1. 72 1. 29 1. 74 1. 32 3.46 1. 47 1. 64 4.96 1. 21 87.27 140.62 149.93 154.35 162.66 174.19 180.20 185.16 230.41 288.09 309. 72 371. 93 418.16 455.98 477.25 483.08 540.83 590.35 600.78 655.93 677 .11 703.68 935.63 1022.15 1093.19 1102. 69 1124.88 1166. 34 1218.54 1231.63 1291. 80 1323.02 1370.30 1455.74 84 137 137 137 137 170 170 170 225 285 305 367 415 453 472 472 536 585 596 652 671 698 921 1016 1090 1090 1119 1161 1213 1226 1286 1316 1363 1449 7 7.36E-03 78.4 28 8.56E-03 71.5 2.06E+OO 28 3.95E-02 19.5 28 6.49E-02 12.7 28 1.18E-02 33.8 22 2.18E-02 31.6 2.52E+OO 22 1.lOE-02 59.7 22 2.09E-02 34.8 9 8.50E-03 82.3 7 8.0lE-03 70.3 9 7.66E-03 90.1 10 2.51E-02 32.3 7 l.21E-02 46.1 8 7.16E-03 77.0 19 1.30E-01 5.9 1.15E+OO 19 4.27E-02 23.7 10 8.89E-03 74.9 12 4.81E-02 14.7 11 1.49E-02 40.8 9 l.32E-02 38.8 10 2.44E-02 25.6 13 7. 68E-02 10. 6 26 2.76E-02 40.4 13 3.87E-03167.9 16 6.23E-03 33.0 16 4.85E-03 46.5 12 8.33E-03 40.8 15 3.85E-02 15.6 13 6.60E-02 8.5 12 6.72E-03 53.8 11 7.79E-03 31.7 16 3.99E-01 2.9 15 4.80E-03 64.6 14 1.25E-02 28.0 Peak Search Report (continued) Page .. 2 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 1 742.92 18 22 1. 88 1485.34 1478 19 4.90E-03 60.0 4.56E+OO 36 1 745.25 23 24 1. 71 1490.00 1478 19 6.48E-03 42.3 37 0 768.89 15 32 1. 42 1537.26 1533 11 .4.28E-03 74.1 38 0 782.30 8 10 1. 50 1564.08 1560 7 2.28E-03 73.4 . 39 0 785.92 14 14 0.68 1571.31 1567 9 3.93E-03 54.0 40 0 911. 42* 75 33 1. 34 1822.26 1816 14 2.08E-02 20.7 41 0 969.24* 63 13 1. 42 1937.87 1932 12 l.75E-02 17.8 42 0 1002.46 13 20 0.66 2004.30 1996 17 3.49E-03 88.4 43 0 1008.37 17 6 2.90 2016.12 2012 9 4.62E-03 37.2 44 0 1072.24 12 8 2.30 2143.83 2139 8 3.39E-03 49.2 45 0 1110.46 10 17 1. 09 2220.28 2209 14 2.67E-03 97.7 46 0 1120.27 50 5 1. 62 2239.89 2235 10 1. 40E-02 16. 3 47 0 1221. 91 13 9 2.28 2443.16 2438 9 3.47E-03 51. 4 48 0 1411. 82 10 7 3.55 2822.96 2816 11 2.69E-03 65.1 49 0 1460.83* 424 7 2.42 2920.98 2914 14 1.18E-01 5.1 50 0 1588.32 9 2 1.11 3175.98 3172 8 2.56E-03 42.0 51 0 1593.67* 3 0 0.73 3186.67' 3183 8 7.84E-04 99.9 52 0 1764.55 26 9 1. 64 3528.46 3522 12 7.24E-03 30.2 Fl.ag: "*" = Peak area was modified by background subtraction Page 3246 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:17:31 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 2-DEC-2015 10:02:00 G405235017 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:16:00 148.56 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA16 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3247of5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.55 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 215E+OO 1.595E+Ol 1.595E+Ol 10.13 OK CD-109 88.03 3.70* 5.400E+OO l.377E+OO 2.181E+OO 116. 66 OK SN-126 64.28 9.60 3.017E+OO Line Not Found Absent 86.94 8.90 5.400E+OO 5.725E-01 5.725E-01 116. 66 OK 87.57 37.00* 5.400E+OO -1.377E-01 1.377E-01 116. 66 OK BA-137M 661.66 89.90* 2.305E+OO 3.661E+OO 3.733E+OO 5.89 OK CS-137 661.66 85.10* 2. 305E+OO -3.868E+OO 3.943E+OO 5.89 OK CE-141 145.44 48.29* 6.768E+OO 1. 517E-02 1.032E+Ol 517.35 OK TL-208 277.37 6.60 4.683E+OO Line Not Found Absent 583.19 85.00* 2.549E+OO 3.420E-01 3.420E-01 31.12 OK 860.56 12.50 1.874E+OO Line Not Found Absent BI-212 727.33 6.67* 2 .137E+OO 1.646E+OO l.646E+00 56.05 OK 785.37 1.10 2:013E+OO 3.316E+OO 3.316E+00 108.05 OK 1620.50 1. 47 1.107E+OO Line Not Found Absent PB-212 74.82 10.28 4.288E+OO l.388E+00 l.388E+OO 59.83 OK 77 .11 17.10 4.519E+00 1.931E+OO 1.931E+OO 25.39 OK 238.63 43.60* 5.251E+OO l.186E+OO l.186E+OO 11. 79 OK 300.09 3.30 4.392E+OO 2 .101E+OO 2.101E+00 81. 58 OK BI-214 609.32 45.49* 2.'461E+OO l.129E+00 1.130E+OO 17.06 OK 1120.29 14.92 l.519E+OO 1.112E+OO l.113E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7. 951E-Ol 60.44 OK PB-214 74.82 5.80 4.274E+OO Line Not Found <<INT Reject 77 .11 9.70 4.519E+OO 3.404E+OO 3.406E+00 25.39 OK 87.09 3.41 5.400E+OO Line Not Found <<INT Reject 242.00 7.25 5.198E+OO Line Not Found <<INT Reject 295.22 18.42 4.455E+OO 1.203E+OO l.203E+00 29.37 OK 351. 93 35.60* 3.858E+OO 1.129E+OO l.129E+00 21.10 OK RN-222 609.32 45.49* 2.461E+OO l.129E+00 1.130E+OO 17.06 OK 1120.29 14.92 l.519E+OO 1.112E+OO 1.113E+OO 32.64 OK 1764.49 15.30 1. 023E+OO 7.948E-01 7.951E-01 60.44 OK RA-224 240.99 4.10* 5.204E+OO 2.048E+OO 2.048E+OO 101.21 OK RA-226 609.32 45.49* 2.461E+OO 1.129E+00 1.130E+OO 17.06 OK 1120.29 14.92 1.519E+OO 1.112E+OO l .113E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 OK AC-228 105.21 1.10 6.393E+OO Line Not Found Absent 338.32 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 OK 794.95 4.25 1.995E+OO Line Not Found Absent 835.71 1. 61 *1. 918E+OO Line Not Found Absent 911.20 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41.38 OK 968. 97 15.80 1. 706E+OO 1.188E+OO l.188E+00 35.66 OK RA-228 105.21 1.10 6.393E+OO Line Not Found Absent 338.32 11. 27 3.983E+00 1.lOOE+OO 1.lOOE+OO 51. 24 OK 794.95 4.25 1.995E+OO Line Not Found Absent 835. 71 1. 61 1.918E+OO Line Not Found Absent 911.20 25.80* 1. 791E+OO 8.287E-01 .8 .287E-01 41. 38 OK 968.97 15.80 1.706E+OO 1.188E+OO l.188E+OO 35.66 OK TH-228 74.82 10.28 4.288E+OO 1.388E+OO 1.388E+OO 59. 83 OK 77 .11 17.10 4.519E+OO 1.931E+OO 1. 931E+OO 25.39 OK 238.63 43.60* 5. 251E+OO 1.186E+OO l.186E+OO 11. 79 OK Page 3248 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.392E+OO 2.101E+OO 2.101E+OO 81. 58 OK TH-230 609.32 45.49* 2.461E+OO 1.129E+OO 1.129E+OO 17.06 OK 1120.29 14.92 1.519E+OO l.112E+OO l .112E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7.948E-01 60.44 OK PA-231 283.69 1. 70 4.600E+OO Line Not Found Absent 301.36 5.35* 4.392E+OO 1. 296E+OO l.296E+OO 81.58 OK TH-232 105.21 1.10 6.393E+OO Line Not Found Absent 338.32 11. 27 3.983E+OO l.lOOE+OO 1.lOOE+OO 51. 24 OK 835. 71 1. 61 l.918E+OO Line Not Found Absent 911.20 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 OK 968. 97 15.80 1. 706E+OO 1.188E+OO 1.188E+OO 35.66 OK U-234 609.32 45.49* 2.461E+OO 1.129E+OO l.129E+OO 17.06 OK 1120.29. 14.92 1.519E+OO l .112E+OO 1.112E+OO 32.64 OK 1764.49 15.30 1. 023E+OO 7.948E-01 7.948E-01 60.44 OK U-235 89. 96 3.47 5.617E+OO 1. 28 6E+OO 1. 28 6E+00 119. 50 OK 93.35 5.60 5.779E+OO 1.461E+OO 1.461E+OO 69.70 OK 143.76 10. 96* 6.770E+OO Line Not Found <<INT Reject 163.33 5.08 6. 541E+OO Line Not Found Absent 185. 72 57.20 6.164E+OO 1.524E-01 1.524E-01 64.51 OK 205.31 5.01 5.819E+OO Line Not Found Absent AM-243 43.53 5.90 4. 061E-01 7.398E+OO 7.398E+OO 156.85 OK 74.66 67.20* 4.288E+OO 2.124E-01 2.124E-01 59.83 OK ANH-511 511. 00 100.00* 2.836E+OO 2.662E-02 2.662E-02 335.79 OK Flag: "*" = Keyline Page 3249 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:17:32.19 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l *
Acquisition date 3-0CT-2016 08:16:00 Sensitivity : 3.000 *
Detector ID GAM16 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit.: 75.000 *
Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
Sample date 2-DEC-2015 10:02:00 Analyst initials: MXRl *
Sample ID G405235017 Sample Quantity 1.4856E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM K-40 l.595E+Ol 1.583E+OO 7.018E-01 CD-109 2 .181E+OO 2.493E+OO 2.282E+OO SN-126 l.377E-01 l.575E-01 1:450E-01 BA-137M 3.733E+OO 2.155E-01 6.780E-02 CS-137 3.943E+OO 2.277E-01 7.163E-02 CE-141 1.032E+Ol 5.234E+Ol 5.673E+Ol TL-208 3.420E-01 l.043E-01 7. 041E-02 BI-212 l.646E+00 9.043E-01 8.373E-01 PB-212 1.18 6E+OO 1.370E-01 9.442E-02 BI-214 1.130E+OO l.889E-01 l.319E-01 PB-214 1.129E+OO 2.336E-01 1.450E-01 RN-222 1.130E+OO 1.889E-01 1.319E-01 RA-224 2.048E+OO 2.032E+OO l.012E+00 RA-226 1.130E+OO 1.889E-01 l.319E-01 AC-22*8 8.287E-01 3.361E-01 2.509E-01 RA-228 8.287E-01 3.361E-01 2.509E-01 TH-228 l.186E+00 1.370E-01 9.442E-02 TH-230 1.129E+OO 1.889E-01 1.318E-01 PA-231 1.296E+OO l.036E+00 9.476E-01 TH-232 8.287E-01 3.361E-01 2.509E-01 U-234 1.129E+OO 1. 888E-01 l.318E-01 U-235 2.358E-01 3.250E-01 3.932E-01 AM-243 2.124E-01 1.245E-01 9.680E-02 .ANH-511 2.662E-02 8.759E-02 6.092E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -1.574E+Ol 1.907E+Ol 3.305E+Ol NOT IDENT. NA-22 l.795E-02 4.081E-02 8.794E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF AL-26 -1.312E-02 2.477E-02 4.715E-02 NOT IDENT. SC-46 -l.637E-01 3.600E-01 6.771E-01 FAIL ABUN V-48 O.OOOE+OO l.669E+04 O.OOOE+OO SHORT HLIF Page 3250 of 5809 CR-51 O.OOOE+OO 5.920E+02 O.OOOE+OO SHORT HLIF MN-54 8.642E-03 5.258E-02 1. 096E-01 NOT IDENT. C0-56 -l.079E-01 4.273E-01 8.351E-01 NOT IDENT. MN-56 O.OOOE+OO 1.747E+41 O.OOOE+OO SHORT HLIF C0-57 -3.425E-02 5.374E-02 9. 531E-02 . NOT IDENT. C0-58 6.255E-02 5.612E-01 1.152E+OO NOT IDENT. FE-59 2.294E-01 5.868E+OO 1.202E+Ol NOT IDENT. C0-60 -1.098E-02 4.174E-02 7.797E-02 NOT IDENT. ZN-65 3.965E-02 2.081E-01 3.690E-01 NOT IDENT. GE-68 -3.464E-01 2.284E+OO 4.278E+OO NOT IDENT. AS-73 -5.475E+OO l.185E+Ol 2.252E+Ol NOT IDENT. AS-74 O.OOOE+OO 8.525E+03 O.OOOE+OO SHORT HLIF SE-75 5.271E-02 2.377E-01 4.707E-01 NOT IDENT. BR-77 O.OOOE+OO l.459E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.459E+02 O.OOOE+OO SHORT HLIF RB-83 8.200E-02 7.940E-01 1.515E+OO FAIL ABUN KR-85 3.266E+OO 9.035E+OO 1.583E+Ol NOT IDENT. SR-85 3.647E-01 1.018E+OO 1. 782E+OO NOT IDENT. RB-86 O.OOOE+OO 3.267E+04 O.OOOE+oo* SHORT HLIF Y-88 2.707E-01 2.425E-01 6.305E-01 NOT IDENT. Y-91 1.368E+02 6.350E+02 1.253E+03 NOT IDENT. NB-94 l.327E-04 3.108E-02 5.836E-02 NOT IDENT. NB-95 -7. 649E-Cll l.133E+00 1.614E+OO NOT IDENT. NB-95M -1. 446E+OO 3:106E+00 4.802E+OO NOT IDENT. ZR-95 2.686E-01 1.355E+OO 2.674E+OO NOT IDENT. NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8.862E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 --l.537E-02 3.813E-02 6.854E-02 NOT IDENT. RH-102 3.642E-02 6.305E-02 1.274E-01 NOT IDENT. RU-103 -1. 921E+OO 7.841E+OO l.440E+Ol FAIL ABUN RH-106 2.697E-01 5.389E-01 1.043E+OO NOT IDENT. RU-106 2.697E-01 5.389E-01 l.043E+OO NOT IDENT. AG-108M -2.261E-02 3.506E-02 6.250E-02 NOT IDENT. AG-llOM -2.589E-03 9.860E-02 1.967E-01 NOT IDENT. SN-113 3.590E-02 3.082E-01 5.891E-01 NOT IDENT. CD-115 O.OOOE+OO 2.519E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.593E+05 O.OOOE+OO SHORT HLIF TE-123M 1.244E-01 1.465E-01 2.843E-01 NOT IDENT. SB-124 -4.188E-01 1.241E+OO 2.495E+OO FAIL ABUN SB-125 1.90JE-02 1.310E-01 2.506E-01 NOT IDENT. TE-125M 1.116E+02 3.124E+02 6.008E+02 NOT IDENT. I-126 O.OOOE+OO l.154E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.556E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.164E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1. 013E+l0 O.OOOE+OO SHORT HLIF' I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.866E+27 O.OOOE+OO SHORT HLIF BA-133 l.839E-02 4.905E-02 8.840E-02 FAIL ABUN I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 3.845E-02 5.577E-02 1.123E-01 FA'IL l;\BUN CS-135 -3.516E-02 1. 742E-01 *2.998E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 *O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.870E+05 0.000E+OO SHORT HLIF CE-139 -8.036E-02 1. 274E-01 2.203E-01 NOT IDENT. BA-140 O.OOOE+OO l.994E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.766E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 9.806E+40 0.000E+OO SHORT HLIF CE-144 2.124E-02 4.147E-01 7.664E-01 FAIL ABUN PM-144 5.082E-02 6.697E-02 l.341E-01 NOT IDENT. PR-144 4.357E+OO 5.828E+OO 1.166E+Ol NOT IDENT. PM-146 -l.414E-02 6.025E-02 l.107E-01 NOT IDENT. ND-147 O.OOOE+OO 5.686E+07 O.OOOE+OO SHORT HLIF PM-147 -5.660E+Ol 9.040E+02 1.675E+03 NOT IDENT. PM-149 O.OOOE+OO l.'497E+41 O.OOOE+OO SHORT HLIF EU-150 -5.178E-03 3.255E-02 5.530E-02 FAIL ABUN EU-152 4.729E-02 l.016E-01 2.032E-01 NOT IDENT. GD-153 4.509E-03 2.296E-01 3.994E-01 FAIL ABUN EU-154 4.386E-02 9.974E-02 2.149E-01 NOT IDENT. EU-155 8.891E-02 l.167E-01 2.305E-01 FAIL ABUN TB-160 -3.736E-01 1.738E+OO 3.409E+OO FAIL ABUN H0-166M -5.948E-02 5.689E-02 8.902E-02 FAIL ABUN TM-171 l.293E+Ol 2.676E+Ol 5.419E+Ol NOT IDENT. HF-172 -5.917E-02 2.532E-01 4.616E-01 FAIL ABUN LU-172 3.339E-02 7.741E-02 1.616E-01 FAIL ABUN LU-176 1.956E-03 2.670E-02 5.202E-02 FAIL ABUN HF-181 7.667E+00 6.760E+OO 1. 374E+Ol NOT IDENT. Page 3251 of 5809 TA-182 1. 036E+OO 1.043E+OO 2. 021E+OO FAIL ABUN RE-183 -1.266E+OO 3.408E+OO 6.517E+OO NOT IDENT. RE-184 2.583E+Ol 3.559E+Ol 7.658E+Ol NOT IDENT. W-188 2.142E+Ol 1.307E+02 2.337E+02 FAIL ABUN IR-192 -2.060E-02 5.417E-01 1.045E+OO FAIL ABUN HG-203 -l.178E-02 2.862E+OO 5.563E+OO FAIL ABUN BI-207 -4.538E-02 4.581E-02 7.574E-02 FAIL ABUN PB-210 -3.189E+OO 4.672E+OO 8.184E+OO NOT IDENT. BI-211 O.OOOE+OO 6.434E-01 8.492E-01 FAIL ABUN PB-211 1. 331E-01 8.190E-01 1.573E+OO NOT IDENT. RN-219 2.806E-01 4.653E-01 9.251E-01 FAIL ABUN RA-223 -1. 701E-01 7.430E-01 1.258E+00 FAIL ABUN AC-227 l.004E-01 2.473E-01 4. 962E-01 FAIL ABUN TH-227 l.004E-01 2.473E-01 4. 962E-01 *FAIL ABUN TH-229 -3.999E-01 5.417E-01 9.153E-01 FAIL ABUN TH-231 -l.701E-01 7.430E-01 1.258E+OO FAIL ABUN PA-233 -3.135E-02 6.316E-02 1.178E-01 FAIL ABUN PA-234 -5.330E-02 2.582E-01 5.009E-01 NOT IDENT. PA-234M 4.560E+OO 7.901E+OO 8.386E+OO FAIL ABUN TH-234 -2.226E-01 l.357E+OO 2°.661E+OO FAIL ABUN NP-237 -3 .135E-02 6.316E-02 1.178E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF U-238 -2. 22 6E-Ol* 1.357E+OO 2.661E+OO FAIL ABUN NP-239 -l.084E-02 2.685E-01 4.624E-01 FAIL ABUN PU-239 l.448E+02 3.547E+02 6.714E+02 NOT IDENT. AM-241 -9.017E-02 1. 58 6E-01 2.978E-01 NOT IDENT. CM-243 -9. 716E-02 1.023E-01 1. 792E-01 FAIL ABUN BK-247 2.00lE-02 7. 981E-0'2 1.583E-01 NOT IDENT. CM-247 2.693E-04 4.349E-02 8.246E-02 NOT .I DENT. CF-249 -9.102E-03 4.912E-02 9.167E-02 NOT IDENT. CF-251 4.402E-02 1.299E-01 2.407E-01 FAIL ABUN Page 3252 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:17:29.71. Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 409 10.66* 1.215E+OO 1.595E+Ol 1.595E+Ol 10.13 CD-109 88.03 98 3.70* 5.400E+OO 2.486E+OO 3.936E+OO 63.30 SN-126 64.28 ------9.60 3.017E+OO ------Line Not Found ------86.94 98 8.90 5.400E+OO 1.033E+OO 1.033E+OO 63.30 87.57 98 37.00* 5.400E+OO 2.486E-01 2.486E-01 63.30 BA-137M 661.66 1501 89.90* *2.305E+OO 3.661E+OO 3.733E+OO 5.89 CS-137 661.66 1501 85.10* 2.305E+OO 3.868E+OO 3.943E+OO 5.89 CE-141 145.44 35 48.29* 6.768E+OO 5.351E-02 3.643E+Ol 140.66 TL-208 277.37 ------6.60 A. 683E+OO ------Line Not Found ------583.19 147 85.00* 2.549E+OO 3.420E-01 3.420E-01 31.12 860.56 ------12.50 1. 874E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 4.060E+OO ------Line Not Found ------351.06 307 12.92* 3.858E+OO* 3. lllE+OO 3. lllE+OO 21.10 BI-212 727. 33 46 6.67* 2.137E+OO l.646E+00 1. 646E+00 56.05 785.37 15 1.10 2.013E+00 3.316E+OO 3.316E+OO 108.05 1620.50 ------1. 47 1.107E+OO ------Line Not Found ------PB-212 74.82 180 10.28 4.288E+OO 2.067E+OO 2.067E+OO 39.02 77 .11 295 17.10 4.519E+OO 1. 931E+OO 1. 931E+OO 25.39 238.63 537 43.60* 5. 251E+OO 1.186E+OO 1.186E+OO 11. 79 300.09 60 3.30 4.392E+00 2.101E+OO 2.lOlE+OO 81. 58 BI-214 609.32 250 45.49* 2.461E+OO 1.129E+OO 1.130E+00 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.113E+OO 32.64 1764.49 25 15.30 l.023E+OO 7.948E-01 7. 951E-01 60.44 PB-214 . 74.82 180 5.80 4.288E+OO 3.663E+OO 3.665E+OO 39.02 77 .11 295 9. 70 4.519E+OO 3.404E+OO 3.406E+OO 25.39 87.09 98 3.41 5.400E+OO 2.697E+OO 2.698E+OO 63.30 242.00 176 7.25 5.204E+OO 2.361E+OO 2.362E+00 47.35 295.22 195 18.42 4.455E+OO 1.203E+OO 1.203E+OO 29.37 351.93 307 35.60* 3.858E+OO 1.129E+OO 1.129E+OO 21.10 RN-222 609.32 250 45.49* 2 . .461E+OO 1.129E+OO 1.130E+OO 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.113E+OO 32.64 1764.49 25 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 RA-224 240.99 176 4.10* 5.204E+OO 4.175E+00 .4.175E+OO 47.35 RA-226 609.32 250 45.49* 2.461E+OO 1.129E+OO 1.130E+OO 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.113E+OO 32.64 1764.49 25 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 AC-228 105.21 ------1.10 6.393E+OO ------Line Not Found ------338.32 98 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 794.95 ------4.25 1.995E+OO ------Line Not Found ------835. 71 ------1. 61 1.918E+OO ------Line Not Found ------911.20 76 25.80* l.791E+00 8.287E-01 8.287E-01 41. 38 968. 97 63 15.80 1.706E+OO 1.188E+OO 1.188E+OO 35.66 RA-228 105.21 ------1.10 6.393E+00 ------Line Not Found ------338.32 98 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 794.95 ------4.25 1.995E+OO ------Line Not Found ------835.71 ------1. 61 1.918E+OO ------Line Not Found ------. 911.20 76 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 Page 3253 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 968.97 63 15.80 1. 706E+OO 1.188E+OO 1.188E+OO 35.66 TH-228 74.82 180 10.28 4.288E+OO 2.067E+OO 2.067E+OO 39.02 77 .11 295 17.10 4.519E+OO 1.931E+OO 1.931E+OO 25.39 238.63 537 43.60* 5.251E+OO 1.186E+OO 1.186E+OO 11.79 300.09 60 3.30 4.392E+OO 2.101E+OO 2.101E+OO* 81. 58 TH-230 609.32 250 45.49* 2.461E+OO l.129E+OO 1.129E+OO 17.06 1120.29 50 14.92 1.519E+OO 1. 112E+OO 1.112E+OO 32.64 1764.4*9 25 15.30 1.023E+OO 7.948E-01 7.948E-01 60.44 PA-231 283.69 ------1. 70 4.600E+OO ------Line Not Found ------301.36 60 5.35* 4.392E+OO 1.296E+OO 1. 296E+OO 81. 58 TH-232 105.21 ------1.10 6.393E+OO ------Line Not Found ------338.32 98 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 835. 71 ------1. 61 1.918E+OO ------. Line Not Found ------911. 20 76 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 968. 97 63 15.80 1. 706E+OO 1.188E+OO 1.188E+OO 35.66 U-234 609.32. 250 45.49* 2.461E+OO 1.129E+OO l.129E+00 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.112E+OO 32.64 1764.49 25 15.30 1. 023E+OO 7.948E-01 7.948E-01 60.44 U-235 89.96 50 3.47 5.617E+OO
1. 28 6E+OO 1.286E+OO 119. 50 93.35 94 5.60 5.779E+OO 1.461E+OO 1.461E+OO 69.70 143.76 35 10. 96* 6.768E+OO 2.358E-01 2.358E-01 140.66 163.33 ------5.08 6.541E+OO ------Line Not Found ------185. 72 106 57.20 6.164E+00 l.524E-01 l.524E-01 64.51 205.31 ------5.01 5.819E+OO ------Line Not Found ------AM-243 43.53 35 5.90 4.061E-01 7.398E+OO 7.398E+OO 156.85 74.66 180 67.20* 4.288E+OO 3.162E-01 3.162E-01 39.02 ANH-511 511. 00 15 100.00* 2.836E+OO 2.662E-02 2.662E-02 335.79 Flag: "*" Key line Page 3254 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235017 Acquisition date 3-0CT-2016 Total number of lines in spectrum 52 Number of unidentified lines 11 Number of lines tentatively identified by NID 41 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 32. 510 l.41E+10Y 7.04E+08Y l.41E+l0Y l.41E+l0Y 1600. DOY 1600. ODY 1600.00Y 1.41E+10Y 1600.00Y l.41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 58 1. 00 1. 02 1. 02 681. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1 .. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.595E+Ol 2.486E+OO 2.486E-01 3.661E+OO 3.868E+OO 5. 351E-02 3.420E-01 3. lllE+OO 1.646E+OO 1.186E+OO 1.129E+OO 1.129E+OO 1.129E+OO 4.175E+OO 1.129E+OO 8.287E-01 8.287E-01 1.186E+OO 1.129E+OO 1.296E+OO 8.287E-01 l.129E+OO 2.358E-01 3.162E-01 2.662E-02 4.905E+Ol 4.905E+Ol Decay Corr pCi/GRAM l.595E+Ol 3.936E+OO 2.486E-01 3.733E+OO 3.943E+OO 3.643E+Ol 3.420E-01 3. lllE+OO 1.646E+OO l.186E+OO 1.130E+OO 1.129E+OO 1.130E+OO 4.175E+OO 1.130E+OO 8.287E-01 8.287E-01 1.186E+OO 1.129E+00 1.296E+OO 8.287E-01 l.129E+OO 2.358E-01 3.162E-01 2.662E-02 8.702E+Ol 8.702E+Ol 78.85% Decay Corr 2-Sigma Error 0.162E+Ol 2.491E+OO l.573E-01 0.220E+OO 0.232E+OO 5.124E+Ol 1.064E-01 0.657E+OO 0.923E+OO 0.140E+00 0.193E+OO 0.238E+OO 0.193E+OO 1.977E+OO 0.193E+OO 3.430E-01 3.430E:_Ol 0.140E+OO 0.193E+00 1.057E+OO 3.430E-01 0.193E+OO 3.317E-01 1.234E-01 ,8. 938E-02 "M" Manually accepted 2-Sigma %Error 10.13 63.30 63.30 5.89 5.89 140.66 31.12 21.10 56.05 11. 79 17.06 21.10 17.06 47.35 17.06 41. 38 41. 38 11. 79 17.06 81. 58 41. 38 17.06 140.66 39.02 335.79 Flags:. "K" "E" Keyline not found Manually edited "A" = Nuclide specific abn. limit Page 3255 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235017 Acquisition date : 3-0CT-2016 08:16:00 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 3 70.29 39 241 1. 22 140.62 137 28 8.56E-03 **** 3.76E+OO T 3 81. 32 54 90 1. 34 162.66 137 28 l.18E-02 67.7 4.92E+OO T 0 115. 21 37 224 1. 66 230.41 225 9 8.50E-03 **** 6.66E+OO T 0 154.89 33 215 1. 75 309.72 305 9 7.66E-03 **** 6.66E+OO T 0 209 .13 51 150 1.18 418.16 415 7 1.21E-02 92.3 5.75E+OO 0 228.05 30 142 1. 48 455.98 453 8 7.16E-03 **** 5.43E+OO T 0 270.50 36 176 1. 06 540.83 536 10 8.89E-03 **** 4.78E+OO T 0 328.07 53 99 1. 60 655.93 652 9 1.32E-02 77.6 4.09E+OO T 0 467.98 107 217 9.84 935.63 921 26 2.76E-02 80.8 3.05E+OO T 1 546.79 24 13 1. 71 1093.19 1090 16 6.23E-03 66.0 2.69E+OO T 1 551.54 19 22 1. 72 1102. 69 1090 16 4.85E-03 92.9 2.67E+OO T 0 562.64 32 32 1. 29 1124.88 1119 i2 8.33E-03 81. 6 2.62E+OO T 0 616.03 25 39 3.46 1231. 63 1226 12 6.72E-03 **** 2.44E+OO 0 646.12 29 14 1. 47 1291. 80 1286 11 7.79E-03 63.3 2.35E+OO T 0 685.39 18 24 4.96 1370.30 1363 15 4.80E-03 **** 2.24E+OO T 1 742.92 18 23 1. 88 1485.34 1478 19 4.90E-03 **** 2.lOE+OO 1 745.25 24 25 1. 71 1490.00 1478 19 6.48E-03 84.5 2.lOE+OO 0 768.89 16 33 1. 42 1537.26 1533 11 4.28E-03 **** 2.05E+00 0 782.30 8 10 1. 50 1564.08 1560 7 2.28E-03 **** 2.02E+OO T 0 1002.46 13 20 0.66 2004.30 1996 17 3.49E-03 **** 1.66E+OO T 0 1008.37 17 6 2.90 2016.12 2012 9 4.62E-03 74.3 1. 65E+OO 0 1072.24 *12 8 2.30 2143.83 2139 8 3.39E-03 98.4 1.57E+OO 0 1110.46 10 17 1. 09 2220.28 2209 14 2.67E-03 **** 1.53E+OO 0 1221.91 12 8 2.28 2443.16 2438 9 3.47E-03 **** 1. 41E+OO T 0 1411. 82 9 7 3.55 2822.96 2816 11 2.69E-03 **** -1.25E+OO 0 1588.32 9 2 1.11 3175.98 3172 8 2.56E-03 83.9 1.13E+00 0 1593.67 3 0 0.73 3186.67 3183 8 7.84E-04 **** 1.12E+OO Flags: "T" = Tentatively associated Page 3256 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:17:46.16 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l *
Acquisition date 3-0CT-2016 08:16:00 Sensitivity : 3.000 *
Detector ID GAM16 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
Sample date 2-DEC-2015 10:02:00 Nuclide Library : SOLID *
Sample ID G405235017 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : l.4856E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 23-SEP...:.2016 08: 25: 42 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.979E-01 1.084E+OO 6.885E-02 3.046E-02 3.218E-02 2.686E+Ol 3.197E-02 3.697E-01 4.409E-02 5. 967E-02 6.734E-02 5. 967E-02 4.727E-01 5. 967E-02 1.105E-01 l.105E-01 4.409E-02 5. 965E-02 4.435E-01 1.105E-01 5. 965E-02 l.869E-01 4.585E-02 2.798E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3257 of 5809 Le (pCi/GRAM l.532E+Ol 3.766E-02 O.OOOE+OO l.671E-02 2.907E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT*. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-11.7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3258 of 5809 4.766E-02 3.604E-01 0.000E+OO 4.492E-02 5.051E-01 5.077E+OO 3.314E-02 1. 631E-01 1.839E+OO 1.062E+Ol O.OOOE+OO 2.207E-01 O.OOOE+OO O.OOOE+OO 6.922E-01 7. 311E+OO 8.230E-01 O.OOOE+OO 2.641E-01 5.571E+02 2.600E-02 7.138E-01 2.252E+00 1.167E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.241E-02 5.758E-02 6.607E+Ob 4.699E-01 4.699E-01 2.885E-02 8.616E-02 2. 7 51E-01 O.OOOE+OO O.OOOE+OO 1. 345E-01 7.885E-01 l.164E-01 2.838E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 0. OOOE+.00 O.OOOE+OO 4.104E-02 O.OOOE+OO 5.074E-02 l.406E-01 O.OOOE+OO O.OOOE+OO 1.037E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO 3. 631E-01 6.137E-02 5.334E+OO 5.150E-02 O.OOOE+OO 7.905E+02 O.OOOE+OO 2.579E-02 9.452E-02 l.897E-01 9.204E-02 1.092E-01 l.469E+OO 3.857E-02 2.560E+Ol 2.180E-01 7 .114E-02 2.425E-02 6.433E+OO 8.954E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF . SHORT HLIF .FAIL ABUN NOT IDENT. NOT IDENT. NOT I DENT.* SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234
PA-234M TH-234 NP-237 *NP-238 U-238 NP-239 PU-239 AM-241 CM-243
BK-247 CM-247 CF-249 CF-251 Page 3259 of 5809
3.054E+00 3.426E+Ol 1.087E+02 4.865E-01 2.604E+OO 3.191E-02 3.836E+OO 4.106E-01 7.323E-01 4.316E-01 5.858E-01 2.330E-01 2.330E-01 4.307E-01 5.858E-01 5.455E-02 2. l 72E-01 3.697E+OO 1.262E+OO 5.455E-02 O.OOOE+OO 1.262E+OO 2.176E-01 3.189E+02 1.403E-01 8.400E-02 7.423E-02 . 3. 839E-02 4.283E-02 l.138E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL.ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:17:51.78 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l *
Acquisition date 3-0CT-2016 08:16:00 Sensitivity : 3.000 *
Detector ID GAM16 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
Sample date 2-DEC-2015 10:02:00 Nuclide Library : SOLID *
Sample ID G405235017 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4856E+02 GRAM *
Quantity Err(%) : l.3462E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-4*0 1.595E+Ol 1. 789E+OO 1. 789E+00 CD-109 2 .181E+OO 2.509E+OO 2.509E+OO SN-126 l.377E-01 1.583E-01 1.583E-01 BA-137M 3.733E+OO 2.689E-01 2.689E-01 CS-137 3.943E+OO 2.838E-01 2.838E-01 CE-141 1.033E+Ol 5.238E+Ol 5.238E+Ol TL-208 3.420E-01 1.053E-01 1.053E-01 BI-212 1.646E+OO 9. 081E-01 9.081E-01 PB-212 l.186E+OO 1.509E-01 1.509E-01 BI-214 1.130E+OO l.951E-01 1.951E-01 PB-214 1.129E+00 2.383E-01 2.383E-01 RN-222 1.130E+OO 1. 951E-01 l.951E-01 RA-224 2.048E+OO 2.040E+OO 2.040E+OO RA-226 1:130E+OO 1. 951E-01 1. 951E-01 AC-228 8.287E-01 3.388E-01 3.388E-:-01 RA-228 8.287E-01 3.388E-01 3.388E-01 TH-228 l.186E+OO 1.509E-01 1.509E-01 TH-230 l.129E+OO l.950E-01 l.950E-01 PA-231 l.296E+OO 1.073E+OO 1.073E+OO TH-232 8.287E-01 3.388E-01 3.388E-01 U-234 1.129E+OO l.950E-01 l.950E-01 U-235 2.358E-01 3.252E-01 3.252E-01 AM-243 2.124E-01 l.259E-01 1.259E-01 ANH-511 2.662E-02 8.760E-02 8.760E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.574E+Ol 1.908E+Ol 2.036E+Ol NOT IDENT. NA-22 1. 795E-02 4.082E-02 4.161E-02 NOT IDENT. NA-24 l.OOOE+41 3.054E+41 O.OOOE+OO SHORT HLIF AL-26 -1.312E-02 .2.478E-02 2.548E-02 NOT IDENT. SC-46 -l.637E-01 3.601E-01 3.676E-01 FAIL ABUN V-48 -5.949E+03 1.669E+04 1. 691E+04 SHORT HLIF Page 3260 of 5809 CR-51. 4.574E+02 5.924E+02 6.272E+02 SHORT HLIF MN-54 8.642E-03 5.258E-02 5.273E-02 NOT IDENT. C0-56 -1. 079E-01 4.273E-01 4. 301E-01 NOT IDENT. MN-56 -1. OOOE+41 l.748E+41 0.000E+OO SHORT HLIF C0-57 -3.425E-02 5.377E-02 5.594E-02 NOT IDENT. C0-58 6.255E-02 5.612E-01 5.619E-01 NOT IDENT. FE-59 2.294E-01 5.868E+OO 5.869E+OO NOT IDENT. C0-60 -l.098E-02 4.174E-02 4.203E-02 NOT IDENT. ZN-65 3. 965E-02 2. 081E-01 2.089E-01 NOT IDENT. GE-68 -3.464E-01 2.284E+OO 2.289E+OO NOT IDENT. AS-73 -5.475E+OO 1.190E+Ol l.215E+Ol NOT IDENT. AS-74 8.846E+02 8.526E+03 8.535E+03 SHORT HLIF SE-75 5.271E-02 2.378E-01 2.389E-01 NOT IDENT. BR-77 1.263E+39 l.116E+40 0.000E+OO SHORT HLIF SR-82 -1.850E+02 8.459E+02 8.500E+02 SHORT HLIF RB-83 8.200E-02 7.941E-01 7.950E-01 FAIL ABUN KR-85 3.266E+OO 9.036E+OO 9 .15.5E+OO NOT IDENT. SR-85 3.647E-01 1.018E+OO 1. 031E+OO NOT IDENT. RB-86 2.978E+03 3.267E+04 3.270E+04 SHORT HLIF Y-88 2.707E-01 2.432E-01 2.721E-01 NOT IDENT. Y-91 1. 368E+02 6.350E+02 6.380E+02 NOT IDENT. NB-94 l.327E-04 3.108E-02 3.108E-02 NOT IDENT. NB-95 -7.649E-01 1.133E+OO l.185E+OO NOT IDENT. NB-95M* -l.446E+OO 3.108E+OO 3.175E+OO NOT IDENT. ZR-95 2.686E-01 1.355E+OO l.360E+OO NOT IDENT: NB-97 -1.000E+41 6.378E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 4.159E+41 0.000E+OO SHORT HLIF M0-99 -4.977E+32 8.870E+32 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 2.536E+41 O.OOOE+OO SHORT HLIF RH-101 -l.537E-02 3.823E-02 3.886E-02 NOT IDENT. RH-102 3.642E-02 6.312E-02 6.522E-'-02 NOT IDENT. RU-103 -1.921E+OO 7.842E+OO 7.889E+OO FAIL ABUN RH-106 2.697E-01 5.391E-01 5.527E-01 NOT IDENT. RU-106 2.697E-01 5.391E-01 5.527E-01 NOT IDENT. AG-108M -2.261E-02 3.507E-02 3.652E-02 NOT IDENT. AG-llOM -2.589E-03 9.860E-02 9. 8 61E-02 NOT IDENT. SN-113 3.590E-02 3.082E-01 3.086E-01 NOT IDENT. CD-115 -2.042E+40 2.547E+40 O.OOOE+OO SHORT HLIF SN-117M 1.632E+04 l.593E+05 1.595E+05 SHORT HLIF TE-123M 1.244E-01 l.466E-01 1.570E-01 NOT IDENT. SB-124 -4.188E-01 l.241E+OO l.255E+OO FAIL ABUN SB-125 l.903E-02 1.310E-01 1.312E-01 NOT IDENT. TE-125M 1.116E+02 3.124E+02 3.165E+02 NOT IDENT. I-126 1.178E+06 1.166E+06 l.281E+06 SHORT HLIF SB-126 -4.101E+05 1.558E+06 1.569E+06 SHORT HLIF SB-127 9.203E+22 1. 739E+23 O.OOOE+OO SHORT HLIF I-131 -4.498E+09 1. 013E+l0 1.033E+10 SHORT HLIF I-132 -1.000E+41 l.940E+42 O.OOOE+OO SHORT HLIF TE-132 1.900E+27 2.972E+27 O.OOOE+OO SHORT HLIF BA-133 l.839E-02. 4.906E-02 4.975E-02 FAIL ABUN I-133 1.000E+41 6.660E+41 O.OOOE+OO SHORT HLIF CS-134 3.845E-02 5.579E-02 5.842E-02 FAIL ABUN CS-135 -3.516E-02 1. 742E'-01 1. 749E-01 NOT IDENT. I-135 1.000E+41 8.045E+41 0.000E+OO SHORT HLIF CS-136 1.181E+05 3.872E+05 3.908E+05 SHORT HLIF CE-139 -8.036E-02 l.284E-01 l.334E-01 NOT IDENT . BA-140 -9. 431E+05 . 1. 995E+06 2.040E+06 SHORT HLIF LA-140 2.523E+05 2.769E+05 2.993E+05 SHORT HLIF CE-143 1.000E+41 9.861E+40 O.OOOE+OO SHORT HLIF CE-144 2.124E-02 4.147E-01 4.148E-01 FAIL ABUN PM-144 5.082E-02 6.705E-02 7.085E-02 NOT IDENT. PR-144 4.357E+OO 5.831E+OO 6.152E+OO NOT IDENT. PM-146 -l.414E-02 6.026E-02 6.060E-02 NOT IDENT. ND-147 3.804E+07 5.690E+07 5.943E+07 SHORT HLIF PM-147 -5.660E+Ol 9.040E:t-02 9.044E+02 NOT IDENT. PM-149 1.000E+41 1.514E+41 O.OOOE+OO SHORT HLIF EU-150 -5.178E-03 3.255E-02 3.264E-02 FAIL ABUN EU-152 4.729E-02 1.017E-01 1.039E-01 NOT IDENT. GD-153 4.509E-03 2.296E-01 2.296E-01 FAIL ABUN EU-154 4.386E-02 9.976E-02 l.017E-01 NOT IDENT. EU-155 8.891E-02 1.168E-01 l.235E-01 FAIL ABUN TB-160 -3.736E-01 1. 738E+OO l.747E+OO FAIL ABUN H0-166M -5.948E-02 5.698E-02 6.297E-02 FAIL ABUN TM-171 1.293E+Ol 2.678E+Ol 2.741E+Ol NOT IDENT. HF-172 -5.917E-02 2.534E-01 2.548E-01 FAIL ABUN LU-172 3.339E-02 7.749E-02 7.894E-02 FAIL ABUN LU-176 l.956E-03 2.670E-02 2.672E-02 FAIL ABUN HF-181 7.667E+OO 6.769E+OO 7.6QOE+OO NOT IDENT. Page 3261of5809 TA-182 1. 036E+OO 1.044E+OO l.144E+00 FAIL ABUN RE-183 -1.266E+OO 3.414E+OO 3.461E+OO NOT IDENT. RE-184 2.583E+Ol 3.614E+Ol 3.797E+Ol NOT IDENT. W-188 2.142E+Ol 1.307E+02 l.310E+02 FAIL ABUN IR-192 -2.060E-02 5.417E-01 5.418E-01 FAIL ABUN HG-203 -1.178E-02 2.862E+OO 2.862E+OO FAIL ABUN BI-207 -4.538E-02 4.585E-02 5.020E-02 FAIL ABUN PB-210 -3.189E+OO 4.681E+OO 4.896E+OO NOT IDENT. BI-211 3. lllE+OO 6.584E-01 1.549E+OO FAIL ABUN PB-211 1. 331E-01 8.190E-01 8.212E-01 NOT IDENT. RN-219 2.806E-01 4.667E-01 4.835E-01 FAIL ABUN RA-223 -l.701E-Ql 7.431E-01 7.470E-01 FAIL ABUN AC-227 l.004E-Ol 2.477E-01 2.518E-01 FAIL ABUN TH-227 l.004E-01 2.477E-01 2.518E-01 FAIL ABUN TH-229 -3.999E-01 5.421E-01 5. 712E-01 FAIL ABUN* TH-231 -1.701E-01 7.431E-01 7.470E-01 FAIL ABUN PA-233 -3.135E-02 6.318E-02 6.474E-02 FAIL ABUN PA-234 -5.330E-02 2.653E-01 2.664E-01 NOT IDENT. PA-234M 4.560E+OO 7.904E+OO 8.167E+00 FAIL ABUN TH-234 -2.226E-01 1.358E+OO 1. 362E+OO FAIL ABUN NP-237 -3.135E-02 6.318E-02 6.474E-02 FAIL ABUN NP-238 -1.000E+41 4.680E+41 O.OOOE+OO SHORT HLIF U-238 -2.226E-01 1.358E+OO 1.362E+OO FAIL ABUN NP-239 -1.084E-02 2.685E-01 2.685E-01 FAIL ABUN PU-239 1.448E+02 3.548E+02 3.608E+02 NOT IDENT. AM-241 -9.017E-02 l.588E-01 1.639E-01 NOT IDENT. CM-243 -9. 716E-02 l.027E-01 l .116E-01 FAIL ABUN BK-247 2.00lE-02 7. 991E-02 8.042E-02 NOT IDENT. CM-247 2.693E-04 4 .349E-02 4.349E-02 NOT IDENT. CF-249 -9.102E-03 4.912E-02 4.929E-02 NOT IDENT. CF-251 4.402E-02 1.300E-01 l.315E-01 FAIL ABUN Page 3262 of 5809
GEL Laboratories LLC *
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.2320 87.09 119.8780 136.47 102.8881 45.60 66.0009 87.57 119. 9950 140.51 0.0000 46.54 83.3537 88.03 120.1066 143.76 95.0439 49.72 0.0000 88.34 120.1814 144.24 95 .1101 51. 35 76.4709 88.47 120.2129 145.44 106.1085 51. 87 79.3869 89. 96 120.5703 152.43 99.6056 52.39 80.4400 1093.63 120.7332 153.25 0.0000 52.97 83.3828 91.11 0.0000 323.87 77.1558 53.44 98.5032 92.59 121.1955 156.02 0.0000 54.07 86.4599 93.35 121.3742 158.56 0.0000 57.36 0.0000 94.56 121. 6578 159.00 78.7979 57*. 53 88.2287 94.65 121.6785 162.33 88.3239 57.98 83.5850 94.67 121. 6834 162.66 0.0000 59.27 99 .1194 94.87 105.9118 163.33 76.9535 59.32 103.8985 97.43 118.8676 165.86 103.7123 59.54 103.9584 98.43 94.5103 176.31 110. 9338 60.96 89.0256 98.44 94.5123 176.60 0.0000 61.17 89.0738 99.53 105 .1110 177.52 90.0499 62.93 109.6769 100 .11 95.8478 181.07 0.0000 63.29 99.1840 102.03 80.5030 181.52 89.3165 63.58 99.2559 103.18 78.5757 184.41 94.3469 64.28 104.2561 103.37 99.5633 143.76 116. 9371 66.73 121. 7188 105.21 86.2235 193.51 106.0936 67.24 106. 3112 105.31 86.2385 197.03 106.5254 '125.81 127.1895 106.12 76.8841 198.01 116. 2310 67.75 129.8065 106.47 84.3091 201.83 108. 3115 69.67 105.6253 109.28 87.9025 203.43 88.0097 70.83 105.9120 111. 00 101.9729 205.31 86.9865 72.81 10.6.3974 111.76 0.0000 210.85 105.3460 72.87 106.4122 114. 06 90.7600 215.65 86.7523 74.66 106.8456 116. 30 0.0000 222 .11 109.4927 74.82 106.8835 116.74 85.8051 227.09 82.4432 74.97 106.9198 119.76 93.7783 227.38 82.4677 77 .11 107.4298 121.12 87.5036 228.16 0.0000 78.74 107.8130 121. 22 96.1616 228.18 84.1865 79.69 108.0354 121.78 98.4114 116.74 84.1865 80.12 108.1351 122.06 108.1932 235.69 89.8220 80.19 0.0000 122.92 78.0068 235. 96 89.8462 80.57 108.2390 123.07 7.8.0255 238.63 66.7301 81. 00 108.3387 265.00 96.5418 238.98 0.0000 81. 07 108.3551 125.81 102.3105 240.99 66.8872 81. 75 101. 8134 127.23 112.3561 242.00 66.9535 83.79 100.9048 127.91 97.1876 244.70 61.6769 84.00 100.9491 129.30 107.2458 252.40 0.0000 85.43 129.5977 131.20 113. 0492 252.80 65.1207 86.55 119.7465 133.02 108.9595 254.15 0.0000 86.79 119.8050 133.52 106.8397 256.23 70.4243 86.94 119.8419 136.00 103.9212 260.90 , 0.0000 Page 3263 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 70.9803 355.39 0.0000 584.27 32.7950 264.80 70.9887 356.01 48.3974 595.83 0.0000 265.00 71. 0022 364.49 0.0000 427.87 26.6622 268.22 82.3652 366.42 0.0000 602.52 0.0000 269.46 75.5874 372.51 50.3789 604. 72 22.4415 270.03 75.6268 375.05 65.4242 607.14 25.6777 271.23 75.7092 377.52 61. 7944 609.32 30.5248 273.65 0.0000 356.01 63.9492 610.33 30.5399. 276.40 66.5541 .388.16 71. 68 60 614.28 16.1041 277.37 75.2630 388.63 0.0000 618.01 29.0391 277.60 74.4119 391.69 64.2965 620.36 38.7627 278.00 75.3037 264.66 57.0789 621. 93 20.6891 279.20 71. 9191 401.81 52.3626 . 630.19 0.0000 279.54 70.2076 402.40 60.9557 631. 2 9 21.6471 279.70 67.6168 404.85 57.2400 633.25 19.5007 280.46 66.7938 410.95 64.1770 634.78 0.0000 283.69 68.7232 413. 71 51.8192 635.95 26.0332 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 51. 4029 423. 72 0.0000 645.85 15.2567 285.90 427.09 61.9505 657.76 37.8032 287.50 63. 7161 427.87 54.2340 657.90 0.0000 290.67 55.1378 433.94 61.2491 661. 66 26.3438 293.27 0.0000 439.40 53.6561 664.57 0.0000 351. 93 61.9428 453.88 64. 9674 666.33 0.0000 295. 96 61.9815 463.37 60.3919 666.50 0.0000 879.38 31.7205 468.07 60.5619 667.71 0.0000 299.98 71. 4551 473.00 0.0000 677.62 30.9565 300.09 71.4617 475.06 53.8352 685.70 0.0000 300.13 71. 4633 476.78 56.8840 695.00 0.0000 301.36 71. 5375 477.60 71. 8887 696.49 26.7559 302.85 78.2585 482.18 48.0537 696. 51 26.7559 256.23 65.0826 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 33.4558 306.78 62.1016 497.08 46.4492 697.49 31. 2288 308.46 71. 9594 505.52 47.1793 702.65 22.3560 311. 90 63.2532 507.63 0.0000 706.68 22.3950 316.51 61.7016 511. 00 42.7438 711. 68 28.0538 319.41 0.0000 514.00 41. 2861 720.70 0.0000 320.08 0.0000 514.00 41.2861 721. 93 0.0000 321.04 60.1312 520.40 35.8061 722. 78. 15.2210 .323. 87 67.4622 520.69 0.0000 722.91 20.2954 325.23 55.3790 522.65 0.0000 723.31 18.6075 328.76 0.0000 527.90 0.0000 724.19 16.9220 333.37 70.6859 528.26 39.0422 727. 33 19.2039 333.97 67.9977 529.59 32.9010 733.00 18.6833 334.37 63.9380 529.87 0.0000 735.93 13.6045 338.28 65.4961 531.02 0.0000 333.97 10.2100 338.32 65.4976 537.26 0.0000 739.50 0.0000 311. 90 46.4709 546.56 0.0000 747.24 29.0455 340.48 46.4709 552.55 40.5917 748.06 20.5100 340.55 0.0000 563.25 34.5388 752.31 26.2526 344.28 50.2600 569.33 34.6476 753.82 0.0000 345.93 65.8770 946.00 34.6503 756.73 13.7217 351. 06 56.9469 569.70 31.5039 756.80 11. 4351 351. 93 56.9834 583.19 32.7773 884.68 15.4825 Page 3264 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 30.9880 1274.44 13.4728 1620.50 3.3085 766.42 30.9957 1001.03 13.4938 1621. 92 6.6189 766.84 24 .1121 1002.74 13.5013 1678.03 0.0000 772. 60 0.0000 1004.73 0.0000 1690.97 2.2389 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.5459 778.90 12 .1141 1028.54 0.0000 1063.66 10.9230 783.70 0.0000 1037.84 13.2745 1771. 35 3.6418 785.37 8.6752 1038.76 0.0000 1791.20 0.0000 792.07 19.7157 631.29 10.4582 1808.65 4.5862 794.95 15.0942 1048.07 0.0000 1810.72 0.0000 795.86 19.7455 1049.04 13.3207 1836.06 1.8443 810.06 14.8911 1050.41 11. 422.9 810.29 15.7681 1063.66 20.0720 344.28 15.7692 1077.00 0.0000 810.76 15.7714 1077.34 14.2605 815.77 0.0000 1085.87 16.3598 1048.07 0.0000 1093*. 63 13.5044 832.01 14.1328 1099.45 9.6631 834.85 13.2637 1112. 07 24.8297 835.71 14.1528 1112. 84 23.2837 836.80 0.0000 1115. 54 17.0887 846.75 0.0000 1120.29 10.6952 846.77 15.9879 1120.55 10.6959 856.80 0.0000 1221.41 3 .1123 860.56 18.7480 1129. 67 12.6747 871.09 13.4427 1131. 51 0.0000 873.19 18.8345 1147. 95 0.0000 875.33 0.0000 1173.23 21. 7220 879.38 15.2812 1177.95 15.8184 880.51 17.0860 1189.05 18.8434 883.24 18.9031 1204.77 18.9269 884.68 17.1115 1221.41 11. 0081 889.28 17.1399 1231.02 21.0705 894.76 18.9806 1235.36 0.0000 898.04 20.8129 1238.28 19.1021 900. 72 22.6440 1260.41 0.0000 903.28 15.4120 1271.87 13.1880 911.20 18.1824 1274.44 8.1216 912.08 18.1879 1274.54 8.1216 923.98 0.0000 1291.59 8.1582 926.50 19.1934 1298.22 0.0000 929 .11 17.3811 1312 .11 0.0000 937.49 16.5135 1332.49 13.3983 944.13 0.0000 1362.66 0.0000 946.00 16.5619 1365.19 11. 4310 949.00 17.5000 1368.63 0.0000 667.71 0.0000 1384.29 9.3972 962.31 19.0321 1408.01 3.3607 964.08 23.6984 1457.56 0.0000 966 .17 16.3040 1460.82 10.6366 911.20 21.3267 1489.16 7.4952 968. 97 21.3267 1505.03 6.4482 983.53 0.0000 1584.12 3.5010 984.45 0.0000 1596.21 0.0000 Page 3265 of 5809 VAX/VMS Nuclide Identification Report Generate9 3-0CT-2016 09:18:22.92 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GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM27.CNF;330 Background date : Z-OCT-2016 11:01:30. Sample date 2-DEC-2015 10:19:00. Acquisition date : 3-0CT-2016 08:16:22. Sample ID G405235018 Sample quantity 1.55815E+02 GRAM Detector name : GAM27 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.98 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 3 3 0 0 0 5 5 0 0 2 2. 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3266 of 5809 Energy 63.29* 74.84* 77.20 83.74* 87.27 93.05* 95.46 105*. 45 136.89 186.02* 238.71* 241.58 270.35 277.65 295.31* 300.02 328.39 338.51* 351. 96* 394.83 408.86 510.67* 536.91 554.81 583.29* 609.62* 645.81 654.80 661.76* 722.27 726.97 755.46 811.35 816.68 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 67 201 260 26 108 63 48 40 52 66 469 129 46 39 178 40 55 60 297 21 47 34 43 18 124 142 23 19 951 16 50 20 12 40 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 266 278 172 199 183 168 152 97 137 204 86 131 93 136 71 68 75 103 84 61 52 100 53 38 54 65 26 34 64 17 23 18 19 15 0.82 1. 31 0.84 1. 52 1. 53 1. 21 1. 41 0. 96 0.90 1. 01 1.11 2.06 1. 76 1. 46 1. 28 1. 63 2.34 1.16 1. 34 0. 72 1.14 2.45 7.37 3.48 1. 44 1. 58 2.44 4.26 1. 43 3.38 1. 90 1. 54 1. 24 4.54 125.90 149.00 153.73 166.81 173.88 185.43 190.27 210.25 273.15 371.45 476.86 482.61 540.18 554.79 590.12 599.53 656.30 676.54 703.47 78.9. 24 817.32 1021.02 1073.53 1109.35 1166.33 1219.03 1291.43 1309.43 1323.36 1444.45 1453.85 1510.85 1622.71 1633.37 122 144 144 165 171 182 182 208 270 366 469 469 536 548 .585 585 651 671 697 786 813 1012 1065 1101 1160 1213 1286 1300 1316 1439 1449 1507 1616 1625 9 l.86E-02 15 5.58E-02 15 7. 21E-02 7 7.29E-03 7 2.99E-02 13 l.75E-02 13 l.35E-02 6 l. llE-02 8 1. 45E-02 11 l.84E-02 21 1. 30E-01 21 3.58E-02 9 l.29E-02 13 1. lOE-02 19 4.95E-02 19 l.12E-02 10 1.52E-02 10 l.66E-02 11 8.26E-02 8 5. 71E-03 9 1. 30E-02 18 9.38E-03 19 1. 20E-02 13 4.98E-03 12 3.45E-02 13 3.95E-02 12 6.33E-03 15 5.38E-03 15 2.64E-01 10 4.40E-03 11 1. 37E-02 9 5.56E-03 9 3.20E-03 19 l.12E-02 46.5 16.0 9.8 92.1 23.0 39.1 52.2 42.3 40.8 44.9 5.8 26.3 40.3 63.0 11. 3 39.7 32.7 35.0 8.4 69.1 31. 3 77.7 42.8 75.4 15.1 14.6 51. 7 69.2 3.7 55.3 23.3 44*. 3 78.3 27.4 Fit 1.14E+OO 1. 75E+OO l.03E+OO l.22E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 862.01 24 43. 4.86 1724.08 1713 19 6.75E-03 67.7 36 0 911.47* 105 28 2.30 1823.05 1815 14 2.92E-02 14.8 37 0 953.31 11 9 1. 71 1906.78 1900 9 3. llE-03 56.6 38 2 964.74 34 16 2.24 1929.66 1923 22 9.46E-03 28.7 1.54E+00 39 2 968.79* 51 9 1. 97 1937.77 1923 22 1.42E-02 20.1 40 0 1120.06* 49 35 2.52 2240.50 2234 14 1.36E-02 29.8 41 0 1150. 90 14 '12 3.15 2302.21 229'6 12 3.89E-03 56.2 42 0 1255.13 9 18 2.84 2510.82 2500 15 2. 40E-03114. 3 43 0 1301.45 7 21 2. 68 2603.53 2591 14 2.04E-03145.3 44 0 1314.68 9 5 0.90 2629.99 2622 11 2.38E-03 63.0 45 0 1318.32 12 5 2.18 2637.29 2632 10 3.33E-03 45.3 46. 0 1339.26 5 11 0.51 2679.20 2668 14 l.48E-03136.7 47 0 1377.72 17 7 1. 08 2756.18 2750 13 4.58E-03 40.3 48 0 1460.95* 423 11 1. 70 2922.75 2915 15 1.17E-01 5.2 49 0 1480.60 10 3 2. 96 2962.08 2956 12 2.74E-03 47.6 50 3 1588.20 13 1 2.90 3177.46 3174 16 3.53E-03 29.5 6.09E-01 51 3 1592.38 11 3 1. 91 3185.83 3174 16 3.02E-03 39.1 52 0 1764.60* 37 3 2.04 3530.55 3524 13 1.04E-02 20.4 53 0 1847.52 15 0 1. 98 3696.53 3690 11 4.17E-03 25.8 Flag:."*" = P.eak area was modified 'by background subtraction Page 3267*of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:18:25 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample -ID 2-DEC-2015 10:19:00 G405235018 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:16:22 155.82 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA27 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3268 of 5809 PB-214 PB'-214. PB-214 PB-214 PB-214 PB-214. PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 87.09 242.00 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide EU-155 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 86.55 86.94 87.57 88.03 240.99 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.98 10.00 0.00 % Peak Energy . 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.403E+OO 1.319E+Ol 1.319E+Ol 10.43 OK C0-58 810.76 99.45* 2. 251E+OO 2. 571E-02 5.127E-01 156.68 OK CD-109 88.03 3.70* 7.568E+00 1. 37 9E+OO 2.183E+OO 81. 38 OK SN-126 64.28 9.60 5.536E+00 8.091E-01 8.091E-01 93.09 OK 86.94 8.90 7.568E+00 5.732E-01 5.732E-01 81. 38 OK 87.57 37.00* 7.568E+OO 1. 379E-01 1. 379E-01 81. 38 OK BA-137M 661.66 89.90* 2.624E+00 2:058E+OO 2.098E+OO 7.49 OK CS-137 661. 66 85.10* 2.624E+00 2.174E+OO 2.216E+OO 7.49 OK EU-155 86.55 30.70 7.568E+OO 1.662E-01 1.878E-01 81. 38 OK 105.31 21.10* 8.063E+OO 1.433E-01 1.619E-01 84.59 OK TL-208 277.37 6.60 5.128E+OO 6.519E-01 6.519E-01 125.97 OK 583.19 85.00* 2.886E+OO 2.619E-01 2.619E-01 30.18' OK 860.56 12.50 2.150E+OO 4.481E-01 4.481E-01 135.31 OK PB-212 74.82 10.28 6.758E+OO 1.207E+OO 1.207E+OO 49.92 OK 77 .11 17.10 6.949E+OO 1.376E+OO 1.376E+OO 19.56 OK 238.63 43.60* 5.747E+OO 1.060E+OO 1. 060E+OO 11. 65 OK 300.09 3.30 4.829E+OO 1.402E+OO 1. 402E+OO 79.42 OK BI-214 609.32 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 OK 1120.29 . 14. 92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 OK 1764.49 15.30 l.177E+OO 9.458E-01 9.461E-01 40.84 OK PB-214 74.82 5.80 6.757E+OO Line Not Found <<INT Reject 77 .11 9.70 6.949E+OO 2.425E+OO 2.426E+00 19.56 OK 87.09 3.41 7.559E+00 Line Not Found -----<<INT Reject 242.00 7.25 5.689E+OO Line Not* Found <<INT Reject 295.22 18.42 4.889E+00 1.099E+OO 1.lOOE+OO 22.56 OK 351. 93 35.60* 4.262E+OO 1.069E+OO 1.070E+OO 16.86 OK RN-222 609.32 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 OK 1120.29 14.92 1. 754E+OO 9.007E-01 9.0lOE--:01 59.54 OK 1764.49 15.30 1.177E+OO 9.458E-01 9.461E-01 40.84 OK RA-224 240.99 4.10* 5.697E+OO 1.181E+OO 1.181E+00 144.23 OK RA-226 609.32 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 OK 1120. 29 14.92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 OK 1764.49 15.30 1.177E+OO 9.458E-01 9.461E-01 40. 84 '* OK AC_.;228 105.21 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 OK 338.32 11. 27 4.394E+OO 6.612E-01 6.612E-01 69.99 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835.71 1. 61 2.201E+OO Line Not Found Absent 911.20 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 OK 968. 97 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 OK RA-228 105.21 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 OK 338.32 11.27 4.394E+OO 6.612E-01 6.612E-01 69.99 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835.71 1. 61 2. 201E+OO Line Not Found Absent 911. 20 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 OK 968. 97 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 OK TH-228 74.82 10. 28 . 6.758E+OO 1.207E+OO 1. 207E+OO 49.92 OK 77 .11 17.10 6.949E+OO 1.376E+OO 1. 37 6E+OO 19.56 OK 238.63 43.60* 5.747E+OO 1.060E+OO 1.060E+OO 11. 65 OK 300.09 3.30 4.829E+OO 1.402E+OO 1. 402E+OO 79.42 OK Page 3269 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff

pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 2.791E+OO 5.775E-Ol 5.775E-01 29.30 OK 1120.29 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 OK 1764.49 15.30 1.177E+OO 9.458E-01 9.458E-01 40.84 OK PA-231 283.69 1. 70 5.044E+OO Line Not Found Absent 301.36 5.35* 4.829E+OO 8.646E-01 8.646E-01 79.42 OK TH-232 105.21 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 OK 338.32 11. 27 4.394E+OO 6.612E-01 6.612E-01 69.99 OK 835.71 1. 61 2.201E+OO Line Not Found Absent 911.20 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 OK 968. 97 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 OK TH-234 63.29 3.70* 5.536E+OO 2.099E+OO 2.099E+OO 93.09 OK 92.59 4.23 7.800E+OO 1.184E+OO 1.184E+OO 78.13 OK U-234 609.32 45.49* 2.791E+OO 5.775E-01 5.775E-01 29.30 OK 1120. 29 14.92 1.754E+OO 9.007E-01 9.007E-01 59.54 OK 1764.49 15.30 l.177E+OO 9.458E-01 9.458E-01 40.84 OK U-238 63.29 3.70* 5.536E+OO 2.099E+OO 2.099E+OO 93.09 OK 92.59 4.23 7.800E+00 1.184E+OO 1.184E+OO 78.13 OK AM-243 43.53 5.90 2.021E+OO Line Not Found Absent 74.66 67.20* 6.758E+OO 1.846E-01 1.846E-01 OK ANH-511 511. 00 100.00* 3.192E+OO 5.553E-02 5.553E-02 155.34 OK Flag: "*" = Keyline Page 3270 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:18:26.16 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l * *Acquisition date 3-0CT-2016 08:16:22 Sensitivity : 3.000 *
Detector ID GAM27 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.98 Half life ratio : ***** *
Sample date 2-DEC-2015 10:19:00 Analyst initials: MXRl *
Sample ID G405235018 Sample Quantity 1.5582E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]'EFF GAM27 CAN.CNF;13 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.319E+Ol 1.348E+OO 4.997E-01 C0-58 5.127E-01 7.873E-01 9.769E-01 CD-109 2.183E+OO 1.741E+OO 1.691E+OO SN-126 1.379E-01 1.lOOE-01 1.071E-01 BA-137M 2.098E+OO 1.540E-01 5.879E-02 CS-137 2.216E+OO l.627E-01 6. 211E-02 EU-155 1.619E-01 1.342E-01 1.553E-01 TL-208 2.619E-01 7.747E-02 5.981E-02 PB-212 1.060E+OO 1. 211E-01 8.503E-02 BI-214 5.777E-01 l.659E-01 1. 211E-01 PB-214 l.070E+OO 1. 767E-01 1.179E-01 RN-222 5.777E-01 1.659E-01 1.211E-01 RA-224 1.181E+OO 1.670E+OO 9 .115E-01 RA-226 5.777E-01 l.659E-01 l.211E-01 AC-228 9.737E-01 2. 821E-01 2.043E-01 RA-228 9.737E-01 2.821E-01 2.043E-01 TH-228 1.060E+OO 1 :211E-01 8.503E-02 TH-230 5.775E-01 l.658E-01 1.210E-01 PA-231 8.646E-01 6. 729E-01 7.896E-01 TH-232 9.737E-01 2.821E-01 2.043E-01 TH-234 2.099E+OO 1.915E+OO 1.443E+OO U-234 5.775E-01 1.658E-01 1.210E-01 U-238 2.099E+:OO 1.915E+OO 1.443E+OO AM-243 l.846E-01 9.030E-02 6.479E-02 ANH-511 5.553E-02 8.454E-02' 5.039E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma) (pCi/GRAM BE-7 1.854E+OO 1.400E+Ol 2.679E+Ol NOT IDENT. NA-22 -1.638E-02 3.530E-02 6.409E-02 NOT IDENT. NA-24 O.OOOE+OO 1:960E+41 0.000E+OO SHORT HLIF AL-26 3.874E-02 2.728E-02 7.380E-02 NOT IDENT. SC-46 9.603E-02 3.228E-01 6.731E-01 FAIL ABUN Page 3271of5809 V-48 O.OOOE+OO l.790E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.233E+02 O.OOOE+OO SHORT HLIF MN-54 5.415E-02 5.306E-02 1.183E-01 NOT IDENT. C0-56 -2.903E-01 4.017E-01 7.258E-01 NOT IDENT. MN-56 O.OOOE+OO l.391E+41 O.OOOE+OO SHORT HLIF C0-57 -3.318E-03 4.215E-02 7.817E-02 FAIL ABUN FE-59 -3.865E+OO 6.688E+OO 1.197E+Ol NOT IDENT. C0-60 l.028E-02 2.364E-02 5.114E-02 NOT IDENT. ZN-65 6.215E-02 1.965E-01 3.498E-01 NOT IDENT. GE-68 -2.862E-01 2.015E+OO 3.890E+OO NOT IDENT. AS-73 -3.048E+OO 4.557E+OO 8.566E+OO NOT IDENT. AS-74 O.OOOE+OO 6.804E+03 0.000E+OO SHORT HLIF SE-75 -2.039E-01 l.943E-01 3.517E-01 FAIL ABUN BR-77 O.OOOE+OO l.285E+38 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 7.184E+o2 O.OOOE+OO SHORT HLIF RB-83 -4.170E-01 6. 969E-01 1.231E+OO NOT IDENT. KR-85 -4.591E+00 8.086E+OO 1.253E+Ol NOT IDENT. SR-85 -5.166E-01 9.109E-01 1.412E+OO NOT IDENT. RB-86 0.000E+OO 2.973E+04 O.OOOE+OO SHORT HLIF Y-88 1.'816E-02 2.207E-01 4.719E-01 NOT IDENT. Y-91 3.156E+02 5.163E+02 1. 07 5E+03 NOT IDENT. NB-94 l.547E-02 2.817E-02 5.626E-02 NOT IDENT. NB-95 -5.483E-01 8.881E-01 l.498E+OO NOT IDENT. NB-95M -4.289E-01 2.602E+OO 4.544E+OO NOT IDENT. ZR-95 2.137E+OO 1. 856E+OO 2.864E+00 FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 o:oooE+oo SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF Mo....:99 O.OOOE+OO 6.460E+32 O'.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 8.920E+40 O.OOOE+OO SHORT HLIF RH-101 -l.392E-02 3.173E-02 5.698E-02 NOT IDENT. RH-102 3. 331E-03 4.936E-02 9.487E-02 NOT IDENT. RU-103 5 .173E+OO-6.562E+OO 1.333E+Ol FAIL ABUN RH-106 -2.414E-01 4.562E-01 8.008E-01 NOT IDENT. RU-106 -2.414E-01 4.562E-01 8.008E-01 NOT IDENT. AG-108M -2.565E-02 J.068E-02 5.325E-02 FAIL ABUN AG-110M -2.689E-02 8. '62 6E-02 l.650E-01 NOT IDENT. SN-113 -8.626E-02 2.513E-01 4.150E-01 NOT IDENT. CD-115 O.OOOE+OO l.908E+40 0.000E+OO SHORT HLIF SN-117M O.OOOE+OO 1.178E+05 O.OOOE+OO SHORT HLIF TE-123M -2.056E-02 l.222E-01 2. 211E-01 NOT IDENT. SB-124 -6.167E-02 1.663E+OO 3. 451E+OO FAIL ABUN SB-125 4.597E-02 l.077E-01 2.124E-01 NOT IDENT. TE-125M l.914E+02 2.394E+02 4.763E+02 NOT IDENT. I-126 O.OOOE+OO 1.295E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.594E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.653E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 8.587E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.314E+27 O.OOOE+OO SHORT HLIF BA-133 -4.407E-02 4.771E-02 7.565E-02 FAIL ABUN I-133 .O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.050E-02 5.159E-02 1.013E-01 NOT IDENT. CS-135 l.794E-02 1.364E-01 2.444E-01 NOT IDENT. I-135 O.OOOE+OO 1.632E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.064E+05 O.OOOE+OO SHORT HLIF CE-139 9.394E-03 9.938E-02 *1.834E-01 NOT IDENT. BA-140 O.OOOE+OO 4.235E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.524E+05 O.OOOE+OO SHORT HLIF CE-141 -1.689E+Ol 2.669E+Ol 4.643E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 2. 211E-01 3.517E-01 6.332E-01 NOT IDENT. PM-144 -1.013E-02 4.502E-02 8. 228E-02 . NOT IDENT. PR-144 -1.243E+OO 3.975E+OO 7.157E+OO NOT IDENT. PM-146 8.201E-03 4.350E-02 8.424E-02 NOT IDENT. ND-147 O.OOOE+OO 4.887E+07 O.OOOE+OO SHORT HLIF PM-147 -3.412E+Ol 7.324E+02 l.361E+03 NOT IDENT. PM-149 0.000E+OO l.237E+41 O.OOOE+OO SHORT HLIF EU-150 -1.696E-03 2.627E-02 4.539E-02 FAIL ABUN EU-152 1.567E-02 9.275E-02 1. 811E-01 FAIL ABUN GD-153 -5.762E-02 1.549E-01 2.621E-01 NOT IDENT. EU-154 -3.713E-02 8.688E-02 1.589E-01 FAIL ABUN TB-160 1.226E+00 1.504E+OO 3.373E+OO FAIL ABUN H0-166M 1.593E-03 4.615E-02 8.804E-02 FAIL ABUN TM-171 5.599E+OO 9.701E+OO 1.982E+Ol NOT IDENT. HF-172 8.408E-03 2.042E-01 3.808E-01 FAIL ABUN LU-172 -4.981E-03 6.783E-02 1.315E-01 FAIL ABUN LU-176 3.662E-03 2.207E-02 4.363E-02 FAIL ABUN HF-181 -8.016E-01 4.807E+OO 8*. 964E+OO NOT IDENT. Page 3272 of 5809 TA-182 8 .139E-02 8. 541E-01 1.666E+OO FAIL ABUN RE-183 1.166E+OO 1.691E+OO 3.450E+OO NOT IDENT. RE-184 9.775E+OO 2.902E+Ol 6.016E+Ol NOT IDENT. W-188 8.433E+OO 1.113E+02 l.983E+02 FAIL ABUN IR-192 3.218E-01 4.774E-01 9.718E-01 FAIL ABUN HG-203 1.448E+OO 2.448E+OO -4. 597E+OO NOT IDENT. BI-207 -1.332E-02 3. 611E-02 6.789E-02 FAIL ABUN PB-210 -4.432E-01 1.285E+OO 2.558E+OO NOT IDENT. BI-211 O.OOOE+OO 4.868E-01 7.353E-01 FAIL ABUN PB-211 3.733E-01 6.982E-01 1.277E+OO NOT IDENT. BI-212 O.OOOE+OO 6.990E-01 l.187E+OO FAIL ABUN RN-219 5.585E-03 3.627E-01 6. 966E-01 FAIL ABUN RA-223 5.092E-01 5.614E-01 l.083E+OO FAIL ABUN AC-227 l.163E-01 2.215E-01 4.484E-01 FAIL ABUN TH-227 l.163E-01 2.215E-01 4.484E-01 FAIL ABUN TH-229 -4.498E-02 4.879E-01 8.695E-01 FAIL ABUN TH-231 5.092E-01 5.614E-01 1.083E+OO FAIL ABUN PA-233 -5.449E-03 5.268E-02 1. 020E-01 FAIL ABQN PA-234 l.837E-01 2.256E-01 4.892E-01 FAIL ABUN PA-234M -2.650E+OO 3.674E+OO 6.504E+OO NOT IDENT. U-235 1.255E-01 1.698E-01 3.256E-01 FAIL ABUN NP-237 -5.449E-03 5.268E-02 l.020E-01 FAIL ABUN NP-238 O.OOOE+OO 1.637E+41 O.OOOE+OO SHORT HLIF NP-239 2.723E-02 2.115E-01 3.989E-01 FAIL ABUN PU-239 2.824E+02 2.898E+02 5.698E+02 NOT IDENT. AM-241 4.583E-03 8.366E-02 1.516E-01 NOT IDENT. CM-243 2.000E-02 7.881E-02 1.415E-01 FAIL ABUN BK-247 -7.230E-02 6.601E-02 1.191E-01 FAIL ABUN CM-247 1.871E-02 3.313E-02 6.670E-02 FAIL ABUN CF-249 1. 4 7 5E-02 3.654E-02 7.250E-02 NOT IDENT. CF-251 1.980E-02 1.136E-01 2.084E-01 NOT IDENT. Page 3273 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:18:23.76 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 409 10.66* 1.403E+OO 1.319E+Ol l.319E+Ol 10.43 C0-58 '810.76 12 99.45* 2. 251E+OO 2.571E-02 5.127E-01 156.68 CD-109 88.03 139 3.70* 7.568E+OO 2.392E+001 3.788E+OO 45.93 SN-126 64.28 89 9.60 5.536E+OO 8. 091E-01 8.091E-01 93.09 86. 94 139 8.90 7.568E+OO 9.944E-01 9.944E-01 45.93 87.57 139 37.00* 7.568E+OO 2.392E-01 2.392E-01 45.93 BA-137M 661. 66 1007 89.90* 2*.624E+00 2.058E+OO 2.098E+OO 7.49 CS-137 661. 66 1007 85.10* 2.624E+OO 2.174E+OO 2.216E+OO 7.49 EU-155 86.55 139 30.70 7.568E+OO 2.883E-01 3.258E-01 45.93 105.31 51 21.10* 8.063E+OO 1.433E-01 1.619E-01 84.59 TL-208 277.37 46 6.60 5.128E+OO 6.519E-01 6.519E-01 125.97 583.19 133 85.00* 2.886E+OO 2.619E-01 2.619E-01 30.18 860.56 25 12.50 2.150E+00 4. 481E-01 4.481E-01 135.31 BI-211 72. 87 ------1. 23 6.585E+OO ------Line Not Found ------351.06 337 12.92* 4.262E+OO 2.946E+OO 2.946E+OO 16.86 PB-212 74.82 263 10.28 6.758E+OO 1.827E+OO 1.827E+OO 32.07 77 .11 339 17.10 6.949E+OO 1.376E+OO 1.376E+00 19.56 238.63 551 43.60* 5.747E+OO 1.060E+OO l.060E+OO 11. 65 300.09 46 3.30 4.829E+OO l.402E+00 1.402E+OO 79.42 BI-214 609.32 152 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 1120.29 49 14.92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 1764.49 35 15.30 *1.177E+00 9.458E-01 9. 461E-01 40.84 PB-214 74.82 263 5.80 6.758E+OO 3.238E+OO 3.239E+OO 32.07 77 .11 339 9.70 6.949E+OO 2.425E+OO 2.426E+OO 19.56 87.09 139 3.41 7.568E+OO 2.595E+00 2.596E+OO 45.93 242.00 152 7.25 5.697E+OO 1. 7 67E+OO 1. 768E+00 52.67 295.22 205 18.42 4.889E+OO l.099E+OO 1.lOOE+OO 22.56 351. 93 337 35.60* 4.262E+OO l.069E+00 1.070E+OO 16.86 RN-222 609.32 152 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 1120. 29 49 14.92 1.754E+OO 9.007E-01 9.0lOE-01 59.54 1764.49 35 15.30 1. l 77E+OO 9.458E-01 9.461E-01 40.84 RA-224 240.99 152 4.10* 5.697E+00 3.125E+OO 3.125E+OO 52.67 RA-226 609.32 152 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 1120.29 49 14.92 1. 754E+OO 9.007E-Ol* 9.0lOE-01 59.54 1764.49 35 15.30 1.177E+OO 9.458E-01 9. 461E-01 40.84 AC-228 105.21 51 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 338.32 68 11. 27 4.394E+OO 6.612E-01 6.612E-01 69.99 794.95 ------4.25 2.286E+OO ------Line Not Found ------835. 71 ------1. 61 2.201E+OO ------Line Not Found ------911. 20 107 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 968.97 52 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 RA-228 105.21 51 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 338.32 68 11. 27 4.394E+oo 6.612E-01 6.612E-01 69.99 794.95 ------4.25 2.286E+OO ------Line Not Found ------835.71 ------1. 61 2.201E+OO ------Line Not Found ------911. 20 107 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 968. 97 52 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 Page 3274 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 263 10.28 6.758E+OO l.827E+OO 1.827E+OO 32.07 77 .11 339 17.10 6.949E+OO 1. 376E+OO 1.376E+OO 19.56 238.63 551 43.60*. 5.747E+OO 1.060E+OO 1.060E+OO 11. 65 300.09 46 3.30 4.829E+OO 1.402E+OO 1.402E+OO 79.42 TH-230 609.32 152 45.49* 2.791E+OO 5.775E-01 5.775E-01 29.30 1120.29 49 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 1764.49 35 15.30 1.177E+OO 9.458E-01 9.458E-01 40.84 PA-231 283.69 ------1. 70 5.044E+OO ------Line Not Found ------301.36 46 5.35* 4.829E+OO 8.646E-01 8.646E-01 79.42 TH-232 105.21 51 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 338. 32 68 11. 27 4.394E+OO 6.612E-01 6.612E-01 69.99 835. 71 ------1. 61 2.201E+OO ------Line Not Found ------911. 20 107 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 968. 97 52 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 TH-234 63.29 89 3.70* 5.536E+OO 2.099E+OO 2.099E+OO 93.09 92.59 81 4.23 7.800E+OO 1.184E+OO 1.184E+00 78.13 U-234 609.32 152 45.49* 2. 791E+OO 5.775E-01 5.775E-01 29.30 1120.29 49 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 1'764.49 35 15.30 1.177E+OO 9.458E-01 9.458E-01 40.84 U-238 63.29 89 3.70* 5.536E+OO 2.099E+OO 2.099E+OO 93.09 92.59 81 4.23 7.800E+OO 1.184E+OO l.184E+00 78.13 AM-243 43.53 ------5.90 2.021E+OO ------Line Not Found ------74.66 263 67.20* 6.758E+OO 2.795E-01 2.795E-01 32.07 ANH-511 511. 00 37 100.00* 3.192E+OO 5.553E-02 5.553E-02 155.34 Flag: '!*" Key line Page 3275 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Total number of lines in spectrum 53 Number of unidentified lines 15 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-22 6 AC-228 RA-228 TH-'-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 70. 8 6D 461. 40D 2.30E+05Y 30.08Y 30.08Y 4.75Y l.41E+10Y 7.04E+08Y. 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+'10Y l.41E+l0Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 19.9 1. 58 1. 00 1. 02 1. 02 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 . 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.319E+Ol 2.571E-02 2.392E+OO 2.392E-01 2.058E+OO 2.174E+OO 1.433E-01 2.619E-01 2.946E+OO 1.060E+OO 5.775E-01 1.069E+00 5.775E-01 3.125E+OO 5.775E-01 9.737E-01 9.737E-01 1.060E+OO 5.775E-01 8.646E-01 9.737E-01 2.099E+OO 5.775E-01 2.099E+00 2.795E-01 5.553E-02 4.095E+Ol 4.095E+Ol Decay Corr pCi/GRAM l.319E+Ol 5.127E-01 3.788E+00 2.392E-01 2.098E+OO 2.216E+OO l.619E-01 2.619E-01 2.946E+OO 1.060E+OO 5.777E-01 1.070E+OO 5.777E-01 3.125E+OO 5.777E-01 9.737E-01 9.737E-01 1.060E+OO 5.775E-01 8.646E-01 9.737E-01 2.099E+OO 5.775E-01 2.099E+OO 2.795E-01 5.553E-02 4.294E+Ol 4.294E+Ol 71. 70% Decay Corr 2-Sigma Error 0.138E+Ol 8.033E-01 1.740E+OO 1.099E-01 0.157E+OO 0.166E+OO l.369E-01 0.791E-01 0.497E+OO 0.124E+OO 1.693E-01 0.180E+OO l.693E-01 1.646E+OO l.693E-01 2. 87'9E-01 2.879E-01 0.124E+OO l.692E-01 6.866E-01 2.879E-01 1.954E+OO l.692E-01 1.954E+OO' 0. 896E-01 8.627E-02 Manually accepted 2-Sigma %Error 10.43 156.68 45.93 45.93 7.49 7.49 84.59 30.18 16. 86 11. 65 29.30 16.86 29.30 52.67 29.30 29.57 29.57 11. 65 29.30 79.42 29.57 93.09 29.30 93.09 32.07 155.34 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 3276 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235018 Acquisition date : 3-0CT-2016 08:16:22 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.74 34 258 . 1. 52 166.81 165 7 7.29E-03 **** 7.38E+OO T 3 95.46 62 195 1. 41 190.27 182 13 1.35E-02 **** 7.87E+OO T 0 136.89 65 170 0.90 273.15 270 8 1. 45E-02 81. 7 7.87E+OO T 0 186.02 80 246 1. 01 371.45 366 11 1. 84E-02 89.9 6.81E+OO T 0 2*70.35 54 108 1. 76 540.18 536 9 1.29E-02 80.7 5.23E+OO T 0 328.39 62 86 2.34 656.30 651 10 1.52E-02 65.3 4.50E+OO T 0 394.83 23 69 0.72 789.24 786 8 5.71E-03 **** 3.89E+OO 0 408.86 *52 58 1.14 817.32 813 9 1. 30E-02 62.6 3.79E+OO 0 536.91 47 57 7.37 1073.53 1065 19 1.20E-02 85.6 3.07E+OO T 0 554.81 19 41 3.48 1109. 35 1101 13 4.98E-03 **** 3.00E+OO 0 645.81 24 28 2.44 1291.43 1286 12 6.33E-03 **** 2.67E+OO T 0 654.80 21 36 4.26 1309.43 1300 15 5.38E-03 **** 2.64E+OO 0 722. 27 17 18 3.38 1444.45 1439 10 4.40E-03 **** 2.46E+OO T 0 72 6. 97 52 24 1. 90 1453.85 1449 11 l.37E-02 46.5 2.44E+OO T 0 755.46 21 19 1. 54 1510.85 1507 9 5.56E-03 88.6 2.38E+OO T 0 816.68 42 15 4.54 1633.37 1625 19 1.12E-02 54.9 2.24E+OO T 0 953.31 11 9 1. 71 1906.78 1900 9 3. llE-03 **** 1.99E+OO T* 2 964.74 35 16 2.24 1929.66 1923 22 *9.46E-03 57.3 1. 97E+00 T 0 1150.90 14 12 3.15 2302.21 2296 12 3.89E-03 **** 1.72E+OO 0 1255.13 9 18 2.84 2510.82 2500 15 2.40E-03 **** 1. 60E+OO 0 1301.45 7 20 2.68 2603.53 2591 14 2.04E-03 **** 1. 55E+OO 0 1314.68 8 5 0.90 2629.99 2622 11 2.38E-03 **** 1.54E+OO 0 1318.32 12 5 2.18 2637.29 2632 10 3.33E-03 90.5 1.53E+OO 0 1339.26 5 10 0.51 2679.20 2668 14 1.48E-03 **** 1.51E+OO 0 1377. 72 16 6 1. 08 2756.18 2750 13 4.58E-03 80.5 1.48E+OO 0 1480.60 10 3 2. 96 '2962.08 2956 12 2.74E-03 95.3 1.39E+OO 3 1588.20 12 1 2.90 3177.46 3174 16 3.53E-03 59.0 l.30E+OO 3 1592.38 10 3 1. 91 3185.83 3174 16 3.02E-03 78.l 1.30E+OO 0 1847.52 14 0 1. 98 3696.53 3690 11 4.17E-03 51. 6 1.12E+OO Flags: "T" = Tentatively associated Page 3277 of 5809 VAX/VMS Nuclide Identification .Report Generated 03-0CT-2016 09:18:38.22 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l *
Acquisition date 3-ocr-2016 08:16:22 Sensitivity 3.000 *
Detector ID GAM27 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.98 Half life ratio : ***** *
Sample date 2-DEC-2015 10:19:00 Nuclide Library : SOLID *
Sample ID G405235018 "Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5582E+02 GRAM * *Wet wt corr 1.00000 Wet Weight
0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;13
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.059E-01 4.291E-01 8.062E-01 5.104E-02 2.650E-02 2.800E-02 7.300E-02 2.717E-02 3.978E-02 5.525E-02 5.445E-02 5.525E-02 4.264E-01 5.525E-02 8. 966E-02 8. 966E-02 3.978E-02 5.523E-02 3.683E-01 8.966E-02 6.868E-01 5.523E-02 6.868E-01 3.084E-02 2.308E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3278 of 5809 Le (pCi/GRAM l.236E+Ol 2.682E-02 O.OOOE+OO 3.121E-02 2.968E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR--95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 . CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3279 of 5809 O.OOOE+OO 5.320E-02 3.152E-01 O.OOOE+OO 3.688E-02 5.212E+OO 2.073E-02 1.572E-01 l.697E+OO 4.043E+OO O.OOOE+OO 1.630E-01 O.OOOE+OO O.OOOE+OO 5.599E-01 5.749E+OO 6.477E-01 O.OOOE+OO l.935E-01 4.801E+02 2.546E-02 6.709E-01 2.141E+OO 1.290E+00 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.697E-02 4.229E-02 6.159E+OO 3. 569E-0.l 3.569E-01 2.456E-02 7.234E-02 1.907E-01 O.OOOE+OO O.OOOE+OO l.040E-01 1.346E+00 9.855E-02 2.253E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.509E-02 O.OOOE+OO 4.613E-02 1.141E-01 O.OOOE+OO O.OOOE+OO 8.617E-02 0.000E+OO O.OOOE+OO 2.195E+Ol* 0.000E+OO 3.000E-01 3.636E-02 3.162E+OO 3.882E-02 O.OOOE+OO 6.429E+02 o. o*ooE+oo 2.107E-02 8.440E-02 1.237E-01 6.668E-02 1.491E+OO 3.904E-02 9.380E+OO 1. 799E-01 5.772E-02 2.028E-02 4.108E+OO 7.375E-Oi SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN . NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABPN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3280 of 5809 l.636E+OO 2. 672E+01 9 .196E+Ol 4.545E-01 2.143E+OO 2.900E-02 1.215E+OO 3.554E-01 5.915E-01 5.528E-01 3.216E-01 5.038E-01 2. llOE-01 2. llOE-01 4 .113E-01 5.038E-01 4.724E-02 2.170E-01 2.840E+OO 1.546E-01 4. 724E-02 O.OOOE+OO 1. 886E-01 2. 711E+02 7.188E-02 6. 651E-02 5.523E-02 3. 090E-02' 3.364E-02 9; 851E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:18:43.44 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407" * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l *
date 3-0CT-2016 08:16:22 Sensitivity : 3.000 *
Detector ID GAM27 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit 75.000 *
Elapsed real time: 0 01:00:00.98 Half life ratio : ***** *
Sample date 2-DEC-2015 10:19:00 Nuclide Library : SOLID *
Sample ID G405235018 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.5582E+02 GRAM *
Quantity Err(%) : 1.2836E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;l3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ) ( 1 . 96-s i grna) ( 1. 96-sigma) K-40 1.319E+Ol 1.514E+OO 1.514E+OO C0-58 5.127E-01 7.876E-01 7.876E-01 CD-109 2.183E+OO 1. 762E+OO 1. 762E+OO SN-126 1. 37 9E-01 1. llOE-01 1. llOE-01 BA-137M 2.098E+OO 1.785E-01 1.785E-01 CS-137 2.216E+OO 1.885E-01 1.885E-01 EU-155 l.619E-01 1. 347E-01 1.347E-01 TL-208 2.619E-01 7.827E-02 7.827E-02 PB-212 1.060E+OO l.338E-01 l.338E-01 BI-214 5.777E-01 l.677E-01 l.677E-01 PB-214 1.070E+OO l.824E-01 l.824E-01 RN-222 5.777E-01 1.677E-01 1.677E-01 RA-224 l.181E+OO 1.676E+OO 1. 676E+00 RA-226 5.777E-01 l.677E-01 l.677E-01 AC-228 9.737E-01 2.865E-01 2.865E-01 RA-228 9.737E-01 2.865E-01 2.865E-01 TH-228 1.060E+OO 1.338E-01 l.338E-01 TH-230 5.775E-01 l.677E-01 1.677E-01 PA-231 8.646E-01 6.978E-01 6.978E-01 TH-232 9.737E-01 2.865E-01 2.865E-01 TH-234 2.099E+OO 1.971E+OO l.971E+OO U-234 5.775E-01 1.677E-01 l.677E-01* U-238 2.099E+OO 1.971E+OO 1. 971E+OO AM-243 1.846E-01 9.180E-02 9.180E-02 ANH-511 5.553E-02 8.457E-02 8.457E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuci'ide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 l.854E+OO l.400E+Ol 1.403E+Ol NOT IDENT. NA-22 -1.638E-02 3.531E-02 3.607E-02 NOT IDENT. NA-24 -l.000E+41 5.275E+41 O.OOOE+OO SHORT HLIF AL-26 3.874E-02 2.739E-02 3. 24'9E-02 NOT IDENT. SC-46 9.603E-02 3.228E-01 3.257E-01 FAIL ABUN Page 3281of5809 V-48 2.628E+03 1. 7 90E+04 l.794E+04 SHORT HLIF CR-51 -i.305E+02 4.233E+02 4.274E+02 SHORT HLIF MN-54 5.415E-02 5. 311E-02 5.845E-02 NOT IDENT. C0-56 -2.903E-01 4.019E-01 4.227E-01 NOT IDENT. MN-56 -l;OOOE+41 l.392E+41 0.000E+OO SHORT HLIF C0-57 -3.318E-03 4.215E-02 4.217E-02 FAIL ABUN FE-59 -3.865E+OO 6.694E+OO 6.917E+OO NOT IDENT. C0-60 l.028E-02 2.365E-02 2.410E-02 NOT IDENT. ZN-65 6.215E-02 1. 965E-01 l.985E-01 NOT IDENT. GE-68 -2.862E-01 2.015E+OO 2.019E+OO NOT IDENT. AS-73 -3.048E+OO 4.600E+OO 4.801E+OO NOT IDENT. AS-74 7.101E+03 6.829E+03 7.543E+03 SHORT HLIF SE-75 -2.039E-01 l.945E-01 2.152E-01 FAIL ABUN BR-77 1.125E+39 9.939E+39 O.OOOE+OO SHORT HLIF SR-82 2.157E+02 7.184E+02 7.250E+02 SHORT HLIF RB-83 -4.170E-01 6.992E-01 7.241E-01 NOT IDENT. KR-85 -4.591E+OO 8.088E+OO 8.349E+OO NOT IDENT. SR-85 -5.166E-01 9. lllE-01 9.404E-01 NOT IDENT. RB-86 -l.055E+04 2.974E+04 3.012E+04 SHORT HLIF Y-88 l.816E-02 2.207E-01 2.209E-01 NOT IDENT. Y-91 3.156E+02 5.165E+02 5.357E+02 NOT IDENT. NB-94 1. 54 7E-02 2.818E-02 2.903E-02 NOT IDENT. NB-95 -5.483E-01 8.884E-01 9.221E-01 NOT IDENT. NB-95M -4.289E-01 2.602E+OO 2.609E+OO NOT IDENT. ZR-95 2 .137E+OO 1. 858E+OO 2.093E+OO FAIL ABUN NB-97 l.OOOE+41 2.235E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.000E+41 2.432E+42 O.OOOE+OO SHORT HLIF M0-99 2. 651E+32 6.463E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 8.974E+40 O.OOOE+OO SHORT HLIF RH-101 -l.392E-02 3.183E-02 3.245E-02 NOT IDENT. RH-102 3. 331E-03 4.936E-02 4.938E-02 NOT IDENT. RU-103 5.173E+OO 6.566E+OO 6. 968E+00 FAIL ABUN RH-106 -2.414E-01 4.564E-01 4.692E-01 NOT IDENT. RU-106 -2.414E-01 4.564E-01 4.692E-01 NOT IDENT. AG-108M -2.565E-02 3.070E-02 3.280E-02 FAIL ABUN AG-llOM -2.689E-02 8.627E-02 8.712E-02 NOT. IDENT. SN-113. -8.626E-02 2.514E-01 2.543E-01 NOT IDENT. CD-115 -8.038E+37 1. 908E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 5.614E+03 l.178E+05 l.178E+05 SHORT HLIF TE-123M -2.056E-02 l.222E-01 1. 22 6E-01 NOT IDENT. SB-124 -6.167E-02 l.663E+OO l.664E+OO FAIL ABUN SB-125 4.597E-02 l.077E-01 l.097E-01 NOT IDENT. TE-125M l.914E+02 2.397E+02 2.548E+02 NOT IDENT. I-126 2.786E+05 l.295E+06 l.301E+06 SHORT HLIF SB-126 l.358E+05 l.595E+06 l.596E+06 SHORT HLIF SB-127 -2. 715E+22 6.816E+22 O.OOOE+OO SHORT HLIF I-131 -9.392E+08 8.587E+09 8.598E+09 SHORT* HLIF I-132 -l.OOOE+41 1. 962E+42 O.OOOE+OO SHORT HLIF TE-132 -2.444E+26 l.318E+27 O.OOOE+OO SHORT HLIF BA-133 -4.407E-02 4.774E-02 5. l 71E-02 FAIL ABUN I-133 l.OOOE+41 2.749E+41 O.OOOE+OO SHORT HLIF CS-134 3.050E-02 5 .161E-02 5. 341E-02 NOT IDENT. CS-135 1. 794E-02 l.364E-01 l.367E-01 NOT IDENT. I-135 l.OOOE+41 7.102E+41 O.OOOE+OO SHORT HLIF CS-136 -6.038E+04 4.065E+05 A.074E+05 SHORT HLIF CE-139 9.394E-03 9.940E-02 9.949E-02 NOT IDENT. BA-140 5.050E+06 4.240E+06 4. 812E+o6 SHORT HLIF LA-140 -l.231E+05 4.524E+05 4.558E+05 SHORT HLIF CE-141 -l.689E+Ol 2.670E+Ol 2.776E+Ol NOT IDENT. CE-143 l.OOOE+41 2.263E+41 O.OOOE+OO SHORT HLIF CE-144 2.211E-01 3.519E-01 3.657E-01 NOT IDENT. PM-144 -l.013E-02 4.503E-02 4. 526E-02* NOT IDENT. PR-144 -l.243E+OO
3.975E+OO 4.014E+OO NOT IDENT. PM-146 8.201E-03 4.350E-02 4.366E-02 NOT IDENT. ND-147 7.012E+06 4.887E+07 4.897E+07 SHORT HLIF PM.:...14 7 -3.412E+Ol 7.324E+02 7.326E+02 NOT IDENT. PM-149 l.OOOE+41 l.256E+41 0.000E+OO SHORT HLIF EU-150 -1. 696E-03 2.627E-02 2.628E-02 FAIL ABUN EU-152 l.567E-02 9.276E:-02 9.303E-02 FAIL ABUN GD-153 -5.762E-02 l.549E-01 1. 571E-01 NOT IDENT. EU-154 -3.713E-02 8.689E-02 8.849E-02 FAIL ABUN TB-160 1. 226E+OO l.506E+OO l.604E+OO FAIL ABUN H0-166M l.593E-03 4.615E-02 4.615E-02 FAIL ABUN TM-171 5.599E+00 9.713E+OO l.004E+Ol NOT IDENT. HF-172 8.408E-03 2.042E-01 2.042E-01 FAIL ABUN LU-172 -4.981E-03 6.783E-02 6.787E-02 FAIL ABUN LU-176 3.662E-03 2.207E-02 2. 213E-02 FAIL ABUN HF-181 -8.0l6E-01 4.807E+OO 4.820E+OO NOT IDENT. Page 3282 of 5809 TA-182 8.139E-02 8.541E-01 8.549E-01 FAIL ABUN RE-183 1.166E+00 1.701E+OO 1. 781E+OO NOT IDENT. RE-184 9.775E+OO 2.912E+Ol 2.945E+Ol NOT IDENT. W-188 8.433E+OO l .113E+02 l .114E+02 FAIL ABUN IR-192 3.218E-01 4.776E-01 4.992E-01 FAIL ABUN HG-203 1.448E+OO 2.449E+OO 2.534E+OO NOT IDENT, BI-207 -l.332E-02 3.611E-02 3. 661E-02 FAIL ABUN PB-210 -4.432E-01 1.285E+OO 1. 301E+OO NOT IDENT. BI-211 2.946E+OO 5.046E-01 l.421E+OO FAIL ABUN PB-211 3.733E-01 6.985E-01 7.185E-01 NOT IDENT. BI-212 1.534E+OO 7.033E-01 9.862E-01 FAIL ABUN RN-219 5.585E-03 3.627E-01 3.627E-01 FAIL ABUN RA-223 5.092E-01 5. 623E-01. 6.074E-01 FAIL ABUN AC-227 1.163E-01 2.221E-01 2.282E-01 FAIL ABUN TH-227 l.163E-01 2.221E-01 2.282E-01 FAIL ABUN TH-229 -4.498E-02 4.879E-01 4.883E-01 FAIL ABUN TH-231 5.092E-01 5.623E-01 6.074E-01 FAIL ABUN PA-233 -5.449E-03 5.268E-02 *5.274E-02 FAIL ABUN PA-234 1.837E-01 3.083E-01 3.193E-01 FAIL ABUN PA-234M -2.650E+OO 3.675E+OO 3.865E+00 NOT IDENT. U-235 l.255E-01 1.699E-01 l.791E-01 FAIL ABUN NP-237 -5.449E-03 5.268E-02 5.274E-02 FAIL ABUN NP-238 -1.000E+41 1.638E+41 O.OOOE+OO SHORT HLIF NP-239 2.723E-02 2 .115E-01 2 .119E-01 FAIL ABUN PU-239 2.824E+02 2. 901E+02 3.168E+02 NOT IDENT. AM-241 4.583E-03 8.366E-02 8.368E-02 NOT IDENT. CM-243 2.000E-02 7.883E-02 7.935E-02 FAIL ABUN BK-247 -7.230E-02 7.505E-02 FAIL ABUN CM-247 1. 871E-02 3.328E-02 3.434E-02 FAIL ABUN CF-249 1. 4 7 5E-02 3.656E-02 3.716E-02 NOT IDENT. CF-251 l.980E-02 l.136E-01 l.140E-01 NOT IDENT. Page 3283 of 5809
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 87.8545 87.09 159.0519 136.47 79.3663 45.60 104.5483 87.57 138.2499 140.51 0.0000 46.54 100.0665 88.03 138.3703 143.76 89.3306 49.72 0.0000 88.34 165.0228 144.24 77.9277 51. 35 106.2390 88.47 165.0636 145.44 111. 3422 51. 87 93.8141 89. 96 111.5187 152.43 84.5711 52.39 88.1330 1093.63 134.8350 153.25 0.0000 52.97 102.8177 91.11 0.0000 323.87 92.8943 53.44 113.6281 92.59 133.2050 156.02 0.0000 54.07 94.3593 93.35 133. 3905 158.56 0.0000 57.36 0.0000 94.56 133. 6827 159.00 87.6228 57.53 96.1768 94.65 133.7039 162.33 90.3354 57 .. 98 92.3545 94. 67. 133.7087 162.66 0.0000 59.27 109.0760 94.87 133. 7572 163.33 97.4961 59.32 109.0895 97.43 105.2203 165.86 77.7687 59.54 109.1482 98.43 86.8883 176.31 89.4882 60. 96 102.9268 98.44 86.8901 176.60 0.0000' 61.17 100.3383 99.53 78.4929 177.52 94.3947 62.93 131.2527 100 .11 92.1433 181.07 0.0000 63.29 131.3635 102.03 83.1325 181.52 94.4334 63.58 131.4532 103.18 74.6791 184.41 98.7601 64.28 131.6682 103.37 74.7029 143.76 98.9077 66.73 101. 6488 105.21 82.1410 193.51 104.6367 67.24 125.8688 105.31 82.1544 197.03 106.2609 125.81 *143.7539 106.12. 96. 6983 198.01 91.7015 67.75 143.7757 106.47 96.7548 201.83 87.1683 69.67 123.188.6 109.28 80.5203 203.43 94.6956 70.83 125.5269 111. 00 97 .1129 205.31 77.6320 72. 81 143. 6872 111.76 0.0000 210.85 87 .. 9971 72. 87 143.7056 114. 06 89.9149 215.65 77.2219 74.66 130.6455 116.30 0.0000 222 .11 90.2615 74.82 130.6895 116.74 96.9026 227.09 84.8273 74.97 130.7305 119.76 92.9318 227.38 78.1301 77 .11 131.3145 121.12 90.9081 228.16 0.0000 78.74 135.8712 121. 22 97.5746 228.18 81.5546 79.69 123.7582 121.78 97.6579 116.74 81. 5546 80.12 125.2416 122.06 95.4791 235.69 94.0040 80.19 0.0000 122.92 101.1614 235. 96 70.3099 80.57 119.8445 123.07 104.5201 238.63 70.4880 81. 00 128.2203 265.00 94.5997 238.98 0.0000 81. 07 117.8965 125.81 97.1342 240.99 70.6451 81. 75 120.1277 127.23 117.4769 242.00 70.7118 83.79 137.2469 127.91 113 .1153 244.70 55.0892 84.00 137.3033 129.30 98.7556 252.40 0.0000 85.43 100.1345 131.20 133.9149 252.80 83.4650 86.55 100.3499 133.02 87.2537 254.15 0.0000 86.79 158. 9603 133.52 88.8205 256.23 72.5024 86.94 159.0056 136.00 90.6445 260.90 0.0000 Page 3284 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 76.5256 355.39 0.0000 584.27 33.0334 264.80 73.0557 356.01 67.2539 595.83 0.0000 265.00 79.1584 364.49 0.0000 427.87 25.7744 268.22 62.8066 366.42 0.0000 602.52 0.0000 269.46 68 .1135 372. 51 44.4058 604.72 27.4382 270.03 68.1469 375.05 59.6252 607.14 37.1644 271.23 66.4675 377.52 65.4119 609.32 36.6632 273.65 0.0000 356.01 40.9371 610.33 36.6798 276.40 59.7352 388.16 47.7376 614.28 38.9092 277.37 59.7836 388.63 0.0000 618.01 25.9844 277.60 59.7961 391. 69 50.2409 620.36 28.1794 278.00 59.8154 264.66 56.7901 621.93 30.3698 279.20 50.1904 401.81 48.1628 630.19 0.0000 279.54 50.2055 402.40 42.3994 631.29 21.7847 279.70 54.1754 404.85 41.9840 633.25 23.9846 280.46 51.5660 410.95 50.8669 634.78 0.0000 283.69 60.9857 413.71 40.7644 635.95 17.4648 284.31 0.0000 414.70 0.0000 636.99 . 0. 0000 285.41 53.1079 423. 72 0.0000 645.85 26.3135 285.90 0.0000 427.09 52.8475 657.76 13.2261 287.50 51.4261 427.87 46.9980 657.90 0.0000 290.67 53.3374 433.94 62.8971 661.66 28.1531 293.27 0.0000 439.40 65.0762 664.57 0.0000 351. 93 62'. 4577 453.88 42.7629 6'66. 33 0.0000 295. 96 62. 4961 463.37 61.9987 666.50 0.0000 879.38 62.6272 468.07 61.1638 667.71 0.0000 299.98 62.6984 473.00 0.0000 677.62 24.4573 300.09 62.7026 475.06 46.3070 685.70 0.0000 300 .13 62.7055 476.78 51.3901 695.00 0.0000 301.36 64.5601 477.60 45.3653 696.49 22.4129 302.85 61.9431 482.18 43.4610 696. 51 23.5336 256.23 55. 0130 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.6623 306.78 54.9325 497.08 35.6672 697.49 24.6641 308.46 57.7096 505.52 19. 9630 702.65 22.4707 311.90 54.2480 507.63 0.0000 706.68 24.7590 316.51 55.3483 511. 00 40.0438 711. 68 18.0436 319.41 0.0000 514.00 53. 9911 720.70 0.0000 320.08 0.0000 514.00 53. 9911 721. 93 0.0000 321. 04 61.0036 520.40 44.3717 722.78 10.1960 323.87 41.0605 520.69 0.0000 722. 91 10 .1964 325.23 47.9530 522.65 0.0000 723.31 10.1982 328.76 0.0000 527.90 0.0000 724.19 10.2019 333.37 67.5440 528.26 29.0117 727.33 15.3221 333.97 57.9205 529.59 28.6175 733.00 17.7461 334.37 52.419"3 529.87 0.0000 735.93 22.7783 338.28 71. 0157 531. 02 0.0000 333.97* 20.5129 338.32 71.0173 537.26 0.0000 739.50 0.0000 311. 90 63.7399 546.56 0.0000 747.24 19.4494 340.48 63.7399 552.55 25.1787 748.06 13.7334 340.55 0.0000 563.25 44.2986 752.31 24.0736 344.28 59.2839 569.33 39.1424 753.82 0.0000 345.93 58.9832 946.00 39.1454 756.73 20.6704 351. 06 49.3327 569.70 39.1484 756.80 20. 6711 351.93 49.3640 583.19 33. 0170 884.68 18.4258 Page 3285 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 34.5728 1274.44 11. 2401 1620.50 9.8849 766.42 31.1232 1001.03 20.6378 1621. 92 14.2830 766.84 31.1287 1002.74 21. 5878 1678.03 0.0000 772. 60 0.0000 1004.73 19.7227 1690.97 4.4578 77 6. 52 0.0000 507.63 0.0000 1750.46. 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.6189 778.90 15.0577 1028.54 0.0000 1063.66 4.5288 783.70 0.0000 1037.84 16.1295 1771.35 5.6622 785.37 17.4170 1038.76 0.0000 1791.20 0.0000 792.07 31.4308 631.29 17.1244 1808.65 0.9125 794.95 25.6380 1048.07 0.0000 1810.72 0.0000 795.86 25.6470 1049.04 22.8486 1836.06 6.4210 810.06 19.6896 1050.41 18. 0966 810.29 19.6909 1063.66 15.2998 344.28 19.6923 1077.00 0.0000 810.76 17.5842 1077.34 17.2815 815.77 0.0000 1085.87 17.3254 1048.07 0.0000 1093.63 18.3297 832.01 22.1527 1099.45 22.2251 834.85 14.1924 1112. 07 17.4573 835. 71 16.8587 1112.84 24.3909 836.80 0.0000 1115. 54 21. 7465 846.75 0.0000 1120. 29 23.3320 846.77 23.1'618 1120.55 23.3335 856.80 0.0000 1221.41 23.3379 860.56 16 .1142 1129. 67 14.6210 871.09 17.9712 1131.51 0.0000 873.19 12.5892 1147.95 0.0000 875.33 0.0000 1173.23 17.7605 879.38 10.8142 1177.95 14. 8196 880.51 17.1289 1189.05 20.8103 883.24 15.3404 1204.77 15.9229 884.68 20.7651 1221. 41 18.9930 889.28 15. 3725 1231. 02 23.0505 894.76 15.4016 1235.36 0.0000 898.04 14.5117 1238.28 27 .1104 900.72 17.2489 1260.41 0.0000 903.28 17.2640 1271. 87 9 .1165 911. 20 17.3104 1274.44 13.1769 912.08 17.3156 1274.54 13.1769 923.98 0.0000 1291. 59 16.2891 926.50 20.1470 1298.22 0.0000 929 .11 19.2479 1312 .11 . 0. 0000 937.49 18.3820 1332.49 3.2914 944.13 0.0000 1362.66 0.0000 946.00 11.5870 1365.19 14.5161 949.00 16.2374 1368.63 0.0000 667. 71 0.0000 1384.29 2.7777 962. 31 .16.3083 1408.01 8.3804 964.08 13.9069 1457.56 0.0000 966.17 13. 9165 1460.82 7.4234 911.20 13.9288 1489.16 7.4717 968. 97 13.9288 1505.03 10.7117 983.53 *0.0000 1584.12 6.9754 984.45 0.0000 1596.21 0.0000 Page 3286 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:21:30.20 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GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l DKA100: ,[CANBERRA. GAMMA.ARCHIVE. GAMMA] BKG GAMll .CNF; 517 . Background date : Z-OCT-2016 11:00:34. Sample date 8-DEC-2015 14:30:00. Acquisition date : 3-0CT-2016 08:21:03. Sample J;D G405235019 Sample quantity : 1.75975E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.63 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000* Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike : . LCS ID . : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 2'6 27 28 29 30 31 32 33 34 0 2* 2 0 0 0 0 0 0 2 2 4 4 4 4 4 0 0 0 0 0 1 1 0 0 0 0 0 0 6 6 0 0 0 Page 3287 of 5809 Energy 63.02* 74.87* 77.15* 83.89* 86.82 89.82 92.82* 185.56* 209.55 238.65* 241. 64 270.47 274.41 276.97 295.35* 300.14 338.45* 351.87* 415.66 428.86 469.33 491. 68 494.93 498.75 510.95* 544.28 583.46* 609.42* 660. 96* 668.21 670.75 701.59 727.59* 747.05 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area* 26 137 212 45 58 64 59 175 50 400 100 56 40 20 182 38 83 248 34 10 25 15 16 . 32 18 12 160 167 23 . 28 9 16 40 20 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 272 156 134 165 157 123 156 124 127 90 95 52 44 72 55 53 87 51 112 41 25 25 18 23 45 22 29 44 18 19 11 38 18 17 1.13 125.95 0.88 149.66 0.91 154.22 1.04 167.71 0.74 173.58 1.37 179.58 1. 46 185. 58 1.20 371.18 1.42 419.20 1.03 477.44 1.41 483.41 1.75 541.11 1.20 549.00 1.76 554.12 1.36 590.91 1.80 600.49 0.92 677.16 1.32 704.01 7.63 831.66 1.41 858.08 1.81 939.06 1.55 983.78 1. 55 990. 28 3.26 997.93 1.03 1022.34 3.54 1089.02 1 . 5 6 .116 7 . 4 3 1. 23 1219. 36 0.84 1322.50 1. 54 1337. 00 1.65 1342.09 5.90 1403.77 1.92 1455.79 1.62 1494.74 122 146 146 165 172 177 182 365 414 473 473 537 537 537 586 586 672 698 813 851 935 977 977 993 1019 1081 1162 1214 1316 1333 1333 1395 1451 1490 11 7.13E-03127.1 14 3.80E-02 15.9 3.97E-01 14 5. 89E-02 11. 0 7 1.26E-02 49;5 6 1.62E-02 36.4 6 1. 78E-02 30. 4 7 1. 65E-02 39. 8 13 4.85E-02 15.6 11 l.37E-02 46.2 15 1.llE-01 6.2 2.44E+OO 15 2. 77E-02 21. 6 27 1.57E-02 28.2 4.29g+oo* 27 1. llE-02 31.1 27 5.44E-03 92.0 23 5.06E-02 3.06E+OO 23 l.06E-02 45.7 11 2.30E-02 24.7 12 6.89E-02 8.7 24 9.52E-03 84.0 9 2. 7 9'E-0312 0 .. 8 9 6. 91E-03 41. 4 17 4.30E-03 63.8 1.99E+OO 17 4.46E-03 48.9 10 8.92E-03 32.8 9 4.92E-03 92.2 10 3.20E-03 82.5 14 4. 45E-02 11. 0 11 4. 63E-02 11. 2 11 6.49E-03 43.8 12 7.79E-03 27.8 9.15E+OO 12 2. 38E-03 71. 4 15 4.31E-03 89.8 11 l.12E-02 26.8 10 5.55E-03 45.0 Peak Search Report (continued) Page : 2 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 768.97 24 27 2.85 1538.59 1533 11 6.59E-03 51. 5 36 0 817.97 15 14 3.22 1636.63 1631 11 4.13E-03 55.0 37 0 860.97 28 12 1. 35 1722.66 1717 11 7.88E-03 31.1 38 0 911.28*. 87 19 2.09 1823.31 1817 15 2.41E-02 15.7 39 0 935.17 11 9 1.29 1871. 08 1867 8 3.18E-03 57.9 40 1 964. 7 9 26 20 1. 90 1930.35 1920 25 7.29E-03 33.5 1.53E+OO 41 1 968. 7 9 50 15 1. 84 1938.35 1920 25 1. 38E-02 21. 9 42 0 1003.33* 30 4 5.74 2007.44 2000 15 8.36E-03 25.3 43 0 1116. 48 11 11 1. 51 2233.79 2225 12 3.03E-03 69.8 44 0 1120. 37* 42 8 1. 39 2241.57 2237 10 1.1 7E-02 20.5 45 0 1153. 38 . 14 22 2.48 2307.60 2301 11 3.89E-03 70.2 46 0 1166 .18 10 7 2.27 2333.20 2329 7 2.78E-03 54.1 47 0 1336. 20 9 4 0.68 2673.26 2669 8 2.36E-03 52.6 48 0 1377.44 18 5 2.28 2755.75 2750 10 5.00E-03 33.1 49 0 1415.36 12 0 0.83 2831.58 2827 9 3.33E-03 28.9 50 0 1460.91* 413 8 1. 73 2922.68 2915 14 1.15E-01 5.1 51 0 1509.86 7 5 1. 79 3020.57 3014 10 l.94E-03 70.7 52 0 1764.78* 32 3 2 .13 3530.35 3524 12 8.81E-03 22.1 53 0 1847.73 7 2 1. 26 3696. 23 3691 9 l.90E-03 54.9 Flag: "*" = Peak area was modified by backgr6und subtraction . Page 3288 of 5809

' VMS Nuc'lide Identification Report V3 .1 Generated 3-0CT-2016 09: 21: 32 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 14:30:00 G405235019 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:21:03 175.98 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMAll 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 TH-229 85.43 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.63 10.00 0.00 % Peak Energy 0.0% Page 3289of5809 Nuclide Line Activity Report Page : 2 Sample ID : G4052350]_9 Acquisition date 3-0CT-2016 08:21:03 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM-pCi/GRAM %Error Status K-40 1460.82 10.66* l.238E+OO 1. 308E+Ol 1.308E+Ol 10.29 OK ZN-65 1115. 54 50.60* 1.552E+OO 6.051E-02 l.418E-01 139.62 OK CD-109 88.03 3.70* 6.225E+OO 4.599E-01 7.215E-01 244.59 OK SN-126 64.28 9.60 3.845E+OO 4.320E-01 4.320E-01 254.25 OK 86.94 8.90 6.225E+OO 1.912E-01 1.912E-01 244.59 OK 87.57 37.00* 6.225E+OO 4.599E-02 4.599E-02 244.59 OK BA-137M 661.66 89.90* 2.341E+OO 5.215E-02 5.314E-02 87.64 OK CS-137 661. 66 85.10* 2.341E+OO 5.509E-02 5.614E-02 87.64 OK TL-208 277.37 6.60 4.720E+OO 3.303E-01 3.303E-01 183.91 OK 583.19 85.00* 2.581E+OO 3.483E-01 3.483E-01 21. 98 OK 860.56 12.50 l.906E+OO 5.387E-01 5.387E-01 62.18 OK PB-212 74.82 10.28 5.239E+OO 9.007E-01 9.007E-01 56.51 OK 77 .11 17.10 5.459E+OO 1.382E+OO 1.382E+OO 21.98 OK 238.63 43.60* 5.299E+OO 9.268E-01 9.269E-01 12.41 OK 300.09 3.30 4.424E+OO 1.357E+OO l.357E+00 91. 45 OK BI-214 609.32 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 OK 1120.29 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 OK 1764.49 15.30 1.040E+OO 8.093E-01 8.096E-01 44.16 OK PB-214 74.82 5.80 5.234E+OO Line Not Found <<INT Reject 77 .11 9.70 5.459E+OO 2.436E+OO 2.437E+OO 21. 98 OK 87.09 3.41 6.242E+OO Line Not Found <<INT Reject 242.00 7.25 5.244E+OO Line Not Found <<INT Reject 295.22 18.42 4.482E+OO 1.150E+OO l.150E+OO 19.77 OK 351.93 35.60* 3.884E+OO 9.156E-01 9.159E-01 17.41 OK RN-222 609.32 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 OK 1120. 29 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 OK 1764.49 15.30 l.040E+OO 8.093E-01 8. 096E-01 44.16 OK RA-224 240.99 4.10* 5.250E+OO 4.419E-01 4.419E-01 258.61 OK RA-226 609.32 45.49* 2.494E+OO 6. 972E-01 6.975E-01 22.43 OK 1120.29 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 OK 1764.49 15.30 1. 040E+oo* 8.093E-01 8.096E-01 44.16 OK AC-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 OK 794.95 4.25 2.028E+OO Line Not Found Absent 835.71 1. 61 1.951E+OO Line Not Found Absent 911.20 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 OK 968. 97 15.80 1.738E+OO 8.072E-01 8. 072E-01 43.85 OK RA-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11.27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 OK 794.95 4.25 2.028E+OO Line Not Found Absent 835. 71 1. 61 1. 951E+OO '-----Line Not Found Absent 911. 20 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 OK 968. 97 15.80 1. 738E+OO 8.072E-01 8. 072E-01 43.85 OK TH-228 74.82 10.28 5.239E+OO 9.007E-01 9.007E-01 56.51 OK 77.11 17.10 5.459E+OO l.382E+OO 1.382E+OO 21. 98 OK 238.63 43.60* 5.299E+00 9.269E-01 9.269E-01 12.41 OK 300.09 3.30 4.424E+OO 1.357E+OO l.357E+OO 91. 45 OK TH-229 85.43 14.70 6.225E+OO 1 .. 158E-01 1.158E-01 244.59 OK 88.47 24.00 6.409E+OO 2.491E-01 2.491E-01 60.75 OK Page 3290 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Nuclide Type: Nuclide Energy %Abn %Eff Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error Status 193.51 4.41* 6 .133E+OO Line Not Found Absent 210.85 2.80 5. 821E+OO 1.651E+OO 1.651E+OO 92.48 OK TH-230 609.32 45.49* 2.494E+OO 6. 972E-01 6. 972E-01 22.43 OK 1120. 29 14. 92* 1.548E+OO 7.912E-01 7.912E-01 41. 03 OK 1764.49 15.30 1.040E+OO' 8.093E-01 8.093E-01 44.16 OK PA-231 283.69 1. 70 4.630E+OO Line Not Found Absent 301.36 5.35* 4.424E+OO 8. 372E-01 8.372E-01 91.45 OK TH-232 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 OK 835. 71 1. 61 1.951E+OO Line Not Found Absent 911. 20 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 OK 968. 97 15.80 1.738E+OO 8.072E-01 8. 072E-01 43.85 OK TH-234 63.29 3.70* *3:845E+OO 1.121E+OO 1.121E+OO 254.25 OK 92.59 4.23 6.570E+OO. 1.273E+OO 1.273E+OO 79.53 OK U-234 609.32 45.49* 2.494E+OO 6.972E-01 6. 972E-01 22.43 OK 1120.29 14.92 1.548E+OO 7.912E-01 7.912E-01 41. 03 OK 1764.49 15.30 1.040E+OO 8.093E-01 8.093E-01 44.16 OK U-235 89.96 3.47 6.409E+OO 1. 723E+OO 1. 723E+OO 60.75 OK 93.35 5.60 6.570E+OO 9.616E-01 9.616E-01 79.53 OK 143.76 10. 96* 7.059E+OO Line Not Found -----Absent 163.33 5.08 6. 731E+OO Line Not Found Absent 185.72 57.20 6.293E+OO 2.677E-01 2.677E-01 31.14 OK 205.31 5.01 5.902E+OO Line Not Found Absent U-238 63.29 3.70* 3.845E+OO l.121E+OO 1.121E+00 254.25 OK 92.59 4.23 6.570E+OO 1.273E+OO l.273E+00 79.53 OK AM-243 43.53 5.90 9.310E-01 Line Not Found Absent 74.66 67.20* 5.239E+OO l.378E-01 1.378E-01 56.51 OK ANH-511 511. 00 100.00* 2.868E+OO 3.004E-02 3.004E-02 184.44 OK Flag: "*" = Keyline Page 3291 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:21:33.25 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 49407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l *
Acquisition date 3-0CT-2016 08:21:03 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
Sample date 8-DEC-2015 14:30:00 Analyst initials: MXRl * *Sample ID G405235019 Sample Quantity 1.7598E+02 GRAM *
Batch Number 1596247 Wet Weight 0."00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN **
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMll 'CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclidei" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.308E+Ol 1.319E+OO ZN-65 l.418E-01 l.940E-01 CD-109 7.215E-01 1. 729E+OO SN-126 4.599E-02 l.102E-01 BA-137M 5.314E-02 4.564E-02 CS-137 5.614E-02 4.822E-02 TL-208 3.483E-01 7.503E-02 PB-212 9.269E-01 l.127E-01 BI-214 6.975E-01 1.533E-01 PB-214 9.159E-01 l.562E-01 RN-222 6.975E-01 l.533E-01 RA-224 4.419E-01 1.120E+OO RA-226 6.975E-01 l.533E-01 AC-228 8.277E-01 2.547E-01 RA-228 8.277E-01 2.547E-01 TH-228 9.269E-01 1.127E-01 TH-229 -8.168E-02 3.649E-01 TH-230 6. 972E-01 l.532E-01 PA-231 8. 372E-01 7.503E-01 TH-232 8.277E-01 2.547E-01 TH-234 1.121E+OO 2.793E+OO U-234 6. 972E-01 1.532E-01 U-235 -2.306E-02 l.394E-01 U-238 1.121E+00 2.793E+OO AM-243 1.378E-01 7. 631E-02 ANH-511 3.004E-02 5.430E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3292 of 5809 Key-Line Activity (pCi/GRAM -2.030E+00 -4.410E-03 O.OOOE+OO 1. 871E-02 K.L. Cnt Uncert ( 1. 96-sigma) 9.521E+OO 3.432E-02 1. 960E+41 2.462E-02 MDA (pCi/GRAM 3.933E-01 2.419E-01 1.412E+OO 9. 996E-02 4. 713E-02 4.978E-02 5.067E-02 8.229E-02 l.022E-01 9. 511E-02 1.022E-01 8.823E-01 1.022E-01 1.987E-01 l.987E-01 8.229E-02 6.825E-01 l.022E-:01 6.279E-01 1.987E-01 1.538E+OO 1.022E-01 2.680E-01 1.538E+OO 7.049E-02 4.182E-02 MDA (pCi/GRAM l.863E+Ol 6.846E-02 O.OOOE+OO 6.2-llE-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 3.402E-01 2.517E-01 6.183E-Ol FAIL ABUN V-48 O.OOOE+OO 9.984E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3. ll 7E+02 0.000E+OO SHORT HLIF MN-54 -5.091E-03 5. 301E-02 l.003E-01 NOT IDENT. C0-56 -1.179E-01 3.829E-01 7.025E-01 NOT IDENT. MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 4.973E-03 3.363E-02 6.752E-02 NOT IDENT. C0-58 -2.941E-01 3.921E-01 6.621E-01 NOT IDENT. FE-59 -1.537E+OO 4. 969E+OO 9.690E+OO NOT IDENT. C0-60 -1.192E-02 4. 096E-02 6.849E-02 NOT IDENT. GE-68 1. 051E+OO 1.852E+OO 4.066E+OO NOT IDENT. AS-73 -6.730E-01 5.407E+00 1.124E+Ol NOT IDENT. AS-74 O.OOOE+OO 4. 441E+03 O.OOOE+OO SHORT HLIF SE-75 -2.080E-02 1.573E-01 2.918E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 978E+3*7 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.237E+02 O.OOOE+OO SHORT HLIF RB-83 8.125E-03 5.009E-01 1.004E+OO NOT IDENT. KR-85 -1. 717E+OO 5.560E+OO 9.456E+OO NOT IDENT. SR-85 -1.822E-01 5.869E-01 9.978E-01 NOT IDENT. RB-86 O.OOOE+OO 2.390E+04 O.OOOE+OO SHORT HLIF Y-88 l.539E-01 1.336E-01 4.012E-01 NOT IDENT. Y-91 l.451E+02 4 .130E+02 8. 711E+02 NOT IDENT. NB-94 3.236E-02 5.694E-02 4.936E-02 FAIL ABUN NB-95 4.936E-01 8.228E-01 1.545E+OO NOT IDENT. NB-95M 2.028E+OO 2.085E+OO 3. 960E+OO NOT IDENT. ZR-95 2.861E-01 1.125E+OO 2.282E+OO NOT IDENT. NB-97 O.OOOE+OO l.585E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 1.205E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -6.699E-03 2.612E-02 5.036E-02 NOT IDENT. RH-102 -1.461E-02 4.451E-02 8.412E-02 NOT IDENT. RU-103 8. 096E+OO 4.274E+OO 9.608E+OO FAIL ABUN RH-106 -2.769E-01 4.128E-01 7.376E-01 NOT IDENT. RU-106 -2.769E-01 4.128E-01 7.376E-01 NOT IDENT. AG-108M 6.667E-03 1.918E-02 4.064E-02 NOT IDENT. AG-llOM -4.382E-03 7.159E-02 1.392E-01 NOT IDENT. SN-113 -5.393E-02 l.605E-01 3.157E-01 NOT IDENT. CD-115 O.OOOE+OO 2.409E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 0.000E+OO 6.910E+04 O.OOOE+OO SHORT HLIF TE-123M -l.664E-02 9.651E-02 l.848E-01 NOT IDENT. SB-124 1.150E+OO 1.310E+OO 3.577E+OO NOT IDENT. SB-125 6.234E-02 l.477E-01 1.689E-01 FAIL ABUN TE-125M 8.779E+Ol 1. 970E+02 4.059E+02 NOT IDENT. I-126 O.OOOE+OO 7.461E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.010E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.446E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3. 541E+09 0.000E+OO S.HORT HLIF I-132 0.000E+OO 5.442E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.044E+26 O.OOOE+OO SHORT HLIF BA-133 2.751E-03 3.202E-02 5.973E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 -1.254E-02 4.511E-02 8.276E-02 NOT IDENT. CS-135 -l.282E-02 l.107E-01 l.886E-01 NOT IDENT. I-135 O.OOOE+OO 1.843E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.139E+05 O.OOOE+OO SHORT HLIF .CE-139 9.921E-02 8.832E-02 1.845E-01 NOT IDENT. BA-140 O.OOOE+OO l.032E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.577E+05 O.OOOE+OO SHORT HLIF CE-141 -l.223E+OO 1.804E+Ol 3.498E+Ol NOT IDENT. CE-143 0.000E+OO 9.385E+40 O.OOOE+OO SHORT HLIF CE-144 5.676E-02 2.533E-01 5.079E-01 NOT IDENT. PM-144 1. 962E-02 4.483E-02 8.540E-02 NOT IDENT. PR-144 1. 786E+OO 3.906E+OO 7.461E+OO NOT IDENT. PM-146 4.898E-04 2.943E-02 6.0lOE-02 FAIL ABUN ND-147 O.OOOE+OO 2*. 339E+07 O.OOOE+OO SHORT HLIF PM-147 2. 411E+02 6.008E+02 1.227E+03 NOT IDENT. PM-149 O.OOOE+OO 3.548E+40 O.OOOE+OO SHORT HLIF EU-150 -5.887E-03 2.094E-02 3.722E-02 FAIL ABUN EU-152 6.035E-03 7.271E-02 1.488E-01 FAIL ABUN GD-153 8.733E-03 1.268E-01 2.560E-01 NOT IDENT. EU-154 -1.268E-02 8.373E-02 l.664E-01 FAIL ABUN EU-155 2.673E-02 7.650E-02 1. 571E-01 FAIL ABUN TB-160 -1.163E+OO 1.475E+OO 2.444E+OO FAIL ABUN H0-166M -1 . .428E-02 4.819E-02 8.957E-02 FAIL ABUN TM-171 -1.285E+OO 1. 2 69E+Ol 2.648E+Ol NOT IDENT. HF-172 -8.547E-02 1. 759E-01 3.337E-01 FAIL ABUN LU-172 2.802E-02 6.473E-02 1. 379E-01 FAIL ABUN Page 3293 of 5809 LU-176 -1. 2 90E-02 1. 860E-02 3.159E-02 FAIL ABUN HF-181 -1. 802E+OO 3*.171E+OO 5.940E+OO NOT IDENT. TA-182 4.024E-Ol 6.947E-01 l.513E+OO FAIL ABUN RE-183 6.868E-01 1. 784E+OO 3.825E+OO NOT IDENT. RE-184 7.369E+OO 2.491E+Ol 5.015E+Ol NOT IDENT. W-188 -8.317E-01 9.107E+Ol 1.564E+02 FAIL ABUN IR-192 1.873E-01 3.482E-01 6.921E-01 FAIL ABUN HG-203 7.031E-01 l.858E+OO 3.612E+OO NOT IDENT. BI-207 l.043E-02 3.756E-02 7. 951E-02 FAIL ABUN PB-210 1.166E+OO 1.708E+OO 3.780E+OO NOT IDENT. BI-211 O.OOOE+OO 4.304E-01 6.421E-01 FAIL ABUN PB-211 -1.196E-01 5.261E-01 9.302E-01 NOT IDENT. BI-212 O.OOOE+OO 6.742E-01 1.117E+OO FAIL ABUN RN-219 5.979E-02 2.698E-01 5.614E-01 FAIL ABUN RA-223 -3.781E-02 4.420E-01 8. 962E-01 FAIL ABUN AC-227 -6.068E-02 1. 723E-01 3 .119E-01 FAIL ABUN TH-227 -6.068E-02 1. 723E-01 3 .119E-01 FAIL ABUN TH-231 -3.781E-02 4.420E-01 8. 962E-01 FAIL ABUN PA-233 -5.017E-02 4. 711E-02 7.543E-02 FAIL ABUN PA-234 2.962E-02 2.102E-01 4.173E-01 NOT IDENT. PA....:234M 3.362E+00 3. lllE+OO 6. 960E+OO NOT IDENT. NP-237 -5.017E-02 4.711E-02 7.543E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 2.354E-02 l.642E-01 3.315E-01 FAIL ABUN PU-239 -2.539E+Ol 2.347E+02 4. 572E+02 NOT IDENT. 9.666E-03 8.947E-02 1. 750E-01 NOT IDENT. CM-243 *-3.383E-03 6.738E-02 1.350E-01 FAIL ABUN BK-247 -1. 496E-02 5.689E-02 l.036E-01 FAIL ABUN CM-247 -4.980E-03 2.489E-02 4.952E-02 FAIL ABUN CF-249 -6.187E-03 2.648E-02 5.266E-02 NOT IDENT. CF-251 4. 211E-02 8.575E-02 1.720E-01 NOT IDENT. Page 3294 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:21:30.92 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 405 10.66* 1.238E+OO 1.308E+Ol 1.308E+Ol 10.29 ZN-65 1115. 54 11 50.60* 1.552E+OO 6. 051E-02 1.418E-01 139.62 CD-109 88.03 82 3.70* 6.225E+OO 1.519E+OO 2.384E+OO 72. 74 SN-126 64.28 37 9.60 3.845E+OO 4.320E-01 4.320E-01 254.25 86.94 82 8.90 6.225E+OO 6.317E-01 6.317E-01 72.74 87.57 82 37.00* 6.225E+OO 1.519E-01 1.519E-01 72.74 BA-137M 661.66 26 89.90* 2. 341E+OO 5.215E-02 5.314E-02 87.64 CS-137 661.66 26 85.10* 2. 341E+OO 5.509E-02 5.614E-02 87.64 TL-208 277.37 24 6.60 4.720E+OO 3.303E-01 3.303E-01 183.91 583.19 179 85.00* 2. 581E+OO 3.483E-01 3.483E-01 21. 98 860.56 30 12.50 1.906E+OO 5.387E-01 5.387E-01 62.18 BI-211 72.87 ------1. 23 5.033E+OO ------Line Not Found ------351.06 297 12.92* 3.884E+OO 2.523E+OO 2.523E+OO 17.41 PB-212 74.82 196 10.28 5 .. 239E+OO 1.549E+OO 1.549E+OO 31. 79 77 .11 302 17.10 .5. 459E+OO 1.382E+OO 1.382E+OO 21. 98 238.63 502 43.60* 5.299E+OO 9.269E-01 9. 2'69E-01 12.41 300.09 46 3.30 4.424E+OO 1.357E+OO 1.357E+OO 91. 45 BI-214 609.32 185 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 1764.49 30 15.30 1.040E+OO 8. 093E--01 8. 096E-01 44.16 PB-214 74.82 196 5.80 5.239E+OO 2.746E+OO 2.747E+OO 31. 79 77 .11 302 9.70 5.459E+OO 2;436E+OO 2.437E+OO 21. 98 87.09 82 3.41 6.225E+OO 1.649E+OO 1.649E+OO 72.74 242.00 125 7.25 5.250E+OO 1.400E+OO l.400E+OO 43.23 295.22 222 18.42 4.482E+OO l.150E+OO l.150E+OO 19.77 351.93 297 35.60* 3.884E+00 9.156E-01 9.159E-01 17.41 RN-222 609.32 185 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 1764.49 30 15.30 1.040E+OO 8.093E-01 8. 096E-01 44.16 RA-224 240.99 125 4.10* 5.250E+OO 2.475E+OO 2.475E+OO 43.23 RA-226 609.32 185 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 1764.49 30 15.30 1.040E+OO 8.093E-01 8. 096E-01 44.16 AC-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 99 11.27 4.0lOE+OO 9.376E-01 9.376E-01 49_50* 794.95 ------4.25 2.028E+OO ------Line Not Found ------835.71 ------1. 61 1. 951E+OO ------Line Not Found ------911.20 91 25.80* l.823E+00 8.277E-01

8.277E-01 31. 41 968. 97 52 15.80 1.738E+OO 8.072E-01 8. 072E-01 43.85 RA-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 99 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 794.95 ------4.25 2.028E+OO ------Line Not Found ------835.71 ------1. 61 1. 951E+OO ------Line Not Found ------911.20 91 25.80* 1.823E+OO 8.277E-Ol 8.277E-01 31. 41 968.97 52 15.80 1.738E+OO 8.072E-01 8.072E-01 43.85 TH-228 74.82 196 10.28 5.239E+OO 1.549E+OO 1.549E+OO 31. 79 77 .11 302 17.10 5.459E+OO 1.382E+OO 1.382E+OO 21. 98 Page 3295 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 502 43.60* 5.299E+OO 9.269E-01 9.269E-01 12.41 300.09 46 3.30 4.424E+OO 1.357E+OO l.357E+00 91. 45 TH-229 85.43 82 14.70 6.225E+OO 3.824E-01 3.825E-01 72. 74 88.47 90 24.00 6.409E+OO 2.491E-01 2.491E-01 60.75 193.51 ------4.41* 6.133E+OO ------Line Not Found ------210.85 63 2.80 5.821E+OO 1. 651E+OO 1. 651E+OO 92.48 TH-230 609.32 185 45.49* 2.494E+OO 6.972E-01 6. 972E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.912E-01 41.03 1764.49 30 15.30 1.040E+OO 8.093E-01 8.093E-01 44.16 PA-231 283.69 ------1. 70 4.630E+OO ------Line Not Found ------301.36 46 5.35* 4.424E+OO 8.372E-01 8.372E-01 91. 45 TH-232 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 99 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 835. 71 ------1. 61 1.951E+OO ------Line Not Found ------911.20 91 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 968. 97 52 15.80 1.738E+OO 8. 072E-01 8. 072E-01 43.85 TH-234 63.29 37 3.70* 3.845E+OO l .121E+OO l.121E+00 254.25 92.59 83 4.23 6.570E+OO 1.273E+OO l.273E+00 79.53 U-234 609.32 185 45.49* 2.494E+OO 6.972E-01 6. 972E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.912E-01 41. 03 1764.49 30 15.30 1.040E+OO 8.093E-01 8.093E-01 44.16 U-235 89. 96 90 3.47 6.409E+OO 1. 723E+OO 1.723E+OO 60.75 93.35 83 5.60 6.570E+oo. 9.616E-01 9.616E-01 79.53 143.76 ------10. 96* 7.059E+OO ------Line Not Found ------163.-33 ------5.08 6.731E+00 ------Line Not Found ------185.72 226 57.20 6.293E+OO 2.677E-01 2.677E-01 31.14 205.31 ------5.01 5.902E+OO ------Line Not Found ------U-238 63.29 37 3.70* 3.845E+OO 1.121E+OO 1.121E+OO 254.25 92.59 83 4.23 6.570E+OO l.273E+00 1.273E+OO 79.53 AM-243 43.53 ------5.90 9.310E-01 ------Line Not Found ------74.66 196 67.20* 5.239E+OO 2.370E-01 2.370E-01 31. 79 ANH-511 511. 00 20 100.00* 2.868E+OO 3.004E-02 3.004E-02 184.44 Flag: "*" Key line Page 3296 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Total number of lines in spectrum 53 Number of unidentified lines 13 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlif e 1. 25E+09Y 244.06D 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y. 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+l0Y 1. 41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 2.34 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total .Activity Uncorrected pCi/GRAM l.308E+Ol 6.051E-02 l.519E+OO l.519E-01 5.215E-02 5.509E-02 3.483E-01 2.523E+OO 9.269E-01 6. 972E-01 9.156E-01 6. 972E-01 2.475E+OO 6. 972E-01 8.277E-01 8.277E-01 9.269E-01 2.491E-01 6. 972E-01 8. 372E-01 8.277E-01 l .121E+OO 6.972E-01 2.677E-01 l.121E+OO 2.370E-01 3.004E-02 3.287E+Ol 3.287E+Ol Decay Corr pCi7GRAM l.308E+Ol l.418E-Ol 2.384E+OO l.519E-01 5.314E-02 5.614E-02 3.483E-01 2.523E+OO 9.269E-01 6.975E-01 9.159E-01 6.975E-01 2.475E+OO 6.975E-01 8.277E-01 8. 277E...:.01 9.269E-01 2. 491E-01 6. 972E-01 8. 372E-01 8.277E-01 l.121E+OO 6.972E-01 2.677E-01 l.121E+OO 2.370E-01 3.004E-02 3.382E+Ol 3.382E+Ol 75.47% Decay Corr 2-Sigma Error 0.135E+Ol 1. 97 9E-01 l.734E+OO l.105E-01 4.658E-02 4.920E-02 0.766E-01 0.439E+OO l.150E-01 l.564E-01 l.594E-01 l.564E-01 l.070E+OO l.564E-01 2.599E-01 2.599E-01 l.150E-01 l.513E-01 l.564E-01 7.656E-01 2.599E-01 2.850E+OO l.564E-01 0.834E-01 2.850E+OO 0.754E-01 5. 541E-02 "M" Manually accepted 2-Sigma %Error Flags 10.29 139. 62 72.74 72. 74 87.64 87.64 21. 98 17.41 12.41 22.43 17. 41 22.43 43.23 22.43 31. 41 31. 41 12.41 60.75 *K 22.43 91. 45 31. 41 254.25 22.43 31.14 K 254.25 31. 79 184.44 Flags: "K" Keyline not found "E" = Manually edited "A" Nuclide specific abn. limit Page 3297 of 5809 Unidentified Energy Lines .Page : 4 Sample ID : G405235019 Acq1:1isition date : 3-0CT-2016 08:21:03 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err . %Eff Flags 0 83.89 64 233 1. 04 167.71 165 7 1.26E-02 98.9 6.02E+OO T 4 270.47 70 65 1. 75 541.11 537 27 1.57E-02 56.3 4.81E+OO T 4 274.41 49 54 1. 20 549.00 537 27 1. llE-02 62.2 4.75E+OO T 0 415.66 40 131 *7.63 831.66 813 24 9.52E-03 **** 3.39E+OO T 0 428.86 12 48 1. 41 858.08 851 9 2.79E-03 **** 3.30E+OO T 0 469.33 29 29 1. 81 939.06 935 9 6.91E-03 82.7 3.07E+OO T 1 491.68 18 29 1. 55 983.78 977 17 4.30E-03 **** 2. 96E+OO T 1 494.93 18 21 1. 55 990.28 977 17 4.46E-03 97.7 2.94E+OO 0 498.75 37 26 3.26 997.93 993 10 8.92E-03 65.7 2.92E+OO 0 544.28 13 25 3.54 1089.02 1081 10 3.20E-03 **** 2.73E+OO 6 668.21 31 21 1. 54 1337.00 1333 12 7.79E-:-03 55.5 2.32E+OO T 6 670.75 9 12 1. 65 1342.09 1333 12 2.38E-03 **** 2. 31E+OO 0 701.59 17 41 5.90 1403.77 1395 15 4.31E-03 **** 2.23E+OO T 0 727.59 44 19 1. 92 1455.79 1451 11 l.12E-02 53.5 2.17E+OO T 0 747.05 22 18 1. 62 1494.74 1490 10 5.55E-03 89.9 2 .13E+OO T 0 768.97 26 29 2.85 1538.59 1533 11 6.59E-03 **** 2.08E+00 0 817.97 16 15 3.22 1636.63 1631 11 4'. l3E-03 **** 1.98E+OO T 0 935.17 12 9 1. 29 1871. 08 1867 8 3.18E-03 **** 1. 7 9E+OO 1 964. 79 27 21 1. 90 1930.35 1920 25 7.29E-03 67.1 1.74E+OO T 0 1003.33 31 4 5*. 74 "2007.44 2000 15 8.36E-03 50.5 1.69E+OO T 0 1153. 38 14 22 2.48 2307.60 2301 11 3.89E-03 **** 1.51E+OO 0 1166.18 10 7 2.27 2333.20 2329 '7 2.78E-03 **** L 50E+00 0 1336.20 8 3 0.68 2673.26 2669 8 2.36E-03 "**** 1. 34E+OO 0 1377.44 18 5 2.28 2755.75 2750 10 5.00E-03 66.2 1. 30E+OO 0 1415.36 12 0 0.83 2831. 58 2827 9 3.33E-03 57.7 l.27E+00 0 1509.86 7 5 1. 79 3020.57 3014 '10 1. 94E-03 **** 1.20E+OO 0 1847.73 6 2 1.26 3696.23 3691 9 1.90E-03 **** 9.94E-01 Flags: "T" Tentatively associated Page 3298 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:21:46.64 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road . *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l *
Acquisition date 3-0CT-2016 08:21:03 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
Sample date 8-DEC-2015 14:30:00 Nuclide Library : SOLID *
Sample ID G405235019 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity: 1.7598E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 .* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.523E-01 1.034E-01 6.630E-01 4.723E-02 2.065E-02 2.181E-02 2.259E-02 3.846E-02 4.579E-02 4.312E-02 4.579E-02 4.124E-01 4.579E-02 8.671E-02 8.671E-02 3.846E-02 3.182E-01 4.577E-02 2.878E-01 8. 671E-02 7. 241E-01 4.577E-02 1.259E-Ol 7. 241E-01 3.341E-02 1.880E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3299 of 5809 Le (pCi/GRAM 8.359E+OO 2.897E-02 O.OOOE+OO 2.532E-02 2.709E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU:-106 AG-108M AG-110M SN-113 CD-115 SN-117M . TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-*139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 . PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3300 of 5809 O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF 4.422E-02 NOT IDENT. 3.057E-01 NOT IDENT. O.OOOE+OO SHORT HLIF 3.156E-02 NOT IDENT. 2.746E-01 NOT IDENT. 4.135E+OO NOT IDENT. 2.937E-02 NOT IDENT. 1.786E+00 NOT IDENT. 5.277E+OO NOT IDENT. 0.000E+OO SHORT HLIF l.337E-01 NOT IDENT. O.OOOE+OO SHORT HLIF 0.000E+OO SHORT HLIF 4.490E-01 NOT IDENT. 4.212E+00 NOT IDENT. 4.444E-01 NOT O.OOOE+OO SHORT HLIF l.595E-01 NOT IDENT. 3.815E+02 NOT IDENT. 2.199E-02 FAIL ABUN 6.989E-01 NOT IDENT. 1.860E+OO NOT IDENT. l.007E+OO NOT IDENT. O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF 2.365E-02 NOT IDENT. 3.690E-02 NOT IDENT. 4.352E+OO FAIL ABUN 3.256E-01 NOT IDENT. 3.256E-01 NOT IDENT. l.826E-02 NOT IDENT. 5.950E-02 NOT IDENT. l.417E-01 NOT IDENT. O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF 8.610E-02 NOT IDENT . 1.432E+OO NOT IDENT. 7.687E-02 FAIL ABUN l.906E+02 NOT IDENT. O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF O.OOOE+OO SHORT HLIF 0.000E+OO *SHORT HLIF 2.715E-02 FAIL ABUN 0.000E+OO SHORT HLIF 3.684E-02 NOT IDENT. 8.634E-02 NOT IDENT. 0.000E+OO SHORT HLIF O.OOOE+OO SHORT HLIF 8.694E-02 NOT IDENT. 0.000E+OO SHORT HLIF O.OOOE+OO SHORT HLIF 1.639E+Ol NOT IDENT. O.OOOE+OO SHORT HLIF 2.375E-01 NOT IDENT. 3.795E-02 NOT IDENT . 3.318E+00 NOT IDENT. 2.676E-02 FAIL ABUN O.OOOE+OO SHORT HLIF 5.753E+02 NOT IDENT. O.OOOE+OO SHORT HLIF l.701E-02 FAIL ABUN 6.831E-02 FAIL ABUN l.203E-01 NOT IDENT. 7.033E-02 FAIL ABUN 7.370E-02 FAIL ABUN 1.035E+00 FAIL ABUN 3.977E-02 FAIL ABUN 1.243E+Ol NOT IDENT. l.563E-01 FAIL ABUN 6.088E-02 FAIL ABUN 1.428.E-02 FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3301of5809 2.632E+OO 6.638E-01 1. 796E+OO 2.207E+Ol 7.154E+Ol 3.167E-01 1.666E+OO 3.476E-02 1. 776E+OO 3.090E-01 4.184E-01 5 .172E-01 2.542E-01 4. llOE-01 1.430E-01 1.430E-01 4. llOE-01 3.398E-02 1.807E-01 3.064E+OO 3.398E-02 O.OOOE+OO 1. 54 7E-01 2.147E+02 8.212E-02 6.302E-02 4.760E-02 2.232E-02 2.374E-02 8.039E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:21:51.99 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l *
Acquisition date 3-0CT-2016 08:21:03 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
Sample date 8-DEC-2015 14:30:00 Nuclide Library : SOLID *
Sample ID G405235019 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM *
Quantity Err(%) : l.1365E-03. % *
Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * * *
Eff. Cal. date 2-AUG-2016 .10:31:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF .GAMll CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (L 96-sigma) K-40 1.308E+Ol 1.485E+00 ZN-65 l.418E-01 1.940E-01 CD-109 7.215E-01 1. 743E+OO SN-126 4.599E-02 l. lllE-01 BA-137M 5.314E-02 4.570E-02 CS-137 5.614E-02 4.828E-02 TL-208 3.483E-01 7.648E-02 PB-212 9.269E-01 1.230E-01 BI-214 6.975E-01 l.562E-01 PB-214 9.159E-01 1.608E-01 RN-222 6.975E-01 1. 562E-01 RA-224 4.419E-01 1.128E+OO RA-22 6 6*. 97 5E-01 1.562E-01 AC-228 8.277E-01 2.582E-01 RA-228 8.277E-01 2.582E-01 TH-228 9.269E-01 l.230E-01 TH-229 -8.168E-02 3.649E-01 TH-230 6. 972E-01 1.561E-01 PA-231 8. 372E-01 7.713E-01 TH-232 8.277E-01 2.582E-01 TH-234 1.121E+OO 2.804E+00 U-234 6.972E-01 l.561E-01 U-235 -2.306E-02 1.394E-01 U-238 1.121E+OO 2.804E+OO AM-243 1. 37 8E-01 7.780E-02 ANH-511 3.004E-02 5.432E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3302 of 5809 Key-Line Activity (pCi/GRAM -2.030E+00 -4.410E-03 l.OOOE+41 1. 871E-02 K.L Act error ( 1. 96-sigma) 9.521E+OO 3.432E-02 6.019E+41 2.465E-02 TPU ( 1. 96-sigma) 1.485E+OO l.940E-01 1. 743E+OO l. lllE-01 4.570E-02 4.828E-02 7.648E-02 l.230E-01 l.562E-01 l.608E-01 1. 562E-01 l.128E+OO l.562E-01 2.582E-01 2.582E-01 l.230E-01 3.649E-01 1.561E-01 7.713E-01 2.582E-01 2.804E+OO 1. 561E-01 l.394E-01 2.804E+OO 7.780E-02 5.432E-02 TPU ( 1. 96-sigma) 9.565E+OO 3.437E-02 0.000E+OO 2.605E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 3.402E-01 2.521E-01 2.951E-01 FAIL ABUN V-48 3.854E+03 9.985E+03 1.014E+04 SHORT HLIF CR-51 1. 703E+02 3 .118E+02 3. 211E+02 SHORT HLIF MN-54 -5.091E-03 5. 301E-02 5.306E-02 NOT IDENT. C0-56 -1.179E-01 3.830E-01 3.866E-01 NOT IDENT. MN-56 -1.000E+41 3.138E+41 O.OOOE+OO SHORT HLIF C0-57 4.973E-03 3.363E-02 3.370E-02 NOT IDENT. C0-58 -2. 941E-01 3.923E-01 4.141E-01 NOT IDENT. FE-59 -1.537E+OO 4.971E+OO 5.019E+OO NOT IDENT. C0-60 -1.192E-02 4.097E-02 4.132E-02 NOT IDENT. GE-68 l.051E+OO 1.853E+OO 1.912E+OO NOT IDENT. AS-73 -6.730E-01 5.408E+OO 5.417E+OO NOT IDENT. AS-74 -1.108E+03 4.442E+03 4.470E+03 SHORT HLIF SE-75 -2.080E-02 1.573E-01 1. 576E-01 NOT IDENT. BR-77 1.627E+38 l.407E+39 O.OOOE+OO SHORT HLIF SR-82 -6. 725E+02 5.246E+02 6.059E+02 SHORT HLIF RB-83 8.125E-03 5.009E-01 5.009E-01 NOT IDENT. KR-85 -1.717E+OO 5.561E+OO 5.614E+OO NOT IDENT. SR-85 -1.822E-01 5.869E-01 5.926E-01 NOT IDENT. RB-86 3. 761E+03 2.391E+04 2.397E+04 SHORT HLIF* Y-88 1. 539E-01 l.340E-01 1.509E-01 NOT IDENT. *Y-91 1. 451E+02 4.130E+02 4; 182E+02 NOT IDEN'.['. NB-94 3.236E-02 5.695E-02 5.879E-02 FAIL ABUN NB-95 4.936E-01 8. 231E-01 8.526E-01 NOT IDENT. NB-95M 2.028E+00 2. 091E+OO 2.282E+OO NOT IDENT. ZR-95 2.861E-01 l.125E+OO 1.132E+OO NOT IDENT. NB-97 -l.000E+41 l.586E+41 0.000E+OO SHORT HLIF ZR-97 -l.OOOE+41 3. 098E+42. O.OOOE+OO SHORT HLIF M0-99 -1.909E+31 l.205E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.402E+41 0.000E+OO SHORT HLIF RH-101 -6.699E-03 2.615E-02 2.633E-02 NOT IDENT. RH-102 -1. 461E-.02 4.453E-02 4.501E-02 NOT IDENT. RU-103 8. 096E+OO 4.292E+OO 5.634E+OO FAIL ABUN RH-106 -2.769E-01 4 .131E-01 4.316E-01 NOT IDENT. RU-106 -2.769E-01 4.131E-01 4.316E-01 NOT IDENT. AG-108M 6.667E-03 1.918E-02 1.942E-02 NOT IDENT. AG-llOM -4.382E-03 7.159E-02 7.162E-02 NOT IDENT. SN-113 -5.393E-02 l.605E-01 l.623E-01 NOT IDENT. CD-115 -1.407E+39 2.423E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -4.171E+03 6. 911E+04 6.913E+04 SHORT HLIF TE-123M -l.664E-02 9.651E-02 9.680E-02 NOT IDENT. SB-124 1.150E+OO 1.312E+OO 1.411E+OO NOT IDENT. SB-125 6.234E-02 1.477E-01 1.503E-01 FAIL ABUN TE-125M 8.779E+Ol 1.970E+02 2.010E+02 NOT IDENT. I-126 4.452E+05 7.485E+05 7.750E+05 SHORT HLIF SB-126 2.165E+05 8.020E+05 8.079E+05 SHORT HLIF . SB-127 -2.355E+21 l.481E+22 O.OOOE+OO SHORT HLIF I-131 1. 211E+08 3.541E+09 3.542E+09 SHORT HLIF I-132 l.000E+41 1.848E+42 O.OOOE+OO SHORT HLIF TE-132 -2.159E+26 3.168E+26 O.OOOE+OO SHORT HLIF BA-133 2.751E-03 3.202E-02 3.205E-02 FAIL ABUN I-133 -l.OOOE+41 7.873E+41 O.OOOE+OO SHORT HLIF CS-134 -1.254E-02 4. 511E-02 4.546E-02 NOT IDENT. CS-135 -l.282E-02 l.107E-01 1.109E-01 NOT IDENT. I-135 -l.000E+41 7.019E+41 O.OOOE+OO SHORT HLIF CS-136 3.372E+04 2.140E+05 2.145E+05 SHORT HLIF CE-139 9.921E-02 9.055E-02 1.0lOE-01 NOT IDENT. BA-140 -3.105E+05 l.032E+06 1.042E+06 SHORT HLIF LA-140 7.780E+04 2.578E+05 2. 601E+05 SHORT HLIF CE-141 -1.223E+OO 1.804E+Ol 1.805E+Ol NOT IDENT. CE-143 l.000E+41 9.440E+40 0.000E+OO SHORT HLIF CE-144 5.676E-02 2.533E-01 2.546E-01 NOT IDENT. PM-144 1. 962E-02 4.485E-02 4.571E-02 NQT IDENT. PR-144 l.786E+OO 3.907E+OO 3.989E+OO NOT IDENT. PM-146 4.898E-04 2.943E-02 2.943E-02 FAIL ABUN ND-H7 4.458E+06 2. 339'E+07 2.348E+07 SHORT HLIF PM-147 2. 411E+02 6.009E+02 6.107E+02 NOT IDENT. PM-149 -4.995E+39 3.550E+40 O.OOOE+OO SHORT HLIF EU-150 -5.887E-03 2.094E-02 2. lllE-02 FAIL ABUN EU-152 6.035E-03 7. 271E-02 7.276E-02 FAIL ABUN GD-153 8.733E-03 1.268E-01 1. 269E-01 NOT IDENT. EU-154 -l.268E-02 8.373E-02 8.393E-02 FAIL ABUN EU-155 2.673E-02 7.652E-02 7.746E-02 FAIL ABUN TB-160 -1.163E+OO 1.477E+OO 1.567E+OO FAIL ABUN H0-166M -1.428E-02 4.820E-02 4.863E-02 FAIL ABUN TM-171 -1.285E+OO l.269E+Ol 1. 271E+Ol NOT IDENT. HF-172 -8.547E-02 1.765E-01 1.806E-01 FAIL ABUN LU-172 2.802E-02 6.480E-02 6.602E-02 FAIL ABUN Page 3303 of 5809 LU-176 -1.290E-02 1. 8 60E-02 l.949E-02 FAIL ABUN HF-181 -1. 802E+OO 3 .172E+OO 3.274E+OO NOT IDENT. TA-182 4.024E-01 6.949E-01 7 .181E-01 FAIL ABUN RE-183 6.868E-01 1.787E+OO l.814E+00 NOT IDENT. RE-184 7.369E+OO 2.49SE+Ol 2.520E+Ol NOT IDENT. W-188 -8.317E-01 9.107E+Ol 9.107E+Ol FAIL ABUN IR-192 l.873E-01 3.483E-01 3.584E-01 FAIL ABUN HG-203 7. 031E-01 1.858E+OO l.885E+OO NOT IDENT. BI-207 l.043E-02 3.757E-02 3.786E-02 FAIL ABUN PB-210 1.166E+OO 1. 711E+OO 1.790E+OO NOT IDENT. BI-211 2.523E+OO 4. 4*49E-01 1.221E+OO FAIL ABUN PB-211 -l .196E"-01 5.261E-01 5.289E-01 NOT IDENT. BI-212 l.286E+OO 6.773E-01 8.9l5E-01 FAIL ABUN RN-219 5.979E-02 2.699E-01 2.713E-01 FAIL ABUN RA-223 -3. 781E-02 4.420E-01 4.423E-01 FAIL ABUN AC-227 -6.068E-02 1.724E-01 1. 746E-01 FAIL ABUN TH-227 -6.068E-02 1. 724E-01 1. 746E-01 FAIL ABUN TH-231 -3. 781E-02 4.420E-01 4.423E-01 FAIL ABUN PA-233 -5.017E-02 4.717E-02 5.231E-02 FAIL ABUN PA-234 2. 962E-02 2.129E-01 2.133E-01 NOT IDENT. PA-234M 3.362E+OO 3 .115E+OO 3.464E+OO NOT IDENT. NP-237 -5.017E-02 4.717E-02 5.231E-02 FAIL ABUN NP-238 6.669E+40 3.130E+41 O.OOOE+OO SHORT HLIF NP-239 2.354E-02 1.642E-01 1.646E-01 FAIL ABUN PU-239 -2. 53.9E+Ol 2.347E+02 2.350E+02 NOT IDENT. AM-241 9.666E-03 8.947E-02 8.958E-02 NOT IDENT. CM-243 -3.383E-03 6.738E-02 6.740E-02 FAIL ABUN BK-247 -1. 496E-02 5.697E-02 5.736E-02 FAIL ABUN CM-247 -4.980E-03 2. 491E-02 2.501E-02 FAIL ABUN CF-249 -6.187E-03 2.649E-02 2.663E-02 NOT IDENT. CF-251 4.211E-02 8.588E-02 8.795E-02 NOT IDENT. Page 3304 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 54.6419 87.09 97.7634 136.47 66.6544 45.60 66.8561 87.57 97.8610 140.51 0.0000 46.54 53.4742 88.03 79.1166 143.76 74.6378 49.72 0.0000 88.34 79.1666 144.24 67.4290 51. 35 77.5164 88.47 79.1877 145.44 74.8213 51. 87 91.4366 89. 96 96. 4491 152.43 77.6697 52.39 80.3444 1093.63 49.2376 153.25 0.0000 52.97 76.1527 91.11 0.0000 323.87 66.2886 53.44 82.3216 92.59 92.5236 156.02 0.0000 54.07 72.9207 93.35 87.5850 158.56 0.0000 57.36 0.0000 94.56 68.7085 159.00 66. 7270 57.53 . 78.0111 94.65 68.7206 162.33 64.9000 57.98 69.3302 94.67 68.7233 162.66 0.0000 59.27 77.4982 94.87 70.0234 163.33 91.6204 59.32 77.5086 97.43 79.6476 165.86 61.9985 59 .*54 75.2041 98.43 59.6093 176.31 62.8410 60. 96. 83.7444 98.44 59.6108 176.60 0.0000 61.17 83.7907 99.53 84.7841 177.52 57. 5110 62.93 86.2496 100 .11 89.6992 181.07 0. 0000 . 63.29 86.3296 102.03 60.9827 181.52 45.0759 63.58 86.3936 103.18 74.6930 184.41 49.2490 64.28 86.5481 103.37 67.9268 143.76 49.3279 66.73 95.7601 105.21 66.2086 193.51 68.6006 67.24 70.7119 105.31 69.1420 197.03 67 ."7733 125.81 80.3872 106.12 70.2191 198.01 78.9736 67.75 97.2010 106.47 74.1671 201.83 67.0322 69.67 94.9440 109.28 68.6558 203.43 90.6590 70.83 103.3682 111. 00 76.7348 205.31 56.8299 72.81 114.1762 111. 76 0.0000 210.85 48.5305 72.87 114.1924 114. 06 70.2205 215.65 61. 2683 74.66 110. 7022 116. 30 0.0000 222 .11 57.1266 74.82 110.7428 116.74 61.6003 227.09 57.4287 74.97 110.7816 119.76 77.8911 227.38 58.5952 77 .11 111.3207 121.12 66.0564 228.16 0.0000 78.74 111. 72 69 121.22 66.0670 228.18 64.3937 79.69 85.1277 121. 78 65.1260 116.74 64.3937 80.12 75.3291 122.06 65.1562 235.69 55.6245 80.19 0.0000 122.92 91.3471 235. 96 63.3677 80.57 85.2926 123.07 91.3694 238.63 68. 5771 81. 00 74.2371 265.00 69.3490 238.98 0.0000 81. 07 74.2480 125.81 85.7244 240.99 68.7400 81. 75 91. 7081 127.23 85.9189 242.00 68.8093 83.79 82.1522 127.91 67.7979 244.70 45.2175 84.00 82.1885 129.30 82.1445 252.40 0.0000 85.43 95.5518 131.20 87.4763 252.80 54.2221 86.55 95.7760 133. 02 65.2832 254.15 0.0000 86.79 97.7023 133.52 64.3122 256.23 47.3059 86.94 97.7333 136.00 84.0270 260.90 0.0000 Page 3305 of 5809 .

ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 42.9170 355.39 0.0000 584.27 22.6846 264. 80 42.9225 356.01 32.1663 595.83 0.0000 265.00 47.7014 364.49 0.0000 427.87 24. 8596 268.22 41.4650 366.42 0.0000 602.52 0.0000 269.46 37.1219 372.51 28.6521 604. 72 26.9033 270.03 37.1417 375.05 26.9648 607.14 20.9504 271.23 37.1824 377.52 27.0127 609.32 24.9674 273.65 0.0000 356.01 32.3863 610.33 24.9797 276.40 37.3584 388.16 31.6069 614.28 27.0308 277.37 37.3915 388.63 0.0000 618.01 21.0615 277.60 37.3990 391.69 30.8044 620. 36 22.0904 278.00 37.4132 264.66 25.6818 621. 93 28.1356 279.20 37.4530 401.81 27.4750 630.19 0. 000.0 279.54 37.4653 402.40 31.0323 631.29 21.1974 279.70 37.4700 404.85 30.6402 633.25 15.1550 280.46 40.3178 410.95 26.7535 634.78 0.0000 283.69 37.2000 413. 71 26.8030 635.95 13.1513 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 36.4471 423. 72 0.0000 645.85 18.2944. 285.90 0.0000 427.09 26.1385 657.76 19.9293 287.50 38.9482 427.87 26.1520 657.90 0.0000 290.67 39.0566 433.94 21.7280 661. 66 16.8934 293.27 0.0000 439.40 21.8037 664.57 0.0000 351. 93 40.4363 453.88 22.0029 666.33 0.0000 295. 96 40.4625 463.37 28.5870 666.50 0.0000 879.38 40.5541 468.07 24. 9697 667. 71 0.0000 299.98 40.6024 473.00 0. 00.00 677.62 15.4700 300.09 40.6055 475.06 25.0752 685.70 0.0000 300.13 40.6075 476.78 28.8,197 695.00 0.0000 301.36 40.6498 477.60 28 .. 8336 696.49 15.6006 302 .*85 40.7011 482.18 27.9797 696. 51 15.6012 256.23 26.3490 487.02 0.0000 697.00 0.0000 304.85 0.0000 . 492. 35 0.0000 697.30 14.0460 306.78 42.0735 497.08 5.6449 697.49 14.0471 308.46 33.4583 505.52 23.6343 702. 65 22.9435 311. 90 47.2252 507.63 0.0000 706.68 29.7745 316.51 29.9392 511. 00 26.5528 711. 68 25.1279 319.41 0.0000 514.00 27. 0724 720.70 0.0000 320.08 . 0.0000 514.00 27.0724 721. 93 0.0000 321.04 35.8937 520.40 23.8332 722.78 22.0920 32'3.87 42.6681 520.69 0.0000 722.91 20.5156 325.23 55.2780 522.65 0.0000 723. '31 14.2053 328.76 0.0000 527.90 0.0000 724.19 12.6318 333.37 45.5208 528.26 19.1496 727. 33 12.6489 333.97 43.0126 529.59 19.1642 733.00 17.4339 334.37 50.6189 529.87 0.0000 735.93 7.4053 338.28 37.2342 531. 02 0.0000 333.97 13.7617 338.32 37.2351 537.26 0.0000 739.50 0.0000 311. 90 47.0461 546.56 0.0000 747.24 20.1960 340.48 47.0461 552.55 31.0443 748.06 19 .1396 340.55 0.0000 563.25 22.4394 752.31 14.0604 344.28 40.8076 569.33 20.5531 753.82 0.0000 345.93 39.8379 946.00 21.5345 756.73 16.0071 351.06 31.6192 569.70 20.5574 7.5 6. 8 0 16.0077 351. 93 31. 6403 583.19 22. 6715 884.68 27.2930 Page 3306 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.8870 1274.44 2.7970 1*620.50 6.1919 766.42 20.8925 1001.03 7.0034 1621. 92 5.1617 766.84 20.8957 1002.74 13.1387 1678.03 0.0000 772. 60 0.0000 1004.73 13.1470 1690.97 1.0477 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49. 1.0638 778.90 10.7682 1028.54 0.0000 1063.66 3.4082 783.70 0.0000 1037.84 7.0869 1771.35 3.6525 785.37 22.6722 1038.76 0.0000 1791.20 0.0000 792.07 23.8154 631.29 17. 7 673 1808.65 2.1466 794.95 19.5081 1048.07 0.0000 1810.72 0.0000 795.86 26.0195 1049.04 13.3356 1836.06 0.0000 810.06 13.0825 1050.41 11.5623 810.29 14.1743 1063.66 13.3969 344.28 14.1748 1077.00 0.0000 810.76 15.2675 1077.34 11. 6599 815.77 0.0000 1085.87 11. 6908 1048.07 0.0000 1093.63 14.4229 832.01 10.9949 1099.45 14.4482 834.85 19.8127 1112. 07 11. 6031 835. 71 14.3140 1112. 84 14.5068 836.80 0.0000 1115. 54 11. 6148 846.75 0.0000 1120.29 11. 6313 846.77 18.7964 1120. 55 11. 6320 856.80 0.0000 1221. 41 14.5439 860.56 16. 6711 1129. 67 20.9589 871.09 20.0830 1131. 51 0.0000 873.19 15.6321 1147. 95 0.0000 875.33 0.0000 1173.23 10.1520 879.38 19.0254 1177.95 11.0896 880.51 12.3155 1189.05 16.6882 883.24 11. 2069 1204.77 13.0370 884.68 12.3343 1221.41 11. 22 66 889.28 4.4927 1231.02 16.8849 894.76 9.0029 1235.36 0.0000 898.04 13.5205 1238.28 11. 2793 900. 72 12.4059 1260.41 0.0000 903.28 14.6747 1271.87 16.1253 911.20 15.8480 1274.44 11. 3906 912.08 15.8531 1274.54 11. 3906 923.98 0.0000 1291.59 8.5820 926.50 14.7959 1298.22 0.0000 929 .11 14.8091 1312 .11 0.0000 937.49 10.2825 1332.49 13.8788 944.13 0.0000 1362.66 0.0000 946.00 12.6042 1365.19 6.8035 949.00 14. 9112 1368. 63 0.0000 667. 71 0.0000 1384.29 4.8828 962.31 12.6749 1408.01 9.8236 964.08 12.6825 1457.56 0.0000 966.17 12.6914 1460.82 3.9802 911. 20 12.7031 1489.16 6.0103 968.97 12.7031 1505.03 8.0435 983.53 0.0000 1584.12 9. 2137 984.45 o.oobo 1596.21 0.0000 Page 3307 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:53:52.33 ********************************************************************************

GEL Laboratories LLC * * . 2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM01.CNF;402 Background date : Z-OCT-2016 10:59:55. Sample date 8-DEC-2015 13:50:00. Acquisition date : 3-0CT-2016 08:53:24. Sample ID G405235020 Sample quantity 1.70763E+02 GRAM Detector name : GAMOl Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.37 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 5 2 5 3 5 4 2 5 2 6 0 7 0 8 0 9 0 10 0 11 3 12 3 13 0 14 0 15 0 16. 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26. 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 35. 35* . 40.33* 45.15* 74.90 77.16* 87.73 92.89* 185.65* 209.98 216.83 238.63* 241. 71* 295.30* 338.55* 351.87* 388.82 463.85 511.04*

566.51* 583.08* 609.50* 636.61 727.70 737.71 768.80 785.79 860.90 904.69* 911.34* 964.44 969.20 1063.09 1119.89* 1143. 54 Page 3308 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 36 29 19 101 150 46 42 85 95 24 344 94 85 53 .224 14 40 46 31 110 118 7 51 25 18 11 31 11 57 28 41 6 39 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 10 55 62 157 151 213 141 176 138 42 59 77 61 55 45 82 66 55 53 35 33 20 20 10 25 13 15 13 22 16 12 5 8 11 1. 84 1. 85 1.16 1. 45 1. 28 0.97 1.12 1. 41 5.43 1. 25 1.15 1. 80 0.84 0.86 1. 27 2.33 4.43 1. 72 0;87 1. 53 1. 75 1. 40 3.47 3.50 0.62 1. 51 1. 86 4.40 1.13 1. 32 1. 61 1. 46 1. 43 0.53 71. 39 81. 37 91. 00 150.50 155.01 176.15 186.47 371. 96 420.62 434.33 477.92 484.09 591. 25. 677.74 704.36 778.26 928.29 1022.65 1133.56 1166.70 1219.53 1273.74 1455.87 1475.89 1538.04 1572. 02 1722.19 1809.75 1823.05 1929.20 1938. 71 2126.44 2239.99 2287.27 67 67 67 143 143 170 183 366 413 431 471 471 587 673 699 766 920 1013 1127 1159 1215 1266 1446 1468 1531 1568 1715 1802 1817 1922 1934 2123 2234 2282 32 32 32 17 17 9 8 14 18 6 21 21 9 10 12 17 *20 20 16 17 11 11 16 14 12 8 15 13 11 13 10 6 11 7 1.0lE-02 40.9 3.54E+OO 8.00E-03 63.5 5.17E-03 72.2 2.81E-02 26.0 1.02E+OO 4.16E-02 17.0 1. 27E-02 59. 7 1.16E-02 56.2 2.37E-02 35.8 2.65E-02 30.8 6.67E-03 47.3 9.55E-02 6.7 1.09E+OO 2.61E-02 24.6 2.37E-02 20.1 l.48E-02 30.5 6.22E-02 9.1 3.93E-03148.2 1. llE-02 52 .1 1.27E-02 46.8 8.51E-03 56.9 3.06E-02 15.7 3.29E-02 13.2. 2.07E-03120.1 1. 41E-02 24. 3 6.82E-03 34.5 4.86E-03 63.4 3.16E-03 63.4 8.61E-03 32.6 3.18E-03 72.3 1. 59E-02 21. 2 7.83E-03 34.9 1.13E-02 22.5 1.77E-03 66.2 1. 08E-02 21. 7 2.08E-03 80.4 Peak Search Report (continued) Page : 2 Sample ID : G40523502'0 Acquisition date 08:53:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw

Cts/Sec %Err Fit 35 0 1155.31 10 10 1. 46 2310.80 2305 10 2.78E-03 67,1 36 0 1173.52 5 4 0.52 2347.20 2346 4 l.45E-03 74.2 37 0 1234.37 8 20 3.32 2468.87 2459 13 2.08E-03126.8 38 0 1254.20 10 0 1. 66 2508.50 2505 7 2.78E-03 31. 6 39 0 1285.78 11 0 1. 28 2571.64 2568 7 3.06E-03 30.2 40 0 1460.69* 257 9 2.06 2921. 30 2915 12 7.15E-02 6.7 41 0 1493.39 12 0 1. 65 2986.67 2982 9 3.33E-03 28.9 42 0 1591.81 10 0 1. 41 3183.40 3179 8 2.78E-03 31. 6 43 0 1729.55 11 0 1. 72 3458.73 3455 7 3.06E-03 30.2 44 0 1764.44* 21 3 1. 00 3528.46 3522 13 5.94E-03 29.1 Flag: "*" == Peak area was modified by backgrou.nd subtraction Page 3309 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:53:54 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 13:50:00 G405235020 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:53:24 170.76 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAl 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3310of5809 PB-214 PB-214. PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-'126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.37 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 9.709E-01 1.069E+Ol l.069E+Ol 13. 46 OK CD-109 88.03 3.70* 4.617E+OO 1.021E+OO l.602E+OO 191.53 OK SN-126 64.28 9.60 2.409E+00 Line Not Found Absent 86.94 8.90 4.617E+00 4.245E-01 4.245E-01 191.53 OK 87.57 37.00* 4.617E+OO 1. 021E-01 1.021E-01 191.53 OK TL-208 277.37 6.60 3.944E+OO Line Not Found Absent 583.19 85.00* 2.090E+OO 3.015E-01 3.015E-01 31. 39 OK 860.56 12.50 1.519E+OO 7.551E-01 7. 551E-01 65.24 OK PB-210 46.54 4.25* 4.948E-01 5.729E+OO 5.877E+OO 144.32 OK BI-211 72.87 1. 23 3.328E+OO Line Not Found Absent 351. 06 12.92* 3.217E+OO 9.887E-01 9.887E-01 89.78 OK BI-212 727.33 6.67* 1. 742E+OO 2.061E+OO 2.061E+OO 48.56 OK 785.37 1.10 1.636E+OO 2.959E+OO 2.959E+OO 126.79 OK 1620.50 1. 47 8.816E-01 Line Not Found Absent PB-212 74.82 10.28 3.530E+OO l.345E+00 l.345E+OO 67.22 OK 77 .11 17.10 3.747E+OO 1.433E+OO 1.433E+OO 34.06 OK 238.63 43.60* 4.455E+00 9.612E-01 9.612E-01 13.33 OK 300.09 3.30 3.690E+OO Line Not Found Absent BI-214 609.32 45.49* 2.015E+OO 6.255E-01 6.257E-01 '26. 31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 OK 1764.49 15.30 8 .116E,Ol 7.200E-01 7.202E-01 58 .11 OK PB-214 74.82 5.80 3.522E+OO Line Not Found <<INT Reject 77 .11 9.70 3.747E+OO 2.527E+OO 2.5288+00 34.06 OK-87.09 3.41 4. 572E+OO Line Not Found <<INT Reject 242.00 7.25 4.406E+OO Line Not Found <<INT Reject 295.22 18.42 3.741E+OO 6.557E-01 6.560E-01 40.21 OK 351.93 35.60* 3.216E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.015E+00 6.255E-01 6.257E-01 26.31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.202E-01 581. ll OK RA-224 240.99 4.10* 4.410E+OO 1.655E+OO 1.655E+OO 88.30 OK RA-226 609.32 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 OK 1120.29 14.92 l.223E+OO 9.517E-01 9.521E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 OK AC-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 OK 794.95 4.25 1.621E+OO Line Not Found Absent 835. 71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 7.028E-01 7.0-28E-01 42.33 OK 968. 97 15.80 1. 37 9E+OO 8.506E-01 8.506E-01 45.09 OK RA-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 OK 794.95 4.25 1. 621E+OO Line Not Found Absent 835.71 1. 61 1.557E+OO Line Not Found Absent 911. 20 25.80* l.450E+OO 7.028E-01 7.028E-01 42.33 OK 968.97 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 OK TH-228 74.82 10.28 3.530E+OO 1.345E+OO 1.345E+OO 67.22 OK 77 .11 17.10 3.747E+OO l.433E+OO l.433E+OO 34.06 OK 238.63 43.60* 4.455E+OO 9.612E-01 9.612E-01 13.33 OK Page 3311 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235020 / Acquisition date 3-0CT-2016 08:53:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3.690E+OO Line Not Found Absent TH-230 609.32 45.49* 2.015E+OO 6.255E-01 6.255E-01 26.31 OK 1120.29 14.92 l.223E+OO 9.517E-01 9.517E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.200E-01 58 .11 OK TH-232 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04. OK 835. 71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* l.450E+OO 7.028E-01 7.028E-01 42.33 OK 968. 97 15.80 1. 379E+00 8.506E-01 8.506E-01 45.09 OK U-234 609.32 45.49* 2.015E+OO 6.255E-01 6.255E-01 26. 31 OK 1120. 29 14.92 1.22'.3E+OO 9.517E-01 9.517E-01 43.42 OK 1764.49 15.30 8.116E-01 7.200E-01 7.200E-01 58 .11 OK AM-243 43.53 5.90 3.822E-01 Line Not Found Absent 74.66 67.20* 3.530E+OO 2.057E-01 2.057E-01 67.22 OK CF-249 252.80 2.50 4.256E+OO Line Not Found Absent 333.37 14.60 3. 371E+OO Line Not Found* Absent 388.16 66.00* 2.950E+OO 3. 721E-02 3.727E-02 296.41 OK ANH-511 511. 00 100.00* 2.334E+OO 9.690E-02 9.690E-02 93.64 OK Flag: "*" = Keyline Page 3312of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:53:55.25 *******************************************************************************

GEL' Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: *
Acquisition date 3-0CT-2016 08:53:24 Sensitivity : 3.000 *
Detector ID GAMOl Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *.Elapsed real time: 0 01:00:00.37 Half life ratio : ***** *
Sample date 8-DEC-2015 13:50:00 Analyst initials: MXRl *
Sample ID G40.5235020 Sample Quantity 1. 7076E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION * *
Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.069E+Ol 1. 409E+o'o CD-109 1.602E+OO 3.007E+OO SN-126 1.021E-01 1.917E-01 3.015E-01 9.276E-02 PB-210 5.877E+OO 8.313E+OO BI-211 9.887E-01 8.698E-01 BI-212 2.061E+OO 9.807E-01 PB-212 9.612E-01 1.255E-01 BI-214 6.257E-01 1. 613E-01 PB-214 1.015E+OO 1.814E-01 RN-222 6 .. 257E-01 1.613E-01 RA-224 1.655E+OO l.432E+OO RA-226 6.257E-01 1.613E-01 AC-228 7.028E-01 2.916E-01 RA-228 7.028E-01 2.916E-01 TH-228 9.612E-01 1.255E-01 TH-230 6.255E-01 l.613E-01 TH-232 7. 028E-01* 2.916E-01 U-234 6.255E-01 1. 613E-01 AM-243 2.057E-01 l.355E-01 CF-249 3.727E-02 1.083E-01 ANH-511 9.690E-02 8.892E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 3313of5809 Key-Line Activity (pCi/GRAM -4.924E+OO 2.738E-02 O.OOOE+OO l.405E-02 4.814E-02 O.OOOE+OO O.OOOE+OO 2. 968E-02 K.L. Cnt Uncert ( 1 . 96-s i gr'na ) l.067E+Ol 4.452E-02 l.960E+41 1.733E-02 3.610E-01 1.335E+04 3.813E+02 5.948E-02 MDA (pCi/GRAM 5.458E-01 2.651E+OO l.565E-01 5.255E-02 5.825E+OO 3.512E-01 7.016E-01 8.471E-02 1.341E-01 3.053E-01 1.341E-01 9.080E-01 l.341E-01 2.577E-01 2.577E-01 8. 471E-02 l.341E-01 2.577E-01 l.341E-01 9.483E-02 6.516E-02 4.329E-02 MDA (pCi/GRAM l.994E+Ol l.007E-01 O.OOOE+OO 5.652E-02 7.244E-01 O.OOOE+OO O.OOOE+OO l.255E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.764E-Ol 4.299E-01 9.045E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO Sl:!ORT HLIF C0-57 -3.997E-02 4.279E-02 8.228E-02 NOT IDENT. C0-58 -2.614E-01 5.486E-01 9.853E-01 NOT IDENT. FE-59 -2.573E+OO 6.343E+OO l.130E+Ol NOT IDENT. C0-60 -2.207E-02 2.975E-02 5.307E-02 FAIL ABUN ZN-65 -2.641E-02 1.685E-01 2.802E-01 NOT IDENT. GE-68 -6.242E-01 2 .138E+OO 3. 931E+OO NOT IDENT. AS-73 2.796E+OO l.080E+Ol 2.143E+Ol NOT IDENT. AS-74 0.000E+OO 5.875E+03 0.000E+OO SHORT HLIF SE-75 5.865E-02 1. 871E-01 3.847E-01 NOT IDENT. BR-77 0.000E+OO 2.235E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.128E+02 O.OOOE+OO SHORT HLIF RB-83 -5.550E-04 5.099E-01 1. 031E+OO NOT IDENT. KR-85 . 2 .*082E+OO 5.606E+OO 1.174E+Ol NOT IDENT. SR-85 2.176E-01 5.918E-01 1.239E+OO NOT IDENT. RB-86 O.OOOE+OO 2.610E+04 O.OOOE+OO SHORT HLIF Y-88 -4. 372E-02 2.273E-01 4.699E-01 NOT IDENT. Y-91 1.208E+02 4.561E+02 9.861E+02 NOT IDENT. NB-94 l.537E-02 3.167E-02 6.535E-02 NOT IDENT. NB-95 4.826E-01 9.693E-01 1.815E+OO NOT IDENT. NB-95M -l.840E-01 2.374E+OO 4.219E+OO NOT IDENT. ZR-95 -2.812E-01 l.414E+OO 2.659E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 531E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 851E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 7.438E-04 3. 293E-02' 6.716E-02 NOT IDENT. RH-102 -l.297E-02 4.933E-02 8.361E-02 NOT IDENT: RU-103 -4.617E+OO 5.126E+OO 8.870E+OO FAIL ABUN RH-106 -4.426E-01 4.392E-01 7.218E-01 NOT IDENT. RU-106 -4.426E-01 4.392E-01 7.218E-01 NOT IDENT. AG-108M 7.609E-05 2.467E-02 4.916E-02 NOT IDENT. AG-110M 4.315E-02 8.373E-02 1.836E-01 NOT IDENT. SN-113 2.244E-01 4.133E-01 NOT IDENT. CD-115 O.OOOE+OO 2.477E+39 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO 8.817E+04 0.000E+OO SHORT HLIF TE-123M 7.173E-02 1.193E-01 2.513E-01 NOT IDENT. SB-124 1.758E+OO 2.005E+OO 5.217E+OO NOT IDENT. SB-125 l.072E-02 8.474E-02 1. 730E-01 FAIL ABUN TE-125M 9.450E+Ol 2. 968E+02 5.647E+02 NOT IDENT. I-126 O.OOOE+OO 7.657E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.341E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.012E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.540E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO 3.687E+26 O.OOOE+OO SHORT HLIF BA-133 -4.435E-03 4.221E-02 7.404E-02 NOT IDENT. I-133 O.OOOE+OO l.823E+41 O.OOOE+OO SHORT HLIF CS-134 3. 2.44E-02 4.509E-02 9.842E-02 NOT IDENT. CS-135 -7.638E-02 l.329E-01 2.513E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.541E+05 O.OOOE+OO SHORT HLIF BA-137M 3. 7 51E-02 3.609E-02 7. 8.69E-02 NOT IDENT. CS-137 3. 962E-02 3.813E-02 8.313E-02 NOT IDENT. CE-139 -3.178E-02 9.683E-02 1. 917E-01 NOT IDENT. BA-140 O.OOOE+OO l.208E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.755E+05 0.000E+OO SHORT HLIF CE-141 3 .115E-01 2.283E+0.1 4.630E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF CE-144 l.498E-01 3.408E-01 7.123E-01 NOT IDENT. PM-144 4.402E-02 5.266E-02 1.146E-01 NOT IDENT. PR-144 3.809E+OO 4. 572E+OO 9. 951E+OO NOT IDENT. PM-146 -l.214E-02 3.260E-02 6.245E-02 NOT IDENT. ND-147 O.OOOE+OO 3.024E+07 O.OOOE+OO SHORT HLIF PM-147 -2.548E+02 7.513E+02 1.508E+03 NOT IDENT. PM-149 0.000E+OO 4.331E+40 O.OOOE+OO SHORT HLIF EU-150 -l.270E-02 2.744E-02 4.574E-02 FAIL ABUN EU-152 -7.684E-02 8.370E-02 1.499E-01 FAIL ABUN GD-153 -l.793E-01 1.938E-01 3.322E-01 NOT IDENT. EU-154 6.338E-02 l.083E-01 2.445E-01 NOT IDENT. EU-155 6.365E-02 l.031E-01 2.037E-01 FAIL ABUN TB-160 -7.199E-01 1. 731E+OO 3 .134E+OO FAIL ABUN H0-166M 2.188E-02 4.819E-02 1. 026E-01 FAIL ABUN TM-171 6.729E+00 2.542E+Ol 5.066E+Ol NOT IDENT. HF-172 -7. 921E-02 2.098E-01 4.189E-01 NOT IDENT. LU-172 3.032E-02 6.454E-02 l.402E-01 FAIL ABUN LU-176 -1.611E-02 2.231E-02 4.127E-02 FAIL ABUN Page 3314 of 5809 HF-181 2.602E+OO 3.542E+OO 7.821E+OO NOT IDENT. TA-182 2.248E-01 8.492E-Ol 1.808E+OO FAIL ABUN RE-183 -5.144E-01 3.730E+OO 7.089E+OO NOT IDENT. RE-184 3.349E+Ol 4.743E+Ol 5.484E+Ol FAIL ABUN W-188 1.903E+Ol l.140E+02 2.079E+02 NOT IDENT. IR-192 6.747E-02 4.262E-01 8. 613E-Ol FAIL ABUN HG-203 -9.829E-01 2.254E+OO 4.310E+OO NOT IDENT. BI-207 3.053E-02 3. 961E-02 9.927E-02 FAIL ABUN PB-211 -l.031E-01 5.692E-01 1. lllE+OO NOT IDENT. RN-219 -1.239E-02 3.529E-01 6. 960E-Ol NOT IDENT. RA-223 -3.173E-01 4.935E-01 9.193E-01 FAIL ABUN AC-227 2.433E-02 2.086E-01 4.208E-01 NOT IDENT. TH-227 2.433E-02 2.086E-01 4.208E-01 NOT IDENT. TH-229 -3.639E-02 4.542E-01 9.037E-01 FAIL ABUN PA-231 1.156E-01 4.450E-01 8.958E-01 NOT IDENT. TH-231 -3.173E-01 4.935E-01 9.193E-01 FAIL ABUN PA-233. -l.389E-02 5.283E-02 1.027E-01 NOT IDENT. PA-234 -1.350E-02 2. 696E-01 5.200E-01 NOT IDENT. PA-234M l.356E+OO 4.383E+OO 9.216E+OO NOT IDENT. TH-234 -4.212E-01 1.464E+OO 2.801E+OO FAIL ABUN U-235 -7.525E-02 1.741E-01 3.446E-01 FAIL ABUN. NP-237 -1.389E-02 5.283E-02 l.027E-01 NOT IDENT. NP-238 O.OOOE+OO l.611E+41 O.OOOE+OO SHORT HLIF U-238 -4.212E-01 l.464E+00 2. 801E+OO FAIL ABUN NP-239 -3.997E-02 2.683E-01 4.895E-01 NOT IDENT. PU-239 2.487E+02 3.152E+02 6.675E+02 NOT IDENT. AM-241 -2.316E-02 1.566E-01 2.979E-01 NOT IDENT. CM-243 -6.645E...:02 1.022E-01 1. 799E-01 NOT IDENT. BK-247 2.848E-02 6.512E-02 1.352E-01 NOT IDENT. CM-247 4.868E-03 3.055E-02 6.195E-02 NOT IDENT. CF-251 -5.439E-02 l.037E-01 2.013E-01 NOT IDENT. Page 3315of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:53:53.04 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM *%Error K-40 1460.82 252 10.66* 9.709E-01 1.069E+Ol l.069E+Ol 13.46 CD-109 88.03 63. 3.70* 4.617E+OO l.625E+00 2.550E+OO 119.39 SN-126 64.28 ------9.60 2.409E+OO ------Line Not Found ------86.94 63 8.90 4.617E+OO 6.758E-01 6.758E-01 119. 39 87.57 63 37.00* 4.617E+OO 1.625E-01 1.625E-01 119.39 TL-208 277.37 ------6.60 3.944E+OO ------Line Not Found ------583.19 122 85.00* 2.090E+OO 3.015E-01 3.015E-01 31. 39 860.56 33 12.50 l.519E+00 7. 551E-01 7. 551E-01 65.24 PB-210 46.54 27 4.25* 4.948E-01 5.729E+00 5.877E+OO 144.32 BI-211 72.87 ------1. 23 3.328E+OO ------Line Not Found ------351. 06 264 12.92* 3.217E+OO 2.795E+OO 2.795E+OO 18.24 BI-212 727. 33 54 6.67* l.742E+00 2.061E+OO 2.061E+OO 48.56 785.37 12 1.10 1. 636E+OO 2.959E+OO 2.959E+OO 126.79 1620.50 ------1. 47 8.816E-01 ------Line Not Found ------PB-212 74.82 142 10.28 3.530E+OO 1.714E+OO 1.714E+OO 52.00 77 .11 209 17.10 3.747E+OO 1.433E+OO 1.433E+OO 34.06 238.63 425 43.60* 4.455E+OO 9.612E-01 9.612E-01 13.33 300.09 ------3.30 3.690E+OO ------Line Not Found ------BI-214 609.32 130 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 1764.49 20 15.30 8.116E-01 7.200E-01 7.202E-01 58 .11 PB-214 74.82 142 5.80 3.530E+OO 3.039E+OO 3.040E+OO 52.00 77 .11 209 9.70 3.747E+OO 2.527E+00 2.528E+OO 34.06 87.09 63 3.41 4.617E+OO 1. 7 64E+00 1. 764E+OO 119. 39 242.00 116 7.25 4.410E+OO 1.592E+OO l.592E+00 49.21 295.22 103 18.42 3.741E+OO 6.557E-01 6.560E-01 40.21 351.93 264 35.60* 3.217E+OO 1.015E+OO l.015E+00 18.24 RN-222 609.32 130 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 1120.29 40 14.92 l.223E+OO 9.517E-01 9. 521E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 RA-224 240.99 116 4.10* 4.410E+OO 2.815E+OO 2.815E+OO 49.21 *RA-226 609.32 130 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 1120. 29 40 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 AC-228 105.21 ------1.10 5.519E+00 ------Line Not Found ------338.32 63 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 794.95 ------4.25 1. 621E+OO ------Line Not Found ------835.71 ------1. 61 1.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 968. 97 42 15.80 1. 379E+OO 8.506E-01 8.506E-01 45.09 RA-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 794.95 ------4.25 l.621E+00 ------Line Not Found ------835. 71 ------1. 61 1.557E+OO ------Line Not* Found ------911.20 60 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 968. 97 42 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 TH-228 74.82 142 10.28 3.530E+OO l.714E+OO 1.714E+OO 52.00 Page 3316of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nucl,ide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 209 17.10 3. 74-7E+00 1.433E+OO l.433E+OO 34. 06-238.63 425 43.60* 4. 45'5E+OO 9.612E-01 9.612E-01 13. 33* 300.09 ------3.30 3.690E+OO ------Line Not Found ------TH-230 609.32 130 45.49* 2.015E+00 6.255E-01 6.255E-01' 26.31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.517E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.200E-01 58 .11 TH-232 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 835. 71 ------1. 61 1.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 968. 97 42 15.80 1. 37 9E+OO 8.506E-01 8.506E-01 45.09 U-234 609.32 130 45.49* 2.015E+OO 6.255E-01 6.255E-01 26.31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.517E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.200E-01 58 .11 AM-243 43.53 ------5.90 3.822E-01 ------Line Not Found ------74.66 142 67.20* 3.530E+OO 2.623E-01 2.623E-01 52.00 CF-249 252.80 ------2.50 4.256E+OO ------Line Not Found ------333.37 ------14.60 3. 371E+OO ------Line N.ot Found* ------388.16 16 66.00* 2.950E+OO 3. 721E-02 3. 727E-02 296.41 ANH-511 511. 00 51 100.00* 2.334£+00 9.690E-02 9.690E-02 93.64 Flag: "*" Key line Page 3317 of 5809 Summary of Nuclide Activity Sample ID : G405235020 Acquisition date Page : 3 3-0CT-2016 08:53:24 Total number of lines in spectrum 44 Number of unidentified lines 11 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide Hlife K-40 -1.25E+09Y CD-109 461.400 SN-126 2.30E+05Y TL-208 l.41E+l0Y PB-210 22.20Y BI-211 7.04E+08Y BI-212 l.41E+10Y PB-212 1.41E+l0Y BI-214 1600.00Y PB-214 1600.00Y RN-222 1600.00Y RA-224 l.41E+l0Y RA-226 1600.00Y AC-228 1.41E+10Y RA-228 1.41E+10Y TH-228 . 1.41E+l0Y TH-230 7.54E+04Y TH-232 l.41E+10Y U-234 2.45E+05Y AM-243 7370.00Y CF-249 351.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.069E+Ol l.625E+00 l.625E-01 3.015E-01 5. 729.E+OO 2.795E+OO 2.061E+OO 9.612E-01 6.255E-01 1.015E+OO 6.255E-01 2.815E+00 6.255E-01 7.028E-01 7.028E-01 6.255E-01 7.028E-01 6.255E-01 2.623E-01 3. 721E-02 9.690E-02 3.475E+Ol 3.475E+Ol Decay Corr pCi/GRAM 1.069E+Ol 2.550E+OO l.625E-01 3.015E-01 5.877E+OO 2.795E+OO 2.061E+OO 9.612E-01 6.257E-01 1.015E+OO 6.257E-01 2.815E+OO 6.257E-01 7.028E-01 7.028E-01 9.612E-01 6.255E-:-01 7.028E-01 6.255E-01 2.623E-01 3.727E-02 9.690E-02 3.582E+Ol 3.582E+Ol 75.00% Decay Corr 2-Sigma Error 0.144E+Ol 3.045E+OO 1. 941E-01 0.947E-01 8.483E+OO 0.510E+OO 1.00lE+OO L-281E-01 1.646E-01 0.185E+OO 1.646E-01 1.385E+OO 1. 646E-01 2.975E-01 2.975E-01 1.281E-01 l.646E-01 2.975E-01 1.646E-01 l.364E-01 11. 05E-02 9.074E-02 "M" Manually accepted 2-Sigma %Error 13.46 119. 39 119. 39 31. 39 144.32 18.24 48.56 13.33 26.31 18.24 26.31 49.21 26.31 42.33 42.33 13.33 26.31 42.33 26.31 52.00 296.41 93.64 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclida specific abn. limit Page 3318 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235020 Acquisition date : 3-0CT-2016 08:53:24 It Energy Area Bkgnd FWHM Channel Left PW Cts/Sec %Err %Eff Flags 5 35.35 55 15 1. 84 71. 39 67 32 1. OlE-02 81. 7 4.02E-02 5 40.33 43 82 1. 85 81. 37 67 32 8.00E-03 **** 2.0lE-01 0 92.89 57 193 1.12 186.47 183 8 1.16E-02 **** 4.95E+OO T 0 185 .. 65 108 223 1. 41 371. 96 366 14 2.37E-02 71. 6 5.30E+oo* T 0 209.98 119 172 5.43 420.62 413 18 2.65E-02 61. 5 4.90E+OO T 0 216.83 30 52 1. 25 434.33 431 6 6.67E-03 94.6 4.79E+OO T 0 463.85 45 75 4.43 928.29 920 20 l. llE-02 **** 2.53E+OO T 0 566.51 34 59 0.87 1133.56 1127 16 8.51E-03 **** 2.14E+OO 0 636.61 8 21 1. 40 1273.74 1266 11 2.07E-03 **** 1. 94E+OO T 0 737. 71 26 11 3.50 1475.89 1468 14 6.82E-03 69.0 .1. 72E+OO T 0 768.80 19 26 0.62 1538.04 1531 12 4.86E-03 **** 1.67E+OO 0 904.69 12 14 4.40 1809.75 1802 13 3.18E-03 **** 1.46E+OO T 0 964.44 29 16 1. 32 1929.20 1922 13 7.83E-03 69.8 1.38E+OO T 0 1063.09 7 5 1. 46 2126.44 2123 6 1.77E-03 **** 1.28E+OO T 0 1143. 54 8 11 0.53 2287.27 2282 7 2.08E-03 **** 1.20E+OO 0 1155.31 10 10 1. 46 . 2310. 80 2305 10 2.78E-03 **** 1.19E+OO 0 1173.52 5 4 0.52 2347.20 2346 4 1. 45E-03 **** 1.18E+OO T 0 1234.37 8 20 3.32 2468.87 2459 13 2.08E-03 **** 1.13E+OO T 0 1254.20 10 0 1. 66 2508.50 2505 7 2.78E-03 63.2 l. llE+OO 0 1285.78 11 0 1. 28 2571.64 2568 7 3.06E-03 60.3 1. 09E+OO 0 1493.39 12 0 1. 65 2986.67 2982 9 3.33E-03 57.7 9.51E-01 0 1591.81 10 0 1. 4'1 3183.40 3179 8 2.78E-03*63.2 8.97E-01 0 1729.55 10 0 1. 72 3458.73 3455 7 3.06E-03 60.3 8.28E-01 Flags: "T" = Tentatively associated Page 3319of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:54:10.66 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l * *Acquisition date 3-0CT-2016 08:53:24 Sensitivity 3.000 *
Detector ID GAMOl Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed reil time: 0 01:00:00.37 Half life ratio : ***** *
Sample date 8-DEC-2015 13:50:00 Nuclide Library : SOLID *
Sample ID G405235020 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7076E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * *. *
Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry* : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214. PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-243 CF-249 ANH-511 Le (pCi/GRAM 2.147E-01 1. 2 66E+OO 7.444E-02 2.278E-02 2.644E+OO 1.605E-01 2.978E-01 3.908E-02 6.032E-02 l.472E-01 6.032E-02 4.189E-01 6.032E-02 l.125E-01 1.125E-01 3.908E-02 6.030E-02 1.125E-01 6.030E-02 4.462E-02 2.935E-02 l.898E-02 ----Non-Identified Nuclides. Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 3320 of 5809 Le (pCi/GRAM 8.769E+OO 4.349E-02 O.OOOE+OO 2.069E-02 3.128E-01 O.OOOE+OO O.OOOE+OO 5.509E-02 3.935E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131* I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181

Page 3321of5809 O.OOOE+OO 3.837E-02 4.200E-01 4.727E+OO 2.014E-02 1.172E-01 1.644E+OO 1.002E+Ol O.OOOE+OO 1.775E-01 O.OOOE+OO O.OOOE+OO 4.485E-01 5.218E+OO 5.506E-01 O.OOOE+OO 1. 807E-01 4.224E+02 2.923E-02 8 .131E-01 1. 963E+OO 1.158E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.167E-02 3.523E-02 3.864E+OO 3.058E-01 3.058E-01 2.200E-02 7.879E-02 1. 8 66E-01 0.000E+OO O.OOOE+OO 1.180E-01 2.139E+OO 7.700E-02 2.664E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.366E-02 O.OOOE+OO 4.337E-02 1.159E-01 O.OOOE+OO O.OOOE+OO 3.563E-02 3.764E-02 8.935E-02 O.OOOE+OO O.OOOE+OO 2.179E+Ol 0.000E+OO 3.357E-01 5.125E-02 4.448E+OO 2.709E-02 0.000E+OO 7.058E+02 0.000E+OO 2.089E-02 6.742E-02 1.558E-01 l.054E-01 9.556E-02 l.326E+00 4.488E-02 2.364E+Ol 1. 963E-01 5. 961E-02 l.877E-02 3.485E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT*. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 RN-219 RA-223 AC-227 TH-227 , TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 3322 of 5809 7.829E-01 3.325E+OO 2.353E+Ol 9.581E+Ol 3.945E-:-01 1.984E+OO 4.314E-02 4.974E-01 3.149E-01 4.139E-01 1.945E-01 l.945E-01 4.238E-01 4.158E-01 4.139E-01 4.676E-02 2.238E-01 4.068E+00 1.323E+OO 1.623E-01 4.676E-02 O.OOOE+OO 1.323E+OO 2.306E-01 3.164E+02 1.392E-01 8. 411E-02 6.244E-02 2.793E-02. 9.384E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT*IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:54:17.70 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l * *Acquisition date 3-0CT-2016 08:53:24 Sensitivity : 3.000 *
Detector ID GAMOl Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.37 Half life ratio : ***** *
Sample date 8-DEC-2015 13:50:00 Nuclide Library : SOLID *
Sample ID G405235020 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity 1.7076E+02 GRAM *
Quantity Err(%) 1.1712E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 20-JUL-2016 07:03:55' Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-243 CF-249 ANH-511 1.069E+Ol 1.602E+OO 1.021E-01 3.015E-01 5.877E+OO 9.887E-01 2.061E+OO 9.612E-01 6.257E-01 1.015E+OO 6.257E-01 1. 655E*+oo 6.257E-01 7.028E-01 7.028E-01 9.612E-01 6.255E-01 7.028E-01 6.255E-01 2.057E-01 3.727E-02 9.690E-02 Act Error ( 1. 96-sigma) 1.516E+OO 3.012E+OO 1.919E-01 9.364E-02 8.343E+OO 8.779E-01 9.862E-01 l.355E-01 l.635E-01 1.862E-01 1.635E-01 l.437E+OO l.635E-01 2.938E-01 2.938E-01 1.355E-01 l.635E-01 2.938E-01 1.635E-01 1.363E-01 l.083E-01 8. 901E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 3323 of 5809 Key-Line Activity (pCi/GRAM -4.924E+00 2.738E-02 1.000E+41 l.405Ei-02 4.814E-02 4.336E+03 -2.615E+02 2. 968E-02 K.L Act error ( 1. 96-sigma) 1.068E+Ol 4.453E-02 2.203E+42 l.736E-02 3. 611E-01 1.335E+04 3.815E+02 5.950E-02 TPU (1.96-sigma) 1.516E+OO 3.012E+OO 1.919E-01 9.364E-02 8.343E+OO 8.779E-01 9.862E-01 l.355E-01 l.635E-01 1.862E-01 l.635E-01 1.437E+OO l.635E-01 2.938E-01 . 2.938E-01 l.355E-01 l.635E-01 2.938E-01 l.635E-01 1. 363E-01 1.083E-01 8. 901E-02 TPU ( 1. 96-sigma) 1.090E+Ol 4.621E-02 0.000E+OO l.848E-02 3.617E-01 l.349E+04 3.993E+02 6.098E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1. 764E-01 4.299E-01 4. 372E-01 NOT IDENT. MN-56 l.OOOE+41 2.437E+41 O.OOOE+OO SHORT HLIF C0-57 -3.997E-02 4.283E-02 4.646E-02 NOT IDENT. C0:-58 -2.614E-01 5.487E-01 5.612E'-01 NOT IDENT. FE-59 -2.573E+OO 6.346E+OO 6. 451E+OO NOT IDENT. C0-60 -2.207E-02 2.976E-02 3.138E-02 FAIL ABUN ZN-65 -2.641E-02 l.685E-01 l.689E-01 NOT IDENT. GE-68 -6.242E-01 2.138E+OO 2.156E+OO NOT IDENT. AS-73 2.796E+OO 1.081E+Ol 1. 088E+Ol NOT IDENT. AS-74 l.607E+03 5.877E+03 5.921E+03 SHORT HLIF SE-75 5.865E-02 1. 871E-01 1.890E-01 NOT IDENT. BR-77 1. 712E+38 1.481E+39 O.OOOE+OO SHORT HLIF SR-82 -l.858E+02 6.129E+02 6.186E+02 SHORT HLIF RB-83 -5.550E-04 5.099E-01 5.099E-01 NOT IDENT. KR-85 2.082E+OO 5.607E+OO 5.685E+OO NOT IDENT. SR-85 2.176E-01 5.918E-01 5.999E-01 NOT IDENT. RB-86 -5.605E+03 2.610E+04 2.622E+04 SHORT HLIF Y-88 -4. 372E-02 2.273E-01 2.282E-01 NOT IDENT. Y-91 l.208E+02 4. 561E+o2 4.594E+02 NOT IDENT. NB-94 l.537E-02 3.167E-02 3.242E-02 NOT IDENT. NB-95 4.826E-01 9.696E-01 9.937E-01 NOT IDENT. NB-95M -l.840E-01 2.374E+OO 2.375E+OO NOT IDENT. ZR-95 -2.812E-01 1. 414E+OO 1.419E+OO NOT IDENT. NB-97 l.OOOE+41 1.668E+42 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 1. 531E+41 O.OOOE+OO SHORT HLIF M0-99 -2.145E+31 1.851E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 2.467E+41 O.OOOE+OO SHORT HLIF RH-101 7.438E-04 3.293E-02 3.294E-02 NOT IDENT. RH-102 -1.297E-02 4.934E-02 4. 969E-02 NOT IDENT. RU-103 -4.617E+OO 5.131E+OO 5.537E+00 FAIL ABUN RH-106 -4.426E-01 4.400E-01 4.832E-01 NOT IDENT. RU-106 -4.426E-01 4.400E-01 4.832E-01 NOT IDENT. AG-108M 7.609E-05 2.467E-02 2.467E-02 NOT IDENT. AG-110M 4.315E-02 8.376E-02 8.599E-02 NOT IDENT. SN-113 4.383E-02 2.245E-01 2.253E-01 NOT IDENT. CD-115 3.351E+38 2.478E+39 O.OOOE+OO SHORT HLIF SN-117M 9. 722E+03 8.818E+04 8.829E+04 SHORT HLIF TE-123M 7.173E-02 1.193E-01 1.236E-01 NOT IDENT. SB-124 1.758E+OO 2.008E+OO 2.158E+OO NOT IDENT. SB-125 1. 072E-02 8.474E-02 8.488E-02 FAIL ABUN TE-125M 9.450E+Ol 2. 969E+02 2.999E+02 NOT IDENT; I-126 3.377E+05 7. 671E+05 7.820E+05 SHORT HLIF SB-126 -1.330E+05 1.341E+06 l.342E+06 SHORT HLIF SB-127 -3.836E+20 2.013E+22 O.OOOE+OO SHORT HLIF I-131 1. 689E+09 4.541E+09 4.604E+09 SHORT HLIF I-132 -1.000E+41 1. 877E+42 O.OOOE+OO SHORT HLIF TE-132 1.652E+26 3.747E+26 O.OOOE+OO SHORT HLIF BA-133 -4.435E-03 4. 221E-02 4.226E-02 NOT IDENT. I-133 l.OOOE+41 2.568E+41 O.OOOE+OO SHORT HLIF CS-134 3.244E-02 4. 511E-02 4.743E-02 NOT IDENT. CS-135 -7.638E-02 l.330E-01 1. 37 4E-01 NOT IDENT. I-135 -1 .. 000E+41 9 .112E+41 O.OOOE+OO SHORT HLIF CS-136 -2.013E+05 2.551E+05 2.707E+05 SHORT HLIF BA-137M 3. 7 51E-02 3. 613E-02 3.989E-02 NOT IDENT. CS-137 3. 962E-02 3.817E-02 4.214E-02 NOT IDENT. CE-139 -3.178E-02 9.704E-02 9.810E-02 . NOT IDENT. BA-140 4 .119E+05 1.208E+06 l.223E+06 SHORT HLIF LA-140 1.304E+05 3.755E+05 3.801E+05 SHORT HLIF CE-141 3 .115E-01 2.283E+Ol 2.283E+Ol NOT IDENT. CE-143 -l.OOOE+41 2.145E+41 O.OOOE+OO SHORT HLIF CE-144 1.498E-01 3.409E-01 3.476E-01 NOT IDENT. PM-144 4.402E-02 5.273E-02 5.634E-02 NOT IDENT. PR-144 3.809E+OO 4.575E+OO 4.886E+OO NOT IDENT. PM-146 -l.214E-02 3.261E-02 3.307E-02 NOT IDENT. ND-147 6.976E+06 3.024E+07 3.040E+07 SHORT HLIF PM-147 -2.548E+02 7.514E+02 7.601E+02 NOT IDENT. PM-149 -2.895E+39 4. 331E+40 O.OOOE+OO SHORT HLIF EU-150 -l.270E-02 2.745E-02 2.804E-02 FAIL ABUN EU-152 -7.684E-02 8.381E-02 9.069E-02 FAIL ABUN GD-153 -1.793E-01 l.941E-01 2.103E-01 NOT IDENT. EU-154 6.338E-02 l.084E-01 l .121E-01 NOT IDENT. EU-155 6.365E-02 l.032E-01 1.071E-01 FAIL ABUN TB-160 -7.199E-01 l.731E+OO 1. 762E+OO FAIL ABUN H0-166M 2. 18 8E-02 4.821E-02 4.921E-02 FAIL ABUN TM-171 6.729E+OO 2.543E+Ol 2. 561E+Ol NOT IDENT. HF-172 -7.921E-02 2.102E-01 2 .132E-01' NOT IDENT. LU-172 3.032E-02 6.461E-02 6.604E-02 FAIL ABUN LU-176 -1. 611E-02 2.232E-02 2.347E-02 FAIL ABUN Page 3324 of 5809 HF-181 2.602E+OO 3.544E+00 3.733E+OO NOT IDENT. TA-182 2.248E-01 8.493E-01 8.553E-Ol FAIL ABUN RE-183 -5.144E-01 3.731E+OO 3.738E+OO NOT IDENT. RE-184 3.349E+Ol 4.810E+Ol 5.042E+Ol FAIL ABUN W-188 1.903E+Ol l .141E+o2 1.144E+02 NOT IDENT. IR-192 6.747E-02 4.262E-01 4.273E-01 FAIL ABUN* HG-203 -9.829E-01 2.255E+OO 2.298E+OO NOT IDENT. BI-207 3.053E-02 3. 963E-02 4.195E-02 FAIL ABUN PB-211 -1. 031E-01 5.692E-01 5.711E-01 NOT IDENT. RN-219 -l.239E-02 3.529E-01 3.529E-01 NOT IDENT. RA-223 -3.173E-01 4.939E-01 5.142E-01 FAIL ABUN AC-227 2. 433E-02. 2.086E-01 2.089E-01 NOT IDENT. TH-227 2.433E-02 2.086E-01 2.089E-01 NOT IDENT. TH-229 -3.639E-02 4.542E-01 4.545E-01 FAIL ABUN PA-231 l.156E-01 4.457E-01 4.487E-01 NOT IDENT. TH-231 -3.173E-01 4.939E-01 5.142E-01 FAIL ABUN PA-233 -1.389E-02 5.284E-02 5.321E-02 NOT IDENT. PA-234 -1.350E-02 2.701E-01 2.702E-01 NOT IDENT. PA-234M l.356E+00 4.383E+OO 4.426E+OO NOT IDENT. TH-234 -4.212E-01 1.467E+OO 1.479E+OO FAIL ABUN U-235 -7.525E-02 l.742E-01 1. 774E-Oi FAIL ABUN NP-237 -l.389E-02 5.284E-02 5.321E-02 NOT IDENT. NP-238 -1. 000E+41 1.612E+41 O.OOOE+OO SHORT HLIF U-238 -4.212E-01 l.467E+OO 1.479E+oo FAIL ABUN NP-239 :....3. 997E-02 2.684E-01 2.690E-01 NOT IDENT. PU-239 2. 487E+02 . 3.154E+02 3.347E+02 NOT IDENT. AM-241 -2.316E-02 l.566E-01 l.569E-01 NOT IDENT. CM-243 -6.645E-02 l.024E-01 l.067E-Ol NOT IDENT. BK-247 2.848E-02 6.537E-02 6.662E-02 NOT IDENT. CM-247 4.868E-03 3.056E-02 3.064E-02 NOT IDENT. CF-251 -5.439E-02 l.039E-01 l.067E-01 NOT IDENT. Page 3325 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 32.3526 87.09 125.0983 136.47 94.4772 45.60 32.4465 87.57 125.1552 140.51 0.0000 46.54 32.4883 88.03 149.1172 143.76 88.1912 49.72 0.0000 88.34 137.8120 144.24 93.3104 51. 35 67.7282 . 88. 4 7 137.8284 145.44 84.8999 51. 87 61. 9311 89. 96 119. 3485 152.43 79.3401 52.39 59.6337 1093.63 119. 4240 153.25 0.0000 52.97 54. 9971 91.11 0.0000 323.87 68.3325 53.44 63.2258 92.59 113. 5360 156.02 0.0000 54.07 73.8219 93.35 113.6148 158.56 0.0000 57.36 0.0000 94.56 66.8581 159.00 65.1254 57.53 71. 7839 94.65 66.8636 162.33 63.5516 57.98 80.0647 94.67 66.8648 162.66 0.0000 59.27 70.7545 94.87 78.2949 163.33 60.1563 59.32 70.7588 97.43 99.3207 165.86 70.5847 59.54 70.7774 98.43 81.0000 176.31 74.5230 60. 96 89.8015 98.44 81. 0010 176.60 'O. 0000 61.17 89.8235 99.53 78.6221 177.52 74*_5790 62.93 82.9012 100 .11 77.4330 181.07 0.0000 63. 29 81.7507 102.03 91.1055 181.52 62.5935 63.58 81. 7779 103.18 86.2669 184.41 71.4130 64.28 86.5877 103.37 86.2813 143.76 71. 4697 66.73 111. 8036 105.21 61.7268 193.51 77.9338 67.24 108.2972 105.31 61.7321 197.03 78.9725 125.81 98.8247 106.12 69.1874 198.01 63.2146 67.75 84.5427 106.47 86.5099 201.83 60.7147 69.67 77.9592 109.28 84.2374 203.43 51.7874 70.83 92.3938 111. 00 94.2822 205.31 46.2884 72.81 85.0064 111. 76 0.0000 210.85 55.7204 72.87 85. 0118 114. 06 104.4681 215.65 37.2465 74.66 85.1716 116. 30 0.0000 222.11 67.6373 74.82 85.1857 116.74 93.4776 227.09 62.4648 74.97 85.1990 119.76 62.4683 227.38 56.2273 77 .11 85.3872 121.12 78.3773 228.16 0.0000 78.74 96.3708 121.22 79.2174 228.18 57.1439 79.69 94.8553 121. 78 85.0918 116.74 57.1439 80.12 94.8961 122.06 85 .1105 235.69 61.8532 80.19 0.0000 122.92 71. 8080 235. 96 57.8278 80.57 109.4209 123.07 71.8163 238.63 47.5838 81. 00 107.8581 265.00 71. 8504 238.98 0.0000 81. 07 *107.8656 125.81 82.8474 240.99 47.6420 81. 75 106.3275 127.23 90.4771 242.00 47.6668 83.79 106.5403 127.91 82.1422 244.70 45.9313 84.00 106.5625 129.30 89.7806 252.40 0.0000 85.43 111. 5607 131.20 110.0755 252.80 56.9720 86.55 125.0338 133.02 81. 6168 254.15 0.0000 86.79 125.0621 133.52 79.1222 256.23 48.0108 86.94 125.0802 136.00 88.5425 260.90 0.0000 Page 3326 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.8429 355.39 0.0000 584.27 14.3287 264.80 40.9360 356.01 35.5156 595.83 0.0000 265.00 40.9396 364.49 0.0000 427.87 22.6230 2 68. 22 58.3164 366.42 0.0000 602.52 0.0000 269.46 43.7637 372. 51 26.6926 604. 72 32.4305 270.03 45.5994 375.05 28.6279 607.14 21.6349 271.23 52.9259 377.52 20.0588 609.32 26.8030 273.65 0.0000 356.01 24.4167 610.33 26.8104 276.40 49.3978 388.16 27.8135 614.28 20.1300 277.37 48.5046 388.63* 0.0000 618.01 20.6681 277.60 45.7642 391.69 25.9305 620. 36 14.4774 278.00 44.8578 264.66 28.9087 621.93 21. 7255 279.20 53.1265 401.81 30.8496 630.19 0.0000 279.54 54.9670 402.40 26.0349 631. 29 12.4468 279.70 57.7205 404.85 27. 02*36 633.25 3 .1134 280.46 43.0766 410.95 *31.9211 634.78 0.0000 283.69 37.6342 413.71 28.0802 635.95 17.6558 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 49.6066 423. 72 0.0000 645.85 14.5793 285.90 0.0000 427.09 21.405.6 657.76 17.7609 287.50 48.7354 427.87 20.4386 657.90 0.0000 290.67 42.8208 433.94 24.3841 661. 66 16.7337 293.27 0.0000 439.40 20.5223 664.57 0.0000 351. 93 33.2205 453.88 18.6614 666.33 0.0000 295. 96 33.2314 463.37 20.6928 666.50 0.0000 879.38 52.6791 468.07 23.6865 667.71 0.0000 299.98 39.9507 473.00 0.0000 677. 62 11. 5532 300.09 44.3916 475.06 24.7314 685.70 0.0000 300 .13 44.3926 476.78 22.7660 695.00 0.0000 301.36 50.8945 477.60 23.7622 696.49 13.7210 302.85 54.6319 482.18 13.8826 696.51 13. 7210 256.23 36.1396 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.8356 306.78 46.3796 497.08 26.9044 697.49 14.7804 308.46 31.5616 505.52 13.4887 702.65 17.9712 311. 90 39.0469 507.63 0.0000 706.68 9.5240 316.51 37.2624 511. 00 17.0157 711. 68 11. 6557 319.41 0.0000 514.00 17.0318 720.70 0.0000 320.08 0.0000 514.00 17.0318 721. 93 0.0000 321. 04 35.4688 520.40 15.0586 722.78 23.9081 323.87 37.3812 520.69 0.0000 722. 91 23.9090 325.23 39.2725 522.65 0.0000 723.31 15.9406 328.76 0.0000 527.90 0.0000 724.19 10.6295 333.37 42.7862 528.26 18 .1150 727.33 10.6380 333.97 46.4576 529.59 14.0951 733.00 6.3918 334.37 38.0174 529;87 0.0000 735.93 11. 7269 338.28 36.6688 531. 02 0.0000 333.97 11. 7314 338.32 36.6696 537.26 0.0000 739.50 0.0000 311. 90 36.7021 546.56 0.0000 747.24 11.7600 340.48. .36. 7021 552.55 17.2366 748.06 12.8315 340.55 0.0000 563.25 10.6803 752.31 14.9855 344.28 41.4729 569.33 25.4751 753.82 0.0000 345.93 27.3533 946.00 18.3428 756.73 16.0736 351.06 37.8076 569.70 18.3442 756.80 16.0736 351. 93 37.8206 583.19 14.3241 884.68 12.8813 Page 3327 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.7199 1274.44 7.9100 1620.50 3.7656 766.42 22.5560 1001.03 10.1796 1621. 92 4.7079 766.84 21.4844 1002.74 20.3665 1678.03 0.0000 772.60 0.0000 1004.73 18 .1107 1690.97 1.9015 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.8413 778.90 8.6188 1028.54 0.0000 1063.66 5. 7 664 783.70 0.0000 1037.84 7.9758 1771.35 2.8835 785.37 14.0273 1038.76 0.0000 1791.20 0.0000 792.07 17.2917 631.29 5.7068 1808 .*65 0.0000 794.95 11. 8961 1048.07 0.0000 1810.72 0.0000 795.86 10.8171 1049.04 9.1348 1836.06 4.8471 810.06 16.2793 1050.41 2.2843 810.29 16.2805 1063.66 22.3295 344.28 . 18.4519 1077.00 0.0000 810.76 16.2823 1077.34 11.4811 815.77 0.0000 1085.87 9.1999 1048.07 0.0000 1093.63 6.9102 832.01 16.3623 1099.45 12.6829 834.85 12.0066 1112. 07 10. 4011 835.71 14.1928 1112.84 12.7143 836.80 0.0000 1115. 54 10.4077 846.75 0.0000 1120.29 10.4172 846.77 10.9448 1120.55 8.6816 856.80 0.0000 1221.41 13.8926 860.56 9.8811 1129. 67 10.4355 871. 09 8.8037 1131.51 0.0000 873.19 11. 0099 1147.95 0.0000 875.33 0.0000 1173.23 18.4070 879.38 14.3325 1177.95 16.0424 880.51 14.3357 1189.05 20.2177 883.24 15.4481 1204.77 9. 6962 884.68 7.7263 1221.41 11.4932 889.28 12.1539 1231.02 17.7112 894.76 12.1682 1235.36 0.0000 898.04 6.6418 1238.28 21. 2798 900.72 4.9843 1260.41 0.0000 903.28 14.6287 1271. 87 11.5932 911.20 15.9861 1274.44 8.0294 912.08 13.3242 1274.54 8.0299 923.98 0.0000 1291. 59 7.1582 926.50 8.9102 1298.22 0.0000 929 .11 12.2582 1312.11 0.0000 937.49 15.6292 1332.49 8.1079 944 .13 0.0000 1362.66 0.0000 946.00 13.4204 1365.19 4.5285 949.00 8.9525 1368.63 0.0000 667.71 0.0000 1384.29 4.5422 962.31 15.1496 1408.01 6.3831 964.08 15.1551 1457.56 0.0000 966.17 0.0000 1460.82 4.5972 911.20 6.7422 1489.16 7. 3872 968. 97 6.7422 1505.03 7.4048 983.53 0.0000 1584.12 7.4922 984.45 0.0000 1596.21 0.0000 Page 3328 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:51:34.03
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621350.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM31.CNF;306 Background date : Z-OCT-2016 11:01:52. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 08:50:58. Sample ID G1203621350 Sample quantity 1.75Q75E+02 GRAM Detector name : GAM31 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.18 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.22* 1 130 0.79 92.08 89 7 3.17E-04***** 2 0 54.71 24 187 1. 30 109.05 103 8 6.75E-03100.3 3 0 62.87* 29 119 1. 89 125.37 122 7 8.02E-03 73.9 4 0 187.22* 18 47 6.25 366 18 4.98E-03100.5 5 0 296.25* 10 24 1*. 89 59i.79 586 9 2.85E-03 97.3 6 0 338.11* 17 8 0.93 675.45 671 8 4. 71E-03 42.2 7 0 397 .11 11 8 3.32 793.37 788 9 2. 96E-03 58.8 8 0 408.80 8 22 1.17 816.72 813 11 2.31E-03123.8 9 0 416.83 23 11 5.28 832.78 825 15 6.38E-03 38.0 10 0 437.75 9 6 1. 73 874.59 871 8 2.40E-03 60.2 11 0 483.85 12 8 1. 86 966.73 960 10 3.42E-03 50.5 12 0 569.56 14 5 3.28 1138. 04 1133 9 3.75E-03 39.3 13 0 609.71* 2 8 1. 53 1218.28 1214 8 5.07E-04344.1 14 0 702.13* 14 15 1. 58 1403.00 1396 15 3.84E-03 68.2 15 0 873.87 8 1 0.69 1746.26 1743 6 2.lOE-03 44.4 16 0 911. 55* 6 2 0.71 1821. 58 1817 8 l.59E-03 75.0 17 0 1121.09 12 2 1. 86 2240.41 2236 9 3.33E-03 36.4 Flag: "*" = Peak area was modified by background subtraction Page 3329 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:51:35 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621350.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621350 SOLID GAMMA31 0 01:00:00.00 1.50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry Detector geometry: Elapsed real time: Half .life ratio : Systematic Error Efficiencies at 3-0CT-2016 08:50:58 175.98 GRAM . CAN 0 01:00:06.18, 10.00 0.00 % Pec?-k Energy 0.2% No interference correction performed Page 3330 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : Gl203621350 Acquisition date 3-0CT-2016 08:50:58 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error AS-73 53.44 36 10.30* 5.699E+OO 2.612E-01 3.141E-01 200.62 PB-210 46.54 2 4.25* 5.454E+OO 3.158E-02 3.164E-02 3576.45 BI-214 609.32 2 45.49* 1.433E+OO l.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RN-222 609.32 2 45.49* l.433E+OO l.328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RA-226 609.32 2 45.49* l.433E+00 1. 328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72. 77 1764.49 ------15.30 5. 813E-01 ------Line Not Found ------TH-230 609.32 2 45.49* 1.433E+OO l.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4. 009E-Ol. 72. 77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------U-234 609.32 2 45.49* 1.433E+OO 1.328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01. 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------Flag: "*" = Keyline* Page 3331 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:51:36.77 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621350.CNF;l *
Acquisition date 3-0CT-2016 08:50:58 Sensitivity : 3.000 *
Detector ID GAM31 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.18 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl * *Sample ID
G1203621350 Sample Quantity 1.7598E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date : 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
Eff. File : 'DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;?'
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide AS-73 PB-210 BI-214 RN-222 RA-226 TH-230 U-234 Activity (pCi/GRAM 3.141E-01 3.164E-02 l.328E-02 1.328E-02 l.328E-02 1.328E-02 1.328E-02 Cnt uncert ( 1. 96-sigma) 6.176E-01 1.109E+OO 8.955E-02 8.955E-02 8.955E-02 8.955E-02 8.955E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 Page 3332 of 5809 Key-Line Activity (pCi/GRAM 3.192E-01 -3.592E-03 O.OOOE+OO 1. 400E-03 -3.065E-01 -5. 700E-03* 3.865E-02 2.452E-01 8.034E-03 2.805E-02 o. *oooE+oo -7.439E-03 l.836E-02 1.914E-02 -1.436E-02

-1.288E-02 4.670E-01 -2.636E-02 4.532E-03 -1. 491E+Ol 1. 672E-01 4.340E-02 -1. 712E+Ol K.L. Cnt Uncert ( 1. 96-sigma) 3.357E-01 3.315E-02 6.647E+08 2.822E-02 4.013E-01 3.058E-02 6.426E-02 3.834E-01 3.087E-02 3. 965E-02 l.398E+41 1. 511E-02 6.225E-02 3.492E-02 8. 718E-02 8.860E-01 1.119E-01 3.091E-02 4.397E+Ol 2.487E-01 5.757E-02 9.643E+OO MDA (pCi/GRAM 4.265E.:_01 8.948E-01 1. 2 64E-01 1.264E-01 1.264E-01 1. 2 64E-01 1.264E-01 MDA (pCi/GRAM 7.599E-01 7.002E-02 O.OOOE+OO 7.048E-02 8.243E-01 6.534E-02 1.635E-01 8.556E-01 6.749E-02 9.091E-02 O.OOOE+OO 2.905E-02 8.673E-02 l.525E-01 6.679E-02 l.630E-01 2.219E+OO 2.179E-Ol 6.271E-02 8.724E+Ol 6.368E-01 l.378E-01 l.474E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SR-85 -9.700E-02 5.458E-02 8. 341E-02 NOT IDENT. RB-86 3.865E-Ol 7.697E-01 l.862E+OO NOT IDENT. Y-88 1.552E-03 3.319E-02 8.264E-02 NOT IDENT. Y-91 -4.665E+OO 1.229E+01 2.485E+Ol NOT IDENT. NB-94 5.045E-02 6.744E-02 7.033E-02 FAIL ABUN NB-95 4.156E-02 3.015E-02 8.291E-02 NOT IDENT. NB-95M 1.991E-02 9.302E-02 1. 864E-01 NOT IDENT. ZR-95 4.506E-02 6.228E-02 1.485E-01 NOT IDENT. NB-97 O.OOOE+OO 9.852E+40 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 9.093E+08 O.OOOE+OO SHORT HLIF M0-99 -3.081E+Ol 4.615E+Ol 7. 911E+Ol NOT IDENT. TC-99M O.OOOE+OO 6.015E+23 O.OOOE+OO SHORT HLIF RH-101 3.524E-03 1.662E-02 3.538E-02 NOT IDENT. RH-102 2 .133E-02 3.833E-02 9.209E-02 NOT IDENT. RU-103 2.408E-02 3.125E-02 7.666E-02 FAIL ABUN RH-106 5.307E-02 2.699E-01 5.795E-01 NOT IDENT. RU-106 5.307E-02 2.699E-01 5.795E-01 NOT IDENT. AG-108M 8.855E-03 2.375E-02 4.941E-02 NOT IDENT. CD-109 -1.024E-01 3.376E-01 6.878E-01 NOT IDENT. AG-llOM 1.994E-02 3.936E-02 9.531E-02 NOT IDENT. SN-113 -9.468E-03 3.346E-02 6.481E-02 NOT IDENT. CD-115 -3.537E+Ol 4.899E+Ol 8. 714E+Ol NOT IDENT. SN-117M 1.612E-02 4.783E-02 l.003E-01 NOT IDENT. TE-123M 1. 619E-02 1. 7 64E-02 3.994E-02 NOT IDENT. SB-124 5.479E-02 8.481E-02 2.295E-01 NOT IDENT. SB-125 -1.106E-02 6.651E-02 1.377E-01 NOT IDENT. TE-125M 2.479E-02 5.160E+OO 1. 079E+Ol NOT IDENT. I-12El 9.312E-02 2.072E-01 4.891E-01 NOT IDENT. SB-126 -8.453E-02 1.438E-01 2.550E-01 NOT IDENT. SN-126 -2.219E-03 3.158E-02 6.630E-02 FAIL ABUN SB-127 -1. 671E+OO 3.741E+OO 6.894E+OO NOT IDENT. I-131 2. 471E-02 1.526E-01 3.312E-01 NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -2.105E+OO 1.983E+OO 3.185E+OO NOT IDENT. BA-133 7.285E-03 2.942E-02 6.533E-02 NOT IDENT. I-133 O.OOOE+OO 5.019E+05 O.OOOE+OO SHORT HLIF CS-134 1.823E-02 3.484E-02 7.903E-02 FAIL ABUN CS-135 -l.955E-02 l.207E-01 2.270E-01 NOT IDENT. I-135 O.OOOE+OO 4.139E+22 O.OOOE+OO SHORT HLIF CS-136 2.886E-03 1.249E-01 2.698E-01 NOT IDENT. BA-137M 2.648E-02 2.396E-02 6.339E-02 NOT IDENT. CS-137 2.797E-02 2. 531E-02 6.697E-02 NOT IDENT. CE-139 -2.293E-02 l.862E-02 3.021E-02 NOT IDENT. BA-140 3.489E-02 3.009E-01 6.447E-01 NOT IDENT. LA-140 -3.715E-03 9.130E-02 2.099E-01 NOT IDENT. CE-141 -2.091E-02 4.305E-02 7.643E-02 NOT IDENT. CE-143 O.OOOE+OO 1.850E+03 O.OOOE+OO SHORT HLIF CE-144 4.573E-02 1.151E:-01 2.477E-01 NOT IDENT. PM-144 6.831E-03 2.977E-02 5.888E-02 NOT IDENT. PR-144 5.181E-01 2.237E+OO 4.425E+OO NOT IDENT. PM-146 7.788E-03 3.754E-02 8.018E-02 NOT IDENT. ND.-14 7 l.559E-01 5.305E-01 l.235E+OO NOT IDENT. PM-147 2.632E+02 3.763E+02 8.582E+02 NOT IDENT. PM-149 2.685E+02 3.623E+02 8. 871E+02 NOT IDENT. EU-150 -1.003E-03 2.085E-02 3. 981E-02 NOT IDENT. EU-152 7.826E-02 6.709E-02 1.670E-01 NOT IDENT. GD-153 -5.142E-03 4.189E-02 8.624E-02 NOT IDENT. EU-154 -7.019E-03 9.461E-02 2.013E-01 FAIL ABUN EU-155 1.538E-02 4.702E-02 1.039E-01 NOT IDENT. TB-160 -6.873E-03 l.069E-01 2.338E-01 FAIL ABUN H0-166M 8.549E-03 5.779E-02 l .114E-01 NOT IDENT. TM-171 6.925E-01 4.164E+OO 8.585E+OO NOT IDENT. HF-172 -3.697E-02 l.130E-01 2.215E-01 FAIL ABUN LU-172 -l.494E-02 4.600E-02 9.335E-02 FAIL ABUN *LU-176 9.537E-04 l.815E-02 3.933E-02 NOT IDENT. HF-181 1. 492E-02 3.663E-02 8.333E-02 NOT IDENT. TA-182 -4.265E-02 1.358E-01 2.710E-01 FAIL ABUN RE-183 -2.075E-02 7.051E-02 l.432E-01 NOT IDENT. RE-184 1. 816E-02 1.288E-01 2.823E-01 NOT IDENT. W-188 -l.002E+OO 4.692E+OO 9.480E+OO FAIL ABUN IR-192 -2.401E-02 2.859E-02 5.361E-02 FAIL ABUN HG-203 -1.315E-02 3.176E-02 5.701E-02 NOT IDENT. BI-207 1. 611E-02 2.576E-02 7.357E-02 FAIL ABUN TL-208 1. 739E-02 3.273E-02 7.812E-02 NOT IDENT. BI-211 -1.654E-01 1.816E-01 3.525E-01 NOT IDENT. PB-211 -2. lOlE-01 5.907E-01 1.035E+OO NOT IDENT. BI-212 -1.201E-02 3.035E-01 6.548E-01 NOT IDENT. PB-212 -2.936E-02 4. 572E-02 8. 696E-02 NOT IDENT. Page 3333 of 5809 PB-214 5.843E-03 6.678E-02 1.460E-01 FAIL ABUN RN-219 l.143E-01 2.486E-01 5.883E-01 NOT IDENT. RA-223 -l.072E-01 4.903E-01 1.008E+OO FAIL ABUN RA-224 -9.417E-02 4.363E-01 8.415E-01 NOT IDENT. AC-227 -2. llOE-03 1.661E-01 3.281E-01 NOT IDENT. TH-227 -2. llOE-03 1.661E-01 3.281E-01 NOT IDENT. AC-228 9.592E-02 1.410E-01 3. OllE-01 FAIL ABUN RA-228 9.592E-02 1.410E-01 3. OllE-01 FAIL ABUN TH-228 -2.936E-02 4. 572E-02 8.696E-02 NOT IDENT .* TH-229 -1.597E-01 3.437E-01 5.754E-01 NOT IDENT. PA-231 -9.458E-02 2.899E-01 6.000E-01 NOT IDENT. TH-231 -1. 072E-01 4.903E-01 l.008E+OO FAIL ABUN TH-232 9.592E-02 l.LllOE-01 3. OllE-01 FAIL ABUN PA-233 -6.134E-03 4.837E-02 l.012E-01 NOT IDENT. PA-234 -l.013E-01 l.891E-01 3.699E-01 FAIL ABUN PA-234M 2.789E+OO 4.242E+OO 9.882E+OO NOT IDENT. TH-234 8.671E-01 . 1. 256E+OO 1.287E+OO FAIL ABUN U-235 2.736E-04 1.196E-01 2.296E-01 NOT IDENT. NP-237 -6.134E-03 4.837E-02 1.012E-01 NOT IDENT. NP-238 O.OOOE+OO l.091E+02 0.000E+OO SHORT HLIF U-238 8.671E-01 1.256E+OO 1.287E+OO FAIL ABUN NP-239 -8.259E-02 l.465E-01 2.802E-01 NOT IDENT. PU-239 -1.068E+Ol 1.757E+02 3.606E+02 NOT IDENT. AM-241 5.273E-02 5.486E-02 1.138E-01 NOT IDENT. AM-243 5.730E-03 2.103E-02 4.489E-02 NOT IDENT. CM-243 2. 968E-03 5.081E-02 1. 07 5E-01 NOT IDENT. BK-247 O.OOOE+OO 5.464E-02 l.077E-01 NOT IDENT. CM-2'47 1. 874E-03 2.444E-02 5.355E-02 NOT IDENT. CF-249 -2.265E-02 2.734E-02 4.984E-02 NOT IDENT. CF-251 -8.210E-02 7. 8 61E-02 1.312E-01 NOT IDENT. ANH-511 -9.288E-02 5.292E-02 1.075E-01 NOT IDENT. Page 3334 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:51:34.86 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error AS-73 53.44 36 10.30* 5.699E+OO 2.612E-01 3.141E-01 200.62 PB-210 46.54 2 4.25* 5.454E+OO 3.158E-02 3.164E-02 3576.45 BI-214 609.32 2 45.49* 1.433E+OO 1.328E-02 1.328E-02 688.26 1120. 29 12 14.92 8.735E-Ol 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5. 813E-01 ------Line Not Found ------RN-222 609.32 2 45.49* 1.433E+OO 1.328E-02 l.328E-02 688.26 1120. 29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RA-226 609.32 2 45.49* l.433E+OO 1. 328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------TH-230 609.32 2 45.49* l.433E+OO l.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4:009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------U-234 609.32 2 45.49* 1.433E+OO 1. 328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 '72. 77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------"*" = Key line Page 3335 of 5809 Summary of Nuclide Activity Sample ID : G1203621350 Acquisition date Page : 2 3-0CT-2016 08:50:58 Total number of lines in spectrum 17 Number of unidentified lines 6 Number of lines tentatively identi.fied by NID 11 Nuclide Type : Nuclide AS-73 PB-210 BI-214 RN-222 RA-226 TH-230 U-234 Hlife 80.30D 22.20Y 1600.00Y 1600.00Y 1600. OOY 7.54E+04Y 2.45E+05Y Decay 1. 20 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected Decay Corr pCi/GRAM pCi7GRAM 2.612E-01 3.141E-01 3.158E-02 3.164E-02 l.328E-02 1. 328E-02 1. 328E-02 1.328E-02 .1. 328E-02 1.328E-02 1. 328E-02 1.328E-02 l.328E-02 l.328E-02 ------------------3. 591E-01 4.122E-01 3.591E-01 4.122E-01 64.71% Decay Corr 2-Sigma Error 6.302E-01 113.lE-02 9.138E-02 9.138E-02 9.138E-02 9.138E-02 9.138E-02 Manually accepted 2-Sigma %Error 200.62 3576.45 688.26 688.26 688.26 688.26 688.26 Flags: "K" Keyline not found "E" = Manually edited "M" "A" Nuclide specific abn. limit Page 3336 of 5809 Flags Unidentified Energy *Lines Page : 3 Sample ID : G1203621350 Acquisition date : 3-0CT-2016 08:50:58 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 62.87 42 174 1. 89 125.37 122 7 8.02E-03 **** 5.59E+OO T 0 187.22 23 61 6.25 373.88 366 18 4.98E-03 **** 3.89E+OO 0 296.25 13 29 1. 89 591. 79 586 9 2.85E-03 **** 2.66E+OO T 0 338 .11 20 9 0.93 675.45 671 8 4.71E-03 84.5 2.37E+OO T 0 397 .11 13 10 3.32 793.37 788 9 2. 96E-03 **** 2.06E+OO 0 408.80 10 25 1.17 816.72 813 11 2. 31E-03 **** 2. OlE+OO 0 416.83 27 13 5.28 832.78 825 15 6.38E-03 75.9 1.97E+OO 0 437.75 10 7 1. 73 874.59 871 8 2.40E-03 **** l.89E+OO 0 483.85 14 9 1. 86 966.73 960 10 3.42E-03 **** 1.74E+OO 0 569.56 15 5 3.28 1138.04 1133 9 3.75E-03 78.6 1. 52E+OO T 0 702.13 15 16 1. 58 1403. oo. 1396 15 3.84E-03 **** 1.28E+OO T 0 873.87 8 2 0.69 1746.26 1743 6 2.lOE-03 88.8 1.07E+OO T 0 911. 55 6 2 o. 71 1821.58 1817 8 1. 59E-03_ **** 1. 03E+OO T Flags: "T" = Tentatively associated Page 3337of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:51:48.60 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621350.CNF;l *
Acqbisition date 3-0CT-2016 08:50:58 Sensitivity 3.000 *
Detector ID GAM31 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.18 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID Gl203621350 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN'.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide AS-73 PB-210 BI-214 RN-222 RA-226 TH-230 U-234
Le (pCi/GRAM l.999E-01 4.194E-01 5. 396E-02 5. 396E-02 5. 396E-02 5.396E-02 5.396E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 Page 3338 of 5809 Le (pCi/GRAM 3.362E-01 2.738E-02 O.OOOE+OO 2.497E-02 3.331E-01 2.593E-02 6.632E-02 3. 851E-01 2. 811E-02 3.887E-02 O.OOOE+OO 1.295E-02 3.685E-02 5.980E-02 2.554E-02 6.733E-02 8.944E-01 9.282E-02 2.729E-02 3.931E+Ol 2.579E-01 5.910E-02 6.523E+00 3.690E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 PB-214 Page 3339 of 5809 7.630E-01 2.928E-02 8.869E+OO 3.046E-02 3.510E-02 8.343E-02 6. 271E-02 O.OOOE+OO 0.000E+OO 3.065E+Ol O.OOOE+OO 1. 576E-02 3.823E-02 3.259E-02 2.449E-01 2.449E-01 2 .117E-02 3.106E-01 3.945E-02 2.725E-02 3.294E+Ol 4.516E-02 1.802E-02 8.890E-02 5.807E-02 4.804E+OO 2.014E-01 9.785E-02 2.993E-02 *2. 857E+OO l.441E-01 O.OOOE+OO 1. 37 4E+OO 2.827E-02 O.OOOE+OO 3.333E-02 1. OOlE-01 O.OOOE+OO l.102E-01 2.670E-02 2.820E-02 l.303E-02 2.724E-01 7.436E-02 3. 371E-02 O.OOOE+OO l.113E-01 2.455E-02 l.845E+OO 3.494E-02 5.062E-01 3.837E+02 3.842E+02 l.722E-02 7.355E-02 3.869E-02 7.908E-02 4.609E-02 9.409E-02 4.690E-02 4.045E+OO 9.909E-02 3.591E-02 1. 711E-02 3.551E-02 1. 049E-01 6.749E-02 l.184E-01 4.036E+OO 2.317E-02 2.478E-02 2.807E-02 3.428E-02 1.555E-01 4.373E-01 2.549E-01 3.903E-02 6.544E-02 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT !DENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN** NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN RN-219 RA-223 RA-224 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-2*34 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3340 of 5809 2.486E-01 4.411E-01 3.730E-01 1.424E-01 1. 424E-01 1.283E-01 1.283E-01 3.903E-02 2.502E-01 2.559E-01 4. 411E-01 1.283E-01 4.429E-02 l.356E-01 4.205E+OO 6.122E-01 l.023E-01 4.429E-02 0.000E+OO 6.122E-01 l.243E-01 1. 596E+02 5.373E-02 2.069E-02 4.788E-02 4.679E-02 2.260E-02 2.049E-02 5.659E-02 5.009E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT iDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT I.DENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Report Generated 03-0CT-2016 09:51:53.99 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621350.CNF;l *
Acquisition date 3-0CT-2016 08:50:58 Sensitivity : 3.000 *
Detector ID GAM31 . Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.18 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID Gl203621350 Analyst initials.: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM *
Quantity Err(%) : 1.1365E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid.
Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM AS-73 PB-210 BI-214 RN-222 RA-226 TH-230 U-234 3.141E-01 3.164E-02 l.328E-02 l.328E-02 l.328E-02 L 328E-02 l.328E-02 Act Error ( 1. 96-sigma) 6.210E-01 1.109E+OO 8.955E-02 8.955E-02 8.955E-02 8.955E-02 8.955E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40. SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82
RB-83 KR-85 Page 3341of5809 Key-Line Activity (pCi/GRAM 3.192E-01 -3.592E-03 2.666E+08 l.400E-03 -3.065E-01 -5.700E-03 3.865E-02 2.452E-01 8.034E-03 2.805E-02 1. OO'OE+41 -7.439E-03 l.836E-02 l.914E-02 -1.436E-02 .:..l.288E-02 4.670E-01 -2.636E-02 4.532E-03 -l.491E+Ol l.672E-01 4.340E-02 -1.712E+Ol K.L Act error ( 1. 96-sigma) 3.360E-01 3.315E-02 6.648E+08 2.822E-02 4.017E-01 3.058E-02 6.427E-02 3.835E-01 3.087E-02 3.967E-02 1.399E+41 l.512E-02 3.933E-02 6.227E-02 3.492E-02 8.718E-02 8.862E-01 l .119E-01 3.091E-02 4.493E+Ol 2.488E-01 5.788E-02 9.669E+OO TPU ( 1 . 96-sigma ) 6.210E-01 1.109E+OO 8.955E-02 8.955E-02 8.955E-02 8.955E-02 8.955E-02 TPU ( 1. 96-sigma) 3.655E-01 3.319E-02 6.756E+08 2.822E-02 4.248E-01 3.068E-02 6.659E-02 3.991E-01 3.108E-02 4 .164E.:._02 O.OOOE+OO l.548E-02 4.019E-02 6.286E-02 3.551E-02 8.737E-02 9.108E-01 1.125E-01 3.098E-02 4.543E+Ol 2.600E-01 6.109E-02 1.237E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT *IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

SR-85 -9.700E-02 5.472E-02 7.005E-02 NOT IDENT. RB-86 3.865E-01 7.699E-01 7.893E-01 NOT IDENT. Y-88 l.552E-03 3.319E-02 3.320E-02 NOT IDENT. Y-91 -4.665E+OO 1.229E+Ol 1. 247E+Ol NOT IDENT. NB-94 5.045E-02 6.748E-02 7.121E-02 FAIL ABUN NB-95 4.156E-02 3.020E-02 3.554E-02 NOT IDENT. NB-95M l.991E-02 9.304E-02 9.347E-02 NOT IDENT. ZR-95 4.506E-02 6.231E-02 6.554E-02 NOT IDENT. NB-97 -l.OOOE+41 9.861E+40 0.000E+OO SHORT HLIF ZR-97 -2.172E+08 9.093E+08 9.146E+08 SHORT HLIF M0-99 -3.0BlE+Ol 4.618E+Ol 4.822E+Ol NOT IDENT. TC-99M -2.273E+23 6. 01'9E+23 O.OOOE+OO SHORT HLIF RH-101 3.524E-03 l.663E-02 l.671E-02 NOT IDENT. RH-102 2 .133E-02 3.837E-02 3.956E-02 NOT IDENT. RU-103 2.408E-02 3.127E-02 3.310E-02 FAIL ABUN RH-106 5.307E-02 2.699E-01 2.710E-01 NOT IDENT. RU-106 5.307E-02 2.699E-01 2.710E-01 NOT IDENT. AG-108M 8.855E-03 2.375E-02 2.408E-02 NOT IDENT. CD-109 -1.024E-01 3.377E-01 3.408E-01 NOT IDENT. AG-llOM l.994E-02 3.937E-02 4.038E-02 NOT IDENT. SN-113 -9.468E-03 3.347E-02 3.374E-02 NOT IDENT. CD-115 -3.537E+Ol 4.904E+Ol 5.156E+Ol NOT IDENT. SN-ll 7M 1.612E-02 4.784E-02 4.839E-02 NOT IDENT. TE-123M 1. 619E-02 1. 765E-02 l.910E-02 NOT IDENT. SB-124 5.479E-02 8.486E-02 8.838E-02 NOT IDENT. SB-125 -1.106E-02 6. 651E-02 6.670E-02 NOT IDENT. TE-125M 2.479E-02 5.160E+OO 5.160E+OO NOT IDENT. I-126 9.312E-02 2.073E-01 2 .115E-01 NOT IDENT. SB-126 -8.453E-02 l.-440E-01 l.490E-01 NOT IDENT. SN-126 -2.219E-03 3.158E-02 3.159E-02 FAIL ABUN SB-127 -1. 671E+OO 3.745E+OO 3.820E+OO NOT IDENT. I-131 2. 471E-02 1.526E-01 l.530E-01 NOT IDENT. I-132 l.OOOE+41 3.056E+41 0.000E+OO SHORT HLIF TE-132 -2.105E+OO 1.991E+OO 2.206E+OO NOT IDENT. BA-133 7.285E-03 2.942E-02 2. 960E-02 NOT IDENT. I-133 1. 472E+05 5.024E+05 5.068E+05 SHORT HLIF CS-134 l.823E-02 3.485E-02 3.580E-02 FAIL ABUN CS-135 -l.955E-02 l.207E-01 1. 210E-01 . NOT IDENT. I-135 9.213E+21 4.163E+22 o*. OOOE+OO SHORT HLIF CS-136 2.886E-03 1.249E-01 1. 249E-01 . NOT IDENT. BA-137M 2.648E-02 2.399E-02 2.679E-02 NOT IDENT. CS-137 2.797E-02 2.534E-02 2.831E-02 NOT IDENT. CE-139 -2.293E-02 1.918E-02 2.179E-02 NOT IDENT. BA-140 3.489E-02 3.009E-01 3.013E-01 NOT IDENT. LA-140 -3.715E-03 9.130E-02 9.132E-02 NOT IDENT. CE-141 -2.091E-02 4.306E-02 4.408E-02 NOT IDENT. CE-143 9.909E+02 1. 851E+03 l.904E+03 SHORT HLIF CE-144 4.573E-02 1.151E-01 1.170E-01 NOT IDENT. PM-144 6. 831E-03 2.978E-02 2.993E-02 NOT IDENT. PR-144 5.181E-01 2.237E+OO 2.249E+OO NOT IDENT. PM-146 7.788E-03 3.754E-02 3.770E-02 NOT IDENT. ND-147 1.559E-01 5.306E-01 5.352E-01 NOT PM-147 2.632E+02 3.765E+02 3.947E+02 NOT IDENT. PM-149 2.685E+02 3. 641E+02 3.837E+02 NOT IDENT. EU-150 -1.003E-03 2.085E-02 2.086E-02 NOT IDENT. EU-152 7.826E-02 6. 723E-02 7.593E-02 NOT IDENT. GD-153 -5.142E-03 4.189E-02 4 .196E-02 NOT IDENT. EU-154 -7.019E-03 9.461E-02 9.466E-02 FAIL ABUN EU-155 l.538E-02 4.703E-02 4.754E-02 NOT I DENT.* TB-160 -6.873E-03 1.069E-01 1.070E-01 FAIL ABUN H0-166M 8.549E-03 5.779E-02 5.792E-02 NOT IDENT. TM-171 6.925E-01 4.165E+OO 4.176E+OO NOT IDENT. HF-172 -3.697E-02 1.132E-01 l.144E-01 FAIL ABUN LU-172 -1.494E-02 A. 602E-02 4. 651E-02 FAIL ABUN LU-176 9.537E-04 l.815E-02 1.815E-02 NOT IDENT. HF-181 1. 492E'-02 3.663E-02 3.725E-02 NOT IDENT. TA-182 -4.265E-02 1.358E-01 1. 371E-01 FAIL ABUN RE-183 -2.075E-02 7.054E-02 7 .116E-02 NOT IDENT. RE-184 l.816E-02 1.288E-01 1.290E-01 NOT IDENT. W-188 -l.002E+00 4.693E+OO 4.715E+OO FAIL ABUN IR-192 -2.401E-02 2.861E-02 3.059E-02 FAIL ABUN HG-203 -l.315E-02 3 .176E-02 3.231E-02 NOT IDENT. BI-207 l.611E-02 2.577E-02 2. 677E-02 . FAIL ABUN TL-208 1.739E-02 3.274E-02 3.366E-02 NOT IDENT. BI-211 -l.654E-01 1.817E-01 1. 964E-01 NOT IDENT. PB-211 -2.lOlE-01 5.908E-01 5.983E-01 NOT IDENT. BI-212 -1.201E-02 3.035E-01 3.036E-01 NOT IDENT. PB-212 -2.936E-02 4.574E-02 4.762E-02 NOT IDENT. Page 3342 of 5809 PB-214 5.843E-03 6.678E-02 6.683E-02 FAIL ABUN RN-219 l.143E-01 2.490E-01 2.542E-01 NOT IDENT. RA-223 -1. 072E-01 4.904E-01 4.928E-01 FAIL ABUN RA-224 -9.417E-02 4.363E-01 4.384E-01 NOT IDENT. AC-227 -2.llOE-03 l.661E-01 l.661E-01 NOT IDENT. TH-227 -2. llOE-03 l.661E-01 l.661E-01 NOT IDENT. AC-228 9.592E-02 l.410E-Ol l.475E-01 FAIL ABUN RA-228 9.592E-02 l.410E-01 1. 4 7 5E-01 FAIL ABUN TH-228 -2.936E-02 4.574E-02 4.762E-02 NOT IDENT. TH-229 -l.597E-01 3.438E-01 3.512E-01 NOT IDENT. PA-231 -9.458E-02 2.906E-Ol 2.937E-01 NOT IDENT. TH-231 -1. 072E-01 4.904E-01 4.928E-01 FAIL ABUN TH-232 9.592E-02 l.410E-01 1. 4 7 5E-01 FAIL ABUN PA-233 -6.134E-03 4.837E-02 4.845E-02 NOT IDENT. PA-234 -l.013E-01 2.218E-01 2.264E-01 FAIL ABUN PA-234M 2.789E+OO 4.244E+OO 4.426E+OO NOT IDENT. TH-234 8.671E-01 l.270E+OO l.329E+OO FAIL ABUN U-235 2.736E-04 l.196E-01 l .196E-01 NOT IDENT. NP-237 -6.134E-03 4.837E-02 4.845E-02 NOT IDENT. NP-238 l.300E+02 l.092E+02 l.239E+02 SHORT HLIF U-238 8 .. 671E-01 l.270E+OO l.329E+OO FAIL ABUN NP-239 -8.259E-02 1. 467E-01 l.513E-01 NOT IDENT. PU-239 -l.068E+Ol 1. 757E+02 1. 758E+02 NOT IDENT. AM-241 5.273E-02 5.500E-02. 5. 991E-02 NOT IDENT. AM-243 5.730E-03 2.103E-02 2 .119E-02 NQT IDENT. CM-243 2. 968E-03 5. 081E-02 5.082E-02 NOT IDENT. BK-247 O.OOOE+OO 5.464E-02 O.OOOE+OO NOT IDENT. CM-247 1. 874E-03 2.444E-02 2.4'45E-02 NOT IDENT. CF-249 -2.265E-02 2.740E-02 2.924E-02 NOT IDENT. CF-.251 -8.210E-02 7.915E-02 8.737E-02 NOT IDENT. ANH-511 -9.288E-02 5.305E-02 6.759E-02 NOT IDENT. Page 3343 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 61.1367 87.09 24.8846 136.47 26.2474 45.60 74.4062 87.57 23.9529 140.51 22.1901 46.54 74.6438 88.03 27.8134 143.76 19,!._1170 49. 72 83.2346 88.34 27.8325 144.24 23 .-3827 51. 35 82. 5072 88.47 26.8802 145.44 22.3612 51. 87 90.7905 89. 96 30.8201 152.43 23.6748 52.39 75.1992 90.64 69.4468 153.25 16.1616 52.97 75.3346 91.11 71.4476 154.21 26.9741 53.44 75.4442 92. 59 23.2454 156.02 29.2095 54.07 75.5899 93.35 28.1334 158.56 22.8024 57.36 0.0000 94.56 74.8887 159.00 16.2978 57.53 77.2653 94.65 74.9028 162.33 24.0175 57.98 96. 9305 94.67 74.9057 162.66 22.9367 59.27 78.5486 94.87 74.9374 163.33 16.3989 59.32 78.5596 97.43 27.3942 165.86 29.6231 59.54 69.0809 98.43 26.4698 176.31 20.0327 60. 96 . 82.5148 98.44 26.4702 176.60 20.0404 61.17 82.5636 99.53 21.6160 177.52 26.7532 62.93 69.4417 100 .11 26.5596 181. 07 . 25.3855 63.29 69.5109 102.03 16.7868 181. 52 22.4124 63.58 71. 0718 103.18 21.7734 184.41 20.2470 64.28 68.7940 103.37 21.7816 185. 72 20.2813 66.73 67.4261 105.21 16.8917 193.51 21. 2410 67.24 65.6922 105.31 16.8949 197.03 24.0005 67. 68 54.8071 106.12 22.8937 198.01 16. 0196 67 .. 75 54.8167 106.47 20.9170 201.83 21. 8423 69.67 39.4825 109. 2'8 22.0305 203.43 17.2771 70.83 48.8088 111. 00 31.1433 205.31 25. 3969 72. 81 40.7236 111. 76 32.1936 210.85 12.7819 72.87 40.7297 114.06 24.2477 215.65 28.0437 74.66 41. 8407 116. 30 16. 2311 222 .11 23.5422 74.82 41. 8569 116.74 28.4268 227.09 7.1020 74.97 44.6638 119.76 22.4560 227.38 18.9446 77 .11 40.2197 121.12 15.3477 228.16 27.2563 78.74 48.8274 121.22 15.3503 228.18 27.2570 79.69 27.2919 121. 78 21. 5116 235.69 21. 5068 80.12 31. 087 6 122.06 29.7208 235. 96 21. 5132 80.19 31.0926 122.92 27.7127 238.63 20:3761 80.57 33.0064 123.07 27. 7199 238.98 17.9855 81. 00 28.3195 123.68 25.6937 240.99 16.8224 81. 07 29.2683 125.81 28.8823 242.00 28.8691 81. 75 38.7706 127.23 19.6460 244.70 26.5386 83.79 24.7013 127.91 22.7743 252.40 12.1594 84.00 24.7132 129.30 20.7523 252.80 12.1645 85.43 31.4680 131. 20 23.9406 254.15 0.0000 86.55 37.2823 133.02 24.0125 256.23 14.6483 86.79 37.3019 133. 52 20.8975 260.90 18.3966 86.94 25.8333 136.00 24.1294 264.66 13.5412 Page 3344 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 13.5429 364.49 *13.4250 600.60 12.4507 265.00 14.7770 366.42 15.2375 602.52 0.0000 268.22 21.0005 372.51 14.4079 604. 72 9.9816 2 69. 4 6 23.4995 375.05 9.0222 607.14 7.8079 270.03 16.0873 377.52 12.6547 609.32 11. 4646 271.23 27.2563 383.85 9.9898 610.33 9.3849 273.65 18.6273 388.16 14.5768 614.28 11.2847 276.40 22.4116 388.63 16.4048 618.01 9.4215 277.37 11.2162 391. 69 12.0570 62 0. 3 6 9.4329 277.60 11.2187 400.66 6.8951 621. 93 8.3913 278.00 12.4701 401.81 6.4407 630.19 0.0000 279.20 19.9746 402.40 9.2049 631.29 4.2153 279.54 17.4833 404.85 13.8315 633.25 9.4937 279.70 17.4859 410.95 5.5564 634.78 4.2227 280.46 13.7490 413.71 5. 567i 635.95 8.4502 283.69 13.3727 414.70 5.5709 636.99 8.4544 284.31 15.8894 423.72 8.4088 645.85 7.4301 285.41 11. 7199 427.09 12.1737 657.76 11.7434 285.90 7.5377 427.87 11. 2434 657.90 0.0000 287.50 12.5815 433.94 8.4672 661.66 2.1392 290.67 13.1231 439.40 12.7472 664.57 0.0000 293.27 0.0000 453.88 13.3455 666.33 4.2878 295.22 16.0498 463.37 10.5499 666.50 3.2161 295. 96 16.0606 468.'07 14.4293 667.71 0.0000 298.58 12.7094 473.00 12.5443 677.62 8.6214 299.98 15.2703 475.06 12.5604 685.70 11.8992 300.09 15.2717 476.78 8.7050 695.00 6.5186 300 .13 15.2725 477.60 8.1288 696.49 6.5229 301.36 14.4399 482.18 7.7638 696. 51 6.5229 302.85 19.5621 487.02 13.1405 697.00 6.5244 304.50 12.7766 492.35 9.7654 697.30 9.7881 304.85 12.7805 497.08 4. 8966 697.49 9.7888 306.78 14.5094 505.52 20.6702 702.65 9. 8119 308.46 15.3856 507.63 0.0000 706.68 9.8302 311.90 18.0037 511. 00 28.6371 711. 68 6.5681 316.51 23.2399 514.00 48.4736 720.70 7.6938 319.41 18.9837 514.00 48.4736 721. 93 0.0000 320.08 18.9944 520.40 5.9578 722.78 2.2003 321.04 23.3306 520.69 5.9587 722.91 2.2004 323.87 19.0557 522.65 0.0000 723. 31 1.1004 325.23 16.4758 527.90 7.9782 724.19 2. 2017 328.76 15.6552 528.26 7.9798 727.33 4.4095 333.37 17.0248 529.59 3.9928 733.00 5.5257 333.97 14.4127 529.87 0.0000 735.93 4.4263 334.37 18.3494 531. 02 4.9951 737.46 3.3219 338.28 14.0254 537.26 9.0234 739.50 8.8662 338.32 14.0257 546.56 0.0000 747.24 8. 8 962 340.48 13.1723 552.55 12.1348 748.06 11.1243 340.55 13.1732 563.25 9.1545 752.31 5.5723 344.28 7.0469 569.33 4.0822 753.82 8.9215 345.93 15.8767 569.50 4.0825 756.73 4.4663 351.06 15.9415 569.70 4.0830 756.80 5.5831 351.93 9.7488 583.19 4.1126 763.94 8.9603 355.39 0.0000 584.27 12.3447 765.81 1.1209 356.01 11. 5586 595.83 13.4549 766.42 5.6061 Page 3345 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 6.7285 1002.74 6.4367 1678.03 0.0000 772.60 0.0000 1004.73 11. 0416 1690.97 1.1062 776.52 2.2520 1021.30 0.0000 1750.46 0.0000 777.92 4.5067 1025.87 0.0000 1764.49 3.3710 778.90 4.5085 1028.54 0.0000 1770.23 5.4000 783.70 4.5176 1037.84 7.4429 1771.35 3.6010 785.37 2.2603 1038.76 0.0000 1791.20 0.0000 792.07 9.0664 1046.59 6.5313 1808.65 1.8144 794.95 4.5386 1048.07 6.5343 1810.72 0.0000 795.86 5.6755 1049.04 10. 2715 1836.06 1.8245 801.95 7. 9653 1050.41 8.4078 810.06 2.2834 1063.66 0.9382 810.29 5.7088 1077.00 3.7690 810.45 5.7092 1077.34 2. 8271 810.76 6.8521 1085.87 4.7247 815.77 3.4329 1093.63 5.6836 818.51 5.7277 1099.45 2.8469 832.01 6.9104 1112. 07 6.6689 834.85 3.4591 1112. 84 6.6706 835. 71 3.4603 1115. 54 8.9015 836.80 0.0000 1120.29 9.1693 846.75 0.0000 1120.55 5.7316 846.77 5.7922 1121.30 3.0574 856.80 6.9778 1129. 67 6.7056 860.56 3.4940 1131.51 0.0000 871.09 8.4196 1147.95' 0.0000 873.19 1. 7 555 1173.23 4.8529 875.33 0.0000 1177.95 3.8877 879.38 6.1585 1189.05 1. 9503 880.51 7.9217 1204.77 3.9185 883.24 7.0486 1221.41 5.9059 884.68 4.4078 1231. 02 2. 9612 889.28 6.1816 1235.36 5.9297 894.76 7.0791 1238.28 3.9563 898.04 5.3159 1260.41 0.0000 900. 72 12. 4162 1271.87 4.9924 903.28 7.9893 1274.44 4.9957 911.20 8.0126 1274.54 4. 9960 1093.63 4.2749 1291.59 5.0195 923.98 0.0000 1298.22 0.0000 926.50 4.4765 1312 .11 2.0190 929 .11 4.4806 1332. 49 6.0901 937.49 5.3930 1362.66 0.0000 944.13 2.7029 1365.19 5.1190 946.00 5.4095 1368.63 0.0000 949.00 3.6101 1384.29 3.0868 954.55 0.0000 1408.01 4.1406 962.31 3. 6272 1457.56 0.0000 964.08 5.4441 1460.82 5.2448 966 .17 5.4481 1489.16 3.1686 968. 97 5.4534 1505.03 6.3618 983.53 2.7405 1584.12 5.4007 984.45 0.0000 1596.21 2.1663 996.26 9.1751 1620.50 2. 17 82 1001.03 4.5949 1621.92 1.0895 Page 3346 of 5809 VAX/VMS Nuclj.de Identi.fication Report Generated 3-0CT-2016 09: 54: 48. 92 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration : DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621351.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date : 10-DEC-2015 14:20:00 Acquisition date : 3-0CT-2016 08:53:50. Sample ID : G1203621351 Sample quantity : 1.41585E+02 GRAM Detector name : GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.64 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch .ID : 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 0 2 2 2 0 4 4 4 0 0 2 2 0 0 0 0 1 1 0 0 2 2 0 0 0 0 0 0 0 0 Page 3347 of 5809 Energy 32.25 39.16 41. 51 45.75* 62.89* 74.47* 76.75* 79.29 83.50* 86,89* 89.44 92.28* 185.83* 208.97 238.32* 241.49 269.53 277.75 294.91* 327.78 337.92*

339.92* 351.75* 409.97 427.28 431.57 463.04 510.54* 530. 4*8 583.24* 609.16* 623.99 661. 90 727.79 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 26 44 22 88 47 260 485 33 44 143 93 134 138 27 486 123 49 18 186 32 100 29 267 30 18 32 28 76 14 118 184 25 163 49 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 121 0.67 91 0.83 84 0.84 180 0.73 239 0.89 182 0.81 135 0.81 127 1. 04 112 1.39 172 . 1.11 185 1.29 174 1.30 134 1. 24 90 1.18 60 0.95 92 1. 37 83 0.93 68 1. 32 68 1.12 37 1. 08 54 1. 37 40 1. 37 76 1. 09 29 1.86 35 1. 62 35 1. 62 41 1.17 68 2.41 30 1.47 49 1.12 18 1.20 28 1. 74 81 1.42 30 2.05 66.34 80.15 84.85 93.31 127.57 150. 71 155.27 160.36 168.76 175.55 180.65 186.32 373.29 419.54 478.20 484.53 540.57 557.00 591.30 656.98 677.25 681.25 704.90 821.26 855.85 864.44 927.33 1022.27 1062.12 1167.58 1219.37 1249.01 1324.79 1456.49 63 76 76 88 124 147 147 147 167 172 172 172 369 416 474 474 536 552 587 654 671 671 700 818 848 848 922 1014 1054 1161 1215 1240 1319 1448 6 7.19E-03 70.8 12 1. 22E-02

35. 0 1*. 94E+OO 12 6.03E-03 70.2 10 2. 44E-02 31. 9 8 1.30E-02 '60. 7 20 7.23E-02 9.7 2.46E+OO 20 1.35E-01 5.9 20 9.28E-03 64.1 5 1.22E-02 40.1 20 3.97E-02 17.2 5.47E-01 20 2.59E-02 27.7 20 3.73E-02 20.7 11 3.83E-02 19.2 7 7.43E-03 62.5 15 l.35E-01 5.3 9.67E-01 15 3.40E-02 16.6 10 l.35E-02 37.8 8 5.00E-03-82.8 10 5.18E-02 11.2 6 8.82E-03 35.2 15 2.77E-02 16.0 6.51E+OO 15 7.98E-03 56.5 11 7.42E-02 8.9 7 8.43E-03 34.7 26 5.02E-03 68.2 2.73E+OO 26 8.90E-03 36.9 11 48.0 17 2.12E-02 30.0 11 4*. 02E-03 77. 8 10 3.28E-02 14.5 9 5.12E-02 8.6 14 7.05E-03 48.4 14 4.52E-02 14.1 17 1.37E-02 29.0 Peak Search Report (continued) Page : 2 Sample ID : Gl203621351 Ac*quisi tion date 3-0CT-2016 08:53:50 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 735.20 4 21 1. 06 1471. 28 1466 9 l.17E-03200.0 36 0 754.89 9 17 0.61 1510.64 1506 8 2.61E-03 83.9 37 0 786.51 25 26 6.39 1573.84 1565 17 6.97E-03 50.3 38 0 795.16 12 25 0.73 1591.13 1587 10 3.33E-03 83.l 39 0 806.54 10 21 0.50 1613.88 1608 9 2.85E-03 87.9 40 0 815.54 7 18 1. 27 1631.86 1626 10 1. 8 8E-03122. 7 41 0 892.23 15 6 1. 85 1785.15 1780 9 4.09E-03 40.9 42 0 911. 09* 112 12 1 . .4 7 1822.85 1815 16 3.12E-02 11. 8 43 0 920.75 7 11 1. 40 1842.14 1836 9 l.94E-03 94.4 44 2 934.55 25 4 2.10 1869.73 1863 19 6.81E-03 29.6 9.47E-01 45 2 938.82 14 0 2-.11 1878.27 1863 19 4.00E-03 28.7 46 0 964. 48 31 11 0.73 1929.55 1924 11 8.61E-03 27.4 47 3 969 .17 51 4 1. 91 1938.93 1935 16 1. 42E-02 15.3 l.40E+OO 48 3 973.23 14 1 2.35 1947.04 1935 16 4.02E-03 33.2 49 0 1035.77 4 21 1. 05 2072.04 2064 10 l.14E-03210.2 50 0 1121.15* 39 23 1. 61 2242.70 2237 13 1. 07E-02 31. 7 51 0 1156. 90 7 8 1.13 2314.17 2311 7 l.95E-03 74.2 52 0 1230.25 13 18 3.83 2460.78 2449 15 3.48E-03 80.4 53 0 1238.71 33 17 2.38 2477.68 2471 11 9.29E-03 29.2 54 0 1280.62 16 3 1. 95 2561.44 2558 7 4. 42E-03 31. 5 55 0 1377.31 17 0 1. 29 2754.71 2748 12 4.72E.:...03 24.3 56 0 1460.98* 471 4 1. 90 2921. 96 2913 15 1. 31E-01 4.7 57 0 1631. 06 12 0 1. 44 3261.92 3257 10 3.33E-03 28.9 58 0 1764.57 42 0 2.74 3528.79 3523 12 l.17E-02 15.4 Flag: "*" = Peak area was modified by background subtraction Page 3348 of 5809 VMS' Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:54:51 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621351.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 14:20:00 Gl203621351 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:53:50 141.59 GRAM Sample type. Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3349 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic* Error Efficiencies at Interfered ------------------Nuclide Lirie RA-224 240.99 TH-229 85.43 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.64 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G1203621351 Acquisition date 3-0CT-2016 08:53:50 ,, Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.244E+OO l.807E+Ol 1.807E+Ol 9.45 OK CD-109 88.03 3.70* 8. 913E+OO 1.624E+OO 2.540E+OO 61. 32 OK* SN-126 64.28 9.60 9.123E+OO . 3. 524E-01 3.524E-01 121. 4 7 OK 86.94 8.90 8 .. 913E+OO 6.751E-01 6.751E-01 61. 32 OK 87.57 37.00* 8. 913E+OO 1.624E-01 1.624E-01 61.32 OK CS-135 268.22 16.00* 5.040E+OO 3.559E-01 3.559E-01 75.52 OK BA-137M 661.66 89.90* 2.416E+OO 4.095E-01 4.173E-01 28.18 OK CS-137 661.66 85.10* 2.416E+OO 4.326E-01 4.408E-01 28.18 OK HG-203 70.83 3.69 9.006E+OO Line Not Found Absent 72. 87 6.19 8.-990E+OO Line Not Found Absent 279.20 81.56* 4.917E+OO 3.160E-03 2.654E-011398.35 OK TL-208 277.37 6.60 4.923E+OO Line Not Found <<INT Reject 583.19 85.00* 2.673E+OO 2.870E-01 2.870E-01 29.00 OK 860.56 . 12. 50 l.959E+OO Line Not Found Absent PB-210 46.54 4.25* 9.655E+OO 1.443E+OO 1.480E+OO 63. 86 OK BI-212 727 .. 33 6.67* 2.240E+OO 1. 795E+OO 1.795E+OO 57.93 OK 785.37 1.10 2.105E+OO 5.833E+OO 5.833E+OO 100.60 OK 1620. 50 1. 47 1.126E+OO Line Not Found Absent PB...:.212 74.82 10.28 8.980E+OO 1.122E+OO l.122E+OO 34.81 OK 77 .11 17.10 8. 967E+OO 2. 051E+OO 2. 051E+OO 11. 84 OK 238.63 43.60* 5.564E+00 1.192E+OO 1.192E+OO 10.57 OK 300.09 3.30 4.613E+OO Line Not Found Absent BI-214 609.32 45.49* 2.581E+OO 8. 641E-01 8.644E-01 17.29 OK 1120.29 14.92 1.575E+OO 8.566E-01 8.569E-01 63.42 OK 1764.49 15.30 1.032E+OO 1. 329E*+oo 1.329E+00 30.86 OK PB-214 74.82 5.80 8.977E+OO Line Not Found <<INT Reject 77 .11 9.70 8. 967E+OO 3.616E+OO 3.618E+OO 11. 84 OK 87.09 3.41 8.912E+OO Line Not Found <<INT Reject 242.00 7.25 5.497E+OO Line Not Found <<INT Reject 295.22 18.42 4.680E+OO 1.264E+OO 1.265E+OO 22.46 OK 351.93 35.60* 4.043E+OO 1.070E+OO 1.070E+OO 17.74 OK RN-222 609.32 45.49* 2.581E+OO 8.641E-01 8.644E-01 17.29 OK 1120.29 14.92 1.575E+OO 8.566E-01 8.569E-01 63.42 OK 1764.49 15.30 1.032E+OO l.329E+OO l.329E+OO 30.86 OK RA-224 240.99 4.10* 5.506E+OO 9.903E-01 9.903E-01 119. 26 OK RA-226 609.32 45.-49* 2.581E+OO 8.641E-01 8. 644E-01-17.29 OK 1120.29 1"4. 92 l.575E+OO 8.566E-01 8.569E-01 63.42 OK 1764.49 15.30 1.032E+OO l.329E+OO l.329E+OO 30.86 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27. 4.180E+OO l.223E+OO 1.223E+OO 31.98 OK 794.95 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911. 20 25.80* l.870E+00 l.236E+OO l.236E+OO 23.55 OK 968.97 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 OK RA-228 105.21 1.10 8.704E+OO *Line Not Found Absent 338.32 11. 27 4.180E+OO l.223E+00 l.223E+00 31. 98 OK 794.95 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* l.870E+OO 1.236E+00 1.236E+00 23.55 OK Page 3350 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G1203621351 Acquisition date 3-0CT-2016 08:53:50 *i Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 968. 97 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 OK TH-228 74.82 10.28 8.980E+OO l.122E+OO l.122E+OO 34.81 OK 77 .11 17.10 8. 967E+OO 2.051E+OO 2.051E+OO 11. 84 OK 238.63 43.60* 5.564E+OO 1.192E+OO l.192E+OO 10.57 OK 300.09 3.30 4.613E+OO Line Not Found Absent TH-229 85.43 14.70 8.913E+OO 4.088E-01 4.088E-01 61.32 OK 88.47 24.00 8.895E+OO 2.808E-01 2.808E-01 55.31 OK 193.51 4.41* 6. 511E+OO Line Not Found Absent 210.85 2.80 6 .116E+OO Line Not Found Absent TH-230 609.32 45.49* 2.581E+OO 8. 641E-01 8.641E-01 17.29 OK 1120. 29 14.92 1.575E:l-00 8.566E-01 8.566E-01 63.42 OK 1764.49 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 OK TH-232 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11.27 4.180E+OO 1.223E+OO l.223E+OO 31. 98 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.870E+OO 1.236E+OO l.236E+OO 23.55 OK 968. 97 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 OK TH-234 63.29 3.70* 9.123E+OO 9.143E-01 9.143E-01 121.47 OK 92.59 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 'OK U-234 609.32 45.49* 2. 581E+OO 8. 641E-01 8.641E-01 *17. 29 OK 1120. 29 14.92 1.575E+OO 8.566E-01 8.566E-01 63.42 OK 1764.49 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 OK U-235 89. 96 3.47 8.895E+OO 1.942E+OO 1.942E+OO 55.31 OK 93.35 5.60 8.870E+OO 1. 732E+OO 1.732E+OO 41. 31 OK 143.76 10. 96* 7.808E+OO Line Not Found Absent 163.33 5.08 7.279E+OO Line Not Found Absent 185. 72 57.20 6.697E+OO 2.183E-01 2.183E-01 38.33 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 *63. 29 3. 70.* 9.123E+OO 9.143E-01 9.143E-01 121. 4 7 OK 92.59 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 OK AM-243 43.53 5.90 9.491E+OO Line Not Found Absent 74.66 67.20* 8.980E+OO l.716E-01 l.716E-01 34.81 OK ANH-511 511. 00 100.00* 2.976E+OO 1.434E-01 l.434E-01 59.99 OK Flag: "*" Key line Page 3351of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:54:51.96 ******************************************"*************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621351.CNF;l *
Acquisition date. 3-0CT-2016 08:53:50 Sensitivity : 3.000 *
Detector ID GAM05 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.64 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Analyst initials: MXRl *
Sample ID Gl203621351 Sample Quantity 1.4159E+02 GRAM *
Batch Number 1596247 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLIO.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
Combined Activity-MDA Report NOTE: Not all "identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA NBclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM K-40 1.807E+Ol 1.673E+OO 5.312E-01 CD-109 2.540E+00 1.527E+OO 1.161E+OO SN-126 1.624E-01 9.759E-02 7.417E-02 CS-135 3.559E-01 2.634E-01 2.149E-01 BA-137M 4.173E-01 1.152E-01 6.556E-02 CS-137 4.408E-01 .1.217E-01 6.925E-02 HG-203 2.654E-01 3.637E+OO 3.759E+OO TL-208 2.870E-01 8.156E-02 6.791E-02 PB-210 1. 480E+OO 9.261E-01 5.346E-01 BI-212 1. 7 95E+OO 1.019E+OO 7.345E-01 PB-212 1.192E+OO l.234E-01 8.005E-02 BI-214 8.644E-01 l.465E-01 9. 851E-02 PB-214 1.070E+OO 1. 8 61E-01 1.207E-01 RN-222 8.644E-01 l.465E-01 9. 851E-02 RA-224 9.903E-01 1.157E+OO 8.588E-01 RA-226 8.644E-01 l.465E-01 9.851E-02 AC-228 1.236E+00 2.852E-01 2.059E-01 RA-228 1.236E+OO 2.852E-01 2.059E-01 TH-228 1.192E+OO 1.234E-01 8.005E-02 TH-229 -2.553E-01 4.379E-01 7. 714E-01 TH-230 8.641E-01 .1. 464E-01 9.848E-02 TH-232 1.236E+OO 2.852E-01 2.059E-01 TH-234 9.143E-01 1.088E+OO 8.558E-01 U-234 8.641E-01 1.464E-01 9.848E-02 U-235 7.009E-04 1.524E-01 2.858E-01 U-238 9.143E-01 1.088E+OO 8.558E-01 AM-243 l.716E-01 5.854E-02 4.948E-02 ANH-511 1.434E-01 8.432E-02 4.633E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 l.198E+00 l.188E+Ol 2.333E+Ol NOT IDENT. NA-22 -8.524E-03 4.026E-02 7.806E-02 NOT IDENT. Page 3352 of 5809 NA-24 O.OOOE+OO 1.218E+41 0.000E+OO SHORT HLIF AL-26 -1.819E-02 2.522E-02 3.887E-02 NOT IDENT. SC-46 2.973E-02 3.425E-01 6.047E-01 FAIL ABUN V-48 0.000E+OO l.099E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 3.698E+02 O.OOOE+OO SHORT HLIF MN-54 2.230E-02 5.728E-02 l.160E-01 NOT IDENT. C0-56 -6. 903E-02. 4. 712E-01 8.916E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 7.749E-03 3.492E-02 6.848E-02 NOT IDENT. C0-58 -l.150E-01 6.885E-01 1.013E+OO NOT IDENT. FE-59 2.591E+OO 6.204E+00 1.314E+Ol NOT IDENT. C0-60 6 .116E-03 3.470E-02 7.276E-02 NOT IDENT. ZN-65 -l.431E-01 2 .130E-01 3.177E-01 NOT IDENT. GE-68 2 .118E+OO 4. l 72E+OO NOT IDENT. AS-73 -1.457E-01 1.670E+OO 3.358E+OO NOT IDENT. AS-74 O.OOOE+OO 4.936E+03 0.000E+OO SHORT HLIF SE-75 l.219E-02 1.742E-01 3.234E-01 NOT IDENT. BR-77 O.OOOE+OO l.219E+37 . 0. OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.493E+02 O.OOOE+OO SHORT HLIF RB-83 -2.829E-01 5.702E-01 1.045E+OO FAIL ABUN KR-85 1.970E+OO 5.981E+OO 1.118E+Ol NOT IDENT. SR-85 2.0lOE-01 6.181E-01 1.155E+OO NOT IDENT. RB-86 O.OOOE+OO 2.381E+04 O.OOOE+OO SHORT HLIF Y-88 9.869E-02 l.990E-01 4.849E-01 NOT IDENT. Y-91 -4.783E+02 5.949E+02 1. 021E+03 NOT IDENT. NB-94 2. llOE-02 3.395E-02 6.849E-02 NOT IDENT. NB-95 -9.650E-01 9.129E-01 1.453E+OO NOT IDENT. NB-95M -1. 421E+OO 2.144E+00 3. 333E+O'O NOT IDENT. ZR-95 -4.361E-02 *1.500E+OO 2.538E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.475E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.007E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.684E+41 O.OOOE+OO SHORT HLIF RH-101 -2.626E-02 2.720E-02 4.825E-02 NOT IDENT. RH-102 1. 073E-02 4.765E-02 9.727E-02 NOT IDENT. RU-103 -3.534E+OO 4.9i8E+OO 8.768E+OO FAIL ABUN RH-106 2.090E-01 4.657E-01 9.522E-01 NOT IDENT. RU-106 2.090E-01 4.657E-01 9.522E-01 NOT IDENT. AG-108M -1.608E-02 2.313E-02 4.206E-02 NOT IDENT. AG-llOM -5.618E-02 8.945E-02 l.502E-01 FAIL ABUN SN-113 -7 . 3 7 3 E-0'2 1. 739E-01 3.317E-01 NOT IDENT. CD-115 O.OOOE+OO 1.474E+39 0.000E+OO SHORT HLIF SN-117M O.OOOE+OO 7.285E+04 0.000E+OO SHORT HLIF TE-123M -3.381E-02 1.057E-01 l.945E-01 NOT IDENT. SB-124 5.851E-01 1.573E+OO 3.832E+OO NOT IDENT. SB-125 1.226E-01 1.638E-01 2.028E-01 FAIL ABUN TE-125M 3.826E+Ol 2. 051E+o2 4.006E+02 NOT IDENT. I-126 O.OOOE+OO 7.802E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.085E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO l.410E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.679E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.222E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.054E+26 O.OOOE+OO SHORT HLIF BA-133 1. 321E-02 3.586E-02 6.805E-02 FAIL ABUN I-133 O.OOOE+OO 1.526E+41 O.OOOE+OO SHORT HLIF CS-134 4.753E-02 7.744E-02 1.062E-01 FAIL ABUN I-135 0.000E+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.302E+05 O.OOOE+OO SHORT HLIF CE-139 5.537E-04 9 .138E-02 l.721E-01 NOT IDENT. BA-140 O.OOOE+OO 9.242E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.833E+05 O.OOOE+OO SHORT HLIF CE-141 1.082E+Ol 1.897E+Ol 3.748E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 4.280E-02 2.800E-01 5. 411E-01 FAIL ABUN PM-144 -1.650E-02 5.341E-02 9.727E-02 NOT IDENT. PR-144 -1.460E+OO 4.631E+OO 8.426E+OO NOT IDENT. PM-146 2.852E-02 4.088E-02 8. 571E-02 FAIL ABUN ND-147 O.OOOE+OO 4.757E+07 O.OOOE+OO SHORT HLIF PM-147 -2.543E+02 6.036E+02 1.126E+03 NOT IDENT. PM-149 O.OOOE+OO 2 .111E+40 O.OOOE+OO SHORT HLIF EU-150 -1.118E-02 2.838E-02 4.399E-02 FAIL ABUN EU-152 1.583E-02 8.325E-02 1.542E-01 FAIL ABUN GD-153 -3.971E-02 l.225E-01 2.322E-01 NOT IDENT. EU-154 -1. 8 62E-02 9.932E-02 l.934E-01 NOT IDENT. EU-155 , 5.563E-02 8.219E-02 l.657E-01 FAIL ABUN TB-160 3.548E-01 1.808E+OO 3.530E+OO FAIL ABUN H0-166M -2.302E-02 5.423E-02 9.785E-02 FAIL ABUN TM-171 1.147E+OO 3.793E+OO 7.812E+OO NOT IDENT. Page 3353 of 5809 HF-172 1. 406E-01 1.800E-01 3. 641E-01 FAIL ABUN LU-172 3.597E-02 8.218E-02 l .. 708E-01 FAIL ABUN LU-176 -2.303E-02 2.340E-02 3.722E-02 FAIL ABUN HF-181 -2.095E+OO 4.058E+OO 7.444E+OO NOT IDENT. TA-182 l.355E-01 8.576E-01 1.568E+OO. FAIL ABUN RE-183 -2.948E-02 8.280E-01 1.657E+OO NOT IDENT. RE-184 l.334E+Ol 2.908E+Ol 5.875E+Ol NOT IDENT. W-188 9.998E+Ol 1.138E+02 2.104E+02 FAIL ABUN IR-192 1.234E-01 4.267E-01 7.979E-01 FAIL ABUN BI-207 l.032E-03 4.267E-02 8.643E-02 FAIL ABUN BI-211 0.000E+OO 5.125E-01 8.430E-01 FAIL ABUN PB-211 2.983E-01 6.093E-01 .1. 254E+OO FAIL ABUN RN-219 -1.275E-01 3.364E-01 6.381E-01 NOT IDENT. RA-223 -:-2.049E-01 6.432E-01 1. 013E+OO FAIL ABUN AC-227 2.618E-02 1.990E-01 3.709E-01 FAIL ABUN TH-227 2.618E-02 l.990E-01 3.709E-01 FAIL ABUN PA-231 -l.344E-01 4.492E-01 7.813E-01 NOT IDENT. TH-231 -2.049E-01 6.432E-01 1. 013E+OO FAIL ABUN PA-233 3.083E-02 5.582E-02 1. 074E-01 FAIL ABUN PA-234 1.892E-01 2.740E-01 5.727E-01 NOT IDENT. PA-234M -6.718E-01 4.014E+OO 7. 941E+OO NOT IDENT. NP-237 3.083E-02 5.582E-02 l.074E-01 FAIL ABUN NP-238 O.OOOE+OO 1.938E+41 O.OOOE+OO SHORT HLIF NP-239 -1.725E-01 1.917E-01 3.4.46E-01 FAIL ABUN PU-239 1.092E+02 2.525E+02 4.958E+02 NOT IDENT. AM-241 2.777E-02 4.648E-02 9.007E-02 NOT IDENT. CM-243 -2.004E-02 6.947E-02 1.323E-01 FAIL ABUN BK-247 1.205E-02 6.575E-02 l.145E-01 FAIL *ABUN CM-247 -4.604E-03 3.008E-02 5.856E-02 FAIL ABUN CF-249 2.627E-02 3. 0 68-E-02 6.637E-02 NOT IDENT. CF-251 -2.207E-02 9.952E-02 1.827E-01 NOT IDENT. Page 3354 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:54:49.80 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 452 10.66* 1.244E+OO 1.807E+Ol L 807E+Ol 9.45 CD-109 88.03 173 3.70* 8.913E+OO 2.789E+OO 4.363E+OO . 34. 45 SN-126 64.28 58 9.60 9.123E+OO 3.524E-01 3.524E-01 121.47 86.94 173 8.90 8.913E+OO 1.160E+OO l.160E+OO 34.45 87.57 173 37.00* 8. 913E+OO 2.789E-01 2.789E-01 34.45 CS-135 268.22 54 16.00* 5.040E+OO 3.559E-01 3.559E-01 75.52 BA-137M 661.66 168 89.90* 2.416E+OO 4.095E-01 4.173E-01 28.18 CS-137 661. 66 168 85.10* 2.416E+OO 4.326E-01 4.408E-"01 28.18 HG-203 70. 83 ------3.69 9.006E+OO ------Line Not Found ------72. 87 ------6.19 8.990E+OO ------Line Not Found ------279.20 20 81.56* 4.917E+OO 2.638E-02 2.215E+OO 165.55 TL-208 277.37 20 6.60 4.917E+OO 3.260E-01 3.260E-01 165.55 583.19 123 85.00* 2.673E+OO 2.870E-01 2.870E-01 29.00 860.56 ------12.50 1.959E+OO ------Line Not Found ------PB-210 46.54 112 4.25* 9.655E+OO 1.443E+OO 1. 480E+OO 63.86 BI-211 72.87 ------1. 23 8.990E+OO ------Line Not Found ------351.06 290 12.92* 4.043E+OO 2.948E+OO 2.948E+OO 17.74 BI-212 727. 33 51 6.67* 2.240E+OO 1.795E+OO 1.795E+OO 57.93 785.37 25 1.10 2.105E+OO 5.833E+OO 5.833E+OO 100.60 1620.50 ------1. 47 1.126E+OO ------Line Not Found ------PB-212 74.82 319 10.28 8.980E+OO 1.835E+OO 1.835E+OO 19.40 77 .11 593 17 .10 8. 967E+OO 2.051E+OO 2.051E+OO 11. 84 238.63 545 43.60* 5.564E+OO l.192E+OO 1.192E+OO 10.57 300.09 ------3.30 4.613E+OO ------Line Not Found ------BI-214 609.32 191 45.49* 2.581E+OO 8. 641E-01 8.644E-01 17.29 1120.29 38 14.92 1.575E+OO 8.566E-01 8.569E-01 63.42 1764.49 40 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 PB-214 74.82 319 5.80 8.980E+OO 3.252E+OO 3.253E+OO 19.40 77 .11 593 9.70 8. 967E+OO 3.616E+00 3.618E+OO 11. 84 87.09 173 3.41 8.913E+OO 3.026E+OO 3.028E+OO 34.45 242.00 137 7.25 5.506E+OO 1.824E+OO 1.825E+OO 33.13 295.22 206 18.42 4.680E+OO 1. 264E+OO 1.265E+OO 22.46 351. 93 290 35.60* 4.043E+OO 1.070E+OO 1.070E+OO 17.74 RN-222 609.32 191 45.49* 2.581E+OO 8.641E-01 8.644E-01 17.29 1120.29 38 14.92 1. 575E+OO 8.566E-01 8.569E-01 63.42 1764.49 40 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 RA-224 240.99 137 4.10* 5.506E+OO 3.226E+OO 3.226E+OO 33.13 RA-226 .. 609.32 191 45.49* 2.581E+OO 8. 641E-01 8.644E-01 17. 29 1120. 29 38 14.92 1. 57 5E+OO 8.566E-01 8.569E-01 63.42 1764-.49 40 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 109 11.27 4.180E+OO 1.223E+OO 1.223E+OO 31. 98 794.95 12 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 835. 71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 112 25.80* 1.870E+OO 1.236E+OO 1.236E+OO 23.55 968. 97 51 15.80 l.778E+OO 9.614E-01 9.614E-01 30.58 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------Page 3355 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G1203621351 Acquisition date 3-0CT-2016 08:53:50 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 338.32 109 11. 27 4.180E+OO 1.223E+OO 1.223E+OO 31. 98 794.95 12 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 112 25.80* 1. 870E+OO l.236E+00 1.236E+OO 23.55 968. 97 51 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 TH-228 74.82 319 10.28 8.980E+OO 1.835E+OO 1.835E+OO 19.40 77 .11 593 17.10 8. 967E+OO 2. 051E+OO 2.051E+OO 11. 84 238.63 545 43.60* 5.564E+OO 1.192E+OO 1.192E+OO 10.57 300.09 ------3.30 4.613E+OO ------Line Not Found ------TH-229* 85.43 173 14.70 8.913E+OO 7.021E-01 7. 021E-01 34.45 88.47 113 24.00 8.895E+OO 2.808E-01 2.808E-01 55.31 193.51 ------4.41* 6. 511E+OO ------Line Not Found ------210.85 ------2.80 6 .116E+OO ------Line Not Found ------TH-230 609.32 191 45.49* 2.581E+OO 8.641E-01 8.641E-01 17.29 1120.29 38 14.92 1.575E+OO 8.566E-01 8.566E-01 63.42 1764.49 40 15.30 1.032E+OO 1.329E+OO 1. 329E+OO 30.86 TH-232 105.21 ------1.10 8.704E+00 ------Line Not Found ------338.32 109 11.27 4.180E+OO 1.223E+OO 1.223E+OO 31. 98 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 112 25.80* 1.870E+OO 1.236E+OO 1.236E+OO 23.55 *968.97 51 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 TH-234 63. 29 58 3.70* 9.123E+OO 9.143E-01 9.143E-01 121.47 92.59 162 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 U-234 609.32 191 45.49* 2.581E+OO 8.641E-01 8. 641E-01 17. 29 1120.29 38 14.92 1.575E+OO 8.566E-01 8.566E-01 63.42 1764.49 40 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 U-235 89. 96 113 3.47 8.895E+OO 1.942E+OO 1.942E+OO 55.31 93.35 162 5.60 8.870E+OO 1.732E+OO 1.732E+00 41. 31 143.76 ------10. 96* 7.808E+OO ------Line Not Found ------163.33 ------5.08 7.279E+00 ------Line Not Found ------185.72 158 57.20 6.697E+00 2.183E-01 2.183E-01 38.33 205.31 ------5.01 6.238E+OO ------Line Not Found ------U-238 63.29 58 3.70* 9.123E+OO 9.143E-01 9.143E-01 121. 4 7 92.59 162 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 AM-243 43.53 ------5.90 9.491E+OO ------Line Not Found ------74.66 319 67.20* 8.980E+OO 2.807E-01 2.807E-01 19.40 ANH-511 511.00 80 100.00* 2.976E+OO 1.434E-01 1.434E-01 59.99 Flag: "*" Key line Page 3356 of 5809 Summary of Nuclide Activity Sample ID : Gl203621351 Acquisition date Page : 3 3-0CT-2016 08:53:50 Total number of lines in spectrum 58 Number of unidentified lines 16 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 46.59D l.41E+10Y 22.20Y 7.04E+08Y 1.41E+l0Y l.41E+10Y 1600. OOY 1600. OOY 1600.00Y 1.41E+10Y 1600. OOY l.41E+l0Y l.41E+l0Y 1.41E+10Y 7340.00Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1. 00E+09Y Qecay 1. 00 1. 56 1. 00 1. 00 1. 02 1. 02 84.0 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.807E+Ol 2.789E+OO 2.789E-01 3.559E-01 4.095E-01 4.326E-01 2.638E-02 2.870E-01 l.443E+OO 2.948E+OO 1. 795E+OO 1.192E+OO 8. 641E-01 l.070E+OO 8. 641E-01 3.226E+OO 8. 641E-01 1.236E+OO 1.236E+OO 1.192E+OO 2.808E-01 8.641E-01 1.236E+OO 9.143E-01 8. 641E-01 2.183E-01 9.143E-01 2.807E-01 l.434E-01 4.629E+Ol 4.629E+Ol Decay Corr pCi/GRAM 1.807E+Ol 4.363E+OO 2.789E-01 3.559E-01 4.173E-01 4.408E-01 2.215E+OO 2.870E-01 l.480E+OO 2.948E+OO 1. 795E+OO 1.192E+OO 8.644E-01 1. 070E+OO 8.644E-01 3.226E+OO 8.644E-01 1.236E+OO 1.236E+OO l.192E+OO 2.808E-01 8.641E-01 1.236E+OO 9.143E-01 8.641E-01 2.183E-01 9.143E-01 2.807E-01 l.434E-01 5. OllE+Ol 5. OllE+Ol 72. 41% Decay Corr 2-Sigma Error 0.171E+Ol 1.503E+OO 0. 961E-01 2.688E-01 l.176E-01 1.242E-01 3.667E+OO 0.832E-01 0.945E+OO 0.523E+OO l.040E+OO 0.126E+OO 1.495E-01 0.190E+OO 1.495E-01 l.069E+00 l.495E-01 0.291E+OO 0.291E+OO o .126E+oo* 1.553E-01. 1.494E-01 0.291E+OO ll. llE-01 l.494E-01 0.837E-01 11. llE-01 0.545E-01 0.860E-01 "M" Manually accepted 2-Sigma %Error 9.45 34.45 34.45 75.52 28.18 28.18 165.55 29.00 63. 86 17.74 57.93 10.57 17.29 17.74 17.29 33.13 17.29 23.55 23.55 10.57 55.31 17.29 23.55 121.47 17.29 38.33 121.47 19.40 59.99 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3357 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G1203621351 Acquisition date : 3-0CT-2016 08:53:50 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 32.25 34 158 0. 67 66.34 63 6 7.19E-03 **** 2 .13E+OO 1 39.16 57 116 0.83 80.15 76 12 1.22E-02 70.0 8.19E+OO 1 41. 51 28 107 0.84 84.85 76 12 6.03E-03 **** 9.lOE+OO 2 79.29 41 155 1. 04 160.36 147 20 9.28E-03 **** 8.95E+OO T 0 83.50 53 137 1. 39 168.76 167 5 l.22E-02 80.3 8.93E+OO T 0 208.97 30 102 1.18 419.54 416 7 7.43E-03 **** 6.16E;t-00 0 327.78 35 41 1. 08 656.98 654 6 8.82E-03 70.5 4.29E+OO T 1 339.92 31 44 1. 37 681.25 671 15 7.98E-03 **** 4.16E+00 T 0 409.97 33 31 1. 86 821. 26 818 7 8.43E-03 69.4 3.56E+OO T 2 427.28 19 37 1. 62 855.85 848 26 5.02E-03 **** 3.44E+OO T 2 431.57 34 37 1. 62 864.44 848 26 8.90E-03 73.7 3.41E+OO 0 463.04 30 43 1.17 927.33 922 11 7.82E-03 96. 0 3.22E+OO T 0 530.48 15 31 1. 47 1062.12 1054 11 4.02E-03 **** 2.88E+OO T 0 623.99 26 29 1. 74 1249.01 1240 14 7.05E-03 96. 8 2.53E+00 0 735.20 4 21 1. 06 1471.28 1466 9 l.17E-03 **** 2.22E+OO T 0 754.89 10 17 0.61 1510.64 1506 8 2. 61E-03 **** 2.18E+OO T 0 806.54 10 21 0.50 1613.88 1608 9 2.85E-03 **** 2.06E+OO 0 815.54 7 18 1. 27 1631.86 1626 10 1. 88E-03 **** 2.05E+OO T 0 892.23 15 6 1. 85 1785.15 1780 9 4*. 09E-03 81. 8 1. 90E+OO 0 920.75 7 11 1. 40 1842.14 1836 9 1. 94E-03 **** 1. 85E+OO 2 934.55 24 4 2.10 1869.73 1863 19 6.81E-03 59.2 1.83E+OO 2 938.82 14 0 2 .11 1878.27 1863 19 4.00E-03 57.4 1. 83E+OO T 0 964. 48 31 11 0.73 1929.55 1924 11 8.61E-03 54.8 1. 79E+OO T 3 973.23 14 1 2.35 1947.04 1935 16 4.02E-03 66.4 1.77E+OO 0 1035.77 4 21 1. 05 2072.04 2064 10 l.14E-03 **** 1. 68E+OO 0 1156.90 7 8 1.13 2314.17 2311 7 l.95E-03 **** l.53E+00 0 1230.25 12 18 3.83 2460.78 2449 15 3.48E-03 **** 1. 45E+OO T 0 1238.71 33 16 2.38 2477.68 2471 11 9.29E-03 58.4 1. 44E+00 T 0 1280.62 15 3 1. 95 2561.44 2558 7 4.42E-03 63.1 1. 40E+OO 0 1377. 31 16 0 1.29 2754.71 2748 12 4. 72E-03 48.5 1.31E+OO 0 1631. 06 11 0 1. 44 3261.92 3257 10 3.33E-03 57.7 l.12E+OO Flags: "T" = Tentatively associated Page 3358 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:55:04.27 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621351.CNF;l* * *Acquisition date 3-0CT-2016 08:53:50 Sensitivity : 3.000 *
Detector ID GAM05 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.64 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
Sample ID G1203621351 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : l.4159E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 . U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2 .113E-01 5.445E-01 3.478E-02 9.828E-02 2.935E-02 3.lOlE-02 l.723E+OO 3.073E-02 2.481E-01 3.184E-01 3.695E-02 4.302E-02 5.519E-02 4.302E-02 3. 965E-01 4.302E-02 8.789E-02 8.789E-02 3.695E-02 3.597E-01 4.300E-02 8.789E-02 4.053E-01 4.300E-02 l.341E-01 4.053E-01 2.348E-02 2.070E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3359 of 5809 Le (pCi/GRAM 1.058E+Ol 3.266E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95' NB-97 ZR-97 M0-99. TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB...:126 SB-127 I-131 I-132 TE-132 BA-133. I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE...:144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152. GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3360 of 5809 l.228E-02 2.576E-01 O.OOOE+OO O.OOOE+OO 5. 096E-02 3.927E-01 O.OOOE+OO 3.199E-02 4.411E-01 5.743E+OO 3.045E-02 l.378E-01 1. 791E+OO 1. 576E+OO 0.000E+OO l.479E-01 O.OOOE+OO O.OOOE+OO 4.616E-01 4.986E+OO 5.149E-01 O.OOOE+OO l.919E-01 4.467E+02 3.107E-02 6.411E-01 l.532E+OO l .114E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.253E-02 4.258E-02 3.874E+OO 4.256E-01 4.256E-01 l.863E-02 6.317E-02 l.474E-01 O.OOOE+OO O.OOOE+OO 9.044E-02 l.484E+OO 9.258E-02 l.885E+02 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.088E-02 O.OOOE+OO 4.776E-02 O.OOOE+OO O.OOOE+OO 8.024E-02 O.OOOE+OO O.OOOE+OO 1. 759E+Ol O.OOOE+OO 2.532E-01 4.305E-02 3. 728E+OO 3.903E-02 O.OOOE+OO 5.240E+02 0. OOOE+OO . 2.014E-02 7.008E-02 1. 091E-01 8.106E-02 7.822E-02 1. 54 7E+OO 4.300E-02 3.676E+OO 1. 711E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT I DENT .. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT I DENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL. ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3361 of 5809 7.575E-02 1. 686E-02 3.340E+OO 6.729E-01 7.826E-01 2.593E+Ol 9.768E+Ol 3.657E-01 3. 722E-02 4.075E-01 5.730E-01 2.882E-01 4.635E-01 l.705E-01 1.705E-01 3.605E-01 4.635E-01 4.938E-02 2.530E-01 3.473E+OO 4.938E-02 O.OOOE+OO l.611E-01 2.334E+02 4.273E-02 6.190E-02 5.237E-02 2.645E-02 3.018E-02 8.510E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL 'ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Genera.ted 03-0CT-2016 09: 55: 09. 89 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621351.CNF;l *
Acquisition date 3-0CT-2016 08:53:50 Sensitivity : 3.000 *
Detector ID GAM05 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.64 Half life ratio : ***** *
Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
Sample ID G1203621351 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.4159E+02 GRAM *
Quantity Err(%) : 1.4126E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry.Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 4-SEP-2016' 08:00:28 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) K-40 1.807E+Ol 1. 921E+OO 1.921E+OO CD-109 2.540E+OO 1.557E+OO 1.557E+OO SN-126 1.624E-01 9.918E-02 9.918E-02 CS-135 .3.559E-01 2.645E-01 2.645E-01 BA-137M 4.173E-01 1.166E-01 l.166E-01 CS-137 4.408E-01 1.232E-01 l.232E-01 HG-203 2.654E-01 3.643E+OO 3.643E+OO TL-208 2.870E-01 8.247E-02 8.247E-02 PB-210 1.480E+00 9.379E-01 9.379E-01 BI-212 1. 795E+OO 1.023E+OO 1.023E+OO PB-212 1.192E+OO 1.387E-01 l.387E-01 BI-214 8.644E-01 1. 511E-01 1. 511E-01 PB-214 1.070E+OO l.913E-01 l.913E-01 RN-222 8. 644E-01. 1. 511E-01 1. 511E-01 RA-224 9.903E-01 l.168E+00 l.168E+OO RA-226 8.644E-01 1. 511E-01 1. 511E-01 AC:..228 l.236E+OO 2. 921E-01 2. 921E-01 RA-228 1.236E+OO 2.921E-01 2. 921E-01 TH-228 1.192E+OO l.387E-01 l.387E-01 TH-229 -2.553E-01 4.381E-01 4.381E-01 TH-230 8. 641E-01 1. 511E-01 1. 511E-01 TH-232 1.236E+OO 2.921E-01 2. 921E-01 TH-234 9.143E-01 1.107E+OO l.107E+00 U-234 8.641E-01 1. 511E-01 l.511E-01 U-235 7.009E-04 1.524E-01 l.524E-01 U-238 9.143E-01 1.107E+OO l.107E+OO AM-243 1. 716E-01 6.106E-02 6.106E-02 ANH-511 1.434E-01 8.452E-02 8.452E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 1.198E+00 1.188E+Ol l.189E+Ol NOT* IDENT. NA-22 -8.524E-03 4.027E-02 4.045E-02 NOT IDENT. Page 3362 of 5809 NA-24 -l.000E+41 1.293E+41 O.OOOE+OO SHORT HLIF AL-26 -l.819E-02 2.525E-02 2.655E-02 NOT IDENT. SC-46 2.973E-02 3.425E-01 3.428E-01 FAIL ABUN V-48 -5.603E+03 1.100E+04 1.128E+04 SHORT HLIF CR-51 -3.415E+Ol 3.698E+02 3. 701E+02 SHORT HLIF MN-54 2.230E-02 5.729E-02 5.816E-02 NOT IDENT. C0-56 -6.903E-02 4. 712E-01 4. 722E-01 FAIL ABUN MN-56 -l.000E+41 7.515E+41 O.OOOE+OO SHORT HLIF C0-57 7.749E-03 3.493E-02 3.510E-02 NOT IDENT. C0-58 -l.150E-01 6.885E-01 6.904E-01 NOT IDENT. FE-59 2.591E+OO 6.206E+OO 6.315E+OO NOT IDENT. C0-60 6 .116E-03 3.470E-02 3.481E-02 NOT IDENT. ZN-65 -1.431E-01 2.130E-01 2.226E-01 NOT IDENT. GE-68 -2.938E-01 2 .118E+OO
2.122E+OO NOT IDENT. AS-73 -l.457E-01 1.670E+OO 1. 671E+OO NOT IDENT. AS-74 -5.065E+02 4.936E+03 4.941E+03 SHORT HLIF SE-75 1.219E-02 1. 742E-01 1. 743E-01 NOT IDENT. BR-77 1.177E+38 1.012E+39 O.OOOE+OO SHORT HLIF SR-82 5.163E+02 6.498E+02 6.902E+02 SHORT HLIF RB-83* --,2.829E-01 5.715E-01 5.855E-01 FAIL ABUN KR-85 1. 970E+OO 5. 981E+OO 6.047E+OO NOT IDENT. SR-85 2.0lOE-01 6.181E-01 6.247E-01 NOT IDENT. RB-86 1.284E+03 2.381E+04 2. 381E+04 SHORT HLIF Y-88 9.869E-02 1. 991E-01 2.040E-01 NOT IDENT. Y-91 -4.783E+02 5.952E+02 6.330E+02 NOT IDENT. NB-94 2. llOE-02 3.396E-02 3.527E-02 NOT IDENT. NB-95 -9.650E-01 9.139E-01 1.012E+OO NOT IDENT. NB-95M ..:l.421E+OO 2.147E+OO 2. 241E+OO NOT IDENT. ZR-95 -4.361E-02 1.500E+OO 1.500E+OO NOT IDENT. NB-97 *l.OOOE+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 7.486E+40 O.OOOE+OO SHORT HLIF M0-99 -3.682E+30 l.007E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.687E+41 O.OOOE+OO SHORT HLIF RH-101 -2.626E-02 2.761E-02 3.004E-02 NOT IDENT. RH-102 *1. 073E-02 4.766E-02 4.790E-02 NOT IDENT. RU-103 -3.534E+OO 4.920E+OO 5.172E+OO FAIL ABUN RH-106 2.090E-01 4.659E-01 4.753E-01 NOT IDENT. RU-106 2.090E-01 4.659E-01 4.753E-01 NOT IDENT. AG-108M -l.608E-02 2.314E-02 2.425E-02 NOT IDENT. AG-llOM -5.618E-02 8.950E-02 9.301E-02 FAIL ABUN SN-113 -7.373E-02 1. 739E-01 1. 771E-01 NOT IDENT. CD-115 -3.925E+38 l.476E+39 0.000E+OO SHORT HLIF SN-ll 7M -5.892E+04 7.318E+04 7.785E+04 SHORT HLIF TE-123M -3.381E-02 1.057E-01 l.068E-01 NOT IDENT. SB-124 5. 851E-01 1.574E+OO 1.595E+OO NOT IDENT. SB-125 1.226E-01 l.639E-01 l.729E-01 FAIL ABUN TE-125M 3.826E+Ol 2. 051E+02 2.058E+02 NOT IDENT. I-126 4. 960E+05 7.831E+05 8.144E+05 SHORT HLIF SB-126 2.163E+05 1. 086E+06 l.090E+06 SHORT HLIF SB-127 1.259E+21 1. 421E+22 O.OOOE+OO SHORT HLIF I-131 -2.082E+08 3.679E+09 3.681E+09 SHORT HLIF I-132 -l.OOOE+41 1.840E+42 O.OOOE+OO SHORT HLIF TE-132 -2.398E+25 2.057E+26 O.OOOE+OO SHORT HLIF BA-133 l.321E-02 3.587E-02 3.636E-02 FAIL ABUN I-133 1.000E+41 2.357E+41 O.OOOE+.00 SHORT HLIF CS-134 4.753E-02 7.747E-02 8.038E-02 FAIL ABUN I-135 l.000E+41 1.080E+42 O.OOOE+OO SHORT HLIF CS-136 4.573E+04 2.303E+05 2.312E+05 SHORT HLIF CE-139 5.537E-04 9.138E-02 9.138E-02 NOT IDENT. BA-140 7.225E+05 9.247E+05 9.804E+05 SHORT HLIF LA-140 -5.438E+05 4.840E+05 5.425E+05 SHORT HLIF CE-141 1.082E+Ol 1. 898E+Ol 1. 960E+Ol NOT IDENT. CE-143 1.000E+41 2.746E+41 O.OOOE+OO SHORT HLIF CE-144 4.280E-02 2.800E-01. 2.807E-01 FAIL ABUN PM-144 -l.650E-02 5.342E-02 5.393E-02 NOT IDENT. PR-144 -l.460E+OO 4.631E+OO 4.678E+OO NOT IDENT. PM-146 2.852E-02 4.093E-02 4.290E-02 FAIL ABUN ND-147 3 .118E+07 4. 7 60E+07 4. 963E+07 SHORT HLIF PM-147 -2.543E+02 6.037E+02 6.145E+02 NOT IDENT. PM-149 7.426E+39 2.117E+40 0.000E+OO SHORT HLIF EU-150 -1.118E-02 2.839E-02 2.883E-02 FAIL ABUN EU-152 1.583E-02 8.325E-02 8.356E-02 FAIL ABUN GD-153 -3. 971E-02 l.225E-01 1.238E-01 NOT IDENT. EU-154 -l.862E-02 9.933E-02 9. 968E-02 NOT IDENT. EU-155 5.563E-02 8.229E-02 8.602E-02 FAIL ABUN TB-160 3.548E-01 1.809E+OO 1.816E+OO FAIL ABUN H0-166M -2.302E-02 5.424E-02 5.523E-02 FAIL ABUN TM-171 1.147E+OO 3.795E+OO 3.830E+OO NOT IDENT: Page 3363 of 5809 HF-172 1. 406E-01 1. 815E-01 1.922E-01 FAIL ABUN LU-172 3.597E-02 8.226E-02 8.384E-02 FAIL ABUN LU-176 -2.303E-02 2.342E-02 2.562E-02 FAIL ABUN HF-181 -2.095E+OO 4.059E+OO 4.168E+OO NOT IDENT. TA-182 l.355E-01 8.576E-01 8.598E-01 FAIL ABUN RE-183 -2.948E-02 8.280E-01 8. 281E-01 NOT IDENT. RE-184 1.334E+Ol 2.926E+Ol 2.987E+Ol NOT IDENT. W-188 9.998E+Ol 1.144E+02 1.229E+02 FAIL ABUN IR-192 1.234E-01 4.267E-01 4.303E-01 FAIL ABUN BI-207 1.032E-03 4.267E-02 4.267E-02 FAIL ABUN BI-211 2.948E+OO 5.292E-01 l.430E+OO FAIL ABUN PB-211 2.983E-01 6.095E-01 6.242E-01 FAIL ABUN RN-219 -l.275E-01 3.368E-01 3.417E-01 NOT IDENT. RA-223 -2.049E-01 6.433E-01 6.499E-01 FAIL ABUN AC-227 2.618E-02 1.990E-01 l.994E-01 FAIL ABUN TH-227 2.618E-02 1.990E-01 l.994E-01 FAIL ABUN PA-231 -l.344E-01 4.501E-01 4.542E-01 NOT IDENT. TH-231 *-2.049E-01 6.433E-01 6.499E-01 FAIL ABUN PA-233 3.083E-02 5.584E-02 5.754E-02 FAIL ABUN PA-234 1.892E-01 3. 491E-01 3.594E-01 NOT IDENT. PA-234M -6.718E-01 4.014E+00 4.025E+OO NOT IDENT. NP-237 3.083E-02 5.584E-02 5.754E-02 FAIL ABUN NP-238 -2.003E+39 l.938E+41 O.OOOE+OO SHORT HLIF NP-239 -l.725E-01 1.922E-01 2.074E-01 FAIL ABUN PU-239 l.092E+02 2.525E+02 2.573E+02 NOT IDENT. AM-241 2.777E-02 4.653E-02 4.818E-02 NOT IDENT. CM-243 -2.004E-02 6.949E-02 7.008E-02 .FAIL ABUN BK-247 l.'205E-02 6.579E-02 6.602E-02 FAIL ABUN CM-247 -4.604E-03 3.009E-02 3.016E-02 FAIL ABUN CF-249 2.627E-02 3.075E-02 3.295E-02 NOT IDENT. CF-251 -2.207E-02 9.955E-02 1.000E-01 NOT IDENT. Page 3364 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 49.1228 87.09 76.1071 136.47 69.0987 45.60 55.7147 87.57 76.1977 140.51 0.0000 46.54 55.9163 88.03 76.2836 143.76 73.9265 49.72 0.0000 88.34 76.3411 144.24 68.0682 51. 35 80.6338 88.47 76.3656 145.44 65.2417 51. 87 66.5273 89. 96 76.6420 152.43 64.0059 52.39 68.2366 1093.63 76. 7676 153.25 0.0000 52.97 71. 5557 91.11 0.0000 323.87 70.2094 53.44 70.8767 92.59 77.1247 156.02 0.0000 54.07 76.6183. 93.35 77.2629 158.56 0.0000 57.36 0.0000 "94.56 73.9057 159.00 65.6982 57.53 91.2452 94.65 73.9214 162.33 67.0594 57.98 97.8495 94.67 73.9246 162.66 0.0000 59.27 93 .1185 94.87 73.9586 163.33 64 .1113 59.32 93 .1339 97.43 84.5951 165.86 63.3415 59.54 96. 4511 98.43 75.7671 176.31 61.2300 60.96 102.3334 98.44 '75.7687 176.60 0.0000 61.17 99.1332 99.53 73.2425 177.52 66.5361 62.93 106.8018 100 .11 66.0944 181.07 0.0000 63.29 106.9211 102.03 72.7411 181.52 55.7690 63.58 107.0168' 103.18 86.5982 184.41 75.5991 64.28 106. 6966 103.37 78.4263 143.76 62.0645 66.73 103.0565 105.21 80.5711 193.51 77.6271 67.24 109.0391 J._05.31 77.8412 197.03 72.6567 125.81 109.1810 106.12 84.3984 198.01 58.8437 67.75 111.7038 106.47 94.5602 201.83 78.5004 69.67 114.8485 109.28 80.3472 203.43 70.0454 70.83 114.3900 111. 00 77.8553 205.31 99.3868 72. 81 121.7988 111.76 0.0000 210.85 66.7343 72.87 121.8197 114. 06 58.7587 215.65 56.9250 74.66 115.6247 116. 30 0.0000 222 .11 46.3483 74.82 115.6755 116. 74 90.9597 227.09 44.4104 74.97 115.7233 119.76 78.2976 227.38 47.7576 77 .11 116. 3987 121.12 69.0474 228.16 0.0000 78.74 116.9072 121. 22 69.0607 228.18 45.5807 79.69 117.2008 121.78 71.9765 116.74 45.5807 80.12 117.3326 122.06 62.5402 235.69 58.3278 '80.19 0.0000 122.92 69.2880 235. 96 58.3469 80.57 117.4706 123.07 71. 2069 238.63 48.3986 81. 00 117.6024 265.00 72.2404 238.98 0.0000 81. 07 117.6241 125.81 63.9442 240.99 48.5312 81.75 62.3809 127.23 89.9520 242.00 48.5882 83.79 80.1266 127.91 76.6528 244.70 45.3381 84.00 88.8835 129.30 74.9293 252.40 0.0000 85.43 89.2041 131.20 73.2643 252.80 41.1784 86.55 76.0059 133.02 84.1472 254.15 0.0000 86.79 76.0509 133.52 67.7655 256.23 41.3350 86.94 76.0793' 136.00 70.0137 260.90 0.0000 Page 3365 of 5809 ENERGY. MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 37.0801 355.39 0.0000 584.27 31.0475 264.80 37.0859 356.01 26.5422 595.83 0.0000 265.00 35.5482 364.49 0.0000 427.87 32.8254 2 68. 22 38.3849 366.42 0.0000 602.52 0.0000 269.46 38.4352 372.51 29.8994 604.72 20.9359 270.03 38.4584 375.05 35.9545 607.14 25.4564 271.23 46.6748 377.52 35.1685 609.32 15.9915 273.65 0.0000 356.01 31.8993 610.33 19.5008 276.40 46.9275 388.16 21.6273 614.28 18. 0396 277.37 46.9751 388.63 0.0000 618.01 18.0754 277.60 46.9861 391.69 26.8929. 620.36 . 21.1154 278.00 43.8719 264.66 27.0815 621. 93 18 .1143 279.20 40.7890 401. 81 34.9748 630.19 0.0000 279.54 34.5254 402.40 31.4912 631.29 12.1362 279.70 34.5308 40*4. 85 29.7977 633.25 22.2730 280.46 45.5538 410.95 33.0177 634.78 0.0000 283.69 39.0062 413.71 27.7926 635.95 19.2636 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42.6270 423.72 0.0000 645.85 16.3060 285.90 0.0000 427.09 29.4067 657.76 29.2248 287.50 46.2756 427.87 29.4235 657.90 0.0000 290.67 38.0908 433.94 29.5538 661. 66 24.6592 293.27 0.0000 439.40 29.6699 664.57 0.0000 351. 93 40.6541 453.88 24.5248 666.33 0.0000 295. 96 40.6842 463.37 22.8577 666.50 0.0000 879.38 51.1849 468.07 26.4164 667.71 0.0000 299.98 44.4479 473.00 0.0000 677.62 21.7520 300.09 44.4524 475.06 31.3334 685.70 0.0000 300.13 44.4547 476.78 34.1380 695.00 0.6000 301.36 54.1310 477.60 30.4635 696.49 24.0463 302.85 37.3442 482.18 33.3347 696.51 24.0472 256.23 37.4028 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.0566 306.78 49 . .S771 497.08 28.9862 697.49 23.0125 308.46 35.1225 505.52 35.2547 702.65 23.0706 311.90 34.0225 507.63 0 .. 0000 706.68 23 .1154 316.51 35.3898 511. 00 23.5850 711.68 21.0645 319.41 0.0000 514.00 18.4312 720.70 0.0000 320.08 0.0000 514.00 18.4312 721. 93 0.0000 321.04 34.3130 520.40 25.6223 722.78 23.8229 323.87 45.8703 520.69 0.0000 722. 91 27. 0014 325.23 36.0857 522.65 0.0000 723. 31 27.0066 328.76 0.0000 527.90 0.0000 724 .19 20.6608 333.37 33.0469 528.26 22.8867 727. 33 14.3245 333.97 47.9439 529.59 22.9053 733.00 12.1671 334.37 56.2295 529.87 0.0000 735.93 17.5789 338.28 41.0748 531. 02 0.0000 333.97 15.9918 338.32 41. 07 58 537.26 0.0000 739.50 0.0000 311.90 41.1543 546.56 0.0000 747.24 13.9225 340.48 41.1543 552.55 20.3215 748.06 18.2133 340.55 0.0000 563.25 22.3973 752.31 16.1023 344.28 30.0300 569.33 19.5451 753.82 0.0000 345.93 31.7440 946.00 19.5475 756.73 17.7481 351.06 38.5972 569.70 17.5942 756.80 17.7488 351. 93 38.6263 583.19 30.5371-884.68 22.6628 . Page 3366 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:12:49.63 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621352.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 08:54:28. Sample ID G1203621352 Sample quantity 1.15000E+02 GRAM Detector name GAM06 Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:04.93 0.5% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 0 9 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 Energy 46.45* 57.98 59.52 79 .. 75 88.05 122.00 176.42 207.48 263.19 344.80 422.27 624.76 652.88 661.31 682.16 868.77 1004.49 1061.17 1070.41 1116.07 1172.55 1331.71 1447.49 1449.99 1494.41 1502.94 1559.77 1628.13 1681.09 1701.37 1741.41 1771.88 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 5184 523 14681 39 2683 183 33 45 46 51 87 4 40 11922 40 65 51 22 51 129 7331 6678 17 19 11 19 10 9 9 7 12 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 5306 1986 1748 920 1645 893 496 455 538 355 507 431 218 534 198 373 *391 263 227 276 305 136 11 7 15 4 6 12 6 16 3 0 0.95 1. 73 0.94 0.73 1. 02 0.97 1. 25 0.62 1. 46 1. 25 2.45 2.97 1. 35 1. 47 1. 27 4.15 3.20 0.95 2.08 3.81 1. 87 2.00 2.03 2.03 3.00 1. 01 0.63 1.10 1. 40 1. 44 0.78 1. 00 92. 64 115. 68 118.76 159.19 175.76 243.61 352.38 414.45 525.79 688.90 843 .. 76 1248.56 1304.78 1321. 64 1363. 33 1736.45 2007.88 2121.24 2139. 72 2231.04 2344.00 2662.38 2894.00 2899.00 2987.87 3004.95 3118. 66 3255.44 3361.40 3401.99 3482.11 3543.09 87 113 113 157 170 240 351 413 524 68 6 841 1237 1301 1314 1359 1730 2001 2118 2134 2225 2338 2653 2889 2889 2976 2998 3111 3250 3356 3396 3476 3539 11 12 12 6 12 8 6 5 7 6 8 13 7 16 8 12 13 9 10 12 16 18 19 19 14 14 12 12 9 .13 11 9 5.76E+00 3.1 5.81E-01 11.5 2.22E+OO 1. 63E+Ol 1. 0 4.33E-02123.8 2.98E+OO 3.6 2.03E-01 29.3 3.71E-02106.6 5.02E-02 72.0 5.13E-02 84.4 5.69E-02 60.0 9.63E-02 46.4 3.90E-03***** 4.42E-02 63.7 1.32E+01 1.0 4.42E-02 63.4 7.18E-02 61.2 5. 64E-02 81. 9 2.46E-02133.3 5.66E-02 57.6 l.43E-01 27.5 8. 15E+OO 1. 3 7. 42E+OO 1. 3 1.89E-02 36.1 1.24E+OO 2.15E-02 38.0 1.27E-02 75.6 2.16E-02 30.5 1.15E-02 56.5 1.00E-02 83.9 1.02E-02 59.7 8. 07E-03119. 9 1.37E-02 38.4 1. 22E-02 30. 2 Flag: "*" = Peak area was modified by background subtraction Page 3368 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:12:51 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621352.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G12.03621352 SOLID GAMMA6 0 00:15:00.00 1.50 keV No Empirical 75.00 Acquisition date : Sample quantity Sample geometry : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 08:54:28 115. 00 GRAM CAN 0 00:15:04.93 10.00 0.00 % Peak Energy 0.5% No performed Page 3369 of 5809 Nuclide Line Activity Report Sample ID : G1203621352 Nuclide Type: Nuclide Energy Area C0-57 122.06 192 136.47 ------C0-60 1173.23 6983 1332.49 6325 ZN-65 1115. 54 123 CD-109 88.03 2848 SN-126 64.28 ------86.94 2848 87.57 2848 BA-137M 661.66 11644 CS-137 661. 66 11644 PM-147 121. 22 192 PB-210 46.54 5644 AM-241 59.54 15831 Flag: "*" Key line Page 3370 of 5809 %Abn 85.60* 10.68 99.85 99.98* 50.60* 3.70* 9.60 8.90 37.00* 89.90* .85 .10* 0.00* 4.25* 35.90* Acquisition date Page : 2 3-0CT-2016 08:54:28 Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi/GRAM %Error 6.177E+OO 9.479E-01 1.00lE+OO 58.57 -6.083E+OO ------Line Not Found ------1.227E+OO 1. 488E+02 1.500E+02 2.57 l.092E+OO 1.513E+02 1.525E+02 2.58 1.284E+OO 4.950E+OO 5.260E+OO 55.01 5.256E+OO 3.825E+02 3.950E+02 7.21 2. 772E+OO ------Line Not Found ------5.256E+OO 1.590E+02 1.590E+02 7.21 5.256E+OO 3.825E+Ol 3.825E+Ol 7.21 2.028E+OO 1.667E+02
1. 670E+02 2.03 2.028E+OO 1. 7 62E+02 1. 7 64E+02 2.03 6.177E+OO 2.847E+04. 2.892E+04 58.57 6.123E-01 5.664E+03 5.674E+03 6.13 2.129E+OO 5.410E+02 5.410E+02 1. 91 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:52.47 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston,. SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl20362l352.CNF;l *
Acquisition date 3-0CT-2016 08:54:28 Sensitivity : 3.000 *
Detector ID GAM06 Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:04.93 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
Sample ID G1203621352 Sample Quantity.: l.1500E+02 GRAM *
Batch Number 1596247 Wet 0.00000 *
Wet-wt corr 1.00000 Dry Weight 0.00000 * *Nuclide-Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4 '* ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) C0-57 1. OOlE+OO 5.745E-01 C0-60 l.525E+02 3.856E+OO ZN-65 5.260E+OO 2.836E+OO CD-109 3.950E+02 2.790E+Ol SN-126 3.825E+Ol 2.702E+OO BA-137M 1.670E+02 3.319E+OO CS-137 l.764E+02 3.506E+OO PM-147 2.892E+04 1. 660E+.04 PB-210 5.674E+03 3.411E+02 AM-241 5.410E+02 l.014E+Ol Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 Page 3371 of 5809 Key-Line Activity (pCi/GRAM -1.880E+OO -2.590E-01 O.OOOE+OO 1. 211E-Ol -4.385E-01 -l.583E-01 1. 084E+00 3.819E+OO -4.769E-01 2.905E-01 O.OOOE+OO 6.436E-01 1. 725E+OO 1.399E+Ol 1.201E+OO -2.402E-02 5.714E-01 -3.457E+02 3.582E+OO 6.686E-01 K.L. Cnt Uncert ( 1. 96-sigma) 6.849E+OO 3.644E-01 6.071E+09 3.017E-01 2.341E+OO 9.402E-01 l.883E+OO '6. 398E+OO 7.182E-01 8.260E-01 -1.960E+41 7.617E-01 2.102E+OO 2.657E+Ol 2.460E+Ol l.812E+OO 9.449E-01 7.879E+02 6.844E+OO l.276E+OO MDA (pCi/GRAM 5.328E-01 8.177E-01 3.052E+OO 1.577E+Ol 1.536E+OO 9.844E-01 1.040E+OO 1.538E+04 1. 962E+02 5.631E+OO MDA (pCi/GRAM 1.196E+Ol 6.230E-01 0.000E+OO 6.159E-01 4.489E+OO 1.566E+OO . 3. 451E+OO 1.185E+Ol 1.177E+OO l.421E+OO O.OOOE+OO l.351E+OO 3.847E+OO 4.826E+Ol 4.445E+Ol 3.171E+OO 1.206E+OO 1.299E+03 l.202E+Ol 2.292E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NO-T IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

KR-85 4.941E+Ol l.076E+02 l.932E+02 NOT IDENT. SR-85 2.804E-01 6.088E-01 l.093E+00 NOT IDENT. RB-86 l.695E+Ol 2.054E+Ol 3.776E+Ol NOT IDENT. Y-88 -6.479E-02 3.626E-01 6.643E-01 NOT IDENT. Y-91 -7.015E+Ol 2.336E+02 4.149E+02 NOT IDENT. NB-94 * -2.860E-01 5.000E-01 8.385E-01 NOT IDENT. NB-95 -2.712E-01 7.392E-01 1.242E+OO NOT IDENT. NB-95M -6.750E-Ol 1.829E+OO 3.021E+OO NOT IDENT. ZR-95 4.638E-01 l.240E+OO 2.173E+OO NOT IDENT. NB-97 O.OOOE+OO 8.509E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.297E+10 O.OOOE+OO SHORT HLIF M0-99 -l.167E+03 1.028E+03 1. 661E+03 NOT IDENT. TC-99M O.OOOE+OO 1.244E+25 O.OOOE+OO SHORT HLIF RH-101 -4.632E-02 3.549E-01 6.178E-01 NOT IDENT. RH-102 3.279E-01 8.920E-01 1.580E+OO NOT IDENT. RU-103 9.859E-02 7.754E-01 1. 374E+OO NOT IDENT. RH-106 4.659E-01 5.185E+OO 9.070E+OO NOT IDENT. RU-106 4.659E-01 5.185E+OO 9.070E+OO NOT IDENT. AG-108M 4.513E-02 5.714E-01 l.016E+OO NOT IDENT. AG-llOM -3.650E-01 l.089E+OO l.803E+OO NOT IDENT. SN-113 -l.085E-01 7.783E-01 1.387E+OO NOT IDENT. CD-115 -2.673E+02 1.305E+03 2.279E+03 NOT IDENT. SN-ll 7M 3.390E-01 8.872E-01 l.550E+OO NOT IDENT. TE-123M 1.288E-01 3.457E-01 6.040E-01 NOT IDENT. SB-124 8.470E-03 6.127E-01 1.222E+00 NOT IDENT. SB-125 -6.472E-01 1.680E+00 2.950E+OO FAIL ABUN TE-125M 3.835E+Ol 1.170E+02 2.085E+02 NOT IDENT. I-126 -1. 724E+OO 5. lOlE+oO 7. 724E+OO NOT IDENT. SB-126 1. 511E+OO 3.208E+OO 5.669E+00 NOT IDENT. SB-127 -3.088E+Ol 7.078E+Ol 1.060E+02 NOT IDENT. I-131 8.704E-01 3.204E+OO 5.820E+OO FAIL ABUN I-132 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF TE-132 -1.951E+Ol 4.099E+Ol 6.761E+Ol NOT IDENT. BA-133 -9. 641E-02 6. 541E-01 l.175E+OO FAIL ABUN I-133 O.OOOE+OO l.400E+07 O.OOOE+OO SHORT HLIF CS-134 -l.044E-01 7.186E-01 1.217E+OO NOT IDENT. CS-135 -2.920E-01 2.333E+00 3.855E+OO NOT IDENT. I-135 O.OOOE+OO 3.793E+23 O.OOOE+OO SHORT HLIF CS-136 2.977E+OO 3.047E+OO 5.642E+OO FAIL ABUN CE-139 1.644E-01 3.677E-01 6.421E-01 NOT IDENT. BA-140 1.513E+00 5.983E+OO l.065E+Ol FAIL ABUN LA-140 -2.759E-01 8.810E-01 l.605E+OO NOT IDENT. CE-141 7.074E-02 8.172E-01 l.421E+OO NOT IDENT. CE-143 O.OOOE+OO 4.321E+04 O.OOOE+OO SHORT HLIF CE-144 -l.056E+00 2.320E+00 3.980E+OO FAIL ABUN PM-144 1.240E-01 5.391E-01 9.429E-01 NOT IDENT. PR-144 9.313E+OO 4.048E+Ol 7.080E+Ol NOT IDENT. PM-146 6.184E-01 8.485E-01 l.532E+OO NOT IDENT. ND-14 7 . -9.575E+OO l.364E+Ol 2.330E+Ol NOT IDENT. PM-149 -4.503E+03 9.654E+03 l.566E+04 NOT IDENT. EU-150 -1. 570E-02 4.035E-01 7.303E-01 NOT IDENT. EU-152 l.510E+OO 1. 776E+OO 2. 717E+OO FAIL ABUN. GD-153 2.130E-01 9.702E-01 1. 732E+OO NOT IDENT. EU-154 -7.977E-01 l.021E+OO 1. 730E+OO FAIL ABUN EU-155 -6.607E-01 l.193E+OO 2.070E+OO FAIL ABUN TB-160 6.482E-01 2. 996E+OO 5.094E+OO FAIL ABUN H0-166M -9.997E-03 9.507E-01 1. 641E+OO FAIL ABUN TM-171 -2.081E+OO 4.953E+02 8. 951E+02 NOT IDENT. HF-172 -7. 571E-01 2.330E+OO 3.720E+OO FAIL ABUN LU-172 -7. 722E-01 l.308E+OO 2.266E+OO FAIL ABUN LU-176 -l .151E-01 3.856E-01 6. 963E-01 FAIL ABUN HF-181 -6.184E-01 9.069E-01 l.561E+OO FAIL ABUN TA-182 -5.438E-02 1.912E+OO 3.480E+OO NOT IDENT. RE-183 0.000E+OO 6.232E+00 l.224E+Ol FAIL ABUN RE-184 2.127E+OO 3.138E+OO 5.420E+00 NOT IDENT. W-188 l.266E+02 l .'178E+02 2.030E+02 NOT IDENT. IR-192 -2.490E-01 5.280E-01 9.467E-01 NOT IDENT. HG-203 9.750E-02 6.268E-01 l.045E+OO NOT IDENT. BI-207 -4.066E-01 l.267E+OO l.816E+OO NOT IDENT. TL-208 -4.466E-02 5. 571E-01 9.726E-01 NOT IDENT. BI-211 7.282E-01 3.057E+OO 5.566E+OO NOT IDENT. PB-211 -l.244E+01 l.190E+Ol 2.052E+Ol NOT IDENT. BI-212 9.954E-01 7.923E+OO 1.374E+Ol NOT IDENT. PB-212 2.726E-01 8.007E-01 1.360E+OO NOT IDENT. BI-214 -3.289E-01 l.084E+OO l.867E+OO NOT IDENT. PB-214 . -3. 957E-01 1.115E+OO 1.990E+OO FAIL ABUN RN-219 2.822E+OO 6.745E+OO l.223E+Ol NOT IDENT. RN-222 -3.289E-01 l.084E+OO 1. 867E+OO NOT IDENT. Page 3372 of 5809 RA-223 3.803E+OO 9.421E+OO 1. 733E+Ol FAIL ABUN RA-224 1. 718E+OO 8.628E+OO l.455E+Ol NOT IDENT. RA-226 -3.289E-Ol 1.084E+OO 1. 8 67E+OO NOT 'IDENT. AC-227 -8.529E-01 3.698E+OO 6. llOE+OO FAIL ABUN TH-227 -8.529E-Ol 3.698E+OO 6. llOE+OO FAIL ABUN AC-228 2.703E-Ol 3.166E+OO 5.319E+OO NOT IDENT. RA-228 2.703E-01 3.166E+OO 5.319E+OO NOT IDENT. TH-228 2.726E-Ol 8.007E-01 1.360E+OO NOT IDENT. TH-229 -5.997E+OO 6.993E+OO l.152E+Ol FAIL ABUN TH-230 -3.289E-01 1.084E+OO 1.867E+OO NOT IDENT. PA-231 -7.971E+OO 6.634E+OO l.165E+Ol NOT IDENT. TH-231 3.803E+OO 9.421E+00 1. 733E+Ol FAIL ABUN TH-232 2.703E-01 3.166E+OO 5.319E+OO NOT IDENT. PA-233 3.978E-01 9.528E-01 1. 757E+OO NOT IDENT. PA-234 4.267E+OO 6.913E+OO 1. 2 63E+Ol NOT IDENT. PA-234M 3.551E+Ol . 1. 052E+02 l.691E+02 NOT IDENT. TH-234 -2.388E+OO 1. 776E+Ol 2.978E+Ol NOT IDENT. U-234 -3.289E-01 1.084E+OO 1.867E+OO NOT IDENT. U-235 -9.497E-01 2.290E+OO 3.917E+OO NOT IDENT. NP-237 3.978E-01 9.528E-01 1. 757E+OO NOT IDENT. NP-238 O.OOOE+OO 3.268E+03 O.OOOE+OO SHORT HLIF U-238 -2.388E+00 1. 776E+Ol 2.978E+Ol NOT IDENT. NP-239 4.059E-01 3 .137E+00 5.528E+OO NOT IDENT. PU-239 -1.314E+03 3.882E+03 6.699E+03 NOT IDENT. AM-243 1.423E-02 6.129E-01 1.101E+OO NOT IDENT. CM-243 7.317E-02 1. 201E+OO 2.129E+OO NOT IDENT. BK-247 -4. 071E-01 1.382E+OO 2.082E+00 NOT IDENT. CM-247 l.264E-01 6.125E-01 l.103E+OO NOT IDENT. CF-249 3.441E-02 6.706E-01 1. 204E+OO NOT IDENT. CF-251 9.590E-01 2.005E+OO 2.687E+OO FAIL ABUN ANH-511 l.798E-01 4.890E-01 8.844E-01 NOT IDENT. Page 3373 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:12:50.44 Nuclide Activity Repcirt Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 192 85.60* 6.177E+OO 9.479E-01 1. OOlE+OO 58.57 136.47 ------10.68 6.083E+OO ------Line Not F,ound ------C0-60 1173.23 6983 99.85 1.227E+OO 1.488E+02 1. 50"0E+02 2.57 1332.49 6325 99.98* 1. 092E+OO 1.5l3E+02 1.525E+02 2.58 ZN-65 1115. 54 123 50.60* 1. 284E+OO 4.950E+OO 5.260E+00 55.01 CD-109 88.03 2848 3.70* 5.256E+OO 3.825E+02 3.950E+02 7.21 SN-126 64.28 ------9.60 2. 772E+00 ------Line Not Found. ------86.94 2848 8.90 5.256E+OO 1.590E+02 1.590E+02 7.21 87.57 2848 37.00* 5.256E+OO 3.825E+Ol 3.825E+Ol 7.21 BA-137M 661. 66 11644 89.90* 2.028E+OO 1.667E+02 1.670E+02 2.03 CS-137 661.66 11644 85.10* 2.028E+OO 1. 762E+02 1. 7 64E+02 2.03 PM-147 121.22 192 0.00* 6.177E+00 2.847E+04 2.892E+04 58.57 PB-210 46.54 5644 4.25* 6.123E-01 5.664E+03 5.674E+03 6.13 AM-241 59.54 15831 35.90* 2.129E+OO 5.410E+02 5.410E+02 1. 91 Flag: "*" Key line Page 3374 of 5809 Summary of Nuclide Activity Sample ID : Gl203621352 Acquisition date Page : 2 3-0CT-2016 08:54:28 Total number of lines in spectrum 32 Number of unidentified lines 16 Number of-lines tentatively identified by NID 16 50.00% Nuclide Type : . Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags C0-57 271.74D 1. 06 9.479E-01 l.OOlE+OO 0.586E+OO 58.57 C0-60 5.27Y 1. 01 l.513E+02 l.525E+02 0.039E+02 2.58 ZN-65 244.06D 1. 06 4.950E+OO 5.260E+OO 2.894E+OO 55.01 CD-109 461.40D 1. 03 3.825E+02 3.950E+02 0.285E+02 7.21 SN-126 2.30E+05Y 1. 00 3.825E+Ol 3.825E+Ol 0.276E+Ol 7.21 BA-137M 30.08Y 1. 00 1.667E+02 1.670E+02 0.034E+02 2.03 CS-137 30.08Y 1. 00 1. 7 62E+02 1.764E+02 0.036E+02 2.03 PM-147 2.62Y 1. 02 2.847E+04 2.892E+04 l.693E+04 58.57 PB-210 22.20Y 1. 00 5.664E+03 5.674E+03 0.348E+03 6.13 AM-241 432.60Y 1. 00 5.410E+02 5.410E+02 0.103E+02 1. 91 ---------I---------Total Activity 3.560E+04 3.607E+04 Grand Total Activity 3.560E+04 3.607E+04 Flags: "K" Keyline not found "M" Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit Page 3375 of 5809 Unidentified Energy Lines Page : 3 Sample ID : G1203621352 Acquisition date : 3-0CT-2016 08:54:28 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 9 57.98 565 2144 1. 73 115. 68 113 12 5.8iE-01 23.0 1. 92E+OO T 0 79.75 42 981 0.73 159.19 157 6 4.33E-02 **** 4.59E+OO T 0 176.42 35 512 1. 25 352.38 351 6 3. 71E-02 **** 5.43E+OO T 0 207.48 46 466 0.62 414.45 413 5 5.02E-02 **** 4.90E+OO 0 263.19 47 546 1.46 525.79 524 7 5.13E-02 **** 4.12E+OO T 0 344.80 51 356 1. 25 688.90 686 6 5.69E-02 **** 3.36E+00 T 0 422.27 86 *505 2.45 843.76 841 8 9.63E-02 92.8 2.88E+OO T 0 624.76 3 422 2. 97 1248.56 1237 13 3.90E-03 **** 2.12E+OO 0 652.88 39 213 1. 35 1304.78 1301 7 4.42E-02 **** 2.05E+OO 0 682.16 39 193 1. 27 1363.33 1359 8 4.42E-02 **** l.98E+OO 0 868.77 62 360 4.15 1736.45 1730 12 7.18E-02 **** 1. 61E+OO 0 1004.49 49 375 3.20 2007.88 2001 13 5.64E-02 **** 1.41E+OO T 0 1061.17 21 251 0.95 2121.24 2118 9 2.46E-02 **** 1. 35E+OO 0 1070.41 49 217 2.08 2139. 72 2134 10 5.66E-02 **** 1.33E+OO 1 1447.49 16 10 2.03 2894.00 2889 19 1. 8 9E-02 72.2 1 .. 0lE+OO 1 1449.99 18 6 2.03 2899.00 2889 19 2.15E-02 76.0 1. OlE+OO 0 1494.41 11 14 3.00 . 2987.87 2976 14 1.27E-02 **** 9.85E-01 0 1502.94 18 3 1. 01 3004.95 2998 14 2.16E-02 61. 0 9.80E-01 0 1559.77 10 5 0.63 3118. 66 3111 12 1.15E-02 **** 9.49E-01 0 1628.13 8 11 1.10 3255.44 3250 12 1. OOE-02 **** 9.15E-01 0 1681.09 9 5 1. 40 3361. 40 3356 9 1.02E-02 **** 8.92E-01 0 1701.37 7 15 1. 44 3401.99 3396. 13 8.07E-03 **** 8.84E-01 0 1741.41 12 2 0.78 3482.11 3476 11 1. 37E-02 76. 8 8.68E-01 0 1771.88 10 0 1. 00 3543.09 3539 9 l.22E-02 60.3 8.56E-01 T Flags: "T" = Tentatively associated Page 3376 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:04.08 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621352.CNF;l *
Acquisition date 3-0CT-2016 08:54:28 Sensitivity : 3.000 *
Detector ID GAM06 Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:04.93 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID Gl203621352 Analyst initials: MXRl *
Batch Number 1596247 Sample Quantity : 1.1500E+02 GRAM *
Wet wt 9orr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO :'[CANBERRA. GAMMA] EFF GAM06 CAN. CNF; 14
Combined Critical Level Report NOTE: Not *all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 PM-147 PB-210 AM-241 Le (pCi/GRAM 2.593E-01 3.765E-01 l.469E+OO 7.698E+OO 7.496E-01 4.730E-01 4. 996E-01 7.486E+03 9.676E+Ol 2.770E+OO ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 Page 3377of5809 Le (pCi/GRAM 5. 811E+OO 2.801E-01 O.OOOE+OO 2.663E-01 1. 917E+OO 7.565E-01 1.664E+OO 5.753E+00 5.664E-01. 6.848E-01 O.OOOE+OO 6.504E-01 1.858E+OO 2.327E+Ol 2.192E+Ol 1. 523E+00 5.866E-01 6.322E+02 5.778E+OO 1.109E+OO 9.332E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

SR-85 RB-86. Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB.:...97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 1.LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 3378 of 5809 5.282E-01 l.821E+Ol 2.835E-01 1.930E+02 4. OllE-01 5. 962E-01 1. 471E+OO l.042E+OO O.OOOE+OO O.OOOE+OO 7. 965E+02 O.OOOE+OO 3.004E-01 7.598E-01 6.652E-01 4.363E+OO 4.363E+OO 4.942E-01 8.694E-01 6.736E-01 1.099E+03 7.540E-01 2.937E-01 5.045E-01 1.433E+OO 1.014E+02 3. 696E+OO 2*. 720E+OO 5.076E+Ol 2.825E+OO O.OOOE+OO 3.291E+Ol 5.700E-01 O.OOOE+OO 5.843E-01 1.874E+OO O.OOOE+OO 2. 722E+00 3.123E-01 5 .132E+OO 6.763E-01 6.910E-01 O.OOOE+OO 1.935E+OO 4.526E-01 3.398E+Ol 7.460E-01 1.122E+Ol 7.594E+03 3.545E-01 1.319E+OO 8.437E-01 7. 7 61E-01 1.007E+OO 2.458E+OO 7.866E-01 4.413E+02 l.808E+00 1.090E+OO 3.379E-01 7.570E-01 1.615E+OO 6.057E+OO 2. 621E+OO 9.869E+Ol 4.589E-01 5.076E-01 8.733E-01 4.680E-01 2.701E+OO 9.949E+oo* 6.592E+OO 6.619E-01 8.982E-01 9.651E-01 5.936E+OO 8.982E-01 8.413E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF* NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT: NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3379 of 5809 7.078E+OO 8.982E-01 2. 967E+OO '2. 967E+OO 2.572E+OO 2. 572E+OO 6.619E-01 5.603E+OO 8.981E-01 5.649E+OO 8.413E+OO 2. 572E+OO 8.532E-01 6.120E+OO 8 .161E+Ol l.453E+Ol *8.981E-01 1.905E+OO 8.532E-01 O.OOOE+OO 1.453E+Ol 2.692E+OO 3.258E+03 5.374E-01 1.036E+OO 1.012E+OO 5.353E-01 5.845E-01 1.306E+OO 4.282E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report 03-0CT-2016 09:13:09.17 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621352.CNF;l *
Acquisition date 3-0CT-2016 08:54:28 Sensitivity : 3.000 *
Detector ID GAM06 Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:04.93 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621352 Analyst initials: MXRl *
Batch .Number 1596247 Sample Quantity 1.1500E+02 GRAM *
Quantity Err(%) 1.7391E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff .. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4 * ********'***************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) C0-57 1.00lE+OO 5.791E-01 5. 791E-01 C0-60 l.525E+02 1.247E+Ol 1.247E+Ol ZN-65 5.260E+OO 2.986E+OO 2.986E+OO CD-109 3.950E+02 4.779E+Ol 4.779E+Ol SN-126 3.825E+Ol 4.161E+OO 4 .161E+OO BA-137M 1.670E+02 1.418E+Ol 1.418E+Ol CS-137 l.764E+02 1.497E+Ol l.497E+Ol PM-147 2.892E+04 1.673E+04 1.673E+04 PB-210 5.674E+03 5.985E+02 5.985E+02 AM-241 5.410E+02 4.310E+Ol 4.310E+Ol Non-Identified Nuclides . Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM* ( 1. 96-s igma) ( 1. 96-sigma) BE-7 -1.880E+OO 6. 851E+OO 6.903E+OO NOT IDENT. NA-22 -2.590E.:_01 3.650E-01 3.833E-01 NOT IDENT. NA-24 5.870E+08 6. 071E+09 6.077E+09 SHORT HLIF AL-26 1.211E-01 3.018E-01 3.067E-01 NOT IDENT. K-40 -4.385E-01 2.341E+OO* 2.350E+OO NOT IDENT. SC-46 -l.583E-01 9.404E-01 9.432E-01 NOT IDENT. V-48 1. 084E+OO 1. 889E+OO l.952E+00 NOT IDENT. CR-51 3.819E+OO 6.408E+OO 6.635E+oo NOT IDENT. MN-54 -4.769E-01 7.202E-01 7.516E-01 NOT IDENT. C0-56 2.905E-01 8.267E-01 8.370E-01 FAIL ABUN MN-56 l.OOOE+41 2.766E+41 O.OOOE+OO SHORT HLIF C0-58 6.436E-01 7.648E-01 8.180E-01 NOT IDENT. FE-59 1. 725E+00 2.126E+OO 2.264E+OO NOT IDENT. GE-68 1.399E+Ol 2.667E+Ol 2.741E+Ol NOT IDENT. AS-73 1.201E+00 2.461E+Ol 2.461E+Ol NOT IDENT. AS-74 -2.402E-02 1.812E+OO 1.812E+OO NOT IDENT. SE-75 5.714E-01 9.464E-01 9.809E-01 FAIL ABUN BR-77 -3.457E+02 8 .168E+o2 8.315E+02 NOT IDENT. SR-82 3.582E+00 6.854E+OO 7.041E+OO NOT IDENT. RB-83 6.686E-01 1.281E+OO l.316E+00 NOT IDENT. Page 3380 of 5809 KR-85 4.941E+Ol 1. 07 6E+02 1.099E+02 NOT IDENT. SR-85 2.804E-01 6.092E-01 6.222E-01 NOT IDENT. RB-86 .1.695E+Ol. 2.073E+Ol 2.210E+Ol NOT IDENT. Y-88 -6.479E-02 3.626E-01 3.638E-01 NOT IDENT. Y-91 -7.015E+Ol 2.337E+02 2.358E+02 NOT IDENT. NB-94 -2.860E-Ol 5.006E-01 5.170E-01 NOT IDENT. NB-95 -2.712E-01 'J.397E-01 7.497E-01 NOT IDENT. NB-95M -6.750E-Ol l.831E+OO l.856E+00 NOT IDENT. ZR-95 4.638E-Ol 1.241E+OO l.258E+00 NOT IDENT. NB-97 1.000E+41 8.549E+40 O.OOOE+OO SHORT HLIF ZR-97 -5.794E+09 l.298E+10. 1.324E+10 SHORT HLIF M0-99 -l.167E+03 l.034E+03 l.160E+03 NOT IDENT. TC-99M -9.070E+24 1.248E+25 0.000E+OO SHORT HLIF RH-101 -4.632E-02 3.551E-01 3.557E-01 NOT IDENT. RH-102 3.279E-01 8.927E-01 9.049E-01 NOT IDENT. RU-103 9.859E-02 7:754E-01 7.767E-01 NOT IDENT. RH-106 4.659E-01 5.185E+OO 5.189E+OO NOT IDENT. RU-106 4.659E-01 5.185E+00 5.189E+OO NOT IDENT. AG-108M 4.513E-02 5.714E-01 5. 718E-01 NOT IDENT. AG-110M -3.650E-01 1.090E+OO l.103E+OO NOT IDENT. SN-113 -1.085E-01 7. 7'83E-01 7.799E-01 NOT IDENT. CD-115 -2.673E+02 1.305E+03 1. 311E+03 NOT IDENT. SN-117M 3.390E-01 8.875E-01 9.006E-01 NOT IDENT. TE-123M 1. 288E-01 3.459E-01 3.507.E-01 NOT IDENT. SB-124 8.470E-03 6.127E-01 6.127E-01 NOT IDENT. SB-125 -6.472E-01 1. 681E+OO 1.706E+OO FAIL ABUN TE-125M 3.835E+Ol 1.170E+02 l 183E+02 NOT IDENT. I-126 -1.724E+OO 5.103E+OO 5.162E+OO NOT IDENT. SB-126 1. 511E+OO 3.214E+OO 3.285E+OO NOT IDENT. SB-127 -3.088E+Ol 7.089E+Ol 7.225E+Ol NOT IDEr:;IT. I-131 8.704E-01 3.204E+OO 3.228E+OO FAIL ABUN I-132 1.000E+41 3.538E+41 O.OOOE+OO SHORT HLIF TE-132 -1. 951E+Ol 4.105E+Ol 4.198E+Ol NOT IDENT. BA-133 -9. 641E-02 6.542E-01 6.556E-01 FAIL ABUN I-133 -4 .132E+06 l.402E+07 1.414E+07 SHORT HLIF CS-134 -1.044E-01 7.187E-01 7.202E-01 NOT IDENT. CS-135 -2.920E-01 2.333E+OO 2.337E+OO NOT IDENT. I-135 -2.706E+23 4.022E+23 O.OOOE+OO SHORT HLIF CS-136 2.977E+OO 3.092E+OO 3.370E+OO FAIL ABUN CE-139 1.644E-01 3.693E-01 3.767E-01 NOT IDENT. BA-140 1.513E+OO 5.984E+OO 6.023E+OO FAIL ABUN LA-140 -2.759E-01 8.813E-01 8.900E-01 NOT IDENT. CE-141 7.074E-02 8.172E-01 8.178E-01 NOT IDENT. CE-143 -5.489E+02-4.321E+04 4.321E+04 SHORT HLIF CE-144 -1. 056E+OO 2.322E+OO 2.370E+OO FAIL ABUN PM-144 l.240E-01 5.392E-01 5. 421E-01 NOT IDENT. PR-144 9.313E+OO 4.048E+Ol 4.070E+Ol NOT IDENT. PM-146 6.184E-01 8.509E-01 8.954E-01 NOT IDENT. ND-147 -9.575E+OO 1.367E+Ol 1.433E+Ol NOT IDENT. PM-149 -4.503E+03 9.680E+03 9.891E+03 NOT IDENT. EU-150 -1.570E-02 4.035E-01 4.036E-01 NOT IDENT. EU-152 1. 510E+OO 1. 782E+OO 1.908E+OO FAIL ABUN GD-153 2 .130E-01 9.703E-01 9.750E-01 NOT IDENT. EU-154 -7.977E-01 1.023E+OO 1.085E+OO FAIL ABUN EU-155 -6.607E-01 1.195E+OO l.231E+OO FAIL ABUN TB-160 6.-482E-01 2.998E+OO 3.012E+OO FAIL ABUN H0-166M -9.997E-03 9.507E-01 9.507E-01 FAIL ABUN TM-171 -2.081E+OO 4.953E+02 4.953E+02 NOT IDENT. HF-172 -7.571E-01 2.334E+OO 2.359E+OO FAIL ABUN LU-172 -7. 722E-01 1.317E+OO l.362E+OO FAIL ABUN LU-176 -1.151E-01 3.857E-01 3.892E-01 FAIL ABUN HF-181 -6.184E-01 9.085E-01 9.503E-01 FAIL ABUN TA-182 -5.438E-02 1.912E+OO l.912E+OO NOT IDENT. RE-183 2.763E+Ol 6.890E+OO 1.423E+Ol FAIL ABUN RE-184 2.127E+OO 3.153E+OO 3.295E+OO NOT IDENT. W-188 l.266E+02 1.19'1E+02 1. 321E+02 NOT IDENT. IR-192 -2.490E-01 5.285E-01 5.403E-01 NOT IDENT. HG-203 9.750E-02 6.268E-01 6.284E-01 NOT IDENT. BI-207 -4.066E-01 1. 2 69E+OO l.282E+OO NOT IDENT. TL-208 -4.466E-02 5.571E-01 5.575E-:-Ol NOT IDENT. BI-211 7.282E-01 3.058E+OO 3.075E+OO NOT IDENT. PB-211 -1.244E+Ol l.195E+Ol l.320E+Ol NOT IDENT. BI-212 9.954E-01 7.924E+OO 7.937E+OO NOT IDENT. PB-212 2.726E-01 8. 011E-01 8.105E-01 NOT IDENT. BI-214 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. PB-214 -3.957E-01 1.115E+OO l.129E+OO FAIL ABUN RN-219 2.822E+00 6.757E+OO 6.876E+OO NOT IDENT. RN-222 -3.289E-01 1.084E+OO l.094E+OO NOT IDENT. Page 3381of5809 RA-223 3.803E+OO 9.430E+OO 9.584E+00 FAIL ABUN RA-224 1.718E+OO 8.629E+OO 8.664E+OO NOT IDENT. RA-226 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. AC-227 -8.529E-01 3.700E+00 3. 720E+OO FAIL ABUN TH-227 -8.529E-01 3.700E+OO 3.720E+00 FAIL ABUN AC-228 2.703E-01 3.166E+OO 3.168E+OO NOT IDENT. RA-228 2.703E-01 3.166E+OO 3.168E+OO NOT IDENT. TH-228 2.726E-01 8. OllE-01 8.105E-01 NOT IDENT. TH-229 -5.997E+OO 7.008E+OO 7. 511E+OO FAIL ABUN TH-230 -3.289E-01 l.084E+OO l.094E+OO NOT IDENT. PA-231 -7.971E+OO 6.881E+OO 7.763E+OO NOT IDENT. TH-231 3.803E+OO 9.430E+OO 9.584E+OO FAIL ABUN TH-232 2.703E-01 3.166E+OO 3.168E+OO NOT IDENT. PA-233 3.978E-01 9.535E-01 9.702E-01 NOT IDENT. PA-234 4.267E+OO 8.481E+OO 8. 696E+OO NOT IDENT. PA-234M 3.551E+Ol 1.053E+02 1.065E+02 NOT IDENT. TH-234 -2.388E+OO 1.777E+Ol 1. 780E+Ol NOT IDENT. U-234 -3.289E-01 1.084E+00 l.094E+OO NOT IDENT. U-235 -9.497E-01 2.291E+OO 2.331E+00 NOT IDENT. NP-237 3.978E-01 9.535E-01 9.702E-01 NOT IDENT. NP-238 1.944E+03 3.280E+03 3.395E+03 SHORT HLIF U-238 -2.388E+OO 1.777E+Ol 1. 780E+Ol NOT IDENT. NP-239 4.059E-01 3.137E+OO 3.142E+OO NOT IDENT. PU-239 -l.314E+03 3. 883E+o3 3.928E+03 NOT IDENT. AM-243 1.423E-02 6.129E-01 6.130E-01 NOT IDENT. CM-243 7.317E-02 1.201E+OO l.202E+OO NOT IDENT. BK-247 -4. 071E-01 1.385E+OO 1.397E+OO NOT IDENT. CM-247 l.264E-01 . 6 .130E-01 6.156E-01 NOT IDENT. CF-249 3. 441E-02 6.706E-01 6.708E-01 NOT IDENT. CF-251 9.590E-01 2.008E+OO 2.054E+OO FAIL ABUN ANH-511 l.798E-01 4.893E-01 4.959E-01 NOT IDENT. Page 3382 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 1964 .1102 87.09 543. 0725 136.47 408. 9632 45.60 1653.5233 87.57 543.6205 140.51 429.2876 46.54 1658.5250 88.03 544.1423 143.76 431.3771 49.72 1488.5717 88.34 544.4946 144.24 396.9384 51. 35 1543.0040 88.47 544.6424 145.44 411. 3519 51. 87 1583.8177 89. 96 412.7759 152.43 367.5838 52.39 1569.6459 90.64 422.3123 153.25 401.0778 52.97 1610.8647 91.11 440.6485 154.21 408.0317 53.44 1625.3617 92.59 422.7026 156.02 394.0771 54.07 1638.0039 93.35 411.1242 158.56 394.4007 57.36 0.0000 94.56 434.3693 159.00 389.2594 57.53 1148. 3273 94.65 434.4481 162.33 379.1556 57.98 1149.7538 94.67 434.4652 162.66 376.0849 59.27 1153.8312 94.87 434.6365 163-. 33 398.0583 59.32 1153.9841 97. 43 442.6662 165.86 391. 8196 59.54 1154.6753 98.43 438.6497 176.31 369.7046 60.96 1159 .1030 98.44 438.6601 176.60 387.4492 61.17 1159.7546 99 .-53 452.2791 177.52 417.2925 62.93 516.2480 100. 11 468.4312 181.07 426.1812 63.29 523.9438 102.03 415.1772 181.52 429.7448 63.58 517.1239 103.18 427.8779 184.41 455.7509 64.28 549.3857 103.37 428.0305 185.72 477.6435 66.73 546.4628 105.21 448.2537 193.51 474.3121 67.24 558.9999 105.31 448.3368 197.03 443. 5702 67.68 586.0448 106.12 402.5224 198.01 431.6502 67.75 586.1478 106.47 423.5623 201.83 418.8242 69.67 572.4478 109.28 412.7963 203.43 442.3439 70.83 547.4277 111. 00 415.0669 205.31 387.4597 72.81 551.8744 111.76 438.6048 210.85 501.5160 72.87 567.6429 114. 06 428.3455 215.65 '462.3163 74.66 553.3564 116.30 421.9538 222 .11 459.7844 74.82 553.5613 116.74 444.4453 227.09 448.2363 74.97 575.0912 119.76 433.5675 227.38 444.8740 77 .11 525.7336 121.12 438.6215 228.16 469.7811 78.74 586.3143 121.22 438.6940 228.18 469.7933 79.69 557. 8715 121. 7 8 439.1027 235.69 464.0754 80.12 558.4072 122.06 439.3070 235. 96 448.8912 80.19 558.4934 122.92 439.9365 238.63 407.5923 80.57 584.9567 123.07 427.8218 446.7409 81. 00 599.3088 123.68 429.6140 240.99 416.8667 81. 07 599.4012 125.81 416.1079 242.00 406.6216 81. 75 605.3193 127.23 410.2280 244.70 387.5279 83.79 584.0486 127.91 400.4141 252.40 364.1497 84.00 608.2906 129.30 436.2925 252.80 373.8801 85.43 643.0718 131.20 408. 7134 254.15 0.0000 86.55 542.4550 133.02 425.4116 256.23 383 .. 5511 86.79 542.7246 133. 52 430.9233 260.90 365.5590 86.94 542.8986 136.00 400.3504 2 64. 66 452.5277 Page 3383 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 452.5847 364.49 350.5050 600.60 203. 7072 265.00 428.4145 366.42 365.9636 602.52 0.0000 268.22 398.9092 372.51 352.5831 604. 72 217.3263 269.46 392.0739 375.05 325.7884 607.14 209.4534 270.03 387. 4072 1093.63 359.1870 609.32 220.8763 271.23 385.4047 383.85 359.9358 610.33 232.1934 273.65 385.0406 388.16 369.9822 614.28 212.2402 276.40 343.1299 388.63 379.0397 618.01 202.4070 277.37 381.4609 391.69 372.6921 620.36 207.7578 277.60 381.5369 400.66 340.7706 621. 93 207.9147 278.00 374.3156 401.81 343.7465 630.19 0.0000 279.20 363.6677 402.40 342.0808 631. 29 196.5180 279.54 400.6453 404.85 386.0566 633.25 212.1441 279.70 400.7050 410.95 411. 2686 634.78 190.6608 280.46 361. 6232 413.71 350.1830 635.95 181. 4857 283.69 386.1206 414.70 374.9927 636.99 206.3395 284.31 355.4736 423. 72 407.9309 645.85 220.6790 285.41 391. 6548 427.09 381.0308 657.76 209.4159 285.90 358.4555 427.87 403.9958 657.90 0.0000 287.50 367.6336 433.94 419.4254 661. 66 199.3547 290.67 337.6343 439.40 449.5836 664.57 0.0000 293.27 0.0000 453.88 417.3255 666.33 177.3005 295.22 363.9128 463.37 441.3995 666.50 177.3143 295. 96 392.8271 468.07 412.5320 667.71 0.0000 298.58 341.2333 473.00 412.8260 677.62 176.6406 299.98 363.7502 475.06 433.2047 685.70 183.6218 300.09 363.7857 476.78 396.7338 695.00 178.0352 300.13 363.7946 477.60 401.6665 696.49 181.3326 301.36 395.0905 482.18 368.5732 696. 51 181.3326 302.85 349.5919 487.02 359.1517 697.00 195.1631 304.50 354.2728 492.35 330.6612 697.30 176.0913 304.85 359.4114 497.08 291.3271 697.49 182.4735 306.78 371. 7444 505.52 287.9408 702.65 181.8267 308.46 391.6042 507.63 0.0000 706.68 166.1753 311. 90 353.9734 511. 00 269.5263 711.68 178.2801 316.51 351.1019 514.oo 246.7615 720.70 169.3376 319.41 362.1230 514.00 246.7615 721. 93 0.0000 320.08 342.7983 520.40 260.2793 722. 78 203.8155 321.04 365.9975 520.69 271.0078 722. 91 208.1221 323.87 349.8250 522.65 0.0000 723. 31 203.8619 325.23 357.0263 527.90 248.7018 724 .19 177.1051 328.76 359.7583 528.26 249.7292 727. 33 178.4216 333.37 372. 2359 529.59 237.215:] 733.00 150.8407 333.97 364.6896 529.87 0.0000 735.93 184.4707 334.37 375.1112 531. 02 256.9429 737.46 166.2443 338.28 363.3517 537.26 224.4994 739.50 223.6520 338.32 378.8680 546.56 0.0000 747.24 202.7051 340.48 340.5182 552.55 206.6018 748.06 178.9178 340.55 340.5423 563.25 216.7227 752.31 184.6647 344.28 352.9492 569.33 230.3890 753.82 189.1301 345.93 344.3108 569.50 230.4078 756.73 165.4212 351.06 342.6258 569.70 230.4266 756.80 165.4212 351.93 360.2538 583.19 215.9798 763.94 203.0288 355.39 0.0000 584.27 217.0986 765.81 208.6420 356.01 361. 37.40 595.83 199.1723 766.42 204.3258 Page 3384 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 199.9924 1002.74 220.8060 1678.03 0.0000 772. 60 0.0000 1004.73 220.9492 1690.97 7.4952 776.52 179.9422 1021.30 0.0000 1750.46 0.0000 777.92 205.2921 1025.87 0.0000 1764.49 8.6982 778.90 183.4105 1028.54 0.0000 1770.23 3.4832 783.70 202.4704 1037.84 221.5378 1771.35 1. 7421 785.37 198.2080 1038.76 0.0000 1791.20 0.0000 792.07 220.8252 1046.59 228.4980 1808.65 9.8734 794.95 195.6536 1048.07 210.4624 1810.72 0.0000 795.86 201.2546 1049.04 229.5901 1836.06 13. 2"363 801.95 191. 7670 1050.41 243.3003 810.06 201.2756 1063.66 222.4504 810.29 202.4098 1077.00 207.8109 810.45 182.4046 1077.34 218.8256 810.76 183.5370 1085.87 207.4609 815.77 215.1067 1093.63 233.7222 818.51 201.9458 1099.45 225.8444 832.01 229.9243 1112. 07 256.1380 834.85 248.1394 1112.84 260.6484 835. 71 234.7423 1115. 54 219.5403 836.80 0.0000 1120.29 149.9120 846.75 0.0000 1120. 55 139.5313 846.77 218.8183 1121.30 142.5375 856.80 260.4065 1129. 67 147.9174 860.56 259.6470 1131.51 0.0000 871.09 . 254. 4022 1147.95 0.0000 873.19 252.8936 1173.23 156.4254 875.33 0.0000 1177.95 99.6445 879*. 38 239.7705 1189.05 85.1935 880.51 227.3083 1204.77 65.6098 883.24 257.2632 1221. 41 56.3640 884.68 256.2565 1231. 02 39.2733 889.28 278.4573 1235.36 47.9523 894.76 312.3086 1238.28 46.0693 898.04 272.4497 1260.41 0.0000 900.72 271. 5594 1271.87 26.1546 903.28 251.0779 1274.44 37.8051 911.20 279.5171 1274.54 37.8051 912.08 258.8086 1291.59 34.0836 923.98 0.0000 1298.22 0.0000 926.50 272.9045 1312. 11 33.2903 929 .11 303.3849 1332.49 45.2813 937.49 291. 4531 1362.66 0.0000 944.13 316.3708 1365.19 14.8901 946.00 296.4102 1368.63 0.0000 949.00 326.5671 1384.29 16.9575 954.55 0.0000 1408.01 17.0591 962. 31 272.4967 1457.56 0.0000 964. 08 302.6686 1460.82 12.1978 966 .17 281. 6951 1489.16 21.2862 968. 97 258.0931 1505.03 11.5049 983.53 220.2847 1584.12 11.5062 . 984.45 0.0000 1596.21 12.5867 996.26 240.8478 1620.50 10.5450 1001.03 240.1547 1621.92 14.0649 Page 3385 of 5809 Effective 3/25/2010 Radiochemistry Balch Checklist Revision 1 Effective March 2010 10/03/16 1596249 Batch# ________ _ Gamma Solid MJWC Product: ________ _ Date: 10/03/16 Criteria: Yes No Comments Sample Solids are less than or equal to 100 mq for GAB. n/a Samples have been blank corrected (If required). n/a Blank correction reoorted included flf reouired). If activity less than lOx MDA/ MDC, error Is less than or equal to 1S0% of sample activity. ../ If greater than 10* MDA/ MDC, error Is 40% or less, If'--*-*** the MOA/ MD<" error Instrument source check Is within limits. Instrument bko ch0ck is within limits. ../ Method RDL/ LLD has been met. ../ If duplicate activities are: Less than S* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, ../ Or meets the client's regulred RER acceetance criteria. Tracer yield Is 15-125%
Carrier yield 25-125%. (Or meets the cllent's contract acceptance criteria). 'n / ;i Method blank ls less than the RDL/ LLD. ../ of Samele was run within hold time. J DER Samole was correctl'i preserved If rcgulred. ../ Smears Taken for Radioactive batches. n/a Method Spike and LCS are wlthin.7S-125% Ir or the client's cnntract accentance criterl" l, ./ No blank spaces on data forms. ./ Ali line outs Initialed and dated. l!ll!..1r..-Ul.5.Cl:ill.tlon errors i\I.e..il.DJlil Aux data is correct. ./ Cllent Special regulrements pane has been checked. ./ Raw Data and I or soectrum are Included and oroocrlv statused. ../ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ./ valunc un*lfh*d Hit lif ./ llatCb !lDtlm:d (otn ./ 1563940 Batch Data Excention Renorts IDERl comnleted if anollcable. ./ DER 1563940 Batch Data Exception Reports (DER) second reviewed. / Dlsoositlon verified to be comoleted. 8JLqyot Correction completed If reoulred n/a Review sample historical results if available ../ {If REMP, results above MDC have been verified bu historical results recount or re-analvsls. l Primary Review Performed By: ____ jr"-1-'( __ _ Secondary Review Performed -3 ** I lo Page 3386 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 03-0CT-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1596249 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE HASL 300, 4.5.2.3/Ga-01-R Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1563940 Revision No.: 1 Type: Process Client Code: MJWC Samples 405235 021, *022, 023, 024, 025, 026, 027, 028, 029, 030, 031, Samples were analyzed in a timely manner upon receipt. Reporting 032, 033, 034, 035, 036, 037, 038, 039, 040, and 1203621355 (duplicate) results. were received outside of the holding period. , Originator's Name: Data Validator/Group Leader: Spencer Collins 03-0CT-16 Michael Hilton 03-0CT-16 Page 1 Page 3387of5809 < Gamma Spec Queue Sheet 09/13/2016 Batch #: 1596249 First Client DueDate:l0/04/2016 Internal Due Date: 09/30/2016 Analyst: MXRl Gamma LCS Isotope: .Mixed Gamma LCS Code: Prep Date: __ Initials: __ __ _ Expiration Date: Y / 1 \ 3 f. Vol: \

0 Sample ID Client Description I Container ID Type 405235021-1 405235022-1 405235023-1 405235024-1 405235025-1 405235026-1 405235027-1 .:0523:::028-l 405235029-1 -105235030-1 405235031-1 405235032-1 405235033-1 405235034-1 405235035-1 405235036-1 405235037-1 405235038-1 405235039-1 405235040-1 4.2B.R.2.3 4.2B.R.l.3 4.2B.R. l l.2 4.28.R.2.2 4.2B.R.1.2 4.2C.R.I.3 4.2C.R.l.4 4.3.ARl.3 4.3.B.R.l.3 4.3A.R.2.3 4.3.BRl9.2 4.3B.R.3.3 4.38.R.3.4 4.3.B.R.l.4 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2.4 4.4C.R.1.3 4.4C.R.1.4 4.4D.R.1.3 1203621354-1 MB 1203621355-1 DUP 4.4C.R.1.3(405235038) 1203621356-1 LCS I GEL Laboratories LLC, Radiochemistry Division SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE .. SAi\lPLE SAMPLE SAMPLE SAMPLE SAJ\-IPLE SAMPLE SAMPLE SAMPLE SAMPLE SAI\>IPLE SAMPLE SAMPLE SAMPLE MB DUP LCS Hazard Code Library: 2(e LI J) Client MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWC001 MJWCOOl MJWCOOl MJWCOOJ MJWCOOl MJWCOOl MJWCOOl MJWCOOI MJWCOOl MJWCOOI M.JWCOOl MJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL* SOIL SOIL SOIL SOIL Balance _____ _ Sealing Dateffime Collect Date Geometry Detector (if Applicable) 0S-0Ec-1514:11:oo-{tf r AN 16uo5 g 7 I tf ff1.--ll It 08-DEC-15 13:43:00 m--161.105 g ('6 ) 02-DEC-1510:40:00\Z_f?...r-' 08-DEC-1514:13:00 *n:ei---4--+--13_s_.96..,,2_g_!--__ 08-DEC-15 13:38:00 flf-.'\,,.l---t----t--l-3_8._24,.,,.4_g-r-l ---=2.,..--+---+-----; 08-DEC-15 +---l------1 OS-DEC-15 10:19:00 \lf1---+--+-i --+-----1 23-l'\OV-15 14:50:00 ft¥-I 125.516 g I 'i i 23-NOV-1511:10:QOTI.{-+j---f-----i 23-NOY-15 14:44:00Rf 131.12 g '2.o I 26-NOV-15 14:25:00"R'f-;--, -+---;,-13""'9-.6-17-g-+j---=o3""2..--+--i-----; 23-NOV-15 11 J---+----+j_l4_6._94_7_g_,_ __ 3-"" __ 23-NOV-15 11:53:00Q? 166.788 g I 1$ I 23-NOV-15 11 :20:0°UR r---+-1--1--l..,..52_.4..,,.87_g--+1--...,1..-=%°""--+-,,--+-----i 23-NOV-15 11 :06:00 ... 23-1\0V-15 11:12:0!\\f...;---i---+--1_6_2._25_7_g--+j __ _, '3* * ....., c-+---+-----i 30-NOV-15 11:19:00 1--;---'--11_s_. 7_5_6 -g-+-1 __ L\.-"-'-.1--'-l---+------1 30-NOV-15 10:40:00'1., _17_0._19-:2-g_,_ll __ ---1-----; 30-NOV-15 10:43:00'fU?,,,_ _ _,___-+_11_5_.3_26_g_,l ___ ... -------< 112.014g n 1 ll hl.-\\v -+-----!-------< 30-NOV-15 I 11 D' Ott i;--1.1 tt\ P-*\ \ \."> 11f1---+_--------.. Data Reviewed By: Jr:t-3-I k,, Page 1 ol 1 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:09.35 *****************************************************************************.***
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM07.CNF;484 Background date : Z-OCT-2016 11:00:17. Sample date : 8-DEC-2015 14:17:00. Acquisition date : 3-0CT-2016 08:57:41. Sample ID : G405235021 Sample quantity : 1.61305E+02 GRAM Detector name : GAM07 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.50 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 4 4 1 1 0 0 0 0 0 0 0 0 0

0 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 Page 3389 of 5809 Energy 62. 66* 70.49 74.85* 77.17 87.24 89.87 92.89* 115. 04 128.68 185.83* 209.68 238.46* 242.08 252.03 269.99 281.65 295.17* 302.16* 338.46* 351. 81* 463.69 485.37 510.66* 514.25 583.25* 609.13* 661. 74 665.33 711.67 728.14* 830.98 852.04 861.03 911.88* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 18 19 124 210 75 30 74 15 48 83. 74 288 70 24 60 26 128 44 50 192 16 40 25 19 103 146 46 16 8 13 12 8 27 91 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 180 1.05 125 1. 37 .170 1. 31 140 1.07 114 1.16 136 1. 02 155 1.47 86 0.60 176 0.63 133 1.20 97 1. 48 122 1. 21 104 1. 02 37 0.92 112 4.94 38 1. 60 81 1.17 84 4.80 63 0.91 71 1.32 31 1. 37 69 12.38 27 2.04 20 2.04 41 1. 27 33 1. 4 8 34 1. 04 13 1. 88 28 0.78 36 0.92 11 1. 50 14 0.67 29 1.54 35 2.35 125.81 141. 47 150.19 154.82 174.95 180.21 186.26 230.55 257.81 372.09 419.78 477.32 484.57 504.47 540.38 563.70 590.72 604.69 677.29 703.97 927.70 971.04 1021.61 1028.79 1166.76 1218.51 1323.73 1330.89 1423.57 1456.50 1662.14 1704.25 1722.24 1823.92 122 140 146 146 172 172 183 228 253 366 414 474 482 501 530 558 584 597 672 698 922 957 1014 1014 1162 1213 1319 1328 1419 1449 1655 1694 1715 1815 9 4.88E-03143.9 6 5.38E-03 94.3 16 3.46E-02 20.9 16 5.84E-02 11.1 11 2.08E-02 23.9 11 8.32E-03 62.4 9 2.07E-02 34.4 6 4.24E-03 99.2 11 l.33E-02 55.4 11 2.30E-02 30.0 11 2.05E-02 28.5 8 8.0lE-02 9.0 9 1. 94E-02 31. 3 6 6.78E-03 44.4 16 l.67E-02 41.4 11 7.12E-03 51.9 13 3. 54E-02 17. 2 16 1. 22E-02 49. 5 9 1.40E-02 32.4 14 5.34E-02 11.9 9 4.47E-03 67.5 30 1.lOE-02 62.7 20 7. 03E-03 61. 4 20 5.24E-03 55.9 12 2.86E-02 16.2 14 4. 07E-02 11. 8 10 l.29E-02 27.9 8 4.31E-03 48.7 12 2.09E-03149.l 12 3.55E-03 99.6 11 3.25E-03 66.7 14 2.22E-03105.3 17 7.47E-03 50.3 22 2.53E-02 19.6 Fit 2.90E+OO 4.37E+OO 2.04E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235021 Acquisition date 3...:ocT-2016 08:57:41 Pk :tt Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964. 23 23 11 1. 35 1928.61 1922 11 6.25E--'0J 35.3 36 0 968.59* 58 9 1. 50 1937.32 1933 10 l.62E-02 16.9 37 0 991. 95 13 1 1. 04 1984.05 1981 6 3.49E-03 32.1 38 0 1055.78 7 16 4.25 2111. 68 2103 13 l.93E-03125.6 39 0 1102.76 12 15 1. 34 2205.63 2200 10 3.33E-03 66.9 40 0 1119. 87 41 12 1. 95 2239.84 2231 16 l.14E-02 24.6 41 0 1128.91 14 2 3.21 2257.93 2253 9 3.86E-03 33.0 42 0 1238.14 12 9 0.64 2476.37 2473 7 3.43E-03 50.8 43 0 1376.74 20 3 1. 40 2753.54 2746 14 5.43E-03 30.4 44 0 1460.29* 304 7 1. 93 2920.63 2913 14 8.44E-02 6.1 45 0 1764.35* 29 3 1. 45 3528.71 3522 12 8.lOE-03 23.5 Flag: "*" = Peak area was modified by background subtraction Page 3390 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:58:11 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 14:17:00 G405235021 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:57:41 161. 30 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA7 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3391 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.50 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.122E+OO 1.148E+Ol l.148E+Ol 12.23 OK KR-85 514.00 0.43* 2.620E+OO 8.514E+OO 8.986E+OO 111. 77 OK SR-85 514.00 96. 00* 2.620E+OO 3.849E-02 9.489E-01 111. 77 OK CD-109 88.03 3.70* 5.745E+OO 1.334E+OO 2.093E+OO 80. 72 OK SN-126 64.28 9.60 3.624E+OO Line Not Found Absent 86.94 8.90 5.745E+OO 5.546E-01 5.546E-01 80. 72 OK 87.57 37.00* 5. 745-E+OO l.334E-01 1.334E-01 80. 72 OK BA-137M 661.66 89.90* 2 .138E+OO 1.205E-01 1.228E-01 55.70 OK CS-137 661.66 85.10* 2.138E+OO 1.273E-01 1. 297E-01 55.70 OK TL-208 277.37 6.60 4.377E+OO Line Not Found Absent 583.19 85.00* 2.365E+OO 2.589E-01 2.589E-01 32.49 OK 860.56 12.50 1. 736E+OO 5.982E-01 5.982E-01 100.52 OK PB-212 74.82 10.28 4.784E+OO 1.070E+OO 1.070E+OO 63.93 OK 77 .11 17.10 4.995E+OO 1.533E+OO l.533E+00 22 .11 OK 238.63 43.6.0* 4.933E+00 7.477E-01 7.477E-01 17.95 OK 300.09 3.30 4.103E+OO Line Not Found Absent BI-214 609.32 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 OK 1120.29 14.92 1.406E+OO 9.123E-01 9.126E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 OK PB-214 74.82 5.80 4.781E+OO Line Not Found <<INT Reject 77 .11 9.70 4.995E+OO 2.703E+OO 2.704E+OO 22 .11 OK 87.09 3.41 5.736E+OO Line Not Found <<INT Reject 242.00 7.25 4.877E+OO Line Not Found <<INT Reject 295.22 18.42 4.160E+OO 9.078E-01 9.082E-01 34.41 OK 351. 93 35.60* 3.593E+OO 8.043E-01 8.045E-01 23.81 OK RN-222 609.32 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 OK 1120.29 14.92 1.406E+OO 9.123E-01 9.126E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8. 922E-*Ol 47.05 OK RA-224 240.99 4.10* 4.876E+00 3.389E-01 3.389E-01 394.49 OK RA-226 609.32 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 OK 1120.29 14.92 l.406E+OO 9.123E-01 9.126E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 OK AC-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.711E+OO 6.479E-01 6.479E-01 64.74 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835. 71 1. 61 1.777E+OO Line Not Found Absent 911. 20 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39.13 OK 968. 97 15.80 1.581E+OO l .112E+OO 1.112E+OO 33.90 OK RA-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3. 711E+OO 6.479E-01 6.479E-01 64.74 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39.13 OK 968. 97 15.80 1. 581E+OO 1.112E+OO 1.112E+OO 33.90 OK TH-228 74.82 10.28 4.784E+OO 1.070E+OO 1. 070E+OO 63.93 OK 77 .11 17.10 4.995E+OO 1.533E+OO 1.533E+OO 22 .11 OK 238.63 43.60* 4.933E+00 7.477E-01 7.477E-01 17.95 OK 300.09 3.30 4.103E+00 Line Not Found Absent TH-230 609.32 45.49* 2.284E+oo 7.086E-01 7.086E-01 23.69 OK Page 3392 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 l.406E+OO 9.123E-01 9.123E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 OK PA-231 283.69 1. 70 4.298E+OO Line Not Found Absent 301.36 5.35* 4.080E+OO 1.090E+OO 1.090E+OO 99.01 OK TH-232 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3. 711E+OO 6.479E-01 6.479E-01 64.74 OK 835. 71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39.13 OK 968. 97 15.80 1. 581E+OO 1.112E+OO 1.112E+OO 33.90 OK TH-234 63.29 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 OK 92.59 4.23 6.053E+OO 1.779E+OO 1. 779E+OO 68.74 OK U-234 609.32 45.49* 2.284E+OO 7.086E-01 7.086E-01 23.69 OK 1120.29 14.92 l.406E+OO 9.123E-01 9.123E-01 49.11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 OK U-235 89. 96 3.47 5.897E+OO 8.997E-01 8.997E-01 124.84 OK 93.35 5.60 6.053E+OO 1.344E+OO 1.344E+OO 68.74 OK 143.76 10.96* 6.563E+00 Line Not Found Absent 163.33 5.08 6.266E+00 Line Not Found Absent 185.72 57.20 '5.856E+OO 1. 417E-01 1. 417E-01 59.94 , OK 205.31 5.01 5. 496E+OO Line Not Found Absent U-238 63.29 3.70* 3.418E+00 8.828E-01 8.828E-01 287.78 OK 92.59 4.23 6.053E+OO 1. 779E+OO 1. 779E+OO 68.74 OK AM-243 43.53 5.90 6.933E-01 Line Not Found Absent 74.66 67.20* 4.784E+OO 1.637E-01 1.637E-01 63.93 OK ANH-511 511. 00 100.00* 2.635E+OO 4.932E-02 4.932E-02 122.78 OK Flag: "*" = Keyline Page 3393 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:58:12.27 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l *
Acquisition date 3-0CT-2016 08:57:41 Sensitivity : 3.000 *
Detector ID GAM07 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Analyst initials: MXRl *
Sample ID G405235021 Sample Quantity 1.6130E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date . 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
Eff. File : DKAlOO:'[CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96'-sigma) (pCi/GRAM K-40 1.148E+Ol l.376E+OO 6.020E-01 KR-85 8.986E+00 9.843E+OO 1.069E+Ol SR-85 9.489E-01 1.039E+OO 1.129E+OO CD-109 2.093E+OO 1.656E+OO 1.856E+OO SN-126 1.334E-01 1.055E-01 l.188E-01 BA-137M 1.228E-01 6.702E-02 6.972E-02 CS-137 1.297E-01 7.080E-02 7.365E-02 TL-208 2.589E-01 8.244E-02 6.287E-02 PB-212 7.477E-01 l.315E-01 1. 031E-01 BI-214 7.089E-01 l.646E-01 1.049E-01 PB-214 8.045E-01 1.877E-01 1.178E-01 RN-222 7.089E-01 1.646E-01 l.049E-01 RA-224 3.389E-01 l.310E+00 1.312E+OO RA-226 7.089E-01 1.646E-01 1.049E-01 AC-228 1.020E+00 3. 911E-01 2.008E-01 RA-228 1.020E+OO 3. 911E-01 2.008E-01 TH-228 7.477E-01 1.315E-01 1. 031E-01 TH-230 7.086E-01 1.645E-01 1.048E-01 PA-231 1.090E+00 1.058E+OO 6.675E-01 TH_..:232 1.020E+OO 3. 911E-01 2.008E-01 TH-234 8.828E-01 2.490E+OO 1. 888E+OO U-234 7.086E-01 1.645E-01 l.048E-01 U-235 3.069E-02 1.661E-01 3.129E-01 U-238 8.828E-01 . 2. 490E+OO 1. 888E+OO AM-243 1.637E-01 1.026E-01 7.753E-02 ANH-511 4.932E-02 5.935E-02 4. 372E-02 Non-Identified Nuclides .Nuclide BE-7 NA-22 NA-24 AL-26 Page 3394 of 5809 Key-Line Activity (pCi/GRAM 2.392E+OO -4.722E-03 0.000E+OO 6.485E-03 K.L. Cnt Uncert MDA ( 1. 96-sigma) _(pCi/GRAM 9.940E+OO 3.491E-02 1. 960E+41 3.382E-02 1. 866E+Ol 6.991E-02 O.OOOE+OO 7.502E-02 NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SC-46 -1.593E-02 2. 996E-01 6.153E-01 FAIL ABUN V-48 O.OOOE+OO 1.277E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.367E+02 O.OOOE+OO SHORT HLIF MN-54 5.176E-02 6.098E-02 1. 2 69E-01 NOT IDENT. C0-56 -2.602E-01 4.253E-01 6.647E-01 FAIL ABUN MN-56 O.OOOE+OO l.702E+41 O.OOOE+OO SHORT HLIF C0-57 -3.235E-02 3.999E-02 7.039E-02 NOT IDENT. C0-58 -3.988E-01 5.759E-01 9.569E-01 NOT IDENT. FE-59 2.626E+OO 6.765E+OO 1.300E+Ol NOT IDENT. C0-60 l.241E-02 3.036E-02 6.856E-02 NOT IDENT. ZN-65 5.526E-02 1. 769E-01 3. 311E-01 NOT IDENT. GE-68 -4.394E-01 2.136E+OO 4.149E+OO NOT IDENT. AS-73 -l.865E+OO 6.599E+OO l.291E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.387E+03 O.OOOE+OO SHORT HLIF SE-75 -2.194E-01 2.022E-01 3.164E-01 NOT IDENT. BR-77 O.OOOE+OO 2. 331E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.800E+02 O.OOOE+OO SHORT HLIF RB-83 1.042E-02 5.040E-01 l.004E+OO NOT IDENT. RB-86 O.OOOE+OO 2.604E+04 O.OOOE+OO SHORT HLIF Y-88 3.393E-03 9.615E-02 2.683E-01 NOT IDENT. Y-91 1.990E+02 6.222E+02 l.242E+03 NOT IDENT. NB-94 -5.126E-03 2.760E-02 5.135E-02 NOT IDENT. NB-95 -5.377E-01 8.952E-01 1.524E+OO NOT IDENT. NB-95M 1.132E+OO 1.907E+OO 3.707E+OO NOT IDENT. ZR-95 -5.668E-02 1.476E+OO 2. 771E+OO NOT IDENT. NB-97 O.OOOE+OO l.082E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1.168E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.603E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.738E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 8.089E-02 5.978E-02 FAIL ABUN RH-102 -2.224E-02 5.089E-02 9.190E-02 NOT IDENT. RU-103 8.950E-02 4.626E+OO 9.162E+OO FAIL ABUN RH-106 l.541E-01 4.129E-01 8.536E-01 NOT IDENT. RU-106 1. 541E-01 4.129E-01 8.536E-01 NOT IDENT. AG-108M -6.525E-03 2.718E-02 5.150E-02 NOT IDENT. AG-llOM -3.167E-02 7.927E-02 l.533E-01 NOT IDENT. SN-113 -2.884E-02 2.214E-01 4.269E-01 NOT IDENT. CD-115 O.OOOE+OO 2.764E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.764E+04 O.OOOE+OO SHORT HLIF TE-123M -1.079E-01 l.253E-01 2.145E-01 NOT IDENT. SB-124 1.146E-01 2.131E+OO 4.424E+OO NOT IDENT. SB-125 -5.414E-02 8.818E-02 l.605E-01 FAIL ABUN TE-125M 6.919E+Ol 2.305E+02 4.499E+02 NOT IDENT. I-126 O.OOOE+OO l.004E+06 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 1.126E+06 O.OOOE+OO SHORT HLIF SB-127 0.000E+OO *1.888E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.311E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.572E+41 *O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO. 3.208E+26 O.OOOE+OO SHORT HLIF BA-133 -l.338E-02 4.086E-02 6.908E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 2.153E-02 5.269E-02 1. 041E-01 NOT IDENT. CS-135 7.379E-02 l.144E-01 2.418E-01 NOT IDENT. I-135 O.OOOE+OO 1.868E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2. 951E+05 O.OOOE+OO SHORT HLIF CE-139 -l.250E-02 l.054E-01 1.927E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 021E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3 .117E+05 O.OOOE+OO SHORT.HLIF CE-141 1.388E+Ol 2.089E+Ol 4.126E+Ol NOT IDENT. CE-143 O.OOOE+OO l.515E+41 O.OOOE+OO SHORT HLIF CE-144 -1.287E-01 3.429E-01 5.708E-01 NOT IDENT. PM-144 2.690E-02 4.832E-02 l.005E-01 NOT IDENT. PR-144 2.365E+OO 4.201E+OO 8.747E+OO NOT IDENT. PM-146 1.296E-02 3.715E-02 7.623E-02 NOT IDENT. ND-147 O.OOOE+OO 2.875E+07 O.OOOE+OO SHORT HLIF PM-14'7 1.924E+02 6.547E+02 1.2B2E+03 NOT IDENT. PM-149 0.000E+OO 3.886E+40 O.OOOE+OO SHORT HLIF EU-150 -l.312E-03 2.262E-02 4.017E-02 FAIL ABUN EU-152 -5.561E-02 7.338E-02 l.339E-01 FAIL ABUN GD-153 -l.028E-01 l.661E-01 2.784E-01 . FAIL ABUN EU-154 -l.158E-02 8.558E-02 1.714E-01 NOT IDENT. EU-155 -3.814E-02 9.072E-02 1. 676E-01 FAIL ABUN TB-160 6.524E-01 l.255E+OO 2.906E+OO FAIL ABUN H0-166M 3.408E-02 9. 961E-02 l.135E-01 FAIL ABUN TM-171 -l.794E-01 l.546E+Ol 3. 096E+Ol NOT IDENT. HF-172 -1.lOlE-01 2.305E-01 3.809E-01 FAIL ABUN LU-172 -5.708E-02 7.403E-02 1.289E-01 FAIL ABUN LU-176 -8.387E-03 2.145E-02 3.656E-02 FAIL ABUN Page 3395 of 5809 HF-181 4.432E-01 3.660E+OO 7.316E+OO NOT IDENT. TA-182 6.389E-01 9.186E-01 1. 966E+OO FAIL ABUN RE-183 -7.564E-01 2.314E+OO 4.481E+OO NOT IDENT. RE-184 1. 372E+Ol 3.124E+Ol 6.567E+Ol NOT IDENT. W-188 1 .. 904E+Ol 1.023E+02 1.882E+02 FAIL ABUN IR-192 1. 089E-01 3.924E-01 7.923E-01 FAIL ABUN HG-203 -9.161E-01 2.069E+OO 3.528E+OO FAIL ABUN BI-207 2. 596E-02 4.647E-02 9.988E-02 FAIL ABUN PB-210 1.035E+OO 2.467E+OO 5. 096E+OO NOT IDENT. BI-211 O.OOOE+OO 5.170E-01 7.320E-01 FAIL ABUN PB-211 2.257E-01 5.095E-01 1. 070E+OO FAIL ABUN BI-212 4.770E-01 9.309E-01 1.119E+OO FAIL ABUN RN-219 -7.130E-02 3.350E-Ol 6.430E-01 FAIL ABUN RA-223 4.393E-02 5.413E-01 1. 076E+OO FAIL ABUN AC-227 -4.093E-02 1.944E-01 3.828E-01 NOT IDENT. TH-227 -4.093E-02 1.944E-01 3.828E-01 NOT IDENT. TH-229 6.714E-02 4.220E-01 7.859E-01 FAIL ABUN TH-231 4.393E-02 5.413E-01 l.076E+OO FAIL ABUN PA-233 8.350E-03 5.037E-02 1. 0*19E-01 NOT IDENT. PA-234 8.053E-02 2.328E-01 5.005E-01 NOT IDENT. PA-234M -6.592E-01 3.983E+OO 7.916E+OO NOT IDENT. NP-237 8.350E-03 5.037E-02 1.019E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 9.356E-02 2.179E-01 4.002E-01 NOT IDENT. PU-239 O.OOOE+OO 7.337E+02 6 .161E+02 FAIL ABUN AM-241 -8.491E-03 1.182E-01 2.151E-01 NOT IDENT. CM-243 2.499E-02 8.365E-02 1.642E-01 NOT IDENT. BK-247 -4.901E-02 7.077E-02 1. l 71E-01 NOT IDENT. CM-247 -2.554E-03 2.981E-02 5.820E-02 NOT IDENT. CF-249 l.748E-02 3.440E-02 7.092E-02 FAIL ABUN CF-251 1.018E-01 9.504E-02 l.944E-01 NOT IDENT. Page 3396 of 5809 VAX/VMS Nuclide*Identification Report Generated 3-0CT-2016 09:58:10.05 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 295 10.66* 1.122E+OO 1.148E+Ol 1.148E+Ol 12.23 KR-85 514.00 21 0.43* 2.620E+OO 8.514E+OO 8.986E+OO 111. 77 SR-85 514.00 21 96. 00* 2.620E+OO 3.849E-02
9.489E-01 111. 77 CD-109 88.03 99 3.70* 5.745E+OO 2.171E+OO 3.406E+OO 47.80 SN-126 64.28 ------9.60 3.624E+OO ------Line Not Found ------86.94 99 8.90 5.745E+OO 9 .-024E-01 9.024E-01 47.80 87.57 99 37.00* 5.745E+OO 2 .171E-01 2.171E-01 47.80 BA-137M 661. 66 50 89.90* 2.138E+OO l.205E-01 1.228E-01 55.70 CS-137* 661. 66 50 85.10* 2.138E+OO 1. 273E-01 1.297E-01 55.70 TL-208 277.37 ------6.60 4.377E+OO ------Line Not Found ------583.19 112 85.00* 2.365E+OO 2.589E-01 2.589E-01 32.49 860.56 28 12.50 1. 736E+OO 5.982E-01. 5.982E-01 100.52 BI-211 72.87 ------1.23 4. 591E+OO ------Line Not Found ------351.06 221 12.92* 3.593E+OO 2.216E+OO 2.216E+OO 23.81 PB-212 74.82 167 10.28 4.784E+OO 1.582E+OO 1.582E+OO 41. 77 77 .11 281 17.10 4.995E+OO l'. 533E+OO 1.533E+OO 22 .11 238.63 346 43.60* 4.933E+OO 7.477E-01 7.477E-01 17.95 300.09 ------3.30 4.103E+OO ------Line Not Found ------BI-214 609.32 158 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 1120.29 41 14.92 1.406E+OO 9.123E-01 9.126E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 PB-214 74.82 167 5.80 4.784E+OO 2.805E+OO 2.806E+OO 41.77 77 .11 281 9.70 4.995E+OO 2.703E+OO 2.704E+OO 22 .11 87.09 99 3.41 5.745E+OO 2.355E+OO 2.356E+OO 47.80 242.00 84 7.25 4.876E+OO l.099E+OO 1.lOOE+OO 62. 62 295.22 149 18.42 4.160E+OO 9.078E-01 9.082E-01 34.41 351. 93 221 35.60* 3.593E+OO 8.043E-01 8.045E-01 23.81 RN-222 609.32 158 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 *1120.29 41 14.92 1. 406E+OO 9.123E-01 9.126E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 RA-224 240.99 84 4.10* 4.876E+OO l.944E+OO 1.944E+OO 62.62 RA-226 609.32 158 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 1120.29 41 14.92 1.406E+OO *9.123E-01 9.126E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8. 922.E-01 47.05 AC-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 58 11.27 3. 711E+OO 6.479E-01 6.479E-01 64.74 794.95 ------4.25 l.849E+OO ------Line Not Found ------835.71 ------1. 61 1.777E+OO ------Line Not Found ------911. 20 94 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39 .13 968.97 60 15.80 1. 581E+OO* 1.112E+OO 1.112E+OO 33.90 RA-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 58 11. 27 3.711E+OO 6.479E-01 6.479E-01 64.74 794.95 ------4.25 1.849E+OO ------Line Not Found ------835. 71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 94 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39.13 968. 97 60 15.80 1. 581E+OO 1.112E+OO l .112E+OO 33.90 TH-228 74.82 167 10.28 4.784E+OO 1.582E+OO 1.582E+OO 41.77 Page 3397 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 281 17.10 4.995E+OO 1.533E+OO 1.533E+OO 22 .11 238.63 346 43.60* 4.933E+OO 7.477E-01 7.477E-01 17.95 300.09 ------3.30 4.103E+OO ------Line Not Found ------TH-230 609.32 158 45.49* 2.284E+OO 7.086E-01 7.086E-01 23.69 1120.29 41 14.92 1.406E+OO 9:123E-01 9.123E-01 49.11 1764.49 28 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 PA-231 283.69 ------1. 70 4.298E+OO ------Line Not Found ------301.36 51 5.35* 4.080E+OO l.090E+OO 1.090E+OO 99.01 TH-232 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 58 11. 27 3.711E+OO 6.479E-01 6.479E-01 64.74 835. 71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 94 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39.13 968.97 60 15.80 1. 58*1E+OO l .112E+OO 1.112E+OO 33.90 TH-234 63.29 24 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 92.59 98 4.23 6.053E+OO
1.779E+OO 1. 779E+00 68.74 U-234 609.32 158 45.49* 2.284E+00 7.086E-01 7.086E-01 23.69 1120.29 41 14.92 1.406E+OO 9.123E-01 9.123E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 ' U-235 89. 96 40 3.47 5.897E+OO 8.997E-01 8.997E-01 124.84 93.35 98 5.60 6.053E+00 1.344E+OO 1.344E+OO 68.74 143.76 ------10. 96* 6.563E+OO ------Line Not Found ------163.33 ------5.08 6.266E+OO ------Line Not Found ------185.72 102 57.20 5.856E+OO 1.417E-01 1. 417E-01 59.94 205.31 ------5.01 5.496E+OO ------Line Not Found ------U-238 63.29 24 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 92.59 98 4.23 6.053E+00 1. 779E+00 1.779E+OO 68.74 AM-243 43.53 ------5.90 ) 6.933E-01 ------Line Not Found ------74.66 167 67.20* 4.784E+OO 2. 421E-01 2.421E-01 41.77 ANH-511 511. 00 28 100.00* 2.635E+OO 4.932E-02 4.932E-02 122.78 Flag: "*" Key line Page 3398 of 5809 Summary of Nuclide Activity Sample ID : G405235021 Acquisition date Page : 3 3-0CT-2016 08:57:41 Total number of lines in spectrum 45 Number of unidentified lines 6 Number of lines identified by NID 39 Nuclide Type : Nuclide K-40 KR-85 SR-85 CD-109 SN-126 CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 10.56Y 64.840 461.400 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 06 24.7 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.148E+Ol 8.514E+OO 3.849E-02 2.171E+OO 2.171E-01 1.205E-01 l.273E-01 2.589E-01 2.216E+OO 7.477E-01 7.086E-01 8.043E-01 7.086E-01 1.944E+OO 7.086E-01 1.020E+OO l.020E+OO 7.477E-01 7.086E-01 l.090E+OO 1.020E+OO 8.828E-01 7.086E-01 1. 417E-01 8.828E-01 2.421E-01 4.932E-02 3.928E+Ol 3.928E+Ol Decay Corr pCi/GRAM 1.148E+Ol 8.986E+OO 9.489E-01 3.406E+OO 2.171E-01
l.228E-01 1. 2 97E-01 2.589E-01 2.216E+OO 7.477E-01 7 .. 089E-01 8.045E-01 7.089E-01 1.944E+OO 7.089E-01 1.020E+OO 1.020E+OO 7.477E-01 7.086E-01 l.090E+OO 1.020E+OO 8.828E-01 7.086E-01 1.417E-01 8.828E-01 2. 421E-01 4.932E-02 4.190E+Ol 4.190E+Ol 86.67% Decay Corr 2-Sigma Error 0.140E+Ol 10.04E+OO 10.61E-01 1.628E+OO l.038E-01 0.684E-01 0. 722E-01 *0.841E-01 0.528E+OO 1. 342E-0.1 1.679E-01 1.915E-01 l.679E-01 1.218E+OO l.679E-01 0.399E+OO 0.399E+OO l.342E-01 1.679E-01 1.079E+00 0.399E+OO 25.40E-01 l.679E-01 0.850E-01 25.40E-01 1. OllE-01 6.056E-02 "M" Manually accepted 2-Sigma %Error 12.23 111. 77 111. 77 47.80 47.80 55.70 55.70 32.49 23.81 17.95 23.69 23.81 23.69 62. 62 23.69 3'9 .13 39.13 17.95 23.69 99.01 39.13 287.78 23.69 59.94 287.78 41.77 122.78 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3399 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235021 Acquisition date : 3-0CT-2016 08:57:41 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 70.49 26 168 1. 37 141. 47 140 6 5.38E-03 **** 4.34E+OO T 0 115. 04 20 111 0.60 230.55 228 6 4.24E-03 **** 6.65E+OO T 0 128.68 61 224 0.63 257.81 253 11 1.33E-02 **** 6.69E+OO T 0 209.68 90 118 1. 48 419.78 414 11 2.05E-02 56.9 5.42E+OO T 0 252.03 29 44 0.92 504.47 501 6 6.78E-03 88.7 4.73E+OO T 0 269.99 71 132 4.94 540.38 530 16 1. 67E-02 82.7 4.47E+OO T 0 281.65 30 45 1. 60 563.70 558 11 7.12E-03 **** 4.32E+OO T 0 463.69 18 34 1. 37 927.70 922 9 4.47E-03 **** 2.85E+OO T 0 485.37 44 77 12.38 971.04 957 30 1.lOE-02 **** 2.75E+OO 0 665.33 . 17 14 1. 88 1330.89 *1328 8 4. 31E-03 97.3 2.13E+OO T 0 711. 67 8 30 0.78 1423.57 1419 12 2.09E-03 **** 2.02E+OO T 0 728.14 14 38 0.92 1456.50 1449 12 3.55E-03 **** 1.98E+OO T 0 830.98 12 12 1. 50 1662.14 1655 11 3.25E-03 **** 1. 7 9E+OO T 0 852.04 8 15 0.67 1704.25 1694 14 2.22E-03 **** 1. 7 5E+OO 0 964. 23 23 11 1. 35 1928.61 1922 11 6.25E-03 70.7 1.59E+OO T 0 991. 95 13 1 1. 04 1984.05 1981 6 3.49E-03 64.1 1.55E+OO 0 1055.78 7 16 4.25 2111. 68 2103 13 1. 93E-03 **** 1.47E+OO 0 1102.76 *12 15 1. 34 2205.63 2200 10 3.33E-03 **** 1.42E+OO 0 1128.91 14 2 3.21 2257.93 2253 9 3.86E-03 66.0 1.40E+00 T 0. 1238.14 12 9 0.64 2476.37 2473 7 3.43E-03 **** 1.29E+OO T 0 1376.74 19 3 1*.40 2753.54 2746 14 5.43E-03 60.8 1.18E+00 Flags: "T" = Tentatively associated Page 3400 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:58:24.66 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l *
date 3-0CT-2016 08:57:41 Sensitivity : 3.000 *
Detector ID GAM07 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : SOLID *
Sample ID G405235021 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : l.6130E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 11:09:59 Eff. Geometry : CAN *
Eff.' File : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.479E-01 4.737E+OO 5.003E-01 8.780E-01 5.622E-02 3.142E-02 3.319E-02 2.819E-02 4.843E-02 4.617E-02 5.372E-02 4.617E-02 6.227E-01 4.617E-02 8.536E-02 8.536E-02 4.843E-02 4.615E-02 3.034E-01 8.536E-02 8.907E-01 4.615E-02 1.471E-01 8.907E-01 3.662E-02 1.938E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3401 of 5809 Le (pCi/GRAM 8.209E+OO 2.866E-02 O.OOOE+OO 3.063E-02 2.621E-01 NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132
TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3402 of 5809 O.OOOE+OO O.OOOE+OO 5.638E-02 2.782E-01 O.OOOE+OO 3.265E-02 4 .114E-01 5.652E+OO 2.844E-02 l.445E-01 1. 779E+OO 6.035E+OO 0.000E+OO 1. 441E-01 O.OOOE+OO O.OOOE+OO 4.395E-01 O.OOOE+OO 8.482E-02 5.566E+02 2.249E-02 6.748E-01 1. 715E+OO 1.227E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 2.812E-02 3.985E-02 4.049E+OO 3.758E-01 3.758E-01 2.334E-02 6.463E-02 l.947E-01 O.OOOE+OO O.OOOE+OO l.OOOE-01 l.784E+OO 7.136E-02 2.106E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.138E-02 0 ."OOOE+OO 4.666E-02 l. ll 7E-01 O.OOOE+OO O.OOOE+OO 9.022E-02 0.000E+OO 0.000E+OO 1.936E+Ol O.OOOE+OO 2.664E-01 4.464E-02 3.884E+OO 3.426E-02 O.OOOE+OO 5.970E+02 O.OOOE+OO 1.822E-02 5.987E-02 l.302E-01 7.027E-02 7.819E-02 1.231E+OO 5.083E-02 1.447E+Ol 1.783E-01 5.482E-02 l.652E-02 3.261E+OO SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF . SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLl'F NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210* BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3403 of 5809 8.720E-Ol 2.099E+OO 2.925E+Ol 8.638E+Ol 3. 621E-01 1.602E+OO 4.398E-02 2. 396E+OO 3.519E-01 4.804E-01 5.105E-Ol 2.905E-01 4.950E-01 1. 7 64E-01 1. 764E-01 3.663E-01 4.950E-01 4.663E-02 2.170E-01 3.462E+OO 4.663E-02 0.000E+OO 1.873E-01 2.920E+02 1. OllE-01 7.695E-02 5.366E-02 2.625E-02 3.244E_.:02 9.076E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:58:30.17 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l *
Acquisition date 3-0CT-2016 08:57:41 Sensitivity : 3.000 *
Detector ID GAM07 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
Sample date 8-DEC-2015 14:17:00 Nuclide Library : SOLID *
Sample .ID G405235021 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity 1.6130E+02 GRAM *
Quantity Err(%) 1.2399E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 19-AU:G-2016 11:09:59 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
Combined Activity-MDA Report NOTE:* Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96:.....sigma) K-40 1.148E+Ol 1. 501E+OO 1. 501E+OO KR-85 8.986E+OO 9 .. 849E+OO 9.849E+OO SR-85 9.489E-01 1.040E+OO l.040E+00 CD-109 2.093E+OO 1. 672E+OO 1. 672E+OO SN-126 l.334E-01 l.064E-01 1.064E-01 BA-137M 1.228E-01 6.723E-02 6.723E-02 CS-137 l.297E-01 7.102E-02 7.102E-02 TL-208 2.589E-01 8.317E-02 8.317E-02 PB-212 7.477E-01 l.374E-01 1.374E-01 BI-214 7.089E-01 l.674E-01 l.674E-01 PB-214 8.045E-01 l.907E-01 1.907E-01 RN-222 7.089E-01 1. 674E-01 l.674E-01 RA-224 . 3.389E-01 l.315E+00 1.315E+OO RA-226 7.089E-01 1.674E-01 1. 674E-01 AC-228 l.020E+00 3.946E-01 3.946E-01 RA...:.228 1.020E+OO 3.946E-01 3.946E-01 TH-228 7.477E-01 l.374E-01 1.374E-01 TH-230 7.086E-01 l.673E-01 l.673E-01 PA-231 1.090E+OO 1.083E+OO 1.083E+OO TH-232 1.020E+OO 3.946E-01 3.946E-01 TH-234 8.828E-01 2.497E+OO 2.497E+OO U-234 7.086E-01 l.673E-01 l.673E-01 U-235 3.069E-ci2 l.661E-01 1.661E-01 U-238 8.828E-01 2.497E+OO 2.497E+OO AM-243 1.637E-01 i.035E-01 1.035E-01 ANH-511 4. 932E...:02 5.938E-02 5.938E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.392E+OO 9.940E+OO 9.999E+OO NOT IDENT. NA-22 -4. 722E-03 3.491E-02 3.497E-02 NOT IDENT. NA-24 l.OOOE+41 2.950E+41 O.OOOE+OO SHORT HLIF AL-26 6.485E-03 3.382E-02 3.395E-02 FAIL ABUN Page 3404 of 5809 SC-46 -l.593E-02 2. 996E-01 2.997E-Ol FAIL ABUN V-48 5.642E+03 l.277E+04 l.302E+04 SHORT HLIF CR-51 -2.792E+02 3.369E+02 3.597E+02 SHORT HLIF MN-54 5. 17 6E-02 6.102E-02 6.532E-02 NOT IDENT. C0-56 -2.602E-01 4.254E-01 4.413E-01 FAIL ABUN MN-56 -l.OOOE+41 1. 703E+41 0.000E+OO SHORT HLIF C0-57 -3.235E-02 4.002E-02 4.259E-02 NOT IDENT. C0-58 -3.988E-01 5.762E-01 6.036E-01 NOT IDENT. FE-59 2.626E+OO 6.767E+00 6.870E+OO NOT IDENT. C0-60 l.241E-02 3.036E-02 3.087E-02 NOT IDENT. ZN-'65 5.526E-02 1. 769E-01 1.786E-01 NOT IDENT. GE-68 -4.394E-01 2.136E+OO 2.145E+OO NOT IDENT. AS-73 -1. 8 65E+OO 6.610E+OO 6.664E+OO NOT IDENT. AS-74 -4*. 685E+03 5.401E+03 5.799E+03 SHORT HLIF SE-75 -2.194E-01 2.025E-01 2.253E-01 NOT IDENT. BR-77 1.325E+38 1.147E+39 O.OOOE+OO SHORT HLIF SR-82 -1. 811E+02 6.801E+02 6.849E+02 SHORT HLIF RB-83 1.042E-02 5.040E-01 5.040E-01 NOT IDENT. RB-86 -3.319E+03 2.604E+04 2.608E+04 SHORT HLIF Y-88 3.393E-03 9.615E-02 9.617E-02 NOT IDENT. Y-91 1. 990E'+02 6.223E+02 6.287E+02 NOT IDENT. NB-94 -5.126E-03 2.760E-02 2.770E-02 NOT IDENT. NB-95 -5.377E-01 8.955E-01 9.277E-01 NOT IDENT. NB-95M 1.132E+OO 1.909E+OO 1.976E+OO NOT IDENT. ZR-95 -5.668E-02 1.476E+OO 1.477E+OO NOT IDENT. NB-97 -1.000E+41 1.083E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 l.168E+41 O.OOOE+OO SHORT HLIF M0-99 8.480E+31 1.604E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1. 741E+41 O.OOOE+OO SHORT HLIF RH-101 7.445E-02 8.201E-02 8.861E-02 FAIL ABUN RH-102 -2.224E-02 5.092E-02 5.190E-02 NOT IDENT. RU-103 8.950E-02 4.626E+OO 4.626E+OO FAIL ABUN RH-106 1.541E-01 4.130E-01 4.188E-01 NOT IDENT. RU-106 l.541E-01 4.130E-01 4.188E-01 NOT IDENT. AG'-108M -6.525E-03 2.718E-02 2.734E-02 NOT IDENT. AG-llOM -3.167E-02 7.928E-02 8.056E-02 NOT IDENT. SN-113 -2.884E-02 2.214E-01 2.217E-01 NOT IDENT. CD-115 1.042E+39 2.770E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -4.146E+04 8.778E+04 8.975E+04 SHORT HLIF TE-123M -l.079E-01 l.254E-01 l.345E-01 NOT IDENT. SB-124 1.146E.:...01 2 .131E+OO 2.132E+OO NOT IDENT. SB-125 -5.414E-02 8.821E-02 9.152E-02 FAIL ABUN TE-125M 6.919E+Ol 2.306E+02 . 2. 327E+02 NOT IDENT. I-126 1.053E+06 l.014E+06 1.120E+06 SHORT HLIF SB-126 -2.367E+04 1.126E+06 l.126E+06 SHORT HLIF SB-127 -7.599E+21 2.158E+22 O.OOOE+OO SHORT HLIF I-131 5.698E+08 4. 311E+09 4.318E+09 SHORT HLIF I-132 l.000E+41 l.855E+42 O.OOOE+OO SHORT HLIF TE-132 -l.446E+26 3.261E+26 O.OOOE+OO SHORT HLIF BA-133 -1.338E-02 4.086E-02 4.130E-02 FAIL ABUN I-133 -1.000!'.:+41 4 .115E+41 O.OOOE+OO SHORT HLIF CS-134 2.153E-02 5.270E-02 5.359E-02 NOT IDENT. CS-135 7.379E-02 l.145E-01 1.193E-01 NOT IDENT. I-135 -1.000E+41 7.026E+41 O.OOOE+OO SHORT HLIF CS-136 -6. 716E+02. 2. 951E+05 2. 951E+05 SHORT HLIF CE-139 -l.250E-02 l.054E-01 l.056E-01 NOT IDENT. BA-140 5.230E+05 1.021E+06 1.048E+06 SHORT HLIF LA-140 -5. 901E+04 3. ll 7E+05 3.129E+05 SHORT HLIF CE-141 1.388E+Ol 2.090E+Ol 2.181E+Ol NOT IDENT. CE-143 1.000E+41 1.519E+41 0. 000.E+OO SHORT HLIF CE-144 -l.287E-01 3.430E-01 3.478E-01 NOT IDENT. PM-144 2.690E-02 4.834E-02 4:984E-02 NOT IDENT. PR-144 2.365E+OO 4.203E+00 4.336E+OO NOT IDENT. PM-146 1.296E-02 3.716E-02 3.762E-02 NOT IDENT. ND-147 1.585E+07 2.876E+07 2. 964E+07 SHORT HLIF PM-147 l.924E+02 6.547E+02 6.604E+02' NOT IDENT. PM-149 1.561E+40 3.901E+40 O.OOOE+OO SHORT HLIF EU-150 -l.312E-03 2.262E-02 2.263E-02 FAIL ABUN EU-152 -5. 561E-02 7.345E-02 7. 761E-02 FAIL ABUN GD-153 -1.028E-01 1.662E-01 l.725E-01 FAIL ABUN EU-154 -l.158E-02 8.558E-02 8.574E-02 NOT IDENT. EU-155 -3.814E-02 9.076E-02 9.238E-02 FAIL ABUN TB-160 6.524E-01 l.255E+OO 1.289E+OO FAIL ABUN H0-166M 3.408E-02 9. 963E-02. 1.008E-01 FAIL ABUN TM-171 -l.794E-01 1.546E+Ol 1.546E+Ol NOT IDENT. HF-172 -1.lOlE-01 2.312E-01 2.364E-01 FAIL ABUN LU-172 -5.708E-02 7.426E-02 7.859E-02 FAIL ABUN LU-176 -8.387E-03 2.145E-02 2.178E-02 FAIL ABUN Page 3405 of 5809 HF-181 4.432E-01 3.661E+OO 3.666E+OO NOT IDENT. TA-182 6.389E-01 9.189E-01 9.630E-01 FAIL ABUN RE-183 -7.564E-01 2.317E+OO 2.342E+OO NOT IDENT. RE-184 1. 372E+Ol 3.141E+Ol 3.201E+Ol NOT IDENT. W-188 1.904E+Ol 1.023E+02 1.027E+02 FAIL ABUN IR-192 1. 089E-01 3.924E-01 3.955E-01 FAIL ABUN HG-203 -9 .161E-01 2.069E+OO 2. llOE+OO FAIL ABUN BI-207 2.596E-02 4.649E-02 FAIL ABUN PB-210 l.035E+OO 2.468E+OO 2.512E+OO NOT IDENT. BI-211 2.216E+OO 5.264E-01 l.129E+OO FAIL ABUN PB-211 2.257E-01 5.096E-01 5 .196E-01 FAIL ABUN BI-212 4.770E-01 9.312E-01 9.557E-01 FAIL ABUN RN-219 -7.130E-02 3.351E-01 3.367E-01 FAIL ABUN RA-223 4.393E-02 5.413E-01 5.417E-01 FAIL ABUN -4.093E-02 1.945E-01 1.953E-Ol NOT IDENT. TH-227 -4.093E-02 1.945E-01 1.953E-01 NOT IDENT. TH-229 6.714E-02 4.220E-01 4. 231E-01 FAIL ABUN TH-231 4.393E-02 5. 413E-01 5.417E-01 FAIL ABUN PA-233 8.350E-03 5.037E-02 5.051E-02 NOT IDENT. PA-234 8.053E-02 2.504E-01 2.530E-01 NOT IDENT. PA-234M -6.592E-01 3.984E+OO 3.995E+OO NOT IDENT. NP-237 8.350E-03 5.037E-02 5. 051E-02 NOT IDENT. NP-238 8.921E+40 4.010E+41 O.OOOE+OO SHORT HLIF NP-239 9.356E-02 2.180E-01 2.221E-01 NOT IDENT. PU-239 6.753E+02 7.343E+02 7.949E+02 FAIL ABUN AM-241 -8.49,lE-03 l.182E-01 l.183E-01 NOT IDENT. CM-243 2.499E-02 8.368E-02 8.444E-02 NOT IDENT. BK-247 -4.901E-02 7.146E-02 7.480E-02 NOT IDENT. CM-247 -2.554E-03 2.982E-02 2.984E-02 NOT IDENT. CF-249 1. 748E-02 3.443E-02 3.532E-02 FAIL ABUN CF-251 1.018E-01 9. 572E-02 l.061E-01 NOT IDENT. Page 3406 of 5809
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GAMMA* SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 61.8428 87.09 102.2612 136.47. 64.7451 45.60 62.2083 87.57 102.3518 140.51 0.0000 46.54 63.3312 88.03 102.4387 143.76 72.2641 49. 72 0.0000 88.34 102.4966 144.24 70.0137 51. 35 74.8469 88.47 102. 5211 145.44 60.9278 51. 87 68.1345 89. 96 95.0544 152.43 64.9585 52.39 69.2008 1093.63 95.1711 153.25 0.0000 52.97 74.1842 91.11 0.0000 323.87 67.4298 53.44 75.2502 92.59 70.7438 156.02 0.0000 54.07 73.4127 93.35 70.8389 158.56 0.0000 57.36 0.0000 94.56 53.9524 159.00 85.3753 57.53 81.9412 94.65 53. 9609 162.33 76.3286 57.98 82.0299 94.67 53. 9628 162.66 0.0000 59.27 77.9876 94.87 53.9818 163.33 72.8937 59.32 77.9969 97.43 77.0515 165.86 75.4746 59.54 84.6510 98.43 69.6799 176.31 64.4645 60. 96 86.2613 98.44 69'. 6809 176.60 0.0000 61.17 84.9756 99.53 71. 9578 177.52 43.0356 62. 93 92. 9871 100 .11 77.4036 181.07 0.0000 63. 29 93.0635 102.03 78.7321 181. 52 49.6352 63.58 93.1251 103.18 66.9956 184.41 67.4647 64.28 92.2697 103.37 67.0169 143.76 67.5621 66.73 99.4977 105.21 74.8086 193.51 59.6201 67.24 95.9074 105.31 74.8207 197.03 62.2862 125.81 90.2739 106.12 68.4049 198.01 47.6800 67.75 90.2875 106.47 73.8754 201.83 56.4633 69.67 94.7226 109.28 61.1137 203.43 60.2459 70.83 93.6003 111. 00 75.5056 205.31 52.5605 72. 81 81.7303 111.76 0.0000 210.85 37.9917 72. 87 81. 7407 114. 06 52.7769 215.65 51. 0373 74.66 97.0840 116.30 0.0000 222 .11 62. 6366 74.82 97 .1158 116.74 60.3543 227.09 57.9029 74.97 97.1461 119.76 56.5633 227.38 5-7. 9190 77 .11 97. 5672 121.12 53.3438 228.16 0.0000 78.74 97.8843 121. 22 54. 4.633 228.18 57. 9633 79.69 103.5927 121. 7 8 71.1948 116.74 57. 9633 80.12 100.9149 122.06 73.4499 235.69 39.3399 80.19 0.0000 122.92 63.5144 235. 96 41. 8882 80.57 101.0040 123.07 63.5284 238.63 81.4395 81.00 113.5508 265.00 69.1625 238.98 0.0000 81. 07 113.5666 125.81 85.0431 240.99 117.3233 81. 75 83.2068 127.23 74.0040 242.00 49.7807 83.79 84.9243 127.91 74.0765 244.70 47.3441 84.00 84.9584 129.30 74.2228 252.40 0.0000 85.43 94. 9630 131. 20 70.6635 252.80 39.9553 86.55 109.1559 133.02 67.8287 254.15 0.0000 86.79 102.2040 133.52 75.4181 256.23 49.9877 86.94 102.2330 136.00 68.1088 2 60. 90 0.0000 Page 3407 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 57.2988 355.39 0.0000 584.27 25.4238 2 64. 80 57.3069 356.01 39.1041 595.83 0.0000 265.00 54.7110 364.49 0.0000 427.87 25.6182 268.22 37.4448 366.42 0.0000 602.52 0.0000 269.46 37.4841 372 .51 32. 0113 604. 72 14.4377 270.03 37.5025 375.05 23.5774 607.14 19.2715 271.23 37.5401 377.52 32.1178 609.32 18.2195 273.65 0.0000 356.01 36.9941 610.33 18.2278 276.40 44.7173 388.16 30.4388 614.28 20.9457 277.37 47.3851 388.63 0.0000 618.01 21. 5194 277.60 52. 6611 391.69 38.1348 620.36 18.3108 278.00 40.8256 264.66 31. 6411 621. 93 14.0125 279.20 40.8663 401. 81 32.6235 630.19 0.0000 279.54 51. 4267 402.40 29.7563 631.29 19.4832 279.70 51.4327 404.85 20.1882 633.25 8.6667 280.46 44.8668 410.95 36.6702 634.78 0.0000 283.69 33.0780 413.71 29.9663 635.95 20.6081 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 34.4487 423. 72 0.0000 645.85 17.4297 285.90 0.0000 427.09 21. 4396 657.76 21.3527 *287.50 42.4707 427.87 30.2249 657.90 0.0000 290.67 38.5864 433.94 35.2273 661. 66 27. 9695 293.27 0.0000 439.40 31. 4141 664.57 0.0000 3'51. 93 38.7263 453.88 21. 7793 666.33 0.0000 295. 96 38.7493 463.37 21.8971 666.50 0.0000 879.38 29.4564 468.07 19.1609 667.71 0.0000 299.98 33.5098 473.00 0.0000 677.62 11. 0429 300.09 33.5129 475.06 17.0315 685.70 0.0000 300.13 33.5144 476.78 18.0505 695.00 0.0000 301.36 33.5464 477.60 15.0488 696.49 14.4690 302.85 33.5854 482.18 21.1218 696.51 14.4690 256.23 33.6281 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18. 9272 306.78 36.3826 497.08 19.2648 697.49 22.2689 308.46 29.1430 505.52 18.3329 702.65 18. 9687 311.90 36.0742 507.63 0.0000 706.68 16.7645 316.51 30.7696 511. 00 20.4285 711. 68 16.7987 319.41 0.0000 514.00 20.4606 720.70 0.0000 320.08 0.0000 514.00 20.4606 721.93 0.0000 321.04 36.3224 520.40 16.4232 722.78 25.3107 323.87 42.7687 520.69 0.0000 722. 91 25.3125 325.23 51. 008 6 522.65 0.0000 723. 31 25.3162 328.76 0.0000 527.90 0.0000 724.19 20.2603 333.37 35.7357 528.26 20.6120 727.33 19.1582 333.97 33.0015 529.59 24.7510 733.00 13.5542 334.37 31.6355 529.87 0.0000 735.93 18.0931 338.28 36.7814 531. 02 0.0000 333.97 16.9727 338.32 36.7830 537.26 0.0000 739.50 0.0000 311. 90 41. 4441 546.56 0.0000 747.24 22.7165 340.48 41.4441 552.55 20.8643 748.06 9.0895 340.55 0.0000 563.25 17.8280 752.31 21. 6232 344.28 35.0916 569.33 18.9324 753.82 0.0000 345.93 31.0646 946.00 18.9338 756.73 20.5203 351.06 36.1872 569.70 15.7794 756.80 20.5210" 351. 93 36.2086 583.19 25.4102 884.68 19.4342 Page 3408 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.6001 1274.44 14.8569 1620.50 3.2587 766.42 26.3186 1001.03 14.8789 1621.92 5.4327 766.84 21. 7445 1002.74 19.5388 1678.03 0.0000 772. 60 0.0000 1004.73 18.6200 1690.97 5. 5096 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.3539 778.90 18.3952 1028.54 0.0000 1063.66 1.1192 783.70 0.0000 1037.84 11. 2844 1771.35 3.3583 785.37 20.7451 1038.76 0.0000 1791.20 0.0000 792.07 26.5741 631.29 12.2573 1808.65 5. 4117 794.95 18.5059 1048.07 0.0000 1810.72 0.0000 795.86 19.6694 1049.04 9.0580 1836.06 0.9066 810.06 16.2832 1050.41 13.5923 810.29 16.2843 1063.66 12.3192 344.28 20.9385 1077.00 0.0000 810.76 20.9407 1077.34 14.2712 815.77 0.0000 1085.87 11. 4448 1048.07 0.0000 1093.63 19.1174 832.01 15.4747 1099.45 10.7242 834.85 11.2656 1112. 07 19.2188 835.71 12.9126 1112. 84 7.6890 836.80 0.0000 1115. 54 12.3117 846.75 0.0000 1120.29 11. 5576 846.77 15.5563 1120.55 11. 5591 856.80 0.0000 1221.41 4.6245 860.56 8.8815 1129. 67 12.3609 871.09 10.6967 1131.51 0.0000 873.19 8.9203 1147.95 0.0000 875.33 0.0000 1173.23 23.4565 "879.38 6.2577 1177.95 18.5930 880.51 12.5200 1189.05 15.7041 883.24 6.2658 . 1204. 77 20.6988 884.68 13. 4335 1221.41 12.8699 889.28 11. 6602 1231.02 16.8713 894.76 15.2766 1235.36 0.0000 898.04 13.4944 1238.28 16.9035 900. 72 20.7097 1260.41 0.0000 903.28 17.1225 1271.87 7.0205 911. 20 10.8431 1274.44 8.0288 912.08 10.8461 1274.54 8.0288 923.98 0.0000 1291. 59 9.0714 926.50 13.6226 1298.22 0.0000 929 .11 14.5430 1312 .11 0.0000 937.49 20. 9631 1332.49 5.0909 944.13 0.0000 1362.66 0.0000 946.00 10.9673 1365.19 5 .1312 949.00 13.7224 1368.63 0.0000 667.71 0.0000 1384.29 7.2166 962. 31 8.8198 1408.01 2.0734 964.08 11. 7 664 1457.56 0.0000 966 .17 11. 0383 1460.82 7.3452 911. 20 10.3117 1489.16 3.1681 968: 97 10.3117 1505.03 3.1793 983.53 0.0000 1584.12 8.6240 984.45 0.0000 1596.21 0.0000 Page 3409 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:59.00 *********************************x**********************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM18.CNF;511 Background date : Z-OCT-2016 11:01:02. Sample date 8-DEC-2015 13:43:00. Acquisition date : 3-0CT-2016 08:58:12. Sample ID G405235022 Sample quantity 1.61105E+02 GRAM Detector name GAM18 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.02 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3410of5809 Energy 49.57 62.89* 74.91 77.20* 87.32 92.44* 129.60 143.83* 185.90* 208.76 238.82* 241. 79 270.17 295.64* 300.66 338.90* 352.34* 453.32* 463.59 511. 57* 571.35 583.63* 609.67** 641.46 662.21 667.87 683.97 708.81 728. 24 769.01 863.01 912.06* 969.92* 997.10 BACKGROUND *CORRECTED SAMPLE PEAK REPORT Area 34 53 129 212 74 192 52 10 71 49 504 145 50 152 39 96 346 13 31 103 24 220 270 . 25 364 39 25 24 62 26 is 86 85 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 109 191 187 178 143 306 285 137 201 105 106 111 111 141 89 119 102 57 69 85 50 60 82 19 68 17 12 55 28 32 35 55 31 25 1. 03 2.02 1.14. 1.15 1.17 1. 65 4.07 *o. 85 1. 52 1. 53 1. 21 1. Bl. 1. 55 1. 37 1. 47 1. 22 1. 48 1.11 1.13 2.85 2.91 1. 63 1. 72 3.12 1. 55 0.89 1. 33 4.85 1. 68 2.53 1. 35 1. 44 2.05 0.55 99.98 126.58 150.61 155.18 175.42 185.63 259.90 288.33 372.40 418.09 478.16 484.10 540.82 591. 71 601.75 678.18 705.04 906.86 927.38 1023.28 1142. 77 1167. 31 1219.35 1282.88 1324. 36 1335. 69 1367.87 1417.52 1456.36 1537.84 1725.74 1823.79 1939.45 1993.80 97 122 146 146 173 179 252 285 366 415 473 473 535 585 597 6.71 697 900 924 1015 1135 1158 1211 1275 1316 1331 1363 1408 1449 1532 1716 1817 1933 1983 6 9.48E-03 51.4 9 1.47E-02 50.0 15 3.59E-02 19.7 15 5.90E-02 12.9 6 2.04E-02 28.3 15 5.33E-02 21.7 15 1. 44E-02 72. 5 7 2.88E-03194.l 12 1.97E-02 42.9 7 1. 35E-02 37. 8 16 1.40E-01 5.7 16 4.03E-02 16.9 12 1. 40E-02 44 .1 12 4.23E-02 17.8 10 1.08E-02 48.8 14 2.68E-02 26.7 16 9.6rn-02 8.*6 10 3.71E-03113.0 9 8.56E-03 51.5 23 2.85E-02 28.2 14 6.58E-03 67.8 16 6.12E-02 10.6 18 7.51E-02 10.1 13 6.86E-03 42.0 16 1. OlE-01 7. 3 13 1.08E-02 26.7 9 6.87E-03 33.2 17 6.54E-03 75.2 16 1. 73E-02 22. 8 11 7.19E-03 47.1 14 7.02E-03 53.5 11 2.39E-02 18.1 13 2.35E-02 17.9 12 2.28E-03130.3 Fit 1. OBE+OO 9.60E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1054.81 8 47 5:05 2109 .1*5 2091 23 2.30E-03215.8 36 0 1062.39 9 15 1. 04 2124.31 2116 11 2.48E-03 93.4 37 0 1065.22 12 8 0.64 2129.97 2126 8 3.22E-03 51. 7 38 0 1121.22* 41 28 1. 63 2241.92 2234 16 1.14E-02 33.8 39 0 1188.16 15 18 0.54 2375.75 2368 14 4.23E-03 63.8 40-0 1239.27 20 27 3.66 2477.93 2470 12 5.58E-03 56.3 41 0 1270.17 37 11 8.03 2539.71 2529 21 1. OlE-02 27.7 42 0 1314.97 14 0 1. 29 2629. 29 2625 9 3.89E-03 26.7 43 0 1337.14 11 18 0. 96 2673.60 2663 16 2. 96E-03 98.0 44 0 1378.49 39 10 2.65 2756.28 2745 17 1.09E-02 23.6 45 0 1406.28 6 17 1. 31 2811.83* 2801 17 1.67E-03162.7 46 0 1411.65 5 6 0.61 2822.57 2817 9 1. 34E-03106. 2 47 0 1461.65* 587 6 2.57 2922.55 2911 24 1. 63E-01 4.3 48 0 1503.19 7 8 0.70 3005.60 2998 12 1.82E-03 98.7 49 0 1590.82 15 13 1.13 3180.82 3173 14 4.15E-03 58.8 50 0 1765.46* 66 0 1. 63 3530.04 3520 18 1. 83E-02 13.2 Flag: *" = Peak area was modified by background subtraction Page 3411of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:59:00 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 13:43:00 G405235022 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:58:12 161.10 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA18 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3412of5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 *87. 57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.02 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 911E+OO 1.305E+Ol 1.305E+Ol 8.61 OK CD-109 88.03 3.70* 6.143E+OO 1.288E+OO 2. 021E+OO 89.80 OK SN-.126 64.28 9.60 3.037E+OO 1.155E+OO 1.155E+OO 100.06 OK 86.94 8.90 6.143E+OO 5.354E-01 5.354E-01 89.80 OK 87.57 37.00* 6.143E+OO 1.288E-01 1.288E-01 89.80 OK BA-137M 661. 66 89.90* 3.370E+OO* 5.994E-01 6.109E-01 14.57 OK CS-137 661. 66 85.10* 3.370E+OO 6.332E-01 6.453E-01 14.57 OK TL-208 277.37 6.60 6.127E+OO Line Not Found Absent 583.19 85.00* 3.675E+OO 3.568E-01 3.568E-01 21.15 OK 860.56 12.50 2.814E+OO Line Not Found Absent BI-211 72. 87 1. 23 4.495E+OO Line Not Found Absent 351.06 12.92* 5.217E+OO 6.331E-01 6. 331E-01 140.40 OK PB-212 74.82 10.28 4.764E+OO 1.217E+OO 1.217E+OO 54.80 OK 77 .11 17.10 5.051E+OO 1.533E+OO 1.533E+OO 25. 72 OK 238.63 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 OK 300.09 3.30 5. 811E+OO 1.102E+OO 1.102E+OO 97.69 OK BI-214 609.32 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 OK 1764.49 15.30 1.633E+OO '1.167E+OO l. l68E+001 26.46 OK PB-214

74.82 5.80 4.752E+OO Line Not Found <<INT Reject 77 .11 9.70 5.051E+OO 2.703E+OO 2.704E+OO 25.72 OK 87.09 3.41 6.121E+OO Line Not Found <<INT Reject 242.00 7.25 6.668E+OO Line Not Found <<INT Reject 295.22 18.42 5.877E+OO 7.669E-01 7.672E-01 35.62 OK 351. 93 35.60* 5. 221E+OO Line Not Found* <<INT Reject RN-222 609.32 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 OK 1120. 29 14.92 2.335E+OO 5.509E-01 5.511E-01 67.60 OK 1764.49 15.30 1. 633E+OO 1.167E+OO 1.168E+OO 26.46 OK RA-224 240.99 4.10* 6.671E+OO 1.597E+OO 1.597E+OO 69.38 OK RA-226 609.32 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 OK 1764.49 *15.30 1.633E+OO 1.167E+OO 1.168E+OO 26.46 OK AC-228 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11.27 5.359E+OO 8.573E-01 53.48 OK 794.95 4.25 2.973E+OO Line Not Found Absent 835 .. 71 1. 61 2. 872E+OO Line Not Found Absent. 911.20 25.80* 2.703E+OO 5.926E-01. 5.926E-01 36.28 OK 968. 97 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 OK RA-228 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 OK 794.95 4.25 2.973E+OO Line Not Found Absent 835. 71 1. 61 2.872E+OO Line Not Found Absent 911. 20 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 OK 968. 97 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 OK TH-228 74.82 10.28 4.764E+OO 1. 217E+OO 1. 217E+OO 54.80 OK 77 .11 17.10 5. 051E+OO 1.533E+OO 1.533E+OO 25. 72 OK 238.63 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 OK 300.09 3.30 5. 811E+OO l.102E+OO 1.102E+OO 97.69 OK TH-230 609.32 45.49* 3.566E+OO 8.388E-01 8.388E-01 20.12 OK Page 3413of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 2.335E+OO 5.509E-01 5.509E-01 67. 60 OK 1764.49 15.30 1.633E+OO l.167E+OO 1.167E+OO 26.46 OK PA-231 283.69 1. 70 6.038E+OO Line Not Found Absent 301. 36 5.35* 5.811E+OO 6.797E-01 6.797E-01 97.69 OK TH-232 105.21 1.10 7.385E+OO Line' Not Found Absent 338.32 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 OK 835.71 1. 61 2.872E+OO -----Line Not Found Absent 911.20 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 OK 968. 97 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 OK TH-234 63.29 3.70* 3.037E+OO 2. 996E+OO 2. 996E+OO 100.06 OK' 92.59 4.23 6.582E+00 4.229E+OO 4.229E+OO 43.37 OK U-234 609.32 45.49* 3.566E+OO 8.388E-01 8.388E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5.509E-01 67.60 OK 1764.49 15.30 1.633E+OO 1.167E+*oo 1.167E+OO 26.46 OK U-235 89. 96 3.47 6.379E+OO Line Not Found Absent 93.35 5.60 6.582E+OO 3.195E+OO 3.195E+00 43.37 OK 143.76 10.96* 8.086E+00 6.871E-02 6.871E-02 388.16 OK 163.33 5.08 7.938E+OO Line Not Found Absent 185.72 57.20 7.616E+OO 9.'318E-02 9.318E-02 85.87 OK 205.31 5.01 7.289E+OO Line Not Found Absent U-238 63.29 3.70* 3.037E+OO 2. 996E+00 2. 996E+OO 100.06 OK 92. 59 4.23 6.582E+OO 4.229E+OO 4.229E+OO 43.37 OK AM-243 43.53 5.90 3.443E-01 Line Not Found Absent 74.66 67.20* 4.764E+OO 1.862E-01 l.862E-01 54.80 OK ANH-511 511. 00 100.00* 4.026E+OO l.308E-01 1.308E-01 56.43 OK Flag: "*" = Keyline / Page 3414of5809 VAX/VMS Nuclide Identification Report Generated, 03-0CT-2016 09:59:01.76 *******************************************************************************
GEL Laboratoiies LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l *
Acquisition date 3-0CT-2016 08:58:12 Sensitivity : 3.000 * *Detector' ID GAM18 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.02 Half life ratio : ***** *
Sample date 8-DEC-2015 13:43:00 Analyst initials: MXRl *
Sample ID G405235022 Sample Quantity 1.6110E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date : 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
Eff. File : 'DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 l.305E+Ol .1.101E+OO CD-109 2.021E+OO 1. 778E+OO SN-126 1.288E-01 1.133E-01 BA-137M 6.109E-01 8.723E-02 CS-137 6.453E-01 9.215E-02 TL-208 3.568E-01 7.397E-02 BI-211 6. 331E-01 8. 711E-01 PB-212 9.605E-01 1.074E-01 BI-214 8.391E-01 1.655E-01 PB-214 9.970E-01 l.682E-01 RN-222 8. 391E-01 1.655E-01 RA-224 l.597E+OO 1. 086E+OO RA-226 8. 391E-01 l.655E-01 AC--228 5.926E-01 2.107E-01 RA-228 5.926E-01 2.107E-01 TH-228 9.605E-01 1.074E-01 TH-230 8.388E-01 l.654E-01 PA-231 6.797E-01 6.507E-01 TH-232 5.926E-01 2.107E-01 TH-234 2. 996E+OO 2.938E+OO U-234 8.388E-01 1.654E-01 U-235 6. 871E-02 2.614E-01 U-238 2. 996E+OO 2.938E+OO AM-243 1. 8 62E-01 9.999E-02 ANH-511 l.'308E-01 7.232E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3415of5809 Key-Line Activity (pCi/GRAM -7. 641E+OO 3.943E-02 O.OOOE+OO -1. 490E-02 6.926E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1. 071E+Ol 3.860E-02 1. 779E+41 2.491E-02 3.070E-01 MDA (pCi/GRAM 3.806E-01 1.651E+OO l.097E-01 5.719E-02 6.041E-02 4.492E-02 2.554E-01 7.630E-02 8.939E-02 2.454E-01 8.939E-02 8.172E-01 8.939E-02 2.003E-01 2.003E-01 7.630E-02 8.936E-02 6.233E-01 2.003E-01 2 .115E+OO 8.936E-02 2.565E-01 2 .115E+OO 8.044E-02 3.680E-02 MDA (pCi/GRAM 1. 808E+Ol 7.597E-02 O.OOOE+OO 4.378E-02 5.862E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.065E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3. 331E+02 O.OOOE+OO SHORT HLIF MN-54 -3.136E-02 4.802E-02 8.224E-02 NOT IDENT. C0-56 l.704E-02 3.528E-01 6.658E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.302E-02 3.740E-02 6.907E-02 NOT IDENT. C0-58 -7.lOlE-02 3.817E-01 7.107E-01 NOT IDENT. FE-59 -4.991E-01 4.655E+OO 8.911E+OO NOT IDENT. C0-60 2.140E-02 3.225E-02 6.121E-02 NOT IDENT. ZN-65 l.107E-01 1.388E-01 2.641E-01 NOT IDENT. GE-68 -l.237E-Ol 1. 8 67E+OO 3.553E+OO NOT IDENT. AS-73 -l.057E+OO 8.772E+OO 1.794E+Ol NOT IDENT. AS-74 0.000E+OO 4.756E+03 0.000E+OO SHORT HLIF SE-75 l.514E-01 1.540E-01 2.998E-01 NOT IDENT. BR-77 O.OOOE+OO l.917E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.434E+02 O.OOOE+OO SHORT HLIF RB-83 -4.114E-02 5.068E-01 8.734E-01 NOT IDENT. KR-85 l.121E+Ol 5.744E+OO l.269E+Ol NOT IDENT. SR-85 l.180E+OO 6.063E-01 l.340E+OO NOT IDENT. RB-86 O.OOOE+OO 2.255E+04 0.000E+OO SHORT HLIF Y-88 2.032E-02 l.233E-01 2.749E-01 NOT IDENT. Y-91 2. 861E+02 4.316E+02 8. 710E+02 NOT IDENT. NB-94 -1. 750E-02 2.858E-02 4.325E-02 NOT IDENT. NB-95 6.325E-01 6.446E-01 1.243E+OO NOT IDENT. NB-95M l.835E-01 l.983E+00 3.507E+OO NOT IDENT. ZR-95 8.519E-02 1.015E+OO 1.956E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 081E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.347E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 1. 447E-02 2.823E-02 5.500E-02 NOT IDENT. RH-102 1.531E-02 4. 391E-02 8.780E-02 NOT IDENT. RU-103 -8. 813E-01 4.179E+OO 7.984E+00 FAIL ABUN RH-106 -2.326E-01 3.658E-01 6.570E-01 NOT IDENT. RU-106 -2.326E-01 3.658E-01 6.570E-01 NOT IDENT. AG-108M -3 .131E-03 2.150E-02 3.932E-02 NOT IDENT. AG-llOM -2.253E-02 7.881E-02 1.412E-01 NOT IDENT. SN-113 -5.019E-02 1.896E-01 3.448E-01 NOT IDENT. CD-115 O.OOOE+OO 2.304E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.166E+04 O.OOOE+OO SHORT HLIF TE-123M 2.086E-03 l.104E-01 2.029E-01 NOT IDENT. SB-124 -3.345E-01 1.404E+OO 2.741E+OO NOT IDENT. SB-125 -4.372E-02 8.373E-02 l.468E-01 FAIL ABUN TE-125M 4.863E+Ol 2.185E+02 4.261E+02 NOT IDENT. I-126 O.OOOE+OO 4.917E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.456E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 716E+22 O.OOOE+OO SHORT HLIF I-'-131 O.OOOE+OO 3.865E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 5.235E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.748E+26 O.OOOE+OO SHORT HLIF BA-133 8.277E-03 3.078E-02 5*. 433E-02 NOT IDENT. I-133 O.OOOE+OO 1.827E+41 O.OOOE+OO SHORT HLIF CS-134 3.357E-02 4.044E-02 8.303E-02 NOT IDENT. CS-135 8 .114E-02 l.129E-01 2.107E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.278E+05 O.OOOE+OO SHORT HLIF CE-139 -5.266E-02 9.230E-02 l.610E-01 NOT IDENT. BA-140 O.OOOE+OO 9. 051E+05 O.OOOE+OO SHORT HLIF LA-140* O.OOOE+OO 3.185E+05 O.OOOE+OO SHORT HLIF CE-141 -9.646E+OO 2.254E+Ol 3.736E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 -9.676E-02 3.061E-01 5 .139E-01 NOT IDENT. PM-144 -2.033E-02 4.393E-02 7.904E-02 NOT IDENT. PR-144 -1.740E+00 3.819E+OO 6.876E+OO NOT IDENT. PM-146 2.708E-02 5.998E-02 6.557E-02 FAIL ABUN ND-147 O.OOOE+oo 2. 45'3E+07 O.OOOE+OO SHORT HLIF PM-147 -5.706E+Ol 6.450E+02 l.218E+03 NOT IDENT. PM-149 O.OOOE+OO 3.512E+40 O.OOOE+OO SHORT HLIF EU-150 1.750E-03 2.173E-02 3. 718E-02 . FAIL ABUN EU-152 4 .113E-02 8.247E-02 1.470E-01 NOT IDENT. GD-153 4.647E-02 1. 481E-01 2.739E-01 NOT IDENT. EU-154 9.519E-02 9.444E-02 l.856E-01 FAIL ABUN EU-155 6.081E-02 8.556E-02 l.733E-01 FAIL ABUN TB-160 1.774E-01 1.284E+OO 2.476E+OO FAIL ABUN H0-166M 2.500E-02 5.246E-02 9.261E-02 FAIL ABUN TM-171 -1. 511E+00 2.280E+Ol 4.364E+Ol NOT IDENT. HF-172 -4.209E-02 2 .115E-01 3.609E-01 FAIL ABUN LU-172 3.188E-02 5.934E-02 l.209E-01 FAIL ABUN Page 3416of5809 LU-176 -2.564E-03 l.836E-02 3.478E-02 FAIL ABUN HF-181 1. 596E+OO 3.138E+OO 6.153E+OO NOT IDENT. TA-182 5.369E-01 7.361E-01 l.495E+OO FAIL ABUN RE-183 -1.204E+OO 2.910E+OO 5.768E+OO NOT IDENT. RE-184 -1.555E+Ol 2.253E+Ol 3.786E+Ol NOT IDENT. W-188 -5.736E+Ol 9.789E+Ol 1.578E+02 FAIL ABUN IR-192 -l.320E-01 3.467E-01 6.411E-01 FAIL ABUN HG-203 1.057E+OO 1.774E+OO 3.582E+OO NOT IDENT. BI-207 2.360E-02 4.321E-02 7.362E-02 FAIL ABUN PB-210 -2.609E+OO 4.585E+OO 8.442E+OO NOT IDENT. PB-211 -l.065E-01 5.620E-01 1.024E+OO NOT IDENT. BI-212 O.OOOE+OO 6.523E-01 9.123E-01 FAIL ABUN RN-219 -1.002E-01 2.939E-01 5.301E-01 FAIL ABUN RA-223 3.255E-01 4.306E-01 8.751E-Ol FAIL ABUN AC-227 -l.191E-01 1. 771E-01 3.270E-01 FAIL ABUN TH-227 -1.191E-01 1.771E-01 3.270E-01 FAIL ABUN TH-229 2.710E-02 3.335E-01 6.695E-01 FAIL ABUN TH-231 3.255E-01 4.306E-01 8.751E-01 FAIL ABUN PA-233 3.015E-02 4.366E-02 8.856E-02 FAIL ABUN PA-234 -5.054E-02 2.023E-01 3.845E-01 NOT IDENT. PA-234M 2. 969E+OO 3.274E+OO 6.539E+OO NOT IDENT. NP-237 3.015E-02 4.366E-02 8.856E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -6.413E-02 1. 986E-01 3.688E-01 NOT IDENT. PU-239 O.OOOE+OO 8.641E+02 5.285E+02 FAIL ABUN AM-241 3.422E-02 1.381E-01 2.661E-01 NOT IDENT. CM-2,43 -5.287E-02 7. 496E-02 1.370E-01 NOT IDENT. BK-247 7. 490E'-02 5.094E-02 l:045E-01 NOT IDENT. CM-247 l.157E-02 2.629E-02 5.127E-02 NOT I DENT.* CF-249 1.428E-02 2.762E-02 5.454E-02 NOT IDENT. CF-251 4.262E-02 8.960E-02 1.697E-01 NOT IDENT. Page 3417 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:59.70 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 570 10.66* 1.911E+OO 1.305E+Ol 1.305E+Ol 8.61 CD-109 88.03 97 3.70* 6.143E+OO 1.995E+OO 3*.129E+OO 56.59 SN-126 64.28 72 9.60 3.037E+OO l.155E+OO l.155E+00 100.06 86.94 97 8.90 6.143E+OO 8.292E-01 8.292E-01 56.59 87.57 97 37.00* 6.143E+OO l.995E-01 l.995E-01 56.59 BA-137M 661. 66 390 89.90* 3.370E+OO 5.994E-01 6.109E-01 14.57 CS-137 661. 66 390 85.10* 3.370E+OO 6.332E-01 6.453E-01 14.57 TL-208 277.37 ------6.60 6.127E+OO ------Line Not Found ------583.19 239 85.00* 3.675E+OO 3.568E-01 3.568E-01 21.15 860.56 ------12.50 2.814E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 4.495E+OO ------Line Not Found ------351.06 397 12.92* 5.217E+OO 2.746E+OO 2.746E+00 17.22 PB-212 74.82 173 10.28 4.764E+OO 1.650E+OO 1.650E+OO 39.33 77 .11 284 17.10 5.051E+OO 1.533E+OO l.533E+OO 25.72 238.63 604 43.60* 6.720E+00 9.605E-01 9.605E-01 11. 41 300.09 . 45 3.30 5. 811E+OO l.102E+OO 1.102E+OO 97.69 BI-214 609.32 292 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 1764.49 63 15.30. 1.633E+OO l.167E+OO 1.168E+OO 26.46 PB-214 74.82 173 5.80 4.764E+OO 2.924E+00 2.925E+00 39.33 77 .11 284 9.70 5.051E+OO 2.703E+OO 2.704E+00 25.72 87.09 97 3.41 6.143E+OO 2.164E+00 2.165E+00 56.59 242.00 173 7.25 6.671E+OO 1. 670E+OO 1.670E+OO 33.76 295.22 178 18.42 5.877E+OO 7.669E-01 7. 672E-01 35.62 351. 93 397 35.60* 5.217E+OO 9. 966E-01 9.970E-01 17.22 RN-222 609.32 292 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 1764.49 63 15.30 1. 633E+OO l.167E+OO 1.168E+OO 26.46 RA-224 240.99 173 4.10* 6. 671E+OO 2.953E+OO i.953E+00 33.76 RA-226 609.32 292 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 1764.49 63 15.30 1.633E+OO 1.167E+OO 1.168E+OO 26.46 AC-228 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 111 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 794.95 ------4.25 2.973E+OO ------Line Not Found ------835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 89 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 968.97 87 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 RA-228 105.21 ------1.10 7.385E+00 ------Line Not Found ------338.32 111 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 794.95 ------4.25 2.973E+OO ------Line Not Found ------835. 71 ------1. 61 2.872E+00 ------Line Not Found ------911. 20 89 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 968. 97 87 15.80 2.589E+00 9.865E-01 9.865E-01 35.85 TH-228 74.82 173 10.28 4.764E+OO 1.650E+OO 1.650E+OO 39.33 77 .11 284 17.10 5. 051E+OO 1.533E+OO 1.533E+OO 25. 72 238.63 604 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 Page 3418of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nucl,ide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 45 3.30 5. 81'1E+OO 1.102E+OO 1.102E+OO 97.69 TH-230 609.32 292 45.49* 3.566E+OO 8.388E-01 8.388E-01 20 .12 1120.29 41 14.92 2.335E+OO 5.509E-01 5.509E-01 67.60 1764.49 63 15.30 1.633E+OO 1.167E+OO 1.167E+OO 26.46 PA-231 283.69 ------1. 70 6.038E+OO ------Line Not Found ------301.36 45 5.35* 5. 811E+OO 6.797E-01 6.797E-01 97.69 TH-23.2 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 111 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 89 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 968. 97 87 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 TH-234 63.29 72 3.70* 3.037E+OO 2. 996E+OO 2. 996E+OO 100.06 92.59 253 4.23 6.582E+OO 4.229E+OO 4.229E+OO 43.37 U-234 609.32 292 45.49* 3.566E+OO 8,388E-01 8.388E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5.509E-01 67.60 1764.49 63 15.30 1.633E+OO 1.167E+OO 1.167E+OO 26.46 U-235 89.96 ------3.47 6.379E+OO ------Line Not Found ------93.35 253 5.60 6.582E+OO 3.195E+OO 3.195E+OO 43.37 143.76 13 10. 96* 8.086E+OO 6.871E-02 6. 871E-02 388.16 163.33 ------5.08 7.938E+OO ------Line Not Found ------185. 72 87 57.20 7.616E+OO 9.318E-02 9.318E-02 85.87 205.31 ------5.01 7.289E+OO ------Line Not Found ------U-238 63.29 72 3.70* 3.037E+OO 2.996E+OO 2. 996E+OO 100.06 92.59 253 4.23 6.582E+OO 4.229E+OO 4.229E+OO 43.37 AM-243 43.53 ------5.90 3.443E-01 ------Line Not Found ------74.66 173 67.20* 4.764E+OO 2.524E-01 2.524E-01 39.33 ANH-511 511. 00 113 100.00* 4.026E+OO 1.308E-01 1.308E-01 56.43 Flag: "*" Key line Page 3419of5809 Summary of Nuclide Activity Sample ID : ,G405235022 Acquisition date Page : 3 3-0CT-2016 08:58:12 Total number of lines in spectrum 50 Number of unidentified lines 17 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228' TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243
ANH-511 Hlife 1.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600. OOY 1600. ODY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+l0Y 1.41E+10Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.305E+Ol 1.995E+OO 1.995E-01 5.994E-01 6.332E-01 3.568E-01 2.746E+OO 9.605E-01 8.388E-01 9.966E-01 8.388E-01 2.953E+OO 8.388E-01 5.926E-01 5.926E-01 9.605E-01 8.388E-01 6.797E-01 5.926E-01 2. 996E+OO 8.388E-01 6. 871E-02 2. 996E+OO 2.524E-01 1.308E-01 3.854E+01 3.854E+Ol Decay Corr pCi/GRAM 1.305E+Ol 3.129E+OO 1.995E-01 6.109E-01 6.453E-01 3.568E-01 2.746E+00 9.605E-01 8.391E-01 9.970E-01 8.391E-01 2.953E+OO 8.391E-01 5.926E-01 5.926E-01 9.605E-01. 8.388E-01 6.797E-01 5.926E-01 2. 996E+OO 8.388E-01 6. 871E-02 2. 996E+OO 2.524E-01 1.308E-01 3.970E+Ol 3.970E+01 66.00% Decay Corr 2-Sigma Error 0 .112E+Ol 1.771E+OO 1.129E-01 0.890E-01 0.940E-01 0.755E-01 0.473E+OO 1. 096E-01 1. 68 9E-01 1.717E-01 1.689E-01 0.997E+OO 1. 689E-01 2.150E-01 2.150E-01 1. 096E-01 1. 688E-01 6.640E-01 2.150E-01 2.998E+OO 1.688E-01 26.67E-02 2.998E+OO 0.993E-01 0.738E-01 "M" Manually accepted 2-Sigma %Error 8.61 56.59 56.59 14.57 14.57 21.15 17.22 11. 41 20.12 17.22 20.12 33.76 20.12 36.28 36.28 11. 41 20.12 97.69 36.28 100.06 20.12 388.16 100.06 39.33 56.43 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3420 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235022 Acquisition date : 3-0CT-2016 08:58:12 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 49.57 48 152 1. 03 99.98 97 6 9.48E-03 **** l.OlE+OO T 0 129.60 66 363 4.07 259.90 252 15 l.44E-02 **** 8.04E+OO T 0 208.76 59 127 1. 53 418.09 415 7 1.35E-02 75.7 7.23E+00 0 270.17 60 131 1. 55 540.82 535 12 1. 40E-02 88. 3 . 6.23E+OO T 0 453.32 15 64 1.11 906.86 900 10 3. 71E-03 **** 4.38E+OO T 0 463.59 34 77 1.13 927.38 924 9 8.56E-03 **** 4. 31E+OO T 0 571.35 26 55 2.91 1142. 77 1135 14 6.58E-03 **** 3.73E+OO 0 641.46 27 21 3.12 1282.88 1275 13 6.86E-03 84.0 3.44E+OO 0 667.87 42 18 0.89 1335.69 1331 13 1. 08E-02 53.4 3.35E+OO T 0 683.97 26 13 1. 33 1367.87 1363 9 6.87E-03 66.4 3.30E+OO 0 708.81 25 59 4.85 1417.52 1408 17 6.54E-03 **** 3.22E+OO 0 728.24 66 29 1. 68 1456.36 1449 16 1. 73E-02 45.5 3.16E+OO T 0 769.01 27 34 2.53 1537.84 1532 11 7.19E-03 94.3 3.04E+OO 0 863.01 26 36 1. 35 1725.74 1716 14 7.02E-03 **** 2.81E+OO 0 997.10 8 25 0.55 1993.80 1983 12 2.28E-03 **** 2.54E+OO T 0 1054.81 8 47 5.05 2109.15 2091 23 2.30E-03 **** 2.44E+OO 0 1062.39 9 15 1. 04 2124.31 2116 11 2.48E-03 **** 2.43E+OO T 0 1065.22 12 8 0.64 2129.97 2126 8 3.22E-03 **** 2.42E+OO 0 1188.16 15 18 0.54 2375.75 2368 14 4.23E-03 **** 2.24E+00 T 0 1239.27 20 27 3.66 2477.93 2470 12 5.58E-03 **** 2.17E+OO T *o 1270.17 36 10 8.03 2539.71 2529 21 l.OlE-02 55.4 2.13E+00 0 1314.97 14 0 1. 29 2629. 29 2625 9 3.89E-03 53.5 2.07E+OO' 0 1337.14 10 18 0. 96 2673.60 2663 16 2.96E-03 **** 2.05E+OO 0 1378.49 38 10 2.65 2756.28 2745 17 1. 09E-02 47.2 2.00E+OO 0 1406.28 6 17 1. 31 2811.83 2801 17 l.67E-03 **** l.97E+OO 0 1411. 65 5 *6 0.61 2822.57 2817 9 l.34E-03 **** 1. 96E+OO 0 1503.19 6 8 0.70 3005.60 2998 12 1. 82E-03 **** 1.87E+OO 0 1590. 82 v 14 13 1.13 3180.82 3173 14 4.15E-03 **** 1.78E+OO Flags: "T" = Tentatively associated Page 3421 of 5809 VAX/VMS Nuclide Identification Generated 03-0CT-2016 09:59:13.78 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l *
Acquisition date 3-0CT-2016 08:58:12 Sensitivity 3.000 *
Detector ID GAM18 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000" *
Elapsed real time: 0 01:00:01.02 Half life ratio : ***** *
Sample date 8-DEC-2015 13:43:00 Nuclide Library : SOLID *
Sample ID G405235022 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.6110E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* ** *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 591E-01 7 .*788E-01 5.186E-02 2.641E-02 2.790E-02 2.037E-02 1.179E-01 3.588E-02 4.068E-02 1.192E-01 4.068E-02 3.843E-01 4.068E-02 9.093E-02 9.093E-02 3.588E-02 4.067E-02 2.903E-01 9.093E-02 9.973E-01 4*. 067E-02 1. 206E-01 9.973E-01 3.806E-02 l.678E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3422 of 5809 Le (pCi/GRAM 8.300E+OO 3.425E-02 O.OOOE+OO 1.793E-02 2.651E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-1'02 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3423 of 5809 O.OOOE+OO 3.675E-02 2.994E-01 O.OOOE+OO 3.239E-02 3.137E-01 3.945E+OO 2. 715E-02 l.194E-01 l.599E+OO 8. 396E+OO O.OOOE+OO 1.397E-01 O.OOOE+OO O.OOOE+OO 3. 960E-01 5.952E+OO 6.281E-01 O.OOOE+OO 1.091E-01 3. 969E+02 1. 962E-02 5.670E-01 1. 651E+OO 8.787E-01 O.OOOE+OO O.OOOE+OO 'O. OOOE+OO 0.000E+OO 2.603E-02 4.002E-02 3.643E+OO 2.959E-01 2.959E-01 l.805E-02 6.324E-02 l.597E-01 O.OOOE+OO O.OOOE+OO 9.573E-02 1.123E+OO 6.747E-02 2.006E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.499E-02 O.OOOE+OO 3.817E-02 9.872E-02 O.OOOE+OO O.OOOE+OO 7.568E-02 O.OOOE+OO O.OOOE+OO 1.765E+Ol O.OOOE+OO 2.413E-Ol 3.597E-02 3 .130E+OO 3.023E-02 O.OOOE+OO 5.715E+02 0.000E+OO 1. 730E-02 6.862E-02 1. 28 9E-01 8.364E-02 8.171E-02 1.101E+OO 4.257E-02 2. 041E+Ol l.703E-01 5.466E-02 1.615E-02 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT I.DENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF 'SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT, NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CI;-251 Page 3424 of 5809 2.815E+OO 6.811E-Ol 2.711E+OO 1.673E+Ol 7.344E+Ol 2.967E-01 1.676E+OO 3.321E-02 3.958E+OO 4.751E-01 4.255E-Ol 2.441E-01 4.076E-01 1.526E-01 l.526E-01 3.144E-01 4.076E-01 4.124E-02 1.719E-01 2. 968E+OO 4.124E-02 O.OOOE+OO 1.734E:._01 2.509E+02 l.254E-01 6. 396E-02 4. 872E-02 2.'371E-02 2.522E-02 7.986E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:59:19.80 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l *
Acquisition date 3-0CT-2016 08:58:12 Sensitivity : 3.000 *
Detector ID GAM18 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.02. Half life ratio : ***** *
Sample date 8-DEC-2015 13:43:00 Nuclide Library : SOLID *
Sample ID G405235022 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.6110E+02 GRAM *
Quantity-Err(%) : 1.2414E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
Combined Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 l.305E+Ol 1.295E+OO CD-109 2.021E+OO 1. 791E+OO SN-126 l.288E-01 1.140E-01 BA-137M 6.109E-01 9. lllE-02 CS-137 6.453E-01 9.623E-02 TL-208 3.568E-01 7. 551E-02 BI-211 6.331E-01 8.810E-01 PB-212 9.605E-01 1.188E-01 BI-214 8.391E-01 l.694E-01 PB-214 9.970E-01 1.733E-01 RN-222 8.391E-01 l.694E-01 RA-224 1.597E+OO 1.093E+OO RA-226 8.391E-01 1.694E-01 AC-228 5.926E-01 2.129E-01 RA-228 5.926E-01 2.129E-01 TH-228 9.605E-01 l.188E-01 TH-230 8.388E-01 1.693E-01 PA-231 6.797E-01 6.667E-01 TH-232 5.926E-01 2.129E-01 TH.:.234 2. 996E+OO 3.012E+OO U-234 8.388E-01 1.693E-01 U-235 6. 871E-02 2.614E-01 U-238 2. 996E+OO 3.012E+OO AM-243 1.862E-01 l.OlOE-01 ANH-511 1.308E-01 7. 251E"-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3425 of 5809 Key-Line Activity (pCi/GRAM -7.641E+OO 3.943E-02 l.000E+41 -l.490E-02 6.926E-02 K.L Act error ( 1. 96-sigma) 1. 072E+Ol 3.863E-02 1.832E+41 2. 493E--02 3.070E-01 TPU ( 1. 96-sigma) 1.295E+OO 1. 791E+OO 1.140E-01 9. lllE-02 9.623E-02 7. 551E-02 8.810E-01 1.188E-01 1.694E-01 l.733E-01 l.694E-01 1.093E+OO l.694E-01 2.129E-01 2.129E-01 1.188E-01 l.693E-01 6.667E-01 2.129E-01 3.012E+OO 1.693E-01 2.614E-01 3.012E+OO 1.0lOE-01 7.251E-02 *TPU ( 1. 96-sigma) 1.126E+Ol 4.252E-02 O.OOOE+OO 2.582E-02 3.086E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 -1. 740E+03 1.065E+04 l.068E+04 SHORT HLIF CR-51 8.068E+Ol 3. 331E+02 3.351E+02 SHORT HLIF MN-54 -3.136E-02 4.804E-02 5.008E-02 NOT .IDENT. C0-56 l.704E-02 3.528E-01 3.529E_:.01 FAIL ABUN MN-56 l.OOOE+41 1. 8 61E+42 O.OOOE+OO SHORT HLIF C0-57 -l.302E-02 3.741E-02 3.786E-02 NOT IDENT. C0-58 -7.lOlE-02 3.817E-01 3.830E-01 NOT IDENT. FE-59 -4.991E-01 4.655E+OO 4. 661E+OO NOT IDENT. C0-60 2.140E-02 3.226E-02 3.367E-02 NOT IDENT. ZN-65 l.107E-01 1.389E-01 1.476E-01 NOT IDENT. GE-68 -l.237E-01 1.867E+OO 1. 868E+OO NOT IDENT. AS-73 -l.057E+OO 8.775E+OO .8.788E+OO NOT IDENT. AS-74 -4.091E+03 4.768E+03 5 .113E+03 SHORT HLIF SE-75 l.514E-01 1.542E-01 1. 686E-01 NOT IDENT. BR-77 l.714E+38 l.484E+39 O.OOOE+OO SHORT HLIF SR-82 -2.549E+Ol 5. 434E+02
5.435E+02 SHORT HLIF RB-83 -4 .114E-02 5.068E-01 5. 072E-01 NOT IDENT. KR-85 l.121E+Ol 5. 7 62E+OO 7.665E+OO NOT IDENT. SR-85 1.180E+OO 6.082E-01 8.080E-01 NOT IDENT. RB-8 6
2.197E+03 2.255E+04 2.257E+04 SHORT HLIF Y-88 2.032E-02 1.233E-01 1.237E-01 NOT IDENT. Y-91 2. 861E+02 4.317E+02 4.506E+02 NOT IDENT. NB-94 -1. 7 50E-02 2.859E-02 2. 966E-02 NOT IDENT. NB-95 6.325E-01 6. 451E-01 7.053E-01 NOT !DENT. NB-95M l.835E-01 1.983E+OO 1.985E+OO NOT IDENT. ZR-95 8.519E-02 1.015E+OO 1.016E+OO NOT IDENT. NB-97 1.000E+41 3.265E+41 O.OOOE+OO SHORT HLIF . ZR-97 1.000E+41 1.082E+41 O.OOOE+OO SHORT HLIF M0-99 -4.397E+31 1.347E+32 0.000E+OO SHORT HLIF TC-99M l.OOOE+41 7.343E+42 O.OOOE+OO SHORT HLIF RH-101 1. 44 7E-02 2.835E-02 2.910E-02 NOT IDENT. RH-102 l.531E-02 4.392E-02 4.446E-02 NOT IDENT. RU-103 -8. 813E-Ell 4.179E+OO 4.198E+OO FAIL ABUN RH-106 -2.326E-01 3.661E-01 3.808E-01 NOT IDENT. RU-106 -2.326E-01 3.661E-01 3.808E-01 NOT IDENT. AG-108M -3 .131E-03 2.150E-02 2.155E-02 NOT IDENT. AG-llOM -2.253E-02 7.881E-02 7.947E-02 NOT IDENT. SN-113 -5.019E-02 l.896E-01 1.909E-01 NOT IDENT. CD-115 1.684E+38 2.304E+39 O.OOOE+OO SHORT HLIF SN-ll 7M l.624E+04 8 .168E+04 8. 201E+04 SHORT HLIF TE-123M 2.086E-03 1.104E-01 1.104E-01 NOT IDENT. SB-124 -3.345E-01 l.404E+00 l.412E+OO NOT IDENT. SB-125 -4.372E-02 8.375E-02 8.604E-02 FAIL ABUN TE-125M 4.863E+Ol 2.185E+02 2 .196E+02 NOT IDENT. I-126 l.560E+06 5.354E+05 8.839E+05 SHORT HLIF SB-126 -l.240E+04 9.456E+05 9.456E+05 SHORT HLIF SB-127 4.877E+21 l.843E+22 O.OOOE+OO SHORT HLIF I-131 6.706E+08 3.865E+09 3.877E+09 SHORT HLIF I-132 1.000E+41 l.849E+42 O.OOOE+OO SHORT HLIF TE-132 -9.294E+25 2.774E+26. O.OOOE+OO SHORT HLIF BA-133 8.277E-03 3.078E-02 3. lOlE-02 NOT IDENT. I-133 l.000E+41 2. 571E+41 O.OOOE+OO SHORT HLIF CS-134 3.357E-02 4.047E-02 4.321E-02 NOT IDENT. CS-135 8 .114E-02 l .130E-01 1.188E-01 NOT IDENT. I-135 -l.OOOE+41 7.385E+41 O.OOOE+OO SHORT HLIF CS-136 l.520E+04 2. 278E+o5* 2.279E+05 SHORT HLIF CE-139 -5.266E-02 9.291E-02 9.589E-02 NOT IDENT. BA-140 -2.767E+05 9.052E+05 9 .137E+05 SHORT HLIF LA-140 2.399E+05 3.187E+05 3.365E+05 SHORT HLIF CE-141 -9.646E+OO 2.255E+Ol 2.296E+Ol NOT IDENT. CE-143 l.000E+41 2.342E+41. O.OOOE+OO SHORT HLIF CE-144 -9.676E-02 3.062E-01 3.093E-01 NOT IDENT. PM-144 -2.033E-02 4.395E-02 4.490E-02 NOT IDENT. PR-144 -l.740E+OO 3.820E+OO 3.900E+00 NOT IDENT. PM-146 2.708E-02 6.00lE-02 6.124E-02 FAIL ABUN ND-147 7.700E+06 2. 453E+0'7 2.478E+07 SHORT HLIF PM-147 -5.706E+01 6.450E+02 6.455E+02 NOT IDENT. PM-149 l.865E+39 3.512E+40 O.OOOE+OO SHORT HLIF EU-150 1.750E-03 2.173E-02* 2.174E-02 FAIL ABUN EU-152 4 .113E-02 8.250E-02 8.456E-02 NOT IDENT. GD-153 4.647E-02 1.482E-01 l.496E-01 NOT IDENT. EU-154 9.519E-02 9. 451E-02 1.038E-01 FAIL ABUN EU-155 6.081E-02 8.567E-02 8.995E-02 FAIL ABUN TB-160 l.774E-01 l.284E+OO l.287E+OO FAIL ABUN H0-166M 2.500E-02 5.248E-02 5.368E-02 FAIL ABUN TM-171 -l.511E+00 2.280E+Ol 2.281E+Ol NOT IDENT. HF-172 -4.209E-02 2 .116E-01 2.124E-01 FAIL ABUN LU-172 3.188E-02 5.942E-02 6 .114E-02 FAIL ABUN* Page 3426 of 5809 LU-176 -2.564E-03 l.836E-02 1. 840E-02 FAIL ABUN HF-181 1. 596E+OO 3.139E+OO 3.220E+OO NOT IDENT. TA-182 5.369E-01 7.364E-01 7. 7 51E-01 FAIL ABUN. RE-183 -l.204E+OO 2.916E+00 2. 966E+OO NOT IDENT. RE-184 -1.555E+Ol 2.283E+01 2.389E+Ol NOT IDENT. W-188 -5.736E+Ol 9.810E+01 1.014E+02 FAIL ABUN IR-192 -l.320E-01 3.467E-01 3.518E-01 FAIL ABUN HG-203 1.057E+OO 1.774E+OO 1.837E+OO NOT IDENT. BI-207 2.360E-02 4.322E-02 4. 451E-02 FAIL ABUN PB-210 -2.609E+OO 4.591E+OO 4.740E+OO NOT IDENT. PB-211 -1.065E-01 5.620E-01 5. 641E-01 NOT IDENT. BI-212 1.461E+OO 6.565E-01 9. 301E-01 FAIL ABUN. RN-219 -l.002E-01 2.942E-01 2.976E-01 FAIL ABUN RA-223 3.255E-01 4.310E-01 4.553E-01 FAIL ABUN AC-227 -1.191E-01 1.778E-01 1.858E-01 FAIL ABUN TH-227 -l.191E-01 1.778E-01 1.858E-01 FAIL ABUN TH-229 2. 710E-02 3.335E-01 3.337E-01 FAIL ABUN TH-231 3.255E-01 4.310E-01 4.553E-01 FAIL ABUN PA-233 3.015E-02 4.368E-02 4.575E-02 FAIL ABUN PA-234 -5.054E-02 2.104E-01 2 .116E-01 NOT IDENT. PA-234M 2. 969E+OO 3.277E+OO 3.540E+OO NOT IDENT. NP-237 3.015E-02 4.368E-02 4.575E-02 FAIL ABUN NP-238 -1.000E+41 3.092E+41 O.OOOE+OO SHORT HLIF NP-239 -6.413E-02 1.987E-01 2.008E-01 NOT IDENT. PU-239 6.081E+02 8.645E+02 9.069E+02 FAIL ABUN AM-241 3.422E-02 l.381E-01 1.389E-01 NOT IDENT. CM-243 -5.287E-02 7.512E-02 7.881E-02 NOT IDENT. BK-247 7.490E-02 5.313E-02 6.295E-02 NOT IDENT .. CM-247 1.157E-02 2.636E-02 2.687E-02 NOT IDENT. CF-249 l.428E-02 2.765E-02 2.839E-02 NOT IDENT. CF-251 4.262E-02 8.973E-02 9.176E-02 NOT IDENT. Page 3427 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 78.8835 87.09 99.2838 136.47 81. 9702 45.60 78.9767 87.57 99.4423 140.51 0.0000 . 46. 54 83.7918 88.03 92.3857 143.76 83.3391 49:72 0.0000 88. 34. 92.4803 144.24 83.4283 51. 35 67.8268 88.47 92.5198 145.44 100.8383 51. 87 63.4697 89. 96 81. 7 622 .152. 43 89.5764 52.39 71. 5876 1093.63 81. 9426 153.25 0.0000 52.97 68.3734 91.11 0.0000 323.87 95.7522 53.44 74.5267 92.59 82.4554 156.02 0.0000 54.07 82.4875 93.35 82.6534 158.56 0.0000 57.36 0.0000 94. 56 82.9681 159.00 91.9906 57.53 96.9429 94.65 82.9915 162.33 77.1796 57.98 91. 8914 94.67 82. 9965 162.66 0.0000 59.27 79.8124 94.87 83.0482 163.33 77.3343 59.32 79.8303 97.43 76.9550 165.86 98.0519 59.54 82.2595 98.43 88.3607 176.31 79.3060 60. 96 92.2402 98.44 88.3634 176.60 ' 0. 0000 61.17 92.3251 99.53 77.4449 177.52 72.1493 62.93 91.2437 100 .11 77.5789 181.07 0.0000 63.29 91. 3844 102.03 76.9947 181.52 70.6317 63.58 91. 4974 103.18 83.4336 184.41 76.7848 64.28 95.9678 103.37 82.4493 143.76 76.9664 66.73 93.3158 105.21 73.5633 193.51 78.0345 67.24 101.1002 105.31 73.5844 197.03 76.8220 125.81 110.4059 106.12 77.9102 198.01 82.8699 67.75 110.4372 106.47 85.2663 201.83 85.1095 69.67 99.3351 109.28 80.7016 203.43 92.1643 70.83 115.8046 111. 00 89.5103 205.31 75.7603 72.81 115. 4553 111. 76 0.0000 210.85 90.7033 72.87 115.4818 114. 06 100.8759 215.65 80.9578 74.66 103.1418 116. 30 0.0000 222 .11 67. 7126 74.82 103.2039 116.74 91: 9727 227.09 63.8013 74.97 103.2618 119.76 79.7649 227.38 50.5314 77 .11 104.0834 121.12 80.0443 228.16 0.0000 78 .*74 104.7019 121. 22 80.0647 228.18 72.7827 79.69 85.3210 121. 78 85.5968 116.74 72.7827 80.12 84.1765 .122.06 84.5734 235.69 84.8235 80.19 0.0000 122.92 86.9312 235. 96 87.5510 80.57 90.6986 123.07 90.2253 238.63 82.9361 81. 00 88.2778 265.00 87.0978 238.98 0.0000 81. 07 88.2996 125.81 99. 2372 240.99 83.2206 81. 75 93.6419 127.23 88.9673 242.00 83.3422 83.79 86.2323 127.91 89.1169 244.70 66.8419 84.00 91. 7885 129.30 89.4181 252.40 0.0000 85.43 116. 9193 131.20 89.8297 252.80 59.7890 86.55 109.5365 133.02 84. 6511 254.15 0.0000 86. 79 109.6237 133.52 87. 7258 256.23 81.3296 86.94 99.2336 136.00 86.3677 260.90 0.0000 Page 3428 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 42.0667 355.39 0.0000 584.27 32.0203 264.80 42.0740 356.01 39.0137 595.83 0.0000 265.00 33.6680 364.49 0.0000 427.87 45.6958 268.22 56.3538 366.42 0.0000 602.52 0.0000 269.46 62.0912 372. 51 43.3748 604.72 36.6539 270.03 62.1368 375.05 37.1206 607.14 41.3016 271.23 62.2349 377.52 55.2849 609.32 34.4663 273.65 0.0000 356.01 45.9998 610.33 34.4883 276.40 69.2989 388.16 40.8203 614.28 46.1016 277.37 71. 28 60 388.63 0.0000 618.01 35.2087 277.60 69.4058 391. 69 58.2034 620.36 33.7460 278.00 62.7827 264.66 44.5668 621. 93 37. 6396 279.20 57.1619 401.81 52.2314 630.19 0.0000 279.54 68.6250 402.40 42.4611 631.29 30.0956 279.70 68.6382 404.85 60.0175 633.25 29 .1605 280.46 60.1174 410.95 58.1596 634.78 0.0000 283.69 68.9854 413.71 47.3051 635.95 31.1563 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 50.8909 423. 72 0.0000 645.85 43.8853 285.90 0.0000 427.09 50.1013 657.76 33.1529 287.50. 65.4641 427.87 53.4785 657.90 0.0000 290.67 75.3871 433.94 44.8031 661. 66 49.0551 293.27 0.0000 439.40 42.7639 664.57 0.0000 351. 93' 58.3142 453.88 46.1409 666.33 0.0000 295.96 58.3667 463.37 63.72.92 666.50 0.0000 879.38 67.3337 468.07 44.9549 667.71 0.0000 299.98 61.5824 473.00 0.0000 677.62 27.3842 300.09 61.5901 475.06 42.8919 685.70 0.0000 300.13 61.5939 476.78 39.4681 695.00 0.0000 301.36 61.6849 477.60 56.9184' 696.49 42.3935 302.85 52. 9662 482.18 30. 3116 696.51 42.3935 256.23 58.9673 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 38.3734 306.78 60 .1114 497.08 33.6159 697.49 40.3979 308.46 54.3051 505.52 35.6146 702.65 3.8. 8957 311. 90 47.5840 507.63 0.0000 706.68 34.5178 316.51 59.7974 511. 00 35.7629 711. 68 34.2070 319.41 0.0000 514.00 35.8435 720.70 0.0000 320.08 0.0000 514.00 35.8435 72L93 0.0000 321. 04 56.0991 520.40 33 .1344 722.78 19.6682 323.87 46.2284 520.69 0.0000 722. 91 26.2258 325.23 82.5322 522.65 0.0000 723.31 26.2320 328.76 0.0000 527.90 0.0000 724.19 37.7265 333.37 68.5533 528.26 36.2244 727.33 30.8084 333.97 57.9277 529.59 32.6338 733.00 26.3719 334.37 62.5285 529.87 0.0000 735.93 25.9424 338.28 58.1991 531. 02 0.0000 333.97 30.9796 338.32 58.2026 537.26 0.0000 739.50 0.0000 311. 90 58.3383 546.56 0.0000 747.24 30.1054 340.48 58.3383 552.55 31. 3313 748.06 27.0029 340.55 0.0000 563.25 39.9214 752.31 30.1877 344.28 53.9505 569.33 37.2925 753.82 0.0000 345.93 60.2222 946.00 37.2961 756.73 25.0415 351.06 48.6457 569.70 37.3010 756.80 25.0422 351.93 48.6906 583.19 31.9974 884.68 21. 7852 Page 3429 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.1293 1274.44 24.8932 1620.50 10.4983 766.42 25.1697 1001.03 16.0342 1621.92 10.5018 766.84 21.8188 1002.74 27.1436 1678.03 0.0000 772.60 0.0000 1004.73 26.2295 1690.97 8.7477 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 .1764.49 6.9294 778.90 26.3893 1028.54 0.0000 1063.66 5.0981 783.70 0.0000 1037.84 24.6835 1771. 35 3.3997 785.37 27.5361 1038.76 0.0000 1791.20 0.0000 792.07 42.5085 631. 29 17.4659 1808.65 12.0059 794.95 19.1569 1048.07 0.0000 1810.72 0.0000 795.86 24.4901 1049.04 19. 0723 '1836.06 4.0282 810.06 19.3035 1050.41 19.0820 810.29 20.3783 l063.66 0.0000 344.28 20.3794 1077.00 0.0000 810.76 21. 4557 1077.34 27.9606 815.77 0.0000 .1085.87 24.1833 1048.07 0.0000 1093.63 22.3149 832.01 32.5223 1099.45 21. 3909 834.85 33.6527 1112. 07 18.4536 835.71 35.8390 ll12.84 19.5449 836.80 0.0000 1115. 54 17.9341 846.75 0.0000 1120.29 24.4983 846.77 26.2039 1120. 55 24.5007 856.80 0.0000 1221. 41 24.5081 860.56 20.8810 1129. 67 31.6857 871. 09 15.4625 1131. 51 0.0000 873.19 22 .1109 1147.95 0.0000 875.33 0.0000 1173.23 29.9700 879.38 19. 9572 1177.95 22.0150 880.51 25.5142 1189.05 26.7891 883.24 29.9894 1204.77 25.2539 884.68 28.8977 1221. 41 24.3832 889.28 26.7312 1231. 02 29.1225 894.76 27.9144 1235.36 0.0000 898.04 20.1286 1238.28 31.6766 900. 72 17.9141 1260.41 0.0000 903.28 29.1437 1271.87 20.6670 911.20 32.6223 1274.44 13.7897 912.08 39.0127 1274.54 13.7904 923.98 0.0000 1291.59 20.8018 926.50 21.7459 1298.22 0.0000 929 .11 21. 7711 1312.11 0.0000 937.49 25.4933 1332.49 12.2944 *944 .13 0.0000. 1362.66 0.0000 946.00 27.4153 1365.19 10.6470 949.0b 21. 9609 1368.63 0.0000 667. 71 0.0000 1384.29 19.6340 962.31 32.2101 1408.01 10.7866 964. 08 30.6991 1457 .56. 0.0000 966 .17 35.3357 1460.82 8.7652 911. 20 35.0702 1489.16 17.4901 968. 97 35.0702 1505.03 11.0967 983.53 0.0000 1584.12 16.2026 984.45 0.0000 1596.21 0.0000 Page 3430 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:59:48.23 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.qAMMA]G405235023.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM24.CNF;330 Background date : 2-0CT-2016 11:01:18. Sample date 2-DEC-2015 10:40:00. Acquisition date : 3-0CT-2016 08:58:40. Sample ID G405235023 Sample quantity l.41404E+02 GRAM Detector name : GAM24 . Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:02.00 0.1% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ********************************************************************************" Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 2 2 4 4 4 4 0 0 0 5 5 o* 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3431 of 5809 Energy 46.77* 63.47* 65.12* 73.16 75.05* 77.26* 84.43* 87.31 90.04 92.84* 110. 08* 186.31* 209.29 238.71* 242.02 295.40 300.12 311.47 338.32 352.11* 464.13 511.80*

583.38* 609.68* 662.16 670.22 727. 02* 768.38* 786.48 794.86* 809.16 860.47 873.29 911. 42* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 16 40 12 37 201 268 48 106 61 111 9 92 ' 27 450 117 186 44 25 105 306 19 1 139 205 135 26 33 14 20 29 10 17 25 71 FWHM Channel Left Pw Cts/Sec %Err 158 168 159 230 215 140 135 138 120 144 136 137 91 59 94 50 38 100 80 56 67 100 36 56 53 43 32 25 15 12 11 21 35 31 1. 35 1. 23 0.94 1. 25 1. 26 1. 04 1. 54 1.16 1. 07 1.19 1.28 1. 07. 0.83 1.24 2.03 1. 32 1. 54 5.35 1. 23 1. 47 1.15 2.36 1. 35 1.76 1. 51 0.73 3.34 0.78 1. 46 1. 56 0.91 0.90 10.38 1. 23 93.59 127.00 130.30 146.38 150.17 154.58 168.92 174.68 180.15 185.75 220.24 372.73 418.71 477.56 484.17 590.97 600.42 623.13 676.84 704.43 928.53 1023.91 1167 .13 1219.74 1324.74 1340.86 1454.52 1537.26 1573.47 1590.24 1618.85 1721. 52 1747.18 1823.47 89 123 123 143 143 143 165 165 165 165 219 *368 416 471 471 586 596 613 670 699 923 1014 1161 1213 1316 1334 1447 1532 1570 1584 1614 1718 1733 1818 9 4.37E-03149.3 10 1. lOE-02 58. 5 10 3.29E-03174.0 22 l.02E-02 76.1 22 5.58E-02 14.6 22 7.45E-02 9.9 27 1. 33E-02 44. 0 27 2. 95E-02 21. 0 27 1. 69E-02 31.1 27 3. 07E-02 21. 6 8 2.58E-03222.l 10 2.56E-02 27.0 7 7.47E-03 62.2 23 1. 25E-01 5. 6 23 3.25E-02 24.1 9 5.17E-02 10.0 8 1.23E-02 28.5 17 6.86E-03 95.7 14 2.91E-02 20.6 13 8.49E-02 7.8 12 5.23E-03 89.5 16 l.53E-04***** 11 3.87E-02 12.l 17 5.70E-02 11.2 18 3.74E-02 15.4 17 7.08E-03 61.8 16 9.29E-03 42.4 11 4.00E-03 73.0 11 5.69E-03 41.7 10 8.15E-03 30.0 8 2.84E-03 65.5 9 4.69E-03 54.1 28 7.03E-03 69.0 13 1.96E-02 20.8 Fit 3.93E+OO 2.62E+OO 8.15E-01 l.69E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235023 Acquisition date : 3-0CT-2016 08:58:40 Pk It 'Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964. 51 33 6 2.25 1929.71 1925 9 9.06E-03 22.6 36 0 968.92* 54 6 2.22 1938.53 1934 11 1.51E-02 17.1 37 0 1053.71 18 6 1.85 2108.19 210*4 10 5.08E-03 33.0 38 0 1120. 43* 41 19 2. 21 2241. 70 2236 11 1.13E-02 26.6 39 0 1161.19 10 12 1. 28 2323. 27 2317 9 2.69E-03 74.7 40 0 1169.26 15 17 0.96 2339.43 2331 14 4,05E-03 66.2 41 0 1256.53 11 14 0.65 2514.06 2507 10 3.07E-03 71.6 42 0 1281.19 14 11 1.80 2563.42 2557 10 3.81E-03 54.7 43 0 1322.81 5 3 1.24 2646. 70 2643 6 1.39E-03 70.7 44 0 1353.65 7 0 0. 73 2708. 43 2705 6 1. 94E-03 37. 8 45 0 1356.56 8 0 0.73 2714.25 2711 6 2.22E-03 35.4 46 0 1377.81 22 3 2.85 2756.78 2751 11 6.19E-03 25.6 47 0 1408.39 15 3 1.93 2817.97 2813 11 4.17E-03 33.6 48 0 1460.82* 352 4 . 2.44 2922.89 2915 15 9.79E-02 5.5 49 0 1588.14 12 2 1.87 3177.70 3173 9 3.30E-03 36.7 50 0 1620.84 13 0 3.16 3243.15 3238 11 3.61E-03 27.7 51 0 1764.52* 37 3 0.86 3530.73 3524 12 1.03E-02 20.0 Flag: "*" = Peak area was modified by background subtraction \, ' Page 3432 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:59:50 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 10:40:00 G405235023 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:58:40 141.40 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit . SOLID GAMMA24 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3433 of 5809 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Lirie RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351 .. 06 CAN 0 01:00:02.00 10.00 0.00 % Peak Energy 0.1% Nuclide Line Activity Report Page : 2 Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.354E+OO 1.243E+Ol l.243E+Ol 11. 03 OK CD-109 88.03 3.70* 7.499E+OO 1. 317E+OO 2.086E+OO 80.27 OK TE-125M 109.28 0.27* 7.981E+OO 2. 721E+OO 1.095E+02 444.12 OK SN-126 64.28 9.60 5.554E+OO 4.883E-01 4.883E-01 116. 90 OK 86.94 8.90 7.499E+OO 5.477E-01 5.477E-01 80.27 OK 87.57 37.00* 7.499E+OO 1. 317E-01 1. 317E-01 80.27 OK BA-137M 661.66 89.90* 2.532E+OO 3.236E-01 3.299E-01 30.82 OK CS-137 661.66 85.10* 2.532E+OO 3.419E-01 3.486E-01 30.82 OK TL-208 277.37 6.60 5.023E+OO Line Not Found Absent 583.19 85.00* 2.790E+OO 3.245E-01 3.245E-01 24.30 OK 860.56 12.50 2.074E+OO 3.480E-01 3.480E-01 108.30 OK PB-210 46.54 4.25* 2.491E+OO 9.993E-01 1. 026E+OO 298.62 OK BI-212 727. 33 6.67* 2.358E+OO 1.153E+OO 1.153E+OO 84.77 OK 785.37 1.10 2. 221E+OO 4. 513E+OO 4.513E+OO 83.37 OK 1620.50 1. 47 1.233E+OO 3.617E+OO 3.617E+OO 55.47 OK PB-212 74.82 10.28 6.749E+OO 1.184E+OO 1.184E+OO 48.04 OK 77 .11 17.10 6.918E+OO 1.472E+OO 1. 472E+OO 19.84 OK 238.63 43.60* 5.637E+OO 1.091E+OO 1. 091E+OO 11.14 OK 300.09 3.30 4.720E+OO 1.656E+OO 1.656E+OO 56 .'97 OK BI-214 609.32 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 OK 1120. 29 14.92 1.689E+OO 8.435E-01 8.438E-01 53.28 OK 1764.49 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 OK PB-214 74.82 5.80 6.730E+OO Line Not Found <<INT Reject 77 .11 9.70 6.918E+OO 2.595E+OO

2.596E+OO 19.84 OK 87.09 3.41 7.489E+OO Line Not Found. -----<<INT Reject *,_ 242.00 7.25 5.579E+OO Line Not Found <<INT Reject 295.22 18.42 4.779E+OO 1.238E+OO l.239E+OO 20.01 OK 351.93 35.60* 4.154E+00 1.193E+OO 1.193E+OO 15.55 OK RN-222 609.32 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 OK 1120.29 14.92 1. 689E+00 8.435E-01 8.438E-01 53.28 OK 1764.49 15.30 l.138E+OO 1.066E+OO l.066E+OO 39.91 OK RA-224 240.99 4.10* 5.579E+00. 8.509E-01 8.509E-01 179.75 OK RA-226 609.32 45.49* 2.697E+00 9.213E-01 9.216E-01 22.32 OK 1120.29 14.92 1.689E+OO 8.435E-01 8.438E-01 53.28 OK 1764.49 15.30 1.138E+OO l.066E+OO 1.066E+OO 39.91 OK AC-228 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.289E+OO 1.254E+OO l.254E+OO 41. 25 OK 794.95 4.25 2.204E+OO 1.687E+OO 1. 687E+OO 60.00 OK 835.71 1. 61 2.121E+OO Line Not Found Absent 911.20 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 OK 968.97 15.80 1.893E+OO 9.598E-01. 9.598E-01 34.24 OK RA-228 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11.27 4.289E+00 1.254E+OO 1.254E+OO 41. 25 OK 794.95 4.25 2.204E+OO l.687E+OO 1.687E+OO 60.00 OK 835.71 1. 61 2 .121E+OO Line Not Found Absent 911.20 25.80* l.985E+00 7.334E-01 7.334E-01 41. 55 OK 968.97 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 OK TH-228 74.82 10.28 6.749E+OO l.184E+00 l.184E+OO 48.04 OK 77 .11 17.10 6.918E+OO 1. 472E+OO 1.472E+OO 19.84 OK Page 3434 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235023 Acquisition.date 3-0CT-2016 08:58:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 5.637E+OO 1.091E+OO 1.091E+OO 11.14 OK 300.09 3.30 4.720E+OO 1.656E+OO l.656E+OO 56.97 OK TH-229 85.43 14.70 7.361E+OO 2.859E-01 2.859E-01 87.98 OK 88.47 24.00 . 7.499E+OO 2.031E-01 2.031E-01 80.27 OK 193.51 4.41* 6.531E+OO Line Not Found Absent 210.85 2.80 6.166E+OO Line Not Found Absent TH-230 609.32 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 OK 1120.29 14.92 1. 689E+OO 8.435E-01 8.435E-01 53.28 OK 1764.49 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 OK PA-231 283.69 1. 70 4.935E+OO Line Not Found Absent 301.36 5.35* 4.720E+00 l.022E+OO 1. 022E+oo* 56.97 *OK TH-232 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.289E+OO 1.254E+OO 1.254E+OO 41. 25 OK 835.71 1. 61 2 .121E+OO Line Not Found Absent 911. 20. 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 OK 968. 97 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 OK PA-233 300 .13 6.63 4.720E+OO 8.243E-01 8.243E-01 56.97 OK 311. 90 38.50* 4.582E+OO 8 .161E-02 8.161E-02 191.33 OK 340.48 4.45 4.267E+OO Line Not Found Absent TH-234 63.29 3.70* 5.554E+OO 1.267E+OO 1.267E+OO 116.90 OK 92.59 4.23 7.706E+OO 2.171E+OO 2.171E+00 43.23 OK U-234 609.32 45.49* 2.697E+OO 9.213E-01 9. 213E..:.01 22.32 OK 1120.29 14.92 1.689E+OO 8.435E-01 8.435E-01 53.28 OK 1764.49 15.30 1.138E+OO 1.066E+OO l.066E+OO 39.91 OK U-235 89. 96 3.47 7.610E+OO l.480E+OO 1.480E+OO 62.13 OK 93.35 5.60 7.706E+00 1.640E+OO 1.640E+OO 43.23 OK 143.76 10. 96* 7.620E+OO Line Not Found Absent 163.33 5.08 7.206E+OO Line Not Found Absent 185.72 57.20 6;689E+OO l.465E-01 1.465E-01 54.04 OK 205.31 5.01 6.280E+OO Line Not Found Absent U-238 63.29 3.70* 5.554E+OO 1.267E+OO 1.267E+OO 116. 90 OK 92. 59 4.23 7.706E+OO 2.171E+OO 2.171E+OO 43.23 OK AM-243 43.53 5.90 1.694E+OO Line Not Found Absent 74.66 67.20* 6.749E+OO l.812E-01 l.812E-01 48.04 OK ANH-511 511. 00 100.00* 3.088E+OO 9.971E-04 9.971E-048945.20 OK Flag: "*" = Keyline Page 3435 of 5809 VAX/VMS ,Nuclide Identification Report Generated 03-0CT-2016 09:59:51.05 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration :* DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l *
Acquisition date 3-0CT-2016 08:58:40 Sensitivity : 3.000 *
Detector ID
GAM24 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:02.00 Half life ratio : ***** *
Sample date 2-DEC-2015 10: 4.0: 00 Analyst initials: MXRl *
Sample ID G405235023 Sample Quantity 1.4140E+02 GRAM *
Batch Number 1596249 Wet Weight* 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid .. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.243E+Ol 1.344E+OO 4.832E-01 .. CD-109 2.086E+OO 1.641E+OO l.487E+00 TE-125M l.095E+02 4.764E+02 4.587E+02 SN-126 l.317E-01 1.036E-01 9. 410E-02. BA-137M 3.299E-01 9. 966E-02 5.785E-02 CS-137 3.486E-01 l.053E-01 6. lllE-02 TL-208 3.245E-01 7.726E-02 5.906E-02 PB-210 1. 026E+OO 3.002E+OO 2.460E+OO BI-212 1.153E+OO 9.578E-01 7.389E-01 PB-212 1.091E+OO l.192E-01 8.285E-02 BI-214 9.216E-01 2.016E-01 l.125E-01 PB-214 1.193E+OO 1.819E-01 1.075E-01 RN-222 9.216E-01 2.016E-01 1.125E-01 RA-224 8.509E-01 1.499E+OO 8.882E-01 RA-226 9.216E-01 2.016E-01 1.125E-01 AC-228 7.334E-01 2.986E-01 2.451E-01 RA-228 7.334E-01 2.986E-01 2.451E-01 TH-228 1.091E+OO 1.192E-01 8.285E-02 TH-229 4.141E-01 4.432E-01 8.579E-01 TH-230 9:213E-01 2.015E-01 1.124E-01 PA-231 1.022E+OO 5.703E-01 7.210E-01 TH-232 7.334E-01 2.986E-01 2.451E-01 PA-233 8.161E-02 l.530E-01 9.713E-02 TH-234 1. 267E+OO 1. 451E+OO l.385E+00 U-234 9.213E-01 2.015E-01 l.124E-01 U-235 -7.143E-02 1.739E-01 3.090E-01 U-238 1. 267E+OO 1.451E+OO 1.385E+OO AM-243 l.812E-01 8.530E-02 6.331E-02 ANH-511 9.971E-04 8.741E-02 5.169E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -4.962E+OO 1.228E+Ol 2.252E+Ol NOT IDENT. Page 3436 of 5809 NA-22 1.243E-02 5.037E-02 9.585E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 7. 081E-03 2.274E-02 5.523E-02 NOT IDENT. SC-46 -5.738E-01 3.732E-01 4.987E-01 FAIL ABUN V-48 O.OOOE+OO l.642E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4 .118E+02 O.OOOE+OO SHORT HLIF MN-54 -3.323E-02 6. 726E-02 1.157E-01 NOT IDENT. C0-56 7.905E-02 4.295E-01 8.435E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 7.259E-03 4.035E-02 7.560E-02 NOT IDENT. C0-58 2.659E-01 3.646E-01 8.222E-01 NOT IDENT. FE-59 -5.545E+OO 6.252E+OO l.070E+Ol NOT IDENT. C0-60 7.350E-03 2.885E-02 6.330E-02 NQT IDENT. ZN-65 1. 056E-01 1. 649E-01 3.299E-01 NOT IDENT. GE--68 -2.103E-01 1. 881E+OO 3.763E+OO NOT IDENT. AS-73 3.431E+OO 4.973E+OO 9.828E+OO NOT IDENT. AS-74 O.OOOE+OO 7.107E+03 O.OOOE+OO SHORT HLIF SE-75 -9.210E-02 1.883E-01 3.549E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 27 0E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.798E+02 O.OOOE+OO SHORT HLIF RB-83 5.320E-02 6.081E-01 1.188E+OO NOT IDENT. KR-85 4.224E+00 7.385E+OO l.359E+Ol NOT IDENT. SR-85 4.720E-01 8.315E-01 1.529E+OO NOT IDENT. RB-86 0.000E+OO 2.780E+04 0.000E+OO SHORT HLIF Y-88 2.103E-02 2.149E-01 4.626E-01 NOT IDENT. Y-91 2. 930E+.01 4.811E+02 9.673E+02 NOT IDENT. NB-94 5.166E-03 2.952E-02 5.700E-02 NOT IDENT. NB-95 -3.463E-01 9.430E-01 1. 461E+OO NOT IDENT. NB-95M -1.482E-01 2.294E+OO 4.049E+OO NOT IDENT. ZR-95 -5.707E-01 1.552E+OO 2.757E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 6.430E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.290E-02 3.143E-02 5.562E-02 NOT IDENT. RH-102 2.lOOE-02 5.312E-02 1. 073E-01 NOT IDENT. RU-103 -1.115E-01 6.133E+OO 1.173E+Ol FAIL ABUN RH-106 -2.431E-01 4.526E-01 7.994E-01 NOT IDENT. RU-106 -2. 431E-01 4.526E-01 7.994E-01 NOT IDENT. AG-108M 6.719E-03 2.650E-02 5.237E-02 NOT IDENT. AG-110M -5.599E-02 9.755E-02 1. 651E-01 NOT IDENT. SN-113 2.579E-02 2.076E-01 4. 091E-01 NOT IDENT. CD-115 O.OOOE+OO 1.904E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1. 176E+05 O.OOOE+OO SHORT HLIF TE-123M 5.449E-02 l.229E-01 2.315E-01 NOT IDENT. SB-124 1. 875E+OO 2.188E+OO 5.319E+OO NOT IDENT. SB-125 2.521E-02 9.217E-02 1.840E-01 FAIL ABUN I-126 O.OOOE+OO 1.484E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 467E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.558E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 7 .131E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.275E+27 O.OOOE+OO SHORT HLIF BA-133 6.630E-03 3.279E-02 6.031E-02 NOT IDENT. I-133 O.OOOE+OO 1. 431E+41 O.OOOE+OO SHORT HLIF 1. lllE-01 6. 531E-02 1.171E-01 FAIL ABUN CS-135 -l.159E-01 1.189E-01 2.139E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 3.586E+05 O.OOOE+OO SHORT HLIF CE-139 2.532E-02 1. 080E-01 1. 988E-01 --NOT IDENT. BA-1"40 O.OOOE+OO 1. 622E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.622E+05 O.OOOE+OO SHORT HLIF CE-141 7.869E+OO 2.563E+Ol 4.766E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -6. 451E-02 3.266E-01 5.875E-01 NOT IDENT. PM-144 1.707E-03. 4. 896E-02 9.367E-02 NOT IDENT. 1.488E-Ol 4.267E+OO 8.163E+OO NOT IDENT. PM-146 2.504E-02 3.878E-02 8.043E-02 NOT IDENT. ND-147 O.OOOE+OO 4.673E+07 O.OOOE+OO SHORT HLIF PM-147 3.721E+02 6.950E+02 1.340E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -8.459E-03 2.594E-02 4.347E-02 FAIL ABUN EU-152 -1.209E-02 8.335E-02 1.531E-01 FAIL ABUN GD-153 -1.662E-02 1.647E-01 2. 7 96E-01 NOT IDENT. EU-154 2. 611E-02 1.224E-01 2.318E-01 FAIL ABUN EU-155 7.348E-02 8.533E-02 1.696E-01 FAIL ABUN TB-160 1.838E-01 2.302E+OO 3.875E+OO FAIL ABUN "H0-166M -9.090E-03 5.178E-02 9.582E-02 FAIL ABUN Page 3437 of 5809 TM-171 1.848E+OO 1.052E+Ol 2.043E+Ol NOT IDENT. HF-172 2.587E-02 1.950E-01 3.630E-01 FAIL ABUN LU-172 3.856E-02 7.593E-02 1.599E-01 FAIL ABUN LU-176 -7.838E-03 2.299E-02 3.883E-02 FAIL ABUN HF-181 -8.063E-01 4.423E+OO 8.338E+OO NOT IDENT. TA-182 9.328E-01 8.809E-01 1. 972E+OO FAIL ABUN RE-183 5 .*395E-01 1.747E+OO 3.407E+OO NOT IDENT. RE-184 3.575E+Ol 3.237E+Ol 7.099E+Ol NOT IDENT. W-188 -l.181E+02 l.134E+02 1. 740E+02 FAIL ABUN IR-192 1.622E-01 4.426E-01 8.208E-01 FAIL ABUN HG-203 -1.083E-01 2.290E+OO 4.467E+OO FAIL ABUN BI-207 -3.287E-03 3.269E-02 6.685E-02 FAIL ABUN
BI-211 O.OOOE+OO 5.009E-01 7.826E-01 FAIL ABUN PB-211 3.499E-01 5.572E-01 l.158E+OO NOT IDENT. RN-219 -6.484E-02 3.377E-01 6.414E-01 NOT IDENT. RA-223 l.260E-01 5.033E-01 l.007E+OO FAIL ABUN AC-227 2.015E-01 2.012E-01 4. 251E-01 FAIL ABUN TH-227 2.015E-01 2.012E-01 4. 251E-01 FAIL ABUN TH-231 1.260E-01 5.033E-01 1.007E+OO FAIL ABUN PA-234 -1. 091E-01 2.326E-01 4.105E-01 FAIL ABUN PA-234M 1.210E+OO 3. 722E+OO 7.801E+OO NOT IDENT. NP-237 8.161E-02 l.530E-01 9.516E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 7.289E-02 2. 051E-01 3.896E-01 NOT IDENT. PU-239 1. 216E+02 3.023E+02 5.660E+02 NOT IDENT. AM-241 -1.082E-02 8.487E-02 l.480E-01 NOT IDENT. CM-243 -1.628E-03 7.335E-02 1.369E-01 NOT IDENT. BK-247 -2.981E-02 '6. 259E-02 l.181E-01 FAIL ABUN CM-247 1. 744E-02 2.802E-02 5.858E-02 NOT IDENT. CF-249 3.766E-03 3.437E-02 6.724E-02 NOT IDENT. CF-251 1. 701E-02 1.069E-01 1.953E-01 NOT IDENT. Page 3438 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:59:48.93 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Erro,r K-40 1460.82 338 10.66* 1.354E+OO 1.243E+Ol 1.243E+Ol 11. 03 CD-109 88.03 128 3.70* 7.499E+OO 2.459E+OO 3.893E+OO 42.00 TE-125M 109.28 11 0.27* 7. 981E+OO 2.721E+OO l.095E+02 444.12 SN-126 64.28 49 9.60 5.554E+OO 4.883E-01 4.883E-01 116. 90 86.94 128 8.90 7.499E+OO 1.022E+OO 1.022E+OO 42.00 87.57 128 37.00* 7.499E+OO 2.459E-01 2.459E-01 42.00 BA-137M 661.66 139 89.90* 2.532E+OO 3.236E-01 3.299E-01 30.82 CS-137 661.66 139 85.10* 2.532E+OO 3.419E-01 3.486E-01 30.82 TL-208 277.37 ------6.60 5.023E+OO ------Line Not Found ------583.19 145 85.00* 2.790E+OO 3.245E-01 3;245E-01 24.30 860.56 17 12.50 2.074E+OO 3.480E-01 3.480E-01 108.30 PB-210 46.54 20 4.25* 2. 491E+OO 9.993E-01 1.026E+OO 298 .. 62 BI-211 72. 87 45 1.23 6.591E+OO 2.940E+OO 2.940E+OO 152.14 351.06 332 12.92* 4.154E+OO 3.287E+OO 3.287E+OO 15.55 BI-212 727.33 34 6.67* 2.358E+OO 1.153E+OO 1.153E+OO 84.77 785.37 21 1.10 2. 221E+OO 4.513E+OO 4.513E+OO 83.37 1620.50 12 1. 47 1.233E+OO 3.617E+OO 3.617E+OO 55.47 PB-212 74.82 246 10.28 6.749E+OO 1.883E+OO 1.883E+OO 29.29 77 .11 328 17.10 6.918E+OO 1. 472E+OO 1.472E+OO 19.84 238.63 505 43.60* 5.637E+OO 1. 091E+OO 1.091E+OO 11.14 300.09 49 3.30 4.720E+OO 1. 656E+OO 1. 656E+OO 56.97 BI-214 609.32 213 45.49* 2.697E+OO 9. 213E-01 9.216E-01 22.32 1120.29 40 14.92 1. 689E+OO 8.435E-01 8.438E-01 53.28 1764.49 35 15.30 l.138E+OO 1.066E+OO 1. 066E+OO 39.91 PB-214 74.82 246 5.80 6.749E+OO 3.337E+OO 3.338E+OO 29.29 77 .11 328 9.70 6.918E+OO 2.595E+OO 2.596E+OO 19.84 87.09 128 3.41 7.499E+OO 2.668E+OO 2.669E+OO 42.00 242.00 131 7.25 5.579E+OO 1. 719E+OO 1. 720E+OO 48.20 295.22 205 18.42 4.779E+OO 1.238E+OO 1.239E+OO 20.01 351.93 332 35.60* 4.154E+OO 1.193E+OO 1.193E+OO 15.55 RN-,222 609.32 213 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 1120.29 40 14.92 1.689E+OO 8.435E-01 8.438E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO l.066E+OO 39.91 RA-224 240.99 131 4.10* 5.579E+OO 3.040E+OO 3.040E+OO 48.20 RA-226 609.32 213 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 1120.29 40 14.92 1.689E+OO 8.435E-01 8.438E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 AC-228 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 114 11. 27 4.289E+OO 1.254E+OO 1.254E+OO 41.25 794.95 30 4.25 2.204E+OO 1.687E+OO 1.687E+OO 60.00 835.71 ------1. 61 2 .121E+OO ------Line Not Found ------911.20 71 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 968. 97 54 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 RA-228 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 114 11. 27 4.289E+OO 1.254E+OO l.254E+OO 41. 25 794.95 30 4.25 2.204E+OO 1.687E+OO 1.687E+OO 60.00 835. 71 ------1. 61 2.121E+OO ------Line Not Found ------Page 3439 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 71 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 968. 97 54 15.80 l.893E+OO 9.598E-01 9.598E-01 34.24 TH-228 74.82 246 10.28 6.749E+OO 1.883E+OO 1.883E+OO 29.29 77 .11 328 17.10 6.918E+OO l.472E+OO 1.472E+OO 19.84 238.63 505 43.60* 5.637E+OO 1. 091E+OO 1.091E+OO 11.14 300.09 49 3.30 4.720E+OO 1.656E+OO 1.656E+OO 56.97 TH-229 85.43 58 14.70 7.361E+OO 2.859E-01 2.859E-01 87.98 88.47 128 24.00 7.499E+OO 3.790E-01 3. 791E-01 42.00 193.51 ------4.41* 6.531E+OO ------Line Not Found ------210.85 ------2.80 6.166E+OO ------Line Not Found ------TH-230 609.32 213 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 1120.29 40 14.92 1.689E+00 8.435E-01 8.435E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 PA-231 283.69 ------1. 70 4.935E+OO ------Line Not Found ------301.36 49 5.35* 4. 720E+OO 1.022E+OO 1.022E+OO 56.97 TH-232 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 114 11.27 4.289E+OO l.254E+OO 1.254E+OO 41. 25 835.71 ------1. 61 2.121E+OO ------Line Not Found ------911.20 71 25.80* 1.985E+OO 7.334E-01' 7.334E-01 41. 55 968. 97 54 15.80 1.893E+00 9.598E-01 9.598E-01 34.24 PA-233 300.13 49 6.63 4.720E+OO 8.243E-01 8.243E-01 56.97 311. 90 27 38.50* 4.582E+OO 8.161E-02 8.161E-02 191.33 340.48 ------4.45 4.267E+OO ------Line Not Found ------TH-234 63.29 49 3.70* 5.554E+OO .l.267E+OO 1. 2 67E+00 116.90 92.59 133 4.23 7.706E+OO 2 .171E+OO 2.171E+OO 43.23 U-234 609.32 213 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 1120. 29 40 14.92 1. 689E+OO 8.435E-01 8.435E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 U-235 89. 96 74 3.47 7.610E+OO 1.480E+OO l.480E+00 92.13 93.35 133 5.60 7.706E+OO 1.640E+OO 1.640E+OO 43.23 143.76 ------10. 96* 7.620E+OO ------Line Not Found ------163.33 ------5.08 7.206E+OO ------Line Not Found ------185.72 106 57.20 6.689E+OO l.465E-01 l.465E-01 54.04 205.31 ------5.01 6.280E+OO ------Line Not Found ------U-238 63.29 49 3.70* 5.554E+OO l.267E+OO l.267E+OO 116.90 92.59 133 4.23 7.706E+OO 2.171E+OO 2. l 71E+OO 43.23 AM-243 43.53 ------5.90 1.694E+OO ------Line Not Found ------246 67.20* 6.749E+OO 2.880E-01 2.881E-01 29.29 ANH-511 511. 00 1 100.00* 3.088E+OO 9. 971E-04 9. 971E-04 8945.20 Flag: "*" Key line Page 3440 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Total number of lines in spectrum 51 Number of unidentified lines 14 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 57.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y l.41E+l0Y 1600. DOY 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1.41E+l0Y 1. 41E+10Y 1. 41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 2.14E+06Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 58 40.2 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.243E+Ol 2.459E+OO 2. 721E+OO 2.459E-01 3.236E-01 3.419E-01 3.245E-01 9.993E-01 3.287E+00 1.153E+OO 1. 091E+OO 9.213E-01 1.193E+OO 9.213E-01 3.040E+OO 9.213E-01 7.334E-01 7.334E-01 1.091E+OO 3.790E-01 9.213E-01 1.022E+OO 7.334E-01 8.161E-02 1.267E+OO 9.213E-01 l.465E-01 1.267E+OO 2.880E-01 9.971E-04 4 .196E+Ol 4 .196E+Ol Decay Corr pCi/GRAM l.243E+Ol 3.893E+OO 1.095E+02 2.459E-01 3.299E-01 3.486E-01 3.245E-01 1.026E+OO 3.287E+OO 1.153E+OO 1.091E+OO 9.216E-01 1.193E+OO 9.216E-01 3.040E+OO . 9.216E-01 7.334E-01 7.334E-01 1. 091E+OO 3. 791E-01 9.213E-01 1.022E+OO 7.334E-01 8.161E-02 1.267E+OO 9.213E-01 1.465E-01 1.267E+OO 2.881E-01 9.971E-04 l.502E+02 l.502E+02 72.55% Decay Corr 2-Sigma Error 0.137E+Ol 1.635E+OO 4.862E+02 1.033E-01 1. 017E-01 l.074E-01 0.788E-01 3.063E+OO 0. 511E+OO 0.977E+OO 0.122E+OO 2.057E-01 0.186E+OO 2.057E-01 1.465E+OO 2.057E-01 3.047E-01 3.047E-01 0.122E+OO l.592E-01 2.056E-01 0.582E+OO 3.047E-01 15.61E-02 1.481E+OO 2.056E-01 0.792E-01 1.481E+OO 0.844E-01 891.9E-04 Manually accepted 2-Sigma %Error 11'. 03 42.00 444.12 42.00 30.82 30.82 24.30 298.62 15.55 "84.77 11.14 22.32 15.55 22.32 48.20 22.32 41. 55 41. 55 11.14 42.00 22.32 56.97 41. 55 191.33 116.90 22.32 54.04 116. 90 29.29 8945.20 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 3441of5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235023 Acquisition date : 3-0CT-2016 08:58:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 2 65.12 15 197 0.94 130. 30 123 10 3.29E-03 **** 5.76E+OO 0 209.29 30 103 0.83 418. 71 416 7 7.47E-03 **** 6.20E+OO 0 464.13 20 71 1.15 928.53 923 12 5.23E-03 **** 3.33E+OO T 0 670.22 26 44 0.73 1340.86 1334 17 7.08E-03 **** 2.51E+OO 0 768.38 15 25 0.78 1537.26 1532 11 4.00E-03 **** 2.26E+OO 0 809.16 10 11 0.91 1618.85 1614 8 2.84E-03 **** 2.17E+00 T 0 873.29 25 35 10.38 1747.18 1733 28 7.03E-03 **** 2.05E+00 T 0 964. 51 32 6 2.25 1929.71 1925 9 9.06E-03 45.1 1.90E+OO T 0 1053.71 18 6 1. 85 2108.19 2104 10 5.08E-03 66.1 l.77E+OO 0 1161.19 g 12 1.28 2323.27 2317 9 2.69E-03 **** 1.64E+OO 0 1169.26 14 17 0. 96 2339.43 2331 14 4.05E-03 **** l.63E+OO 0 1256.53 11 14 0.65 2514.06 2507 10 3.07E-03 **** 1.54E+00 0 1281.19 13 11 1. 80 2563.42 2557 10 3.81E-03 **** l.51E+00 0 1322.81 5 3 1. 24 2646. 70 2643 6. 1. 39E-03 **** 1.47E+00 0 1353.65 7 0 0.73 2708.43 2705 6 1.94E-03 75.6 1.45E+OO 0 1356.56 8 0 0.73 2714. 25 2711 6 2.22E-03 70.7 1.44E+OO 0 1377.81 21 3 2.85 2756.78 2751 11 6.19E-03 51.2 1.42E+OO 0 1408.39 14 3 1. 93 2817.97 2813 11 4.17E-03 67.3 1.40E+00 T 0 1588.14 11 2 1. 87 3177.70 3173 9 3.30E-03 73.4 1. 2 6E+00 Flags: "T" = Tentatively associated Page 3442 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:02.50 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE. DATA * *
Configuration DKAlOO: *
Acquisition date 3-0CT-2016 08:58:40 Sensitivity : 3.000 *
Detector ID GAM24 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:02.00 Half life ratio : ***** *
Sample date .2-DEC-2015 10: 40: 00 Nuclide Library : SOLID *
Sample ID G405235023 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.4140E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis.* Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.917E-01 7.002E-01 2.152E+02 4.432E-02 2.565E-02 2.710E-02 2.644E-02 1.154E+OO 3.230E-01 3.839E-02 5.027E-02 4.876E-02 5.027E-02 4 .116E-01 5.027E-02 1.084E-01 1.084E-01 3.839E-02 4.030E-01 5.026E-02 3.310E-01 1.084E-01 4.435E-02 6. 551E-01 5.026E-02 1.455E-01 6.551E-01 2.997E-02 2.347E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3443 of 5809 Le (pCi/GRAM 1.0lOE+Ol NOT IDENT. 4.199E-02 NOT IDENT.

NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-5.6 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-14 6. ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 3444 of 5809

O.OOOE+OO 2 .114E-02 2. 041E-01 O.OOOE+OO O.OOOE+OO 5 .110E-02 3.677E-01 O.OOOE+OO 3.538E-02 3.437E-01 4.470E+OO 2.615E-02 l.448E-01 1.599E+OO 4.651E+OO O.OOOE+OO 1.632E-01 O.OOOE+OO O.OOOE+OO 5. 311E-01 6.214E+OO 6.993E-01 O.OOOE+OO l.830E-01 4.182E+02 2.547E-02 6.421E-01 1.880E+OO' 1.218E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.614E-02 4.784E-02 5.298E+00 3.506E-01 3.506E-01 2.386E-02 7.102E-02 l.857E-01 O.OOOE+OO O.OOOE+OO l.085E-01 2.228E+OO 8.342E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0. OOOE+OO' O.OOOE+OO O.OOOE+OO 2.709E-02 O.OOOE+OO 5.344E-02 9. 7 91E-02 O.OOOE+OO O.OOOE+OO 9.327E-02 O.OOOE+OO 0.000E+OO 2.243E+Ol O.OOOE+OO 2.755E-01 4.143E-02 3.610E:+oo 3.651E-02 O.OOOE+OO 6.282E+02 O.OOOE+OO l.993E-02 6. 966E-02 1.317E-01 1.014E-01 7.971E-02 1.715E+OO 4.228E-02 9.628E+OO SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. . SHORT HLIF SHORT HLIF* NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT I DENT .. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT.IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 . RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-231 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3445 of 5809 1.700E-01 7.084E-02 1. 771E-02 3.748E+OO 8.778E-01 l.607E+OO 3.168E+Ol 7.904E+Ol 3.754E-01 2.061E+OO 2.780E-02 3.777E-01 5.266E-01 2.907E-01 4.616E-01 1. 979E-01 l.979E-01 4.616E-01 1.738E-01 3.433E+OO 4.337E-02 O.OOOE+OO 1.829E-01 2,678E+02 6.973E-02 6.380E-02 5.431E-02 2.654E-02 3.070E-02 9.136E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL.ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:07.74 . *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 _ * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l * *Acquisition date 3-0CT-2016 08:58:40 Sensitivity : 3.000 *
Detector ID GAM24 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:02.00 Half life ratio : ***** *
Sample date 2-DEC-2015 10:40:00 Nuclide Library : SOLID *
Sample ID G405235023 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity l.4140E+02 GRAM *
Quantity Err ( % ) 1. 4144E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.243E+Ol l.492E+OO CD-109 2.086E+OO l.665E+OO TE-;-l25M l.095E+02 4.765E+02 SN-126 1. 317E-01 1. 049E-01 BA-137M 3.299E-01 l.007E-01 CS-137 3.486E-01 1.063E-01 TL-208 3.245E-01 7.848E-02 PB-210 l.026E+00 3.003E+00 BI-212 1.153E+OO 9. 596E-01 PB-212 l.091E+OO l.323E-01 BI-214 9.216E-01 2.0S4E-01 PB-214 1.193E+OO 1.884E-01 RN-222 9 ""216E-01 2.054E-01 RA-224 8.509E-01 l.506E+OO RA-226 9.216E-01 2.054E-01 AC-228 7.334E-01 3.009E-01 RA-228 7.334E-01 3.009E-01 TH-228 l.091E+OO 1.323E-01 TH-229 4.141E-01 4.436E-01 TH-230 9.213E-01 2.053E-01 PA-231 l.022E+00 6.106E-01 TH-232 7.334E-01 3.009E-01 PA-233 8.161E-02 1. 531E-01 TH-234 1. 267E+00 l.478E+OO u-234 9. 213E-01 2.053E-01 U-235 -7 .*143E-02 l.739E-01 U-238 l.267E+OO l.478E+OO AM-243 l.812E-01 8.708E-02 ANH-511 9. 971E-04 8.741E-02 Non-Identified Nuclides Nuclide BE-7 Page 3446 of 5809 Key-Line Activity (pCi/GRAM -4. 962E+OO K.L Act error ( 1. 96-sigma) 1.228E+Ol TPU ( 1. 96:....sigma) l.492E+OO l.665E+OO 4.765E+02 1.049E-01 l.007E-01 l.063E-01 7.848E-02 3.003E+OO 9. 596E-01 l.323E-01 2.054E-01 l.884E-01 2.054E-01 l.506E+00 2.054E-01 3.009E-01 3.009E-01 l.323E-01 4.436E-01 2.053E-01 6.106E-01 3.009E-01 1. 531E-01 1. 478E+00 2.053E-01 l.739E-01 l.478E+OO '8.708E-02 8.741E-02 TPU (1. 96-sigma) l.248E+Ol NOT IDENT.

NA-22 l.243E-02 5.037E-02 5.069E-02 NOT IDENT. NA-24 -1.000E+41 2.535E+41 0.000E+OO SHORT HLIF AL-26 7. OBlE-03 2.274E-02 2.296E-02 NOT IDENT. SC-46 -5.738E-01 3.740E-01 4.547E-01 FAIL ABUN V-48 -l.990E+03 l.642E+04 l.644E+04 SHORT HLIF CR-51 -3.344E+02 4 .120E+o2 4.387E+02 SHORT HLIF MN-54 -:-3.323E-02 6. 727E-02 6.892E-02 NOT IDENT. C0-56 7.905E-02 4.295E-01 4.310E-01 NOT IDENT. MN-56 1.000E+41 3.373E+41 O.OOOE+OO SHORT HLIF. C0-57 7.259E-03 4.035E-02 4.048E-02 NOT IDENT. C0-58 2.659E-01 3.648E-01 3.840E-01 NOT IDENT. FE-59 -5.545E+OO 6.265E+OO 6.745E+OO NOT IDENT. C0-60 7.350E-03 2.885E-02 2.904E-02 NOT IDENT. ZN-65 l.056E-01 l.650E-01 1. 717E-01 NOT IDENT. GE-68 -2.103E-01 l.881E+OO 1.884E+OO NOT IDENT. AS-73 3.431E+OO 5.023E+00 5.256E+OO NOT IDENT. AS-74 -2.915E+03 7 .111E+03 7.232E+03 SHORT HLIF SE-75 -9.210E-02 1.883E-01 l.928E-01 NOT IDENT. BR-77 l.163E+39 1. 027E+40 O.OOOE+OO SHORT HLIF SR-82 6.237E+02 7.804E+02 8.295E+02 SHORT HLIF RB-83 5.320E-02 6.082E-01 6.087E-01 NOT IDENT. KR-85 4.224E+OO 7.386E+OO 7.628E+OO NOT IDENT. SR-85 4.720E-01 8.317E-01 8.585E-01 NOT IDENT. RB-86 -3.932E+03 2.780E+04 2.786E+04 SHORT HLIF Y-88 2.103E-02 2.149E-01 2.152E-01 NOT IDENT. Y-91 2.930E+Ol 4. 811E+02 4.813E+02 NOT IDENT. NB-94 5.166E-03 2.952E-02 2. 961E-02 NOT IDENT. NB-95 -3.463E-01 9 .'431E-01 9.559E-01 NOT IDENT. NB-95M 2.295E+OO 2.295E+OO NOT IDENT. ZR-95 -5.707E-01 1.552E+OO 1. 573E+OO. NOT IDENT. NB-97 -1.000E+41 4.064E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 2.321E+41 O.OOOE+OO SHORT HLIF M0-99 -6.949Et32 6.450E+32 O.OOOE+OO SHORT HLIF TC-99M l .. 000E+41 3.406E+41 O.OOOE+OO SHORT HLIF RH-101 -l.290E-02 3.152E-02 3.205E-02 NOT IDENT. RH-102 2.lOOE-02 5.315E-02 5.399E-02 NOT IDENT. RU-103 -l .115E-01 6.133E+OO 6.133E+OO FAIL ABUN RH-106 -2. 431E-01 4.528E-01 4.659E-01 NOT IDENT. RU-106 -2. 431E-01 4.528E-01 4.659E-01 NOT IDENT. AG-108M 6.719E-03 2.650E-02 2.667E-02 NOT IDENT. AG-110M -5.599E-02 9.759E-02 1.008E-01 NOT IDENT. SN-113 2.579E-02 2.076E-01 2.079E-01 NOT IDENT. CD-115 8.801E+38 l.904E+40 O.OOOE+OO SHORT HLIF SN-117M 2.188E+04 1.177E+05 1.181E+05 SHORT HLIF TE-123M 5.449E-02 l.229E-01 l.254E-01 NOT IDENT. SB-124 1.875E+OO 2.190E+OO 2.348E+OO NOT IDENT. SB-125 2.521E-02 9.218E-02 9.288E-02 FAIL ABUN I-126 l.099E+06 1.492E+06 l.572E+06 SHORT HLIF SB-126 6.407E+05 1.472E+06 l.500E+06 SHORT HLIF SB-127 2.035E+21 6.564E+22 O.OOOE+OO SHORT HLIF I-131 -5.209E+08 7 .131E+09 7.135E+09 SHORT HLIF I-132 1.000E+41 1.897E+42 0.000E+OO SHORT HLIF TE-132 9.883E+26 l.339E+27 O.OOOE+OO SHORT HLIF BA-133 6.630E-03 3.279E-02 3.293E-02 NOT IDENT. I-133 -1.000E+41 2.336E+41 O.OOOE+OO SHORT HLIF CS-134 1.111E-01 6.548E-02 8.243E-02 FAIL ABUN CS-135 -l.159E-01 l.191E-01 1. 301E-01 NOT IDENT. I-135 l.000E+41 l.020E+42 O.OOOE+OO SHORT HLIF CS-136 *4 .103E+05 3.614E+05 4.060E+05 SHORT HLIF CE-139 2.532E-02 1. 081E-01 1.087E-01 NOT IDENT. BA-140 -8.149E+05 l.622E+06 l.663E+06 SHORT HLIF LA-140 2.849E+05 4.624E+05 4.799E+05 SHORT HLIF CE-141 7.869E+OO 2.563E+Ol 2.587E+Ol NOT IDENT. CE-143 l.000E+41 2.129E+41 O.OOOE+OO SHORT HLIF CE-144 -6.451E-02 3.266E-01 3.279E-01 NOT IDENT. PM-144 l.707E-03 4. 896E-02 4.897E-02 NOT IDENT. PR-144 1.488E-01 4.267E+OO 4.267E+OO NOT IDENT. PM-146 2.504E-02 3.883E-02 4.043E-02 NOT IDENT. ND-147 7.057E+06 4.673E+07 4.684E+07 SHORT HLIF PM-147 3.721E+02 6.952E+02 7.151E+02 NOT IDENT. PM-149 l.OOOE+41 2.219E+41 O.OOOE+OO SHORT HLIF EU-150 -8.459E-03 2.595E-02 2.622E-02 FAIL ABUN EU-152 -1.209E-02 8.335E-02 8.353E-02 FAIL ABUN GD-153 -l.662E-02 1.647E-01 1.649E-01 NOT IDENT. EU-154 2. 611E-02 l.224E-01 1.230E-01 FAIL ABUN EU-155 7.348E-02 8.549E-02 9.168E-02 FAIL ABUN TB-160 1.838E-01 2.302E+OO 2.304E+OO FAIL ABUN H0-166M -9.090E-03 5.179E-02 5.195E-02 FAIL ABUN Page 3447of5809 TM-171 1.848E+OO 1.052E+Ol 1.055E+Ol NOT IDENT. HF-172 2.587E-02 1. 951E-01 L 954E-01 FAIL ABUN LU-172 3.856E-02 7.603E-02 7.799E-02 FAIL ABUN LU-176 -7.838E-03 2.299E-02 2.326E-02 FAIL ABUN HF-181 -8.063E-01 4.424E+OO 4.439E+OO NOT IDENT. TA-182 9.328E-01 8.816E-01 9.768E-01 FAIL ABUN RE-183 5.395E-01 1. 749E+OO 1. 766E+OO NOT IDENT. RE-184 3.575E+Ol 3.352E+Ol 3.719E+Ol NOT IDENT. W-188 -1.181E+02 1.142E+02 1. 2 60E+02 FAIL ABUN IR-192 1.622E-01 4.427E-01 4.487E-01 FAIL ABUN HG-203 -1.083E-01 2.290E+OO 2.290E+OO FAIL ABUN BI-207 -3.287E-03 3.269E-02 3.273E-02 FAIL ABUN BI-211 3.287E+OO 5.218E-01 1. 571E+OO FAIL ABUN PB-211 3.499E-01 5.574E-01 5.793E-01 NOT IDENT. RN-219 -6.484E-02 3.378E-01 3.391E-01 NOT IDENT. RA-223 l.260E-01 5.034E-01 5.066E-01 FAIL ABUN AC-227 2.015E-01 2.030E-01 2.224E-01 FAIL ABUN TH-227 2.015E-01 2.030E-01 2.224E-01 FAIL ABUN TH-231 1.260E-01 5.034E-01 5.066E-01 FAIL ABUN PA-234 -l.091E-01 2.640E-01 2.685E-01 FAIL ABUN PA-234M 1.210E+OO 3.722E+OO 3.762E+OO NOT IDENT. NP-237 8 .161E-02 1. 531E-01 1.574E-01 FAIL ABUN NP-238 1.000E+41 5.725E+41 O.OOOE+OO SHORT HLIF NP-239 7.289E-02 2.052E-01 2.078E-01 NOT IDENT. PU-239 1.216E+02

3. 023E+02 3.073E+02 NOT IDENT. AM-241 -l.082E-02 8.488E-02 8.502E-02 NOT IDENT. CM-243 -1.628E-03 7.335E-02 7.336E-02 NOT IDENT. BK-247 -2.981E-02 6.287E-02 6.429E-02 FAIL ABUN CM-247 1. 744E-02 2.817E-02 2.925E-02 NOT IDENT. CF-249 3.766E-03 3.437E-02 3. 441E-02 NOT IDENT. CF-251 1. 701E-02 1.069E-01 l.072E-01 NOT IDENT. Page 3448 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 77.8223 87.09 87.6782 136.47 70.4387 45.60 76.2650 87.57 87.7463 140.51 0.0000 46.54 76.4388 88.03 87.8113 143.76 90.5337 49.72 0. 0000-88.34 87.8554 144.24 88.2910 51.35 83.2463 88.47 87.8737 145.44 78.0803 51.87 96.2426 89.96 88.0831 152.43 68.2890 52.39 84.4345 1093.63 88.1783 153.25 0.0000 52.97 78. 57 6.0 91.11 0.0000 323.87 69.5856 53.44 82.6403 92.59 88.4489 156.02 0.0000 54.07 87.7402 93.35 88.5530 158.56 0.0000 57.36 0.0000 94.56 88.7188 159.00 64.1250 57.53 86.3865 94.65 91.5938 162.33 73.7176 57.98 83.4515 94. 67 91. 5964 162.66 0.0000 59.27 92.7493 94.87 91.6244 163.33 76.1401 59.32 92.7591 97.43 91.9824 165.86 71.6473 59.54 92.8012 98.43 83.1249 176.31 68.8679 60. 96 98.44 83.1261 176.60 0.0000 61.17 86.3639 99.53 73.5299 177.52 66.5752 62. 93 102.5824 100 .11 76.8399 181.07 0.0000 63.29 102.6558 102.03 64.0339 181.52 77.9841 63.58 102.7151 103.18 68.4900 184.41 84.5928 64.28 102. 8571 103.37 63.0715 143.76 75.5133 66.73 124.1539 105.21 64.3300 193.51 57. 9697 67.24 140.6631 105.31 61.0676 197.03 59.3756 125.81 129.8470 106.12 61.1385 198.01 65.4953 67.75 125.7635 106.47 66.6303 201.83 69.3809 69.67 112.5006 109.28 77.4965 203.43 60.9512 70.83 141.6166 111. 00 84.6447 205.31 61.0565 72.81 104.8742 111. 76 0.0000 210.85 67.0921 72. 87 104.8858 114. 06 89.7849 215.65 59.1636 74.66 105.2252 116. 30 0.0000 222 .11 60.7401 74.82 105.2553 116.74 69.7993 227.09 62.2467 74.97 105. 2 83.2 . 119. 76 76.7543 227.38 62.2620 77 .11 105.6829 121.12 63.5192 228.16 0.0000 78.74 105.9836 121. 22 63.5275 228.18 41.1211 79.69 106.1568 121.78 63.5740 116.74 41.1211 80.12 106.2356 122.06 66.9447 235.69 57.6846 80.19 0.0000 122.92 71.4873 235. 96 57.6972 80.57 106.3168 123.07 71.5015 238.63 53.6354 81. 00 106.3949 265.00 71.5576 238.98 0.0000 81. 07 106.4073 125. 81. 69. 5116 240.99 53.7396 81. 75 79.8976 127.23 92.1005 242.00 53.7845 83.79 87.2039 127.91 94.4285 244.70 53.9030 84.00 87.2342 129.30 92.3413 252.40 0.0000 85.43 87.4404 131.20 99.3330 252.80 60.1886 86.55 87.6012 133. 02 82.5873 254.15 0.0000 86.79 87.6353 133.52 80.3744 .256.23 41.6518 86.94 87.6567 136.00 77.2118 260.90 0.0000 Page 3449 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 53.0492 355.39 0.0000 584.27 29.2097 264.80 53.0542 356.01 23.2386 595.83 0.0000 265.00 52.2072 364.49 0.0000 427.87 35.0902 268.22 57.4841 366.42 0.0000 602.52 0.0000 269.46 48.0908 372. 51 35.9023 604. 72 31.0156 270.03 38.6618 375.05 37.8010 607.14 21.7332 271.23 34.3970 377.52 26.7769 609.32 23.8254 273.65 0.0000 356.01 37. 9996 610.33 23.8348 276.40' 44.8906 388.16 35.3080 614.28 23.3551 277.37 47.5140 388.63 0.0000 618.01 22.8719 277.60 49. 2511 391.69 30. 7253 620. 36 16.6504 278.00 50.1293 264.66 31. 8204 621. 93 23.9499 279.20 48.4440 401.81 34.6514 630.19 0.0000 279.54 43.2648 402.40 22.4839 631.29 17.7706 279.70 43.2699. 404.85 24.3914 633.25 26.1536 -280.46 41. 5625 410.95. 32.0064 634.78 0.0000 283.69 39.9253 413. 71 33.9419 635.95 24.0875 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.0235 423.72 0.0000 645.85 17.8750 285.90 0.0000 427.09 37.9923 657.76 23.7708 287.50 34.8140 427.87 27.5563 657.90 0.0000 290.67 53.6498 433.94 31. 4605 661. 66 20.6331 293.27 0.0000 439.40 30. 5964 664.57 0.0000 351. 93 38.0714 453.88 23.1235 666:33 0.0000 295. 96 26.2695' 463.37 27 .1102 666.50 0.0000 879.38 18.4229 468.07 33.4843 667. 71 0.0000 299.98 27.6618 473.00 0.0000 677.62 19.1646 300.09 27.6638 475.06 17.5320 685.70 0.0000 300.13 27.6644 476.78 25.3462 695.00 0.0000 301.36 42.1924 .477.60 31. 2083 696.49 19.3037 302.85 35.6369 482.18 29.3250 696.51 19.3037 256.23 27.7496 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 27.8916 306.78 42.3516 497.08 29.5410 697.49 22.5295 308.46 37.1012 505.52 29.6625 702.65 21. 4982 311. 90 37.1884 507.63 0.0000 706.68 21.5308 316.51 31. 97 61 511. 00 32.7140 711. 68 18.3350 319.41 0.0000 514.00 28.2936 720.70 0.0000 320.08 0.0000 514.00 28.2936 721. 93 0.0000 321.04 35.6380 520.40 22.9027 722.78 14.6206 323.87 36.5982 520.69 0.0000 722. 91 14.6212 325.23 50.0334 522.65 0.0000 723.31 14.6234 328.76 0.0000 527.90 0.0000 724 .19 14.6277 333.37 4.8. 5057 528.26 20.9889 727.33 16.2720 333.97 47.1765 529.59 27.0022 733.00 17.9361 334.37 51.2330 529.87 0.0000 735.93 9.7939 338.28 39.6494 531. 02 0.0000 333.97 6.5330 338.32 39.6503 537.26 0.0000 739.50 0.0000 311. 90 35.1938 546.56 0.0000 747.24 13 .1118 340.48 35.1938 552.55* 23.2443 748.06 16.3947 340.55 0.0000 563.25 23.3566 752.31 19.7036 344.28 36.9078 569.33 30.5469 753.82 0.0000 345.93 28.0717 946.00 30.5493 756.73 24 .1198 351.06 31.7971 569.70 24.4414 756.80 24.1207 351. 93 31. 8142 583.19 24.5859. 884.68 16.4874 Page 3450 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:00:36.81 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM29.CNF;354 Background date : Z-OCT-2016 11:01:41. Sample date 8-DEC-2015 14:13:00. Acquisition date : 3-0CT-2016 08:59:12. Sample ID G405235024 Sample quantity 1.38962E+02 GRAM Detector name : GAM29 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.43 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 0 5 5 0 0 1 1 3 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 Page 3452 of 5809 Energy 63.35* 72. 24 74.74* 77.19* 87.06 90.00 92.91* 128.68 185.79* 208.71 210.22 238.69* 241.95 243.51 270.38 295.21* 300.42 327.86 338.30* 352.07* 438. 11 462. 81 471.19 480.06 511. 21
533.31 583.44* 603.29 609.37* 651. 41 66i. 67 727.72 795.15 799.26 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 17 48 139 219 68 53 111 41 90 53 26 404 88 24 36 178 35 50 92 256 13 36 4 69 33 19 115 8 209 23 296 35 26 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 148 66 152 150 170 73 170 175 180 79 78 91 107 93 83 93 51 89 42 98 38 62 32 128 64 27 56 38 63 15 49 9 9 4 0.70 1. 21 1. 22 1. 22 1.17 0.95 1.47 0.89 1. 44 1.16 1.16 1.14 1. 59 1. 44 1. 43 1. 30 2.04 2.44 0.88 1. 42 0.67 1. 93 0.53 7.12 1. 92 2.54 1. 43 0.64 1. 50 2.54 1. 48 0.97 2.04 2.04 126. 67 144.42 149.42 154.32 174.02 179.90 185.71 257.14 371. 21 417.00 420.00 476.89 483.39 486.50 540.20 589.79 600.19 655.01 675.88 703.39 875.32 924.67 941.41 959.14 1021. 39 1065.57 1165.76 1205.44 1217.59 1301.62 1322 .13 1454.18 1588.99 1597.21 124 143 143 143 172 178 178 253 366 413 413 472 472 472 536 582 596 650 673 697 872 918 939 944 1013 1059 1160 1199 1209 1298 1315 1449 1582 1582 7 4.76E-03126.2 23 1.32E-02 24.4 23 3.86E-02 17.6 23 6. 08E-02 11. 8 7 1.89E-02 34.1 13 1.48E-02 26.2 13 3.07E-02 24.5 9 1.15E-02 59. 6 13 2.51E-02 33.4 12 1. 48E-02 31. 5 12 7.31E-03 62.0 26 1.12E-01 6.3 26 2.45E-02 26.3 26 6.56E-03 88.0 9 1.00E-02 48.5 15 4.95E-02 14.1 8 9.85E-03 38.4 13 1.38E-02 41.6 7 2.56E-02 15.8 11 7.llE-02 9.8 8 3.61E-03 89.5 12 9.87E-03 47.7 6 1.22E-03210.9 34 1.91E-02 52.1 14 9.27E-03 62.0 11 5.24E-03 58.5 14 3.20E-02 17.2 9 2.23E-03143.5 18 5.80E-02 11.4 8 6.52E-03 35.6 14 8.22E-02 7.7 9 9.71E-03 22.9 19 7.19E-03 34.3 19 3.90E-03 38.4 Fit 2.62E+OO 9.81E-01 3.60E+OO 2.81E+OO 1.08E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235024 Acquisition date : 3-0CT-2016 08:59:12 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 835.84 12 17 2.48 1670.35 1664 10 3.41E-03 69.5 36 0 860.94 14 22 0.90 1720.54 1716 10 3.84E-03 69.5 37 0 911.32* 86 27 1.45 1821.29 1816 13 2.40E-02 16.6 38 0 933.01 12 16 1.37 1864.68 1859 9 3.19E-03 68.7 39 0 954.17 17 30 6.47 1907.01 1892 20 4.67E-03 83.5 40 0 965.07 26 13 1.94 1928.80 1924 9 7.14E-03 32.4 41 0 969.22* 51 19 1. 50 1937. 09 1933 12 1. 41E-02 22. 7 42 0 1000.45* 16 15 0.88 1999.57 1993
14 4.48E-03 57.5 43 0 1052.34 6 23 1. 50 2103. 36 2097 12 1. 63E-03163 .1 44 0 1093.39 13 11 2.16 2185.47 2179 12 3.66E-03 58.8 45 0 1120.44* 44 6 1.61 2239.59 2234 11 1.23E-02 19.2 46 0 1148. 58 9 13 0.92 2295.89 2288 10 2.61E-03 77.6 47 0 1151.13 11 13 1.35 2300.99 2298 8 3. 15E-03 61. 1 48 0 1300. 05 10 2 3.25 2598.97 2594 9 2.73E-03 42.0 49 0 1352.11 10 4 1.16 2703.17 2698 9 2.74E-03 49.8 50 0 1378.52* 9 12 0.88 2756.02 2747 16 2.59E-03 91.3 51 0 1425.60 16 0 4.00 2850.25 2845 11 4.44E-03 25.0 52 0 1460.87* 360 13 1.77 2920.86 2912 14 1.00E-01 5.7 53 0 1508.11 10 3 0.64 3015.41 3009 10 2.84E-03 42.9 54 0 1729.99 12 2 1. 93 3459. 68 3454 9 3.40E-03 35.6 55 0 1764.73* 37 0 1.36 3529.26 3524 10 1. 03E-02 18. I 56 0 1871. 53 6 0 0.99 3743.17 3739 7 1.67E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 3453 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:00:38 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 14:13:00 G405235024 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:59:12 138. 96 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA29 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3454 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 .74. 82 PB-212 74.82
BI-211 351.06 CAN 0 01:00:01.43 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460:82 10.66* 1.347E+OO 1.298E+Ol 1.298E+Ol 11. 35 OK MN-54 834.85 99.98* 2 .116E+OO 3.152E-02 6.135E-02 138. 96 OK CD-109 88.03 3.70* 6.255E+OO 7.744E-01 l.215E+OO 172. 03 OK SN-126 64.28 9.60 3.603E+OO 3.278E-01 3.278E-01 252.49 OK 86.94 8.90 6.255E+OO 3.219E-01 3.219E-01 172.03 OK 87.57 37.00* 6.255E+OO 7.744E-02 7.744E-02 172.03 OK CS-134 563.25 8.34 2.846E+OO Line Not Found Absent 569.33 15.37 2.823E+OO Line Not Found Absent 604. 72 97. 62 2.703E+OO 1.695E-02 2.231E-02 286.91 OK 795.86 85.46* 2.197E+OO 7.517E-02 9.896E-02 68.70 OK 801.95 8.69 2.183E+OO Line Not Found Absent 1365.19 3.02 1.430E+OO Line Not Found Absent BA-137M 661.66 89.90* 2.522E+OO 7.232E-01 7.370E-01 15.36 OK CS-137 661.66 85.10* 2.522E+OO 7.640E-01 7.785E-01 15.36 OK TL-208 277.37 6.60 4.914E+OO Line Not Found Absent 583.19 85.00* 2.772E+OO 2.734E-01 2.734E-01 34.39 OK 860.56 12.50 2.069E+OO 2.895E-01 2.895E-01 139.00 OK PB-212 74.82 10.28 5.094E+OO 1.050E+OO 1.050E+OO 60.99 OK ' 77 .11 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 OK 238.63 43.60* 5.495E+OO 1.013E+OO 1.013E+OO 12. 55. OK 300.09 3.30 4.622E+OO 1.373E+OO 1.373E+OO 76.89 OK BI-214 609.32 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 OK 1120.29 14.92 l.685E+OO 9.323E-01 9.326E-01 38;48 OK 1764.49 15.30 1.129E+OO l.090E+OO 1. 091E+OO 36.10 OK PB-214 74.82 5.80 5.103E+OO Line Not Found <<INT Reject 77 .11 9.70 5.365E+OO 2.745E+OO 2.746E+OO 23.57 OK 87.09 3.41 6.257E+OO Line Not Found <<INT Reject 242.00 7.25 5. 441E+OO Line Not Found <<INT Reject 295.22 18.42 4.685E+OO 1.219E+OO 1.220E+OO 28.25 OK 351. 93 35.60* 4.086E+OO 1.026E+OO 1.026E+OO 19.69 OK RN-222 609.32 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 OK 1120. 29 14.92 1.685E+OO 9.323E-01 38.48 OK 1764.49 15.30 1.129E+OO l.090E+OO 1.091E+OO 36.10 OK RA-224 240.99 4.10* 5. 441E+OO 2.178E-01 2.178E-01 638.47 OK RA-226 609.32 45.49* 2;683E+OO 9.538E-01 9.541E-01 22.80 OK 1120.29 14.92 1.685E+OO 9.326E-01 38.48 OK 1764.49 15.30 l.129E+OO 1.090E+OO 1. 091E+OO 36.10 OK AC-228 105.21 1.10 7.155E+OO Line Not Found Absent 338. 3'2 11. 27 4.215E+OO 1.134E+OO l.134E+OO 31. 65 OK 794.95 4.25 2.197E+OO 1.512E+OO 1.512E+OO 68.70 OK 835.71 1. 61 2 .116E+OO l.957E+OO 1.957E+OO 138. 96 OK 911. 20 25.80* 1. 981E+OO 9.123E-01 9.123E-01 33.21 OK 968. 97 15.80 1. 889E+OO 9.088E-01 9.088E-01 45.33 OK RA-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 OK 794.95 4.25 2.197E+OO 1.512E+OO 1.512E+OO 68.70 OK 835.71 1. 61 2 .116E+OO l.957E+OO 1.957E+OO 138. 96 OK 911.20 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 OK 968. 97 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 OK Page 3455 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 5.094E+OO 1.050E+OO 1.050E+OO 60.99 OK 77 .11 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 OK 238.63 43.60* 5.495E+OO 1.013E+OO 1.013E+OO 12.55 OK 300.09 3.30 4.622E+OO 1.373E+OO 1.373E+OO 76.89 OK TH-230 609.32 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 OK 1120.29 14.92 l.685E+OO 9.323E-01 9.323E-01 38.48 OK 1764.49 15.30 1.129E+OO 1.090E+OO 1.090E+OO 36.10 OK PA-231 283.69 1. 70 4. 831E+OO Line Not Found Absent 301.36 5.35* 4.622E+OO 8.467E-01 8.467E-01 76.89 OK TH-232 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.134E+00 1.134E+OO 31. 65 OK 835.71 1. 61 2 .116E+OO 1.957E+OO 1.957E+OO 138. 96 OK 911.20 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 OK 968. 97 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 OK TH-234 63.29 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 OK 92.59 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 OK U-234 609.32 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 OK 1120.29 14.92 1.685E+OO 9.323E-01 9.323E-01 38.48 OK 17 6'4. 4 9 15.30 l.129E+OO 1.090E+OO 1.090E+OO 36.10 OK U-235 89. 96 3.47 6.460E+00 1.538E+OO 1.538E+OO 52.32 OK 93.35 5.60 6.639E+OO 1.916E+OO 1.916E+OO 48.92 OK 143.76 10. 96* 7.247E+OO Line Not Found Absent 163.33 5.08 6.922E+00 Line Not Found Absent 185.72 57.20 6.480E+OO 1.493E-01 1.493E-01 66.77 OK 205.31 5.01 6.095E+OO Line Not Found Absent U-238 63.29 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 OK 92. 59 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 OK AM-243 43.53 5.90 7.707E-01 Line Not Found Absent 74.66 67.20* 5.094E+OO l.607E-01 1.607E-01 60.99 OK ANH-511 511. 00 100.00* 3.064E+OO 6.163E-02 6.163E-02 123. 96 OK Flag: "*" = Keyline Page 3456 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:39.74 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l * *Acquisition date 3-0CT-2016 08:59:12 Sensitivity 3.000 *
Detector ID GAM29 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.43 Half life ratio : ***** *
Sample date 8-DEC-2015 14:13:00 Analyst initials: MXRl * *Sample ID G405235024 Sample.Quantity l.3896E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr : 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO *. Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM K-40 l.298E+Ol l.444E+OO 6. 781E-01 MN-54 6.135E-02 8.355E-02 l.027E-01 CD-109 l.215E+OO 2.048E+OO 2. ll 7E+OO SN-126 7.744E-02 l.306E-01 l.356E-01 CS-134 9.896E-02 6.662E-02 7.303E-02 BA-137M 7.370E-01 l.109E-01 5.493E-02 CS-137 7.785E-01 l.172E-01 5.803E-02 TL-208 2.734E-01 9.212E-02 6.244E-02 PB-212 l.013E+OO l.246E-01 8.337E-02 BI-214 9.541E-01 2.132E-01 l.065E-01 PB-214 l.026E+OO l.980E-01 l.278E-01 RN-222 9.541E-01 2.132E-01 l.065E-01 RA-224 2.178E-01 l.363E+OO 8.935E-01 RA-226 9. 541E-01 2.132E-01 l.065E-01 AC-228 9.123E-01 2. 969E-01 2.203E-01 RA-228 9.123E-01 2.969E-01 2.203E-01 TH-228 l.013E+OO l.246E-01 8.337E-02 TH-230 9.538E-01 2 .132E-01 l.064E-01 PA-231 8.467E-01 6.380E-01 8.399E-01 TH-232 9.123E-01 2. 969E-01 2.203E-01 TH-234 8.506E-01 2.105E+OO l.985E+OO U-234 9.538E-01 2 .132E-01 1.064E-01 U-235 3.851E-02 l.724E-01 3.178E-01 U-238 8.506E-01 2.105E+OO l.985E+OO* AM-243 l.607E-01 9:604E-02 8.528E-02 ANH-511 6.163E-02 7.487E-02 5.255E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 9.431E+OO l.239E+Ol 2.423E+Ol NOT IDENT. 7.646E-03 3.797E-02 7.704E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 2.291E-02 2. 462E-02 6.743E-02 NOT IDENT. Page 3457 of 5809 SC-46 -2.693E-01 3.440E-01 5.743E-01 FAIL ABUN V-48 O.OOOE+OO 1.12 9E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.959E+02 O.OOOE+OO SHORT HLIF C0-56 -2.534E-01 3.559E-01 6.065E-01 NOT IDENT. MN-56 O.OOOE+OO l.395E+41 O.OOOE+OO SHORT HLIF C0-57 1.558E-02 4.338E-02 8.298E-02 NOT IDENT. C0-58 2.225E-01 5.020E-01 1. 047E+OO NOT IDENT. FE-59 2.115E+OO 4*. 555E+OO l.006E+Ol NOT IDENT. C0-60 1.120E-02 4.075E-02 8.128E-02 NOT IDENT. ZN-65 l.345E-01 1. 373E-01 3.0lOE-01 NOT IDENT. GE-68 -1.424E-02 2. 313E+OO 4.389E+OO NOT IDENT. AS-73 8.773E+OO 8.373E+OO 1. 723E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.409E+03 O.OOOE+OO SHORT HLIF SE-75 -8.318E-02 2.192E-01 3.769E-01 NOT IDENT. BR-77 O.OOOE+OO 2.210E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 4.547E+02 O.OOOE+OO SHORT HLIF RB-83 6.235E-01 5.286E-01 1.200E+OO NOT IDENT. KR-85 3.208E+OO 6.712E+OO 1. 2 61E+Ol NOT IDENT. SR-85 3.371E-01 7.086E-01 1.331E+OO NOT IDENT. RB-86 O.OOOE+OO 2. 726E+04 O.OOOE+OO SHORT HLIF Y-88 -4.574E-02 2.182E-01 4.409E-01 NOT IDENT. Y-91 -3.038E+02 4.663E+02 7.730E+02 NOT IDENT. NB-94 -l.188E-02 3.102E-02 5.650E-02 NOT IDENT. NB-95 -7.194E-01 7.903E-01 1.315E+OO NOT IDENT. NB-95M 1.462E+OO 2.276E+OO 4.075E+OO NOT IDENT. ZR-95 1. 729E+OO l.232E+OO 2.873E+OO NOT IDENT. NB-97 O.OOOE+OO 1.040E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.444E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 6.146E-02 7.180E-02 6.150E-02 FAIL ABUN RH-102 -2.658E-03 5.395E-02 1.045E-01 NOT IDENT. RU-103 -1.204E+OO 4.498E+OO 8.645E+OO FAIL ABUN RH-106 2. 714E-01 3.874E-01 8.462E-01 NOT IDENT. RU-106 2.714E-01 3.874E-01 8.462E-01 NOT IDENT. AG-108M 2.457E-03 2.876E-02 5 .137E-02 NOT IDENT. AG-llOM 8.045E-03 8.857E-02 1. 7 4 7E-01 NOT IDENT. SN-113 -5.652E-02 2.109E-01 4.040E-01 NOT IDENT. CD-115 O.OOOE+oo. 2.793E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.367E+04 O.OOOE+OO SHORT HLIF TE-123M 1.418E-02 l.339E-01 2.462E-01 NOT IDENT. SB-124 4.256E-01 1.338E+OO 3.388E+OO NOT IDENT. SB-125 -4.288E-03 1.*0 60E-01 2.054E-01 FAIL ABUN TE-125M -2.771E+02 2.477E+02 4.197E+02 NOT IDENT. I-126 O.OOOE+OO 8.877E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8. 696E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.022E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 5.128E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3. 771E+26 O.OOOE+OO SHORT HLIF BA-133 -6.492E-03 4.293E-02 7.464E-02 NOT IDENT. I-133 O.OOOE+OO 9.586E+40 O.OOOE+OO SHORT HLIF CS-135 -2.064E-02 1.533E-01 2.480E-01 NOT IDENT. I-135 O.OOOE+OO 1.675E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.467E+05 0.000E+OO SHORT HLIF CE-139 -8.108E-02 1.058E-01 1.805E-01 NOT IDENT. BA-140 O.OOOE+OO 1.274E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.585E+05 O.OOOE+OO SHORT HLIF CE-141 3.964E+OO 2.230E+Ol 4.161E+Ol NOT IDENT. CE-143 O.OOOE+OO 8.562E+40 O.OOOE+OO SHORT HLIF CE-144 *4.415E-03 3.617E-01 6.655E-01 NOT IDENT. PM-144 2.748E-02 5. 811E-02 l.165E-01 NOT IDENT. PR-144 2.387E+OO 5.048E+OO 1.012E+Ol NOT IDENT. PM-146 2.273E-02 4.257E-02 8.737E-02 NOT IDENT. ND-147 0.000E+OO 3.268E+07 O.OOOE+OO SHORT HLIF PM-147 -2.367E+02 7.745E+02 1.403E+03 NOT IDENT. PM-149 0.000E+OO 4.543E+40 O.OOOE+OO SHORT-HLIF EU-150 1. 741E-02 2.574E-02 4.919E-02 FAIL ABUN EU-152 -7.064E-02 8. 836E-02 1.612E-01 FAIL ABUN GD-153 6. 911E-03 1. 562E-01 2.942E-01 NOT IDENT. EU-154 l.656E-02 9.259E-02 l.872E-01 NOT IDENT. EU-155 1.163E-01 1.025E-Ol 2.067E-01 FAIL ABUN TB-160 -l.887E-03 1.843E+OO 3.530E+OO FAIL ABUN H0-166M -1.095E-02 4.703E-02 8.884E-02 FAIL ABUN TM-171 -6.546E+OO l.997E+Ol 3.758E+Ol NOT IDENT. HF-172 1.328E-01 2.274E-01 4 .114E-01 FAIL ABUN LU-172 8.750E-02 l.009E-01 l.382E-01 FAIL ABUN LU-176 1. 356E-02 2.450E-02 4.642E-02 FAIL ABUN Page 3458 of 5809 HF-181 -1.184E+OO 3. 796E+OO 6.425E+OO NOT IDENT. TA-182 -1.535E-01 8.0lOE-01 1.468E+OO FAIL ABUN RE-183 -1.494E-01 2.816E+OO 5.376E+OO NOT IDENT. RE-184 l.433E+Ol 2.680E+Ol 5.620E+Ol NOT IDENT. W-188 -4.208E+Ol l.163E+02 1.819E+02 FAIL ABUN IR-192 L 969E-01 5.028E-01 9.290E-01 FAIL ABUN HG-203 -l.693E+OO 2.470E+OO 4.085E+OO FAIL ABUN BI-207 -l.873E-02 5.148E-02 9 .119E-02 FAIL ABUN PB-210 -3.241E-01 3.128E+OO 6.038E+OO NOT IDENT. BI-211 O.OOOE+OO 5.453E-01 8.020E-01 FAIL ABUN PB-211 1.292E-01 6.637E-01 1.316E+OO NOT IDENT. BI-212 O.OOOE+OO 5.512E-01 l.133E+OO FAIL ABUN RN-219 -l.207E-01 3.592E-01 6.807E-01 FAIL ABUN RA-223 3. 231E-01 5.187E-01 l.008E+OO FAIL ABUN AC-227 -l.829E-01 2.270E-01 3. 725E-01 FAIL ABUN TH-227 -l.829E-01 2.270E-01 3. 725E-01 FAIL ABUN TH-229 3.173E-03 4.456E-01 8.095E-01 FAIL ABUN TH-231 3.231E-01 5.187E-01 1.008E+OO FAIL ABUN PA-233 -2.598E-02 6.275E-02 1.058E-01 FAIL ABUN PA-234 -1.214E-01 2.758E-01 4.254E-01 NOT IDENT. PA-234M 5.576E+OO 6.280E+OO 8.564E+OO FAIL ABUN NP-237 -2.598E-02 6.275E-02 l.058E-01 FAIL ABUN NP-238 O.OOOE+OO l.244E+41 0.000E+OO SHORT HLIF NP-239 4.189E-02 2.277E-01 4.292E-01 NOT IDENT. PU-239 5.574E+02 6.512E+02 6. 596E+02 FAIL ABUN AM-241 l.625E-02 1.317E-01 2.537E-01 NOT IDENT. CM-243 -6.249E-02 9.406E-02 1.667E-01 NOT IDENT.
BK-247 -8.779E-03 7.529E-02 l.332E-01 NOT'IDENT. CM-247 2.728E-02 3.317E-02 6.974E-02 NOT IDENT. CF-249 -9 .112E-03 3.637E-02 6.950E-02 NOT IDENT. CF-251 8.0SOE-03 1.058E-01 1.946E-01 NOT IDENT. Page 3459 of 5809 VAX/VMS Nuclide Identification *Report Generated 3-0CT-2016 10:00:37.59 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 345 10.66* 1. 347E+OO l.298E+Ol 1.298E+Ol 11. 35 MN-54 834.85 12 99.98* 2 .116E+OO 3.152E-02 6.135E-02 138. 96 CD-109 88.03 81 3.70* 6.255E+OO 1.898E+OO 2.978E+OO 68.17 SN-126 64.28 21 9.60 3.603E+OO 3.278E-01 3.278E-01 252.49 86.94 81 8.90 6.255E+OO 7.890E-01 7.890E-01 68.17 87.57 81 37.00* 6.255E+OO 1. 898E-01 1. 898E-01 68.17 CS-134 563.25 ------8.34 2.846E+OO ------Line Not Found ------569.33. ------15.37 2.823E+OO ------Line Not Found ------604.72 8 97. 62 2.703E+OO l.695E-02 2. 231E-02 286.91 795.86 26 85.46* 2.197E+OO 7.517E-02 9. 896E-02 68.70 801.95 ------8.69 2.183E+OO ------Line Not Found ------1365.19 ------3.02 1.430E+OO ------Line Not Found ------BA-137M 661. 66 303 89.90* 2.522E+OO 7.232E-01 7.370E-01 15.36 CS-137 661. 66 303 85.10* 2.522E+00 7.640E-01 7.785E-01 15.36 TL-208 277.37 ------6.60 4.914E+00 ------Lihe Not Found ------583.19 '119 85.00* 2.772E+OO 2.734E-01 2.734E-01 34.39 860.56 14 12.50 2.069E+OO 2.895E-01 2.895E-01 139.00 BI-211 72.87 58 1. 23 4.798E+00 5.284E+00 5.284E+OO 48.75 351. 06 276 12.92* 4.086E+OO . 2.826E+OO 2.826E+OO 19.69 PB-212 74.82 168 10.28 5.094E+OO 1.738E+OO l.738E+00 35.12 77 .11 264 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 238.63 449 43.60* 5.495E+OO 1.013E+OO 1.013E+OO 12.55 300.09 39 3.30 4.622E+OO 1.373E+OO l.373E+OO 76.89 BI-214 609.32 215 45.49* 2.683E+OO 9.538E-01 9. 541E-01 22.80 1120. 29 43 14 :92 . 1.685E+OO 9.323E-01 9.326E-01 38.48 1764.49 35 15.30 l.129E+OO 1.090E+OO 1. 091E+OO 36.10 PB--,214 74.82 168 5.80 5.094E+00 3.081E+00 3.082E+OO 35.12 77 .11 264 9.70 5.365E+00 2.745E+OO 2.746E+OO 23.57 87.09 81 3.41 6.255E+OO 2.059E+OO 2.060E+OO 68.17 242.00 98 7.25 5.441E+OO 1.342E+OO 1.343E+OO 52.67 295.22 195 18.42 4.685E+OO l.219E+OO 1.220E+OO 28. 25. 351. 93 276 35.60* 4.086E+OO 1.026E+OO 1. 026E+OO 19.69 RN-222 609.32 215 45.49* 2.683E+00 9.538E-01 9.541E-01 22.80 1120.29 43 14.92 1.685E+OO 9.323E-01 9.326E-01 38.48 1764.49 35 15.30 l.129E+OO 1.090E+OO 1. 091E+OO 36.10 RA-224 240.99 98 4.10* 5.441E+OO 2 .. 374E+OO 2.374E+OO 52.67 RA-22 6 609.32 215 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 1120.29 43 14.92 1.685E+OO 9.323E-01 9.326E-01 38.48 1764.49 35 15.30 l.129E+OO l.090E+00 1.091E+OO 36.10 AC-228 105.21 ------1.10 7.155E+00 ------Line Not Found ------338.32 100 11. 27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 794.95 26 4.25 2.197E+OO 1.512E+OO l.512E+00 68.70 835. 71 12 1. 61 2 .116E+OO 1.957E+OO 1. 957E+001 138.96 911. 20 86 25.80* 1. 9.81E+OO 9.123E-01 9.123E-01 33.21 968. 97 50 15.80 l.889E+OO 9.088E-01 9.088E-01 45.33 RA-228 105.21 ------1.10 7.155E+00 ------Line Not Found ------338.32 100 11. 27 4.215E+OO 1.134E+00 1.134E+OO 31. 65 Page 3460 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235024 Acquisition da.te 3-0CT-2016 08:59:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 26 4.25 2.197E+OO l.512E+OO 1.512E+OO 68. 7*0 835.71 12 1. 61 2 .116E+OO 1.957E+OO l.957E+OO 138.96 911. 20 86 25.80* 1. 981E+OO 9.123E-01 9.123E-01 33.21 968. 97 50 15.80 l.889E+OO 9.088E-01 9.088E-01 45.33 TH-228 74.82 168 10.28 5.094E+OO 1. 738E+OO l.738E+OO 35.12 77 .11 264 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 238.63 449 43.60* 5.495E+OO 1.013E+OO 1.013E+OO 12.55 300.09 39 3.30 4.622E+OO 1.373E+OO 1.373E+OO 76. 89 TH-230 609.32 215 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 1120.29 43 14.92 l.685E+OO 9.323E-01 9.323E-01 38.48 1764.49 35 15.30 1.129E+OO 1.090E+OO 1.090E+OO 36 .10 PA-231 283.69 ------1. 70 4. 831E+OO ------Line Not Found ------301.36 39 5.35* 4.622E+OO 8.467E-01 8.467E-01 76. 89 TH-232 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 ;LOO 11. 27 4.215E+OO l.134E+OO l.134E+OO 31. 65 835.71 12 1. 61 2 .116E+OO 1.957E+OO 1.957E+OO 138. 96 911.20 86 25.80* 1. 981E+OO 9.123E-01 9.123E-01 33.21 968. 97 50 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 TH--,234 63.29 21 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 92.59 132 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 U-234 609.32 215 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 1120.29 43 14 .. 92 1.685E+OO 9.323E-01 9.323E-01 38.48 1764.49 35 15.30 l.129E+OO l.090E+OO l.090E+OO 36 .10 U-235 89. 96 64 3.47 6.460E+OO 1.538E+OO 1.538E+OO 52 ."32 93.35 132 5.60 6.639E+OO 1.916E+OO 1.916E+OO 48.92 143.76 ------10. 96* 7.247E+OO ------Line Not Found ------163.33 ------5.08 6.922E+OO ------Line Not Found ------185. 72 102 57.20 6.480E+OO* 1.493E-01 1.493E-01 66.77 205.31 ------5.01 6.095E+OO ------Line Not Found ------U-238 63.29 21 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 92.59 132 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 AM-243 43.53 ------5.90 7.707E-01 ------Line Not Found ------74.66 168 67.20* 5.094E+OO 2.659E-01 2.659E-01 35.12 ANH-511 511. 00 35 100.00* 3.064E+OO 6.163E-02 6.163E-02 123. 96 Flag: "*" Key line Page 3461of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Total number of lines in spectrum 56 Number of unidentified lines 16 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 MN-54 CD-109 SN-126 CS-134 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226. AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243
ANH-511 Hlife l.25E+09Y 312.05D 461. 40D 2.30E+05Y 2.07Y 30.08Y 30.08Y l.41E+10Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+l0Y 1. 41E+10Y 1.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 95 1. 57 1. 00 1. 32 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1 .. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.298E+Ol 3.152E-02 l.898E+OO l.898E-01 7.517E-02 7.232E-01 7.640E-01 2.734E-01 2.826E+OO 1. 013E+OO 9.538E-01 1.026E+OO 9.538E-01 2.374E+OO 9.538E-01 9.123E-01 9.123E-01 1.013E+OO 9.538E-01 8.467E-01 9.123E-01 8.506E-01* 9.538E-01 1.493E-01 8.506E-01 2.659E-01 6.163E-02 3. 572E+Ol 3. 572E+Ol Decay Corr pCi/GRAM 1.298E+Ol 6.135E-02 2.978E+OO l.898E-01 9.896E-02 7.370E-01 7.785E-01 2.734E-01 2.826E+OO 1.013E+OO 9.541E-01 1. 026E+00 9.541E-01 2.374E+OO 9. 541E-01 9 .123E-01' 9.123E-01 1. 013E+OO 9.538E-01 8.467E-01 9.123E-01 8.506E-01 9.538E-01 1.493E-01 8.506E-01 2.659E-01 6.163E-02 3.689E+Ol 3.689E+Ol 71. 43% De*cay Corr 2-Sigma Error 0.147E+Ol 8.525E-02 2.030E+OO 1. 2 94E-01 6.798E-02 l.132E-01 l .196E-01 0.940E-01 0.556E+OO 0.127E+OO 2.176E-01 0.202E+OO 2.176E-01 1.250E+OO 2 .*17 6E-01 3.029E-01 3.029E-01 0.127E+OO 2.175E-01 6.510E-01 3.029E-01 21. 48E-01 2.175E-01 0.997E-01 21.48E-01 0.934E-01 7.640E-02 "M" Manually accepted 2-Sigma %Error 11. 35 138.96 68.17 68.17 68.70 15.36 15.36 34.39 19.69 12.55 22.80 19.69 22.80 52.67 22.80 33.21 33.21 12.55 22.80 76.89 33.21 252.49 22.80 66.77 252.49 35.12 123. 96 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3462 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235024 Acquisition date : 3-0CT-2016 08:59:12 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 128.68 48 203 0.89 257.14 253 9 1.15E-02 **** 7.39E+00 T 1 208.71 60 89 1.16 417.00 413 12 l.48E-02 63.0 6.03E+OO 1 210.22 30 87 1.16 420.00 413 12 7. 31E-03 **** 6.00E+OO T 3 243.51 26 103 1. 44 486.50 472 26 6.56E-03 **** 5.42E+00 T 0 270.38 40 91 1. 43 540.20 536 9 1. OOE-02 97.0 5. OlE+OO T 0 327.86 54 97 2.44 655.01 650 13 l.38E-02 83.2 4.32E+00 T 0 438 .11 14 40 0.67 875.32 872 8 3.61E-03 **** 3.45E+OO T 0 462.81 38 66 1. 93 924.67 918 12 9.87E-03 95.3 3. 31E+OO T 0 471.19 5 33 0.53 941.41 939 6 l.22E-03 **** 3.26E+OO 0 480.06 72 135 7.12 959.14 944 34 1. 91E-02 **** 3.21E+OO 0 533.31 20 28 2.54 1065.57 1059 11 5.24E-03 **** 2.97E+OO 0 651.41 24 15 2.54 1301.62 1298 8 6.52E-03 71. 3 2.55E+OO 0 727. 72 36 9 0.97 1454.18 1449 9 9.71E-03 45.9 2.35E+OO T 3 799.26 14 4 2.04 1597.21 1582 19 3.90E-03 76. 7 2.19E+OO 0 933.01 11 15 1. 37 1864.68 1859 9 3.19E-03 **** 1. 95E+OO 0 954.17 17 30 6.47 1907.01 1892 20 4.67E-03 **** 1. 91E+OO *T 0 965. 07 26 13 1. 94 1928.80 1924 9 7.14E-03 64.8 1. 90E+OO T 0 1000.45 16 15 0.88 1999.57 1993 14 4.48E-03 **** 1. 84E+OO T 0 1052.34 6 23 1. 50 2103.36 2097 12 1. 63E-03 **** l.77E+00 0 1093.39 13 11 2.16 2185.47 2179 12 3.66E-03 **** 1.72E+OO T 0 1148.58 9 12 0.92 2295.89 2288 10 2. 61E-03 **** 1.65E+OO T 0 1151.13 11 12 1:35 2300.99 2298 8 3.15E:-03 **** 1. 65E+OO 0 1300. 05 10 2 3.25 2598.97 2594 9 2.73E-03 84.0 1.49E+00 0 1352 .11 10 4 1.16 2703.17 2698 9 2.74E-03 99.7 1.44E+OO 0 1378.52' 9 11 0.88 2756.02 2747 16 2.59E-03 **** 1.42E+OO 0 1425.60 15 0 4.00 2850.25 2845 11 4. 44E...:.03 50.0 1. 38E+00 0 1508 .11 10 3 *0.64 3015.41 3009 10 2.84E_.:03 85.8 1.31E+OO 0 1729.99 12 2 1. 93 3459.68 3454 9 3.40E-03 71. 3 l.15E+00 0 1871.53 6 0 0.99 3743.17 3739 7 l.67E-03 81. 6 1.06E+OO Flags: "T" = Tentatively associated / Page 3463 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:51.61 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration. DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l *
Acquisition date 3-0CT-2016 08:59:12 Sensitivity : 3.000 *
Detector ID GAM29 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.43 Half life ratio : ***** *
Sample date 8-DEC-2015 14:13:00 Nuclide Library : SOLID *
Sample ID G405235024 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.3896E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 CD-109 SN-126 CS-134 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.881E-01 4.454E-02 l.007E+OO 6.452E-02 3.132E-02 2.412E-02 2.548E-02 2.806E-02 3.853E-02 4. 714E-02 5.875E-02 4.714E-02 4.129E-01 4.714E-02 9.568E-02 9.568E-02 3.853E-02 4.712E-02 3.894E-01 9.568E-02 9.342E-01 4. 712E-02 1.493E-01 9.342E-01 4.039E-02 2.384E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3464 of 5809 Le (pCi/GRAM l.101E+Ol 3.249E-02 O.OOOE+OO 2.707E-02 2.434E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3465 of 5809 O.OOOE+OO O.OOOE+OO 2. 511E-01 O.OOOE+OO 3.889E-02 4.590E-01 4.218E+OO 3.504E-02 l.303E-01 1. 911E+OO 8.142E+OO O.OOOE+OO 1. 742E-01 O.OOOE+OO O.OOOE+OO 5.388E-01 5.708E+OO 6.025E-01 O.OOOE+OO 1. 729E-01 3.244E+02 2.517E-02 5.733E-01 1. 8.96E+OO l.283E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.895E-02 4.632E-02 3.800E+OO 3.735E-01 3.735E-01 2.330E-02 7.581E-02 1.833E-01 O.OOOE+OO O.OOOE+OO l.157E-01 l.282E+OO 9.389E-02 1.952E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.417E-02 O.OOOE+OO l.147E-01 O.OOOE+OO O.OOOE+OO 8.398E-02 O.OOOE+OO O.OOOE+OO 1.950E+Ol O.OOOE+OO 3.134E-01 5.283E-02 4.589E+OO 3.988E-02 O.OOOE+OO 6.563E+02 O.OOOE+OO 2.273E-02 7.354E-02 1. 380E-Ol 7.882E-02 9.764E-02 1.551E+OO 3.867E-02 1. 7 66E+Ol 1.933E-01 5.989E-02 2.144E-02 2.822E+OO SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT-HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT .. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247. CF-'-249 *, CF-251 Page 3466 of 5809 6.275E-01 2. 531E+OO 2.466E+Ol 8.316E+Ol 4.303E-01 l.879E+OO 3.988E-02 2.854E+OO 3:869E-01 6.039E-01 5.190E-01 3.095E-01 4.607E-01 1. 710E-01 1. 710E-01 3.776E-01 4.607E-01 4.856E-02 1.807E-01 3.806E+OO 4.856E-02 O.OOOE+OO 2.015E-01 3.134E+02 1.197E-01 7.807E-02 6.165E-02 3'. 205E-02 3.175E-02 9.068E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:56.72 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND* SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l * *Acquisition date 3-0CT-2016 08:59:12 Sensitivity : 3.000 *
Detector ID GAM29 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.43 Half life ratio : ***** *
Sample date 8-DEC-2015 14:13:00 Nuclide Library : SOLID *
Sample ID G405235024 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.3896E+02 GRAM *
Quantity Err(%) : l.4392E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 25-JUN-2016 09: 55: 57 Eff .. Geometry : CAN
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO *
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40. 1.298E+Ol 1.596E+OO MN-54 6.135E-02 8.359E-02 CD-109 1.215E+OO 2.062E+OO SN-126 7.744E-02 1.314E-01 CS-134 9. 896E-02 6.675E-02 BA-137M 7.370E-01 1.154E-01 CS-137 7.785E-01 1.219E-01 TL-208 2.734E-01 9. 28.5E-02 PB-212 1.013E+OO 1. 356E-01 BI-214 9.541E-01 2 .171E-01 PB-214 1.026E+OO 2.025E-01 RN-222 9.541E-01 2. l 71E-01 RA-224 2.178E-01 1.370E+OO RA-226 9.541E-01 2. l 71E-01 AC-228 9.123E-01 3.006E-01 RA-228 9.123E-01 3.006E-01 TH-228 1.013E+OO 1.356E-01 TH-230 9.538E-01 2.171E-01 PA-231 8.467E-01 6.631E-01 TH-232 9.123E-01 3.006E-01 TH-234 8.506E-01 2 .113E+OO U-234 9.538E-01 2.171E-01 U-235 3.851E-02 1.724E-01 U-238 8.506E-01 2 .113E+OO AM-243 1.607E-01 9.746E-02 ANH-511 6.163E-02 7.491E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3467 of 5809 Key-Line Activity (pCi/GRAM 9.431E+OO 7.646E-03 l.OOOE+41 2.291E-02 K.L Act error ( 1. 96-sigma) 1.240E+Ol 3.797E-02 4.382E+41 2.466E-02 TPU ( 1. 96-sigma) 1. 596E+OO 8.359E-02 2.062E+OO l.314E-01 6.675E-02 l.154E-01 1.219E-Ol 9.285E-02 1. 356E-01 2.171E-01 2.025E-01 2.171E-01 1.370E+OO 2.171E-01 3.006E-01 3.006E-01 l.356E-01 2.171E-01 6.631E-01 3.006E-01 2 .113E+OO 2.171E-01 1.724E-01 2 .113E+OO 9.746E-02 7.491E-02 TPU ( 1. 96-sigma) 1.310E+Ol 3.813E-02 O.OOOE+OO 2.674E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -2.693E-01 3.442E-01 3.650E-01 FAIL ABUN V-48 -9.055E+03 1.129E+04 l.201E+04 SHORT HLIF CR-51 -3.470E+02 3. 961E+02 4.259E+02 SHORT HLIF C0-56 -2.534E-01 3.561E-01 3.739E-01 NOT IDENT. MN-56 -l.000E+41 1.396E+41 O.OOOE+OO SHORT HLIF C0-57 l.558E-02 4.339E-02 4.395E-02 NOT IDENT. C0-58 2.225E-01 5.021E-01 5.120E-01 NOT IDENT. FE-59 2 .115E+OO 4.558E+OO 4.657E+OO NOT IDENT. C0-60 1.120E-02 4.076E-02 4.107E-02 NOT IDENT. ZN-65 1.345E-01 l.374E-01 1.501E-01 NOT IDENT. GE-68 -l.424E-02 2.313E+OO 2.313E+OO NOT IDENT. AS-73 8.773E+OO 8.566E+00 9.434E+OO NOT IDENT. AS-74 -3.451E+03 5.416E+03 5.635E+03 SHORT HLIF SE-75 -8.318E-02 2.192E-01 2.224E-01 NOT IDENT. BR-77 1. 798E+38 l.556E+39 O.OOOE+OO SHORT HLIF SR-82 -2. 26'6E+Ol 4.547E+02 4.548E+02 SHORT HLIF RB-83 6.235E-01 5.355E-01 6.047E-01 NOT IDENT. KR-85 3.208E+OO 6. 713E+OO 6.867E+00 NOT IDENT. SR-85 3.371E-01 7.088E-01 7.249E-01 NOT IDENT. RB-86 -3.282E+03 2.726E+04 2.730E+04 SHORT HLIF Y-88 -4.574E-02 2.182E-01 2.192E-01 NOT IDENT. Y-91 -3.038E+02 4.664E+02 4. 861E+02 NOT IDENT. NB-94 -1.188E-02 3.103E-02 3.149E-02 NOT IDENT. NB-95 -7.194E-01 7.909E-01 8.548E-01 NOT IDEN.T. NB-95M 1.462E+OO 2.279E+OO 2. 372E+OO NOT IDENT. ZR-95 1. 729E+OO 1.235E+OO 1.460E+OO NOT IDENT. NB:.._97 -1.000E+41 l.041E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 2.148E+41 O.OOOE+OO SHORT HLIF M0-99 -3.130E+31 l.445E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.986E+41 O.OOOE+OO SHORT HLIF RH-101 6.146E-02 7.266E-02 7.776E-02 FAIL ABUN RH-102 -2.658E-03 5.395E-02 5.397E-02 NOT IDENT. RU-103 -1.204E+00 4.498E+OO 4. 531E+OO FAIL ABUN RH-106 2.714E-01 3.877E-01 4.066E-01 NOT IDENT. RU-106 2.714E-01 3.877E-01 4.066E-01 NOT IDENT. AG-108M 2.457E-03 2.876E-02 2.878E-02 NOT IDENT. AG-llOM 8.045E-03 8.857E-02 8.865E-02 NOT IDENT. SN-113 -5.652E-02 2.109E-01 2.125E-01 NOT IDENT. CD-115 1.278E+38 2.793E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 2.248E+04 9.371E+04 9.426E+04 SHORT HLIF TE-123M l.418E-02 l.339E-01 1.340E-01 NOT IDENT. SB-124 4.256E-01 1.338E+OO l.352E+OO NOT IDENT. SB-125 -4.288E-03 1.060E-01 1.060E-01 FAIL ABUN TE-125M -2. 771E+02 2.482E+02 2.779E+02 NO':r IDENT. I-126 -9.604E+04 8.878E+05 8.889E+05 SHORT HLIF SB-126 6.220E+04 8.697E+05 8.701E+05 SHORT HLIF SB-127 -1.280E+22 2.680E+22 O.OOOE+OO SHORT HLIF I-131 6.239E+09 5 .136E+09 5.855E+09 SHORT HLIF I-132 1.000E+41 l.898E+42 O.OOOE+OO SHORT HLIF TE-132 l.837E+26 3.844E+26 O.OOOE+OO SHORT HLIF BA-133 -6.492E-03 4.293E-02 4.303E-02 NOT IDENT. I-133* -l.000E+41 2.047E+41 O.OOOE+OO SHORT HLIF CS-135 -2.064E-02 1.533E-01 l.536E-01 NOT IDENT. I-135 1.000E+41 6.978E+41 O.OOOE+OO SHORT HLIF CS-136 2.233E+05 2.479E+05 2.676E+05 SHORT HLIF CE-139 -8.108E-02 1. 071E-01 l.132E-01 NOT IDENT. BA-140 2.003E+05 1.274E+06 l.277E+06 SHORT HLIF LA-140 3.376E+04 3.585E+05 3.589E+05 SHORT HLIF CE-141 3. 964E+OO 2.230E+Ol 2.237E+Ol NOT IDENT. CE-143 1.000E+41 8.622E+40 O.OOOE+OO SHORT HLIF CE-144 4.415E-03 3.617E-01 3.617E-01 NOT IDENT. PM-144 2.748E-02 5. 813E-02 5.944E-02 NOT IDENT. PR-144 2.387E+OO 5.049E+OO 5.162E+OO NOT IDENT. PM-146 2.273E-02 4.260E-02* 4.381E-02 NOT IDENT. ND-147 6.708E+06 3.269E+07 3.282E+07 SHORT HLIF PM-147 -2.367E+02 7.746E+02 7.819E+02 NOT IDENT. PM-149 -4.743E+40 4.661E+40 O.OOOE+OO SHORT HLIF EU-150 1. 741E-02 2.575E-02 2.692E-02 FAIL ABUN EU-152 -7.064E-02 8.845E-02 9*. 401E-02 FAIL ABUN GD-153 6. 911E-03 1.562E-01 1.562E-01 NOT IDENT. EU-154 1.656E-02 9.259E-02 9.289E-02 NOT IDENT. EU-155 l.163E-01 1. 029E-01 1.155E-01 FAIL ABUN TB-160 -1. 887E-03 1.843E+OO l.843E+OO FAIL ABUN H0-166M -1.095E-02 4.704E-02 4.729E-02 FAIL ABUN TM-171 -6.546E+OO 1.998E+Ol 2.020E+Ol NOT IDENT. HF-172 1.328E-01 2.284E-01 2.361E-01 FAIL ABUN LU-172 8.750E-02 1.013E-01 1.087E-01 FAIL ABUN LU-176 l.356E-02 2.450E-02 2.525E-02 FAIL ABUN Page 3468 of 5809 HF-181 -1.184E+OO 3.796E+OO 3.834E+OO NOT IDENT. TA-182 -1.535E-01 8.0lOE-01 8.040E-01 FAIL ABUN RE-183 -1.494E-01 2.816E+OO 2.817E+OO NOT IDENT. RE-184 1.433E+Ol 2. 701E+Ol 2.778E+Ol NOT IDENT. W-188 -4.208E+Ol l.164E+02 l.180E+02 FAIL ABUN IR-192 1. 969E-01 5.029E-01 5.106E-01 FAIL ABUN HG-203 -1.693E+OO 2.471E+OO 2.586E+OO FAIL ABUN BI-207 -1. 873E-02 5.149E-02 5.218E-02 FAIL ABUN PB-210 -3.241E-01 3.128E+OO 3 .131E+OO-NOT IDENT. BI-211 2.826E+OO 5.597E-01 1.392E+OO FAIL ABUN PB-211 1.292E-01 6.637E-01 6.662E-01 NOT IDENT. BI-212 1.226E+OO 5.547E-01 7. 831E-01 FAIL ABUN RN-219 -1.207E-01 3.595E-01 3.636E-01 FAIL ABUN RA-223 3.231E-01 5.190E-01 5.391E-01 FAIL ABUN AC-227 -1.829E-01 2.282E-01 2.427E-01 FAIL ABUN TH-227 -1.829E-01 2.282E-01 2.427E-01 FAIL ABUN TH-229 3.173E-03 4.456E-01 4.456E-01 FAIL ABUN TH-231 3.231E-01 5.190E-01 5.391E-01 FAIL ABUN PA-233 -2.598E-02 6.276E-02 6.384E-02 FAIL ABUN PA-234 -l.214E-01 3.088E-01 3.136E-01 NOT IDENT. PA-234M 5.576E+OO 6.285E+OO 6.769E+OO FAIL ABUN NP-237 -2.598E-02 6.276E-02 6.384E-02 FAIL ABUN NP-238 -l.000E+41 1.245E+41 O.OOOE+OO SHORT HLIF NP-239 4.189E-02 2.277E-01 2.285E-01 NOT IDENT. PU-239 5.574E+02 6.517E+02 6.985E+02 FAIL' ABUN AM-241 l.625E-02 l.318E-01 l.320E-01 NOT IDENT. CM-243 -6.249E-02 9.424E-02 9.836E-02 NOT IDENT. BK-247 -8. 77 9E-03. 7. 531E-02 7.542E-02 NOT IDENT'. CM-247 2.728E-02 3.349E-02 3.567E-02 NOT IDENT. CF-249 -9 .112E-03 3.637E-02 3.661E-02 NOT IDENT. CF-251 8.050E-03 l.058E-01 1.058E-01 NOT IDENT. Page 3469 of 5809

GEL Laboratories LLC *
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Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 93.1266 87.09 126.8845 136.47 79.2768 45.60 75.3984 87.57 126.9696 140.51 0.0000 46.54 85.1069 88.03 127.0510 143. 7 6 66.7467 49. 72 0.0000 88.34 53.3025 144.24 72.2530 51. 35 99.4402 88.47 53.3120 145.44 70.1484 51. 87 94.7076 89,. 96 95.8847 152.43 84.9860 52.39 88.9976 1093.63 78.1500 153.25 0.0000 52.97 81.3484 91.11 0.0000 323.87 59.7044 53.44 71.7276 92.59 78.3567 156.02 0.0000 54.07 78.6056 93.35 78.4365 158.56 0.0000 57.36 0.0000 94.56 70.2936 159.00 78.8631 57.53 86.9195 94.65 70.3019 162.33 76.8838 57.98 87. 9672 94.67 70.3040 162.66 0.0000 59.27 96.0067 94.87 67.5644 163.33 69.1483 59.32 91.1165 97.43 74.7098 165.86 78.2555 59.54 91.1520 98.43 78.9630 176.31 59.8159 60. 96 90.3965 98.44 78.9641 176.60 0.0000 61.17 90.4295 99.53 80 .1153 177.52 61. 0096 62.93 85.7740 100 .11 83.2990 181.07 0.0000 63.29 85.8270 102.03 84.5466 181.52 58.9570 63.58 85.8691 103.18 76.3071 184.41 65.9253 64.28 77.7359 103.37 89.9171 143.76 65. 9996 66.73 88.6375 105.21 67.0693 193.51 64.1467 67.24 104.6004 105.31 68.1257 197.03 75.8241 125.81 99.3759 106.12 82.8815 198.01 79.3348 67.75 99.3866 106.47 78.7193 201.83 70.3563 69.67 94.3792 109.28 86.3624 203.43 63.5182 70.83 117.1937 111. 00 81.2650 205.31 50.8918 72.81 106.2046 111.76 0.0000 210.85 55.7644 72.87 106.2143 114.06 92.1537 215.65 62. 9723 74.66 106.5095 116. 30 0.0000 222 .11 66.8030 74.82 106.5354 116.74 74.3798 227.09 52.9383 74.97 106. 5596 119. 76 69.3080 227.38 54.1266 77 .11 106.9074 121.12 77.9590 228.16 0.0000 78.74 107.1686 121.22 77.9674 228.18 60.0466 79.69 107.3190 121. 78 83.3606 116.74 60.0466 80.12 107.3869 122.06 66.2823 235.69 45.7798 80.19 0.0000 122.92 66.3466 235.96 45.7886 80.57 107.4581 123.07 65.2872 238.63 49.8333 81. 00 107.5260 265.00 83.5391 238.98 0.0000 81. 07 107.5374 125 .. 81 65.8452 240.99 49.9186 81. 75 107.6433 127.23 86.0193 242.00 49.9551 83.79 101.8501 127.91 94.6924 244.70 50.0519 84.00 85.5797 129.30 94.8361 252.40 0.0000 85.43 119. 7834 131. 20 96.4720 252.80 57.5317 86.55 113.1557 133.02 96.2994 254.15 0.0000 86.79 113.1937 133.52 86.6077 256.23 58.8709 86.94 126.8580 136.00 93.3486 260.90 0.0000 Page 3470 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 58.0034 355.39 0.0000 584.27 26.4950 264.80 58.0093 356.01 42.1674 595.83 0.0000 265.00 54.3906 364.49 0.0000 427.87 29.9952 2 68. 22 53.2987 366.42 0.0000 602.52 0.0000 269.46 38.7949 372.51 37.8215 604. 72 22.8896 270.03 38.8096 375.05 46 .. 4 799 607.14 20.0464 271.23 38.8408 377.52 49.1270 609.32 20.0626 273.65 0.0000 356.01 30.2668 610.33 20.0703 276.40 43.8464 388.16 41.6016 614.28 18.6645 277.37 42.6552 388.63 0.0000 618.01 15.3359 277.60 42.6616 391.69 36.4689 620. 36 23.0244 278.00 42.6733 264.66 37.5095 621.93 11. 5190 279.20 58.5688 401.81 39.2770 630.19 0.0000 279.54 57.3616 402.40 29.6850 631. 29 21.1908 279.70 57.3673 404.85 38.4633 633.25 12.5308 280.46 47.6265 410.95 28.9361 634.78 0.0000 283.69 40.3839 413.71 32.4887 635.95 19.2977 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 37.9790 423. 72 0.0000 645.85 26.1453 285.90 0.0000 427.09 3.9. 7742 657.76 27. 7161 287.50 40.4836 427.87 38.9055 657.90 0.0000 290.67 45.8919 433.94 30.5946 661. 66 17.5291 293.27 0.0000 439.40 28.0079 664.57 0.0000 351.93 32.8743 453.88 28.6471 666.33 0.0000 295. 96 32.8898 463.37 29.6726 666.50 0.0000 879.38 19.7666 468.07 25.2309 667.71 0.0000 299.98 37.9187 473.00 0.0000 677.62 21. 5452 300.09 37.9215 475.06 21. 6953 685.70 0.0000 300.13 37.9225 476.78 21.7124 695.00 0.0000 301.36 54.4521 477.60 21.7202 696.49 24.6440 302.85 39.6377 482.18 21.7651 696. 51 24.6440 256.23 44.6385 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 28.5953 306.78 38.4927 497.08 20.9958 697.49 27.6104 308.46 44.7473 505.52 27.4866 702.65 27.6593 311. 90 47.3318 507.63 0.0000 706.68 10.8809 316.51 44.9659 511. 00 32.1432 711. 68 17.8352 319.41 0.0000 514.00 23.4487 720.70 0.0000 320.08 0.0000 514.00 23.4487 721. 93 0.0000 321.04 47.5928 520.40 11. 9870 722.78 10.4427 323.87 27.6000 520.69 0.0000 722.91 17.9026 325.23 35.1555 522.65 0.0000 723.31 17.9048 328.76 0.0000 527.90 0.0000 724.19 14.9249 333.37 39.1076 528.26 16.6523 727.33 9. 9605 333.97 36.5969 529.59 16. 6611 733.00 12.9725 334.37 36.6058 529.87 0.0000 735.93 13.9840 338.28 43.0136 531. 02 0.0000 333.97 8.9941 338.32 43.0146 537.26 0.0000 739.50 0.0000 311. 90 40.5342 546.56 0.0000 747.24 19.0487 340.48 40.5342 552.55 19.6226 748.06 17.0477 340.55 0.0000 563.25 23.4609 752.31 16.0671 344.28 49.9313 569.33 20.6957 753.82 0.0000 345.93 40.6602 946.00 23.5199 756.73 8.0452 351.06 43.3259 569.70 23.5209 756.80 8.0452 351.93 43.3477 583.19 26.4836 884.68 19.1515 Page 3471 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 27.2318 1274.44 12.9336 1620.50 *6.4706 766.42 25.2187 1001.03 12.9497 1621. 92 3.6985 766.84 25.2228 1002.74 14.5750 1678.03 0.0000 772.60 0.0000 1004.73 12. 9624 1690.97 1. 8718 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9477 778.90 10.1278 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 18.5204 1771.35 0.9488 785.37 20.2962 1038.76 0.0000 1791.20 0.0000 792.07 16.7793 631. 29 13.1016 1808.65 0.9547 794.95 12.2144 1048.07 0.0000 1810.72 0.0000 795.86 12.2178 1049.04 4.9160 1836.06 5.7539 810.06 10.2258 1050.41 11.4750 810.29 10.2266 1063.66 20.8338 344.28 12. 2725 1077.00 0.0000 810.76 12.2739 1077.34 15.4025 815.77 0.0000 1085.87 18.7432 1048.07 0.0000 1093.63 9.9412 832.01 18.5295 1099.45 5.5310 834.85 14.4238 1112. 07 16.6431 835.71 14.4278 1112.84 17.7565 836.80 0.0000 1115. 54 4. 9969 846.75 0.0000 1120.29 8.8939 846.77 14.4751 1120.55 8.8945 *856.80 0.0000 1221.41 10.0078 860.56 14.5338 1129. 67 12.2568 871.09 17.7028 1131. 51 0.0000 873.19 15.6293 1147.95 0.0000 875.33 0.0000 1173.23 15.7591 879.38 17.7450 1177.95 15.7762 880.51 18.7947 1189.05 9.0378 883.24 14.6295 1204.77 15.8730 884.68 13.5903 1221. 41 13. 6563 889.28 18.8423 1231. 02 19.3879 894.76 18.8716 1235.36 0.0000 898.04 14.6916 1238.28 20.5620 900. 72 17.8529 1260.41 0.0000 903.28 10.5094 1271.87 11.5072 911.20 14.7463 1274.44 8. 0596 912.08 14.7497 1274.54 8.0601 923.98 0.0000 1291.59 10. 4011 92 6. 50 5.2889 1298.22 0.0000 929 .11 12.7026 1312.11 0.0000 937.49 17.8247 1332.49 10.4912 944.13 0.0000 1362.66 0.0000 946.00 15.9515 1365.19 10.5630 949.00 13.8363 1368.63 0.0000 667.71 0.0000 1384.29 8.4832 962. 31 12.8179 1408.01 8.8788 964.08 9.6178 1457.56 0.0000 966.17 6.4155 1460.82 10.7666 911.20 14.4459 1489.16 4.5105 968. 97 14.4459 1505.03 2.8955 983.53 0.0000 1584.12 8.2645 984.45 0.0000 1596.21 0.0000 Page 3472 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:01:37.87 *********************************************************************************
GEL Laboratories LLC *
2040 Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Z-OCT-2016 11:00:01. Sample date 8-DEC-2015 13:38:00. Acquisition date : *3-0CT-2016 09:01:15. Sample ID G405235025 Sample quantity : l.38244E+02 GRAM Detector name GAM02 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.48 0.0% Energy*tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 3 2 3 3 3 4. 0 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 .o 27 0 28 0 29 0 30 0 31 0 32 0 33 0 Energy 72.58* 74.86* 77.02 87.50 92.77* 185.73* 238.46* 242.28 270*. 66 278.10 295.35 299.97 338.51* 351.90* 457.37 462.66 517. 62 583.23* 609.31* 661. 52* 709.24 727. 23 769.76 891.86 911. 10* 941.84 965.23* 968.88* 1120.15* 1228.04 1258.08 1460.57* 1764.70* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 8 86 165 30 60 76 324 79 69 28 148 27 88 200 40 41 40 90 161 1629 14 37 17 11 83 17 10 33 34 7 25 306 25' Bkgnd FWHM Channel Left Pw Cts/Sec %E+r Fit 75 183 168 232 244 182 189 134 180 154 169 91 105 103 63 72 66 62 51 34 23 21 34 12 14 19 27 15 18 23 23 11 3 1.14 1.14 0.95 0.94 1. 33 1. 47 1.11 1. 24 3.44 1. 63 1.13 1. 41 1. 56 1. 36 1. 75 2.74 2.35 1. 50 1. 59 1. 56 5.22 2.30 2.83 3.64 2.19 3.94 0.66 1. 54 1. 42 2.58 4.37 2.50 2.33 144.66 149.21 153.52 174.46 185.00 370.75 476.11 483.75 540.46 555.32 589.79 599.04 676.04 702.80 913.56 924.15 1033.97 1165. 09 1217.22 1321.56 1416:93 1452.88 1537.87 1781.91 1820.35 1881. 79 1928.54 1935.83 2238.18 2453.83 2513.88 2918.62 3526.57 143 143 143 169 181 366 471 481 531 550 583 596 672 697 910 920 1029 1158 1210 1313 1409 1448 1527 1775 1815 1874 1921 1932 2229 2443 2501 2911 3520 15 2.19E-03162.l 2.95E+OO 15 2.40E-02 29.3 15 4.59E-02 14.3 8 8.38E-03 89.8 10 1.68E-02 54.2 11 2.lOE-02 38.3 10 9.0lE-02 9.8 9 2.20E-02 29.9 16 1.93E-02 45.3 11 7.78E-03 87.9 13 4.12E-02 19.8 8 7.40E-03 65.2 12 2.45E-02 25.6 10 5.55E-02 12.0 9 1.llE-02 38.6 8 1.14E-02*39.1 13 1.llE-02 44.5 14 2.50E-02 21.7 15 4.48E-02 12.8 15 4.52E-01 2.6 15 3.75E-03 81.3 11 1.02E-02 29.5 15 4.74E-03 78.1 12 3.06E-03 69.8 11 2.30E-02 14.5 16 4.64E-03 64.5 12 2.86E-03108.1 11 9.21E-03 28.7 14 9.43E-03 32.5 12 1.90E-03153.8 24 7.03E-03 54.8 15 8.51E-02 6.3 12 6.90E-03 27.5 Flag: "*" = Peak area was modified by background subtraction Page 3473of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:01:39 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl ' Sample title Sample date 8-DEC-2015 13:38:00 Acquisition date : 3-0CT-2016 09:01:15 Sample ID G405235025 Sample quantity 138.24 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID Sample geometry : GAMMA2 Detector geometry: 0 01:00:00.00 Elapsed real time: 1.50 keV Half life ratio No Linear 75.00 Systematic Error Efficiencies at Interference Report Interfering Interfered Nuclide Page 3474 of 5809 PB-214. PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351.93 Nuclide RA-224 SN-126 SN-126 CD-109 HG..'..203 AM-243 TH-228 PB-212 . BI-211 Line 240.99 86.94 87.57 88.03 279.20 74.66 74.82 74.82 351.06 CAN 0 01:00:00.48 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235025 Acquisition date 3-0CT-2016 09:01:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.060E+OO 1.410E+Ol 1.410E+Ol 12.62 OK BA-137M 661.66 89.90* 2.016E+OO 4.997E+OO 5.092E+OO 5.22 OK CS-137 661.66 85.10* 2.016E+OO 5.279E+OO 5.379E+OO 5.22 OK HG-203 70. 83" 3.69 3.355E+OO Line Not Found Absent 72.87 6.19 3.544E+OO 2.360E-01 2.043E+Ol 324.14 OK 279.20 81.56* 4.164E+OO 2.751E-02 2.381E+OO 315.48 OK TL-208 277.37 6.60 4.173E+OO Line Not Found <<INT Reject 583.19 85.00* 2.233E+OO 2.666E-01 2.666E-01 43.48 OK 860.56 12.50 1.634E+OO Line Not Found Absent PB-212 74.82 10.28 3.779E+OO 7.765E-01 7.765E-01 115. 07 OK 77 .11 17.10 3.992E+OO 1.584E+OO 1.584E+OO 28.65 OK 238.63 43.60* 4.703E+OO 9.530E-01 9.530E-01 19.57 OK 300.09 3.30 3.911E+OO 1.222E+OO 1.222E+OO 130.41 OK BI-214 609.32 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 OK 1120.29 14.92 1.323E+OO 9.153E-01 9.156E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 OK PB-214 74.82 5.80 3.775E+OO Line Not Found <<IN.T Reject 77 .11 9.70 3.992E+OO 2.792E+OO 2 .*793E+OO 28.65 OK 87.09 3.41 4.866E+OO 1.178E+OO 1.178E+OO 179.68 OK 242.00 7.25 4. 651E+OO Line Not Found <<INT Reject 295.22 18.42 3. 962E+OO 1.206E+OO 1.206E+00 39.65 OK 351.93 35.60* 3.416E+OO 9.612E-01 9.615E-01 23.99 OK RN-222 609.32 45.49* 2.154E+OO 9.207E-01 9.210E-01 25 .. 70 OK 1120.29 14.92 1.3238+00 9.153E-01 9.156E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 OK RA-224 240.99 4.10* 4.647E+OO 3.704E-01 3. 704E-'01 464.33 OK RA-226 609.32 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 OK 1120.29 14.92 1. 323E+OO 9.153E-01 9.156E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 OK AC-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11.27 3. 531E+OO 1. 301E+OO 1. 301E+OO 51.16 OK 794.95 4.25 1. 740E+00 Line Not Found Absent 835. 71 1. 61 1. 672E+OO Line Not Found* Absent 911.20 25.80* 1.561E+OO 1.114E+OO 1.114E+OO 28.98 OK 968. 97 15.80 1. 487E+OO 7.606E-01 7.606E-01 57.36 OK RA-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.531E+OO 1. 301E+OO 1.301E+OO 51.16 OK 794.95 4.25 1.740E+OO Line Not Found Absent 835.71 1. 61 1.672E+oo Line Not Found Absent 911.20 25.80* 1. 561E+OO 1.114E+OO 1.114E+OO 28.98 OK 968. 97 15.80 1.487E+OO 7.606E-01 7.606E-01 57.36 OK TH-228 74.82 10.28 3.779E+OO 7.765E-01 7.765E-01 115.07 OK 77 .11 *17 .10 3.992E+OO 1.584E+OO l.584E+OO 28.65 OK 238.63 43.60* 4.703E+OO 9.530E-01 9.530E-01 19.57 OK 300.09 3.30 3. 911E+OO 1.222E+OO 1.222E+OO 130.41 OK TH-230 609.32 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 OK 1120.29 14.92 1.323E+OO. 9.153E-01 9.153E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 OK PA-231 283.69" 1. 70 4.097E+OO Line Not Found Absent Page 3475 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235025 Acquisition date 3-0CT-2016 09:01:15 Nuclide Type: Nuclide Uncorrected Decay Corr 2-Sigma Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 301.36 5.35* 3. 911E+00 7.540E-01 7.540E-01 130.41 OK TH-232 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 li.27 3.531E+OO l.301E+OO 1.301E+OO 51.16 OK 835.71 1. 61 1. 672E+OO Line Not Found Absent 911.20 25.80* 1.561E+OO 1.114E+00 1.114E+OO 28. 98. OK 968. 97 15.80 l.487E+OO 7.606E-01 7.606E-01 57.36 OK U-234 609.32 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 OK 1120.29 14.92 l.323E+OO 9.153E-01 9.153E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 OK AM-243 43.53 5.90 2.878E-01 Line Not Found Absent 74.66 67.20* 3.779E+OO 1.188E-01 1.188E-01 115. 07 OK Flag: "*" Key line Page 3476 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:01:40.65 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l *
Acquisition date 3-0CT-2016 09:01:15 Sensitivity : 3:000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
S.ample date 8-DEC-2015 13: 38: 00 Analyst initials: MXRl *
Sample ID G405235025 Sample Quantity 1.3824E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
Eff. *File : DKA100: [CANBERRA .. GAMMAJEFF GAM02 CAN. CNF; 15
Combined Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM K-40 1.410E+Ol 1.743E+OO 7.327E-01 BA-137M 5.092E+OO 2.603E-01 8.412E-02 CS-137 5.379E+OO 2.750E-01 8.887E-02 HG-203 2.381E+OO 7.361E+OO 6 .196E+OO TL-208 2.666E-01 l.136E-01 7.886E-02 PB-212 9.530E-01 1. 828E-'-01 l.378E-01 BI-214 9.210E-01 2.320E-01 1.646E-01 PB-214 9.615E-01 2.261E-01 1.913E-01 RN-222 9.210E-01 2.320E-01 1. 646E-01 RA-224 3.704E-01 l.686E+OO 1.667E+OO RA-226 9.210E-01 2.320E-01 1.646E-01 AC-228 1.114E+OO 3.165E-01 3.234E-01 RA-228 1.114E+OO 3.165E-01 3.234E-01 TH-228 9.530E-01 l.828E-01 *1. 378E-01 TH-230 9.207E-01 2.319E-01 1.645E-01 PA-231 7.540E-01 9.636E-01 1.125E+OO TH-232 1.114E+OO 3.165E-01 3.234E-01 U-234 9.207E-01 2.319E-01 1.645E-01 AM-243 l.188E-01 1.340E-01 1.270E-01 Non-Identified Nuclides Key-Line Activity K.L; Cnt Uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM BE-7 1.116E+Ol 2.205E+Ol 4.168E+Ol NOT IDENT. NA-22 2. 511E-02 5.260E-02' l .115E-01 NOT IDENT. NA-24 O.OOOE+OO 7.426E+40 O.OOOE+OO SHORT HLIF AL-26 -l.146E-02 3.389E-02 6.708E-02 NOT IDENT. SC-46 7.694E-02 4.747E-01 8.380E-01 FAIL ABUN V-48 O.OOOE+OO l.589E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 5.855E+02 O.OOOE+OO SHORT HLIF MN-54 8.808E-03 7.637E-02 l.515E-01 NOT IDENT. C0-56 -2.099E-01 5. 713E-01 l.061E+OO NOT IDENT. MN-56 0.000E+OO l.960E+41 0.000E+OO SHORT HLIF C0-57 -5.256E-02 6.336E-02 l.059E-01 NOT IDENT. Page 3477 of 5809 C0-58 6. 041E-02 6.614E-01 l.327E+OO NOT IDENT. FE-59 1.134E+OO 7.697E+OO 1.540E+Ol NOT IDENT. C0-60 2.904E-03 5.003E-02 9.793E-02 NOT IDENT. ZN-65 8.404E-02 2.056E-01 3.882E-01 NOT IDENT. GE-68 -5. 071E-01 2.600E+OO 4.934E+OO NOT IDENT. AS-73 2.324E+OO l.603E+Ol 3.032E+Ol NOT IDENT. AS-74 0.000E+OO 8.622E+03 O.OOOE+OO SHORT HLIF SE-75 -2. 396E-01 3.288E-01 5.183E-01 FAIL ABUN BR-77 O.OOOE+OO 3.268E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.797E+02 O.OOOE+OO SHORT HLIF RB-83 2,277E-01 l.076E+OO l.813E+OO NOT IDENT. KR-85 -4.606E+Ol 1. 729E+Ol 1.942E+Ol NOT IDENT. SR-85 -4.867E+OO 1.827E+OO 2.052E+OO NOT IDENT. RB-86 O.OOOE+OO 3.100E+04 O.OOOE+OO SHORT HLIF Y-88 5.231E-02 1.540E-01 4.248E-01 NOT IDENT. Y-91 -3.265E+02 6.188E+02 l.080E+03 NOT IDENT. NB-9.4 l.383E-02 3.938E-02 7.290E-02 NOT IDENT. NB-95 -5.155E-01 1.065E+OO 1. 735E+OO NOT IDENT. NB-95M -5.541E-01 3.365E+OO 5. 660E+oo* NOT IDENT. ZR-95 -4.858E-02 1.638E+OO 3. 231E+OO NOT IDENT. NB-97 O.OOOE+OO 1.364E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.813E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.977E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 347E-.02 4. 720'E-02 8.212E-02 NOT IDENT. RH-102 -5.587E-02 7.999E-02 l.320E-01 NOT IQENT. RU-103 5.291E+OO 8.698E+OO 1.691E+Ol FAIL ABUN RH_.:.106 3.664E-01 6.435E-01 1.277E+OO NOT IDENT. RU-106 3.664E-01 6.435E-:-01 1.277E+OO NOT IDENT. AG-108M -1. 789E-02 4.639E-02 8.208E-02 NOT IDENT. CD-109 1. 703E+OO 2.999E+OO 2.952E+OO FAIL ABUN AG-llOM 3.027E-02 1.070E-01 2.175E-01 NOT IDENT. SN-113 3.862E-01 3.802E-01 7.527E-01 NOT IDENT. CD-115 O.OOOE+OO 4.476E+39 0.000E+OO SHORT HLIF SN-117M O.OOOE+OO l.285E+05 O.OOOE+OO SHORT HLIF TE-123M -3.518E-02 1. 753E-01 3.357E-01 NOT IDENT. SB-124 -5.349E-01 1.858E+OO 3.847E+OO NOT IDENT. SB-125 1.483E-01 l.868E-01 3.607E-01 FAIL ABUN TE-125M 8. 963E+Ol 3.866E+02 7.050E+02 NOT IDENT. I-126 O.OOOE+OO l.165E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.430E+06 O.OOOE+OO SHORT HLIF SN-126 1. 086E-01 l.912E-01 1.943E-01 FAIL ABUN SB-127 O.OOOE+OO 2.622E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.924E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.277E+26 O.OOOE+OO SHORT HLIF BA-133 1.067E-03 6.629E-02 1.106E-01 NOT IDENT. I-133 O.OOOE+OO 1.258E+41 O.OOOE+OO SHORT HLIF CS-134 6.142E-02 5.941E-02 1.307E-01 NOT IDENT. CS-135 l.531E-01 1.950E-01 3.867E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.086E+05 O.OOOE+oo* SHORT HLIF CE-139 2.862E-02 1.241E-01 2.455E-01 NOT IDENT. BA-140 O.OOOE+OO 1.987E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.069E+05 0.000E+OO SHORT HLIF c*E-141 -4.192E+Ol 3. 231E+Ol 5.107E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 2 8 OE+41 O.OOOE+OO SHORT HLIF CE.,-144 -2.177E-01 4.719E-01 8.085E-01 NOT IDENT. PM-144 i .131E-02 6. 551E-02 l.314E-01 NOT IDENT. PR-144 9.825E-01 5.690E+OO 1.141E+Ol NOT IDENT. PM-146 -3.209E-03 8.445E-02 1.366E-01 NOT IDENT. ND-147 O.OOOE+OO 4.732E+07 O.OOOE+OO SHORT HLIF PM-147 3 .119E+02 l.017E+03 l.873E+03 NOT IDENT. PM-149 O.OOOE+OO 6.279E+40 O.OOOE+OO SHORT HLIF EU-150 1.919E-02 4.046E-02 7.085E-02 FAIL ABUN EU-152 2.596E-02 1.421E-01 2.429E-01 FAIL ABUN GD-153 -5. 715E-02 2.777E-01 4. 591E-01 NOT IDENT. EU-154 6.448E-02 l.295E-01 2.751E-01 NOT IDENT. EU-155 7.081E-02 1.415E-01 2.650E-01 FAIL ABUN TB-160 l.360E+00 2 .113E+OO 4.563E+OO FAIL ABUN H0-166M -l.342E-02 6.223E-02 l.058E-01 FAIL ABUN TM-171 -1.346E+Ol 3.933E+Ol 7.211E+Ol NOT IDENT. HF-172 -2.579E-02 3.085E-01 5.465E-01 NOT IDENT. LU-172* 2.066E-02 9.199E-02 1.848E-01 FAIL ABUN LU-176 -9.477E-03 3.347E-02 6.151E-02 FAIL ABUN HF-181 l.524E+00 7.273E+OO 1.350E+Ol NOT IDENT. TA-182 1.341E+OO 2.081E+OO FAIL ABUN RE-183 -1.506E+00 5.135E+OO 9.379E+OO NOT IDENT. Page 3478 of 5809 RE-184 8. 722E+OO 3.298E+Ol 6.799E+Ol NOT IDENT. W-188 9.662E+Ol l.655E+02 2. 960E+02 NOT IDENT. IR-192 -3.103E-02 6.270E-01 l.174E+OO FAIL ABUN BI-207 1. 700E-02 4.652E-02 9.940E-02 FAIL ABUN PB-210 1.178E+OO 6.676E+00 l.269E+Ol NOT IDENT. BI-211 O.OOOE+OO 6.228E-01 9.734E-01 FAIL ABUN PB-211 -4.126E-01 l.098E+OO l.953E+OO NOT IDENT. BI-212 O.OOOE+OO 9.447E-01 1.529E+OO FAIL ABUN RN-219 -l.423E-01 6.267E-01 1.129E+OO FAIL ABUN RA-223 3.427E-01 8.308E-01 l.603E+OO FAIL ABUN AC-227 3.517E-02 2.972E-01 5.691E-01 FAIL ABUN TH-227 3.517E-02 2.972E-01 5.691E-01 FAIL ABUN TH-229 -3.194E-01 6.313E-01 1.173E+OO FAIL ABUN TH-231 3.427E-01 8.308E-01 l.603E+OO FAIL ABUN PA-233 -5.642E-02 7.810E-02 l.381E-01 FAIL ABUN PA-234 -1.635E-01 3.451E-01 5.308E-01 NOT IDENT. PA-234M -5 .196E+OO 5.090E+OO 8.894E+OO NOT IDENT. TH-234 1. 896E+OO 1.987E+OO 4.038E+OO FAIL ABUN U-235 5.759E-02 2.464E-01 4.461E-01 FAIL ABUN NP-237 -5.642E-02 7.810E-02 1.381E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 l.896E+OO 1.987E+OO 4.038E+OO FAIL ABUN 'NP-239 1.878E-01 3.205E-01 5.998E-01 FAIL ABUN PU-239 -2.524E+01 4.323E+02 7.636E+02 NOT IDENT. AM-241 -3. 896E-02 2.244E-01 4.127E-01 NOT IDENT. CM-243 4.668E-02 1.316E-01 2.440E-01 FAIL ABUN BK-247 -7.946E-02 l.143E-01 l.809E-01 NOT IDENT. CM-247 4.401E-03 5.597E-02 1.036E-01 FAIL ABUN CF-249 -4.305E-02 5.805E-02 *1.004E-01 NOT IDENT. CF-251 -7.255E-02 1.350E-01 2.527E-01 NOT IDENT. ANH-511 -3.056E-02 6.123E-02 1.218E-01 NOT IDENT. Page 3479 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:01:38.57 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 293 10.66* 1.060E+OO 1.410E+Ol 1.410E+Ol 12.62 CD-109 88.03 36 3.70* 4.866E+OO 1.086E+OO 1. 703E+OO 179.68 SN-126 64.28 ------9.60 2.600E+OO ------Line Not Found ------86.94 36 8.90 4.866E+OO 4.513E-01 4.513E-01 179.68 87.57 36 37.00* 4.866E+OO 1. 086E-01 1. 086E-01 179.68 BA-137M 661. 66 1667 89.90* 2.016E+OO 4.997E+OO 5.092E+OO 5.22 CS-137 661. 66 1667 85.10* 2.016E+OO 5;279E+OO 5.379E+OO 5.22 HG-203 70.83 ------3.69 3.355E+OO ------Line Not Found ------72.87 10 6.19 3.544E+OO 2.360E-01 2.043E+Ol 324.14 279.20 31 81.56* 4.164E+OO 4.909E-02 4.248E+OO 175.76 TL-208 277.37 31 6.60 4.164E+OO 6.066E-01 6.066E-01 175.76 583.19 93 85.00* 2.233E+OO 2.666E-01 2.666E-01 43.48* 860.56 ------12.50 1.634E+OO ------Line Not Found ------BI-211 72. 87 10 1. 23 3.544E+OO l.188E+OO 1.188E+OO 324.14 351.06 215 12.92* 3.416E+OO 2.648E+OO 2.648E+OO 23.99 PB-212 74.82 104 10.28 3.779E+OO 1.456E+OO 1. 456E+OO 58.65 77 .11 199 17.10 3.992E+OO l.584E+00 1. 584E+OO 28.65 238.63 360 43.60* 4.703E+00 9.530E-01 9.530E-01 19.57 300.09 29 3.30 3. 911E+OO l.222E+00 l.222E+00 130. 41 BI-214 609.32 166 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 1120.29 33 14.92 '1.323E+00 9.153E-01 9.156E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 PB-214 74.82 104 5.80 3.779E+OO 2.581E+OO 2.581E+OO 58.65 77 .11 199 9.70 3.992E+OO 2.792E+OO 2.793E+OO 28.65 87.09 36 3.41 4.866E+OO l.178E+OO 1.178E+OO 179.68 242.00 88 7.25 4.647E+00 1.415E+OO l.416E+00 59.86 295.22 162 18.42 3.962E+OO l.206E+OO 1.206E+OO 39.65 351. 93 215 35.60* 3.416E+OO 9.612E-01 9.615E-01 23.99 RN-222 609.32 166 45.49* 2.154E+00 9.207E-01. 9.210E-01 25.70 1120.29 33 14.92 1.323E+00 9.153E-01 9.156E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.293E-01. 55.03 RA-224 240.99 88 4.10* 4.647E+OO 2.502E+OO 2.502E+OO 59.86 RA-226 609.32 166 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 1120.29 33 14.92 l.323E+OO
9 .153E-01 9.156E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.293E-01 55:03 AC-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 95 11. 27 3.531E+OO l.301E+OO l.301E+OO 51.16 794.95 ------4.25 1.740E+OO ------Line Not Found ------835.71 ------1. 61 1. 672E+OO ------Line Not Found ------911.20 83 25.80* l.561E+OO l .114E+OO 1.114E+OO 28.98 968. 97. 33 15.80 1. 487E+OO 7.606E-01 7.606E-01 57.36 RA-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 95 11. 27 3.531E+OO l.301E+00 1. 301E+OO 51.16 794.95 ------4.25 1. 740E+OO ------Line Not Found ------835 .'71 ------1. 61 1. 672E+OO ------Line Not Found ------911. 20 83 25. 80* l.561E+OO l .114E+OO 1.114E+OO 28.98 968. 97 33 15.80 1.487E+OO 7.606E-01 7.606E-01 57.36 Page 3480 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235025 Acquisition date 3-0CT-2016 09:01:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Er.ror TH-228 74.82 104 10.28 3.779E+OO 1. 456E+OO 1.456E+OO 58.65 77 .11 199 17.10 3.992E+OO 1. 584E+OO 1.584E+OO 28. 65 238.63 360 43.60* 4.703E+OO 9.530E-01 9.530E.-01 19.57 300.09 29 3.30 3. 911E+OO l.222E+OO 1.222E+OO 130.41 TH-230 609.32 166 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 1120.29 33 14.92 1.323E+OO 9.153E-01 9.153E-01 64.96 1764.49 23 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 PA-231 283.69 ------1. 70 4.097E+OO ------Line Not Found ------301.36 29 5.35* 3. 911E+OO 7.540E-01 7.540E-01 130.41 TH-232 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 95 11. 27. 3.531E+OO 1.301E+OO 1.301E+OO 51.16 835. 71 ------1. 61 1.672E+OO ------Line Not Found ------911. 20 83 25.80* l.561E+OO 1.114E+OO 1.114E+OO 28.98 968. 97 33 15.80 l.487E+OO 7.606E-01 7.606E-01 57.36 U-234 609.32 166 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 1120.29 33 14.92 1.323E+OO 9.153E-01 9.153E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 AM-243 43.53 ------5.90 2.878E-01 ------Line Not Found ------74.66 104 67.20* 3.779E+OO 2. 227E-'01 2.227E-01 58.65 Flag: "*" Key line Page 3481of5809 Summary of Nuclide Activity Sample ID : G405235025 Acquisition date Page : 3 3-0CT-2016 09:01:15 Total number of lines in spectrum 33 Number of unidentified lines 8 Number of lines tentatively identified by NID 25 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 46.59D 1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1. 41E+10Y 1. 41E+lOY 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 86.6 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.410E+Ol 1.086E+OO l.086E-01 4.997E+OO 5.279E+OO 4.909E-02 2.666E-01 2.648E+OO 9.530E-01 9.207E-01 9.612E-01 9.207E-01 2.502E+OO 9.207E-01 l .114E+OO l .114E+OO 9.530E-01 9.207E-01 7.540E-01 l.114E+OO 9.207E-01 2.227E-01 4.283E+Ol 4.283E+Ol Decay Corr pCi7GRAM 1.410E+Ol 1.703E+OO 1.086E-01 5.092E+OO 5.379E+OO 4.248E+OO 2.666E-01 2.648E+OO 9.530E-01 9.210E-01 9.615E-01 9.210E-01 2.502E+OO 9.210E-01 1.114E+OO 1.114E+OO 9.530E-01 9.207E-01 7.540E-01 1.114E+OO 9.207E-01 2.227E-01 4.784E+Ol 4.784E+Ol 75.76% Decay Corr 2-Sigma Error 0.178E+Ol 3.060E+OO l.951E-01 0.266E+OO 0.281E+OO 7.467E+OO l.159E-01 0.635E+OO l.865E-01 2.367E-01 2.307E-01 2.367E-01 l.498E+OO 2.367E-01 0.323E+OO 0. 32'3E+OO 1.865E-01 2.366E-01 9.833E-01 0.323E+OO 2.366E-01 1.306E-01 "M" Manually accepted 2-Sigma %Error 12. 62 179.68 179.68 5.22 5.22 175.76 43.48 23.99 19.57 25.70 23.99 25.70 59.86 25.70 28.98 28.98 19.57 25.70 130.41 28.98 25.70 58.65 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3482 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235025 Acquisition date : 3-0CT-2016 09:01:15 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 92.77 72 290 1. 33 185.00 181 10 l.68E-02 **** 5.21E+OO T 0 185.73 86 206 1. 47 370.75 366 11 2.lOE-02 76.6 5.56E+OO T 0 270.66 76 197 3.44 540.46 531 16 1.93E-02 90.5 4.26E+OO T 0 457.37 42 66 1. 75 913.56 910 9 l.llE-02 77.2 2.73E+OO 0 462.66 43 76 2.74 924.15 920 8 l.14E-02 78.2 2.71E+OO T 0 517.62 42 69 2.35 1033.97 1029 13 l.llE-02 88.9 2.46E+OO 0 709.24 14 23 5.22 1416.93 1409 15 3.75E-03 **** l.91E+OO 0 727.23 37 21 2.30 1452.88 1448 11 l.02E-02 59.1 1.87E+OO T 0 769.76 17 34 2.83 1537.87 1527 15 4.74E-03 **** 1. 79E+OO 0 891.86 11 12 3.64 1781.91 1775 12 3.06E-03 **** 1.59E+OO 0 941. 84 17 19 3.94 1881.79 1874 16 4.64E-03 **** l.52E+OO 0 965. 23 10 27 0.66 1928.54 1921 12 2.86E-03 **** l.49E+00 T 0 1228.04 7 22 2.58 2453.83 2443 12 l.90E-03 **** 1.23E+OO 0 1258.08 25 22 4.37 2513.88 2501 24 7.03E-03 **** l.20E+OO Flags: "T" = Tentatively associated Page 3483 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:01:52.92 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l * *Acquisition date 3-0CT-2016 09:01:15 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
Sample date 8-DEC-2015 13:38:00 Nuclide Library : SOLID *
Sample ID G405235025 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.3824E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 22-AUG-2016 09: 02: 05 E_ff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate 9f Analysis. Identified Nuclides Nuclide K-40 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Le (pCi"/GRAM 3.012E-01 3.786E-02 4.000E-02 2.905E+OO 3.549E-02 6.521E-02 7.465E-02 8.946E-02 7.465E-02 7.941E-01 7.465E-02 1.433E-01 1.433E-01 6.521E-02 7.463E-02 5.264E-01 l.433E-01 7.463E-02
6.046E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3484 of 5809 Le (pCi/GRAM 1. 949E+Ol 4.802E-02 O.OOOE+OO 2. 511E-02 3.633E-01 O.OOOE+OO O.OOOE+OO 6.712E-02 4.642E-01 O.OOOE+OO 4.982E-02 5.814E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 *sN-117M *TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3485 of 5809 6.660E+OO 4.180E-02 1.683E-01 2.104E+OO 1.437E+Ol 0.000E+OO 2.423E-01 O.OOOE+OO O.OOOE+OO 8.308E-01 8.978E+OO 9.483E-01 O.OOOE+OO 1.520E-01 4.607E+02 3.256E-02 7.606E-01 2.664E+00 1.421E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.889E-02 5.860E-02 7.810E+OO 5.762E-01 5. 762E-'01 3.813E-02 1.410E+OO 9.403E-02 3.538E-01 O.OOOE+OO O.OOOE+OO 1.592E-01 1.399E+OO 1.697E-01 3.345Et02 O.OOOE+OO O.OOOE+OO 9.289E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 5.149E-02 O.OOOE+OO 5.876E-02 1.823E-01 O.OOOE+OO O.OOOE+OO 1.154E-01 O.OOOE+OO O.OOOE+OO 2.399E+Ol 0.000E+OO 3.810E-01 5.882E-02 5.109E+OO 6.367E-02 0.000E+OO 8.819E+02 O.OOOE+OO 3.320E-02 1.130E-01 2.180E-01 1.186E-01 l.254E-01 2.009E+OO 4.563E-02 3. 411E+Ol 2.583E-01 8.060E-02 2.865E-02 6.270E+OO 9.043E-01 4.448E+OO 2. 960E+Ol NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. .FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227' TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3486 of 5809 1. 38 8E+02 5.462E-01 4.238E-02 5.988E+OO 4.698E-01 9.107E-01 7.049E-01 5.273E-01 7.501E-01 2.666E-01 2.666E-01 5.548E-01 7.501E-01 6.388E-02 2.246E-01 3.838E+OO 1.935E+OO 2. ll 7E-01 6.388E-02 O.OOOE+OO 1.935E+OO 2.840E-01 3. 621E+02 l.956E-01 1.154E-01 8.460E-02 4.836E-02 4.657E-02 1.186E-01 5.790E-02 NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN E:'AIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:01:58.87 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l * *Acquisition date 3-0CT-2016 09:01:15 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
Sample date 8-DEC-2015 13: 38: 00 Nuclide Library* : SOLID *
Sample ID G405235025 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.3824E+02 GRAM *
Quantity Err(%) : 1.4467E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 22-AUG-20lq 09:02:05 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. refer to Certificate of Analysis. ----Identi!ied Nuclides Activity Nuclide (pCi/GRAM K-40 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 PB.:...214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 1.410E+Ol 5.092E+OO 5.379E+OO 2.381E+OO 2.666E-01 9.530E-01 9.210E-01 9.615E-01 9.210E-01 3.704E-01 9.210E-01 1.114E+OO 1.114E+OO 9.530E-01 9.207E-01 7.540E-01 1.114E+00 9.207E-01 1.188E-01 Act Error ( 1. 96-sigma) 1.892E+OO 3.404E-01 3.592E-01 7.365E+OO 1.142E-01 1.897E-01 2.353E-01 2. 296E-01 2.353E-01 1.692E+OO 2.353E-01 3.216E-01 3.216E-01 L 897E-01 2.352E-01 9.770E-01 3.216E-01 2.352E-01 1.348E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3487 of 5809 Key-Line Activity (pCi/GRAM 1.116E+Ol 2.517E-02 -1.000E+41 -1.146E-02 7.694E-02 -6.158E+03 8.994E+Ol 8.808E-03 -2.099E-01 -1.000E+41 -5.256E-02 K.L Act error ( 1. 96-sigma) 2.205E+Ol 5.261E-02 8.612E+40 3.390E-02 4.747E-01 1.590E+04 5.855E+02 7.638E-02 5.714E-01 2.750E+41 6.340E-02 TPU ( 1. 96-sigma) 1.892E+OO. 3.404E-01 3.592E-01 7.365E+OO 1.142E-01 1.897E-01 2.353E-01 2.296E-01 2.353E-01 1.692E+OO 2.353E--'01 3.216E-01 3.216E-01 1.897E-01 2.352E-01 9. 770K-01 3.216E-01 2.352E-01 1.348E-01 TPU ( 1. 96-sigma) 2.262E+Ol 5.382E-02 O.OOOE+OO 3.429E-02 4.760E-01 1.614E+04 5.869E+02 7.648E-02 5.792E-01 O.OOOE+OO 6.769E-02 NOT IDENT. NOT IDENT. *SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 6.041E-02 6.614E-01 6.619E-01 NOT IDENT. FE-59 1.134E+OO 7.697E+OO 7. 714E+OO NOT IDENT. C0-60 2.904E-03 5.003E-02 5.005E-02 NOT IDENT. ZN-65 8.404E-02 2.056E-01 2.091E-01 NOT IDENT. GE-68 -5. 071E-01 2.600E+OO 2.610E+OO NOT IDENT. AS-73 2.324E+OO 1.604E+Ol 1.607E+Ol' NOT IDENT. AS-74 -3.375E-f-03 8.626E+03 8.759E+03 SHORT HLIF SE-75 -2. 396E-01 3.290E-01 3.463E-01 FAIL ABUN BR-77 1. 704E+38 l.475E+39 O.OOOE+OO SHORT HLIF SR-82 2.385E+02 8.798E+02 8.864E+02 SHORT HLIF RB-83 2.277E-01 1.077E+OO 1.081E+OO NOT IDENT. KR-85 -4.606E+Ol 1. 740E+Ol 2.709E+Ol NOT IDENT. SR-85 -4.867E+OO l.838E+OO 2.862E+OO NOT IDENT. RB-86 :-8.835E+02 3.100E+04 3.100E+04 SHORT HLIF Y-88 5. 231E-02 l.540E-01 l.558E-01 NOT IDENT. Y-91 -3.265E+02 6.189E+o2 6.362E+02 NOT IDENT. NB-94 l.383E-02 3.939E-02 3.988E-02 NOT IDENT. NB-95 -5.155E-01 l.065E+OO l.090E+00 NOT IDENT. NB-95M -5.541E-01 3.366E+OO 3.375E+OO NOT IDENT. ZR-95 -4.858E-02 l.638E+00 l.638E+OO NOT IDENT. NB-97 1.000E+41 1. 365E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 7.823E+40 0.000E+OO SHORT HLIF M0-99 5.166E+31 l.977E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 2.763E+41 O.OOOE+OO SHORT HLIF RH-101 -l.347E-02 4.726E-02 4.765E-02 NOT IDENT. RH-102 -5.587E-02 8.012E-02 8.399E-02 NOT IDENT. RU-103 5.291E+OO 8.701E+OO 9.022E+OO FAIL ABUN RH-106' 3.664E-01 6.439E-01 6.647E-01 NOT IDENT. RU-106 3.664E-01 6.439E-01 6.647E-01 NOT IDENT. AG-108M -1. 789E-02 4.640E-02 4.709E-02 NOT IDENT. CD-109 1. 703E+OO 3.002E+OO 3.099E+00 FAIL ABUN AG-110M 3.027E-02 1.070E-01 1.078E-01 NOT IDENT. SN-113 3.862E-01 3.805E-01 4 .185E.-01 NOT IDENT. CD-115 -1.930E+39 4.489E+39 O.OOOE+OO SHORT HLIF SN-117M -l.162E+04 l.285E+05 1.286E+05 SHORT HLIF TE-123M -3.518E-02 1. 753E-01 l.760E-01 NOT IDENT. SB-124 -5.349E-01 l.859E+OO l.874E+OO NOT IDENT. SB-125 l.483E-01 1. 869E-01 l.985E-01 FAIL ABUN TE-125M 8. 963E+Ol 3.866E+02 3.887E+02 NOT IDENT. I-126 7.253E+05 l.169E+06 l.214E+06 SHORT HLIF SB-126 5. 661E+05 1.434E+06 1.457E+06 SHORT HLIF SN-126 1. 086E-01 l.913E-01 l.974E-01 FAIL ABUN SB-127 -2.502E+21 2.644E+22 O.OOOE+OO SHORT HLIF I-131 -l.906E+08 7.924E+09 7.925E+09 SHORT HLIF I-132 l.OOOE+41 1.906E+42 O.OOOE+OO SHORT HLIF TE-132 -2.869E+26 5.404E+26 O.OOOE+OO SHORT HLIF BA-133 l.067E-03 6.629E-02 6.629E-02 NOT IDENT. I-133 -1.000E+41 2.203E+41 O.OOOE+OO SHORT HLIF CS-134 6.142E-02 5.947E-02 6.560E-02 NOT IDENT. CS-135 1. 531E-01 1.952E-01 2. 071E-01 NOT IDENT. I-135 -l.000E+41 9.774E+41 O.OOOE+OO SHORT HLIF CS-136 -4.679E+04 4.086E+05 4. 091E+05 SHORT HLIF CE-139 2.862E-02 1.242E-01 l.249E-01 NOT IDENT. BA-140 -2.192E+05 l.987E+06 l.990E+06 SHORT HLIF LA-140 -3.699E+04 5.069E+05 5. 072E+05 SHORT HLIF CE-141 -4.192E+Ol 3.236E+Ol 3.748E+Ol NOT IDENT. CE-143 1.000E+41 l.284E+41 O.OOOE+OO SHORT HLIF CE-144 -2.177E-01 4. 721E-01 4.822E-01 NOT IDENT. PM-144 l .131E-02 6. 551E-02 6.571E-02 NOT IDENT. PR-144 9.825E-01 5.690E+OO 5.708E+OO NOT IDENT. PM-146 -3.209E-03 8.445E-02 8.446E-02 NOT IDENT. ND-147 . -2 .152E+07 4.733E+07 4.832E+07 SHORT HLIF PM-147 3 .119E+02 1. 017E+03 1.027E+03 NOT IDENT. PM-149 2.724E+40 6.307E+40 O.OOOE+OO SHORT HLIF EU-150 1.919E-02 4.047E-02 4.138E-02 FAIL ABUN EU'....152 2. 596E-02 l.421E-01 1.426E-01 FAIL ABUN GD-153 -5.715E-02 2.777E-01 2.789E-01 NOT IDENT. EU-154 6.448E-02 l.296E-01 l.328E-01 NOT IDENT. EU-155 7.081E-02 l.416E-01 l.452E-01 FAIL ABUN TB-160 1.360E+OO 2. 115E+OO 2.202E+OO FAIL ABUN H0-166M -l.342E-02 6.223E-02 6.253E-02 FAIL ABUN TM-171 -l.346E+Ol 3.935E+Ol 3.981E+Ol NOT IDENT. HF-172 -2.579E-02 3.085E-01 3.087E-01 NOT IDENT. LU-172 2.066E-02 9.201E-02 9.248E-02 FAIL ABUN LU-176 -9.477E-03 3.348E-02 3.375E-02 FAIL ABUN HF-181 l.524E+OO 7.273E+OO 7.305E+00 NOT IDENT. TA-182 -3.884E-01 1.341E+OO l.353E+OO FAIL ABUN RE-183 -1.506E+OO 5.140E+OO 5.185E+OO NOT IDENT. Page 3488 of 5809 RE-184 8. 722E+OO 3.304E+Ol 3.327E+Ol NOT IDENT. W-188 9.662E+Ol 1.659E+02 1.715E+02 NOT IDENT. IR-192 -3.103E-02 6.270E-Ol 6. 272E-01 FAIL ABUN BI-207 1.700E-02 4.653E-02 4.715E-02 FAIL ABUN PB-210 l.178E+OO 6.676E+OO 6.698E+OO NOT IDENT. BI-211 2.648E+OO 6.340E-Ol l.352E+OO FAIL ABUN PB-211 -4.126E-01 1.098E+OO l .114E+OO NOT IDENT. BI-212 1.632E+OO 9.483E-01 l.200E+OO FAIL ABUN RN-219 -l.423E-01 6.270E-01 6.303E-01 FAIL ABUN RA-223 3.427E-01 8.310E-Ol 8.453E-01 FAIL ABUN AC-227 3. 517E-02 2.973E-01 2.977E-01 FAIL ABUN TH-227 3.517E-02 2.973E-01 2.977E-01 FAIL ABUN TH-229 -3.194E-01 6.315E-01 6.477E-01 FAIL ABUN TH-231 3.427E-01 8.310E-01 8.453E-01 FAIL ABUN PA-233 -5.642E-02 I 7.815E-02 8.218E-02 FAIL ABUN PA-234 -1.635E-01 3. 925E-01 3.994E-01 NOT IDENT. PA-234M -5 .196E+OO 5.095E+OO 5.608E+OO NOT IDENT. TH-234 1.896E+OO 2. 031E+OO 2.204E+OO FAIL ABUN U-235 5.759E-02 2.464E-01 2.478E-01 FAIL ABUN NP-237 -5.642E-02 7.815E-02 8.218E-02 FAIL ABUN NP-238 -5.579E+40 5.144E+41 O.OOOE+OO SHORT HLIF U-238 1.896E+OO 2.031E+OO 2.204E+OO FAIL ABUN NP-239 1.878E-01 3.209E-01 3.319E-01 FAIL ABUN PU-239 -2.524E+Ol 4.323E+02 4.325E+02 NOT IDENT. AM-241 -3.896E-02 2.244E-01 2. 251E-01 NOT IDENT. CM-243 4.668E-02 1.317E-01 1.333E-01 FAIL ABUN BK-247 -7.946E-02 l.155E-01 1.209E-01 NOT IDENT. CM-247 . 4. 401E-03 5'. 598E-02 5.601E-02 FAIL ABUN CF-249 -4.305E-02 5.816E-02 6 .131E-02 NOT IDENT. CF-251 -7.255E-02 l.353E-01 1.392E-01 NOT IDENT. ANH-511 -3.056E-02 6.124E-02 6.277E-02 NOT IDENT. Page 3489 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 91.4849 87.09 139.2739 136.47 93.5441 45.60 82.8264 87.57 148.3922 140.51 0.0000 46.54 84.0705 88.03 154.5189 143.76 93.2419 49.72 0.0000 88.34 154.6079 144 .. 24 76.1140 51. 35 94.5186 88.47 132.8742 145.44 118.0415 51.87 110. 2482 89. 96 124.2040 152.43 107.9469 52.39 112.4799 1093.63 133.4018 153.25 0.0000 52.97 110. 5624 91.11 0.0000 323.87 103.2168 53.44 105.4741 92.59 133.8708 156.02 0.0000 54. 07. 103.5515 93.35 134. 0527 158.56 0.0000 57.36 0.0000 94.56 92.5958 159.00 116.7635 57.53 107. 6116 94.65 92.6107 162.33 91. 2813 57.98 121. 4591 94.67 92. 6138 162.66 0.0000 59.27 114.4208 94.87 92. 6461 163.33 99.7768 59.32 114.4344 97.43 114.4188 165.86 76.5332 59.54 115.5547 98.43 99.7156 176.31 83.4392 60. 96 145.7276 98.44 99.7176 176. 60 0.0000' 61.17 144.7350 99.53 101.0518 177.52 91. 2282 62.93 97.2415 100 .11 120.6917 181.07 0.0000 63.29 98.3912 102.03 110.7048 181. 52 79.6532 63.58 118. 7903 103.18 97.0526 184.41 92.8004 64.28 129.6987 103.37 92.4603 143.76 92.9355 66.73 101. 3129 105.21 89.2633 193.51 115.4266 67.24 116.5331 105.31 89.2780 197.03 114 .1199 125.81 119.8861 106.12 106. 8116 198.01 112.4944 67.75 119.9039 106.47 91.7711 201.83 106.8195 69.67 131.6160 109.28 107.3577 203.43 108.7510 70.83 121.7933 111. 00 119. 3530 205.31 91. 3883 72.81 128.8554 111. 7 6 0.0000 210.85 119. 3033 72.87 128.8716 114. 06 89.3576 215.65 103.0092 74.66 129.3515 116.30 0.0000 222.11 90.2624 74.82 129.3938 116.74 88.5469 227.09 97.8831 74.97 129.4343 119.76 86.5811 227.38 97.9097 77 .11 129.9988 121.12 78.4384 228.16 0.0000 78.74 113.4760 121.22 78.4500 228.18 93.4904 79.69 126.9782 121. 7 8 105.8769 116.74 93.4904 80 .12. 118. 2194 122.06 107. 1112 235.69 90.9882 80.19 0.0000 122.92 85.7977 235. 96 91. 0117 80.57 109.4493 123.07 85.8170 238.63 103.4934 81. 00 118. 4237 265.00 90.6657 238.98 0.0000 81. 07 118. 4399 125.81 101. 7189 240.99 133.7436 81. 75 110.0721 127.23 115.1180 242.00 133.8677 83.79 122.0399 127.91 98.4273 244.70 75.3162 84.00 122.0883 129.30 114. 2577 252.40 0.0000 85.43 135.8557 131. 2 0 121.8023 252.80 81. 8441 86.55 139.1339 133.02 96. 7249 254.15 0.0000 86.79 139.1963 133.52 102.8415 256.23 71.0243 86.94 139.2351 136.00 94.6971 260.90 0.0000 Page 3490 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 89.2012 355.39 0.0000 584.27 27.2334 264.80 89.2129 356.01 61.3036 595.83 0.0000 265.00 89.2285 364.49 0.0000 427.87 37.7346 268.22 71.7661 366.42 0.0000 602.52 0.0000 269.46 71. 8413 372. 51 70.5640 604.72 34.3689 270.03 71. 87 57 375.05 76.7422 607.14 39.5692 271.23 71.9494 377.52 61. 6962 609.32 32.1460 273.65 0.0000 356.01 54.8438 610.33 32.1608 276.40 76.9551 388.16 71. 2946 614.28 31. 0682 277.37 75.1383 388.63 0.0000 618.01 31.1210 277.60 75.1530 391. 69 58.1863 620. 36 31.1539 278.00 75.1774 264.66 57.4936 621. 93 20.7847 279.20 75.2523 401.81 71.9198 630.19 0.0000 279.54 71.9802 402.40 64.7509 631. 29 31.3077 279.70 71.9896 404.85 73.0859 633.25 18.5690 280.46 81. 9218 410.95 . 61. 9983 634.78 0.0000 283.69 67.9775 413.71 71.4202 635.95 32.5345 284.31 0.0000 414.70 0.00.00 636.99 0.0000 285.41 67.1273 423. 72 0.0000 645.85 24.5077 285.90 0.0000 427.09 70. 9620 657.76 23.9312 287.50 80.5003 427.87 64.7322 657.90 0.0000 290.67 61.2417 433.94 66.0146 661. 66 27.3208 293.27 0.0000 439.40 68.3312 664.57 0.0000 351.93 75.7589 453.88 63. 6096 666.33 0.0000 295. 96 75.8042. 463.37 71. 9508 666.50 0.0000 879.38 68.7949 468.07 66.2635 667.71 0.0000 299.98 61.6970 473.00 0.0000 677.62 20.4086 300.09 61. 7023 475.06 72; 9611 685.70 0.0000 300.13 61. 7036 476.78 64.4385 695.00 0.0000 301.36 70.3822 477.60 58.0210 696.49 22.3587 302.85 67.5869 482.18 52.7823 696.51 22.3587 256.23 57. 5952 . 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697. 3.0 21.4717 306.78 68.2742 497.08 38.0078 697.49 19.6837 308.46 56.8081 505.52 45.8153 702.65 18.6494 311. 90 61. 7852 50.7. 63 0.0000 706.68 22.9914 316.51 61.0338 511. 00 59.0762 711. 68 15.8388 319.41 0.0000 514.00 136.4188 720.70 0.0000 320.08 0.0000 514.00 136.4188 721. 93 0.0000 321.04 80.6832 520.40 36.2791 722.78 24.5877 323.87 61.3696 520.69 0.0000 722.9*1 28.9287 325.23 85.8104 522.65 0.0000 723.31 28.9336 328.76 0.0000 527.90 0.0000 724.19 24.6019 333.37 60.0333 528.26 41. 9460 727. 33 19.0178 333.97 61.8259 529 .. 59 35.3477 733.00 14.5229 334.37 61. 8439 529.87 0.0000 735.93 23.6268 338.28 61.0350 531.02 0.0000 333.97 19.0947 338.32 61. 0363 537.26 0.0000 73*9. 50 0.0000 311. 90 61.1309 546.56 0.0000 747.24 16.4301 340.48 61.1309 552.55 40.2275 748.06 13.6958 340 .. 55 0.0000 563.25 42.6866 752.31 24.6937 344.28 54.8699 569.33 42.8134 753.82 0.0000 345.93 60.5762 946.00 42.8165 756.73 18.3228 351.06 69.5372 569.70 38.3136 756.80 19.2395 351. 93 69.5785 583.19 27.2197 884.68 14.6992 Page 3491of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY* MDA COUNTS 765.81 19.1229 1274.44 12.9381 1620.50 3.7273 766.42 20.2309 . 1001. 03 17.9407 1621. 92 3.7285 766.84 20.2336 1002.74 15.9561 1678.03 0.0000 772. 60 0.0000 1004.73 10.9765 1690.97 3.7814 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9591 778.90 19.4030 1028.54 0.0000 1063.66 9.6021 783.70 0.0000 1037.84 19.1508 1771. 35 1.9208 785.37 17.5980 ' 1038.76 0.0000 1791.20 0.0000 792.07 18.5706 631.29 12.1274 1808.65 4.8364 794.95 19.5202 1048.07-0.0000 1810.72 0.0000 795.86 13.9476 1049.04 21.2384 1836.06 0. 9723 810.06 16.8250 1050.41 22.2592 810.29 15.8918 1063.66 8.1260 344.28 15.8929 1077.00 0.0000 810.76 15.8944 1077.34 13.2579 815.77 0.0000 1085.87 11. 2457 1048.07 0.0000 1093.63 13.3206 832.01 18.8440 1099.45 12.3164 834.85 18.8635 1112. 07 15.1071 835.71 23.5863 1112. 84 18. 1328 836.80 0.0000 1115. 54 9.8982 846.75 0.0000 1120.29 16.5195 846.77 20.8378 1120.55 16.5205 856.80 0.0000 1221.41 9.9141 860.56 7.6143 1129. 67 10.3516 871.09 18.1500 1131.51 0.0000 873.19 19.1193 1147.95 0.0000 875.33 0.0000 1173.23 10.4767 879.38 11.4961 1177.95 17.8332 880.51 18.2091 1189.05 12.6262* 883.24 10.5518 1204.77 16.9063 884.68 10. 9685 1221.41 18.6785 889.28 10.7659 1231.02 18. 7258 894.76 24.6539 1235.36 0.0000 898.04 9.*9166 1238.28 15.9897 900.72 15.4395 1260.41 0.0000 903.28* 12.5557 1271.87 18.2783 911.20 20.3361 1274.44 8.6074 912.08 24.7977 1274.54 8.6074 923.98 0.0000 1291.59 8.6445 926.50 15.5728 1298.22 0.0000 929 .11 16.5601 1312 .11 0.0000 937.49 15.6289 1332.49 10.9161 944 .13 0.0000 1362.66 0.0000 946.00 15.6724 1365.19 4.4011 949.00 16.9948 1368.63 0.0000 667. 71 0.0000 1384.29 6.6317 962.31 18.9053 1408.01 11.1151 964.08 26.7982 1457.56 0.0000 966 .17 0.0000 1460.82 7.2008 911. 20 12.6305 1489.16 4.5293 968. 97 12.6305 1505.03 5.4542 983.53 0.0000 1584.12 9.2476 984.45 0.0000 1596.21 0.0000 Page 3492 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:02:27.59 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM30.CNF;300 Background date : Z-OCT-2016 11:01:47. Sample date 8-DEC-2015.10:15:00. Acquisition date : 3-0CT-2016 09:01:37. Sample ID G405235026 Sample quantity : 1.55202E+02 GRAM Detector name : GAM30 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.46 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 4 4 4 4 5 5 0 0 0 5* 5 1 1 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3493 of 5809 Energy 63.60* 74.83 77.11* 84.35* 87.28 89.75 92.88* 140.12* 143.67* 164.59 186.09* 209.99 238.66* 241. 78 269.13 270.63 277.77 290.40 295.09* 300.23 307.04 338 .45* 352 .13* 412.99 486.39 511. 00* 565.29 583.49* 609.62* 648.41 661.77 723.15 727.63 764.91 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 33 152 193 31 109 59 91 28 36 20 57 29 378 80 21 42 28 19 146 32 22 91 224 29 19 22 12 130 157 19 64 12 65 4 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 153 174 156 .183 125. 96 120 52 120 126 131 150 83 96 33 42 63 24 65 52 69 49 79 9 32 59 27 33 47 20 20 10 11 15 1. 01 1.19 0.93 1. 47 1.10 1. 07 1. 49 1. 03 1. 75 1. 55 1. 05 1. 30 1. 09 1. 57 1. 21 1. 21 1. 21 1. 33 1. 37 1. 82 1. 83 1.16 1. 06 0.92 3.61 2.58 4.36 1. 67 1. 36 3.48 1. 68 1. 37 1. 67 0.56 126.92* 149.38 153.94 168.43 174.28 179.22 185.49 279.98' 287.07 328.92 371.92 419.73 477.07 483.31 538.00 541.00 555.29 580.56 589.93 600.22 613.84 676.66 704.02 825.76 972. 59 1021.81 1130. 42 1166. 83 1219.10 1296.69 1323.42 1446.22 1455.17 1529.75-124 145 145 163 163 163 163 278 . 278 320 366 414 472 472 535 535 550 578 583 596 596 672 699 823 966 1016 1122 1161 1214 1290 1318 1443 1450 1522 8 9.21E-03 68.8 14 4.23E-02 16.4 1.79E+OO 14 5.35E-02 12.7 28 8.48E-03 77.1 1.85E+OO 28 3.04E-02 19.1 28 1.65E-02 29.5 28 2.53E-02 27.8 16 7.68E-03 42.6 1.77E+OO 16 9.91E-03 62.0 11 5. 61E-03111. 0 11 l.58E-02 42.3 13 8.18E-03 89.0 25 1.05E-01 6.6 1.34E+OO 25 2.21E-02 25.9 13 5.92E-03 44.1 3.06E+OO 13 1.16E-02 31.0 9 7.70E-03 55.1 5 5.15E-03 46.5 13 4.07E-02 14.2 24 8.96E-03 45.8 1.51E+OO 24 6.08E-03 74.9 11 2.54E-02 18.3 11 6.21E-02 10.2 8 7.93E-03 26.7 11 5.29E-03 62.5 13 5.99E-03 89.1 13 3.28E-03 98.1 10 3.61E-02 12.3 13 4.37E-02 12.3 12 5.36E-03 52.3 13 l.76E-02 19.1 7 3.43E-03 53.3 14 1.80E-02 16.4 10 l.llE-03187.9 Peak Search Report (continued) Page : 2 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 767.85 23 7 1.19 1535.64 1531 9 6.44E-03 29.0 36 0 795.50 19* 28 2.00 1590.95 1582 14 5.28E-03 63.4 37 0 860.66 24 19 1. 23 1721. 31 1714 13 6.54E-03 43.8 38 0 911. 55 99 35 1. 49 1823.13 1815 14 2.75E-02 16.2 39 0 956.30 22 8 3.97 1912.65 1906 15 5.97E-03 35.2 40 0 966.07* 5 18 1. 33 1932.21 1926 10 l.48E-03164.5 41 0 969.48* 61 10 1. 64 1939.03 1935 10 1.70E-02 16.4 42 0 1015.29 7 20 3.21 2030.68 2019 16 l.85E-03155.6 43 0 1072.58 15 7 1. 22 2145.31 2140 10 4.29E-03 41. 3 44 0 1120.76* 39 17 0.87 2241. 70 2237 10 l.09E-02 26.1 45 0 1363.20 11 0 0.66 2726.82 2721 11 3.06E-03 30.2 46 0 1373.89 6 2 0.80 2748.20 2745 7 1.68E-03 54.9 47 0 1461.18* 371 0 1. 70 2922.88 2916 14 1.03E-01 5.2 48 0 1509.43 8 3 3.81 3019.44 3012 11 2.23E-03 53.6 49 0 1589.74 10 6 1. 03 3180.15 3172 12 2.78E-03 58.3 50 0 1765.19* 41 0 1. 21 3531.27 3525 13 1.14E-02 16.6 Flag: "*" = Peak area was modified by background subtraction Page 3494 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:02:29 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID , Sample type Detector name * : 8-DEC-2015 10:15:00 G405235026 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:01:37 155.20 GRAM Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA30 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 3495 of 5809 PB-214 PB-214 PB-214 PB-214' TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 279.20 74.66 74.82 74.82 351.06 CAN 0 01:00:01.46 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Nuclide Type: Uncorrected De.cay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.307E+OO 1.245E+Ol l.245E+Ol 10.48 OK NB-95 765.81 99.81* 2.266E+OO 8.910E-03 2.292E-01 375.83 OK CD-109 88.03 3.70* 6.554E+OO 1.930E+OO 3.028E+OO 57.12 OK SN-126 64.28 9.60 3.928E+OO 5.635E-01 5.636E-01 137.56 OK 86.94 8.90 6.554E+OO 8.022E-01 8.022E-01 57.12 OK 87.57 37.00* 6.554E+OO 1.930E-01 1.930E-01 57.12 OK CS-135 268.22 16.00* 4.925E+OO 1.519E-01 1.519E-01 88.27 OK BA-137M 661. 66 89.90* 2. 541E+oo. l.423E-01 1.450E-01 38 .11 OK CS-137 661. 66 85.10** 2.541E+OO 1.503E-01 1.532E-01 38 .11 OK CE-139 165.86 80.00* 6. 725E+OO 2.208E-02 l.OOOE-01 221. 95 OK HG-203 70.83 3.69 4.957E+OO Line Not Found *-----Absent 72. 87. 6.19 5.213E+00 Line Not Found Absent 279.20 81.56* 4.815E+00 1.615E-02 1.400E+00 271.55 OK TL-208 277.37 6.60 4.820E+OO Line Not Found <<INT Reject 583.19 85.00* 2.799E+OO 2.834E-01 2.834E-01 24.60 OK 860.56 12.50 2.058E+OO 4.553E-01 4.553E-01 87.56 OK PB-212 74.82 10.28 5.442E+OO l.179E+00 l.179E+OO 49.56 OK 77 .11 17.10 5.691E+OO 1.248E+OO l.248E+00 25.50 OK 238.63 43.60* 5. 357E+OO

9.204E-01 9.204E-01 13.13 OK 300.09 3.30 4.554E+00 1.192E+OO 1.192E+00 91. 66 OK BI-214 609.32 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 OK 1120.29 14.92 1.645E+OO 7.714E-01 7. 717E-01 52.15 OK 1764.49 15.30 l.121E+OO 1.092E+OO 1.093E+OO 33.24 OK PB-214 74.82 5.80 5.442E+OO Line Not Found <<INT Reject 77 .11 9.70 5. 691E+OO 2.200E+OO 2.201E+OO 25.50 OK 87.09 3.41 6.542E+00 Line Not Found <<INT Reject 242.00 7.25 5.305E+OO Line Not Found <<INT Reject 295.22 18.42 4. 611E+OO 9. 588E-01. 9.591E-01 28.38 OK 351.93 35.60* 4.059E+OO 8.465E-01 8.468E-01 20.43 OK RN-222 609.32 45.49* 2.707E+00 6.600E-01 6.602E-01 24.57 OK 1120.29 14.92 1.645E+OO 7. 714E-01 7.717E-01 52.15 OK 1764.49 15.30 L 121E+OO 1.092E+OO 1.093E+OO 33.24 OK RA-224 240.99 4.10* 5.309E+OO 3.817E-01 3.817E-01 308.85 OK RA-226 609.32 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 OK 1120.29 14.92 1.645E+OO 7. 714E-01 7. 717E-01 52.15 OK 1764.49 15.30 l.121E+OO 1.092E+OO 1.093E+OO 33.24 OK AC-228 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 1.064E+00 1.064E+OO 36.57 OK 794.95 4.25 2.196E+OO 1.021E+OO l.021E+OO 126.75 OK. 835.71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 OK 968. 97 15.80 1. 863E+OO 1.019E+OO 1.019E+OO 32.73 OK RA-228 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 OK 794.95 4.25 2 .196E+OO 1.021E+OO 1.021E+OO 126.75 OK 835.71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 OK 968. 97 15.80 1.863E+OO 1.019E+OO 1.019E+OO 32.73 OK TH-228 74.82 10.28 5.442E+OO 1.179E+OO l.179E+OO 49.56 OK Page 3496 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Nuclide Type: ' Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 17.10 5.691E+OO 1.248E+OO 1.248E+OO 25.50 OK 238.63 43.60* 5.357E+OO 9.204E-01 9.204E-01 13 .13 OK 300.09 3.30 4.554E+OO 1.192E+OO 1.192E+OO 91. 66 OK TH-229 85.43 14.70 6.345E+OO 2.049E-01 2.049E-01 154.20 OK 88.47 24.00 6.554E+OO 2.975E-01 2.975E-01 57.12 OK 193.51 4.41* 6.145E+OO Line Not Found Absent 210.85 2.80 5.837E+OO 1.036E+OO 1.036E+OO 177.94 OK TH-230 609.32 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 OK 1120.29 14.92 1. 645E+OO 7. 714E-01 7. 714E-01 52.15 OK 1764.49 15.30 1.121E+OO 1.092E;+OO 1.092E+OO 33.24 OK PA-231 283.69 1. 70 4.743E+OO Line Not Found Absent 301.36 5.35* 4.554E+OO 7.353E-01 7.353E-01 91. 66 OK TH-232 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911. 20 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 OK 968. 97 15.80 1.863E+OO 1.019E+OO 1.019E+OO 32.73 OK TH-234 63.29 3.70* 3.928E+OO 1.462E+OO 1. 462E+OO 137.56 OK 92'. 59 4.23 6.875E+OO 1.939E+OO 1. 939E4-00 55.61 OK U-234 609.32 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 OK 1120.29 14.92 l.645E+OO 7.714E-01 7.714E-01 52.15 OK 1764.49 15.30 1.121E+OO 1.092E+OO 1.092E+OO 33.24 OK U-235 89. 96 3.47 6.708E+OO 1.584E+OO l.584E+00 58.92 OK 93.35 5.60 6.875E+OO 1.465E+OO 1.465E+OO 55.61 OK 143.76 10. 96* 7.122E+OO 2.726E-01 2.726E-01 123.99 OK 163.33 5.08 6.725E+OO 3.477E-01 3.477E-01 221.95 OK 185.72 57.20 6.291E+OO 9.212E-02 9.212E-02 84.53 OK 205.31 5.01 5.922E+00 Line Not Found Absent U-238 63.29 3.70* 3.928E+OO 1.462E+OO l.462E+OO 137.56' OK 92.59 4.23 6.875E+OO 1.939E+OO . 1. 939E+00 55.61 OK AM-243 43.53 5.90 8.765E-01 Line Not Found Absent 74.66 67.20* 5.442E+OO 1.804E-01 l.804E-01 49.56 OK 511. 00 100.00* 3. 091E+06 3.668E-02 3.668E-02 178.21 OK Flag: "*" = Keyline Page 3497 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:02:30.67 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l *
Acquisition date 3-0CT-2016 09:01:37 Sensitivity : 3.DOO *
Detector ID GAM30 Energy tolerance: 1.500 * *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: . 0 01:00:01.46 Half life ratio : ***** *
Sample date 8-DEC-2015 10:15:00 Analyst initials: MXRl *
Sample ID G405235026 Sample Quantity l.5520E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date . : ll-MAR-2016 05: 58: 49 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM30
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.245E+Ol 1.278E+OO NB-95 2.292E-01 8.440E-01 CD-109 3.028E+OO 1.695E+OO SN-126 1.930E-01 1.080E-01 CS-135 l.519E-01 l.314E-01 BA-137M l.450E-01 5.415E-02 CS-137 1.532E-01 5.720E-02 CE-139 1.000E-01 2.175E-01 HG-203 l.400E+00 3. 727'E+OO TL-208 2.834E-01 6.830E-02 PB-212 9.204E-01 l.185E-01 BI-214 6.602E-01 1.590E-01 PB-214 8.468E-01 l.695E-01 RN-222 6.602E-01 1.590E-01 RA-224 3.817E-01 1.155E+00 RA-226 6.602E-01 1.590E-01 AC-228 9.663E-01 3.064E-01 RA-228 9.663E-01 3.064E-01 TH-228 9.204E-01 l.185E-01 TH-229 -2.684E-01 4.158E-01 TH-230 6.600E-01 1. 589E-01 PA-231 7.353E-01 6.605E-01 TH-232 9.663E-01 3.064E-01 TH-234 1.462E+OO 1.971E+OO U-234 6.600E-01 1. 58 9E-01 U-235 2.726E-01 3.313E-01 U-238 1.462E+OO 1. 971E+OO AM-243 l.804E-01 8.762E-02 ANH-511 3.668E-02 6.406E-02 Non-Identified Nuclides Nuclide BE-7 Page 3498 of 5809 Key-Line Activity (pCi/GRAM -4.614E+OO K.L. Cnt Uncert ( 1. 96-sigma) 8.882E+OO MDA (pCi/GRAM 3.163E-01 l.532E-01 1.577E+OO l.009E-01 2.124E-01 4. 720E-02 4.986E-02 1.662E-01 4.277E+OO 5.062E-02 8.444E-02 9.413E-02 l.073E-01 9. 413E-02 9.046E-01 9.413E-02 1. 963E-01 1. 963E-01 8.444E-02 7. 241E-01 9.409E-02 5.885E-01 1.963E-01 1.588E+OO 9. 409E-0'2 2.892E-01 1.588E+OO 6.903E-02 4.362E-02 MDA (pCi/GRAM 1.663E+Ol NOT IDENT.

NA-22 1.327E-02 3.109E-02 7.054E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+4.l O.OOOE+OO SHORT HLIF AL-26 1.336E-02 2.580E-02 6.224E-02 NOT IDENT. SC-46 8.247E-02 2.832E-01 5.857E-01 FAIL ABUN V-48 O.OOOE+OO l.349E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 3.244E+02 O.OOOE+OO SHORT HLIF MN-54 4.931E-03 4.362E-02 8.809E-02 NOT IDENT. C0-56 6.270E-02 3.105E-01 6.442E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 9.927E-03 3.585E-02 7.029E-02 NOT IDENT. C0-58 2. 969E-01 4.248E-01 9.347E-01 NOT IDENT. FE-59 -l.656E-01 5.760E+00 1. 096E+Ol NOT IDENT. C0-60 -2.654E-02 2.919E-02 4.943E-02 NOT IDENT. ZN-65 -1.207E-01 1.907E-01 2.716E-01 NOT IDENT. GE-68 1.598E-Ol 1.561E+OO 3.032E+OO NOT IDENT. AS-73 1.152E+OO 5.597E+OO 1.145E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.379E+03 O.OOOE+OO SHORT HLIF SE-75 -1.264E-01 l.845E-01 3 .115E--:Ol NOT IDENT. BR-77 O.OOOE+OO 2.207E+37 0. OOOE+OO. SHORT HLIF SR-82 O.OOOE+OO 5.523E+02 0.000E+OO SHORT HLIF RB-83 -3.046E-01 5.354E-01 9.842E-01 NOT IDENT. KR-85 1.452E+OO 6.449E+OO 1.169E+Ol NOT IDENT. SR-85 l.519E-01 6.820E-01 1.236E+OO NOT IDENT. RB-86 O.OOOE+OO 1.887E+04 O.OOOE+OO SHORT HLIF Y-88 -4.737E-02 l.700E-01 3.548E-01 NOT IDENT. Y-91 3.774E+Ol 4.010E+02 7.854E+02 NOT IDENT. NB-94 1.287E-02 2.468E-02 5 .133E-02 NOT IDENT. NB-95M -1.045E+OO 2.239E+OO 3.605E+OO NOT IDENT. ZR-95 -7.945E-01 1.065E+OO 1. 829E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.434E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.054E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 8.347E+40 O.OOOE+OO SHORT HLIF *RH-101 -2.137E-02 2.686E-02 4.761E-02 NOT IDENT. RH-102 3.756E-02 4.175E-02 9.383E-02 FAIL ABUN RU-103 -2.637E+00 3.888E+OO 7.093E+OO FAIL ABUN RH-106 3.137E-01 3.596E-01 8.013E-01 NOT IDENT. RU-106 3.137E-01 3.596E-01 8.013E-01 NOT IDENT. AG-108M 5.223E-04 1.928E-02 3:910E-02 FAIL ABUN AG-llOM -2.162E-02 7.255E-02 1.353E-01 FAIL ABUN SN-113 -7.688E-02 l.636E-01 3.126E-01 NOT IDENT. CD-115 O.OOOE+OO 2.473E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.694E+04 O.OOOE+OO SHORT HLIF TE-123M -5.563E-02 l.164E-01 l.911E-01 NOT IDENT. SB-124 -5.007E-01 1. 075E+OO 2 .113E+OO FAIL ABUN SB-125 -3.335E-03 7.016E-02 1.414E-01 NOT IDENT. TE-125M. 1.695E+02 2.106E+02 4.239E+02 NOT IDENT. I-126 O.OOOE+OO 7.471E+05 0. OOOE+OO_ SHORT HLIF SB-126 O.OOOE+OO l.062E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.328E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.850E+09 O.OOOE+OO SHORT HLIF I-132 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 0. OOOE-fOO 3.058E+26 O.OOOE+OO SHORT HLIF BA-133 -l.023E-02 3.653E-02 6.349E-02 FAIL ABUN I-133 O.OOOE+OO 1.294E+41 O.OOOE+OO SHORT HLIF CS-134 6.688E-02 8.308E-02 9.467E-02 FAIL ABUN I-135 0.000E+OO l.057E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.083E+05 O.OOOE+OO SHORT HLIF BA-140 O.OOOE+OO 9.168E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2. 511E+05 O.OOOE+OO SHORT HLIF CE-141 1.269E+OO 2 .115E+Ol 3.988E+Ol NOT IDENT. CE-143 O.OOOE+OO 7. 451E+40 O.OOOE+OO SHORT HLIF CE-144 -2.300E-01 2.824E-01 4.997E-01 NOT IDENT. PM-144 -2.303E-02 4.145E-02 7.676E-02 NOT IDENT. PR-144 -2. 013E+OO 3.599E+OO 6.661E+OO NOT IDENT. PM-146 6.808E-03 3.24SE-02 6.656E-02 NOT IDENT. ND-147 O.OOOE+OO 2.604E+07 O.OOOE+OO SHORT HLIF PM-147 -5.319E+02 6.518E+02 1.157E+03 NOT IDENT. PM-149 O.OOOE+OO 4. 001E+40 O.OOOE+OO SHORT HLIF EU-150 1.286E-02 1. 963E-02 3.896E-02 FAIL ABUN EU-152 -9.259E-02 6.418E-02 1. 08 6E-01 NOT IDENT. GD-153 -2.272E-01 l.255E-01 2.007E-Ol NOT IDENT. EU-154 3.051E-02 7.569E-02 1. 714E-01 FAIL ABUN EU-155 8.181E-02 7.943E-02 l.657E-01 FAIL ABUN TB-160 l.600E-01 l.668E+OO 3.253E+OO FAIL ABUN H0-166M -2.302E-02 4.155E-02 7.466E-02 NOT IDENT. TM-171 -6. 472E+00 1.393E+Ol 2.693E+Ol NOT IDENT. 72 -8.490E-03 l.795E-01 3.407E-01 FAIL ABUN Page 3499 of 5809 LU-172 1. 469E-03 7.094E-02 1.347E-01 FAIL ABUN LU-176 2.891E-02 4.244E-02 4.162E-02 FAIL ABUN HF-181 1.970E+00 3.380E+OO 6.703E+OO* NOT IDENT. TA-182 -4.880E-01 6.779E-01. 1.222E+00 FAIL ABUN RE-183 -8.280E-01 2.007E+OO 3. 871E+OO NOT IDENT. RE-184 -1.644E+Ol 2.388E+Ol 4.063E+Ol NOT IDENT. W-188 1.085E+02 9.881E+Ol 1. 811E+02 FAIL ABUN IR-192 -8.973E-02 3.174E-01 6.287E-01 FAIL ABUN BI-207 -4.942E-03 3.758E-02 7.097E-02 FAIL ABUN PB-210 8.066E-01 1.978E+OO 4.133E+OO NOT IDENT. BI-211 O.OOOE+OO 4.669E-01 6.745E-01 *FAIL ABUN PB-211 2.926E-02 4.865E-01 9.838E-01 NOT IDENT. BI-212 O.OOOE+OO 6.702E-01 l.233E+OO FAIL ABUN RN-219 6.479E-02 2.920E-01 5.973E-01 FAIL ABUN RA-223 -5.056E-02 4.lOlE-01 8. 231E-01 FAIL ABUN AC-227 9.580E-03 2.097E-01 3.847E-01 FAIL ABUN TH-227 9.580E-03 2.097E-01 3.847E-01 FAIL ABUN TH-231 -5.056E-02 4.lOlE-01 8.231E-01 FAIL ABUN PA-233 -2.204E-02 4.683E-02 8.043E-02 FAIL ABUN PA-234 -1. 747E-01 2.018E-01 3.248E-01 NOT IDENT. PA-234M 1.140E+OO 2.777E+OO 5.945E+OO FAIL ABUN NP-237 -2.204E-02 4.683E-02 8.043E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1.059E-01 1.852E-01 3. 714E-01 FAIL ABUN PU-239 -8.761E+OO 2.558E+02 4.846E+02 FAIL ABUN AM-241 2.073E-02 9.276E-02 1.876E-01 NOT IDENT. CM-243 -2.230E-02 7.324E-02 l.378E-01 FAIL ABUN BK-247 -3.012E-02 6.189E-02 1. 072E-01 FAIL ABUN CM-247 4.372E-03 2.660E-02 5.413E-02 FAIL ABUN CF-249 2.169E-02 2.702E-02 5.900E-02 NOT IDENT. CF*-251 -7.413E-02 9. 965E-02 1. 731E-01 NOT IDENT. Page 3500 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:02:28.38 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 359 10.66* 1.307E+OO 1.245E+Ol 1.245E+Ol 10.48 NB-95 765.81 4 99.81* 2.266E+OO 8.910E-03 2.292E-01 375.83 CD-109 88.03 141 3.70* 6.554E+OO 2.813E+OO 4.415E+OO 38.15 SN-126 64.28 44 9.60 3.928E+OO 5.635E-01 5.636E-01 137.56 86.94 141 8.90 6.554E+OO 1. l 70E+OO 1.170E+OO 38.15 87.57 141 37.00* 6.554E+OO 2.813E-01 2.813E-01 38.15 CS-135 268.22 25 16.00* 4.925E+OO

1. 519E-01 1.519E-01 88.27 BA-137M 661.66 67 89.90* 2.541E+OO 1.423E-01 l.450E-01 38 .11 CS-137 661.66 67 85.10* 2. 541E+OO l.503E-01 l.532E-01 38 .11 CE-139 165.86 25 80.00* 6.725E+OO 2.208E-02 1.000E-01 221. 95 HG-203 70.83 ------3.69 4.957E+OO ------Line Not Found ------72.87 ------6.19 5.213E+OO ------Line Not Found ------279.20 32 81.56* 4.815E+OO 3.425E+OO 110 .14 TL-2*08 277.37 32 6.60 4.815E+OO 4.880E-01 4.880E-01 110 .14 583.19 139 85.00* 2.834E-01 2.834E-01 24.60 860.56 '24 12.50 2.058E+OO 4.553E-01 4. 553E..'.Ol 87.56 BI-211 72.87 ------1.23 5. 213E+OO ------Line Not Found ------351.06 253 12.92* 4.059E+OO 2.332E+OO 2.332E+OO 20.43 PB-212 74.82 199 10.28 5.442E+OO 1. 720E+OO 1. 720E+OO 32'. 78 77 .11 251 17.10 5. 691E+OO 1. 248E+.00 1.248E+OO 25.50 238.63 444 43.60* 5.357E+OO 9.204E-01 9.204E-01 13.13 300.09 37 3.30 4.554E+OO 1.192E+OO 1.192E+OO 91. 66 BI-214 609.32 168 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 1120.29 39 14.92 1.645E+OO 7.714E-01' 7.717E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO 1.093E+OO 33.24 PB-214 74.82 199 5.80 5.442E+OO 3.049E+OO 3.050E+OO *32. 78 77 .11 251 9.70 5.691E+OO 2.200E+OO 2.201E+OO 25.50 87.09' 141 3.41 6.554E+OO 3.052E+OO 3.054E+OO 38.15 242.00 93 7.25 5.309E+OO 1.175E+OO 1. 17 5E+OO 51. 81 295.22 168 18.42 4. 611E+OO 9.588E-01 9.591E-01 28.38 351. 93 253 35.60* 4.059E+OO 8.465E-01 8.468E-01 20.43 RN-222 609.32 168 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 1120.29 39 14.92 1.645E+OO 7.714E-01 7.717E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO l.093E+OO 33.24 RA-224 240.99 93 4.10* 5.309E+OO 2.077E+OO 2.077E+OO 51. 81 RA-226 609.32 168 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 1120.29 39 14.92 1. 645E+OO 7. 714E-01 7. 717E-01 52.15 1764.49 39 15.30 l .121E+OO. 1.092E+OO 1.093E+OO 33.24 AC-228 105.21 ------1.10' 7.278E+OO ------Line Not Found ------338.32 104 11.27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 794.95 20 4.25 2 .1.96E+OO 1.021E+OO 1. 021E+OO 126.75 835. 71 ------1. 61 2.109E+OO ------Line Not Found ------911.20 101 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 968. 97 62 15.80 1.863E+OO 1.019E+OO l.019E+OO 32.73 RA-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 104 11. 27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 794.95 20 4.25 2 .196E+OO 1.021E+OO 1. 021E+OO 126.75 Page 3501 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911.20 101 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 968. 97 62 15.80 1.863E+OO 1.019E+OO l.019E+OO 32.73 TH-228 74.82 199 10*. 28 5.442E+OO 1. 720E+OO 1. 720E+OO 32.78 77 .11 251 17.10 5.691E+OO l.248E+OO 1.248E+00 25.50 238.63 444 43.60* 5.357E+OO 9.204E-01 9.204E-01 13.13 300.09 37 3.30 4.554E+OO l.192E+OO 1.192E+OO 91.66 TH-229 85.43 40 14.70 6.345E+OO 2.049E-01 2.049E-01 154.20 88.47 141 24.00 6.554E+OO 4.337E-01 4.337E-01 38.15 193.51 ------4.41* 6.145E+OO ------Line Not Found* ------210.85 35 2.80 5.837E+OO 1.036E+OO l.036E+00 177. 94 .TH-230 609.32 168 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 1120.29 39 14.92 1.645E+OO 7.714E-01 7. 714E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO 1.092E+OO 33.24 PA-231 283.69 ------1. 70 4.743E+OO ------Line Not Found ------301.36 37 5.35* 4.554E+OO 7.353E-01 7.353E-01 91.66 TH-232 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 104 11.27 4.177E+OO 1. 064E+00 1.064E+OO 36.57 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911.20 101 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 968. 97 62 15.80 l.863E+00 1.019E+OO 1.019E+OO 32.73 TH-234 63.29 44 3.70* 3.928E+00 1.462E+OO 1.462E+OO 137.56 92.59 117 4.23 6.875E+OO 1.939E+OO l.939E+OO 55.61 U-234 609.32 168 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 1120.29 39 14.92 1.645E+OO 7.714E-01 7. 714E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO 1.092E+OO 33.24 U-235 89. 96 76 3.47 6.708E+OO 1.584E+OO 1.584E+OO 58.92 93.35 117 5.60 6.875E+OO 1.465E+OO l.465E+00 55.61 143.76 44 10. 96* 7.122E+OO 2.726E-01 2.726E-01 123.99 163.33 25 5.08 6. 725E+OO 3.477E-01 3.477E-01 221.95 185.72 69 57.20 6.291E+OO 9.212E-02 9.212E-02 84.53 205.31 ------5.01 5.922E+00 ------Line Not Found ------U-238 63.29 44 3.70* 3.928E+OO l.462E+OO 1.462E+OO 137.56 92.59 117 4.23 6.875E+OO 1.939E+OO 1.939E+OO 55.61 AM-243 43.53 ------5.90 *8.765E-01 ------Line Not Found ------74.66 199 67.20* 5.442E+OO 2. 631E-01 2. 632E-01' 32.78 ANH-511 511. 00 23 100.00* 3.091E+00 3.668E-02 3.668E-02 178.21 Flag: "*" Key line Page 3502 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Total number of lines in spectrum 50 Number of unidentified lines 8 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 NB-95 CD-109 SN-126 CS-135 BA-137M CS-137 CE-139 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232. TH-234 U-234
U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 64.03D 461.400 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 137.640 46.590 l.41E+lOY 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600. OOY 1.41E+10Y 1.41E+10Y l.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 25.7 1. 57 1. 00 1. 00 1. 02 1. 02 4.53 86.7 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.245E+Ol 8.910E-03 2.813E+00 2.813E-01 l.519E-01 1.423E-01 1.503E-01 2.208E-02 3.949E-02 2.834E-01 2.332E+OO 9.204E-01 6.600E-01 8.465E-01 6.600E-01 2.077E+00 6.600E-01 9.663E-01 9.663E-01 9.204E-01 4.337E-01 6.600E-01 7.353E-01 9.663E-01 1.462E+OO 6.600E-01 2.726E-01 l.462E+OO 2.631E-01 3.668E-02 3.430E+Ol 3.430E+Ol Decay Corr pCi/GRAM 1.245E+Ol 2.292E-01 4.415E+OO 2.813E-Ol 1.519E-01 1.450E-01 1.532E-01 1.000E-01 3.425E+OO 2.834E-01 2.332E+OO 9.204E-01 6.602E-01 8.468E-01 6.602E-01 2.077E+OO 6.602E-01 9.663E-01 9.663E-01 9.204E-01 4.337E-01 6.600E-01 7.353E-01 9.663E-01 1.462E+OO 6.600E-01 2.726E-01 l.462E+OO 2.632E-01 3.668E-02 3.959E+Ol 3.959E+Ol 84.00% Decay Corr 2-Sigma Error 0.130E+Ol 8.613E-01 1. 684E+OO l.073E-01 1.341E-01 0.553E-01 0. 584E-01 2.220E-01 3.772E+OO 0.697E-01 0.476E+OO 1.209E-01 l.622E-01 1.730E-01 l.622E-01 1. 076E+OO l.622E-01 3.127E-01 3.127E-01 l.209E-01 1.655E-01 1.622E-01 6.740E-01 3.127E-01 2. OllE+OO l.622E-01 3.380E-01 2. OllE+OO 0.863E-01 6.537E-02 "M" Manually accepted 2-Sigma %Error 10'.48 375.83 38.15 38.15 88.27 38 .11 38 .11 221.95 110 .14 24.60 20.43 13.13 2*4. 57 20.43 24.57 51. 81 24.57 32.35 32.35 13.13 38.15 24.57 91. 66 32.35 137.56 24.57 123.99 137.56 32.78 178.21 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3503 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235026 Acquisition date : 3-0CT-2016 09:01:37 It Energy Area Bkgn'd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 140.12 34 65 1. 03 279.98 278 16 7.68E-03 85.2 *7 .18E+OO T 1 270.63 48 49 1. 21 541.00 535 13 1.16E-02 62 .1 4.91E+OO T 0 290.40 21 28 1. 33 580.56 578 5 5.15E-03 92.9 4.66E+OO T 4 307.04 25 79 1. 83 613.84 596 24 6.08E-03 **** 4.48E+OO T 0 412.99 32 10 0.92 825.76 823 8 7. 93E-03* 53.3 3.61E+00 T 0 486.39 21 35 3.61 972.59 966 11 5.29E-03 **** 3.21E+OO T 0 565.29 13 29 4.36 1130.42" 1122 13 3.28E-03 **** 2.87E+00 0 648.41 20 21 3.48 1296.69 1290 12 5.36E-03 **** 2.58E+OO 0 723.15 13 10 1. 37 1446.22 1443 7 3.43E-03 **** 2.37E+OO T 0 727. 63 68 12 1. 67 1455.17 1450 14 1.80E-02 32.8 2.36E+OO T 0 767.85 24 7 1.19 1535.64 1531 9 6.44E-03 58.0 2.26E+OO T 0 956". 30 22 8 3.97 1912.65 1906 15 5.97E-03 70.3 1. 88E+OO 0 966. 07 5 18 1. 33 1932.21 1926 10 1.48E-03 **** 1.87E+OO T 0 1015.29 7 21 3.21 2030.68 2019 16 1.85E-03 **** 1. 79E+OO 0 1072. 58 16 7 1.22 2145.31 2140 10 4.29E-03 82.6 1. 71E+OO 0 1363.20 11 0 0.66 2726.82 2721 11 3.06E-03 60.3 1.39E+OO T 0 1373.89 6 2 0.80 2748.20 2745 7 l.68E_:03 **** 1.38E+OO 0 1509.43 8 3 3.81 3019.44 3012 11 2.23E-03 **** l.27E+OO 0 1589.74 10 6 1. 03 3180.15 3172 12 2.78E-03 **** 1. 22E+00 Flags: "T" Tentatively associated ( Page 3504 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:02:42.32 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l *
Acquisition date 3-0CT-2016 09:01:37 Sensitivity 3.000 *
Detector ID GAM30 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01: 00: 01. 46 Half life ra.tio : ***** *
Sample date 8-DEC-2015 10:15:00 Nuclide Library : SOLID *
Sample ID G405235026 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.5520E+02 GRAM * **Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 11-MAR-2016*05:58:49 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;?
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-95 CD-109 SN-126 CS-135 BA-137M CS-137 CE-139 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 tc (pCi/GRAM 1.108E-01 O.OOOE+OO 7.432E-01 4.756E-02 9. 751E-02 2.060E-02 2.176E-02 7.722E-02 1.987E+OO 2.248E-02 3.927E-02 4.159E-02 4.891E-02 4.159E-02 4.208E-01 4.159E-02 8.499E-02 8.499E-02 3.927E-02 3.365E-01 4.158E-02 2.660E-01 8.499E-02 .7.444E-01 4.158E-02 l.357E-01 7.444E-01 3.258E-02 1. 962E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3505 of 5809 Le (pCi/GRAM 7.320E+OO NOT IDENT. 2.967E-02 NOT IDENT.

NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR.,-85 RB-86 Y-88 Y-91 NB-94 NB-95M ZR-95 NB-97 ', ZR-97

M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3506 of 5809 O.OOOE+OO 2.515E-02 2.530E-01 O.OOOE+OO O.OOOE+OO 3.787E-02 2.747E-01 O.OOOE+OO 3.276E-02 4.088E-01 4.727E+OO 1. 951E-02 l.172E-01 1.255E+OO 5.324E+OO O.OOOE+OO 1.425E-01 O.OOOE+OO O.OOOE+OO 4.371E-01 5. 311E+oo* 5.615E-01 O.OOOE+OO 1.348E-01 3.351E+02 2.289E-02 l.670E+00 7.756E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.214E-02 4.160E-02 3.075E+OO 3.562E-01 3.562E-01 1.739E-02 5.716E-02 l.393E-01 O.OOOE+OO O.OOOE+OO 8.863E-02 6.794E-01 6.271E-02 1.987E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.886E-02 0.000E+OO 4.264E-02 O.OOOE+OO 0.000E+OO O.OOOE+OO 0.-000E+OO 1.872E+Ol O.OOOE+OO 2.319E-01 3.348E-02 2.904E+OO 2.985E-02 O.OOOE+OO 5.373E+02 O.OOOE+OO 1.777E-02 4.778E-02 9.219E-02 7 .196E-02 7.769E-02 1.432E+OO 3.216E-02 1.250E+Ol 1.590E-01 5.883E-02 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN' SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAILABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT. HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT !DENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 .PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3507 of 5809 l.918E-02 2.999E+OO 5.123E-01 1. 802E+OO 1. 716E+Ol 8.333E+Ol 2.828E-01 3.022E-02 l.928E+OO 3.244E-01 4.428E-01 5.742E-01 2.707E-01 3.718E-01 1. 781E-01 l.781E-01 3.718E-01 3.620E-02 l.332E-01 2.535E+OO 3.620E-02 O.OOOE+Oci 1.738E-01 2. 272E+02 8.774E-02 6.415E-02 4.899E-02 2.450E-02 2.676E-02 8.032E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:02:47.56 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l *
Acquisition date 3-0CT-2016 09:01:37 Sensitivity : 3.000 *
Detector ID GAM30 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
Sample date 8-DEC-2015 10:15:00 Nuclide Library : SOLID *
Sample ID G405235026 Analyst initials: MXRl *
Batch Number *1596249 Sample Quantity 1. 5520E+02 GRAM *
Quantity Err(%) 1.2886E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
Combined Ac.tivity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.245E+Ol 1.693E+OO NB-95 2.292E-01 8.443E-01 CD-109 3.028E+OO 1.733E+OO SN-126 1.930E-01 1.099E-01 CS-135 1.519E-01 l.322E-01 BA-137M l.450E-01 5.533E-02 CS-137 1.532E-01 5.845E-02 CE-139 1.000E-01 2.185E-01 HG-203 1.397E+OO 3.740E+OO TL-208 2.834E-01 7.214E-02 PB-212 9.204E-01 l.404E-01 BI-214 6.602E-01 1.678E-01 PB-214 8.468E-01 1.834E.,..01 RN-222 6.602E-01 1.678E-01 RA-224 3.817E-01 l.172E+OO RA-226 6.602E-01 l.678E-01 AC-228 9.663E-01 3.348E-01 RA-228 9.663E-01 3.348E-01 TH-228 9.204E-01 1.404E-01 TH-229 -2.684E-01 4.162E-01 TH-230 6.600E-01 1.677E-01 PA-231 7.353E-01 6.809E-01 TH-232 9.663E-01 3.348E-01 TH-2-34 1. 462E+OO 1.998E+OO U-234 6.600E-01 1.677E-01 U-235 2.726E-01 .3. 319E-01 U-238 l.462E+OO l.998E+OO AM-243 . 1. 804E-01 8.950E-02 ANH-511 3.668E-02 6.413E-02 Non-Identified Nuclides Nuclide BE-7 Page 3508 of 5809 Key-Line Activity (pCi/GRAM -4.614E+00 K.L Act error ( 1. 96-sigma) 8.891E+OO TPU ( 1. 96-sigma) 1.693E+OO 8.443E-01 1.733E+OO l.099E-01 1'. 322E-01 5.533E-02 5.845E-02 2.185E-01 3.740E+00 7.214E-02 l.404E-01 l.678E-01 l.834E-01 1.678E-01 l .172E+OO l.678E-01 3.348E-01 3.348E-01 l.404E-01 4.162E-01 1.677E-01 6.809E-01 3.348E-01 l.998E+OO 1.677E-01 3.319E-01 *1.998E+OO 8.950E-02 6.413E-02 TPU ( 1. 96-sigma) 9.131E+00 NOT IDENT.

NA-22 1. 327E-02 3 .111E-02 3.168E-02 NOT IDENT. NA-24 -l.OOOE+41 9.771E+41 0.000E+OO SHORT HLIF AL-26 l.336E-02 2.581E-02 2. 651E-02 NOT IDENT. SC-46 8.247E-02 2.834E-01 2.858E-01 FAIL ABUN V-48 l.525E+03 l.349E+04 1. 351E+04 SHORT HLIF CR-51 2.408E+02 3.250E+02 3.427E+02 SHORT HLIF MN-54 4.931E-03 4.363E-02 4.368E-02 NOT IDENT. C0-56 6.270E-02 3.106E-01 3 .119E...:.01 NOT IDENT. MN-56 l.OOOE+41 4.953E+41 0.000E+OO SHORT HLIF C0-57 9.927E-03 3.586E-02 3.614E-02 NOT IDENT. C0-58 2. 969E-01 4.260E-01 4.466E-01 NOT IDENT. FE-59 -l.656E-01 5.760E+OO 5.761E+OO NOT IDENT. C0-60 -2.654E-02 2.927E-02 3.163E-02 NOT IDENT. ZN-65 -1. 207E-01 l.922E-01 l.997E-01 NOT IDENT. GE-68 l.598E-01 l.561E+OO l.563E+OO NOT IDENT. AS-73 l.152E+00 5.602E+OO 5.626E+OO NOT IDENT. AS-74 -4.053E+02 4.379E+03 4.383E+03 SHORT HLIF SE-75 -1. 2 64E-01 l.848E-01 l.934E-01 NOT IDENT. BR-77 l.715E+38 l.485E+39 O.OOOE+OO SHORT HLIF SR-82 -2.361E+02 5.529E+02 5.630E+02 SHORT HLIF RB-83 -3.046E-01 5.375E-01 5.548E-01 NOT IDENT. KR-85 l.452E+00 6.450E+OO 6.483E+OO NOT SR-85 l.519E-01 6.821E-01 6.856E-01 NOT IDENT. RB-86 l.932E+03 l.887E+04 l.889E+04 SHORT HLIF Y-88 -4.737E-02 1. 701E-01 1. 714E-01 NOT IDENT. Y-91 3.774E+Ol 4.010E+02 4.013E+02 NOT IDENT. NB-94 l.287E-02 2.471E-02 2.538E-02 NOT IDENT. * 'NB-95M -l.045E+OO 2. 241E+OO 2.290E+OO NOT IDENT. ZR-95 -7.945E-01 l.067E+OO l.126E+OO FAIL ABUN. NB-97 1. 000E+41 9.568E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 l.437E+41 O.OOOE+OO SHORT HLIF M0-99 7.43iE+31 l.057E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 8.421E+40 O.OOOE+OO SHORT HLIF RH-101 -2 .137E-02 2.716E-02 2.882E-02 NOT IDENT. RH-102 3.756E-02 4.194E-02 4.523E-02 FAIL ABUN RU-103 -2.637E+OO 3.895E+OO 4. 072E+OO FAIL ABUN RH-106 3.137E-01 3.607E-'01 ;3.875E-01 NOT IDENT. RU-106 3.137E-01 3.607E-01 3.875E-01 NOT IDENT. AG-108M 5.223E-04 1;928E-02 l.928E-02 FAIL ABUN AG-110M -2.162E-02 7.261E-02 7.326E-02 FAIL ABUN

SN-113 -7.688E-02 l.637E-01 l.673E-01 NOT IDENT. CD-115 -l.509E+38 2.473E+39 O.OOOE+OO SHORT HLIF SN-117M -3.098E+04 8.704E+04 8.815E+04 SHORT HLIF TE-123M -5.563E-02 l.165E-01 l.191E-01 NOT IDENT. SB-124 -5.007E-01 1. 076E+OO l.099E+OO FAIL ABUN SB-125 -3.335E-03 7.016E-02 7.018E-02 NOT IDENT. TE-125M l.695E+02 2.110E+02 2.244E+02 NOT IDENT. I-126 -5.215E+05 7.512E+05 7. 871E+05 SHORT HLIF SB-126 2.268E+05 l.063E+06 l.068E+06 SHORT HLIF SB-127 3.067E+21 1. 394E+22 O.OOOE+OO SHORT HLIF I-131 -l.018E+09 3. 851E+09 3.879E+09 SHORT HLIF I-132 -1. OOOE+41 l.892E+42 O.OOOE+OO SHORT HLIF TE-132 -l.218E+26 3.099E+26 O.OOOE+OO SHORT HLIF BA-133 -l.023E-02 3.653E-02 3.682E-02 FAIL ABUN I-133 l.OOOE+41 2.226E+41 O.OOOE+OO SHORT HLIF CS-134 6.688E-02 8.339E-02 8.867E-02 FAIL ABUN I-135 -l.OOOE+41 6.860E+41 O.OOOE+CiO SHORT HLIF CS-136 -3.178E+04 2.084E+05 2.089E+05 SHORT HLIF BA-140 8.059E+05 9.192E+05 9.884E+05 SHORT HLIF LA-140 -4.952E+04 2. 511E+05 2.521E+05 SHORT HLIF CE-141 1. 2 69E+OO 2 .115E+Ol 2 .115E+Ol NOT IDENT. CE-143 l.OOOE+41 7.553E+40 O.OOOE+OO SHORT HLIF CE-144 -2.300E-01 2.830E-01 3.014E-01 NOT IDENT. PM-144 -2.303E-02 4 .151E-02 4.279E-02 NOT IDENT. PR-144 -2. 013E+OO 3.603E+OO 3.715E+OO NOT IDENT. PM-146 6.808E-03 3.246E-02 3. 261E-02 NOT IDENT. ND-147 l.454E+07 2.607E+07 2.688E+07 SHORT HLIF PM-147 -5.319E+02 6.529E+02 6.955E+02 NOT IDENT. PM-149 -3.301E+40 4.073E+40 0.000E+OO SHORT HLIF EU-150 l.286E-02 1. 966E-02 2.050E-02 FAIL ABUN EU-152 -9.259E-02 6.473E-02 7.702E-02 NOT IDENT. GD-153 --,2.272E-01 1. 2 67E-01 1. 629E-01 NOT IDENT. EU-154 3.051E-02 7.574E-02 7.698E-02 FAIL ABUN EU-155 8 .181E-02 7.973E-02 8.785E-02 FAIL ABUN TB-160 l.600E-01 l.668E+OO l.670E+OO FAIL ABUN H0-166M -2.302E-02 4.161E-02 4.288E-02 NOT IDENT. TM-171 -6.472E+OO l.394E+Ol l.425E+Ol NOT IDENT. HF-172 -8.490E-03 1. 795E-Ol l.795E-01 FAIL ABUN Page 3509 of 5809 LU-172 1.469E-03 7.094E-02 7.095E-02 FAIL ABUN LU-176 2.891E-02 4.251E-02 4.446E-02 FAIL ABUN HF-181 1.970E+OO 3.384E+OO 3.498E+OO NOT IDENT. TA-182 -4.880E-Ol 6.794E-01 7.142E-01 FAIL ABUN RE-183 -8.280E-01 2. OllE+OO 2.045E+OO NOT IDENT. RE-184 -1.644E+Ol 2.430E+Ol 2.540E+Ol NOT IDENT. W-188 1.085E+02 9.984E+Ol l .112E+02 FAIL ABUN IR-192 -8.973E-02 3.175E-01 3.201E-01 FAIL ABUN BI-207 -4.942E-03 3.759E-02 3.766E-02 FAIL ABUN PB-210 8.066E-01 1.979E+OO 2.012E+OO NOT IDENT. BI-211 2.332E+OO 5.065E-01 l.167E+OO FAIL ABUN PB-211 2.926E-02 4.865E-01 4.866E-01 NOT IDENT. BI-212 2.085E+OO 6.993E-01 1.172E+OO FAIL ABUN RN-219 6.479E-02 2.922E-01 2.936E-01 FAIL ABUN RA:.._223 -5.056E-02 4.102E-01 4.108E-01 FAIL ABUN AC-227 9.580E-03 2.097E-01 2.098E-01 FAIL ABUN TH-227 9.580E-03 2.097E-01 2.098E-01 FAIL ABUN TH-231 -5.056E-02 4.102E-01 4.108E-01 FAIL ABUN PA-233 -2.204E-02 4.687E-02 4.791E-02 FAIL ABUN PA-234 -1. 747E-01 2.851E-01 2.958E-01 NOT IDENT. PA-234M 1.140E+OO 2.783E+OO 2.831E+OO FAIL ABUN NP-237 -2.204E-02 4.687E-02 4.791E-02 FAIL ABUN NP-238 1.000E+41 2.741E+41 O.OOOE+OO SHORT HLIF NP-239 l.059E-01 1.855E-01 l.915E-01 FAIL ABUN PU-239 -8. 7 61E+OO 2.558E+02 2.559E+02 FAIL ABUN AM-241 2.073E-02 9.278E-02 9.325E-02 NOT IDENT. CM-243 -2.230E-02 7.328E-02 7.397E-02 FAIL ABUN BK-247 -3.012E-02 6.222E-02 6.368E-02 FAIL ABUN CM-247 4. 372E-03 2.661E-02 2.668E-02 FAIL ABUN CF-249 2.169E-02 2.712E-02 NOT IDENT. CF-251 -7.413E-02 1. OOlE-01 l.055E-01 NOT IDENT. Page 3510of5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 49.1170 87.09 89.5969 136.47 69.9026 45.60 67.0512 87.57 89.6634 140.51 0.0000 46.54 50.3978 88.03 89.7272 143.76 76.9943 49.72 0.0000 88.34 89.7700 144.24 77.0366 51. 35 49.0542 88.47 89.7883 145.44 77.1395 51. 87 60.4421 89. 96 89.9934 152.43 59.1218 52.39. 66. *1823 1093.63 90.0864 153.25 0.0000 52.97 51.1179 91.11 0.0000 323.87 81.1746 53.44 54. 0115 92.59 90.3519 156.02 0.0000 54.07 70.2134 93.35 90.4545 158.56 0.0000 57. 36. 0.0000 94.56 66.5202 159.00 66.1533 57.53 70.7147 94.65 66.5291 162.33 60.8511 57.98 69.8221 94.67 66. 5311 162.66 0.0000 . 59. 27 65.2073 94.87 52.9688 163.33 60.9141 59.32 65.2138 97.43 78.7289 165.86 57.7415 59.54 65.2421 98.43 59.3877 176.31 60.5934 60. 96 76.9696 98.44 59.3886 176.60 *o.oooo 61.17 77.0010 99.53 47.1750 177.52 73.0228 62. 93 75.3307 100 .11 64.6626 181.07 0.0000 63.29 75.3825 102.03 67.9260 181.52 58.6452 63.58 75.4238 103.18 68.0358 184.41 58.8079 64.28 75.5238 103.37 68.0539 143.76 58.8809 66.73 75.2205 105.21 52.7214 193.51. 72.9990 67.24 75.2913 105.31 52.7288 197.03 62.9358 125.81 74.0523 106.12 63.1380 198.01 53.8295 67.75 74.0616 106.47 79.7370 201.83 51.7168 69.67 89.9659 109.28 54.0541 203.43 50.6393 70.83 78.3929 111. 00 64.5978 205.31 70.7061 72. 81 93.0885 111. 76 0.0000 210.85 57.9216 72. 87 93.0979 114.06 72.1817 215.65 56.9987 74.66 93.7157 116. 30 0.0000 222 .11 50.2942 74.82 93. 7410' 116.74 57 .. 7372 227.09 54.0263 74.97 93.7650 119.76 56.9066 227.38 62.2630 77 .11. 94.1063 121.12 74.9500 228.16 0.0000 78.74 98.0050 121.22 74.9597 228.18 44.6710 79.69 109.4335 121. 78 64.4472 116.74 44.6710 80.12 97.5641 122.06 57. 0718 235.69 59.9262 80.19 0.0000 122.92 67. 7134 235. 96 59.9394 80.57 97.6366 123.07 70.9007 238.63 59.2773 81. 00 109.6685 265.00 61.4232 238.98 0.0000 81. 07 109. 6811 125.81 65.8320 240.99 59.3887 81.75 97.1588 127.23 77.6466 242.00 59.4360 83.79 89.1317 127.91 58.5495 244.70 59.5627 84.00 89.1616 129.30 72. 5104 252.40 0.0000 85.43 89.3640 131.20 68.4004 252.80 43.1554 86.55 89.5215 133.02 74.9753 254.15 0.0000 86.79 89.5548 133. 52 70.7333 256.23 51. 6819 86.94 89.5758 136.00 68.7891 260.90 0.0000 Page 3511of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52. 0113 355.39 0.0000 584.27 15.8474 264.80 47.1778 356.01 38.5675 595.83 0.0000 265.00 47.1849 364.49 0.0000 427.87 20.3070 268.22 42.0416 366.42 0.0000 602.52 0.0000 269.46 35.2013 372. 51 34.6191 604.72 17.4353 270.03 35.2163 375.05 22.5358 607.14 18.9073 271.23 35.2473 377.52 29.5120 609.32 19.4092 273.65 0.0000 356.01 29.6200 610.33 19.4173 276.40 37.8200 388.16 20.9595 614.28 11. 6689 277.37 37.8456 388.63 0.0000 618.01 19.4775 277.60 37.8522 391. 69 28,8763 620.36 19.4954 278.00 37.8636 264.66 27.2625 621.93 11.7051 279.20 57.0473 401.81 28.1602 630.19 0.0000 279.54 57.0616 402.40 28.1693 631.29 10.7695 279.70 39.1318 404.85 26.4441 633.25 19. 5964 280.46 42.4161 410.95 21. 2261 634.78 0.0000 283.69 34.3378 413.71 33.6582 635.95 18.6359 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.5189 423. 72 0.0000 645.85 17.7239 285.90 0.0000 427.09 21. '4106 657.76 16.3221 287.50 29.5115 427.87 21.4194 657.90 0.0000 290.67 22.1830 433.94 21. 4878 661. 66 15.8509 293.27 0.0000 439.40 19.7531 664.57 0.0000 351. 93 19.7803 '453.88 22.6140 666.33 0:0000 295.96 19.7905 463.37 26.3574 666.50 0.0000 879.38 27.2603 468.07 24.5967 667. 71 0.0000 299.98 29.7671 473.00 0.0000 677.62 14.9506 300.09 29. 7693 475.06 18.2825 685.70 0.0000 300.13 29.7700 476.78 28.3618 695.00 0.0000 301. 36 29.7949 477.60 24.7121 696.49 18.0674 302.85 29.8250 482.18 16. 5114 696.51 18.0674 256.23 29.8586 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.0685 306.78 29.9041 497.08 22.1729 697.49 17.0699 308.46 29.9377 505.52 16.6959 702.65 15.0897 311. 90 35.0077 507.63 0.0000 706.68 19.1423 316.51 30.9335 511. 00 26.9677 711. 6'8 19.1770 319.41 0.0000 514.00 29.3326 720.70 0.0000 320.08 0.0000 514.00 29.3326 721. 93 0.0000 321.04 30.1868 520.40 28.9528 722.78 21.2803 323.87 31.0817 520.69 0.0000 722.91 21. 2811 325.23 49.6072 522.65 0.0000 723. 31 19.7642 328.76 0.0000 527.90 0.0000 724 .19 3.0416 333.37 23.3268 528.26 24.3697 727.33 4.5674 333.97 25.3644 529.59 18.7573 733.00 6.1023 334.37 31. 7139 529.87 0.0000 735.93 19.3440 338.28 28.8245 531. 02 0.0000 333.97 8.1491 338.32 28.8252 537.26 0.0000 739.50 0.0000 311. 90 30.5618 546.56 0.0000 747.24 17.3763 340.48 30.5618 552.55 28.4241 748.06 10.2242 340.55 0.0000 563.25 15.2305 752.31 16.3828 344.28 38.2928 569.33 15.7474 753.82 0.0000 345.93 27.2578 946.00 18.6121 756.73 18.4592 351.06 35.8887 569.70 18. 6137 756.80 19.4855 351. 93 35.9075 583.19 21.1200 884.68 12.3369 Page 3512of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:08:36.16 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : Z-OCT-2016 11:00:23. Sample date 8-DEC-2015 10:19:00. Acquisition date : 3-0CT-2016 09:08:01. Sample ID G405235027 Sample quantity 1.58553E+02 GRAM Detector name GAM08 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.68 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 74.88* 76.98* 83.55* 87.08* 92.62* 129.17 185.97* 209.64 238.61* 241.91 295.39* 300.66 328.15 338.63* 351. 96* 384.53 406.41 468.34 511. 08* 576.94 583.60* 609.17* 628.44 663.83 669 .11 727.14* 797.54 829.90 859.90* 911. 33* 961.41* 969.81* 994.04 1001. 96* Page 3514of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 97 150 49 47 24 33 85 39 312 74 119 32 37 67 158 53 57 11 52 8 119 148 9 29 14 32 5 20 21 65 5 39 10 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 130 1.18 111 1. 04 147 1.67 90 0.91 216 1.16 96 1. 54 66 1. 66 74 1.01 54 1.16 66 1.79 46 1.31 69 1. 07 31 1.86 76 1.43 47 1.16 76 9.77 75 10.03 24 0.93 66 2.48 14 0.59 24 1. 84 2 6 1. 68 14 1. 01 24 5.39 4 0.58 23 1. 27 32 1.21 0 1. 99 10 2.66 30 1. 62 6 0.94 32 1. 03 7 2.90 13 1.86 150.02 154.22 167.36 174.43 185.52 258.64 372.30 419.67 477.63 484.23 591.23 601.77 656.77 677.75 704.42 769.59 813.36 937.28 1022.78 1154.56 1167.88 1219.03 1257.59 1328.40 1338. 96 1455.07 1595.91 1660.65 1720.67 1823.57 1923.75 1940.57 1989.03 2004.89 146 146 165 172 181 255 367 416 472 472 587 597 653 672 699 759 801 931 1014 1150 1161 1211 1254 1319 1336 1449 1589 1656 1713 1815 1921 1930 1979 1999 12 2.71E-02 22.2 9.93E-01 12 4.17E-02 14.4 8 1. 37E-02 -45 .1 5 1.31E-02 34.2 10 6.60E-03123.0 8 9.21E-03 54.3 11 2.36E-02 23.1 8 1. 08E-02 41. 6' 29 8.66E-02 7.0 1.55E+OO 29 2.05E-02 28.4 9 3.31E-02 14.2 11 8. 95E-03 52. 2 9 1. 03E-02 31.1 13 1.85E-02 30.3 12 4.38E-02 12.1 23 1.47E-02 44.7 27 1. 59E-02 44. 0 8 3.07E-03 82.4 22 1.45E-02 46.0 8 2.18E-03 90.2 17 3.30E-02 13.5 15 4.llE-02 11.4 6 2.60E-03 70.4 17 8.17E-03 43.2 8 3.89E...:.03 36.4 13 8.92E-03 36.8 10 l.43E-03210.7 11 5.56E-03 22.4 14 5.83E-03 40.9 15 1. 80E-02 22. 6 6 1. 39E-03 98. 6 19 l.08E-02 39.3 13 2. 81E-03 61. 0 10 2.98E-03 72.8 Peak Search Report (continued) Page : 2 Sample ID : G405235027 Acquisition date 3-0CT-2016 09:08:01 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1071. 27 13 8 1. 78 2143.54 2138 11 3.63E-03 50.6 36 0 1120.39* 26 25 2.18 2241.82 2231 17 7.19E-03 49.4 37 0 1150.35 7 4 1. 24 2301.74 2297 9 2.02E-03 63.2 38 0 1154. 66 16 2 1. 98 2310.36 2306 9 4.35E-03 30.7 39 0 1173.23 12 2 1. 50 2347.51 2344 8 3.26E-03 36.1 40 0 1302.27 4 6 0.81 2605.66 2600 8 1. lOE-03118. 7 41 0 1460.80 315 4 2.30 2922.80 2915 14 8.75E-02 5.8 42 0 1728.85 19 0 1. 76 3459.00 3452 12 5.28E-03 22.9 43 0 1764.94* 19 4 1. 68 3531.20 3523 13 5.22E-03 33.6 Flag: "*" == Peak area was modified by background subtraction Page 3515of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:08:38 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 10:19:00 G405235027 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:08:01 158.55 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3516of5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.68 10.00 0.00 % Peak Energy 0.0% '

Line Activity Report Page : 2 Sample ID : G405235027 Acquisition date 3-0CT-2016 09:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 9.671E-01 l.404E+Ol 1.404E+Ol 11. 55 OK CD-109 88.03 3.70* 4.287E+OO 9.133E-01 l.433E+OO 141.09 OK SN-126 64.28 9.60 2.248E+OO Line Not Found Absent 86.94 8.90 4.287E+OO 3.797E-01 3.797E-01 141.09 OK 87.57 37.00* 4.287E+OO 9.133E-02 9.134E-02 141. 09 OK TL-208 277.37 6.60 3.710E+OO Line Not Found Absent 583.19 85.00* 2.006E+OO 3.567E-01 3.567E-01 27.01 OK 860.56 12.50 1.479E+OO 5.555E-01 5.555E-01 81. 86 OK PB-212 74.82 10.28 3.324E+00 l.222E+OO 1.222E+OO 66.34 OK 77 .11 17.10 3. 513E+00 1.567E+OO 1.567E+OO 28.77 OK 238.63 43.60* 4.174E+OO 9.631E-01 9.631E-01 14.09 OK *300.09 3.30 3.474E+OO 1.544E+OO l.544E+OO 104.34 OK BI-214 609.32 45.49* l.938E+00 8.533E-01 8.536E-01 22.78 OK 1120.29 14.92 1.202E+OO 6.847E-01 6.850E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 OK PB-214 74.82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3.513E+OO 2.762E+OO 2.763E+OO 28.77 OK 87.09 3.41 4.288E+00 Line Not Found <<INT Reject 242.00 7'. 25 4.130E+OO Line Not Found -----<<INT Reject 295.22 18.42 3.524E+00 l.009E+OO 1.009E+OO 28.32 OK 351. 93 35.60* 3.045E+OO 7.856E-01 7.858E-01 24.22 OK RN-222 609.32 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 OK 1120.29 14.92 1. 202E+00 6.847E-01 6.850E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 OK RA-224 240.99 4.10* 4.131E+OO 6.650E-01 6.650E-01 222.68 OK RA-226 609.32 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 OK 1120.29 14.92 1.202E+OO 6.847E-01 6.850E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 OK AC-228 105.21 1.10 5 .138E+OO Line Not Found Absent 338.32 11. 27 3.146E+oo 1.020E+OO l.020E+OO 60.55 OK 794.95 4.25 1.572E+00 Line Not Found Absent 835.71 1. 61 1.512E+OO Line Not Found Absent 911. 20 25.80* l.414E+OO 8.645E-01 8.645E-01 45.16 OK 968. 97 15.80 1.347E+OO 8. 811E-01 8. 811E-01 78.68 OK RA-228 105.21 1.10 5 .138E+OO Line Not Found Absent 338.32 11. 27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 OK 794.95 4.25 1. 572E+OO -----Line Not Found Absent 835.71 1. 61 1.512E+OO Lin*e Not Found Absent 911.20 25.80* 1.414E+OO 8.645E-01 8.645E-01 45.16 OK 968. 97 15.80 1.347E+OO 8. 811E-01 8. 811E-01 78.68 OK TH-228 74.82 10.28 3.324E+OO 1.222E+OO l.222E+00 66.34 OK 77 .11 17.10 3. 513E+OO 1.567E+OO 1.567E+OO 28. 7.7 OK 238.63 43.60* 4.174E+OO 9.631E-01 9. 631E-01 14.09 OK 300.09 3.30 3.474E+OO 1.544E+OO l.544E+OO 104.34 OK TH-230 609.32 45.49* 1.938E+OO 8.533E-01 8.533E-01 22.78 OK 1120. 29 14.92 1.202E+OO 6.847E-01 6.847E-01 98.80 OK 1764.49 15.30" 8.178E-01 6.740E-01 6.740E-01 67 .14 OK PA-231 283.69 1. 70 3.643E+OO Line Not Found Absent 301.36 5.35* 3.474E+OO 9.521E-01 9.521E-01 104.34 OK Page 3517 of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235027 Acquisition date : 3-0CT-2016 09:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-232 105.21 1.10 5.138E+OO Line Not Found Absent 338.32 11. 27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 OK 835.71 1. 61 1.512E+OO Line Not Found Absent 911.20 25.80* l.414E+OO 8.645E-01 8.645E-01 45.16 OK 968.97 15.80 1. 347E+OO 8. 811E-01 8. 811E-01 78.68 OK U-234 609.32 45.49* l.938E+OO 8.533E-01 8.533E-01 22.78 OK 1120.29 14.92 1. 202E+OO 6.847E-01 6.847E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.740E-01 67.14 OK AM-243 43.53 5.90 2.327E-01 Line Not Found Absent 74.66 67.20* 3.324E+OO l.870E-01 1.870E-01 66.34 OK ANH-511 511. 00 100.00* 2.233E+OO l.215E-01 1.215E-01 91. 93 OK Flag: "*" = Keyline Page 3518of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:08:39.77 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l * *Acquisition date 3-0CT-2016 09:08:01 Sensitivity : 3.000 *
Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 Ol:OO:IT0.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date 8-DEC-2015 10:19:00 Analyst initials: MXRl *
Sample ID G405235027 Sample Quantity 1.5855E+02 GRAM *
Batch Number. 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Activity (pCi/GRAM 1.404E+Ol 1.433E+OO 9.134E-02 3.567E-01 9. 631E-01 8.536E-01 7.858E-01 8.536E-01 6.650E-01 8.536E-01 8.645E-01 8.645E-01 9. 631E-01 8.533E-01 9.521E-01 8.645E-01 8.533E-01 1.870E-01 1.215E-01 Cnt uncert ( 1. 96-sigma) 1.589E+OO 1.982E+OO 1.263E-01 9.441E-02 l.330E-01 1.906E-01 1.865E-01 1.906E-01 1.451E+OO 1.906E-01 3.826E-01 3.826E-01 1.330E-01 1.905E-01. 9.735E-01 3.826E-01 1.905E-01 1.216E-01 1.095E-01 Non-Identified Nuclides *Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3519of5809
Key-Line Activity K.L. Cnt Uncert (pCi/GRAM ) . (1.96-sigma) 6.504E+OO 4.213E-02 O.OOOE+OO 2.021E-02 -2.279E-01 O.OOOE+OO O.OOOE+OO 2.085E-02 2.340E-01 O.OOOE+OO -1.607E-02 1.145E+Ol 4.337E-02 1. 960E+41 3.844E-02 3.905E-01 1.140E+04 4.416E+02 6.875E-02 4.575E-01 1.941E+41 5.053E-02 MDA (pCi/GRAM 7.692E-01 2.309E+OO 1.579E-01 6.442E-02 1. 031E-01 1.144E-01 l.262E-01 1.144E-01 1.106E+OO 1.144E-01 2. 701E-01 2. 7 OlE-01 l.031E-01 1*.143E-01 8.617E-01 2. 701E-01 1.143E-01 1.125E-01 5.481E-02 MDA (pCi/GRAM 2.425E+Ol 1.038E-01 O.OOOE+OO 9.064E-02 7 .114E-01 O.OOOE+OO O.OOOE+OO . 1. 308E-01 1.002E+00 O.OOOE+OO 9.168E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 2.274E-01 5.281E-01 1.163E+OO NOT IDENT. FE-59 -8.323E-01 6.966E+OO 1.358E+Ol NOT IDENT. C0-60 -2.168E-02 4.226E-02 7.539E-02 FAIL ABUN ZN-65 -l.915E-02 2.638E-01 4.365E-01 NOT IDENT. GE-68 1.983E+OO 2.631E+OO 5.691E+OO NOT IDENT. AS-73 -6.587E+OO 1.307E+Ol 2.458E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.045E+03 O.OOOE+OO SHORT HLIF SE-75 1. 870E-01 2.150E-01 4.561E-01 NOT IDENT. BR-77 O.OOOE+OO 2.479E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.164E+02 O.OOOE:t-00 SHORT HLIF RB-83 4 .196E-01 7.599E-01 l.501E+OO NOT IDENT. KR-85 3.660E+OO 7.482E+OO 1.513E+Ol NOT IDENT. SR-85 3.810E-01 7.908E-01 1.598E+OO NOT IDENT. RB-86 O.OOOE+OO 3.471E+04 O.OOOE+OO SHORT HLIF Y-88 -8.357E-02 2.283E-01 4.508E-01 NOT IDENT. Y-91 -2.909E+02 5.701E+02 1.012E+03 NOT IDENT. NB-94 2.014E-02 3.428E-02 7.343E-02 NOT IDENT. NB-95 -8.599E-01 9.997E-01 1. 764E+OO NOT IDENT. NB-95M -2.035E+OO 2.808E+OO 4. 596E+OO NOT IDENT. ZR-95 2.936E-01 1.234E+OO 2.664E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.306E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 891E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 9.131E-03 3.689E-02 6.517E-02 NOT IDENT. RH-102 l.055E-02 6.795E-02 1.197E-01 NOT IDENT. RU-103 4.992E-01 5. 610.E+OO 1.108E+Ol FAIL ABUN RH-106 -8.768E-02 5. 710E-01 1.056E+OO NOT IDENT. RU-106 -8.768E-02 5.710E-01 1.056E+OO NOT IDENT. AG-108M 6. 716E-03 2.641E-02 5.349E-02 NOT IDENT. AG-llOM -3.887E-02 8.707E-02 1.649E-01 NOT IDENT. SN-113 l.470E-01 2.612E-01 4.943E-01 NOT IDENT. CD-115 O.OOOE+OO 3.789E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.062E+05 O.OOOE+OO SHORT HLIF TE-123M -9.638E-03 1.360E-01 2. 481E-01 NOT IDENT. SB-124 7.086E-02 1. 721E+OO 4.004E+OO NOT IDENT. SB-125 -3.865E-02 1.081E-01 2.002E-01 NOT IDENT. TE-125M 1.640E+Ol 3.259E+02 6.058E+02 NOT IDENT. I-126 O.OOOE+OO 7.697E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 1.382E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.08.1E+22 O.OOOE+OO SHORT HLIF. I-131 O.OOOE+OO 5.044E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 7.139E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.310E+26 O.OOOE+OO SHORT HLIF BA-133 8. 272E-03 4.338E-02 7.863E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.493E-02 6.034E-02 l.336E-01 NOT IDENT. CS-135 1.302E-02 l.510E-01 2.983E-01 NOT IDENT. I-135 O.OOOE+OO 1. 050E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.149E+05 O.OOOE+OO SHORT HLIF .BA-137M 5.530E-02 4.183E-02 8. 721E-02 NOT IDENT. CS-137 5.842E-02 4.419E-02 9.213E-02 NOT IDENT. CE-139 4.175E-02 l.267E-01 2. 372E-01 NOT IDENT. BA-140 O.OOOE+OO l.417E+06 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 4.892E+05 O.OOOE+OO SHORT HLIF CE-141 -8.205E+OO 2.795E+Ol 4.990E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.864E+41 O.OOOE+OO SHORT HLIF CE-144 7.581E-03 3.674E-01 6.760E-01 NOT IDENT. PM-144 9. 004E-.03 6.253E-02 1.271E-01 NOT IDENT. PR-144 5.425E+OO 1.102E+Ol NOT IDENT. PM-146 -4.860E-02 4.515E-02 7.404E-02 NOT IDENT. ND-147 O.OOOE+OO 3.516E+07 O.OOOE+OO SHORT HLIF PM-147 1.708E+02 8.258E+02 1.581E+03 NOT IDENT. PM-149 O.OOOE+OO 5.024E+40 O.OOOE+OO SHORT HLIF EU-150 -3.078E-03 2.875E-02 4. 961E-02 FAIL ABUN EU-152 -2.251E-02 9.157E-02 1.560E-01 NOT IDENT. GD-153 -2.881E-02 l.927E-01 3.602E-01 NOT IDENT. EU-154 1.033E-01 l.063E-01 2.544E-01 NOT IDENT. EU-155

1.347E-01 1.234E-01 2.515E-01 FAIL ABUN TB-160 -8.125E-01 1.959E+OO 3.684E+OO FAIL ABUN H0-166M -2.912E-02 4.958E-02 9.285E-02 NOT IDENT. TM-171 -3.054E+OO 3.295E+Ol 6.422E+Ol NOT IDENT. HF-172 -5.277E-02 2.759E-01 4.622E-01 FAIL ABUN LU-172 -l.452E-02 8.554E-02 1.670E-01 FAIL ABUN LU-176 -1.481E-03 2.347E-02 4.603E-02 FAIL ABUN HF-181 -3.218E-01 4.122E+OO 7. 960E+OO NOT IDENT. TA-182 -1. 921E-02 9.545E-01 l.863E+OO FAIL ABUN RE-183 -2.253E+OO 3.904E+OO 7.300E+OO NOT IDENT. Page 3520 of 5809 RE-184 -2. 091E+Ol 3.319E+Ol 5.698E+Ol NOT IDENT . W-188 ._l.239E+02 1.328E+02 2.051E+02 NOT IDENT. IR-192 -5.255E-01 4.755E-01 8.214E-01 FAIL ABUN HG-203 -9. 311E-01 2.515E+OO 4.758E+OO NOT IDENT. BI-207 -2.076E-02 4. 967E-02 9.162E-02 FAIL ABUN PB-210 3.177E+OO 6.242E+OO l.286E+Ol NOT IDENT. BI-211 0.000E+OO 5.137E-01 7.917E-01 FAI;L ABUN PB-211 5.463E-01 6.832E-01 1.447E+OO NOT IDENT. BI-212 l.426E+OO 1.028E+OO 1. 486E+OO *FAIL ABUN RN-219 1.594E-01 3.681E-01 7.573E-01 NOT IDENT. RA-223 2.525E-Ol 6.153E-01 l.135E+OO FAIL ABUN AC-227 5.033E-02 2.330E-01 4.692E-01 FAIL ABUN TH-227 5.033E-02 2.330E-01 4.692E-01 FAIL ABUN TH-229 -l.659E-01 4.541E-01 8.847E-01 FAIL ABUN TH-231 2.525E-01 6.153E-01 1.135E+OO FAIL ABUN PA-233 1.298E-02 5.757E-02 l.162E-01 FAIL ABUN PA-234 -3.659E-02 2.617E-01 5 .191E-01 NOT IDENT. PA-234M 4.681E+OO 6.678E+OO 1.131E+Ol FAIL ABUN TH-234 -8.951E-01 1. 646E+OO 3.154E+OO FAIL ABUN U-235 -l.495E-02 2.094E-01 3.874E-01 FAIL ABUN NP-237. 1.298E-02 5.757E-02 l.162E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -8.951E-01 1.646E+OO 3.154E+OO FAIL ABUN NP-239 4.169E-02 2.647E-01 5.019E-01 NOT IDENT. PU-239 5.725E+02 6.099E+02 7.002E+02 FAIL ABUN AM-241 1.133E-01. 1. 732E-01 3.575E-01 NOT IDENT. CM-243 -7.545E-02 1.075E-01 l.904E-01 NOT IDENT. BK-247 5. 725E-02 7.294E-02 1.542E-01 FAIL ABUN .CM-247 2. 614E-02
3.534E-02 7.457E-02 NOT IDENT. CF-249 l.604E-02 4.279E-02 8. 566K-02 NOT IDENT. CF-251 -1.970E-02 l.169E-01 2. 321E-01 NOT IDENT. Page 3521of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:08:36.97 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 306 10.66* 9.671E-01 1.404E+Ol 1.404E+Ol 11. 55 CD-109 88.03 62 3.70* 4.287E+OO 1.843E+OO 2.892E+OO 68.45 SN-126 64.28 ------9.60 2.248E+OO ------Line Not Found ------86.94 62 8.90 4.287E+OO 7.662E-01 7.662E-01 68.45 87.57 62 37.00* 4.287E+OO 1:843E-01 1.843E-01 68.45 TL-208 277.37 ------6.60 3. 710E+OO ------Line Not Found ------583.19 128 85.00* 2.006E+00 3.567E-01 3.567E-01 27.01 860.56 22 12.50 l.479E+00 5.555E-01 5.555E-01 81.86 BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 180 12.92* 3.045E+OO 2.165E+OO 2.165E+OO 24.22 PB-212 74.82 129 10.28 3.324E+OO 1. 791E+OO 1. 791E+OO 44.36 77 .11 199 17.10 3.513E+00 1.567E+00 1.567E+00 28.77 238.63 370 43.60* 4.174E+OO 9. 631E-01 9. 631E-01 14.09 300.09 37 3.30 3.474E+OO 1.544E+OO 1.544E+OO 104.34 BI-214 609.32 159 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 1120.29 26 14.92 1. 202El+OO 6.8471'.:-01 6.850E-01 98.80 1764.49 18 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 PB-214 74.82 129 5.80 3.324E+OO 3.175E+OO 3.176E+OO 44.36 77 .11 199 9.70 3.513E+OO 2.762E+OO 2.763E+OO 28.77 87.09 62 3.41 4.287E+OO 2.000E+OO 2.000E+OO 68.45 242.00 88 7.25 4.131E+OO 1.385E+OO 1.385E+OO 56.85 295.22 138. 18.42 3.524E+OO 1.009E+OO 1.009E+OO 28.32 351. 93 180 35.60* 3.045E+OO 7.856E-01 7.858E-01 24.22 RN-222 609.32 159 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 1120.29 26 14.92 l.202E+00 6.847E-01 6.850E-01 98.80 1764.49 18 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 RA-224 240.99 88 4.10* 4 .131E+OO 2.449E+OO 2.449E+OO 56.85 RA-226 609.32 159 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 1120.29 26 14.92 1. 202E+OO 6.847E-01 6.850E-01 98.80 1764.49 18 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 AC-228 105.21 ------1.10 5.138E+00 ------Line Not Found ------338.32 76 11. 27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 794.95 ------4.25 1.572E+OO ------Line Not Found ------835. 71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 67 25.80* 1.414E+OO 8.645E-01 8.645E-01 45.16 968. 97 40 15.80 1. 34 7E+OO 8. 811E-01 8. 811E-01 78.68 RA-228 105.21 ------1.10 5.138E+OO ------Line Not Found ------338.32 76 11. 27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 794.95 ------4.25 1.572E+OO ------Line Not Found* ------835.71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 67 25.80* 1.414E+OO 8.645E-01 8.645E-01 45.16 968. 97 40 15.80 1.347E+OO 8.811E-01 8. 811E-01 78.68 TH-228 74.82 129 10.28 3.324E+00 1. 791E+OO 1.791E+OO 44.36 77 .11 199 17.10 3.513E+OO 1.567E+OO 1.567E+OO 28.77 238.63 370 43.60* 4.174E+OO 9. 631E-01 9. 631E-01 14.09 300.09 37 3.30 3.474E+OO 1.544E+OO l.544E+OO 104.34 TH-230 609.32 159 45.49* 1.938E+OO 8.533E-01 8.533E-01 22.78 Page 3522 of 5809 Nuclide Line Activity Report (continued) .Page : 2 Sample ID : G405235027 Acquisition date : 3-0CT-2016 09:08:01 Nuclide Type: Nuclide PA-231 TH-232 U-234 AM-243 ANH-511 Flag: "*" Page 3523 of 5809 Energy 1120.29 1764.49 283.69 301.36 105.21 338.32 835.71 911. 20 968. 97 609.32 1120.29 1764.49 43.53 74.66 511. oo. Key line Area %Abn 26 14.92 18 15.30 ------1. 70 37 5.35* ------1.10 76 11.27 ------1. 61 67 25.80* 40 15.80 159 45.49* 26 14.92 18 15.30 ------5.90 129 67.20* 57 100.00* Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi/GRAM %Error 1.202E+OO 6.847E-01 6.847E-01 98.80 8.178E-01 6.740E-01 67.14 3.643E+OO ------Line Not Found ------3.474E+OO 9.521E-01 9. 521E-01 104.34 5.138E+OO ------Line Not Found ------3.146E+OO 1.020E+OO 1.020E+OO 60.55 1.512E+OO ------Line Not Found ------l.414E+OO 8.645E-01 8.645E-01 4.5 .16 1. 34 7E+OO 8.811E-01 8. 811E-01 78.68 1.938E+OO 8.533E-01 8.533E-Oi 22.78 1.202E+OO 6.847E-01 6.847E-01 98.80 8.178E-01 6.740E-01 6.740E-01 67.14 2.327E-01 ------Line Not Found ------3.324E+OO 2.740E-01 2.740E-01 44.36 2.233E+OO 1.215E-01 1.215E-01 91. 93 Summary of Nuclide Activity Sample ID : G405235027 Page : 3 Acquisition date .. 3-0CT-2016 09:08:01 Total number of lines in spectrum 43 Number of unidentified lines 11 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y l.41E+10Y 7.04E+08Y l.41E+10Y 1600.00Y 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+l0Y 1. 41E+10Y l.41E+10Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 2.45E+05Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.404E+Ol l.843E+OO 1.843E-01 3.567E-01 2.165E+OO 9. 631E-01 8.533E-01 7.856E-01 8.533E-01 2.449E+OO 8.533E-01 8.645E-01 8.645E-01 9. 631E-01 8.533E-01 9.521E-01 8.645E-01 8.533E-01 2.740E-01 1.215E-01 3.195E+Ol 3.195E+Ol Decay Corr pCi7GRAM 1.404E+Ol 2.892E+OO 1 .. 843E-01 3.567E-01 2.165E+OO 9. 631E-01 8 .-536E-01 7.858E-01 8.536E-01 2.449E+OO 8.536E-01 8.645E-01 8.645E-01 9.631E-01 8.533E-01 9.521E-01 8.645E-01 8.533E-01 2.740E-01 1.215E-01 3.300E+Ol 3.300E+Ol 74.42% Decay Corr 2-Sigma Error 0.162E+Ol 1.980E+OO 1. 261E-01 0. 963E-01 0.524E+OO 1.357E-01 1.945E-01 1.903E-01 1.945E-01 1.392E+OO 1.945E-01 3.904E-01 3.904E-01 1.357E-01 1.944E-01 9. 934E-'01 3.904E-01 1.944E-01 l.216E-01 1.117E-01 "M" Manually accepted 2-Sigma %Error 11. 55 68.45 68.45 27.01 24.22 14.09 22.78 24.22 22.78 56.85 22.78 45.16 45.16 14.09 22.78 104.34 45.16 22.78 44.36 91. 93 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3524 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235027 Acquisition date : 3-0CT-2016 09:08:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.55 65 194 1. 67 167.36 165 8 1.37E-02 90.3 4.04E+OO T 0 92.62 31 281 1.16 185.52 181 10 6.60E-03 **** 4.62E+OO T 0 129.17 42 121 1. 54 258.64 255 8 9.21E-03 **** 5.48E+00 T 0 185.97 104 80 1. 66 372. 30 367 11 2.36E-02 46.3 4.93E+OO T 0 209.64 47 89 1. 01 419.67 416 8 1.08E-02 83.3 4.58E+OO T 0 328.15 43 35 1. 86 656.77 653 9 l.03E-02 62.2 3.23E+00 T 0 384.53 60 86 9.77 769.59 759 23 1. 4 7E-02 89.3 2.83E+OO T 0 406.41 64 84 10.03 813.36 801 27 l.59E-02 88.0 2.70E+OO 0 468.34 12 26 0.93 937.28 931 8 3.07E-03 **** 2.40E+OO T 0 576.94 8 15 0.59 1154. 56 1150 8 2.18E-03 **** 2.02E+OO 0 628.44 10 15 1. 01 1257.59 1254 6 2.60E-03 **** l.89E+OO 0 663.83 31 25 5.39 1328.40 1319 17 8.17E-03 86.4 l.81E+00 T 0 669 .11 15 4 0.58 1338. 96 1336 8 3.89E-03 72. 8 l.80E+OO T 0 727.14 34 24 1. 27 1455.07 1449 13 8.92E-03 73.6 1. 69E+OO *T 0 797.54 5 33 1. 21 1595.91 1589 10 1..43E-03 **** 1.57E+OO 0 21 0 1. 99 1660.65 1656 11 5.56E-03 44.7 1.52E+OO 0 961. 41 5 6 0.94 1923.75 1921 6 1.39E-03 **** 1.36E+OO T 0 994.04 10 7 2.90 1989.03 1979 13 2.81E-03 **** 1.32E+OO 0 1001. 96 11 13 1. 86 2004.89 1999 10 2.98E-03 **** 1.31E+OO T 0 1071.27 13 8 1. 78 2143.54 2138 11 3.63E-03 **** l.25E+00 0 1150.35 7 4 1. 24 2301.74 2297 9 2.02E-03 **** 1.18E+OO 0 1154. 66 .16 2 1. 98 2310.36 2306 9 4.35E-03 61. 3 1.17E+OO 0 1173.23 12 2 1. 50 2347.51 2344 8 3.26E-03 72 .2 1.16E+OO T 0 1302. 27 4 6 0.81 2605.66 2600 8 l.lOE--:03 **** l.06E+OO 0 1728.85 18 0 1. 76 3459.00 3452 12 5.28E-03 45.9 8.34E-01 Flags: "T" = Tentatively associated Page 3525 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:08:51.75 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l * *Acquisition date 3-0CT-2016 09:08:01 Sensitivity 3.000 *
Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date 8-DEC-2015 10:19:00 Nuclide Library : SOLID *
Sample ID G405235027 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.5855E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN * '* Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM 3.220E-01 1.0S7E+OO 7.460E-02 2.833E-02 4.785E-02 4. 968E-02 5.694E-02 4. 968E-02 5.131E-01 4. 968E.:...02 1.171E-01 1.171E-01 4.785E-02 4. 966E-02
3.946E-01 1. l 71E-01 4. 966E-02 5.314E-02 2.443E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3526 of 5809 Le (pCi/GRAM 1.078E+Ol 4.445E-02 .O.OOOE+OO 3. 727E-02 3.013E-01 O.OOOE+OO O.OOOE+OO 5.699E-02 4.363E-01 O.OOOE+OO 4.267E-02 5.015E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDEN'J;'. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M . SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3527 of 5809 5.782E+OO 3.078E-02 1.933E-01 2.495E+oo l.144E+Ol O.OOOE+OO 2 .112E-Ol O.OOOE+OO O.OOOE+OO 6.756E-Ol 6.840E+OO 7.223E-01 0.000E+OO 1.677E-01 4.292E+02 3.291E-02 7.773E-01 2 .131E+OO 1.141E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.039E-02 5.256E-02 4.899E+OO 4.669E-01 4.669E-01 2.386E-02 6.812E-02 2.247E-01 O.OOOE+OO O.OOOE+OO 1.152E-01 1.499E+OO 8.945E-02 2.847E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.553E-02 O.OOOE+OO 6.039E-02 1. 381E-01 O.OOOE+OO O.OOOE+OO 3.949E-02 4. l 72E-02 1.112E-01 O.OOOE+OO 0.000E+OO 2.339E+Ol O.OOOE+OO 3.146E-01 5.683E-02 4.925E+00 3.240E-02 O.OOOE+OO 7.353E+02 O.OOOE+OO 2.257E-02 6.952E-02 1.684E-01 l.090E-01 l.186E-01 l.576E+OO 3.931E-02 3.00lE+Ol 2.161E-01 7.206E-02 2.091E-02 3.504E+00 7.998E-01 3.393E+OO 2.420E+Ol NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN. *NOT IDENT. 'NOT I DENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT* IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. *FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3528 of 5809 9.332E+Ol 3.699E-01 2.185E+OO 3.872E-02 6.036E+OO 3.790E-01 6.584E-01 6.844E-01 3.415E-01 5.161E-01 *2 .166E-01 2.166E-01 4.103E-01 5.161E-01 5.293E'-02 2.198E-01 5.067E+OO 1.489E+OO 1.822E-01 5.293E-02 O.OOOE+OO 1.489E+OO 2.348E-01 3.303E+02 1. 674E-01 8.855E-02 7.124E-02 3.388E-02 3. 92rn*-02 1.082E-01 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:08:57.24 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l * *Acquisition date 3-0CT-2016 09:08:01 Sensitivity : 3.000 *
Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date 8-DEC-2015 10:19:00 Nuclide Library : SOLID *
Sample ID G405235027 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity 1.5855E+02 GRAM *
Quantity Err(%) 1.2614E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION . * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-:228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 l.404E+Ol l.433E+OO 9.134E-02 3.567E-01 9.631E-01 8.536E-01 7.858E-01 8.536E-01 6.650E-01 8.536E-01 8.645E-01 8.645E-01 9.631E-01 8.533E-01 9.521E-01 8.645E-01 8.533E-01 l.870E-01 1.215E-01 Act Error ( 1. 96-sigma) 1.750E+OO 1.994E+OO 1.269E-01 9.562E-02 1. 425E--Ol 1. 941E-01 1. 893E-01 1. 941E-01 l.456E+OO 1.941E-01 3. 851E-01 3. 851E-01 1.425E-01 1. 940E-01 9.945E-01 3.851E-01 1.940E-01 l.226E-01 1. 096E-01 Non-Identified Nuclides Nuclide BE-7 NA...:22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3529 of 5809 Key-Line Activity (pCi/GRAM 6.504E+OO 4. 213E-02 1. 000E+41 2.021E-02 -2.279E-01 -6.902E+02 2.475E+02 2.085E-02 2.340E-01 1.000E+41 -l.607E-02 K.L Act error ( 1. 96-sigma) l.145E+Ol 4.339E-02 5 .. 665E+41 3.846E-02 3.906E-01 l.140E+Q.4 4.417E+02 6.875E-02 4.576E-01 1. 941E+41 5.054E-02 TPU ( 1. 96-sigma) 1. 750E+OO 1.994E+OO 1.269E-01 9.562E-02 1.425E-01 1.941E-01 l.893E-01 1.941E-01 l.456E+OO l.941E-01 3. 851E-01 3. 851E-01 1.425E-01 1.940E-01 9.945E-01 3. 851E-01 1.940E-01 1. 22 6E-01 1. 096E-01 TPU (1. 96-sigma) 1.182E+Ol A.737E-02 O.OOOE+OO 3.952E-02 4.039E-01 1.141E+04 4.556E+02 6.939E-02 4.696E-01 O.OOOE+OO 5.106E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 2.274E-01 5.282E-01 5.381E-01 NOT IDENT. FE-59 -8.323E-01 6. 966E+OO 6.976E+00 NOT IDENT. C0-60 -2.168'E-02 4.227E-02 4.338E-02 FAIL ABUN ZN-65 -l.915E-02 2.638E-01 2.639E-01 NOT IDENT. GE-68 1.983E+OO 2.632E+OO 2.780E+OO NOT IDENT. AS-73 -6.587E+OO 1.314E+Ol 1.347E+Ol NOT IDENT. AS-74 -7.177E+02 7.045E+03 7.053E+03 SHORT HLIF SE-75 l.870E-01 2.152E-01 2. 311E-01 NOT IDENT. BR-77 1. 795E+38 1. 554E+39 O.OOOE+OO SHORT HLIF SR-82 l.349E+02 6.165E+02 6.195E+02 SHORT HLIF RB-83 4 .196E-01 7.621E-01 7.852E-01 NOT IDENT. KR-85 3.660E+OO 7.484E+OO 7.664E+OO NOT IDENT. SR-85 3.810E-01 7.909E-01 8.094E-01 NOT IDENT. RB-86 l.391E+04 3.471E+04 3.527E+04 SHORT HLIF Y-88 -8.357E-02 2.284E-01 2.315E-01 NOT IDENT. Y-91 -2.909E+02 5.702E+02 5.851E+02 NOT IDENT. NB-94 2.014E-02 3.429E-02 3.547E-02 NOT IDENT. NB-95 -8.599E-01 1.000E+OO 1. 073E+OO NOT IDENT. NB-95M -2.035E+OO 2. 813E+OO 2.959E+OO NOT IDENT. ZR-95 2.936E-01 1.234E+OO l.241E+OO NOT IDENT. NB-97 -l.000E+41 4.063E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.307E+41 O.OOOE+OO SHORT HLIF M0-99 -1.083E+32 1.892E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.129E+41 O.OOOE+OO SHORT HLIF RH-101 9.131E-03 3.693E-02 3.716E-02 NOT IDENT. RH-102 1.055E-02 6.795E-02 6.812E-02 NOT IDENT. RU-103 4.992E-01 5.610E+OO 5.615E+OO FAIL ABUN RH-106 -8.768E-02 5.711E-01 5. 724E_..:01 NOT IDENT. RU-106 -8.768E-02 5. 711E-01 5.724E-01 NOT IDENT. AG-108M 6. 716E-.03 2. 641E-02 2.658E-02 NOT IDENT. AG-llOM -3.887E-02 8.709E-02 8.884E-02 NOT IDENT. SN-113 l.470E-01 2. 613E-01 2.695E-01 NOT IDENT. CD-115 -l.921E+39 3.805E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -7.708E+04 l.066E+05 l.121E+05 SHORT HLIF TE-123M -9.638E-03 1.360E-01 l.361E-01 NOT IDENT. SB-124 7.086E-02 1.721E+OO 1. 721E+00 NOT IDENT. SB-125 -3.865E-02 l.082E-01 l.096E-01 NOT IDENT. TE-125M 1.640E+Ol 3.259E+02 3.260E+02 NOT IDENT. I-126 8.055E+05 7.774E+05 8.580E+05 SHORT HLIF SB-126 l.356E+06 1.405E+06 l.533E+06 SHORT HLIF SB-127 -1. 77 9E+22 3.212E+22 O.QOOE+OO SHORT HLIF I-131 2.690E+09 5.045E+09 5.189E+09 SHORT HLIF I-132 l.000E+41 1.850E+42 O.OOOE+OO SHORT HLIF TE-132 2.099E+26 4.394E+26 O.OOOE+OO SHORT HLIF BA-133 8. 272E-03 4.338E-02 4.354E-02 FAIL ABUN I-133 -l.000E+41 7.469E+41 O.OOOE+OO SHORT HLIF CS-134 6.493E-02 6.040E-02 6.712E-02 NOT IDENT. CS-135 1.302E-02 l.510E-01 1.511E-01 NOT IDENT. I-135 -1.000E+41 6.858E+41 O.OOOE+OO SHORT HLIF CS-136 8.062E+04 3.150E+05 3 .171E+05 SHORT HLIF BA-137M 5.530E-02 4.190E-02 4.875E-02 NOT IDENT. CS-137 5.842E-02 4.426E-02 5.150E-02 NOT IDENT .. CE-139 4.175E-02 l.270E-01 l.284E-01 NOT IDENT. BA-140 l.265E+06 1.418E+o6 l.529E+06 SHORT HLIF LA-140 -4.856E+05 4.898E+05 5.365E+05 SHORT HLIF CE-141 -8.205E+00 2.795E+Ol 2.819E+Ol NOT IDENT. CE-143 1.000E+41 1.867E+41 O.OOOE+OO SHORT HLIF CE-144 7.581E-03 3.674E-01 3.674E-01 NOT IDENT. PM-144 9.004E-03 6.254E-02 6.267E-02 NOT !DENT. PR-144 7.316E-01 5.425E+OO 5.435E+OO NOT IDENT. PM-146 -4.860E-02 4.529E-02 5. 031E-02 NOT IDENT. NP-147 1.296E+07 3.517E+07 3.565E+07 SHORT HLIF PM-147 1. 708E+02 8.259E+02 8.294E+02 NOT IDENT. PM-149 -4.055E+40 5.102E+40 O.OOOE+OO SHORT HLIF EU-150 -3.078E-03 2.875E-02 2.878E-02 FAIL ABUN EU-152 -2.251E-02 9.158E-02 9.214E-02 NOT IDENT. GD-153 -2.881E-02 l.927E-01 l .. 931E-01 NOT IDENT. EU-154 1:033E-01 l.064E-01 1.161E-01 NOT IDENT. EU-155 1. 34 7E-01 1.237E-01 1.378E-01 FAIL ABUN TB-160 -8.125E-01 1. 960E+OO l.994E+OO FAIL ABUN H0-166M -2.912E-02 4. 960E-02 5 .131E-02 NOT IDENT. TM-171 -3.054E+OO 3.295E+Ol 3.298E+Ol NOT IDENT. HF-172 -5.277E-02 2.761E-01 2. 771E-01 FAIL ABUN LU-172 -1.452E-02 8.555E-02 8.580E-02 FAIL ABUN LU-176 -l.481E-03 2.347E-02 2.348E-02 FAIL ABUN HF-181 -3.218E-01 4.122E+OO 4.124E+OO NOT IDENT. TA-182 -1.921E-02 9.545E-01 9.546E-01 FAIL ABUN RE-183 -2.253E+OO 3.920E+OO 4.050E+OO NOT IDENT. Page 3530 of 5809 RE-184 -2.091E+Ol 3.356E+Ol 3.486E+Ol NOT IDENT. W-188 -l.239E+02 l.335E+02 1.447E+02 NOT IDENT. IR-192 -5.255E-01 4.760E-01 5.317E-01 FAIL ABUN HG-203 -9 .*311E-01 2.516E+OO 2.550E+OO NOT IDENT. BI-207 -2.076E-02 4. 968E-02 5.055E-02 FAIL ABUN PB-210 3.177E+OO 6.249E+00 6. 411E+OO NOT IDENT. BI-211 2.165E+OO 5.227E-01 l.107E+OO FAIL ABUN PB-211 5.463E-01 6.838E-01 7.268E-01 NOT IDENT. BI-212 1.426E+OO 1.031E+OO l.215E+OO FAIL ABUN RN-219 l.594E-01 3.687E-01 3.756E-01 NOT IDENT. RA-223 2.525E-01 6.155E-01 6.259E-01 FAIL ABUN AC-227 5.033E-02 2.331E-01 2.342E-01 FAIL ABUN TH-227 5.033E-02 2. 331E-01 2.342E-01 FAIL ABUN TH-229 -1.659E-01 4.541E-01 4 .'603E-01 FAIL ABUN TH-231 2.525E-01 6.155E-01 6.259E-01 FAIL ABUN PA-233 1.298E-02 5.757E-02 5.787E-02 FAIL ABUN PA-234 -3.659E-02 2. 651E-01 2.656E-01 NOT IDENT. PA-234M 4. 681E+OO 6. 681E+OO 7.007E+00 FAIL ABUN TH-'234 -8. 951E-01 1.658E+OO 1.707E+OO FAIL ABUN .U-235 -1.495E-02 2.094E-01 2.095E-01 FAIL ABUN NP-237 1. 298E-02 5.757E-02 5.787E-02 FAIL ABUN NP-238 l.OOOE+41 3.059E+41 O.OOOE+OO SHORT HLIF U-238 -8.951E-01 1.658E+OO 1.707E+OO FAIL ABUN NP-239 4.169E-02 2.647E-01 2.654E-01 NOT IDENT. PU-239 5. 725E+02 6.104E+02 6.628E+02 FAIL ABUN AM-241 1.133E-01 l.734E-01 l.807E-01 NOT IDENT. CM-243 -7.545E-02 l.078E-01 1.130E-01 NOT IDENT. BK-247 5. 725E-02 7.384E-02 7.822E-02 FAIL ABUN CM-247 2.614E-02 3.561E-02 3.751E-02 NOT IDENT. CF-249 l.604E-02 4.281E-02 4.342E-02 NOT. I DENT. CF-251 -1.970E-02 l.170E-01 l.173E-01 NOT IDENT. Page 3531 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 48.7462 87.09 107.2032 136.47 64.4216 45.60 68.0586 87.57 98.4812 140.51 0.0000 46.54 66.2352 88.03 86.0623 143.76 74.7101 49. 72 0.0000 88.34 86.1123 144.24 71.1410 51. 35 68.1366 88.47 86.1331 145.44 82.1248 51. 87 71.2863 89. 96 86.3730 152.43 63.3821 52.39 65.2659 1093.63 90.1777 153.25 0.0000 52.97 68.4295 91.11 0.0000 323.87 70.8574 53.44 66.4684 92.59 99. 0311 156.02 0.0000 54.07 68.6258 93.35 99.1683 158.56 0.0000 57.36 0.0000 94.56 68.4899 159.00 58.9988 57.53 77.4974 94.65 68.5007 162.33 77.7589 57.98 71. 3771 94.67 68.5035 162.66 0.0000 59.27 58.1129 94.87 68.5278 163.33 63.0255 59.32 58.1202 97.43 72. 9554 165.86 66.9405 59.54 58.1512 98.43 68.5859 176.31 62.7602 60. 96 87.5264 98.44 68.5873 176.60 0.0000 61.17 90.6978 99.53 68.7176 177.52 67.8766 62.93 78.5145 100 .11 75.5524 181.07 0.0000 63.29 89.0581 102.03 74.6705 181.52 58.0889 63.58 83.8760 103.18 72.5488 184.41 63.3484 64.28 86.1129 103.37 75.9741 143.76 63.4422 66.73 89.7652 105.21 64.8352 193.51 62.2866 67.24 91. 982 8 105.31 63.7084 197.03 59.9562 125.81 85. 7238 106.12 66.0726 198.01 60.0195 67.75 81. 5029 106.47 75.2299 201.83 67.1526 69.67 80.7883 109.28 73.2876 203.43 64.6797 70.83 93.7813 111. 00 67.7502 205.31 71". 2887 72.81 88.4735 111.76 0.0000 210.85 56.0563 72.87 88.4848 114. 06 68.0819 215.65 61.1354 74.66 95.6258 116. 30 0.0000 222 .11 60.6537 74.82 95.6578 116.74 67.2099 227.09 64.4847 74.97 95.6876 119.76 57.0462 227.38 63. 6196 77 .11 96 .1134 121.12 54. 8311 228.16 0.0000 78.74 85.2374 121.22 54.8397 228.18 54.8258 79:69 88.2962 121.78 58.3893 116.74 54.8258 80.12 67.3655 122.06 67.7603 235.69 72.1464 80.19 0.0000 122.92 69.0182 235. 96 64.1470 80.57 67.4265 123.07 65.5233 2.38. 63 55. 3771 81. 00 82.7226 265.00 67.9258 238.98 0.0000 81. 07 89.9916 125.81 73.6240 240.99 *55.5000 81. 75 82.8455 127.23 58.0801 242.00 55.5524 83.79 97.7704 127.91 73.8515 244.70 55.6918 84.00 97.8106 129.30 63.7666 252.40 0.0000 85.43 83.4416 131.20 50.5221 252.80 45.6083 86.55 95.3570 133. 02 55.4024 254.15 0.0000 86.79 .95. 4000 133.52 57.0264 256.23 44.4780 86.94 95.4277 136.00 60.8030 2 60. 90 0.0000 Page 3532 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.5804 355.39 0.0000 584.27 17.9180 264.80 39.3283 356.01 26.5155 595.83 0.0000 265.00 35.6762 364.49 0.0000 427.87 25.9574 268.22 50.4536 366.42 0.0000 602.52 0.0000 269.46 39.4875 372. 51 32.7784 604. 72 11. 8732 270.03 44.1016 375.05 31. 8405 607.14 14. 7165 271.23 43.2268 377.52 26.9099 609.32 14.7313 273.65 0.0000 356.01 33.0289 610.33 14.7387 276.40 30.4850 388.16 33.1229 614.28 8.5184 277.37 40.6798 388.63 0.0000 618.01 15.9283 277.60 45. 3114 391.69 24.1450 620. 36 20.5020 278.00 42.5513 264.66 18.2142 621.93 21. 6564 279.20 40.7424 401.81 22.2784 630.19 0.0000 279.54 41. 6803 402.40 22.2865 631.29 15.4528 279.70 46.3175 404.85 22.3214 633.25 13.7480 280.46 40.7854 410.95 22.4078 634.(8 0.0000 283.69 29.7422 413.71 18.3655 635.95 24.0881 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 46.5383 423.72 0.0000 645.85 27.6514 285.90 0.0000 427.09 28.8061 657.76 15.6357 287.50 41. 0244 427.87 28.8197 657.90 0.0000 290.67 53.2833 433.94 19.6285 661.66 12.1821 293.27 0.0000 439.40 19.6927 664.57 0.0000 351.93 28.14'76 453.88 31.3611 666 .'33 0.0000 295.96 28.1641 463.37 25. 2271 666.50 0.0000 879.38 22.5786 468.07 30.0377 667. 71 0.0000 299.98 39.5570 473.00 0.0000 677. 62 17.5226 300.09 39.5604 475.06 22.2211 685.70 0.0000 300.13 39.5613 476.78 16.9466 695.00 0.0000 301.36 39.6006 477.60 14.8351 696. 49 22.0787 302.85 38.2308 482.18 19.1224 696. 51 22.0795 256.23 46.7879 48_7. 02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 26.5036 306.78 34.0884 497.08 17.1377 697.49 26.5054 308.46 37.9256 505.52 11. 2981 7 02. 65 17.7087 311. 90 31.3726 507.63 0.0000 706.68 20.3987 316.51 45.7949 511. 00 22.6626 711.68 15.9972 319.41 0.0000 514.00 22.6987 720.70 0.0000 320.08 0.0000 514.00 22.6987 721.93 0.0000 321.04 38.2943 520.40 19.5220 722.78 25. 7115 323.87 24.4650 520.69 0.0000 722. 91 25. 7133 325.23 17.2870 522.65 0.0000 723. 31 25.7177 328.76 0.0000 527.90 0.0000 724 .19 20.0095 333.37 36.7162 528.26 25.0468 727.33 15.2050 333.97 36.2488 529.59 23.9748 733.00 24.3835 334.37 42.0610 529.87 0.0000 735.93 16.1554 338.28 39.7580 531.02 0.0000 333.97 14.3691 338.32 39.7588 537.26 0.0000 739.50 0.0000 311. 90 39.8214 546.56 0.0000 747.24 19.8348 340.48 39.8214 552.55 19.8464 748.06 18.0371 340.55 0.0000 563.25 18.8442 752.31 11.7440 344.28 26.2958 569.33 25.5708 753.82 0.0000 345.93 30.2274 946.00 25.5736 756.73 9.9543 351. 06 28.3805 569.70 23.3516 756.80 9.9547 351. 93 28.3982 583.19 17.9089 884.68 13. 6125 Page 3533 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 29.9687 1274.44 3.9359 1620.50 3.6908 766.42 21. 8005 1001.03 10.8399 1621. 92 0.0000 766.84 19.9872 1002.74 18.9305 1678.03 0.0000 772. 60 0.0000 1004.73 17.3637 1690.97 2.8085 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.8500 778.90 13. 6913 1028.54 0.0000 1063.66 12.3633 783. 70* 0.0000 1037.84 13.9530 1771. 35 2.8538 785.37 11. 8947 1038.76 0.0000 1791.20 0.0000 792.07 14.6772 631. 29 4. 9966 1808.65 3.8324 794.95 17.6314 1048.07 0.0000 1810. 72 0.0000 795.86 15.6169 1049.04 13.0008 1836.06 4.8157 810.06 12.0058 1050.41 14.0068 810.29 10.1594 1063.66 14.0624 344.28 10.1601 1077.00 0.0000 810.76 9.2374 1077.34 9.2204 815.77 0.0000 1085.87 12 .1326 1048.07 0.0000 1093.63 13.1730 832.01 16.3851 1099.45 12.1802 834.85 11. 9289 1112. 07 17.9298 835.71 14.9155 1112. 84 22.8252 836.80 0.0000 1115. 54 21.2113 846.75 0.0000 1120.29 15.3168 846.77 10.2954 1120.55 15.3177 856.80 0.0000 1221.41 14.7085 860.56 9.4055 1129. 67 10.2386 871.09 13.2164 1131. 51 0.0000 873.19 18.8947 1147.95 0.0000 875.33 0.0000 1173.23 10.3638 879.38 16.0947 1177.95 13.2828 880.51 11.3654 1189.05 *9. 3675 883.24 12.3244 1204.77 15.6793 884.68 11. 3818 1221.41 12.5991 889.28 16.1502 1231. 02 15.7892 894.76 18.0839 1235.36 0.0000 898.04 11. 4342 1238.28 8.4370 900. 72 14.3060 1260.41 0.0000 903.28 17.4548 1271.87 9.5746 911.20 14.3568 1274.44 4.2583 912.08 14.3610 1274.54 4.2583 923.98 0.0000 1291.59 9.6229 926.50 8.6583 1298.22 0.0000 929 .11 14.4429 1312 .11 0.0000 937.49 13.5176 1332. 49 9. 7224 944.13 0.0000 1362.66 0.0000 946.00 11. 6191 1365.19 5.4446 949.00 12.5997 1368.63 0.0000 667. 71 0.0000 1384.29 6. 5636 962. 31 11. 6807 1408.01 7.7007 964.08 15.5830 1457.56 0.0000 966 .17 20.7917 1460.82 8.9097 911. 20 16.7228 1489.16 2.2418 968. 97 16.7228 1505.03 2.2498 983.53 0.0000 1584.12 14.6500 984.45 0.0000 1596.21 0.0000 Page 3534 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:09:27.24 ********************************************************************************
GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Backgr01.).nd file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG .GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 23-NOV-2015 14:50:00 Acquisition date : 3-0CT-2016 09:08:29. Sample ID G405235028 Sample quantity : 1.25516E+02 GRAM Detector name : GAM09 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.50 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 5 2 5 3 2 4 2 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 2 14 2 15 0 16 0 17 0 18 2 19 2 20 0 21 0 22 2 23 2 24 0 25 0 26 0 27 8 28 . 8 29 0 30 0 31 0 32 0 33 0 34 0 Page 3535 of 5809 Energy 63.45* 66.17* 75.00 77.13 87.01 92.87* 106.39 119. 81 129.51 143.90* 186.28* 209.07 238.72* 241.86 252.87 271.22 295.22* 300.05 301.81 310.57 338.61* 351.87* 354.59 438.55 463. 64 478.15* 510.76* 516.91 528.48 558.41* 564.80 578.37 583.01* 609.05* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 46 22 99 148 36 71 23 17 25 28 52 76 400 95 17 26 132 43 18 20 61 230 25 10 25 14 23 17 8 14 37 11 119 182 60 106 123 96 162 126 48 78 115 86 156 95 67 55 ,_52 77 44 40 44 13 78 25 15 14 46 18 30 16 13 11 33 12 14 13 1.18 1. 34 1. 03 0.90 1. 27 0.94 1. 36 1. 33 0.56 1. 04 1. 07 1. 25 1. 01 1. 33 1. 06 3.19 1. 06 1. 41 1. 41 1. 32 1. 09 1. 08 1. 47 0.72 1. 00 0.63 2.90 1. 99 1. 60 1. 80 8.03 0.66 1. 62 1. 22 126.57 132.01 149.68 153.94 173.71 185.45 212.49 239.35 258.74 287.53 372. 33 417.93 477.25 483.54 505. 57 . 542.28 590.30 599.98 603.49 621. 03 677 .12 703.66 709 .11 877.10 927.29 956.32 1021.58 1033.88 1057.04 1116.93 1129.72 1156.86 1166 .15 1218.25 124 124 146 146 171 182 210 236 254 284 367 412 472 472 501 536 585 596 596 619 672 698 698 874 921 951 1015 1015 1052 1114 1121 1150 1160 1211 13 l.26E-02 13 6.21E-03 14 2.74E-02 14 4. llE-02 7 9.87E-03 8 1. 96E-02 5 6.35E-03 7 4.81E-03 10 6.94E-03 8 7.69E-03 11 l.46E-02 13 2.lOE-02 16 l. llE-01 16 2.64E-02 8 4.69E-03 11 7.35E-03 11 3.66E-02 14 l.19E-02 14 4.87E-03 5 5.64E-03 12 l.68E-02 15 6.39E-02 15 6.92E-03 7 2.78E-03 12 7.02E-03 10 3.99E-03 23 6.50E-03 23 4.60E-03 7 2.28E-03 7 3.95E-03 21 l.03E-02 10 2.93E-03 11 3. 32E-02 13 5. 05E-02 31. 4 l.14E+OO 85.3 19.9 2.89E+OO 12.9 61. 6 32.1 51.1 87.5 82.7 62.4 50.5 28.8 5.9 2.09E+OO 18.9 77.9 67.1 13.2 30.7 l.09E+OO 75.5 34.9 31. 8 7.4 4.86E-01 37.7 69.6 56.8 62.l 67.7 1.65E+OO 49.8 82.4 51. 0 41. 5 69.9 11. 2 8.7 Peak Search Report (continued) Page : 2 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 613.75 7 14 0.89 1227.64 1223 6 2.06E-03 86.5 36 0 650 .11 10 14 1. 37 1300.41 1295 8 2.82E-03 70.9 37 0 661. 42 40 29 1.10 1323.03 1318 11 1. llE-02 30.2 38 0 703.29 18 14 1. 79 1406.82 1401 10 5.05E-03 45.8 39 0 727.30 41 15 1. 48 1454.86 1449 13 l.15E-02 25.1 40 0 763.48 10 7 0.57 1527.25 1524 6 2.71E-03 54.4 41 0 772.21 13 18 0.52 1544.73 1538 10 3.67E-03 68.0 42 0 786.69 27 7 3.56 1573.70 1568 13 7.36E-03 27.8 43 0 794.71 19 20 3.02 1589.74 1585 11 5.32E-03 50.1 44 0 906.46 10 8 0.54 1813.34 1806 10 2.83E-03 59.5 45 0 910.92* 61 10 1. 51 1822.27 1818 10 1.70E-02 16.7 46 0 928.71 11 10 3.73 1857.87 1850 13 3.15E-03 64.0 47 0 933.91 22 5 1. 90 1868.28 1863 10 6.17E-03 28.3 48 0 969. 07 60 8 1. 31 1938.63 1933 13 l.67E-02 16.6 49 0 1003.12 15 19 2.89 2006.77 2000 13 4.04E-03 71. 4 50 0 1078.97* 15 6 3.30 2158.55 2152 11 4.09E-03 41. 6 51 0 1097.54 7 6 0.75 2195.69 2191 8 2.02E-03 68. 8* 52 0 1119. 96 39 6 1. 88 2240.55 2235 12 1. 08E-02 20.4 53 0 . 1124. 78 10 4 0.83 2250.21 2247 7 2.64E-03 46.0 54 0 1138. 08 4 16 0.45 2276.82 2271 12 1.24E-03180.2 55 *o 1156.29 13 20 3.87 2313.25 '2302 16 3.74E-03 79.0 56 0 1180.73 10 12 0.61 2362.16 2356 9 2.66E-03 75.5 57 0 1378.46 7 6 1. 23 2757.82 2752 8 1.92E-03 72.2 58 0 1460.16* 313 0 1. 95 2921.32 2914 15 8.69E-02 5.7 59 0 1587.68 6 5 0.87 3176.50 3169 10 1.67E-03 80.8 60 0 1763.90* 30 0 2.05 3529.12 3521 15 8.22E-03 19.8 Flag: "*" = Peak area was modified by background subtraction Page 3536 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:09:29 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 23-NOV-2015 14:50:00 G405235028 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:08:29 125.52 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA9 0 01:00:00.00 1.50 keV No Linear 75.00 Report Interfering Nuclide Page 3537 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 87.09 242.00 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio
Systematic Error Efficiencies at Interfered Nuclide EU-155 SN-126 SN-126 CD-109 RA-224 . AM-243 TH-228 PB-212 BI-211 Line 86.55 86. 94 87.57 88.03 240.99 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.50 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status BE-7 477.60 10.44* 2.792E+OO 2.997E-01 1.808E+Ol 124.28 OK K-40 1460.82 10.66* l.146E+OO l.455E+Ol l.455E+Ol 11. 45 OK CD-109 88.03 3.70* 4.842E+OO 3.338E-01 5.357E-01 497.78 OK SN-126 64.28 9.60 2.286E+OO l.416E+OO 1.416E+OO 62. 78 OK 86.94 8.90 4.842E+OO 1.388E-01 l.388E-01 497.78 OK 87.57 37.00* 4.842E+OO 3.338E-02 3.339E-02 497.78 OK BA-137M 661. 66 89.90* 2.157E+OO 1.226E-01 l.250E-01 60.39 OK CS-137 66l.66 85.10* 2.157E+OO 1.295E-01 1.321E-01 60.39 OK PM-147 121.22 0.00* 6.261E+OO 6.398E+02 8.035E+02 175.07 OK EU-155 86.55 30.70 4-. 842E+OO 4.024E-02 4.563E-02 497.78 OK 105.31 21.10* 5.939E+OO 1.210E-01 1.373E-01 102.30 OK TL-208 277.37 6.60 4.352E+OO Line Not Found Absent 583.19 85.00* 2.382E+00 3.546E-01 3.546E-01 22.39 OK 860.56 12.50 1. 758E+OO Line Not Found Absent BI-211 72.87 1.23 3.4ll8E+OO Line Not Found Absent 351.06 12.92* 3.589E+OO 9.525E-02 9.525E-02 958.15 OK BI-212 727.33 6.67* 2.003E+OO 1.843E+OO 1.843E+OO 50.28 OK 785.37 1.10 l.885E+00 7.548E+OO 7.548E+OO 55.52 OK 1620.50 1. 47 1. 04'5E+OO Line Not Found Absent PB-212 74.82 10.28 3.689E+OO 1.148E+OO l.148E+00 62.52 OK 77 .11 17.10 3.920E+OO l.490E+OO 1.490E+OO 25.72 OK 238.63 43.60* 4.881E+OO l.192E+00 1.192E+OO 11. 89 OK 300.09 3.30 4.087E+OO 1. 991E+OO 1.991E+OO 61. 31 OK BI-214 609.32 45.49* 2.302E+OO l.041E+00 1. 041E+OO 17.44 OK 1120.29 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 1.123E+OO 1.124E+OO 39. 59 OK PB-214 74.82 5.80 3.669E+00 Line Not Found <<INT Reject 77 .11 9.70 3.920E+OO 2.627E+OO 2.628E+OO 25. 72 OK 87.09 3.41 4.849E+OO Line Not Found <<INT Reject 242.00 7.25 4. 832E+00 . Line Not Found <<INT Reject 295.22 18.42 4.141E+OO 1.082E+OO 1.083E+OO 26.47 OK 351.93 35.60* 3.588E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.302E+OO l.041E+OO 1. 041E+OO 17.44 OK 1120.29 14.92 1.429E+OO 1.057E+00 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 1.123E+OO 1.124E+o*o 39.59 OK RA-224 240.99 4.10* 4.834E+OO l.125E+OO 1.125E+OO 111.80 OK RA-226 609.32 45.49* 2.302E+OO l.041E+OO 1.041E+OO 17.44 OK 1120. 29 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 1.123E+OO 1.124E+OO 39.59 OK AC-228 105.21 1.10 5.939E+OO 2 .-322E+OO 2.322E+OO 102.30 OK 338.32 11. 27 3.704E+00 9.016E-01 9.016E-01 63.62 OK 794.95 4.25 l.870E+00 1.422E+OO 1.422E+OO 100.12 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 OK 968. 97 15.80 l.603E+OO 1.383E+OO 1.383E+OO 33.25 OK RA-228 105.21 1.10 5.939E+OO 2.322E+OO 2.322E+00 102.30 OK 338.32 11. 27 3.704E+OO 9.016E-01 9.016E-01 63.62 OK. 794.95 4.25 l.870E+00 1. 422E+OO 1.422E+OO 100.12 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent Page 3538 of 5809 Nuclide Line Report (continued) Page : 3 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 25.80* 1.682E+OO 8.265E-01 8. 2 65E-01 33.32 OK 968. 97 15.80 1.603E+OO 1.383E+OO 1.383E+OO 33.25 OK TH-228 74.82 10.28 3.689E+OO 1.148E+OO l.148E+OO 62.52 OK 77 .11 17.10 3.920E+OO l.490E+OO 1. 490E+OO 25.72 OK 238.63 43.60* 4.881E+OO 1.192E+OO l.192E+OO 11. 89 OK 300.09 3.30 4.087E+OO 1.991E+OO 1. 991E+OO 61. 31 OK TH-230 609.32 45.49* 2.302E+OO 1.041E+OO 1.041E+OO 17.44 OK 1120.29 14*. 92 1. 429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 1.123E+OO l.123E+OO . 39. 59 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301.36 5.35* 4.068E+OO 5.038E-01 5.038E-01 150.97 OK TH-232 105.21 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 OK 338.32 11. 27 3.704E+OO 9.016E-01 9.016E-01 63. 62 OK 835.71 1. 61 1.799E+OO Line Not Found Absent 911. 20 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 OK 968.97 15.80 1.603E+OO 1.383E+OO l.383E+OO 33.25 OK PA-233 300.13 6.63 4.087E+OO 9.909E-01 9.909E-01 61. 31 OK 311. 90 38.50* 3.975E+OO 8. 293E-02 . 8.293E-02 69.73 OK 340.48 4.45 3.687E+OO Line Not Found Absent TH-234 63.29 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62.78 OK 92.59 4.23 5.269E+OO 2.122E+OO 2.122E+OO 64.22 OK U-234 609.32 45.49* 2.302E+OO 1. 041E+OO 1. 041E+OO 17. 44 OK 1120.29 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 1.123E+OO 1.123E+OO 39.59 OK U-235 89. 96 3.47 5.068E+OO Line Not Found Absent 93.35 5.60 5.269E+OO 1.603E+OO 1.603E+OO 64.22 OK 143.76 10. 96*. 6.310E+OO 2. 613E-01 2. 613E-01 124 .. 72 OK 163.33 5.08 6.096E+OO Line Not Found Absent 185. 72 57.20 5.735E+OO l.027E-01 l.027E-01 101.07 OK 205.31 5.01 5.415E+00 Line Not Found Absent U-238 63.29 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62.78 OK 92.59 4.23 5.269E+OO 2.122E+OO 2.122E+OO 64.22 OK .AM-243 43.53 5.90 1. 969E-01 Line Not Found Absent 74.66 67.20* 3.689E+OO 1.756E-01 1. 757E-01 62.52 OK ANH-511 511. 00 100.00* 2.647E+OO 5. 361E-02 5. 361E-02 135.49 OK Flag: "*" = Keyline Page 3539 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:09:30.25 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l * *Acquisition date 3-0CT-2016 09:08:29 Sensitivity : 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
Sample date 23-NOV-2015 14:50:00 Analyst initials: MXRl *
Sample ID G405235028 Sample Quantity 1.2552E+02 GRAM *
Batch Number 1596249 Wet Weight
0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry . : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16 * .Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 1.808E+Ol 2.202E+Ol 2.537E+Ol K-40 1.455E+Ol 1.633E+OO 5.780E-01 CD-109 5.357E-01 2.613E+OO 2.642E+OO SN-126 3.339E-02 1.629E-01 1.567E-01 BA-137M 1.250E-01 7.400E-02 6.889E-02 CS-137 1.321E-01 7.818E-02 7.278E-02 PM-147 8.035E+02 1.379E+03 1.471E+03 EU-155 1.373E-01 1.376E-01 1.936E-01 TL-208 3.546E-01 7.780E-02 5.179E-02 BI-211 9.525E-02 8.943E-01 2.961E-'01 BI-212 1.843E+OO 9.080E-01 8.217E-01 PB-212 1.192E+00 1.388E-01 1.019E-01 BI-214 1.041E+OO 1. 780E-01 1.173E-01 PB-214 1.117E+OO 1.628E-01 3.643E-01 RN-222 1.041E+OO 1.780E-01 1.173E-01 RA-224 1.125E+OO 1.232E+OO 1.092E+OO RA-226 1.041E+OO 1.780E-01 1.173E-01 AC-228 8.265E-01 2. 699E-Ol* 2.702E-01 RA-228 8.265E-01 2.699E-01 2.702E-01 TH-228 1.192E+OO 1. 388E-01 1.019E-01 TH-230 1.041E+OO 1. 779E-0.1 1.173E-01 PA-231 5.038E-01 7.453E-01 7.462E-01 TH-232 8.265E-01 2.699E-01 2.702E-01 PA-233 8.293E-02 5.667E-02 9.811E-02 TH-234 3.673E+OO 2.260E+OO 2.660E+00 U-234 1.041E+OO 1.779E-01 l.173E-01 U-235 2.613E-01 3.194E-01 3.047E-01 U-238 3.673E+OO 2.260E+OO 2.660E+OO AM-243 1.757E-01 1. 07 6E-01 1.018E-01 ANH-511 5.361E-02 7 .119E-02 4.918E-02 Non-Identified Nuclides Key-Line Cnt Uncert MDA Activity K.L. Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM Page 3540 of 5809 NA-22 1.756E-02 4.724E-02 1. 033E-01 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF AL-26 -2.615E-02 3.992E-02 6. 817E-02 NOT IDENT. SC-46 -1. 364.E-01. 3.834E-01 7.040E-01 FAIL*ABUN V-48 O.OOOE+OO 2.257E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 6 .119E+02 O.OOOE+OO SHORT HLIF MN-54 3.315E-02 6.476E-02 1.373E-01 NOT IDENT. C0-56 -5.328E-02 5. 071E-01 9.791E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1. 256E-02 4. 967E-02 8.579E-02 NOT IDENT. C0-58 -1.170E-01 6.807E-01 l.291E+OO NOT IDENT. FE-59 1.602E+OO 7.670E+OO 1.466E+Ol NOT IDENT. C0-60 -2.154E-03 3.686E-02 7.673E-02 NOT IDENT. ZN-65 9.149E-02 1.921E-01 3.738E-01 NOT IDENT. GE-68 4.253E-01 2.527E+OO 5.191E+OO NOT IDENT. AS-73 4.979E+OO l.469E+Ol 3.036E+Ol NOT IDENT. AS-74 O.OOOE+OO l.023E+04 O.OOOE+OO SHORT HLIF SE-75 -7.611E-02 2.177E-01 3.834E-01 FAIL ABUN BR-77 O.OOOE+OO 1.945E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1.280E+03 O.OOOE+OO SHORT HLIF RB-83 -3.059E-02 6.694E-01 1.212E+OO FAIL ABUN KR-85 6.317E+OO 7.064E+OO 1.526E+Ol NOT IDENT. SR-85 7.776E-01 8.727E-01 1.885E+OO NOT IDENT. RB-86 O.OOOE+OO 5.587E+04 O.OOOE+OO SHORT HLIF Y-88 1.465E-01 2.634E-01 6.554E-01 NOT IDENT. Y-91 -5.891E+02 7.282E+02 1.267E+03 NOT IDENT. NB-94 5.270E-02 4.734E-02 7.625E-02 FAIL ABUN NB-95 -1.152E+OO 1.662E+OO 2 .151E+OO NOT IDENT. NB-95M 9.905E.,-01 3.326E+OO 5.763E+OO NOT IDENT. ZR-95 -1.217E+OO 1.834E+OO 3.156E+00 NOT IDENT. NB-97 O.OOOE+OO l.486E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.540E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8 .116E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 4.562E-03 3 .112E-02 5.643E-02 NOT IDENT. RH-102 -4.028E-03 5.142E-02 l.020E-01 NOT IDENT. RU-103 -7.032E+OO 7.433E+OO l.280E+Ol FAIL ABUN RH-106 l.548E-01 5.407E-01 1.101E+OO NOT IDENT. RU-106 1.548E-01 5.407E-01 1.101E+OO NOT IDENT. AG-108M 1.214E-02 2.629E-02 5.542E-02 FAIL ABUN AG-llOM 5.191E-02 9.494E-02 2.088E-01 .FAIL ABUN SN-113 5.300E-02 2.431E-01 4. 966E-01 NOT IDENT. CD-115 O.OOOE+OO 1.614E+41 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2.047E+05 0.000E+OO SHORT HLIF TE-123M -8. OOlE-02 l.355E-01 2.405E-01. NOT IDENT. SB-124 -l.427E+OO 2.073E+OO 3.444E+00 NOT IDENT. SB-125 1. 741E-02 l.128E-01 2.259E-01 FAIL ABUN TE-125M 7.959E+Ol 3.427E+02 6.264E+02 NOT IDENT. I-126 O.OOOE+OO 2.574E+06 O.OOOE+OO SHORT. HLIF SB-126 . 0.000E+OO 2.566E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.398E+23 O.OOOE+OO SHORT HLIF I-131 0.000E+OO l.842E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.253E+27 O.OOOE+OO SHORT HLIF BA-133 O.OOOE+OO 5.448E-02 6.917E-02 FAIL ABUN I-133 O.OOOE+OO l.614E+41 O.OOOE+OO SHORT HLIF CS-134 9.440E-02 9.262E-02 1.315E-01 FAIL ABUN CS-135 1. 502E-02 l.440E-01 2.481E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.482E+05 O.OOOE+OO SHORT HLIF CE-139 -1. 851E-02 l .115E-01 2.061E-01 NOT IDENT. BA-140 O.OOOE+OO 2.611E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 8.833E+05 O.OOOE+OO SHORT HLIF CE-141 1.848E+Ol 3 .181E+Ol. 5.958E+Ol NOT IDENT. CE-143 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.757E-01 3. 59'3E-01 5.769E-01 'NOT IDENT. PM-144 4.008E-03 6.903E-02 1.327E-01 FAIL ABUN PR-144 3.695E-01 6.046E+OO 1.162E+Ol NOT IDENT. PM-146 6.640E-03 3.953E-02 8. llOE-02 NOT IDENT. ND-147 0.000E+OO 9. 701E+07 O.OOOE+OO SHORT HLIF PM-149 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 2.547E-02 2.832E-02 5.375E-02 FAIL ABUN EU-152 -l.123E-03 9.637E-02 1.745E-01 NOT IDENT. GD-153 -1. 396E-01 1.842E-01 3. 311E-01 NOT IDENT. EU-154 4.025E-02 l.144E-01 2. 496E-01 NOT IDENT. TB-160 -1. 721E-01 2.134E+OO 4 .117E+OO FAIL ABUN H0-166M -6.627E-06 5.425E-02 l.067E-01 NOT IDENT. TM-171 -3.799E+Ol 3.069E+Ol 5.512E+Ol FAIL ABUN Page 3541 of 5809 HF-172 -9.466E-02 2. 221E-01 3.752E-01 FAIL ABUN LU-172 8.053E-03 1.025E-01 1. 754E-01 FAIL ABUN LU-176 l.258E-03 2.585E-02 4.393E-02 FAIL ABUN HF-181 -2.856E+OO 5.271E+OO 8. 511E+OO NOT IDENT. TA-182 -2.635E-01 l.203E+OO 2.305E+OO FAIL ABUN RE-183 -1. 317E+OO 4.465E+OO 8. 714E+OO FAIL ABUN RE-184 -l.442E+Ol 4.071E+Ol 6.438E+Ol NOT IDENT. W-188 -4.982E+Ol l.307E+02 2. 071E+02 FAIL ABUN IR-192 2.345E-01 5.058E-01 9.876E-01 FAIL ABUN HG-203 -1. 7 92E+OO 3.411E+OO 5.806E+OO NOT IDENT. BI-207 -1.288E-02 5.720E-02 1.054E-01 FAIL ABUN PB-210 4.970E+OO 7.193E+OO 1.502E+Ol NOT IDENT. PB-211 l.667E-01 5.689E-01 1.190E+OO NOT IDENT. RN-219 -9.467E-02 3.489E-01 6.765E-01 FAIL ABUN RA-223 -l.686E-01 6.674E-01 1.164E+OO FAIL ABUN AC-227 -l.360E-01 2.527E-01 3.935E-01 FAIL ABUN TH-227 -l.360E-01 2.527E-01 3.935E-01 FAIL ABUN TH-229 3.335E-02 4.608E-01 8.606E-01 FAIL ABUN TH-231 -1. 68 6E-01 6.674E-01 1.164E+OO FAIL ABUN PA-234 1.703E-01 2. 931E-01 6.240E-01 NOT IDENT. PA-234M 3. 661E-01 6.507E+OO 1.145E+Ol NOT IDENT. NP-237 8.293E-02 5.667E-02 1.027E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -l.455E-01 2.759E-01 4.615E-01 FAIL ABUN PU-239 4 .101E+02 6.648E+02 6.211E+02 FAIL ABUN AM-241 1.354E-02 1.698E-01 3.410E-01 NOT IDENT. CM-243 -5.031E-02 1.030E-01 1. 751E-01 NOT IDENT. BK-247 1.326E-02 6.734E-02 1.276E-01 FAIL ABUN CM-247 -2.270E-02 3.109E-02 5.675E-02 NOT IDENT. CF-249 -1.524E-02 4.413E-02 7.493E-02 FAIL ABUN CF-251 7.510E-02 1.124E-01 2.225E-01 NOT IDENT. Page 3542 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:09:27.99 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error BE-7 477.60 15 10.44* 2.792E+OO 2.997E-01 l.808E+Ol 124.28 K-40 1460.82 297 10.66* l.146E+OO 1.455E+Ol 1.455E+Ol 11. 45 CD-109 88.03 40 3.70* 4.842E+OO 1. 331E+OO 2.136E+OO 123.24 SN-126 64.28 52 9.60 2.286E+OO l.416E+00 1.416E+OO 62.78 86.94 40 8.90 4.842E+OO 5.535E-01 5.535E-01 123.24 87.57 40 37.00* 5. 4. 842E+OO 1.331E-01 l.331E-01 123.24 BA-137M 661.66 40 89.90* 2.157E+OO l.226E-01 l.250E-01 60.39 CS-137 661.66 40 85.10* 2.157E+OO l.295E-01 l.321E-01 60.39 PM-147 121.22 19 0.00* 6.261E+OO 6.398E+02 8.035E+02 -175. 07 EU-155 86.55 40 30.70 4.842E+OO 1.605E-01 1.820E-01 123.24 105.31 25 21.10* ' 5.939E+OO 1.210E-01 1.373E-01 102.30 TL-208 277.37 ------6.60 4.352E+OO ------Line Not Found ------583.19 120 .85.00* 2.382E+OO 3.546E-01 3.546E-01 22.39 860.56 ------12*. 50 1. 75aE+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.448E+OO ------Line Not Found ------351.06 '239 12.92* 3.589E+OO 3.077E+00 3.077E'+OO 14.87 BI-212 727. 33 41 6.67* 2.003E+OO l.843E+OO 1.843E+OO 50.28 785.37 26 1.10 l.885E+OO 7.548E+OO 7.548E+OO 55.52 1620.50 ------1. 47 1.045E+OO ------Line Not Found ------PB-212 74.82 112 10.28 3.689E+OO l.759E+OO 1. 759E+OO 39.77 77 .11 167 17.10 3.920E+OO 1.490E+OO 1.490E+OO 25. 72 238.63 424 43.60* 4. 881E+OO l.192E+OO 1.192E+OO 11. 89 300.09 45 3.30 4.087E+OO 1.991E+OO l.991E+00 61. 31 BI-214 609.32 182 45.49* 2.302E+OO 1. 041E+OO 1.041E+OO 17.44 1120.29 38 14.92 1.429E+OO 1.057E+OO l.057E+OO 40.70 1764.49 28 15.30 9.659E-01 l.123E+OO 1.124E+OO 39.59 PB-214 74.82 112 5.80 3.689E+OO 3.117E+OO 3 .119E+OO 39.77 77 .11 167 9.70 3.920E+OO 2.627E+OO 2.628E+OO 25.72 87.09 40 3.41 4.842E+OO 1.445E+OO l.445E+OO 123.24 242.00 101 7.25 4.834E+OO 1. 718E+OO 1. 719E+OO 37.88 295.22 138 18.42 4 .141E+OO 1.082E+OO l.083E+OO 26. 47 351.93 239 35.60* 3.589E+OO l .117E+OO l.117E+OO 14.87 RN-222 609.32 182 45.49* 2.302E+OO l.041E+OO 1.041E+OO 17.44 1120.29 38 14.92 l.429E+OO 1.057E+OO 1.057E+OO 40.70 1764.49' 28 15.30 9.659E-01 l.123E+OO l.124E+OO 39.59 RA-224 240.99 101 4.10* 4.834E+OO 3.039E+OO 3.039E+OO 37.88 RA-226 609.32 182 45.49* 2.302E+OO 1.041E+OO 1. 041E+OO 17.44 1120.29 38 14.92 1.429E+OO l.057E+OO 1.057E+OO 40.70 1764.49 28 15.30 9.659E-01 l.123E+OO l.124E+OO 39.59 AC-228 105.21 25 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 338.32 63 11. 27 3.704E+OO 9.016E-01 9.016E-01 63 .. 62 794.95 19 4.25 1.870E+OO 1.422E+OO 1.422E+OO 100.12 835.71 ------1. 61 1.799E+OO ------Line Not Found ------911.20 60 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 968.97 59 15.80 1.603E+OO 1.383E+OO 1. 383E+OO 33.25 RA-228 105.21 25 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 338.32 63 11.27 3.704E+OO 9.016E-01 9.016E-01 63.62 Page 3543 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 19 4.25 1.870E+OO 1.422E+OO 1.422E+OO 100.12 835. 71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 60 25.80* 1.682E+OO 8. 265E-01. 8.265E-01 33.32 968. 97 59 15.80 1. 603E+OO. l.383E+OO 1.383E+OO 33.25 TH-228 74.82 112 10.28 3.689E+OO 1. 759E+OO 1. 759E+OO 39.77 77 .11 167 17.10 3.920E+OO 1.490E+OO 1.490E+OO 25.72 238.63 424 43.60* 4.881E+.00 l.192E+OO 1.192E+OO 11. 89 300.09 45 3.30 4.087E+OO 1.991E+OO 1.991E+OO 61. 31 TH-230 609.32 182 45.49* 2.302E+OO 1. 041E+OO 1. 041E+OO 17.44 1120.29 38 14.92 l.429E+OO l.057E+00 1.057E+OO 40.70 1764.49 28 15.30 9.659E-01 l.123E+OO 1.123E+OO 39.59 PA-231 283.69 ------1. 70 4.275E+00 ------Line Not Found ------301.36 18 5.35* 4.068E+OO 5.038E-01 5.038E-01 150.97 TH-232 105.21 25 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 338.32 63 11. 27 3.704E+OO 9.016E-01 9.016E-01 63.62 835.71 ------1. 61 1. 799E+00 ------Line Not Found ------911.20 60 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 968. 97 59 15.80 1.603E+OO 1.383E+OO 1.383E+OO 33.25 PA-233 300.13 45 6.63 4.087E+OO 9.909E-01 9.909E-0"1 61. 31 311. 90 21 38.50* 3.975E+00 8.293E-02 8.293E-02 69.73 340.48 ------4.45 3.687E+OO ------Line Not Found ------TH-234 63.29 52 3.70* 2.286E+OO 3.673E+00 3.673E+OO 62.78 92.59 79 4.23 5.269E+00 2.122E+OO 2.122E+00 64.22 U-234 609.32 182 45.49* 2.302E+OO 1. 041E+OO l.041E+00 17.44 1120.29 38 14.92 1.429E+OO 1.057E+OO 1.057E+00 40.70 1764.49 28 15.30 9.659E-01 l.123E+OO 1.123E+OO 39.59 U-235 89. 96 ------3.47 5.068E+OO ------Line Not Found ------93.35 79 5.60 5.269E+OO 1.603E+OO 1.603E+OO 64.22 143.76 30 10. 96* 6.310E+OO 2.613E-01 2.613E-01 124. 72 163.33 ------5.08 6. 096E+OO ------Line Not Found ------185.72 56 57.20 5.735E+OO 1.027E-01 l.027E-01 101.07 205.31 ------5.01 5.415E+OO ------Line Not Found ------U-238 63.29 52 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62.78 92.59 79 4.23 5.269E+OO 2 .122E+00 . 2.122E+OO 64.22 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 112 67.20* 3.689E+OO 2. 691E-01 2.691E-01 39.77 ANH-511 511. 00 24 100.00* 2.647E+OO 5.361E-02 5.361E-02 135.49 Flag: "*" Key line Page 3544 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Total number of lines in spectrum 60 Number of unidentified lines 16 Number of lines tentatively identified by NID 44 Nuclide Type : Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 PM-147 EU-155 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224' RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-233 TH-234 u--234 U-235 U-238 AM-243 ANH-511 Hlife 53.22D l.25E+09Y 461. 400 . 2.30E+05Y 30.08Y 30.08Y 2.62Y 4.75Y l.41E+l0Y 7.04E+08Y 1. 41E+10Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600. OOY 1. 41E+10Y 1.41E+10Y l.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.14E+06Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 60.3 1. 00 1. 60 1. 00 1. 02 1. 02 1. 26 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 2.997E-01 1.455E+Ol 1. 331E+OO 1. 331E-01 l.226E-01 1.295E-01 6.398E+02 l.210E-01 3.546E-01 3.077E+OO l.843E+00 1.192E+OO 1.041E+OO 1.117E+OO 1. 041E+OO 3.039E+OO 1.041E+OO 8.265E-01 8.265E-01 l.192E+00 1.041E+OO 5.038E-01 8.265E-01 8.293E-02 3.673E+OO 1.041E+OO 2.613E-01 3.673E+OO 2.691E-01 5.361E-02 6.845E+02 6.845E+02 Decay Corr pCi/GRAM 1. 808E+Ol l.455E+Ol 2.136E+OO l.331E-01 l.250E-01 l.321E-01 8.035E+02 1.373E-01 3.546E-01 3.077E+OO 1.843E+OO 1.192E+OO 1.041E+OO 1.117E+OO 1. 041E+OO 3.039E+OO' l.041E+00 8.265E-01 8.265E-01 1.192E+OO 1. 041E+OO 5.038E-01 8.265E-01 8.293E-02 3.673E+OO 1. 041E+OO 2.613E-01 3.673E+OO 2.691E-01 5.361E-02 8.668E+02 8.668E+02 73.33% Decay Corr 2-Sigma Error 2.247E+01 0.167E+Ol 2.633E+00 1.641E-01 0.755E-01 0.798E-01 14.07E+02 1.404E-01 0.794E-01. 0.458E+00 0.927E+OO 0.142E+OO 0.182E+OO 0.166E+OO 0.182E+OO 1.151E+OO 0.182E+OO 2.754E-01 2.754E-01 0.142E+OO 0.182E+00 7.605E-01 2.754E-01 5.783E-02 2.306E+OO 0.182E+00 3.259E-01 2.306E+OO 1.070E-01 7.264E-02 "M" Manually accepted 2-Sigma %Error 124.28 11. 45 123.24 123.24 60.39 60.39 175.07 102.30 22.39 14.87 50.28 11. 89 17.44 14.87 17.44 37.88 17.44 33.32 33.32 11. 89 17.44 150.97 33.32 69.73 62.78 17.44 124.72 62.78 39.77 135.49 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3545 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235028 Acquisition date : 3-0CT-2016 09:08:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 66.17 25 121 1. 34 132.01 124 13 6.21E-03 **** 2.63E+00 T 0 129.51 27 126 0.56 258.74 254 10 6.94E-03 **** 6.34E+OO T 0 209.07 81 102 1. 25 417.93 412 13 2.lOE-02 57.7 5.35E+OO 0 252.87 18 55 1. 06 505.57 501 8 4.69E-03 **** 4.68E+OO T 0 271.22 28 81 3.19 542.28 536 11 7.35E-03 **** 4.43E+OO T 2 354.59 26 16 1. 47 709.11 698 15 6.92E-03 75.3 3.57E+OO T 0 438.55 10 14 0.72 877.10 874 7 2.78E-03 **** 3.00E+OO T 0 463.64 26 47 1. 00 927.29 921 12 7.02E-0'.3 **** 2.86E+OO T 8 516.91 17 17 1. 99 1033.88 1015 23 4.60E-03 99.7 2.62E+OO 0 528.48 8 13 1. 60 1057.04 1052 7 2.28E-03 **** 2.58E+OO T 0 558.41 14 11 1. 80 1116. 93 1114 7 3.95E-03 **** 2.47E+OO 0 564.80 37 33 8.03 1129.72 1121 21 l.03E-02 83.0 2.44E+OO 0 578.37 11 13 0.66 1156.86 1150 10 2.93E-03 **** 2.40E+OO 0 613.75 7 14 0.89 1227.64 1223 6 2.06E-03 **** 2.29E+OO T 0 650 .11 10 14 1. 37 1300.41 1295 8 2.82E-03 **** 2.19E+OO 0 703.29 18 14 1. 79 1406.82 1401 10 5.05E-03 91. 7 2.06E+OO T 0 763.48 10 7 0.57 1527.25 1524 6 2. 71E-03 **** 1.93E+OO T 0 772.21 13 18 0.52 1544.73 1538 10 3.67E-03 **** 1. 91E+OO T 0 906;46 10 8 0.54 1813.34 1806 10 2.83E-03 **** 1.69E+OO 0 928.71 11 9 3.73 1857.87 1850 13 3.15E-03 **** 1.66E+OO T 0 933.91 22 5 1. 90 1868.28 1863 10 6.17E-03 56.6 l.65E+OO 0 1003 *.12 14 19 2.89 2006.77 2000 .13 4.04E-03 **** 1.56E+OO T 0 1078.97 14 5 3.30 2158.55 2152 11 4.09E-03 83.1 1. 4 7E+OO 0 1097.54 7 6 0.75 2195.69 2191 8 2.02E-03 **** 1.45E+OO 0 1124.78 9 3 0.83 2250.21 2247 7 2.64E-03 92.1 1. 42E+OO 0 1138. 08 4 15 0.45 2276.82 2271 12 1.24E-03 **** 1. 41E+OO 0 1156.29 13 19 3.87 2313.25 2302 16 3.74E-03 **** 1.39E+OO 0 1180. 73 9 12 0.61 2362.16 2356 9 2.66E-03 **** 1.37E+OO 0 1378.46 7 6 1. 23 2757.82 2752 8 1.92E-03 **** 1.20E+OO 0 1587.68 6 5 0.87 3176.50 3169 10 l.67E-03 **** l.06E+OO Flags: "T" = Tentatively associated Page 3546 of 5809.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:09:42.84 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l *
Acquisition date 3-0CT-2016 09:08:29 Sensitivity : 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
Sample date 23-NOV-2015 14:50:00 Nuclide Library : SOLID *
s*ample ID G405235028 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.2552E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA. GAMMA] EFF GAM09 CAN. CNF; 16
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 PM-147 EU-155 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/i;;RAM 1.099E+Ol 2.228E-01 L247E+OO 7.373E-02 3.015E-02 3.186E-02 6. 771E+02 8.918E-02 2.185E-02 1.303E-01 3.498E-01 4.705E-02 5.086E-02 1. 758E-01 5.086E-02 5.046E-01 5.086E-02 1.164E-01 1.164E-01 4.705E-02 5.084E-02 3.353E-01 1.164E-01 4.365E-02 1.230E+OO 5.084E-02 l.403E-01 1.230E+OO 4.748E-02 2.149E-02 ----Non-Identified Nuclide NA-22 Page 3547 of 5809 Le (pCi/GRAM 4.375E-02 NOT IDENT.

NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 Page 3548 of 5809 O.OOOE+OO 2.552E-02 2.878E-01 O.OOOE+OO O.OOOE+OO 5.955E-02 4.124E-01 O.OOOE+OO 3.944E-02 5.488E-01 5.998E+OO 3.105E-02 1. 596E-01 2.214E+OO l.400E+Ol O.OOOE+OO 1. 725E-01 O.OOOE+OO O.OOOE+OO 5.185E-01 6.874E+OO 8.490E-01 O.OOOE+OO 2.601E-01 5.371E+02 3.416E-02 9.476E-01 2.677E+OO 1.345E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0 .-OOOE+OO 2.590E-02 4.337E-02 5.538E+OO 4.852E-01 4.852E-01 2.471E-02 8.884E-02 2.227E-01 O.OOOE+OO O.OOOE+OO 1.102E-01 1.089E+OO 1.018E-01 2.903E+02 O.OOOE+0.0 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 5.896E-02 1.125E-01 O.OOOE+OO O.OOOE+OO 9.472E-02 O.OOOE+OO O.OOOE+OO 2.755E+Ol O.OOOE+OO 2.630E-01 5.912E-02 5 .181E+OO 3. 572E-02 O.OOOE+OO O.OOOE+OO 2.455E-02 7.841E-02 l.527E-01 1. 056E-01 1.739E+OO 4.597E-02 2.493E+Ol 1. 716E-01 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT*. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN . NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL 'ABUN* NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-2*19 RA-223 AC-227 TH-227 TH-229 TH-231 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3549 of 5809 7.553E-02 1.977E-02 3.624E+OO 1.00lE+OO 4.009E+OO 2.620E+Ol 9.241E+Ol 4.449E-Ol 2. 651E+OO 4.529E-02 6.984E+OO 5.268E-01 2.996E-01 5.283E-Ol 1. 780E-01 l.780E-01 3. 969E-01 5.283E-01 2.706E-01 5.107E+OO 4.592E-02 O.OOOE+OO 2.139E-01 2.898E+02 l.573E-01 8.054E-02 5.770E-02 2:482E-02 3,370E-02 l.031E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABBN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:09:48.76 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l * *Acquisition date 3-0CT-2016 09:08:29 Sensitivity : 3.000 *
Detector ID *GAM09 Energy tolerance: .1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.50 Half life ratio : '***** *
Sample date 23-NOV-2015 14:50:00 Nuclide Library : SOLID *
Sample ID G405235028 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.2552E+02 GRAM *
Quantity Err(%) : 1.5934E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * *****************************************************************t************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate 1of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ). ( 1. 96-sigma) ( 1. 96-sigma) BE-7 l.808E+Ol 2.204E+Ol 2.204E+Ol K-40 1.455E+Ol 1. 800E+OO 1.800E+OO CD-109 5.357E-01 2.621E+OO 2. 621E+OO SN-126 3.339E-02 l.633E-01 l.633E-01 BA-137M 1.250E-01 7.420E-02 7.420E-02 CS-137 l.321E-01 7.838E-02 7.838E-02 PM-147 8.035E+02 1. 37 9E+03 1.379E+03 EU-155 1.373E-01 l.379E-01 1. 379E-01 TL-208 3.546E-01 7.924E-02 7.924E-02 BI-211 9.525E-02 9 .126E...:.01 9.126E-01 BI-212 1.843E+OO 9.128E-01 9.128E-01 PB-212 1.192E+OO 1.524E-01 l.524E-01 BI-214 1.041E+OO 1.835E-01 l.835E-01 PB-214 1.117E+OO 1.693E-01 l.693E-01 RN-222 1.041E+OO 1.835E-01 1.835E-01 RA-224 1.125E+OO 1.240E+OO l.240E+OO RA-226 1.041E+00 1.835E-01 1.835E-01 AC-228 8.265E-01 2.732E-01 2.732E-01 RA-228 8.265E-01 2.732E-01 2.732E-01 TH-228 1.192E+OO 1.524E-01 1.524E-01 TH-230 1. 041E+OO l.834E-01 1.834E-01 PA-231 5.038E-01 7.530E-01 7.530E-01 TH-232 8.265E-01 2.732E-01 2.732E-01 PA-233 8.293E-02 5.681E-02 5.681E-02 TH-234 3.673E+OO 2.402E+Ci0 2.402E+OO U-234 1.041E+OO l.834E-01 l.834E-01 U-235 2.613E-01 3 .196E-01 3 .196E-01 U-238 3.673E+OO 2.402E+OO 2.402E+OO AM-243 1.757E-01 1.088E-01 1.088E-01 ANH-511 5.361E-02 7.122E-02 7.122E-02 Non-Identified Nuclides Key-Line TPU Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) Page 3550 of 5809 NA-22 1. 756E-02 4. 725E-02 4.791E-02 NOT IDENT. NA-24 -l.OOOE+41 1.020E+42 0.000E+OO SHORT HLIF AL-26 -2.615E-02 3. 996E-02 4.166E-02 NOT IDENT. SC-46 -l.364E-01 3.835E-01 3.884E-01 FAIL ABUN V-48 l.045E+04 2.257E+04 2.306E+04 SHORT HLIF CR-51 2.576E+02 6.120E+02 6.229E+02 SHORT HLIF MN-54 3.315E-02 6.478E-02 6.648E-02 NOT IDENT. C0-56 -5.328E-02 5.071E-01 5.077E-01 NOT IDENT. MN-56 -1. OOOE+41 l.094E+42 O.OOOE+OO SHORT HLIF C0-57 -l.256E-02 4. 968E-02 5.000E-02 NOT IDENT. C0-58 -1.170E-01 6.807E-01 6.827E-01 NOT IDENT. FE-59 1. 602E+OO 7.671E+OO 7.705E+OO NOT IDENT. C0-60 -2.154E-03 3.686E-02 3.687E-02 NOT IDENT. ZN-65 9.149E-02 1.921E-01 1 :965E-01 NOT IDENT. GE-68 4.253E-01 2.527E+OO 2.534E+OO NOT IDENT. AS-73 4.979E+OO 1.473E+Ol l.490E+Ol NOT IDENT. AS-74 1.334E+02 l.023E+04 l.023E+04 SHORT HLIF SE-75 -7.611E-02 2.177E-01 2.204E-01 FAIL ABUN BR-77 l.670E+40 1.517E+41 0.000E+OO SHORT HLIF SR-82 2.876E+02 1.280E+03 l.287E+03 SHORT HLIF RB-83 -3.059E-02 6.694E-01 6.695E-01 FAIL ABUN KR-85 6.317E+OO 7.069E+OO 7.621E+OO NOT IDENT. SR-85 7.776E-01* 8.733E-01 9.410E-01 NOT IDENT. RB-86 -2.782E+03 5.587E+04 5.588E+04 SHORT HLIF Y-88 1. 465E-01 2.636E-01 2.718E-01 NOT IDENT. Y-91 -5.891E+02 7.285E+02 7.754E+02 NOT IDENT. NB'-94 5.270E-02 4.740E-02 5.302E-02 FAIL ABUN *. NB-95 -1.152E+OO 1.662E+OO 1.742E+OO NOT IDENT. NB-95M 9.905E-01 3.326E+OO 3.356E+OO NOT IDENT. ZR-95 -1. 217E+OO 1.835E+OO 1.915E+OO NOT IDENT. NB-97 1. OOOE+41 l.487E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.540E+41 O.OOOE+OO SHORT HLIF M0-99 3.489E+33 8.120E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.294E+41 O.OOOE+OO SHORT HLIF RH-101 4.562E-03 3 .113E-02 3.120E-02 NOT IDENT. RH-102 -4.028E-03 5.142E-02 5.145E-02 NOT IDENT. RU-103 -7.032E+OO 7.441E+OO 8.088E+OO FAIL ABUN RH-106 l.548E-01 5.408E-01 5.453E-01 NOT IDENT. RU-106 1.548E-01 5.408E-01 5.453E-01 NOT IDENT. AG-108M 1.214E-02 2.630E-02 2.686E-02 FAIL ABUN AG-llOM 5.191E-02 9.498E-02 9.782E-02 FAIL ABUN SN-113 5.300E-02 2. 431E-01 2.443E-01 NOT IDENT. CD-115 l.000E+41 l.625E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -1. 501E+05 2.055E+05 2.164E+05 SHORT HLIF TE-123M -8.00lE-02 1.355E-01 l.403E-01 NOT IDENT. SB-124 -l.427E+OO 2.075E+OO 2.172E+OO NOT IDENT. SB-125 1. 741E-02 1.128E-01 1.130E-01 FAIL ABUN TE-125M 7.959E+Ol 3.427E+02 3.446E+02 NOT IDENT. I-126 -2.242E+06 2.593E+06 2.783E+06 SHORT HLIF SB-126 -1. 7 66E+05 2.566E+06 2.567E+06 SHORT HLIF SB-127 -3. 841E+22 3.443E+23 O.OOOE+OO SHORT HLIF I-131 -1.353E+10 1.843E+10 1. 941E+10 SHORT HLIF I-132 l.000E+41 2. 096E+42 O*. OOOE+OO SHORT HLIF TE-132 l.051E+28 l.028E+28 O.OOOE+OO SHORT HLIF *BA-133 7.383E-02 5.457E-02 6.392E-02 FAIL ABUN I-133 1.000E+41 2.492E+41 O.OOOE+OO SHORT HLIF CS-134 9.440E-02 9. 271E-02 l.020E-01 FAIL ABUN CS-135 1.502E-02 1.441E-01 1.442E-01 NOT IDENT. I-135 -1.000E+41 2. 7 66E+42 O.OOOE+OO SHORT HLIF CS-136 -4.440E+05 7.498E+05 7.761E+05 SHORT HLIF CE-139 -1. 851E-02 1.116E-01 1.119E-01 NOT IDENT. BA-140 -1. 4'36E+06 2.612E+06 2.691E+06 SHORT HLIF LA-140 9.574E+03 8.833E+05 8.834E+05 SHORT HLIF CE-141 1.848E+Ol 3.182E+Ol 3.289E+Ol NOT IDENT. CE-143 l.000E+41 2.630E+41 O.OOOE+OO SHORT HLIF CE-144 -2.757E-01 3.596E-01 3.805E-01 NOT IDENT. PM-144 4.008E-03 6.903E-02 6.906E-02 FAIL ABUN PR-144 3.695E-01 6.046E+OO 6.049E+OO NOT IDENT. PM-146 6.640E-03 3.953E-02 3.965E-02 NOT IDENT. ND-147 2. 722E+07 9.703E+07 9.780E+07 SHORT HLIF PM-149 -l.OOOE+41 2.133E+41 O.OOOE+OO SHORT HLIF EU-150 2.547E-02 2.834E-02 3.058E-02 FAIL ABUN EU-152 -1.123E-03 9.637E-02 9.637E-02 NOT IDENT. GD-153 -1. 396E-01 l.844E-01 1.949E-01 NOT IDENT. EU-154 4.025E-02 l.144E-01 l.158E-01 NOT IDENT. TB-160 -1. 721E-01 2.134E+OO 2.135E+00 FAIL ABUN H0-166M -6.627E-06 5.425E-02 5.425E-02 NOT IDENT. TM-171 *-3. 799E+01 3.088E+Ol 3.531E+Ol FAIL ABUN Page 3551 of 5809 HF-172 -9.466E-02 2.226E-01 2.267E-01 FAIL ABUN* LU-172 8.053E-03 1.025E-01 l.025E-01 FAIL ABUN LU-176 1.258E-03 2.585E-02 2.585E-02 FAIL ABUN HF-181 -2.856E+OO 5. 272E+OO 5.427E+OO NOT IDENT. TA-182 -2.635E-01 1. 203E+OO l.209E+OO FAIL ABUN RE-183 -1.317E+OO 4.470E+OO 4.509E+OO FAIL ABUN RE-184 -1.442E+Ol 4.087E+Ol 4.138E+Ol NOT IDENT. W-188 -4.982E+Ol 1.308E+02 1.327E+02 FAIL ABUN IR-192 2.345E-01 5.059E-01 5.168E-01 FAIL ABUN HG-203 -1. 792E+OO 3.412E+OO 3.506E+OO NOT IDENT. BI-207 -1.288E-02 5.720E-02 5.750E-02 FAIL ABUN PB-210 4.970E+OO 7.208E+OO 7.548E+OO NOT IDENT. PB-211 1.667E-01 5.689E-01 5.739E-01 NOT IDENT. RN-219 -9.467E-02 3.491E-01 3.517E-01 FAIL ABUN RA-223 -1. 68 6E-01 6.675E-01 6.718E-01 FAIL ABUN AC-227 -1.360E-01 2.533E-01 2.606E-01 FAIL ABUN TH-227 -1.360E-01 2.533E-01 2.606E-01 FAIL ABUN TH-229 3.'335E-02 4.608E-01 4. 611E-01 FAIL ABUN TH-231 -1.686E-01 6.675E-01 6. 718E-01 FAIL ABUN PA-234 1.703E-01 3.519E-01 3.602E-01 NOT IDENT. PA-234M 3.661E-01 6.507E+OO 6.509E+OO NOT IDENT. NP-237 8.293E-02 5.681E-02 6.801E-02 FAIL ABUN NP-238 1.000E+41 4.439E+41 O.OOOE+OO SHORT HLIF NP-239 -l.455E-01 2.761E-01 2.838E-01 FAIL ABUN PU-239 4 .101E+02 6.650E+02 6.903E+02 FAIL ABUN AM-241 1. 354E-02 l.698E-01 l.699E-01 NOT IDENT. CM-243 -5. 031E-02 l.031E-01 1.056E-01 NOT IDENT. BK-247 1. 32 6E-02 6.740E-02 6.766E-02 FAIL ABUN CM-247 -2.270E-02 3.132E-02 3.295E-02 NOT IDENT. CF-249 -1.524E-02 4.415E-02 4.468E-02 FAIL ABUN CF-251 7. 510E-.02 1.127E-01 l.177E-01 NOT IDENT. Page 3552 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 74.66 38.0285 105.31 84.7366 131.20 51.9924 879.38 51.5907 86.79 84.7818 133.02 39.4293 46.54 36.0'.719 86.94 84.8099 133.52 50.9180 228.16 0.0000 87.09 84.8380 136.00 41. 2183 52.39 31.0659 87.57 84.9283 136.47 46.0459 1093.63 38.2976 88.03 95.8227 739.50 0.0000 52.39 50.3473 306.78 95.8877 140.51 0.0000 125.81 48.8370 88.47 95.9152 143.76 45.6080 53.44 40.8900 143.76 51. 0469 144.24 45.6417 54.07 30.5259 90.64 89.9037 145.44 38.9160 293.27 0.0000 531. 02 0.0000 152.43 51.1280 482.18 46.2649 92.59 72.5764 1048.07 0.0000 57.98 49.5762 93.35 72.6928 154.21 47.3188 59.27 46.4984 94.56 50.9549 158.56 0.0000 59.32 46.5051 311. 90 50. 9641 159.00 51. 6207 59.54 46.5343 946.00 50. 9663 162.33 48.8744 60.96 43.7166 94.87 50.9877 537.26 '0.0000 61.17 44.8360 97.43 57.2173 163.33 40.9531 62. 93 50.2762 98.43 47.4797 165.86 46.1109 63.29 50.3260 98.44 47.4805 427.87 48.8064 290.67 50.3659 103.37 55.6658 176.60 0.0000 87.57 50.4621 116.74 55.6658 177.52 40.7379 66.73 50.7949 100 .11 55.7306 181. 07 0.0000 67.24 50.8633 102.03 45 .1160 .181.52 55.9688 67.68 55.6529 103.18 59. 0852 184.41 61.6599 1221.41 55.6625 103.37 54.2821 185. 72 61.7642 97.43 61.5354 911. 20 42. 3711 193.51 45.7422 279.20 64.8037 105.31 46.0118 197.03 42.8093 1063.66 76.6875 106 .*12 50.0250 198.01 38.6796 72.87 76.6992 106.47 50.0586 201.83 38.8597 351.06 76.6992 109.28 48.8017 203.43 43.1440 74 .*66 64.5773 111. 00 56.9150 205.31 42.1863 '238.63 64.6028 111.76 0.0000 210.85 33.9702 351.93 64.6028 114. 06 65.5458 215.65 41. 6321 238.63 64.6028 116. 30 0.0000 222 .11 38.7131 74.97 64.6266 116.74 65.5556 227.09 43.2538 77 .11 64. 9623 119.76 45.7012 227.38 42.1861 78.74 65.2151 264.66 44.8759 228.16 0.0000 256.23 68.8013 121. 22 44.8835 228.18 25.9838 133.52 67. 7230 344.28 53.6634 235.69 50.9384 364.49 0.0000 122.06 48.6953 235. 96 64.0557 711. 68 62.0486 122.92 43.7662 238.63 49.2737 356.01 56.3597 1274.44 40.0251 238.98 0.0000 323.87 48.3164 123.68 41.3195 240.99 49.3973 81. 75 65.6755 125.81 46.4973 242.00 49.4501 83.79 61.3519 127.23 39.0512 244.70 30.8561 2 65. 00 61. 3810 127.91 '45.4021 685.70 0.0000 193.51 75.5212 129.30 45.5076 388.16 38.8943 Page 3553 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 507.63 0.0000 345. 93 . 21. 7 535 569.50 25.1686 256.23 40.1451 351.06 18.2021 569.70 25.1708 527.90 0.0000 351. 93 18.2149 583.19 9. 8596 264.66 32. 6117 355.39 0.0000 584.27 14.0930 264.80 31.4915 356.01 27.6132 595.83 0.0000 265.00 26.9978 364.49 0.0000 600.60 17.0566 2 68. 22 30.0928 366.42 0.0000 602.52 0.0000 269.46 38.4150 372.51 27.1435 604.72 15.6688 270.03 38.4357 375.05 19.7788 607.14 14.2621 401.81 38.4803 377.52 24.7693 609.32 14.2780 273.65 0.0000 383.85 27.3745 610.33 0.0000 276.40 50.0465 388.16 32.4548 614.28 8.5884 583.19 28.4615 666.33 0.0000 618.01 22.9463 277.60 27.3289 391.69 22.5269 884.68 15. 3151. 402.40 30.7565 400.66 18.4743 621. 93 15.3275 279.20 46.7581 401.81 23.5316 630.19 0.0000 279.54 44.4915 402.40 25.2234 631.29 11.5493 279.70 44.4975 404.85 16.8449 633.25 17.3408 280.46 41.1042 410.95 27.9136 634.78 0.0000 301.36 32.0674 413. 71 28.8148 635.95 12.5409 284.31 0.0000 720.70 0.0000 636.99 0.0000 285.41 34.4128 423.72 0.0000 1690.97 23.2646 285.90 0.0000 427.09 23.9497 657.76 5.8499 287.50 28.7331 427.87 25.6738 657.90 0'.0000 290.67 29.2012 433.94 17.1863 661. 66 16.6057 293.27 0.0000 439.40 15.5240 664.57 0.0000 295.22 21. 6061 453.88 16.5427 666.33 0.0000 316.51 21. 6204 463.37 13.1400 666.50 0.0000 298.58 20.8976 468.07 21.0864 667.71 0.0000 299.98 26.3488 473.00 0.0000 677.62 15.7474 300.09 26.3508 631. 29 18.5322 685.70 0.0000 300.13 26.3522 696. 49 14 .1348 695.00 0.0000 311. 90 26.3522 477.60 14.1419 .696.49 21.8433 301.36 26.3813 482.18 17.2847 696. 51 21.8433 302.85 26.4159 487.02 0.0000 697.00 0.0000 304.50 31.1230 492.35 0.0000 697.30 23.8379 304.85 0.0000 497.08 25.0452 697.49 23.8398 306.78 26.5079 505.52 12.1366 702.65 16.9260 308.46 26.5473 507.63 0.0000 706.68 13.4659 311. 90 21.9280 511. 00 16.2345 711. 68 12.9968 316.51 21. 2294 514.00 16.2634 720.70 0.0000 319.41 0.0000 514.00 16.2634 721.93 0.0000 320.08 0.0000 520.40 12.2432 722.78 9.0425 321. 04 28.4150 520.69 0.0000 722. 91 9.0428 323.87 36.7907 667. 71 0.0000 723.31 13.5670 325.23 33.2688 527.90 0.0000 756.73 21.1119 1596.21 0.0000 528. 26 10.9321 727.33 11. 0743 333.37 25.1214 529.59 25.9835 733.00. 15.1392 333.97 22.3410 529.87 0.0000 735.93 10.1058 334.37 23.9447 531.02 0.0000 737.46 17.1909 338.28 27.6248 537.26 0.0000 '739.50 0.0000 338.32 27.6255 1260.41 0.0000 747.24 15.2332 340.48 27.6740 552.55 17.5481 748.06 13.2068 340.55 0.0000 795.86 18. 1154 752.31 16.2845 344.28 26.5527 569.33 25.1664 753.82 0.0000 Page 3554 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:10:18.82 *********************************************************************************
GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM19.CNF;561 Background date : Z-OCT-2016 11:01:07. Sample date 23-NOV-2015 11:10:00 Acquisition date : 3-0CT-2016 09:08:53. Sample ID G405235029 Sample quantity 1.51202E+02 GRAM Detector name GAM19 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.76 0.0%
Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 5 5 0 0 0 0 4 4 0 0 1 1 0 0 0 0 0 0 0 0 1 1 0 8 8 0 0 0 0 4 Page 3556 of 5809 Energy 62.52* 74.69* 77.07* 86. 79 89.88 92.81* 129.14 143.25* 186.00* 209.48 238.55* 241.66 255.93 274.31 295.16* 300.36 338.55 351.84* 410.33 510.76* 583.11* 609.54* 625.69 661.59 723.01* 726.99 748.16 781.40 785.81 804.73 859.99 911.02* 946.99 963. 76 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 22 131 207 70 58 74 51 37 71 40 403 146 14 82 139 31 56 269 29 49 124 151 17 108 15 27 14 13 17 17 26 74 22 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 186 171 123 244 102 173 116 123 143 105 73 103 80 203 75 75 63 58 68 47 29 43 8 24 35 33 10 16 18 24 10 22 13 15 0.54 1.30 1. 07 1. 00 1.14 1. 56 0.79 2.78 1. 49 0.91 1.10 2.07 0.57 8.38 1. 62 1. 63 1. 51 1. 32 2.16 2.14 1. 75 1. 53 0.91 1.26 1. 98 1. 98 1. 39 2.20 2.29 1. 55 1. 80 1. 31 4.32 2.84 125.82 150.19 154.93 174.38 180.56 186.43 259.12 287.35 372. 89 419.88 478.04 484.25 512.80 549.58 591. 29 601.70 678.12 704.70 821. 74 1022.67 1167.44 1220.32 1252.65 1324.47 1447.36 1455.34 1497.69 1564.19 1573.03 1610.87 1721. 45 1823.55 1895.53 1929.07 121 143 143 168 178 178 256 283 369 416 470 470 509 533 586 586 674 698 812 1016 1162 1212 1249 1319 1440 1440 1494 1561 1561 1605 1717 1818 1886 1920 10 6 .15E-03119. 5 18 3.65E-02 19.8 2.59E+OO 18 5. 7 6E-02 11.1 11 1. 93E-02 45. 1 13 l.62E-02 28.4 4.40E--01 13 2.04E-02 35.9 8 1.41E-02 39.2 9 1.03E-02 57.4 11 l.98E-02 35.7 10 1.llE-02 50.9 24 1.12E-01 6.2 24 4.06E-02 20.7 9 3.79E-03121.7 28 2.28E-02 50.4 26 3.86E-02 14.6 1.62E+00 26 8.50E-03 56.7 9 1.55E-02 29.5 13 7.47E-02 8.6 13 7.98E-03 62.1 16 l.35E-02 39.7 12 3.46E-02 12.7 14 4.20E-02 12.4 8 4.72E-03 37.7 11 2.99E-02 13.1 27 4.06E-03 83.9 27 7.39E-03 48.0 10 3.92E-03 52.6 17 3.50E-03 54.1 2.80E+OO 17 4.83E-03 52.7 12 4.61E-03 64.1 12 7.35E-03 30.0 12 2.06E-02 17.5 17 6.21E-03 42.2 23 4.95E-03 56.9 3.57E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 4 968. 62 53 6 1. 82 1938.81 1920 23 l.46E-02 16.2 36 0 1063.76* 10 22 1. 73 2129.16 2121 15 2.67E-03160.0 37 0 1120.42 41 14 1. 66 2242.54 2237 11 l.14E-02 23.4 38 0 1134. 69 13 15 3.50 2271.08 2263 15 3.61E-03 70.6 39 0 1143.20 15 12 3.51 2288.11 2282 12 4.16E-03 53.0 40 0 1168.70 19 12 1. 24 2339.14 2333 13 5.26E-03 45.2 41 0 1200.59 13 9 3.91 2402.95 2394 14 3.55E-03 59.9 42 3 1203.95 11 2 1. 89 2409.67 2407 13 3.16E-03 28.6 l.41E-01 43 3 1207.52 13 1 2.05 2416.82 2407 13 3.70E-03 28.3 44 0 1236.70 32 28 8.17 2475.21 2464 27 8.92E-03 48.5 45 0 1263.32 9 8 1. 37 2528.47 2521 12 2.57E-03 71.8 46 1 1272.80 20 6 2.30 2547.42 2542 19 5. 48E-03 31. 7 2 .13E+OO 47 1 1275.58 15 7 2.09 2553.00 2542 19 4.30E-03 41.9 48 0 1280.93 7 4 1. 39 2563.69 2560 7 l.81E-03 61. 8 49 0 1460.59 368 3 1. 93 2923.18 2916 14 l.02E-01 5.3 50 0 1511. 05 7 5 1. 34 3024.14 3017 10 l.94E-03 70.7 51 0 1764.29* 34 0 3.25 3530.84 3522 15 9.40E-03 18.4 Flag: "*" = Peak area was modified by background subtraction Page 3557 of 5809

\ VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:10:20 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 11:10:00 G405235029 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:08:53 151.20 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA19 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 TH-229 SN-126 SN-126 CD-10'9 AM-243 TH-228 PB-212 BI-211 Line 240.99 85.43 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.76 10.00 0.00 % Peak Energy 0.0% Page 3558 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : G405235029 Acquisition date 3-0CT-2016 09: 08.: 53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* 1.297E+OO 5.808E-02 7.308E-02 83.90 OK K-40 1460.82 10.66* 1.161E+OO l.424E+Ol 1.424E+Ol 10.65 OK Y-91 1204.77 0.26* 1.358E+OO 1.576E+Ol 6.574E+02 57.20 OK CD-109 88.03 3.70* 5.459E+OO l.234E+OO 1.980E+OO 160.25 OK SN-126 64.28 9.60 3.426E+OO Line Not Found Absent 86.94 8.90 5.459E+OO 5.128E:.._01 5.128E-01 160.25 OK 87.57 37.00* 5.459E+00 1.234E-01 1.234E-01 160.25 OK BA-137M 661. 66 89.90* 2.164E+OO 2.887E-01 2.945E-01 26.26 OK CS-137 661. 66 85.10* 2.164E+OO 3.050E-01 3. lllE-01 26. 26 OK TL-208 277.37 6.60 4.415E+OO Line Not Found Absent 583.19 85.00* 2.392E+OO 3. 231E-01 3. 231E-01 25.47 OK 860.56 12.50 1. 764E+00 6.089E-"01 6.089E-01 60.00 OK BI-:-211 72. 87 1. 23 4.361-E+OO Line Not Found Absent 351.06 12.92* 3.630E+OO 3.842E-01 3.842E-01 255.35 OK BI-212 727.33 6.67* 2.0lOE+OO 1.025E+OO 1.025E+OO 95.99 OK 785.37 1.10 1.892E+OO *4.277E+OO 4.277E+OO 105.50 OK 1620.50 1. 47 1.063E+OO Line Not Found Absent PB-212 74.82 10.28 4.533E+OO* 1.224E+OO 1.224E+OO 59.67 OK 77 .11 17 .10 4.743E+OO 1.624E+OO l.624E+OO 22: 16 OK 238.63 43.60* 4.961E+OO 1.074E+OO l.074E+OO 12.45 OK 300.09 3.30 4.139E+OO 1.262E+OO 1.262E+OO 113. 35 OK BI-214 609.32 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.468E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO l.052E+OO 36.70 OK PB-214 74.82 5.80 4.544E+00 Line Not Found <<INT Reject 77 .11 9.70 4.743E+OO 2.862E+OO 2.863E+OO 22.16 OK 87.09 3.41 5.478E+OO Line Not Found <<INT Reject 242.00 7.25 4.908E+OO Line Not Found <<INT Reject 295.22 18.42 4.198E+OO l.015E+OO 1.016E+OO 29.18 OK 351. 93 35.60* 3.629E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 OK 1120.29 14.92 l.437E+OO 9.465E-01 9.468E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 OK RA-224 240.99 4.10* 4. 913E+OO 2.381E+OO 2.381E+OO 75.98 OK RA-226 609.32 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.468E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 OK AC-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 OK 794.95 4.25 1.875E+OO Line Not Found Absent 835.71 1. 61 1.803E+OO Line Not Found Absent 911.20 25.80* l.687E+OO 8.586E-01 8.586E-01 35.02 OK 968.97 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 OK RA-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 OK 794.95 4.25 1.875E+OO Line Not Found Absent 835. 71 1. 61 1.803E+OO Line Not Found Absent 911. 20 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 OK 968.97 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 OK Page 3559 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 4.533E+OO l.224E+OO 1.224E+OO 59.67 OK 77 .11 17.10 4.743E+OO 1.624E+OO 1. 624E+OO 22.16 OK 238.63 43.60* 4. 961E+OO l.074E+OO 1.074E+OO 12.45 OK 300.09 3.30 4 .139E+OO 1.262E+OO 1.262E+OO 113. 35 OK TH-229 85.43 14.70 5.459E+oo 3.105E-01 3.105E-01 160.25 OK 88.47 24.00 5.640E+OO 2.705E-01 2.705E-01 56. 87 OK 193.51 4.41* 5.711E+OO Line Not Found Absent 210.85 2.80 5.435E+OO 1.529E+OO 1.529E+OO 101.84 OK TH-230 609.32 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 OK PA-231 283.69 1. 70 4.336E+OO Line Not Found Absent 301.36 5.35* 4 .139E+OO 7.782E-01 7.782E-01 113. 35 OK TH-232 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11.27 3.748E+OO 7.358E-01 7.358E-01 58.98 OK 835.71 1. 61 1..803E+00 Line Not Found Absent 911. 20 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 OK 968. 97 15.80 1. 609E+OO l.038E+OO l.038E+OO 32.48 OK TH-234 63.29 3.70* 3.208E+OO 1.207E+OO 1.207E+OO 239.06 OK 92.59 4.23 5.793E+OO 1.879E+00 1.879E+OO 71.76 OK U-234 609.32 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 OK 1764.49 15.30 9.862E-01 l.052E+OO 1.052E+OO 36.70 OK U-235 89. 96 3.47 5.640E+OO 1.871E+OO 1.871E+OO 56. 87 OK 93.35 5.60 5.793E+OO l.419E+OO 1.419E+OO 71. 76 OK 143.76 10. 96* 6.467E+00 3.153E-01 3.153E-01 114. 86 OK 163.33 5.08 6.216E+OO Line Not Found Absent 185. 72 57.20 5.841E+OO 1.258E-01 1.258E-01 71. 50 OK 205.31 5.01 5.506E+OO Line Not Found Absent U-238 63.29 3.70* 3.208E+OO 1.207E+OO 1.207E+OO 239.06 OK 92.59 4.23 5.793E+OO 1.879E+OO l.879E+OO 71. 76 OK AM-243 43.53 5.90 5.190E-01 Line Not Found Absent 74.66 67.20* 4.533E+OO 1.. 873E-01 1.873E-01 59.67 OK ANH-511 511. 00 100.00* 2.663E+OO 9.783E-02 9.783E-02 79 .36 OK Flag: "*" = Keyline Page 3560 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:10:21.79 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l * *Acquisition date 3-0CT-2016 09:08:53 Sensitivity : 3.000 *
Detector ID GAM19 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
Sample date 23-NOV-2015 11:10:00 Analyst initials: MXRl *
Sample ID G405235029 Sample Quantity 1.5120E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN * ** E'ff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1 . 96-sigma ) NA-22 7.308E-02 6.009E-02 K-40 l.424E+Ol ;L.486E+OO Y-91 6.574E+02 3.685E+02 CD-109 1.980E+OO 3.109E+OO SN-126 l.234E-01 l.937E-01 BA-137M 2.945E-01 7.580E-02 CS-137 3. lllE-01 8.007E-02 TL-208 3.231E-01 8.062E-02 BI-211 3.842E-01 9.615E-01 BI-212 1.025E+OO 9.640E-01 PB-212 1.074E+OO l.310E-01 BI-214 7.577E-01 l.846E-01 PB-214 1.155E+OO 1.937E-01 RN-222 7.577E-01 1.846E-01 RA-224 2.381E+00 1.773E+OO RA-226 7.577E-01 1.846E-01 AC,...228 8.586E-01 2.947E-01 RA-228 8.586E-01 2.947E-01 TH-228 1.074E+OO l.310E-01 TH-229 1.099E-01 4.780E-01 TH-230 7.574E-01 l.846E-01 PA-231 7.782E-01 8.644E-01 TH-232 8.586E-01 2.947E-01 TH-234. 1. 207E+OO 2.828E+OO U-234 7.574E--'01 l.846E-01 U-235 3.153E-01 3.549E-01 U-238 1.207E+OO 2.828E+00 AM-243 l.873E-01 l.095E-01 ANH-511 9.783E-02 7.608E-02 Non-Identified Nuclides Nuclide BE-7 Page 3561of5809 Key-Line Activity (pCi/GRAM -1 .. 453E+01 K.L. Cnt Uncert ( 1. 96-sigma) 1. 671E+Ol MDA (pCi/GRAM ,) 8.499E-02 5.018E-01 9.545E+02 1.938E+OO l.371E-01 6.679E-02 7.055E-02 6.673E-02 3.653E-01 9.073E-01 9.802E-02 l.440E-01 3.270E-01 1.440E-01 1. 051E+Oci 1. 440E-01 2.737E-01 2.737E-01 9.802E-02 9.407E-01 1.439E-01 8.855E-01 2.737E-01 2.050E+OO 1.439E-01 3.256E-01 2.050E+OO 8.635E-02 5. 772E-02 MDA (pCi/GRAM 2.797E+Ol NOT IDENT.

NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 5.527E-03 l.712E-02 4.800E-02 NOT IDENT. SC-46 4.859E-02 4.254E-01 8.598E-01 FAIL ABUN V-48 O.OOOE+OO 2.902E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.549E+02 0.000E+OO SHORT HLIF MN-54 5.341E-02 7.338E-02 l.554E-01 NOT IDENT. C0-56 -l .196E-01 5.202E-01 l.002E+OO NOT IDENT. MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.255E-02 4.8llE-02 9.420E-02 NOT IDENT. C0-58 -4.650E-03 7.415E-Ol l.366E+OO NOT IDENT. FE-59 -3.147E+OO 7.184E+OO l.322E+Ol NOT IDENT. C0-60 1. 7 64E-03 3.682E-02 7.433E-02 NOT IDENT. ZN-65 -l.572E-01 l.983E-01 2.720E-01 NOT IDENT. GE-68 -9.278E-01 2.040E+OO 3.751E+OO NOT IDENT. AS-73 -5.050E-01 9.791E+OO l.836E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.046E+04 O.OOOE+OO SHORT HLIF SE-75 -l.882E-02 2.424E-01 4.155E-01 NOT IDENT. BR-77 O.OOOE+OO l.919E+39 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO l. ll3E+03 O.OOOE+OO SHORT HLIF RB-83 l.073E-01 7.244E-01 l.401E+OO NOT IDENT. KR-85 -3.223E-01 8.982E+OO 1.473E+Ol NOT IDENT. SR-85 -4.160E-02 l. ll2E+OO l.823E+OO NOT IDENT. RB-86 O.OOOE+OO 4 .141E+o4 O.OOOE+OO SHORT HLIF Y-88 8. 967E-02 2.204E-01 5.349E-01 NOT IDENT. NB-94 4.531E-03 3.256E-02 6.536E-02 NOT IDENT. NB-95 3.129E-01 l.035E+OO 2.106E+OO NOT IDENT. NB-95M -5.126E-02 3.181E+OO 5.462E+OO NOT IDENT. ZR-95' 4.002E-01 l.703E+OO 3.490E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 9.997E+40 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 7.075E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.348E+41 O.OOOE+OO SHORT HLIF RH-101 .,-6.025E-03 3.588E-02 6.334E-02 NOT IDENT. RH-102 2.108E-02 5.714E-02 l.140E-01 NOT IDENT. RU-103 5.562E+OO 8.283E+OO 1. 671E+Ol FAIL ABUN RH-106 -l.176E-01 5.939E-01 9.486E-01 NOT IDE.NT. RU-106 -1.17 6E-01 5.939E-01 9.486E-01 NOT IDENT. AG-108M -l.943E-03 2.940E-02 5.510E-02 FAIL ABUN AG-llOM -6.504E-02 9.867E-02 1. 764E-01 NOT IDENT. SN-ll3 -l.233E-01 2.916E-01 5.249E-01 NOT IDENT. CD-ll5 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1. 97 5E+05 O.OOOE+OO SHORT HLIF TE-123M -2.844E-02 l.300E-01 2.524E-01 NOT IDENT. SB-124 1. 719E-01 2.269E+OO 5.036E+OO FAIL ABUN SB-125 -6. 7llE-02 l.221E-01 2.154E-01 NOT IDENT. TE-125M 3.728E+Ol 3.485E+02 6.358E+02 NOT IDENT. I-126 O.OOOE+OO l.936E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.089E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.556E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.150E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.138E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 068E+28 O.OOOE+OO SHORT HLIF BA-133 -7.632E-03 4.557E-02 7. 581E-02 NOT IDEI'{T. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.499E-02 5.828E-02 l.230E-01 NOT IDENT. CS-135 2.104E-02 l.352E-01 2.635E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.600E+05 O.OOOE+OO SHORT HLIF CE-139 -2.342E-02 l.250E-01 2.409E-01 NOT IDENT. BA-140 O.OOOE+OO 3.081E+06 O.OOOE+oo* SHORT HLIF LA-140 O.OOOE+OO l.063E+06 O.OOOE+OO SHORT HLIF CE-141 -2.317E+OO 3.52'4E+Ol 6.223E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.226E+41 O.OOOE+OO SHORT HLIF CE-144 l.442E-01 4.299E-01 7.843E-01 NOT IDENT. PM-144 -l.616E-02 5.745E-02 l. ll2E-01 NOT IDENT. PR-144 -l.415E+OO 5.030E+OO 9.733E+00 NOT IDENT. PM-146 3.302E-02 4.418E-02 9.098E-02 FAIL ABUN ND-147 O.OOOE+OO 9.122E+07 O.OOOE+OO SHORT HLIF PM-147 -3.599E+02 8. 051E+02 l.558E+03 NOT I DENT.

PM-149 O.OOOE+OO l.350E+41 O.OOOE+OO SHORT HLIF EU-150 -5.813E-03 2.843E-02 4.715E-02 FAIL ABUN EU-152 2. 077E-02
9.563E-02 l.859E-01 FAIL ABUN GD-153 6.480E-02 2.002E-01 3.735E-01 NOT IDENT. EU-154 l.778E-01 l.462E-01 2.544E-01 FAIL ABUN EU-155 2.016E-02 l.094E-01 2.020E-01 FAIL ABUN TB-160 l.846E+OO 2.382E+OO 5.125E+OO FAIL ABUN H0-166M -l.935E-02 4.932E-02 9.416E-02 FAIL ABUN TM-171 -5.108E+OO l.995E+Ol 3.692E+Ol NOT I DENT .. Page 3562 of 5809 HF-172 2.179E-02 2.578E-01 4.644E-01 FAIL ABUN LU-172 -3.290E-02 7.642E-02 l.395E-01 FAIL ABUN LU-176 1. 887E-03 2.750E-02 4.748E-02 NOT IDENT. HF-1-81 1.695E-01 5.978E+00 1.128E+Ol NOT IDENT. TA-182 -7.827E-01 1.081E+00 1.834E+OO FAIL ABUN RE-183 -3. 873E-'01 3. 611E+OO 6.168E+OO NOT IDENT. RE-184 1.204E+Ol 4.234E+01 8.666E+Ol NOT IDENT. W-188 -2. 611E+Ol l.555E+02 2.594E+02 FAIL ABUN IR-192 -1.159E-01 5.398E-01 1. OllE+OO FAIL ABUN HG-203 -1.561E+OO 3.603E+OO 5.903E+OO NOT IDENT. BI-207 4.348E-02 l.364E-01 2.539E-01 FAIL ABUN PB-210 -1.349E+OO 3.389E+OO 6.214E+OO NOT IDENT. PB-211 -2.626E-01 8.082E-01 1. 296E+OO NOT IDENT. RN-219 5.338E-02 4.152E-01 7.924E-01 NOT IDENT. RA-223 8.816E-02 6.lOSE-01 1.178E+OO FAIL ABUN AC-227 1. 748E-01 4.780E-01 FAIL ABUN TH-227 1. 748E-01 4.169E-01 4.780E-01 FAIL ABUN TH-231 8.816E-02 6.105E-01 l.178E+OO FAIL ABUN PA-233 2.158E-03 6. 096E-02 1.168E-01 FAIL ABUN PA-234 5. 719E-01 4.732E-01 5.968E-01 FAIL ABUN PA-234M -1.459E+OO 4.351E+OO 8.286E+OO NOT *IDENT. NP-237 2.158E-03 6.096E-02 l.168E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 l.473E-01 2.327E-01 4.827E-01 NOT IDENT. PU-239 O.OOOE+OO 5.744E+02 6.895E+02 FAIL ABUN AM-241 -3.107E-02 1. 37 9E-01 2.326E-01 NOT IDENT .* CM-243 1. 986E-02 9.940E-02 l.840E-01 NOT IDENT. BK-247 -1.230E-02 *7. 877E-02 1.335E-01 NOT IDENT. CM-247 1.685E-03 3.922E-02 7.085E-02 NOT IDENT. CF-249 1.638E-03 4.231E-02 7.992E-02 NOT IDENT. CF-251 4.163E-02 1.130E-01 2.261E-01 NOT IDENT. Page 3563 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-:2016 10:10:19.56 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area * %Abn %Eff pCi/GRAM pCi/GRAM %Error NA-22 1274.54 15 99.94* l.297E+OO 5.808E-02 7.308E-02 83.90 K-40 1460.82 355 10.66* 1.161E+OO 1.424E+Ol 1.424E+Ol 10.65 Y-91 1204.77 11 0. 26* 1.358E+OO 1.576E+Ol 6.574E+02 57.20 CD-109 88.03 88 3.70* 5.459E+OO 2.169E+OO 3.482E+OO 90.26 SN-126 64.28 ------9.60 3.426E+OO ------Line Not Found ------86.94 88 8.90 5.459E+OO 9.018E-01 9.018E-01 90. 26 87.57 88 37.00* 5.459E+OO 2.169E-01 2.169E-01 90. 26 BA-137M 661.66 113 89.90* 2.164E+OO 2.887E-01 2.945E-01 26. 26 CS-137 661.66 113 85.10* 2.164E+OO 3.050E-01 3. lllE-01 26.26 TL-208 277.37 ------6.60 4.415E+OO ------Line Not Found ------583.19 132 85.00* 2.392E+OO 3.231E-01 3.231E-01 25.47 860.56 27 12.50 1. 764E+OO
6.089E-01 6.089E-01 60.00 BI-211 72. 87 ------1. 23 4.361E+OO ------Line Not Found ------351.06 300 12.92* 3.630E+OO 3.182E+OO 3.182E+OO 17 .11 BI-212 727. 33 28 6.67* 2.0lOE+OO 1.025E+OO 1.025E+OO 95.99 785.37 18 1.10 1.892E+00 4.277E+OO 4.277E+OO 105 .'50 1620.50 ------1. 47 1.063E+OO ------Line Not Found ------PB-212 74.82 169 10.28 4.533E+OO 1. 797E+OO 1. 797E+OO 39.57 77 .11 265 17.10 4.743E+OO 1.624E+OO 1.624E+OO 22.16 238.63 4 68 43.60* 4. 961E+OO 1.074E+OO 1.074E+00 12.45 300.09 35 3.30 4.139E+OO l.262E+OO l.262E+00 113. 35 BI-214 609.32 160 45.49* 2.309E+00 7.574E-01 7.577E-01 24.87 1120.29 41 14.92 1.437E+OO 9.465E-01 9.468E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1.052E+OO 36. 70 PB-214 74.82 169 5.80 4.533E+OO 3.185E+00 3.186E+OO 39.57 77.11 265 9.70 4.743E+OO 2.862E+OO 2.863E+OO 22.16 87.09 88 3.41 5.459E+OO 2.354E+OO 2.355E+00 90.26 242.00 169 7.25 4.913E+OO 2.362E+00 2.362E+00 41. 46 295.22 158 18.42 4.198E+OO l.015E+00 1.016E+OO 29.18 351. 93 300 35.60* 3.630E+OO l.155E+OO 1.155E+OO 17 .11 RN-222 609.32 160 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 1120.29 41 14.92 l.437E+OO 9.465E-01 9.468E-01 46.85 1764.49 32 15.30 9.862E-01 l.052E+OO 1.052E+OO 36. 70 RA-224 240.99 169 4.10* 4.913E+OO 4.176E+00 4.176E+OO 41. 46 RA-226 609.32 160 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 1120.29 41 14.92 1. 437E+OQ 9.465E-01 9.468E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 AC-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 63 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 794.95 ------4.25 1. 875E+OO ------Line Not Found ------835. 71 ------1. 61 1. 803E.+00 ------Line Not Found ------911. 20 75 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 968.97 53 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 RA-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 63 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 794.95 ------4.25 1.875E+OO ------Line Not Found ------835.71 ------1. 61 1.803E+OO ------Line Not Found ------Page 3564 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 75 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 968. 97 53 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 TH-228 74.82 169 10.28 4.533E+OO 1..7 97E+OO 1. 797E+00 39.57 77 .11 265 17.10 4.743E+OO 1.624E+OO L 624E+OO 22.16 238.63 468 43.60* 4. 961E+OO 1. 074E+OO 1.074E+OO 12.45 300.09 35 3.30 4.139E+OO 1. 2 62E+OO 1.262E+OO 113. 35 TH-229 85.43 88 14.70 5.459E+OO 5.460E-01 5.460E-01 90.26 88.47 74 24.00 5.640E+00 2.705E-01 2.705E-01 56.87 193.51 ------4.41* 5.711E+00 ------Line Not Found ------210.85 47 2.80 5.435E+OO 1.529E+OO 1.529E+00 101.84 TH-230 609.32 160 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 1120.29 41 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO l.052E+OO 36.70 PA-231 283.69 ------1. 70 4.336E+OO ------Line Not Found ------301.36 35 5.35* 4.139E+OO 7.782E-01 7.782E-01 113. 35 TH-232 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 63 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 835. 71 ------1. 61 1.803E+OO ------Line Not Found ------. 911. 20 75 25.80* 1.687E+00 8.586E-01. 8.586E-01 35.02 968. 97 53 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 TH-234 63.29 29 3.70* 3.208E+OO 1.207E+OO 1.207E+OO 23.9.06 92.59 93 4.23 1.879E+OO 1.879E+OO 71. 76 U-234 609.32 160 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 1120.29 41 14.92 1.437E+00 9.465E-01 '9. 465E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO l.052E+00 36.70 U-235 89. 96 74 3.47 5.640E+OO 1. 871E+OO 1.871E+OO 56.87 93.35 93 5.60 5.793E+OO 1.419E+OO l.419E+OO 71. 76 143.76 A5 10.96* 6.467E+OO 3.153E-01 3.153E-01 114. 8 6 163.33 ------5.08 6.216E+OO ------Line Not Found ------185.72 85 57.20 5.841E+OO 1.258E-01 l.258E-01 71. 50 205.31 ------5.01 5.506E+OO ------Line Not Found ------U-238
63.29 29 3.70* 3.208E+OO 1.207E+OO 1.207E+OO 239.06 92.59 93 4.23 5.793E+OO 1.879E+OO 1.879E+OO 71. 76 AM-243 43.53 ------5.90 5.190E-01 ------Line Not Found ------74.66 169 67.20* 4.533E+OO 2.749E-01 2.749E-01 39.57 ANH-511 511. 00 52 100.00* 2.663E+OO 9.783E-02 9.783E-02 79.36 Flag: "*" Key line Page 3565 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Total number of lines in spectrum 51 Number of unidentified lines 11 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide NA-22 K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226
AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 2.60Y 1.25E+09Y 58. 510 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1.41E+l0Y 1.41E+10Y 1600. OOY 1600.00Y 1600. OOY 1.41E+10Y 1600. OOY 1.41E+l0Y 1.41E+10Y 1. 41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 26 1. 00 41. 7 1. 60 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 i. oo* 1. 00 1. 00 1. 00 1. 0.0 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 i.*oo Total Activity Grand Total Activity Uncorrected pCi/GRAM 5.808E-02 1.424E+Ol 1.576E+Ol 2.169E+OO 2.169E-01 2.887E-01 3.050E-01 3. 231E-01 3.182E+OO 1.025E+OO 1. 074E+OO 7.574E-01 1.155E+OO 7. 5.74E-01 4.176E+OO 7.574E-01 8.586E-01 8.586E-01 1.074E+OO 2.705E-01 7.574E-01 7.782E-01 8.586E-01 1.207E+OO 7.574E-01 3.153E-01 1.207E+OO 2.749E-01 9.783E-02 5.556E+Ol 5.556E+Ol Decay Corr pCi/GRAM 7.308E-02 1.424E+Ol 6.574E+02 3.482E+OO 2.169E-01 2.945E-01 3. lllE-01 3. 231E-01 3.182E+OO 1.025E+OO 1.074E+OO 7.577E-01 1.155E+00 7.577E-01 4.176E+OO 7.577E-01 8.586E-01 8.586E-01 1. 0.74E+OO 2.705E-01 7.574E-01 7.782E-01 8.586E-01 1.207E+OO 7.574E-01 3.153E-01 1.207E+OO 2.749E-01 9. 783E-02 . 6.986E+02 6.986E+02 78.43% Decay Corr 2-Sigma Error 6.132E-02 0.152E+Ol 3.760E+02 3.142E+OO l.958E-01 0.773E-01 0.817E-01 0.823E-01 0.544E+OO 0 .. 984E+00 0.134E+OO 1.884E-01 0.198E+OO l.884E-01 1.731E+OO 1.884£.'...0l 3.007E-01 3.007E-01 0.134E+OO 1.539E-01 l.883E-01 8. 821E-01 3.007E-01 2.886E+00 l.883E-01 3. 621E-01 2.886E+00 1.088E-01 7.763E-02 "M" Manually accepted 2-Sigma %Error 83.90 10.65 57.20 90. 26 90. 26 26 .26 26.26 25.47 17 .11 95.99 12.45 24.87 17 .11 24.87 41. 46 24.87 35.02 35.02 12.45 56. 87 24.87 113. 35 35.02 239.06 24.87 114. 86 239.06 39.57 79.36 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3566 of 5809 Flags K

' Unidentified Energy Lines Page : 4 Sample ID : G405235029 Acquisition date : 3-0CT-2016 09:08:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.14 62 143 0.79 259.12 256 8 1. 41E-02 78.5 6.54E+OO T 0 255.93 16 93 0.57 512.80 509 9 3.79E-03 **** 4.70E+OO T 0 274.31 94 232 8.38 549.58 533 28 2.28E-02 **** 4.45E+OO T 0 410.33 32 75 2.16 821. 74 812 13 7.98E-03 **** 3.19E+OO T 0 625.69 18 8 0.91 1252.65 1249 8 4.72E-03 75.3 2.26E+OO 1 723.01 15 36 1. 98 1447.36 1440 27 4.06E-03 **** 2.02E+OO T 0 748.16 15 10 1. 39 1497.69 1494 10 3.92E-03 **** l.97E+OO T 8 781.40 13 16 2.20 1564.19 1561 17 3.50E-03 **** 1. 90E+OO 0 804.73 17 25 1. 55 1610.87 1605 12 4.61E-03 **** 1. 86E+OO 0 946.99 23 13 4.32 1895.53 1886 17 6.21E-03 84.4 1.64E+OO T 4 963. 76 18 15 2.84 1929.07 1920 23 4.95E-03 **** 1.62E+OO T 0 1063.76 10 22 1. 73 2129.16 2121 15 2.67E-03 **** 1.50E+OO T 0 1134. 69 13 15 3.50 2271. 08 2263 15 3.61E-03 **** 1.42E+OO 0 1143.20 15 12 3.51 2288.11 2282 12 4.16E-03 **** 1. 41E+OO 0 1168.70 19 12 1.24 2339.14 2333 13 5.26E-03 90.3 1.39E+OO 0 1200.59 13 9 3.91 2402.95 2394 14 3.55E-03 **** 1.36E+00 3 1207.52 13 1 2.05 2416.82 2407 13 3.70E-03 56.6 1.35E+OO 0 1236.70 32 27 8.17 2475.21 2464 27 8.92E-03 97.0 1.33E+OO T 0 1263.32 9 8 1.37 2528.47 2521 12 2.57E-03 **** 1.31E+OO 1 1272.80 19 6 2.30 2547.42 2542 19 5.48E-03 63.4 l.30E+00 T 0 1280.93 6 3 1. 39 2563.69 2560 7 1. 81E-03 **** 1.29E+OO 0 1511. 05 7 5 1. 34 3024.1'4 3017 10 l.94E-03 **** 1.13E+OO Flags: "T" = Tentatively associated Page 3567 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:10:34.27 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l *
Acquisition date 3-0CT-2016 09:08:53 Sensitivity : 3.000 *
Detector ID GAM19 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.76 Half .life ratio : ***** *
Sample date 23-NOV-2015 11:10:00 Nuclide Library : SOLID *
Sample ID G405235029 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.5120E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7 *' Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.592E-02 1. 963E-01 3.970E+02 9.125E-01 6.504E-02 2.978E-02 3.146E-02 2.997E-02 1.678E-01 4.024E-01 4.576E-02 6.542E-02 1.582E-01 6.542E-02 4.905E-01 6.542E-02 1.212E-01 l.212E-01 4.576E-02 4.423E-01 6.540E-02 4. lllE-01 1.212E-01 9.659E-01 6.540E-02 l.528E-01 9.659E-01 4.080E-02 2.626E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-24 Page 3568 of 5809 Le (pCi/GRAM 1.256E+Ol NOT IDENT. O.OOOE+OO SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU...:.103 RH-106 RU-106 AG-108M AG-110M SN-.113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3569 of 5809 1.701E-02 3.761E-01 O.OOOE+OO O.OOOE+OO 7.005E-02 4.361E-01 O.OOOE+OO 4.424E-02 6. 015E-01. 5.496E+OO ' 3 .110E-02 1.132E-01 1.556E+OO 8.631E+OO O.OOOE+OO 1. 917E-01 O.OOOE+OO O.OOOE+OO 6.265E-01 6.727E+OO 8.326E-01 O.OOOE+OO 2.123E-01 2.934E-02 9.456E-01 2.560E+OO 1. 549E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO o*. OOOE+OO 2.975E-02 5.057E-02 7. 631E+OO 4.193E-01 4.193E-01 2.503E-02 7. 513E-02 2.409E-01 O.OOOE+OO O.OOOE+OO 1.178E-01 1.998E+OO 9.828E-02 2.992E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.459E-02 O.OOOE+OO 5.580E-02 1.221E-01 O.OOOE+OO O.OOOE+OO 1.135E-01 O.OOOE+OO O.OOOE+OO 2.923E+Ol O.OOOE+OO 3.710E-01 4.951E-02 4.335E+OO . 4 .144E-02 O.OOOE+OO 7.308E+02 O.OOOE+OO 2.162E-02 8.553E-02 1. 765E-01 1.112E-01 9.483E-02 2.294E+OO 4.085E-02 1. 728E+Ol 2.189E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.
FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT . FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3570 of 5809 5.959E-02 2.190E-02 5.107E+OO 7.907E-01 2.900E+OO 3.830E+Ol l.203E+02 4.643E-01 2.739E+OO 1.208E-01 2.914E+OO 5. 911E-01 3.638E-01 5.439E-01 2.233E-01 2.233E-01 5.439E-01 5.388E-02 2.637E-01 3.626E+00 5.388E-02 O.OOOE+OO 2.275E-01 3.275E+02 1.091E-01 8.638E-02 6.165E-02 3.244E-02 3.680E-02 l.062E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. 'FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:10:40.06 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *-. * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l * *Acquisition date 3-0CT-2016 09:08:53 Sensitivity : 3.000 *
Detector ID GAM19 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 Half life ratio : ***** *
Sample date 23-NOV-2015 11:10:00 Nuclide Library : SOLID *
Sample ID G405235029 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.5120E+02 GRAM *
Quantity Err(%) : 1.3227E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * * *' Eff. Cal. date 15-JUN-2016 10:35:16 Ef'f. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 7.308E-02 6.015E-02 K-40 1. 424E+Ol 1.663E+OO Y-91 6.574E+02 3.693E+02 CD-109 1.980E+OO 3 .119E+OO SN-126 l.234E-01 1.942E-01 BA-137M 2.945E-01 7.686E-02 CS-137 3. lllE-01 B .119E-02 TL-208 3. 231E-01 8.180E-02 BI-211 3.842E-01 9.768E-01 BI-212 1.025E+OO 9.654E-01 PB-212 1.074E+OO 1.428E-01 BI-214 7.577E-01 1. 875E-01 PB-214 l.155E+OO 1. 996E-01 RN-222 *7.577E-01 1. 87 5E-01 RA-224 2.381E+OO 1.781E+OO RA-226 7.577E-01 1. 87 5E-01 AC-228 8.586E-01 2.980E-01 RA-228 8.586E-01 2.980E-01 TH-228 1.074E+OO 1.428E-01 TH-229 1.099E-01 4.781E-01 TH-230 7.574E-01 1.874E-01 PA-231 7.782E-01 8.802E-01 TH-232 8.586E-01 2.980E-01 TH-234 1.207E+OO 2.841E+OO U-234 7.574E-01 1.874E-01 U-235 3.153E-01 3.553E-01 U-238 1.207E+OO 2.841E+OO AM-243 l.873E-01 1.107E-01. ANH-511 9.783E-02 7.619E-02 Non-Identified Nuclides Nuclide BE-7 Page 3571of5809 Key-Line Activity (pCi/GRAM -1.453E+Ol K.L.Act error ( 1. 96-sigma) 1.672E+Ol TPU ( 1. 96-sigma) 6.015E-02 l.663E+00 3.693E+02 3 .119E+OO 1.942E-01 7.686E-02 8 .119E-02 8.180E-02 9.768E-01 9.654E-01 1.428E-01 1.875E-01 1. 996E-01 l.875E-01 1.781E+OO 1.875E-01 2.980E-01 2.980E-01 1.428E-01 4.781E-01 l.874E-01 8.802E-01 2.980E-01 2.841E+OO 'l.874E-01 3.553E-01 2.841E+OO 1.107E-01 7.619E-02 TPU (1. 96-sigma) l.796E+Ol NOT IDENT.

NA-24 l.000E+41 3.370E+41 O.OOOE+OO SHORT HLIF AL-26 5.527E-03 1. 712E-02 1.730E-02 NOT IDENT. SC-46 4.859E-02 4.254E-01 4.259E-01 FAIL ABUN V-48 8.593E+03 2.902E+04 2.927E+04 SHORT HLIF CR-51 2.128E+02 6.550E+02 6.619E+02 SHORT HLIF MN-54 5.341E-02 7.342E-02 7.727E-02 NOT IDENT. C0-56 -l .196E-01 5.203E-01 5.230E-01 NOT IDENT. MN-56 -1.000E+41 4.574E+41 *O.OOOE+OO SHORT HLIF C0-57 -1.255E-02 4.811E-02 4.844E-02 NOT IDENT. C0-58 -4.650E-03 7.415E-01 7.415E-01 NOT IDENT. FE-59 -3.147E+OO 7.188E+OO 7.326E+OO NOT IDENT. C0-60 1. 7 64E-03 3.682E-02 3.683E-02 NOT IDENT. ZN-65 -1.572E-01 1. 984E-01 2.107E-01 NOT IDENT. GE-68 -9.278E-01 2.040E+OO 2.083E+OO NOT IDENT. AS-73 -5.050E-01 9.792E+OO 9.795E+OO NOT IDENT. AS-74 6.443E+03 l.048E+04 1.087E+04 SHORT HLIF SE-75 -l.882E-02 2.424E-01 2.426E-01 NOT IDENT. BR-77 l.573E+40 1.430E+41 O.OOOE+OO SHORT HLIF SR-82 3.226E+02 l .113E+03 l.123E+03 SHORT HLIF RB-83 l.073E-01 7.245E-01 7.261E-01 NOT IDENT. KR-85 -3.223E-01 8.982E+OO 8.983E+OO NOT IDENT. SR-85 -4.160E-02 l.112E+00 1.112E+OO NOT IDENT. RB-86 -l.883E+04 4 .142E+0*4 4.228E+04 SHORT HLIF Y-88 8. 967E-02 2.205E-01 2.242E-01 NOT IDENT. NB-94 4.531E-03 3.256E-02 3.263E-02 NOT IDENT. NB-95 3.129E-01 1.035E+OO 1.045E+OO NOT IDENT. NB-95M -5.126E-02 3.181E+OO 3.181E+OO NOT IDENT. ZR-'95 4.002E-01 1. 703E+OO 1. 713E+OO FAIL ABUN NB-97 -1.000E+41 2.803E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.001E+41 O.OOOE+OO SHORT HLIF M0-99 2.584E+33 7.077E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 l.352E+41 O.OOOE+OO SHORT HLIF RH-101 -6.025E-03 3.589E-02 3.600E-02 NOT IDENT. RH-102 2.108E-02 5.717E-02 5.795E-02 NOT IDENT. RU-103 5.562E+OO 8.287E+OO 8.658E+OO FAIL ABUN RH-106 -1. l 76E-01 5.939E-01 5. 963E-01 NOT IDENT. RU-106 -l.176E-01 5.939E-01 5.963E-01 NOT IDENT. AG-108M -1.943E-03 2.940E-02 2. 941E-02 FAIL ABUN AG-llOM -6.504E-02 9. 872E-02 l.030E-01 NOT IDENT. SN-113 -l.233E-01 2.916E-01 2. 969E-01 NOT IDENT. CD-115 -l.OOOE+41 2.080E+41 O.OOOE+OO SHORT HLIF SN-117M -4.185E+04 1. 97 6E+05 l.985E+05 SHORT HLIF TE-123M -2.844E-02 1.300E-01 1.307E-01 NOT IDENT. SB-124 1.719E-01 2.269E+OO 2.271E+OO FAIL ABUN SB-125 -6. 711E-02 l.221E-01 l.258E-01 NOT I DENT*. TE-125M 3.728E+Ol 3.486E+02 3.490E+02 NOT IDENT. I-126 3.262E+05 1.936E+06 1.942E+06 SHORT HLIF SB-126 8.123E+04 3.089E+06 3.089E+06 SHORT HLIF SB-127 -l.859E+23 4.455E+23 O.OOOE+OO SHORT HLIF I-131 3.083E+09 2.150E+10 2.155E+10 SHORT HLIF I-132 -1.000E+41 l.944E+42 O.OOOE+OO SHORT HLIF TE-132 -3.774E+27 1.080E+28 O.OOOE+OO SHORT HLIF BA-133 -7.632E-03 4.557E-02 4.570E-02 NOT IDENT. I-133 -l.OOOE+4i 7.518E+41 O.OOOE+OO SHORT*HLIF CS-134 4.499E-02 5.831E-02 6.174E-02 NOT IDENT. CS-135 2.104E-02 1.352E-01 l.355E-01 NOT IDENT. I-135 1.000E+41 7.389E+41 O.OOOE+OO SHORT HLIF CS-136 9.174E+04 7. 601E+05 7.612E+05 SHORT HLIF CE-139 -2.342E-02 1. 251E-01 l.255E-01 NOT IDENT. BA-140 8.583E+04 3.081E+06 3.081E+06 SHORT HLIF LA-140 -8.895E+05 1.064E+06 1.137E+06 SHORT HLIF CE-141 -2.317E+OO 3.524E+Ol 3.525E+Ol NOT IDENT. CE-143 l.000E+41 1.230E+41 O.OOOE+OO SHORT HLIF CE-144 1.442E-01 4.300E-01 4.348E-01 NOT IDENT. PM-144 -1.616E-02 5.746E-02 5.792E-02 NOT IDENT. PR-144 -l.415E+00 5.030E+OO 5.070E+OO NOT IDENT. PM-146 3.302E-02 4.424E-02 4.668E-02 FAIL ABUN ND-147 4.440E+07 9.125E+07 9.342E+07 SHORT HLIF PM-147 -3.599E+02 8.053E+02 8.214E+02 NOT IDENT. PM-149 -l.OOOE+41 1.368E+41 O.OOOE+OO SHORT HLIF EU-150 -5.813E-03 2.843E-02 2.855E-02 FAIL ABUN EU-152 2.077E-02 9.564E-02 9.609E-02 FAIL ABUN GD-153 6.480E-02 2.002E-01 2.023E-01 NOT IDENT. EU-154 1.778E-01 l.464E-01 l.669E-01 FAIL ABUN EU-155 2.016E-02 1.094E-01 1.098E-Ol FAIL ABUN TB-160 1.846E+OO 2.384E+OO 2.525E+00 FAIL ABUN H0-166M -1.935E-02 4.933E-02 5.009E-02 FAIL ABUN TM-171 -5.108E+OO 1. 996E+01 2.009E+Ol NOT IDENT. Page 3572 of 5809 HF-172 2.179E-02 2.579E-01 2.581E-01 FAIL ABUN LU-172 -3.290E-02 7.649E-02 7.791E-02 FAIL ABUN LU-176 1.887E-03 2.750E-02 2.751E-02 NOT IDENT. HF-181 1.695E-01 5.978E+OO 5.978E+OO NOT IDENT; TA-182 -7.827E-01 1.081E+OO l.138E+OO FAIL ABUN RE-183 -3.873E-01 3.612E+OO 3.616E+OO NOT IDENT. RE-184 1. 204E+Ol 4.245E+Ol 4.279E+Ol NOT IDENT. W-188 -2. 611E+Ol l.556E+02 1. 560E+02 FAIL ABUN IR-192 -l.159E-01 5.398E-01 5.423E-01 FAIL ABUN HG-203 -1. 561E+OO 3.604E+OO 3. 672E+OO NOT IDENT. BI-207 4.348E-02 l.364E-01 l.378E-Ol FAIL ABUN PB-210 -1.349E+OO 3.391E+OO 3.445E+OO NOT IDENT. PB-211 -2.626E-01 8.083E-01 8.170E-01 NOT IDENT. RN-219 5.338E-02 4.152E-01 4.159E-01 NOT IDENT. RA-223 8.816E-02 6.lOSE-01 6.118E-01 FAIL ABUN AC-227 1.748E-01 4.176E-01 4.249E-01 FAIL ABUN TH-227 l.748E-01 4.176E-01 4.249E-01 FAIL ABUN TH-231 8.816E-02 6.lOSE-01 6 .118E-01 FAIL ABUN PA-233 2.158E-03 6.096E-02 6. 096E-02 FAIL ABUN PA-234 5.719E-01 8.074E-01 8.476E-01 FAIL ABUN PA-234M -1.459E+OO 4.352E+OO 4. 401E+OO NOT IDENT. NP-237 2.158E-03 6. 096E-02 6. 096E-02 FAIL ABUN NP-238 l.OOOE+41 3.756E+41 O.OOOE+OO SHORT HLIF NP-239 1.473E-01 2.330E-01 2.423E-01 NOT IDENT. PU-239 7.470E+02 5.753E+02 6.666E+02 FAIL ABUN AM-241 -3.107E-02 1.379E-01 1. 386E-01 NOT IDENT. CM-243 l.986E-02 9.941E-02 9.982E-02 NOT IDENT. BK-247 -l.230E-02 7.881E-02 7.900E-02 NOT IDENT. CM-247 1.685E-03 3.922E-02 3.922E-02 NOT IDENT. CF-249 l.638E-03 4.231E-02 4.232E-02 NOT IDENT. CF-251 4.163E-02 1.131E-01 l.147E-01 NOT IDENT. Page 3573 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.6616 879.38 112.8485 482.18 100.1077 45.60 62. 8962 87.57 112.8741 133.52 92.4598 46.54 79.9083 87.09 112.8991 264.66 89.2840 49. 72 0.0000 87.57 112.9795 122.06 100. 4969 51. 35 69.3568 88.03 87.2150 140.51 0.0000 51. 87 78.5368 88.34 87.2545 143.76 77.0593 52.39 77.4805 193.51 87.2715 144.24 81.8637 52.97 75.2901 89. 96 92.3206 145.44 81. 9684 53.44 83.3542 90. 6.4 92.4122 152.43 110.0975 125.81 70.8834 91.11 0.0000 153.25 0.0000 57.36 0.0000 63.29 92.6714 154.21 88.4151 57.53 81.7246 143.76. 92.7717 156.02 0.0000 57.98 86.0189 94.56 89.6704 158.56 0.0000 1093.63 87.7696 94.65 92.9427 159.00 70.3743 57.98 87.7779 94.67 92.9456 162.33 73.2574 59.54 83.1923 94.87 92.9717 162.66 0.0000 60. 96 77.2344 . 97. 43 83.4825 163.33 66.2621 61.17 8*8.0817 311. 90 78.6802 165.86 92 .1119 62.93 88.3663 946.00 78.6816 176.31 78.7268 63.29 88.4241 99.53 75.1051 1048.07 0.0000 63.58 88.4705 1221.41 107.2021 177.52 71. 6512 64.28 97.9062 265.00 79.0664 739.50 0.0000 66.73 112.3799 103.18 73.0014 181.52 78.2110 67.24 106.6219 103.37 73.0199 711. 68 63.5464 67. 68 103.1861 116.74 73.0199 185.72 78.5128 67.75 96 .1619 105,21 74.4388 193.51 77.2448 69.67 106.6782 105.31 74.4484 197.03 88.4233 70.83 111. 6041 106.12 78.2544 127.23 71.1644 72.81 98.1750 106.47 78.2900 306.78 85.1299 279.20 98.1851 109.28 82.3177 203.43 78.8307 72. 87 98.1851 111. 00 88.7489 205.31 68.8576 74.66 98.4751 228.16 0.0000 210.85 71.0243 74.82 98.5004 114. 06 85.3279 215.65 72. 2339 1063.66 98. 5245 116.30 0.0000 222 .11 80.0616 238.63 98.8665 116.74 73.8615 290.67 77.5769' 351.93 98.8665 119.76 81. 7165 177.52 74.7908 78.74 98.7248 121.12 86.9136 228.16 0.0000 79.69 86.1152 121. 22 86.9241 228.18 74.8381 80.12 86.1735 121.78 86.1382 235.69 74.8086 80.19 0.0000 122.06 86.1673 256.23 65.8828 80.57 95.8154 122.92 83.7191 238.63 66.0181 81. 00 97.4775 123.07 86.2711 238.98 0.0000 81. 07 110.2734 123.68 82.9482 240.99 66.1377 81. 75 100.7908 125.81 87.8240 242.00 66.1883 323.87 93.0818 127.23 84.1448 344.28 66.3235 84.00 93 .1119 127.91 88.0399 252.40 0.0000 85.43 112. 6192 129.30 85.1990 252.80 48.6146 86.55 112.8086 131. 20 96. 0583 254.15 0.0000 Page 3574 of 5809 ENERGY MDA COUNTS ENERGY: MDA COUNTS *ENERGY MDA COUNTS 256.23 56.3820 351. 93 42.7203 583.19 26.1651 260.90 0.0000 507.63 0.0000 584.27 26.1773 264.66 49.0348 356.01 39.7633 595.83 0.0000 264.80 51..9247 364.49 0.0000 600.60 28.6407 265.00 51.9313 366.42 0.0000 602.52 0.0000 268.22 50.1232 372. 51 32.9355 604.72 30.9825 269.46 50.1666 129.30 38.1359 607.14 33.3094 270.03 50.1867 377.52 35.0922 609.32 33.3377 271.23 50.2290 383.85 45.5737 497.08 33.3507 273.65 0.0000 388.16 44.6429 433.94 10.3663 356.01 50. 4110 388.63 0.0000 696.49 23.0705 277.37 50.4448 391.69 49.9297 620.36 11. 5454 277.60 50.4533 400.66 39.7194 621. 93 22.5278 278.00 50.4670 401.81 39.7434 667.71 0.0000 279.20 61.1927 402.40 38.9195 631. 29 16.2319 279.54 64.1215 404.85 42.4273 453.88 23.2064 279.70 64.1295 410.95 39.4104 595.83 0.0000 280.46 55.4136 413.71 52.0973 635.95 24.3915 283.69 58.4583 414.70 0.0000 636.99 0.0000 364.49 0.0000 423.72 0.0000 645.85 30.3132 285.41 56.5757 404.85 39.2116 884.68 32.3224 285.90 0.0000 427.87 46.6479 657.90 0.0000 402.40 46.8877 433.94 34.0306 661. 66 22.8698 290.67 52.8618 333.97 33.0573 664.57 0.0000 293.27 0.0000 453.88 23.6288 666.33 0.0000 295.22 55.9679 463.37 20.5006 720.70 0.0000 295. 96 55.9946 468.07 25.9541 667. 71 0.0000 298.58 56.0920 685.70 0.0000 677. 62 17.6953 299.98 56.1430 475.06 34.7207 685.70 0.0000 300.09 56.1476 476.78 33.6628 .695.00 0.0000 300.13 56.1488 477.60 40.1940 696.49 23.1610 301.36 56.1940 482.18 30.4826 696. 51 23.1610 302.85 56.2485 1596.21 0.0000 697.00 0.0000 304.50 47.4180 527.90 0.0000 697.30 21. 3853 537.26 . 0. 0000 497.08 26.3081 697.49 22.2778 306.78 46.0043 505.52 19.8073 702.65 24.1046 316.51 43.5775 507.63 0.0000 706.68 24.1383 311. 90 46.6519 511. 00 34 .1964 711. 68 18.8076 3lq. 51. 46.7877 514.00 38.1078 720.70 0.0000 531. 02 0.0000 514.00 38.1078 721. 93 0.0000 320.08 0.0000 520.40 22.1549 1690.97 20.6788 427.87 48.9183 238.98 0.0000 722.91 20.6795 323.87 46.0037 522.65 0.0000 1274.44 20.6823 325.23 54.0505 527.90 0.0000 724 .19 20.6886 328.76 0.0000 528.26 25.5662 727.33 20.7111 388.16 51.9065 520.40 28.9178 733.00 14.4360 333.97 45.2838 529.87 0.0000 735.93 25.8048 334.37 49.8243 531. 02 0.0000 737.46 14.4580 338.28 45.4019 537.26 0.0000 . 739.50 0.0000 911.20 45.4037 546.56 0.0000 747.24 20.3089 340.48 45.462T 552.55 22.4650 748.06 16.3240 340.55 0.0000 563.25 33.8489 752.31 24.7023 344.28 40.5029 795.86 31.6732 753.82 0.0000 345.93 36.4885 569.50 29.4129 756.73 18.1909. 351.06 42.6990 569.70 29.4150 756.80 19.1005 Page 3575 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 763.94 26.4406 984.45 0.0000 1596.21 0.0000 765.81 21.8950 996.26 16.6176 1620.50 3.3697 766.42 13. 6871 1001.03 15.6606 1621. 92 3.3706 766.84 14.6016 1002.74 16.6467 1678.03 0.0000 772.60 0.0000 1004.73 17.6358 1690.97 4.5510 776.52 0.0000 1021.30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 1. 8441 778.90 20.5235 1028.54 0.0000 1770.23 11. 0760 783.70 0.0000 846.77 11. 8 616' 1771.35 3.4618 727.33 14.6909 1038.76 0.0000 1791.20 0.0000 792.07 25.7655 1046.59 16.8423 1808.65 0.9291 794.95 23.0263 1048.07 0.0000 846.75 0.0000 795.86 21.1898 1049.04 19.8267 1836.06 2.8000 801.95 19.2010 621.93 19.8340 810.06 20.7313 .1063.66 10.9463 810.29 19.2518 1077.00 0.0000 810.45 18.5126 1077.34 11. 9832 810.76 18.5144 1085.87 11. 0087 815.77 0.0000 1093.63 16.0439 818.51 0.0000 1099.45 12.0513 832.01 19.5709 1112. 07 11. 0819 834.85 18.6554 1112. 84 13.0992 835.71 21. 4593 1115. 54 17.7461 1260.41 ' 0. 0000 609.32 li.1041 846.75 0.0000 889.28 11. 104 7 846.77 17.7876 1121.30 11. 3094 856.80 0.0000 1129. 67 14.5705 860.56 14.1023 1131.51 0.0000 702.65 16.0335 1147.95 0.0000 873.19 12.2688 1173.23 6.5445 529.87 0.0000 1177.95 16.3799 879.38 15.1279 1189.05' 13.3436 880.51 17.0250 1204.77 8.2422 '883.24 18.9319 1221.41 21. 7191 884.68 17.9928 1231.02 18.2435 889.28 15.1729 1235.36 0.0000 903.28 18.0468 1238.28 10.3827 898.04 18.0641 1260.41 0.0000 900.72 19.0302 1271.87 10.0441 903.28 16.1876 1274.44 10.0500 911. 20 20.0425 1274.54 -10.0500 912.08 20.0477 1099.45 4.2034 923.98 0.0000 1298.22 0.0000 926.50 16.2970 1312 .11 0.0000 929 .11 13.4313 1332.49 8.4824 937.49 19.2334 1362.66 0.0000 944.13 0.0000 1365.19 9.6103 946.00 10.6039 1368.63 0.0000 949.00 10.8059 1384.29 6.4325 954.55 0.0000 1408.01 8. 6196 962. 31 8. 7157 1457.56 0.0000 '964.08 8.7201 1460.82 4.3564 .966.17 8.7251 696. 51 5.4764 968. 97 9.3141 1505.03 5 .. 2740 983.53 0.0000 1584.12 11.1560 Page 3576 of 5809 Nuclide Identification Report Generated 3-0CT-2016 10:11:09.21 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road
Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date : 23-NOV-2015 14:44:00 Acquisition date : 3-0CT-2016 09:09:22. Sample ID : G405235030 Sample quantity : 1.31120E+02 GRAM Detector name : GAM20 Detector geometry: CAN . Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:15.23 0.4% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 3 3 3 4 3 5 3 6 3 7 3 8 3 9. 0 10 0 11 0 12 4 13 4 14 0 15 1 16 1 17 0 18 0 19 1 20 1 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 '34 0 Energy 63.17* 74.94 77.25 87.53 90.08* 92.88* 129.39 131.32 161.55 186.00* 208.97 238.54* 241.80 270.50 295.18* 300.19 327.64 338.27* 351.92* 355.92* 416.83 463.17 510.97* 583.15* 609.31* 657. 2 6 661.74* 710. 81 727.71 860.58 911. 09* 922.69 969. 00 1001.87* Page 3577 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 43 159 261 112 53 129 41 24 27 133 59 490 131 21 162 38 36 68 231 13 11 34 40 175 164 19 26 10 37 32 86 17 57 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 187 178 153 173 130 138 111 93 63 130 86 48 65 75 65 69 51 60 50 34 17 27 53 18 50 9 11 14 39 20 16 10 24 3 1. 39 1.17 1. 22 1. 32 1.19 1. 48 1.36 1.14 1. 56 1. 69 1. 23 1.21 1. 85 2.05 1. 27 1. 51 1. 31 1. 03 1. 55 1. 56 1. 33 1. 62 1. 72 1. 56 1. 46 1. 53 0.62 1. 33 1. 38 1. 75 1. 67 4.74 2.10 1.31 126.50 150.02 154.64 175.17 180.28 185.86 258.84 262.70 323.13 372. 01 417.91 477.02 483.56 540.93 590.27 600.27 655.16 676.42 703.72 711.72 833.50 926.18 1021. 77 1166.14 1218.47 1314.39 1323.34 1421.52 1455.33 1721.19 1822.28 1845.49 1938.18 2003.97 123 145 145 171 1"71 171 254 254 321 366 415 472 472 539 585 585 650 671 699 699 830 922 1016 1157 1213 1306 1319 1417 1449 1712 1815 1837 1933 2000 9 l.20E-02 60.3 15 4.42E-02 15.9 1.23E+OO 15 7.26E-02 10.4 21 3.llE-02 21.2 2.21E+OO 21 1.46E-02 38.5 21 3.59E-02 21.l 12 l.13E-02 47.8 1.57E+OO 12 6.80E-03 72.2 6 7.50E-03 50.3 13 3.69E-02 20.5 9 1.64E-02 30.9 26 1.36E-01 5.2 1.lOE+OO 26 3.63E-02 18.0 8 5.75E-03 77.9 20 4.51E-02 11.4 2.45E+OO 20 1. 07E-02 41. 5 9 9.89E-03 38.0 10 1.88E-02 24.9 17 6.40E-02 8.7 5.15E+OO 17 3.59E-03101.2 6 3.14E-03 64.3 11 9.55E-03 33.0 13 1.llE-02 47.3 18 4.87E-02 9.6 13 4.57E-02 12 .. 0 14 5.14E-03 43.5 9 7 .23E-03 31. 7 9 2.76E-03 77.6 12 1.03E-02 37.4 17 8.87E-03 37.4 13 2. 38E,--02 14. 7 12 4.81E-03 42.4 11 1.59E-02 2J,.4 7 2.81E-03 48.7 Peak Search Report (continued) Page : 2 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1121. 07 37 37 1. 65 2242.58 2237 15" 1.04E-02 37.9 36 0 1238.15 21 11 2.37 2477.01 2472 9 5.79E-03 36.3 37 0 1432.30 6 4 1.39 2865.83 2861 8 1. 67E-03 70.7 38 0 1460.87* 386 'o 2. 07 2923.05 2916 13 1.07E-01 5.1 39 0 1504.53 8 3 0.56 3010.52 3004 10 2.31E-03 49.9 40 0 1729.83 18 2 1. 32 3461. 94 3457 10 4.92E-03 28.9 41 0 1764.61 44 12 2.38 3531.63 3522 15 1.23E-02 22.4 42 0 1846.37 16 0 1. 04 3695.50 3690 11 4.44E-03 25.0 Flag: "*" = Peak area was modified by background subtraction* Page 3578 of ?809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:11:11 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 14:44:00 G405235030 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:09:22 131.12 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA20 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3579 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214
PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real Half life ratio Systema.tic Error Efficiencies at Interfered Nuclide RA:-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-2il . Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:15.23 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.312E+OO l.507E+Ol 1.507E+Ol 10.25 OK CD-109 88.03 3.70* 6.859E+00 1.859E+OO 2.983E+OO 67.66 OK SN-126 64.28 9.60 4. 772E+OO 6.364E-01 6.364E-01 120.63 OK 86.94 8.90 6.859E+OO 7.727E-01 7. 727E-01 67. 66 OK 87.57 37.00* 6.859E+OO

1. 859E-01 l.859E-01 67. 66 OK BA-137M 661. 66 89.90* 2.464E+OO 6.788E-02 6.924E-02 63.43 OK CS-137 661. 66 85.10* 2.464E+OO 7.170E-02 7.314E-02 63.43 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.720E+OO 4.419E-01 4.419E-01 19.14 OK 860.56 12.50 2. OllE+OO 7.206E-01 7.206E-01 74.72 OK PB-212 74.82 10.28 6.006E+OO 1. 071E+OO 1. 071E+OO 52.68 OK 77 .11 17.10 6.195E+OO 1.641E+OO 1. 641E+OO 20. 71 OK 238.63 43.60* 5.554E+OO 1.253E+OO 1.253E+OO. 10.39 OK 300.09 3.30 4.645E+00 l.532E+OO 1.532E+OO 82.97 OK BI-214 609.32 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 OK 1120.29 14.92 1.635E+OO 8.518E-01 8. 521E-01 75.87 OK 1764.49 15.30 1.106E+OO l.404E+OO 1.405E+OO 44.86 OK PB-214 74.82 5.80 5.996E+00 Line Not Found <<INT Reject 77 .11 9.70' 6.195E+OO 2.893E+OO 2.894E+OO 20.71 . OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.495E+OO Line Not Found <<INT Reject 295.22 18.42 4.708E+OO 1.144E+OO 1.144E+OO 22.73 OK 351. 93 35.60* 4.083E+OO 9. 572E-01 9.576E-01 17.36 OK RN-222 609.32 45.49* 2.628E+OO 7.998E-01 8.00lE-01 24.10 OK .1120. 29 14.92 1.635E+OO 8.518E-01 8.521E-01 75.87 OK 1764.49 15.30 1.106E+Ob 1.404E+OO l.405E+00 44.86 OK RA-224 240.99 4.10* 5. 498E+oo* 1.568E+00 1.568E+OO 87.46 OK RA-226 609.32 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 OK 1120.29 14.92 1.635E+OO 8.518E-01 8. 521E-01 75.87 OK 1764.49 15.30 1.106E+OO l.404E+OO 1.405E+OO 44.86 OK AC-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11.27 4.217E+OO 8.632E-01 8.632E-01 49.76 OK 794.95 4.25 2 .138E+OO Line Not Found Absent 835. 71 1. 61 2.057E+OO Line Not Found Absent 911. 20 25.80* 1.924E+OO 9.747E-01 9.747E_:_Ol 29.48 OK 968. 97 15.80 1.834E+OO 1. llOE+OO l. llOE+OO 42.70 OK RA-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 OK 794.95 4.25 2.138E+OO Line Not Found Absent 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25. 80* ' 1.924E+OO. 9.747E-01 9.747E-01 29.48 OK 968. 97 15. 80 l.834E+00 1. llOE+OO 1. llOE+OO 42.70 OK TH-228 74.82 10.28 6.006E+OO 1. 071E+OO 1. 071E+OO 52.68 OK 77 .11 17.10 6.195E+OO 1. 641E+OO 1.641E+OO 20.71 OK 238.63 43.60* 5.554E+OO l.253E+00 l.253E+OO 10.39 OK 300.09 3.30 4.645E+OO 1.532E+OO 1.532E+OO 82.97 OK TH-230 609.32 45.49* 2.628E+OO 7.998E-01 7.998E-01 24.10 OK 1120.29 14.92 1. 635E+OO 8.518E-01 8.518E-01 75.87 OK 1764.49 15.30 1.106E+OO l.404E+OO 1.404E+OO 44.86 OK Page 3580 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.645E+OO 9.449E-01 9.449E-01 82.97 OK TH-232 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.217E+OO 8.632E-01 8.632E-01 49. 76 OK 835. 71 1. 61 2.057E+OO Line Not Found Absent 911. 20 25.80* 1.924E+OO 9.747E-01 9.747E-01 29.48 OK 968. 97 15.80 l.834E+OO 1.llOE+OO 1. llOE+OO 42.70 OK TH-234 63. 29 3.70* 4.772E+OO *1. 651E+OO 1. 651E+OO 120.63 OK 92.59 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 OK U-234 609.32 45.49* 2.628E+OO 7.998E-01 7.998E-01 24.10 OK 1120.29 14.92 1. 635E+OO 8.518E-01 8.518E-01 75.87 OK 1764.49 15.30 1.106E+OO 1.404E+OO 1. 404E+OO 44.86 . OK U-235 89. 96 3.47 6.984E+00 1.434E+OO 1.434E+OO 77.01 OK 93.35 5.60 7.103E+OO 2 .136E+OO 2.136E+OO 42.14 OK 143.76 10. 96* 7.370E+00 Line Not Found Absent 163.33 5.08 7.024E+OO Line Not Found Absent 185. 72 57.20 6.563E+OO 2.227E-01 2.227E-01 41. 06 OK 205.31 5.01 6.171E+OO Line Not Found Absent U-238 . 63.29 3.70* 4. 772E+OO 1. 651E+OO . 1. 651E+OO 120.63 OK 92.59 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 OK AM-243 43.53 5.90 1. 315*E+OO Line.Not Found Absent 74.66 67.20* 6.006E+OO 1.639E-01 1.639E-01 52.68 OK ANH-511 511. 00 100.00* 3.019E+OO 7.810E-02 7.810E-02 94.68 OK Flag: "*" = Keyline Page 3581of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:11:12.14 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l *
Acquisition date 3-0CT-2016 09:09:22 Sensitivity : 3.000 *
Detector ID GAM20 Energy 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: .0 01:00:15.23 Half life ratio : ***** * *.Sample date 23-NOV-2015 14:44:00 Analyst initials: MXRl *
Sample ID G405235030 Sample Quantity 1.3112E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. "File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.507E+Ol l.514E+OO CD-109 2.983E+OO l.978E+OO SN-126 l.859E-01 1.233E-01 BA-137M 6.924E-02 4.304E-02 CS-137 7.314E-02 4.546E-02 TL-208 4.419E-01 8.288E-02 PB-212 1.253E+OO l.276E-01 BI-214 8.00lE-01 1.889E-01 PB-214 9.576E-01 l.629E-01 RN-222 8.00lE-01 1.889E-01 RA-224 l.568E+OO 1.344E+OO RA-226 8. OOlE-01 1. 889E-01 AC-228 9.747E-01 2.816E-01 RA-228 9.747E-01 2.816E-01 TH-228 l.253E+OO 1.276E-01 TH-230 7.998E-01 1.889E-01 PA-231 9.449E-01 7.683E-01 TH-232 9.747E-01 2.816E-01 TH-234 1. 651E+OO 1.952E+OO U-234 7.998E-01 l.889E-01 U-235 -2.216E-02 l.820E-01 U-238 1. 651E+OO l.952E+OO AM-243 .1. 639E-01 8. 461E-02 ANH-511 7.810E-02 7.247E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3582 of 5809 Key-Line Activity (pCi/GRAM -5.191E+OO -2.891E-02 O.OOOE+OO 3.919E-03 5.750E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) l.334E+Ol 4.082E-02 1. 960E+41 1. 766E-02 3.774E-01 2.440E+04 MDA (pCi/GRAM 3. 7 83E-01. 1. 876E+OO 1.173E-01 5.190E-02 5.483E-02 4.272E-02 8. 8 96E-02 1.294E-01 l.188E-01 l.294E-01 9.536E-01 1.294E-01 2.158"E-01 2.158E-01 8. 896E-02 1.294E-01 7.239E-01 2.158E-01 1. 661E+OO 1. 2 94E-01 3.210E-01. 1.661E+OO 7.554E-02 MDA (pCi/GRAM 2.434E+Ol 7 .116E-02 O.OOOE+OO 4.726E-02 7.455E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 5.321E+02 O.OOOE+OO SHORT HLIF MN-54 3.804E-02 5.866E-02 1.238E-Ol NOT IDENT. C0-56 2.432E-02 4.637E-01 8.989E-Ol FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -5.382E-02 5.013E-02 8.085E-02 NOT IDENT. C0-58 -2.598E-01 6.789E-01 1.196E+OO NOT IDENT. FE-59 2. 421E-01. 8.558E+OO 1. 708E+Ol NOT IDENT. C0-60 2.369E-02 3. 601E-02 8.216E-02 NOT IDENT. ZN-65 6.554E-02 l.670E-01 3.266E-01 NOT IDENT. GE-68 -5.813E-01 2.548E+OO 4.883E+OO NOT IDENT. AS-73 2.459E+OO 6.369E+OO l.214E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.068E+04 O.OOOE+OO SHORT HLIF SE-75 -5.855E-02 2.090E-01 . 3. 937E-01 NOT IDENT. BR-77 O.OOOE+OO 1.790E+39 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO l.060E+03 O.OOOE+OO SHORT HLIF RB-83 -2.797E-01 7.158E-01 l.294E+OO NOT IDENT. KR-85 2.480E+OO 7.227E+OO 1.297E+Ol NOT IDENT. SR-85 3.059E-01 8.933E-01 1.603E+OO NOT IDENT. RB-86 O.OOOE+OO 5.102E+04 O.OOOE+OO SHORT HLIF Y-88 -6. 971E-02 2.168E-01 4.233E-01 NOT IDENT. Y-91 -l.463E+02 5.109E+02 9.832E+02 NOT IDENT. NB-94 -6. 041E-03 3.051E-02 5.576E-02 NOT IDENT. NB-95 -3.666E-01 1.205E+OO 2.121E+OO NOT IDENT. NB-95M 2.424E+OO 2.635E+00 5. 031E+OO NOT IDENT. ZR-95 -8.124E-01 1.394E+OO 2.384E+OO NOT IDENT. NB-97 O.OOOE+OO 8.517E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 6.'694E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 8.237E-03 3.475E-02 5.858E-02 NOT IDENT. RH-102 -4.122E-03 6.028E-02 1.129E-01 NOT IDENT. RU-103 -1.577E+OO 6. 996E+OO l.300E+Ol FAIL ABUN RH-106 -l.630E-01 5.076E-01 9.176E-01 NOT IDENT. RU-106 -1.630E-01 5.076E-01 9.176E-01 NOT IDENT. AG-108M 1.808E-02 2.465E-02 5.173E-02 NOT IDENT. AG-llOM 2.838E-02 8.461E-02 1. 756E-01 FAIL ABUN SN-113 5.595E-02 2.420E-01 4.747E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 2.242E+05 0.000E+OO SHORT HLIF TE-123M 5.483E-02 l.550E-01 2.624E-01 NOT IDENT. SB-124 9.869E-02 1.958E+OO 4.383E+OO NOT IDENT. 2.725E-02 9.345E-02 1.864E-01 FAIL ABUN TE-125M :....1. 420E+02 3.103E+02 5. 351E+02. NOT IDENT. I-126 O.OOOE+OO l.881E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.675E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.891E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.492E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.342E+27 O.OOOE+OO SHORT HLIF BA-133 3.287E-02 6.517E-02 7.453E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.534E-02 5.875E-02 1. 214E-01 NOT IDENT. CS-135 8. 038E.-02 1. 421E-01 2.623E-01 NOT IDENT .. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 5.874E+05 0.000E+OO SHORT HLIF CE-139 -4.901E-02 1.llBE-01 1. 890E-01 NOT IDENT. BA-140 O.OOOE+OO 2.717E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 8.756E+05 O.OOOE+OO SHORT HLIF CE-141 -4 .. 732E+Ol 3. 413E+Ol 5.290E+Ol NOT IDENT. CE-143 O.OOOE+OO l.204E+41 O.OOOE+OO SHORT HLIF CE-144 -1. 7 32E-01 4.037E-01 6.288E-01 NOT IDENT. PM-144 4.007E-02 5. 701E-02 l.174E-01 NOT IDENT. PR-144 3.477E+OO 4.986E+00 1.026E+Ol NOT IDENT. PM-146 -1.605E-02 3.918E-02 7.140E-02 NOT IDENT. ND-147 O.OOOE+OO 7 .119E+07 O.OOOE+OO SHORT HLIF PM-147 3.755E+02 7.836E+02 1. 464E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF EU-150 -8.685E-03 2. 611E-02 4.296E-02 FAIL ABUN EU-152 5.652E-02 8.423E-02 1.733E-01 NOT IDENT. GD-153 -1.544E-02 l.937E-01 3.200E-01 NOT IDENT. EU-154 -5.707E-02 9.728E-02 1. 749E-01 NOT IDENT. EU-155 l.721E-02 l.027E-01 1.873E-01 FAIL ABUN TB-160 1. 611E+OO 2.126E+OO 4.514E+OO FAIL ABUN H0-166M 4.534E-02 6.894E-02 9.764E-02 FAIL ABUN TM-171 9.197E-01 l.300E+Ol 2.426E+01 NOT IDENT. HF-172 -7.889E-02 2.624E-01 4.157E-01 FAIL ABUN LU-172 -1.581E-03 8.202E-02 1.616E-01 FAIL ABUN LU-176 -9.895E-03 2.278E-02 4.200E-02 FAIL ABUN Page 3583 of 5809 HF-181 -5.063E-01 4. 960E+OO 9.421E+OO NOT IDENT. TA-182 3. 2.45E-01 1.046E+OO 2.133E+OO FAIL ABUN RE-183 2.875E-01 2.455E+OO 4.555E+OO FAIL ABUN RE-184 3.007E+Ol 4. 311E+Ol 8.915E+Ol NOT IDENT. W-188 -4.717E+Ol 1. 309E+02 2.163E+02 FAIL ABUN IR-192 -3.451E-02 4.503E-01 8.673E-01 FAIL ABUN HG-203 -1.845E+OO 2.597E+OO 4.678E+00 NOT IDENT. BI-207 -4.604E-02 4 .113E-02 6.609E-02 FAIL ABUN PB-210 1.033E+OO 1.856E+OO 3.617E+00 NOT IDENT. BI-211 O.OOOE+OO 4.488E-01 8.123E-01 *FAIL ABUN PB-211 -4.082E-01 6.342E-01 1.123E+OO NOT IDENT. BI-212 1.398E+OO 1.024E+OO l.446E+OO FAIL ABUN RN-219 l.717E-01 3.548E-01 7.156E-01 FAIL ABUN RA-223 -2.322E-01 5. 966E-01 9.761E-01 FAIL ABUN AC-227 1.576E-01 2. lOlE-01 4.310E-01 FAIL ABUN TH-227 l.576E-01 2.lOlE-01 4.310E-01 FAIL ABUN TH-229 -3.144E-01 4.163E-01 7.625E-01 FAIL ABUN TH-231 -2.322E-01 5. 966E-01 9. 761E-01 FAIL ABUN PA-233 5.683E-03 5.437E-02 l.059E-01 FAIL ABUN PA-234 4.956E-02 2.242E-01 4.775E-01 FAIL ABUN PA-234M 3.779E+OO 3.610E+OO 8.733E+00 FAIL ABUN NP-237 5.683E-03 5.437E-02 1.059E-01 FAIL ABUN .NP-238 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF NP-239 8.044E-02 2.107E-01 3.936E-01 NOT IDENT. PU-239 5.533E+02 5.183E+02 6.391E+02 FAIL ABUN AM-241 1.108E-01 1.030E-01 1. 921E-01 NOT IDENT. CM-243 5.665E-03 8.751E-02 1.591E-01 NOT IDENT. BK-247 -7.044E-03 6.501E-02 1. 24 6E-01 NOT IDENT. CM-247 2. 966E-02 3.276E-02 6.874E-02 NOT IDENT. CF-249 -4. 716E-03 3.330E-02 6.312E-02 NOT IDENT. CF-251 8. 311E-02 l.055E-01 2.163E-01 NOT.IDENT. Page 3584 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:09.92 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn. %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 368 10.66* 1. 312E+OO 1. 507E+Ol
1.507E+Ol 10.25 CD-109 88.03 129 3.70* 6.859E+OO 2.913E+OO 4:675E+OO 42.38 SN-126 64.28 51 9.60 4. 772E+OO 6.364E-01 6.364E-01 120. 63 86.94 129 8.90 6.859E+OO 1.211E+OO 1.211E+OO 42.38 87.57 129 37.00* 6.859E+OO 2.913E-01 2.913E-Ol 42.38 BA-137M 661. 66 26 89.90* 2.464E+OO 6.788E-02 6.924E-02 63.43 CS-137 661. 66 26 85.10* 2.464E+OO 7.170E-02 7.314E-02 63.43 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 178 85.00* 2.720E+OO 4.419E-01 4.419E-01 19.14 860.56 32 12.50 2. OllE+OO 7.206E-01 7.206E-01 74.72 BI-211 72. 87 ------1. 23 5.823E+OO ------Line Not Found ------351.06 243 12.92* 4.083E+OO 2.638E+OO 2.638E+00 17.36 PB-212 74.82 185 10.28 6.006E+OO 1.717E+OO 1.717E+OO 31.74 77 .11 304 17.10 6.195E+OO 1.641E+OO 1. 641E+OO 20.71 238.63 530 43.60* 5.554E+OO l.253E+00 1.253E+OO 10.39 300.09 41 3.30 4.645E+OO l.532E+OO . 1. 532E+OO 82.97 BI-214 609.32 167 45.49* 2.628E+OO 7.998E-01 8.00lE-01 24.10 1120.29 36 14.92 1.635E+OO 8.518E-01 8.521E-01 75.87 1764.49 4'2 15.30 1.106E+OO l.404E+OO 1.405E+OO 44.86 PB-214 74.82 185 5.80 6.006E+OO 3.043E+OO 3.044E+00 31.74 77 .11 304 9.70 6.195E+OO 2.893E+OO 2.894E+OO 20.71 87.09 129 3.41 6.859E+OO 3.161E+OO 3.162E+00 42.38 242.00 141 7.25 5.498E+OO 2. 031E+OO 2.032E+OO 35.98 295.22 173 18.42 4.708E+OO 1.144E+OO 1.144E+OO 22.73 351. 93 243 35.60* 4.083E+OO 9. 572E-01 9.576E-01 17.36 RN-222 609.32 167 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 1120.29 36 14.92 l.635E+OO 8.518E-01 8.521E-01 75.87 1764.49 42 15.30 1.106E+OO 1.404E+00 1.405E+OO 44.86 RA-224 240.99 141 4.10* 5.498E+OO 3.591E+00 3. 591E+OO 35.98 RA-226 609.32 167 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 1120.29 36 14.92 1.635E+OO 8.518E-01 8.521E-01 75.87 1764.49 42 15.30 1.106E+OO l.404E+OO 1.405E+OO 44.86 AC-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 72 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 794.95 ------4.25 2.138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------911.20 84 25.80* 1.924E+OO 9.747E-01 9.747E.,-01 29.48 968. 97 56 15.80 1.834E+OO 1. llOE+OO 1. llOE+OO 42.70 RA-228 105.21 ------1.10 7.453E+00 ------. Line Not Found ------338.32 72 11.27 4 .. 217E+OO 8.632E-01 8.632E-01 49.76 794.95 ------4.25 2.138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------911. 20 84 25.80* 1.924E+OO 9.747E-01 .9. 7 4 7E-01 29.48 968. 97 56 15.80 1.834E+OO 1. llOE+OO 1. llOE+OO 42.70 TH-228 74.82 185 10.28 6.006E+OO 1.717E+OO 1. 717E+OO 31.74 77 .11 304 17.10 6 .19'5E+OO 1. 641E+OO 1. 641E+OO 20.71 238.63 530 43.60* 5.554E+OO 1.253E+OO 1.253E+OO 10.39 Page 3585 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 41 3.30 4.645E+OO 1.532E+OO l.532E+OO 82.97 TH-230 609.32 167 45.49* 2.628E+OO 7.998E-01 7.998E-01 24.10 1120.29 36 14.92 1.635E+OO 8.518E-01 8.518E-01 75.87 1764.49 42 15.30 l.106E+OO 1.404E+OO 1. 404E+OO 44. 86 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 41 5.35* 4.645E+OO 9.449E-01 9.449E-01 82.97 TH-232 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 72 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 835.71 ------1. 61 2.057E+00 ------Line Not Found ------911. 20 84 25.80* 1.924E+00 9.747E-01 9.747E-01 29.48 968. 97 56 15.80 l.834E+OO 1. llOE+OO 1. llOE+OO 42.70 TH-234 63.29 51 3.70* 4.772E+OO l.651E+OO 1. 651E+OO 120.63 92.59 148 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 U-234 609.32 167 45.49* 2.628E+00 7.998E-01 7.998E-01 24.10 1120.29 36 14.92 1.635E+OO 8.518E-01 8.518E-01 75.87 1764.49 42 15.30 1.106E+OO 1.404E+OO 1. 404E+OO 44.86 U-235 89. 96 61 3.47 6.984E+OO 1.434E+OO 1.434E+OO 77.01 93.35 148 5.60 7.103E+OO 2.136E+OO 2.136E+OO 42.14 143.76' ------10. 96* 7 .. 370E+OO ------Line Not Found ------163.33 ------5.08 7.024E+OO ------Line Not Found ------185.72 146 57.20 6.563E+00 2.227E-01 2.227E-01 41. 06 205.31 ------5.01 6.171E+OO ------Line Not Found ------U-238 63.29 51 3.70* 4.772E+OO 1. 651E+OO 1.651E+OO 120.63 92.59 148 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 185 67.20* 6.006E+OO 2.626E-01 2.626E-01 31.74 ANH-511* 511. 00 41 *100. 00* 3.019E+OO 7.810E-02 7.810E-02 94.68 Flag: "*" Key line Page 3586 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Total number of lines in spectrum 42 Number of unidentified lines 5 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226
AC-228 RA-228 'TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y 1600. DOY 1600.00Y 1600. DOY 1. 41E+l0Y 1600. DOY l.41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 60 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.507E+Ol 2.913E+OO 2.913E-01 6.788E-02 7.170E-02 4.419E-01 2.638E+OO 1.253E+OO 7.998E-01 9.572E-01 7.998E-01 3.591E+OO 7.998E-01 9.747E-01 9.747E-01 1.253E+OO 7.998E-01 9.449E-01 9.747E-01 l.651E+00 7.998E-01 2.227E-01 1.651E+OO 2.626E-01 7.810E-02 4.029E+Ol 4.029E+Ol Decay Corr pCi/GRAM 1.507E+Ol 4.675E+OO 2.913E-01 6.924E-02 7.314E-02 4.419E-01 2.638E+OO 1.253E+OO 8. OOlE-01 9.576E-01 8.00lE-01 3.591E+OO 8. OOlE-01 9.747E-01 9.747E-01 l.253E+OO 7.998E-01 9.449E-01 9.747E-01 l.651E+OO 7.998E-01 2.227E-01 1.651E+OO 2.626E-01 7.810E-02 4.205E+Ol 4.205E+Ol 88.10% Decay Corr 2-Sigma Error 0.155E+Ol l.981E+00 l.235E-01 4.392E-02 4.639E-02 0.846E-01 0.458E+OO 0.130E+OO l.928E-01 1.663E-01 1.928E-01 l.292E+00 1.928E-01 2.873E-01 2.873E-01 0.130E+00 1.927E-01 7.840E-01 2 .. 873E-01 1.992E+OO l.927E-01 0.914E-01 l.992E+OO 0.834E-01 7.395E-02 "M" Manually accepted 2-Sigma %Error 10.25 42.38 42.38 63.43 63.43 19.14 17.36 10.39 24.10 17.36 24.10 35.98 24.10 29.48 29.48 10.39 24.10 82.97 29.48 120.63 24.10 41. 06 120.63 31. 74 94.68 Flags: "K" Keyline nbt found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3587 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235030 Acquisition date : 3-0CT-2016 09:09:22 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 129.39 46 125 1. 36 258.84 254 12 1.13E-02 95.6 7.54E+OO T 3 131. 32 28 105 1.14 262. 70 254 12 6.80E-03 **** 7.52E+OO T 0 161. 55 30 70 1. 56 323 .13 321 6 7.50E-03 **** 7.06E+OO T 0 208.97 64 94 1. 23 417.91 415 9 1.64E-02 61. 7 6.lOE+OO 0 270.50 22 81 2.05 540.93 539 8 5.75E-03 **** 5.05E+OO T 0 327.64 38 54 1. 31 655.16 650 9 9.89E-03 76.1 4.33E+OO T 1 355.92 14 35 1. 56 711. 72 699 17 3.59E-03 **** 4.05E+OO T 0 416.83 12 17 1. 33 833.50 830 6 3.14E-03 **** 3.56E+OO 0 463.17 36 28 1. 62 926.18 922 11 9.55E-03 66.1 3.27E+OO T 0 657.26 19 10 1. 53 1314.39 1306 14 5.14E-03 86.9 2.48E+OO T 0 710.81 10 14 1. 33 1421. 52 1417 9 2.76E-03 **** 2.33E+OO T 0 727.71 37 39 1. 38 1455.33 1449 12 1.03E-02 74.7 2.29E+OO T 0 922.69 17 10 4.74 1845.49 1837 12 4.81E-03 84.8 1. 91E+OO T 0 1001.87 10 3 1. 31 2003.97 2000 7 2.81E-03 97.5 1.79E+OO T 0 1238.15 20 11 2.37 2477.01 2472 9 5.79E-03 72. 6 1.51E+OO T 0 1432.30 6 4 1. 39 2865.83 2861 8 1.67E-03 **** 1. 33E+OO 0 1504.53 8 3 0.56 3010.52 3004 10 2. 31E-03 99.9 1.28E+OO T 0 1729.83 17 2 1. 32 3461.94 3457 10 4.92E-03 57.9 1.13E+OO 0 1846.37 15. 0 1. 04 3695.50 3690 11 4.44E-03 50.0 1. 06E+OO Flags: "T" = Tentatively associated Page 3588 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:11:23.75 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l *
Acquisition date 3-0CT-2016 09:09:22 Sensitivity 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:15.23 Half life ratio : ***** *
Sample date 23-NOV-2015 14:44:00 Nuclide Library : SOLID *
Sample ID G405235030 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : l.3112E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-22 6 AC-228 RA-228 TH-228 TH-230 PA-23i TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM l.337E-01 8.871E-01 5.546E-02 2.234E-02 2.360E-02 l.796E-02 4.120E-02 5.814E-02 5.393E-02 5.814E-02
4.416E-01 5.814E-02 9.220E-02 9.220E-02 4.120E-02 5.812E-02 3.300E-01 9.220E-02 7.849E-01 5.812E-02 l.506E-01 7.849E-01 3.576E-02 2. 521E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3589 of 5809 Le (pCi/GRAM 1.074E+Ol 2.894E-02 O.OOOE+OO l.646E-02 3.189E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0--:56 MN-56 C0-57 ' C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB"-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 .TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-.172 LU-172 LU-176 HF-181 Page 3590 of 5809 5.427E-02 3.847E-01 O.OOOE+OO 3.766E-02 5.167E-01 7.425E+OO 3. 496E-02 l.404E-01 2.121E+OO 5.709E+OO 0.000E+OO l.806E-01 O.OOOE+OO O.OOOE+OO 5.732E-01 5.846E+OO 7.226E-01 0.000E+OO l.551E-01 4.109E+02 2.454E-02 9.533E-01 2.343E+OO 9. 960E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.742E-02 5.004E-02 5.773E+OO 4.039E-01 4.039E-01 2.333E-02 7.472E-02 2.157E-01 O.OOOE+OO O.OOOE+OO 1.229E-01 1.662E+OO 8.378E-02 2.498E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.393E-02 O.OOOE+OO 5.498E-02 1.214E-01 O.OOOE+OO O.OOOE+OO 8.751E-02 O.OOOE+OO O.OOOE+OO 2.459E+Ol O.OOOE+OO 2.937E-01 5.263E-02 4.600E+OO 3.163E-02 O.OOOE+OO 6.855E+02 0. OOOE+oo* 1. 951E-02 7.919E-02 1.506E-01 7.132E-02 8.785E-02 1.989E+OO 4.260E-02 1.137E+Ol l.949E-01 7.063E-02 1. 915E-02 4.179E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF .NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT I DENT.* NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192* HG-203 BI-207 PB-210 BI-21l PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3591of5809 9.395E-01 2.146E+OO 3.956E+Ol 9.873E+Ol 3.923E-01 2.125E+OO 2.681E-02 1. 708E+OO 3.913E-Ol 5.042E-01 6.719E-01 3.252E-01 4.426E-01 1. 996E-01 1.996E-01 3.530E-01 4.426E-01 4.838E-02 2.040E-01 3.848E+OO 4.838E-02 O.OOOE+OO 1.834E-01 3.027E+02 9.077E-02 7.428E-02 5.714E-02 3.138E-02 2.838E-02 1.013E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN' NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-,0CT-2016 10:11:28.93 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030 .. CNF;l *
Acquisition date 3-0CT-2016 09:09:22 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:15.23 Half life ratio : ***** *
Sample date 23-NOV-2015 14:44:00 Nuclide Library : SOLID *
Sample ID G405235030 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity 1.3112E+02 GRAM *
Quantity Err ( % ) 1. 5253E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal.' date 30-JUN-2016 06:52:39 Eff. Geometr'y : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
Combined Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma ) ( 1. 96-sigma) K-40 1.507E+Ol 1. 706E+OO 1. 706E+OO CD-109 2.983E+OO 2.004E+OO 2.004E+OO SN-126 l.859E-01 1.245E-01 1.245E-01 BA-137M 6.924E-02 4.314E-02 4.314E-02 CS-137 7.314E-02 4.557E-02 4.557E-02 TL-208 4. 419E.-01 8.498E-02 8.498E-02 PB-212 1.253E+OO l.437E-01 l.437E-01 BI-214 8.00lE-01 l.920E-01 l.920E-01 PB-214 9.576E-01 1.677E-01 l.677E-01 RN-222 8.00lE-01 1.920E-01 l.920E-01 RA-224 1.568E+OO 1.353E+OO 1.353E+OO RA-226 8.00lE-01 l.920E-01 l.920E-01 AC-228 9.747E-01 2.860E-01 2.860E-01 RA-228 9.747E-01 2.860E-01 2.860E-01 TH-228 1.253E+OO l.437E-01 l.437E-01 TH-230 7.998E-01 l.920E-01 l.920E-01 PA-231 9.449E-01 7.944E-01 7.944E-01 TH-232 9.747E-01 2.860E-01 2.860E-01 TH-234 1. 651E+OO 1. 986E+OO 1.986E+OO U-234 7.998E-01 1.920E-01 1.920E-01 U-235 -2.216E-02 l.820E-01 l.820E-01 U-238 1. 651E+OO 1. 986E+OO 1. 98 6E+OO AM-243 1.639E-01 8.612E-02 8.612E-02 ANH-511 7.810E-02 7.254E-02 7.254E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -5 .191E+OO 1.335E+Ol l.355E+Ol NOT IDENT. NA-22 -2.891E-02 4.083E-02 4.286E-02 NOT IDENT. NA-24 l.OOOE+41 6.080E+41 O.OOOE+OO SHORT HLIF AL-26 3.919E-03 1. 766E-02 l.775E-02 NOT IDENT. SC-46 5.750E-02 3.774E-01 3.782E-01 FAIL ABUN V-48 -6.282E+03 2.441E+04 2.457E+04 SHORT HLIF Page 3592 of 5809 CR-51 4.764E+02 5.325E+02 5.742E+02 SHORT HLIF MN-54 3.804E-02 5.868E-02 6 .114E-02 NOT IDENT. C0-56 2.432E-02 4.637E-01 4.638E-01 FAIL ABUN MN-56 l.OOOE+41 .1. 548E+42 0.000E+OO SHORT HLIF C0-57 -5.382E-02 5.019E-02 5.574E-02 NOT IDENT. C0-58 -2.598E-01 6.790E-01 6.890E-01 NOT IDENT.
FE-59 2.421E-01 8.558E+OO 8.558E+OO NOT IDENT. C0-60 2.369E-02 3.602E-02 3.757E-02 NOT IDENT. ZN-65 6.554E-02 l.670E-01 l.696E-01 NOT IDENT. GE-68 -5.813E-01 2.548E+OO 2.562E+OO NOT IDENT. AS-73 2.459E+OO 6.389E+OO 6.485E+OO NOT IDENT. AS-74 -2.231E+03 l.068E+04 l.073E+04 SHORT HLIF SE-75 -5.855E-02 2.090E-01 2.107E-Ol NOT IDENT. BR-77 1. 758E+40 l.597E+41 O.OOOE+OO SHORT HLIF SR-82 -5.368E+02 l.060E+03 l.087E+03 SHORT HLIF RB-83 -2.797E-01 7.168E-01 7.278E-01 NOT IDENT. KR-85 2.480E+OO 7.228E+OO 7.313E+OO NOT IDENT. SR-85 3.059E-01 8.934E-01 9.040E-01 NOT IDENT. RB-86 -1. 417E+04 5.102E+04 5.142E+04 SHORT HLIF Y-88 -6. 971E-02 2.169E-01 2.191E-01 NOT IDENT. Y-91 -1. 463E+02 5.109E+02 5.152E+02 NOT IDENT. NB-94 -6. 041E-03 3. 051E-02 3.064E-02 NOT IDENT. NB-95 -3.666E-01 1. 2 05E+OO l.217E+OO NOT IDENT. NB-95M 2.424E+OO 2.642E+OO 2.859E+OO NOT IDENT. ZR-95 -8.124E-01 l.395E+OO l.442E+OO NOT IDENT. NB-97 l.OOOE+41 8.528E+40 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 2. 811E+41 O.OOOE+OO SHORT HLIF M0-99 -5.817E+33 6.707E+33 O.OOOE+OO SHORT HLIF TC-99M -1. 000E+41 2.102E+41 0.000E+OO SHORT HLIF RH-101 8.237E-03 3.478E-02 3.498E-02. NOT IDENT. RH-102 -4.122E-03 6.028E-02 6. 031E-02 NOT IDENT. RU-103 -l.577E+OO 6. 996E+OO 7.032E+OO FAIL ABUN RH-106 -l.630E-01 5.077E-01 5.130E-01 NOT IDENT. RU-106 -l.630E-01 5.077E-01 5.130E-01 NOT IDENT. AG-108M l.808E-02 2.466E-02 2.597E-02 NOT IDENT. AG-llOM 2.838E-02 8.462E-02 8.558E-02 FAIL ABUN SN-113 5.595E-02 2.420E-01 2.433E-01 NOT IDENT. CD-115 l.000E+41 2.668E+41 O.OOOE+OO SHORT HLIF SN-ll 7M l.581E+05 2.251E+05 2.361E+05 SHORT HLIF TE-123M 5.483E-02 l.550E-01 l.570E-01 NOT IDENT. SB-124 9.869E-02 l.958E+OO l.958E+OO NOT IDENT. SB-125 2. 725E-02 9.346E-02 9.426E-02 FAIL ABUN TE-125M -l.420E+02 3.104E+02 3.170E+02 NOT IDENT. I-126 3.392E+05 l.ff82E+06 l.888E+06 SHORT HLIF SB-126 5.891E+05 2.677E+06 2.690E+06 SHORT HLIF SB-127 -2.647E+23 4.791E+23 O.OOOE+OO SHORT HLIF I-131 l.256E+l0 l.493E+l0 l.597E+l0 SHORT HLIF I-132 l.OOOE+41 2.546E+42 O.OOOE+OO SHORT HLIF TE-132 2.590E+27 8.415E+27 O.OOOE+OO SHORT HLIF BA-133 3.287E-02 6.519E-02 6.685E-02 FAIL ABUN I-133 -l.OOOE+41 3.947E+41 O.OOOE+OO SHORT HLIF CS-134 5.534E-02 5.880E-02 6.387E-02 NOT IDENT. CS-135 8.038E-02 l.422E-01 l.467E-01 NOT IDENT. I-135 -l.OOOE+41 l.129E+42 O.OOOE+OO SHORT HLIF CS-136 l.009E+04 5.874E+05 5.874E+05 SHORT HLIF CE-139 -4.901E-02 l.122E-01 l.143E-01 NOT IDENT. BA-140 -3.097E+05 2.717E+06 2.721E+06 SHORT HLIF LA-1.40 -6.788E+05 8.762E+05 9.281E+05 SHORT HLIF CE-141 -4.732E+Ol 3.419E+Ol 4.030E+Ol NOT IDENT. CE-143 l.OOOE+41 l.209E+41 O.OOOE+OO SHORT HLIF CE-144 -1. 732E-01 4.038E-01 4 .113E-01 NOT IDENT .. PM-144 4.007E-02 5.707E-02 5.986E-02 NOT IDENT. PR-144 3.477E+OO 4.989E+OO 5.229E+OO NOT IDENT. PM-146 -l.605E-02 3.920E-02 3.986E-02 NOT IDENT. ND-147 -5. '655E+07 7.126E+07 7.568E+07 SHORT HLIF PM-147 3.755E+02 7'. 838E+02 8.018E+02 NOT. IDENT. PM-149 -l.OOOE+41 2.231E+41 O.OOOE+OO SHORT HLIF EU-150 -8.685E-03 2. 611E-02 2.640E-02 FAIL ABUN EU-152 5.652E-02 8.429E-02 8.806E-02 NOT IDENT. GD-153 -l.544E-02 l.937E-01 l.938E-01 NOT IDENT. EU-154 -5.707E-02 9.730E-02 l.006E_:Ol NOT IDENT. EU-155 l.721E-02 l.027E-01 l.030E-01 FAIL ABUN TB-160 1. 611E+OO 2.128E+OO 2.249E+OO FAIL ABUN H0-166M 4.534E-02 6.898E-02 7.194E-02 FAIL ABUN TM-171 9.197E-01 l.300E+Ol l.301E+Ol NOT IDENT. HF-172 -7.889E-02 2.627E-01 2.651E-01 FAIL ABUN LU-172 -l.581E-03 8.202E-02 8.202E-02 FAIL ABUN LU-176 -9.895E-03 2.279E-02 2.322E-02 FAIL ABUN Page 3593 of 5809 HF-181 -5.063E-01 4. 960E+OO 4. 966E+OO NOT IDENT. TA-182 3.245E-01 1.046E+OO l.056E+OO FAIL ABUN RE-183 2.875E-01 2.456E+OO 2.459E+OO FAIL ABUN RE-184 3.007E+Ol 4.376E+Ol 4.581E+Ol NOT IDENT. W-188 -4.717E+Ol l.310E+02 l.327E+02 FAIL ABUN IR-192 -3. 451E-'-02 4.503E-01 4.505E-01 FAIL ABUN HG-203 -1. 845E+OO 2.598E+OO 2.728E+OO NOT IDENT. BI-207 -4.604E-02 4. ll 7E-02 4. 611E-02 FAIL ABUN PB-210 1.033E+OO 1.858E+OO 1.916E+OO NOT IDENT. BI-211 2.638E+OO 4.639E-01 1.276E+OO FAIL ABUN . PB-211 -4.082E-01 6.345E-01 6.607E-01 NOT IDENT. BI-212 l.398E+OO 1. 02 6E+OO 1.204E+OO FAIL ABUN RN-219 1.717E-01 3.554E-01 3.638E-01 FAIL ABUN RA-223 -2.322E-01 5 .. 968E-01 6.059E-01 FAIL ABUN AC-227 l.576E-01 2. lllE-01 2.228E-01 FAIL ABUN TH-227 l.576E-01 2. lllE-01 2.228E-01 FAIL ABUN TH-229 -3.144E-01 4.166E-01 4.400E-01 FAIL ABUN TH-231 -2.322E-01 5. 968E-01 6.059E-01 FAIL ABUN PA-233 5.683E-03 5.437E-02 5.444E-02 FAIL ABUN PA-234 4.956E-02 2.312E-01 2.323E-01 FAIL ABUN PA-234M 3.779E+OO 3.614E+00 3.995E+OO FAIL ABUN NP-237 5.683E-03 5.437E-02 5.444E-02 FAIL ABUN NP-238 1.000E+41 1.834E+42 O.OOOE+OO SHORT HLIF NP-239 8.044E-02 2.108E-01 2.139E-01 NOT IDENT. PU-239 5.533E+02 5.189E+02 5.757E+02 FAIL ABUN AM-241 l.108E-01 1.033E-01 l.148E-01 NOT IDENT. CM-243 5.665E-03 8. 7 51E-02 8.755E-02 NOT IDENT. BK-247 -7.044E-03 6.502E-02 6.510E-02 NOT IDENT. CM-247 2. 966E-02 3.314E-02 3.574E-02 NOT IDENT. CF-249 -4. 716E-03 3.330E-02 3.337E-02 NOT IDENT. CF-251 8. 311E-02 1.059E-01 l.123E-01 NOT IDENT. Page 3594 of 5809
- - - - * . GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 72.2845 87.09 101. 57 67 136.47 53.1785 45.60 72.5864 87.57 101.6419 140.51 0.0000 46.54 70.5825 88.03 101.7051 143.76 74.2628 49.72 0.0000 88.34 101. 7472 144.24 70.6432 51.35 86.3422 88.47 101.7645 145.44 90.2372 51. 87 79.9433 89. 96 101. 9658 152.43 73.6569 52.39 73.5314 1093.63 102.0568 153.25* 0.0000 52. 97 70.3618 91.11 0.0000 323.87 78.6992 53.44 73.6720 92.59 102.3162 156.02 0.0000 54.07 80.2634 93.35 102.4167 158.56 0.0000 57.36 0.0000 94.56 72.2255 159.00 59.2881 57.53 91.6674 94.65 72.2341 162.33 69.3796 57.98 85.1854 94.67 72.2360 162.66 0.0000 59.27 68.5909 94.87 72. 2542 163.33 57.8691 59.32 68. 5966 97.43 81.7423 165.86 62.1437 59.54 68.6222 98.43 75.2817 176.31 56.8617 60.96 87.8125 98.44 75.2827 176.60 0.0000 61.17 87.8433 99.53 80.0234 177. 52 56.0841 62.93 98.0102 100 .11 77. 7596 181.07 0.0000 63.29 98.0681 102.03 67.4731 181.52 49.1356 63.58 98 .1144 103.18 66.4024 184.41 63.1470 64.28 98.2260 103.37 64.0872 143.76 63.2164 66.73 113.7548 105.21 72*. 4037 193.51 67.8630 67.24 110.8887 105.31 72.4122 197.03 69.7564 125.81 110. 9657 106.12 71. 3131 198.01 59.5944 67.75 110.9779 106.47 72.5125 201.83 63.1910 69.67 134.6849 109.28 77.4462 203.43 51.3000 70.83 112.9942 111. 00 65.8433 205.31 52.6601 72.81 128.2459 111.76 0.0000 210.85 73.5235 72.87 128.2573 114. 06 57.8152 215.65 68.1823 74.66 105.4215 116.30 0.0000 222 .11 56.3698 74.82 105.4466 116.74 54.4400 227.09 47.0017 74.97 105.4696 119.76 78.3720 227.38 47.0116 77 .11 105.8002 121.12 60.6504 228.16 0.0000 78.74 96.2715 121.22 60.6571 228.18 41. 8125 79.69 111.4645 121. 78. 83.3060 116.74 41.8125 80.12 120.5754 122.06 89.2834 235.69 42.0386 80 .19 0.0000 122.92 65.5357 235.96 42.0464 80.57 110.0948 123.07 60.7796 238.63 52.6575 81. 00 101.1073 265.00 69.1675 238.98 0.0000 81. 07 98.0991 125.81 84.4660 240.99 52.7448 81.75 135.9586 127.23 65.4401 242.00 52.7820 83.79 115.1349 127.91 71.8764 244.70 52.8809 84.00 124.2604 129.30 76.7803 252.40 0.0000 85.43 139.6874 131. 20 76.9326 252.80 51. 4025 86.55 101.5027 133.02 73.8665 254.15 0.0000 86.79 101.5353 133.52 78.7248 256.23 39.0854 86.94 101. 5564 136.00 68.8573 260.90 0.0000 Page 3595 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 46.4511 355.39 0.0000 584.27 9.3977 2 64. 8 0 46.4553 356.01 33.0026 595.83 0.0000 265.00 42.8877 364.49 0.0000 427.87 22.0621 268.22 40.2914 366.42 0.0000 602.52 0.0000 269.46 49.7334 372.51 31. 3887 604. 72 15.7825 270.03 44.3730 375.05 25.7157 607.14 30.0134 271.23 36.7817 377.52 39.0998 609.32 26.3489 273.65 0.0000 356.01 27.7456 610.33 26.3590 276.40 37.8044 *388.16 28.7653 614.28 25.3408 277.37 29.7216 388.63 0.0000 618.01 25.3750 277.60 28.8255 391.69 29.7771 620.36 13.7570 278.00 32.4368 264.66 25.0859 621.93 22.2347 279.20. 45.0857 401.81 26.0656 630.19 0.0000 279.54 50.5062 402.40 23.1763 631.29 21.2476 279.70 54 .1199 404.85 35.7730 633.25 14.8835 280.46 49.6334 410.95 39.7588 634.78 0.0000 283.69 40.6915 413.71 13.1089 635.95 25.5391 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 47.9773 423.72 0.0000 645.85 20.2896 285.90 0.0000 427.09 24.4314 657.76 14.4767 287.50 32.6309 427.87 22.4848 657.90 0.0000 290.67 43.5938 433.94 18.6277 661. 66 12.8853 293.27 0.0000 439.40 25.5551 664.57 0.0000 351. 93 36.4290 453.88 25. 7255 666.33 o. oo*oo 295.96 36.4461 463.37 21.8608 666.50 0.0000 879.38 36.5039 468.07 25.3916 667.71 0.0000 299.98 36.5348 473.00 0.0000 677.62 17.2747 300.09 36.5373 475.06 13.9835 685.70 0.0000 300.13 36.5381 476.78 20.9910 695.00 0.0000 301.36 35.6508 477.60 23.9980 696. 49 16.2982 302.85 41.1722 482.18 22.0421 696. 51 16.2982 256.23 50.8298 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.3893 306.78 43.1034 497.08 24.2002 697.49 17.3906 308.46 37.6384 505.52 25.8045 702.65 20.6862 311. 90 35.8754 507.63 0.0000 706.68 22.8944 31°6.51 31. 3604 511. 00 31.4421 711. 68 16.3800 319.41 0.0000 514.00 22.8497 720.70 0.0000 320.08 0.0000 514.00 22.8497 721. 93 0.0000 321. 04 36.0666 ,520. 40 25.4557 722.78 18.0831 323.87 38.9042 520.69 0.0000 722.91 18.0838 325.23 25.0291 522.65 0.0000 723.31 19.7307 328.76 0.0000 527.90 0.0000 724 .19 19.7366 333.37 33.5259 528.26 16.3438 727.33 23.0491 333.97 39.1272 529.59 16.3529 733.00 18.4728 334.37 47.5220 529.87 0.0000 735.93 14.3081 338.28 39.2212 531. 02 0.0000 333.97 9.9104 338.32 39.2220 537.26 0.0000 739.50 0.0000 311. 90 44.8789 546.56 0.0000 747.24 27.6143 340.48 44.8789 552.55 26.8178 748.06 17.6777 340.55 0 .. 0000 563.25 14. 5013 752.31 17.7012 344.28 27.1710 569.33 25.9562 753.82 0.0000 345.93 42.2003 946.00 29.0721 756.73 14.4023 351.06 32.9143 569.70 29.0744 756.80 14.4028 351.93 32.9300 583.19 9.3937 884.68 22.2078 Page 3596 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 31.1081 1274.44 7 .1118 1620.50 5.0671 766.42 24.4474 1001.03 11. 5706 1621. 92 5.0684 766.84 22.2274 1002.74 12.8224 1678.03 0.0000 772.60 0.0000 1004.73 5.7016 1690.97 3.0775 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 6.2307 778.90 10.0397 1028.54 0.0000 1063.66 2.7718 783.70 0.0000 1037.84 12.5764 1771. 35 6.2380 785.37 17.8835 1038.76 0.0000 1791.20 0.0000 792.07 27.9999 631.29 13.5040 1808.65 1.0460 794.95 25.7823 1048.07 0.0000 1810.72 0.0000 795.86 17.9408 1049.04 9. 9083* 1836.06 4.2021 810.06 13.5127 1050.41 10.8127 810.29 14.6398 1063.66 16.2719 344.28 18.0189 1077.00 0.0000 810.76 18.0208 1077.34 17.2327 815.77 0.0000 1085.87 14.5420 1048.07 0.0000 1093.63 16.3894 832.01 17.0007 1099.45 14.5889 834.85 10.2089 1112. 07 10.9739 835.71 12.4806 1112. 84 10.0614 836.80 0.0000 1115. 54 . 8. 78 67 846.75 0.0000 1120. 29 16.4927 846.77 11. 3822 1120.55 16.4938 856.80 0.0000 1221.41 16.4971 860.56 9.1419 1129. 67 13.7741 871.09 19.4847 1131. 51 0.0000 873.19 12.6154.* 1147.95 0.0000 875.33 0.0000 1173.23 11.1299 879.38 10.3396 1177.95 10.2131 880.51 13.7905 1189.05 14.8926 883.24 17.2510 1204.77 11.2083 884.68 8.0539 1221.41 14.9990 889.28 10.3682 1231.02 10.3333 894.76 19.6141 1235.36 0.0000 898.04 13.8579 1238.28 18.0645 900. 72 25.4250 1260.41 0.0000 903.28 12.7214 1271. 87 13.2677 911.20 11. 5898 1274.44 11. 3782 912.08 13. 9111 1274.54 12.3264 923.98 0.0000 1291.59 6.6612 926.50 3.4915 1298.22 0.0000 929 .11 8.1524 1312 .11 0.0000 937.49 19.2594 1332.49 5.7583 944.13 0.0000 '1362.66 0.0000 946.00 9.6515 1365.19 9.6606 949.00 15.8060 1368.63 0.0000 667.71 0.0000 1384. 29 6.7881 962.31 21.1487 1408.01 6.8201 964. 08 18.3371 1457.56 0.0000 966 .17 22. 5813 1460.82 1. 9685 911.20 23.8335 1489.16 4.9478 968. 97 23.8335 1505.03 12.7039 983.53 0.0000 1584.12 8.0552 984.45 0.0000 1596.21 0.0000 Page 3597 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:57.99 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277 Background date : Z-OCT-2016 11:01:57. Sample date 26-NOV-2015 14:25:00 Acquisition date : 3-0CT-2016 Sample ID G405235031 Sample quantity l.39617E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.58 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 **************************t***************************************************** Pk It 1 1 2 1 3 0 4 0 5 0 6 0 7 0 8 2 9 2 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 -o 22 0 23 1 24 1 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 3598 of 5809 Energy 75.28 77.48 87.22 93.20* 144.44 186.03* 208.93 239.03* 242 .11 271.27 295.94* 328.63 338.57 352.65* 367.02 463.71 511.32* 563.44 572 .16 583.88* 609.76* 627.98 662. 26 666.32 670.67 717.06 727.72* 7 68. 71 785.95 799.40 883.49 911.73* 961. 54 965.08* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 98 171 50 62 41 74 45 405 76 33 159 64 78 230 18 15 49 27 19 97 181 16 65 17 9 12 20 33 14 25 9 71 11 14 122 124 186 172 124 173 123 66 93 108 98 57 84 90 36 28 54 12 26 45 40 18 11 9 11 19 11 23 7 50 2 26 5 9 1.19 1. 29 1. 07 1.17 1. 75 1. 48 0.93 1. 28 1. 59 2.19 1. 21 1. 61 1.14 1. 30 2.46 0. 67 1. 45 1. 81 1. 44 1.17 1.13 0.82 1. 79 1. 80 0. 67 4.54 1. 31 6.07 1. 61 4.04 1. 23 1. 24 0.81 0. 96 151: 77 156.18. 175.66 187.61 290.10 373.27 419.07 479.27 485.43 543.76 593 .11 658.48 678.37 706.53 735.27 928.65 1023.88 1128.11 1145.56 1169. 00 1220.77 1257.20 1325*. 76 1333.89 1342. 59 1435.36 1456.69 1538.68 1573.15 1600. 05 1768.23 1824.72 1924.35 1931.43 148 148 171 184 284 367 413 472 472 536 586 652 671 699 730 925 1017 1123 1140 1163 1215 1250 1317 1317 1338 1427 1452 1531 1569 1583 1764 1819 1921 1927 13 2. 71E-02 13 4.74E-02 9 1.40E-02 8 1. 72E-02 10 1.13E-02 14 2.06E-02 12 1.24E-02 19 .l .12E-01 19 2.12E-02 13 9.lOE-03 14 4.42E-02 15 1.77E-02 12 2.18E-02 16 6.39E-02 11 4.95E-03 9 4.17E-03 15. 1.36E-02 12 7.50E-03 14 5.32E-03 13 2 .'71E-02 13 5.02E-02 12 4.50E-03 22 1. 81E-02 22 4.76E-03 7 2.36E-03 13 3.45E-03 9 5.44E-03 15 9.03E-03 9 3.77E-03 29 6.94E-03 8 2.54E-03 13 1.96E-02 7 2.99E-03 9 4. OlE-03 20.7 4.09E+00 14.4 50.9 40.8 54.1 40.1 51. 9 6.1 2.21E+OO 26. 8 68.3 15.5 28.6 26. 0 11. 6 69.2 67.9 40.0 32.1 65.0 17.7 10.5 57.9 16.7 8.0lE-01 40.1 71. 9 78.2 40.2 36.3 44.3 84.3 42.4 19.4 49.4 48.5 Peak Search Report (continued) Page : 2 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969.78 48 15 1. 70 1940.82 1936 . 13 l.32E-02 22.6 36 0 1054.10 7 17 3.99 2109.46 2100 11 l.81E-03127.2 37 0 1115. 94 14 9 1. 62 2233.14 2228 9 3.89E-03 47.0 38 0 1120.87* 42 11 2.43 2243.02 2238 11 l.16E-02 22.l 39 0 1175.28 8 7 1. 28 2351. 84 2345 9 2.22E-03 68.7 40 7 1191. 67 20 11 2.92 2384.61 2381 12 5.64E-03 31.*6 5.19E+00 41 7 1194.36 8 9 1. 83 2390. o*o 2381 12 2.15E-03 58.4 42 0 1302.02 14 3 4.15 2605.31 2598 13 3.85E-03 37.9 43 0 1378.71 10 11 1. 52 2758.70 2751 11 2.78E-03 71. 6 44 0 1461.25* 324 0 2.25 2923.80 2917 15 8.99E-02 5.o 45 0 1765.07* 32 0 2.89 3531. 46 3524 13 8.90E-03 18.6 Flag: "*" = Peak area was modified by background subtraction Page 3599 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:11:59 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 26-NOV-2015 14:25:00 G405235031 Acquisition date : Sample quantity Sample geometry . Detector geometry: 3-0CT-2016 09:09:51 139.62 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA32 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Interfering Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 Page 3600 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87 .*57 CD-109 88.03 AM-243 74.66 TH-228 .74.82 PB-212 74.82 CAN 0 01:00:00.58 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide, Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.119E+OO 1.398E+Ol 1.398E+Ol 11.23 OK ZN-65 1115. 54 so*. 60* 1.397E+OO l.045E-01 2.534E-01 93.95 OK CD-109 88.03 3.70* 4.556E+OO 8.954E-01 1.430E+OO 220.35 OK SN-126 64.28 9.60 2.229E+OO Line Not Found Absent 86.94 8.90 4.556E+OO 3. 722E-01 3.722E-01 220.35 OK 87.57 37.00* 4.556E+OO 8.954E-02 8.954E-02 220.35 OK BA-137M 661. 66 89.90* 2.104E+OO l.903E-01 1.941E-01 33.35 OK CS-137 661. 66 85.10* 2.104E+OO 2. OllE-01 2.051E-01 33.35 OK CE-141 145.44 48.29* 6.092E+OO 5.132E-02 3.958E+Ol 188.15 OK TL-208 277.37 6.60 4.277E+OO Line Not Found Absent 583.19 85.00* 2.325E+OO . 2. 750E-01 2.750E-01 35.35 OK 860.56 12.50 1. 714E+OO Line Not Found Absent BI-212 727. 33 6.67* 1.953E+OO 8.238E-01 8.238E-01 80.37 OK 785.37 1.10 1.839E+OO 3.649E+OO 3.649E+OO 88.65 OK 1620. 5.0 1. 47 1.022E+OO Line Not Found Absent PB-212 74.82 10.28 3.470E+OO 1.154E+OO 1.154E+OO 65.05 OK 77 .11 17.10 3.695E+OO 1.759E+OO 1. 759E+OO 28.75 OK 238.63 43.60* 4.787E+OO l.162E+OO l.162E+OO 12.28 OK 300 ."09 3.30 4.016E+OO Line Not Fou"nd Absent BI-214 609.32 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 OK 1120. 29 14.92 1.392E+OO 1.065E+OO l.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO l .121E+OO 37.23 OK PB-214 74.82 5.80 3.423E+OO Line Not Found <<INT Reject 77 .11 9.70 3.695E+OO 3 .101E+OO 3.102E+OO 28.75 OK 87.09 3.41 4.545E+OO Line Not Found <<INT Reject 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 18.42 4.062E+OO 1.254E+OO 1.255E+OO 31. 06 OK 351. 93 35.60* 3.518E+OO 1.068E+OO 1.069E+OO 23.21 OK RN-222 609.32 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 OK 1120. 29 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 OK RA-224 240.99 4.10* 4.743E+OO 3.688E-01 3.688E-01 356.75 OK RA-226 609.32 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 OK 1120. 29 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 OK AC-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11.27 3.639E+OO 1.114E+OO 1.114E+OO 51. 96 OK. 794.95 4.25 1.823E+OO Line Not Found Absent 835.71 1. 61 1. 7 53E+OO -----. Line Not Found Absent 911.20 25.80* 1.638E+OO 8.982E-01 8.982E-01 38.82 OK 968. 97 15.80 l.561E+OO l.031E+OO 1.031E+OO 45.21 OK RA-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11.27 3.639E+OO 1.114E+OO l .114E+OO 51. 96 OK 794.95 4.25 1.823E+OO Line Not Found Absent 835. 71 1. 61 1. 753E+OO Line Not Found Absent 911. 20 25.80* 1.638E+OO 8.982E-01 8.982E-01 38.82 OK 968. 97 15.80 1.561E+OO i. 031E+OO 1.031E+OO 45.21 OK TH-228 74.82 10.28 3.470E+OO 1.154E+OO 1.154E+OO 65.05 OK 77 .11 17'.10 3.695E+OO 1.759E+OO 1. 759E+OO 28.75 OK Page 3601 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 4.787E+OO l.162E+OO 1.162E+OO 12.28 OK 300.09 3.30 4. 016E+OO

Line Not Found Absent TH-230 609.32 45.49* 2.246E+OO 9.824E-01 9.824E-01 20. 96 OK 1120.29 14.92 l.392E+OO l.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 l.121E+OO 1.121E+OO 37.23 OK TH-232 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.639E+OO l .114E+00 l .114E+OO 51. 96 OK 835.71 1. 61 1.753E+OO Line Not Found Absent 911.20 25.80* 1.638E+OO 8.982E-01 8.982E-01 38.82 OK 968. 97 15.80 1. 561E+OO 1.031E+OO 1.031E+OO 45.21 OK U-234 609.32 45.49* 2.246E+OO 9.824E-01 9.824E-01 20. 96 OK 1120.29 14.92 l.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO l .121E+OO 37.23 OK U-235 89. 96 3.47 4.758E+00 Line Not Found Absent 93.35 5.60 4.976E+OO l.429E+00 1.429E+OO 81. 61 OK 143.76 10. 96* 6.095E+OO Line Not Found <<INT Reject. 163.33 5.08 5.924E+OO Line Not Found Absent 185. 72 57.20 5.605E+OO 1.411E-01 1. 411E-01 80.25 OK 205.31 5.01 5.302E+00 Line Not Found Absent AM-243 43.53 5.90 1.701E-01 Line Not Found Absent 74.66 67.20* 3.470E+OO 1. 765E-01 1. 765E-01 65.05 OK ANH-511 511. 00 100.00* 2.588E+00 l.067E-01 1.067E-01 80.01 OK Flag: "*" = *Keyline Page 3602 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:00.81 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *********************************************************************'********** * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l * *Acquisition date 3-0CT-2016 09:09:51 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
Sample date 26-NOV-2015 14:25:00 Analyst initials: MXRl *
Sample ID G405235031 Sample Quantity l.3962E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll * ***********************************************T*****T************************* Combined Activity-MDA NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuc1ide (pCi/GRAM ( 1. 96-sigma) K-40 1. 398E+Ol 1.539E+OO ZN-65 2.534E-01 2.333E-01 CD-109 1.430E+OO 3.089E+00 SN-126 8.954E-02 l.934E-01 BA-137M 1.941E-01 6. 344E...:.02 CS-137 2.051E-01 6.702E-02 CE-141 3.958E+Ol 7.297E+Ol TL-208 2.750E-01 9.527E-02 BI-212 8.238E-01 6.489E-01 PB-212 l.162E+OO 1.399E-01 BI-214 9.827E-01 2.019E-01 PB-214 1.069E+OO 2. 431E-01 RN-222 9.827E-01 2.019E-01 RA-224 3.688E-01 1. 289E+OO RA-226 9.827E-01 2.019E-01 AC-228 8.982E-01 3.417E-01 RA-228 8.982E-01 3.417E-01 TH-228 1.162E+00 1.399E-01 TH-230 9.824E-01 2.018E-01 TH-232 8.982E-01 3.417E-01 U-234 9.824E-01 2.018E-01 U-235 3.792E-01 4*. 020E-01 AM-243 1. 765E-01 1.125E-01 ANH-511 1.067E-01 8.368E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3603 of 5809 Key-Line Activity (pCi/GRAM -4.375E+OO 2.714E-02 0.000E+OO -1. 733E-02 8.642E-02 O.OOOE+OO K.L. Cnt Uncert (l.96-sigma) 1.407E+Ol 4.918E-02 1.129E+41 3.578E-02 3.686E-01 2.266E+04 MDA (pCi/GRAM 7.486E-01 3.281E-01 3.077E+OO 1.781E-01 5.102E-02 5.390E-02 6.698E+Ol 6.553E-02 7. 965E-01 9.344E-02 1.212E-01 1.382E-01 1.212E-01 1.00lE+OO 1.212E-01 2.730E-01 2.730E-01 9.344E-02 1. 211E-01 2.730E-01 1. 211E-01 4 .. 136E-01 1.255E-01 5.400E-02 MDA (pCi/GRAM 2.602E+Ol 1. 076E-01 0.000E+OO 6.485E-02 7.552E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 6.299E+02 O.OOOE+OO SHORT HLIF MN-54 -2.251E-02 7.482E-02 l.316E-01 NOT IDENT. C0-56 6.602E-02 5.547E-01 1.073E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.209E-02 5.630E-02 l.028E-01 NOT IDENT. C0-58 -2.868E-02 6.680E-01 1.267E+OO NOT IDENT. FE-59 7.864E-01 7.630E+OO l.584E+Ol NOT IDENT. C0-60 -1. 891E-02 3.538E-02 6.479E-02 NOT IDENT. GE-68 -1.027E+OO 2.286E+OO 4.299E+OO NOT IDENT. AS-73 9.986E+OO 1.955E+Ol 3.783E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.086E+04 O.OOOE+OO SHORT HLIF SE-75 3.508E-02 2.303E-01 4.339E-01 NOT IDENT. BR-77 O.OOOE+OO 8.219E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 1.012E+03 O.OOOE+OO SHORT HLIF RB-83 2.436E-01 6.334E-01 l.312E+OO NOT IDENT. KR-85 7.363E+OO 9.00lE+OO 1.690E+Ol NOT IDENT. SR-85 8.803E-01 1.078E+OO 2.024E+00 NOT IDENT. RB-86 O.OOOE+OO 4.289E+04 O.OOOE+OO SHORT HLIF Y-88 1. 089E-01 2.289E-01 5. 671E-01 NOT IDENT. Y-91 -2. 296E+02 5.789E+02 l.086E+03 NOT IDENT. NB-94 2.991E-02 3.730E-02 7.610E-02 NOT IDENT. NB-95 -5.163E-01 1.193E+OO l.806E+00 NOT IDENT. NB-95M -5.773E-01 2.845E+OO 4.843E+00 NOT IDENT. ZR-95 1.562E+OO 1. 743E+OO 3.764E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 672E+41 O.OOOE+OO SHORT.HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.638E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 406E+41 O.OOOE+OO SHORT HLIF RH-101 8.540E-03 3. 671E-02 6. 721E-02 NOT IDENT. RH-102 -4.078E-02 6.598E-02 9 ."7 OlE-02 NOT IDENT. RU-103 -5.023E+OO 7.687E+00 1.341E+Ol FAIL ABUN RH-106 -6.563E-02 6.005E-01 9. 996E-01 NOT IDENT. RU-106 -6.563E-02 6.005E-01 9. 996E-01 NOT IDENT. AG-108M 1.395E-02 2.864E-02 5.819E-02 NOT IDENT. AG-llOM 9.579E-02 7.959E-02 l.881E-01 FAIL ABUN SN-113 -5.297E-02 2.842E-01 5.306E-01 NOT IDENT. CD-115 O.OOOE+OO 1.186E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.777E+05 O.OOOE+OO SHORT HLIF TE-123M -4.232E-02 1.427E-01 2.739E-01 NOT IDENT. SB-124 3.304E-01 1. 813E+OO 4.393E+OO NOT IDENT. SB-125 -8.641E-02 l .115E-01 l.933E-01 FAIL ABUN TE-125M 7.801E+Ol 3.956E+02 7.207E+02 NOT IDENT. I-126 O.OOOE+OO 1. 960E+06 O.OOOE+OO SHORT HLIF SB-126 . O.OOOE+OO 3.054E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.015E+23 O.OOOE+OO SHORT HLIF I-131 0.000E+OO l.427E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 7.858E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.187E+27 O.OOOE+OO SHORT HLIF* BA-133 -2.023E-02 4.523E-02 7.292E-02 NOT IDENT. I-133 O.OOOE+OO 1.376E+41 0.000E+OO SHORT HLIF CS-134 3.667E-02 6.464E-02 1.284E-01 FAIL ABUN CS-135 1. 759E-02 1.624E-01 2.845E-01 NOT IDENT. I-135 O.OOOE+OO l.339E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.284E+05 0.000E+OO SHORT HLIF CE-139 3.429E-02 l.219E-01 2.428E-01 NOT IDENT. BA-140 O.OOOE+OO 2.846E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 7.893E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -3.216E-01 4.212E-01 6. 965E-01 NOT IDENT. PM-144 1.165E-02 6.301E-02 l.217E-01 NOT IDENT. PR-144 1.018E+OO 5.507E+OO 1.063E+Ol NOT IDENT. PM-146 3.303E-03 4.718E-02 9.095E-02 NOT IDENT. ND-147 O.OOOE+OO 6.622E+07 O.OOOE+OO SHORT HLIF PM-147 -4.625E+Ol 9.551E+02 l.705E+03 NOT IDENT. PM-149 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF EU-150 -4. 213E-03 3. 597E--02 4.801E-02 FAIL ABUN EU-152 -2.159E-04 l.060E-01 2.022E-01 FAIL ABUN GD-153 -5.504E-02 2.355E-01 4.158E-01 NOT IDENT. EU-154 5.825E-02 1.182E_:Ol 2.571E-01 NOT IDENT. EU-155 -9.052E-03 l.310E-01 2.344E-01 FAIL ABUN TB-160 -7.102E-02 2.371E+OO 3.997E+OO FAIL ABUN H0-166M -3.605E-02 7.798E-02 l.180E-01 NOT IDENT. TM-171 3.902E+OO 4. 541E+Ol 8.493E+Ol NOT IDENT. HF-172 -2.723E-01 2.607E-01 4.192E-01 NOT IDENT. LU-172 -1.317E-02 7.127E-02 l.412E-01 FAIL ABUN LU-176 -1.385E-02 2.550E-02 4.650E-02 FAIL ABUN HF-181 1.333E+OO 5.734E+OO 1.126E+Ol NOT IDENT. TA-182 l.057E-01 1. 024E+OO 2.066E+OO FAIL ABUN Page 3604 of 5809 RE-183 -1. 978E+00 5.353E+OO 9.626E+OO NOT IDENT. RE-184 -5.128E+OO 3.263E+Ol 6.161E+Ol NOT IDENT. W-188 -6.558E+Ol 1.394E+02 2.270E+02 NOT IDENT. IR-192 -3.755E-01 5.903E-01 1.062E+OO FAIL ABUN HG-203 2.157E+OO 3.262E+OO 6.567E+OO NOT IDENT. BI-207 -1.820E-02 5.147E-02* 9.798E-02 FAIL ABUN PB-210 3.590E+00 8.738E+OO l.698E+Ol NOT IDENT. BI-211 0.000E+OO 3.382E-01 7.893E-01 NOT IDENT. PB-211 1. 608E-01 7.550E-01 l.468E+OO NOT IDENT. RN-219 -1. 209E-01 4.508E-01 8.314E-01 FAIL ABUN RA-223 6.234E-02 6.689E-01 l. l 70E+OO FAIL ABUN AC-227 5.266E-02 2.289E-01 4.523E-01 NOT IDENT. TH-227 5.266E-02 2.289E-01 4.523E-01 NOT IDENT. TH-229 8.785E-02 5.032E-01 9.864E-01 FAIL ABUN PA-231 9.055E-02 5.282E-01 9.263E-01 NOT IDENT. TH-231 6.234E-02 6.689E-01 l.170E+OO FAIL ABUN PA-233 -3.171E-03 6.204E-02 l.189E-01 NOT IDENT. PA-234 6.928E-02 2.412E-01 5.230E--'01 FAIL ABUN' PA-234M -5.147E-01 4.015E+OO 8.051E+OO NOT IDENT. TH-234 l.369E-03 1. 948E+00 3.628E+OO FAIL ABUN NP-237 -3 .171E-03 6.204E-02 1.189E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF U-238 1.369E-03 1.948E+OO 3.628E+OO FAIL ABUN NP-239 5.605E-02 2.818E-01 5.145E-01 NOT IDENT. PU-239 1.082E+02 3.543E+02 6.482E+02 NOT IDENT. AM-241 -l.804E-01 2.143E-01 3.672E-01 NOT IDENT. CM-243 2.973E-02 l.157E-01 2.138E-01 NOT IDENT. BK-247 2. 0"27E-02' 7.794E-02 l.404E-01 NOT IDENT. CM-247 -6.403E-03 3.984E-02 7.448E-02 NOT IDENT. CF-249 -2.454E-02 3.752E-02 6.666E-02 NOT IDENT. CF-251 7.552E-02 1.234E-01 2.499E-01 NOT IDENT. Page 3605 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:58.68 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area. %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 310 10.66* 1.119E+OO 1.398E+Ol l.398E+Ol 11.23 ZN-65 1115. 54 14 50.60* l.397E+OO l.045E-01 2.534E-01 93.95 CD-109 88.03 60 3.70* 4.556E+OO 1.929E+OO 3.082E+OO 101.77 SN-126 64.28 ------9.60 2.229E+Od ------Line Not Found ------86.94 60 8.90 4.556E+OO 8.021E-01 8. 021E-01 101.77 87.57 60 37.00* 4.556E+OO 1.929E-01 1.929E-01 101.77 BA-137M 661.66 67 89.90* 2.104E+OO l.903E-01 1. 941E-01 33.35 CS-137 661.66 67 85.10* 2.104E+OO 2. OllE-01 2. 051E-01 33.35 CE-141 145.44 47 48.29* 6.092E+OO 8.607E-02 6.638E+Ol 108.17 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 101 85.00* 2.325E+OO 2.750E-01 2.750E-01 35.35 860.56 ------12.50 1.714E+OO ------Line Not Found ------BI-212 727. 33 20 6. 67* 1.953E+OO 8.238E-01 8.238E-01 80.37 785.37 14 1.10 1.839E+OO 3.649E+OO 3.649E+OO 88.65 1620.50 ------1. 47 1.022E+OO ------Line Not Found ------PB-212 74.82 119' 10.28 3.470E+OO 1.787E+OO 1. 787E+OO' 41. 48 77 .11 207 17.10 3.695E+00 1.759E+OO 1. 759E+00 28.75 238.63 451 43.60* 4.787E+OO l.162E+OO 1.162E+OO 12.28 300.09 ------3.30 4.016E+OO ------Line Not Found ------BI-214 609.32 187 45.49* 2.246E+00 9.824E-01 9.827E-01 20.96 1120.29 41 14.92 l.392E+OO l.065E+00 l.065E+00 44.24 1764.49 30 15.30 9.460E-01 l .121E+OO 1.121E+OO 37.23 PB-214 74.82 .119 5.80 3.470E+OO 3.167E+OO 3.168E+OO 41. 48 77 .11 207 9.70 3.695E+OO 3. lOlE+OO 3.102E+OO 28.75 87.09 60 3.41 4.556E+OO 2.093E+00 2.094E+OO 101.77 242.00 85 7.25 4.743E+OO l.330E+00 1.331E+OO 53. 67 295.22 174 18.42 4.062E+OO 1.254E+OO 1.255E+OO 31. 06 351.93 249 35.60* 3.518E+OO 1.068E+OO l.069E+00 23.21 RN-222 609.32 187 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 1120.29 41 14.92 1.392E+OO l.065E+00 1.065E+OO 44.24 1764.49 30 15.30 9.460E-01 l .121E+OO 1.121E+OO 37.23 RA-224 240.99 85 4.10* 4.743E+00 2.353E+OO 2.353E+OO 53.67 RA-226 60,9.32 187 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 1120.29 41 14.92 1.392E+OO l.065E+00 1.065E+OO 44.24 1764.49 30 15.30 9.460E-01 l .121E+OO 1.121E+OO 37.23 AC-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 85 11. 27 3.639E+OO l.114E+OO 1.114E+OO 51. 96 794.95 ------4.25 1.823E+OO ------Line Not Found ------835.71 ------1. 61 1. 753E+OO ------Line Not Found ------911. 20 71 25.80* 1.638E+OO 8.982E-01 8.982E-01 38.82 968.97 47 15.80 l.561E+00 1.031E+OO 1.031E+OO 45.21 RA-'-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 85 11. 27 3.639E+OO l .114E+OO 1.114E+OO 51. 96 794.95 ------4.25 1.823E+00 ------Line Not Found ------835.71 ------1. 61 1. 753E+Ob ------Line Not Found ------911.20 71 25.80* 1. 638E*+oo 8.982E-01 8.982E-01 38.82 968. 97 47 15.80 l.561E+00 1. 031E+OO l.031E+OO 45.21 Page 3606 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 119 10.28 3.470E+OO 1.787E+OO 1.787E+OO 41. 48 77 .11 207 17.10 3.695E+OO 1.759E+OO 1.759E+OO 28.75 238.63 451 43.60* 4.787E+OO 1.162E+OO 1.162E+OO 12.28 300.09 ------3.30 4.016E+OO ------Line Not Found ------TH-230 609.32 187 45.49* 2.246E+OO 9.824E-01 9.824E-01 20.96 1120.29 41 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 1764.49 30 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 TH-232 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 85 11. 27 3.639E+OO l .114E+OO 1.114E+OO 51. 96 835. 71 ------1.61 1. 753E+OO ------Line Not Found ------911. 20 71 *25.80* l.638E+OO 8.982E-01 8.982E-01 38.82 968. 97 47 15.80 1. 561E+OO 1.031E+OO 1. 031E+OO 45.21 U-234 609.32 187 45.49* 2.246E+OO 9. 824E-01 . 9.824E-01 20.96 1120.29 41 14.92 1.392E+OO 1.065E+OO 1. 065E+00 44.24 1764.49 30 15.30 9.460E-01 l.121E+OO 1.121E+OO 37.23 U-235 89.96 ------3.47 4.758E+OO ------Line Not Found ------93.35 74 5.60 4.976E+OO 1. 429E+OO 1.429E+OO 81. 61 143.76 47 J,0.96* .6. 092E+OO 3.792E-01 3.792E-01 108.17 163.33 ------5.08 5.924E+OO ------Line Not Found ------185.72 84 57.20 5.605E+OO 1. 411E-01 1. 411E-01 80.25 205.31 ------5.01 5.302E:+OO ------Line Not Found ------AM-243 43.53 ------5.90 1. 701E-01 ------Line Not Found ------74.66 119 67.20* 3.470E+OO 2.733E-01 2.733E-01 41. 48 ANH-511 511. 00 51 100.00* 2.588E+OO l.067E-01 1.067E-01 80.01 Flag: "*" Key line Page 3607 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Total number of lines in spectrum 45 Number of unidentified lines 13 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 ZN-65 CD-109 SN-126
BA-137M CS-137 CE-141 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1.25E+09Y 244.06D 461. 40D 2.30E+05Y* 30.08Y 30.08Y 32.51D l.41E+l0Y 1. 41E+10Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1: 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 2.42 1. 60 1. 00 1. 02 1. 02 771. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.398E+Ol l.045E-01 1.929E+OO 1. 929E-01 l.903E-01 2. OllE-01 8.607E-02 2.750E-01 8.238E-01 l.162E+OO 9.824E-01 1.068E+OO 9.824E-01 2.353E+00 9.824E-01 8.982E-01 8.982E-01 l.162E+OO 9.824E-01 8.982E-01 9.824E-01 3.792E-01 2.733E-01 l.067E-01 3.189E+Ol 3.189E+Ol Decay Corr pCi7GRAM 1.398E+Ol 2.534E-01 3.082E+OO 1.929E-01 l.941E-01 2.051E-01 6.638E+Ol 2.750E-01 8.238E-01 1.162E+OO 9.827E-01 1.069E+OO 9.827E-01 2.353E+00 9.827E-01 8.982E-01 8.982E-01 l.162E+00 9.824E-01 8.982E-01 9.824E-01 3.792E-01 2.733E-01 1.067E-01 9.950E+Ol 9.950E+Ol 71.11% Decay Corr 2-Sigma Error 0.157E+Ol 2.380E-01 3.137E+OO 1. 964E-01 0.647E-01 0.684E-01 7.180E+Ol 0. 972E-01 6.621E-01 0.143E+OO 2.060E-01 0.248E+OO 2.060E-01 1.263E+OO 2.060E-01 *3. 487E-01 3.487E-01 0.143E+OO 2.059E-01 3.487E-01 2.059E-01 4.102E-01 l .134E-01 0.854E-01 "M" Manually accepted 2-Sigma %Error 11.23 93.95 101.77 101.77 33.35 33.35 108.17 35.35 80.37 12.28 20. 96 23.21 20. 96 53.67 20. 96 38.82 38.82 12.28 20. 96 38.82 20. 96 108.17 41. 48 80.01 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3608 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235031 Acquisition date : 3-0CT-2016 09:09:51 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 208.93 50 139 0.93 419.07 413 12 1. 24E-02 **** 5.24E+OO 0 271.27 36 119 2.19 543.76 536 13 9.lOE-03 **** 4.35E+OO T 0 328.63 69 62 1. 61 658.48 652 15 1. 77E...:.02 57.3 3.73E+00 T 0 367. 02 19 39 2.46 735.27 730 11. 4. 95E-03 **** 3.40E+OO T 0 463. 71 16 30 0.67 928.65 925 9 4.17E-03 **** 2.80E+OO T 0 563.44 28 12 1. 81 1128 .11 1123 12 7.50E-03 64.2 2.39E+OO T 0 572.16 20 27 1. 44 1145.56 1140 14 5. 32E:.._03 **** 2.36E+OO 0 627.98 17 18 0.82 1257.20 1250 12 4.50E-03 **** 2.19E+00 1 666.32 18 9 1. 80 1333.89 1317 22 4.76E-03 80.2 2.09E+OO T 0 670.67 9 11 0.67 1342. 59 1338 7 2.36E-03 **** 2.08E+OO 0 717.06 13 19 4.54 1435.36 1427 13 3.45E-03 **** l.98E+OO 0 768.71 33 23 6.07 1538.68 1531 15 9.03E-03 72. 7 1.87E+OO 0 799.40 25 51 4.04 1600.05 1583 29 6.94E-03 **** 1. 81E+OO 0 883.49 9 2 1.23 1768.23 1764 8 2.54E-03 84.8 1.68E+OO T 0 961. 54 11 5 0.81 1924.35 1921 7 2.99E-03 98 ._9 1.57E+OO T 0 965.08 14 9 0. 96 1931.43 1927 9 4.0lE-03 96. 9 1. 57E+OO T 0 1054.10 6 16 3.99 2109.46 2100 11 1. 81E-03 **** 1.46E+OO 0 1175.28 8 7 1.28 2351. 84 2345 9 2.22E-03 **** 1.34E+OO 7 1191. 67 20 10 2.92 2384.61 2381 12 5.64E-03 63.1 l.33E+00 7 1194.36 8 9 1. 83 2390.00 2381 12 2.15E-03 **** l.32E+OO 0 1302.02 13 3 4.15 2605.31 2598 13 3.85E-03 75.8 1.23E+OO 0 1378.71 10 11 1. 52 '2758.70 2751 11 2. 78E-03 **** 1.18E+OO Flags: "T" = Tentatively associated Page 3609 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:12.78
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA. GAMMA.ARCHIVE. GAMMA] G40.5235031. CNF; 1 * *Acquisition date 3-0CT-2016 09:09:51 Sensitivity 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
Sample date 26-NOV-2015 14:25:00 Nuclide Library : SOLID *
Sample ID G405235031 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.3962E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF CAN.CNF;ll
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le .(pCi/GRAM 3.132E-01 1. 389E-01. 1.467E+OO 8.456E-02 2.152E-02 2.273E-02 3.150E+Ol 2.902E-02 3.415E-01 4. 311E-02 5.333E-02 6.314E-02 5.333E-02 4.620E-01 5.333E-02 l.191E-01 1.191E-01 4.311E-02 5.331E-02 l.191E-01 5. 331E-02 1.955E-01 5.939E-02 2.413E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3610 of 5809 Le (pCi/GRAM 1.150E+Ol 4.647E-02 O.OOOE+OO 2.455E-02 3.194E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 . M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 No.:.147 PM-147 PM-149 EU-150 EU-152 .GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page3611of5809 5.738E-02 4.669E-01 O.OOOE+OO 4.814E-02 5.461E-01 6.740E+OO 2.563E-02 1.797E+OO 1.777E+Ol 0.000E+OO l.994E-01 O.OOOE+OO O.OOOE+OO 5.766E-01 7.749E+OO 9.281E-01 O.OOOE+OO 2.226E-01 4.571E+02 3.437E-02 7.879E-01 2.238E+OO 1.672E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.I40E-02 4.141E-02 5.944E+OO 4.394E-01 4.394E-01 2. 631.E-02 7. 971E-02 2.420E-01 O.OOOE+OO O.OOOE+OO 1.277E-01 1.633E+OO 8.627E-02 3. 391E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.280E-02 O.OOOE+OO 5.790E-02 1.316E-01 O.OOOE+OO O.OOOE+OO 1.137E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.243E-01 5.416E-02 4.734E+oo* 4.lOlE-02 0.000E+OO 7. 965E+02 0.000E+OO 2.185E-02 9.291E-02 1.955E-01 1.107E-01 l.098E-01 1.710E+OO 5.210E-02 3.986E+Ol 1.943E-01 5.936E-02 2.122E-02 5.073E+OO 8.952E-01 4.479E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF .SHORT HLIF
SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT*. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 .AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3612 of 5809 2.555E+01 1.034E+02 4.871E-01 3.060E+OO 4.209E-02 7.947E+OO 3.784E-01 6.709E-01 3.799E-01. 5.351E-01 2.087E-01 2.087E-01 4.620E-01 4.281E-01 5. 351E-*01 5.444E-02 2.230E-01 3.451E+OO 1.715E+OO 5.444E-02 O.OOOE+OO 1. 715E+OO 2.410E-01 3.043E+02 1. 706E-01 1. OOlE-01 6.455E-02 3.395E-02 2.983E-02 l.173E-01 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:17.87 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l *
Acquisition date 3-0CT-2016 09:09:51 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
Sample .date 2 6-NOV-2015 14: 25: 00 Nuclide Library : SOLID *
Sample ID G405235031 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.3962E+02 GRAM *
Quantity Err(%) : 1.4325E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.398E+Ol 1. 703E+OO 1. 703E+OO ZN-65 2.534E-01 2.335E-01 2.335E-01 CD-109 l.430E+OO 3.097E+OO 3.097E+OO SN-126 8.950E-02 1.938E-01 l.938E-01 BA-137M 1. 941E-01 6.399E-02 6.399E-02 CS-137 2. 051E-01 6.759E-02 6.759E-02 CE-141 3.958E+Ol 7.302E+Ol 7.302E+Ol TL-208 2.750E-01 9.599E-02 9.599E-02 BI-212 8.238E-01 6.502E-01 6.502E-01 PB-212 1.162E+OO 1.530E-01 1.530E-01 BI-214 9.827E-01 2.062E-01 2.062E-01 PB-214 1.069E+OO 2.472E--:Ol 2. 472E-01 RN-222 9.827E-01 2.062E-01 2.062E-01 RA-224 3.680E-01 1.295E+OO 1.295E+00 RA-226 9.827E-01 2.062E-01 2.062E-01 AC-228 8.982E-01 3.448E-01 3.448E-01 RA-228 8.982E-01 3.448E-01 3.448E-01 TH-228 1.162E+OO l.530E-01 1.530E-01 TH-230 9.824E-01 2.062E-01 2.062E-01 TH-232 8.982E-01 3.448E-01 3.448E-01 U-234 9.824E-01 2.062E-01 2.062E-01 U-235 3.792E-01 4.025E-01 4.025E-01 AM-243 1. 765E-01 l.137E-01 l.137E-01 ANH-511 l.067E-01 8.379E-02 8.379E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide ('pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) BE-7 -4.375E+OO 1.408E+Ol 1. 421E+Ol NOT IDENT. NA-22 2. 714E-02 5.068E-02 NOT IDENT. NA-24 l.OOOE+41 1.217E+41 O.OOOE+OO SHORT HLIF AL-26 -1.733E-02 3.579E-02 3.664E-02 NOT IDENT. SC-46 8.642E-02 3.686E-01 3.706E-01 FAIL ABUN V-48 1.544E+04 2.267E+04 2.372E+04 SHORT HLIF Page 3613 of 5809 CR-51 1. 41 7E+02 6.299E+02 6.332E+02 SHORT HLIF MN-54 -2.251E-02 7.483E-02 7. 551E-02 NOT IDENT. C0-56 6.602E-02 5.547E-01 5.555E-01 NOT IDENT. MN-56 l.000E+41 7.923E+41 O.OOOE+OO SHORT HLIF C0-57 l.209E-02 5.631E-02 5.657E-02 NOT IDENT. C0-58 -2.868E-02 6.680E-01 6.681E-01 NOT IDENT. FE-59 7.864E-01 7.630E+OO 7.638E+OO NOT IDENT. C0-60 -1. 8 91E-02 3.539E-02 3.640E-02 NOT IDENT. GE-68 -l.027E+OO 2.286E+OO 2.332E+OO NOT IDENT. AS-73 9.986E+OO 1. 966E+Ol 2.017E+Ol NOT IDENT. AS-74 -l.574E+03 l.086E+04 l.089E+04 SHORT HLIF. SE-75 3.508E-02 2.304E-01 2.309E-01 NOT IDENT. BR-77 6.827E+39 6.144E+40 O.OOOE+OO SHORT HLIF SR-82 -4.920E+02 l.013E+03 1.037E+03 SHORT HLIF RB-83 2.436E-01 6.343E-01 6.437E-01 NOT IDENT. KR-85 7.363E+OO 9.006E+OO 9.598E+OO NOT IDENT. SR-85 8.803E-01 1.079E+OO l.149E+OO NOT IDENT. RB-86 -l.277E+04 4.289E+04 4.328E+04 SHORT HLIF Y-88 1. 089E-01 2.291E-01 2.343E-01 NOT IDENT. Y-91 -2. 296E+02 5.790E+02 5.882E+02 NOT IDENT. NB-94 2.991E-02* 3.732E-02 3. 969E-02 NOT IDENT. NB-95 -5.163E-01 l.193E+OO l.216E+OO NOT IDENT. NB-95M :...5.773E-01 2.846E+OO 2.858E+OO NOT IDENT. ZR-95 1.562E+OO 1. 745E+OO 1. 881E+OO NOT IDENT. NB-97 1.000E+41 1.672E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.000E+41 1. 37 6E+43 O.OOOE+OO SHORT HLIF M0-99 -1.495E+33 3.640E+33 O.OOOE+OO SHORT HLIF TC.:...99M -1.000E+41 1.409E+41 O.OOOE+OO SHORT HLIF RH-101 8.540E-03 3.674E-02 3. 69AE-02 NOT IDENT. RH-102 -4.078E-02 6.607E-02 6.85BE-02 NOT IDENT. RU-103 -5.023E+OO 7. 691E+OO 8.017E+OO FAIL ABUN RH-106 -6.563E-02 6.005E-01 6.012E-01 NOT IDENT. RU-106 -6.563E-02 6.00SE-01 6.012E-01 NOT IDENT. AG-108M l.395E-02 2.864E-02 2.933E-02 NOT IDENT. AG-llOM 9.579E-02 7.974E-02 9.068E-02 FAIL ABUN SN-113 -5.297E-02 2.842E-01 2.852E-01 NOT IDENT. CD-115 6.198E+39 1.18 6E+4 l O.OOOE+OO SHORT HLIF SN-ll 7M 9.306E+03 l.777E+05 l.777E+05 SHORT HLIF TE-123M -4.232E-02 l.427E-01 l.440E-01 NOT IDENT. SB-124 3.304E-01 1. 813E+OO l.819E+00 NOT IDENT. SB-125 -8.641E-02 l .115E-01 l.181E-01 FAIL ABUN TE-125M 7.801E+Ol 3.957E+02 3. 972E+02 NOT IDENT. I-126 2.494E+06 l.991E+06
2 .287E+06 SHORT HLIF SB-126 -l.412E+06 3.066E+06 3 .131E+06 SHORT HLIF SB-127 -l.142E+22 2. 021E+23 O.OOOE+OO SHORT HLIF I-131 9.326E+09 l.427E+l0 l.488E+l0 SHORT HLIF I-132 l.000E+41 1.923E+42 O.OOOE+OO SHORT HLIF TE-132 7.335E+26 5.197E+27 O.OOOE+OO SHORT HLIF BA-133 -2.023E-02 4.524E-02 4.61'.5E-02 NOT IDENT. I-133 -l.000E+41 2.331E+41 0.000E+OO SHORT HLIF CS-134 3.667E-02 6.466E-02 6.674E-02 FAIL ABUN CS-135 l.759E-02 l.624E-01 1. 62 6E-01 NOT IDENT. I-135 l.000E+41 7.171E+41 O.OOOE+OO SHORT HLIF CS-136 2.163E+04 7.284E+05 7.285E+05 SHORT HLIF CE-139 3.429E-02 1.221E-01 1. 231E-01 NOT IDENT. BA-140 3.653E+05 2.846E+06 2.851E+06 SHORT HLIF LA-140 -4.757E+05 7.896E+05 8.183E+05 SHORT HLIF CE-143 l.OOOE+41 2.451E+41 0.000E+OO SHORT HLIF CE-144 -3.216E-01 4.216E-01 4.458E-01 NOT IDENT. PM-144 l.165E-02 6.301E-02 6.323E-02 NOT IDENT. PR-144 l.018E+OO 5.508E+OO 5.527E+OO NOT IDENT. PM-146 3.303E-03 4.718E-02 4. 720E-02 NOT IDENT. ND-147 -l.085E+07 6.622E+07 6.640E+07 SHORT HLIF PM-147 -4.625E+Ol 9. 551E+02 9.553E+02 NOT IDENT. PM-149 -1. OOOE+41 2.143E+41 O.OOOE+OO SHORT HLIF EU-150 -4. 213E-03 3.597E-02 3.602E-02 FAIL ABUN EU-152 -2. 15.9E-04 l.060E-01 l.060E-01 FAIL ABUN GD-153 .-5. 504E-02 2.355E-01 2.368E-01 NOT IDENT. EU-154 5.825E-02 l.182E-01 l.211E-01 NOT IDENT. EU-155 1.310E-01 1.310E-01 FAIL ABUN TB-160 -7.102E-02 2. 371E+OO 2. 371E+OO FAIL ABUN H0-166M -3.605E-02 7.800E-02 7. 968E-02 NOT IDENT. TM-171 3.902E+OO 4.541E+Ol 4.544E+Ol NOT IDENT. HF-172 -2. 723E-01 2.644E-01 2.915E-01 NOT IDENT. LU-172 -l.317E-02 7.129E-02 7.153E-02 FAIL ABUN LU-176 -1. 385E-02
2.550E-02 2.626E-02 FAIL ABUN HF-181 l.333E+OO 5.735E+OO 5.766E+OO NOT IDENT. TA-182 l.057E-01 l.024E+OO l.025E+OO FAIL ABUN Page 3614 of 5809 RE-183 -1. 978E+.00 5.363E+OO 5.436E+OO NOT IDENT. RE-184 -5.128E+OO 3.265E+Ol 3.273E+Ol NOT IDENT. W-188 -6.558E+Ol l.396E+02 l.427E+02 NOT IDENT. IR-192 -3.755E-01 5.905E-01 6.143E-01 FAIL ABUN HG-203 2.157E+OO 3.264E+OO 3.406E+OO NOT IDENT. BI-207 -l.820E-02 5.147E-02 5.212E-02 FAIL ABUN PB-210 3.590E+OO 8.744E+OO* 8.893E+OO NOT IDENT. BI-211 1.660E+OO 3.463E-01 8.244E-01 NOT IDENT. PB-211 1.608E-01 7.550E-01 7.585E-01 NOT IDENT. RN-219 -1.209E-01
4. 511E-01 4.544E-01 FAIL ABUN RA-223 6.234E-02 6.689E-01 6.695E-01 FAIL ABUN AC-227 5.266E-02 2.290E-01 2.302E-01 NOT IDENT. TH-227 5.266E-02 2.290E-01 2.302E-01 NOT IDENT. TH-229 8.785E-02 5.032E-01 5.048E-01 FAIL ABUN PA-231 9.055E-02 5.285E-01 5. 301E-01 NOT IDENT. TH-231 6.234E-02 6.689E-01 6.695E-01 FAIL ABUN PA-233 -3.171E-03 6.204E-02 6.206E-02 NOT IDENT. PA-234 6.928E-02 2.539E-01 2.558E-01 FAIL ABUN PA-234M -5.147E-01 4.015E+OO 4.022E+OO NOT IDENT. TH-234 1.369E-03 1.948E+OO 1.948E+OO FAIL ABUN NP-237 -3 .171E-03 6.204E-02 6.206E-02 FAIL ABUN NP-238 l.OOOE+41 3.763E+41 0.000E+OO SHORT HLIF U-238 1. 369E-03 1.948E+OO 1.948E+OO FAIL ABUN NP-239 5.605E-02 2.818E-01 2.829E-01 NOT IDENT. PU-239 l.082E+02 3.543E+02 3.577E+02 NOT IDENT. AM-241 -1. 804E-01 2.147E-01 2.296E-01 NOT IDENT. CM-243 2.973E-02 1.157E-01 l.165E-01 NOT IDENT. BK-247 2.027E-02 7.804E-02 7.858E-02 NOT IDENT. CM-247 -6.403E-03 3.985E-02 3.995E-02 NOT IDENT. CF-249 -2.454E-02 3.757E-02 3.916E-02 NOT IDENT. CF-251 7.552E-02 1.237E-01 1.283E-01 NOT IDENT. Page 3615 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY . MDA COUNTS ENERGY MDA COUNTS 43.53 67.9872 87.09 116.4670 136.47 80.9586 45.60 57.0555 87.57 116. 5350 140.51 0.0000 46.54 56.0303 88.03 139.6028 143.76 77.2956 49.72 0.0000 88.34 139.6547 144.24 77.3293 51. 35 74.5733 88.47 142.8516 145.44 83.3016 51.87 73.5071 89.96 124.0261 152.43 64.3407 52.39 75.8340 1093.63 97.8692 153.25 0.0000 52.97 66.8429 91.11 0.0000 323.87 71. 2228 53.44 68.0280 92.59 122.0207 156.02 0.0000 54.07 78.3123 93.35 122.1289 158.56 0.0000 57.36 0.0000 94.56 92.7254 159.00 69.8098 57.53 66.1910 94.65 92.7349 162.33 72. 5644 57.98 68.5213 94.67 92.7372 162.66 0.0000 59.27 68.6579 94.87 92.7585 163.33 73.4793 59.32 76.6738 97.43 89.0211 165.86 65.9259 59.54 77.8445 98.43 97.5526 176.31 68.2073 60. 96 73.4236 98.44 97.5539 176.60 0.0000 61.17 70.0040 99.53 74.7626 177.52 64.8148 62.93 87.4475 100 .11 69.9848 181.07 0.0000 63.29 87.4939 102.03 89.4818 181.52 65.0169 63.58 82.9244 103.18 70.2233 184.41 67. 7676 64.28 94.5386 103.37 66.6049 143.76 67.8350 66.73 83.3038 105.21 76.4462 193.51 69.1073 67.24 91. 4697 105.31 76.4549 197.03 69.2865 125.81 90.3684 106.12 83.8095 198.01 69.3364 67.75 90.3773 106.47 75.3354 201.83 62.4876 69.67 91.7834 109.28 79.2183 203.43 59.4759 70.83 97.7492 111. 00 84.2464 205.31 71. 4666 72.81 108.9050 111.76 0.0000 210.85 50.4885 72. 87 105.8018 114.06 71.0419 . 215. 65 47.1023 74.66 104.1074 116.30 0.0000 2°22 .11 55.3449 74.82 104.1298 116.74 68.7806 227.09 51. 0521 74.97 104.1509 119. 76 68.9908 227.38 47.4786 77 .11 104.4463 121.12 69.0848 228.16 0.0000 78.74 101.9242 121.22 69.0917 228.18 51. 0892 79.69 87.9193 121. 78 72.8335 116.74 51.0892 80.12 78.5426 122.06 66.6797 235.69 54.0448 80.19 0.0000 122.92 61.7928 235. 96 54. 054.0 80.57 110. 0230 123.07 61. 8019 238.63 47.8307 81. 00 84.9210 265.00 66.7860 238.98 0.0000 81. 07 84.9287 125.81 79.3188 240.99 47.9035 81.75 113. 3364 127.23 62.0529 242.00 47.9342 83.79 80.4859 127.91 73.2708 244.70 54.3591 84.00 71. 0353 129.30 70.8812 252.40 0.0000 85.43 105.9518 131.20 64.7810 252.80 . 49.1726 86.55 116. 3900 133.02 67.3879 254.15 0.0000 86.79 116. 4243 133.52 79.9043 256.23 43.8020 86.94 116.4460 136. 00 72.5805 260.90 0.0000 Page 3616of5809 ENERGY MDA .COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 40.7262 355.39 0.0000 584.27 20.1334 264.80 38.5282 356.01 34.7073 595.83 0.0000 265.00 38.5325 364.49 0.0000 427.87 22.3792 268.22 48.2585 366.42 0.0000 602.52 0.0000 269.46 46.9150 372. 51 31.4890 604.72 22. 4108 270.03 46.9305 375.05 30.1650 607.14 17.6232 271.23 46.9637 377.52 33.1229 609.32 18.1711 273.65 0.0000 356.01 28.3368 610.33 18.1773 276.40 58.7464 388.16 34.2687 614.28 17.6662 277.37 49.9076 388.63 0.0000 618.01 22.5125 277.60 48.9898 391.69 39.2285 620.36 17.1660 278.00 46.2270 264.66 30.5282 621.93 19.3220 279.20 49.0351 401.81 42.3675 630.19 0.0000 279.54 59.2240 402.40 38.4366 631. 29 19.3828 27*9. 70 59.2292 404.85 34.5329 633.25 9.6976 280.46 67.5880 410.95 38.5858 634.78 0.0000 283.69 41. 7426 413.71 28.7274 635.95 17.2559 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 50.1405 423. 72 0.0000 645.85 11. 9019 285.90 0.0000 427.09 34.8768 657.76 9.7760 287.50 35.3258 427.87 34.8889 657.90 0.0000 290.67 44.7031 433.94 22.9874 661.66 9.7881 293.27 0.0000 439.40 17.0308 664.57 0.0000 351. 93 42.9509 453.88 27.2153 666.33 0.0000 295. 96 42. 9687 463.37 23:2751 666.50 0.0000 879.38 63.1439 468.07 27.3763 667. 71 0.0000 299.98 42.1289 473.00 0.0000 677. 62 17.4902 300.09 42.1317 475.06 18.3029 685.70 0.0000 300.13 42.1326 476.78 27.4735 695.00 0.0000 301.36 46.3770 477.60 23.4113 696.49 19.7930 302.85 49.6972 482.18 24.4741 696.51 19.7930 256.23 39.4186 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.8980 306.78 46.0462 497.08 29.7487 697.49 20.8995 308.46 36.6823 505.52 15.4382 702.65 16.5259 311. 90 40.5207 507.63 0.0000 706.68 28.6798 316.51 52.9022 511. 00 23. 7225 711.68 26.5146 319.41 0.00'00 514.00 26.3311 720.70 0.0000 320.08 0.0000 514.00 26.3311 721.93 0.0000 321. 04 46.4011 520.40 13.4570 722.78 11. 6395 323.87 36.9870 520.69 0.0000 722. 91 14. 9656 325.23 48.4019 522.65 0.0000 723.31 13.3042 328.76 0.0000 527.90 0.0000 724.19 19.9614 333.37 37.1711 528.26. 13. 4972 727.33 12.2103 333.97 37.1822 529.59 17.6585 733.00 6.6714" 334.37 31. 4686 529.87 0.0000 735.93 8.9030 338.28 42.9977 531. 02 0.0000 333.97 17.8145 338.32 42. 9987 537.26 0.0000 739.50 0.0000 . 311. 90 45. 9160' 546.56 0.0000 747.24 6.6997 340.4.8 45.9160 552.55 34.5724 748.06 12.2859 340.55 0.0000 563.25 18.9309 752.31 12. 3011 344.28* 43.1296 569.33 27.4049 753.82 0.0000 345.93 48.3461 946.00 27.4060 756.73 11.1975 351.06 37.5067 569.70 27.4081 756.80 11.1979 351. 93 37.5234 583.19 20.1257 884.68 6.7327 Page 3617 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 21.8931 1274.44 7.1567 1620.50 4.0481 766.42 21.3356 1001.03 10.7476 1621.92 6.0736 766.84 21.3379 1002.74 6.2720 1678.03 0.0000 772. 60 0.0000 1004.73 12.5499 1690.97 2.0475 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0714 778.90 12. 3965 1028.54 0.0000 1063.66 9.3296 783.70 0.0000 1037.84 12.6473 1771. 35 2.0736 785.37 10.1613 1038.76 0.0000 1791.20 0.0000 792.07 16.9678 631.29 5.7934 1808.65 6.2563 794.95 20.3782 1048.07 0.0000 1810.72 0.0000 795.86 20.3833 1049.04 15.9414 1836.06 2.0941 810.06 15.9169 1050.41 11. 5977 810.29 15.9180 1063.66 12.7234 344.28 13.6445 1077.00 0.0000 810.76 13.6455 1077.34 12.7627 815.77 0.0000 1085.87 10.0473 1048.07 0.0000 1093.63 10.9797 832.01 12.5818 1099.45 10.0775 834.85 18.3151 1112. 07 11. 7 594 835. 71 14.8847 1112.84 7. 3511 836.80 0.0000 1115. 54 10.2977 846.75 0.0000 1120.29 10.3079 846.77 '13.7808 1120. 55 10.3086 856.80 0.0000 1221.41 10.3106 860.56 12.6794 1129. 67 11. 0669 871.09 8.0912 1131. 51 0.0000 873.19 9.2523 1147.95 0.0000 875.33 0.0000 1173.23 7.4473 879.38 12.1633 1177.95 5. 9641 880.51 15.6429 1189.05 4.4833 883.24 8.1171 1204.77 13 .1199 884.68 5.2200 1221.41 13.1643 889.28 8.1299 1231.02 11.3064 894.76 8.1413 1235.36 0.0000 898.04 16.2969 1238.28 16.9849 900. 72 6.9890 1260.41 0.0000 903.28 9.3249 1271.87 14.2502 911.20 15.7676 1274.44 8.5545 912.08 15.7714 1274.54 8.5545 923.98 0.0000 1291.59 10. 4911 926.50 7.9146 1298.22 0.0000 929 .11 18.4795 1312 .11 0.0000 937.49 17.6367 1332.49 8.6523 944 .13 0.0000 1362.66 0.0000 946.00 8.8370 1365.19 9.6735 949.00 12.3812 1368.63 0.0000 667.71 0.0000 1384.29 4.8541 962. 31 0.0000 1408.01 6.8257 964.08 0.0000 1457.56 0.0000 966.17 10.6575 1460.82 8.8610 911.20 11.3758 1489.16 3.9583 968. 97 11.3758 1505.03 8.9308 983 .*53 0.0000 1584.12 8.0474 984.45 0.0000 1596.21 0.0000 Page 3618of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:12:46.63 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * , Charleston, SC 2 9407 , * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;134 Background date : Z-OCT-2016 11:02:13. Sample date 23-NOV-2015 11:48:00 Acquisition date : 3-0CT-2016 09:10:21. Sample ID G40523-5032 Sample quantity : 1.46947E+02 GRAM Detector name : GAM39 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:07.00 0.2% Energy tolerance 1. 50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID LCS ID 1556 ******************************************************************************** Pk It 1 0 2 0 3 3 4 3 5 0 6 0 7 0 8 0 9 0 10 0 11 4 12 4 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 . 0 23 0 . 24 . 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 46.54* 63.44* 74.79* 77.18* 84.33* 86.94 92.93* 185.82* 195.09 210.13 238.80* 241.85 295.22* 300.60* 327.47 338.81* 352.21* 463.35 511. 57* 583.73* 601. 68 609.44* 661. 59 694.50 727.35* 785.08 870.59 87 5. 67 911.48* 969. 95* 1027.79 1095.58 1102. 55 1120.45 Page 3619of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 79 93 238 305 35 63 83 83 21 46 373 115 119 23 57 65 164 30 37 86 21 153 57 26 39 30 16 8 71 27 7 7 20 28 173 303 179 135 167 157 163 83 76 109 65 59 41 57 45 62 79 17 32 42 6 17 41 38 16 15 13 6 13 34 3 12 0 9 2.05 1. 39 1. 55 1. 08 1. 03 0.82 1.29 1. 33 0.52 2.74. 1. 33 1. 90 1. 36 0.93 2.41 1. 34 1. 40 1. 02 2.17 1. 27 1. 81 0.90 1. 51 5.16 1. 72 1. 43 0.75 0.75 0.84 1. 59 1. 06 1. 47 1. 28 0.68 92.93 126. 72 149.42 154.20 168.50 173.72 185.71 371. 48 390.02 420 .11 477.45 483.56 590.29 601.04 654.79 677.47 704.28 926. 56 1023.02 1167. 35 1203.24 1218.76 1323.08 1388.89 1454.62 1570.07 1741.13 1751.27 1822.90 1939.87 2055.57 2191.17 2205.10 2240.91 87 119 142 142 164 172 182 366 384 415 469 469 584 596 648 672 699 923 1015 1160 1200 1212 1315 1381 1448 1563 1736 1748 1817 1931 2052 2186 2200 2236 12 2.18E-02 14 2.60E-02 16 6.62E-02 16 8.47E-02 8 9.69E-03 7 1. 7 5E-02 9 2.30E-02 10 2.32E-02 8 5.83E-03 12 l.28E-02 21 1.03E-01 21 3.21E-02 11 3. 32E-02 9 6.32E-03 12 l.59E-02 11 1.81E-02 13 4.57E-02 7 8.26E-03 16 1.04E-02 14 2.39E-02 7 5.73E-03 12 4.25E-02 15 1.58E-02 17 *7.17E-03 13 1.07E-02 13 8. 24E-03 13 4.44E-03 7 2.35E-03 16 1.99E-02 14 7.59E-03 6 2.00E-03 9 2.08E-03 11 5.56E-03 .9 7.83E-03 36.2 42.0 13.0 3.58E+OO 9.1 68.1 35.2 32.5 24.5 75.8 47.9 6.6 3.79E-01 21. 0 14.2 64.4. 26.8 27 ..4 14.0 29.6 47.1 19.8 30.4 10.1 28.0 58.3 28.1 33.3 52.8 56.9 16.9 50.3 52.9 89.1 22.4 26.9 Peak Search Report (continued) Page : 2 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1276.45 13 5 1. 55 2552. 96 2547 *11 3.64E-03 43.9 36 0 1378.17* 14 8 2.49 2756.43 2750 11 3.89E-03 50.0 37 0 1408. 72* 7 3 1. 58 2817.55 2810 11 l.98E-03 63.9 38 0 1461. 03* 271 7 1. 82 2922.19 2915 14 7.52E-02 6.5 39 0 1764.74* 23 0 1. 60 3529.75 3523 12 6.40E-03 21. 9 Flag: "*" = Pea*k area was modified by background subtraction Page 3620 of 5809 VMS Nuclide Identification Report V3.1 Generated 10:12:48 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl . Sample title Sample date Sample ID 23-NOV-2015 11:48:00 G405235032 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:10:21 146.95 GRAM . Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA39 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 *74. 82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3621of5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Inte;r-fered Nuclide Line RA-224 240.99 .SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:07.00 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.983E-01 1.391E+Ol l.391E+Ol 13.08 OK CD-109 88.03 3.70* 6.756E+OO 6.225E-01 9.991E-01 186.05 OK SN-126 64.28 9.60 6.928E+OO 9.148E-01 9.148E-01 84.02 OK 86.94 8.90 6.756E+OO 2.588E-01 2.588E-01 186.05 OK 87.57 37.00* 6.756E+OO 6.225E-02 6.225E-02 186.05 OK BA-137M 661. 66 89.90* 1. 758E+OO 1.909E-01 1.947E-01 56.06 OK CS-137 661. 66 85.10* 1. 758E+OO 2.017E-01 2.057E-01 56.06 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* 1. 951E+OO 2.793E-01 2.793E-01 39.69 OK 860.56 12.50 1.416E+OO Line Not Found Absent PB-210 46.54 4.25* 6.818E+OO 1. 80.9E+OO 1.858E+OO 72.39 OK BI-212 727.33 6.67* 1. 626E+OO 1.877E+OO 1.877E+OO 56.14 OK 785.37 1.10 1.527E+OO 9.243E+OO 9.243E+OO 66.67 OK 1620.50 1. 47 8.143E-01 Line Not Found Absent PB-212 74.82 10.28 6.812E+OO 1.591E+OO 1. 591E+OO 37.30 OK 77 .11 17.10 6.799E+OO 1.682E+OO 1. 682E+OO 18 .11 OK 238.63 43.60* 4.209E+OO 1.185E+OO 1.185E+OO 13.14 OK 300.09 3.30 3.460E+OO l .139E+00 1.139E+OO 128.73 OK BI-214 609.32 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 OK 1120.29 14.92 l.136E+00 8.399E-01 8.402E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9. 711E-01 . 43.82 OK PB-214 74.82 5.80 6.812E+OO Line Not Found <<INT Reject 77 .11 9.70 6.799E+00 2. 965E+OO 2. 967E+OO 18 .11 OK 87.09 3.41 6.755E+OO Line Not Found <<INT Reject 242.00 7.25 4.163E+00 Line Not Found <<INT.Reject 295.22 18.42 3.514E+OO 1.058E+00 l.058E+OO 28.48 OK 351. 93 35.60* 3.012E+OO 8.653E-01 8.656E-01 27.98 OK RN-222 609.32 45.49* 1. 882E+OO 9.574E-01 9.578E-01 20.12 OK 1120.29 14.92 l.136E+OO 8.399E-01 8.402E-01 53. 71 OK 1764.49 15.30 7.484E-01 9.708E-01 9.711E-01 43.82 OK RA-224 240.99 4.10* 4.165E+OO 2.073E+OO 2.073E+OO 84.04 OK RA-22 6' 609.32 45.49* l.882E+OO 9.574E-01 9.578E-01 20.12 OK 1120.29 14.92 l.136E+00 8.399E-01 8.402E-01 53. 71 OK 1764.49 15.30 7.484E-01 9.708E-01 9. 711E-01 43.82 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .116E+OO l.051E+OO 1. 051E+OO 54.90 OK 794.95 4.25 l.512E+OO Line Not Found Absent 835. 71 1. 61 1. 451E+OO Line Not Found Absent 911. 20 25.80* 1. 351E+OO 1.058E+OO l.058E+OO 33.79 OK 968. 97 15.80 l.283E+OO 6. 913E-01 6. 913E-01 100.57 OK RA-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .116E+00 1.051E+OO 1. 051E+OO 54.90 OK 794.95 4.25 1. 512E+OO Line Not Found Absent 835.71 1. 61 1. 451E+OO Line Not Found Absent 911.20 25.80* 1.351E+OO 1.058E+OO 1. 058E.+00 33.79 OK 968. 97 15.80 l.283E+OO 6.913E-01 6.913E-01 100.57 OK TH-228 74.82 10.28 6.812E+OO l.591E+OO 1. 591E+OO 37 .. 30 OK 77 .11 17.10 6.799E+OO l.682E+OO l.682E+OO 18.11 OK 238.63 43.60* 4.209E+OO l.185E+OO l.185E+OO 13.14 OK Page 3622 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3.460E+OO l.139E+OO l.139E+OO 128.73 OK TH-230 609.32 45.49* 1.882E+OO 9.574E-01 9.574E-01 20.12 OK 1120.29 14.92 l.136E+00 8.399E-01 8.399E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 OK PA-231 283.69 1. 70 3.638E+OO Line Not Found Absent 301.36 5.35* 3.460E+OO 7.028E-01 7.028E-01 128.73 OK TH-232 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .116E+OO 1.051E+OO l.051E+OO 54.90 OK 835.71 1.61" i.451E+00 Line Not Found Absent 911. 20 25.80* l.351E+00 1.058E+OO 1.058E+OO 33.79 OK 968.97 15.80 1.283E+OO 6.913E-01 6.913E-01 100.57 OK TH-234 63.29 3.70* 6.928E+OO 2.373E+OO 2.373E+OO 84.02 OK 92.59 4.23 6.722E+OO l.838E+00 1.838E+OO 65.07 OK U-234 609.32 45.49* 1.882E+OO 9.574E-01 9.574E-01 20.12 OK 1120. 29 14.92 1.136E+OO 8.399E-01 8.399E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 OK U-238 63.29 3.70* 6.928E+OO 2.373E+OO 2.373E+00 *84. 02 OK 92. 59 4.23 6. 722E+OO 1.838E+OO 1.838E+OO 65.07 OK AM-243 43.53 5.90 6.236E+00 Line Not Found Absent 74.66 67.20* 6.812E+OO 2.434E-01 2.434E-01 37.30 OK ANH-511 511. 00 100.00* 2.181E+OO 9.366E-02 9.366E-02 94.28 OK Flag: "*"" = Keyline

Page 3623 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:49.55
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l *
Acquisition date 3-0CT-2016 09:10:21 Sensitivity : 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:07.00 Half life ratio : ***** *
Sample date 23-NOV-2015 11:48:00 Analyst initials: MXRl *
Sample ID G405235032 Sample Quantity 1.4695E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
Eff.' File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuciides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.391E+Ol 1. 783E+OO 7.664E-01 CD-109 9.991E-01 1.822E+OO l.959E+OO SN-126 6.225E-02 1.135E-01 l.220E-01 BA-137M 1.947E-01 1.070E-01 8. 901E-02 CS-137 2.057E-01 1.130E-01 9.403E-02 TL-208 2.793E-01 1. 086E-01 7.193E-02 PB-210 1.858E+OO 1.318E+OO 8.477E-01 BI-212 1.877E+OO 1.033E+OO l.120E+00 PB-212 1.185E+OO l.527E-01 9. 966E-02 BI-214 9.578E-01 1.889E-01 1.435E-01 PB-214 8.656E-01 2.374E-01 1. 405E-01 RN-222 9.578E-01 1.889E-01 1.435E-01 RA-224 2.073E+OO 1.707E+OO 1.069E+00 RA-226 9.578E-01 1.889E-01 1.435E-01 AC-228 1.058E+OO 3.503E-01 2.695E-01 RA-228 1.058E+OO 3;503E-01 2.695E-01 TH-228 1.185E+OO 1.527E-01 9. 966E-02 TH-230 9.574E-01 1.888E-01 1.434E-01 PA-231 7.028E-01 8.866E-01 9.121E-01 TH-232 1.058E+OO 3.503E-01 2.695E-01 TH-234 2.373E+00 1.954E+OO 1.lOOE+OO U-234 9.574E-01 l.888E-01 1.434E-01 U-238 2.373E+00 1.954E+OO 1.lOOE+OO AM-243 2.434E-01 8.898E-02 5.812E-02 ANH-511 9.366E-02 8.653E-02 *5. 68 9E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM BE-7 -6.462E+00 1.861E+Ol 3.370E+Ol NOT IDENT. NA-22 -7.868E-03 7.425E-02 1.247E-01 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 3.435E-03 3.741E-02 8.253E-02 NOT IDENT. SC-46 1.055E-01 5.506E-01 1.131E+OO FAIL ABUN Page 3624 of 5809 V-48 O.OOOE+OO 3.276E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.835E+02 O.OOOE+OO SHORT HLIF MN-54 -1.174E-02 8.448E-02 1.652E-Ol NOT IDENT. C0-56 .3. l 79E-03 6.325E-01 l.279E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 -7.879E-02 5.591E-02 8.788E-02 NOT IDENT. C0-58 3.985E-01 7.408E-01 l.630E+OO NOT IDENT. FE-59 6.214E+OO 1. 021E+Ol 1.841E+Ol NOT IDENT. C0-60 6.175E-03 4.475E-02 9.417E-02 NOT IDENT. ZN-65 3.938E-02 2.435E-01 4.421E-Ol NOT IDENT. GE-68 -5.495E-02 3.006E+OO 5.989E+Ob NOT IDENT. AS-73 -2. 061E+OO 3.140E+OO 5.570E+OO NOT IDENT. AS-74 O.OOOE+OO l.278E+04 O.OOOE+OO SHORT HLIF SE-75 -6.568E-02 2.402E-01 4.567E-Ol NOT IDENT. BR-77 O.OOOE+OO 2.221E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l.445E+03 O.OOOE+OO SHORT HLIF RB-83 l.496E-01 8.844E-01 1. 730E+OO NOT IDENT. KR-85 6.786E+OO 8. 496E+OO l.650E+Ol NOT IDENT. SR-85 8.362E-01 l.051E+OO 2.040E+OO NOT IDENT. RB-86 O.OOOE+OO 5.737E+04 0.000E+OO SHORT HLIF Y-88 1. 282E-01 1.653E-01 5.428E-01 NOT IDENT. Y-91 -5.732E+02 8.145E+02 l.406E+03 NOT IDENT. NB-94 -l.139E-02 4.232E-02 7. 572E-02 FAIL ABUN NB-95 2.377E-01 1.270E+OO 2.436E+OO NOT IDENT. NB-95M 3.200E-01 3.371E+OO 5.933E+OO NOT IDENT. ZR-95 1.020E+OO 2 .112E+OO 4.292E+00 NOT IDENT. NB-97 Ci.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1'. 960E+41 O.OOOE+OO SHORT HLIF -M0-99 O.OOOE+OO 1.022E+34 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.577E+41 O.OOOE+OO SHORT HLIF RH-101 -3.871E-02 3.819E-02 6.240E-02 NOT IDENT. RH-102 -6.147E-03 7.564E-02 1.414E-01 NOT IDENT. RU-103 -5.187E+OO 8.262E+OO l.445E+Ol FAIL ABUN RH-106 5.840E-01 5.986E-01 l.305E+OO NOT IDENT. RU-106 5.840E-01 5.986E-01 l.305E+OO NOT IDENT. AG-108M -9.803E-03 3.lOlE-02 5.742E-02 NOT IDENT. AG-llOM 8.754E-03 l.377E-01 2.771E-01 NOT IDENT. SN-113 -3.520E-01 3.081E-01 5. lllE-01 NOT IDENT. CD-115 O.OOOE+OO l.538E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2.127E+05 O.OOOE+OO SHORT HLIF TE-123M -4.061E-02 l.430E-01 2. 772E-01 NOT IDENT. SB-124 9.029E-01 2.943E+OO 6.773E+OO NOT IDENT. SB-125 -8.656E-02 1.246E-01 2.182E-01 FAIL ABUN TE-125M -2.878E+02 3.106E+02 5.160E+02 NOT IDENT. I-126 O.OOOE+OO 3.079E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.433E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4 .114E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.263E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O,OOOE+OO l .110E+28 O.OOOE+OO SHORT HLIF BA-133 -l.616E-02 5.183E-02 8.539E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 3.412E-04 6.250E-02 1. 251E-01 NOT IDENT. CS-135 -5.162E-02 1.712E-01 3.214E-01 NOT IDENT. I-135 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 8.142E+05 O.OOOE+OO SHORT HLIF CE-139 -l.305E-01 l.262E-01 2.299E-01 NOT IDENT. BA-140 O.OOOE+OO 3.535E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1. 380E+06 O.OOOE+OO SHORT HLIF CE-141 -2.275E+Ol 3.372E+Ol 6.394E+Ol NOT IDENT. CE-143 O.OOOE+OO l.100E+41 O.OOOE+OO SHORT HLIF CE-144 -6.124E-02 3.475E-01 6.852E-01 NOT IDENT. PM-144 7.378E-02 7.863E-02 l.639E-01 NOT IDENT. PR-144 6.445E+OO 6.882E+OO 1.434E+Ol NOT IDENT. PM-146 -4.878E-03 5.283E-02 9.995E-02 NOT IDENT. ND-147 O.OOOE+OO l.137E+08 O.OOOE+OO SHORT HLIF PM-147 -4. 251E+02 8.860E+02 l.531E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 4.225E-03 3.281E-02 5.755E-02 FAIL ABUN EU-152 4.650E-02 l .115E-01 2.152E-01 FAIL ABUN GD-153 -l.553E-01 l.940E-01 2.981E-01 NOT IDENT. EU-154 -3.456E-02 l.781E-01 2.931E-01 NOT IDENT. EU-155 6.434E-02 l.064E-01 2.031E-01 FAIL ABUN TB-160 4.028E-01 2. 971E+OO 5.426E+OO FAIL ABUN H0-166M 2.250E-02 6.452E-02* l.299E-01 FAIL ABUN TM-171 3.074E+OO 5. 872E+OO 1.137E+Ol NOT IDENT. HF-172 -3.020E-01 2.639E-01 4.258E-01 FAIL ABUN LU-172 5.645E-02 9.457E-02 l.930E-01 FAIL ABUN Page 3625 of 5809 LU-176 1.0SOE-02 2.740E-02 5. 351E-02 FAIL ABUN HF-181 5.006E+OO 6.683E+OO 1.395E+Ol NOT IDENT. TA-182 -4.823E-01 1.278E+OO 2.355E+00 FAIL ABUN RE-183 4.347E-01 1.419E+OO 2.509E+OO NOT IDENT. RE-184 3.156E+Ol 4.974E+Ol 1.085E+02 NOT IDENT. W-188 -4.407E+Ol l.548E+02 2. 596E+02 FAIL ABUN IR-192 l.918E-01 5.619E-01 1.134E+OO FAIL ABUN HG-203 1.718E+OO 3. 5.12E+OO 7.062E+OO NOT IDENT. BI-207 9.375E-03 6.418E-02 1.294E-01 FAIL ABUN BI-211 O.OOOE+OO 6.539E-01 8.785E-01 FAIL ABUN PB-211 6.792E-01 8.782E-01 1.794E+OO NOT IDENT. RN-219 -8.680E-02 5.175E-01 9.636E-01 NOT IDENT. RA-223 -4.522E-01 7.949E-01 1.265E+OO FAIL ABUN AC-227 2. 963E-02 2.816E-01 FAIL ABUN TH-227 2. 963E-02 2.816E-01 5.478E-01 FAIL ABUN TH-229 l .113E-01 4.786E-01 9.562E-01 FAIL ABUN TH-231 -4.522E-01 7.949E-01 1.265E+OO FAIL ABUN PA-233 -1.112E-02 6.766E-02 1.287E-01 FAIL ABUN PA-234 -7.373E-02 3.457E-01 6.699E-01 NOT IDENT. PA-234M 1. 24 7E+OO 4.672E+OO 9.997E+OO NOT IDENT. U-235 -3.449E-03 1. 8'67E-01 3. 696E-01 FAIL ABUN NP-237 -l .112E-02 6.766E-02 l.287E-01 FAIL ABUN NP-238 O.OOOE+OO 1.535E+41 *o.OOOE+OO SHORT HLI'F NP-239 9 .117E-03 2.591E-01 4.694E-01 NOT IDENT. PU-239 5.093E+02 3. 321E+02 6. 720E+02 NOT IDENT. AM-241 -l.444E-02 6.603E-02 l.108E-01 NOT IDENT. CM-243 -3.460E-03 9.758E-02 1. 769E-01 NOT IDENT. BK-247 -5.904E-02 7. 8'2 7E.:._02 1.414E-01 FAIL ABUN CM-247 -l.206E-02 4.764E-02 8.791E-02 NOT IDENT. CF-249 -2.708E-03 4.882E-02 9.238E-02 NOT IDENT. CF-251 -4.573E-02 l.222E-01 2.336E-01 NOT IDENT. Page 3626 of 5809 VAX/VMS Nuclide Report Generated 3'-0CT-2016 10:.12:47.43 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 261 10.66* 8.983E-01 1.391E+Ol 1.391E+Ol 13. 08 CD-109 88.03 78 3.70* 6.756E+OO 1.597E+OO 2.563E+OO 70.40 SN-126 64.28 119 9.60 6.928E+OO 9.148E-01 9.148E-01 84.02 86.94 78 8.90 6.756E+OO 6.640E-01 6.640E-01 70.40 87.57 78 37.00* 6.756E+OO 1.597E-01 1.597E-01 70.40 BA-137M 661. 66 59 89.90* 1. 758E+OO 1.909E-01 1.947E-01 56.06 CS-137 661.66 59 85.10* 1. 758E+OO 2.017E-01 2.057E-01 56.06 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 91 85.00* 1. 951E+OO 2.793E-01 2.793E-01 39.69 860.56 ------12.50 1.416E+OO ------Line Not Found ------PB-210 46.54 103 4.25* 6.818E+OO 1.809E+OO 1.858E+00 72.39 BI-211 72.87 ------1. 23 6.824E+OO ------Line Not Found ------351.06 182 12.92* 3.012E+OO 2.384E+OO 2.384E+OO 27.98 BI-212 727. 33 40 6.67* 1.626E+OO 1.877E+OO 1.877E+OO 56 .. 14 785.37 30 1.10 1.527E+OO 9.243E+OO 9.243E+OO 66.67 1620:50 ------1. 47 8.143E-01 ------Lirie Not Found ------PB-212 74.82 300 10.28 6.812E+OO 2.188E+OO 2.188E+OO 25.99 77 .11 383 17.10 6.799E+OO 1.682E+OO 1.682E+OO 18 .11 238.63 426 43.60* 4.209E+OO 1.185E+OO 1.185E+OO 13.14 300.09 25 3.30 3.460E+OO 1.139E+OO 1.139E+OO 128.73 .BI-214 609.32 160 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 1120.29 28 14.92 1.136E+OO 8.399E-01 8.402E-01 53. 71 1764.49 22 15.30 7.484E-01 9.708E-01 9. 711E'-01 43.82 PB-214 74.82 300 5.80 6.812E+OO 3.877E+OO 3.879E+OO 25.99 77 .11 383 9.70 6.799E+OO 2. 965E+OO 2. 967E+OO 18 .11 87.09 78 3.41 6.756E+OO 1.733E+OO 1.734E+00 70.40 242.00 132 7.25 4.165E+OO 2.230E+OO 2. 231E+OO 42.07 295.22 134 18.42 3.514E+OO 1.058E+OO 1.058E+OO 28.48 351.93 182 35.60* 3.012E+OO 8.653E-01 8.656E-01 27.98 RN-222 609.32 160 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 1120.29 28 14.92 1.136E+OO 8.399E-01 8.402E-01 53. 71 1764.49 22 15.30 7.484E-01 9.708E-01 9.711E-01 43.82 RA-224 240.99 132 4.10* 4.165E+OO 3.943E+OO 3.943E+OO 42.07 RA-226 609.32 16.0 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 1120.29 28 14.92 1.136E+OO 8.399E-01 8.402E-01 53. 71 1764.49 22 15.30 7.484E-01 9.708E-01 9.711E-01 43.82 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 72 11. 27 3 .116E+OO 1.051E+OO 1. 051E+OO 54.90 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1.451E+OO ------Line Not Found ------911. 20 72 25.80* 1. 351E+OO l.058E+OO l.058E+OO 33.79 968. 97 27 15.80 1.283E+00 6.913E-01 6.913E-01 1_00. 57 RA-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 72 11. 27 3 .116E+OO 1. 051E+OO 1.051E+OO 54.90 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 72 25.80* 1.351E+OO 1.058E+OO 1.058E+OO 33.79 Page 3627 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968.97 27 15.80 1.283E+OO 6.913E-01 6.913E-01 100.57 TH-228 74.82 300 10.28 6. 812E+O.O 2.188E+OO 2.188E+OO 25.99 77 .11 383 17.10 6.799E+OO 1.682E+OO l.682E+OO 18 .11 238.63 426 43.60* 4.209E+OO 1.185E+OO 1.185E+OO 13.14 300.09 25 3.30 3.460E+OO 1.139E+OO 1.139E+OO 128.73 TH-230 609.32 160 45.49* 1. 882E+OO 9.574E-01 9.574E-01 20.12 1120.29 28 14.92 1.136E+OO 8.399E-01 8.399E-01 53.71 1764.49 22 *15. 30 7.484E-01 9.708E-01 9.708E-01 43.82 PA-231 283.69 ------1. 70 3.638E+OO ------Line Not Found ------301.36 25 5.35* 3.460E+OO 7.028E-01 7.028E-01 128.73 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 72 11. 27 3 .116E+OO 1. 051E+OO 1. 051E+OO 54.90 835.71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 72 25.80* 1.351E+OO 1.058E+OO 1.058E+OO 33.79 968. 97 27 15.80 1.283E+OO 6.913E-01 6. 9.13E-01 100.57 TH-234 63.29 119 3.70* 6.928E+OO 2.373E+OO 2.373E+OO 84.02 92.59 102 4.23 6. 722E+OO 1.838E+OO 1.838E+OO 65.07 U-234 609.32 160 45.49* 1.882E+OO 9.574E-01 9.574E-01 20.12 1120.29 28 14.92 1.136E+OO 8.399E-01 8.399E-01 53. 71 1764.49 22 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 U-238 63. 29 119 3.70* 6.928E+00 2.373E+OO 2.373E+OO 84.02 92.59 102 4.23 6. 722E+OO 1.838E+OO 1.838E+OO 65.07 AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 300 67.20* 6.812E+OO 3.347E-01 3.347E-01 25.99 ANH-511 511. 00 40 100. 00* 2.181E+OO 9.366E-02 9.366E-02 94.28 Flag: "*" Key line Page 3628 of 5809 Summary of Nuclide Activity Sample ID : 8405235032 Acquisition date Page : 3 3-0CT-2016 09:10:21 Total number of lines in spectrum 39 Number of unidentified lines 5 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-22 6 . AC-228 RA-228 TH-228 TH-230* PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 22.20Y 7.04E+08Y l.41E+l0Y 1.41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+10Y 1.41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 60 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.391E+Ol l.597E+OO l.597E-01 l.909E-01 2.017E-01 2.793E-01 1. 809E+OO 2.384E+OO 1.877E+OO 1.185E+OO 9.574E-01 8. 653E-01
9.574E-01 3.943E+OO 9.574E-01 1.058E+OO 1.058E+OO 1.185E+OO 9.574E-01 7.028E-01 1.058E+OO 2.373E+OO 9.574E-01 2.373E+OO 3.347E-01 9.366E-02 4.343E+Ol 4.343E+Ol Decay Corr pCi/GRAM 1. 391E+Ol 2.563E+OO l.597E-01 1. 947E-01 2.057E-01 2.793E-01 l.858E+OO. 2.384E+OO 1.877E+OO 1.185E+OO 9.578E-01 8.656E-01 9.578E-01 3.943E+OO 9.578E-01 1.058E+OO 1.058E+OO 1.185E+OO 9.574E-01 7.028E-01 l.058E+OO 2.373E+OO 9.574E-01 2.373E+OO 3.347E-01 9.366E-02 4.445E+Ol 4.445E+Ol 87.18% Decay Corr 2-Sigma Error 0.182E+Ol 1.805E+OO l.124E-01 1.092E-01 l.153E-01 1.109E-01 l.345E+OO 0.667E+OO l.054E+OO 0.156E+OO 1.927E-01 2.422E-01 1.927E-01 1.659E+OO 1.927E-01 0.357E+OO 0.357E+OO 0.156E+OO 1.927E-01 9.047E-01 0.357E+OO 1.994E+OO 1.927E-01 1.994E+OO 0.870E-01 8.830E-02 "M" Manually 2-Sigma %Error 13.08 70.40 70.40 56.06 56.06 39.69 72.39 27.98 56.14 13 .14 20.12 27.98 20.12 42.07 20.12 33. 7.9 33.79 13.14 20.12 128.73 33.79 84.02 20.12 84.02 25.99 94.28 Flags: ."K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3629 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235032 Acquisition date : 3-0CT-2016 09:10:21 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err. %Eff Flags 0 84.33 43 209 1. 03 168.50 164 8 9.69E-03 **** 6.77E+OO T 0 185.82 97 96 1. 33 371.48 366 10 2.32E-0.2 49.0 5. llE+OO T 0 195.09 24 88 0.52 390.02 384 8 5.83E-03 **** 4.93E+OO 0 210.13 53 126 2.74 420 .11 415 12 1.28E-02 95.9 4.66E+OO T 0 327.47 64 50 2.41 654.79 648 12 1.59E-02 53.6 3.21E+OO T 0 463.35 32 19 1. 02 926.56 923 7 8.26E-03 59.2 2.37E+OO T 0 601.68 22 7 1. 81 1203.24 1200 7 5.73E-03 60.8 1. 90E+OO T 0 694.50 27 40 5.16 1388.89 1381 17 7.17E-03 **** 1.69E+OO T 0 870.59 16 13 0.75 1741.13 1736 13 4.44E-03 **** 1.40E+OO T 0 875.67 9 6 0.75 1751.27 1748 7 2.35E-03 **** 1.40E+OO T 0 1027.79 7 3 1. 06 2055.57 2052 6 2.00E-03 **** l.22E+OO T 0 1095.58 7 11 1. 47 2191.17 2186 9 2.08E-03 **** 1.16E+OO 0 1102. 55 20 0 1. 28 2205.10 2200 11 5.56E-03 44.7 1.15E+OO 0 . 1276.45 13 5 1. 55 2552. 96 2547 11 3.64E-03 87.8 1. OlE+OO 0 1378.17 14 8 2.49 2756.43 2750 11 3.89E-03 **** 9.48E-01 0 1408. 72 7 3 1. 58 2817.55 2810 11 1. 98E-03 **** 9.29E-01 T Flags: "Tn = Tentatively associated Page 3630 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:13:01.06 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l * *Acquisition date 3-0CT-2016 09:10:21 Sensitivity 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:07.00 Half life ratio : ***** *
Sample date 23-NOV-2015 11:48:00 Nuclide Library : SOLID *
Sample ID G405235032 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.4695E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
Eff. File : DKAIOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.107E-01 9.323E-01 5.806E-02 3.995E-02 4.220E-02 3.169E-02 3.974E-01 4.950E-01 4.590E-02 6.348E-02 6.355E-02 6.348E-02 4.924E-01 6.348E-02 l.146E-01 l.146E-01 4.590E-02 6.346E-02 4 .171E-01 1.146E-01 5.213E-01 6.346E-02 5.213E-01 2.745E-02 2.519E.:..02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3631 of 5809 Le (pCi/GRAM 1.507E+Ol 5. 372E-02 O.OOOE+OO 3.177E-02 4. 966E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3632 of 5809 O.OOOE+OO 7.287E-02 5.566E-01 O.OOOE+OO 4.094E-02 7.117E-01 7.757E+OO 3.910E-02 l.914E-01 2.581E+OO 2.631E+OO O.OOOE+OO 2.087E-01 O.OOOE+OO O.OOOE+OO 7.729E-01 7. 451E+OO 9.215E-01 O.OOOE+OO 1. 963E-01 5.984E+02 3.364E-02 1.081E+OO 2.760E+OO 1. 897E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.915E-02 6.258E-02 6.318E+OO 5.832E-01 5.832E-01 2.557E-02 1.218E-01 2.288E-01 O.OOOE+OO O.OOOE+OO l.290E-01 2.687E+00 9.742E-02 2.394E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.860E-02 O.OOOE+OO 5.528E-02 1. 489E-01 O.OOOE+OO O.OOOE+OO 1.069E-01 O.OOOE+OO O.OOOE+OO 2.987E+Ol O.OOOE+OO 3.196E-01 7.426E-02 6.498E+OO 4.492E-02 O.OOOE+OO 7.149E+02 O.OOOE+OO 2.637E-02 9.847E-02 l.397E-01 l.256E-01 9.561E-02 2.370E+00 5.707E-02 5.381E+00 1.988E-01 8.332E-02 2.450E-02 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SH,ORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA'-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 . CF-251 Page 3633 of 5809 6. 313E+OO 1.013E+00 1.185E+OO 4.783E+Ol 1.183E+02 5.164E-01 3. 272E+OO 5.667E-02 4.211E-01 8.262E-01 4.415E-01 5. 771E-01 2.548E-01 2.548E-01 4.450E-01 5. 771E-01 5.881E-02 2.903E-01 4.331E+OO 1. 737E-01 5.881E-02 O.OOOE+OO 2.204E-01 3.175E+02 5.245E-02 8.307E-02 6.448E-02 4.026E-02 4.228E-02 1. 088E-01 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:13:06.62 *******************************************************************************

GEL Laboratories LLC * ** 2040 Savage Road. *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l *
Acquisition date 3-0CT-2016 09:10:21 Sensitivity : 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:07.00 Half life ratio : ***** *
Sample date 23-NOV-2015 11:48:00 Nuclide. Library : SOLID *
Sample ID G405235032 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity l.469SE+02 GRAM *
Quantity Err(%) 1.3610E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************** * *
CALIBRATION INFORMATION * * *
Eff. date 27-JUL-2016 13:04:01 Eff. Geometiy : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Activity-MDA Report NOTE: Ncit all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.391E+Ol 1.925E+OO 1.925E+OO CD-109 9. 991E""""'.01 1.834E+OO 1.834E+OO SN-126 6.225E-02 1.142E-01 1.142E-01 BA-137M 1. 94 7E-01 l.073E-01 l.073E-01 CS-137 2.057E-01 1.134E-01 l .134E-01 TL-208 2.793E-01 1.093E-01 l.093E-01 PB-210 l.858E+OO 1.328E+OO 1.328E+OO BI-212 1.877E+OO 1.037E+OO 1.037E+OO PB-212 1.185E+OO 1. 651E-01 l.651E-01 BI-214 9.578E-01 1.933E-01 1.933E-01 PB-214 8.656E-01 2. 401E-01 2.401E-01 RN-222 9.578E-01 1.933E-01 1.933E-01 RA-224 2.073E+OO 1. 715E+OO 1. 715E+OO RA..::22 6 9.578E-01 l.933E-01 l.933E-01 AC-228 1.058E+OO 3. 544E-.Ol 3.544E-01 RA-228 1.058E+OO 3.544E-01 3.544E-01 TH-228 1.185E+OO 1. 651E-01 l.651E-01 TH-230 9.574E-01 1.933E-01 1.933E-01 PA-231 7.028E-01 8.992E-01 8.992E-01 TH-232 1.058E+OO 3.544E-01 3.544E-01 TH-234 2.373E+OO 2.024E+OO 2.024E+OO U-234 9.574E-01 l.933E-01 1.933E-01 U-238 2.373E+OO 2.024E+OO 2.024E+00 AM-243 2.434E-01 9. 096E-02 9. 096E-02 ANH-511 9.366E-02 8.662E-02 8. 6.62E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma) BE-7 -6.462E+OO 1. 861E+Ol l.884E+Ol NOT IDENT. NA-22 -7.868E-03 7.425E-02 7.433E-02 NOT IDENT. NA-24 -l.OOOE+41 4.673E+41 0.000E+OO SHORT HLIF AL-26 3.435E-03 3.741E-02 3.744E-02 NOT IDENT. SC-46 1.055E-01 5.507E-01 5.527E-01 FAIL ABUN Page 3634 of 5809 V-48 -4.997E+02 3.276E+04 3.276E+04 SHORT HLIF CR-51 9.148E+Ol 6.835E+02 6.848E+02 SHORT HLIF MN-54 -1.174E-02 8.448E-02 8.464E-02 NOT IDENT. C0-56 3.179E-03 6.325E-01 6.325E-01 NOT IDENT. MN-56 -1.000E+41 3.858E+43 O.OOOE+OO SHORT HLIF C0-57 -7.879E-02 5.602E-02 6.633E-02 NOT IDENT. C0-58 3.985E-01 7.410E-01 7.624E-01 NOT IDENT. FE-59 6.214E+OO 1.022E+Ol 1.060E+Ol NOT IDENT. C0-60 6.175E-03 4.475E-02 4.483E-02 NOT IDENT. ZN-65 3.938E-02 2.435E-01 2.441E-01 NOT IDENT. GE-68 -5.495E-02 3.006E+OO 3.006E+OO NOT IDENT. AS-73 -2.061E+OO 3.169E+OO 3.302E+OO NOT IDENT. AS-74 -l.214E+03 1.278E+04 1.279E+04 SHORT HLIF SE-75 -6.568E-02 2.402E-01 2.420E-01 NOT IDENT. BR-77 1.724E+40 l.567E+41 O.OOOE+OO SHORT HLIF SR-82 8.449E+02 l.445E+03 l.494E+03 SHORT HLIF RB-83 1. 496E-01 8.846E-01 8 ;872E-01 NOT IDENT. KR-85 6.786E+OO 8. 501E+OO 9.034E+OO NOT IDENT. SR-85 8.362E-01 1.052E+OO 1.117E+OO NOT IDENT. RB-86 -7.807E+03 5.738E+04 5.748E+04 SHORT HLIF Y-88 1. 282E-01 l.655E-01 l.753E-01 NOT IDENT. Y-91 -5.732E+02 8.147E+02 8.547E+02 NOT IDENT. NB-94 -1.139E-02 4.232E-02 4.263E-02 FAIL ABUN NB-95 2.377E-01 l.270E+OO 1. 274E+OO NOT IDENT. NB-95M 3.200E-01 3.371E+OO 3.374E+OO NOT IDENT. ZR-95 l.020E+OO 2 .112E+OO 2.162E+OO NOT IDENT. NB-97 l.000E+41 1.625E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 7.286E+41 O.OOOE+OO SHORT HLIF M0-99 -6.571E+32 l.022E+34 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 1.580E+41 O.OOOE+OO SHORT HLIF RH-101 -3.871E-02 3.883E-02 4.257E-02 NOT IDENT. RH-102 -6.147E-03 7.564E-02 7.569E-02 NOT IDENT. RU-103 -5.187E+OO 8.266E+OO 8. 591E+OO FAIL ABUN RH-106 5.840E-01 5.997E-01 6.549E-01 NOT I DENT.* RU-106 5.840E-01 5.997E-01 6.549E-01 NOT IDENT. AG-108M -9.803E-03 3.102E-02 3.133E-02 NOT IDENT. AG-llOM 8.754E-03 l.377E-01 l.378E-01 NOT IDENT. SN-113 -:-3.520E-01 3.084E-01 3.468E-01 NOT IDENT. CD-115 -1.000E+41 1. 549E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -9.578E+04 2 .130E+05 2.173E+05 SHORT HLIF TE-123M -4.061E-02 l.430E-01 l.442E-01 NOT IDENT. SB-124 9.029E-01 2.944E+OO 2.972E+OO NOT IDENT. SB-125 -8.656E-02 l.246E-01 1. 306E-01 FAIL ABUN TE-125M -2.878E+02 3 .111E+02 3.371E+02 NOT IDENT. I-126 -8.599E+05 3.082E+06 3.106E+06 SHORT HLIF SB-126 -l.382E+06 3.444E+06 3.499E+06 SHORT HLIF SB-127 -2.333E+23 5.316E+23 O.OOOE+OO SHORT HLIF I-131 -2.147E+09 2.263E+l0 2.265E+10 SHORT HLIF I-132 1.000E+41 5.818E+42 O.OOOE+OO SHORT HLIF TE-132 -7.447E+27 l.154E+28 .. O.OOOE+OO SHORT HLIF BA-133 -l.616E-02 5.183E-02 5.234E-02 NOT IDENT. I-133 -l.000E+41 3.252E+41 *o. OOOE+OO SHORT HLIF CS-134 3.412E-04 6.250E-02 6.250E-02 NOT IDENT. CS-135 -5.162E-02 1. 712E-01 1. 728E-01 NOT IDENT. I-135 -l.000E+41 1. 021E+42 O.OOOE+OO SHORT HLIF CS-136 -l.013E+05 8.143E+05 8.155E+05 SHORT HLIF CE-139 -l.305E-01 l.289E-01 1.417E-01 NOT IDENT. BA-140 -1.522E+05 3.535E+06 3.536E+06 SHORT HLIF LA-140. -l.806E+06 1.383E+06 l.605E+06 SHORT HLIF CE-141 -2.275E+Ol 3.374E+Ol 3.526E+Ol NOT IDENT. CE-143 1.000E+41 1.105E+41 O.OOOE+OO SHORT HLIF CE-144 -6.124E-02 3.476E-01 3.487E-01 NOT IDENT. PM-144 7.378E-02 7.877E-02 8.550E-02 NOT IDENT. PR-144 6.445E+OO 6.888E+OO 7.476E+OO NOT IDENT. PM-146 -4.878E-03 5.283E-02 5.287E-02 NOT IDENT. ND-147 -6.719E+07 1.137E+08 l.177E+08 SHORT HLIF PM-147 -4.251E+02 8.862E+02 9.067E+02 NOT IDENT. PM-149 l.000E+41 4.643E+41 O.OOOE+OO SHORT HLIF EU-150 4.225E-03 3.281E-02 3.287E-02 FAIL ABUN EU-152 4.650E-02 l .115E-01 1.135E-01 FAIL ABUN GD-153 -l.553E-01 l.942E-01 2.064E-01 NOT IDENT. EU-154 -3.456E-02 1.781E-01 1. 788E-01 NOT IDENT. EU-155 6.434E-02 l.065E-01 l.104E-01 FAIL ABUN TB-160 4.028E-01 2.972E+OO 2.977E+OO FAIL ABUN H0-166M 2.250E-02 6.453E-02 6.532E-02 FAIL ABUN TM-171 3.074E+OO 5.878E+OO 6.039E+OO NOT IDENT. HF-172 -3.020E-Ol 2.685E-01 3.0lOE-01 FAIL ABUN LU-172 5.645E-02 9.475E-02 9.BlOE-02 FAIL ABUN Page 3635 of 5809 LU-176 1.050E-02 2.740E-02 2.780E-02 FAIL ABUN HF-181 5.006E+OO 6.686E+OO 7.057E+OO NOT IDENT. TA-182 -4.823E-01 1.278E+OO 1.296E+OO FAIL ABUN RE-183 4.347E-01 1. 420E+OO 1.434E+OO NOT IDENT. RE-184 3.156E+Ol 5.036E+Ol 5.233E+Ol NOT IDENT. W-188 -4.407E+Ol 1.549E+02 1.562E+02 FAIL ABUN IR-192 l.918E-01 5.620E-01 5.686E-01 FAIL ABUN HG-203 1.718E+OO 3.513E+OO 3.597E+OO NOT IDENT. BI-207 9.375E-03 6.418E-02 6.432E-02 FAIL ABUN BI-211 2.384E+OO 6.625E-01 1.263E+OO FAIL.ABUN PB-211 6.792E-01 8.789E-01 9.307E-Ol NOT IDENT. RN-219 -8.680E-02 5.176E-01 5.190E-01 NOT IDENT. RA-223 --:4.522E-01 7.953E-01 8.210E-01 FAIL ABUN AC-227 2. 963E-02 2.817E-01 2.820E-01 FAIL ABUN TH-227 2. 963E-02 2.817E-01 2.820E-01 FAIL ABUN TH-229 l .113E-01 4.786E-01 4.812E-01 FAIL ABUN TH-231 -4.522E-01 7.953E-01 8:210E-01 FAIL ABUN PA-233 -1.112E-02 6.766E-02 6.785E-02 FAIL ABUN PA-234 -7.373E-02 3.558E-01 3.574E-01 NOT IDENT. PA-234M 1.247E+OO 4.672E+OO 4.706E+OO NOT IDENT. U-235. -3.449E-03 1. 8 67E-0.1 1.867E-01 FAIL ABUN NP-237 -1.112E-02 6.766E-02 6.785E-02 FAIL ABUN NP-238 -l.000E+41 1.536E+41 O.OOOE+OO SHORT HLIF NP-239 9. ll 7E-03 2. 591E-01 2.591E-01 NOT IDENT. PU-239 5.093E+02 3.328E+02 4.044E+02 NOT IDENT. AM-241 -1.444E-02 6.604E-02 6.636E-02 NOT IDENT. CM-243 -3.460E-03 9.759E-02 9.760E-02 NOT IDENT. BK-247 -5.904E-02 7. 91 7E-'02 8.352E-02 FAIL ABUN CM-247 .-1.206E-02 4.768E-02 4.799E-02 NOT IDENT. CF-249 -2.708E-03 4.882E-02 4.883E-02 NOT IDENT. CF-251 -4.573E-02 1.223E-01 1.240E-01 NOT IDENT. Page 3636 of 5809
- - - - '
GEL LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 96.7190 87.09 129.2920 136.47 64.3860 45.60 75.0593 87.57 129 .. 3771 140.51 0.0000 46.54 75.2030 88.03 129.4596 143.76 69.0807 49.72 0.0000 88.34 140.5708 144.24 73.3284 51. 35 90.8022 88.47 140.5953 145.44 70.8853 51. 87 83.8145 89. 96 135.3411 152.43 59. 4.791 52.39 78.3038 1093.63 102.1932 153.25 0.0000 52.97 91. 8274 91.11 0.0000 323.87 83.4133 53.44 105.3581 92.59 106.0352 156.02 0.0000 54.07 96.5040 93.35 106.1418 158.56 0.0000 57.36 0.0000 94.56 82.8195 159.00 66.6940 57.53 111. 4159 94.65 84.4218 162.33 61.7563 57.98 87.3956 94.67 84.4245 162.66 0.0000 59.27 111. 7584 94.87 84*. 4466 163.33 49.7942 59.32 111. 7 682 97.43 97.5172 165.86 81. 7508 59.54 111.8111 98.43 90.0393 176.31 68.6243 60.96 107.9212 98.44 90.0404 176.60 0.0000 61.17 107. 9600 99.53 72.1326 177.52 70.4366 62.93 108.2840 100 .11 62.5609 181.07 0.0000 63.29 108.3500 102.03 92.8627 181. 52 70.6822 63.58 108.4027 103.18 79.7109 184.41 55.9870 64.28 108.5297 103.37 79.7300 143.76 56.0495 66.73 116. 2327 105.21 70.2251 193.51 55.5364 67.24 120.9213 105.31 70.2339 197.03 68.9594 125.81 114.8804 106.12 71.5155 198.01 53.0884 67.75 94.9785 106.47 71.5461 201.83 71. 8918 69.67 102.9543 109.28 77.8740 203.43 62.2092 70.83 110.8396 111. 00 52.4289 205.31 64.0825 72. 81 96.1264 111.76 0.0000 210.85 49.1668 72.87 96 .1353 114. 06 67.3025 215.65 52.4913 74.66 96. 3994 116.30 0.0000 222 .11 57.7109 74.82 96.4228 116.74 78.5596 227.09 53.4015 74.97 96. 4443 119.76 72. 6719 227.38 57.0341 77 .11 96. 7552 121.12 78.9517 228.16 0.0000 78.74 105.9484 121. 22 78.9604 228.18 60.6918 79.69 102.9753 121.78 99.9974 116.74 60.6918 80.12 74.9380 122.06 100.0289 235.69 57.3847 80.19 0.0000 122.92 55.6248 235. 96 45.5521 80.57 117.1677 123.07 54.3978 238.63 45.6406 81. 00 103.1720 265.00 76.7034 238.98 0.0000 81. 07 106.3088 125.81 96.7246 240.99 4:\.7179 81.75 100.1536 127.23 94.3906 242.00 45.7509 83.79 100.4456 127.91 88.2462 244.70 30.2537 84.00 100.4753 129.30 58.5042 252.40 0.0000 85.43 94.3854 131.20 88.5593 252.80 47.9444 86.55 94.5331. 133.02 73.7347 254.15 0.0000 86.79 94.5642 133.52 68.3550 256.23 57.3000 86.94 108.7720 136.00 62.6831 260.90 0.0000 Page 3637of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 42.7572 355.39 0.0000 584.27 18.5356 264.80 47.4099 356.01 35.3672 595.83 0.0000 265.00 49.2756 364.49 0.0000 427.87 23.0405 2 68. 22 59,6302 366.42 0.0000 602.52 0.0000 269.46 49.4222 372.51 36.6748 604.72 6.5933 270.03 46.6420 375.05 30.7692 607 .14 ' 16.4978 271.23 44.8125 377.52 29.8151 609.32 19.8135 273.65 0.0000 356.01 25.9259 610.33 28.0805 276.40 54.3325 388.16 39.9748 614.28 21. 5051 277.37 61.8656 388.63 0.0000 618.01 23.1909 277.60 55.3125 391.69 43.0516 620.36 27.6326 278.00 43.1362 264.66 32.1849 621.93 12.1655 279.20 44.1084 401.81 43.2738 630.19 0.0000 279.54 60.0755 402.40 44.2936 631. 2 9 21. 0851 279.70 60.0820 .404.85 32.2533 633.25 21.1005 280.46 53.5372 410.95 16.1758 634.78 0.0000 283.69 50.8250 413. 71 27.3340 635.95 17.7858 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 45.2275 423. 72 0.0000 645.85 24.5432 285.90 0.0000 427.09 30.5701 657.76. 21.8470 287.50 39.6271 427.87 33.6398 657.90 0.0000 290.67 41.1246 43.3. 94 26.5813 661. 66 25.8039 293.27 o. *oooo 439.40 21.5255 664.57 0.0000 351.93 31. 2873 453.88 27.8635 666.33' '0.0000 295. 96 31. 3021 463.37 25.9125 666.50 0.0000 879.38 28.5028 468.07 20.7743 667. 71 0.0000 299.98 38.5117 473.00 0.0000 677.62 21.4353 300.09 38.5142 475.06 29.1758 685.70 0.0000 300.13 38.5150 476.78 31. 2836 695.00 0.0000 301.36 38.5447 477.60 27.1225 696.49 18.1680 302.85 34.2935 482.18 19.8609 696. 51 18.1680 256.23 44.3402 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 27.2598 306.78 31.5109 497.08 24.1993 697.49 27.2607 308.46 33.4548 505.52 17.4238 702.65 25.0329 311. 90 40.2295 507.63 0.0000 706.68 20.5093 316.51 29.7752 511. 00 20.1106 711. 68 13. 6958 319.41 '0.0000 514.00 17.4869 720.70 0.0000 320.08 0.0000 514.00 17.4869 721. 93 0.0000 321.04 23.1138 520.40 21.2533 722.78 15.4649 323.87 47.7517 520.69 0.0000 722.91 15.4655 325.23 39.1001 522.65 0.0000 723. 31 15.4677 328.76 0.0000 527.90 0.0000 724 .19 10.3147 333.37 32.0104 528.26 24.5217 727. 33 19.5034 333.97 37.8431 529.59 18.1351 733.00 15.5165 334.37 37.8519 529.87 0.0000 735.93 13.8062 338.28 35.9913 531. 02 0.0000 333.97 17.2662 338.32 35.9920 537.26 0.0000 739.50 0.0000 311. 90 42.3663 546.56 0.0000 747.24 12.7017 340.48 42.3663 552.55 23.6892 748.06 11. 5503 340.55 0.0000 563.25 27.0355 752.31 16.1926 344.28 31.6235 569.33 28.1847 753.82 0.0000 345.93 42.0088 946.00 27.1016 756.73 13.8989 351.06 30.3718 569.70 27.1037 756.80 13.8994 351. 93 30.3863 583.19 18.5280 884.68 16.2524 Page 3638 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:15:51.19 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407
Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 23-NOV-2015 11:53:00 Acquisition date : 3-0CT-2016 09:15:18. Sample ID G405235033 Sample quantity 1.66788E+02 GRAM Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.54 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ********************************************************************************. Pk It 1 2 3 4 5 6 7 8 9 10 . 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 2 2 0 0 0 0 0 0 0 0 0 4 4 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3640 of 5809 Energy 46.58* 57.57* 63.27* 74.83* 77.19* 84. 07*" 88.48 92.91* 128.95 177.16 178.79 185.90* 191.54 210.34 238.76* 241. 75 270.37 293.03 295.35* 300.61 338.48* 352.02* 422. 96 463.13 511.36* 527.08 5 63. 5 6 583.36* 609.42* 662.06 683.77 704.20 770.18 796.52 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 56 18 32 229 344 63 219 143 19 13 20 100 14 60 408 102 50 25 131 22 59 252 11 26 61 16 16 91 166 19 7 20 6 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 183 141 267 166 126 140 216 169 124 46 75 127 52 76 61 89 62 38 45 68 54 50 25 16 38 15 13 42 36 17 24 32 39 24 0.97 0.98 0.75 0.95 0.87 2.09 3.77 1. 22 0.96 1. 25 1.10 1. 58 0.90 0.98 1.11 1. 65 2.58 1. 49 1.15 0. 99, 1. 23 1.18 0. 63 1. 45 2.79 1. 41 1. 89 0.99 1*. 27 2.14 3.26 4.88 0.59 1.17 92. 67 114. 63 126.04 149.16 153.88 167.62 176.45 185.31 257.38 353.79 357.04 371.27 382.54 420.14 476.99 482.96 540.20 585.52 590.16 600.67 676.42 703.49 845.40 925.75 1022.21 1053.66 1126.63 1166. 25 1218.37 1323.68 1367 .12 1408.00 1539.99 1592.69 89 113 122 143 143 164 171 182 253 351 356 365 379 416 470 470 535 582 582 597 672 698 841 922 1014 1049 1122 1160 1212 1320 1359 1400 1530 1587 9 1.55E-02 47.3 6 5.03E-03107.1 9 8.96E-03 96.2 15 6.37E-02 11.1 15 9.54E-02 7.5 7 1.76E-02 34.2 11 6.07E-02 14.7 9 3.96E-02 19.6 8 5.23E-03105.5 5 3.49E-03 84.9 7 5. 64E-03 72. 6 11 2.78E-02 24.8 6 3.84E-03 87.0 10 l.66E-02 30.4 19 1.13E-01 6. 0 19 2.83E-02 22.7 9 1. 31. 9 16 6.85E-03 50.3 16 3.63E-02 12.6 10 6.llE-03 73.1 10 1. 65E-02 27. 0 11 8.4 6 2.98E-03 80.3 8 7.29E-03 33.6 17 1. 69E-02 30. 6 10 4.44E-03 51.7 10 4.46E-03 48.3 12 2.52E-02 18.0 13 4.61E-02 10.9 8 5.39E-03 43.7 10 2.03E-03132.6 16 5.56E-03 67.1 14 1.77E-03210.2 9 2.13E-03122.1 Fit 5.16E-01 1.33E+OO 5.34E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 805.08 15 10 4.41 1609.82 1602 14 4.lOE-03 53.2 36 0 *814.59 9 11 0.60 1628.84 1624 8 2.40E-03 76.7 37 0 860.60 26 18 2.74 1720.91 1715 12 7. llE-03 38.6 38 0 911. 28* 95 6 1. 76 1822.33 1816 15 2.63E-02 12.3 39 0 969. 67* 34 24 1. 56 1939.15 1933 13 9.51E-03 35.9 40 0 981.44 9 4 1. 46 1962. 71 1958 9 2.59E-03 51. 7 41 0 1105. 03 31 19 6.14 2210.03 2195 25 8.62E-03 41. 6 42 0 1121.65* 27 57. 0.97 2243.29 2234 20 7.59E-03 69.6 43 0 1239. 96 7 30 0.67 2480.08 2471 12 2.05E-03152.7 44 0 1260 .11 15 6 1. 61 2520.40 2513 13 4.14E-03 43.5 45 0 1265.43 16 0 1. 39 2531.06 2526 10 4.44E-03 25.0 46 0 1376.80 21 2 2.39 2753.97 2749 11 5.74E-03 26.8 47 0 1389.44 7 2 1. 56 2779.27 2775 8 1. 91E-03 52.3 48 0 1460.79* 342 0 2.43 2922.11 2915 16 9.50E-02 5.5 49 0 1764.68* 30 0 2.15 3530.50 3524 13 8.28E-03 19.2 Flag: "*" ,,,,; Peak area was modified by background subtraction Page 3641of5809 VMS Nuclide I-dentification Report 'v3 .1 Generated 3-0CT-2016 1.0: 15: 53 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l PEAK Vl6.9,PEAKEFF V2.2;ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 11:53:00 G405235033 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:15:18 166.79 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA25 0 01:00:00.00 1.50 keV No. Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3642 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 87.57 CD-109 88.03 TH-229 88.47 U-235 89. 96 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.54 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.131E+OO 1.245E+Ol l.245E+Ol 10.91 OK CD-109 88.03 3.70* 9.261E+OO 3 .116E+OO 5. OOOE+o*o 37.19 OK SN-126 64.28 9.60 9.543E+OO 2.217E-01 2.217E-01 192.38 OK 86.94 8.90 9.280E+OO Line Not Found Absent 87.57 37.00* 9.261E+OO 3 .116E-01 3 .116E-01 37.19 OK BA-137M 661.66 89.90* 2.256E+OO 4.661E-02 4.754E-02 87.40 OK CS-137 661. 66 85.10* 2.256E+OO 4.924E-02 5.023E-02 87.40 OK TL-208 277.37 6.60 4.809E+OO Line Not Found Absent 583.19 85.00* 2.510E+OO 2.099E-01 2.099E-01 36.00 OK 860.56 12.50 l.810E+OO 5.330E-01 5.330E-01 77.30 OK PB-210 46.54 4.25* 9.147E+OO 9.292E-01 9.546E-01 94.62 OK BI-211 72. 87 1. 23 9.424E+OO Line Not Found Absent 351.06 12.92* 3.893E+OO 3.254E-01 3.254E-01 224.40 OK PB-212 74.82 10.28 9.405E+OO 9.975E-01 9.975E-01 34.80 OK 77 .11 17.10 9.382E+OO 1.322E+OO l.322E+OO 14.98 OK 238.63 43.60* 5.476E+OO 9. 371E-01 9. 371E-01 11. 95 OK 300.09 3.30 4.479E+OO 7. 962E-01 7.962E-01 146.20 OK BI-214 609.32 45.49* 2.419E+OO 7.421E-01 7.424E-01 21. 77 OK 1120*. 29 14.92 l.442E+OO 5.778E-01 5. 780E.:...01 139. 21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 OK PB-214 74.82 5.80 9.405E+OO Line Not Found <<INT Reject 77 .11 9.70 9.382E+OO 2.331E+OO 2.332E+OO 14.98 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Rej e*ct 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.550E+OO 8.355E-01 8.358E-01 25.28 OK 351. 93 35.60* 3.894E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.419E+OO 7. 421E-01 7.424E-01 21.77 OK 1120.29 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 OK RA-224 240.99 4.10* 5.418E+OO 1.039E+OO 1.039E+OO 115. 47 OK RA-226 609.32 45.49* 2.419E+OO 7. 421E-01. 7.424E-01 21.77 OK 1120.29 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 OK AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 OK 794.95 4.25 1.935E+OO Line Not Found Absent 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1.725E+OO 9.939E-01 9.939E-01 24.61 OK 968.97 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4. 031E+OO 6.879E-01 6.879E-01 54.05 OK 794.95 4.25 1.935E+OO Line Not Found Absent 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1. 725E+OO 9.939E-01 9.939E-01 24.61 OK 968. 97 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 OK TH-228 74.82 10.28 9.405E+OO 9.975E-01 9.975E-01 34.80 OK 77 .11 17.10 9.382E+OO 1.322E+OO 1.322E+OO 14.98 OK 238.63 43.60* 5.476E+OO 9.371E-01 9. 371E-01 11. 95 OK 300.09 3.30 4.479E+OO 7. 962E-01 7.962E-01 146.20 OK Page 3643 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-229 85.43 14.70 9.313E+OO 2.827E-01 2.828E-01 68.42 OK 88.47 24.00 9.261E+OO 4.803E-01 4.804E-01 37.19 OK 193.51 4.41* 6. 496E+OO Line Not Found Absent* 210.85 2.80 6.083E+OO 1.951E+OO l.951E+00 60.83 OK TH-230 609.32 45.49* 2.419E+OO 7.421E-01 7.421E-01 21.77 OK 1120. 29 14.92 l.442E+OO 5.778E-01 5.778E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 OK PA-231 283.69 1. 70 4. 715E+OO Line Not Found Absent 301.36 5.35* 4.479E+OO 4. 911E-01 4. 911E-01 146.20 OK TH-232 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.031E+00 6.879E-01 6.879E-01 54.05 *OK 835. 71 1. 61 1.856E+OO Line Not Found Absent 911. 20 25.80* 1.725E+OO 9.939E-01 *9.939E-01 24.61 OK 968. 97 15.80 1. 636E+OO 6.143E-01 6.143E-01 71. 84 OK TH-234 63.29 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 OK 92.59 4.23 9.200E+OO 2. 221E+'00 2.221E+OO 39. 28 OK U-234 609.32 45.49* 2.419E+OO 7. 421E-01 7. 421E-01 21.77 OK 1120.29 14.92 1.442E+OO *5. 778E-01 5.778E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 OK U-235 89. 96 3.47 9.261E+OO 3.322E+OO 3.322E+OO 37.19 OK 93.35 5.60 9.200E+OO 1.677E+OO 1.677E+OO 39.28 OK 143.76 10. 96* 7.922E+OO Line Not Found Absent 163.33 5.08 7.333E+00 Line Not Found Absent 185. 72 57.20 6. 696E+OO 1. 4 7 5E-01 1.475E-01 49. 63 . OK 205.31 5.01 6.202E+OO -----. Line Not Found Absent U-238 63.29 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 OK 92.59 4. 23. 9.200E+OO 2.221E+00 2.221E+OO 39.28 OK AM-243 43.53 5.90 8.344E+OO Line Not Found Absent 74.66 67.20* 9.405E+OO l.526E-01 1.526E-01 34.80 OK ANH-511 511. 00 100.00* 2.808E+OO 1. 086E-01 l.086E-01 61.15 OK Flag: "*" = Keyline Page 3644 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:15:54.03 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l * *Acquisition date 3-0CT-2016 09:15:18 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.54 Half life ratio : ***** *
Sample date 23-NOV-2015 11:53:00 Analyst initials: MXRl *
Sample ID G405235033 Sample Quantity l.6679E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 . * ******************************************************************************* *
CALIBRATION INFORMATION * * * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified are valid. Please refer to Certificate of Analy&is. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.245E+Ol 1. 331E+OO CD-109 5.000E+OO 1.823E+OO SN-126 3 .116E-01 l.136E-01 BA-137M 4.754E-02 4. 072E-02 CS-137 5.023E-02 4.302E-02 TL-208 2.099E-01 7.404E-02 PB-210 9.546E-01 8.852E-01 BI-211 3.254E-01 7.156E-01 PB-212 9.371E-01 1.097E-01 BI-214 7.424E-01 1.584E-01 PB-214 9.540E-01 l.570E-01 RN-222 7.424E-01 1. 584E-01 RA-224 1.039E+OO 1.176E+OO RA-226 7. 42.4E-01 l.584E-01 AC-228 9.939E-01 2.397E-01 RA-228 9.939E-01 2.397E-01 TH-228 9. 371E-01 l.097E-01 TH-229 -l.356E-01 3.616E-01 TH-230 7. 421E-01 1.583E-01 PA-231 4. 911E-01 7.036E-01 TH-232 9.939E-01 2.397E-01 TH-234 5.752E-01 1.084E+OO U-234 7. 421E-01 l.583E-01 U-235 -6.673E-02 l.223E-01 U-238 5.752E-01 l.084E+OO AM-243 1. 52 6E-01 5.205E-02 ANH-511 1. 086E-01 6.509E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3645 of 5809 Key-Line Activity (pCi/GRAM 5. 797E+oo* 7.739E-03 O.OOOE+OO K.L. Cnt Uncert (1.96-sigma) l.150E+Ol 4.402E-02 1. 960E+41 MDA (pCi/GRAM 5. lllE-01 9.225E-01 5.741E-02 6.128E-02 6.473E-02 5.157E-02 5.458E-01 2.390E-01 7.373E-02 l.029E-01 2.740E-01 1. 029E-01 7.916E-01 l.029E-01 1. 898E-01 1. 8 98E-01* 7.373E-02 6 .115E-01 1.029E-01 5.767E-01 1. 898E-01 7.002E-01 1. 029E-01 2.284E-01 7.002E-01 3.806E-02 3.849E-02 MDA (pCi/GRAM 2.428E+Ol 8.863E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -4.657E-03 2. 551E-02 5.368E-02 NOT IDENT. SC-46 -7.630E-02 3.097E-01 6.142E-01 FAIL ABUN V-48 O.OOOE+OO 2.247E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4. 591E+02 O.OOOE+OO SHORT HLIF MN-54 2.332E-02 6.353E-02 1.317E-01 NOT IDENT. C0-56 -l.888E-02 4.738E-01 9. 496E-01 NOT IDENT. MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.701E-02 2.807E-02 5.350E-02 NOT IDENT. .C0-58 1.488E-01 5.994E-01 1. 018E.+00 NOT IDENT. FE-59 -1.548E+OO 6.509E+OO 1.292E+Ol NOT IDENT. C0-60 -2.902E-02 3.783E-02 6.229E-02 NOT IDENT. ZN-65 6.868E-02 l.823E-01 3.398E-01 NOT IDENT. GE-68 -2.094E-01 2.278E+OO 4.427E+OO NOT IDENT. AS-73 -5.035E-02 l.581E+OO 3.319E+OO NOT IDENT. AS-74 O.OOOE+OO 9.573E+03 O.OOOE+OO SHORT HLIF SE-TS 1.970E-02 l.682E-01 3.197E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 596E+39 O.OOOE+OO SHORT HLIF SR-82 O*. OOOE+OO 8.813E+02 O.OOOE+OO SHORT HLIF RB-83 -3.363E-01 5. lllE-01 9.174E-01 NOT IDENT. KR-85 5.943E+OO 5.607E+OO 1.228E+Ol NOT IDENT. SR-85 7. 311E-01 6.935E-01 1.518E+OO NOT IDENT. RB-86 O.OOOE+OO 4.543E+04 O.OOOE+OO SHORT HLIF Y-88 -8.004E-02 2.411E-01 4.697E-01 NOT IDENT. Y-91 -4.258E+02 6.690E+02 l.157E+03 NOT IDENT. NB-94 2.705E-02 2.873E-02 6 .112E-02 NOT IDENT. NB-95 5.409E-01 7.547E-01 1.530E+OO NOT IDENT. NB-95M 5. 313E-01 2.103E+OO 3.768E+OO NOT IDENT. ZR-95 -l.002E-01 1.520E+OO 2.857E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 5.757E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 7.546E-04 2.171E-02 4.029E-02 NOT IDENT. RH-102 2.362E-02 5.353E-02 l.090E-01 NOT IDENT. RU-103 -2. 313E+OO 5.470E+OO 9.940E+OO FAIL ABUN .RH-106 5. 091E-02 4.445E-01 8.725E-01 NOT IDENT. RU-106 5. 091E-02 4.445E-01 8. 725E-01 NOT IDENT. AG-108M 1. 42 9E-02 2.158E-02 4.623E-02 NOT IDENT. AG-llOM -5.220E-02 8.605E-02 l.581E-01 NOT IDENT. SN-113 -1.333E-01 1.932E-01 3.581E-01 NOT IDENT. CD-115 O.OOOE+OO l.014E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.365E+05 O.OOOE+OO SHORT HLIF TE-123M 2.838E-02 9.220E-02 l.852E-01 NOT IDENT. SB-124 1.014E+OO 2.487E+OO 5.684E+OO NOT IDENT. SB-125 -3.301E-03 8.494E-02 l.681E-01 FAIL ABUN TE-125M , -1. 522E+Ol 1. 787E+02 3.591E+02 NOT IDENT. I-126 O.OOOE+OO 2.039E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.894E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.779E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.408E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.686E+27 O.OOOE+OO SHORT HLIF BA-133 l.032E-02 3.173E-02 6.073E-02 NOT IDENT. I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 2.949E-02 7.056E-02 l.044E-01 FAIL ABUN CS-135 4.657E-02 1.153E-01 2.086E-01 NOT IDENT. I-135 O.OOOE+OO 8.535E+40 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO .6. 666E+05 O.OOOE+OO SHORT HLIF CE-139 -5.265E-02 8.435E-02 1.548E-01 NOT IDENT. BA-140 O.OOOE+OO 2.373E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 9.283E+05 O.OOOE+OO SHORT HLIF CE-141 -8 .118E+OO 2.186E+Ol 4.142E+Ol NOT IDENT. CE-143 O.OOOE+OO 9.855E+40 O.OOOE+OO SHORT HLIF CE-144 -1.102E-Ol 2.362E-01 4.502E-01 NOT IDENT. PM-144 3:034E-02 4.212E-02 9.126E-02 NOT IDENT. PR-144 2.670E+OO 3.690E+OO 7.997E+OO NOT IDENT. PM-146 3.413E-04 2.975E-02 6.018E-02 NOT IDENT. ND-147 O.OOOE+OO 6.760E+07 O.OOOE+OO SHORT HLIF PM-147 1.649E+02 4.869E'+02 1.002E+03 NOT IDENT. PM-149 O.OOOE+OO 1.569E+41 O.OOOE+OO SHORT HLIF EU-150 3.398E-02 1.919E-02 4.289E-02 FAIL ABUN EU-.152 1.815E-03 6.684E-02 1.362E-01 NOT IDENT. GD-153 -3.060E-02 9.651E-02 1.895E-01 NOT IDENT. EU-154 2.098E'-02 1.075E-01 2.170E-01 NOT IDENT. EU-155 2.049E-02 6. 031E-02 1.249E-01 NOT IDENT. TB-160 1.399E+OO l.713E+OO 3.908E+OO FAIL ABUN H0-166M -2.306E-02 4.847E-02 8.553E-02 FAIL ABUN TM-171 2.265E+OO 2. 968E+OO 6;558E+OO NOT IDENT. Page 3646 of 5809 HF-172 l.815E-02 l.438E-Ol 2.703E-01 FAIL ABUN LU-172 5.152E-02 6.525E-02 l.442E-01 FAIL ABUN LU-176. -5.952E-03 2.034E-02 3.604E-02 FAIL ABUN HF-181 -5.165E-01 4.276E+OO 8.363E+OO FAIL ABUN TA-182 l.570E-01 8.981E-01 l.797E+OO FAIL ABUN RE-183 7. 872E-01 l.652E+OO 1. 672E+OO FAIL ABUN RE-184 -5.474E+OO 3.609E+Ol 7.085E+Ol NOT IDENT. W-188 -7.519E+OO 1. 050E+02 1. 775E+02 FAIL ABUN IR-192 -9.633E-02 4.069E-01 8.085E-01 FAIL ABUN HG-203 -l.666E+OO 2.574E+OO 4.423E+OO NOT IDENT. BI-207 -7.231E-03 4.892E-02 9.341E-02 FAIL ABUN PB-211 -6.909E-02 4.916E-01 9.714E-01 NOT IDENT. BI-212 5.654E-01 5.254E-Ol l.093E+OO NOT IDENT. RN-219 2.788E-02 2.881E-01 5.832E-01 FAIL ABUN RA-223 -l.224E-01 4.698E-01 9.264E-01 FAIL ABUN. AC-227 -2.602E-02 l.727E-01 3.182E-01 FAIL ABUN TH-227 -2.602E-02 l.727E-01 3.182E-01 FAIL ABUN TH-231 -l.224E-01 4.698E-01 9.264E-01 FAIL ABUN PA-233 -2.878E-02 4.547E-02 8.707E-02 FAIL ABUN PA-234 l. l 76E-01 2.449E-01 5.230E-01 NOT IDENT . PA-234M -1. 218E+OO . 3. 796E+OO 7.333E+OO NOT IDENT. NP-237 -2.878E-02 4.547E-02 8.707E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -6.581E-02 l.366E-01 2.642E-01 NOT IDENT. PU-239 2.092E+02 4.327E+02 4.054E+02 FAIL ABUN AM-241 -2.037E-02 3.827E-02 6.426E-02 NOT IDENT. CM-243 l.669E-02 5.052E-02 l.054E-01 NOT. I DENT. BK-247 9.306E-03 5.382E-02 l.029E-01 FAIL ABUN CM-247 1. 127E-02 2.593E-02 5.447E-02 NOT IDENT. CF-249 -2.139E-02 2.847E-02 5. 241E-02. NOT IDENT. CF-251 5.937E-02 9.882E-02 l.334E-01 FAIL ABUN Page 3647of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:15:51.91 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 333 10.66* 1.131E+OO l.245E+Ol 1.245E+Ol 10.91 CD-109 88.03 296 3.70* 9.261E+OO 3.886E+OO 6.236E+OO 29.40 SN-126 64.28 45 9.60 9.543E+OO 2.217E-01 2.217E-01 192.38 86.94 ------8.90 9.280E+OO ------Line Not Found ------87.57 296 37.00* 9.261E+OO 3.886E-Ol 3.886E-01 29.40 BA-137M 661.66 21 89.90* 2.256E+00 4. 661E-02 4.754E-02 87.40 CS-137 661.66 21 85.10* 2.256E+OO 4.924E-02 5.023E-02 87.40 TL-208 277.37 ------6.60 4.809E+OO ------Line Not Found ------583.19 99 85.00* 2.510E+OO 2.099E-01 2.099E-01 36.00 860.56 27 12.50 1.810E+OO 5.330E-01 5.330E-01 77.30 PB-210 46.54 80 4.25* 9.147E+OO 9.292E-01 . 9.546E-01 94.62 BI-211 72.87 ------1.23 9.424E+OO ------Line Not Found ------351.06 294 12.92* 3.893E+OO 2.628E+OO 2.628E+OO 16.79 PB-212 74.82 316 10.28 9.405E+OO 1.469E+OO l.469E+OO 22.20 77 .11 471 17.10 9.382E+OO 1.322E+OO 1.322E+OO 14.98 238.63 497 43.60* 5.476E+OO 9.371E-01 9. 371E-01 11. 95 300.09 26 3.30 4.479E+OO 7. 962E-01 7. 962E-01 146.20 BI-214 609.32 181 45.49* 2.419E+OO 7. 421E-01 7.424E-01 21.77 1120. 29 28 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 PB-214 74.82 316 5.80 9.405E+OO 2.604E+OO 2. 605E+OO . 22.20 77.11 471 9.70 9.382E+OO 2. 331E+OO 2.332E+OO 14.98 87.09 296 3.41 9.261E+OO 4.216E+OO 4.218E+OO 29.40 242.00 124 7.25 *5.418E+00 1.423E+OO l.424E+00 45.30 295.22 156 18.42 4.550E+OO 8.355E-01 8.358E-01 25.28 351.93 294 35.60* 3.893E+OO 9.536E-01 9.540E-01 16.79 RN-2.22 609.32 181 45.49* 2.419E+00 7. 421E-01 7.424E-01 21.77 1120.29 28 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 RA-224 240.99 *. 124 4.10* 5.418E+OO 2.516E+00 2.516E+OO 45.30 RA-226 609.32 181 45.49* 2.419E+OO 7.421E-01 7.424E-01 21.77 1120.29 28 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 AC-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 69 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 794.95 ------4.25 1.935E+OO ------Line Not Found ------835.71 ------1. 61 1.856E+OO ------Line Not Found ------911.20 98 25.80* 1.725E+OO 9.939E-01 9.939E-01 24.61 968. 97 35 15.80 1. 636E+OO 6.143E-01 6.143E-01 71.84 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------*338.32 69 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 794.95 ------4.25 1.935E+OO ------Line Not Found ------835.71 ------1. 61 1.856E+OO ------Line Not Found ------911.20 98 25.80* 1.725E+OO 9.939E-01 9.939E-01 24.61 968. 97 35 15.80 1. 636E+OO 6.143E-01 6.143E-01 71. 84 TH:-228 74.82 316 10.28 9.405E+OO 1.469E+OO 1.469E+OO 22.20 77 .11 471 17.10 9.382E+OO 1.322E+OO 1.322E+OO 14.98 Page 3648 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 497 43.60* 5.476E+OO 9. 371E-01 9. 371E-01 11. 95 300.09 26 3.30 4.479E+OO 7. 962E-01 7. 962E-01 146.20 TH-229 85.43 86 14.70 9.313E+OO 2.827E-01 2.828E-01 68.42 88.47 296 24.00 9.261E+OO 5.990E-01 5.991E-01 29.40 193.51 ------4.41* 6.496E+OO ------Line Not Found ------210.85 74 2.80 6.083E+OO l.951E+OO 1. 951E+OO .. 60.83 TH-230 609.32 181 45.49* 2.419E+OO 7. 421E-01 7. 421E-01 21.77 1120.29 28 14.92 1.442E+OO 5.778E-01 5.778E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 PA-231 283.69 ------1. 70 4.715E+OO ------Line Not Found ------301.36 26 5.35* . 4.479E+OO 4. 911E-01 4. 911E-01 146.20 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 69 11.27 4.031E+OO 6.879E-01 6.879E-01 54.05 835.71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 98 25.80* 1.725E+OO 9.939E-01 9.939E-01 24.61 968. 97 35 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 TH-234 63.29 45 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 92.59 192 4.23 9.200E+OO 2.221E+OO 2.221E+OO 39.28 U-234 609.32 181 45.49* 2.419E+00 7.'421E-01 7. 421E-01 21.77 1120.29 28 14.92 1.442E+OO 5.778E-01 5.778E-01 139 .21 .1764.49 28 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 U-235 89.96 296 3.47 9.261E+00 4.143E+OO 4.143E+OO 29.40 93.35 192 5.60 9.200E+OO 1.677E+OO 1.677E+OO 39.28 143.76 ------10.96* 7.922E+OO ------Line Not Found ------163.33 ------5.08 7.333E+OO ------Line Not Found ------185. 72 125 -57.20 6. 696E+OO 1. 475E-01 l.475E-01 49.63 *205.31 ------5.01 6.202E+OO ------Line Not Found ------U-238 63.29 45 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 92.59 192 4.23 9.200E+OO 2.221E+OO 2.221E+OO 39.28 AM-243 43.53 ------5.90 8.344E+00 ------Line Not Found ------74.66 316 67.20* 9.405E+OO 2.247E-01 2.247E-01 22. 20. ANH-511 511. 00 68 100.00* 2.808E+00 1. 086E-01 l.086E-01 61.15 Flag: "*" Key line Page 3649 of 5809 Page : 3 Summary of Nuclide Activity ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Total number of lines in spectrum 49 Number of unidentified lines 12 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 3'0. OBY l.41E+l0Y 22.20Y 7.04E+08Y l.41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+10Y l'. 41E+l0Y 1. 41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y J 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 60 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.245E+Ol 3.886E+OO 3.886E-01 4.661E-02 4.924E-02 2.099E-01 9.292E-01 2.628E+OO 9.371E-01 7.421E-01 9.536E-01 7.421E-01 2.516E+OO 7. 421E-01 9.939E-01 9.939E-01 9. 371E-01 5.990E-01 7. 421E-01 4. 911E-01 9.939E-01 5.752E-01 7.421E-01 1. 475E-01 5.752E-01 2.247E-01 l.086E:.._01 3.534E+Ol 3.534E+Ol Decay Corr pCi/GRAM 1.245E+Ol 6.236E+OO 3.886E-01 4.754E-02 5.023E-02 2.099E-01 9.546E-01 2.628E+OO 9.371E-01 7.424E-01 9.540E-01 7.424E-01 2.516E+OO 7.424E-01 9.939E-01 9.939E-01 9.371E-01 5. 991E-01 7.421E-01 4. 911E-01 9.939E-01 5. 7 52E-.01 7.421E-01 l.475E-01 5.752E-01 2.247E-01 1. 086E-01 3.772E+Ol 3. 772E+OL 75.51% Decay Corr 2-Sigma Error 0.136E+Ol 1.833E+OO 1.142E-01 4.155E-02 4.390E-02 0.756E-01 9.033E-01 0.441E+OO 1.120E-01 l.616E-01 1.602E-01 l.616E-01 1.140E+OO l.616E-01 2.446E-01 . 2.446E-01 1.120E-01 l.761E-01 l.616E-01 7.180E-01 2.446E-01 11. 06E-01 1.616E-01 0.732E-01 11. 06E-01 0.499E-01 0.664E-01 "M" Manually accepted 2-Sigma %Error 10.91 29.40 29.40 87.40 87.40 36.00 94.62 16.79 11. 95 21.77 16.79 21. 77 45.30 21.77 24.61 24.61 11. 95 29.40 21.77 146.20 24.61 192.38 21.77 49.63 192.38 22.20 61.15 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3650 of5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235033 Acquisition date : 3-0CT-2016 09:15:18 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 57.57 26 199 0.98 114. 63 113 6 5.03E-03 **** 9.63E+OO T 0 128.95 25 162 0. 96 257.38 253 8 5.23E-03 **** 8.36E+00 T 0 177.16 16 58 1. 25 353.79 351 5 3.49E-03 **** 6.93E+OO T 0 178.79 26 94 1.10 357.04 356 7 5.64E-03 **** 6.89E+OO 0 191.54 17 65 0.90 382.54 379 6 3.84E-03 **** 6.55E+00 0 270.37 60 75 2.58 540.20 535 9 1.39E-02 63.9 4.92E+OO T 2 293.03 29 45 1. 49 585.52 582 16 6.85E-03 **** 4.58E+OO T 0 422.96 12 29 0.63 845.40 841 6 2.98E-03 **** 3. 31E+OO T 0 4 63 .13 30 18 1. 45 925.75 922 8 7.29E-03 67.3 3.06E+OO T 0 527.08 18 17 1. 41 1053.66 1049 10 4.44E-03 **** 2.74E+OO T 0 563.56 18 14 1. 89 1126.63 1122 10 4.46E-03 96. 6 2.58E+OO T 0 683.77 8 26 3.26 1367 .12 1359 10 2.03E-03 **** 2.20E+OO 0 704.20 21 34 4.88 1408.00 1400 16 5.56E-03 **** 2.14E+OO 0 770.18 7 41 0.59 1539.99 1530 14 1.77E-03 **** l.99E+OO 0 796. 52 8 26 1.17 1592.69 1587 9 2.13E-03 **** 1.93E+OO T 0 805.08 16 11 4.41 1609.82 1602 14 4.lOE-03 **** 1.91E+OO 0 814.59 9 12 0.60 1628.84 1624 8 2.40E-03 **** l.90E+OO T 0 981.44 10 4 1. 46 1962.71 1958 9 2.59E-03 **** l.62E+OO 0 1105. 03 31 19 6.14 2210.03 2195 25 8.62E-03 83.3 1.46E+OO 0 1239.96 7 30 0.67 2480.08 2471 12 2.05E-03 **** 1.32E+OO 0 1260.11 15 6 1. 61 2520.40 2513 13 4.14E-03 87.1 l.30E+00 T 0 1265.43 16 0 1. 39' 2531. 06 2526 10 4.44E-03 50.0 1.29E+OO 0 1376.80 20 2 2.39 2753.97 2749 11 5.74E-03 53.5 1. 20E+OO 0 1389 . .44 7 2 1. 56 2779.27 2775 8 1. 91E-03 **** 1.19E+OO Flags: "T" = Tentatively associated Page 3651of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:06.40 *******************************************************************************
GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l * *Acquisition date 3-0CT-2016 09:15:18 Sensitivity 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.54 Half life ratio : ***** *
Sample date 23-NOV-2015 11:53:00 Nuclide Library : SOLID *
Sample ID G405235033 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.6679E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5 '* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.044E-01 4.300E-01 2.676E-02 2.747E-02 2.902E-02 2.282E-02 2.549E-01 l.067E-01 3.415E-02 4.573E-02 1. 324E-01 4.573E-02 3.667E-01 4.573E-02 8.086E-02 8.086E-02 3.415E-02 2.830E-01 4.571E-02 2.613E-01 8.086E-02 3. 311E-01 4.571E-02 l.066E-01 3. 311E-01 l.797E-02 l.698E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3652 of 5809 Le (pCi/GRAM 1.090E+Ol 3.827E-02 O.OOOE+OO 2.009E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 .AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3653 of 5809 2.590E-Ol O.OOOE+OO O.OOOE+OO 5.906E-02 4.172E-01 O.OOOE+OO 2.473E-02 4.369E-01 5.448E+OO 2.554E-02 1. 492E-01 1. 924E+00 1.556E+OO 0.000E+OO 1. 463E-01 O.OOOE+OO O.OOOE+OO 3.944E-01 5.584E+00 6.903E-01 O.OOOE+OO 1.815E-01 5.053E+02 2.762E-02 6. 696E-01 1. 741E+00 l.255E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 1. 876E-02 4.887E-02 4.338E+OO 3. 881E-01 3.881E-01 2.094E-02 6.742E-02 1.605E-01 O.OOOE+OO O.OOOE+OO 8.605E-02 2.347E+OO 7.593E-02 1. 672E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.752E-02 O.OOOE+OO 4. 714E-02 9.612E-02 O.OOOE+OO O.OOOE+OO 7.188E-02 0.000E+OO 0.000E+OO 1.928E+Ol O.OOOE+OO 2.096E-Ol 4.029E-02 3. 531E+OO 2.658E-02 O.OOOE+OO 4.670E+02 O.OOOE+OO 1.978E-02 6.172E-02 8.850E-02 9.379E-02 5.849E-02 1.715E+OO 3.728E-02 3.075E+00 l.256E-01 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLI.F NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3654 of 5809 6.290E-02 1. 64 6E-02 3.720E+OO 7.831E-01 7.901E-01* 3.093E+Ol 8.078E+Ol 3.692E-01 2.032E+OO 4.109E-02 4.365E-01 5.014E-01 2.636E-01 4.248E-01 l.459E-01 l.459E-01 4.248E-01 3.967E-02 2.304E-01 3. 201E+OO 3. 967E-02 O.OOOE+OO 1.225E-01 1. 902E+02 3.017E-02 A. 913E-02 4. 712E-02 2.467.E-02 2.348E-02 6.124E-02 FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:11.91 *******************************************************************************

GEL Laboratories LLC * *' 2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l *
Acquisition date 3-0CT-2016 09:15:18 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.54 Half life ratio : ***** *
Sample date 23-NOV-2015 11:53:00 Nuclide Library : SOLID *
Sample ID G405235033 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.6679E+02 GRAM *
Quantity Err(%) : 1.1991E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN * *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.245E+Ol 1.481E+OO CD-109 5.000E+OO l.874E+OO SN-126 3 .116E-01 l.156E-01 BA-137M 4.754E-02 4.077E-02 CS-:--137 5.023E-02 4.307E-02 TL-208 2.099E-01 7.458E-02 PB-210 9.546E-01 8.888E-01 BI-211 3.254E-01 7.294E-01 PB-212 9.371E-01 l.204E-01 BI-214 7.424E-01 l.616E-01 PB-214 9.540E-01 l.619E-01 RN-222 7.424E-01 l.616E-01 RA-224 l.039E+OO l .181E+OO RA-226 7.424E-01 l.616E-01 AC-228 9.939E-01 2.450E-01 RA-228 9.939E-01 2.450E-01 TH-228 9. 371E-01 l.204E-01 TH-229 -l.356E-01 3.616E-01 TH-230 7.421E-01 l.615E-01 PA-231 4. 911E-01 7 .114E-01 TH-232 9.939E-01 2.450E-01 TH-234 5.752E-01 1.092E+OO U-234 7. 421E-01 1.615E-01 U-235 -6.673E-02 l.224E-01 U-238 5.752E-01 1.092E+OO AM-243 l.526E-01 5.366E-02 ANH-511 1. 086E-Ol 6.524E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3655 of 5809 Key-Line Activity (pCi/GRAM 5.797E+OO 7.739E-03 -l.OOOE+41 K.L Act error (1. 96-sigma) l.151E+Ol 4.402E-02 6.763E+41 TPU ( 1. 96-sigma) 1. 481E+OO l.874E+OO l.156E-01 4.077E-02 *4.307E-02 *7.458E-02 8.888E-01 7.294E-01 1. 204E-01 1. 616E-01 1.619E-01 l.616E-01 .l .181E+OO 1.616E-01 2.450E-01 2.450E-01 l.204E-01 3.616E-01 l.615E-01 7 .114E-01 2.450E-01 l.092E+OO l.615E-01 l.224E-01 l.092E+OO 5.366E-02 6.524E-02 TPU ( 1. 96-sigma) l.180E+Ol 4.416E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -4.657E-03 2. 551E-02 2.560E-02 NOT IDENT. SC-46 -7.630E-02 3.097E-01 3 .116E-01 FAIL ABUN V-48 -l.526E+03 2.247E+04 2.248E+04 SHORT HLIF CR-51 -1. 8 61E+02 4.592E+02 4.668E+02 SHORT HLIF MN-54 2.332E-02 6.354E-02 6.440E-02 NOT IDENT. C0-56 -l.888E-02 4.738E-01 4.739E-01 NOT IDENT. MN-56 -l.000E+41 3.414E+42 O.OOOE+OO SHORT HLIF C0-57 -1.701E-02 2.808E-02 2. 911E-02 NOT IDENT. C0-58 1. 488E-01 5.994E-01 6.032E-01 NOT IDENT. FE-59 -1.548E+OO 6.510E+OO 6.547E+OO NOT IDENT. C0-60 -2.902E-02 3.784E-02 4.004E-02 NOT IDENT. ZN-65 6.868E-02 1.823E-01 l.849E-01 NOT IDENT. GE-68 -2.094E-01 2.278E+OO 2.280E+OO NOT IDENT. AS-73 -5.035E-02 1.581E+OO l.582E+OO NOT IDENT. AS-74 -6.126E+02 9.573E+03 9.577E+03 SHORT HLIF SE-75 1.970E-02 1.682E-01 l.685E-01 NOT IDENT. BR-77 l.363E+40 l.239E+41 O.OOOE+OO SHORT HLIF SR-82 -2.913E+02 8. 814E+02 8. 911E+02 SHORT HLIF RB-83 -3.363E-01 5 .131E-01 5. 351E-01 NOT IDENT. KR-85 5.943E+OO 5.612E+OO 6.219E+OO NOT IDENT. SR-85 7. 311E-01 6.941E-01 7.684E-01 NOT IDENT. RB-86 -l.944E+Ol 4.543E+04 4.543E+04 SHORT HLIF Y-88 -8.004E-02 2.411E-01 2.438E-01 NOT IDENT. Y-91 -4.258E+02 6.692E+02 6. 961E+02 NOT IDENT. NB-94 2.705E-02 2.875E-02 3.123E-02 NOT IDENT. NB-95 5.409E-01 7. 551E-01 7.935E-01 NOT IDENT. NB-95M 5.313E-01 2.103E+00 2 .117E+OO NOT IDENT. ZR-95 -l.002E-01 1.520E+OO 1.521E+OO NOT IDENT. NB-97 1.000E+41 2.735E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 6.038E+41 O.OOOE+OO SHORT HLIF M0-99 -5.458E+32 5.757E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 1. 017E+42 O.OOOE+OO SHORT HLIF RH-101 7.546E-04 2 .171E-02 2. l 71E-02 NOT IDENT. RH-102 2.362E-02 5.357E_.:02 5.462E-02 NOT IDENT. RU-103 -2.313E+OO 5.471E+OO 5.569E+OO FAIL ABUN RH-106 5.091E-02 4.445E-01 4.451E-01 NOT IDENT. RU-106 5.091E-02 4.445E-01 4. 451E-01 NOT IDENT. AG-108M 1. 429E-02 2.159E-02 2.253E-02 NOT IDENT. AG-llOM -5.220E-02 8.609E-02 8.925E-02 NOT IDENT. SN-113 -l.333E-01 l.933E-01 2.024E-01 NOT IDENT. CD-115 l.OOOE+41 1. 031E+41 O.OOOE+OO SHORT HLIF SN-117M 6. 966E+04 1.368E+05 1.403E+05 SHORT HLIF TE-123M 2.838E-02 9. 221E-02 9.309E-02 NOT IDENT. SB-124 1.014E+OO 2.488E+OO 2.530E+OO NOT IDENT. SB-125 -3.301E-03 8.494E-02 8. 496E-02 FAIL ABUN TE-125M -1.522E+Ol 1. 787E+02 1.789E+02 NOT IDENT. I-126 8.265E+05 2.043E+06 2.077E+06 SHORT HLIF SB-126 3.727E+05 l.895E+06 1.903E+06 SHORT HLIF SB-127 2.244E+22 2.797E+23 0.000E+OO SHORT HLIF I-131 7.160E+08 l.408E+l0 1.408E+l0 SHORT HLIF I-132 1.000E+41 4.736E+42 0.000E+OO SHORTHLIF TE-132 4.058E+27 7.878E+27 O.OOOE+OO SHORT HLIF BA-133 1.032E-02 3.174E-02 3.208E-02 NOT IDENT. I-'133 -1.000E+41 8.397E+41 O.OOOE+OO SHORT HLIF CS-134 2.949E-02 7.057E-02 7 .181E-02 FAIL ABUN CS-135 4.657E-02 1.154E-01 1.172E-01 NOT IDENT. I-135 l.000E+41 7.166E+41 O.OOOE+OO SHORT HLIF CS-136 -4.422E+05 6.684E+05 6.975E+05 SHORT HLIF
CE-139 -5.265E-02 8.502E-02 8.827E-02 NOT IDENT. BA-140 -5.634E+05 2.373E+06 2.386E+06 SHORT HLIF LA-140 -2.105E+05 9.284E+05 9.332E+05 SHORT HLIF CE-141 -8.118E+OO 2.186E+Ol 2.217E+Ol NOT IDENT. CE-143 l.OOOE+41 9.912E+40 O.OOOE+OO SHORT HLIF CE-144 -l.102E-01 2.363E-01 2.414E-01 NOT IDENT. PM-144 3.034E-02 4.216E-02 4.432E-02 NOT IDENT. PR-144 2.670E+OO 3.692E+OO 3.883E+OO NOT IDENT. PM-146 3.413E-04 2.975E-02 2.975E-02 NOT IDENT. ND-147 -4.752E+05 6.760E+07 6.760E+07 SHORT HLIF PM-147 l.649E+02 4.870E+02 4.926E+02 NOT IDENT. PM-149 -1.000E+41 l.585E+41 O.OOOE+OO SHORT HLIF EU-150 3.398E-02 l.924E-02 2.460E-02 FAIL ABUN EU-152 l.815E-03 6.684E-02 6.685E-02 NOT IDENT. GD-153 -3.060E-02 9.653E-02 9.751E-02 NOT IDENT. EU-154 2.098E-02 1. 075E-01 l.079E-01 NOT IDENT. EU-155 2.049E-02 6.033E-02 6.103E-02 NOT IDENT. TB-160 l.399E+00 1. 715E+OO l.827E+OO FAIL ABUN H0-166M -2.306E-02 4.848E-02 . 4. 958E-02 FAIL ABUN TM-171 2.265E+00 2.974E+OO 3.144E+OO NOT IDENT. Page 3656 of 5809 HF-172 1.815E-02 l.438E-01 l.440E-01 FAIL ABUN LU-172 5.152E-02 6.546E-02 6.946E-02 FAIL ABUN LU-176 -5.952E-03 2.034E-02 2.052E-02 FAIL ABUN HF-181 -5.165E-01 4.276E+OO 4.282E+OO FAIL ABUN TA-182 1.570E-01 8. 981E-01 9.009E-01 FAIL ABUN RE-183 7. 872E-01 1.657E+OO 1.694E+OO FAIL ABUN RE-184 .-5.474E+OO 3.611E+Ol 3.620E+Ol NOT IDENT. W-188 -7.519E+OO l.050E+02 l.050E+02 FAIL IR-192 -9.633E-02 4. *o69E-Ol 4.092E-01 FAIL ABUN HG-203 -1.666E+OO 2.575E+OO 2.682E+OO NOT IDENT. BI-207 -7.231E-03 4.892E-02 4.903E-02 FAIL ABUN PB-211 -6.909E-02 4.916E-01 4.926E-01 NOT IDENT. BI-212 5.654E-01 5.262E-01 5.846E-01 NOT IDENT. RN-219 2.788E-02 2.881E-01 2.884E-01 FAIL ABUN RA-223 -l.224E-01 4.699E-01 4.731E-01 FAIL ABUN AC-227 -2.602E-02 1. 728E-01 1. 732E-01 FAIL ABUN TH-227 -2.602E-02 1. 728E-01 1.732E-01 FAIL ABUN TH-231 -1.224E-01 4.699E-01 4. 731E-01 FAIL ABUN PA-233 -2.878E-02 4.549E-02 4.730E-02 FAIL ABUN PA-234 1.176E-01 2.794E-01 2.844E-01 NOT IDENT. PA-234M -1.218E+OO 3.796E+OO 3.835E+OO NOT IDENT. NP-237 -2.878E-02 4.549E-02 4.730E-02 FAIL ABUN NP-238 -1. OOOE+41 9.347E+41 O.OOOE+OO SHORT HLIF NP-239 -6.581E-02 l.367E-01 l.399E-01 NOT IDENT. PU-239 2.092E+02 4.328E+02 4.430E+02 FAIL ABUN AM-241 -2.037E-02 3.830E-02 3.938E-02 NOT IDENT. CM-243 1.669E-02 5.054E-02 5. llOE-02 NOT IDENT. BK-247 9.306E-03 5.386E-02 5.402E-02 FAIL ABUN CM-247 1.127E-02 2.599E-02 2.649E-02 NOT IDENT. CF-249 -2.139E-02 2.852E-02 3. OllE-02 NOT'IDENT. CF-251 5.937E-02 9.904E-02 1.026E-01 FAIL ABUN Page 3657 of 5809
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.3078 87.09 63 .1127 136.47 52.2037 45.60 66.9659 87.57 63.2048 140.51 0.0000 46.54 67.2744 88.03 63.2928 143.76 68.7161 49.72 0.0000 88.34 63.3521 144 .24 61.9060 51. 35 ,77. 7822 88.47 63.3770 145.44 59.1028 51. 87 68.9688 89. 96 63.6598 152.43 65.9285 52.39 56.3553 1093.63 63.7880 153.25 0.0000 52.97 55.7473 91.11 0.0000 323.87 62.1495 53.44 73.9804 92.59 63.5753 156.02 0.0000 54.07 77. 9694 93.35 63.7152 158.56 0.0000 57.36 0.0000 94.56 63.9373 159.00 51.5953 57.53 70.6758 94.65 54.6512 162.33 70.2455 57.98 70.8071 94.67 54.6545 162.66 0.0000 59.27 89.7519 94.87 54.6856 163.33 53.0370 59.32 89.7701 97.43 70.3174 165.86 70.7056 59.54 89.8506 98.43 66.9876 176.31 62.6450 60. 96 90.3644 98.44 66.9894 176.60 0:0000 61.17 90.4400 99.53 56.5820 177.52 20.9256 62.93 100.4888 100 .11 55.7864 181.07 0.0000 63.29 100.6294 102.03 65.8696 181.52 61.1037 63.58 100.7422 103.18 55.3583 184.41 58.2281 64.28 101.0137 103.37 55.3867 143.76 58.3561 66.73 80.7121 105.21 64.6342 193.51 60.1853 67.24 87.2493 105.31 64.6512 197.03 52. 9612 125.81 97.5157 106.12 61.1892 198.01 62.7861 67.75 98.3403 106.47 63.0466 201.83 62.0767 69.67 90.9806 109.28 62.5981 203.43 56.7734 70.83 86.2386 111. 00 70.1613 205.31 62.4142 72.81 95.2553 111. 76 0.0000 210.85 50.7968 72. 87 95.2749 114.06 67.0268 215.65 57.8367 74.66 95.8659 116. 30 0.0000 222 .11 46.0362 74.82 95.9176 116.74 64.6957 227.09 56.5437 74.97 95. 9667 119.76 60.5120 227.38 57.6987 77 .11 96.6630 121.12 56.0371 228.16 0.0000 78.74 79.7424 121. 22 56.0504 228.18 45. 30,52 79.69 91.1005 121.78 61. 7365 116.74 45.3052 80.12 83.4404 122.06 62.7133 235.69 44.2570 80.19 0.0000 122.92 49.7089 235. 96 44.2735 80.57 85.2329 123.07 46.9116 238.63 52.8632 81. 00 71. 4050 265.00 53.5549 238.98 0.0000 81. 07 71.4212 125.81 55.3921 240.99 53.0331 81. 75 73.8136 127.23 60.6226 242.00 53.1054 83.79 83.2967 127.91 59.7679 244.70 50.9811 84.00 83.3516 129.30 59.9546 252.40 0.0000 85.43 71. 2781 131.20 62.4393 252.8'0 50.3578 86.55 63.0089 133.02 63.3292 254.15 0.0000 86. 79 63.0546 133. 52 71. 0834 256.23 43.5237 86.94 63.0839 136.00 55.0483 260.90 0.0000 Page 3658 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.8579 355.39 0.0000 584.27 19.9107 264.80 35.6754 356.01 26.2988 595.83 0.0000 265.00 36.8740 364.49 0.0000 427.87 20.1171 268.22 38.2158 366.42 0.0000 602.52 0.0000 269.46 33.4901 372. 51 40.9678 604. 72 14.3300 270.03 33.5140 375.05 35.7088 607.14 14.3514 271.23 35.1619 377.52 38.4753 609.32 21. 2907 273.65 0.0000 356.01 33.3009 610.33 21.3037 276.40 39.8069 388.16 36.1426 614.28 17.6179 277.37 48.3069 388.63 0.0000 618.01 20.3336 277.60 48.3203 391.69 35.3517 620. 36 12.8604 278.00 42.3006 264.66 26.4978 621.93 20.3816 279.20 53.2544 401.81 28.3542 630.19 0.0000 279.54 56.9083 402.40 24.7083 631.29 19.4180 279.70 56.9198 404.85 28.4299 633.25 24.8409 280.46 46.0620 410.95 37.8010 ,634.78 0.0000 283.69 48.6731 413.71 25.8769 635.95 12.9810 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 53.6492 423.72 0.0000 645.85 11. 968 6 285.90 0.0000 427.09 20.5637 657.76 18.0778 287.50 39.1133 427.87 29.9303 657.90 0.0000 290.67 35.9863 433.94 21. 6210 661.66 25.2555 293.27 0.0000 439.40 22.6621 664.57 0.0000 351.93 34.5309 453.88 19.1064 666.33 0.0000 295. 96 34.5599 463.37 24.0621 666.50 0.0000 879.38 29. 7114 468.07 28.0141 667.71 0.0000 299.98 34.7180 473.00 0.0000 677.62 14.9584 300.09 34.7223 475.06 29.1364 685.70 0.0000 300.13 34.7240 476.78 20.4219 695.00 0.0000 301.36 31.4602 477.60 19.4617 696.49 11.1963 302.85 38.1471 482.18 23. 43.51 696. 51 11.1967 256.23 43.2021 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 16.8024 306.78 42.4792 497.08 19.7469 697.49 16.8036 308.46 42.5581 505.52 20.8620 702.65 16.8512 311.90 46.0694 507.63 0.0000 706.68 21.9542 316.51 41.2490 511. 00 18.9497 711. 68 21.4492 319.41 0.0000 514.00 18.9900 720.70 0.0000 320.08 0.0000 514.00 18.9907 721. 93 0.0000 321.04 42.2963 520.40 20.0806 722.78 15.8981 323.87 42.4235 520.69 0.0000 722.91 15.8993 325.23 46.7330 522.65 0.0000 723.31 17.0386 328.76 0.0000 527.90 0.0000 724.19 29.5473 333.37 31. 8779 528.26 16.6584 727.33 23.9044 333.97 18.0067 529.59 15.1575 733.00 27.4014 334.37 24.4475 529.87 0.0000 735.93 16.0081 .338.28 39.6183 531.02 0.0000 333.97 14.8768 338.32 39.6192 537.26 0.0000. 739.50 0,0000 311. 90 44.0222 546.56 0.0000 747.24 21.8528 340.48 44.0222 552.55 13.3438 748.06 24.1633 340.55 0.0000 563.25 14.4728 752.31 20.7568 344.28 31.1946 569.33 29.0618 753.82 0.0000 345.93 32.9817 946.00 22.8361 756.73 18.4922 351.06 23.5541 569.70 22.8397 756.80 18.4928 351. 93 23.5745 583.19 19.8976 884.68 13. 9199 Page 3659 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 8.7079 1274. 44 18.3361 1620.50 3.7621 766.42 13.9370 1001.03 16.4371 1621.92 4.7043 766.84 19.7482 1002.74 14.5129 1678.03 0.0000 772. 60 0.0000 1004.73 10.6512 1690.97 4. 7864-776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.8721 778.90 18.4064 1028.54 0.0000 1063.66 8.7820 783.70 0.0000 1037.84 9.8083 1771.35 5.8562 785.37 13.1895 1038.76 0.0000 1791.20 0.0000 792.07 16.9383 631.29 18.6985 1808.65 3.9383 794.95 19.7887 1048.07 0.0000 1810.72 0.0000 795.86 15.9088 1049.04 19.7009 1836.06 5.9446 810.06 7 .1191 1050.41 12.8120 810.29 10.6798 1063.66 19.8096 344.28 10.6809 1077.00 0.0000 810.76 9.4954 1077.34 15.9287 815.77 0.0000 1085.87 13.9821 1048.07 0.0000 1093.63 8.0122 832.01 28.7734 1099.45 9.0330 834.85 20.7083 1112. 07 14.5195 835. 71 18.9153 1112.84 12.9094 836.80 0.0000 1115. 54 12.9219 846.75 0.0000 1120. 29 14. 1572 846.77 18.1067 1120. 55 14.1589 856.80 0.0000 1221.41 14.1624 860.56 10.9329 1129. 67 19.4813 871.09 17.3927 1131.51 0.0000 873.19 11. 9114 1147.95 0.0000 875.33 0.0000 1173.23 14.4230 879.38 9.1879 1177.95 11. 3505 880.51 10 .1118 1189.05 16. 5723 883.24 15.6465 1204.77 23.9490 884.68 17.4982 1221.41 13. 6118 889.28 11. 9967 1231.02 18.9075 894.76 12.9507 1235.36 0.0000 898.04 12.0431 1238.28 21.0583 900. 72 16.6943 1260.41 0.0000 903.28 17.6414 1271. 87 11. 7083 911.20 11.18 01 1274.44 11. 7177 912.08 11.1844 1274.54 11. 7184 923.98 0.0000 1291. 59 9.6394 926.50 15.9427 1298.22 0.0000 929 .11 12.2050 1312 .11 0.0000 937.49 28.2651 1332.49 14.1013 944.13 0.0000 1362.66 0.0000 946.00 13.2374 1365.19 7.6686 949.00 14.2003 1368. 63 0.0000 667. 71 0.0000 1384.29 8.8140 962. 31 19.9900 1408.01 3.3283 964.08 15.2417 1457.56 0.0000 966 .17 16.7804 1460.82 5.4064 911.20 18.1355 1489.16 10.8984 968. 97 18.1355 1505.03 8.2099 983.53 0.0000 1584.12 6.5218 984.45 0.0000 1596.21 0.0000 Page 3660 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:16:40.80 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNf;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date 23-NOV-2015 11:20:00 Acquisition date : 3-0CT-2016 09:15:46. Sample ID G405235034 Sample quantity : 1.52487E+02 GRAM Detector name : GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.42 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It Energy 1 2 2 2 3 2 4 2 5 0 6 0 7 0 8 0 9 0 10 3 11 3 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20* 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 3 32 3 33 0 34 0 60.47 63.24* 75.22* 77.22 87.28 89.87 92.97* 109.97 186.34* 238 .. 92* 242.24 277.86 295.76 301.27 338.61 352.21* 371. 44 511.41* 564.49 579.28 583.86* 609.82* 662:78* 729.51 767.85* 861.59 886.67 911. 97* 969. 38 1002.53* 1014.01 1016.81 1102 .17 1121. 77* Page 3661of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 29 42 141 258 44 41 87 41 82 450 86 31 146 41 78 258 23 46 27 19 120 153 41 37 22 35 9 90 71 13 14 19 11 48 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 26 114 147 142 133 96 151 94 137 58 65 70 69 78 66 63 34 47 32 22 35 42 53 60 21 16 7 18 39 23 0 0 5 34 1. 08 121. 00 1.32 126.54 1.32 150.53 1.35 154.53 0.86 174.66 1.33 179.85 1. 64 . 18 6. 05 1.49 220.08 1.80 372.94 1.55 478.17 1.80 484.82 1.26 556.11 1. 32 591. 93 0.98 602.97 0.92. 677.70 1.58 704.91 1.52 743.40 3.26 1023.57 2.23 1129.79 1.34 1159.39 1.60 1168.57 1. 87 1220. 53 1.69 1326.52 3.28 1460.08 0.74 1536.82 2.06 1724.45 1.16 1774.63 1.79 1825.28 5. 81 .1940 .18 0.71 2006.54 1.39 2029.50 1. 70 2035 .10 1.23 2205.96 2.03 2245.18 120 120 143 143 172 178 183 217 368 474 474 551 587 598 674 699 739 1014 112.3 1153 1163 1214 1320 1450 1530 1715 1771 1818 1925 1999 2028 2028 2200 2238 19 8. llE-03 19 l.17E-02 21 3.93E-02 21 7.18E-02 6 1. 21E-02 5 1.15E-02 8 2.41E-02 8 1. 13E-02 12 2.29E-02 25 25 2.39E-02 10 8.54E-03 10 4.05E-02 11 1.13E-02 9 2.16E-02 12 7.17E-02 9 6.26E-03 17 1.29E-02 14 7.58E-03 9 5.15E-03 12 3.33E-02 14 4.26E-02 12 1.14E-02 26 1. 02E-02 12 6.08E-03 16 9.85E-03 8 2.52E-03 15 2.50E-02 26 1. 99E-02 19 3.62E-03 11 3.88E-03 11 5.25E-03 10 3. llE-03 18 l.33E-02 24.6 50.2 18.8 10.8 44.7 39.0 28.7 43.8 31. 7 5.7 27.6 54.6 13.6 45.2 21. 8 8. 9 52.1 43.2 47.7 51. 6 13. 7 12.4 39.8 59.3 47.9 30.2 58.4 15.1 26. 7 95.9 14.3 22.4 47.7 31. 4 Fit 3.57E+OO 1.93E+OO 2.65E+OO 9.90E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1157 .11 8 13 1.16 2315.93 2311 9 .2.34E-03 85.0 36 0 1189.83 49 0 4. 7.1 2381. 41 2371 18 l.36E-02 14.3 37 0 1345.72 24 0 2.53 2693.42 2684 17 6.67E-03 20.4 38 0 1461.78* 369 15 1. 86 2925.71 2919 14 1.03E-01 5.7 39 0 1592.90 5 5 0.48 3188.16 3186 6 1.39E-03 81. 9 40 0 1730.16 16 3 2.30 3462.88 3457 11 4.52E-03 31. 6 41 0 1765.64* 37 0 1. 95 3533.88 3526 15 1. 03E-02 17.3 Flag: "*" = Peak area was modified by background subtraction Page 3662 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:16:42 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;1 PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 23-NOV-2015 11:20:00 G405235034 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:15:46 152.49 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA28 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3663 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.42 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235034 Acquisition date 3-'0CT-2016 09:15:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* l.237E+OO 1.332E+Ol 1.332E+Ol 11. 33 OK CD-109 88.03 3.70* 5.423E+OO 4.194E-01 6. 731E-01 296.78 OK TE-125M 109.28 0.27* 6:445E+OO 1.441E+Ol 6.460E+02 87.60 OK SN-126 64.28 9.60 2.991E+OO 9.454E-01 9.454E-01 100.42 OK 86.94 8.90 5.423E+OO 1.744E-01 1.744E-01 296.78 OK 87.57 37.00* 5.423E+OO 4.194E-02 4.194E-02 296.78 OK BA-137M 661.66 89.90* 2.303E+OO 1.028E-01 1.048E-01 79.68 OK CS-137 661.66 85.10* 2.303E+OO 1.086E-01 l.107E-01 79.68 OK HG-203 70.83 3.69 3.912E+OO Line Not Found Absent 72. 87 6.19 4.138E+OO Line Not Found Absent 279.20 81.56* 4.559E+OO 2.198E-02 2.382E+OO 234.08 OK TL-208 277.37 6.60 4.566E+OO Line Not Found <<INT Reject 583.19 85.00* 2.539E+OO 2.920E-01 2.920E-01 27.44 OK 860.56 12.50 l.886E+OO 7.583E-01 7.583E-01 60.47 OK BI-211 72.87 1. 23 4 .138E+OO Line Not Found Absent 351. 06 12.92* 3.783E+OO l.015E-01 l.015E-01 910.10 OK PB-212 74.82 10.28 4.384E+OO 1.417E+OO 1.417E+OO 54.14 OK 77 .11 17.10 4.583E+OO 2.090E+OO 2.090E+OO 21. 68 OK 238.63 43.6'0* 5.lOlE+OO l.160E+OO 1.160E+OO 11.38' OK 300.09 3.30 4.282E+00 l.613E+00 1.613E+OO 90.48 OK BI-214 609.32 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 OK 1120.29 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO 1.086E+OO 34.63 OK PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.583E+00 3.684E+00 3.685E+OO 21. 68 OK 87.09 3.41 5.409E+OO Line Not Found <<INT Reject 242. 00 7.25 5.054E+OO Line Not Found <<INT Reject 295.22 18.42 4.344E+OO 1.022E+OO l.023E+00 27.12 OK 351. 93 35.60* 3.786E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 OK 1120.29 14.92 l.538E+OO 1.025E+OO 1.025E+OO 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO 1. 086E+OO 34.63 OK RA-224 240.99 4.10* 5.051E+OO 5.683E-01 5.683E-01 246.02 OK RA-226 609.32 45.49* 2.455E+00 7.170E-01 7.173E-01 24.75 OK 1120.29 14.92 l.538E+00 1.025E+OO 1.025E+OO 62.84 OK 1764.49 15.30 l.044E+OO 1.085E+OO 1. 086E+OO 34.63 OK AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835. 71 1. 61 l.930E+00 Line Not Found Absent 911.20 25.80* 1.806E+OO 9.674E-01 9.674E-01 30.11 OK 968. 97 15.80 1. 723E+OO 1.306E+OO 1.306E+OO 53.35 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 *11.27 3.904E+OO 9.786E-01 9.786E-01 43.53 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 1.930E+OO Line Not Found -----Absent 911.20 25.80* l.806E+OO 9.674E-01 9.674E-01 30.11 OK 968.97 15.80 1. 723E+00 1.306E+OO 1.306E+OO 53.35 OK TH-228 74.82 10.28 4.384E+OO 1.417E+OO 1.417E+00 54.14 OK Page 3664 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 17.10 4.583E+OO 2.090E+OO 2.090E+OO 21. 68 OK 238.63 43.60* 5.101E+OO 1.160E+OO 1.160E+OO 11. 38 OK 300.09 3.30 4.282E+OO 1.613E+OO 1. 613E+OO 90.48 OK TH-230 609.32 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 OK 1120. 29 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO l.085E+OO 34.63 OK PA-231 283.69 1. 70 4.487E+OO Line Not Found Absent 301.36 5.35* 4.282E+OO 9.950E-01 9.950E-01 90.48 OK TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 OK 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80*. 1.806E+OO 9.674E-01 9.674E-01 30 .11 OK 968. 97 15.80 1. 723E+OO 1.306E+OO 1. 306E+OO 53.35 OK TH-234 63.29 3.70* 2. 991E+OO 2.453E+OO 2.453E+OO 100.42 OK 92.59 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 OK U-234 609.32 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 OK 112 0. 2 9 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62. 84 OK 1764.49 15.30 1.044E+OO 1.085E+OO 1.085E+OO 34.63 OK U-235 89. 96 3.47 5.597E+OO 1. 330E+OO . 1.330E+OO 77.94 OK 93.35 5.60 5.783E+OO l.671E+OO 1.671E+OO 57.47 OK 143.76 10.96* 6.593E+00 Line Not Found Absent 163.33 5.08 6.352E+OO Line Not Found Absent 185.72 57.20 5.975E+OO l.413E-01 1. 413E-01 63.45 OK 205.31 5.01 5.647E+OO Line Not Found Absent U-238 63.29 3.70* 2.991E+OO 2.453E+OO 2.453E+OO 100.42 OK 92.59 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 OK AM-241 59.54 35.90* 2.628E+OO 2.003E-01 2.006E-01 49.14 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.384E+OO 2.168E-01 2.168E-01 54.14 OK ANH-511 511. 00 100.00* 2.814E+OO 8.764E-02 8.764E-02 86.30 OK Flag: "*" = Keyline Page 3665 of 5809 VAX/VMS Nuclide Identification.Report Generated 03-0CT-2016 10:16:43.69 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l *
Acquisition date 3-0CT-2016 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.42 Half life ratio : ***** *
Sample date 23-NOV-2015 11:20:00 Analyst initials: MXRl *
Sample ID G405235034 Sample Quantity 1.5249E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry*Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date * : l-AUG-2016 10:02:35 Eff. Geometry : CAN *
EfL File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
Combi'ned Acti vi ty-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.332E+Ol 1.478E+OO 6.426E-01 CD-109 6. 731E-01 1.958E+OO 2.032E+00 TE-125M 6.460E+02 5.546E+02 5.213E+02 SN-126 4.194E-02 l.220E-01 l.273E-01 BA-137M 1.048E-01 8.185E-02 7.083E-02 CS-137 1.107E-01 8.646E-02 7.483E-02 HG-203 2.382E+OO 5.463E+OO 4.560E+00 TL-208 2.920E-01 7.852E-02 4.606E-02 BI-211 l.015E-01 9.051E-01 3.331E-01 PB-212 l.160E+00 1.293E-01 8.924E-02 BI-214 7.173E-01 1. 739E-01 1.093E-01 PB-214 1. 059E+OO 1. 847E-01 3.126E-01 RN-222 7.173E-01 1. 739E-01 1.093E-01 RA-224 5.683E-01 l.370E+OO 9.563E-01 RA-226 7.173E-01 l.739E-01 l.093E-01 AC-228 9.674E-01 2.854E-01 l.962E-01 RA-228 9.674E-01 2.854E-01 1.962E-01 TH-228 1.160E+OO 1. 293E-01 8.924E-02 TH-230 7.170E-01 1.739E-01 1.093E-01 PA-231 9.950E-01 8.823E-01 6.843E-01 TH-232 9.674E-01 2.854E-01 1. 962E-01 TH-234 2.453E+OO 2.414E+OO 2.094E+00 U-234 7.170E-01 l.739E-01 l.092E-01 U-235 -l.439E-03 l.846E-01 3.356E-01 u:...238 2.453E+OO 2.414E+OO 2.094E+OO AM-241 2.006E-01 9.659E-02 2. 451E-'01 AM-243 2.168E-01 l.151E-01 8.252E-02 ANH-511 8.764E-02 7.412E-02 4.272E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 8.348E-01 1.271E+Ol 2.481E+Ol NOT IDENT. NA-22 -4.777E-02 4.131E-02 6.204E-02 NOT IDENT. Page 3666of5809 NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 1.547E-02 2.448E-02 6.358E-02 NOT IDENT. SC-46 -2.201E-01 3.903E-01 6.050E-01 FAIL ABUN V-48 O.OOOE+OO 2.604E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.097E+02 O.OOOE+OO SHORT HLIF MN-54 2.235E-02 5.521E-02 1.175E-01 NOT IDENT. C0-56 -1. 782E-01 5. 096E-01 9.679E-Ol NOT IDENT. MN-56 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.905E-02 4.852E-02 8. 596E-02 NOT IDENT. C0-58 3.946E-02 6.144E-01 l.245E+OO NOT IDENT. FE-59 -5.883E+OO 8.378E+OO l.201E+Ol NOT IDENT. C0-60 1.348E-02 3.622E-02 7.706E-02 NOT IDENT. ZN-65 -8.759E-02 l.973E-01 3.060E-01 NOT IDENT. GE:-68 -5.803E-01 2.493E+OO 4.821E+OO NOT IDENT. AS-73 -8.156E+OO 9.830E+OO 1.737E+Ol NOT IDENT. AS-74 O.OOOE+OO l .183E+04 0.000E+OO SHORT HLIF SE-75 l.688E-01 2.081E-01 4.340E-01 NOT IDENT. BR-77 O.OOOE+OO l.894E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9.634E+02 O.OOOE+OO SHORT HLIF RB-83 -9.954E-02 6.778E-01 1.272E+OO NOT IDENT. KR-85 8.167E+OO 6.956E+OO l.395E+Ol NOT IDENT. SR-85 1. OllE+OO 8.612E-01 1. 727E+OO NOT IDENT. RB-86 0.000E+OO 4.938E+04 0.000E+OO SHORT HLIF Y-88 3.775E-02 1.239E-01 3.491E-01 NOT IDENT. Y-91 5.339E+02 5.828E+o2 l.290E+03 NOT IDENT. NB-94 1.047E-02 2.836E-02 5.633E-02 NOT IDENT. NB-95 -6.412E-02 9. 401E-01 1. 676E+OO NOT IDENT. NB-95M 5.124E-01 2.638E+OO 4.747E+OO NOT IDENT. ZR-95 4.297E-01 1.518E+OO 3.168E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.037E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 9.763E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 -6.833E-03 3.482E-02 6.242E-02 NOT IDEt-:)T. RH-102 -2.568E-02 5.892E-02 1.040E-01 FAIL ABUN RU-103 2. 38.8E-01 6.'790E+OO 1.308E+Ol FAIL ABUN RH-106 -3.706E-02 4.378E-01 8.279E-01 NOT IDENT. RU-106 -3.706E-02 4.378E-01 8.279E-01 NOT IDENT. AG-108M 1.296E-04 2.579E-02 4.959E-02 NOT IDENT. AG-llOM -6.847E-02 1.028E-01 1.550E-01 NOT IDENT. SN-113 -2.662E-02 2.129E-01 4.078E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2.107E+05 O.OOOE+OO SHORT HLIF TE-123M -5. 996E-02 l.441E-01 2.499E-01 NOT IDENT. SB-124 1.555E-01 2.448E+OO 5.061E+OO NOT IDENT. SB-125 -l.639E-03 9.043E-02 1. 746E-01 NOT IDENT. I-126 0. OOOE+OO* 2.107E+06 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 2.542E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO *3. 288E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.683E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.823E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 9.151E+27 O.OOOE+OO SHORT HL:tF . BA-133 3.794E-03 4.035E-02 7.104E-02 FAIL ABUN I-133 O.OOOE+OO l.207E+41 O.OOOE+OO SHORT HLIF CS-134 4.324E-02 4.652E-02 l.030E-01 FAIL ABUN CS-135 -1.680E-01 l.393E-01 2.434E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 6. 571E+05 O.OOOE+OO SHORT HLIF CE-139 -4.221E-02 1.lOOE-01 2.133E-01 NOT IDENT. BA-140 O.OOOE+OO 2.742E+06 0.000E+OO SHORT HLIF LA-140 0.000E+OO l.076E+06 O.OOOE+OO SHORT HLIF CE-141 -8.592E+OO 3.332E+Ol 5.893E+Ol NOT I DENT.* CE-143 O.OOOE+OO 1.292E+41 O.OOOE+OO SHORT HLIF CE-144 -9.719E-02 3.463E-01 6.169E-01 NOT IDENT. PM-144 -l.774E-02 6.166E-02 1.095E-01 NOT IDENT. PR-144 -1. 5.39E+OO 5.400E+OO 9.596E+OO NOT IDENT. PM-146 3.158E-02 4.136E-02 8.603E-02 NOT IDENT. ND-147 O.OOOE+OO 8.050E+07 O.OOOE+OO SHORT HLIF PM-147 -3.560E+02 8.368E+02 1.478E+03 NOT I DENT.* PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 8.007E-03 2.395E-02 4.590E-02 FAIL ABUN EU-152 -4.794E-02 9.410E-02 1. 7.21E-01 NOT IDENT. GD-153 -1.638E-01 l.877E-01 3.242E-01 NOT IDENT. EU-154 -1.140E-01 l.009E-01 l.531E-01 NOT IDENT. EU-155 6.302E-02 1.069E-01 2.070E-01 FAIL ABUN TB-160 6.260E-02 2.053E+OO 4.109E+OO FAIL ABUN H0-166M -5.778E-02 5.685E-02 8.882E-02 NOT IDENT. TM-171 1. 286E+Ol l.988E+Ol 4.027E+Ol NOT IDENT. Page 3667 of 5809 HF-172 -1.829E-01 2.340E-01 3.986E-01 FAIL ABUN LU-172 -3.839E-02 6.747E-02 1.212E-01 FAIL ABUN LU-176 -8.265E-03 2.379E-02 4.245E-02 FAIL ABUN HF-181 3.274E+OO 5.054E+OO 1.047E+Ol NOT IDENT. TA-182 -2.729E-01 9.655E-01 1.790E+OO FAIL ABUN RE-183 -1. 981E-01 3.687E+OO 6.503E+OO FAIL ABUN RE-184 -2.086E+OO 3.266E+Ol 6. 572E+Ol NOT IDENT. W-188 -1.149E+Ol l.219E+02 2 .131E+02 FAIL ABUN IR-192 2.380E-01 4.900E-01 9.945E-01 FAIL ABUN BI-207 2.278E-02 4.652E-02 9.781E-02 FAIL ABUN PB-210 2.036E+OO 3.637E+OO 7.284E+OO NOT IDENT. PB-211 -5.210E-02 6.358E-01 1.208E+OO NOT IDENT. BI-212 *1.109E+OO 6.120E-01 1.318E+OO NOT IDENT. RN-219 2.893E-02 3.732E-01 7.197E-01 NOT IDENT. RA-223 -8.507E-03 5.594E-01 1.080E+OO FAIL ABUN AC-227 -2.436E-02 l.927E-01 3.749E-01 FAIL ABUN TH-227 -2.436E-02 1.927E-01 3.749E-01 FAIL ABUN TH-229 -2.682E-01 4.271E-01 8.053E-01 FAIL ABUN TH-231 -8.507E-03 5.594E-01 1. 080E+OO FAIL ABUN PA-233 -1. 896E-02 5.582E-02 l.048E-01 FAIL ABUN PA-234 -l.484E-01 2.345E-01 4.231E-01 FAIL ABUN PA-234M 3.134E+OO 3.917E+OO 8.979E+OO FAIL ABUN NP-237 -1. 896E-02 5.582E-02 1.048E-01 FAIL ABUN NP-238 O.OOOE+OO 1'. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -1. l 74E-01 2.442E-01 4. 301E-01 FAIL ABUN PU-239 1.029E+02 3.251E+02 6.050E+02 NOT IDENT. CM-243 4.367E-02 9.608E-02 1.848E-01 FAIL ABUN BK-247 3.465E-02 6.670E-02 1.359E-01 NOT IDENT. CM-247 l.436E-02 3.556E-02 7.047E-02 FAIL ABUN CF-249 1. 748E-02 3.125E-02 6.464E-02 NOT IDENT. CF-251 8. 23*7E-02 l.084E-01 2.250E-01 NOT IDENT. Page 3668 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:16:41.51 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 357 10.66* 1.237E+OO 1 .. 332E+Ol 1.332E+Ol 11. 33 CD-109 88.03 55 3.70* 5.423E+OO 1.361E+OO 2.185E+OO 89.48 TE-125M 109.28 51 0.27* 6.445E+OO 1.441Et01 6.460E+02 87.60 SN-126 64.28 55 9.60 2.991E+OO 9.454E-01 9.454E-01 100.42 86.94 55 8.90 5.423E+OO 5.660E-01 5.660E-01 89.48 87.57 55 37.00* 5.423E+OO 1.361E-01 1.361E-01 89.48 BA-137M 661.66 43 89.90* 2.303E+OO 1. 028E-01 1.048E-01 79.68 CS-137 661.66 43 85.10* 2.303E+OO 1. 086E-01 1.107E-01 79.68 HG-203 70.83 ------3.69 3.912E+OO ------Line Not Found ------72.87 ------6.19 4.138E+OO ------Line Not Found ------279.20 .35 81. 56* 4.559E+OO 4.672E-02 5.063E+OO 109.26 TL-208 277.37 35 6.60 4.559E+OO 5.774E-01 5.774E-01 109.26 583.19 128 85.00* 2.539E+OO 2.920E-01 2.920E-01 27.44 860.56 36 12.50 1.886E+OO 7.583E-01 7.583E-01 60.47 BI-211 72. 87. ------1. 23 4.138E+OO ------Line Not Found ------351.06 290 12.92* 3.783E+oo 2. 918E+oo.
2.918E+OO 17.79 PB-212 74.82 183 10.28 4.384E+00 1.994E+OO l.994E+OO 37. 68 77 .11 333 17.10 4.583E+OO 2.090E+OO 2.090E+OO 21. 68 238.63 524 43.60* 5.101E+OO 1.160E+OO 1.160E+OO 11. 38 300.09 46 3.30 4.282E+OO 1.613E+OO 1.613E+OO 90.48 BI-214 609.32 163 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO l.025E+OO 62.84 1764.49 35 15.30 1.044E+OO 1.085E+OO 1.086E+OO 34.63 PB-214 74.82 183 5.80 4.384E+OO 3.534E+OO 3.536E+OO 37.68 77 .11 333 9.70 4.583E+OO 3.684E+OO 3.685E+OO 2.1.68 87.09 55 3.41 5.423E+OO 1. 477E+OO l.478E+OO 89.48 242.00 100 7.25 5.051E+OO 1.344E+OO 1.344E+OO 55.12 295.22 166 18.42 4.344E+OO l.022E+OO 1.023E+OO 27.12 351. 93 290 35.60* 3.783E+OO 1.059E+OO 1.059E+OO 17.79 RN-222 609.32 163 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO l.085E+OO 1. 086E+OO 34.63 RA-224 240.99 100 4 .10* . 5. 051E+OO 2.376E+00 2.376E+OO 55.12 RA-226 609.32 163 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO 1.085E+OO 1.086E+OO 34.63 AC-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 87 11.27 3.904E+OO 9.786E-01 9.786E-01 43.53 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 92 25*. 80* 1.806E+OO 9.674E-01 9.674E-01 30 .11 968. 97 72 15.80 1.723E+OO l.306E+00 1.306E+00 53.35 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 87 11.27 3.904E+OO 9.786E-01 9.786E-01 43.53 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911. 20 92 25.80* 1.806E+OO 9.674E-01 9.674E-01 30 .11 Page 3669 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 72 15.80 1. 723E+OO 1.306E+00 1.306E+OO 53.35 TH-228 74.82 183 10.28 4.384E+OO 1.994E+OO 1.994E+OO 37.68 77 .11 333 17.10 4.583E+OO 2.090E+00 2.090E+OO 21. 68 238.63 524 43.60* 5.101E+OO 1.160E+OO l.160E+OO 11. 38 300.09 46 3.30 4.282E+OO 1.613E+OO 1.613E+OO 90.48 TH-230 609.32 163 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 1120.29 48 14.92 1.538E+OO l.025E+00 l.025E+00 62.84 1764.49 35 15.30 1.044E+OO l.085E+OO 1.085E+OO 34.63 PA-231 283.69 ------. 1. 70 4.487E+OO ------Line Not Found ------301.36 46 5.35* 4.282E+OO 9.950E-01 9.950E-01 90.48 TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 87 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 835. 71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 92 25.80* 1.806E+OO 9.674E-01 9.674E:-01 30 .11 968. 97 72 15.80 1.723E+OO 1.306E+OO 1.306E+OO 53.35 TH-234 63.29 55 3.70* 2.991E+OO 2.453E+OO 2.453E+00 100.42 92.59 110 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 U-234 609.32 163 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 1120.29 48 14.92 l.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO l.085E+00 1.085E+OO 34.63 U-235 89. 96 52 3.47 5.597E+oo 1.330E+OO l.330E+00 77.94 93.35 110 5.60 5.783E+OO
1. 671E+OO 1. 671E+OO 57.47 143.76 ------10.96*' 6.593E+OO ------Line Not Found ------163.33 ------5.08 6.352E+00 ------Line Not Found ------185. 72 98 57.20 5.975E+OO 1. 413E-01 l.413E-01 63.45 205.31 ------5.01 5.647E+OO ------Line Not Found ------U-238 63.29 55 3.70* 2.991E+OO 2.453E+OO 2.453E+OO 100.42 92.59 110 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 AM-241 59.54 38 35.90* 2.628E+OO 2.003E-01 2.006E-01 49.14 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 183 67. 20* 4.384E+OO 3.050E_..:01 3.051E-01 37.68 ANH-511 511. 00 50 100.00* 2.814E+OO 8.764E-02 8.764E-02 86.30 Flag: "*" Key line Page 3670 of 5809 Summary of Nuclide Activity Sample ID : G405235034 Acquisition date Page : 3 3-0CT-2016 09:15:46 Total number of lines in spectrum 41 Number of unidentified lines 10 Number of lines tentatively. identified by NID 31 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-241 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 57.40D 2.30E+05Y 30.08Y 30.08Y 46.59D 1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OdY 1.41E+l0Y 1600. OOY 1. 41E+10Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y. 432.60Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 60 44.8 1. 00 1. 02 1. 02 108. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. .00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.332E+Ol 1.361E+OO 1. 441E+Ol 1. 361E-01 1.028E-01 1. 086E-01 4.672E-02 2.920E-01 2.918E+OO l.160E+OO 7.170E-01 1.059E+OO 7.170E-01 2.376E+00 7.170E-01 9.674E-01 9.674E-01 1.160E+OO 7.170E-01 9.950E-01 9.674E-01 2.453E+OO 7.170E-01 1. 413E-01 2.453E+OO 2.003E-01 3.050E-01 8.764E-02 5.157E+Ol 5.157E+Ol Decay Corr pCi/GRAM 1.332E+Ol 2.185E+OO 6.460E+02 1. 361E-01 1.048E-01 1.107E-01 5.063E+OO 2.920E-01 2.918E+OO 1.160E+OO 7.173E-01 1.059E+OO 7.173E-01 2.376E+OO 7.173E_:Ol 9:674E-01 9.674E-01 1.160E+OO 7.170E-01 9.950E-01 9.674E-01 2.453E+OO 7.170E-01 l.413E-01 2.453E+OO 2.006E-01 3.051E-01 8.764E-02 6.890E+02 6.890E+02 75.61% Decay Corr 2-Sigma Error 0.151E+Ol 1.955E+OO 5.659E+02 1.218E-01 0.835E-01 0.882E-01 5.532E+OO 0.801E-01 0.519E+OO .o .132E+OO 1.775E-01 0.189E+OO l.775E-01 1.309E+OO 1. 775E-01 2.913E-01 2. 913E-01 0 .132E+OO 1.774E-01 9.003E-01 2.913E-01 2.463E+00 l.774E-01 0.897E-01 2.463E+OO 0.986E-01 l.149E-01 7.563E-02 "M" Manually accepted 2-Sigrna %Error 11. 33 89.48 87.60 89.48 79.68 79.68 109.26 27.44 17.79 11. 38 24.75 17.79 24.75 55.12 24.75 30 .11 30.11 11. 38 24.75 90.48 30 .11 100.42 24.75 63.45 100.42 49.14 37.68 86.30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3671 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235034* Acquisition date : 3-0CT-2016 09:15:46 It Energy Area Bkgnd FWHM Channel Left Pw c*ts/Sec %Err %Eff Flags* 0 371.44 25 38 1. 52 743.40 739 9 6.26E-03 **** 3.63E+OO T 0 564.49 29 34 2.23 1129.79 1123 14 7.58E-03 95.4 2.61E+OO T 0 579.28 20 24 1. 34 1159.39 1153 9 5.15E-03 **** 2.55E+OO 0 729.51 38 63 3.28 1460.08 1450 26 1.02E-02 **** 2.14E+OO 0 767.85 23 22 0.74 1536.82 1530 12 6.08E-03 95.7 2.06E+OO T 0 886.67 9 7 1.16 1774.63 1771 8 2.52E-03 **** 1. 85E+OO 0 1002.53 13 23 0. 71 2006.54 1999 19 3.62E-03 **** 1.68E+OO T 3 1014.01 14 0 1. 39 2029.50 2028 11 3.88E-03 28.7 1. 66E+OO 3 1016.81 19 0 1. 70 2035.10 2028 11 5.25E-03 44.9 1. 66E+OO 0 1102.17 11 5 1. 23 2205.96 2200 10 3. llE-03 95.4 1.56E+OO 0 1157 .11 8 12 1.16 2315.93.2311 9 2.34E-03 **** 1.50E+OO 0 1189.83 48 0 4. 71 2381.41 2371 18 1.36E-02 28.6 1.47E+OO T 0 1345.72 23 0 2.53 2693.42 2684 17 6.67E-03 40.8 1.33E+OO 0 1592.90 5 5 0.48 3188.16 3186 6 1.39E-03 **** 1.15E+OO 0 1730.16 15 3 2.30 3462.88 3457 11 4.52E-03 63.3 1. 06E+OO Flags: "T" = Tentatively associated Page 3672 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:56.33 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l *
Acquisition date 3-0CT-2016 09:15:46 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.42 Half life ratio : ***** *
Sample date 23-NOV-2015 11:20:00 Nuclide Library : SOLID *
Sample ID G405235034 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.5249E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-241 AM-243 ANH-511 Le (pCi/GRAM 2.705E-01 9.592E-01 2.423E+02 6.0lOE-02 3.206E-02 3.387E-02 2.076E+OO 1.985E-02 1.524E-01 4.148E-02 4.852E-02 l.512E-01 4.852E-02 4.446E-01. 4.852E-02 8.353E-02 8.353E-02 4.148E-02 4.850E-02 3 .118E-01 8.353E-02 9.822E-01 4.850E-02 l.580E-01 9.822E-01 1.145E-01 3.879E-02 1. 8 92E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3673 of 5809 *Le (pCi/GRAM 1.106E+Ol 2.492E-02 0. OOOE.+00 NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I...:131 I-132 TE-l32 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3674 of 5809 2.524E-02 2.526E-01 O.OOOE+OO O.OOOE+OO 5.165E-02 4.239E-01 O.OOOE+OO 4.019E-02 5.473E-01 4. 971E+OO 3.291E-02 l.319E-01 2 .115E+OO 8.050E+OO 0. OOOE+OO. 2.015E-01 O.OOOE+OO O.OOOE+OO 5.666E-01 6.377E+OO 7.895E-01 O.OOOE+OO l.228E-01 5.708E+02 2.506E-02 7.378E-01 2.208E+OO l.402E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.934E-02 4.598E-02 5.859E+OO 3.627E-01 3.627E-01 2.241E-02 6.538E-02 l.835E-01 0. OOOE+OO O.OOOE+OO l.168E-01 2.046E+OO 7.844E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.237E-02 O.OOOE+OO 4.620E-02 l.124E-01 O.OOOE+OO O.OOOE+OO 9.982E-02 O.OOOE+OO O.OOOE+OO 2.763E+Ol O.OOOE+OO 2.878E-01 4.912E-02 4.304E+OO 3:919E-02 O.OOOE+OO 6.916E+02 O.OOOE+OO 2.109E-02 7.897E-02 1.520E-01 6.169E-02 9.744E-02 l.806E+00 3.862E-02 1.877E+Ol 1.863E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT. IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 . CF-251 Page 3675 of 5809 5.122E-02 1.946E-02 4.734E+OO 7.783E-01 3.044E+OO 2.820E+Ol 9.759E+Ol 4.580E-01 4.316E-02 3.425E+00 5. 501E-01 6.117E-01 3. 2*91E-01 4. 968E-01 1. 723E-01 1.723E-01 3.754E-01 4. 968E-01 4.806E-02 1. 794E-01 4. OllE+OO 4.806E-02 O.OOOE+OO 2.015E-01 2.857E+02 8.683E-02 6.302E-02 3.242E-02 2.932E-02 l.059E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABU:N NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT . NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:01.60 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l * *Acquisition date 3-0CT-2016 09:15:46 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.42 Half life ratio : ***** *
Sample date 23-NOV-2015 11:20:00 Nuclide Library : SOLID *
Sample ID G405235034 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.5249E+02 GRAM *
Quantity Err(%) : 1.3116E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 10: 02: 35 Eff. . Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.332E+Ol 1.635E+OO CD-109 6.731E-01 1. 968E+OO TE-125M 6.460E+02 5.559E+02 SN-126 4 .. 194E-02 1. 226E-01 BA-137M l.048E-01 8.197E-02 CS-137 l.107E-01 8.660E-02 HG-203 2.379E+OO 5.472E+OO TL-208 2.920E-01 7.952E-02 BI-211 1.015E-01 9.217E-01 PB-212 1.160E+OO 1.434E-01 BI-214 7.173E-01 1. 767E-01 PB-214 1.059E+OO 1.900E-01 RN-222 7.173E-01 1. 767E-01 RA-224 5.683E-01 l.376E+00 RA-226 7.173E-01 1. 767E-01 AC-228 9.674E-01 2.898E-01 *RA-228 9.674E-01 2.898E-01 TH-228 1.160E+OO 1.434E-01 TH-230 7.170E-01 1. 766E-01 PA-231 9.950E-01 9.075E-01 TH-232 9.674E-01 2.898E-01 TH-234 2.453E+OO 2.474E+OO U-234 7.170E-01 1.766E-01 U-235 -1.439E-03 1.846E-01 U-238 2.453E+OO 2.474E+OO AM-241 2.006E-01 9.769E-02 AM-243 2.168E-01 1.164E-01 ANH-511 8.764E-02 7.421E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3676 of 5809 Key-Line Activity (pCi/GRAM 8.348E-01 -4.777E-02 K.L Act error ( 1. 96-sigma) 1. 271E+Ol 4.135E-02 TPU ( 1. 96-sigma) 1.635E+OO 1. 968E+OO 5.559E+02 l.226E-01 8.197E-02 8.660E-02 5.472E+OO 7.952E-02 9.217E-01 1.434E-01 1. 767E-01 1.900E-01 1. 767E-01 l.376E+OO 1.767E-01 2.898E-01 2.S98E-01 1.434E-01 1. 766E-01 9.075E-01 2.898E-01 2.474E+OO 1.766E-01 l.846E-01 .2.474E+OO 9.769E-02 l.164E-01 7. 421E-02 TPU (1.96-sigma) l.272E+Ol NOT IDENT. 4.662E-02 NOT IDENT.

NA-24 -1.000E+41 2.042E+41 o. o*ooE+oo SHORT HLIF AL-26 1. 54 7E-02 2.450E-02 2.547E-02 NOT IDENT. SC-46 -2. 201E-01 3.904E-01 4.028E-01 FAIL ABUN V-48 -l.653E+04 2.605E+04 2.710E+04 SHORT HLIF CR-51 3.092E+02 6.099E+02 6.256E+02 SHORT HLIF MN-54 2.235E-02 5.522E-02 5. 613E-02 NOT-IDENT. C0-56 -l.782E-01 5.097E-01 5.160E-01 NOT IDENT. MN-56 -1.000E+41 2. 861E+41 O.OOOE+OO SHORT HLIF C0-57 -1.905E-02 4.853E-02 4.929E-02 NOT IDENT. C0-58 3.946E-02 6.144E-01 6.147E-Oi NOT IDENT. FE-59 -5.883E+00 8.389E+OO 8.798E+OO NOT IDENT. C0-60 l.348E-02 3.622E-02 3.673E-02 NOT IDENT. ZN-65 -8.759E-02 1.973E-01 2.012E-01 NOT IDENT. GE-68 -5.803E-01 2.493E+OO 2.506E+OO NOT IDENT. AS-73 -8.156E+00 9. 972E+OO l.063E+Ol NOT IDENT. AS-74 -1.144E+04 1.187E+04 l.294E+04 SHORT HLIF

SE-75 1.688E-01 2.083E-01 2.217E-01 NOT IDENT. BR-77 l.698E+40 1.544E+41 O.OOOE+OO SHORT HLIF SR-82 -4.785E+02 9.636E+02 9.875E+02 SHORT HLIF RB-83 -9.954E-02 6.779E-01 6.794E-01 NOT IDENT. KR-85 8.167E+OO 6. 964E+OO 7.877E+OO NOT IDENT. SR-85 1. OllE+OO 8.622E-01 9.752E-01 NOT IDENT. RB-86 6.148E+03 4.939E+04 4.946E+04 SHORT HLIF Y-88 3.775E-02 l.239E-01 l.251E-01 NOT IDENT. Y-91 5.339E+02 5.832E+02 6.309E+02 NOT IDENT. NB-94 1. 04 7E-02 2.837E-02 2.876E-02 NOT IDENT. NB-95 -6.412E-02 9. 401E-01 9.405E-01 NOT IDENT. NB-95M 5.124E-01 2.638E+OO 2.648E+OO NOT IDENT. ZR-95 4.297*E-01 1.518E+OO 1.531E+OO NOT IDENT. NB-97 1.000E+41 1.041E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.038E+41 O.OOOE+OO SHORT HLIF M0-99 -6 . 7 9 3 E + 3-3 9.776E+33 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 2.389E+42 O.OOOE+OO SHORT HLIF RH-101 -6.833E-03 3.484E-02 3.497E-02 NOT IDENT. RH-102 -2.568E-02 5.896E-02 6.008E-02 FAIL ABUN RU-103 2.388E-01 6.790E+OO 6.791E+OO FAIL ABUN RH-106 -3.706E-02 4.378E-01 4.381E-01 NOT IDENT. RU-106 -3.706E-02 4.378E-01 4.381E-01 NOT IDENT. AG-108M 1.296E-04 2.579E-02 2.579E-02 NOT IDENT. AG-llOM -6.847E-02 1.029E-01 1. 074E-01 NOT IDENT. SN-113 -2.662E-02 2.130E-01 2.133E-01 NOT IDENT. CD-115 6.312E+40 3 .113E+41 O.OOOE+OO SHORT HLIF SN-117M -5.127E+04 2.108E+05 2.120E+05 SHORT HLIF TE-123M -5. 996E-02 l.442E-01 1.467E-01 NOT IDENT. SB-124 1.555E-01 2.448E+OO 2.449E+OO NOT IDENT. SB-125 -1.639E-03 9.043E-02 9.043E-02 NOT IDENT. I-126 1.378E+06 2.116E+06 2.205E+06 SHORT HLIF SB-126 -6.778E+05 2.545E+06 2.564E+06 SHORT HLIF SB-127 l.364E+23 3.833E+23 O.OOOE+OO SHORT HLIF I-131 -1.753E+10 l.685E+l0 1. 861E+l0 SHORT HLIF I-132 -l.000E+41 1.950E+42 O.OOOE+OO SHORT HLIF TE-132 -8.859E+27 9.898E+27 O.OOOE+OO SHORT HLIF BA-133 3.794E-03 4.035E-02 4.039E-02 FAIL ABUN I-133 -1.000E+41 2.251E+41 O.OOOE+OO SHORT HLIF CS-134 4.324E-02 4.656E-02 5.048E-02 FAIL ABUN CS-135 -1.680E-01 1.398E-01 l.590E-01 NOT IDENT. I-135 -1.000E+41 9.394E+41 O.OOOE+OO SHORT HLIF CS-136 -5.567E+05 6. 601E+0.5 7.062E+05 SHORT HLIF CE-139 -4.221E-02 1.104E-01 l.120E-01 NOT IDENT. BA-140 -l.147E+06 2.743E-r06 2.791E+06 SHORT HLIF LA-140 9.198E+04 l.076E+06 l.077E+06 SHORT HLIF CE-141 -8.592E+OO 3.332E+Ol 3.354E+Ol NOT IDENT. CE-143 1.000E+41 l.297E+41 O.OOOE+OO SHORT HLIF CE-144 -9.719E-02 3.463E-:-01 3.491E-01 NOT IDENT. PM-144 -1.774E-02 6.167E-02 6.219E-02 NOT IDENT. PR-144 -1. 539E+OO . 5.401E+OO 5.445E+OO NOT IDENT. PM-146 3.158E-02 4.142E-02 4.380E-02 NOT IDENT. ND-147 -4.384E+07 8.053E+07 8.292E+07 SHORT HLIF PM-147 -3.560E+02 8.369E+02 8.522E+02 NOT IDENT: PM-149 l.000E+41 2.522E+41 O.OOOE+OO SHORT HLIF EU-150 8.007E-03 2.395E-02 2.422E-02 FAIL ABUN EU-152 -4.794E-02 9.414E-02 9.659E-02 NOT IDENT. GD-153 -l.638E-01 l.880E-01 2.019E-01 NOT IDENT. EU-154 -1.140E-01 l.OlOE-01 1.134E-01 NOT IDENT. EU-155 6.302E-02 1. 070E-01 l.107E-01 FAIL ABUN TB-160 6.260E-02 2.053E+OO 2.053E+OO FAIL ABUN H0-166M -5.778E-02 5.693E-02 6.261E-02 NOT IDENT. TM-171 1.286E+01 1.991E+Ol 2.074E+Ol NOT IDENT. Page 3677 of 5809 HF-172 -l.829E-01 2.359E-01 2.499E-01 FAIL ABUN LU-172 -3.839E-02 6.758E-02 6.977E-02 FAIL ABUN LU-176 -8.265E-03 2.379E-02 2.408E-02 FAIL ABUN HF-181 3.274E+OO 5.056E+OO 5.267E+OO NOT IDENT. TA-182 -2. 729E-01 9.656E-01 9.734E-01 FAIL ABUN RE-183 -1.981E-01 3.687E+OO 3.688E+OO FAIL ABUN RE-184 -2.086E+OO 3.267E+Ol 3.268E+Ol NOT IDENT. W-188 -1.149E+Ol l.219E+02 1.220E+02 FAIL ABUN IR-192 2.380E-01 4.901E-01 5.017E-Ol FAIL ABUN BI-207 2.278E-02 4.653E-02 4.765E.,-02 FAIL ABUN PB-210 2.036E+OO 3.642E+OO 3.755E+OO NOT IDENT. PB-211 -5.210E-02 6.358E-01 6.362E-01 NOT IDENT. BI-212 l.109E+OO 6.146E-01 7.922E-01 NOT IDENT. RN-219 2.893E-02 3.732E-01 3.735E-01 NOT IDENT. RA-223 -8.507E-03 5.594E-01 5.594E-01 FAIL ABUN AC-227 -2.436E-02 1. 928E-01 l.931E-01 FAIL ABUN TH-227 -2.436E-02 l.928E-01 l.931E-01 FAIL ABUN TH-229 -2.682E-01 4.273E-01 4.441E-01 FAIL ABUN TH-231 -8.507E-03 5.594E-01 5.594E-01 FAIL ABUN PA-233 -l.896E-02 5.582E-02 5.648E-02 FAIL ABUN PA-234 -1.484E-01 2.895E-01 2.972E-01 FAIL ABUN PA-234M 3.134E+OO 3.919E+00 4.166E+OO FAIL ABUN NP-237 -1. 896E-02 5.582E-02 5.648E-02 FAIL ABUN NP-238 -l.000E+41 4.811E+41 O.OOOE+OO SHORT HLIF NP-239 -1. l 74E-01 2.444E-01 2. 501E-01 FAIL ABUN PU-239 1.029E+02 3.252E+02 3.285E+02 NOT IDENT. CM-243 4.367E-02 9. 617E-02 . 9.816E-02 FAIL ABUN BK-247 3.465E-02 "6.706E-02 6.886E-02 NOT IDENT. CM-247 l.436E-02 3.564E-02 . 3. 622E-02 FAIL ABUN CF-249 1. 748E-02 3.128E-02 3.226E-02 NOT IDENT. CF-251 8.237E-02 1.088E-01 l.150E-01 NOT IDENT. Page 3678 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 67.7320 87.09 106.0090 136.47 72.9840 4*5. 60 79.5984 87.57 95.4818 140.51 0.0000 46.54 64.0330 88.03 95.5523 143.76 79.7523 49.72 0.0000 88.34 95.6004 144.24 71.2035 51. 35 59.4449 88.47 95.6202 145.44 82.3668 51. 87 52.0750 89. 96 100. 4113 152.43 66.9158 52.39 45.7516 1093.63 82.2431 153.25 0.0000 52.97 53.2681 91.11 0.0000 323.87 62.0819 53.44 69.3204 92.59 80.9670 156.02 0.0000 54.07 64.0764 93.35 81.0624 158.56 0.0000 57.36 0.0000 94.56 87.3433 159.00 78.6366 57.53 62.4014 94.65 87.3549 162.33 60.9648 57.98 73.2290 94.67 87.3578 162.66 0.0000 59.27 66.2270 94.87 87.3845 163.33 64.3750 59.32 67.6737 97.43 93. 4962 165.86 80.4756 59.54 67.7043 98.43 77.4524 176.31 76.2680 60. 96 75.8466 98.44 77.4534 176.60 0.0000 61.17 75.8789 99.53 60.2111 177.52 67.0283 62.93 76.1473 100 .11 74.1694 181.07 0.0000 63.29 76.2016 102.03 84.8384 181.52 70.2799 63.58 76.2453 103.18 68.6828 184.41 76.8887 64.28 76.3505 103.37 69.8666 143.76 75.2768 66.73 76.7136 105.21 71.2193 193.51 77.5699 67.24 76.7884 105.31 71.2293 197.03 51.0212 125.81 76.8530 106.12 73.2601 198.01 57.1270 67.75 76. 8626 106.47 67.0589 201. 83 65.1489 69.67 83.7535 109.28 57.9307 203.43 61.7653 70.83 77.3070 111. 00 69.4476 205.31 74.9438 72.81 82.0215 111. 76 0.0000 210.85 74.4459 72.87 82.0300 114. 06 75.6499 215.65 70.3670 74.66 82.2947 116. 30 0.0000 222 .11 61. 0362 74.82 82.3179 116.74 85.4138 227.09 58.6329 74.97 82.3399 119.76 75.0370 227.38 66.6451 77 .11 82.6516 121.12 82.3302 228.16 0.0000 78.74 82.8858 121. 22 82.3407 228.18 67.5793 79.69 83. 0213 121.78 84.7897 116.74 67.5793 80.12 83.0823 122.06 78.8473 235.69 55.0331 80.19 0.0000 122.92 56.2112 235. 96 55.0450 80.57 83.1461 123.07 55.0261 238.63 58.3065 81. 00 97.4491 265.00 65.8437 238. 98' 0.0000 81. 07 97.4610 125.81 88.8320 240.99 58. 4196 81. 75 103.5772 127.23 86.5863 242.00 58.4679 83.79 90.3748 127.91 75.8284 244.70 58. 5968 84.00 88.8997 129.30 86.8118 252.40 0.0000 85.43 110.2537 131. 20 83.3925 252.80 50.8121 86.55 110.4550 133.02 62.9878 254.15 0.0000 86.79 110.4980 133.52 71.5101 256.23 45.4908 86.94 105.9827 136.00 86.3146 260.90 0.0000 Page 3679 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.2106 355.39 0.0000 584.27 13.1577 264.80 43.0470 356.01 33.6451 595.83 0.0000 265.00 44.8858 364.49 0.0000. 427.87 41.9583 268.22 74.3802 366.42 0.0000 602.52 0.0000 269.46 65.2596 372. 51 31.0309 604.72 16.5912 270.03 62.5284 375.05 34.0381 607.14 19.9292 271(.23 53.3814 377.52 32.6066 609.32 21. 0557 273.65 0.0000 356.01 33. 7205 610.33 21.0650 276.40 51.2792 388.16 23.8628 614.28 21.6550 277.37 40.6833 388.63 0.0000 618.01 17.7956 277.60 40.6896 391.69 28.8938 620.36 14.4727 278.00 40.7021 264.66 39.0579 621. 93 17.8242 279.20 34.7198 401.81 37.0790 630.19 0.0000 279.54 34.7290 402.40 37.0918 631.29 25.7206 279.70 34.7328 404.85 36.1392 633.25 21.2644 280.46 33.3625 410.95 26.1904 634.78 0.0000 283.69 40.8731 413.71 44.3903 635.95 16.8060 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 38.1339 423. 72 0.0000 645.85 22.4976 285.90 0.0000 427.09 25.4084 657.76 22.0391 287.50 40.9859 427.87 26.4359 657.90 0.0000 290.67 36.4117 433.94 29.5829 661.66 30.5629 293.27 0.0000 439.40 30.6927 664.57 0.0000 351.93 46.3660 453.88 23. 7113 '666. 33 0.0000 295. 96 46.3901 463.37 32 .1157 666.50 0.0000 879.38 33.8005 468.07 18.6929 667.71 0.0000 299.98 35.2440 473.00 0.0000 677.62 22.7799 300.09 35.2463 475.06 18.7592 685.70 0.0000 300.13 35.2470 476.78 23.9906 695.00 0.0000 301.36 35.2776 477.60 21.9135 696.49 29.8276 302.85 39.5519 482.18 20.9176 696. 51 29.8276 256.23 32.5269 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6565 306.78 47.5925 497.08 24.2325 697.49 20.6580 308.46 44.4335 505.52 22.2159 702.65 17.2485 311. 90 47.3806 507.63 0.0000 706.68 23.0322 316.51 37.0735 511. 00 20.1529 711. 68 28.8442 319.41 0.0000 514.00 19 .1191 720.70 0.0000 320.08 0.0000 514.00 19 .1191 721. 93 0.0000 321. 04 36.2327 520.40 24.5039 722.78 27.8047 323.87 44.8992 520.69 0.0000 722.91 27.8057 325.23 57.3694 522.65 0.0000 723.31 20. 8572 328.76 0.0000 527.90 0.0000 724 .19 10.4319 333.37 52.8706 528.26 17.1094 727.33 23.2088 333.97 36.9281 529.59 25.6797 733.00 23.2568 334.37 33.1860 529.87 0.0000 735.93 19.2070 338.28 55.9326 531. 02 0.0000 333.97 26.2061 338.32 55.9338 537.26 0.0000 739.50 0.0000 311. 90 40.5602 546.56 0.0000 747.24 15.7791 340.48 40.5602 552.55 20.5439 748.06 14.9066 340.55 0.0000 563.25 19.5564 752.31 16.6859 344.28 51. 3071 569.33 29.4126 753.82 0.0000 345.93 36.8249 946.00 27.7806 756.73 16.7120 351.06 38.8892 569.70 27.7838 756. 80 16.7126 351.93 38.9103 583.19 13.1519 884.68 9.8766 Page 3680 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.9424 1274.44 7.5930 1620.50 5.4907 766.42 21.1824 1001.03 8.5537 1621. 92 4.3938 766.84 21.1853 1002.74 8.5578 1678.03 0.0000 772. 60 0.0000 1004.73 8.5627 1690.97 5.5652 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.8051 778.90 17.7289 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 12.4835 1771.35 7.2293 785.37 23.0991 1038.76 0.0000 1791.20 0.0000 792.07 22.2618 631. 2 9 5.7759 1808.65 1.8194 794.95 14.2617 1048.07 0.0000 1810.72 0.0000 795.86 14.2661 1049.04 21.1917 1836.06 0.9141 810.06 17.0228 1050.41 15.4180 810.29 17.0239 1063.66 13.5394 344.28 17.0245 1077.00 0.0000 810.76 17.0268 1077.34 16.5020 815.77 0.0000 1085.87 15.5674 1048.07 0.0000 1093.63 15. 5996 832.01 17.1474 1099.45 15.6230 834.85 13. 5498 1112. 07 13.7163 835.71 15.3611 1112.84 15.6787 836.80 0.0000 1115. 54 18.8273 846.75 0.0000 1120.29 13.7454 846.77 20.8578 1120. 55 13.7462 856.80 0.0000 1221.41 13.7488. 860.56 9.1092 1129. 67 17.3218 871. 09 11.8816 1131. 51 0.0000 873.19 12.8041 1147.95 0.0000 875.33 0.0000 1173.23 13. 9333 879.38 17.4113 1177.95 20.9244 . 880.51 11.9173 1189.05 8.9923 883.24 10.2758 1204.77 10.0305 884.68 17.6238 1221.41 18.1285 889.28 14.7075 1231.02 18.1714 894.76 13.8121 1235.36 0.0000 898.04 12.9045 1238.28 18.2032 900.72 13.8377 1260.41 0.0000 903.28 12.9255 1271.87 8.1553 911.20 11.1061 1274.44 16.3203 912.08 11.1090 1274.54 16.3213 923.98 0.0000 1291. 59 8.1929 926.50 12.0875 1298.22 0.0000 929.11' 11.1665 1312 .11 0.0000 937.49 17.7255 1332.49 8.2705 944.13 0.0000 1362.66 0.0000 946.00 *16. 8349 1365.19 5.2072 949.00 14.9780 1368.63 0.0000 667.71 0.0000 1384 .*29 5.2295 962. 31 19.5482 1408.01 4.2053 964.08 7.5225 1457.56 0.0000 966 .17 7. 5271 1460.82 9.5696 911. 20 7.5332 1489.16 2.1392 968.97 7.5332 1505.03 4.2925 983.53 0.0000 1584.12 8.7231 984.45 0.0000 1596.21 0.0000 Page 3681of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:17:30.81
GEL Laboratories LLC *
2040* Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 23-NOV-2015 11:06:00 Acquisition date : 3-0CT-2016 09:16:17. Sample ID G405235035 Sample quantity 1.64073E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.73 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 1 1 8 8 8 0 0 0 6 6 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3682 of 5809 Energy 40.90 64.05* 68.49 75.06* 77.06 87.03 89.83 94.27 118. 51 128.82 154.68 163.47* 166.25 186.12* 209.48 224.37 238.59* 241. 74 270.13 295.21 300.05 338.80* 351.99* 424.65 462.97 510.89* 562.17 583.40* 597.97 609.40* 644.53 661.59 705.95 727. 69 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 20 13 29 75 157 43 46 59 29 20 20 28 22 44 73 47 353 70 . 49 129 26 72 181 21 22 25 17 89 15 138 8 9 *11 23 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 82 201 70 124 107 192 179 90 67 95 36 84 52 102 82 105 72 59 64 56 46 46 88 13 13 38 7 38 29 48 25 36 14 12 1. 43 1. 23 0.94 1.10
1.11 1. 33 1. 43 1. 25. 0.92 0.93 1. 34 2.01 1. 05 1. 06 1. 63 3.68 1.19 1. 44 1.19 0.88 1. 44 1. 05 . 1. 49 0.87 1. 05 2.74 1. 41 1.26 0.57 1. 36 2.18 0.60 0.95 2.01 81. 97 128.21 137. 07 150.20 154.20 174 .11 179.69 188.57 236.98 257.58 309.23 326.79 332.34 372.05 418.71 448.45 476.86 483.14 539.87 589.97 599.64 677.07 703.44 848.63 925.21 1020.98 1123.47 1165. 92 1195. 04 1217.88 1288.12 1322.22 1410.91 1454.37* 76 123 135 143 143 169 169 169 234 255 307 323 323 368 414 442 469 469 535 585 596 673 696 845 922 1014 1120 1161 1190 1213 1283 1319 1408 1451 8 5.54E-03 83.0 11 3.50E-03224.5 5 8.00E-03 47.8 16 2.lOE-02 28.5 16 4.35E-02 14.4 25 l.19E-02 51.6 25 l.27E-02 53.8 25 1.65E-02 39.4 7 7. 98E-03 51.1 7 5.55E-03 83.9 5 5. 54E-03 51. 3 12 7.71E-03 60.8 12 6.18E-03 58.4 10 1.22E-02 49.8 10 2.02E-02 26.4 13 1.32E-02 46.7 18 9.79E-02 6.8 18 1.95E-02 22.5 10 1. 35E-02 34. 2 10 3.58E-02 14.1 9 7.28E-03 50.2 10 2.00E-02 22.0 16 5.04E-02 13.8 7 5.80E-03 36.6 7 6.02E-03 35.6 14 6.83E-03 70.3 7 4.70E-03 35.6 10 2.48E-02 17.5 12 4.08E-03 81.4 12 3.83E-02 13.4 12 2.31E-03123.0 9 2.50E-03124.7 7 3.06E-03 64.0 8 6.27E-03 35.1 Fit 7.47E-01 5.71E+OO l.98E+00 1.56E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235035 Acquisition date 09:16:17 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 767.90 25 24 1.14 1534.78 1529 11 6.84E-03 43.9 36 0 786.15 16 8 1. 00 1571. 25 1567 10 4.52E-03 40.2 37 0 795.80 8 18 0.54 1590.56 1585 9 2.18E-03107.6 38 0 806.45 7 12 1.17 1611. 85 1605 9 l.95E-03100.0 39 0 821.53 18 5 3.01 1642.01 1637 11 4.86E-03 34.8 40 0 860.72 19 11 1. 08 1720.37 1715 11 5.28E-03 40.9 41 0 911.09* 88 6 1. 57 1821.10 1814 13 2.44E-02 12.5 42 3 965.06 37 7 2.28 1929.05 1921 22 1. 03E-02 22.4 1.49E+00 43 3 969. 50* 40 6" 1. 82 1937.94 1921 22 l.lOE-02 20.6 44 0 1121.12* 29 28 0.63 2241.23 2232 16 7.94E-03 45.9 45 0 1137. 59 7 2 1. 41 2274.18 2271 7 1. 96E-03 49.2 46 0 1378.42 15 6 1. 62 2756.10 2749 11 4.03E-03 40.9 47 0 1406.85* 10 0 1. 49 2813.00 2806 11 2.75E-03 35.8 48 0 1460.88* 335 3 2.07 2921.16 2913 15 9.30E-02 5.7 49 0 1501.18 7 2 1. 36 3001. 84 2998 7 2.04E-03 47.4 50 0 1764.68* 27 0 2.61 3529.43 3522 13 7.45E-03 20.7 Flag: "*" = Peak area was modified by background subtraction Page 3683 of 5809 VMS.Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:17:33 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 11:06:00 G405235035 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:16:17 164.07 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type* Abundance limit SOLID GAMMA33 . 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3684 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74 .'82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio. Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.73 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page* : 2 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.134E+OO 1.233E+Ol 1. 233E+Ol* 11. 33 OK CD-109 88.03 3.70* 4.887E+OO 5.956E-01 9.559E-01 255.58 OK SN-126 64.28 9.60 2.549E+OO 3.248E-01 3.248E-01 448.91 OK 86.94 8.90 4.887E+OO 2.476E-01 2.476E-01 255.58 OK 87.57 37.00* 4.887E+OO 5.956E-02 5.956E-02 255.58 OK BA-137M 661.66 89.90* 2 .115E+OO 2. 331E-02 2.378E-02 249.44 OK CS-137 661.66 85.10* 2 .115E+OO 2.462E-02 2.512E-02 249.44 OK CE-139 165.86 80.00* 5.922E+OO 2.700E-02 l.319E-01 116.79 OK TL-208 277.37 6.60 4.258E+OO Line Not Found Absent 583.19 85.00* 2.334E+OO 2.253E-01 2.253E-01 OK 860.56 12.50 1.727E+OO 4.197E-01 4.197E-01 81. 71 OK BI-212 727.33 6.67* 1. 965E+OO 8.389E-01 8.389E-01 70.29 OK 785.37 1.10 1. 851E+OO 3.852E+OO 3.852E+OO 80.37 OK 1620.50 1. 47 1.036E+oo. Line Not Found Absent PB-212 74.82 10.28 3.825E+OO 6.676E-01 6.676E-01 io4.28 OK 77 .11 17.10 4.028E+OO 1. 410E+OO 1. 410E+OO 28.90 OK 238.63 43.60* 4.776E+OO 9.366E-01 9.366E-01 13.53 OK 300.09 3.30 4.000E+OO 1. 071E+OO 1.071E+OO 100. 50. OK BI-214' 609.32 45.49* 2.255E+OO 6.677E-01 . 6. 679E-01 26.76 OK 1120.29 14.92 1.407E+OO 6.277E-01 6.279E-01 91. 79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 OK PB-214 74.82 5.80 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.028E+OO 2.485E+OO 2.486E+00 28.90 OK 87.09 3.41 4.892E+00 Line Not Found <<INT Reject 242.00 7.25 4. 727E+OO Line Not Found <<INT Reject 295.22 18.42 4.052E+OO 9.326E-01 9.330E-01 28.15 OK 351. 93 35.60* 3.512E+OO 7.685E-01 7.688E-01 27.69 OK. RN-222 609.32 45.49* 2.255E+OO 6.677E-01 6.679E-01 26.76 OK 1120.29 14.92 l.407E+00 6.277E-01 6.279E-01 91. 79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 OK RA-224 240.99 4.10* 4. 731E+OO 3.453E-01 3.453E-01 292. 72 OK RA-226 609.32 45.49* 2.255E+OO 6.677E-01 6.679E-01 26. 76 OK 1120. 29 14.92 1.407E+OO 6.277E-01 6.279E-01 91.79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.624E+OO 9.380E-01 9.380E-01 44.00 OK 794.95 4.25 l.834E+OO 4.858E-01 4.858E-01 215.11 OK 835.71 1. 61 1.766E+OO Line Not Found .Absent 911. 20 25.80* l.653E+OO 9.736E-01 9.736E-01 25.07 OK 968. 97 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.624E+OO 9.380E-01 9.380E-01 44.00 OK 794.95 4.25 1. 834E+00 4.858E-01 4.858E-01 215.11 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* l.653E+OO 9.736E-01 9.736E-01 25.07 OK 968.97 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 OK TH-228 74.82 10.28 3.825E+00 6.676E-01 6.676E-01 104.28 OK 77 .11 17.10 . 4. 028E+OO l.410E+OO l.410E+OO 28.90 OK 238.63 43.60* 4.776E+OO 9.366E-01 9.366E-01 13.53 OK Page 3685 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.000E+OO 1.071E+OO l.071E+OO 100.50 OK TH-230 609.32 45.49* 2.255E+OO 6.677E-01 6.677E-01 26.76 OK 1120.29 14.92 l.407E+OO 6.277E-01 6.277E-01 91.79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent 301.36 5.35* 4.000E+OO 6.604E-01 6.604E-01 100.50 OK TH-232 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.624E+OO 9.380E-01 9.380E-01 44.00 OK 835. 71 1. 61 1. 766E+OO Line Not Found Absent 911. 20 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 OK 968. 97 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 OK U-234 609.32 45.49* 2.255E+OO 6.677E-01 6.677E-01 26. 76 OK 1120.29 14.92 l.407E+OO 6.277E-01 6.277E-01 91. 79 OK 1764;49 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 OK U-235 89. 96 3.47 5.083E+00 1.587E+OO 1.587E+OO 107.70 OK* 93.35 5.60 5.355E+OO 1.203E+OO 1.203E+OO 78.78 OK 143.76 10. 96* 6.181E+OO Line Not Found Absent 163.33 5.08 5.962E+OO 5.276E-01 5.276E-01 121.65 OK 185.72 57.20 5.611E+OO 7.762E-02 7:762E-02 99.67 OK 205.31 5.01 5.295E+OO Line Not Found Absent AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.825E+OO 1. 021E-01 l.021E-01 104.28 OK ANH-511 511. 00 100.00* 2.593E+OO 4.819E-02 4.819E-02 140.62 OK Flag: "*" Key line Page 3686 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:34.08 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR.AND SAMPLE DATA *
*
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l * *Acquisition date 3-0CT-2016 09:16:17 Sensitivity : 3.000 ' *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
Sample date 23-NOV-2015 11:06:00 Analyst initials: MXRl *
Sample ID G405235035 Sample Quantity l.6407E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 233E+Ol l.369E+OO CD-109 9.559E-01 2.394E+OO SN-126 5.956E-02 l.492E-01 BA-137M 2.378E-02 5.812E-02 CS-137 2.512E-02 6.140E-02 CE-139 l.319E-01 l.510E-01 TL-208 2.253E-01 7.729E-02 BI-212 8.389E-01 5.778E-01 PB-212 9.366E-01 l.241E-01 BI-214 6.679E-01 1. 752E-01 PB-214 7.688E-01 2.086E-01 RN-222 6.679E-01 1. 752E-01 RA-224 3.453E-01 9.906E-01 RA-226. 6.679E-01 l.752E-01 AC-228 9.736E-01 2.392E-01 RA-228 9.736E-01 2.392E-01 TH-228 9.366E-01 1. 241E-01 TH-230 6.677E-01 1. 751E-01 PA-231 6.604E-01 6.504E-01 TH-232 9.736E-01 2.392E-01 U-234 6.677E-01 1. 751E-01 U-235 4.831E-02 l.566E-01 AM-243 l.021E-01 l.044E-01 ANH-511 4.819E-02 6.640E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3687 of 5809 Key-Line Activity (pCi/GRAM 2.251E+00 l.208E-02 O.OOOE+OO -l.033E-02 -8.621E-02 O.OOOE+OO K.L. Cnt Uncert (1. 96-sigma) l.393E+Ol 3.855E-02 1. 960E+41 l.972E-02 3.710E-01 2.508E+04 MDA (pCi/GRAJY,l 5.330E-01 1. 911E+OO l.198E-01 6.443E-02 6.806E-02 l.884E-01 6.325E-02 l.017E+00 8.057E-02 l.140E-01 l.131E-01 l.140E-01 8.635E-01 l.140E-01 1. 926E-01 1. 926E-01 8. 057E-02* l .139E-01 7.170E-01 1. 92 6E-01 l .139E-01 3. llOE-01 8.539E-02 4.704E-02 MDA (pCi/GRAM 2.804E+Ol 8.363E-02 0.000E+OO 3.617E-02 7.030E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 0.000E+OO 4.792E+02 O.OOOE+OO SHORT HLIF MN-54 3.984E-03 6.251E-02 1.212E-01 NOT IDENT. C0-56 -1.071E-02 4.907E-01 9.465E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 4.350E-04 4.306E-02 7.707E-02 NOT IDENT. C0-58 7.502E-01 5.416E-01 1. 311E+OO NOT IDENT. FE-59 3.728E+OO 8.452E+OO 1. 799E+Ol NOT IDENT. C0-60 -l.357E-02 3.719E-02 7.075E-02 NOT IDENT. ZN-65 6.778E-03 1.415E-01 2.661E-01 NOT IDENT. GE-68 2.070E+OO 2.329E+OO 5 .-2 64E+OO NOT IDENT. AS-73 -2.675E+OO 1.0lOE+Ol 2.023E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.073E+04 O.OOOE+OO SHORT HLIF SE-75 -8.750E-02 2.047E-01 3.577E-01 NOT IDENT. BR-77 O.OOOE+OO l.823E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8. 272E+02 O.OOOE+OO SHORT HLIF RB-83 -7.747E-02 5.927E-01 l.167E+OO NOT IDENT. KR-85 5. 968E+OO 6.150E+OO 1. 2 67E+Ol NOT IDENT. SR-85 7.378E-01 7.613E-01 1.568E+OO NOT IDENT. RB-86 O.OOOE+OO 4.446E+04 O.OOOE+OO SHORT HLIF Y-88 3.215E-02 2.316E-01 5.087E-01 NOT IDENT. Y-91 l.332E+02 5.795E+02 1.202E+03 NOT IDENT. NB-94 2.102E-02 3.131E-02 6.092E-02 NOT IDENT. NB-95 l.323E-01 9. 351E-01 1.693E+OO NOT IDENT. NB-95M 1. 782E+OO 2.459E+00 4.848E+OO NOT IDENT. ZR-95 -2.318E-01 1.610E+OO 3.050E+OO NOT IDENT. NB-97 O.OOOE+OO 1.382E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO 7. l 75E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -9.528E-04 3.162E-02 5.582E-02 NOT IDENT. RH-102 3.375E-03 4.645E-02 9.395E-02 FAIL ABUN RU-103 2.025E-01 6.227E+OO 1.250E+Ol FAIL ABUN RH-106 -3.279E-01 4.390E-01 7.670E-01 NOT IDENT. RU-106 -3.279E-01 4.390E-01 7.670E-01 NOT IDENT. AG-108M -4.500E-03 2. 2 60E-02 4.435E-02 NOT IDENT. AG-llOM 4.260E-02 8. 491E-02 l.825E-01 FAIL ABUN SN-113 -2.090E-02 2.126E-01 4.222E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO 1. 735E+05 O.OOOE+OO SHORT HLIF TE-123M -2.574E-02 l.175E-01 2.185E-01 NOT IDENT. SB-124 1. 221E+OO l.653E+00 4.539E+00 FAIL ABUN SB-125 6.022E-02 1.0lOE-01 1.967E-01 FAIL ABUN TE-125M 1.209E+02 2.995E+02 5.946E+02 NOT IDENT. I-126 O.OOOE+OO 1.922E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.329E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.768E+23 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 1.576E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.305E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.843E+27 O.OOOE+OO SHORT HLIF BA-133 -9.869E-03 3.413E-02 5:972E-02 NOT IDENT. I-133 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.225E-02 6.798E-02 9.161E-02 FAIL ABUN CS-135 -l.342E-02 1.440E-01 2.388E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.578E+05 O.OOOE+OO SHORT HLIF BA-140 O.OOOE+OO 2.224E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 8.643E+05 O.OOOE+OO SHORT HLIF CE-141 -1.916E+Ol 2.777E+Ol 4.947E+Ol NOT IDENT. CE-143 O.OOOE+OO l.256E+41 O.OOOE+OO SHORT HLIF CE-144 5.756E-02 2.980E-01 5.831E-01 NOT IDENT. PM-144 -4.602E-02 4.686E-02 7. 6.68E-02 NOT IDENT. PR-144 -4. OOOE+O.O 4.108E+OO 6.735E+OO NOT IDENT. PM-146 l.194E-02 3.579E-02 7. 471E-02 NOT IDENT. ND-147 O.OOOE+OO 6.337E+07 O.OOOE+OO SHORT HLIF PM-147 4.642E+Ol 7 .112E+02 l.284E+03 NOT IDENT. PM-149 O.OOOE+OO 9.353E+40 O.OOOE+OO SHORT HLIF EU-150 -6.931E-03 2.125E-02 3.955E-02 FAIL ABUN EU-152 -l.637E-02 7. 724E-02 l.458E-01 FAIL ABUN GD-153 2.156E-02 ' 1. 643E-01 2.997E-01 FAIL ABUN EU-154 3.822E-02 9.576E-02 2. 096E-01 NOT IDENT. EU-155 4.946E-02 l.059E-Ol 2 .114E-01 FAIL ABUN TB-160 8.292E-01 2.053E+OO 4.211E+OO FAIL ABUN H0-166M 2.036E-02 4.253E-02 9.148E-02 NOT IDENT. TM-171 2.748E-01 2.331E+Ol 4.782E+Ol NOT IDENT. HF-172 1.131E-01 2.229E-01 4 .148E-0*1 FAIL ABUN LU-172 3.522E-02 6.618E-02 l.466E-01 FAIL ABUN LU-176 -9.939E-03 1.988E-02 3.838E-02 FAIL ABUN HF-181 -1.409E+OO 4.890E+OO 9.378E+OO NOT IDENT. Page 3688 of 5809 TA-182 -1.830E-03 8.743E-01 1. 762E+OO FAIL ABUN RE-183 -2.048E-01 3.389E+OO 6.845E+OO FAIL ABUN RE-184 -3.690E+OO 3.036E+Ol 5.885E+Ol NOT IDENT. W-188 -8.986E+Ol l.154E+02 l.901E+02 FAIL ABUN IR-192 8.661E-02 4.353E-01 8.989E-01 FAIL ABUN HG-203 -5.679E-01 2.352E+OO 4.686E+OO NOT IDENT. BI-207 1. 311E-02 4. 401E-02 9.336E-02 FAIL ABU_N
PB-210 3. 521E-01 4.807E+OO 9. 913E+OO NOT IDENT. BI-211 0.000E+OO 5.746E-01 7.122E-01 FAIL ABUN PB-211 2.560E-01 5.632E-01 1.182E+OO NOT IDENT. RN-2:)_9 4.562E-02 2.849E-01 5.887E-01 FAIL ABUN RA-223 1.418E-02 4.697E-01 9.545E-01 FAIL ABUN AC-227 4.818E-02 2.123E-01 3. 996E-01 FAIL ABUN TH-227 4.818E-02 2.123E-01 3. 996E-01 FAIL ABUN TH-229 4.153E-01 7.369E-01 FAIL ABUN TH-231 1. 418E-02 4.697E-01 9.545E-01 FAIL ABUN PA-233 -2.122E-02 4.464E-02 8.664E-02 FAIL ABUN PA-234 l.512E-01 2.361E-01 5.108E-01 FAIL ABUN PA-234M 3.563E+OO 4.139E+OO 9.064E+OO FAIL ABUN TH-234 8.427E-01 3.707E+OO 2.795E+OO FAIL ABUN NP-237 -2.122E-02 4.464E-02 8.664E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 8.427E-01 3.707E+OO 2.795E+OO FAIL ABUN NP-239 -6.923E-03 2. llOE-01 3.769E-01 NOT IDENT. PU-239 2.999E+02 4.929E+02 5.588E+02 FAIL ABUN AM-241 1.337E-02 1.443E-01 2.730E-01 NOT IDENT. CM-243 -1.303E-02 9.263E-02 1.774E-01 NOT IDENT. BK-247 -8:280E-03 6. 511E-02 l.181E-01 'FAIL ABUN CM-247 -5.190E-03 2.683E-02 5.300E-02 NOT IDENT. CF-249 -l.475E-02 3.155E-02 6.008E-02 NOT IDENT. CF-251 -2.099E-02 9.731E-02 l.793E-01 NOT IDENT. Page 3689 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:17:31.58 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide *Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 326 *10.66* 1.134E+OO l.233E+Ol 1.233E+Ol 11. 33 CD-109 88.03 58 3.70* 4.887E+OO 1.455E+OO 2.335E+OO 103.28 SN-126 64.28 17 9.60 2.549E+OO 3.248E-01 3.248E-01 448.91 86.94 58 8.90 4.887E+00 6.049E-01 6.049E-01 103.28 87.57 58 37.00* 4.887E+OO 1.455E-01 l.455E-01 103.28 BA-137M 661.66 10 89.90* 2 .115E+OO 2. 331E-02 2.378E-02 249.44 CS-137 661. 66 . 10 85.10* 2 .115E+OO 2.462E-02 2.512E-02 249.44 CE-139 165.86 28 80.00* 5.922E+OO 2.700E-02 1.319E-01 116.79 TL-208 277.37 ------6.60 4.258E+OO ------Line Not Found ------583.19 98 85.00* 2.334E+OO 2.253E-01 2.253E-01 35.00 860.56 20 12.50 1. 727E+OO 4.197E-01 4.197E-01 81. 71 BI-211 72. 87 ------1. 23 3.591E+OO ------Line Not Found ------351. 06 210 *12. 92* *3. 512E+OO 2 .118E+OO 2 .118E+OO 27.69 BI-212 727. 33 24 6.67* 1. 965E+OO 8.389E-01 8.389E-01 70.29 785.37 17 1.10 1. 851E+OO 3.852E+OO 3.852E+OO 80.37 1620.50' ------1. 47 1.036E+OO ------Line Not Found ------PB-212 74.82 103 10.28 3.825E+00 l.194E+OO 1.194E+OO 56.98 77 .11 212 17.10 4.028E+OO 1.410E+OO 1.410E+OO 28.90 238.63 426 43.60* 4.776E+00 9.366E-01 9.366E-01 13.53 300.09 31. 3. 30 . 4.000E+OO 1. 071E+OO 1. 071E+OO 100.50 BI-214 609.32 150 45.49* 2.255E+00 6.677E-01 6.679E-01 26. 76 1120.29 29 14.92 1.407E+00 6.277E-01 6.279E-01 91. 79 1764.49 25 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 PB-214 74.82 103 5.80 3.825E+OO 2 .116E+00 2. ll 7E+00 56.98 77 .11 212 9.70 4.028E+OO 2.485E+OO 2.486E+OO 28.90 87.09 58 3.41 4.887E+OO 1.579E+OO 1.579E+OO 103.28 242.00 85 7.25 4.731E+OO l.128E+00 1.128E+OO 45.02 295.22 152 18.42 4.052E+OO 9.326E-01 9.330E-01 28.15 351. 93 210 35.60* 3.512E+OO 7.685E-01 7.688E-01 27.69 RN-222 609.32 150 45.49* 2.255E+OO 6.677E-01 6.679E-01 26.76 1120. 29 29 14.92 l.407E+OO 6.277E-01 6.279E-01 91. 79 1764.49 25 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 RA-224 240.99 85 4.10* 4.731E+OO l.994E+OO 1.994E+OO 45.02 RA-226 609.32 150 45.49* 2.255E+OO 6.677E-01 6.679E-01 26. 76 1120.29 29 14.92 1. 407E+OO 6.277E-01 6.279E-01 91. 79 1764.49 25 15.30 9. 591E-01 7.932E-01 7.935E-01 41. 37 AC-228 105.21 ------1.10 5.839E+00 ------Line Not Found ------338.32 84 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 794.95 8 4.25 1.834E+00 4.858E-01 4.858E-01 215 .11 835. 71 ------1. 61 1. 766E+OO ------Line Not* Found' ------911. 20 91 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 968. 97 41. 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 RA-228 105,.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 84 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 794.95 8 4.25 l.834E+OO 4.858E-01 4.858E-01 215 .11 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911. 20 91 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 Page 3690 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma: Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 41 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 TH-228 74.82 103 10.28 3.825E+OO 1.194E+OO 1.194E+OO 56.98 77 .11 212 17.10 4.028E+OO 1.410E+OO 1.410E+OO 28.90 238.63 426 4.776E+OO 9.366E-01 9.366E-01 13. 53 300.09 31 3.30 4.000E+OO 1.071E+OO 1. 071E+OO 100.50 TH-230 609.32 150 45.49* 2.255E+OO 6.677E-01 6.677E-01 26.76 1120.29 29 14.92 1.407E+OO 6.277E-01 6.277E-01 91. 79 1764.49 25 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 31 5.35* 4.000E+OO 6.604E-01 6.604E-Oi 100.50 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 84 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 835.71 ------1. 61 1.766E+OO ------Line Not Found ------911.20 91 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 968. 97 41 . 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 U-234 609.32 150 45.49* 2.255E+OO 6.677E-01 6.677E-01 26. 76 1120.29 29 14.92 l.407E+00 6.277E-01 6.277E-01 91. 79 1764.49 25 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 U-235 89. 96 61 3.47 5.083E+OO 1.587E+OO 1.587E+OO 107.70 93.35 79 5.60 5.355E+OO 1.203E+OO 1.203E+OO 78.78 143.76 ------10. 96* 6 .181E+OO ------Line Not Found ------163.33 35 5.08 5. 962E+OO 5.276E-01 5.276E-01 121.65 185.72 54 57.20 . 5. 611E+OO 7.762E-02 7.762E-02 99,67 205.31 ------5.01 5.295E+OO ------Line Not Found ------AM-243 43.53 ------5.90 2. 461E-01 ------Line Not Found ------74.66 103 67.20* 3.825E+OO 1. 826E-01 1. 826E-01 56.98 ANH-511 511. 00 27 100.00* 2.593E+OO 4.819E-02 4.819E-02 140.62 Flag: "*" Key line Page 3691of5809 Summary of Nuclide Activity Sample ID : G405235035 . Acquisition date Page : 3 3-0CT-2016 09:16:17 Total number of lines in spectrum 50 Number of unidentified lines 8 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-139 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 Ac:...228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Hlif e 1. 25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 137.64D 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y l.41E+l0Y 1600. OOY 1600. OOY 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 61 1. 00 1. 02 1. 02 4.88 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.233E+Ol 1.455E+OO l.455E-01 2.331E-02 2.462E-02 2.700E-02 2.253E-01 2 .118E+OO 8.389E-01 9.366E-01 6.677E-01 7.685E-01 6.677E-01 1.994E+OO 6.677E-01 9.736E-01 9.736E-01 9.366E-01 6.677E-01 6.604E-01 9.736E-01 6.677E-01 7.762E-02 1.826E-01 4.819E-02 2.905E+Ol 2.905E+Ol Decay Corr pCi/GRAM 1.233E+Ol 2.335E+OO l.455E-01 2.378E-02 2.512E-02 l.319E-01 2.253E-01 2 .118E+OO 8.389E-01 9.366E-01 6.679E-01 7.688E-01 6.679E-01 1. 994E+OO 6.679E-01 9.736E-01 9.736E-01 9.366E-01 6.677E-01 6.604E-01 9.736E-01 6.677E-01 7.762E-02 1.826E-01 4.819E-02 3.004E+Ol 3.004E+Ol 84.00% Decay Corr 2-Sigma Error 0.140E+Ol 2.412E+OO 1.503E-01 5. 931E-02 6.265E-02 1.540E-01 0.789E-01 0.586E+00 5.896E-01 1.267E-01 1.787E-01 2.129E-01 1. 787E-01 0.898E+OO l.787E-01 2.441E-01 2. 441E-01 1. 267E-01 1.787E-01 6.637E-01 2. 441E-01 l.787E-01 7.737E-02 l.041E-01 6.776E-02 Manually accepted 2-Sigma %Error 11. 33 103.28 103.28 249.44 249.44 116.79 35.00 27.69 70.29 13. 53 26.76 27.69 26.76 45.02 26.76 25.07 25.07 13.53 26. 76 100.50 25.07 26.76 99.67 56.98 140.62 Flags: "K" Keyline not found "E" = M.anually edited "A" = Nuclide specific abn. limit Page 3692 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235035 Acquisition date : 3-0CT-2016 09:16:17 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 40.90 29 118 1. 43 81.97 76 8 5.54E-03 **** 1.12E-01 0 68.49 39 96 0.94 137.07 135 5 8.00E-03 95.7 3.09E+OO T 0 118. 51 37 87 0.92 236.98 234 7 7.98E-03 **** 6.14E+OO T 0 128.82 26 123 0.93 257.58 255 7 5.55E-03 ***** 6.22E+OO T 0 154.68 25 46 1. 34 309.23 307 5 5.54E-03 **** 6.08E+OO T 0 209.48 89 101 1. 63 418.71 414 10 2.02E-02 52.7 5.23E+OO T 0 224.37 58 127 3.68 448.45 442 13 1.32E-02 93.3 4.99E+OO 0 270.13 58 77 1.19 539.87 535 10 1. 35E-02 68.3 4.35E+OO T 0 424.65 24 15 0.87 848.63 845 7 5.80E-03 73.3 3.0lE+OO T 0 462.97 24 15 1. 05 925.21 922 7 6.02E-03 71. 2 2.81E+OO T 0 562.17 19 8 1. 41 1123.47 1120 7 4.70E-03 71. 2 2.40E+OO T 0 597.97 16 32 0.57 1195. 04 1190 12 4.08E-03 **** 2.29E+OO 0 644.53 9 27 2.18 1288.12 1283 12 2.31E-03 **** 2.16E+OO T 0 705.95 12 15 0.95 1410.91 1408 7 3.06E-03 **** 2.0lE+OO T 0 767.90 26 26 1.14 1534.78 1529 11 6.84E-03 87.8 1. 88E+OO T 0 806.45 7 13 1.17 1611. 85 1605 9 1. 95E-03 ****. 1. 82E+OO 0 821. 53 18 5 3.01 1642.01 1637 11 4.86E-03 69.6 1.79E+OO 3 965.06 38 7 2.28 1929.05 1921 22 l.03E-02 44.8 l.58E+00 T 0 1137. 59 7 2 1. 41 2274.18 2271 7 1. 96E-03 98.5 1. 39E+OO 0 1378.42 14 5 1. 62 2756.10 2749 11 4.03E-03 81. 7 1.19E+OO 0 1406.85 10 0 1. 49 2813.00 2806 11 2.75E-03 71. 6 1.17E+OO T 0 1501.18 7 2 1. 36 3001.84 2998 7 2.04E-03 9.4. 7 l. llE+OO Flags: "T" = Tentatively associated Page 3693 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:46.92 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l *
Acquisition date 3-0CT-2016 09:16:17 Sensitivity : 3.000 *
Detector ID
GAM33 Energy tolerance: 1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
Sample date 23-NOV-2015 11:06:00 Nuclide Library : SOLID *
Sample ID G405235035 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.6407E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION. INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File : DKA100 :'[CANBERRA. GAMMA] EFF GAM33 CAN. CNF*; 8
Combined Critical Level Report NOTE: Not all "identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-139 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.148E-01 8. 963E-01 5.620E-02 2.878E-02 3.041E-02 8.734E-02 2.839E-02 4.600E-01 3.713E-02 5.074E-02 5.135E-02 5.074E-02 3.979E-01 5.074E-02 8.142E-02 8.142E-02 3.713E-02 5. 072E-02 3.278E-01 8.142E-02 5. 072E-02 l.457E-01 4.003E-02 2.104E-02. ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3694 of 5809 Le (pCi/GRAM 1.265E+Ol 3.559E-02 O.OOOE+OO 1.143E-02. 3.005E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-ll5 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3695 of 5809 5.335E-02 4. ll9E-01 O.OOOE+OO 3.571E-02 5.784E-01 7. 941E+OO
2.964E-02 l. ll5E-01 2.330E+OO 9.277E+OO O.OOOE+OO l.633E-Ol O.OOOE+OO O.OOOE+OO 5.130E-Ol 5.726E+OO 7.087E-01 O.OOOE+OO 2.019E-01 5. 251E+02 2.729E-02 7.441E-01 2.258E+OO l.339E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.602E-02 4.085E-02 5.553E+OO 3. 3llE-01 3. 3llE-01 1. 97 5E-02 7.885E-02 l.904E-01 O.OOOE+OO O.OOOE+OO l.OlOE-01 l.777E+OO 8.936E-02 2.786E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.00CiE+OO 2.667E-02 O.OOOE+OO 4.039E-02 l.lOOE-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.289E+Ol O.OOOE+OO 2.707E-01 3.257E-02 2.862E+OO 3.347E-02 O.OOOE+OO 5.942E+02 O.OOOE+OO 1. 789E-02 6.575E-02 l.394E-01 8. 968E-02 9.952E-02 l.851E+OO 3.983E-02 2.207E+Ol l.943E-01 6.369E-02 1. 741E-02 4.180E+OO 7.619E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF . NOT I DENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF *NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3696 of 5809 3.169E+OO 2.465E+Ol 8.598E+Ol 4.098E-01 2.138E+OO 4.081E-02 4.604E+OO 3.419E-01 5.360E-01 2.631E-01 4.337E-01 l.846E-01 1. 846E-01 3.411E-01 4.337E-01 3.894E-02 2.226E-01 4.043E+OO 1. 322E+OO 3.894E-02 O.OOOE+OO 1.322E+OO 1.746E-01 2.624E+02 1. 268E-01 8.303E-02 5.409E-02 2.364E-02 2.700E-02 8.297E-02 FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:52.20 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l *
Acquisition date 3-0CT-2016 09:16:17 Sensitivity : 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
Sample date 23-NOV-2015 11:06:00 Nuclide Library : SOLID *
Sample ID G405235035 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity 1.6407E+02 GRAM *
Quantity Err(%) 1.2190E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* . * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *'
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
Combined Activity-MDA Report Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 BA-137M CS-137 CE-139 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 1.233E+Ol 9.559E-01 5.956E-02 2.378E-02 2.512E-02 1.319E-01 2.253E-01 8.389E-01 9.366E-01 6.679E-01 7.688E-01 6.679E-01 3.453E-01 6.679E-01 9.736E-01 9.736E-01 9.366E-01 6.677E-01 6.604E-01 9.736E-01 6.677E-01 4.831E-02 l.021E-01 4.819E-02 Act Error ( 1 . 96-sigma ) 1.512E+OO 2.402E+OO 1. 496E-01 5.813E-02 6.141E-02 l.533E-01 7.787E-02 5.794E-01 1.336E-01 1. 775E-01 2. llOE-01 1. 775E-01 9. 966E-01 1. 775E-01 2.443E-01 2.443E-01 1.336E:....01 l.774E-01 6.655E-01 2.443E-01 1.774E-01 l.566E-01 1. 051E-01 6.643E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3697 of 5809 Key-Line Activity (pCi/GRAM 2.251E+OO 1.208E-02 1. OOOE+41 -1.033E-02 -8.621E-02 * -1. 048E+04 K.L Act error ( 1 . 96-sigma) 1.393E+Ol 3.855E-02 7.360E+41 l.973E-02 3.710E-01 2.509E+04 TPU ( 1.*96-sigma) 1.512E+OO 2.402E+OO l.496E-01 5.813E-02 6 .141E-02 1.533E-01 7.787E-02 5.794E-01 1. 336E:....01 1. 775E-01 2. llOE-01 1. 775E-01 9. 966E-01 1. 775E-01 2.443E-01 2.443E-01 1.336E-01 1.774E-01 6.655E-01 2.443E-01 1.774E-01 1. 566E-01 1. 051E-01 6.643E-02 TPU ( 1. 96-sigma) 1.396E+Ol 3.893E-02 O.OOOE+OO 2.027E-02 3.730E-01 2.553E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -4.693E+02 4.796E+02 5.242E+02 SHORT HLIF MN-54 3.984E-03 6.251E-02 6.254E-02 NOT IDENT. C0-56 -l.071E-02 4.907E-01 4.907E-01 NOT IDENT. MN-56 -1. 000E+41 3.439E+42 0.000E+OO SHORT HLIF C0-57 4.350E-04 4.306E-02 4.306E-02 NOT IDENT. C0-58 7.502E-Ol 5.425E-01 6.393E-01 NO!I' IDENT. FE-59 3. 728E+OO 8.456E+OO 8.622E+OO NOT IDENT. C0-60 -l.357E-02 3.719E-02 3.769E-02 NOT I DENT.
ZN-65 6.778E-03 l.415E-01 1;415E-01 NOT IDENT. GE-68 2.070E+OO 2.330E+OO 2.510E+OO NOT IDENT. AS-73 -2.675E+OO 1. OllE+Ol l.018E+Ol NOT IDENT. AS-74 2.573E+03 1. 073E+04 l.079E+04 SHORT HLIF SE-75 -8.750E-02 2.048E-01 2.086E-01 NOT IDENT. BR-77 l.376E+40 l.251E+41 O.OOOE+OO SHORT HLIF SR-82 1. 210E+Ol 8.272E+02 8. 272E+02 SHORT HLIF RB-83 -7.747E-02 5.928E-01 5.938E-01 NOT IDENT. KR-85 5.968E+OO 6.155E+OO 6.717E+OO NOT IDENT. SR-85 7.378E-01 7.619E-01 8.314E-01 NOT IDENT. RB-86 4.167E+04 4.450E+04 4.831E+04 SHORT. HLIF Y-88 3.215E-02 2.316E-01 2.321E-01 NOT. IDENT. Y-91 l.332E+02 5.795E+02 5.826E+02 NOT IDENT. NB-94 2.102E-02 3.132E-02 3. 272E-02 NOT IDENT. NB-95 l.323E-01 9. 351E-01 9.370E-01 NOT IDENT. NB-95M l.782E+OO 2.463E+OO 2.591E+OO NOT IDENT. ZR-95 -2.318E-01 1. 610E+OO l.614E+OO NOT IDENT. NB-97 l.OOOE+41 l.383E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 2.944E+42 O.OOOE+OO SHORT HLIF M0-99 -4.416E+33 7.182E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 8.984E+41 O.OOOE+OO SHORT HLIF RH-101 -9.528E-04 3 .162E...:.02 3.162E-02 NOT IDENT. RH-102 3.375E-03 4.645E-02 4.648E-02 FAIL ABUN RU-103 2.025E-01 6.227E+OO 6.227E+OO FAIL ABUN RH-106 -3.279E-01 4.394E-01 4.636E-01 NOT IDENT. RU-106 -3.279E-01 4.394E-01 4.636E-01 NOT IDENT. AG-108M -4.500E-03 2.260E-02 2.269E-02 NOT IDENT. AG-llOM 4.260E-02 8.494E-02 8.708E-02 FAIL ABUN SN-113 -2.090E-02 2.126E-01 2.128E-01 NOT IDENT. CD-115 5.774E+40 2.786E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -6.967E+04 l.737E+05 l.765E+05 SHORT HLIF TE-123M -2.574E-02 l.175E-01 . l.181E-01 NOT IDENT. SB-124 l.221E+OO l.654E+00 1. 743E+OO FAIL ABUN SB-125 6.022E-02 l.OlOE-01 1. 046E-01 FAIL ABUN TE-125M l.209E+02 2. 996E+02 3.045E+02 NOT IDENT. I-126 -l.058E+06 l.927E+06 l.986E+06 SHORT HLIF SB-126 -5. 671E+05 2.332E+06 2.346E+06 SHORT HLIF SB-127 8.054E+22 3.002E+23 O.OOOE+OO SHORT HLIF I-131 -7.539E+09 l.576E+l0 l.613E+l0 SHORT HLIF I-132 -1. OOOE+41 l.946E+42 O.OOOE+OO SHORT HLIF TE-132 -3.492E+27 9.955E+27 O.OOOE+OO SHORT HLIF BA-133 -9.869E-03 3.413E-02 3.442E-02 NOT IDENT. I-133 l.OOOE+41 3.751E+41 O.OOOE+OO SHORT HLIF CS-134 3.225E-02 6.799E-02 6.953E-02 FAIL ABUN CS-135 -l.342E-02 l.440E-01 l.441E-01 NOT IDENT. I-135 -l.OOOE+41 2.184E+42 O.OOOE+OO SHORT HLIF CS-136' -3.336E+05 4.593E+05 4.833E+05 SHORT HLIF BA-140 3.406E+05 2.224E+06 2.230E+06 SHORT HLIF LA-140 -1. 752E+05 8.643E+05 8.679E+05 SHORT HLIF CE-141 -l.916E+Ol 2.778E+Ol 2.910E+Ol NOT IDENT. CE-143 l.OOOE+41 l.261E+41 O.OOOE+OO SHORT HLIF CE-144 5.756E-02 2. 981E-01 2.992E-01 NOT IDENT. PM-144 -4.602E-02 4.695E-02 5.133E-02 NOT IDENT. PR-144 -4.000E+OO 4. lllE+OO 4.489E+OO NOT IDENT. PM-146 l.194E-02 3.580E-02 3.620E-02 NOT IDENT. ND-147 -2.038E+07 6.338E+07 6.404E+07 SHORT HLIF* PM-147 4.642E+Ol 7 .113E+02 7 .116E+02 NOT IDENT. PM-149 -l.OOOE+41 9.623E+40 O.OOOE+OO SHORT HLIF EU-150 -6. 931E-03 2.125E-02 2.148E-02 FAIL ABUN EU-152 -l.637E-02 7. 725E-02 7.760E-02 FAIL ABUN GD-153 2.156E-02 l.643E-01 l.646E-01 FAIL ABUN EU-154 3.822E-02 9.577E-02 9.731E-02 NOT IDENT. EU-155 4.946E-02 l.060E-01 l.083E-01 FAIL ABUN TB-160 8.292E-01 2.054E+OO 2.087E+OO FAIL ABUN H0-166M 2.036E-02 4.254E-02 4.352E-02 NOT IDENT. TM-171 2.748E-01 2.331E+Ol 2. 331E+Ol NOT IDENT. HF-172 l.131E-01 2.236E-01 2.294E-01 FAIL ABUN LU-172 3.522E-02 6.628E-02 6.816E-02 FAIL ABUN LU-176 * -9.939E-03 l.989E-02 2.039E-02 FAIL ABUN HF-181 -l.409E+OO 4.890E+OO 4. 931E+OO NOT IDENT. Page 3698 of 5809 TA-182 -1.830E-03 8.743E-01 8.743E-01 FAIL ABUN RE-183 -2.048E-01 3.389E+OO 3.391E+OO FAIL ABUN RE-184 -3.690E+OO 3.038E+Ol 3.042E+Ol NOT IDENT. W-188 -8.986E+Oi *l.158E+02 l.227E+02 FAIL ABUN IR-192 8.661E-02 4.353E-01 4. 371E-01 FAIL ABUN HG-203 -5.679E-01 2.352E+OO 2.366E+OO NOT IDENT. BI-207 1. 311E-02 4.401E-02 4 ..441E-02 FAIL ABUN PB-210 3.521E-01 4.807E+OO 4.809E+OO NOT'IDENT. BI-211 2 .118E+OO 5.822E-01 1.118E+OO FAIL ABUN PB-211 2.560E-01 5.633E-01 5.750E-01 NOT IDENT. RN-219 4.562E-02 2.850E-01 2.857E-01 FAIL ABUN RA-223 1.418E-02 4.697E-01 4.697E-01 FAIL ABUN AC-227 4.818E-02 2.124E-01 2.135E-01 FAIL ABUN TH-227 4.818E-02 2.124E-01 2.135E-01 FAIL ABUN TH-229 -2.067E-01 4.154E-01 4.257E-01 FAIL ABUN TH-231 1.418E-02 4.697E-01 4.697E-01 FAIL ABUN PA-233--2.122E-02 4.465E-02 4. 566E-02 FAIL ABUN PA-234 l.512E-01 2.927E-01 3.005E-01 FAIL ABUN PA-234M 3.563E+OO 4.141E+OO 4.442E+OO FAIL ABUN TH-234 8.427E-01 3.712E+OO 3. 731E+OO FAIL ABUN NP-237 -2.122E-02 4.465E-02 4.566E-02 FAIL ABUN NP-238 -1. OOOE+41 4.750E+41 O.OOOE+OO SHORT HLIF U-238 8.427E-01 3.712E+OO 3.731E+00 FAIL ABUN NP-239 -6.923E-03 2. llOE-01 2. llOE-01 NOT IDENT. PU-239 2.999E+02 4. 931E+02 5 .113E+02 FAIL ABUN AM-241 1.337E-02 l.443E-01 1.444E-01 NOT IDENT. CM-243 -l.303E-02 9.264E-02 9.282E-02 NOT IDENT. BK-247 -8.280E-03 6.513E-02 6.524E-02 FAIL ABUN CM-247 -5.190E-03 2.685E-02 2.695E-02 NOT IDENT. CF-249 -1.475E-02 3.157E-02* 3.227E-02 NOT IDENT. CF-251 -2.099E-02 9.734E-02 9.780E-02 NOT IDENT. ' Page 3699 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 43.6508 87.09 76.6525 136.47 51.5361 45.60 51.7159 87.57 76.7138 140.51 0.0000 46.54 55.6064 88.03 76.7721 143.76 50.8881 49.72 0.0000 88.34 76.8113 144.24 46.4899 51. 35 45.7623 88.47 76.8276 145.44 66.5085 51. 87 46.7719 89. 96 77.0153 152.43 61.0929 52.39 47.7835 1093.63 77.1000 153.25 0.0000 52.97 46.8899 91.11 0.0000 323.87 45.9129 53.44 45.9820 92.59 77.3426 156.02 0.0000 54.07 45.0879 93.35 77.4359 158.56 0.0000 57.36 0.0000 94.56 77.5846 159.00 55.1691 57.53 49.2998 94.65 77.5955 162.33 57.2567 57.98 53.2179 94.67 77.5978 162.66 0.0000 59.27 55.6287 94.87 77.6224 163.33 54.3025 59.32 55.6346 97.43 54.0332 165.86 54.4526 59.54 55.6604 98.43 58.2794 176.31 51. 6193 60. 96 63.6164 98.44 58;2802 ,176.60 0.0000 61.17 66.2421 99.53 67.7597 177.52 56.2779 62.93 69.0899 100 .11 67.8193 181.07 0.0000 63.29 69.1408 102.03 71.1553 181.52 62.2760 63.58 69.1815 103.18 74.4218 184.41 55.5190 64.28 69.2794 103.37 74.4430 143.76 50; 9596 66.73 70.9321 105.21 74.6461 193.51 63.0258 67.24 71. 0030 105.31 74.6569 197.03 57.3852 125.81 71. 0640 106.12 82 .1148 198.01 64.4733 67.75 71.0739 106.47 92.6896 201.83 65.8848 69.67 87.1917 109.28 60.2820 203.43 60.0932 70.83 65.5383 111. 00 71. 0316 205.31 55.0848 72.81 74.7528 111. 76 0.0000 210.85 33.2209 72. 87 74.7614 114. 06 61. 7 551 215.65 48.8589 74.66 75.0086 116. 30 0.0000 222 .11 49.1423 74.82 75.0309 116.74 54.1476 227.09 49.7594 74.97 75.0515 119.76 55.8011 227.38 48.1665 77 .11 75.3433 121.12 44.4360 228.16 0.0000 78.74 64.4800 121. 22 50.1765 228.18 51.4134 79.69 76.6987 121. 78 50.2139 116.74 51.4134 80.12 79.4499 122.06 53.1032 235.69 46.0872 80.19 0.0000 122.92 63.5810 235. 96 46.0980 80.57 63.3403 123.07 63.5936 238.63 46.2023 81. 00 55.2956 265.00 66.8811 238.98 0.0000 81. 07 55.3023 125.81 60.5784 240.99 46.2939 81. 75 85.0773 127.23 63.5801 242.00 46.3334 83.79 93.5070 127.91 67.9749 244.70 24.4406 84.00 93.5400 129.30 61.9384 252.40 0.0000 85.43 76.4402 131. 20 56.6433 252.80 44.2864 86.55 76.5839 133.02 42.5801 254.15 0.0000 86.79 76.6142 133. 52 52.4392 256.23 44.4089 86.94 76.6336 136.00 63.5605 260.90 0.0000 Page 3700 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MOA COUNTS 2 64. 66 44.7067 355.39 0.0000 584.27 10.4462 264.80 42.2281 356.01 27.8092 595.83 0.0000 265.00 42.2344 364.49 0.0000 427.87 18.0359 268.22 48.1516 366.42 0.0000 602.52 0.0000 269.46 41.1352 372. 51 22.2992 604. 72 22.5842 270.03 41.1533 *375.05 33.9473 607.14 15.0720 271.23 41.6077 377.52 27.7355 609.32 22.1262 273.65 0.0000 356.01 34 .1290. 610.33 22.1352 276.40 45.9497 3.8 8. 16 33.3167 614.28 16.6296 277.37 47.6554 388.63 0.0000 618.01 17.1605 277.60 47.6635 391.69 29.7773 620.36 14.1458 278.00 35.9681 264.66 20.8634 621. 93 22.2444 279.20 40.1865 401.81 21.7847 630.19 0.0000 279.54 43.5470 402.40 25.4246 631. 29 14.2108 279.70 41.0397 404.85 25.4604 633.25 16.2539 280.46 35 .1965* 410.95 31. 0249 634.78 0.0000 283.69 34.4419 413.71 31. 0733 635.95 12.2041 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 36.1684 423.72 0.0000 645.85 12.2534 285.90 0.0000 427.09 24.8621 657.76 15 ."3906 287.50 25.2728 427.87 23.4912 657.90 0.0000 290.67 44.3311 433.94 24.9565 661. 66 23.6364 293.27 0.0000 439.40 21.3224 664.57 0.0000 351. 93 27.9579 453.88 20.5547 666.33 0.0000 295. 96 27.9727 463.37 16.9017 666.50 0.0000 879.38 20.3823 468.07 22.5908 667.71 0.0000 299.98 30.6042 473.00 0.0000 677.62 16.5469 300.09 30.6072 475.06 23.6170 685.70 0.0000 300 .13 30.6079 476.78 25.5289 695.00 0.0000 301.36 38.2938 477.60 26.4858 696.49 21. 877 6 302.85 38.3340 482.18 26.5474 696.51 21. 8776 256.23 28.1445 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.5896 306.78 40.1497 497.08 21. 0153 697.49 14.5907 308.46 30.7896 505.52 23.0215 702.65 15.6635 311. 90 33.4355 507.63 0.0000 706.68 14 .1191 316.51 32.6825 511. 00 24.0448 711. 68 10.4781 319.41 0.0000 514.00 15.8924 720.70 0.0000 320. 08 0.0000 514.00 15.8924 721. 93 . 0.0000 321.04 30 .1963 520.40 19.3229 722.78 26.5156 323.87 32.8480 520.69 0.0000 722.91 26.5166 325.23 32.8781 522.65 0.0000 723.31 20.5220 328.76 0.0000 527.90 0.0000 724 .19 15.7916 333.37 34.7982 528.26 17.4565 727.33 30.0389 333.97 35.5083 529.59 15.5267 733.00 20.0677 334.37 30.0331 529.87 0.0000 735.93 15.8600 338.28 32.2929 531. 02 0.0000 333.97 12.6953 338.32 32.2937 537.26 0.0000 739.50 0.0000 311. 90 26.2213 546.56 0.0000 747.24 15.9259 340.48 26.2213 552.55 10.7892 748.06 7.4344 340.55 0.0000 563.25 19.2191 752.31 24.4646 344.28 31.5439 569.33 19.7664 753.82 0.0000 345.93 30.2619 946.00 19.7681 756.73 19.1770 351.06 32.5617 569.70 18.7812 756.80 19.1777 351.93 32.5798 583.19 25.8551 884.68 16.0223 Page 3701 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 14.4300 1274.44 11. 5108 1620.50 3.0031 766.42 22.4509 1001.03 9.2214 1621. 92 8.0103 766.84 22.4543 1002.74 16.1453 1678.03 0.0000 772.60 0.0000 1004.73 13.8467 1690.97 1.0148 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50' 0.0000 1025.87 0.0000 1764.49 1.0287 778.90 8.5908 1028.54 0.0000 1063.66 7.2089 783.70 0.0000 1037.84 10.4839 1771.35 3.0901 785.37 11. 3011 1038.76 0.0000 1791.20 0.0000 792.07 17.8005 631. 2 9 10.5095 1808.65 3 .1111 794.95 16.1981 1048.07 0.0000 1810.72 0.0000 795.86 8.1018 1049.04 10.5168 1836.06 4.1685 810.06 11. 7237 1050.41 7.8904 810.29 10.4219 1063.66 12.3192 344.28 8.6852 1077.00 0.0000 810.76 5.4289 1077.34 10.5989 815.77 0.0000 1085.87 9.7385 1048.07 0.0000 1093.63 9.7586 832.01 12.0299 1099.45 14.2168 834.85 17.5143 1112. 07 13.3731 835.71. 17.5195 1112. 84 14.2676 836.80 0.0000 1115. 54 8.5670 846.75 0.0000 1120.29 15.1894 846.77 15.3860 1120.55 15.1904' 856.80 0.0000 1221.41 15.1935 860.56 8.8319 1129. 67 10.7490 871.09 11. 0775 1131. 51 0.0000 873.19 14.4108 1147.95 0.0000 875.33 0.0000 1173.23 7.2471 879.38 13.3286 1177.95 10.8838 880.51 8.8890 1189.05 10.9146 883.24 17.7936 1204.77 13.6972 884.68 8.9007 1221.41 13.7540 889.28 12.2568 1231.02 18.3826 894.76 13.3940 1235.36 0.0000 898.04 12.2909 1238.28 11.9701 900. 72 14.5377 1260.41 0.0000 903.28 10.0726 1271. 87 10. 2111 911. 20 10.0975 1274.44 8.3595 912.08 10.1005 1274.54 8.3595 923.98 0.0000 1291.59 6.5283 926.50 6.7637 1298.22 0.0000 929 .11 11.2821 1312 .11 0.0000 937.49 18.0977 1332.49 12 . .2407 944 .13 0.0000 1362.66 0.0000 946.00 9. 0723 1365.19 6.6403 949.00 13. 6206 1368.63 0.0000 667.71 0.0000 1384.29 2.8581 962. 31 5.1282 1408.01 4.5973 964.08 4.5609 1457.56 0.0000 966 .17 4.5636 1460.82 5.8129 911. 20 4.5674 1489.16 3.8984 968.97 4.5674 1505.03 10.9525 983.53" 1584.12 7.9507 984.45 0.0000 1596. 21 0.0000 Page 3702 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:18:21.50 ********************************************************************************
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2040 Savage Road *
Charleston, SC 29407
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 23-NOV-2015 11:12:00 Acquisition date : 3-0CT-2016 09:16:44. Sample ID G405235036 Sample quantity : 1.62257E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.33 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity 3.00000 Batch ID :* 1596249 Detector SN# Matrix Spike ID : LCS ID . : 1556 ******************************************************************************** Pk It 1 1 2 1 3 0 4 0 5 0 6 0 7 0 8 0 9 5 10 5 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 5 22 0 23 0 24 0 25 0 26 0 . 27 0 28 0 29 0 30 0 31 . 0 32 4 33 4 34 0 Energy 74.95* 77.10* 87.19 92.82* 137.93 147.89 186.09* 209.98 238.63* 241. 61 245.61 270.50 295.45* 300.31 305.63 338.51 349.45 351.99* 409.99 464.25 515.57 538.68 543.65 562.29 583.75* 603.12 609.47* 727.30 900.61 905.40* 911. 55* 966 .14 969 .14 1120. 69* Page 3703of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 71 142 70 40 30 22 42 24 256 71 22 26 90 32 10 46 10 137 19 11 16 12 22 8 59 15 106 22 13 10 50 9 15 27 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 98 98 103 128 71 44 106 77 31 38 30 49 58 41 29 66 21 33 22 35 12 36 7 1 34 8 8 , 11 0 2 5 7 7 8 0.87 149.88 0.93 154.17 1.37 174.36 1.50 185.62 1.27 275.85 0.75 295.77 0.86 372.16 1.49 419.94 0.93 477.25 1.78 483.20 1.35 491.21 0.77 540.98 1.08. 590.88 0.59 600.60 1.40 611.24 1.85 677.00 1.16 698.88 1.28 703.96 1.70 819.95 1.29 928.46 2. 21 1031.10 5.95 1077.29 2.36 1087.24 0.711124.52 1.17 1167.42 1.84 1206.16 1.28 1218.86 0.77 1454.47 0.83 1801.00 2.72 1810.56 2.04 1822.86 1.83 1932.00 1. 68 1938. 00 2.39 2240.98 146 146 172 182 272 293 367 414 472 .472 488 536 585 597 606 669 692 700 815 923 1014 1062 1083 1123 1161 1200 1214 1450 1797 1806 1818 1930 1930 2233 12 l.98E-02 23.6 12 3.93E-02 14.4 7 1.94E-02 26.7 8 1. llE-02 54. 0 8 8.20E-03 53.0 6 6.02E-03 53.8 10 l.16E-02 50.7 10 6.72E-03 71.0 16 7.12E-02 7.4 16 1.96E-02 21.3 7 6.llE-03 46.4 8 7. llE-03 51. 7 12 2.50E-02 20.3 10 8.89E-03 41.1 9 2.64E-03112.4 14 1.27E-02 40.7 8 2.79E-03 86.2 10 3.81E-02 11.6 10 5.20E-03 52.7 12 2.99E-03112.0 22 4.52E-03 57.1 18 3. 45E-03116. 7 10 6. 09E-03 31. 5 5 2.13E-03 45.4 13 1.65E-02 24.2 11 4.16E-03 45.l 11 2. 95E-02 11. 5 10 6.19E-03 34.2 8 3.61E-03 27.7 9. 2.72E-03 45.1 10 1. 39E-02 17. 0 12 2.62E-03 42.8 12 4.25E-03 44.3 16 7.60E-03 30.5 Fit 1. 27E+OO .1. 08E+OO 1.71E+OO Peak Search Report (continued) Sample ID : G405235036 Pk It Energy Area Bkgnd 35 0 1280.68* 5 9 36 0 1291.10 7 2 37 0 1461.09* 164 7 FWHM 0.47 1. 38 2.06 Flag: "*" = Peak area was modified by Page 3704 of 5809 Acquisition date Channel Left Pw 2560.83 2554 9 2581.65 2578 7 2921.44 2914 13 Page : 2 3-0CT-2016 09:16:44 Cts/Sec %Err Fit 1.52E-03109.5 2. OlE-03 48.1 4.57E-02 8.5 background subtraction VMS Nuclide Identification Report V3 .1 Generated 3'-0CT-2016 10: 18: 23 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl 'Sample title Sample date Sample ID 23-NOV-2015 11:12:00 G405235036 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:16:44 162.26 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3705of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error . Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.33 10.00 0.00 % Peak Energy 0;0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235036 Acquisition date 3-0CT-2016 09:16:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 6.546E-01 1.060E+Ol 1.060E+Ol 17,07 OK CD-109 88.03 3.70* 4.292E+OO l.850E+OO 2.970E+OO 80.29 OK SN-126 64.28 9.60 2.567E+OO -----Line Not Found '-----Absent 86.94 8.90 4.292E+OO 7.693E-01 7.693E-01 80.29 OK 87.57 37.00* 4.292E+OO l.850E-01 l.850E-01 80.29 OK TL-208 277.37 6.60 3.041E+OO Line Not Found Absent 583.19 85.00* 1. 495E+OO 2.349E-01 2.349E-01 48.40 OK 860.56 12.50 1.058E+OO Line Not Found Absent PB-212 74.82 10.28 3.493E+OO 7 .135E-01 7.135E-01 87.15 OK 77 .11 17.10 3.655E+OO 1.410E+OO 1.410E+OO 28.78 OK 238.63 43.60* 3.499E+OO 9.340E-01 9.340E-01 14.72 OK 300.09 3.30 2.817E+OO 1.868E+OO 1. 8 68E+00 82.17 OK BI-214 609.32 45.49* l.437E+OO 8.142E-01 8.145E-01 22.99 OK 1120. 29 14.92 8.369E-01 1. 019E+OO* 1.019E+OO 60.99 OK 1764.49 15.30 5.419E-01 Line Not Found Absent PB-214 74.82 5.80 3.482E+OO Line Not Found <<INT Reject 77 .11 9.70 3.655E+00 2.485E+00 2.486E+OO 28.78 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00' 7.25 3.455E+OO Line Not Found' <<INT Reject .295.22 18.42 2.862E+OO 9.287E-01 9.290E-01 40.66 OK 351.93 35.60* 2.414E+00 8.501E-01 8.504E-01 23.27 OK RN-222 609.32 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 OK 1120.29 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 OK 1764.49 15.30 5.419E-01 Line Not Found Absent RA-224 240.99 4.10* 3.460E+OO l.123E+OO 1.123E+OO 120.72 OK RA-226 609.32 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 OK 1120. 29 14.92 8.369E-01 1.019E+OO l.019E+00 60.99 OK 1764.49 15.30 5.419E-01 Lin!" Not Found Absent AC-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 8.644E-01 8*. 644E-01 81. 42 OK 794.95 4.25 l.134E+OO Line Not Found Absent 835.71 1. 61 1.085E+OO Line Not -Found Absent 911.20 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 OK 968. 97 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 8.644E-01 8.644E-01 81. 42 OK 794.95 4.25 l.134E+OO Line Not Found Absent 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 OK 968". 97 l;:i. 80 9.524E-01 4.816E-01 4.816E-01 88.69 OK TH-228 74.82 10.28 3.493E+00 7.135E-01 7.135E-01 87.15 OK 77 .11 17.10 3. 655E+OO* 1.410E+OO l.410E+00 28.78 OK 238.63 43.60* 3.499E+00 9.340E-01 9.340E-01 14. 72 OK 300.09 3.30 2.817E+OO l.868E+OO l.868E+OO 82.17 OK TH-230 609.32 45.49* l.437E+OO 8.142E-01 8.142E-01 22.99 OK 1120.29 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 OK 1764.49 15 .. 30 5.419E-01 Line Not Found Absent PA-231 283.69 1. 70 2.976E+OO Line Not Found Absent 301.36 5.35* 2.817E+00 l.152E+OO 1.152E+OO 82.17 OK Page 3706 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235036 Acquisition date Nuclide Type: Nuclide TH-232 U-234 AM-243 Energy 105.21 338.32 835. 71 911.20 968.97 609. 32* 1120.29 1764.49 43.53 74.66 Flag: "*" = Keyline Page 3707of5809 %Abn 1.10 11. 27 1. 61 25.80* 15.80 45.49* 14.92 15.30 5.90 67.20* Uncorrected Decay Corr %Eff pCi/GRAM pCi/GRAM 4.933E+OO Line Not Found 2.507E+OO 8.644E-01 8.644E-01 1.085E+OO Line Not Found 1. 005E+OO 9.219E-01 9.219E-01 9.524E-01 4.816E-01 4.816E-01 1.437E+00 8.142E-01 8.142E-01 8.369E-01 1.019E+OO 1.019E+OO 5.419E-01 Line Not Found 5.957E-01 Line Not Found 3.493E+00 1. 091E-01 1.092E-01 Page : 3 3-0CT-2016 09:16:44 2-Sigma %Error Status Absent 81.42 OK Absent 34.07 OK 88.69 OK 22.99 OK 60.99 OK Absent Absent 87,15 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:18:24.60 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l *
Acquisition date 3-0CT-2016 09:16:44 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
Sample date 23-NOV-2015 11:12:00 Analyst initials: MXRl *
Sample ID G405235036 Sample Quantity l.6226E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr l.ODOOO Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;? .
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.060E+Ol 1.773E+OO CD-109 2.970E+OO 2.337E+OO SN-126 1.850E-01 1.456E-01 TL-208 2.349E-01 1.114E-01 PB-212 9.340E-01 1. 347E-01 BI-214 8.145E-01 1.835E-01 PB-214 8.504E-01 1.939E-01 RN-222 8.145E-01 1.835E-01 RA-224 1.123E+00 l.329E+OO RA-226 8.145E-01 1:835E-01 AC-228 9.219E-01 3.078E-01 RA-228 9.219E-01 3.078E-01 TH-228 9.340E-01 1.347E-01 TH-230 8.142E-01 l.835E-01 PA-231 l.152E+00 9.281E-01 TH-232 9.219E-01 3.078E-01 U-234 8.142E-01 1.835E-01 *AM-243 l.092E-01 9.322E-02 Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3708 of 5809 Key-Line Activity (pCi/GRAM -l.064E+Ol 3.170E-02 O.OOOE+OO 3.627E-02 2.299E-01 O.OOOE+OO O.OOOE+OO 1.838E-02 -3.226E-02 O.OOOE+OO 2.380E-02 -1.390E-01 K.L. Cnt Uncert (1. 96-sigma) 1.355E+Ol 5.942E-02 1.960E+41 4.312E-02 4.645E-01 3.529E+04 6.254E+02 7.036E-02 5.935E-01 1. 960E+41 3.952E-02 7.991E-01 MDA (pCi/GRAM 7.126E-01 2. 096E+OO l.313E-01 5.556E-02 9.819E-02 1.360E-01 l.167E-01 1.360E-01 1.054E+OO 1.360E-01 2.486E-01 2.486E-01 9.819E-02 1.359E-01 6.582E-01 2.486E-01 1.359E-01 8.170E-02 MDA (pCi/GRAM 2.471E+Ol 1.290E-01 O.OOOE+OO 1.172E-01 1.052E+OO O.OOOE+OO O.OOOE+OO 1.509E-01 1.195E+OO O.OOOE+OO 8.466E-02 1.559E+OO NOT IDENT.* NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT.

FE'--59 9.008E-01 1. 861E+Ol FAIL ABUN C0-60 -2.800E-02 4.645E-02 8.517E-02 NOT IDENT. ZN-65 -5.428E-02 2.233E-01 3.929E-01 NOT IDENT. GE-68 3.071E+OO 3. llOE+OO 7.350E+OO NOT IDENT. AS-73 -3.276E+OO 7.927E+OO 1.631E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.195E+04 O.OOOE+OO SHORT HLIF SE-75 -1. llOE-01 2.086E-01 3.721E-01 NOT IDENT. BR-77 O.OOOE+OO l.977E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l .131E+03 O.OOOE+OO SHORT HLIF RB-83 -l.912E-01 8.405E-01 1.607E+OO NOT IDENT. KR-85 6.430E+OO 7.474E+OO 1.698E+Ol NOT IDENT. SR-85 7.952E-01 9.253E-01 2.102E+OO NOT IDENT. RB-86 0.000E+OO 6.654E+04 0.000E+OO SHORT HLIF Y-88 -7.376E-03 2.799E-01 6.479E-Ol NOT IDENT. Y-91 4. 011E+02 7.878E+02 1.777E+03 NOT IDENT. NB-94 1.108E-02 3.145E-02 6.887E-02 NOT IDENT. NB-95 -l.178E-01 1.104E+OO 2.183E+OO NOT IDENT. NB-95M 1.968E+OO 2.817E+OO 5.479E+OO NOT IDENT. ZR-95 1.042E+OO 1.878E+OO 4.217E+OO NOT IDENT. NB-97 O.OOOE+OO 1.718E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1.913E+41 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO 9.814E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.598E-02 3.391E-02 6.459E-02 NOT IDENT. RH-102 1. 880E-02 7.656E-02 1.591E-01 NOT IDENT. RU-103 -1.082E+OO 6.248E+OO 1.296E+Ol FAIL ABUN RH-106 9.562E-02 5. lllE-01 1.109E+OO NOT IDENT. RU-106 9.562E-02. 5. lllE-01 1.109E+OO NOT IDENT. AG-108M -5.279E-03 2.571E-02 5.252E-02 NOT IDENT. AG-llOM 3.206E-02 9.701E-02 2.211E-01 NOT IDENT. SN-113 l.611E-01 2.368E-01 5. 396E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.982E+05 O.OOOE+OO SHORT HLIF TE-123M -7.255E-02 l.257E-01 2.334E-01 NOT IDENT. SB-124 6.176E-01. 2.853E+OO 6.988E+OO NOT IDENT. SB-125 l.210E-01 1.242E-01 2.806E-01 FAIL ABUN TE-125M 1.274E+02 3. 096E+02 6. 431E+02 NOT IDENT. I-126 O.OOOE+OO 2.122E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.012E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4.174E+23 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 2.142E+10 O.OOOE+OO SHORT HLIF I-132 *O.OOOE+OO 1.394E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 1.056E+28 O.OOOE+OO SHORT HLIF BA-133 -3.443E-03 4.624E-02 7.943E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 6.324E-02 5.968E-02 1.407E-01 FAIL ABUN CS-135 6.958E-02 l.497E-01 2.835E-01 NOT IDENT. I-135 0.000E+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 6.074E+05 O.OOOE+OO SHORT HLIF BA-137M 1.080E-02 3.802E-02 8.088E-02 NOT IDENT. CS-137 1.141E-02 4.016E-02 8.544E-02 NOT IDENT. CE-139 -1.998E-02 1.070E-01 2.065E-01 NOT IDENT. BA-140 O.OOOE+OO l.003E+07 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO l.224E+06 0.000E+OO SHORT HLIF CE-141 -6.765E+OO 3.143E+Ol 5.496E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.726E+41 O.OOOE+OO SHORT HLIF CE-144 l.124E-01 3.258E-01 6.706E-01 NOT IDENT. PM-144 2.471E-03 6.715E-02 1.358E-01 NOT IDENT. PR-144 2.396E-01 5.884E+OO 1.191E+Ol NOT IDENT. PM-146 1.672E-02 4.152E-02 9.215E-02 NOT IDENT. ND-147 O.OOOE+OO 1.051E+08 O.OOOE+OO SHORT HLIF PM-147 3. 096E+02 7. 296E+02 1. 523E+03 NOT IDENT. PM-149 0.000E+OO 1.409E+41 O.OOOE+OO SHORT HLIF EU-150 5.709E-03 3.261E-02 5.769E-02 FAIL ABUN EU-152 -6.003E-02 l.197E-01 1. 872E-01 FAIL ABUN GD-153 -l.144E-01 l.635E-01 3 .115E-01 NOT IDENT. EU-154 6.950E-02 l.426E-01 3.077E-01 NOT IDENT. EU-155 -1. 7 61E-02 8. 967E-02 1.793E-01 FAIL ABUN TB-160 2.992E-01 2.082E+OO 4.508E+OO FAIL ABUN H0-166M -l.913E-02 5. 611E-02 1.080E-01 FAIL ABUN TM-171 2.088E+OO l.620E+Ol 3.503E+Ol NOT IDENT. HF-172 1.068E-01 2.175E-01 4.515E-01 NOT IDENT. LU-172 3.250E-02 8.303E-02 l.852E-01 FAIL ABUN LU-176 1.985E-02 4. 371E-02 3.638E-02 FAIL ABUN HF-181 -3.044E+OO 5.261E+OO 9.995E+OO NOT IDENT. TA-182 8.676E-01 l.177E+OO 2.777E+OO FAIL ABUN RE-183 -5.533E-01 2.781E+OO 5.793E+OO NOT IDENT. RE-184 2.855E+Ol 2.503E+Ol 7.678E+Ol NOT IDENT. Page 3709 of 5809 W-188 7.686E+Ol 1.278E+02 2. 514E+02 NOT IDENT. IR-192 -4.386E-02 5.485E-01 1.033E+OO FAIL ABUN HG-203 -2.129E+OO 2.928E+00 5.016E+OO NOT IDENT. BI-207 1.217E-03 5.013E-02 1.032E-01 FAIL ABUN PB-210 1.423E-01 2.128E+OO 4.604E+OO NOT IDENT. BI-211 O.OOOE+OO 5.342E-01 8.095E-01 FAIL ABUN PB-211 3.558E-01 *7.958E-01 1.656E+OO NOT IDENT. BI-212 1. 336E+OO 8.951E-01 1.624E+OO FAIL ABUN RN-219 5.605E-02 3.895E-01 8.222E-01 FAIL ABUN RA-223 -3.544E-01 6.451E-01 1.119E+OO FAIL ABUN AC-227 -3.757E-02 2.338E-01 4.388E-01 FAIL ABUN TH-227 -3.757E-02 2.338E-01 4.388E-01 FAIL ABUN TH-229 -3.053E-01 4.171E-01 7.455E-01 FAIL ABUN TH-231 -3.544E-01 6.451E-Ol 1.119E+OO FAIL ABUN PA-233 1. 871E-02 6.343E-02 l.254E-01 FAIL ABUN PA-234 1.488E-01 2.550E-01 6.124E-01 NOT IJ;JENT. PA-234M 3.609E+OO 4.654E+OO 1. ll 7E+Ol NOT IDENT. TH-234 -l.884E-01 1.035E+OO 2.145E+OO FAIL ABUN U-235 4.722E-02. l.592E-01 3.157E-01 FAIL ABUN NP-237 l.871E-02 6.343E-02 l.254E-01 FAIL ABUN NP-238 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -l.884E-01 l.035E+00 2.145E+OO FAIL ABUN NP-239 -8.077E-02 2.142E-01 4.165E-01 NOT IDENT. PU-239 2.454E+02 2.999E+02 6.329E+02 NOT IDENT. AM-241 2.294E-02 1. 074E-01 2.313E-01 NOT IDENT. CM-243 -2.489E-02 8.694E-02 l.720E-01 NOT IDENT. BK-247 -l.090E-02 6.476E-02 1.227E-01 NOT IDENT. CM-247 -4.952E-03 3.793E-02 7. 696E-02 NOT IDENT.' CF-249 8.157E-04 3.414E-02 7. 213E-02 NOT IDENT. CF-251 4.614E-03 1.028E-01 2.027E-01 NOT IDENT. ANH-511 -1.687E-02 4.760E--:02 1.088E-01 NOT IDENT. Page 3710 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:18:22.26 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 160 10.66* 6.546E-01 1.060E+Ol 1. 060E+Ol 17.07 CD-109 88.03 93 3.70* 4.292E+OO 2.706E+OO 4.344E+OO 53.37 SN-126 64.28 ------9.60 2.567E+OO ------Line Not Found ------86.94 93 8.90 4.292E+OO 1.125E+OO 1.125E+OO 53.37 87.57 93 37.00* 4.292E+OO 2.706E-01 2.706E-01 53.37 TL-208 277.37 ------6.60 3.041E+OO ------Line Not Found ------583.19 64 85.00* l.495E+OO 2.349E-01 2.349E-01 48.40 860.56 ------12.50 1.058E+OO ------Line Not Found ------BI-211 72. 87 ------1.23 3.327E+OO ------Line Not Found ------351.06 158 12.92* 2.414E+OO 2.342E+OO 2.342E+OO 23.27 PB-212 74.82 96 10.28 3.493E+OO 1.237E+OO 1.237E+OO 47.20 77 .11 190 17.10 3.655E+OO 1.410E+OO 1.410E+OO 28.78 238.63 308 43.60* 3.499E+OO 9.340E-01 9.340E-01 14.72 300.09 38 3.30 2.817E+OO l.868E+00 1. 8 68E+OO 82.17 BI-214 609.32 115 45.49* l.437E+OO 8.142E-01 8.145E-01 22.99 1120.29 27 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------PB-214 74.82 96 5.80 3.493E+OO 2.193E+OO 2.194E+00 47.20 77 .11 190 9.70 3.655E+OO 2.485E+OO 2.486E+OO 28.78 87.09 93 3.41 4.292E+OO 2.936E+OO 2.938E+OO 53.37 242.00 85 7.25 3.460E+OO 1.564E+OO 1.564E+OO 42.68 295.22 106 18.42 2.862E+OO 9.287E-01 9.290E-01 40.66 351. 93 158 35.60* 2.414E+OO 8.501E-01 8.504E-01 23.27 RN-222 609.32 115 45.49* l.437E+OO 8.142E-01 8.145E-01 22.99 1120.29 27 14.92 8.369E-01 l.019E+OO 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------RA-224 240.99 85 4.10* 3.460E+OO 2.765E+OO 2.765E+OO 42.68 RA-226 609.32 115 45;49* l.437E+OO 8.142E-01 8.145E-01 22.99 1120.29 27 14.92 8.369E-01 l.019E+OO 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 53 11. 27 2.507E+OO 8.644E-01 8.644E-01 81. 42 794.95 ------4.25 1.134E+OO ------Line Not Found ------835.71 ------1. 61 1.085E+OO ------Line Not Found ------911. 2.0 52 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 968.97 16 15.80 9.524E-01 4.816E-01 4*. 816E-01 88.69 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 53 11. 27 2.507E+OO 8.644E-01 8.644E-01 81. 42 794.95 ------4.25 l .134E+00 ------Line Not Found ------835.71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 52 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 968.97 16 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 TH-228 74.82 96 10.28 3.493E+OO 1.237E+OO 1.237E+OO 47.20 77 .11 190 17.10 3.655E+OO 1.410E+OO l.410E+OO 28.78 238.63 *308 43. 6.0* 3.499E+OO 9.340E-01 9.340E-01 14.72 300.09 38 3.30 2.817E+OO 1. 868E+OO 1.868E+OO 82.17 TH-230 609.32 115 45.49* 1.437E+OO 8.142E-01 8.142E-01 22.99 Page 3711 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235036 Acquisition date Page : 2 3-0CT-2016 09:16:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 1120.29 27 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 2.976E+OO ------Line Not Found ------301.36 38 5.35* 2.817E+OO l.152E+OO l.152E+OO 82.17 TH-232 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 53 11. 27 2.507E+OO 8.644E-01 8.644E-01 81. 42 835. 71 ------i. 61 1.085E+OO ------Line Not Found ------911. 20 52 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 968.97 16 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 U-234 609.32 115 45.49* l.437E+OO 8.142E-01 8.142E-01 22.99 1120.29 27 14.92 8.369E-01 1.019E+OO 1.019E+00 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 96 67.20* 3.493E+OO 1.893E-01 1.893E-01 47.20 Flag: "*" Key line Page 3712 of 5809 Summary of .Nuclide Activity Sample ID : G405235036 Acquisition date Page : 3 3-0CT-2016 09:16:44 Total number of lines in spectrum 37 Number of unidentified lines 6 Number of lines tentatively identified by NID 31 Nuclide "J;'ype : Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Hlife l.25E+09Y 461.40D 2.30E+05Y 1. 41E+l0Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY l.41E+l0Y l.41E+l0Y 1.41E+10Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 2.45E+05Y 7370.00Y Decay 1. 00 1. 61 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.060E+Ol 2.706E+OO 2.706E-01 2.349E-01 2.342E+OO* 9.340E-01 8.142E-01 8.501E-01 8.142E-01 2.765E+OO 8.142E-01 9.219E-01 9.219E-01 9.340E-01 8.142E-01 1.152E+OO 9.219E-01 8.142E-01 l.893E-01 2.982E+Ol 2.982E+Ol Decay Corr pCi/GRAM l.060E+Ol 4.344E+OO 2.706E-01 2.349E-01 2.342E+OO 9.340E-01 8.145E-01 8.504E-01 8.145E-01 2.765E+OO 8.145E-01 9.219E-01 9.219E-01 9.340E-01 8.142E-01 1.152E+OO 9.219E-01 8.142E-01 l.893E-01 3.146E+Ol 3.146E+Ol 83.78% Decay Corr 2-Sigma Error 0.181E+Ol 2.318E+00 l.444E-01 1.137E-01 0.545E+OO 1.375E-01 1.873E-01 l.979E-01 1.873E-01 l.180E+OO 1.873E-01 3 .141E-01 3.141E-01 l.375E-01 l.872E-01 0.947E+OO 3 .141E-01 1. 872E-01 0.894E-01 "M" Manually accepted 2-Sigma %Error 17.07 53.37 53.37 48.40 23.27 14.72 22.99 23.27 22.99 42.68 22.99 34.07 34.07 14. 72 . 22.99 82.17 34.07 22.99 47.20 Flags: "K" Keyline not found "E" = Manually edited "A" = specific abn. limit Page 3713of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235036 Acquisition date : 3-0CT-2016 09:16:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 92.82 53 169 1. 50 185.62 182 8 l.llE-02 **** 4.56E+OO T 0 137. 93 38 91 1. 27 275.85 272 8 8.20E-03 **** $.02E+OO T 0 147.89 27 56 0.75 295.77 293 6 6.02E-03 **** 4.90E+OO 0 186.09 51 131 0.86 372.16 367 10 l.16E-02 **** 4.30E+OO T 0 209.98 29 94 1. 49 419.94 414 10 6.72E-03 **** .3. 91E+OO T 0 245.61 26 36 1. 35 491.21 488 7 6.llE-03 92.8 3. 41E+OO T 0 270.5b 30 59 0.77 540.98 536 8 7.llE-03 **** 3. llE+OO T 0 305.63 11 33 1. 40 611. 24 606 9 2.64E-03 **** 2.77E+OO T 0 349.45 12 24 1.16 698.88 692 8 2.79E-03 **** 2.43E+OO 0 409.99 21 25 1. 70 819.95 815 10 **** 2.08E+OO T 0 464.25 12 39 1. 29 928.46 923 12 2.99E-03 **** 1. 85E+OO T 5 515.57 18 14 2.21 1031.10 1014 22 4.52E-03 **** 1. 68E;+OO 0 538.68 14 39 5.95 1077.29 1062 18 3.45E-03 **** 1. 61E+OO T 0 543.65 24 8 2.36 1087.24 1083 10 6.09E-03 63.0 1. 60E+OO 0 562.29 8 1 0.71 H24. 52 1123 5 2.13E-03 90.8 1. 55E+00 T 0 603.12 16 9 1. 84 1206.16 1200 11 4.16E-03 90.3 l.45E+00 T 0 727. 30 24 11 0.77 1454.47 1450 10 6.19E-03 68.4 1.23E+00 T 0 900.61 13 0 0.83 1801.00 1797 8 3.61E-03 55.5 1. 02E+00 T 0 905.40 10 2 2. 72 1810.56 1806 9 2.72E-03 90,2 1. OlE+OO 4 966.14 10 7 1. 83 1932.00 1930 12 2.62E-03 85.5 9.55E-01 T 0 1280.68 5 9 0.47 2560.83 2554 9 l.52E-03 **** 7.41E-01 0 1291.10 7 2 1. 38 2581.65 2578 7 2.0lE-03 96.2 7.36E-01 T Flags: "T" = Tentatively associated Page 3714of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:18:37.96 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l *
Acquisition date 3-0CT-2016 09:16:44 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: . O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: O 01:00:00.33 Half life ratio : ***** *
Sample date 23-NOV-2015 11:12:00 Nuclide Library : SOLID *
Sample ID G405235036 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : l.6226E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Le . (pCi/GRAM 2.657E-01 9.797E-01 6.136E-02 2.267E-02 4.474E-02 5.806E-02 5.069E-02 5.806E-02 4.805E-01 5.806E-02 9.958E-02 9.958E-02 4.474E-02 5.804E-02 2.851E-01 9.958E-02 5.804E-02 3.791E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 , C0-57 C0-58 FE-59 Page 3715of5809 Le (pCi/GRAM 1.026E+Ol 5.380E-02 O.OOOE+OO 4.667E-02 4.416E-01 O.OOOE+OO O.OOOE+OO 6.354E-02 4. 963E-01 O.OOOE+OO 3.887E-02 6.532E-01 7.515E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 .Y-8 8 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 . LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 Page 3716of5809 3.264E-02 1.598E-01 3.164E+OO 7.481E+OO O.OOOE+OO l.641E-01 O.OOOE+OO 0.000E+OO 6.938E-01 7.544E+Ob 9.338E-01 O.OOOE+OO 2.295E-01 7.586E+02 2.932E-02 9.250E-01 2. 511E+OO 1.806E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 996E-02 6.983E-02 5.403E+00 4.712E-01 4.712E-01 2.258E-02 9.003E-02 2."388E-01 O.OOOE+OO O.OOOE+OO 1.062E-01 2.616E+00 1.267E-01 2. 991E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.501E-02 O.OOOE+OO 6.150E-02 l.285E-01 0.000E+OO O.OOOE+OO* 3.494E-02 3.691E-02 9.442E-02 O.OOOE+OO O.OOOE+OO 2.515E+Ol O.OOOE+OO 3.094E-01 5.863E-02 5.141E+OO 4.014E-02 O.OOOE+OO 7.029E+02 O.OOOE+OO 2.610E-02 8.312E-02 1.435E-01 1. 277E-01 8.223E-02 l.833E+00 4. 445E-02 . 1.609E+Ol 2. 096E-01 7.634E-02 1.563E-02 4.214E+OO 1.184E+OO 2.664E+OO 3.047E+Ol 1.128E+02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT "IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3717 of 5809 4.590E-01 2.217E+OO 4.169E-02 2.106E+OO 3.838E-01 7.459E-01 7.333E-01 3.643E-01 4. 964E-01 l.981E-01 l.981E-01 3.364E-01 4. 964E-01 5.637E-02 2.513E-01 4.763E+OO 9.972E-01 1.455E-01 5.637E-02 O.OOOE+OO 9. 972E-01 1.914E-01 2.954E+02 l.065E-01 7.924E-02 5.437E-02 3.419E-02 3.153E-02 9.264E-02 5.056E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT 'IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT I DENT .. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:18:43.38 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l *
Acquisition date 3-0CT-2016 09:16:44 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
Sample date 23-NOV-2015 11:12:00 Nuclide Library : SOLID *
Sample ID G405235036 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.6226E+02 GRAM *
Quantity Err(%) : 1.2326E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* *
INFORMATION * * *
Eff. Cal. date 1-JUN-2016 09:39:12 Eff. Geometry *: CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
Combined Activity-MDA Report NOTE: Nbt all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU *Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.060E+Ol 1.858E+OO l.858E+00 CD-109 2.970E+OO 2.356E+OO 2.356E+OO SN-126 l.850E-01 l.464E-01 l.464E-01 TL-208 2.349E-01 l .119E-01 l.119E-01 PB-212 9.340E-01 1.435E-01 l.435E-01 BI-214 8.145E-01 1. 869E-01 1. 869E-01 PB-214 8.504E-01 1. 971E-01 1. 971E-01 RN-222 8.145E-01 1. 869E-01 1. 8 69E-01 RA-224 l.123E+OO 1.335E+OO 1.335E+OO RA-226 8.145E-01 1. 8 69E-01 1. 869E-01 AC-228 9.219E-01 3. 114E-01 3 .114E-01 RA-228 9.219E-01 3 .114E-01 3.114E-01 TH-228 9.340E-01 1.435E-01 1.435E-01 TH-230 8.142E-01 1.868E-01 l.868E-01 PA-231 l.152E+OO 9.601E-01 9.601E-01 TH-232 9.219E-01 3 .114E-01 3 .114E-01 U-234 8.142E-01 1. 868E-01 l.868E-01 AM-243 1.092E-01 9.402E-02 9.402E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.064E+Ol 1.356E+Ol 1.438E+Ol NOT IDENT. NA-22 3.170E-02 5.944E-02 6 .113E-02 NOT IDENT. NA-24 1.000E+41 2.638E+41 O.OOOE+OO SHORT HLIF AL-26 3.627E-02 4.318E-02 4.618E-02 NOT IDENT. SC-46 2.299E-01 4.646E-01 4.760E-01 FAIL ABUN V-48 -4. 571E+04 3.533E+04 4.090E+04 SHORT HLIF CR-51 -3.855E+02 6.256E+02 6.493E+02 SHORT HLIF
MN-54 1.838E-02 7.037E-02 7.085E-02 NOT IDENT. C0-56 -3.226E-02 5.935E-01 5.937E-01 NOT IDENT. MN-56 -1.000E+41 l.555E+42 O.OOOE+OO SHORT HLIF C0-57 2.380E-02 3.954E-02 4.097E-02 FAIL ABUN C0-58 -1.390E-01 7.991E-01 8.016E-01 NOT IDENT. Page 3718of5809 FE-59 9.008E-01 8. 271E+OO 8.281E+OO FAIL ABUN C0-60 -2.800E-02 4.646E-02 4.814E-02 NOT IDENT. ZN-65 -5.428E-02 2.-233E-01 2.246E-01 NOT IDENT. GE-68 3. 071E+00 3.112E+OO 3.406E+OO NOT IDENT. AS-73 -3.276E+00 *7.955E+OO 8.091E+OO NOT IDENT. AS-74 4.053E+03 l.195E+04 l.209E+04 SHORT HLIF SE-75 -1. llOE-01 2.086E-01 2.145E-01 NOT IDENT. BR-77 1.370E+40 l.246E+41 O.OOOE+OO SHORT HLIF SR-82 4.368E+02 l.132E+03 l.149E+03 SHORT HLIF RB-83 -l.912E-01 8.409E-01 8.453E-01 NOT IDENT. KR-85 6.430E+OO 7.479E+OO 8. 021E+OO NOT IDENT. SR-85 7.952E-01 9.259E-01 9.928E-01 NOT IDENT. RB-86 3. 988E+o4 6.656E+04 6.895E+04 SHORT HLIF Y-88 -7.376E-03 2.799E-01 2.799E-01 NOT IDENT. Y-91 4. 011E+02 7.880E+02 8.084E+02 NOT IDENT. NB-94 l.108E-02 3.145E-02 3.185E-02 NOT IDENT. NB-95 -1.178E-01 l.104E+OO l.105E+OO NOT IDENT. NB-95M 1. 968E+OO 2.821E+OO 2.957E+OO NOT IDENT. ZR-95 1.042E+OO l.878E+OO 1. 936E+OO NOT IDENT. NB-97 -l.000E+41 1. 719E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1. 914E+41 O.OOOE+OO SHORT HLIF M0-99 3.797E+33 9.818E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 6.280E+41 O.OOOE+OO SHORT HLIF RH-101 -1.598E-02 3.404E-02 3.479E-02 NOT IDENT. RH-102 1. 880E-02 7.657E-02 7.704E-02 NOT IDENT. RU-103 -l.082E+OO 6.248E+OO 6.267E+OO FAIL ABUN RH-106 9.562E-02 5. lllE-01 5.129E-01 NOT IDENT. RU-106 9.562E-02 5. lllE-01 5.129E-01 NOT IDENT. AG-108M -5.279E-03 2.571E-02 2.582E-02 NOT IDENT. AG-llOM 3.206E-02 9.702E-02 9.809E-02 NOT IDENT. SN-113 1.611E-01 2.369E-01 2.478E-01 NOT IDENT. CD-115 -7.985E+39 3 .*858E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -2.346E+05 2.003E+05 2.265E+05 SHORT HLIF TE-123M -7.255E-02 l.257E-01 l.299E-01 NOT IDENT. SB-124 6.176E-01 2.853E+OO 2.867E+OO NOT IDENT. SB-125 l.210E-01 l.243E-01 1.357E-01 FAIL ABUN TE-125M 1. 274E+02 3.097E+02 3.150E+02 NOT IDENT. I-126 2.106E+05 2.122E+06 2.124E+06 SHORT HLIF SB-126 -l.624E+06 3.028E+06 3 .115E+06 SHORT HLIF SB-127 2.055E+23 5.121E+23 O.OOOE+OO SHORT HLIF I-131 -2.268E+l0 2.145E+l0 2.376E+l0 SHORT HLIF I-132 -l.000E+41 l.946E+42 O.OOOE+OO SHORT HLIF TE-132 l.296E+27 l.057E+28 O.OOOE+OO SHORT HLIF BA-133 -3.443E-03 4.624E-02 4.626E-02 NOT IDENT. I-133 -1.000E+41 8.737E+41 O.OOOE+OO SHORT HLIF CS-134 6.324E-02 5.974E-02 6.619E-02 FAIL ABUN CS-135 6.958E-02 l.498E-01 l.530E-01 NOT IDENT. I-135 -l.000E+41 7.734E+41 O.OOOE+OO SHORT HLIF CS-136 l.507E+05 6.076E+05 6 .114E+05 SHORT HLIF BA-137M l.080E-02 3.802E-02 3.833E-02 NOT IDENT. CS-137 l .141E-02 4.016E-02 4.049E-02 NOT IDENT. CE-139 -1. 998E-02 1. 070E-01 1. 074E-01 NOT IDENT. BA-140 4.387E+06 l.004E+07 l.023E+07 SHORT HLIF LA-140 -8.774E+05 l.224E+06 l.287E+06 SHORT HLIF CE-141 -6.765E+OO 3.143E+Ol 3.158E+Ol NOT IDENT. CE-143 1.000E+41 l.729E+41 O.OOOE+OO SHORT HLIF CE-144 l.124E-01 3.259E-01 3.298E-01 NOT IDENT. PM-144 2. 471E-03 6.715E-02 6.716E-02 NOT IDENT. PR-144 2. 396E-01 5.884E+OO 5.885E+OO NOT IDENT. PM-146 1.672E-02 4.154E-02 4. 222E'-02 NOT IDENT. ND-147 -6.125E+07 1. 051E+08 l.087E+08 SHORT HLIF PM-147. 3. 096E+02 7.297E+02 7.429E+02 NOT IDENT. PM-149 l.OOOE+41 l.427E+41 O.OOOE+OO SHORT HLIF EU-150 5.709E-03 3.261E-02 3.271E-02 FAIL ABUN EU-152 -6.003E-02 l.197E-01 l.227E-01 FAIL ABUN GD-153 -l .144E-01' 1.636E-01 1. 716E-01 NOT I DENT'. EU-154 6.950E-02 1.426E-01 l.460E-01 NOT IDENT. EU-155 -1. 7 61E-02 8. 968E-02 9.003E-02 FAIL ABUN TB-160 2.992E-01 2.082E+OO 2.087E+OO FAIL ABUN H0-166M -l.913E-02 5.612E-02 5.678E-02 FAIL ABUN TM-171 2.088E+OO 1.620E+Ol l.623E+Ol NOT IDENT. HF-172 1. 068E-01 2.182E-Ol 2.234E-01 NOT IDENT. LU-172 3.250E-02 8.310E-02 8.438E-02 FAIL ABUN LU-176 l.985E-02 4.371E-02 4.462E-02 FAIL ABUN HF-181 -3.044E+OO 5.263E+OO 5.439E+OO NOT IDENT. TA-182 8.676E-01 l.178E+OO l.241E+OO FAIL ABUN RE-183 -5.533E-Ol 2.782E+OO 2.794E+OO NOT IDENT. RE-184 2.855E+Ol 2.603E+Ol 2.904E+Ol NOT IDENT. Page 3719of5809 W-188 7.686E+Ol 1. 281E+o2 l.327E+02 NOT IDENT. IR-192 -4.386E-02 5.485E-01 5.488E-01 FAIL ABUN HG-203 -2.129E+OO 2.929E+00 3.083E+00 NOT IDENT. BI-207 1. 217E-03 5.013E-02 5.013E-02 FAIL ABUN PB-210 1.423E-Ol *2.128E+OO 2.129E+OO NOT IDENT. BI-211 2.342E+OO 5.443E-01 l.188E+OO FAIL ABUN PB-211 3.558E-01 7. 960E-01 8.120E-01 NOT IDENT. BI-212 1.336E+OO 8.976E-01 1.081E+OO FAIL ABUN RN-219 5.605E-02 3.895E-01 3.904E-Ol FAIL ABUN RA-223 -3.544E-01 6.455E-01 6.649E-01 FAIL ABUN AC-227 -3.757E-02 2.339E_:Ol 2.345E-01 FAIL ABUN TH-227 -3.757E-02 2.339E-01 2.345E-01 'FAIL ABUN TH-229 -3.053E-01 4.173E-01 4.394E-01 FAIL ABUN TH-231 -3.544E-01 6.455E-01 6.649E-01 FAIL ABUN PA-233 1. 871E-02 6.344E-02 6.400E-02 FAIL ABUN PA-234 3.066E-01 3.139E-01 NOT IDENT. PA-234M 3.609E+OO 4.657E+OO 4.933E+OO NOT IDENT. TH-234 -1.884E:...01 1.036E+OO 1.039E+OO FAIL ABUN U-235 4.722E-02 l.592E-01 1.606E-01 FAIL ABUN NP-237 1.871E-02 6.344E-02 6*. 400E-02 FAIL ABUN NP-238 1.000E+41 1.904E+42 O.OOOE+OO SHORT HLIF U-238 -1.884E-01 1.036E+OO 1.039E+OO FAIL ABUN NP-239 -8.077E-02 2.143E-01 2.174E-01 NOT IDENT. PU-239 2.454E+02 3.001E+02 3.199E+02 NOT IDENT. AM-241 2.294E-02 1. 074E-01 1. 079E-01 NOT IDENT. CM-243 -2.489E-02 8.697E-02 8;769E-02 NOT IDENT. BK-247 -l.090E-02 6.479E-02 6.498E-02 NOT IDENT. CM-247 -4.952E-03 '3.794E-02 3.800E-02 NOT IDENT. CF-249 8.157E-04 3.414E-02 3.414E-02 NOT I0DENT. CF-251 . 4. 614E-03 1.028E-01 l.028E-01 NOT IDENT. ANH-511 -l.687E-02 4.760E-02 4.821E-02 NOT IDENT. Page 3720 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 22.6668 87.09 68.7588 136.47 39.9849 45.60 35.4275 87.57 68.8320 140.51 0.0000 46.54 30.8024 88.03 68.9016 143.76 39.1449 49. 72 0.0000 88.34 68.9486 144.24 36.2361 51. 35 44.9328 88.47 83.7051 145.44 41. 8639 51. 87 43.3996 89. 96 72.7416 152.43 58.5067 52.39 40.2504 1093.63 58.6345 153.25 0.0000 52. 97 47.5817 91.11 0.0000 323.87 48.7189 53.44 48.4589 92.59 74.9381 156.02 0.0000 54.07 32.3686 93.35 75.0592 158.56 0.0000 57.36 0.0000 94.56 48.9728 159.00 44.0557 57.53 31. 8897 94.65 48.9820 162.33 43.2605 57.98 47.4881. 94.67 48.9840 162.66 0.0000 59.27 36.1609 94.87 46.6140 163.33 42.3147 59.32 36.1661 97.43 50.4667 165.86 41. 4548 59.54 41.9464 98.43 46.0549 176.31 44.1049 60. 96 43.7685 98.44 46.0561 176. 60 0.0000 61.17 55.3630 99.53 52.4935 177.52 36.9849 62.93 51. 4845 100 .11 56.1795 181. 07 0.0000 63.29 53.1981 102.03 45.4803 181. 52 45.4435 63.58 46.5856 103.18 56.5243 184.41 45.6154 64.28 48.3422 103.37 51. 0734 143.76 45.6926 66.73 48.6631 105.21 44.8504 193.51 40.9037 67.24 52.9299 105.31 44.8593 197.03 45.2964 125.81 56.3559 106.12 46.7635 198.01 36.9141 67.75 56.3661 106.47 44. 9603 201.83 32.8481 69.67 .53.2682 109.28 50.7375 203.43 33.9736 70.83 61. 0593 111. 00 55.5295 205.31 39.7253 72. 81 62.5033 111.76 0.0000 210.85 29.9905 72.87 62.5128 114. 06 44.6766 215.65 26.9272 74.66 55.6565 116. 30 0.0000 222 .11 36.8923 74.82 55.6784 116. 74 50. 5072 227.09 33.8254 74.97 55.6992 119.76 47.0196 227.38 40.3852 77 .11 55.9903 121.12 46.1902 228.16 0.0000 78.74 58.8038 121. 22 40.5415 228.18 32.7740 79.69 54.3141 121. 78 32.0874 116.74 32.7740 80.12 56.6827 122.06 32.1033 235.69 27.9039 80.19 0.0000 122.92 43.4991 235. 96 24.9739 80.57 61.3745 123.07 43.5103 238.63 35.3589 81. 00 49.5549 265.00 49.2380 238.98 0.0000 81. 07 49.5628 125.81 46.5680 240.99 35.4478 81. 75 60. 9632 127.23 64.7811 242.00 35.4858 83.79 56.0000 127.91 61. 9950 244.70 17.7935 84. 00. 57.1941 129.30 48.7565 252.40 0.0000 85.43 67.9186 . 131. 20 65.2161 252.80 26.9154 86.55 64.5673 133. 02 43.2875 254.15 0.0000 86.79 68. 7124 133. 52 41.3977 256.23 31. 5111 86.94 68.7356 136.00 41. 2435 260.90 0.0000 ..J Page 3721of5809
ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 26.1038 355.39 0.0000 584.27 6.6440 264.80 26.1073 356.01 19.6787 595.83 0.0000 265.00 22.7063 364.49 0.0000 427.87 12.9238 268.22 24. 2969 366.42 0.0000 602.52 0.0000 269.46 34. 2.096 372. 51 23.6688 604.72 2.8781 270.03 34.2279 375.05 22.4665 607.14 0.0000 271.23 31.9836 377.52 23.3419 609.32 11. 5396 273.65 0.0000 356.01 16.7517 610.33 11. 5454 276.40 26.4035 388.16 15. 9648 614.28 13.0150 277.37 16.0867 388.63 0.0000 618.01 9.6590 277.60 19.5380 391.69 12.6364 620.36 9.6704 278.00 25.2945 264.66 24.5897 621. 93 7.7425 279.20 29 .'9276 401.81 18.6699 630.19 0.0000 279.54 28.7857 402.40 22.9224 631.29 14.5856 279.70 26.4871 404.85 19.3906 633.25 13.6263 280.46 11.5244 410.95 . 13.6663 634.78 0 . .0000 283.69 21. 9630 413.71 20.5391 635.95 8.7715 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 18.5249 423.72 0.0000 645.85 6.8556 285.90 0.0000 427.09 15.5475 657.76 9.8507 287.50 18.5610 427.87 16.4201 657:90 0.0000 290.67 17.0644 433.94 14.7522 661.66 10.8559 293.27 0.0000 439.40 12.1933 664.57 0.0000 351.93 '26. 4823 453.88 11. 4308 ' 666. 33 0.0000 295. 96 26.4996 463.37 13.2703 666.50 0.0000 879.38 16.4063 468.07 14.6413 667. 71 0.0000 299.98 14.0804 473.00 0.0000 677.62 9.9443 300.09 14.0819 475.06
12.4779 685.70 0.0000 300 .13 14.0823 476.78 12.4913 695.00 0.0000 301.36 14.0977 477.60 15.1756 696.49 13. 0418 302.85 23.5278 .482.18 15.2188 696. 51 13.0418 256.23 29.8452 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.0501 306.78 15.7402 497.08 9.9376 697.49 14.0513 308.46 9.4580 505.52 9.5342 702.65 8.0482 311. 90 22.5306 507.63 0.0000 706.68 8.0632 316.51 22.6205 511. 00 11. 8427 711. 68 10.1017 319.41 0.0000 514.00 11.8638 720.70 0.0000 320.08 0.0000 514.00 11.8638 721. 93 0.0000 321. 04 22.7086 520.40 14.2898 722. 78 6.0913 323.87 28.7542 520.69 0.0000 722. 91 10.6602 325.23 32.3855 522.65 0.0000 723. 31 12.1855 328.76 0.0000 527.90 0.0000 724.19 9.1428 333.37 25.7630 528.26 13.2510 727. 33 8.1383 333.97 27.3870 529.59 11.0508 733.00 9.1783 334.37 27. 3960 529.87 0.0000 735.93 13.2751 338.28 26. 6762 531.02 0.0000 333.97 10.2185 338.32 26. 6769 537. 2 6 0.0000 739.50 0.0000 311. 90 .29.1533 546.56 0.0000 747.24 9.2358 340.48 29.1533 552.55 13. 0612 748.06 9.2391 340.55 0.0000 563.25 12.6689 752.31 12. 3413 344.28 29.2434 569.33 13.1820 753.82 0.0000 345.93 22.7751 946.00 13 .1831 756.73 7.2131 351.06 14.7015 569.70 14.1260 756.80 6.1826 351. 93 *14.7118 583.19 6.6403 884.68 11. 3697 Page 3722of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 11. 3787 1274.44 5.6460 1620.50 1.0057 766.42 12.4165 1001.03 3.3931 1621. 92 1.0060 766.84 8.2790 1002.74 11.3167 1678.03 0.0000 772. 60 0.0000 1004.73 13.5894 1690.97 2.0430 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1. 0377 778.90 9.3615 1028.54 0.0000 1063.66 3 .1166 783.70 0.0000* 1037.84 6.8706 1771. 35 2.0782 785.37 13.5586 1038.76 0.0000 1791.20 0.0000 792.07 9.4131 631.29 8.0385 1808.65 1. 0472 794.95 7.3298 1048.07 0.0000 1810.72 0.0000 795.86 6.2852 1049.04 6.8955 1836.06 2.1061 810.06 10.5363 1050.41 3.4495 810.29 8.4297 1063.66 5.7739 344.28 7.3765 1077.00 0.0000 810.76 10.5391 1077.34 4.6393 815.77 0.0000 1085.87 8.1410 1048.07 0.0000 1093.63 4.6634 832.01 8.5036 1099.45 5.2562 834.85 7.4492 1112. 07 4.3973 835.71 11. 7099 1112. 84 4.0215 836.80 0.0000 1115. 54 8.4521 846.75 0.0000 1120. 29 7.0537 846.77 8.5534 1120.55 7.0542 856.80 0.0000 1221.41 7.0562 860.56 .7.5244 1129. 67 7.0742 871.09 "9. 7134 1131. 51 0.0000 873.19 9.7211 1147.95 0.0000 875.33 0.0000 1173.23 4.4800 879.38 5.4134 1177.95 10.7673 880.51 8.6650 1189.05 6.3015 883.24 3.2528 1204.77 7.2349 884.68 4.3394 1221. 41 5.4525 889.28 5.4338 1231.02 8.2013 894.76 7.6229 1235.36 0.0000 898.04 8.1772 1238.28 10.0446 900. 72 8.1854 1260.41 0.0000 903.28 0.0000 1271.87 8.2958 911. 20 5.4781 1274.44 4.4276 912.08 5.4799 1274.54 4.4279 923.98 0.0000 1291.59 7.4146 926.50 7.7124 1298.22 0.0000 929 .11 11.0282 1312 .11 0.0000 937.49 4.4246 1332.49 7. 4971 944.13 0.0000 1362.66 0.0000 946.00 3.3286 1365.19 3.7810 949.00 14.4393 1368.63 0.0000 667. 71 0.0000 1384.29 2.8499 962. 31 5.0219 1408.01 4.7787 964.08 8.3749 1457.56 0.0000 966.17 18.4383 1460.82 2.9055 911. 20 16.7786 1489.16 3.9009 968. 97 16.7786 1505.03 2.9370 983.53 0.0000 1584.12 3.9895 984.45 0.0000 1596.21 0.0000 Page 3723of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:19:12.36 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;l19 Background date : Z-OCT-2016 11:02:18. Sample date 30-NOV-2015 11:19:00 Acquisition date : 3-0CT-2016 09:17:13. Sample ID G405235037* Sample quantity 1.78756E+02 GRAM Detector name GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:05.72 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity -3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2-5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3724of5809 Energy 46.55* 61.13 63.48* 74.97* 77.27* 87.41 90.02 93.06* 143.25* 186.02* 210.01 230.38 238.99* 242.05 277.81 286.06 296.16 301.08 322.00 329.47* 338.97 352.20* 444.91 462.81* 511.40* 583.76* 609.85* 620.72 679.71 728.45* 767.97 886.62* 912.01* 965. 51 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 39 .25 82 179 223 92 62 110 24 101 26 23 275 81 33. 22 90 19 19 14 38 187 11 39 31 77 120 19 8 17 37 6 43 25 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 87 121 111 168 109 79 94 130 112 95 83 52 70 44 40 57 62 70 44 52 58 55 18 21 38 32 32 15 18 20 37 4 10 12 0.98 1. 32 1. 04 1.14 0.85 1.12 1.19 1.18 3.86 1. 20 0.92 0.87 0.95 1. 50 1. 63 0.89 1. 27 1. 00 1. 82 0.89 0.92 1.14 1. 41 1. 42 1. 23 1. 53 1. 68 2.75 0.83 1.12 6.58 0.65 1.13 1. 69 93.39 122.54 127.24 _150.21 154.81 175.10 180.30 186. '.39 286.74 372.24 420.23 460.95 478.17 484.29 555.80 572.28 592.49 602.32 644.16 659.08 678.08 704.55 .889.94 925.74 1022.90 1167. 60 1219.79 1241.53 1359.50 1456.98 1536.03 1773.35 1824.14 1931.15 90 120 120 145 145 173 178 183 281 365 415 458 473 482 552 568 584 596 637 653 674 699 886 919 1016 1159 1211 1234 1353 1450 1520 1770 1817 1925 7 1. 09E-02 47. 4 18 6.90E-03 69.8 18 2.27E-02 25.8 15 4. 96E-02 13. 8 15 6.19E-02 9.9 5 2.56E-02 17.8 6 1. 72E-02 27. 9 10 3.06E-02 24.4 11 6.73E-03 89.4 14 2.81E-02 23.8 9 7.llE-03 67.3 8 6.36E-03 57.8 9 7.65E-02 8.3 7 2.24E-02 17.8 9 9.03E-03 38.7 10 6.08E-03 68.1 11 2.50E-02 19.6 12 5.26E-03 90.9 11 5.28E-03 71.4 9 3.80E-03101.0 12 1.04E-02 44.3 13 5.19E-02 11.0 7 3.05E-03 72.2 12 l.09E-02 29.6 14 8.63E-03 54.5 14 2.15E-02 19.5 14 3.35E-02 13.7 12 5.24E-03 47.1 9 2.22E-03101.9 10 4.70E-03 56.2 24 1. 03E-02 45. 7 7 l.55E-03 78.4 12 1.20E-02 21.4 12 7.02E-03 33.8 Fit 1. 95E+OO 3.45E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969.88* 38 7 1. 57 1939.89 1936 9 1. 05E-02 21. 9 36 0 1053.89 15 0 2.39 2107.93 2103 9 4.17E-03 25.8 37 0 1121.45 26 15 1. 57 2243.08 2235 12 7.16E-03 36.0 38 0 1204.21 9 26 5.89 2408.65 2390 21 2.46E-03148.2 39 0 1207.05 *15 5 1. 54 2414.33 2410 10 4.17E-03 38.0 40 0 1237.81 22 7 3.75 2475.86 2469 14 6. llE-03 33.2 41 0 1264.29 10 5 0.78 2528.85 2521 13 2.65E-03 63.0 42 0 1461.78* 275 0 1. 92 2923.96 2917 14 7.63E-02 6.1 43 0 1766.23 18 3 2.53 3533.15 3527 11 5.05E-03 29.4 Flag:* "*" = Peak area was modified by background subtraction Page 3725 of 5809 VMS Nuclide Identification Report V3 .1 Generated 3-0CT-2016 .10: 19: 14 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 11:19:00 G405235037 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:17:13 178.76 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA41 0 01:00:00.00 1. 50 keV No Empirical 75.00 . Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3726 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:05.72 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff *pci/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.926E-01 1.191E+Ol 1.191E+Ol 12.18 OK Y-91 1204.77 0. 26* l.058E+OO 1. 372E+Ol 5.267E+02 296.36 OK RH-106 621.93 9.93* 1.938E+OO 4.592E-01 8.153E-01 94.29 OK 1050.41 1. 56 1.196E+OO Line Not Found Absent RU-106 621.93 9.93* 1.938E+00 4.592E-01 8.153E-01 94.29 OK 1050.41 1. 56 1.196E+OO Line Not Found Absent CD-109 88.03 3.70* 7.447E+00 1.367E+OO 2 .172E+OO 55.08 OK SN-126 . 64.28 9.60 7.794E+00 6.753E-01 6.753E-01 51. 53 OK 86.94 8.90 7.447E+00 5.685E-01 5.685E-01 55.08 OK 87.57 37.00* 7.447E+00 l.367E-01 l.367E-01 55.08 OK HG-203 70.83 3.69 7.737E+00 Line Not Found Absent 72. 87 6.19 7. 711E+OO Line Not Found Absent 279.20 81.56* 3.902E+OO 3.626E-02 3.541E+OO 115. 06 OK TL-208 277.37 6.60 3.907E+OO Line Not Found <<INT Reject 583.19 85.00* 2.050E+OO 2.099E-01 2.099E-01 38.95 OK 860.56 12.50 l.434E+OO Line Not Found Absent PB-210 46.54 4.25* 7.553E+OO 7.803E-01 8. OllE-01 94.74 OK BI-211 72.87 1. 23

7. 711E+OO Line Not Found Absent 351.06 12.92* 3.212E+OO 4.002E-01 4.002E-01 222.31 OK PB-212 74.82 10.28 7.681E+OO 9. 891E-01 9.891E-01 41. 37 OK 77 .11 17.10 7.644E+OO 1.032E+OO i.032E+OO 19.74 OK 238.63 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 OK 300.09 3.30 3.659E+OO 8.094E-01 8.094E-01 181.75 OK BI-214 609.32 45.49* 1. 969E+00 6.315E-01 6.317E-01 27.31 OK 1120.29 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent PB-214 74.82 5.80 7.683E+OO Line Not Found <<INT Reject 77 .11 9.70 7.644E+OO 1.819E+OO 1.820E+OO 19.74 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3.708E+OO 6.813E-01 6.816E-01 39.20 OK 351.93 35.60* 3.214E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 OK 1120. 29 14.92 1.127E-f00 6.586E-01 6.589E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent RA-224 240.99 4.10* 4.340E+OO 1.197E+OO 1.197E+OO 81. 47 OK RA-226 609.32 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 OK 1120. 29 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent AC-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11.27 3.317E+OO 5.105E-01 5.105E-01 88.51 OK 794.95 4.25 1.543E+OO Line Not Found Absent 835. 71 1. 61 1.473E+OO Line Not Found Absent 911. 20 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 OK 968. 97 15.80 1.285E+OO 8.194E-01 8.194E-01 43.89 OK RA-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 OK 794.95 4.25 1.543E+OO Line Not Found Absent 835.71 1. 61 1. 473E+OO Line Not Found Absent Page 3727of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 25.80* l.360E+OO 5.447E-01 5.447E-01 42.74 OK 968. 97 15.80 1.285E+OO 8 .,194E-01 8.194E-01 43.89 OK TH-228 74.82 10.28 7.681E+OO 9.891E-01 9.891E-01 41. 37 OK 77 .11 17.10 7.644E+OO 1.032E+OO 1.032E+OO 19.74 OK 238.63 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 OK 300.09 3.30 3.659E+OO 8.094E-01 8.094E-01 181. 7 5 OK TH-230 609.32 45.49* 1. 969E+OO 6. 315E....:01 6.315E-01 27.31 OK 1120. 29 14.92 1.127E+OO 6.586E-01. 6.586E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.659E+OO 4.993E-01 4.993E-01 181. 75 OK TH-232 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 OK 835.71 1. 61 l.473E+00 Line Not Found Absent 911.20 25.80* l.360E+00 5.447E-01 5.447E-01 42.74 OK 968. 97 15.80 1.285E+OO 8.194E-01 8.194E-01 43.89 OK TH-234 63.29 3.70* 7.794E+OO 1.752E+OO 1.752E+OO 51. 53 OK 92.59 4.23 7.320E+OO 2.112E+00 2 .112E+OO 48.79 OK U-234 609.32 45.49* 1. 969E+00 6.315E-01 6.315E-01 27.31 OK 1120. 29 14.92 1.127E+OO 6.586E-01 6.586E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Ab"sent U-235 89. 96 3.47 7.390E+OO 1.435E+OO 1.435E+OO 55.85 OK 93.35 5.60 7.320E+OO 1.595E+00 1. 595E+OO. 48.79 OK 143.76 10. 96* 6.105E+OO 2.047E-01 2.047E-01 178.90 OK 163.33 5.08 5.667E+OO Line Not Found Absent 185.72 57.20 5.223E+OO 1.858E-01 1.858E-01 47.55 OK 205.31 5.01 4.887E+OO Line Not Found Absent U-238 63.29 3.70* 7.794E+00 1. 752E+OO l.752E+00 51. 53 OK 92.59 4.23 7.320E+OO 2.112E+OO 2 .112E+OO 48.79 OK AM-243 43.53 5.90 7.421E+OO Line Not Found Absent 74.66 67.20* 7. 681E+OO 1.513E-01 1. 513E-01 41. 37 OK ANH-511 511. 00 100.00* 2. 313E+00 6.463E-02 6. 463.E-02 108.92 OK Flag: "*" = Keyline Page 3728 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l * *Acquisition date 3-0CT-2016 09:17:13 Sensitivity : 3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: O 01:00:05.72 Half life ratio : ***** *
Sample date 30-NOV-2015 11:19:00 Analyst initials: MXRl * *Sample ID G405235037 Sample Quantity 1.7876E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.191E+Ol 1.422E+OO Y-91 5.267E+02 l.530E+03 RH-106 8.153E-01 7.533E-01 RU-106 8.153E-01 7.533E-01 CD-109 2. l 72E+OO 1. l 72E+OO SN-126 l.367E-01 7.381E-02 HG-203 3.541E+OO 3.993E+OO TL-208 2.099E-01 8.012E-02 PB-210 8. OllE-01 7.438E-01 BI-211 4.002E-01 8.719E-01 PB-212 7.662E-01 l.243E-01 BI-214 6.317E-01 1.691E-01 PB-214 8.269E-01 1. 779E-01 RN-222 6.317E-01 l.691E-01 RA-224 1.197E+OO 9.555E-01 RA-226 6.317E-01 1. 691E-01 AC-228 5.447E-01 2. 281E-01 RA-228 5.447E-01 2.281E-01 TH-228 7.662E-01 l.243E-01 TH-230 6.315E-01 l.690E-01 PA-231 4.993E-01 8.893E-01 TH-232 5.447E-01 2.281E-01 TH-234 1. 752E+OO 8.849E-01 U-234 6.315E-01 l.690E-01 U-235 2.047E-01 3.589E-01 U-238 1. 752E+OO 8.849E-01 AM-243 1.513E-:-01 6.135E-02 ANH-511 6.463E-02 6.899E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3729 of 5809 Key-Line Activity (pCi/GRAM 4. 951E+OO 2.148E-02 K.L. Cnt Uncert ( 1. 96-sigma) l.183E+Ol MDA (pCi/GRAM 4.971E-01 1.627E+02 9.015E-01 9.015E-01 1.205E+OO 8.663E-02 4.637E+OO 6.035E-02 6. 551E-01 3.181E-01 8.523E-02 1.118E-01 2.782E-01 1.118E-01 8.243E-01 l.118E_..:01. 2.023E-01 2.023E-01 8.523E-02 1.118E-01 6.810E-01 2.023E-01 8.832E-01 1.118E-01 2.927E-01 8.832E-01 4.876E-02 4.164E-02 MDA (pCi/GRAM 2.443E+Ol 1.189E-01 NOT IDENT. NOT IDENT.

NA-24 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -9.950E-03 2.081E-02 4.180E-02 NOT IDENT. SC-46 1.846E-02 3.663E-01 6.833E-01 FAIL ABUN V-48 O.OOOE+OO l.675E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 4.474E+02 O.OOOE+OO SHORT HLIF MN-54 -l.910E-02 5.795E-02 1.123E-01 NOT IDENT. C0-56 l.179E-01 5.198E-01 l.079E+OO FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 9.342E-04 3.829E-02 7.865E-02 NOT IDENT. C0-58 -3.216E-01 5.118E-01 9.465E-01 NOT IDENT. FE-59 4.637E-01 6.280E+OO 1.318E+Ol NOT IDENT. C0-60 -1.435E-02 3.329E-02 6.186E-02 NOT IDENT. ZN-65 5.808E-02 l.972E-01 3.692E-01 NOT IDENT. GE-68 4.767E-01 2.351E+OO 4.899E+OO NOT IDENr. AS-73 5.366E-01 2.lOOE+OO 4 .135E+OO NOT IDENT. AS-74 0.000E+OO 6.310E+03 O.OOOE+OO SHORT HLIF SE-75 -5.786E-02 1.594E-01 3.076E-01 NOT IDENT. BR-77 O.OOOE+OO 2.365E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.176E+02 0.000E+OO SHORT HLIF RB-83 2.332E-02 5.549E-01 l.101E+OO NOT IDENT. KR-85 9.059E+OO 6.785E+OO l.426E+Ol NOT IDENT. SR-85 1.041E+OO 7.804E-01 1. 640E+OO NOT IDENT. RB-86 O.OOOE+OO 3. 723E+04 O.OOOE+OO SHORT HLIF Y-88 -7.732E-02 1.lOOE-01 l.512E-01 NOT IDENT. NB-94 3.035E-03 3.221E-02 6.550E-02 NOT IDENT. NB-95 9.359E-01 8. 413E-01 1.948E+OO NOT IDENT. NB-95M -8. 811E-01 2.324E+OO 3.952E+00 NOT IDENT. ZR-95 -3.235E-01 1.504E+OO 2.758E+OO NOT IDENT. NB-97 0. OOOE+OO -1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.268E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -1.423E-02 2.746E-02 5.414E-02 NOT IDENT. RH-102 4.448E-03 4.258E-02 9.179E-02 FAIL ABUN RU:._103 6.983E-01 4.765E+OO 9.746E+00 FAIL ABUN AG-108M 9.877E-03 2.190E-02 4.602E-02 NOT IDENT. AG-llOM -1.078E-01 1.126E-01 1.638E-01 FAIL ABUN SN-113 -1.763E-01 2.004E-01 3.466E-01 NOT IDENT. CD-115 O.OOOE+OO 3.426E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.131E+05 O.OOOE+OO SHORT HLIF TE-123M -8.763E-02 1.073E-01 2.037E-01 NOT IDENT. SB-124 -1.014E+OO 1.570E+OO 2.882E+OO NOT IDENT. SB-125 6. 964E-02 8.785E-02 1.897E-01 FAIL ABUN TE-125M -1.005E+Ol 2.120E+02 4.356E+02 NOT IDENT. I-126 O.OOOE+OO 1.283E+0*6 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 709E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.987E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.087E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.020E+27 O.OOOE+OO SHORT HLIF BA-133 1. 961E-03 3.948E-02 6.973E-02 FAIL ABUN I-133 0.000E+OO l.580E+41 O.OOOE+OO SHORT HLIF CS-134 2.644E-02 4.629E-02 1.015E-01 NOT IDENT. CS-135 5.875E-02 1.113E-01 2.332E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.886E+05 O.OOOE+OO SHORT HLIF BA-137M 1.295E-02 3.584E-02 7.557E-02 NOT IDENT. CS-137 l.368E-02 3.786E-02 7.983E-02 NOT IDENT. CE-139 -4.497E-02 9.740E-02 1.898E-01 NOT IDENT. BA-140 O.OOOE+OO 2.103E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.695E+05 O.OOOE+OO SHORT HLIF CE-141 5. 951E+OO 2.498E+Ol 4.682E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 3.493E-02 2.796E-01 5.776E-01 NOT IDENT. PM-144 2.328E-02 5.124E-02 1.105E-01 NOT IDENT. PR-144 2.387E+OO 4.422E+OO 9.645E+OO NOT IDENT. PM-146 -3.748E-03 3.535E-02 6.848E-02 , NOT IDENT. ND-147 0.000E+OO 5.077E+07 O.OOOE+OO SHORT HLIF PM-147 3.548E+02 6.434E+02 1.369E+03 NOT IDENT. PM-1°49 0.000E+OO 1.335E+41. O.OOOE+OO SHORT HLIF EU-150 2.641E-03 2.134E-02 4.085E-02 FAIL ABUN EU-152 2. 960E-02 8.183E-02 1.533E-01 FAIL ABUN GD-153 -4.303E-02 1.307E-01 2.376E-01 NOT IDENT. EU-154 6.833E-02 1.393E-01 2.917E-01 NOT IDENT. EU-155 6.519E-02 7.019E-02 1.551E-01 FAIL ABUN TB-160 1.995E+OO 4.307E+OO FAIL ABUN H0-166M 2.744E-03 5.261E-02 1.080E-01 NOT IDENT. TM-171 6.914E-01 4.234E+OO 8.305E+OO NOT I DENT*. Page 3730of5809 HF-172 -6.034E-02 1. 846E-01 3.675E-01 . FAIL ABUN LU-172 8.908E-03 7.132E-02 l.480E-01 FAIL ABUN LU-176 -3.688E-03 1. 887E-02 3.673E-02 FAIL ABUN HF-181 -1. 08 6E+OO 4. lllE+OO 7.737E+OO NOT IDENT. TA-182 8.428E-01 1.028E+OO 2.265E+OO FAIL ABUN RE-183 -3.351E-01 9.872E-01 l.693E+OO NOT IDENT. RE-184 -9.713E+OO 2.597E+Ol 5.073E+Ol NOT IDENT. W-188 -6.489E+Ol l.449E+02 1.820E+02 FAIL ABUN IR-192 2.320E-01 4.392E-01 8.425E-01 FAIL ABUN BI-207 -9.682E-03 5.354E-02 1.030E-01 FAIL ABUN PB-211 4. 972E-02 5.259E-01 l.051E+OO NOT IDENT. BI-212 6.954E-01 7.661E-01 1. 202E+OO FAIL ABUN RN-219 -3.126E-01 3.188E-01 5.408E-01 NOT IDENT. RA-223 -6.418E-Ol 7.388E-01 7.995E-01 FAIL ABUN AC-227 -4.557E-02 l.756E-01 3.421E-Ol FAIL Al3UN TH-227 -4.557E-02 1. 756E-Ol 3.421E-01 FAIL ABUN TH-229 -8.083E-02 3. 831E-01 7.562E-Ol FAIL ABUN TH-231 -6.418E-01 7.388E-01 7.995E-01 FAIL ABUN PA-233 l.631E-02 4.587E-02 9.512E-02 FAIL ABUN PA-234 -2.836E-01 2.629E-01 4.289E-01 NOT IDENT. PA-234M 3.633E+OO 4.330E+OO 9.626E+OO NOT IDENT. NP-237 1. 631E-02 4.587E-02 9.512E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -4.034E-02 1. 757E-01 3.567E-01 FAIL ABUN PU-239 1.881E+o2 2.415E+02 5.190E+02 NOT IDENT. AM-241 1.506E-02 4.595E-02 8.377E-02 NOT IDENT. CM-243 -3.773E-02 6.573E-02 l.310E-01 FAIL ABUN BK-247 -4*. 058E-02 5.590E-02 1. 029E-01 'NOT IDENT. CM-247 -2.013E-02 2.738E-02 4. 834E-02 . FAIL ABUN CF-249 3.363E-02 3.060E-02 6.815E-02 NOT IDENT. CF-251 2.247E-02 9.675E-02 l.983E-01 FAIL ABUN /, Page 3731of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:19:13.13 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 270 10.66* 8.926E-01 1.191E+Ol 1.191E+Ol 12.18 Y-91 1204.77 9 0. 26* 1.058E+OO 1.372E+Ol 5.267E+02 296.36 RH-106 621.93 21 9.93* l.938E+OO 4.592E-01 8.153E-01 94.29 1050.41 ------1. 56 l .196E+OO ------Line Not Found ------RU-106 621. 93 21 9.93* 1.938E+OO 4.592E-01 8.153E-01 94.29 1050.41 ------1. 56 1.196E+OO ------Line Not Found ------CD-109 88.03 131 3.70* 7.447E+OO 1. 995E+OO 3.169E+OO 35.67 SN-126 64.28 120 9.60 7.794E+OO 6.753E-01 6.753E-01 51. 53 86.94 131 8.90 7.447E+OO 8.295E-01 8.295E-01 35. 67 87.57 131 37.00* 7.447E+OO l.995E-01 l.995E-01 35.67 HG-203 70.83 ------3.69 7.737E+OO ------Line Not Found ------72. 87 ------6.19 7. 711E+00 ------Line Not Found ------279.20 40 81.56* 3.902E+OO 5.325E-02 5.199E+00 77.37 TL-208 277.37 40 6.60 3.902E+OO 6.580E-01 6.580E-01 77.37 583.19 87 85.00* 2.050E+OO 2.099E-01 2.099E-01 38.95 860.56 ------12.50 1.434E+OO ------Line Not Found ------PB-210 46.54 60 4.25* 7.553E+00 7 .. 803E-01 8. OllE-01 94.74 BI-211 72. 87 ------1. 23 7.711E+OO ------Line Not Found ------351.06 225 12.92* 3.212E+OO 2.277E+OO 2.277E+OO 21. 96 PB-212 74.82 258 10.28 7.681E+OO l.373E+00 1.373E+OO 27.70 77 .11 321 17.10 7.644E+00 1.032E+OO l.032E+00 19.74 238.63 348 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 300.09 23 3.30 3.659E+OO 8.094E-01 8.094E-01 181. 75 BI-214 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 1120.29 26 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------PB-214 74.82 258 5.80 7. 681E+OO 2.434E+OO 2.435E+OO 27.70 77 .11 321 9.70 7.644E+OO 1.819E+OO l.820E+00 19.74 87.09 131 3.41 7.447E+OO 2.165E+OO 2.166E+OO 35.67 242 .*oo 102 7.25 4.340E+OO 1.358E+OO 1.359E+OO 35.52 295.22 111 18.42 3.708E+00 6.813E-01 6.816E-01 39.20 351. 93 225 35.60* 3.212E+00 8.266E-01 8.269E-01 21. 96 RN-222 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 1120.29 26 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------RA-224 240.99 102 4.10* 4.340E+OO 2.402E+00 2.402E+OO 35.52 RA-226 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 1120.29 26 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 1764.49 ------15.30 7.620E-01 ------. Line Not Found ------AC-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 45 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 794.95 ------4.25 1.543E+OO ------Line Not Found ------835.71 ------1. 61 1. 473E+OO ------Line Not Found ------911. 20 45 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 968. 97 40 15.80 1. 285E+00 8.194E-01 8.194E-01 43.89 RA-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 45 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 Page 3732 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Nuclide Type: Uncorrected Decay Corr 2-sigrria Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 ------4.25 l.543E+OO ------Line Not Found ------835.71 ------1. 61 1. 473E+OO ------Line Not Found ------911. 20 45 25.80* l.360E+OO 5.447E-01 5.447E-01 42.74 968. 97 40 15.80 1.285E+OO 8.194E-01 8.194E-01 43.89 TH-228 74.82 258 10.28 7. 681E+OO 1.373E+OO l.373E+OO 27.70 77 .11 321 17.10 7.644E+OO 1.032E+OO l.032E+OO 19.74 238.63 348 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 300.09 23 3.30 3.659E+OO 8.094E-01 8.094E-01 181. 7 5 TH-230 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.315E-01 27.31 1120.29 26 14.92 1.127E+OO 6.586E-01 6.586E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 3.838E+OO ------Line Not Found ------301.36 23 5.35* 3.659E+OO 4.993E-01 4.993E-01 181. 75 TH-232 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 45 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 835. 71 ------1. 61 l.473E+OO ------Line Not Found ------911. 20 45 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 96.8. 97 40 15.80 1.285E+OO 8.194E-01 8.194E-01 43.89 'TH-234 63.29 120 3.70* 7.794E+OO 1. 7 52E+OO 1. 752E+00 51. 53 92.59 156 4.23 7.320E+OO 2 .112E+OO 2 .112E+OO 48.79 U-234 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.315E-01 27. :n 1120.29 26 14.92 1.127E+OO 6.586E-01 6.586E-01 71. 98 .. 1764.49 ------15.30 7.620E-01 ------Line Not Found ------U-235 89.96 88 3.47 7.390E+00 1.435E+OO 1.435E+OO 55.85 93.35 156 5.60 7.320E+OO 1.595E+OO 1.595E+OO 48.79 143.76 33 10. 96* 6.105E+OO 2.047E-01 2.047E-01 178. 90 163.33 ------5.08 5.667E+OO ------Line. Not Found ------185.72 132 57.20 5.223E+OO 1.858E-01 1.858E-01 47.55 205.31 ------* 5.01 4.887E+OO ------Line Not Found ------U-238 63.29 120 3.70* 7.794E+OO 1. 7 52E+OO 1. 752E+OO 51. 53 92.59 156 4.23 7.320E+OO 2 .112E+OO 2 .112E+OO 48.79 AM-243 43.53 ------5.90 7.421E+OO ------Line Not Found ------74.66 258 67.20* 7.681E+OO 2.lOlE-01 2.lOlE-01 27.70 ANH-511 511. 00 36 100.00* 2.313E+OO 6.463E-02 6.463E-02 108.92 Flag: "*" Key line Page 3733of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Total number of lines in spectrum 43 Number of unidentified lines 8 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 Y-91 RH-106 RU-106 CD-109 SN-126 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 58.51D 371. 80D 371. 80D 461.40D 2.30E+05Y 46.59D' l.41E+l0Y 22.20Y 7.04E+08Y 1.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600.00Y l.41E+l0Y 1. 41E+l0Y l.41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 38.4 1. 78 1,78 1. 59 1. 00 97.6 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 T*otal Ac ti vi ty Grand Total Activity Uncorrected pCi/GRAM 1.191E+Ol l.372E+Ol 4.592E-01 4.592E-01 1.995E+OO l.995E-01 5.325E-02 2.099E-01 7.803E-01 2.277E+00 7.662E-01 6.315E-01 8.266E-01 6.315E-01 2. 402E+O.O 6.315E-01 5.447E-01 5.447E-01 7.662E-01 6*. 315E-01 4.993E-01 5.447E-01 1. 752E+OO 6.315E-01 2.047E-01 1.752E+OO 2.lOlE-01 6.463E-02 4.609E+Ol 4.609E+Ol Decay Corr pCi7GRAM 1.191E+Ol 5.267E+02 8.153E-01 8 .153E-01. 3.169E+OO 1.995E-01 5.199E+OO 2.099E-01 8. OllE-01 2.277E+OO 7.662E-01 6.317E-01 8.269E-01 6 .. 317E-01 2.402E+OO 6.317E-01 5.447E-01 5.447E-01 7.662E-01 6.315E-01 4.993E-01 5.447E-01 l.752E+00 6.315E-01 2.047E-01 1.752E+OO 2.lOlE-01 6.463E-02 5.661E+02 5.661E+02 81.40% Decay Corr 2-Sigma Error 0.145E+Ol 15.61E+02 7.687E-01 7.687E-01 1.130E+OO 0.712E-01 4.023E+OO 0.818E-01 7.590E-01 0.500E+OO l.269E-01 1.725E-01 l.816E-01 l.725E-01 0.853E+OO 1. 725E-01 2.328E-01 2.328E-01 1. 269E-01 1. 725E-01 9.074E-01 2.328E-01 0.903E+00 1. 725E-01 3.662E-01 0.903E+OO 0.582E-01 7.040E-02 "M" Manually accepted 2-Sigma %Error 12.18 296.36 94.29 94.29 35. 67 35. 67 77.37 38.95 94.74 21. 96 16.56 27.31 21..96 27.31 35.52 27.31 42.74 42.74 16.56 27.31 181.75 42.74 51. 53 27.31 178.90 51. 53 27.70 108.92 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide. specific abn. limit Page 3734of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235037 Acquisition date : 3-0CT-2016 09:17:13 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 61.13 37 179 1. 32 122.54 120 18 6.90E-03 **** 7.80E+OO T 0 210.01 33 107 0.92 420.23 415 9 7. llE-03 **** 4.81E+OO T 0 230.38 29 66 0.87 460.95 458 8 6.36E-03 **** 4.50E+OO 0 286.06 27 71 0.89 572.28 568 10 6.08E-03 **** 3.81E+00 T 0 322.00 23 54 1. 82 644.16 637 11 5.28E-03 **** 3.46E+00 T 0 329.47 17 63 0.89 659.08 653 9 3.80E-03 **** 3.40E+OO T 0 444.91 13 21 1. 41 889.94 886 7 3.05E-03 **** 2.62E+OO 0 462.Bl 45 24 1. 42 925.74 919 12 1.09E-02 59.2 2.53E+OO T 0 679.71 9 20 0.83 1359.50 1353 9 2.22E-03 **** 1.78E+OO 0 728.45 18 22 1.12 1456.98 1450 10 4.70E-03 **** 1.67E+OO T 0 767.97 40 40 6.58 1536.03 1520 24 l.03E-02 91. 4 l.59E+OO T *o 886.62 6 4 0.65 1773.35 1770 7 l.55E-03 **** 1.40E+OO 0 965. 51 26 12 1. 69 1931.15 1925 12 7.02E-03 67.6 1.29E+OO T 0 1053.89 15 0 2.39 2107.93 2103 9 4.17E-03 51. 6 l.19E+OO 0 1207.05 15 5 1. 54 2414.33 2410 10 4.17E-03 76.0 1.06E+OO 0 1237.81 22 7 3.75 2475.86 2469 14 6. llE-03 66.5 l.03E+00 T 0 1264.29 10 5 0.78 2528.85 2521 13 2.65E-03 **** 1.0lE+OO 0 1766.23 17 3 2.53 3533.15 3527 11 5.05E-03 58.8 7. 61E-01 Flags: "T" = Tentatively associated Page 3735 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:19:27.21 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * *
**Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l * *Acquisition date 3-0CT-2016 09:17:13 Sensitivity : 3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:05.72 Half life ratio : ***** *
Sample date 30-NOV-2015 11:19:00 Nuclide Library : SOLID *
Sample ID G405235037 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKA100*: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 Y-91 RH-106 RU-106 CD-109 SN--,126 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-22.8 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM O.OOOE+OO 3.958E-Ol 3.958E-01 5.662E-01 4.102E-02 2 .131E+OO 2.676E-02 3.069E-01 1.445E-01 3. 941E-02 4.926E-02 1.339E-01 4.926E-02 3.778E-01 4.926E-02 8.443E-02 8.443E-02 3.941E-02 4.924E-02 3.094E-01 8.443E-02 4.195E-01 4.924E-02 1. 371E-Ol 4.195E-01 2.315E-02 l.823E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3736 of 5809 Le (pCi/GRAM 1.093E+Ol 5.224E-02 O.OOOE+OO NOT IDENT. NOT -IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 .CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3737of5809 1.321E-02 2.877E-01 O.OOOE+OO O.OOOE+OO 4.823E-02 4.756E-01 O.OOOE+OO 3.690E-02 3.937E-01 5.502E+OO 2.424E-02 l.603E-01 2.109E+OO 1.953E+OO O.OOOE+OO 1. 38 6E--'01 O.OOOE+OO O.OOOE+OO 4.812E-01 6.498E+OO 7.474E-01 O.OOOE+OO 1. 766E-02 2.932E-02 8.702E-01 1.819E+00 1.191E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.538E-02 3.939E-02 4.236E+OO 2.053E-02 6.831E-02 l.530E-01 O.OOOE+OO O.OOOE+OO 9.416E-02 9.109E-01 8.564E-02 2.039E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.163E-02 O.OOOE+OO 4.481E-02 1. 071E-01 O.OOOE+OO O.OOOE+OO 3. 411E-02 3.603E-02 8. 841E-02 O.OOOE+OO O.OOOE+OO 2.190E+Ol O.OOOE+OO 2.700E-01 4.909E-02 4.287E+OO 3.025E-02 O.OOOE+OO 6.434E+02 O.OOOE+OO l.852E-02 6.938E-02 l .115E-01 1.283E-01 7.274E-02 1.888E+OO 4.762E-02 3.913E+OO l.722E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT. I DENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 'AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3738 of 5809 6.306E-02 1. 656E-02 3.399E+OO 9.997E-01 7. 960E-01 2.070E+Ol 8.240E+Ol 3.836E-01 4.478E-02 4.694E-01 5.480E-01 2.385E-01 3.556E-01 1.556E-01 1.556E-01 3.506E-01 3.556E-01 4.312E-02 l.773E-01 4 . .256E+OO 4.312E-02 O.OOOE+OO 1.666E-01 2.441E+02 3. 960E-02 6.118E-02 4.642E-02 2.124E-02 3.098E-02 9.250E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:19:32.98 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l *
Acquisition date 3-0CT-2016 09:17:13 Sensitivity *
3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:05.72 Half life ratio : ***** *
Sample date 30-NOV-2015 11:19:00 Nuclide Library : SOLID *
Sample ID G405235037 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM *
Quantity Err(%) : 1.1188E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.191E+Ol 1. 747E+OO Y-91 5.267E+02 l.530E+03 RH-106 8.153E-01 7.574E-01 RU-106 8.153E-01 7.574E-01 CD-109 2.172E+OO 1.203E+OO SN-126 1.367E-01 7.540E-02 HG-203 3.541E+OO 4. 013E+OO TL-208 2.099E-01 8.210E-02 PB-210 8.0llE-01 7.505E-01 BI-211 4.002E-01 9.023E-01 PB-212 7.662E-01 1.440E-01 BI-214 6.317E-01 l.773E-01 PB-214 8.269E-01 1. 914E-*Ol RN-222 6.317E-01 1.773E-01 RA-224 1.197E+OO 9.744E-01 RA-226 6.317E-01 l.773E-01 AC-228 5.447E-01 2. 371E-01 RA-228 5.447E-01 2. 371E-01 TH-228 7.662E-01 l.440E-01 TH-230 6.315E-01 l.772E-01 PA-231 4.993E-01 8. 964E-01 TH-232 5.447E-01 2.371E-01 TH-234 1. 7 52E+OO 9.852E-01 U-234 6.315E-01 l.772E-01 U-235 2.047E-01 3*. 596E-01 U-238 1. 752E+OO 9.852E-01 AM-243 1. 513E-01 6.427E-02 ANH-511 6.463E-02 6.921E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3739of5809 Key-Line Activity (pCi/GRAM 4.951E+OO 2.148E-02 K.L Act error ( 1. 96-sigma) l.184E+Ol 5.788E-02 TPU ( 1. 96-sigma) 1. 7 4 7E+OO l.530E+03 7.574E-01 7.574E-'01 1.203E+OO 7.540E-02 4.013E+OO 8.210E-02 7.505E-01 9.023E-01 1.440E-01 1.773E-01 l.914E-01 1.773E-01 9.744E-01 1.773E-01 2.371E-01 2. 371E-01 1.440E-01 l.772E-01 8.964E-01 2.371E-01 9.852E-01 1. 772E-01 3. 596E-01 9. 852E.-01 6.427E-02 6. 921E-02 TPU ( 1. 96-sigma) l.204E+Ol NOT IDENT. 5.868E-02 NOT IDENT.

NA-24 1.000E+41 2.350E+41 O.OOOE+OO SHORT HLIF AL-26 -9.950E-03 2.083E-02 2 .131E-02 NOT IDENT. SC-46 l.846E-02 3.663E-01 3.664E-01 FAIL ABUN V-48 2 .110E+03 1. 676E+04 1.678E+04 SHORT HLIF CR-51 3.204E+02 4.482E+02 4.709E+02 SHORT HLIF MN-54 -l.910E-02 5.798E-02 5.862E-02 NOT IDENT. C0-56 l.179E-01 5.199E-01 5.226E-01 FAIL ABUN MN-56 l.000E+41 4.410E+41 O.OOOE+OO SHORT HLIF C0-57 9.342E-04 3.829E-02 3.829E-02 NOT IDENT. C0-58 -3.216E-01 5.128E-01 5.329E-01 NOT IDENT. FE-59 4.637E-01 6.280E+OO 6.284E+OO NOT IDENT. C0-60 -1.435E-02 3.331E-02 3.393E-02 NOT IDENT. ZN-65 5.808E-02 l.975E-01 l.992E-01 NOT IDENT. GE-68 4.767E-01 2.352E+OO 2.362E+OO NOT IDENT. AS-73 5.366E-01 2.104E+OO 2 .118E+OO NOT IDENT. AS-74 -2.462E+03 6.315E+03 6.412E+03 SHORT HLIF. SE-75 -5.786E-02 l.595E-01 l.616E-01

NOT IDENT. BR-77 l.458E+39 1. 296E+40 O.OOOE+OO SHORT HLIF SR-82 -2.573E+Ol 7.176E+02 7.177E+02 SHORT HLIF RB-83 2.332E-02 5.549E-01 5.550E-01 NOT IDENT. KR-85 9.059E+OO 6.829E+OO 7.957E+OO NOT IDENT. SR-85 1. 041E+OO 7.855E-01 9.150E-01 NOT IDENT. RB-86 2.215E+04 3.742E+04 3.873E+04 SHORT HLIF Y-88* -7.732E-02 l.102E-01 l.155E-01 NOT IDENT. NB-94 3.035E-03 3.221E-02 3.224E-02 NOT IDENT. NB-95* 9.359E-01 8.460E-01 9.453E-01 NOT IDENT. NB-95M -8. 811E-01 2.326E+OO 2.360E+OO NOT IDENT. ZR-95 -3.235E-01 1.505E+OO 1.512E+OO NOT IDENT. NB-97 l.OOOE+41 2.243E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 6. 296E+41 0.000E+OO SHORT HLIF M0-99 8.364E+32 1. 271E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 8.473E+42 O.OOOE+OO SHORT HLIF RH-101 -l.423E-02 2.762E-02 2.836E-02 NOT IDENT. RH-102 4.448E-03 4.258E-02 4.263E-02 FAIL ABUN RU-103 6.983E-01 4.765E+OO 4.776E+OO FAIL ABUN AG-lOffM 9.877E-03 2.192E-02 2.237E-02 NOT IDENT. AG-llOM -1.078E-01 1.132E-01 l.232E-01 FAIL ABUN SN-113 -1. 7 63E-01 2.009E-01 2.160E-01 NOT IDENT. CD-115 -4.606E+39 3.427E+40 O.OOOE+OO SHORT HLIF SN-117M l.469E+04 l.131E+05 l.133E+05 SHORT.HLIF TE-123M -8.763E-02 1.076E-01 l.146E-01 NOT IDENT. SB-'124 -1.014E+OO 1. 572E+OO 1.637E+OO NOT IDENT. SB-125 6. 964E-02 8.804E-02 9.347E-02 FAIL ABUN TE-125M -1.005E+Ol 2.120E+02 2 .121E+02 NOT IDENT. I-126 6.486E+05 1.287E+06 l.320E+06 SHORT HLIF SB-126 -9.864E+05 1.721E+06 1. 778E+06 SHORT HLIF SB-127 -4.399E+22 9.354E+22 O.OOOE+OO SHORT HLIF I-131-1. 201E+09 8.088E+09 SHORT HLIF I-132 1.000E+41 1.909E+42 O.OOOE+OO SHORT HLIF TE-132 -7.918E+25 2.021E+27 O.OOOE+OO SHORT HLIF BA-133 1. 961E-03 3.949E-02 3.949E-02 FAIL ABUN I-133 1.000E+41 2.440E+41 O.OOOE+OO SHORT HLIF CS-134 2.644E-02 4.637E-02 4.787E-02 NOT IDENT. CS-135 5.875E-02 l .115E-01 l.146E-01 NOT IDENT. I-135 -1. OOOEi-41 8.129E+41 O.OOOE+OO SHORT HLIF CS-136 2.405E+05 4.907E+05 5.026E+05 SHORT HLIF BA-137M 1.295E-02 3.586E-02 3.633E-02 NOT IDENT. CS-137 1. 368E-02
3.788E-02 3.838E-02 NOT IDENT. CE-139 -4.497E-02 9.789E-02 9. 996E-02 NOT IDENT. BA-140 2.016E+06 2 .110E+06 2.298E+06 SHORT HLIF LA-140 -6.821E+05 6. 716E+05 7.386E+05 SHORT HLIF CE-141 5. 951E+OO 2.499E+Ol 2. 513E+Ol NOT IDENT. CE-143 1.000E+41 7.079E+41 O.OOOE+OO SHORT HLIF CE-144 3.493E-02 2.797E-01 2.801E-01 NOT IDENT. PM-144 2.328E-02 5.129E-02 5.235E-02 NOT IDENT. PR-144 2.387E+OO 4. 4.27E+OO 4.556E+OO NOT IDENT. PM-146 -3.748E-03 3.535E-02 3.539E-02. NOT IDENT. ND-147 -1.141E+07 5.079E+07 5.105E+07 SHORT HLIF PM-147 3.548E+02 6.447E+02 6.643E+02 NOT IDENT. PM-149 l.OOOE+41 l.356E+41 O.OOOE+OO SHORT HLIF EU-150 2.641E-03 2.134E-02 2.138E-02 FAIL ABUN EU-152 2. 960E-02 8.188E-02 8. 296E-02 FAIL ABUN GD-153 -4.303E-02 1.308E-01 1.322E-01 NOT IDENT. EU-154 6.833E-02 l.394E-01 l.427E-01 NOT IDENT. EU-155 6.519E-02 7.057E-02 7.644E-02 FAIL ABUN TB-160 8.906E-01 l.998E+OO 2.038E+OO FAIL ABUN H0-166M 2.744E-03 5.261E-02 5.262E-02 NOT IDENT. TM-171 6.914E-01 4.235E+OO 4.246E+OO NOT IDENT. Page 3740 of 5809 HF-172 -6.034E-02 l.850E-01 l.870E-01 FAIL ABUN LU-172 8.908E-03 7.134E-02 7.146E-02 FAIL ABUN LU-176 -3.688E-03 1.887E-02 1.894E-02 FAIL ABUN HF-181 -l.086E+OO 4 .112E+OO 4.142E+OO NOT IDENT. TA-182 8.428E-01 1.030E+OO 1.098E+OO FAIL ABUN RE-183 -3.351E-01 9.894E-01 1. OOlE+OO NOT IDENT. RE-184 -9.713E+OO 2.610E+Ol 2.646E+Ol NOT IDENT. W-188 -6.489E+Ol l.452E+02 1. 481E+o2 FAIL ABUN IR-192 2.320E-01 4.397E-01 4.520E-01 FAIL ABUN BI-207 -9.682E-03 5.357E-02 5.374E-02 FAIL ABUN PB-211 4.972E-02 5.259E-01 5.264E-01 NOT IDENT. BI-212 6.954E-01 7.688E-01 8.303E-Ol FAIL ABUN RN-219 -3.126E-01 3.220E-01 3.515E-01 NOT IDENT. RA-223 -6.418E-01 7.415E-01 7.959E-01 FAIL ABUN AC-227 -4. 55*7E-02 1. 757E-01 1. 769E-01 FAIL ABUN TH-227 -4.557E-02 1. 757E-01 l.769E-01 FAIL ABUN TH-229 -8.083E-02 3.832E-01 3.849E-01 FAIL ABUN TH-231 -6.418E-01 7.415E-01 7.959E-01 FAIL ABUN PA-233 1. 631E-02 4.589E-02 4.648E-02 FAIL ABUN PA-234 -2.836E-01 4.190E-01 4.381E-01 NOT IDENT. PA-234M 3.633E+OO 4.361E+OO 4.659E+OO NOT IDENT. NP-237. 1.631E-02 4.589E-02 4.648E-02 FAIL ABUN NP-238 -1.000E+41 4.469E+41 O.OOOE+OO SHORT HLIF NP-239 -4.034E-02 l.758E-01 1. 768E-01 FAIL ABUN PU-239 1. 881E+02 2.425E+02 2.569E+02 NOT IDENT. AM-241 l.506E-02 4.600E-02 4.650E-02 NOT IDENT. CM-243 -3.773E-02 6.589E-02 6.805E-02 FAIL ABUN BK-247 -4.0SS'E-02 5.658E-02 5.947E-02 NOT IDENT. CM-247 -2.013E-02 2.762E-02 2.907E-02 FAIL ABUN CF-249 3.363E-02 3.082E-02 3.435E-02 NOT IDENT. CF-251 2.247E-02 9.680E-02 9.733E-02 FAIL ABUN Page 3741 of 5809
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Charleston, SC 29407 * * . GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 57.4984 87.09 123. 9638 136.47 72.5224 45.60 68.6647 87.57 106.5029 140.51 0.0000 46.54 73.8750 '88. 03 80.2402 143.76 72.1645 49.72 0.0000 88.34 80.2739 144.24 72 .1991 51. 35 91.1306 88.47 80.2876 145.44 64.2524 . 51. 87 101. 8809 89. 96 98.0457 152.43 77.2665 52.39 78.2630 1093.63 40.2603 153.25 0.0000 52.97 72. 4112 91.11 0.0000 323.87 53.9978 53.44 83.1661 92.59 78.2043 156.02 0.0000 54.07 89.2087 93.35 83.3318 158.56 0.0000 57.36 0 .*0000 94.56 83.4628 159.00 66.8969 57.53 110.1053 94.65 83.4723 162.33 52.5938 57.98 92.6242 94.67 83.4743 162.66 0.0000 59.27 89.6297 94.87 72 .1102 163.33 62.6253 59.32 89.6374 97.43 .86.3074 165.86 71. 8662 59.54 89.6713 98.43 73.1997 176.31 57.8429 60. 96 119.1815 98.44 73.2006 176.60 0.0000 61.17 119. 2234 99.53 64.4772 177. 52 59.7414 62.93 119.5741 100 .11 66.2219 181.07 0.0000 63. 29 119.6449 102.03 83.3998 181.52 56. 7185 63.58 119. 7023 103.18 73.2904 184.41 42.5274 64.28 119. 8396 103.37 79.2743 143.76 42.5742 66.73 120.3141 105.21 56.3847 193.51 58.6844 67.24 120.4123 105.31 56.3918 197.03 61.6548 125.81 107.1077 106.12 73.5515 198.01 67.3125 67.75 107 .1191 106.47 74.4382 201.83 60.0163 69.67 126.9777 109.28 68.6776 203.43 50.7030 70.83 100.2966 111. 00 86.8801 205.31 50.7777 72.81 107. 9610 111.76 0.0000 210.85 43.9140 72. 87 124.3303 114. 06 72.5126 215.65 43.6014 74.66 118 .1038 116.30 0.0000 222 .11 48.5762 74.82 118.1316 116.74 72.7339 227.09 40.1513 74.97 118.1580 119.76 72 .1116 227.38 41. 5941 77 .11 118. 5315 121.12 67.8695 228.16 0.0000 78.74 95.7097 121. 22 67. 8771 228.18 45.9238 79.69 99.1455 121.78 66.1776 116.74 45.9238 80.12 104.1669 122.06 76.6500 235.69 53.3885 80.19 0.0000 122.92 79.3380 235.96 53.3987 80.57 102.5790 123.07 83. 7109 238.63 50.6084 81. 00 92.7090 265.00 76.7861 238.98 0.0000 81. 07 92.7181 125.81 77.8379 240.99 40.5542 81. 75 132.5814 127.23 87.5910 242.00 40.5833 83 .. 79 97.2274 127.91 74.5071 244.70 30.4951 84.00 94.7623 129.30 65.8379 252.40 0.0000 85.43 123.2671 131.20 86.2016 252.80 35.0468 86.55 135.1343 133.02 67.8583 254 .15 0.0000 86. 79 135.1780 133.52 66.1301 256.23 38.0558 86.94 123.9388 136.00 63.6475 260.90 0.0000 Page 3742 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 33.3643 355.39 0.0000 584.27 20 .. 6689 264.80 40.2376 356.01 31.0870 595.83 0.0000 265.00 40.2426 364.49 0.0000 427.87 18.4857 268.22 33.4425 366.42 0.0000 602 .. 52 0.0000 269:46 30.5169 372.51 19.8620 604.72 26.0358 270.03 39.3913 375.05 28.2623 607.14 18.5306 271.23 44.3500 377.52 25.1543 609.32 18.5456 273.65 0.0000 356.01 25.2368 610.33 18.5527 276.40 38.5652 388.16 17.9152 614.28 6. 9673 277.37 33.6417 388.63 0.0000. 618.01 6.9768 277.60 33.6465 391.69 31. 6718 620.36 12.8020 278.00 33.6555 264.66 24.3912 621. 93 17.4670 279.20 43.0920 401.81 32.8940 630.19 0.0000 279.54 43.1017 402.40 27.5964 631.29 11.3921 279.70 50.5383 404.85 22.3168 633.25 12.2769 280.46 44.6136 410.95 27.7128 634.78 0.0000 283.69 40.2347 413.71 30.9523 635.95 21.9444 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 36.7975 423.72 0.0000 645.85 10.5707 285.90 0.0000 427.09 19.3359 657.76 19.4608 287.50 28.3811 427.87 18.2683 657.90 0.0000 2 90. 67 41.9077 433.94 17.2432 661. 66 21.2585 293.27 0.0000 439.40 22.6898 664.57 0.0000 351. 93 30.0183 453.88 20.6664 666.33 0.0000 295. 96 27.0286 463.37 -20.7554 666.50 0.0000 879.38 18.0480 468.07 26.2725 667. 71 0.0000 299.98 33 .1161 473.00 0.0000 677.62 15.6755 300.09 33 .1182 475.06 21.9617 685.70 0.0000 300.13 33 .1195 476.78 21. 9784 695.00 0.0000 301.36 33.1437 477.60 18.6882 696.49 16.1345 302.85 27.1423 482.'18 20.9289 696. 51 15.2382 256.23 39.2444 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.0355 306.78 31.2371 497.08 13.3036 697.49 19.7267 308.46 29.2513 505.52. 26.7026 702.65 23.3538 311. 90 26.2788 507.63 0.0000 706.68 20.6865 316.51 25.8434 511. 00 16.7276 711. 68 18.0182 319.41 0.0000 514.00 15.0738 720.70 0.0000 320.08 0.0000 514.00 15.0738 721. 93 0.0000 321.04 29.4685 520.40 15.6737 722.78 11. 5734 323.87 42.7485 520.69 0.0000 722.91 15.9146 325.23 24.4468 522.65 0.0000 723.31 18.8106 328.76 0.0000 527.90 0.0000 724 .19 20.2631 333.37 31.9287 528.26 19.0939 727. 33 19.0159 333.97 29.4826 529.59 13.4854 733.00 18.1439 334.37 36.8613 529.87 0.0000 735.93 15.4369 338.28 30.7855 531.02 0.0000 333.97 18.1702 338.32 30.7861 537.26 0.0000 739.50 0.0000 311. 90 30.8234 546.56 0.0000 747.24 9 .1135 340.48 30.8234 552.55 15.8793 748.06 15.4965 340.55 0.0000 563.25 1'5. 94 60 752.31 15.5178 344.28 24. 7104 569.33 22.8337 753.82 0.0000 345.93 32.9779 946.00 20.5518 756.73 15.8443 351.06 33.0703 569.70 20.5532 756.80 15.8443 351.93 33.0859 583.19 20.6602 884.68 10.9937 Page 3743of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 11.0002 14.6750 1620.50 7.8122 766.42 11.0024 1001.03 8.8157 1621. 92 3.3490 766.84 11. 0039 1002.74 13.7193 1678.03 0.0000 772. 60 0.0000 1004.73 18.6283 1690.97 3.6152 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.5752 778.90 7.3633 1028.54 0.0000 1063.66 1. 52 64 783.70 0.0000 1037.84 5.9319 1771. 35 1.5268 785.37 11. 0669 1038.76 0.0000 1791.20 0.0000 792.07 17.5585 631.29 10.8986 1808.65 2.7649 794.95 15.7243 1048.07 0.0000 1810 72 0.0000 795.86 12.9528 1049.04 15.8623 1836.06 1. 8515 810.06 12.0792 1050.41 14.2813 810.29 12.0800 1063.66 16.9149 344.28 13. 0101 1077.00 0.0000 810.76 13. 9407 1077.34 10.9812 815.77 0.0000 1085.87 5.0015 1048.07 0.0000 1093.63 10.0220 832.01 10.2877 1099.45 8.0288 834.85 15.9126 1112. 07 11. 0725 835. 71 14.9800 1112.84 12.0813 836.80 0.0000 1115. 54 11. 2834 846.75 0.0000 1120. 29 11. 0940 846:77 15. 9676 1120.55 11.0947" 856.80 0.0000 1221.41 6.4563 860.56 16.0314 1129. 67 11.1182 871.09 10.4045 1131. 51 0.0000 873.19 13. 2498 1147.95 0.0000 875.33 0.0000 1173.23 16.3350 879.38 12.3252 1177.95 11.2424 880.51 9.4836 1189.05 12.2952 883.24 19.7412 1204.77 0.0000 884.68 16. 7111 *1221. 41 10.3198 889.28 9.1269 1231. 02 13.7882 894.76 10.4740 1235.36 0.0000 898.04 10.4834 1238.28 14.5007 900. 72 11. 4448 1260.41 0.0000 903-.28 9.5441 1271. 87 14.6058 911.20 8.6086 1274.44 12.5259 912.08 8.6105 1274.54 13. 5705 923.98 0.0000 1291. 59 5.2383 926.50 11.5261 1298.22 0.0000 929 .11 11. 5342 1312 .11 0.0000 937.49 14.4502 1332.49 7. 3961 944.13 0.0000 1362.66 0.0000 946.00 18.3454 1365.19 4. 25.4 6 949.00 10.6294 1368. 63 0.0000 667. 71 0.0000 1384.29 8.5420 962. 31 9.3094 1408.01 2.1455 964.08 3.1046 1457.56 0.0000 966 .17 7.7656 1460.82 3.2514 911.20 0.0000 1489.16 1.0897 968.97 0.0000 1505.03 5.4645 983.53 0.0000 1584.12 -4.4353 984.45 0.0000 1596.21 0.0000 Page 3744 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:03.75 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l Background file DKAlOO: [CANBERRA.GAMMA,ARCHIVE.GAMMA]BKG GAM43.CNF;l51 Background date : Z-OCT-2016 11:02:23. Sample date 30-NOV-2015 10:40:00 Acquisition date : 3-0CT-2016 09:17:37. Sample ID G405235038 Sample quantity : 1.70192E+02 GRAM Detector name : GAM43 Detector geometry: CAN Elapsed live time: 0 01:00:00.QO Elapsed real time: 0 01:00:00.65 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID . : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 1 1 0 0 0 4 4 0 0 4 4 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3745 of 5809 Energy 42. 96 51. 69 54.53* 74.69 77.06 88.08 92.78* 111. 81 126.75 129 .11 185. 96* 209.35 238.57* 241.64 258.87 266.78 270.05 277.60 295.27* 299.95* 308.04 338.35 351. 67* 389.09 392.32 463.79 490.97 511. 12* 583.09* 609.40* 661.42 720. 47 728.72 769.43 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 32 60 29 82 145 101 51 14 17 37 66 30 356 77 27 22 36 24 111 26 7 75 182 10 14 71 26 2 109 112 40 16 61 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 134 85 66 .111 123 157 105 88 45 109 117 84 63 94 67 35 67 67 46 39 47 46 54 20 21 24 39 45 15 34* 16 16 32 29 2.91 1. 57 1. 03 1. 23 1.11 3.87 1. 51 0.44 1. 21 1.39 1. 23 1. 34 1.10 1. 71 0.94 1. 56 1. 95 0.98 1. 57 1. 21 0.55 1. 04 1. 38 0.94 1. 32 2.35 6.33 2.79 1. 70 1. 45 1.16 1.24 2.78 1. 31 85.69 103.16 1.08. 84 149.18 153.92 175.96 185.37 223.43 253.32 258.05 371. 78 418.57 477.03 483.18 517.65 533.46 540.00 555 .11 590.45 599.82 616.00 676.64 703.29 778.14 784.61 927.58 981.95 1022.26 1166. 23 1218.87 1322.93 1441. 05 1457.56 1538.98 81 99 107 144 144 171 182 219 252 252 366 415 469 469 512 531 531 549 586 596 609 673 697 774 780 918 973 1015 1161 1212 1317 1437 1446 1533 9 9.02E-03 66.7 8 l.68E-02 29.7 6 7.93E-03 49.3 15 2.28E-02 25.0 15 4.04E-02 15.0 11 2.81E-02 26.0 7 1. 42E-02 38. 0 7 3.77E-03120.3 10 4.75E-03 52.2 10 l.04E-02 51.4 9 1. 82E-02 33. 2 10 8.40E-03 59.2 20 9.89E-02 6.6 20 2.15E-02 29.0 10 7.41E-03 60.7 14 6.llE-03 42.2 14 9.98E-03 45.9 10 6.55E-03 70.0 10 3.08E-02 15.2 8 7.33E-03 46.1 8 2.0lE-03169.6 8 2.08E-02 19.5 12 5.06E-02 11.0 6 2.78E-03 78.4 7 3.83E-03 55.9 19 1.98E-02 20.2 19 7.28E-03 59.8 14 4.37E-04***** 10 3.03E-02 12.0 11 3. 12E-02 13. 9 13 1.lOE-02 26.3 10 4.54E-03 51.0 26 l.71E-02 28.4 14. 5. llE-03 65. 4 Fit 9.49E-01 4.25E+OO 4.42E-01 1. 95E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35. 0 796. 61 9 25 3.78 1593.35 1581 14 2.62E-03115.9 36 0 827.72 16 8 2.40 1655.58 1650 11 4.46E-03 42.6 37 1 854.43 15 16 2.04 1709.00 1703 20 4.28E-03 57.4 7.43E+OO 38 1 856.93 29 15 2.04 1714.00 1703 20 8.14E-03 30.9 39 0 911.28* 69 40 1. 30 1822.73 1815 16 1. 92E-02 24. 0 40 1 965 .12 20 11 2.34 1930.43 1926 24 5.52E-03 34.1 1. 79E+OO 41 1 968. 70 45 *13 2.34 1937.57 1926 24 1.26E-02 24.4 42 0 1032. 96 9 5 1. 42 2066.10 2062 8 2.58E-03 54.9 43 4 1065.40 16 7 2.20 2131.00 2125 14 4.39E-03 35.8 4.26E-01 44 4 1067.83 8 1 1. 80 2135.85 2125 14 2.14E-03 53.6 45 0 1120.89 18 25 1. 43 2241.98 2235 15 4.98E-03 63.0 46 0 1177.22 15 13 1. 65 2354.66 2348 14 4.27E-03 57.1 47 0 1244.93 6 9 0.47 2490.08 2484 8 l.69E-03 97.0 48 0 1460.55* 307 3 2.10 2921.34 2913 15 8.52E-02 5.9 49 0 1764.03* 17 0 0. 72 3528.30 3520 15 4.77E-03 26.5 Flag: "*" = Peak area was modified by background subtraction Page 3746 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:20:05 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 10:40:00 G405235038 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:17:37 170.19 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA43 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide. Page 3747 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87. 09. 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.65 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pC{/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.002E+OO l.238E+Ol 1.238E+Ol 11. 86 OK AS-73 53.44 10.30* 9.178E-01 1.918E+OO 2.738E+Ol 98.59 OK CD-109 88.03 3.70* 4.365E+oo* 3.050E+OO 4.845E+OO 64. 96 OK* SN-113 391.69 64.94* 3.112E+OO 3.501E-02 2.237E-01 111. 79 OK SN-126 64.28 9.60 l.983E+OO Line Not Found Absent 86.94 8.90 4.365E+OO 1. 268E+OO 1.268E+OO 64. 96 OK 87.57 37.00* 4.365E+OO 3.050E-01 3.050E-01 64. 96 OK CS-135 268.22 16.00* 4.342E+OO l.698E-01 l.698E-01 84.47 OK BA-137M 661.66 89.90* 1.974E+OO l.071E-01 l.092E-01 52.70 OK CS-137 661.66 85.10* l.974E+OO 1.131E-01 1.154E-01 52.70 OK TM-171 51.35 0.27 6.497E-01 2.199E+02 2.982E+02 59.33 OK 52.39 o*. 47* 6.497E-01 l.263E+02 l.713E+02 59.33 OK .66. 73 0.14 2.262E+OO Line Not Found Absent TL-208 277.37 6.60 4.202E+OO 4.542E-01 4.542E-01 139. 97 OK 583.19 85.00* 2.199E+OO 2.845E-01 2.845E-01 23.91 OK 860.56 12.50 1.582E+OO Line Not Found Absent PB-212 74.82 10.28 3 .134E+OO l.118E+00 l .118E+00 71. 23 OK 77 .11 17.10 3.377E+OO 1.546E+OO 1.546E+OO 30.01 OK 238.63 43.60* 4.739E+OO 9.370E-01 9.370E-01 13.13 OK 300.09 3.30 3.937E+00 1. 076E+OO 1. 076E+OO 92.17 OK BI-214 609.32 45.49* 2. ll 7E+OO 5. 666E-01 . 5.668E-01 27.84 OK 1120.29. 14.92 l.266E+OO 4.246E-01 4.247E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 OK PB-214 74.82 5.80 .3.147E+OO Line Not Found <<INT Reject 77 .11 9.70 3.377E+00 2.725E+OO 2. 726E+Oci 30.01 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.990E+OO 8.000E-01 8".003E-01 30.31 OK 351. 93 35.60* 3.428E+OO 7.757E-01 7.760E-01 22.09 OK RN-222 609.32 45.49* 2. ll 7E+OO 5.666E-01 5.668E-01 27.84 OK 1120. 29 14.92 1. 266E+OO 4.246E-01 4.247E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 OK RA-224 240.99 4.10* 4.694E+OO 7.685E-01 7.685E-01 174.16 OK RA-226 609.32 45.49* 2. ll 7E+OO 5.666E-01 5.668E-01 27.84 OK 1120.29 14.92 1. 2 66E+OO 4.246E-01 4.247E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 OK AC-228 105.21 LlO 5.396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 9.761E-01 9. 7 61E-01 39.05 OK 794.95 4.25 l.691E+00 Line Not Found Absent 835. 71 1. 61 l.621E+00 Line Not Found Absent 911.20 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 OK 968.97 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 OK RA-228 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 9.761E-01 9.761E-01 39.05 OK 794.95 4.25 1. 691E+OO Line Not Found Absent 835.71 1. 61 1.621E+OO Line Not Found Absent 911. 20 25.80* l.508E+OO 8.193E-01 8.193E-01 48.07 OK 968.97 15.80 l.432E+00 9.129E-01 9.129E-01 48.81 OK TH-228 74.82 10.28 3.134E+OO l.118E+00 1.118E+OO 71. 23 OK Page 3748 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 17.10 3.377E+OO 1.546E+OO 1.546E+00 30.01 OK 238.63 43.60* 4.739E+OO 9.370E-01 *9. 370E-01 13 .13 OK 300.09 3.30 3.937E+OO 1.076E+OO 1. 076E+OO 92.17 OK TH-230 609.32 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 OK 1120.29 14.92 1. 2 66E+OO 4.246E-01 4.246E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 OK PA-231 283.69 1. 70 4.127E+OO Line Not Found Absent '301.36 5.35* 3.937E+OO 6.635E-01 6.635E-01 92.17 OK TH-232 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11.27 3.546E+OO 9.761E-01 9.761E-01 39.05 OK 835.71 1. 61 1.621E+OO Line Not Found Absent 911. 20 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 OK 968. 97 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 OK U-234 609.32 45.49* 2.117E+OO 5.666E-01 5.666E-01 27.84 OK 1120.29 14.92 1. 2 66E+OO 4.246E-01 4.246E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 OK AM-243 43.53 5.90 1.014E-01 3.532E+Ol 3.532E+Ol 133.45 OK 74.66 67.20* 3.134E+OO 1. 711E-01 1. 711E-01 71.23 OK CF-249 252.80 2.50 4.533E+OO Line Not Found Absent 333.37 14.60 3.593E+OO Line Not Found Absent 388.16 66.00* 3.135E+OO 2.481E-02 2.485E-02 156.84 OK ANH-511 511. 00 100.00* 2.465E+OO 3.170E-03 3.170E-032134.97 OK Flag: "*" = Keyline Page 3749of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:06.82 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA. GAMMA.ARCHIVE. GAMMA] G4052*35038. CNF; 1 * *Acquisition date 3-0CT-2016 09:17:37 Sensitivity : 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.65 Half life ratio : *
Sample date 30-NOV-2015 10:40:00 Analyst initials: MXRl * *Sample ID G405235038 Sample Quantity 1.7019E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Ideniified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.238E+Ol 1.439E+OO AS-73 2.738E+Ol 2.645E+Ol CD-109 4.845E+OO 3.084E+OO SN-113 2.237E-01 2. 451E-01 SN-126 3.050E-01 1.942E-01 CS-135 l.698E-01 1.406E-01 BA-137M 1.092E-01 5.640E-02 CS-137 1.154E-01 5.958E-02 TM-171 1. 713E+02 9. 960E+Ol TL-208 2.845E-01 6.666E-02 PB-212 9.370E-01 l.206E-01 BI-214 5.668E-01 1. 54 7E-01 PB-214 7.760E-01 1.680E-01 RN-222 5.668E-01 1.547E-01 RA-224 7.685E-01 1.312E+OO RA-226 5.668E-01 1.547E-01 AC-228 8.193E-01 3.860E-01 RA-228 8.193E-01 3.860E-01 TH-228 9.370E-01 l.206E-01 TH-230 5.666E-01 1.546E-01 PA-231 6.635E-01 5.993E-01 TH-232 8.193E-01 3.860E-01 U-234 5.666E-01 1.546E-01 AM-243 1. 711E-01 1.194E-01 CF-249 2.485E-02 3. 819E--02 ANH-511 3.170E-03 6.633E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3750 of 5809 Key-Line Activity (p_Ci/GRAM -5.736E+OO -1.412E-02 O.OOOE+OO -l.236E-02 K.L. Cnt Uncert ( 1 . 96-sigma ) 1. 263E+Ol 4.877E-02 1. 960E+41 3. lllE-02 MDA (pCi/GRAM 6.582E-01 2.522E+Ol 2.130E+OO 4.203E-01 1.352E-01 2.407E-01 5.907E-02 6.240E-02 5.971E+Ol 6 .132E-02 .8. 681E-02 1. 317E-01 1.140E-01 1. 317E-01 9.308E-01 1.317E-01 2.602E-01 2.602E-01 8.681E-02 1.316E-01 7. 396E-01 2.602E-01 l.316E-01 1.051E-01 3.879E-02 4.723E-02 MDA ([JCi/GRAM 2. 251E+Ol 9.365E-02 O.OOOE+OO 5.866E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 2.703E-01 3. 968E-01 8.625E-01 FAIL ABUN V-48 O.OOOE+OO 2.035E+04 0.000E+OO SHORT HLIF CR-51* O.OOOE+OO 4.353E+02 O.OOOE+OO SHORT HLIF MN-54 2.686E-02 6.304E-02 l.314E-01 NOT IDENT. C0-56 -3. 201E-03 4.586E-01 9 .115E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0. OOOE+OO

SHORT HLIF C0-57 5.143E-03 4.857E-02 9.125E-02 NOT IDENT. C0-58 l.387E-01 6.086E-01 l.247E+OO NOT IDENT. FE-59 2. 372E+OO 8.065E+OO l.626E+Ol NOT IDENT. C0-60 l.128E-02 4.240E-02 8.942E-02 NOT IDENT. ZN-65 O.OOOE+OO l.607E-01 2.792E-01 NOT IDENT. GE-68 -2.413E-01 2.007E+OO 3.901E+OO NOT IDENT. AS-74 O.OOOE+OO 6.439E+03 0.000E+OO SHORT HLIF SE-75 3.837E-02 2.005E-01 3.632E-01 NOT IDENT. BR-77 O.OOOE+OO 2.312E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1.044E+03 O.OOOE+OO SHORT HLIF RB-83 -2. 502E.-01 7.342E-01 1.419E+OO NOT IDENT. KR-85 -2.349E+OO 7. 961E+OO l.253E+Ol NOT IDENT. SR-85 -2. 721E-01 9.159E-01 l.441E+OO NOT IDENT. RB-86 O.OOOE+OO 3.308E+04 O.OOOE+OO SHORT HLIF Y-88 -8.303E-02 l.711E-01 3.177E-01 NOT IDENT. Y-91 -1.197E+02 5.995E+02 l.165E+03 NOT IDENT. NB-94 -1.205E-02 2.924E-02 5.483E-02 NOT IDENT. NB-95 -9.290E-02 9.182E-01 1.570E+OO NOT IDENT. NB-95M -3.887E-01 2.454E+OO 4.255E+OO NOT IDENT. ZR-95 8.792E-01 l.478E+OO 3.183E+OO NOT IDENT. *NB-97 O.OOOE+OO 9.864E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.403E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO .l.525E+41 O.OOOE+OO SHORT HLIF RH-101 2.937E-02 3.003E-02 6.382E-02 FAIL ABUN RH-102 1.634E-02 5.397E-02 l .130E-01 NOT IDENT. RU-103 -3.664E+OO 7.344E+OO 1.116E+Ol FAIL ABUN RH-106 .-4. 07 4E-02 4.694E-01 9.335E-01 NOT IDENT. RU-106 -4.074E-02 4.694E-01 9.335E-01 NOT IDENT. AG-108M -1.106E-02 2.638E-02 4.762E-02 NOT IDENT. AG-llOM -1.242E-01 l.035E-01 1.604E-01 NOT IDENT. CD-115 O.OOOE+OO 3.462E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.160E+05 O.OOOE+OO SHORT HLIF TE-123M 2.577E-02 l.123E-01 2.318E-01 NOT IDENT. SB-124 1.463E+OO 1.779E+OO 4.871E+OO NOT IDENT. SB-125 -6.762E-02 9.768E-02 l.697E-01 FAIL ABUN TE-125M 3.479E+Ol 3.382E+02 5.900E+02 NOT IDENT. I-126 O.OOOE+OO l.433E+06 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 2.521E+06 O.OOOE+OO , SHORT HLIF SB-127 O.OOOE+OO 9.023E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.615E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.838E+27 O.OOOE+OO SHORT HLIF BA-133 5.826E-03 3.982E-02 7.036E-02 FAIL ABUN I-133 O.OOOE+OO 9.779E+40 O.OOOE+OO SHORT HLIF CS-134 4.068E-02 9.241E-02 l .113E-01 FAIL ABUN I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.898E+05 O.OOOE+OO SHORT HLIF CE-139 -1.039E-01 9.441E-02 1.748E-01 NOT IDENT. BA-140 0.000E+OO 2.035E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 6.136E+05 O.OOOE+OO SHORT HLIF CE-141 -l.347E+Ol
2. 513E+Ol 4.921E+Ol NOT IDENT. CE-143 0.000E+OO l.415E+41 O.OOOE+OO SHORT HLIF CE-144 . -2.379E-01 3.257E-01 6.022E-01 NOT IDENT. PM-144 l.692E-02 5.685E-02 1.160E-01 NOT IDENT. PR-144 1.550E+OO 4.970E+OO 1.016E+Ol NOT IDENT. PM-146 -l.941E-02 4.176E-02 7.563E-02. NOT IDENT. ND-147 O.OOOE+OO 4.899E+07 O.OOOE+OO SHORT HLIF PM-147 3.652E+Ol 8.214E+02 l.537E+03 NOT IDENT. PM-149 O.OOOE+OO l.410E+41 O.OOOE+OO SHORT HLIF EU-150 -l.836E-02 2.754E-02 4.297E-02 FAIL ABUN EU-152 -3.342E-02 8.725E-02 l.613E-01 FAIL ABUN GD-153 -l.124E-01 l.983E-01 3.575E-01 NOT IDENT. EU-154 -4.213E-02 l.217E-01 2.310E-01 NOT IDENT. EU-155 2.382E-02 1.030E-01 l.989E--:01 NOT IDENT. TB-160 1.138E+OO 1. 776E+OO 3.923E+OO FAIL ABUN H0-166M -3.298E-02 5.440E-02 9.885E-02 NOT IDENT. HF-172 2.024E-01 2 .-069E-01 4.546E-01 FAIL ABUN LU-172 -3.067E-02 7.432E-02 l.334E-01 FAIL ABUN LU-176 l.058E-02 3.517E-02 4.423E-02 FAIL ABUN HF-181 2.507E-01 4.386E+OO 8.466E+OO NOT IDENT. TA-182 3.567E-01 1.128E+OO . 2.303E+OO FAIL ABUN Page 3751of5809 RE-183 2.083E+OO 5.140E+OO 9.809E+OO NOT IDENT. RE-184 -1.787E+Ol 3.726E+Ol 6.436E+Ol NOT IDENT. W-188 2.622E+Ol l.143E+02 2.062E+02 NOT IDENT. IR-192 3.321E-01 4.274E-01 9.004E-01 FAIL ABUN HG-203 -2.113E-01 2.204E+OO 3.861E+OO NOT IDENT. BI-207 -8.451E-03 5.413E-02 8.826E-02 FAIL ABUN PB-210 -3.340E+OO 9.826E+OO 1. 762E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.626E-01 7.270E-01 FAIL*ABUN PB-211 -2.421E-01 6.675E-01 1. 217E+OO NOT IDENT. BI-212 O.OOOE+OO 1.336E+OO 1.339E+OO FAIL ABUN RN-219 1.009E-01 3.491E-01 6.917E-01 FAIL ABUN RA-223 l.027E-01 5.134E-01 1.019E+OO FAIL ABUN AC-227 -2.400E-02 2.142E-01 3. 730E-01
FAIL ABUN TH-227 -2.400E-02 2.142E-01 3.730E-01 FAIL ABUN TH-229 *1. 7 58E-03 3.749E-01 7.516E-01 FAIL ABUN TH-231 l.027E-01 5.134E-01 1.019E+OO FAIL ABUN PA-233 3.351E-02 5.235E-02 1.084E-01 FAIL ABUN PA-234 -9. 969E-02 3. OllE-01 5.528E-01 FAIL ABUN PA-234M -3.021E+OO 3.889E+OO 6.504E+OO NOT IDENT. TH-234 -l.459E-01 1.591E+OO 3 .114E+00 FAIL ABUN U-235 2.090E-01 l.573E-01 3.451E-01 FAIL ABUN NP-237 3.351E-02 5.235E-02 1.084E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -1. 459E-01 1. 591E+OO 3 .114E+OO FAIL ABUN NP-239 1. 137E-01 2.239E-01 4.401E-01 FAIL ABUN PU-239 5.759E+02 5.796E+02 6.423E+02 FAIL ABUN AM-241 -l.384E-01 1.909E-01 3.534E-01 NOT IDENT. CM-243 -4.867E-02 9.784E-02 1. 7 68E-01 FAIL ABUN' BK-247 4.107E-03 6.672E-02 l.188E-01 NOT IDENT. CM-247 1. 285E-02 3.248E-02 6.498E-02 FAIL ABUN CF-251 -7.742E-02 9.753E-02 1.842E-01 *NOT IDENT. Page 3752 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:04.51 Nuclide Line Activiti Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 300 10.66* 1.002E+OO 1.238E+Ol 1.238E+Ol 11. 86 AS-73 53.44 41 10.30* 9.178E-01 1. 918E+O.O 2.738E+Ol 98.59 CD-109 88.03 139 3.70* 4.365E+OO 3.787E+OO 6.016E+OO 51. 98 SN-113 391.69 16 64.94* 3 .112E+OO 3. 501E-02 2.237E-01 111.79 SN-126 64.28 ------9.60 1.983E+OO ------Line Not Found ------86.94 139 8.90 4.365E+OO 1.575E+OO 1.575E+OO 51. 98 87.57 139 37.00* 4.365E+OO 3.787E-01 3.787E-01 51. 98 CS-135 268.22 27 16.00* 4.342E+OO 1.698E-01 1.698E-01 84.47 BA-137M 661.66 43 89.90* 1.974E+OO 1. 071E-01 l.092E-01 52.70 CS-137 661. 66 43 85.10* 1. 974E+OO 1.131E-01 l.154E-01 52.70 TM-171 51. 35 87 0.27 6.497E-01 2.199E+02 2.982E+02 59.33 52.39 87 0.47* 6.497E-01 1. 263E+02 1. 713E+02 59.33 66.73 ------0.14 2.262E+OO ------Line Not Found ------TL-208 277.37 29 6.60 4.202E+OO 4.542E-01 4.542E-01 139.97 583.19 121 85.00* 2.199E+OO 2.845E-01 2.845E-01 23.91 860.56 ------12.50 1.582E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 2.941E+OO ------Line Not Found ------351.06 215 12.92* 3.428E+OO 2 .137E+OO 2.137E+OO 22.09 PB-212 74.82 115 10.28 3 .134E+OO 1.570E+OO 1.570E+OO 49.99 77 .11 202 17.10 3.377E+OO 1. 546E+OO 1.546E+OO 30.01 238.63 439 43.60* 4.739E+00 9.370E-01 9.370E-01 13 .13 300.09 32 3.30 3.937E+OO 1.076E+OO 1. 076E+OO 92.17 BI-214 609.32 124 45.49* 2. ll 7E+OO 5.666E-01 5.668E-01 27.84 1120.29 18 14.92 1. 266E+OO 4.246E-01 4.247E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 PB-214 74.82 115 5.80 3.134E+OO 2.782E+OO 2.783E+00 49.99 77 .11 202 9.70 3.377E+OO 2. 725E+OO 2.726E+OO 30.01 *87.09 139 3.41 4.365E+OO 4. llOE+OO 4. lllE+OO 51. 98 242.00 95 7.25 4.694E+00 1.235E+OO 1.235E+OO 58.08 295.22 133 18.42 3.990E+OO 8.000E-01 8.003E-01 30.31 351. 93 215 35.60* 3.428E+OO *7. 7 57E-01 7.760E-01 22.09 RN-222 609.32 124 45.49* 2. ll 7E+OO 5.666E-01 5.668E-01 27.84 1120.29 18 14.92 1.266E+OO 4.246E-01 4.247E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 RA-224 240.99 95 4 .10* 4.694E+OO 2.183E+OO 2.183E+OO 58.08 RA-226 609.32 124 45.49* 2. ll 7E+OO 5.666E-01 5.668E-01 27.84 1120.29 18 14.92 1. 2 66E+OO 4.246E-01 4.247E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 AC-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 88 11. 27 3.546E+OO 9. 761E-01 9.761E-01 39.05 794.95 ------4.25 1. 691E+OO ------Line Not Found ------835. 71 ------1. 61 1. 621E+OO ------Line Not Found ------911. 20 72 25.80* l.508E+OO 8.193E-01 8.193E-01 48.07 968. 97 47 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 RA-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 88 11. 27 3.546E+OO 9.761E-01 9.761E-Ol 39.05 794.95 ------4.25 1.691E+OO ------Line Not Found ------Page 3753 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 835.71 ------1. 61 1.621E+OO ------Line Not Found ------911.20 72 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 968. 97 47 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 TH-228 74.82 115 10.28 3.134E+OO 1.570E+OO 1.570E+OO 49.99 77 .11 202 17 .10 3.377E+OO 1.546E+OO 1.546E+OO 30.01 238.63 439 43.60* 4.739E+OO 9.370E-01 9;370E-01 13.13 300.09 32 3.30 3.937E+OO 1. 076E+OO 1.076E+OO 92 .17 TH-230 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 1120.29 18 14.92 1. 2 66E+OO 4.246E-01 4.246E-01 125.97 1764.49 16 15.30 8.365E-01 5. 620E.-01 5.620E-01 52.95 PA-231 283.69 ------1. 70 4.127E+OO ------Line Not Found ------301.36 32 5.35* 3.937E+OO 6.635E-01 6.635E-01 92.17 TH-232 105.21 ------1.10 5.396E+OO ------Line Not Found ------338.32 88 11.27 3.546E+OO 9.761E-01 9.761E-01 39.05 835.71 ------1. 61 1. 621E+OO ------Line Not Found ------911.20 72 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 968. 97 47 15.80 1.432E+OO 9.129E-01 9.129E-01' 48.81 U-234 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 1120.29 18 14.92 l.266E+OO 4.246E-01 4.246E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 AM-243 43.53 48 5.90 1.014E-01 3.532E+Ol 3.532E+Ol 133.45 74.66 115 67.20* 3.134E+OO 2.401E-01 2.401E-01 49.99 CF-249 252.80 ------2.50 4.533E+00 ------Line Not Found ------333.37 ------14.60 3.593E+OO ------Line Not Found ------388.16 12 66.00* 3.135E+OO 2.481E-02 2.485E-02 156.84 ANH-511 511. 00 2 100.00* 2.465E+OO 3.170E-03 3.170E-03 2134.97 Flag: "*" Key line Page 3754of5809 Summary of Nuclide Activity Sample ID : G405235038 Acquisition date Page : 3 3-0CT-2016 09:17:37 Total number of lines in spectrum 49 Number of unidentified lines 9 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-113 SN-126 CS-135 BA-137M CS-137 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 CF-249 ANH-511 Hlife l.25E+09Y 80.30D 461.40D 115. 09D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y l.92Y 1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600. OOY 1600. OOY l.41E+10Y 1600.00Y 1. 41E+10Y l.41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y 351.00Y l.00E+09Y Decay 1. 00 14.3 1. 59 6.39 1. 00 1. 00 1. 02 1. 02 1. 36 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Total Activity Uncorrected pCi/GRAM 1.238E+Ol 1.918E+OO 3.787E+OO 3. 501E-02 3.787E-01 l.698E-01 1.071E-01 1.131E-01 l.263E+02 2.845E-01 2.137E+OO 9.370E-01 5.666E-01 7.757E-01 5.666E-01 2.183E+'OO 5.666E-01 8.193E-01 8.193E-01 9.370E-01 5.666E-01 6.635E-01 8.193E-01 5.666E-01 2.401E-01 2. 481E-02 3.170E-03 1:587E+o2 1.587E+02 Decay Corr 'pCi/GRAM l.238E+Ol 2.738E+Ol 6.016E+OO 2.237E-01 3.787E-01 1.698E-01 l.092E-01 l.154E-01 1. 713E+02 2.845E-01 2.137E+OO 9.370E-01 5.668E-01 7.760E-01 5.668E-01 2.183E+OO 5.668E-01 8.193E-01 8.193E-01 9.370E-01 5.666E-01 6.635E-01 8.193E-01 5.666E-01 2.401E-01 2.485E-02 3.170E-03 2.315E+02 2.315E+02 81.63% Decay Corr 2-Sigma Error 0.147E+Ol 2.699E+Ol 3.127E+OO 2.501E-01 1. 969E-01 l.435E-01 0.575E-01 0.608E-01 l.016E+02 0.680E-01 0.472E+OO 1.230E-01 1.578E-01 1. 714E-01 1.578E-01 1. 2 68E+OO 1.578E-01 3.939E-01 3.939E-01 1.230E-01 1. 578,E-01 6.116E-01 3.939E-01 l.578E-01 1.200E-01 3.897E-02 67.68E-03 "M" Manually 2-Sigma %Error 11. 86 98.59 51. 98 111.79 51. 98 84.47 52.70 52.70 59.33 23.91 22.09 13.13 27.84 22.09 27.84 58.08 27.84 48.07 48.07 13.13 27.84 92.17 48.07 27.84 49.99 156.84 2134.97 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide abn. limit Page 3755 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235038 Acquisition date : 3-0CT-2016 09:17:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.78 70 144 1. 51 185.37 182 7 1. 42E-02 75.9 4. 71E+00 T 0 111-.81 18 118 0.44 223.43 219 7 3.77E-03 **** 5.64E+OO T 4 126.75 23 59 1. 21 253.32 252 10 4.75E-03 **** 5. 96E+OO T 4 129 .11 49 143 1. 39 258.05 252 10 1. 04E-02 **** 5.98E+OO T 0 185. 96 83 148 1. 23 371. 78 366 9 1.82E-02 66.4 5.57E+OO T 0 209.35 38 105 1. 34 418.57 415 10 8.40E-03 **** 5.19E+OO 0 258.87 3*3 82 0.94 517.65 512 10 7.41E-03 **** 4.45E+OO 3 270.05 44 81 1. 95 540.00 531 14 9.98E-03 91. 8 4.30E+OO T 0 308.04 9 56 0.55 616.00 609 8 2.0lE-03 **** 3.85E+OO T 0 463.79 81 27 2.35 927.58 918 19 1. 98E-02 40.4 2.68E+OO. T 0 490.97 30 44 6.33 981.95 973 19 7.28E-03 **** 2.55E+00 T 0 720.47" 18 17 1. 24 1441.05 1437 10 4.54E-03 **** 1.84E+OO T 0 728. 72 66 34 2.78 1457.56 1446 26 1.71E-02 56.8 l.82E+00 T 0 769.43 20 31 1. 31 1538.98 1533 14 5. llE-03 **** 1.74E+OO 0 796.61 10 26 3.78 1593.35 1581 14 2.62E-03 **** 1. 69E+OO T 0 827.72 17 8 2.40 1655.58 1650 11 4.46E-03 85.2 1.63E+OO 1 854.43 16 17 2.04 1709.00 1703 20 4.28E-03 **** 1. 59E+OO 1 856.93. 31 16' 2.04 1714.00 1703 20 8.14E-03 61. 8 1. 59E+OO T 1 965 .12 21 11 2.34 1930.43 1926 24 5.52E-03 68.2 1. 44E+OO T b 1032. 96 10 5 1. 42 2066.10 2062 8 2.58E-03 **** l.36E+00 4 1065.40 16 7 2.20 2131*. 00 2125 14 4.39E-03 71. 7 l.32E+OO 4 1067.83 8 1 1. 80 2135. 85. 2125 14 2.14E-03 **** l.32E+00 0 1177.22 15 13 1. 65 2354.66 2348 14 4.27E-03 **** 1.21E+OO T 0 1244.93 6 9 0.47 2490.08 2484 8 1.69E-03 **** 1.16E+OO Flags: "T" = Tentatively associated Page 3756 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:18.98 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l * *Acquisition date 3-0CT-2016 09:17:37 Sensitivity : 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: . 0 01:00:00.65 Half life ratio : ***** *
Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
Sample ID G405235038 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7019E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-113 SN-126 CS-135 BA-137M CS-137 TM-171 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 'RA-22 6 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 CF-249 ANH-511 Le (pCi/GRAM 2. 725E-01 1.147E+Ol 1.000E+OO l.903E-01 6.348E-02 l. lllE-01 2.598E-02 2.744E-02 2. 715E+Ol 2.734E-02 4.032E-02 5.938E-02 5.180E-02 5.938E-02 4.323E-01 5.938E-02 l.144E-01 1.144E-01 4.032E-02 5.936E-02 3.396E-01 l.144E-01 5.936E-02 4.942E-02 l.635E-02 2.108E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3757of5809 Le (pCi/GRAM 9.992E+OO 4. 012E-02
O.OOOE+OO 2 .196E-02 3.803E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3758 of 5809 O.OOOE+OO O.OOOE+OO 5. 818E-02 3.949E-01 O.OOOE+OO 4.280E-02 5.476E-01 7.116E+OO 3.849E-02 1.169E-01 l.632E+OO O.OOOE+OO 1.669E-01 O.OOOE+OO 0.000E+OO 6.414E-01 5.644E+OO 6.491E-01 0.000E+OO 1.031E-01 5. 072E+02 2.411E-02 6.859E-01 1.977E+OO 1. 411E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.000E-02 5.0lBE-02 4.956E+OO 4.134E-01 4.134E-01 2.137E-02 6.734E-02 O.OOOE+OO O.OOOE+OO 1. OBlE-01 1.933E+OO 7.582E-02 2.771E+02 O.OOOE+OO *o.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.201E-02 O.OOOE+OO 5.002E-02 O.OOOE+OO O.OOOE+OO 8.090E-02 O;OOOE+OO O.OOOE+OO 2.302E+Ol O.OOOE+OO 2.805E-01 5.210E-02 4.562E+OO 3.390E-02 0.000E+OO 7.202E+02 O.OOOE+OO l. 962E-02 7.357E-02 l.678E-01 9. 911E-02 9.297E-02 1. 710E+OO 4.327E-02 2.141E-01 5.647E-02 2.036E-02 3. 772E+OO 1.028E+OO 4.584E+OO SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. .SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192

HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM=--241 CM-243 BK-247 CM-247 CF-251 Page 3759of5809 2.777E+Ol 9.476E+Ol 4.135E-01 1.749E+OO 3.784E-02 8.202E+OO 3.494E-01 5.535E-01 6.189E-01 3.146E-01 4.663E-01 1. 716E-01 1. 716E-01 3.491E-01 4.663E-01 4.989E-02 2.415E-01 2.729E+OO 1.462E+OO 1.628E-01 4.989E-02 O.OOOE+OO 1.462E+OO 2.059E-01 3.040E+02 l.639E-01 8.239E-02 5.455E-02 2.962E-02 8.557E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:24.07 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l *
Acquisition date 3-0CT-2016 09:17:37 Sensitivity : 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.65 Half life ratio : ***** *
Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
Sample ID G405235038 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity l.7019E+02 GRAM *
Quantity Err(%) 1.1751E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 07: 25: 20 Eff'. Geometry * : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides* Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.238E+Ol 1. 578E+OO l.578E+OO AS-73 2.738E+Ol 2.705E+Ol 2.705E+Ol CD-109 4.845E+OO 3 .113E+OO 3 .113E+OO SN-113 2.237E-01 2.453E-01 2.453E-01 SN-126 3.050E-01 1.953E-01 1.953E-01 CS-135 l.698E-01 1. 411E-01 1. 411E-01 BA-137M 1.092E-01 5.659E-02 5.659E-02 CS-137 l.154E-01 5.978E-02 5.978E-02 TM-171 l.713E+02 l.008E+02 l.008E+02 TL-208 2.845E-01 6.776E-02 6.776E-02 PB-212 9.370E-01 l.306E-01 1. 306E-01 BI-214 5.668E-01 1.566E-01 1.566E-01 PB-214 7.760E-01 l.711E-01 l.711E-01 RN-222 5.668E-01 l.566E-01 1.566E-01 RA-224 7.685E-01 l.316E+OO l.316E+OO RA-226 5.668E-01 1.566E-01 l.566E-01 AC-228 8.193E-01 3.883E-01 3.883E-01 RA-228 8.193E-01 3.883E-01 3.883E-01 TH-228 9.370E-01 1.306E-01 1.306E-01 TH-230 5.666E-01 l.565E-01 l.565E-01 PA-231 6.635E-01 6.158E-01 6.158E-01 TH-232 .8 .193E-01 3.883E-01 3.883E-01 U-234 5.666E-01 l.565E-01 AM-243 1.711E-01 1. 202E-01 l.202E-01 CF-249 2.485E-02 3 .*825E-02 3.825E-02 ANH-511 3.170E-03 6.633E-02 6.633E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM *) ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -5.736E+OO 1.264E+Ol 1.290E+Ol NOT IDENT. NA-22 -1.412E-02 4.878E-02 4.919E-02 NOT IDENT. NA-24 1.000E+41 2.190E+41 O.OOOE+OO SHORT HLIF AL-26 -l.236E-02 3 .112E-02 3.162E-02 NOT IDENT. Page 3760of5809 SC-46 2.703E-Ol 3.969E-01 4.152E-01 FAIL ABUN V-48 -1.199E+04 2.036E+04 2.106E+04 SHORT HLIF CR-51 -6.908E+Ol 4.353E+02 4.364E+02 SHORT HLIF MN-54 2.686E-02 6.305E-02 6.420E-02 NOT IDENT. C0-56 -3.201E-03 4.586E-01 4.586E-01 NOT IDENT. MN-56 -l.OOOE+41 3.143E+43 O.OOOE+OO SHORT HLIF C0-57 5.143E-03 4.857E-02 4.863E-02 NOT IDENT. C0-58 1.387E-01 6.086E-01 6 .119E-01 NOT IDENT. FE-59 2. 372E+OO 8.066E+OO 8.137E+OO NOT IDENT. C0-60 l.128E-02 4.240E-02 4.270E-02 NOT IDENT. ZN-65 O.OOOE+OO l.607E-01 0.000E+OO NOT IDENT. GE-68 -2.413E-01 2.007E+OO 2.0lOE+OO NOT IDENT. AS-74 l.938E+03 6.441E+03 6.500E+03 SHORT HLIF SE-75 3.837E-02 2.005E-01 2.013E-01 NOT IDENT. BR-77 1. 797E+39 l.597E+40 O.OOOE+OO SHORT HLIF SR-82 -7. 878E+02 l.044E+03 l.103E+03 SHORT HL*IF RB'-83 -2.502E-Ol 7.350E-01 7.436E-01 NOT IDENT. KR-85 -2.349E+OO 7. 962E+OO 8.032E+OO NOT IDENT. SR-85 -2. 721E-01 9.160E-01 9.241E-01 NOT IDENT. RB-86 1.139E+03 3.308E+04 3.308E+04 SHORT HLIF Y-88 -8.303E-02 1. 712E-01 1. 753E-01 NOT IDENT. Y-91 -l.197E+02 5.995E+02 6.020E+02 NOT IDENT. NB-94 -l.205E-02 2.924E-02 2.974E-02 NOT IDENT. NB-95 -9.290E-02 9.182E-01 9.192E-01 NOT IDENT. NB-95M -3.887E-01 2.455E+OO 2.461E+OO NOT IDENT. ZR-95 8.792E-01 l.478E+OO 1.530E+OO NOT IDENT. NB-97 l.OOOE+41 9.874E+40 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 6.661E+41 O.OOOE+OO SHORT HLIF M0-99 -1.597E+32 1.403E+33 0. OOOE+0.0 SHORT HLIF TC-99M -1. 000E+41 1.528E+41 O.OOOE+OO SHORT HLIF RH-101 2.937E-02 3.049E-02 3.324E-02 FAIL ABUN RH-102 1.634E-02 5.399E-02 5.449E-02 NOT IDENT. RU-103 -3.664E+OO 7.346E+OO 7.529E+00 FAIL ABUN RH-106 -4.074E-02 4.694E-01 4.698E-01 NOT IDENT. RU-106 -4.074E-02 4.694E-01 4.698E-01 NOT IDENT. AG-108M -1.106E-02 2.638E-02 2.685E-02 NOT IDENT. AG-llOM -1.242E-01 l.037E-01 1.17 9E-01 NOT IDENT. CD-115 -4.955E+40 3.581E+40 O.OOOE+OO *sHORT HLIF SN-ll 7M * -2.620E+04 l.160E+05 l.166E+05 SHORT HLIF TE-123M 2.577E-02 l.123E-01 l.129E-01 NOT IDENT. SB-124 1.463E+OO 1. 781E+OO 1. 899E+OO NOT IDENT. SB-125 -6.762E-02 9.772E-02 l.024E-01 FAIL ABUN TE-125M 3.479E+Ol 3.382E+02 3.386E+02 NOT IDENT. I-126 -4.637E+05 l.435E+06 l.450E+06 SHORT HLIF SB-126 2.522E+06 2.567E+06 2.807E+06 SHORT HLIF SB-127 -2.615E+22 9.749E+22 O.OOOE+OO SHORT HLIF I-131 7.203E+09 9.621E+09 1.015E+10 SHORT HLIF I-132 1.000E+41 2.054E+42 O.OOOE+OO SHORT HLIF TE-132 -5.779E+26 l.853E+27 O.OOOE+OO SHORT HLIF BA-133 5.826E-03 3.982E-02 3.991E-02 FAIL ABUN I-133 1.000E+41 2.100E+41 O.OCiOE+OO SHORT HLIF CS-134 4.068E-02 9.243E-02 9.423E-02 FAIL ABUN I-135 l.000E+41 1.305E+42 0.000E+OO SHORT HLIF CS-136 -1.930E+05 4.903E+05 4.979E+05 SHORT HLIF CE-139 -1.039E-01 9.669E-02 1.074E-01 NOT IDENT. BA-140 -3.555E+05 2.035E+06
2.041E+06 SHORT HLIF LA-140 -6.638E+05 6.144E+05 6.834E+05 SHORT HLIF CE-141 -1.347E+Ol 2. 513E+Ol 2.586E+Ol NOT IDENT. CE-143 1.000E+41 l.419E+41 O.OOOE+OO SHORT HLIF CE-144 -2.379E-01 3.260E-01 3.432E-01 NOT IDENT. PM-144 1. 692E-02 5.686E-02 5.737E-02 NOT IDENT. PR-144 1.550E+OO 4.970E+OO 5.019E+OO NOT IDENT. PM-146 -1.941E-02 4.179E-02 4.269E-02 NOT IDENT. ND-147 -2.956E+07 4.901E+07 5.079E+07 SHORT HLIF PM-147 3.652E+Ol 8.214E+02 8.216E+02 NOT IDENT. PM-149 l.000E+41 l.428E+41 O.OOOE+OO SHORT HLIF EU-150 -1. 836E-02 2.755E-02 2.877E-02 FAIL ABUN EU-152 -'-3.342E-02 8. 727E-02 8.856E-02 FAIL ABUN GD-153 -l.124E-01 l.984E-01 2.047E-01 NOT IDENT. EU-154 -4. 213E-02 l.217E-01 l.232E-01 NOT IDENT. EU-155 2.382E-02 l.030E-01 l.035E-01 NOT IDENT. TB-160 1.138E+OO 1. 777E+O.O l.850E+OO FAIL ABUN H0-166M -3.298E-02 5.443E-02 5.642E-02 NOT IDENT. HF-172 2.024E-01 2.095E-01 2.285E-01 FAIL ABUN LU-172 -3.067E-02 7.438E-:-02 7.566E-02 FAIL ABUN LU-176 l.058E-02 3.518E-02 3.550E-02 FAIL ABUN HF-181 2.507E-01 4.386E+OO 4.388E+OO NOT IDENT. TA-182 3.567E-01 l.128E+OO l.140E+OO FAIL ABUN Page 3761 of 5809 RE-183 2.083E+OO 5 .151E+OO 5.236E+OO NOT IDENT. RE-184 -1.787E+Ol 3.752E+Ol 3.837E+Ol NOT IDENT. W-188 2.622E+Ol l.143E+02 l.150E+02 NOT IDENT. IR-192 3.321E-01 4.276E-01 4.531E-01 FAIL ABUN HG-203 -2.113E-01 2.204E+OO 2.206E+OO NOT IDENT. BI-207 -8. 451E-03 5.413E-02 5.426E-02 FAIL ABUN PB-210 -3.340E+OO 9.832E+OO 9.947E+OO NOT IDENT. BI-211 2.137E+OO 4. 725E-01 1.073E+OO FAIL ABUN PB-211 -2.421E-01 6.676E-01 6.764E-01 NOT IDENT. BI-212 2.400E+OO l.342E+OO 1. 723E+OO FAIL ABUN RN-219 1.009E-01 3.493E-01 3.522E-01 FAIL ABUN RA-223 l.027E-01 5.134E-01 5.155E-01 FAIL ABUN AC-227 -2.400E-02 2.142E-01 2.145E-01 FAIL ABUN TH-227 -2.400E-02 2.142E-01 2.145E-01 FAIL ABUN TH-229 1. 758E-03 3.749E-01 3 .*749E-01 FAIL ABUN TH-231 l.027E-01 5.134E-01 5.155E-01 FAIL ABUN PA-233 3.351E-02 5.237E-02 5. 451E-02 FAIL ABUN PA-234 -9. 969E-02 3.220E-01 3. 251E-01 FAIL ABUN PA-234M -3.021E+OO 3.892E+OO 4.123E+OO NOT IDENT. TH-234 -1.459E-01 1.592E+OO 1. 593E+OO FAIL ABUN U-235 2.090E-01 1.577E-01 1.837E-01 FAIL ABUN NP-237 3. 351E-02 5.237E-02 5.451E-02 FAIL ABUN NP-238. -l.000E+41 2.624E+41 O.OOOE+OO SHORT HLIF U-238 -1.459E-01 1.592E+OO 1.593E+OO FAIL ABUN NP-239 1.137E-01 2.241E-01 2.299E-01 FAIL ABUN PU-239 5.759E+02 5.802E+02 6.356E+02 FAIL ABUN AM-241 -1.384E-01 1.912E-01 2. OllE-01 NOT IbENT. CM-243 -4.867E-02 9.795E-02 l.004E-01 FAIL ABUN BK-247 4.107E-03 6. 672E-02 6.675E-02 NOT IDENT. CM-247 1.285E-02* 3.255E-02 3.306E-02 FAIL ABUN CF-251 -7.742E-02 9.792E-02 1. 040E-01 NOT IDENT. Page 3762 of 5809
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 68.8594 87.09 79.7662 136.47 80.3799 45.60 57.9438 87.57 79.8461 140.51 0.0000 46.54 69.1879 88.03 79.9228 143.76 56.7160 49.72 0.0000 88.34 79.9741 144.24 67.7686 51. 35 50.5560 88.47 79.9953 145.44 83.1620 51. 87 50.6340 89. 96 67 .12.45 152.43 77.1451 52.39 33.8077 1093.63 67.2178 153.25 0.0000 52.97 33.8651 91.,11 0.0000 323.87 63.5892 53.44 33. 9114 92.59 80.6692 156.02 0.0000 54.07 33.9731 93.35 74.5771 158.56 0.0000 57.36 0.0000 94.56 74.7563 159.00 59.6878 57.53 55.7471 94.65 74.7695 162.33 65.1733 . 57. 98 58.6783 94.67 74.7725 162.66 0.0000 59.27 74.3243 94.87 79.4774 163.33 42. 6372 59.32 75.4116 97.43 90.4476 165.86 75.0864 59.54 71.1447 98.43 63.5532 176.31 63.7236 60.96 72.4976 98.44 63.5544 176.60 0.0000 61.17 72. 5380 99.53 79.0191 177.52 74.4587 62.93 85.9262 100 .11 73.2031 181.07 0.0000 63.29 72. 9421 102.03 60.4341 181.52 74.8339 63.58 59.9228 103.18 74.8139 184.41 71. 5259 64.28 66.5797 103.37 74.8409 143.76 71. 6414 66.73 87.8613 105.21 63.1757 193.51 56.9508 67.24 81. 37 50 105.31 63 .1870' 197.03 68.9886 125.81 79.2625 106.12 78.8025 198.01 67.2507 67.75 79.2757 106.47 80.0476 201.83 72 .1137 69.67 82. 9697 109.28 76.8521 203.43 64.9302 70.83 85.7905 111. 00 71.0649 205.31 59.1132 72.81 90.6542 111.76 0.0000 210.85 59.0221 72.87 90.6673 114. 06 61.3553 215.65 59.3372 74.66 82.8384 116. 30 0.0000 222 .11 57.8879 74.82 82.8689 116. 74 58.3949 227.09 52.5644 74.97 82.8977 119.76 78.2588 227.38 50.7025 77 .11 83.3053 121.12 72.3087 228.16 0.0000 78.74 .84.3652 121.22 72.3208 228.18 52.6248 . 79. 69 67.9372 121.78 73.6148 116.74 52.6248 80.12 66.4910 122.06 73.6491 235.69 61. 0881 80.19 0.0000 122.92 72.5247 235. 96 56.8420 80.57 81.6833 123.07 75.0014 238.63 56.9977 81. 00 83.2749 265.00 85.3331 238.98 0.0000 81. 07 83.2878 125.81 79.0430 240.99 57.1344 81. 75 90.9949 127.23 89.1266 242.00 57.1930 83.79 59.4081 127.91 89.2246 244.70 44.4447 84.00 73.1509 129.30 89.4221 252.40 0.0000 85.43 76.4313 131. 20 71. 4208 252.80 39.5031 86.55 .79.6763 133.02 63. 2962 254.15 0.0000 86.79 79.7160 133.52 79.0154 256.23 46.4016 86.94 79.7414 136.00 75.3021 260.90 0.0000 Page 3763of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 39.4676 355.39 0.0000 584.27 15.9849 264.80 40.9353 356.01 31.5692 595.83 0.0000 265.00 40.9430 364.49 0.0000 427.87 28.3889 2 68. 22 48.8892 366.42 0.0000 602.52 0.0000 269.46 48.9451 372. 51 35.1531 604. 72 30.8335 270.03 48. 9716 375.05 33.0832 607.14 39.6905 271.23 52.9486 377.52 31.0043 609.32 28.5119 273.65 0.0000 356.01 25.7749 610.33 20.6124 276.40 41.3779 388.16 9.6953 614.28 33.1919 277.37 41. 414 7 388.63 0.0000 618.01 28.6339 277.60 41. 4232 391.69 30.7776 620.36 24.0433 278.00 26.6391 264.66 29.3401 621.93 21. 2852 279.20 32.5945 401. 81 29.3632 630.19 0.0000 279.54 41.4967 402.40 29.3747 631.29 17.6635 279.70 41.5027 404.85 40.3220 633.25 18.6102 280.46 38.5644 410.95 36 .1119 634.78 0.0000 283.69 39.6688 413.71 28.5047 635.95 13.0443 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 39.7298 423.72 0.0000 645.85 14.9775 285.90 0.0000 427.09 32.0769 657.76 7.5308 287.50 51. 7440 427.87 34.3067 657.90 0.0000 290.67 38.9175 433.94 32.2203 661.66 17.9180 293.27 0.0000 439.40 24.5289 664.57 0.0000 351. 93 . 39.0722 453.88 29.2553 666.33 0.0000 295. 96 39.0976 463.37 16.9775 666.50 0.0000 879.38 24 .1143 468.07 22.1343 667.71 0.0000 299.98 31.6884 473.00 0.0000 677.62 15.1997 300.09 31.6916 475.06 20.5181 685.70 0.0000 300.13 31.6923 476.78 21.6804 695.00 0.0000 301.36 42.3008 477.60 27.3994 696. 49 22.0349 302.85 39.32-93 482.18 21. 7 507 696. 51 22.0349 256.23 40.3947 487.02 0.0000 697:00 0.0000 304.85 0.0000 492.35. 0.0000 697.30 23.0010 306.78 34.9078 497.08 29.4486 697.49 23.0032 308.46 45. 5960 505.52 22.6294 702.65 23.0559 311. 90 33.5338 507.63 0.0000 706.68 19.2474 316.51 2.9. 5817 511. 00 23.2823 711. 68 24.1119 319.41 0.0000 514.00 33.2338 720. 70 0.0000 320.08 0.0000 514.00 33.2338 721. 93 0.0000 321.04 34.8114 520.40 35.1099 722. 78 15.5059 323.87 35.9179 520.69 0.0000 722.91 15.5068 325.23 35.9570 522.65 0.0000 723.31 15.5093 328.76 0.0000 527.90 0.0000 724.19 15.5151 333.37 44.6713 528.26 23.8030 727. 33 21.'7506 333.97 51.2100 529.59 11. 4690 733.00 21. 8032 334.37 41.9123 529.87 0.0000 735.93 17.1526 338.28 49. 8271 531. 02 0.0000 333.97 20.2846 338.32 49.8291 537.26 0.0000 739.50 0.0000 311. 90 45.2337 546.56 0.0000 747.24 15.6680 340.48 45.2337 552.55 16.9729 748.06 19.5917 340.55 0.0000 563.25 22.4602 752.31 16.6825 344.28 42.7601 569.33 18.9265 753.82 0.0000 345.93 37.5930 946.00 19.8294 756.73 13.7637 351.06 33.5475 569.70 20.7328 756.80 13.7642 351.93 33.5697 583.19 22.6936 884.68 18.9322 Page 3764 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.3680 1274.44 9.6671 1620.50 6.0920 766.42 18.9516 1001.03 17.2129 1621. 92 4.0625 766.84 15.7959 1002.74 7.5349 1678.03 0.0000 772.60 0.0000 1004.73 10.7712 1690.97 1.0309 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.1403 778.90 15.8735 1028.54 0.0000 1063.66 14.6720 783.70 0.0000 1037.84 8.7100 1771. 35 5.2412 785.37 12.9310 1038.76 0.0000 1791.20 0.0000 792.07 9.5748 631. 29 12.0098 1808.65 5.2808 794.95 18. 9722 1048.07 0.0000 1810.72 0.0000 795.86 23.9729 1049.04 14.2045 1836.06 3.1857 810.06 17.0768 1050.41 8.7451 810.29 18.0829 1063.66 14.0500 344.28 18.0840 1077.00 0.0000 810.76 15.0719 1077.34 9.9212 815.77 0.0000 1085.87 8.8423 1048.07 0.0000 1093.63 14.4028 832.01 19.4514 1099.45 13.3191 834.85 15.2129 1112. 07 10.0272 835.71 13.1888 1112. 84 11.1444 836.80 0.0000 1115:54 8.9224 846.75 0.0000 1120. 29 16.7542 846.77 14.2636 1120. 55 16.7551 856.80 0.0000 1221.41 16.7587 860.56 13.1086 1129. 67 19.0410 871.09 16.4502 1131. 51 0.0000 873.19 14.4050 1147.95 0.0000 875.33 0.0000 1173.23 7.5631 879.38 9.2815 1177.95 10.9055 880.51 11. 3488 1189.05 15.4992 883.24 16.5239 1204.77 17.3997 884.68 22.7318 1221.41 19.3214 889.28 11. 3850 1231. 02 16.6052 894.76 8.2966 1235.36 0.0000 898.04 13.4979 1238.28 17.1668 900.72 14.5503 1260.41 0.0000 903.28 . 19.0218 1271.87 8. 3962 911.20 17.7346 1274.44 15.8703 912.08 17.7398 1274.54 14.9367 923.98 0.0000 1291.59 9.3784 926.50 17. 8306 1298.22 0.0000 929 .11 17.8472 1312 .11 0.0000 937.49 22 .1113 1332.49 10.4274 944 .13 0.0000 1362.66 0.0000 946.00 20.0646 1365.19 5.7357 949.00 20.0849 1368.63 0.0000 667.71 0.0000 1384.29 9.6060 962. 31 16.9912 1408.01 4.8315 964.08 15.3013 1457.56 0.0000 966 .17 15.9499 1460.82 7.8305 911.20 15. 9654 1489.16 1.9709 968.97 15.9654 1505.03 9.8911 983.53 0.0000 1584.12 12.0861 984.45 0.0000 1596.21 0.0000 Page 3765 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:52.95 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 30-NOV-2015 10:43:00 Acquisition date : 3-0CT-2016 09:18:06. Sample ID G405235039 Sample quantity 1.75326E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.74 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : . LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 3 3 3 4. 0 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 0 14 2 15 2 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 40.61* 75.04 77.09* 87 .13 92.79* 178.00 181.98 186.14* 209.28 238.57* 241.92 259.16 272.46 295.31 300.41 338.82 351.74* 419.10 462.78 510.73* 518.48 583.37* 596.54 609.37* 728.90 795.09 861. 58 911. 87* 969.18* 1011. 06 1031.91 1104.71 1120.13 1136. 61 Page 3766of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 26 84 141 37 58 32 22 72 49 271 55 32 16 106 34 88 244. 19 41 75 13 93 6 158 17 15 26 58 36 11 8 13 34 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 86 131 92 119 128 55. 57 103 90 110 48 57 73 63 50 57 28 24 29 22 18 38 20 12 40 22 9 27 8 5 10 4 3 5 1. 05 1.16 1. 05 0.69 0.83 1. 05 0.94 0.80 1. 05 1.19 0.89 1.18 0.63 1. 54 1. 56 1. 67 1. 35 0.99 1. 37 1. 97 0.76 1. 46 0.64 1. 39 1. 37 1. 72 4.22 0.89 2.19 1.16 0.50 1. 29 2.31 0.85 81. 66 150.54 154.65 174.74 186.05 356.55 364.51 372.82 419.14 477.73 484.44 518.92 545.55 59l.25 601.46 678.32 704.17 838.96 926.37 1022.31 1037.82 1167. 68 1194. 03 1219.70 1458.93 1591.39 1724.45 1825 .11 1939.81 2023.64 2065.38 2211. 07 2241.95 2274.93 78 146 146 172 183 353 362 368 414 472 482 514 541 586 586 673 696 835 919 1014 1033 1163 1188 1214 1452 1582 1719 1817 1935 2017 2060 2208 2236 2272 8 7.12E-03 67.4 13 2.33E-02 24.9 13 3.91E-02 14.7 6 1.03E-02 49.8 8 1. 60E-02 37. 7 8 8.78E-03 44.2 7 6.00E-03 62.2 10 2.0lE-02 29.6 10 l.37E-02 39.1 10 7.52E-02 9.6 6 1. 53E-02 24. 8 10 8.84E-03 47.9 10 4.51E-03104.6 25 2.93E-02 16.4 25 9.38E-03 43.7 14 2. 44E-02 21. 0 16 6.77E-02 8.2 8 5.40E-03 50.1 15 1.13E-02 33. 2 15 2.08E-02 21.6 10 3.68E-03 67.9 13 2.58E-02 17.3 9 1.71E-03137.5 14 4.39E-02 9.3 15 4.59E-03 88.1 12 4.30E-03 64.6 12 7.35E-03 29.8 18 1.61E-02 25.1 12 1.00E-02 24.1 9 3.06E-03 46.5 10 2.22E-03 82.0 7 3.62E-03 39.3 11 9.57E-03 19.4 6 2 .14E-03 61. 0 Fit 7.66E-01 2.19E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235039 Acquisition date 3-0CT-2016 09:18:06 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1156.28 14 6 4.08 2314.30 2308 11 3.75E-03 43.3 36 0 1318. 67 10 7 1. 32 2639.37 2631 13 2.64E-03 64.1 37 0 1360.33 7 2 0.95 2722.75 2718 8 l.94E-03 51. 5 38 0 1460.76* 347 15 2.26 2923.82 2914 20 9.64E-02 6.1 39 0 1764.36 25 0 0.67 3531.64 3526 10 6.94E-03 20.0 Flag: "*" == Peak area was modified by background subtraction Page 3767 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:20:54 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 10:43:00 G405235039 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:18:06 175.33 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3768 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.74 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235039 Acquisition date 3-0CT-2016 09:18:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.030E+OO l.326E+Ol l.326E+Ol 12.16 OK CD-109 88.03 3.70* 4.450E+OO 6.341E-01 1. 007E+OO 214.94 SN-126 64.28 9.60 2.161E+OO Line Not Found Absent 86.94 8.90 4.450E+OO 2.636E-01 2.636E-01 214.94 OK 87.57 37.00* 4.450E+OO 6.341E-02 6.341E-02 214.94 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent 583.19 85.00* 2.178E+OO 2.398E-01 2.398E-01 34.57 OK 860.56 12.50 1. 591E+OO 6.033E-01 6.033E-01 59.55 OK BI-211 72. 87 1. 23 3.135E+OO Line Not Found Absent 351. 06 12.92* 3.338E+OO 7.570E-01 7.570E-01 111. 45 OK PB-212 74.82 10.28 3.363E+OO 1. 044E+OO. 1.044E+OO 72.10 OK 77 .11 17.10 3.570E+OO l.404E+OO l.404E+OO 29.48 OK 238. 63. 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 OK 300.09 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 OK BI-214 609.32 45.49* 2.102E+OO 7.863E-01" 7.865E-01 18.53 OK 1120. 29 14. 92 1. 288E+OO 7. 831E-01 7.834E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 3.570E+OO 2.476E+OO 2.477E+OO 29.48 OK 87.09 3.41 4.447E:+-00 Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.870E+OO 7.744E-01 7.747E-01 32.77 OK 351. 93 35.60* 3.336E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 OK 1120. 29 14.92 l.288E+OO 7. 831E-01 7.834E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 OK RA-224 240.99 4.10* 4.539E+OO 2 .131E-01 2 .131E-01 424.31 OK RA-226 609.32 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 OK 1120. 29 14.92 l.288E+OO 7.831E-01 7.834E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11.27 3.446E+OO 1.162E+OO 1.162E+OO 42.03 OK 794.95 4.25 1. 696E+OO 9.848E-01 9.848E-01 12 9. 2 6 OK 835.71 1. 61 l.630E+OO Line Not Found Absent 911.20 25.80* 1.520E+OO 6.656E-01 6.656E-01 50.14 OK 968. 97 15.80 1.448E+00 7.020E-01 7.020E-01 48.17 OK RA-228 105.21 1.10 5.460E+00 Line Not Found Absent 338.32 11.27 3.446E+OO l.162E+OO 1.162E+OO 42.03 OK 794.95 4.25 1. 696E+OO 9.848E-01 9.848E-01 129.26 OK 835.71 1. 61 l.630E+OO Line Not Found Absent 911.20 25.80* 1.520E+OO 6.656E-01 6.656E-01 50.14 OK 968. 97 15.80 l.448E+OO 7.020E-01 7.020E-01 48.17 OK TH-228 74.82 10.28 3.363E+OO 1.044E+OO 1.044E+OO 72.10 OK 77 .11 17.10 3.570E+OO 1.404E+OO l.404E+OO 29.48 OK 238.63 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 OK 300.09 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 OK TH-230 609.32 45.49* 2.102E+OO 7.863E-01 7.863E-01 18.53 OK 1120.29 14.92 1.288E+OO 7.831E-01 7. 831E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.675E-01 40.00 OK Page 3769 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235039 Acquisition date 3-0CT-2016 09:18:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status PA-231 283.69 1. 70 4.000E+OO Line Not Found Absent 301. 36 5.35* 3.815E+OO 8.623E-01 8.623E-01 87.41 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11.27 3.446E+OO l.162E+OO 1.162E+OO 42.03 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1.520E+OO 6.656E-01 6.656E-01 50.14 OK 968. 97 15.80 1.448E+OO 7.020E-01 7.020E-01 48.17 OK U-234 609.32 45.49* 2.102E+OO 7.863E-01 7.863E-01 18.53 OK 1120.29 14.92 1. 288E+OO 7.831E-01 7. 831E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.675E-01 40.00 OK AM-243 43.53 5.90 1.573E-01 Line Not Found Absent 74.66 67.20* 3.363E+OO 1.597E-01 1.597E-01 72 .10 OK ANH-511 511. 00 100.00* 2.432E+OO 1.498E-01 1. 498E-01 43.22 OK Flag: "*" = Keyline Page 3770of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:55.72 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l * *Acquisition date :-3-0CT-2016 09:18:06 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
Sample date 30-NOV-2015 10:43:00 Analyst initials: MXRl * *Sample ID G405235039 Sample Quantity l.7533E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF*;3 * ****************************************.*******F*****F************************* Combined Activity-MDA Report . NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.326E+Ol 1. 580E+OO CD-109 1.007E+OO 2 .121E+OO SN-126 6.341E-02 1. 336E-01 TL-208 2.398E-01 8.122E-02 BI-211 7.570E-01 8.268E-01 PB-212 7.262E-01 1.369E-01 BI-214 7.865E-01 l.428E-01 PB-214 1.049E+OO 1. 679E-01 RN-222* 7.865E-01 l.428E-01 RA-224 2 .131E-01 8.863E-01 RA-226 7.865E-01 l.428E-01 AC-228 6.656E-01 3. 271E-01 RA-228 6.656E-01 3. 271E-01 TH-228 7.262E-01 1.369E-01 TH-230 7.863E-01 1.428E--:Ol PA-231 8.623E-01 7.387E-01 TH-232 6.656E-01 3. 271E-01 U-234 7.863E-01 l.428E-01 AM-243 1. 597E-01 1.128E-01 ANH-511 1.498E-01 6.346E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 3771 of 5809 Key-Line Activity (pCi/GRAM 5.243E+OO l.652E-02 O.OOOE+OO 4.463E-03 3.230E-03 O.OOOE+OO O.OOOE+OO 6.097E-02 -3.090E-01 0.000E+OO K:L. Cnt Uncert ( 1. 96-sigma) 9.283E+OO 3.994E-02 1. 922E+41 1. 791E-02 3.450E-01 1. 799E+04 4.103E+02 5.493E-02 5.054E-01 l.666E+41 MDA (pCi/GRAM 6.697E-01 2.206E+OO l.451E-01 5.900E-02 2. 611E-01 8.133E'-02 5.130E-02 2.705E-01 5 .130E-02 1.002E+OO 5.130E-02 2.215E-01 2.215E-01 8.133E-02 5.128E-02 7.205E-01 2.215E-01 5.128E-02 9. 712E-02 4.247E-02 MDA (pCi/GRAM 2.066E+Ol 8.728E-02 O.OOOE+OO 4.736E-02 7.165E-01 O.OOOE+OO O.OOOE+OO 1.260E-01 8.620E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 -:-7.484E-03 3.959E-02 7.670E-02 NOT IDENT. C0-58 -7.752E-02 5.647E-01 1.070E+OO NOT IDENT. FE-59 -5.222E+OO 7.033E+OO 1.183E+Ol NOT IDENT. C0-60 -8.632E-03 3.585E-02 6.948E-02 NOT IDENT. ZN-65 7.066E-02 l.719E-01 3.344E-01 NOT IDENT. GE-68 1.875E+OO 2.148E+OO 4.931E+00 NOT IDENT. AS-73 2.388E+OO 1.164E+Ol 2.484E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.034E+04 O.OOOE+OO SHORT HLIF SE-75 7.491E-02 l.913E-01 3.718E-01 NOT IDENT. BR-77 O.OOOE+OO 2.624E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.916E+02 O.OOOE+OO SHORT HLIF RB-83 -6.218E-02 5.262E-01 9.413E-01 NOT IDENT. KR-85 3.336E+OO 7.501E+OO 1.191E+Ol NOT IDENT. *SR-85 3.821E-01 8.629E-01 1.370E+OO NOT IDENT. RB-86 O.OOOE+OO 3.330E+04 0.000E+OO SHORT HLIF Y-88 -9.573E-02 l.845E-01 3.575E-01 NOT IDENT. Y-91 l.148E+02 5.506E+02 1.130E+03 NOT IDENT. NB-94 l.948E-02 2.932E-02 6.179E-02 NOT IDENT. NB-95 -9.620E-01 9.766E-01 l.579E+00 NOT IDENT. NB-95M -1.519E+OO 2.407E+OO 3.782E+00 NOT IDENT. ZR-95 4.581E-01 l.437E+OO 2.929E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 759E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.106E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1.440E-02 2.937E-02 5.499E-02 NOT IDENT. RH-102 -7.529E-03 4.589E-02 8.928E-02 NOT IDENT. RU-103 -2.584E+OO 5.040E+OO 9.413E+OO FAIL ABUN RH-106 -2.712E-01 4.400E-01 7.843E-01 NOT IDENT. RU-106 -2.712E-01 4.400E-01 7.843E-01 NOT IDENT. AG-108M -1. 62 6E-03 l.942E-02 3.939E-02 NOT IDENT. AG-llOM 3.866E-02 9.659E-02 2. 081E-01 NOT IDENT. SN-113 -7.694E-02 l.833E-01 3.543E-01 NOT IDENT. CD-115 O.OOOE+OO 2. 2,98E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.196E+05 O.OOOE+OO
SHORT HLIF TE-123M -2.888E-02 1.149E-01 2 .161E-01 NOT IDENT. SB-124 -9.616E-02 1.738E+OO 3.755E+OO NOT IDENT. SB-125 -4.279E-02 8.552E-02 1*. 617E-01 FAIL. ABUN TE-125M -4.637E+Ol 2.518E+02 4.920E+02 NOT IDENT. I-126 O.OOOE+OO 1.212E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO .. 1. 678E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE-too 9 .117E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.179E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.688E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 781E+27 O.OOOE+OO SHORT HLIF 'BA-133 -2.530E-02 3.716E-02 6.099E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6. 496E-02 8.228E-02 l.044E-01 FAIL ABUN CS-135 -4.172E-02 1.274E-01 2.267E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3. 451E+05 O.OOOE+OO SHORT HLIF *-. BA-137M 3.342E-02 3.149E-02 6.981E-02 NOT*IDENT. CS-137 3.531E-02 3.327E-02 7.375E-02 NOT IDENT. CE-139 3.897E-02 9.331E-02 l.863E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 929E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.378E+05 O.OOOE+OO SHORT HLIF CE-141 -4.003E-02 2.481E+Ol 4.789E+Ol NOT IDENT. CE-143 O.OOOE+OO l.203E+41 0 .. OOOE+OO SHORT HLIF CE-144 4.438E-02 3.091E-01 6.095E-01 NOT IDENT. PM-144 2.998E-02 5.585E-02 l.148E-01 NOT IDENT. PR-144 2.630E+OO 4. 8'74E+OO l.002E+Ol NOT IDENT. PM-146 -l.209E-02 3.848E-02 7.393E-02 NOT IDENT. ND-147 O.OOOE+OO 3. 972E+07 O.OOOE+OO SHORT HLIF PM-147 1. 716E+02 6.675E+02 l.348E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 911E+41 O.OOOE+OO SHORT HLIF EU-150 l.204E-02 2.187E-02 4.305E-02 FAIL ABUN EU-152 -l.932E-02 7. 201E-02 l.279E-01 NOT IDENT. GD-153 -1.216E-01 l.455E-01 2.701E-01 NOT IDENT. EU-154 3.807E-02 9.700E-02 2 .115E-01 NOT IDENT. EU-155 -6.484E-02 *9.195E-02 l.718E-01 FAIL ABUN TB-160 -8.553E-01 1. 696E+OO 3.246E+OO FAIL ABUN H0-166M -4.712E-02 5.402E-02 8.980E-02 NOT IDENT. TM-171 -2.068E+Ol 2.838E+Ol 5.554E+Ol NOT IDENT. HF-172 5.585E-02 l.978E-01 3. 963E-01 NOT IDENT. LU-172 -4.625E-02 5.750E-02 1. OOlE-01 FAIL ABUN LU-176 -l.041E-03 2.284E-02 4.166E-02 FAIL ABUN HF-181 l.437E-01 3.402E+OO 7.025E+OO NOT IDENT. TA-182 -2.623E-01 1.024E+OO l.9JOE+00 FAIL ABUN Page 3772 of 5809 RE-183 2.188E+OO 3.788E+OO 8.248E+OO NOT IDENT. RE-184 -3.40SE+OO 2.920E+Ol 5.957E+Ol NOT IDENT. W-188 l.452E+Ol 1.003E+02 1.895E+02 NOT IDENT. IR-192 2.705E-02 3.866E-01 7.977E-01 FAIL ABUN HG-203 -5.983E-02 2.089E+00 4.283E+OO NOT IDENT. BI-207 -l.693E-03 4.688E-02 9.373E-02 FAIL ABUN PB-210 5.454E+OO 6.175E+OO 1.401E+Ol NOT IDENT. PB-211 1.141E-01 4.985E-01 l.042E+OO NOT IDENT. BI-212 8.082E-Ol 5.029E-01 l.140E+OO NOT IDENT. RN-219 l .119E-01 3. ll 7E-01 6.533E-01 FAIL ABUN RA-223 2.153E-01 4.781E-01 l.014E+OO FAIL ABUN 'AC-227 -1.229E-01 2.223E-01 3.497E-01 FAIL ABUN TH-227 -l.229E-01 2.223E-01 3.497E-01 FAIL ABUN TH-229 -6. 383E-02 . 3.761E-01 7.027E-01 FAIL ABUN TH-231 2.153E-01 4.781E-01 l.014E+OO FAIL ABUN PA-233 -2. 411E-03 4.832E-02 9.814E-02 FAIL ABUN PA-234 -1.025E-01 2.354E-01 4.520E-01 NOT IDENT. PA-234M -1. 321E-01 3.478E+OO 7.102E+OO NOT IDENT. TH-234 1. 396E+OO 1.253E+OO 2.786E+OO FAIL ABUN U-235 6.815E-02 1.477E-01 2.974E-01 FAIL ABUN NP-237 -2. 4.832E-02 9.814E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 1. 396E+OO l.253E+OO 2.786E+OO FAIL ABUN NP-239 7.875E-03 1. 966E-01 3.902E-01 NOT IDENT. PU-239 6.336E+Ol 2.626E+02 5.225E+02 NOT IDENT. AM-241 3.515E-02 1.553E-01 3.283E-01 NOT IDENT. CM-243 3.830E-02 7.988E-02 l.664E-01 NOT IDENT. BK-247 -l.032E-02 6.550E-02 1.193E-01 NOT IDENT. CM-247 -5.977E-03 2.931E-02 5. 7 61E-02 NOT IDENT. CF-249 -1.810E-03 2.889E-02 5.831E-02 NOT IDENT. CF-251 l.837E-01 1.590E-01 1.899E-01 FAIL ABUN Page 3773 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:53.64 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 340 10.66* l.030E+OO 1. 326E+Ol 1.326E+Ol 12.16 CD-109 88.03 52 3.70* 4.450E+OO 1.348E+OO 2.141E+OO 99.62 SN-126 64.28 ------9.60 2.161E+OO ------Line Not Found ------86.94 52 8.90 4.450E+OO 5.603E-01 5.603E-01 99.62 87.57 52 37.00* 4.450E+OO l.348E-01 l.348E-01 99.62 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 104 85.00* 2.178E+OO 2.398E-01 2.398E-01 34.57 860.56 28 12.50 1.591E+OO 6.033E-01 6.033E-01 59.55 BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 291 12.92* 3.338E+OO 2.891E+OO 2.891E+OO 16.33 PB-212 74.82 120 10.28 3.363E+OO 1.481E+OO 1.481E+OO 49.90 77 .11 200 17.10 3.570E+00 1.404E+OO 1.404E+OO 29.48 238.63 339 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 300.09 41 3.30 3.815E+OO l.398E+00 1.39BE+OO 87.41 BI-214 609.32 176 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 1120.29 35 14.92 l.288E+OO 7. 831E-01 7.834E-01 38.74 1764.49 24 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 PB-214 74.82 120 5.80 3.363E+OO 2.624E+OO 2.625E+OO 49,90 77 .11. 200 9.70 3.570E+00 2.476E+OO 2.477E+OO 29.48 87.09 52 3.41 4.450E+00 1.462E+OO 1.463E+OO 99.62 242.00 69 7.25 4.539E+OO 8.949E-01 8.952E-01 49.62 295.22 129 18.42 3.870E+OO 7.744E-01 7.747E-01 32.77 351. 93 291 35.60* 3.338E+OO 1. 04'9E+OO 1.049E+OO 16.33 RN-222 609.32 176 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 1120.29 35 14.92 1.288E+OO 7.831E-01 7.834E-01 38.74 1764.49 24 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 RA-224 240.99 69 4.10* 4.539E+OO 1.582E+OO l'. 582E+OO 49.62 RA-226 609.32 176 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 1120.29 35 14.92 1.288E+OO 7. 831E-01 7.834E-01 38.74 1764.49 24 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 AC-228 105.21 ------1.10 5.460E+00 ------Line Not Found ------338.32 105 11. 27 3.446E+00 l.162E+OO l.162E+OO 42.03 794'.95 17 . 4.25 1. 696E+OO 9.848E-01 9.848E-01 129. 26 835.71 ------1. 61 1.630E+00 ------Line Not Found ------911. 20 61 25.80* 1. 520E+OO 6.656E-01 6.656E-01 50.14 968. 97 37 15.80 1.448E+OO 7.020E-01 7.020E-01 48.17 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 105 11. 27 3.446E+OO l.162E+OO 1.162E+OO 42.03 794.95 17 4.25 1. 696E+OO 9.848E-01 9.848E-01 129.26 835. 71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 61 25.80* 1.520E+OO 6.656E-01 6.656E-01 50.14 968. 97 37 15.80 1.448E+OO 7.020E-01 7.020E-01 48.17 TH-228 74.82 120 10.28 3.363E+OO 1. 481E+OO 1.481E+OO 49.90 77.11 200 17.10 3.570E+OO 1.404E+OO 1.404E+OO 29.48 238.63 339 43.60* 4.587E+00 7.262E-01 7.262E-01 i'9. 24 300.09 41 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 TH-230 609.32 176 45.49* 2.102E+00 7.863E-01 7.863E'-01 18.53 Page 3774of5809 Nuclide Line Activity Report (continued) Sample ID : G405235039 Acquisition date Page : 2 3-0CT-2016 09:18:06 Nuclide Type: Nuclide PA-231 TH-232 U-234 AM-243 ANH-511 Flag: "*" Page 3775 of 5809 Energy 1120.29 1764.49 283.69 301.36 105.21 338.32 835. 71 911.20 968.97 609.32 1120. 29 1764.49 43.53 74.66 511. 00 Key line Area %Abn 35 14.92 24 15.30 ------1. 70 41 5.35* ------1.10 105 11.27 ------61 25.80* 37 15.80 . 176 45.49* 35 14.92 24 15.30 ------5.90 120 67.20* 85 100.00* Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi7GRAM %Error 1.288E+OO 7. 831E-01 7. 831E-01 38.74 8.674E-01 7.675E-01 7.675E-Ol 40.00 4.000E+OO ------Line Not Found ------3.815E+OO 8.623E-01 8.623E-01 87.41 5.460E+OO ------Line Not Found ------3.446E+OO l.162E+OO 1.162E+OO 42.03 1.630E+OO ------Line Not Found ------l.520E+OO 6.656E-01 6.656E-01 50.14 l.448E+OO 7.020E-01 7.020E-01 48.17 2.102E+OO 7.863E-01 7.863E-01 18.53 1.288E+OO 7. 831E-01 7.831E-01 38.74 8.674E-01 7.675E-01 7.675E-01 40.00 l.573E-01 ------Line Not Found ------3.363E+OO 2.265E-01 2.265E-01 49. 90. 2.432-E+OO l.498E-01 l.498E-01 43.22 Summary of Nuclide Activity Sample ID : G405235039 Acquisition date Page : 3 3-0CT-2016 09:18:06 Total number of lines +/-n spectrum 39 Number of unidentified lines 13 Number of lines tentatively identified by NID 26 66.67% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi7GRAM 2-Sigma Error %Error Flags K-40
1. 25E+09Y 1. 00 1.326E+Ol 1.326E+Ol 0.161E+Ol 12.16 CD-109 461.40D 1. 59 1.348E+OO 2.141E+OO 2.132E+OO 99.62 SN-126 2.30E+05Y 1. 00 l.348E-01 1.348E-01 l.343E-01 99.62 TL*-208 l.41E+10Y 1. 00 2.398E-01 2.398E-01 0.829E-01 34.57 BI-211 7.04E+08Y .1. 00 2.891E+OO 2.891E+OO 0.472E+OO 16.33 PB-212 1. 41E+10Y 1. 00 7 .-262E-01 7.262E-01 1.397E-01 19.24 BI-214 1600.00Y 1. 00 7.863E-01 7.865E-01 1.457E-01 18.53 PB-214 1600. OOY 1. 00 1.049E+OO 1.049E+OO 0.171E+OO 16.33 RN-222 1600. OOY 1. 00 7.863E-01 7.865E-01 l.457E-01 18.53 RA-224 l.41E+l0Y 1. 00 1.582E+OO 1.582E+OO 0.785E+OO 49.62 RA-226 1600. OOY 1. 00 7.863E-01 7.865E-01 1.457E-01 18.53 AC-228 1.41E+10Y 1. 00 6.656E-01 6.656E-01 3.337E-01 50.14 RA-228 l.41E+10Y 1. 00 6.656E-01 6.656E-01 3.337E-01 50.14 TH-228 l.41E+l0Y 1. 00 7.262E-01 7.262E-01 1.397E-01 19.24 TH-230 7.54E+04Y 1. 00 7.863E-01 7.863E-01 1.457E-01 18.53 PA-231 7.04E+08Y 1. 00 8.623E-01 8. 62'3E-01 7.537E-01 87.41 TH-232 l.41E+l0Y 1. 00 6.656E-01 6.656E-01 3.337E-01 50.14 U-234 2.45E+05Y 1. 00 7.863E-01 7.863E-01 1.457E-01 18.53 *AM-243 7370.00Y 1. 00 2.265E-01 2.265E-01 1.130E-01 49.90 ANH-511 l.OOE+09Y 1. 00 1.498E-01 1.498E-01 0.648E-01 43.22 ------------------Total Activity 2. 913E+Ol 2.992E+Ol Grand Total Activity 2.913E+Ol 2.992E+Ol Flags: "K" Keyline not found "M" Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit Page 3776of5809 Unidentified Energy Lines Page : 4 Sample ID : G405235039 Acquisition date : 3-0CT-2016 09:18:06 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags* 0 40.61 39 131 1. 05 81. 66 78 8 7.12E-03 **** 5.88E-02 0 92.79 80 179 0.83 186.05 183 8 l.60E-02 75.5 4.84E+00 T 0 178.00 41 72 1. 05 356.55 353 8 8.78E-03 88.3 5.53E+OO T 0 181.98 28 74 0.94 364.51 362 7 6.00E-03 **** 5.46E+OO T 0 186.14 93 133 0.80 372. 82 368 10 2. OlE-02 59.2 5.40E+OO T 0 209.28 63 114 1. 05 419.14 414 10 l.37E-02 78.3 5.03E+OO 0 259.16 39 71 1.18 518.92 514 10 8.84E-03 95.8 4.30E+OO 0 272.46 20 90 0.63 545.55 541 10 4.51E-03 **** 4.13E+OO T 0 419.10 23 28 0.99 838. 96 835 8 5.40E-03 **** 2.87E+OO 0 462.78 47 34 1. 37 926.37 919 15 1.13E-02 66.4 2.64E+OO T 0 518.48 15 20 0.76 1037.82 1033 10 3.68E-03 **** 2.40E+OO 0 596. 54 7 22 0.64 1194. 03 1188 9 1.71E-03 **** 2.14E+OO T 0 728.90 18 44 1. 37 1458.93 1452 15 4.59E-03 **** 1.82E+OO 0 1011. 06 11 5 1.16 2023.64 2017 9 3.06E-03 92.9 1.40E+OO 0 1031.91 8 10 0.50 2065.38 2060 10 2.22E-03 **** 1.38E+OO 0 1104.71 13 4 1. 29 22:1!1. 07 2208 7 3.62E-03 78.6 1.30E+OO 0 1136.61 8 5 0.85 2274.93 2272 6 2.14E-03 **** l.27E+OO 0 1156.28 14 6 4.08 2314.30 2308 11 3.75E-03 86.5 l.25E+00 0 1318. 67 9 6 1. 32 2639.37 2631 13 2.64E-03 **** 1.12E+OO 0 1360.33 7 2 O.Q5 2722.75 2718 8 1.94E-03 **** 1. lOE+OO Flags: "T" = Tentatively associated Page 3777of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:21:08.10 ******************************************************************************* .
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l * *Acquisition date 3-0CT-2016 09:18:06 Sensitivity 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
Sample date 30-NOV-2015 10:43:00 Nuclide Library : SOLID *
Sample ID G405235039 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7533E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Cri tica.l Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM 2.814E-01 1.042E+OO 6.871E-02 2.623E-02 l.163E-01 3.755E-02 1. 931E-02 1.301E-01 1. 931E-02 4.678E-01 1. 93.lE-02 9.554E-02 9.554E-02 3.755E-02 l.930E-02 3.299E-01 9.554E-02 l.930E-02 4.568E-02 l.873E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3778 of 5809 Le (pCi/GRAM 9.075E+OO 3.726E-02 O.OOOE+OO 1.678E-02 -3. 091E-01 O.OOOE+OO O.OOOE+OO 5.573E-02 3. 721E-01 O.OOOE+OO 3.557E-02 NOT IDENT. NOT TDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 FE-59 C0-60 ZN-65 . GE-68 AS-73 A*S-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3779of5809 4.616E-01 4.944E+OO 2.883E-02 l.455E-01 2.161E+OO l.144E+Ol 0. OOOE'+oo 1. 711E-01 O.OOOE+OO O.OOOE+OO 4.034E-Ol 5.345E+OO 6.146E-01 O.OOOE+OO 1. 2 67E-Ol 4.928E+02 2.767E-02 6.929E-01 1. 739E+OO 1.289E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 561E-02 3.846E-02 4.088E+OO 3.398E-01 3.398E-01 1. 727E-02 9.166E-02 1. 57 3E-01 O.OOOE+OO O.OOOE+OO l.003E-01 l.406E+OO 7.186E-02 2.286E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.732E-02 O.OOOE+OO 4.669E-02 1. 041E-01 O.OOOE+OO O.OOOE+OO 3.143E-02 3.320E-02 8.666E-02 O.OOOE+OO O.OOOE+OO *2.237E+Ol 0.000E+OO 2.844E-01 5.162E-02 4.506E+OO 3.308E-02 O.OOOE+OO 6. 2 63E+02 0.000E+OO 1. 966E-02 5.685E-02 l.245E-01 9.017E-02 7. 961E-02 l.380E+OO 3.890E-02 2.547E+Ol 1. 851E-01 4.026E-02 1.907E-02 3.056E+OO 8.472E-01 3.843E+OO NOT IDENT. NOT IDENT. NOT .IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDE.NT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT, NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT I DENT .. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIE:' NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3780 of 5809 2.553E+Ol 8.639E+Ol 3.620E-01 l.958E+OO 4.084E-02 6.516E+OO 4.664E-01 5.207E-01 2.955E-01 4.639E-01 l.598E-01 l.598E-01 3.245E-01 4.639E-01 4.473E-02 l.924E-01 3.049E+oo* l.307E+OO l.390E-01 4.473E-02 O.OOOE+OO l.307E+OO l.812E-01 2.443E+02 l.528E-01 7.739E-02 5.475E-02 2.595E-02 2.612E-02 8.839E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT.IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:21:14.84 ' *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l *
Acquisition date 3-0CT-2016 09:18:06 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
Sample date 30-NOV-2015 10:43:00 Nuclide Library : SOLID * * *Sample ID G405235039 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : l.7533E+02 GRAM *
Quantity Err(%) : l.1407E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM
K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 1. 326E+Ol 1.007E+OO 6. 341E-02 2.398E-01 7.570E-01 7.262E-01 7.865E-01 1.049E+OO 7.865E-01 2.131E-01 7.865E-01 6.656E-01 6.656E-01 *7.262E-01 7.863E-01 8.623E-01 6.656E-01 7.863E-01 l.597E-01 l.498E-01 Act Error (1. 96-sigma) 1. 724E+OO 2.128E+OO l.339E-01 8.186E-02 8.377E-01 l.422E-01 1. 467E-01 1.735E-01 1. 467E-01 8.909E-01 l.467E-01 3.288E-01 3.288E-01 l.422E-01 1. 467E-01 7.613E-01 3.288E-01 l.467E-01 l .136E-01 6.375E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 3781of5809 Key-Line Activity (pCi/GRAM 5.243E+OO l.652E-02 -l.OOOE+41 4.463E-03 3.230E-03 -8.919E+03 1.329E+02 6.097E-02 -3.090E-01 -1.000E+-41 K.L Act error (1. 96-sigma) 9.285E+OO 3.994E-02 1. 974E+41 l.791E-02 3.450E-01 1. 799E+04 4.103E+02 5.499E-02 5.056E-01 1.666E+41 TPU (1.96-sigma) 1. 724E+OO 2.128E+OO l.339E-01 8.186E-02 8.377E-01 l.422E-01 1.467E-01 1.735E-01 1:467E-01 8.909E-01 l.467E-01 3.288E-01 3.288E-01 1.422E-01 l.467E-01 7. 613E-01 3.288E-01 l.467E-01 l.136E-01 6.375E-02 TPU ( 1. 96-sigma) 9.581E+OO 4.063E-02 O.OOOE+OO l.803E-02 3.450E-01 l.844E+04 4.147E+02 6.148E-02 5.244E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 -7.484E-03 3.959E-02 3.973E-02 NOT IDENT. C0-58 -7.752E-02 5.647E-01 5.658E-01 NOT IDENT. FE-59 -5.222E+00 7.043E+OO 7.426E+OO NOT IDENT. C0-60. -8.632E-03 3.585E-02 3.606E-02 NOT IDENT. ZN-65 7.066E-02 l.719E-01 l.748E-01 NOT IDENT. GE-68 1. 875E+OO 2.149E+OO 2.310E+OO NOT IDENT. AS-73 2.388E+OO 1.165E+Ol l.170E+Ol NOT IDENT. AS-74 3.836E+03 l.034E+04 1.048E+04 SHORT HLIF SE-75 7.491E-02 1. 913E-01 l.943E-01 NOT IDENT. BR-77 l.392E+39 l.237E+40 0.000E+OO SHORT HLIF SR-82 5.203E+Ol 7.916E+02 7.920E+02 SHORT HLIF RB-83 -6.218E-02 5.263E-01 5.270E-01 NOT IDENT. KR-85 3.336E+OO 7.502E+OO 7. 651E+OO NOT IDENT. SR-85 3.821E-01 8.631E-01 8.801E-01 NOT IDENT. RB-86 3.786E+04 3.335E+04 3.746E+04 SHORT HLIF Y-88 -9.573E-02 1.847E-01 1. 896E-01 NOT IDENT. Y-91 l.148E+02 5.507E+02 5.531E+02 NOT IDENT. NB-94 l.948E-02 2.933E-02 3.062E-02 NOT IDENT. NB-95 -9.620E-01 9.775E-01 1.069E+OO NOT IDENT. NB-95M -1.519E+OO 2.410E+OO 2.505E+OO NOT IDENT. ZR-95 4.581E-01 1.437E+OO 1. 451E+OO NOT IDENT. NB-97 -l.000E+41 2.180E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 1. 760E+41 O.OOOE+OO SHORT HLIF M0-99 -6.006E+32 1.107E+33 O.OOOE+OO SHORT HLIF TC-99M 1. OOOE+41 3.595E+41 0.000E+OO SHORT HLIF RH-101 -1. 440E-02 2.949E-02 3.020E-02 NOT IDENT. RH-102 -7.529E-03 4.590E-02 4.602E-02 NOT IDENT .* RU-10-3 -2.584E+OO 5.042E+OO 5.174E+OO FAIL ABUN RH-106 -2.712E-01 4.403E-01 4.570E-01 NOT IDENT. RU-106 -2.712E-01 4.403E-01 4.570E-01 NOT IDENT. AG-108M -1. 62 6E-03 1.942E-02 l.943E-02 NOT IDENT. AG-llOM 3.866E-02 9.661E-02 9.817E-02 NOT IDENT. SN-113 -7.694E-02 1.833E-01 1. 866E-01 NOT IDENT. CD-115 1.191E+40 2.308E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 7.387E+04 l.200E+05 l.245E+05 SHORT HLIF TE-123M -2.888E-02 l.149E-01 l.157E-01 NOT IDENT. SB-124 -9.616E-02 1. 738E+OO 1.739E+OO NOT IDENT. SB-125 -4.279E-02 8.554E-02 8.768E-02 FAIL ABUN TE-125M -4.637E+Ol 2.518E+02 2.527E+02 NOT IDENT. I-126 l.661E+05 l.212E+06 l.214E+06 SHORT HLIF SB-126 -l.473E+06 1. 701E+06 l.826E+06 SHORT HLIF SB-127 1.312E+23 2.064E+23 O.OOOE+OO SHORT HLIF I-131 -4.759E+09 7.182E+09 7.496E+09 SHORT HLIF I-132 -l.OOOE+41 1.906E+42 0.000E+OO SHORT HLIF TE-132 9. 811E+26 1. 828E+27 O.OOOE+OO SHORT HLIF BA-133 -2.530E-02 3.718E-02 3.889E-02 NOT IDENT. I-133 1.000E+41 9.506E+41 O.OOOE+OO SHORT HLIF CS-134 6. 496E-02 8.233E-02 8.738E-02 FAIL ABUN CS-135 -4.172E-02 1. 27 4E-01 l.288E-01 NOT IDENT. I-135. l.OOOE+41 2.240E+42 O.OOOE+OO SHORT HLIF CS-136 -6.943E+04 3.452E+05 3.466E+05 SHORT HLIF BA-137M 3.342E-02 3.153E-02 3.494E-02 NOT IDENT. CS-137 3.531E-02 3. 331E-02 3. 691E-02 NOT IDENT. CE-139 3.897E-02 9.364E-02 9.527E-02 NOT IDENT. BA-140 9.426E+05 1.930E+06 1.976E+06 SHORT HLIF LA-140 -1.865E+04 4.378E+05 4.379E+05 SHORT HLIF CE-141 -4.003E-02 2.481E+Ol 2.481E+Ol NOT IDENT. CE-143 l.000E+41 l .'208E+41 O.OOOE+OO SHORT HLIF CE-144 4.438E-02 3. 091E-01 3.097E-01 NOT IDENT. PM-144 2.998E-02 5.588E-02 5.749E-02 NOT IDENT. PR-144 2.630E+OO 4.875E+OO 5.017E+OO NOT IDENT. PM-146 -1. 209E-02 3.849E-02 3.888E-02 NOT IDENT. ND-147 -1.703E+07 3.973E+07 4.046E+07 SHORT HLIF PM-147 1. 716E+02 6.675E+02 6. 720E+02 NOT IDENT. PM-149 -1.000E+41 l.923E+41 0.000E+OO SHORT HLIF EU-150 2.188E-02 2.254E-02 FAIL ABUN EU-152 -1.932E-02 7.202E-02 7.254E-02 NOT IDENT. GD-153 -1.216E-01 1.456E-01 1.556E-01 NOT IDENT. EU-154 3.807E-02 9. 701E-02 9.851E-02 NOT' IDENT. EU-155 -6.484E-02 9.207E-02 9.660E-02 FAIL ABUN TB-160 -8.553E-01 1. 696E+OO 1. 740E+OO FAIL ABUN H0-166M -4.712E-02 5.408E-02 5. 811E-02 NOT IDENT. TM-171 -2.068E+Ol 2.844E+Ol 2.993E+Ol NOT IDENT. HF-172 5.585E-02 1.980E-01 1. 996E-01 NOT IDENT. LU-172 -4. 62'5E-02 5.769E-02 6 .134E-02 FAIL ABUN LU-176 -1. 041E-03 2.284E-02 2.285E-02 FAIL ABUN HF-181 l.437E-01 3.402E+OO 3.403E+OO NOT IDENT. TA-182 -2.623E-01 1.024E+OO 1.031E+OO FAIL ABUN Page 3782 of 5809 RE-183 2.188E+OO 3.804E+OO 3.930E+OO NOT IDENT. RE-184 -3.405E+OO 2.922E+Ol 2.926E+Ol NOT IDENT. W-188 1.452E+Ol 1.003E+02 l.005E+02 NOT IDENT. IR-192 2.705E-02 3.866E-01 3.868E-01 FAIL ABUN HG-203 -5.983E-02 2.089E+OO 2.089E+OO NOT IDENT. BI-207 -1.693E-03 4.688E-02 4.688E-02 FAIL ABUN PB-21.0 5.454E+OO 6.195E+OO 6.665E+OO NOT IDENT. PB-211 1.141E-Ol 4.985E-01 5.012E-01 NOT IDENT. BI-212 8 .. 082E-01 5.046E-01 6.223E-01 NOT IDENT. RN-219 1.119E-01 3.120E-01 3 .161E-01 FAIL ABUN RA-223 2'.153E-Ol 4.783E-01 4.880E-01 FAIL ABUN AC-227 -1.229E-01 2.228E-01 2.296E-01 FAIL ABUN TH-227 -l.229E-01 2.228E-01 2.296E-01 FAIL ABUN TH-229 -6.383E-02 3.761E:-01 3. 772E-01 FAIL ABUN TH-231 2.153E-01 4.783E-01 4.880E-01 FAIL ABUN PA-233 -2. 411E-03 4.832E-02 4.833E-02 FAIL ABUN PA-234 -1.025E-01 2.630E-01 2.671E-01 NOT IDENT. PA-234M -1. 321E-01 3.478E+OO 3.479E+OO NOT IDENT. TH-234 1. 396E+OO 1.291E+OO l.436E+OO FAIL ABUN U-235 6.815E-02 l.478E-01 l.509E-01 FAIL ABUN NP-237 -2. 411E-03 4.832E-02 4.833E-02 FAIL ABUN NP-238 1.000E+41 6.595E+41 O.OOOE+OO SHORT HLIF U-238 1.396E+OO 1. 2 91E+OO 1.436E+OO FAIL ABUN NP-239 7.875E-03 1. 966E-01 1. 966E-01 NOT IDENT. PU-239 6.336E+Ol 2. 62 6E+02 2.642E+02 NOT IDENT. AM-241 3.515E-02 1.553E-01 1. 561E-01 NOT IDENT. CM-243 3.830E-02 7. 996E-02 8.180E-02 NOT IDENT. BK-247 -l.032E-02 6.553E-02 6.570E-02 NOT IDENT. CM-247 -5.977E-03 2.932E-02 2.945E-02 NOT IDENT. CF-249 -1.810E-03 2.889E-02 2.890E-02 NOT IDENT. CF-251 l.837E-01 1.604E-01 1. 805E-01 FAIL ABUN Page 3783 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 48.2185 87.09 90.6453 136.47 65.5134 45.60 55.0496 87.57 105.2002 140.51 0.0000 46.54 42.7447 88.03 97.4013 143.76 57.5377 49. 72 0.0000 88.34 97.4630 144.24 57.5781 51. 35 45.1748 88.47 97.4886 145.44 67.4719 51. 87 47.0528 89. 96 49.5518 152.43 56.0528 52.39 51.6545 1093.63 82. 0372 153.25 0.0000 52.97 44.4788 91.11 0.0000 323.87 59.4959 53.44 39.0847 92.59 63.7588 156.02 0.0000 54.07 45.5284 93.35 63.8540 158.56 0.0000 57.36 0.0000 94.56 54.6708 159.00 60.9955 57.53 56.9976 94.65 54.6804 162.33 50.1286 57.98 50.6236 94.67 54.6825 162.66 0.0000 59.27 59 .1111 94.87 54.7038 163.33 68.0423 59.32 59.1189 97.43 64.3589 165.86 50.3627 59.54 56.3805 98.43 62.4659 176.31 34.7836 60. 96 63.0852 98.44 62. 4671 176.60 0.0000 61.17 67.7608 99.53 58. 5571 177.52 31. 8072 62.93 53.1497 100 .11 64.6846 181.07 0.0000 63.29 46.6652 102.03 68.9727 181.52 36.5313 63.58 57.9075 103.18 49.8056 184.41 36.6602 64.28 71.1091 103.37 49.8232 143.76 35.1888 66.73 57.4230 105.21 69.3738 193.51 52 .1157 67.24 65.0349 105.31. 69.3862 197.03 55.8186 125.81 66.9921 106.12 60.2905 198.01 48.8964 67.75 67.0029 106.47 60.3283 201.83 52.6190 69.67 70.1581 109.28 61. 6571 203.43 55.0573 70.83 72.2525 111. 00 59.7815 205.31 48.5214 72. 81 68.7673 111.76 0.0000 210.85 47.2461 72.87 68. 7772 114.06 76. 6755. 215.65 51.0566 74.66 83.4476 116. 30 0.0000 222.11 51. 4109 74.82 83.4781 116.74 56.2070 227.09 45.6712 74.97 83.5066 119. 7 6 62.7667 227.38 37.2694 77 .11 83.9095 121.12 52.4223 228.16 0.0000 78.74 74.8559 121. 22 5.2.4311 228.18 43.3169 79.69 67.2518 121. 78 59.8258 116.74 43.3169 80.12 62.1367 122.06 58.8032 235.69 58.2026 80.19 0.0000 122. 92 62.0398 235. 96 58.2180 80.57 67.3804 123.07 62. 0551 238.63 48.6462 81. 00 69.0646 265.00 63.1691 238.98 0.0000 81. 07 72. 9664 125.81 61.2723 240.99 65.8273 81. 75 76.9700 127.23 73.0567 242.00 35.7943 83.79 84.8067 127.91 69.9558 244.70 19.5764 84.00 82.2338 129.30 63.7344 252.40 0.0000 85.43 85.0983 131.20 64.9893 252.80 35.7632 86.55 90.5450 133.02 64.1025 254.15 0.0000 86. 79 90.5892 133.52 62.0135 256.23 49.4910 86.94 90.6180 136.00 57.9543 260.90 0.0000 Page 3784 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 37.4139 355.39 0.0000 584.27 21.6375 264.80 44.9033 356.01 36.3224 595.83 0.0000 265.00 44. 9110 364.49 0.0000 427.87 16.2049 268.22 48.7988 366.42 0.0000 602.52 0.0000 269. 4.6 . 50.1074 372.51 28.1398 604. 72 17.1747 270.03 45 .1198 375.05 30.9197 607.14 10.9422 271.23 "43.4973 377.52 29.1517 . 609. 32 3.1298 273.65 0.0000 356.01 24.7072 610.33 3.1312 276.40 31.5155 388.16 25.6997 614.28 14.1180 277.37 39.3656 388.63 0.0000 618.01 18.8577 277.60 39.3732 391.69 26.6825 620.36 17.8301 278.00 37.0310 264.66 24.0698 621.93 19.9432 279.20 38.7563 401. 81 25.0148 630.19 0.0000 279.54 42.9814 402.40 30.5864 631.29 14.7611 279.70 40.4590 404.85 21.3529 633.25 16.8854 28.0. 46 37.9559 410.95 28.8979 634.78 0.0000 283.69 36.3731 413.71 28.0170 635.95 17.9636 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.8867 423. 72 0.0000 645.85 15.9241 285.90 0.0000 427.09 8.4791. 657.76 17.0794 287.50 27.1595 427.87 28:2776. 657.90 0.0000 290.67 33.1919 433.94 17.9791 661. 66 13.9019 293.27 0.0000 439.40 14.2432 664.57 0.0000 351. 93 39.3029 453.88 28.7451 666.33 0.0000 295. 96 39.3282 463.37 16.3837 666.50 0.0000 879.38 39.4161 468.07 14.4974 667.71 0.0000 299.98 39.4629 473.00 0.0000 677.62 8.6172 300.09 39.4667 475.06 21. 3519 685.70 0.0000 300.13 39.4676 476.78 18.4592 695.00 o. *oooo 301.36 39.5088 477.60 11. 6641 696.49 19. 5513 302.85 39.5584 482.18 14.6198 696. 51 19.5520 256.23 37.4607 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6452 306.78 40.1208 497.08 20.6454 697.49 28.2534 308.46 38.8806 505.52 20.7449 702.65 16.3367 311. 90 36.3920 507.63 0.0000 706.68 17.4564 316.51 31. 3110 511. 00 18.8276 711. 68 25.1478 319.41 0.0000 514.00 17.8667 720.70 0.0000 320.08 0.0000 514*. 00 17.8667 721. 93 0.0000 321.04 38.4087 520.40 13.4478 722.78 13.1836 323.87 31.4971 520.69 0.0000 722.91 11.5361 325.23 42.9179 522.65 0.0000 723.31 11.5382 328.76 0.0000 527:90 0.0000 724.19 14.8403 333.37 25.3875 528.26 7.0031 727.33 14.3097 333.97 27.7804 529.59 12.0142 733.00 9.9305 334.37 33.0826 529.87 0.0000 735.93 8.8379 338.28 26.5466 531. 02 0.0000 333.97 11.0547 338.32 26.5472 537.26 0.0000 739.50 0.0000 311. 90 26.5918 546.56 0.0000 747.24 21. 0897 340.48 26.5918 552.55 20.2718 748.06 16.6553 340.55 0.0000 563.25 28.5400 752.31 13.3477 344.28 25.3358 569. 33 . 20.4500 753.82 0.0000 345.93 18.6920 946.00 20.4517 756.73 14.4864 351.06 22.3389 569.70 20.4541 756.80 14.4869 351. 93 22.3531 583.19 21. 6255 884.68 15.6469 Page 3785 of 5809 ENERGY MDA COUNTS )::NERGY MDA COUNTS ENERGY MDA COUNTS 765.81 31. 3177 1274.44 10. 0352. 1620.50 4.3054 766.42 24.6121 1001.03 12.7922 1621. 92 2.1534 766.84 24.6166 1002.74 7.3137 1678.03 0.0000 772. 60 0.0000 1004.73 16.1009 1690.97 3.2781 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1. 77 50 778.90 15.7415 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 14.7939 1771.35 *2.2219 785.37 18.0371 1038.76 0.0000 1791.20 0.0000 792.07 15.8246 631. 29 8.3441 1808.65 1.1193 794.95 20.3687 1048.07 0.0000 1810.72 0.0000 795.86 16.9800 1049.04 6.4950 1836.06 4.5012 810.06 15.9363 1050.41 8.3546 810.29 15.9380 1063.66 15.8462 344.28 14.8001 1077.00 0.0000 810.76 .14.8022 1077.34 8 .*4243 815.77 0.0000 1085.87 10.3232 1048.07 0.0000 1093.63 12.2296 832.01 19.5151 1099.45 16.1551 834.85 8.0442 1112. 07 17.0277 835. 71 16.0941 1112.84 14.1925 836.80 0.0000 1115.54 10.6060 846.75 0.0000 1120.29 12.3279 846.77 20.7788 1120. 55 10.6217 856.80 0.0000 1221.41 7.5884 860.56 11. 6032 1129. 67 12.3621 871.09 12.8127 1131.51 0.0000 873.19 16.3197 1147.95 0.0000 875.33 0.0000 1173.23 9.6307 879.38 15. 7725 1177.95 11. 5723 880.51 14.9025 1189.05 8.7067 883.24 17.5494 1204.77 13.6035 884.68 14.0469 1221.41 20.5001 889.28 13.1909 1231.02 18. 5964 894.76 8. 8113 1235.36 0.0000 898.04 11. 4678 1238.28 18.6335 900.-72 13.2449 1260.41 0.0000 903.28 13.2568 1271.87 8.9072 911. 20 13.2944 1274.44 7.9229 912.08 13.2985 1274.54 7.9229 923.98 0.0000 1291.59 10.9436 926.50 8.9105 1298.22 0.0000 929 .11 10.7021 1312 .11 0.0000 937.49 9.8388 1332.49 10.0555 944.13 0.0000 1362.66 0.0000 946.00 15.2501 1365.19 1.3519 949.00 11. 6737 1368. 63 0.0000 667.71 0.0000 1384.29 4.0752 962. 31 18.9428 1408.01 8.1982 964.08 14.4414 1457.56 0.0000 966 .17 18.7872 1460.82 9.3417 911.20 18.9857 1489.16 4.1797 968. 97 18.9857 1505.03 6. 2926 983.53 0.0000 1584.12 4. 2712 984.45 0.0000 1596.21 0.0000 Page 3786 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:21:50.63 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l Background file DKAlOD: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM12.CNF;467 Background date : Z-OCT-2016 11:00:40. Sample date 30-NOV-2015 13:23:00 Acquisition date : 3-0CT-2016 09:20:08. Sample ID G405235040 Sample quantity 1.72014E+02 GRAM Detector name GAM12 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapse*d real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 4 2 4 3 0 4 2 5 2 6 0 7 0 8 0 9 0 10 0 11 2 12 2 13 0 14 4 15 4 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 5 33 5 34 0 Page 3787of5809 Energy 36.14* 37.58* 59.26 77.41* 86.98 93.16* 116. 83 154.17 185.69* 238.54* 241.43 270.09 295.02 299.82 310.07 328.27 338.20* 351.83* 433.68 463.28 510.64* 568.90 583.04* 609.35* 662.07 696. 57 7°11. 78 727.75 786.26 809.27 839.82 842.93 860.90 *BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 36 14 30 94 132 39 65 22 12 95 360 98 53 119 29 16 22 72 184 14 33 16 45 97 155 51 8 22 21 17 11 10 23 23 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 28 1.76 72.12 34 1.21 75.00 88 1.29 118.36 171 1.54 149.53 142 1.29 154.66 148 1.46 173.78 128 1.65 186.14 72 0.49 233.50 103 1.17 308.17 84 1. 20 371. 22 85 1.46 476.93 68 1.75 482.70 66 1.26 540.03 53 1.69 589.89 57 2.18 599.50 61 1.78 620.00 57 1.37 656.40 66 1.19 676.27 49 1.27 703.52 42 0.71 867.27 49 1.84 *926.47 74 1.60 1021.23 48 1. 95 1137. 78 32 1.52. 1166.07 52 1.51 1218.71 30 2.69 1324.19 33 4.22 1393.23 8 0.53 1423.66 36 0.71 1455.61 18 2.75 1572.70 4 1.67 1618.73 4 1.36 1679.87 7 2.76 1686.08 19 2.12 1722.04 68 68 116 144 144 171 182 230 305 367 470 470 535 585 585 612 649 670 698 859 919 1017 1131 1159 1210 1317 1382 1420 1449 1564 1615 1678 1678 1718 16 1.00E-02 43.6 3.61E+OO 16 3.75E-03109.4 7 8.19E-03 55.7 16 2.62E-02 27.3 5.56E-01 16 3.66E-02 18.5 7 1. 07E-02 54. 6 9 1.80E-02 37.2 6 6.07E-03 65.4 7 3.27E-03146.6 10 2.65E-02 21.6 22 1.00E-01 7.1 2.19E+OO 22 2.72E-02 25.9 10 1.47E-02 32.2 21 3.32E-02 14.6 2.17E+00 21 8.17E-03 60.5 11 4.53E..:.03 95.6 9 6.12E-03 57.5 11 2.0lE-02 25.2 11 5.12E-02 10.6 12 3.97E-03 94.3 13 9.25E-03 46.6 14 4.51E-03126.1 16 l.25E-02 37.5 14 2.69E-02 16.2 15 4.32E-02 13.1 12 1.41E-02 25.8 15 2.34E-03153.4 10 6.07E-03 31.9 11 5.96E-03 58.1 12 4.82E-03 54.4 7 2.92E-03 42.7 14 2.70E-03 38.5 5.98E-01 14 6.43E-03 32.8 9 6.49E-03 38.8 Peak Search Report (continued) Page.: 2 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911.13* 78 7 2.06 1822.57 1817 13 2.15E-02 13.7 36 0 918.40 6 4 0.49 1837.13 1833 6 l.54E-03 73.7 37 0 934.87 23 8 2.45 1870.07 1864 12 6.45E-03 32.8 38 0 954.97 9 6 l. 47 1910.29 1903 11 2.36E:-03 63.5 39 0 969. 92 36 33 l. 09 1940.23 1931 12 l. OlE-02 35.5 40. 0 1099.51 7 20 4.47 2199.60 2189 12 l. 94E-03142 .1 41 0 1120.28 42 21 l. 75 2241.15 2234 14 l.17E-02 27.8 42 0 1185. 40 12 6 2.75 2371. 50 2365 12 3.33E-03 50.0 43 0 1238.67 26 6 0.74 2478.13 2474 10 7.35E-03 26.9 44 0 1242.98 7 2 0.62 2486.77 2484 6 2.04E-03 45.7 45 0 1255.12 11 24 3.73 2511.07 2499 18 3.08E-03112.8 46 0 1321. 66 10 2 2 .11 2644.27 2638 10 2.78E-03 42.7 47 0 1325.88 7 0 0.58 2652: 71 2650 6 l.94E-03 37.8 48 0 1337.19 8 2 0.69 2675.36 2672 6 2.08E-03 44.7 49 0 1340.06 6 3 0.52 2681.10 2678 6 l. 60E-03 63.6 50 0 1460.76 350 0 2.12 2922.75 2916 14 9.72E-02 5.3 51 0 1589.14 10 3 3.47 3179.79 3173 13 2.67E-03 50.5 52 0 1764.76 16 9 4.12 3531. 46 3525 12 4.49E-03 44.6 Flag: "*" = Peak area was modified by background subtraction Page 3788of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:21:52 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 13:23:00 G405235040 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:20:08 172.01 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA12 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3789of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ' ------------------Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08* Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.082E+OO l.295E+Ol 1.295E+Ol 10.69 OK C0-58 810.76 99 . .45* 1. 744E+OO 2.810E-02 5.708E-01 85.45 OK CD-109 88.03 3.70* 4.287E+OO 6.705E-01 1.065E+OO 242.14 OK SN-126 64.28 9.60 2.033E+OO Line Not Found Absent 86.94 8.90 4.287E+OO 2.788E-01 2.788E-01 242.14 OK 87.57 37.00* 4.287E+OO 6.705E-02 6.705E-02 242.14 OK BA-137M 661.66 89.90* 2.040E+OO l.320E-01 l.345E-01 51. 51 OK CS-137 661.66 85.10* 2.040E+OO l.394E-01 l.421E-01 51. 51 OK PR-144 696. 51 1.34* 1. 960E+OO 1.521E+00 3.217E+OO 306.78 OK 1489.16 0.28 *1.064E+OO Line Not Found Absent TL-208 277.37 6.60 4.142E+OO -----Line Not Found Absent 583.19 85.00* 2.256E+OO 2. 451E-01 2. 451E-01 32.38 OK 860.56 12.50 l.662E+OO 5.180E-01 5.180E-01 77.70 OK BI-212 727. 33 6.67* l.894E+00 7.986E-01 7.986E-01 116.26 OK 785.37 1.10 1.783E+OO 4 .118E+OO 4 .118E+OO 108.79 OK 1620.50 1. 47. 9.870E-01 Line Not Found Absent PB-212 74.82 10.28 3.170E+OO l.286E+00 l.286E+OO 76.32 OK 77 .11 17 .10 3.429E+OO 1.374E+OO 1.374E+OO 37.08 OK 238.63 43.60* 4.647E+OO 9. 611E-01. 9. 611E-01 14.14 OK 300.09 3.30 3.891E+OO l.207E+OO l.207E+00 121. 08 OK BI-214 609.32 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 OK 1120. 29 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 OK PB-214 74.82 5.80 3.167E+OO Line Not Found <<INT Reject 77 .11 9.70 3.429E+OO 2.422E+OO 2.423E+OO 37.08 OK 87.09 3.41 4.296E+OO Line Not Found <<INT Reject 242.00 7.25 4.599E+00 Line Not Found <<INT Reject 295.22 18.42 3.942E+OO 8.680E-01 8.683E-01 29.19 OK 351.93 35.60* 3. 411E+OO 7.832E-01 7.835E-01 21. 24 OK RN-222 609.32 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9. 253E-01 . 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 OK RA-224 240.99 4.10* 4.607E+OO l.262E+OO 1. 2 62E+00 120.32 OK RA-226 609.32 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 OK 1764.49 15.30 9.120E-01 4.811E-01 4.813E-01 89.14 OK AC-228 105.21 1.10 5.379E+00 Line Not Found Absent 338.32 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 OK 794.95 4.25 1. 768E+OO Line Not Found Absent 835.71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1.590E+OO 8.631E-01 8. 631E-01 27.35 OK 968. 97 15.80 l.513E+OO 6.904E-01 6.904E-01 71.06 OK RA-228 105.21 1.10 5.379E+00 Line Not Found Absent 338.32 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 OK 794.95 4.25 1.768E+OO Line Not Found Absent 835.71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1.590E+OO 8. 631E-01 8.631E-01 27.35 OK 968.97 15.80 1.513E+OO 6.904E-01 6.904E-01 71. 06 OK TH-228 74.82 10.28 3.170E+OO l.286E+OO 1.286E+OO 76.32 OK Page 3790 of 5809 I Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 17.10 3.429E+OO 1.374E+OO 1. 37 4E+OO 37.08 OK 238.63 43.60* 4.647E+00 9.611E-01 9.611E-01 14.14 OK 300.09 3.30 3.891E+OO 1.207E+OO 1.207E+OO 121.08 OK TH-230 609.32 45.49* 2.179E+OO 7.560E-01 7.560E-01 26 .14 OK 1120.29 14.92 1.350E+00 9.249E-01 9.250E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4. 811E-01 89.14 OK TH-232 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 OK 835.71 1. 61 1.701E+OO Line Not Found Absent 911.20 25.80* 1.590E+OO 8.631E-01 8.631E-01 27.35 OK 968. 97 15.80 1.513E+OO' 6.904E-01 6.904E-01 71. 06 OK U-234 609.32 45.49* 2.179E+OO 7.560E-01 7.560E-01 26.14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9.250E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4.811E-01 89.14 OK AM-241 59.54 35.90* 1.495E+OO 3.456E-01 3.461E-01 lJ,1. 43 OK AM-243 43.53 5.90 2.347E-01 Line Not Found Absent 74.66 67. 20*' 3.170E+OO 1. 968E-01 1. 968E-01 76.32 OK ANH-511 511. 00 100.00* 2.510E+OO 3.192E-02 3.192E-02 252.30 OK Flag: "*" = Keyline Page 3791of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:21:54.56. *********************************.**********************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l *
Acquisition date 3-0CT-2016 09:20:08 Sensitivity : 3.000 *
Detector ID GAM12 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 30-NOV-2015 13:23:00 Analyst initials: MXRl * *Sample ID G405235040 Sample Quantity 1.7201E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN * * .Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;13
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 295E+Ol 1.356E+OO C0-58 5.708E-01 4.780E-01 CD-109 l.065E+OO 2.527E+OO SN-126 6.705E-02 1.591E-01 BA-137M 1.345E-01 6.791E-02 CS-137 l.421E-01 7.174E-02 PR-144 3.217E+OO 9.670E+OO TL-208 2.451E-01 7.777E-02 BI-212 7.986E-01 9.099E-01 PB-212 9. 611E-01 l.332E-01 BI-214 7.563E-01 1.938E-01 PB-214 7.835E-01 l.631E-01 RN-222 7.563E-01 l.938E-01 RA-224 1. 2 62E+OO 1.488E+OO RA-226 7.563E-01 l.938E-01 AC-228 8.631E-01 2. 313E-01 RA-228 8.631E-01 2. 313E-01 TH-228 9. 611E-01 l.332E-01 TH-230 7.560E-01 l.937E-01 TH-232 8.631E-01 2.313E-01 U-234 7.560E-01 l.937E-01 AM-241 3.461E-01 3.779E-01 AM-243 1. 968E-01 1.472E-01 ANH-511 3.192E-02 7.892E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3792 of 5809 Key-Line Activity K.L. Cnt Uncert (pCi/GRAM ). (1.96-sigma) -5.510E+OO -2.605E-02 0.000E+OO 3.655E-03 -1. 997E_:._01 O.OOOE+OO 1 .. 165E+Ol 3.679E-02 1. 960E+41 2.971E-02 3.379E-01 1. 728E+04 MDA (pCi/GRAM 4.622E-01 1. 071E+OO 2.870E+OO 1.822E-01 5.994E-02 6.332E-02 6.447E+OO *5. 007E-02 8.785E-01 8.824E-02 1. 300E-01 l.070E-01 1.300E-01 9.454E-01 l.300E-01 2.020E-01 2.020E-01 8.824E-02 1.300E-01 2.020E-01 1.300E-01 3.665E-01 1.090E-01 4.917E-02 MDA (pCi/GRAM 2.120E+Ol 6.434E-02 O.OOOE+OO 6.474E-02 6.293E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.942E+02 O.OOOE+OO SHORT HLIF MN-54 1.118E-02 5.682E-02 l.186E-01 NOT IDENT. C0-56 l.057E-01 3.900E-01 7.747E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 l.864E-02 4.421E-02 9.225E-02 NOT IDENT. FE-59 4.862E+OO 1.355E+Ol 1.477E+Ol FAIL ABUN C0-60 -8.745E-03 3.492E-02 5.893E-02 NOT IDENT. ZN-65 2.053E-02 1. 586E-01 2.936E-01 NOT IDENT. GE-68 2.099E-01 2.160E+00 4.428E+OO NOT IDENT. AS-73 -1.083E+Ol l.604E+Ol 2.876E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.006E+03 O.OOOE+OO SHORT HLIF SE-75 -l.393E-02 1.958E-01 3.654E-01 NOT IDENT. BR-77 O.OOOE+OO 2.472E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.126E+02 0.000E+OO SHORT HLIF RB-83 2.144E-02 6.767E-01 1. 306E+OO NOT IDENT. KR-85 1. 67 5E+OO 7.881E+OO l.376E+Ol NOT IDENT. SR-'85 1. 917E-01 9.057E-01 l.582E+OO NOT IDENT. RB-86 O.OOOE+OO 3.628E+04 O.OOOE+OO SHORT HLIF Y-88 l.230E-01 2.291E-01 5.435E-01 NOT IDENT. Y-91 2.977E+02 5.810E+02 1.223E+03 NOT IDENT. NB-94 8.461E-03 2.810E-02 5.607E-02 NOT IDENT. NB-95 -8.984E-02 8.139E-01 1.628E+OO NOT IDENT.
NB-95M 2.774E+OO 2.690E+OO 5.176E+OO NOT IDENT. ZR-95 7.492E-02 1.627E+OO 3.085E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 047E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 208E+33 O.OOOE+OO SHORT HLIF TC-99M 0.000E+OO l.960E+41 0. OOOE+OO . SHORT HLIF RH-101 2.038E-02 3.455E-02 7.177E-02 NOT IDENT. RH-102 9.662E-03 5. 963E-02 1.160E-01 FAIL ABUN RU-103 6.176E+OO 5.541E+OO 1.240E+Ol FAIL ABUN RH-106 2.252E-02 4. 572E-01 8.870E-01 NOT IDENT. RU-106 2.252E-02 4. 572E-01 8.870E-01 NOT IDENT. AG-108M 2.777E-02 5.133E-02 4.782E-02 FAIL ABUN AG-110M 4.762E-02 8. 962E-02 1. 969E-01 NOT IDENT. SN-113 9.502E-02 2.388E-01 4.793E-01 NOT IDENT. CD-115 O.OOOE+OO 3.192E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.465E+05 O.OOOE+OO SHORT HLIF TE-123M -5.088E-02 l.299E-01 2.518E-01 NOT IDENT. SB-124 -7.465E-01 1.909E+OO 3.633E+OO NOT IDENT. SB-125 -1.222E-01 l .133E-01 1.596E-01 FAIL ABUN TE-125M 2.179E+02 2.902E+02 6.187E+02 NOT IDENT. I-126 O.OOOE+OO 1.308E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.839E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.591E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.512E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.949E+27 O.OOOE+OO SHORT HLIF BA-133 2.374E-03 3.724E-02 6.607E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.00lE-02 4.828E-02 1.085E-01 FAIL ABUN CS-135 1.438E-01 l.335E-01 2.646E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.275E+05 O.OOOE+OO SHORT HLIF CE-139 4.305E-02 9.510E-02 1.973E-01 NOT IDENT. BA-140 O.OOOE+OO l.594E+06 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 5.716E+05 O.OOOE+OO SHORT HLIF CE-141 -1.054E+Ol 2.674E+Ol 5.208E+Ol NOT IDENT. CE-143 O.OOOE+OO 7.831E+40 O.OOOE+OO SHORT HLIF CE-144 -1.168E-01 3.322E-01 6.532E-01 NOT IDENT. PM-144 3.688E-02 l.109E-01 9.315E-02 FAIL ABUN PM-146 4.302E-03 4.119E-02 8.055E-02 NOT IDENT. ND-147 O.OOOE+OO 4.816E+07 O.OOOE+OO SHORT HLIF PM-147 8.258E+02 7.543E+02 1. 643E+03 NOT IDENT. PM-149 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF EU-150 l.016E-02 2.381E-02 4.419E-02 FAIL ABUN EU-152 -2.983E-02 S.740E-02 1.638E-01 FAIL ABUN GD-1.53 2.578E-02 1.825E-01 3.424E-01 NOT IDENT. EU-154 -5. 921E-02 9.084E-02 1. 613E-01 NOT IDENT. EU-155 l.112E-02 1.031E-01 2 .119E-Ol FAIL ABUN TB-160 1. 228E+OO 1.583E+OO 3.665E+OO FAIL ABUN H0-166M 9.904E-02 6.199E-02 l.134E-01 FAIL ABUN TM-171 -3.224E+00 3.515E+Ol 6.700E+Ol NOT IDENT. HF-172 7.206E-02 2.255E-01 4.634E-01 NOT IDENT. LU-172 -3.215E-03 l.013E-01 1. 734E-01 FAIL ABUN LU-176 -6.254E-03 2.198E-02 3.717E-02 FAIL ABUN HF-181 2.035E+00 4.611E+OO 9.390E+OO NOT IDENT. TA-182 -4.575E-01 7.802E-01 1. 409E+OO FAIL ABUN Page 3793of5809 RE-183 7.625E+OO 8.327E+OO 9.525E+OO FAIL ABUN RE-184 5.040E+OO 3.152E+Ol 6.557E+Ol NOT IDENT. W-188 1. 599E+Ol 1.208E+02 2.149E+02 NOT IDENT. IR-192 2.863E-02 4.810E-01 9.154E-01 FAIL ABUN HG-203 1. 581E+OO 2.532E+OO 5.203E+OO NOT IDENT. BI-207 l.108E-02 3.946E-02 8.433E-02 FAIL ABUN PB-210 4.707E+OO 6.881E+OO 1.394E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.493E-01 7.265E-01 FAIL ABUN PB-211 3.784E-01 6.576E-01 1.340E+OO NOT IDENT. RN-219 , 3. 760E.:...01 7.153E-01 FAIL ABUN RA-223 -1.179E-01 5.697E-Ol 9.681E-01 FAIL ABUN AC-227 8.106E-02 2.059E-01 4.180E-01 FAIL ABUN TH-227 8.106E-02 2.059E-01 4.180E-01 FAIL ABUN TH-229 3.593E-01 4.398E-01 9.166E-01 FAIL ABUN PA-231 4.441E-01 4.183E-01 8.293E-01 NOT IDENT. TH-231 -1.179E-01 5.697E-01 9. 681E-01 FAIL ABUN PA-233 4.532E-03 5. 972E-02 1.055E-01 FAIL ABUN PA-234 7.769E-02 2.107E-01 4.636E-01 FAIL ABUN PA-234M -9.195E-01 4.037E+OO 7.943E+OO NOT IDENT. TH-234 1.104E+OO 1.816E+OO 3.602E+OO FAIL ABUN U-235 -6.166E-02 1.672E-01 3.288E-01 FAIL ABUN NP-237 4.532E-03 5.972E-02 l.055E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 l.104E+OO 1.816E+OO 3.602E+OO FAIL ABUN NP-239 2.808E-01 3.602E-01 4.731E-01 FAIL ABUN PU-239 1.204E+Ol 3.104E+02 6.240E+02 NOT IDENT. CM-243 .-3. 044E-02 9.247E-02 1.849E-01 NOT IDENT . BK-247 . 1. 772E-02 6.728E-02 1. 231E-01 NOT IDENT. CM-247 -5.995E-03 3.520E-02 6.644E-02 NOT IDENT. CF-249 9.005E-04 3.234E-02 6.331E-02 NOT IDENT. CF-251 -1. 44 7E-02 9. 716E-02 1.917E-01 NOT IPENT. Page 3794of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:21:51.43 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM -%Error K-40 1460.82 342 10.66* 1.082E+OO l.295E+Ol 1.295E+Ol 10.69 C0-58 810.76 11 99.45* 1. 744E+OO 2.810E-02 5.708E-01 85.45 CD-109 88.03 53 3.70* 4.287E+OO 1.470E+OO 2.335E+OO 109.26 SN-126 64.28 ------9.60 2.033E+OO ------Line Not Found ------86.94 53 8.90 4.287E+OO 6 .113E-01 6 .113E-01 109.26 87.57 53 37.00* 4.287E+OO 1.470E-01 l.470E-01 109.26 BA-137M 661. 66 55 89.90* 2.040E+OO l.320E-01 1.345E-01 51. 51 CS-137 661. 66 55 85.10* 2.040E+OO 1.394E-01 1.421E-01 51. 51 PR-144 696. 51 9 1.34* 1. 960E+OO 1.521E+OO 3.217E+OO 306.78 1489.16 ------0.28 1.064E+OO ------Line Not Found ------TL-208 277.37 ------6.60 4.142E+OO ------Line Not Found ------583.19 108 85.00* 2.256E+OO 2. 451E-01 2. 451E-01 32.38 860.56 25 12.50 1.662E+OO 5.180E-01 5.180E-01 77.70 BI-211 72.87 ------1. 23 2. 964E+OO ------Line Not Found ------351. 06 218 12.92* 3. 411E+OO 2.158E+OO 2.158E+OO 21. 24 BI-212 727. 33 23 6.67* 1.894E+OO 7.986E-01 7.986E-01 116.26 785.37 19 1.10 1.783E+OO 4 .118E+OO 4 .118E+OO 108.79 1620.50 ------1. 47 9.870E-01 ------Line Not Found ------PB-212 74.82 133 10.28 3.170E+OO 1. 776E+OO 1.776E+OO 54.69 77 .11 185 17.10 3.429E+OO 1.374E+OO 1.374E+OO 37.08 238.63 446 43.60* 4.647E+OO 9.611E-01 9. 611E-01 14.14 300.09 35 3.30 3.891E+OO 1.207E+OO 1.207E+OO 121.08 BI-214 609.32 172 45.49* 2.179E+OO 7.560E-01 7.563E-01 26 .14 1120.29 43 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 1764.49 15 15.30 9.120E-01 4.811E-01 4.813E-01 89.14 PB-214 74.82 133 5.80 3.170E+OO 3.148E+OO 3.149E+OO 54.69 77 .11 185 9.70 3.429E+OO 2.422E+OO 2.423E+OO 37.08 87.09 53 3.41 4.287E+OO 1. 596E+OO 1. 596E+OO 109.26 242*. 00 121 7.25 4.607E+OO 1.582E+OO 1.582E+OO 51. 87 295.22 144 18.42 3.942E+OO 8.680E-01 8.683E-01 29.19 351.93 218 35.60* 3. 411E+OO 7.832E-01 7.835E-01 21. 24 RN-222 609.32 172 45.49* 2.179E+00 7.560E-01 7.563E-01 26 .14 1120.29 43 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 1764.49 15 15.30 9 .120E...,01 4. 811E-01 4.813E-01 89.14 RA-224 240.99 121 4.10* 4.607E+OO 2.797E+OO 2.797E+OO 5r. 87 RA-226 609.32 172 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 1120. 29 43 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 1764.49 15 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 AC-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 86 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 794.95 ------4.25 1. 768E+OO ------Line Not Found ------835.71 ------1. 61 1. 701E+OO ------Line Not Found ------911.20 81 25.80* 1.590E+OO 8. 631E-01 8. 631E-01 27.35 968. 97 38 15.80 1. 513E+OO 6.904E-01 6.904E-01 71. 06 RA-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 86 11.27 3.525E+OO 9.430E-01 9.430E-01 50.35 794.95 ------4.25 1. 768E+OO ------Line Not Found ------Page 3795of5809 Nuclide Line Activity Report *(continued) Page : 2 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff . pCi/GRAM pCi7GRAM *%Error 835.71 ------1. 61 1.701E+OO ------Line Not Found ------911.20 81 25.80* 1.590E+OO 8.631E-01 8.631E-01 27.35 968. 97 38 15.80 1. 513E+OO 6.904E-01 6.904E-01 71. 06 TH-228 74.82 133 10.28 3.170E+OO 1. 776E+OO 1. 776E+OO 54.69 77 .11 185 17.10 3.429E+OO 1.374E+OO 1.374E+OO 37.08 238.63 446 43.60* 4.647E+OO 9. 611E-01 9. 611E-01 14.14 300.09 35 3.30 3.891E+OO 1.207E+OO 1.207E+OO 121. 08 TH-230 609.32 172 45.49* 2.179E+OO 7.560E-01 7.560E-01 26.i4 1120.29 43 14.92 1.350E+OO 9.249E-01 9.250E-01 55.63 1764.49 15 15.30 9.120E-01 4.811E-01 4.811E-01 89.14 TH-232 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 86 11. 27 3.525E+00 9.430E-01 9.430E-01 50.35 835. 71 ------1. 61 1. 701E+OO ------Line Not Found ------911. 20 81 25.80* 1.590E+OO 8.631E-01 8.631E-01 27.35 968. 97 38 15.80 1.513E+OO 6.904E-01 6.904E-01 71. 06 U-234 609.32 172 45.49* 2.179E+OO 7.560E-01 7.560E-01 26.14 1120.29 43 14.92 l.350E+00 9.249E-01 9.250E-01 55.63 1764.49 15 15.30 9.120E-01 4.BllE-01 4. 811E-01 89.14 AM-241 59.54 42 35.90* 1.495E+OO 3.456E-01 3.461E-01 111. 43 AM-243 43.53 ------5.90 2.347E-01 ------Line Not Found ------74.66 133 67.20* 3.170E+OO 2.717E-01 2.717E-01 54.69 ANH-511 511. 00 18 100.00* 2 .*510E+OO 3.192E-02 3.192E-02 252.30 Flag: "*" Key line Page 3796 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Total number of lines in spectrum 52 Number of unidentified lines 15 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 PR-144 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226* AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-241 AM-243 ANH-511 Hlife l.25E+09Y 70.86D 461.40D 2.30E+05Y 30.08Y 30.08Y 284.910 l.41E+l0Y 7.04E+08Y l.41E+10Y l.41E+l0Y 1600.00Y 1600. ODY 1600. DOY 1.41E+10Y 1600. OOY 1.41E+10Y 1.41E+l0Y l.41E+l0Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 432.60Y 7370.00Y 1.00E+09Y Decay 1. 00 20.3 1. 59 1. 00 1. 02 1. 02 2 .11 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.295E+Ol 2.810E-02 1.470E+OO 1.470E-01 l.320E-01 1.394E-01 1.521E+OO 2. 451E-01 2.158E+OO 7.986E-01 9.611E-01 7.560E-01 7.832E-01 7.560E-01 2.797E+OO 7.560E-01 8.631E-01 8.631E-01 9.611E-01 7.560E-01 8.631E-01 7.560E-01 3.456E-01 2.717E-01 3.192E-02 3.211E+Ol 3.211E+Ol Decay Corr pCi/GRAM l.295E+Ol 5.708E-01 2.335E+OO 1.470E-01 l.345E-01 l.421E-01 3.217E+OO 2. 451E-01 2.158E+OO 7.986E-01 9.611E-01 7.563E-01 7.835E-01 7.563E-01 2.797E+OO 7.563E-01 8. 631E-01 8.631E-01 9. 611E-01 7.560E-01 8. 631E-01 7.560E-01 3.461E-01 2. 717E-01 3.192E-02 3.522E+Ol 3.522E+Ol 71.15% Decay Corr 2-Sigma Error 0.138E+Ol 4.877E-01 2 .. 551E+OO l.607E-01 0.693E-01 0.732E-01 9.868E+OO 0.794E-01 0.458E+OO 9.285E-01 1.359E-01 1.977E-01 1.664E-01 l.977E-01 1.451E+OO l.977E-01 2.361E-01 .2. 361E-01 l.359E-01 1. 97 6E-01 2. 361E-01 1.976E-01 3.856E-01 1. 486E-01 8.053E-02 "M" Manually accepted 2-Sigma %Error 10.69 85.45 109.26 109.26 51. 51 51.51 306.78 32.38 21. 24 116.26 14.14 26.14 21.24 26.14 51. 87 '2 6. *14 27.35 27.35 14.14 26.14 27.35 26.14 111. 43 54.69 252.30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3797 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 36.14 55 42 1. 76 72 .12 68 16 1. OOE-02 87.2 2.66E-02 4 37.58 20 51 1. 21 75.00 68 16 3.75E-03 **** 4.73E-02 0 93.16 89 175 1. 65 186.14 182 9 1. 80E-02 74.4 4.74E+OO T 0 116. 83 29 97 0.49 233.50 230 6 6.07E-03 **** 5.74E+OO T 0 154.17 15 134 1.17 308 .*17 305 7 3.27E-03 **** 5.86E+OO T 0 185.69 122 107 1. 20 371.22 367 10 2.65E-02 43.2 5.45E+OO T 0 270.09 64 81 1. 26 540.03 535 10 1. 4 7E-02 64.3 4.23E+OO T 0 310.07 20 73 1. 78 620.00 612 11 4.53E-03 **** 3.79E+OO 0 328.27 26 68 1. 37 656.40 649 9 6.12E-03 **** 3.61E+OO T 0 433.68 16 48 0. 71 867.27 859 12 3.97E-03 **** 2.87E+OO T 0 463.28 38 56 1. 84 926.47 919 13 9.25E-03 93.2 2.72E+OO T 0 568.90 50 53 1. 95 1137. 78 1131 16 l.25E-02 75.0 2.30E+OO T 0 711.78 24 9 0.53 1423.66 1420 10 6.07E-03 63.9 1. 93E+OO T 5 839.82 10 4 1. 36 1679.87 1678 14 2.70E-03 76.9 1. 69E+OO 5 842.93 24 8 2.76 1686.08 1678 14 6.43E-03 65.7 l.69E+00 0 918.40 6 5 0.49 1837 .13 1833 6 1.54E-03 **** 1.58E+OO 0 934.87 24 8 2 .45 1870.07 1864 12 6.45E-03 65.6 l.56E+OO 0 954.97 9 6 1. 47 1910.29 1903 11 2.36E-03 **** 1. 53E+OO T 0 1099.51 7 20 4.47 2199.60 2189 12 1.94E-03 **** 1. 37E+OO T 0 1185.40 12 6 2.75 2371.50 2365 12 3. 33E-03* **** l.29E+OO 0 1238.67 27 6 o.74 2478.13 2474 10 7.35E-03 53.8 1.24E+OO T 0 1242.98 7 2 0.62 2486.77 2484 6 2.04E-03 91. 5 l .'24E+OO 0 1255.12 11 24 3.73 2511. 07 2499 18 3.08E-03 **** 1.23E+OO 0 1321. 66 10 2 2 .11 2644.27 2638 10 2.78E-03 85.4 l.18E+OO 0 1325.88 7 0 0.58 2652.71 2650 6 l.94E-03 75.6 l.18E+OO 0 1337.19 7 1 0.69 2675.36 2672 6 2.08E-03 89.4 l.17E+OO 0 1340.06 6 3 0.52 2681.10 2678 6 l.60E-03 **** l.17E+00 0 1589.14 9 3 3.47 3179.79 3173 13 2.67E-03 **** 1. OOE+OO Flags: "T" = Tentatively associated Page 3798of5809.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:22:08.76 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l *
Acquisition date 3-0CT-2016 09:20:08 Sensitivity : 3.000 *
Detector ID GAM12 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real. time: 0 01:00:00.56 Half life ratio *
Sample date 30-NOV-2015 13:23:00 Nuclide Library : SOLID *
Sample ID G405235040 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : l.7201E+02 GRAM * **Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN *
File : DKAlOO: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
Combined Critical Level Report NOTE: Not "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 PR-144 TL-208 BI-212 PB....:212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-241 AM-243 ANH-511 Le (pCi/GRAM 1. 792E-01 4.640E-01 l.371E+OO 8.705E-02 2.656E-02 2.806E-02 2.730E+OO 2.182E-02 3.909E-01 4.lOOE-02 5. 881E-02 ' 4. 833E-02 5. 881E-02 4.393E-01 5. 881E-02 8.619E-02 8.619E-02 4.lOOE-02 5.878E-02 8.619E-02 5.878E-02 l.712E-01 5.140E-02 2.212E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3799of5809 Le (pCi/GRAM 9.365E+OO 2.598E-02 O.OOOE+OO 2.569E-02 2.667E-01 O.OOOE+OO 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65
GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-l02 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-°152 GD-153 EU-154 Eu...:.155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3800 of 5809 5.220E-02 3.300E-01 0.000E+OO 4.330E-02 . 6. 444E+OO 2.374E-02 l.257E-01 l.918E+OO l.339E+Ol O.OOOE+OO 1. 679E-01 O.OOOE+OO O.OOOE+OO 5.868E-Ol 6.280E+OO 7.216E-01 O.OOOE+OO 2.214E-01 5.420E+02 2.489E-02 7.199E-01 2.436E+OO l.371E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.397E-02 5.193E-02 5.591E+OO 3.922E-01 3.922E-01 2 .151E-02 8.636E-02 2.200E-01 O.OOOE+OO 0.000E+OO l.180E-01 1. 360E+OO 7.090E-02 2.915E+02 O.OOOE+OO O.OOOE-f-00 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.988E-02 O.OOOE+OO 4.890E-02 1. 231E-01 O.OOOE+OO O.OOOE+OO 9.208E-02 O .. OOOE+OO O.OOOE+OO 2.445E+Ol O.OOOE+OO 3.060E-01 4.092E-02 3.643E-02 O.OOOE+OO 7.730E+02 O.OOOE+OO 2.023E-02 7.484E-02 l.603E-01 6.553E-02 9.952E-02. 1. 596E+OO 5.083E-02 3.121E+Ol 2.185E-01 7.721E-02 1. 683E-02 4.246E+OO 5.903E-01 4.465E+00 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT . FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT.IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF ,SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. *FAIL ABUN FAIL ABUN RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3801of5809 2.865E+Ol 9.913E+Ol 4.210E-Ol 2.419E+OO 3.631E-02 6.569E+OO 3.492E-01 6.160E-Ol 3.268E-01 4.410E-01 1.939E--,Ol 1. 939E-01 4.313E-01 3.844E-01 4.410E-01 4.842E-02 1.990E-01 3.484E+OO 1. 709E+OO l.546E-01 4.842E-02 O.OOOE+OO 1. 709E+OO 2.224E-01 2.948E+02 8.650E-02 5.663E-02 3.039E-02 2.865E-02 8.923E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL Ai3UN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:22:16.21 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l * *Acquisition date 3-0CT-2016 09:20:08 Sensitivity : 3.000 *
Detector ID GAM12 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 30-NOV-2015 13:23:00 Nuclide Library : SOLID *
Sample ID G405235040 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7201E+02 GRAM *
Quantity Err(%) : 1.1627E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 11:41:01 Eff. Geometry : CAN . *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 C0-58 CD-109 SN-126 BA-137M CS-137 PR-144 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224. RA-226 'AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-241 AM-243 ANH-511 1.295E+Ol 5.708E-01 1. 065E+OO 6.705E-02 l.345E-01 1. 421E-01 3.217E+OO 2.451E-01 7.986E-01 9. 611E-01 7.563E-01 7.835E-01 7.563E-01 1.262E+OO 7.563E-01 8. 631E-01 8. 631E-01 9. 611E-01 7.560E-01 8. 631E-01 7.560E-01 3.461E-01 l.968E-01 3.192E-02 Act Error ( 1. 96-sigma) 1. 517E+OO 4.786E-01 2.533E+OO l.595E-01 6 .. 816E-02 7.201E-02 9.671E+OO 7.848E-02 9.109E-01 l.429E-01 1. 965E-01 1. 665E-01 1. 965E-01 1. 493E+OO 1. 965E-01 2.355E-01 2.355E-01 1. 429E-01 1. 964E-01 2.355E-01 1. 964E-01 3.788E-01 l.480E-01 7.893E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3802 of 5809 Key-Line Activity (pCi/GRAM -5.510E+OO -2.605E-02 1.000E+41 3.655E-03 -1.997E-01 -1.061E+04 K.L Act error (1.96-sigma) l.166E+Ol 3.680E-02 3.840E+41 2.971E-02 3.380E-01 1.728E+04 TPU ( 1. 96-sigma) l.517E+00 4.786E-01 2.533E+OO .1.595E-01 6.816E-02 7.201E-02 9.671E+OO 7.848E-02 9.109E-01 l.429E-01 1. 965E-01 l.665E-01 1. 965E-01 1.493E+OO 1. 965E-01 2.355E-01 2.355E-01 1.429E-01 1. 964E-01 2.355E-01 1. 964E-01 3.788E-01 1. 480E-01 7.893E-02 TPU ( 1. 96-signi.a) l.192E+Ol 3.863E-02 O.OOOE+OO 2.975E-02 3.498E-01 1. 793E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -9.408E+Ol 4.942E+02 4.960E+02 SHORT HLIF' MN-54 l .118E-02 5.683E-02 5.705E-02 NOT IDENT. C0-56 l.057E-01 3.901E-01 3.929E-01 FAIL ABUN MN-56 1. 000E+41 3.691E+41 0.000E+OO SHORT HLIF C0-57 l.864E-02 4.422E-02 4.501E-02 NOT IDENT. FE-59 4.862E+OO l.355E+Ol l.373E+Ol FAIL ABUN C0-60 -8.745E-03 3.492E-02 3.514E-02 NOT IDENT. ZN-65 2.053E-02 1. 58 6E-01 1. 588E-01 NOT IDENT. GE-68 2.099E-01 2.160E+OO 2.162E+OO NOT IDE0NT. AS-73 -1.083E+Ol 1.619E+Ol l.691E+Ol NOT IDENT. AS-74 l.824E+02 7.006E+03 7.006E+03 SHORT HLIF SE-75 -1.393E-02 1.958E-01 1.959E-01 NOT IDENT. BR-77 1. 784E+39 l.585E+40 O.OOOE+OO SHORT HLIF SR-82 6.831E+02 8.132E+02 8. 696E+02 SHORT HLIF RB-83 2.144E-02 6.767E-01 6.768E-01 NOT IDENT. KR-85 l.675E+OO 7.881E+OO 7.918E+OO NOT IDENT. SR-85 1.917E-01 9.057E-01 9.099E-01 NOT IDENT. RB-86 l.561E+03 3.628E+04 3.628E+04 SHORT HLIF Y-88 l.230E-01 2.292E-01 2.359E-01 NOT IDENT. Y-91 2.977E+02 5.811E+02 5. 964E+02 NOT IDENT. NB-94 8.461E-03 2.810E-02 2.836E-02 NOT IDENT. NB-95 -8.984E-02 8.139E-01 8.149E-01 NOT IDENT. NB-95M 2.774E+OO 2.699E+OO 2.975E+OO NOT IDENT. ZR-95 7.492E-02 1.627E+OO l.627E+OO NOT IDENT. NB-97 1. OOOE+41 9.049E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.048E+41 0.000E+OO SHORT HLIF M0-99 6.152E+31 1.208E+33 O.OOOE+OO SHORT HLIF TC-99M -l:OOOE+41 7.838E+41 O.OOOE+OO SHORT HLIF RH-101 2.038E-02 3.475E-02 3.594E-02 NOT IDENT. RH-102 9.662E-03 5. 964E-02 5.980E-02 FAIL ABUN RU-103 6.176E+OO 5.549E+OO 6.208E+OO FAIL'ABUN RH-106 2.252E_:_02 4.572E-01 4.573E-01 NOT IDENT. RU-106 2.252E-02 4.572E-01 4.573E-01 NOT IDENT. AG-108M 2.777E-02 5.134E-02 5.284E-02 FAIL ABUN AG-llOM 4.762E-02 8. 965E-02 9.218E-02 NOT IDENT. SN-113 9.502E-02 2.388E-01 2.426E-01 NOT IDENT. CD-ll5 -2.288E+40 3.220E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -9.273E+04 l.469E+05 l.527E+05 SHORT HLIF TE-123M -5.088E-02 l.299E-01 l.319E-01 NOT IDENT. SB-124 -7.465E-01 l.910E+OO l.939E+OO NOT IDENT. SB-125 -l.222E-01 l.134E-01 l.261E-01 FAIL ABUN TE-125M 2.179E+02 2.904E+02 3.066E+02 NOT IDENT. I-126 2.075E+05 l.308E+06 1.311E+06 SHORT HLIF SB-126 -5.838E+05 l.842E+06 l.861E+06 SHORT HLIF SB-127 6.613E+21 7.648E+22 O.OOOE+OO SHORT HLIF I-131 4.771E+09 9.515E+09 9.755E+09 SHORT HLIF I-132 l.OOOE+41 6.859E+42 0.000E+OO SHORT HLIF TE-132 l.845E+27 2.095E+27 O.OOOE+OO SHORT HLIF BA-133 2.374E-03 3. 724E-02 3. 725E-0*2 NOT IDENT. I-133 -l.OOOE+41 8.787E+42 O.OOOE+OO SHORT HLIF
CS-134 5. OOlE-02 4.833E-02 5.333E-02 FAIL ABUN cs-135 l.438E-01 l.339E-01 1.487E-01 NOT IDENT. I-135 l.OOOE+41 l.162E+42 O.OOOE+OO SHORT HLIF CS-136 -9.550E+04 4.277E+05 4.298E+05 SHORT HLIF CE-139 4.305E-02 9.550E-02 9.745E-02 NOT IDENT. BA-140 3.900E+05 l.594E+06 l.603E+06 SHORT HLIF LA-140 l.140E+05 5.716E+05 5.739E+05 SHORT HLIF CE-141 -1.054E+Ol 2.674E+Ol 2.716E+Ol NOT IDENT. CE-143 l.OOOE+41 7.901E+40 0.000E+OO SHORT HLIF CE-144 -l.168E-01 3.323E-01 3.364E-01 NOT IDENT. PM-144 3.688E-02 l.109E-01 l .121E-01 FAIL ABUN PM-146 4.302E-03 4 .119E-02 4.124E-02 NOT IDENT. ND-147 -3.261E+06 4.816E+07 4.819E+07 SHORT HLIF PM-147 8.258E+02 7.552E+02 8.420E+02 NOT IDENT. PM-149 -1.000E+41 2.688E+41 O.OOOE+OO SHORT HLIF EU-150 1.016E-02 2.381E-02 2.425E-02 FAIL ABUN EU-152 -2.983E-02 8.741E-02 8.844E-02 FAIL ABUN GD-153 2.578E-02 1.825E-01 l.829E-01 NOT IDENT. EU-154 -5. 921E-02 9.088E-02 9.471E-02 NOT IDENT. EU-155 l.ll2E-02 l.031E-01 l.033E-01 FAIL ABUN TB-160 l.228E+OO 1.585E+OO 1. 679E+OO FAIL ABUN H0-166M 9.904E-02 6.222E-02 7.658E-02 FAIL ABUN TM-171 -3.224E+OO 3.515E+Ol 3.518E+Ol NOT IDENT. HF-172 7.206E-02 2.258E-01 2.281E-01 NOT IDENT. LU-172 -3.215E-03 1.013E-01 1.013E-01 FAIL ABUN LU-176 -6.254E-03 2.198E-02 2.216E-02 FAIL ABUN HF-181 2.035E+OO 4.611E+OO 4.702E+OO NOT IDENT. TA-182 -4.575E-01 7.804E-01 8. 072E-01 FAIL ABUN Page 3803of5809 RE-183 7.625E+OO 8.414E+OO 9.089E+OO FAIL ABUN RE-184 5.040E+OO 3.154E+Ol 3.162E+Ol NOT IDENT. W-188 1.599E+Ol l.208E+02 1. 210E+02 NOT IDENT. IR-192 2.863E-02 4.810E-01 4. 811E-01 FAIL ABUN HG-203 1.581E+OO 2.533E+OO 2.632E+OO NOT IDENT. BI-207 l.108E-02 3.946E-02 3.978E-02 FAIL ABUN PB-210 4.707E+OO 6.895E+OO 7.214E+OO NOT IDENT. BI-211 2.158E+OO 4.599E-01 1.076E+OO FAIL ABUN PB-211 3.784E-01 6.579E-01 6.797E-01 NOT IDENT. RN-219 -4.178E-02 3.760E-01 3.765E-01 FAIL ABUN RA-223 -1.179E-01 5.698E-01 5.722E-01 FAIL ABUN AC-227 8.106E-02 2.062E-01 2.094E-01 FAIL ABUN TH-227 8.106E-02 2.062E-01 2.094E-01 FAIL ABUN TH-229 3.593E-01 4.401E-01 4.690E-01 FAIL ABUN PA-231 4. 441E-01 4.289E-01 4.733E-01 NOT IDENT. TH-231 -1.179E-01 5.698E-01 5. 722E-01 FAIL ABUN PA-233 4.532E-03 5.972E-02 5.975E-02 FAIL ABUN PA-234 7.769E-02 2.287E-01 2.314E-01 FAIL ABUN PA-234M -9.195E-01 4.037E+OO 4.059E+00 NOT IDENT. TH-234 1.104E+OO 1. 833E+OO 1.899E+OO FAIL ABUN *u-235 -6.166E-02 l.673E-01 1. 696E-01 FAIL ABUN NP-237 4.532E-03 5. 972E-02 5.975E-02 FAIL ABUN NP-238 -l.000E+41 2.125E+41 O.OOOE+OO SHORT HLIF U-238 1.104E+OO 1.833E+OO 1.899E+OO FAIL ABUN NP-239 2.808E-01 3.609E-01 3.825E-01 FAIL ABUN PU-239 1.204E+Ol 3.104E+02 3.105E+02 NOT IDENT. C:M-243 -3.044E-02 9. 251E-02 9.352E-02 NOT IDENT. BK-247 1.772E-02 6.738E-02 6.785E-02 NOT .IDENT. CM-247 -5.995E-03 3.521E-02 3. 531E-02 NOT IDENT. CF-249 9.00SE-04 3.234E-02 3.234E-02 NOT IDENT. CF-251 -1.447E-02 9.717E-02 9.739E-02 NOT IDENT. Page 3804 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS *ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 51.9531 87.09 132.1236 136.47 66.4241 45.60 85.5104 87.57 153.2205 140.51 0.0000 46.54 70.9532 88.03 153.2949 143.76 82.1577 49. 72 0.0000 88.34 142.6056 144.24 70.4471 51. 35 72.6906 88.47 142. 6250* 145.44 88.5932 51. 87 73.9776 89. 96 136.8226 152.43 74.9796 52.39 61.6936 1093.63 136.9188 153.25 0.0000 52.97 70.3883 91.11 0.0000 323.87 88.2753 53.44 75.3776 92.59 103. 5413 156.02 0.0000 54.07 80.3913 93.35 103.6212 158.56 0.0000 57.36 0.0000 94.56 67.4359 159.00 84.9359 57.53 76.2164 94.65 67.4423 162.33 76.9026 57.98 81.2358 94.67 67.4435 162.66 0.0000 59.27 67_. 2592 94.87 67.4569 163.33 80.6228 59.32 67.2635 97.43 68.9297 165.86 55.9880 59.54 67.2831 98.43 59.8844 176.31 59.1732 60. 96 91.5419 98.44 59.8851 176.60 0.0000 61.17 104.8859 99.53 67.7684 177.52 63.8494 62.93 98.8662 100 .11 79.1075 181.07 0.0000 63.29 85.1390 102.03 70.5450 181.52 52.8884 63.58 85.1703 103.18 77.5980 184.41 65.5423 64.28 85.2458 103.37 77.6120 143.76 66.0649 66.73 98.9191 105.21 76.8738 193.51 65.4683 67.24 99.8204 105.31 76.8809 197.03 71.2415 125.81 105.7492 106.12 83.0598 198.01 59.0926 67.75 105.7581 106.47 76.9646 201.83 62.9972 69.67 83.2896 109.28 71. 0274 203.43 .* 64.0025 70.83 89.7234 111. 00 205.31 49.0007 72.81 103.8670 111.76 0.0000 210.85 71. 8631 72. 87 103.8745 114. 06 68.6947 215.65 57.8490 74.66 92.2432 116.30 0.0000 222 .11 65.6898 74.82 92.2598 116.74 58.2656 227.09 68.7480 74.97 92.2759 119.76 74.3532 227.38 66.8498 77 .11 92.5015 121.12 58.4892 228.16 0.0000 78.74 79.0685 121. 22 59.3805 228.18 46.8168 79.69 97.0254 121.78 66.5031 116.74 46:8168 80.12 103.4580 122.06 68.2930 235.69 59.0157 80.19 0.0000 122.92 83.4324 235. 96 60.4647 80.57 111.1767 123.07 87.8813 238.63 57.6733 81. 00 111.2298 265.00 90.5916 238.98 0.0000 81. 07 102.2882 125.81 82.7482 240.99 57.7502 81. 75 104.9236 127.23 89.0828 242.00 57 .. 7832 83.79 85.9204 127.91 82.8946 244.70 47.7437 84.00 85.9398 129.30 96.3762 252.40 0.0000 85.43 116. 9034 131.20 84.9090 252.80 46.5049 86.55 110.6120 133.02 82.3512 254.15 0.0000 86.79 132.0813 133.52 81. 4894 256.23 47.5625 86.94 132.1025 136.00 61.0156 260.90 0.0000 Page 3805 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.4635 355.39 0.0000 584.27 15.5199 264.80 45.6374 356.01 29.0410 595.83 0.0000 265.00 39.4980 364.49 0.0000 427.87 15.5990 268.22 36.6348 366.42 0.0000 602.52 0.0000 269.46 43.9902 372. 51 36.9463 604.72 26.7754 270.03 44.0030 375.05 45.2049 607.14 30.1443 271.23 44.0314 377.52 43.1954 609.32 30.1641 273.65 0.0000 356.01 32.9987 610.33 30.1740 276.40 51. 0172 388.16 29.9588 614.28 15.1051 277.37 46.1346 388.63 0.0000 618.01 23.5233 277. 60 46.1404 391.69 35.1753 620.36 20.1775 278.00 46.1499 264.66 39.4581 621.93 19.0655 279.20 46.1786 401.81 39.4766 630.19 0.0000 279.54 40.2901 402.40 41. 5641 631. 2 9 22.4927 279.70 40.2935 404.85 33.2845 633.25 22.5065 280.46 52 .1072 410.95 35.4513 634.78 0.0000 283.69 56.1326 413.71 34.4468 635.95 .30.4080 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 44.3536 423.72 0.0000 645.85 11.2952 285.90 0.0000 427.09 42.4981 657.76 17.0020 287.50 49.3347 427.87 40.9368 657.90 0.0000 290.67 44.4717 433.94 36.2983 *661. 66 20.4250 293.27 0.0000 439.40 30.5759 664.57 0.0000 351.93 38.6295 453.88 28.6232 666.33 0.0000 295.96 38.6437 463.37 29.7882 666.50 0.0000 879.38 38.6937 468.07 23.9781 667.71 0.0000 299.98 38.7207 473.00 0.0000 677.62 17.0990 300.09 38. 7223 475.06 16.0263 685.70 0.0000 300.13 38.7231 476.78 21. 3818 695.00 0.0000 301.36 32.7858 477.60 25.6655 696.49 12.6064 302.85 29.8267 482.18 23.5657 696. 51 10.3143 256.23 29.8511 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.7554 306.78 35.8608 497.08 13.9992 697.49 13.7563 308.46 38.8810 505.52 23.3288 702.65 17.2198 311. 90 40.4431 507.63 0.0000 706.68 15.1701 316.51 41.0325 511. 00 27.0523 711. 68 17.2626 319.41 0.0000 514.00 32. 4963 720.70 0.0000 320.08 0.0000 514.00 32. 4963 721.93 0.0000 321. 04 39 .1143 520.40 26.0537 722.78 29.4356 323.87 39.1658 520.69 0.0000 722.91 29.4366 325.23 43.7133 .522.65 0.0000 723.31 24.2454 328.76 0.0000 527.90 0.0000 724.19 17.3218 333.37 34.7997 528.26 25.0355 727. 33 21. 9602 333.97 31.7820 529.59 14.1569 733.00 17.3633 334.37 28.7609 0.0000 735.93 17.3767 338.28 44.4816 531. 02 0.0000 .333. 97 19.7019 338.32 44.4825 537.26 0.0000 739.SO 0.0000 311.90 42.5024 546.56 0.0000 747.24 13.9438 340.48 42.5024 552.55 15.3621 748.06 15.1090 340.55 0.0000 563.25 24.7751 752.31 15.1259 344.28 43.5888 569.33 24.2720 753.82 0.0000 345.93 36.5200 '946. 00 24.2738 756.73 20.9678 351.06 29.4862 569.70 24.2756 756.80 20.9685 351.93 29.4974 583.19 . 15.5142 884.68 17.5067 Page 3806 of 5809 ENERGY MD.A COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 21.0183 1274.44 14.8003 1620.50 3.1053 766.42 20.1454 1001.03 16.6679 1621. 92 5.1767 766.84 17.5195 1002.74 12.0423 1678.03 0.0000 772. 60 0.0000 1004.73 12.9742 1690.97 5.2304 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 5.2866 778.90 17.5751 1028.54 0.0000 1063'. 66 9.5235 783.70 0.0000 1037.84 11.1995 1771. 35 5.2914 785.37 7.0417 1038.76 0.0000 1791.20 0.0000 792.07 17.6343 631.29 9.3500 1808.65 4.2556 794.95 15.0000 1048.07 0.0000 1810.72 0.0000 795.86 15.0037 1049.04 14.9678 1836.06 3.2040 810.06 14.1719 1050.41 13.1002 810.29 14.1729 1063.66 10.3219 344.28 14.1733 1077.00 0.0000 810.76 14.1743 1077.34 13.1737 *815.77 0.0000 1085.87 12.2542 1048.07 0.0000 1093.63 22.6582 832.01 12.4683 1099.45 18.1488 834.85 16. 0417 1112. 07 16.1097 835.71 19.0163 1112. 84 20.5798 836.80 0.0000 1115. 54 10.6210 846.75 0.0000 1120.29 13.2882 846.77 8.5808 1120. 55 13.2891 856.80 0.0000 1221.41 13. 2916 860.56 23.3173 1129.67 17.1167 871.09 12. 5871 1131.51 0.0000 873.19 10.7944 114'7. 95 0.0000 875.33 0.0000 1173.23 11. 5093 879.38 8.1076 1177. 95 12.4795 880.51 13.5164 1189.05 7.6958 883.24 17.1318 1204.77 14.4736 884.68 11. 7257 1221. 41 14.5184 889.28 16.2532* 1231. 02 14.5450 894.76 9.9453 1235.36 0.0000 898.04 15.3819 1238.28 21. 7492 900. 72 11. 7697 1260.41 0.0000 903.28 14.4946 1271.87 11. 7231 911.20 11. 4097. 1274.44 11. 7290 912.08 11.4120 1274.54 11.7290 923.98 0.0000 1291.59 5.8828 926.50 10.0184 1298.22 0.0000 929 .11 4.3743 1312 .11 0.0000 937.49 13.1480 1332. 49 7.9009 944.13 0.0000 1362.66 0.0000 946.00 9.1483 1365 .19 6.9526 949.00 5.8588 1368. 63 0.0000 667.71 o.ooob 1384.29 3.9861 962. 31 10.2833 1408.01 7.0034 964.08 19.1052 1457.56 0.0000 966.17 16.1734 1460.82 4.0374 911.20 18.3905 1489.16 2.0281 968. 97 18.3905 1505.03 6. 0996 983.53 0.0000 1584.12 8.2349 984 .. 45 0.0000 1596.21 0.0000 Page 3807 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:22:45.84 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
SC 29407 . * ******************************************************************************** co'nfiguration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621354.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM16.CNF;440 Background date : Z-OCT-2016 11:00:50. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 09:20:38. Sample ID G1203621354 Sample quantity 1.78756E+02 GRAM Detector name : GAM16 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.18 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID
1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err. Fit 1 0 92.48* 46 60 1. 41 184.98 178 15 1.29E-02 42.6 2 0 111.49 18 29 1. 43 222.97 218 9 4.91E-03 60.1 3 0 144.01* 17 35 1. 23 287.97 283 11 4.76E-03 74.8 4 0 185.87* 6 35 2.03 371.66 368 9 l.57E-03218.9 5 0 199.03* 16 26 1. 28 397.97 393 8 4.49E-03 63.9 6 0 273.79 23 68 5.30 547.42 534 21 6. 41E-03 91. 8 7 0 299.66 22 9 0.88 599.14 595 9 6.llE-03 32.5 8 0 383.80 8 22 0.80 7 67. 34 760 10 2.15E-03119.8 9 0 422.80 16 6 2.99 845.31 840 9 4.33E-03 39.1 10 0 511.46* 19 9 2.61 1022.57 1016 16 5.15E-03 70.0 11 0 551.98 7 2 1. 46 1103.57 1100 7 2.07E-03 46:7 12 0 565.28 9 9 1. 58 1130.16 1126 11 2.62E-03 67.7 13 0 638.92 7 9 0.59 1277.39 1269 11 l.94E-03 97.2 14 0 838.68 7 5 1. 37 1676.81 1672 10 1.94E-03 70.7 15 0 849.09 8 0 1. 49 1697.63 1695 6 2.22E-03 35.4 16 0 1461. 40* 4 5 0.89 2922.12 2916 10 1.05E-03136.7 Flag: "*" = Peak area was modified by background subtraction Page 3808 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:22:47 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621354.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 12-SEP-2016 00:00:00 Acquisition date : Gl203621354 Sample quantity 3-0CT-2016 178.76 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID Sample geometry : GAMMA16 Detector geometry: 0 01:00:00.00 Elapsed real time: 1.50 keV Half life ratio No Linear 75.00 Systematic Error Efficiencies at Interference Report Interfering Interfered Nuclide Line Nuclide Line U-235 143.76 CE-141 145.44 Page 3809of5809 CAN 0 01:00:00.18 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Sample ID : G1203621354 Nuclide Type: Nuclide Energy %Abn %Ef f K-40 1460.82 10.66* 1.215E+OO CE-141 145.44 48.29* 6.768E+OO U-235 89. 96 3.47 5.608E+OO 93.35 5.60 5.774E+OO 143.76 10. 96:" 6.770E+OO 163.33 5.08 6.541E+OO 185.72 57.20 6.166E+OO 205.31 5.01 5.819E+OO ANH-511 511. 00 100.00* 2.835E+OO Flag: "*" = Keyline Page 3810of5809 Page : 2 Acquisition date 3-0CT-2016 09:20:38 Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error Status l.203E-01 1.203E-01 273.45 OK 2.709E-02 4.277E-02 166.66 OK Line Not Found Absent 8.508E-01 8.508E-01 85.24 OK Line Not Found <<INT Reject Line Not Found Absent 8.759E-03 8.759E-03 437.85 OK Line Not Found Absent 3.146E-02 3.146E-02 139. 98 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:22:48.93 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621354.CNF;l *
Acquisition date 3-0CT-2016 09:20:38 Sensitivity : 3.000 *
Detector ID GAM16 Energy tole'rance: 1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl * *Sample ID Gl203621354 Sample Quantity 1.7876E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;14 *' ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.203E-01 3.224E-01 CE-141 4.277E-02 6.985E-02 U-235 1.305E-01 1.913E-01 ANH-511 3.146E-02 4.315E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Page 3811of5809 Key-:--Line Activity (pCi/GRAM -8 .196E-02 -3.268E-03 O.OOOE-+:00 -2 .113E-02 -5.940E-03 -3.725E-03 -5.904E-02 -9. 996E-03 8.005E-03 O.OOOE+OO -2.793E-03 -9.923E-03 -3.439E-02 3.549E-03 -l.849E-03 2.389E-01 -7.761E-02 2.345E-02 -2.877E-02 -3.293E+Ol -9.639E-02 3.589E-02 4.513E+OO 2.544E-02 l.416E-01 -4.175E-03 K.L. Cnt Uncert (1.96-sigma) l.605E-01 1.382E-02 2.654E+08 2.232E-02 1.535E-02 3. 951E-02 2. 081E-01 2.156E-02 1.918E-02 1. 960E+41 9.920E-03 l.852E-02 4.188E-02 1.* 450E-02 3.450E-02 3.694E-01 4.120E-Ol 6.759E-02 2.497E-02 2.741E+Ol 1.598E-01 3.236E-02 3.668E+OO 2.075E-02 3.250E-01 1.593E-02 MDA (pCi/GRAM 4.423E-01 4.733E-02 1. 847E-01 2.498E-02 MDA (pCi/GRAM 3.033E-01 2. 963E-02 O.OOOE+OO 3.495E-02 3.152E-02 8.527E-02 4.194E-01 3.567E-02 4.236E-02 O.OOOE+OO l.955E-02 3.614E-02 7.070E-02 3.602E-02 7.490E-02 1.050E+OO 8.695E-01 l.437E-01 3.829E-02 4.947E+Ol 2.756E-01 8 .191E-02 8.776E+OO 4. 962E-02 8.465E:._01 3.664E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

Y-91 -4.335E+OO 7.522E+OO 1.382E+Ol NOT IDENT. NB-94 -3.675E-03 1.843E-02 3.535E-02 NOT IDENT. NB-95 4.021E-03 1.515E-02 _3. 523E-02 NOT IDENT. NB-95M -l.822E-02 4.654E-02 8. 496E-02 NOT IDENT. ZR-95 -9.992E-03 3.568E-02 6.837E-02 NOT IDENT. NB-97 O.OOOE+OO l.603E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 4.378E+08 O.OOOE+OO SHORT HLIF M0-99 -8.378E+OO 2.729E+Ol 5.212E+Ol NOT IDENT .. TC-99M . O.OOOE+OO 4.994E+23 O.OOOE+OO SHORT HLIF RH-101 -4.797E-03 l.177E-02 2.266E-02 FAIL ABUN RH-102 5.097E-03 2.416E-02 5.295E-02 NOT IDENT. RU-103 2.0lOE-02 2.270E-02 5.333E-02 NOT IDENT. RH-106 -1.539E-02 l.472E-01 2.988E-01 NOT IDENT. RU-106 -1.539E-02 l.472E-01 2.988E-01 NOT IDENT. AG-108M -5.794E-03 l.447E-02 2.809E-02 NOT IDENT. CD-109 4.947E-02 2.679E-01 5.464E-01 NOT IDENT. AG-110M -2.342E-02 2.084E-02 3.214E-02 NOT IDENT. SN-113 -6.025E-03 2.378E-02 4.737E-02 NOT IDENT. CD-115 l.203E+Ol 3.738E+Ol 8. 272E+Ol NOT IDENT. SN-117M l.659E-02 2.693E-02 5.953E-02 NOT IDENT. TE-123M 5.520E-03 1.104E-02 2.383E-02 NOT IDENT. SB-124 9.344E-03 3.751E-02 9.952E-02 NOT IDENT. SB-125 3.455E-02 3.759E-02 9.238E-02 NOT IDENT. TE-125M--2.689E+OO 3.779E+OO 6.245E+OO NOT IDENT. I-126 -l.158E-01 1. 580E-01 2.690E-01 NOT IDENT. SB-126 -4.417E-02 9.452E-02 1.826E-01 NOT IDENT. SN-126 8.352E-03 2.663E-02 5.532E-02 NOT IDENT. SB-127 -1.324E+OO 2. 239E+O'O 3.945E+00 NOT IDENT. I-131 4.884E-02 9.468E-02 2.123E-01 NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 1. 497E-01 l.279E+00 2.513E+OO FAIL ABUN BA-133 -7.059E-03 1. 841E-02 3.657E-02 FAIL ABUN I-133 O.OOOE+OO 3.624E+05 O.OOOE+OO SHORT HLIF CS-134 7.014E-03 l.931E-02 4. 271E-02 NOT IDENT. CS-135 4.886E-03 6.127E-02 1.325E-01 NOT IDENT. I-135 O.OOOE+OO 1. 707E+22 O.OOOE+OO SHORT HLIF CS-136 -2.788E-02 5.064E-02 9.663E-02 FAIL ABUN BA-137M -1. 475E-02 1.893E-02 3.187E-02 NOT IDENT. CS-137 -l.558E-02 2.000E-02 3.367E-02 NOT IDENT. CE-139 -4.285E-03 1. 390E-02 2.624E-02 NOT IDENT. BA-140 -8.493E-02 l.818E-01 3.420E-01 FAIL ABUN LA-140 -9.886E-02 8.816E-02 l.180E-01 NOT IDENT. CE-143 0.000E+OO 1.277E+03 O.OOOE+OO SHORT HLIF CE-144 -7.222E-02 7.936E-02 l.390E-01 NOT IDENT. PM-144 -4.886E-03 1. 789E-02 3.406E-02 NOT IDENT. PR-144 -3.668E-01 l.343E+OO 2.557E+00 NOT IDENT. PM-146 l.896E-03 l.559E-02 3.467E-02 NOT IDENT. ND-147 -3.394E-01 3.225E-01 4.955E-01 FAIL ABUN PM-147 l.232E+02 2.642E+02 5.862E+02 NOT IDENT. PM-149 9.794E+Ol 2.886E+02 6.356E+02 NOT IDENT. EU-150 5.203E-03 l.246E-02 2.751E-02 NOT IDENT. EU-152 -3.694E-02 4.644E-02 8.594E-02 NOT IDENT. GD-15.3 -1.229E-02 3.678E-02 6.684E-02 NOT IDENT. EU-154 -9.229E-03 3.904E-02 8.369E-02 NOT IDENT. EU-155 -2.888E-02 3; 696E-02 6.782E-02 NOT IDENT. TB-160 -1. 7 56E-02 7.490E-02 1.527E-01 FAIL ABUN H0-166M -2 .132E-02 3.657E-02 6.409E-02 FAIL ABUN TM-171 -l.465E+00 7.523E+OO 1.602E+Ol NOT IDENT. HF-172 -9.223E-03 7. 061E-02 1.424E-01 NOT IDENT. LU-172 -3.036E-02 2.993E-02 4.704E-02 NOT IDENT. LU-176 1.223E-03 1.077E-02 2.339E-02 NOT IDENT. HF-181 1.194E-03 2.099E-02 4.488E-02 NOT IDENT. TA-182 -4.403E-03 7.623E-02 l.630E-01 NOT IDENT. RE-183 8.638E-03 8.641E-02 1.905E-01 NOT IDENT. RE-184 -5. 311E-03 3. 913E-02 9.157E-02 NOT IDENT. W-188 l.309E+00 3.508E+OO 7. 710E+OO NOT IDENT. IR-192 l.686E-03 l.791E-02 3.789E-02 NOT IDENT. HG-203 -3.844E-03 2 .133E-02 3.927E-02 NOT IDENT. BI-207 -7.275E-03 2.318E-02 4.659E-02 NOT IDENT. TL-208 1.068E-03 1.483E-02 3.336E-02 NOT IDENT. PB-210 -6.798E-02 1.892E+OO 4.125E+OO NOT IDENT. BI-211 1. 14 7E-02 1.074E-01 2.225E-01 NOT IDENT. PB-211 6.915E-02 3.478E-01 7.428E-01 NOT IDENT. BI-212 2.834E-03 2.220E-01 4.607E-01 NOT IDENT. PB-212 -4.025E-02 2.735E-02 4. 741E-02 FAIL ABUN BI-214 2.178E-02 4.304E-02 9.221E-02 NOT IDENT .* PB-214 2.002E-02 3.820E-02 8. 331E-02 NOT IDENT. RN-219 5.933E-03 l.785E-01 3.780E-01 NOT IDENT. Page 3812of5809 RN-222 2.178E-02 4.304E-02 9. 221E-02 NOT IDENT. RA-223 2.099E-01 3.049E-01 6.907E-01 FAIL ABUN RA-224 l.697E-01 2.767E-01 6:183E-01 NOT IDENT. RA-226 2.178E-02 4.304E-02 9. 221E-02 NOT IDENT. AC-227 2.399E-03 l.093E-01 2.330E-01 FAIL ABUN TH-227 2.399E-03

1. 093E-01 2.330E-01 FAIL ABUN AC-228 -4.298E-02 6.603E-02 1. 411E-01 NOT IDENT. RA-228 -4.298E-02 6.603E-02 l.411E-01 NOT IDENT. TH-228 -4.025E-02 2.735E-02 4.741E-02 FAIL ABUN TH-229 -l.046E-01 2.207E-01 4.018E-01 NOT IDENT. TH-230 2.178E-02 4.304E-02 9.221E-02 NOT IDENT. PA-231 2.805E-02 1. 797E-01 3.648E-01 NOT IDENT. TH-231 2.099E-01 3.049E-01 6.907E-01 FAIL ABUN TH-232 -4.298E-02 6.603E-02 l.411E-01 NOT IDENT. PA-233 -1. 360E-02 2.509E-02 4.934E-02 FAIL ABUN PA-234 -7.284E-02 l.478E-01 2.846E-01 FAIL ABUN PA-234M -9.380E-01 l.908E+OO 4.369E+OO NOT IDENT. TH-234 -5.147E-01 6. 441E-Ol l.333E+OO FAIL ABUN U-234 2.178E-02 4.304E-02 9.221E-02 NOT IDENT. NP-237 -l.360E-02 2.509E-02 4.934E-02 FAIL ABUN NP-238 O.OOOE+OO 6.197E+Ol O.OOOE+OO SHORT HLIF U-238 -5.147E-01 6. 441E-01 l.333E+OO FAIL ABUN NP-239 4.052E-02 8.103E-02 1. 8 63E-01 NOT IDENT. PU-239 7.359E+Ol l.306E+02 2.864E+02 NOT IDENT. AM-241 -8.443E-03 6.021E-02 1. 285E-01 NOT IDENT. AM-243 l.957E-03 1. 7 91E-02 3.897E-02 NOT IDENT. CM-243 8.762E-03 3. 572E-02 7.845E-02 NOT IDENT. BK-247 -5.194E-02 4.312E-02 6.525E-02 NOT 'IDENT. CM-247 -3.138E-03 l.690E-02 3.438E-02 NOT IDENT. CF-249 l.870E-03 l.873E-02 3.975E-02 NOT IDENT. CF-251 1. 446E-02 5.694E-02 l.156E-01 NOT IDENT. Page 3813of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:22:46.72 Nuclide Line Activity Report Nuclide Type: Nuclide K-40 CE-141 U-235 ANH-511 Flag*: "*" Page 3814 of 5809 Energy 1460.82 145.44 89. 96 93.35 143.76 163.33 185. 72 205.31 511. 00. Key line Area 4 23 ------66 23 ------7 ------21 %Abn 10.66* 48.29* 3.47 5.60 10. 96* 5.08 57.20 5.01 100.00* Uncorrected Decay Corr %Eff pCi/GRAM pCi/GRAM 1.215E+OO 1. 203E-01 l.203E-01 6.768E+OO 2. 961E-02 4.674E-02 5.608E+OO ------Line Not Found 5.774E+OO 8.508E-01 8.508E-01 6.768E+00 l.305E-01 1.305E-01 6.541E+OO ------Line Not Found 6.166E+OO 8.759E-03 8.759E-03 5.819E+OO ------Line Not Found 2.835E+OO 3.146E-02 3.146E-02 2-Sigma %Error 273.45 149.62 ------85.24 149.62 ------437.85 ------139.98 Surrunary of Nuclide Activity Sample ID : Gl203621354 Acquisition date Page : 2 3-0CT-2016 09:20:38 Total number of lines in spectrum 16 Number of unidentified lines
4 Number of lines tentatively identified by NID 12 Nuclide Type : Nuclide K-40 CE-141 U-235 ANH-511 Hlife 1.25E+09Y 32.51D 7.04E+08Y l.OOE+09Y Decay 1. 00 1. 58 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected Decay Corr pCi/GRAM pCi/GRAM 1.203E-01 1.203E-01 2. 961E-02 4.674E-02 l.305E-01 1.305E-01 3.146E-02 3.146E-02 ------------------3 .119E-01 3.290E-01 3 .119E-01 3.290E-01 75.00% Decay Corr 2-Sigma 2-Sigma Error %Error 3.290E-01 273.45 6.994E-02 149.62 1.952E-01 149.62 4.403E-02 139.98 Flags: "K" "E" Keyline not found Manually edited "M" Manually accepted "A" -Nuclide specific.abn. limit Page 3815of5809 Flags Unidentified Energy Lines Page : 3 Sample ID : G1203621354 Acquisition date : 3-0CT-2016 09:20:38 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 111.49 24 41 1. 43 222.97 218 9 4.91E-03 **** 6.58E+OO T 0 199.03 21 33 1. 28 397.97 393 8 4.49E-03 **** 5.93E+OO T 0 273.79 29 84 5.30 547.42 534 21 6.41E-03 **** 4.73E+OO T 0 299.66 27 11 0.88 599.14 595 9 6. llE-03 65.1 4.40E+OO T 0 383.80 9 27 0.80 767.34 760 10 2.15E-03 **** 3.59E+OO T 0 422.80 18 8 2.99 845.31 840 9* 4.33E-03 78.2 3. 31E+OO T 0 551.98 8 2 1. 46 1103. 57 1100 7 2.07E-03 93.3 2.66E+OO T 0 565.28 11 10 1.58 1130 .16 1126 11 2.62E-03 **** 2.61E+OO 0 638.92 8 10 0.59 1277.39 1269 11 1. 94E-03 **** 2.37E+OO 0 838.68 7 5 1. 37 1676.81 1672 10 l.94E-03 **** 1.91E+OO 0 849.09 9 0 1. 49 1697.63 1695 6 2.22E-03 70.7 l.89E+OO Flags: "T" = Tentatively associated Page 3816of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:23:03.47 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l *
Acquisition date 3-0CT-2016 09:20:38 Sensitivity : 3.000 *
Detector ID GAM16 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621354 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CE-141 U-235 ANH-511 Le (pCi/GRAM 1. 767E-01 2.064E-02 8.394E-02 l.038E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR.,.-85 SR-85 RB-86 Y-88 Y-91 Page 3817of5809 Le (pCi/GRAM 1.263E-01 l.050E-02 O.OOOE+OO 1.173E-02 1.192E-02 3.384E-02 l.845E-01 1.462E-02 1. 742E-02 O.OOOE+OO 8.629E-03 l.435E-02 2.600E-02 1.357E-02 2.942E-02 .4.029E-01 3.864E-01 6.255E-02 1. 672E-02 l.032E-01 3.530E-02 3.898E+00 2.204E-02 3.277E-01 l.158E-02 4.896E+00 NOT IDENT; NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W.,.-188 IR-192 HG-203 BI-207 TL-208 PB-210 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 Page 3818of5809 l.497E-02 l.398E-02 3.658E-02 2.757E-02 O.OOOE+OO O.OOOE+OO 2.094E+Ol O.OOOE+OO 9.956E-03 2.199E-02 2.336E-02 l.236E-01 1.236E-01 l.199E-02 2.408E-01. l .139E-02 2.069E-02 3. 520E+Ol . 2.652E-02 l.065E-02 3.526E-02 3.994E-02 2.658E+OO 1.097E-01* 7.433E-02 2. 451E-02 1.633E+OO 9.355E-02 O.OOOE+OO 1.123E+OO l.572E-02 O.OOOE+OO 1. 783E-02 5.829E-02 O.OOOE+OO 3.423E-02 1.307E-02 l.380E-02 1.17 9E-02 1.421E-01 4.182E-02 O.OOOE+OO 6.078E-02 1.423E-02 1.068E+OO l.435E-02 l.835E-01 2.599E+02 2.825E+02 1.218E-02 3.714E-02 2.959E-02 2. 965E-02 2.919E-02 6.335E-02 2.702E-02 7.020E+OO 6.283E-02 1. 741E-02 1.019E-02 1. 8 8 8E-0.2 6.422E-02 8.459E-02 3.278E-02 3.439E+00 1.681E-02 1.742E-02 1.835E-02 1.393E-02 l.844E+OO 9. 911E-02 3.249E-01 1.889E-01 2.102E-02 4.080E-02 3.724E-02 l.625E-01 4.080E-02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT*IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT.IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN .NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. RA-223 RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 NP-237 NP-238 0-238 NP-23.9 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3819of5809 3.085E-Ol 2.805E-Ol 4.080E-02 l.035E-01 l.035E-01 5.783E-02 5.783E-02 2.102E-02 1. 776E-01 4.080E-02 1.564E-01 3.085E-01 5.783E-02 2.095E-02 l.142E-01 1. 766E+OO 6.068E-01 4.080E-02 2.095E-02 O.OOOE+OO 6.068E-01 8.129E-02 1. 28 6E+02 5.676E-02 1. 726E-02 3.444E-02 2.842E-02 . 1. 476E-02 1. 730E-02 5.215E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:23:13.33 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * . * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l *
Acquisition date Sensitivity : 3.000 *
Detector ID GAM16 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621354 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM *
Quantity Err(%) : 1.1188E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
Eff. File *: DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CE-141 U-235 ANH-511 1.203E-01 4.277E-02 1.305E-01 3.146E-02 Act Error (1. 96-sigma) 3.225E-01 6.987E-02 l.914E-01 4.317E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 . CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Page 3820 of 5809 Key-Line Activity (pCi/GRAM -8 .196E-02 -3.268E-03 1.313E+08 -2 .113E-02 -5.940E-03 -3.725E-03 -5.904E-02 -9. 996E-03 8.005E-03 1.000E+41 -2.793E-03 -9.923E-03 -3.439E-02 3.549E-03 -l.849E-03 2.389E-01 -7. 7 61E-02 2.345E-02 -2.877E-02 -3.293E+Ol -9.639E-02 3.589E-02 4.513E+OO 2.544E-02 1.416E-01 -4.175E-03 K.L Act error ( 1. 96-sigma) l.605E-01 l.382E-02 2.654E+08 2.236E-02 1.535E-02 3. 951E-02 2.081E-01 2.157E-02 l.919E-02 2.419E+41 9.921E-03 l.852E-02 4 .196E-02 1.450E-02 3.450E-02 3.695E-01 4.123E-01 6.762E-02 2.501E-02 3.418E+Ol 1.599E-01 3.273E-02 3.673E+OO 2.077E-02 3. 251E-01 l.593E-02 TPU ( 1. 96-sigma) 3.225E-01 6.987E-02 l.914E-01 4.317E-02 TPU ( 1. 96-sigma) 1.647E-01 l.390E-02 2.720E+08 2.431E-02 1.558E-02 3.955E-02 2.098E-01 2.203E-02 1.952E-02 O.OOOE+OO 1.000E-02 l.905E-02 4.473E-02 1. 459E-0'2 3.451E-02 3.849E-01 4.138E-01 6.844E-02 2.818E-02 3.726E+Ol 1.657E-01 3.651E-02 4.199E+OO 2.373E-02 3.313E-01 l.604E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

Y-91 -4.335E+OO 7.523E+00 7.773E+OO NOT IDENT. NB-94 -3.675E-03 1. 843E-02 l.850E-02 NOT IDENT. NB-95 4. 021E-03 l.515E-02 l.526E-02 NOT IDENT. NB-95M -l.822E-02 4.656E-02 4.728E-02 NOT IDENT. ZR-95 -9.992E-03 3.569E-02 3.597E-02 NOT IDENT. NB-97 1. OOOE+41 l.604E+41 0.000E+OO SHORT HLIF ZR-97 2.002E+08 4.379E+08 4. 471E+08 SHORT HLIF M0-99 -8.378E+OO 2.730E+Ol 2.756E+Ol NOT IDENT. TC-99M -1. 787E+23 4.997E+23 0.000E+OO SHORT HLIF RH-101 -4.797E-03 l.180E-02 l.200E-02 FAIL ABUN RH-102 5.097E-03 2.416E-02 2.427E-02 NOT IDENT. RU-103 2.0lOE-02 2. 272E-02 2.446E-02 NOT IDENT. RH-106 -l.539E-02 l.472E-01 l.473E-01 NOT IDENT. RU-106 -l.539E-02 1. 4 72E-01 l.473E-01 NOT IDENT. AG-108M -5.794E-03 l.447E-02 1. 471E-02 NOT IDENT. CD-109 4.947E-02 2.680E-01 2.689E-01 NOT IDENT. AG-llOM -2.342E-02 2.087E-02 2.339E-02 NOT IDENT. SN-ll3 -6.025E-03 2.378E-02 2.394E-02 NOT IDENT. CD-ll5 l.203E+Ol 3.738E+Ol 3.778E+Ol NOT IDENT. SN-ll 7M l.659E-02 2.694E-02 2. 796E-02 NOT IDENT. TE-123M 5.520E-03 l.104E-02 l.132E-02 NOT IDENT. SB-124 9.344E-03 3.752E-02 3.775E-02 NOT IDENT. SB-125 3.455E-02 3.762E-02 4. 072E-02 NOT IDENT. TE-125M -2.689E+OO 3.782E+00 3.971E+OO NOT IDENT. I-126 -l.158E-01 l.582E-01 l.666E-01 NOT IDENT. SB-126 -4.417E-02 9.462E-02 9.670E-02 NOT IDENT. SN-126 8.352E-03 2.663E-02 2.690E-02 NOT IDENT. $8-127 -l.324E+OO 2.244E+OO 2.322E+OO NOT IDENT. I-131 4.884E-02 9.47lE-02 9. 723E-02 NOT IDENT. I-132 1. OOOE+41 7.094E+41 O.OOOE+OO SHORT HLIF TE-132 l.497E-01 l.279E+OO l.281E+OO FAIL ABUN BA-133 -7.059E-03 l.842E-02 l.869E-02 FAIL ABUN I-133 -8.566E+04 3.626E+05 3.646E+05 SHORT HLIF CS-134 7.014E-03 1. 931E-02 l.957E-02 NOT IDENT. CS-135 4.886E-03 6.127E-02 6.131E-02 NOT IDENT. I-135 2.219E+22 2.022E+22 O.OOOE+OO SHORT HLIF CS-136 -2.788E-02 5.070E-02 5.223E-02 FAIL ABUN BA-137M -l.475E-02 l.894E-02 2.008E-02 NOT IDENT. CS-137 -l.558E-02 2.00lE-02 2.121E-02 NOT IDENT. CE-139 -4.285E-03 l.393E-02 l.406E-02 NOT IDENT. BA-140 -8.493E-02 l.818E-01 l.858E-01 FAIL ABUN . LA-140 -9.886E-02 8.829E-02 9.890E-02 NOT IDENT. CE-143 2.193E+02 l.277E+03 l.281E+03 SHORT HLIF CE-144 -7.222E-02 7.946E-02 8.587E-02 NOT IDENT. -4.886E-03 1. 789E-02 l.803E-02 NOT IDENT. PR-144 -3.668E-01 l.344E+OO l.354E+OO NOT IDENT. PM-146 l.896E-03 l.559E-02 l.561E-02 NOT IDENT. ND-147 -3. 39,4E-01 3.229E-01 3.573E-01 FAIL ABUN PM-147 l.232E+02 2.643E+02 2.701E+02 NOT IDENT. PM-149 9.794E+Ol 2.889E+02 2.922E+02 NOT IDENT. EU-150 5.203E-03 l.246E-02 1. 2 68E-02 NOT IDENT. EU-152 -3.694E-02 4.649E-02 4.938E-02 NOT IDENT. GD-153 -l.229E-02 3.679E-02 3. 721E-02 NOT IDENT. EU-154 -9.229E-03 3.904E-02 3.926E-02 NOT IDENT. EU-155 -2.888E-02 3.702E-02 3.924E-02 NOT IDENT. TB-160 -1. 756E-02 7.491E-02 7.533E-02 FAIL ABUN H0-166M -2 .132E-02 3.659E-02 3.783E-02 FAIL ABUN TM-171 -l.465E+OO 7.524E+OO 7.553E+OO NOT IDENT. HF-172 -9.223E-03 7.062E-02 7.074E-02 NOT IDENT. LU-172 -3.036E-02 3.008E-02 3.305E-02 NOT IDENT. LU-176 l.223E-03 l.077E-02 l.078E-02 NOT IDENT. HF-181 l.194E-03 2.099E-02 2.lOOE-02 NOT IDENT. TA-182 -4.403E-03 7.623E-02 7.626E-02 NOT IDENT. RE-183 8.638E-03 8. 641E-02 8.650E-02 NOT IDENT. RE-184 -5. 3llE-03 3.913E-02 3.920E-02 NOT IDENT. W-188 l.309E+OO 3. 5ll:E+OO 3.560E+OO NOT IDENT. IR-192 l.686E-03 l.791E-02 1. 7 93E-02 NOT IDENT. HG-203 -3.844E-03 2 .133E-02 2.140E-02 NOT IDENT. BI-207 -7.275E-03 2.318E-02 2. 341E-02 NOT IDENT. TL-208 l.068E-03 l.483E-02 l.484E-02 NOT IDENT. PB-210 -6.798E-02 l.892E+OO l.892E+OO NOT IDENT. BI-2ll 1.14 7E-02 l.074E-01 l.075E-01 NOT IDENT. PB-2ll 6.915E-02 3.478E-01 3.492E-01 NOT IDENT. *sI-212 2.834E-03 2.220E-01 2.220E-01 NOT IDENT. PB-212 -4.025E-02 2.744E-02 3.289E-02 FAIL ABUN BI-214 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. PB-214 2.002E-02 3.821E-02 3.926E-02 NOT IDENT. RN-219 5.933E-03 l.785E-01 l.786E-01 NOT IDENT. Page 3821of5809 RN-222 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. RA-223 2.099E-01 3.052E-01 3.195E-01 FAIL ABUN RA-224 l.697E-01 2.768E-01 2.872E-01 NOT IDENT. RA-226 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. AC-227 2.399E-03 1.093E-01 l.093E-01 FAIL ABUN TH-227 2.399E-03 1.093E-01 1.093E-01 FAIL ABUN AC-228 -4.298E-02 6.606E-02 6.885E-02 NOT IDENT. RA-228 -4.298E-02 6 .* 606E-02 6.885E-02 NOT IDENT. TH-228 -4.025E-02 2.744E-02 3.289E-02 FAIL ABUN TH-229 -l.046E-01 2.208E-01 2.258E-01 NOT IDENT. TH-230 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. PA-231 2.805E-02 1. 798E-01 l.803E-01 NOT IDENT. TH-231 2.099E-01 3.052E-01 3.195E-01 FAIL ABUN TH-232 -4.298E-02 6.606E-02 6.885E-02 NOT IDENT. PA.-233 -l.360E-02 2.510E-02 2.584E-02 FAIL ABUN PA-234 -7.284E-02 l.697E-01 1. 729E-01 FAIL ABUN PA-234M -9 .. 380E-01 1.908E+OO l.954E+OO NOT IDENT. TH-234 -5.147E-01 6.541E-01 6.940E-01 FAIL ABUN U-234 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. NP-237 -1.360E-02 2.510E-02 2.584E-02 FAIL ABUN NP-238 3.348E+Ol 6.199E+.01 6.380E+Ol SHORT HLIF U-238 -5.147E-01 6.541E-01 6.940E-01 FAIL ABUN NP-239 4.052E-02 8. llOE-02 8.313E-02 NOT IDENT. PU-239 7.359E+Ol l.306E+02 1.348E+02 NOT IDENT. AM-241 -8.443E-03 6. 021E-02 6.033E-02 NOT IDENT. AM-243 l.957E-03 1. 7 91E-02 1. 7 93E-02 NOT IDENT. CM-243 8.762E-03 3.573E-02 3.594E-02 NOT IDENT. BK-247 -5.194E-02 4.438E-02 5.017E-02 NOT IDENT. CM-247 -3.138E-03 1.691E-02 1. 696E-02 NOT IDENT. CF-249 l.870E-03 l.873E-02 1.875E-02 NOT IDENT. CF-251 1.446E-02 5. 696E-02 5.733E-02 NOT IDENT. Page 3822of5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT
ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 19.1250 87.09 21.6729 136.47 15.4885 45.60 17.4169 87.57 16.2705 140.51 19.2908 46.54 14.7095 88.03 16.2856 143.76 15.6543 49.72 12.0661 88.34 19.0117 144.24 15.6652 51. 35 16.7863 88.47 19.0167 145.44 15.6921 51. 87 18.6793 89. 96 21. 4574 152.43 24.9014 52.39 14.9656 1093.63 21.4864 153.25 23.7961 52.97 14.9902 91.11 21. 5063 323.87 19.2889 53.44 19.7006 92.59 21.5687 156.02 18.1990 54.07 24.4343 93.35 21.6005 158.56 14.8374 57. 36 . 0.0000 94.56 21.6510 159.00 17.1300 57.53 23.7174 94.65 21. 6546 162.33 24.0883 57.98 19.9464 94.67 21. 6555 162.66 2Q.6559 59.27 20.0145 94.87 21. 6638 163.33 21. 8226 59.32 20.9703 97.43 24.8793 165.86 31.1137 59.54 20.9824 98.43 22.8486 176.31 31.3672 60. 96 28.7179 98.44 22.8491 176.60 30. 3719 61.17 28.7335 99.53 10.4070 177.52 24.5591 62.93 20.2036 100 .11 19.7947 181.07 21.1424 63.29 29.85*15 102.03 18.8189 181.52 27.0300 63.58 29.8731 103.18 9.4291 184.41 18.8694 64.28 31. 8560 103.37 14.6725 143.76 27 .1672 66.73 30.1060 105.21 23.1331 193.51 26.2254 67.24 24.3090 105.31 22.0855 197.03 20.7465 125.81 28.2283 106.12 20.0109 198.01 15.5773 67.75 25.3123 106.47 14.7541 201. 83 24.0692 69.67 27.3843 109.28 19.7692 203.43 24 .1122 70.83 21. 5747 111. 00 22.3066 205.31 30.2036 72. 81 26.5993 111. 76 22.3357 210.85 21.8795 72. 87 26.6031 114. 06 24.2027 215.65 34.2122 74.66 18.7969 116. 30 19.2921 222 .11 14.7631 74.82 26.7209 116.74 10.7256 227.09 24.7330 74.97 26.7299 119.76 24.7920 227.38 24.7403 77 .11 24.8680 121.12 16.2044 228.16 22.2841 78.74 28;9498 121.22 15.1265 228.18 22.2847 79.69 22. 0072 121.78 23.7918 116.74 22.2847 80.12 25.0313 122.06 22.7206 235.69 17.4654 80.19 25.0351 122.92 26.0023 235.96 17.4701 80.57 22.0487 123.07 26.0085 238.63 30.8627 81. 00 18.0564 265.00 17.3558 238.98 30.8736 81. 07 18.0592 125.81 20.6798 240.99 23.4105 81.75 32.1516 127.23 22.9075 242.00 26.7814 83.79 20.1810 127.91 26.2079 244.70 25.1743 84.00 20.1898 129.30 18.6039 252.40 26.2073 85.43 29.3620 131.20 17.5610 252.80 24'.5260 86.55 22.3256 133.02 22.0120 254.15 0.0000 86.79 21. 6597 133.52 28.6375 256.23 21.2121 86.94 21.6663 136.00 14.3721 260.90 22.1576 Page 3823 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 33.3522 355.39 0.0000 584.27 5.2895 264.80 33.3561 356.01 16.5934 595.83 11. 7041 265.00 33°. 3625 364.49 12.9863. 427.87 11.7314 268.22 17.1594 366.42 19.5068 602.52 0.0000 269.46 17.1790 372.51 14. 9271 604. 72 6.4119 270.03 17.1879 375.05 12.1502 607.14 17.1185 271. 23 17.2066 377.52 9.8309 609.32 9.6394 273.65 17.2441 356.01 14.i064 610.33 12.8589 276.40 22.0406 388.16 14.1486 614.28 7.5153 277.37 20.7622 388.63 14.1531 618.01 10.7552 277.60 20.7661 391.69 18.9107 620.36 8.6139 278. 00 20.7734 264.66 13.3184 621.93 8.6204 279.20 23.3954 401. 81 12.3766 630.19 0.0000 279.54 23.4025 402.40 14.2865 631.29 6.4941 279.70 24.9662 404.85 14.3100 633.25 9.7504 280.46 *20.8188 410.95 14.3680 634.78 8 .1311 283.69 25.2275 413. 71 13. 4346 635.95 11. 3895 284.31 20.8896 414.70 12.4829 636.99 10.8525 285.41 16.5535 423.72 8.6929 645.85 9.8079 285.90 17.4320 427.09 4.6463 657.76 4.3830 287.50 19.2021 427.87 5.8108 657.90 0.0000 290.67 18.3793 433.94 15.5553 661. 66 14.2695 293.27 0.0000 439.40 13.6579 664.57 0.0000 351. 93 15.8152 453. 88 6.8905 666.33 13.2002 295. 96 15.8251 463.37 7.9202 666.50 12.1011. 879.38 10.5735 468.07 6.9497 667. 71 0.0000 299.98 9.7038 473.00 8. 961 7 677.62 8.8447 300.09 9.7047 475.06 13.9573 685.70 13.3145 300.13 9.7049 476.78 7.9837 695.00 11.1410 301.36 10.5981 477.60 12.9799 696.49 11.1483 302.85 15.9170 482.18 9.0101 696.51 11.1483 256.23 11. 68 83 487.02 10.0395 697.00 14.4959 304.85 15.0576 492.35 11. 0774 697.30 16.7279 306.78 14.1947 497.08 8.0781 697.49 16.7297 308.46 13.3258 505.52 16.7410 702.65 12.2958 311. 90 16.0360 507.63 0.0000 706.68 14.5568 316.51 19.6730 511. 00 8.1417 711. 68 15.7101 319.41 17.9264 514.00 8.1553 720.70 6.7588 320.08 21. 5229 514.00 8.1553 721. 93 0.0000 321. 04 25.1295 520.40 4.0921 722.78 3.3824 323.87 15.2914 520.69 5.1160 722.91 1.127 5 325.23 21. 6113 522.65 0.0000 723.31 2.2555 328.76 21.6714 527.90 8.2178 724 .19 2.2563 333.37 21.7495 528.26 5 .1371 727. 33 5.6482 333.97 15.4128 529.59 8.2253 733.00 7.9263 334.37 18.1384 529.87 0.0000 735.93 3. 4011 338.28 14.5547 531.02 10.2897 333.97 9.0755 338.32 14.5550 537.26 12.3892 739.50 7.9479 311.90 20.9575 546.56 0.0000 747.24 2.2781 340.48 20.9575 552.55 4.6837 748.06 3.4183 340.55 22.7809 563.25 4.7098 752.31 3.4243 344.28 22.8455 569.33 11. 0242 753.82 4.5685 345.93 13.7244 946.00 6.3000 756.73 8.0043 351.06 16.5330 569.70 6.3008 756.80 5.7176 351.93 12.8672 583.19 4.2293 884.68 4.5874 Page 3824 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 3.4431 1274.44 7.4849 1620.50 5.5142 766.42 3.4440 1001.03 2. 8112 1621. 92 4.4126 766.84 6.8892 1002.74 1.8752 1678.03 0.0000 772. 60 0.0000 1004.73 6.5674 1690.97 1.1194 776.52 6.9158 507.63 0.0000 1750.46 0.0000 739.50 5.7664 1025.87 0.0000 1764.49 4.5459 778.90 4.6149 1028.54 0.0000 1063.66 1.8205 783.70 5.7798 1037.84 2.8445 1771. 35 1.8209 785.37 2.3134 1038.76 0.0000 1791.20 0.0000 792.07 8 .1182 631.29 3.8030 1808.65 6.4207 794.95 5.8055 1048.07 4.7559 1810.72 0.0000 795.86 5.8075 1049.04 4.7574 1836.06 1.8443 810.06 11. 3873 1050.41 5. 7114 810.29 8.7601 1063.66 6.6907 344.28 8.7607 1077.00 1.9194 810.76 8.7619 1077.34 0.9598 815.77 6.1451 1085.87 5.7740 1048.07 4.3939 1093.63 9.6460 832.01 5.2998 1099.45 7.7305 834.85 11.3184 1112. 07 1.9398 835.71 9.9070 1112.84 3.8806 836.80 0.0000 1115.54 4.8547 846.75 0.0000 1120.29 7.7783 846.77 4.2634 1120.55 6.8065 856.80 6.2406 1221.41 8.7534 860.56 7'.1421 1129. 67 1. 9500 871.09 3.5847 1131.51 0.0000 873.19 13.4532 1147.95 0.0000 875.33 0.0000 1173.23 1. 9747 879.38 9.8878 1177.95 3.9546 880.51 5.3956 1189.05 0.9918 883.24 9.9016 1204.77 4.9808 884.68 9.0060 1221. 41 5.0037 889.28 5.4126 1231. 02 4. 0134 894.76 1.8077 1235.36 4.0183 898.04 3.6196 1238.28 3.0161 900.72 2.7173 1260.41 0.0000 903.28 2.7198 1271. 87 3.0434 911.20 4.5456 1274.44 3.0456 912.08 2.7282 1274.54 3.0456 923.98 0.0000 1291. 59 5.0989 926.50 5.4838 1298.22 0.0000 929 .11 3.6592 1312 .11 2.0505 937.49 2.7523 1332.49 2.0613 944.13 5.5172 1362.66 0.0000 946.00 9.2010 1365.19 2.0784 949.00 6.4474 1368.63 0.0000 667. 71 0.0000 1384.29 2.0883 962. 31 6.4762 1408.01 3.1507 964.08 5.5543 1457.56 0.0000 966 .17 8. 3372 1460.82 5.3183 911. 20 6.4907 1489.16 3.2122 968. 97 6.4907 1505.03 2.1494 983.53 5.5904 1584.12 3.2822 984.45 0.0000 1596.21 9.8729 Page 3825 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:23:48.28 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621355.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM27.CNF;330 Background date : Z-OCT-2016 11:01:30. Sample date 30-NOV-2015 10:40:00 Acquisition date : 3-0CT-2016 09:21:06. Sample ID G1203621355 *sample quantity 1.70095E+02 GRAM Detector name : GAM27 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.94 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3826 of 5809 Energy 46.85* 63.28* 72. 95 75.00* 77.05 87.08 89.88 92.83* 128.35 143.77* 163.65* 186.05* 209 .11 225.87 238.68* 241. 80 270.69 295.59* 300.50 328.98 338.07* 351.90* 463.97 491. 06 511. 06* 583.46* 609.47* 642.39 663.05* 728.29 742.43 845.51 8 60. 2 9 881.21 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 19 36 35 161 284 63 59 45 50 15 7 70 46 20 404 88 42 200 53 15 90 312 20 17 73 155 202 15 17 38 27 8 29 15 Bkgnd FWHM Channel Left Pw Cts/Sec 136 167 212 168 168 227 82 196 106 81 133 106 77 54 161 74 70 74 52 76 57 69 71 20 55 42 53 18 46 41 12 7 12 17 1.58 93.01 1.00 125.87 1. 23 145. 23 0.95 149.32 1.24 153.43 1.15 173.50 1.22 179.10 1.29 185.01 2.38 256.06 0.75 286.91 1.40 326.69 1.72 371.51 0.85 417.64 1. 27 451.18 1.14 476.81 1.22 483.06 2.21 540.85 1.08 590.67 1.18 600.50 1.29 657.49 1.34 675.67 '1.28 703.35 3.36 927.58 1.56 981.79 1.83 1021.80 1.46 1166.67 1.46 1218.71 1.60 1284.60 1. 97 1325. 95 1.82 1456.48 0.81 1484.78 1. 23 1691. 05 1.45 1720.62 3.68 1762.50 89 122 142 142 142 171 177 177 252' 284 324 367 415 449 471 481 536 586 597 651 669 697 919 979 1016 1159 1212 1279 1320 1448 1480 1687 1715 1754 8 5.25E-03115.3 7 1.0lE-02 63.9 15 9.80E-03 68.3 15 4.47E-02 15.1 15 7.89E-02 10.1 7 1. 7 5E-02 41. 5 12 1. 65E-02 21. 8 12 1.25E-02 60.7 8 1. 39E-02 38. 2 6 4.lOE-03103.6 8 l.98E-03287.1 8 1. 93E-02 30. 4 8 1.29E-02 35.6 6 5.45E-03 63.0 10 1.12E-01 7. 8 6 2.46E-02 19.3 11 1.16E-02 41.7 11 5.56E-02 11.1 8 1.47E-02 27.3 10 4.26E-03108.8 11 2.49E-02 20.1 13 8.67E-02 7.9 13 5.57E-03 89.7 9 4.68E-03 52.2 15 2.02E-02 29.1 16 4.30E-02 12.7 15 5.62E-02 10.7 9 4.26E-03 57.7 15 4.77E-03 93.8 15 1. 05E-02 40. 3 10 7.42E-03 31.4 6 2.11&...:03 67.4 10 7.93E-03 29.8 14 4.12E-03 65.1 Fit 4.62E+OO 9.35E-01 Peak Search Report (continued) Page : 2 sample ro : G1203621355 Acquisition date 3-0CT-2016 09:21:06 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 893.41 69 26 15.20 1786.90 1773 33 1.93E-02 24.9 36 0 911. 45* 90 . 43 1.14 1823.01 . 1817 13 2.50E-02 18.6 37 0 927.40 23 14 4.86 1854.93 1846 15 6.46E-03 41. 5 38 0 969.64* 55 45 1.46'1939.47 1934 14 1.54E-02 29.4 39 0 1120.31* 66 11 1.73 2240.99 2235 11 1.83E-02 16.1 40 0 1126.44 10 6 1. 44 2253. 27 2250 8 2.72E-03 54.1 41 0 1177.68 15 2 0.98 2355.81 2352 8 .4 .13E-03 30.8 42 0 1180.97 13 2 0.76 2362.41 2359 8 3. 72E-03 32.5 43 0 1193.17 10 17 3.36 2386.82 2379 10 2.79E-03 83.6 44 0 1237.59 31 19 0.92 2475.71 2467 15 8.73E-03 34.9 45 0 1279.23 12 1 0.64 2559.04 2556 8 3.22E-03 35.6 46 0 1297.27 6 16 2.86 2595.15 2585 13 1.66E-03144.7 47 0 1364.61 4 6 1.23 2729.93 2722 9 1.19E-03116.7 48 0 1376.86 31 0 1.21 2754.45 2747 14 8. 61E-03 18.0 49 0 1409.66 18 3 3.28 2820.10 2813 14 4.94E-03 32.4 50 0 1460.82* 417 4 2.06 2922.50 2915 16 l.16E-01 5.1 51 0 1765.04* 27 7 2.24 3531.43 3524 13 7.52E-03 29.0 Flag: "*" = Peak area was modified by background subtraction Page 3827 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:.23:51 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621355.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 10:40:00 Gl203621355 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:21:06 170.10 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA27 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 *74. 82 PB-214 351. 93 Page 3828 of 5809. Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM...:243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.94 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : Gl203621355 Acquisition date 3-0CT-2016 09:21:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.403E+.00 l.202E+Ol 1.202E+Ol 10.14 OK C0-56 846.77 99.94* 2.182E+OO 1. 621E-02 2.572E-01 134.83 OK 1037.84 14.17 l.863E+OO Line Not Found Absent 1238.28 66.90 l.617E+OO l.282E-01 2.033E+OO 69.84 OK 1771. 35 15.47 l.172E+OO Line Not Found Absent CD-109 88.03 3.70* 7.559E+OO 2.810E-01 4.463E-01 409.78 OK SN-126 64.28 9.60 5.534E+OO 4.297E-01 4.297E-01 127.75 OK 86.94 8.90 7.559E+OO l.168E-01 l.168E-01 409.78 OK 87.57 37.00* 7.559E+OO 2.810E-02 2.810E-02 409.78 OK BA-137M 661. 66 89.90* 2.620E+OO 3.503E-02 3.572E-02 187.70 OK CS-137 661. 66 85.10* 2.620E+OO 3.701E-02 3.773E-02 187.70 OK TL-208 277.37 6.60 5.132E+OO Line Not Found Absent 583.19 85.00* 2.885E+OO 3.083E-01 3.083E-01 25.31 OK 860.56 12.50 2.153E+OO 4.920E-01 4.920E-01 59.57 OK PB-210 46.54 4.25* 2.754E+OO 1.042E+OO 1.070E+OO 230.61 OK PB-212 74.82 10.28 6.772E+OO 7.609E-01 7.609E-01 58.94 OK 77 .11 17.10 6.937E+OO 1.470E+OO 1.470E+OO 20 .11 OK 238.63 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 OK 300.09 3.30 4.823E+00 1.763E+OO 1. 763E+OO 54.55 OK BI-214 609.32 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 OK 1120.29 14.92 i. 754E+OO l.129E+OO 1.129E+OO 32.27 OK 1764.49 15.30 l.177E+OO 6.303E-01 6.305E-01 58.08 OK PB-214 74.82 5.80 6.757E+OO Line Not Found <<INT Reject 77 .11 9.70 6.937E+OO 2.591E+OO 2.592E+OO 20 .11 OK 87.09 3.41 7.559E+OO Line Not Found <<INT Reject 242.00 7.25 5.693E+OO l.163E+OO 1.164E+OO 38.53 OK 295.22 18.42 4.885E+OO l.180E+OO l.180E+00 22.14 OK 351. 93 35.60* 4.262E+OO 1.069E+OO l.069E+OO 15.89 OK RN-222 609.32 45.49* 2.791E+OO 7.732E-01 7.735E-01 2.1. 38 OK 1120.29 14.92 1. 754E+OO l.129E+OO l.129E+00 32.27 OK 1764.49 15.30 l.177E+OO 6.303E-01 6.305E-01 58.08 OK RA-226 609.32 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 OK 1120.29 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 OK 1764.49 15.30 l.177E+OO 6.303E-01 6.305E-01 58.08 OK AC-228 105.21 1.10 8.060E+OO Line Not Found Absent 338.32 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835. 71 1. 61 2.201E+OO Line Not Found Absent 911. 20 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 OK 968.97 15.80 1. 964E+OO 8.137E-01 8.137E-01 58.83 OK RA-228 105.21 1.10 8.060E+OO Line Not Found Absent 338.32 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835. 71 1. 61 2.201E+OO Line Not* Found Absent 911.20 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 OK 968. 97 15.80 1. 964E+OO 8.137E-01 8.137E-01 58.83 OK TH-228 74.82 10.28 6. 772E+OO 7.609E-01 7.609E-01 58.94 OK 77 .11 17.10 6.937E+OO 1.470E+OO l.470E+OO 20.11 OK 238.63 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 OK Page 3829of5809 Nuclide Line Activity Report *(continued) Page : 3 Sample ID : Gl203621355 Acquisition date 3-0CT-2016 09:21:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.823E+OO 1. 763E+OO l.763E+OO 54.55 OK TH-230 609.32 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 OK 1120.29 14.92 1. 754E+OO l.129E+OO l.129E+OO 32.27 OK 1764.49 15.30 l.177E+OO 6.303E-01 6.303E-01 58.08 OK PA-231 283.69 1. 70 5.044E+OO Line Not Found Absent 301.36 5.35* 4.823E+OO l.087E+OO l.087E+OO 54.55 OK TH-232 105.21 1.10 8.060E+OO Line Not Found Absent 338.32 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 OK 835.71 1. 61 2.201E+OO Line Not Found Absent 911.20 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 OK 968. 97 15.80 1. 964E+OO 8.137E-01 8 .137E-01 58.83 OK TH-234 63.29 3.70* 5.534E+OO l .115E+OO l .115E+OO 127.75 OK 92.59 4.23 7.793E+OO -8.209E-01 8.209E-01 '121.48 OK U-234 609.32 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 OK 1120. 29 14.92 1. 754E+OO l.129E+OO l.129E+OO 32.27 OK 1764.49 15.30 l. l 77E+OO 6.303E-01 6.303E-01 58.08 OK U-235 89. 96 3.47 7.683E+OO l.346E+00 l.346E+OO 43.58 OK 93.35 5.60 7.793E+OO 6.201E-01 6.201E-01 121. 48 OK 143.76 10. 96* 7.743E+OO l.OOlE-01 l.OOlE-01 OK 163.33 5.08 7.318E+OO l.089E-01 1. 089E-01 574.18 OK 185.72 57.20 6.810E+OO 9.991E-02 9.991E-02 60.79 OK 205.31 5.01 6.393E+OO Line Not Found Absent U-238 63.29 3.70* 5.534E+OO l .115E+OO l .115E+OO 127.75 OK 92.59 4.23 7.793E+OO 8.209E-01 8.209E-01 121.48 OK AM-243 43.53 5.90 2.021E+OO Line Not Found Absent 74.66 67. 20'1< 6. 772E+OO l.164E-01 l.164E-01 58.94 OK ANH-511 511. 00 100.00* 3.191E+00 l.133E-01 l.133E-01 58.16 OK Flag: "*" = Keyline Page 3830 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:23:53.38 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621355.CNF;l * *Acquisition date 3-0CT-2016 09:21:06 Sensitivity : 3.000 *
Detector ID GAM27 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.94 Half life ratio : ***** *
Sample date 30-NOV-2015 10:40:00 Analyst initials: MXRl * *Sample ID G1203621355 Sample Quantity 1.7010E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;13
Combined Activity-MDA Report *NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-s igma) K-40 1.202E+Ol 1.195E+OO C0-56 2.572E-01 3.398E-01 CD-109 4.463E-01 1.792E+OO SN-126 2.810E-02 1.129E-01 BA-137M 3. 572E-02 6.570E-02 cs.:...137 3.773E-02 6.941E-02 TL-208 3.083E-01 7.646E-02 PB-210 1.070E+OO 2.417E+OO PB-212 8.762E-01 l.346E-01 BI-214 7.735E-01 1. 621E-01 PB-214 1.069E+OO l.665E-01 RN-222 7.735E-01 1. 621E-01 RA-226 7.735E-01 1. 621E-01 AC-228 7.786E-01 2.839E-01 RA-228 7.786E-01 2.839E-01 TH-228 8.762E-01 l.346E-01 Tff-230 7.732E-01 l.620E-01 PA-231 1.087E+OO 5.814E-01 TH-232 7.786E-01 2.839E-01 TH-234 1.115E+OO 1.396E+OO U-234 7.732E-01 1.620E-01 U-235 1.00lE-01 2.032E-01 U-238 l .115E+OO 1.396E+OO AM-243 1.164E-01 6.724E-02 ANH-511 l .133E-01 6.461E-02. Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3831 of 5809 Key-Line Activity (pCi/GRAM 3.678E+OO 2.007E-02 0.000E+OO l.348E-03 1. 969E-01 K.L. Cnt Uncert ( 1. 96-sigma) l.018E+Ol 3.275E-02 1.163E+41 2.044E-02 3.186E-01 MDA (pCi/GRAM 4.316E-01 7.009E-01 1.622E+OO 1. 024E-01 4.983E-02 5.264E-02 4.442E-02 1. 808E+OO 8.079E-02 9.914E-02 9.042E-02 9.914E-02 1.841E-01 l.841E-01 8.079E-02 9.910E-02 5.989E-01 1.841E-01 l.264E+OO 9.910E-02 2.518E-01 1. 264E+OO 5.755E-02 4.140E-02 MDA (pCi/GRAM 2.073E+Ol 6.762E-02 O.OOOE+OO 4.652E-02 6.883E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.530E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.922E+02 O.OOOE+OO SHORT HLIF MN-54 2.301E-02 4.982E-02 1.054E-01 NOT IDENT. MN-56 O.OOOE+OO 1.321E+41 O.OOOE+OO SHORT HLIF C0-57 -4.736E-03 3.484E-02 6.586E-02 NOT IDENT. C0-58 -1.976E-01 4.286E-01 8.210E-01 NOT IDENT. FE-59 -3.122E+OO 6.409E+OO l.170E+Ol NOT IDENT. C0-60 3.445E-03 2.518E-02 5.302E-02 NOT IDENT.
ZN-65 4.042E-03 l.320E-01 2.349E-01 NOT IDENT. GE-68 2.096E+OO 2.037E+OO 4.508E+OO NOT IDENT. AS-73 -1.544E+OO 3.929E+OO 7.706E+OO NOT IDENT. AS-74 O.OOOE+OO 5.787E+03 O.OOOE+OO SHORT HLIF SE-75 -6.294E-02 1.598E-01 3. llOE-01 NOT I DENT .. BR-77 O.OOOE+OO 2.583E+38 O.OOOE+OO SHORT HLIF. SR-82 O.OOOE+OO 6. 968E+02 O.OOOE+OO SHORT HLIF RB-83 3.257E-02 5. 307E-01 . 1.040E+OO NOT IDENT. KR-85 7.659E-01 6.101E+OO l.068E+Ol NOT IDENT. SR-85 8. 7 67E-02 7.020E-01 l.229E+OO NOT IDENT. RB-86 O.OOOE+OO 3.195E+04 O.OOOE+OO SHORT HLIF Y-88 2.683E-02 1.421E-01 3.400E-01 NOT IDENT. Y-91 -3.144E+02 4.620E+02 8.069E+02 NOT IDENT. NB-94 -2. 081E-02 2.563E-02 4. 271E-02 NOT IDENT. NB-95 -9.650E-01 7. 396E-01 l.098E+00 NOT IDENT. NB-95M -4.666E-01 2.107E+OO 3.739E+OO NOT IDENT. ZR-95 7.913E-01 l.365E+00 2.755E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF Mo...:99 O.OOOE+OO 1.139E+33 o*. OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.693E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 4.806E-02 4.741E-02 FAIL ABUN RH-102 2.394E-02 4. 712E-02 9.612E-02 NOT IDENT. RU-103 1. 021E+O.O 4.656E+OO 9.393E+OO FAIL ABUN RH-106 7.037E-02 4. 641E-01 8.916E-01 NOT IDENT. RU-106 7.037E-02 4.641E-01 8.916E-01 NOT IDENT. AG-108M -1.534E-02 2.186E-02 3.870E-02 NOT IDENT. AG-llOM 3.414E-03 9.427E-02 1.282E-01 NOT IDENT. SN-113 -l.954E-02 1.656E-01 3.248E-01 NOT IDENT . CD-115 . 0. OOOE+OO 3.293E+40 O.OOOE+OO .SHORT HLIF SN-117M O.OOOE+OO 1.140E+05 O.OOOE+OO SHORT HLIF TE-123M 6.327E-02 l.058E-01 2.078E-01 NOT IDENT. SB-124 6.668E-01 1. 779E+OO 3. 969E+OO NOT IDENT. SB-125 1. BlOE-02 7.460E-02 1. 511E-01 FAIL ABUN TE-125M 1. 07 5E+02 2.210E+02 4. 391E+02 NOT IDENT. I-126 O.OOOE+OO 1. 049E+06 o. o*ooE+oo SHORT HLIF SB-126 O.OOOE+OO 1. 521E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 8.688E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.297E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.554E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.819E+27 O.OOOE+OO SHORT HLIF BA-133 -3.907E-02 3.499E-02 5.465E-02 NOT IDENT. I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 1.935E-02 3.801E-02 7.724E-02 FAIL ABUN CS-135 -3.494E-02 1.022E-01 l.784E-01 NOT IDENT. I-135 O.OOOE+OO 1. 742E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.398E+05 O.OOOE+OO SHORT HLIF CE-139 2.436E-02 9.839E-02 1.730E-01 NOT IDENT. BA-140 O.OOOE+OO 1.615E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.438E+05 O.OOOE+OO SHORT HLIF CE-141 -7.203E+OO 2.469E+Ol 4.148E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 6.426E-02 2.633E-01 5.098E-01 NOT IDENT. PM-144 8.028E-03 4.591E-02 8.860E-02 NOT IDENT. PR-144 :-2.579E-01 4 .136E+OO 7. 714E+OO NOT IDENT. PM-146 -1. 331E-02 2.789E-02 5.190E-02 NOT IDENT. ND-147 O.OOOE+OO 4 .112E+07 O.OOOE+OO SHORT HLIF PM-147 -1.748E+02 5.920E+02 1.105E+03 NOT IDENT. PM-149 O.OOOE+OO l.313E+41 O.OOOE+OO SHORT HLIF EU-150 6.773E-03 1. 8 66E-02 3.517E-02 FAIL ABUN EU-152 -2.135E-02 6.860E-02 l.320E-01 NOT IDENT. GD-153 -l.419E-01 1.253E-01 2.217E-01 NOT IDENT. EU-154 3.377E-02 8.418E-02 l.642E-01 NOT IDENT. EU-155 6. 871E-02 7.541E-02 1. 551E-01 FAIL ABUN TB-160 -4.399E-01 l.406E+OO 2.733E+OO FAIL ABUN H0-166M l.746E-02 4.678E-02 9.286E-02 NOT IDENT. TM-171 -8.480E-01 7.778E+OO 1.566E+Ol NOT IDENT. HF-172 -l.107E-01 1. 7 65E-01 2.904E-01 FAIL ABUN LU-172 1. 076E-02 5.610E-02 l.152E-01 FAIL ABUN LU-176 -1. 847E-02 1. 786E-02 3.221E-02 FAIL ABUN Page 3832 of 5809 HF-181 1.264E+OO 3.195E+OO 6.672E+OO NOT IDENT. TA-182 2.691E-01 6.952E-01 1. 447E+OO FAIL ABUN RE-183 1.17 5E-02 1. 620E+OO 3.234E+OO FAIL ABUN RE-184 1.190E+01 2.907E+Ol 5.578E+Ol FAIL ABUN W-188 4.785E+Ol 9.976E+Ol 1.976E+02 FAIL ABUN IR-192 7.654E-02 3. 8 65E-01 7.803E-01 FAIL ABUN HG-203 -l.326E-02 2.120E+OO 4.222E+OO FAIL ABUN BI-207 2.323E-02 3. 724E-02 8.0lOE-02 FAIL ABUN BI-211 O.OOOE+OO 4.586E-01 6.803E-01 FAIL ABUN PB-211 -1.684E-01 5.093E-01 9.648E-01 NOT IDENT. BI-212 O.OOOE+OO 8. 728E-01 1.043E+OO FAIL ABUN RN-219 -6.253E-02 2.896E-01 5.558E-01 FAIL ABUN RA-223 -2.036E-01 4. 961E-01 8.402E-01 FAIL ABUN RA-224 O.OOOE+OO 7.768E-01 l.223E+OO FAIL ABUN AC-227 3.791E-02 1.769E-01 3.602E-01 FAIL ABUN TH-227 3.791E-02 1.769E-01 3.602E-01 FAIL ABUN TH-229 l.694E-01 3.792E-01 7.245E-01 FAIL ABUN TH-231 -2.036E-01 4. 961E-01 8.402E-01 FAIL ABUN PA-233 -3.877E-02 4.164E-02 7.577E-02 *FAIL ABUN PA-234 -l.719E-01 2.017E-01 3.534E-01 FAIL ABUN PA-234M 8.732E-01 3.256E+OO 6.693E+OO NOT IDENT. NP-237 -3.877E-02 4.164E-02 7.577E-02 FAIL ABUN NP-238 O.OOOE+OO l.915E+41 O.OOOE+OO SHORT HLIF NP-239 1. 071E-01 l.685E-01 3.395E-01 NOT IDENT. PU-239 O.OOOE+OO 4.339E+02 4.530E+02 FAIL ABUN AM-241 -1. 913E-02 7.794E-02 1.409E-01 NOT IDENT. CM-243 -3.200E-02 6.561E-02 l.221E-01 NOT IDENT. BK-247 -l.725E-02 5. 2.35E-02 1.025E-01 NOT IDENT. CM-247 3.584E-03 2. 661E-02 5.293E-02 NOT IDENT. CF-249 9 .104E-03 2.940E-02 5.940E-02 NOT IDENT. CF-251 -2.734E-02 l.003E-01 1.810E-01 NOT IDENT. Page 3833 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:23:49.59 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 407 10.66* 1.403E+OO l.202E+Ol l.202E+Ol 10.14 C0-56 846.77 8 99.94* 2.182E+OO l.621E-02 2. 572E-01 134.83 1037.84 ------14.17 1. 8 63E+OO ------Line Not Found ------1238.28 31 66.90 1.617E+OO l.282E-01 2.033E+OO 69.84 1771.35 ------15.47 1. l 72E+OO ------Line Not Found ------CD-109 88.03 86 3.70* 7.559E+OO 1.364E+OO 2.167E+OO 83.01 SN-126 64.28 52 9.60 5.534E+OO 4.297E-01 4.297E-01 127.75 86.94 86 8.90 7.559E+OO 5. 672E-01 5.672E-01 83.01 87.57 86 37.00* 7.559E+00 l.364E-01 1.364E-01 83.01 BA-137M 661.66 19 89.90* 2.620E+OO 3.503E-02 3.572E-02 187.70 CS-137 661.66 19 85.10* 2. 620E+'oo 3.701E-02 3.773E-02 187.70 TL-208 277.37 ------6.60 5.132E+OO ------Line Not Found ------583.19 171 85.00* 2.885E+OO 3.083E-01 3.083E-01 25.31 860.56 30 12.50 2.153E+OO 4.920E-01 4.920E-01 59.57 PB-210 46.54 28 4.25* 2.754E+OO l.042E+00 1.070E+OO 230.61 BI-211 72. 87 49 1.23 6.59.2E+OO 2.686E+OO 2.686E+OO 136. 52 351. 06 367 12.92* 4.262E+OO 2.945E+OO 2.945E+OO 15.89 PB-212 74.82 225 10.28 6.772E+OO 1.424E+00 1.424E+OO 3'0. 20 77 .11 395 17.10 6.937E+OO 1.470E+OO 1.470E+00 20.11 238.63 497 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 300.09 64 3.30 4.823E+OO 1. 763E+OO 1. 763E+OO 54.55 BI-214 609.32 222 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 1120.29 67 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 1764.49 26 15.30 1. l 77E+OO 6.303E-01 6.305E-01 58.08 PB-214 74.82 225 5.80 6. 772E+OO 2.524E+OO 2. 52*5E+OO 30.20 77 .11 395 9.70 6.937E+OO 2.591E+OO 2.592E+OO 20 .11 87.09 86 . 3. 41 7.559E+00 1.480E+OO l.481E+OO 83.01 242.00 109 7.25 5.693E+00 l.163E+OO l.164E+OO 38.53 295.22 241 18.42 4.885E+OO l.180E+OO 1.180E+00 22.14 351. 93 367 35.60* 4.262E+OO 1.069E+OO l.069E+00 15.89 RN-222 609.32 222 45.49* 2.791E+OO 7. 732E-01. 7.735E-01 21. 38 1120. 29 67 14.92 1. 754E+OO l.129E+00 1.129E+OO 32.27 1764.49 26 15.30 l.177E+OO 6.303E-01 6.305E-01 58.08 RA-224 240.99 109 4.10* 5.693E+OO 2.057E+OO 2.057E+OO 38.53 RA-226 609.32 222 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 1120.29 67 14.92 1. 754E+OO l.129E+OO 1.129E+OO 32.27 1764.49 26 15.30 1.177E+OO 6.303E-01 6.305E-01 58.08 AC-228 105.21 ------1.10 8.060E+OO ------Line Not Found ------338.32 106 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 794.95 ------4.25 2.286E+00 ------Line Not Found ------835.71 ------1. 61 2. 201E+OO ------Line Not Found ------911. 20 94 25.80* 2.060E+OO 7.786E-01 *7.786E-01 37.20 968.97 57 15.80 1. 964E+OO 8 .137E-01 8.137E-01 58.83 RA-228 105.21 ------1.10 8.060E+OO ------Line Not Found ------338.32 106 11.27 4.399E+OO 9.435E-01 9.435E-01 40.20 794.95 ------4.25 2.286E+OO ------Line Not Found ------835.71 ------1. 61 2.201E+OO ------Line Not Found ------Page 3834of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : Gl203621355 Acquisition date 3-0CT-2016 09:21:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 94 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 968. 97 57 15.80 l.964E+OO 8.137E-01 8.137E-01 58.83 TH-228 74.82 225 10.28 6. 772E+OO 1. 424E+OO l.424E+OO 30.20 77 .11 395 17.10 6.937E+OO 1. 470E+OO 1.470E+OO 20 .11 238.63 497 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 300.09 64 3.30 4.823E+OO 1. 763E+OO 1.763E+OO 54.55 TH-230 609.32 222 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 1120.29 67 14.92 1. 754E+OO l.129E+OO l.129E+OO 32.27 1764.49 26 15.30 1.177E+OO 6.303E-01 6.303E-01 58.08 PA-231 283.69 ------1. 70 5.044E+OO ------Line Not Found ------301.36 64 5.35* 4.823E+OO 1.087E+OO 1.087E+OO 54.55 TH-232 105.21 ------1.10 8.060E+OO ------Line Not Found ------338.32 106 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 835. 71 ------1. 61 2.201E+OO ------Line Not Found ------911. 20 94 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 968.97 57 15.80 1. 964E+OO 8.137E-01 8 .137E-01 58.83 TH-234 63.29 52 3.70* 5.534E+OO 1.115E+OO 1.115E+OO 127.75 92.59 61 4.23 7.793E+OO 8.209E-01 8.209E-01 121. 48 U-234 609.32 222 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 1120.29 67 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 1764.49 26 15.30 1.177E+OO 6.303E-01 6.303E-01 58.08 U-235 89. 96 81 3.47 7.683E+OO 1.346E+OO 1.346E+OO 43.58 93.35 61 5.60 7.793E+OO 6. 201E-01 6. 201E-01 121.48 143.76 19 10.96* 7.743E+OO l.OOlE-01 1. OOlE-01 207.10 163.33 9 5.08 7.318E+OO l.089E-01 l.089E-01 574.18 185.72 88 57.20 6.810E+OO 9.991E-02 9.991E-02 60.79 205.31 ------5.01 6.393E+OO ------Line Not Found ------U-238 63.29 52 3.70* 5.534E+OO 1.115E+OO 1.115E+OO 127.75 92.59 61 4.23 7.793E+OO 8.209E-01 8.209E-01 121. 48 AM-243 43.53 ------5.90 2.021E+OO ------Line Not Found ------74.66 225 67.20* 6.772E+OO 2.179E-01 2.179E-01 30.20 ANH-511 511.00 82 100.00* 3.191E+OO 1.133E-01 l.133E-01 58.16 Flag: "*" Key line Page 3835 of 5809 Summary of Nuclide Activity Sample ID : G1203621355 Acquisition date Page : 3 09:21:06 Total number of lines in spectrum .51 Number of unidentified lines 9 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 C0-56 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH..,.234 U-234 U-235 U-238* AM-243 ANH-511 Hlife l.25E+09Y 77.23D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+'l0Y l.41E+10Y 1. 41E+lOY* 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 15.9 1. 59 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Uncorrected pCi/GRAM l.202E+Ol l.621E-02 l.364E+OO 1. 364E-01 -3.503E-02 3. 701E-02 3.083E-01 l.042E+OO 2.945E+OO 8.762E-01 7.732E-01 l.069E+OO 7.732E-01 2.057E+OO 7.732E-01 7.786E-01 7.786E-01 8.762E-01 7.732E-01 l.087E+OO 7.786E-01 l .115E+OO 7.732E-01 1.00lE-01 l .115E+00 2.179E-01 l.133E-01 Total Activity 3.273E+Ol Grand Total Activity . 3.273E+Ol Decay Corr pCi7GRAM 1.202E+Ol 2.572E-01 2.167E+OO 1.364E-01 3. 572E-02 3.773E-02 3.083E-01 l.070E+OO 2.945E+OO 8.762E-01 7.735E-01 1. 069E+OO 7.735E-01 2.057E+OO 7.735E-01 7.786E-01 7.786E-01 8.762E-01 7.732E-01 1.087E+OO 7.786E-01 l .115E+00 7.732E-01 1. OOlE-01 1.115E+OO 2.179E-01 1.133E-01 3.381E+Ol 3.381E+Ol 82.35% Decay Corr 2-Sigma Error 0.122E+Ol 3.468E-01 1. 799E+OO l.133E-01 6.704E-02 7.082E-02 0.780E-01 2.467E+OO 0.468E+OO 1.37.4E-01 l.654E-01 0.170E+00 1.654E-01 0.793E+OO 1.654E-01 2.896E-01 2.896E-01 1.374E-01 l.653E-01 0.593E+OO 2.896E-01 1.424E+OO
1.653E-01 2.073E-01 1.424E+OO 0.658E-01 0.659E-01 Manually accepted 2-Sigma %Error 10.14 134.83 83.01 83.01 187.70 187.70 25.31 230.61 15.89 15.68 21. 38 15.89 21. 38 38.53 21. 38 37.20 37.20 15.68 21. 38 54.55 37.20 127.75 21. 38 207.10 127.75 30.20 58.16 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 3836 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : Gl203621355 Acquisition date : 3-0CT-2016 09:21:06 . It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 128.35 66 140 2.38 '256.06 252 8 1. 39E-02 76.5 8.00E+OO T 0 209.11 58 96 0.85 417.64 415 8 l.29E-02 71.1 6.31E+OO 0 225.87 24 67 1. 27 451.18 449 6 5.45E-03 **** 5.98E+OO T 0 270.69 51 85 2.21 540.85 536 11 1.16E-02 83.4 5.23E+OO T 0. 328.98 18 90 1. 29 657.49 651 10 4.26E-03 **** 4.49E+OO T 0 463.97 23 81 3.36 927.58 919 13 5.57E-03 **** 3.44E+OO T 0 491. 06 19 23 1. 56 981. 79 979 9 4.68E-03 **** 3.29E+oo* T 0 642.39 17 19 1. 60 1284.60 1279 9 4.26E-03 **** 2.68E+OO 0 728. 29 41 44 1. 82 1456.48 1448 15 1.05E-02 80.6 2.44E+OO T 0 742.43 29 13 0.81 1484.78 1480 10 7.42E-03 62.7 2.41E+OO 0 881.21 16 18 3.68 1762.50 1754 14 4.12E-03 **** 2. llE+OO T 0 893.41 73 27 15.20 1786.90 1773 33 l.93E-02 49.8 2.09E+OO T 0 927.40. 24 14 4.86 1854.93 1846 15 6.46E-03 83.0 2.03E+OO T 0 1126.44 10 6 1. 44 2253.27 2250 8 2.72E-03 **** 1.75E+OO 0 1177.68 15 2 0.98 2355.81 2352 8 4 .13E-03 61. 6 1. 68E+OO T 0 1180.97 13 2 0.76 2362.41 2359 8 3. 72E-03 65.1 1.68E+OO 0 1193.17 10 17 3.36 2386.82 2379 10 2.79E-03 **** 1.67E+OO 0 1279.23 12 1 0.64 2559.04 2556 8 3.22E-03 71. 2 1.57E+OO 0 1297.27 6 16 2.86 2595.15 2585 13 1.66E-03 **** 1.55E+00 T 0 1364.61 4 6 1. 23 2729.93 2722 9 1.19E-03 **** 1. 49E+OO T 0 1376.86 31 0 1. 21 2754.45 2747 14 8.61E-03 35.9 1. 48E+OO 0 1409.66 17 3 3.28 2820.10 2813 14 4.94E-03 64.8 1.45E+OO Flags: "T" = Tentatively associated Page 3837 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:24:13.77 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: *
Acquisition date 3-0CT-2016 09:21:06 Sensitivity 3.000 *
Detector ID GAM27 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.94 Half life ratio : ***** *
Sample date 10:40:00 Nuclide Library : SOLID *
Sample ID G1203621355 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7010E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;l3
Combined Critical Level Report NOTE: Not* all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-56 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-214 PB-214 RN-222 RA-226
AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 754E-01 3.057E-01 7.742E-01 4.887E-02 2.224E-02 2.349E-02 1. 967E-02 8.441E-01 3.785E-02 4.468E-02 4.105E-02 4.468E-02 4.468E-02 8.052E-02 8.052E-02 3.785E-02 4.467E-02 2.748E-01 8.052E-02 5.997E-01 4.466E-02 l.183E-01 5.997E-01 2.732E-02 l.874E-02 ----Non-Identified Nuclides Nuclide BE-7 .NA-22 NA-24 AL-26 SC-46 V-48 Page 3838 of 5809 \ Le (pCi/GRAM 9.383E+00 2.900E-02 O.OOOE+OO l.802E-02 3.068E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3839 of 5809 O.OOOE+OO 4. 715E-02 O.OOOE+OO 3.086E-02 3.546E-Ol 5. ll 7E+OO 2.205E-02 l.OlOE-01 2.024E+OO 3.625E+OO O.OOOE+OO 1.434E-01 O.OOOE+OO O.OOOE+OO 4.673E-01 4.862E+OO 5.594E-01 O.OOOE+OO l.305E-01 3.492E+02 1. 889E-02 4. 7 51E-01 1. 745E+OO 1.244E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.228E-02 4.330E-02 4.212E+OO 4.055E-01 4.055E-01 1. 743E-02 5.466E-02 1. 466E-01 O.OOOE+OO O.OOOE+OO 9.770E-02 1.627E+OO 6.843E-02 2.073E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.478E-02 O.OOOE+OO 3.444E-02 8.165E-02 O.OOOE+OO O.OOOE+OO 8.129E-02 O.OOOE+OO O.OOOE+OO L 951E+bl O.OOOE+OO 2.393E-01 3.987E-02 3.471E+OO *. 2.288E-02 O.OOOE+OO 5.173E+02 0. O'OOE+OO l.608E-02 6.030E-02 l.039E-01 7.033E-02 7.322E-02 1.182E+OO 4.183E-02 7.333E+OO l.354E-01 5.023E-02 l.468E-02 2.978E+00 SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 6.345E-01 FAIL ABUN RE-183 1.532E+OO FAIL ABUN RE-184 2.467E+Ol FAIL ABUN W-188 9.201E+Ol FAIL ABUN IR-192 3.604E-01 FAIL ABUN HG-203 1. 962E+OO FAIL ABUN BI-207 3.550E-02 FAIL ABUN BI-211 3.288E-01 FAIL ABUN PB-211 4.388E-01 NOT IDENT. BI-212 4.835E-01 FAIL ABUN RN-219 2.531E-01 FAIL ABUN RA-223 3.852E-01 FAIL ABUN RA-224 5.843E-01 FAIL ABUN AC-227 1.678E-01 FAIL ABUN TH-227 FAIL ABUN TH-229 3.404E-01 FAIL ABUN TH-231 3.852E-01 FAIL ABUN PA-233 3.437E-02 FAIL ABUN PA-234 l.512E-01 FAIL ABUN PA-234M 2. 967E+OO NOT IDENT. NP-237 3.437E-02 FAIL ABUN NP-238 O.OOOE+OO SHORT HLIF NP-239 1. 596E-01 NOT IDENT. PU-239 2.136E+02 FAIL ABUN AM-241 6.676E-02 NOT IDENT. CM-243 5.705E-02 NOT IDENT. BK-247 4. 725E-02 NOT IDENT. CM-247 2. 419E-02' . NOT IDENT. CF-249 2.728E-02 NOT IDENT. CF-251 8.517E-02 NOT IDENT. Page 3840 of 5809 . VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:24:20.53 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621355.CNF;l *
Acquisition date
3-0CT-2016 09:21:06 Sensitivity : 3.000 *
Detector ID GAM27 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.94 Half life ratio : ***** *
Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
Sample ID G1203621355 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity 1.7010E+02 GRAM *
Quantity Err(%) 1.1758E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;l3 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 C0-56 -CD-109 SN-126 BA-137M CS-137 TL-208 PB-210* PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-23'5 U-238 AM-243 ANH-511 l.202E+Ol 2. 572E-01 4.465E-01 2. 811E-02 3. 572E-02 3.773E-02 3.083E-01 l.070E+OO 8.762E-01 7.735E-01 1.069E+OO 7.735E-01 7.735E-01 7.786E-01 7.786E-01 8.762E-01 7.732E-01 l.087E+OO 7.786E-01 1.115E+OO 7.732E-01 l.OOlE-01 1.115E+OO l.164E-01 1.133E-01 Act Error (1.96-sigma) 1.349E+OO 3.400E-01 1.805E+OO l .136E-01 6. 572E-02 6.943E-02 7.759E-02 2.419E+OO 1. 426E-01 1*. 655E-01 1.725E-01 l.655E-01 l.655E-01 2.866E-01 2.866E-01 1.426E-01 l.654E-01 6.261E-01 . 2.866E-01 1.417E+OO 1.654E-01 2.032E-01 l.417E+OO 6.878E-02 6.477E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3841of5809 Key-Line Activity (pCi/GRAM 3.678E+OO 2.007E-02 l.OOOE+41 l.348E-03 1. 969E-01 K.L Act error ( 1. 96-sigma) l.018E+Ol 3.275E-02 l.246E+41 2.044E-02 3.187E-01 TPU (1.96-sigma) 1.349E+OO 3.400E-01 1.805E+OO 1.136E-01 6.572E-02 6.943E-02 7.759E-02 2.419E+OO 1. 426E-01 1.655E-01 1. 725E-01 l.655E-01 1.655E-01 2.866E-01 2.866E-01 l.426E-01 1.654E-01 6.261E-01 2.866E-01 1.417E+OO 1.654E-01 2.032E-01 1.417E+OO 6.878E-02 6.477E-02 TPU ( 1. 96-sigma) l.031E+Ol 3.398E-02 O.OOOE+OO 2.045E-02 3.308E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 -7.696E+03 1.530E+04 1.569E+04 SHORT HLIF CR-51 -1.543E+Ol 3.922E+02 3.923E+02 SHORT HLIF MN-54 2.301E-02 4.983E-02 5.090E-02 NOT IDENT. 'MN-56 l.OOOE+41 1.322E+41 O.OOOE+OO SHORT HLIF C0-57 -4.736E-03 3.484E-02 3.490E-02 NOT IDENT. C0-58 -1. 97 6E-01 4.287E-01 4.379E-01 NOT IDENT. FE-59 -3.122E+OO 6.413E+OO 6.566E+OO NOT IDENT. C0-60 3.445E-03 2.518E-02 2.523E-02 NOT IDENT. ZN-65 4.042E-03 l.320E-01 1.320E-01 NOT IDENT. GE-68 2.096E+OO 2.039E+OO 2.247E+00 NOT IDENT. AS-73 -1.544E+OO 3.942E+OO 4.003E+OO NOT IDENT. AS-74 5.615E+03 5.806E+03 6.333E+03 SHORT HLIF SE-75 -6.294E-02 l.598E-01 l.623E-01 NOT IDENT. BR-77 1. 681E+39 l.495E+40 O.OOOE+OO SHORT HLIF SR-82 9.295E+02 6.982E+02 8.143E+02 SHORT HLIF RB-83 3.257E-02 5.307E-01 5.309E-01 NOT IDENT. KR-85 7.659E-01 6 .101E+*oo 6. lllE+OO NOT IDENT. SR-85 8.767E-02 7.020E-01 7.031E-01 NOT IDENT. RB-86 3.506E+04 3.199E+04 3.568Ef04 SHORT HLIF Y-88 2.683E-02 1.421E-01 , 1. 426E-01 NOT IDENT. Y-91 -3.144E+02 4.621E+02 4.834E+02 NOT IDENT. NB-94 -2.081E-02 2.565E-02 2. 731E-02 NOT IDENT. NB-95 -9.650E-01 7.407E-01 8.590E-01 NOT IDENT. NB-95M -4.666E-01 2.107E+OO 2 .118E+OO NOT IDENT. ZR-95 7.913E-01 1.365E+OO 1. 411E+OO NOT IDENT. *NB-97 l.000E+41 2.440E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.000E+41 6.698E+41 O.OOOE+OO SHORT HLIF M0-99 5.807E+32 l.140E+33 O.OO'OE+OO SHORT HLIF TC-99M 1.000E+41 1. 696E+41 O.OOOE+OO SHORT HLIF RH-101 6.413E-02 4.945E-02 5.728E-02 FAIL ABUN RH-102 2.394E-02 4.716E-02 4.838E-02 NOT IDENT. RU-103 1.021E+OO 4.657E+OO 4.679E+OO FAIL ABUN RH-106 7.037E-02 4.641E-01 4.652E-01 NOT IDENT. RU-106 7.037E-02 4.641E-01 4.652E-01 NOT IDENT. AG-108M -1.534E-02 2.186E-02 2.293E-02 NOT IDENT. AG-llOM 3.414E-03 9.427E-02 9.429E-02 NOT IDENT. SN-113 -l.954E-02 l.656E-01 1.659E-01 NOT IDENT. CD-115 -4.280E+39 3.294E+40 O.OOOE+OO SHORT HLIF SN-117M 4.373E+04 1.142E+05 l.158E+05 SHORT HLIF TE-123M 6.327E-02 1.059E-01 1. 096E-01 NOT IDENT. SB-124 6.668E-01 1. 779E+OO l.804E+OO NOT I DENT*. SB-125 1.810E-02 7.460E-02 7.505E-02 FAIL ABUN TE-125M 1.075E+02 2. 211E+o2 2.263E+02 NOT IDENT. I-126 8.075E+04 1.049E+06 l.050E+06 SHORT HLIF SB...:126 -2.045E+05 1. 521E+06 l.524E+06 SHORT HLIF SB-127 2.156E+21. 8.694E+22 0.000E+OO SHORT HLIF I-131 -3.985E+09 7.299E+09 7.517E+09 SHORT HLIF I-132 -l.000E+41 1.905E+42 O.OOOE+OO SHORT HLIF TE-132 9.226E+25 1. 819E+27 O.OOOE+OO SHORT HLIF BA-133 -3.907E-02 3.502E-02 3.920E-02 NOT IDENT. I-133 1.000E+41 l.497E+42 SHORT HLIF CS-134 1.935E-02 3. 801E-02 3.900E-02 FAIL ABUN CS-135 -3.494E-02 l.022E-01 l.034E-01 NOT IDENT. I-135 -1.000E+41 7.173E+41 O.OOOE+OO SHORT HLIF CS-136 4.882E+04 3.398E+05 3.406E+05 SHORT HLIF CE-139 2.436E-02 9.851E-02 9.912E-02 NOT IDENT. BA-140 3.266E+05 l.615E+06 1. 621E+06 SHORT HLIF LA-140 -3.715E+05 5.441E+05 5.693E+05 SHORT HLIF CE-141 2.469E+Ol 2.490E+Ol NOT IDENT. CE-143 -l.OOOE+41 2 .110E+41 O.OOOE+OO SHORT HLIF CE-144 6.426E-02 2.633E-01 2.649E-01 NOT IDENT. PM-144 8.028E-03 4 .. 591E-02 4.606E-02 NOT IDENT. PR-144 -2.579E-01 4.136E+OO 4.138E+OO NOT IDENT. PM-146 -1. 331E-02 2.791E-02 2.854E-02 NOT IDENT. ND-147 -7.226E+06 4 .112E+07 4.125E+07 SHORT HLIF PM.'...14 7 -1. 7 48E+02 5. 921E+02* 5.973E+02 NOT IDENT. PM-149 -l.OOOE+41 l.332E+41 O.OOOE+OO SHORT HLIF EU-150 6.773E-03 l.866E-02 1. 8 91E-02 FAIL ABUN ED-152 -2 .135E-02 6.861E-02 6.928E-02 NOT IDENT. GD-153 -1.419E-01 1.256E-01 l.410E-01 NOT IDENT. EU.:...154 3.377E-02 8.419E-02 8.555E-02 NOT IDENT. EU-155 6.871E-02 7.557E-02 8.167E-02 FAIL ABUN TB-160 -4.399E-01 l.406E+OO 1.420E+OO FAIL ABUN H0-166M 1. 746E-02 4.678E-02 4.744E-02 NOT IDENT. TM-171 -8.480E-01 7.778E+00 7.787E+OO NOT IDENT. HF-172 -l.107E-01 1.77£\E-01 1.843E-OI FAIL ABUN LU-172 l.076E-02 5. 611E-02 5.632E-02 FAIL ABUN LU-176 -1. 847E-02 1. 788E-02 1.972E-02 FAIL ABUN Page 3842 of 5809 HF-181 l.264E+OO 3 .196E+OO 3.246E+OO NOT IDENT. TA-182 2.691E-01 6.952E-01 7.057E-01 FAIL ABUN RE-183 l.175E-02 l.620E+OO l.620E+OO FAIL ABUN RE-184 l.190E+Ol 2.921E+Ol 2.970E+Ol FAIL ABUN W-188 4 .. 785E+Ol 9. 991E+Ol l.022E+02 FAIL ABUN IR-192 7.654E-02 3.865E-01 3.880E-01 FAIL ABUN HG-203 -l.326E-02 2.120E+00 2.120E+OO FAIL ABUN BI-207 2.323E-02 3.725E-02 3.870E-02 FAIL ABUN BI-211 2.945E+OO 4.775E-01 l.411E+OO FAIL ABUN PB-211 -l.684E-01 5.094E-01 5.150E-01 NOT IDENT. BI-212 l.105E+00 8.746E-01 l.007E+OO FAIL ABUN RN-219 -6.253E-02 2.897E-01 2. 911E-01 FAIL ABUN RA-223 -2.036E-01 4. 962E-01 5.047E-01 FAIL ABUN RA-224 2.057E+OO 7.847E-01 l.215E+OO FAIL ABUN AC-227 3.791E-02 l.770E-01 l.778E-01 FAIL ABUN TH-227 3.791E-02 l.770E-01 l.778E-01 FAIL ABUN TH-229 l.694E-01 3.793E-01 3.869E-01 FAIL ABUN TH-231 -2.036E-01 4. 962E-01 5.047E-01 FAIL ABUN PA-233 -3.877E-02 4.169E-02 4.520E-02 FAIL ABUN PA-234 -l.719E-01 2.817E-01 2.922E-01 *FAIL ABUN PA'--234M 8.732E-01 3.256E+OO 3.280E+OO NOT IDENT. NP-237 -3.877E-02 4.169E-02 4.520E-02 FAIL ABUN NP-238 -l.OOOE+41 l.916E+41 0.000E+OO SHORT HLIF NP-239 1. 071E-01 l.687E-01 l.755E-01 NOT IDENT. PU-239 5.790E+02 4.346E+02 5.070E+02 FAIL ABUN AM-241 -l.913E-02 7.795E-02 7.843E-02 NOT IDENT. CM-243 -3.200E-02 6.568E-02 6.724E-02 NOT IDENT. BK-247 -1. 725E-02 5:246E-02 5.304E-02 NOT IDENT. CM-247 3.584E-03 2.662E-02 2.667E-02 NOT IDENT. CF-249 9.104E-03 2. 941E-02 2.970E-02 NOT IDENT. CF-251 -2.734E-02 l.004E-01 1. OllE-01 NOT IDENT. Page 3843 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 75.5737 87.09 145.1000 136.47 86.1691 45.60 65.5803 87.57 145.2323 140.51 0.0000 46.54 65.7580 88.03 145.3587 143.76 80.1685 49.72 0.0000 88.34 109.0829 144.24 90.1517 51. 35 80.1621 88.47 109.1099 145.44 84.1762 51. 87 78.3396 89. 96 108. 0118 152.43 77.6201 52.39 74.5741 -1093. 63 108.1489 153.25 0.0000 52.97 86.3281 91.11 0.0000 323.87 73.1543 53.44 94.2045 92.59 108.5374 156.02 0.0000 54.07 97.2776 93.35 108.6886 158.56 0.0000 57.36 0.0000 94.56 80.6340 159.00 67.7617 57.53 116.7861 94.65 80.6468 162.33 79.7767 57*. 98 107.0919 94.67 80.6497 162.66 0.0000 59.27 116.9610 80.6790 163.33 81. 0510 59.32 116.9755 97.43 105.5757 165.86 73.8410 59.54 117.0384 98.43 76.9175 176.31 94.2609 60. 96 113.4834 98.44 76.9191 176.60 0.0000* 61.17 114.8610 99.53 74.9251 177.52 93.1999 62.93 114.3490 100 .11 70.7146 181.07 0.0000 63.29 114. 4455 102.03 77.3992 181.52 89.6317 63.58 114.5236 103.18 80.7827 184.41 83.5045 64.28 121. 0283 103.37 80.8084 143.76 91. 6706 66.73 120.3735 105.21 71. 3330 193.51 69.3522 67.24 135.5768 105.31 71. 3446 197.03 81.8331 125.81 126.6643 106.12 85.5130 198.01 62.3570 67.75 126.6835 106.47 93.1446 201.83 65.0693 69.67 125.2081 109.28 81.6084 203.43 82.3974 70.83 137.6747 111. 00 80.7455 205.31 59.1482 72.81 116. 9153 111. 76 0.0000 210.85 69.4061 72.87 116. 9302 114. 06 71. 2740* 215.65 63.5212 74.66 117.3768 116. 30 0.0000 222 .11 70.2034 74.82 117.4163 116.74 67.1711 227.09 65.5102 74.97 117.4532 119. 76 70.8052 227.38 59.2276 77 .11 117.9778 121.12 7 5 .. 3872 228.16 0.0000 78.74 126.2642 121. 22 78.7250 228.18 60.5354 79.69 89.3810 121.78 81. 0117 116.74 60.5354 80.12 99.0923 122.06 77.7155 235.69 71.1382 80.19 0.0000 122.92 77.8165 235. 96 67.3450 80.57 99.1816 123.07 68.9388 238.63 73.8850 81. 00 103.4035 265.00 62.3245 238.98 0.0000 81. 07 98.2471 125.81 80.3870 240.99. 102.1375 81. 75 115. 9854 127.23 70.4862 242.00 46.0052 83.79 109.5202 127.91 70.5571 244.70 49.9646 84.00 109.5652 129.30 77.8075 252.40 0.0000 85.43 125.1682 131. 20 76.5228 252.80 55.9301 86.55 133.7998 133.02 83.4928 254.15 0.0000 86.79 145.0164 133.52 72.2607 256.23 57.8293 86.94 145.0577 136.00 73.6487 260.90 0.0000 Page 3844of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY -MDA COUNTS 264.66 54.7853 355.39 0.0000 584.27 20.2463 264.80 356.01 43.4348 595.83 0.0000 265.00 53.0623 364.49 0.0000 427.87 26.8483 268.22 45.7965 366.42 0.0000 602.52 0.0000 269.46 47.1555 372.51 30.2337 604.72 40.3503 270.03 47.1786 375.05 40. 6966 607.14 22.6218 271.23 47.2269 377.52 35.0759 609.32 28.0365 273.65 0.0000 .356.01 39.0331 610.33 28.0492 276.40 57.0998 388.16 37.2354 614.28 14.5909 277.37 43.9585 388.63 0.0000 618.01 25.9844 277.60 43. 9677 391.69 30.6230 620.36 23.8441 278.00 51.0190 264.66 42.3520 621. 93 31.4544 279.20 58 .1152 401. 81 38.5303 630.19 0.0000 279.54 59.0135 402.40 35.6541 631.29 20.6954 279.70 58.1394 404.85 39.5711 633.25 20.7140 280.46 55.5326 410.95 40.6935 634.78 0.0000 283.69 45.0764 413.71 39.7938 635.95 .22.9226 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.2228 423. 72 0.0000 645.85 13.1567 285.90 0.0000 427.09 38.1677 657.76 21.4924 287.50 47.8795 427.87 27.4155 657.90 0.0000 290.67 51.2039 433.94 3'7. 3452 661.66 23.1849 293.27 0.0000 439.40 31. 5521 664.57 0.0000 351. 93 45'. 504 9 453.88 24.8622 6'66.33 0.0000 295. 96 45.5329 463.37 32.9993 666.50 0.0000 879.38 34.8923 468.07 33.0886 667.71 0.0000 299.98 44.3367 473. o*o 0.0000 677.62 21.1222 300.09 44.3397 475.06 35.2336 685.70 0.0000 300 .13 44.3417 476.78 26.1989 695.00 0.0000 301.36 41.6950 477.60 25.2029 696. 49 24.6542 302.85 43.0908 482.18 18.1930 696. 51 28.0162 256.23 39.1024 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 36.9934 306.78 54.0320 497.08 22.4194 697.49 36.9961 308.46 35.1668 505.52 27. 6411 702.65 31.4590 311. 90 47.9191 507.63 0.0000 706.68 19.1319 316.51 45.3674 511. 00 30.8029 711. 68 20.2991 319.41 0.0000 514.00 32.3947 720.70 0.0000 320.08 0.0000 514.00 32.3947 721. 93 0.0000 321.04 41. 8831 520.40 25.7975 722.78 23.7908 323.87 -49.2726 520.69 0.0000 722. 91 23.7916 325.23 28.7718 522.65 0.0000 723.31 18. 6968 328.76 0.0000 527.90 0.0000 724.19 18.7035 333.37 35.8397 528.26 25.9033 727.33 23.8344 333.97 31. 7184 529.59 23.8479 733.00 17.0636 334.37 40.0042 529.87 0.0000 735.93 26.1951 338.28 43.3473 5'31. 02 0. 0000 ' 333.97 13.6753 338.32 43.3482 537.26 0.0000 739.50 0.0000 311. 90 40.1839 546.56 0.0000 747.24 25.7419 340.48 40.1839 552.55 26.2278 748.06 20.6001 340.55 0.0000 563 *. 25 16.8757 752.31 21.7809 344.28 42.6103 569.33 31.7371 753.82 0.0000 345.93 34. 4996 946.00 31.7395 756.73 20.6704 351.06 32.5782 569.70 31.7419 756.80 20. 6711 351.93 32.5989 583.19 20.2362 884.68 19.5774 Page 3845 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 32.2679 1274.44 18.7335 1620.50 3.2950 766.42 27.6650 1001.03 13.1331 1621.92 8.7896 766.84 25.3641 1002.74 18.7720 1678.03 0.0000 772. 60 0.0000 1004.73 15. 9660 1690.97 4.4578 776.52 0.0000 . 507. 63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.6189 778.90 25.4823 1028.54 0.0000 1063.66 15.3979 783.70 0.0000 1037.84 26.5662 1771.35 3.3973 785.37 17.4170 1038.76 0.0000 1791.20 0.0000 792.07 18.6257 631.29 23.7839 1808.65 3.6500 794.95 13.9844 1048.07 0.0000 1810.72 0.0000 795.86 16.3208 1049.04 12.3763 1836.06 2.7519 810.06 19.3380 1050.41 19.0491 810.29 19.3393 1063.66 13.3873 344.28 19.3406 1077.00 0.0000 810.76 18.4634 1077.34 13.4412 815.77 0.0000 1085.87 12.5128 1048.07 0.0000 1093.63 13.5061 832.01 26.5833 1099.45 22.2251 834.85 18.6275 1112. 07 10.6683 835. 71 23.9571 1112.84 12. 6112 836.80 0.0000 1115. 54 12.4266 846.75 0.0000 1120.29 13. 6104 846. 77 15.6788 1120.55 13. 6112 856.80 0.0000 1221.41 12.9655 860.56 14.3237 1129. 67 18.7148 871.09 17.0726 1131. 51 0.0000 873 .. 19 17.4708 1147.95 875.33 0.0000 1173.23 7.8936 879.38 17 .1225 1177.95 11. 0653 880.51 17.1289 1189.05 17.4410 883.24 14.4380 1204.77 21.8939 884.68 10.8340 1221.41 12.9952 889.28 15.3725 1231. 02 22.4492 894.76 15.4016 1235.36 0.0000 898.04 15.4187 1238.28 19.0777 900. 72 15.4332 1260.41 0.0000 903.28 14.5381 1271.87 11.1423 911.20 16.3993 1274.44 8.1089 912.08 16.4042 1274.54 6. 4871 923.98 0.0000 1291.59 14.6602 926.50 21. 9785 1298. 22. 0.0000 929 .11 17.5980 1312.11 0.0000 937.49 20.2202 1332.49 7.2000 944.13 0.0000 1362.66 0.0000 946.00 21.1989 1365.19 3.3180 949.00 15.6838 1368.63 0.0000 667.71 0.0000 1384.29 6.2498 962. 31 21. 3119 1408.01 5.2377 964.08 17.8008 1457.56 0.0000 966 .17 26.7196 1460.82 6.3629 911.20 18. 5718 1489.16 8.5391 968. 97 18. 5718 1505.03 10.7117 983.53 0.0000 1584.12 9.8091 984.45 0.0000 1596.21 0.0000 Page 3846 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:26:31.23 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621356.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 09:11:02. Sample ID G1203621356 Sample quantity : 1.15000E+02 GRAM Detector name : GAM06 Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:04.89 0.5% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 0 9 ' 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy* 37.09 45.10 46.51* 51.85 59.50 88.00 122.28 164.58 167.41 225.90 284.90 385.80 661. 30 739.32 891.33 996. 25 1086.07 1115. 01 1162. 31 1172.54 1331.69 1351. 56 1398.56 1484.54 1548.58 1585.08 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 94 450 5038 142 14909 2482 298 98 39 80 66 72 11854 61 42 42 81 167 49 7487 6682 22 11 7 15 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2568 2604 2670 2206 3321 1352 865 639 491 770 474 471 494 264 198 227 406 346 105 330 73 9 10 15 7 6 1.24 1. 83 0.92 1. 45 0.98 1. 01 1. 02 1. 37 1. 38 1. 51 1. 57 1. 33 1. 46 4.33 0.73 1. 32 6.36 4.31 1. 81 1. 92 2.13 2.31 0.88 1.16 2.25 0.59 73.94 89.95 92.76 103.43 118. 71 175.67 244.18 328. 71 334.36 451.26 569.18 770.85 1321.61 1477.62 1781. 56 1991. 39 2171.03 2228.91 2323.52 2343.98 2662.34 2702.08 2796.11
2968.13 3096. 27 3169.29 72 87 87 102 114 171 240 325 333 448 567 767 1316 1472 1779 1987 2164 2221 2321 2334 2653 2696 2791 2960 3087 3160 5 1.04E-01 81.9 10 5.00E-01 17.4 10 5.60E+OO 2.2 5 1.58E-01 50.2 11 1. 66E+Ol 1.1 10 2.76E+OO 3.4 9 3.31E-01 18.8 8 1.09E-01 46.0 6 4.30E-02 91.6 8 8. 91E-02 61. 0 7 7.33E-02 55.8 8 7.99E-02 53.6 14 1. 32E+Ol 1. 0 11 6.81E-02 53.1 6 4.64E-02 55.6 8 4.62E-02 64.9 17 9.05E-02 57.9 15 l.85E-01 25.6 9 5.48E-02 39.6 20 8.32E+.OO 1.3 18 7.42E+OO 1.3 12 2 . .47E-02 34.2 10 1.19E-02 71.4 10 7.27E-03123.9 14 l.67E-02 45.5 12 7.78E-03 79.5 Flag: "*" = Peak area was modified by background subtraction Page 3847 of 5809 Fit 1. 64E+OO VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:26:33 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621356.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621356 SOLID GAMMA6 0 00:15:00.00 1. 50 keV No Empirical 75.00 Acquisition date : Sample quantity Sample geometry Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 09:11:02 115.00 GRAM CAN 0 00:15:04.89 10.00 0.00 % Peak Energy No interference correction performed Page 3848 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : Gl203621356 Acquisition date 3-0CT-2016 09:11:02 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 312 85.60* 6.177E+OO l.540E+OO l.627E+OO 37.61 136.47 ------10.68 6.083E+OO ------Line Not Found ------C0-60 1173.23 7132 99.85 l.227E:t-OO 1.520E+02 l.532E+02 2.60 1332.49 6329 99.98* l.092E+OO l.514E+02 l.526E+02 2.52 ZN-65 1115. 54 159 50.60* l.285E+OO 6.384E+OO 6.784E+OO 51.23 CD-109 88.03 2636 3.70* 5.253E+OO 3.541E+02 3.657E+02 6. 86
SN-12 6 64.28 ------9.60 2.772E+OO ------Line Not Found ------86.94 2636 8.90 5.253E+OO 1.472E+02 1. 472E+02 6. 86 87.57 2636 37.00* 5.253E+OO 3.541E+Ol 3. 541E+Ol 6. 86 BA-137M 661. 66 11577 89.90* 2.028E+OO l.658E+02 l.660E+02 2.00 CS-137 661. 66 11577 85.10* 2.028E+OO 1. 751E+02 1.754E+02 2.00 CE-139 165.86 101 80.00* 5.647E+OO 5.856E-01 6.522E-01 91. 98 PM-147 121. 22 312 0.00* 6.177E+OO 4.626E+04 4.698E+04 37.61 PM-149 285.90 67 3.10* 3.879E+OO 1.450E+Ol l.181E+04 111. 62 TM-171 51. 35 154 0.27 1.156E+OO 1.290E+03 l.318E+03 100.40 52.39 154 0.47* l.156E+OO 7.413E+02 7. 572E+02 100.40 66.73 ------0.14 3.097E+OO ------Line Not Found ------PB-210 46.54 5485 4.25* 6.176E-01 5.456E+03 5.466E+03 4.39 AM-241 59.54 16078' 35.90* 2.126E+OO 5.502E+02 5.503E+02' 2.27 Flag: "*" Key line Page 3849 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:26:34.13 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621356.CNF;l * *Acquisition date 3-0CT-2016 09:11:02 Sensitivity : 3.000 *
Detector ID GAM06 . Energy tolerance: 1. 500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:04.89 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
Sample ID G1203621356 Sample Quantity 1.1500E+02 GRAM *
Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO': [CANBERRA. GAMMA] EFF GAM06 CAN. CNF; 14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) C0-57 1.627E+OO 5. 996E-01 C0-60 1.526E+02 3.766E+OO ZN-65 6.784E+OO 3.406E+00 CD-109 3 .. 657E+02 2.458E+Ol SN-126 3.541E+Ol 2.380E+OO BA-137M 1.660E+02 3.261E+OO CS-137 1.754E+02 3.445E+00 CE-139 6.522E-01 5.879E-01 PM-147 4.698E+04 1. 732E+04 PM-149 1.181E+o4 1.292E+04 TM-171 7. 572E+02 7.450E+02 PB-210 5.466E+03 2.349E+02* AM-241 5.503E+02 1.222E+Ol Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Ali-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 Page 3850 of 5809 Key-Line Activity (pCi/GRAM -1.900E+OO 1.218E-01 O.OOOE+OO 1.818E-01 2.569E-0l 8.129E-01 -3. 611E-01 7.870E+00 2. 281E-01 -7.242E-01 O.OOOE+OO -3.445E-01 -*1.166E+OO 2.860E+OO -2.lOOE+Ol -1.482E+OO 4. 911E-01 K.L. Cnt Uncert ( 1. 96-s igma) 6.816E+OO 4.037E-01 4. 969E+09 2.534E-01 2.569E+OO 9.793E-01 1.899E+OO 6.403E+OO 6.938E-01 8.545E-01 1.170E+41 8.146E-01 2.025E+OO 2.610E+Ol 2.669E+Ol 1.940E+OO 6.981E-01 MDA (pCi/GRAM 5.200E-01 7. 581E-01 2.990E+OO 1.573E+Ol 1.532E+OO 1.030E+OO 1.088E+OO 5.730E-01 1. 501E+04 1.770E+04 9. 011E+02 1.949E+02 5. 831E+OO MDA (pCi/GRAM 1.190E+01 7.655E-01 O.OOOE+OO 5.666E-01 5.087E+OO 1.540E+OO 3.376E+OO 1.208E+Ol 1.195E+OO 1.385E+OO O.OOOE+OO 1.355E+OO 3.508E+OO 4.665E+Ol 4.415E:+-01 3.269E+OO 1.193E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN BR-77 l.824E+02 7.495E+02 1.270E+03 NOT IDENT. SR-82 1.460E-01 6.875E+OO 1.178E+Ol NOT IDENT. RB-83 6.953E-01 1.238E+OO 2.231E+OO NOT IDENT. KR-85 -4.998E+Ol 1. 071E+02 1.852E+02 NOT IDENT. SR-85 -2.829E-01 6.060E-01 l.048E+OO NOT IDENT. RB-86 5.068E+OO 2.0lOE+Ol 3.617E+Ol NOT IDENT. Y-88 1.861E-01 3.lOlE-01 6. 718E-01 NOT IDENT. Y-91 -1.102E+02 2.525E+02 4.423E+02 NOT IDENT. NB-94 l.422E-02 5.048E-01 8.744E-01 NOT IDENT. NB-95 1.502E-01 7.252E-01 1.255E+OO NOT IDENT. NB-95M 1.075E+OO 1.742E+OO 2.986E+OO NOT IDENT. ZR-95 -5.329E-01 l.334E+OO 2.239E+OO NOT IDENT. NB-97 O.OOOE+OO 5.816E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.203E+l0 O.OOOE+OO SHORT HLIF M0-99 l.529E+03 1.590E+03 l.722E+03 FAIL ABUN TC-99M O.OOOE+OO 1. 311E+25 O.OOOE+OO SHORT HLIF RH-101 -5.671E-02 3.599£-01 6.257£-01 NOT IDENT. RH-102 -5.007E-02 8.620£-01 *1.498E+OO NOT IDENT. RU-103 6 .113E-01 7.813E-01 1.418E+00 NOT IDENT. RH-106 -1.772E+OO 5.129E+OO 8.791E+OO NOT IDENT. RU-106 -1. 772E+OO 5.129E+00 8.791E+OO NOT IDENT. AG-108M 1.015£-01 5.671£-01 1. OllE+OO NOT IDENT. AG-llOM -2.468£-01 1.090E+OO 1.813E+OO NOT IDENT. SN-113 4.319E-01 7.584£-01 1.384E+OO NOT IDENT. CD-115 4.932E+02 l.318E+03 2.356E+03 NOT IDENT. SN-ll 7M 6.257£-01 8.749£-01 1. 54 7E+OO NOT IDENT. TE-123M 1.149£-01 3.439£-01 6.00lE-01 NOT IDENT. SB-124 -8.329£-01 7.390£-01 l.073E+OO NOT IDENT. SB-125 -9.187£-01 1.645E+OO 2.871E+OO NOT IDENT. TE-125M 6.992E+Ol 1.179E+02 2 .118E+02 NOT IDENT. I-126 -3.153£-01 5.416E+OO 8. 351E+OO NOT IDENT. SB-126 l.420E+OO 3.273E+OO 5.766E+OO NOT IDENT. SB-127 -4.207E+Ol 6.444E+Ol 1.078E+02 NOT IDENT. I-131 -3.580E-01 3.103E+OO 5.574E+OO FAIL ABUN I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 1.188E+Ol 4.376E+Ol 6.845E+Ol NOT IDENT. BA-133 -l.834E-01 6.572E-01 1.175E+OO . NOT IDENT. I-133 O.OOOE+OO 1. 446E+07 0.000E+OO SHORT HLIF CS-134 -1.346E-01 7.171£-01 1. 212E+OO NOT IDENT. CS-135 3.058E-01 2.324E+OO 3.880E+OO NOT IDENT. I-135 O.OOOE+OO 4.270E+23 O.OOOE+OO SHORT HLIF CS-136 -l.037E-01 3.030E+OO 5.394E+OO NOT IDENT. BA-140 2.364E+OO 6.151E+OO l.099E+Ol NOT IDENT. LA-140 2.730E-01 9.107E-01 l.847E+OO NOT IDENT. CE-141 -5.769E-01 8.028E-01 l.357E+00 NOT IDENT. CE-143 O.OOOE+OO 4.336E+04 O.OOOE+OO SHORT HLIF CE-144 1.140E+00 2.299E+OO 4.074E+OO NOT IDENT. PM-144 -5.622E-02 5.315E-01 9 .145E-'-01 NOT IDENT. PR-144 -4.644E+OO 3.989E+Ol 6.859E+Ol NOT IDENT. PM-146 -5. 729E-01 8.390E-01 1. 451E+OO NOT IDENT. ND-147 -9.134E-01 1.371E+Ol 2.407E+Ol NOT IDENT .* EU-150 -1. 7 68E-01 3.984E-01 7 .119E-01 NOT IDENT. EU-152 -2.253E-01 1.440E+OO 2.593E+00 FAIL ABUN .GD-153 -4.815E-01 9.736E-01 l.700E+00 NOT IDENT. EU-154 3.175E-01 1.137E+OO 2.153E+OO FAIL ABUN EU-155 2.236E-01 1.233E+OO 2.189E+OO FAIL ABUN TB-160 9.867E-01 2.934E+OO 5.021E+OO FAIL ABUN H0-166M 7.945E-'01 9.576E-01 1.723E+00 NOT IDENT. HF-172 2.123E+OO 2.339E+OO 3.926E+OO FAIL ABUN LU-172 -3.481E-01 1. 541E+OO 2.379E+OO FAIL ABUN LU-176 -9.479E-02 3.846E-01 6.956E-01 FAIL ABUN HF-181 -2.714E-01 9.176E-01 l.601E+OO NOT IDENT . TA-182 -1. lOlE+OO 1.741E+OO . 3. OlOE+OO NOT IDENT. RE-183 O.OOOE+OO 5.916E+OO 1.229E+Ol FAIL ABUN RE-184 9.017E-01 3.102E+OO 5. 271E+OO NOT IDENT. W-188 -8.103E+Ol l.177E+02 1. 888E+02 FAIL ABUN IR-192 -3.332E-01 5.418E-01 9.665E-01 NOT IDENT. HG-203 -l.094E-01 6.467E-01 1.063E+OO NOT IDENT. BI-207 -3.845E-01 l.022E+OO 1. 793E+OO NOT IDENT. TL-208 -l.255E-01 5.507E-01 9.552E-01 NOT IDENT. BI-211 2.417E+OO 3.053E+OO 5.656E+OO NOT IDENT. PB-211 2.617E+OO 1.173E+Ol 2 .112E+Ol NOT IDENT. BI-212 3.240E+OO 8.152E+OO 1.431E+Ol NOT IDENT. PB-212 l.849E-01 7.737E-01 1.311E+OO NOT IDENT. BI-214 -3.655E-01 l.097E+OO 1.887E+OO NOT IDENT. PB-214 8.612E-01 1. lllE+OO 2.057E+OO FAIL ABUN RN-219 -9.777E-01 6.652E+OO 1.184E+Ol NOT IDENT. RN-222 -3.655E-01 1.097E+OO. 1.887E+OO NOT IDENT. Page 3851of5809 RA-223 6.770E+OO 9.522E+OO 1.766E+Ol NOT IDENT. RA-224 -4. 861E+OO 8.388E+OO 1. 37 4E+Ol NOT IDENT. RA-226 -3.655E-01 1.097E+OO 1'. 887E+OO NOT IDENT. AC-227 2.578E-02 3.693E+OO 6.160E+OO NOT IDENT. TH-227 2.578E-02 3.693E+OO 6.160E+OO NOT IDENT. AC-228 1.598E+OO 3.237E+OO 5.530E+OO NOT IDENT. RA-228 1.598E+OO 3.237E+OO 5.530E+OO NOT IDENT. TH-228 1. 849E-01 7.737E-01 1. 311E+OO NOT IDENT. TH-229 2.881E-01 6.823E+OO 1.161E+Ol FAIL*ABUN TH-230 -3.655E-01 1.097E+OO 1.887E+OO NOT IDENT. PA-231 -1.169E+OO 6.678E+OO 1. 212E+Ol FAIL ABUN TH-231 6.770E+OO 9.522E+OO 1. 766E+Ol NOT IDENT. TH-232 1.598E+OO 3.237E+OO 5.530E+OO NOT IDENT. PA-233 4.085E-01 9.866E-01 1.816E+OO NOT IDENT. PA-234 -3.750E+OO 7.176E+OO 1.260E+Ol NOT IDENT. PA-234M 4.808E+Ol 9.825E+Ol 1.672E+02 NOT IDENT. TH-234 -3.161E+OO 1. 7 4 7E+Ol 2.925E+Ol NOT IDENT. U-234 -3.655E-01 1.097E+OO 1.887E+OO NOT IDENT. U-235 4.519E-02 2.294E+OO 3.983E+OO FAIL ABUN NP-237 4.085E-01 9.866E-01 1.816E+OO NOT IDENT. NP-238 O.OOOE+OO 3.252E+03 O.OOOE+OO SHORT HLIF U-238 -3.161E+OO 1.747E+Ol 2.925E+Ol NOT IDENT. NP-239 4.003E+OO 3.145E+OO 5.739E+OO NOT IDENT. PU-239 -7.410E+02 3.782E+03 6.563E+03 NOT IDENT. AM-243 8.737E-02 6.262E-01 1.127E+OO NOT IDENT. CM-243 7.468E-01 1.220E+OO 2 .198E+oo' NOT IDENT. BK-247 7.513E-01 1. 215E+OO 2.069E+OO FAIL ABUN CM-247 -1.226E-01 6.205E-01 1.102E+OO NOT IDENT. CF-249 -5.793E-02 6.933E-01 1.115E+OO NOT IDENT. CF-251 6.516E-01 1.500E+OO 2.613E+OO FAIL ABUN ANH-511 6.898E-03 4.657E-01 8.338E-01 NOT IDENT. Page 3852 of 5809 J VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:26:32.25 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn '%Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 312 85.60* 6.177E+OO l.540E+OO l.627E+OO 37.61 136.47 ------10.68 6.083E+OO ------Line Not Found ------C0-60 1173.23 7132 99.85 1.227E+OO l.520E+02 1.532E+02 2.60 1332.49 6329 99.98* 1. 092E+OO 1.514E+02 1. 526E+02 2.52 ZN-65 1115. 54 159 50.60* 1.285E+OO 6.384E+OO 6.784E+OO 51. 23 CD-109 88.03 2636 3.70* 5.253E+OO 3. 541E+02 3.657E+02 6.86 SN-126 64.28 ------9.60 2. 772E+OO ------Line Not Found ------86. 94 . 2636 8.90 5.253E+OO 1. 472E+02 1. 4 72E+02 6.86 87.57 2636 37.00* 5.253E+OO 3.541E+Ol 3.541E+Ol 6.86 BA-137M 661.66 11577 89.90* 2.028E+OO l.658E+02 l.660E+02 2.00 CS-137 661.66 11577 85.10* 2.028E+OO 1. 751E+02 l.754E+02 2.00 CE-139 165.86 101 80.00* 5.647E+OO 5.856E-01 6.522E-01 91. 98
PM-14 7 121.22 312 0.00* 6.177E+OO 4.626E+04 4.698E+04 37.61 PM-149 285.90 67 3.10* 3.879E+OO 1.450E+Ol 1.181E+04 111. 62 TM-171 51. 35 154 0.27 1.156E+OO 1. 2 90E+03 1.318E+03 100.40 52.39 154 0.47* '1.156E+OO 7.413E+02 7. 572E+02 100.40 66.73 ------0.14 3.097E+OO ------Line Not Found ------PB-210 46.54 5485 4.25* 6.176E-01 5.456E+03 5.466E+03 4.39 AM-241 59.54 16078 35.90* 2.126E+OO 5.502E+02 5.503E+02 2.27 Flag: "*" Key line Page 3853 of 5809 Summary of Nuclide Activity Sample ID : G1203621356 . Page : 2 Acquisition date 3-0CT-2016 09:11:02 Total number of lines in spectrum 26 Number of unidentified lines 9 Number of lines tentatively identified by NID 17 65.38% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags C0-57 271. 74D 1. 06 1.540E+OO 1.627E+OO 0.612E+OO 37.61 C0-60 5.27Y 1. 01 l.514E+02 l.526E+02 0.038E+02 2.52 ZN-65 244.06D 1. 06 6.384E+OO 6.784E+OO 3.476E+OO 51. 23 CD-1.09 461. 40D 1. 03 3. 541E+02 3.657E+02 0. 251E+02 6.86 SN-126 2.30E+05Y 1. 00 3.541E+Ol 3.541E+Ol 0.243E+Ol 6.86 BA-137M 30.08Y 1. 00 1.658E+02 1. 660E+02 0.033E+02 2.00 CS-137 30.08Y 1. 00 1. 751E+02 l.754E+02 0.035E+02 2.00 CE-139 137.640 1.11 5.856E-01 6.522E-01 5.999E-01 91. 98 PM-147 2.62Y 1. 02 4.626E+04 4.698E+04 1. 7 67E+04 37.61 PM-149 53.08H 815. 1.450E+Ol 1.181E+04 l.319E+04 111. 62 TM-171 1.92Y 1. 02 7. 413E+02 7.572E+02 7.602E+02 100.40 PB-210 22.20Y 1. 00 5.456E+03 5.466E+03 0.240E+03 4.39 AM-241 432.60Y 1. 00 5.502E+02 5.503E+02 0 .125E+02 2.27 ------------------Total Activity 5.392E+04 6.648E+04 Grand Total Activity 5.392E+04 6.648E+04 Flags: "K" Keyline not found "M" Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit Page 3854 of 5809 Unidentified Energy Lines Page : 3 Sample ID : Gl203621356 Acquisition date : 3-0CT-2016 09:11:02 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 37.09 103 2821 1. 24 73.94 72 5 1.04E-01 **** 1.0lE-01 9 45.10 491 2838 1. 83 '89. 95 87 10 5.00E-01 34.9 5.04E-01 T O* 167.41 40 508 1. 38 334.36 333 6 4.30E-02 **** 5.60E+OO 0 225.90 82 787 1. 51 451. 2 6 448 8 8. 91E-02 **** 4. 61E+OO T 0 385.80 72 471 1. 33 770.85 767 8 7.99E-02 **** 3.08E+OO 0 739.32 60 256 4.33 1477.62 1472 11 6.81E-02 **** 1.85E+OO T 0 891.33 40 191 0.73 1781. 56 1779 6 4.64E-02 **** 1.57E+OO 0 996. 25 40 218 1. 32 1991.39 1987 8 4.62E-02 **** 1.42E+OO T 0 1086.07 78 388 6.36 2171.03 2164 17 9.05E-02 **** 1.32E+OO T 0 1162. 31 47 100 1. 81 2323.52 2321 9 5.48E-02 79.3 1.24E+OO 0 1351.56 21 8 2.31 2702.08 2696 12 2.47E-02 68.5 l.08E+OO . 0 1398.56 10 10 0.88 2796.11 2791 10 1.19E-02 **** 1.04E+00 0 1484.54 6 15 1.16 2968.13 2960 10 7.27E-03 **** 9.90E-01 0 1548.58 14 7 2.25 3096. 27 3087 14 1.67E-02 90.9 9.55E-01 0 1585.08 7 6 0.59 3169.29 3160 12 7.78E-03 **** 9.36E-01 T Flags: "T" = Tentatively associated Page 3855 of 5809 VAX/VMS Nuclide Identification Report 03-0CT-2016 09:26:46.69 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621356.CNF;l * *Acquisition date 3-0CT-2016 09:11:02 Sensitivity 3.000 *
Detector ID GAM06 Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:04.89 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621356 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : 1.1500E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4'
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-139 PM-147 PM-149 TM-171 PB-210 AM-241 Le (pCi/GRAM 2.530E-01 3.467E-01 1.438E+OO 7.678E+OO 7.477E-01 4.959E-01 5.239E-01 2.778E-01 7.302E+03 8.612E+03 4.443E+02 9.613E+Ol 2.870E+OO ----Non-Identified 'Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-'-68 AS-73 AS-74 SE-75 BR-77 Page 3856 of 5809 Le (pCi/GRAM 5.782E+00 3.514E-01 O.OOOE+OO 2.417E-01 2.216E+00 7.435E-01 1.627E+OO 5.869E+OO 5.754E-01 6.668E-01 0.000E+OO 6.523E-01 1.688E+OO 2.247E+Ol 2.177E+Ol 1.573E+OO 5.800E-01 6.175E+02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB.:.125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 -CS-134 CS-135 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223

Page 3857of5809 5.653E+OO l.078E+OO 8.933E+Ol 5.056E-01 1. 741E+Ol 2.873E-01 2.066E+02 4.190E-01 6.029E-01 l.453E+OO l.075E+OO O.OOOE+OO O.OOOE+OO 8.266E+02 O.OOOE+OO 3.043E-01 7.191E-01 6.869E-01 4.223E+OO 4.223E+OO 4.921E-01 8.742E-01 6.721E-01 l .137E+03 7.525E-01 2.918E-01 4.303E-01 l.394E+OO l.031E+02 4.009E+OO 2.769E+OO 5.163E+Ol 2.702E+OO O.OOOE+OO 3.333E+Ol 5.702E-01 O.OOOE+OO 5.818E-01 l.886E+OO O.OOOE+OO 2.598E+OO 5.305E+OO 7.970E-01 6.590E-01 O.OOOE+OO l.982E+OO 4.384E-01 3.288E+Ol 7.056E-01 l.161E+Ol 3.453E-01 l.257E+OO 8.274E-01 9.877E-01 l.066E+OO 2.421E+OO 8.276E-01 1. 911E+OO l.146E+OO 3.376E-01 7.769E-01 1. 380E+OO 6.083E+OO 2.546E+OO 9.159E+Ol 4.687E-01 5.167E-01 8.616E-01 4.592E-01 2.746E+OO l.025E+Ol 6.876E+OO 6.374E-01 9.082E-Ol 9.989E-01 5.744E+OO 9.082E-01 8.583E+OO NOT IDENT. NOT IDENT. NOT .I DENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL "ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239. AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3858 of 5809 6.673E+OO 9.082E-01 2.992E+00 2. 992E+OO . 2.677E+OO 2.677E+OO 6.374E-01 5.651E+OO 9.082E-01 5.884E+OO 8.583E+OO 2.677E+OO 8.831E-01 6.106E+OO 8.070E+Ol l.426E+Ol 9.082E-01 1.938E+OO 8.831E-01 O.OOOE+OO 1:426E+Ol 2.797E+OO 3.190E+03 5.507E-01 l.070E+00 1.006E+OO 5.348E-01 5.404E-01 1. 269E+OO 4.028E-01 NOT IDENT. NOT IDENT. NOT °IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:26:52.45 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621356.CNF;l *
Acquisition date 3-0CT-2016 09:11:02 Sensitivity : 3.000 *
Detector ID GAM06 Energy 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:04.89 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621356 Analyst initials: MXRl *
Batch Number 1596249 Sample Quantity : l.1500E+02 GRAM *
Quantity Err(%) : 1. 7391E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* *
CALIBRATION INFORMATION * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) C0-57 1.627E+OO 6. llOE-01 6. llOE-01 C0-60 1. 52 6E+02 1.245E+Ol 1.245E+Ol ZN-65 6.784E+OO 3.615E+OO 3.615E+OO CD-109 3.657E+02 4.352E+Ol 4.352E+Ol SN-126 3. 541E+Ol 3.774E+OO 3.774E+OO BA-137M 1.660E+02 l.409E+Ol 1.409E+Ol CS-137 1. 754E+02 1.488E+Ol 1.488E+Ol CE-139 6.522E-01 6.035E-01 PM-147 4.698E+04 1. 7 65E+04 1. 765E+04 PM-149 1.181E+04 1.306E+04 1.306E+04 TM-171 7. 572E+02 7.483E+02 7.483E+02 PB-210 5.466E+03 5.253E+02 5.253E+02 AM-241 5.503E+02 4.434E+Ol 4.434E+Ol Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 -1.900E+OO 6.818E+OO 6. 872E+OO NOT IDENT. NA-22 l.218E-01 4.038E-01 4.075E-01 NOT IDENT. NA-24 -5.212E+08 4.970E+09 4.975E+09 SHORT HLIF AL-26 l.818E-01 2.538E-01 2.667E-01 NOT IDENT. K-40 2.569E-01 2.569E+OO 2.572E+oo-NOT IDENT. SC-46 8.129E-01 9.843E-01 1.050E+OO NOT IDENT. V-48 -3.611E-01 1.900E+OO l.907E+OO NOT IDENT. CR-51 7.870E+00 6.445E+OO 7.357E+OO NOT IDENT. MN-54 2.281E-01 6.943E-01 7.018E-01 NOT IDENT. C0-56 -7.242E-01 8.585E-01 9.185E-01 NOT IDENT. MN-56 -1.000E+41 1.175E+4! O.OOOE+OO SHORT HLIF C0-58 -3.445E-01 8.155E-01 8.301E-01 NOT IDENT. FE-59 -1.166E+OO 2.037E+OO 2.103E+OO NOT IDENT. *GE-68 2.860E+OO 2.610E+Ol 2.614E+Ol NOT IDENT. AS-73 -2.lOOE+Ol 2.704E+Ol 2.865E+Ol NOT IDENT. AS-74 -1.482E+00 1.946E+OO 2.058E+OO NOT IDENT. SE-75 4. 911E-01 6. 996E-01 7.338E-01 FAIL ABUN Page 3859 of 5809 BR-77 l.824E+02 7.581E+02 7.625E+02 NOT IDENT. SR-82 l.460E-01 6.875E+OO 6.876E+OO NOT IDENT. RB-83 6.953E-01 l.243E+OO 1.282E+00 NOT IDENT. KR-85 -4.998E+Ol l.072E+02 1. 095E+02 NOT IDENT. SR-85 -2.829E-01 6.065E-01 6 .198E-0.1 NOT IDENT. RB-86 5.068E+OO 2.012E+Ol 2.025E+Ol NOT IDENT. Y-88 1. 861E-01 3.104E-01 3.215E-01 NOT IDENT. Y-91 -1.102E+02 2.527E+02 2.575E+02. NOT IDENT. NB-94 l.422E-02 5.048E-01 5.048E-01 NOT IDENT. NB-95 1.502E-01 7.254E-01 7.285E-01 NOT IDENT. NB-95M 1. 075E+OO 1. 745E+OO l.812E+OO NOT I-DENT. ZR-95 -5.329E-01 1.335E+OO 1.356E+OO NOT IDENT. NB-97 l.OOOE+41 5.875E+40 O.OOOE+OO SHORT HLIF ZR-97 2.497E+08 1.203E+10 1.203E+10 SHORT HLIF M0-99 1. 529E+03 1.598E+03 1. 740E+03 FAIL ABUN TC-99M -8.303E+22 l.311E+25 0.000E+OO SHORT HLIF RH-101 -5.671E-02 3.601E-01 3.610E-01 NOT IDENT. RH-102 -5.007E-02 8.620E-01 8.623E-01 NOT IDENT. RU-103 6.113E-01 7.832E-01 8.303E-01 NOT IDENT. RH-106 -1.772E+OO 5.132E+OO 5.194E+OO NOT IDENT. RU-106 -1. 772E+OO 5.132E+OO 5.194E+OO NOT IDENT. AG-108M 1.015E-01 5.671E-01 5.690E-01 NOT IDENT. AG-llOM -2.468E-01 1.090E+OO 1. 096E+OO NOT IDENT. SN-113 4.319E-01 7.593E-01 7.838E-01 NOT IDENT. CD-115 4.932E+02 l.319E+03 1.337E+03 NOT IDENT. SN-ll 7M 6.257E-01 8. 761E-Ol
9.203E-01 NOT IDENT. TE-123M 1.149E-01 3.440E-01 3.479E-01 NOT IDENT. SB-124 -8.329E-01 7".417E-01 8.314E-01 NOT IDENT. SB-125 -9.187E-01 1. 647E+OO 1.698E+OO NOT IDENT. TE-125M 6.992E+Ol 1.180E+02 1.222E+02 NOT IDENT. I-126 -3.153E-01 5.416E+OO 5.418E+00 NOT IDENT. SB-126 1.420E+OO 3.278E+OO 3.339E+OO NOT IDENT. SB-127 -4.207E+Ol 6.467E+Ol 6.740E+Ol NOT IDENT. I-131 -3.580E-01 3.104E+OO 3.108E+OO FAIL ABUN I-132 -1.000E+41 5.004E+41 O.OOOE+OO *sHORT HLIF TE-132 1.188E+Ol 4.378E+Ol 4. 410E+o,J NOT IDENT. BA-133 -1.834E-01 6.574E-01 6.626E-01 NOT IDENT. I-133 5.749E+06 l.449E+07 1. 472E+07 SHORT HLIF CS-134 -1.346E-01 7.173E-01 7.198E-01 NOT IDENT. CS-135 3.058E-01 2.325E+OO 2.329E+OO NOT IDENT. I-135 -1. 8 60E+23 4.368E+23 O.OOOE+OO SHORT HLIF CS-136 -l.037E-01 3.030E+OO 3.030E+OO NOT IDENT. BA-140 2.364E+OO 6.155E+OO 6.246E+OO NOT IDENT. LA-140 2.730E-01 9. llOE-01 9.193E-01 NOT IDENT. CE-141 -5.769E-01 8.038E-01 8.448E-01 NOT IDENT. CE-143 -3 .131E+04 4.346E+04 4.570E+04 SHORT HLIF CE-144 1.140E+00 2. 301E+OO 2.358E+OO NOT IDENT. PM-144 -5.622E-02 5.316E-01 5.322E-01 NOT IDENT. PR-144 -4.644E+OO 3.989E+Ol 3.995E+Ol NOT IDENT. PM-146 -5.729E-01 8.412E-01 8.799E-01 NOT IDENT. ND-147 -9.134E-01 l.371E+Ol 1. 372E+Ol NOT IDENT. EU-150 -l.768E-01 3.987E-01 4.066E-01 NOT IDENT. EU-152 -2.253E-01 1.440E+OO 1.443E+OO FAIL ABUN GD-153 -4.815E-01 9.743E-01 9.982E-01 NOT IDENT. EU-154 3.175E-01 1.138E+OO 1.146E+OO FAIL ABUN EU-155 2.236E-01 1.233E+OO 1.237E+OO FAIL ABUN TB-160 9.867E-01 2.936E+OO 2.970E+OO FAIL ABUN H0-166M 7.945E-01 9.606E-01 1.025E+OO NOT IDENT. HF-172 2.123E+00 2.367E+OO 2.554E+OO FAIL ABUN LU-172 -3.481E-01 1.542E+OO 1.550E+OO FAIL ABUN LU-176 -9.479E-02 3.847E-01 3.870E-01 FAIL ABUN HF-181 -2.714E-01 9.179E-01 9.260E-01 NOT IDENT. TA-182 -1.lOlE+OO l.744E+00 1.813E+OO NOT IDENT. RE-183 7.211E+Ol 9.687E+OO 3.392E+Ol FAIL ABUN RE-184 9.017E-01 3.105E+OO 3 .131E+OO NOT IDENT. W-188 -8.103E+Ol l.182E+02 1.238E+02 FAIL ABUN IR-192 -3.332E-01 5.427E-01 5. 631E-01 NOT IDENT. HG-203 -1.094E-01 6.468E-01 6.487E-01 NOT IDENT. BI-207 -3.845E-01 1.024E+OO 1.038E+OO NOT IDENT. TL-208 -l.255E-01 5.508E-01 5.537E-01 NOT IDENT. BI-211 2.417E+OO 3.061E+OO 3.249E+OO NOT IDENT. PB-211 2.617E+OO 1.173E+Ol 1.179E+Ol NOT IDENT. BI-212 3.240E+OO 8.158E+OO 8.287E+OO NOT IDENT. PB-212 l.849E-01 7.739E-01 7.784E-01 NOT IDENT. BI-214 -3.655E-01 1.098E+OO l. llOE+OO NOT IDENT. PB-214 8.612E-01 1.114E+OO 1.180E+OO FAIL ABUN RN-219 -9.777E-01 6.654E+OO 6.668E+OO NOT IDENT. RN-_222 -3.655E-01 1.098E+OO 1. llOE+OO NOT IDENT. Page 3860 of 5809 RA-223 6.770E+OO 9.548E+OO l.002E+01 NOT IDENT. RA-224 -4.861E+OO 8.400E+00 8.681E+OO NOT IDENT. RA-226 -3.655E-Ol l.098E+00 l. llOE+OO NOT IDENT. AC-227 2.578E-02 3.693E+OO 3.693E+OO NOT IDENT. TH-227 2.578E-02 3.693E+OO 3.693E+OO NOT IDENT. AC-228 l.598E+OO 3.244E+OO 3.323E+OO NOT IDENT. RA-228 l.598E+OO 3.244E+OO 3.323E+OO NOT IDENT. TH-228 l.849E-01 7. 739E-01' 7.784E-01 NOT IDENT. TH-229 2.881E-Ol 6.823E+OO 6.824E+OO FAIL ABUN TH-230 -3.655E-Ol l.098E+OO l. llOE+OO NOT IDENT. PA-231 -l.169E+OO 6.684E+OO 6.704E+OO FAIL ABUN TH-231 6.770E+OO 9.548E+OO l.002E+Ol NOT IDENT. TH-232 l.598E+OO 3.244E+OO 3.323E+OO NOT IDENT. PA-233 4.085E-01 9.874E-01 l.004E+OO NOT IDENT. PA-234 -3.750E+OO 8.374E+OO 8.543E+OO NOT IDENT. PA-234M 4.808E+Ol 9.851E+Ol l.009E+02 NOT IDENT. TH-234 -3.161E+OO 1. 749E+Ol 1. 754E+Ol NOT IDENT. U-234 -3.655E-01 l.098E+OO l. llOE+OO NOT IDENT. U-235 4.519E-02 2.294E+OO 2.295E+OO FAIL ABUN NP-237 4.085E-01 9.874E-01 l.004E+OO NOT IDENT. NP-238 9.343E+02 3.255E+03 3.282E+03 SHORT HLIF U-238 -3.161E+00 1. 749E+Ol 1. 754E+Ol NOT IDENT. NP-239 4. oo3E+.oo 3.169E+OO 3.647E+OO NOT IDENT. PU-239 -7.410E+02 3.783E+03 3.798E+03 NOT IDENT. AM-243 8.737E-02 6.263E-01 6.275E-01 NOT IDENT. CM-243 7.468E-01 l.222E+OO l.268E+OO NOT IDENT. BK-247 7 .. 513E-Ol l.226E+OO 1. 272E+OO FAIL ABUN CM-247 -l.226E-01 6.209E-01 6. 233E-01 . NOT IDENT. CF-249 -5.793E-02 6.933E-01 6.938E-01 NOT IDENT. CF-251 6.516E-01 l.502E+OO l.530E+OO FAIL ABUN ANH-511 6.898E-03 4.657E-01 4.657E-01 NOT IDENT. Page 3861of5809
GEL Laboratories LLC *
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 1841.6368 87.09 540.2142 136.47 460.9942 45.60 1632 .1157 87.57 540.7593 140.51 426.1465 46.54 1637.0526 88.03 541.2784 143.76 420.8557 49. 72 1436.5237 88.34 541. 6288 144.24 399.0442 51. 35 1549.3970 88.47 541. 7759 145.44 418.7352 51. 87 1588.1833 89. 96 477.9510 152.43 392.0894 52.39 1590.6327 90.64 485.0193 153.25 408.5446 52.97 1670.1371 91.11 459.8628 154.21 377.0555 53.44 1700.5043 92.59 474.0950. 156.02 407.9984 54.07 1766.8883 93.35 448.7623 158.56 373.9821 57.36 0.0000 94.56 435.3367 159.00 386.0335 57.53 1896. 7218 94.65 435.4156 162.33 361.5121 57.98 1234.1639 94.67 435.4328 162.66 377.5258 59.27 1238.5405 94.87 *435. 6045 163.33 406.7118 59.32 1238.7048 97.43 466.9885 165.86 329.9534 59.54 1239.4467 98.43 431. 82 63 176.31 398.3127 60.96 1244.1995 98.44 431.8365 17 6. 60 375.3.414 61.17 1244.8989 99.53 425.9043 177.52 347.1316 62.93 483.8324 100.11* 442.0270 181.07 391. 8653 63.29 508.3216 102.03 438. 7333. 181.52 376.5805 63.58 535.1631 103.18 424.9270 184.41 463.5320 64.28 585.5295 103.37 425.0786 185. 72 443.1284 66.73 544.6443 105.21 456.1524 193.51 427.1057 67.24 587.2230 105.31 456.2370 197.03 428.8974 67. 68 615.2103 106.12 442.0823 198.01 456.5096 67.75 615.3185 106.47 465.1269 201.83 418.8242 69.67 596.2616 109.28 411. 8016 203.43 430.9726 70.83 '568. 5532 111. 00 414.0692 205.31 412.5306 72.81 570.3317 111. 76 417.6237 210.85 463.2906 72.87 546.4139 114.06 432.3581 215.65 448.4814 74.66 573.7481 116. 30 444.1089 222 .11 478.3616 74.82 573.9606 116.74 413.2031 227.09 449.7927 74.97 592.7150 119.76 460.5810 227.38 435.9221 77 .11 606.8308 121.12 417.2996 228.16 431.6065 78.74 575.3989 121.22 417.3686 228.18 431.6178 79.69 593.5003 121. 78 417.7574 235.69 394.5819 80.12 623.1636 122.06 417.9518 235. 96 417.0800 80.19 623.2599 122.92 418.5507 238.63 382.7823 80. 57' 634.1205 123.07 418.6542 238.98 384.1026 81. 00 641.3106 123.68 414.6590 240.99 414.4981 81. 07 641. 4095 125.81 387.4579 242.00 387.6539 81. 75 637.6574 127.23 422.5348 244.70 400.6040 83.79 614.3232 127.91 446.6158 252.40 389.3047 84.00 598.1945 129.30 410.5677 252.80 377.4751 85.43 627.8812 131.20 412.8418 254.15 0.0000 86.55 539.6000 133. 02 410.9207 256.23 376.3369 8 6. 7 9 539.8682 133. 52 396.7395 260.90 370.7928 86. 94 540.0412 136.00 433.6263 264.66 364.8504 Page 3862of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 352.7736 364.49 338.2066 600.60 219.9227 265.00 368.5981 366.42 368.6027 602.52 0.0000 268.22 389.1797 372. 51 332.2588 604. 72 214.2797 269.46 405.4677 375.05 345.2649 607.14 216.5708 270.03 393.4985 1093.63 321. 0511 609.32 226.9834 271.23 408.5777 383.85 342.1172 610.33 202.6600 273.65 398.4865 388.16 323.0641 614.28 217.3422 276.40 357.8354 388.63 333.8947 618.01 189.1176 277.37 391.2734 391.69 335.0645 620.36 198.5469 277.60 391.3513 400.66 357.8993 621.93 212. 0116 278.00 417.2699 401.81 349.1598 630.19 0.0000 279.20 395.6115 402.40 361.9377 631.29 191.3735 279.54 376.0659 404.85 341. 7 550 633.25 201.8459 279.70 376.1219 410.95 396.7425 634.78 217.4564 280.46 392.3735 413.71 373.8317 635.95 199.0155 283.69 317.4495 414.70 405.0286 636.99 182.6105 284.31 370.2850 423. 72 355.2798 645.85 204.1021 285.41 390.4193 427.09 371.6702 657.76 221.9183 285.90 425.2024 427.87 392.0595 657.90 0.0000 287.50 364.7453 433.94 410.2072 661.66 219.1858 290.67 381. 0799 439.40 393.1544 664.57 0.0000 293.27 0.0000 453.88 449.0684 666.33 194.5598 295.22 362.6666 463.37 442.3387 666.50 194.5750 295.96 339.2031 468.07 '469.9850 667.71 0.0000 298.58 358.7325 473.00 437.3877 677.62 178.7435 299.98 372.0931 475.06 400.0995 685.70 195.2301 300.09 372.1295 476.78 409.9898 695.00 168.4976 300.13 372 .1385 477.60 397.8772 696. 49 182.3931 301.36 371.7025 482.18 366.6733 696.51 182.3931 302.85 355.4464 487.02 325.8087 697.00 180.3137 304.50 378.5610 492.35 327.7942 697.30 186.6992 304.85 370.3027 497.08 279.8274 697.49 184.5953 306.78 368.3877 505.52 255.1984 702.65 174.3835 308.46 376.4778 507.63 0.0000 706.68 169. 3710 311. 90 380.1000 511. 00 251.1715 711. 68 165.4696 316.51 373.0986 514.00 265.1476 720.70 176.8399 319.41 331.5927 514.00 265.1476 721. 93 0.0000 320.08 325.8281 520.40 243.7690 722.78 169.4887 321.04 377.0369 520.69 241.8672 722. 91 173.7927 323.87 348.9738 522.65 0.0000 723. 31 183.4757 325.23 362.9910 527.90 238.9488 724 .19 205.0126 328.76 348.6494 528.26 240.9496 727.33 183.7958 333.37 353.3668 529.59 243.0729 733.00 206.8672 333.97 366.4058 529.87 0.0000 735.93 171. 5254 334.37 359.6604 531.02 245.2193 737.46 194. 3115 338.28 377.1281 537.26 234.3029 739.50 . 199. 8822 338.32 381.4512 546.56 0.0000 747.24 214.6289 340.48 351.0408 552.55 222.4182 748.06 204.9423 340.55 351.0657 563.25 222.6875 752.31 197.6999 344.28 340.8382 569.33 225.4023 753.82 192.3910 345.93 349.0748 569.50 225.4207 756.73 206.7765 351.06 326.9728 569.70 225.4391 756.80 206.7765 351.93 328.0572 583 .19, 213.9707 763.94 192 .1133 355.39 0.0000 584.27 206.0427 765.81 190.0718 356.01 368.3571 595.83 243.6575 766.42 202.1405 Page 3863 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 205.4567 1002.74 241.3669 1678.03 0.0000 772. 60 0.0000 1004.73 243.3125 1690.97 16. 0611 776.52 190.9143 1021.30 0.0000 1750.46 0.0000 777.92 216.2703 1025.87 0.0000 1764.49 15.2219 778.90 216.3585 1028.54 0.0000 1770.23 15.2390 783.70 *212. 3738 1037,84 216.1124 1771.35 9.7993 785.37 213.6242 1038.76 0.0000 1791.20 0.0000 792.07 194.3262 1046.59 215.8037 1808.65 5.4852 794.95 198. 9697 1048.07 229.5129 1810. 72 0.0000 795.86 201.2546 1049.04 236.8499 1836.06 6.6182 801. 95 230.5638 1050.41 211.5260 810.06 223.5160 1063.66 216.0687 810.29 212.4191 1077.00 210.5573 810.45 225.7813 1077.34 219.7412 810.76 236.9296 1085.87 214.8047 815.77 212.8777 1093.63 242.9238 818.51 219.7973 1099 .. 45 238.7498 832.01 211. 9790 1112. 07 239.8518 834.85 212.2097 1112.84 210 .1108 835.71 213.4021 1115.54 210.2770 836.80 0.0000 1120.29 164.7548 "-846.75 0.0000 1120. 55 169.2188 846.77 259.4238 1121.30 175.6973 856.80 232.1015 1129. 67 146.9871 860.56 239.2381 1131.51 0.0000 871.09 252.6948 . 1147.95 0.0000 873.19 250.6152 1173.23 109.3093 875.33 0.0000 1177.95 78.5078 879.38 227.2111 1189. 05 75.7275 880.51 229.5928 1204.77 77.9711 883.24 226.3916 1221.41 52.5427 884.68 253. 9685 1231. 02 34.4839 889.28 220.0156 1235.36 43.1570 894.76 254.8989 1238.28 41.2704 898.04 260.9539 1260.41 0.0000 900. 72 276.1621 1271. 87 39. 7162 903.28 253.3814 1274.44 36.8357 911.20 282.9822 1274.54 36.8357 912.08 283.07i9 1291.59 26.2930 923.98 0.0000 1298.22 0.0000 926.50 292.6465 1312 .11 27.4155 929.11 302.2225 1332.49 38.3906 937.49 314.7693 1362.66 0.0000 944.13 334.7746 1365.19 12.9048 946.00 349.9043 1368.63 0.0000 949.00 323.9335 1384.29 20.9474 954.55 0.0000 1408.01 9.0313 962.31 298.0709 1457.56 0.0000 964. 08 307.0807 1460.82 13.2142 966 .17 271. 0984 1489.16 9.3566 968. 97 256.3254 1505.03 17. 4 628 983.53 240.7143 15.84.12 3.3473 984.45 0.0000 1596.21 10.4889 996.26 259.7588 1620.50 7.3815 1001.03 228.7188 1621. 92 12.6584 Page 3864 of 5809 QS-Oci;-2016 I So!Ws are f:han oa: ioo mq sampfcs have been blaru:: ccmeded 111mnk C<JJn-ection*re.,,ortildJ.1nert.idi!C1 nr *.. if less, than tO ,150'.".lb ,of saanpfe actfyitY. . 1f greater til3n io* W:Ot"ls 46% u tier.;w, ..:..;..: l\ioA*., ii!m>r rs:.. ** _... . .. l£nsttQm<lnt 'uairir& * * : .. wr*..:*r. iW....,, .. lf du1Jii;;a-t:o al'.'!; . . . . . . le$$ than Mll,C, RPI) !s less, If s*. MDA/ Ulen RP.D 20% or le$$, * * ' tfie M9¢, Ri>D'IS oD;b,* . ' ' or*meets 'tfie etlent*s* .rMuii'ed HER' acceatance criteria. Tracer vletd J5*1s,.125% yield 25-125%; CO!' rnl:etig ti,1e ii:ccelitiin'ce I '=am;.,lc vras Dreserved If reauirod. smears;raken for: Radioactive batches. Method Spike and LC.s ave \\llthln meets* the :ti:ce;;'{:ii.f.n critnrl"'\* No blank spaces 'on'.data forn\s. AH i1ne at'itl; 1ii1tia1ed anci*
fN....;; * -*-'"' ..
AUX data IS Ravi Cata arliii or sisec:tru"1 are Included 'and nroneriv statused.' 'I .... ' ..... [)11t? .seco*nd. fev!ewed. Dlsoosltlon verified to be *comnleted, , ... Review s'amp!C hlStorfcal 'results If available cir results above MDC ilave been verlfled bv.tllstorlciil results.' recount or re-,analiisls.) , . ./ / / "* / **.r* **/. 'j,/ ./'" ./ ': --' .. _ _.. *. -.... -. . . . --. .. . . . . I.. , .. . .* '.,£,. ' ' JV'f k' ... ... .I " secondary Review Peiformod +-, ___ * ....,(_..,..CJ..,..(_5_(_,,,...1.b.,.,. .. ...,.. of 5809 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 03-0CT-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1596252 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE HASL 300, 4.5.2.3/Ga-01-R Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1563784 Revision No.: 1 Type: Process Client Code: MJWC Sample received out of holding for sample 405235041, sample Samples were analyzed as soon as possible. Reporting results. 405235042, sample 405235043, sample 405235044, sample 405235045, sample 405235046, sample 405235047, sample 405235048, sample 405235049, sample 405235050, sample 405235051, sample 405235052, sample 405235053, sample 405235054, sample 405235055, sample 405235056, sample 405235057, sample 405235058, sample 405235059, sample 405235060 and DUP 1203621362 Originator's Name: Data Validator/Group Leader:: Bryan Williams 03-0CT-16 Spencer Collins 03-0CT-16 Page 1 Page 3866 of 5809 G.* .amm .. a S .. pee. :Q .. 11eue S.h.e.e .. t

r. [r.,.,r ,(',,ej;;,,.-r*lO . 09/16/2016 . Analyst: First .Internal Due Date: 09/J0/201 () . .Lcs*code:' l:.rr!Q :Exptratfori,Datc: *vol.: *)to '"1V Initials: f1,<;_ Prep*.Date: .. 'tJli:.hte BalnncelD:._: ..... +'-fA ....
___ _ lln7.itril .'SampleiD 'type ,Code Matrix 40S23504M 4.4D.R.J;.j* SAMP.I;;E *M.Jwcoor SOIL 4;4D.ltl.3 :sAMPDE: .M.Ji\'CO(>t\ SOIL 405iJS04J*I *4.*U>:R2;4 1s;u1ru: MJWCiio1* SOIL .i.;m.1.t.i.2 'SAMl'LE S()IL 405235045"1 4.-.io;R.s.2 \MJ\Vtooi SOIL 405235046..1 *MJ\\rCO!Jt* sofL **4052JS04N 4;SA.Jt1;4. '.SAMI'L;E. !)OIL;. 4:5B.lt.tl :SAMPt.:E: S!)IL 405235049* J 4.iSB.R;J:J . SAMPLE. M.J\\rtl>if.t: s<;>fr. * . 405235050. t 4;sB;1t.1;4: :SAMPLE M;JWCOOI 405235051,-1 4;5IUU\3, .SAMi'L\E *MJwcoot* SOIL* ,4*osl3s0st.1 4:5Rlti:4 sAMi>tE; .t\tJ\VCOOi' . salt.* *4{)52351J53;.1 <i.scresi SAMP.Llli'. ,SOIL SAMPLE *MJWCOOi 0SOU. 405235055-1 4:sclli1.4; SAMP.fE' M:n,*cooi', :,soi1:. 4052350SG;;i. * *SAl\fPLE-M,IWC001 >>So'ti .4Q523505701: .4;5Clt2!J* SAMPL'E: MJWCOOJ* lSOJL 405235058-1 ,4.5C:R.2;4* MJ\Vcoo1 *so1t *.:;,tA;R.J.2* SOIL, '.MA.RJ;,3' SAMPLE* l\fJWCOOl :son. i20362136J-i . MB MB* . :s6iL . ll036213<i2"f ,DUP.4.4D.R.'!.4(40sl35041) ppr: 'S.OIL. . )2Q362.l363-J .LCS LCS ACGOUi\'Ti .. SOIL *GEL.Ltib'oratories1.JLC., .RililioClii:iitistry:DivisiOir *Geometry J().;N0\'*1513:27:00'/1.f-: *<J;t. N ; . 30-No\*:.15 : J3j50:00 07-DEC*i5.tO:oz:o'O ()7*DE.Q'J5)0:'10:011.tt:.f. . ' /-. , 'fW i3:3lioci ' ltf. .* : , . * . OhQEC-15*14:24:00 *1
1J2.ntc-1!!.14:s9:oon,.l
0 16;-DEC-15 . .. (lLJV*F) 181'483 g. I" 176.8 g. .16M!13g 128;844g I30.599*g .. J$6;9l.3_g 151.34911 131.517 !I *1'1J,604Jl 15a.012a . :165;2!1S'S I 1'3;628g J J4G,461:g 102'48lg UU35g ! 140.0:.12.g. L.1s4*2?!1: I I i .. J 1-l i *seating Detector-(iiAppUcnbtti)' .. -** -* K Q L ! F fl:t .. *'t..S. .. *'">';) .. , .. t..\\. Vii.:* "t!1* \\J .. f '! .' ' .. 7. ,,_., .. .. .. ll2-DEC'15'15'00'1 I 152.266 g I V& 1 li:t-J . *t .. . .. . .. . . ... .. I :'l.'t.'. ..-*a.?f ... , l llS ! i..,l . ol t ,_

VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:57:25.97 ********************************************************************************

GEL Laboratories LLC *
20AO Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date : 30-NOV-201,5 13: 27: 00 A_cquisi tion date : 3-0CT-2016 05: 54: 08. Sample ID : G405235041 Sample quantity : 1.81483E+02 GRAM Detector name : GAM2 8 Detector geometry_: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.41 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 3 3 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 74.82* 77.24 87.41 93.17* 116. 91 186.22* 208.98 238.89* 241. 70 295.86 300.31 338.63 352.28* 448.85 463.26 480.40 511. 83* 523.66 583.75* 601.53 609.77* 618.45 662.53* 675.73 727.33 816.35 8 61. 08 867.40 912.08* 969. 82 1120.37* 1183. 05 1239.39 14 61. 82* Page 3868 of 5809
BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 126 171 39 30 33 71 42 340 104 125 34 80 215 16 47 21 56 13 126 28 191 16 17 15 30 15 17 24 67 51 49 13 16 383 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 198 204 259 155 143 116 91 95 112 89 39 51 72 19 36 30 76 14 51 30 32 39 25 26 23 10 16 18 23 35 26 13 25 7 1. 48 1. 31 1. 54 1. 25 1. 43 1. 21 0.95 1. 24 1. 97 1.11 1. 85 0.97 1. 60 2.29 1. 37 4.87 2 .11 1. 36 1. 51 3.98 1. 75 3.06 1. 48 3.34 1. 44 0.53 1. 30 3.86 1. 35 1. 33 1. 35 5.36 2.13 2.08 149.74 154.57 174.93 186.45 233.97 372.69 418.24 478.12 483.75 592.13 601.04 677.73 705.06 898.35 927.19 961.49 1024.40 1048.08 1168. 34 1203.93 1220.43 1237.79 1326.02 1352.44 1455.73 1633.90 1723.41 1736.07 1825.49 1941.06 2242.38 2367.85 2480.60 2925.80 142 142 169 183 227 369 414 472 472 585 597 672 699 894 922 955 1014 1044 1161 1197 1211 1229 1321 1345 1448 1628 1717 1729 1817 1935 2234 2360 2476 2919 19 3.50E-02 23.2 l.55E+OO 19 4.74E-02 16.4 11 1.09E-02 81.4 8 8.22E-03 81.9 10 9.21E-03 70.4 10 1.96E-02 32.4 8 1.17E-02 42.2 24 9.45E-02 7.2 2.49E+OO 24 2.88E-02 29.0 11 3.46E-02 17.1 8 9.39E-03 36.6 12 2.22E-02 21.1 12 5.98E-02 10.6 9 4.56E-03 52.9 12 1. 31E-02 27. 2 13 5.97E-03 56.3 22 1.57E-02 45.7 9 3. 4*7E-03 60 .1 16 3.50E-02 15.1 15 7.78E-03 46.6 18 5.29E-02 10.2 17 4.41E-03 92.8 9 4.66E-03 62.3 13 4.14E-03 75.2 13 8.43E-03 37.1 11 4.07E-03 50.7 12 4.76E-03 54.5 17 6.73E-03 44.1 15 1.86E-02 20.0 14 1. 42E-02 28. 3 16 1.37E-02 28.0 13 3.61E-03 63.5 9 4. 4 6E-03 61. 2 13 1.07E-01 5.3 Peak Search Report (continued) Sample ID : G405235041 Pk It Energy Area Bkgnd 35 0 1540.81 9 0 36 0 1765.92* 28 8 37 0 1848.94 13 3 FWHM 0.62 2.73 1. 48 Flag: "*" = Peak area was modified by Page 3869 of 5809 Acquisition date Channel Left Pw. 3083.89 3079 10 3534.45 3526 16 3700.61 3695 10 Page : 2 3-0CT-2016 05:54:08 Cts/Sec %Err Fit 2.50E-03 33.3 7.85E-03 30.2 3.74E-03 35.0 background subtraction VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 06:57:28 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 13:27:00 G405235041 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:54:08 181.48 GRAM
Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA28 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB'-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3870of5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.41 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.237E+OO l.183E+Ol l.183E+Ol 10.64 OK CD-109 88.03 3.70* 5.432E+OO 4.268E-01 6.777E-01 447.68 OK SN-126 64.28 9.60 3.124E+OO Line Not Found -----Absent 86.94 8.90 5.432E+OO 1. 775E-01 l.775E-01 447.68 OK 87.57 37.00* 5.432E+OO 4.268E-02 4.268E-02 447.68 OK BA-137M 661.66 89.90* 2.304E+OO 3. 721E-02 3.794E-02 124.68 OK CS-137 661. 66 85.10* 2.304E+OO 3.931E-02 4.008E-02 124.68 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2.539E+OO 2.731E-01 2. 731E-01 30.19 OK 860.56 12.50 l.887E+OO 3.210E-01 3.210E-01 108. 96 OK BI-211 72. 87 1. 23 4.138E+OO Line Not Found Absent 351.06 12.92* 3.783E+OO 8.826E-03 8.826E-03******* OK PB-212 74.82 10.28 4.344E+OO 1.256E+OO 1.256E+OO 64.18 OK 77 .11 17.10 4.585E+OO 1. 313E+OO 1.313E+OO 32.89 OK 238.63 43.60* 5.101E+OO 8.071E-01 8. 071E-01 14.30 OK 300.09 3.30 4.293E+OO 1.224E+OO 1.224E+OO 73.14 OK BI-214 609.32 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 OK 1120.29 14.92 1.539E+OO 9 .14-9E-01 9.152E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 OK PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.585E+OO 2.315E+OO 2.316E+00 32.89 OK 87.09 3.41 5.409E+OO Line Not Found <<INT Reject 242.00 7.25 5.054E+OO Line Not Found <<INT Reject 295.22 18.42 4.343E+OO 7.994E-01 7.997E-01 34.29 OK 351. 93 35.60* 3.786E+OO Line Not Found <<INT Reject RN.,-222 609.32 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 OK 1120.29 14.92 l.539E+OO 9.149E-01 9.152E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 OK RA-224 240.99 4.10* 5.059E+OO l.221E+OO 1.221E+OO 131. 43 OK RA-226 609.32 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 OK 1120.29 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-:-Ol 6.977E-01 60.31 OK AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.153E-01 9.153E-01 42.22 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 1.930E+OO Line Not Found Absent 911. 20 25.80* 1.806E+OO 6.291E-01 6.291E-Ql 39.97 OK 968. 97 15.80 1. 723E-too 8.137E-01 8.137E-01 56.63 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.153E-01 9.153E-01 42.22 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 l.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 OK 968. 97 15.80 1. 723E+OO 8.137E-01 8.137E-01 56.63 OK TH-228 74.82 10.28 4. 344E+oo* l.256E+OO 1.256E+OO 64.18 OK 77 .11 17.10 4.585E+OO 1. 313E+OO 1.313E+OO 32.89 OK 238.63 43.60* 5.101E+OO 8.071E-01 8. 071E-01 14.30 OK 300.09 3.30 4.293E+OO 1.224E+OO 1.224E+OO 73.14 OK TH-230 609.32 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 OK Page 3871 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 l.539E+00 9.149E-01 9.149E-01 55.98 OK 1764.49 15.30 *1. 044E+OO 6.974E-01 6.974E-01 60.31 OK PA-231 283.69 1. 70 4.487E+OO Line Not Found Absent 301.36 5.35* 4.293E+OO 7.547E-01 7.547E-01 73.14 OK TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.153E-01 9.153E-01 42.22 OK 835.71 1. 61 1.930E+OO Line Not Found Absent 911. 20 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 OK 968. 97 15.80 1. 723E+OO 8.137E-01 8."137E-01 56.63 OK U-234 609.32 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 OK 1120.29 14.92 l.539E+OO 9.149E-01 9.149E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-01 6.974E-01 60.31 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.344E+OO 1.922E-01 l.922E-01 64.18 OK ANH-511 511. 00 100.00* 2.812E+OO 9.561E-02 9.561E-02 91. 39 OK Flag: "*" = Keyline Page 3872 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:57:29.76 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l *
Acquisition date 3-0CT-2016 05:54:08 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.41 Half life : ***** *
Sample date 30-NOV-2015 13:27:00 Analyst initials: MXRl *
Sample ID G405235041 Sample Quantity l.8148E+02 *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lo
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.183E+Ol 1.233E+OO 4.280E-01 CD-109 6.777E-01 2.973E+OO 2.012E+OO SN-126 4.268E-02 1.873E-01 l.275E-01 BA-137M 3.794E-02 4.636E-02 5.412E-02 CS-137 4.008E-02 4.898E-02 5.717E-02 TL.-208 2. 731E-01 8.080E-02 4.938E-02 BI-211 8.826E-03 8.712E-01 2.838E-01 PB-212 8. 071E-01 l.131E-01 7.667E-02 BI-214 7.942E-01 1.594E-01 8.436E-02 PB-214 8.029E-01 l.668E-01 2.522E-01 RN-222 7.942E-01 l.594E-01 8.436E-02 RA-224 1. 221E+OO l.572E+00 8.215E-01 RA-226 7.942E-01 l.594E-01 8.436E-02 AC-228 6.291E-01 2.464E-01 2.040E-01 RA-228 6.291E-01 2.040E-01 TH-228 8. 071E-01 l.131E-01 7. 667E-0.2 TH-230 7.939E-01 l.594E-01 8.433E-02 PA-231 7.547E-01 5.410E-01 6. 421E-01 TH-232 6.291E-01 2.464E-01 2.040E-01 U-234 7.939E-01 1.594E-01 8.433E-02 AM-243 1.922E-01 l.209E-01 8.042E-02 ANH-511 9.561E-02 8.563E-02 4.218E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -2.191E-01 l.151E+Ol 2.013E+Ol NOT IDENT. NA-22 -3.133E-03 4.147E-02 8.013E-02 NOT IDENT. NA-24 O.OOOE+OO 1.640E+41 O.OOOE+OO SHORT HLIF AL-26 9.807E-03 1.932E-02 5.027E-02 NOT IDENT. SC-46 -5.154E-02 3.074E-01 6.107E-01 FAIL ABUN V-48 O.OOOE+OO 1. 631E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4 .11'4E+02 O.OOOE+OO SHORT HLIF MN-54 -1.507E-02 4.486E-02 8.755E-02 NOT IDENT. Page 3873 of 5809 C0-56 2.359E-01 3.183E-01 7.383E-01 FAIL ABUN MN-56 O.OOOE+OO 1.330E+41 O.OOOE+OO SHORT HLIF C0-57 2.007E-02 3.755E-02 7.512E-02 NOT IDENT. C0-58 -5.366E-01 5.507E-01 7.859E-01 NOT IDENT. FE-59 -2.765E+OO 7.132E+OO 1.321E+Ol NOT IDENT. C0-60 1. 676E-02 3.302E-02 7.121E-02 NOT IDENT. ZN-65 3.236E-02 l.379E-01 2.582E-01 NOT IDENT. GE-68 3.568E-01 l.967E+OO 4. llOE+OO NOT IDENT. AS-73 7 .118E-01 7.667E+OO l.542E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.412E+03 O.OOOE+OO SHORT HLIF SE-75 3.921E-02 1.560E-01 3.226E-01 NOT IDENT. BR-77 O.OOOE+OO 2.013E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.619E+02 O.OOOE+OO SHORT HLIF RB-83 -7.956E-02 5.151E-01 8.069E-01 NOT IDENT. KR-85 l.199E+Ol 6.695E+OO l.484E+Ol NOT IDENT. SR-85 1. 37 4E+OO 7.680E-01 1. 702E+OO NOT IDENT. RB-86 O.OOOE+OO 3.086E+04 O.OOOE+OO SHORT HLIF Y-88 -3.347E-02 l.661E-01 3.512E-01 NOT IDENT. y:....91 -8.323E+Ol 4.945E+02 9.417E+02 NOT IDENT. NB-94 3.764E-03 2.770E-02 5.314E-02 NOT IDENT. NB-95 -2.157E-01 7.525E-01 *l. 468E+OO NOT IDENT. NB-95M 6.486E-01 2.187E+OO 4.070E+OO NOT IDENT. ZR-95 -4.732E-01 l.213E+OO 2.353E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.670E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+.41 O.OOOE+OO SHORT HLIF RH-101 7.707E'...04 2.980E-02 5.632E-02 NOT IDENT. RH-102 7.192E-03 4.975E-02 9. 731E-02. NOT IDENT. RU-103 4.882E+OO 4.914E+OO l.085E+Ol FAIL ABUN RH-106 -6.489E-02 4.481E-01 7.483E-01 NOT IDENT. RU-106 -6.489E-02 4.481E-01 7.483E-01 NOT IDENT. AG-108M -1.657E-03 2 .181E-02 4.250E-02 NOT IDENT. AG-llOM -2.353E-02 6.819E-02 l.333E-01 NOT IDENT. SN-113 -l.516E-01 l.871E-01 3.351E-01 NOT IDENT. CD-115 0.000E+OO 2.626E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.185E+05 O.OOOE+OO SHORT HLIF TE*d23M 4.146E-02 1.180E-01 2.263E-01 NOT IDENT. SB-124 -5.395E-01 l.225E+OO . 2.288E+OO NOT IDENT. SB-125 -5.858E-02 7.809E-02 1.397E-01 FAIL ABUN TE-125M 3.575E+02 2.626E+02 5.525E+02 NOT IDENT. I-126 O.OOOE+OO l.294E+06 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 1. 650E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.770E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.049E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.684E+27 O.OOOE+OO SHORT HLIF BA-133 5.065E-03 3.547E-02 6.415E-02 NOT IDENT. I-133 O.OOOE+OO 1.811E+41 O.OOOE+OO SHORT HLIF CS-134 2.947E-02 3.597E-02 8.122E-02 NOT IDENT. CS-135 -3.974E-02 1.121E-01 2.176E-01 NOT IDENT. I-135 O.OOOE+OO 1. 017E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4. 021E+05 O.OOOE+OO SHORT HLIF CE-139 -2.894E-02 8.760E-02 1. 763E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 663E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.030E+05 O.OOOE+OO SHORT HLIF CE-141 -4.633E+OO 2.484E+Ol 4.568E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.477E-01 2.927E-01 5 . .104E-01 NOT IDENT. PM-144 -7.349E-03 4.538E-02 8.436E-02 FAIL ABUN PR-144 -6.410E-01 3.959E+OO 7.358E+OO NOT IDENT. PM-146 4.002E-02 3.280E-02 7. 211E-02 NOT IDENT. ND-147 O.OOOE+OO 4 .119E+07 O.OOOE+OO SHORT HLIF PM-:147 -2.057E+02 6.735E+02 l.248E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -l .. 533E-02 1. 960E-02 3.lOlE-02 FAIL ABUN EU-152 -3.274E-02 7.623E-02 l.371E-01 NOT IDENT. GD-153 -2.430E-02 l.542E-01 2.939E-01 NOT IDENT. EU-154 -7:654E-03 l.013E-01 l.957E-01 NOT IDENT. EU-155 l.440E-01 9.169E-02 1. 967E-01 FAIL ABUN TB-160 -l.598E-01 l.485E+OO 2.989E+OO FAIL ABUN H0-166M 4.164E-02 4.165E-02 9.240E-02 NOT J:DENT. TM-171 3.747E+00 1. 817E+Ol 3.684E+Ol NOT IDENT. HF-172 l.520E-01 l.927E-01 3.887E-01 NOT IDENT. LU-172 -1. 882E-02 5.670E-02 l.080E-01 FAIL ABUN LU-176 -l.850E-04 2.079E-02 4.115E-02 FAIL ABUN HF-181 -l.030E+OO 4.586E+OO 7.676E+OO NOT IDENT. TA-182 8.049E-02 8.034E-01 l.591E+OO FAIL ABUN Page 3874 of 5809 RE-183 7.150E-01 2. 591E+OO 5.320E+OO NOT IDENT. RE-184 -9.123E+OO 2.949E+Ol 5.672E+Ol NOT IDENT. W-188 -7.636E+Ol l.150E+02 l.905E+02 NOT IDENT. IR-192 -l.241E-Ol 4.075E-01 7.863E-01 FAIL ABUN HG-203 1.115E+OO 2.026E+OO 4.255E+OO NOT IDENT. BI-207 -5.187E-03 3. 713E-02 7.285E-02 FAIL ABUN PB-210 2.871E-01 2 .. 941E+OO 5. 962E+OO NOT IDENT. PB-211 1.675E-01 5.050E-01 l.033E+OO NOT IDENT. BI-212 9.611E-01 6.997E-01 9.733E-01 FAIL ABUN RN-219 9.597E-02 2. 962E-01 6.035E-01 NOT IDENT. RA-223 1.121E-01 4.307E-01 8.828E-01 FAIL ABUN AC-227 3.136E-02 1. 768E-01 3.607E-01 FAIL ABUN TH-227 3.136E-02 1. 768E-01 3.607E-01 FAIL ABUN TH-229 -1.910E-01 3. 872E-01 7.594E-01 FAIL ABUN TH-231 1.121E-01 4.307E-01 8.828E-01 FAIL ABUN PA-233 -1.434E-02 4.449E-02 8.618E-02 FAIL ABUN PA-234 6.026E-03 2.016E-01 4.124E-01 NOT IDENT. PA-234M -2.242E+OO 3.002E+00 5.820E+OO NOT IDENT. TH-234 1. 378E-01 1. 031E+OO 2.078E+OO FAIL ABUN U-235 8.410E-02 1.545E-01 3.035E-01 FAIL ABUN NP-237 -l.434E-02 4.449E-02 8.618E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 1.378E-01 1. 031E+OO 2.078E+OO FAIL ABUN NP-239 3.654E-01 5.044E-01 4.283E-01 . FAIL ABUN PU-239 1. 305E+02 2.816E+02 5.474E+02 NOT IDENT. AM-241 5.439E-02 1.190E-01 2.450E-01 NOT IDENT. CM-243 -l.148E-01 8.637E-02 1.472E-01 NOT IDENT. BK-247 -3.643E-03 5.211E-02 'l. 04 7E-01 NOT IDENT. CM-247 7.164E-03 2.740E-02 5.541E-02 NOT IDENT. CF-249 1. 758E-02 2.798E-02 5.915E-02 NOT CF-251 -2.456E-03 8.975E-02 l.833E-01 NOT IDENT. Page 3875 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:57:26.91 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 377 10.66* 1.237E+OO 1.183E+Ol 1.183E+Ol 10.64 CD-109 88.03 57 3.70* *5.432E+OO l.164E+OO 1-. 84 7E+OO 162.79 SN-126 64.28 ------9.60 3.124E+OO ------Line Not Found ------86.94 57 8.90 5.432E+OO 4.837E-01 4. 837E-01* 162.79 87.57 57. 37.00* 5.432E+OO l.164E-01 l.164E-01 162.79 BA-137M 661.66 19 89.90* 2.304E+OO 3.721E-02 3.794E-02 124.68 CS-137 661.66 19 85.10* 2.304E+OO 3. 931E-02 4.008E-02 124.68 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 142 85.00* 2.539E+00 2. 731E-01 2. 731E-01 30.19 860.56 18 12.50 1.887E+OO 3.210E-01 3.210E-01 108.96 BI-211 72. 87 ------1. 23 4.138E+OO ------Line Not Found ------351. 06 261 12.92* 3.783E+OO 2. 211E+OO 2.211E+OO 21. 20 PB-212 74.82 184 10.28 4.344E+OO 1. 707E+OO 1.707E+OO 46.35 77 .11 249 17.10 4 . .585E+00 l.313E+00 1.313E+OO 32.89 238.63 434 43.60* 5.101E+OO 8. 071E-01 8. 071E-01 14.30 300.09 42 3.30 4.293E+00 *1. 224E+OO 1.224E+OO 73.14 BI-214 609.32 214 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 . 9.152E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 .6. 977E-01 60.31 PB-214 74.82 184 5.80 4.344E+OO 3.026E+OO 3.027E+OO 46.35 77 .11 249 9.70 4.585E+00 2.315E+OO 2.316E+OO 32.89 87.09 57 3.41 5.432E+OO l.263E+OO l.263E+OO 162.79 242.00 132 7.25 5.059E+OO 1.490E+OO 1.490E+OO 58.06 295.22 155 18.42 4.343E+OO 7.994E-01 7.997E-01 34.29 351. 93 261 35.60* 3.783E+OO 8.026E-01 8.029E-01 21. 20 RN-222 609.32 214 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 1764.49 27 15.30 l.044E+00 6.974E-01 6.977E-01 60.31 RA-224 240.99 132 4.10* 5.059E+00 2.634E+OO 2.634E+OO 58.06 RA-226 609.32 214 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 1120.29 51 14.92 1.539E+OO 9 .149E-.01 9.152E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 AC-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 97 11. 27 3.904E+00 9.153E-01 9.153E-01 42.22 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------9.11. 20 71 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 968.97 54 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 97 11.27 3.904E+OO 9.153E-01 9.153E-01 42.22 794.95 ------4.25 2.005E+OO ------Line Not Found ------835. 71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 71 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 968. 97 54 15.80 1. 723E+OO 8.137E-01 8.137E-01 56.63 TH-228 74.82 184 10.28 4.344E+OO l.707E+00 1.707E+OO 46.35 77 .11 249 17.10 4.585E+OO 1.313E+OO 1. 313E+OO 32.89 238.63 434 43.60* 5 .101E+OO 8.071E-01 8. 071E-01 14.30 Page 3876 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy* Area %Abn %Ef f pCi/GRAM pCi/GRAM %Error 300.09 42 3.30 4.293E+OO 1.224E+OO 1.224E+00 73.14 TH-230 609.32 214 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.149E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 6.974E-01 60.31 PA-231 283.69 ------1. 70 4.487E+OO ------Line Not Found ------301.36 42 5.35* 4.293E+OO 7.547E-01 7.547E-01 73.14 TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 97 11.27 3.904E+OO 9.153E-01 9.153E-01 42.22 835. 71 ------1. 61 l.930E+OO ------Line Not Found ------911. 20 71 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 968. 97 54 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 U-234 609.32 214 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.149E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 6.974E-01 60.31 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 184 67.20* 4.344E+OO 2.612E-01 2.612E-01 46.35 ANH-511 511. 00 65 100.00* 2.812E+OO 9.561E-02 9.561E-02 91. 39 Flag: "*" Key line Page 3877of5809 Summary of Nuclide Activity Sample ID : G405235041 Acquisition date Page : 3 3-0CT-2016 05:54:08 Total number of lines in spectrum 37 Number of unidentified lines 8 Number of lines tentatively identified by NID 29 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M
CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+OBY 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+10Y 1600. OOY 1.41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 59 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1*. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.183E+Ol 1.164E+OO l.164E-01 3. 721E-02 3.931E-02 2.731E-01 2. 211E+OO 8. 071E-01 7.939E-01 8.026E-01 7.939E-01 2.634E+OO 7.939E-01 6.291E-01 6.291E-01 8.071E-01 7.939E-01 7.547E-01 6.291E-01 7.939E-01 2.612E-01 9.561E-02 2.769E+Ol 2.769E+Ol Decay Corr pCi/GRAM 1.183E+Ol l.847E+OO l.164E-01 3.794E-02 4.008E-02 2. 731E-01 2.211E+OO 8. 071E-01 7.942E-01 8.029E-01 7.942E-01 2.634E+OO 7.942E-01 6.291E-01 6.291E-01 8. 071E-01 7.939E-01 7.547E-01 6.291E-01 7.939E-01 2.612E-01 9.561E-02 2.837E+Ol 2.837E+Ol 78.38% Decay Corr 2-Sigma Error 0.126E+Ol 3.007E+OO 1. 8 94E-01 4.731E-02 4.998E-02 0.824E-01 0.469E+OO 1.154E-01 1.627E-01 1. 702E-01 1.627E-01 1.530E+OO l.627E-01 2.514E-01 2.514E-01 1.154E-01 l.626E-01 5.520E-01 2.514E-01 l.626E-01 1.210E-01 8.738E-02 "M" Manually accepted 2-Sigma %Error 10.64 162.79 162.79 124.68 124.68 30.19 21. 20 14.30 20. 48 21. 20 20.48 58.06 20.48 39.97 39.97 14.30 20.48 73.14 39.97 20.48 46:35 91. 39 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit . Page 3878 of 5809 Flags Unidentified Energy Lines Page : 4 SampJ,e ID : G405235041 Acquisition date : 3-0CT-2016 05:54:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 93.17 42 222 1. 25 186.45 183 8 8.22E-03 **** 5.79E+OO T 0 116. 91 46 199 1. 43 233.97 227 10 9.21E-03 **** 6.57E+OO T 0 186.22 93 152 1. 21 372.69 369 10 1. 96E-02 64.7 5.98E+OO T 0 208.98 55 118 0.95 418.24 414 8 1. l 7E-02 84.4 5.58E+OO 0 448.85 19 22 2.29 898.35 8 94 9 4.56E-03 **** 3.12E+OO 0 463.26 55 42 1. 37 927.19 922 .12 1.31E-02 54.5 3.04E+OO T 0 480.40 25 34 4.87 961. 49 955 13 5.97E-03 **** 2. 96E+OO 0 523.66 14 16 1. 36 1048.08 1044 9 3.47E-03 **** 2.76E+00 T 0 601.53 32 34 3.98 1203.93 1197 15 7.78E-03 93.3 2.48E+OO T 0 618.45 18 44 3.06 1237.79 1229 17 4.41E-03 **** 2.43E+OO T 0 675.73 16 29 3.34 1352.44 1345 13 4.14E-03 **** 2.27E+OO 0 727.33 33 25 1. 44 1455.73 1448 13 8.43E-03 74.3 2.15E+OO T* 0 816.35 16 11 0.53 1633.90 1628 11 4.07E-03 **** l.97E+OO T 0 867.40 26 19 3.86 1736.07 1729 17 88.3 l.88E+00 0 1183. 05 13 13 5.36 2367.85 2360 13 3.61E-03 **** 1.47E+OO 0 1239.39 16 25 2.13 2480.60 2476 9 4.46E-03 **** 1. 42E+OO T. 0 1540.81 9 0 0.62 3083.89 3079 10 2.50E-03 66.7 1.18E+OO 0 1848.94 13 2 1. 48 3700.61 3695 10 3.74E-03 70.0 9.99E-01 Flags: "T" = Tentatively associated Page 3879of5809 VAX/VMS Nuclide Identification Report 03-0CT-2016 06:57:46.05 *******************************************************************************
GEL Laboratories LLC" *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l * *Acquisition date. 3-0CT-2016 05:54:08 Sensitivity 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.41 Half life ratio : ***** *
Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
Sample ID G405235041 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *'
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM 1. 709E-01. 9.572E-01 6.063E-02 2.419E-02 2.555E-02 2.197E-02 1.297E..:.01 3.562E-02 3.693E-02 1.217E-01 3.693E-02 3.817E-01 3.693E-02 8.962E-02 8. 962E-02 3.562E-02 3.691E-02 2.948E-01 8. 962E-02 3.691E-02 3.805E-02 1.899E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54. C0-56 Page 3880 of 5809 Le _(pCi/GRAM 9.013E+OO 3.492E-02 O.OOOE+OO 1. 960E-02 2.653E-01 O.OOOE+OO O.OOOE+OO 3.782E-02 3. 211E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 . BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-.140 LA-14*0 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3881 of 5809 O.OOOE+OO 3.517E-02 3.330E-01 5.822E+OO 3.085E-02 1.115E-01 1.808E+OO 7.186E+OO O.OOOE+OO 1.485E-01 O.OOOE+OO O.OOOE+OO 3.473E-01 6.908E+OO 7.923E-01 0.000E+OO 1.339E-01 4.129E+02 2.392E-02 6.551E-01 1.903E+OO 1.033E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 2.653E-02 4.354E-02 4.907E+OO 3.308E-01 3.308E-01 1. 920E-02 5.654E-02 1.507E-01 O.OOOE+OO O.OOOE+OO 1.063E-01 7.659E-01 6.222E-02 2.616E+02 O.OOOE+OO O.OOOE+OO *o. OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.936E-02 O.OOOE+OO 3.612E-02 l.007E-01 O.OOOE+OO 0.000E+OO 8.243E-02 O.OOOE+OO O.OOOE+OO 2.148E+Ol O.OOOE+OO 2.375E-01 3.742E-02 3.264E+OO 3.278E-02 O.OOOE+OO 5.832E+02 O.OOOE+OO 1.390E-02 6.245E-02 1.383E-01 8.526E-02 9.310E-02 1.296E+OO 4.126E-02 1. 723E+Ol 1.831E-01 4.605E-02 1.906E-02 3.456E+OO 7.004E-01 2.491E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT I DENT .. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT"HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF *NOT I DENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3882 of 5809 2.491E+Ol 8.802E+Ol 3.615E-01 1. 970E+OO 3.154E-02 2.790E+OO 4.700E-01 4.460E-01 2.753E-01 4.043E-01 1. 672E-01 1.672E-01 3.561E-01 4.043E-01 3.935E-02 1. 788E-01 2.502E+OO 9.821E-01 l.433E-01 3.935E-02 O.OOOE+OO 9.821E-01 2.023E-01 2.590E+02 1.155E-01 6.873E-02 4.808E-02 2.528E-02 2.700E-02 8.589E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:57:52.29 *******************************************************************************

GEL Laboratories LLC * *
2040 Savage Road * *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l * *Acquisition date 3-0CT-2016 05:54:08 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.41 Half life ratio : ***** *
Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
Sample ID G405235041 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
Quantity Err(%) : 1.1020E-03 % *
Wet wt corr 1.00000 Wet Weight
0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity .Nuclide (pCi/GRAM K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 1.183E+Ol 6.777E-01 4.268E-02 3.794E-02 4.008E-02 2.731E-01 8.826E-03 8.071E-01 7.942E-01 8.029E-01 7.942E-01 1.221E+OO 7.942E-01 6.291E-01 6.291E-01 8.071E-01 7.939E-01 7.547E-01 6.291E-01 7.939E-01 l.922E-01 9.561E-02 Act Error ( 1. 96-sigma) l.380E+00 2.977E+OO l.875E-01 4.639E-02 4. 901E-02 8.164E-02 8.817E-01 l.211E-01 l.631E-01 l.702E-01 l.631E-01 l.577E+OO 1. 631E-01 2.485E-01 2.485E-01 1. 211E-01 1. 630E--Ol 5.645E-01 2.485E-01 1.630E-01 1.218E-01 8.572E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 3883 of 5809 Key-Line Activity (pCi/GRAM -2 .191E-01 -3.133E-03 1. 000E+41 . 9.807E-03 -5.154E-02 2.863E+03 -1. 913E+02 -l.507E-02 K.L Act error (1. 96-sigma) 1.151E+Ol 4.147E-02 1. 700E+41 1.933E-02 3.074E-01 1.631E+04 4 .115E+02 4.487E-02 TPU ( 1. 96-sigma) 1.380E+OO 2.977E+OO 1. 87 5E-01 4.639E-02 4. 901E-02 8.164E-02 8.817E-01 1. 211E-01 1.631E-01 1.702E-01 1.631E-01 1.577E+OO 1. 631E-01 2. 485E-Ol. 2.485E-01 1.211E-01 l.630E-01 5.645E-01 2.485E-01 l.630E-01 1.218E-01 . 8. 572E-02 TPU (1.96-sigma) l.151E+Ol '-4 .149E-02 O.OOOE+OO 1.983E-02 3.082E-01 l.636E+04 4.204E+02 4.538E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 2.359E-01 3.184E-01 3.357E-01 FAIL ABUN MN-56 1.000E+41 1.330E+41 O.OOOE+OO SHORT HLIF C0-57 2.007E-02 3.756E-02 3. 8 64E-02 NOT IDENT. C0-58 -5.366E-01 5.512E-01 6.020E-01 NOT IDENT. FE-59 -2.765E+OO 7.135E+OO 7.243E+OO NOT IDENT. C0-60 1. 676E-02 3.302E-02 3.387E-02 NOT IDENT. ZN-65 3.236E-02 l.379E-01 1. 386E-01 NOT IDENT. GE-68 3.568E-01 1. 967E+OO 1.974E+OO NOT IDENT. AS-73 7 .118E-01 7.668E+OO 7.675E+OO NOT IDENT. AS-74 -7.144E+02 6.412E+03 6.420E+03 SHORT HLIF SE-75 3.921E-02 l.560E-01 1.570E-01 NOT IDENT. BR-77 1.436E+39 1.275E+40 O.OOOE+OO SHORT HLIF SR-82 -l.409E+02 6.620E+02 6.650E+02 SHORT HLIF RB-83 -7.956E-02 5.153E-01 5.165E-01 NOT IDENT. KR-85 l.199E+Ol 6. 713E+OO 8.619E+OO NOT IDENT. SR-85 1. 37 4E+OO 7.701E-01 9.882E-01 NOT IDENT. RB-86 -l.011E+03 3.086E+04 3.086E+04 SHORT HLIF Y-88 -3.347E-02 l.661E-01 1.668E-01 NOT IDENT. Y-91 -8.323E+Ol 4.945E+02 4.959E+02 NOT IDENT. NB-94 3.764E-03 2.770E-02 2.775E-02 NOT IDENT. NB-95 -2.157E-01 7.525E-01 7.588E-01 NOT IDENT. NB-95M 6.486E-01 2.188E+OO 2.207E+OO NOT IDENT. ZR-95 -4.732E-01 1.214E+OO l.232E+OO NOT IDENT. NB-97 1. OOOE+41 2 .113E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 2.218E+41* O.OOOE+OO SHORT HLIF M0-99 -6.514E+32 9.682E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 2.065E+41 O.OOOE+OO SHORT HLIF RH-101 7.707E-04 2.980E-02 2.980E-02 NOT IDENT. RH-102 7.192E-03 4.975E-02 4.986E-02 NOT IDENT. RU-103 4.882E+OO 4.920E+OO 5.390E+OO FAIL ABUN RH-106 -6.489E-02 4.481E-01 4.490E-01 NOT IDENT. RU-106 -6.489E-02 4.481E-01 4.490E-01 NOT IDENT. AG-108M -l.657E-03 2.181E-02 2.183E-02 NOT IDENT. AG-llOM -2.353E-02 6.820E-02 6.902E-02 NOT IDENT .. SN-113 -l.516E-01 l.872E-01 1.992E-01 NOT IDENT. CD-115 1.503E+40 2.640E+40 0.000E+OO SHORT HLIF SN-117M 6.715E+04 1.187E+05 1.225E+05 SHORT HLIF TE-123M 4.146E-02 l.181E-01 l.195E-01 NOT IDENT. SB-124 -5.395E-01 1.225E+OO l.249E+OO NOT IDENT. SB-125 -5.858E-02 7.813E-02 8.247E-02 FAIL ABUN TE-125M 3.575E+02 2.634E+02 3.088E+02 NOT IDENT. I-126 6.654E+04 1.294E+06 l.294E+06 SHORT HLIF SB-126 9.420E+05 1. 660E+06 l.713E+06 SHORT HLIF SB-127 -3.575E+22 9.264E+22 O.OOOE+OO SHORT HLIF I-131 -5.677E+09 8.053E+09 8.450E+09 SHORT HLIF I-132 -1.000E+41 l.909E+42 0.000E+OO SHORT HLIF TE-132 4.747E+26 l.695E+27 O.OOOE+OO SHORT HLIF BA-133 5.065E-03 3.547E-02 3.554E-02 NOT IDENT. I-133 -1.000E+41 2.594E+41 O.OOOE+OO SHORT HLIF CS-134 2.947E-02. 3.599E-02 3.836E-02 NOT IDENT. CS:-135 -3.974E-02 1.121E-01 1.135E-01 NOT IDENT. I-135 1.000E+41 7.026E+41 0.000E+OO SHORT HLIF CS-136 -4.347E+04 4.022E+05 4.026E+05 SHORT HLIF CE-139 -2.894E-02 8.780E-02 8.876E-02 NOT IDENT. BA-140 -8.930E+05 1.664E+06 1.712E+06 SHORT HLIF LA-140 -7.616E+04 6.030E+05 6.040E+05 SHORT HLIF CE-141 -4.633E+OO 2.484E+Ol 2.493E+Ol NOT IDENT. CE-143 -1.000E+41 3.231E+41 O.OOOE+OO SHORT HLIF CE-144 -2.477E-01 2. 931E-01 3.136E-01 NOT IDENT. PM-144 -7.349E-03 4.539E-02 4. 551E-02 FAIL ABUN PR-144 -6.410E-01 3.959E+OO 3. 969E+OO NOT IDENT. PM-146 4.002E-02 3.292E-02 3.754E-02 NOT IDENT. ND-147 -2.792E+07 4.122E+07 4.309E+07 SHORT HLIF PM-147 -2.057E+02 6.736E+02 6.799E+02 NOT IDENT. PM-149 6.814E+40 4.470E+41 O.OOOE+OO SHORT HLIF EU-150 -1. 533E-02. 1. 961E-02 2.080E-02 FAIL ABUN EU-152 -3.274E-02 7.625E-02 7.766E-02 NOT IDENT. GD-153 .:...2.430E-02 1.542E-01 1.546E-01 NOT IDENT . EU-154 -7.654E-03 l.013E-01 1.013E-01 NOT IDENT. EU-155 l.440E-01 9.226E-02 l.128E-01 FAIL ABUN TB-160 -1.598E-01 1.485E+OO 1.487E+OO FAIL ABUN H0-166M 4.164E-02 4. l 72E-02 4.574E-02 NOT IDENT. TM-171 3.747E+OO 1. 817E+Ol 1.825E+Ol NOT IDENT. HF-172 1.520E-01 l.943E-01 2.060E-01 NOT IDENT. LU-172 -1.882E-02 5.674E-02 5.737E-02 FAIL ABUN LU-176 -1.850E-04 2.079E-02 2.079E-02 FAIL ABUN HF-181 -1.030E+OO 4.586E+OO 4.610E+OO NOT IDENT. TA-182 8.049E-02 8.034E-01 8.043E-01 FAIL ABUN Page 3884 o.f 58.09 RE-183 7.lSOE-01 2.594E+OO 2.614E+OO NOT IDENT. RE-184 -9:123E+OO 2.957E+Ol 2.986E+Ol NOT IDENT. W-188 -7.636E+Ol 1. 153E+02 1. 203E+02 NOT IDENT. IR-192 -1.241E-01 4.075E-01 4 .113E-01 FAIL ABUN , HG-203 1.llSE+OO 2.027E+OO 2.088E+OO NOT IDENT. BI-207 .-5.187E-03 3.713E-02 3.720E-02 FAIL ABUN PB-210 2. 871E-01 2.941E+OO 2.944E+OO NOT IDENT. PB-211 l.675E-01 5.0SlE-01 s*.107E-01 NOT IDENT. BI-212 9.611E-01 7.014E-01 8.244E-01 FAIL ABUN RN-219 9.597E-02 2. 964E-01 2. 996E-01 NOT IDENT. RA-223 l.121E-01 4.308E-01 4.337E-01 FAIL ABUN AC-227 3.136E-02 1. 768E-01 1.774E-01 FAIL ABUN TH-227 3.136E-02 1.768E-01 l.774E-01 FAIL ABUN TH-229 -l.910E-01 3.873E-01 3. 967E-01 FAIL ABUN TH-231 1.121E-01 4.308E-01 4.337E-01 FAIL ABUN PA-233 -1.434E-02 4.450E-02 4.497E-02 FAIL ABUN PA-234 6.026E-03 2.017E-01 2.018E-01 NOT IDENT. PA-234M -2.242E+OO 3.003E+OO 3.169E+OO NOT IDENT. TH-234 1. 378E-01 1.032E+OO 1.033E+OO FAIL ABUN U-235 8.410E-02 1.545E-01 1.591E-01 FAIL ABUN NP-237 -1.434E-02 4.450E-02 4.497E-02 FAIL ABUN NP-238 -1.000E+41 7.561E+41 O.OOOE+OO SHORT HLIF U-238 1.378E-01 1.032E+OO 1.033E+OO FAIL ABUN NP-239 3.654E-01 5.053E-01 5.315E-01 FAIL ABUN PU-239 1. 305E+02 2. 816E+02 2.877E+02 NOT IDENT. AM-241 5.439E-02 1.190E-01 l.215E-01 NOT IDENT .. CM-243 -l.148E-01 8.702E-02 l.012E-01 NOT IDENT. BK-247 -3.643E-03 5.212E-02 5.215E-02 NOT IDENT. CM-247 7.164E-03 2.742E-02 2.761E-02 NOT IDENT. CF-249 1. 758E-02 2.801E-02 2. 911E-02 NOT IDENT. CF-251 -2.456E-03 8.975E-02 8.976E-02 NOT IDENT. Page 3885 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 63.5639 87.09 127.2108 136.47 87.5808 45.60 77.5038 87.57 127.3091 140.51 0.0000 46.54 64.0330 88.03 127.4031 143.76 72.3906 49.72 0.0000 88.34 127.4672 144.24 74.8864 51. 35 57.3219 88.47 127.4937 145.44 87.2842 51. 87 53.1378 89. 96 95.8471 152.43 86.7427 52.39 61. 7115 1093.63 125.6492 153.25 0.0000 52.97 57.5295 91.11 0.0000 323.87 78.2232 53.44 57.5892 92.59 116.8675 156.02 0.0000 54.07 61.9405 93.35 117.0052 158.56 0.0000 57.36 0.0000 94.56 87.3433 159.00 72.3956 57.53 73.1602 94.65 87.3549 162.33 70.9864 57.98 65.6907 94.67 87.3578 162.66 0.0000 59.27 68.0267 94.87 87.3845 163.33 62.7029 59.32 77.7527 97.43 84.2620 165.86 *77.1224 59.54 77.7879 98.43 85.5444 176.31 67.7938 60.96 93.1830 98.44 85.5456 176.60 0.0000 61.17 102.9785 99.53 86.8429 177.52 74.6645 62.93 .76.1473 100 .11 64.8983 181.07 0.0000 63.29 81.6446 102.03 84.8384 181.52 74.6245 63.58 72.9776 103.18 93.1293 184.41 64.0739 64.28 74.1690 103.37 102.4711 143.76 76.9876 66.73 75.6177 105.21 63.0466 193.51 87.9125 67.24 82.2733 105.31 63.0555 197.03 80.4233 125.81 79.0488 106.12 86.5093 198.01 78.7660 67.75 79.0587 106.47 97.0795 201.83 63. 4116 69.67 95.5084 109.28 69.2820 203.43 73.9444 70.83 89.8233 111. 00 108.2912 205.31 58.8222 72.81 103. 0811 111.76 0.0000 210.85 57.8051 72. 87 103.0917 114.06 85.1061 215.65 62.4507 74.66 103.4245 116. 30 0.0000 222 .11 59.2670 74.82 103.4536 116.74 87.7864 227.09 65.7399 74.97 103.4812 119.76 65 .1114 227.38 57.7590 77 .11 103.8729 121.12 75.1711 228.16 0.0000 78.74 104.1674 121. 22 75.1807 228.18 59.5765 79.69 124.1581 121.78 64.4880 116.74 59.5765 80.12 110. 7764 122.06 59.7328 235.69 61. 7444 80.19 0.0000 122.92 71. 7 590 235.96 61.7578 80.57 110.8615 123.07 72. 9694 238.63 57.4095 81. 00 265.00 83.8011 238.98 0.0000 81. 07 107.9568 125.81 68.4246 240.99 57.5208 81. 75 106.5794 127.23 87.7889 242.00 57.5684 83.79 112.9684 127.91 104. 7154 244.70 57.6953 84.00 99.4471 129.30 90.4289 252.40 0.0000 85.43 126.8673 131. 20 73.7238 252.80 47.1827 86.55 127.0989 133. 02 78.7347 254.15 0.0000 86. 79 127.1484 133.52 81. 2064 256.23 50.9497 86.94 127.1792 136.00 79.0204 260.90 0.0000 Page 3886of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 40.2948 355.39 0.0000 584.27 21. 9295 264.80 39.3834 356.01 36.5707 595.83 0.0000 265.00 43. 9697 364.49 0.0000 427.87 23.1875 268.22 59.6878 366.42 0.0000 602.52 0.0000 269.46 50.5532 372.51 30.5383 604. 72 0.0000 270.03 45.9768 375.05 39.4645 607.14 16.6077 271.23 57.0629 377.52 29.6423 609.32 16.6229 273.65 0.0000 356.01 31.7370 610.33 16.6302 276.40 51. 7412 388.16 26.8456 614.28 9.9946 277.37 50.8542 388.63 0.0000 618.01 16.6833 277.60 50.8620 391.69 39.8535 620. 36 16.6992 278.00 49.9526 264.66 34.0505 621.93 21.7233 279.20 41.6638 401. 81 31. 0662 630.19 0.0000 279.54 44.4531 402.40 32.0794 631. 29 22.3657 279.70 46.3104 404.85 29.1121 633.25 21. 2 644 280.46 52.8240 410.95 33.2417 634.78 0.0000 283.69 50.1625 .413. 71 29.2572 635.95 25.7692 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 46.5047 423.72 0.0000 645.85 22.4976 285.90 0.0000 427.09 30.4901 657.76 11.8672 287.50 48.4379 427.87 33.5532 657.90 0.0000 290.67 60.2194 433.94 30.6030 661.66 23.7711 293.27 0.0000 439.40 22.5080 664.57 0.0000 351.93 44.9609 453.88' 16.0824 666.33 0.0000 295.96 44.9844 463.37 24.8638 666.50 0.0000 879.38 33.8005 468.07 23.3661 667.71 0.0000 299.98 26.7B54 473.00 0.0000 677.62 18.7935 300.09 26.7872 475.06 21. 8857 685.70 0.0000 300 .13 26.7878 476.78 20.3399 695.00 0.0000 301.36 42.3331 477.60 25.0439 696.49 22.9443 302.85 45.2021 482.18 31.3763 696. 51 22.9443 256.23 47.5176 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 27.5420 306.78 52.8805 497.08 16.8574 697.49 27.5439 308.46 34.0342 505.52 23.8028 702.65 25.2979 311. 90 42.6425 507.63 0.0000 706.68 13.8193 316.51 49.4313 511. 00 27.5777 711.68 11. 5377 319.41 o .*o o o o 514.00 27.6165 720.70 0.0000 320.08 0.0000 514.00 27.6165 721. 93 0.0000 321.04 49.5815 520.40 14.9154 722.78 19 .1157 323.87 35.3462 520.69 0.0000 722.91 19 .1164 325.23 53.5448 522.65 0.0000 723. 31 22.5953 328.76 0.0000* 527.90 0.0000 724.19 24.3411 333.37 33.1643 528.26 17.6440 727.33 19.7275 333.97 38.9476 529.59. 18.1898 733.00 23.2568 "334.37 36.0718 529.87 0.0000 735.93 8.1484 338.28 27. 9663 531. 02 0.0000 333.97 11. 6471 338.32 27. 9669 537.26 0.0000 739.50 0.0000 311. 90 34.7659 546.56 0.0000 747.24 15.7791 340.48 34.7659 552.55 30.2752 748.06 10.5223 340.55 0.0000 563.25 27.1617 752.31 22.8333 344.28 42.9818 569.33 20.6978 753.82 0.0000 345.93 34.8867 946.00 16.3416 756.73 21. 98 94 351.06 37.9169 569.70 16.3434 756.80 21. 9902 351.93 37.9376 583.19 21.9198 884.68 20.2822 Page 3887 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.7076 1274.44 10.4404 1620.50 6.5889 766.42 22.0650 1001.03 14.2561 1621. 92 3.2953 766.84 16.7717 1002.74 11. 4104 1678.03 0.0000 772.60 0.0000 1004.73 18.0769 1690.97 3.3391 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.5127 778.90 10.6373 1028.54 0.0000 1063.66 4.5173 783.70 0.0000 1037.84 13.4437 1771.35 1. 5061 785.37 11. 5496 1038.76 0.0000 1791.20 0.0000 792.07 12.4666 631. 29 14.4397 1808.65 1.8194 794.95 13.3704 1048.07 0.0000 1810.72 0.0000 795.86 12.4828 1049.04 17.3386 1836.06 4.5706 810.06 21. 5024 1050.41 15.4180 810.29 21. 5039 1063.66 15.4736 344.28 22.9383 1077.00 0.0000 810.76 22.9414 1077.34 12.6191 815.77 0.0000 1085.87 12.6485 1048.07 0.0000 1093.63 14.6246 832.01 11.7325 1099.45 23.4346 834.85 17.1631 1112. 07 11.1970 835. 71 21.6863 1112.84 11. 7 590 836.80 0.0000 1115. 54 10.9826 846.75 0.0000 1120.29 11.7817 846.77 8.1617 1120.55 11. 7825 856.80 0.0000 1221.41 11. 7847 860.56 14.5747 1129. 67 6.8893 871.09 11. 6988 1131.51 0.0000 873.19 16. 0966 1147.95 0.0000 875.33 0.0000 1173.23 12.9381 879.38 15.5785 1177.95 12.7539 880.51 13.7508 1189.05 19.4120 883.24 13.7622 1204.77 19.0580 884.68 13.7686 1221. 41 17.1214 889.28 16.5460 1231.02 12 .1143 894.76 12.8913 1235.36 0.0000 898.04 17.5133 1238.28 16.1807 900.72 13.8377 1260.41 0.0000 903.28 21.2347 1271. 87 *17.3300 911.20 17.5846 1274.44 16.3203 912.08 17.5893 1274.54 16.3213 923.98 0.0000 1291.59 16.3857" 926.50 12.0875 1298.22 0.0000 929 .11 13.0276 1312 .11 0.0000 937.49 20.5243 1332.49 9.3043 944.13 0.0000 1362.66 0.0000 946.00 14.0291 1365.19 3.1243 949.00 14.0419. 1368.63 0.0000 667. 71 0-.0000 1384.29 5.2295 962.31 19.7362 1408.01 12.6160 964.08 10.5314 1457.56 0.0000 966 .17 19.5705 1460.82 5.3165 911.20 24.4829 1489.16 6.4175 968. 97 24.4829 1505.03 6.4387 983.53 0.0000 1584.12 7.6328 984.45 0.0000 1596.21 0.0000 Page 3888 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:57:48.10 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : Z-OCT-2016 11:00:23. Sample date 30-NOV-2015 13:53:00 Acquisition date 3-0CT-2016 06:55:55. Sample ID G405235042 Sample quantity : 1.76800E+02 GRAM Detector name GAM08 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.67 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID ** LCS ID : 1556 ***************************************************t**************************** Pk It 1 0 2 -1 3 1 4 3 5 3 6 0 7 0 8 0 9 0 10 0 11 0 12 1 13 1 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 62.99* 74.79* 76.94* 92.73* 94.82 144.04* 185.86* 213. 01 238.59* 241. 7 6 270. 96 295.37* 300.25 307.48 339.27*

352.15* 370.31 463.41 511. 28* 583.44* 609.45* 661. 7 4 728.09* 733.46 794.49 861. 60* 911. 20* 924.29 971.14* 1001.34* 1028.25 1120.48* 1155. 72 1163.80 Page 3889 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 19 105 124 66 23 5 47 94 234 56 27 101 21 13 66 170 33 30 47 110 121 81 34 9 16 14 66 9 23 17 8 24 18 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 93 121 120 150 83 87 92 223 119 49 71 39 44 62 63 83 57 29 22 15 49 29 18 8 8 23 11 *2 41 3 19 7 8 9 1. 39 1.18 1.18 "1. 48 1. 08 0.88 1. 29 8.20 1. 00 1. 65 0.73 1. 55 1. 55 4.45 1. 39 1. 43 7.15 2.78 2.42 1. 59 1. 46 1. 57 1. 63 1. 77 1.29 0.73 1.11 0.53 1. 02 0.62 1. 42 1. 57 1. 59 1. 26 126.24 149.84 154.13 i85.74 189.91 288.40 372.09 42 6. 41 477.59 483.93 542.35 591.20 600.95 615.43 679.03 704.81 741.13 927.42 1023.18 1167. 56 1219.61 1324.21 1456.96 1467.71 1589.80 1724.07 1823.30 1849.49 1943.22 2003.65 2057.47 2241. 99 2312.49 2328.65 123 144 144 170 170 285 368 412 473 482 537 586 586 607 672 699 733 922 1017 1162 1214 1319 1449 1463 . 1583 1714 1816 1845 1933 1997 2051 2237 2305 2322 7 5.23E-03 92.6 16 2.91E-02 20.2 l.23E+OO 16 3.45E-02 17.6 23 1.84E-02 3.36E+OO 23 6.40E-03 75.5 6 1. 45E-032 98 .1 9 1. 31E-02 42. 6 27 2.61E-02 46.0 9 6.50E-02 10.9 6 l.55E-02 24.4 10 7.56E-03 61.4 19 2.81E-02 15.6 1.13E+OO 19 5. 85E-03 61. 0 12 3.66E-03123.5 14 1.82E-02 29.5 14 4.72E-02 14.l 18 9.30E-03 56.2 12 8.28E-03 40.9 19 1.31E-02 35.4 143.07E-02 12.2 14 3.37E-02 15.5 11 2.24E-02 17.2 15 9.58E-03 33.5 7 2.43E-03 65.1 11 4.36E-03 43.5 19 3.97E-03 87.4 15 1.82E-02 17.1 7 2.51E-03 41.5 16 6.49E-03 67.1 13 4. 7.6E-03 35. 7 10 2.12E-03115.0 10 6.79E-03 30.3 17 4.94E-03 44.4 12 2.63E-03 70.8 Peak Search Report (continued) Page : 2 Sample ID : G405235042 Acquisition date 3-0CT-2016 .06: 55: 55 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1168. 05 10 7 1. 08 2337.17 2333 9 2.76E-03 57.1 36 0 1261.90 12 7 1. 33 2524.91 2519 11 *3.41E-03 *52_5 37 0 1301.59 13 0 0.83 2604.31 2599 10 3.61E-03 27.7 38 0 1460.69 305 4 2.03 2922.58 2915 15 8.48E-02 5.9 39 0 1764.43* 18 0 1.18 3530.17 3523 13 4.88E-03 28 .1* Flag: "*" = Peak area was modified by background subtraction Page 3890 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 07:57:50 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 13:53:00 G405235042 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:55:55 176.80 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3891 of 5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 74.66 74.82 *74. 82 351.06 CAN 0 01:00:00.67 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235042 Acquisition date 3-0CT-2016 06:55:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 9.672E-01 1.233E+Ol 1.233E+Ol 11. 78 OK BA-137M 661.66 89.90* 1. 815E+OO 2. 313E-01 2.358E-01 34.47 OK CS-137 661.66 85.10* 1.815E+OO 2.443E-01 2.491E-01 34 .. 47 OK TL-208 277.37 6.60 3.710E+OO Line Not Found Absent 583.19 85.00* 2.006E+OO 3.083E-01 3.083E-01 24.40 OK 860.56 12.50 1.477E+OO 3.489E-01 3.489E-01 174.76 OK PB-212 74.82 10.28 3.316E+OO 1.414E+OO l.414E+OO 54.34 OK '77.11 17.10 3.509E+OO l.258E+OO l.258E+00 35.22 OK 238.63 43.60* 4.174E+OO 6.871E-01 6.871E-01 21.74 OK 300.09 3.30 3.477E+OO 9.534E-01 9.534E-01 121. 97 OK BI-214 609.32 45.49* l.937E+OO 6.508E-01 6. 511E-01 30.99 OK 1120.29 14.92 1. 202E+OO 5. 911E-01 5. 913E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 OK PB-214 74 .*82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3.509E+OO 2.218E+OO 2.218E+OO 35.22 OK 87.09 3.41 4.288E+OO Line Not Found r Absent 242.00 7.25 4.130E+OO Line Not Found <<INT Reject 295.22 18.42 3.525E+OO 8. llOE-01 8 .113E-01 31.12 OI<: 351. 93 35.60* 3.044E+OO 7.984E-01 7.987E-01 28.20 OK RN-222 609.32 45.49* 1. 937E+00 6.508E-01 6. 511E-01 30.99 OK 1120.29 14.92 l.202E+OO 5. 911E-01 5.913E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 OK RA-224 240.99 4.10* 4 .133E+OO 3.237E-01 3.237E-01 298.89 OK RA-226 609.32 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 OK 1120.29 14.92 1. 202E+00 5. 911E-01 5. 913E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 OK TH-228 74.82 10.28 3.316E+OO 1.414E+OO l.414E+00 54.34 OK 77.11 17.10 3.509E+OO l.258E+OO 1.258E+OO 35.22 OK 238.63 43.60* 4.174E+OO 6. 871E-01 , 6. 871E-01 21. 74 OK 300.09 3.30 3.477E+OO 9.534E-01 9.534E-01 121.97 OK TH-230 609.32 45.49* 1.937E+OO 6.508E-01 6.508E-01 30.99 OK 1120. 29 14.92 1. 202E+OO 5 911E-01 5. 911E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.677E-01 56.10 OK PA-231 283.69 1. 70 3.643E+OO Line Not Found Absent 301.36 5.35* 3.477E+OO 5.881E-01 5.881E-01 121. 97 OK TH-234 63.29 3.70* 2.108E+OO 1.498E+OO 1.498E+OO 185.14 OK 92.59 4.23 4:622E+OO 2.017E+OO 2.017E+OO 78.54 OK U-234 609.32 45.49* l.937E+OO 6.508E-01 6.508E-01 30.99 OK 1120. 29 14.92 l.202E+OO 5. 911E-01 5. 911E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.677E-01 56.10 OK U-235 89. 96 3.47 4.467E+OO Line Not Found Absent 93.35 5.60 4.622E+OO 1.523E+OO l.523E+00 78.54 OK 143.76 10. 96* 5.442E+OO 4.947E-02 4.947E-02 596. 16 OK 163.33 5.08 5.246E+OO Line Not Found Absent 185. 72 57.20 4.930E+OO 9 .. 198E-02 9.198E-02 85 .11 OK 205.31 5.01 4. 641E+OO Line Not Found Absent U-238 63. 29 3.70* 2.108E+00 1.498E+OO l.498E+00 185.14 OK 92.59 4.23 4.622E+00 2.017E+OO 2.017E+00 78.54 OK AM-243 43.53 5.90 2.327E-01 Line Not Found Absent Page 3892 of 5809 Nuclide Line Activity Report (continued) Page : 3 3-0CT-2016 06:55:55 Sample ID : G405235042 Acquisition date Nuclide Type: Nuclide ANH-511 Energy 74.66 511. 00 %Abn 67.20* 100.00* Flag: "*" = Keyline Page 3893 of 5809 %Eff 3.316E+OO 2.232E+OO Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error 2.163E-01 2.163E-01 54.34 l.023E-01 1.023E-01 70.85 Status OK OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:57:51.10 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l *
Acquisition date 3-0CT-2016 06:55:55 Sensitivity : 3.000 *
Detector ID GAMOB Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.67 Half life ratio : ***** *
Sample date 30-NOV-2015 13:53:00 Analyst initials: MXRl * *Sample ID G405235042 Sample Quantity 1.7680E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 * *Nuclide Library : SOLID.NLB;6 . * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Nuclides Activity* Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.233E+Ol 1. 423E+OO BA-137M 2.358E-01 7. 965E-02 CS-137 2.491E-01 8.415E-02 TL-208 3.083E-01 7. 372E-02 PB-212 6.871E-01 l.464E-01 BI-214 6. 511E-01 l.977E-01 PB-214 7.987E-01 2.207E-01 RN-222 6. 511E-01 1.977E-01 RA-224 3.237E-01 9.481E-01 RA-226 6. 511E-01 1.977E-01 TH-228 6. 871E-01 1. 464E-01 TH-230 6.508E-01 1.976E-01 PA-231 5.881E-01 7.029E-01 TH-234 1.498E+OO 2.718E+OO U-234 6.508E-01 1.976E-01 U-235 4.947E-02 2.890E-01 U-238 1.498E+OO 2.718E+OO AM-243 2.163E.:..01 1.152E-01 ANH-511 l.023E-01 7.103E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3894 of 5809 Key-Line Activity (pCi/GRAM 1.495E+Ol -1.235E-02 O.QOOE+OO 8.641E-03 7.510E-02 O.OOOE+OO O.OOOE+OO 3.215E-02 -2.901E-01 O.OOOE+OO 1. 7 67E-02 K.L. Cnt Uncert * (1. 96-sigma) 1.265E+Ol 3.734E-02 1. 960E+41 1.952E-02 4.817E-01 1.689E+04 4.524E+02 4. 8 96E-02 4.658E-01 1.617E+41 4.884E-02 MDA (pCi/GRAM 6.159E-01 6.643E-02 7.018E-02 6. 311E-02 1.0lOE-01 l.309E-01 l.220E-01 1.309E-01 1.062E+OO 1.309E-01 1.0lOE-01 l.309E-01 6.746E-01 2.540E+OO 1.309E-01 3.150E-01 2.540E+OO 9.787E-02 4 .. 036E-02 MDA (pCi/GRAM 2. 850E+0.1 7.060E-02 O.OOOE+OO 5.458E-02 9.700E-01 O.OOOE+OO O.OOOE+OO 1.131E-01 8.545E-01 O.OOOE+OO 9.585E-02 NOT IDENT. NOT IDENT .. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3895of5809 -4.666E-01 -5.049E+OO 5.863E-03 3.864E-02 -l.369E+OO -l.025E+Ol O.OOOE+OO 5.548E-02 0.000E+OO 0.000E+OO -9.802E-02 6.097E+OO 6.954E-01 O.OOOE+OO 3.127E-02 -5.682E+Ol -1. 328E-02 -2.528E-01 -4.655E-01 4.518E-01 O.OOOE+OO O.OOOE+OO 0.000E+OO 0.000E+OO 9.922E-03 -8.216E-03 2.616E+00 '-3. l 75E-01 -3.175E-01 -6.266E-03 8. 134E-02 -1.853E-02 -4.937E-02 O.OOOE+OO O.OOOE+OO 2.142E-02 1.157E-02 8.939E-02 -1.322E+02 O.OOOE+OO O.OOOE+OO 3.738E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 1.310E-02 O.OOOE+OO 7.066E-02 7.375E-04 O.OOOE+OO O.OOOE+OO -7.099E-02 O.OOOE+OO O.OOOE+OO 7.939E+OO O.OOOE+OO -3.430E-02 -1.214E-03 -5.977E-02 4.624E-03 O.OOOE+OO 2.994E+02 O.OOOE+OO 9.557E-:03 -3.597E-03 l.846E-01 -3.016E-02 3.030E-02 -3.385E-01 -3.375E-02 1.165E+Ol -5.657E-02 -8.596E-02 2.135E-02 2.002E+OO 2.198E-01 -4.373E-02 5.904E-01 7.984E+OO 3.677E-02 l.443E-01 2. 44BE+oo* 1.199E+Ol 7.929E+03 2.054E-01 2.623E+38 7. 896E+02 5.823E-01 5.934E+OO 6.805E-01 3.924E+04 6.945E-02 5.592E+02 2.623E-02 8.902E-01 2.690E+OO 1.375E+OO 1. 960E+41 1.331E+41 l.027E+33 l.838E+41 3. 491E-02 4.404E-02 5.933E+OO 4.677E-01 4.677E-01 2.733E-02 .1.168E+OO 9.769E-02 2.262E-01 3.202E+40 1.378E+05 l.354E-01 1.920E+OO 1.008E-01 3.099E+02 l.659E+06 1. 785E+06 7.618E-02 8.020E+22 1.060E+10 l.960E+41 2.057E+27 3.859E-02 l.241E+41 6.025E-02 1.330E-01 l.030E+41 3.564E+05 1.126E-01 1. 762E+06 6.662E+05 4.638E+Ol l.507E+41 3.694E-01 4. 960E-02 4.334E+OO 4.204E-02 4.802E+07 8.013E+02 1. 792E+41 2.385E-02 8.187E-02 1.794E-01 9 .116E-02 1.114E-01 2.036E+OO 5. 772E-02 2.787E+Ol 2.454E-01 7.803E-02 5.166E-02 4.765E+OO 9.055E-01 3.753E+OO 1.055E+00 1.408E+Ol 7.723E-02 2.827E-01 4.398E+OO 2.243E+Ol O.OOOE+OO 4.219E-01 O.OOOE+OO O.OOOE+OO l.069E+OO l.322E+Ol 1.515E+OO O.OOOE+OO 2.753E-01 1.082E+03 5.022E-02 1.730E+OO 4.769E+OO 2.967E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 6.760E-02 8.467E-02 1.239E+Ol 7.996E-01 7.996E-01 5.201E-02 2.260E+OO l.924E-01 4.350E-01 O.OOOE+OO O.OOOE+OO 2.566E-01 4.303E+OO 2.176E-01 5.665E+02 O.OOOE+OO O.OOOE+OO l.516E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 7.271E-02 O.OOOE+OO 9.993E-02 2. 411E-01 O.OOOE+OO 0.000E+OO 1. 968E-01 O.OOOE+OO O.OOOE+OO 5.258E+Ol O.OOOE+OO 6.850E-01 1.016E-01 8.886E+OO 8.344E-02 O.OOOE+OO 1. 581E+03 O.OOOE+OO 4.526E-02 1.468E..:.01 3.565E-01 1. 724E-01 ' 2.189E-01 4.000E+OO l.082E-01 5.840E+Ol 4.555E-01 l.271E-01 3.864E-02 9.808E+OO 1.857E+OO 7.573E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN

NOT I DENT. FAIL ABUN NOT IDENT.

RE-184 -l.125E+OO 3.339E+Ol 6. 727E+Ol NOT IDENT. W-188 1.987E+Ol l .196E+02 2.197E+02 FAIL ABUN IR-192 -4.992E-01 4.595E-01 8.093E-01 FAIL ABUN HG-203 -3.595E+00 2.484E+OO 4.248E+OO NOT IDENT. BI-207 6.315E-03 3.790E-02 8.061E-02 FAIL ABUN PB-210 -3.347E+00 5.445E+OO 1.058E+Ol NOT IDENT. BI-211 O.OOOE+OO 6.079E-01 7.644E-01 FAIL ABUN PB-211 5.547E-02 6.223E-01 1.238E+OO NOT IDENT. BI-212 O.OOOE+OO 9. 296E-01 1.302E+OO FAIL ABUN RN-219 -1.052E-01 3.421E-01 6.507E-01 FAIL ABUN RA-223 4.151E-02 5.534E-01. 1.082E+OO FAIL ABUN AC-227 -6.853E-02 1. 989E-01 3.892E-01 FAIL ABUN TH-227 -6.853E-02 1. 989E-01 3.892E-01 FAIL ABUN AC-228 O.OOOE+OO 2.700E-01 5.024E-01 FAIL ABUN RA-228 O.OOOE+OO 2.700E-01 5.024E-01 FAIL ABUN TH-229 -4.067E-02 4 .114E-01 8.342E-01 NOT IDENT. TH-231 4 .151E-02 5.534E-01 l.082E+OO FAIL ABUN TH-232 O.OOOE+OO 2.700E-01 5.024E-01 FAIL ABUN PA-233 -1.259E-02 6. 296E-02 l.165E-01 FAIL ABUN PA-234 -1.738E-01 2.461E-01 4.376E-01 FAIL ABUN PA-234M 6.851E+OO 4.793E+OO 8.846E+OO FAIL ABUN NP-237 -1.259E-02 6.296E-02 1.165E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 4.936E-02 2.323E-01 4.536E-01 NOT IDENT. PU-239 9. 967E+Ol 3 .116E+02 6.049E+02 NOT IDENT. AM-241 1.412E-01 l.EJ44E-01 3.327E-01 NOT IDENT. CM-243 -5.309E-02 1.00BE-01 1.857E-01 NOT IDENT. BK-247 2.102E-02 6. 631E-02 1.371E-01 NOT IDENT. CM-247 3.517E-03 3. OBlE-02 6.187E-02 NOT IDENT. CF-249 6.041E-03 3.398E-02 6.864E-02 NOT IDENT. CF-251 2.BlOE-02 1.029E-01 2.153E-01 NOT IDENT. Page 3896 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:57:49.01 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 299 10.66* 9.672E-01 l.233E+Ol 1.233E+Ol 11. 78 BA-137M 661.66 89 89.90* 1.815E+OO 2.313E-01 2.358E-01 34.47 CS-137 661.66 89 85.10* 1.815E+00 2.443E-01 2.491E-01 34.47 CE-141 145.44 7 48.29* 5.442E+OO l.123E-02 7.939E+OO 596 .16 TL-208 277.37 ------6.60 3.710E+OO ------Line Not Found ------583.19 124 . 85.00* 2.006E+OO 3.083E-01 3.083E-01 24.40 860.56 15 12.50 1. 477E+OO 3.489E-01 3.489E-'01 174.76 BI-211 72.87 ------1.23 3.135E+OO ------Line Not Found ------351.06 204 12.92* 3.044E+OO 2.200E+OO 2.200E+OO 28.20 PB-212 74.82 150 10.28 3.316E+OO 1. 871E+OO 1.871E+OO 40.34 77 .11 178 17.10 3.509E+OO l.258E+OO 1.258E+OO 35.22 238.63 295 43.60* 4.174E+OO 6. 871E-01 6.871E-01 21.74 300.09 26 3.30 3.477E+00 9.534E-01 9.534E-01 121.97 BI-214 609.32 135 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 1120.29 25 14.92 l.202E+00 5. 911E-01 5. 913E-01 60.69 1764.49 17 15.30 B.lBOE-01 5.677E-01 5.679E-01 56.10 PB-214 74.82 150 5 .'BO 3.316E+OO 3.317E+OO 3.31BE+OO 40.34 77 .11 178 9.70 3.509E+OO 2.21BE+OO 2.218E+OO 35.22 87.09 ------3.41 4.288E+OO ------Line Not Found ------242.00 70 7.25 4 .133E+OO 9.941E-01 9.945E-01 48.83 295.22 124 18.42 3.525E+OO 8. llOE-01 8 .113E-01 31.12 351. 93 204 35.60* 3.044E+OO 7.984E-01 7.987E-01 28.20 RN-222 609.32 135 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5.913E-01 60.69 1764.49 17 15.30 8.lBOE-01 5.677E-01 5.679E-01 56.10 RA-224 240.99 70 4.10* 4.133E+OO 1. 7 58E+OO 1. 758E+OO 48.83 RA-226 609.32 135 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5.913E-01 60.69 1764.49 17 15.30 8.lBOE-01 5.677E-01 5.679E-01 56.10 TH-228 74.82 150 10.28 3.316E+OO 1. 871E+OO l.871E+OO 40.34 77 .11 178 17.10 3.509E+OO l.258E+OO l.258E+OO 35.22 238.63 295 43.60* 4.174E+OO 6.871E-01 6.871E-01 21. 74 300.09 26 3.30 3.477E+OO 9.534E-01 9.534E-01 121.97 TH-230 609.32 135 45.49* 1.937E+OO 6.508E-01 6.508E-01 30.99 1120.29 25 14.92 1. 202E+"OO 5. 911E-01 5. 911E-01 60.69 1764.49 17 15.30 8.lBOE-01 5.677E-01 5.677E-01 56.10 PA-231 283.69 ------1. 70 3.643E+OO ------Line Not Found ------301. 36. 26 5.35* 3.477E+OO 5. BBlE-01 5. BBlE-01 121. 97 TH-234 63.29 28 3 .*70* 2.lOBE+OO 1.49BE+OO l.498E+OO 185.14 92.59 93 4.23 4.622E+OO 2.017E+OO 2.017E+OO 78.54 U-234 609.32 135 45.49* 1.937E+OO 6.508E-01 6.508E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5. 911E-01 60.69 1764.49 17 15.30 8.lBOE-01 5.677E-01 5.677E-01 56.10 U-235 89. 96 ------3.47 4.467E+OO ------Line Not Found ------93.35 93 5.60 4.622E+OO 1.523E+OO 1.523E+OO 78.54 143.76 7 10.96* 5.442E+OO 4.947E-02 4.947E-02 596 .16 163.33 ------5.08 5.246E+OO ------Line Not Found ------Page 3897 of 5809 Nuclide Line Activity Report (continued) , Page : 2 Sample ID : G405235042 Acquisition date 3-0CT-2016 06:55:55 Nuclide Type: Uncorrected Decay Corr 2-sigma Nuclide Ene:r;gy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 185.72 61 57.20 4.930E+OO 9.198E-02 9.198E-02 85 .11 205.31 ------5.01 4.641E+OO ------Line Not Found ------U-238 63.29 28 3.70* 2.108E+OO 1.498E+OO 1.498E+OO 185.14 92.59 93 4.23 4.622E+OO 2.017E+OO 2.017E+OO 78.54 AM-243 43.53 ------5.90 2.327E-01 ------Line Not Found ------74.66 150 67:20* 3.316E+OO 2.863E-01 2.863E-01 40.34 ANH-511 511. 00 54 100.00* 2.232E+OO 1.023E-01 1.023E-01 70.85 Flag: "*" Key line Page 3898 of 5809 Page : 3 Surrunary of Nuclide Activity Sample ID : G405235042 Acquisition date 3-0CT-2016 06:55:55 Total number of lines in spectrum 39 Number of unidentified lines 7 Number of lines tentatively identified NID 32 Nuclide Type : Nuclide K-40 BA-137M CS-137 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-"243 ANH-511 Hlife 1. 25E+09Y 30.08Y 30.08Y 32. 51D l.41E+10Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+10Y 1600. ODY 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+Q5y* 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 02 1. 02 707. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. o*o 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.233E+Ol 2.313E-01 2.443E-01 l.123E-02 3.083E-01 2.200E+OO 6. 871E-01 6.508E-01 7.984E-01 6.508E-01 1. 758E+OO 6.508E-01 6. 871E-01 6.508E-01 5. 881E-01 1.498E+OO 6.508E-01 4 *. 94 7E-02 1.498E+OO 2.863E-01. l.023E-01 2.653E+Ol 2.653E+Ol Decay Corr pCi/GRAM 1.233E+Ol 2.358E-01 2.491E-01 7.939E+OO 3.083E-01 2.200E+OO 6.871E-01 6. 511E-01 7.987E-01 6. 511E-01 1. 758E+OO 6. 511E-01 6.871E-01 6.508E-01 5.881E-01 l.498E+OO 6.508E-01 4.947E-02 1.498E+OO 2.863E-01 1.023E-01 3.447E+Ol 3.447E+Ol 82.05% Decay Corr 2-Sigma Error 0.145E+Ol 0.813E-01 0.859E-01 47.33E+OO 0.752E-Ol 0.620E+OO 1.494E-01 2.017E-01 2.252E-01 2.017E-01 0.858E+OO 2.017E-01 1.494E-01 . 2.017E-01 7.173E-01 2.773E+OO 2.017E-01 29.49E-02 2.773E+00 1.155E-01 o*. 725E-01 "M" Manually accepted 2-Sigma %Error 11. 78 34.47 34.47 596 .16 24.40 28.20 21.74 30.99 28.20 30.99 48.83 30. 9.9 21. 74 30.99 '121. 97 185.14 30.99 596 .16 185.14 40.34 70.85 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3899of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235042 Acquisition date : 3-0CT-2016 06:55:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 94.82 32 116 1. 08 189.91 170 23 6.40E-03 **** 4.73E+OO T 0 213.01 120 284 8.20 426.41 412 27 2.61E-02 92.0 4.53E+OO 0 270.96 34 88 0.73 542.35 537 10 7.56E-03 **** 3.78E+OO T 0 307.48 16 75 4.45 615.43 607 12 3.66E-03 **** 3.41E+OO T 0 339.27 79 76 1. 39 679.03 672 14 l.82E-02 58.9 3.14E+OO T 0 370.31 40 67 7.15 7 41. 13 733 18 9.30E-03 **** 2.92E+OO 0 463.41 34 34 2.78 927.42 922 12 8.28E-03 81. 9 2.42E+OO T 0 728.09 37 19 1. 63 1456.96 1449 15 9.58E-03 66.9 l.68E+OO T 0 733.46 9 9 1. 77 1467.71 1463 7 2.43E-03 **** 1. 67E+OO T 0 794.49 17 9 1. 29 1589.80 1583 11 4.36E-03 87 .. 0 1.57E+OO T 0 911.20 69 12 1.11 1823.30 1816 15 1. 82E-02 34.2 1. 41E+00 T 0 924.29 10 2 0.53 1849.49 1845 7 2. 51E-03 82.9 1.40E+OO T 0 971.14 24 43 1. 02 1943.22 1933 16 6.49E-03 **** l.35E+OO 0 1001.34 18 3 0.62 2003.65 1997 13 4.76E-03 71. 4 1.31E+OO T 0 1028.25 8 20 1. 42 2057.47 2051 10 2.12E-03 **** 1.29E+OO T 0 1155. 72 18 8 1. 59 2312.49 2305 17 4.94E-03 88.7 1.17E+OO 0 1163.80 10 9 1. 26 2328.65 2322 12 2.63E-03 **** 1.17E+OO 0 1168. 05 10 7 1. 08 2337.17 2333 9 2.76E-03 **** 1.16E+OO 0 12 61. 90 12 7 1. 33 2524.91 2519 11 3.41E-03 **** 1. 09E+OO T 0 1301.59 13 0 0.83 2604.31 2599 10 3. 61E-03 55.5 1.07E+OO Flags: "T" = Tentatively a'ssociated Page 3900 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:03.38 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l *
Acquisition date 3-0CT-2016 06:55:55 Sensitivity 3.000 * *
Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.67 Half life ratio : ***** *
Sample date 30-NOV-2015 13:53:00 Nuclide Library : SOLID *
Sample ID G405235042 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : l.7680E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight . : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
Eff. 'File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.514E-01 2.948E-02 3 .114E-02 2.803E-02 4. 711E-02 5.866E-02 5.534E-02 5.866E-02 4.945E-01 5.866E-02 4. 711E-02 5.864E-02 3.042E-01 l.189E+OO 5.864E-02 1.470E-01 1.189E+OO 4.605E-02 1.747E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3901of5809 Le (pCi/GRAM 1.290E+Ol 2.853E-02 O.OOOE+OO 2.004E-02 4.326E-01 O.OOOE+OO O.OOOE+OO 4.876E-02 3.644E-01 O.OOOE+OO 4.496E-02 4.491E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 *I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-1'53 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3902 of 5809 6.0llE+OO 3.236E-02 l.183E-01 1. 875E+OO 1.037E+Ol O.OOOE+OO 1.948E-01 O.OOOE+OO O.OOOE+OO 4.621E-01 5.947E+OO 6.816E-01 O.OOOE+OO 8.295E-02 4.649E+02 2.165E-02 7.619E-01 2.219E+00 l.296E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3 .178E-02 3.569E-02 5.532E+OO 3.435E-01 3.435E-01 2.337E-02 1.067E+OO 8.297E-02 1. 960E-01 O.OOOE+OO O.OOOE+OO 1.199E-01 1. 656E+OO 9.908E-02 2.649E+02 O.OOOE+OO O.OOOE+OO 7.182E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.290E-02 O.OOOE+OO 4.409E-02 1.105E-01 O.OOOE+OO O.OOOE+OO 9.133E-02 O.OOOE+OO O.OOOE+OO 2.460E+Ol O.OOOE+OO 3.206E-01 4.458E-02 3.902E+OO 3.751E-02 O.OOOE+OO 7.399E+02 0.000E+OO 2.059E-02 6.568E-02 1.673E-01 6.967E-02 l.029E-01 1. 741E+OO 4.766E-02 2. 725E+Ol 2.138E-01 5. 311E-02 1. 740E-02 4.412E+OO 8.038E-01 3.531E+OO 2.912E+Ol NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT I DENT .. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF* SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 AC-228 RA-228 TH-229 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3903 of 5809 1. 007E+02 .3. 646E-01 1. 925E+OO 3.389E-02 4.926E+OO 3.668E-01 5. 596E-01 5.980E-01 2.915E-01 4.941E-01 1.782.E-01 1.782E-01 2.350E-01 2.350E-01 3.878E-01 4. 941E-01 2.350E-01 5.352E-02 1.829E-01 3.889E+OO 5.352E-02 O.OOOE+OO 2.120E-01 2.843E+02 l.559E-01 8.673E-02 6.321E-02 2.783E-02 3.103E-02 1.005E-01 FAIL ABUN. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:08.87 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l *
Acquisition date 3-0CT-2016 06:55:55 Sensitivity : 3.000 *
Detector ID GAM08 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.67 Half life ratio : ***** *
Sample date 30-NOV-2015 13:53:00 Nuclide Library : SOLID *
Sample ID G405235042 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : 1.7680E+02 GRAM *
Quantity Err(%) : 1.1312E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000. * ******************************************************************************* * * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 21-JUL:-2016 06': 09: 19 Eff. Geometry : CAN '*
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.233E+Ol 1.562E+OO 1.562E+OO BA-137M 2.358E-01 8.030E-02 8.030E-02 CS-137 2.491E-01 8.482E-02 8.482E-02 TL-208 3.083E-01 7.488E-02 7.488E-02 PB-212 6. 871E-01 1.509E-01 1. 509E_.:01 BI-214 6. 511E-01 1.997E-01 1.997E-01 PB-214 7.987E-01 2.232E-01 2. 232E-Ol
RN-222 6. 511E-01 l.997E-01 1.997E-01 RA-224 3.237E-01 9.529E-01 9.529E-01 RA-226 6. 511E-01 l.997E-01 1.997E-01 TH-228 6.871E-01 l.509E-01 l.509E-01 TH-230 6.508E-01 1.996E-01 1.996E-01 PA-231 5.881E-01 7.140E-01 7.140E-01 TH-234 1.498E+OO 2.738E+OO 2.738E+OO U-234 6.508E-01 1. 996E-01 1. 996E-01 U-235 4.947E-02 2.890E-01 2.890E-01 U-238 1. 498E+00 2.738E+OO 2.738E+00 AM-243 2.163E-01. 1.163E-01 1.163E-01 ANH-511 l.023E-01 7 .116E-02 7 .116E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1.495E+01 1.267E+Ol l.435E+Ol NOT IDENT. NA-22 -l.235E-02 3.734E-02 3.775E-02 NOT IDENT. NA-24 1. OOOE+41 4.268E+41 O.OOOE+OO SHORT HLIF AL-26 8.641E-03 1.953E-02 1.991E-02 NOT IDENT. SC-46 7.510E-02 4.817E-01 4.829E-01 FAIL ABUN V-48 l.342E+04 1.690E+04 1. 795E+04 SHORT HLIF CR-51 8.273E+Ol 4.525E+02 4.540E+02 SHORT HLIF MN-54 3.215E-02 4.898E-02 5.107E-02 NOT IDENT. C0-56 -2.901E-01 4.660E-01 4.840E-01 NOT IDENT. MN-56 -1.000E+41 1.618E+41 O.OOOE+OO SHORT HLIF C0-57 1. 7 67E-02 4.884E-02 4.949E-02 NOT IDENT. Page 3904 of 5809 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH.,..101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3905 of 5809 -4.666E-01 -5.049E+OO 5.863E-03 3.864E-02 -1.369E+00 -1.025E+Ol -3.921E+03 5.548E-02 l.231E+39 -2.936E+Ol -9.802E-02 6.097E+OO 6.954E-01 -1.880E+04 3.127E-02 -5.682E+Ol -1.328E-02 -2.528E-01

-4.655E-01 4.518E-01 l.OOOE+41 1.000E+41 7.632E+31 -1.000E+41 9.922E-03 -8.216E-03 2.616E+OO -3. 175E-01 -3.175E.:.01 -6.266E-03 8.134E-02 -1.853E-02 -4.937E-02 3.469E+40 5.137E+04 2.142E-02 1.157E-02 8.939E-02 -1.322E+02 -l.299E+05 -8.927E+05 3.738E-02 3. 571E+22 -1.329E+09 l.OOOE+41 4.759E+26 l.310E-02 -1.000E+41 7.066E-02 7.375E-04 1.000E+41 -2.869E+05 -7.099E-02 2. 571E+05 -1.908E+05 7.939E+OO l.000E+41 -3.430E-02 -l.214E-03 -5.977E-02 4.624E-03 -5.879E+07 2.994E+02 --l.OOOE+41 9.557E-03 *-3.597E-03 1. 846E-01 -3.016E-02 3.030E-02 -3.385E-01 -3.375E-02 1.165E+Ol -5.657E-02 -8. 596E-02 2.135E-02 2.002E+OO 2.198E-01 -4.373E-02 5.908E-01 7.992E+OO 3.677E-02 1.443E-01 2.449E+OO 1. 218E+Ol 7.936E+03 2.054E-01 l.094E+40 7. 8 96E+02 5.824E-01 5.939E+OO 6.811E-01 3.925E+04 6.948E-02 5.592E+02 . 2.624E-02 8.902E-01 2.690E+OO l.375E+OO 2.204E+41 1.332E+41 1.027E+33 1.840E+41 3.495E-02 4.404E-02 5.935E+00 4.681E-01 4.681E-01 2.733E-02 1.168E+OO 9.769E-02 2.262E-01 3.266E+40 1.380E+05 l.354E-01 1.920E+OO 1.008E-01 3 .100E+02 l.659E+06 l.794E+06 7.622E-02 9.471E+22 l.060E+10 1.932E+42 2.066E+27 3.859E-02 2.233E+41 6.032E-02 l.330E-01 7.029E+41 3.578E+05 1.135E-01 1.762E+06 6.663E+05 4.639E+Ol l.511E+41 3.694E-01 4. 960E-02 4.334E+OO 4.204E-02 4. 813E+07 8.014E+02 1.806E+41 2.385E-02 8.187E-02

1. 798E-01 9. ll 7E-02 l .115E-01 2.036E+OO 5.775E-02 2.788E+Ol 2.455E-01 7.851E-02 5.167E-02 4.766E+OO 9.056E-01 3.753E+OO 6. 271E-01 8.310E+OO 3.687E-02 1.453E-01 2.525E+OO l.303E+Ol 8.130E+03 2.069E-01 0.000E+OO 7.897E+02 5.841E-01 6.544E+OO 7.497E-01 4.015E+04 7.090E-Oi 5.598E+02 2.691E-02 8.975E-01 2.698E+OO l.390E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.524E-02 4.420E-02 6;051E+OO 4.895E-01 4.895E-01 2.747E-02 l.168E+OO 9.805E-02 2.273E-01 O.OOOE+OO l.399E+05 1.357E-01 1.920E+OO 1.086E-01 *3.157E+02 l.660E+06 l.838E+06 7.806E-02 O.OOOE+OO 1.062E+10 O.OOOE+OO 0.000E+OO 3.904E-02 O.OOOE+OO 6.822E-02 1.330E-01 O.OOOE+OO 3.805E+05 l.179E-01 l.766E+06 6.718E+05 4.652E+Ol O.OOOE+OO 3.698E-01 4. 960E-02 4.334E+OO 4.209E-02 5.495E+07 8.127E+02 O.OOOE+OO 2.424E-02 8.188E-02' 1. 981E-01 9.218E-02 l.123E-01 2.041E+OO 5.972E-02 2.837E+Ol 2.468E-01 8.756E-02 5.255E-02 4.850E+OO 9.llOE-01 3.753E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT.HLIF SHORT HLIF .NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT ,I DENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 -l.125E+OO 3.339E+Ol 3.339E+Ol NOT IDENT. W-188 1.987E+Ol 1.196E+02 1.199E+02 FAIL ABUN IR-192 -4.992E-01 4.600E-01 5.121E-01 FAIL ABUN HG-203 -3.595E+OO 2.489E+OO 2.970E+OO NOT IDENT. BI-207 6.315E-03 3.790E-02 3.800E-02 FAIL ABUN PB-210 -3.347E+OO 5.454E+OO 5.659E+OO NOT IDENT. BI-211 2.200E+OO 6.158E-01 1.167E+OO FAIL ABUN PB-211 5.547E-02 6.223E-01 6.228E-01 NOT IDENT. BI-212 l.417E+OO 9.324E-01 1.130E+OO FAIL ABUN RN-219 -l.052E-01 3.424E-01 3.456E-01 FAIL ABUN RA-223 4 .151E-02 5.534E-01 5.537E-01 FAIL ABUN AC-227 -6.853E-02 1.991E-01 2.015E-01 FAIL ABUN TH-227 -6.853E-02 l.991E-01 2.015E-01 FAIL ABUN AC-228 8.044E-01 2.731E-01 4.539E-01 FAIL ABUN RA-228 8.044E-01 2.731E-01 4.539E-01 FAIL ABUN TH-229 -4.067E-02 4 .114E-01 4 .118E-01 NOT IDENT. TH-231 4.151E-02 5.534E-01 5.537E-01 FAIL ABUN TH-232 8.044E-01 2.731E-01 4.539E-01 FAIL ABUN PA-233 -l.259E-02 6.296E-02 6.321E-02 FAIL ABUN PA-234 -1.738E-01 3.164E-01 3.260E-01 FAIL ABUN PA-234M 6. 851E+OO. 4.803E+OO _, 5. 710E+OO FAIL ABUN NP-237 -l.259E-02 6.296E-02 6.321E-02 FAIL ABUN NP-238 1. OOOE+41 3.207E+41 O.OOOE+OO SHORT HLIF NP-239 4.936E-02 2.323E-01 2.334E-01 NOT IDENT. PU-239 9. 967E+Ol 3 .116E+02 3 .148E+02 NOT IDENT. AM-241 1.412E-01 1. 64 7E-01 l.766E-01 NOT IDENT. CM-243 -5.309E-02 l.009E-01 1.037E-01 NOT IDENT. BK-247 2.102E-02 6.644E-02 6. 711E-02 NOT !DENT. CM-247 3.517E-03 3.081E-02 3.085E-02 NOT IDENT. CF-249 6.041E-03 3.398E-02 3.409E-02 NOT IDENT. CF-251 2.810E-02 1.030E-01 l.037E-01 NOT IDENT. 3906 of 5809

GEL Laboratories LLC *
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 72.6218 87.09 91.4164 136.47 82.3165 45.60 65.0560 87.57 91.4993 140.51 0.0000 46.54 75.2672 88.03 91. 5791 143.76 65.0701 49.72 0.0000 88.34 91. 6323 144.24 70.7391 51. 35 51.8652 88.47 91.6545 145.44 66.0219 51.87 48.8820 89. 96 91.9097 152 .. 43 71.9144 52.39 50.9890 1093.63 92.0256 153.25 0.0000 52.97 59.2375 91.11 0.0000 323.87 64.7490 53.44 64.4232 92.59 92.3549 156.02 0.0000 54.07 65.5530 93.35 92.4828 158.56 0.0000 57.36 0.0000 94.56 92.6848 159.00 63.9153 57.53 59.9313 94.65 92.6993 162.33 70.3533 57.98 64.1359 94.67 92.7031 162.66 0.0000 59.27 53.9620 94.87 92.7361 163.33 55.6107 59.32 53.9688 97.43 52.3782 165.86 70.6594 59.54 53.9975 98.43 79.8295 176.31 61.9234 60. 96 66.6868 98.44 176. 60 0.0000 61.17 68.1102 99.53 70.9706 177.52 60.3347 62.93 71.1865 100 .11 68.7865 181.07 0.0000 63.29 71.2465 102.03 73.5391 181. 52 61.8773 63.58 69.8967 103.18 85.0182 184.41 .72.2172 64.28 64.4097 103.37 80.5099 143.76 62. 5963 66.73 79.2046 105.21 76.2097 193.51 60.5801 67.24 88.8110 105.31 73.9472 197.03 58.2431 125.81 89.9571 106.12 69.4902 198.01 54.0176 67.75 85.7368 106.47 76.3697 201.83 57.6824 69.67 79.3709 109.28 73.2876 203.43 46.5694 70.83 99.4650 111. 00 82.6782 205.31 53.1425 72.81 84.5493 111. 76 0.0000 210.85 58.2290 72. 87 84.5601 114. 06 66.9280 215.65 58.5153 74.66 84.8814 116. 30 0.0000 222 .11 59.7746 74.82 84.9097 116.74 63.7335 227.09 65.3680 74.97 84.9362 119.76 72.1809 227.38 60.0852 77 .11 85.3141 121.12 61.8308 228.16 0.0000 78.74 75.1245 121.22 61.8405 228.18 56.5944 79.69 68.0315 121. 7 8 64.2282 116.74 56.5944 80.12 75.3335 122.06 67.7603 235.69 64.1301 80.19 0.0000 122.92 73.6974 235. 96 72 .1653 80.57 66.7015 123.07 67.8634 238.63 64.3088 81. 00 66.7586 265.00 80.8083 238.98 0.0000 81. 07 69.6709 125.81 84.5892 240.99 61. 7 662 81. 75 83.9356 127.23 75.3472 242.00 38.9763 83.79 86. 0963 127.91 84.8507 244.70 37.7267 84.00 86.1317 129.30 73.2135 252.40 0.0000 85.43 98.0805 131. 20 81. 7038 252.80 42.5316 86.55 91.3227 133. 02 72.4189 254.15 0.0000 86.79 91.3638 133.52 71.2830 256.23 45.3857 86.94 91.3904 136.00 67.9563 260.90 0.0000 Page 3907 of 5809

. ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 43.8965 355.39 0.0000 584.27 21.2776 264.80 43.9014 356.01 25.0424 595.83 0 .. oooo 265.00 41.1649 364.49 0.0000 427.87 22.5716 268.22 39.9042 366.42 0.0000 602.52 0.0000 269.46 36.7326 372.51 29.7986 604. 72 13.5693 270.03 36.7513 375.05 31.3430 607.14 16.9806 271.23 36.7887 377.52 25 .1159 609.32 24.9299 273.65 0.0000 356.01 23.0201 610.33 24.9425 276.40 35.1039 388.16 27.1005 614.28 17.0367 277.37 39.7552 388.63 0.0000 618.01 19.3415 277.60 41. 6125 391.69 31.1873 620.36 14.8070 278.00 36.0761 264.66 24.2856 621. 93 20.5166 279.20 49.0761 401.81 29.3670 630.19 0.0000 279.54 . 51. 8688 402.40 25.3255 631. 29 11. 4465 279.70 52.8020 404.85 28.4090 633.25 10. 3110 280.46 44.4932 410.95 28.5190 634.78 0.0000 283.69 35.3188 413.71 28.5685 635.95 20.6470 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.1229 423.72 0.0000 645.85 19.5864 285.90 0.0000 427.09 27.7773 657.76 17.3730 287.50 42.8892 427.87 21. 6148 657.90 0.0000 290.67 37.8592 433.94 29.9594 661.66 20.8835 293.27 0.0000 439.40 26.9479 664. 57. 0.0000 351. 93 39.4066 453.88 25.0889 666.33 0.0000 295.96 39.4297 463.37 21.0225 666.50 0.0000 879.38 39.5126 468.07 22 .1331 667.71 0.0000 299.98 39.5570 473.00 0.0000 677.62 16.6465 300.09 39.5604 475.06 30.6862 685.70 0.0000 300.13 39.5613 476.78 18.0058 695.00 0.0000 301.36 28.2861 477.60 14.8351 696.49 17.6630 302.85 45.3105 482.18 21.2472 696. 51 17.6636 256.23 39.6989 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.3194 306.78 39.7698 497.08 16.0666 697.49 20.3208 308.46 42.6663 505.52 12.9121 702.65 18.5942 311.90 46.7736 507.63 0.0000 706.68 14.1904 316.51 45.7949 511. 00 14.0292 711. 68 25.7733 319.41 0.0000 514.00 14.0516 720.70 0.0000 320.08 0.0000 514.00 14.0516 721.93 0.0000 321. 04 40.2090 520.40 15.6176 722.78 12.8558 323.87 33.5794 520.69 0.0000 722.91 12.8566 325.23 37.4551 522.65 0.0000 723. 31 11. 4301 328.76 0.0000 527.90 0.0000 724 .19 15.7217 333.37 42.0304 528.26 14.1569 727. 33 20.0348 333.97 27.5491 529.59 18.5260 733.00 17.2119 334.37 34.8091 529.87 0.0000 735.93 10.0522 338.28 30.0609 531.02 0.0000 333.97 16.7640 338.32 30.0615 537.26 0.0000 739.50 0.0000 311. 90 30'.1088 546.56 0.0000 747.24 19.8348 3'40. 48 30.1088 552.55 16.5387 748.06 11. 7241 340.55 0.0000 563. 25. 17.7357 752.31 22.5845 344.28 24.8349 569.33 14.4531 753.82 0.0000 345.93 31.2025 946.00 14.4547 756.73 12.6691 351.06 32.2950 569.70 12.2318 756.80 12. 6696 351. 93 32.3152 583.19 21.2668 884.68 16.3350 Page 3908 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 21. 7954 1274.44 6.2975 1620.50 2.7681 766.42 22.7089 1001.03 9.8544 1621.92 7.3836 766.84 21. 8042 1002.74 11. 0428 1678.03 0.0000 772.60 0.0000 1004.73 3.1570 1690 .. 97 3.7447 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9500 778.90 15.5168 1028.54 0.0000 1063.66 4.7551 783.70 0.0000 1037.84 8. 9698 1771. 35 2.8538 785.37 16.4696 1038.76 0.0000 1791.20 0.0000 792.07 11.7418 631.29 7.9946 1808.65 0.9581 794.95 16.1622 1048.07 0.0000 1810.72 0.0000 795.86 13.2284 1049.04 11. 0007 1836.06 0.0000 810.06 15.6999 1050.41 10.0049 810.29 15.7009 1063.66 8.0356 344.28 15.7020 1077.00 0.0000 810.76 '19.3985 1077.34 17.1442 815.77 0.0000 1085.87 20.2209 1048.07 0.0000 1093.63 18.2395 832.01 16.7574 1099.45 18.2703 834.85 7.4556 1112. 07 10.1874 835.71 13. 0511 1112. 84 13.2468 836.80 0.0000 1115. 54 6.5266 846.75 0.0000 1120.29 9.1901 846.77 17.7829 1120. 55 9.1906 856.80 0.0000 1221. 41 11.4399 860.56 11.2866 1129. 67 14.3341 871.09 9.4403 1131.51 0.0000 873.19 14.1710 1147.95 0.0000 875.33 0.0000 1173.23 8.2910 879.38 17.0414 1177.95 7.2640 880.51 11.3654 1189.05 15.6125 883.24 16.1165 1204.77 13.5887 884.68 15.1758 1221. 41 11. 5492 889.28 20.9003 1231.02 17.8944 894.76 18.0839 1235.36 0.0000 898.04 12.3871 1238.28 14.7648 900. 72 14.3060 1260.41 0.0000 903.28 14.3184 1271.87 3.1915 911.20 9.5712 1274.44 8.5166 912.08 9.5740 1274.54 8.5166 923.98 0.0000 1291. 59 7.4845 926. 5*0 9.2355 1298.22 0.0000 929.11 7.7029 1312 .11 0.0000 937.49 13.5176 1332.49 6.4816 944.13 0.0000 1362.66 0.0000 946.00 15.4922 1365.19 4.3557 949.00 12.5997 1368.63 0.0000 667. 71 0.0000 1384.29 6.5636 962. 31 24.4738 1408.01 4.4004 964.08 23.3745 1457.56 0.0000 966 .17 17.1531 1460.82 6.6823 911. 20 23. 4119 1489.16 4.4836 968. 97 23. 4119 1505.03 6.7493 983.53 0.0000 1584.12 10.9875 984.45 0.0000 1596.21 0.0000 Page 3909 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:58:38.72 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 30-NOV-2015 13:59:00 Acquisition date : 3-0CT-2016 06:56:18. Sample ID G405235043 Sample quantity 1.65795E+02 GRAM Detector name : GAM09 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.51 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 1 1 0 0 2 2 7 7 0 0 2 2 1 1 0 0 0 0 0 0 0 0 0 3 3 0 0 0 0 0 0 Page 3910of5809 Energy 63.36* 74.99 77.16 87.24 90.12 92.99* 143.38* 185.90* 188.10 238.69* 241.63 270.56 277.63 295.16* 300.32 338.43* 343.92 352.00* 369.64 462.19 510.73* 532.02 558. 91* 583.04* 608.93* 630.75 656.18 661.39 727.56 767.05 785.17 796.66 910.81* 935.55 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 40 98 145 64 47 61 17 84 21 369 96 33 34 156 33 92 18 212 69 55 23 19 6 121 149 16 13 26 45 31 22 17 63 16 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 126 122 101 110 84 119 102 73 84 60 60 76 61 36 48 27-24 55 51 15 70 17 11 24 14 12 18 15 12 11 8 20 12 22 1. 26 1. 03 0.90 0. 96 0.93 1. 25 0.94 1.16 1. 25 1.10 2.14 1. 2*1 1.13 1. 27 1. 41 1. 32 1. 33 1. 04 8.98 0.92 1. 41 1. 04 1. 21 1. 44 1. 39 1. 71 1. 94 1. 95 2 .11 2.94 1. 49 0.85 1. 56 0.58 126.39 149.66 154.00 174.17 179.93 185.68 286.49 371.57 375.98 477.20 483.08 540.97 555.12 590.18 600.51 676.76 687.76 703.92 739.21 924.39 1021.52 1064.11 1117.92 1166. 20 1218.01 12 61. 66 1312.56 1322.97 1455.38 1534.38 1570.66 1593.64 1822.04 1871. 55 123 145 145 170 170 182 284 365 365 473 473 534 550 583 583 672 672 699 728 918 1014 1061 1114 1160 1210 1258 1308 1308 1449 1528 1564 1588 1816 1864 9 l.llE-02 54.6 14 2.73E-02 20.3 3.15E+OO 14 4.02E-02 13.2 13 1.78E-02 27.8 2.34E+OO 13 l.30E-02 35.8 8 1. 71E-02 35. 8 8 4.80E-03105.4 14 2.34E-02 21.5 5.47E+OO 14 5.83E-03 78.3 16 l.02E-01 6.2 2,73E+OO 16 2.67E-02 23.8 11 9.06E-03 54.9 10 9.42E-03 46.7 24 4.32E-02 10.8 1.85E+OO 24 9.27E-03 38.0 21 14.5 1.43E+OO 21 4.89E-03 57.0 11 5.90E-02 9.7 23 l.91E-02 29.7 12 l.53E-02 19.5 14 6.35E-03 90.2 9 5.30E-03 44.3 7 1.79E-03107.0 12 3.37E-02 12.3 12 4.14E-02 9.8 7 4 . 4 2 E*-0 3 4 4 . 1 27 3.53E-03 58.5 1.86E+OO 27 7.lOE-03 39.3 12 l.25E-02 21.4 11 8.64E-03 27.3 10 6.14E-03 31.6 13 4.58E-03 60.4 12 l.76E-02 17.3 17 4.46E-03 70.6 Peak Search Report (continued) Page : 2 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 968. 97 39 20 1. 06 1938.44 1934 9 1. 08E-02 26.2 36 0 1001. 21* 6 12 1. 57 2002.94 1995 10 1. 71E-03122. 6 37 0 1008.00 6 10 0.70 2016.53 2011 7 l.77E-03 92.0 38 0 1086.29 11 10 1. 94 2173.18 2168 10 3.06E-03 61. 7 39 0 1119 _,57 42 6 2.99 2239.77 2234 11 l.15E-02 19.0 40 0 1175.33 16 11 3.35 2351. 36 2346 12 4.53E-03 48.7 41 0 1200.56 29 3 5.17 2401. 84 2396 14 8. llE-03 22.8 42 0 1238.33 13 16 0.69 2477.42 2472 9 3.64E-03 61. 3 43 0 1271.23 16 0 0.98 2543.25 2537 12 4.44E-03 25.0 44 0 1377.36 7 3 1. 05 2755.63 2752 6 1.97E-03 53.6 45 0 1450.18* 5 0 0. 96 2 901. 33 2898 6 l.42E-03 48.7 46 0 1460.09* '377 4 2.13 2921.16 2911 18 1.05E-01 5.4 47 0 1607.01 7 2 0.94 3215.17 3212 6 1. 81E-03 49.3 48 0 1763.59* 31 0 1. 32 3528.50 3522 13 8.49E-03 19.4 Flag: . "*" = Peak area was modified by background subtract{on Page 39,11 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:58:40 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 13:59:00 G405235043 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 06:56:18 165.79 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA9 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3912of5809 PB-214 PA-234M PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 766.42 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 NB-95 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 765.81 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.51 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.146E+OO l.361E+Ol 1.361E+Ol 10.73 OK NB-95 765.81 99.81* 1.922E+00 7.079E-02 1.980E+OO 64.76 OK CD-109 88.03 3.70* 4.861E+OO 1.169E+OO 1.856E+OO 105.33 OK SN-126 64.28 9.60 2.275E+OO l.153E+OO 1.153E+OO 109.24 OK 86.94 8.90 4.861E+OO 4.860E-01 4.860E-01 105.33 OK 87.57 37.00* 4.861E+OO 1.169E-01 1.169E-01 105.33 OK BA-137M 661.66 89.90* 2.157E+OO 6.441E-02 6.567E-02 78.66 OK CS-137 661. 66 85.10* 2.157E+OO 6.804E-02 6.938E-02 78.66 OK TL-208 277.37 6.60 4 .-349E+OO 6.397E-01 6.397E-01 93.46 OK 583.19 85.00* 2.382E+OO 2.978E-01 2. 978E-01

24.69 OK 860.56 12.50 1. 758E+OO Line Not Found Absent BI-212 727. 33 6.67* 2.003E+OO 1.627E+OO 1.627E+OO 42. 86 OK 785.37 1.10 1.888E+OO 5.097E+OO 5.097E+OO 63.14 OK 1620.50 1. 47 1.045E+OO Line Not Found Absent PB-212 74.82 10.28 3.688E+OO 9.898E-01 9.898E-01 67.41 OK 77 .11 17.10 3.924E+00 l.334E+00 l.334E+OO 26.50 OK 238.63 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 OK 300.09 3.30 4.084E+00 1.329E+OO 1. 329E+OO 76.02 OK BI-214 609.32 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 OK 1120.29 14.92 1.430E+OO 8.894E-01 8.898E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 OK PB-214 74.82 5.80 3.669E+OO Line Not Found <<INT Reject 77 .11 9.70 3.924E+OO 2.351E+OO 2.352E+OO 26. 50 OK 87.09 3.41 4.849E+OO Line Not Found <<INT Reject 242.00 7.25 4.832E+OO Line Not Found <<INT Reject 295.22 18.42 4.142E+OO 1.096E+OO 1. 097E+00 21. 60 OK 351. 93 35.60* 3.588E+OO 8.760E-01 8.763E-01 19.50 OK RN-222 609.32 45.49* 2.302E+00 7.025E-01 7.028E-01 19.58 OK 1120.29 14.92 l.430E+OO 8.894E-01 8.898E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 OK RA-224 240.99 4.10* 4.838E+OO 7.219E-01 7.219E-01 185.06 OK RA-226 609.32 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 OK 1120.29 14.92 l.430E+OO 8.894E-01 8.898E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 OK AC-228 105.21 1.10 5. 896E+OO Line Not Found Absent 338.32 11. 27 3. 705E+oo* 1.164E+OO 1.164E+00 29.06 OK 794.95 4.25 1.870E+OO Line Not Found Absent 835. 71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 OK 968. 97 15.80 1.603E+OO 7.182E-01 7.182E-01 52.38 OK RA-228 105.21 1.10 5. 896E+00 Line Not Found Absent 338.32 11. 27 3.705E+OO 1.164E+OO 1.164E+OO 29.06 OK 794.95 4.25 1.870E+OO Line Not Found Absent 835.71 1. 61 1. 799E+OO Line Not Found Absent 911. 20 25.80* 1.682E+OO 6.848E..:01 6.848E-01 34.51 OK 968. 97 15.80 1.603E+OO 7.182E-01 7.182E-01 52.38 OK TH-228 74.82 10.28 3.688E+OO 9.898E-01 9.898E-01 67.41 OK 77 .11 17.10 3.924E+OO 1.334E+OO 1.334E+OO 26.50 OK 238.63 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 OK Page 3913 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff ,pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.084E+OO 1.329E+OO 1.329E+OO 76.02 OK
TH-230 609.32 45.49* 2.302E+OO 7.025E-01 7.025E-01 19 .*58 OK 1120.29* 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8. 891E-01 38.85 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301.36 5.35* 4.084E+OO 8.196E-01 8 .196E-01 76.02 OK TH-232 105.21 1.10 5. 896E+OO Line Not Found Absent 338.32 11.27 3.705E+OO 1.164E+OO 1.164E+OO 29.06 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 OK 968. 97 15.80 l.603E+OO 7.182E-01 7.182E-01
52.38 OK PA-234M 766.42 0.32 1.924E+OO Line Not Found <<INT Reject 1001.03 0.84* l.562E+OO 2.181E+OO 2.181E+OO 245 .11 OK TH-234 63.29 3.70* 2.275E+00 2.992E+OO 2.992E+OO 109.24 OK 92.59 4.23 5.276E+OO 1. 671E+OO 1.671E+OO 71. 54 OK U-234 609.32 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 OK 1120.29 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.891E-01 38.85 OK U-235 89. 96 3.47 5.079E+OO 1. '616E+OO 1.616E+OO 71. 57 OK 93.35 5.60 5.276E+OO 1. 262E+00 1.262E+00 71.54. OK 143.76 10. 96* 6.313E+OO l.450E-01 1.450E-01 210.79 OK 163.33 5.08 6. 096E+OO Line Not Found Absent 185.72 57.20 5.741E+OO 1.453E-01 l.453E-01 42.94 OK 205.31 5.01 5.415E+OO Line Not Found Absent U-238 63.29 3.70* 2.275E+OO 2.992E+OO 2.992E+00 109.24 OK 92.59 4.23 5.276E+OO 1.671E+OO 1.671E+OO 71. 54 OK AM-243 43.53 5.90 1. 969E-01 Line Not Found Absent 74.66 67.20* 3.688E+OO l.514E-01 1.514E-01 67.41 OK ANH-511 511. 00 2.647E+OO 4.355E-02 4.355E-02 180.49 OK Flag: "*" = Keyline Page 3914of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:41.93 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l * *Acquisition date 3-0CT-2016 06:56:18 Sensitivity : 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.51 Half life ratio : ***** *
Sample date 30-NOV-2015 13:59:00 Analyst initials: MXRl *
Sample ID G405235043 Sample Quantity 1.6579E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
Eff. File : 'DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 /1.361E+Ol 1.432E+OO 4.430E-01 NB-95 1.980E+OO 1.257E+OO 1. 295E+OO CD-109 1.856E+OO 1.916E+OO l.782E+OO SN-126 1.169E-01 l.207E-01 1.130E-01 BA-137M 6.567E-02 5.063E-02 4.764E-02 CS-137 6.938E-02 5.348E-02 5.033E-02 TL-208 2.978E-01 7.204E-02 4.698E-02 BI-212 1. 627E+OO 6.836E-01 7.695E-01 PB-212 9.538E-01 l.157E-01 7.710E-02 BI-214 7.028E-01 l.349E-01 8;726E-02 PB-214 8.763E-01 1.674E-01 9.397E-02 RN-222 7.028E-01 l.349E-01 8.726E-02 RA-224 7.219E-01 1.309E+OO 8.266E-01 RA-226 7.028E-01 1.349E-01 8.726E--:02 AC-228 6.848E-01 2.316E-01 2.162E-01 RA-228 6.848E-01 2.316E-01 2.162E-01 TH-228 9.538E-01 1.157E-01 7. 710E-02 TH-230 7.025E-01 l.348E-01 8. 723E-02 PA-231 8.196E-01 6.106E-01 5.796E-01 TH:._232 6.848E-01 2.316E-01 2.162E-01 PA-234M 2.181E+OO 5.238E+OO 6.979E+OO TH-234 2.992E+OO 3.203E+OO 2.269E+00 U-234 7.025E-01 l.348E-01 8. 723E-02 U-235 1.450E-01 2.995E-01 2.542E-01 U-238 2.992E+OO 3.203E+OO 2.269E+OO AM-243 1.514E-01 l.OOOE-01 8.182E-02 ANH-511 4.355E-02 7.703E-02 4.957E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigrria) (pCi/GRAM BE-7 -5.083E+OO l.049E+Ol 2.008E+Ol NOT IDENT. NA-22 -3.298E-02 4.607E-02 6.771E-02 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF Page 3915 of 5809 AL-26 -l.929E-02 1.898E-02 l.310E-02 NOT IDENT. SC-46 -6.499E-04 2.958E-01 5.945E-01 FAIL ABUN V-48 0.000E+OO 1. 674E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 3.952E+02 O.OOOE+OO SHORT HLIF MN-54 -2.346E-02 6.064E-02 1.105E-01 NOT IDENT. C0-56 -7.088E-02 4. 541E-01 8.636E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.012E-02 3.674E-02 7.207E-02 NOT IDENT. C0-58 -6.584E-02 5.251E-01 1. Ol 7E+*oo NOT IDENT. FE-59 -l.864E+OO 7.402E+OO 1.343E+Ol NOT IDENT. C0-60 l.303E-02 2.081E-02 5.449E-02 NOT IDENT. ZN-65 4.lOlE-02 1. 211E-01 2.417E-01 NOT IDENT. GE-68 -9.442E-01 2.044E+OO 3. 711E+OO NOT IDENT. AS-73 6.689E-01 9.848E+OO 2.137E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.697E+03 O.OOOE+OO SHORT HLIF SE-75 1.556E-01 1.574E-01 3.378E-01 NOT IDENT. BR-77 O.OOOE+OO 2. 072E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.913E+02 O.OOOE+OO SHORT HLIF RB-83 4.079E-02 5.848E-01 l.190E+OO NOT IDENT. KR-85 2.432E+OO 7.155E+OO 1. 334E+Ol NOT IDENT. SR-85 2.780E-01 8. 211E-01 1. 531E+OO NOT IDENT. RB-86 O.OOOE+OO 3.324E+04 O.OOOE+OO SHORT HLIF Y-88 -l.493E-03 l.027E-01 2.683E-01 NOT IDENT. Y-91 1. 700E+Ol 4.088E+02 7.785E+02 NOT IDENT. NB-94 2.445E-02 2.626E-02 5.825E-02 NOT IDENT. NB-95M 8.954E-01 2 .118E+OO 3.928E+OO NOT IDENT. ZR-95 7.360E-01 1.261E+OO 2.736E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 726E+41 O.OOOE+OO SHORT*HLIF M0-99 O.OOOE+OO l.060E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 272E-02 2.820E-02 5.405E-02 NOT IDENT. RH-102 7.303E-02 6.318E-02 l.150E-01 FAIL ABUN RU-103 -1. 355E+OO
4.568E+OO 9.041E+OO FAIL ABUN RH-106 -l.012E-01 3.653E-01 7.117E-01 NOT IDENT. RU-106 -l.012E-01 3.653E-01 7 .117E-01 NOT IDENT. AG-108M . l.481E-02 2.037E-02 4.547E-02 NOT IDENT. AG-llOM -6.400E-03 9.520E-02 l.830E-01 NOT IDENT. SN-113 6.763E-02 1.714E-01 3.709E-01 NOT IDENT. CD-115 O.OOOE+OO 3.341E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.103E+05 O.OOOE+OO SHORT HLIF TE-123M 2.882E-02 1. 070E-01 2.150E-01 NOT IDENT. SB-124 -9.836E-03 1.580E+OO 3.550E+OO NOT IDENT. SB-125 3.695E-02 8.420E-02 l.797E-01 FAIL ABUN TE-125M 6.063E+Ol 2.445E+02 5.020E+02 NOT IDENT. I-126 0.000E+OO l.057E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.368E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.099E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 8'.207E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.522E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.630E+27 O.OOOE+OO SHORT HLIF BA-133 -2.088E-02 3.135E-02 4.720E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6. 551E-02 7.757E-02 9.008E-02 FAIL ABUN CS-135 -1.554E-02 9.616E-02 l.812E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.927E+05 O.OOOE+OO SHORT HLIF CE-139 -5.700E-02 8.154E-'-02 1. 496E-01 NOT IDENT. BA-140 0.000E+OO 1.548E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 4.165E+05 O.OOOE+OO SHORT HLIF CE-141 -2.573E+OO 2.420E+Ol 4.376E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.305E+41 0.000E+OO SHORT HLIF CE-144 l.490E-01 2 .' 697E-01 5.630E-01 NOT IDENT. PM-144 -l .161E-02 4.815E-02 9. l 71E-02 NOT IDENT. PR-.144 -l.012E+OO 4.200E+OO 7.999E+OO NOT IDENT. PM-146 -2.84BE-02 3.418E-02 6.265E-02 NOT IDENT. ND-147 O.OOOE+OO 6.773E+07 O.OOOE+OO SHORT HLIF PM-147 -3. 271E+02 6.308E+02 l.212E+03 NOT IDENT. PM-149 O.OOOE+OO 1.636E+41 O.OOOE+OO SHORT HLIF EU-150 l.443E-02 2.087E-02 4.023E-02 FAIL ABUN EU-152 9. 991E-02 1. ll 7E-01 l.407E-01 FAIL ABUN GD-153 -7.806E-02 l.391E-01 2.692E-01 NOT IDENT. EU-154 -7.594E-02 l.133E-01 l.693E-01 NOT IDENT. EU-155 5.660E-02 8.148E-02 1. 74*7E-01 FAIL ABUN TB-160 8.732E-01 1.486E+OO 3.303E+OO FAIL ABUN H0-166M -l.685E-02 3.937E-02 7.378E-02 FAIL ABUN TM-171 -6.819E+OO 2.278E+Ol 4.796E+Ol NOT IDENT. HF-172 -2.022E-02 l.833E-01 3.626E-01 FAIL ABUN Page 3916of5809 LU-172 1.477E-03 6.615E-02 1. 284E-01 FAIL ABUN LU-176 1. 063E-02 2.043E-02 4.075E-02 FAIL ABUN HF-181 2.753E+00 3.720E+OO 8.291E+OO NOT IDENT. TA-182 -4.634E-01 8.979E-01 1.665E+OO NOT IDENT. RE-183 -5.402E-01 3.429E+OO 7.173E+OO NOT IDENT. RE-184 5.587E-'01 3.089E+Ol 6.047E+Ol NOT IDENT. W-188 -8.200E+OO 9.014E+Ol 1. 569E+02 FAIL ABUN IR-192 -7.425E-02 4. 0 95E.-01 7.529E--:01 FAIL ABUN HG-203 -4.247E-02 2.137E+OO 3.752E+OO NOT IDENT. BI-207 -1.958E-02 3.944E-02 7.065E-02 FAIL ABUN PB-210 -7.391E-01 5.468E+OO 1.150E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.612E-01 7.057E-01 FAIL ABUN PB-211 1.140E-01 4.836E-01 1.024E+OO NOT IDENT. RN-219 -5.026E-02 2.822E-01 5.695E-01 FAIL ABUN RA-223 2.867E-01 4.449E-01 9.125E-01 FAIL ABUN AC-227 -8.344E-02 1. 874E-01 3.388E-01 FAIL ABUN TH-227 -8.344E-02 1. 874E-01 3.388E-01 FAIL ABUN TH-229 -3.259E-01 3.564E-01 6. 281E-01 FAIL ABUN TH-231 2.867E-01 4.449E-01 9.125E-01 FAIL ABUN PA-233 1.935E-02 4.971E-02 9.780E-02 FAIL ABUN PA-234 4.847E-02 2. 372E-01 4.792E-01 NOT IDENT. NP-237 1.935E-02 4.971E-02 9.780E-02 FAIL ABUN NP-238 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -4.255E-02 1.709E-01 3.385E-01 FAIL ABUN PU-239 4.167E+Ol 2.540E+02 5.099E+02 NOT IDENT. AM-241 5.728E-02 l.417E-01 3.076E-01 NOT IDENT. CM-243 3.221E-03 7.276E-02 1.489E-01 FAIL ABUN BK-247 3.348E-02 5.776E-02 1.107E-01 NOT IDENT. CM-247 2.355E-03 2.560E-02 5.329E-02 FAIL ABUN CF-249 3.848E-02 2.778E-02 6.265E-02 NOT IDENT. CF-251 -3.990E-02 8.458E-02 1.579E-01 NOT IDENT. Page 3917 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:58:39.67 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 367 10.66* 1.146E+OO 1. 361E+Ol 1.361E+Ol 10.73 NB-95 765.81 33 99.81* 1. 922E+OO *7.778E-02 2.176E+OO 54.67 CD-109 88.03 87 3.70* 4.861E+OO 2.179E+OO 3.460E+OO 55.60 SN-126 64.28 56 9.60 2.275E+OO 1.153E+OO 1.153E+OO 109.24 86.94 87 8.90 4.861E+OO 9.061E-01 9.061E-01 55.60 87.57 87 37.00* 4.861E+00 2.179E-01 2.179E-01 55.60 BA-137M 661. 66 28 89.90* 2.157E+OO 6.441E-02 6.567E-02 78.66 CS-137 661.66 28 85.10* 2.157E+OO 6.804E-02 6.938E-02 78.66 TL-208 277.37 41 6.60 4.349E+00 6.397E-01 6.397E-01 93.46 583.19 133 85.00* 2.382E+00 2.978E-01 2.978E-01 24.69 860.56 ------12.50 1. 758E+OO ------Line Not Found ------. BI-211 72.87 ------1. 23 *3. 448E+OO ------Line Not Found ------351. 06 247 12.92* 3.588E+OO 2.414E+00 2.414E+OO 19.50 BI-212 727. 33 48 6.67* 2.003E+00 1.627E+OO l.627E+OO 42.86 785.37 23 1.10 1.888E+OO 5.097E+00 5.097E+OO. 63.14 1620.50 ------1. 47 1.045E+OO ------Line Not Found ------PB-212 74.82 135 10.28 3.688E+OO 1.608E+OO 1.608E+OO 40.64 77 .11 198 17.10 3.924E+OO 1.334E+OO 1.334E+OO 26.50 238.63 448 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 300.09 40 3.30 . 4. 084E+OO 1.329E+OO 1. 32 9E+OO 76.02 BI-214 609.32 162 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 1120.29 42 14.92 l.430E+OO 8.894E-01 8.898E-01 37.99 176'4. 49 29 15.30 9.661E-01 8. 891E-01 8.894E-01 38.85 PB-214 74.82 135 5.80 3.688E+00 2.851E+OO 2.852E+OO 40.64 77 .11 198 9.70 3.924E+OO 2. 351E+OO 2.352E+00 26.50 87.09 87 3.41 4.861E+OO 2.365E+OO 2.366E+00 55.60 242.00 117 7.25 4.838E+00 i.505E+OO l.505E+OO 47.68 295.22 185 18.42 4.142E+OO 1. 096E+OO l.097E+00 21. 60 351.93 247 35.60* 3.588E+OO 8.760E-01 8.763E-01 19.50 RN-222 609.32 162 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 1120. 29 42 14.92 1 .. 430E+OO 8.894E-01 8.898E-01 37.99 1764.49 29 15.30 9.661E-01 8. 8 91E-01 8.894E-01 38.85 RA-224 240.99 117 4.10* 4.838E+OO 2.661E+OO 2. 661E+OO 47.68 RA-226 609.32 162 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 1120.29 42 14.92 1.430E+OO 8.894E-01 8.898E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 AC-228 105.21 ------1.10 5. 896E+OO ------Line Not Found ------338.32 107 11. 27 3.705E+OO l.164E+OO 1.164E+OO 29.06 794.95 ------4.25 1.870E+OO ------Line Not Fou_nd ------835. 71 ------1. 61 1. 799E+OO ------Line Not Fourid ------911.20 66 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 968.97 40 15.80 1.603E+OO 7.182E-01 7.182E-01 52.38 RA-228 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 . 107 11. 27 3.705E+OO 1.164E+OO l.164E+00 29.06 794.95 ------4.25 1. 870E+OO ------Line Not Found ------835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 66 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 Page 3918 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 968. 97 40 15.80 1.603E+OO 7.182E-:-01 7.182E-01 52.38 TH-228 74.82 135 10.28 3.688E+OO l.608E+OO 1.608E+OO 40.64 77 .11 198 17.10 3.924E+OO 1.334E+OO 1.334E+.00 26.50 238.63 448 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 300.09 40 3.30 4.084E+OO 1.329E+OO 1.329E+OO 76. 02 TH-230 609.32 162 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 1120. 29 42 14.92 l.430E+OO 8.894E-01 8.894E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8.891E-01 38.85 PA-231 283.69 ------1. 70 4.275E+OO ------Line Not Found ------301.36 40 5 .*35* 4.084E+OO 8.196E-01 8 .196E-01 76.02 TH-232 105. 21* ------1.10 5. 896E+OO ------Line Not Found ------338.32 107 11.27 3.705E+OO 1.164E+OO 1.164E+OO 29.06 835.71 ------1. 61 1.799E+OO ------Line Not Found ------911.20 66 25.80* 1.682E+OO 6.848E-01 6.848E-01 34. 51. 968. 97 40 15.80 1.603E+OO 7.182E-01 7.182E-01 52.38 PA-234M 766.42 33 0.32 l.922E+00 2.426E+Ol 2.426E+Ol 54.67 1001.03 6 0.84* 1.562E+OO 2.181E+OO 2.181E+OO 245 .11 TH-234 63.29 56 3.70* 2.275E+OO 2.992E+OO 2.992E+OO 109.24 92.59 82 4 .*23 5.276E+OO 1. 671E+OO 1.671E+OO 71'.54 U-234 609.32 162 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 1120. 29 42 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8.891E-01 38.85 U-235 89. 96 63 3.47 5.079E+OO 1.616E+OO l.616E+00 71. 57 93.35 82 5.60 5.276E+OO 1.262E+OO 1. 2 62E+OO 71. 54 143.76 22 10. 96* 6.313E+OO l.450E-01 l.450E-01 210.79 163.33 ------5.08 6.096E+00 ------Line Not Found ------185. 72 105 57.20 5.741E+OO 1.453E-01 1.453E-01 42.94 205.31 ------5.01 5.415E+OO ------Line Not Found ------U-238 63.29 56 3.70* 2.275E+OO 2.992E+OO 2.992E+OO 109.24 92.59 82 *4.23 5.276E+OO 1.671E+OO 1. 671E+OO 71. 54 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 135 67.20* 3.688E+OO 2.460E-01 2.461E-01 40.64 ANH-511 511. do 25 100.00* 2.647E+OO 4.355E-02 4.355E-02 180.49 Flag: "*" Key line Page 3919of5809 Page : 3 Surrunary of Nuclide Activity Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Total number of lines in spectrum 48 Number of unidentified lines 11* Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 NB-95 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-234M TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 64.03D 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY l.41E+l0Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay . 1. 00 28.0 1. 59 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 361E+Ol 7.778E-02 2.179E+OO 2.179E-01 6.441E-02 6.804E-02 2.978E-01 2.414E+OO 1.627E+OO 9.538E-01 7.025E-01 8.760E-01 7.025E-01 2.661E+OO 7.025E-01 6. 848E...:01 6.848E-01 9.538E-01 7.025E-01 8 .196E-01 6.848E-01 2.181E+OO 2.992E+OO 7.025E-01 1.450E-01 2.992E+OO 2.460E-01 4.355E-02 4.099E+Ol 4.099E+Ol Decay Corr pCi/GRAM 1.361E+Ol 2.176E+OO 3.460E+OO 2.179E-01 6.567E-02 6.938E-02 2.978E-01 2.414E+OO 1.627E+OO 9.538E-01 7.028E-01 8.763E-01 7.028E-01 2.661E+OO 7.028E-01 6.848E-01 6.848E-01 9.538E-01 7.025E-01 8 .196E-01 6.848E-01 2.181E+OO 2.992E+OO 7.025E-01 l.450E-01 2.992E+OO 2.461E-01 4.355E-02 4.437E+Ol 4.437E+Ol 77.08% Decay Corr 2-Sigma Error 0.146E+Ol 1.190E+OO 1.924E+OO l.212E-01 5.166E-02 5.457E-02 0.735E-01 0-.471E+OO 0.698E+OO l.181E-01 1. 376E-01 1. 709E-01 1. 376E-01 1. 269E+00 l.376E-01 2.363E-01 2.363E-01 l.181E-01 1.376E-01 6.231E-01 2.363E-01 5.345E+OO 3.268E+OO 1. 37 6E-01 3.056E-01 3.268E+OO l.OOOE-01 7.860E-02 "M" Manually accepted 2-Sigma %Error 10.73 54 .. 67 55.60 55.60 78.66 78.66 24.69 19.50 42.86 12.38 19.58 19.50 19.58 47.68 19.58 34.51 34.51 12.38 19.58 76.02 34.51 245 .11 109.24 19.58 210.79 109.24 40.64 180.49 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3920 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235043 Acquisition date.: 3-0CT-2016 06:56:18 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags .2 188.10 26 105 1. 25 375.98 365 14 5.83E-03 **** 5.70E+OO 0 270.56 39 92 1. 21 540.97 534 11 9.06E-03 **** 4.44E+OO T 1 343.92 21 29 1. 33 687.76 672 21 4.89E-03 **** 3.66E+OO T 0 369.64 80 59 8. 98 739.21 728 23 1. 91E-02 59.4 3.45E+OO 0 462.19 62 17 0.92 924.39 918 12 l.53E-02 39.0 2.87E+00 T 0 532.02 21 19 1. 04 1064.11 1061 9 5.30E-03 88.6 2.56E+OO T 0 558.91 7 12 1. 21 1117.92 1114 7 1. 7 9E-03 **** 2.46E+OO 0 630.75 17 13 1. 71 1261.66 1258 7 4.42E-03 88.3 2.24E+OO T 3 656.18 14 20 1. 94 1312.56 1308 27 3.53E-03 **** 2.17E+OO 0 796. 66 17 21 0.85 1593.64 1588 13 4.58E-03 **** 1. 87E+OO T 0 935.55 17 23 0.58 1871. 55 1864 17 4.46E-03 **** 1.65E+OO 0 1008.00 7 10 0. 70 . 2016.53 2011 7 l.77E-03 **** 1. 55E+OO 0 1086.29 11 10 1. 94 2173.18 2168 10 3.06E-03 **** 1. 46E+00 T 0 1175. 33 16 . 11 3.35 2351.36 2346 12 4.53E-03 97.4 l.37E+00 b 1200.56 29 3 5.17 2401. 84 2396 14 8. llE-03 45.6 1.35E+OO 0 1238.33 13 16 0.69 2477.42 2472 9 3.64E-03 **** 1.32E+OO T 0 1271.23 16 0 0.98 2543.25 2537 12 4.44E-03 50.0 1.29E+OO T 0 1377.36 7 3 1. 05 2755.63 2752 6 l.97E-03 **** 1. 21E+OO 0 1450.18 5 0 0. 96 2901.33 2898 6 1. 42E-03 97.4 1.15E+OO 0 1607.01 6 1 0.94 3215.17 3212 6 1.81E-03 98.5 1.05E+OO Flags: "T" = Tentatively associated Page 3921of5809 VAX/VMS Nuclide.Identification Report Generated 03-0CT-2016 07:58:53.48 *******************************************************************************
GEL.Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l *
Acquisition date 3-0CT-2016 06:56:18 Sensitivity 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Aoundance limit : 75.000 *
Elapsed real time: 0 01:00:00.51 Half life ratio : ***** *
Sample date 30-NOV-2015 13:59:00 Nuclide Library : SOLID *
Sample ID G405235043 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.6579E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* *
CALIBRATION INFORMATION * * * * * .Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nucli.de K-40 NB-95 CD-109 SN-126 BA-137M CS-137 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-234M TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.708E-01 5.553E-01 8.325E-01 5.280E-02 2.049E-02 2.164E-02 2.035E-02 3.374E-01 3.549E-02 3.755E-02 4.193E-02 3.755E-02 3.805E-01 3.755E-02 9.363E-02 9.363E-02 3.549E-02 3.754E-02 2.600E-01 9.363E-02 3.012E+OO 1.054E+00 3.754E-02 l.175E-01 1. 054E+OO* 3.817E-02 2.237E-02 ----Non-Identified *Nuclides Nuclide BE-7 NA-22 AL-26 Page 3922 of 5809 Le (pCi/GRAM 8.834E+00 2. 7,80E-02 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3923 of 5809 2.505E-01 O.OOOE+OO O.OOOE+OO 4.830E-02 3.758E-01 O.OOOE+OO 3.333E-02 4.387E-01 5.795E+OO 2.164E-02 l.002E-01 1. 566E+OO 9.783E+OO O.OOOE+OO 1.544E-01 O.OOOE+OO O.OOOE+OO 5.305E-01 6.080E+OO 6.976E-01 O.OOOE+OO 8.480E-02 3.212E+02 2.604E-02 1.815E+OO 1.201E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.519E-02 5.160E-02 3.926E+OO 3.057E-01 3.057E-01 2.038E-02 7. 968E-02 1.662E-01 O.OOOE+OO O.OOOE+OO 9.984E-02 1.329E+OO 8. 112E-02 2.342E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0 .. OOOE+OO 0.000E+OO O.OOOE+OO 2.050E-02 O.OOOE+OO 3. 981E-02 8.150E-02 O.OOOE+OO 0.000E+OO 6.840E-02 O.OOOE+OO O.OOOE+OO 2.034E+Ol O.OOOE+OO 2.616E-01 4.033E-02 3.518E+OO 2.756E-02 0.000E+OO 5.593E+02 O.OOOE+OO l.829E-02 6.342E-02 l.245E-01 6.989E-02 8.128E-02 1. 421E+OO 3 .114E-02 2.187E+Ol 1.686E-01 .5. 492E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN "FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211. PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 'CM-247 CF-249 .CF-251 Page 3924 of 5809 1. 865E-02 3.706E+OO 7.209E-01 3.324E+OO* 2.621E+Ol 7.025E+Ol 3.405E-01 1.697E+OO 2. 960E-02 5.325E+OO 3. 391E-01 4.586E-01 2.545E-01 4.140E-01 l.546E-01 1.546E-01 2.875E-01 4.140E-01 4.465E-02 2.076E-01 4.465E-02 O.OOOE+OO 1.558E-01 2.384E+02 l.432E-01 6.888E-02 5.055E-02 2.386E-02 2.838E-02 7.248E-02 FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:58.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l *
Acquisition date 3-0CT-2016 06:56:18 Sensitivity : 3.000 *
Detector ID GAM09 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : .75.000 *
Elapsed real time: 0 01:00:00.51 Half. life ratio : ***** *
Sample date 30-NOV-2015 13:59:00 Nuclide Library : SOLID *
Sample ID G405235043 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.6579E+02 GRAM *
Quantity Err(%) 1.2063E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * * *
CALIBRATION INFORMA.TION * * *
Eff. Cal. date 3-JUN-2016 07:32:22 Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 361E+Ol 1.598E+OO NB-95 1.980E+OO 1. 2 60E+OO CD-109 1.856E+OO 1.932E+OO SN-126 l.169E-Ol 1.215E-01 BA-137M 6.567E-02 5.071E-02 CS-137 6.938E-02 5.356E-02 TL-208 2.978E-01 7.314E-02 BI-212 1. 62*7E+OO 6.885E-01 PB-212 9.538E-01 1.262E-01 BI-214 7.028E-01 1.382E-01 PB-214 8.763E-01 1. 713E-01 RN-222 7;028E-01 l.382E-01 RA-224 7.219E-01 1.316E+OO RA-226 7.028E-01 1.382E-01 AC-228 6.848E-01 2.342E-01 RA-228 6.848E-01 2.342E-01 TH-228 9.538E-01 1. 2 62E-01 TH-230 7.025E-01 1. 381E-01 PA-231 8 .196E-01 6.352E-01 TH-232 6.848E-01 2.342E-01 PA-234M 2.181E+OO 5.239E+OO TH-234 2.992E+OO 3. 271E+OO U-234 7.025E-01 1. 381E-01 U-235 1.450E-01 2. 996E-01 U-238 2.992E+OO 3.271E+OO AM-243 l.514E-01 .1.012E-01 ANH-511 4.355E-02 7.705E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3925 of 5809 Key-Line Activity (pCi/GRAM -5.083E+OO -3.298E-02 1.000E+41 K.L Act error (1.96-sigma) l.050E+Ol 4.608E-02 2.714E+41 TPU ( 1. 96-sigma) 1. 598E+OO 1. 260E+OO 1. 932E+OO 1. 215E-01 5. 071E-02 5.356E-02 7.314E-02 6.885E-01 1.262E-01 1.382E-01 l.713E-01 1.382E-01 1.316E+OO 1.382E-01 2.342E-01 2.342E-01 1.262E-01 1.381E-01 6.352E-01 2.342E-01 5.239E+OO 3. 271E+OO . 1. 381E-01 2. 996E-01 3.271E+OO l.012E-01 7.705E-02 TPU (1. 96-sigma) 1. 074E+Ol 4.842E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -l.929E-02 l.902E-02 2.091E-02 NOT IDENT. SC-46 -6.499E-04 2.958E-01 2.958E-01 FAIL ABUN V-48 6.456E+03 1.675E+04 1. 700E+04 SHORT HLIF CR-51 8.305E+Ol 3.952E+02 3.970E+02 SHORT HLIF MN-54 -2.346E-02 6.064E-02 6.156E-02 NOT IDENT. C0-56 -7.088E-02 4.541E-01 4.552E-01 FAIL ABUN MN-56 -1.000E+41 6.120E+41 O.OOOE+OO SHORT HLIF C0-57 -1.012E-02 3.674E-02 3.702E-02 NOT IDENT. C0-58 -6.584E-02 5.251E-01 5.260E-01 NOT IDENT. FE-59 -1. 8 64E+OO 7.403E+OO 7. 451E+OO NOT IDENT. C0-60 l.303E-02 2.081E-02 2.162E-02 NOT IDENT. ZN-65 4. lOlE-02 1. 211E-01 1.225E-01 NOT IDENT. GE-68 -9.442E-01 2.044E+OO 2.088E+OO NOT IDE.NT. AS-73 6.689E-01 9.849E+OO 9.853E+OO NOT IDENT. AS-74 3. 681E+Ol 5.697E+03 5.697E+03 SHORT HLIF SE-75 1.556E-01 1. 57 6E-01 l.725E-01 NOT IDENT. BR-77 1. 707E+39 l.516E+40 O.OOOE+OO SHORT HLIF SR-82 -2.042E+02 5.914E+02 5.985E+02 SHORT HLIF RB-83 4.079E_:_02 5.848E-01 5. 851E-01 NOT IDENT. KR-85 2.432E+00 7.156E+OO 7.239E+OO NOT IDENT. SR-85 2.780E-01 8.212E-01 8.307E-01 NOT IDENT. RB-86 -1.835E+04 3.325E+04 3.426E+04 SHORT HLIF Y-88 -1.493E-03 1.027E-01 l.027E-01 NOT IDEN'I'.. Y-91 1.700E+Ol 4.088E+02 4.088E+02 NOT IDENT. NB-94 2.445E-02 2.628E-02 2.850E-02 NOT IDENT. NB-95M 8.954E-01 2.120E+OO 2.158E+OO NOT IDENT. ZR-95 7.360E-01 1. 261E+OO 1.304E+OO NOT IDENT. NB-97 1.000E+41 7.501E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1.727E+41 O.OOOE+OO SHORT HLIF M0-99 -2.204E+32 l.060E+33 0.000E+OO SHORT HLIF TC-99M -l.000E+41 3.088E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 272E-02 2.829E-02 2.887E-02 NOT IDENT. RH-102 7.303E-02 6.346E-02 7.150E-02 FAIL ABUN RU-103 -l.355E+00 4.569E+OO 4.609E+OO FAIL ABUN RH-106 -1.012E-01 3.653E-01 3.682E-01 NOT IDENT. RU-106 -1.012E-01 3.653E-01 3.682E-01 NOT IDENT. AG-108M l.481E-02 2.038E-02 2.145E-02 NOT IDENT. AG-110M -6.400E-03 9.520E-02 9.524E-02 NOT IDENT. SN-113 6.763E-02 l.715E-01 1.742E-01 NOT IDENT. CD-11,5 6.029E+39 3.343E+40 O.OOOE+OO. SHORT HLIF SN-117M 3.007E+04 1.104E+05 1.112E+05 SHORT HLIF TE-123M 2.882E-02 1.070E-01 l.078E-01 NOT IDENT. SB-124 -9.836E-03 1.580E+OO 1.580E+OO NOT IDENT. ss.:..125 3.695E-02 8.422E-02 8.585E-02 FAIL ABUN TE-125M 6.063E+Ol 2.445E+02 2.461E+02 NOT IDENT. I-126 3.889E+05 1.059E+06 1.073E+06 SHORT HLIF SB-126 2.324E+05 1.369E+06 l.373E+06 SHORT HLIF SB-12.7 -5.464E+22 1.048E+23 O.OOOE+OO SHORT HLIF -1. 029E+09 8.207E+09 8.220E+09 SHORT HLIF I-132 -1.000E+41 l.903E+42 O.OOOE+OO SHORT HLIF TE-132 7.295E+25 1.630E+27 O.OOOE+OO SHORT HLIF BA-133 -2.088E-02 3.136E-02 3.275E-02 FAIL ABUN I-133 1.000E+41 8.721E+42 O.OOOE+OO SHORT HLIF CS-134 6.551E-02 7.763E-02 8.305E-02 FAIL ABUN CS-135 ' -1.554E-02 9.616E-02 9.642E-02 NOT IDENT. I-135 -l.000E+41 1.188E+42 O.OOOE+OO SHORT HLIF CS-136 -2.153E+04 3.927E+05 3.929E+05 SHORT HLIF CE-139 -5.700E-02 8.235E-02 8.626E-02 NOT IDENT. BA-140 l.218E+06 1. 548E+06 1. 643E+06 SHORT HLIF LA-140 5.954E+04 4.165E+05 4.173E+05 SHORT HLIF CE-141 -2.573E+00 2.420E+Ol 2.423E+Ol NOT IDENT. CE-143 1.000E+41 1.309E+41 O.OOOE+OO SHORT HLIF CE-144 l.490E-01 2.698E-01 2.780E-01 NOT IDENT. PM-144 -l.161E-02 4.815E-02 4.844E-02 NOT IDENT. PR-144 -1.012E+OO 4.200E+OO 4.225E+00 NOT IDENT. PM-146 -2.848E-02 3.424E-02 3.657E-02 NOT IDENT. ND-147 7.802E+07 6.787E+07 7.644E+07 SHORT HLIF PM-147 -3.271E+02 6.310E+02 6.480E+02 NOT IDENT. PM-149 l.OOOE+41 l.651E+41 O.OOOE+OO SHORT HL'IF EU-150 1.443E-02 2.088E-02 2.187E-02 FAIL ABUN EU-152 9.991E-02 1.118E-01 l.206E-01 FAIL ABUN GD-153 -7.806E-02 l.392E-01 l.436E-01 NOT IDENT. EU-154 -7.594E-02 l.134E-01 1.184E-01 NOT IDENT. EU-155 5.660E-02 8.158E-02 8.548E-02 FAIL ABUN TB-160 8.732E-01 1. 487E+OO 1.538E+OO FAIL ABUN H0-166M -l.685E-02 3.938E-02 4. OllE-02 FAIL ABUN TM-171 -6.819E+OO 2.279E+Ol 2.299E+Ol NOT IDENT. HF-172 -2.022E-02 1.834E-01 l.836E-01 FAIL ABUN Page 3926 of 5809 LU-172
1. 477E-03 6.615E-02 6.616E-02 FAIL ABUN LU-176 l.063E-02 2.043E-02 2.099E-02 FAIL ABUN HF-181 2.753E+OO 3. 721E+OO 3.923E+OO NOT IDENT. TA-182 -4.634E-01 8.981E-01 9.220E-01 NOT IDENT. RE-183 -5.402E-01 3.430E+00 3.438E+OO NOT IDENT. RE-184 5.587E-01 3.089E+Ol 3.089E+Ol NOT IDENT. W-188 -8.200E+OO 9.014E+Ol 9.022E+Ol FAIL ABUN IR-192 -7.425E-02 4.095E-01 4.108E-01 FAIL ABUN HG-203 -4.247E-02 2.137E+OO 2.137E+OO NOT IDENT. BI-207 -l.958E-02 3.944E-02 4.042E-02 FAIL ABUN PB-210 -7.391E-01 5.468E+OO 5.478E+00 NOT IDENT. BI-211 2.414E+OO 4.735E-01 l.187E+OO FAIL ABUN PB-211 1.140E-01 4.837E-01 4.864E-01 NOT IDENT . RN-219 -5.026E-02 2.823E-01 . 2. 832E-01 FAIL ABUN RA-223 2.867E-01 4.452E-01 4.636E-01 FAIL ABUN AC-227 -8.344E-02 l.878E-01 1.915E-01 FAIL ABUN TH-227 -8.344E-02 l.878E-01 l.915E-01 FAIL ABUN TH-229 -3.259E-01 3.567E-01 3.858E-01 FAIL ABUN TH-231 2.867E-01 4.452E-01 4.636E-01 FAIL ABUN PA-233 1.935E-02 4.971E-02 5.047E-02 FAIL ABUN PA-234 4.847E-02 2.436E-01 2.445E-01 NOT IDENT. NP-237 1.935E-02 4.971E-02 5.047E-02 FAIL ABUN N.P-238 -1.DOOE+41 2.896E+41 O.OOOE+OO SHORT HLIF NP-239 -4.255E-02 l.709E-01 1. 720E-01 FAIL ABUN PU-239 4.167E+Ol 2.540E+02 2.547E+02 NOT IDENT. AM-241 5. 728E-02 1.418E-01 1. 441E-01 NOT IDENT. CM-243 3. 221E-03 7.276E-02 7.277E-02 FAIL ABUN BK-247 3.348E-02 5.816E-02 6.008E-02 NOT IDENT. CM-247 2.355E-03 2.560E-02 2.562E-02 FAIL ABUN CF-249 3.848E-02 2.795E-02 3.290E-02 NOT IDENT. CF-251 -3.990E-02 8.470E-02 8.659E-02 NOT IDENT. Page 3927 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 41.9090 87.09 67. 6372 136.47 52.7609 45.60 52.3724 87.57 67.7092 140.51 0.0000 46.54 45.4820 88.03 67.7770 143.76 50.4599 49.72 0.0000 88.34 67.8230 144.24 50.4972 51. 35 43.8109 88.47 67.8425 145.44 60.9684 51. 87 40.6912 89.96 68.0626 152.43 54.0777 52.39 40.7574 1093.63 31. 7307 153.25 0.0000 52.97 44.8339 91.11 0.0000 323.87 55.2053 53.44 38.4847 92.59 49.5644 156.02 0.0000 54.07 46.5922 93.35 49.6439 158.56 0.0000 57.36 0.0000 94.56 53.3249 159.00 51.6207 57.53 55.1932 94.65 53.3345 162.33 40.8949 57.98 56.8908 94.67 53.3368 162.66 0.0000 59.27 53.0245 94.87 53.3592 163.33 47.9451 59.32 53.0322 97.43 57.2173 165.86 51.1230 59.54 53.0654 98.43 54.6465 176.31 47.7896 60. 96 59.0175 98.44 54.6474 176.60 0.0000 61.17 59.0523 99.53 52.9723' 177.52 50.9224 62.93 56.8698 100.11 58. 4272 181.07 0.0000 63.29 56.9261 102. 03 46.9207 181.52 40.9528 63.58 56.9712 103.18. 52.4532 184.41 55.4939 64.28 57.0801 103.37 49.7586 143.76 55.5878 66.73 51.0724 105.21 49.0294 193.51 57.1778 67.24 50.0294 105.31 46.3145 197.03 57.4271 125.81 63.4443 106.12 51.8441 198.01 52.2697 67.75 64.2902 106.47 53.6992 201.83 46.2115 69.67 57.0601 109.28 59.4770 203.43 46.3008 70.83 68.4506 111. 00 71. 6028 205.31 43.2409 72.81 72.1764 111.76 0.0000 210.85 49.8938 72. 87 72.1875 114. 06 56.3140 215.65 38.4296 74.66 64.5773 116. 30 0.0000 222 .11 51.6174 74.82 64.6028 116.74 49.1667 227.09 42.1724 74 .. 97 64.6266 119.76 42.9032 227.38 31.3692 77 .11 64. 9623 121.12 58.8996 228.16 0.0000 78.74 61.7827 121. 22 58.9097 228.18 40.0583 79.69 74.5347 121.78 48. 6714 116.74 40.0583 80.12 68.8708 122.06 56.1868 235.69 80.19 0.0000 122.92 48.7681 235. 96 49'. 4976 80.57 67.7938 123.07 47.8425 238.63 44.8938 81. 00 70.1620 265.00 61. 0402 238.98 0.0000 81. 07 73.6250 125.81 61.2633 240.99 45.0064 81. 75 65.6755 127.23 72.7485 242.00 45.0546 83.79 74.0853 127.91 63.3738 244.70 27.9175 84.00 74.1204 129.30 65.4171 252.40 0.0000 85.43 7.3.1975 131.20 64.6735 252.80 31.1155 86.55 67.5563 133. 02 57.2360 254.15 0.0000 86.79 67.5923 133.52 46.7809 256.23 44.6057 86. 94 67.6147 136.00 55. 5968 260.90 0.0000 Page 3928 of 58,09 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 22.4908 355.39 0.0000 584.27 14.0930 264.80 20.9943 356.01 24.3646 595.83 .0. 0000 265.00 26.9978 364.49 0.0000 427.87 24.6374 268.22 29.3405 366.42 0.0000 602.52 0.0000 269.46 29.3762 372. 51 17.2731 604. 72 14.2444 270.03 29.3920 375.05 29.6682 607.14 12.3605 271.23 36.2168 377.52 19.8154 609.32 12.8502 273.65 0.0000 356.01 14.9315 610.33 18.5709 . 276.40 31. 8478 388.16 12.4826 614.28 *13. 3597 277.37 31. 87 68 388.63 0.0000 618.01 12.4292 277.60 31. 8837 391.69 20.0239 620.36 16.2723 278.00 31.8956 264.66 25.1923 621. 93 15.3275 279.20 30. 4118 401.81 26.0528 630.19 0.0000 279.54 30.4215 402.40 23.5418 631.29 24.5423 279.70 31. 9469 404.85 21.8984 633.25 23.1211 280.46 31.9700 410.95 26.2218 634.78 0.0000 283.69 37.7937 413.71 28.8148 635.95 19.2936 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 20.6477 423.72 0.0000 645.85 12.6017 285.90 0.0000 427.09 23.0944 657.76. 12.6747 287.50 33.3304 427.87 23.1064 657.90 0.0000 290.67 26.1274 433.94 16.3270 661.66 12.6985 293.27 0.0000 439.40 21.5612 664.57 0.0000 351. 93 25.4644 453.88 28.7320 666.33 0.0000 295. 96 25.4811 463.37 18.3959 666.50 0.0000 879.38 25.5416 468.07 667.71 0.0000 299.98 25.5738 473.00 0.0000 677.62 12.7948 300.09 25.5758 475.06 18.5322 685.70 0.0000 300.13 25.5771 476.78 21.2021 695.00 0.0000 301.36 25.6053 477.60 22. 0968 696.49 20.8505 302.85 29.5236 482.18 15.0687 696. 51 20.8505 256.23 37.3477 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.8784 306.78 30.4061 497.08 17.8894 697.49 17.8799 308.46 40.9921 505.52 20.2277 702.65 12.9434 311. 90 30.5425 507.63 0.0000 706.68 15. 9596 316.51 33.0236 511. 00 .28.8613 711. 68 13. 9966 319.41 0.0000 514.00 29.8163 720.70 0.0000 320.08 0.0000 514.00 29.8163 721. 93 0.0000 321. 04 34.3348 520.40 21.7656 722.78 15.0708 323.87 22.5492 520.69 0.0000 722. 91 15. 0714 325.23 45.1505 522.65 0.0000 723.31 13.5670 328.76 0.0000 527.90 0.0000 724.19 19.6039 333.37 23.9252 528.26 15.0317 727. 33 17.1148 333 .*97 22.3410 529.59 17.7782 733.00 9.6891 334.37 20.7521 529.87 0.0000 735.93 14.1481 338.28 20.4184 531. 02 0.0000 333.97 12.1348 338.32 20.4189 537.26 0.0000 739.50 0.0000 311. 90 20.4547 546.56 0.0000 747.24 20.3109 340.48 20.4547 552.55 22.1660 748.06 18.2864 340.55 0.0000 563.25 19.5089 752.31 13.2312 344.28 20.5180 569.33 21. 4380 753.82 0.0000 345.93 22.5592 946.00 21.4399 756.73 11. 2166 351.06 23.0559 569.70 19.5773 756.80 11.2171 351.93 23. 0722 583.19 14.0851 884.68 10.7401 Page 3929 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 12.2837 1274.44 11. 7296 1620.50 2.9833 766.42 12.2871 1001.03 13. 4272 1621.92 1.9895 766.84 12.2891 1002.74 13.4351 1678.03 0.0000 772.60 0.0000 1004.73 11. 2032 . 1690.97 3.0300 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0519 778.90 7. 4112 1028.54 0.0000 1063.66 4.1089 783.70 0.0000 1037.84 7.9297 1771.35 *4.1096 785.37 9.2889 1038.76 0.0000 1791.20 0.0000 792.07 15.5243 631.29 11.3607 1808.65 2.0708 794.95 9.3256 1048.07 0.0000 1810. 72 0.0000 795.86 9. 3292. 1049.04 11. 3696 1836.06 1. 0411 810.06 15.6390 1050.41 19.3367 810.29 13.5549 1063.66 11. 4233 344.28 13.5559 1077.00 . 0.0000 810.76 14.6004 ' 1077. 34 12. 6212 815.77 0.0000 1085.87 4.6019 1048.07 0.0000 1093.63 11. 5332 832.01 12.6216. 1099.45 16.1761 834.85 21.0596 111*2. 07 15.0799 835. 71 14.7468 . 1112.84 11. 6024 836.80 0.0000 1115. 54 5.2255 846.75 0.0000 1120.29 10.4663 846.77 16.9264 1120. 55 10.4670 856.80 0.0000 1221.41 6.9795 860.56 17.0176 1129. 67 9.3301 871.09 7.4751 1131.51 0.0000 873.19 5.3436 1147.95 0.0000 875.33 0.0000 1173.23 15.5987 879.38 7.4987 1177.95 9.9401 880.51 18.2188 1189.05 16.0280 883.24 9.6552 1204.77 7.1563 884.68 16.1011 1221.41 19.7737 889.28 9.6771 1231.02 14.4209 894.76 16.1615 1235.36 0.0000 898.04 11.8665 1238.28 18.7853 900.72 20.5168 1260.41 0.0000 903.28 14. 0511 1271.87 2.7350 911. 20 14.0923 1274.44 14.5977 912.08 21.1456 1274.54 14.5977 923.98 0.0000 1291.59 6.4168 926.50 10.9009 1298.22 0.0000 929 .11 8.1833 1312 .11 0.0000 937.49 12.0384 1332.49 1.8536 944.13 0.0000 1362 .*66 0.0000 946.00 12.0751 1365;19 7.4790 949.00 14.2859 1368.63 0.0000 667. 71 0.0000 1384.29 11. 2742 962. 31 15. 4572 1408.01 3.7808 964.08 18.2288 1457.56 0.0000 966 .17 28.1926 1460.82 3. 8311 911.20 18.8130 1489.16 4.8221 968.97 18.8130 1505.03 5.8088 983.53 0.0000 1584.12 12.8215 984.45 0.0000 1596.21 0.0000 Page 3930 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:59:26.88 * ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * *Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277 Background date : 2-0CT-2016 11:01:57. Sample date 30-NOV-2015 13:50:00 Acquisition date*: 3-0CT-2016 06:56.:59. Sample ID G405235044 Sample quantity
1. 28844E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.0D Elapsed real time: 0 01:00:00.59 0.0% Energy tole.ranee : 1. 50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 . 0 2 4 3 4 4 0 5 0 6 0 7 0 8 2 9 2 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 54.86 75.44 77.42 89.77 93.17* 186.38* 210.19 239.04* 242 .11 271. 41 295.65* 299.84 339.15 352.37* 391.59 466.45 511.13* 583.63* 609.82* 662. 31 729.12* 774.90 795.25 835.57 841.13 860.36 911. 98* 969.82 993.29 1028.32 1038.30 1120. 99* 1157. 37 1171.94 Page 3931 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 38 130 151 51 51 115 53 388 97 25 146 34 63 232 21 20 71 107 181 93 26 9 13 20 22 40 80 71 20 10 8 40 16 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 83 180 126 263 125 148 121 58 44 68 52 43 103 59 44 59 .41 35 36 43 48 31 18 6 6 10 31 11 6 5 8 24 5 6 1.11 1. 59 1.15 3.52 1.15 1. 59 2.38 1.26 1. 49 1. 42 1. 43 1. 58 1.30 1. 31 2.32 5.18 2.83 1.27 1. 60 1.22 0.74 4.60 1. 03 4.54 1. 58 2.46 1. 59 1. 47 1. 51 2.60 0.66 1. 68 2.46 1. 87 110. 93 152.10 156.04 180.75 187.55 373.98 421. 60 479.30 485.45 544.04 592.53 600.89 679.52 705.97 784.40 934 .13 1023.49 1168. 50 1220.89 1325.87 1459.49 1551.05 1591.76 1672.40 1683.51 1721.97 1825.21 1940.90 1987.85 2057.90 2077.88 2243.25 2316.02 2345.15 107 147 147 172 184 368 415 472 472 538 587 598 672 701 780 925 1015 1162 1215 1321 1451 1544 1586 1666 1678 1715 1820 1935 . 1981 2051 2073 2238 2312 2341 8 1.05E-02 44.8 14 3.62E-02 22.5 14 4.19E-02 15.1 12 1.42E-02 65.4 8 1.41E-02 43.2 15 3.20E-02 25.3 11 1.46E-02 43.3 17 1.08E-01 6.2 17 2.70E-02 15.9 9 6.81E-03 63.7 10 4.06E-02 12.6 8 9.45E-03 37.3 15 1. 75E-02 37 .1 12 6.43E-02 9.5 10 5.85E-03 63.3 15 5.61E-03 86.4 14 l.96E-02 26.3 12 2.97E-02 15.0 10 5.04E-02 9.8 12 2.59E-02 17.4 17 7.21E-03 64.3 14 2.57E-03132.5 10 3.58E-03 67.2 12 5.56E-03 33.2 11 5.97E-03 30.2 13 1.12E-02 22.3 12 2.23E-02 18.4 12 1.97E-02 15.3 14 5.53E-03 35.7 10 2.72E-03 53.5 8 2.22E-03 70.7 13 1.12E-02 29.4 9 4.38E-03 38.1 8 3.40E-03 44:8 Fit 1.51E+OO 2.43E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1322.39 7 8 3.09 2646.06 2639 11 1.97E-03 86.5 36 0 1377.89 22 7 1. 35 2757.07 2749 14 6.11E-03 33.2 37 0 1461. 23* 330 0 2 .11 2923.75 2918 13 9.16E-02 5.6 38 5 1492.06 7 1 1. 39 2985.42 2984 11 1.83E-03 27.3 6.33E-01 39 5 1494.77* 10 2 1. 92 2990.84 2984 11 2.68E-03 46.7 40 0 1765.20* 34 3 2.54 3531. 71 3526 11 9.53E-03 20.2 Flag: "*" = Peak area was m6dif{ed by background subtraction Page 3932 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:59:28. Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l Analyses by PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3,4,INTERF V2.4 Sample title MXRl Sample date 30-NOV-2015 13:50:00 Sample ID G405235044 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 06:56:59 128.84 GRAM Sample type SOLID Detector name : GAMMA32 Elapsed live time:. 0 01:00:00.00 Energy tolerance : 1.50 keV Errors propagated: No Efficiency type : Linear Abundance limit* 75.00 Report Interfering Nuclide Page 3933 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA:-224 AM-243 TH-228 PB-212 BI-211 Line 240.99 74.66 74.82 74.82 351.06 CAN 0 01:00:00.59 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* l .119E+OO 1.532E+Ol 1. 532E+Ol 11.13 OK MN-54 834.85 99.98* 1. 753E+OO 6.575E-02 1.302E-01 66.33 OK AS-73 53.44 10.30* 1.124E+OO 2.236E+OO 3.186E+Ol 89.65 OK SN-113 391.69 64.94* 3.225E+OO 6.089E-02 3.886E-01 126.61 OK BA-137M 661.66 89.90* 2.104E+OO 2.882E-01 2.939E-01 34.77 OK CS-137 661.66 85.10* 2.104E+OO 3.045E-01 3.105E-01 34.77 OK TL-208 277.37 6.60 4.277E+00 Line Not Found Absent 583.19 85.00* 2.326E+OO 3.194E-01 3.194E-01 29.96 OK 860.56 12.50 1.714E+OO l.087E+OO 1.087E+OO 44.65 OK PB-212 74.82 10.28 3.488E+OO 1. 754E+OO 1. 754E+OO 63.15 OK 77 .11 17.10 3.688E+OO 1.602E+OO 1.602E+OO 30.19 OK 238.63 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12 .*49 OK 300.09 3.30 4.019E+OO 1.581E+OO 1.581E+OO 74.58 OK BI-214 609.32 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 OK 1120.29 14.92 l.392E+OO 1.099E+OO l.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1. 296E+OO 1. 297E+00 40.46 OK PB-214 74.82 5.80 3.423E+OO Line Not Found <<INT Reject 77 .11 9.70 3.688E+OO 2.824E+OO 2.825E+OO 30.19 OK 87.09 3.41 4.545E+00 Lin"e Not Found Absent 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 18.42 4.065E+OO l.204E+00 1.204E+OO 25.26 OK 351.93 35.60* 3.520E+OO 1.127E+OO 1.128E+OO 18.92 OK RN-222 609.32 45.49* 2.246E+OO l.044E+OO l.045E+00 19.61 OK 1120.29 14.92 l.392E+00 1.099E+OO 1.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO 1.297E+OO 40.46 OK RA-224 240.99 4.10* 4.743E+OO 9.949E-01 9.949E-01 113.31 OK RA-226 609.32 45.49* 2.246E+OO l.044E+00 1.045E+OO 19.61 OK 1120.29 14.92 l.392E+00 1.099E+OO 1.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO l.297E+00 40.46 OK AC-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 OK 794.95 4.25 l.822E+OO 9.610E-01 9.610E-01 134.35 OK 835.71 1. 61 1. 753E+OO 4.083E+OO 4.083E+00 66.33 OK 911.20 25.80* l.638E+OO 1.089E+OO l.089E+00 36.74 OK 968. 97 15.80 1.561E+OO 1.644E+OO 1.644E+00 30.57 OK RA-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 OK 794.95 4.25 l.822E+00 9.610E-01 9.610E-01 134.35 OK 835.71 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 OK 911.20 25.80* 1. 638E+OO l.089E+OO 1.089E+OO 36.74 OK 968.97 15.80 1. 561E+OO 1.644E+00 1.644E+OO 30.57 OK 'I'H-228 74.82 10.28 3.488E+OO 1. 754E+OO 1.754E+OO 63.15 OK 77 .11 17.10 3.688E+OO 1.602E+OO 1.602E+OO 30 .19 . OK 238.63 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12.49 OK 300.09 3.30 4.019E+OO l.581E+00 1. 581E+OO 74.58 OK TH-230 609.32 45.49* 2.246E+OO 1.044E+OO 1.044E+OO 19.61 OK 1120.29 14. 9.2 l.392E+OO 1.099E+OO 1.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO 1.296E+OO 40.46 OK TH-232 105.21 1.10 .5. 586E+OO Line Not Found Absent Page 3934 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 338.32 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 OK 835.71 1. 61 1.753E+OO 4;083E+OO 4.083E+OO 66.33 OK 911.20 25.80* 1.638E+OO 1.089E+OO 1. 089E+OO 36.74 OK 968.97 15.80 1.561E+OO 1.644E+OO l.644E+OO 30.57 OK U-234 609.32 45.49* 2.246E+OO 1.044E+OO 1.044E+OO 19.61 OK 1120.29 14-. 92 l.392E+OO 1:099E+OO l.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 l.296E+OO l.296E+OO 40.46 OK U-235 89. 96 3.47 4.745E+OO 2.057E+OO 2.057E+OO 130.83 OK 93.35 5.60 4.974E+OO 1.206E+OO l.206E+OO 86.31 OK 143.76 10. 96* 6.095E+OO Line Not Found Absent 163.33 5.08 5.924E+OO Line Not Found Absent 185. 72 57.20 5.599E+OO 2.286E-01 2.286E-01 50.50 OK 205.31 5.01 5.302E+OO Line Not Found Absent AM-243 43.53 5.90 1.701E-01 Line Not Found Absent 74.66 67.20* 3.488E+OO 2.684E-01 2.684E-01 63.15 OK ANH-511 511. 00 100.00* 2.589E+OO l.623E-01 1.623E-01 52.51 OK Flag: "*" = Keyline Page 3935 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:59:29.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l *
Acquisition date 3-0CT-2016 06:56:59 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
Sample date 30-NOV-2015 13:50:00 Analyst initials: MXRl *
Sample ID G405235044 Sample Quantity l.2884E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date* 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 9 6-sigrria) K-40 1.532E+Ol 1.671E+OO MN-54 l.302E-01 8.467E-02 AS-73 3.186E+Ol 2.799E+Ol SN-113 3.886E-01 4.821E-01 BA-137M 2.939E-01 1. OOlE-01 CS-137 3.105E..:01 l.058E-01 TL-208 3.194E-01 9.377E-02 PB-212 l.161E+OO 1.422E-01 BI-214 1.045E+OO 2.008E-01 PB-214 1.128E+OO 2.091E-01 RN-222 1.045E+OO 2.008E-01 RA-224 9.949E-01 1.105E+OO RA-226 1.045E+OO 2.008E-01 AC-228 1.089E+OO 3. 921E-01 RA-228 1.089E+OO 3. 921E-01 TH-228 1.161E+OO l.422E-01 TH-230 1.044E+OO 2.008E-01 TH-232 1.089E+OO 3. 921E-01 U-234 1.044E+OO 2.007E-01 U-235 5.108E-02 1. 911E-01 AM-243 2.684E-01 1.661E-01 ANH-511 l.623E-01 8.350E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 C0-56 Page 3936 of 5809 Key-Line Activity (pCi/GRAM 2.506E+OO -8.921E-03 O.OOOE+OO 6.046E-03 4.123E-02 O.OOOE+OO O.OOOE+OO 5.512E-01 K.L. Cnt Uncert ( 1. 96-sigma) 1. 547E+Ol 5.188E-02 9.800E+40 2.175E-02 4.229E-01 2.167E+04 6.341E+02 5. 713E-Ol MDA (pCi/GRAM 4. 511E-01 1. 251E-01 3.319E+Ol 5.433E-01 7.404E-02 7.822E-02 7.671E-02 l.OOlE-01 1.519E-01 l.500E-01 1. 519E-01 l.072E+00 1.519E-01 2.638E-01 2.638E-01 1.00lE-01 1.518E-01 .2.638E-01 1.518E-01 3.779E-01 l.194E-01 5.915E-02 MDA (pCi/GRAM 3. OOlE+Ol l.OlOE-01 O.OOOE+OO 5.847E-02 8.253E-01 O.OOOE+OO 0.000E+OO 1.223E+00 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN MN-56 O.OOOE+OO l.040E+41 O.OOOE+OO SHORT HLIF C0-57 3.406E-02 5.823E-02 1. 086E-01 NOT IDENT. C0-58 -l.143E-01 7.650E-01 l.399E+OO NOT IDENT. FE-59 -4.330E+OO 7.303E+00 .l.328E+Ol NOT IDENT: C0-60 -l.343E-02 4.507E-02 8.589E-02 FAIL ABUN ZN-65 4.067E-02 l.891E-01 3.581E-01 NOT IDENT. GE-68 -5.810E-01 2. 7 54E.+00 5.325E+OO NOT IDENT. AS-74 O.OOOE+OO 9.203E+03
O.OOOE+OO SHORT HLIF SE-75 2. 311E-02 2.574E-01 4.937E-01 NOT IDENT. BR-77 O.OOOE+OO 2.549E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.952E+02 O.OOOE+OO SHORT HLIF RB-83 l.167E-01 7.457E-01 l.459E+OO NOT IDENT. KR-85 6.281E+OO 9.799E+OO 1. 784E+Ol NOT IDENT. SR-85 7.154E-01 l.124E+OO 2.045E+OO NOT IDENT. RB-86 0.000E+OO 4.291E+04 O.OOOE+OO SHORT HLIF Y-88 -4.482E-03 1. 911E-01 4.407E-01 NOT IDENT. Y-91 -3.384E+02 7.146E+02 1. 301E+03 NOT IDENT. NB-94 l.416E-02 4.069E-02 7.803E-02 NOT IDENT. NB-95 -l.161E+OO l.098E+OO l.683E+OO NOT IDENT. NB-95M -1. 28 8E+OO 3.004E+OO 4.916E+OO NOT IDENT. ZR-95 -2 .196E-01 1. 750E+OO 3.245E+OO NOT IDENT. NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1. 025E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.442E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 2 62E-02 4.516E-02 7.724E-02 NOT IDENT. RH-102 -2.012E-02 6. 996E-02 l.264E-01 NOT IbENT. RU-103 2.299E+00 7.164E+OO l.426E+Ol FAIL ABUN RH-106 -4.744E-01 5.920E-01 9.785E-01 NOT IDENT. RU-106 -:-4.744E-01 5.920E-01 9.785E-01 NOT IDENT. AG-108M 2.176E-02 3.465E-02 6.963E-02 NOT IDENT. CD-109 2.428E+OO l.849E+OO 3.319E+OO NOT IDENT. AG-llOM 3.685E-02 l.118E-01 2.257E-01 NOT IDENT. CD-115 O.OOOE+OO 4.189E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.595E+05 O.OOOE+OO SHORT HLIF TE-123M 5.386E-02 l.461E-01 2.907E-01 NOT IDENT. SB-124 -9.120E-01 2.422E+OO 4.624E+00 NOT IDENT. SB-125 8.443E-02 l.266E-01 2.561E-01 NOT IDENT. TE-125M 5.334E+02 3.889E+o2 7.665E+02 NOT IDENT. I-126 O.OOOE+OO l.684E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.052E+06 O.OOOE+OO SHORT HLIF SN-126 l.573E-01 l.174E-01 2 .112E-01 NOT IDENT. SB-127 O.OOOE+OO l .116E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.133E+l0 0.000E+OO SHORT HLIF I-132 O.OOOE+OO l.453E+41 0. OOOE+OO' SHORT HLIF TE-132 O.OOOE+OO 2.439E+27 O.OOOE+OO SHORT HLIF BA-133 l.622E-02 4.874E-02 8.748E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.337E-02 8.343E-02 l.326E-01 FAIL ABUN CS-135 l.792E-02 1. 576E-01 2.761E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 4.740E+05 O.OOOE+OO SHORT HLIF CE-139 9.947E-03 l.365E-01 2.636E-01 NOT IDENT. BA-140 O.OOOE+OO 2.122E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 7.184E+05 O.OOOE+OO SHORT. HLIF CE-141 * -6.399E+oo* 3.227E+Ol 6.163E+Ol NOT IDENT. CE-143 O.OOOE+OO l.187E+41 O.OOOE+OO SHORT HLIF CE-144 9.855E-02 4.739E-01 8.445E-01 NOT IDENT. PM-144 3.148E-02 6.516E-02 l.308E-01 NOT IDENT. PR-144 2.710E+00 5.678E+OO l.139E+Ol NOT IDENT. PM-146 3.352E-03 5.285E-02 l.005E-01 NOT IDENT. ND-147 O.OOOE+OO 6.956E+07 O.OOOE+OO SHORT HLIF PM-147 -l.808E+02 l.058E+03 l.838E+03 NOT IDENT. PM-149 0.000E+OO l.233E+41 O.OOOE+OO SHORT HLIF EU-150 6.617E-03 3.070E-02 5.401E-02 FAIL ABUN EU-152 -5.155E-02 l.185E-01 1. 897E-01 NOT IDENT. GD-153 -l.069E-01 2.415E-01 4.129E-01 NOT IDENT. EU-154 2.369E-03 1. 204E-01 2.444E-01 NOT IDENT. EU-155 l.676E-01 l.345E-01 2.648E-01 NOT IDENT. TB-160 5. 871E-01 l.933E+OO 3.981E+OO FAIL ABUN H0-166M -4.417E-02 6.777E-02 l .138E-01 NOT IDENT. TM-171 7.814E-01 4.477E+Ol 7.632E+Ol NOT IDENT. HF-172 3.331E-01 2.772E-01 5.414E-01 FAIL ABUN LU-172 -3.785E-03 7'.576E-02 l.534E-01 FAIL ABUN LU-176 4.00lE-03 2.484E-02 4.856E-02 FAIL ABUN HF-181 3.763E+OO 5.799E+OO L 183E+Ol NOT IDENT. TA-182 -6.339E-01 l.090E+OO l.9SOE+OO FAIL ABUN RE-183 -8.362E-01 6.026E+OO 9. 996E+OO NOT IDENT. Page 3937 of 5809 RE-184 -2.181E+Ol
4.265E+Ol 7.224E+Ol NOT IDENT. W-188* -1. 2 66E+02 1.539E+02 2.354E+02 NOT IDENT. IR-192 -9.195E-02 5.634E-01 1.057E+OO FAIL ABUN HG-203 6 .113E-01 3.203E+OO 6.174E+OO NOT IDENT. BI-207 -4.214E-02 4.513E-02 7.618E-02 FAIL ABUN PB-210 l.356E+00 1. 040E+Ol 1.925E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.759E-01 8.395E-01 FAIL ABUN PB-211 -l.771E-01 7.765E-01 1.433E+OO NOT IDENT. BI-212 1.169E+OO 7.675E-01 1.618E+OO NOT IDENT. RN-219 1.888E-02 4.558E-01 8.647E-01 FAIL ABUN RA-223 -3.368E-01 7.014E-01 1.268E+OO FAIL ABUN AC-227 -3.623E-02 2.456E-01 4.646E-01 FAIL ABUN TH-227 -3.623E-02 2.456E-01 4.646E-01 FAIL ABUN TH-229 3.743E-02 5.301E-01 1.021E+OO FAIL ABUN PA-231 5.779E-01 4.931E-01 9.741E-01 NOT IDENT. TH-231 -3.368E-01 7.014E-01 1.268E+OO FAIL ABUN PA-233 4.165E-02 6.750E-02 1.359E-01 FAIL ABUN PA-234 -l.260E-01 2.940E-01 5.549E-01 FAIL ABUN PA-234M l.419E+OO 4.281E+OO 9.168E+OO NOT IDENT. TH-234 -2.028E+OO 2.086E+OO 3.544E+OO FAIL ABUN NP-237 4.165E-02 6.750E-02 l.359E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -2.028E+OO 2.086E+00 3.544E+OO FAIL ABUN NP-239 2.873E-02 3.333E-01 5.902E-01 NOT IDENT. PU-239 3.179E+02 4.286E+02 7.909E+02 NOT IDENT. AM-241 -2.473E-02 2.382E-01 4.294E-01 NOT IDENT. CM-243 -1.356E-01 1.305E-01 2.098E-01 NOT IDENT. BK-247 '2.219E-03 8.321E-02 1. 591E-01 NOT IDENT. CM-247 2.447E-02 3.973E-02 8. 037E-02
NOT IDENT. CF-249 -2.829E-02 4.991E-02 7.748E-02 NOT IDENT. CF-251 -2. 551E-03 l.168E-01 2.259E-01 NOT* IDENT. Page 3938 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:59:27.56 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 314 10.66* 1.119E+OO 1.532E+Ol 1.532E+Ol 11.13 MN-54 834.85 20 99.98* 1. 753E+OO 6.575E-02 1.302E-01 66.33 AS-73 53.44 44 10.30* 1.124E+OO 2.236E+OO 3.186E+Ol 89.65 SN-113 391.69 22 64.94* 3.225E+OO 6.089E-02 3.886E-01 126.61 BA-137M 661.66 94 89.90* 2.104E+OO 2.882E-01 2.939E-01 34.77 CS-137 661.66 94 85.10* 2.104E+OO 3.045E-01 3.105E-01 34.77 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 108 85.00* 2.326E+00 3.194E-01 3.194E-01 29. 96 860.56 40 12.50 1.714E+OO 1.087E+OO 1.087E+OO 44.65 BI-211 72. 87 ------1. 23 3.214E+OO ------Line Not Found ------351.06 242 12.92* 3.520E+OO 3.106E+OO 3.106E+OO 18.92 PB-212 74.82 150 10.28 3.488E+OO 2.434E+OO 2.434E+OO 44.97 77 .11 173 17.10 3.688E+OO 1.602E+OO 1.602E+OO 30.19 238.63 416 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12.49 300.09 36 3.30 4.019E+OO 1. 581E+OO 1. 581E+OO 74.58 BI-214 609 .*32 183 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 1120.29 39 14.92 1.392E+OO 1.099E+OO l.099E+OO 58.70 1764.49 32 15.30 9.460E-01 1.296E+OO 1.297E+OO 40.46 PB-214 74.82 150 5.80 3.488E+OO 4.314E+OO 4.315E+OO 44.97 77 .11 173 9.70 3.688E+OO 2.824E+OO 2.825E+OO 30.19 87.09 ------3.41 4.545E+OO ------Line Not Found ------242.00 104 7.25 4.743E+OO 1. 766E+00 1. 767E+OO 31. 72 295.22 155 18.42 4.065E+OO 1.204E+OO l.204E+OO 25. 26 351. 93 242 35.60* 3.520E+OO l.127E+OO 1.128E+OO 18.92 RN-222 609.32 183 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 1120.29 39 14.92 l.392E+00 1.099E+OO 1.099E+OO 58.70 1764.49 32 15.30 9.460E-01 l.296E+OO 1.297E+OO 40.46 RA-224 240.99 104 4.10* 4.743E+OO 3.124E+OO 3.124E+OO 31. 72 RA-226 609.32 183 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 1120.29 39 14.92 l.392E+00 1.099E+OO 1.099E+OO 58.70 1764.49 32 15.30 9.460E-01 1.296E+OO 1.297E+OO 40.46 AC-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 66 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 794.95 13 4.25 1.822E+OO 9.610E-01 9.610E-01 134.35 835. 71 20 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 911.20 79 25.80* 1.638E+00 1. 089E+OO 1.089E+OO 36.74 968. 97 70 15.80 1.561E+OO 1.644E+OO 1.644E+OO 30.57 RA-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 66 11. 27 3.634E+00 9.413E-01 9.413E-01 74.12 794.95 13 4.25 1.822E+OO 9.610E-01 9.610E-01 134.35 835.71 20 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 911.20 79 25.80* 1.638E+00 1. 089E+OO 1.089E+OO 36.74 968. 97 70 15.80
1. 561E+OO 1.644E+00 1.644E+OO 30.57 TH-228 74.82 150 10.28 3.488E+OO 2.434E+OO 2.434E+OO 44.97 77 .11 173 17.10 3.688E+OO 1.602E+OO 1.602E+00 30.19 238.63 416 43.60* 4.787E+oo l .161E+OO 1.161E+OO 12.49 300.09 36 3.30 4.019E+OO 1.581E+OO 1.581E+OO 74.58 Page 3939 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-230 609.32 183 45.49* 2.246E+OO 1.044E+OO 1.044E+OO 19.61 1120.29 39 14.92 1. 392E+OO 1.099E+OO l.099E+00 58.70 1764.49 32 15.30 9.460E-01 l.296E+OO 1.296E+OO 40.46 TH-232 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 66 11.27 3.634E+OO 9.413E-01 9.413E-01 74.12 835.71 20 1. 61 1.753E+OO 4.083E+OO 4.083E+OO 66.33 911. 20 79 25.80* 1.638E+OO 1. 089E+OO 1.089E+OO 36.74 968. 97 70 15.80 1.561E+OO l.644E+00 1.644E+OO 30.57 U-234 609.32 183 45.49* 2.246E+OO l.044E+OO l.044E+OO 19.61 1120.29 39 . 14. 92 l.392E+OO l.099E+OO 1.099E+OO 58.70 1764.49 32 15.30 9.460E-01 1. 296E+OO 1.296E+00 40.46 U-235. 89.96 58 3.47 4.745E+OO 2.057E+00 2.057E+OO 130.83 93.35 58 5.60 4.974E+OO l.206E+OO 1.206E+OO 86.31 143.76 ------10. 96* 6.095E+OO ------Line Not Found ------163.33 ------5.08 5.924E+OO ------Line Not Found ------185.72 126 57.20 5.599E+OO 2.286E-01 2.2B6E-01 50.50 205.31 ------5.01 5.302E+OO ------Line Not Found ------AM-243 43.53 ------5.90 l.701E-01 ------Line Not Found ------74.66 150 67.20* 3.488E+OO 3. 723E-01 3. 723E-01 44.97 ANH-511 511. 00 72 100.00* 2.589E+OO 1.623E-01 1.623E-01 52.51 Flag: "*" Key line Page 3940 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Total number of lines in spectrum 40 Number of unidentified lines 10 Number of lines tentatively identified by NID 30 Nuclide Type : Nuclide K-40 MN-54 AS-73 SN-113 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM_.:.243 ANH-511 Hlif e l.25E+09Y 312.05D 80.30D 115. 09D 30.08Y 30.08Y l.41E+10Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600. OOY 1. 41E+10Y 1600.00Y l.41E+l0Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 1;41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y l.00E+09Y Decay 1. 00 1. 98 14.2 6.38 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.532E+Ol 6.575E-02 2.236E+OO 6.089E-02 2.882E-01 3.045E-01 3.194E-01 3.106E+OO 1.161E+OO 1.044E+OO 1.127E+OO 1.044E+OO 3.124E+OO 1.044E+OO 1.089E+OO l.089E+00 1.161E+OO 1.044E+OO 1. 089E+00 l.044E+OO 2.286E-01 3. 723E-01 1.623E-01 3.753E+Ql 3.753E+Ol Decay Corr pCi/GRAM 1.532E+Ol l.302E-01 3.186E+Ol 3.886E-01 2.939E-01 3.105E-01 3.194E-01 3.106E+OO 1.161E+OO 1.045E+OO 1.128E+OO 1.045E+OO 3.124E+OO 1.045E+OO 1.089E+OO 1.089E+OO 1.161E+00 1.044E+OO 1.089E+OO 1.044E+OO 2.286E-01 3. 723E-01 l.623E-01 6.756E+Ol 6.756E+Ol 75:00% Decay Corr 2-Sigma Error 0 .171E+Ol 0.864E-01 2.856E+Ol 4.919E-01 1.022E-01 l.079E-01 0.957E-01 0.588E+OO 0.145E+OO 0.205E+OO 0.213E+OO 0.205E+OO 0. 991E+OO 0.205E+OO 0.400E+OO 0.400E+OO 0.145E+OO 0.205E+OO 0.400E+00 0.205E+OO l.155E-01 1.675E-01 0.852E-01 "M" Manually accepted 2-;-Sigma %Error 11.13 66.33 89.65 126.61 34.77 34.77 29. 96 18.92 12.49 19.61 18.92 19.61 31.72 19.61 36.74 36.74 12.49 19.61 36.74 19.61 50.50 44.97 52.51 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3941of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235044 Acquisition date : 3-0CT-2016 06:56:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff .Flags 0 210.19 57 131 2.38 421. 60 415 11 1.46E-02 86.7 5.22E+OO T 0 271.41 26 72 1. 42 544.04 538 9 6.81E-03 **** 4.35E+OO T 0 466.45 21 60 5.18 934.13 925 15 5.61E-03 **** 2.79E+OO 0 729 .12 26 48 0.74 1459.49 1451 17 7.21E-03 **** 1. 95E+OO 0 774.90 9 31 4.60 1551. 05 1544 14 2.57E-03 **** 1. 86E+OO 0 841.13 21 5 1. 58 1683.51 1678 11 5.97E-03 60.4 1.74E+OO 0 993.29 19 6 1. 51 1987.85 1981 14 5.53E-03 71. 3 1.53E+OO 0 1028.32 10 5 2. 60 . 2057.90 2051 10 2. 72E-03 **** 1. 49E+OO T 0 1038.30 8 8 0.66 2077.88 2073 8 2.22E-03 **** l.48E+OO T 0 1157.37 15 5 2.46 2316.02 2312 9 4.38E-03 76.2 1.36E+OO 0 1171.94 12 6 1. 87 2345.15 2341 8 3.40E-03 89.6 l.34E+OO T 0 1322.39 7 8 3.09 2646.06 2639 11 1.97E-03 **** 1.22E+OO 0 1377.89 21 7 1. 35 2757.07 2749 14 6.llE-03 66.5 1.18E+OO 5 1492.06 6 1 1. 39 2985.42 2984 11 l.83E-03 54.6 1.lOE+OO 5 1494.77 9 2 1. 92 2990.84 2984 11 2.68E-03 93.3 1. lOE+OO Flags: "T" = Tentatively associated Page 3942 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:59:41.13 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l *
Acquisition date 3-0CT-2016 06:56:59 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
Sample date 30-NOV-2015 13:50:00 Nuclide Library : SOLID *
Sample ID G405235044 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.2884E+02 GRAM *
Wet wt corr 1.00000 Wet Weight
0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff.. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are vaiid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 AS-73 SN-113 BA-137M CS-137 *TL-208 PB-212 BI-214 PB-214 RN-222 RA-224
RA-226 AC-228 RA-228 TH-228 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 1.595E-01 5.356E-02 1.542E+Ol 2.472E-01 3.273E-02 3.458E-02 3.433E-02 4.617E-02 6.814E-02 6. 8 61E-02 6.814E-02 4.948E-01 6.814E-02 l.132E-01 1.132E-01 4.617E-02 6.812E-02 1.132E-01 6.812E,-02 1. 768E-01 5.614E-02 2.649E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 C0-56 MN-56 Page 3943 of 5809 Le (pCi/GRAM 1.346E+Ol 4.261E-02 O.OOOE+OO 2.071E-02 3.521E-01 O.OOOEtOO O.OOOE+OO 5.390E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-i53 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3944 of 5809 5.083E-02 6.092E-01 5.444E+00 3.566E-02 l.523E-01 2.287E+00 O.OOOE+OO 2.285E-01 O.OOOE+OO O.OOOE+OO 6.466E-01 8.165E+OO 9.362E-01 0.000E+OO l.562E-01
5. 618E+02 3.505E-02 7.227E-01 2.270E+OO l.407E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.627E-02 5.558E-02 6.369E+OO 4.248E-01 4.248E-01 3.183E-02 l.584E+OO 9. 756E-02 0.000E+OO O.OOOE+OO l.357E-01 1. 731E+OO 1.170E-01 3.616E+02 O.OOOE+OO O.OOOE+OO l;008E-01 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.982E-02 O.OOOE+OO 5.953E-02 1.266E-01 O.OOOE+OO O.OOOE+OO l.237E-01 O.OOOE+OO O.OOOE+OO 2.886E+Ol O.OOOE+OO 3. 969E-01 5.828E-02 5.074E+OO 4.548E-02 O.OOOE+OO 8.597E+02 O.OOOE+OO 2.469E-02 8.606E-02 1.933E-01 l.030E-01 1.692E+OO 4.951E-02 3. 540E+Ol. 2.545E-01 6.462E-02 2.210E-02 5.354E+OO 8.296E-01 4.656E+OO 3.090E+Ol NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3945 of 5809 1.073E+02 4.829E-01 2.861E+OO 3.065E-02 9.049E+OO 4.023E-01 6.490E-01 7. 481E-01 3.939E-01 5.808E-01 2.136E-01 2.136E-01 4.771E-01 4.495E-01 5.808E-01 6.260E-02 2.360E-01 3.965E+OO 1.667E+OO 6.260E-02 O.OOOE+OO 1.667E+OO 2.778E-01 3.743E+02 2.009E-01 9.768E-02 7.347E-02 3.665E-02 3.499E-02 1.048E-01 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN .FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:59:46.46 *******************************************************************************

GEL Laboratories LLC * * . 2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l *
Acquisition date 3-0CT-2016 06:56:59 Sensitivity : 3.000 *
Detector ID GAM32 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time:
0 01:00:00.59 Half life ratio : ***** *
Sample date 30-NOV-2015 13:50:00 Nuclide Library : SOLID *
Sample ID G405235044 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.2884E+02 GRAM *
Quantity Err ( % ) : 1. 5523E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight. : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) (1.96-sigma) K-40 1.532E+Ol 1.853E+OO 1.853E+OO MN-54 l.302E-01 8.485E-02 8.485E-02 AS-73 3.186E+Ol 2.875E+Ol 2.875E+Ol SN-113 3.886E-01 4.824E-01 4.824E-01 BA-137M 2.939E-01 1.009E-01 1.009E-01 CS-137 3.105E-01 1.066E-01 1.066E-01 TL-208 3.194E-01 9.475E-02 9.475E-02 PB-212 1.161E+OO l.550E-01 .1.550E-01 BI-214 1.045E+OO 2.058E-01 2.058E-01 PB-214 1.128E+OO 2.143E-01 2.143E-01 RN-222 1.045E+OO 2.058E-01 2.058E-01 RA-224 9.949E-01 1.115E+OO 1.115E+OO RA-226 l.045E+00 2.058E-01 2.058E-01 AC-228 1.089E+OO 3.960E-01 3. 960E-01 RA-228 1.089E+OO 3. 960E-01 3. 960E-01 TH-228 .1.161E+OO l.550E-01 l.550E-01 TH-230 1.044E+OO 2.057E-01 2.057E-01 TH-232 1. 089E+00 3.960E-01 3.960E-01 U-234 1.044E+OO 2.057E-01 2.057E-01 U-235 5.108E-02 1. 911E-01 1. 911E-01 AM-243 2.684E-01 1.675E-01 l.675E-01 ANH-511 1.623E-01 8.376E-02 8.376E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide .(pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.506E+oo l.547E+Ol 1.551E+Ol NOT IDENT. NA-22 -8.921E-03 5.188E-02 5.203E-02 NOT IDENT. NA-24 1.000E+41 1.077E+41 O.OOOE+OO SHORT HLIF AL-26 6.046E-03 2.176E-02 2.193E-02 NOT IDENT. SC-46 4.123E-02 4.229E-01 4.234E-01 FAIL ABUN V-48 -1.319E+04 2.167E+04 2.248E+04 SHORT HLIF CR-51 -1. 960E+02 6.341E+02 6.403E+02 SHORT HLIF C0-56 5.512E-01 5.717E-01 6.234E-01 FAIL ABUN Page 3946 of 5809 MN-56 1.000E+41 1.040E+41 O.OOOE+OO SHORT HLIF C0-57 3.406E-02 5.825E-02 6.024E-02 NOT IDENT. C0-58 -1.143E-01 7.650E-01 7.667E-01 NOT IDENT. FE-59 -4.330E+OO 7.310E+OO 7.566E+OO NOT IDENT. C0-60 -1.343E-02 4.507E-02 4.547E-02 FAIL ABUN ZN-65 4.067E-02 1.891E-01 1.900E-01 NOT IDENT. GE-68 -5.810E-01 2.755E+OO 2.767E+OO NOT IDENT. AS-74 3.403E+03 9.208E+03 9.335E+03 SHORT HLIF SE-75 2. 311E-02 2.574E-01 2.576E-01 NOT IDENT. BR-77 2.083E+39 1.850E+40 O.OOOE+OO SHORT HLIF SR-82 9.421E+02 8. 963E+02 9.918E+02 SHORT HLIF RB-83 1.167E-01 7.459E-01 7.478E-01 NOT IDENT. KR-85 6.281E+OO 9.802E+OO 1.020E+Ol NOT IDENT. SR-85 7.154E-01 1.125E+OO 1.170E+OO NOT IDENT. RB-86 -1.259E+04 4.291E+04 4.328E+04 SHORT HLIF Y-88 -4.482E-03 1. 911E-01 1. 911E-01 NOT IDENT. Y-91 -3.384E+02 7.147E+02 7.308E+02 NOT IDENT. NB-94 1.416E-02 4.069E-02 4 .119E-02 NOT IDENT. NB-95 -1.161E+OO 1.099E+OO 1.218E+OO NOT IDENT. NB-95M -1.288E+OO 3.005E+OO 3. 061E+OO NOT IDENT. ZR-95 -2 .196E-01 1. 750E+00 1. 753E+OO NOT IDENT. NB-97 1.000E+41 2.404E+41 0.000E+OO SHORT HLIF ZR-97 1.000E+41 1. 026E+41 O.OOOE+OO SHORT HLIF M0-99 -1.0'64E+32 1.442E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 3.275E+41 O.OOOE+OO SHORT HLIF RH-101 -1.262E-02 4.522E-02 4.558E-02 NOT IDENT. RH-102 -2.012E-02 6.998E-02 7.056E-02 NOT IDENT. RU-103 2.299E+OO 7.164E+OO 7.239E+OO FAIL ABUN RH-106 -4.744E-01 6.301E-01 NOT IDENT. RU-106 -4.744E-01 5.927E-01 6.301E-01 NOT IDENT. AG-108M 2.176E-02 3.466E-02 3.602E-02 NOT IDENT. CD-109 2.428E+OO 1.859E+OO 2.157E+OO NOT IDENT. AG-llOM 3.685E-02 1.119E-01 1.131E-01 NOT IDENT. CD-115 2.749E+39 4.189E+'40 O.OOOE+OO SHORT HLIF SN-117M -4.939E+04 1.596E+05 1.612E+05 SHORT HLIF TE-123M 5.386E-02 1. 4 61E-01 1. 481E-01 NOT IDENT. SB-124 -9.120E-01 2.422E+OO 2.457E+OO NOT IDENT. SB-125 8.443E-02 1.267E-01 1.323E-01 NOT IDENT. TE-125M 5.334E+02 3.901E+02 4.583E+02 NOT IDENT. I-126 1.239E+05 1. 684E+06 1.685E+06 SHORT HLIF SB-126 -1.046E+06 2.062E+06 2 .115E+06 SHORT HLIF SN-126 1.573E-01 1.179E-01 1. 37 5E-01 NOT IDENT. SB-127 5.625E+22 1.369E+23 O.OOOE+OO SHORT HLIF I-131 1.357E+09 1.133E+10 1.135E+10 SHORT*HLIF I-132 -1.000E+41 1.902E+42 O.OOOE+OO SHORT HLIF TE-132 -7.437E+26 2.459E+27 O.OOOE+OO SHORT HLIF BA-133 1.622E-02 4.874E-02 4.929E-02 NOT IDENT. I-133 -1.000E+41 1.905E+42 O.OOOE+OO SHORT HLI.F CS-134 6.337E-02 8.347E-02 8.822E-02 FAIL ABUN CS-135 1. 792E-02 1.576E-01 1.578E-01 NOT IDENT. I-135 -l.000E+41 5. 696E+42 O.OOOE+OO SHORT HLIF CS-136 -3.287E+05 4.753E+05 4.979E+05 SHORT HLIF CE-139 9.947E-03 1.365E-01 1.366E-01 NOT IDENT. BA-140 1.717E+06 2.123E+06 2.259E+06 SHORT HLIF LA-140 -5.228E+05 7.189E+05 7.565E+05 SHORT HLIF CE-141 -6.399E+OO 3.227E+Ol 3.240E+Ol NOT IDENT. CE-143 1.000E+41 1.191E+41 O.OOOE+OO SHORT HLIF CE-144 9.855E-02 4.739E-01 4. 760E.:...01 NOT IDENT. PM-144 3.148E-02 6.519E-02 6.672E-02 NOT IDENT. PR_..:144 2.710E+OO 5.679E+OO 5.809E+00 NOT IDENT. PM-146 3.352E-03 5.285E-02 5.287E-02 NOT IDENT. ND-147 3.136E+06 6.956E+07 6.957E+07 SHORT HLIF PM-147 -1.808E+02 l.058E+03 1.062E+03 NOT IDENT. PM-149 -1.000E+41 l.253E+41 O.OOOE+OO SHORT HLIF EU-150 6.617E-03 3.070E-02 3.084E-02 FAIL ABUN EU-152 -5.155E-02 1.186E-01 1.208E-01 NOT IDENT. GD-153 -1. 069E-01 2.416E-01 2.463E-01 NOT IDENT. EU-154 2.369E-03 1.204E-01 l.204E-01 NOT IDENT. EU-155 1.676E-01 1.350E-01 1. 547E-01 NOT I DENT .. TB-160 5.871E-01 l.933E+OO l.951E+OO FAIL ABUN H0-166M -4.417E-02 6.781E-02 7.067E-02 NOT IDENT. TM-171 7.814E-01 4.477E+Ol 4.477E+Ol NOT IDENT. HF-172 3.331E-01 2.825E-01 3.199E-01 FAIL ABUN LU-172 -3.785E-03 7.576E-02 7.578E-02 FAIL ABUN LU-176 4.00lE-03 2.484E-02 2.491E-02 FAIL ABUN HF-181 3.763E+00 5.801E+OO 6.044E+OO NOT IDENT. TA-182 -6.339E-01 1.090E+OO 1.127E+OO FAIL ABUN RE-183 -8.362E-01 6.027E+OO 6.039E+OO NOT IDENT. Page 3947of5809 RE-184 4.298E+Ol 4.409E+Ol NOT IDENT. W-188. -l.266E+02 1.546E+02 'l. 648E+02 NOT IDENT. IR-192 -9.195E-02 5.635E-01 5.650E-01 FAIL ABUN HG-203 6 .113E-01 3.203E+OO 3.215E+OO NOT IDENT. BI-207 -4.214E-02 4.516E-02 4.900E-02 FAIL ABUN PB-210 1.356E+OO 1.040E+Ol 1.042E+Ol NOT IDENT. BI-211 3.106E+OO 5.925E-01 1.521E+OO FAIL ABUN PB-211 -1.771E-01 7.766E-01 7.807E-01 NOT IDENT. BI-212 l.169E+OO 7.697E-01 9.328E-01 NOT IDENT. RN-219 1.888E-02 4.558E-01 4.559E-01 FAIL ABUN RA-223 -3.368E-01 7.017E-01 7.179E-01 FAIL ABUN AC-227 -3.623E-02 2.457E-01 2.462E-01 FAIL ABUN TH-227 -3.623E-02 2*. 457E-01 2.462E-01 FAIL ABUN TH-229 3.743E-02 5.301E-01 5.304E-01 FAIL ABUN PA-231 5.779E-01 5.082E-01 5.711E-01 NOT IDENT. TH-231 -3.368E-01 7.017E-01 7.179E-01 FAIL ABUN PA-233 4.165E-02 6.753E-02 7.009E-02 FAIL ABUN PA-234 -l.260E-01 3.274E-01 3.323E-01 FAIL ABUN PA-234M 1.419E+OO 4.282E+OO 4.329E+OO NOT IDENT. TH-234 -2.028E+OO 2.134E+OO 2. 321E+OO FAIL ABUN NP-237 4.165E-02 6.753E-02 7.009E-02 FAIL ABUN NP-238 -1.000E+41 3.908E+41 O.OOOE+OO SHORT HLIF U-238 -2.028E+OO 2.134E+OO 2. 321E+OO FAIL ABUN NP-239 2.873E-02 3.333E-01 3.335E-01 NOT IDENT. PU-239 3.179E+02 4.289E+02 4.522E+02 NOT IDENT. AM-241 -2.473E-02 2.382E-01 2.384E-01 NOT IDENT. CM-243 -1.356E-01 1. 311E-01 1. 447E-01 NOT IDENT. BK-247 2. 21'9E-03 8.321E-02 8.321E-02 NOT IDENT. CM-247 2.447*E-02 3.995E-02 4.144E-02 NOT IDENT. CF-249 -2.829E-02 4. 996E-02 5.156E-02 NOT IDENT. CF-251 -2.551E-03 1.168E-01 1.168E-01 NOT IDENT. Page 3948 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 81.3617 87.09 99.8288 136.47 73.4470 45.60 69.3616 87.57 99.8871 140.51 0.0000 46.54 72.8394 88.03 99.9429 143.76 64.6930 49.72 0.0000 88.34 99.9801 144.24 67.'2428 51. 35 54.2351 88.47 99. 9961 145.44 77.4116 51. 87 52.7743 89. 96 81.0940 152.43 66.0339 52.39 54.3289 1093.63 81.1599 153.25 0.0000 52.97 55.8913 91.11 0.0000 323.87 62.7439 53.44 57.4459 92.59 94.1075 156.02 0.0000 54.07 56.7480 93.35 94.1909 158.56 0.0000 57.36 0.0000 94.56 62.3499 159.00 57.8910 57.53 63.9085 94.65 62.3562 162.33 70.0033 57.98 65.4759 94.67 62.3578 162.66 0.0000 59.27 74.3794 94.87 62.3721 163.33 81.1690 59.32 83.5401 97.43 84.2091 165.86 76.2001 59.54 73.2654 98.43 65.0351 176.31 69.0706 60. 96 74.5708 98.44 65.0359 176.60 0.0000 61.17 78.0372 99.53 81.9977 177.52 55.3086 62. 93 90.8994 100 .11 80.8445 181.07 0.0000 63.29 97.8550 102.03 66.5067 181.52 52. 0135 63.58 85.2279 103.18 93.2275 184.41 57.3418 64.28 72. 6333 103.37 87.1919 143.76 61.7473 66.73 80.9898 105.21 54.6045 193.51 66.4830 67.24 99.57.46 105.31 54.6106 197.03 81. 5652 125.81 90.3684 106.12 72.8778 198.01 63.1926 67.75 90.3773 106.47 76.5505 201.83 75.6892 69.67 101. 0780 109.28 58.4996 203.43 67.8465 70.83 96.1976 111. 00 84.2464 205.31 74.1135 72.81 71.5662 111. 76 0.0000 210.85 65.1035 72.87 85.5750 114. 06 78.3911 215.65 72.8753 74.66 81. 8822 116. 30 0.0000 222 .11 61.5935 74.82 81. 8999 116.74 83.5193 227.09 53.7390 74.97 81.9164 119.76 72.6868 227.38 54.6452 77 .11 82.1487 121.12 74.0195 228.16 0.0000 78.74 87.8116 121. 22 74.0268 228.18 60.9485 79.69 87.9193 121.78 59.2544 116.74 60.9485 80.12 84.8260 122.06 58.0361 235.69 58.0982 80.19 0.0000 122.92 85.2740 235. 96 58.1080 80.57 103.7360 123.07 85.2866 238.63 47.8307 81. 00 89.6389 265.00 66.7860 238.98 0.0000 81. 07 89.6470 125.81 53.2924 240.99 47.9035 81. 75 *80. 2800 127.23 86.8741 242.00 47.9342 83.79 104.1583 127.91 99.3503 244.70 *54.3591 84.00 102.6066 129.30 83.3165 252.40 0.0000 85.43 98.0449 131.20 83.4678 252.80 43.7090 86.55 99. 7628 133.02 81.1151 254.15 0.0000 86.79 99.7923 133.52 76.1588 256.23 46.5396 86.94 99.8109 136.00 72.5805 260.90 0.0000 Page 3949 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 50.4491 355.39 0.0000 584.27 24.3720 264.80 48.6189 356.01 28.9227 595.83 0.0000 265.00 48.6243 364.49 0.0000 427.87 15.9851 268.22 38.6068 366.42 0.0000 602.52 0.0000 269.46 40.0157 372.51 36.9316 604. 72 '30.4146 270.03 42.3295 375.05 29.1919 607.14 24.0317 271.23 42.3595 377.52 36.0455 609.32 25.6533 273.65 0.00.00 356.01 34 .1996 610.33 22.4543 276.40 43.4132 388.16 39.6538 614.28 19. 2722 277.37 54.5287 388.63 0.0000 618.01 17.1523 277.60 52.6872 391. 69 34.3250 62 0. 3 6 7.5101 278.00 49.9252 264.66 36.4369 621. 93 24.6892 279.20 49. 9603 401.81 34.4852 630.19 0.0000 279.54 59.2240 402.40 26.6100 631.29 21.5365 279.70 59.2292 404.85 34.5329 633.25 19.3953 280.46 61.1069 410.95 29.6814 634.78 0.0000 283.69 38.9597 413.71 29. 7180. 635.95 18.3344 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 48.2834 423. 72 0.0000 645.85 23.8038 285.90 0.0000 427.09 31. 8874 657.76 14.6640 287.50 31.6073 427.87 26.9143 657.90 0.0000 290.67 53.0850 433.94 27.9846 661. 66 19.5762 293.27 0.0000 439.40 29.0525 664.57 0.0000 351. 93 46.2189 453.88 29. 2313 666.33 0.0000 295. 96 46.2381 463.37 29.3469 666.50 0.0000 879.38 33.6768 468.07 27.3763 667. 71 0.0000 299.98 39.3203 473.00 0.0000 677.62 14.2108 300.09 39.3229 475.06 23.3870 685.70 0.0000 300 .13 39.3237 476.78 24.4209 695.00 0.0000 301.36 26.7019 477.60 23.4113 696.49 16.4941 302.85 40.7892 482.18 21.4149 696. 51 16.4941 256.23 30.9717 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.8980 306.78 31.9504 497.08 19.4905 697.49 24.1995 308.46 43.2663 505.52 30.8765 702.65 19. 8311 311.90 34.8667 507.63 0.0000 706.68 25.3706 316.51 40.6213 511. 00 24.7539 711. 68 23.2003 319.41 0.0000 514.00 27.8800 720.70 0.0000 320.08 0.0000 514.00 27.8800 721. 93 0.0000 321. 04 40.7193 520.40 18.6328 722.78 9. 9767 323.87 48.3676 520.69 0.0000 722.91 16.6284 325.23 48.4019 522.65 0.0000 723.31 16.6302 328.76 0.0000 527.90 0.0000 724.19 18.2980 333.37 22.8745 528.26 19.7267 727.33 21.0905 333.97 34.3220 529.59 21. 8135 733.00 16.6785 334.37 38.6205 529.87 0.0000 735.93 13.3545 338.28 34.3982 531. 02 0.0000 333.97 14.4742 338.32 34.3989 537.26 0.0000 739.50 0.0000 311. 90 34.4370 546.56 0.0000 747.24 20.0991 340.48 34.4370 552.55 25.1436 748.06 14.5197 340.55 0.0000 563.25 17.8792 752.31 10.0646 344.28 40.2543 569.33 15.8105 753.82 0.0000 345.93 36.4515 946.00 15. 8112 756.73 15.6765 351.06 41.8344 569.70 20.0290 756.80 15.6771 351. 93 38.4855 583.19 24.3626 884.68 15.7096 P1!-ge 3950 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 25.8226 1274.44 4.2940 1620.50 2*. 0240 766.42 26.9502 1001.03 8.0607 1621. 92 1. 0123 766.84 21. 337 9 1002;74 8.0640 1678.03 0.0000 772.60 0.0000 1004.73 11. 6535 1690.97 5 .1187 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0714 778.90 11. 8330 1028.54 0.0000 1063.66 5.1831 783.70 0.0000 1037.84 11.7440 1771.35 2.0736 785.37 9.0322 1038.76 0.0000 1791.20 0.0000 792.07 10.1807 631.29 10.8625 1808.65 1.0427 794.95 16.9818 1048.07 0.0000 1810.72 0.0000 795.86 16.9861 1049.04 10.8691 1836.06 2.0941 81Ci.06 17.0538 1050.41 9. 9667 810.29 17.0551 1063.66 9. 9969 344.28 17.0557 1077.00 0.0000 810.76 17.0569 1077.34 14.5859 815.77 0.0000 1085.87 13.7009 1048.07 0.0000 1093.63 10.0648 832.01 13.7256 1099.45 11. 9098 834.85 12.0193 1112. 07 12.8618 835.71 12.0223 1112.84 13.7833 836.80 0.0000 1115. 54 8.8266 846.75 0.0000 1120. 29 11. 9645 846.77 8.2685 i120.55 11. 9653 856.80 0.0000 1221.41 11. 9677 860.56 13.8320 1129. 67 7.3779 871.09 13.8706 1131. 51 0.0000 873.19 13*.8784 1147.95 0.0000 875.33 0.0000 1173.23 19.3629 879.38 8.1088 1177.95 17.7058 880.51 16.2222 1189.05 11. 2083 883.24 6.9575 1204.77 18.7427 884.68 10.4399 1221.41 16.9255 889.28 10.4528 1231. 02 19.7862 894.76 8.1413 1235.36 0.0000 898.04 13.9688 1238.28 18.8721 900.72 3.4945 1260.41 0.0000 903.28 17.4841 1271. 87 4.7501 911.20 12.2637 1274.44 9.5050 912.08 12.2667 1274.54 11. 4060 923.98 0.0000 1291.59 7.6299 926.50 7.9146 1298.22 0.0000 929 .11 14.9596 1312 .11 0.0000 937.49 15.8730 1332.49 10.5750 944.13 0.0000 1362.66 0.0000 946.00 15.0229 1365.19 5.8041 949.00 12.3812 1368.63 0.0000 667.71 0.0000 1384.29 4.4381 962.31 17.7454 1408.01 3.9004 964. 08 12.7824 1457.56 0.0000 966 .17 19.8939 1460.82 1.9691 911. 20 24.8845 1489.16 3.1666 968. 97 24.8845 1505.03 5.9539 983.53 0.0000 1584.12 8.0474 984.45 0.0000 1596.21 0.0000 Page 3951 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:00:16.02 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;l34 Background date : 2-0CT-2016 11: 02 :*13. Sample date 30-NOV-2015 14:15:00 Acquisition date : 3-0CT-2016 06:57:26. Sample ID G405235045 Sample quantity 1.30599E+02 GRAM Detector name : GAM39 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.96 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 2 2 0 0 1 1 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3952 of 5809 Energy 46.69* 63.24* 74.84* 77.22* 87.36 89.78 92.73* 98. 29 129.50 185.71* 188.58 238.76* 241.52 253.81 270.62* 295.68* 328.16 338.56* 352.21* 402.02 405.46 511. 00* 518.51 550.08 .583.56* 609.72* 626.25 634.04 653.39 661.71 731.13 801.05 911. 52* 949 .. 47 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 45 94 212 319 77 71 92 33 60 58 36 293 110 31 38 129 28 53 205 23 18 27 19 43 119 104 14 13 8 223 78 6 63 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 126 0.82 93.22 265 1.19 126.33 189 1.41 149.51 173 1.27 154.29 167 1.42 174.55 172 1.28 179.41 132 1.20 185.29 128 0.63 196.43 137 1.58 258.85 59 1.44 371.26 57 1.32 377.00 102 1.27 477.36 107 1.92 482.89 144 3.13 507.47 124 2.47 541.09 111 1.70 591.20 49 0.91 656.17 65 1.51 676.97 83 1.41 704.28 34 1.43 803.90 8 0.72 810.79 60 1.44 1021.86 35 4.84 1036.89 29 7.41 1100.04 44 1.97 1167.01 67 1. 67 1219. 33 30 0.54 1252.38 18 1.26 1267.96 27 0.93 1306.68 45 1. 27 1323. 32 48 11.48 1462.16 23 3.85 1602.02 31 1. 45 1822. 98 7 2.86*1898.90 90 121 143 143 171 171 171 193 253 365 365 473 473 496 538 585 652 671 696 798 808 1015 1031 1090 1158 1212 1246 1262 1299 1316 1446 1593 1815 1893 8 1.*25E-02 4 7. 8 12 2.62E-02 37.2 18 5.89E-02 13.3 2.59E+OO 18 8.87E-02 9.7 20 2.14E-02 28.8 2.92E+OO 20 l.97E-02 33.6 20 2.54E-02 26.3 8 9.03E-03 62.8 13 1. 65E-02 42. 5 19 l.62E-02 32.2 3.39E+OO 19 9.93E-03 43.3 15 8.14E-02 8.7 1.57E+OO 15 3.06E-02 26.5 19 8.58E-03 94.5 13 1.04E-02 63.2 13 3.59E-02 19.2 9 7.87E-03 48.4 11 l.47E-02 33.3 16 5.70E-02 12.4 11 6.37E-03 54.3 6 5.llE-03 33.2 15 7.63E-03 73.8 14 5.28E-03 69.9 23 1.19E-02 36.1 19 3.31E-02 16.9 15 2.90E-02 20.0 13 3.93E-03 83.3 8 3.63E-03 64.5 12 2.12E-03141.4 14 6.19E-02 9.3 40 2.16E-02 32.2 12 1. 80E-03161. 8 16 l.75E-02 24.4 10 3.49E-03 49.6 Peak Search Report (continued) Page : 2 Sample ID : G405235045 A.cquisi tion date 3-0CT-2016 06:57:26 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 1 965.08 24 21 2.03 1930.11 '1921 23 6.77E-03 37.6 8.95E-01 36 1 969.68* 25 13 2.03 1939.31 1921 23 6.86E-03 37.1 37 0 1120.38 26 11 1. 89 2240.76 2236 10 7.08E-03 30.6 38 0 1219.97 9 8 1. 03 2439.98 2435 8 2.58E-03 61. 8 39 0 1351.60 7 2 0.80 2703.30 2697 10 l.82E-03 59.6 40 0 1461. 00* 218 3 1. 69 2922.13 2916 15 6.05E-02 7.2 41 0 1764.89* 25 6 2.03 3530.06 3522 12 6. 96E-03 28.6 Flag: "*" = Peak area was modified by background subtraction Page 3953 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:00:17 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 14:15:00 G405235045 Acquisition date : Sample quantity Sample geometry : 3-0CT-2G16 06:57:26 130.60 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA39 0 01:00:00.00 1.50 keV No Linear 175. 00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3954 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 7.4.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:06.96 10.00 0.00 % Peak Energy \ 0.2%

Nuclide Line Activity Report

Page : 2 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.983E-Ol 1.246E+Ol 1.246E+Ol 14.40 OK CD-109 88.03 3.70* 6.753E+OO 9.131E-01 1.450E+OO 137 .17 OK SN-126 64.28 9.60 6.931E+OO 9.550E-01 9.550E-01 74.43 OK 86.94 8.90 6.753E+OO 3.796E-Ol 3.796E-01 137.17 OK 87.57 37.00* 6.753E+OO 9 .131E-02 9 :131E-02 137.17 OK BA-137M 661.66 89.90* 1. 758E+OO 8 .17"1E-01 8. 331E-01 18.55 OK CS-137 661. 66 85.10* 1. 758E+OO 8.632E-01 8.801E-01 18.55 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* 1.952E+OO 4.201E-01 4.201E-01 33.77 OK 860.56 12.50 1.416E+OO Line Not Found Absent PB-210 46.54 4.25* 6.835E+OO 1. 060E+OO 1.088E+OO 95.59 OK PB-212 74.82 10.28 6.812E+OO 1.330E.f-OO 1.330E+OO 44.93 OK 77 .11 17.10 6.799E+OO 1.830E+OO 1.830E+OO 19.49 OK 238.63 43.60* 4.209E+OO 9.906E-01 9.906E-01 17.39 OK 300.09 3.30 3.465E+OO Line Not Found Absent BI-214 609.32 45.49* 1. 882E+OO 7 .116E-01 7 .119E-01 40.00 OK 1120.29 14.92 l.136E+OO 8.399E-01 8.402E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK PB-214 74.82 5.80 6.812E+OO Line Not Found <<INT Reject 77 .11 9.70 6.799E+OO 3.226E+OO 3.227E+OO 19.49 OK 87.09 3.41 6.755E+OO Line Not Found <<INT Reject 242.00 7.25 4.163E+OO Line Not Found <<INT Reject 295.22 18.42 3.510E+OO 1.225E+OO l.226E+OO 38.30 OK 351. 93 35.60* 3.012E+OO 1.158E+OO L 159E+OO 24.76 OK RN-219 271. 23 10.80 3.788E+OO 5.644E-01 5.644E-01 126.49 OK 401.81 6.60* 2.683E+OO 7. 771E-01 7. 771E-01 108.62 OK RN-222 609.32 45.49* l.882E+OO 7 .116E-01 7 .119E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.402E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK RA-224 240.99 4.10* 4.170E+OO 1.830E+OO 1.830E+OO 124.19 OK RA-226 609.32 45.49* 1.882E+OO 7 .116E-01 7 .119E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 *8.402E-01 61. 26 OK 1764.49 15.30 7.483E-01 l.182E+OO 1.182E+OO 57.30 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835.71 1. 61 1.451E+OO Line Not Found Absent 911. 20 25.80* 1. 351E+OO 1. 024E+00 1.024E+OO 48.76 OK 968. 97 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 OK RA-228. 105.21 1.10 6.612E+00 Line Not Found Absent 338.32 11. 27 3.118E+OO 9.148E-01 9.148E-01 66.59 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835. 71 1. 61 1. 451E+oo Line Not Found Absent 911. 20 25.80* L 351E+OO 1.024E+OO 1.024E+OO 48.76 OK 968. 97 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 OK TH-228 74.82 10.28 6.812E+OO 1.330E+OO 1.330E+OO 44.93 OK 77 .11 17.10 6.799E+OO l.830E+00 1.830E+OO 19.49 OK 238.63 43.60* 4.209E+OO 9.906E-01 9.906E-01 17. 39 OK 300.09 3.30 3.465E+OO Line Not Found Absent Page 3955 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 1. 882E+OO 7.116E-01 7 .116E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.399E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK TH-232 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 OK 835.71 1. 61 1. 451E.+00 Line Not Found Absent 911.20 25.80* 1.351E+OO 1.024E+OO 1.024E+OO 48.76 OK 968. 97 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 OK TH-234 63.29 3.70* 6.931E+OO 2.478E+OO 2.478E+00 74.43 OK 92.59 4.23 6. 723E+OO 2.120E+OO 2.120E+00 52.64 OK U-234 609.32 45.49* l.882E+OO 7 .116E-01 7 .116E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.399E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK U-235 89. 96 3.47 6.741E+OO 2.003E+OO 2.003E+OO 67.29 OK 93.35 5.60 6. 723E+OO 1.602E+00 1.602E+OO 52.64 OK 143.76 10. 96* 5.959E+OO Line Not Found Absent 163.33 5.08 5.556E+OO -----. Line Not Found Absent 185.72 57. 20 . 5.108E+OO 1.256E-01 1.256E-01 64.32 OK 205.31 5.01 4.746E+OO Line Not Found Absent U-238 . 63.29 3.70* 6.931E+OO 2.478E+OO 2.478E+OO 74.43 OK 92.59 4.23 6.723E+OO 2.120E+OO 2.120E+OO 52.64 OK AM-243 43.53 5.90 6.236E+OO Line Not Found Absent 74.66 67.20* 6.812E+OO 2.035E-01 2.035E-01 44.93 OK CM-247 278.00 3.40 3.702E+OO Line Not Found Absent 287.50 2.00 3.596E+OO Line Not Found Absent '402.40 72. 00* 2.683E+OO 7.124E-02 7.124E-02 108.62 OK ANH-511 511. 00 100.00* 2.183E+OO 7.425E-02 7.425E-02 147.59 OK Flag: "*" = Keyline Page 3956 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:00:19.09 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l *
Acquisition date 3-0CT-2016 06:57:26 Sensitivity : 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.96 Half life ratio : ***** *
Sample date 30-NOV-2015 14:15:00 Analyst initials: MXRl *
Sample ID G405235045 Sample Quantity 1.3060E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4'
Combined Activity-MDA Report NOTE.: Not all "Identified Nuclides" are valid. Please refer to certificate of Analysis. Identified Nuclides . Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.246E+Ol 1.759E+OO CD-109 1.450E+oo 1.949E+OO SN-126 9.131E-02 1.227E-01 BA-137M 8.331E-01 l.515E-01 CS-137 8. 801E-01 1.600E-01 TL-208 4. 201E-01 l.390E-01 PB-210 1.088E+OO 1.019E+OO PB-212 9.906E-01 1.688E-01 BI-214 7 .119E-01 2.791E-01 PB-214 1.159E+OO 2. 811E-01 RN-219 7. 771E-01 8.272E-01 RN-222 7 .119E-01 2.791E-01 RA-224 1.830E+OO 2.228E+OO RA-226 7 .119E-01 2.791E-01 AC-228 1.024E+OO 4.895E-01 RA-228 1.024E+OO 4.895E-01 TH-228 9.906E-01 1.688E-01 TH-230 7.116E-01 2.790E-01 TH-232 1.024E+OO 4.895E-01 TH-234 2.478E+OO l.807E+OO U-234 7 .116E-01 2.790E-01 U-235 -1.990E-01 1. 996E-01 U-238 2.478E+OO 1.807E+OO AM-243 2.035E-01 8. 962E-02 CM-247 7:124E-02 7.583E-02 ANH-511 7.425E-02 1.074E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3957 of 5809 Key-Line Activity (pCi/GRAM 1. 751E+OO 4.445E-02 O.OOOE+OO -8.668E-03 K.L. Cnt Uncert ( 1. 96-sigma) 2.149E+Ol 5.918E-02 1.432E+41 1.699E-02 MDA (pCi/GRAM 9.655E-01 2. OllE+OO 1. 2 66E-01 8.879E-02 9.379E-02 8. 596E-02 1.013E+OO 1.370E-01 l.914E-01 1.463E-01 8.942E-01 l.914E-01 1.470E+OO 1.914E-01 3.751E-01 3.751E-01 1.370E-01 l.913E-01 3.751E-01 1.248E+OO l.913E-01 3.622E-01 1.248E+OO 6.731E-02 8.208E-02 6.394E-02 MDA (pCi/GRAM 4.017E+Ol 1.349E-01 O.OOOE+OO 2.134E-02 NOT *I DENT .. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -5.846E-02 5.860E-01 1.146E+00 FAIL ABUN V-48 0.000E+OO 3.139E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6. 613E+02 O.OOOE+OO SHORT HLIF MN-54 l.545E-02 8.954E-02 l.816E-01 NOT IDENT. C0-56 4.078E-01 6.426E-01 l.407E+OO NOT IDENT. MN-56 O.OOOE+OO l.576E+41 O.OOOE+OO SHORT HLIF C0-57 -3.654E-03 5.449E-02 9.604E-02 NOT IDENT. C0-58 -4.402E-01 7.885E-01 l.456E+OO NOT IDENT. FE-59 2.037E+OO 9.875E+OO 2.042E+Ol NOT IDENT. C0-60 3.264E-02 5.325E-02 l.195E-01 NOT IDENT. ZN-65 l.253E-01 2.324E-01 4.662E-01 NOT IDENT. GE-68 6.924E-01 2.970E+OO 6.224E+OO NOT IDENT. AS-73 -4.170E-Ol 3 .118E+OO 5.609E+OO NOT IDENT. AS-74 O.OOOE+OO 1. 086E+04 O.OOOE+OO SHORT HLIF SE-75 -2.095E-01 2.733E-01 4.849E-01 FAIL ABUN BR-77 O.OOOE+OO 3.012E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l.209E+03 O.OOOE+OO SHORT HLIF RB-83 -3.386E-01 1. 046E+OO l.656E+OO NOT IDENT. KR-85 l.421E+Ol 1. 096E+Ol l.978E+Ol NOT IDENT. SR-85 l.628E+OO l.257E+OO 2.269E+OO NOT IDENT. RB-86 O.OOOE+OO 4.581E+04 O.OOOE+OO SHORT HLIF Y-88 -l. l 76E-01 2.608E-01 4.803E-01 NOT IDENT. Y-91 6.397E+02 8.695E+02 l.859E+03 NOT IDENT. NB-94 -l.941E-02 4.900E-02 8.496E-02 NOT IDENT. NB-95 7.626E-02 1. 446E+OO 2.664E+00 NOT IDENT. NB-95M l.422E+00 3.906E+OO 6.866E+OO NOT IDENT. ZR-95 -2.056E-01 l.979E+OO 3.678E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT.HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.815E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -4.958E-03 4 .141E-02 6.638E-02 NOT IDENT. RH-102 7.185E-02 l. l 72E-01 l.808E-01 NOT IDENT. RU-103 2.587E+OO 9.471E+OO l.836E+Ol FAIL ABUN RH-106 l.318E-01 7.418E-01 1. 294E+00 NOT IDENT. RU-106 l.318E-01 7.418E-01 1. 294E+OO NOT IDENT. AG-108M -6.352E-03 3. 896E-02 7.200E-02 NOT IDENT. AG-llOM -5.919E-03 l.410E-01 2.799E-01 NOT IDENT. SN-113 6.530E-02 3.406E-01 6.542E-01 NOT IDENT. cn...:115 O.OOOE+OO 5.024E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1. 651E+05 O.OOOE+OO SHORT HLIF TE-123M 3.697E-02 l.543E-01 3.045E-01 NOT IDENT. SB-124 l.262E+OO 3.157E+OO 7.318E+OO NOT IDENT. SB-125 2.918E-02 1. 27 9E-01 2. 511E-01 NOT IDENT. TE-125M l.444E+02 3.487E+02 6.389E+02 NOT IDENT. I-126 O.OOOE+OO 2.273E+06 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 3.068E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.232E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.435E+l0 O.OOOE+OO SHORT HLIF I-132. O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.922E+27 O.OOOE+OO SHORT HLIF BA-133 1. 791E-03 5.375E-02 9.266E-02 NOT IDENT. I-=-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 *8.342E-02 9.081E-02 l.777E-01 FAIL ABUN CS-135 l.249E-02 2.037E-01 3.500E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 6.216E+05 O.OOOE+OO SHORT HLIF CE-139 -5.362E-02 1. 317E-01 2.472E-01 NOT IDENT. BA-140 O.OOOE+OO 3.037E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1. 052E+06 O.OOOE+OO SHORT HLIF CE-141 -2.619E+Ol 3.200E+Ol 5.883E+Ol NOT IDENT. CE-143 O.OOOE+OO l.346E+41 O.OOOE+OO SHORT HLIF CE-144 -l.957E-01 4.220E-01 7 .114E-01 NOT IDENT. PM-144 -2. 872E-03 8. 9_94E-02 l.642E-01 NOT IDENT. PR-144 3.310E-01 7.749E+OO l.431E+Ol NOT IDENT. PM-146 9.024E-03 6.539E-02 l.242E-01 FAIL ABUN ND-147 O.OOOE+OO 8.100E+o7 O.OOOE+OO SHORT HLIF PM-147 -9.931E+Ol 9.089E+02 l.598E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF EU-150 -1. 350E-02 4.044E-02 6.529E-02 FAIL ABUN EU-152 7. 796E-02 l.224E-01 2.469E-01 FAIL ABUN GD-153 2.676E-01 3.293E-01 3.699E-01 FAIL ABUN EU-154 l.120E-01 l.453E-01 3.316E-01 NOT IDENT. EU-155 l .119E-01 l.167E-01 2.243E-01 FAIL ABUN TB-160 3.131E-01 2.750E+OO 5.584E+OO FAIL ABUN H0-166M -5.493E-02 8.688E-02 l.449E-01 FAIL ABUN TM-171 -4.845E+OO 6.447E+OO l.105E+Ol NOT IDENT. HF-172 -9.526E-02 2.935E-01 4.588E-01 FAIL ABUN Page 3958 of 5809 LU-172 8.858E-02 l.092E-01 2.413E-01 FAIL ABUN LU-176 -1.185E-03 3.308E-02 6.085E-02 FAIL ABUN HF-181 -2.819E+OO 6.867E+00 1.225E+Ol NOT IDENT. TA-182 1.167E+OO 1.413E+OO 2.752E+OO FAIL ABUN RE-183 -2.629E-01 1.463E+OO 2.617E+OO NOT IDENT. RE-184 -1.577E+Ol 4.880E+Ol 9.253E+Ol NOT IDENT. W-188 -9.552E+Ol 2.001E+02 3.197E+02 FAIL ABUN IR-192 l.602E-01 6.201E-01 1.215E+OO FAIL ABUN HG-203 -6.154E-01 3.619E+OO 6.762E+OO NOT IDENT. BI-207 l.393E-02 6.840E-02 1.392E-01 FAIL ABUN BI-211 O.OOOE+OO 7.743E-01 1.056E+OO FAIL ABUN PB-211 1.095E+OO 7.122E-01 1. 517E+OO FAIL ABUN BI-212 6.161E-01 8.263E-01 1.649E+OO NOT IDENT. RA-223 1.374E-01 8.338E-01 1.453E+OO FAIL ABUN AC_.:_227 -1. 511E-01 3.262E-01 5.279E-01 NOT IDENT. TH-227 -1. 511E-01 3.262E-01 5.279E-01 NOT IDENT. TH-229 l.256E-01 6.026E-01 1.067E+OO FAIL ABUN PA-231 7.262E-01. 6.223E-01 1.248E+OO NOT IDENT. TH-231 1.374E-01 8.338E-01 1.453E+OO FAIL ABUN PA-233 -1.932E-02 7.146E-02 l.329E-01 NOT IDENT .. PA-234 -3.674E-01 4.776E-01 6.938E-01 FAIL ABUN PA-234M -2.144E+OO 6.396E+OO 1.208E+Ol NOT IDENT. NP-237 -l.932E-02 7.146E-02 1.329E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 -5.772E-02 2.933E-01 5.093E-01 FAIL ABUN PU-239 O.OOOE+OO 8.128E+02 7.298E+02 FAIL ABUN AM-241 3.412E-03 7.181E-02 1.204E-01 NOT IDENT. CM-243 -3.753E-02 1.064E-01 1."836E-01 FAIL ABUN BK-247 -5.036E-02 9. 351E-b2 1. 696E-01 NOT IDENT. CF-249 -7.312E-03 4.930E-02 9.183E-02 FAIL ABUN CF-251 -6.946E-03 1.387E-01 2.661E-01 NOT IDENT. Page 3959 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:00:16.70 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 208 10.66* 8.983E-01 1.246E+Ol 1.246E+Ol 14.40 CD-109 88.03 89 3.70* 6.753E+00 2.042E+OO 3.242E+OO 57.56 SN-126 64.28 111 9.60 6.931E+OO 9.550E-01 9.550E-01 74.43 86.94 89 8.90 6.753E+OO 8.490E-01 8.490E-01 57.56 87.57 89 37.00* 6.753E+OO 2.042E-01 2.042E-01 57.56 BA-137M 661.66 225 89.90* 1. 758E+OO 8.171E-01 8.331E-01 18.55 CS-137 661.66 225 85.10* 1. 758E+OO 8.632E-01 8.801E-01 18;55 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 121 85.00* 1.952E+OO 4.201E-01 4.201E-01 33.77 860.56 ------12.50 l.416E+00 ------Line Not Found ------PB-210 46.54 54 4.25* 6.835E+OO 1.060E+OO 1.088E+OO 95.59 BI-211 72. 87 ------1. 23 6.824E+OO ------Line Not Found ------351.06 216 12.92* 3.012E+OO 3 .191E+OO 3 .191E+OO 24.76 PB-212 74.82 246 10.28 6.812E+00 2.022E+OO 2.022E+00 26.51 77 .11 370 17.10 6.799E+OO 1.830E+OO l.830E+00 19.49 238.63 316 43.60* 4.209E+OO 9:906E-01 9.906E-01 17. 39 300.09 ------3.30 3.465E+OO ------Line Not Found ------BI-214 609.32 106 45.49* 1.882E+00 7 .116E-01 7 .119E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.402E-01 61. 26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 PB-214 74.82 246 5.80 6.812E+OO 3.583E+OO 3.584E+OO 26.51 77.11 370 9.70 6.799E+OO 3.226E+OO 3.227E+OO 19.49 87.09 89 3.41 6.753E+OO 2.216E+OO 2.217E+00 57.56 242.00 119 7.25 4.170E+OO 2.260E+OO 2.261E+OO 52.95 295.22 138 18.42 3.510E+OO 1.225E+OO 1. 22 6E+OO 38.30 351. 93 216 35.60* 3.012E+OO 1.158E+OO 1.159E+OO 24.76 RN-219 271.23 40 10.80 3.788E+00 5.644E-01 5.644E-01 126.49 401.81 24 6.60* 2.683E+00 7. 771E-01 7 .. 771E-01 108.62 RN-222 609.32 106 45.49* 1.882E+OO 7.116E-01 7 .119E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.402E-01 61.26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 RA-224 240.99 119 4.10* 4.170E+OO 3.997E+OO 3.997E+OO 52.95 RA-226 609.32 106 45.49* 1.882E+00 7 .116E-01 7 .119E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.402E-01 61.26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 56 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 62 25.80* 1. 351E+OO 1. 024E+OO 1.024E+OO 48.76 968. 97 24 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 RA-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 56 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 794.95 ------4.25 1.512E+OO ------Line Not Found ------835. 71 ------1. 61 1. 451E+OO ------Line Not Found ------911.20 62 25.80* 1. 351E+OO 1.024E+OO 1.024E+OO 48.76 968. 97 24 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 Page 3960 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Nuclide Type: Nuclide Uncorrected Decay Corr 2-Sigma Energy Area %Abn %Eff pCi/GRAM pCi,/GRAM %Error TH-228 74.82 246 10.28 6.812E+OO 2.022E+OO 2.022E+OO 26.51 77 .11 370 17.10 6.7.99E+OO 1.830E+OO 1.830E+OO 19.49 238.63 316 43.60* 4.209E+OO 9.906E-01 9.906E-01 17.39 300.09 ------3.30 3.465E+OO ------Line Not Found ------TH-230 609.32 106 45.49* 1.882E+OO 7 .116E-01 7.116E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.399E-01 61. 26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 56 11. 27 3.118E+OO 9.148E-01 9.148E-01 66.59 835.71 ------1. 61 l.451E+OO ------Line Not Found ------911.20 62 25.80* l.351E+OO 1.024E+OO 1.024E+OO 48.76 968. 97 24 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 TH-234 63.29 111 3.70* 6.931E+OO 2.478E+OO 2.478E+OO 74.43 92.59 105 4.23 6.723E+OO 2.120E+OO 2.120E+OO 52. 64 U-234 609.32 106 45.49* 1.882E+OO 7 .116E-01 7 .116E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.399E-01 61.26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 U-235 89.96 81 3.47 6.741E+OO 2.003E+OO .2.003E+OO 67.29 93.35 105 5*_ 60 6. 723E+OO 1.602E+OO 1.602E+OO 52.64 143.76 ------10. 96* 5.959E+OO * ------Line Not Found ------163.33 ------5.08 5.556E+OO ------Line Not Found ------185. 72 64 57.20 5.108E+OO 1.256E-01 l.256E-01 64.32 205.31 ------5.01 4.746E+OO ------Line Not Found ------U-238 63.29 111 3.70* 6. 931E+OO 2.478E+OO 2.478E+OO 74.43 92.59 105 4.23 6. 723E+00 2.120E+OO 2.120E+OO 52.64 AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 246 67.20* 6.812E+OO 3.093E-01 3.093E-01 26. 51 CM-247 278.00 ------3.40 3.702E+OO ------Line Not Found ------287.50 ------2.00 3. 596E+OO ------Line Not Found ------402.40 24 72.00* 2.683E+OO 7.124E-02 7.124E-02 108.62 ANH-511 511. 00 28 100.00* 2.183E+OO 7.425E-02 7.425E-02 147.59 Flag: "*" Key line Page 3961 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235045 Acquisition date 3-0CT-20l6 06:57:26 Total number of lines in spectrum 41 Number of unidentified lines 7 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Hlif e l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.D8Y l.41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600. OOY 7.04E+08Y 1600. OOY l.41E+10Y 1600. OOY 1.41E+10Y 1.41E+10Y l.41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.56E+07Y 1.00E+09Y Decay 1. 00 1. 59 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.246E+Ol 2.042E+OO 2.042E-01 8.171E-01 8.632E-01 4. 201E-01 1. 060E+OO 3.191E+OO 9.906E-01 7 .116E-01 l.158E+OO 7. 771E-01 7 .116E-01 3.997E+OO 7 .116E-01 l.024Ei-00 1. 024E+OO 9.906E-01 7 .116E-01 1.024E+OO 2.478E+OO 7.116E-01 l.256E-01 2.478E+OO 3.093E-01 7.124E-02 7.425E-02 4 .114E+Ol 4 .114E+Ol Decay Corr pCi/GRAM 1.246E+Ol 3.242E+OO 2.042E-01 8.331E-01 8.801E-01 4.201E-01 1.088E+00 3 .191E+OO 9.906E-01 7 .119E-01 1.159E+OO 7. 771E-01 7 .119E-01 3.997E+OO 7 .119E-01 1.024E+OO 1.024E+OO 9.906E-01 7 .116E-01 l.024E+OO 2.478E+OO 7 .116E-01 1.256E-01 2.478E+OO 3.093E-01 7.124E-02 7.425E-02 4.240E+Ol 4.240E+Ol 82.93% Decay Corr 2-Sigma Error 0.179E+Ol 1. 866E+OO 1.175E-01 1. 546E-01 l.633E-01 1.419E-01 l.040E+00 0.790E+OO 1.723E-01 2.848E-01 0.287E+OO 8. 441E-01 2.848E-01 2 .116E+OO 2.848E-01 0.499E+OO 0.499E+00 1.-723E-01 2.847E-01 0.499E+OO 1.844E+OO 2.847E-01 0.808E-01 1. 844E+OO 0.820E-01 7.738E-02 10.96E-02 "M" Manually accepted 2-Sigma %Error 14.40 57.56 57.56 18.55 18.55 33.77 95.59 24.76 17.39 40.00 24.76 108.62 40.00 52.95 40.00 48.76 48.76 17.39 40.00 48.76 74.43 40.00 64.32 74.43 26.-51 108.62 147.59 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3962 of 5809

Flags K Unidentified Energy Lines Page : 4 Sample ID :. G405235045 Acquisition date : 3-0CT-2016 06:57:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 98.29 37 147 0.63 196. 43 193 8 9.03E-03 **** 6.68E+OO T 0 129.50 67 153 1. 58 258.85 253 13 1.65E-02 85.0 6.24E+OO T 1 188.58 39 62 1. 32 377.00 365 19 9.93E-03 86.7 5.05E+OO 0 253.81 33 155 3.13 507.47 496 19 8.58E-03 **** 4.00E+OO T 0 328.16 30 51 0.91 656.17 652 9 7.87E-03 96. 9 *3.20E+00 T 0 405.46 19 8 0. 72 810.79 808 6 5. llE-03 66.4 2.66E+OO T 0 518.51 19 36 4.84 1036.89 1031 14 5.28E-03 **** 2.16E+00 0 550.08 44 30 7.41 1100. 04 1090 23 1.19E-02 72.2 2.05E+OO 0 62 6. 25 14 30 0.54 1252.38 1246 13 3.93E-03 **** 1.84E+OO 0 634.04 13 18 1. 26 1267. 96 1262 8 3.63E-03 **** 1. 82E+OO T 0 653.39 8 28 0.93 1306. 68 1299 12 2.12E-03 **** 1. 78E+00 0 731.13 78 48 11. 48 1462.16 1446 40 2.16E-02 64.5 1.62E+OO 0 801.05 6 22 3.85 1602.02 1593 12 1.80E-03 **** 1.50E+OO T 0 949.47 12 7 2.86 1898.90 1893 10 3.49E-03 99.2 1. 31E+OO T 1 965. 08 24 21 2.03 1930 .11 1921 23 6.77E-03 75.2 1.29E+OO T 0 1219.97 9 7 1. 03 2439.98 2435 8 2.58E-03 **** 1.06E+OO T 0 1351.60 6 2 0.80 2703.30 2697 10 l.82E-03 **** 9.64E-01 Flags: "T" = Tentatively associated Page 3963 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:00:31.38 *******************************************************************************
GEL Laboratories LLC *
2940 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l *
Acquisition date 3-0CT-2016 06:57:26 Sensitivity 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.96 Half life ratio : ***** *
Sample date 30-NOV-2015 14:15:00 Nuclide Library : SOLID *
Sample ID G405235045 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.3060E+02 GRAM * *Wet wt corr 1.000QO Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-JUL-2016 13: 04: 01 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M. CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 4.016E-01 9.544E-01 6.008E-02 3.932E-02 4.154E-02 3.823E-02 4.774E-01 6.418E-02 8.649E-02 6.573E-02 4.024E-01 8.649E-02 6.886E-01 8.649E-02 1.651E-01 1. 651E-01 6.418E-02 8.646E-02 l.651E-01 5.923E:.._01 8.646E-02 1.688E-01 5.923E-01 3.189E-02 3.694E-02 2.835E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3964 of 5809 Le (pCi/GRAM 1.828E+Ol 5.784E-02 O.OOOE+OO O.OOOE+OO 5.007E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3965 of 5809 0.000E+OO O.OOOE+OO 8.0lOE-02 6 .172E-01 O.OOOE+OO 4.478E-02 6.206E-01 8.768E+OO 5.086E-02 2.007E-01 2.659E+OO 2.646E+OO O.OOOE+OO 2.217E-01 0.000E+OO O.OOOE+OO 7.310E-01 9.005E+OO 1.033E+OO O.OOOE+OO l.597E-01 8.218E+02 3.778E-02 1.191E+OO 3.222E+OO 1.582E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.094E-02 8.143E-02 8.293E+OO 5.710E-01 5. 710E-01 3.251E-02 l.216E-01 2.988E-01 0 .*OOOE+OO O.OOOE+OO l.421E-01 2.937E+OO 1.126E-01 3.008E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.180E-02 O.OOOE+OO 8.080E-02 1. 620E-01 O.OOOE+OO O.OOOE+OO 1.150E-01 O.OOOE+OO O.OOOE+OO 2.743E+Ol O.OOOE+OO 3.308E-01 7.367E-02 6.419E-i-OO 5.651E-02 O.OOOE+OO . 7. 439E+02 O.OOOE+OO 2.998E-02 l .133E-01 1. 749E-01 1.424E-01 l.056E-01 2.434E+OO 6.366E-02 5.196E+OO 2.140E-01 l.061E-01 SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. . NOT IDENT. SHORT HLIF FAIL ABUN . SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF "NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 . HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-.203 BI-207 BI-211 PB-211 BI-212 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233* PA-234 PA--:234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 . BK-24 7 CF-249 CF-251 Page 3966 of 5809 2.793E-02 5.468E+OO 1.200E+OO 1.238E+OO 4. OOlE+Ol l.480E+02 5.550E-01 3.123E+OO 6.061E-02 5.0BOE-01 6.BOOE-01 7.520E-01 6.649E-01 2.428E-01 2.428E-01 4. 967E-01 5.BllE-01 6.649E-01 6.028E-02 2. 971E-01 5.297E+OO 6.028E-02 O.OOOE+OO 2.389E-01 3.445E+02 5.694E-02 8.584E-02 7.793E-02 4.157E-02 1.243E-01 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:00:36.69 *******************************************************************************

GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l *
Acquisition date 3-0CT-2016 06:57:26 Sensitivity : 3.000 *
Detector ID GAM39 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.96 Half life ratio : ***** *
Sample date 30-NOV-2015 14:15:00 Nuclide Library : SOLID *
Sample ID G405235045 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.3060E+02 GRAM *
Quantity Err(%) : 1.5314E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 27-'JUL-2016 13: 04: 01 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.246E+Ol l.876E+OO CD-109 1.450E+OO 1. 965E+OO SN-126 9 .131E-02 1.237E-01 BA-137M 8. 331E-01 l.557E-01 CS-137 8.801E-01 l.644E-01 TL-208 4.201E-01 l.402E-01 PB-210 1.088E+OO 1.023E+OO PB-212 9.906E-01 1. 768E-01 BI-214 7 .119E-01 2.807E-01 PB-214 1.159E+OO 2.852E-01 RN-219 7. 771E-01 8.329E-01 RN-222 7 .119E-01 2.807E-01 RA-224 1.830E+OO 2.234E+00 RA-226 7 .119E-01 2.807E-01 AC-228 l.024E+OO 4.923E-01 RA-228 1.024E+OO 4.923E-01 TH-228 9.906E-01 1. 768E-01 TH-230 7 .116E-01 2.806E-01 TH-232 l.024E+OO 4.923E-01 TH-234 2.478E+OO 1.889E+OO U-234 7 .116E-01 2.806E-01 U-235 -1.990E-01 l.999E-01 U-238 2.478E+OO 1.889E+OO AM-243 2.035E-01 9.148E-02 CM-247 7.124E-02 7.677E-02 ANH-511 7.425E-02 l.074E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3967 of 5809 Key-Line Activity (pCi/GRAM 1. 751E+OO 4.445E-02 -1.000E+41 --8.668E-03 K.L Act error ( 1. 96-sigma) 2.149E+Ol 5.920E-02 1.500E+41 1.700E-02 TPU ( 1. 96-sigma) 1.876E+OO 1. 965E+OO l.237E-01 l.557E-01 l.644E-01 l.402E-01 1.023E+OO 1. 768E-01 2.807E-01 2.852E-01 8.329E-01 2.807E-01 2.234E+OO 2.807E-01 4.923E-01 4.923E-01 1. 768E-01 2.806E-01 4.923E-01 1. 889E+OO 2.806E-01 1.999E-01 1. 889E+OO 9.148E-02 7.677E-02 l.074E-01 TPU (1.96-sigma) 2.150E+Ol 6.250E-02 O.OOOE+OO 1. 7:44E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -5.846E-02 5.860E-01 5.866E-01 FAIL ABUN V-48 2.548E+03 3.139E+04 3.141E+04 SHORT HLIF CR-51 -2.672E+02 6.614E+02 6.723E+02 SHORT HLIF MN-54 l.545E-02 8.955E-02 8.982E-02 NOT IDENT. C0-56 4.078E-01 6.429E-01 6*. 686E-01 NOT IDENT. MN-56 1.000E+41 l.576E+41 O.OOOE+OO SHORT HLIF C0-57 -3.654E-03 5.449E-02 5.451E-02 NOT IDENT. C0-58 -4.402E-01 7.887E-01 8.133E-01 NOT IDENT. FE-59 2.037E+OO 9.876E+OO 9.919E+OO NOT IDENT. C0-60 3.264E-02 5.327E-02 5.526E-02 NOT IDENT. ZN-65 l.253E-01 2.325E-01 2.392E-01 NOT IDENT. GE-68 6.924E-01 2.970E+OO 2.987E+OO NOT IDENT. AS-73 *-4.170E-01 3 .119E+OO 3.125E+OO NOT IDENT. AS-74 -4.862E+03 1.086E+04 l.108E+04 SHORT HLIF SE-75 -2.095E-01 2.735E-01 2.894E-01 FAIL ABUN BR-77 1. 768E+39 l.570E+40 0.000E+OO SHORT HLIF SR-82 -2.467E+02 l.210E+03 l.215E+03 SHORT HLIF RB-83 -3.386E-01 1.048E+OO 1.059E+OO NOT IDENT. KR-85 1.421E+.01 1.097E+Ol 1.. 270E+Ol NOT IDENT. SR-85 1.628E+OO 1. 259E+OO 1.457E+OO NOT IDENT. RB-86 5.743E+03 4.581E+04 4.589E+04 SHORT HLIF Y-88 -l.176E-01 2.609E-01 2.662E-01 NOT IDENT. Y-91 6.397E+02 8.698E+02 9.164E+02 NOT I NB-94 -1.941E-02 4.901E-02 4.979E-02 NOT IDENT. NB-95 7.626E-02 1. 446E+OO 1. 446E+OO NOT IDENT. NB-95M 1.422E+OO 3.907E+OO 3.959E+OO NOT IDENT. ZR-95 -2.056E-01 l.979E+OO 1.982E+OO NOT IDENT. NB-97 -l.OOOE+41 3.808E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 2.-985E+42 O.OOOE+OO SHORT HLIF M0-99 -8.621E+32 1.816E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.893E+41 O.OOOE+OO SHORT HLIF RH-101 -4.958E-03 4.142E-02 4.148E-02 NOT IDENT. RH-102 7.185E-02 l.174E-01 l.218E-01 NOT IDENT. RU-103 2.587E+00 9.472E+OO 9.544E+OO FAIL ABUN RH-106 l.318E-01 7.419E-01 7.443E-01 NOT IDENT. RU-106 l.318E-01 7.419E-01 7.443E-01 NOT IDENT. AG-108M -6.352E-03 3.896E-02 3.907E-02 NOT IDENT. AG-llOM -5.919E-03 1.410E-01 l.411E-01 NOT IDENT. SN-113 6.530E-02 3.406E-01 3.419E-01 NOT IDENT. CD-115 -4.432E+40 5.090E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 6.192E+04 l.653E+05 1. 67 6E+05 SHORT HLIF TE-123M 3 .*697E-02 1.543E-01 l.552E-01 NOT IDENT. SB-124 l.262E+OO 3.157E+00 3.208E+OO NOT IDENT. SB-125 2.918E-02 l.279E-01 l.286E-01 NOT IDENT. TE-125M 1.444E+02 3.488E+02 3.548E+02 NOT IDENT. I-126 -2.537E+04 2.273E+06 2.273E+06 SHORT HLIF SB-126 -6.603E+05 3.070E+06 3.085E+06 SHORT HLIF SB-127 -6.841E+22 l.565E+23 O.OOOE+OO SHORT HLIF I-131 7.795E+09 1.435E+10 l.478E+10 SHORT HLIF I-132 1.000E+41 2.206E+42 O.OOOE+OO SHORT HLIF TE-132 -2.439E+27 3.094E+27 O.OOOE+OO SHORT HLIF BA-133 1.791E-03 5.375E-02 5.375E-02 NOT IDENT. I-133 1. OOOE+41 6.330E+41 O.OOOE+OO SHORT HLIF CS-134 8.342E-02 9.088E-02 9.835E-02 FAIL ABUN CS-135 l.249E-02 2.037E-01 2.038E-01 NOT IDENT. I-135 -l.OOOE+41 8.207E+41 O.OOOE+OO SHORT HLIF CS-136 -2.253E+05 6. 221E+05 6.304E+05 SHORT HLIF CE-139 -5.362E-02 1. 321E-01 l.343E-01 NOT IDENT. BA-140 -2.679E+06 3.039E+06 3.270E+06 SHORT HLIF LA-140 -1.973E+05 l.052E+06 l.056E+06 SHORT HLIF CE-141 -2.619E+01 3.202E+Ol* 3.413E+Ol NOT IDENT. CE-143 1.000E+41 l.350E+41 O.OOOE+OO SHORT HLIF CE-144 -1.957E-01 4.221E-01 4.313E-01 NOT IDENT. PM-144 -2. 872E-03 8.994E-02 8.995E-02 NOT IDENT. PR-144 3.310E-01 7.749E+OO 7.750E+OO NOT IDENT. PM-146 9.024E-03 6.539E-02 6.552E-02 FAIL ABUN ND-147 6.312E+07 8.107E+07 8.592E+07 SHORT HLIF PM-147 -9.931E+Ol 9.089E+02 9.100E+02 NOT IDENT. PM-149 -1. OOOE+41 2.673E+41 O.OOOE+OO SHORT HLIF EU-150 -l.350E-02 4.044E-02 4.090E-02 FAIL ABUN EU-152 7.796E-02 l.225E-01 l.274E-01 FAIL ABUN GD-153 2.676E-01 3.297E-01 3.511E-01 FAIL ABUN

EU-154 l.120E-01 l.454E-01 1.539E-01 NOT IDENT. EU-155 l .119E-01 l. l 70E-01 l.274E-01 FAIL ABUN TB-160 3.131E-01 2.751E+OO 2.754E+OO FAIL ABUN H0-166M -5.493E-02 8.694E-02 9.039E-02 FAIL ABUN TM-171 -4.845E+OO 6.461E+OO 6.820E+OO NOT IDENT. HF-172 -9.526E-02 2.939E-01 2.970E-01 FAIL ABUN Page 3968 of 5809 LU-172 8.858E-02 l.096E-01 l.166E-01 FAIL ABUN LU-176 *-1.185E-03 3.308E-02 3.308E-02 FAIL ABUN HF-181 -2.819E+OO 6.868E+OO 6.985E+OO NOT IDENT. TA-182 1.167E+OO 1.414E+OO 1.509E+OO FAIL ABUN RE-183 -2.629E-Ol
1. 464E+OO l.468E+OO NOT IDENT. RE-184 -1.577E+Ol 4.895E+Ol 4.947E+Ol NOT IDENT. W-188 -9.552E+Ol 2.004E+02 2.049E+02 FAIL ABUN IR-192 1.602E-01 6.201E-01 6.243E-01 FAIL ABUN HG-203 -6.154E-01 3.619E+OO 3.630E+OO NOT IDENT. BI-207 1.393E-02 6.840E-02 6.869E-02 FAIL ABUN BI-211 3.191E+OO 7.874E-01 1.640E+OO FAIL ABUN PB-211 1.095E+OO 7.144E-01 8.682E-01 FAIL ABUN BI-212 6.161E-01 8.269E-01 8. 723E-01 NOT IDENT. RA-223 1.374E-01 8.338E-01 8. 361E-01 FAIL ABUN AC-227 -1. 511E-01 3.268E-01 3*. 338E-01 NOT IDENT. TH-227 -1. 511E-01 3.268E-01 3.338E-01 NOT IDENT. TH-229 1.256E-01 6.026E-01 6.053E-01 FAIL ABUN PA-231 7.262E-01 6.414E-01 7 .201E-01 NOT IDENT. TH-231 l.374E-01 8.338E-01 8.361E-01 FAIL ABUN PA-233 -l.932E-02 7.147E-02 7.200E-02 NOT IDENT. PA-234 -3.674E-01 6.362E-01 6.574E-01 FAIL ABUN PA-234M -2.144E+OO 6.397E+OO 6.469E+OO NOT IDENT. NP-237 -1.932E-02 7.147E-02 7.200E-02 FAIL ABUN NP-238 1.000E+41 5.675E+41 O.OOOE+OO SHORT HLIF NP-239 -5.772E-02 2.933E-01 2.945E-01 FAIL ABUN PU-239 9.757E+02 8.140E+02 9.252E+02 FAIL ABUN AM-241 3.412E-03 7.181E-02 7.183E-02 NOT IDENT. CM-243 -3.753E-02 l.064E-01 1. 078E-01 FAIL ABUN BK-247 -5.036E-02 9.406E-02 9.676E-02 NOT IDENT. CF-249 -7.312E-03 4.931E-02 4.942E-02 FAIL ABUN CF-251 -6.946E-03 l.387E-01 1.387E-01 NOT IDENT. Page 3969 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 77.6683 87.09 114. 7072 136.47 61. 8774 45.60 86.8333 87.57 114.7827 140.51 0.0000 46.54 90.6860 88.03 114.8560 143.76 73.2930 49. 72 0.0000 88.34 114.9048 144.24 77.5426 51. 35 101.5943 88.47 114.9248 145.44 70.0414 51. 87 97.2249 89. 96 115.1586 152.43 80.7216 52.39 91.7273 1093.63 115.2645 153.25 0.0000 52.97 90.7076 91.11 0.0000 323.87 68.0924 53.44 85.1831 92.59 115.5664 156.02 0.0000 54.07 78.5497 93.35 115.6826 158.56 0.0000 57.36 0.0000 94.56 95.5609 159.00 60.7087 57.53 100.5002 94.65 78.8468 162.33 63.4718 57.98 106.2309 94.67 78.8493 162.66 0.0000 59.27 111. 7584 94.87 78.8700 163.33 61.8135 59.32 111. 7682 97.43 95.9186 165.86 68.8428 59.54 101.2344 98.43 88.8387 176.31 59.0690 60. 96 87.8517 98.44 8'8. 8399 176.60 0.0000 61.17 104.5508 99.53 73.7355 177.52 67.8279 62.93 116.2628 100 .11 96.2476 181.07 0.0000 63.29 116. 3336 102.03 57.8884 181.52 64.1375 63.58 116. 3903 103.18 78.5032 184.41 58. 6114 64.28 116.5266 103.37 78.5220 143.76 58.6768 66.73 133.0559 105.21 62. 9604 193.51 56.8587 67.24 134. 6972 105. 31 . 62. 9684 197.03 61. 0025 125.81 119.4756 106.12 83.6368 198.01 60.1668 67.75 121.0210 106.47 83.6726 201.83 67.4540 69.67 129.0770 109.28 75.4405 203.43 78.2058 70.83 132.3917 111. 00 86.5686 205.31 69.4227 72. 81 107.7079 111. 76 0.0000 210.85 62.5759 72.87 107.7179 114.06 75.8683 215.65 48.4536 74.66 108.0137 116. 30 0.0000 222 .11 60.4161 74.82 108.0400 116.74 82.2421 227.09 65.1680 74.97 108.0641 119.76 64.0498 227.38 68.8031 77 .11 108.4125 121.12 62.9146 228.16 0.0000 78.74 108.6750 121.22 62.9216 228.18 76.0912 79.69 88.9332 121. 78 65.4304 116.74 76.0912 80.12 88.9889 122.06 65.4510 235.69 68.3151 80.19 0.0000 122.92 69.2220 235. 96 65.5950 80.57 93.7341 123.07 64.2883 238.63 73.0249 81. 00 104.7352 265.00 61.8576 238.98 0.0000 81. 07 104.7454 125.81 72.7501 240.99 73.1486 81. 75 125.1921 127.23 66.2390 242.00 73.2015 83.79 98.8762 127. 91 . 67 .1169 244.70' 39.8799 84.00 98.9053 129 .. 30 67. 217 6 252.40 0.0000 85.43 117.9817 131. 20 67.3550 252.80 43.3343 86.55 114. 6214 133.02 61. 6539 254.15 0.0000 86.79 114.6591 133. 52 70.0222 256.23 54.0654 86.94 114. 6835 136.00 61.8473 260.90 0.0000 Page 3970 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52.0522 355.39 0.0000 584.27 21. 8 066 264.8,0 49.2691 356.01 27.9990 595.83 0.0000 265.00 52.9945 364.49 0.0000 427.87 34.0122 268.22 50.3130 366.42 0.0000 602.52 0.0000 269.46 47.5573 372. 51 32 .. 7100 604. 72 28.0214 270.03 53.1719 375.05 32.7543 60'7 .14 34.6454 271.23 56.9492 377.52 35.7781 60*9. 32 29.7202 273.65 0.0000 356.01 34.9003 610.33 29.7323 276.40 63.2318 388.16 32.9792 614.28 21.5051 277.37 54.8354 388.63 0.0000 618.01 23.1909 277.60 49.2188 391.69 34.0408 620.36 14.9216 278.00 48.3876 264.66 27.1560 621. 93 16.5894 279.20 52.5547 401.81 27.1719 630.19 0.0000 279.54 54.4434 402.40 27.1802 631.29 16.6461 279.70 54.4493 404. 85 ' 22.6781 633.25 9.9950 280.46 46.0232 410.95 31.3406 634.78 0.0000 283.69 41.4129 413. 71 38.4701 635.95 20.0090 284.31 0.0000 414.70 0.0000 636.99 0.0000' 285.41 50.8810 423.72 0.0000 645.85 16.7340 285.90 0.0000 427.09 34.6461 657.76 23.5276 287.50 53.7796 427.87 22.4266 657.90 0.0000 290.67 63.8141 433.94 31.6931 661. 66 20.1943 293.27 0.0000 439.40 27.6757 664.57 0.0000 351. 93 51.1974 453.88 31.9915 666.33 0.0000 295. 96 51.2216 463.37 25.9125 666.50 0.0000 879.38 54.1553 468.07 24.9292 667.71 0.0000 299.98 49.9226 473.00 0.0000 677.62 18.0508 300.09 49.9258 475.06 29.1758 685.70 0.0000 300 .13 49.9269 476.78 20.8557 695.00 0.0000 301.36 37.6882 477.60 31.2952 696.49 26.1165 302.85 58.1084 482.18 29.2686 696.51 24.9810 '256.23 47.6776 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 26.1239 306.78 41.0596 497.08 25.2515 697.49 26.1249 308.46 33.4548 505.52 26.9277 702.65 27.3086 311. 90 36.3981 507.63 0.0000 706.68 12.5334 316.51 33.6171 511. 00 20.6398 711. 68 26.2503 319.41 0.0000 514.00 12. 7178 720.70 0.0000 320.08 0.0000 514.00 12.7178 721. 93 0.0000 321.04 34.6707 520.40 23.9099 722.78 10.3099 323.87 36.1755 520.69 0.0000 722. 91 10.3103 325.23 34.7556 522.65 0.0000 723. 31 15.4677 328.76 0.0000 527.90 0.0000 724.19 22.3485 333.37 53.8356 528.26 24.5217 727.33 19.5034 333.97 49.4872 529.59 21.3354 733.00 19.5393 334.37 39.3077 529.87 0.0000 735.93 19.5587 338.28 38.9095 531. 02 0.0000 333.97 19.5684 338.32 38.9103 537.26 0.0000 739.50 0.0000 311. 90 39.4445 546.56 0.0000 747.24 19.6300 340.48 39.4445 552.55 12. 9214 748.06 13.8604 340.55 0.0000 563.25 24.8727 752.31 15.0360 344.28 31.2331 569.33 14.0923 753.82 0.0000 345.93 41.0319 946.00 14.0929 756.73 13.8989 351.06 26.4529 569.70 15.1781 756.80 13.8994 351. 93 26.4655 583.19 21. 7977 884.68 27.8613 Page 3971 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.2316 1274.44 10.2363 1620.50 4.2529 766.42 .16.2655 1001.03 16.7706 1621. 92 6.3809 766.84 17.4298 1002.74 8.3892 1678.03 0.0000 772. 60 0.0000 1004.73 16.7871 1690.97 3.2292 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 6.9754 778.90 12.8302 1028.54 0.0000 1063.66 5.4550 783.70 0.0000 1037.84 15.0479 1771. 35 3.2736 785.37 12.2718 1038.76 0.0000 1791.20 0.0000 792.07 20.2022 631.29 10.3682 1808.65 1.0979 794.95 15.4730 1048.07 0.0000 1810.72 0.0000 795.86 19.6984 1049.04 14.1476 1836.06 3.3083 810.06 14.1313 1050.41 12.2653 810.29 14.1323 1063.66 13.2523 344.28 14.1333 1077.00 0.0000 810.76 16.7850 1077.34 9.4977 815.77 0.0000 1085.87 12.3732 1048.07 0.0000 1093.63 9.5355 832.01 15 .1142 1099.45 10.5038 834.85 16.9068 1112 .'07 13.4087 835.71 13.3507 1112. 84 9.5795 836.80 0.0000 1115. 54 7.6685 846.75 0.0000 1120.29 14.3948 846.77 10.7153 1120.55 14.3958 856.80 0.0000 1221.41 18.4301 860.56 12.5516 1129. 67 11.5415 871.09 15.2880 1131.51 0.0000 873.19 15.2973 1147:95 0.0000 875.33 0.0000 1173.23 8.7446 879.38 14.4229 1177. 95 17.5078 880.51 16.2307 1189.05 17. 5.518 883.24 14.4385 1204.77 10.7643 884.68 15.3476 1221.41 7.8579 889.28 17.1753 1231. 02 16.7333 894.76 17.2019 1235.36 0.0000 898.04 10.8743 1238.28 10.8449 900. 72 15.4171 1260.41 0.0000 903.28 17.2431 1271. 87 10.9248 911. 20 18.1909 1274.44 5. 9623 912.08 18.1952 1274.54 5. 9623 923.98 0.0000 1291.59 7.9785 926.50 18.2678 1298.22 0.0000 929 .11 f9.1947 1312 .11 0.0000 937.49 25.6519 1332.49 6.0359 944.13 0.0000 1362.66 0.0000 946.00 22.0378 1365.19 7.0893 949.00 10.1091 1368. 63 0.0000 667. 71 0.0000 1384.29 8.1333 962. 31 14.7563 1408.01 3.0646 964. 08 14.7637 1457.56 0.0000 966 .17 14.7720 1460.82 8.2573 911. 20 14.7827 1489.16 2.0756 968. 97 14.7827 1505.03 6.2457 983.53 0.0000 1584.12 6.3376 984.45 0.0000 1596.21 0.0000 Page 3972 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:01:06.36 *******x************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ***********************************x******************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date 2-0CT-2016 11:01:13. Sample date 7-DEC-2015 10:02:00. Acquisition date : 3-0CT-2016 06:57:53. Sample ID G405235046 Sample quantity l.56928E+02 GRAM Detector name : GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:14.88 0.4% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID .. 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 6 2 6 3 0 4 0 5 0 6 2 7 2 8 0 9 0 10 0 11 0 12 0 13 0 14 0 15* 2 16 2 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 3973 of 5809 Energy 27.05* 28.79* 32.30*

36.95* 63.44* 74.90 77.25 87.38 93.51* 99.39* 131.15 180.90 185.56* 208.31 238,58* 241. 74 295.01* 300.35 328.73 338.48* 351.89* 445 .11 510.66* 548.49 583.27* 609.38* 661.42* 727. 53 736.94 768.78 786.28 882.98 887.80 911.36* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 50 .29 16 32 47 . 178 310 120 52 37 41 42 107 17 437 114 166 41 61 61 251 9 29 8 121 207 66 32 28 30 29 10 16 112 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 13 45 90 150 194 197 160 133 280 114 194 99 126 113 62 74 90 84 77 56 51 30 68 17 48 22 24 16 21 37 17 16 7 17 1. 29 1.13 1. 75 2.80 0.85 1. 36 1.11 1. 05 1. 5.0 1. 98 3.89 1. 44 1. 81 0.72 1.13 1. 54 1. 34 0.79 4.87 1.13 1.17 0.80 2.09 0.78 1. 74 1. 60 1. 54 2.18 4.54 1. 30 0.79 1. 01 1. 20 1. 73 54.31 57.79 64.80 74.10 127.03 14.9. 93 154.64 174.87 187.13 198.89 262.37 361.81 371.12 416.59 477 .11 483.43 589.92 600.60 657.34 676.85 703.64 890.05 1021.16 1096. 82 1166. 38 1218.60 1322.72 1454.97 1473.80 1537.51 1572.53 1766.01 1775.67 1822.82 51 51 63 72 124 145 145 172 181 195 254 357 366 414 471 471 582 596 650 671 698 884 1013 1089 1160 1213 1315 1450 1466 1531 1568 1757 1770 1816 12 1.38E-02 24.7 2.07E+OO 12 7.95E-03 54.7 6 4.37E-03103.0 11 8.93E-03 77.4 8 1.31E-02 54.5 14 4.95E-02 15.8 2.15E+OO 14 8.60E-02 9.1 6 3.32E-02 17.9 10 1.44E-02 65.1 8 1. 04E-02 53. 0 13 1.14E-02 72.5 9 l.18E-02 45.1 12 2.98E-02 23.9 8 4.84E-03108.0 19 1.21E-01 5.7 1.05E+OO 19 3.16E-02 17.5 15 4.62E-02 14.7 13 l.15E-02 47.8 15 1. 69E-02 34. 3 9 1.69E-02 26.0 10 6.98E-02 8.3 8 2. 46E-03114. 7 14 8.llE-03 70.9 9 2. llE-03106. 5 16 3.37E-02 15.5 13 5.74E-02 8.6 14 l.82E-02 20.5 11 8. 87E-03 31. 5 14 7.78E-03 39.5 13 8.30E-03 46.6 11 7.92E-03 33.4 12 2.69E-03 92.3 10 4.32E-03 41.5 14 3.llE-02 12.5 Peak Search Report (continued) Page : 2 sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964.70 13 25 2.59 1929.58 1923 12 3.63E-03 80.4 36 0 969. 38 63 5 1. 49 1938.94 1934 10 1.76E-02 14.2 37 0 989.92 9 4 1. 42 1980.05 1977 6 2.43E-03 50.9 38 0 1010.46 18 12 1. 45 2021 .. 17 2016 12 5.00E-03 45.1 39 0 1080.88 27 8 2.47 2162.12 2153 16 7.54E-03 30.2 40 2 1117.13 14 0 1. 60 2234.70 2233 26 3.77E-03 26.5 5.65E-01 41 2 1120. 44 58 6 2.22 2241.33 2233 26 1.60E-02 17.2 42 0 1174.53 18 14 3.77 2349.61 2342 14 5.00E-03 50.0 43 0 1214.72 16 10 1. 04 2430.08 2423 11 4.32E-03 48.3 44 0 1238.62 36 13 1. 06 2477.94 2471 13 1. OlE-02 26 .3 45 0 1263. 96 12 3 0.62 2528.68 2525 7 3.28E-03 39.0 46 0 1377. 92 23 4 2.06 2756.91 2750 14 6.25E-03 27.5 47 0 1460.87* 383 4 1. 84 2923.06 2917 15 1.06E-01 5.3 48 0 1509.50 16 4 3.13 3020.48 3012 14 4:53E-03 34.8 49 0 1764.35 38 0 1. 91 3531.11 3525 12 1.06E-02 16.2 Flag: "*" = Peak area was modified by background subtraction Page 3974 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:01:08 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 10:02:00 G405235046 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:57:53 156.93 GRAM Sample type Detector name : Elapsed live 'time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA20 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3975 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:14.88 10.00 0.00 % Peak Energy 0.4% Nuclide Line Activity Report Page : 2 Sample* ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 *Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* l.312E+OO l.269E+Ol l.269E+Ol 10.54 OK SC-46 889.28 99.98* 1. 963E+OO 3.897E-02 4. 696E-01 83.02 OK 1120.55 99.99 l.635E+OO l.683E-01 2.028E+OO 34.44 OK CD-109 88.03 3.70* 6. 851E+OO l.952E+OO 3.068E+OO 55.60 OK SN-126 64.28 9.60 4.805E+OO 6.542E-01 6.542E-01 108.99 OK 86.94 8.90 6. 851E+OO 8 .116E-01 8 .116E-01 55.60 OK 87.57 37.00* 6.851E+OO 1. 952E-01 l.952E-01 55.60 OK BA-137M 661.66 89.90* 2.465E+OO l.506E-01 l.535E-01 40.91 OK CS-137 661.66 85.10* 2.465E+OO l.591E-01 1. 621E-01 40.91 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.719E+OO 2.705E-01 2.705E-01 30.91 OK 860.56 12.50 2. OllE+OO Line Not Found Absent BI-212 727. 33 6.67* 2.289E+OO l.051E+OO l.051E+OO 62.94 OK 785.37 1.10 2.156E+OO 5.987E+OO 5.987E+OO 66.71 OK 1620.50 1. 47 l.197E+00 Line Not Found Absent PB-212 74.82 10.28 6.003E+OO l.220E+OO 1. 220E+OO 49.27 OK 77 .11 17.10 6.195E+OO l.837E+00 l.837E+OO 18.29 OK 238.63 43.60* 5.553E+OO l.020E+00 . i°. 020E+OO 11. 49 OK 300.09 3.30 4. 643E+OO . l.487E+OO l.487E+OO 95.58 OK BI-214 609.32 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 OK 1120.29 14.92 l.635E+OO l.128E+OO l.128E+OO 34.44 OK 1764.49 15.30 l.106E+00 1. Ol 7E+OO l.017E+00 32.44 OK PB-214 74.82 5.80 5. 996E+OO Line Not Found <<INT Reject 77.11 9.70 6.195E+00 3.239E+OO 3.240E+00 18.29 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.495E+OO Line Not Found <<INT Reject 295.22 18.42 4. 711E+OO l.061E+OO 1.062E+OO 29.44 OK 351. 93 35.60* 4.084E+OO 9.393E-01 9. 396E-01 16.64 OK RN-222 609.32 45.49* 2.627E+00 8.865E-01 8.868E-01 17 .11 OK 1120.29 14.92 1.635E+OO l.128E+OO 1.128E+OO 34.44 OK 1764.49 15.30 l.106E+OO 1. Ol 7E+OO 1.017E+OO 32.44 OK RA-224 240.99 4.10* 5.499E+OO 9.734E-01 9.734E-01 117.17 OK RA-226 609.32 45.49* 2.627E+00 8.865E-01 8.868E-01 17 .11 OK 1120.29 14.92 1.635E+OO l.128E+OO l.128E+00 34.44 OK 1764.49 15.30 l.106E+00 1. Ol 7E+OO 1. 017E+OO 32.44 OK AC-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 OK 794.95 4.25 2.138E+00 Line Not Found Absent 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* 1. 923E+OO l.105E+OO 1.105E+OO 24.93 OK 968.97 15.80 1.833E+OO l.062E+00 1.062E+OO 28.37 OK RA-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 OK 794.95 4.25 2.138E+OO Line Not Found Absent 835.71 1. 61 2.057E+OO Line Not Found Absent 911. 2.0 25.80* l.923E+OO l.105E+OO 1.105E+OO 24.93 OK 968. 97 15.80 l.833E+OO l.062E+OO 1.062E+OO 28.37 OK TH-228 74.82 10.28 6.003E+OO l.220E+OO 1.220E+OO 49.27 OK 77 .11 17.10 6.195E+OO l.837E+OO 1.837E+oo. 18.29 OK Page 3976 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 5.553E+OO 1.020E+OO l.020E+00 11. 49 OK 300.09 3.30 4.643E+OO l.487E+OO l.487E+OO 95.58 OK TH-230 609.32 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 OK 1120.29 14.92 1.635E+OO 1.128E+OO 1.128E+00 34.44 OK 1764.49 15.30 1.106E+OO l.017E+OO 1.017E+OO 32.44 OK PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.643E+OO 9.175E-01 9.175E-01 95.58 OK TH-232 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 OK 835. 71 1. 61 2.057E+OO Line Not Found Absent 911. 20 25.80* 1.923E+OO 1.105E+OO 1.105E+OO 24.93 OK 968. 97 15.80 1.833E+OO 1.062E+OO 1.062E+OO 28.37 OK TH-234 63.29 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 OK 92.59 4.23 7.128E+OO 1.062E+OO 1.062E+OO 130 .16 OK U-234 609.32 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 OK 1120.29 14.92 1.635E+OO 1.128E+OO 1.128E+OO 34.44 OK 1764.49 15.30 1.106E+OO 1.017E+OO l.017E+00 32.44 OK U-238 63.29 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 OK 92.59 4.23 7.128E+OO 1.062E+OO l.062E+OO 130 .16 OK AM-243 43.53 5.90 1.315E+00 Line Not Found Absent 74.66 67.20* 6.003E+OO 1.866E-01 1.866E-01 49.27 OK ANH-511 511. 00 100.00* 3. 021E+OO 5.052E-02 5.052E-02 141.86 OK Flag: "*" = Keyline Page 3977 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:01:09.75 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l *
Acquisition date 3-0CT-2016 06:57:53 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000* *
Elapsed real time: 0 01:00:14.88 Half life ratio : ***** *
Sample date 7-DEC-2015 10:02:00 Analyst initials: MXRl *
Sample ID G405235046 Sample Quantity 1.5693E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry *o.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.269E+Ol 1. 311E+OO SC-46 4. 696E-01 3.821E-01 CD-109 3.068E+OO 1.672E+OO SN-126 l.952E-01 l.064E-01 BA-137M l.535E-01 6.152E-02 CS-137 1. 621E-01 6.499E-02 TL-208 2.705E-01 8.194E-02 BI-212 1. 051E+OO 6.481E-01 PB-212 1. 020E+OO 1.149E-01 BI-214 8.868E-01 1.487E-01 PB-214 9.396E-01 1.532E-01 RN-222 8.868E-01 l.487E-01 RA-224 9.734E-01 1.118E+OO RA-226 8.868E-01 l.487E-01 AC-228 1.105E+OO 2.701E-01 RA-228 1.105E+OO 2.701E-01 TH-228 1.020E+OO 1.149E-01 TH-230 8.865E-01 1.486E-01 PA-231 9.175E-01 8.594E-01 TH-232 1.105E+OO 2. 701E-01 TH-234 1.697E+OO 1.813E+OO U-234 8.865E-01 1.486E-01 1.697E+OO 1.813E+OO AM-243 1. 866E-01 9.009E-02 ANH-511 5*. 052E-02 7.024E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 Page 3978 of 5809 Key-Line Activity (pCi/GRAM -5 .115E+OO -1.917E-02 O.OOOE+OO 1.086E-02 O.OOOE+OO K.L. Cnt Uncert (1. 96-sigma) 1.107E+Ol 4.237E-02 1. 960E+41 2.590E-02 l.139E+04 MDA (pCi/GRAM 5.147E-01 6.020E-01 1.930E+OO l.232E-01 5.128E-02 5.417E-02 5.019E-02 6.314E-01 7.929E-02 8. 519E-02
1.067E-01 8.519E-02 8.498E-01 8.519E-02 1.828E-01 l.828E-01 7.929E-02 8.516E-02 6.520E-01 1.828E-01 1. 671E+00 8.516E-02 1. 671E+OO 7.188E-02 4.670E-02 MDA (pCi/GRAM 2.023E+Ol 7.807E-02 O.OOOE+OO 6.097E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF CR-51 O.OOOE+OO 3.656E+02 O.OOOE+OO SHORT HLIF MN-54 -4.845E-02 5.460E-02 8.750E-02 NOT IDENT. C0-56 1.518E-01 4 .115E-01 8.268E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -3.777E-02 3.927E-02 6.622E-02 NOT IDENT. C0-58 5.550E-03 4.930E-01 9.453E-01 NOT IDENT. FE-59 -l.985E+OO 5.718E+OO 1.090E+Ol NOT IDENT. C0-60 l.430E-02 3.034E-02 6.764E-02 FAIL ABUN ZN-65 3. 964E-02 1.497E-01 2.823E-01 NOT IDENT. GE-68 -1.014E+OO 1. 792E+OO 2.779E+OO NOT IDENT. AS-73 1.646E+OO 4.739E+OO 9.386E+OO NOT IDENT. AS-74 0.000E+OO 4.220E+03 O.OOOE+OO SHORT HLIF SE-75 3.793E-03 1.565E-01 3 .119E-01 NOT IDENT. BR-77 0.000E+OO 2.802E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.008E+02 0.000E+OO SHORT HLIF RB-83 3.339E-02 5.459E-01 1.068E+OO NOT IDENT. KR-85 5.665E-01 7.039E+OO 1.215E+Ol NOT IDENT. SR-85 5.953E-02 7.518E-01 1.298E+OO NOT IDENT. RB-86 o*. OOOE+OO 2.212E+04 0.000E+OO SHORT HLIF Y-88 l.568E-02 l.020E-01 2. 722E-01 NOT IDENT. Y-91 -2.924E+02 5.226E+02 9.439E+02 NOT IDENT. NB-94 2. 041E-02 2.513E-02 5.369E-02 NOT IDENT. NB-95 3.249E-02 9.390E-01 1.569E+OO NOT IDENT. NB-95M -6.130E-01 2.090E+OO 3.604E+OO NOT IDENT. ZR-95 l.472E-01 l.330E+OO 2. 561E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.267E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.104E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 9 .118E-03 3.061E-02 5.340E-02 NOT IDENT. RH-102 1. 775E-02 4.669E-02 9.560E-02 NOT IDENT. RU-103 1.059E+OO 4.673E+OO 9.369E+00 FAIL ABUN RH-106 -1.928E-01 4.256E-01 7.655E-01 NOT IDENT. RU-106 -1.928E-01 4.256E-01 7.655E-01 NOT IDENT. AG-108M 8.832E-03 2.139E-02 4.404E-02 NOT IDENT. AG-llOM 2.149E-03 8. 411E-02 l.197E-01 NOT IDENT. SN-113 -9. lBlE-02 1.833E-01 3.389E-01 NOT IDENT. CD-115 0.000E+OO 3.586E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.641E+04 O.OOOE+OO SHORT HLIF TE-123M 3.681E-02 1. 211E-01 2.248E-01 NOT IDENT. SB-124 -3.225E-01 1.841E+OO 3.677E+OO NOT IDENT. SB-125 -5.840E-03 8.387E-02 1.625E-01 NOT IDENT. TE-125M l.597E+02 2.287E+02 4. 481E+02 NOT IDENT. I-126 O.OOOE+OO 8.697E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.073E+06 O.OOOE+OO SHORT HLIF. SB-127 O.OOOE+OO 2.244E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.461E+09 0.000E+OO SHORT HLIF I-132 0.000E+OO l.712E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.775E+26 O.OOOE+OO SHORT HLIF BA-133 2.859E-03 3.448E-02 6.442E-02 NOT IDENT. I-133 O.OOOE+OO 1.850E+41 O.OOOE+OO SHORT HLIF CS-134 2.659E-02 4. 811E-02 9.665E-02 NOT IDENT. CS-135 -7.178E-02 l.210E-01 2.261E-01 NOT IDENT. I-135 O.OOOE+OO l.632E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.761E+05 O.OOOE+OO SHORT HLIF CE-139 -5.926E-02 1.0lOE-01 l.731E-01 NOT IDENT. BA-140 O.OOOE+OO 8.619E+05 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO *4.160E+05 O.OOOE+OO SHORT HLIF. CE-141 3. 271E+OO 2. 081E+Ol 3.867E+Ol NOT IDENT. CE-143 O.OOOE+OO 7.946E+40 O.OOOE+OO SHORT HLIF CE-144 -l.112E-01 3.246E-01 5.279E-01 NOT IDENT. PM-144 -6.332E-03 4.154E-02 7.840E-02 NOT IDENT. PR-144 -5.377E-01 3.612E+OO 6.822E+OO NOT IDENT. PM-146 8.016E-03 2.997E-02 6.164E-02 FAIL ABUN ND-147 O.OOOE+OO 2.688E+07 O.OOOE+OO SHORT HLIF PM-147 -2.573E+Ol 6. 2 62E+02 . l.160E+03 NOT IDENT. PM-149 O.OOOE+OO 4.503E+40 O.OOOE+OO SHORT HLIF EU-150 2.957E-02 2.439E-02 4.329E-02 FAIL ABUN EU-152 -2.624E-02 7. 325E-02' 1.387E-01 FAIL ABUN GD-153 -6.298E-02 l.605E-01 2.662E-01 NOT IDENT. EU-154 -6.036E-02 1. 047E-01 l.886E-01 NOT IDENT. EU-155 3.293E-02 9.435E-02 1. 793E-01 FAIL ABUN TB-160 l.519E-01 1. 752E+OO 3.037E+OO FAIL ABUN H0-166M 2.843E-02 4.399E-02 9.315E-02 FAIL ABUN TM-171 -3.299E+00 l.153E+Ol 2.173E+Ol NOT IDENT. HF-172 -1.727E-01 2.236E-Ol 3.476E-01 FAIL ABUN LU-172 -3.901E-04 7.317E-02 l.447E-01 FAIL ABUN LU-176 4.360E-03 l.993E-02 3.845E-02 FAIL ABUN Page 3979 of 5809 HF-181 , -1. 825E+OO 3.746E+OO 6.828E+00 NOT IDENT. TA-182 -7.189E-02 7.464E-01 l.466E+OO FAIL ABUN RE-183 8.555E-02 1.801E+OO 3.461E+OO NOT IDENT. RE-184 1.310E+Ol 2. 741E+Ol 5.575E+Ol NOT IDENT. W-188 -3.759E+Ol 9.494E+Ol l.602E+02 FAIL ABUN IR-192 1.964E-01 3. 964E-01 8.104E-01 FAIL ABUN HG-203 2.030E-01 2.051E+OO 4.059E+OO NOT IDENT. BI-207 1.858E-02 3.790E-02 8.239E-02 FAIL ABUN PB-210 1.886E+OO 1.478E+OO 3.170E+OO NOT. I DENT. BI-211 O.OOOE+OO 4.220E-01 7.389E-01 FAIL ABUN PB-211 2.369E-01 5.108E-01 1.054E+OO NOT IDENT. RN-219 -9.674E-03 3.102E-01 6.031E-01 NOT. IDENT. RA-223 2.368E-01 4.959E-01 9.336E-01 FAIL ABUN AC-227 l.446E-01 2.003E-01 4.146E-01 FAIL ABUN TH-227 1. 44 6E-01 2.003E-01 4.146E-01 FAIL ABUN TH-229 2.438E-02 3.644E-01 7.304E-01 FAIL ABUN TH-231 2.368E-01 4.959E-01 9.336E-01 FAIL ABUN PA-233 -6.129E-04 4.304E-02 8.536E-02 FAIL ABUN PA-234 6. lllE-02 2.261E-01 4.758E-01 FAIL ABUN PA-234M -3.214E-01 3.541E+00 7.209E+OO NOT IDENT. U-235 -2.878E-02 1. 651E-01 2.979E-01 FAIL ABUN NP-237 -6.129E-04 4.304E-02 8.536E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF NP-239 l.386E-01 2.049E-01 3.993E-01 FAIL ABUN PU-239 1.953E+02 2.743E+02 5.298E+02 NOT IDENT. AM-241 -6. 961E-02 8.839E-02 l.588E-01 NOT IDENT. CM-243 -3.105E-02 8.490E-02 l.530E-01 FAIL ABUN BK....:247 2.122E-02 5.382E-02 l'.108E-01 NOT IDENT. CM-247 -7.907E-03 2. 716E-02 5.145E-02 NOT IDENT. CF-249 -3.610E-03 2.972E-02 5.744E-02 NOT IDENT. CF-251 -2.636E-02 9.359E-02 1. 651E-01 NOT IDENT. Page 3980 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:01:07.19 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 371 10.66* l.312E+OO 1. 2 69E+Ol 1. 269E+Ol 10.54 SC-46 889.28 16 99.98* 1. 963E+OO 3.897E-02 4. 696E-01 83.02 1120.55 58 99.99 l.635E+OO l.683E-01 2.028E+OO 34.44 CD-109 88.03 155 3.70* 6. 851E+OO 2.930E+OO 4.605E+OO 35.71 SN-126 64.28 63 9.60 4.805E+OO 6.542E-01 6.542E-01 108.99 86.94 155 8.90 6. 851E+OO l.218E+OO l.218E+OO 35.71 87.57 155 37.00* 6.851E+OO 2.930E-01 2.930E-01 35. 71 BA-137M 661.66 70 89.90* 2.465E+OO l.506E-01 l.535E-01 40.91 CS-137 661.66 70 85.10* 2.465E+OO l.591E-01 l.621E-01 40.91 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 131 85.00* 2. 719E+OO 2.705E-01 2. 705E-01. 30.91 860.56 ------12.50 2. OllE+OO ------Line Not Found ------BI-211 72.87 ------1. 23 5.823E+OO ------Line Not Found ------351.06 285 12.92* 4.084E+OO 2.588E+OO 2.588E+OO 16.64 BI-212 727. 33 34 6.67* 2.289E+OO l.051E+OO i. o5rn+oo 62.94 785.37 30 1.10. 2.156E+OO 5.987E+OO 5. *987E+OO 66.71 1620.50 ------1. 47 l.197E+00 ------Line Not Found ------PB-212 74.82 235 . 10.28 6.003E+OO l.818E+OO l.818E+OO 31. 59 77 .11 407 17.10 6.195E+OO l.837E+OO l.837E+OO 18.29 238.63 516 43.60* 5.553E+OO l.020E+OO l.020E+OO 11. 49 300.09 48 3.30 4.643E+OO l.487E+OO
1. 487E+OO 95.58 BI-214 609.32 221 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 1120.29 58 14.92 l.635E+OO l.128E+OO l.128E+OO 34.44 1764.49 36 15.30 l.106E+OO 1.017E+OO l.017E+OO 32.44 PB-214 74.82 235 5.80 6.003E+OO 3.223E+OO 3.224E+OO 31. 59 77 .11 407 9.70 6.195E+OO 3.239E+OO 3.240E+OO 18.29 87.09 155 3.41 6.851E+OO 3.180E+OO 3.181E+OO 35.71 242.00 134 7.25 5.499E+OO l.612E+OO l.612E+OO 35.01 295.22 192 18.42 4. 711E+OO 1. 061E+OO 1. 062E+OO 29.44 351. 93 285 35.60* 4.084E+OO 9.393E-01 9.396E-01 16.64 RN.-222 609.32 221 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 1120.29 58 14.92 l.635E+OO l.128E+OO l.128E+OO 34.44 1764.49 36 15.30 l.106E+OO l.017E+OO 1. Ol 7E+OO 32.44 RA-224 240.99 134 4.10* 5.499E+OO 2.850E+OO 2.850E+OO 35.01 RA-226 609.32 221 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 1120.29 58 14.92 l.635E+OO l.128E+OO l.128E+OO 34.44 1764.49 36 15.30 l.106E+OO 1. Ol 7E+OO l .,Ol 7E+OO 32.44 AC-228 105.21 ------1.10 7.453E+00 ------Line Not Found ------338.32 69 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 794.95 ------4.25 2.138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------911.20 115 25.80* l.923E+OO l.105E+OO l .. 105E+OO 24.93 968. 97 64 15.80 l.833E+OO l.062E+OO l.062E+OO 28.37 RA-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 69 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 794.95 ------4.25 2.138E+00 ------Line Not Found ------835. 71 ------1. 61 2.057E+OO ------Line Not Found ------Page 3981of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911.20 115 25.80* 1. 923E+OO l.105E+OO 1.105E+OO 24.93 968.97 64 15.80 1.833E+OO 1.062E+OO 1.062E+OO 28.37 TH-228 74.82 235 10.28 6.003E+OO 1.818E+OO 1.818E+OO 31. 59 77 .11 407 17.IO 6.195E+OO 1.837E+OO 1.837E+OO 18.29 238.63 516 43.60* 5.553E+OO 1.020E+OO 1.020E+OO 11. 49 300.09 48 3.30 4.643E+OO l.487E+OO l.487E+00 95.58 TH-230 609.32 221 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 1120.29 58 14.92 1.635E+00 l.128E+00 1.128E+OO 34.44 1764.49 36 1*5. 30 l.106E+OO l.017E+OO 1. 017.E+OO 32.44 PA-231 283.69 ------1.70 4.860E+OO ------Line Not Found ------301.36 48 5.35* 4.643E+OO 9.175E-Ol 9.175E-01 95.58 TH-232 105.21 ------1.10 7.453E+00 ------Line Not Found ------338.32 69 11. 27 4.215E+OO 6.986E-Oi 6.986E-01 51. 98 835.71 ------1. 61 2.057E+OO ------Line Not Found ------911. 20 115 25.80* 1. 923E+OO 1.105E+OO 1.105E+OO 24.93 968. 97 64 15.80 1. 833E+OO 1. 062E+00 1. 062E+OO 28.37 TH-234 . 63. 29 63 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 92.59 67 4.23 7.128E+00 1.062E+OO 1.062E+OO 130.16 U-234 609.32 221 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 1120.29 58 14.92 1.635E+oo l.128E+00 1.128E+OO 34.44 1764.49 36 15.30 l.106E+OO 1. 017E+OO 1. Ol 7E+OO 32.44 U-238 63.29 63 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 92.59 67 4.23 7.128E+00 l.062E+00 1.062E+OO 130.16 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 235 67.20* 6.003E+OO 2.782E-01 2.782E-01 31. 59 ANH-511 511. 00 32 100.00* 3.021E+OO 5.052E-02 5.052E-02 141.86 Flag: "*" Key line Page 3982 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235.046 Acquisition date 3-0CT-2016 06:57:53 Total number of lines in spectrum 49 Number of unidentified lines 16 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 S'C-46 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 83.790 461. 40D 2.30E+05Y* 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1.41E+l0Y 1.41E+10Y 1. 4.lE+lOY 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1. OOE+09Y Decay 1. 00 12.1 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. ob 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 :i. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.269E+Ol 3.897E-02 2.930E+OO 2.930E-01 1.506E-01 1. 591E-01 2.705E-01 2.588E+OO 1.051E+00 1.020E+OO 8.865E-01 9.393E-01 8.865E-01 2.850E+OO 8.865E-01 1.105E+OO 1.105E+OO 1.020E+00 8.865E-01 9.175E-01 1.105E+OO 1. 697E+OO 8.865E-01 1.697E+OO 2.782E-Ol* 5.052E-02 3.839E+Ol 3.839E+Ol Decay Corr pCi/GRAM l.269E+Ol 4. 696E-01 4.605E+OO 2.930E-01 1.535E-01 1.621E-01 2.705E-01 2.588E+OO 1. 051E+OO 1.020E+OO 8.868E-01 9. 396E-01 *8.868E-01 2.850E+OO 8.868E-01 1.105E+OO 1.105E+OO 1.020E+OO 8.865E-01 9.175E-01 1.105E+OO l.697E+OO 8. 8.65E-01 1.697E+OO 2.782E-01 5.052E-02 4.050E+Ol 4.050E+Ol 67.35% Decay Corr 2-Sigma Error 0.134E+Ol 3.899E-Ol 1.645E+OO 1.047E-01 0.628E-01 0.663E-01 0.836E-01 0. 431E+OO 0.661E+OO 0 .117E+OO l.517E-01 l.563E-01 1. 517E-01 0.998E+OO 1. 517E-01 0.276E+OO 0.276E+OO 0 .117E+OO 1.516E-01 8.769E-01 0.276E+OO 1.850E+OO 1.516E-01 1.850E+OO 0.879E-01 7.167E-02 "M" .= Manually accepted 2-Sigma %Error 10.54 83.02 35.71 35.71 40.91 40.91 30.91 16.64 62.94 11. 49 17 .11 16.64 17 .11 35.01 17 .11 24.93 24.93 11. 49 17 .11 95.58 24.93 108.99 17 .11 108.99 31. 59 141.86 "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3983 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235046 Acquisition *date : 3-0CT-2016 06:57:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 27.05 71 19 1. 29 54.31 51 12 l.38E-02 49.4. 4.65E-07 6 28.79 41 65 1.13 57.79 51 12 7.95E-03 **** 4.59E-05 0 32.30 22 128 1. 75 64.80 63 6 4.37E-03 **** 9.28E-03 0 36.95 45. 210 2.80 74.10 72 11 8.93E-03 **** 2.24E-01 0 99.39 48 146 1. 98 198.89 195 8 l.04E-02 **** 7.32E+OO T 0 l31.15 51 243 3.89 262.37 254 13 l.14E-02 **** 7.52E+OO T 0 180.90 51 120 1. 44 361.81 357 9 1. 18.E-02 90.2 6.67E+OO T 0 185.56 130 153 ,1. 81 371.12 366 12 2.98E-02 47.9 6.57E+OO T 0 208.31 21 J.35 0.72 416.59 414 8 4.84E-03 **** 6.llE+OO 0 328.73 69 88 4.87 657.34 650 15 1.69E-02 68.5 4.32E+OO T 0 445 .11 10 33 0.80 890.05 884 8 2.46E-03 **** 3.37E+OO 0 548.49 8 19 0. 7, 8 1096. 82 1089 9 2. llE-03 **** 2.85E+OO 0 736.94 29 22 4.54 1473.80 1466 14 7.78E-03 79.1 2.27E+OO T 0 768.78 31 39 1. 30 1537.51 1531 13 8.30E-03 93.1 2.19E+00 0 882.98 10 17 1. 01 1766.01 1757 12 2.69E-03 **** 1. 97E+OO T 0 964.70 13 25 2.59 1929.58 1923 12 3.63E-03 **** 1.84E+OO T 0 989.92 9 4 1. 42 1980.05 1977 6 2.43E-03 **** 1.80E+OO 0 1010.46 18 12 1. 45 2021.17 2016*12 5.00E-03 90.3 l.77E+00 0 1080.88 27 8 2.47 2162.12 2153 16 7.54E-03 60.3 1. 68E+OO 2 1117.13 14 0 1. 60 2234.70 2233 26 3.77E-03 53.1 1. 64E+OO 0 1174.53 18 14 3.77 2349.61 2342 14 5.00E-03 **** 1.57E+OO T 0 1214.72 15 10 1. 04 2430.08 2423 11 4.32E-03 96.5 l.53E+OO 0 1238.62 36 13 1. 06 2477.94 2471 13 1.0lE-02 52.6 1. 51E+OO T 0 1263. 96 12 3 0.62 2528.68 2525 7 3.28E-03 77.9 1. 48E+00 0 1377.92 22 3 2.06 2756.91 2750 14 6.25E-03 55.0 1.38E+OO 0 1509.50 16 4 3.13 3020.48 3012 14 4.53E-03 69.7 l.28E+00 Flags: "T" = Tentatively associated Page 3984 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:01:25.66 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l *
Acquisition date 3-0CT-2016 06:57:53 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.88 Half life ratio : ***** *
Sample date 7-DEC-2015 Nuclide Library : SOLID *
Sample ID G405235046 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.5693E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * **
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.'GAMMA]EFF GAM20 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 . Le (pCi/GRAM 2.107E-01 2.604E-01 9. 221E-01 5.887E-02 2.257E-02 2.385E-02 2.220E-02 2.722E-01 3.683E-02 3.700E-02 4.870E-02 3.700E-02 3.947E-01 3.700E-02 7.807E-02 7.807E-02 3.683E-02 3.699E-02 2.986E-01 7.807E-02 7.959E-01 3 .. 699E-02. 7.959E-01 3.420E-02 2 .113E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 Page 3985 of 5809 Le (pCi/GRAM 9.099E+OO 3.350E-02 O:OOOE+OO 2.447E-02 O.OOOE+OO 0. OOOE.+00 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139. BA-140 LA-:-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3986 of 5809 3.747E-02 3.650E-01 O.OOOE+OO 3.081E-02 4.126E-01 4.690E+OO 2.869E-02 l.226E-01 l.128E+OO 4.414E+OO O.OOOE+OO 1.431E-01 0.000E+OO O.OOOE+OO 4.779E-01 5.535E+OO 5. 911E-01 0.000E+OO 9.266E-02 4.143E+02 2.401E-02 7.061E-01 1. 674E+00 1.138E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.510E-02 4.237E-02 4.200E+OO 3.372E-01 3.372E-01 1. 986E-02 4.917E-02 l.524E-01 O.OOOE+OO O.OOOE+OO l.058E-01 l.459E+OO 7.327E-02 2 .111E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.937E-02 O.OOOE+OO 4.355E-02 1.047E-01 O.OOOE+OO 0.000E+OO 8.093E-02 O.OOOE+OO O.OOOE+OO 1.815E+Ol O.OOOE+OO 2.467E-01 3.419E-02 2.975E+OO 2.736E-02 0.000E+OO 5.399E+02 O.OOOE+OO l.997E-02 6. 296E-02 l.252E-01 8.073E-02 8.469E-02 l.320E+OO 4.130E-02 l.022E+Ol l.628E-01 6.387E-02 l.764E-02 3.053E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.' SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT*. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL'ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3987 of 5809 6.346E-01 l.631E+00 2.464E+Ol 7.305E+Ol 3.741E-01 l.881E+00 3.593E-02 l.498E+OO 3.568E-01 4.779E-01 2.737E-01 4.279E-01 l.937E-01 1.937E-01 3.409E-01 4.279E-01 3.876E-02 2.085E-01 3.166E+OO 1. 404E-01 3.876E-02 O.OOOE+OO l.881E-01 2.504E+02 7.483E-02 7.192E-02 5.099E-02 2.317E-02 2.600E-02 7.666E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:01:31.39 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l *
Acquisition date 3-0CT-2016 06:57:53 Sensitivity : 3.000 *
Detector ID : GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.88 Half life ratio : ***** *
Sample date 7-DEC-2015 10:02:00 Nuclide Library : SOLID *
Sample ID G405235046 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.5693E+02 GRAM *
Quantity Err(%) : 1.2745E-03 % * *Wet wt corr 1;00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 06:52:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5 .
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" valid. Please refer to Certificate of Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.269E+Ol l.468E+00 l.468E+00 SC-46 ,4. 696E-01 3.826E-01 3.826E-01 CD-109 3.068E+OO 1. 701E+00 1. 701E+00 SN-126 l.952E-01 1.078E-01 1.078E-01 BA-137M l.535E-01 6.187E-02 6.187E-02 CS-137 l.621E-01 6.536E-02 6.536E-02 TL-208 2.705E-01 8.274E-02 8.274E-02 BI-212 1.051E+OO 6.503E-01 6.503E-01 PB-212 l.020E+00 1.269E-01 1. 2 69E-01 BI-214 8.868E-01 l.534E-01 1.534E-01 PB-214 9. 396E-01 1.581E-01 1.581E-01 RN-222 8.868E-01 1.534E-01 l.534E-01 RA-224 9.734E-01 1.126E+OO 1.126E+OO RA-22 6 8.868E-01 1.534E-01 *1. 534E-01 AC-228 1 *.105E+OO 2.759E-01 2.759E-01 RA-228 1.105E+OO 2.759E-01 2.759E-01 TH-228 1.020E+OO 1.269E-01 1. 269E-Cil TH-230 8.865E-01 l.534E-01 1.534E-01 PA-231 9.175E-01 8.814E-01 8.814E-01 TH-232 1.105E+OO 2.759E-01 2.759E-01 TH-234 1.697E+OO 1.852E+OO 1.852E+OO U-234 8.865E-01 1.534E-01 1. 534E-01 . U-238 1.697E+OO 1.852E+OO 1.852E+OO
AM-243 1. 8 66E-01 9.155E-02 9.155E-02 ANH-511 5. 052.E-02 7.027E-02 7.027E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) BE-7 -5.115E+OO 1.108E+Ol 1.131E+Ol NOT IDENT. NA-22 -1.917E-02 4.237E-02 4.324E-02 NO.T IDENT. NA-24 -l.OOOE+41 6.259E+41 O.OOOE+OO SHORT HLIF AL-26 1.086E-02 2.591E-02 2.637E-02 NOT IDENT. V-48 -5.929E+03 1.139E+04 l.170E+04 SHORT HLIF Page 3988 of 5809 CR-51 l.126E+02 3.656E+02 3. 691E+02 SHORT HLIF MN-54 -4.845E-02 5.464E-02 5.885E-02 NOT IDENT. C0-56 l.518E-01 4 .115E-01 4.172E-01 FAIL ABUN MN-56 l.000E+41 2.735E+41 O.OOOE+OO SHORT HLIF C0-57 -3.777E-02 3.930E-02 4.283E-02 NOT IDENT. C0-58 5.550E-03 4.930E-01 4.930E-01 NOT IDENT. FE-59 -l.985E+OO 5. 720E+OO 5.790E+OO NOT IDENT. C0-60 l.430E-02 3.034E-02 3.102E-02 FAIL ABUN ZN-65 3. 964E-02 l.497E-Ol l.507E-01 NOT IDENT. GE-68 -l.014E+QO 1. 7 92E+OO l.850E+OO NOT IDENT. AS-73 l.646E+OO 4.751E+OO 4.809E+OO NOT IDENT. AS-74 -1. 713E+OO 4.220E+03 4.220E+03 SHORT HLIF SE-75 3.793E-03 1. 565E-01 l.565E-01 NOT IDENT. BR-77 2.488E+38 2.161E+39 O.OOOE+OO SHORT HLIF SR-82 l.806E+02 6.009E+02 6.063E+02 SHORT HLIF RB-83 3.339E-02 5.459E-01 5.461E-01 NOT IDENT. KR-85 5.665E-Ol 7.039E+OO 7.043E+OO NOT IDENT. SR-85 5.953E-02 7.518E-01 7.523E-01 NOT IDENT. RB-86 -l.386E+04 2.213E+04 2.299E+04 SHORT HLIF Y-88 l.568E-02 l.021E-01 l.023E-01 NOT IDENT. Y-91 -2.924E+02 5.227E+02 5.391E+02 NOT IDENT. NB-94 2.041E-02 2.515E-02 2.678E-02 NOT IDENT. NB-95 3.249E-02 9.390E-01 9.391E-01 NOT IDENT. NB-95M -6.130E-01 2.090E+OO 2.108E+OO NOT IDENT. ZR-95 1. 472E-01 1. 330.E+OO 1. 331E+OO NOT IDENT. NB-97 l.OOOE+41 3.004E+41 O.OOOE+OO SHORT HLIF ZR-97 1. 000E+41 1. 2 68E+41 O.OOOE+OO SHORT HLIF M0-99 7.318E+31 2.104E+32 o .*oooE+oo SHORT HLIF TC-99M 1. OOOE+41 4.564E+41 O.OOOE+OO SHORT HLIF RH-101 9 .118E-03 3.066E-02 3.093E-02 NOT IDENT. RH-102 1. 775E-02 4. 671E-02 .4.739E-02 NOT IDENT. RU-103 l.059E+OO 4.673E+OO 4.697E+OO FAIL ABUN RH-106 -l.928E-01 4.258E-01 4.345E-01 NOT IDENT. RU-106 -l.928E-01 4.258E-01 4.345E-01 NOT IDENT. AG-108M 8.832E-03 2.139E-02 2.176E-02 NOT IDENT. AG-llOM 2.149E-03 8. 411E-02 8. 411E-02 NOT IDENT. , SN-113 -9 .181E-02 l.834E-01 l.880E-01 NOT IDENT. CD-115 3.850E+39 3.654E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -l.833E+04 9.643E+04 9.679E+04 SHORT HLIF TE-123M 3.681E-02 1. 211E-01 l.222E-01 NOT IDENT. SB-124 -3.225E-01 l.841E+OO l.847E+OO NOT IDENT. SB-125 -5.840E-03 8.387E-02. 8.391E-02 NOT IDENT. TE-125M l.597E+02 2.289E+02 2.399E+02 NOT IDENT. I-126 -5.194E+05 8.726E+05 9.035E+05 SHORT HLIF SB-126 -2.742E+04 l.073E+06 l.073E+06 SHORT HLIF SB-127 -l.038E+22 2.662E+22 O.OOOE+OO SHORT HLIF I-131 -3.345E+08 4.461E+09 4.463E+09 SHORT HLIF I-132 -l.OOOE+41 l.862E+42 O.OOOE+OO SHORT HLIF TE-132 -6. 031E+25 3.783E+26 O.OOOE+OO SHORT HLIF BA-133 2.859E-03 3.448E-02 3.450E-02 NOT IDENT. I-133 -l.OOOE+41 2.592E+41 O.OOOE+OO SHORT HLIF CS-134 2.659E-02 4.812E-02 4.959E-02 NOT IDENT. CS-135 -7.178E-02 1. 211E-01 l.254E-01 NOT IDENT. I-135 -l.OOOE+41 6.992E+41 O.OOOE+OO SHORT HLIF CS-136 -2.112E+04 2.761E+05 2.763E+05 SHORT HLIF CE-139 -5.926E-02 l.017E-01 1. 051E-01 NOT IDENT. BA-140 4.661E+05 8.621E+05 8.873E+05 SHORT HLIF LA-140 -2.072E+05 4.161E+05 4.265E+05 SHORT HLIF CE-141 3.271E+OO 2. 081E+Ol 2.086E+Ol NOT IDENT. CE-143 l.OOOE+41 8. 011E+40 O.OOOE+OO SHORT HLIF CE-144 -l.112E-01 3.246E-01 3.285E-01 NOT IDENT. PM-144 -6.332E-03 4.154E-02 4.164E-02 NOT IDENT. PR-144 -5.377E-01 3.612E+OO 3.621E+OO NOT IDENT. PM-146 8.016E-03 2.997E-02 3.019E-02 FAIL ABUN ND-147 -l.122E+07 2.689E+07 2.736E+07 SHORT HLIF PM-147 -2.573E+Ol 6.262E+02 6.263E+02 NOT IDENT. PM-149 -4.003E+40 4.588E+40 O.OOOE+OO SHORT HLIF EU-150 2.957E-02 2.442E-02 2.782E-02 FAIL ABUN EU-152 -2.624E-02 7.327E-02 7.422E-02 FAIL ABUN GD-153 -6.298E-02 l.606E-01 l.631E-01 NOT IDENT. EU-154 -6.036E-02 l.047E-01 l.082E-01 NOT IDENT. EU-155 3.293E-02 9.438E-02 9.554E-02 FAIL ABUN TB-160 l.519E-01 l.752E+OO l.753E+OO FAIL ABUN H0-166M 2.843E-02 4.402E-02 4.584E-02 FAIL ABUN TM-171 -3.299E+00 l.154E+Ol l.163E+Ol NOT I DENT*. HF-172 -l.727E-01 2.253E-01 2.384E-01 FAIL ABUN LU-172 -3. 901E-04 7.317E-02 7.317E-02 FAIL ABUN LU-176 4.360E-03 l.993E-02 2.003E-02 FAIL ABUN Page 3989 of 5809 HF-181 -l.825E+OO 3.747E+OO 3.836E+OO NOT IDENT. TA-182 -7.189E-02 7.464E-01 7.471E-01 FAIL ABUN RE-183 8.555E-02 1. 801E+OO 1.802E+OO NOT IDENT. RE-184 1.310E+Ol 2.759E+Ol 2.822E+Ol NOT IDENT. W-188 -3.759E+Ol 9.503E+Ol 9.653E+Ol FAIL ABUN IR-192 1. 964E-01 3. 965E-01 4.062E-01 FAIL ABUN HG-203 2.030E-01 2.051E+OO 2.053E+OO NOT IDENT. BI-207 1.858E-02 3.791E-02 3.882E-02 FAIL ABUN PB-210 l.886E+OO 1.487E+OO 1. 713E+OO NOT IDENT. BI-211 2.588E+OO 4.375E-01 1.246E+OO FAIL ABUN PB-211 2.369E-01 5.109E-01 5.220E-01 NOT IDENT. RN-219 -9.674E-03 3.102E-01 3.102E-01 NOT IDENT. RA-223 2.368E-01 4. 961E-01 5.074E-01 FAIL ABUN AC-227 l.446E-01 2.013E-01 2 .115E-01 FAIL ABUN TH-227 1. 446E-01 2.013E-01 2 .115E-01 FAIL ABUN TH-229 2.438E-02 3.644E-01 3.645E-01 FAIL ABUN TH-231 2.368E-01 4. 961E-01 5.074E-01 FAIL ABUN PA-233 -6.129E-04 4.304E-02 4.304E-02 FAIL ABUN PA-234 6. lllE-02 2.366E-01 2.382E-01 FAIL ABUN PA-234M -3.214E-01 3.541E+OO 3.544E+OO NOT IDENT. U-235 -2.878E-02 1.651E-01 1.656E-01 FAIL ABUN NP-237 -6.129E-04 4.304E-02 4.304E-02 FAIL.ABUN NP-238 4.781E+40 5.270E+41 O.OOOE+OO SHORT HLIF NP-239 1. 38 6E-01 2.052E-01 2.145E-01 FAIL ABUN PU-239 l.953E+02 2.744E+02 2.882E+02 NOT IDENT. AM-241 -6. 961E-02 8.853E-02 9.393E-02 NOT IDENT. CM-243 -3.105E-02 8.495E-02 8.609E-02 FAIL ABUN BK-247 ' 2.122E-02 5.399E-02 5. 48'3E-02 NOT IDENT. CM-247 -7.907E-03 2.719E-02 2.743E-02 NOT IDENT. CF-249 -3.610E-03 2.972E-02 2.977E-02 NOT IDENT. CF-251 -2.636E-02 9.364E-02 9.439E-02 NOT IDENT. Page 3990 of 5809
GEL Laboratories LLC * * *2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* *ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 82.9146 87.09 128.9682 136.47 78.5592 45.60 91.8005 87.57 152. 2725 140.51 0.0000 46.54 54.5410 88.03 152.3671 143.76 88.8718 49.72 0.0000 88.34 155.4788 144.24 73.0792 51. 35 83.1043 88.47 155.5053 145.44 69.5070 51. 87 95.0677 89. 96 153.5216 152.43 72. 4293 52.39 89.7516 1093.63 155.9520 153.25 0.0000 52.97 82.2692 91.11 0.0000 323.87 88.5366 53.44 74.7554 92.59 136.8048 156.02 0.0000 54.07 78.0941 93.35 136.9392 158.56 0.0000 57.36 0.0000 94.56 89.1293 159.00 72.8749 57.53 79.6633 94.65 89.1400 162.33 75.5742 57.98 87.3697 94.67 89.1423 162.66 0.0000 59.27 110. 5481 94.87 89.1647 163.33 70.6829 59.32 110.5574 97.43 90. 9961 165.86 84.5154 59.54 110.5986 98.43 79.9144 176.31 62. 7151 60. 96 96. 5938 98.44 79.9155 176.60 0.0000 61.17 96. 6277 99.53 80.0234 177.52 62.7808 62. 93 133.2498 100 .11 83.5626 181.07 0.0000 63.29 133.3285 102.03 65.1465 181.52 52.9153 63.58 133.3915 103.18 94.7497 184.41 56.8323 64.28 133.5432 103.37 92.0526 143.76 56.8948 66.73 125.5735 105.21 86.4173 193.51 64.4698 67.24 103.4961 105.31 86.4274 197.03 85.9195 125.81 109.4862 106.12 79.4966 198.01 66.4052 67.75 109.4982 106.47 86.5471 201.83 77.7079 69.67 125.7801 109.28 70.4057 203.43 66.6901 70.83 107.0471 111. 00 96.4134 205.31 62.9353 72. 81 137.1933 111.76 0.0000 210.85 74.8134 72.87 137.2054 114.06 100.2916 215.65 60.4147 74.66 127.8517 116. 30 0.0000 222 .11 66.7766 74.82 127.8821 116.74 71. 0088 227.09 54.8353 74.97 127.9099 119.76 45.1233 227.38 54.8469 77 .11 128.3109 121.12 61. 8397 228*.16 0.0000 78.74 114.3224 121. 22 61.8464 228.18 55.7500 79.69 114.4770 121.78 78.5457 116.74 55.7500 80.12 108.5178 122.06 83. 3311 235.69 64.3716 80.19 0.0000 122.92 51. 2370 235. 96 64.3835 80.57 81. 4400 123.07 54.8208 238.63 57.0456 81. 00 98.0891 265.00 50.0868 238.98 0.0000 81. 07 107.1544 125.81 95.6219 240.99 57.1401 81. 75 120.0967 127.23 73.4206 242.00 57.1805 83.79 118 .1648 127.91 84.6545 244.70 46.2708 84.00 112.1374 129.30 79.1797 252.40 0.0000 85.43 130.5773 131.20 79.3368 252.80 53.1750 86.55 133.8163 133. 02 75.4723 254.15 0.0000 86.79 133.8593 133.52 77 .1182 256.23 52.4100 86.94 128.9424 136.00 70.0653 260.90 0.0000 Page 3991of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.0913 355.39 0.0000 584.27 19. 8396 264.80 41.0951 356.01 25.4592 595.83 0.0000 265.00 37.5267 364.49 0.0000 427.87 16.8092 268.22 64.4663 366.42 0.0000 602.52 0.0000 269.46 38.5322 372. 51 33.2910 604.72 9.4695 270.03 36.7534 . 375.05 40.9546 607.14 15.7965 271.23 59.2096 377.52 33*. 377 9 609.32 14.7554 273.65 0.0000 356.01 34.4429 610.33 14.7611 276.40 52.2061 388.16 32.6006 614.28 22.1732 277.37 53.1386 388.63 0.0000 618.01 23.2604 277.60 42.3375 391.69 34.5798 620.36 19.0481 278.00 38.7439 264.66 26.0508 621.93 24.3523 279.20 51. 3976 401.81 32.8234 630.19 0.0000 279.54 54 .1138 402.40 31.8674* 631.29 15.9357 279.70 54 .1199 404.85 25.1378 633.25 17.0098 280.46 49.6334 410.95 36.8496 634.78 0.0000 283.69 35.2660 413. 71 29.1309 635.95 14.8978 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 41. 6407 423. 72 0.0000 645.85 17.0859. .285.90 0.0000 427.09 27.3631 657.76 12.8682 287.50 32.6309 427.87 29.3280 657.90 0.0000 290.67 43.5938 433.94 22.5494 661. 66 18.2541 293.27 0.0000 439.40 30. 9610 664.57 0.0000 351. 93 40.9827 453.88 17.8099 666.33 0.0000. 295.96 41. 0019 463.37 27.8228 666.50 0.0000 879.38 21.9023 468.07 29.8724 667.71 0.0000 299.98 39.7316 473.00 0.0000 677.62 23.7528 300.09 39.7343 475.06 28.9658 685.70 0.0000 300.13 39.7352 476.78 19.9915 695.00 0.0000 301.36 39.7644 4 77. 6'0 33. 9972 696.49 17.3848 302.85 39.7998 482.18 31.0593 696. 51 17.3848 256 .23 41.2134 487.02 0.0000 697.00 0.0000 304.85 0.0000 492. 35 0.0000 697.30 9.7815 306.78 37.4174 497.08 22.1835 697.49 8.6953 308.46 41.3104 505.52 19.7329 702.65 14.1537 311. 90 33 .1157 507.63 0.0000 706.68 15.2629 316.51 39.6616 511. 00 30.4279 711. 68 13.1040 319.41 0.0000 514.00 33.5129 720.70 0.0000 320.08 0.0000 514.00 33.5129 72-1. 93 0.0000 321.04 43.4649 520.40 23.4193 722.78 18.0831 323.87 31. 9570 520.69 0.0000 722. 91 18.0838 325.23 43.1056 522.65 0.0000 .723.31 31.2403 328.76 0.0000 527.90 0.0000 724.19 24.6707 333.37 41. 9073 528.26 15.3223 727.33 13.1709 333.97 22.3584 529.59 25.5513 733.00 8.7965 334.37 41. 9312 529.87 0.0000 735.93 14.3081 338.28 52.2949 531. 02 0.0000 333.97 14.3150 338.32 52.2961 537.26 0.0000 739.50 0.0000 311. 90 36.4641 546.56 0.0000 747.24 16.5686 340.48 36.4641 552.55 17.5347 748.06 18.7826 340.55 0.0000 563.25 21.7520 752.31 17.7012 344.28 38.4141 569.33 24.9180 753.82 0.0000 345.93 31. 5096 946.00 22.8424 756.73 19.9417 351.06 36.6760 569.70 22.8442 756.80 19.9424 351.93 36.6934 583.19 19.8311 884.68 26.6494 Page 3992 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:03:01.04 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 7-DEC-2015 10:10:00. Acquisition date : 3-0CT-2016 07:00:30. Sample ID G405235047 Sample quantity 1.51349E+02 GRAM Detector name GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 0 4 2 5 2 6 0 7 0 8 0 9 0 10 0 11 0 12 3 13 3 14 0 15 4 16' 4 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 . 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Energy 46.64* 53.35* 63.13* 74.85* 77.15* 83.83* 88.17 92.83* 129.09 186.02* 209.42 238.77* 2 41. 67 270.41 276.52 277.89* 295.19* . 300. 34 328.32 338.88* 352. ('.)9* 447.74 464.79 482.67 511.26* 556.69 583.58* 588.90 609.55* 626.45 690.83 694.35 727 .11 797.89 Page 3994 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 68 38 55 165 430 32 244 126 23 86 37 449 110 44 17 25 169 43 41 96 268 22 14 19 8 15 108 8 185 36 17 10 37 30 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 221 110 241 227 177 143 264 159 138 134 106 80 104 83 12 44 64 53 58 66 74 11 49 23 62 21 42 19 54 45 18 13 7 28 1. 04 1.16 0.72 0.76 0.79 1.14 3.47 1. 39 0.78 1.12 0.99 1. 03 1. 54 0.79 0.83 1. 33 1.19 0.90 2.39 1. 56 1. 08 2.19 0.90 1. 77 1. 24 0.64 1.32 1. 25 1. 40 7.10 2.00 1. 38 1. 72 5.52 92.79 106.19 125.75 149.19 153.79 167.14 175.83 185.15 257.66 371.50 418.30 477.00 482.79 540.29 552.49 555.24 589.83 600.13 656 .11 677.21 703.63 894.95 929.06 964.83 1022.01 1112.89 1166. 69 1177.33 1218.63 1252.45 1381.24 1388.28 1453.82 1595.43 88 104 122 146 146 165 170 182 254 368 414 470 470 535 551 551 583 596 651 671 698 892 922 962 1015 1105 1162 1174 1212 1238 1372 1385 1449 1586 10 1.88E-02 44.2 6 1.06E-02 47.4 8 1.54E-02 52.4 16 4.59E-02 14.8 16 1. 20E-01 6. 8 6 8.93E-03 62.3 12 6.78E-02 14.9 8 3.51E-02 20.8 8 6. 33E-03 91. 8 9 2.40E-02 27.7 9 1. OlE-02 53. 4 17 1.25E-01 5.7 17 3.07E-02 22.3 10 l.22E-02 41.4 9 4.79E-03 36.9 9 6.92E-03 53.1 12 4.69E-02 12:4 9 1.20E-02 34.1 10 1.13E-02 38.3 15 2. 66E-02 21. 6 11 7.45E-02 8.8 7 5.97E-03 33.0 11 3.80E-03101.3 8 5.14E-03 50.1 13 2 .17E-03241.1 11 4.lOE-03 66.5 13 3.00E-02 15.6 7 2.36E-03 89.5 15 5. 13E-02 11. 4 21 1.0lE-02 50.1 12 4.61E-03 56.8 6 2. 71E-03 67. 5 10 1. 02E-02 21. 6 18 8.39E-03 46.8 Fit 4.09E+00 1.25E+OO 3.14E+OO Peak Search Report (continued) Page : 2 Sample ID*: G405235047 Acquisition date 3-0CT-2016 07:00:30 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 877.76 4 17 1. 25 1755.24 1749 8 l.17E-03179 .1 36 0 911. 59* 78 28 1. 93 1822.94 1816 14 2.17E-02 18.5 37 0 922.94 8 5 1. 72 1845.64 1841 7 2.16E-03 60.6 38 0 . 964.31 21 6 1. 90 1928.42 1922 11 5.92E-03 30.5 39 0 969.34* 61 0 2.33 1938.49 1933 13 1. 69E-02 13.8 40 0 1009.53 5 10 0.67 2018.92 2013 8 1.35E-03128.3 41 0 1120.86* 39 18 1. 60 2241.72 2233 14 1.08E-02 28,2 42 0 1154 .11 9 19 0.42 2308.26 2297 13 2.51E-03105.8 43 0 1178.35 18 13 4.77 2356.78 2351 13 5.00E-03 47.5 44 0 1258.31 l6 18 1. 86 2516.80 2509 17 4.57E-03 62.7 45 0 1338.77 5 9 4.35 2677.86 2668 11 1.39E-03133.0 46 0 1460.65* 402 0 1. 98 2921. 82 2913 18 1.12E-01 5.0 47 0 1764.66* 42 4 2.63 3530.46 3523 14 1.17E-02 18.5 Flag: "*" = Peak area was modified by background subtraction Page 3995 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:03:03 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 10:10:00 G405235047 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:00:30 151.35 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA25 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3996 of 5809 PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 279.20 74.66 74.82 74.82 351. 06 CAN . 0 01:00:00.56 10.00 o*. oo % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.13°1E+OO 1.597E+Ol 1.597E+Ol 10.05 OK AS-73 53.44 10.30* 9.638E+OO 2.507E-01 3.366E+OO 94.70 OK CD-109 88.03 3.70* 9.265E+OO 3.424E+OO 5.381E+OO 39.59 OK SN-126 64.28 9.60 9.545E+00 3.905E-01 3.905E-01 104.75 OK* 86.94 8.90 9.265E+00 1.423E+OO 1.423E+OO 39.59 OK 87.57 37.00* 9.265E+00 3.424E-01 3.424E-01 39.59 OK HG-203 70.83 3.69 9.445E+OO Line Not Found Absent 72. 87 6.19 9.424E+OO Line Not Found Absent 279.20 81.56* 4.801E+OO l.447E-02 1. 272E+OO 268.94 OK TL-208 277.37 6.60 4.809E+OO Line Not Found <<INT Reject 583.19 85.00* 2.509E+OO 2.673E-01 2.673E-01 31.22 OK 860.56 12.50 1.810E+00 Line Not Found Absent PB-210 46.54 4.25* 9.157E+00 1.149E+OO 1.179E+OO 88.41 OK PB-212 74.82 10.28 9.404E+OO 4.478E-01 4.478E-01 80.06 OK 77 .11 17.10 9.382E+OO 1. 704E+OO 1.704E+OO 13.54 OK 238.63 43.60* 5.476E+OO 1.083E+OO 1.083E+OO 11. 42 OK 300.09 3.30 4.483E+OO 1. 645E+OO 1.645E+00 68.26 OK BI-214 609.32 45.49* 2.418E+OO 8. 813E-01 8.816E-01 22.84 OK 1120.29 14.92 1.443E+OO 8. 896E-01 8.899E-01 56.43 OK 1764.49 15.30 9.335E-01 1.386E+OO 1.387E+OO 37.02 OK PB-214 74.82 5.80 9.405E+00 Line Not Found <<INT Reject 77.11 9.70 9.382E+OO 3.005E+OO 3.006E+OO 13.54 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.552E+OO 1.135E+OO 1.136E+OO 24. 72 OK 351.93 35.60* 3.893E+00 1.074E+OO 1.074E+OO 17.57 OK RN-222 609.32 45.49* 2.418E+00 8.813E-01 8.816E-01 22.84 OK 1120.29 14.92 1.443E+OO 8.896E-01 8.899E-01 56. 43 OK 1764.49 15.30 9.335E-01 1.386E+OO l.387E+OO 37.02 OK RA-224 240.99 4.10* 5.420E+OO 8.483E-01 8.483E-01 161.11 OK RA-226 609.32 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 OK 1120.29 14.92 l.443E+00 8. 896E-01 8.899E-01 56.43 OK 1764.49 15.30 9.335E-01 1.386E+OO l.387E+OO 37.02 OK AC-228 105. 21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.027E+OO l.176E+OO 1.176E+OO 43.10 OK 794.95 4.25 l.935E+OO Line Not Found Absent 835.71 1. 61 l.856E+OO Line Not Found Absent 911. 20 25.80* 1. 724E+OO 8.859E-01 8.859E-01 37.10 OK 968.97 15.80 l.637E+OO l.177E+OO l.177E+00 27.51 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.027E+OO 1.176E+OO l.176E+OO 43.10 OK 794.95 4.25 1.935E+OO Line Not Found Absent 835. 71 1. 61 l.856E+OO Line Not Found Absent 911.20 25.80* l.724E+OO 8.859E-01 8.859E-01 37.10 OK 968. 97 15.80 l.637E+OO 1.177E+OO l.177E+OO 27.51 OK TH-228. 74.82 10.28 9.404E+OO 4.478E-01 4.478E-01 80.06 OK 77 .11 17.10 9.382E+OO l.704E+OO l.704E+OO 13.54 OK 238.63 43.60* 5.476E+OO l.083E+OO 11. 42 OK 300.09 3.30 4.483E+OO l.645E+OO l.645E+OO 68.26 OK Page 3997 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nucl.ide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status TH-230 609.32 45.49* 2.418E+OO 8.813E-01 8.813E-01 22.84 OK 1120.29 14.92 1.443E+OO 8.896E-01 8. 896E-01 56.43 OK 1764.49 15.30 9.335E-01 1.386E+OO 1.386E+OO 37.02 OK PA-231 283.69 1. 70 4.715E+OO Line Not Found Absent 301".36 5.35* 4.483E+OO 1.014E+OO l.014E+OO 68. 26 OK TH-232 105.21 1.10 8.977E+.00 Line Not Found Absent 338.32 11. 27 4.027E+OO 1.176E+OO 1.176E+OO 43.10 OK 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20. 25.80* l.724E+OO 8.859E-01 8.859E-01 37.10 OK 968.97 15.80 1.637E+OO 1.177E+OO 1.177E+OO 27.51 OK TH-234 63.29 3.70* 9.545E+OO 1. 013E+OO 1.013E+OO 104.75 OK 92. 5*9 4.23 9.202E+OO 2.029E+OO 2.029E+OO 41. 59 OK U-234 609.32 45.49* 2.418E+OO 8. 813E-01 8.813E-01 22.84 OK 1120.29 14.92 1.443E+OO 8. 896E-01 8. 896E-01 56.43 OK 176.4. 4 9 15.30 9.335E-01 1. 386E+OO 1.386E+OO 37.02 OK U-238 63.29 3.10* 9.545E+OO 1. 013E+OO 1.013E+OO 104.75 OK 92.59 4.23 9.202E+OO 2.029E+OO 2.029E+OO 41. 59 OK AM-243 43.53 5.90 8.344E+OO Line Not Found Absent 74.66 67.20* 9.404E+OO 6. 851E-02 6.851E-02 80.06 OK ANH-511 511. 00 100.00* 2.809E+OO l.484E-02 1.484E-02 482.27 OK Flag: "*" = Keyline Page 3998 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:05.02 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l *
Acquisition date 3-0CT-2016 07:00:30 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 7-DEC-2015 10:10:00 Analyst initials: MXRl *
Sample ID G405235047 Sample Quantity 1.5135E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00800 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM )* K-40 1.597E+Ol 1.573E+OO 4.293E-01 AS-73 3.366E+OO 3.124E+OO 2.878E+OO CD-109 5. 381E+OO 2.088E+00 1.045E+OO SN-126 3.424E-01 1. 329E-01 6.644E-02 HG-203 1.272E+OO 3.352E+OO 3.925E+OO TL-208 2.673E-01 8.178E-02 6.899E-02 PB-210 1.179E+00 1.022E+OO 6.320E-01 PB-212 1.083E+OO 1. 212E-01 9.189E-02 BI-214 8.816E-01 1. 97 4E-01 1.195E-01 PB-214 1. 074E+00 1. 849E:-01 1.203E-01 RN-222 8.816E-01 1.974E-01 1.195E-01 RA-224 8.483E-01 1.339E+OO 9.866E-01 RA-226 8.816E-01 1.974E-01 1.195E-01 AC-228 8.859E-01 3.221E-01 2.472E-01 RA-228 8.859E-01 3. 221E-01 2.472E-01 TH-228 1.083E+OO 1.212E-01 9.189E-02 TH-230 8.813E-01 1.973E-01 1.194E-01 PA-231 1.014E+OO 6.786E-01 6.694E-01 TH-232 8.859E-01 3.221E-01 2. 472E-01 TH-234 1.013E+OO 1.040E+OO 7.514E-01 U-234 8.813E-Ol-1.973E-01 l.194E-01 U-238 1.013E+OO 1.040E+OO 7.514E-01 AM-243 6. 851E-02 5.375-E-02 4.420E-02 ANH-511 1.484E-02 7.016E-02 4.474E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM BE-7 -1.498E+OO l.024E+Ol 1. 979E+Ol NOT IDENT. NA-22 l.892E-02 4.591E-02 9.629E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF . AL-2 6 1. 641E-02 1.857E-02 5. 896E-02 NOT IDENT. SC-46 2.375E-01 3.539E-01 7.786E-01 FAIL ABUN V-48 O.OOOE+OO l.554E+04 O.OOOE+OO SHORT HLIF Page 3999 of 5809 CR-51 O.OOOE+OO 3.623E+02 O.OOOE+OO SHORT HLIF MN-54 3 .114E-02 6.194E-02 1. 311E-01 NOT IDENT. C0-56 1.064E-02 4.034E-01 8.232E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.562E-02 3.077E-02 6.282E-02 NOT IDENT. C0-58 5.071E-01 5.222E-Ol l.195E+OO NOT IDENT. FE-59 3.160E-01 7.548E+OO l.493E+Ol NOT IDENT. C0-60 3.414E-02 4.531E-02 9.255E-02 NOT IDENT. ZN-65 l.009E-01 2.076E-01 3.865E-01 NOT IDENT. GE-68 l.277E+OO 2.743E+OO 5.617E+OO NOT IDENT. AS-74 O.OOOE+OO 5.628E+03 O.OOOE+OO SHORT HLIF SE-75 l.437E-01 l.597E-01 3.281E-01 NOT IDENT. BR-77 O.OOOE+OO 2.953E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.800E+02 O.OOOE+OO SHORT HLIF RB-83 3.605E-01 5. 972E-01 l.248E+OO NOT IDENT. KR-85 4.580E-01 6.606E+OO 1.160E+Ol NOT IDENT. SR-85 4.702E-02 7.055E-01 l.238E+OO NOT IDENT. RB-86 O.OOOE+OO 3.500E+04 O.OOOE+OO SHORT HLIF Y-88 6.973E-02 l.498E-01 4.127E-01 NOT IDENT. Y-91 7.802E+Ol 6.323E+02 l.220E+03 NOT IDENT. NB-94 -9.474E-03 3.525E-02 6.307E-02 NOT IDENT. NB-95 1.140E-01 8. 681E-01 1.646E+OO NOT IDENT. NB-95M 3.327E-01 2.338E+OO 4. OllE+OO NOT IDENT. ZR-95 9.346E-01 1.592E+OO 3.205E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 808E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 920E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1'. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.326E-02 2.612E-02 4.489E-02 NOT IDENT. RH-102 -3.004E-02 5.983E-02 9.153E-02 NOT IDENT. RU-103 -5.389E-01 5.149E+OO 9.684E+OO FAIL ABUN RH-106 2.099E-01 4.636E-01 9.457E-01 NOT IDENT. RU-106 2.099E-01 4.636E-01 9.457E-01 NOT IDENT. AG-108M 8.297E-03 2.274E-02 4.695E-02 NOT IDENT. AG-llOM -4.504E-02 9.872E-02 1.840E-01 NOT IDENT. SN-113 9.424E-03 2.025E-01 4.016E-01 NOT IDENT. CD-115 O.OOOE+OO 4.158E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.316E+04 O.OOOE+OO SHORT HLIF TE-123M 4 .133E-02 9.566E-02 l.902E-01 NOT IDENT. SB-124 -1.156E+OO l.636E+OO 2.812E+OO NOT IDENT. SB-125 -1.212E-03 8.542E-02 1.687E-01 FAIL ABUN TE-125M l.087E+02 l.724E+02 3.564E+02 NOT IDENT. I-126 O.OOOE+OO 8.372E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.319E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2. 848E+22 *o.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.385E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.264E+26 0.000E+OO SHORT HLIF BA-133 4.513E-02 3.874E-02 7.902E-02 FAIL ABUN I-133 O.OOOE+OO 1.076E+41 O.OOOE+OO SHORT HLIF CS-134 6.562E-02 5.098E-02 l.153E-01 NOT IDENT. CS-135 9.733E-02 1.108E-01 2.139E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.344E+05 O.OOOE+OO SHORT HLIF BA-137M 5.086E-02 3.696E-02 8.035E-02 NOT IDENT. CS-137 5. 372E-02 3.904E-02 8.488E-02 NOT IDENT. CE-139 3.480E-02 9.004E-02 1. 761E-01 NOT IDENT. BA-140 O.OOOE+OO 1.194E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.190E+05 O.OOOE+OO SHORT HLIF CE-141 -1.922E+Ol 1.915E+Ol 3.371E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 696E+41 O.OOOE+OO SHORT HLIF CE-144 -2.232E-02 2.469E-01 4.765E-01 NOT IDENT. PM-144 -4.633E-02 6.018E-02 8.427E-02 NOT IDENT. PR-144 -4.041E+OO 5.229E+OO 7.316E+OO NOT IDENT. PM-146 l.016E-02 3.492E-02 7.165E-02 NOT IDENT. ND-147 O.OOOE+OO 3. 219E+.07 O.OOOE+OO SHORT HLIF PM-147 3.208E+02 5.398E+02 1.108E+03 NOT IDENT. PM-149 O.OOOE+OO 4.846E+40 O.OOOE+OO SHORT HLIF EU-150 8.107E-03 2.252E-02 4.244E-02 FAIL ABUN EU-152 4.306E-03 8.512E-02 1.540E-01 FAIL ABUN GD-153 -4.498E-02 9.529E-02 1.812E-01 NOT IDENT. EU-154 4.277E-02 1.118E-01 2.336E-01 NOT IDENT. EU-155 5.468E-02 7.004E-02 1.454E-01 NOT IDENT. TB-160 l.515E-01 l.780E+OO 3.262E+OO FAIL ABUN H0-166M 2.706E-03 5.909E-02 1.113E-01 NOT IDENT. TM-171 O.OOOE+OO 6.866E+OO 6.828E+OO FAIL ABUN HF-172 l.406E-01 1.631E-01 3.198E-01 FAIL ABUN LU-172 5.697E-02 8.025E-02 l.724E-01 FAIL ABUN Page 4000 of 5809 LU-176 -4.754E-03 2.189E-02 3.866E-02 FAIL ABUN HF-181 5.741E+OO 5.637E+OO 8.816E+OO FAIL ABUN TA-182 6.906E-02 1.102E+OO 2.lOOE+OO FAIL ABUN RE-183 -3.469E-02 6.934E-01 1.427E+OO NOT IDENT. RE-18.4 1.807E+Ol 2.820E+Ol 6.177E+Ol NOT IDENT. W-188 -5.588E+Ol 1.114E+02 1. 726E+02 FAIL ABUN IR-192 1.113E-01 3.827E-01 7.877E-01 FAIL ABUN BI-207 -1. 804E-02 4.080E-02 7.525E-02 FAIL ABUN BI-211 O.OOOE+OO 5.094E-01 7.673E-01 FAIL ABUN PB-211 4.898E-01 5.806E-01 1.240E+OO NOT IDENT. BI-212 O.OOOE+OO 5.759E-01 l.156E+OO FAIL ABUN RN-219 6.834E-02 3.174E-01 6.423E-01 FAIL ABUN RA-223 1. 866E-02 5.773E-01 1.045E+OO FAIL ABUN AC-227 1. 689E-01 l.997E-01 3.983E-01 FAIL ABUN TH-227 1. 689E-01 l.997E-01 3.983E-01 FAIL ABUN TH-229 2.414E-01 3.557E-01 7 .116E-01 FAIL ABUN TH-231 1. 866E-02 5.773E-01 l.045E+OO FAIL ABUN PA-233 6.112E-03 4. 972E-02 1.007E-01 FAIL ABUN PA-234 2.434E-01 2.739E-01 6.077E-01 NOT IDENT. PA-234M 2. 972E+OO 4.197E+OO 9.205E+OO NOT IDENT. U-235 6.915E-02 1. 391E-01 2.752E-01 FAIL ABUN NP-237 6 .112E-03 4. 972E-02 l.007E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1.134E-01 1.602E-01 FAIL ABUN PU-239 2.625E+02 4. 723E+02 4.801E+02 FAIL ABUN AM-241 -2.899E-02 3.793E-02 6.903E-02 NOT IDENT. CM-243 -1.313E-03 5.876E-02 1.166E-01 FAIL ABUN BK-247 4.518E-02 5.654E-02 l.144E-01 FAIL .ABUN CM-247 5.547E-03 3.083E-02 6 .176E-02 FAIL ABUN CF-249 8.787E-03 3.316E-02 6.707E-02 NOT IDENT. CF-251 -4.824E-02 9.093E-02 l.641E-01 NOT IDENT. Page 4001of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:.03:02.14 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 388 10.66* l.131E+OO 1.597E+Ol 1.597E+Ol 10.05 AS-73 53.44 50 10.30* 9.638E+OO 2.507E-01 3.366E+OO 94.70 CD-109 88.03 309 3.70* 9. 2 65E+OO 4.470E+OO 7.025E+OO 29.77 SN-126 64.28 72 *9.60 9.545E+OO 3.905E-01 3.905E-01 104.75 86.94 309 8.90 9.265E+OO 1.858E+OO 1.858E+OO 29.77 87.57 309 37.00* 9.265E+OO 4.470E-01 4.470E-01 29.77 HG-203 70.83 ------3.69 9.445E+OO ------Line Not Found ------72. 87 ------6.19 9.424E+OO ------Line Not Found ------279.20 28 81.56* 4.801E+OO 3.609E-02 3.174E+OO 106.15 TL-208 277.37 28 6.60 4.801E+OO 4.460E-01 4.460E-01 106.15 .583 .19 115 85.00* 2.509E+OO 2.673E-01 2.673E-01 31. 22 860.56 ------12.50 1.810E+OO ------Line Not Found ------PB-210 46.54 90 4.25* 9.157E+OO 1.149E+OO 1.179E+00 88.41 BI-211 72.87 ------1. 23 9.424E+OO ------Line Not Found ------351. 06 300 12.92* 3.893E+00 2.959E+OO 2.959E+00 17.57 PB-212 74:82 212 10.28 9.404E+OO 1.088E+OO l.088E+OO 29.55 77 .11 551 17.10 9.382E+OO 1. 704E+OO 1. 704E+OO 13.54 238.63 521 43.60* 5.476E+OO l.083E+OO l.083E+00 11. 42 300.09 49 3.30 4.483E+OO l.645E+00 l.645E+OO 68.26 BI-214 609.32 195 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 1120.29 39 14.92 1.443E+OO 8.896E-01 8.899E-01 56.43 1764.49 40 15.30 9.335E-01 1.386E+OO l.387E+OO 37.02 PB-214 74.82 212 5.80 9.404E+00 1.929E+OO l.930E+00 29.55 77 .11 551 9.70 9.382E+OO 3.005E+OO 3.006E+OO 13.54 87.09 309 3.41 9.265E+OO 4.850E+00 4.852E+OO 29.77 242.00 128 7.25 5.420E+OO l.615E+OO l.616E+OO 44.59 295.22 192 18.42 4.552E+OO l .135E+OO 1.136E+OO 24.72 351. 93 300 35.60* 3.893E+OO 1.074E+OO 1.074E+OO 17.57 RN-222 609.32 195 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 1120.29 39 14.92 1.443E+OO 8.896E-01 8.899E-01 56.43 1764.49 40 15.30 9.335E-01 1. 38 GE+OO 1.387E+00 37.02 RA-224 240.99 128 4.10* 5.420E+OO 2.856E+OO 2.856E+OO 44. 5*9 RA-226 609.32 195 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 1120.29 39 14.92 l.443E+OO 8.896E-01 8.899E-01 56.43 1764.49 40 15.30 9.335E-01 1. 38 6E+OO 1.387E+OO 37.02 AC-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 108 11.27 4.027E+OO 1.176E+OO 1.176E+OO 43.10 794.95 ------4.25 1.935E+OO ------Line Not Found ------835.71 ------1. 61 l.856E+OO ------Line Not Found ------911.20 79 25.80* 1. 724E+OO 8.859E-01 8.859E-01 37.10 968. 97 61 15.ffO l.637E+OO 1. l 77E+OO l.177E+OO 27.51 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32" 108 11.27 4.027E+OO l.176E+OO 1.176E+OO 43.10 794.95 ------4.25 l.935E+OO ------Line Not Found ------835.71 ------1. 61 l.856E+OO ------Line Not Found ------911.20 79 25.80* 1. 724E+OO 8.859E-01 8.859E-01 37.10 968. 97 61 15.80 l.637E+OO 1. l 77E+OO l.177E+OO 27.51 Page 4002 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235047 Acquisition date Page : 2 3-0CT-2016 07:00:30 Nuclide Type: Nuclide TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Flag: "*" Page 4003 of 5809 Energy 74.82 77 .11 238.63 300.09 609.32 1120.29 1764.49 283.69 301.36 105.21 338.32 835. 71 911. 20 968. 97 63.29 92.59 609.32 1120.29 1764.49 63.29 92.59 43.53 74.66 511. 00 Key line Area 212 551 521 49 195 39 40 49 108 79 61 72 159 195 39 40 72 159 212 8 %Abn 10.28 17.10 43.60* 3.30 45.49* 14.92 15.30 1. 70 5.35* 1.10 11. 27 1. 61 25.80* 15.80 3.70* 4.23 45.49* 14.92 15.30 3.70* 4.23 5.90 67.20* 100.00* %Eff 9.404E+OO 9.382E+00 5.476E+OO 4.483E+OO 2.418E+OO l.443E+OO 9.335E-01 4.715E+OO 4.483E+OO 8.977E+OO 4.027E+OO 1.856E+OO 1. 724E+OO 1.637E+OO 9.545E+OO 9.202E+OO 2.418E+OO 1.443E+OO 9.335E-01 9.545E+OO 9.202E+00 8.344E+OO 9.404E+OO 2.809E+OO Uncorrected Decay Corr pCi/GRAM pCi/GRAM 1.088E+00 1.088E+OO 1.704E+OO 1.704E+OO 1.083E+OO 1.083E+OO 1.645E+OO l.645E+OO 8.813E-01 8.813E-01 8.896E-Dl 8.896E-01 1.386E+OO 1.386E+OO ------Line Not Found 1.014E+OO 1.014E+OO ------Line Not Found 1.176E+OO l.176E+OO ------Line Not Found 8.859E-01 8.859E-01 1.177E+OO 1.177E+OO 1.013E+OO 1.013E+OO 2.029E+OO 2.029E+OO 8.813E-01 8.813E-01 8.896E-01 8.896E-01 1.386E+OO 1.386E+OO 1.013E+OO 1.013E+OO 2.029E+OO 2.029E+OO ------Line Not Found l.665E-01 l.665E-01 l.484E-02 l.484E-02 2-Sigma %Error 29.55 13.54 11. 42 68.26 22.84 56.43 37.02 68.26 43.10 37.10 27.51 104.75 41.59 22.84 56.43 37. 02' 104.75 41. 59 29.55 482.27 Summary of Nuclide Activity Sample ID : G405235047 Acquisition date Page : 3 3-0CT-2016 07:00:30 Total number of lines in spectrum 47 Number of unidentified lines 11 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 , RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 80.30D 461.40D 2.30E+05Y 46.59D 1. 41E+10Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+l0Y 1.41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1. 00E+09Y Decay 1. 00 13.4 1. 57 1. 00 87.9 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. od 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.597E+Ol 2.507E-01 4.470E+OO 4.470E-01 3.609E-02 2.673E-01 1.149E+OO 2.959E+OO 1.083E+OO 8.813E-01 1.074E+OO 8.813E-01 2.856E+OO 8. 813E-01 8.859E-01 8.859E-01 1.083E+OO 8.813E-01 1.014E+OO 8.859E-01 1. 013E+OO 8.813E-01 1.013E+OO 1.665E-01 1.484E-02 4.193E+Ol 4.193E+Ol Decay Corr pCi/GRAM 1.597E+Ol 3.366E+OO 7.025E+OO 4.470E-01 3.174E+OO 2.673E-01 1.179E+OO 2.959E+OO 1.083E+OO 8.816E-01 1.074E+OO 8.816E-01 2.856E+OO 8.816E-01 8.859E-01 8.859E-01 1.083E+OO 8.813E-01 1.014E+OO 8.859E-01 1.013E+OO 8. 813E-01 1.013E+OO l.665E-01 1.484E-02 5.077E+Ol 5.077E+Ol 76.60% Decay Corr 2-Sigma Error 0.160E+Ol 3.188E+OO 2. 091E+OO 1. 331E-01 3.369E+OO 0.834E-01 l.043E+OO 0.520E+OO 0.124E+OO 2.014E-01 0.189E+OO 2.014E-01 l.273E+OO 2.014E-01 3.286E-01 3.286E-01 , 0.124E+OO 2.013E-01 0.692E+OO 3.286E-01 1.061E+OO 2.013E-01 1.061E+OO 0.492E-01 7.159E-02 "M" Manually accepted 2-Sigma %Error 10.05 94.70 29.77 29.77 106.15 31. 22 88.41 17.57 11. 42 22.84 17.57 22.84 44.59 22.84 37.10 37.10 11. 42 22.84 68. 26 37.10 104.75 22.84 104.75 29.55 482.27 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4004 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235047 Acquisition date : 3-0CT-2016 07:00:30 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.83 41 181 1.14 167.14 165 6 .8. 93E-03 **** 9.32E+OO T 0 129.09 28 169 0.78 257.66 254 8 6.33E-03 **** 8.36E+OO T 0 186.02 103 159 1.12 371.50 368 9 2.40E-02 55.3 6.69E+OO T 0 209.42 43 125 0.99 418.30 414 9 l.OlE-02 **** 6.lOE+OO T 0 270.41 50 95 0.79 540.29 535 10 1.22E-02 82.9 4.92E+OO T 4 276.52 20 14 0.83 552.49 551 9 4.79E-03 73.7 4.82E+OO T 0 328.32 46 66 2.39 656 .11 651 10 1.13E-02 76.5 4.14E+OO T 0 447.74 23 11 2.19 894.95 892 7 5.97E-03 66.0 3.15E+OO 0 464.79 15 54 0.90 929.06 922 11 3;80E-03 **** 3.05E+OO T 0 482.67 20 25 1. 77 964. 83 962 8 5.14E-03 **** 2.95E+OQ T 0 556.69 16 23 0.64 1112.89 1105 11 4.lOE-03 **** 2*.61E+OO 0 588.90 9 20 1. 25 1177.33 1174 7.2.36E-03 **** 2.49E+OO 0 626.45 38 47 7.10 1252.45 1238 21 l.OlE-02 **** 2.36E+OO 0 690.83 17 19 2.00 1381.24 1372 12 4.61E-03 **** 2.18E+OO 0 694.35 10 14 1. 38 1388.28 1385 6 2.71E-03 **** 2.17E+OO T 0 727 .11 38 8 1. 72 1453.82 1449 10 l.02E-02 43.1 2.09E+OO T 0 797.89 31 29 5.52 1595.43 1586 18 8.39E-03 93.6 1. 93E+OO 0 877.76 4 17 1. 25 1755.24 1749 8 1.17E-03 **** 1. 78E+00 0 922.94 8 5 1. 72 1845.64 1841 7 2.16E-03 **** 1. 71E+OO T 0 964. 31 22 6 1. 90 1928.42 1922 11 5.92E-03 61.0* 1.64E+OO *T 0 1009.53 5 10 0.67 2018. 92 2013 8 1.35E-03 **** 1. 58E+OO 0 1154 .11 9 19 0.42 2308.26 2297 13 2.51E-03 **** I. 41E+OO 0 1178.35 18 13 4.77 2356.78 2351 13 5.00E-03 95.1 l.38E+OO T 0 1258.31 16 17 1. 86 2516.80 2509 17 4.57E-03 **** 1. 30E+OO 0 1338.77 5 9 4.35 2677.86 2668 11 l.39E-03 **** l.23E+00 Flags: "T" = associated Page 4005 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:19.19 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l *
Acquisition date 3-0CT-2016 07:00:30 Sensitivity * : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
live time:. 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00.:00.56 Half life ratio : ***** *
Sample date 7-DEC-2015 10:10:00 Nuclide Library : SOLID *
Sample ID G405235047 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.5135E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 HG-203 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 58 6E-01 1.341E+OO 4.897E-01 3 .112E-02 l.804E+00 3.126E-02 2. 967E-01 4.300E-02 5.348E-02 5.512E-02 5.348E-02 4.618E-01 5.348E-02 1.083E-01 *l.083E-01 4.300E-02 5.346E-02 3.054E-01 1.083E-01 3.552E-01 5.346E-02 3.552E-01 2.096E-02 1.991E-02 ----Nuclides Nuclide BE-:-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4006 of 5809 Le (pCi/GRAM 8. 772E+OO 4.158E-02 O.OOOE+OO 2.207E-02 3.426E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 .SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101'. RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131
I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 . BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4007 of 5809 5.836E-02 3.561E-01 O.OOOE+OO 2.931E-02 5.290E-01 6.575E+OO 4.017E-02 1. 715E-01 2.504E+OO O.OOOE+OO 1.505E-01 O.OOOE+OO O.OOOE+OO . 5. 613E-01 5.199E+OO 5.549E-01 O.OOOE+OO l.528E-01 5.420E+02 2.833E-02 7.335E-01 l.873E+OO 1. 440E+00 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 096E-02 3. 966E-02 4.306E+OO 4.217E-01 4.217E-01 2. llOE-02 7 .. 97 6E-02 1.823E-01 O.OOOE+OO O.OOOE+OO 8.857E-02 9.427E-01 7. 561E-02 1.669E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.643E-02 O.OOOE+OO 5.220E-02 9.808E-02 0.000E+OO O.OOOE+OO 3.673E-02 3.880E-02 8.247E-02 0.000E+OO O.OOOE+OO 1.571E+Ol O.OOOE+OO 2.220E-01 3.646E-02 3.164E+OO 3.202E-02 O.OOOE+OO 5.177E+02 O.OOOE+OO 1. 941E-02 7. 013E-02 8.412E-02 l.007E-01 6.846E-02 1.403E+00 4.969E-02 3.197E+00 1. 498E-01 7.630E-02 1. 763E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. .NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-22-7 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Pa'ge 4008 -0f 5809 4.009E+OO 9.341E-01 6.703E-01 2. 715E+Ol 7.878E+Ol 3.605E-01 3.148E-02 3.700E-01 5.664E-01 5.288E-01 2.907E-01 4.807E-01 1.848E-01 1.848E-01 3. 311E-01 4.807E-01 4.615E-02 2.699E-01 4.094E+OO 1.294E-01 4.615E-02 O.OOOE+OO 1. 551E-01 2.265E+02 3.240E-02 5.442E-02 5.254E-02 2.809E-02 3.058E-02 7.613E;-02 FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0.CT-2016 08: 03: 24. 87 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l *
Acquisition date 3-0CT-2016 07:00:30 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
Sample date 7-DEC-2015 10:10:00 Nuclide Library : SOLID *
Sample ID G405235047 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.5135E+02 GRAM *
Quantity Err ( % ) 1. 3214E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 '08:41:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.597E+Ol 1.780E+OO 1. 780E+OO AS-73 3.366E+OO 3.200E+OO 3.200E+OO CD-109 5. 381E+OO 2.143E+OO 2.143E+OO SN-126 3.424E-01 l.352E-01 1.352E-01 HG-203 1.272E+OO 3.359E+OO 3.359E+OO TL-208 2.673E-01 8.256E-02 8.256E-02 PB-210 1.179E+OO 1. 026E+OO 1.026E+OO PB-212 l.083E+00 1. 341E-01 1.341E-01 BI-214 8.816E-01 2.0lOE-01 2.0lOE-01 PB-214 l.074E+00 1.902E-01 1.902E-01 RN-222 8.816E-01 2.0lOE-01 2.0lOE-01 RA-224 8.483E-01 1.347E+OO 1. 347E+OO RA-226 8.816E-01 2.0lOE-01 2.0lOE-01 AC-228 8.859E-01 3.252E-01 3.252E-01 RA-228 8.859E-01 3.252E-01 3.252E-01 TH-228 1.083E+OO 1. 341E-01 1. 341E-01 TH-230 8. 813E-01 2.009E-01 2.009E-01 PA-231 1.014E+OO 7.123E-01 7.123E-01 TH-232 8.859E-01 3.252E-01 3.252E-01 TH-234 1. 013E+OO 1.064E+OO 1. 064E+OO U-234 8.813E-01 2.009E-01 2.009E-01 U-238 1.013E+OO 1.064E+OO 1.064E+OO AM-243 6.851E-02 5.532E-02 5.532E-02 ANH-511 l.484E-02 7.016E-02 7.016E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 -1.498E+OO l.024E+Ol 1.026E+Ol NOT IDENT. NA-22 1.892E-02 4.592E-02 4.671E-02 NOT IDENT. NA-24 -1.000E+41 2.491E+41 O.OOOE+OO SHORT HLIF AL-26 1.641E-02 1.860E-02 2.00lE-02 NOT IDENT. SC-46 2.375E-01 3.540E-01 3.699E-01 FAIL ABUN V-48 5.650E+03 1.554E+04 1.575E+04 SHORT HLIF Page 4009 of 5809 CR-51 -3.670E+02 3.627E+02 3.986E+02 SHORT HLIF MN-54 3 .114E-02 6.196E-02 6.353E-02 NOT IDENT. C0-56 1.064E-02 4.034E-01 4.035E-01 NOT IDENT. MN-56 1.000E+41 4.464E+42 O.OOOE+OO SHORT HLIF C0-57 1.562E-02 3.077E-02 3.157E-02 NOT IDENT. C0-58 5.071E-01 5. 227E-01. 5.705E-01 NOT IDENT. FE-59 3.160E-01 7.548E+OO 7.550E+OO NOT IDENT. C0-60 3.414E-02 4.533E-02 4.787E-02 NOT IDENT. ZN-65 1.009E-01 2.076E-01 2.126E-01 NOT IDENT. GE-68 1.277E+OO 2.743E+OO 2.803E+OO NOT IDENT. AS-74 1. 744E+03 5.630E+03 5.684E+03 SHORT HLIF SE-75 1.437E-01 1.598E-01 1.725E-01 NOT IDENT. BR-77 2.638E+38 2.291E+39 O.OOOE+OO SHORT HLIF SR-82 2.920E+02 6.801E+02 6.927E+02 SHORT HLIF RB-83 3.605E-01 5.992E-01 6.209E-01 NOT IDENT. KR-85 4.580E-01 6.606E+OO 6.609E+OO NOT IDENT. SR-85 4.702E-02 7.055E-01 7.058E-01 NOT IDENT. RB-86 1.543E+04 3. 501E+04 3.569E+04 SHORT HLIF Y-88 6.973E-02 1.498E-01 1.531E-01 NOT IDENT. Y-91 7.802E+Ol 6.323E+02 6.333E+02 NOT IDENT. NB-94 -9.474E-03 3.525E-02 3. 551E-02 NOT IDENT. NB-95 1.140E-01 8. 681E-01 8. 696E-01 NOT IDENT. NB-95M 3.327E-01 2.339E+00 2.343E+OO NOT IDENT. ZR-95 9.346E-01 1. 593E+OO l.648E+00 NOT IDENT. NB-97 -1.000E+41 1. 809E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 2.320E+41 O.OOOE+OO SHORT HLIF M0-99 1.127E+32 1. 921E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 3.386E+41 O.OOOE+OO SHORT HLIF RH-101 -1.326E-02 2.623E-02 2.691E-02 NOT IDENT. RH-102 -3.004£-02 5.988E-02 6.139E-02 NOT IDENT. RU-103 -5.389E-01 5.149E+OO 5.155E+OO FAIL ABUN RH-106 2.099E-01 4.638E-01 4.733E-01 NOT IDENT. RU-106 2.099E-01 4.638E-01 4.733E-01 NOT IDENT. AG-108M 8.297E-03 2.274E-02 2.305E-02 NOT IDENT. AG-110M -4.504E-02 9.874E-02 1.008E-01 NOT IDENT. SN-113 9.424E-03 2.025E-01 2.025E-01 NOT IDENT. CD-115 3.397E+37 4.158E+39 O.OOOE+OO SHORT HLIF SN-117M 2.569E+04 7.323E+04 7.414E+04 SHORT HLIF TE-123M 4.133E-02 9.568E-02 9.747E-02 NOT JDENT. SB-124 -1.156E+OO. 1.637E+OO l.718E+OO NOT IDENT. SB-125 -1.212E-03 8.542E-02 8.542E-02 FAIL ABUN TE-125M 1.087E+02 1.725E+02 1. 7 93E+02 NOT IDENT. I-126 3.238E+05 8.383E+05 8.510E+05 SHORT HLIF SB-126 -3.794E+04 1.319E+06 1.319E+06 SHORT HLIF SB-127 -8.473E+21 3.079E+22 O.OOOE+OO SHORT HLIF I-131 1.985E+09 4.386E+09 4.477E+09 SHORT HLIF I-132 -1.000E+41 2.025E+42 O.OOOE+OO SHORT HLIF TE-132 1.425E+26 4.303E+26 0.000E+OO SHORT HLIF BA-133 4. 513E-02 3.879E-02 4.380E-02 FAIL ABUN I-133 1.000E+41 2.110E+41 O.OOOE+OO SHORT HLIF CS-134 6.562E-02 5.105E-02 5. 901E-02 NOT IDENT. CS-135 9.733E-02 1.llOE-01 1.194E-01 NOT IDENT. I-135 1.000E+41 8.825E+41 0.000E+OO SHORT HLIF CS-136 9.445E+04 3.345E+05 3.372E+05 SHORT HLIF BA-137M 5.086E-02 3.702E-02 4.354E-02 NOT IDENT. CS-137 5.372E-02 3. 911E-02 4.600E-02 NOT IDENT. CE:._139 3.480E-02 9. 031E-02 9.167E-02 NOT IDENT. BA-140 -6.689E+04 1.194E+06 1.194E+06 SHORT HLIF LA-140 -3.217E+05 4.193E+05 4.436E+05 SHORT HLIF CE-141 -1.922E+Ol 1.917E+Ol 2.103E+Ol NOT IDENT. CE-143 1.000E+41 1.699E+41 O.OOOE+OO SHORT HLIF CE-144 -2.232E-02 2.469E-01 2. 471E-01 NOT IDENT. PM-144 -4.633E-02 6.025E-02 6.377E-02 NOT IDENT. PR-144 -4.041E+00 5.232E+OO 5.540E+OO NOT IDENT. PM-146 l.016E-02 3.493E-02 3.523E-02 NOT IDENT. ND-147 -1.229E+06 3.219E+07 3.219E+07 SHORT HLIF PM-147 3.208E+02 5.400E+02 5.590E+02 NOT IDENT. PM-149 -1. 7 62E+40 4.862E+40 O.OOOE+OO SHORT HLIF EU-150 8.107E-03 2.253E-02 2.282E-02 FAIL ABUN EU-152 4.306E-03 8.512E-02 8. 51°4E-02 FAIL ABUN GD-153 -4.498E-02 9.532E-02 9.746E-02 NOT IDENT. EU-154 4.277E-02 1. 118E-01 1.134E-01 NOT IDENT. EU-155 5.468E-02 7.015E-02 7.435E-02 NOT IDENT. TB-160 1.515E-01 1. 780E+OO 1. 781E+OO FAIL ABUN H0-166M 2.706E-03 5.909E-02 5.910E-02 NOT IDENT. TM-171 7.398E+OO 6. 8 96E+OO 7.660E+OO FAIL ABUN HF-172 l.406E-01 1. 64 7E-01 l.764E-01 FAIL ABUN LU-172 5.697E-02 8.045E-02 8.445E-02 FAIL ABUN Page 4010 of 5809 LU-176 -4.754E-03 '2.190E-02 2.200E-02 FAIL ABUN HF-181 5.741E+OO 5.643E+OO 6.208E+OO FAIL ABUN TA-182 6.906E-02 1.102E+OO 1.102E+OO FAIL ABUN RE-183 -3.469E-02 6.934E-01 6.936E-01 NOT IDENT. RE-184 "l.807E+Ol 2.853E+Ol 2. 967E+Ol NOT IDENT. W-188 -5.588E+Ol l. ll6E+02 l.144E+02 FAIL"ABUN IR-192 l .113E-Ol 3.827E-01 3.860E-01 FAIL ABUN BI-207 -l.804E-02 4.081E-02 4.161E-02 FAIL ABUN BI-2ll 2.959E+OO 5.262E-01 l.434E+OO FAIL ABUN PB-2ll 4.898E-Ol 5.811E-01 6.217E-01 NOT IDENT. BI-212 1. 362E+OO 5.800E-01 8.448E-01 FAIL ABUN RN-219 6.834E-02 3.175E-01 3.190E-01 FAIL ABUN RA-223 1. 8 66E-02 5.773E-01 5.774E-01 FAIL ABUN AC-227 1. 689E-Ol 2.0lOE-01 2.149E-01 FAIL ABUN TH-227 1. 689E-Ol 2.0lOE-01 2.149E-01 FAIL ABUN TH-229 2.414E-Ol 3.559E-01 3.722E-01 FAIL ABUN TH-231 1. 8 66E-02 5.773E-01 5.774E-01 FAIL ABUN PA-233 6.112E-03 4.973E-02 4.980E-02 FAIL ABUN PA-234 2.434E-01 3.906E-01 4.057E-01 NOT IDENT. PA-234M 2. 972E+OO 4.199E+OO 4.407E+OO NOT. IDENT. U-235 6.915E-02 l.392E-01 l.426E-01 FAIL ABUN NP-237 6.112E-03 4.973E-02 4.980E-02 FAIL ABUN NP-238 -l.OOOE+41 2.115E+41 O.OOOE+OO SHORT HLIF NP-239 1.134E-01 l.605E-01 l.684E-01 FAIL ABUN PU-239 2.625E+02 4. 724E+02 4.870E+02 FAIL ABUN AM-241 -2.899E-02 3.799E-02 4.018E-02 NOT* I DENT. CM-243 -1.313E-03 5.876E-02 5.876E-02 FAIL ABUN BK-247 4.518E-02 5. 727E-02 6.078E-02 FAIL ABUN CM-247 5.547E-03 3.085E-02 3.095E-02 FAIL ABUN CF-249 8.787E-03 3.316E-02 3.340E-02 NOT IDENT. CF-251 -4.824E-02 9.109E-02 9.365E-02 NOT IDENT. Page 4011 of 5809
GEL Laboratories LLC *
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Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 80.6820 87.09 73.3472 136.47 50.2703 45.60 78.6121 87.57 73.4542 140.51 . 0.0000 46.54 78.9743 88.03 73.5565 143.76 60.8629 49. 72 0.0000 88.34 73.6254 144.24 63.8713 51. 35 58.3366 88.47' 73.6543 145.44 76.8336 51. 87 76.4654 89. 96 73.9830 152.43 72.9209 52.39 74.1385 1093.63 60.3400 153.25 0.0000 52.97 61. 77 40 91.11 0.0000 323.87 71.1712 53.44 61. 9020 92.59 69.3549 156.02 0.0000 54.07 62.0727 93.35 69.5074 158.56 0.0000 57.36 0.0000 94.56 68.5873 159.00 52.6070 57.53 80.6626 94.65 67.4419 162.33 53.9567 57.98 76.1945 94.67 67.4460 162.66 0.0000 59.27 93.8785 94.87 67.4844 163.33 63.2365 59.32 93.8974 97.43 62.4067 165.86 64.5573 59.54 93.9817 98.43 67.8691 176.31 54.2923 60. 96 93.4804 98.44 67.8708 176.60 0.0000 61.17 93.5587 99.53 49.5093 177.52 66. 9619 62.93 99.7037 100 .11 61.0994 181.07 0.0000 63.29 99.8432 102.03 63.1992 181.52 66.3713 63.58 99.9551 103.18 66.0728 184.41 79.0491 64.28 113. 6404 103.37 66.1067 143.76 67.9053 66.73 108.3242 105.21 67.3273 193.51 46.2137 67.24 101.3475 105.31 67.3450 197.03 59.4463 125.81 101.5122 *106.12 69.2878 198.01 58.4561 67.75 99.1398 106.47 70.2519 201.83 55.5423 69.67 89.3703 109.28 58. 9692 203.43 57.8652 70.83 112. 3797 111. 00 76.5396 205.31 58.3993 72.81 117.2373 111.76 0.0000 210.85 54.4777 72.87 130.2905 114. 06 73.4540 215.65 55.6122 74.66 112. 253'2 116. 30 0.0000 222 .11 64.0015 74.82 112.3138 116.74 59.1504 227.09 47. 4967 74.97 112.3713 119.76 68.8906 227.38 50.9106 77 .11 113.1866 121.12 55.1032 228.16 0.0000 78.74 113.7991 121.22 55 .1162 228.18 52.1010 79.69 114 .1534 121. 78 57.9949 116.74 52.1010 80.12 114. 3133 122.06 54.2892 235.69 62.5702 80.19 0.0000 122.92 64. 7154 235. 96 62.5936 80.57 80.2192 123.07 65.6763 238.63 71.2504 81. 00 87.0248 265.00 75.1648 238.98 0.0000 81. 07 87.0446 125.81 52.8743 240.99 71.4794 81. 75 87.2343 127.23 79.5671 242.00 71. 57 68 83.79 77.6685 127.91 70.8360 244.70 50.9811 84.00 77. 7198 129.30 71. 3745 252.40 0.0000 85.43 95.0375 131. 20 67.5364 252.80 40.9889 86.55 73.2265 133. 02 60.4506 254.15 0.0000 86.79 73.2796 133.52 64.3593 256.23 38.8184 86.94 73.3138 136.00 53 .1168 260.90 0.0000 Page 4012 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 26.1572 355.39 0.0000 584.27 31. 4380 264.80 32.1078 356.01 26.2988 595.83 0.0000 265.00 28.5476 364.49 0.0000 427.87 25. 4111 268.22 25.4772 366.42 0.0000 602.52 0.0000 269.46 26.3137 372.51 32.0618 604. 72 19.1067 270.03 26.3325 375.05 34.8161 607.14 27.1083 271.23 26.3714 377.52 28.6328 609.32 24.4843 273.65 0.0000 356.01 39.6011 610.33 24.4993 276.40 36.9922 388.16 31.6248 614.28 24.0244 277.37 41.0609 388.63 0.0000 618.01 25.6846 277.60 41. 0723 391.69 31. 7259 620.36 17.6830 278.00 41.0920 264.66 '25. 5841 621. 93 17.1634 279.20 43.5718 401.81 27. 4396 630.19 0.0000 279.54 35.5173 402.40 31.1141 631. 29 21.0361 279.70 35.5244 404.85 24.7615 633.25 24.8409 280.46 40.4053 410.95 31.3472 634.78 0.0000 283.69 31.6375 413.71 28.6494 635.95 24.8802 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 26. 8246 423. 72 0.0000 645.85 19.5850 285.90 0.0000 427.09 28.9761 657.76 27.3905 287.50 34.2241 427.87 25.2537 657.90 0.0000 290.67 47.4365 433.94 21.6210 661. 66 17.5690 293.27 0.0000. 439.40 25.4949 664.57 0.0000 351. 93 36.1752 453.88 20*. 0618 666.33 0.0000 295. 96 36.2057 463.37 15.3997 666.50 0.0000 879.38 19.8076 468.07 20.2861 667.71 0.0000 299.98 28.1051 473.00 0.0000 677.62 19.9446 300.09 28.1085 475.06 24.2803 685.70 0.0000 300.13 28.1099 476.78 17.5045 695.00 0.0000 301.36 36.4277 477.60 22.3809 696. 49 25 .1917 302.85 31.5128 482.18 20.5057 696. 51 25.1926 256.23 23.2627 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 21.8431 306.78 39.9805 497.08 21.7216 697.49 21. 8447 308.46 33.3789 505.52 23.8423 702.65 30.3322 311. 90 38.5308 507.63 0.0000 706.68 21.3912 316.51 34.5145 511. 00 21. 9418 711. 68 22.5781 319.41 0.0000 514.00 23.9873 720. 70 0.0000 320.08 0.0000 514.00 23.9883 721. 93 0.0000 321. 04 39.7586 520.40 19.0765 722. 78 20.4404 323.87 40.7266 520.69 0.0000 722.91 20.4419 325.23 43.3342 522.65 0.0000 723. 31 15.3347 328.76 0.0000 527.90 0.0000 724.19 17.0465 333.37 29.5642 528.26 27.2593 727. 33 19.3512 333.97 32.1548 529.59 17.1785 733.00 14.8424 ( 334.37 28.3077 529.87 0.0000 735.93 14.8646 338.28 34.4507 531.02 0.0000 333.97 13. 7324 338.32 34.4515 537.26 0.0000 739.50 0.0000 311. 90 34.5272 546.56 0.0000 747.24 19.5525 340.48 34.5272 552.55 16.9364 748.06 16.1089 340.55 0.0000 563.25 16.5404 752.31 24.2163 344.28 33.7941 569.33 29.0618. 753.82 0.0000 345.93 32.9817 946.00 30.1021 75,6.73 18.4922 351.06 40.1293 569.70 32.1832 756.80 18.4928 351. 93 40.1639 583.19 31. 4172 884.68 28.9998 Page 4013of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS *ENERGY MDA COUNTS 765.81 20.8989 1274.44 13.5108 1620.50 4.7026 766.42 23.2284 1001.03 10.6358 1621. 92 6.5861 766.84 20.9099 1002.74 17.6920 1678.03 0.0000 772.60 0.0000 1004.73 23.2390 1690.97 4.7864 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1. 9488 778.90 20.1594 1028.54 0.0000 1063.66 17.5641 783.70 0.0000 1037.84 12.7509 1771.35 1.9521 785.37 19.3447 1038.76 0.0000 1791.20 0.0000 792.07 15. 52 68 631.29 15.7461 1808.65 0.0000 794.95 14.1348 1048.07 0.0000 1810. 72 0.0000 795.86 14 .1411 1049.04 9.8505 1836.06 0.9908 810.06 14.2383 1050.41 10.8409 810.29 12.4598 1063.66 12.8762 344.28 12. 4611 1077.00 0.0000 810.76 9.7922 1077.34 16.9243 815.77 0.0000 1085.87 9.9872 1048.07 0.0000 1093.63 12.0183 832.01 19.7817 1099.45 15.0549 834.85 '16.2065 1112. 07 18.1494 835.71 16.2131 1112.84 28.2393 836.80 0.0000 1115. 54 14.5371 846.75 0.0000 1120.29 15.1685 8'46.77 13.5800 1120.55 15.1703 856.80 0.0000 1221.41 9. 7113 860.56 13.6661 1129. 67 7.1025 871.09 17.0876 1131. 51 0.0000 873.19 11. 7281 1147.95 0.0000 875.33 0.0000 1173.23 11. 5384 879.38 11. 7 605 1177.95 18.5735 880.51 13.2372 1189.05 15.5365 883.24 14.7261 1204.77 19.7839 884.68 19.3401 1221.41 20.9412 889.28 11. 0739 1231. 02 16.8066 894.76 13.8757 1235.36 0.0000 898.04 16.6750 1238.28 17.8996 900. 72 21. 3316 1260.41 0.0000 903.28 11.1420 1271. 87 11.7083 911.20 16.7701 1274.44 9. 5872 912.08 16.7767 1274.54 9.5878 923.98 0.0000 1291. 59 9.6394 926.50 10.5034 1298.22 0.0000 929 .11 17.8380 1312 .11 0.0000 937.49 16.9590 1332.49 6.9422 944.13 0.0000 1362.66 0.0000 946.00 11.3463 1365.19 7.6686 949.00 21.7738 1368.63 0.0000 667.71 0.0000 1384.29 6.6105 962. 31 16.7535 1408.01 5.5472 964. 08 9.1450 1457.56 0.0000 966 .17 0.0000 1460.82 2.7032 911. 20 3.0544 1489.16 5.4492 968. 97 3.0544 1505.03 10.0343 983.53 0.0000 1584.12 9.3169 984.45 0.0000 1596.21 0.0000 Page 4014of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08_: 03: 55. 4 7 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : 11:01:35. Sample date 7-DEC-2015 13:28:00. Acquisition date : 3-0CT-2016 07:00:55. Sample ID G405235048 Sample quantity : 1.31577E+02 GRAM Detector name GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.46 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 0 2 2 3 2 4 2 5 0 6 2 7 2 8 0 9 0 10 0 11 0 12 0 13 0 14 3 15 3 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 . 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 4015of5809 Energy 63.54* 75.02* 77.22 79.44 87.82 92.89* 95.17 105.77 115 .15 128.10 144.18* 185.94* 238.97* 241.98 271.68 295.65 338.8_8 352.49* 428.57 496. 82 510.95* 583.58* 599.58 609.81* 653.27 662.11* 679.99* 727. 7 5 783.28 795.70 861.65 912.02* 955 .13* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area* 30 110 231 52 69 58 25 18 30 15 18 18 65 416 118 35 148 84 304 23 14 71 136 32 187 17 508 16 28 13 35 12 88 17 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 134 164 123 121 247 171 122 100 139 128 134 86 174 83 66 97 110 78 60 50 24 59 19 34 39 9 49 17 16 22 9 18 32 22 1. 88 1. 35 1.22 1. 36 3.04 1.25 1.12 1. 24 0.65 1. 28 1. 82 1. 36 1. 59 1. 39 1. 57 2.26 1. 50 0.97 1. 56 4.00 1. 08 1. 78 1. 65 3.31 1. 98 1. 37 1. 84 0.80 2.07 1. 73 3. 72 0.58 1.56 2.23 127.16 150.13 154.53 158.97 175.75 185.90-190.46 211. 67 230.46 2-56. 36 281.13 288.55 372.14 478.27 484.30 543.75 591. 71 678.25 705.49 857.75 994.35 1022.64 1168. 00 1200.03 1220.52 1307.50 1325.18 1360. 96 1456.57 1567.70 1592.56 1724.56 1825.38 1911. 65 124 145 145 145 172 181 181 208 227 254 275 286 367 474 474 536 586 672 698 851 990 1014 1163 1192 1215 1303 1318 1357 1452 1562 1587 1721 1820 1902 7 8.42E-03 67.7 19 3.06E-02 22.6 19 6.41E-02 10.8 19 l.44E-02 47.1 10 1.91E-02 44.3 13 1. 62E-02 41. 8 13 6.89E-03 86.9 6 5.13E-03 88.7 10 8.20E-03 77.7 8 4.25E-03129.8 9 4.97E-03120.5 6 5.03E-03 87.4 11 1.81E-02 42.4 17 1.15E-01 6.3 17 3.28E-02 17.7 12 9.61E-03 59.2 11 4.12E-02 16.0 10 2.34E-02 22.3 16 8.44E-02 8.3 12 6.45E-03 64.7 8 3.81E-03 69.2 16*1.98E-02 30.7 11 3.77E-02 10.8 14 8.93E-03 42.7 12 5.21E-02 10.1 8 4.59E-03 41.1 15 1.41E-01 5.4 8 4.47E-03 52.7 10 7.85E-03 31.9 10 3.58E-03 74.1 12 9.81E-03 23.9 9 3.32E-03 72.7 14 2.45E-02 17.4 15 4.66E-03 66.2 Fit 1. 09E+OO 7.13E-01 4.18E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Pk It Energy Area Bkg"nd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969. 93 49 23 2.70 1941.28 1936 11 1.37E-02 24.0 36 0 1000.35* 23 0 2. 62 2002.17 1996 12 6.37E-03 23.9 37 0 1120.64* 64 15 2.10 2242.92 2235 15 1.78E-02 18.4 38 0 1461.76* 397 3 2.14 2925.67 2919 13 i.lOE-01 5.1 39 0 1510.25 9 4 1. 43 3022.72 3018 8 2.50E-03 50.9 40 0 1517.03 5 5 0. 72 3036.30 3030 10 1.39E-03 94.9 41 0 1631.84 12 0 0.62 3266.08 3261 10 3.33E-03 28.9 42 0 1766.05* 36 7 1. 49 3534.71 3527 12 1. OlE-02 22.3 Flag: "*" = Peak area was modified by background subtraction Page 4016 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:03:57 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses *by Sample title Sample date Sample ID 7-DEC-2015 13:28:00 G405235048 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:00:55 131. 58 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit IntE?rference Report SOLID GAMMA28 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB:....214 242.00 U-235 143.76 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4017 of 5809 Detector geometry: Elapsed real time: Halt life ratio Systematic Error Efficiencies *at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86. 94 SN-126 87.57 CD-109 88.03 RA-224 240.99 CE-141 145.44 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.46 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.237E+OO 1.636E+Ol 1. 636E+Ol 10.27 OK RU-103 497.08 91.00* 2.878E+OO 3.079E-02 6.229E+OO 138.39 OK 610.33 5.76 2.455E+OO 7.687E+OO 1.555E+03 20.25 OK CD-109 88.03 3.70* 5.460E+OO 1.205E+OO 1.893E+00 167.38 OK SN-126 64.28 9.60 3.030E+OO 7.008E-01 7.008E-01 135.48 OK 86.94 8.90 5.460E+OO 5.008E-01 5.008E-01 167.38 OK 87.57 37.00* 5.460E+OO 1.205E-01 l.205E-01 167.38 OK BA-137M 661.66 89.90* 2.305E+OO 1.413E+OO l.440E+OO 10.79 OK CS-137 661.66 85.10* 2.305E+OO l.493E+OO 1.522E+OO 10.79 OK CE-141 145.44 48.29* 6.589E+OO 9.228E-03 5.623E+OO 733.36 OK EU-155 86 .*55 30.70 5.460E+OO 1.452E-01 l.637E-01 167.38 OK 105.31 21.10* 6.332E+OO 9.0lOE-02 1.016E-01 177.47 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2.539E+OO 3.661E-01 3.661E-01 21. 63 OK 860.56 12.50 1. 886E+OO 2.867E-01 2.867E-01 145.48 OK BI-211 72.87 1. 23 4.138E+OO Line Not Found Absent 351. 06 12.92* 3. 781E+OO 6.364E-01 6.364E-01 184.21 OK PB-212 74.82 10.28 4.364E+OO 9.956E-01 9.956E-01 77.00 OK 77'.11 17.10 4.583E+OO 1.957E+OO l.957E-\-00 21. 68 OK 23.8. 63 43.60* 5.lOOE+OO 1.156E+OO 1.156E+OO 12.51 OK 300.09 3.30 4.295E+OO Line Not Found Absent BI-214 609.32 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 OK 1120.29 14.92 1.539E+OO 1.546E+OO l.546E+OO 36.87 OK 1764.49 15.30 l.045E+OO Line Not Found Absent PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.583E+OO 3.450E+OO 3.451E+OO 21. 68 OK 87.09 3.41 5.409E+OO Line Not Found <<INT Reject 242.00 7.25 5.054E+OO Line Not Found <<INT Reject 295.22 18.42 4.345E+OO 1.128E+OO l.129E+00 31. 95 OK 351. 93 35.60* 3.786E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 OK 1120.29 14.92 1.539E+OO 1.546E+OO l.546E+00 36.87 OK 1764.49 15.30 l.045E+OO Line Not Found Absent RA-224 240.99 4.10* 5.054E+00 1. 526E+OO 1.526E+OO 91. 57 OK RA-226 609.32 45.49* 2.455E+00 9.734E-01 9. 737E-Ol 20.25 OK 1120.29 14.92 1.539E+OO l.546E+00 1.546E+OO 36.87 OK 1764.49 15.30 1.045E+OO Line Not Found Absent AC-228 105.21 1.10 6.332E+00 1.728E+OO 1.728E+OO 177.47 OK 338.32 11. 27 3.901E+00 1.159E+OO 1.159E+OO 44.69 OK 794.95 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 OK 835.71. 1. 61 1.930E+OO Line Not Found Absent 911. 20 25.80* 1. 806E+OO 1.067E+OO 1.067E+OO 34.78 OK 968. 97 15.80 1. 723E+OO 1.018E+OO 1. 018E+OO 47.91 OK RA-228 105.21 1.10 6.332E+OO 1. 728E+OO 1. 728E+OO 177.47 OK 338.32 11. 27 3. 901E+OO l.159E+OO 1.159E+OO 44.69 OK 794.95 4.25 2.004E+00 2.358E+OO 2.358E+OO 47.73 OK 835 .. 71 1. 61 l.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.067E+OO 1.067E+OO 34.78 OK 968. 97 15.80 1. 723E+00 1.018E+OO 1.018E+OO 47.91 OK Page 4018of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235048 Acquisition date 07:00:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 4.364E+OO 9.956E-01 9.956E-Ol 77.00 OK 77 .11 17.10 4.583E+OO l.957E+OO 1.957E+OO 21. 68 OK 238.63 43.60* 5.lOOE+OO 1.156E+OO 1.156E+OO 12.51 OK 300.09 3.30 4.295E+OO Line Not Found Absent TH-230 609.32 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 OK 1120.29 *14.92 1.539E+OO 1.546E+OO 1.546E+OO 36.87 OK 1764.49 15.30 1.045E+OO Line Not Found Absent TH-232 105.21 1.10 6.332E+OO 1.728E+OO 1.728E+OO 177.47 OK 338.32 11. 27 3.901E+OO 1.i59E+OO 1.159E+OO 44.69 OK 835. 71 1. 61 1.930E+OO Line Not Found Absent 911. 20 25.80* 1.806E+OO 1.067E+OO 1.067E+OO 34.78 OK 968. 97 15.80 1. 723E+OO 1. 018E+OO' 1.018E+OO 47.91 OK TH-234 63.29 3.70* 3.030E+OO 1.818E+OO 1.818E+OO 135.48 OK 92.59 4.23 5.779E+00 l.570E+OO 1.570E+OO 83.57 OK U-234 609.32 45.49* 2.455E+00 9.734E-01 9.734E-01 20.25 OK 1120.29 14.92 1.539E+OO 1.546E+OO 1.546E+OO 36.87 OK 1764.49 15.30 1.045E+OO Line Not Found Absent U-235 89. 96 3.47 5.602E+OO Line Not Found Absent 93.35 5.60 5.779E+OO 'l .186E+OO 1.18 6E+OO 83.57 OK 143.76 10. 96* 6.593E+OO Line Not Found <<INT Reject 163.33 5.08 6.352E+OO Line Not Found Absent 185. 72 57.20 5.981E+00 1.197E-01 1.197E-01 84.89 OK 205.31 5.01 5.647E+OO Line Not Found Absent U-238 63.29 3.70* 3.030E+OO l.818E+OO l.818E+00 135.48 OK 92.59 4.23 5.779E+OO 1.570E+OO l.570E+OO 83.57 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.364E+OO 1.523E-01 1.523E-01 77.00 OK ANH-511 511. 00 100.00* 2.816E+OO l.484E-01 1.484E-01 61.42 OK Flag: "*" = Keyline Page 4019 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:58.74 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Rdad *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l. * *Acquisition date 3-0CT-2016 07.:00:55 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
Sample date 7-DEC-2015 13:28:00 Analyst initials: MXRl *
Sample ID G405235048 Sample Quantity 1.3158E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid.
Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM K-40 1.636E+Ol 1. 647E+OO 6.664E-01 RU-103 6.229E+OO 8.448E+OO l.105E+Ol CD-109 1.893E+OO 3.105E+OO 2.489E+OO SN-126 l.205E-01 1. 976E-01 1.593E-01 BA-137M 1.440E+OO l.523E-01 6.579E-02 CS-137 1.522E+OO 1.609E-01 6.950E-02 CE-141 5.623E+OO 4.041E+Ol 5.007E+Ol EU-155 l.016E-01 l.767E-01 2.334E-01 TL-208 3. 661E-01 7.763E-02 7.269E-02 BI-211 6.364E-01 l.149E+00 3.563E-01 PB-212 1.156E+OO 1. 417E-01 1. 140E-01 BI-214 9.737E-01 1.932E-01 1.386E-01 PB-214 1.360E+OO 2.215E-01 3.598E-01 RN-222 9.737E-01 1. 932E-01 1. 38 6E-01 RA-224 1.526E+OO 1.370E+00 1.222E+OO RA-226 9.737E-01 1.932E-01 1.386E-.01 AC-228 1.067E+OO 3.635E-01 2.743E-01 RA-228 1.067E+OO 3.635E-01 2.743E-01 TH-228 1.156E+OO 1.417E-01 1.140E-01 9.734E-01 l.932E-01 1.385E-01 TH-232 1.067E+OO 3.635E-01 2.743E-01 TH-234 l.818E+OO 2.414E+OO 2.644E+OO U-234 9.734E-01 l.932E-01 1.385E-01 U-235 1.603E-01 2.747E-01 4.061E-01 U-238 l.818E+OO 2.414E+OO 2.644E+OO AM-243 1.523E-01 l.149E-01 9.726E-02 ANH-511 1.484E-01 8.936E-02 5.887E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 -l.122E+OO 1.683E+Ol 3.086E+Ol NA-22 3.668E-02 4.882E-02 1. 075E-01 NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO Page 4020 of 5809 NOT IDENT. NOT IDENT. SHORT HLIF AL-26 6.615E-03 2.369E-02 6.016E-02 NOT IDENT. SC-46 7.763E-02 4 .141E-01 8.393E-01 FAIL ABUN V-48 O.OOOE+OO 1. 755E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.886E+02 O.OOOE+OO SHORT HLIF MN-54 2.311E-02 6.839E-02 l.404E-01 NOT IDENT. C0-56 4.028E-01 5 .151E-01 1.116E+OO NOT IDENT. MN-56 O.OOOE+OO 1.284E+41 O.OOOE+OO SHORT HLIF C0-57 -4.445E-03 5.719E-02 1. OllE-01 NOT IDENT. C0-58 5.473E-02 5.371E-01 l.103E+OO NOT IDENT. FE-59 -2. 871E+00 6.836E+OO 1.254E+Ol NOT IDENT. C0-60 1.241E-02 3.878E-02 8.247E-02 NOT IDENT. ZN-65 7. lllE-02 1.912E-01 3.588E-01 NOT IDENT. GE-68 -2.365E+OO 2.651E+OO 4.572E+OO NOT IDENT. AS-73 -3.549E+00 1. 079E+Ol 1.932E+Ol NOT IDENT. AS-74 O.OOOE+OO 8.245E+03 O.OOOE+OO SHORT HLIF SE-75 -7.304E-02 2.172E-01 4.040E-01 NOT IDENT. BR-77 O.OOOE+OO
3. 316E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.583E+02 O.OOOE+OO SHORT HLIF RB-83 4.221E-01 7.417E-01 1. 486E+OO NOT IDENT. KR-85 8.618E+OO 9.504E+OO 1. 757E+Ol NOT IDENT. SR-85 9.158E-01 1. 013E+OO 1. 873E+OO NOT IDENT. RB-86 O.OOOE+OO 3.268E+04 O.OOOE+OO SHORT HLIF Y-88 -2.699E-02 2.250E-01 4.790E-01 NOT IDENT. Y-91 -2.762E+02 5.997E+02 1. 072E+03 NOT IDENT. NB-94 3.432E-02 3.332E-02 7.074E-02 NOT IDENT. NB-95 -1.003E+OO 1.043E+OO 1.810E+OO NOT IDENT. NB-95M -3.520E-01 3.172E+OO 5.348E+00 NOT IDENT. ZR-95 5. 605E.:..01 l.458E+OO 3.059E+OO NOT IDENT. NB-97 O.OOOE+OO l.195E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.485E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.715E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 2.590E-02 6.588E-02 7. lllE-02 FAIL ABUN RH-102 4.350E-02 6.814E-02 1. 372E-01 NOT IDENT. RH-106 5.829E-01 4.'841E-01 1. 07 9E+OO NOT IDENT. RU-106 5.829E-01 4.841E-01 1. 079E+OO NOT IDENT. AG-108M 5.930E-03 3.257E-02 5.977E-02 NOT IDENT. AG-llOM -3 .118E-02 1.085E-01 2.057E-01 NOT IDENT. SN-113 6.313E-02 2.706E-01 5.199E-01 NOT IDENT. CD-115 O.OOOE+OO 4.428E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.246E+05 O.OOOE+OO SHORT HLIF TE-123M -3.515E-02 1.623E-01 2.787E-01 NOT IDENT. SB-124 -2. 351E+OO 1.881E+OO 9.527E-01 NOT IDENT. SB-125 1. 761E-01 2.234E-01* 2.451E-01 FAIL ABUN TE-125M 9.495E+Ol 3.277E+02 5.999E+02 NOT IDENT. I-126 O.OOOE+OO l.031E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.348E+06 O.OOOE+OO SHORT HLIF *SB-127 O.OOOE+OO 2.857E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 6.345E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 781E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4. 963E+26 O.OOOE+OO SHORT HLIF BA-133 -9.114E-03 4.620E-02 7.656E-02 NOT IDENT. I-133 0 .. OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 0.000E+OO 7.228E-02 l.316E-01 FAIL ABUN CS-135 -3.619E-02 1.493E-01 2.500E-01 NOT IDENT. I-135 O.OOOE+OO 8.777E+40 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.365E+05 O.OOOE+OO SHORT HLIF CE-139 -3.694E-03 1.241E-01 2.395E-01 NOT IDENT. BA-140 O.OOOE+OO l.464E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.043E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 5.094E-01 3.990E-01 7.839E-01 FAIL ABUN PM-144 l.300E-02 6.183E-02 1.176E-01 NOT IDENT. PR-144 1.113E+OO *5. 371E+OO 1.021E+Ol NOT IDENT. PM-146 -l.524E-02 5. 696E-02 1.027E-01 NOT IDENT. ND-147 0. 'OOOE+OO 3.747E+07 O.OOOE+OO SHORT HLIF PM-147 -5.018E+02 9.528E+02 l.622E+03 NOT IDENT. PM-149 O.OOOE+OO 7.246E+40 O.OOOE+OO SHORT HLIF EU-150 1.'114E-04 3.134E-02 5.312E-02 FAIL ABUN EU-152 l.540E-02 1.126E-01 2.141E-01 NOT IDENT. GD-153 6.185E-02 2.184E-01 3.750E-01 NOT IDENT. EU-154 8.987E-02 1.196E-01 2.634E-01 NOT IDENT. TB-160 -1.076E+OO 1.991E+OO 3.630E+OO FAIL ABUN H0-166M 1.626E-03 5.814E-02 1.091E-01 FAIL ABUN TM-.171 -9.139E+00 2.562E+Ol 4.581E+Ol NOT IDENT. HF-172 -3.073E-03 3.026E-01 4.930E-01 FAIL ABUN LU-172 3.354E-02 8.580E-02 1. 765E-01 FAIL ABUN LU-176 -1.213E-02 2.829E-02 5.151E-02 FAIL ABUN Page 4021 of 5 809 HF-181 -l.503E+OO 5.321E+OO 9.594E+OO NOT IDENT. TA-182 8.899E-02 8.587E-01 1. 722E+00 FAIL ABUN RE-183 4.972E-Oi 3.302E+OO 6.224E+00 NOT IDENT. RE-184 l.600E+Ol 3.386E+Ol 7.076E+Ol NOT IDENT. W-188 -7.076E+Ol l.374E+02 2.214E+02 FAIL ABUN IR-192 3.741E-01 5.436E-01 l.087E+OO FAIL ABUN HG-203 -1. 814E-02 2.738E+OO 5.194E+OO NOT IDENT. BI-207 -1. 596E-02 4. 596E-02 8.598E-02 FAIL ABUN PB-210 1. 340E+OO 4.413E+OO 8.351E+OO NOT IDENT. PB-211 8.252E-01 7.860E-01 l.619E+OO FAIL ABUN BI-212 l.132E+OO 7.082E-01 l.288E+00 FAIL ABUN RN-219 3.568E-02 4.606E-01 8.673E-01 FAIL ABUN RA-223 1. 968E-01 6.763E-01 l.309E+OO FAIL ABUN AC-227 -2.699E-02 2.495E-01 4.721E-01 FAIL ABUN TH-227 -2.699E-02 2.495E-01 4.721E-01 FAIL ABUN TH-229 9.613E-02 5.592E-01 l.081E+OO FAIL ABUN PA-231 l.950E-01 .5. 331E-01 l.031E+OO NOT IDENT. TH-231 1. 968E-01 6. 763E-01. 1. 309E+OO . FAIL ABUN PA-233 -3.749E-02 6.581E-02 l.183E-01 NOT IDENT. , PA-234 3.449E-02 2.443E-01 *5. 059E-01 FAIL ABUN PA-234M 9.084E+OO 4.260E+OO l.009E+Ol FAIL ABUN NP-237 -3.749E-02 6.581E-02 l.183E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.553E-02 2.635E-01 4.781E-01 FAIL ABUN PU-239 2.347E+02 5. 972E+02 6.686E+02 FAIL ABUN AM-241 -5.943E-02 l.515E-01 2. 721E-01 NOT IDENT. CM-243 -7.438E-02 l.250E-01 l.942E-01 NOT IDENT. BK-247 -3.949E-02 7.927E-02 l.377E-01 FAIL ABUN CM-247 -l. lllE-02 4.322E-02 7.862E-02 NOT IDENT. CF-249 -4. 551E-03 4.584E-02 8. 491E-02 NOT IDENT. CF-251 3.599E-02 l.250E-01 2.459E-01 NOT IDENT. Page 4022 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:03:56.57 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 378 10.66* l.237E+OO 1.636E+Ol 1.636E+Ol 10.27 RU-103 497.08 14 91.00* 2.878E+OO 3.079E-02 6.229E+OO 138.39 610.33 191 5.76 2.455E+OO 7.687E+OO l.555E+03 20.25 CD-109 88.03 79 3.70* 5.460E+OO 2.245E+OO 3.527E+OO 88.60 SN-126 64.28 36 9.60 3.030E+OO 7.008E-01 7.008E-01 135.48 86.94 79 8.90 5.460E+00 9.332E-01 9.332E-01 88.60 87.57 79 37.00* 5.460E+OO 2.245E-01 2.245E-01 88.60 BA-137M 661. 66 513 89.90* 2.305E+OO l.413E+OO 1.440E+OO 10.79 CS-137 661. 66 513 85.10* 2.305E+OO 1. 493E+OO 1.522E+OO 10.79 CE-141 145.44 20 48.29* 6.589E+OO 3.639E-02 2.217E+Ol 174.83 EU-155 86.55 79 30.70 5.460E+OO 2.705E-01 3. 051E-01 88.60 105.31 21 21.10* 6.332E+OO 9.0lOE-02 1.016E-01 177.47 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 139 '85. 00* 2.539E+OO 3.661E-01 3.661E-01 21. 63 860.56 12 12.50 1.886E+OO 2.867E-01 2. 8 67E-01 145.48 BI-21'1 72.87 ------1. 23 4 .138E+OO ------Line Not Found ------351. 06 321 12.92* 3.781E+OO 3.746E+OO 3.746E+OO 16.62 PB-212 74.82 128 10.28 4.364E+OO 1.632E+OO 1.632E+OO 45.28 77 .11 269 17.10 4.583E+OO 1.957E+OO 1.957E+OO 21. 68 238.63 450 43.60* 5.lOOE+OO 1.156E+OO l.156E+00 12.51 300.09 ------3.30 4.295E+OO ------Line Not Found ------BI-:-214 609.32 191 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 1120. 29 62 14.92 1.539E+OO 1.546E+OO 1.546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not F.ound ------PB-214 7 4 . .82 128 5.80 4. 3'64E+OO 2.893E+OO 2.894E+OO 45.28 77 .11 269 9.70 4.583E+OO 3.450E+00 3. 451E+OO 21. 68 87.09 79 3.41 5.460E+OO 2.436E+OO 2.436E+OO 88.60 242.00 128 7.25 5.054E+OO 1.992E+OO 1.992E+OO 35.32 295.22 158 18.42 4.345E+OO 1.128E+OO 1.129E+OO 31. 95 351. 93 321 35.60* 3.781E+OO 1.359E+OO 1. 360E+OO 16.62 RN-222 609.32 191 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 1120.29 62 14.92 1.539E+OO 1. 546E+00 1.546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------RA-224 240.99 128 4.10* 5.054E+OO 3.522E+OO 3.522E+OO 35.32 RA-226 609.32 191 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 1120.29 62 14.92 1.539E+OO 1. 546E+OO l.546E+00 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------AC-228 105.21 21 1.10 6.332E+OO l.728E+OO 1.728E+OO 177.47 338.32 89 11. 27 3. 901E+OO 1.159E+OO l.159E+00 44.69 794.95 35 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 835. 71 ------1. 61 1.930E+OO ------Line Not Found ------911. 20 87 25.80* 1.806E+OO 1.067E+OO 1.067E+00 34.78 968.97 49 15.80 1.723E+00 1.018E+OO 1.018E+OO 47.91 RA-228 105.21 21 1.10 6.332E+OO 1.728E+OO 1. 728E+OO 177.47 338.32 89 11. 27 3.901E+00 1.159E+OO 1.159E+OO 44.69 794.95 35 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 835.71 ------1. 61 1.930E+OO ------Line Not Found ------Page 4023 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235048
Acquisition date 3-0CT-2016 07:00:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 911. 20 87 25.80* 1.806E+OO 1.067E+OO 1.067E+OO 34.78 968. 97 49 15.80 1. 723E+OO 1.018E+OO l.018E+OO 47.91 TH-228 74.82 128 10.28 4.364E+OO 1.632E+OO 1.632E+OO 45.28 77 .11 269 17.10 4.583E+OO 1.957E+OO 1.957E+OO 21. 68 238.63 450 43.60* 5.lOOE+OO 1.156E+OO 1.156E+OO 12.51 300.09 ------3.30 4.295E+OO ------Line Not Found ------TH-230 609.32 191 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 1120.29 62 14.92 1.539E+OO 1.546E+OO 1.546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------TH-232 105.21 21 1.10 6.332E+OO 1. 728E+OO 1.728E+OO 177.47 338.32 89 11.27 3.901E+OO l.159E+OO 1.159E+OO 44.69 835.71 ------1. 61 1.930E+OO ------Line Not Found ------9°11.20 87 25.80* 1. 806E+OO 1.067E+OO 1.067E+OO 34.78 968. 97 49 15.80 1. 723.E+OO l.018E+00 1.018E+OO 47.91 TH-234 63.29 36 3.70* 3.030E+00 1.818E+OO l.818E+00 135. 48 92.59 67 4.23 5.779E+OO 1. 570E+OO 1.570E+OO 83.57 U-234 609.32 191 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 1120.29 62 14.92 l.539E+OO 1. 546E+OO 1.546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------U-235 89. 96 ------3.47 5.602E+OO ------Line Not Found ------93.35 67 5.60. 5.779E+OO l.186E+OO 1.186E+OO 83.57 143.76 20 10. 96* 6.589E+OO l.603E-01 l.603E-:-01 174.83 163.33 ------5.08 6.352E+OO ------Line Not Found ------185. 72 72 57.20 5.981E+OO l.197E-01 l.197E-01 84.89 205.31 ------5.01 5.647E+OO ------Line Not Found ------U-238 63.29 36 3.70* 3.030E+OO 1.818E+OO 1.818E+OO 135.48 92.59 67 4.23 5.779E+OO 1.570E+OO 1.570E+OO 83.57 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 128 67.20* 4.364E+00 2.497E-01 2.497E-01 45.28 ANH-511 511. 00 73 100.00* 2.816E+OO 1.484E-01 l.484E-01 61. 42 Flag: "*" Key line Page 4024 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Total number of lines in spectrum 42 Number of unidentified lines 6 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 CE-141 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 39.26D 461.40D 2.30E+05Y 30.08Y 30.08Y 32. 51D 4.75Y -1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+10Y 1600.00Y 1. 41E+10Y 1.41E+10Y l.41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1. OOE+09Y Decay 1. 00 202. 1. 57 1. 00 1. 02 1. 02 609. 1.13 1. 00 1. 00 1. 00 1. 00 1. 00. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 636E+01 3.079E-02 2.245E+OO 2.245E-01 1.413E+00 1.493E+OO 3.639E-02 9.0lOE-02 3.661E-01 3.746E+00 1.156E+00 9.734E-01 1.359E+OO 9.734E-01 3.522E+OO 9.734E-01 1.067E+00 1.067E+OO 1.156E+OO 9.734E-01 1.067E+OO 1. 818E+OO 9.734E-01 1.603E-01 1.818E+OO 2.497E-01 1.484E-01 4.546E+Ol 4.546E+Ol Decay Corr pCi/GRAM 1.636E+Ol 6.229E+OO 3.527E+OO 2.245E-01 1.440E+OO 1. 522E+00 2.217E+Ol 1.016E-01 3.661E-01 3.746E+OO l.156E+OO 9.737E-01 1.360E+OO 9.737E-01 3.522E+OO 9.737E-01 1. 067E+OO 1.067E+OO 1.156E+OO 9.734E-01 1.067E+OO 1.818E+OO 9.734E-01 1.603E-01 1.818E+OO 2.497E-01 1.484E-01 7.515E+Ol 7.515E+Ol 85.71% Decay Corr 2-Sigma Error 0.168E+Ol 8.620E+OO 3.125E+00 1.989E-01 0.155E+OO 0.164E+OO 3.877E+Ol 1. 803E-01 0.792E-01 0.622E+OO 0.145E+OO 1.972E-01 0.226E+00 l.972E-01 1. 244E+oo* 1.972E-01 0.371E+00 0.371E+OO 0.145E+OO 1. 971E-01 0.371E+OO 2.464E+OO 1. 971E-01 2.803E-01 2.464E+OO 1.131E-01 0.912E-01 "M" Manually accepted 2-Sigma %Error 10.27 138.39 88.60 88.60 10.79 10. 79 174.83 177.47 21. 63 16.62 12.51 20.25 16.62 20.25 35.32 20.25 34.78 34.78 12.51 20.25 34.78 135.48 20.25 174.83 135.48 45.28 61. 42 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4025 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235048 Acquisition date : 3-0CT-2016 07:00:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 79.44 60 141 1. 36 158.97 145 19 1. 44E-02 94.1 4.79E+OO T 2 95.17 29 140 1.12 190.46 181 13 6.89E-03 **** 5.90E+OO T 0 115 .15 34 158 0.65 230.46 227 10 8.20E-03 **** 6.55E+OO T 0 128.10 17 144 1.28 256.36 254 8 4.25E-03 **** 6.65E+OO T 0 140.47 20 150 1. 82 281.13 275 9 4.97E-03 **** 6.62E+OO T 0 271.68 37 105 2.26 543.75 536 12 9.61E-03 **** 4.64E+OO T 0 428.57 24 52 4.00 857.75 851 12 6.45E-03 **** 3.23E+OO T 0 599.58 33 34 3.31 1200.03 1192 14 8.93E-03 85.4 2.49E+OO T 0 653.27 17 10 1. 37 1307.50 1303 8 4.59E-03 82.1 2.33E+OO 0 679.99 16 17 0.80 1360. 96 1357 8 4.47E-03 **** 2.26E+OO 0 727.75 28 16 2.07 1456.57 1452 10 7.85E-03 63.9 2.14E+OO T 0 783.28 13 22 1. 73 1567.70 1562 10 3.58E-03 **** 2.03E+OO T 0 955 .13 16 22 2.23 1911. 65 1902 15 4.66E-03 **** l.74E+OO T 0 1000.35 22 0 2.62 2002.17 1996 12 6.37E-03 47.8 l.68E+OO T 0 1510.25 9 4 1:43 3022.72 3018 .8 2.50E-03 **** 1.20E+OO 0 1517.03 5 5 0. 72 3036.30 3030 10 1.39E-03 **** 1.20E+OO 0 1631.84 11 0 0.62 3266.08 3261 10 3. 33E-0.3 57.7 1.12E+OO 0 1766.05 34 7 1. 49 3534.71 3527 12 1. OlE-02 44.6 l.04E+OO Flags: "T" = Tentatively associated Page 4026 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:10.39 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA' * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l *
Acquisition date 3-0CT-2016 07:00:55 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
Sample date 7-DEC-2015 13:28:00 Nuclide Library : SOLID *
Sample ID G405235048 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.3158E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides* ----Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 CE-141 EU-155 TL-208 BI-211 PB-2.12 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 .AM-243 ANH-511 Le (pCi/GRAM 2.747E-01 4.920E+OO 1.182E+OO 7.567E-02 2.905E-02 3.069E-02 2. 351E+Ol 1.099E-01 3. 272E-02 1. 621E-01 5.344E-02 6.229E-02 1. 741E-01 6.229E-02 5. 728E-01 6.229E-.02 1.205E-01 1.205E-01 5.344E-02 6.226E-02 1.205E-01 1.249E+OO 6.226E-02 1.920E-01 1.249E+00 4.586E-02 2.665E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4027 of 5809 Le (pCi/GRAM 1.416E+Ol 4.681E-02 0.000E+OO 2.252E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.
sc-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144* PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4028 of 5809 3.688E-01 0.000E+OO O.OOOE+OO 6.235E-02 4.972E-01 O.OOOE+OO 4.750E-02 4.766E-01 5.318E+OO 3.480E-02 1.561E-01 1.959E+OO 9.032E+OO O.OOOE+OO 1.858E-01 O.OOOE+OO O.OOOE+OO 6.726E-01 8.107E+OO 8.641E-01 O.OOOE+OO 1.850E-01 4.637E+02 3.182E-02 8.068E-01 2.513E+OO 1.351E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.346E-02 6.183E-02 4.823E-01 4.823E-01 2.717E-02 8.952E-02 2.386E-01 O.OOOE+OO O.OOOE+OO 1.309E-01 O.OOOE+OO 1.125E-01 2.825E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.470E ... 02 O.OOOE+OO 5.981E-02 1.144E-01 O.OOOE+OO O.OOOE+OO 1.126E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.695E-01 5.250E-02 4.559E+OO 4.702E-02 O.OOOE+OO 7.581E+02 O.OOOE+OO 2.444E-02 9.906E-02 1. 765E-01 1.147E-01 1. 566E+OO 4.791E-02 2.140E+Ol '2.321E-01 7.764E-02 2.376E-02 4.345E+00 FAIL ABUN .SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHOR*T HLIF NOT IDENT. NOT IDENT. NOT IDENT. .NOT I DENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT .IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT.
NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-.207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4029 of 5809 7.377E-01 2.910E+OO 3.133E+Ol l.018E+o2 5.047E-01 2.410E+Ci0 3.639E-02 3.932E+OO 7 .. 479E-01 5.897E-01 3.987E-01 6.059E-01 2.189E-01 2.189E-01 5.095E-01 4.813E-01 6.059E-01 5.421E-02 2.161E-01 4.498E+OO 5.421E-02 O.OOOE+OO 2.237E-01 3.153E+02 1.270E-01 9.082E-02 6.325E-02 3.610E-02 3.905E-02 1.154E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:15.77 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l * *Acquisition date 3-0CT-2016 07:00:55 Sensitivity : 3.000 *
Detector ID GAM28 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 Half life ratio : ***** *
Sample date 7-DEC-2015 13:28:00 Nuclide Library : SOLID *
Sample ID G405235048 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.3158E+02 GRAM *
Quantity Err(%) 1.5200E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * * '* Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1. 636E+Ol 1.857E+OO 1.857E+OO RU-103 6.229E+OO 8.453E+OO 8.453E+OO CD-109 l.893E+00 3 .115E+OO 3.115E+OO SN-126 1.205E-01 l.982E-01 1.982E-01 BA-137M 1.440E+OO l.646E-01 1.646E-01 CS-137 1.522E+00 "1. 739E-01 1.739E-01 CE-141 5.623E+OO 4.043E+Ol 4.043E+Ol EU-155 1.016E-01 1. 769E-01 1. 769E-01 TL-208 3.661E-01 7.920E-02 7.920E-02 BI-211 6.364E-01 1.165E+OO l.165E+00 PB-212 l.156E+OO l.545E-01 1.545E-01 BI-214 9.737E-01 1.978E-01 l.978E-01 PB-214 l.360E+OO 2.287E-01 2.287E-01 RN-222 9.737E-01 l.978E-01 1.978E-01 RA-224 1.526E+OO 1.379E+OO l.379E+OO RA-226 9.737E-01 1.978E-01 1.978E-01 AC-228 1.067E+OO 3.677E-01 3.677E-01 RA-228 l.067E+00 3.677E-01 3.677E-01 TH-228 1.156E+OO 1.545E-01 1.545E-01 TH-230 9.734E-01 1.977E-01 1.977E-01 TH-232 1.067E+OO 3.677E-01 3.677E-01 TH-234 1.818E+OO 2.448E+OO 2.448E+00 U-234 9.734E-01 l.977E-01 l.977E-01 U-235 l.603E-01 2.748E-01 2.748E-01 U-238 1.818E+OO 2.448E+00 2.448E+OO AM-243 l .. 523E-01 l.160E-01 l.160E-01 ANH-511 l.484E-01 8.956E-02 8.956E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-s;igma) BE-7 -1.122E+OO 1.683E+Ol 1.684E+Ol NOT IDENT. NA-22 3.668E-02 4.884E-02 5.156E-02 NOT IDENT. NA-24 -1.000E+41 4.768E+41 O.OOOE+OO SHORT HLIF Page 4030 of 5809 AL-26 6.615E-03 2.370E-02 2.389E-02 NOT IDENT. SC-46 7.763E-02 4.141E-01 4.156E-01 FAIL ABUN V-48 -4.998E+02 1. 755E+04 1.755E+04 SHORT HLIF CR-51 -5.934E+Ol 4.887E+02 4.894E+02 SHORT HLIF MN-54 2. 311E-02 6.840E-02 6.919E-02 NOT IDENT. C0-56 4.028E-01 5.154E-01 5.464E-01 NOT IDENT. MN-56 1. OOOE+41 1.284E+41 O.OOOE+OO SHORT HLIF C0-57 -4.445E-03 5. 719E-02 5. 723E-02 NOT IDENT. C0-58 5.473E-02 5. 371E-01 5.377E-01 NOT IDENT. FE-59 -2.871E+OO 6.840E+OO 6. 961E+OO NOT IDENT. C0-60 1.241E-02 3.878E-02 3.919E-02 NOT IDENT. ZN-65 7. lllE-02 l.912E-01 l.939E-01 NOT IDENT. GE-68 -2.365E+OO 2.652E+OO 2.858E+OO NOT IDENT. AS-73 -3.549E+OO 1.081E+Ol l.093E+Ol NOT IDENT. AS-74 -3.353E+03 8.250E+03 8.387E+03 SHORT HLIF SE-75 -7.304E-02 2.173E-01 2.198E-01 NOT IDENT. BR-77 2.705E+38 2.348E+39 O.OOOE+OO SHORT HLIF SR-82 -4.613E+02 8.585E+02 8.834E+02 SHORT HLIF RB-83 4.221E-01 7.440E-01 7.679E-01 NOT IDENT. KR-85 8.618E+OO 9. 511E+00 l.027E+Ol NOT IDENT. SR-85 9.158E-01 1.014E+OO 1.095E+OO NOT IDENT. RB-86 -3.646E+04 3. 272E+04 3.662E+04 SHORT HLIF* Y-88 -2.699E-02 2.250E-01 2.253E-01 NOT IDENT. Y-91 -2.762E+02 5.998E+02 6.126E+02 NOT IDENT. NB-94 3.432E-02 3.335E-02 3.676E-02 NOT IDENT. NB-95 -l.003E+OO 1.044E+OO l.138E+OO NOT IDENT. NB-95M -3.520E-01 3 .172E+OO *3.176E+00 NOT IDENT. ZR-95 5.605E-01 1.459E+OO l.480E+OO NOT IDENT. NB-97 1.000E+41 l.196E+41 0. OOOE+OO. SHORT HLIF ZR-97 1.000E+41 8.495E+40 O.OOOE+OO SHORT HLIF M0-99 l.190E+31 2.715E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.364E+41 O.OOOE+OO SHORT HLIF RH-101 2.590E-02 6.605E-02 6.707E-02 FAIL ABUN RH-102 4.350E-02 6.824E-02 7.lOOE-02 NOT IDENT. RH-106 5.829E-01 4.855E-01 5.520E-01 NOT IDENT. RU-106 5.829E-01 4.855E-01 5.520E-01 NOT IDENT. AG-108M 5.930E-03 3.257E-02 3.268E-02 NOT IDENT. AG-llOM -3 .118E-02 1.085E-01 1.094E-01 NOT IDENT. SN-113 6.313E-02 2.706E-01 2.721E-01 NOT IDENT. CD-115 -2.381E+39 4.449E+39 O.OOOE+OO SHORT HLIF SN-117M 1.417E+04 .1. 246E+05 1.247E+05 SHORT HLIF TE-123M -3.515E-02 l.623E-01 l.631E-01 NOT IDENT. SB-124 -2. 351E+OO l.886E+OO 2.163E+OO NOT IDENT. SB-125 1. 761E-01 2.235E-01 2. 372E-01 FAIL ABUN TE-125M 9.495E+Ol 3.278E+02 3.305E+02 NOT IDENT. I-126 -7.382E+04 1. 031E+06 1.032E+06 SHORT HLIF SB-126 * -7.545E+05 l.355E+06 1.397E+06 SHORT HLIF SB-127 -4.602E+20 2.858E+22 O.OOOE+OO SHORT HLIF I-131 1.481E+09 6.346E+09 6.381E+09 SHORT HLIF I-132 -1.000E+41 1.862E+42 O.OOOE+OO SHORT HLIF TE-132 -4.221E+26 5.253E+26 O.OOOE+OO SHORT HLIF BA-133 -9.114E-03 4.620E-02 4.638E-02 NOT IDENT. I-133 -l.000E+41 1. 273E+42 O.OOOE+OO SHORT HLIF CS-134 l.545E-01 7.259E-02 l.006E-01 FAIL ABUN . CS-135 -3.619E-02 *1. 493E-01 1.502E-01 NOT IDENT. I-135 -1.000E+41 6.852E+41 O.OOOE+OO SHORT HLIF CS-136 -3.752E+05 3.390E+05 3.788E+05 SHORT HLIF CE-139 -3.694E-03 1. 241E-01 l.241E-01 NOT IDENT. BA-140 7.368E+04 l.464E+06 1.465E+06 SHORT HLIF LA-140 -1. 070E+05 4.044E+05 4.072E+05 SHORT HLIF CE-143 1.000E+41 2.514E+41 O.OOOE+OO SHORT HLIF CE-144 5.094E-01 4.000E-01 4.612E-01 FAIL ABUN PM-144 1.300E-02 6.183E-02 6.211E-02 NOT IDENT. PR-144 l.113E+OO 5.371E+OO .5. 394E+OO NOT IDENT. PM-146 -1.524E-02 5.697E-:-02 5.739E-02 NOT IDENT. ND-147 -6. 558E'+06 3.747E+07 3.759E+07 SHORT HLIF PM-147 -5.018E+02 9.531E+02 9.796E+02 NOT IDENT. PM-149 3.943E+40 7.298E+40 O.OOOE+OO SHORT HLIF EU-150 1.114E-04 3.134E-02 3.134E-02 FAIL ABUN EU-152 l.540E-02 l.126E-01 l.129E-01 NOT IDENT. GD-153 6.185E-02 2.184E-01 2.202E-01 NOT IDENT. EU-154 8.987E-02 l.197E-01 l.263E-01 NOT IDENT. TB-160 -1. 07 6E+OO l.992E+OO 2.050E+OO FAIL *ABUN H0-166M 1. 62 6E-03 5.815E-02 5.815E-02 FAIL ABUN TM-171 -9.139E+00 2.563E+Ol 2. 596E+Ol NOT IDENT. HF-172 -3.073E-03 3.026E-01 3.026E-01 FAIL ABUN LU-172 3.354E-02 8.587E-02 8.719E-02 FAIL ABUN LU-176 -1.213E-02 2.830E-02 2.882E-02 FAIL ABUN Page 4031 of 5809 HF-181 -1.503E+OO 5.322E+OO 5.365E+OO NOT IDENT. TA-182 8.899E-02 8.587E-01 8.597E-01 FAIL ABUN RE-183 4.972E-01 3.303E+00 3.310E+OO NOT IDENT. RE-184 1.600E+Ol 3.408E+Ol 3.483E+Ol NOT IDENT. W-188 -7.076E+Ol 1.377E+02 1.413E+02 FAIL ABUN IR-192 3.741E-01 5.438E-01 5.694E-01 FAIL ABUN HG-203 -l.814E-02 2.738E+OO 2.738E+OO NOT IDENT. BI-207 -1. 596E-02 4. 596E-02 4.652E-02 FAIL ABUN PB-210 1.340E+OO 4.414E+OO 4.455E+OO NOT IDENT. PB-211 8.252E-01 7. 871E-01 8.706E-01 FAIL ABUN BI-212 1.132E+OO 7.106E-01 8.747E-01 FAIL ABUN RN-219 3.568E-02 4.606E-01 4.609E-01 FAIL ABUN RA-223 1. 968E-01 6.764E-01 6.822E-01 FAIL ABUN AC-227 -2.699E-02 2.495E-01 2.498E-01 FAIL ABUN TH-227 -2.699E-02 2.495E-01 2.498E-01 FAIL ABUN TH-229 9.613E-02 5.592E-01 5.609E-01 FAIL ABUN PA-231 l.950E-01 5.347E-01 5.419E-01 NOT IDENT. TH-231 1. 968E-01 6.764E-01 6.822E-01 FAIL ABUN PA-233 -3.749E-02 6.584E-02 6.797E-02 NOT IDENT. PA-234 3.449E-02 2.474E-01 2.479E-01 FAIL ABUN PA-234M 9 .. 084E+OO 4.278E+00 5.922E+OO FAIL ABUN NP-237 -3.749E-02 6.584E-02 6 .*797E-02 FAIL ABUN NP-238 -l.OOOE+41 2.414E+41 O.OOOE+OO SHORT HLIF NP-239 3.553E-02 2.635E-01 2.640E-01 FAIL ABUN PU-239 2.347E+02 5.973E+02 6.066E+02 FAIL ABUN AM-241 -5.943E-02 1.515E-01 1.539E-01 NOT IDENT. CM-243 -7.438E-02 1.252E-01 1.296E-01 NOT IDENT. BK-247 -3.949E-02 7. 967E-02 8.164E-02 FAIL ABUN CM-247 -1. lllE-02 4.326E-02 4.355E-02 NOT IDENT. CF-249 -4.551E-03 4.584E-02 4.588E-02 NOT IDENT. CF-251 3.599E-02 1.250E-01 1.261E-01 NOT IDENT. Page 4032 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 59.3957 87.09 119. 6387 136.47 76.2277 45.60 79.5984 87.57 119.7312 140.51 0.0000 46.54 74.5302 88.03 119.8196 143.76 83.4332 49. 72 0.0000 88.34 119.8798 144.24 51. 35 60.5064 88.47 119.9047 145.44 78.6787 51. 87 60.5771 89. 96 109. 5396 152.43 89.2211 52.39 72.3514 1093.63 109.6575 153.25 0.0000 52.97 72. 4445 91.11 0.0000 323.87 79.4648 53.44 73.5862 92.59 117. 6313 156.02 0.0000 54.07 74.7558 93.35 117.7700 158.56 0.0000 57.36 0.0000 94.56 117.9901 159.00 84.8776. 57.53 74.2361 94.65 118. 0057 162.33 78.5026 57.98 65.6907 94.67 118. 0096 162.66 0.0000 59.27 78.8245 94.87 118. 0457 163.33 82.7679 59.32 75.5929 97.43 73.8735 165.86 82. 9904 . 59.54 75.6271 98.43 66.2777 176.31 83.8948 60. 96 72.2348 98.44 66.2785 176.60 0.0000 61.17 72.2656 99.53 83.3692 177.52 72 .1191 62.93 97.9036 100 .11 78.8050 181.07 0.0000 63.29 97.9735 102.03 60.4329 181.52 66.4465 63.58 . 98.0296 103.18 79.1599 184.41 78.5974 64.28 103.2549 103.37 86.9451 143.76 78.6984 66.73 100.8236 105.21 87.5648 193.51 87.0507 67.24 92.1461 105.31 87.5771 197.03 84.7471 125.81 111.9858 106.12 85.7299 198.01 79.6315 67.75 111. 9998 106.47 85.7730 201.83 80.7847 69.67 102.4879 109.28 79.8504 203.43 64.3751 70.83 86.8783 111. 00 77. 6872 205.31 97.6012 72. 81 103.4505 111.76 0.0000 210.85 94.5901 72. 87 96. 0711 114. 06 63.0416 215.65 72 .1262 74.66 91.1915 116. 30 0.0000 222 .11 75.1895 74.82 91.2171 116.74 67.6192 227.09 71. 0701 74.97 91.2415 119.76 63.5234 227.38 73.7539 77 .11 91. 5869 121.12 82.3302 228.16 0.0000 78.74 91. 8465 121.22 82.3407 228.18 67.5793 79.69 91. 9966 121. 78 85.9839 116.74 67.5793 80.12 92.0642 122.06 83.6259 235.69 84.5630 80.19 0.0000 122.92 96.8747 235. 96 65.7854 80.57 92.1349 123.07 83.7354 238.63 75.3500 81. 00 97.4491 265.00 77.8153 238.98 0.0000 81. 07 97.4610 125.81 86.4311 240.99 75.4961 81. 75 91.5683 127.23 86.5863 242.00 75.5585 83.79 88.1154 127.91 81.8465 244.70 62.2028. 84.00 94.9268 129.30 81. 9889 252.40 0.0000 85.43 105.7228 131. 20 101.5214 252.80 53.5342 86.55 128.6120 133. 02 70.2556 254.15 0.0000 86.79 128.6621 133.52 58.1777 256.23 56.4086 86.94 119. 6090 136.00 81.0465 260.90 0.0000 Page 4033 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 50.3686 355.39 0.0000 584.27 27. 4119 264.80 48.3592 356.01 35.1079 595.83 0.0000 265.00 52.7637 364.49 *o. 0000 427.87 23.1875 268.22 44.0771 366.42 0.0000 602.52 0.0000 269.46 56.9872 372.51 43.3447 604.72 13.2729 270.03 57. 0112 375.05 45.3842 607.14 28.2330 271. 23 57.0629 377.52 44.4635 609.32 26.5967 273.65 0.0000 356.01 39.6712 610.33 26.6084 276.40 60.9807 388.16 45.7370 614.28 23.3208 277.37 51. 7788 388.63 0.0060 618.01 26.6934 277.60 48.0877 391.69 37.8608 620.36 23.3789 278.00 53.6528 264.66 49.0728 621. 93 10.0261 279.20 55.5518 401. 81 42.0897 630.19 0.0000 279.54 61.1230 402.40 47.1167 631.29 19.0109 279.70 61.1298 404.85 31.1198 633.25 27.9795 280.46 58.3845 410.95 34.2490 634.78 0.0000 283.69 57.5940 413.71 47.4169 635.95 25.7692 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.0853 423. 72 0.0000 645.85 21.3727 285.90 0.0000 427.09 33.5391 657.76 11. 3021 287*. 50 48.4379 427.87 33.5532 657.90 0.0000 290.67 50.4163 433.94 30.6030 661.66 19.2433 293.27 0.0000 439.40 33.7620 664.57 0.0000 351. 93 59.0112 453.88 44.3298 666.33 0,0000 295. 96 59.0420 463.37 44.5476 666.50 0.0000 879.38 70.4178 468.07 39.4627 667.71 0.0000 299.98 54.9806 473.00 0.0000 677.62 22.2104 300.09 54.9842 475.06 45.8557 685.70 0.0000 300.13 45 .1162 476.78 43.8090 695.00 0.0000 301.36 57.3848 477.60 42.7834 696. 49 20.6499 302.85 68.7449 482.18 35.5599 696. 51 20.6499 256.23 49.9689 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.9517 306.78 55. 7134 497.08 22.1254 697.49 20.6580 308.46 45.3789 505.52 25.3896 702.65 13.7988 311. 90 51.1710 507.63 0.0000 706.68 23.0322 316.51 42.7771 511. 00 30.7597 711. 68 17.3065 319.41 0.0000 514.00 30.2720 720.70 0.0000 320.08 0.0000 514.00 30.2720 721. 93 0.0000 0321. 04 41.0001 520.40 22.3732 722. 78 10.4268 323.87 45.8545 520.69 0.0000 722.91 10.4271 325.23 45.8955 522.65 0.0000 723. 31 6.9524 328.76 0.0000 527.90 0.0000 724.19 10.4319 333.37 50.4674 528.26 18.1787 727.33 18.5671 333.97 44.7177 529.59 19.2598 733.00 16.7449 334.37 50.5005 529.87 0.0000 735.93 18.6250 338.28 47.2534 531.02 0.0000 333.97 15.1413 338.32 47.2544 537.26 0.0000 739.50 0.0000 311. 90 52.1488 546.56 0.0000 747. 24 14. 9025 . 340.48 52.1488 552.55 24.8689 748.06 14.9066 340.55 0.0000 563.25 21.7293 752.31 21. 0769 344.28 48.4029 569.33 22.8765 753.82 0.0000 345.93 43.0270 946.00 19.6099 756.73 14.9528 351.06 34.0280 569.70 19.6121 756.80 14.9533 351 .. 93 34.0465 583.19 27.3997 884.68 23. 8096 Page 4034 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:04:44.51 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GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 7-DEC-2015 13:33:00. Acquisition date : 3-0CT-2016 07:01:16. Sample ID G405235049 -Sample quantity : l.47303E+02 GRAM Detector name GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.77 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 10 3 10 4 10 5 0 6 0 7 0 8 0 9 3 10. 3 11 3 . 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 5 27 5 28 3 29 3 30 0 31 0 32 0 33 0 34 0 Page 4036 of 5809 Energy 63.19* 73.22 74.90* 77.17 87. 63 . 92.73* 185.77* 207.99 238.66* 241.51 245.47 270.40 274.70 277.39 295.34 300.67 328.12* 338.02* 351.99* 432.80 471. 21 511.13* 576.91 583.28* 609.36* 661. 65 665.34 727 .15 731.15 743.62 768.25 794.57 809.82 860.63 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 48 33 93 205 86 78 31 32 380 87 41 23. 19 25 121 46 23 93 202 20 30 36 15 119 212 160 20 35 16 20 16 21 14 24 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 120 112 169 153 227 215 162 157 69 71 47 77 51 58 75 66 72 48 62 32 139 39 15 34 23 20 6 17 1 18 41 28 3 15 1.13 126.50 2.59 146.53 1.47 149.88 1.40 154.41 4.11 175.31 1.71 185.50 1.16 371. 33 0.62 415.73 1.17 477.00 1.62 482.69 1.63 490.60 0.53 540.40 1.37 549.00 0.70 554.37 1.13 590.25 0.74 600.90 1.58 655.74 0.88 675.52 1.39 703.44 1.01 864.90 11.76 941.67 2.65 1021.45 0.59 .1152.93 1.14 1165.67 1.45 l217.81 1.79 1322.34 2 .13 1329. 71 2.11 1453.29 2. 09 1461. 28 3.75 1486.23 2.55 1535.47 4.48 1588.09 0.74 1618.59 0.82 1720.19 122 144 144 144 171 182 367 410 470 470 470 536 545 552 586 596 647 671 698 861 921 1016 1149 1161 1211 1317 1317 1447 1447 1477 1523 1576 1615 1714 9 1. 35E-02 44. 7 18 9.05E-03 57.1 18 2.58E-02 29.0 18 5.71E-02 12.9 11 2.38E-02 35.7 13 2.16E-02 42.7 10 8.61E-03 83.1 13 8.90E-03 82.3 25 1. 05E-01 6. 4 25 2.41E-02 26.6 25 1.14E-02 37.3 9 6.35E-03 72.1 7 5.30E-03 66.7 8 7.06E-03 55.0 10 3.37E-02 16.0 11 1.27E-02 38.3 12 6.29E-03 79.0 10 2.59E-02 17.6 9 5.61E-02 10.0 8 5.47E-03 54.7 28 8.35E-03115.1 12 l.OlE-02 47.2 7 4.14E-03 50.9 12 3.31E-02 13.6 13 5.89E-02 8.4 17 4.44E-02 9.6 17 5.52E-03 42.2 18 9.70E-03 30.6 18 4.38E-03 33.1 18 5.65E-03 53.6 17 4.41E-03 97.0 16 5.77E-03 61.0 7 3.84E-03 34.8 12 6.71E-03 37.9 Fit 2.73E+OO 1. 83E+00 l.53E+00 8.28E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 23* 87 14 1. 32 1821. 40 1816 13 2.41E-02 14.1 36 0 969.41* 51 37 1. 57 1937.74 1929 15 1.42E-02 29.9 37 0 1015.67 7 8 1. 41 2030.29 2026 8 1.94E-03 79.5 38 0 1021.36 10 2 1. 90 2041. 66 2039 6 2.86E-03 36.7 39 0 1063.75* 10 12 0.74 2126.45 2119 12 2.82E-03 76.1 40 0 1097.44 9 12 0.49 2193.86 2184 12 2.54E-03 82.6 41 0 1121.55* 24 28 0.93 2242.10 2233 14 6.56E-03 52.3 42 0 1216.62 14 11 2.12 2432.32 2427 9 3.86E-03 51. 0 43 0 1267 :42 7 6 0.88 2533.97 2528 8 2.04E-03 68.1 44 0 1290.36 10 13 0.61 2579.88 2571 14 2.73E-03 86. 4 *45 0 1338.05 5 4 0.97 2675.30 2670 8 l.39E-03 82.5 46 0 1367.85 6 5 1.10"2734.94 2731 7 l.55E-03 80.4 47 0 1460.94* 322 4 1. 71 2921.28 2915 15 8.94E-02 5.8 48 0 1589.47 10 4 0.60 3178.58 3175 7 2.64E-03 46.0 49 0 1764.74* 31 0 2.92 3529.56 3521 15 8.56E-03 19.1 Flag: "*" = Peak area was modified by background subtraction Page 4037of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:04:46 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 13:33:00 G405235049 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:01:16 147.30 GRAM Sample type Detector name : Elapsed live* time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA33 0 01:00:00.00 1.50 keV No Linear 75. 00, Interference Report Interfering Nuclide Page 4038 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.-93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.77 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.133E+OO l.307E+Ol l.307E+Ol 11. 59 OK C0-58 810.76 99.45* 1. 810E+OO 4.00lE-02 7.582E-01 69.57 OK CD-109 88.03 3.70* 4.931E+OO 2.128E+OO 3.343E+OO 101.05 OK SN-126 64.28 9.60 2.441E+OO 1.346E+OO 1. 34.6E+00 89.42 OK 86.94 8.90 4.931E+OO 8.846E-01 8.846E-01 101.05 OK 87.57 37.00* 4.931E+OO 2.128E-01 2.128E-01 101.05 OK BA-137M 661. 66 89.90* 2 .115E+OO 4.469E-01 4.554E-01 19.25 OK CS-137 661.66 85.10* 2 .115E+OO 4.721E-01 4. 811E-01 19.25 OK TL-208 277.37 6.60 4.258E+OO 5.203E-01 5.203E-01 109.91 OK 583.19 85.00* 2.334E+OO 3. 231E-01 3.231E-01 27.18 OK 860.56 12.50 1. 727E+O'O 5.793E-01 5.793E-01 75.89 OK PB-212 74.82 10.28 3.808E+OO 1.002E+OO l.002E+00 89.84 OK 77 .11 17.10 4.039E+OO 1.906E+OO 1.906E+OO 25.78 OK 238.63 43.60* 4.775E+OO 1.064E+OO 1.064E+OO 12.85 OK 300.09 3.30 3.993E+OO 1.988E+OO l.988E+OO 76.62 OK BI-214 609.32 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 l.406E+OO 5.678E-01 5.680E-01 104.69 OK 1764.49 15.30 9. 591E-01 1.0lOE+OO 1. OllE+OO 38.27 OK *74.82 5.80 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.039E+OO 3.359E+OO 3.361E+OO 25.78 OK 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4.727E+OO Line Not Found <<INT Reject 295.22 . 18. 42 4. 051E+OO 9.297E-01 9.300E-01 32.05 OK 351. 93 35.60* 3.512E+OO 9.108E-01 9. lllE-01 20.02 OK RN-222 609.32 45.49* 2.255E+00 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 OK 1764.49 15.30 9.591E-01 1.0lOE+OO 1.0llE+OO 38.27 OK RA-224 240.99 4.10* 4.734E+OO 9.609E-01 9.609E-01 154.07 OK RA-:-226 609.32 45.49* 2.255E+OO l.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 l.406E+OO 5.678E-01 5.680E-01 104.69 OK 1764.49 15.30 9. 591E-01 1.0lOE+OO 1.0llE+OO 38. 27* OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.630E+OO 1.288E+OO 1.288E+OO 35.17 OK 794.95 4.25 l.836E+OO l.390E+OO 1.390E+OO 122.09 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 1.047E+OO 1.047E+OO 28.16 OK 968. 97 15.80 1.576E+OO 1.052E+OO 1.052E+OO 59.76 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.630E+OO 1.288E+OO 1.288E+OO 35.17 OK 794.95 4.25 1. 836E+OO 1.390E+OO 1.390E+OO 122.09 OK 835.71 1. 61 1.766E+OO Line Not Found Absent 911. 20 25.80* 1.653E+OO 1. 047E+OO 1. 047E+OO 28.16 OK 968. 97 15.80 1.576E+OO 1.052E+OO 1.052E+OO 59.76 OK TH-228 74.82 10.28 3.808E+OO 1.002E+OO 1.002E+OO 89.84 OK 77 .11 17.10 4.039E+OO 1. 906E+OO 1.906E+OO 25.78 OK 238.63 43.60* 4.775E+OO 1.064E+OO 1.064E+OO 12.85 OK 300.09 3.30 3.993E+OO 1. 988E+OO. l.988E+OO 76.62 OK TH-230 609,32 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 1. 406E+00-5.678E-01 5.678E-01 104.69 OK Page 4039 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 1764.49 15.30 9. 591E-01 l.OlOE+OO l.OllE+OO 38.27 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent 301.36 5.35* 3.993E+OO l.227E+OO l.227E+OO 76.62 OK TH-232 105.21 i.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.630E+OO 1. 288E+OO 1. 288E+OO 35.17 OK _, 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* l.653E+OO 1. 047E+OO 1. 047E+OO 28.16 OK 968. 97 15.80 1. 57 6E+OO l.052E+OO l.052E+OO 59.76 OK TH-234 63. 29 3.70* 2.441E+OO 3.492E+OO 3.492E+OO 89.42 OK 92.59 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 OK u-234* 609.32 45.49* 2.255E+OO l.106E+OO l.106E+OO 16.85 OK 1120. 29 14.92 1. 406E+OO 5.678E-01 5.678E-01 104.69 OK 1764.49 15.30 9.591E-01 1.0lOE+OO 1.0lOE+OO 38.27 OK U-238 63.29 3.70* 2.441E+OO 3.492E+OO 3.492E+OO 89.42 OK 92.59 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 OK AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.808E+OO l.533E-01 1.533E-01 89.84 OK ANH-511 511. 00 100.00* 2.592E+00 7.630E-02 7.630E-02 94.30 OK Flag: "*" = Keyline Page 4040 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:47.40 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l * *Acquisition date 3-0CT-2016 07:01:16 Sensitivity : 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
Sample date 7-DEC-2015 13:33:00 Analyst initials: MXRl *
Sample ID G405235049 Sample Quantity l.4730E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
Combined Activity-MDA NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.307E+Ol 1.484E+OO C0-58 7.582E-01 5.170E-01 CD-109 3.343E+OO 3.310E+OO SN-126 2.128E-01 2.107E-01 BA-137M 4.554E-01 8.590E-02 CS-137 4. 811E-01 9.075E-02 TL-208 3.231E-01 8.606E-02 PB-212 1.064E+OO 1.340E-01 BI-214 1.106E+OO 1.826E-01 PB-214 9. lllE-01 1. 788E-Ol RN-222 1.106E+OO 1.826E-01 RA-224 9.609E-01 1. 451E+OO RA-226 1.106E+OO l.826E-01 AC-228 1.047E+OO 2.889E-01 RA-228 1. 047E+OO 2.889E-01 TH-228 1. 064E+OO 1.340E-01 TH-230 1.106E+OO l.826E-01 PA-231 l.227E+OO 9.209E-01 TH-232 1. 047E+OO 2.889E-01 TH-234 3.492E+OO 3.061E+OO U-234 1.106E+OO l.825E-01 U-238 3.492E+OO 3.061E+OO AM-243 1.533E-Ol l.350E-01 ANH-511 7.630E-02 7.052E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4041 of 5 809 Key-Line Activity (pCi/GRAM -l.221E+Ol 2.539E-02 O.OOOE+OO 7.665E-03. -1.930E-01 O.OOOE+OO K.L. Cnt Uncert (1.96-sigma) i.055E+Ol 4.514E-02 l.575E+41 2.004E-02 3.950E-01 1. 631E+04 MDA (pCi/GRAM 5.034E-01 7.993E-01 2.225E+OO 1.425E-01 6.954E-02 7.346E-02 6.056E-02 l.OOlE-01 l.091E-01 l.315E-01 1. 091E-01 1. 073E+oo 1.091E-01 2.024E-01 2.024E-01 l.OOlE-01 1.090E-01 6. 541E-01 2.024E-01 2.449E+OO 1.090E-01 2.449E+OO 9.399E-02 5.863E-02 MDA (pCi/GRAM l.738E+Ol 9.975E-02 O.OOOE+OO 5.442E-02 7.000E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.940E+02 O.OOOE+OO SHORT HLIF MN-54 -4.259E-03 6.172E-02 1.173E-01 NOT IDENT. C0-56 -3.144E-02 4. 413E-01 8.455E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 -7.400E-03 4.603E-02 8.555E-02 NOT IDENT. FE-59 1.278E+OO 5. 854E+OO l.153E+Ol FAIL ABUN C0-60 6.073E-05 3.063E-02 5.900E-02 NOT IDENT. ZN-65 -7.186E-02 1. 911E-01 3.126E-01 NOT IDENT. GE-68 -1.254E-01 2.033E+OO 4.166E+OO NOT IDENT. AS-73 2.037E+OO 1.171E+Ol 2.348E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.171E+03 O.OOOE+OO SHORT HLIF SE-75 -7.025E-02 2.272E-01 3.949E-01 NOT IDENT. BR-77 O.OOOE+OO 3.132E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.490E+02 O.OOOE+OO SHORT HLIF RB-83 1. 911E-01 6.309E-01 1.288E+OO NOT IDENT. KR-85 5.945E+OO 7.189E+OO 1. 421E+Ol NOT IDENT. SR-85 6.302E-01 7.663E-01 1.514E+OO NOT IDENT. RB-86 O.OOOE+OO 2.525E+04 O.OOOE+OO SHORT HLIF Y-88 -l.244E-01 1.779E-01 2.891E-01 NOT IDENT. Y-91 1. 748E+02 5.545E+02 l.153E+03 NOT IDENT. NB-94 -3. 501E-02 3 .117E-02 4.921E-02 NOT IDENT. NB-95 5.625E-01 9.123E-01 1.882E+OO NOT IDENT. NB-95M l.092E-01 2.721E+OO 4.528E+OO NOT IDENT. ZR-95 3.557E-01 1.129E+OO 2.392E+OO NOT IDENT. NB-97. O.OOOE+OO 1.601E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+CiO 1. 929E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 782E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101* 1.786E-02 3.229E-02 6.345E-02 NOT IDENT. RH-102 2. 911E-04 5.074E-02 l.006E-01 FAIL ABUN RU-103 2.516E+OO 5.743E+OO 1.184E+Ol FAIL ABUN RH-106 -2.765E-01 4.620E-01 8.209E-Oi NOT IDENT. RU-106 -2.765E-01 4.620E-01 8.209E-01 NOT IDENT. AG-108M 4.062E-02 4.355E-02 6.170E-02 FAIL ABUN AG-llOM 2.267E-02 9.083E-02 l.856E-01 NOT IDENT. SN-113 l.497E-01 2.129E-01 4.533E-01 NOT IDENT. CD-115 O.OOOE+OO 4.184E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O;OOOE+OO 1. 046E+05 O.OOOE+OO SHORT HLIF TE-123M 3.333E-02 1.283E-01 2.434E-01 NOT IDENT. SB-124 2.304E+00 1. 989E+OO 5.375E+OO NOT IDENT. SB-125 l.073E-03 9.645E-02 1.834E-01 NOT IDENT. TE-125M 1.209E+02 2.879E+02 5.587E+02 NOT IDENT. I-126 O.OOOE+OO 1.266E+06* O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.276E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.428E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.319E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.054E+26 O.OOOE+OO SHORT HLIF BA-133 8.003E-03 4.236E-02 8.152E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 9.106E-02 l.090E-01 1.082E-01 FAIL ABUN CS-135 -2.384E-03 1.586E-01 2.617E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.902E+05 O.OOOE+OO SHORT HLIF CE-139 -2.357E-02 1.125E-01 2.036E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 2 65E+O 6 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 2.844E+05 O.OOOE+OO SHORT HLIF CE-141 -l.131E+Ol 2.447E+Ol 4.363E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 l.190E-01 3.591E-01 6.890E-01 NOT IDENT. PM-144 1. 731E-03 5.304E-02 1.031E-01 NOT IDENT. PR-144 l.972E-01 4.617E+OO 8.987E+OO NOT IDENT. PM-146 -9.144E-03 4.275E-02 8.190E-02 NOT IDENT. ND-147 O.OOOE+OO 3 .196E+07 O.OOOE+OO SHORT HLIF PM-147 1. 761E+02 7.686E+02 l.483E+03 NOT IDENT. PM-149 0.000E+OO 5. 964E+40 O.OOOE+OO SHORT HLIF EU-150 -7.554E-03 2.361E-02 4.062E-02 FAIL ABUN EU-152 -1. 92 6E-02 7.680E-02 l.499E-01 FAIL ABUN GD-153 -5.941E-02 l.948E-01 3.301E-01 NOT IDENT. EU-154 6.468E-02 1. lllE-01 2.460E-01 NOT IDENT. EU-155 -2.088E-02 1.098E-01 2.047E-01 FAIL ABUN TB-160 1.574E+OO 1. 755E+OO 3.931E+OO FAIL ABUN H0-166M -2.492E-02 5.337E-02 9.579E-02 FAIL ABUN TM-171 -1.740E+Ol 2.827E+Ol 5.313E+Ol NOT IDENT. HF-172 -7.752E-02 2.060E-01 3.754E-01 FAIL ABUN LU-172 -4.987E-02 8.386E-02 l.298E-01 FAIL ABUN LU-176 1.997E-02 2.346E-02 4.998E-02 FAIL ABUN HF-181 -9.543E-01 3.924E+OO 7.531E+OO NOT IDENT. Page 4042 of 5809 TA-182 9.744E-03 9.093E-01 1.709E+OO FAIL ABUN RE-183 -2.148E+OO 3.507E+OO 6.554E+OO NOT IDENT. RE-184 1.519E+OO 3.528E+Ol 6.697E+Ol NOT IDENT. W-188 3.457E+Ol l.054E+02 2.084E+02 FAIL ABUN IR-192 -3.428E-01 4.034E-01 7.359E-01 FAIL ABUN HG-203 -4.527E-01 2.589E+OO 4.554E+OO FAIL ABUN BI-207 4.788E-02 7. 142E-02 . 1.033E-01 FAIL ABUN PB-210 2.201E+OO 5.293E+OO 1.093E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.925E-01 8.068E-01 FAIL ABUN PB-211 -9.557E-02 6.164E-01 L 198E+OO NOT IDENT. BI-212 O.OOOE+OO 8.393E-01 1. 35.4E+OO FAIL ABUN RN-219 7.810E-02 3.837E-01 7. 681E-01 FAIL ABUN RA-223 -3.259E-02 5.823E-01 1.039E+OO FAIL ABUN AC-227 6.674E-02 2. 077E-Ol. 3.940E-01 FAIL ABUN TH-227 6.674E-02 2.077E-01 3.940E-01 FAIL ABUN TH-229 -9 .114E-03 4.860E-01 8.849E-01 FAIL ABUN TH-231 -3.259E-02 5.823E-01 1.039E+OO FAIL ABUN PA-233 -2.429E-02 4. 963E-02 9.468E-02 FAIL ABUN PA-234 1. 804E-01 2.888E-01 6.058E-01 NOT IDENT. PA-234M -2.468E+OO 4.834E+OO 8.513E+OO NOT IDENT. U-235 -8.013E-02 1. 749E-01 3.193E-01 FAIL ABUN NP-237 -2.429E-02 4. 963E-02 9.468E-02 FAIL ABUN NP-238 0.000E+OO 1. 228E+41 O.OOOE+OO SHORT HLIF -2.527E-Oi 2.467E-01 4.238E-01 FAIL ABUN PU-239 8.0llE+Ol 3.009E+02 5.759E+02 . NOT IDENT. AM-241 9.052E-02 l.635E-01 3.147E-01 NOT IDENT. CM-243 -2.619E-03 9.952E-02 1.885E-01 FAIL ABUN BK-247 -4.551E-02 7. 741E-02 *l.301E-01 NOT IDENT. CM-247 l.137E-02 3.279E-02 6.713E-02 FAIL ABUN CF-249 3.025E-02 3.318E-02 7.239E-02 NOT IDENT. CF-251 7.615E-04 1.213E-01 2.223E-01 NOT IDENT. Page 4043 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:04:45.25 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 310 10.66* 1.133E+OO 1.307E+Ol l.307E+Ol 11. 59 C0-58 810.76 14 99.45* 1.810E+OO 4.00lE-02 7.582E-01 69.57 CD-109 88.03 107 3.70* 4.931E+OO 2.985E+OO 4.689E+OO 71. 45 SN-126 64.28 62 9.60 2.441E+OO l.346E+OO l.346E+00 89.42 86.94 107 8.90 4. 931E+OO 1.241E+OO 1.241E+00 71. 45 87.57 107 37.00* 4.931E+OO 2.985E-01 2.985E-01 71. 45 BA-137M 661.66 167 89.90* 2 .115E+OO 4.469E-01 4.554E-01 19.25 CS-137 661.66 167 85.10* 2 .115E+OO 4.721E-01 4. BllE-01 19.25 TL-208 277.37 29 6.60 4.258E+OO 5.203E-01 5.203E-01 109.91 583.19 126 85.00* 2.334E+OO 3. 231E-01 3. 231E-01 27.18 860.56 25 12.50 1. 727E+OO 5.793E-01 5.793E-01 75.89 BI-211 72. 87 41 1.23 3.629E+OO 4.698E+OO 4.698E+OO 114.29 351. 06 223 12.92* 3.512E+OO 2.510E+OO 2.510E+00 20.02 PB-212 74.82 117 10.28 3.BOBE+OO l.527E+OO 1.527E+OO 57.94 77 .11 258 17.10 4.039E+00 1.906E+OO l.906E+00 25.78 238'.63 434 43.60* 4.775E+OO l.064E+00 1.064E+OO 12.85 300.09 51 3.30 3.993E+OO 1. 988E+OO l.988E+OO 76.62 BI-214 609.32 223 45.49* 2.255E+OO 1.106E+OO . 1.106E+00 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO 1. OllE+OO 38.27 PB-214 74.82 117 5.80 3.BOBE+OO 2.706E+OO 2.707E+OO 57.94 77 .11 258 9.70 4.039E+OO 3.359E+OO 3.361E+OO 25.78 87.09 107 3.41 4. 931E+OO 3.238E+OO 3.240E+OO 71. 45 242.00 99 7.25 4.734E+OO 1.473E+00 1.474E+OO 53 .11 295.22 136 18.42 4. 051E+OO 9.297E-01 9.300E-01 32.05 351.93 223 35.60* 3.512E+OO 9.lOBE-01 9. lllE-01 20.02 RN-222 609.32 223 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16. 85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO 1. OllE+OO 38.27 RA-224 240.99 99 4.10* 4.734E+OO 2.605E+OO 2.605E+OO 53 .11 RA-22 6 609.32 223 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 1764.49 29 15. 30. 9.591E-01 1.0lOE+OO 1. OllE+OO 38.27 AC-2,28 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 103 11. 27 3.630E+OO 1.288E+OO 1.288E+00 35.17 794.95 21 4.25 1.836E+OO 1.390E+OO 1.390E+OO 122.09 835. 71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 BB 25.80* 1.653E+OO 1. 04.7E+00 1. 047E+OO 28.16 968. 97 51 15.80 1.576E+OO 1.052E+OO 1.052E+OO 59.76 RA-228 105.21 ------1.10 5. 839E+OO-------Line Not Found ------338.32 103 11. 27 3.630E+OO 1.288E+OO 1.288E+OO 35.17 794.95 21 4.25 l.836E+00 l.390E+00 1.390E+OO 122.09 835.71 ------1. 61 1. 7 6*6E+OO ------Line Not Found ------911. 20 88 25.80* 1.653E+00 1.047E+OO 1.047E+OO 28.16 968. 97 51 15.80 1.576E+00 1.052E+OO 1.052E+OO 59.76 TH-228 74.82 117 10.28 3.808E+OO 1.527E+OO 1.527E+OO 57.94 77 .11 258 17.10 4.039E+OO 1.906E+OO 1.906E+OO 25.78 Page 4044 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 434 43.60* 4.775E+OO l.064E+OO 1.064E+OO 12.85 300.09 51 3.30 3.993E+OO 1.988E+OO 1.988E+OO 76.62 TH-230 609.32 223 45.49* 2.255E+OO l.106E+OO 1.106E+OO 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.678E-01 104.69 1764.49 29 15.30 9. 591E-01
1.0lOE+OO 1. OllE+OO 38.27 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 51 5.35* 3.993E+OO l.227E+OO 1.227E+00 76. 62 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 103 11. 27 3.630E+OO 1.288E+OO l.288E+OO 35.17 835. 71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 88 1.653E+OO 1.047E+OO 1. 047E+OO 28.16 968. 97 51 15.80 l.576E+OO 1.052E+OO l.052E+00 59. 76 TH-234 63.29 62 3.70* 2.441E+00 3.492E+OO 3.492E+OO 89.42 92.59 96 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 U-234 609.32 223 45.49* 2.255E+OO 1.106E+OO l.106E+OO 16.85 . 1120. 29 23 14.92 1.406E+OO 5.678E-01 5.678E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO l.OlOE+OO 38.27 U-238 63.29 62 3.70* 2. 441E+OO 3.492E+OO 3.492E+OO 89.42 92.59 96 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 117 67.20* 3.808E+OO 2.336E-01 2.336E-01 57.94 ANH-511 511. 00 39 100.00* 2.592E+OO 7.630E-02 7.630E-02 94.30 Flag: "*" = Keyline Page 4045 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Total number of lines in spectrum 49 Number of unidentified lines 11 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 70.86D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600. OOY 1.4lE+lOY 1600.00Y 1. 41E+10Y 1.41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 19.0 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Grand Total Activity Uncorrected pCi/GRAM 1.307E+Ol 4*. OOlE-02 2.985E+OO 2.985E-01 4.469E-01 4.721E-01 3. 231E-01-2. 510E+OO l.064E+OO l.106E+OO 9.108E-01 l.106E+00 2.605E+OO l.106E+OO 1.047E+OO 1.047E+OO 1.064E+OO l.106E+OO l.227E+OO l.047E+OO 3.492E+OO l.106E+00 3.492E+OO 2.336E-01 7.630E-02 4.297E+Ol 4.297E+Ol Decay Corr pCi/GRAM 1.307E+Ol 7.582E-01 4.689E+OO 2.985E-01 4.554E-01 4. 811E-01 3.231E-01 2.510E+00 1. 064E+OO 1.106E+OO 9. lllE-01 1.106E+OO 2.605E+OO 1.106E+OO l.047E+OO L 04 7E+00 1.064E+OO l.106E+OO 1.227E+OO 1. 04 7E+OO 3.492E+OO 1.106E+OO 3.492E+OO 2.336E-01 7.630E-02 4.542E+Ol 4.542E+Ol 77.55% Decay Corr 2-Sigma Error 0 .151E+Ol 5.275E-Ol 3.350E+OO 2 .132E-01 0.877E-01 0.926E-01 0.878E-01 0.503E+00 0.137E+OO 0.186E+OO 1.824E-01 0.186E+OO 1.384E+OO 0.186E+OO 0.295E+OO 0.295E+OO 0.137E+OO 0.186E+OO 0.940E+OO 0.295E+OO 3.123E+OO 0.186E+OO 3.123E+OO l.353E-01 7.196E-02 "M" Manually accepted : 2-Sigma %Error 11. 59 69.57 71.45 71. 45 19.25 19.25 27.18 20.02 12.85 16.85 20.02 16.85 53.11 16.85 28.16 28.16 12.85 16.85 76.62 28.16 89.42 "16. 85 89.42 57.94 94.30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4046 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235049 Acquisition date : 3-0CT-2016 07:01:16 It . Energy. Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 185.77 36 189 1.16 371. 33 367 10 8.61E-03 **** 5.62E+OO T 0 207.99 37 182 0.62 415.73 410 13 8.90E-03 **** 5.25E+OO 3 245.47 47 54 1. 63 490.60 470 25 l.14E-02 74.5 4.68E+OO T 0 270.40 26 87 0 .. 53 540.40 536 9 6.35E-03 **** 4.34E+OO T 0 274.70 22 58 1. 37 549.00 545 7 5.30E-03 **** 4.29E+OO T 0 328.12 25 80 1. 58 655.74 647 12 6.29E-03 **** 3. 72E+OO . T 0 432.80 21 35 1. 01 864.90 861 8 5.47E-03 **** 2.96E+OO T 0 471. 21 32 150 11. 76 941.67 921 28 8.35E-03 **** *2.77E+OO 0 576.91 16 16 0.59 1152. 93 1149 7 4.14E-03 **** 2.35E+OO 5 665.34 21 6 2.13 1329.71 1317 17 5.52E-03 84.4 2. llE+OO T 3 727.15 36 17 2 .11 1453.29 1447 18 9.70E-03 61.1 1. 97E+OO T 3 731.15 16 1 2.09 1461. 28 1447 18 4.38E-03 66.3 1. 96E+OO 0 743.62 21 18 3.75 1486.23 1477 18 5.65E-03 **** 1. 93E+OO 0 768.25 16 42 2.55 1535.47 1523 17 4.41E-03 **** l.88E+OO T 0 1015.67 7 8 1. 41 2030.29 2026 8 l.94E-03 **** 1.52E+OO 0 1021. 36 10 2 1. 90 2041. 66 2039 6 2.86E-03 73.4 1. 51E+OO T 0 1063.75 10 12 0.74 2126.45 2119 12 2.82E-03 **** 1. 4 7E+OO T 0 1097.44 9 12 0.49 2193.86 2184 12 2.54E-03 **** 1.43E+OO 0 1216. 62 14 11 2.12 2432.32 2427 9 3.86E-03 **** l.32E+00 0 1267.42 7 6 0.88 2533.97 2528 8 2.04E-03 **** 1.28E+OO 0 1290.36 10 13 0.61 2579.88 2571 14 2.73E-03 **** 1.26E+OO T 0 1338.05 5 4 0.97 2675.30 2670 8 1.39E-03 **** 1.22E+OO 0 1367.85 5 5 1.10 2734.94 2731 7 1.55E-03 **** 1.20E+OO T 0 1589.47 9 3 0.60 3178.58 3175 7 2.64E-03 92.1 1. 05E+OO Flags: "T" .= Tentatively associated Page 4047of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:59.82 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMP.LE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l *
Acquisition date 3-0CT-2016 07:01:16 Sensitivity 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
Sample date 7-DEC-2015 13:33:00 Nuclide Library : SOLID *
Sample ID G405235049 Analyst initials: MXRl *
Batch Number Sample Quantity : 1.4730E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************** * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File . : DKAlOO: [CANBERRA. GAMMA] EFF GAM33 CAN. CNF; 8 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to.Certificate of Analysis.* Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM l.943E-01 3.255E-01 1.050E+OO 6. 725E-02 3.099E-02 3.274E-02 2. 672E-02 4.661E-02 4.765E-02 6.003E-02 4.765E-02 4.997E-01 4.765E-02 8.478E-02 8.478E-02 4.661E-02 4.764E-02 2.934E-01 8.478E-02 1.143E+OO 4.764E-02 l.143E+00 4.409E-02 2.658E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4048 of 5809 Le' (pCi/GRAM 7.438E+OO 4.306E-02 O.OOOE+OO 1.983E-02 2.999E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 . EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 .LU-176 HF-181 TA-182 Page 4049 of 5809 5.093E-02 3. 631E-01 O.OOOE+OO 3.980E-02 4.828E+OO 2.318E-02 1.334E-01 1. 761E+OO 1.094E+Ol O.OOOE+OO 1. 817E-01 O.OOOE+OO O.OOOE+OO 5.747E-01 6.435E+OO 6.856E-01 O.OOOE+OO 9.138E-02 5.053E+02 2. lllE-02 8.443E-01 2.108E+OO 1.020E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 968E-02 4.360E-02 5.325E+OO 3.543E-01 3.543E-01 2.819E-02 7. 966E-02 2.058E-01 O.OOOE+OO O.OOOE+OO 1.135E-01 2.223E+OO 8.188E-02 2.622E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.727E-02 O.OOOE+OO 4. 821E-02 1.206E-01 O.OOOE+OO O.OOOE+OO 9.485E-02 O.OOOE+OO O.OOOE+OO 2.033E+Ol O.OOOE+OO 3.226E-01 4.537E-02 3.956E+OO 3.670E-02 O.OOOE+OO 6.898E+02 O.OOOE+OO l.824E-02 6.713E.:.02 1.542E-01 l.063E-01 9.568E-02 1. 721E+OO 4.138E-02 2.460E+Ol l.736E-01 5.440E-02 2.305E-02 3.321E+OO 7.333E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT*. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251* Page 4050 of 5809 3.037E+OO 2.950E+Ol 9.555E+Ol 3.299E-01 2.095E+OO 4.516E-02 5.083E+OO 3.878E-01 5.388E-01 6.233E-01 3.498E-01 4.717E-01 1. 803E-01 1.803E-01 4.126E-01 4.717E-01 4.254E-02 2.666E-01 3.715E+OO l.489E-01 4.254E-02 O.OOOE+OO 1. 968E-01 2.694E+02 1.469E-01 8.807E-02 5. 962E-02 3.042E-02 3.286E-02 1.039E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:05.52 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l * *Acquisition date 3-0CT-2016 07:01:16 Sensitivity : 3.000 *
Detector ID _ GAM33 Energy tolerance:-1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
Sample date 7-DEC-2015 13:33:00 Nuclide Library : SOLID *
Sample ID G405235049 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity l.4730E+02 GRAM *
Quantity Err(%) l.3577E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 10-JUN-2016' 07:00:49 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 l.307E+Ol l.632E+OO C0-58 7.582E-01 5.180E-01 CD-109 3.343E+OO 3.326E+OO SN-126 2.128E-01 2 .114E-01 BA-137M 4.554E-01 8.810E-02 CS-137 4. 811E-01 9.306E-02 TL-208 3. 231E-01 8.714E-02 PB-212 l.064E+OO l.452E-01 BI-214 l.106E+OO 1. 887E-01 PB-214 9. lllE-01 l.827E-01 RN-222 l.106E+OO l.887E-01 RA-224 9.609E-01 l.456E+OO RA-226 l.106E+OO 1. 8-87E-01 AC-228 1. 047E+OO 2.938E-01 RA-228 1. 047E+OO 2.938E-01 -TH-228 l.064E+00 l.452E-01 TH-230 l.106E+OO 1. 886E-01 PA-231 1. 227E+OO* 9.574E-01 TH-232 l.047E+OO 2.938E-01 TH-234 3.492E+00 3.157E+OO U-234 l.106E+OO l.886E-01 U-238 3.492E+OO 3.157E+OO AM-243 l.533E-01 l.357E-01 ANH-511 7.630E-02 7.058E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 4051 of 5 809 Key-Line Activity (pCi/GRAM -l.221E+Ol 2.539E-02 l.000E+41 7.665E-03 -l.930E-01 1. 153E+04 K.L Act error ( 1. 96-sigma) l.056E+Ol 4.515E-02 l.635E+41 2.004E-02 3.950E-01 l.632E+04 TPU ( 1. 96-sigma) l.632E+OO 5.180E-01 3.326E+OO 2 .114E-01 8.810E-02 9.306E-02 8.714E-02 l.452E-01 l.887E-01 l.827E-01 l.887E-01 l.456E+OO l.887E-01 2.938E-01 2.938E-01 l.452E-01 1. 886E-01 9.574E-01 2.938E-01 3.157E+OO 1. 886E-01 3.157E+OO l.357E-01 7.058E-02 TPU (1. 96-sigma) l .191E+Ol 4.658E-02 O.OOOE+OO 2.034E-02 4.045E-01 1. 713E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 2.755E+02 3.941E+02 4.133E+02 SHORT HLIF MN-54 -4.259E-03 6.172E-02 6.175E-02 NOT IDENT. C0-56 -3.144E-02 4.413E-01 4.415E-01 NOT IDENT. MN-56 -l.000E+41 l.329E+42 O.OOOE+OO SHORT HLIF C0-57 -7.400E-03 4.604E-02 4.616E-02 NOT IDENT. FE-59 1.278E+OO 5.854E+OO 5.883E+00 FAIL ABUN C0-60 6.073E-05 3.063E-02 3.063E-02 NOT IDENT. ZN-65 -7.186E-02 l.911E-01 1.938E-01 NOT IDENT. GE-68 -1.254E-01 2.033E+OO 2.034E+OO NOT IDENT. AS-73 2.037E+OO 1.172E+Ol 1. 176E+Ol NOT IDENT. AS-74 2.445E+03 6.174E+03 6. 271E+03 SHORT HLIF SE-75 -7.025E-02 2.273E-01 2.294E-01 NOT IDENT. BR-77 2.487E+38 2.159E+39 O.OOOE+OO SHORT HLIF SR-82 -8.216E+Ol 7.490E+02 7.499E+02 SHORT HLIF RB-83 1. 911E-01 6.315E-01 6.373E-01 NOT IDENT. KR-85 5.945E+OO 7.193E+OO 7.676E+OO NOT IDENT. SR-85 6.302E-01 7.667E-01 8.177E-01 NOT IDENT. RB-86 -1.557E+03 2.525E+04 2.526E+04 SHORT HLIF Y-88 -1.244E-01 1. 781E-01 1. 867E-01 NOT IDENT. Y-91 1. 748E+02 5.546E+02 5. 601E+02 NOT IDENT. NB-94 -3.501E-02 3.121E-02 3.497E-02 NOT IDENT. NB-95 5.625E-01 9.126E-01 9.472E-01 NOT IDENT. NB-95M 1.092E-01 2.721E+OO 2.722E+OO NOT IDENT. ZR-95 3.557E-01 1.129E+OO 1.140E+OO NOT IDENT. NB-97 1.000E+41 1.601E+41 0.000E+OO SHORT HLIF ZR-97 1.000E+41 1. 929E+41 O.OOOE+OO SHORT HLIF M0-99 -1.303E+32 l.785E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 1.025E+42 O.OOOE+OO SHORT HLIF RH-101 1.786E-02 3.245E-02 3.343E-02 NOT IDENT. RH-102 2. 911E-04 5.074E-02 5.074E-02 FAIL ABUN RU-103 2.516E+OO 5.744E+OO 5.855E+OO FAIL ABUN RH-106 -2.765E-01 4.623E-01 4.788E-01 NOT IDENT. RU-106 -2.765E-01 4.623E-01 4.788E-01 NOT IDENT. AG-108M 4.062E-02 4.358E-02 4.727E-02 FAIL ABUN AG-llOM 2.267E-02 9.083E-02 9 .141E-02 NOT IDENT. SN-113 l.497E-01 2 .130E-01 2.234E-01 NOT IDENT. CD-115 -1.335E+39 4.191E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -8.136E+04 1.050E+05 1.113E+05 SHORT HLIF TE-123M 3.333E-02 l.283E-01 l.292E-01 NOT IDENT. SB-124 2.304E+OO 1.993E+OO 2.247E+OO NOT IDENT. SB-125 l.073E-03 9.645E-02 9.646E-02 NOT IDENT. TE-125M l.209E+02 2.880E+02 2. 931E+02 NOT IDENT. I-126 l.530E+06 1.283E+06 1.457E+06 SHORT HLIF SB-126 -2.492E+05 l.277E+06 1. 282E+06. SHORT HLIF SB-127 8.943E+21 2.723E+22 O.OOOE+OO SHORT HLIF I-131 -1. 7 45E+09 5.320E+09 5.377E+09 SHORT HLIF I-132 -1.000E+41 1.906E+42 O.OOOE+OO SHORT HLIF TE-132 -3.481E+26 5.249E+26 O.OOOE+OO SHORT HLIF BA-133 8.003E-03 4.237E-02 4.252E-02 FAIL ABUN I-133 l.OOOE+41 5.820E+42 O.OOOE+OO SHORT HLIF CS-134 9.106E-02 1.090E-01 l.165E-01 FAIL ABUN CS-135 -2.384E-03 1.586E-01 1. 586E-01 NOT IDENT. I-135 -1.000E+41 7.400E+41 O.OOOE+OO SHORT HLIF CS-136 1.383E+05 2.906E+05 2.972E+05 SHORT HLIF CE-139 -2.357E-02 1.126E-01 1.131E-01 NOT IDENT. BA-140 -1.282E+05 1.265E+06 l.267E+06 SHORT HLIF . LA-140 -5.470E+04 2.844E+05 2.855E+05 SHORT HLIF CE-141 -1.131E+Ol 2.447E+Ol 2.500E+Ol NOT IDENT. CE-143 l.OOOE+41 1.787E+42 O.OOOE+OO SHORT HLIF CE-144 1.190E-01 3.591E-01 3. 631E-01 NOT IDENT. PM-144 1. 731E-03 5.304E-02 5.305E-02 NOT IDENT. PR-144 1. 972E-01 4.617E+OO 4.618E+OO NOT IDENT. PM-146 -9.144E-03 4.276E-02 4.296E-02 NOT IDENT. ND-147 9.035E+06 3 .196E+07 3.222E+07 SHORT HLIF PM-147 1. 761E+02 7.686E+02 7.727E+02 NOT IDENT. PM-149 8.219E+39 *5. 966E+40 O.OOOE+OO SHORT HLIF EU-150 -7.554E-03 2.361E-02 2.386E-02 FAIL ABUN EU-152 -1. 926E-02 7.680E-02 7.729E-02 FAIL ABUN GD-153 -5.941E-02 *1.948E-01 1. 967E-01 NOT IDENT. EU-154 6.468E-02 1.112E-01 1.149E-01 NOT IDENT. EU-155 -2.088E-02 1.098E-01 1.102E-01 FAIL ABUN TB-160 1.574E+00 1. 757E+OO 1. 8 95E+OO FAIL ABUN H0-166M -2.492E-02 5.338E-02 5.455E-02 FAIL ABUN TM-171 -1. 740E+Ol 2.831E+Ol 2.938E+Ol NOT IDENT. HF-172 -7.752E-02 2.063E-01 2.093E-01 FAIL ABUN LU-172 -4.987E-02 8.401E-02 8.697E-02 FAIL ABUN LU-176 l.997E-02 2.348E-02 2.515E-02 FAIL ABUN HF-181 -9.543E-01 3.925E+OO 3.948E+OO NOT IDENT. Page 4052 of 5809 TA-182 9 . .744E-03 9.093E-01 9.093E-01 FAIL ABUN RE-183 -2.148E+OO 3.523E+00 3.654E+OO NOT IDENT. RE-184 1.519E+OO 3.528E+Ol 3.529E+Ol NOT IDENT. W-188 3.457E+Ol l.055E+02 1.067E+02 FAIL ABUN IR-192 -3.428E-01 4.036E-01 4.322E-01 FAIL ABUN HG-203 -4.527E-01 2.589E+OO 2.597E+OO FAIL ABUN BI-207 4.788E-02 7.144E-02 7.463E-02 FAIL ABUN PB-210 2.201E+OO 5.297E+OO 5.389E+OO NOT IDENT. BI-211 2.510E+OO 5.050E-01 l.239E+OO FAIL ABUN PB-211 -9.557E-02 6.164E-01 6.180E-01 NOT IDENT. BI-212 1.401E+OO 8.423E-01 l.053E+OO FAIL ABUN RN-219 7.810E-02 3.838E-01 3.855E-01 FAIL ABUN RA-223 -3.259E-02 5.823E-01 5.825E-01 FAIL ABUN AC-227 6.674E-02 2.079E-01 2.lOlE-01 FAIL ABUN TH-227 6.674E-02 2.079E-01 2. lOlE-01 FAIL ABUN TH-229 -9.114E-03 4.860E-01 4.860E-01 FAIL ABUN TH-231 -3.259E-02 5.823E-01 5.825E-01 FAIL ABUN PA-233 -2.429E-02 4. 965E-02 5. 084E-02
FAIL ABUN PA-234 1.804E-01 *3. 549E-Ol 3. 641E-01 NOT IDENT. PA-234M -2.468E+OO 4.836E+OO 4. 962E+OO NOT IDENT. U'-235 -8. 013E-02 1. 750E-01 1.787E-01 FAIL ABUN NP-237 -2.429E-02 4. 965E-02 5.084E-02 FAIL ABUN NP-238 1.000E+41 1.229E+41 O.OOOE+OO SHORT HLIF NP-239 -2.527E-01 2.476E-01 2.726E-01 FAIL ABUN PU-239 8. OllE+Ol 3.009E+02 3. 031E+02 NOT IDENT. AM-241 9.052E-02 l.637E-01 l.687E-01 NOT IDENT. CM-243 -2.619E-03 9.952E-02 9.953E-02 FAIL ABUN BK-247 -4 .'551E-02 7.795E-02 8. 061E-02 NOT IDENT. CM-247 1.137E-02 3.284E-02 3.324E-02 FAIL ABUN CF-249 3.025E-02 3.327E-02 3. 596E-02 NOT IDENT. CF-251 7.615E-04 1. 213E-01 1.213E-01 NOT IDENT. Page 4053 of 5809
GEL Laboratories LLC *
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA.COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 52.3810 87.09 92.6644 136.47 71.2733 45.60 55.4770 *87.57 92.7384 140.51 0.0000 46.54 50.8940 88.03 92.8090 143.76 59.7382 49.72 0.0000 88.34 92.8563 144.24 70.8418 51. 35 61.0164 88.47 92.8761 145.44 73.1593 51. 87 58.2263 89. 96 82.1497 152.43 68.1708 52.39 64.9855 1093.63 82.2400 153.25 0.0000 52.97 56.4592 91.11 0.0000 323.87 71. 6689 53.44 58.4355 92.59 82.4988 156.02 0.0000 54.07 59.4776 93.35 82.5983 158.56 0.0000 57.36 0.0000 94.56 82.7570 159.00 57.4209 57.53 69.5998 94.65 82.7686 162.33 77.9745 57.98 66.7643 94.67 82.7710 162.66 0.0000 59.27 53.0413 94.87 82.7972 163.33 46.3834 59.32 53.0470 97.43 72.0443 165.86 66.9314 59.54 53.0716 98.43 .63.8298 176.31 65.3844 60. 96 63.6164 98.44 63.8307 176.'60 0.0000 61.17 66.2421 99.53 80.2692 177.52 67.7632 62.93 65.5051 100 .11 78.2530 181.07 0.0000 63.29 65.5533 102.03 79.5266 181.52 70.7332 63.58 65.5919 103.18 79.6628 184.41 78.6520 64.28 66.6651 103.37 68.1520 143.76 6.6. 0158 66.73 73.5592 105.21 59.9271 193.51 64.1930 67.24 71. 0030 105.31 72.5539 197.03 60.8986 125.81 71.0640 106.12 68.4290 198.01 72.6790 67.75 74.0353 106.47 68.4639 201.83 72.9438 69.67 83.2284 109.28 63.4547 203.43 56.5583 70.83 75.4683 111. 00 72.0918 205.31 64.5280 72.81 76. 7462 111.76 0.0000 210.85 49.0404 72. 87 76.7550 114. 06 69.2083 215.65 50.0506 74.66 77.0088 116. 30 0.0000 222 .11 70.7170 74.82 77.0317 116.74 81.2214 227.09 56.5813 74.97 77.0529 119.76 57.9473 227.38 63.8206 77 .11 77.3525 121. 12 61.2787 228.16 0.0000 77.5775 121.22 54.8357 228.18 63.8651 79.69 77.7079 121. 78 60.2567 116.74 63.8651 80.12 76.7567 122.06 63.5085 235.69 59.8326 80.19 0.0000 122.92 45.2611 235. 96 59.8465 80.57 76.8170 123.07 45.2700 238.63 60.7925 81. 00 66.0850 265.00 48.5427 238.98 0.0000 81. 07 66.0930 125.81 58.4149 240.99 . 60. 9131 81. 75 95.8808 127.23 57.4388 242.00 60.9650 83.79 81. 3104 127.91 60.7435 244.70 61.1015 84.00 81.3391 129.30 64.1117 252.40 0.0000 85.43 97.8435 131.20 72. 9827 252.80 33.2148 86.55 92.5814 133.02 68.7832 254.15 0.0000 86.79 92.6180 133. 52 64.4565 256.23 33.3067 86.94 92.6416 136.00 70 .1357 260.90 0.0000 Page 4054 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 50.9159 355.39 0.0000 584.27 18.9026 264.80 52.1642 356.01 .34. 9602 595.83 0.0000 265.00 52.1719 364.49 0.0000 427.87 19.0379 268.22 46.4912 366.42 0.0000 602.52 0.0000 269.46 44.8748 372. 51 33.8948 604.72 15.0562 270.03 44.8945 375.05 27.6939 607.14 19.5936 271.23 44.9363 377.52 32.2090 609.32 16.0918 273.65 0.0000 356.01 30.5365 610.33 16.0983 276.40 30.0762 388.16 19.8099 614.28 22.6767 277.37 41. 3849 388.63 0.0000 618.01 18.1699 277.60 41.3920 391.69 22.5586 620.36 22.2292 278.00 41. 4051 264.66 29.0273 621. 93 20.2222 279.20 47.7215 401.81 31.7693 630.19 0.0000 279.54 47.7343 402.40 26.3326 631. 29 14. 2108 279.70 42. 7148 404.85 29.0977 633.25 16.2539 280.46 45.2527 410.95 31. 0249 634.78 0.0000 283.69 42.8424 413.71 39.2986 635.95 19.3232 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 44.5797 423.72 0.0000 645.85 10.2112 285.90 0.0000 427.09 18.4163 657.76 16.9297 287.50 41.2790 427.87 23.2148 657.90 0.0000 290.67 35.4648 433.94 19.4106 661.66 22.6087 293.27 0.0000 439.40 27. 8119 664.57 0.0000 351. 93 44.4785 453.88 28.0292 666.33 0.0000 295. 96 44.5020 463.37 27.2306 666.50 0.0000 879.38 45.8602 468.07 27.2972 667. 71 0.0000 299.98 25.5035 473.00 0.0000* 677.62 18.6152 300.09 25.5060 475.06 11.3362 685.70 0.0000 300.13 25.5066 476.78 25.5289 695.00 0.0000 301.36 25.5292 477.60 25.5399 696.49 17.7104 302.85 37.0562 482.18 21.8068 696. 51 17.7104 256.23 39.6582 487.02 0.0000 69*7. 00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.5475 306.78 32.4614 497.08 21. 0153 697.49 14.5907 308.46 37.6317 505.52 26.4747 702.65 26.1058 311. 90 33.4355 507.63 0.0000 706.68 16.7337 316.51 37.8429 511. 00 31.7391 711. 68 18.8606 319 . .41 0.0000 514.00 "18.7819 720.70 0.0000 320.08 0.0000 514.00 18.7819 721. 93 0.0000 321.04 37.2709 520.40 19.3229 722.78 17.3614 323.87 33.7124 520.69 0.0000 722.91 12.6270 325.23 35.4738 *522. 65 0.0000 723.31 12.6289 328.76 0. 00.00 527.90 0.0000 724.19 15.7916 333.37 28.7085 528.26 24.2452 727.33 13.7019 333.97 31.3308 529.59 21. 3492 733.00 11. 0900 334.37 32.6447 529.87 0.0000 735.93 6.3440 338.28 24.4379 531.02 0.0000 333.97 12.6953 338.32 24.4385 537.26 0.0000 739.50 0.0000 311. 90 31. 4656 546.56 0.0000 747.24 12.7407* 340.48 31. 4656 552.55 16.6742 748.06 7. 9654 340 .. 55 0.0000 563.25 17.7407 752.31 13.8278 344.28 28.0391 569.33 13.8365 753.82 0.0000 345.93 35.0863 946.00 13.8376 756.73 8.5231 351.06 36. 9619 569.70 14.8273 756.80 8.5234 351.93 36.9824 583.19 18.8941 884.68 16.0223 Page 4055 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.0333 1274.44 18.4173 1620.50 4.0042 766. 4.2 16.0364 1001.03 18.4427 1621. 92 5.0064 766.84 16.0388 1002.74 16.1453 1678.03 0.0000 772.60 0.0000 1004.73 9. 2311 1690.97 1.0148 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 5.1437 778.90 12.8862 1028.54 0.0000 1063.66 8.2388 783.70 0.0000 1037.84 6.9893 1771. 35 4.1201 785.37 14.2071 1038.76 0.0000 1791.20 0.0000 792.07 19.4187 631. 29 10.5095 1808.65 1.0370 794.95 17.8179 1048.07 0.0000 1810. 72 0.0000 795.86 9. 7222 1049.04 9.6404 1836.06 4.1685 810.06 11. 3981 1050.41 14.9041 810.29 13.0273 1063.66 7.9195 344.28 13.0278 1077.00 0.0000 810.76 6.5146 1077.34 10.5989 815.77 0.0000 1085.87 9.7385 1048.07 0.0000 1093.63 15.6138 832.01 15.3108 1099.45 7.1084 834.85 15.3250 1112. 07 9.8069 835. 71 10.9497 1112.84 11.5924 836.80 0.0000 1115. 54 15.7062 846.75 0.0000 1120.29 12.5089 846.77 13.1880 1120.55 12.5098 856.80 0.0000 1221.41 12.5123 860.56 6.6239 1129. 67 2.6873 871. 09 12.1852 1131. 51 0.0000 873.19 7.7596 1147.95 0.0000 875.33 0.0000 1173.23 17.2118 879.38 7.7750 1177.95 18.1396 880.51 12.2224 1189.05 20.0100 883.24 13. 3452 1204.77 13.6972 884.68 10.0133 1221.41 12.2257 889.28 15.5996 1231.02 11.0295 894.76 13.3940 1235.36 0.0000 898.04 10.0562 1238.28 16.5740 900. 72 10.0646 1260.41 0.0000 903.28 17.9069 1271.87 12.7307 911. 20 8.9756 1274.44 8.3595 912.08 8.9782 1274.54 8.3595 923.98 0.0000 1291.59 11.9375 926.50 18.0365 1298.22 0.0000 929 .11 16.9232 1312 .11 0.0000 937.49 20.3599 1332. 49 4.5196 944 .13 0.0000 1362.66 0.0000 946.00 11. 3403 1365.19 7.5889 949.00 19.2959 1368.63 0.0000 667.71 0.0000 1384.29 6.6689 962. 31 13.6753 1408.01 6.7043 964.08 20.5239 1457.56 0.0000 966 .17 22.2477 1460.82 3.8752 911. 20 23.9788 1489.16 2.9238 968.97 23.9788 1505.03 6.8453 983.53 0.0000 1584.12 5.3005 984.45 0.0000 1596. 21 0.0000 Page 4056 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:05:34.85 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 7-DEC-2015 13:42:00. Acquisition date : 3-0CT-2016 07:01:40. Sample ID G405235050 Sample quantity : 1.71604E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.33 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 2 4 2 5 2 6 0 7 2 8 2 9 0 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 9 19 9 20 . 0 21 0 22 2 23 2 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 4057 of 5809 Energy 46.21* 63.24* 74.87* 77.13* 80.83 87. 28" 89.70 92.70* 186.15* 227.19 238.61* 262.50 270.55 295.36* 303.06 327.54* 338.76 350.03 351. 88* 426.49 511. 05* 583.18* 587.54 601.50 609.43* 635.18 662.20 700.74 727.85 763.74 768.42 794.70 897.43 910.82* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 18 37 100 135 18 79 36 61 63 25 226 28 23 59 39 33 34 10. 158 25 20 61 12 12 98 5 16 8 18 9 15 31 7 60 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 81 126 73 66 69 98 25. 83 71 51 101 99 30 54 99 35 40 6 28 24 27 14 17 27 14 13 14 14 8 14 3 7 8 7 1. 02 1.19 0.87 0.92 1. 05 1. 29 *o.97 1. 08 1. 24 1. 71 1. 06 6.92 1. 43 0.97 7.57 0.88 0.84 1. 76 1. 35 6.53 2.74 1. 72 1. 43 4.23 1. 40 0.51 1.29 0. 96 1.27 4.41 1. 48 0.66 0.68 2.02 92.38 126.44 149. 72 154.22 161. 63 174.52 179.37 185.37 372.29 454.36 477.20 524.99 541.09 590.71 606 .11 655.06 677.51 700.05 703.75 852.94 1022.06 1166.29 1175.00 1202.92 1218.78 1270.27 1324. 30 1401. 36 1455.57 1527.33 1536.69 1589.24 1794.64 1821. 41 90 122 144 144 144 171 178 178 368 451 471 513 538 586 596 650 673 699 699 845 1016 1158 1158 1192 1212 1265 1320 1395 1451 1519 1533 1581 1789 1813 8 4.90E-03 93.3 9 1. 03E-02 57. 9 21 2.79E-02 16.4 21 3.74E-02 12.8 21 4.90E-03 84.7 7 2.19E-02 23.7 14 1. OlE-02 19. 8 14 1.68E-02 28.7 10 1.75E-02 29.5 8 7.05E-03 52.8 10 6.27E-02 10.9 19 7.87E-03 86.6 6 6.30E-03 43.7 10 1.64E-02 26.8 20 1.08E-02 66.2 10 9.lOE-03 38.7 10 9.51E-03 37.8 12 2.73E-03 47.6 12 4.39E-02 9.9 16 6.94E-03 48.2 11 5.45E-03 69.2 22 1. 68E-02 19 .1 22 3.41E-03 62.2 17 3.25E-03110.0 14 2.73E-02 13.4 8 1.45E-03124.1 9 4.55E-03 47.5 10 2.17E-03 98.7 9 4.89E-03 38.6 14 2.50E-03 94.3 7 4.09E-03 33.4 15 8.51E-03 26.5 9 l.86E-03 88.6 14 1.66E-02 16.5 Fit 1. 39E+OO 2.77E+OO 7.59E+OO 9.52E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 955.36 13 0 1. 50 1910.46 1905 10 3. 61E-03 27.7 36 0 965. 48 13 8 1.11 1930.69 1925 10 3.47E-03 49.8 37 0 969. 05 35 2 1. 95 1937.84 1934 9 9.76E-03 18.5 38 0 1019.06 16 0 4.53 2037.81 2031 13 4.44E-03 25.0 39 0 1120.22* 16 10 0.83 2240.05 2235 10 4.58E-03 44.4 40 0 1239.25 8 11 1. 27 2478.00 2471 11 2.22E-03 87.7 41 0 1305. 01 8 5 0. 96 2609.47 2605 9 2.08E-03 62.7 42 0 1461. 06* 205 0 2.09 2921.39 2915 13 5.69E-02 7 .1 43 0 1764.65* 9 5 0. 71 3528.17 3522 11 2.43E-03 66.3 Flag: "*" = Peak area was modified by background subtraction Page 4058 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:05:36 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 13:42:00 G405235050 Acquisition date : Sample quant.ity Sample geometry : 3-0CT-2016 07:01:40 171. 60 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4059 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.33 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Nuclide Type: Uncorrected Decay.Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 6.546E-01 1.255E+Ol 1.255E+Ol 14.12 OK CD-109 88.03 3.70* 4.297E+OO 2.459E+OO 3.863E+OO 59.22 OK SB-125 176.31 6.89 4.460E+OO Line Not Found Absent 321. 04 0.42 2.640E+OO Line Not Found Absent 427.87 29.80* 2.005E+OO 2 .114E-01 2.599E-01 96.33 OK 463.37 10.56 1. 852E+OO Line Not Found Absent 600.60 17.77 1.455E+OO 2.187E-01 2.689E-01 220.01 OK 635.95 11. 29 1.385E+OO l.604E-01 1. 972E-01 248.20 OK SN-126 64.28 9.60 2.468E+OO 9.790E-01 115. 79 OK 86.94 8.90 4.297E+OO l.022E+00 1.022E+OO 59.22 OK 87.57 37.00* 4.297E+OO 2.459E-01 2.459E-01 59.22 OK BA-137M 661.66 89.90* 1.334E+OO 6.517E-02 6.642E-02 94.95 OK CS-137 661.66 85.10* 1.334E+OO 6.884E-02 7.016E-02 94.95 OK TL-208 277.37 6.60 3. 041E+OO Line Not Found Absent 583.19 85.00* l.496E+00 2.315E-01 2.315E-01 38 .11 OK 860.56 12.50 1.058E+OO Line Not Found Absent PB-210 46.54 4.25* 8.252E-01 3.242E+OO 3.326E+OO 186.69 OK BI-211 72. 87 1. 23 3. 327E+OO Line Not Found -----Absent 351. 06 12.92* 2.415E+OO 9.855E-01 9.855E-01 103.12 OK PB-212 74.82 10.28 3.486E+00 l.385E+OO 1.385E+OO 42.80 OK 77 .11 17.10 3.657E+OO 1.319E+OO 1.319E+OO 25.66 OK 238.63 43.60* 3.500E+OO 8.007E-01 8.007E-01 21. 88 OK 300.09 3.30 2.819E+00 Line Not Found Absent BI-214 609.32 45.49* 1.437E+OO 7.244E-01 7.246E-01 26. 85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 OK PB-214 74.82 5.80 3.482E+OO Line Not Found* <<INT Reject 77 .11 9.70 3.657E+OO 2.325E+OO 2.326E+OO 25.66 OK 87.09 3.41 4.287E+OO -----Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found Absent 295.22 18.42 2.863E+OO 5.924E-01 5.926E-01 53.64 OK 351. 93 35.60* 2.414E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* l.437E+OO 7.244E-01 7.246E-01 26.85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.868E-01. 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 OK RA-226 609.32 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 OK AC-228 105.21 1.10 4.933E+00 Line Not Found Absent 338.32 11. 27 2.506E+OO 6.299E-01 6.299E-01 75.66 OK 794.95 4.25 1.134E+OO 2.961E+OO 2. 961E+00 53.09 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 OK 968.97 15.80 9.525E-01 1.059E+OO 1. 059E+OO 36.92 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11.27 2.506E+OO 6.299E-01 6.299E-01 75.66 OK 794.95 4.25 l.134E+OO 2. 961E+OO 2. 961E+OO 53.09* OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* l.006E+OO 1.053E+OO 1.053E+OO 32.94 OK Page 4060 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 968.97 15.80 9.525E-01 1.059E+OO l.059E+OO 36.92 OK TH-228 74.82 10.28 3.486E+00 1.385E+OO l.385E+OO 42.80 OK 77 .11 17.10 3.657E+OO 1.319E+OO 1.319E+OO 25.66 OK 238 .. 63 43.60* 3.500E+00 8.007E-01 8.007E-01 21. 88 OK 300.09 3.30 2.819E+OO Line Not Found Absent TH-230 609.32 45.49* 1.437E+00 7.244E-01 7.244E-01 26. 85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.866E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.384E-01 132.56 OK TH-232 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.506E+00 6.299E-01 6.299E-Ol 75.66 OK 835. 71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 OK 968.97 15.80 9.525E-01 1.059E+OO 1.059E+OO 36.92* OK TH-234 63. 29 3.70* 2.468E+OO 2.540E+OO 2.5LJOE+OO 115. 79 OK 92. 59 4.23 4.552E+OO 1. 892E+OO 1.892E+OO 57.46 OK U-234 609.32 45.49* 1.437E+OO 7.244E-01 7.244E-01 26.85 OK 1120.29 14.92 8.373E-01 5.866E-Ol 5.866E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.384E-01 132.56 OK U-235 89. 96 3.47 4.418E+OO . 1. 428E+OO 1.428E+00 39.64 OK 93.35 5.60 4.552E+OO. 1.429E+OO l.429E+OO 57.46 OK 143.76 10. 96* 4 .,954E+OO Line Not Found Absent 163.33 5.08 4.674E+OO Line Not Found Absent 185. 72 57.20 4. 296E+OO 1.429E-01 l.429E-01 59.00 OK 205.31 5.01 3.984E+OO Line Not Found Absent U-238 63.29 3.70* 2.468E+OO 2.540E+OO 2.540E+OO 115. 79 OK 92.59 4.23 4.552E+OO 1.892E+OO 1.892E+OO 57.46 OK AM-243 43.53 5.90 5.957E-01 Line Not Found Absent 74.66 67.20* 3.486E+OO 2 .119E-01 2.120E-01 42.80 OK ANH-511 511. 00 100.00* 1.690E+OO 5.738E-02 5.738E-02 138.38 OK Flag: "*" = Keyline Page 4061of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:37.83 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 ** ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l *
Acquisition date 3-0CT-2016 07:01:40 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
Sample date 7-DEC-2015 13:42:00 Analyst initials: MXRl * *Sample ID G405235050 Sample Quantity 1.7160E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr. 1.00000 Dry Weight 0.00000 *
Nuclide Library : * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File. : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.255E+Ol 1. 737E+OO CD-109 3.863E+OO 2.242E+OO SB-125 2.599E-01 2.454E-01 SN-126 2.459E-01 l.427E-01 BA-137M 6.642E-02 6.180E-02 CS-137 7.016E-02 6.529E-02 TL-208 2.315E-01 8.647E-02 PB-210 3.326E+OO 6.086E+OO BI-211 9.855E-01 9.959E-01 PB-212 8.007E-01 1. 717E-01 BI-214 7.246E-01 1.907E-01 PB-214 9.503E-01 1.835E-01 RN-222 7.246E-01 l.907E-01 RA-226 7.246E-01 1.907E-01 AC-228 l.053E+00 3.398E-01 RA-228 1.053E+OO 3. 398E....:01 TH-228 8.007E-01 l.717E-01 TH-230 7.244E-01 1.906E-01 TH-232 1.053E+OO 3.398E-01 TH-234 2.540E+OO 2.882E+OO U-234 7.244E-01 1.906E-01 U-235 7.049E-02 1.766E-01 U-238 2.540E+OO 2.882E+OO AM-243 2.120E-01 8.891E-02 ANH-511 5.738E-02 7.78.lE-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 4062 of 5809 Key-Line Activity (pCi/GRAM 5.186E-01 8.759E-04 O.OOOE+OO -2.649E-02 -1.420E-01 K.L. Cnt Uncert ( 1. 96-sigma) l.085E+Ol 5.428E-02 1.960E+41 3.778E-02 3.637E-01 MDA (pCi/GRAM 8.223E-01 l.569E+OO 2.009E-01 l.124E-01 8.421E-02 8.896E-02 6.129E-02 4.500E+00 3.467E-01 l.140E-01 1.197E-01 3.357E-01 l.197E-01 1.197E-01 2.708E-01 2.708E-01 1.140E-01 l.l97E-01 2.708E-01 1.919E+OO 1.197E-01 3.540E-01 l.919E+OO 7.184E-02 6.892E-02 MDA (pCi/GRAM 2.321E+Ol 1.152E-01 O.OOOE+OO 6.149E-02 6.838E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO l.680E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.971E+02 O.OOOE+OO SHORT HLIF MN-54 -2.864E-02 7.340E-02 1. 361E-01 NOT IDENT. C0-56 -5.145E-02 5.192E-01 l.033E+OO FAIL ABUN MN-56 .O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -6.166E-03 3. 951E-02 7.917E-02 NOT IDENT. C0-58 1. 804E-01 4.878E-01 l.136E+OO NOT IDENT. FE-59 6.390E-01 7.582E+OO l.642E+Ol NOT IDENT. C0-60 -l.833E-02 3.382E-02 6.445E-02 NOT IDENT. ZN-65 4.087E-02 l.851E-01 3.782E-Ol NOT IDENT. GE-68 -3.244E-01 2.487E+OO. 4.885E+OO NOT IDENT. AS-73 -4.126E+OO 6.353E+OO l.300E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.176E+03 O.OOOE+OO SHORT HLIF SE-75 -6.605E-03 2.268E-01 4.012E-01 NOT IDENT. BR-77 O.OOOE+OO 4.008E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.294E+02 O.OOOE+OO SHORT HLIF RB-83 l.325E-01 5.587E-01 l.250E+OO NOT IDENT. KR-85 3.824E+OO 7.365E+OO l.505E+Ol NOT IDENT. SR-85 4.066E-01 7.853E-01 l.605E+OO NOT IDENT. RB-86 O.OOOE+OO 3.046E+04 O.OOOE+OO SHORT HLIF Y-88 -6. 631E-02 2.108E-01 4.436E-01 FAIL ABUN Y-91 1. 459E+02 6.492E+02 1. 399E+03 NOT IDENT. NB-94 5.731E-03 3.353E-02 6.457E-02 NOT IDENT. NB-95 5.050E-01 l.053E+OO l.852E+OO NOT IDENT. NB-95M -l.150E-01 2. 496E+OO 4.409E+OO NOT IDENT. ZR-95 3.079E-01 l.687E+00 3.393E+00 NOT IDENT. NB-97 O.OOOE+OO l.816E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.077E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.673E-02 2.826E-02 5.204E-02 NOT IDENT. RH-102 * -2.757E-02 6.786E-02 l .131E-01 NOT IDENT. RU-103 3.330E+OO 4.878E+OO l.155E+Ol FAIL ABUN RH-106 -1. 784E-02 5.749E-01 1.172.E+OO NOT IDENT. RU-106 -1. 784E-02 5.749E-01 l. l 72E+00 NOT IDENT. AG-108M -l.800E-02 2.331E-02 4.351E-02 NOT IDENT. AG-llOM 5.908E-03 l.134E-01 2.321E-01 FAIL ABUN SN-113 -l.267E-01 2.203E-01 4.284E-01 NOT IDENT. CD-115 O.OOOE+OO 4. ll 7E+39 0.000E+OO SHORT HLIF SN-ll 7M 0.000E+OO 8.980E+04 O.OOOE+OO SHORT HLIF TE-123M -8.092E-02 l .130E-01 2.087E-01 NOT IDENT. SB-124 -l.059E+OO l.467E+OO l.416E+OO NOT IDENT. TE-125M 2.075E+02 2.485E+02 5.384E+02 NOT IDENT. I-126 O.OOOE+OO l.167E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.261E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.050E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 5.900E+09 0.000E+OO SHORT HLIF I-:-132
O.OOOE+OO 1. 911E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.708E+26 O.OOOE+OO SHORT HLIF BA-133 -l.023E-02 4.627E-02 7.735E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 1. 009E-01 l.519E-01 FAIL ABUN CS-135 -3. 451E-02 l.415E-01 2.420E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.636E+05 O.OOOE+OO SHORT HLIF CE-139 -5.049E-02 8.923E-02 l.673E-01 NOT IDENT. BA-140 O.OOOE+OO l.290E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 4.995E+05 O.OOOE+OO SHORT HLIF CE-141 -l.165E+Ol 2.362E+Ol 4.384E+Ol NOT IDENT. CE-143 O.OOOE+OO l.669E+41 O.OOOE+OO SHORT HLIF CE-144 -l.069E-01 3.257E-01 6.342E-01 FAIL ABUN PM-144 -9.170E-04 5.191E-02 9.768E-02 NOT IDENT. PR-144 -5.838E-02 4.516E+OO 8.508E+OO NOT IDENT. PM-146 -2.352E-02 4.604E-02 8.884E-02 NOT IDENT. ND-147 O.OOOE+OO 3.648E+07 O.OOOE+OO SHORT HLIF PM-147 4: 273E+02, 6.682E+02 l.441E+03 NOT IDENT. PM-149 0.000E+OO 6.313E+40 O.OOOE+OO SHORT HLIF EU-150 l.233E-02 2.643E-02 5.344E-02 FAIL ABUN EU-152 -1. 903E-02 9.506E-02 1. 756E-01 . FAIL ABUN GD-153 -2.205E-01 l.651E-01 2.727E-01 NOT IDENT. EU-154 -l.454E-03 l.321E-01 2.790E-01 NOT IDENT. EU-155 l.191E-01 9.630E-02 2.150E-01 FAIL ABUN TB-160 -l .134E+OO 2.083E+OO 3.713E+OO FAIL ABUN H0-166M 1.215E-02 6.496E-02 l.352E-01 FAIL ABUN TM-171 3.224E+OO 1.481E+Ol 3.277E+Ol NOT IDENT. HF-172 3.257E-02 l.921E-01 3.950E-01 FAIL ABUN LU-172 -1.693E-03 7.624E-02 l.555E-01 FAIL ABUN LU-176 -1. 761E-03 2.815E-02 4.885E-02 FAIL ABUN Page 4063 of 5809 HF-181 -8. 911E-01 4.476E+OO 9.045E+OO NOT IDENT. TA-182 2.495E-01 8.907E-01 2.025E+OO FAIL ABUN RE-183 1.068E+OO 2.222E+OO 4. 968E+OO NOT IDENT. RE-184 2.926E+Ol 2.914E+Ol 7.270Et01 NOT IDENT. W-188 1. 966E+Ol 1.146E+02 2. 096E+02 FAIL ABUN IR-192 -l.459E-01 3.695E-01 6.746E-01 FAIL ABUN HG-203 -4.548E-01 2.344E+OO 4.397E+OO NOT IDENT. BI-207 -4.601E-03 6. 561E-02 l.258E-01 FAIL ABUN, PB-211 8.667E-02 6.513E-01 l.387E+OO FAIL ABUN BI-212 1.016E+OO 7.686E-01 1.418E+OO FAIL ABUN RN-219 -l.212E-01 3.718E-01 7. 451E-01 FAIL ABUN RA-223 6.744E-02 6 .119E-01 1.103E+OO FAIL ABUN RA-224 5.292E-01 7.537E-01 l.408E+OO NOT IDENT. AC-227 -l.323E-01 2.415E-01 3.925E-01 FAIL ABUN TH-227 -1.323E-01 2.415E-01 *3.925E-01 FAIL ABUN TH-229 -8. 710E-03 4.030E-01 7.918E-01 FAIL ABUN PA-231 2.909E-01 5.052E-01 9.602E-01 NOT IDENT. TH-231 6.744E-02 6 .119E-01 1.103E+OO FAIL ABUN PA-233 -4.939E-02 5.971E-02 9.985E-02 NOT IDENT. PA-234 4.934E-02 3.090E-01 6.449E-01 NOT IDENT. PA-234M 1.565E+OO 4.278E+OO 9.702E+OO NOT IDENT. NP-237 -4.939E-02 5. 971E-02 9.985E-02 NOT IDENT. NP-238 O.OOOE+OO l.454E+41 O.OOOE+OO SHORT HLIF NP-239 -9.777E-02 2.083E-01 4.058E-01 FAIL ABUN PU-239 2.082E+02 2.717E+02 5.808E+02 NOT IDENT. AM-241 -4.695E-02 l.066E-01 2.036E-01 NOT IDENT. CM-243 -3.837E-02 8.216E-02 1.618E-01 FAIL ABUN BK-247 9. 963E-04 7.866E-02 l.399E-01 NOT IDENT. CM-247 -1.347E-02 3.376E-02 6.705E-02 NOT IDENT. CF-249 1.280E-02 3.812E-02 8.234E-02 NOT IDENT. CF-251 2.427E-02 1. 020E-01 2.063E-01 FAIL ABUN Page 4064 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:05:35.56 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 200 10.66* 6.546E-01 l.255E+Ol l.255E+Ol 14.12 CD-109 88.03 109 3.70* 4.297E+OO 3.005E+OO 4.721E+OO 47.47 SB-125 176.31 ------6.89 4.460E+OO ------Line Not Found ------321.04 ------0.42 2.640E+OO ------Line Not Found ------427.87 29 29.80* 2.005E+OO 2 .114E-01 2.599E-01 96. 33 463.37 ------10.56 1.852E+OO ------Line Not Found ------600.60 13 17.77 1.455E-too 2.187E-01 . 2.689E-01 220.01 635.95 6 11. 29 1.385E+OO 1.604E-01 1. 972E-01 248.20 SN-126 64.28 53 9.60 2.468E+OO 9.790E-01 9.790E-01 115.79 86. 94 109 8.90 4.297E+OO 1.249E+OO 1.249E+OO 47.47 87.57 109 37.00* 4.297E+OO 3.005E-01 3.005E-01 47.47 BA-137M 661. 66 18 89.90* 1.334E+OO 6.517E-02 6.642E-02 94.95 CS-137 661. 66 18 85.10* 1.334E+OO 6.884E-02 7.016E-02 94.95 TL-208 277.37 ------6.60 3.041E+OO ------Line Not Found ------583.19 67 85.00* 1. 496E+00 2.315E-01 2.315E-01 38 .11 860.56 ------12.50 1.058E+OO ------Line Not Found ------PB-210 46.54 26 4.25* 8.252E-01 3.242E+OO 3.326E+OO 186.69 BI-211 72. 87 ------1.23 3.327E+OO ------Line Not Found ------351.06 187 12.92* 2.415E+OO 2.618E+OO 2.618E+OO 19.71 PB-212 74.82 141 10.28 3.486E+OO 1. 720E+OO 1. 720E+OO 32.87 77 .11 189 17.10 3.657E+OO 1.319E+OO 1.319E+OO 25.66 238.63 279 43.60* 3.500E+OO 8.007E-01 8.007E-01 21. 88 300.09 ------3.30 2.819E+OO ------Line Not Found ------BI-214 609.32 108 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 1120.29 17 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 PB-214 74.82 141 5.80 3.486E+OO 3.048E+OO 3.049E+OO 32.87 77 .11 189 9.70 3.657E+OO 2.325E+OO 2.326E+OO 25.66 87.09 109 3.41 4.297E+OO 3.260E+OO 3.262E+OO 47.47 242.00 ------7.25 3.455E+OO ------Line Not Found ------295.22 71 18. 42. 2.863E+OO 5.924E-01 5.926E-01 53.64 351. 93 187 35.60* 2.415E+OO 9.500E-01 9.503E-01 19.71 RN-222 609.32 108 45.49* 1.437E+OO 7.244E-01 7.246.E-01 26.85 1120.29 17 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 RA-226 609.32 . 108 45.49* l.437E+OO 7.244E-01 7.246E-01 26.85 1120.29 17 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 41 11. 27 2.506E+OO 6.299E-01 6.299E-01 75.66 794.95 33 4.25 1.134E+OO 2. 961E+OO 2. 961E+OO 53.09 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 62 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 968. 97 36 15.80 9.525E-01 1.059E+OO 1.059E+OO 36.92 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 41 11. 27 2.506E+OO 6.299E-01 6.299E.:.01 75.66 794.95 33 4.25 1.134E+OO 2. 961E+OO 2. 961E+OO 53.09 Page 4065 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235050 Acquisition date Page : .2 3-0CT-2016 07:01:40 Nuclide Type: Nuclide TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Energy 835.71 911.20 968. 97 74.82 77 .11 238.63 300.09 609.32 1120.29 1764.49 105.21 338.32 835.71 911.20 968. 97 63.29 92.59 609.32 1120. 29 1764.49 89. 96 93.35 143.76 163.33 185.72 205.31 63.29 92.59 43.53 74.66 511. 00 Flag: "*" = Keyline Page 4066 of 5809 Area 62 36 141 18'9 279 108 17 8 41 62 36 53 83 108 17 8 50 83 80 53 83 141 22 %Abn 1. 61 25.80* 15.80 10.28 17.10 43.60* 3.30 45.49* 14.92 15.30 1.10 11. 27 1. 61 25.80* 15.80 3.70* 4.23 45.49* 14.92 15.30 3.47 5.60 10. 96* 5.08 57.20 5.01 3.70* 4.23 5.90 67.20* 100.00* %Eff l.085E+OO 1.006E+OO 9.525E-01 '3.486E+OO 3.657E+OO 3.500E+OO 2.819E+OO 1.437E+OO 8.373E-01 5.418E-01 4.933E+OO 2.506E+OO 1.085E+OO 1.006E+OO 9.525E-01 2.468E+OO 4.552E+OO 1.437E+OO 8.373E-01 5.418E-01 4.418E+OO 4.552E+OO 4.954E+00 4.674E+OO 4.296E+OO 3.984E+OO 2.468E+OO 4.552E+OO 5.957E-01 3.486E+OO 1.690E+OO Uncorrected Decay Corr pCi/GRAM pCi7GRAM ------Line Not Found l.053E+OO 1.053E+OO 1.059E+OO 1.059E+OO l.720E+OO 1.720E+OO 1.319E+OO l.319E+OO 8.007E-01 8.007E-01 ------Line Not Found 7.244E-01 7.244E-01 5.866E-01 5.866E-01 4.384E-01 4.384E-01 ------Line Not Found 6.299E-01 6.299E-01 ------Line Not Found 1.053E+OO 1.053E+00 1.059E+OO 1.059E+00 2.540E+OO 2.540E+OO 1.892E+OO 1.892E+OO 7.244E-01 7.244E-01 5:866E-01 5.866E-01 4.384E-01 4.384E-01 1.428E+OO 1.428E+OO 1.429E+OO 1.429E+OO ------Line Not Found ------Line Not Found l.429E-01 l.429E-01 ------Line Not Found 2.540E+OO 2.540E+OO 1.892E+OO 1.892E+00 ------Line Not Found 2.631E-01 2.631E-01 5.738E-02 5.738E-02 2-Sigma %Error 32.94 36.92 3:2.87 25.66 21. 88 26.85 88.76 132.56 75.66 32.94 36.92 115. 79 57.46 26.85 88.76 132.56 39.64 57.46 59.00 115. 79 57.46 32.87 138.38 Page : 3 Summary of Nuclide Activity Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Total number of lines in spectrum 43 Number of unidentified lines 7 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 CD-109 SB-125 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461. 40D 2. 76Y 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y l.41E+10Y 1600. OOY 1600. OOY 1600. DOY 1600. DOY 1. 41E+l0Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 57 1. 23 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.255E+Ol 3.005E+OO 2 .114E-01 3.005E-01 6.517E-02 6.884E-02 2.315E-01 3.242E+OO 2.618E+OO 8.007E-01 7.244E-01 9.500E-01 7.244E-01 7.244E-01 1.053E+OO 1.053E+00 8.007E-01 7.244E-01. 1.053E+OO 2.540E+OO 7.244E-01 1.429E-01 2.540E+OO 2.631E-01 5.738E-02 3. 717E+Ol 3.717E+Ol Decay Corr pCi/GRAM 1.255E+Ol 4.721E+OO 2.599E-01 3.005E-01 6.642E-02 7.016E-02 2.315E-01 3.326E+OO 2.618E+OO 8.007E-01 7.246E-01 9.503E-01 7.246E-01 7.246E-01 1.053E+OO 1.053E+OO 8.007E-01 7.244E-01 1.053E+OO 2.540E+OO 7.244E-01 1.429E-01 2.540E+OO 2.631E-01 5.738E-02 3.902E+Ol 3.902E+Ol 83. 72% Decay Corr 2-Sigma Error 0.177E+Ol 2.241E+OO 2.504E-01 l.427E-01 6.306E-02 6.662E-02 0.882E-01 6 .. 210E+OO 0.516E+OO 1. 752E-01 l.945E-01 l.873E-01 l.945E-01 1.945E-01 0.347E+.00 0.347E+OO 1. 752E-01 l.945E-01 0.347E+OO 2. 941E+OO l.945E-01 0.843E-01 2. 941E+OO 0.865E-01 7.940E-02 "M" Manually accepted 2-Sigma %Error 14.12 47.47 96.33 47.47 94.95 94.95 38 .11 186:69 19. 71 21. 88 26. 85 19. 71 26. 85 26. 85 32.94 32.94 21. 88 26. 85 32.94 115.79 26.85 59.00 115. 79 32.87 138.38 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4067 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235050 Acquisition date : 3-0CT-2016 07:01:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 80.83 25 96 1. 05 161. 63 144 21 .4. 90E-03 **** 3.91E+00 T 0 227.19 32 63 1. 71 454.36 451 8 7.05E-03 **** *3.66E+OO T 0 262.50 35 121 6.92 524.99 513 19 7.87E-03 **** 3.20E+OO 0 270.55 28 37 1. 43 541.09 538 6 6.30E-03 87.3 3.llE+OO T 0 303.06 47 119 7.57 606.11 596 20 1. 08E-02 **** 2.79E+OO T 0 327.54 39 42 0.88 655.06 650 10 9.lOE-03 77.3 2.59E+OO T 9 350.03 12 8 1. 76 700.05 699 12 2.73E-03 95.1 2.43E+OO 2 587.54 14 19 1. 43 1175.00 1158 22 3.41E-03 **** l.49E+OO 0 700.74 8 15 0. 96 1401.36 1395 10 2.17E-03 **** 1. 27E+OO 0 727. 85 19 9 1. 27 1455.57 1451 9 4.89E-03 77.2 1. 23E+OO T 0 763.74 10 15 4.41 1527.33 1519 14 2.50E-03 **** 1.17E+00 T 0 768.42 16 4 1. 48 1536.69 1533 7 4.09E-03 66.7 l.17E+OO 0 897.43 7 9 0.68 1794.64 1789 9 1. 8 6E-03 **** 1.02E+OO T 0 955.36 14 0 1. 50 1910.46 1905 10 3.61E-03 55.5 9.65E-01 T 0 965. 48 13 8 1.11 1930.69 1925 10 3.47E-03 99.6 9.56E-01 T 0 1019.06 16 0 4.53 2037.81 2031 13 4.44E-03 50.0 9. llE-01 0 1239.25 8 11 1. 27 2478.00 2471 11 2.22E-03 **** 7.64E-01 T 0 1305.01 7 4 0. 96 2609.47 2605 9 2.08E-03 **** 7.28E-01 Flags: "T" = Tentatively associated Page 4068 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:49:60 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * * *configuration DKAlOO: [CANBERRA. GAMMA.ARCHIVE. GAMMA] G405235050. CNF; 1 *
Acquisition date 3-0CT-2016 07:01:40 Sensitivity 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
Sample date 7-DEC-2015 13:42:00 Nuclide Library : SOLID *
Sample ID G405235050 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : l.7160E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. Fiie : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Ide.ntified Nuclides ----Nuclide K-40 CD-109 SB-125 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235
U-238 AM-243 ANH-511 Le (pCi/GRAM 3.252E-01 7.204E-01 8.759E-02 5.210E-02 3.688E-02 3. 896E-02 2.578E-02 2.062E+OO 1.533E-01 5.285E-02 5.042E-02 1.606E-01 5.042E-02 5.042E-02 1.119E-01 l .119E-01 5.285E-02 5.041E-02 1.119E-01 8.876E-01 5. 041E-02 1. 651E-01 8.876E-01 3. 311E-02 3.079E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4069 of 5809 Le (pCi/GRAM 9.944E+00 4.750E-02 O.OOOE+OO 1.943E-02 2.704E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN. SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 'SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 . GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4070 of 5809 O.OOOE+OO 5.707E-02 4.319E-01 O.OOOE+OO 3.639E-02 4.634E-01 6.849E+OO 2.283E-02 1.557E-01 1. 974E+OO 5.925E+OO O.OOOE+OO 1. 813E-01 O.OOOE+OO O.OOOE+OO 5.320E-01 6.629E+OO 7.066E-01 O.OOOE+OO l.402E-01 5.951E+02 2.742E-02 7.901E-01 2.017E+OO l.450E+OO O.OOOE+OO O.OOOE+OO o:ooOE+OO O.OOOE+OO 2.380E-02 4.735E-02 4.978E+OO 5.088E-01 5.088E-01 l.825E-02 9.733E-02 l.871E-01 O.OOOE+OO O.OOOE+OO 9.507E-02 O.OOOE+OO 2. 511E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.421E-02 O.OOOE+OO 6.764E-02 1.084E-01 O.OOOE+OO O.OOOE+OO 7.575E-02 O.OOOE+OO O.OOOE+OO 2.028E+Ol O.OOOE+OO 2.932E-01 4.023E-02 3.506E+OO 3.880E-02 O.OOOE+OO 6.649E+02 O.OOOE+OO 2.411E-02 7.780E-02 l.251E-01 l.148E-01 l.005E-01 l.508E+OO 5.851E-02 l.504E+Ol l.823E-01 6.250E-02 2.199E-02 3.931E+OO SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 RA-224 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4071of5809 8.341E-01 2.291E+OO 3.066E+Ol 9.408E+Ol 2.894E-01 1. 974E+OO 5.349E-02 6.151E-01 6.340E-01 3.280E-01 4.915E-01 6. 596E-01 1. 759E-01 1. 759E-01 3.612E-01 4.382E-01 4.915E-01 4.390E-02 2.703E-01 4.070E+OO 4.390E-02 O.OOOE+OO 1.868E-01 2.703E+02 9.303E-02 7.444E-02 6.333E-02 2.943E-02 3.684E-02 9.480E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:54.96 *******************************************************************************

GEL Laboratories LLC'
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l *
Acquisition date 3-0CT-2016 07:-01:40 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
Sample date 7-DEC-2015 13:42:00 Nuclide Library : SOLID *
Sample ID G405235050 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : 1.7160E+02 GRAM *
Quantity Err ( % ) : 1.1655E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-JUN,-2016 09: 39: 12 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7 * ******************************************************************************* Combined Ac ti vi ty-MDA Repo,rt NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.255E+Ol 1.856E+OO 1.856E+OO CD-109 3.863E+OO 2.267E+00 2.267E+00 SB-125 2.599E-01 2.456E-01 2. 456E-01. SN-126 2.459E-01 1.437E-01 1.437E-01 BA-137M 6.642E-02 6.187E-02 6.187E-02 CS-137 7.016E-02 6.536E-02 6.536E-02 TL-208 2.315E-01 8.703E-02 8.703E-02 PB-210 3.326E+OO 6.093E+OO 6.093E+OO BI-211 9.855E-01 1.002E+OO 1.002E+OO PB-212 8.007E-01 l.768E-01 1.768E-01 BI-214 7.246E-01 1.932E-01 1.932E-01 PB-214 9.503E-01 l.877E-01 l.877E-01 RN-222 7.246E-01 1.932E-01 1.932E-01 RA-226 7.246E-01 1.932E-01 1.932E-01 AC-228 1.053E+OO 3. 441E-01 3.441E-01 RA-228 1.053E+OO 3.441E-01 3.441E-01 TH-228 8.007E-01 1.768E-01 1. 768E-01 TH-230 7.244E-01 l.931E-01 1.931E-01 TH-232 1.053E+OO 3.441E-01 3.441E-01 TH-234 2.540E+OO 2.937E+OO 2.937E+OO U-234 7.244E-01 l.931E-01 1: 931E-01 U-235 7.049E-02 1. 766E-01 1. 766E-01 U-238 2.540E+OO 2.937E+OO 2.937E+OO AM-243 2.120E-01 9.009E-02 9.009E-02* ANH-511 5.738E-02 7.785E-02 7.785E-02 Non-Identified Nuclides Key-Line Activity* K.L Act error TPU Nuclide (pCi/GRAM ) (1.96-sigma) ( 1. 96-sigma) BE-7 5.186E-01 1.085E+Ol 1.085E+Ol NOT IDENT. NA-22 8.759E-04 5.428E-02 5.428E-02 NOT IDENT. NA-24 l.000E+41 6.064E+41 O.OOOE+OO SHORT HLIF AL-26 -2.649E-02 3.782E-02 3. 966E-02 NOT IDENT. SC-46 -l.420E-01 3.637E-01 3.693E-01 FAIL ABUN Page 4072 of 5809 V-48 2.724E+03 1.680E+04 1.685E+04 SHORT HLIF CR-51 2.742E+02 3.973E+02 4 .161E+02 SHORT HLIF MN-54 -2.864E-02 7. 341E-02 7.454E-02 NOT I DENT .. C0-56 -5.145E-02 5.192E-01 5.198E-01 FAIL ABUN MN-56 -1.000E+41 l.060E+42 0.000E+OO SHORT HLIF C0-57 -6.166E-03 3. 951E-02 3. 961E-02 NOT IDENT. C0-58 l.804E-01 4.879E-01 4.946E-01 NOT IDENT. FE-59 6.390E-01 7.582E+OO 7.588E+OO NOT IDENT. C0-60 -l.833E-02 3.383E-02 3.482E-02 NOT IDENT. ZN-65 4.087E-02 l.851E-01 1. 860E-01 NOT IDENT. GE-68 -3.244E-01 2.487E+OO 2. 491E+OO NOT IDENT. AS-73 -4.126E+OO 6.409E+OO 6.673E+OO NOT IDENT. AS-74 -5.756E+02 7.176E+03 7 .181E+o3 SHORT HLIF SE-75 -6.605E-03 2.268E-01 2.268E-01 NOT IDENT. BR-77 1.869E+38 1.623E+39 0.000E+OO SHORT HLIF SR-82 -6.093E+Ol 8.295E+02 8.299E+02 SHORT HLIF RB-83 l.325E-01 5.590E-01 5.622E-01 NOT IDENT. KR-85 3.824E+OO 7.366E+OO 7.565E+OO NOT IDENT. SR-85 4.066E-01 7.855E-01 8.066E-01 NOT IDENT. RB-86 -5. 591E+03 3.046E+04 3.057E+04 SHORT HLIF Y-88 -6.631E-02 2.108E-01 2.129E-01 FAIL ABUN Y-91 1. 459E+02 6.492E+02 6.525E+02 NOT IDENT. NB-94 5.731E-03 3.353E-02 3.363E-02 NOT IDENT. NB-95 5.050E-01 1.053E+OO 1.078E+OO NOT IDENT. NB-95M -1. 150E-01 2. 496E+OO 2. 496E+OO NOT IDENT. ZR-95 3.079E-01 1.687E+OO l.693E+OO NOT IDENT. NB-97 l.000E+41 1.816E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 3.256E+42 O.OOOE+OO SHORT HLIF M0-99 2.561E+32 2.085E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.569E+41 O.OOOE+OO SHORT HLIF RH-101 -2.673E-02 2.867E-02 3.llOE-02 NOT IDENT. RH-102 -2.757E-02 6.789E-02 6.902E-02 NOT IDENT. RU-103 3.330E+OO 4.881E+OO 5.107E+OO FAIL ABUN RH-106 -1.784E-02 5.749E-01 5.750E-01 NOT IDENT. RU-106 -1. 784E-02 5.749E-01 5.750E-01 NOT IDENT. AG-108M -1.800E-02 2.332E-02 2.469E-02 NOT IDENT. AG-llOM 5.908E-03 1.134E-01 l .134E-01 FAIL ABUN SN-113 -1.267E-01 2.204E-01 2.277E-01 NOT 'IDENT. CD-115 -9.636E+38 4.121E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -3.114E+04 8.987E+04 9. 096E+04 SHORT HLIF TE-123M -8.092E-02 1.130E-01
l.188E-01 NOT IDENT. SB-124 -1.059E+OO 1.468E+OO 1.544E+OO -NOT IDENT. TE-125M 2.075E+02 2.488E+02 2.658E+02 NOT IDENT. I-126 l.293E+06 1.180E+o6 1.316E+06 SHORT HLIF SB-126 -5.115E+05 1. 2 64E+06 l.285E+06 SHORT HLIF SB-127 -2.163E+22 4.266E+22 O.OOOE+OO SHORT HLIF I-131 1. 759E+09 5.900E+09 5.953E+09 SHORT HLIF I-132 -1. 000E+41 1.863E+42 0.000E+OO SHORT HLIF TE-132 8.409E+26 9.358E+26 O.OOOE+OO SHORT HLIF BA-133 -1.023E-02 4.627E-02 4.650E-02 FAIL ABUN I-133 l.OOOE+41 2.748E+41 O.OOOE+OO .SHORT HLIF CS-134 1.940E-01 1.013E-01 1.338E-01 FAIL ABUN CS-135 -3. 451E-02 l.415E-01 1.424E-01 NOT IDENT. I-135 -l.000E+41 7*. 670E+41 O.OOOE+OO SHORT HLIF CS-136 -1.827E+05 3.641E+05 3.733E+05 SHORT HLIF CE-139 -5.049E-02 8.980E-02 9.264E-02 NOT IDENT. BA-140 -6.535E+05 l.290E+06 1.324E+06 SHORT HLIF LA-140 -2.890E+05 4.997E+05 5.164E+05 SHORT HLIF CE-141 -1.165E+Ol 2.362E+Ol 2.420E+Ol NOT IDENT. CE-143 1.000E+41 1. 673E+41 O.OOOE+OO SHORT HLIF CE-144 -l.069E-01 3.258E-01 3.293E-01 FAIL ABUN PM-144 -9.170E-04 5.191E-02 5.191E-02 NOT IDENT. PR-144 -5.838E-02 4.516E+OO 4.516E+OO NOT IDENT. PM-146 -2.352E-02 4.607E-02 4.727E-02 NOT IDENT. ND-147 1.322E+07 3.649E+07 3.697E+07 SHORT HLIF PM-147 4.273E+02 6.685E+02 6;957E+02 NOT IDENT. PM-149 -2.438E+40 6.335E+40 O.OOOE+OO SHORT HLIF EU-150 l.233E-02 2.643E-02 2.701E-02 FAIL ABUN EU-152* -1.903E-02 9.507E-02 9.545E-02 FAIL ABUN GD-153 -2.205E-Ol 1.656E-01 1. 931E-01 NOT IDENT. EU-154 -l.454E-03 l.321E-01 1.321E-01 NOT IDENT. EU-155 1.191E-Ol 9.667E-02 *l .106E-01 FAIL ABUN TB-160 -l.134E+OO 2.084E+OO 2.146E+OO FAIL ABUN H0-166M l.215E-02 6.496E-02 6.519E-02 FAIL ABUN TM-171 3.224E+OO l.481E+Ol l.488E+Ol NOT IDENT. HF-172 3.257E-02 1.922E-01 1.928E-01 FAIL ABUN LU-172 -1.693E-03 7.624E-02 7.624E-02 FAIL ABUN LU-176 -1. 761E-03 2.815E-02 2.816E-02 FAIL ABUN Page 4073 of 5809 HF-181 -8. 911E-01 4.477E+OO 4.495E+00 NOT IDENT. TA-182 2.495E-01 8.908E-01 8.979E-01 FAIL ABUN RE-183 l.068E+OO 2.228E+OO 2.279E+OO NOT IDENT. RE-184 2.926E+Ol 2.997E+Ol 3.275E+Ol NOT IDENT. W-188 1. 966E+Ol 1.14 6E+02 l.150E+02 FAIL ABUN IR-192 -l.459E-01 3.696E-01 3.754E-01 FAIL ABUN HG-203 -4.548E-01 2.344E+OO 2.353E+OO NOT IDENT. BI-207 -4.601E-03 6.561E-02 6.565E-02 FAIL ABUN PB-211 8.667E-02 6.513E-01 6.525E-01 FAIL ABUN BI-212 1.016E+OO 7.703E-01 8. 961E-01 FAIL ABUN RN-219 -1.212E-01 3. 721E-01 3.761E-01 FAIL ABUN RA-223 6.744E-02 6 .119E-01 6.126E-01 FAIL ABUN RA-224 5.292E-01 7.542E-01 7. 910E-.01 NOT IDENT. AC-227 -l.323E-01 2. 421E-01 2.493E-01 FAIL ABUN TH-227 -1.323E-01 2.421E-01 2.493E-01 FAIL ABUN TH-229 -8. 710E-03 4.030E-01 4.030E-01 FAIL ABUN PA-231 2.909E-01 5.090E-01 5.257E-01 NOT IDENT. TH-231 6.744E-02 6 .119E-01 6.126E-01 FAIL ABUN PA-233 -4.939E-02 5.976E-02 6.377E-02 NOT IDENT. PA-234 4.934E-02 3.141E-01 3.149E-01 NOT IDENT. PA-234M 1. 565E+OO 4.279E+OO 4.336E+OO NOT IDENT. NP-237 -4.939E-02 5.976E-02 6.377E-02 NOT IDENT. NP-238 1.000E+41 l.455E+41 0.000E+OO SHORT HLIF NP-239 -9.777E-02 2.085E-01 2 .131E-01 FAIL ABUN PU-239 2.082E+02 2.719E+02 2.876E+02 NOT IDENT. AM-241 "'"4.695E-02 1. 067E-01 1.087E-01 NOT IDENT. CM-243 -3.837E-02 8.224E-02 8.404E-02 FAIL ABUN BK-247 9. 963E-04 7.866E-02 7. 8 66E-02 NOT IDENT. CM-247 -l.347E-02 3.384E-02 3.438E-02 NOT IDENT. CF-249 1.280E-02 3.813E-02 3.857E-02 NOT IDENT. CF-251 2.427E-02 1.021E-01 1.026E-01 FAIL ABUN Page 4074 of 5809
GEL Laboratories LLC *
2040 Savage Road * '* Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 6.2529 87.09 54.0667 136.47. 43.5320 45.60 40 .1511 87.57 54.1243 140.51 0.0000 46.54 40.2801 88.03 42.4010 143.76 54.8029 49.72 0.0000 88.34 42.4299 144.24 52.8852 51. 35 32.8973 88.47 42.4420 145.44 59.8523 51. 87 38.5774 89. 96 49.6772 152.43 58.5067 52.39 37.8354 1093.63 49.7505 153.25 0.0000 52. 97 43.5493 91.11 0.0000 323.87 47.7246 53.44 46.8436 92.59 49.9587 156.02 0.0000 54.07 41.2*700 93.35 50.0395 158.56 0.0000 57.36 0.0000 94.56 50 .1672 159.00 48.0608 57.53 40.0665 94.65 50.1766 162.33 46.2787 57.98 38.4817 94.67 50.1788 162.66 0.0000 59.27 58.0766 94.87 49.0045 163.33 . 44.3297 59.32 58.0849 97.43 61.2810 165.86. 40.4437 59.54 46.0588 98.43 46.9580 176.31 46.1563 60. 96' 48.4482 98.44 46.9592 176.60 0.0000 61.17 46.2735 99.53 41.6328 177.52 39. 0396 62.93 50.6541 100 .11 41. 6815 181.07 0.0000 63.29 50.7045 102.03 48.2092 181.52 38.2138 63.58 50.7451 103.18 59.2593 184.41 41.4685 64.28 50.8427 103.37 52.8975 143.76 34.2694 66.73 58.1720 105.21 43.0197 193.51 36.7085 67.24 57.1306 105.31 43.0284 197.03 45.2964 125.81 51.3091 106.12 53.1820 198.01 33.7500 67..75 51.3184 106.47 69.7343 201.83 50.8616 69.67 56.6504 109.28 47.0475 203.43 39.2820 70.83 56.5364 111. 00 60.1569 205.31 46.8192 72. 81 46.0252 111. 76 0.0000 210.85 55.6967 72. 87 46.0322 114. 06 55.8458 215.65 29.0814 74.66 46.2377 116. 30 0.0000 222 .11 37.9774 74.82 46.2559 116.74 54.2484 227.09 34.9165 74.97 46.2732 119. 76 43.2580 227.38 34.9277 77 .11 46.5150 121.12 43.3622 228.16 0.0000 78.74 46.6971 121. 22 36:7702 228.18 30.5891 79.69 46. 80.26 121.78 42.4687 116.74 30.5891 80.12 46.8500 122.06 46.2665 235.69 39.6530 80.19 0.0000 122.92 51.0642 235. 96 36.7264 80.57 46.8994 123.07 51. 0774 238.63 54.1433 81. 00 46.9468 265.00 55.8662 238.98 0.0000 81. 07 46.9542 125.81 44.6672 240.99 56.1256 81.75 55.7378 127.23 56.2071 242.00 45.8359 83.79 61.2500 127.91 47.6885 244.70 33.3627 84.00 42.0201 129.30 44.9324 252.40 0.0000 85.43 81.9707 131.20 46 .*9940 252.80 25.7939 86.55 54.0017 133.02 50. 0211 254.15 0.0000 8 6. 7 9 54.0303 133.52 56.8015 256.23 34.5122 86.94 54.0485 136.00 43.4990 260.90 0.0000 Page 4075 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 . 30.2653 355.39 0.0000 584.27 9.4914 264.80 30.2694 356.01 22.9585 595.83 0.0000 265.00 30.2751 364.49 0.0000 427.87 9.5732 268.22 28.8525 366.42 0.0000 602.52 0.0000 269.46 27.3677 372. 51 21.1774 604. 72 8.6342 270.03 30.8051 375.05 23.7146 607.14 5.7632 271. 23 41.1218 377.52 12.5046 609.32 9.6163 273.65 0.0000 356.01 21 *. 7772 610.33 9.6212 276.40 30.9955 388.16 20.1660 614.28 5.7844 277.37 32.1733 388.63 0.0000 618.01 20.2839 277.60 31.0309 391.69 22.7455 620. 36 12. 5715 278.00 26.4442 264.66 21.1980 621. 93 13.5494 279.20 28.7766 401.81 22.0645 630.19 0.0000 279.54 32.2400 402.40 22.0734 631. 29 13.1270 279.70 28.7903 404.85 17.0093 633.25 8.7598 280.46 26.5060 410.95 14.5205 634.78 0.0000 283.69 15.0273 413.71 14.5485 635.95 11. 6953 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 28.9452 423. 72 0.0000 645.85 7.8350 285.90 0.0000 427.09 15.5475 657.76 8.8656 287.50 20.8812 427.87 15.5559 657.90 0.0000 290.67 23.2697 433.94 16.4878 661. 66 16.7773 293.27 0.0000 439.40 21.7738 664.57 0.0000 351. 93 29.5978 453.88 21.9823 666.33 0.0000 295.96 29.6171 463.37 19.4631 666.50 0.0000 879.38 32.8125 468.07 12.4229 667. 71 0.0000 299.98 26.5964 473.00 0.0000 677.62 11. 9331 300.09 26.5992 475.06 11. 58 66 685.70 Q.0000 300.13 26.5999 476.78 11. 5990 695.00 0.0000 301.36 26.6289 477.60 11. 6048 696.49 7.5241 302.85 26.6649 482.18 17.0092 696. 51 7.5241 256.23 26.7036 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 7.5269 306.78 28.3323 497.08 7.2274 697.49 9.0330 308.46 31.5267 505.52 19.0684 702.65 9.0542 311. 90 29.6455 507.63 0.0000 706.68 12.0947 316.51 16.6677 511. 00 23.6855 711. 68 12.1221 319.41 0.0000 514.00 12.3201 720. 70 0.0000 320.08 0.0000 514.00 12.3201 721. 93 0.0000 321. 04 25.0990 520.40 7.3281 722.78 9.7461 323.87 20.7669 520.69 0.0000 722. 91 13.7060 325.23 23.9893 522.65 0.0000 723.31 12.1855 328.76 0.0000 527.90 0.0000 724.19 7.6190 333.37 21.7375 528.26 13.8031 727. 33 8 .1383 333.97 21.7485 529.59 11. 0508 733.00 6.1189 334.37 25.7845 529.87 0.0000 735.93 15.3174 338.28 20.6134 531.02 0.0000 333.97 8.1748 338.32 20.6140 537.26 0.0000 739.50 0.0000 311. 90 30.7729 546.56 0.0000 747.24 9.2358 340.48 30.7729 552.55 15.8600 748.06 11.2923 340.55 0.0000 563.25 15.0150 752.31 14.3982 344.28 23.1510 569.33 6.5910 753.82 0.0000 345.93 19.5215 946.00 5.6499 756.73 9.8922 351. 06 19.6021 569.70 5.6504 756.80 7.7283 351.93 19.6157 583.19 9.4861 884.68 10.8529 Page 4076 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:06:24.63 *********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;119 Background date : Z-OCT-2016 11:02:18. Sample date 7-DEC-2015 13:02:00. Acquisition date : 3-0CT-2016 07:04:39. Sample ID G405235051 Sample quantity 1.53012E+02 GRAM Detector name : GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:05.93 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 6 6 2 2 2 2 0 0 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4078 of 5809 Energy 46.53* 63.22* 74.93* 77.27* 84.44* 87.37 89.91 92.78* 156.62 186.12* 238.79* 241. 96 260.11 271.39 277".18 280.70 295.61 300.46 328.52* 338.49 352.28* 458.10 494.31 512.04* 543.77 548.25 583.75* 609.86*

662.29* 728.27* 735.71 786.96 853.65 860.64 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 22 50 232 289 58 128 76 107 39 65 304 76 19 65 48 19 109 19 24 61 198 10 14 24 11 12 112 142 41 39 27 10 13 33 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 188 256 180 113 115 124 103 95 94 118 100 65 50 64 15 31 58 41 65 54 38 19 20 55 12 30 13 42 27 16 12 10 12 3 1. 04 0.73 1. 26 0.78 1. 51 1. 32 1.16 1.19 4.03 1. 02 0.89 1.22 0.86 3.61 2.39 1. 98 1. 44 0.90 2.29 1.19 1. 06 1. 05 1.18 2.31 1. 00 0.60 1. 33 1. 34 1. 49 1. 54 3.28 0.70 0.97 3.12 93.36 126.73 150.14 154.82 169.16 175.00 180.08 185.83 313. 48 372.45 477.78 484.10 520.41 542. 96 554.54 561.57 591.39 601.08 .657.20 677.12 704.71 916.32 988.71 1024.17 1087.64 1096.59 1167. 58 1219.80 1324. 66 1456.62 1471. 51 1574.02 1707.39 1721. 38 88 122 145 145 166 166 166 166 307 368 473 482 515 535 550 550 587 597 651 672 700 910 982 1015 1081 1090 1163 1214 1318 1450 1464 1570 1698 1715 10 6.24E-03121.4 10 l.39E-02 64.6 14 6.46E-02 11.9 14 8.03E-02 8.2 26 l.61E-02 33.6 26 3.56E-02 17.3 26 2.llE-02 25.0 26 2.97E-02 21.6 11 1. 07E-02 51. 7 10 1.80E-02 35.8 9 8.43E-02 8.4 7 2.12E-02 21.5 9 5.14E-03 72.4 15 l.80E-02 30.7 19 1. 33E-02 21. 2 19 5.40E-03 66.1 10 3.03E-02 16.1 8 5.29E-03 63.0 12 6.74E-03 71.0 12 1.70E-02 26.8 10 5.51E-02 9.3 8 2.76E-03 85.9 10 3.89E-03 65.5 22 6. 73E-03 91. 7 9 3.02E-03 67.2 16 3.31E-03104.1 13 3. lOE-02 11. 8 14 3.96E-02 12.9 13 1.14E-02 30. 6 14 l.08E-02 28.0 16 7.46E-03 34.7 7 2.81E-03 61.3 12 3.61E-03 60.1 13 9.09E-03 20.9 Fit 1.87E+OO 1. 75E+00 1.41E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 900. 96 10 18 3.43 1802.03 1794 13 .2.65E-03100.2 36 0 911. 87* 61 23 1. 48 1823.85 1817 15 1.70E-02 21.5 37 0 970.76* 23 43 1. 28 1941.66 1931 15-6. 27E-03 68.4 38 0 1028.71 13 4 0.99 2057.58 2054 8 3.61E-03 38.5 39 0 1048.47 8 11 1. 45 2097.10 2090 9 2.35E-03 78.6 40 0 1121.13 38 11 1. 56 2242.45 2234 16 1.05E-02 26.0 41 0 1134.76 9 14 4.57 2269.70 2259 18 2.54E-03100.0 42 0 1205.40 7 12 1. 52 2411.03 2405 11 2. OOE-03 97.7 43 0 1238.36 28 7 3.28 2476.97 2471 13 7.82E-03 26.6 44 0 1342.79 10 2 1. 34 2685.89 2680 10 2.65E-03 44.8 45 0 1461. 79* 261 8 1. 95 2923.97 2916 15 7.25E-02 6.7 46 0 1765.78 31 0 2.15 3532.26 3525 13 8.61E-03 18.0 Flag: "*" = Peak area was modified by background subtraction Page 4079 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:06:27 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 7-DEC-2015 13:02:00 G405235051 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:04:39 153.01 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA41 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 4080 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:05.93 10.00 0.00 % Peak Energy 0.2% Nuclide Line Activity Report Page : 2 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.926E-01 1.300E+Ol l.300E+Ol 13. 33* OK Y-91 1204.77 0.26* 1.057E+OO l.267E+Ol 4.470E+02 195.37 OK CD-109 88.03 3.70* 7.448E+00 2.086E+OO 3.278E+OO 49.90 OK SN-126 64.28 9.60 7.794E+OO 4.293E-01 4.293E-01 129.22 OK 86.94 8.90 7.448E+OO 8.674E-01 8.674E-01 49.90 OK 87.57 37.00* 7.448E+OO 2.086E-01 2.086E-01 49.90 OK BA-137M 661. 66 89.90* 1. 826E+00 1.288E-01 l.313E-01 61. 28 OK CS-137 661.66 85.10* l.826E+00 l.361E-01 l.387E-01 61. 28 OK TL-208 277.37 6.60 3.909E+OO l.048E+OO 1.048E+OO 42.35 OK 583.19 85.00* 2.050E+OO 3.357E-01 3.357E-01 23.63 OK 860.56 12.50 l.434E+OO 9.175E-01 9.175E-01 41.72 OK PB-210 46.54 4.25* 7.553E+00 4.626E-01 4.746E-01 242.82 OK BI-211 72.87 1.23 7. 711E+OO Line Not Found Absent 351.06 12.92* 3.211E+OO 1.678E-01 l.678E-01 557.00 OK PB-212 74.82 10.28 7.682E+OO 1.364E+OO 1.364E+OO 34.74 OK 77.11 17 .10 7.644E+OO 1.400E+OO 1.400E+OO 16.44 OK 238.63 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 OK 300.09 3.30 3.665E+OO 8.817E-01 8.817E-01 125.98 OK BI"-214 609.32 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 OK 1120.29 14.92 1.127E+OO 1.101E+OO 1.102E+OO 51. 95 OK 1764.49 15.30 7.616E-01 1.234E+OO 1.235E+OO 35.92 OK PB-214 74.82 5.80 7.683E+OO -----* Line Not Found <<INT Reject 77 .11 9.70 7.644E+OO 2.469E+OO 2.470E+OO 16.44 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3. 713E+OO 8.949E-01 8.952E-01 32.29 OK 351. 93 35.60* 3.214E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 OK 1120. 29 14.92 1.127E+OO 1.101E+OO l.102E+OO 51. 95 OK 1764.49 15.30 7.616E,-01 1.234E+OO 1.235E+OO 35.92 OK RA-224 240.99 4.10* 4.341E+OO 8.710E-01 8.710E-01 134.52 OK RA-226 609.32 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 OK 1120.29 14.92 1.127E+OO l.101E+OO l.102E+OO 51. 95 OK 1764.49 15.30 7.616E-01 l.234E+OO l.235E+OO 35.92 OK TH-228 74.82 10.28 7.682E+OO 1.364E+OO l.364E+OO 34.74 OK 77.11 17 .10' 7.644E+OO 1.400E+OO 1.400E+OO 16.44 OK 238.63 43.60* 4.384E+OO 9.086E-01 9.086E-Gl 16.78. OK 300.09 3. 30_ 3.665E+OO 8.817E-01 8.817E-01 125.98 OK TH-229 85.43 14.70 7.510E+OO 3.303E-01 3.303E-01 67.29 OK 88.47 24.00 7.448E+OO 3.217E-01 3.217E-01 49.90 OK 193.51 4.41* 5.088E+OO Line Not Found Absent 210.85 2.80 4.797E+OO Line Not Found Absent TH-230 609.32 45.49* 1. 969E+OO 8.289E-01 8.289E-01 25.86 OK 1120.29 *14. 92 1.127E+OO 1.101E+OO 1.101E+OO 51. 95 OK 1764.49 15.30 7.616E-01 1.234E+OO 1.234E+OO 35.92 OK PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.665E+OO 5.438E-01 5.438E-01 125.98 OK TH-234 63.29 3.70* 7.794E+OO 1.114E+OO 1.114E+OO 129.22 OK 92.59 4.23 7.327E+OO 2.152E+OO 2.152E+OO 43 .13 OK Page 4081 of 5 809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Nuclide Type: Uncorrected Decay* Corr 2-Sigma Nuclide .Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status U-234 609.32 45.49* 1. 969E+OO 8.289E-01 8.289E-01 25.86 OK 1120.29 14.92 l.127E+OO l.101E+OO 1.101E+OO 51. 95 OK p64. 49 15.30 7.616E-01 1.234E+OO 1.234E+OO 35.92 OK U-235 89. 96 3.47 7.392E+OO 1.853E+OO 1.853E+OO 50.01 OK 93.35 5.60 7.327E+OO 1.626E+OO 1. 626E+OO 43.13 OK 143.76 10. 96* 6.093E+OO Line Not Found .-----Absent 163.33 5.08 5.667E+OO Line Not Found Absent 185. 72 57.20 5. 221E+OO 1.270E-01 l.270E-01 71. 51 OK 205.31 5.01 4.887E+00 Line Not Found Absent U-238 63.29 3.70* 7.794E+OO l .114E+OO 1.114E+OO 129.22 OK 92.59 4.23 7.327E+OO 2.152E+OO 2.152E+OO 43.13 OK AM-243 43.53 5.90 7.421E+00 Line Not Found Absent 74.66 67.20* 7.682E+OO 2.087E-01 2.087E-01 34.74 OK ANH-511 511.00 100.00* 2.310E+OO 5.569E-02 5.569E-02 183.43 OK Flag: "*" = Keyline Page 4082 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:06:28.18 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l *
Acquisition date 3-0CT-2016 07:04:39 Sensitivity : 3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:05.93 Half life ratio : ***** *
Sample date 7-DEC-2015 13:02:00 Analyst initials: MXRl *
Sample ID G405235051 Sample Quantity 1.5301E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3 .
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.300E+Ol 1.698E+OO Y-91 4.470E+02 8.558E+02 CD-109 3.278E+00 1.603E+OO SN-126 2.086E-01 1. 02.0E-01 BA-137M 1.313E-01 7.883E-0'2 CS-137 1.387E-01 .8. 328E-02 TL-208 3.357E-01 7.773E-02 PB-210 4.746E-01 1.130E+OO BI-211 l.678E-01 9.159E-01 PB-212 9.086E-01 l.494E-01 BI-214 8.292E-01 2.lOlE-01 PB-214 9.561E-01 l.742E-01 RN-222 8.292E-01 2.lOlE-01 RA-224 8. 710E-01 1.148E+OO RA-226 8.292E-01 2.lOlE-01 TH-228 9.086E-01 1.494E-01 TH-229 -2.973E-01 4.543E-01 TH-230 8.289E-01 2.lOlE-01 PA-231 5.438E-01 6.714E-01 TH-234 1.114E+OO 1.411E+OO U-234 8.289E-01 2.lOlE-01 U-235 4.726E-02 1.889E-01 U-238 1.114E+OO 1. 411E+OO AM-243 2.087E-01 7.104E-02 ANH-511 5.569E-02. 1.00lE-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 4083 of 5809 Key-Line Activity (pCi/GRAM -9.905E+OO . -3.849E-02 O.OOOE+OO 1.664E-03 2.488E-01 K.L. Cnt Uncert ( 1. 96-sigma) 1.264E+Ol 6.037E-02 1.960E+41 l.836E-02 4.412E-01 MDA (pCi/GRAM 5.762E-01 l.170E+03 1. 471E+OO 9.347E-02 7.425E-02 7.844E-02 6.576E-02 7.877E-01 3.364E-01 1.177E-01 l.538E-01 3.267E-01 1.538E-01 1.294E+OO 1.538E-01 1.177E-01 8.385E-01 l.537E-01 8.080E-01 9.795E-01 1. 537E-01 3.814E-01 9.795E-01 5.273E-02 4.910E-02 MDA (pCi/GRAM 2.128E+Ol 1.040E-01 O.OOOE+OO 5 .113E-02 9.554E-01 NOT IDENT . NOT IDENT. SHORT HLIF NOT IDENT-. FAIL ABUN V-48 0.000E+OO 1.406E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 3.986E+02 O.OOOE+OO SHORT HLIF MN-54 3.448E-03 6.698E-02 l.359E-01 NOT IDENT. C0-56 -l.502E-01 5.118E-01 8.557E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.592E-02 4.512E-02 9.149E-02 NOT IDENT. C0-58 -4.077E-01 5.687E-01 l.016E+OO NOT IDENT. FE-59 4.668E-Ol 8.611E+OO 1.706E+Ol NOT IDENT. C0-60 1.536E-02 4.084E-02 9.061E-02 NOT IDENT. ZN-65 6.570E-02 l.945E-01 3.750E-01 NOT IDENT. GE-68 4.490E-01 2.176E+OO 4. 672E+OO NOT IDENT. AS-73 2.039E+OO 2.404E+OO 4.729E+OO NOT IDENT. AS-74 O.OOOE+OO 6.889E+03 O.OOOE+OO SHORT HLIF SE-75 -l.930E-01 2.066E-01 3.385E-01 FAIL ABUN BR-77 O.OOOE+OO 3.519E+37 O.OOOE+OO SHORT HLIF SR-8'2 O.OOOE+Od 8.857E+02 O.OOOE+OO SHORT HLIF RB....,83 3.740E-01 7.598E-01 l.413E+OO NOT IDENT. KR-85 6.826E+OO 7.254E+OO 1.537E+Ol NOT IDENT. SR-85 7.262E-01 7.737E-01 1.639E+OO NOT IDENT. RB-86 O.OOOE+OO 2.824E+04 O.OOOE+OO SHORT HLIF Y-88 7.026E-02 1.131E-01 3. 972E-01 NOT IDENT. NB-94 -1. 570E-02 3.316E-02 6.234E-02 NOT IDENT. NB-95 l.098E-01 9.230E-01 l.873E+00 NOT IDENT. NB-95M -3. 960E_:Ol 2.489E+OO 4.241E+OO NOT IDENT. ZR-95 l.370E-01 1.662E+OO 3.362E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO *2. 544E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 241E+41 O.OOOE+OO SHORT HLIF RH-101 -1.179E-02 3.198E-02 6 .172E-02 NOT IDENT. RH-102 2.537E-02 6.707E-02 l.406E-01 NOT IDENT. RU-103 -2.731E+OO 7.0lOE+OO 1. 096E+Ol . FAIL ABUN RH-106 4.272E-02 5.094E-01 9.857E-01 NOT IDENT. RU-106 4.272E-02 5.094E-01 9.857E-01 NOT IDENT. AG-108M 5.362E-03 3.040E-02 5.904E-02 NOT IDENT. AG-llOM -5.692E-02 l.085E-01 2.067E-01 NOT IDENT. SN-113 -8.789E-03 2.399E-01 4.566E-01 NOT IDENT. CD-115 O.OOOE+OO 4.233E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.069E+05 O.OOOE+OO SHORT HLIF TE-123M -2.612E-02 1. 380E-01 2. 396E-01 NOT IDENT. SB-124 -5.218E-01 1.617E+OO 3.487E+OO NOT IDENT. SB-125 -2.784E-02 1.162E-01 2 .139E-01 NOT IDENT. TE-125M -1. 675E+Ol 2.421E+02 4.789E+02 NOT IDENT. I-126 O.OOOE+OO l.258E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1 .. 222E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.780E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 6.007E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.214E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 4.475E+26 O.OOOE+OO SHORT HLIF BA-133 -6 .117E-03 4.514E-02 7.584E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.308E-02 4.045E-02 9.921E-02 NOT IDENT. CS-135 5.576E-02 1.594E-01 2.868E-01 NOT IDENT. I-135 O.OOOE+OO 8.234E+40 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 5.085E+05 O.OOOE+OO SHORT HLIF CE-139 1.499E-03 1.113E-01 2.'182E-01 NOT IDENT. BA-140 O.OOOE+OO 1.592E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.103E+05 O.OOOE+OO SHORT HLIF CE-141 -5.610E+OO 2.576E+Ol 4.975E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.612E-01 3.344E-01 6.250E-01 NOT IDENT. PM-144 -1. 271E-02 5.816E-02 1.136E-01 NOT IDENT. PR-144 -1.122E+OO 5.052E+OO 9.862E+OO NOT IDENT. PM-146 1.233E-02 4. 551E-02 8.241E-02 FAIL ABUN ND-147 O.OOOE+OO 3.647E+07 O.OOOE+OO SHORT HLIF PM-147 5.635E+02 7.602E+02 l.583E+03 NOT IDENT: PM-149 O.OOOE+OO 6. 451E+40 O.OOOE+OO SHORT HLIF EU-150 2.322E-02 2.665E-02 4.924E-02 FAIL ABUN EU-152 -4.215E-02 1.073E-01 l.855E-01 NOT I DENT'. GD-153 -5.847E-03 1.593E-01 2.862E-01 NOT IDENT. EU-154 -6.285E-02 *l.416E-01 2. 551E-01 NOT IDENT. EU-155 7.073E-02 8.831E-02 l.856E-01 FAIL ABUN TB-160 3.949E-01 1. 749E+OO 3.755E+OO FAIL ABUN H0-166M 2.629E-03 6.136E-02 1.240E-01 FAIL ABUN TM-171 -4.548E+OO 5.503E+OO 9.567E+OO NOT IDENT. HF-172 7.144E-05 2.174E-01 4.284E-01 FAIL ABUN LU-172 4.815E-02 9.393E-02 1.999E-01 FAIL ABUN LU-176 3.198E-03 2.297E-02 4.520E-02 FAIL ABUN Page 4084 of 5809 HF-181 3.504E-02 3.953E+OO 7.685E+OO NOT IDENT. TA-182 3.794E-01 l.170E+OO 2.381E+OO FAIL ABUN RE-183 4.452E-01 1.069E+OO 2.036E+OO NOT IDENT. RE-184 -2.397E+OO 4.090E+Ol 7.080E+Ol NOT IDENT. W-188 3. 965E+Ol l.145E+02 2.194E+02 FAIL ABUN IR-192 l.141E-01 4.360E-01 8.704E-01 FAIL ABUN HG-203 2.914E+OO 2.444E+OO 4.930E+OO NOT IDENT. . BI-207 -3.388E-02 6. 251E-02 l .118E-01 FAIL ABUN PB-211 1. 721E-01 7.210E-01 l.408E+OO NOT IDENT. BI-212 O.OOOE+OO 9.842E-01 *1.501E+OO FAIL ABUN RN-219 2.931E-01 3.618E-01 7.664E-01 FAIL ABUN RA-223 1. 282E-01 6.579E-01 l.162E+OO FAIL ABUN AC-227 1. 819E-03 2.360E-01 4.121E-01 FAIL ABUN TH-227 l.819E-03 2.360E-01 .4 .121E-01 FAIL ABUN AC-228 O.OOOE+OO 3.673E-01 5.974E-01 FAIL ABUN RA-228 O.OOOE+OO 3.673E-01 5.974E-01 FAIL ABUN TH-231 l.282E-01 6.579E-01 l.162E+OO FAIL ABUN TH-232 O.OOOE+OO 3.673E-01 5.974E-01 FAIL ABUN PA-233 5.092E-02 6.0lOE-02 l.256E-01 FAIL ABUN PA-234 2.470E-02 2.577E-01 5.399E-01 NOT IDENT. PA-234M l.659E-01 5 .139E+OO 1. OllE+Ol NOT IDENT. NP-237 5.092E-02 6.0lOE-02 1. 25 6E-01 FAIL ABUN NP-238 O.OOOE+OO l.144E+41 O.OOOE+OO SHORT HLIF NP-239 2.606E-02 2.200E-01 4.407E-01 FAIL ABUN PU-239 -9.135E+Ol 2.876E+02 5.568E+02 NOT IDENT. AM-241 3.959E-02 5.594E-02 l.OlOE-01 NOT IDENT. CM-243 -l.313E-02 8.149E-02 l.613E-01 FAIL ABUN BK.:._247 -6.742E-02 7.765E-02 l.180E-01' FAIL ABUN CM-247 -3.867E-04 3.580E-02 6. 831E-02 FAIL ABUN CF-249 4.362E-03 3.545E-02 6.945E-02 NOT IDENT. CF-251 -7.098E-02 l.159E-01 2.158E-01 NOT IDENT. Page 4085 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:06:25.44 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 252 10.66* 8.926E-01 l.300E+Ol l.300E+Ol 13.33 Y-91 1204.77 7 0.26* l.057E+OO l.267E+Ol 4.470E+02 195.37 CD-109 88.03 164 3.70* 7.448E+OO 2.911E+OO 4.574E+OO 34.58 SN-126 64.28 65 9.60 7.794E+OO 4.293E-01 4.293E-01 129.22 86.94 164 8.90 7.448E+OO l.210E+OO l.210E+00 34.58 87.57 164 37.00* 7.448E+OO 2. 911E-01 2. 911E-01 . 34.58 BA-137M 661. 66 43 89.90* l.826E+OO l.288E-01 1. 313E-01 61. 28 CS-137 661.66 43 85.10* l.826E+OO l.361E-01 l.387E-01 61.28 TL-208 277.37 55 6.60 3.909E+00 l.048E+OO . 1. 048E+OO 42.35 583.19 119 85.00* 2.050E+00 3.357E-01 3.357E-01 23.63 860.56 34 12.50 l.434E+OO 9.175E-01 9.175E-01 41.72 PB-210 46.54 30 4.25* 7.553E+OO 4.626E-01 4.746E-01 242.82 BI-211 72. 87 ------1. 23 7.711E+OO ------Line Not Found ------351.06 223 12.92* 3.211E+OO 2.633E+00 2.633E+00 18.59 PB-212 74.82 301 10.28 7.682E+00 l.869E+00 l.869E+OO 23.80 77.11 373 17.10 7.644E+OO l.400E+oo* l.400E+OO 16.44 238.63 354 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 300.09 22 3.30 3.665E+00 8.817E-01 8.817E-01 125.98 BI-214 609.32 151 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 1120.29 38 14.92 l.127E+OO l.lOlE+OO l.102E+OO 51. 95 1764.49 29 15.30 7.616E-01 l.234E+OO l.235E+OO 35.92 PB-214 74.82 301 5.80 7.682E+OO 3.312E+OO 3.314E+OO 23.80 77 .11 373 9.70 7.644E+OO 2.469E+OO 2.470E+OO 16.44 87.09 164 3.41 7.448E+00 3.159E+OO 3.160E+OO 34.58 242.00 89 7.25 4.341E+00 l.387E+OO l.388E+OO 42.98 295.22 125 18.42 3.713E+OO 8.949E-01 8.952E-01 32.29 351.93 223 35.60* 3.211E+OO 9.557E-01 9.561E-01 18.59 RN-222 609.32 151 45.49* 1. 969E+OO 8.289E-01
8 .292E-01 25.86 1120.29 38 *14.92 l.127E+OO l.101E+OO l.102E+OO 51. 95 1764.49 29 15.30 7.616E-01 l.234E+OO l.235E+OO 35.92 RA-224 240.99 89 4.10* 4. 341E+OO 2.453E+OO 2.453E+OO 42.98 RA-226 609.32 151 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 1120.29 38 14.92 l.127E+00 l .101E+OO l.102E+OO 51. 95 1764.49 29 15.30 7.616E-01 l.234E+OO l.235E+OO 35.92 TH-228 74.82 301 10.28 7.682E+OO l.869E+OO 1. 869E+OO 23.80 77 .11 373 17.10 7.644E+OO l.400E+OO l.400E+00 16.44 238.63 354 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 300.09 22 3.30 3.665E+OO 8.817E-01 8.817E-01 125.98 TH-229 85.43 74 14.70 7.510E+OO 3.303E-01 3.303E-01 67.29 88.47 164 24.00 7.448E+OD 4.488E-01 4.488E-01 34.58 193.51 ------4.41* 5.088E+OO ------Line Not Found ------210.85 ------2.80 4.797E+OO ------Line Not Found ------TH-230 609.32 151 45.49* 1. 969E+OO 8.289E-01 8.289E-01 25.86 1120.29 38 14.92 l.127E+OO l.101E+OO l.101E+OO 51. 95 1764.49 29 15.30 7.616E-01 l.234E+00 l.234E+OO 35.92 PA-231 283.69 ------1. 70 3.838E+00 ------Line Not Found ------301.36 22 5.35* 3.665E+OO 5.438E-01 5.438E-01 125.98 Page 4086 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235051 Acquisition date Page : 2 3-0CT-2016 07:04:39 Nuclide Type: Nuclide TH-234 U-234 U-235 U-238 AM-243 ANH-511 . Flag: "*" Page 4087 of 5809 Energy 63.29 92.59 609.32 1120.29 1764.49 89.96 93.35 143.76 163.33 185. 72 205.31 63.29 92.59 43.53 74.66 511.00 Key line Area 65 136 151 38 29 97 136 ------------77 ------65 136 ------301 26 %Abn %Ef f 3.70* 7.794E+OO 4.23 7.327E+OO 45.49* 1. 969E+OO 14.92 1.127E+OO 15.30 7.616E-01 3.47 7.392E+OO 5.60 7.327E+OO 10. 96* 6.093E+OO 5.08 5.667E+OO 57.20 5.221E+OO 5.01 4.887E+OO 3.70* 7.794E+OO 4.23 7.327E+OO 5.90 7. 421E+OO 67.20*. 7.682E+OO 100.00* 2.310E+OO Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi7GRAM %Error 1.114E+OO l.114E+OO 129.22 2.152E+OO 2.152E+OO 43 .13 8.289E-01 8.289E-01 25. 86 1.101E+OO l.101E+OO 51.95 1.234E+OO 1.234E+OO 35.92 1.853E+OO l.853E+OO 50.01 1.626E+OO 1.626E+OO 43 .. 13 ------Line Not Found ------------Line Not Found'-*------1.270E-01 1.270E-01 71. 51 ------Line Not Found ------1.114E+OO l .114E+OO 129.22 2.i52E+OO 2.152E+OO 43 .13 ------Line Not Found ------2.859E-01 2. 859E.-01 23.80 5.569E-02 5.569E-:-02 183.43 Page : 3 Summary of Nuclide Activity Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Total number of lines in spectrum 46 Number of unidentified lines 9 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlif e 1.25E+09Y 58.51D 461. 40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600. OOY 1600.00Y 1. 41E+10Y 1600.00Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 35.3 1. 57 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 . 1. 00 1. 00 1. 00 . 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM .1.300E+Ol 1.267E+Ol 2. 911E+OO 2. 911E-01 1.288E-01 1.361E-01 3.357E-01 4.626E-01 2.633E+OO 9.086E-01 8.289E-01 9.557E-01 8.289E-01 2.453E+OO 8.289E-01 9.086E-01 4.488E-01 8.289E-01 5.438E-01 1.114E+OO 8.289E-01 1. 270K-01 1.114E+OO 2.859E-01 5.569E-02 4.563E+Ol 4.563E+Ol Decay Corr pCi/GRAM 1.300E+Ol 4.470E+02 4.574E+OO 2. 911E-01 1. 313E-01 l.387E-01 3.357E-01 4.746E-01 2.633E+00 9.086E-01 8.292E-01 9.561E-01 8.292E-01 2.453E+OO 8.292E-01 9'.086E-01 4.488E-01 8.289E-01 5.438E-01 1.114E+OO 8.289E-01 1.270E-01 1.114E+OO 2.859E-01 5.569E-02 4.816E+02 4.816E+02 80.43% Decay Corr 2-Sigma Error 0.173E+Ol 8.732E+02 1.582E+OO 1.007E-01 0. 804E-0-1 0.850E-01 0.793E-01 11. 53E-01 0.489E+OO 1.525E-01 2.144E-01 1.777E-01 2.144E-01 1.054E+00 2.144E-01 1.525E-01 1.552E-01 2.144E-01 6. 851E-01 1.439E+OO 2.144E-01 0.908E-01 1.439E+OO 0.681E-01 10.21E-02 "M" Manually .accepted 2-Sigma %Error 13.33 195.37 34.58 34.58 61. 28 61. 28 23.63 242.82 18.59 16.78 25.86 18.59 25.86 42.98 25.86 16.78 34.58 25.86 125.98 129.22 25.86 71. 51 129.22 23.80 183.43 Flags: "K" Keyline not found = Manually edited "A" = Nuclide specific abn. limit Page 4088 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235051 Acquisition date : 3-0CT-2016 07:04:39 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 156.62 47 114 4.03 313.48 307 11 1.07E-02 **** 5.81E+OO T 0 260 .11 21 57 0.86 520.41 515 9 5.14E-03 **** 4. llE+OO T 0 271.39 75 74 3.61 542. 96 535 15 l.80E-02 61. 5 3.97E+00 T 5 280.70 22 36 1. 98 561.57 550 19 5.40E-03 **** 3.87E+00 T 0 328.52 27 74 . 2.29 657.20 651 12 6.74E-03 **** 3.41E+OO T 0 338.49 69 61 1.19 677.12 672 12 1.70E-02 53.5 3.32E+00 T 0 458.10 11 21 1. 05 916.32 910 8 2.76E-03 **** 2.55E+OO 0 494.31 15 22 1.18 988.71 982 10 3.89E-03 **** 2.38E+OO 0 543.77 12 13 1. 00 1087.64 1081 9 3.02E-03 **** 2.19E+00 0 548.25 13 32 0.60 1096.59 1090 16 3.31E-03 **** 2.17E+OO 0 728. 27 41 17 1. 54 1456.62 1450 14 1.08E-02 56.1 1.67E+OO T 0 735.71 28 13 3.28 1471.51 1464 16 7.46E-03 69.4 1. 66E+OO T 0 786.96 10 10 0.70 1574.02 1570 7 2.81E-03 **** 1.56E+00 0 853.65 13 12 0.97 1707.39 1698 12 3.61E-03 **** 1.44E+OO 0 900. 96 10 19 3.43 1802.03 1794 13 2.65E-03 **** 1.37E+OO T 0 911. 87 62 23 1. 48 1823.85 1817 15 1.70E-02 43.0 1.36E+OO T 0 970. 76 23 44 1.28 1941.66 1931 15 6.27E-03 **** 1.28E+00 0 1028.71 13 4 0.99 2057.58 2054 8 3. 61E-03 76.9 1. 22E+00 T 0 1048.47 8 11 1. 45 2097.10 2090 9 2.35E-03 **** 1.20E+OO T 0 1134.76 9 14 4.57 2269.70 2259 18 2.54E-03 **** 1.12E+OO 0 1238.36 28 7 3.28 2476.97 2471 13 7.82E-03 53.2 1. 03E+OO T 0 1342.79 9 2 1. 34' 2685.89 2680 10 2.65E-03 89.5 '9. 61E-01 Flags: "T" = Tentatively associated Page 4089 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:06:43.28 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l *
Acquisition date 3-0CT-2016 07:04:39 Sensitivity : 3.000 *
Detector ID
GAM41 Energy tolerance: 1. 500 *
Elapsed live time: 0 01:00:00.00 *Abundance limit : 75.000 *
Elapsed real time: 0 01:00:05.93 Half life ratio : ***** *
Sample date 7-DEC-2015 13:02:00 Nuclide Library : SOLID *
Sample ID G405235051 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.5301E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 * * . . Dry Weight * : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.179E-01 4.991E+02 6.947E-01 4.415E-02 3.290E-02 3.476E-02 2. 896E-02 3.707E-01 1.516E-01 5.519E-02 6.928E-02 1. 57 4E-01 6.928E-02 6.081E-01 6.928E-02 5.519E-02 3.880E-01 6.926E-02 3.685E-01 4.649E-01 6.926E-02 1. 80.lE-01 4.649E-01 2.498E-02 2.159E-02 *----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4090 of 5809 Le (pCi/GRAM 9. 296E+00 4.368E-02 O.OOOE+OO 1.664E-02 4.192E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB...:95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4091 of 5809 O.OOOE+OO *5.897E-02 3.586E-Ol 0.000E+OO 4.305E-02 4.228E-01 7.405E+OO 3.759E-02 1.599E-01 1.949E+OO 2.243E+OO O.OOOE+OO 1.526E-01 O.OOOE+OO O.OOOE+OO 6.315E-01 6. 960E+OO 7.421E-01 O.OOOE+OO l.344E-01 2. 723E-02 8.259E-01 1.956E+OO 1.481E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.896E-02 6.285E-02 4.837E+OO 4.306E-01 4.306E-01 2.668E-02 . 8. 801E-02 2.061E-01 0.000E+OO O.OOOE+OO l .114E-01 1.177E+OO 9.649E-02 2.251E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.422E-02 O.OOOE+OO 4.282E-02 1.325E-01 O.OOOE+OO O.OOOE+OO 1.020E-01 O.OOOE+OO O.OOOE+OO 2.341E+Ol O.OOOE+OO 2.916E-01 4.983E-02 4.325E+OO 3.665E-02 O.OOOE+OO 7.448E+02 0.000E+OO 2.244E-02 8.445E-02 l.350E-01 l.072E-01 8.742E-02 1.592E+OO 5.461E-02 4.516E+OO 2.012E-01 8.739E-02 2.054E-02 3.364E+00 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL. ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 AC-228 RA-228 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4092 of 5809 1.043E+OO 9.650E-01 3.073E+Ol 1.006E+02 3.950E-01 2.273E+OO 4.812E-02 6.399E-01 6.899E-Ol 3.468E-01 5.307E-01 l.884E-01 1.884E-01 2.795E-01 2.795E-01 5.307E-01 2.795E-01 5.773E-02 2.271E-01 4.410E+OO 5.773E-02 O.OOOE+OO 2.071E-01 2.610E+02 4.792E-02 7.576E-02 5.329E-02 3. 081E-02 3.118E-02 l.004E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIJ;, ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:06:48.82 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l * *Acquisition date 3-0CT-2016 07:04:39 Sensitivity : 3.000 *
Detector ID GAM41 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:05.93 Half life ratio : ***** *
Sample date 7-DEC-2015 13:02:00 Nuclide Library ; SOLID *
Sample ID G405235051 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.5301E+02 GRAM *
Quantity Err(%) 1.3071E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.300E+Ol 2.028E+OO 2.028E+OO Y-91 4.470E+02 8.566E+02. 8.566E+02 CD-109 3 .278E+OO 1.650E+OO 1.650E+OO SN-126 Z.086E-01 1.044E-01 l.044E-01 BA-137M 1.313E-01 7.956E-02 7.956E-02 CS-137 l.387E-01 8.405E-02 8.405E-02 TL-208 3.357E-01 8.285E-02 8.285E-02 PB-210 4.746E-01 l.131Ef00 1.131E+OO BI-211 1.678E-01 9.645E-01 9.645E-01 PB-212 9.086E-01 1. 725E-01 1. 725E-01 BI-214 8.292E-01 2.215E-01 2.215E-01 PB-214 9.561E-01 l.923E-01 l.923E-01 RN-222 8.292E-01 2.215E-01 2. 2.15E-01 RA-224 8.710E-01 l.169E+OO 1.169E+OO RA-226 8.292E-01 2.215E-01 2.215E-01 TH-228 9.086E-01 1.725E-01 l.725E-01 .TH-229 -2.973E-01 4.551E-01 4.551E-01 TH-230 8.289E-01 2.215E-01 2.215E-01 PA-231 5.438E-01 6.826E-01 6.826E-01 TH-234 1.114E+OO 1.437E+OO 1.437E+OO U-234 8.289E-01 2.215E-01 2.215E-01 U-235 4.726E-02 1. 890E-01 1. 890E-01 U-238 1.114E+OO 1.437E+OO 1.437E+OO AM-243 2.087E-01 7.567E-02 7.567E-02 ANH-511 5.569E-02 1.002E-01 1.002E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) BE-7 -9.905E+OO l.267E+Ol 1.343E+Ol NOT IDENT. NA-22 -3.849E-02 6.045E-02 6.289E-02 NOT IDENT. NA-24 -l.000E+41 4.876E+41 O,OOOE+OO SHORT HLIF AL-26 1.664E-03 1. 836E-02 l.838E-02 NOT IDENT. SC-46 2.488E-01 4.421E-01 4.561E-01 FAIL ABUN Page 4093 of 5809 V-48 -1.673E+04 1. 425E+04 1. 612E+04 SHORT HLIF CR-51 -4.343E+02 4. 004E+o2 4.457E+02 SHORT HLIF MN-54 3.448E-03 6.698E-02 6.700E-02 NOT IDENT. C0-56 -l.502E-01 5.120E-01 5.165E-01 FAIL ABUN MN-56 -l.000E+41 3.409E+41 O.OOOE+OO SHORT HLIF C0-57 l.592E-02 4.516E-02 4.573E-02 NOT IDENT. C0-58 -4.077E-01 5.701E-01 5.990E-01 NOT IDENT. FE-59 4.668E-01 8. 611E+OO 8.614E+OO NOT IDENT. C0-60 1. 536E-02 4.086E-02 4.144E-02 NOT IDENT. ZN-65 6.570E-02 1.948E-01 l.970E-01 NOT IDENT . GE-68 . 4.490E-01 2.178E+OO 2.187E+OO NOT IDENT. AS-73 2.039E+OO 2.449E+OO 2.616E+OO NOT IDENT. AS-74 -1.552E+03 6.891E+03 6.927E+03 SHORT HLIF SE-75 -l.930E-01 2.073E-01 2.248E-01 FAIL ABUN BR-77 2 .139E+38 1.858E+39 O.OOOE+OO SHORT HLIF SR-82 7.499E+02 8.887E+02 9.508E+02 SHORT HLIF RB-83 3.740E-01 7.620E-01 7.805E-01 NOT IDENT. KR-85 6.826E+OO 7.278E+OO 7.901E+OO NOT IDENT. SR-85 7.262E-01 7.762E-01 8.424E-01 NOT IDENT. RB-86 1.049E+04 2.829E+04 2.869E+04 SHORT HLIF Y-88 7.026E-02 1.132E-01 l.175E-01 NOT IDENT. NB-94 -l.570E-02 3.319E-02 3.394E-02 NOT IDENT. NB-95 1.098E-01 9.231E-01 9.244E-01 NOT IDENT. NB-95M -3. 960E-01 2.490E+OO 2. 496E+OO NOT IDENT. ZR-95 l.370E-01 1.662E+OO l.663E+00 NOT IDENT. NB-97 -1.000E+41 3.611E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 4.071E+41 O.OOOE+OO SHORT HLIF M0-99 5.418E+31 2.545E+32 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 1.249E+41 O.OOOE+OO SHORT HLIF RH-101 -1.17 9E-02 3.208E-02 3.252E-02 NOT IDENT. RH-102 2.537E-02 6.712E-02 6.809E-02 NOT IDENT. RU-103 -2. 731E+OO 7.015E+OO 7.122E+00 FAIL ABUN RH-106 4.272E-02 5.094E-01 5.097E-01 NOT IDENT. RU-106 4.272E-02 5.094E-01 5.097E-01 NOT IDENT. AG-108M 5.362E-03 3.041E-02 3.050E-02 NOT IDENT. AG-llOM -5.692E-02 1.087E-01 l .117E-01 NOT IDENT. SN-113 -8.789E-03 2.399E-01 2.399E-01 NOT IDENT. CD-115 6.370E+38 4.235E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -9.312E+04 1. 077E+05 1.156E+05 SHORT HLIF TE-123M -2.612E-02 1. 380E-01 l.385E-01 NOT IDENT. SB-124 -5.218E-01 1.617E+OO 1.634E+OO NOT IDENT. SB-125 -2.784E-02 l.163E-01 l.169E-01 NOT IDENT. TE-125M -1. 675E+Ol 2.421E+02 2.422E+02 NOT IDENT. I-126 -l.208E+05 1.258E+06 l.259E+06 SHORT HLIF SB-126 9.679E+05 *1.238E+06 1.313E+06 SHORT HLIF SB-127 -2.878E+21 2.808E+22 O.OOOE+OO SHORT HLIF I-131 l.067E+09 6.007E+09 6.027E+09 SHORT HLIF I-132 l.000E+41 1.858E+42 O.OOOE+OO SHORT HLIF TE-132 2.030E+26 4.553E+26 O.OOOE+OO SHORT HLIF BA-133 -6 .117E-03 4.514E-02 4.523E-02 FAIL ABUN I-133 1.000E+41 1.213E+42 O.OOOE+OO SHORT HLIF CS-134 4.308E-02 4.068E-02 4.507E-02 NOT IDENT. CS-135 5.576E-02 1.595E-01 1.615E-01 NOT IDENT. I-135 1*. OOOE+41 6.846E+41 0.000E+OO SHORT HLIF CS-136 3.302E+05 5.122E+05 5.334E+05 SHORT HLIF CE-139 1.499E-03 1.113E-01 l .113E-01 NOT IDENT. BA-140 2.603E+05 1.592E+06 1.596E+06 SHORT HLIF LA-140 -2.351E+05 6.106E+05 6.197E+05 SHORT HLIF CE-141 -5.610E+OO 2.577E+Ol 2.589E+Ol. NOT IDENT. CE*-143 -1.000E+41 2.461E+41 O.OOOE+OO SHORT HLIF CE-144 -2.612E-01 3.358E-01 3.558E-01 NOT IDENT. PM-144 -1.271E-02 5.818E-02 5.846E-02 NOT IDENT. PR-144 -1.122E+OO 5.053E+OO 5.078E+OO NOT IDENT. PM-146 1.233E-02 4.553E-02 4.587E-02 FAIL ABUN ND-147 l.143E+07 3.648E+07 3.685E+07 SHORT HLIF PM-147 5.635E+02 7. 631E+02 8.042E+02 NOT PM-149 -2.023E+40 6.468E+40 O.OOOE+OO SHORT HLIF EU-150 2.322E-02 2.673E-02 2.870E-02 FAIL ABUN EU-152 -4.215E-02 1. 073E-01 l.090E-01 NOT IDENT. GD-153 -5.847E-03 l.593E-01 l.593E-01 NOT IDENT. EU-154 -6.285E-02 1. 417E-01 l.445E-01 NOT IDENT. EU-155 7.073E-02 8.866E-02 9.422E-02 FAIL ABUN TB-160 3.949E-01 1. 749E+OO 1. 758E+OO FAIL ABUN H0-166M 2.629E-03 6.136E-02 6.137E-02 FAIL ABUN TM-171 -4.548E+OO 5.537E+OO 5.905E+OO NOT IDENT. HF-172 7.144E-05 2.174E-01 2.174E-01 FAIL ABUN LU-172 4.815E-02 9.440E-02 9.686E-02 FAIL ABUN LU-176 3.198E-03 2.298E-02 2.302E-02 FAIL ABUN Page 4094 of 5809 HF-181 3.504E-02 3.953E+OO 3.953E+OO NOT IDENT. TA-182 3.794E-01 1.171E+OO 1.183E+OO FAIL ABUN RE-183 4.452E-01 1.072E+OO 1.091E+OO NOT IDENT. RE-184 -2.397E+OO 4.091E+Ol 4.092Et01 NOT IDENT. W-188 3.965E+Ol 1.146E+02 l .160E+02 FAIL ABUN IR-192 1.141E-01 4.361E-01 4.391E-01 FAIL ABUN HG-203 2.914E+OO 2.457E+OO 2.786E+OO NOT IDENT. BI-207 -3.388E-02 6.275E-02 6.458E-02 FAIL ABUN PB-211 1.721E-01 7.212E-01 7.253E-01 NOT IDENT. BI-212 1.791E+OO 9.983E-01 1.284E+OO FAIL ABUN RN-219' 2.931E-01 3.642E-01 3.875E-01 FAIL ABUN RA-223 1.282E-01 6.580E-01 6.605E-01 FAIL ABUN AC-227 l.8i9E-03 2.360E-01 2.360E-01 FAIL ABUN TH-227 l.819E-03 2.360E-01 2.360E-01 FAIL ABUN AC-228 8.719E-01 3.817E-01 5.479E-01 FAIL ABUN RA-228 8.719E-01 3.817E-01 5.479E-01 FAIL ABUN TH-231 1.282E-01 6.580E-01 6."605E-01 FAIL ABUN TH-232 8.719E-01 3.817E-01 5.479E-01 FAIL ABUN PA-233 5.092E-02 6.027E-02 6.449E-02 FAIL ABUN PA-234 2.470E-02 2.592E-01 2.595E-01 NOT IDENT. PA-234M 1.659E-01 5.139E+00 5.140E+OO NOT IDENT. NP-237 5.092E-02 6.027E-02 6.449E-02 FAIL ABUN NP-238 -1. OOOE+41 l.152E+41 O.OOOE+OO SHORT HLIF NP-239 2.606E-02 2.200E-01 2.203E-01 FAIL ABUN PU-239 -9.135E+Ol 2. 878E+o2 2.907E+02 NOT IDENT. AM-241 3.959E-02 5.620E-02 5.896E-02 NOT IDENT. CM-243 -1.313E-02 8.150E-02 8 .1 72E-02 FAIL ABUN BK-247 -6.742E-02 7.900E-02 8.464E.:...02 FAIL ABUN CM-247 -3.867E-04 3.580E-02 3.580°E-02 FAIL ABUN CF-249 4.362E-03 3.546E-02 3. 551E-02 NOT IDENT. CF-251 -7.098E-02 1.164E-01 1.207E-01 NOT IDENT. Page 4095 of 5809
GEL Laboratories LLC *
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GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.2546 87.09 96.8336 136.47 82.2510 45.60 85.4408 87.57 96.8968 140.51 0.0000 46.54 85.6012 88.03 96. 9570 143.76 74.8373 49.72 0.0000 88.34 96.9977 144.24 73.9818 51. 35 104.1492 88.47 97.0142 145.44 90.1319 51. 87 130.3128 89. 96 97.2077 152.43 67.3836 52.39 113.8370 1093.63 97.2956 153.25 0.0000 52.97 87.8431 91.11 0.0000 323.87 66.1473 53.44 83.1661 92.59 97.5452 156.02 0.0000 54.07 88.0192 93.35 97.6414 158.56 0.0000 57.36 0.0000 94.56 69.5523 159.00 63.7328 57.53 113.6957 94.65 69.5603 162.33 68.0092 57.98 98.2136 94.67 69.5620 162.66 0.0000 59.27 99.2329 94.87 83. 4960 163.33 78.0547 59.32 105.6440 97.43 93.9227 165.86 68.2274 59.54 92.8738 98.43 76.2497 176.31 58.7611 60. 96 107.5443 98.44 76.2506 176.60 0.0000 61.17 107.5821 99.53 79.7481 177.52 72. 6087 62.93 115.9506 100 .11 83.2019 181.07 0.0000 63.29 116. 0193 102.03 98. 7181 181.52 58.1018 63.58 116.0750 103.18 88.6302 184.41 55.4706 64.28 116.2081 103.37 83.5364 143.76 62.0103 66.73 140.9741 105.21 68.3451 193.51 65.2049 67.24 129.7371 105.31 68. 3.537 197.03 59.7865 125.81 116.8447 106.12 76.1172 198.01 71.0521 67.75 116. 8572 106.47 90.6948 201. 83 65.6428 69.67 122.0940 109.28 78.9792 203.43 58.2146 70.83 122.3129 111. 00 89.4607 205.31 55.4793 72. 81 135. 7691 111.76 0.0000 210.85 62.3295 72. 87 117.7866 114. 06 77.6921 215.65 62.5585 74.66 108.2618 116. 30 0.0000 222 .11 45.7188 74. 82' 108.2873 116.74 78.7951 227.09 44.9312 74.97 108. 3115 119.76 84.2751 227.38 50.6779 77 .11 108.6539 121.12 67.8695 228.16 0.0000 78.74 117.16H 121. 22 67.8771 228.18 41.1401 79.69 127.2367 121. 78 74.8852 116.74 41.1401 80.12 119.0479 122.06 76.6500 235.69 50.5026 80.19 0.0000 122.92 82.8254 235. 96 50.5122 80.57 96.7883 123.07 78.4790 238.63 76.6355 81. 00 99.3311 265.00 79.4038 238.98 0.0000 81. 07 99.3408 125.81 76.0887 240.99 "81.1084 81. 75 102.7506 127.23 85.8392 242.00 52.1785 83.79 118. 0025 127:91 84.1492 244.70 49.3730 84.00 91.0217 129.30 82.5168 252.40 0.0000 85.43 91.2010 131.20 70.3687 252.80 45.7555 86.55 96.7628 133.02 89.0089 254.15 0.0000 86.79 96.7941 133.52 82.8830 256.23 38.0558 86.94 96.8142 136.00 74.2554 260.90 0.0000 Page 4096 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.7474 355.39 0.0000 584.27 18. 3724 264.80 45.6353 356.01 31. 0870 595.83 0.0000 265.00 45.6410 364.49 0.0000 427.87 20.7964 268.22 42.7867 366.42 0.0000 602.52 0.0000 269.46 36.9156 372. 51 38.6787 604.72 13.8857 270.03 36.9293 375.05 '30.3558 607.14 20.8469 271.23 36.9583 377.52 36.6833 609.32 27.8184 273.65 0.0000 356.01 23.1337 610.33 27.8291 276.40 25.2157 388.16 24.2382 614.28 12.1927 277.37 25.2313 388.63 0.0000 618.01 27.9072 277.60 25.2349 391. 69 29.5603 620.36 10.4744 278.00 25.2416 264.66 24.3912 621. 93 15.1381 279.20 25.2608 401.81 19.0997 630.19 0.0000 279.54 25.2665 402.40 28.6578 631.29 19.2789 279.70 25.2691' 404.85 29.7557 633.25 24.5538 280.46 25.2811 410.95 33.0422 634.78 0.0000 283.69 22.3526 413.71 24.5484 635.95 11.4111 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 26.8522 423.72 0.0000 645.85 11. 4516 285.90 0.0000 427.09 32.2266 657.76 18.3993 287.50 33.8582 427.87 32.2382 657.90 0.0000 290.67 34. 7235 433.94 26.9424 661.66 20.3728 293.27 0.0000 439.40 28.0921 664.57 0.0000 351. 93 31.5192 453. 88 ' 17.9472 666.33 0.0000 295. 96 31.5333 463.37 27.3097 666.50 0.0000 879.38 36.0959 468.07 19.7043 667.71 0.0000 299.98 28.6003 473.00 0.0000 677.62 20.4851 300.09 28.6021 475.06 18.6674 685.70 0.0000 300.13 28.6032 476.78 15.3848 695.00 0.0000 301.36 36.1567 477.60 26.3833 696.49 19.7200 302.85 24.1265 482.18 16.5228 696. 51 19.7200 256.23 37.7350 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6219 306.78 31. 2371 497.08 24.9442 697.49 17.9333 308.46 34.2947 505.52 18.3581 702.65 21.5574 311. 90 29.3109 507.63 0.0000 706.68 18.8877 316.51 28.3771 511. 00 17.8428 7-11.68 18.0182 319.41 0.0000 514.00 17.8652 720.70 0.0000 320.08 0.0000 514.00 17.8652 721. 93 0.0000 321. 04 29.4685 520.40 16.7932 722.78 17.3602 323.87 33.5881 520.69 0.0000 722. 91 17.3613 325.23 42.7819 522.65 0.0000 723. 31 20.2576 328.76 0.0000 527.90 0.0000 724 .19 17.3684 333.37 27.6306 528.26 16.8475 727. 33 13.0395 333.97 20.4740 529.59 19.1042 733.00 3.6288 334.37 33.7896 529.87 0.0000 735.93 11. 6230 338.28 31.8117 531. 02 0.0000 333.97 11.6289 338.32 31.8123 537.26 0.0000 739.50 0.0000 311. 90 32.3645 546.56 0.0000 747.24 17.3156 340.48 32.3645 552.55 23.8190 748.06 18.2312 340.55 0.0000 563.25 14.8070 752.31 19.1690 344.28 42.0078 569.33 20.5503 753.82 0.0000 345.93 36.0695 946.00 23.9771 756.73 17.3678 351.06 27.9031 569.70 2'3. 97 8 8 756.80 17.3678 351. 93 24.8145 583.19 18.3646 884.68 17.4066 Page 4097 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.4171 1274.44 12. 7183 1620.50 3.3481 766.42 16.5037 1001. 03 13.7133 1621.92 4.4653 766.84 16.5059 1002.74 11.7594 1678.03 0.0000 772. 60 0.0000 1004.73 9.8044 1690.97 2. 7114 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.5752 778. 90 19.3286 1028.54 0.0000 1063.66 3.0529 783.70 0.0000 1037.84 10.8751 1771. 35 10.0767 785.37 17.7070 1038.76 0.0000 1791.20 0.0000 792.07 15. 7103 631.29 12.6820 1808.65 0.9216 794.95 9.2496 1048.07 0.0000 1810.72 0.0000 795.86 4.6260 1049.04 12.6898 1836.06 0.0000 810.06 19.5125 1050.41 12.6945 810.29 19.5138 1063.66 18.9049 344.28 17.6565 1077.00 0.0000 810.76 14.8701 1077.34 6.9880 815.77 0.0000 1085.87 12.0037 1048.07 0.0000 1093.63 11. 0242 832.01 18.7048 1099.45 14.0504 834.85 14.0405 1112. 07 7.0461 835.71 14.9800 1112. 84 9.2048 836.80 0.0000 1115. 54 8. 0596 846.75 0.0000 1120.29 8.0684 846.77 12.0227 1120. 55 8.0688 856.80 0.0000 1221.41 8.0703 860.56 7.5442 1129. 67 8.0859 871. 09 17.9714 1131. 51 0.0000 873.19 15.1426 1147.95 0.0000 875.33 0.0000 1173.23 13.2722 879.38 8.5328 1177.95 15.3305 880.51 16.1222 1189.05 .6.1476 883.24 8. 541.9 1204.77 11. 3102 884.68 13.2929 1221.41 13.4158 889.28 11. 4086 1231. 02 11. 37 53 894.76 7.6174 1235.36 0.0000 898.04 16.7734 1238.28 8.2861 900. 72 15.2598 1260.41 0.0000 903.28 15.2705 1271.87 4.1731 911.20 13.3912 1274.44 13.5697 912.08 13.3942 1274.54 15.6583 923.98 0.0000 1291.59 8.3813 926.50 9.6051 1298.22 0.0000 929 .11 20.1848 1312 .11 0.0000 937.49 18:3036 1332.49 5.2829 944 .13 0.0000 1362.66 0.0000 946.00 8.6899 1365.19 2.1273 949.00 11.5957 1368.63 0.0000 667.71 0.0000 1384.29 4. 2710 962. 31 15.5156 1408.01 5.3638 964. 08 13.9707 1457.56 0.0000 966 .17 23.2969 1460.82 3.2514 911.20 21.3716 1489.16 6.5380 968. 97 21. 3'716 1505.03 6.5574 983.53 0.0000 1584.12 3.3265 984.45 0.0000 1596.21 0.0000 Page 4098 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:07:20.79 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 7-DEC-2015 13:11:00. Acquisition date : 3-0CT-2016 07:04:59. Sample ID G405235052 Sample quantity 1.65245E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.77 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 2 2 0 6 6 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 4 4 0 Energy 74.84 77.17*' 87.28 89.95 92.79* 143.99 183.84* 185.83* 227.79 238.68* 241.86 255.61 270.60 295.22 300.90 328.45 339.15 351.95* 372.61 511. 08* 517.16 583.31* 609.48* 661.81 676.17 728. 23 755.54 760.26 768.70 873.29 911.29* 964.88 969.04* 1033.95 Page 4099 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 80 136 49 44 63 28 13 38 17 329 87 . 10 32 125 17 48 88 231 25 38 24 74 134 . 50 10 15 16 15 22 17 71 27 36 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 118 109 140 78 116 88 47 74 78 79 80 66 40 55 42 51 84 97 49 43 22 51 40 19 25 39 13 9 6 21 18 8 11 14 0.93 1. 06 1. 47 1. 04 1. 21 1. 00 1. 51 1. 39 1. 51 1. 20 1. 54 1. 29 1. 30 1. 20 0.98 1.10 1. 24 1. 33 4.02 2.59 1. 39 1. 26 1. 82 1. 00 0.53 0.67 0.86 0.52 2.08 4.16 1. 68 2.64 1. 77 0.82 150.13 154.81 175.02 180.38 186.05 288.49 .368.22 372.21 456.15 477.95 484.31 511. 82 541.82 591.09 602.44 657.58 678.98 704.59 745.94 1023.01 1035.19 1167.56 1219.93 1324.65 1353.40 1457.57 1512.22 1521.68 1538.58 1747.89 1823.94 1931. 20 1939.53 2069.46 143 143 172 178 178 285 366 366 451 473 473 507 539 585 599 653 673 697 739 1015 1030 1162 1214 1321 1346 1449 1505 1516 1535 1737 1819 1925 1925 2062 18 2.23E-02 23.8 8.91E-01 18 3.78E-02 15.2 7 1. 35E-02 43. 0 15 1.22E-02 30.6 1.63E+OO 15 1.76E-02 33.0 7 7.76E-03 59.l 17 3.67E-03 85.7 1.34E+OO 17 1.06E-02 47.0 8 4.68E-03 94.9 28 9.14E-02 7.1 9.25E-01 28 2.42E-02 22.9 8 2.87E-03139.5 6 8.93E-03 35.8 11 3.47E-02 14.6 7 4.81E-03 68.8 11 1. 34E-02 32. 3 13 2.45E-02 24.5 16 6.41E-02 11.7 14 6.94E-03 62.7 16 1.06E-02 47.9 9 6. 55E-03 41. 7 13 2.04E-02 23.3 11 3.72E-02 12.2 8 1. 38E-02 21.1 13 2.75E-03110.4 12 4.26E-03 85.3 11 4.36E-03 52.1 12 4.09E-03 48.6 8 6.03E-03 29.1 18 4.71E-03 69.6 10 1.97E-02 16.5 19 7.36E-03 31.6 6.84E-01 19 9.96E-03 23.4 11 2.57E-03 84.4 Peak Search Report (continued) Page : 2 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1120.27 57 8 1. 45 2242.23 2235 15 1.57E-02 17.0 36 0 1238.15 40 0 0.82 2478.18 2471 16 l. llE-02 15.8 37 0 1277.10 11 1 0.84 2556.16 2553 6 2.93E-03 35.8 38 0 1308. 72 11 4 1. 33 2619.44 2614 9 2. 96E-03 47.0 39 0 1343.50 13 0 1. 00 2689.08 2683 12 3.61E-03 27*. 7 40 0 1460.79* 351 7 2.14 2923.88 2917 14 9.76E-02 5.6 41 0 1765.23 19 7 0.91 3533.38 3525 12 5.31E-03 34.7 Flag: "*" = Peak area was modified by background subtraction Page 4100 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:07:22 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 13:11:00 G405235052 Acquisition date : Sample quantity *: 3-0CT-2016 07:04:59 165.24 GRAM Sample type* Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4101 of5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 87.09 87.09 87.09 74. 82 . 74.82 74.82 351. 93 Sample geometry : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 86.94 87.57 '88. 03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.77 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page *: 2 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.030E+00 1.416E+Ol 1.416E+Ol 11. 24 OK CD-109 88.03 3.70* 4.461E+OO 9.321E-01 1.465E+00 168.44 OK SN-.126 64.28 9.60 2.161E+OO Line Not Found Absent 86.94 8.90 4.461E+OO 3.875E-01 3.875E-01 168.44 OK 87.57 37.00* 4.461E+OO 9.321E-02 9.321E-02 168.44 OK BA-137M 661. 66 89.90* 1. 965E+OO 1.373E-01 1. 399E-01 42.18 OK CS-137 661.66 85.10* 1. 965E+00 l.450E-01 1.478E-01 42.18 OK CE-141 145.44 48.29* 5.917E+OO 3.792E-02 2. 311E+Ol 181.44 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent* 583.19 85.00* 2.178E+OO l.978E-01 1.978E-01 46.53 OK 860.56 12.50 1. 592E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.135E+OO Line Not Found Absent 351. 06 12.92* 3.336E+OO 2.268E-01 2.268E-01 442.79 OK PB-212 74.82 10.28 3.342E+OO 9.186E-01 9.186E-01 77.05 OK 77 .11 17.10 3.578E+OO 1.376E+OO 1. 37 6E+OO 30.45 OK 238.63 43.60* 4.585E+OO 9. 072E-01 9. 072E-01 14.24 OK 300.09 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 OK BI-214 609.32 45.49* 2. lOlE+OO 6.925E-01 6.928E-01 24.32 OK 1120.29 14.92 l.288E+OO l.348E+00 1.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 3.578E+00 2.426E+00 2 ..427E+OO 30.45 OK 87.09 3.41 4.447E+OO Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.870E+OO 9.441E-01 9.444E-01 29.12 OK 351. 93 35.60* 3.336E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2. lOlE+OO 6.925E-01 6.928E-01 24.32 OK 1120.29 14.92 l.288E+OO 1.348E+OO l.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 OK RA-224 240.99 4.10* 4.540E+OO 9.091E-01 9.091E-01 140.33 OK RA-226 609.32 45.49* 2.lOlE+OO 6.925E-01 6.928E-01 24.32 OK 1120.29 14.92 l.288E+OO 1.348E+OO l.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.443E+OO 1. 207E+OO 1.207E+OO 48.95 OK 794.95 4.25 1. 696E+00 Line Not Found Absent 835. 71 1. 61 l.630E+00 Line Not Found Absent 911.20 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 OK 968. 97 15.80 1.448E+OO 7.324E-01 7.324E-01 46. 79 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.443E+OO 1.207E+OO 1.207E+OO 48.95 OK 794.95 4.25 1.696E+OO Line Not Found Absent 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1. 521E+OO 8.518E-01 8.518E-01 33.07 OK 968. 97 15.80 l.448E+OO 7.324E-01 7.324E-01 46.79 OK TH-228 74.82 10.28 3.342E+OO 9.186E-01 9.186E-01 77.05 OK 77 .11 17.10 3.578E+OO 1.376E+OO 1.376E+OO 30.45 OK 238.63 43.60* 4.585E+OO 9.072E-01 9. 072E-01 14.24 OK 300.09 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 OK Page 4102of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status TH-230 609.32 45.49* 2.101E+OO 6.925E-01 6.925E-01 24.32 OK 1120.29 14.92 1.288E+OO l.348E+OO l.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6. 211E-01 6.211E-01 69.40 OK PA-231 283.69 1. 70 4.000E+OO Line Not Found Absent 301.36 5.35* 3.810E+OO 4.565E-01 4.565E-01 137.50 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent .338.32 11. 27 3.443E+OO l.207E+OO 1.207E+OO 48.95 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911. 20 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 OK 968. 97 15.80 1.448E+OO 7.324E-01 7.324E-01 46.79 OK U-234 609.32 45.49* 2.101E+OO 6.925E-01 6.925E-01 24.32 OK 1120.29 14.92 1.288E+OO 1.348E+OO 1.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6.211E-01 6.211E-01 69.40 OK U-235 89. 96 , 3.47 4.655E+OO 1.664E+OO 1.664E+OO 61. 21 OK 93.35 5.60 4.842E+OO 1.422E+OO 1.422E+OO 66.02 OK 143.76 10. 96* 5.918E+OO Line Not Found <<INT Reject 163.33 5.08 5.731E+OO Line Not Found Absent 185.72 57. 20* 5.405E+OO 7.020E-02 7.020E-02 94.05 OK 205.31 5.01 5.095E+OO Line Not Found Abserit AM-243 43.53 5.90 1. 573E-01 Line Not Found Absent 74.66 67.20* 3.342E+OO 1.405E-01 l.405E-01 77.05 OK ANH-511 511. 00 100.00* 2.430E+OO 7.973E-02 7.973E-02 95.89 OK Flag: "*" = Keyline Page 4103 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:07:24.32 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l *
Acquisition date 3-0CT-2016 07:04:59 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
Sample date 7-DEC-2015 13:11:00 Analyst initials: MXRl *
Sample ID G405235052 Sample Quantity 1.6524E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.416E+Ol 1.560E+OO CD-109 1.465E+OO 2.418E+00 SN-126 9.321E-02 l.539E-01 BA-137M 1.399E-01 5.784E-02. CS-137 1.478E-01 6.llOE-02 CE-141 2.311E+Ol 4. llOE+Ol TL-208 l.978E-01 9.018E-02 BI-211 2.268E-01 9.842E-01 PB-212 9. 072E-01 1.266E-01 BI-214 6.928E-01 1. 651E-01 PB-214 1.027E+OO 2.346E-01 RN-222 6.928E-01 1. 651E-01 RA-224 9.091E-01 1.250E+OO RA-226 6.928E-01 1. 651E-01 AC-228 8.518E-01 2.761E-01 RA-228 8.518E-01 2.761E-01 'l'H-228 9. 072E-01 1.266E-01 TH-230 6.925E-01 l.651E-01 PA-231 4.565E-01 6 .151E-Ol TH-232 8.518E-01 2. 761E-01 U-234 6.925E-01 1.651E-01 U-235 2.505E-01 2.900E-01 AM-243 l.405E-01 1.061E-01 ANH-511 7.973E-02 7.492E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 sc.:..46 V-48 Page 4104of5809 Key-Line Activity (pCi/GRAM 5.078E+OO -4.709E-04 O.OOOE+OO 2.565E-03 -1.242E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.179E+Ol 4.743E-02 1. 960E+41 3.326E-02 3.861E-01 l.297E+04 MDA (pCi/GRAM 5.992E-01 1.864E+OO l.417E-01 5. 965E-02 6. 301E-02 4.062E+Ol 6.347E-02 3.315E-01 8.443E-02 1.308E-01 3.187E-01 l.308E-01 9.052E-01 1.308E-01 2.468E-01 2.468E-01 8.443E-02 1.307E-01 6.774E-01 2.468E-01 1.307E-01 3.374E-01 9.419E-02 4.675E-02 MDA (pCi/GRAM 2.446E+Ol 8.435E-02 O.OOOE+OO 7.052E-02 7.500E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.780E+02 O.OOOE+OO SHORT HLIF MN-54 -1. 8 68E-02 6.175E-02 1.118E-01 NOT IDENT. C0-56 -2.089E-01 4.671E-01 8.216E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 2.319E-02 4.537E-02 9.129E-02 NOT IDENT. C0-58 -6.565E-02 6.036E-01 l.133E+OO NOT IDENT. FE-59 -1.102E+OO 6. 391E+OO 1.258E+Ol NOT IDENT. C0-60 6.926E-03 3.033E-02 6.734E-02 NOT IDENT. ZN-65 -l.140E-Ol 1. 891E-01 2.862E-01 NOT IDENT. GE-68 -l.309E-02 2.177E+OO 4.422E+OO NOT IDENT. AS-73 -1.359E+OO 1. 371E+Ol 2.782E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.435E+03 O.OOOE+OO SHORT HLIF SE-75 -2. 272E-02 1.935E-01 3.516E-01 NOT IDENT. BR-77 0.000E+OO 2.976E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.557E+02 O.OOOE+OO SHORT HLIF RB-83 -5.029E-Ol 6.740E-01 1.019E+OO NOT IDENT. KR-85 8.711E+OO 5.855E+OO 1.240E+Ol NOT IDENT. SR-85 9.287E-01 6.245E-01 1.323E+OO NOT IDENT. RB-86 O.OOOE+OO 2.684E+04 O.OOOE+OO SHORT HLIF Y-88 3.866E-03 1.022E-01 2.863E-01 NOT IDENT. Y-91 -2.922E+Ol 5.285E+02 l.040E+03 NOT IDENT. NB-94 9.007E-03 3.567E-02 6.959E-02 NOT IDENT. NB-95 7.526E-01 6.721E-01 1.424E+OO NOT IDENT. NB-95M -5.399E-01 2.510E+OO 4;127E+OO NOT IDENT. ZR-95 2.042E+OO 2.086E+OO 2.693E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 736E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.173E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.063E-02 3.034E-02 5.514E-02 NOT IDENT. RH-102 -6.334E-03 4.881E-02 9.485E-02 NOT IDENT. RU-103 2.050E+OO 5.283E+OO 1.098E+Ol FAIL ABUN RH-106 -2*. 491E-01 4.662E-01 8.376E-01 NOT IDENT. RU-106 -2.491E-01 4.662E-01 8.376E-01 NOT IDENT. AG-108M 1.034E-05 2.625E-02 5.205E-02 NOT IDENT. AG-llOM -7.645E-02 9.590E-02 1.727E-01 FAIL ABUN SN-113 2.238E-01 2.040E-01 4.546E-01 NOT IDENT. CD-115 O.OOOE+OO 3.639E+39 O.OOOE+OO SHORT HLIF SN-:ll 7M O.ObOE+OO 9.785E+04 O.OOOE+OO SHORT HLIF TE-123M -4.514E-02 1. 313E-01 2.409E-01 NOT IDENT. SB-124 -6. 2 61E-02 1.386E+OO 3.156E+OO NOT IDENT. SB-125 -3.326E-02 9.688E-02 1.847E-01 NOT IDENT. TE-125M 2.643E+Ol 2.573E+02 5.068E+02 NOT IDENT. I-126 0.000E+OO . 9.732E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.238E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.248E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.380E+09 O.OOOE+OO SHORT HLIF I-132 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF TE:..132 O.OOOE+OO 8.165E+26 O.OOOE+OO SHORT HLIF BA-133 l.889E-02 3.694E-02 7.206E-02 NOT IDENT. I-133 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-l34 6.979E-03 4.658E-02 9 .184E,-02 NOT IDENT. CS-135 8.429E-03 1. 271E-01 2.356E-01 NOT IDENT. I-135 O.OOOE+OO l.494E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.098E+05 O.OOOE+OO SHORT HLIF CE-139 -3.729E-03 l.039E-01 l.957E-01 NOT IDENT. BA-140 O.OOOE+OO 1.322E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.814E+05 0.000E+OO SHORT HLIF CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -8.229E-02 3.166E-01 5. 963E-01 NOT IDENT. PM-144 -2.043E-02 5.660E-02 l.027E-01 NOT IDENT. PR-144 -1. 746E+OO 4.924E+OO 8.941E+OO NOT IDENT. PM-146 -9. 611E-03 3. 967E-02 7.647E-02 NOT IDENT. ND-147 0.000E+OO 3.374E+07 O.OOOE+OO SHORT HLIF PM-147 3.370E+02 7.818E+02 1. 566E+03 NOT IDENT. PM-149 O.OOOE+OO 5.844E+40 O.OOOE+OO SHORT HLIF EU-150 -1.239E-02 2.869E-02 4.416E-02 FAIL ABUN EU-152 -2.530E-02 8.774E-02 l.527E-01 FAIL ABUN GD-153 5.218E-02 l.667E-01 3.151E-01 NOT IDENT. EU-154 -3.556E-03 l.157E-01 2.048E-01 FAIL ABUN EU-155 5.619E-02 1.017E-01 2.077E-01 FAIL ABUN TB-160 6.498E-01 2. ll 7E+OO 4.179E+OO FAIL ABUN H0-166M -2.757E-03 5.332E-02 1.024E-01 FAIL ABUN TM-171 -2.908E+OO . 3. 255E+Ol 6.632E+Ol NOT IDENT. HF-172 l.615E-01 2.086E-01 4.286E-01 NOT IDENT. LU-172 -3.505E-02 6. 371E-02 1. l 77E-01 FAIL ABUN LU-176 1.238E-02 2.034E-02 4.360E-02 FAIL ABUN HF-181 -5.949E-01 3.582E+OO 7.025E+OO NOT IDENT. Page 4105 of 5809 TA-182 -9.336E-01 1.067E+OO 1.808E+OO FAIL ABUN RE-183 ...:9.267E-01 3.633E+OO 7.315E+OO NOT IDENT. RE-184 1.339E+Ol 3.00SE+Ol 6.483E+Ol NOT IDENT. W-188 -1.392E+02 l.004E+02 1.479E+02 FAIL ABUN IR-192 -1. 7 63E-01 3. 991E-01 7. 722E-01 FAIL ABUN HG-203 4.008E-01 2.127E+OO 4.375E+OO NOT IDENT. BI-207 -4.335E-02 4.505E-02 7.599E-02 FAIL ABUN PB-210 1.292E+OO 6.720E+OO 1.422E+Ol NOT IDENT. PB-211 -4.806E-01 6.684E-01 1.221E+OO NOT IDENT. BI-212 6.115E-01 1.023E+OO l.225E+OO FAIL ABUN RN-219 2.462E-01 3.367E-01 7. 241E-01 FAIL ABUN RA-223 -5.160E-02 5.894E-01 l.054E+OO FAIL ABUN AC-227 1.368E-01 3.743E-01 3.983E-01 FAIL ABUN TH-227 l.368E-01 3.743E-01 3.983E-01 FAIL ABUN TH-229 l.215E-01 3.985E-01 7.721E-01 FAIL ABUN TH-231 -5.160E-02 5.894E-01 1.054E+OO FAIL ABUN PA-233 2.694E-02 5.046E-02 l.073E-01 FAIL ABUN PA-234 -l.333E-01 2.619E-01 4.925E-01 NOT IDENT. PA-234M 2.979E+OO 3.777E+00 . 8.571E+00 NOT IDENT. TH-234 2.685E-01 1.471E+OO 3.000E+OO FAIL ABUN NP-237 2.694E-02 5.046E-02 1.073E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF U-238 2.685E-01 1.471E+OO 3.000E+OO FAIL ABUN NP-239 -1. 431E-02 2.103E-01 4.082E-01 FAIL ABUN PU-239 2 .114E+02 2.728E+02 5.600E+02 NOT IDENT. AM-241 6.150E-02 1.657E-01 3.488E-01 NOT IDENT. CM-243 -4.899E-02 9.466E-02 l.777E-01 FAIL ABUN BK-247 -3'. 478E-02 6.913E-02 l.195E-01 . NOT IDENT. CM-247 1. 793E-02 3.227E-02 6.780E-02 NOT IDENT. CF-249 -6.726E-03 3.109E-02 6.lOlE-02 NOT IDENT. CF-251 -1.197E-02 1.045E-01 l.949E-01 FAIL ABUN Page 4106of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:07:21.56 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40* 1460.82 342 10.66* 1.030E+OO l.416E+Ol l.416E+Ol 11. 24 CD-109 88.03 65 3.70* 4.461E+OO l.802E+OO 2.832E+OO 85.98 SN-126 64.28 ------9.60 2 .161E+OO ------Line Not Found ------86.94 65 8.90 4.461E+OO 7.492E-01 7.492E-01 85.98 87.57 65 37.00* 4.461E+OO 1.802E-01 1.802E-01 85.98 BA-137M 661.66 53 89.90* 1. 965E+OO 1.373E-01 1.399E-01 42 .18* CS-137 661.66 53 85.10* 1. 965E+OO l.450E-01 l.478E-01 42.18 CE-141 145.44 36 48.29* 5.917E+OO 5.686E-02 3.466E+Ol 118 .12 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 81 85.00* 2.178E+OO 1.978E-01 l.978E-01 46.53 860.56 ------12.50 1.592E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351. 06 268 12.92* 3.336E+OO 2.828E+OO 2.828E+OO 23.31 .PB-212 74.82 110 10.28 3.342E+OO 1. 451E+OO l.451E+00 47.59 77 .11 185 17.10 3.578E+OO l.376E+OO l.376E+OO 30.45 238.63 399 43.60* 4.585E+OO 9.072E-01 9. 072E-01 14.24 300:09 20 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 BI-214 609.32 146 45.49* 2 .101E+OO 6.925E-01 6.928E-01 24.32 1120.29 57 14.92 1.288E+OO 1. 348E+OO l.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 PB-214 74.82 110 5.80 3.342E+OO 2.572E+OO 2.573E+OO 47.59 77 .11 185 9.70 3.578E+OO 2.426E+OO 2.427E+OO 30.45 87.09 65 3.41 4.461E+OO 1.956E+OO 1.956E+OO 85.98 242.00 106 7.25 4.540E+OO 1.458E+OO l.459E+OO 45.74 295.22 148 18.42 3.870E+OO 9.441E-01 9.444E-01 29.12 351. 93 268 35.60* 3.336E+OO 1. 026E+OO 1.027E+OO 23.31 RN-222 609.32 146 45.49* 2.101E+OO 6.925E-01 6.928E-01 24.32 1120.29 57 14.92 1. 288E+OO 1.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 RA-224 240.99 106 4.10* 4.540E+OO 2.579E+OO -2. 579E+OO 45.74 RA-226 609.32 146 45.49* 2. lOlE+OO 6.925E-01 6.928E-01 24.32 1120.29 57 14.92 1.288E+OO 1.348E+OO l.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 AC-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338 .*32 103 11. 27 3.443E+OO 1.207E+OO 1.207E+OO 48.95 794.95 ------4.25 1. 696E+OO ------Line Not Found ------835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 74 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 968.97 37 15.80 1.448E+OO 7.324E-01 7.324E-01 46. 79 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 103 11. 27 3.443E+OO 1.207E+OO . 1. 207E+OO 48.95 794.95 ------4.25 l.696E+OO ------Line Not Found ------835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 74 25.80* 1. 521E+OO 8.518E-01 8.518E-01 33.07 968. 97 37 15.80 1.448E+OO 7.324E-01 7.324E-01 46.79 TH-228 74.82 110 10.28 3.342E+OO 1.451E+OO 1. 451E+OO 47.59 77.11 185 17.10 3.578E+OO 1.376E+OO l.376E+OO 30.45 Page 4107of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 399 43.60* 4.585E+OO 9.072E-01 9. 072E-01 14.24 300.09 20 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 TH-230 609.32 146 45.49* 2.101E+OO 6.925E-01 6.925E-01 24.32 1120.29 57 14.92 1.288E+OO l.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.211E-01 69.40 PA-231 283.69 ------1. 70 4.000E+OO ------Line Not .Found ------301.36 20 5.35* 3.810E+OO 4.565E-01 4.565E-01 137.50 TH-232 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 103 11. 27 3.443E+OO l.207E+OO 1.207E+OO 48.95 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 74 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 968. 97 37 15.80 l.448E+00 7.324E-01 7.324E-01 46.79 U-234 609.32 146 45.49* 2.101E+OO 6.925E-01 6.925E-01 *, 24.32 1120.29 57 14.92 l.288E+00 1.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.211E-01 69.40 U-235 89. 96 59 3.47 *4.655E+OO 1.664E+OO 1.664E+OO 61. 21 93.35 85 5.60 4.842E+OO 1.422E+OO l.422E+00 66.02 143.76 36 10.96* 5.917E+OO 2.505E-01 2.50SE-01 *118.12 163.33 ------5.08 5.731E+OO ------Line Not Found ------185. 72 48 57.20 *5.405E+OO 7.020E-02 7.020E-02 94.05 205.31 ------5.01 . 5. 095E+OO ------Line Not Found ------AM-243 43.53 ------5.90 l.573E-01 ------Line Not Found ------74.66 110 67.20* 3.342E+OO 2.220E-01 2.220E-01 47.59 ANH-511 511. 00 43 100.00* 2.430E+OO 7.973E-02 7.973E-02 Flag: "*" Key line Page 4108of5809 Summary of Nuclide Activity Sample ID : G405235052 Acquisition date Page : 3 3-0CT-2016 07:04:59 Total number of lines in spectrum 41 Number of unidentified lines 7 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 32.51D l.41E+10Y 7.04E+08Y l.41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600. ODY l.41E+l0Y 1. 41E+l0.Y l.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y l.00E+09Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 610. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total*Activity Grand Total Activity Uncorrected pCi/GRAM l.416E+Ol 1. 802E+OO l.802E-01 1.373E-01 1.450E-01 5.686E-02 1.978E-01 2.828E+OO 9. 072E-01 6.925E-01 1. 026E+OO 6.925E-01 2.579E+OO 6.925E-01 8.518E-01 8.518E-01 9.072E-01 6.925E-01 4.565E-01 8.518E-01 6.925E-01 2.505E-01 2.220E-01 7.973E-02 3.195E+Ol 3.195E+Ol Decay Corr pCi/GRAM 1.416E+Ol 2.832E+OO 1.802E-01 1.399E-01 l.478E-01 3.466E+Ol 1.978E-01 2.828E+OO 9. 072E-01 6.928E-01 1.027E+OO 6.928E-01 2.579E+OO 6.928E-01 8.518E-01 8.518E-01 9. 072E-01 6.925E-01 4.565E-01 8.518E-01 6.925E-01 2.505E-01 2.220E-01 7.973E-02 6.759E+Ol 6.759E+Ol 82.93% Decay Corr 2-Sigma Error 0.159E+Ol 2.435E+OO 1.550E-01 0.590E-01 0.623E-01 4.094E+Ol 0.920E-01 0.659E+OO 1.292E-01 1.685E-01 0.239E+OO 1.685E-01 1.179E+OO l.685E-01 2.817E-01 2.817E-01 1.292E-01 l.684E-01 6.276E-01 2.817E-01 1.,684E-01 2.959E-01 1.057E-01 7.645E-02 "M" Manually accepted 2-Sigma %Error 11. 24 85.98 85.98 42.18 42.18 118 .12 46.53 23.31 14.24 24.32 23.31 24.32 45.74 24.32 33.07 33.07 14.24 24.32 137. 50 33.07 24.32 118 .12 47.59 95.89 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide spedific abn. limit Page 4109 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235052
Acquisition date : 3-0CT-2016 07:04:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 183.84 17 59 1. 51 368.22 366 17 3.67E-03 ***** 5.44E+00 T 0 227.79 21 95 1. 51 456.15 451 8 4.68E-03 **** 4.75E+OO T 0 255.61 12 79 1. 29 511. 82 507 8 2.87E-03 **** 4.35E+OO T 0 270.60 38 48 1. 30 541.82 539 6 8.93E-03 71. 7 4.16E+OO T 0 328.45 56 59 1.10 657.58 653 11 1.34E-02 64.6 3.54E+OO T 0 372.61 29 57 4.02 745.94 739 14 6.94E-03 **** 3.18E+OO T 0 517.16 26 25 1. 39 1035.19 1030 9 6.55E-03 83.4 2.41E+OO 0 676.17 11 27 0.53 1353.40 1346 13 2.75E-03 **** 1. 93E+OO T 0 728.23 16 41 0.67 1457.57 1449 12 4.26E-03 **** 1.82E+OO T 0 755.54 17 14 0.86 1512.22 1505 11 4.36:E-o3 **** 1.77E+OO T 0 760.26 16 10 0.52 1521.68 1516 12 4.09E-03 97.1 1. 76E+00 0 768.70 23 7 2.08 1538.58 1535 8 6.03E-03 58.3 1. 74E+OO 0 873.29 18 22 4.16 1747.89 1737 18 4.71E-03 **** 1.57E+OO T 4 964. 88 27 9 2.64 1931.20 1925 19 7.36E.,...03 63.1 1.45E+OO T 0 1033.95 9 14 0.82 2069.46 2062 11 2.57E-03 **** 1.37E+OO 0 1238.15 40 0 0.82 2478.18 2471 16 l. llE-02 31. 6 1.19E+OO T 0 1277.10 10 1 0.84 2556.16 2553 6 2.93E-03 71. 6 l.16E+OO 0 1308. 72 11 4 1. 33 2619.44 2614 9 2. 96E-03 94.0 l.13E+OO 0 1343.50 13 0 1. 00 2689.08 2683 12 3. 61E-03 55.5 1. llE+OO Flags: "T" = Tentatively associated Page 4110of5809 VAX/VMS Nuclide Identification Report_ Generated 03-0CT-2016 08:07:39.57 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l *
Acquisition date 3-0CT-2016 07:04:59 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
Sample date 7-DEC-2015 13:11:00 Nuclide Library : SOLID *
Sample ID : G405235052 Analyst initials: MXRl *
Batch Number : 1596252 Sample Quantity : 1.6524E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date . 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. 'File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3 * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211. PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230. PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.430E-01 8.690E-01 6.680E-02 2.616E-02 2.763E-02 1.890E+Ol 2.829E-02 l.508E-01 3.894E-02 5.873E-02 1.540E-01 5.873E-02 4.176E-01 5.873E-02 1.074E-01 l.074E-01 3.894E-02 5.871E-02 3.068E-01 l.074E-01 5.871E-02 1.585E-01 4.408E-02 2.074E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4111of5809 Le (pCi/GRAM 1.103E+Ol 3.546E-02 0.000E+OO 2.796E-02 3.261E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131
I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-*14 7 PM-147 PM-149 EU-1$0 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4112 of 5809 4.837E-02 3.526E-01 O.OOOE+OO 4.279E-02 4.946E-01 5.373E+OO 2.744E-02 l.206E-01 1.895E+OO l.295E+Ol O.OOOE+OO 1.609E-01 O.OOOE+OO O.OOOE+OO 4.426E-01 5.558E+OO 5.928E-01 O.OOOE+OO 9.051E-02 4.502E+02 3.140E-02 6.180E-01 1.916E+OO 1.175E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.561E-02 4.093E-02 4.916E+OO 3.644E-01 3.644E-01 2.347E-02 7.350E-02 2.074E-01 O.OOOE+OO O.OOOE+OO 1.126E-01 1; 118E+OO 8.296E-02 2.367E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.270E-02 O.OOOE+OO 4.017E-02 1.081E-01 O.OOOE+OO O.OOOE+OO 9.125E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.772E-01 4.534E-02 3.948E+OO 3.415E-02 0.000E+OO 7.332E+02 O.OOOE+OO 2. OllE-02 6.889E-02 l.468E-01 8.597E-02 9.729E-02 l.850E+00 4.485E-02 3.077E+Ol 2.008E-01 4.856E-02 l.995E-02 3.085E+OO 7.851E-01 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 *cF-249 CF-251 Page 4113 of 5809 3.384E+OO 2.852E+Ol 6.577E+Ol 3.499E-01 2.015E+OO 3.162E-02 6.601E+OO 5.528E-01 5.603E-01 3.293E-01 4.819E-01 *l.833E-01 l.833E-01 3.578E-01 4.819E-01 4.908E-02 2 .107E-01 . 3.756E+OO 1. 411E+OO 4.908E-02 O.OOOE+OO 1. 411E+OO l.895E-01 2.622E+02 1. 62 6E-01 8.278E-02 5.460E-02 3.089E-02 2.731E-02 9.055E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:07:45.84 *******************************************************************************
GEL Laboratories *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l *
Acquisition date 3-0CT-2016 07:04:59 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
Sample date 7-DEC-2015 13:11:00 Nuclide Library : SOLID *
Sample ID G405235052 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.6524E+02 GRAM *
Quantity Err(%) 1.2103E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.416E+Ol 1. 726E+OO 1. 726E+OO CD-109 1.465E+00 2.426E+OO 2.426E+OO SN-126 9. 321E-02 1.544E-01 l.544E-01 BA-137M 1. 399E-01 5.815E-02 5.815E-02 CS-137 1. 478E-01 6.143E-02 6.143E-02 CE-141 2.313E+Ol 4. lllE+Ol 4. lllE+Ol TL-208 1.978E-01 9.057E-02 9.057E-02 BI-211 2.268E-01 9.970E-01 9.970E-01 PB-212 9.072E-01 l.354E-01 1. 354E-01' BI-214 6.928E-01 l.678E-01 l.678E-01 PB-214 1. 027E+OO 2.384E-01 2.384E-01 RN-222 6.928E-01 1.678E-01 1.678E-01 RA-224 9.091E-01 l.256E+OO 1.256E+OO RA-226 6.928E-01 1.678E-01 l.678E-01 AC-228 8.518E-01 2.795E-01 2.795E-01 RA-228 8.518E-01 2.795E-01 2.795E-01 TH-228 9.072E-01 l.354E-01 l.354E-01 TH-230 6.925E-01 1.677.E-01 1.677E-01 PA-231 4.565E-01 6.228E-01 6.228E-01 TH-232 8.518E-01 2.795E-01 2.795E-01 U-234 6.925E-01 l.677E-01 1.677E-01 U-235 2.505E-01 2.903E-01 2.903E-01 AM-243 1.405E-01 1.070E-01 1.070E-01 ANH-511 7.973E-02 7.499E-02 7.499E-02 Non-Identified Nuclides Key-Line K.L Act Activity error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 5.078E+00 l.179E+Ol l.201E+Ol NOT IDENT. NA-22 -4.709E-04 4.743E-02 4.743E-02 NOT IDENT. NA-24 1.000E+41 7.082E+41 O.OOOE+OO SHORT HLIF AL-26 2.565E-03 3.326E-02 3.328E-02 NOT IDENT. SC-46 -1.242E-01 3.861E-01 3.901E-01 FAIL ABUN V-48 -6.508E+03 l.297E+04 l.330E+04 SHORT HLIF Page 4114of5809 CR-51 1.591E+02 3.780E+02 3.848E+02 SHORT HLIF MN-54 -1.868E-02 6.175E-02 6. 232E-02 NOT IDENT. C0-56 -2.089E-01 4.672E-01 4.766E-01 FAIL ABUN MN-56 -1.000E+41 2.199E+41 0. OOOE+o*o SHORT HLIF C0-57 2.319E-02 4.538E-02 4.657E-02 NOT IDENT. C0-58 -6.565E-02 6.036E-01 6.044E-01 NOT IDENT. FE-59 -1.102E+OO 6.391E+OO 6. 411E+OO NOT IDENT. C0-60 6.926E-03 3.033E-02 3.049E-02 NOT IDENT. ZN-65 -1.140E-01 1.892E-01 1. 960E-01 NOT IDENT. GE-68 -l.309E-02 2.177E+OO 2.177E+OO NOT IDENT. AS-73 -1.359E+OO 1. 372E+Ol l.373E+Ol NOT IDENT. AS-74 1.111E+o3 5.436E+03 5.459E+03 SHORT HLIF SE-75 -2.272E-02 l.935E-01 l.938E-01 NOT IDENT. BR-77 2.132E+38 l.851E+39 O.OOOE+OO SHORT HLIF SR-82 4.813E+02 6.561E+02 6. 911E+02 SHORT HLIF RB-83 -5.029E-01 6.775E-01 7.145E-01 NOT IDENT. KR-85 8. 711E+OO 5.865E+OO 7.058E+OO NOT lDENT. SR-85 9.287E-01 6.257E-01 7.528E-01 NOT IDENT. RB-86 -1. 209E+03 2.684E+04 2.684E+04 SHORT HLIF Y-88 3.866E-03 l.022E-01 1.022E-01 NOT IDENT. Y-91 -2.922E+Ol 5.285E+02 5.286E+02 NOT IDENT. NB-94 9.007E-03 3.567E-02 3.590E-02 NOT IDENT. NB-95 7.526E-01 6.729E-01 7.536E-01 NOT IDENT. NB-95M -5.399E-01 2.510E+OO 2.522E+OO NOT IDENT. ZR-95 2.042E+OO 2.0S7E+OO 2.281E+OO FAIL ABUN NB-97 1.000E+41 1. 736E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 3.070E+41 O.OOOE+OO SHORT HLIF M0-99 4. 5'42E+31 2.173E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 6.857E+41 O.OOOE+OO SHORT HLIF RH-101 -2.063E-02 3.057E-02 3.195E-02 NOT IDENT. RH-102 -6.334E-03 4. 881E-02 4.890E-02 NOT IDENT. RU-103 2.050E+OO 5.284E+00 5.364E+OO FAIL ABUN RH-106 -2.491E-01 4.665E-01 4.798E-01 NOT IDENT. RU-106 -2. 491E-01 4.665E-01 4.798E-01 NOT IDENT. AG-108M l.034E-05 2.625E-02 2.625E-02 NOT IDENT. AG-llOM -7.645E-02 9.598E-02 l.020E-01 FAIL ABUN SN-113 2.238E-01 2.042E-01 2.278E-01 NOT IDENT. CD-115 9.063E+35 3.639E+39 O.OOOE+OO SHORT HLIF SN-117M -3.524E+03 9.785E+04 9.786E+04 SHORT HLIF TE-123M -4.514E-02 l.313E-01 l.329E-01 NOT IDENT. SB-124 -6.261E-02 1.386E+OO l.387E+OO NOT IDENT. SB-125 -3.326E-02 9.689E-02 9.805E-02 NOT IDENT. TE-125M 2.643E+Ol 2.573E+02 2.576E+02 NOT IDENT. I-126 4.940E+05 9.756E+05 SHORT HLIF SB-126 4.295E+05 l.241E+06 l.256E+06 ,SHORT HLIF SB-127 -5.030E+21 2.353E+22 O.OOOE+OO SHORT HLIF I-131 -l.318E+09 4.381E+09 4.421E+09 SHORT HLIF I-132 l.000E+41 1.875E+42 O.OOOE+OO SHORT HLIF TE-132 4.391E+26 8.359E+26 O.OOOE+OO SHORT HLIF BA-133 1.889E-02 3.694E-02 3.791E-02 NOT IDENT. I-133 1.000E+41 6.820E+41 O.OOOE+OO SHORT HLIF CS-134 6.979E-03 4.658E-02 4.669E-02 NOT IDENT. CS-135 8.429E-03 1.271E-01 1. 271E-01 NOT IDENT. I-135 l.000E+41 6.958E+41 0.000E+OO SHORT HLIF CS-136 -4.572E+03 3.098E+05 3.098E+05 SHORT HLIF CE-139 -3.729E-03 1.039E-01 l.039E-01 NOT IDENT. BA-140 -7.780E+05 1.322E+06 1.368E+06 SHORT HLIF LA-140 -1.006E+05 3.814E+05 3. 841E+05 SHORT HLIF CE-143 1.000E+41 l.074E+42 O.OOOE+OO SHORT HLIF CE-144 -8.229E-02 3.167E-01 3.188E-01 NOT IDENT. PM-144 --:2.043E-02 5.662E-02 5.736E-02 NOT IDENT. PR-144 -1. 746E+OO 4.924E+OO 4.987E+OO NOT IDENT. PM-146 -9.611E-03 3. 968E-02 3.992E-02 NOT IDENT. ND-147 4.848E+06 3.374E+07 3 .. 381E+07 SHORT HLIF PM-147 3.370E+02 7.819E+02 7.965E+02 NOT IDENT. PM-149 1.357E+40 5. 851E+40 0. OOOE+OO . SHORT HLIF EU-150 -1.239E-02 2.869E-02 2.923E-02 FAIL ABUN EU-152 -2.530E-02 8.775E-02 8.849E-02 FAIL ABUN GD-153 5.218E-02 1.667E-01 l.683E-01. NOT IDENT. EU-154 -3.556E-03 1.157E-01 1.157E-01 FAIL ABUN EU-155 5.619E-02 1.018E-01 l.049E-01 FAIL ABUN TB-160 6.498E-01 2 .117E+OO 2.138E+OO FAIL ABUN H0-166M -2.757E-03 5.332E-02 5. 334E-02* FAIL ABUN TM-171 -2.908E+00 3.255E+Ol 3.257E+Ol NOT IDENT. HF-172 l.615E-01 2.102E-Ol 2.225E-01 NOT IDENT. LU-172 -3.505E-02 6.381E-02 6.574E-02 FAIL ABUN LU-176 l.238E-02 2.034E-02 2. llOE-02 FAIL ABUN HF-181 -5.949E-01 3.582E+OO 3.592E+OO NOT IDENT. Page 4115 of 5809 TA-182 -9.336E-01 1.068E+OO 1.148E+OO FAIL ABUN RE-183 -9.267E-01 3.636E+OO 3.660E+00 NOT IDENT. RE-184 1. 33*9E+Ol 3.022E+Ol 3.082E+Ol NOT IDENT. W-188 -l.392E+02 1.016E+02 l.194E+02 FAIL ABUN IR-192 -1. 763E-01 3.992E-01 4.070E-01 FAIL ABUN HG-203 4.008E-01 2.127E+OO 2.135E+00 NOT IDENT. BI-207 -4.335E-02 4.508E-02 4.914E-02 FAIL ABUN PB-210 l.292E+OO 6. 721E+OO 6.746E+OO NOT IDENT. PB-211 -4.806E-01 6.688E-01 7.030E-01 NOT IDENT. BI-212 6 .115E-01 1.023E+OO 1.060E+OO FAIL ABUN RN-'219 2.462E-01 3.381E-01 3.559E-01 FAIL ABUN RA-223 -5.160E-02 5.894E-01 5.898E-01 FAIL ABUN AC-227 1.368E-01 3.747E-01 3.797E-01 FAIL ABUN TH-227 1.368E-01 3.747E-01 3.797E-01 FAIL ABUN TH-229 1.215E-01 3. 985E:..._01 4.023E-01 FAIL ABUN TH-231 -5.160E-02 5.894E-01 5.898E-01 FAIL ABUN PA-233 2.694E-02 5.048E-02 5.192E-02 FAIL ABUN PA-234 -l.333E-01 3.030E-01 3.089E-01 NOT IDENT. PA-234M 2.979E+OO 3.779E+OO 4. OllE+OO NOT IDENT. TH-234 2.685E-01 1.472E+OO 1.477E+00 FAIL ABUN NP-237 2.694E-02 5.048E-02 5.192E-02 FAIL ABUN NP-238 -1.000E+41 3.151E+41 O.OOOE+OO SHORT HLIF U-238 2.685E-:-01 1. 472E+OO l.477E+OO . FAIL ABUN NP-239 -1.431E-02 2.103E-01 2.104E-01 FAIL ABUN PU-239 2 .114E+02 2.730E+02 2.892E+02 NOT IDENT. AM-241 6.150E-02 1.658E-01 1.681E-01 NOT IDENT. CM-243 -4.899E-02 9.477E-02 9.731E-02 FAIL ABUN BK-247 -3.478B-02 6.948E-02 7.123E-02 NOT IDENT. CM-247 1.793E-02 3. 241E-02 3.340E-02 NOT IDENT. CF-249 -6. 72 6E-03 3.109E-02 3.124E-02 NOT IDENT. CF-251 -1.197E-02 l.045E-01 l.047E-01 FAIL ABUN Page 4116 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 56.4509 87.09 90.6453 136.47 56.9215 45.60 50.6102 87.57 90.7352 140.51 0.0000 46.54 52.5403 88.03 63.1792 143.76 59.7089 49.72 0.0000 88.34 63.2192 144.24 59.7509 51. 35 60.5342 88.47 63.2358 145.44 59.4914 51. 87 68.7695 89. 96 72.6759 152.43 62.6473 5"2.39 54.3732 1093.63 72.7750 153.25 0.0000 52.97 50.8329 91.11 0.0000 323.87 82.6332 53.44 59.9905 92.59 73.0569 156.02 0.0000 54.07 52.8130 93.35 73.1660 158.56 0.0000 57.36 0.0000 94.56 73.3389 159.00 77.6306 57.53 59.7555 94.65 73.3518 162.33 64.6101 57.98 56.1462 94.67 73.3546 162.66 0.0000 59.27 53.5694 94.87 73.3831 163.33 82.5432 59.32 53.5765 97.43 . 54.9732 165.86 64. 9119 59.54 55.4562 98.43 62.4659 176.31 45.3699 60. 96 65.8683 98.44 62.4671 176.60 0.0000 61.17 76.1149 99.53 72. 6916 177.52 60.2065 62. 93 65.2716 100 .11 66.7060 181.07 0.0000 63.29 71. 8644 102.03 64.9155 181.52 56.3190 63.58 73.7854 103.18 74.2002 184.41 51. 5533 64.28 77.6586 103.37 74.2264 143.76 51.6357 66.73 71. 5434 105.21 61.2122 193.51 47.4832 67.24 91.4259 105.31 61.2231 197.03 61. 6330 125.81 91.5244 106.12 76.6405 198.01 58.2100 67.75 91. 5392 106.47 76.6886 201. 83 58.4656 69.67 77 .1107 109.28 64.7400 203.43 58.5716 70.83 93.8015 111. 00 70.0887 205.31 58.6952 72. 81 70.6775 111. 76 0.0000 210.85 62. 6011 72.87 70.6876 114'.06 67.3501 215.65 51. 0566 74.66 70.9784 116. 30 0.0000 222.11 41.8461 74.82 71.0044 116.74 58.2888 227.09 46.8731 74.97 71. 0286 119.76 70.0895 227.38 46.8874 77 .11 71.3713 121.12 62.9068 228.16 0. 0000 ' 78.:J4 71.6293 121. 22 62.9173 228.18 43.3169 79.69 72.4250 121.78 70.3216 116. 74 43.3169 80.12 71.1983 122.06 63.0034 235.69 61. 4361 80.19 *o.oooo 122.92 75.7095 235. 96 61.4524 80.57 63.4930 123.07 83.0907 238.63 47.4301 81. 00 68.7403 265.00 77.9086 238.98 0.0000 81. 07 64.8590 125.81 55.9902 240.99 47.5420 81.75 72.7480 127.23 71. 9979 242.00 47.5902 83.79 84.8067 127.91 68.8959 244.70 47.7175 84.00 77.0126 129.30 55.2365 252.40 0.0000 85.43 86.4075 131.20 68.1855 252.80 36.1743 86.55 90.5450 133.02 63.0341 254.15 0.0000 86.79 90.5892 133.52 64.1519 256.23 46.1916 86.94 90.6180 136.00 56.8810 260.90 0.0000 Page 4117 of 5809 ENERGY MDA COUNTS ENERGY MQA COUNTS ENERGY MDA COUNTS 264.66 41.1553 355.39 0.0000 584.27 22.6678 264. 8 0 47.3979 356. 01 . 24.2150 595.83 0.0000 265.00 47.4061 364.49 0.0000 427.87 24.9307 268.22 40.0400 366.42 0.0000 602.52 0.0000 269.46 41. 338 6 372. 51 30.8630 604.72 12.4907 270.03 45 .1198 375.05 28.6462 607.14 21.8844 271.23 45.1703 377.52 24. 5967 609.32 26.0813 273.65 0.0000 356.01 33.8579 610.33 31.3123 276.40 44.5419 388.16 27.5354 614.28 20.3926 277.37 43.7396 388.63 0.0000 618. 01. 9.4288 277.60 43.7480 391.69 20.2419 620. 36 10.4883 278.00 43.7639 264.66 34.2532 621.93 19.9432 279.20 42.1265 401.81 23.1618 630.19 0.0000 279.54 48.0381 402.40 26.8789 631. 29 14.7611 279.70 52.2595 404.85 42.7057 633.25 14.7747 280.46 47.2340 410.95 31.6945 634.78 0.0000 283.69 38.0649 413.71 25.2153 635.95. 12.6802 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42.3584 423.72 0.0000 645.85 15.9241 285.90 0.0000 427.09 31. 0899 657.76 14.4108 287.50 37.3443 427.87 31.1053 657.90 0.0000 290.67 45.9580 433.94 28.3881 661. 66 . 17.1100 293.27 0.0000 439.40 30.3854 664.57 0.0000 351.93 37.5941 453.88 26.8288 666.33 0.0000 295. 96 37.6182 463.37 25.0574 666.50 0.0000 879.38 48.8417 468.07 25.1288 667. 71 0.0000 299.98 49.7576 473.00 0.0000 677.62 17.7729 300.09 49.7623 475.06 29 .1162 685.70 0.0000 300.13 49.7635 476.78 24.2884 695.00 0.0000 301.36 30.9199 477.60 22.3561 696. 49 23.8960 302.85 29.6688 482.18 19.4930 696.51 23.8969 256.23 24.5432 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.3854 306.78 29.3357 497.08 19.6623 697.49 16.3000 308.46 34.5605 505.52 16.2996 702.65 25.0496 311. 90 30.3266 507.63 0.0000 706.68 22. 9115 316.51 38.2690 511. 00 20.8094 711. 68 17.4941 319.41 0.0000 514.00 5.9556 720.70 0.0000 *320.08 0.0000 514.00 5.9556 721.93 0.0000 321. 04 37.5358 520.40 25.4014 722.78 18.1274 323.87 39.3713 520.69 0.0000* 722. 91 19.7761 325.23 31. 5315 522.65 0.0000 723.31 19.7798 328.76 0.0000 527.90 0.0000 724.19 23.0850 333.37 35.2604 528.26 18.0081 727. 33 20.9142 333.97 44.0959 529.59 25.0295 733.00 20.9645 334.37 38.3758 529.87 0.0000 735.93 17.6758 338.28 36.2804 531.02 0.0000 333.97 23.2148 338.32 36.2812 537.26 0.0000 739.50 0.0000 311. 90 36.3421 546.56 0.0000 747.24 13.3198 340.48 36.3421 552.55 13.1767 748.06 14.4346 340.55 0.0000 563.25 21.4050 752.31 18.3530 344.28 33.3366 569.33 24.5400 753.82 0.0000 345.93 28.0380 946.00 24.5420 756.73 3.3430 351.06 33.9551 569.70 24.5449 756.80 3.3431 351. 93 33.9767 583.19 22.6553 884.68 8. 9411 Page 4118of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 3.3555 1274.44 17.3336 1620.50 7.5345 766.42 8.3905 1001.03 9.1373 1621. 92 8.6138 766.84 8.3920 1002.74 15.5417 1678.03 0.0000 772. 60 0.0000 1004.73 15.5520 1690.97 2.1854 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.1094 778.90 13.4927 1028.54 0.0000 1063.66 3.3322 783.70 0.0000 1037.84 7.3970 1771. 35 1.1110 785.37 7.8912 1038.76 0.0000 1791.20 0.0000 792.07 14.6943 631. 29 10.1984 1808.65 4.4771 794.95 12.4475 1048.07 0.0000 1810.72 0.0000 795.86 14.7160 1049.04 7.4229 1836.06 0.9002 810.06 18.2129 1050.41 13. 9243 810.29 18.2148. 1063.66 17. 7104 344.28 17.0770 1077.00 0.0000 810.76 17.0795 1077.34 12.1685 815.77 0.0000 1085.87 8'.4463 1048.07 0.0000 1093.63 12. 2296 832.01 12.6274 1099.45 13 .1934 834.85 17.2375 1112. 07 12.2978 835.71 13.7949 1112. 84 14.0573 836.80 0.0000 1115. 54 16.6665 846.75 0.0000 1120.29 7.5864 846.77 17.3157 '1120.55 7.5869 856.80 0.0000 1221. 41 7.5884 860.56 4.6413 1129. 67 2.8528 871. 09 15.1423 1131.51 0.0000 873.19 15.1540 1147.95 0.0000 875. 33 0.0000 1173.23 13. 4830 879.38 16.3567 1177.95 17.3584 880.51 9.6428 1189.05 14. 5111 883.24 19.3044 1204.77 14.5752 884.68 19.3145 , 1221. 41 25.3811 889.28 18.4673 1231.02 16.9652 894.76 16.7415 1235.36 0.0000 898.04 14. 9964 1238.28 7.8457 900. 72 15.0109 1260.41 0.0000 903.28 13.2568 1271.87 9. 2371 911.20* 15.0670 1274.44 9.5074 912.08 15.6036 1274.54 9.5074 923.98 0.0000 1291.59 8.9539 926.50 14.2568 1298.22 0.0000 929 .11 16.0532 1312 .11 0.0000 937.49 18.7832 1332.49 5.0278 944.13 0.0000* 1362.66 0.0000 946.00 17.0442 1365.19 8 .1113 949.00 14.3677 1368.63 0.0000 667.71 0.0000 1384.29 7.1316 962. 31 12.9894 1408.01 4.0991 964.08 12.6362 1457.56 0.0000 966.17 12.6452 1460.82 6.2278 911.20 12.6572 1489.16 4.1797 968. 97 12.6572 1505.03 9.4389 983.53 0.0000 1584.12 5.3391 984.45 0.0000 1596.21 0.0000 Page 4119 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:08:16.27 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM31.CNF;306 Background date : Z-OCT-2016 11:01:52. Sample date 1-DEC-2015 14:24:00. Acquisition date : 3-0CT-2016 07:06:55. Sample ID G405235053 Sample quantity 1.13628E+02 GRAM Detector name : GAM31 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.45 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 0 4 0 5 3 6 3 7 3 8 3 9 3 10 0 11 0 12 0 13 0 14 0 15 6 16 6 17 6 18 0 19 0 20 0 21 0 22. 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 4 Page 4120 of 5809 Energy 34.92 46.45* 52.85* 63.32* 74.89 77.09* 87.25* 89.89 92.79* 129.83 186.17* 192.13 209.30 213 .. 16 237.07* 238.66* 241.75* 253.16 295.61* 301.10 317.48 338.66*

352.12* 393.88 417.46 463. 71 583.40* 609.81* 662 .11 679.68 706.37 727.99 771.11 785.68 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 33 48 10 33 160 250 84 77 104 63 90 19 29 6 9 323 93 24 90 19 11 60 203 15 32 19 63 137 45 18 9 31 28 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 156 257 207 247 203 111 82 123 115 54 77 37 38 61 15 45 81 27 75 51 20 59 57 14 41 55 32 33 32 31 21 12 17 14 0.67 1. 31 1. 27 0.92 1. 09 0.87 0.91 1. 28 1. 29 2.25 1. 30 0.95 0.92 0.75 1. 45 1.29 2.13 1. 27 1. 21 1. 74 1.17 1.19 1. 20 1. 55 0.77 1. 02 1. 73 1. 29 1. 47 '3. 97 3.43 4.14 5.25 1. 70 69.51 92.54 105.34 126.25 149.38 153.78 174.08 179.36 185.16 259.17 371. 79 383.69 418.00 425.72 473.50 476.68 482.85 505.66 590.50 601.48 634.21 676.54 703.44 786.91 834.03 926.48 1165. 69 1218.48 1323.01 1358.14 1411.47 1454.68 1540.88 1570.00 68 88 104 123 146 146 170 170 170 '255 366 381 415 422 472 472 472 503 585 596 631 672 698 784 827 920 1159 1214 1316 1347 1404 1448 1534 1566 6 9. 25E-03 61. 1 8 1. 34E-02 61. 2 6 2.77E-03235.6 7 9.07E-03 87.3 12 4.43E-02 16.1 12 6.95E-02 9.4 21 2.33E-02 19.7 21 2.15E-02 27.7 21 2.89E-02 22.5 8 1.76E-02 23.8 11 2.50E-02 22.7 5 5.14E-03 54.1 6 8.05E-03 38.6 7 1.61E-03225.0 17 2.58E-03 76.1 17 8.96E-02 6.8 17 2.58E-02 28.7 7 6.63E-03 41.2 12 2.50E-02 22.5 9 5.25E-03 72.3 6 3.15E-03 72.1 12 1.67E-02 28.8 12 5.64E-02 10.5 6 4.26E-03 45.7 14 8.89E-03 46.4 12 5.39E-03 79.2 15 1.76E-02 23.4 10 3.82E-02 12.0 12 l.25E-02 29.6 18 5.12E-03 74.9 12 2.41E-03111.3 13 8.49E-03 30.2 14 7.83E-03 38.6 12 3.30E-03 56.4 Fit 1.26E+OO 1.59E+OO 4.83E+OO l.63E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 4 788.17 13 4 1. 43 1574.97 1566 12 3.49E-03 40.l 36 0 795.74 13 7 1. 73 1590 .11 1585 10 3.56E-03 48.5 37 0 804.59* 17 19 4.07 1607.78 1601 15 4.71E-03 62.0 38 0 842.05 18 8 1. 27 1682.66 1676 10 5.06E-03 36.7 39 0 861.42 11 20 0.85 1721.38 1712 13 2.92E-03 92.0 40 0 866.61 16 2 2.09 1731.76 1727 9 4.38E-03 30.4 41 0 873.71. 15 3 1. 95 1745.95 1740 10 4.24E-03 32.2 42 0 911. 70* 57 8 1. 63 1821. 88 1817 10 l.59E-02 16.6 43 0 935.55 5 17 2.41 1869.56 1860 11 l.25E-03181.0 44 0 964. 65 24 8 1. 57 1927.71 1921 11 6.68E-03 30.8 45 0 969. 69 20 19 0.69 1937.80 1933 10 5.55E-03 47.2 46 0 1093.35 11 2 1. 54 2184.98 2181 8 3.llE-03 36.8 47 0 1121. 84 18 21 1. 49 2241.92 2235 11 4.88E-03 56.8 48 0 1151. 31 6 12 0.61 2300.83 2290 12 1.67E-03122.S 49 0 1174.94 14 11 1. 53 2348.06 2342 12 3.86E-03 60.2 50 0 1239.26 47 4 0.68 2476.62 2468 18 1. 30E-02 18.0 51 0 1305.66 10 2 0.90 2609.36 2605 9 2.79E-03 41.1 52 0 1461. 40* 222 3 2 .11 2920.68 2913 14 6.16E-02 7. 0 53 0 1580.37 8 0 0.83 3158.50 3155 8 2.22E-03 35.4 54 0 1765.49* 21 0 1. 97 3528.57 3523 10 5.81E-03 23.4 Flag: "*" = Peak area was modified by background subtraction Page 4121 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:08:18 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 1-DEC-2015 14:24:00 G405235053 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:06:55 113. 63 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA31 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4122 of 5809 PB-214 PB-214 PB-214 PB-214* PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:06.45 10.00 0.00 % Peak Energy 0.2% Nuclide Line Activity Report Page : 2 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 6.945E-01 1.865E+Ol 1.865E+Ol 14.10 OK AS-73 53.44 10.30* 5.707E+OO 1.204E-01 l.699E+OO 471. 25 OK NB-95M 235.69 24.80* 3. 221E+OO 7.798E-02 2.158E+OO 152.26 OK CD-109 88.03 3.70* 5.391E+OO 1.807E+OO 2.865E+OO 69. 72 OK SN-126 64.28 9.60 5.587E+OO 4.291E-01 4.291E-01 174.69 OK 86.94 8.90 5.391E+OO 7.513E-01 7.513E-01 69. 72 OK 87.57 37.00* 5.391E+OO l.807E-01 1.807E-01 69. 72 OK BA-137M 661. 66 89.90* 1.340E+OO 2.395E-01 2.442E-01 59.17 OK CS-137 661. 66 85.10* 1.340E+OO 2.530E-01 2.580E-01 59.17 OK TL-208 277.37 6.60 2.816E+OO Line Not Found Absent 583.19 85.00* 1.486E+OO 3.237E-01 3.237E-01 46.76 OK 860.56 12.50 1.083E+OO *4.936E-01 4.936E-01 184.06 OK PB-210 46.54 4.25* 5.476E+OO 1.482E+OO 1. 521E+OO 122.39 OK BI-211 72.87 1. 23 5.491E+OO Line Not Found Absent 351. 06 12.92* 2.285E+OO 1.179E+OO 1.179E+OO 151. 34 OK BI-212 727.33 6.67* 1. 241E+OO 2.367E+00 2.367E+OO 60.41 OK 785.37* 1.10 1.167E+OO 5. 920E+OO

5.920E+OO 112.83 *oK 1620.50 1. 47 6.312E-01 Line Not Found Absent PB-212 74.82 10.28 5.476E+OO 1.299E+OO 1.299E+OO 54.73 OK 77 .11 17.10 5.460E+OO 1.*877E+OO 1.877E+OO 18.80 OK 238.63 43.60* 3.203E+OO 1.549E+OO 1.549E+OO 13.65 OK 300.09 3.30 2. 621E+OO 1. 451E+OO 1. 451E+OO 144.54 OK BI-214 609.32 45.49* l.433E+OO 1.361E+OO 1. 361E+OO 23.96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 l.453E+00 1.453E+OO 46.87 OK PB-214 74.82 5.80 5.476E+OO Line Not Found <<INT Reject 77 .11 9.70 5.460E+OO 3.308E+OO 3.309E+OO 18.80 OK 87.09 3.41 5.392E+OO Line Not Found <<INT Reject 242.00 7.25 3.165E+OO Line Not Found <<INT Reject 295.22 18.42 2.664E+OO 1.218E+OO 1.219E+OO 44.95 OK 351. 93 35.60* 2.286E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1.433E+OO 1.361E+OO 1.361E+OO 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO l.453E+OO 46.87 OK RA-224 240.99 4.10* 3.168E+OO 2.630E+OO 2.630E+OO 110.71 OK RA-226 609.32 45.49* 1.433E+OO 1. 361E+OO l.361E+00 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 OK AC-228 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11. 27 2.364E+OO 1.495E+OO l.495E+OO 57.51 OK 794.95 4.25 1.155E+OO l.669E+OO 1.669E+OO 97.08 OK 835. 71 1. 61 1. llOE+OO Line Not Found Absent 911. 20 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 OK 968. 97 15.80 9.842E-01 8 .136E-01 8.136E-01 94.46 OK RA-228 105.21 1.10 5.215E+OO Line Not Found Absent 33S.32 11. 27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 OK 794.95 4.25 1.155E+OO 1. 669E+oo* 1.669E+OO 97.08 OK 835. 71 1. 61 1. llOE+OO Line Not Found Absent 911. 20 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 OK Page 4123of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 968. 97 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 OK TH-228 74.82 10.28 5.476E+OO 1.299E+OO 1.299E+OO 54.73 OK 77 .11 17.10 5.460E+OO l.877E+OO 1.877E+OO 18.80 OK 238.63 43.60* 3.203E+OO 1.549E+OO l.549E+OO 13.65 OK 300.09 3.30 2.621E+OO l.451E+OO l.451E+OO 144.54 OK TH-230 609.32 45.49* 1. 433E+-oo 1.361E+OO 1.361E+OO 23. 96 OK 1120. 29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 OK PA-231 283.69 1. 70 2.761E+OO Line Not Found Absent 301.36 5.35* 2. 621E+OO 8.948E-01 8.948E-01 144.54 OK TH-232 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11. 27 2.364E+OO l.495E+OO 1.495E+OO 57.51 OK 835.71 1. 61 1. llOE+OO Line Not Found Absent 911.20 25.80* 1.035E+OO 1.359E+OO 1.359E+OO_ 33.22 OK 968. 97 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 OK TH-234 63.29 3.70* 5.587E+OO 1.113E+OO 1.113E+OO 174.69 OK. 92.59 4.23 5.346E+OO 3.199E+00 3.199E+OO 45.04 OK U-234 609.32 45.49* 1.433E+OO l.361E+OO 1. 361E+.oo 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found -----Absent 1764.49 15.30 5.810E-01 1. 453E+OO 1.453E+OO 46.87 OK U-235 89. 96 3.47 5.370E+OO 2.885E+00 2.885E+OO 55.41 OK 93.35 5. 60. 5.346E+OO 2.416E+OO 2.416E+00 45.04 OK 143.76 10.96* 4. 611E+00 Line Not Found Absent 163.33 5.08 4.273E+OO Line Not Found Absent 185.72 57.20 3.902E+OO 2.725E-01 2.725E-01 45.34 OK 205.31 5.01 3.621E+OO Line Not Found Absent U-238 63.29 3.70* 5.587E+OO l .113E+OO 1.li3E+OO 174.69 OK 92.59 4.23 5.346E+oo-3.199E+OO 3.199E+OO 45.04 OK AM-243 43.53 5.90 5.049E+OO Line Not Found Absent 74.66 67.20* 5.476E+OO l.987E-01 l.987E-01 54.73 OK Flag: "*" = Keyline Page 4124 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:08:19.65 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 2 9407 , * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l *
Acquisition date 3-0CT-2016 07:06:55 Sensitivity : 3.000 *
Detector ID GAM31 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.45 Half life ratio : ***** *
Sample date 1-DEC-2015 14:24:00 Analyst initials: MXRl *
Sample ID G405235053 Sample Quantity 1.1363E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;?
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 865E+Ol 2.577E+OO 9.734E-01 AS-73 1.699E+OO 7.848E+OO 9.571E+OO NB,-95M 2.158E+OO 3.220E+OO 7 .112E+OO CD-109 2. 8 65E+OO 1.957E+OO 2. 331E+OO SN-126 1. 807E-01 1.235E-01 l.469E-01 BA-137M 2.442E-01 1.416E-01 l .196E-01 CS-!37 2.580E-01 l.496E-01 l.263E-01 TL-208 3.237E-01 l.483E-01 1.132E-01 PB-210 1.521E+OO 1.825E+OO 1.575E+OO BI-211 1.179E+OO 1. 749E+OO 6.353E-01 BI-212 2.367E+OO l.401E+OO 1.623E+OO PB-212 l.549E+OO 2. 072E-01 1.5"08E-01 BI-214 1.361E+OO 3.196E-01 2.487E-01 PB-214 1. 647E+OO 3.387E-01 6.060E-01 RN-222 1. 361E+OO 3 .196E-01 2.487E-01 RA-224 2.630E+OO 2.853E+OO l.619E+OO RA-22 6 . 1. 361E+OO 3 .196E-01 2.487E-01 AC-228 1. 359E+OO 4.425E-01 4.269E-01 RA-228 1.359E+OO 4.425E-01 4.269E-01 TH-228 1. 549E+OO 2.072E-01 1.508E-01 TH-230 l.361E+OO 3.195E-01 2.486E-01 PA-231 8.948E-01 l.268E+OO l.247E+OO TH-232 l.359E+OO 4.425E-01 4.269E-01 TH-234 l .113E+OO 1.906E+OO l.934E+OO U-234 1.361E+OO 3.195E-01 2.486E-01 U-235 l .112E-01 2.856E-01 5.214E-01 U-238 l .113E+OO 1.906E+OO l.934E+OO AM-243 l.987E-01 1.066E-01 9.914E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 -1.162E+Ol 2.455E+Ol 4.373E+Ol NOT IDENT. NA-22 -4.217E-02 9.695E-02 1. 752E-01 NOT IDENT. Page 4125 of 5809 NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -8.769E-03 5.684E-02 1.230E-01 NOT IDENT. SC-46 8.840E-02 6. 221E-01 l.323E+00 FAIL ABUN V-48 O.OOOE+OO 3.685E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 8.926E+02 O.OOOE+OO SHORT HLIF MN-54 -2.729E-02 1.379E-01 2.479E-01 NOT IDENT. C0-56 6.006E-01 l.077E+OO 2.176E+00 FAIL ABUN MN-56 0.000E+OO 1.814E+41 O.OOOE+OO SHORT HLIF C0-57 3.881E-02 6.601E-02 1.278E-01 NOT IDENT. C0-58 6.132E-02 1. 22 6E+OO 2 .113E+OO NOT IDENT. FE-59 3.195E+OO 1. 567E+Ol 3.178E+Ol NOT IDENT. C0-60 -4.484E-03 8.580E-02 l.676E-01 NOT IDENT. ZN-65 1. 64 7E-01 3.409E-01 6.743E-01 NOT IDENT. GE-68 -2.607E-01 3.669E+OO 7.472E+OO NOT IDENT. AS-74 O.OOOE+OO l.473E+04 O.OOOE+OO SHORT HLIF SE-75 -l.205E-01 4.214E-01 7 .135E-01 NOT IDENT. BR-77 O.OOOE+OO 2.762E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l.813E+03 O.OOOE+OO SHORT HLIF RB-83 1.675E+OO 1.272E+oo* 2.846E+OO NOT IDENT. KR-85 -3.053E+Ol l.857E+Ol 2.840E+Ol NOT IDENT. SR-85 -3.468E+OO 2.109E+OO 3.225E+OO NOT IDENT. RB-86 O.OOOE+OO 5.854E+04 O.OOOE+OO SHORT HLIF Y-88 1. 564E-01 3.224E-01 9.000E-01 NOT IDENT. Y-91 1.363E+02 l.088E+03 2 .191E+03 NOT IDENT. NB-94 -7.107E-03 6.854E-02 l .112E-01 NOT IDENT. NB-95 3.041E-03 2.217E+00 3.635E+00 NOT IDENT. ZR-95 2.419E-01 3.079E+OO 5.864E+00 NOT IDENT. NB-97 0. OOOE+oo* 1. 92 9E+4 l O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 549E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.084E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.143E+41 O.OOOE+OO SHORT HLIF RH-101 -l.496E-02 5 .119E-02 8.373E-02 NOT IDENT. RH-102 -9.265E-04 9.445E-02 1.834E-01 NOT IDENT. RU-103 -l.245E+00 9.576E+OO l.845E+Ol FAIL ABUN RH-106 2.162E-01 . 8. 727E-01 1.746E+OO NOT IDENT. RU-106 2.162E-01 8.727E-01 1.746E+OO NOT IDENT. AG-108M 7.238E-03 5.566E-02 l.074E-01 NOT IDENT. AG-llOM 2.637E-03 l.349E-01 2.888E-01 FAIL ABUN SN-ll3 -l.369E-01 4.188E-01 6.919E-01 NOT IDENT. CD-l15 O.OOOE+OO 4.224E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2. l18E+05 O.OOOE+OO SHORT HLIF TE-123M -2.899E-02 2.079E-01 3.712E-01 NOT IDENT. SB-124 -l.536E-01 5.196E+OO l.048E+Ol NOT IDENT. SB-125 3. 2l1E-02 l.991E-01 3.874E-01 FAIL ABUN TE-125M 3.297E+Ol 4.267E+02 7.870E+02 NOT IDENT. I-126 0.000E+OO 2.091E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.884E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.488E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1. 572E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.806E+27 O.OOOE+OO SHORT HLIF BA-133 6.087E-03 8.316E-02 l.453E-01 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 d.OOOE+OO SHORT HLIF CS-134 l.099E-01 1. 046E-01 l.998E-01 FAIL ABUN CS-135 1.598E-02 2.682E-01 4.724E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.328E+05 0.000E+OO SHORT HLIF CE-139 1.094E-01 1. 869E-01 3. 541E-01 NOT IDENT. BA-140 O.OOOE+OO 3.403E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1.283E+06 O.OOOE+OO SHORT HLIF CE-141 -l.163E+Ol 4.342E+Ol 7.463E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 3.845E-01 5.588E-01 1.016E+OO NOT IDENT. PM-144 -4. ll 7E-03 9.409E-02 l.787E-01 NOT IDENT. PR-144 -2.133E+OO 8.554E+OO 1.556E+Ol NOT IDENT. PM-146 6.430E-02 7.829E-02 l.655E-01 NOT IDENT. ND-147 O.OOOE+OO 6. 963E+07 O.OOOE+OO SHORT HLIF PM-147 -l.987E+02 1.102E+03 l.995E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 3.877E-03 4.925E-02 8.644E-02 FAIL ABUN EU-152 8.353E-02 l.595E-01 3.032E-01 FAIL ABUN GD-153 -2.851E-02 2.426E-01 4.105E-01 NOT IDENT. EU-154 -1.030E-01 2.368E-Ol 4.280E-01 FAIL ABUN EU-155 -4.819E-02 1. 468E-01 2.627E-01 FAIL ABUN TB-160 -3. 728E-01 3.322E+OO 6.676E+OO FAIL ABUN H0-166M -5.595E-02 l.134E-01 l.843E-01 NOT IDENT. TM-171* 3. 572E+00 1.649E+Ol FAIL ABUN HF-172 l.564E-01 3.590E-01 6.356E-01 FAIL ABUN. Page 4126 of 5809 LU-172 1. 714E-01 1.238E-01 3.016E-01 FAIL ABUN LU-176 -2.145E-02 3.821E-02 7.012E-02 FAIL ABUN HF-181 4.405E-03 8.388E+OO 1.619E+Ol NOT IDENT. TA-182 6.625E-01 1.889E+OO 3.902E+OO FAIL ABUN RE-183 -4.310E-01 2.217E+OO 4.075E+OO NOT IDENT. RE-184 -3.087E+O'i 6.468E+Ol l.200E+02 NOT IDENT. W-188 -5.636E+Ol 2.052E+02 3.482E+02 FAIL ABUN IR-192 6.475E-01 9.149E-01 1. 773E+OO FAIL ABUN HG-203 -3.671E+OO 5.096E+OO 8.102E+OO NOT IDENT. BI-207 -7.355E-02 9.382E-02 l.605E-01 FAIL ABUN PB-211 -4.319E-01 1.037E+OO 1.910E+OO NOT IDENT. RN-219 -2.174E-01 6.073E-0'1 1.126E+OO NOT IDENT. RA-223 2.570E-01 1.012E+OO 2.007E+OO FAIL ABUN AC-227 l.942E-01 3.963E-01 6.999E-01 FAIL ABUN TH-227 l.942E-01 3. 963E-01 6.999E-01 FAIL ABUN TH-229 7.441E-01 7.895E-01 l.383E+OO FAIL ABUN TH-231 2.570E-01 1.012E+OO 2.007E+OO FAIL ABUN PA-233 2.688E-02 1.023E-01 2.033E-01 FAIL ABUN PA-234 1.555E-01 5.005E-01 l.059E+OO FAIL ABUN PA-234M
4.413E-01 7.927E+OO 1. 58 OE+Ol NOT IDENT. NP-237 2.688E-02 l.023E-01 2.033E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1. 391E-01 3.487E-01 6.601E-01 NOT IDENT. PU-239 0.000E+OO 6.651E+02 9.589E+02 FAIL ABUN AM-241 -1.079E-02 l.060E-01 1.953E-01 NOT IDENT. CM-243 1.828E-02 1.318E-01 2.457E-01 NOT IDENT. BK-247 1.855E-02 1.380E-01 2.460E-01 NOT IDENT. CM-247 -l.538E-02 5.768E-02 1.080E-01 NOT IDENT. CF-249 -8.217E-03 5.797E-02 1.112E-01 FAIL ABUN CF-251 -7.304E-02 2.008E-01 3.460E-01 NOT IDENT. ANH-511 -8.832E-02 9.035E-02 1. 794E-01 NOT IDENT. Page 4127of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:08:17.30 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 209 10.66.* 6.945E-01 l.865E+Ol 1. 865E+Ol 14.10 AS-73 53.44 11 10.30* 5.707E+OO 1.204E-01 l.699E+OO 471.25 NB-95M 235.69 9 24.80* 3.221E+OO 7.798E-02 2.158E+OO 152.26 CD-109 88.03 88 3.70* 5.391E+OO 2.930E+OO 4.645E+OO 39.40 SN-126 64.28 35 9.60 5.587E+OO 4.291E-01 4.291E-01 174.69 86.94 88 8.90 5.391E+OO 1.218E+00 1.218E+OO 39.40 87.57 88 37.00* 5.391E+OO 2.930E-01 2.930E-01 39.40 BA-137M 661.66 44 89.90* 1.340E+OO 2.395E-01 2.442E-01 59.17 CS-137 661. 66 44 85.10* 1.340E+OO 2.530E-01 2.580E-01 59.17 TL-208 277.37 ------6.60 2.816E+00 ------Line Not Found ------583.19 62 85.00* 1.486E+OO 3.237E-01 3.237E-01 46.76 860.56 10 12.50 1.083E+OO 4.936E-01 4.936E-01 184.06 PB-210 .46.54 52 4.25* 5.476E+OO 1.482E+OO l.521E+OO 122.39 BI-211 72. 87 ------1. 23 5.491E+OO ------Line Not Found ------351.06 203 12.92* 2.285E+00 4. 536E.+00 4.536E+OO 20.99 BI-212 727.33 30 6.67* 1. 241E+OO 2.367E+00 2.367E+OO 60.41 785.37 11 1.10 1.167E+OO 5.920E+OO 5.920E+OO 112. 83 1620.50 ------1. 47 6.312E-01 ------Line Not Found ------PB-212 74.82 169 10.28 5.476E+OO 1.986E+OO 1. 986E+OO 32.23 77 .11 265 17.10 5.460E+OO 1.877E+OO 1.877E+OO 18.80 238.63 327 43.60* 3.203E+OO l.549E+00 1. 549E+OO 13. 65 300.09 19 3.30 2.621E+OO 1.451E+OO 1. 451E+OO 144.54 BI-214 609.32 134 45.49* l.433E+OO 1. 361E+OO 1.361E+OO 23. 96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 l.453E+OO 1.453E+OO 46.87 PB-214 74.82 169 5.80 5.476E+OO 3.521E+OO 3.522E+OO 32.23 77 .11 265 9.70 5.460E+00 3.308E+OO 3.309E+00 18.80 87.09 88 3.41 5.391E+00 3.179E+OO 3.180E+OO 39.40 242.00 94 7.25 3.168E+OO 2.705E+OO 2.706E+OO 57.39 295.22 90 18.42 2.664E+OO 1.218E+OO 1.219E+OO 44.95 351.93 203 35.60* 2.285E+OO 1. 646E+OO 1. 647E+OO 20.99 RN-222 609.32 134 45.49* 1.433E+OO 1. 361E+OO 1.361E+OO 23. 96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 l.453E+OO 1.453E+OO 46.87 RA-224 240.99 94 4.10* 3.168E+OO 4.784E+OO 4.784E+OO 57.39 RA-226 609.32 134 45.49* 1.433E+OO 1.361E+OO l.361E+OO 23. 96 1120.29 ------*14. 92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 AC-228 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 60 .11. 27 2.364E+OO l.495E+OO l.495E+OO 57.51 794.95 12 4.25 1.155E+OO 1.669E+OO 1.669E+OO 97.08 835. 71 ------1. 61 1. llOE+OO ------Line Not Found ------911.20 55 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 968. 97 19 15.80 9.842E-01 8.136E-01 8 .136E-01 94.46 RA*-228 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 60 11. 27 2.364E+OO 1.495E+OO l.495E+OO 57.51 794.95 12 4.25 1.155E+OO 1.669E+OO l.669E+00 97.08 Page 4128of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn . %Eff pCi/GRAM pCi/GRAM %Error 835.71 ------1. 61 l.llOE+OO ------Line Not Found ------911.20 55 25.80* 1.035E+OO 1.359E+OO l.359E+OO 33.22 968. 97 19 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 TH-228 74.82 169 10.28 5.476E+OO 1. 986E+OO 1.986E+OO 32.23 77 .11 265 17.10 S.460E+OO 1.877E+OO 1.877E+OO 18.80 238.63 327 43.60* 3.203E+OO 1. 549E+OO 1. 549E+OO 13.65 300.09 19 3.30 2.621E+OO l.451E+OO l.451E+OO
144.54 TH-230 609.32 134 45.49* l.433E+OO 1.361E+OO 1.361E+OO 23.96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764 .. 49 20 15.30 5.810E-01 1.453E+OO l.453E+OO 46.87 PA-231 283.69 ------1. 70 2.761E+OO ------Line Not Found ------301.36 19 5.35* 2.621E+OO 8.948E-01 8.948E-01 144.54 TH-232 105.21 ------1.10 5. 215E+.oo ------Line Not Found ------338.32 60 11. 27 2.364E+OO l.495E+OO 1.495E+OO 57.51 835.71 ------1. 61 1.llOE+OO ------Line Not Found ------911.20 55 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 968.97 19 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 TH-234 63.29 35 3.70* 5.587E+OO 1.113E+OO 1.113E+OO 174.69 92.59 109 4.23 5.346E+OO 3.199E+OO 3.199E+OO U-234 609.32 134 45.49* l.433E+OO 1. 361E+OO l.361E+OO 23. 96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 1. 453E+OO 1.453E+OO 46.87 U-235 89.96 81 3.47 5.370E+OO 2.885E+OO 2.885E+OO 55.41 93.35 109 5.60 5.346E+OO 2.416E+OO 2.416E+OO 45.04 143.76 ------10.96* 4. 611E+OO ------Line Not Found ------163.33 ------5.08 4.273E+OO ------Line Not Found ------185.72 92 57.20 3.902E+OO 2.725E-01 2. 725E-01 45.34 205.31 ------5.01 3.621E+OO ------Line Not Found ------U-238 63.29 35 3.70* 5.587E+OO 1.113E+OO 1.113E+OO 174.69 92.59 109 4.23 5.346E+OO 3.199E+OO 3.199E+OO 45.04 AM-243 43.53 ------5.90 5.049E+OO ------Line Not Found ------74.66 169 67.20* 5.476E+OO 3.039E-01 3.039E-01 32.23 Flag: "*" Key line Page 4129 of 5809 Surrunary of Nuclide Activity Sample ID : G405235053 Page : 3 Acquisition date 3-0CT-2016 07:06:55 Total number of lines in spectrum 54 Number of unidentified lines 15 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 AS-73 NB-95M CD-109 SN-126 BA-137M CS-137* TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 Hlife l.25E+09Y 80.30D 64.03D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y 1. 41E+10Y l.41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y l.41E+l0Y l.41E+l0Y 1.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y .4. 47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y Decay 1. 00 14:1 27.7 1. 59 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.865E+Ol l.204E-01 7.798E-02 2.930E+OO 2.930E-01 2.395E-01 2.530E-01 3.237E-01 l.482E+OO 4.536E+OO 2.367E+00 1.549E+OO 1. 361E+OO l.646E+00 1. 361E+OO 4.784E+00 1. 361E+OO l.359E+00 1.359E+OO 1.361E+OO 8.948E-01 l.359E+OO 1.113E+OO 1.361E+OO 2. 725E-01 l .113E+OO 3.039E-01 5.538E+Ol 5.538E+Ol Decay Corr pCi/GRAM 1.865E+Ol l.699E+OO 2.158E+OO 4.645E+OO 2.930E-01 2.442E-01 2.580E-01 3.237E-01 1. 521E+OO 4.536E+OO 2.367E+OO 1.549E+OO 1. 3 61E+OO 1. 64 7E+OO 1. 361E+OO 4.784E+OO 1.361E+OO 1.359E+OO 1.359E+OO 1.549E+OO 1.361E+OO 8.948E-01 l.359E+OO i .113E+00 1.361E+OO 2. 725E-01 1.113E+OO 3.039E-01 6. 081E+Ol 6.081E+Ol 72. 22% Decay Corr _2-Sigma 2-Sigma Error %Error 0.263E+Ol 14.10 8.008E+OO 471.25 3.285E+OO 152.26 1.830E+OO 39.40 1.154E-01 39.40 1.445E-01 59.17 1.526E-01 59.17 1.513E-01 46.76 1.862E+OO 122.39 0.952E+OO 20.99 l.430E+00 60.41 0.211E+OO 13.65 0.326E+OO 23.96 0.346E+00 20.99 0.326E+OO 23.96 2.745E+OO 57.39 0.326E+OO 23.96 0.451E+00 33.22 0.451E+OO 33.22 0.211E+OO 13.65 0.326E+OO 23.96 12.93E-01 144.54 0.451E+OO 33.22 l.945E+00 174.69 0.326E+OO 23.96 1.236E-01 45.34 1.945E+OO 174.69 0.980E-01 32.23 Flags: "K" Keyline not found "E" = Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Page 4130of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235053 Acquisition date : 3-0CT-2016 07:06:55 It Energy Area Bkgnd FWHM Channel Left Pw cts/sec %Err %Eff Flags 0 34.92 36 170 0.67 69.51 68 6 9.25E-03 **** 1. 44E+OO 0 129.83 66 56 2.25 259.17 255 8 1. 7 6E-02 47.7 4.85E+OO T 0 192.13 19 37 0.95 383.69 381 5 5.14E-03 **** 3.81E+OO T 0 209.30 30 39 0.92 418.00 415 6 8.05E-03 77.3 3.57E+OO 0 213.16 6 62 0.75 425.72 422 7 1. 61E-03 **** 3.51E+OO 0 253 .16 ' 24 27 1. 27 505.66 503 7 6.63E-03 82.5 3.05E+00 T 0 317.48 11 20 1.17 634.21 631 6 3.15E-03 **** 2.50E+OO T 0 393.88 15 14 1. 55 786.91 784 6 4.26E-03 91. 5 2.07E+OO 0 417.46 32 41 0.77 834.03 827 14 8.89E-03 92.7 1.97E+OO 0 463.71 19 54 1. 02 926.48 920 12 5.39E-03 **** 1.80E+OO T 0 679.68 18 30 3.97 1358.14 1347 18 5.12E-03 **** 1.31E+OO 0 706.37 8 21 3.43 1411. 41 1404 12 2.41E-03 **** 1.27E+OO T 0 771.11 27 16 5.25 1540.88 1534 14 7.83E-03 77.2 1.18E+OO T 4 788.17 12 4 1. 43 1574.97 1566 12 3.49E-03 80.2 1.16E+OO 0 804.59 16 19 4.07 1607.78 1601 15 4. 71E-03 **** 1.14E+00 0 842.05 18 8. 1.27 1682.66 1676 10 5.06E-03 73.5 l. lOE+OO 0 866.61 15 2 2.09 1731. 76 1727 9 4.38E-03 60.9 1. 08E+OO 0 873.71 15 3 1. 95 1745.95 1740 10 4.24E-03 64.5 1. 07E+OO T 0 935.55 4 16 2.41 1869.56 1860 11 l.25E-03 **** 1. OlE+OO 0 964. 65 23 8 1. 57 1927.71 1921 11 6.68E-03 61. 5 9.88E-01 T 0 1093.35 11 2 1. 54 2184.98 2181 8 3. llE-03 73.7 8. 9.2E-01 T 0 1121. 84 17 20 1. 49 2241.92 2235 11 4.88E-03 **** 8.73E-01 T 0 1151.31 6 11 0.61 2300.83 2290 12 l.67E-03 **** ' 8.54E-01 0 1174.94 13 11 1. 53 2348.06 2342 12 3.86E-03 **** 8.40E-01 0 1239.26 44 4 0.68 2476.62 2468 18 1.30E-02 36.0 8.03E-01 T 0 1305.66 10 2 0.90 2609.36 2605 9 2.79E-03 82.3 7.67E-01 0 1580.37 8 0 0.83 3158.50 3155 8 2.22E-03 70.7 6.46E-01 Flags: "T" = Tentatively associated Page 4131 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:08:31.28 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l *
Acquisition date 3-0CT-2016 07:06:55 Sensitivity 3.000 *
Detector ID GAM31 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.45 Half life ratio : ***** *
Sample date 1-DEC-2015 14:24:00 Nuclide Library : SOLID *
Sample ID G405235053 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.1363E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 NB-95M CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 Le (pCi/GRAM 3.666E-01 4.568E+00 3.246E+00 1.093E+OO 6.890E-02 5.222E-02 5.517E-02 4.953E-02 7.476E-01 2.873E-01 7.039E-01 6.897E-02 1.107E-01 2.921E-01 1.107E-01 7.404E-01 1.107E:-01 1. 801E-01 1.801E-01 6.897E-02 1.106E-01 5.592E-01 l.801E-01 9.232E-01 l.106E-01 2.428E-01 9.232E-01 4. 711E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4132of5809 Le (pCi/GRAM 1. 921E+Ol 7.339E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-'103 RH-106 RU-106 AG-108M . AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM--:146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 4133of5809 4.579E-02 5.544E--:Ol O.OOOE+OO 0.000E+OO 1.081E-01 9.605E-01 O.OOOE+OO 5.928E-02 8.979E-01 l.378E+Ol 7.065E-02 2.892E-Ol 3.064E+OO O.OOOE+OO 3. 2 61E-01 O.OOOE+OO O.OOOE+OO 1.280E+OO 1.288E+Ol 1.463E+OO O.OOOE+OO 3.324E-01 9.379E+02 4.860E-02 1.610E+OO 2.554E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3. 8 62E-02 7. 831E-02 7.920E+OO 7.599E-01 7.599E-01 4.850E-02 1.173E-01 3.038E-01 O.OOOE+OO O.OOOE+OO 1.709E-01 4.185E+OO 1.744E-01 3.671E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 6.588E-02 0.000E+OO 8.793E-02 . 2.168E-01 O.OOOE+OO O.OOOE+OO 1.646E-01 O.OOOE+OO O.OOOE+OO 3.449E+Ol O.OOOE+OO 4. 722E-01 7.678E-02 6.688E+OO 7.439E-02 O.OOOE+OO 9.180E+02 O.OOOE+OO 3.925E-02 1.365E-01 l.910E-01 1. 793E-01 1.220E-01 2. 811E+OO 7.909E-02 9.400E+OO 2.956E-01 1.292E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT I DENT .. SHORT HLIF SHORT HLIF SHORT tILIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT.IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 RN-219 RA-223 AC-227 TH:...227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4134of5809 3 .133E-02 7.132E+OO 1. 691E+OO l.940E+00 5.091E+Ol l.567E+02 8.093E-01 3.673E+OO 6.693E-02 8.376E-01 4. 964E-Ol 9 .119E-01 3.185E-01 3.185E-01 6.377E-01 9 .119E-01 9.245E-02 4.553E-01 6.794E+OO 9.245E-02 O.OOOE+OO 3.075E-01 4.500E+02 9.318E-02 l.144E-01 1.128E-01 4.788E-02 4. 911E-02 l.601E-01 8.431E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:08:37.00 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l * *Acquisition date 3-0CT-2016 07:06:55 Sensitivity : 3.000 , *
Detector ID GAM31 Energy tolerance: 1.500 *
Elapsed live time: o* 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:06.45 . Half life ratio : ***** *
Sample date 1-DEC-2015 14:24:00 Nuclide Library : SOLID *
Sample ID G405235053 Analyst initials: MXRl
t Batch Number 1596252 Sample Quantity : 1.1363E+02 GRAM *
Quantity Err(%): 1.7601E-03 % * *Wet wt corr 1.00000 *Wet Weight 0.00000-*
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 9 6-sigma) ( 1. 96-sigma) K-40 1.865E+Ol 2.755E+OO 2.755E+OO AS-73 1.699E+OO 7.856E+OO 7.856E+OO NB-95M 2.158E+OO 3.224E+OO 3.224E+OO CD-109 2.865E+OO 1.984E+OO 1. 984E+OO SN-126 1.807E-01 1.248E-01 1. 248E-01 BA-137M 2.442E-01 1.420E-01 1.420E-01 CS-137 2.580E-01 1. 500E-01 1.500E-01 TL-208 3.237E-01 1. LJ89E-01 1. 489E-01 PB-210 1. 521E+OO l.830E+OO 1.830E+OO BI-211 1.179E+OO 1. 761E+OO 1. 761E+OO BI-212 2.367E+OO 1.407E+OO 1.407E+00 PB-212 1.549E+OO 2.228E-01 2.228E-01 BI-214 1. 361E+OO 3.249E-01 3.249E-01 PB-214 1.647E+OO 3.456E-01 3.456E-01 RN-222 1. 361E+OO 3.249E-01 3.249E-01 RA-224 2.630E+OO 2.860E+OO 2.860E+OO RA-226 1.361E+OO 3.249E-01 3.249E-01 AC-228 1. 359E+OO 4.479E-01 4.479E-01 RA-228 1. 359E+OO 4.479E-01 4.479E-01 TH-228 1. 549E+OO 2.228E-01 2.228E-01 TH-230 1. 361E+OO 3.248E-01 3.248E-01 PA-231 8.948E-01 1.282E+OO 1. 282E+OO TH-232 1.359E+OO 4.479E-01 4.479E-01 TH-234 1.113E+OO l.922E+OO 1.922E+OO U-234 1. 361E+oo 3.248E-01 3.248E-01 U-235 l .112E-01 2.857E-01 2.857E-01 U-238 l .113E+OO 1.922E+OO 1.922E+OO AM-243 1. 987E:....01 1.081E-01 1.081E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.162E+Ol 2.455E+Ol 2.510E+Ol NOT IDENT. NA-22 -4.217E-02. 9.697E-02 9.881E-02 NOT IDENT. Page 4135 of 5809 NA-24 -l.OOOE+41 2.992E+41 O.OOOE+OO SHORT HLIF AL-26 -8.769E-03 5.685E-02 5.698E-02 NOT IDENT. SC-46 8.840E-02 6.221E-01 6.234E-01 FAIL ABUN V-48 1. 42 8E+04 3.686E+04 3.741E+04 SHORT HLIF CR-51 -2.080E+Ol 8.926E+02 8.926E+02 SHORT HLIF MN-54 -2. 729E-02 1.379E-01 l.384E-01 NOT IDENT. C0-56 6.006E-01 1.077E+OO 1. lllE+OO FAIL ABUN MN-56 l.000E+41 1.814E+41 0.000E+OO SHORT HLIF C0-57 3.881E-02 6.603E-02 6.831E-02 NOT IDENT. C0-58 6 .132E-02 1.226E+OO l.226E+OO NOT IDENT. FE-59 3.195E+OO 1.567E+Ol l.573E+Ol NOT IDENT. C0-60 -4.484E-03 8.580E-02 8.582E-02 NOT IDENT. ZN-65 1. 647E-01 3.409E-01 3.489E-01 NOT IDENT. GE-68 -2.607E-01 3.669E+OO 3. 671E+OO NOT IDENT. AS-74 -6.317E+03 l.474E+04 1. 501E+o4 SHORT HLIF SE-75 -l.205E-01 4.215E-01 4.249E-01 NOT IDENT. BR-77 2.065E+39 -l.828E+40 0.000E+OO SHORT HLIF SR-82 5.037E+Ol 1. 813E+03 l.813E+03 SHORT HLIF RB-83 1. 675E+OO 1.292E+OO 1.497E+OO . NOT IDENT. KR-85 -3.053E+Ol 1.861E+Ol 2.315E+Ol NOT IDENT. SR-85 -3.468E+OO 2 .114E+OO 2.629E+OO NOT IDENT. RB-86 -2.194E+04 5.854E+04 5.937E+04 SHORT HLIF Y-88 l.564E-01 *3.226E-01 3.302E-01 NOT IDENT. Y-91 1.363E+02 1.088E+03 1.089E+03 NOT IDENT. NB-94 -7.107E-03 6.854E-02 6.861E-02 NOT IDENT. NB-95 3.041E-03 2.217E+OO 2.217E+OO NOT IDENT. ZR-95 2.419E-01 3.079E+00 3.081E+OO NOT IDENT. NB-97 1.000E+41 1. 929E+41 0.000E+OO SHORT HLIF ZR-97 -1.000E+41 1.550E+41 O.OOOE+OO SHORT HLIF M0-99 *2 .120E+33 2.090E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 1.147E+41 O.OOOE+OO SHORT HLIF RH-101 -1.496E-02 5.126E-02 5.171E-02 NOT IDENT. RH-102 -9.265E-04 9.445E-02 9.445E-02 NOT IDENT. RU-103 -1.245E+OO 9.576E+OO 9.592E+OO FAIL ABUN RH-106 2.162E-01 8. 728E-01 8.782E-01 NOT IDENT. RU-106 2.162E-01 8.728E-01 . 8.782E-01 NOT IDENT. AG-108M 7.238E-03 5.566E-02 5.576E-02 NOT IDENT. AG-llOM 2.637E-03 1.349E-01 l.349E-01 FAIL ABUN SN-113 -1.369E-01 4.188E-01 4.233E-01 NOT IDENT. CD-115 -6.488E+39 4.226E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -6. 911E+04 2.120E+05 2.143E+05 SHORT HLIF TE-123M -2.899E-02 2.079E-01 2.083E-01 NOT IDENT. SB-124 -l.536E-01 5 .196E+OO 5 .1-96E+OO NOT IDENT. SB-125 3.211E-02 1.991E-01 l.997E-01 FAIL ABUN TE-125M 3.297E+Ol 4.267E+02 4.269E+02 NOT IDENT. I-126 l.095E+06 2.097E+06 2.154E+06 SHORT HLIF SB-126 1.263E+06 2.894E+06 2.949E+06 SHORT HLIF SB-127 4.091E+22 1.595E+23 O.OOOE+OO SHORT HLIF I-131 7.012E+09 -1.572E+10 l.604E+l0 SHORT HLIF I-132 -1.000E+41 l.920E+42 O.OOOE+OO SHORT HLIF TE-132 1.453E+27 2.870E+27 O.OOOE+OO SHORT HLIF BA-133 6.087E-03 8.316E-02 8.321E-02 NOT IDENT. I-133 -1.000E+41 3.567E+41 O.OOOE+OO SHORT HLIF CS-134 l.099E-01 1. 047E-01 l.158E-01 FAIL ABUN CS-135 1.598E-02 2.682E-01 2.683E-01 NOT IDENT. I-135 -1.000E+41 7.508E+41 O.OOOE+OO SHORT HLIF CS-136 -8.042E+02 7.328E+05 7.328E+05 SHORT HLIF CE-139 1.094E-01 l.882E-01 l.945E-01 NOT IDENT. BA-140 -1.774E+06 3.404E+06 3.497E+06 SHORT HLIF LA-140 L2.828E+05 1.283E+06 l.290E+06 SHORT HLIF CE-141 -1.163E+Ol 4.342E+Ol 4.374E+Ol NOT IDENT. CE-143 1.000E+41 4.432E+41 O.OOOE+OO SHORT HLIF CE-144 3.845E-01 5.592E-01 5.854E-01 NOT IDENT. PM-144 -4.117E-03 9.409E-02 9.411E-02 NOT IDENT. PR-144 -2.133E+00 8.554E+OO 8.608E+OO NOT IDENT. PM-146 6.430E-02 7.843E-02 8.362E-02* NOT IDENT. ND-147 2. 814E+07 6. 964E+07 7*. 079E+07 SHORT HLIF PM-147 -1.987E+02 l.102E+03 l.105E+03 NOT IDENT. PM-149 7.516E+40 6.692E+41 O.OOOE+OO SHORT HLIF EU-150 3.877E-03 4.925E-02 4.928E-02 FAIL ABUN EU-152 8.353E-02 1. 596E-01 l.640E-01 FAIL ABUN GD-153 -2. 851E-02 2.426E-01 2.430E-01 NOT IDENT. EU-154 -1.030E-01 2.369E-01 2.414E-01 FAIL ABUN EU-155 -4.819E-02 1.468E-01 l.484E-01 FAIL ABUN TB-160 -3.728E-01 3.322E+OO 3.326E+OO FAIL ABUN H0-166M -5.595E-02 1.134E-01 l.162E-01 NOT IDENT. TM-171 3.572E+OO l.650E+Ol l.658E+Ol ,FAIL ABUN HF-172 l.564E-01 3.599E-01 3.667E-01 FAIL ABUN Page 4136of5809 LU-172 l.714E-01 l.250E-01 1. 469E-01 FAIL ABUN LU-176 -2.145E-02 3.822E-02 3.942E-02 FAIL ABUN HF-181 4.405E-03 8.388E+OO 8.388E+OO NOT IDENT. TA-182 6.625E-01 1. 889E+OO 1.912E+OO FAIL ABUN RE-183 -4.310E-01 2.218E+OO 2.227E+OO NOT IDENT. RE-184 -3.087E+Ol 6.512E+Ol 6.659E+Ol NOT IDENT. W-188 -5.636E+Ol 2.053E+02 2.069E+02 FAIL ABUN IR-192 6.475E-01 9.153E-01 9.607E-01 FAIL ABUN HG-203 -3.671E+OO 5.099E+OO 5.361E+OO NOT IDENT. BI-207 -7.355E-02 9.386E-02 9.955E-02 FAIL ABUN PB-211 -4.319E-01 1.037E+OO 1. 056E+OO NOT IDENT. RN-219 -2.174E-01 6.079E-01 6.158E-01 NOT IDENT. RA-223 2.570E-01 1.012E+OO 1.019E+OO FAIL ABUN AC-227 1.942E-01 3. 972E-01 4.067E-01 FAIL ABUN TH-227 l.942E-01 3.972E-01 4.067E-01 FAIL ABUN TH-229 7. 441E-01 7.903E-Ol 8.586E-01 FAIL ABUN TH-231 2.570E-01 1.012E+OO 1.019E+OO FAIL ABUN PA-233 2.688E-02 l.023E-01 l.030E-01 FAIL ABUN PA-234 1.555E-01 5.312E-01 5.358E-01 FAIL ABUN PA-234M 4. 413E-01 7.927E+OO 7.930E+OO NOT IDENT. NP-237 2.688E-02 1.023E-01 1.030E-01 FAIL ABUN NP-238 1. OOOE+41-3.104E+41 O.OOOE+OO SHORT HLIF NP-239 1. 391E-01 3.488E-01 3.544E-01 NOT IDENT. PU-239 1.423E+03 6.681E+02 9.263E+02 FAIL ABUN AM-241 -1. 07 9E-02 1.060E-01 1.062E-01 NOT IDENT. CM-243 1. 828E-02' l.318E-01 l.321E-01 NOT IDENT. BK-247 1.855E-02 1. 381E-01 1.383E-01 NOT IDENT. CM-247 -l.538E-02 5.773E-02 5.815E-02 NOT IDENT. CF-249 -8.217E-03 5.798E-02 5.809E-02 FAIL ABUN CF-251 -7.304E-02 2.0lOE-01 2.037E-01 NOT IDENT. ANH-511 -8.832E-02 9.043E-02 9.880E-02 NOT IDENT. Page 4137of5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 100.7624 87.09 76.5680 136.47 61.9439 45.60 115.4579 87.57 76.6492 140.51. 0.0000 46.54 115.8266 88.03 76.7267 143.76 49.9167 49.72 0.0000 88.34 76.7792 144.24 45.7026 51. 35 110.3970 88.47 76.8005 145.44 52.1761 51. 87 122.2180 89. 96 77.0502 152.43 44.1212 52.39 136.4078 1093.63 77.1631 153.25 0.0000 52.97 145.4134 91.11 0.0000 323.87 58.2641 53.44 145.6249 92.59 77.4847 156.02 o.oboo 54.07 140.6323 93.35 77.6093 158.56 0.0000 57.36 0.0000 94.56 59.6516 159.00 47.8068 57.53 137.6566 94.65 59.6628 162.33 44.7599 57.98 137.8370 94.67 59.6651 162.66 0.0000 59.27 152.6341 94.87 59.6904 163.33 53.5698 *59*. 32 152.6557 97.43 62.6152 165.86 46.0804 59.54 146.4992 98.43 57.8414 176.31 51.1948 60. 96 148.2875 98.44 57. 8.423 176.60 0.0000 61.17 148.3752 99.53 59.9352 177.52 59.0799 62.93 147.0000 100 .11 55.0865 181.07 0.0000 63.29 147.1464 102.03. 57.2725 181.52 52.2956 63.58 147.2633 103.18 58.3923 184.41 42.7436 64.28 125.5188 103.37 58.4144 143.76 42.8161 66.73 134.8522 *105. 21 64.5859 193.51 57.6541 67.24 134.1216 105.31 64.5983 197.03 57.1442 125.81 117.8353 106.12 54.7457 198.01 50.3473 67.75 117.8560 106.47 65.7392 201.83 41.3855 69.67 117.5293 109.28 63.0875 203.43 42.6170 70.83 147.3474 111. 00 60.2774 205.31 38.0953 72.81 119.7028 111.76 0.0000 210.85 32.5356 72. 87 119.7206 114. 06 59.6090 215.65 40.5076 74.66 121.8031 116. 30 0.0000 222.11 35.3133 74.82 121. 8500 116.74 53.8079 227.09 42.6121 74.97 121.8950 119.76 58.1816 227.38 39.0732 77 .11 122.5297 121.12 48.0894 228.16 0.0000 78.74 83.8829 121. 22 48.0976 228.18 31. 9974 79.69 90.3457 121.78 45. 0719 116.74 31.9974 80.12 67.8274 122.06 43.0440 235.69 36.6413 80.19 0.0000 122.92 50.2935 235. 96 36.6520 80.57 76.7005 123.07 55.4399 238.63 38.3550 81. 00 83.0707 265.00-59.6094 238.98 0.0000 81. 07 84.9724 125.81 49.5125 240.99 38.4512 81. 75 83.2150 127.23 53.7680 242.00 38.4922 83.79 69.6704 127.91 51.0696 244.70 35.3848 84.00 65.9019 129.30 50.8430 252.40 0.0000 85.43 94.0861 131.20 38.8600 252.80 26.7618 86.55 76.4764 133.02 41.7609 254.15 0.0000 86.79 76.5167 133.52 43.1882 256.23 26.0413 86.94 76.5430 136.00 56.6516 260.90 0.0000 Page 4138of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 43.0856 355.39 0 .. 0000 584.27 16.4596 264.80 43.0910 356.01 30.6746 595.83 0.0000 265.00 38.1739 364.49 0.0000 427.87 25.9389 268.22 40.7656 366.42 0.0000 602.52 0.0000 269.46 27.2100 372. 51 18.9103 . 604. 72 18.7156 270.03 32.1747 375.05 24.3600 607.14 26.5469 271.23 43.3623 377.52 22.5978 609.32 21. 8870 273.65 0.0000 356.01 25.4285 610.33 21.8981 276.40 26.1468 388.16 20.9542 614.28 12.5386 277.37 27.4174 388.63 0.0000 618.01 15.7025 277.60 27.4235 391.69 Zl. 9219 620. 36 14.6733 278.00 14. 9641 264.66 22.0645 621.93 12.5869 279.20 44.9429 401.81 23.0026 630.19 0.0000 279.54 46.2060 402.40 23.9328 631.29 11. 5922 279.70 46.2127 404.85 22.1304 633.25 8.4388 280.46 29.9978 410.95 21.1143 634.78 0.0000 283.69 31. 7 602 413.71. 30.6193 635.95 12.6753 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 30 .. 97 41 423.72 0.0000 645.85 10.6144. 285.90 0.0000 427.09 21.5382 657.76 12.8110 287.50 31. 8731 427.87 25.2977 657.90 0.0000 290.67 31.5460 433.94 27.2831 661.66 16.0437 293.27 0.0000 439.40 19.8289 664.57 0.0000 351. 93 29.1431 453.88' 16.2052 666.33 0.0000 295.96 29.1627 463.37 22.0590 666.50 0.0000 879.38 20.3350 .468.07 25. 9728 667.71 0.0000 299.98 29.2680 473.00 0.0000 677.62 12.9321 300.09 29.2708 475.06 19.3237 685.70 0.0000 300 .13 29.2722 476.78 20.3117 695.00 0.0000 301.36 25.4822 477.60 22.2574 696. 49 13.0459 302.85 33.1705 482.18 18.4391 696. 51 15.2202 256.23 25.5533 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.1383 306.78 31.5793 497.08 13. 7106 697.49 14.1394 308.46 29.9165 505.52 29.5288 702.65 16.3531 311. 90 30.0062 507.63 0.0000 706.68 14.1992 316.51 29.6955 511. 00 33.5746 711. 68 16.4203 319.41 0.0000 514.00 63.3125 720.70 0.0000 320.08 0.0000 514.00 63.3125 721.93 0.0000 321.04 27. 9967 520.40 10.9226 722. 78 13.2017 323.87 29.4498 520.69 0.0000 722.91 13.2026 325.23 39.0216 522.65 0.0000 723.31 14.8557 328.76 0.0000 527.90 0.0000 724 .19 14.8612 333.37 28.2874 528.26 13.9647 727.33 14.3309 333.97 31. 4458 529.59 13.9749 733.00 3.3154 334.37 28.8347 529.87 0.0000 735.93 16.5985 338.28 21. 9147 531. 02 0.0000 333.97 21.0387 338.32 21.9152 537.26 0.0000 739.50 0.0000 311. 90 21. 9538 546.56 0.0000 747.24 11.1202 340.48 21.9538 552.55 17.1909 748.06 12.2367 340.55 0.0000 563.25 19.3263 752.31 12.2591 344.28 19.8193 569.33 24.4932 753.82 0.0000 345.93 27.3432 946.00 24.4951 756.73 14 *. 5155 351.06 30 .1118 569.70 24.4980 756.80 14.5160 351.93 30 .1325 583.19 16.4505 884.68 17.9206 Page 4139of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.1768 1274.44 12.8452 1620.50 2.1782 766.42 25.2274 1001.03 11. 0277 1621. 92 2.1790 766.84 26.9141 1002.74 12.8734 1678.03 0.0000 772.60 0.0000 1004.73 7.3611 1690.97 5.5310 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.0000 778.90 14.6525 1028.54 0.0000 1063.66 9.9000 783.70 0.0000 1037.84 8.3732 1771.35 3.6010 785.37 14.6922 1038.76 0.0000 1791.20 0.0000 792.07 6.7998 631.29 6.5313 1808.65 3.6287 794.95 6.8079 1048.07 0.0000 1810.72 0.0000 795.86 6.8105 1049.04 11.2053 1836 .. 06 0.9123 810.06 10.2751 1050.41 13.0789 810.29 6.8506 1063.66 15.9500 344.28 6. 8511 1077.00 0.0000 810 .. 76 10.2781 1077.34 7.5391 815.77 0.0000 1085.87 4.7247 1048.07 0.0000 1093.63 4.5469 832.01 10.3656 1099.45 12.3367 834.85 14.9895 1112. 07 12.3851 835.71 12.4572 1112.84 13.3412 836.80 0.0000 1115. 54 7.6299 846.75 0.0000 1120.29 11.4617 846.77 12.7429 1120.55 11. 4631 856.80 0.0000 1221.41 11.4653 860.56 6.9880 1129. 67 6.7056 871.09 3.5082 1131.51 0.0000 873.19 8.7775 1147.95 0.0000 875.33 0.0000 1173.23 13. 9764 879.38 10.5575 1177.95 6.2203 880.51 11. 4424 1189.05 13. 6522 883.24 9.6918 1204.77 10.7758 884.68 6.1709 1221.41 10.8275 889.28 7.9478 1231.02 11. 2807 894.76 9.7338 1235.36 0.0000 898.04 10.6318 1238.28 12.8580 900. 72. 8.8687 1260.41 0.0000 903.28 15.0908 1271. 87 15.9756 911.20 9.7932 1274.44 12.9889 912.08 9. 7965 1274.54 12.9897 923.98 0.0000 1291.59 13.0508 926.50 7.1624 1298.22 0.0000 929 .11 7.1689 1312.11 0.0000 937.49 8.6288 1332.49 10.1501 944.13 0.0000 1362.66 0.0000 946.00 9 .. 9174 1365 .19 4.0952 949.00 9.0253 1368.63 0.0000 667.71 0.0000' 1384.29 4 .1157 962.31 4.3526 1408.01 6.2109 964.08 10.1623 1457.56 0.0000 966.17 14.5283 1460.82 3.1469 911.20 14.5425 1489.16 1. 0562 968. 97 14.5425 1505.03 5.3015 983.53 0.0000 1584.12 8. 6411 984.45 0.0000 1596.21 0.0000 Page 4140 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:09:08.68 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM43.CNF;151 Background date : Z-OCT-2016 11:02:23. Sample date 2-DEC-2015 14:51:00. Acquisition date : 3-0CT-2016 07:07:21. Sample ID G405235054 Sample quantity 1.46461E+02 GRAM Detector name : GAM43 , Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.68 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 1 0 5 5 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 Page 4141 of 5809 Energy 59.35 74.65 76.99 80.99 86.94 89.52 92.80* 114. 29 129. 76 143.95* 185.66* 208.40 219.04 238.49* 241.58 295.04* 320.25 338.38 351.85* 382.39 409.10 441. 72 464.44 511. 23* 566.62 582.95* 609.22* 722 .*93 726.85 767.75 774.19 833.02 884.64 888.09 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 33 136 191 35 50 43 102 31 28 13 107 52 41 425 122 142 25 86 240 38 36 21 19 16 7 117 150 12 44 27 19 6 15 4 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 103 132 110 89 103 64 .165 107 109 116 102 122 128 42 70 50 45 70 49 84 21 18 55 83 30 21 44 7 9 13 11 9 5 4 1. 50 1. 23 1.12 1.25 1. 04 1. 06 1. 76 2.27 1. 28 1. 38 1. 54 0.68 6.21 1. 03 1. 68 1. 24 0.65 1. 26 1.19 7'. 31 3.19 1.10 3.37 1. 42 1. 47 1. 55 1. 71 1. 22 2.06 1. 88 1. 77 0.72 0.85 0.58 118. 49 149.08 153.77 161.77 173.69 178.85 185.41 228.39 259.36 287.74 371.19 416.67 437.95 476.87 483.05 590.00 640.43 67 6. 71 703.65 764.75 818.17 883.43 928.88 1022.49 1133.29 1165. 95 1218.50 1445. 96 1453.81 1535.63 1548.50 1666.18 1769.43 1.776.34 115 141 141 141 171 177 177 225 253 283 365 412 429 469 469 585 634 670 698 748 813 880 920 1014 1126 1161 1210 1443 1449 1530 1543 1660 1765 1773 8 9.17E-03 55.9 24 3.77E-02 15.8 3:07E+OO 24 5.30E-02 12.2 24 9.67E-03 52.0 6 1. 39E-02 35. 0 16 1.20E-02 29.9 l.03E+OO l6_2.83E-02 27.3 9 8.52E-03 63.6 9 7.80E-03 70.3 9 3.63E-03153.0 12 2.96E-02 21.9 11 l.44E-02 43.5 15 l.12E-02 62.8 20 1.18E-01 5.5 1.31E+OO 20 3.40E-02 17.7 9 3.93E-02 12.4 12 7.0lE-03 56.8 14 2.40E-02 23.2 11 6.66E-02 8.7 21 1. 05E-02 62. 6 10 1.00E-02 29.5 8 5. 77E-03 41. 7 13 5.18E-03 85.3 14 4.47E-03134.7 10 l.94E-03151.2 13 3.25E-02 12.4 19 4.16E-02 13.4 6 3.23E-03 50.7 11 l.23E-02 19.6 10 7.62E-03 30.8 10 5.37E-03 40.5 8 1.58E-03103.8 9 4.03E-03 40.8 7 l.OlE-03103.7 Peak Search Report (continued) Page : 2 Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 890.84 9 1 0.95 1781.84 1779 6 2.42E-03 40.2 36 0 902.44 10 15 4.10 1805.04 1797 12 2.75E-03 84.5 37 0 910.91 98 4 1.79 1821.99 1814 17 2.71E-02 11.2 38 0 922.79 19 17 4.11 1845.74 1836 17 5. 41E-03 53.4 39 0 969. 69 39 41 0. 72 1939.57 1929 17 1.09E-02 42.6 40 0 1042.99 8 8 1.24 2086.17 2080 10 2.26E-03 78.8 41 0 1120. 95 39 26 1.27 2242 .11 2235 20 1.08E-02 35.4 42 0 1215.78 19 6 3.78 2431.79 2425 13 5.34E-03 35.3 43 0 1314.44 4 4 0.94 2629 .13 2623 8 l.llE-03100.0 44 0 1341.47 10 3 0.96 2683.18 2676 11 2.79E-03 45.2 45 0 1353.06 6 2 0.75 2706.35 2702 8 1. 63E-03 59.0 46 0 1460.66* 336 0 1. 99 2921.57 2914 18 9.33E-02 5.5 47 0 1764.57* 29 0 2.08 3529.38 3522 14 8.lOE-03 19.6 48 0 1847.26 12 0 2.31 3694.75 3690 10 3.33E-03 28.9 Flag: "*" = Peak area was modified by background subtraction Page 4142of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:09:10 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID Sample .type 2-DEC-2015 14:51:00 G405235054 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:07:21. 146.46 GRAM . Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA43 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Inte_rfering -Nuclide Page 4143of5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 86.94 87.57 "88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.68 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235054 Acquisition.date 3-0CT-2016 07:07:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.OOlE+OO 1.552E+Ol l.552E+Ol 11. 02 OK SC-46 889.28 99.98* 1.541E+OO l.220E-02 l.530E-01 207.36 OK 1120.55 99.99 l.265E+OO 1.561E-01 1. 957E+OO 70.74 OK CD-109 88.03 3.70* 4.275E+OO 9.991E-01 1.581E+OO 143.54 OK SN-126 64.28 9.60 l.983E+OO Line Not Found Absent 86.94 8.90 4.275E+OO 4.153E-01 4.153E-01 143.54 OK 87.57 37.00* 4.275E+OO 9.991E-02 9.991E-02 143.54 OK TL-208 277.37 6.60 4.205E+OO Line Not Found Absent 583.19 85.00* 2.199E+OO 3.376E-01 3.376E-01* 24.76 OK 860.56 12.50 1.582E+OO Line Not Found Absent BI-211 72. 87 1. 23 2. 941E+OO Line Not Found Absent 351. 06 12.92* 3.426E+00 1. 521E-02-1. 521E-026072 .10 OK PB-212 74.82 10.28 3.129E+OO 2.088E+OO 2.088E+00 41. 68 OK 77 .11 17.10 3.370E+OO 2.127E+OO 2.127E+00 24.49 OK 238.63 43.60* 4.741E+OO l.202E+00 1.202E+OO 11. 04 OK 300.09 3.30 3.935E+OO Line Not Found Absent BI-214 609.32 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26.88 OK 1120.29 14.92 l.265E+OO l . .046E+OO l.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 l.103E+00 1.103E+OO 39.19 OK PB-214 74.82 5.80 3.147E+OO Line Not Found <<INT Reject 77 .11 9.70 3.370E+OO 3.749E+OO 3.750E+00 24.49 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.992E+OO l.106E+00 1.106E+OO 24.81 OK 351. 93 35.60* 3.426E+OO Line Not Found* <<INT Reject RN-'222 609.32 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26. 88 OK 1120.29 14.92 1. 2 65E+OO 1.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 1.103E+OO 1.103E+00 39.19 OK RA-224 240.99 4.10* 4.695E+OO 1. 761E+OO 1. 761E+00 79.67 OK RA-226 609.32 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26.88 OK 1120.29 14.92 l.265E+OO 1.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 l.103E+OO 1.103E+00 39.19 OK AC-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 1.225E+OO 1.225E+OO 46.39 OK 794.95 4.25 1.691E+OO Line Not Found Absent 835.71 1. 61 1.621E+OO Line Not Found Absent 911.20 25.80* 1.508E+OO l.296E+OO 1.296E+00 22.47 OK 968. 97 15.80 1.431E+OO 8.914E-01 8.914E-01 85.15 OK RA-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11.27 3.546E+OO 1.225E+OO l.225E+OO 46.39 OK 794.95 4.25 1. 691E+OO Line Not Found Absent 835. 71 1. 61 1.621E+OO Line Not Found Absent 911. 20 25.80* l.508E+OO 1.296E+OO 1. 296E+OO 22.47 OK 968. 97 15.80 1. 431E+OO 8.914E-01 8.914E-01 85.15 OK TH-228* T4. 82 10.28 3.129E+OO 2.088E+OO 2.088E+OO 41. 68 OK 77 .11 17.10 3.370E+OO 2.127E+00 2.127E+OO 24.49 OK 238.63 43.60* 4.741E+OO 1.202E+OO 1. 202E+00 11. 04 OK 300.09 3.30 3.935E+OO Line Not Found Absent TH-230 609.32 45.49* 2 .118E+OO 8.347E-01 8.347E-01 26.88 OK Page 4144 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235054 _ Acquisition date 3-0CT-2016 07:07:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120. 29 14.92 1. 265E+OO 1.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8 . .362E-01 1.103E+OO 1.103E+OO 39.19 OK TH-232 105.21 1.10 5. 396E+00 Line Not Found Absent 338.32 11. 27 3.546E+OO 1.225E+OO 1.225E+OO 46.39 OK 835. 71 1. 61 1.621E+OO Line Not Found Absent 911.20 25.80* 1.508E+00 1.296E+OO 1.296E+OO 22.47 OK 968. 97 15.80 1.431E+OO 8.914E-01 8.914E-01 85.15 OK U-234 609.32 45.49* 2 .118E+OO 8.347E-01 8.347,E-01 26.88 OK 1120.29 14.92 1.265E+OO 1.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 OK U-235 89. 96 3.47 4.476E+OO 1.770E+OO 1.770E+OO 59.83 OK 93.35 5.60 4.711E+00 2.441E+OO 2.441E+OO 54.61 OK 143.76 .10. 96* 6.023E+OO 1.209E-01 1.209E-01 306.07 OK 163.33 5.08 5.876E+OO Line Not Found Absent 185.72 57.20 5.570E+OO 1.999E-01 1.999E-01 43. 72 OK 205.31 5.01 5.260E+OO Line Not Found Absent AM-241 59.54 35.90* 1.428E+OO .4.218E-01 4.223E-01 111.73 OK AM-243 43.53 5.90 1.216E-01 Line Not Found Absent 74.66 67.20* 3.1'29E+OO 3.195E-01 3.195E-01 41. 68 OK ANH-511 511. 00 100.00* 2.464E+OO 3.567E-02 3.567E-02 269.31 OK Flag: "*" = Keyline Page 4145 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:09:11.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l *
Acquisition date 3-0CT-2016 07:07:21 Sensitivity : 3.000 * *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed. live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : *
Sample date 2-DEC-2015 14:51:00 Analyst initials: MXRl *
Sample ID G405235054 Sample Quantity 1.4646E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * * *' Eff. Cal. date 6-SEP-2016 07: 25: 20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.552E+Ol 1.677E+OO 5.157E-01 SC-46 l.530E-01 3.108E-01 1.152E-01 CD-109 1.581E+OO 2.224E+OO 2.332E+OO SN-126 9. 9°91E-02 l.405E-01 1. 485E-01 TL-208 3.376E-01 8 .191E-02 7. 719E-02 BI-211 1.521E-02 9.053E-01 3.806E-01 PB-212 1.202E+OO l.300E-01 9. 611E-02 BI-214 8.350E-01 2.200E-01 1. 211E-01 PB-214 1.112E+OO 1.888E-01 3.461E-01 RN-222 8.350E-01 2.200E-01 1. 211E-01 RA-224 1. 761E+OO 1.375E+OO 1.031E+OO RA-226 8.350E-01 2.200E-01 1. 211E-01 AC-228* 1. 296E+OO 2.854E-01 2.273E-01 RA-228 l.296E+OO 2.854E-01 2.273E-01 TH-228 1.202E+OO 1.300E-01 9.611E-02 TH-230 8.347E-01 2.199E-01 1.210E-01 TH-232 1. 296E+00 2.854E-01 2.273E-01 U-234 8.347E-01 2.199E-01 l.210E-01 U-235 l.209E-01 3.628E-01 3.434E-01 AM-241 4.223E-01 4.624E-01 4.211E-01 AM-243 3.195E-01 l.305E-01 l.225E-01 ANH-511 3.567E-02. 9.414E-02 6.666E-02 Non-Identified Key-Line. Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -4.0lOE+OO 1.522E+Ol 2.731E+Ol NOT IDENT. NA-22 . 1. 351E-02 4.553E-02 9.890E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -7.073E-04 2.539E-02 5.852E-02 NOT IDENT. V-48 O.OOOE+OO l.636E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 9.109E+02 O.OOOE+OO SHORT HLIF MN-54 -5.347E-02 8.349E-02 l.217E-01 NOT IDENT. C0-56 5. 34.6E-02* 4.945E-01 9. 964E-01 NOT IDENT. Page 4146 of 5809 MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 l.423E-02 5.200E-02 9.678E-02 NOT IDENT. C0-58 -3.193E-01 6.514E-01 1.179E+OO NOT, I DENT. FE-59 -6. 345E-,01 9.474E+OO 1. 774E+Ol NOT IDENT. C0-60 9.919E-03 3. 967E-02 8.633E-02 NOT IDENT. ZN-65 -1.844E-01 2.496E-01 3.338E-01 NOT IDENT. GE-68 1. 968E+OO 2.654E+OO 5.774E+OO NOT IDENT. AS-73 5.872E+OO 1.930E+Ol 3.759E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.773E+03 O.OOOE+OO SHORT HLIF SE-75 -1.202E-01 2.122E-01 3.855E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 288E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1. 04 7E+03 O.OOOE+OO SHORT HLIF RB--83 4.129E-01 7.755E-01 1.622E+OO NOT IDENT. KR-85 6.607E+OO 9.456E+OO 1.703E+Ol NOT IDENT. SR-85 7.420E-01 1.062E+OO l.914E+OO NOT IDENT. RB-86 O.OOOE+OO 3.808E+04 O.OOOE+OO SHORT HLIF Y-88 l.067E-01 2.734E-01 6.370E-01 NOT IDENT. Y-91 -1. 996E+02 5.378E+02 l.028E+03 NOT IDENT. NB-94 4. 359E-02* 3.490E-02 7.821E-02 NOT IDENT. NB-95 3.122E-01 1.190E+OO 2 .113E+OO NOT IDENT. NB-95M -7. 960E-01 2.917E+OO 4. 8 60E+OO NOT IDENT. ZR-95 -5.800E-01 l.550E+00 2.888E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 960E+4'1 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.257E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.173E-02 4.177E-02 6. 511E-02 NOT IDENT. RH-102 3.239E-02 6.329E-02 l.334E-01 FAIL ABUN RU-103 8.324E-:-Ol 6.924E+OO l.314E+Ol FAIL ABUN RH-106 3.598E-02 5.063E-01 l.020E+OO NOT IDENT. RU-106 3.598E-02 5.063E-01 l.020E+OO NOT IDENT. AG-108M l.463E-03 2.826E-02 5.371E-02 FAIL ABUN AG-llOM l.566E-01 l.253E-01 2.549E-01 FAIL ABUN SN-113 4.918E-02 2.585E-01 4. 966E-01 NOT IDENT. CD-115 O.OOOE+OO 2.199E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1. 400E+05 O.OOOE+OO SHORT HLIF TE-123M 2.600E-02 l.429E-01 2.836E-01 NOT IDENT. SB-124 9.314E-03 2.371E+OO 5.094E+OO FAIL ABUN SB-125 1.178E-01 l.121E-01 2.364E-01 FAIL ABUN TE-125M -6.842E+Ol 3.182E+02 5.709E+02 NOT IDENT. I-126 O.OOOE+OO l.380E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.031E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.976E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.918E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.444E+27 0.000E+OO SHORT HLIF BA-133 -1. 789E-02 4.913E-02 7.821E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.433E-02 5.312E-02 l.134E-01 NOT IDENT. CS-135 -2.465E-02 l.432E-01 2. 696E-01 NOT IDENT. I-135 0.000Et00 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 5.068E+05 O.OOOE+OO SHORT HLIF BA-137M -4.439E-03 4.073E-02 7.821E-02 NOT IDENT. CS-137 -4.689E-03 4.303E-02 8.262E-02 NOT IDENT. CE-139 5.433E-02 1.184E-01 2.388E-01 NOT IDENT. BA-140 O.OOOE+OO l.973E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.045E+05 O.OOOE+OO SHORT HLIF CE-141 l.859E+Ol 5.575E+Ol 5.063E+Ol FAIL ABUN CE-143 O.OOOE+OO 6.699E+40 O.OOOE+OO SHORT HLIF CE-144 -8.299E-02 3.789E-01 7.097E-01 FAIL ABUN PM-144 2.420E-02 5.510E-02 l.158E-01 NOT IDENT. PR-144 2.108E+OO 4.801E+OO l.009E+Ol NOT IDENT. PM-146 4.022E-02 4.464E-02 9.503E-02 NOT IDENT. ND-147 O.OOOE+OO 5.542E+07 O.OOOE+OO SHORT HLIF PM-147 6.992E+02 8.977E+02 1. 744E+03 NOT IDENT. PM-149 O.OOOE+OO l.102E+41 O.OOOE+OO SHORT HLIF EU-150 3 .134E-04 2.641E-02 4.519E-02 FAIL ABUN EU-152 -5.728E-02 l.164E-01 1. 821E-01 NOT IDENT. GD-153 -l.661E-01 2.432E-01 3.825E-01 NOT IDENT. EU-154 3.504E-02 1.118E-01 2.432E-01 FAIL ABUN EU-155 l.012E-01 1.353E-01 2.607E-01 FAIL ABUN TB-160 5.072E-01 2.464E+OO 4.417E+OO .FAIL ABUN
H0-166M 3.067E-02 6.914E-02 l.410E-01 FAIL ABUN TM-171 -3.926E+Ol 4.874E+Ol 8.606E+Ol NOT IDENT. HF-172 6.398E-02 2.869E-01 4.864E-01 FAIL ABUN LU-172 -l.178E-01 9.316E-02 l.330E-01 FAIL ABUN LU-176 7.663E-03 2.368E-02 4.686E-02 FAIL ABUN HF-181 -;l.270E-01 5.104E+OO 9.522E+OO NOT IDENT. Page 4147of5809 TA-182 6.423E-01 1. 097E+OO 2.182E+OO FAIL ABUN RE-183 9. llOE+OO 9.974E+00 1.0lOE+Ol FAIL ABUN RE-184 3.519E+Ol 5.828E+Ol 8. 691E+Ol FAIL ABUN W-188 2.453E+Ol l.430E+02 2.479E+02 NOT IDENT. IR-192 -4.296E-01 6.059E-01 9.246E-01 FAIL ABUN HG-203 -2.098E+OO 2.797E+OO 4.952E+OO NOT IDENT. BI-207 -2.219E-02 5.014E-02 8. 911E-02 FAIL ABUN PB-210 2.532E+OO 1.049E+Ol 2.072E+Ol NOT IDENT. PB-211 -1.013E+OO 7.892E-01 1.006E+OO FAIL ABUN BI-212 O.OOOE+OO 7.412E-01 l.514E+OO FAIL ABUN RN-219 2.876E-01 3. 7 62E-01 7.780E-01 NOT IDENT. RA-223 -1.866E-01 6.284E-01 l.025E+OO FAIL ABUN AC-227 -5.008E-02 2.225E-01 4.193E-01 FAIL ABUN TH-227 -5.008E-02 2.225E-01 4.193E-01 FAIL ABUN TH-229 1.847E-01 4.558E-01 9.137E-01 FAIL ABUN PA-231 3.344E-01 4.556E-01 9.238E-01 NOT IDENT. TH-231 -1.866E-01 6.284E-01 1.025E+OO FAIL ABUN PA-233 -1.938E-02 6.151E-02 l .132E-01 NOT IDENT. PA-234 -l.068E-01 3.195E-01 5.832E-01 FAIL ABUN PA-234M -3.132E+OO 4.935E+OO 8.429E+00 FAIL ABUN TH-234 1.355E+OO 1.928E+OO 3.641E+OO FAIL ABUN NP-237 -l.938E-02 6 .151E-02 1.132E-01 NOT IDENT. NP-238 O.OOOE+OO 7.173E+40 O.OOOE+OO SHORT HLIF U-238 1.355E+OO 1. 928E+OO 3. 641E+OO FAIL ABUN NP-239 -1.463E-01 2.923E-01 4;606E-01 NOT IDENT. PU-239 4.577E+02 6.308E+02 6.731E+02 FAIL ABUN CM-243 8.128E-03 1.140E-01 2.102E-01 NOT IDENT. BK-247 -3.669E-02 6.994E-02 l.277E-01 NOT IDENT. CM-247 2.675E-02 3.317E-02 6.940E-02 NOT IDENT. CF-249 1.211E-02 4 .119E-02 7.985E-02 NOT IDENT. CF-251 -3.552E-02 l.151E-01 2.197E-01 NOT IDENT. Page 4148of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:09:09.44 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 323 10.66* l.OOlE+OO l.552E+Ol l.552E+Ol 11. 02 SC-46 889.28 4 99.98* l.541E+OO l.220E-02 l.530E-01 207.36 1120.55 39 99.99 l.265E+OO l.561E-01 l.957E+OO 70.74 CD-109 88.03 62 3.70* 4.275E+OO 2.018E+OO 3.195E+OO 69.94 SN-126 64.28 ------9.60 l.983E+OO ------Line Not Found ------86.94 62 8.90 4.275E+OO 8.390E-01 8.390E-01 69.94 87.57 62 37.00* 4.275E+OO 2.018E-01 2.018E-01 69.94 CE-141 145.44 16 48.29* 6.023E+OO 2.745E-02 l.859E+Ol 306.07 TL-208 277.37 ------6.60 4.205E+OO ------Line Not Found ------583.19 123 85. 00.* 2.199E+OO 3.376E-01 3.376E-01 24.76 860.56 ------12.50 l.582E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 2.941E+OO ------Line Not Found ------351.06 264 12.92* 3,.426E+OO 3.062E+00 3.062E+OO 17.33 PB-212 74."82 170 10.28 3.129E+OO 2.712E+OO 2.712E+OO 31. 58 77 .11 239 17.10 3.370E+OO 2.127E+OO 2.127E+OO 24.49 238.63 485 43.60* 4. 7'41E+OO l.202E+OO l.202E+OO 11. 04 300.09 ------3.30 3.935E+OO ------Line Not Found ------BI-214 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26. 88 1120.29 39 14.92 l.265E+OO l.046E+OO l.046E+OO 70.74 1764.49 28 15.30 8.362E-01 l.103E+OO l.103E+OO 39.19 PB-214 74.82 170 5.80 3.129E+00 4.807E+OO 4.809E+OO 31. 58 77 .11 239 9.70 3.370E+OO 3.749E+OO 3.750E+OO 24.49 87.09 62 3.41 4.275E+OO 2.190E+OO 2.191E+OO 69.94 242.00 140 7.25 4.695E+OO 2.101E+OO 2.102E+OO 35.42 295.22 159 18.42 3.992E+OO l.106E+OO l.106E+OO 24.81 351. 93 264 35.60* 3.426E+OO l. lllE+OO l .112E+OO 17.33 RN-222 609.32 157 45.49* 2 .118E+OO 8;347E-01 8.350E-01 26.88 1120.29 39 14.92 1. 2 65E+OO 1. 046E+OO l.046E+OO 70.74 1764.49 28 15.30 8.362E-01 l.103E+OO l.103E+OO 39.19 RA-224 240.99 140 4.10* 4.695E+OO 3.716E+OO 3.716E+OO 35.42 RA-226 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26. 88 1120.29 39 14.92 l.265E+OO l.046E+OO l.046E+OO 70.74 1764.49 28 15.30 8.362E-01 l.103E+OO l.103E+OO 39.19 AC-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 96 11. 27 3.546E+OO l.225E+OO l.225E+OO 46.39 794.95 ------4.25 1. 691E+OO ------Line Not Found ------835. 71 ------1. 61 1. 621E+OO ------Line Not Found ------911. 20 98 25.80* l.508E+OO l.296E+OO l.296E+OO 22.47 968.97 39 15.80 1. 431E+OO 8.914E-01 8.914E-01 85.15 RA-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 96 11. 27 3.546E+OO l.225E+OO l.225E+OO 46.39 794.95 ------4.25 1. 691E+OO ------Line Not Found ------835.71 ------1. 61 l.621E+OO ------Line Not Found ------911.20 98 25.80* l.508E+OO l.296E+OO l.296E+OO 22.47 968. 97 39 15.80 l.431E+OO 8.914E-01 8.914E-01 85.15 TH-228 74.82 170 10.28 3.129E+OO 2.712E+00 2.712E+OO 31. 58 77 .11 239 17.10 3.370E+OO 2.127E+OO 2.127E+00 24.49 Page 4149of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 485 43.60*
4.741E+OO l.202E+OO 1.202E+OO 11. 04 300.09 ------3.30 3. *935E+OO ------Line Not Found ------TH-230 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.347E-01 26.88 1120.29 39 14.92 1.265E+OO 1. 046E+OO l.046E+OO 70.74 1764.49 28 15.30 8.362E-01 l.103E+OO 1.103E+OO 39.19 TH-232 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 96 11. 27 3.546E+OO l.225E+OO 1.225E+OO 46.39 835. 71 ------1. 61 1.621E+OO ------Line Not Found ------911. 20 98 25.80* l.508E+OO l.29.6E+OO l.296E+OO 22.47 968. 97 39 15.80 1.431E+OO 8.914E-01 8.914E-01 85.15 U-234 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.347E-01 26. 88 1120.29 39 14.92 1. 265E+OO 1.046E+OO 1.046E+OO 70.74 1764.49 28 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 U-235 89. 96 54 3.47 4.476E+OO 1. 770E+OO 1. 770E+OO 59.83 93.35 126 5.60 4. 711E+OO 2. 441E+OO 2.441E+00 54.61 143.76 16 10. 96* 6.023E+OO l.209E-01 1. 209E-01 306.07 163-. 33 ------5.08 5.876E+OO ------Line Not Found ------185. 72 124' 57.20 5.570E+OO l.999E-01 l.999E-01 43.72 205.31 ------5.01 5.260E+oo ------Line Not Found ------AM-241 59.54 42 35.90* 1.428E+OO 4.218E-01 4.223E-01 111.73 AM-243 43.53 ------5.90 1.216E-01 ------Line Not Found ------74.66 170 67.20* 3.129E+OO 4.149E-01 4.149E-01 31. 58 ANH-511 511. 00 17 100.00* 2.464E+OO 3.567E-02 3.567E-02 269.31 Flag: "*" Key line Page 4150of5809 Summary of Nuclide Activity Sample ID : G405235054 Acquisition date Page : 3 3-0CT-2016 07:07:21 Total number of lines in spectrum 48 Number of unidentified lines 13 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 SC-46 C0-109 SN-:-126 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-241 AM-243 ANH-Sil Hlife 1.25E+09Y 83.790 461. 400 2.30E+05Y 32.510. 1. 41E+10Y 7.04E+08Y l.41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1.41E+10Y 1. 41E+10Y 7.54E+04Y i.41E+10Y 2.45E+05Y 7.04E+08Y 432.60Y 7370.00Y 1.00E+09Y Decay 1. 00 12.5 1. 58 1. 00 677. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM. 1.552E+Ol .1. 220E-02 2.018E+OO 2.018E-01 2.745E-02 3.376E-01 3.062E+OO 1.202E+OO 8.347E-01 1. lllE+OO 8.347E-01 3.716E+OO 8.347E-01 1.296E+OO l.296E+OO 1;202E+OO 8.347E-01 1.296E+OO 8.347E-01 1.209E-01 4.218E-01 4.149E-01 3. 5.67E-02 3.747E+Ol 3.747E+Ol Decay Corr pCi/GRAM 1.552E+Ol 1.530E-01 3.195E+OO 2.018E-01 1.859E+Ol 3.376E-01 3.062E+OO 1. 202E+OO 8.350E-01 1.112E+OO 8.350E-01 3.716E+OO 8.350E-01 1.296E+OO 1.296E+OO 1.202E+OO 8.347E-01 1.296E+OO 8.347E-01 1. 2 09E-01 4.223E-01 4.149E-01 3.567E-02 5.735E+Ol 5.735E+Ol 72. 92% Decay Corr 2-Sigma Error 0.171E+Ol 3 .172E-01 2.234E+OO 1.412:E-01 5.689E+Ol 0.836E-01 0.531E+OO 0.133E+OO 2.245E-01 0.193E+OO 2.245E-01 1.316E+OO 2.245E-01 0.291E+OO 0.291E+OO 0.133E+OO 2.244E-01 0.291E+OO 2.244E-01 3.702E-01 4.719E-01 l.310E-01 9.606E-02 "M" Manually accepted 2-Sigma %Error 11. 02 207.36 69.94 69.94 306.07 24.76 17.33 11. 04 26.88 17.33 26.88 35.42 26.88 22.47 22.47 I1. 04 26.88 22.47 26.88 306.07 111. 73 31. 58 269.31 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4151of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235054 Acquisition date : 3-0CT-2016 07:07:21 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 1 80.99 43 111 1. 25 161.77 141 24 9.67E-03 **** 3.76E+00 T 0 114.29 37 130 2.27 228.39 225 9 8.52E-03 **** 5.72E+OO T 0 129.76 34 131 1. 28 259.36 253 9 7.80E-03 **** 5.99E+00 T 0 208.40 60 141 0.68 416.67 412 11 l.44E-02 87.0 5. 21E+OO 0 219.04 47 147 6.21 437.95 429 15 l.12E-02 **** 5.04E+OO 0 320.25 28 50 0.65 640.43 634 12 7.0lE-03 **** 3.72E+OO T 0 382.39 41 92 7.31 764.75 748 21 1.05E-02 **** 3.18E+OO T 0 409.10 39 23 3.19 818.17 813 10 1.00E-02 58.9 3.00E+OO 0 441.72 22 20 1.10 883.43 880 8 5.77E-03 83.4 2.80E+OO 0 464.44 20 60 3.37 928.88 920 13 5.18E-03 **** 2.68E+OO T 0 566.62 7 32 1. 47 1133. 29 1126 10 1. 94E-03 **** 2.25E+OO 0 722.93 12 8 1. 22 1445. 96 1443 6 3.23E-03 **** l.83E+OO T 0 "726.85 46 9 2.06 1453.81 1449 11 1. 23E-02 39.3 1. 82E+OO T 0 767.75 28 13 1. 88 1535.63 1530 10 7.62E-03 61. 5 1.74E+OO T 0 774.19 20 11 1. 77 1548.50 1543 10 5.37E-03 81. 0 1. 73E+OO 0 833.02 6 9 0.72 1666.18 1660 8 1.58E-03 **** l.63E+00 T 0 884.64 15 6 0.85 1769.43 1765 9 4.03E-03 81. 7 1.55E+OO T 0 890.84 9 1 0.95 1781.8'4 1779 6 2.42E-03 80.5 1. 54E+OO 0 902.44 10 15 4.10 1805.04 1797 12 2.75E-03 **** 1.52E+OO T 0 922.79 20 17 4 .11 1845.74 1836 17 5.41E-03 **** 1. 49E+OO . T 0 1042.99 8 8 1. 24 2086.17 2080 10 2.26E-03 **** 1.35E+OO 0 1215.78 19 . '6 3.78 2431. 79 2425 13 5.34E-03 70.6 l.18E+OO 0 1314.44 4 4 . 0. 94 2629 .13 2623 8 1. llE-03 **** 1.lOE+OO 0 1341.47 10 3 0. 96 2683.18 2676 11 2.79E-03 90.3 l.08E+00 0 1353.06 6 2 0.75 2706.35 2702 8 1. 63E-03 **** 1.07E+OO 0 1847.26 11 0 2.31 3694.75 3690 10 3.33E-03 57.7 7.99E-01 Flags: "T" = Tentatively associated Page 4152of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:09:23.50 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l * *Acquisition date 3-0CT-2016 07:07:21 Sensitivity : 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
Sample date 2-DEC-2015 14:51:00 Nuclide Library : SOLID *
Sample ID G405235054 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.4646E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * ** *
Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
Eff.' File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-241 AM-243 ANH-511 Le (pCi/GRAM l.925E-01 O.OOOE+OO 1.094E+OO 6.965E-02 3.480E-02 1. 741E-01 4.456E-02 5.316E-02 l.672E-01 5.316E-02 4.778E-01 5.316E-02 9.553E-02 9.553E-02 4.456E-02 5.314E-02 9.553E-02 5. 314E.:..02 1.606E-01 1. 962E-01 5.772E-02 3.044E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 MN-56 Page 4153 of 5809 Le (pCi/GRAM 1.225E+Ol 4.173E-02 O.OOOE+OO 2.073E-02 0.000E+OO O.OOOE+OO 5.226E-02 4.298E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153* EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4154of5809 4.522E-02 5.047E-01 7. 7 41E+OO 3.600E-02 1.409E-01 2.523E+OO 1. 755E+Ol O.OOOE+OO 1. 763E-01 O.OOOE+OO O.OOOE+OO 7.349E-01 7.810E+OO 8.775E-01 O.OOOE+OO 2.551E-01 4.295E+02 3.533E-02 9.455E-01 2.263E+OO 1.242E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.040E-02 5.951E-02 5.885E+OO 4.493E-01 4.493E-01 2.408E-02 1.128E-01 2.260E-01 O.OOOE+OO O.OOOE+OO 1. 331E-01 1. 981E+OO 1.079E-01 2.658E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.550E-02 O.OOOE+OO 5.025E-02 1.244E-01 O.OOOE+OO O.OOOE+OO 3.504E-02 3.701E-02 1.122E-01 O.OOOE+OO O.OOOE+OO 2.361E+Ol O.OOOE+OO 3.318E-01 5 .116E-02 4.458E+OO 4.306E-02 O.OOOE+OO 8.176E+02 O.OOOE+OO 2.047E-02 8.296E-02 1. 7 90E-01 1. 028E-01 1.231E-01 1. 926E+OO 6.344E-02 4.00lE+Ol 2.283E-01 5.476E-02 2.144E-02 4.254E+OO 9.505E-01 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. . NOT I DENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUl':J NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. Nor IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4155of5809 4.697E+OO 3.862E+Ol 1.14 7E+02 4.215E-01 2.276E+OO 3.732E-02 9.681E+OO 4.405E-01 6.991E-01 3.534E-01 4.633E-01 l.927E-01 l.927E-01 4.266E-01 4.276E-01 4.633E-01 5.170E-02 2.515E-01 3.614E+OO 1. 713E+OO 5.170E-02 O.OOOE+OO 1. 713E+OO 2.143E-01 3.172E+02 9.835E-02 5,832E-02 3.143E-02 3.646E-02 1. 025E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT I DENT .. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:09:28.85 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l *
Acquisition date 3-0CT-2016 07:07:21 Sensitivity : 3.000 *
Detector ID GAM43 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.68 Half life ratio : *****. *
Sample date 2-DEC-2015 14:51:00 Nuclide Library : SOLID *
Sample ID G405235054 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.4646E+02 GRAM *
Quantity Err(%) 1.3656E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7 .* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma ) ( 1. 96-sigma) K-40 1.552E+Ol 1.863E+OO l.863E+OO SC-46 l.530E-01 3.109E-01 3.109E-01 CD-109 1.581E+OO 2.237E+OO 2.237E+OO SN-126 9. 991E-02 1.412E-01 1.412E-01 TL-208 3.376E-01 8.317E-02 8.317E-02 BI-211 l.521E-02 9.247E-01 9:247E-01 PB-212 1.202E+OO l.450E-01 l.450E-01 BI-214 8.350E-01 2.229E-01 2.229E-01 PB-214 1.112E+00 l.945E-01 l.945E-01 RN-222 8.350E-01 2.229E-01 2.229E-01 RA-224 1.761E+OO 1.384E+OO 1.384E+OO RA-226 8.350E-01 2.229E-01 2.229E-01 AC-228 1.296E+OO 2.930E-01 2.930E-01 RA-228 1.296E+OO 2.930E-01 2.930E-01 TH-228 1.202E+OO l.450E-01 l.450E-01 TH-230 8.347E-01 2.228E-01 2.228E-01 TH-232 1.296E+OO 2.930E-01 2.930E-01 U-234 8.347E-01 2.228E-01 2.228E-01 U-235 1.209E-01 3.628E-01 3.628E-01 AM-241 4.223E-01 4.635E-01 4.635E-01 AM-243 3.195E-01 1.326E-01 l.326E-01 ANH-511 3.567E-02 9.415E-02 9.415E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 -4.0lOE+OO 1.522E+Ol l.533E+Ol NOT IDENT. NA-22 1. 351E-02 4.553E-02 4.594E-02 NOT IDENT. NA-24 -1.000E+41 2.080E+41 O.OOOE+OO SHORT HLIF AL-26 -7.073E-04 2.539E-02 2.539E-02 NOT IDENT. V-48 -8.580E+03 l.636E+04 1. 681E+o4 SHORT HLIF CR-51 8.187E+02 9 .116E+02 9.835E+02 SHORT HLIF MN'-54 -5.347E-02 8.352E-02 8.693E-02 NOT IDENT. C0-56 5.346E-02 4.945E-01 4.951E-01 NOT IDENT. Page 4156 of 5809 MN-56 1.000E+41 9.252E+41 0.000E+OO SHORT HLIF C0-57 1.423E-02 5.200E-02 5.239E-02 NOT IDENT . C0-58 ...:.3 .193E-01 6.516E-01. 6.673E-01 NOT IDENT. FE-59 -6.345E-01 9.474E+OO 9.478E+OO NOT IDENT. C0-60 9.919E-03 3. 968E-02 3.993E-02 NOT IDENT. ZN-65 -1. 844E-01 2.497E-01 2.632E-01 NOT IDENT. GE-68 1. 968E+OO 2.655E+OO 2.799E+OO NOT IDENT. AS-73 5. 872E+OO l.934E+Ol 1.952E+Ol NOT IDENT. AS-74 1. 610E+03 6.774E+03 6.813E+03 SHORT HLIF SE-75 -1. 202E-01 2.123E-01 2 .19.lE-01 NOT IDENT. BR-77 1.190E+39 l.050E+40 0.000E+OO SHORT HLI-F SR-82 5.027E+Ol 1. 04 7E+03 l.047E+03 SHORT HLIF RB-83 4.129E-01 7.775E-01 7.995E-01 NOT IDENT. KR-85 6.607E+OO 9.460E+OO 9.918E+OO NOT IDENT. SR-85 7.420E-01 l.063E+OO 1.114E+OO NOT IDENT. RB-86 2.367E+04 3.809E+04 3.956E+04 SHORT HLIF Y-88 1.067E-01 2.735E-01 2.777E-01 NOT IDENT. Y-91 -1. 996E+02 5.379E+02 5.453E+02 NOT IDENT. NB-94 A. 359E-02 3.495E-02 4.009E-02 NOT IDENT. NB-95 3.122E-01 1.190E+OO l.198E+OO NOT IDENT. NB-95M -7. 960E-01 2.918E+00 2.940E+OO NOT IDENT. ZR-95 -5.800E-01 1.550E+OO 1.572E+OO FAIL ABUN NB-97 1.000E+41 3.737E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 2.783E+41 O.OOOE+OO SHORT HLIF M0-99 3.133E+32 7.261E+32 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 1.492E+42 O.OOOE+OO SHORT HLIF RH-101 -2.173E-02 4 .196E-02 4.309E-02 NOT IDENT. RH-102 3.239E-02 6.335E-02 6. 501E-02 FAIL ABUN RU-103 8.324E-01 6.925E+OO 6.935E+OO FAIL ABUN RH-106 3.598E-02 5.063E-01 5.066E-01 NOT IDENT. RU-106 3.598E-02 5.063E-01 5.066E-01 NOT IDENT. AG-108M 1.463E-03 2.826E-02 2.826E-02 FAIL ABUN AG-llOM 1.566E-01 1.256E-01 1. 441E-01 FAIL ABUN SN-113 4.918E-02 2.585E-01 2.594E-01 NOT IDENT. CD-115 4.496E+39 2.201E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 5.210E+04 1. 401E+05 1. 421E+05 SHORT HLIF TE-123M 2.600E-02 1.429E-01 1.434E-01 NOT IDENT. SB-124 9.314E-03 2.371E+00 2.371E+OO FAIL ABUN SB-125 1.178E-01 1.122E-01 1.241E-01 FAIL ABUN TE-125M -6.842E+Ol 3 .182E+02 3.197E+02 NOT IDENT. I-126 -3.929E+05 1.381E+06 1.393E+06 SHORT HLIF SB-126 l.523E+06 2.051E+06 2.163E+06 SHORT HLIF SB-127 3.402E+22 8.449E+22 O.OOOE+OO SHORT HLIF I-131 -2.282E+09 7.919E+09 7.986E+09 SHORT HLIF I-132 -1.000E+41 6.113E+42 O.OOOE+OO SHORT HLIF TE-132 -5.877E+26 1.464E+27 O.OOOE+OO SHORT HLIF BA-133 -1. 789E-02
4. 913E-02 4.979E-02 FAIL ABUN I-133 -1.000E+41 6.871E+41 O.OOOE+OO SHORT HLIF CS-134 3.433E-02 5.314E-02 5.535E-02 NOT IDENT. CS-135 -2.465E-02 l.433E-01 l.437E-01 NOT IDENT. I-135 -1.000E+41 1.157E+42 O.OOOE+OO SHORT HLIF CS-136 7.616E+04 5.069E+05 5.080E+05 SHORT HLIF BA-137M -4.439E-03 4.073E-02 4.078E-02 NOT IDENT .. CS-137 -4.689E-03 4.303E-02 4.308E-02 NOT IDENT. CE-139 5.433E-02 l.189E-01 1.214E-01 NOT IDENT. BA-140 -7.218E+05 l.973E+06 2.000E+06 SHORT HLIF LA-140 4.028E+05 6.048E+05 6.314E+05 SHORT HLIF CE-141 l.859E+Ol 5.576E+Ol 5.638E+Ol FAIL ABUN CE-143 l.OOOE+41 6.779E+40 O.OOOE+OO SHORT HLIF CE-144 -8.299E-02 3.789E-01 3.808E-01 FAIL ABUN PM-144 2.420E-02 5.512E-02 5.619E-02 NOT IDENT. PR-144 2.108E+OO 4.802E+OO 4 .*895E+00 NOT IDENT. PM-146 4.022E-02 4.474E-02 4.827E-02 NOT IDENT. ND-147 -5. 996E+07 5.552E+07 6.175E+07 SHORT HLIF PM-147 6.992E+02 8.982E+02 9.519E+02 NOT IDENT. PM-149 1.000E+41 l.124E+41 0. OOOE+oo* SHORT HLIF EU-150 3.134E-04 2. 641E-02 2.641E-02 FAIL ABUN EU-152 -5.728E-02 l.165E-01 1.193E-01 NOT IDENT. GD-153 -1.661E-01 2.434E-01 2.546E-01 NOT IDENT. EU-154 3.504E-02 1.118E-01 1.129E-01 FAIL ABUN EU-155 l.012E-01 l.355E-01 1.430E-01 FAIL ABUN TB-160 5.072E-01 2.464E+OO 2.475E+OO FAIL ABUN H0-166M 3.067E-02 6.916E-02 7.053E-02 FAIL ABUN TM-171 -3. 926E+.01 4.887E+Ol 5.198E+Ol NOT IDENT. HF-172 6.398E-02 2. 871E-01 2.885E-01 FAIL ABUN LU-172 -1.178E-01 9.392E-02 . 1. 079E-01 FAIL ABUN LU-176 7.663E-03 2.368E-02 2.393E-02 FAIL ABUN HF-181 -l.270E-01 5.104E+OO 5.105E+OO NOT IDENT. Page 4157 of 5809 TA-182 6.423E-01 l.097E+OO l .135E+OO FAIL ABUN RE-183 9. llOE+OO 1.008E+Ol l.088E+Ol FAIL ABUN RE-184 3.519E+Ol 5.891E+Ol 6.lOlE+Ol FAIL ABUN W-188 2.453E+Ol 1.430E+02 l.435E+02 NOT IDENT. IR-192 -4. 296E-01 6.061E-01 6.363E-01 FAIL ABUN HG-203 -2.098E+OO 2.798E+OO 2.954E+00 NOT IDENT. BI-207 -2.219E-02 5.014E-02 5 .113E-02 FAIL ABUN PB-210 2.532E+OO 1.050E+Ol 1.056E+Ol NOT IDENT. PB-211 -1. 013E+OO 7.909E-01 9.134E-01 FAIL ABUN BI-212 1.926E+OO 7.476E-01 l.146E+OO FAIL ABUN RN-219 2.876E-01 3.779E-01 3. 996E-01 NOT IDENT. RA-223 -l.866E-01 6.285E-01 6.341E-01 FAIL ABUN AC-227 -5.00BE-02 2.226E-01 2.237E-01 FAIL ABUN TH-227 -5.00BE-02 2.226E-01 2.237E-01 FAIL ABUN TH-229 1.847E-01 4.559E-01 4.635E-01 FAIL ABUN PA-231 3.344E-01 4.612E-01 4.852E-01 NOT IDENT. TH-231 -1.866E-01 6.285E-01 6.341E-01 FAIL ABUN PA-233 -1.938E-02 6.152E-02 6.213E-02 NOT IDENT. PA-234 -1.068E-01 3.420E-01 3.454E-01 FAIL ABUN PA-234M -3.132E+OO 4.937E+OO 5.135E+OO FAIL ABUN TH-234 1.355E+OO 1. 951E+OO. 2.045E+OO FAIL ABUN NP-237 -1.938E-02 6.152E-02 6.213E-02 NOT IDENT. NP-238 -l.OOOE+41 7.184E+40 O.OOOE+OO SHORT HLIF U-238 1.355E+OO 1.951E+OO 2.045E+OO FAIL ABUN NP-239 -l.463E-01 2.926E-01 2.999E-01 NOT IDENT. PU-239 4.577E+02 6. 311E+02 6.640E+02 FAIL ABUN CM-243 8.128E-03 1.140E-01 l.140E-01 NOT IDENT. BK-247 -3.669E-02 7.033E-02 7.225E-02 NOT IDENT. CM-247 2.675E-02 3.348E-02 3.558E-02 NOT IDENT. CF-249 1. 211E-02 4.121E-02 4.157E-02 NOT IDENT. CF-251 -3.552E-02 l.151E-01 1.162E-01 NOT IDENT. Page 4158o.f5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 56.5264 87.09 88.9700 136.47 69.4951 45.60 58.9785 87.57 76.0074 140.51 0.0000 46.54 62.2691 88. 03 . 76.0804 143.76 70.2601 49.72 0.0000 88.34 76.1292 144.24 70.3099 51. 35 71.6210 88.47 76.1494 145.44 64.9173 51. 87 64.3473 89. 96 69.4391 152.43 78.0023 52.39 75.0109 1093.63 69.5357 153.25 0.0000 52.97 62.4388 91.11 0.0000 323.87 71.3231 53.44 56.1657 92.59 69.8099 156.02 O.OOOQ 54.07 66.8845 93.35 69.9161 158.56 0.0000 57.36 0.0000 94.56 70.0841 159.00 74.3935 57.53 55.7471 94. 65 70.0964 162.33 76.4701 57.98 62. 9718 94.67 70.0992 162.66 0.0000 59.27 62.4755 94.87 70.1271 163.33 81.7939 59.32 62.4839 97.43 87.7068 165.86 68.9747 59.54 62. 5211 98.43 67.4762 176.31 71.6891 60. 96 77.9079 98.44 67. 4775 176.60 0.0000 61.17 77.9513 99.53 56.6107 177.52 70.9131 62 .. 93 62.3599 100 .11 60.2154 181. 07 0.0000 63.29 59.5149 102.03 73.4689 181. 52 58.7980 63.58 65.3704 103.18 68.8763 184.41 61. 6911 64.28 86.2262 103.37 68. 9011 143.76 61. 7 907 66.73 70.2891 105.21 75.0956 193.51 57.8548 67.24 67.0794 105.31 75.1091 197.03 66.2654 125.81 84.7669 106.12 84. 7724 198.01 63.6155 67.75 84.7810 106.47 83.6318 201.83 67.5495 69.67 76.7009 109.28 66.0447 203.43 47.1887 70.83 84.3113 111. 00 57.8156 205.31 50.8648 72.81 89.1681 111. 76 0.0000 210.85 71. 9332 72.87 89.1809 114. 06 70.2357 215.65 62.5822 74.66 89.5551 116. 30 0.0000 222 .11 50.4185 74.82 89.5880 116.74 72. 9936 227.09 59.1349 74.97 89.6191 119. 76 67.2536 227.38 66.6643 77 .11 .90.0598 121.12 .56.3763 228.16 0.0000 78.74 90.3912 121. 22 56.3857 228.18 64.8412 79.69 90.5829 121.78 61.3457 116.74 64.8412 80.12 90. 6696 122.06 61.3743 235.69 68.1914 80.19 0.0000 122.92 79.9001 235. 96 53.9999 80.57 90.7593 123.07 71.3128 238.63 54.1478 81. 00 90.8453 265.00 78.7690 238.98 0.0000 81. 07 90.8594 125.81 72.4561 240.99 54.2777 81.75 78.8622 127.23 80.8741 242.00 54.3333 83.79 61.6930 127.91 71. 87 54 244.70 41. 5773 84.00 75.4368 129.30 72. 0345 252.40 0.0000 85.43 B7.1317 131.20 63 .1161 252.80 37.5761 86.55 88.8697 133. 02 59. 9648 254.15. 0.0000 86.79 88.9140 133. 52 74.0145 256.23 47.3683 86.94 88.9423 136.00 72.7921 260.90 0.0000 Page 4159of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.7254 355.39 0.0000 584.27 28.1552 2 64. 80 48.7325 356.01 39.4615 595.83 0.0000 46.7920 364.49 0 . .0000 427.87 12.8208 268.22 50.8447 366.42 0.0000 602.52 0.0000 269.46 47.9662 372. 51 35.1531 604.72 19.0874 270.03 46.0333 375.05 22. 4112 607.14 17.4565 271.23 43.1433 377.52 22.4514 609.32 17.4750 273.65 0.0000 356.01 35.4405 610.33 17.4837 276.40 39.4076 388.16 32.3175 614.28 16.2271 277.37 53.2474 388.63 0.0000 618.01 21.1126 277.60 53.2584 391. 69 31.3175 620.36 14.7959 278.00 51. 3049 264.66 22.8201 621.93 17.5835 279.20 58.2750 401. 81 21. 7505 630.19 0.0000 279.54 64.2211 402.40 19.5831 631. 29 16.7338 279.70 64.2303 404.85 39.2322 633.25 26.0543 280.46 37.5756 410.95 37.7533 634.78 0.0000 283.69 53.5529 413.71 18.0895 635.95 14.9077 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 41. 7163 423.72 0.0000 645.85 20.5941 285.90 0.0000 427.09 28.7586 657.76 21. 6509 287.50 53.7341 427.87 21.0267 657.90 0.0000 290.67 47.8984 433.94 24.4430 661.66 26.4055 293.27 0.0000 439.40 25.0864 664:57 0.0000 3'51. 93 46.0852 453.88 15. T528 666.33 0.0000 295.96 37.5938 463.37 29.4277 666.50 0.0000 879.38 .46.7214 468.07 25.5396 667.71 0.0000 299.98 36.2153 473.00 0.0000 677.62 20.8996 300.09 36.2190 475.06 27.3574 685.70 0.0000 300.13 36.2197 476.78 23. 9625 695.00 0.0000 301.36 38.2721 477.60 29.6827 696.49 '14.3706 302.85 58.4897 482.18 24.0403 696. 51 14.3706 256.23 40.3947 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.2091 306.78 33.3901 497.08 23.0969. 697.49 18.2108 308.46 36.4768 505.52 34.8145 702.65 13.4493 311'. 90 42.6793 507.63 0.0000 706.68 26.9464 316.51 50.4930 511. 00 37.2516 711. 68 21.2185 319.41 0.0000 514.00 27.9863 720.70 0. 0000* 320.08 0.0000 514.00 27.9863 721.93 0.0000 321.04 32.7637 520.40 23.6992 722.78 23.2588 323.87 35.4048 520.69 0.0000 722.91 23.2603 325.23 52.3945 522.65 0.0000 723.31 20.1621 328.76 0.0000 527.90 0.0000 724.19 0.0000 333.37 31.0217 528.26 24.6846, 727.33 7.7681 333.97 31.0364 529.59 22.9380 733 .. 00 9.0847 334.37 27.9415 529.87 0.0000 735.93 18.5170 338,28 28.0278 531. 02 0.0000 333.97 21. 4548 338.32 28.0289 537.26 0.0000 739.50 0.0000 311.90 38.9946 546.56 0;0000 747.24 17.6265 340.48 38.9946 552.55 22.3328 748.06 24.4896 340.55 0.0000 563.25. 20.1243 752.31 16.6825 344.28 45.3674 569.33 31. 7244 753.82 0.0000 345.93 38.8461 946.00 25.9585 756.73 16. 7131 351.06 38.7893 569.70 20.1920 756.80 16. 7136 351. 93 38.8149 583.19 28.1401 884.68 22.0876 Page 4160of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.5258 1274.44 11. 8154 1620.50 2.0307 766.42 14.2137 1001.03 19.3645 1621.92 3.0469 766.84 12.4111 1002.74 13.9934 1678.03 0.0000 772.60 0.0000 1004.73 15.0797 1690.97 4.1234 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0936 778.90 7.9368 1028.54 0.0000 1063.66 1. 74 67 783.70 0.0000 1037.84 10.4520 1771.35 2.9950 785.37 15.9150 1038.76 o .. 0000 1791.20 0.0000 792.07 23.9370 631.29 5.2406 1808.65 2 .1123 794.95 11. 9824 1048.07 0.0000 1810.72 0.0000 795.86 12.9853 1049.04 14.2045 1836.06 3.1857 810.06 10.0452 1050.41 14.2108 810.29 12.0553 1063.66 13.1719 344.28 12.0560 1077.00 0.0000 810.76 17.0815 *1077.34 8.8188 815.77 0.0000 1085.87 14.3687 1048.07 0.0000 1093.63 21.0503 832.01 10.1309 1099.45 16.6489 834.85 21.0952 1112. 07 8.9131 835.71 17. 8557 1112. 84 11.1444 836.80 0.0000 1115. 54 19.6292 846.75 0.0000 1120.29 15.6372 846.77 12.2260 1120.55 15.6381 856.80 0.0000 1221.41 15.6415 860.56 19.4581 1129. 67 19. 7130 871.09 21. 5909 1131. 51 0.0000 873.19 10.2893 1147.95 0.0000 875.33 0.0000 1173.23 14. 5211 879.38 13.2004 1177.95 9.9967 880.51 16.5073 1189.05 10.0289 883.24 18.1763 1204.77 11. 9050 884.68 14.8790 1221.41 9.2007 889.28 0.0000 1231.02 15.6827 894.76 8.2966 1235.36 0.0000 898.04 19.9354 1238.28 15.7142 ' 900. 72 16.6289 1260.41 0.0000 903.28 11. 0960 1271.87 15.8595 911.20 9.3889 1274.44 7.4684 912.08 9.3917 1274.54 7.4684 923.98 *o. 0000 1291.59 7.5027 926.50 11.7472 1298.22 0.0000 929 .11 20.1568 1312.11 0.0000 937.49 14.7408 1332.49 6.6356 944.13 0.0000 1362.66 0.0000 946.00 16.8965 1365'.19 2.8679 949.00 15.8565 1368.63 0.0000 667.71 0.0000 1384.29 8.6454 962. 31 11. 8938 1408. 0'1 9.6631 964. 08 15.3013 1457.56 0.0000 966 .17 25.5198 1460.82 2. 9364 911. 20 20.2229 1489.16 5.9127 968. 97 20.2229 1505.03 5.9347 983.53 0.0000 1584.12 4.0287 984.45 0.0000 1596. 21 0.0000 Page 4161of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:19:11.60
GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : 2-0CT-2016 11:00:34. Sample date 2-DEC-2015 14:59:00.-Acquisition date : 3-0CT-2016 07:18:44. Sample ID G405235055 Sample quantity 1.42583E+02 GRAM Detector name GAMll Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.58 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 1 5 5 5 5 0 0 0 6 6 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4162of5809 Energy 63.34* 73.12* 74.95* 77.09* 87.10 88.77 90.10 92.62* 186.16* 209.16 216.23 238.58* 241. 80 270.53 277.21 280.00* 295.32* 299.81 328.23 338.39*

352.03* 409.52 463.24 466.55 511.15* 546.28 583.16* 609.52* 724. 04 727.29* 795.61 806.09 835.33 861.31 BACKGROUND*CORRECTED SAMPLE PEAK REPORT Area 14 22 158 247 125 45 90 112 95 55 10 444 115 29 35 15 132 21 43 102 260 26 31 15 55 12 138 163 16 21 20 25 22 21 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 132 130 127 122 155 148 110 128 138 101 77 50 87 74 48 48 84 75 50 47 82 41 32 25 39 9 22 46 11 24 15 27 17 24 0.86 1. 00 1. 01 1. 01 1. 45 1. 52 1.12 1. 53 1. 39 1. 29 1.18 0. 96 1. 97 0.75 1. 28 1. 61 1. 02 0.72 2.96 1. 07 1. 29 0.78 0.97 0.61 1. 68 1. 33 1. 47 1. 38 2,30 1. 41 0.98 5.27 1. 88 3.79 126.58 146.16 149.82 154.11 174.14 177.48 180.13 185.18 372.40 418.42 432.57 477.29 483.74 541.23 554.60 560. 20 590.85 599.83 656. 71 677.03 704.33 819.37 926 . .88 933.50 1022.75 1093.04 1166. 82 1219.56 1448.71 1455.21 1591. 89 1612.85 1671.35 1723.33 124 143 143 143 165 165 165 165 368 413 429 471 471 538 551 551 586 599 652 673 697 815 924 930 1015 1090 1161 1214 1445 1452 1586 1597 1665 1717 7 3.93E-03142.8 17 6.03E-03 88.0 17 4.38E-02 14.2 17 6.87E-02 9.8 29 3.48E-02 19.9 29 1.24E-02 58.2 29 2.50E-02 23.2 29 3.12E-02 23.3 11 2.63E-02 27.8 10 l.54E-02 36.6 7 2.67E-03154.9 20 1.23E-01 5.5 20 3.20E-02 22.6 9 8.08E-03 57.0 13 38.4 13 4.03E-03 89.8 10 3.68E-02 15.7 7 5. 90E-03 71. 0 10 1.19E-02 34.6 10 2.84E-02 16.4 13 7. 23E-02 .9. 6 9 7.08E-03 49.2 6 8.49E-03 33.3 8 4.26E-03 62.5 16 1. 54E-02

33. 8 6 3.44E-03 47.4 12 3.83E-02 11.3 11 4. 52E-02 11. 5 7 4.31E-03 43.0 9 5.95E-03 47.0 12 5.45E-03 48.1 21 7.00E-03 54.7 11 5.97E-03 42.5 16 5.83E-03 56.5 Fit 4. 6.5E+po 5.13E+00 1. 70E+OO 1.99E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 902 .13 24 17 3.44 1804.99 1796 17 6.64E-03 44.5 36 0 911. 50* 85 .20 1. 66 1823.73 1818 15 2.35E-02 16.0 37 0 968.97* 54 11 1. 04 1938.70 1934 9 1.49E-02 18.2 38 *o 992.16 6 7* 0.59 1985.10 1982 8 1.78E-03 77.8 39 0 1004.93 15 3 1. 99 2010.65 2007 8 4.lOE-03 34.5 40 0 1011. 06 6 8 0.74 2022.90 2017 8 1. 73E-03 88.1 41 0 '1120.75* 41 30 2.17 2242.33 2235 12 1.14E-02 31. 5 42 0 1218. 96 10 16 0.54 2438.77 2431 12 2.80E-03 88.8 43 0 1238.47 24 11 0.87 2477.79 2472 11 6.67E-03 33.7 44 0 1307.89 8 4 0.65 2616.65 2613 7 2.15E-03 59.4 45 0 1311. 09 6 2 0.98 2623.04 2620 7 1. 67E-03 55.4 46 0 1378.42 18 3 1.37 2757.71 2751 14 4.98E-03 32.2 47 0 1460.98* 409 12 1. 83 2922.82 2915 16 l.14E-01 5.3 48 0 1510.64 6 3 1. 33 3022.13 3018 8 1. 67E-03 68.7 49 0 1765.50* 9 18 1. 53 3531.79 3524 10 2.49E-03 97.1 Flag: "*" = Peak area was modified by background subtraction Page 4163of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:19:13 Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 *. MXRl Analyses by Sample title Sample date Sample ID 2-DEC-2015 14:59:00 G405235055 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:18:44 142.58 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAll 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4164of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242*. 00 74.82 74.82 74.82 351. 93 87.09 87.09 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 AM-243 TH-228 PB-212 BI-211 SN-126 SN-126 Line 240.99 74.66 74.82 74.82 351.06 86.94 87.57 CAN 0 01:00:00.58 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.238E+OO 1. 566E+Ol l.566E+Ol 10.65 OK MN-54 834.85 99.98* 1.951E+OO 5.867E-02 l.157E-01 84.94 OK CD-109 88.03 3.70* 6.347E+OO 1.222E+OO 1.934E+OO 116. 41 OK SN-126 64.28 9.60 3.887E+OO 2.492E-01 2.492E-01 285.54 OK 86.94 8.90 6.243E+OO 1.089E+OO 1. 089E+OO 53.79 OK 87.57 37.00* 6.243E+OO 2.620E-01 2.620E-01 53.79 OK HG-203 70.83 3.69 4.810E+OO Line Not Found Absent 72. 87 6.19 5.060E+OO 4.502E-01 4.252E;+Ol 176.05 OK 279.20 81.56* 4.679E+OO 2.224E-02 2 .101E+OO 179.62 OK TL-208 277.37 6.60 4. 717E+OO 6.579E-01 6.579E-01 76.73 OK 583.19 85.00* 2.582E+OO 3.451E-01 3. 451E-01 22.59 OK 860.56 12.50 1.906E+OO 4. 681E-01 4.681E-01 113.09 OK BI-211 72. 87 1. 23 5.060E+OO 2.266E+OO 2.266E+OO 176.05 OK 351.06 12.92* 3.883E+OO 4.031E-01 4.031E-01 245.18 OK PB-212 74.82 10.28 5.247E+OO 1.369E+OO 1. 369E+OO 41.15 OK 77 .11 17.10 5.454E+OO 1.718E+OO 1.718E+OO 19.51 OK 238.63 43.60* 5. 301E+OO l.140E+00 l.140E+00 10.96 OK 300.09 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 OK BI-214 609.32 45.49* 2.494E+OO 7. 851E-01 7.853E-01 22.91 OK 1120.29 14.92 1. 547E+00 9.205E-01 9.209E-01 62.91 OK 1764.49 15.30 1. 039E+OO 2.798E-01 2.799E-01 194.22 OK PB-214 74.82 5.80 5.234E+OO Line Not Found <<INT Reject 77 .11 9.70 5.454E+OO 3.028E+OO 3.029E+OO 19.51 OK 87.09 3.41 6.242E+OO Line Not Found <<INT Reject 242.00 7.25 5.244E+OO Line Not Found <<INT Reject 295.22 18.42 4.482E+OO 9.343E-01 9.346E-01 31. 36 OK 351.93 35.60* 3.884E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.494E+OO 7. 851E-01 7.853E-01 22.91 OK 1120.29 14.92 1. 547E+OO 9.205E-01 9.209E-01. 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 OK RA-224 240.99 4.10* 5.247E+OO 1.519E+OO l.519E+OO 100.40 OK ,, RA-226 609.32 45.49* 2.494E+OO 7.851E-01 7.853E-01 22.91 OK 1120. 29 14.92 1. 547E+OO

9.205E-01 9.209E-01 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 OK AC-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4. OllE+OO 1.305E+OO l.305E+00 32.77 OK 794.95 4.25 2.027E+OO 1.219E+OO 1.219E+OO 96.12 OK 835.71 1. 61 1. 951E+OO 3.643E+OO 3.643E+OO 84.94 OK 911. 20 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 OK 968. 97 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 OK RA-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4. OllE+OO 1.305E+OO l.305E+OO 32.77 OK 794.95 4.25 2.027E+OO 1.219E+OO 1.219E+OO 96.12 OK 835.71 1. 61 1. 951E+OO 3.643E+OO 3.643E+OO 84.94 OK 911.20 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 OK 968. 97 15.80 1. 738E+OO 1.028E+OO 1.028E+OO 36.48 OK TH-228 74.82 10.28 5.247E+OO 1.369E+OO 1.369E+OO 41.15 OK 77 .11 17.10 5.454E+OO 1. 718E+OO 1.718E+OO 19.51 OK 238.63 43.60* 5. 301E+OO l.140E+OO 1.140E+OO 10. 96 OK Page 4165 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Nuclide Type: Uncorrected Decay Corr . Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 OK TH-230 609.32 45.49* 2.494E+OO 7 .. 851E-01 7. 851E-01 22.91 OK 1120.29 14.92 1.547E+OO 9.205E-01 9.206E-01 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.798E-01 194.22 OK TH-232 105.21 *1.10 7.023E+OO Line Not Found Absent 338.32 11.27 4. OllE+OO 1.305E+OO l.305E+OO 32.77 OK 835.71 1. 61 1.951E+OO 3. 6.43E+OO 3.643E+OO 84.94 OK 911.20 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 OK 968. 97 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 OK TH-234 63.29 3.70* 3.887E+OO 6.466E-01 6.466E-01 285.54 OK 92.59 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 OK U-234 609.32 45.49* 2.494E+OO 7.851E-01 7.851E-01 22.91 OK 1120. 29 14.92 1.547E+OO 9.205E-01 9.205E-01 62.91 OK 1764.49 15.30 l.039E+OO 2.798E-01 2.798E-01 194.22 OK U-235 89.96 3.47 6.425E+OO 2.578E+OO 2.578E+OO 46.33 OK 93.35 5.60 6.560E+OO 1.953E+OO 1.953E+OO 46.65 OK 143.76 10.96* 7.059E+OO Line Not Found Absent 163.33 5.08 6.731E+OO Line Not Found Absent 185.72 57. 20. 6.280E+00 1.'592E-01 l.592E-01 55.51 OK 205.31 5.01 5.902E+OO Line Not Found Absent U-238 63.29 3.70* 3.887E+OO 6.466E-01 6.466E-01 285.54 OK 92.59 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 OK AM-243 43 .. 53 5.90 9.310E-01 Line Not Found Absent 74.66 67.20* 5.247E+OO 2.095E-01 2.095E-01 41.15 OK ANH-511 511. 00 100.00* 2.867E+OO 1. 07 6E-01 1. 076E-01 67.65 OK Flag: "*" = Keyline Page 4166 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 0*8:19:14.50 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHiVE.GAMMA]G405235055.CNF;l *
Acquisition date 3-0CT-2016 07:18:44 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
Sample date 2-DEC-2015 14:59:00 Analyst initials: MXRl *
Sample ID G405235055 Sample Quantity l.4258E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
Eff. File :'DKAlOO:[CANBERRA.GAMMA]EFF GAM11CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Jdentified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.566E+Ol l.635E+OO MN-54 l.157E-01 9.631E-02 CD-109 1.934E+OO 2.207E+OO SN-126 2.620E-01 1. 381E-01 HG-203 2. lOlE+OO 3.698E+OO TL-208 3. 451E-01 7.639E-02 BI-211 4. 031E-01 9.685E-01. PB-212 1.140E+OO l.224E-01 BI-214 7.853E-01 1. 764E-01 PB-214 1. 081E+OO 2.029E-01 RN-222 7.853E-01 1. 764E-01 RA-224 1.519E+OO 1.495E+OO RA-226 7.853E-01 1. 764E-01 AC-228 9.506E-01 2.983E-01 RA-228 9.506E-01 2.983E-01 TH-228 1.140E+OO 1.224E-01 TH-230 7.851E-01 1. 763E-01 TH-232 9.506E-01 2.983E-01 TH-234 6.466E-01 1.809E+OO U-234 7.851E-01 1. 763E-01 U-235 1.054E-Ol l.839E-01 U-238 6.466E-01 1.809E+OO AM-243 2.095E-Ol 8.449E-02 ANH-511 1. 07 6E-01 7.132E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4167of5809 Key-Line Activity (pCi/GRAM 2.135E+OO -7.539E-03 O.OOOE+OO -2.270E-02 -l.034E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) l.313E+Ol 3.370E-02 l.960E+41 2.650E-02 3.186E-01 1.852E+04 MDA (pCi/GRAM 7.527E-01 l.061E-01 1.583E+OO 1.004E-01 4.402E+OO 6.780E-02 3.207E-01 8.561E-02 l .117E-01 3.276E-01 l.117E-01 9.180E-01 1.117E-01 1.994E-01 l.994E-01 8.561E-02 1.116E-01 l.994E-01 1. 744E+OO 1.116E-01 3.559E-01 1. 744E+OO 7.061E-02 4.428E-02 MDA (pCi/GRAM 2.602E+Ol 6. 721E-02 O.OOOE+OO 3.826E-02 5.819E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.940E+02 O.OOOE+OO SHORT HLIF C0-56 -9.827E-02 4.747E-01 8.743E-01 FAIL ABUN MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.965E-02 4.152E-02 7.600E-02 NOT IDENT. C0-58 5.349E-01 5.409E-01 1.165E+OO NOT IDENT. FE-59 -2.997E+OO 6.039E+OO l.130E+Ol NOT IDENT. C0-60 5.845E-03 3.957E-02 8.222E-02 NOT IDENT. ZN-65 -5.151E-02 1. 780E-01 2.958E-01 NOT IDENT. GE-68 8.335E-01 2.155E+OO 4.619E+OO NOT IDENT. AS-73 2.915E-01 6.694E+OO 1. 341E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.458E+03 0.000E+OO SHORT HLIF SE-75 1.280E-01 2.108E-01 4.065E-'-01 FAIL ABUN BR-77 O.OOOE+OO 1.213E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.781E+02 O.OOOE+OO SHORT HLIF RB-83 1.943E-01 5.513E-01 l.149E+OO NOT IDENT. KR-85 4.389E+OO 7.099E+OO l.350E+Ol NOT IDENT. SR-85 4.913E-01 7.974E-01 1.516E+OO NOT IDENT. RB-86 O.OOOE+OO 3.281E+04 O.OOOE+OO SHORT HLIF Y-88 5 .113E-02 1.433E-01 3.836E-01 NOT IDENT. Y-91 5.437E+Ol 4.841E+02 9.935E+02 NOT IDENT. NB-94 2.015E-03 2.978E-02 5.755E-02 NOT IDENT. NB-95 -7.864E-01 9.864E-01 1.645E+OO NOT IDENT. NB-95M 7.041E-01 2.337E+OO 4.087E+OO NOT IDENT. ZR-95 l.273E+00 l.398E+00 3.065E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 777E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 451E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.218E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -8.904E-03 3.026E-02 5.594E-02 NOT IDENT. RH-102. 2.331E-02 5.997E-02 1.209E-01 NOT IDENT. RU-103 -l.254E+OO 5.342E+OO 1.024E+Ol FAIL ABUN RH-106 -3.852E-01 4.630E-01 7.868E-01 NOT IDENT. RU-106 -3.852E-01 4.630E-01 7.868E-01 NOT IDENT. AG-108M -1. 872E:_02 2.145E-02 3.788E-02 FAIL ABUN AG-llOM 7.178E-02 1.000E-01 2.123E-01 NOT IDENT. SN-113 -1.212E-01 2.078E-01 3.857E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 703E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.170E+05 O.OOOE+OO SHORT HLIF TE-123M -2. 961E-02 1. 236E-01 2.261E-01 NOT IDENT. SB-124 -7.729E-01 1. 971E+OO 3. 721E+OO FAIL ABUN SB-125 3.077E-03 1. 04 6E-01 2.047E-01 FAIL ABUN TE-125M 4.238E+Ol 2.603E+02 5.035E+02 NOT IDENT. I-126 O.OOOE+OO 1. 091E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 564E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.586E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 6.899E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+4.l O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.256E+27 O.OOOE+OO SHORT HLIF BA-133 -7.207E-03 3.586E-02 6.292E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 8.021E-02 7.556E-02 1.061E-01 FAIL ABUN CS-135 -8.247E-02 1.558E-01 2.408E-01 NOT IDENT. I-135 *O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.942E+05 O.OOOE+OO SHORT HLIF BA-137M -l.994E-03 2.939E-02 6.125E-02 NOT IDENT. CS'-137 -2.107E-03 3.105E-02 6.470E-02 NOT IDENT. CE-139 6.543E-02 1.032E-01 2.023E-01 NOT IDENT. BA-140 O.OOOE+OO l.696E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.159E+05 O.OOOE+OO SHORT HLIF CE-141 -2.425E+Ol 2.762E+Ol 4.810E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 7.253E-02 3.338E-01 6.393E-01 NOT IDENT. PM-144 2.415E-02 5.483E-02 1.108E-01 NOT IDEN'I'.. PR-144 2.030E+00 4.767E+00 9.618E+00 NOT IDENT. PM-146 -4.580E-04 3.984E-02 7.823E-02 NOT IDENT. ND-147 0. oo'OE+OO 4.655E+07 O.OOOE+OO SHORT HLIF PM-147 -5.363E+Ol 6.984E+02 1.324E+03 NOT IDENT. PM-149 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF EU-150 -6.984E-03 2.588E-02 4.469E-02 FAIL ABUN EU-152 -5.224E-03 7.306E-02 l.457E-01 NOT IDENT. GD-153 -9.376E-02 1.649E-01 2.789E-01 NOT IDENT. EU-154 -1.843E-02 8.236E-02 1.643E-01 FAIL ABUN EU-155 4.286E-02 9.480E-02 1. 876E-01 FAIL ABUN TB-160 -6.734E-02 1.655E+OO 3.197E+OO FAIL ABUN H0-166M -5.234E-03 5.855E-02 1.099E-01 FAIL ABUN TM-171 -7. 729E-01 1.458E+Ol 2. 911E+Ol NOT IDENT. HF-172 -3.845E-02 2. lllE-01 3.938E-01 FAIL ABUN LU-172 4.600E-02 6.608E-02 l.490E-01 FAIL ABUN Page 4168 of 5809 LU-176 -1.423E-02 2.274E-02 3.781E-02 FAIL ABUN HF-181 -3.849E+OO 4.018E+OO 6.906E+OO NOT IDENT. TA-182 5. 096E-02 8. lOlE-01 1.486E+OO FAIL ABUN RE-183 -1. 584E-01 2.217E+OO 4.397E+OO NOT IDENT. RE-184 O.OOOE+OO 6.264E+Ol 6.706E+Ol FAIL ABUN W-188 4.864E+Ol 1.191E+o2 2.096E+02 FAIL ABUN IR-192 -9.828E-02 4.658E-01 8.178E-Ol FAIL ABUN BI-207 2.538E-02 4.149E-02 9.231E-02 FAIL ABUN PB-210 -1.565E-01 2.157E+00 4.309E+OO NOT IDENT. PB-211 4.857E-01 7. 072E-01 1.356E+OO NOT IDENT. BI-212 7.973E-01 7.343E-01 l.204E+OO FAIL ABUN RN-219 -2.008E-01 3.705E-01 6.866E-01 FAIL ABUN RA-223 . 3. 371E-03 5.541E-01 9.988E-01 FAIL ABUN AC-227 -4.685E-02 2.038E-01 3.629E-01 FAIL ABUN TH-227 -4.685E-02 2.038E-01 3.629E-01 FAIL ABUN TH-229 2.503E-01 4.606E-01 8.830E-01 FAIL ABUN PA-231 4.614E-01 4.617E-01 9.078E-01 NOT IDENT. TH-231 3. 371E-03 5. 541E-01 9.988E-01 FAIL ABUN PA-233 * -4.883E-03 5.664E-02 1. OllE-01 FAIL ABUN PA-234 -7.978E-02 2.245E-01 4.036E-01 NOT IDENT. PA-234M 2.193E-01 4.447E+OO 7.990E+OO NOT IDENT. NP-237 -4.883E-03 5.664E-02 1. OllE-01 FAIL ABUN NP-238
O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -l.615E-01 2.036E-01 3.634E-01 FAIL ABUN PU-239 8.953E+Ol 2.788E+02 5.389E+02 NOT IDENT. AM-241 2.645E-02 1.014E-01 2.048E-01 NOT IDENT. CM-243 -7.247E-02 8.916E-02 1.604E-01 FAIL ABUN BK-247 4.946E-02 *7. 313E-02 l .'413E-01 NOT IDENT. CM-247 -3.300E-02 3.395E-02 5.992E-02 FAIL ABUN CF-249 8.827E-03 3.478E-02 7.019E-02 NOT IDENT. CF-251 1.028E-01 9. 801E-02 l.997E-01 NOT IDENT. Page 4169of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:19:12.30 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 393 10.66* l.238E+OO 1.566E+Ol 1.566E+Ol 10.65 MN-54 834.85 22 99.98* 1.951E+00 5.867E-02 1.157E-01 84.94 CD-109 88.03 55 3.70* 6.347E+OO 1.222E+OO 1.934E+OO 116. 41 SN-126 64.28 18 9.60 3.887E+OO 2.492E-01 2.492E-01 285.54 86.94 153 8.90 6.243E+OO 1.447E+OO 1. 447E+OO 39.73 87.57 153 37.00* 6.243E+OO 3.481E-01 3.481E-01 39.73 HG-203 70.83 ------3.69 4.810E+OO ------Line Not Found ------72. 87 27 6.19 5.060E+OO 4.502E-01 4.252E+Ol 176.05 279.20 16 81.56* 4.679E+OO 2.224E-02 2 .101E+OO 179.62 TL-208 277.37 39 6.60 4. 717E+OO 6.579E-01 6.579E-01 76.73 583.19 144 85.00* 2.582E+OO 3. 451E-01 3.451E-01 22.59 860.56 21 12.50 1.906E+OO 4. 681E-01 4.681E-01 113. 09 BI-211 72.87 27 1. 23 5.060E+00 2.266E+OO 2.266E+OO 176.05 351.06 284 12.92* 3.883E+OO 2.977E+OO 2.977E+OO 19.15 PB-212 74.82 194 10.28 5.247E+OO 1.897E+OO 1.897E+OO 28.41 77 .11 304 17.10 5.454E+OO 1.718E+OO 1.718E+00 19.51 238.63 500 43.60* 5.301E+OO 1.140E+OO 1.140E+OO 10.96 300.09 23 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 BI-214 609.32 169 45.49* 2.494E+OO 7. 851E-01 7.853E-01 22.91 1120.29 40 14.92 1.547E+OO 9.205E-01 9.209E-01 62.91 1764.49 8 15.30 1.039E+00 2.798E-01 2.799E-01 194.22 PB-214 74.82 194 5.80 5.247E+OO 3. 361E+OO 3.363E+OO 28.41 77 .11 304 9.70 5.454E+OO 3.028E+00 3.029E+OO 19.51 87.09 153 3.41 6.243E+OO 3.777E+OO 3.778E+00 39.73 242.00 130 7.25 5.247E+OO 1.793E+OO 1. 79.4E+OO 45.24 295.22 147 18.42 4.482E+OO 9.343E-01 9.346E-01 31. 36 351. 93 284 35.60* 3.883E+OO 1.081E+OO 1.081E+OO 19.15 RN-222 609.32 169 45.49* 2.494E+OO 7. 851E-01 7.853E-01 22.91 1120.29 40 14.92 l.547E+OO 9.205E-01 9.209E-01 62.91 1764.49 8 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 RA-224 240.99 130 4.10* 5.247E+OO 3.171E+OO 3 .171E+OO 45.24 RA-226 609.32 169 45.49* 2.494E+OO 7.851E-01 7.853E-01 22.91 1120*. 29 40 14.92 l.547E+OO 9. 2*05E-01 9.209E-01 62.91 1764.49 8 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 AC-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 112 11. 27 4. OllE+OO l.305E+OO 1.305E+OO 32.77 794.95 20 4.25 2.027E+00 1.219E+OO 1.219E+OO 96.12 835.71 22 1. 61 1. 951E+OO 3.643E+00 3.643E+OO 84.94 911.20 85 25.80* 1.823E+00 9.506E-01 9.506E-01 32.02 968. 97 54 15.80 1. 738E+OO 1.028E+OO 1.028E+OO 36.48 RA-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 112 11. 27 4. OllE+OO 1.305E+00 1.305E+OO 32.77 794.95 20 4.25 2.027E+OO 1.219E+OO 1.219E+00 96.12 835.71 22 1. 61 1. 951E+OO 3.643E+OO 3.643E+OO 84.94 911.20 85 25.80* 1.823E+00 9.506E-01 9.506E-01 32.02 968. 97 54 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 TH-228 74.82 194 10.28 5.247E+OO 1.89"7E+OO 1.897E+OO 28.41 Page 4170 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 77 .11 304 17.10 5.454E+OO 1. 718E+OO l.718E+OO 19.51 238.63 500 43'. 60* 5. 301E+OO l.140E+OO l.140E+OO 10. 96 300.09 23 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 TH-230 609.32 169 45.49* 2.494E+OO 7.851E-01 7.851E-01 22.91 1120.29 40 14.92 1.547E+OO 9.205E-01 9.206E-01 62.91 1764.49 8 15.30 1.039E+OO 2. 7*98E-01 2.798E-01 194.22 TH-232 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 112 11. 27 4. OllE+OO 1.305E+OO 1.305E+OO 32.77 835.71 22 1. 61 l.951E+OO 3.643E+OO 3.643E+OO 84.94 911.20 85 25.80* l.823E+OO 9.506E-01 9.506E-01 32.02 968. 97 54 15.80 1. 738E+OO 1.028E+OO 1.028E+OO 36.48 TH-234 63.29 18 3.70* 3.887E+OO 6.466E-01 6.466E-01 285.54 92.59 136 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 U-234 609.32 169 45.49* 2.494E+OO 7. 851E-01 7.851E-01 22.91 1120. 29 40 14.92 1.547E+OO 9.205E-01 9.205E-01 62.91 1764.49 8 15.30 1.039E+OO 2.798E-01 2.798E-01 194.22 U-235 89.96 109 3.47 6.425E+OO 2.578E+OO 2.578E+OO 46.33 93.35 136 5.60 6.560E+OO 1.953E+OO l.953E+00 46.65 143.76 ------10: 96* 7.059E+OO ------Line Not Found ------163.33 ------5.08 6. 731E+OO ------Line Not Found ------185. 72 109 57.20 6.280E+OO 1.592E-01 l.592E-01 55.51 205.31 ------5.01 5.902E+OO ------Line Not Found ------U-238 63.29 18 3.70* 3.887E+OO 6.466E-01 6.466E-Ol
285.54 92.59 136 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 AM-243 43.53 ------5.90 9.310E-01 ------Line Not Found ------74.66 194 67.20* 5.247E+OO 2.901E-01 2.901E-01 28.41 ANH-511 511. 00 59 100.00* 2.867E+OO 1.076E-01 l.076E-01 67. 65 Flag: "*" Key line Page 4171 of 5809
Page : 3 Summary of Nuclide Activity Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Total number of lines .in spectrum 49 Number of unidentified lines 9 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 MN-54 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 312.05D 461.40D 2.30E+05Y 46.59D 1.41E+10Y 7.04E+08Y 1.41E+l0Y 1600.00Y 1600 .. OOY 1600. OOY l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+10Y l .41E+10Y 7.54E+04Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay l:OO 1. 97 1. 58 1. 00 94.5 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 566E+Ol 5.867E-02 1.222E+OO 3.481E-01 2.224E-02 3. 451E-01 2.977E+OO l.140E+OO 7.851E-01 1.081E+OO 7. 851E-01 3 .171E+OO 7. 851E-01 9.506E-01 9.506E-01 1.140Ef00 7. 851E-01 9.506E-01 6.466E-01 7.851E-01 1.592E-01 6.466E-01 2.901E-01 1.076E-01 3.580E+Ol 3.580E+Ol Decay Corr pCi7GRAM 1. 566E+Ol 1.157E-01 1.934E+OO 3.481E-01 2*.101E+OO 3. 451E-01 2.977E+OO 1.140E+OO 7.853E-01 l.081E+OO 7.853E-01 3. l 71E+OO 7.853E-01 9.506E-01 9.506E-01 1.140E+OO 7.851E-01 9.506E-01 6.466E-01 7. 851E-01 1.592E-01 6.466E-01 2.901E-01 1.076E-01 3.865E+Ol 3.865E+Ol 81.63% Decay Corr 2-Sigma Error 0.167E+Ol 0.983E-01 2.252E+OO 1.383E-01 3.774E+OO 0.780E-01 0.570E+OO 0.125E+00 1.800E-01 0.207E+OO 1.800E-01 1.435E+OO 1.800E-01 3.044E-01 3.044E-01 0.125E+OO 1.799E-01 3.044E-01 18.46E-01 1. 799E-01 0.884E-01 18.46E-01 0.824E-01 0.728E-01 "M" Manually accepted 2-Sigma %Error 10.65 84.94 116. 41 39.73 179. 62. 22.59 19.15 10. 96 22.91 19.15 22.91 45.24 22.91 32.02 32.02 10. 96 22.91 32.02 285.54 22.91 55.51 285.54 28.41 67. 65 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4172of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235055 Acquisition date : 3-0CT-2016 07:18:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.16 63 114 1. 29 418.42 413 10 l.54E-02 73.2 5.83E+OO 0 216.23 11 88 1.18 432.57 429 7 2.67E-03 **** 5.70E+OO T 0 270.53 32 82 0.75 541.23 538* 9 8.08E-03 **** 4.81E+OO T 0 328.23 47 55 2.96 656.71 652 10 1. 19E-02 69.2 4. llE+OO T 0 409.52 27 44 0.78 819.37 815 9 7.08E-03 98.3 3.43E+OO T 0 463.24 33 35 0.97 926.88 924 6 8.49E-03 66.6 3.lOE+'OO T 0 466.55 16 26 0.61 933.50 930 8 4.26E-03 **** 3.09E+OO 0 546.28 13 9 1. 33 1093.04 1090 6 3.44E-03 94.9 2. 72E+OO T 0 724. 04 16 11 2.30 1448.71 1445 7 4.31E-03 86.0 2.18E+OO T 0 727.29 22 25 1. 41 1455.21 1452 9 5.95E-03 94.0 2.17E+OO T 0 806.09 26 27 5.27 1612.85 1597 21 7.00E-03 **** 2.0lE+OO 0 902.13 24 17 3.44 1804.99 1796 17 6.64E-03 89.0 1. 84E+OO T 0 992.16 6 7 0.59 1985.10 1982 8 l.78E-03 **** l.71E+OO 0 1004.93 15 3 1. 99 2010.65 2007 8 4.lOE-03 69.0 1. 69E+00 T 0 1011. 06 6 8 0.74 2022.90 2017 8 1.73E-03 **** 1. 68E+OO 0 1218. 96 10 16 0.54 2438.77 2431 12 2.80E-03 **** 1. 44E+00 0 1238.47 23 11 0.87 2477.79 2472 11 6.67E-03 67.3 1. 43E+OO T 0 1307.89 8 4 0.65 2616.65 2613 7 2.15E-03 **** 1.36E+OO 0 1311. 09 6 2 0.98 2623.04 2620 7 l.67E-03 **** l.36E+OO T 0 1378.42 17 3 1. 37 2757. 71 2751 14 4.98E-03 64.3 1. 30E+OO 0 1510.64 6 3 1. 33 3022.13 3018 8 1.67E-03 **** 1.20E+OO Flags: "T" = Tentatively associated Page 4173 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:19:26.49 *******************************************************************************
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Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.-GAMMA.ARCHIVE. GAMMA] G405235055. CNF; 1 *
Acquisition date 3-0CT-2016 07:18:44 Sensitivity 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
Sample date 2-DEC-2015 14:59:00 Nuclide Library : SOLID *
Sample ID . G405235055 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.4258E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
Combined Critical Level Report NOTE: Not ali "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.222E-01 4.574E-02 7. 401E-01 4. 696E-02 2.019E+OO 3.059E-02 1.457E-01 3. 960E-02 4.942E-02 1.585E-01 4.942E-02 4.247E-01 4.942E-02 8.436E-02 8.436E-02 3. 960E-02 4.940E-02 8.436E-02 8.192E-01 4.940E-02 1.683E-01 8.192E-01 3.315E-02
1. 960E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4174 of 5809 Le (pCi/GRAM l.177E+01 2. 716E-02 O.OOOE+OO l.209E-02 2.422E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4175 of 5809 3.790E-01 O.OOOE+OO 3.535E-02 5.lOOE-01 4.705E+OO 3.515E-02 1. 261E-01 2.004E+00 6.282E+OO O.OOOE+OO 1.882E-01 O.OOOE+OO O.OOOE+OO 5.076E-01 6.128E+OO 6.882E-01 O.OOOE+OO l.394E-01 4.260E+02 2.552E-02 7.275E-01 1.891E+OO 1.360E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.615E-02 5.423E-02 4.517E+OO 3.407E-01 3.407E-01 l.646E-02 9.371E-02 1.728E-01 O.OOOE+OO O.OOOE+OO l.054E-01 1.393E+OO 9.321E-02 2.361E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.821E-02 0.000E+OO 4.754E-02 l.109E-01 0. OOOE+OO. O.OOOE+OO 2. 710E-02 2.863E-02 9.467E-02 O.OOOE+OO O.OOOE+OO 2.256E+Ol O.OOOE+OO 2.999E-01 4.958E-02 4.302E+OO 3.515E-02 *O.OOOE+OO 6.166E+02 O.OOOE+OO 2.043E-02 6.554E-02 1.302E-01 6.639E-02 8.808E-02 l.359E+OO 4.890E-02 1. 359E+01* l.844E-01 6.465E-02 1. 709E-02 FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT.IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT*. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN 1 ' HF..,.181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231
TH-231 PA-233 PA-234 PA-234M NP-237 'NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 'CM-247 CF-249 CF-251 Page 4176 of 5809 3.005E+OO 6.254E-01
2. 053E+OO 2.943E+Ol 9.638E+Ol 3.718E-01 4.008E-02 2.020E+OO 6.221E-01 5.519E-01 3 .114E-01 4.550E-01 1:659E-01 l.659E-01 4 .141E-01 4.227E-01 4.550E-01 4.609E-02 l.678E-01 3.489E+OO 4.609E-02 O.OOOE+OO l.685E-01 2.530E+02 9.609E-02 7.493E-02 6.559E-02 2.703E-02 3.199E-02 9.317E-02 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:19:32.42 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l * *Acquisition date 3-0CT-2016 07:18:44 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time:
0 01:00:00.58 Half life ratio : ***** *
Sample date 2-DEC-2015 14:59:00 Nuclide Library : SOLID *
Sample ID G405235055 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.4258E+02 GRAM *
Quantity Err(%) : 1.4027E-03 % *
Wet wt corr 1.00000 Wet Weight* 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM11 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 MN-54 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 1.566E+Ol 1.157E-01 1.934E+OO 2.620E-01 2.101E+OO 3.451E-01 4. 031E-01 1.140E+OO 7.853E-01 1.081E+OO 7.853E-01 1.519E+OO 7.853E-Oi 9.506E-01 9.506E-01 1.140E+OO 7. 851E--01 9.506E-01 6.466E-01 7. 851E-01 1.054E-01 6.466E-01 2.095E-01 1.076E-01 Act Error ( 1. 96-sigma) 1. 828E+OO 9.643E-02 2.212E+OO 1.395E-01 3.700E+OO 7.779E-02 9. 81'4E-01 l.365E-01 1. 795E-01 2.078E-01 1. 795E-01 1. 501E+OO 1. 795E-01 3.023E-01 .3. 023E-01 l.365E-01 l.795E-01 3.023E-01 1.815E+OO 1. 795E-01 1.840E-01 1.815E+OO 8.608E-02 7.145E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4177 of 5809 Key-Line Activity (pCi/GRAM 2.135E+OO -7.539E-03 1.000E+41 -2.270E-02 -1.034E-01 5.826E+03 K.L Act error ( 1. 96-sigma) 1.313E+Ol 3.370E-02 2.584E+41 2.654E-02 3.187E-01 l.852E+04 TPU ( 1. 96-sigma) 1.828E+OO 9.643E-02 2.212E+OO 1.395E-01 3.700E+OO 7.779E-02 9.814E-01 1.365E-01 1.795E-01 2.078E-01 1. 795E-01 1. 501E+OO 1. 795E-01 3.023E-01 3.023E-01 1.365E-01 1.795E-01 3.023E-01 1.815E+OO 1.795E-01 l.840E-01 1.815E+OO 8.608E-02 7.145E-02 TPU ( 1. 96-sigma) 1.316E+Ol 3.387E-02 O.OOOE+OO 2.844E-02 3.221E-01 l.870E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -2.688E+02 3.941E+02 4.123E+02 SHORT HLIF C0-56 -9.827E-02 4.747E-01 4.768E-01 FAIL ABUN MN-56 -l.000E+41 4.830E+41 O.OOOE+OO SHORT HLIF C0-57 -l.965E-02 4.153E-02 4.247E-02 NOT IDENT. C0-58 5.349E-01 5.414E-01 5.927E-01 NOT IDENT. FE-59 -2.997E+OO 6.043E+OO 6.192E+OO NOT IDENT. C0-60 5.845E-03 3.957E-02 3. 966E-02 NOT IDENT. ZN-65 -5.151E-02 1. 780E-01 1.795E-01 NOT IDENT. GE-68 8.335E-01 2.155E+OO 2.188E+OO NOT IDENT. AS-73 2.915E-01 6.695E+OO 6.696E+OO NOT IDENT. AS-74 6.843E+03 6.483E+03 7 .180E+03 SHORT HLIF SE-75 1.280E-01 2.109E-01 2.187E-01 FAIL ABUN BR-77 1.130E+39 9. 968E+39 O.OOOE+OO SHORT HLIF SR-82 -8.309E+Ol 5.781E+02 5.793E+02 SHORT HLIF RB-83 1.943E-01 5.519E-01 5.588E-01 NOT IDENT. KR-85 4.389E+OO 7.101E+OO 7. 372E+OO NOT IDENT. SR-85 4.913E-01 7.977E-01 8.279E-01 NOT IDENT. RB-86 -1.047E+04 3.281E+04 3.315E+04 SHORT HLIF Y-88 5 .113E-02 *1.433E-01 1.452E-01 NOT IDENT. Y-91 5.437E+Ol 4. 841E+02 4.847E+02 NOT IDENT. NB-94 2.015E-03 2.978E_.:02 2.980E-02 NOT IDENT. NB-95 -7.864E-01 9.870E-01 1.049E+OO NOT IDENT. NB-95M 7.041E-01 2.338E+00 2.359E+OO NOT IDENT. ZR-95 1. 273E+OO 1.399E+OO 1.512E+OO FAIL ABUN NB-97 1.000E+41 1.777E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1. 451E+41 O.OOOE+OO SHORT HLIF M0-99 8.174E+31 7.219E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 7.433E+41 O.OOOE+OO SHORT HLIF RH-101 -8.904E-03 3. 031E-02 3.057E-02 NOT IDENT. RH-102 2. 331E-02 6.000E-02 6. 091E-02 NOT IDENT. RU-103 -1.254E+OO 5.342E+OO 5.372E+OO FAIL ABUN RH-106 -3.852E-01 4.636E-01 4.951E-01 NOT IDENT. RU-106 -3.852E-01 4.636E-01 .4.951E-01 NOT IDENT. AG-108M -1. 872E-02 2.147E-02 2.307E-02 FAIL ABUN AG-llOM 7.178E-02 1. OOlE-01 l.052E-01 NOT IDENT. SN-113 -1.212E-01 2.079E-01 2.149E-01 NOT IDENT. CD-115 6.075E+38 1. 703E+40 O.OOOE+OO SHORT HLIF SN-117M -3. 391E+04 1.171E+05 1.181E+05 SHORT HLIF TE-123M -2. 961E-02 l.236E-01 1.243E-01 NOT IDENT. SB-124 -7. 729E-01 1.972E+00 2.002E+OO FAIL ABUN SB-125 3.077E-03 1. 04 6E-01 1. 046E-01 FAIL ABUN TE-125M 4.238E+Ol 2.604E+02 2. 611E+02 NOT IDENT. I-126 1.381E+06 1.108E+06 1.271E+06 SHORT HLIF SB-126 -9. 968E+04 1.564E+06 1.565E+06 SHORT HLIF SB-127 -7.840E+21 5.693E+22 O.OOOE+OO SHORT HLIF I-131 6.016E+09 6.905E+09 7.418E+09 SHORT HLIF I-132 -1. OOOE+41 2.068E+42 0.000E+OO SHORT HLIF TE-132 3.828E+26 l.266E+27 O.OOOE+OO SHORT HLIF BA-133 -7.207E-03 3.587E-02 3.601E-02 FAIL ABUN I-133 1.000E+41 2.903E+41 O.OOOE+OO SHORT HLIF CS-134 8.021E-02 7.564E-02 8.384E-02 FAIL ABUN CS-135 -8.247E-02 1.559E-01 1.603E-01 NOT IDENT. I-135 1.000E+41 7.480E+41 0.000E+OO SHORT HLIF CS-136 -4.421E+04 3.943E+05 3.948E+05 SHORT HLIF BA-137M -1.994E-03 2.939E-02 2.940E-02 NOT IDENT. CS-137 -2.107E-03 3.105E-02 3.106E-02 NOT IDENT. CE-139 6.543E-02 l.040E-01 1. 081E-01 NOT IDENT. BA-140 1.882E+06 1.698E+06 1. 898E+06 SHORT HLIF LA-140 -4.197E+05 6.162E+05 6.446E+05 SHORT HLIF CE-141 -2.425E+Ol 2.764E+Ol 2.973E+Ol NOT IDENT. CE-143 1.000E+41 2.204E+42 O.OOOE+OO SHORT HLIF CE-144 7.253E-02 3.338E-Ol 3.354E-01 NOT IDENT. PM-144 2.415E-02 5.485E-02 5.592E-02 NOT IDENT. PR-144 2.030E+OO 4.768E+00 4.855E+OO NOT IDENT. PM-146 -4.580E-04 3.984E-02 3.984E-02 NOT IDENT. ND-147 -7. 527E+0'6 4.655E+07 4.667E+07 SHORT HL0IF PM-147 -5.363E+Ol 6.984E+02 6.988E+02 NOT IDENT. PM-149 2.313E+39 2.510E+41 0.000E+OO SHORT HLIF EU-150 -6.984E-03 2.588E-02 2.608E-02 FAIL ABUN EU-152 -5.224E-03 7.306E-02 7.310E-02 NOT IDENT. GD-153 -9.376E-02 l.650E-01 l.704E-01 NOT IDENT. EU-154 -1.843E-02 8.237E-02 8.279E-02 FAIL ABUN EU-155 4.286E-02 9.485E-02 9.680E-02 FAIL ABUN TB-160 -6:734E-02 1.655E+OO 1.656E+OO FAIL ABUN H0-166M -5.234E-03 5.855E-02 5.860E-02 FAIL ABUN TM-171 -7. 729E-01 1.458E+Ol l.458E+Ol NOT IDENT. HF-172 -3.845E-02 2 .112E-01 2 .119E-01 FAIL ABUN LU-172 4.600E-02 6.625E-02 6.942E-02 FAIL ABUN Page 4178 of 5809 LU-176 -1.423E-02 2.275E-02 2.364E-02 FAIL ABUN HF-181 -3.849E+OO 4.021E+OO 4.379E+OO NOT IDENT. TA-182 5. 096E-02 8. lOlE-01 8.104E-01 FAIL ABUN RE-183 -l.584E-01 2.217E+OO 2.218E+OO NOT IDENT. RE-184 7.182E+Ol 6:503E+Ol 7.265E+Ol FAIL ABUN W-188 4.864E+Ol l.192E+02 1.212E+02 FAIL ABUN IR-192 -9.828E-02 4.658E-01 4.679E-01 FAIL ABUN BI-207 2.538E-02 4.150E-02 4.305E-02 FAIL ABUN PB-210 -1.565E-01 2.157E+OO 2.158E+OO NOT IDENT. PB-211 4.857E-01 7.076E-01 7.407E-01 NOT IDENT. BI-212 7.973E-01 7.354E-01 8.185E-01 FAIL ABUN RN-219 -2.008E-01 3. 714E-01 3.822E-01 FAIL ABUN RA-223 3.371E-03 5.541E-01 5. 541E-01 FAIL ABUN AC-227 -4.685E-02 2.039E-01 2.050E-01 FAIL ABUN TH-227 -4.685E-02 2.039E-01 2.050E-01 FAIL ABUN TH-229 2.503E-01 4.607E-01 4.744E-01 FAIL ABUN PA-231 4.614E-01 4.721E-01 5.159E-01 NOT IDENT. TH-231 3. 371E-03 5.541E-01 5.541E-01 FAIL ABUN PA-233 -4.883E-03 5.664E-02 5.668E-02 FAIL ABUN PA-234 -7.978E-02 2.423E-01 2.450E-01 NOT IDENT. PA-234M 2.193E-01 4.447E+OO 4.448E+OO NOT IDENT. NP-237 -4.883E-03 5.664E-02 5. 668E.:..02 FAIL ABUN NP-238 1.000E+41 4.420E+41 O.OOOE+OO SHORT HLIF NP-239 -l.615E-01 2.040E-01 2.166E-01 FAIL ABUN PU-239 8.953E+Ol 2.788E+o2 2.817E+02 NOT IDENT. AM-241 2.645E-02 l.015E-01 1.022E-01 NOT IDENT. CM-243 -7.247E-02 8.941E-02 9.519E-02 FAIL ABUN BK-247 4.946E-02 7.381E-02 7. 7 lO'E-02 NOT IDENT. CM-247 -3.300E-02 3.440E-02 3.748E-02 FAIL ABUN CF-249 8.827E-03 3.478E-02 3. 501E-02 NOT IDENT. CF-251 1. 028E-01 9.869E-02 1.090E-01 NOT IDENT. Page 4179 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ***************************************************************.**************** ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.4826 87.09 69.5624 136.47 58.4507 45.60 62.6247 87.57 69.6319 140.51 0.0000 46.54 66.2062 88.03 69.6979 143.76 76.7111 49.72 0.0000 88.34 69.7420. 144.24 68.4663 51. 35 63.7357 88.47 69.7606 145.44 99.7617 51. 87 62.9705 89. 96 69.9729 152.43 72.4218 52.39 68.2495 1093.63 70.0689 153.25 0.0000 52.97 56.2492 91.11 0.0000 323.87 53.6622 53.44 72.7896 92.59 70.3432 156.02 0.0000 54.07 83.3379 93.35 70.4488 158.56 0.0000 57.36 0.0000 94.56 70.6171 159.00 6'7.7861 57.53 83.2703 94.65 70.6295 162.33 67.0279 57.98 67.5750 94.67 70.6323 162.66 0.0000 59.27 81. 9015 94.87 70.6600 163.33 71. 3787 59. 32 81. 9125 97.43 80.6072 165.86 56.6538 59.54 71. 3851 98.43 64. 0961 176.31 72. 5922 60. 96 76.6674 98.44 64.0976 176.60 0.0000 61.17 76.7098 99.53 86 .7110 177.52 43.4045 62. 93 . 80.0254 100 .11 91.6283 181.07 0.0000 63.29 80.0996 102.03 72.5985 181. 52 59.9800 63.58 80.1590 103.18 91.1837 184.41 67.1245 64.28 80.3023 103.37 87.3344 143.76 66.8667 66.73 76.6081 105.21 68.1559 193.51 63.0683 67.24 88.9891 105.31 68.1682 197.03 47.7746 125.81 87.2861 106.12 69.2439 198.01 67.8506 67.75 89.1009 106.47 79.0466 201.83 53.6257 69.67 63.8988 109.28 71. 5982 203.43 66.0356 70.83 91.8828 . 111. 00 76.7348 205.31 68.7941 72.81 78.3443 111.76 0.0000 210.85 51.1639 72.87 78.3555 114. 06 70.2205 215.65 53.3261 74.66 78.6809 116. 30 0.0000 222 .11 65.1243 74.82 78.7098 116.74 72.5294 227.09 39.0515 74.97 78.7373 119.76 61. 9134 227.38 37.9146 77 .11 79.1205 121.12 63.0538 228.16 0.0000 78.74 79.4092 121.22 63.0639 228.18 45.9955 79. 6°9 86.3614 121. 78 70.1357 116.74 45.9955 80.12 81.5037 122.06 70.1682 235.69 44.8086 80.19 0.0000 122.92 64.2441 235. 96 52.5488 80.57 74.1675 123.07 64.2598 238.63 51.1422 81. 00 70.5252 265.00 64.3237 238.98 0.0000 81. 07 70.5356 125.81 76.6477 240.99 51.2637 81. 75 79.3151 127.23 75.8108 242.00 51.3154 83.79 69.0826 127.91 75.8932 244.70 38.9806 84:00 69 .1130 129.30 70.9891 252.40 0.0000 85.43 69.3219 131. 20 73.2360 252.80 43.6134 86.55 69.4845 133.02 57.1228 254.15 0.0000 8 6. 7 9 69.5190 133.52 71. 4580 256.23 42.5753 86.94 69.5410 136.00 62.5079 260.90 0.0000 Page 4180 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 40.5327 355.39 0.0000 584.27 28.6023 264.80 40.5379 356.01 28.3063 595.83 0.0000 265.00 42. 9313 364.49 0.0000 427.87 20.8821 268.22 57. 4131 366.42 0.0000 602.52 0.0000 269.46 39.9160 372.51 27.7839 604.72 23.9141 270.03 33.5474 375.05 35.6631 607.14 19.4540 271.23 33.5841 377.52 38.3407 609.32 19.9740 273.65 0.0000 356.01 34.1369 610.33 19.9837 276.40 40.9737 388.16 31.6069 614.28 19.5222 277.37 41.0100 388.63 0.0000 618.01 14.0410 277.60 41.0183 391.69 33.4448 620.36 11.0452 278.00 41.0339 264.66 30.1097 621. 93 24 .1162 279.20 41. 077 5 401. 81 40.7694 630.19 0.0000 279.54 41. 0909 402.40 44.3319 631.29 20.1880 279.70 41.0961 404.85 29.3080 633.25 31.3204 280.46 37.0924 410.95 20.0652 634.78 0.0000 283.69 33. 9652 413.71 25.4628 635.95 23.2677 284. 3*1 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.0919 423. 72 0.0000 645.85 18.2944 285.90 0.0000 427.09 32.4478 657.76 16.3522 287.50 36.5140 427.87 34.2682 .657.90 0.0000 290.67 35.8019 433.94 25.3494 661.66 12.2861 293.27 0.0000 439.40 34.5225 664.57 0.0000 351.93 35.5349 453.88 26.5869 666.33 0.0000 295. 96 35.5579 463.37 16.5989 666.50 0.0000 879.38 44.2408 468.07 16.6465 667.71 0.0000 299.98 42.6531 473.00 0.0000 677.62 14.4386 300.09 42. 6563 475.06 26.0039 685.70 0.0000 300.13 42.6584 476.78 32.5384 695.00 0.0000 301.36 40.6498 477.60 27.9034 696. 49 18.7207 302.85 42.7568 482.18 27.0471 696. 51 18.7214 256.23 37.8766 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.9707 306.78 40.8361 497.08 21.6388 697.49 23.9321 308.46 42 .1327 505.52 18.4348 702.65 19.8149 311. 90 37.2830 507.63 0.0000 706.68 21. 9391 316.51 . 37. 4240 511. 00 19.9146 711. 68 23.0339 319.41 0.0000 514.00 22.7979 720. 70 0.0000 320.08 0.0000 514.00 22.7979 7 21. 93 0.0000 321.04 28.3811 520.40 15.2533 722.78 17.3580 323.87 35.1384 520.69 0.0000 722. 91 17.3594 325.23 37.6895 522.65 0.0000 723. 31 11. 0486 328.76 0.0000 527.90 0.0000 724 .19 9.4739 333.37 34.1406 528.26 19.1496 727.33 22.1356 333.97 43.0126 529.59 18.2060 733.00 21. 5546 334.37 41. 7606 529.87 0.0000 735.93 20.1001 338.28 40.6191 531.02 0.0000 333.97 17.9961 338.32 40.6201 537.26 0.0000 739.50 0.0000 311. 90 25.4303 546.56 0.0000 747.24 17.0072 340.48 25.4303 552.55 18.4325 748.06 19 .1396 340.55 0.0000 563.25 22.4394 752.31 19.1733 344.28 28.0552 569.33 21.5318 753.82 0.0000 345.93 26.8140 946.00 20.5557 756.73 10. 6714 351. 06 33.3284 569.70 17.6206 756.80 10. 6718 351.93 33.3506 583.19 28.5858 884.68 21. 4063 Page 4181of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765. 81 31.0627 1274.44 6.9924 1620.50 6.1919 766.42 31.0709 1001.03 15.4075 1621. 92 7.2264 766.84 22.5031 1002 .'74 11. 2117 1678.03* 0.0000 772. 60 0.0000 1004.73 12.8548 1690.97 5.2386 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 6.8086 778.90 10.7682 1028.54 0.0000 1063.66 3.1952 783.70 0.0000 1037.84 i5.0597 1771.35 3.1959 785.37 8.6370 1038.76 0.0000 1791.20 0.0000 792.07 9.7427 631.29 13.3255 1808.65 5.3665 794.95 11. 37 97 1048.07 0.0000 1810.72 0.0000 795.86 11. 3835 1049.04 17.7808 1836.06 1.0792 810.06 4.9059 1050.41 12.4517 810.29 3.2710 1063.66 8. 9313 344.28 3. 2711 1077.00 0.0000 810.76 6.5432 1077.34 10.7629 815.77 0.0000 1085.87 16.1873 1048.07 0.0000 1093.63 8 .1129 832.01 18.1415 1099.45 12.6422 834.85 13.2085 1112. 07 11.7844 835. 71 13.2129 1112. 84 13.6002 836.80 0.0000 1115. 54 14.5186 846.75 0.0000 1120.29 12.7217 846.77 16.5851 1120.55 12.7225 856.80 0.0000 1221.41 10.1808 860.56 13.3369 1129. 67 16.4026 871.09 15.6201 1131. 51 0.0000 873.19. 16.7487 1147.95 0.0000 875.33 0.0000 1173.23 19.3812 879.38 11.1914 1177.95 10.1655 880.51 12.3155 1189.05 12;9797 883.24 15.6896 1204.77 11.1746 884.68 11.2130 1221. 41 8.9813 889.28 11. 2317 1231. 02 15.0088 894.76 8.440.2 1235.36 0.0000 898.04 13.5205 1238.28 15.0391 900.72 15.7893 1260.41 0.0000 903.28 15.8035 1271.87 9.4855 911.20 10.1880 1274.44 7.5938 912.08 10.1913 1274.54 7.5938 923.98 0.0000 1291.59 11. 4426 926.50 12. 5196 1298.22 0.0000 929.11 15.9482 1312 .11 0.0000 937.49 14.8525 1332.49 8.6743 944.13 0.0000 1362.66 0.0000 946.00 11. 4583 1365.19 4.8596 949.00 14. 9112 1368.63 0.0000 667.71 0.0000 1384.29 3.1250 962.31 19.5885 1408.01 7.8589 964. 08 19.0237 1457.56 0.0000 966 .17 15.5759 1460.82 11. 9407 911.20 15.0127 1489.16 2.0034 968. 97 15. 012T 1505.03 9.3840 983.53 0.0000 1584.12 3.0712 984.45 0.0000 1596.21 0.0000 Page 4182 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:51:13.42 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM01.CNF;402 Background date : Z-OCT-2016 10:59:55. Sample .date 2-DEC-2015 14:50:00. Acquisition date : 3-0CT-2016 07:50:44. Sample ID G405235056 Sample quantity 1.01481E+02 GRAM Detector name GAMOl Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.36 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 4 4 4 4 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4183 of 5809 Energy 63.24* 74.92 77.27* 84.19* 87.35 89.92 92.69* 118. 89 129.46 185. 72* 209.81 238.68* 241.62* 270.14 277.36 295.66* 301.88 329.38 338.46* 352.05* 402.08 435.49 463.09 510.91* 565.33* 583.25* 609.44* 661.77 719. 57 770.32 786.97 795.19 879.40 883.43 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 29 119 187 37 99 67 115 25 46 105 34 358 99 34 32 115 25 16 66 246 50 11 23 39 50 89 193 51 23 30 8 13 9 4 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 118 129 109 167 142 131 96 73 109 107 104 58 93 63 43 98 73 72 65 60 95 33 19 46 27 24 19 24 9 30 16 15 4 9 1.18 l.09 1.17 1.77 1. 64 1. 63 1.25 0.89 1. 07 1. 62 0. 96 1. 03 2.17 1.11 .0. 69 1.19 3. 81 1. 44 1. 04 1. 38 8.98 1.25 1. 49 2.44 5.07 1. 47 1. 39 1. 07 2.59 4.46 0.88 1. 42 0.96 0.53 127.18 150.53 155.24 169.08 175.39 180.54 186. 07 238.46 259.61 372.12 420.28 478.02 483.90 540.93 555.37 591.97 604.41 659.39 677.55 704.73 804.77 871. 57 926.77 1022.39 1131.21 1167. 05 1219.40 1324.04 1439.62 1541.09 1574.38 1590.81 1759.18 1767.23 124* 147 147 164 164 164 164 235. 256 365 415 474 474 535 552 585 598 651 672 700 790 865 922 1014 1122 1160 1215 1321 1435 1530 1568 1585 1756 1762 8 8.09E-03 70.2 15 3.30E-02 18.0 6.86E-01 15 5.20E-02 12.3 31 1.02E-02 68.8 1.36E+OO 31 2.76E-02 24.7 31 l.87E-02 37.0 31 3.20E-02 19.9 7 6. 90E-03 61. 0 10 1.28E-02 44.8 13 2.91E-02 23.7 10 9.49E-03 59.0 19 9.95E-02 6.3 6.39E+OO 19 2. 74E-02 31. 0 10 9.46E-03 46.7 8 8.81E-03 40.2 13 3.20E-02 20.2 12 6.95E-03 71.8 12 4.33E-03111.9 11 1.82E-02 27.5 12 6.82E-02 9.2 26 l.40E-02 55.5 10 2.92E-03106.2 8 6.31E-03 39.9 17 1.07E-02 49.4 18 1. 40E-02 28. 9 14 2.48E-02 16.2 12 5.36E-02 8.7 9 1.41E-02 22.5 11 6.47E-03 31.7 21 8.25E-03 50.5 8 2.22E-03 93.5 10 3.61E-03 62.3 7 2.36E-03 50.1 7 1.12E-03131. 8 Peak Search Report (continued) Page : 2 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 67* 63 20 1. 42 1823.70 1819 13 1. 76E-02 20.9 36 0 920.31. 9 13 0.94 1840.98 1833 11 2.37E-03 90.5 37 0 923.70 9 12 1.. 26 1847.74 1843 10 2.54E-03 83.7 38 0 969 .18 37 12 1.19 1938.68 1935 10 1. 03E-02 24.1 39 0 1043.52 9 5 1. 47 2087.31 2081 10 2.58E-03 55.4 40 0 1109.70 18 3 3.67 2219.61 2214 11 5.08E-03 29 .. 2 41 0 1120.23* 28 18 1. 84 2240.67 2236 10 7.86E-03 33.8 42 0 1225.45 6 12 0.50 2451.03 2447 8 1. 59E-03113. 3 43 0 1266.62 6 4 0.89 2533.33 2530 6 1.78E-03 63.9 44 0 1275.23 5 7 1. 39 2550.54 2543 10 l.26E-03122.l 45 0 1378.12 16 5 0.54 2756.24 2751 10 4.55E-03 35.3 46 0 1460.75* 288 0 1. 63 2921. 40 2914 14 7.99E-02 6.0 47 0 1589.26 8 1 1. 39 3178.30 3175 6 2.lOE-03 44.4 48 0 1764.50* 30 7 1. 53 3528.60 3522 10 8.19E-03 26. 0 49 0 1799.81 6 0 0.99 3599.17 3596 6 l.67E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 4184 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:51:15 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 14:50:00 G405235056 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:50:44 101.48 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAl 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4185 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:00.36 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* 1.095E+OO 2.878E-02 3. 596E-02 244.20 OK K-40 1460.82 10.66* 9.709E-01 1.922E+Ol 1.922E+Ol 11. 93 OK CD-109 88.03 3.70* 4.590E+OO 3.160E+OO 5.003E+OO 67.98 OK SN-126 64.28 9.60 2.294E+OO 9. 696E-01 9.696E-01 140.35 OK 86.94 8.90 4.590E+OO 1.314E+OO 1.314E+OO 67.98 OK 87.57 37.00* 4.590E+OO 3.160E-01 3.160E-01 67.98 OK BA-137M 661. 66 89.90* 1.883E+OO 2.112E-01 2.154E-01 44.91 OK CS-137 661. 66 85.10* 1.883E+OO 2.232E-01 2.275E-01 44.91 OK TL-208 277.37 6.60 3.944E+OO 8.703E-01 8.703E-01 80.47 OK 583.19 85.00* 2.090E+OO 3.536E-01 3.536E-01 32.35 OK 860.56 12.50

1. 520E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.328E+OO Line Not Found Absent 351. 06 12.92* 3.215E+OO 9.152E-01 9.152E-01 167.70 OK PB-212 74.82 10.28 3.532E+OO 1.722E+OO 1.722E+OO 52.62 OK 77.11 17.10 3.757E+OO 2.130E+OO 2.130E+OO 24.57 OK 238.63 43.60* 4.454E+OO 1. 321E+OO 1.321E+00 12.53 OK 300.09 3.30 3.690E+OO Line Not Found. Absent BI-214 609.32 45.49* 2.015E+OO 1.479E+OO 1.480E+00 17.43 OK 1120.29 14.92 1.223E+OO 1. 078E+OO . 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 OK PB-214 74.82 5.80 3.522E+OO Line Not Found <<INT Reject 77 .11 9.70 3.757E+OO 3.755E+OO 3.757E+OO 24.57 OK 87.09 3.41 4.572E+OO Line Not Found <<INT Reject 242.00 7.25 4.406E+OO Line Not Found <<INT Reject 295.22 18.42 3.737E+OO 1.193E+OO 1.193E+00 40.38 OK 351.93 35.60* 3.216E+OO Line Not Found <<INT Reject RN-219 271. 23 10.80 4.031E+OO 5.586E-01 5.586E-01 93.47 OK 401. 81 6.60* 2.865E+OO 1.886E+OO 1.886E+OO 110. 94 OK RN-222 609.32 45.49* 2.015E+OO 1.479E+OO 1.480E+OO 17.43 OK 1120. 29 14.92 1.223E+00 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+00 1.638E+OO 52.01 OK RA-224 240.99 4.10* 4. 411E+OO 1. 794E+OO 1.794E+OO 143 .11 OK RA-226 609.32 45.49* 2.015E+OO 1.479E+OO 1. 480E+OO 17.43 OK 1120. 29 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.638E+00 52.01 OK AC-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11.27 3.327E+OO 1.243E+OO 1.243E+OO 54.91 OK 794.95 4.25 1. 621E+OO 1.321E+OO 1.321E+OO 124.51 OK 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 1.181E+OO 1.181E+OO 41.80 OK 968.97 15.80 1. 379E+OO 1.190E+OO 1.190E+OO 48.16 OK RA-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.327E+OO 1.243E+00 1.243E+OO 54.91 OK 794.95 4.25 1. 621E+OO 1.321E+OO 1.321E+OO 124.51 OK 835. 71 1. 61 1.557E+OO Line Not Found Absent 911. 20 25.80* 1.450E+OO 1.181E+OO 1.181E+OO 41. 80 OK 968. 97 15.80 1. 379E+OO 1.190E+OO 1.190E+OO 48.16 OK TH-228 74.82 10.28 3.532E+OO 1. 722E+OO 1.722E+OO 52. 62 OK 77 .11 17.10 3.757E+OO 2 .130E+OO 2.130E+OO 24.57 OK Page 4186of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235056 Acquisition date 3-:-0CT-2016 07:50:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 4.454E+OO 1.321E+OO 1.321E+OO 12.53 OK 300.09 3.30 3.690E+OO Line Not Found Absent TH-229 85.43 14.70 4.354E+OO 4.200E-01 4.200E-01 137.59 OK 88.47 24.00 4.590E+OO 4.872E-01 4.873E-01 67.98 . OK 193.51 4.41* 5.168E+OO Line Not Found Absent 210.85 2.80 4.899E+OO 1.787E+OO 1. 787E+OO 118. 06 OK TH-230 609.32 45.49* 2.015E+OO l.479E+OO 1.480E+OO 17.43 OK 1120.29 14.92 l.223E+OO 1.078E+OO l.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.637E+OO 52.01 OK PA-231 283.69 1. 70 3.870E+OO Line Not Found Absent 301.36 5.35* 3. 671E+OO 9.078E-01 9.078E-01 143.69 OK TH-232 105.21 1.10 5.519E+OO -----. Line Not Found Absent 338.32 11. 27 3.327E+OO 1.243E+OO l.243E+00 54.91 OK 835.71 1. 61 l.557E+OO Line*Not Found Absent 911.20 25.80* l.450E+OO 1.181E+OO 1.181E+OO 41. 80 OK 968. 97 15.80 l.379E+OO 1.190E+OO l.190E+00 48.16 OK TH-234 63.29 3.70* 2.294E+OO 2.516E+OO 2.516E+OO 140.35 OK 92.59 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 OK U-234 609.32 45.49* 2.015E+OO 1.479E+OO 1.479E+OO 17.43 OK 1120.29 14.92 1.223E+00 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.637E+OO 52.01 OK U-235 89. 96 3.47 4.767E+OO 2. 967E+OO 2. 967E+OO 73.97 OK 93.35 5.60 4.940E+OO 3. 031E+OO 3. 031E+OO 39.80 OK 143.76 10. 96* 5.868E+OO Line Not Found Absent 163.33 5.08 5.647E+OO Line Not Found Absent 185. 72 57.20 5.297E+OO 2.485E-01 2.485E-01 47 .. 46 OK 205.31 5.01 4.973E+OO Line Not Found Absent U-238 63.29 3.70* 2.294E+OO 2.516E+OO 2.516E+OO 140. 35. OK 92.59 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 OK AM-243 43.53 5.90 3.822E-01 Line-Not Found Absent 74.66 67.20* 3.532E+OO 2.634E-01 2.634E-01 52.62 OK CM-247 278.00 3.40 3.944E+OO 1.689E+OO 1. 689E+OO 80.47 OK 287.50 2.00 3.826E+OO Line Not Found Absent 402.40 72.00* 2.865E+OO l.729E-01 1. 729E-01 110.94 OK ANH-511 511. 00 100.00* 2.335E+OO l.168E-01 ;t..168E-01 98.90 OK Flag: "*" = Keyline Page 4187 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:51:16.73 *************************"******************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l *
Acquisition date 3-0CT-2016 07:50:44 Sensitivity : 3.000 *
Detector ID GAMOl Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.36 Half life ratio : ***** *
Sample date 2-DEC-2015 14:50:00 Analyst initials: MXRl *
Sample ID G405235056 Sample Quantity 1.0148E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * **
Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Activity (pCi/GRAM 3. 596E-02 l.922E+Ol 5.003E+00 3.160E-01 2.154E-01 2.275E-01 3.536E-01 9.152E-01 1. 321E+OO 1.480E+OO 1.526E+OO 1.886E+OO 1.480E+OO 1.794E+OO 1.480E+OO 1.181E+OO 1.181E+OO 1.321E+OO -7.270E-01 1.480E+OO 9.078E-01 1.181E+OO 2.516E+OO 1.479E+00 l.323E-03 2.516E+OO 2.634E-01 1. 729E-01 l.168E-01 Cnt uncert ( 1. 96-sigma) 8.607E-02 2.247E+OO 3.333E+OO 2.105E-01 9.478E-02 1. OOlE-01 1.121E-01 1.504E+OO l.622E-01 2.528E-01 2.742E-01 2.050E+OO 2.528E-01 2.516E+OO 2.528E-01 4.839E-01 4.839E-01 1.622E-01 7.080E-01 2.527E-01 1.278E+OO 4.839E-01 3.460E+OO 2.527E-01 2.863E-01 3.460E+OO l.358E-01 1.879E-01 1.132E-01 Non-Identified Nuclides Nuclide BE-7 Page 4188 of 5809 Key-Line Activity (pCi/GRAM -8.317E+OO K.L. Cnt Uncert (1.96-sigma) l.757E+Ol MDA (pCi/GRAM 1.623E-01 9.665E-01 2.829E+00 1.799E-01 8.188E-02 8.650E-02 8.415E-02 5.541E-01 1.463E-01 1.585E-01 5.099E-01 l.157E+00 1.585E-01 1.569E+OO 1.585E-01 4.780E-01 4.780E-01 l.463E-01* 1. 211E+OO l.584E-01 1.149E+OO 4.780E-01 4.004E+OO 1.584E-01 5.332E-01 4.004E+OO 1.527E-01 l.062E-01 7.738E-02 MDA (pCi/GRAM 3 .114E+Ol NOT IDENT.

NA-24 O.OOOE+OO l.638E+41 0.000E+OO SHORT HLIF AL-26 -8.408E-03 4. 021E-02 8.619E-02 NOT IDENT. SC-46 -2.005E-01 4.825E-01 8.570E-01 FAIL ABUN V-48 O.OOOE+OO 2.715E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 7.276E+02 O.OOOE+OO SHORT HLIF MN-54 2.357E-02 9.243E-02 l.838E-01 NOT IDENT. C0-56 -1. 269E-01 7.765E-01 l.424E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 5.378E-02 7.240E-02 l.319E-01 NOT IDENT. C0-58 -5.712E-01 9.971E-01 1. 685E+OO NOT IDENT. FE-59 -3.805E+OO l.249E+Ol 2.198E+Ol NOT IDENT. C0-60 4. 963E-02 6.260E-02 l.449E-01 NOT IDENT. ZN-65 -2.445E-01 3.013E-01 3.769E-01 NOT IDENT. GE-68 -l.554E+OO 3.948E+OO 6.833E+OO NOT IDENT. AS-73 l.065E+OO l.931E+Ol 3.355E+Ol NOT IDENT. AS-74 O.OOOE+OO l .161E+04 O.OOOE+OO SHORT HLIF SE-75 4.107E-01 3.104E-01 6.141E-01 FAIL ABUN BR-77 O.OOOE+OO l.621E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO l.439E+03 O.OOOE+OO SHORT HLIF RB-83 2.602E-01 9.162E-01 l.828E+00 NOT IDENT. KR-85 3.894E+OO l.076E+Ol l.932E+Ol NOT IDENT. SR-85 4.377E-01 l.210E+OO 2.172E+OO NOT IDENT. RB-86 0.000E+OO 5.748E+04 O.OOOE+OO SHORT HLIF Y-88 -6.096E-02 3.556E-01 7.446E-01 NOT IDENT. Y-91 -7.074E+02 8.861E+02 1. 537E+03 NOT IDENT. NB-94 5.150E-03 4.562E-02 8.771E-02 NOT IDENT. NB-95 -8.782E-01 l.565E+OO 2.279E+OO NOT IDENT. NB-95M -l.423E+OO 4.446E+OO 7.129E+OO NOT IDENT. ZR-95 4.433E-01 2.447E+OO 4. 714E+OO NOT IDENT. NB-97 O.OOOE+OO l.436E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.223E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.*i57E+41 O.OOOE+OO SHORT HLIF RH-101 -2.685E-02 5.212E-02 8.382E-02 NOT IDENT. RH-102 -2.462E-02 9.129E-02 l.650E-Ol NOT IDENT. RU-103 -l.435E-01 9.725E+00 l.824E+Ol FAIL ABUN RH-106 8.675E-02 7.708E-01 l.479E+OO NOT IDENT. RU.:.106 8.675E-02 7.708E-01 l.479E+OO NOT IDENT. AG-108M 3.834E-02 4.025E-02 8.450E-02 NOT IDENT. AG-llOM 6.092E-02 l.573E-01 3 .112E-01 FAIL ABUN SN-113 7.437E-02 3.723E-01 6.830E-01 NOT IDENT. CD-115 O.OOOE+OO 2.779E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.803E+05 O.OOOE+OO SHORT HLIF TE-123M 6.262E-02 1. 880E-01 3.603E-01 NOT IDENT. SB-124 2.949E+OO 2.653E+00 7.907E+OO NOT IDENT. SB-125 7.366E-02 l.513E-01 3.017E-01 FAIL ABUN TE-125M 2.398E+02 5.144E+02 9.023E+02 NOT IDENT. I-126 O.OOOE+OO 2.205E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.043E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 9.620E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.308E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.284E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 2.104E+27 O.OOOE+OO SHORT HLIF BA-133 -2.190E-02 7.246E-02 l.157E-01 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 8.693E-02 l.061E-01 l.698E-01 FAIL ABUN CS-135 2.504E-02 2.262E-01 3.838E-01 NOT IDENT. I-135 O.OOOE+OO 8.597E+40 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 4.883E+05 O.OOOE+OO SHORT HLIF CE-139 -4.365E-03 1. 647E-01 3.064E-01 NOT IDENT. BA-140 O.OOOE+OO 2.606E+06 0. 00.0E+OO SHORT HLIF LA-140 O.OOOE+OO 8.560E+05 O.OOOE+OO SHORT HLIF CE-141 5.775E+OO 4.223E+Ol 7.912E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.250E-01 5.813E-01 9.450E-01 NOT IDENT. PM-144 -l.405E-02 9.562E-02 1. 735E-01 NOT IDENT. PR-144 -l.173E+OO 8.339E+OO l.515E+Ol NOT IDENT. PM-146 -5.622E-02 7.224E-02 l.217E-01 NOT IDENT. ND-147 O.OOOE+OO 7.615E+07 O.OOOE+OO SHORT HLIF PM-147 6. 631E+02 l.236E+03 2.213E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 l.302E-02 4.168E-02 7. 271E-02 FAIL ABUN EU-152 -4.123E-02 l.359E-01 2.460E-01 NOT IDENT. GD-153 -3.395E-02 3.lOlE-01 4. 791E-Ol NOT IDENT. EU-154 8.791E-02 2.104E-01 3.576E-01 FAIL ABUN EU-155 8.291E-02 l.812E-01 3.193E-01 FAIL ABUN TB-160 2.476E+OO 2.431E+OO 5.699E+OO FAIL ABUN H0-166M -1. 346E-02 8.706E-02 l.598E-01 FAIL ABUN Page 4189of5809 TM-171 -2.061E+OO 4.545E+Ol 7.822E+Ol NOT IDENT. HF-172 2.944E-01 3.454E-01 6.337E-01 FAIL ABUN LU-172 -2.267E-02 1.069E-01 1. 962E-01 FAIL ABUN LU-176 -1. 540E-02 3.814E-02 6.050E-02 FAIL ABUN HF-181 3.098E+OO 6.816E+OO l.368E+Ol NOT IDENT. TA-182 -4.430E-01 1. 488E+OO 2.471E+OO FAIL ABUN RE-183 -4.553E-01 6.173E+OO 1.058E+Ol NOT IDENT. RE-184 8.850E+OO 4.939E+Ol 9.761E+Ol NOT IDENT. W-188 -5.362E+Ol 1.982E+02 3.199E+02 FAIL ABUN IR-192 2.829E-01 7.398E-01 1.431E+OO FAIL ABUN HG-203 -3.501E+OO

4. 243E+OO 6.329E+OO NOT IDENT. BI-207 1. 941E-02 8.051E-02 l.573E-01 FAIL ABUN PB-210 -2.426E+OO 7.363E+OO 1.260E+Ol NOT IDENT. PB-211 -6.006E-01 1.022E+OO 1. 778E+OO NOT IDENT. BI-212 l.071E+OO 8.800E-01 1.856E+OO NOT IDENT. RA-223 -1. 870E-01 8.835E-01 1.445E+OO FAIL ABUN AC-227 -8.628E-02 3.606E-01 6.548E-01 NOT IDENT. TH-227 -8.628E-02 3.606E-01 6.548E-01 NOT IDENT. TH-231 -l.870E-01 8.835E-01 1.445E+OO FAIL ABUN PA-233 -2.617E-02 9.190E-02 l.663E-01 NOT IDENT. PA-234 -4.521E-01 4. 511E-01 6.750E-01 FAIL ABUN PA-234M l. lllE-01 8.053E+OO 1.541E+Ol NOT IDENT. NP-237 -2.617E-02 9.190E-02 l.663E-01 NOT IDENT. NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -8.382E-03 4.284E-01 6. 651E-01 FAIL ABUN. PU-239 8.918E+02 7.830E+02 9.430E+02 FAIL ABUN AM-241 -8.625E-02 2.930E-01 4.494E-01 NOT IDENT. CM-243 ...:5.985E-02 l.650E-01 2.708E-01 FAIL ABUN BK-247 8.175E-02 1. 086E-01 2.007E-01 FAIL ABUN CF-249 1. 794E-02 5.157E-02 1.014E-01 NOT IDENT. CF-251 1.485E-01 1.675E-01 3.313E-01 NOT IDENT. Page 4190of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:51:14.24 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error NA-22 1274.54 4 99.94* 1. 095E+OO 2.878E-02 3.596E-02 244.20 K-40 1460.82 269 10.66* 9.709E-01 1.922E+Ol 1.922E+Ol 11. 93 CD-109 88.03 98 3.70* 4.590E+OO 4.260E+OO 6.743E+OO 49.35 SN-126 64.28 29 9.60 2.294E+OO 9. 696E-01 9. 696E-01 140.35 86.94 98 8.90 4.590E+OO 1. 771E+OO 1. 771E+OO 49.35 87.57 98 37.00* 4.590E+OO 4.260E-01 4.260E-01 49.35 BA-137M 661. 66 48 89.90* 1.883E+OO 2 .112E-01 2.154E-01 44.91 CS-137 661.66 48 85.10* 1.883E+OO 2.232E-01 2.275E-01 44.91 TL-208 277.37 31 6.60 3.944E+OO 8.703E-01 8.703E-01 80.47 583.19 85 85.00* 2.090E+OO 3.536E-01 3.536E-01 32.35 860.56 ------12.50 l.520E+OO ------Line Not Found ------BI""'.211 72.87 ------1. 23 3.328E+00 ------Line Not Found ------351.06 236 12.92* 3.215E+OO 4.202E+OO 4.202E+OO 18.34 PB-212 74.82 118 10.28 3.532E+OO 2.395E+OO 2.395E+OO 36.09 77 .11 185 17.10 3.757E+OO 2 .130E+OO 2 .130E+00 24.57 238.63 347 43.60* 4.454E+OO 1.321E+OO 1.321E+OO 12.53 300.09 ------3.30 3.690E+OO ------Line Not Found ------BI-214 609.32 183 45.49* 2.015E+OO l.479E+OO 1. 480E+OO 17.43 1120.29 27 14.92 l.223E+OO 1. 078E+OO 1.078E+OO 67.61 1764.49 27 15.30 8 .116E-01 l.637E+OO 1.638E+OO 52.01 PB-214 74.82 118 5.80 3.532E+OO 4.244E+OO 4.246E+OO 36.09 77 .11 185 9.70 3.757E+OO 3.755E+OO 3.757E+OO 24.57 87.09 98 3.41 4.590E+OO 4.622E+OO 4.624E+00 49.35 242.00 95 7.25 4. 411E+OO 2.207E+OO 2.208E+OO 62.04 295.22 111 18.42 3.737E+OO l.193E+OO 1.193E+OO 40.38 351. 93 236 35.60* 3.215E+OO 1.525E+OO 1.526E+OO 18.34 RN-219 271.23 33 10.80 4. 031E+OO 5.586E-Oi 5.586E-01 93.47 401. 81 48 6.60* 2.865E+OO l.886E+OO 1.886E+OO 110. 94 RN-222 609.32 183 45.49* 2.015E+OO 1.479E+OO 1.480E+OO 17.43 1120.29 27 14.92 l.223E+OO l.078E+00 1. 078E+OO 67.61 1764.49 27 15.30 8 .116E-01 l.637E+00 1.638E+OO 52.01 RA-224 240.99 95 4.10* 4. 411E+OO 3.903E+00 3.903E+OO 62.04 RA-226 609.32 183 45.49* 2.015E+OO 1. 479E+OO 1. 480E+OO 17.43 1120.29 27 14.92 l.223E+OO 1.078E+OO 1.078E+OO 1764.49 27 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 AC-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3. 327E+00
l.243E+00 1.243E+OO 54 .*91 794.95 12 4.25 l.621E+OO l.321E+OO 1. 321E+OO 124.51 835.71 ------1. 61 l.557E+00 ------Line Not Found ------911.20 60 25.80* 1.450E+OO l .181E+OO 1.181E+OO 41. 80 968. 97 35 15.80 1.379E+OO l.190E+OO l.190E+00 48.16 RA-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.327E+OO l.243E+00 1.243E+00 54.91 794.95 12 4.25 1. 621E+OO 1.321E+OO l.321E+OO 124.51 835. 71 ------1. 61 1.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+00 l. lBlE+OO 1.181E+OO 41. 80 968.97 35 15.80 1.379E+OO l.190E+OO 1.190E+OO 48.16 Page of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 118 10.28 3*. 532E+OO 2.395E+00 2.395E+OO 36.09 77 .11 185 17.10 3.757E+OO 2.130E+OO 2.130E+OO 24.57 238.63 347 43.60* 4.454E+OO 1.321E+OO 1.321E+OO 12.53 300.09 ------3.30 3.690E+OO ------Line Not Found ------TH-229 85.43 36 14. 70. 4.354E+OO 4.200E-01 4.200E-01 137.59 88.47 98 24.00 4.590E+OO 6.567E-01 '6.568E-01 49.35 193.51 ------4.41* 5.168E+OO ------Line Not Found ------210.85 33 2.80 4.899E+OO 1.787E+OO 1. 787E+OO 118. 06 TH-230 609.32 183 45.49* 2.015E+OO l.4'79E+OO 1.480E+OO 17.43 1120.29 27 14.92 1.223E+OO l.078E+OO l.078E+00 67.61 1764.49 27 15.30 8 .116E-01 l.637E+OO l.637E+OO 52.01 PA-231 283.69 ------1. 70 3.870E+OO ------Line Not Found ------301.36 24 5.35* 3.671E+OO 9 .. 078E-01 9.078E-01 143.69 TH-232 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.327E+OO l.243E+OO l.243E+OO 54.91 835. 71 ------1. 61 l.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+OO l.181E+OO l.181E+00 41. 80 968.97 35 15.80 1.3'79E+OO 1.190E+OO 1.190E+OO 48.16 TH-234 63.29 29 3.70* 2.294E+OO 2.516E+OO 2.516E+00 140.35 92.59 113 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 U-234 609.32 183 45.49* 2.015E+OO 1. 4 7 9E+00 1.479E+OO 17.43 1120.29 27 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67. 61 1764.49 27 15.30 8 .116E-01 l.637E+OO 1.637E+OO 52.01 U-235 89.96 66 3.47 4.767E+OO 2. 967E+OO 2. 967E+OO 73.97 93.35 113 5.60 4.940E+OO 3. 031E+OO 3. 031E+OO 39.80 143.76 ------10. 96* 5.868E+OO ------Line Not Found ------163.33 ------5.08 5.647E+OO ------Line Not Found ------185.72 102 57.20 5.297E+OO 2.485E-01 2.485E-01 47.46 205.31 ------5.01 4.973E+OO ------Line Not Found ------U-238 63.29 29 3.70* 2.294E+00 2.516E+OO 2.516E+OO 140.35 92.59 113 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 AM-243 43.53 ------5.90 3.822E-01 ------Line Not Found ------74.66 118 67.20* 3.532E+OO 3.663E-01 3.663E-01 36.09 CM-247 278.00 31 3.40 3.944E+OO 1. 689E+OO 1. 68 9E+OO 80.47 287.50 ------2.00 3.826E+OO ------Line Not Found ------402.40 48 72.00* 2.865E+OO l.729E-01 1.729E-01 110. 94 ANH-511 511. 00 37 100.00* 2.335E+OO l.168E-01 l.168E-01 98.90 Flag: "*" Key line *Page 4192 of 5 809 Page : 3 Summary of Nuclide Activity Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Total number of lines in spectrum 49 Number of unidentified lines 12 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide NA-22 K-40 CD-109 SN-126 *BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Hlife 2.60Y 1. 25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 7.04E+08Y 1600. OOY 1.41E+10Y 1600. OOY 1. 41E+10Y 1.41E+10Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7. 0.4E+08Y 4.47E+09Y 7370.00Y 1.56E+07Y 1.00E+09Y Decay 1. 25 1. 00 1. 58 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.*00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 2.878E-02 1.922E+Ol 4.260E+OO 4.260E-01 2 .112E-01 2.232E-01 3.536E-01 4.202E+OO 1. 321E+OO 1. 479E-f-OO 1.525E+OO l.886E+00 1.479E+OO 3.903E+OO 1.479E+00 1.181E+OO 1.181E+OO 1. 321E+OO 6.567E-01 1.479E+OO 9.078E-01 1.181E+OO 2.516E+OO 1.479E+OO 2.485E-01 2.516E+OO 3.663E-01 l.729E-01 l.168E-01 5.732E+Ol 5.732E+Ol Decay Corr pCi/GRAM 3. 596E-02 1.922E+Ol 6.743E+OO 4.260E-01 2.154E-01 2.275E-01 3.536E-01 4.202E+OO 1. 321E+OO 1.480E+OO 1.526E+OO 1.886E+OO 1.480E+OO 3.903E+OO 1.480E+OO 1.181E+OO 1.181E+OO 1.321E+OO 6.568E-01 1.480E+OO 9.078E-01 1.181E+OO 2.516E+OO 1.479E+OO 2.485E-01 2.516E+OO 3.663E-01 1.729E-01 1.168E-01 5.982E+Ol 5.982E+Ol 75.51% Decay Corr 2-Sigma Error 8.782E-02 0.229E+Ol 3.327E+OO 2.102E-01 0.967E-01 1.022E-01 1.144E-01 0. 771E+OO 0.166E+OO 0.258E+OO 0.280E+OO 2.092E+OO 0.258E+00 2.422E+OO 0.258E+00 0.494E+OO 0.494E+OO 0.166E+00 3. 241E-01 0.258E+OO 13.04E-01 0 .. 494E+OO 3.531E+OO 0.258E+OO 1.179E-01 3. 531E+OO 1.322E-01 1.918E-01 1.155E-01 "M" = Manually accepted 2-Sigma %Error 244.20 11. 93 49.35 49.35 44.91 44.91 32.35 18.34 12.53 17.43 18.34 110. 94 17.43 62. 04 17.43 41. 80 41. 80 12.53 49.35 17.43 143.69 41. 80 140.35 17.43 47.46 140.35 36.09 110. 94 98.90 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4193 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235056 Acquisition date : 3-0CT-2016 07:50:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 118. 89 24 72 0.89 238.46 235 7 6.90E-03 **** 5.83E+OO T 0 129.46 45 107 1. 07 259.61 256 10 1.28E-02 89.6 5.91E+OO T 0 329.38 15 70 1. 44 659.39 651 12 4.33E-03 **** 3.41E+OO T 0 435.49 10 31 1. 25 871.57 865 10 2.92E-03 **** 2.67E+OO 0 463.09 22 18 1. 49 926.77 922 8 6.31E-03 79.7 2.54E+OO T 0 565.33 48 26 5.07 1131.21 1122 18 1.40E-02 57.7 2.14E+OO 0 719.57 22 8 2.59 1439.62 1435 11 6.47E-03 63.5 1. 76E+OO T 0 770.32 28 29 4.46 1541.09 1530 21 8.25E-03 **** 1. 66E+OO 0 786.97 8 15 0.88 1574.38 1568 8 2.22E-03 **** 1.63E+OO 0 879.40 8 3 0. 96 1759.18 1756 7 2.36E-03 **** 1.49E+OO T 0 883.43 4 8 0.53 1767.23 1762 7 l.12E-03 **** 1. 49E+OO T 0 920.31 8 13 0.94 1840.98 1833 11 2.37E-03 **** 1. 44E+OO 0 923.70 9 11 1.26 1847.74 1843 10 2.54E-03 **** 1. 43E+OO T 0 1043.52 9 4 1. 47 2087. 31 .2081* 10 2.58E-03 **** 1.30E+OO 0 1109.70 17 3 3.67 2219.61 2214 11 5.08E-03 58.5 1.23E+OO 0 1225.45 5 12 0.50 2451.03 2447 8 l.59E-03 **** 1.13E+OO 0 1266.62 6 3 0.89 2533.33 2530 6 1. 78E-03 ****
1. lOE+OO *o 1378.12 15 4 0.54 2756.24 2751 10 4.55E-03 70.7 1.02E+OO 0 1589.26 7 1 1. 39 3178.30 3175 6 2.lOE-03 88.8 8.98E-01 0 1799.81 6 0 0.99 3599.17 3596 6 l.67E-03 81. 6 7. 96E-01 Flags: "T" = Tentatively Page 4194of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:51:28.87 *******************************************************************************
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DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l *
Acquisition date 3-0CT-2016 07:50:44 Sensitivity : 3.000 *
Detector ID GAMOl Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.36 Half life ratio : ***** *
Sample date .. 2-DEC-2015 14: 50: 00 Nuclide Library : SOLID* *
Sample ID G405235056 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.0148E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************** * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
Eff: File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 6.986E-02 3.874E-01 1.323E+OO 8.413E-02 3. 496E-02 3. 693E-02 3.648E-02 2.532E-01 6.806E-02 6.839E-02 2.464E-01 5.262E-01 6.839E-02 7.297E-01 6.839E-02 2.125E-01 2.125E-01 6.806E-02 5.620E-01 6.836E-02 5.241E-01 2.125E-01 1.885E+OO 6.836E-02 2.512E-01 1. 885E+OO 7.211E-02 4.830E-02 3.443E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-24 Page 4195 of 5809 Le_ (pCi/GRAM 1.350E+Ol NOT IDENT. O.OOOE+OO SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M *I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-t44 PM-146 ND-147 PM...:147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 4196 of 5809 3.054E-02 3.443E-01 O.OOOE+OO O.OOOE+OO 7.935E-02 6 .115E-01 O.OOOE+OO 6.163E-02 7.182E-01 9.336E+OO 6.197E-02 1.504E-01 2.883E+OO l.568E+Ol O.OOOE+OO 2.829E-01 O.OOOE+OO O.OOOE+OO 8.018E-01 8.619E+OO 9.688E-01 O.OOOE+OO 2.788E-01 6.447E+02 3. 831E-02 9.765E-01 3.321E+OO 2. 061E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3. 896E-02 7.191E-02 8 .113E+OO 6.501E-01 6. 501E-01 3. 81*5E-02 l.342E-01 3.086E-01 0.000E+OO O.OOOE+OO 1.679E-01 3 .121E+OO l.357E-01 4.250E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 5.254E-02 O.OOOE+OO 7.540E-02 l.766E-01 O.OOOE+OO *O.OOOE+OO 1.429E-01 O.OOOE+OO O.OOOE+OO 3.718E+Ol O.OOOE+OO 4.406E-01 7.687E-02 6. 711E+OO 5.426E-02 O.OOOE+OO 1.032E+03 O.OOOE+OO 3. 323E-02
1.111E-01 2.236E-01 1. 511E-01 1.500E-01 2.436E+OO 6.956E-02 3.657E+Ol NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 w-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4197of5809 2. 965E-01 8.087E-02 2.732E-02 6. 096E+OO 1.030E+OO 4.942E+OO 4. l 71E+Ol 1.464E+02 6.554E-01 2. 871E+OO 6.806E-02 5.898E+OO 7. 966E-01 8.428E-01 6.507E-01 3.026E-01 3.026E-01 6.507E-01 7.591E-02 2.787E-01 6.829E+00 7.591E-02 O.OOOE+OO 3. llOE-01 4.449E+02 2.099E-01 1. 265E-01 9.228E-02 4.558E-02 1. 551E-01 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:51:34.75 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l * *Acquisition date 3-0CT-2016 07:50:44 Sensitivity : 3.0QO *
Detector ID GAMOl Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.36 Half life ratio : ***** *
Sample date 2-DEC-2015,i4:50:00 Nuclide Library : SOLID *
Sample ID G405235056 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.0148E+02 GRAM *
Quantity Err(%) 1.9708E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 . * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN '*
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides . Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) NA-22 3. 596E-02 8.608E-02 8.608E-02 K-40 1.922E+Ol 2.460E+OO 2.460E+OO CD-109 5.003E+OO 3.365E+OO 3.365E+OO SN-126 3.160E-01 2 .119E-01 2 .119E-01 BA-137M 2.154E-01 9.523E-02 9.523E-02 CS-137 2.275E-01 1. 006E-01 l.006E-01 TL-208 3.536E-01 l.131E-01 l .131E-01 BI-211 9.152E-01 1.518E+OO 1.518E+OO PB-212 1.321E+OO 1. 766E.-01 1. 766E-01 BI-214 1. 480E+OO 2.607E-01 2.607E-01 PB-214 1.526E+OO 2.815E-01 2.815E-01 RN-219 1.886E+OO 2.064E+OO 2.064E+OO RN-222 1.480E+OO 2.607E-01 2.607E-01 RA-224 1. 794E+OO 2.521E+OO 2. 521E+OO RA-226 1.480E+OO 2.607E-01 2.607E-01 AC-228 1.181E+OO 4.876E-01 4.876E-01 RA-228 1.181E+OO 4.876E-01 4.876E-01 TH-228 1.321E+OO 1. 7 66E-01 1. 766E-01 TH-229 -7.270E-01 7.088E-01 7.088E-01 TH-230 1.480E+OO 2.606E-01 2.606E-01 PA-231 9.078E-01 1.293E+OO 1. 293E+OO TH-232 1.181E+OO 4.876E-01 4.876E-01 TH-234 2.516E+OO 3.505E+OO 3.505E+OO U-234 1. 479E+OO 2.606E-01 2.606E-01 U-235 1.323E-03 '2. 863E-01 2.863E-01 U-238 2.516E+OO 3.505E+OO 3.505E+OO AM-243 2.634E-01 l.374E-01 l.374E-01 CM-247 l.729E-01 l.902E-01 l.902E-01 ANH-511 l.168E-01 1.133E-01 l.133E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -8.317E+00 1. 757E+Ol 1. 796E+Ol NOT IDENT. Page 4198of5809 NA-24 1. OOOE+41 l.698E+41 O.OOOE+OO SHORT HLIF AL-26 -8.408E-03 4.022E-02 4.039E-02 NOT IDENT. SC-46 -2.005E.:_01 4.826E-01 4.910E-Ol FAIL ABUN V-48 2.328E+04 2.716E+04 2.912E+04 SHORT HLIF CR-51 7. 961E+Ol 7.276E+02 7.285E+02 SHORT HLIF MN-54 2.357E-02 9.243E-02 9.304E-02 NOT IDENT. C0-56 -1.269E-01 7.766E-01 7.787E-01 NOT IDENT. MN-56 -l.000E+41 6.597E+41 O.OOOE+OO SHORT.HLIF C0-57 5.378E-02 7.244E-02 7.639E-02 NOT IDENT. -5.712E-01 9.974E-01 l.030E+OO NOT IDENT. FE-59 -3.805E+OO 1. 249E+Ol l.261E+Ol NOT IDENT. C0-60 4. 963E-02 6.263E-02 6.651E-02 NOT IDENT. ZN-65 -2.445E-01 3.014E-01 3.209E-01 NOT IDENT. GE-68 -l.554E+OO 3.948E+OO 4.0lOE+OO NOT IDENT. AS-73 l.065E+OO l.931E+Ol l.931E+Ol NOT IDENT. AS-74 -8.097E+03 l.163E+04 l.218E+04 SHORT HLIF SE-75 4.107E-01 3. lllE-01 3.620E-01 FAIL ABUN BR-77 l.320E+39 l.165E+40 O.OOOE+OO SHORT HLIF SR-82 -l.120E+03 l.440E+03 l.526E+03 SHORT HLIF RB-83 2.602E-01 9.169E-01 9.243E-01 NOT IDENT. KR-85 3.894E+OO l.076E+Ol l.091E+Ol NOT IDENT. SR-85 4.377E-01 l.210E+00 1.226E+OO NOT IDENT. RB-86 -2.691E+04 5.749E+04 5.876E+04 SHORT HLIF Y-88 -6.096E-02 3.557E-01 3.567E-01 NOT IDENT. Y-91 -7.074E+02 8.865E+02 9. 421E+02 NOT IDENT. NB-94 5.150E-03 4.563E-02 4.568E-02 NOT IDENT. NB-95 -8.782E-01 l.565E+OO 1. 615E+OO NOT IDENT. NB-95M -l.'423E+OO 4.448E+OO 4.494E+OO NOT IDENT. ZR-95 4.433E-01 2.448E+OO 2.456E+00 NOT IDENT. NB-97 -l.OOOE+41 l.437E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 2.376E+41 0.000E+OO SHORT HLIF M0-99 -1. l 77E+33 l.226E+33 O.OOOE+OO SHORT HLIF TC-99M 1. OOOE+41 l.659E+41 O.OOOE+OO SHORT HLIF RH-101 -2.685E-02 5.235E-02 5.373E-02 NOT IDENT. RH-102 -2.462E-02 9 .131E-02 9.199E-02 NOT IDENT. RU-103 -l.435E-01 9. 725E+OO 9. 725E+OO FAIL ABUN RH-106 8.675E-02 7.708E-01 7.718E-01 NOT IDENT. RU-106 8.675E-Ci2 7.708E-01 7.718E.:.01 NOT IDENT. AG-108M 3.834E-02 4.028E-02 4.383E-02 NOT IDENT. AG-llOM 6.092E-02 1. 573E-01 l.597E-01 FAIL ABUN SN-113 7.437E-02 3.723E-01 3.738E-01 NOT IDENT. CD-115 2.222E+40 2.809E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 8.576E+04 1. 806E+05 1. 847E+05 SHORT HLIF TE-123M 6.262E-02 1. 880E-01 l.901E-01 NOT IDENT. SB-124 2.949E+OO 2.657E+OO 2.971E+OO NOT IDENT. SB-125 7.366E-02 l.514E-01 l.550E-01 FAIL ABUN TE-125M 2.398E+02 5.146E+02 5.258E+02 NOT IDENT. I-126 -2.409E+05 2.205E+06 2.208E+06 SHORT HLIF SB-126 4.891E+o6 3.182E+06 3. 871E+06 SHORT HLIF SB-127 -3.246E+22 l.064E+23 O.OOOE+OO SHORT HLIF I-131 -8.032E+09 l.309E+l0 l.358E+l0 SHORT HLIF I-132 l.OOOE+41 1. 889E+42 O.OOOE+OO SHORT HLIF TE-132 4.936E+26 2 .114E+27 O.OOOE+OO SHORT HLIF BA-133 -2.190E-02 7.247E-02 7;314E-02 FAIL ABUN I-133 -l.OOOE+41 9.507E+41 O.OOOE+OO SHORT HLIF CS-134 8.693E-02 l.061E-01 l .131E-01 FAIL ABUN CS-135 2.504E-02. 2.262E-01 2.265E-01 NOT IDENT. I-135 -1.000E+41 6. 961E+41. O.OOOE+OO SHORT HLIF CS-136 -3.382E+04 4.883E+05 4.886E+05 SHORT HLIF CE-139 -4.365E-03 1. 647E-01 1. 647E-01 NOT IDENT. BA-140 -l.651E+06 2.607E+06 2.711E+06 SHORT HLIF LA-140 -2.335E+05 8.560E+05 8.625E+05 SHORT HLIF CE-141 5.775E+OO 4.223E+Ol 4.231E+Ol NOT IDENT. CE-143 l.000E+41 2.275E+41 O.OOOE+OO SHORT HLIF CE-144 -2.250E-01 5.814E-01 5.902E-01 NOT IDENT. PM-144 -1. 405E-02 9.562E-02 9.583E-02 NOT IDENT. PR-144 -1. l 73E+OO 8.339E+OO 8.356E+OO NOT IDENT. PM-146 -5.622E-02 7.235E-02 7.666E-02 NOT IDENT. ND-147 7:175E+06 7.615E+07 7.622E+07 SHORT HLIF PM-147 6.631E+02 l.236E+03 1. 272E+03 NOT IDENT. PM-149 l.OOOE+41 4. ll 7.E+41 O.OOOE+OO SHORT HLIF EU-150 l.302E-02 4.168E-02 4.209E-02 FAIL ABUN .EU-152 -4.123E-02 l.359E-01 l.371E-01 NOT IDENT. GD-153 -3.395E-02 3. lOlE-01 3.105E-01 NOT IDENT. EU-154 8.791E-02 2.104E-01 2.141E-01 FAih ABUN EU-155 8.291E-02 l.813E-01 l.851E-01 FAIL ABUN TB-160 2.476E+00 2.435E+OO 2.679E+OO FAIL ABUN H0-166M -l.346E-02 8.707E-02 8.728E-02 FAIL ABUN Page 4199of5809 TM-171 -2.061E+OO 4.545E+Ol 4.546E+Ol NOT IDENT. HF-172 2.944E-01 3.487E-01 3. 731E-01 FAIL ABUN LU-172 -2.267E-02 1.069E-01 1. 074E-01 FAIL ABUN LU-176 -l.540E-02 3.814E-02 3.877E-02 FAIL ABUN HF-181 3.098E+OO 6.818E+OO 6.959E+OO NOT IDENT. TA-182 -4.430E-01 l.488E+OO 1.502E+OO FAIL ABUN RE-183 -4.553E-01 6.173E+OO 6.176E+OO NOT IDENT. RE-184 8.850E+OO 4.944E+Ol 4. 960E+Ol NOT IDENT. W-188 l.983E+02 1.998E+02 FAIL ABUN IR-192 2.829E-01 7.399E-01 7.508E-01 FAIL ABUN HG-203 -3.501E+OO 4.246E+OO 4.530E+OO NOT IDENT. BI-207 1.941E-02 8.051E-02 8.099E-02 FAIL ABUN PB-210 -2.426E+OO 7.366E+OO 7.447E+OO NOT IDENT. PB-211 -6.006E-01 l.023E+OO 1.058E+OO NOT IDENT. BI-212 1. 071E+OO 8.816E-01 l.005E+OO NOT IDENT. RA-223 -1.870E-01 8.835E-01 8.875E-01 FAIL ABUN AC-227 -8.628E-02 3.608E-01 3.629E-01 NOT IDENT. TH-227 -8.628E-02 3.608E-01 3.629E-01 NOT IDENT. TH-231 -l.870E-01 8.835E-01 8.875E-01 FAIL ABUN PA-233 -2.617E-02 9.i90E-02 9.266E-02 NOT IDENT. PA-234 -4.521E-01 6.863E-01 7.160E-01 FAIL ABUN PA-234M l. lllE-01 8.053E+OO 8.053E+OO NOT IDENT. NP-237 -2.617E-02 9.190E-02 9.266E-02 NOT IDENT. NP-238 l.000E+41 O.OOOE+OO SHORT HLIF NP-239 -8.382E-03 4.284E-01 4.284E-01 FAIL ABUN PU-239 8.918E+02 7.840E+02 8. 811E+02 FAIL ABUN AM-241 -8. 625E-*02 2.930E-01 2.956E-01 NOT IDENT. CM-243 -5.985E-02 1. 651E-01 1. 673E-01 FAIL ABUN BK-247 8.175E-02 1. 098E-01 l.158E-01 FAIL ABUN CF-249 1. 794E-02 5.159E-02 5.222E-02 NOT IDENT. CF-251 l.485E-01 1.683E-01 1.811E-01 ,NOT IDENT. Page 4200 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 80.8814 879.38 69.2091 482.18 68.1542 45.60 59.0989 87.57 69.2191 133.52 73.2301 46.54 70.7781 87.09 69.2291 2 64. 66 61.5581 49. 72 0.0000 87.57 69.2607 122.06 61. 5789 51. 35 67.7282 88.03 69.2909 140.51 0.0000 51. 87 73.6162 88.34 69.3113 143.76 78.0153 5Z. 39 70.1573 193.51 69.3196 144.24 72. 9518 52.97 60.8478 89. 96 69.4170 145.44 78.1079 53.44 66.7384 90.64 69.4609 152.43 73.3682 125.81 72. 6501 91.11 0.0000 153.25 0.0000 57.36 0.0000 63.29 69.5866 154.21 55.5202 57.53 70.6071 143.76 69.6349 156.02 0.0000 57.98 68.2905 94'. 56 69. 7118 158.56 0.0000 1093.63 75.4714 94.65 69.7175 159.00 55.6994 57.98 75.4761 94.67 69.7188 162.33 66 .1280' 59.54 75.4958 94.87 69.7314 162.66 0.0000 60. 96 56.7167 97.43 65.3963 163.33 53.2813 61.17 69.3375 311. 90 65.4545 165.86 64.5592 62.93 86.4541 946.00 65.4553 176.31 71.9234 63.29 86.4899 99.53 61.4235 1048.07 0.0000 63.58 86.5186 1221. 41 62.6839 177.52 52.8991 64.28 94.8906 265.00 72. 6382 739.50 0.0000 66.73 74.5357 103.18 76.4078 181.52 70. 4177 67.24 79.3386 103.37 76.4206 711.68 65.3168 67.68 86.9181 116.74 76.4206 185. 72 65.3687 67.75 95.2594 105.21 69.1340 193.51 77.9338 69.67 95.4602 105.31 69.1400 197.03 61.4230 70.83 79.6499 106.12 71. 6584 127.23 65.8485 72.81 90.9928 106.47 77.8589 306.78 57.1950 279.20 90.9986 109.28 75.5659 203.43 56.3672 72. 87 90.9986 111. 00 88.0794 205.31 68. 7713 74.66 97.1676 228.16 0.0000 210.85 51. 7403 74.82 97.1837 114. 06 78.3511 215.65 68.2852 1063.66 97.1988 116. 30 0.0000 222 .11 48.0580 238.63 97.4136 116.74 69.7966 290.67 55.3260 351. 93 97.4136 119.76 73. 2962 177.52 58.9048 78.74 97.5755 121.12 56.2816 228.16 0.0000 79.69 81.9936 121. 22 52.5336 228.18 52. 6795 80.12 67.5532 121. 78 51. 3054 235.69 69.9210 80.19 0.0000 122.06 51.3166 256.23 65. 8968 80.57 82.0657 122.92 68 .1341 238.63 59.2552 81. 00 82.1010 123.07 68.1419 238.98 0.0000 81. 07 82.1067 123.68 76.8632 240.99 59.3278 81. 75 74.9126 125.81 51.4658 242.00 59.3586 323.87 69.0091 127.23 70.3711 344.28 43.2295 84.00 69.0234 127.91 75.4367 252.40 0.0000 85.43 69.1191 129.30 63.7694 252.80 61. 4936 86.55 69.1935 131.20 64.2807 254.15 0.0000 Page 4201 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 256.23 54 .*3518 351. 93 37.8206 583.19 14.3241 260.90 0.0000 "507.63 0.0000 584.27 14.3287 264.66 23.1955 356.01 38.3568 595.83 0.0000 264.80 30.0197 364.49 0.0000 600.60 21.5947 265.00 30.0224 366.42 0.0000 602.52 0.0000 268.22 42.3705 372. 51 22.8794 604. 72 24.7090 269.46 37.3815 129.30 37.2163 607.14 24.7256 270.03 37.3915 377.52 23.8795 609.32 13.4015 271.23 50.6447 383.85 33.5132 497.08 13.4052 273.65 0.0000 388.16 22.0590 433.94 7.7423 356.01 57.6308 388.63 0.0000 6'96. 49 23.7684 277.37 40.2680 391.69 26.5067 620. 36 18.6138 277.60 40. 2725 .400.66 33.7268 621.93 16.5527 278.00 40.2805 401.81 33.7418 667.71 0.0000 279.20 48.0887 402.40 33.7489 631.29 18.6702 279.54 48.0962 404.85 33.7795 453.88 14.5292 279.70 48.1004 410.95 34.8230 595.83 0.0000 280.46 39.8688 413.71 24.2071 635.95 18.6943 283.69 40.3879 414.70 0.0000 636.99 0.0000 364.49 0.0000 423.72 0.0000 645.85 18.7449 285.41 42.2574 404.85 28.2165 884.68 18.8057 285.90 0.0000 427.87 20.4386 657.90 0.0000 402.40 44.1377 433.94 16.5812 661. 66 11. 5044 290.67 44.2021 333.97 20.5223 664.57 0.0000 293.27 0.0000 453.88 34.3762 666.33 0.0000 295.22 38.7572 463.37 22.1709 720. 70 0.0000 295.96 38.7700 468.07 27.6343 667. 71 0.0000 298.58 41.5887 685.70 0.0000 677.62 16.8047 299.98 36.0666 475.06 22.7529 685.70 0.0000 300.09 36.0682 476.78 18.8067 695.00 0.0000 300.13 36.0690 477.60 19.8018 696.49 22.1647 301.36 36.0888 482.18 16.8575 696. 51 22.1647 302.85 36.1126 1596.21 0.0000 697.00 o.oocio 304.50 29.1897 527.90 0.0000 697.30 14.7799 537.26 0.0000 497.08 21. 9221 697.49 14.7804 306.78 36.1761 505.52 23.9800 702.65 14.7998 316.51 37.1313 507.63 0.0000 706.68 20.1063 311. 90 41. 8359 511. 00 22.0204 711. 68 16.9538 316.51 33.5361 514.00 18.0337 720.70 0.0000 531. 02 0.0000 514.00 18.0337 721. 93 0.0000 320.08 0.0000 520.40 14.0547 1690.97 12.7510 427.87 27.0683 238.98 0.0000 722. 91 12.7515 323.87 30.8395 522.65 0.0000 1274.44 19.1287 325.23 28.0518 527.90 0.0000 724 .19 27.1052 328.76 0.0000 528.26 17.1086 727.33 15.9570 388.16 39.4083 520.40 22.1495 733.00 12.7837 333.97 32.3795 529.87 0.0000 735.93 11. 72 69 334.37 29.5691 531.02 0.0000 737.46 11. 7314 338.28 36.6688 537.26 0.0000 739.50 0.0000 911.20 36.6696 546.56 0.0000 747.24 12.8291 340.48 36.7021 552.55 18.2505 748.06 8.5544 340.55 0.0000 563.25 18.3091 752.31 9.6335 344.28 33.9324 795.86 22.9276 753.82 0.0000 345.93 30.1829 569.50 21. 3999 756.73 12.8589 351.06 37.8076 569.70 21. 4016 756.80 12.8589 Page 4202 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:04.97 ********************************************************************************
GEL Laboratories LLC* *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date 2-DEC-2015 14:55:00. Acquisition date : 3-0CT-2016 07:51:32. Sample ID G405235057 Sample quantity l.15835E+02 GRAM Detector name GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.59 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 . Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 1 1 1 5 5 5 5 0 3 3 0 0 0 0 3 3 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4204 of 5809 Energy 31. 49 46.20* 62.83* 72.69 74.52* 76.70* 83.62* 86.72* 89.64 92.39* 117. 65 128.93 130. 85 143.91* 185.50* 209.04 231. 7 6 238.36* 241.38 269.63 276.86 284.39 287.37 294.89* 299.82 310.55 327.51 338.09* 351.68* 373.77 463 .11 510.47* 583.14* 609.27* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 24 37 129 36 241 384 56 141 120 133 33 45 36 12 93 35 20 424 130 40 18 15 41 169 29 26 29 119 *259 19 34 44 115 205 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 93 164 200 136 137 139 118 150 107 118 73 77 59 135 101 88 69 59 58 39 66 64 31 57 67 47 35 45 68 33 26 67 42 27 0.53 0.70 0.90 0.93 0.94 0.94 0.96 1. 41 1. 03 1.15 1. 66 1. 28 1.17 1. 40 0.87 1. 04 1. 82 0.96 1. 50 1. 55 1. 56 4.54 2.31 1. 09 1.12 3.44 1. 59 1.11 1. 05 1. 57 1.17 1. 39 1. 27 1. 24 64.83 94.21 127.46 147.17 150.83 155.17 169.01 175.21 181.04 186.54 237.01 259.56 263.40 289.50 372. 62 419.68 465.07 478.27 484.31 540.77 555.22 570.27 576.23 591.26 601.10 622.55 656.45 677.59 704.76 748.92 927.48 1022.12 1167. 37 1219.59 63 91 123 144 144 144 166 166 166 166 234 256 256 284 368 416 462 471 471 537 537 562 572 586 597 616 653 672 700 746 924 1014 1160 1213 6 6.56E-03 67.5 8 1. 03E-02 66. 2 9 3.57E-02 22.4 18 9.90E-03 55.4 2.04E+00 18 6.69E-02 10.4 18 1. 07E-01 7. 3 27 l.55E-02 33.4 8.49E-01 27 3.92E-02 17.4 27 3.34E-02 16.5 27 3.70E-02 17.7 7 9.18E-03 46.4 13 1.26E-02 37.2 2 .. 80E+00 13 9.96E-03 43.2 9 3.37E.:._03176.9 9 2.60E-02 23.0 8 9.61E-03 50.0 7 5.69E-03 70.5 17 1.18E-01 5.7 1.06E+OO 17 3.62E-02 13.6 25 1.lOE-02 33.2 1.16E+OO 25 5.0lE-03 81.6 11 4. llE-03110. 7 10 1.14E-02 29.6 10 4.70E-02 11.5 10 7.99E-03 55.9 11 7.28E-03 54.2 7 7.95E-03 39.1 13 3.29E-02 15.1 11 7.20E-02 8.8 7 5.27E-03 54.6 8 9.36E-03 31.4 16 1.21E-02 49.8 14 3.18E-02 15.4 14 5.70E-02 9.0 Peak Search Report (continued) Page : 2 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fft 35 0 661.41 72 22 1. 45 1323.81 1316 13 1.99E-02 18.1 36 0 665.98 21 15 1. 75 1332.95 1329 11 5.90E-03 42.5 37 0 727. 39 31 15 2.33 1455.68 1451 10 8.61E-03 29.5 38 0 802.80* 18 7 0.66 1606.41 1601 9 5.03E-03 38.1 39 0 806.83 19 6 0.95 1614.45 1611 8 5.28E-03 33.7 40 0 842.74 22 11 2.80 1686.23 1681 11 6. llE-03 36.1 41 0 904.18 14 6 0.91 1809.04 1805 8 3.95E-03 39.8 42 0 911.32* 112 18 1. 67 1823.31 1817 12 3.12E-02 12.2 43 0 957.80 11 7 0.95 1916.20 1913 8 3.12E-03 52.0 44 0 964.81 14 6 1. 01 1930.22 1927 7 3.82E-03 41. 3 45 0 969.02 69 6 1. 29 1938.64 1934 12 1.92E-02 14.0 46 0 1000.86* 10 17 0.67 2002.27 1992 14 2.66E-03100.5 47 0 1006.36 7 3 1.10 2013. 27 2010 6 2.06E-03 51.5 48 0 1021.14* 8 14 1. 42 2042.80 2039 9 2.19E-03 93.2 49 0 1045.66 9 5 0. 62 2091.82 2087 8 2.43E-03 58.3 50 0 1120.83* 29 23 1. 55 2242.07 2233 18 8.06E-03 43.1 51 0 1239.14 23 26 1. 40 2478.53 2473 14 6.47E-0.3 49.8 52 0 1279.37 5 12 4.20 2558.95 2549 12 1.39E-03145.6 53 0 1285.23 6 2 0.64* 2570.67 2567 7 1. 74E-03 53. 2 54 0 1337.51 7 8 1.34 2675.16 2668 11 1. 85E-03 92.1 55 *o 1396. 44 8 2 0.70 2792.94 '2788 9 2.19E-03 49.1 56 0 1408.26 12 0 1.74 2816.58 2812 10 3.33E-03 28.9 57 0 1461. 08* 321 19 2.412922.16 2914 15 8.93E-02 6.3 58 0 1764.58 41 0 l.07 3528.80 3523 13 1.14E-02 15.6 Flag: "*" = Peak area was modified by background subtraction Page 4205 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:52:07 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 14:55:00 G405235057 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:51:32 115. 83 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : SOLID GAMMAS. 0 01:00:00.00 1.50 keV Errors propagated:. No Efficiency type Linear Abundance limit 75.00 Interference Report Interfering Nuclide Page 4206 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real .time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 TH-229 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 85.43 86.94 87.57 88:03 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.59 10.00 . 0. 00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.244E+OO 1.482E+Ol l.482E+Ol 12.70 OK CD-109 88.03 3.70* 8.914E+OO 1. 772E+OO 2.806E+OO 60.17 'OK SN-126 64 .. 28 9.60 9.124E+OO 1.029E+OO l.029E+OO 44.76 OK 86.94 8.90 8.914E+OO 7.368E-01 7.368E-01 60.17 OK 87.57 37.00* 8.914E+OO 1. 772E-01 1. 772E-01 60.17 'OK CS-135 268.22 16.00* 5.038E+OO 3.243E-01 3.243E-01 66.49 OK BA-137M 661. 66 89.90* 2.417E+OO 2.089E-01 2.129E-01 36.21 OK CS-137 661. 66 85.10* 2.417E+OO 2.207E-01 2.250E-01 36. 21 OK TL-208 277.37 6.60 4.930E+OO 3.652E-01 3.652E-01 163.20 OK 583.19 85.00* 2.673E+OO 3.217E-01 3.217E-01 30.77 OK 860.56 12.50 1.959E+OO Line Not Found Absent PB-210 46.54 4.25* 9.666E+OO 6.380E-01 6.549E-01 132.41 OK PB-212 74.82 10.28 8.979E+OO 1.087E+OO 1.087E+OO 37.83 OK 77 .11 17.10 8. 967E+OO 1. 741E+OO 1.741E+OO . 14. 56 OK 238.63 43.60* 5.564E+OO 1.160E+OO 1.160E+OO 11. 42 OK 300.09 3.30 4.617E+OO 1.239E+OO l.239E+OO 111. 85 OK BI-214 609.32 45.49* 2. 581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120.29 14.92 1. 57 5E+OO 7.645E-01 7. 648E.:...01 86.25 OK 1764.49 15.30 1.032E+OO 1. 574E+OO l.574E+00 31.23 OK PB-214 74.82 5.80 8.977E+OO Line Not Found <<INT Reject 77 .11 9.70 8. 967E+OO 3.070E+OO 3. 071E+OO 14.56 OK 87.09 3.41 8.912E+OO Line Not Found <<INT Reject 242.00 7.25 5.497E+00 Line Not Found <<INT Reject 295.22 18.42 4. 681E+OO 1. 290E+OO 1.290E+OO 23.00 OK 351 *. 93 35.60* 4.043E+OO 1.173E+OO 1.174E+OO 17. 65. OK RN-222 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120.29 14.92 1.575E+OO 7.645E-01 7.648E-01 86.25 OK 1764.49 15.30 1.032E+OO 1. 574E+OO 1.574E+OO 31.23 OK RA-224 240.99 4.10* 5.508E+OO 1.542E+OO 1.542E+OO 75.39 OK RA-226 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120:29 14.92 1. 57 5E+OO 7.645E-01 7.648E-01 86.25 OK 1764.49 15.30 l.032E+OO 1. 574E+OO 1.574E+OO 31.23 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO l.645E+OO 1.645E+OO 30.14 OK 794.95 4.25 2.087E+OO Line Not Found Absent 835. 71 1. 61 2.005E+OO Line Not Found Absent 911. 20 25.80* 1.870E+OO l.457E+OO 1.457E+OO 24.31 OK 968. 97 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 OK RA-228 105.21 1.10 8.704E+OO Line Not Found Absent . 338.32 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 OK 794.95 4.25 2.087E+OO Line Not Found Absent 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.870E+OO 1.457E+OO 1.457E+OO 24.31 OK 968.97 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 OK TH-228 74.82 10.28 8.979E+OO 1.087E+OO 1.087E+OO 37.83 OK 77 .11 17.10 8. 967E+OO 1. 741E+OO 1. 741E+OO 14.56 .OK 238.63 43.60* 5.564E+OO 1.160E+OO 1.160E+OO 11. 42 OK 300.09 3.30 4.617E+OO l.239E+00 1.239E+OO 111. 85 OK TH-229 85.43 14.70 8.914E+00 4.461E-01 4.461E-01 60 .17 OK Page 4207 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 88.47 24.00 8.893E+OO 3.886E-01 3.886E-01 33.02 OK 193.51 4.41* 6. 511E+OO Line Not Found Absent 210.85 2.80 6 .116E+OO Line Not Found Absent TH-230 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120.29 14.92 l.575E+OO 7.645E-01 7.645E-01 86.25 OK 1764.49 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 OK TH-232 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 OK 835.71* 1. 61 2.005E+OO Line Not Found Absent. 911. 20 25.80* 1.870E+OO 1.457E+OO l.457E+OO 24.31 OK 968. 97 15.80 1. 779E+OO 1.530E+OO l.530E+OO 27.95 OK PA-233 300 .13 6.63 4.617E+00 6.166E-01 6.166E-01 111. 85 OK 311. 90 38.50* 4.484E+OO 9.945E-02 9.945E-02 108.41 OK 340.48 4.45 4 .154E+OO. Line Not Founq Absent TH-234 63.29 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44. 76 OK 92.59 4.23 8.869E+OO 2.447E+OO 2.447E+OO 35.39 OK U-234 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120.29 14.92 1.575E+OO 7.645E-01 7 .. 645E-01 86. 25 OK 1764.49 15.30 1.032E+OO l.574E+OO 1.574E+OO 31.23 OK U-235 89. 96 3.47 8.893E+OO 2.688E+OO 2. 68'8E+O 0 33.02 OK 93.35 5.60 8.869E+00 1.849E+OO l.849E+00 35.39 OK 143 .. 76 10. 96* 7.805E+OO 9.619E-02 9. 619E-0.2 353. 72 OK 163.33 5.08 7.279E+OO Line Not Found Absent 185.72 57.20 6.705E+OO 1.634E-01 1.634E-01 45.99 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 63.29 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44. 76 OK 92.59 4.23 8.869E+00 2.447E+OO 2.447E+OO 35.39 OK PU-239 129.30 0.01* 8.197E+OO 5.946E+02 5.946E+02 74.31 OK 375.05 0.00 3.844E+OO 2.064E+03 2.064E+03 109.17 OK 413.71 0.00 3.534E+00 Line Not Found Absent AM-243 43.53 5.90 9.491E+00 Line Not Found Absent 74.66 67.20* 8.979E+OO l.663E-01 1.663E-01 37.83 OK ANH-511 511. 00 100.00* 2.976E+OO 9.425E-02 9.425E-02 99.66 OK Flag: "*" = Keyline Page 4208 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:52:08.13 *******************************************************************************

GEL Laboratories LLC * *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l *
Acquisition date 3-0CT-2016 07:51:32 Sensitivity : 3.000 *
Detector ID GAM05 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.59 Half life ratio : ***** * *Sample date 2-DEC-2015 Analyst initials: MXRl *
Sample ID G405235057 Sample Quantity 1.1583E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
CALIBRATION INFORMATION *
*
Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.482E+Ol 1.845E+OO 6.930E-01 CD-109 2.806E+OO 1.654E+OO 1.283E+OO SN-126 1.772E-01 1.045E-01 8.lOOE-02 CS-135 3.243E-01 2 .113E-01 2. 661E-01 BA-137M 2.129E-01 7.556E-02 7.185E-02 CS-137 2.250E-01 7.982E-02 7.590E-02 TL-208 3.217E-01 9.701E-02 6.547E-02 PB-210 6.549E-01 8.498E-01 6.972E-01 PB-212 1.160E+OO l.298E-01 9. 511E-02 BI-214 1.112E+OO 1. 964E-01 1.275E-01 PB-214 1.174E+OO 2.030E-01 l.304E-01 RN-222 1.112E+OO 1. 964E-01 1. 27 5E-01 RA-224 1.542E+OO 1.139E+OO 1.020E+OO RA-226 1.112E+OO 1. 964E-01 1. 27 5E-01. AC-228 1.457E+OO 3.470E-01 2.959E-01 RA-228 1.457E+OO 3.470E-01 2.959E-01 TH-228 l.160E+OO l.298E-01 9. 511E-02 TH-229 -1.705E-01 4.424E-01 7.744E-01 TH-230 l .112E+OO 1. 964E-01 l.275E-01 TH-232 l.457E+OO 3.470E-01 2.959E-01 PA-233 9.945E-02 l.057E-01 9.168E-02 TH-234 2.669E+OO 1.171E+OO 8.652E-01 U-234 1.112E+OO 1. 964E-01 1. 27 5E-01 U-235 9.619E-02 3.334E-01 2.876E-01 U-238 2.669E+OO 1.171E+OO 8.652E-01 PU-239 5.946E+02 4.330E+02 4.347E+02 AW-243 1.663E-01 6.167E-02 5.094E-02 ANH-511 9.425E-02 9.205E-02 5.649E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -4.080E-01 1.560E+Ol 2.970E+Ol NOT IDENT. NA-22 l.150E-02 5.274E-02 9.900E-02 NOT IDENT. Page 4209 of 5809 NA-24 O.OOOE+OO 1.887E+41 O.OOOE+OO SHORT HLIF AL-26 -2.923E-03 4.248E-02 8.481E-02 NOT IDENT. SC-46 3.292E-01 4.356E-01 9.297E-01 FAIL ABUN V-48 O.OOOE+OO 2.219E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.096E+02 O.OOOE+OO SHORT HLIF MN-54 -l.825E-02 8.935E-02 l.588E-01 NOT IDENT. C0-56 -1. 8 67E-01 6.254E-01 1.032E+OO FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.356E-02 4.248E-02 *7.717E-02 NOT IDENT. C0-58 -5.131E-01 8.645E-01 1.246E+OO NOT IDENT. FE-59 -2.163E+OO 7.424E+OO 1. 420E+Ol NOT IDENT. C0-60 -6.648E-03 4.244E-02 7.341E-02 NOT IDENT. ZN-65 -3.291E-02 1. 991E-01 3.378E-01 NOT IDENT. GE-68 1.482E+OO 2.539E+OO 5.533E+OO NOT IDENT. AS-73 1. 372E+OO 2.258E+OO 4.518E+OO NOT IDENT. AS-74 O.OOOE+OO 8.017E+03 O.OOOE+OO SHORT HLIF SE-75 -1. 731E-02 2.457E-01 4.334E-01 NOT IDENT. BR-77 0.000E+OO 1.296E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9.019E+02 O.OOOE+OO SHORT HLIF RB-83 5.226E-01 6.834E-01 l.456E+OO NOT IDENT. KR-85 -2.533E+OO 9. 981E+.00 1.621E+Ol NOT IDENT. SR-85 -2.890E-01 1.121E+OO 1.820E+OO NOT IDENT. RB-86 O.OOOE+OO 3.750E+04 O.OOOE+OO SHORT HLIF Y-88 2.007E-01 2.412E-01 6.413E-01 NOT IDENT. Y-91 -4.706E+02 5.827E+02 9.852E+02 NOT IDENT. NB-94 2.358E-02 3.520E-02 7.225E-02 NOT IDENT. NB-95 -6.240E-01 l.155E+00 1. 971E+00 NOT IDENT. NB-95M -l.'684E-01 2. 511E+OO 4.468E+OO 'NOT IDENT. ZR-95 -4.362E-01 1. 798E+OO 3.251E+OO NOT IDENT. NB-97 O.OOOE+OO l.642E-f-41 0. OOOE+OO
SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.557E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 8.332E+40 O.OOOE+OO SHORT HLIF RH-101 -2.473E-02 2.979E-02 4.689E-02 NOT IDENT. RH-102 5.794E-03 7.128E-02 l.363E-01 FAIL ABUN RU-103 -2:458E+00 6.735E+OO 1.238E+Ol FAIL ABUN RH-106 -l.378E-01 5.142E-01 9.486E-01 NOT*IDENT. RU-106 -1.378E-01 5.142E-01 9.486E-01 NOT IDENT. AG-108M 1.293E-02 2.933E-02 5.944E-02 NOT IDENT. AG-llOM l.235E-02 l.124E-01 2.164E-01 NOT IDENT. SN-113 -2. 551E-02 2.405E-01 4.626E-01 NOT IDENT. CD-115 O.OOOE+OO 2.162E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.254E+05 O.OOOE+OO SHORT HLIF TE-123M 1.236E-02 l.313E-01 2.427E-01 NOT IDENT. SB-124 8.533E-01 2 .134E+OO 5.179E+OO NOT IDENT. SB-125 2.586E-03 9. 572E-02 1.885E-01 FAIL ABUN TE-125M 7.125E+Ol 2.584E+02 4.920E+02 NOT IDENT. I-126 O.OOOE+OO 1. 858E+o6 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.977E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.673E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. *470E+27 O.OOOE+OO SHORT HLIF BA-133 3 .118E-02 4.185E-02 8.175E-02 FAIL ABUN I-133 O.OOOE+OO 1.054E+41" O.OOOE+OO SHORT HLIF CS-134 8.lOOE-02 6.282E-02 l.359E-01 . FAIL ABUN I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.575E+05 O.OOOE+OO SHORT HLIF CE-139 2. 891E-02 1.040E-01 l.959E-01 NOT IDENT. BA-140 O.OOOE+OO 1.950E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.868E+05 O.OOOE+OO SHORT HLIF CE-141 -6.913E+00 2.633E+Ol 4. 381E+Ol NOT IDENT. CE-143 O.OOOE+OO l.002E+41 O.OOOE+OO SHORT HLIF CE-144 6.266E-03 2. 721E-01 4.785E-01 NOT IDENT. PM-144 4.109E-02 6. 091E-02 l.259E-01 NOT IDENT. PR-144 3.545E+OO 5.302E+OO 1.095E+Ol NOT IDENT. PM-146 5.332E-02 4.458E-02 9.779E-02 NOT IDENT. ND-147 O.OOOE+OO 4. 966E+07 O.OOOE+OO SHORT HLIF PM-147 -1. 960E+02 7.428E+02 1.255E+03 NOT IDENT. PM-149 O.OOOE+OO 5.800E+40 O.OOOE+OO SHORT HLIF EU-150 1.283E-02 3.042E-02 5.234E-02 FAIL ABUN EU-152 9.310E-02 9.925E-02 2.031E-01 FAIL ABUN GD-153 -5.012E-03 1.443E-01 2.694E-01 NOT IDENT. EU-154 2.812E-02 l.289E-01 2.420E-01 NOT IDENT. EU-155 3.631E-02 8.797E-02 1.702E-01 FAIL ABUN TB-160 -4*. 829E-01 2.026E+OO 3.683E+OO FAIL ABUN H0-166M -7.540E-03 6.419E-02 1.198E-01 FAIL ABUN TM-171 l.374E-01 4.592E+OO 8.916E+OO NOT IDENT. Page 4210 of 5809 HF-172 -2 .133E-02 2.188E-01 3.740E-01 FAIL ABUN LU-172 -4.430E-02 7.225E-02 l.299E-01 FAIL ABUN LU-176 -8.702E-03 2.509E-02 3.893E-02 FAIL ABUN HF-181 -2. 728E+OO 4.912E+00 8.827E+OO NOT IDENT. TA-182 -8.829E-01 l .139E+00 l.940E+OO FAIL ABUN RE-183 2.162E-01 l.OOOE+OO l.957E+OO NOT IDENT. RE-184 4.936E+Ol 3.847E+Ol 8.300E+Ol FAIL ABUN W-188 2.368E-01 l.422E+02 2.053E+02 FAIL ABUN IR-192 -2.643E-02 5.317E-01 9.364E-Ol FAIL ABUN HG-203 -2.678E-01 3.354E+00 4.749E+OO FAIL ABUN BI-207 9.534E-03 5.008E-02 l.035E-01 FAIL ABUN BI-211 O.OOOE+OO 5.591E-01 l.OOOE+OO FAIL ABUN PB-211 -l.130E-02 6.654E-01 l.291E+OO NOT IDENT. BI-212 l.310E+OO 7.566E-01 l.425E+OO FAIL ABUN RN-219 -l.032E-01 3.581E-01 6.770E-01 NOT IDENT. RA-223 -2.873E-01 6.702E-01 l.015E+OO FAIL ABUN AC-227 -l.220E-02 2.177E-01 3.902E-01 FAIL ABUN TH-227 -l.220E-02 2.177E-01 3.902E-01 FAIL ABUN PA-231 3;039E-02 5.201E-01 8. 531E-01 FAIL ABUN TH-231 -2.873E-01 6.702E-01 l.015E+OO FAIL ABUN PA-234 4.694E-02 3.417E-01 6.469E-01 FAIL ABUN PA-234M 4.103E+OO 8.086E+OO l.091E+Ol FAIL ABUN NP-237 9.945E-02 l.057E-01 l .119E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 3.358E-01 3.052E-01 3.731E-01' FAIL ABUN AM-241 2.664E-03 5.058E-02 9.129E-02 NOT IDENT. CM-243 -3.432E-02 7.706E-02 l.402E-01 FAIL ABUN BK-247 4.861E-02 7.488E-02 l.437E-01 FAIL ABUN CM-247 -l.586E-02 3.372E-02 6.222E-02 FAIL ABUN CF-249 3.662E-02 4.189E-02 8. 713E-02 NOT IDENT. CF-251 -9.189E-03 l.076E-01 l.952E-01 FAIL ABUN Page 4211of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:05.87 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 303 10.66* 1.244E+OO 1.482E+Ol 1.482E+Ol 12.70 CD-109 88.03 151 3.70* 8.914E+OO 2. 961E+OO 4.687E+OO 34.81 SN-126 64.28 139 9.60 9.124E+OO 1.029E+OO 1.029E+OO 44.76 86.94 151 8.90 8.914E+OO 1.231E+OO 1.231E+OO 34.81 87.57 151 37.00* 8.914E+OO 2. 961E-01 2. 961E-01 34.81 CS-135 268.22 40 16.00* 5.038E+OO 3.243E-01 3.243E-01 66.49 BA-137M 661. 66 70 89.90* 2.417E+OO 2.089E-01 2.129E-01 36.21 CS-137 661.66 70 85.10* 2.417E+OO 2. 2,07E-01 2.250E-01 36.21 TL-208 277.37 18 6.60 4.930E+00 3.652E-01 3.652E-01 163.20 583.19 113 85.00* 2.673E+OO 3.217E-01 3.217E-01 30.77 860.56 ------12.50 1. 959E+OO ------Line Not Found ------PB-210 46.54 40 4.25* 9.666E+OO 6.380E-01 6.549E-01 132.41 BI-211 72.87 38 1. 23 8.991E+OO 2.246E+OO 2.246E+OO 110.80 351. 06 261 12.92* 4.043E+OO 3.233E+OO 3.233E+OO 17.65 PB-212 74.82 258 10.28 8.979E+OO 1.815E+OO 1.815E+OO 20.70 77 .11 412 17 .10 8. 967E+OO 1. 741E+OO 1.741E+OO 14.56 238.63 434 43.60* 5.564E+OO 1.160E+OO 1.160E+OO 11. 42 300.09 29 3.30 4.617E+00 1.239E+OO 1.239E+OO 111. 85 BI-214 609.32 201 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 1120.29 28 14.92 1. 575E+OO 7.645E-01 7.648E-01. 86.25 1764.49 38 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 PB-214 74.82 258 5.80 8.979E+OO 3.217E+OO 3.218E+OO 20.70 77 .11 412 9.70 8. 967E+00 3.070E+OO 3. 071E+OO 14.56 87.09 151 3.41 8.914E+OO 3. 213E+OO 3.214E+00 34.81 242.00 133 7.25 5.508E+OO 2.162E+OO 2.162E+OO 27.13 295.22 172 18.42 4.681E+OO 1.290E+OO 1. 290E+OO 23.00 351.93 261 35.60* 4.043E+00 1.173E+OO 1.174E+OO 17.65 RN-222 609.32 201 45.49* 2.581E+OO l .112E+OO 1.112E+OO 18.02 1120.29 28 14.92 1.575E+OO 7.645E-01 7.648E-01 86.25 1764.49 38 15.30 1.032E+OO 1. 574E+OO 1.574E+OO 31. 23 RA-224 240.99 133 4.10* 5.508E+OO 3.822E+OO 3.822E+OO 27.13 RA-226 609.32 201 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 1120. 29 28 14.92 1.575E+OO 7.645E-01 7.648E-01 86.25 1764.49 38 15.30 1.032E+OO l.574E+00 1.574E+OO 31. 23 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 120 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 794.95 ------4.25 2.087E+OO ------Line Not Found ------835.71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 108 25.80* 1. 870E+OO 1.457E+OO 1.457E+OO 24.31 968.97 66 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 120 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 794.95 ------4.25 2.087E+OO ------Line Not Found ------835:71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 108 25.80* 1. 870E+OO 1.457E+OO 1.457E+OO 24.31 968. 97 66 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 TH-228 74:82 258 10.28 8. 97 9E+_oo 1.815E+OO 1.815E+OO 20.70 Page 4212 of 5809 Nuclide Line*Activity Report (continued) Page : 2 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 412 17.10 8. 967E+OO 1. 741E+OO 1. 741E+OO 14.56 238.63 434 43.60* 5.564E+OO 1.160E+OO l.160E+OO 11. 42 300.09 29 3.30 4.617E+OO l.239E+OO 1.239E+OO 111. 85 TH-229 85.43 151 14.70 8.914E+OO 7.453E-01 7.454E-01 34.81 88.47 128 24.00 8.893E+OO 3.886E-01 3.886E-01 33.02 193.51 ------4.41* 6. 511E+OO ------Line Not Found ------210.85 ------2.80 6 .116E+OO ------Line Not Found ------TH-230 609.32 201 45.49* 2.581E+OO 1.112E+OO l .112E+OO 18.02 1120.29 28 14.92 1.575E+OO 7.645E-01 7.645E-01 86.25 1764.49 38 15.30 1.032E+OO 1. 574E+OO 1. 574E+OO 31.23 TH-232 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 120 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 108 25.80* 1.870E+OO l.457E+OO 1.457E+OO 24.31 968.97 66 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 PA-233 300.13 29 6.63 4.617E+OO 6.166E-01 6.166E-01 111. 85 311. 90 26 38.50* 4.484E+OO 9.945E-02 9.945E-02 108.41 340.48 ------4.45 4.154E+OO ------Line Not Found ------TH-234 63.29 139 3.70* 9.124E+OO 2.669E+OO 2. 669E+O'O 44.76 92.59 142 4.23 8.869E+OO 2.447E+OO 2.447E+OO 35.39 U-234 609.32 201 45.49* 2. 581E+OO 1, 112E+OO l .112E+OO 18. 02 1120.29 28 14.92 1. 57 5E+00 7.645E-01 7.645E-01 86.25 1764.49 38 15.30 1.032E+OO l.574E+00 1.574E+OO 31.23 U-235 89. 96 128 3.47 8.893E+OO 2.688E+00 2.688E+OO 33.02 93.35 142 5.60 8.869E+OO l.849E+00 1.849E+OO 35.39 143.76 13 10.96* 7.805E+OO 9.619E-02 9.619E-02 353.72 163.33 ------5.08 7.279E+OO ------Line Not Found ------185. 72 97 57.20 6.705E+OO 1.634E-01 l.634E-01 45.99 205.31 ------5.01 6.238E+OO ------Line Not Found ------U-238 63.29 139 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44.76 92.59 142 4.23 8.869E+OO 2.447E+OO 2.447E+OO 35.39 PU-239 129.30 47 0.01* 8.197E+OO 5.946E+02 5.946E+02 74.31 375.05 19 0.00 3.844E+OO 2.064E+03 2.064E+03 109.17 413.71 ------0.00 3.534E+OO ------Line Not Found ------AM-243 43.53 ------5.90 9.491E+OO ------Line Not Found ------74.66 258 67.20* 8.979E+OO 2.776E-01 2.777E-01 20.70 ANH-511 511. 00 43 100.00* 2.976E+OO 9.425E-02 9.425E-02 . 99. 66 Flag: "*" Key line Page 4213of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Total number of lines in spectrum 58 Number of unidentified lines 11 Number of lines tentatively identified by NID 47 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 PA-233 TH-234 U-234 U-235 U-238
PU-239 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1.41E+10Y 1. 41E+10Y 1. 41E+10Y 7340.00Y 7.54E+04Y 1. 41E+10Y 2.14E+06Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 24110. OOY 7370.00Y 1.00E+09Y Decay 1. 00 1. 58 1. 00 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1."00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.482E+Ol 2. 961E+OO 2. 961E-01 3.243E-01 2.089E-01 2.207E-01 3.217E-01 6.380E-01 3.233E+OO 1.160E+OO 1.112E+OO 1.173E+OO 1.112E+OO 3.822E+OO 1.112E+OO '1. 457E+OO 1.457E+OO 1.160E+OO 3.886E-01 1.112E+OO 1.457E+00 9.945E-02 2.669E+OO 1.112E+OO 9.619E-02 2.669E+00 5.946E+02 2.776E-01 9.425E-02 6.412E+02 6.412E+02 Decay Corr pCi/GRAM l.482E+Ol 4.687E+OO 2.961E-01 3.243E-01 2.129E-01 2.250E-01 3.217E-01 6.549E-01 3.233E+OO 1.160E+OO 1.112E+OO 1.174E+00 1.112E+OO 3.822E+OO 1.112E+OO 1.457E+OO 1.457E+OO 1.160E+OO 3.886E-01 1.112E+OO l.457E+OO 9.945E-02 2.669E+OO 1.112E+OO 9.619E-02 2.669E+00 5.946E+02 2.777E-01 9.425E-02 6.429E+02 6.429E+02 81. 03% Decay Corr 2-Sigma Error 0.188E+Ol 1.632E+OO l.031E-01 2.156E-01 0. 771E-01 0.814E-01 0.990E-01 8.672E-01 0. 571E+00 0.132E+OO 0.200E+OO 0.207E+OO 0.200E+OO 1.037E+00 0.200E+OO 0.354E+OO 0.354E+OO 0.132E+00 1. 283E-01 0.200E+OO 0.354E+OO 10.78E-02 l.194E+00 0.200.E+OO 34.02E-02 1.194E+OO 4.418E+02 0.575E-01 9.393E-02 "M" Manually accepted 2-Sigma %Error 12.70 34.81 34.81 66.49 36.21 36.21 30.77 132.41 17.65 11. 42 18.02 17.65 18.02 27.13 18.02 24.31 24.31 11. 42 33.02 18.02 24.31 108.41 44. 76 18.02 353. 72 44. 76 74.31 20.70 99.66 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4214 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235057 Acquisition date : 3-0CT-2016 07:51:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 31. 49 26 104 0.53 64.83 63 6 6.56E-03 **** 1.49E+OO 5 83.62 60 126 0. 96 169.01 166 27 1.55E-02 66.8 8.93E+OO T 0 117. 65 35 77 1. 66 237.01 234 7 9.18E-03 92.7 8.46E+OO T 3 130.85 38 61 1.17 .263.40 256 13 9. 96E-03 86.3 8.15E+OO T 0 209.04 36 91 1. 04 419.68 416 8 9.61E-03 99.9 6.15E+OO 0 231. 76 21 70 1. 82 465.07 462 7 5.69E-03 **** 5.69E+OO 0 284.39 15 65 4.54 570.27 562 11 4. llE-03 **** 4.82E+OO T 0 287.37 42 31 2.31 576.23 572 10 l.14E-02 59.2 4.78E+OO T 0 327.51 29 36 1. 59 656.45 653 7 7.95E-03 78.2 4.29E+OO T 0 463 .11 33 26 1.17 927.48 924 8 9.36E-03 62. 8 3.22E+OO T 0 665.98 21 14 1. 75 1332. 95 1329 11 5.90E-03 85.0 2.40E+OO T 0 727.39 30 15 2.33 1455.68 1451 10 8. 61E-03 59.0 2.24E+OO T 0 802.80 18 7 0.66 1606.41 1601 9 5.03E-03 76.2 2.07E+OO T 0 806.83 18 6 0.95 1614.45 1611 8 5.28E-03 67.4 2.06E+OO 0 842.74 21 11 2.80 1686.23 1681 11 6.llE-03 72.3 l.99E+00 0 904.18 14 6 0.91 1809.04 1805 8 3.95E-03 79.5 1. 88E+00 T 0 957.80 11 7 0.95 1916.20 1913 8 3.12E-03 **** 1. 80E+OO 0 964.81 13 6 1. 01 1930.22 1927 7 3.82E-03 82.6 1.78E+OO T 0 1000.86 9 17 0.67 2002.27 1992 14 2.66E-03 **** 1.73E+OO T 0 1006.36 7 2 1.10 2013.27 2010 6 2.06E-03 **** 1.72E+OO 0 1021.14 8 14 1. 42 2042.80 2039 9 2.19E-03 **** 1.70E+OO T 0 8 5 0.62 2091. 82 2087 8. 2.43E-03 **** 1. 67E+OO T 0 1239.14 22 24 1. 40 2478.53 2473 14 6.47E-03 99.6 1. 44E+OO T 0 1279.37 5 11 4.20 2558.95 2549 12 1.39E-03 **** 1. 40E+OO 0 1285.23 6 2 0.64 2570.67 2567 7 1. 7 4E-03 **** 1.40E+OO 0 1337. 51 6 8 1. 34 2675.16 2668 11 l.85E-03 **** 1.35E+OO 0 1396.44 7 2 0.70 2792.94 2788 9 2.19E-03 98.3 1.30E+OO 0 1408.26 11 0 1. 74 2816.58 2812 10 3.33E-03 57.7 l.29E+OO T Flags: "T" = Tentatively associated Page 4215of5809
VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:52:20 . .43 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l *
Acquisition date 3-0CT-2016 07:51:32 Sensitivity : 3.000 *
Detector ID GAM05 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit :* 75.000 '*
real time: 0 01:00:00.59 Half life* ratio : ***** *
Sample date 2-DEC-2015 14:55:00 Nuclide Library : SOLID *
Sample ID G405235057 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.1583E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20 * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 PA-233 TH-234 U-234 U-235 U-238 PU-239 AM-243 ANH-511 Le (pCi/GRAM 2.807E-01 5.988E-01 3.779E-02 1.221E-01 3.180E-02 3.360E-02 2.887E-02 3.262E-01 4.390E-02 5. 627E-02. 5.906E-02 5 .. 627E-02 4. 711E-01 5.627E-02 1.298E-01 1.298E-01 4.390E-02 3.563E-01 5.625E-02 1.298E-01 4.070E-02 4.061E-01 5.625E-02 l.334E-01 4. 061E-01 2. 001E+02 2.399E-02 2.529E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4216of5809 Le (pCi/GRAM 1. 341E+Ol 4.175E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95* NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 'PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 4217 of 5809 3.373E-02 4.073E-01 O.OOOE+OO O.OOOE+OO 7.079E-02 4.475E-01 O.OOOE+OO 3.588E-02 5.376E-01 5.971E+OO 2.950E-02 l.429E-01 2.402E+OO 2.130E+OO O.OOOE+OO 1.995E-01 O.OOOE+OO O.OOOE+OO 6.498E-01 7. 381E+OO '8. 288E-01 O.OOOE+OO 2.560E-01 4.076E+02 3. 231E-02 8.736E--,01 2.060E+OO 1.422E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.155E-02 6.084E-02 5.488E+OO 4.127E-01 4.127E-01 2.685E-02 9. 351E-02 2.082E-01 O.OOOE+OO O.OOOE+OO 1.129E-01 2.016E+OO 8.363E-02 2.307E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.712E-02 O.OOOE+OO 6.144E-02 O.OOOE+OO O.OOOE+OO 9.077E-02 O.OOOE+OO O.OOOE+OO 2.030E+Ol O.OOOE+OO 2.183E-01 5.613E-02 4.882E+OO 4.430E-02 O.OOOE+OO 5.810E+02 O.OOOE+OO 2. 396E-02 9.314E-02 l.263E-Ol 1.020E-01 7. 963E-02 1.558E+OO 5.281E-02 4.187E+OO 1.740E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT .IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT'. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF . FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-234 PA-234M NP-237 NP-238 NP-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4218 of 5809 5.316E-02 1.738E-02 3.893E+OO 8.289E-01 9.206E-01 3.664E+Ol 9.300E+Ol 4.255E-01 2.165E+OO 4.450E-02 4.835E-01 5.806E-01 6.538E-01 3.016E-01 4.564E-01 l.773E-01 l.773E-01 3.907E-01 4.564E-01 2.832E-01 4.853E+OO 5.080E-02 O.OOOE+OO 1.733E-01 4.294E-02 6.512E-02 6.610E-02 2. 772E-02 3.998E-02 9.015E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL .ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT, FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:52:26.17 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l *
Acquisition date 3-0CT-2016 07:51:32 Sensitivity : 3.000 *
Detector ID GAM05 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
Sample date 2-DEC-2015 14:55:00 Nuclide Library : SOLID *
Sample ID G405235057 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.1583E+02 GRAM *
Quantity Err(%) : 1. 7266E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date . : 4-SEP-2016 08: 00: 28 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.482E+Ol 2.00lE+OO CD-109 2.806E+OO 1.687E+OO SN-126 1.772E-01 1.061E-01 CS-135 3.243E-01 2.124E-01 BA-137M 2.129E-01 7. 611E-02 CS-137 2.250E-01 8.040E-02 TL-208 3.217E-01 9.798E-02 PB-210 6.549E-01 .8. 519E-01 PB-212 L 160E+00 l.437E-01 BI-214 1.112E+OO 2. 021E-01 PB-214 1.174E+OO 2.088E-01 RN-222 1.112E+OO 2.021E-01 RA-224 1.542E+OO l.152E+OO RA-226 1.112E+OO 2. 021E-01 AC-228 1.457E+OO 3.549E-Oi RA-228 1.457E+OO 3.549E-01 TH-228 1.160E+OO 1.437E-01 TH-229 -1. 705E-01 4.425E-01 TH-230 1.112E+OO 2. 021E-01 TH-232 1.457E+OO 3.549E-01 PA-233 9.945E-02 l.058E-01 TH-234 2.669E+OO 1. 311E+OO U-234 1.112E+OO 2.021E-01 U-235 9.619E-02 3.335E-01 U-238 '2.669E+OO 1. 311E+OO PU-239 5.946E+02 4.338E+02 AM-243 l.663E-01 6.408E-02 ANH-511 9.425E-02 9.213E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 4219of5809 Key-Line Activity (pCi/GRAM -4.080E-01 1.150E-02 K.L Act error (1.96-sigma) 1.560E+Ol 5.274E-02 TPU (1.96-sigma) 2.00lE+OO 1.687E+OO 1.061E-01 2.124E-01 7. 611E-02 8.040E-02 9.798E-02 8.519E-01 1.437E-01 2.021E-01 2.088E-01 2.021E-01 1.152E+OO 2. 021E-01 3.549E-01 3.549E-01 l.437E-01 4.425E-01 2. 021E-01 3.549E-01 1.058E-01 1.311E+OO 2.021E-01 3.335E-01 1. 311E+OO 4.338E+02 6.408E-02 9.213E-02 TPU ( 1 . 96-sigma ) 1.560E+Ol NOT IDENT. 5.300E-02 NOT IDENT.

NA-24 1.000E+41 1.939E+41 O.OOOE+OO SHORT HLIF AL-26 -2.923E-03 4.248E-02 4.250E-02 NOT IDENT. SC-46 3.292E-01 4.358E-01 4.604E-01 FAIL ABUN V-48 -7.745E+03 2.219E+04 2.246E+04 SHORT HLIF CR-51 -4.315E+02 6.099E+02 6. 401E+02 SHORT HLIF MN-54 -l.825E-02 8.935E-02 8.973E-02 NOT IDENT. C0-56 -l.867E-01 6.254E-01 6. 311E-01 FAIL ABUN MN-56 -1.000E+41 3.275E+41 O.OOOE+OO SHORT HLIF C0-57 -1. 356E-02 4.248E-02 4.292E-02 NOT IDENT. C0-58 -5.131E-01 8.648E-01 8.952E-01 NOT IDENT. FE-59 -2.163E+OO 7.425E+OO 7.489E+OO NOT IDENT. C0-60 -6.648E-03 4.244E-02 4.254E-02 NOT IDENT. ZN-65 -3.291E-02 1.991E-01 1. 996E-01 NOT IDENT. GE-68 1.482E+OO 2.539E+OO 2.626E+OO NOT IDENT. AS-73 1.372E+OO 2.275E+OO 2.358E+OO NOT IDENT. AS-74 l.536E+03 8. 018E+03 8.048E+03 SHORT HLIF SE-75 -1. 731E-02 2.457E-01 2.458E-01 NOT IDENT. BR-77 1.158E+39 l.022E+40 O.OOOE+OO SHORT HLIF SR-82 5.007E+02 9.022E+02 9.300E+02 SHORT HLIF RB-83 5.226E-01 6.872E-01 7.264E-01 NOT IDENT. -2.533E+00 9.981E+OO 1.005E+Ol NOT IDENT. SR-85 -2.890E-01 1.121E+OO 1.129E+OO NOT IDENT. RB-86 1.513E+04 3.751E+04 3.812E+04 SHORT HLIF Y-88 2.007E-01 2.416E-01 2.580E-01 NOT IDENT. Y-91 -4.706E+02 5.830E+02 6.204E+02 NOT IDENT. NB-94 2.358E-02 3.522E-02 3.679E-02 NOT IDENT. NB-95 -6.240E-01 1.156E+OO l.189E+OO NOT IDENT. NB-95M -1.684E-01 2. 511E+OO 2.512E+OO NOT IDENT. ZR-95 -4.362E-01 1.798E+OO 1.809E+OO NOT IDENT. NB-97 1.000E+41 1. 642E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 2.092E+41 O.OOOE+OO SHORT HLIF M0-99 -4.577E+31 9.557E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 8.390E+40 O.OOOE+OO SHORT HLIF RH-101 -2.473E-02 3.013E-02 3.212E-02 NOT IDENT. RH-102 5.794E-03 7.128E-02 7.133E-02 FAIL ABUN RU-103 -2.458E+OO 6.736E+OO 6.826E+OO FAIL ABUN RH-106 -l.378E-01 5.143E-01 5.180E-01 NOT IDENT. RU-106 -l.378E-01 5.143E-01 5.180E-01 NOT IDENT. AG-108M 1.293E-02 2.933E-02 2.991E-02 NOT IDENT. AG-llOM 1.235E-02 1.124E-01 1.125E-01 NOT IDENT. SN-113 -2.551E-02 2.405E-01 2.407E-01 NOT IDENT. CD-115 l.871E+40 2.190E+40 O.OOOE+OO SHORT HLIF SN-117M -5.451E+04 l.256E+05 l.280E+05 SHORT HLIF TE-123M 1.236E-02 1. 313E-01 l.315E-01 NOT IDENT. SB-124 8.533E-01 2.134E+OO 2.169E+OO NOT IDENT. SB-125 2.586E-03 9. 572E-02 9.573E-02 FAIL ABUN TE-125M 7.125E+Ol 2.584E+02 2.604E+02 NOT IDENT. I-126 2.231E+06 1.884E+06 2.i35E+06 SHORT HLIF SB-126 -1. 558E+06 1.891E+06 2.017E+06 SHORT HLIF SB-127 -3.139E+22 9 .110E+22 O.OOOE+OO SHORT HLIF I-131 2.122E+08 9.673E+09 9.674E+09 SHORT HLIF I-132 l.OOOE+41 l.939E+42 O.OOOE+OO SHORT HLIF TE-132 5.883E+26 1.490E+27 O.OOOE+OO SHORT HLIF BA-133 3 .118E-02 4.187E-02 4;417E-02 FAIL ABUN I-133 1.000E+41 2.124E+41 O.OOOE+OO SHORT"HLIF CS-134 8.lOOE-02 6.291E-02 7.274E-02 FAIL ABUN I-135 l.000E+41 l .132E+42 O.OOOE+OO SH.ORT HLIF CS-136 -2.198E+05 4.581E+05 4.687E+05 SHORT HLIF CE-139 2.891E-02 1.042E-01 l.050E-01 NOT IDENT. BA-140 -7.912E+05 1.950E+06 1.982E+06 SHORT HLIF LA-140 -3.570E+04 6.868E+05 6.870E+05 SHORT HLIF CE-141 -6.913E+OO 2.634E+Ol 2.652E+Ol NOT IDENT. CE-143 l.000E+41 l.007E+41 0.000E+OO SHORT HLIF CE-144 6.266E-03 2.721E-01 2.721E-01 NOT IDENT. PM-144 4.109E-02 6.096E-02 6. 371E-02 NOT IDENT. PR-144 3*. 545E+00 5.304E+OO 5.539E+OO NOT IDENT. PM-146 5.332E-02 4.475E-02 5.079E-02 NOT IDENT. ND-147 -3.013E+07 4. 969E+07 5.151E+07 SHORT HLIF PM-147 -1.960E+02 7.429E+02 7.481E+02 NOT IDENT. PM-149 1.000E+41 6.211E+40 O.OOOE+OO SHORT HLIF EU-150 1.283E-02 3.042E-02 3.097E-02 FAIL ABUN EU-152 9.310E-02 9.938E-02 1. 07 9E-01 FAIL ABUN GD-153 -5.012E-03 1.443E-01 1.443E-01 NOT IDENT. EU-154 2.812E-02 1. 28'9E-01 l.295E-01 NOT IDENT. EU-155 3.631E-02 8.801E-02 8.952E-02 FAIL ABUN TB-160 -4.829E-01 2 .. 026E+00 2.038E+OO FAIL ABUN H0-166M -7.540E-03 6.419E-02 6.428E-02 FAIL ABUN TM-171 1. 374E-01 4.592E+OO 4.593E+OO NOT IDENT. Page 4220 of 5809 HF-172 -2 .133E-02 2.188E-01 2.190E-01 FAIL ABUN LU-172 -4.430E-02 7.239E-02 7.510E-02 FAIL ABUN LU-176 -8.702E-03 2.509E-02 2.540E-02 FAIL ABUN HF-181 -2. 728E+OO 4.914E+OO 5.065E+OO NOT IDENT. TA-182 -8.829E-01 l.140E+OO l.207E+OO FAIL ABUN . RE-183 2.162E-01 l.OOlE+OO l.006E+OO NOT IDENT. RE-184 4.936E+Ol 4.031E+Ol 4.604E+Ol FAIL ABUN W-188 2.368E-01 l.422E+02 l.422E+02 FAIL ABUN IR-192 -2.643E-02 5.317E-01 5.319E-01 FAIL ABUN HG-203 -2.678E-01 3.354E+OO 3.356E+OO FAIL ABUN BI-207 9.534E-03 5.00BE-02 5.027E-02 FAIL ABUN BI-211 3.233E+OO 5.776E-01 l.568E+OO FAIL ABUN PB-211 -l.130E-02 6.654E-01 6.654E-01 NOT IDENT. BI-212 l.310E+OO 7.595E-01 9.619E-01 FAIL ABUN RN-219 -l.032E-01 3.583E-01 3.613E-01 NOT IDENT. RA-223 -2.873E-01 6.705E-01 6.829E-01 FAIL ABUN AC-227 -1. 220E-02 2.177E-01 2.177E-01 FAIL ABUN TH-227 -1. 220E-02 2.177E-01 2.177E-01 FAIL ABUN PA-231 3.039E-02 5.201E-01 5.203E-01 FAIL ABUN TH-231 -2.873E-01 6.705E-01 6.829E-01 FAIL ABUN PA-234 4.694E-02 3.459E-01 3.466E-01 FAIL ABUN PA-234M 4.103E+OO 8.088E+00 8.296E+OO FAIL ABUN NP-237 9.945E-02 l.058E-01 l.149E-01 FAIL ABUN NP-238 -1. 000E+41 2.483E+41 O.OOOE+OO SHORT HLIF NP-239 3.358E-01 3.064E-01 3.418E-01 FAIL ABUN AM-241 2.664E-03 5.058E-02 5.060E-02 NOT IDENT. CM-243 -3.432E-02 7.712E-02 7.866E-02 FAIL ABUN BK-247 4.861E-02 7. 551E-02 7.863E-02 FAIL ABUN CM-247 -l.586E-02 3. 382E-02 3.457E-02 FAIL ABtJN CF-249 3.662E-02 4.199E-02 4.512E-02 NOT IDENT. CF-251 -9.189E-03 1. 07 6E-01 l.076E-01 FAIL ABUN Page 4221 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *-GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 63.4503 87.09 64.9837 136.47 47.6878 45.60 70.4172 87.57 65. 0611 140.51 0.0000 46.54 70.6720 88.03 65.1345 143.76 55.1985 49. 72 0.0000 88.34 65.1836 144.24 55.2438 51. 35 79.8433 88.47 65.2045 145.44 59.3106 51. 87 76.8232 89. 96 65.4405 152.43 59.0054 52.39 69.0301 1093-. 63 65.5477 153.25 0.0000 52.97 68.3754 91.11 0.0000 323.87 52.1555 53.44 66.8949 92.59 65.8526 156.02 0.0000 54.07 59.8580 93.35 65.9706 158.56 0.0000 57.36 0.0000 94.56 60.7934 159.00 57.6123 57.53 72.6732 94.65 60.8063 162.33 46.7384 57.98 78.4414 94.67 60.8089 162.66 0.0000 59.27 77.9597 94.87 60.8369 163.33 45.7938 59.32 77.9725 97.43 71. 0959 165.86 48.0169 59.54 82.3627 98.43 80.2770 176.31 52.9276 6'0. 96 83.8263 98.44 80.2787 176. 60 0.0000 61.17 77.6180 99.53 56 .. 0621 177.52 50.9417 62.93 78.0475 100 .11 66.9998 181. 07 0.0000 63.29 78.1346 102.03 59.1021 181.52 43.2210 63.58 78.2046 103.18 61.0745 184.41 49.3494 64.28 86.8973 103.37 66.5712 143.76 49.4412 66.73 89.7589 105.21 57.6816 193.51 52.1059 67.24 99.0508 105.31 61.3572 197.03 49.1501 125.81 91.6787 106.12 67.8857 198.01 72.7522 67.75 86.6955 106.47 79 .. 8712 201.83 69.8976 69.67 86.0665 109.28 69.2648 203.43 56.0363 70.83 77.3814 111. 00 58.3915 205.31 56.1752 72.81 87.1200 111.76 0.0000 210.85 53.6776 72. 87 87.1349 114. 06 49.7428 215.65 38.3149 74.66 87.5687 116. 30 0.0000 222.11 39.7271 74.82 87.6072 116.74 62.5153 227.09 48.8514 74.97 87.6434 119. 76 44.0227 227.38 51. 08 95 77 .11 88.1549 121.12 58.0124 228.16 0.0000 78.74 88.5400 lZl. 22 58.0236 228.18 38.5398 79.69 83.8790 121. 78 57.7706 116.74 38.5398 80.12 86.2740 122.06 65.3829 235.69 48.2326 80.19 0.0000 122.92 51. 2541 235. 96 48.2484 80.57 82.9204 123.07 51.2689 238.63 48.3986 81. 00 67.4484 265.00 64.6361 238.98 0.0000 81. 07 67.4609 125.81 62.3536 240.99 48.5312 81. 75 94.7266 127.23 61.2439 242.00 45.1984 83.79 64.4496 127.91 45.0335 244:70 40.8043 84.00 64.4841 129.30 45.1497 252.40 0.0000 85.43 64. 7167 131. 2 0 45.3082 252.80 41.1784 86.55 64.8974 133.02 41. 2676 254.15 0.0000 86.79 64.9357 133.52 36.1416 256.23 34.4458 86.94 64. 9600 136.00 48.6206 260.90 0.0000 Page 4222 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 46.3501 355.39 0.0000 584.27 18.7271 264.80 46.3574 356.01 21.4866 595.83 0.0000 265.00 32.4570 364.49 0.0000 427.87 28.8466 268.22 41. 8744 366.42 0.0000 602.52 0.0000 269.46 35.7176 372. 51 30.7537. 604.72 26.9176 270.03 35.7391 375.05 34.6704 607.14 17.9692 271.23 35.7840 377.52 36.0262 609.32 18.9900 273.65 0.0000 356.01 38.7964 610.33 19.0008 276.40 35.9777 388.16 27.6829 614.28 13.5297 277.37 36.0142 388.63 0.0000 618.01 15.0629 277.60 36.0227 391.69 28.6279 620. 36 20.1099 *278.00 36.0376 264.66 23. 5871 621. 93 18 .1143 279.20 37.6514 401.81 26.2311 630.19 0.0000 279.54 37.6641 402.40 28.8669 631.29 20.2271 279.70 37.6699 404.85 27.1685 633.25 21. 2606 280.46 37.6997 410.95 45.7846 634.78 0.0000 283.69 30.7322 413. 71 30.8806 635.95 17.2359 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 4.7363 423.72 0.0000 645.85 23.4399 285.90 0.0000 427.09 16.0400 657.76 10.7670 287.50 26.8952 427.87 20.5073 657.90 0.0000 290.67 30.9488 .433.94 23.2848 661.66 20.0356 293.27 0.0000 439.40 17.9818 664.57 0.0000 351. 31. 8856 453.88 15.4415 666.33 0.0000 295.96 21.5387 463.37 23. 7720 666.50 0.0000 879.38 23.9929 468.07 30.2688 667.71 0.0000 299.98 35.2380 473.00 0.0000 677.62 14.5013 300.09 35.2415 475.06 28.5687 685.70 0.0000 300.13 35.2433 476.78 24. 9115 695.00 0.0000 301.36 38.4932 477.60 29.5404 696.49 14.6369 302.85 40.1550 482.18 25.9270 696. 51 14.6375 256.23 38.6094 487.02 0.0000 697.00 0.0000 304.85 0.0000 . 492.35 0.0000 697.30 20.9188 306.78 29.0208 497.08 25.2460 697.49 23.0125 308.46 29.0669 505.52 22.5630 702.65 15:7300 311. 90 21.0615 5'07. 63 0.0000 706.68 22.0647 316.51 34.1694 511. 00 24.5284 711. 68 17.9048 319.41 0.0000 514.00 39.6980 720.70 0.0000 320.08 0.0000 514.00 39.6980 721. 93 0.0000 321.04 20.8329 520.40 14.2346 722.78 15.8820 323.87 34.4027 520.69 0.0000 722. 91 12.7065 325.23 18.0428 522.65 0.0000 723.31 14.2976 328.76 . 0. 0000 527.90 0.0000 724 .19 9.5358 333.37 38.0039 528.26 13.3506 727.33 14.8551 333.97 31.4115 529.59 13.3614 733.00 14.8949 334.37 28.1147 529.87 0.0000 735.93 17.0462 338.28 23.6491 531.02 0.0000 333.97 13. 8596 338.32 23.6497 537.26 0.0000 739.50 0.0000 311. 90 24.9420 546.56 0.0000 747.24 13.9225 340.48 24.9420 552.55 19.3538 748.06 18.2133 340.55 0.0000 563.25 25.3187 752.31 20.3962 344.28 26.0260 569.33 17.5906 753.82 0.0000 345.93 36. 7562 946.00 17.5928 756.73 19.3616 351.06 31.0456 569.70 15.6393 756.80 19.3623 351. 93 31. 0689 583.19 18.7163 884.68 18.3461 Page 4223 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.0820 1274.44 8.5321 1620.50 2.1292 766.42 25.9287 1001.03 12.4641 1621.92 6.3896 766.84 20.5308 1002.74 14.2534 1678.03 0.0000 772. 60 0.0000 1004.73 3.5658 1690.97 2.1642 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.3999 778.90 10.8643 1028.54 0.0000 1063.66 4.4053 783.70 0.0000 1037.84 9.0192 1771. 35 3.3049 785.37 25.0599 1038.76 0.0000 1791.20 0.0000 792.07 21.8555 631.29 10.1322 1808.65 5.5527 794.95 18.6007 1048.07 0.0000 1810.72 0.0000 795.86 13.1353 1049.04 17.3848 1836.06 1.1170 810.06 16.5204 1050.41 18.6353 810.29 19.8259 1063.66 10.9197 344.28 19.8274 1077.00 0.0000 810.76 21.4828 1077.34 9.1425 815.77 0.0000 1085.87 17.4205 1048.07 0.0000 1093.63 11.9503 832.01 15.5632 1099.45 11. 9733 834.85 25.5989 1112. 07 11. 0984 835. 71 24.4949 1112. 84 12.3340 836.80 0.0000 1115. 54 11. 8516 84.6.75 0.0000 1120. 29 12.0550 846.77 13.4224 1120.55 12.0566 856.80 0.0000 1221. 41 12.0590 860.56 19.1236 1129. 67 17.6733 871.09 12.4269 1131.51 0.0000 873.19 6.7842 1147.95 0.0000 875.33 0.0000 1173.23 16.9761 879.38 12.4685 1177.95 9.4452 880.51 15.8765 1189.05 12.3216 883.24 13. 6230 1204.77 15.2383 884.68 12.4950 1221. 41 20.1015 889.28. 9.1042 1231. 02 18.2404 894.76 9.1237 1235.36 0.0000 898.04 15.9875 1238.28 12.5073 900.72 12.0031 1260.41 0.0000 903.28 17.1643 1271.87 3.1094 911.20 17.2180 1274.44 7.7793 912.08 17.2235 1274.54 "7.7793 923.98 0.0000 1291.59 8.7951 926.50 17.3199 1298.22 0.0000 92 9. 11 15.0254 1312 .11 0.0000 937.49 18.5521 1332.49 6.3273 944 .13 0.0000 1362.66 0.0000 946.00 15.1222 1365.19 5.9861 949.00 13.9746 1368.63 0:0000 667.71 0.0000 1384.29 2.0057 962. 31 10.5333 1408.01 6.0557 964.08 12.6483 1457.56 0.0000 966 .17 3.5161 1460.82 6.1403 911.20 8.4475 1489.16 10.3088 968. 97 8.4475 1505.03 6.2102 983.53 0.0000 1584.12 9.4982 984.45 0.0000 1596.21 0.0000 Page 4224 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:57.76 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 2-DEC-2015 15:00:00. Acquisition date : 3-0CT-2016 07:51:57. Sample ID G405235058 Sample quantity : l.40622E+02 GRAM Detector n-ame : GAMO 6 Detector geometry: CAN Elapsed live time: .0 01:00:00.00 Elapsed real time: 0 01:00:00.66 0.0% Energy tolerance : 1.50000 kev* Analyst* Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 2.9 30 31 32 33 34 0 4 4 4 0 3 3 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 63.38* 74.89* 77.17 79.22 87.15 89.98 92.87* 102.61 129.51 153.61 177.33 185.74* 209.36 238.57*

241.97* 289.24 295.20* 314.64 338.31 351.91 358.65 401.80 408.85 463.77 546.34 583.42* 609.15* 614.41 637.75 782.94 860.04* 911.12* 967. 76 1070. 72 Page 4225 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 25 124 202 51 60 65 76 24 27 30 25 66 52 359 100 42 129 8 71 239 20 39 . 33 32 10 73 160 8 20 9 15 43 89 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 133 128 88 87 120 94 129 88 161 81 64 127 96 46 62 55 58 52 70 57 45 73 56 33 12 48 35 11 13 11 8 35 19 8 1. 24 1. 36 1.14 1. 37 1. 49 1.13 '1. 28 1. 23 0. 96 0.86 0.86 1. 23 1.19 1.18 1. 70 2.13 1. 27 0.69 1.18 1. 06 1. 42 6.83 3.49 1. 61 1. 41 0.82 1. 32 1. 72 0.92 1.11 1.25 1.63 4.91 1. 02 126.47 149.48 154.03 158.13 173.97 179.63 185.40 204.88 258.63 306.80 354.20 370.99 418.21 476.59 483.37 577.85 589.77 628.63 675.94 703.12 716.60 802.84 816.93 926. 71 1091.79 1165. 92 1217.36 1227.87 1274.53 1564.83 1719.00 1821.14 1934.42 2140.32 123 143 143 143 171 177 177 200 253 304 349 365 412 469 469 573 585 622 670 697 712 788 810 921 1088 1157 1212 1224 1269 1558 1715 1814 1924 2132 8 7.03E-03 83.1 19 3.43E-02 18.8 1.73E+OO 19 5. 60E-02 11. l 19 1. 41E-02 44. 5 6 1. 67E-02 31. 6 14 1.80E-02 24.7 2.15E+OO 14 2.12E-02 30.3 8 6.65E-03 71.4 12 7.57E-03 95.3 7 8.19E-03 53.7 8 7.06E-03 58.5 11 1.84E-02 35.9 10 1. 44E-02 38 .1 24 9.97E-02 6.3 1.28E+OO 24 2.79E-02 19.8 13 1.18E-02 39. 3 10 3.58E-02 14.4 8 2.22E-03160.l 13 1.99E-02 26.7 12 6.64E-02 9.0 9 5.56E-03 64.5 22 1. 08E-02 59. 4 18 9.03E-03 56.0 12 9.00E-03 40.6 8 2.65E-03 71.1 16 2.04E-02 24.4 13 4.46E-02 11.4 8 2.17E-03 79.9 13 5.45E-03 44.2 9 2.43E-03 76.9 8 4.03E-03 44.7 14 l.19E.:_02 33. 2 20 2.47E-02 16.2 11 2.66E-03 66.6 Peak Search Report (continued) Page : 2 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1074.01 7 4 1.12 2146.91 2144 6 1.89E-03 61. 8 36 0 1119. 38 47 0 1. 63 2237.66 2232 11 1.31E-02 14.6 37 0 1184.25 16 8 3.85 2367.40 2361 12 4.46E-03 44.5 38 0 1211.50 10 19 4.02 2421.91 2411 13 2.76E-03 96.8 39 0 1238.54* 13 20 0. 96 2476.01 2466 14 3.63E-03 79.6 40 0 1274.57 13 8 0.59 2548.08 2541 15 3.68E-03 52.9 41 0 1280.43 13 4 2.12 2559.80 2555 9 3.58E-03 40.4 42 0 1291.47 8 0 1. 35 2581. 88 2579 6 2.22E-03 35.4 43 0 1459.92* 268 5 2.15 2918.87 2911 18 7.43E-02 6.5 44 0 1558.82 8 0 0.88 3116.75 3111 11 2.22E-03 35.4 45 0 1764.00 29 6 2.40 3527.33 3522 11 7.92E-03 24.6 Flag: "*" = Peak area was modified by background subtraction Page 4226 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:53:00 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample da*te Sample ID 2-DEC-2015 15:00:00 G405235058 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:51:57 140.62 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA6 0 01:00:00.00 1.50 keV No

Empirical 75.00 Interference Report Interfering Nuclide Page 4227 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 *AM-24'3 TH-228 PB-212 BI-211* Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.66 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* 1.136E+OO 6.042E-02 7.552E-02 105.89 OK K-40 1460.82 10.66* l.005E+OO 1.278E+Ol 1.278E+Ol 12.92 OK CD-109 88.03 3.70* 5.194E+OO l.008E+OO 1. 596E+OO 129.43 OK SN-126 64.28 9.60 2.650E+OO 6.557E-01 6. 557E-01 *166 .19 OK 86.94 8.90 5.194E+OO 4.192E-01 4.192E-01 129.43 OK 87.57 37.00* 5.194E+OO 1.008E-01 1.008E-01 129.43 OK TL-208 277.37 6.60 3.958E+OO Line Not Found Absent 583.19 85.00* 2.242E+OO 2.136E-01 2.136E-01 48.76 OK . 860.56 12.50 1.625E+OO 3.833E-01 3.833E-01 89.41 OK BI-211 72.87 1. 23 3.859E+OO Line Not Found Absent 351. 06 12.92* 3.304E+OO 2.400E-01 2.400E-01 435.46 OK PB-212 74.82 10.28 4.088E+OO 1.302E+OO l.302E+OO 56.98 OK 77 .11 17.10 4.331E+OO 1.770E+OO l.770E+OO 22.26 OK 238.63 43.60* 4.430E+OO 1. llOE+OO 1. llOE+OO 12.54 OK 300.09 3.30 3.729E+00 Line Not Found Absent BI-214 609.32 45.49* 2.167E+OO 8.998E-01 9. OOlE-01 22.81 OK 1120.29 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO 1. 091E+OO 49.19 OK PB-214 74.82 5.80 4.080E+OO Line Not Found <<.INT Reject 77 .11 9.70 4.331E+OO 3.121E+00 3.122E+OO 22.26 OK 87.09 3.41 5.190E+OO Line Not Found <<INT Reject 242.00 7.25 4.384E+OO Line Not Found <<INT Reject 295.22 18.42 3.776E+OO 1.089E+OO 1.090E+OO 28.83 OK 351.93 35.60* 3.304E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 OK 1120.29 14.92 1.281E+OO l.290E+OO 1.290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO 1.091E+OO 49.19 OK RA-224 240.99 4.10* 4.384E+OO 1.403E+OO 1.403E+00 102.14 OK RA-226 609.32 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 OK 1120.29 14.92 1. 2 8 lE+O 0 1.290E+OO 1. 290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO l.091E+OO 49.19 OK AC-228 105.21 1.10 6.007E+OO Line Not Found Absent 338.32 11. 27 3.404E+00 *1. 082E+OO 1.082E+OO 53.31 OK 794.95 4.25 1. 739E+00 Line Not Found Absent 835.71 1. 61 l.666E+00 Line Not Found Absent 911. 20 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 OK 968. 97 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 OK RA-228 105.21 1.10 6.007E+OO Line Not Found Absent 338.32 11.27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 OK 794.95 4.25 1. 739E+OO Line Not Found Absent 835.71 1. 61 1.666E+OO Line Not Found Absent 911.20 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 OK 968. 97 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 OK TH-228 74.82 10.28 4.088E+OO 1.302E+OO 1.302E+OO 56.98 OK 77 .11 17.10 4.331E+OO l.770E+OO 1.770E+OO 22.26 OK 238.63 43.60* 4.430E+OO 1. llOE+OO 1. llOE+OO 12.54 OK 300.09 3.30 3.729E+00 Line Not Found Absent TH-230 609.32 45.49* 2.167E+OO 8.998E-01 8.998E-01 22.81 OK 1120.29 14.92 1. 281E+OO l.290E+OO 1.290E+OO 29.17 OK Page 4228 of 5809 Line Activity Report (continued) Page : 3 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.30 8.593E-01 1.090E+OO 1.090E+OO 49.19 OK TH-232 105.21 1.10 6.007E+OO Line Not Found Absent 338.32 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 OK 835.71 1. 61 1.666E+OO Line Not Found Absent 911.20 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 OK 968. 97 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 OK TH-234 . 63. 29 3.70* 2.650E+OO 1.701E+OO 1. 701E+OO 166.19 OK 92.59 4.23 5.546E+OO 2.088E+OO 2.088E+OO 60.51 OK U-234 609.32 45.49* 2.167E+00 8.998E-01 8.998E-01 22.81 OK 1120.29 14.92 1.281E+OO l.290E+00 1.290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO 1.090E+OO 49.19 OK U-235 89. 96 3.47 5.381E+OO 2.237E+OO 2.237E+oo 49.44 OK 93.35 5.60 5.546E+OO 1.577E+OO 1.577E+00 60.51 OK 143.76 10. 96* 5.990E+OO Line Not Found Absent 163.33 5.08 5.669E+OO Line Not Found Absent 185.72 57.20 . 5.267E+OO 1.340E-01 l.340E-01 71. 82 OK 205.31 5.01 4. 931E+OO Line Not Found Absent U-238 63.29 3.70* 2.650E+OO 1. 701E+OO 1. 701E+OO 166.19 OK 92.59 4.23 5.546E+OO 2.088E+OO 2.088E+00 60.51 OK AM-243 43.53 5.90 3.924E-01 Line Not Found Absent 74.66 67,20* 4.088E+oo* l.992E-01 1.992E-01 56.98 OK CM-247 278.00 3.40 3.951E+OO Line Not Found Abseri.t 287.50 2.00 3.852E+OO Line Not Found *Absent 402.40 72. 00* 2.988E+OO 1.037E-01 1.037E-01 118.78 OK Flag: "*" = Keyline Page 4229 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:01.63 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 . * ******************************************************************************* * . * *
DETECTOR.AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l *
Acquisition date 3-0CT-2016 07:51:57 Sensitivity : 3.000 *
Detector ID GAM06 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.66 Half life ratio : ***** *
Sample date 2-DEC-2015 15:00:00 Analyst initials: MXRl *
Sample ID G405235058 Sample Quantity 1.4062E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 7.552E-02 7.836E-02 K-40 1. 27 8E+Ol 1.618E+OO CD-109 l.596E+00 2.025E+OO SN-126 l.008E-01 1.279E-01 TL-208 2.136E-01 1.020E-01 BI-211 2.400E-01 l.024E+00 PB-212 1. llOE+OO l.364E-01 BI-214 9. OOlE-01 2.012E-01 PB-214 1.177E+OO 2.085E-01 RN-222 9.00lE-01 2.012E-01 RA-224 1.403E+OO 1.404E+OO RA-226 9.00lE-01 2.012E-01 AC-228 5.761E-01 3.752E-01 RA-228 5.761E-01 3.752E-01 TH-228 1. llOE+OO l.364E-01 TH-230 8.998E-01 2.012E-01 TH-232 5.761E-01 3.752E-01 TH-234 1. 701E+00 2.771E+OO U-234 8.998E-01 2.012E-01 U-235 -1.530E-01 l.872E-01 U-238 1. 701E+OO 2 .. 771E+OO AM-243 l.992E-01 1.112E-01 CM-247 l.037E-01 1. 207E-01 Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4230 of 5809 Key-Line Actiyity (pCi/GRAM -4.102E+OO O.OOOE+OO 1.269E-02 -1.707E-01 0.000E+OO O.OOOE+OO l.705E-03 K.L. Cnt Uncert ( 1. 96-sigma) 1.362E+Ol l.960E+41 1.758E-02 4.398E-01 1. 713E+04 5.082E+02 6.077E-02 MDA (pCi/GRAM 9. 996E-02 7.994E-01 2'.003E+OO l.272E-01 6.600E-02 3. 567E.:...Ol 9.399E-02 1.463E-01 3.626E-01 1.463E-01 1.008E+OO l.463E-01 2.910E-01 2.910E-01 9.399E-02 l.463E-01 2.910E-01 2.380E+OO 1.463E-01 3.260E-01 2.380E+OO 8.266E-02 6.739E-02 MDA (pCi/GRAM 2.569E+Ol O.OOOE+OO 5.887E-02 7.772E-01 O.OOOE+OO O.OOOE+OO l.186E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 l.384E-01 4.630E-01 9.559E-Ol FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.016E-02 4. 351E-02 7.949E-02 NOT IDENT. C0-58 1. 792E-01 6.560E-01 1.320E+OO NOT IDENT. FE-59 -1.947E+OO 7.246E+OO 1. 413E+01 FAIL ABUN C0-60 -2.169E-02 4 .*225E-02 7.685E-02 NOT IDENT. ZN-65 8.983E-02 1.839E-01 3.719E-01 NOT IDENT. GE-68 2.020E+OO 2.047E+OO 4.873E+OO NOT IDENT. AS-73 7.549E+OO 1.039E+Ol 2.208E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.044E+03 O.OOOE+OO SHORT HLIF SE-75 -2.326E-02 2.292E-01 4. ll 7E-01 FAIL ABUN BR-77 O.OOOE+OO 1.361E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8. 291E+02 O.OOOE+OO SHORT HLIF RB-83 -3.538E-01 6.272E-01 1.136E+OO NOT IDENT. KR-85 -1.858E+Ol 9.356E-t-00 1. 389E+Ol NOT IDENT. SR-85 -2.090E+OO 1.051E+OO 1.560E+OO NOT IDENT. RB-86 O.OOOE+OO 3.208E+04 O.OOOE+OO SHORT HLIF Y-88 6. 817E-02 1.110E-01 3.905E-01 NOT IDENT. Y-91 -2.083E+02 7.454E+02 l.216E+03 NOT IDENT. NB-94 -1.263E-02 3.108E-02 5.598E-02 NOT IDENT. NB-95 5.774E-01 9. 991E-01 2.050E+OO NOT IDENT. NB-95M 1.957E-01 2.765E+00 4.683E+OO NOT IDENT. ZR-95 -2.882E-01 1.759E+OO 3.263E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.022E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.855E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.229E-02 3.652E-02 5. 969E-02 NOT IDENT. RH-102 6.837E-02 6.025E-02 1.357E-01 NOT IDENT. -2.835E+OO 5.818E+OO 1.072E+Ol FAIL ABUN RH-106 2.237E-02 4.221E-01 8.509E-01 NOT IDENT. RU-106 2.237E-02 4.221E-01 8.509E-01 NOT IDENT. AG-108M -3.215E-02 2.698E-02 4.484E-02 FAIL ABUN AG-llOM 5.421E-02 8.817E-02 1. 971E-01 NOT IDENT. SN-113 -7.223E-02 2.496E-01 4.541E-01 NOT IDENT. CD-115 O.OOOE+OO 2.009E+40 O.OOOE+OO SHORT HLIF SN-117M 0. O.OOE+OO 1.359E+05 O.OOOE+OO SHORT HLIF TE-123M -3.504E-02 1.363E-01 2.485E-01 NOT IDENT. SB-124 7. 596E-02 3.073E+OO 6.265E+OO NOT IDENT. SB-125 -2.627E-02 1.070E-01 2.044E-01 FAIL ABUN TE-125M 9.559E+Ol 2. 871E+o2 5.625E+02 NOT IDENT. I-126 O.OOOE+OO 1.303E+06 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 1.648E+06 O.OOOE+OO

SHORT HLIF SB-127 O.OOOE+OO 6.412E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.269E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.869E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.592E+27 O.OOOE+OO SHORT HLIF BA-133 4.894E-03 5.346E-02 7.836E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.284E-02 5.281E-02 1.164E-01 NOT IDENT. CS-135 3.380E-02 1.620E-01 2.983E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.683E+05 O.OOOE+OO SHORT HLIF BA-137M 4.642E-02 3.850E-02 8.476E-02 NOT IDENT. CS-137 4.904E-02 4.067E-02 8.954E-02 NOT IDENT. CE-139 -8.686E-02 l.131E-01 1. 949E-01 NOT IDENT. BA-140 O.OOOE+OO 1.662E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.663E+05 O.OOOE+OO SHORT HLIF CE-141 2.817E+Ol 2.646E+Ol 5. 419E+.01 NOT IDENT. CE-143 O.OOOE+OO 6.984E+40 O.OOOE+OO SHORT HLIF CE-144 -7.366E-02 3.891E-01 6.645E-01 FAIL ABUN PM-144 1.324E-02 5.214E-02 1.058E-01 NOT IDENT. PR-144 1.189E+OO 4.549E+OO 9.238E+OO NOT IDENT. PM-146 1.308E-02 4.512E-02 9.156E-02 NOT IDENT. ND-147 O.OOOE+OO 5.207E+07 O.OOOE+OO SHORT HLIF PM-147 -3.347E+Ell 7.316E+02 1.394E+03 NOT IDENT. PM-149 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -1.835E-02 2.882E-02 4.702E-02 FAIL ABUN EU-152 1.166E-03 9.081E-02 1.739E-01 NOT IDENT. GD-153 -5.349E-02 1.574E-01 2.953E-01 FAIL ABUN EU-154 1.846E-01 1.916E-01 2.716E-01 FAIL ABUN EU-155 2.398E-02 1.112E-01 2.016E-01 FAIL ABUN TB-160 1.937E+OO 1. 786E+OO 4.239E+OO FAIL ABUN H0-166M 7.871E-03 5.148E-02 1.036E-01 FAIL ABUN TM-171 -2.742E+Ol 2.468E+Ol 4.497E+Ol NOT IDENT. HF-172 4.928E-02 2.480E-01 4.426E-01 FAIL ABUN LU-172 5.876E-02 9.137E-02 1.987E-01 FAIL ABUN LU-176 -1.208E-02 2.141E-02 4.057E-02* FAIL ABUN Page 4231 of 5809 HF-181 8.071E-01 4.529E+OO 9.173E+OO NOT IDENT. TA-182 -1. 536E-02 1.066E+OO 2.109E+OO FAIL ABUN RE-183 1.327E+OO 3.440E+OO 7.0SOE+OO NOT IDENT. RE-184 1.813E+Ol 3.674E+Ol 7.623E+Ol NOT IDENT. W-188 O.OOOE+OO 2.591E+02 2.156E+02 FAIL ABUN IR-192 -7.938E-03 5.172E-01 9.318E-01 FAIL ABUN HG-203 -3.093E+OO 3.173E+OO 5.047E+OO NOT IDENT. BI-207 -l.544E-02 5.957E-02 1.003E-01 FAIL ABUN PB-210 2.381E+OO 4.614E+OO 9.569E+OO NOT IDENT. PB-211 5.370E-01 6.003E-01 l.138E+00 NOT IDENT. BI-212 1.783E-Ol 5.427E-01 1. 076E+OO NOT IDENT. RN-219 O.OOOE+OO 1. 317E+OO 7.759E-01 FAIL ABUN RA-223 5.720E-01 5.498E-01 1.211E+OO FAIL ABUN AC-227 4.106E-02 2.457E-Ol 4. 551E-01 FAIL ABUN TH-227 4.106E-02 2.457E-01 4. 551E-01 FAIL ABUN TH-229 3.130E-02 4.717E-01 8.765E-01 FAIL ABUN PA-231 -4.929E-02 4.551E-01 8.940E-01 NOT IDENT. TH-231 5.720E-01 5.498E-01 1. 211E+OO FAIL ABUN PA-233 2.0SlE-02 6.940E-02 l.286E-01 NOT IDENT. PA-234 -l.490E-01 2.800E-01 5.238E-01 NOT IDENT. PA-234M 2.711E+OO 5.044E+00 1.066E+Ol NOT IDENT. NP-237 2.0SlE-02 6.940E-02 1.286E-01 NOT IDENT. NP-238 O.OOOE+OO 8.269E+40 O.OOOE+OO SHORT HLIF NP-239 -6.698E-02 2.234E-01 4.153E-01 FAIL ABUN PU-239 4.395E+02 8. 211E+02 6.694E+02 FAIL ABUN AM-241 -2.189E-02 1. 57 5E-01 2.870E-01 NOT IDENT. CM-243 l.252E-01 1. 753E-01 1.629E-01 FAIL ABUN BK-247 -1.648E-02 7.841E-02 1. 388E-01 FAIL ABUN CF-249 3. 881E-03 3.619E-02 7.266E-02 NOT IDENT. CF-251 1.658E-01 l.901E-01 2.156E-01 FAIL ABUN ANH-511 -7.462E-03 5.064E-02 1. 081E-01 NOT IDENT. / Page 4232 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:59.18 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error NA-22 1274.54 13 99.94* 1.136E+OO 6.042E-02 7.552E-02 105.89 K-40 1460.82 257 10.66* 1.005E+OO 1.278E+Ol l.278E+Ol 12.92 CD-109 88.03 72 3.70* 5.194E+OO 2. 012E+OO . 3.185E+OO 63.25 SN-126 64.28 31 9.60 2.650E+OO 6.557E-01 6.557E-01 166.19 86.94 72 8.90 5.194E+OO 8.365E-01 8.365E-01 63.25 87.57 72 37.00* 5.194E+OO 2.012E-01 2.012E-01 63.25 TL-208 277.37 ------6.60 3.958E+OO ------Line Not Found ------583.19 76 85.00* 2.242E+OO 2.136E-01 48.76 860.56 15 12.50 1.625E+OO 3.833E-01 3.833E-01 89.41 BI-2.11 72.87 ------1.23 3.859E+OO ------Line Not Found ------351.06 259 12.92* 3.304E+OO 3. 241E+OO 3. 241E+OO 18.08 PB-212 74.82 151 10.28 4.088E+OO 1.917E+OO 1.917E+OO 37.59 77 .11 246 17.10 4. 331E+OO 1. 770E+OO 1. 770E+OO 22.26 238.63 402 43.60* 4.430E+OO 1. llOE+OO l. llOE+OO 12.54 300.09 ------3.30 3.729E+OO ------Line Not Found ------BI-214 609.32 166 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 1120. 29 46 14.92 1. 281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO 1.091E+OO 49.19 PB-214 74.82 151 5.80 4.088E+OO 3.397E+OO 3.398E+OO 37.59 77 .11 246 9.70 4. 331E+OO 3.121E+OO 3.122E+OO 22.26 87.09 72 3.41 5.194E+OO 2.183E+OO 2.184E+OO 63.25 242.00 112 7.25 4.384E+OO 1.883E+OO 1. 883E+OO 39.68 295.22 142 18.42 3.776E+OO 1. 089E+OO 1.090E+OO 28.83 351.93 259 35.60* 3.304E+OO 1.176E+OO l.177E+OO 18.08 RN-222 609.32 166 4'5.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 1120.29 46 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO l.091E+OO 49.19 RA-224 240.99 112 4.10* 4.384E+OO 3.329E+OO 3.329E+OO 39.68 RA-226 609.32 166 45.49* 2.167E+OO 8.998E-01 9. OOlE-D.1 22.81 1120.29 46 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO .1. 091E+OO 49.19 AC-228 105.21 ------1.10 6.007E+OO ------Line Not Found ------338.32 78 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 794.95 ------4.25 l.739E+OO ------Line Not Found ------835.71 ------1. 61 ------Line Not Found ------911. 20 43 25.80* 1.544E+OO 5. 761E-01 5.761E-01 66.46 968. 97 89 15.80 1.463E+GO 2.045E+OO 2.045E+OO 32.42 RA-228 105.21 ------1.10 6.007E+OO ------Line Not Found ------338.32 78 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 794.95 ------4.25 1.739E+OO ------Line Not Found ------835.71 ------1. 61 1.666E+OO ------Line Not Found ------911.20 43 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 968.97 89 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 TH:....228 74.82 151 10.28 4.088E+OO 1.917E+OO 1. 917E+OO 37.59 77 .11 246 17.10 4.331E+OO 1. 770E+OO 1. 770E+OO 22.26 238.63 402 43.60* 4.430E+OO l. llOE+OO l. llOE+OO 12.54 300.09 ------3.30 3.729E+OO ------Line Not Found ------Page 4233 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-230 609.32 166 45.49* 2.167E+OO 8.998E-01 8.998E-01 22.81 1120.29 46 14.92 1.281E+OO l.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 l.090E+OO 1.090E+OO 49.19 TH-232 105.21 ------1.10 6.007E+OO ------Line Not Found ------338.32 78 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 835. 71 ------1. 61 1.666E+OO ------Line Not Found ------911.20 43 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 968.97 89 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 TH-234 63.29 31 3.70* 2.650E+OO 1.701E+OO 1. 701E+OO 166.19 92.59 92 4.23 5.546E+OO 2.088E+OO 2.088E+00 60.51 U-234 609.32 166 45.49* 2.167E+OO 8.998E-01 8.998E-01 22.81 1120.29 46 14.92 1. 281E+OO l.290E+OO 1. 290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO 1.090E+OO 49.19 U-235 89. 96 78 3.47 5.381E+OO 2.237E+OO 2.237E+OO 49.44 93.35 92 5.60 5 .*546E+OO 1.577E+OO l.577E+OO 60.51 143.76 ------10. 96* 5.990E+OO -------Line .Not Found ------163.33 ------5.08 5.669E+OO ------Line Not Found ------185.72 76 57.20 5.267E+OO l.340E-01 l.340E-01 71. 82 205.31 ------5. 01 . 4. 931E+OO ------Line Not Found ------U-238 63.29 31 3.70* 2.650E+OO 1. 701E+OO 1. 701E+OO 166.19 92.59 92 4.23 5.546E+OO 2.088E+00 2.088E+OO 60.51 AM-243 43.53 ------5.90 3.924E-01 ------Line Not Found ------74.66 151 67.20* 4 .. 088E+OO 2.932E-01 2.932E-01 37.59 CM-247 278.00 ------3.40 3.951E+OO ------Line Not Found ------287.50 ------2.00 3.852E+OO ------Line Not Found ------402.40 42 72.00* 2.988E+OO l.037E-01 l.037E-01 118.78 Flag: "*" = Keyline Page 4234 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Total number of lines in spectrum 45 Number of unidentified lines 9 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide NA-22 K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 Hlife 2.60Y l.25E+09Y 461. 40D 2.30E+05Y l.41E+l0Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1.41E+10Y 1. 41E+l0Y l.41E+l0Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y '1. 56E+07Y Decay 1. 25 1. 00 1. 58 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 6.042E-02 1.278E+Ol 2.012E+OO 2.012E-01 2 .136E-01 3.241E+OO 1.llOE+OO 8.998E-01 l.176E+OO 8.998E-01 3.329E+OO 8.998E-01 5.761E-01 5.761E-01 1. llOE+OO 8.998E-01 5.761E-01 1. 701E+OO 8.998E-01 1.340E-01 1.701E+OO 2.932E-01 l.037E-01 3.540E+Ol 3.540E+Ol Decay Corr pCi/GRAM 7.552E-02 1.278E+Ol 3.185E+OO 2.012E-01 2.136E-01 3. 241E+OO 1. llOE+OO 9.00lE-01 1.177E+OO 9.00lE-01 3.329E+OO 9.00lE-01 5. 761E-01 5.761E-01 1. llOE+OO 8.998E-01 5.761E-01 1. 701E+OO 8.998E-01 l.340E-01 1. 701E+OO 2.932E-01 1.037E-01 3.659E+Ol 3.659E+Ol 80.00% Decay Corr 2-Sigma Error 7. 996E-02 0.165E+Ol 2.014E+OO 1.273E-01 1. 041E-01 0.586E+OO 0.139E+OO 2.053E-01 0.213E+OO 2.053E-01 l.321E+OO 2.053E-01 3.829E-01 3.829E-01 0 .139E+OO 2.053E.:_01 3.829E-01 2.827E+OO 2.053E-01 0. 962E-01 2.827E+OO 1.102E-01 1.232E-01 "M" Manually accepted 2-Sigma %Error 105.89 12. 92 63.25 63.25 48.76 18.08 12.54 22.81 18.08 22.81 39.68 22.81 66.46 66.46 12.54 22.81 66.46 166.19 22.81 71. 82 166.19 37.59 118.78 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4235 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235058 Acquisition date : 3-0CT-2016 07:51:57 It Energy Area Bkgnd FWl-!M Channel Left Pw Cts/Sec %Err %Eff Flags 4 79.22 62. 106 1. 37 158.13 143 19 1.41E-02 88.9 4.54E+OO T 0 102.61 29 105 1. 23 204.88 200 8 6.65E-03 **** 5.94E+OO T 0 129.51 32 188 0.96 258.63 253 12 7.57E-03 **** 6.15E+OO T 0 153.61 34 93 0.86 306.80 304 7 8.19E-03 **** 5.84E+OO T 0 177.33 29 73 0.86 354.20 349 8 7.06E-03 **** 5.42E+OO T 0 209.36 59 108 1.19 418.21 412 10 l.44E-02 76.1 4.86E+OO T 0 289.24 47 60 2.13 577.85 573 13 1.18E-02 78.5 3.83E+OO T 0 314.64 9 57 0.69 628.63 622 8 2.22E-03 **** 3.60E+OO 0 358.65 22 49 1. 42 716.60 712 9 5.56E-03 **** 3.26E+OO 0 408.85 35 59 3.49 816.93 810 18 9.03E-03 **** 2.95E+OO 0 463.77 34 35 1. 61 926. 71 921 12 9.00E-03 81.2 2.68E+OO T 0 546.34 10 13 1. 41 1091.79 1088 8 2.65E-03 **** 2.36E+OO T 0 614.41 8 12 1. 72 1227.87 1224 8 2.17E-03 **** 2.15E+00 T 0 637.75 20 14 0.92 1274.53 1269 13 5.45E-03 88.4 2.09E+OO T 0 782.94 9 11 1.11 1564.83 1558 9 2.43E-03 **** 1. 76E+OO T 0 1070. 72 9 8 1. 02 2140.32 2132 11 2.66E-03 **** 1.33E+OO 0 1074.01 7 4 1.12 2146.91 2144 6 l.89E-03 **** 1.33E+OO 0 1184.25 16 8 3.85 2367.40 2361 12 4.46E-03 88.9 1.22E+OO 0 1211.50 10 19 4.02 2421.91 2411 13 2.76E-03 **** l.19E+OO 0 1238.54 13 19 0.96 2476.01 2466 14 3.63E-03 **** l.17E+OO T 0 1280.43 13 4 2;12 2559.80 2555 9 3.58E-03 80.9 1.13E+OO* 0 1291. 47 8 0 1. 35 2581. 88 2579 6 2.22E-03 70.7 l.12E+OO T 0 1558.82 8 0 0.88 3116.75 3111 11 2.22E-03 70.7 9.49E-01 Flags: "T" = Tentatively associated Page 4236 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:15.84 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l *
Acquisition date 3-0CT-2016 07:51:57 Sensitivity 3.000 *
Detector ID GAM0*6 Energy tolerance: 1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.66 Half life ratio : ***** *
Sample date 2-DEC-2015 15:00:00 Nuclide Library : SOLID *
Sample ID G405235058 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.4062E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer tp Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 Le (pCi/GRAM 4.199E-02 3.321E-01 9.394E-01 5. 968E-02.' 2.913E-02 l.609E-01 4. 311E-02 6.569E-02 1.750E-01 6.569E-02 4.623E-01 6.569E-02 l.272E-01 1. 272E-01 4. 311E-02 6.566E-02 1.272E-01 1.112E+OO 6.566E-02 l.515E-01 1.112E+OO 3.853E-02 3.024E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 423 7 of 5809 Le (pCi/GRAM 1.139E+Ol 0.000E+OO 2.086E-02 3.305E-01 O.OOOE+OO 0.000E+OO 5.062E-02 4.088E-01 NOT IDENT. SHORT HLIF NOT* IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 -I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171. HF-172 LU-172 LU-176 HF-181 Page 4238 of 5809 O.OOOE+OO 3. 661E-02 5.741E-01 5.907E+OO 3.lOOE-02 l.592E-01 2.064E+OO 1. 026E+Ol O.OOOE+OO 1.877E-01 O.OOOE+OO O.OOOE+OO 4.898E-01 6.218E+OO 6.984E-01 O.OOOE+OO l.316E-01 5.207E+02 2.418E-02 9.133E-01 2.156E+OO 1.428E+OO O.OOOE+OO O.OOOE+OO O*. OOOE+OO O.OOOE+OO 2.769E-02 6.057E-02 4.652E+00 3.639E-01 3.639E-01 1. 951E-02 8.370E-02 2.034E-01 O.OOOE+OO O.OOOE+OO l.150E-01 2.555E+OO 9.143E-02 2.627E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0. OOOE+OO
3.531E-02 O.OOOE+OO 5.166E-02 1. 37 6E-01 O.OOOE+OO O.OOOE+OO 3.827E.:.02 4.043E-02 8. 965E-02 O.OOOE+OO O.OOOE+OO 2.532E+01 O.OOOE+OO 3.088E-01 4.608E-02 4.026E+OO 4 .113E-02 O.OOOE+OO 6.433E+02 O.OOOE+OO 2.122E-02 7.826E-02 1.366E-01 l.163E-01 9.402E-02 l.834E+OO 4.466E-02 2.066E+Ol 2.065E-01 8.732E-02 1. 811E-02 4.062E+OO SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 ANH-511 Page 4239 of 5809 9.093E-01 3.284E+00 3. 321E+Ol 9.768E+01 4.215E-01 2.304E+OO 4.276E-02 4.484E+OO 5.029E-01 4.794E-01 3.503E-01 5.524E-01 2.088E-01 2.088E-01 4.050E-01 4.095E-01 5.524E-01 5.897E-02 2. 211E-01 4.717E+OO 5.897E-02 O.OOOE+OO 1.922E-01 3.152E+02 1. 334E-01 7. 521E-02 6.330E-02 3.266E-02 9.973E-02 5. lllE-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:21.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l * *Acquisition date 3-0CT-2016 07:51:57 Sensitivity : 3.000 *
Detector ID GAM06 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.66 Half life ratio : ***** *
Sample date 2-DEC-2015 15:00:00 Nuclide Library : SOLID *
Sample ID G405235058 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity l.4062E+02 GRAM *
Quantity Err ( % ) 1. 4223E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 07:26:53 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 7.552E-02 7.862E-02 K-40 l.278E+Ol 1.950E+OO CD-109 l.596E+OO 2.046E+OO SN-126 1.008E-01 1. 292E-01 TL-208 2.136E-01 1.037E-01 BI-211 2.400E-01 1.097E+OO PB-212 1. llOE+OO 1. 691E-01 BI-214 9. OOlE-01 2.153E-01 PB-214 1. l 77E+00 2.337E-01 RN-222 9.00lE-01 2.153E-01 RA-224 1.403E+OO 1.432E+OO RA-226 9.00lE-01 2.153E-01 AC-228 5.761E-01 3.827E-01 RA-228 5.761E-01 3.827E-01 TH-228 1. llOE+OO 1. 691E-01 TH-230 8.998E-01 2.152E-01 TH-232 5.761E-01 3.827E-01 TH-234 1. 701E+OO 2.797E+OO U-234 8.998E-01 2.152E-01 U-235 -l.530E-01 1. 875E-01 U-238 l.701E+OO 2.797E+OO AM-243 1.992E-01 l.132E-01 CM-247 l.037E-01 1.222E-01 Non-Identified Nuciides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4240 of 5809 Key-Line Activity* (pCi/GRAM -4.102E+OO 1.000E+41 l.269E-02 -1.707E-01 3.213E+03 3.086E+02 1. 705E-03 K.L Act error ( 1. 96-sigma) 1. 362E+Ol 1.630E+43 1.761E-02 4.403E-01 1. 713E+04 5.090E+02 6.077E-02 TPU ( 1. 96-sigma) 7.862E-02 1.950E+OO 2.046E+OO 1. 292E-01 l.037E-01 1.097E+OO 1.691E-01 2.153E-01 2.337E-01 2.153E-01 l.432E+OO 2.153E-01 3.827E-01 3.827E-01 1.691E-01 2.152E-01 3.827E-01 2.797E+OO 2.152E-01 1. 875E-01 2.797E+OO l.132E-01 l.222E-01 TPU (1.96-sigma) 1.375E+Ol O.OOOE+OO 1. 851E-02 4.470E-01 l.720E+04 5.277E+02 6.078E-02 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.384E-01 4.633E-01 4.675E-01 FAIL ABUN MN-56 1.000E+41 3.348E+41 O.OOOE+OO SHORT HLIF C0-57 -2.016E-02 4.353E-02 4.447E-02 NOT IDENT. C0-58 1.792E-Ol 6.563E-01 6.612E-Ol NOT IDENT. FE-59 -1.947E+OO 7.255E+OO 7.308E+OO FAIL ABUN C0-60 -2.169E-02 4.229E-02 4 .. 340E-02 NOT IDENT. ZN-65 8.983E-02 l.846E-01 l.890E-Ol NOT IDENT. GE-68 2.020E+OO 2.075E+OO 2.266E+OO NOT IDENT. AS-73 7.549E+OO 1.051E+Ol 1.105E+Ol NOT IDENT. AS-74 -3.527E+03 7.054E+03 7.231E+03 SHORT HLIF SE-75 -2.326E-02 2.292E-01 2.294E-01 FAIL ABUN BR-77 l.107E+39 9. 771E.+39 O.OOOE+OO SHORT HLIF SR-82 2.146E+Ol 8.291E+02 8.291E+02 SHORT HLIF RB-83 -3.538E-01 6.297E-01 6.496E-01 NOT IDENT. KR-85 -l.858E+Ol 9.492E+OO 1.266E+Ol NOT IDENT. SR-85 -2.090E+OO 1.067E+OO 1.423E+OO NOT IDENT. RB-86

2.281E+o4 3.231E+04 3.391E+04 SHORT HLIF Y-88 6.817E-02 1. lllE-01 l.153E-01 NOT IDENT. Y-91 -2.083E+02 7.456E+02 7.515E+02 NOT IDENT. NB-94 -l.263E-02 3. lllE-02 3.162E-02 NOT IDENT. NB-95 5.774E-01 1. OOlE+OO 1.034E+OO NOT IDENT. NB-95M l.957E-01 2.765E+OO 2.767E+OO NOT IDENT. ZR-95 -2.882E-01 1.759E+OO 1.764E+OO NOT IDENT. NB-97 -1.000E+41 4.274E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 1. 02 6E.+4 l O.OOOE+OO SHORT HLIF M0-99 3.047E+32 7.863E+32 O.OOOE+OO* SHORT HLIF TC-99M l.000E+41 2.984E+41 O.OOOE+OO SHORT HLIF RH-101 -2.229E-02 3.677E-02 3. 812E:....02 NOT IDENT. RH-102 6.837E-02 6.071E-02 6.809E-02 NOT IDENT. RU-103 -2.835E+OO 5.823E+OO 5.962E+OO FAIL ABUN RH-106 2.237E-02 4.221E-01 4.222E-01 NOT IDENT. RU-106 2.237E-02 4. 221E-01 4.222E-01 NOT IDENT. AG-108M -3.215E-02 2.712E-02 3.075E-02 FAIL ABUN AG-llOM 5.421E-02 8.843E-02 9.175E-02 NOT IDENT. SN-113 -7.223E-02 2.496E-01 2.517E-01 NOT IDENT. CD-115 -3.768E+39 2.010E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -7.517E+04 l.363E+05 l.404E+05 SHORT HLIF TE-123M -3.504E-02 l.363E-01 l.373E-01 NOT IDENT. SB-124 7.596E-02 3.073E+OO 3.074E+OO NOT IDENT. SB-125 -2.627E-02 l.070E-01 1. 07 6E-01 FAIL ABUN TE-125M 9.559E+Ol 2.872E+02 2.904E+02 NOT IDENT. I-126 -l.044E+05 l.303E+06 l.304E+06 SHORT HLIF SB-126 -l.950E+05 l.649E+06 1. 6.51E+06 SHORT HLIF SB-127 -2.415E+22 7.253E+22 O.OOOE+OO SHORT HLIF I-131 -5.715E+09 9.284E+09 9.634E+09 SHORT HLIF I-132 -l.000E+41 l.894E+42 O.OOOE+OO SHORT HLIF TE-132 3.407E+26 l.599E+27 O.OOOE+OO SHORT HLIF BA-133 4.894E-03 5.346E-02 5.351E-02 NOT IDENT. I-133 -l.000E+41 5. 32 6.E+41 O.OOOE+OO SHORT HLIF CS-134 5.284E-02* 5.310E-02 5.820E-02 NOT IDENT. CS-135 3.380E-02 1. 621E-01 l.628E-01 NOT IDENT. I-135 l.000E+41 8 .141E+41 O.OOOE+OO SHORT HLIF CS-136 2.296E+05 3.709E+05 3.850E+05 SHORT HLIF BA-137M 4.642E-02 3.869E-02 4.399E-02 NOT IDENT. CS-137 4.904E-02 4.087E-02 4.647E-02 NOT IDENT. CE-139 -8.686E-02 1.145E-01 1. 211E-01 NOT IDENT. BA-140 6.440E+05 l.663E+06 1.688E+06 SHORT HLIF LA-140 -3.322E+05 6.668E+05 6.834E+05 SHORT HLIF CE-141 2.817E+Ol 2.654E+Ol 2.942E+Ol NOT IDENT. CE-143 1. OOOE+41 7.109E+40 O.OOOE+OO SHORT HLIF CE-144 -7.366E-02 3.891E-01 3.905E-01 FAIL ABUN PM-144 1. 324E-02 5.216E-02 5.250E-02 NOT IDENT. PR-144 1.189E+OO 4. 551E+OO 4.582E+OO NOT IDENT. PM-146 1.308E-02 4.514E-02 4.553E-02 NOT IDENT. ND-147 -7.103E+06 5.208E+07 5.217E+07 SHORT HLIF PM-147 -3.347E+Ol 7.317E+02 7.318E+02 NOT IDENT. PM-149 -3.033E+40 3.220E+41 O.OOOE+OO SHORT HLIF EU-150 -l.835E-02 2.887E-02 3.004E-02 FAIL ABUN EU-152 1.166E-03 9.081E-02 NOT IDENT. GD-153 -5.349E-02 l.574E-01 1.593E-01 FAIL ABUN EU-154 1. 846E-01 l.922E-01 2.094E-01 FAIL ABUN EU-155 2.398E-02 1.113E-01 1.118E-01 FAIL ABUN TB-160 1. 937E+OO l.803E+OO 2.004E+OO FAIL ABUN H0-166M 7.871E-03 5.148E-02 5.160E-02 FAIL ABUN TM-171 -2.742E+Ol 2.481E+Ol 2.771E+Ol NOT IDENT. HF-172 4.928E-02 2.481E-01 2.491E-01 FAIL ABUN LU-172 5.876E-02 9.209E-02 9.583E-02 FAIL ABUN LU-176 -l.208E-02 2.144E-02 2.212E-02 FAIL ABUN Page 4241 of 5809 HF-181 8.071E-01 4.529E+OO 4.544E+OO NOT IDENT. TA-182 -l.536E-02 1.066E+OO 1.066E+OO FAIL ABUN RE-183 l.327E+OO 3.446E+OO 3.498E+OO NOT IDENT. RE-184 1.813E+Ol 3.707E+Ol 3.796E+Ol NOT IDENT. W-188 3.367E+02 2.634E+02 3.040E+02 FAIL ABUN IR-192 -7.938E-03 5 .172E-01 5 .172E-01 FAIL ABUN HG-203 -3.093E+OO 3.186E+OO 3.478E+OO NOT IDENT. BI-207 -l.544E-02 5. 963E-02 6.003E-02 FAIL ABUN PB-210 2.381E+OO 4.618E+OO 4.742E+OO NOT IDENT. PB-211 5.370E-01 6.022E-01 6. 491E-01 NOT IDENT. BI-212 l.783E-01 5.430E-01 5.489E-01 NOT IDENT. RN-219 l.131E+OO 1.327E+OO 1.422E+OO FAIL ABUN RA-223 5.720E-01 5.530E-01 6.lOlE-01 FAIL ABUN AC-227 4.106E-02 2.457E-01 2.464E-01 FAIL ABUN TH-227 4.106E-02 2.457E-01 2.464E-01 FAIL ABUN TH-229 3.130E-02 4.717E-01 4.719E-01 FAIL ABUN PA-231 -4.929E-02 4.553E-01 4.558E-01 NOT IDENT. TH-231 5.720E-01 5.530E-01 6. lOlE-01 FAIL ABUN PA-233 2.051E-02 6.943E-02 7.004E-02 NOT IDENT. PA-234 -l.490E-01 3.284E-01 3.352E-01 NOT IDENT. PA-234M 2. 711E+OO 5.061E+OO 5.206E+OO NOT IDENT. NP-237 2.051E-02 6.943E-02 7.004E-02 NOT IDENT. NP-238 -1.000E+41 8.394E+40 O.OOOE+OO SHORT HLIF NP-239 -6.698E-02 2.235E-01 2.255E-01 FAIL ABUN PU-239 4.395E+02 8.217E+02 8.453E+02 FAIL ABUN AM-241 -2.189E-02 1. 57 SE-01 l.578E-01 NOT IDENT. CM-243 l.252E-01 l.758E-01 1. 846E-01 FAIL ABUN BK-247 -1.648E-02 7.849E-02 7.884E-02 FAIL ABUN CF-249 3. 8*81E-03 3.619E-02 3.624E-02 NOT IDENT. CF-251 1.658E-01 1.913E-01 2.053E-01 FAIL ABUN ANH-511 -7.462E-03 5.065E-02 5.076E-02 NOT IDENT. Page 4242 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 62.9377 879.38 77.4414 482.18 66.2441 45.60 71.0732 87.57 77.4662 133.52 62.1524 46.54 56.6870 87.09 77.4911 264.66 54.0733 49. 72 0.0000 87.57 76.2976 122.06 58.2747 51. 35 44.4594 88.03 76.3708 140.51 0.0000 51. 87 60.2444 88.34 76.4203 143.76 72.5976 52.39 64.7096 193.51 76.4410 144.24 63.1732 52. 97 54.3087 89. 96 72.8428 145.44 45.3542 53.44 43.8576 90.64 72. 944"9 152.43 53.9833 125.81 43.9379 91.11 0.0000 153.25 0.0000 57.36 0.0000 63.29 73.2342 154.21 58.7480 57.53 56.7952 143.76 "73.3461 156.02 0.0000 57.98 54.2001 94.56 65.7842 158.56 0.0000 1093.63 59.7424 94.65 65.7961 159.00 56.9910 57.98 62.4257 94.67 65.7987 162.33 62.6525 59.54 61.8682 94.87 65.8247 162.66 0.0000 60.96 56 .1338 97. 43. 58.3736 163.33 53.0023 61.17 56.1653 311. 90 46.7893 165.86 59.6955 62.93" 66.6320 946.00 46.7904 176.31 41. 8118 63.29 66.6947 99.53 53.4008 1048.07 0.0000 63.58 66.7451 1221. 41 46.9409 177. 52 42.6109 64.28 66.8660 265.00 41.2233 739.50 0.0000 66.73 67.8911 103.18 49.8371 181.52 59.0714 67.24 86.1867 103.37 49.8549 711. 68 60.0257 67.68 90.2309 116.74 49.8549 185.72 60.1230 67.75 90.2467 105.21 59.2406 193.51 48.3304 69.67 72. 0521 105.31 59.2516 197.03 55.3052 70.83 97.9736 106.12 45.4939 127.23 49.7189 72.81 62.7549 106.47 70.2638 306.78 48.8061 279.20 62.7638 109.28 59 .*6814 203.43 57.9937* 72.87 62.7638 111. 00 52.8811 205.31 51. 6613 74.66 63.0289 228.16 0.0000 210.85 48.9284 74.82 63.0522 114.06 55.1733 215.65 46.1163 1063.66 63.0745 116. 30 0.0000 222 .11 55.7314 238.63 63.3863 116.74 57.4453 290.67 39.6876 351. 93 63.3863 119.76 43.5593 177.52 46.7059 78.74 63.6213 121.12 48.7357 228.16 0.0000 79 .. 69 63.7567 121. 22 48.7438 228.18 50.2515 80.12 51. 3046 121.78 45.7399 235.69 43.9733 80.19 0.0000 122.06 54.9134 256.23 41. 2367 80.57 53. 8611 122.92 54.9921 238.63 41. 3499 81. 00 50.1514 123.07 49.9125 238.98 0.0000 81. 07 50.1591 123. 68 . 57.1006 240.99 41. 4498 81. 75 65.3042 125.81 60.0287 242.00 41.4920 323.87 64.3336 127.23 69.7388 344.28 41. 6058 84.00 64.3627 127.91 63.6556 252.40 0.0000 85.43 92.4099 129.30 63.7975 252.80 39.5450 86.55 77.4029 131.20 63.9905 254.15 0.0000 Page 4243 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 256.23 38.4753 351.93 28.7159 583.19 19.0866 260.90 0.0000 507.63 0.0000 584.27 19. 0966 264.66 37.5760 356.01 26.1865 595.83 0.0000 264.80 35.1561 364.49 0.0000 600.60 18.2424 265.00 40.0123 366.42 0.0000 602.52 0.0000 268.22 43.7827 372. 51 28.2773 604. 72 16.7565 269.46 42.6167 129.30 19.4765 607.14 30.5029 270.03 34 .1113 377.52 22.1720 609.32 25.9555 271.23 51. 2247 383.85 26. 7279 497.08 25. 9690 273.65 0.0000 388.16 25.0229 433.94 16.8364 356.01 41.6658 388.63 0.0000 696. 49 9.2003 277.37 39.2500 391. 69 29.0270 620.36 12.2813" 277.60 39.2578 400.66 25.6930 621.93 11.2663 278.00 41. 7270 401. 81 25.7133 667. 71 0.0000 279.20 56.5159 402.40 25.7238 631. 2 9 10.2889 279.54 54.0748 404.85 8.1370 453.88 16.9921 279.70 54.0829 410.95 20. 4272 595.83 0.0000 280.46 44.2804 413.71 31. 3800 635.95 6.1870 283.69 40.7092 414.70 0.0000 636.99 0.0000 364.49 0.0000 423.72 0.0000 645.85 13.4687 285.41 39.5361 404.85 24.7780 884.68 18.7537 285.90 0.0000 427.87 27.5452 657.90 0.0000 402.40 33.0086 433.94 30.4199 661. 66 13.5686 290.67 29.7913 333.97 31.4524 664.57 . 0.0000 293.27 0.0000 453.88 22.4067 666.33 0.0000 295.22 29.9106 463.37 19.7221 720.70 0.0000 295. 96 29.9297 468.07 16.9534 667. 71 0.0000 298.58 43.3312 685.70 0.0000 677.62 9.4629 299.98 39.0448 475.06 15.1338 685.70 0.0000 300.09 39.0486 476.78 27.4589 695.00 0.0000 300.13 39.0495 477.60 24.6305 696.49 12. 7251 301.36 41. 7643 482.18 18.0487 696.51 12. 7251 302.85 32.6174 1596.21 0.0000 697.00 0.0000 304.50 30.9884 527.90 0.0000 697.30 15. 9119 537.26 0.0000 497.08 20.1246 697.49 13.7916 306.78 31. 048 6 505.52 26.0013 702.65 18.0763 316.51 27.2274 507.63 0.0000 706.68 18.1088 311. 90 35.3973 511. 00 35.7436 711. 68 11. 7430 316.51 30.4570 514.00* 59. 9969 720. 70 0.0000 531.02 0.0000 514.00 59. 9969 721. 93 0.0000 320.08 0.0000 520.40 19.4238 1690.97 18,. 2361 427. 87 ' 38.2132 238.98 *o.oooo 722.91 15.0191 323.87 21. 2789 522.65 0.0000 1274.44 17.1673 325.23 35.7878 527.90 0.0000 724.19 20.3939 328.76 0.0000 528. 2 6 17.5591 727.33 18. 2721 388.16 33.4498 520.40 18.5477 733.00 12.9292 333.97 39. 9013 529.87 0.0000 735.93 21. 5755 334.37 39.9146 5.31. 02 0.0000 737.46 10.7951 338.28 32.7189 537.26 0.0000 739.50 0.0000 911.20 32.7204 546.56 0.0000 747.24 10.8398 340.48 25.8752 552.55 17.7935 748.06 7.5905 340.55 0.0000 563.25 17.8945 752.31 16.2939 344.28 26.9902 795.86 17.9524 753.82 0.0000 345.93 22.8674 569.50 17.9539 756.73 18. 5011 351. 06 28.6971 569.70 17.9553 756.80 18. 5011 Page 4244 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 763.94 15.2817 984.45 0.0000 1596.21 0.0000 765.81 15.2931 996.26 15.1645 1620.50 6.3270 766.42 14.2045 1001.03 13.4015 1621. 92 7.3841 766.84 16.3928 1002.74 12.5153 1678.03 0.0000 772.60 0.0000 1004.73 16.1016 1690.97 6.4244 776.52 0.0000 1021. 30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 d.0000 1764.49 1. 7396 778. '90 6.5896 1028.54 0.0000. 1770.23 6.5310 783.70 0.0000 846.77 8.1381 1771.35 2.1776 727. 33 9.9104 1038.76 0.0000 1791.20 0.0000 792.07 20.9784 1046.59 11. 7876 1808.65 0.0000 794.95 7.7377 1048.07 0.0000 846.75 0.0000 795.86 9.9521 1049.04 7.2598 1836.06 0.0000 801. 95 15.5187 621. 93 6.3549 810.06 14.4563 1063.66 13.1282 810.29 13.3457 1077.00 0.0000 810.45 12.2345 1077.34 2.9299 810.76 12.2358 1085.87 8.2617 815.77 0.0000 1093.63 11.0420 818.51 0.0000 1099.45 11.0618 832.01 12.3374 1112. 07 13.8803 834.85 11. 228 0 1112. 84 10.5783 835.71 12;3549 1115. 54 7.4106 1260.41 0.0000 609.32 8.9057 846.75 0.0000 889.28 8.9063 846.77 9.0234 1121. 30 5.9391 856.80 0.0600 1129.67 12.0939 860.56 5.1022 1131.51 0.0000 702.65 4.5531 1147.95 0.0000 873.19 9 .1133 1173.23 15.0771 529.87 0.0000 1177.95 9.0586 879.38 4. 5671 1189.05 9.0873 880.51 11. 4225 1204.77 15.2139 883.24 10.2905 1221.41 13.3745 884.68 5. 7200 1231. 02 18.3914 889.28 14.8969 1235.36 0.0000 903.28 18. 3711 1238.28 12.4771 898.04 11. 4958 1260.41 0.0000 900.72 17.2601 1271.87 3.0998 903.28 10.3656 1274.44 9.3059 911.20 16.1704. 1274.54 9.3059 912.08 16.1755 1099.45 9.7382 923.98 0.0000 1298.22 0.0000 926.50 8.1291 1312 .11 0.0000 929 .11 9.2992 1332. 49 9.8438 937.49 11.6581 1362.66 0.0000 944.13 0.0000 1365.19 3.9707 946.00 14.9082 1368. 63 0.0000 949.00 6.1451 1384.29 2.9925 954.55 0.0000 1408.01 3.0104 962.31 16.9318 1457.56 0.0000 964.08 14 .1187 1460.82 8.1318 966 .17 14.1289 696. 51 5.1169 968.97 14.1421 1505.03 5 .1361 983.53 0.0000 1584.12 8.3682 Page 4245 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:53:53.65 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM07.CNF;484 Background date : Z-OCT-2016 11:00:17. Sample date 16-DEC-2015 12:26:00 Acquisition date : 3-0CT-2016 07:52:25. Sample ID G405235059 Sample quantity 1.54222E+02 GRAM Detector name : GAM07 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.48 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 0 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 2 2 2 2 0 0 0 0 0 0 0 0 0 Page 4246 of 5809 Energy 63.60* 72. 79 74.78* 77.22 87.32 92.80* 134. 52 148.88 179.99 186.25* 209.57 238.62* 241.92 278.61 295.23* 338.34* 352.03* 382.20 399.15 452. 96 463.12 510.65*" 513.20 583.03* 588.34* 598.02 609.32* 657.01 661.62 670.17 727.18* 769.31 860.05 911. 05* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 15 29 152 184 66 71 38 16 17 68 49 351 99 26 138 71 198 12 20 23 32 15 19 110 19 10 159 24 25 7 34 35 17 44 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit
144 97 115 113 157 121 90 49 99 108 102 53 65 46 53 51 60 . 21 35 44 27 22 20 17 18 30 58 18 10 32 28 23 9 15 1. 36 1. 24 1. 08 1. 07 1. 23 1. 62 0.71 0.66 0.62 0.79 1. 94 1.15 1. 87 1".41 1. 33 1. 08 1. 24 0.78 1. 03 1. 83 1. 23 1. 85 1. 69 1. 92 1. 93 0.50 1. 63 2.79 1. 9-8 4.30 1. 59 6.17 0.78 0. 96 127.70 146.07 150.05 154.93 175.11 186.09 269.50 298.21 360.41 372. 93 419.57 477.65 484.24 557.62 590.84 677.05 704.43 764.75 798.Ei5 906.24 926. 56 1021. 59 1026.69 1166.33 1176.94 1196. 30 1218.89 1314.27 1323.48 1340.57 1454.57 1538.83 1720.29 1822.26 124 143 143 143 171 183 266 296 359 368 415 471 471 553 586 673 698 762 794 896 921 1016 1016 1159 1159 1187 1210 1305 1319 1328 1448 1528 1715 1815 7 4.04E-03144.1 17 8.04E-03 54.1 1.91E+OO 17 4.23E-02 13.8 17 5.llE-02 11.8 8 1. 83E-02 35. 2 7 1. 98E-02 30. 0 8 l.06E-02 46.7 5 4.52E-03 69.4 8 4.86E-03100.4 10 l.90E-02 32.1 11 l.36E-02 42.5 28 9.75E-02 6.5 1.45E+OO 28 2.76E-02 21.5 10 7.15E-03 52.7 11 3.84E-02 13.6 10 l.98E-02 22.8 12 5.51E-02 10.7 7 3.33E-03 69.6 11 5.52E-03 62.4 16 6.46E-03 67.0 11 8.87E-03 36.4 16 4.28E-03 93.3 9.12E-01 16 5.37E-03 62.8 27 3.06E-02 12.6 2.47E+OO 27 5.36E-03 49.1 12 2.78E-03114.0 18 4.42E-02 13.9 15 6.58E-03 44.8 10 6.94E-03 31.0 16 1. 94E-*03184. 6 14 9.39E-03 38.0 19 9.72E-03 37.3 10 4.60E-03 43.1 13 1. 23E-02 25. 0 Peak Search Report (continued) Page : 2 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 963.99 14 8 0.63 1928.14 1922 9 3.79E-03 47.7 36 0 968.61* 50 18 1. 51 1937.38 1932 11 l.39E-02 22.5 37 0 1121.69 29 36 2.37 2243.49 2232 18 8.19E-03 51. l 38 0 1236.82 39 10 4.95 2473.72 2464 20 1. 08E-02 25.5 39 0 1244.12 14 3 1. 57 2488.33 2485 8 3.89E-03 35.7 40 0 1250.13 21 0 1. 06 2500.33 2494 13 5.83E-03 21. 8 41 0 1460.43* 277 9 2.49 2920.91 2914 16 7.69E-02 6.5 42 0 1763.79* 32 0 1. 67 3527.61 3521 13 8.98E-03 19.1 Flag: "*" = Peak area was modified by background subtraction Page 4247 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:53:56 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 16-DEC-2015 12:26:00 G405235059 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:52:25 154. 22 GRAM -Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA7 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4248 of 5809 PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 279'.20 74.66 74.82 74.82 351.06 CAN 0 01:00:00.48 10.00 ' 0. 00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.122E+OO 1.089E+Ol l.089E+Ol 13.08 OK KR-85 514.00 0.43* 2.624E+OO 8.956E+OO 9.438E+OO 125.53 OK SR-85 514.00 96. 00* 2.624E+00 4.049E-02 9.167E-01 125.53 OK CD-109 88.03 3.70* 5.750E+00 1.0lOE+OO 1.566E+OO 137.29 OK SN-126 64.28 9.60 3.539E+OO 2.749E-01 2.749E-01 288.28 OK 86.94 8.90 5.750E+00 4. 201E-01 4.201E-01 137.29 OK 87.57 37.00* 5.750E+OO 1.0lOE-01 l.OlOE-01 137.29 OK BA-137M 661.66 89.90* 2.138E+00 6.687E-02 6.811E-02 61. 97 OK CS-137 661.66 85.10* 2 .138E+00 7.064E-02 7.195E-02 61.97 OK CE-144 80.12 1. 36 5.243E+OO Line Not Found Absent 133.52 11. 09* 6.655E+OO 3.103E-01 6.312E-01 93.36 OK HG-203 70.83 3.69 4.380E+00 Line Not Found Absent 72.87 6.19 4.582E+00 6.482E-01 4.981E+Ol 108.28 OK 279.20 81.56* 4.361E+OO 1.716E-02 1.319E+OO 252.06 OK TL-208 277.37 6.60 4.377E+OO Line Not Found <<INT Reject 583.19 85.00* 2.366E+00 2.859E-01 2.859E-01 25.13 OK 860.56 12.50 1.737E+OO 3.815E-01 3.815E-01 86.16 OK PB-212 74.82 10.28 4.777E+OO 1.398E+OO 1.398E+OO 40.28 OK 77 .11 17.10 5.000E+OO 1.359E+OO 1.359E+OO 23.60 OK' 238.63 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 OK 300.09 3.30 4.103E+OO Line Not Found Absent BI-214 609.32 45.49* 2.284E+00 7.943E-01 7.946E-01 27.84 OK 1120.29 14.92 l.404E+OO 6.828E-01 6.831E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 OK PB-214 74.82 5.80 4.781E+OO Line Not Found <<INT Reject 77 .11 9.70 5.000E+OO 2.395E+OO 2.396E+OO 23.60 OK 87.09 3.41 5.736E+OO Line Not Found <<INT Reject 242.00 7.25 4.877E+OO Line Not Found <<INT Reject 295.22 18.42 4.159E+OO 1.006E+OO 1.007E+OO 27.17 OK 351.93 35.60* 3. 591E+OO 8.509E-01 8.512E-01 21. 49 OK RN-222 609.32 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 OK 1120.29 14.92 1.404E+OO 6.828E-01 6.831E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 OK RA-224 240.99 4.10* 4.879E+OO l.048E+OO 1.048E+OO 124.88 OK RA-226 609.32 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 OK 1120.29 14.92 1.404E+OO 6.8.28E-01 6. 831E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+OO 1. 032E+OO 38.16 OK AC-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 OK 794.95 4.25 l.849E+00 Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not *Found Absent 911.20 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 OK 968. 97 15.80 1. 581E+OO 9.879E-01 9.879E-01 45.02 OK RA-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11.27 3.713E+OO 9.407E-01 9.407E-01 45.57 OK 794.95 4.25 1. 849E+OO Line Not Found Absent 835.71 1. 61 l.777E+OO Line Not Found Absent 911. 20 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 OK 968. 97 15.80 1.581E+OO 9.879E-01

9.879E-01 45.02 OK Page 4249 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff p'Ci/GRAM pCi7GRAM %Error Status TH-228 74.82 10.28 4.777E+OO 1.398E+00 1.398E+OO 40.28 OK 77 .11 17.10 5.000E+OO 1.359E+OO l.359E+OO 23.60 OK 238.63 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 OK 300.09 3.30 4.103E+OO Line Not Found Absent TH-230 609.32 45.49* 2.284E+OO 7.943E-01 . 7. 943E-01 27.84 OK 1120.29 14.92 l.404E+OO 6.828E-01 6.828E-01 102.23 OK 1764.49 15.30 9.426E-01 l.032E+00 1. 032E+OO 38.16 OK TH-232 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 OK 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 OK 968.97 15.80 1.581E+OO 9.879E-01 9.879E-01 45.02 OK TH-234 *63.29 3.70* 3.539E+OO 7 .133E-01 7.133E-01 288.28 OK 92.59 4.23 6.049E+OO 1.730E+OO 1.730E+OO 60.04 OK U-234 609.32 45.49* 2.284E+00 7. 943E-01* 7.943E-01 27.84 OK 1120.29 14.92 1.404E+OO 6.828E-01 6 .. 828E-01 102*. 23 OK 1764.49 15.30 9.426E-01 1.032E+OO l.032E+00 38.16 OK U-238 63.29 3.70* 3.539E+OO 7.133E-01 7.133E-01 288.28 OK 92.59 4.23 6.049E+OO 1. 730E+OO 1. 730E+00 60.04 OK AM-243 43.53 5.90 6.933E-01 Lin.e Not Found Absent 74.66 67.20* 4.777E+OO 2.139E-01 2.139E-01 40.28 OK ANH-511 511. 00 100.00* 2.635E+OO 3. 091E-02 3.091E-02 186.67 OK Flag: "*" Key line Page 4250 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:57.55 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l *
Acquisition date 3-0CT-2016 07:52:25 Sensitivity : 3.000 *
Detector ID GAM07 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
Sample date 16-DEC-2015 12:26:00 Analyst initials: MXRl *
Sample ID G405235059 Sample Quantity l.5422E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1 . 96-sigma ) (pCi/GRAM K-40 l.089E+Ol 1. 396E+OO 5.482E-01 KR-85 9.438E+OO l.161E+Ol *1.007E+Ol SR-85 9.167E-01 l.128E+OO 9.777E-01 CD-109 l.566E+OO 2.108E+OO 2.042E+OO SN-126 l.OlOE-01 1.360E-01 l.235E-01 BA-137M 6.811E-02 4.136E-02 5.203E-02 CS-137 7.195E-02 4.370E-02 5.497E-02 CE-144 6.312E-01 5.775E-01 6.368E-01 HG-203 1.319E+OO 3.257E+OO 3.283E+OO TL-208 2.859E-01 7.039E-02 5.315E-02 PB-212 9.310E-01 1. 181E-01 8.188E-02 BI-214 7.946E-01 2.168E-01 l.003E-01 PB-214 8.512E-01 1.793E-01 l .119E-01 . RN-222 7.946E-01 2.168E-01 l.003E-01 RA-224 1.048E+OO l.283E+OO 8.779E-01 RA-226 7.946E-01 2.168E-01 1.003E-01 AC-228 5.125E-01 2.514E-01 1.938E-01 RA-228 5.125E-01 2.514E-01 l.938E-01 TH-228 9.310E-01 1.181E-01 8.188E-02 TH-230 7.943E-01 2.167E-01 l.002E-01 TH-232 5.125E-01 2.514E-01 l.938E-01 TH-234 7.133E-01 2.015E+OO l.894E+OO U-234 7.943E-01 2.167E-01 l.002E-01 U-238 7.133E-01 2.015E+OO 1. 894E+OO AM-243 2.139E-01 8.445E-02 7. 012E...:02 ANH-511 3.091E-02 5.655E-02 4.124E-02 Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 7.517E+OO l.102E+Ol 2.294E+Ol NOT IDENT. NA-22 -l.128E-02 3.941E-02 7.530E-02 NOT IDENT. NA-24 O.OOOE+OO 1.022E+41 O.OOOE+OO SHORT HLIF AL-26 l.592E-02 l.801E-02 5.723E-02 NOT IDENT. Page 4251of5809 SC-46 4.706E-02 2.583E-01 5. 613E-01 FAIL ABUN V-48 O.OOOE+OO 8.489E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.034E+02 O.OOOE+OO SHORT HLIF MN-54 l.713E-02 5.108E-02 1.lOlE-01 NOT IDENT. C0-56 1.229E-01 3.322E-01 7.339E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 9.700E-04 4.375E-02 8.216E-02 NOT IDENT. C0-58 -4.837E-01 5.007E-01 7.692E-01 NOT IDENT. FE-59 .:.l.555E-01 4.542E+OO 9.330E+OO NOT IDENT. C0-60 -3.350E-02 3.385E-02 5.224E-02 NOT IDENT. ZN-65 -9.375E-02 1. 7 61E-01 2. 691E-01 NOT IDENT. GE-68 1.547E-01 2.376E+OO 4.753E+OO NOT IDENT. AS-73 1.536E+OO 6.234E+OO 1.259E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.219E+03 O.OOOE+OO SHORT HLIF SE-75 3.439E-02 1.517E-01 3.126E-01 FAIL ABUN BR-77 O.OOOE+OO 2.049E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5. 713E+02 O.OOOE+OO SHORT HLIF RB-83 6.140E-02 5.735E-01 1.129E+OO NOT IDENT. RB-86 O.OOOE+OO 2.103E+04 O.OOOE+OO SHORT HLIF Y-88 1. OllE-02 l.654E-01 3.892E-01 NOT IDENT. Y-91 1.307E+02 4.997E+02 1.013E+03 NOT IDENT. NB-94 3.563E-03 3.026E-02 5.843E-02 NOT IDENT. NB-95 1.723E-01 6.969E-01. 1.380E+OO NOT IDENT. NB-95M -6.126E-01 2.043E+OO 3.555E+OO NOT IDENT. ZR-95 1.402E+OO 1. 311E+OO 2.880E+OO NOT IDENT. NB-97 O.OOOE+OO 8.772E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 o*. OOOE+OO l.858E+31 O.OOOE+OO . SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.778E-03 3.109E-02 5.766E-02 NOT IDENT. RH-102 l.395E-02 6.030E-02 l.186E-01 NOT IDENT. RU-103 -7. 381E-01 3.839E+OO 7.400E+OO FAIL ABUN RH-106 2.025E-01 4.601E-01 9.427E-01 NOT IDENT. RU-106 2.025E-01 4.601E-01 9.427E-01 NOT IDENT. AG-108M -1. 490E-03 2.210E-02 4.348E-02 NOT IDENT. AG-llOM -2. 896E-02 8.181E-02 1.588E-01 FAIL ABUN SN-113 1. 07 OE-01 1. 674E-01 3.605E-01 NOT IDENT. CD-115 O.OOOE+OO 2.577E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 5.855E+04 O.OOOE+OO SHORT HLIE' TE-123M -l.493E-02 l.121E-01 2.048E-01 NOT IDENT. SB-124 5.087E-01 1. 730E+00 3.951E+00 NOT IDENT. SB-125 -8.908E-04 9.241E-02 l.808E-01 FAIL ABUN TE-125M -2.700E+Ol 2.166E+02 4.046E+02 NOT IDENT. I-126 O.OOOE+OO 5.751E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 6.989E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4.437E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.211E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5. 996E+25 O.OOOE+OO SHORT HLIF BA-133 2. 962E-02 3.615E-02 7.228E-02 NOT IDENT. I-133 O.OOOE+OO 1.747E+41 O.OOOE+OO SHORT HLIF CS-134 4.534E-02 4.753E-02 1.030E-01 NOT "IDENT. CS-135 -7.331E-02 1. 201E-01 2.259E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.051E+05 O.OOOE+OO SHORT HLIF CE-139 4.492E-02 l.OOlE-01 1.912E-01 NOT IDENT. BA-140 O.OOOE+OO 7.700E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1. 968E+05 O.OOOE+OO SHORT HLIF CE-141 -7.395E+OO 2.023E+Ol 3.319E+Ol NOT IDENT. CE-.143 O.OOOE+OO l.585E+41 O.OOOE+OO SHORT HLIF PM-144 -7.689E-03 5.624E-02 1.040E-01 NOT IDENT. PR-144 -7.228E-01 4.857E+OO 8.963E+OO NOT IDENT. PM-146 7.277E-02 9.556E-02 7.303E-02 FAIL ABUN ND-147 O.OOOE+OO 1.914E+07 O.OOOE+OO SHORT HLIF PM-147 -1. 964E+02 7.712E+02 l.416E+03 NOT IDENT. PM-149 O.OOOE+OO 3.386E+39 O.OOOE+Od SHORT HLIF EU-150 l.155E-02 2.408E-02 4.548E-02 FAIL ABUN EU-152 7.353E-02 8.385E-02 1. 790E-01 FAIL ABUN GD-153 -2.923E-02 l.502E-01 2.806E-01 NOT IDENT. EU-154 -3.012E-02 9.645E-02 1.833E-01 NOT .IDENT. EU-155 l.494E-02 9.463E-02 l.818E-01 FAIL ABUN TB-160 l.505E-01 1.227E+OO 2.650E+OO FAIL ABUN H0-166M 2.305E-02 5.073E-02 l.044E-01 NOT IDENT. TM-171 l.147E+Ol 1.577E+Ol 3.302E+Ol NOT IDENT. HF-172 -4.844E-02 1.948E-01 3.582E-01 FAIL ABUN LU-172 3.773E-02 6.077E-02 l.381E-01 FAIL ABUN LU-176 l.260E-02 2.082E-02 4. 372E-02 FAIL ABUN HF-:)..81 7.512E-01 3.840E+OO 7.579E+OO FAIL ABUN Page 4252 of 5809 TA-182 5.890E-01 7.914E-01 1. 752E+OO FAIL ABUN RE-183 1.356E+00 2.158E+OO 4.444E+OO NOT IDENT. RE-184 l.928E+01 2.132E+Ol 4.980E+Ol NOT IDENT. W-188 2.429E+Ol 9 .. 271E+Ol 1. 721E+02 FAIL ABUN IR-192 -4.843E-02 4.043E-01 7.776E-01 FAIL ABUN BI-207 4.790E-02 4.467E-02 l.037E-01 FAIL ABUN PB-210 1.llOE+OO 2.483E+oo* 5.099E+OO NOT IDENT. BI-211 O.OOOE+OO 4.938E-01 7. 661E-01 FAIL ABUN PB-211 -l.553E-01 6.407E-01 l.158E+OO NOT IDENT. BI-212 O.OOOE+OO 9.695E-01 1. 263E+OO FAIL ABUN RN-219 -l.461E-01 3.692E-01 6.090E-Ol NOT IDENT. RA-223 -4.198E-01 5.266E-01 9.556E-01 FAIL ABUN AC-227 9.510E-03 l.800E-01 3 .*635E-01 NOT IDENT. TH-227 9.510E-03 l.800E-01 3.635E-01 NOT IDENT. TH-229 -3.598E-01 4.533E-01 7.603E-01 FAIL ABUN PA-231 4.705E-02 3.484E-01 6.817E-01 NOT IDENT. TH-231 -4.198E-01 5.266E-01 9.556E-01 FAIL ABUN PA-233 l.272E-02 5.619E-02 l.128E-01 NOT IDENT. PA-234 l.094E-01 2.485E-01 5. 372E-01 NOT IDENT. PA-234M -2.999E+OO 3.997E+OO 7.239E+OO NOT IDENT. U-235 -4.179E-02 l.642E-01 2. 964E-01 FAIL ABUN NP-237 1. 272E-02 5.619E-02 l.128E-01 NOT IDENT. NP-238 O.OOOE+OO 2.881E+40 0 .. OOOE+OO SHORT HLIF NP-239 3.381E-03 2 .131E-01 4.026E-01 FAIL ABUN PU-239 -2.255E+Ol 2. 991E+02 5. 531E+02 NOT IDENT. AM-241 -4.930E-02 l.177E-01 2.055E-01 NOT IDENT. CM-243 -l.268E-02 8.494E-02 l.596E-01 FAIL ABUN BK-247 l.355E-02 5.526E-02 *. l.140E-01 NOT IDENT. CM-247 -2.023E-02 3.396E-02 5.398E-02 FAIL ABUN CF-249 -2.376E-04 3.370E-02 6.606E-02 NOT IDENT. CF-251 5.777E-02 l.120E-01 2.005E-01 NOT IDENT. Page 4253 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:53:54.48 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 268 10.66* 1.122E+OO 1.089E+Ol l.089E+Ol 13.08 KR-85 514.00 21 0.43* 2.624E+OO 8.956E+OO 9.438E+OO 125.53 SR-85 .514.00 21 96. 00* 2.624E+OO 4.049E-02 9.167E-01 125.53 CD-109 88.03 85 3.70* 5.750E+OO l.938E+OO 3.004E+OO 70.39 SN-126 64.28 19 9.60 3.539E+OO 2.749E-01 2.749E-01 288.28 86.94 85 8.90 5.750E+OO 8.057E-01 8.057E-01 70.39 87.57 85 37.00* 5.750E+OO l.938E-01 l.938E-01 70.39 BA-137M 661.66 26 89.90* 2.138E+OO 6.687E-02 6. 811E-02 61.97 CS-137 661.66 26 85.10* 2.138E+OO 7.064E-02 7.195E-02 61. 97 CE-144 80 .12 ------1. 36 5.243E+OO ------Line Not Found ------133. 52 47 11. 09* 6.655E+OO 3.103E-01 6.312E-01 93.36 HG-203 70.83 ------3.69 4.380E+OO ------Line Not Found ------72. 87 38 6.19 4.582E+00 6.482E-01 4.981E+Ol 108.28 279.20 30 81. 56* 4.361E+OO 4.065E-02 3.123E+OO 105.50 TL-208 277.37 30 6.60 4.36],E+OO 5.023E-01 5.023E-01 105.50 583.19 ll8 85.00* 2.366E+OO 2.859E-01 2.859E-01 25.13 860.56 17 12.50 l.737E+OO 3.ffl5E-01 3.815E-01 86.16 BI-211 72.87 38 1.23 4.582E+00 3.262E+OO 3.262E+00 108.28 351.06 223 12.92* 3.591E+OO 2.345E+OO 2.345E+OO 21. 49 PB-212 74.82 198 10.28 4.777E+OO 1. 966E+00 1. 966E+OO 27.55 77 .11 239 17.10 5.000E+OO 1.359E+OO 1.359E+OO 23.60 238.63 411 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 300.09 ------3.30 4.103E+00 ------Line Not Found ------BI-214 609.32 170 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 1120.29 29 14.92 1.404E+OO 6.828E-01 6.831E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO l.032E+00 38.16 PB-214 74.82 198 5.80 4.777E+OO 3.485E+OO 3.486E+OO 27.55 77 .11 239 9.70 5.000E+OO 2.395E+OO 2.396E+OO 23.60 87.09 85 3.41 5.750E+OO 2.103E+OO 2.104E+OO 70.39 242.00 116 7.25 4.879E+OO 1.599E+OO l.600E+00 43.01 295.22 158 18.42 4.159E+OO l.006E+00 1.007E+OO 27.17 351. 93 223 35.60* 3.591E+OO 8.509E-01 8.512E-01 21. 49 RN-222 609.32 170 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 1120.29 29 14.92 1.404E+OO 6.828E-01 6.831E-01 102.23 1764.49 31 15.30 9.426E-01 l.032E+OO 1.032E+OO 38.16 RA-224 240.99 116 4.10* 4.879E+OO 2.828E+00 2.828E+OO 43.01 RA-226 609.32 170 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 1120.29 29 14.92 1.404E+00 6.828E-01 6.831E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO 1.032E+00 38.16 AC-228 105.21 ------1.10 6.488E+00 ------Line Not Found ------338.32 81 11.27 3.713E+OO 9.407E-01 9.407E-01 45.57 794.95 ------. 4. 25 l.849E+OO ------Line Not Found ------835.71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 45 25.80* l.660E+OO 5.125E-01 5.125E-01 50.05 968. 97 51 15.80 1.581E+OO 9.879E-01 9.879E-01 45.02 RA-228 105.21 ------1.10 6.488E+00 ------Line Not Found ------338.32 81 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 Page 4254 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 ------4.25 1.849E+OO ------Line Not Found ------835. 71 ------1. 61 1.777E+OO ------Line Not Found ------911. 20 45 25.80* 1.660E+OO 5.125E-Ol 5.125E-01 50.05 968. 97 51 15.80 1.581E+OO 9.879E-01 9.879E-01 45.02 TH-228 74.82 198 10.28 4.777E+OO 1. 966E+OO 1. 966E+OO 27.55 77 .11 239 17.10 5.000E+OO l.359E+OO 1.359E+OO 23.60 238.63 411 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 300.09 ------3.30 4.103E+OO ------Line Not Found ------TH-230 609.32 170 45.49* 2.284E+OO 7.943E-01 7.943E-01 27.84 1120.29 29 14.92 1.404E+OO 6.828E-01 6.828E-01 102.23 1764.49 31 15.30 9.426E-01 l.032E+OO 1.032E+OO 38.16 TH-232 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 81 11. 27 3. 713E+OO 9.407E:-01 9.407E-01 45.57 835. 71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 45 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 968.97 51 15.80 1.581E+OO 9.879E-01 9.879E-01 45. 02* TH-234 63.29 19 3.70* 3.539E+OO 7.133E-01 7.133E-01 288.28 92.59 91 4.23 6.049E+OO l.730E+OO 1. 730E+00 60.04 U-234 609.32 170 45.49* 2.284E+OO 7.943E-01 7.943E-01 27.84 1120.29 29 14.92 1. 404E+OO 6.828E-01 6.828E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 U-238 63.29 19 3.70* 3.539E+OO 7.133E-01 7.133E-01 288.28 92.59 91 4.23 6.049E+OO 1. 730E+OO 1.730E+OO 60.04 AM-243 43.53 ------5. 9'0 6.933E-01 ------Line Not Found ------74.66 198 67.20* 4.777E+OO 3.008E-01 3.008E-01 27.55 ANH-511 511. 00* 17 100.00* 2.635E+OO 3.091E-02 3. 091E-02 186.67 Flag: "*" Key line Page 4255 of 5809
Page : 3 Summary of Nuclide Activity Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Total number of lines in spectrum 42 Number of unidentified lines 9 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 CE-144 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 10.56Y 64.84D 461. 40D 2.30E+05Y 30.08Y 30.08Y 284.91D 46.59D l.41E+l0Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600. OOY 1600.00Y 1. 41E+10Y 1600.00Y 1. 41E+l0Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 05 22.6 1. 55 1. 00 1. 02 1. 02 2.03 76. 8 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.089E+Ol 8.956E+OO 4.049E-02. l.938E+OO l.938E-01 6.687E-02 7.064E-02 3.103E-01 4.065E-02 2.859E-01 2.345E+00 9.310E-01 7.943E-01 8.509E-01 7.943E-01 . 2.828E+OO 7.943E-01 5.125E-01 5.125E-01 9.310E-01 7.943E-01 5.125E-01 7.133E-01 7.943E-01 7.133E-01 3.008E-01 3.091E-02 3.795E+Ol 3.795E+Ol Decay Corr pCi/GRAM 1. 089E+Ol 9.438E+OO 9.167E-01 3.004E+OO l.938E-01 6. 811E-02* 7.195E-02 6.312E-01 3.123E+OO 2.859E-01 2.345E+OO 9.310E-01 7.946E-01 8.512E-01 7.946E-01 2.828E+OO 7.946E-01 5.125E-01 5.125E-01 9.310E-01 7.943E-01 5.125E-01 7.133E-01 7.943E-01 7 .133E-01 3.008E-01 3. 091E-02 4.378E+Ol 4.378E+Ol 78.57% Decay Corr 2-Sigma Error 0.142E+Ol 11. 85E+OO 11. 51E-01 2 .115E+OO 1.364E-01 4.221E-02 4.459E-02 5.892E-01 3.295E+OO 0.718E-01 0.504E+OO l.205E-01 2.212E-01 1.829E-01 2.212E-01 1.216E+OO 2.212E-01 2.565E-01 2.565E-01 l.205E-01 2.212E-01 2.565E-01 20.56E-01 2.212E-01 20.56E-01 0.829E-01 5. 771E-02 "M" Manually accepted 2-Sigma %Error 13.08 125.53 125.53 70.39 70.39 61.97 61. 97 93.36 105.50 25.13 21. 49 12.94 27.84 21. 49 27.84 43.01 27.84 50.05 50.05 12.94 27.84 50.05 288.28 27.84 288.28 27.55 186.67 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit . Page 4256 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235059 Acquisition date : 3-0CT-2016 07:52:25 It Energy Area* Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 148.88 20 60 0.66 298.21 296 5 4.52E-03 **** 6.50E+OO 0 179.99 21 118 0.62 360.41 359 8 4.86E-03 **** 5. 96E+OO T 0 186.25 82 129 0.79 372.93 368 10 l.90E-02 64.2 5.85E+OO T 0 209.57 58 121 1. 94 419.57 415 11 1.36E-02 85.0 5.42E+OO T 0 382.20 13 23 0.78 764.75 762 7 3.33E-03 **** 3.35E+OO 0 399.15 22 39 1. 03 798.65 794 11 5.52E-03 **** 3.23E+OO 0 452. 96 26 48 1. 83 906.24 896 16 6.46E-03 **** 2.91E+OO T 0 463.12 35 30 1. 23 926.56 921 11 8.87E-03 72.7 2.86E+OO T 2 588.34 21 19 1. 93 1176.94 1159 27 5.36E-03 98.3 2.35E+OO 0 598.02 11 32 0.50 1196. 30 1187 12 2.78E-03 **** 2.32E+OO 0 657.01 25 19 2.79 1314.27 1305 15 6.58E-03 89.5 2.15E+OO T 0 670.17 7 34 4.30 1340.57 1328 16 1.94E-03 **** 2.12E+00 0 727.18 35 29 1. 59 1454.57 1448 14 9.39E-03 76.1 1.98E+OO T 0 769.31 36 24 6.17 1538.83 1528 19 9.72E-03 74.7 1. 90E+OO 0 963. 99 14 8 0.63 1928.14 1922 9 3.79E-03 95.3 1.59E+OO T 0 1236.82 38 10 4.95 2473.72 2464 20 1.08E-02 51. 0 l.29E+00 T 0 1244.12 14 3 1. 57 2488.33 2485 8 3.89E-03 71. 4 1.29E+OO 0 1250.13 21 0 1. 06 2500.33 2494 13 5.83E-03 43.6 l.28E+OO Flags: "T" Tentatively associated Page 4257 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:54:12.33 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l *
Acquisition date 3-0CT-2016 07:52:25 Sensitivity 3.000 * *
Detector ID GAM07 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
Sample date 16-DEC-2015 12:26:00 Nuclide Library : SOLID *
Sample ID G405235059 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.5422E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
Combined Critical' Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 CE-144 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.186E-01 4.402E+OO 4.275E-01 9. 696E-01 5.842E-02 2.243E-02 2.369E-02 2.991E-01 l.492E+00 2.320E-02 3. 771E-02 4.361E-02 5.057E-02 4.361E-02 4.044E-01 4.361E-02 8 .121E-02 8 .121E-02 3. 771E-02 4.359E-02 8.121E-02 8.916E-01 4.359E-02 8.916E-01 3.284E-02 l.803E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 4258 of 5809 Le (pCi/GRAM 1.042E+Ol 3 .112E-02 O.OOOE+OO 2.142E-02 2.362E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 co-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 *TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4259 of 5809 O.OOOE+OO O.OOOE+OO 4.782E-02 3.144E-01 O.OOOE+OO 3.849E-02 3.199E-01 3.884E+OO 2.004E-02 1.131E-01 2.075E+OO 5.889E+OO O.OOOE+OO l.423E-01 O.OOOE+OO O.OOOE+OO 5.036E-01 O.OOOE+OO l.457E-01 4.452E+02 2.589E-02 6.063E-01 l.645E+OO 1. 288E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 2.700E-02 5.298E-02 3.219E+OO 4.190E-01 4.190E-01 1.923E-02 6.717E-02 1.616E-01 O.OOOE+OO O.OOOE+OO 9.524E-02 l.568E+OO 8.122E-02 1.888E+02 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 4 . .S91E-02 l.034E-01 O.OOOE+OO O.OOOE+OO 8.951E-02 O.OOOE+OO O.OOOE+OO 1.548E+Ol O.OOOE+OO 4.621E-02 3.982E+OO 3.252E-02 0. OOOE*+oo 6.623E+02 O.OOOE+OO 2. 081E-02 8. 213E-02 1.312E-01 7.561E-02 8.512E-02 1. llOE+OO 4.603E-02 l.548E+Ol l.666E-01 5. 911E-02 2.004E-02 3.427E+00 7.658E-01 SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF . SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF
NOT I DENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL. ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4260 of 5809 2.087E+OO 2.170E+Ol 7.866E+Ol 3.560E-01 4.564E-02 2.392E+OO 3.684E-01 5.221E-01 5.804E-01 2. 722E-01 4.330E-01 1. 661E-01 1.661E-01 3.525E-Ol 3.093E-01 4.330E-01 5.192E-02 2.339E-01 3.101E+OO l.385E-01 5.192E-02 O.OOOE+OO l.880E-01 2.599E+02 9. 611E-02 7.444E-02 5.193E-02 2.403E-02 2.989E-02 9.357E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN . NOT I DENT. FAIL ABUN , NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:54:19.23 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l * *Acquisition date 3-0CT-2016 07:52:25 Sensitivity : 3.000 * *
Detector ID GAM07 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
Sample date 16-DEC-2015 12:26:00 Nuclide Library : SOLID *
Sample ID G405235059 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.5422E+02 GRAM *
Quantity Err(%) : 1.2968E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.089E+Ol 1.508E+OO KR-85 9.438E+OO 1.162E+Ol SR-85 9.167E-01 1.128E+OO CD-109 l.566E+00 2 .119E+OO SN-126 1.0lOE-01 1. 366E-01 BA-137M 6. 811E-02 4.147E-02 CS-137 7.195E-02 4.381E-02 CE-144 6.312E-01 5.785E-01 HG-203 1.318E+OO 3.264E+OO TL-208 2.859E-01 7.143E-02 PB-212 9.310E-01 l.280E-01 BI-214 7.946E-01 2.195E-01 PB-214 8.512E-01 1.827E-01 RN-222 7.946E-01 2.195E-01 RA-224 1.048E+OO 1.289E+OO RA-226 7.946E-01 2.195E-01 AC-228 5.125E-01 2.528E-01 RA-228 5.125E-01 2.528E-01 TH-228 9.310E-01 l.280E-01 TH-230 7.943E-01 2.194E-01 TH-232 5.125E-01 2.528E-01 TH-234 7.133E-01 2.021E+OO U-234 7.943E-01 2.194E-01 U-238 7.133E-01 2.021E+OO AM-243 2.139E-01 8.617E-02 ANH-511 3.091E-02 5.657E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4261 of 5809 Key-Line Activity (pCi/GRAM ) 7.517E+OO -l.128E-02 1.000E+41 1.592E-02 K.L Act error (1. 96-sigma) 1.102E+Ol 3.941E-02 1.107E+41 1.804E-02 TPU ( 1. 96-sigma) 1.508E+OO 1.162E+Ol 1.128E+OO 2 .119E+OO 1.366E-01 4.147E-02 4.381E-02 5.785E-01 3.264E+OO 7.143E-02 1. 280E-01 2.195E-01 1.827E-01 2.195E-01 1. 289E+OO 2.195E-01 2.528E-01 2.528E-01 1. 280E-01 2.194E-01 2.528E,-01 2. 021E+OO 2.194E-01 2.021E+OO 8.617E-02. 5.657E-02 TPU (1. 96-sigma) 1.153E+Ol 3.974E-02 O.OOOE+OO 1.941E-02 NOT IDENT. *NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 4.706E-02 2.583E-01 2.592E-01 FAIL ABUN V-48 -3. 711E+02 8.489E+0'3 8.491E+03 SHORT HLIF CR-51 1.104E+02 3.035E+02 3.075E+02 SHORT HLIF MN-54 1. 713E-02 5.109E-02 5.167E-02 NOT IDENT. C0-56 1.229E-01 3.323E-01 3.369E-01 FAIL ABUN MN-56 1.000E+41 2.704E+41 O.OOOE+OO SHORT HLIF C0-57 9.700E-04 4.375E-02 4.376E-02 NOT IDENT. C0-58 -4.837E-01 5.012E-01 5.465E-01 NOT IDENT. FE-59 -1.555E-Ol 4.542E+OO 4.543E+OO NOT IDENT. C0-60 -3.350E-02 3.388E-02 3.709E-02 NOT IDENT. ZN-65 -9.375E-02 1. 762E-01 l.812E-01 NOT IDENT. GE-68 1. 54 7E-01 2.376E+OO 2.377E+OO NOT IDENT. AS-73 1.536E+OO 6.242E+OO 6.281E+OO NOT IDENT. AS-74 -5. 451E+02 5.219E+03 5.225E+03 SHORT HLIF SE-75 3.439E-02 1.517E-01 1.525E-01 FAIL ABUN BR-77 1.615E+37 1.361E+38 O.OOOE+OO SHORT HLIF SR-82 -2.799E+02 5. 715E+02 5.852E+02 SHORT HLIF RB-83 6.140E-02 5.736E-01 5.742E-01 NOT IDENIT'. RB-86 5.340E+03 2.103E+04 2. ll 7E+04 SHORT HLIF Y-88 1. OllE-02 l.654E-01 l.655E-01 NOT IDENT. Y-91 1.307E+02 4.997E+02 5.032E+02 NOT IDENT. NB-94 3.563E-03 3.026E-02 3.030E-02 NOT IDENT. NB-95 1. 723E-01 6.970E-01 7. 013E-01 NOT IDENT. NB-95M -6.126E-01 2.043E+00 2.062E+OO NOT IDENT. ZR-95 l.402E+OO 1. 312E+OO l.457E+00 NOT IDENT. NB-97 1.000E+41 8.783E+40 O.OOOE+OO SHORT HLIF ZR-97 ' 1.000E+41 3.836E+42 O.OOOE+OO SHORT HLIF M0-99 -1 . 9 8 4'E + 2 9 1.858E+31 O.OOOE+OO SHORT' HLIF TC-99M -l.OOOE+41 6.515E+41 .O.OOOE+OO SHORT HLIF RH-101 -2.778E-03 3.109E-02 3 .112E-02 NOT IDENT. RH-102 1.395E-02 6.031E-02 6.064E-02 NOT IDENT. RU-103 -7.381E-01 3.839E+OO 3.854E+OO FAIL ABUN RH-106 2.025E-01 4.603E-01 4.693E-01 NOT IDENT. RU-106 2.025E-01 4.603E-01 4.693E-01 NOT IDENT. AG-108M -1.490E-03 2.210E-02 2.211E-02 NOT IDENT. AG-llOM -2. 896E-02 8.183E-02 8.286E-02 FAIL ABUN SN-113 1. 070E-01 1.674E-01 1. 742E-01 NOT IDENT. CD-115 -7.974E+37 2.581E+38 O.OOOE+bO SHORT HLIF SN-117M -2.712E+04 5.864E+04 5.990E+04 SHORT HLIF TE-123M -l.493E-02 l.121E-01 1.123E-01 NOT IDENT. SB-124 5.087E-01 1.730E+00 1.745E+OO NOT IDENT. SB-125 -8.908E-04 . 9.241E-02 9.241E-02 FAIL ABUN TE-125M -2.700E+Ol 2.166E+02 2.170E+02 NOT IDENT. I-126 9.486E+04 5.753E+05 5.769E+05 SHORT HLIF SB-126 -6.315E+05 7.085E+05 7.636E+05 SHORT HLIF SB-127 -1.457E+21 4.846E+21 O.OOOE+OO SHORT HLIF I-131 6.764E+08 2. 211E+09 2.232E+09 SHORT HLIF I-132 -l.OOOE+41 l.919E+42 O.OOOE+OO SHORT HLIF TE-132 -4.833E+25 6.293E+25 O.OOOE+OO SHORT HLIF BA-133 2.962E-02 3.617E-02 3.856E-02 NOT IDENT. I-133 1.000E+41 2.480E+41 O.OOOE+OO SHORT HLIF CS-134 4.534E-02 4.757E-02 5.178E-02 NOT IDENT. CS-135 -7.331E-02 1.202E-01 1.246E-01 NOT IDENT. I-135 1.000E+41 8.580E+41 O.OOOE+OO SHORT HLIF CS-136 -l.130E+05 2.055E+05 2 .117E+05 $HORT HLIF CE-139 4.492E-02 l.005E-01 l.025E-01 NOT IDENT. BA-140 -6. 681E+04 7.700E+05 7.706E+05 SHORT HLIF LA-140 9.152E+04 1. 969E+05 2.012E+05 SHORT HLIF CE-141 -7.395E+OO 2.024E+Ol 2.051E+Ol NOT IDENT. CE-143 1.000E+41 1.588E+41 O.OOOE+OO SHORT HLIF PM-144 -7.689E-03 5.624E-02 5.635E-02 NOT IDENT. PR-144 -7.228E-01 4.857E+00 4.868E+OO NOT IDENT. PM-146 7.277E-02 9.570E-02 FAIL ABUN ND-147 4.171E+06 l.914E+07 1.924E+07 SHORT HLIF PM-147 -l.964E+02 7.712E+02 7.763E+02 NOT IDENT. PM-149 -6.735E+38 3.389E+39 O.OOOE+OO SHORT HLIF EU-150 1'.155E-02 2.409E-02 2.464E-02 FAIL ABUN EU-152 7.353E-02 8.395E-02 9.025E-02 FAIL ABUN GD-153 -2.923E-02 1.502E-01 1.508E-01 NOT IDENT. EU-154 -3.012E-02 *9.646E-02 9.741E-02 NOT IDENT. EU-155 l.494E-02 9.464E-02 9.488E-02 FAIL ABUN TB-160 l.505E-01 1.227E+OO l.229E+OO FAIL ABUN H0-166M 2.305E-02 5.075E-02 5.180E-02 NOT IDENT. TM-171 1.14 7E+01 l.581E+Ol 1.663E+Ol NOT IDENT. HF-172 -4.844E-02 1.950E-01 l.962E-01 FAIL ABUN LU-172 3.773E-02 6.089E-02 6.322E-02 FAIL ABUN LU-176 1. 2 60E-02 2.083E-02 2.159E-02 FAIL ABUN HF-181 7.512E-01 3.841E+OO 3.856E+OO FAIL ABUN Page 4262 of 5809 "TA-182 5.890E-01 7.917E-01 8.350E-01 FAIL ABUN RE-183 1.356E+OO 2.169E+OO 2.253E+OO NOT IDENT. RE-184 1.928E+Ol 2.179E+Ol 2.346E+Ol NOT IDENT. W-188 2.429E+Ol 9.275E+Ol 9.340E+Ol FAIL ABUN IR-192 -4.843E-02. 4.043E-01 4.049E-01 FAIL ABUN BI-207 4.790E-02 4.471E-02 4. 965E-02 FAIL ABUN PB-210 1. llOE+OO 2.485E+OO 2.535E+OO NOT IDENT. BI-211 2.345E+OO 5.048E-01 l .171E+OO FAIL ABUN PB-211 -l.553E-01 6.408E-01 6.446E-01 NOT IDENT. BI-212 1.300E+OO 9.717E-01 l.135E+OO FAIL ABUN RN-219 -1. 461E-01 3.697E-01 3.755E-01 NOT IDENT. RA-223 -4.198E-01 5. 272E-01 5.602E-01 FAIL ABUN AC-227 9.510E-03 1.800E-01 l.800E-01 NOT IDENT. TH-227 9.510E-03 1.800E-01 1. 800E-01 NOT IDENT. TH-229 -3.598E-01 4.536E-01 4.817E-01 FAIL ABUN PA-231 4.705E-02 3.485E-01 3.492E-01 NOT IDENT. TH-231 -4.198E-01 5. 272E-01 5.602E-01 FAIL ABUN PA-233 l.272E-02 5.619E-02 5.649E-02 NOT IDENT. PA-234 l.094E-01 2.782E-01 2.826E-01 NOT IDENT. PA-234M -2.999E+OO 3.999E+OO 4.221E+OO NOT IDENT. U-235 -4.179E-02 1.642E-01 l.653E-01 FAIL ABUN NP-237 1. 272E-02 5.619E-02 5. 649E-02" NOT IDENT. NP-238 -1.519E+40 2.882E+40 0.000E+OO *SHORT HLIF NP-239 3.381E-03 2 .131E-01 2.131E-01 FAIL ABUN PU-239 -2.255E+Ol 2.991E+02 2.993E+02 NOT IDENT. AM-241 -4.930E-02 1.178E-01 l.199E-01 NOT IDENT. CM-243 -1. 268E-02 8.495E-02 8.514E-02 FAIL ABUN BK-247 1.355E-02 5.532E-02 5. 566.E-02 NOT IDENT. CM-247 -2.023E-02 3.413E-02 3.533E-02 FAIL ABUN CF-249 -2.376E-04 3.370E-02 3.370E-02 NOT IbENT. CF-251 5.777E-02 l.122E-01 l.152E-01 NOT IDENT. Page 4263 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 61. 8428 87.09 102. 9616 136.47 51. 4932 45.60 57.4230 87.57 103.0528 140.51 0.0000 46.54 57.5739 88.03 119.2779 143.76 68.8229 49.72 0.0000 88.34 119. 3454 144.24 61. 97 94 51. 35 64.1545 88.47 101.1167 145.44 7.3. 5732 51. 87 58.4010 89. 96 88.7174 152.43 67.2784 52.39 58.4795 1093.63 88.8264 153.25 0.0000 52.97 60.5187 91.11 0.0000 323.87 74.4053 53.44 64.5002 92.59 96.5653 156.02 0.0000 54.07 67.5397 93.35 96. 6951 158.56 0.0000 57.36 0.0000 94.56 86.6078 159.00 61.9848 57.53 65.1581 94.65 86.6214 162.33 65.7600 57.98 65.2286 94.67 86.6245 162.66 0.0000 59.27 87.2403 94.87 86.6550 163.33 59.9610 59.32 87.2507 97.43 64.2096 165.86 61.3231 59.54 80.6830 98.43 81.4719 176.31 65.6583 60. 96 72 .. 9904 98.44 81.4731 176.60 0.0000 61.17 67.7149 99.53 64.4398 177.52 52.5991 62.93 86.9879 100 .11 64.5030 181.07 0.0000 63.29 87.0594 102.03 64.7113 181. 52 52.8375 63.58 87.1170 103.18 68.0762 184.41 67.4647 64.28 82.9090 103.37 68.0978 143.76 49.8673 66.73 95.4640 105.21 68.3035 193.51 73.0042 67.24 85.8119 105.31 68.3146 197.03 54.9584 125.81 88.9265 106.12 48.8607 198.01 79.4667 67.75 88.9399 106.47 49.9745 201.83 73.6478 69.67 90.6631 109.28 64.3877 203.43 62.7049 70.83 81.3916 111. 00 72. 2227 205.31 54.2031 72. 81 72. 5357 111. 76 0.0000 210.85 52.0322 72. 87 72.5449 114. 06 73.6677 215.65 54.7717 74.66 72.8130 116. 30 0.0000 222 .11 41.7577 74.82 72.8369 116.74 66.2425 227.09 46.1545 74.97 72.8596 119. 7 6 68.7633 227.38 52.0432 77 .11 73.1754 121.12 73.3477 228.16 0.0000 78.74 85.4764 121. 22 76.6932 228.18 62.1635 79.69 78.7304 121. 78 81. 2066 116.74 62.1635 80.12 78.7965 122.06 73.4499 235.69 58.3753 80.19 0.0000 122.92 61.2859 235. 96 52.0430 80.57 65.0300 123.07 61.2993 238.63 45.8097 81. 00 73.3926 265.00 58.0073 238.98 0.0000 81. 07 74.7878 125.81 64.9013 240.99 45.9091 81. 75 78.0064 127.23 75.1253 242.00 45.9514 83.79 79.3555 127.91 54.9962 244.70 46.0646 84.00 84.9584 129.30 83.2195 252.40 0.0000 85.43 86.5839 131. 20 66.1531 252.80 48.9774 86.55 102.8584 133.02 88.9309 254.15 0.0000 86.79 102.9040 133.52 79.9432 256.23 37.0599 86. 94 102.9332 136. 00 57.5141 260.90 0.0000 Page 4264 of 5809

( ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31.2539 355.39 0.0000 584.27 15.8899 264.80 29.5217 356.01 20.9486 595.83 0.0000 265.00 31.2634 364.49 0.0000 427.87 22.4159 268.22 49.6361 366.42 0.0000 602.52 0.0000 269.46 37.4841 372.51 31.0698 604. 72 17.6461 270.03 37.5025 375.05 26.4067 607.14 14.9889 271. 23 37.5401 377.52 27.3946 609.32 15.0043 273.65 0.0000 356.01 32.7256 610.33 15. 0111 276.40 27.6195 388.16 30.4388 614.28 8.0560 277.37 34.2226 388.63 0.0000 618.01 21. 5194 277.60 33.3521 391.69 17.1606 620.36 21.5422 278.00 33.3629 264.66 24.4500 621.93 16.1682 279.20 33. 3961 401. 81 30.2247 630.19 0.0000 279.54 33.4054 402.40 31.6760 631.29 20.5656 279.70 33.4093 404.85 32.3012 633.25 22.7500 280.46 46.1864 410.95 33.7752 634.78 0.0000 283.69 38.1059 413.71 28.9996 635.95 24.9466 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.6318 423. 72. 0.0000 645.85 10.8936 285.90 0.0000 427.09 29.2358 657.76 22.9952 287.50 40. 7011 427.87 26.3249 657.90 0.0000 290.67 33.2642 433.94 20.5493 661. 66 13.1621 293.27 0.0000 439.40 25.5239 664.57 0.0000 351. 93 39.1714 453.88 21. 7793 666.33 0.0000 295.96 39.1947 463.37 21.8971 666.50 0.0000 879.38 33.4732 468.07 13.4725 667.71 0.0000 299.98 25.4675 473.00 0.0000 677.62 14.3558 300.09 25.4698 475.06 22.0407 685.70 0.0000 300 .13 25.4709 476.78 28.0786 695.00 0.0000 301.36 29.5209 477.60 23.0749 696. 49 23.3729 302.85 42.0937 482.18 27.1566 696. 51 23.3729 256.23 33.1797 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.2673 306.78 30.5434 497.08 17.2369 697.49 23.3823 308.46 38.6774 505.52 22.9161 702.65 18. 9687 311. 90 40.5835 507.63 0.0000 706.68 16.7645 316.51 38.9145 511. 00 16.3428 711. 68 13.4390 319.41 0.0000 514.00 16.3685 720.70 0.0000 320.08 0.0000 514.00 16.3685 .721.93 0.0000 321. 04 28.1499 520.40 21.5554 722.78 15.1864 323.87 44.5887 520.69 0.0000 722.91 11.8125 325.23 50.0978 522.65 0.0000 723. 31 11. 8142 328.76 0.0000 527.90 0.0000 724.19 3.3767 333.37 20.8916 528.26 22.6732 727. 33 15.7773 333.97 30.2513 529 .-59 18.5632 733 .. 00 11. 8599 334.37 33. 0110 529.87 0.0000 735.93 9.0465 338.28 28.5056 531.02 0.0000 333.97 10.1836 338.32 28.5069 537.26 0.0000 739.50 0.0000 311.90 24.8665 546.56 0.0000 747.24 7.9508 340.48 24.8665 552.55 20.8643 748.06 14.7705 340.55 0.0000 563.25 15.7306 752.31 14.7948 344.28 27.7039 569.33 29.4504 753.82 0.0000 345.93 27.7362 946.00 29.4526 756.73 11. 4001 . 351.06 29.6921 569.70 28.4030 756.80 11. 4006 351.93 29. 7096 583.19 15.8813 884.68 17.1478 Page 4265 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 14. 8720 1274.44 12.9998 1620.50 5.4312 766.42 14.8757 1001.03 16.7388 1621. 92 2.1731 766.84 14.8778 1002.74 15.8171 1678.03 0.0000 772. 60 0.0000 1004.73 12.1030 1690.97 3.3058 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.2360 778.90 16.0958 1028.54 0.0000 1063.66 3.3576 783.70 0.0000 1037.84 9.4037 1771.35 1.1194 785.37 19.5926 1038.76 0.0000 1791.20 0.0000 792.07 24.2633 631.29 16.0288 1808.65 0.0000 794.95 15.0360 1048.07 0.0000 1810.72 0.0000 795.86 11. 5702 1049.04 14.1531 1836.06 2.7199 810.06 17.4463 1050.41 11.3269 810.29 17.4475 1063.66 7. 5811 344.28 18.6120 1077.00 0.0000 810.76 18.6139 1077.34 15.2227 815.77 0.0000 *1085.87 13.3523 1048.07 0.0000 1093.63 6. 6911 832.01 16.7056 1099.45 8.6177 834.85 11. 4417 1112. 07 6.5893 835.71 10.5648 1112.84 9.2268 836.80 0.0000 1115 .. 54 15.3896 846.75 0.0000 1120.29 10.5945 846.77 8.8388 1120.55 10.5958 856.80 0.0000 1221.41 10.5978 860.56 9.9473 1129. 67 6.7599 871.09 15.1536 1131.51 0.0000 873.19 8.9203 1147.95 0.0000 875.33 0.0000 1173.23 17.5924 879.38 8.0456 1177.95 .15.6572 880.51 12.5200 1189.05 10.7966 883.24 5.3707 1204.77 14.7849 884.68 13.4335 1221.41 8.9099 889.28 8.0725 1231.02 6.3516 894.76 12.5807 1235.36 0.0000 898.04 8. 9963 1238.28 12.7273 900.72 14.4067 1260.41 0.0000 903.28 7.2095 1271.87 8.0234 911. 20 9.0359 1274.44 10.0360 912.08 13.0153 1274.54 10.0360 923.98 0.0000 1291.59 9.0714 926.50 9.0817 1298.22 0.0000 929 .11 9.9983 1312 .11 0.0000 937.49 21. 8745 1332.49 11.2001 944 .13 0.0000 1362.66 0.0000 946.00 10.9673 1365.19 4.1050 949.00 19.2113 1368.63 0.0000 667. 71 0.0000 1384.29 6.1857 962. 31 11. 7598 1408.01 6.2201 964. 08 22.0620 1457.56 0.0000 966 .17 22.0767 1460.82 5.2466 911.20 10.3117 1489.16 4.2241 968. 97 10.3117 1505.03 10.5975 983.53 0.0000 1584.12 9.7020 984.45 0.0000 1596.21 0.0000 Page 4266 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:54:50.50 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM18.CNF;511 Background date : Z-OCT-2016 11:01:02. Sample date 16-DEC-2015 12:33:00 Acquisition date : 3-0CT-2016 07:52:52. Sample ID G405235060 Sample quantity 1.52266E+02 GRAM Detector name : GAM18 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.97 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 4 4 0 4 4 4 0 3 3 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 52.18 63.20* 74.85 77.19* 84.19* 87.07 89.95 92. 65* 98.34 105.29 107.63 129.29 166.52 209.69 238.86* 241. 93 277.02 295.58* 328.12 337.01*

352.22* 463.23 511.13* 584.24* 609.73* 661.89 728.51 770.32 794.93* 861.65 912.24* 936.58 970.08* 1072. 48 Page 4267 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 14 11 151 196 30 93 74 92 83 55 32 30 94 74 -414 131 44 199 52 25 359 27 64 130 265 51 50 52 25 30 121 34 53 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 130 195 154 142 12.7 106 119 113 101 98 64 124 215 161 95 68 70 99 96 211 98 44 86 90 89 24 . 33 55 22 24 35 59 41 31 1.29 1.10 1.15 1.18 1.13 1. 34 1.16 1.12 2.24 1. 38 1. 04 1.11 5.83 1. 29 1. 23 1. 53 1. 73 1. 08 6.58 1. 46 1.30 1. 48 3 .11 1.10 .1. 94 2.64 0.90 4.57 2.36 1. 63 1. 79 2.90 1. 53 0.49 105.19 127.21 150.50 155.16 169.15 174.91 180.67 186.05 197.43 211.31 216.00 259.27 333.68 419.95 478.25 484.38 554.50 591.59 656.64 674.41 704.79 926.66 1022.40 1168; 51 1219.48 1323.73 1456.88 1540.47 1589.66 1723.03 1824.15 1872.80 1939.78 2144.48 101 122 146 146 166 172 172 172 193 205 205 255 324 414 473 473 550 586 648 671 698 921 1013 1160 1213 1317 1449 1527 1582 1715 1816 1862 1933 2134 7 3.75E-03142.4 9 2.97E-03243.0 13 4.21E-02 15.8 4.04E-01 13 5.45E-02 12.8 6 8.40E-03 63.6 21 2.58E-02 20.1 2.30E+OO 21 2.05E-02 27.0 21 2.56E-02 24.3 9 2.30E-02 24.8 .15 1.52E-02 35.0 1.67E+OO 15 8.93E-03 45.0 8 8.40E-03 67.0 19 2.61E-02 39.1 13 2.05E-02 37.4 16 1.15E-01 6.3 5.06E+oo 16 3.63E-02 17.1 9 1.21E-02 38.2 12 5.53E-02 12.4 16 l.45E-02 44.7 18 6.91E-03140.8 14 9.98E-02 8.0 10 7.47E-03 50.4 19 1.77E-02 41.8 19 3.62E-02 20.5 17 7.36E-02 10.5 12 1. 42E-02 23. 8 14 1.38E-02 28.9 22 1. 45E-02 38. 9 15 7.05E-03 46.7 14 8.39E-03 39.2 18 3.36E-02 15.2 26 9.49E-03 60.8 14 l.47E-02 29.9 16 l.96E-03173.7 Peak Search Report (continued) Page : 2 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1100.48. 34 28 8.92 2200.47 2187 23 9.46E-03 44.2 36 0 1121.39* 51 31 2.03 2242.26 2236 12 l.42E-02 27.2 37 0 1238.36 52 8 1. 96 2476.12 2467 17 1. 43E-02 19.0 38 0 1281. 49 26 17 8.79 2562.33 2551 22 7.34E-03 43.8 39 0 1416.11 14 7 1. 58 2831. 50 2825 14 3.89E-03 48.2 40 0 1461.62* 538 0 2.88 2922.49 2912 20 1.49E-01 4.4 41 0 1624.62 8 7 1. 34 3248.40 3240 13 2.08E-03 79.0 42 0 1766.95* 25 21 1. 91 3533.01 3522 16 7.02E-03 46.2 Flag: "*" = Peak area was modified by background subtraction Page 4268 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:54:52 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 16-DEC-2015 12:33:00 G405235060 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:52:52 152.27 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA18 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4269 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47. RA-224 240.99 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.97 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 911E+OO 1.258E+Ol l.258E+Ol 8.70 OK AS-73 53.44 10.30* l.379E+OO 6.226E-01 7.731E+OO 284.82 OK CD-109 88.03 3.70* 6 .119E+OO 1.619E+OO 2. 510E+o*o 65.60 OK SN-126 64.28 9.60 3.086E+OO 2.325E-01 2.325E-01 486.00 OK 86.94 8.90 6.119E+OO 6.732E-01 6.732E-01 65.60 OK 87.57 37.00* 6 .119E+OO l.619E-01 l.619E-01 65.60 OK BA-137M 661. 66 89.90* 3. 371E+OO 8.731E-02 8.893E-02 47.55 OK CS-137 661. 66 85.10* 3.371E+OO 9.223E-02 9.395E-02 47.55 OK CE-139 165.86 80.00* 7.900E+OO 8.805E-02 3.828E-01 78.21 OK EU-155 86.55 30.70 6 .119E+OO l.952E-01 2.193E-01 65.60 OK 105.31 21.10* 7.389E+OO 2.170E-01 2.439E-01 70.02 OK TM-171 51. 35 0.27 1.379E+OO 2.375E+Ol 3.169E+Ol 284.82 OK 52.39 0.47* '1.379E+OO l.364E+Ol 1.821E+Ol 284.82 OK 66.73 0.14 3.622E+OO Line Not Found Absent TL-208 277.37 6.60 6.132E+OO 6.083E-01 6.083E-01 76.34 OK 583.19 85.00* 3.673E+OO '2.195E-01 2.195E-01 41.05 OK 860.56 12.50 2.812E+OO 4.335E-01 4.335E-01 78.30 OK BI-211 72. 87 1. 23 4.495E+00 Line Not Found Absent 351. 06 12.92* 5.219E+OO 9.795E-02 9.795E-02 868.18 OK PB-212 74.82 10.28 4.756E+OO 1.387E+OO l.387E+00 46.14 OK 77 .11 17.10 5.050E+OO 1.440E+OO l.440E+OO 25.57 OK 238.63 43.60* 6.719E+OO 8.109E-01 8.109E-01 12. 67 OK 300.09 3.30 5.819E+OO Line Not Found Absent BI-214 609.32 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 OK 1120. 29 14.92 . 2. 335E+OO 7.203E-01 7.205E-01 54.33 OK 1764.49 15.30 l.634E+00 Line Not Found Absent PB-214 74.82 5.80 4.752E+OO Line Not Found <<INT Reject 77 .11 9.70 5.050E+OO 2.539E+OO 2.540E+OO 25.57 OK 87.09 3.41 6 .121E+OO Line Not Found <<INT. Reject 242.00 7.25 6.668E+OO Line Not Found <<INT Reject 295.22 18.42 5.877E+OO l.033E+OO 1.033E+OO 24.89 OK 351. 93 35.60* 5.221E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent RA-224 240.99 4.10* 6.669E+OO 9.142E-01 9.142E-01 113. 85 OK RA-226 609.32 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent AC-228 105.21 1.10 7.389E+00 4.163E+OO 4.163E+OO 70.02 OK 338.32 11. 27 5.379E+00 2.278E-01 2.278E-01 281. 64 OK 794.95 4.25 2.973E+00 1.022E+OO 1.022E+OO 93.48 OK 835.71 1. 61 2. 872E+OO Line Not Found Absent 911.20 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 OK 968.97 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 OK RA-228 105.21 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 OK 338.32 11. 27 5.379E+OO 2.278E-01 2.278E-01 281. 64 OK 794.95 4.25 2.973E+OO 1.022E+OO l.022E+00 93.48 OK 835.71 1. 61 2.872E+00 Line Not Found Absent Page 4270 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 OK 968. 97 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 OK TH-228 74.82 10.28 4.756E+OO 1.387E+OO l.387E+OO 46.14 OK 77 .11 17.10 5.050E+OO 1.440E+OO 1.440E+OO 25.57 OK 238.63 43.60* 6.719E+OO 8.109E-01 8.109E-01 12. 67 OK 300.09 3.30 5.819E+OO Line Not Found Absent TH-229 85.43 14.70 5.837E+OO 2.220E-01 2.220E-01 127.28 OK 88.47 24.00 6 .119E+OO 2. 496E-01 2.497E-01 65.60 OK 193.51 4.41* 7.490E+OO Line Not Found Absent 210.85. 2.80 7.213E+OO 2.121E+OO 2 .121E+OO 74.87 OK TH-230 609.32 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 OK 1120.29 14.92 2.335E+00 7.203E-01 7.203E-01 54.33 OK 1764.49 15.30 l .'634E+OO Line Not Found Absent TH-232 105.21 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 OK 338.32 11. 27 5.379E+OO 2.278E-01 2.278E-01 281.64 OK 835. 71 1. 61 2. 872E+OO -----Line Not Found Absent *911.20 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 *OK 968. 97 15.80 2.589E+OO 6.436E-01 6.436E-01 59. 83 OK TH-234 63.29 3 .'70* 3.086E+OO 6.033E-01 6.033E-01 486. o*o OK 92.59 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 OK U-234 609.32 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.203E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent U-238 63.29 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 OK 92.59 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 OK AM-243 43.53 5.90 3.443E-01 Line Not Found Absent 74.66 67.20* 4.756E+OO 2.122E-01 2.122E-01 46.14 OK ANH-511 511. 00 100.00* 4.028E+OO 8.422E-02 8.422E-02 83.59 OK Flag: "*" = Keyline Page 4271of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:54:53.45 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *************.****************************************************************** * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l *
Acquisition date 3-0CT-2016 07:52:52 Sensitivity : 3.000 *
Detector ID GAM18 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
Sample date 16-DEC-2015 12:33:00 Analyst initials: MXRl *
Sample ID G405235060 Sample Quantity l.5227E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma} (pCi/GRAM K-40 1.258E+Ol l.073E+00 4.220E-01 AS-73 7.731E+OO 2.158E+Ol 1. 736E+Ol CD-109 2.510E+OO 1.614E+OO l.485E+OO
SN-126 l.619E-01 1. 041E-01 9.638E-02 BA-137M 8.893E-02 4.144E-02 4.779E-02 CS-137 9.395E-02 4:377E-02 5.049E-02 CE-139 3.828E-01 2.934E-01 l.495E-01 EU-155 2.439E-01 l.674E-01 l.640E-01 TM-171 1.821E+Ol 5.082E+Ol 4.304E+Ol TL-208 2.195E-01 8.832E-02 4.724E-02 BI-211 9.795E-02 8.334E-01 2.654E-01 PB-212 8.109E-01 1.007E-01 7.359E-02 BI-214 8.548E-01 1. 760E-01 1.083E-01 PB-214 1. 069E+00 l.672E-01 2.692E-01 RN-222 8.548E-01 l.760E-01 l.083E-01 RA-224 9.142E-01 1.020E+OO 7.882E-01 RA-226 8.548E-01 l.760E-01 1.083E-01 AC-228 8.687E-01 2.591E-01 1.617E-01 RA-228 8.687E-01 2 .. 591E-01 l.617E-01 TH-228 8.109E-01 l.007E-01 7.359E-02 TH-229 -3.947E-02 3.454E-'01 6.788E-01 TH-230 8.545E-01 1.759E-01 1.082E-01 TH-232 8.687E-01 2.591E-01 1.617E-01 TH-234 6.033E-01 2.874E+OO 2.136E+OO U-234 8.545E-01 1.759E-01 1.082E-01 U-238 6.033E-01 2.874E+OO 2.136E+OO AM-243 2.122E-01 9.595E-02 7.523E-02 ANH-511 8.422E-02 6.899E-02 3.998E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma} (pCi/GRAM BE-7 -5.557E+OO 8.733E+OO 1.478E+Ol NOT IDENT. NA-22 2.268E-02 4.171E-02 7.560E-02 NOT I.DENT. Page 4272 of 5809 NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 -2.989E-04 1.908E-02 4.029E-02 NOT IDENT. SC-46 -7.038E-02 2.922E-01 5.247E-01 FAIL ABUN V-48 O.OOOE+OO 8.240E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.845E+02 O.OOOE+OO SHORT HLIF MN-54 l.610E-02 5.573E-02 l.060E-01 NOT IDENT. C0-56 3.776E-01 3.590E-01 7.502E-01 FAIL ABUN MN-56 0.000E+OO 9.528E+40 O.OOOE+OO SHORT HLIF C0-57 4.337E-03 3.855E-02 7.303E-02 NOT IDENT. C0-58 7.600E-02 4.554E-01 8.663E-01 NOT IDENT. FE-59 O.OOOE+OO l.023E+Ol 9.408E+OO FAIL ABUN C0-60 l.634E-02 2.645E-02 5.680E-02 NOT IDENT. ZN-65 4.146E-02 l.594E-01 2.741E-01 NOT IDENT. GE-68 -4.203E-01 1.888E+OO 3.046E+OO NOT IDENT. AS-74 O.OOOE+OO 3.459E+03 O.OOOE+OO SHORT HLIF SE-75 -4.605E-02 1. 588E-01 2.988E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 745E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.995E+02 O.OOOE+OO SHORT HLIF RB-83 2.200E-01 4.577E-01 9.376E-01 NOT IDENT. KR-85 1.238E+Ol 6.724E+OO 1.359E+Ol NOT IDENT. SR-85 1.198E+OO 6.527E-01 1.318E+OO NOT IDENT. RB-86 O.OOOE+OO l.777E+04 O.OOOE+OO SHORT HLIF Y-88 -4.490E-03 l.644E-01 3.309E-01 NOT IDENT. Y-91 -5.238E+Ol 3.562E+02 6.648E+02 NOT IDENT. NB-94 -2.393E-04 2.378E-02 4.447E-02 NOT IDENT. NB-95 1.615E-01 5.690E-01 1.109E+OO NOT IDENT. NB-95M . 9. 593E-01 1.887E+OO 3.429E+OO NOT IDENT. ZR-95 8.370E-01 l.007E+00 2.092E+OO NOT IDENT; NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 051E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.892E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 3.778E-03 2.789E-02 4.893E-02 NOT IDENT. RH-102 -3.628E-02 4.095E-02 7.046E-02 NOT IDENT. RU-103 -1.015E+OO 4.028E+OO 7.599E+OO FAIL ABUN RH-106 -3.191E-01 3.943E-01 6.886E-01 NOT IDENT. RU-106 -3 .191E-01 3.943E-01 6.886E-01 NOT IDENT. AG-108M -2.547E-05 2.128E-02 3.946E-02 NOT IDENT. AG-110M 3.550E-02 7.729E-02 l.529E-01 FAIL ABUN SN-113 -2.955E-05 l.553E-01 2. 921E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 989E+38 0.000E+OO SHORT HLIF SN-117M O.OOOE+OO 5.101E+04 O.OOOE+OO SHORT HLIF TE-123M 2. 728E-02 1.006E-01 1. 880E-01 NOT IDENT. SB-124 2.685E-01 l.046E+OO 2.390E+OO NOT IDENT. SB-125 2.614E-02 8.280E-02 l.580E-01 FAIL ABUN TE-125M -l.277E+02 2.022E+02 3.333E+02 NOT IDENT. I-126 O.OOOE+OO 5.246E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.304E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.855E+21 O.OOOE+OO SHORT HLIF I-131 0. OOOE'+OO 2.065E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.094E+25 O.OOOE+OO SHORT HLIF BA-133 7.916E-03 3.483E-02 6.022E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 6.643E-02 6.086E-02 8.178E-02 FAIL ABUN CS-135 2.868E-02 l.188E-01 2.308E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 1.433E+05 O.OOOE+OO SHORT HLIF BA-140 O.OOOE+oo* 6.668E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.154E+05 O.OOOE+OO SHORT HLIF CE-141 -1.295E+Ol 1.806E+Ol 3.148E+Ol NOT IDENT. CE-143 O.OOOE+OO 9.214E+40 O.OOOE+OO SHORT HLIF CE-144 -2.495E-01 2.813E-01 4.850E-01 NOT IDENT. PM-144 3. 621E-02 4.308E-02 8.859E-02 NOT IDENT. PR-144 3.123E+OO 3.726E+OO 7.660E+OO NOT IDENT. PM-146 9.919E-03 3.422E-02 6.507E-02 NOT IDENT. ND-147 O.OOOE+OO 1.537E+07 O.OOOE+OO SHORT HLIF PM-147 -7.533E+Ol 6.585E+02 1.229E+03 NOT IDENT. PM-149 O.OOOE+OO 2.804E+39 0.000E+OO SHORT HLIF EU-150 5.816E-03 2.852E-02 3.932E.:.02 FAIL ABUN EU-:-152 2.385E-02 8.200E-02 l.428E-01 NOT IDENT. GD-153 O.OOOE+OO 2.857E-01 2.985E-01 FAIL ABUN EU-154 6.113E-02 1.034E-01 l.886E-01 NOT IDENT. TB-160 1. 2 67E-01 l.410E+OO 2.652E+OO FAIL ABUN H0-166M -3.137E-02 4.273E-02 7.382E-02 NOT IDENT. HF-172 -8.909E-02 1.977E-01 3.265E-01 FAIL ABUN LU-172 4.267E-02 6.744E-02 1.248E-01 FAIL ABUN LU-176 -l.803E-04 l.849E-02 3.524E-02 FAIL ABUN Page 4273 of 5809 HF-181 3.068E+OO 3.180E+OO 6.393E+OO NOT IDENT. TA-182 -2.158E-01 7.473E-01 1. 351E+OO FAIL ABUN RE-183 5.465E-01 2.527E+OO 5.193E+OO NOT IDENT. RE-184 5.823E+OO 1.670E+Ol 3.349E+Ol NOT IDENT. W-188 9.420E+OO 8.269E+Ol 1.442E+02 FAIL ABUN IR-192 -8.742E-02 3.319E-01 6.161E-01 FAIL ABUN HG-203 -2.850E-01 1.735E+OO 2.937E+OO NOT IDENT. BI-207 l.454E-02 4.325E-02 7.645E-02 FAIL ABUN PB-210 2.770E+OO 4.415E+OO 9.309E+OO NOT IDENT. PB-211 l.805E-01 5.147E-01 9.913E-01 NOT IDENT. BI-212 O.OOOE+OO 6.855E-01 9.833E-01 FAIL ABUN RN-219 -2.561E-02 2.713E-01 5.031E-01 NOT IDENT. RA-223 1.134E-02 5.329E-01 9.020E-01 FAIL ABUN AC-227 -7.758E-03 1. 889E-01 3.623E-01 NOT IDENT. TH-227 -7.758E-03 l.889E-01 3.623E-01 NOT IDENT. PA-231 2.007E-01 3.755E-01 7.107E-01 NOT IDENT. TH-231 l.134E-02 5.329E-01 9.020E-01 FAIL ABUN PA-233 -2.676E-02 4.398E-02 7.919E-02 NOT IDENT. PA-234 -1.247E-02 2.597E-01 4.351E-01 FAIL ABUN PA-234M -4.999E-01 3.162E+OO 5.920E+OO NOT IDENT. U-235 -5.600E-02 1.548E-01 2.781E-01 FAIL ABUN NP-237 -2.676E-02 4.398E-02 7.919E-02 FAIL ABUN NP-238 O.OOOE+OO 2.948E+40 O.OOOE+OO SHORT HLIF NP-239 5.043E-02 1. 882E-01 3.640E-01 FAIL ABUN PU-239 3.616E+02 4.747E+02 5 .111E+02 FAIL ABUN AM-241 -3.858E-02 1. 363E-01 2.492E-01 NOT IDENT. CM-243 5.940E-03 7.980E-02 l.536E-01 FAIL ABUN BK-247' -1.357E-02 5.673E-02 1. 073E-01 FAIL ABUN CM-247 -2.657E-02 2.618E-02 4.327E-02 FAIL ABUN CF-249 1.658E-03 2.597E-02 4.928E-02 NOT IDENT. CF-251 -4.537E-02 8.860E-02 1.528E-01 NOT IDENT. Page 4274 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:54:51.23 Nuclide Line Activity Report Nuclide Type:. Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 520 10.66* 1. 911E+OO l.258E+Ol l.258E+Ol 8.70 AS-73 53.44 18 10.30* 1.379E+OO 6.226E-01 7.731E+OO 284.82 CD-109 88.03 118 3.70* 6.119E+OO 2.571E+OO 3.986E+OO 40.27 SN-126 64.28 14 9.60 3.086E+OO 2.325E-01 2.325E-01 486.00 86. 94 118 8.90 6 .119E+OO 1. 069E+OO l.069E+OO 40.27 87.57 118 37.00* 6 .119E+OO 2. 571E-01 2. 571E-01 40.27 BA-137M 661. 66 54 89.90* 3.371E+OO 8.731E-02 8.893E-02 47.55 CS-137 661.66 54 85.10* 3.371E+OO 9.223E-02 9.395E-02 47.55 CE-139 165.86 113 80.00* 7.900E+OO 8.805E-02 3.828E-01 78.21 EU-155 86.55 118 30.70 6 .119E+OO 3.099E-01 3.482E-01 40.27 105.31 69 21.10* 7.389E+OO 2.170E-01 2.439E-01 70.02 TM-171 51. 35 18 0.27 1.379E+OO 2.375E+Ol 3.169E+Ol 284.82 52.39 18 0.47* 1. 37 9E+OO l.364E+Ol 1. 821E+Ol 284.82 66 .,73 ------0.14 3.622E+OO ------Line Not Found ------TL-208 277.37 50 6.60 6 .132E+OO 6.083E-01 6.083E-01 76. 34 583.19 139 85.'00* 3.673E+OO 2.195E-01 2.195E-01 41'.05 860.56 31 12.50 2.812E+OO 4.335E-01 4.335E-01 78.30 BI-211 72.87 ------1. 23 4.495E+00 ------Line Not Found ------351.06 403 12.92* 5.219E+OO 2.945E+OO 2.945E+OO 15. 96 PB-212 74.82 195 10.28 4.756E+OO 1.970E+OO 1.970E+OO 31. 64 77 .11 252 17.10 5.050E+OO 1.440E+OO l.440E+00 25.57 238.63 482 43.60* 6.719E+OO 8.109E-01 8.109E-01 12.67 300.09 ------3.30 5.819E+OO ------Line Not Found ------BI-214 609.32 281 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------PB-214 74.82 195 5.80 4.756E+OO 3.491E+OO 3.492E+OO 31. 64 77 .11 252 9.70 5.050E+OO 2.539E+OO 2.540E+OO 25.57 87.09 118 3.41 6 .119E+OO 2.790E+OO 2.791E+OO 40.27 242.00 152 7.25 6.669E+OO 1.550E+OO 1. 551E+OO . 34 .16 295.22 227 18.42 5.877E+OO 1.033E+OO l.033E+OO 24.89 351. 93. 403 35.60* 5.219E+OO 1.069E+OO l.069E+OO 15.96 RN-222 609.32 281 45. 49:1< 3.566E+OO 8.545E-01 8.548E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------RA-224 240.99 152 4.10* 6.669E+OO 2.741E+OO 2.741E+OO 34.16
RA-226 609.32 281 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.205E-0'1 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------AC-228 105.21 69 1.10 7.389E+OO 4.163E+00 4.163E+OO 70.02 338.32 28 11. 27 5.379E+OO 2.278E:._01 2.278E-01 281.64 794.95 26 4.25 2.973E+OO 1.022E+OO 1.022E+OO 93.48 835.71 ------1. 61 2. 872E+OO ------Line Not Found ------911.20 123 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 968. 97 53 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 RA-228 105.21 69 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 338.32 28 11.27 5.379E+OO 2.278E-01 2.278E-01 281.64 Page 4275 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 26 4.25 2.973E+OO 1.022E+OO 1.022E+OO 93.48 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 123 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 968. 97 53 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 TH-228 74. 82 195 10.28 4.756E+OO 1.970E+OO 1.970E+OO 31. 64 77 .11 252 17.10 5.050E+OO 1.440E+OO 1.440E+OO 25.57 238.63 482 43.60* 6.719E+OO 8.109E-01 8.109E-01 12.67 300.09 ------3.30 5.819E+OO ------Line Not Found ------TH-229 85.43 39 14.70 5.837E+OO 2.220E-01 2.220E-01 127.28 88.47 118 24.00 6 .119E+OO 3. 964E-01 3. 965E-01 40.27 193.51 ------4.41* 7.490E+OO ------Line Not Found ------210.85 87 2.80 7.213E+OO 2 .121E+OO 2.121E+OO 74.87 TH-230 609.32 281 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.203E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------TH-232 105.21 69 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 338.32 28 11.27 5.379E+OO 2.278E-01 2.278E-01 281. 64 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911. 20 123 25.80'* 2.703E+OO 8.687E-01 8.687E-01 30.43 968. 97 53 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 TH-234 63.29 14 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 92.59 117 4.23 6.599E+OO 2.060E+00 2.060E-t-OO 48.52 U-234 609.32 281 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 1120.29 51 14.92 2.335E+00 7.203E-01 7.203E-01 54.33 ------15.30 1.634E+OO ------Line Not Found ------U-238 63.29 14 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 92.59 117 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 AM-243 43.53 ------5.90 3.443E-01 ------Line Not Found ------74.66 195 67.20* 4.756E+00 3.013E-01 3.014E-01 31. 64 ANH-511 511.00 69 100.00* 4.028E+OO 8.422E-02 8.422E-02 83.59 Flag: "*" Key line Page 4276 of 5809 Summary of Activity Sample ID : G405235060 Acquisition date Page : 3 3-0CT-2016 07:52:52 Total number of lines in spectrum 42 Number of unidentified lines 6 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 CE-139 EU-155 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlif e 1.25E+09Y '80.30D 461. 40D 2.30E+05Y 30.08Y 30.08Y 137.64D 4.75Y l.92Y l.41E+l0Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1. 41E+10Y l.41E+l0Y 1. 41E+10Y 7340.00Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 12.4 1. 55 1. 00 1. 02 1. 02 4.35 1.12 1. 33 LOO 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.. 00 1. 00 1. 00 LOO 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.258E+Ol 6.226E-01 2.571E+OO 2. 571E-01 8.731E-02 9.223E-02 8.805E-02 2.170E-01 1.364E+Ol 2.195E-01 2.945E+OO 8.109E-01 8.545E-01 1.069E+OO 8.545E-01 2. 741E+OO 8.545E-01 8.687E-01 8.687E-01 8.109E-01 3. 964E-01 8.545E-01 8.687E-01 6.033E-01 8.545E-01 6.033E-01 3. 013E-01 8.422E-02 4.762E+Ol 4.762E+Ol Decay Corr pCi/GRAM l.258E+Ol 7.731E+OO 3.986E+OO 2.571E-01 8.893E-02 9.395E-02 3.828E-01 2.439E-01 1.821E+Ol 2.195E-01 2.945E+OO 8.109E-01 8.548E-01 l.069E+OO 8.548E-01 2.741E+OO 8.548E-01 8.687E-01 8.687E-01 8.109E-01 3. 965E-01 8.545E-01 8.687E-01 6.033E-01 8.545E-01 6.033E-01 3.014E-01 8.422E-02 6.103E+Ol 6.103E+Ol 85.71% Decay Corr 2-Sigma Error 0.109E+Ol 22.02E+OO 1.605E+OO 1.036E-01 4.228E-02 4.467E-02 2.994E-01 l.708E-01 5.186E+Ol 0.901E-01 0.470E+OO l.028E-01 1.796E-01 0.171E+OO 1. 796E-01 0.936E+OO l.796E-01 2.644E-01 2.644E-01 l.028E-01 l.597E-01 1. 795E-01 2.644E-01 29.32E-01 1. 7 95E-01 29.32E-01 0.954E-01 7.039E-02 "M" Manually accepted 2-Sigma %Error 8.70 284.82 40.27 40.27 47.55 47.55 78.21 70.02 284.82 41. 05 15. 96 12.67 21. 01 15. 96 21. 01 34.16 21. 01 30.43 30.43 12.67 40.27 21. 01 30.43 486.00 21. 01 486.00 31. 64 83.59 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4277 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235060 Acquisition date : 3-0CT-2016 07:52:52 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 89.95 94 151 1.16 180.67 172 "21 2.05E-02 54.1 6.38E+OO T 0 98.34 104 127 2.24 197.43 193 9 2.30E-02 49.6 7.00E+OO T 3 107.63 40 80 1. 04 216.00 205 15 8.93E-03 90.0 7.50E+OO T 0 129.29 37 152 1.11 259.27 255 8 8.40E-03 **** 8. 04E+OO* T 0 328.12 59 108 6.58 656.64 648 16 l.45E-02 89.4 5.48E+OO T 0 463.23 29 48 1. 48 926.66 921 10 7.47E-03 **** 4.31E+OO T 0 728.51 52 35 0.90 1456.88 1449 14 1.38E-02 57.8 3.16E+OO T O* 770.32 54 57 4.57 1540.47 1527 22 l.45E-02 77.7 3.04E+OO 0 936.58 35 60 2.90 1872.80 1862 26 9.49E-03 **** 2.65E+OO T 0 1072.48 7 31 0.49 2144.48 2134 16 1. 96E-03 **** 2.41E+OO 0 1100. 48 34 28 8.92 2200.47 2187 23 9.46E-03 88.5 2.37E+OO T 0 1238.36 51 8 1. 96 2476.12 2467 17 1. 43E-02 38.1 2.17E+OO T 0 1281. 49 26 16 8.79 2562.33 2551 22 7.34E-03 87.6 2.12E+OO 0 1416 .11 14 7 1. 58 2831.5.0 2825 14 3.89E-03 96. 4 1. 96E+OO 0 1624.62 7 6 1. 34 3248.40 3240 13 2.08E-03 **** 1. 75E+00 0 1766.95 24 20 1. 91 3533.01 3522 16 7.02E-03 92.4 l.63E+00 Flags: "T" = Tentatively associated Page 4278 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:55:05.22 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l *
Acquisition date 07:52:52 Sensitivity : 3.000 *
Detector ID GAM18 Energy tolerance:. 1. 500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
Sample date 16-DEC-2015 12:33:00 Nuclide Library : SOLID *
Sample ID G405235060 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : l.5227E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 CE-139 EU-155 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 781E-01 8.124E+OO 6.940E-01 4.505E-02 2.160E-02 2.282E-02 6.990E-02 7.686E-02 2.006E+Ol 2.143E-02 l.224E-01 3.441E-02 4.992E-02 1.309E-01 4.992E-02 3.686E-01 4.992E-02 7.114E-02 7. 114E-02 3.441E-02 3.181E-01 4.990E-02 7. 114E-02 1. 005E+OO . 4.990E-02 1. 005E+00 3.536E-02 1.828E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4279 of 5809 Le (pCi/GRAM 6.692E+00 3.389E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 . TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M *I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 HO-l66M HF-172 LU-172 LU-176 HF-181 Page 4280 of 5809 1. 596E-02 2.348E-01 O.OOOE+OO 0.000E+OO 4.847E-02 3.423E-01 O.OOOE+OO 3. 431E-02 3.927E-01 4.229E+OO 2.476E-02 1.240E-01 l.339E+OO 0.000E+OO l.392E-01 O.OOOE+OO O.OOOE+OO 4.287E-01 6.379E+OO 6.189E-01 0.000E+OO 1.370E-01 2.953E+02 2.012E-02 5.018E-01 1. 617E+OO 9.502E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.292E-02 3 .115E-02 3.481E+00 3.105E-01 3.105E-01 1.804E-02 6.883E-02 1.333E-01 0.000E+OO O.OOOE+OO 8.827E-02 9.563E-01 7.281E-02 l.548E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.784E-02 O.OOOE+OO 3.739E-02 l.085E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 1.483E+Ol O.OOOE+OO 2.264E-01 4.062E-02 3.512E+OO 2.986E-02 0.000E+OO 5.754E+02 O.OOOE+OO 1.831E-02 6.625E-02 l.410E-01 8.464E-02 1.192E+OO 3.298E-02 1.527E-Ol 5.635E-02 l.632E-02 2.956E+00 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN , NOT I DENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF *SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT*IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4281 of 5809 6.088E-01 2.429E+OO 1.476E+Ol 6.681E+Ol 2.849E-01 1.361E+OO 3.443E-02 4.381E+OO 4.571E-01 4.594E-01 2.295E-01 4.195E-01 l.698E-01 1.698E-01 3.330E-01 4.195E-01 3.641E-02 1. 961E-01 2.642E+OO 1. 311E-01 3.641E-02 O.OOOE+OO l.705E-01 2.416E+02 1.166E-01 7.201E-02 4.994E-02 l.962E-02 2.249E-02 7 .114E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN 'FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:55:10.62 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l * ** Acquisition date 3-0CT-2016 07:52:52 Sensitivity : 3.000 *
Detector ID GAM18 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
Sample date 16-DEC-2015 12:33:00 Nuclide Library : SOLID *
Sample ID G40523'5060 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity: 1.522'7E+02 GRAM' *
Quantity Err(%) : 1.3135E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 * * , Dry Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.258E+Ol l.258E+00 AS-73 7. 731E+OO 2.164E+Ol CD-109 2.510E+OO 1.637E+OO SN-126 l.619E-01 1.053E-'01 BA-137M 8.893E-02 4.161E-02 CS-137 9.395E-02 4. 396E-02 CE-139 3.828E-01 3.033E-01 EU-155 2.439E-01 1.683E-01 TM-171 l.821E+Ol 5.084E+Ol TL-208 2.195E-01 8.882E-02 BI-211 9.795E-02 8. 513E-01 PB-212 8.109E-01 l.095E-01 BI-214 8.548E-01 1.798E-01 PB-214 l.069E+00 1. 730E-01 RN-222 8.548E-01 1:798E-01 RA-224 9.142E-01 1.028E+OO RA-226 8.548E-01 1.798E-01 AC-228 8.687E-01 2.629E-01 RA-228 8.687E-01 2.629E-01 TH-228 8.109E-01 1.095E-01 TH-229 -3.947E-02 3.454E-01 TH-230 8.545E-01 1.797E-01 TH-232 8.687E-01 2.629E-01 TH-234 6.033E-01 2.877E+OO U-234 8.545E-01 l.797E-01 U-238 6.033E-01 2.877E+OO AM-243 2.122E-01 9.750E-02 ANH-511 8.422E-02 6.907E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 4282 of 5809 Key-Line Activity (pCi/GRAM -5.557E+OO 2.268E-02 K.L Act error ( 1 . 96-sigma ) 8.736E+OO 4.171E-02 TPU ( 1. 96-sigma) l.258E+OO 2.164E+Ol 1. 637E+OO l.053E-01 4.161E-02 4.396E-02 3.033E-01 1.683E-01 5.084E+Ol 8.882E-02 8.513E-01 l.095E-01 1. 79BE-01 l.730E-01 1. 7 98E-01 1.028E+OO 1. 798E-01 2.629E-01 2.629E-01 1-. 095E-01 3.454E-01 1. 797E-01 2.629E-01 2.877E+OO l.797E-01 2.877E+OO 9.750E-02 6.907E-02 TPU ( 1. 96-sigma) 9.088E+OO NOT IDENT. 4.295E-02 NOT IDENT.

NA-24 1.000E+41 7.562E+41 O.OOOE+OO SHORT HLIF AL-26 -2.989E-04 l.908E-02 1.908E-02 NOT IDENT. SC-46 -7.038E-02 2.922E-01 2.939E-01 FAIL ABUN V-48 6.086E+03 8.244E+03 8.688E+03 SHORT HLIF CR-51 7.805E+01 2.845E+02 2.867E+02 SHORT HLIF MN-54 l.610E-02 5.573E-02 5.620E-02 NOT IDENT. C0-56 3.776E-01 3.593E-01 3.976E-01 FAIL ABUN MN-56 l.OOOE+41 9.537E+40 O.OOOE+OO SHORT HLIF C0-57 4.337E-03 3.855E-02 3.860E-02 NOT IDENT. C0-58 7.600E-02 4.554E-01 4.567E-01 NOT IDENT. FE-59 1.180E+Ol 1.027E+Ol l.156E+Ol FAIL ABUN C0-60 1.634E-02 2.646E-02 2.747E-02 NOT IDENT. ZN-65 4.146E-02 1.594E-01 1. 605E-01 NOT IDENT. GE-68 -4.203E-01 1. 888E+OO l.897E+OO NOT IDENT. AS-74 -2.237E+03 3.464E+03 3.608E+03 SHORT HLIF SE-75 -4.605E-02 1.588E-01 l.601E-01 NOT IDENT. BR-77 1.405E+37 1.184E+38 O.OOOE+OO SHORT HLIF SR-82 l.925E+02 4. 996E+02 5.070E+02 SHORT HLIF RB-83 2.200E-01 4.587E-01 4.693E-01 NOT IDENT. KR-85 1.238E+Ol 6.743E+OO 8.753E+OO NOT IDENT. SR-85 1.198E+OO 6.545E-01 8.485E-01 NOT IDENT. RB-86 -4.772E+03 1.778E+04 1. 791E+04 SHORT HLIF Y-88 -4.490E-03 1.644E-01 l.644E-01 NOT IDENT. Y-91 -5.238E+Ol 3.562E+02 3.569E+02 NOT IDENT. NB-94 -2.393E-04 2.378E-02 2.378E-02 NOT IDENT. NB-95 1.615E-01 5.690E-01 5.737E-01 NOT IDENT. NB-95M 9.593E-01 1.889E+OO 1.938E+OO NOT IDENT. ZR-95 8.370E-01 1.007E+OO 1. 076E+OO NOT IDENT. NB-97 -1.000E+41 1. 996E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1.052E+41 O.OOOE+OO SHORT HLIF M0-99 -3.870E+30 1.892E+31 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 3. 611E+42 O.OOOE+OO SHORT HLIF RH-101 3.778E-03 2.790E-02 2.795E-02 NOT IDENT. RH-102 -3.628E-02 4.105E-02 4.419E-02 NOT IDENT. RU-103 -l.015E+OO 4.028E+OO 4.054E+OO FAIL ABUN RH-106 -3.191E-01 3.948E-01 4.202E-01 NOT IDENT. RU-106 -3.191E-01 3.948E-01 4.202E-01 NOT IDENT. AG-108M -2.547E-05 2.128E-02 2.128E-02 NOT IDENT. AG-llOM 3.550E-02 7.'731E-02 7.895E-02 FAIL ABUN SN-113 -2.955E-05 l.553E-01 1.553E-01 NOT IDENT. CD-115 2.784E+37 1. 989E+38 O.OOOE+OO SHORT HLIF SN-117M 1.238E+04 5.103E+04 5.133E+04 SHORT HLIF TE-123M 2.728E-02 l.006E-01 1.013E-01 NOT IDENT. SB-124 2.685E-01 -1. 046E+OO

1. 053E+OO NOT IDENT. SB-125 2.614E-02 8.281E-02 8.364E-02 FAIL ABUN TE-125M -l.277E+02 2.023E+02 2.103E+02 NOT IDENT. I-126 l.801E+05 5.252E+05 5.314E+05 SHORT HLIF SB-126 2.980E+05 6.328E+05 6.469E+05 SHORT HLIF SB-127 -3.301E+21 5.862E+21 O.OOOE+OO SHORT HLIF I-131 7.324E+08 2.066E+09 . 2.092E+09 SHORT HLIF I-132 1. OOOE+41 l.998E+42 O.OOOE+OO SHORT HLIF TE-132 3.772E+24 5.096E+25 O.OOOE+OO SHORT HLIF BA-133 7.916E-03 3.483E-02 3.501E-02 FAIL ABUN I-133 -l.OOOE+41 3.059E+41 O.OOOE+OO SHORT HLIF CS-134 6.643E-02 6.092E-02 6.788E-02 FAIL ABUN CS-135 2.868E-02 1.188E-01 l.195E-Ol NOT IDENT. I-135 -1.000E+41 1.825E+42 O.OOOE+OO SHORT HLIF CS-136 -3.901E+04 1.433E+05 l.444E+05 SHORT HLIF BA-140 7.617E+05 6.676E+05 7.507E+05 SHORT HLIF LA-140 -1.309E+05 2.155E+05 2.235E+05 SHORT HLIF CE-141 -1. 295E+Ol l.807E+Ol 1.899E+Ol NOT IDENT. CE-143 l.OOOE+41 9.268E+40 O.OOOE+OO SHORT HLIF CE-144 -2 .495E.-01 2.817E-01 3.033E-01 NOT IDENT. PM-144 3.621E-02 4.314E-02 4.612E-02 NOT IDENT. PR-144 3.123E+OO 3.728E+OO 3.985E+OO NOT IDENT. PM-t46 9.919E-03 3.423E-02 3'. 452E-02 NOT IDENT. ND-147 7.832E+05 1.537E+07 l.538E+07 SHORT HLIF PM-147 -7.533E+Ol 6.585E+02 6.594E+02 NOT IDENT. PM-149 1.084E+39 2.813E+39 O.OOOE+OO SHORT HLIF EU-150 5.816E-03 2.852E-02 2.864E-02 FAIL ABUN EU-152 2.385E-02 8.201E-02 8. 271E-02 NOT IDENT. GD-153 5.877E-01 2.877E-01 3. 911E-01 FAIL ABUN EU-154 6 .113E-02 l.034E-01 l.070E-01 NOT IDENT. TB-160 1. 267E-01 l.410E+OO l.411E+OO FAIL ABUN H0-166M -3 .137E-02 4.277E-02 4.505E-02 NOT IDENT. HF-172 -8.909E-02 l.982E-01 2.023E-01 FAIL ABUN LU-172 4.267E-02 6.757E-02 7.026E-02 FAIL ABUN LU-176 -l.803E-04 l.849E-02 l.849E-02 FAIL ABUN Page 4283 of 5809 HF-181 3.068E+OO 3.183E+OO 3.471E+OO NOT IDENT. TA-182 -2.158E-01 7.474E-01 7.537E-01 FAIL ABUN RE-'183 5.465E-01 2.528E+OO 2.540E+00 NOT IDENT. RE-184 5.823E+OO 1.676E+Ol l.696E+Ol NOT IDENT. W-188 9.420E+OO 8.270E+Ol 8.281E+Ol FAIL ABUN IR-192 -8.742E-02 3.320E-01 3.343E-01 FAIL ABUN HG-203 -2.850E-01 1. 735E+OO 1. 739E+OO NOT IDENT. BI-207 l.454E-02 4.325E-02 4.375E-02 FAIL ABUN PB-210 2.770E+OO 4.423E+OO 4. 596E+OO NOT IDENT. PB-211 l.805E-01 5.148E-01 5.212E-01 NOT IDENT. BI-212 l.210E+OO 6.882E-01 8.781E-01 FAIL ABUN RN-219 -2.561E-02 2.714E-01 2. 716E-01 NOT IDENT. RA-223 1.134E-02 5.329E-01 5.330E-01 FAIL ABUN AC-227 -7.758E-03 l.889E-01 1.889E-01 NOT IDENT. TH-227 -7.758E-03 l.889E-01 1.889E-01 NOT IDENT. PA-231 2.007E-01 3.780E-01 3.886E-01 NOT IDENT. TH-231 l .134E-02 5.329E-01 5.330E-01 FAIL ABUN PA-233 *-2. 67 6E-02 4.400E-02 4.562E-02 NOT IDENT. PA-234 -1.247E-02 2.601E-01 2.602E-01 FAIL ABUN . PA-234M -4.999E-01 3.162E+OO 3.170E+OO NOT IDENT. .U-235 -5.600E-02 1.549E-01 1.569E-01 FAIL ABUN NP-237 -2.676E-02 4.400E-02 4.562E-02 FAIL ABUN NP-238 -7.812E+38 2.948E+40 O.OOOE+OO SHORT HLIF NP-239 5.043E-02 1.882E-01 1. 896E-01 FAIL ABUN PU-239 3.616E+02 4.750E+02 5.022E+02 FAIL ABUN AM-241 -3.858E-02 l.364E-01 1. 375E-01 NOT IDENT. CM-243 5.940E-03 7.980E-02 7.984E-02 FAIL ABUN BK-247 -1.357E-02 5.679E-02 5. 712E-02 FAIL ABUN CM-247 -2.657E-02 2.656E-02 2.914E-02 FAIL ABUN CF-249 l.658E-03 2.597E-02 2.598E-02 NOT IDENT. CF-251 -4.537E-02 8.874E-02 9.107E-02 NOT IDENT. Page 4284 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 65.8718 87.09 68.5842 136.47 72. 9871 45.60 66.6366 87.57 68.6937 140.51 0.0000 46.54 63.6707 88.03 68.7978 143.76 90.1889 49.72 0.0000 88.34 68.8683 "144.24 82.2854 51. 35 62.7398 88.47 68.8977 145.44 98.5465 51. 87 62.9030 89.96 69.2342 152.43 86.0864 52.39 63.0653 1093.63 69.3869 153.25 0.0000 52.97 64.9547 91.*11 0.0000 323.87 60.7209 53.44 70.8146 92.59 69.8211 156.02 0.0000 54.07 65.3026 93.35 69.9888 158.56 0.0000 57.36 0.0000 94.56 70.2553 159.00 71.9414 57.53 61.1352 94.65 70.2750 162.33 64.9100 57.98 65.6367 94.67 70.2793 162.66 0.0000 59.27 70.4227 94.87 62. 28 62 163.33 69.0060 59.32 70.4385 97.43 49.9532 165.86 69.3538 59.54 77.5589 98.43 50.1049 176.31 75.6458 60.96 70.9540 98. 44' 50.1064 176.60 0.0000 61.17 71. 0193 99.53 58.4234 177.52 73.3722 62. 93 84.9819 100 .11 51.0387 181.07 0.0000 63.29 85 .1129 102.03 51.3298 181.52 81.3086 63.58 85.2182 103.18 74.1632 184.41 146.1388 64.28 85.1714 103.37 74.2044 143.76 78.2078 66.73 93.3158 105.21 74.5994 193.51 77.1954 67.24 96.5461 105.31 74.6208 197.03 85.2640 125.81 85.7698 106.12 74.7938 198.01 85.4068 67.75 85.7942 106.47 74.8680 201.83 84.2584 69.67 72.6618 109.28 72.6664 203.43 76.8036 70.83 89.9334 111. 00 80.0327 205.31 71. 9081 72.81 76.9702 111.76 0.0000 210.85 70.8349 72.87 76.9879 114. 06 87. 0718 215.65 69.9893 74.66 81. 57 58 116. 30 0.0000 222 .11 72.1095 74.82 81.6249 116.74 67.3754 227.09 70.0042 74.97 81.6707" 119. 76 74.3754 227.38 62.0561 77 .11 82.3205 121.12 75.7176 228.16 0.0000 78.74 90.1071 121.22 75.7368 228.18 66.5695 79.69 85.3210 121. 7 8 82.3463 116.74 66.5695 80.12 80.3503 122.06 78.0677 235.69 76.7451 80.19 0.0000 122.92 57.5919 235.96 79.4694 80.57 78.5629 123.07 64 .1360 238.63 69.4139 81. 00 89.5572 265.00 71.8557 238.98 0.0000 81. 07 89.5793 125.81 81.7248 240.99 69.6520 81. 75 73.1176 127.23 70.2952 242.00 69.7538 83.79 82.6797 127.91 76.2811 244.70 51.8366 84.00 82.7389 129.30 76.1710 252.40 0.0000 85.43 70.1516 131.20 63.5832 252.80 59.7890 86.55 68.4603 133.02 79.0820 254.15 0.0000 86.79 68.5148 133.52 88.0975 256.23 74.8602 86.94 68.5495 136.00 69.5428 260.90 0.0000 Page 4285 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 69.1763 355.39 0.0000 584.27 32.0203 264.80 69.1883 356.01 45.2559 595.83 0.0000 265.00 66.4007 364.49 0.0000 427.87 57 .1198 268.22 75.1383 366.42 0.0000 602.52 0.0000 269.46 79.9659 372.51 40.2010 604.72 48.8719 270.03 75.3174 375.05 44.5447 607.14 58.1281 271.23 74.4932 377.52 48.9059 609.32 46.9125 273.65 0.0000 356.01 31.0231 610.33 46.9424 276.40 56.9580 388.16 35.4492 614.28 41. 4914 277.37 57.0288 388.63 0.0000 618.01 32.0913 277.60 51. 3413 391.69 36.6466 620.36 34.7102 278.00 51.3677 264.66 35.8708 621. 93 41.5001 279.20 57.1619 401.81 38.0854 630.19 0.0000 279.54 57.1875 402.40 50.0823 631.29 32. 0372 279.70 52.9086 404.85 40.3754 633.25 32.0765 280.46. 52.9605 410.95 47.1861 634.78 0.0000 283.69 56.5297 413. 71 46.2050 635.95 25.3145 284.31 *O. 0000 414.70 0.0000 636.99 0.0000 285.41 51. 8511 423. 72 0.0000 645.85 23.5100 285.90 0.0000 427.09 36.7410 657.76 28.4168 287.50 63.5387 427.87 40.1089 657.90 0.0000 2 90. 67 50.7413 433.94 38.0826 661. 66 29.6704 293.27 0.0000 439.40 55.1429 664.57 0.0000 351.93 56.3704 453.88 33.0392 666.33 0.0000 295. 96 56.4211 463.37 32.1517 666.50 0.0000 879.38 73.1888 468.07 34.5807 667. 71 0.0000 299.98 58.6499 473.00 0.0000 677.62 25.9579 300.09 46.9258 475.06 37.0957 685.70 0.0000 300.13 46.9287 476.78 32.5032 695.00 0.0000 301.36 61.0975 477.60 41.8176 696.49 27.2530 302.85 72.5833 482.18 32.6433 696.51 27.2530 256.23 59.9501 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 33.3243 306.78 53.2134 497.08 38.0390 697.49 28.2786 308.46 53.3177 505.52 31. 3409 702.65 25.3227 311. 90 55.5146 507.63 0.0000 706.68 27. 4112 316.51 55.8109 511. 00 38.4452 711. 68 34.6143 319.41 0.0000 514.00 37. 2772 720.70 0.0000 320.08 0.0000 514.00 37.2772 721. 93 0.0000 321.04 61.3083 520.40 30.6133 722.78 40.9753 323.87 58.7904 520.69 0.0000 722.91 40.9778 325.23 56.3634 522.65 0.0000 723. 31 40.9875 328.76 0.0000 527.90 0.0000 724 .19 34.4459 333.37 51. 7958 528.26 32.6019 727.33 24.6467 333.97 54.8789 529.59 37.1663 733.00 21. 4271 334.37 61.0034 529.87 0.0000 735.93 23.7314 338.28 63.3043 531.02 0.0000 333.97 23.7510 338.32 63.3081 537.26 0.0000 739.50 0.0000 311. 90* 63.4556 546.56 0.0000 747.24 30.1054 340.48 63.4556 552.55 39.6249 748.06 28.0415 340.55 0.0000 563.25 34.3510 752.31 29.1467 344.28 49.3262 569.33 39 .1571 753.82 0.0000 345.93 55.5897 946.00 37. 2961 756.73 20.8679 351.06 47.6106 569.70 *36.3685 756.80 19.8251 351.93 47.6546 583.19 31.9974 884.68 23.4609 Page 4286 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:55:45.11 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM24.CNF;330 Background date : Z-OCT-2016 11:01:18. Sample date 12-SEP-2016 00: 00: 00 Acquisition date .: 3-0CT-2016 07: 53: 26. Sample ID G1203621361 Sample quantity 1.81483E+02 GRAM Detector name : GAM24 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.55 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit 75. 00000 Sen'sitivity 3. 00000 Batch ID 1596252 Detector SN# Matrix Spike ID .: LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.60* 14 31 0. 91 ' 93.26 89 8 3.93E-03 81. 4 2 3 63 .13* 4 36 1. 35 126.33 122 31 1. 24E-032°61. 2 3.68E+OO 3 3 66.47* 7 27 1. 02 133.00 122 31 1. 89E-03132. 6 4 3 73.06' 12 36 1. 38 146.17 122 31 3.25E-03 96.2 5 3 75.07* 15 23 1.14 150.21 122 31 4.14E-03 59.1 6 0 84.41* 22 47 0.64 168.88 164 10 6.00E-03 65.9 7 0 181.10 10 12 1.19 362.32 361 4 2.83E-03 59.7 8 1 191.50 19 27 1. 33 383.12 366 21 5.33E-03 47.5 4.49E+OO 9 0 211. 96 16 32 1. 39 424.05 418 9 4.32E-03 73.1 10 0 306.90 18 43 3.21 613. 97 605 17 4.86E-03 88.6 11 0 331.10 25 17 0.95 662.39 657 11 7.03E-03 38.5 12 0 337.70 29 8 4.44 675.60 668 15 *7. 92E-03 28.1 13 0 409.56 10 12 1:15 819;37 813 8 2.71E-03 69.4 14 0 569.81 18 3 1. 56 1139. 97 1135 10 5.13E-03 28.3 15 0 641. 91 7 10 0.86 1284.22 1277 9 2.03E-03 89.2 16 0 781. 57 9 2 1. 41 1563.65 1558 9 2.40E-03 46.4 17 0 1294.14 6 0 0. 96 2589.33 2586 6 1.67E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 4288 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:55:47 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance.: Errors propagated: Efficiency type Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621361 SOLID GAMMA24 0 01:00:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Sample.geometry Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 07:53:26 181.48 GRAM CAN 0 01:00:01.55 10.00 0.00 % Peak Energy 0.0% No interference correction performed Page 4289 of 5809 Nuclide Line Activity Report Sample ID : Gl203621361 Nuclide Type: Nuclide PB-210 AM-243 Flag: "*" Page 4290 of 5809 Energy 46.54 43.53 74.66 Key line Area 22 22 %Abn 4.25* 5.90 67.20* Acquisition date Page : 2 3-0CT-2016 07:53:26 %Eff 2.450E+OO 1.694E+OO 6.751E+OO Uncorrected Decay Corr pCi/GRAM pCi/GRAM 8.655E-01 8.671E-01 ------Line Not Found 1.985E-02 l.985E-02 2-Sigma %Error 162.73 118 .19 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:55:49.37 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G120362136l:CNF;l *
Acquisition date 3-0CT-2016 07:53:26 Sensitivity : 3.000 *
Detector ID GAM24 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.55 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
Sample ID G1203621361 Sample Quantity l.8148E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;?
Combined Activity-MDA Report Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM PB-210 8. 671E-01 l.383E+00 1.139E+OO AM-243 l.985E-02 2.300E-02 2.924E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 5.083E-02 1.425E-01 3.198E-01 NOT IDENT. NA-22 8.425E-04 l.088E-02 2. 720E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 866E+08 O.OOOE+OO SHORT HLIF AL-26 -l.587E-02 1.555E-02 l.019E-02 NOT IDENT. K-40 -1.089E-01 1.708E-01 3.500E-01 NOT IDENT. SC-46 -l.338E-02 l.742E-02 3*. OOlE-02 NOT IDENT. V-48 -2.147E-02 3.061E-02 5.669E-02 NOT IDENT. CR-51 5.287E-02 l.805E-01 3. 960E-01 NOT IDENT: MN-54 -1.049E-02 1.623E-02 2.783E-02 NOT IDENT. C0-56 1.008E-02 2.022E-02 4. 496E-02 NOT IDENT. MN-56 O.OOOE+OO l.528E+41 O.OOOE+OO SHORT HLIF C0-57 -6.419E-03 8.602E-03 1.555E-02 NOT IDENT. C0-58 7.859E-03 l.802E-02 4.075E-02 NOT IDENT. FE-59 -l.580E-02 2.430E-02 4.506E-02 NOT IDENT. C0-60 1.433E-02 l.469E-02 4.094E-02 NOT IDENT. ZN-65 8.535E-03 3.984E-02 8.774E-02 NOT IDENT. GE-68 2.552E-Ol 4.443E-01 l.130E+OO NOT IDENT. AS-73 -4.145E-02 l.536E-01 3.019E-01 NOT IDENT. AS-74 l.504E-03 5.796E-02 l.188E-01 NOT IDENT. SE-75 1.002E-02 1.998E-02 4.448E-02 NOT IDENT. BR-77 -2.546E+OO 2.272E+Ol 4.783E+Ol NOT IDENT. SR-82 2.193E-02 1.853E-01 3.552E-01 NOT IDENT. RB-83 7.944E-03 2.447E-02 5.750E-02 NOT IDENT. KR-85 -l.077E+Ol 5.521E+OO 8.373E+OO NOT IDENT. SR-85 -6.lOOE-02 3.123E-02 4.735E-02 NOT IDENT. RB-86 1.950E-01 3.453E-01 8.775E-01 NOT IDENT. Y-88 3.774E-03 1. 971E-02 4.743E-02 NOT IDENT. Y-91 -1.230E+OO 7.191E+OO 1.541E+Ol NOT IDENT. Page 4291of5809 NB-94 4.237E-03 1.744E-02 3.634E-02 NOT IDENT. NB-95 -5. 581E-03 l.674E-02 3.215E-02 NOT IDENT. NB-95M -1.053E-02 4.315E-02 9.025E-02 NOT IDENT. ZR-95 4.166E-03 3.394E-02 7.166E-02 NOT IDENT. NB-97 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 5.550E+08 O.OOOE+OO SHORT HLIF M0-99 -7.767E+OO 2.491E+Ol 4.798E+Ol FAIL ABUN. TC-99M O.OOOE+OO 3.637E+23 0.000E+OO SHORT HLIF RH-101 l.476E-03 1.077E-02 2.225E-02 NOT IDENT. RH-102 5.533E-03 2.142E-02 4.788E-02 NOT IDENT. RU-103 -1. 478E-02 l.940E-02 3.474E-02 NOT IDENT. RH-106 3.409E-02 1.318E-01 2.906E-01 NOT IDENT. RU-106 3.409E-02 1.318E-01 2.906E-01 NOT IDENT. AG-108M 6.198E-03 1.372E-02 3.041E-02 NOT IDENT. CD-109 l.316E-03 2.225E-01 4.290E-01 NOT IDENT. AG-llOM -3. 511E-03 2.331E-02 4.581E-02 NOT IDENT. SN-113 9.437E-03 l.982E-02 4.449E-02 NOT IDENT. CD-115 1. 772E+Ol 4.154E+Ol 9.000E+Ol NOT IDENT. SN-ll 7M -4.194E-03 2.848E-02 5.529E-02 NOT IDENT. TE-123M 2. 596E-03 1.046E-02 2 .161E-02 NOT IDENT. SB-124 -l.053E-02 4.213E-02 8.802E-02 NOT IDENT. SB-125 -4.232E-02 3.698E-02 6. ll 7E-02 NOT IDENT. TE-125M 3.022E-01 3.727E+OO 7.616E+OO NOT IDENT. I-126 -4.795E-02 1.074E-01 2.039E-01 NOT IDENT. SB-126 -3.335E-02 9.273E-02 1. 752E-01 NOT IDENT. SN-126 9.BOOE-03 2. 013E-02 4.233E-02 FAIL ABUN SB-127 -6.387E-01 1.336E+OO 2.517E+OO NOT IDENT. I-131 4 .115E-02 7.123E-02 l.678E-01 NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -l.025E-01 1.097E+OO 2.102E+OO NOT IDENT. BA-133 -6.204E-04 1.870E-02 3.895E-02 NOT IDENT. I-133 O.OOOE+OO 4.340E+05 0.000E+OO SHORT HLIF CS-134 -8.249E-03 1.710E-02 3.159E-02 FAIL ABUN CS-135 1. 8 93E-03 5.851E-02 l.255E-01 NOT IDENT. I-135 0.000E+OO l.148E+22 O.OOOE+OO SHORT HLIF CS-136 -4.382E-02 5.679E-02 l.016E-01 NOT IDENT. BA-137M 2.663E-03 1.359E-02 2.994E-02 NOT IDENT. CS-137 2.814E-03 l.435E-02 3.163E-02 NOT IDENT. CE-139 -l.022E-03 l.249E-02 2.426E-02 NOT IDENT. BA-140 l.999E-01 1. 786E-01 4.315E-01 NOT IDENT. LA-140 -l.503E-02 5.703E-02 l.165E-01 NOT IDENT. CE-141 -2.172E-02 2.514E-02 4.379E-02 NOT IDENT. CE-143 O.OOOE+OO 1.000E+03 O.OOOE+OO SHORT HLIF CE-144 3.865E-02 6.539E-02 1. 441E-01 NOT IDENT. PM-144 -1. 381E-03 l.695E-02 3.374E-02 NOT IDENT. PR-144 -l.144E-01 1.270E+OO 2.525E+OO NOT IDENT. PM-146 -l.143E-02 1.823E-02 3.402E-02 NOT IDENT. ND-147 2.901E-02 4.257E-01 8.797E-01 NOT IDENT. PM-147 -1.922E+02 2.532E+02 4. 572E+02 NOT IDENT. PM-149 2.042E+02 2.830E+02 6.421E+02 NOT IDENT. EU-150 7.724E-03 8.214E-03 1.898E-02 NOT IDENT. EU-152 l.383E-02 4. 045E-02. 8. 931E-02 NOT IDENT. GD-153 -7.600E-03 3.074E-02 6.072E-02 NOT IDENT; EU-154 3.944E-03 3.149E-02 7.928E-02 NOT IDENT. EU-155 -1.714E-02 2. 941E-02 5.559E_:02 NOT IDENT. TB-160 -9.336E-03 5.400E-02 1.086E-01 FAIL ABUN H0-166M -8.732E-04 2.717E-02 5.555E-02 FAIL ABUN TM-171 -l.036E+OO 2.947E+OO 6.087E+OO FAIL ABUN HF-172 1. 749E-02 6.942E-02 1.445E-01 FAIL ABUN LU-172 -5.810E-03 2.053E-02 4.350E-02 FAIL ABUN LU-176 2.061E-02 3.580E-02 2.683E-02 FAIL ABUN HF-181 -2.601E-03 2. 072E-02 4.258E-02 NOT IDENT. TA-182 1.301E-02 5.601E-02 1. 361E-01 FAIL ABUN RE-183 7.863E-03 3. 921E-02 8. 681E-02 FAIL ABUN RE-184 -1. 591E-02 6.839E-02 l.304E-01 NOT IDENT. W-188 -3.575E-01 2.727E+OO 5.766E+OO FAIL ABUN IR-192 5.539E-03 1.303E-02 2.992E-02 NOT IDENT. HG-203 l.574E-02 1. 736E-02 4.043E-02 FAIL ABUN BI-207 -1.265E-02 1.932E-02 3. 591E-02 FAIL ABUN TL-208 1.lOlE-02 2. 031E-02 4.155E-02 NOT IDENT. BI-211 -3.067E-02 9.367E-02 1.919E-01 FAIL ABUN PB-211 5.158E-02 3.lOlE-01 6.124E-01 NOT IDENT. BI-212 1. 793E-02 2.377E-01 4.863E-01 NOT IDENT. PB-212 4.675E-03 2.370E-02 5.148E-02 FAIL ABUN BI-214 l.102E-02 3.905E-02 8.256E-02 NOT IDENT. PB-214 -5.032E-03 3.503E-02 7.316E-02 FAIL ABUN RN-219 -l.890E-02 1.356E-01 2.874E-01 NOT IDENT. RN-222 1.102E-02 3.905E-02 8.256E-02 NOT IDENT. Page 4292 of 5809 RA-223 5.608E-02 2.687E-01 5.818E-01 FAIL ABUN RA-224 -2.299E-01 2.271E-01 4.247E-01 NOT IDENT. RA-226 1.102E-02 3.905E-02 8.256E-02 NOT IDENT. AC-227 -2.798E-02 9.981E-02 2.056E-01 NOT IDENT. TH-227 -2.798E-02 9.981E-02 2.056E-01 NOT IDENT. AC-228 2.649E-03 6.232E-02 1. 388E-01 FAIL ABUN RA-228 2.649E-03 6.232E-02 1. 388E-01 FAIL ABUN TH-228 4.675E-03 2.370E-02 5.148E-02 FAIL ABUN TH-229 -2.463E-02 2.048E-01 3.633E-01 FAIL ABUN TH-230 l.102E-02 3.905E-02 8.256E-02 NOT IDENT. PA-231 2.464E-02 1.735E-01 3.494E-01 NOT IDENT. TH-231 5.608E-02 2.687E-01 *5.818E-01 FAIL ABUN TH-232 2.649E-03 .6. 232E-02 1.388E-01 FAIL ABUN PA-233 l.142E-02 2.503E-02 5.313E-02 NOT IDENT. PA-234 5.794E-02 1.336E-01 3.078E-01 FAIL ABUN PA-234M 1.223E+OO 2.026E+OO 4.849E+OO NOT IDENT. TH-234 1.346E-01 6.889E-01 7.164E-01 FAIL ABUN U-234 1.102E-02 3.905E-02 8.256E-02 NOT IDENT. U-235 -1.238E-02 6.765E-02 1. 38 9E-01 NOT IDENT. NP-237 l.142E-02 2.503E-02 5.313E-02 NOT IDENT. NP-238 O.OOOE+OO 5.014E+Ol O.OOOE+OO SHORT HLIF . U-238 1.346E-01 6.889E-01 7.164E-01 FAIL ABUN NP-239 2.474E-02 9.305E-02 1.957E-01 NOT IDENT. PU-239 -7.617E+Ol l.164E+02 2.128E+02 NOT IDENT. AM-241 9.456E-03 2.924E-02 6.198E-02 NOT IDENT. CM-243 2. 281E-03 3.079E-02 6.483E-02 NOT IDENT. BK-247 9. 729E-03 3.420E-02 7.460E-02 FAIL ABUN CM-247 1. 87 9E-03 1.264E-02 2.818E-02 NOT IDENT. CF-249 1.532E-03 1.453E-02 3.181E-02 NOT IDENT. CF-251* 6.146E-02 S.357E-02 1.195E-01 NOT IDENT. ANH-511 -2.504E-02 3.025E-02 6.659E-02 NOT IDENT. Page 4293 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:55:46.38 Nuclide Line Activity Report Nuclide Type: Nuclide PB-210 AM-243 Flag: "*" Page 4294 of 5809 Energy 46.54 43.53 74.66 Key line Area 22 22 %Abn 4.25* 5.90 67.20* %Eff 2.450E+OO *1. 694E+OO 6.751E+OO Uncorrected Decay Corr pCi/GRAM pCi/GRAM 8.655E-01 8.671E-01 ------Line Not Found l.985E-02 l.985E-02 2-Sigma %Error 162.73 118 .19 Summary of Nuclide Activity Sample ID : G1203621361 Page : 2 Acquisition date : 3-0CT-2016 07:53:26 Total number of lines in spectrum 17 Number of unidentified lines 5 Number of lines tentatively identified by NID 12 Nuclide Type : Nuclide PB-210 AM-243 Hlife 22.20Y 7370.00Y Decay 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCJ../GRAM 8.655E-01 l.985E-02 8.854E-01 8.854E-01 Decay Corr pCi/GRAM 8,671E-01 l.985E-02 8.870E-01 8.870E-01 70.59% Decay Corr 2-Sigma Error . 14. llE-01 2.347E-02 Manually accepted* 2-Sigma %Error Flags 162.73 118 .19 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 4295 of 5809 Unidentified Energy Lines Page : 3 Sample ID : G1203621361 Acquisition date : 3-0CT-2016 07:53:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 63.13 7 54 1. 35 126.33 122 31 l.24E-03 **** 5.51E+OO T 3 66.47 10 40 1. 02 133.00 122 31 1.89E-03 **** 5.92E+OO T 3 73.06 17 53 1. 38 146.17 122 31 3.25E-03 **** 6.58E+OO T 0 84.41 31 67 0.64 168.88 164 10 6.00E-03 **** 7.36E+OO T 0 181.10 13 16 1.19 362.32 361 4 2.83E-03 **** 6.81E+OO T 1 191.50 25 36 1. 33 383.12 366 21 5.33E-03 95.0 6.57E+OO 0 211. 96 20 42 1. 39 424.05 418 9 4.32E-03 **** 6.14E+OO T 0 306.90 22 53 3.21 613.97 605 17 4.86E-03 **** 4.64E+OO T 0 331.10 31 20 0.95 662.39 657 11 7.03E-03 77.0 4.36E+OO 0 337.70 35 9 4.44 67°5. 60 668 15 7.92E-03 56.2 4.30E+OO T 0 409.56 12 15 1. 75 819.37 813 8 2.71E-03 ***** 3.68E+OO T 0 569.81 21 3 1. 56 1139. 97 1135 10 5 .13E-03 56.5 2.84E+00 T 0 641. 91 8 11 0.86 1284.22 1277 9 2.03E-03 **** 2.59E+OO 0 781. 57 9 3 1. 41 1563.65 1558 9 2.40E-03 92.8 2.23E+OO 0 1294.14 6 0 0. 96 2589.33 .258 6 6 1.67E-03 81. 6 1. 50E+OO Flags: "T" = Tentatively associated Page 4296 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:05.18 *******************************************************************************
GEL Laboratories LLC * -* 2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l * *Acquisition date 3-0CT-2016 07:53:26 Sensitivity : 3.000 *
Detector ID GAM24 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.55 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID * *Sample ID G1203621361 Analyst initials:.MXRl *
Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
Wet wt 'corr 1. 00000 Wet Weight
0. 00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
Combined Critical Level Report NOTE: Not all "Identified Nuc1ides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide PB-210 AM-243 Le (pCi/GRAM 5.074E-01 1.322E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 Page 4297 of 5809 Le (pCi/GRAM 1.369E-01 9.778E-03 O.OOOE+OO 0.000E+OO 1.356E-01 l.159E-02 2. 0.54E-02 1. 750E-01 l.105E-02 1.913E-02 O.OOOE+OO 6.812E-03 1. 706E-02 1. 424E-02 1.655E-02 3.675E-02 4. 56'6E-01 1. 321E-01 5.106E-02 2.00lE-02 2.156E+Ol l.467E-01 2.363E-02 3.743E+OO 2.116E-02 3.543E-01 1. 77 5E-02 5.923E+OO 1. 57 5E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT . . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-l32 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 4298 of 5809 l.283E-02 3.971E-02 2.993E-02 O.OOOE+OO O.OOOE+OO 1.948E+Ol O.OOOE+OO 9.956E-03 1.991E-02 1.437E-02 1.221E-01 1.221E-01 l.334E-02 1.913E-01 1.874E-02 1. 951E-02 3.954E+Ol 2.476E-02 9.671E-03 . 3 .119E-02 2.488E-02 3.434E+OO 7.976E-02 7.246E-02 1.891E-02 9.570E-01 7.245E-02 O.OOOE+OO 9.302E-01 1. 713E-02 O.OOOE+OO 1. 2 64E-02 5.542E-02 O.OOOE+OO 3.834E-02 1. 239E-02 1.309E-02 1.093E-02 1.898E-01 4.310E-02 1.924E-02 O.OOOE+OO 6.452E-02 1.436E-02 1. 074E+OO 1.430E-02 3.821E-01 2. 008E+o2 2.892E+02 8.046E-03 3. 931E-02 2.743E-02 2.884E-02 2.404E-02 4.269E-02 2.327E-02 2.673E+OO 6.515E-02 1.633E-02 1.203E-02 1.807E-02 5.274E-02 3.859E-02 5.365E-02 2.500E+00 1.300E:_02 1. 818E-02 1.356E-02 1.830E-02 8. 483E-02' 2.638E-01 2.060E-01 2.328E-02 3.650E-02 3.253E-02 1.195E-01 3.650E-02 2.570E-01 NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF . FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. , SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. .NOT IDENT. FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 . TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249. CF-251 ANH-511 Page 4299 of 5809 1.859E-01 3.650E-02 9.087E-02 9.087E-02 5.810E-02 5.810E-02 2.328E-02 1.604E-01 3.650E-02 1.508E-01 2.570E-01 5.810E-02 2.315E-02 l.289E-01 2.053E+OO 3.273E-01 3.650E-02 6.205E-02 2.315E-02 O.OOOE+OO 3.273E-01 8.804E-02 9.392E+Ol 2.745E-02 2.864E-02 3.343E-02 l.187E-02 1.355E-02 5.463E-02 3 .139E-02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. *NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:10.51 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l *
Acquisition date 3-0CT-2016 07:53:26 Sensitivity : 3.000 *
Detector ID GAM24 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.55 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621361 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity 1.8148E+02 GRAM *
Quantity Err(%) l.1020E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. date 17-JUN-2016 07:45:20 Eff. : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide PB-210 AM-243 8.671E-01 l.985E-02 Act Error (1. 96-sigma) 1.385E+OO 2.303E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 Page 4300 of 5809 Key-Line Activity (pCi/GRAM 5.083E-02 8.425E-04 5*. 683E+07 -1.587E-02 -1.089E-01 -1.338E-02

-2.147E-02 5.287E-02 -1.049E-02 1.008E-02 1.000E+41 -6.419E-03 7*. 859E-03 -l.580E-02 1.A33E-02 8.535E-03 2.552E-01 -4.145E-02 l.504E-03 l.002E-02 -2.546E+OO 2.193E-02 7.944E-03 -1.077E+Ol -6.lOOE-02 l.950E-01 3.774E-03 -1.230E+OO K.L Act error ( 1. 96-sigma) l.425E-01 1.088E-02 l.866E+08 1.559E-02 1. 709E-01 1.743E-02 3.062E-02 1.806E-01 l.624E-02 2.023E-02 1. 529E+41 8.608E-03 l.802E-02 2.433E-02 1. 470E-02 3.984E-02 4.444E-01 l.538E-01 5. 796E-02 1.999E-02 2.278E+Ol 1.853E-01 2.449E-02 5.538E+OO 3.133E-02 3.454E-01 l.971E-02 7.191E+OO TPU ( l'. 96-sigma) l.385E+OO 2.303E-02 TPU ( 1. 96-:--sigma) l.443E-01 l.089E-02 l.883E+08 1.715E-02 1.778E-01 1.844E-02 3.211E-02 l.821E-01 1.691E-02 2.073E-02 0.000E+OO 9.081E-03 1.836E-02 2.535E-02 l.606E-02 4*. 003E-02 4.591E-01 l.550E-01 5. 796E-02 2.049E-02 2.281E+Ol 1. 856E-01 2.475E-02 7.365E+OO 4.168E-02 3.564E-01 1.978E-02 7.212E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR.:...144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM..:171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 Page 4301 of 5809 4.237E-03 -5.581E-03 -1.053E-02 4.166E-03 -l.OOOE+41 -l.260E+09 -7.767E+OO 2.463E+23 1.476E-03 5.533E-03 -1. 478E-02 3.409E-02 3.409E-02 6.198E-03 1.316E-03 -3. 511E-03 9.437E-03 1.772E+Ol -4.194E-03 2. 596E-03 -l.053E-02 -4.232E-02 3.022E-01 -4.795E-02 -3.335E-02 9.800E-03 -6.387E-01 4 .115E-02 -l.000E+41 -l.025E-01 -6.204E-04 2.013E+05 1. 8 9.3E-03 -6.036E+21 -4.382E-02 2.663E-03 2.814E-03 -1.022E-03 1.999E-01 -1.503E-02 -2. l 72E-02 1.540E+Ol 3.865E-02 -1. 381E-03 -1.144E-01 -1.143E-02 2. 901E-02 -l.922E+02 2.042E+02 7. 724E-03 l.383E-02 -7.600E-03 3.944E-03 -1.714E-02 -9.336E-03 -8.732E-04 -1.036E+OO 1. 749E-02 -'-5.810E-03 2.061E-02 -2.601E-03 1. 301E-02' 7.863E-03 -l.591E-02 -3.575E-01 5.539E-03 1.574E-02 -1. 265E-02 1.lOlE-02 -3.067E-02 5.158E-02 1.793E-02 4 .. 675E-03 1.102E-02 -5.032E-03 -l.890E-02 1.102E-02 1. 744E-02 l.674E-02 4.315E-02 3.394E-02 3.817E+41 5.573E+08 2.491E+Ol 3.645E+23 l.078E-02 2.143E-02 l.942E-02 1.318E-01 1.318E-01 1. 372E-02 2.225E-01 2.331E-02 l.982E-02 4.155E+01 2.848E-02 1.046E-02 4.213E-02 3.702E-02 3.727E+OO l.074E-01 9.279E-02 2.014E-02 1.338E+OO 7.125E-02 7.291E+41 1.097E+OO 1.870E-02 4.350E+05 1. 710E-02 5.851E-02 1.185E+22 5.690E-02 l.359E-02 l.435E-02 1.249E-02 . 1. 788E-01 5.703E-02 2.516E-02 l.OOOE+03 6. 543K-02 1.695E-02 1.270E+OO l.824E-02 4.257E-01 2.534E+02 2.844E+02 8.220E-03 4.046E-02 3.074E-02 3.149E-02 2.944E-02 5. 401E-02 2. 717E-02 2.949E+OO 6.948E-02 2.054E-02 3.581E-02 2.072E-02 5. 601E-02 3.922E-02 6.840E-02 2.728E+OO l.304E-02 l.737E-02 l.933E-02 2.032E-02 9.368E-02 3.lOlE-01 2.377E-01 2 :. 370E-02 3.905E-02 3.503E-02 l.356E-01 3.905E-02 1.755E-02 l.693E-02 4. 341E-02 3.400E-02 0.000E+OO 7.958E+08 2.516E+Ol 0.000E+OO 1.080E-02 2.157E-02 2.053E-02 l.327E-01 l.327E-01 1.400E-02 2.225E-01 2.336E-02 2.027E-02 4.231E+Ol 2.855E-02 l.053E-02 4.240E-02 4.165E-02 3.729E+OO 1. 096E-01 9.400E-02 2.062E-02 l.369E+OO 7.363E-02 O.OOOE+OO 1.098E+OO l.870E-02 4.443E+05 1. 750E-02 5.852E-02 0.000E+OO 6.024E-02 1.364E-02 1.441E-02 l.250E-02 2.003E-01 5.743E-02 2.700E-02 1.000E+03* 6. 771E-02 1. 696E-02 l.272E+OO 1. 896E-02 4.259E-01 2.678E+02 2.989E+02 8.927E-03 4.094E-02 3.093E-02 3.154E-02 3.044E-02 5.417E-02 2. 717E-02 2.985E+OO 6.992E-02 2. 071E-02 3.700E-02. 2.076E-02 5.632E-02 3.938E-02 6.878E-02 2.732E+OO l.327E-02 l.877E-02 2.015E-02 2.092E-02 9.470E-02 3 .110E-01 2.379E-01 2.380E-02 3.936E-02 3.510E-02 1.359E-01 3.936E-02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT .. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. RA-223 5.608E-02 2.688E-01 2.700E-01 FAIL ABUN RA-224 -2.299E-01 2.274E-01 2.499E-01 NOT IDENT. RA-226 l.102E-02 3.905E-02 3.936E-02 NOT IDENT. AC-227 -2.798E-02 9.988E-02 l.007E-01 NOT IDENT. TH-227 -2.798E-02 9.988E-02 l.007E-01 NOT IDENT. AC-228 2.649E-03 6.232E-02 6.233E-02 FAIL ABUN RA-228 2.649E-03 6.232E-02 6.233E-02 FAIL ABUN TH-228 * . 4.675E-03 2.370E-02 2.380E-02 FAIL ABUN TH-229 -2.463E-02 2.048E-01 2. 051E-01 FAIL ABUN TH-230 l.102E-02 3.905E-02 3.936E-02 NOT IDENT. PA-231 2.464E-02 1.736E-01 1.740E-01 NOT IDENT. TH-231 5.608E-02 2.688E-01 2.700E-01 FAIL ABUN TH-232 2.649E-03 6.232E-02 6.233E-02 FAIL ABUN PA-233 1.142E-02 2.504E-02 2.556E-02 NOT IDENT. PA-234 5.794E-02 l.492E-01 1.514E-01 FAIL ABUN PA-234M l.223E+OO 2.027E+OO 2.lOOE+OO NOT IDENT. TH-234 l.346E-01 6.896E-01 6.922E-01 FAIL ABUN U-234 l.102E-02 3.905E-02 3.936E-02 NOT IDENT. U-235 -1.238E-02 6.765E-02 6.788E-02 NOT IDENT. NP-237 1.142E-02 *2. 504E-02 2.556E-02 NOT IDENT. NP-238 -2.515E+Ol 5.015E+Ol 5.141E+Ol SHORT HLIF U-238 l.346E-01 6. 896E-01 6.922E-01 FAIL ABUN NP-239 2.474E-02 9.307E-02 9.374E-02 NOT IDENT. PU-239 -7.617E+Ol 1.164E+02 l.214E+02 NOT IDENT. AM-241 9.456E-03 2.925E-02 2.956E-02 NOT IDENT. CM-243 2.281E-03 3.079E-02 3.081E-02 NOT IDENT. BK-247 9.729E-03 3.426E-02 3.454E-02 FAIL ABUN CM-247 l.879E-03 1.264E-02 l.267E-02 NOT IDENT. CF-249 1.532E-03 l.454E-02 1.455E-02 NOT IDENT. CF-251 6.146E-02 5.401E-02 6.070E-02 NOT IDENT. ANH-511 -2.504E-02 3.027E-02 3.230E-02 NOT IDENT. Page 4302 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 23.3467 87.09 12.7275 136.47 17.0416 45.60 22.4884 87.57 16.9832 140.51 20.5491 46.54 22. 5396 88.03 22.6610 143.76 18.3359 49. 72 21. 0634 88.34 21.2553 144.24 18.3462 51. 35 17.8385 88.47 21. 2598 145.44 29.8542 51. 87 17.8594 89. 96 21.3104 152.43 39.3530 52.39 21. 8536 90.64 38.4002 153.25 22.0117 52.97 22.8766 91.11 59.7777 154.21 23.1952 53.44 17.9220 92. 59 34.2383 156.02 27.8903 54.07 23.9291 93.35 22.4953 158.56 26.8029 57.36 0.0000 94.56 67.6123 159.00 20.9864 57.53 22.0989 94.65 60.1084 162.33 17.5518 57.98 19.1034 94.67 60 .1101 162.66 30.4338 59.27 16.1303 94.87 51.5387 16.3. 33 31.6274 59.32 16.1320 97.43 33.4155 165.86 29.3636 59.54 16.1393 98.43 17.2727 176.31 23.7476 60. 96 21. 5818 98.44 17.2729 176.60 21. 3791 61.17. 21. 5910 99.53 34.6023 177.52 20.2103 62.93 29.4543 100 .11 28.1386 181.07 14.3172 63.29 29.4754 102.03 18.4504 181.52 17.5066 63.58 29.4925 103.18 21.7429 184.41 19.1531 64.28 29.5332 103.37 18.4865 185. 72 19.1780 66.73 29.6742 105.21 20.7165 193.51 20.9335 67.24 29.7031 105.31 20.7194 197.03 16. 9644 67. 68 29.7281 106.12 25 .1105 198.01 24.2575 67.75 29.7321 106.47 26.2152 201.83 21. 9098 69.67 29.8401 109.28 21.9330 203.43 23.1615 70.83 29.9045 111. 00 25.2835 205.31 25.6437 72.81 30.0133 111.76 24.2097 210.85 18.4094 72.87 30.0167 114. 06 27.5978 215.65 16.0235 74.66 30 .1138 116. 30 19.9308 222 .11 18.5939 74.82 30.1224 116.74 23.2664 227.09 23.6537 74.97 30 .1304 119.76 18.9105 227.38 77 .11 22.2490 121.12 27.8593 228.16 21.1831 78.74 28.2391 121. 22 27.8629 228.18 21.1836 79.69 30. 7296 121.78 24.5373 235.69 20.9002 80.12 25 .1611 122.06 26.7779 235. 96 23.4134 80.19 23.7660 122.92 18.9888 238.63 16.7611 80.57 22.3825 123.07 18.9926 238.98 19.2808 81. 00 22.3989 123.68 26.8341 240.99 29.3888 81. 07 22.4015 125.81 24.6654 242.00 22.6903 81. 75 23.8291 127.23 22.4635 244.70 16.8447 83.79 26.3721 127.91 25.8554 252.40 16.1018 84.00 26.3813 129.30 28.1528 252.80 14. 4114 85.43 26.4437 131. 20 25.9620 254.15 0.0000 86.55 19.7809 133.02 18.1013 256.23 22.9510 86.79 12.7213 133.52 16.9805 260.90 23.0350 86.94 12.7244 136. 00 22.7094 264.66 20.5352 Page 4303 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 20.5371 364.49 8.2449 600.60 14.4489 265.00 21.3964 366.42 10.0889 602.52 0.0000 268.22 18.8754 372.51 8.2852 604. 72 19.6432 269.46 20.6104 375.05 17.5176 607.14 18.6284 270.03 23.1971 377.52 13.8501 609.32 10.3589 271.23 17.1985 383.85 8.3414 610.33 15.5444 273.65 15.5068 388.16 10.2207 614.28 6.2280 276.40 19.8555 388.63 10.2237 618.01 11. 4360 277.37 21. 5973 391.69 12.1039 620. 36 5.2032 277.60 20.7373 400.66 8.4230 621. 93 7.2891 278.00 16.4217 401.81 9.3652 630.19 0.0000 279.20 15.5713 402.40 8.4315 631.29 6.2720 279.54 22.4977 404.85 11. 257 6 633.25 10.4614 279.70 22.5003 410.95 11. 2964 634.78 8.3743 280.46 26.8424 413.71 11.3140 635.95 7.8546 283.69 22.5664 414.70 16.0368 636.99 7.8580 284.31 27.7865 423.72 15.1689 645.85 8. 4118 285.41 23.4641 427.09 15 .1969 657.76 13.7342 285.90 18.2562 427.87 17.1039 657.90 0.0000 287.50 18.2774 433.94 12.3935 661.66 6.3486 290.67 15.7024 439.40 18.1666 664.57 0.0000 293.27 0.0000 453.88 15.4157 666.33 7.4204 295.22 14.0033 463.37 16.4598 666.50 8.4808 295. 96 14.8861 468.07 11. 6467 667.71 0.0000 298.58 17.5456 473.00 10.7030 677.62 8.5176 299.98 11. 8551 475.06 11. 6880 685.70 6.4082 300.09 6.5866 476.78 '4.8743 695.00 10.7182 300.13 6.5868 477.60 8.7773 696. 49 11.7967 301.36 11. 8 666 482.18 11.7300 696. 51 11. 7967 302.85 9.2392 487.02 12.7379 697.00 15. 0168 304.50 13.2141 492.35 14.7363 697.30 13.9458 304.85 13.2172 497.08 14.7705 697.49 13.9469 306.78 13. 234.9 505.52 12.8537 702.65 11. 8240 308.46 13.2504 507.63 0.0000 706.68 13.9950 311.90 10.6252 511. 00 22.8007 711. 68 6.4712 316.51 10.6587 514.00 58. 5727 720. 70 10.8215 319.41 15 .1296 514.00 58. 5727 721. 93 0.0000 320.08 16.0269 520.40 4.9788 722.78 8.6641 321.04 14.2552 520.69 5.9756 722.91 5.4152 323.87 16. 9601 522.65 0.0000 723.31 5.4161 325.23 18.7625 527.90 12.9905 724 .19 9.7518 328.76 16 .1195 528.26 10.9942 727.33 6.5088 333.37 2.6948 529.59 13. 0011 733.00 7.6093 333.97 2.6958 529.87 0.0000 735.93 9.7939 334.37 2. 6965 531.02 14.0103 737.46 8.7106 338.28 9.4618 537.26 7.0253 739.50 8. 7168 338.32 9.4620 546.56 0.0000 747.24 3.2780 340.48 17.5969 10.1062 748.06 3.2789 340.55 17.5977 563.25 8.1240 752.31 4.3786 344.28 14.4736 569.33 6.1094 753.82 7.6665 345.93 14.4886 569.50 6.1099 756.73 7.6745 351.06 15.4443 569.70 6 .1104 756.80* 7.6748 351.93 15.4526 583.19 8.1953 763.94 4. 3966 355.39 0.0000 584.27 8.1992 765.81 7.6993 356.01 18.2263 595.83 12.3599 766.42 12 .1011 Page 4304 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:56:39.30 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621362.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM29.CNF;354 Background date : 2-0CT-2016 11:01:41. Sample date 30-NOV-2015 13:27:00 Acquisition date : 3-0CT-2016 07:54:00. Sample ID G1203621362 Sample quantity 1.81483E+02 GRAM Detector name GAM29 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.45 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 2 8" 29 30 31 32 33 34 2 2 0 3 3 3 0 0 0 0 3 3 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 0 0 0 Page 4306 of 5809 Energy 74.86* 77.22* 84.04* 86.89 90.20 92.91* 128.29 159.92 186.23* 194.46 207.21 209.20 238.64* 241.48 295.24* 329.40 334.02 338.38*

351.93* 397.75 400.82 405.54 463.19 510.81* 547.02* 583.62* 609.36* 662.86. 684.20 709.15 712 .16 727.66 750.81 757.59 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 121 181 36 92 44 95 62 49 53 31 28 54 334 84 165 12 19 89 271 7 17 18 32 13 11 116 172 25 11 11 13 27 15 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 162 163 146 125 159 113 170 234 139 116 31 99 85 103 78 69 38 56 64 29 34 45 33 70 29 49 49 41 15 5 18 44 9 16 1. 08 1.22 1.16 1. 36 1. 35 1. 08 1. 37 3.84 1. 26 1. 33 1. 23 1. 55 1. 02 1. 75 1.13 0.49 1. 24 0.94 1. 31 1. 24 3.16 0.67 2.50 1. 23 0.74 1. 03 1.14 1.13 1. 02 1. 40 1. 80 0.78 1.16 0.52 149.65 154.37 167.99 173.68 180.29 185.69 256.36 319.53 372.08 388.54 414.00 417.97 476.79 482.45 589.85 658.10 667.34 676.04 703.12 794.65 800.79 810.22 925.42 1020.60 1092.97 1166 .13 1217.57 1324. 51 1367.17 1417.06 1423.06 1454.05 1500.33 1513.91 145 145 165 171 171 171 251 314 367 383 412 412 472 472 584 652 665 672 698 790 796 805 922 1014 1089 1160 1213 1318 1363 1415 1415 1446 1496 1506 16 3.35E-02 18.8 16 5.02E-02 14.6 7 1. OlE-02 58. 6 32 2.56E-02 21.4 32 1. 23E-02 51. 6 32 2.63E-02 22.4 11 1.71E-02 43.3 16 1.36E-02 71.2 9 1.47E-02 45.2 10 8.61E-03 69.6 12 7. 66E-03 31. 6 12 1.51E-02 37.0 15 9.29E-02 7.1 15 2.33E-02 27.6 10 4.57E-02 12.8 8 3.28E-03126.0 7 5.28E-03 59.4 10 2.46E-02 19.2 12 7.52E-02 8.6 7 l.82E-03140.4 9 4.62E-03 67.8 10 5.00E-03 73.6 9 8.81E-03 37.5 14 3.72E-03156.3 9 2.95E-03 99.4 12 3.21E-02 15.7 9 4.77E-02 10.8 13 6.94E-03 57.1 8 3.18E-03 66.4 22 3.18E-03 40.0 22 3.70E-03 72.4 16 7.44E-03 58.7 8 4.lOE-03 45.0 11 3.07E-03 77.1 Fit 1.15E+OO 1.65E+OO 3.06E+OO 1. 89E+OO 1.0lE+OO Peak Search Report (continued) Page : 2 Sample ID : Gl203621362 Acquisition date : 3-0CT-2016 07:54:00 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 768.46 19 30 3.80 1535.63 1528 12 5.23E-03 62.7 36 0 795.83 27 25 3.40 1590.35 1585 13 7.58E-03 42.8 37 0 860.59 23 25 4.07 1719.85 1712 14 6.50E-03 49.5 38 0 894.62 15 12 1.44 1787.89 1782 11 4.06E-03 55.1 39 0 911.51* 62 31 1. 57 1821. 68 1817 11 1. 71E-02 22. 0 40 0 915.66 15 5 1.47 1829.98 1827 8 4.06E-03 38.7 41 o* 934.11* 20 11 2.04 1866.87 1860 11 5.68E-03 40.5 42 0 955.28 8 9 0.69 1909.21 1902 9 2.23E-03 76.0 43 2 964. 83 22 11 1.94 1928.33 1924 24 6.14E-03 38.4 3.59E-01 44 2 968.70* 46 15 1.95 1936.06 1924 24 1.29E-02 24.1 45 0 984.31 28 41 7.88 1967.27 1951 26 7.65E-03 69.3 46 0 1000.59* 9 10 0.87 1999.84 1994 10 2.48E-03 79.2 47 0 1120.76* 51 20 1. 49 2240. 22 *2235 13 l.42E-02 23.2 48 0 1170.26 9 17 1. 84 2339. 27 2333 10 2.48E-03 93.6 49 0 1238.99* 16 32' 1.39 2476.79 2469 13 4.39E-03 79.8 50 0 1327.38 6 10 0.56 2653.67 2647 10 1. 61E-03110. 2 51 0 1377.71* 15 2 0.98 2754.40 2750 9 4.05E.:.03 34.8 52 0 1395.69 7 *5 0.64 2790.38 2785 9 1.81E-03 70.7 53 0 1408.25 7 10 1.19 2815.51 2810 10 2.08E-03 86.8 54 0 1460.91* 473 11 1.85 2920.93 2913 14 1. 31E-01 4. 9 55 0 1593.69 . 4 7 0.95 3186.75 3181 7 1.llE-03120.5 56. 0 1730.19 14 3 1.12 3460.08 3454 9 3.98E-03 32.8 57 0 1764.63* 32 0 2.25 3529.05 3523 11 8.89E-03 19.7 58 0 1846.28 10 0 1.05 3692.60 3686 11 2.78E-03 31.6 Flag: "i" = Peak area was modified by background subtraction Page 4307 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:56:41 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621362.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 13:27:00 G1203621362 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:54:00 181.48 GRAM Sample type Detector name : live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA29 0 01:00:00.00 1.50 keV No Linear 75.00 Report Interfering Nuclide Page 4308 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:01.45 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G1203621362 Acquisition date 3-0CT-2016 07:54:00 Nuclide Type: -Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 347.E+OO 1.339E+Ol l.339E+Ol 9.73 OK CD-109 88.03 3.70* 6.242E+OO 1.468E+OO 2.330E+OO 70. 96 OK TE-123M 159.00 84.00* 6.985E+OO 4.621E-02 2.767E-01 142.35 OK SN-126 64.28 9.60 3.737E+OO Line Not Found Absent 86.94 8.90 6.242E+OO 6.102E-01 6.102E-01 70. 96 OK 87.57 37.00* 6.242E+OO 1.468E-01 1.468E-01 70. 96 OK BA-137M 661. 66 89.90* 2.518E+OO 5. 071E-02 5.170E-02 114.17 OK CS-137 661. 66 85.10* 2.518E+OO 5.357E-02 5.462E-02 114 .17 OK TL-208 277.37 6.60 4.914E+OO Line Not Found Absent 583.19 85.00* 2. 771E+OO 2.297E-01 2.297E-01 31. 44 OK 860.56 12.50 2.069E+OO 3.998E-01 3.998E-01 98.91 OK PB-212 74.82 10.28 5.108E+OO 8.367E-01 8.367E-01 64. 85 OK 77 .11 17.10 5.368E+00 1.187E+OO 1.187E+OO 29.14 OK 238.63 43.60* 5.496E+OO 7.363E-01 7.363E-01 14.13 OK 300.09 3.30 4.626E+OO Line Not Found Absent BI-214 609.32 45.49* 2.683E+OO 6. 541E-01 6.544E-01 21. 56 OK 1120.29 14.92 l.685E+OO 8.658E-01 *8.661E-01 46.46 OK 1764.49 15.30 l.129E+00 7.309E-01 7. 311E-01 39.34 OK PB-214 74.82 5.80 5.103E+OO Line Not Found <<INT Reject 77 .11 9.70 5.368E+OO 2.092E+OO 2.093E+OO 29.14 OK 87.09 3.41 6.257E+OO Line Not Found <<INT Reject 242.00 7.25 5. 441E+OO Line Not Found <<INT Reject 295.22 18.42 4.685E+OO 9. 801E-01 9.805E-01 25.67 OK 351. 93 35.60* 4.087E+OO 9.335E-01 9.338E-01 17.17 OK RN-222 609.32 45.49* 2.683E+OO 6.541E-01 6.544E-01 21.56 OK 1120.29 14.92 1.685E+OO 8.658E-01 8.661E-01 46.46 OK 1764.49 15.30 l.129E+OO 7.309E-01 7. 311E-01 39.34 OK RA-224 240.99 4.10* 5.449E+OO 2.414E-01 2.414E-01 487.99 OK RA-226 609.32 45.49* 2.683E+OO 6. 541E-01 6.544E-01 21. 56 OK 1120.29 14.92 l.685E+OO 8.658E-01 8.661E-01 46.46 OK 1764.49 15.30 l.129E+OO 7.309E-01 7. 311E-01 39.34 OK AC-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4. 214E+OO 9.416E-01 9.416E-01 38.45 OK 794.95 4.25 2 .196E+OO 1.309E+OO l.309E+OO 85.63 OK 835. 71 1. 61 2 .116E+OO Line .Not Found Absent 911.20 25.80* 1. 981E+OO 5.294E-01 5.294E-01 43.94 OK 968. 97 15.80 1. 890E+OO 6.731E-01 6.731E-01 48.20 OK RA-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 OK 794.95 4.25 2 .196E+OO 1.309E+OO 1.309E+OO 85.63 OK 835.71 1. 61 2 .116E+OO Line Not Found Absent 911.20 25.80* 1. 981E+OO 5.294E-01 5.294E-01 43.94 OK 968. 97 15.80 1.890E+OO 6. 731E-01 6.731E-01 48.20 OK TH-228 74.82 10.28 5.108E+OO 8.367E-01 8.367E-01 64.85 OK 77 .11 17.10 5.368E+OO 1.187E+OO 1.187E+OO 29.14 OK 238.63 43.60* 5.496E+OO 7.363E-01 7.363E-01 14.13 OK 300.09 3.30 4.626E+OO Line Not Found Absent TH-230 609.32 45.49* 2.683E+OO 6. 541E-01 6.541E-01 21. 56 OK 1120. 29 14.92 1.685E+OO 8.658E-01 8.658E-01 46.46 OK Page 4309 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G1203621362 Acquisition date 3-0CT-2016 07:54:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.30 1.129E+OO 7.309E-01 7.309E-01 39.34 OK TH-232 105.21 1.10 7.155E+OO Line Not Found. Absent 338.32 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 OK 835.71 1. 61 2 .116E+OO Line Not*Found Absent 911. 20 25.80* 1.981E+OO 5.294E-01 5.294E-01 43.94 OK 968. 97 15.80 1.890E+OO 6.731E-01 6.731E-01 48.20 OK U-234 609.32 45.49* 2.683E+OO. 6.541E-01 6.541E-01 21. 56 OK 1120.29 14.92 1.685E+OO 8.658E-01 8.658E-01 46.46 OK 1764.49 15.30 1.129E+OO 7.309E-01 7.309E-01 39.34 OK U-235 89. 96 3.47 6.473E+OO 1.167E+00 l.167E+00 103.23 OK 93.35 5.60 6.639E+OO 1.505E+OO 1.505E+OO 44.72 OK 143.76 10. 96* 7.247E+OO Line Not Found Absent 163.33 5.08 6.922E+OO Line Not Found Absent 185.72 57.20 6.471E+OO 7.775E-02 7.775E-02 90.32 OK 205.31 5.01 6.095E+OO Line Not Found Absent AM-243 43.53 5.90 7. 707.E-01 Line Not Found Absent 74.66 67.20* 5.108E+OO 1. 280E-01 l.280E-01 64.85 OK ANH-511 511. 00 100.00* 3.065E+OO 2.085E-02 2.085E-02 312.60 OK Flag: "*" = Keyline Page 4310 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:42.36 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621362.CNF;l *
Acquisition date 3-0CT-2016 07:54:00 Sensitivity : 3.000
ID GAM29 Energy tolerance: 1.500 *-* Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
Sample date 30-NOV-2015 13:27:00 Analyst initials: MXRl *
Sample ID G1203621362 Sample Quantity 1.8148E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 . * ******************************************************************************* * *
CALIBRATION INFORMATION * * * *.Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.339E+Ol 1.276E+OO CD-109 2.330E+OO 1.621E+OO TE-123M 2.767E-01 3.860E-01 SN-126 1.468E-01 1.021E-01 BA-137M 5.170E-02 5.785E-02 CS-137 5.462E-02 6. lllE-02 TL-208 2.297E-01 7.078E-02 PB-212 7.363E-01 1.020E-01 BI-214 6.544E-01 1.383E-01 PB-214 9.338E-01 1. 572E-01 RN-222 6.544E-01 1.383E-01 RA-224 2.414E-01 1.154E+OO RA-226 6.544E-01 1.383E-01 AC-228 5.294E-01 2.280E-01 RA-228 5.294E-01 2.280E-01 TH-228 7.363E-01 l.020E-01 TH-230 6.541E-01 1.382E-01 TH-232 5.294E-01 2.280E-01 U-234 6.541E-01 1.382E-01 U-235 -2.847E-02 1.491E-01 AM-243 1.280E-01 8.136E-02 ANH-511 2.085E-02 6.386E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4311 of 5809 Key-Line Activity (pCi/GRAM 9.094E-01 -l.468E-02 O.OOOE+OO 6.821E-04 2.276E-01 O.OOOE+OO O.OOOE+OO 4.316E-02 K.L. Cnt Uncert ( 1. 96-sigma) 9.337E+OO 2.842E-02 1. 960E+41 2.041E-02 2.941E-01 5.505E+04 3.635E+02 4.434E-02 MDA (pCi/GRAM 5.070E-01 1.436E+OO 1.844E-01 9.090E-02 4.530E-02 4.785E-02 5.229E-02 7.430E-02 9.840E-02 8. 672E-02 9.840E-02 7. 961E-01 9.840E-02 2.060E-01 2.060E-01 7.430E-02 9.837E-02 2.060E-01 9.837E-02. 2.793E-01 6.750E-02 3.988E-02 MDA (pCi/GRAM 1.918E+Ol 4.947E-02 O.OOOE+OO 4.558E-02 6.lOOE-01 O.OOOE+OO O.OOOE+OO 9.957E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.033E-01 3.510E-01 7. 251E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF , C0-57 4.277E-03 3.403E-02 6.743E-02 NOT IDENT. C0-58 5.487E-02 3.594E-01 7.535E-01 NOT IDENT. FE-59 -2.740E+OO 5.065E+OO 8.886E+OO NOT IDENT. C0-60 -7.006E-03 3.288E-02 6.029E-02 NOT IDENT. *ZN-65 2.254E-02 1.305E-01 2.364E-01 NOT IDENT. GE-68 -4.440E-01 1. 798E+OO 3.335E+OO NOT IDENT. AS-73 4. 681E+OO 6.756E+OO l.454E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.841E+03 0.000E+OO. SHORT HLIF SE-75 1. 286E-01 l.656E-01 3.349E-01 FAIL ABUN BR-77 O.OOOE+OO 1.859E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6. 413E+02 O.OOOE+OO SHORT HLIF RB-83 l.582E-01 4.759E-01 1.002E+OO NOT IDENT. KR-85 3.418E-01 5.153E+OO 9.424E+OO NOT IDENT. SR-85 3.880E-02 5.918E-01 1.082E+OO NOT IDENT. RB-86 O.OOOE+OO 2.904E+04 O.OOOE+OO SHORT HLIF Y-88 1. 07 9E-02 1.566E-01 3.510E-01 NOT IDENT. Y-91 -l.819E+02 4.831E+02 8.560E+02 NOT IDENT. NB-94 6.68.2E-03 2. lllE-02 4.379E-02 NOT IDENT. NB-95 -2.330E-01 7.290E-01 1.205E+OO NOT IDENT. NB-95M l.479E+OO 2.217E+OO 4.075E+OO NOT IDENT; ZR-95 1.124E+OO l.698E+OO 2.308E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8.295E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.480E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 7. 0'55E-02 5.013E-02 FAIL ABUN RH-102 4.599E-02 3.920E-02 9.085E-02 NOT IDENT. RU-103 -3.314E+OO 4.665E+OO 8.641E+OO FAIL ABUN RH-106 4.064E-02 3.430E-01 7.0lOE-01 NOT IDENT. RU-106 4.064E-02 3.430E-01 7.0lOE-01 NOT IDENT. AG-108M 8. 960E-03 1. 8 62E-02 3. 996E-02 NOT IDENT. AG-llOM -1.036E-02 7.142E-02 1.380E-01 NOT IDENT. SN-113 1. 274E-01 1.557E-01 3.462E-01 NOT IDENT. CD-115 O.OOOE+OO 2.181E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 4.072E+05 O.OOOE+OO SHORT HLIF SB-124 -5.048E-01 1.334E+OO 2.677E+OO NOT IDENT. SB-125 l.686E-03 7.121E-02 1.455E-01 FAIL ABUN TE-125M 1.314E+Ol 2.277E+02 4.490E+02 NOT IDENT. I-126 O.OOOE+OO 9. 963E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.227E+06 O.OOOE+OO SHORT HLIF SB-127 0.000E+OO 8.784E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 6.253E+09 O.OOOE+oo* SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.650E+27 O.OOOE+OO SHORT HLIF BA-133 -l.667E-03 2.947E-02 5.432E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 8.629E-02 7. 241E-02 9.031E-02 FAIL ABUN CS-135 -7.265E-02 1.lOOE-01 1.910E-01 NOT IDENT. I-135 O.OOOE+OO 7.372E+40 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 3.324E+05 O.OOOE+OO SHORT HLIF CE-139 -6.776E-03 9.510E-02 1.668E-01 NOT IDENT. BA-140 O.OOOE+OO 1.469E+06 O.OOOE+OO SHORT HLIF LA-140 0.0.00E+OO 4.049E+05 O.OOOE+OO SHORT HLIF CE-141 3.839E+OO 2.286E+Ol 4.447E+Ol NOT IDENT. CE-143 O.OOOE+OO l.806E+41 O.OOOE+OO SHORT HLIF CE-144 -4.504E-02 2.679E-01 5 .138E-01 NOT IDENT. PM-144 -6 .136E-G4 4.134E-02 8.140E-02 NOT IDENT. PR-144 -6.429E-02 3.605E+OO 7.094E+OO NOT IDENT. PM-146 -2.209E-02 2.514E-02 4.586E-02 NOT IDENT. ND-147 O.OOOE+OO 3.356E+07 O.OOOE+OO SHORT HLIF PM-147 -5.927E-01 6.148E+02 1.202E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 2.388E-02 2.780E-02 3.802E-02 FAIL ABUN EU-152 1.248E-02 6.054E-02 1.272E-01 FAIL ABUN GD-153 -1.710E-02 l.401E-01 2.538E-01 NOT IDENT. EU-154 -3.249E-02 7.015E-02 l.240E-01 FAIL ABUN EU-155 4.094E-02 8.398E-02 1.705E-01 FAIL ABUN TB-160 -8.481E-01 l.164E+OO 2.009E+OO FAIL ABUN H0-166M 4.695E-02 6.660E-02 8.460E-02 FAIL ABUN TM-171 l.623E+00 1.449E+Ol 3.014E+Ol NOT IDENT. HF-172 1.635E-01 1.695E-01 3.358E-01 FAIL ABUN LU-172 1. 780E-02 5.510E-02 1.130E-01 FAIL ABUN LU-176 -2.430E-02 l.933E-02 3.043E-02 FAIL ABUN HF-181 -8.918E-01 3.035E+OO 6.002E+OO NOT IDENT. TA-182 -5.704E-01 7.761E-01 1.283E+OO FAIL ABUN RE-183 7.041E-01 2.223E+OO 4.656E+OO NOT IDENT. Page 4312 of RE-184 -l.718E+Ol 2.791E+Ol 4.908E+Ol FAIL ABUN W-188 9.367E+OO 8.920E+Ol l.566E+02 NOT IDENT. IR-192 l.371E-01 3.548E-01 6.946E-01 FAIL ABUN HG-203 2.471E-Ol 2.085E+OO 3.934E+OO NOT IDENT. BI-207 4.148E-03 2.953E-02 6.034E-02 FAIL ABUN PB-:-210 -l.075E+OO 2.373E+OO 4.790E+OO NOT IDENT. BI-211 O.OOOE+OO 4.329E-01 6.209E-01 FAIL ABUN PB-211 6.406E-01 9.241E-01 1. 076E+OO FAIL ABUN BI-212 7.755E-01 8.917E-01 9.038E-01 FAIL ABUN RN-219 3.362E-01 4.468E-01 4.997E-01 FAIL ABUN RA-223 -l.952E-01 4.837E-01 8.512E-01 FAIL ABUN AC-227 4.606E-02 l.642E-01 3.185E-01 FAIL ABUN TH-227 4.606E-02 l.642E-01 3.185E-01 FAIL ABUN TH-229 6 .. 036E-01 8.236E-01 6.840E-01 FAIL ABUN. PA-231 -l.822E-01 3.419E-01 5. 962E-01 NOT IDENT. TH-231 -l.952E-01 4.837E-01 8.512E-01 FAIL ABUN PA-233 2.428E-02 4.514E-02 8.861E-02 NOT IDENT. PA-234 -2.679E-02 1. 968E-01 3.775E-01 NOT IDENT. PA-234M 2.492E+OO 3.870E+OO 6.166E+OO FAIL ABUN TH-234 8.227E-01 9.835E-01 2.126E+OO FAIL ABUN 2.428E-02 4.514E-02 8. 861E-02 NOT IDENT. NP-238 O.OOOE+OO l.358E+41 O.OOOE+OO SHORT HLIF* U-238 8.227E-01 9.835E-01 2.126E+00 FAIL ABUN NP-239 -3.416E-02 1. 776E-01 3.430E-01 NOT IDENT. PU-239 O.OOOE+OO 6.370E+02 4.999E+02 FAIL ABUN AM-241 -6.995E-02 9.698E-02 l.877E-01 NOT IDENT. CM-243 -6.220E-02 7 5.06E-02 l.388E-01 NOT IDENT. BK-247 2. 966E-02 5.635E-02 l. llOE-01 FAIL ABUN CM-247 3.387E-03 2.860E-02 4.380E-02 NOT IDENT. CF-249 -2.697E-02 2.478E-02 4.482E-02 FAIL ABUN CF-251 4.046E-02 8.095E-02 1.621E-01 NOT IDENT. Page 4313 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:56:40.12 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn. %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 465 10.66* l.347E+OO 1.339E+Ol 1.339E+Ol 9.73 CD-109 88.03 132 3.70* 6.242E+OO 2.371E+OO 3.765E+OO 42.83 TE-123M 159.00 66 84.00* 6.985E+OO 4.621E-02 2.767E-01 142.35 SN-126 64.28 ------9.60 3.737E+OO ------Line Not Found ------86.94 132 8.90 6.242E+OO 9.857E-01 9.857E-01 42.83 87.57 132 37.00* 6.242E+OO 2.371E-01 2.371E-01 42.83 BA-137M 661. 66 28 89.90* 2.518E+00 5. 071E-02 5.170E-02 114 .17 CS-137 661.66 28 85.10* 2.518E+OO 5.357E-02 5.462E-02 114 .17 TL-208 277.37 ------6.60 4.914E+OO ------Line Not Found ------583.19 131 85.00* 2. 771E+OO 2.297E-01 2.297E-01 31. 44 860.56 25 12.50 2.069E+OO 3.998E-01 3.998E-01 98.91 BI-211 72. 87 ------1. 23 4.875E+OO ------Line Not Found ------351.06 328 12. 92

4.087E+OO 2. 572E+OO 2. 572E+OO 17.17 PB-212 74.82 176 10.28 5.108E+OO 1.390E+OO 1.390E+OO 37.69 77 .11 263 17.10 5.368E+OO l.187E+OO 1.187E+OO 29.14 238.63 426 43.60* 5.496E+OO 7.363E-01 7.363E-01 14 .13 300.09 ------3.30 4. 626t+oo ------Line Not Found ------BI-214 609.32 193 45.49* 2.683E+OO 6.541E-01 6.544E-01 ,21.56 1120.29 53 14.92 1.685E+OO 8.658E-01 8.661E-01 46.46 1764.49 31 15.30 l.129E+00 7.309E-01 7. 311E-01 39.34 PB-214 74.82 176 5.80 5.108E+OO 2.463E+OO 2.464E+00 37.69 77 .11 263 9.70 5.368E+OO 2.092E+OO 2.093E+OO 29.14 87.09 132 3.41 6.242E+OO 2.573E+OO 2.574E+OO 42.83 242.00 107 7.25 5.449E+OO 1.117E+OO l. ll 7E+00 55.24 295.22 204 18.42 4.685E+OO 9.801E-01 9.805E-01 25.67 351. 93 328 35.60* 4.087E+OO 9.335E-01 9.338E-01 17.17 RN-222 609.32 193 45.49* 2.683E+OO 6.541E-01 6.544E-01 21.56 1120.29 53 14.92 1.685E+OO 8.658E-01 8.661E-01 46.46 1764.49 31 15.30 l.129E+OO 7.309E-01 7. 311E-01 . 39.34 RA-224 240.99 107 4.10* 5.449E+OO 1.974E+OO 1.974E+OO 55.24 RA-226 609.32 193 45.49* 2.683E+OO 6.541E-01 6.544E-Ol 21. 56 1120. 29 53 14.92 l.685E+OO 8.658E-01 8.661E-01 46 .46 1764.49 31 15.30 l.129E+OO 7.309E-01 7. 311E-01 39.34 AC-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 108 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 794.95 30 4.25 2 .196E+OO l.309E+OO l.309E+00 85.63 835.71 ------1. 61 2 .116E+OO ------Line Not Found ------911.20 65 25.80* 1. 981E+OO 5.294E-01 5.294E-01 43.94 968. 97 49 15.80 1. 890E+00 6.731E-01 6.731E-01 48.20 RA-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338:32 108 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 794.95 30 4.25 2 .196E+OO 1.309E+OO 1.309E+OO 85.63 835.71 ------1. 61 2.116E+OO ------Line Not Found ------911. 20 65 25.80* l.981E+00 5.294E-01 5.294E-01 43.94 968. 97 49 15.80 1.890E+OO 6.731E-01 6. 731E-01 48.20 TH-228 74.82 176 10.28 5.108E+OO 1.390E+OO 1.390E+OO 37.69 77 .11 263 17.10 5.368E+OO l.187E+00 l.187E+OO 29.14 Page 4314 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : Gl203621362 Acquisition date .. 3-0CT-2016 07:54:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 42 6 43.60* 5. 496E+OO 7 .. 363E-01 7.363E-01 14.13 300.09 ------3.30 4.626E+OO ------Line Not Found ------TH-230 609.32 193 45.49* 2.683E+OO 6.541E-01 6. 541E-01 21. 56 1120.29 53 14.92 1. 685E+OO 8.658E-01 8.658E-01 46.46 1764.49 31 15.30 1.129E+OO 7.309E-01 7.309E-01 39.34 TH-232 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 108 11. 27 4.214E+OO 9.416E-01 9.416E-01 38:45 835. 71 ------1. 61 2 .116E+OO ------Line Not Found ------911.20 65 25.80* 1. 981E+OO 5.294E-01 5.294E-01 43.94 968. 97 49 15.80 1. 890E+OO 6. 731E-01 6.731E-01 48.20 U-234 609.32 193 45.49* 2.683E+OO 6.541E-01 6.541E-01 21. 56 1120.29 53 14.92 1. 685E+OO 8.658E-01 8.658E-01 46.46 1764.49 31 15.30 1.129E+OO 7.309E-01 7.309E-01 39.34 U-235 89. 96 63 3.47 6.473E+OO 1.167E+OO 1.167E+OO 103.23 93.35 135 5.60 6.639E+OO 1.505E+OO 1.505E+OO 44. 72 143.76 ------10. 96* 7.247E+OO ------Line Not Found ------163.33 ------5.08 6.922E+OO ------Line Not Found ------185.72 70 57.20 6.471E+OO 7.775E,-02 7.775E-02 90.32 205*.31 ------5.01 6.095E+OO ------Line Not Found ------AM-243 43.53 ------5.90 7.707E-01 ------Line Not Found ------74.66 176. 67.20* 5.108E+OO 2.126E-01' 2.126E-01 37.69 ANH-511 511. 00 15 100.00* 3.065E+OO 2.085E-02 2.085E-02 312.60 Flag: "*" Key line Page 4315 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G1203621362 Acquisition date 3-0CT-2016 07:54:00 Total number of lines in spectrum 58 Number of unidentified lines 15 Number of lines tentatively identified by NID 43 Nuclide Type : Nuclide K-40 CD-109 TE-123M SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 119. 20D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+l0Y 1.41E+10Y 1. 41E+l0Y 7.54E+04Y l.41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 59 5.99 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00 ]J. 0 0 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.339E+Ol 2.371E+OO 4.621E-02 2.371E-01 5.071E-02 5.357E-02 2.297E-01 2. 572E+OO 7.363E-01 6.541E-01 9.335E-01 6.541E-01 1.974E+OO 6. 541E-01 5.294E-01 5.294E-01 7.363E-01 6.541E-01 5.294E-01 6.541E-01 7.775E-02 2.126E-01 2.085E-02 2.850E+Ol 2.850E+Ol Decay Corr pCi/GRAM 1.339E+Ol 3.765E+OO 2.767E-01 2. 371E-01 5.170E-02 5.462E-02 2.297E-01 2. 572E+OO 7.363E-01 6.544E-01 9.338E-01 6.544E-01 1.974E+OO 6.544E-01 5.294E-01 5.294E-01 7.363E-01 6.541E-01 5.294E-01 6.541E-01 7.775E-02 2.126E-01 2.085E-02 3.013E+Ol 3.013E+Ol 74.14% Decay Corr 2-Sigma Error 0.130E+Ol 1.612E+OO 3.939E-01 l.015E-01 5.903E-02 6.236E-02 0.722E-01 0.442E+OO 1.041E-01 l.411E-01 l.604E-01 l.411E-01 1. 091E+OO 1.411E-01 2.327E-01 2.327E-01 1.041E-01 1.410E-01 2.327E-01 1.410E-01 7.022E-02 0. 801E-01 6.516E-02 "M" Manually accepted 2-Sign:ia %Error 9.73 42.83 142.35 42.83 114. 1 7 114. 1 7 31.44 17.17 14.13 21. 56 17.17 21. 56 55.24 21. 56 43.94 43.94 14.13 21. 56 43.94 21. 56 90.32 37.69 312.60 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4316of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G1203621362 Acquisition date : 3-0CT-2016 07:54:00 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 84.04 53 211 1.16 167.99 165 7 l.OlE-02 **** 6.02E+00 T 0 128.29 85 235 1. 37 256.36 251 11 1.71E-02 86.6 7.39E+00 T 0 194.46 41 152 1. 33 388.54 383 10 8.61E-03 **** 6.31E+OO T 3 207.21 36 40 1. 23 414.00 412 12 7.66E-03 63.2 6.06E+OO 3 209.20 70 129 1. 55 417.97 412 12 l.51E-02 74.0 6.02E+OO 0 329.40 14 85 0.49 658.10 652 8 3.28E-03 **** 4.30E+OO T 0 334.02 23 46 1. 24 667.34 665 7 5.28E-03 **** 4.26E+OO T 0 397.75 8 35 1. 24 794.65 790 7 l.82E-03 **** 3.72E+OO 0 400.82 20 4} 3.16 800.79 796 9 4.62E-03 **** 3.69E+OO T 0 405.54 21 54 0.67 810.22 805 10 5.00E-03 ***** 3.66E+OO T 0 463.19 37 39 2.50 925.42 922 9 8.81E-03 74.9 3.30E+OO T *0 547.02 12 33 0.74 1092.97 1089 9 2.95E-03 **** 2.91E+OO T 0 684.20 13 16 1. 02 1367.17 1363 8 3.18E-03 **** 2.46E+OO T 3 709.15 13 5 1. 40 1417.06 1415 22 3.18E-03 80.1 2.39E+00 3 712.16 15 20 1. 80 1423.06 1415 22 3.70E-03 **** 2.39E+OO T 0 727.66 29 48 0.78 1454.05 1446 16 7.44E-03 **** 2.35E+OO T 0 750.81 16 10 1.16* 1500.33 1496 8 4.lOE-03 89.9 2.29E+OO 0 7 57. 59 12 17 0.52 1513.91 1506 11 3.07E-03 **** 2.28E+OO T 0 768.46 20 33 3.80 1535.63 1528 12 5.23E-03 **** 2.25E+OO 0 894.62 16 13 1. 44 1787.89 1782 11 4.06E-03 **** 2. OlE+OO T 0 915.66 15 6 1. 47 1829.98 1827 8 4.06E-03 77.5 1. 97E+OO 0 934 .11 22 12 2.04 1866.87 1860 11 5.68E-03 81.0 1. 94E+OO 0 955.28 8 9 0.69 1909.21 1902 9 2.23E-03 **** 1. 91E+OO T 2 964.83 23 11 1. 94 1928.33 1924 24 6.14E-03 76.8 1.90E+OO T 0 984.31 29 43 7.88 1967.27 1951 26 7.65E-03 **** 1.87E+OO T 0 1000.59 9 10 0.87 1999.84 1994 10 2.48E-03 **** 1.84E+OO T 0 1170.26 9 17 1. 84 2339.27 2333 10 2.48E-03 **** l.63E+OO o* 1238.99 16 33 1. 39 2476.79 2469 13 4.39E-03 **** 1.55E+OO T 0 1327.38 6 10 0.56 2653.67 2647 10 1:61E-03 **** 1.46E+OO 0 1377. 71 14 2 0.98 2754.40 2750 9 4.05E-03 69.5 1. 42E+00 0 1395.69 6 4 0.64 2790.38 2785 9 1.81E-03 **** 1. 40E+'OO 0 1408.25 7 9 1.19 2815.51 2810 10 **** 1.39E+OO T 0 1593.69 4 7 0.95 3186.75 3181 7 1.llE-03 **** 1.24E+OO 0 1730.19 14 3 1.12 3460.08 3454 9 3.98E-03 65.6 l.15E+OO 0 1846.28 9 0 1. 05 3692.60 3686 11 2.78E-03 63.2 l.08E+OO Flags: "T" = associated Page 4317 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:57.15 *******************************************************************************
GEL Laboratories LLC *
2040 Sayage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA *
*
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621362.CNF;l *
Acquisition date 3-0CT-2016 07:54:00 Sensitivity 3.000 *
Detector ID GAM29 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
Sample ID G1203621362 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-123M SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 . TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.140E-01 6.756E-01 8.596E-02 4.277E-02 2.002E-02 2 .115E-02 2.365E-02 3.463E-02 4.440E-02 3.925E-02 4.440E-02 3. 711E-01 4.440E-02 9.169E-02 9.169E-02 3.463E-02 4.438E-02 9.169E-02 4.438E-02 l.319E-01 3 .191E-02 1. 801E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4318 of 5809 Le (pCi/GRAM. 8.621E+OO 2. OOlE-02 O.OOOE+OO 1. 766E-02 2.684E-01 O.OOOE+OO 0.000E+OO 4.436E-02 3.187E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM . SN-113 CD-115 SN-ll 7M SB-124 SB-125 TE-125M I-126 SB-126 *sB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 .cs-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-l53 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 4319o.f5809 O.OOOE+OO 3.157E-02 3.219E-01 3. 725E+OO 2.579E-02 l.021E-01 1.442E+00 6.857E+OO O.OOOE+OO 1.555E-01 O.OOOE+OO O.OOOE+OO 4.497E-01 4.241E+00 4. 871E-01 O.OOOE+OO l.368E-01 3.749E+02 l.947E-02 5.304E-01 1.914E+OO 1.023E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 2.360E-02 4.075E-02 3.845E+OO 3.108E-01 3 .108E-01. 1. 809E-02 5.977E-02 1.575E-01 O.OOOE+OO 0.000E+OO 9.889E-01 6.576E-02 2 .115E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.465E-02 O.OOOE+OO 4.106E-02 8.801E-02 O.OOOE+OO O.OOOE+OO 7.815E-02 O.OOOE+OO 0.000E+OO 2.099E+Ol O.OOOE+OO 2.409E-01. 3.635E-02 3.168E+OO 1.991E-02 0.000E+OO 5.646E+02 0.000E+OO 1. 7 53E-02 5.798E-02 l.193E-01 5.045E-02 8.062E-02 8.238E-01 3.779E-02 1. 413E+Ol 1. 578E-01 4.927E-02 1.381E-02 2.649E+00 5.546E-01 2.189E+OO 2.139E+Ol SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT . NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4320 of 5809 7.157E+Ol 3.179E-01 1.820E+OO 2.570E-02 2.260E+OO 2.993E-01 4.950E-01 4.148E-01. 2.254E-01 3.912E-01 1.471E-01 3.202E-01 2.738E-01 3.912E-01 4.084E-02 1.638E-01 2. 711E+OO l.016E+OO 4.084E-02 O.OOOE+OO l.016E+OO 1.609E-01 2.367E+02 8.805E-02 6.513E-02 5.154E-02 1. 966E-02 2.002E-02 7. 572E-02 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:57:04.76 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charlestort, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621362:CNF;l * *.Acquisition date 07:54:00 Sensitivity : 3.000 *
Detector ID GAM29 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
Sample ID G1203621362 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
Quantity Err ( % ) : 1. 1020E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * * *
_CALIBRATION INFORMATION * * *
Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF.GAM29 CAN.CNF;lO
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.339E+Ol 1.456E+OO 1.456E+OO CD-109 2.330E+OO 1.642E+OO 1.642E+OO TE-123M 2.767E-01 3.862E-01 3.862E-01 SN-126 l.468E-01 l.031E-01 1.031E-01 BA-137M 5.170E-02 5.789E-02 5.789E-02 CS-137 5.462E-02 6 .116E-02 6 .116E-02 TL-208 2.297E-01 7.146E-02 7.146E-02 PB-212 7.363E-01 1.092E-01 1.092E-01 BI-214 6.544E-01 1.411E-01 l.411E-01 PB-214 9.338E-01 l.619E-01 1.619E-01 RN-222 6.544E-01 1. 411E-01 1. 411E-01 RA-224 2.414E-01 1,160E+OO 1.160E+OO RA-226 6.544E-01 1.411E-01 1. 411E-01 AC-228 5.294E-01 2.296E-01 2. 296E-01 RA-228 5.294E-01 2.296E-01 2.296E-01 TH-228 7.363E-01 l.092E-01 1.092E-01 TH-230 6.541E-01 1. 411E-01 1. 411E-01 TH-232 5.294E-01 2. 296E-01 2. 296E-01 U-234 6.541E-01 1. 411E-01 1. 411E-01 U-235 -2.847E-02 l.491E-01 l.491E-Oi AM-243. 1. 280E-01 8.244E-02 8.244E-02 ANH-511 2.085E-02 6.387E-02 6.387E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 9.094E-'-01 9.338E+OO 9.347E+OO NOT IDENT. NA-22 -1. 4 68E-02 2.842E-02 2.918E-02 NOT IDENT. NA-24 l.OOOE+41 3.468E+41 O.OOOE+OO SHORT HLIF AL-26 6. 821E-04 2.041E-02 2. 041E-02 NOT IDENT. SC-46 2.276E-01 2.942E-01 3 .116E-01 FAIL ABUN V-48 4.053E+04 5.507E+04 5.803E+04 SHORT HLIF CR-51 9.687E+Ol 3.635E+02 3. 661E+02 . SHORT HLIF MN-54 4.316E-02 4.438E-02 4.846E-02 NOT IDENT. Page 4321 of 5809 C0-56 1.033E-01 3.510E-01 3.541E-01 FAIL ABUN MN-56 l.OOOE+41 ,3. 321E+41 O.OOOE+OO SHORT HLIF C0-57 4.277E-03 3.403E-02 3.409E-02 NOT IDENT. C0-58 5.487E-02 3.594E-01 3.603E-01 NOT IDENT. FE-59 .-2. 740E+OO 5.069E+OO 5.217E+OO NOT IDENT. C0-60 -7.006E-03 3.288E-02 3.304E-02 NOT IDENT. ZN-65 2.254E-02 1.305E-01 l.309E-01 NOT IDENT. GE-68 -4.440E-01 1. 798E+OO l.809E+OO NOT IDENT. AS-73 4.681E+OO 6.824E+OO 7.143E+OO NOT IDENT. AS-74 1. 611E+03 5.843E+03 5.887E+03 SHORT HLIF SE-75 1.286E-01 1.657E-01 1.755E-01 FAIL ABUN BR-77 1.342E+39 1.192E+40 O.OOOE+OO SHORT HLIF SR-82 1.332E+Ol 6.413E+02 6.413E+02 SHORT HLIF RB-83 l.582E-01 4.764E-01 4.817E-01 NOT IDENT. KR-85 3.418E-01 5.153E+OO 5.155E+OO NOT IDENT. SR-85 3.880E-02 5.918E-01 5.920E-01 NOT IDENT. RB-86 -l.577E+04 2.904E+04 2.990E+04 SHORT HLIF Y-88 1. 07 9E-02 1.566E-01 l.566E-01 NOT IDENT. Y-91 :....1.819E+02 4. 831E+o2 .4. 900E+02 NOT IDENT. NB-94 6.682E-03 2. lllE-02 2.132E-02 NOT IDENT. NB-95 -2.330E-Ol 7.290E-01 7.366E-01 NOT IDENT. NB-95M 1.479E+OO 2.220E+OO 2.318E+OO NOT IDENT. ZR-95 1.124E+OO 1.699E+OO 1. 773E+OO FAIL ABUN NB-97 1.000E+41 7. 6-05E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 2.077E+41 O.OOOE+OO SHORT HLIF M0-99 4.417E+32 8.301E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.483E+41 O.OOOE+OO SHORT HLIF RH-101 8.318E-02 7.214E_.:02 8 .131E-02 FAIL ABUN RH-102 4.599E-02 3.938E-02 4.450E-02 NOT IDENT. RU-103 -3.314E+OO 4.668E+OO 4. 901E+OO FAIL ABUN RH-106 4.064E-02 3.430E-01 3.435E-01 NOT IDENT. RU-106 4.064E-02 3.430E-01 3.435E-01 NOT IDENT; AG-108M 8. 960E-03 l.862E-02 1. 906E-02 NOT IDENT. AG-llOM -1.036E-02 7.142E-02 7.157E-02 NOT IDENT. SN-113 1. 27 4E-01 1.558E-01 l.660E-01 NOT IDENT. CD-115 -l.050E+39 2.181E+40 O.OOOE+OO SHORT HLIF SN-117M 2.919E+05 4.088E+05 4.294E+05 SHORT HLIF SB-124 -5.048E-01 1.334E+OO 1.354E+OO NOT IDENT. SB-125 1. 68 6E-03 7.122E-02 7.122E-02 FAIL ABUN TE-125M 1.314E+Ol 2.277E+02 2.278E+02 NOT IDENT. I-126 3.437E+05 9.975E+05 1.009E+06 SHORT HLIF SB-126 l.948E+06 1.282E+06 l.554E+06 SHORT HLIF SB-127 6.744E+22 l.295E+23 O.OOOE+OO SHORT HLIF I-131 2.067E+09 6.253E+09 6.322E+09 SHORT HLIF I-132 1. OOOE+41 l.931E+42 O.OOOE+OO SHORT HLIF TE-132 8.806E+25 1.651E+27 O.OOOE+OO SHORT HLIF BA-133 -1.667E-03 2.947E-02 2.948E-02 NOT IDENT. I-133 1.000E+41 3.076E+41 0.000E+OO SHORT HLIF CS-134 8.629E-02 7. 251E-02 8.228E-02 FAIL ABUN CS-135 -7.265E-02 1.lOlE-01 l.149E-01 NOT IDENT. I-135 -1.000E+41 6.993E+41 O.OOOE+OO SHORT HLIF CS-136 .,-l.218E+05 3.326E+05 3.371E+05 SHORT HLIF CE-139 -6.776E-03 9. 511E-02 9.516E-02 *NOT IDENT. BA-140 5.208E+05 1.469E+06 l.487E+06 SHORT HLIF LA-140 -1.579E+05 4.049E+05 4 .112E+05 SHORT HLIF CE-141 3.839E+OO 2.286E+Ol 2.292E+Ol NOT IDENT. CE-143 1.000E+41 l.809E+41 O.OOOE+OO SHORT HLIF CE-144 -4.504E-02 2.679E-01 2.687E-01 NOT IDENT. PM-144 -6.136E-04 4 .134E-02 4.134E-02 NOT IDENT. PR-144 -6.429E-02 3.605E+OO 3.605E+OO NOT IDENT. PM-146 -2.209E-02 2.519E-02 2.709E-02 NOT IDENT. ND-147 2.020E+06 3.356E+07 3.358E+07 SHORT HLIF PM-147 -5.927E-01 6.148E+o2 6 .148E+02 NOT IDENT . PM-149 . -1. 993E+40 4.142E+41 0.000E+OO SHORT HLIF EU-150 2.388E-02 2.782E-02 2.983E-02 FAIL ABUN EU-152 l.248E-02 6.Cl55E-02 6.081E-02 FAIL ABUN GD-153 -l.710E-02 1.401E-01 l.404E-01 NOT IDENT. EU-154 -3.249E-02 7.016E-02 7.167E-02 FAIL ABUN EU-155 4.094E-02 8.403E-02 8.603E-02 FAIL ABUN TB-160 -8. 481E-01 l.165E+OO 1.226E+OO FAIL ABUN H0-166M 4.695E-02 6.6656-02 6.993E-02 FAIL ABUN TM-171 1.623E+OO 1.449E+Ol 1.450E+Ol NOT IDENT. HF-172 l.635E-01 1. 716E-01 l.867E-01 FAIL ABUN LU-172 l.780E-02 5.513E-02 5. 571E-02 FAIL ABUN LU-176 -2.430E-02 l.936E-02 2.225E-02 FAIL ABUN HF-181 -8.918E-01 3.035E+OO 3.062E+OO NOT IDENT. TA-182 -5.704E-01 7.764E-01 8.179E-01 FAIL ABUN RE-183 7.041E-01 2.226E+OO 2.248E+OO NOT IDENT. Page 4322 of 5809 RE-184 -1. 718E+Ol 2.822E+Ol 2.927E+Ol FAIL ABUN W-188 9.367E+OO 8.921E+Ol 8.931E+Ol NOT IDENT. IR-192 1. 371E-01 3.549E-01 3.602E-01 FAIL ABUN HG-203 2.471E-01 2.085E+OO 2.088E+OO NOT IDENT. BI-207 4.148E-03 2.953E-02 2.959E-02 FAIL ABUN" PB-210 -1.075E+OO 2.375E+OO 2.424E+OO NOT IDENT. BI-211 2.572E+OO 4.479E-01 1.243E+OO FAIL ABUN PB-211 6.406E-01 9.247E-01 9.687E-01 FAIL ABUN BI-212 7.755E-01 8.926E-01 9.586E-01 FAIL ABUN RN-219 3.362E-01 4.487E-01 4.736E-01 FAIL ABUN RA-223 -1.952E-01 4.839E-01 4.918E-01 FAIL ABUN AC-227 4.606E-02 l.643E-01 1. 656E-01 FAIL ABUN TH-227 4.606E-02 1.643E-01 1.656E-01 FAIL ABUN TH-229 6.036E-01 8.241E-01 8.679E-01 FAIL ABUN PA-231 -l.822E-01 3.441E-01 3.537E-01 NOT IDENT. TH-231 -l.952E-01 4.839E-01 4.918E-01 FAIL ABUN PA-233 2.428E-02 4.515E-02 4.646E-02 NOT IDENT. PA-234 -2.679E-02 1. 991E-01 l.995E-01 NOT IDENT. PA-234M 2.492E+OO 3. 871E+OO 4.031E+OO FAIL ABUN TH-234 8.227E-01 l.OOOE+OO 1.067E+OO FAIL ABUN NP-237 2.428E-02 4.515E-02 4.646E-02 NOT IDENT. NP-238 l.000E+41 1.359E+41 O.OOOE+OO SHORT HLIF U-238 8.227E-01 1.000E+OO l.067E+00 FAIL ABUN NP-239 -3.416E-02 1.776E-01 l.783E-01 NOT IDENT. PU-239 7.510E+02 6.378E+02 7. 221E+02 FAIL ABUN AM-241 -6.995E-02 9.712E-02 1.021E-01 NOT IDENT. CM-243 -6.220E-02 7.529E-02 8.034E-02 NOT IDENT. BK-247 2. 966E-02 5.666E-02 5.822E-02 FAIL'ABUN CM-247 3.387E-03 2. 8 61E-02 2.865E-02 NOT IDENT. CF-249 -2.697E-02 2.488E-02 2.769E-02 FAIL ABUN *cF-251 4.046E-02 8.107E-02 8.310E-02 NOT IDENT. Page 4323 of 5809
GEL Laboratories LLC *
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Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY. MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.8228 87.09 84.5897 136.47 72.7609 45.60 90.6690 87.57 84.6464 140 .. 51 *o. 0000 46.54 87.9756 88.03 84.7007 143.76 94.1019 49. 72 0.0000 88.34 84.7372 144.24 81.0109 51.35 81. 0969 88.47 84.7524 145.44 89.8777 51. 87 83 .1107 89.96 84.9265 152.43 77.2600 52.39 73.5198 1093.63 85.0053 153.25 0.0000 52.97 80.3800 91.11 0;0000 323.87 70.7607 53.44 73.6662 92.59 85.2301 156.02 0.0000 54.07 78.6056 93.35 85.3168 158.56 0.0000 57.36 0.0000 94.56 85.4550 159.00 63.3127 57.53 76.1766 94.65 85.4651 162.33 63.5127 57.98 75.2608 94.67 85.4676 162.66 0.0000 59.27 87.1897 94.87 85.4897 163.33 63.5718 59.32 95.0355 97.43 85.7779 165.86 76.0196 59.54 95. 0725 98.43 85.8895 176.31 72.2305 60. 96 103.1699' 98. 44 . 85.8908 176.60' 0.0000 61.17 103.2076 99.53 86.0112 177.52 56.4903 62.93 110.4218 100 .11 86.0756 181.07 0.0000 63.29 99.6382 102.03 75.1525 181.52 72.5625 63.58 99.6871 103.18 89.1992 184.41 86.3848 64.28 129.4501 103.37 99.3270 143.76 85.3443 66.73 102.1977 105.21 82.7887 193.51 56.1284 67.24 109.2346 105.31 86.9913 197.03 59.7402 125.81 121.2386 106.12 84.9798 198.01 62.8547 67.75 l21. 2516 106.47 90.2648 201.83 71. 5096 69.67 97.7024 109.28 86.3624 203.43 69.2926 70.83 103.8762 111. 00 89.7081 205.31 60.1448 72.81 112. 2162 111. 76 0.0000 210.85 74.3525 72. 87 112.2264 114.06 78.3836 215.65 64.1384 74.66 100.4807 116. 30 0.0000 222 .11 65.6310 74.82 100.5051 116.74 81.8178 227.09 62. 3496 74.97 100.5280 119. 7 6 78.9045 227.38 57.6566 77 .11 100.8560 121.12 79.0270 228.16 0.0000 78.74 101.1024 121. 22 79.0354 228.18 52.9823 79.69 95.8447 121. 78 79.0857 116. 74 52.9823 80.12 91.8530 122.06 69.4895 235.69 63.1445 80.19 0.0000 122.92 94.1694 235. 96 63.1567 80.57 83.1280 123.07 87.7631 238.63 62.8849 81. 00 79.1229 265.00 62.8328 238.98 0.0000 81. 07 79.1313 125.81 57.2567 240.99 62.9925 81. 75 93.4263 127.23 90.3203 242.00 63.0386 83.79 ' 96. 4181 127.91 90.3882 244.70 54.0243 84.00 96.4470 129.30 90.5253 252.40 0.0000 85.43 77.5870 131. 20 76.3137 252.80 47.9431 86. 55 80.4360 133. 02 76.8231 254.15 0.0000 86.79 80.4630 133. 52 80.1121 256.23 43.2521 86. 94 84.5720 136.00 68.3833 260.90 0.0000 Page 4324 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41. 0858 355.39 0.0000 584.27 . 30.2799 264.80 49.5496 356.01 33.2228 595.83 0.0000 265.00 45.9298 364.49 0.0000 427.87 19.0446 268.22 60.5667 366.42, 0.0000 602.52 0.0000 269.46 56.9800 372. 51 32.6640 604.72 28.6121 270.03 44.8736 375.05 .28.4044 607.14 31.5015 271.23 57.0475 377.52 40.5082 609.32 28.6609 273.65 0.0000 356.01 38.0497 610.33 25.8047 276.40 41.4105 388.16 39.8682 614.28 25.8431 277.37 49.9675 388.63 0.0000 618.01 21. 08 69 277.60 49.9750 391.69 22.5760 620. 36 18.2277 278.00 54.8657 264.66 26.1694 621.93 19.1984 279.20 48.8074 401.81 23.5662 630.19 0.0000 279.54 63.4639 402.40 23.5734 631.29 11. 5586 279.70 6,3.4702 404.85 28.8475 633.25 23.1338 280.46 41.5205 410.95 36.8278 634.78 0.0000 283.69 44.0552 413.71 32.4887 635.95 12.5435 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 '52.6805 423.72 0.0000 645.85 15.4935 285.90 0.0000 427.09 33. 5871 657.76 21. 8811 287.50 39.2568 427.87 29.1791 657.90 0.0000 290.67 36.0579 433.94 23.9436 661. 66 19.4767 293.27 0.0000 439.40 32.0090 664.57 0.0000 3'51. 93 39.4492 453.88 25. 0'662 666.33 0.0000 295.96 32.8898 463.37 31. 4709 666.50 0.0000 879.38 39.5332 468.07 20.2748 667.71 0.0000 299.98 37.0944 473.00 0.0000 677. 62 12.7313 300.09 37.0972 475.06 25. 3112 685.70 0.0000 300.13 37.0981 476.78 20.8077 695.00 0.0000 301.36 53.2146 477.60 25.3403 696.49 23.6582 302.85 43.3537 482.18 22.6720 696. 51 23.6582 256.23 27.279i 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.7069 306.78 57 .1182 497.08 31.9502 697.49 18.7356 308.46 27.3456 505.52 19.2406 702.65 17.7810 311. 90 33.6305 507.63 0.0000 706.68 10.3864 316.51 32.4754 511. 00 29.3880 711.68 20.8077 319.41 0.0000 514.00 26.2073 720.70 0.0000 320.08 0.0000 514.00 26.2073 721. 93 0.0000 321. 04 40.0781 520.40 21.2078 722.78 19.3937 323.87 51.4364 520.69 0.0000 722.91 20.8864 325.23 43.9444 522.65 0.0000 723. 31 20.8889 328.76 0.0000 527.90 0.0000 724 .19 23.8799 333.37 42.8922 528.26 17.5775 727. 33 18.9250 333.97 40.3828 529.59 14.8099 733.00 16.4651 334.37 40.3926 529.87 0.0000 735.93 15.9818 338.28 32.8928 531. 02 0.0000 333.97 18.9876 338.32 32.8936 537.26 0.0000 739.50 0.0000 311. 90 32.9340 546.56 0.0000 747.24 15.0385 340.48 32.9340 552.55 26.1634 748.06 13.5379 340.55 0.0000 563.25 17.8303 752.31 9.0377 344.28 32.1591 569.33 31. 0436 753.82 0.0000 345.93 33.0364 946.00 31. 9871 756.73 15.6882 351.06 30.5830 569.70 31. 9884 756.80 15.6882 351. 93 30.5984 583.19 30.2669 884.68 ' 12. 0957 Page 4325 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 22.6932 1274.44 21. 0171 1620.50 6.4706 766.42 22.1925 1001.03 14.5684 1621. 92 5.5477 766.84 22.1960 1002.74 16.1945 1678.03 0.0000 772. 60 0.0000 1004.73 19.4436 1690.97 4. 6796 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.7385 778.90 21. 2683 1028.54 0.0000 1063.66 1.2648 783.70 0.0000 1037.84 11. 9838 1771.35 3.7952 785.37 14.2074 1038.76 0.0000 1791.20 0.0000 792.07 19.8301 631.29 16.3770 1808.65 3.8188 794.95 18.3215 1048.07 0.0000 1810.72 0.0000 795.86 18.3267 1049.04 18.5716 1836.06 3.8359 810.06 15.3387 1050.41 4.3714 810.29 15.3400 10"63. 66 9.8687 344.28 10.2271 1077.00 0.0000 810.76 10.2283 1077.34 16.5027 815.77 0.0000 1085.87 12.1279 1048.07 0.0000 1093.63 12.1503 832.01 22.6472 1099.45 14.3806 834.85 11. 3330 1112. 07 15.5335 835.71 12.3667 1112. 84 15.5369 836.80 0.0000 1115. 54 11. 6595 846.75 0.0000 1120.29 16.6760 846. 77 14.4751 1120.55 16.6772 856.80 0.0000 1221. 41 16.6797 860.56 14.5338 1129. 67 13.3711 871.09 14.5788 1131.51 0.0000 873.19 13.5454 1147.95 0.0000 875.33 0.0000 1173.23 20.2617 879.38 13.5697 1177.95 19.1568 880.51 10.4415 1189.05 19.2052 883.24 7.3147 1204.77 21. 5420 884.68 15.6812 1221.41 22.7604 889.28 9.4211 1231.02 20.5283 894.76 23.0653 1235.36 0.0000 898.04 15.7410 1238.28 18.2773 900. 72 25.2041 1260.41 0.0000 903.28 22.0698 1271.87 8.0550 911.20 22 .1194 1274.44 10.3623 912.08 22.1245 1274.54 10.3630 923.98 0.0000 1291.59 12. 7125 926.50 11.6356 1298.22 0.0000 929 .11 19.0540 1312 .11 0. 000'0 937.49 11.1404 1332.49 13.9883 944 .13 0.0000 1362.66 0.0000 946.00 15.9515 1365.19 7.9222 949.00 12.7720 1368.63 0.0000 667. 71 0.0000 1384.29 6.1857 962. 31 11. 2156 1408.01 8.8788 964. 08 17.0983 1457.56 0.0000 966 .17 17.1081 1460.82 9.8694 911. 20 17.1211 1489.16 9.9231 968. 97 17.1211 1505.03 4.5242 983.53 0.0000 1584.12 3.6731 984.45 0.0000 1596.21 0.0000 Page 4326 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:01:10.66 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621363.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 05:45:34. Sample ID G1203621363 Sample quantity 1.15000E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:06.48 0.7% Energy tolerance 1. 500.00 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 Pk It 1 0 2 5 3 5 4 0 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17' 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 Energy 46.43* 58.09 59.50 79.25 83.11* 87.94 122.04 279.02* 346.35 351.38* 484.34 523.51 661. 65* 747.77 754.57_ 812.46 950.54 962. 27* 1116 .17 1121.69* 1173.30 1248.71 1332.59* 1529.97 1609.64 1647.87 1795.57 1916.83 1928.89 BACKGROUND*CORRECTED SAMPLE PEAK REPORT Area 11869 828 23283 191 164 3417 207 95 .go 72 47 93 14716 67 53 29 56 28 117 12 9325 6 8448 11 15 8 7 8 19 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6185 4025 2291 1329 1277 1521 982 512 554 611 493 318 578 337 257 384 457 368 334 194 342 33 127 12 9 14 14 7 3 0.84 1. 41 0. 8.8 1. 39 1. 78 0.83 0.74 1. 69 1. 26 2.18 1. 68 1.14 1. 39 0.83 1. 47 1. 80 1. 94 0.94 1.16 0.97 1. 78 0.51 1. 84 1.19 3.90 3.49 1. 34 0.64 0.75 92.73 116. 07 118. 90 158.42 166.16 175.82 244.06 558.24 692.98 703.04 969. 09 1047.47 1323.87 1496 .19 1509.78 1625.61 1901. 83 1925.31 2233.16 2244.20 2347.45 2498.28 2666.03 3060.79 3220.12 3296.57 3591.92 3834.38 3858.50 88 113 113 155 163 171 241 555 68 9 700 966 1044 1317 1490 1505 1618 1895 1923 2228 2243 2338 2493 2657 3053 3214 3289 3587 3825 3851 9 1. 32E+Ol 1. 5 12 9.20E-01 15.0 12 2.59E+Ol 0.7 8 2.12E-01 33.9 8 1. 82E-01 38. 6 10 3.80E+OO 2.7 8 2.30E-01 27.1 7 1.06E-01 -41.0 8 9.98E-02 46.9 9 8.05E-02 8 5.26E-02.82.2 8 1. 03E-01 35. 0 15 1. 64E+Ol 0. 9 12 7.41E-02 56.5 8 5.85E-02 55.0 11 3.23E-02132.5 10 6.17E-02 73.4 8 3.14E-02118.8 12 1. 30E-01 33 .1 8 1.29E-02209.7 17 1. 04E+Ol 1.1 8 7.14E-03161.0 19 9.39E+OO 1.1 13 1.22E-02 73.6 12 1.65E-02 48.1 11 9.09E-03 94.5 9 7.22E-03109.2 14 8.89E-03 78.6 14 2.07E-02 31.4 Flag: "*" = Peak area was modified background subtraction Page 4327 of 5809 Fit 1.37E+Ol VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:01:12 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKA100"[CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621363.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 Gl203621363 SOLID GAMMAll 0 00:15:00.00 1.50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at* 3-0CT-2016 05:45:34 115. 00 GRAM CAN 0 00:15:06.48 10.00 0.00 % Peak Energy 0.7% No interference correction performed Page 4328 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : Gl203621363 Acquisition date 3-0CT-2016 05:45:34 Nuclide *Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 217 85.60* 7.219E+OO 9.181E-01 9.692E-01 54.18 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 8882 99.85 1. 491E+OO l.558E+02 1.570E+02 2.26 1332.49 8001 99.98* l.340E+OO l.559E+02 l.571E+02 2.27 ZN-65 1115. 54 112 50. 60*' l.552E+OO 3.724E+OO 3.955E+OO 66.10 CD-109 88.03 3628 3.70* 6.296E+OO 4.067E+02 4.199E+02 5.48 SN-126 64.28 ------9.60 4.012E+OO ------Line Not Found ------86.94 3628 8.90 6.296E+OO l.691E+02 1.691E+02 5.48 87.57 3628 37.00* 6.296E+OO 4.067E+Ol 4.067E+Ol 5.48 BA-137M 661. 66 14372 89.90* 2.339E+OO 1. 785E+02 1. 787E+02 1. 80 CS-137 661. 66 14372 85.10* 2.339E+OO 1.886E+02 1. 888E+02 1.80 PM-147 121.22 217 0.00* 7.219E+OO 2.758E+04 2.800E+04 54.18 HG-203 70.83 ------3.69 4.810E+OO ------Line Not Found ------72.87 ------6.19 5.033E+OO ------Line Not Found ------279.20 96 81.56* 4.692E+OO 6.570E-01 9.012E-01 82.00 PB-210 46.54 12924 4. 25** 1. 359E+OO 5.843E+03 5.854E+03 3.02 BI-211 72.87 ------1. 23 5.033E+OO ------Line Not Found ------351.06 73 12.92* 3.889E+OO 3.777E+OO 3.777E+OO 125.27 AM-241 59.54 25108 35.90* 3.356E+OO 5.441E+02 5.442E+02 1. 46 Flag: "*" Key line Page 4329 of 5809 VAX(VMS Nuclide Identification Report Generated 03-0CT-2016 06:01:13.81 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621363.CNF;l *
Acquisition date 3-0CT-2016 05:45:34 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:06.48 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
Sample ID G1203621363 Sample Quantity 1.1500E+02 GRAM *
Batch Number 1596252 Wet Weight 0.00000 * *Wet wt 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN'.CNF;14
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM C0-57 9.692E-01 5.146E-01 4.902E-01 C0-60 1.571E+02 3.493E+OO 7.217E-01 ZN-65 3.955E+00 2.562E+OO 2.638E+OO CD-109 4.199E+02 1.295E+Ol SN-126 4.067E+Ol 2.182E+OO 1.260E+OO BA-137M 1. 787E+02 3.146E+OO 9.642E-01 CS-137 1. 888E+02 3.323E+OO 1.019E+OO PM-147 2.800E+04 l.487E+04 1.400E+04 HG-203 9.012E-01 7.241E-01 8.785E-01 PB-210 5.854E+03 1.732E+02 1. 041E+02 BI-211 3.777E+OO 4.636E+OO 4.860E+OO AM-241 5.442E+02 7.766E+OO 4 .131E+OO Non-Identified Nuclides
Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 2.361E+OO 6.023E+OO 1.078E+Ol NOT IDENT. NA-22 -1.262E-01 3.311E-01 5.897E-01 NOT IDENT. NA-24 O.OOOE+OO 4.671E+09 O.OOOE+OO SHORT HLIF AL-26 3. 251E-01 2.787E-01 6.182E-01 NOT IDENT. K-40 -1.005E+OO 2.190E+OO 3. 961E+00 NOT IDENT. SC-46 6.565E-01 8.353E-01 1. 452E+o*o FAIL ABUN V-48' -2.380E-01 1.841E+OO 3.056E+OO NOT IDENT. CR-51. l.364E-01 5.498E+OO 1.003E+Ol NOT IDENT. MN-54 8. 471E-03 6.506E-01 1.105E+OO NOT IDENT. C0-56 6. OllE-01 7.259E-01 1. 27 9E+OO NOT IDENT. MN-56 O.OOOE+OO l.223E+41 0.000E+OO SHORT HLIF C0-58 l.392E-01 7 .196E-01 l.237E+OO NOT IDENT. FE-59 7.674E-01 1.801E+OO 3.255E+OO NOT IDENT. GE-68 7.808E+OO 2.304E+Ol 4.163E+Ol NOT IDENT. AS-73 -1.905E+Ol 1. 565E+O*l 2.782E+Ol NOT IDENT. AS-74 -4.548E-01 1. 701E+OO 2.948E+OO NOT IDENT. SE-75 2. 961E-01 6.057E-01 1.029E+OO FAIL ABUN BR-77 8.649E+Ol 6.523E+02 1.102E+03 NOT IDENT. Page 4330 of 5809 SR-82 -3. 962E+OO 6.319E+00 1.051E+Ol NOT IDENT. RB-83 -1.573E-Ol 1. 27 5E+OO 2.005E+OO NOT IDENT. KR-85 -1. 076E+Ol 1.029E+02 L 809E+02 NOT IDENT. SR-85 -6.062E-02 5.815E-01 l.023E+OO NOT IDENT. RB-86 1.005E+OO 1.787E+Ol 3.196E+Ol NOT IDENT. Y-88 -7.479E-02 3.186E-01 5.777E-01 NOT IDENT. Y-91 4.385E+Ol 2.053E+02 3.793E+02 NOT IDENT. NB-94 -4.242E-02 4.528E-01 7.821E-01 NOT IDENT. NB-95 -3.273E-01 6.407E-01 1.074E+OO NOT IDENT. NB-95M 7.626E-01 1.537E+OO 2.627E+OO NOT IDENT. ZR-95 2. 396E-01 l.267E+OO 1.971E+OO NOT IDENT. NB-97 0.000E+OO 1.088E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 9.912E+09 O.OOOE+OO SHORT HLIF M0-99 6.896E+Ol 8. 901E+02 -l.539E+03 NOT IDENT. TC-99M O.OOOE+OO 7. 650E+24. O.OOOE+OO SHORT HLIF RH-101 -l.543E-01 3.223E-01 5.560E-01 NOT IDENT. RH-102 3.538E-02 8.329E-01 l.455E+OO NOT IDENT. RU-103 4.764E-01 7.050E-01 1.277E+OO NOT IDENT. RH-106 2.461E+OO 4.742E+OO 8 .. 469E+OO NOT IDENT. RU-106 2.461E+OO 4.742E+OO 8.469E+OO NOT IDENT. AG-108M 4.979E-01 5.191E-01 9.483E-01 NOT IDENT. AG-llOM -1.126E+OO 9.986E-01 1. 600E+OO NOT IDENT. SN-113 -l.261E-01 6.918E-01 1.235E+OO NOT IDENT. CD-115 1.159E+03 1.191E+03 1.992E+03 NOT IDENT. SN-117M 1.978E-02 7.636E-01 1.322E+OO NOT IDENT. TE-123M -9.382E-02 3.048E-01 5.213E-01 NOT IDENT. SB-124 1. 480E-01 6.182E-01 1.244E+OO NOT IDENT. SB-125 5.573E-01 l.533E+OO 2.760E+OO NOT IDENT. TE-125M -7.839E+Ol 1.070E+02 1.848E+02 NOT IDENT. I-126 -1.379E+OO 5.035E+OO 7.683E+00 FAIL ABUN SB-126 2.324E+OO 3.009E+OO 5.384E+OO NOT IDENT. SB-127 -1. 079E+OO 5.496E+Ol 9.550E+Ol NOT IDENT. I-131 -5.030E-01 2.815E+OO 5.056E+OO FAIL ABUN I-132 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -2. 361E+Ol 3.447E+Ol 5.667E+Ol NOT IDENT. BA-133 2.451E-01 6.569E-01 1.086E+OO NOT IDENT. I-133 O.OOOE+OO 1.131E+07 O.OOOE+OO SHORT HLIF CS-134 -l.715E-01 6.811E-01 1.150Et00 NOT IDENT. CS-135. 1.285E+OO 2.0lOE+OO 3.430E+OO NOT IDENT. I-135 O.OOOE+OO 2.400E+23 O.OOOE+OO SHORT HLIF CS-136 1.699E+OO 2.537E+OO 4.662E+OO NOT IDENT. CE-139 9.897E-03 3.140E-01 5.423E-01 NOT IDENT. BA-140 6.420E-01 5.536E+OO 9.809E+OO NOT IDENT. LA-140 -l.362E-01 7.487E-01 1.401E+OO NOT IDENT. CE-141 4.788E-01 7.126E-01 1.266E+OO. NOT IDENT. CE-143 O.OOOE+OO 3.547E+04 O.OOOE+OO SHORT HLIF CE-144 1.131E-01 2.024E+OO 3.544E+OO FAIL ABUN PM-144 -6.812E-02 4.903E-01 8.444E-01 NOT IDENT. PR-144 . -5.151E+OO 3. 681E+Ol 6.339E+Ol NOT IDENT. PM-146 1.784E-01 7.527E-01 1.343E+OO FAIL ABUN ND-147 -1. 611E+OO 1.189E+Ol 2.090E+Ol NOT IDENT. PM-149 8 .191E+03 8.289E+03 1. 428E+04 NOT IDENT. EU-150 -4.957E-02 3.460E-01 6.263E-01 FAIL ABUN EU-152 -1.397E-01 l.476E+OO 2.403E+OO FAIL ABUN GD-153 2.539E-01 8. 941E-01 1.600E+OO NOT IDENT. EU-154 -3.241E-01 9.387E-01 1.678E+OO FAIL ABUN EU-155 1. 291E-01 1. 072E+OO 1.904E+OO FAIL ABUN TB-160 -1.035E+OO 2.836E+OO 4.706E+OO FAIL ABUN H0-166M -3.273E-01 8. 291E-01 1.409E+OO FAIL ABUN TM-171 -1. 563E+Ol 3.027E+02 5.472E+02 NOT IDENT. HF-172 -9.408E-01 2. 096E+OO 3.341E+OO FAIL ABUN LU-172 -2.990E-01 l.151E+OO 2.030E+OO FAIL ABUN LU-176 l.367E-01 3.732E-01 6.249E-01 FAIL ABUN HF-181 9.245E-02 8.533E-01 l.364E+00 FAIL ABUN TA-182 7.318E-02 1. 689E+OO 3.091E+OO FAIL ABUN RE-183 0.000E+OO 7.846E+OO 9. 511E+OO FAIL ABUN RE-184 l .196E+OO 2.803E+OO 4.798E+OO NOT IDENT. W-188 -7. 911E+Ol l.058E+02 1. 702E+02 NOT IDENT. IR-192 -3.021E-01 5. 30'0E-01 8.525E-01 NOT IDENT. BI-207 5.956E-01 9. 396E-01 1.718E+OO NOT IDENT. TL-208 -4.315E-01 5.089E-01 8.616E-01 NOT IDENT. PB-211 3.525E+OO 1.102E+Ol 1. 992E+o1* NOT IDENT. BI-212 -1. 371E+OO 7.064E+OO 1.210E+Ol NOT IDENT. PB-212 -2.450E-02 7.074E-01 1.188E+OO NOT IDENT. BI-214 l.150E-01 9.607E-01 1.693E+OO FAIL ABUN PB-214 1. 371E+OO 1.683E+OO 1.880E+OO FAIL ABUN RN-219 4.541E-01 *6. 367E+OO 1.143E+Ol NOT IDENT. RN-222 l.150E-01 9.607E-01 l.693E+OO FAIL ABUN Page 4331 of 5809 RA-223 2.893E+OO 8.439E+OO 1.551E+Ol FAIL ABUN RA-224 -1.636E+OO 7.647E+OO 1.273E+Ol NOT IDENT. RA-22 6 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN AC-227 1.333E+OO 3. 421E+OO 5.792E+OO FAIL ABUN TH-227 1.333E+OO 3.421E+OO 5.792E+OO FAIL ABUN AC-228 -2.568E+OO 2.820E+00 4.559E+OO NOT IDENT. RA-228 -2.568E+OO 2.820E+OO 4.559E+OO NOT IDENT. TH-228 -2.450E-02 7.074E-01 1.188E+OO NOT IDENT. TH-229 -8. 972E-01 6.039E+OO 1.024E+Ol FAIL ABUN TH-230 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN PA-231 -7.880E-01 6.409E+OO 1.054E+Ol NOT IDENT. TH-231 2.893E+OO 8.439E+00 1. 551E+Ol. FAIL ABUN TH-232 -2.568E+OO 2.820E+OO 4.559E+OO NOT IDENT. PA-233 l.358E-01 .9.376E-01 1.553E+OO NOT IDENT. PA-234 -3.540E+OO 7.560E+OO l.094E+Ol NOT IDENT. PA-234M l.182E+02 8.249E+Ol 1.553E+02 NOT IDENT. TH-234 2.714E+OO 1.268E+Ol 2.156E+Ol NOT IDENT. U-234 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN U-235 6.448E-01 2.040E+OO 3.586E+OO NOT IDENT. NP-237 1.358E-01 9.376E-01 1.553E+OO NOT IDENT. NP-238 O.OOOE+OO 3.044E+03 0.000E+OO SHORT HLIF U-238 2.714E+OO 1.268E+Ol 2.156E+Ol NOT IDENT. NP-239 -1. 961E.:...01 2.712E+OO 4.764E+00 FAIL ABUN PU-239 2.654E+03 3.394E+03 6.089E+03 NOT IDENT. AM-243 -3.661E-01 5.147E-01 9.083E-01 NOT IDENT. CM-243 -3.044E-01 1.095E+OO 1.923E+OO FAIL ABUN BK-247 3.790E-01 1.055E+OO 1.783E+OO FAIL ABUN CM-247 2.140E-01 5.785E-01 1. 047E+00 FAIL ABUN CF-249 3.677E-02 5.769E-01 1.040E+OO NOT IDENT. CF-251 2.301E-01 1.383E+OO 2.387E+00 NOT IDENT. ANH-511 -l.054E-01 4.336E-01 7. 712E-01 NOT IDENT. Page 4332 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:01:11.57 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 217 85.60* 7.219E+OO 9.181E-01 9.692E-01 54.18 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 8882 99.85 1.491E+OO l.558E+02 1. 570E+02 2.26 1332.49 8001 99.98* 1.340E+OO l.559E+02 1.571E+02 2.27 ZN-65 1115. 54 112 50.60* 1.552E+OO 3.724E+OO 3.955E+OO 66.10 CD-109 88.03 3628 3.70* 6.296E+OO 4.067E+02 4.199E+02 5.48 SN-126 64.28 ------9:6o 4.012E+OO ------Line Not Found ------86.94 3628 8.90 6.296E+OO 1.691E+02 l.691E+02 5.48 87.57 3628 37.00* 6.296E+OO 4.067E+Ol 4.067E+Ol 5.48 BA-137M 661. 66 14372 89.90* 2.339E+OO 1.785E+02 1:787E+02 1. 80 CS-137 661.66 14372 85.10* 2.339E+OO 1.886E+02 l.888E+o2 1. 80 PM-147 121. 22 217 0.00* 7.219E+OO 2.758E+04 2.800E+04 54.18 HG-203 70.83 ------3.69 4.810E+00 ------Line Not Found ------72.87 ------6.19 5.033E+OO ------Line Not Found ------279.20 96 81.56* 4.692E+OO 6.570E-01 9.012E-01 82.00 PB-210 46.54 12924 4.25* 1.359E+OO 5.843E+03 5.854E+03 3.02 BI-211 72.87 ------1. 23 5.033E+OO ------Line Not Found ------351.06 73 12.92* 3.889E+OO 3.777E+OO 3.777E+OO 125.27 AM-241 59.54 25108 35.90* 3.356E+OO 5. 441E+02 5.442E+02 1. 46 Flag: "*" Key line Page 4333 of 5809 Summary of Nuclide Activity Sample ID : Gl203621363 Acquisition date Page : 2 3-0CT-2016 05:45:34 To.tal number of lines in spectrum 2 9 Number of unidentified lines 10 Number of lines tentatively identified by NID 19 65.52% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags C0-57 271.74D 1. 06 9.181E-01 9.692E-01 5.251E-01 54.18 C0-60 5.27Y 1. 01 1.559E+02 1. 571E+02 0.036E+02 2.27 ZN-65 244.06D 1. 06 3. 724E+OO 3:955E+OO 2.614E+OO 66.10 CD-109 461. 40D 1. 03 4.067E+02 4.199E+02 0.230E+02 5.48 SN-126 2.30E+05Y 1. 00 4.067E+Ol 4.067E+Ol 0.223E+Ol 5.48 BA-137M 30.08Y 1. 00 1. 785E+02 1. 787E+02 0.032E+02 1. 80 CS-137 30.08Y 1. 00 l.886E+02 1. 888E+02 0.034E+02 1. 80 PM-147 2.62Y 1. 02 2.758E+04 2.800E+04 1.517E+04 54.18 HG-203 46.59D 1. 37 6.570E-01 9.012E-01 7.389E-01 82.00 PB-210 22.20Y '1. 00 5.843E+03 5.854E+03 0.177E+03 3.02 BI-211 7.04E+08Y 1. 00 3.777E+OO 3.777E+00 4.731E+OO 125.27 AM-241 432.60Y 1. 00 5.441E+02 5.442E+02 0.079E+02 1. 46 ------------------Total Activity 3.494E+04' 3.540E+04 Grand Total Activity 3.494E+04 3.540E+04 Flags: "K" Keyline not found "M" Manually accepted "E" = Manually edited "*A" = Nuclide specific abn. limit Page 4334 of 5809 Unidentified Energy Lines Page : 3 Sample ID : Gl203621363 *Acquisition date : 3-0CT-2016 05:45:34 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 58.09 894 . 4344 1. 41 116. 07 113 12 9.20E-01 30.0 3.15E+OO T 0 79.25 204 1417 1. 39 158.42 155 8 2.12E-01 67.7 5.65E+OO T 0 83 .11 174 1359 1. 78 166.16 163 .8 l.82E-01 77.2 5.96E+OO T 0 346.35 90 556 1. 26 692.98 689 8 9.98E-02 93.8 3. 94E+OO* T 0 484.34 47 488 1. 68 969.09 966 8 5.26E-02 **** 2.99E+OO 0 523.51 92 314 1.14 1047.47 1044 8 l.03E-01 70.0 2.81E+OO T 0 747.77 65 328 0.83 1496.19 1490 12 7.41E-02 **** 2.13E+OO T 0 754.57 51 250 1. 47 1509.78 1505 8 5.85E-02 **** 2. llE+OO T 0 812.46 28 372 1. 80 1625.61 1618 11 3.23E-02 **** 1. 99E+OO 0 950.54 53 440 1. 94 1901.83 1895 10 6.17E-02 **** 1.76E+00 0 962.27 27 353 0.94 1925.31 1923 8 3.14E-02 **** 1. 75E+OO T 0 1121. 69 11 185 0.97 2244.20 2243 8 l.29E-02 **** 1. 55E+OO T 0 1248. 71 6 31 0.51 2498.28 2493 8 7.14E-03 **** l.42E+OO 0 1529.97 10 11 1.19 3060.79 3053 13 1.22E-02 **** 1.19E+OO 0 1609.64 14 9 3.90 3220.12 3214 12 l.65E-02 96.2 1.13E+OO 0 1647.87 8 13 3.49 3296.57 3289 11 9.09E-03 **** 1. llE+OO 0 1795.57 6 13 1. 34 3591. 92 3587 9 7.22E-03 **** 1.02E+OO 0 1916.83 7 7 0.64 3834.38 3825 14 8.B9E-03 **** 9.58E-01 0 1928.89 17 3 0.75 3858.50 3851 14 2.07E-02 62.7 9.52E:-01 Flags: "T" Tentatively associated Page 4335 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:01:28.00 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* *
DETECTOR AND SAMPLE DATA * * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621363.CNF;l *
Acquisition date 3-0CT-2016 05:45:34 Sensitivity 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:06.48 Half life ratio : ***** *
Sample date 12-SEP-2016 00: oo*: 00 Nuclide Library : SOLID *
Sample ID G1203621363 Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.1500E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10:31:39 Eff. : CAN *
Eff. Eile : DKA100: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
Combined Critical Level Report NOTE: Not all Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M. CS-137 PM-147 HG-203 PB-210 BI-211 AM-241 Le (pCi/GRAM 2.391E-01 3.345E-01 1. 272E+OO 6.319E+OO 6.146E-01 4.655E-01 4.917E-01 6.825E+03 4.267E-01 5.148E+Ol 2.360E+OO 2.036E+00 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 Page 4336 of 5809 Le (pCi/GRAM 5.246E+OO 2.692E-01 O.OOOE+OO 2.745E-01 1. 714E+OO 7.0"38E-01 1.477E+OO *4.873E+OO 5.338E-01 6.177E-01 O.OOOE+OO 5.971E-01 1.573E+OO 2.0lOE+Ol 1.375E+Ol 1.420E+OO 5.008E-01 5. 371E+02 5. 05*4E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT" IDENT.

RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB*-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 TL-208 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 4337of5809 9.700E-01 8.764E+Ol 4.954E-01 1.542E+Ol 2.483E-01 . 1. 778E+02 3."753E-01 5.158E-01 1.280E+OO 9.469E-01 O.OOOE+OO O.OOOE+OO 7.409E+02 O.OOOE+OO 2.707E-01 7.016E-01 6.192E-01 4.085E+OO 4.085E+OO 4.624E-01 7.730E-01 6.005E-01 9.620E+02 6.433E-01 2.537E-01 5. 351E-01 1.344E+OO 9.002E+Ol 3.699E+OO 2.594E+OO 4.583E+Ol 2.457E+OO 0.000E+OO 2.761E+Ol 5.285E-01 O.OOOE+OO 5.544E-01 1.670E+OO O.OOOE+OO 2.249E+OO 2.638E-01 4.739E+OO 5.982E-01 6.166E-01 O.OOOE+OO l.725E+OO 4.059E-01 3.047E+Ol 6.546E-01 1.008E+Ol 6.947E+03 3 .-041E-01 1.168E+OO 7. 811E-01 7.666E-01 9.281E-01 2.278E+OO 6.753E-01 2.703E+02 1. 626E+OO 9.793E-01 3.038E-01 6.617E-01 l.443E+OO 4. 717E+OO 2.324E+OO 8. 272E+Ol 4.141E-01 8.299E-01 4.148E-Ol 9.694E+OO 5.810E+OO 5.790E-01 8.155E-01 9.149E-01 5.561E+OO 8.155E-01 7.545E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF* SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT; NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT' IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 . NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4338 of 5809 6.203E+OO 8.155E-01 2.823E+OO 2.823E+OO 2.205E+OO 2.205E+OO 5.790E-01 4.989E+OO 8.155E-01 5.123E+OO 7.545E+OO 2.205E+OO 7.555E-01 5.305E+OO 7. 521E+Ol 1. 053E+Ol 8.155E-01 1.747E+OO 7.555E-01 O.OOOE+OO 1.053E+Ol 2.320E+OO 2. 967E+03 4.441E-01 9.374E-01 8.676E-01 5.098E-01 5. 051E-01 l.162E+00 3.734E-01 NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT: NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-.2016 06: 01: 33. 73 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621363.CNF;l *
Acquisition date 3-0CT-2016 05:45:34 Sensitivity : 3.000 *
Detector ID GAMll Energy tolerance: 1.500 *
Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 00:15:06.48 Half life ratio : ***** *
Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
Sample ID G1203621363
Analyst initials: MXRl *
Batch Number 1596252 Sample Quantity : 1.1500E+02 GRAM *
Quantity Err(%) : 1. 7391E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 2-AUG-2016 10: 31: 39 Eff. Geometry : . CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are Please refer to Certificate of Identified Nuclides Activity Nuclide (pCi/GRAM C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 PM-147 HG-203 PB-210 BI-211 AM-241 9.692E-01 1.571E+02 3.955E+OO 4.199E+02 4.067E+Ol 1. 787E+02 1.888E+02 2.800E+04 9.012E-01 5.854E+03 3.777E+OO 5.442E+02 Act Error ( 1. 96-sigma) 5.165E-01 6.753E+OO 2.566E+OO 4 .101E+Ol 3.337E+OO 8.302E+OO 8.751E+OO l.492E+04 7.253E-01 5.374E+02 4.639E+OO 4.078E+Ol Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 Page 4339 of 5809 Key-Line Activity (pCi/GRAM 2.361E+OO -1.262E-01 -3.221E+08 3.251E-01 -l.005E+OO 6.565E-01 -2.380E-01 1.364E-01 8.471E-03 6. OllE-01 l.OOOE+41 l.392E-01 7.674E-01 7.808E+00 -1.905E+Ol -4.548E-01 2. 961E-01 8.649E+01 K.L Act error (1.96-sigma) 6.024E+OO 3. 311E-01 4.671E+09 2.795E-01 2.191E+OO 8.358E-01 1.841E+OO 5.498E+OO 6.506E-01 7.264E-01 l.224E+41 7.197E-01 1.801E+OO 2.304E+Ol 1.613E+Ol 1.702E+OO 6.058E-01 6.544E+02 TPU ( 1. 96-siqma) 5 .165E-01 . 6.753E+OO 2.566E+OO 4.101E+Ol 3.337E+00 8.302E+OO 8.751E+00 l.492E+04 7.253E-01 5.374E+02 4.639E+OO 4.078E+Ol TPU ( 1. 6 .117E+OO 3.359E-01 4.673E+09 3.156E-01 2.237E+OO 8.866E-01' 1.844E+OO 5.498E+OO 6.506E-01 7.753E-01 O.OOOE+OO 7.224E-01 1.834E+OO 2. 331E+Ol 1.828E+Ol 1. 714E+OO 6.204E-01 6.556E+02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

SR-82 -3. 962E+OO 6. 321E+OO 6.568E+OO NOT IDENT. RB-83 -1.573E-01 1.275E+OO 1.277E+OO NOT IDENT. KR-85 -1.076E+Ol 1.029E+02 1.030E+02 NOT IDENT. SR-85 -6.062E-02 5.815E-01 5.822E-01 NOT IDENT. RB-86 1.005E+OO l.787E+Ol 1.788E+Ol NOT IDENT. Y-88 -7.479E-02 3.186E-01 3.204E-01 NOT IDENT. Y-91 4.385E+Ol 2.053E+02 2.062E+02 NOT IDENT. NB-94 -4.242E-02 4.528E-01 4.532E-01 NOT IDENT. NB-95 -3.273E-01 6.409E-01 6.577E-01 NOT IDENT. NB-95M 7.626E-01 1.538E+OO 1.576E+OO NOT IDENT. ZR-95 2. 396E-01 1.267E+OO 1.272E+OO NOT IDENT. NB-97 l.OOOE+41 1.089E+41 O.OOOE+OO SHORT HLIF ZR-97 -2.917E+09 9.913E+09 1.000E+lO SHORT HLIF M0-99 6. 896E+Ol 8.901E+02 8.907E+02 NOT IDENT. TC-99M -5.812E+23 7.650E+24 O.OOOE+OO SHORT HLIF RH-101 -l.543E-01 3.235E-01 3.309E-01 NOT IDENT. RH-102 3.538E-02 8.329E-01 8.330E-01 NOT IDENT. RU-103 4.764E-01 7.054E-01 7.374E-01 NOT IDENT. RH-106 2. 461E+OO 4.745E+OO 4.873E+OO NOT IDENT. RU-106 2.461E+OO 4.745E+OO 4.873E+OO NOT IDENT. AG-108M 4.979E-01 5.195E-01 5.659E-01 NOT IDENT. AG-llOM -1.12 6E+OO 1.000E+OO 1.122E+OO NOT IDENT. SN-113 -1. 261E-01 6.918E-01 6.941E-01 NOT IDENT. CD-115 1.159E+03 1.193E+03 1.302E+03 NOT IDENT. SN-ll 7M l.978E-02 7.636E-01 7. 637E-01. NOT IDENT. TE-123M -9.382E:-02 3.048E-01 3.077E-01 NOT IDENT. SB-124 1.480E-01 6.183E-01 6.218E-01 NOT IDENT. SB-125 5.573E-01 1.533E+OO 1.554E+OO NOT IDENT. TE-125M -7.839E+Ol 1.071E+02 1.128E+02 NOT I DENT*. I-126 -1.379E+OO *5.036E+OO 5.074E+OO FAIL ABUN SB-126' 2.324E+OO 3.018E+OO ' 3.195E+OO NOT IDENT. SB-127 -l.079E+00 5.496E+Ol 5. 496E+Ol NOT IDENT. I-131 -5.030E-01 2.815E+OO 2.824E+OO FAIL ABUN

I-132 1.000E+41 3.210E+41 O.OOOE+OO SHORT HLIF TE-132 -2.361E+Ol 3.453E+Ol 3. 613E+Ol NOT IDENT. BA-133 2. 451E-01 6.569E-01 6.662E-01 NOT IDENT. I-133 -9. 551E+06 1.139E+07 l.218E+07 SHORT HLIF CS-134 -1.715E-01 6.812E-01 6.856E-01 NOT IDENT. CS-135 1.285E+OO 2.012E+OO 2.094E+00 NOT IDENT. I-135 1.294E+23 2.4SOE+23 O.OOOE+OO SHORT HLIF CS-136 1.699E+OO 2.541E+OO 2.654E+OO NOT IDENT. CE-139 9.897E-03 3.140E-01 3 .141E-01 NOT IDENT. BA-140 6.420E-01 5.536E+OO 5.543E+OO NOT IDENT. LA-140 -l.362E-01 7.487E-01 7. 513E-01 NOT IDENT. CE-141 4.788E-01 7.129E-01 7.449E-01 NOT IDENT. CE-143 9.974E+03 3.547E+04 3.575E+04 SHORT HLIF CE-144 l.131E-01 2.024E+OO 2.025E+OO FAIL ABUN PM-144 -6.812E-02 4.903E-01 4.913E-01 NOT IDENT. PR-144 -5.151E+OO 3.681E+Ol 3.688E+Ol NOT IDENT. PM-146 1. 784E-01 7.528E-01 7.570E-01 FAIL ABUN ND-147 -l.611E+00 1.189E+Ol l.191E+Ol NOT IDENT. PM-149 8 .191E+03 8.362E+03 9.141E+03 NOT IDENT. EU-150 -4.957E-02 3.460E-01 3.467E-01 FAIL ABUN EU-152 -l.397E-01 1.476E+OO l.477E+OO FAIL ABUN GD-153 2.539E-01 8.943E-01 9.016£-01 NOT IDENT. EU-154 -3. 241E-01 9.388E-01 9.501E-01 FAIL ABUN EU-155 1.291E-01 1. 072E+OO 1.073E+OO FAIL ABUN TB-160 -1.035E+OO 2.836E+OO 2.874E+OO FAIL ABUN H0-166M -3.273E-01 8.293E-01 8.423E-01 FAIL ABUN TM-171 -l.563E+Ol 3.027E+02 3.028E+02 NOT IDENT. HF-172 -9.408E-01 2.102E+OO 2.144E+OO FAIL ABUN LU-172 -2.990E-01 1.152E+OO 1.159E+OO FAIL ABUN LU-176 1.367E-01 3.732E-01 3.783E-01 FAIL ABUN HF-181 9.245E-02 8.533E-01 8.543E-01 FAIL ABUN TA-182 7.318E-02 1.689E+OO 1.690E+OO FAIL ABUN RE-183 2.665E+Ol 8.325E+OO l.462E+Ol FAIL ABUN RE-184 1.196E+OO 2.804E+OO 2.856E+OO NOT IDENT. W-188 -7.911E+Ol 1.062E+02 l.120E+02 NOT IDENT. IR-192 :...3. 021E-01 5.302E-01 5.474E-01 NOT IDENT. BI-207 5.956E-01 9.399E-01 9.775E-01 NOT IDENT. TL-208 -4.315E-01 5.093E-01 5.452E-01 NOT IDENT. PB-211 3.525E+OO l.102E+Ol 1.114E+Ol NOT IDENT. BI-212 -1.371E+OO 7.065E+OO 7.092E+OO NOT IDENT. PB-212 -2.450E-02 7.074E-01 7.074E-01 NOT IDENT. BI-214 1.150E-01 9.607E-01 9.621E-01 FAIL ABUN PB-214 1. 371E+OO 1.684E+OO 1. 793E+OO FAIL ABUN RN-219 4. 541E-01 6.368E+OO 6. 371E+OO NOT IDENT. RN-222 1.150E-01 9.607E-01 9.621E-01 FAIL ABUN Page 4340 of 5809 RA-223 2.893E+OO 8.441E+OO 8.541E+OO FAIL ABUN 'RA-224 -1.636E+OO 7.647E+OO 7.683E+OO NOT IDENT. RA-226 l.150E-01 9.607E-01 9. 621E-01 FAIL ABUN AC-227 1.333E+OO 3.426E+OO 3.478E+OO FAIL ABUN TH-227 1. 333E+oo* 3.426E+OO 3.478E+OO FAIL ABUN AC-228 -2.568E+OO 2.823E+OO 3.052E+OO NOT IDENT. RA-228 -2.568E+OO 2.823E+OO 3.052E+OO NOT IDENT. TH-228 -2.450E-02 7.074E-01 7.074E-01 NOT IDENT. TH-229 -8. 972E-01 6.039E+OO 6.053E+OO FAIL ABUN TH-230 1.150E-01 9.607E-01 9.621E-01 FAIL ABUN PA-231 -7.880E-01 6. 411E+OO 6.421E+OO NOT IDENT. TH-231 2.893E+OO 8.441E+OO 8.541E+OO FAIL ABUN TH-232 -2.568E+OO 2.823E+OO 3.052E+OO NOT IDENT. PA-233 l.358E-01 9.376E-01 9. 396E-01 NOT IDENT. PA-234 -3.540E+OO 8.577E+OO 8.724E+OO NOT IDENT. PA-234M 1.182E+02 8.265E+Ol 9.835E+Ol NOT IDENT. TH-234 2. 714E+OO l.269E+Ol 1.275E+Ol NOT IDENT. U-234 1.150E-01 9.607E-01 9.621E-01 FAIL ABUN U-235 6.448E-01 2.040E+OO 2.061E+OO NOT IDENT. NP-237 1.358E-01 9.376E-01 9. 396E-01 NOT IDENT. NP-238 -2.836E+03 3.046E+03 3.304E+03 SHORT HLIF U-238 2.714E+OO 1. 2 69E+Ol 1.275E+Ol NOT IDENT. NP-239 ;,-1. 961E-01 2.712E+OO 2. 713E+OO FAIL ABUN PU-239 2.654E+03 3. 396E+03 3.600E+03 NOT IDENT. AM-243 -3.661E-01 5.152E-01 5.410E-01 NOT IDENT. CM-243 -3.044E-01 1.095E+OO 1.104E+OO FAIL ABUN BK-247 3.790E-01 1. 057E+OO 1. 071E+OO FAIL ABUN 'CM-247 2.140E-01 5.796E-01 5.B76E-01 FAIL ABUN CF-249 3.677E-02 5.770E-01 5. 772E-01 NOT IDENT. CF-251 2.301E-01 1.383E+OO 1.387E+OO NOT IDENT. ANH-511 -l.054E-01 4.336E-01 4.362E-01 NOT IDENT. Page 4341of5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT
ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 2 607 .1199 87.09 526.4185 136.47 462.4787 45.60 2305.2644 87.57 526.9440 140.51 447.7479 46.54 2312.1226 88.03 527.4438 143.76 456.1200 49.72 1998.8229 88.34 527.7771 144.24 464.7412 51. 35 2036.0985 88.47 527.9181 145.44 423.9873 51. 87 2091.8289 89.96 598.8670 152.43 487.0103 52.39 2084.6348 90.64 558.0259 153.25 478.1124 52.97 2249. 9666 91.11 535.8098 154.21 441.9241 53.44 2294.6055 92.59 485.7486 156.02 460.9651 54.07 2239.7058 93.35 575.0147 158.56 429.7643 57.36 0.0000 94.56 518.1766 159.00 449.0831 57.53 1544.4453 94.65 518.2677 162.33 436.2131 57.98 1546.3274 94. 67 518.2885 162.66 436.4070 59.27 1551. 7247 94.87 531. 8596 163.33 443.1870 59.32 1551.9331 97.43 522.9874 165.86 419.0242 59.54 1552.8472 98.43 507.6409 176.31 455.0555 '60. 96 1558.7084 98.44 507.6530 176.60 455.2222 61.17 1559.5687 99.53 516.4120 177.52 431. 87 52 62.93 636.6469 100 .11 537.2310 181.07 416.3553 63.29 569.5972 102.03 474.3099 181.52 443.8521 63.58 561. 7068 103.18 481.*1395 184.41 467.3179 64.28 596.0218 103.37 500.7175 185. 72 471.3557 66.73 617.6526 105.21 494.6171 193.51 487.9491 67.24 625.6205 105.31 476.2035 197.03 496.6341 67. 68 634.3989 106.12 486.6575 198.01 472.7295 67.75 652.5067 106.47 501.6041 201.83 432.3575 69.67 594.0779 109.28 509.0335 203.43 477.9187 70.83 641. 0640 111. 00 462.3766 205.31 458.7520 72.81 629.4874 111.76 499.4379 210.85 510.1346 72.87 629.5770 114. 06 468.7961 215.65 553.6837 74.66 674.2770 116. 30 461. 6581 222 .11 524.4224 74.82 669.9482 116.74 462.0022 227.09 501. 9272 74.97 661. 9428 119.76 495.3075 227.38 490.5913 77 .11 588.8037 121.12 497.7583 228.16 513.9859 78:74 658.6654 121. 22 497.8380 228 .. 18 513.9995 79.69 660.0477 121. 78 509.9864 235.69 449.6315 80.12 660.6736 122.06 510.2233 235. 96 448.5966 80.19 660.7770 122.92 510.9417 238.63 470.7408 80.57 595.1940 123.07 511.0659 238.98 460.4400 81. 00 595.7524 123.68 490.4684 240.99 485.8404 81. 07 595.8406 125.81 467.9542 242.00 456.0076 81. 75 596. 7222 127.23 477.1027 244.70 495.8334 83.79 591.8694 127.91 436.1330 252.40 461. 8872 84.00 592.1306 129.30 427. 9627 252.80 464.4241 85.43 595.7939 131. 20 484.1711 254.15 0.0000 86.55 525.8289 133.02 433.5213 256.23 454.1367 86. 79 526.0895 133.52 439.9770 260.90 416.9625 86.94 526.2561 136. 00 429.3574 264.66 401.7507 Page 4342 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 401. 8022 364.49 397.0626 600.60 234.6748 265.00 406.6546 366.42 382.0649 602.52 0.0000 268.22 404.2838 372. 51 385.5010 604.72 224.1943 269.46 435.8824 375.05 380.9866 607.14 250.4076 270.03 467.2668 1093.63 394.7345 609.32 223.7083 271.23 429.3968 383.85 402.6404 610.33 218.8218 273.65 438.7730 388.16 376.6493 614.28 *237.2700 276.40 425.8051 388.63 402.2409 618.01 220.6445 277.37 443.8730 391.69 406.6187 620.36 235. 9658 277.60 443.9629 400.66 415.3367 621. 93 224.0798 278.00 428.0396 401. 81 431. 6240 630.19 0.0000 279.20 374.5297 402.40 414.0597 631.29 237.2089 279.54 380.2926 404.85 411.2007 633.25 244. 5011 279.70 380.3406 410.95 436.9745 634.78 218.3906 280.46 362.8601 413.71 379.7089 635.95 230.6533 283.69 395.4521 414.70 444.3293 636.99 224.6919 284.31 428.4413 423. 72 423.5953 645.85 219.5332 285.41 379.0503 427.09 439.8474 657.76 240.6841 285.90 370.7042 427.87 434.6649 657.90 0.0000 287.50 377. 3111 433.94 443.6139 661. 66 256.9849 290.67 440.6077 439.40 432.4403 664.57 0.0000 293 .*27 0.0000 453.88 460.2279 666.33 233.9375 295.22 410.4895 463.37 501.6549 666.50 204.7115 295.96 409.5292 468.07 482.7480 667.71 '0.0000 298.58 376.0472 473.00 477.6889 677.62 200.0783 299.98 394. 9511 475.06 469.9277 685.70 189.4187 300.09 394.9805 476.78 396.9679 695.00 183.9717 300 .13 395.0001 477.60 400.8795 696.49 210.0879 301.36 394.1797 482.18 335.7568 696. 51 210. 0961 302.85 377.4106 487.02 378.7976 697.00 202.8552 304.50 410.0557 492.35 327.4431 697.30 195.6039 304.85 410.1671 497.08 311. 4102 697.49 190.4165 306.78 383. 6118 505.52 318.5909 702.65 191. 8913 308.46 421.3269 507.63 0.0000 706.68 196. 4071 311. 90 403.8994 511. 00 297.7704 711. 68 190.5535 316.51 407.9217 514.00 318.2200 720.70 199.7025 319.41 388.4661 514.00 318.2200 721. 93 0.0000 320.08 375.3296 520.40 296.0085 722. 78 232.4924 321. 04 376.4664 520.69 290.3381 722. 91 226.1979 323.87 397.3989 522.65 0.0000 723. 31 232.5464 325.23 409.5594 527.90 218.2681 724.19 202.1094 328.76 367.8872 528.26 244.7316 727. 33 198.1665 333.37 369.2239 529.59 274.0484 733.00 204.9804 333.97 378.6793 529.87 0.0000 735.93 231.6805 334.37 396.5147 531. 02 253 .1611 737.46 211. 7187 338.28 365. 5723 537.26 264.6047 739.50 218.2547 338.32 365.5811 546.56 0.0000 747.24 214.7154 340.48 418.7523 552.55 247.3840 748.06 214.7894 340.55 418.7723 563.25 248.7848 752.31 204.5156 344.28 404.2505 569.33 238.8075 753.82 208.9040 345.93 382.2054 569.50 241. 7738 756.73 192.0850 351.06 374.3032 569.70 250.6042 756.80 192.0923 351.93 374.5527 583.19 257.2723 7 63. 94 195.8672 355.39 0.0000 584.27 246.5719 765.81 217.4386 356.01 397.5753 595.83 243.0461 7 66. 42 201. 4253 Page 4343 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 221. 8158 1002.74 307.4464 1678.03 0.0000 772. 60 0.0000 1004.73 294.4922 1690.97 10.4773 776.52 235.6014 1021.30 0.0000 1750.46 0.0000 777.92 234.6587 1025.87 0.0000 1764.49 17.0215 778.90 218.5950 1028.54 0.0000 1770.23 10.6506 783.70 217:9374 1037.84 240.0692 1771. 35 20.2408 785.37 233.2002 1038.76 0.0000 1791.20 0.0000 792.07 238.1543 1046.59 253.1845 1808.65 8.5864 794.95 251. 4372 1048.07 222.1985 1810.72 0.0000 795.86 250.4380 1049.04 215.1472 1836.06 15.1083 801.95 241.2588 1050.41 245.4756 810.06 242.0266 1063.66 242.9307 810.29 242.0537 1077.00 251.1182 810.45 242.0627 1077.34 245.7538 810.76 242.0989 1085.87 227.5209 815.77 240.9296 1093.63 257.8085 818.51 241.7367 1099.45 254.6503 832.01 257.2800 1112. 07 259. 6199. 834.85 266.3713 1112.84 259. 6724 835.71 251.0449 1115.54 240.5932 836.80 0.0000 1'120. 29 185.3730 846.75 0.0000 1120. 55 185.3855 846.77 225. 5571 1121.30 134.5315 856.80 258.5934 1129. 67 180.4285 860.56 257.8470 1131.51 0.0000 871.09 280.0464 1147.95 0.0000 873.19 255. 6962 1173.23 134.7452 875.33 0.0000 1177.95 134.5538 879.38 315.5977 1189.05 90.8582 880.51 301.1692 1204.77 69.8410 883:24 267.8441 1221. 41 65.4883 884.68 319.5697 1231. 02 49.7166 889.28 28 6. 4081* 1235.36 63.8662 894.76 319.6040 1238.28 46.0571 898.04 282.8040 1260.41 0.0000 900. 72 321.4252 -1271.87 40.7875 903.28 290.1080 1274.44 43.6641 911. 20 336.2036 1274.54 43.6641 912.08 297.8120 1291.59 39.0956 923.98 0.0000 1298.22 0.0000 926.50 343. 7191 1312 .11 38.3496 929 .11 323.5215 1332. 49 53.9731 937.49 325. 6116 1362.66 0.0000 944 .13 336.6597 1365.19 27.2139 946.00 372. 9688 1368.63 0.0000 949.00 330.3398 1384.29 25.3906 954.55 0.0000 1408.01 22.5943 962. 31 337.0367 1457.56 0.0000 964.08 314.7565 1460.82 17.9110 966 .17 299.4028 1489.16 20.0342 968. 97 296.7902 1505.03 22 .1195 983.53 281. 9971 1584.12 17.4036 984.45 0.0000 1596. 21 13.3444 996.26 282.0281 1620.50 12.3838 1001.03 245.9951 1621.92 10.3235 Page 4344 of 5809 Effective 3/25/2010 Radiochemistry Batch Checklist Revision 1 Effective March 2010 26-Sep-2016 _ . Product: !criteria: Yes No Sample Solids are less than or equal to 100 m11 for GAB. !VA Samples have been blank corrected (If required}. !VA-Blank correction renorted Included flf renulredl. If activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. ....---If greater than 10* MDA/ MDC, error Is 40% or less. llf *hA Mnll I ----le _,,m,. !Instrument source check Is within llmlts. J/ ITn,.trument bkn rh..rk Is within limits. Method RDL/ LLD has been met. v* If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, v If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 0%, 'SGG ;J A n n.a:.n' ,/£, Or meets the client's renulred RER accentance criteria. Tracer yield Is 15-125%
Carrier yield 25-1250/o, (Or meets the client's contract acceptance criteria). tJA-Method blank Is less than the RDL/ LLD. v frf <' t;oJ. nf IA ... nrtlulhll Sam Pie was run within hold time. v Samele was correctlv nreserved If reouired. A)('r Smears Taken for Radioactive batches. Nil-Method Spike and LCS are within 75-125% v !f nr the client's rontrart rrlt .. ria l No blank spaces on data forms. v All line outs Initialed and dated. 1 .. A -------Aux data Is correct. fl/A-Client Soecial reoulrements oaoe has been checked. V" Raw Data and I or saectrum are Included and nronerlv statused. v MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and v* "'" uo*lllo.I lur* *-flf JJP,. la ............ __ ................ , ..... ,,, r"!!ll.r.n i/ Batch Data Exceotlon Recarts (DERl comnleted If annllcable. v vGfLti:_ Batch Data Exception Reports (DER} second reviewed. / Olsoositlon verified to be "omnleted. Allouot co---rtlnn CA-nleted If r--.. 1-". NA Review sample historical results If avallable (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.1 u Primary Review Performed By: -IAJ :;/--\,, / ... -/61-Secondary Review Performed By: . / r, . Page 4345 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 03-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GAMMA SPECTROMETER DOE HASL 300, 4.5.2.3/Ga-01-R Solid Batch ID: Sample Numbers: 1596254 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Sample received and analyzed out of holding: 1. Reporting Results 405235061,062,063,064,065,066,067,068,069,' 070,071,072,073,074,075,076,077,078, 1203621365DUP Originator's Name: Data Validator/Group Leader: Tim Winters 03-0CT-16 Bryan Williams 03-0CT-16 Page 1 Page 4346 of 5809 DER Report No.: 1563729 Revision No.: 1 Type: Process Client Code: MJWC Gamma Spec Queue Sheet \.G.-to{-:s{tc,o 09/16/2016 Batch #:1596254 Analyst: MXRI Gamma LCS Isotope: Mixed Gamma LCS Code: Initials: H.:} Prep Date: __ Wet/ ry Hazard Sealing Dateffime Sample ID ID Type Code Client Matrix Collect Date Geometry ( 1 g F) Detector (if Applicable) 405235061-1 5.IB.R.2.2 SAMPLE MJWCOOl SOIL 144.233g q \'Z.. 405235062-1 5.2.A. R.1.2 SAMPLE MJWCOOl SOIL 146.441 g 405235063-1 5.L\.R.1.3 SAMPLE MJWCOOI SOIL 147.883 g 405235064-1 5.2.A.R.l.4 SAMPLE MJWCOOl SOIL 174.637 g 405235065-1 5.2A.R.2.3 SAMPLE MJWCOOI SOIL 147.836g 405235066-1 5.2.A.R.2.4 SAMPLE MJWCOOl SOIL 157.422 g 405235067-1 5.2A.R.6.2 SAMPLE MJWCOOI SOIL 158.21 g 405235068-1 5.2A.R.4.2 SAMPLE MJWCOOl SOIL 140.907 g 405235069-1 5.2.B.R.l.4 SAMPLE MJWCOOJ SOIL 156.084 g 405235070-1 5.2.B.R.3.2 SAMPLE MJWCOOI SOIL 145.32 g 405235071-1 5.2.B.R.4.2 SAMPLE M.JWCOOI SOIL 149.695 g 405235072-1 5.2.B.R.2.4 SAMPLE MJWCOOI SOIL 166.107 g 405235073-1 5.2.B.R.8.2 SAMPLE MJWCOOI SOIL 147.132 g I 40:>""235074-1 5.3.A.R. l.J SAMPLE MJWCOOI SOIL 169.068 g 405235075-1 5.4A.R.1.J SAMPLE MJWCOOl SOIL 151.411 g 405235076-1 5.4A:R.4.2 SAMPLE MJWCOOI SOIL 144.47 g 405235077-1 5.5A.R.l.J SAMPLE MJWCOOl SOIL 172.799 g 405235078-1 5.6A.R.l.3 SAMPLE MJWCOOI SOIL 156.072 g 1203621364-1 MB MB QC ACCOUNT SOIL 1203621365-1 DUP 5.IB.R.2.2(405235061) DUP QC ACCOUNT SOIL I 44.'L?,3 -1203621366-1 LCS LCS QC ACCOUNT SOIL ht;" GEL Laboratories LLC, Radiocl1einistry Division Data Reviewed By:

VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:54:36.57 ********************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date 14-DEC-2015 13:47:00 Acquisition date : 3-0CT-2016 05:52:51. Sample ID G405235061 Sample quantity : l.44233E+02 GRAM Detector name : GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 Ol:OIT:14.55 0.4% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 5 5 0 0 0 0 4 4 0 0 4 4 2 2 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 0 Energy 47.05* 63.50* 74.92 77.15 87.37 92.64* 129.70 144.40* 186.06* 209.70 238.52* 241.49 270.20 295.09* 299.97 304. 96 351.90* 356.36* 510.90* 583.44* 609.37* 623.21 723. 27 763,00 768.40 796.11 861.13 911. 42* 1001.94* 1120.51 1156.21 1305.58 1320.12 1332.48 Page 4348 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 34 10 168 242 56 75 19 29 86 21 330 70 43 194 43 23 302 19 56 112 203 33 67 19 38 32 19 85 19 58 21 17 5 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 141 165 176 142 225 225 117 125 116 89 77 71 71 30 25 21 38 29 24 29 29 31 42 30 20 14 11 8 8 17 4 2 5 3 1. 86 0.72 1. 23 0.98 1. 29 1. 85 1. 40 1. 38 0.97 1. 39 1.17 1. 43 1. 58 1.17 2.01 2.01 1. 30 1. 71 1. 74 1. 29 1. 26 5.67 11. 05 1. 83 1. 84 3. 96 2.54 1. 78 3.13 2.04 2.57 3.63 . 1. 29 1. 23 94.29 127.15 149.98 154.43 174.87 185.40 259.47 288.84 372 .12 419.38 476.98 482.93 540.33 590.08 599.84 609.83 703.68 712.60 1021. 62 1166. 72 1218.58 1246.28 1446.45 1525.94 1536.75 1592.18 1722.29 1822.93 2004.11 2241. 46 2312.95 2612.04 2641.15 2665.90 88 124 146 146 *170 170 253 283 367 415 473 473 535 585 595 595 697 697 1016 1161 1212 1237 1431 1518 1518 1583 1716 1818 1994 2232 2308 2608 2636 2661 10 9.48E-03 68.7 8 2.88E-03224.3 14 4.67E-02 15.0 14 6.73E-02 10.6 22 l.56E-02 44.6 22 2.09E-02 44.6 8 5.17E-03104.1 10 8.03E-03 75.5 10 2.38E-02 27.2 8 5.92E-03 79.9 14 9.16E-02 7.1 14 l.96E-02 23.7 9 1.20E-0.2 38.6 10 5.40E-02 9.0 21 1.20E-02 28.1 21 6.44E-03 53.2 19 8.39E-02 6.8 19 5.26E-03 58.2 13 1.56E-02 28.2 13 3.llE-02 14.2 13 5.64E-02 9.0 18 9.16E-03 43.5 31 1. 85E-02 32. 5 23 5.18E-03 55.1 23 1.06E-02 25.5 18 *9.02E-03 31.8 12 5.20E-03 43.4 11 2.35E-02 12.9 16 5.34E-03 41.7 17 1.61E-02 21.0 11 5.70E-03 30.9 10 4.74E-03 29.4 7 1.49E-03 81.9 7 1. 57E-03 68. 6 Fit 2.03E-01 4.08E+OO 4. 51E+OO 1.97E+OO 2.90E+OO 3.60E+OO Peak Search Report (continqed) Sample ID : G405235061 Pk It Energy Area Bkgnd 35 0 1460.95* 293 16 36 0 1587.68 19 0 37 0 1764.42 39 0 FWHM 1. 97 2.16 2.10 Acquisition date Page : 2 3-0CT-2016 05:52:51 Channel Left Pw cts/sec %Err Fit 2923.21 2916 16 8.15E-02 6.6 3177.11 3172 11 5.28E-03 22.9 3531. 2 6 3525 13 l.OBE-02 16.0 Flag: "*" = Peak area was modified by background subtraction Page 4349 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:54:39 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 14-DEC-2015 13:47:00 G405235061 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:52:51 144.23 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance. limit SOLID GAMMA20 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4350 of 5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214* PB-214 PB-214 PB-214 Line 242.00 143.76 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 86. 94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:14.55 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : G405235061 Acquisition date 3-0CT-2016 05:52:.51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.312E+OO 1.049E+Ol l.049E+Ol 13.27 OK RH-106 621. 93 9.93* 2.582E+OO 6.971E-01 1.205E+OO 87.04 OK 1050.41 1. 56 1. 721E+OO. Line Not Found Absent RU-106 ' 621. 93 9.93* 2.582E+00 6.971E-01 l.205E+OO 87.04 OK 1050.41 1. 56 1.721E+OO Line Not Found Absent CD-109 88.03 3.70* 6.851E+OO 2.608E-01 4.055E-01 488.47 OK SN-126 64.28 9.60 4.813E+00 l.467E-01 l.467E-01 448.65 OK 86.94 8.90 6.851E+OO 1.084E-01 1.084E-01 488.47 OK 87.57 37.00* 6.851E+OO 2.608E-02 2.608E-02 488.47 OK CE-141 145.44 48.29* 7.360E+OO l.879E-02 9.847E+OO 411. 67 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.719E+OO 2.641E-01 2.641E-01 28.47 OK 860.56 12.50 2.0lOE+OO 3.924E-01 3.924E-01 86.73 OK PB-210 46.54 4.25* 2.063E+OO 2.605E+00 2.671E+OO 137. 44 OK PB-212 74.82 10.28 6.005E+OO 1.057E+00 1.057E+OO 51. 32 OK 77 .11 17.10 6.187E+OO 1. 477E+OO 1.477E+OO 21.12 OK 238.63 43.60* 5.554E+OO 8.023E-01 8.023E-01 14.23 OK 300.09 3.30 4.648E+OO 1.625E+OO 1.625E+OO 56.28 OK BI-214 609.32 45.49* 2.627E+OO . 9. 221E-01 9.224E-01 18.09 OK 1120. 29 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 1..106E+OO 1.131E+OO 1.132E+OO 32.03 OK PB-214 74.82 5.80 5. 996E+OO Line Not Found <<INT Reject 77 .11 9.70 6.187E+OO 2.603E+OO 2.604E+OO 21.12 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.503E+OO 1.040E+OO 1.040E+OO 47.31 OK 295.22 18.42 4.710E+OO 1.296E+OO 1.297E+OO 18.01 OK 351.93 35.60* 4.084E+OO 1.185E+OO l.185E+00 13. 60 *OK RN-222 609.32 45.49* 2.627E+OO 9.221E-01 9.224E-01 18. 09 OK 1120.29 14.92 1. 635E+ci0 l.218E+00 1.218E+OO 41. 93 OK 1764.49 15.30 1.106E+OO 1.131E+OO 1.132E+OO 32.03 OK RA-226 609.32 45.49* 2.627E+OO 9. 221E-01 9.224E-01 18.09 OK 1120.29 14.92 1.635E+OO 1.218E+OO l.218E+00 41. 93 OK 1764.49 15.30 1.106E+OO 1.131E+OO l .132E+00 32.03 OK TH-228 74.82 10.28 6.005E+OO 1.057E+OO l.057E+OO 51. 32 OK 77 .11 17.10 6.187E+OO 1.477E+OO l.477E+OO 21.12 OK 238.63 43.60* 5.554E+OO 8.023E-01 8.023E-01 14.23 OK 300.09 3.30 4.648E+OO 1.625E+OO 1.625E+OO 56.28 OK TH-230 609.32 45.49* 2.627E+OO 9.221E-01 9. 221E-01 18. 09 OK 1120.29 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 t.106E+OO 1.131E+OO. 1.131E+OO 32.03 OK PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5 .. 35* 4.648E+OO 1.003E+00 1.003E+OO 56.28 OK TH-234 63.29 3.70* 4.813E+OO 3.806E-01 3.806E-01 448.65 OK 92.59 4.23 7.094E+OO 1. 596E+OO 1. 596E+OO 89.29 OK U-234 609.32 45.49* 2.627E+OO 9.221E-01 9.221E-01 18.09 OK 1120.29 14.92 1.635E+OO l.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 1.106E+OO 1.131E+OO 1.131E+OO 32.03 OK U-235 89.96 3.47 6.978E+OO Line Not Found Absent 93.35 5.60 7.094E+OO 1.205E+OO 1. 205E+OO 89.29 OK Page 4351of5809 Nuclide Line Activity Report (continued) Sample ID : G405235061 Acquisition date Nuclide Type: Nuclide U-238 AM-243 ANH-511 Energy 143.76 163.33 185.72 205.31 63.29 92.59 43.53 74.66 511. 00 %Abn 10. 96* 5.08 57.20 *5.01 3.70* 4.23 5.90 67.20* 100.00* Flag: "*" = Page 4352 o.f 5809 Uncorrected Decay Corr %Eff pCi/GRAM pCi7GRAM 7.370E+OO Line Not Found 7.024E+OO Line Not Found 6.562E+OO L 374E-01 1.374E-01 6.171E+OO Line Not Found 4.813E+OO 3.806E-01 3.806E-01 7.094E+OO 1. 596E+OO 1. 596E+OO 1. 315E+OO Line Not Found 6.005E+OO 1.618E-01 1.618E-01 3.020E+OO 1.028E-01 1.028E-01 Page : 3 3-0CT-2016 05:52:51 2-Sigma %Error Status <<INT Reject Absent 54.37 OK Absent 448.65 OK 89.29 OK Absent 51. 32 OK 56.43 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:54:41.50 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l *
Acquisition date 3-0CT-2016 05:52:51 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.55 Half life ratio ***** *
Sample date 14-DEC-2015 13:47:00 Analyst initials: MXRl *
Sample ID G405235061 Sample Quantity l.4423E+02 GRAM *
Batch Number 1596254 Wet Wei,ght 0. 00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.049E+Ol 1.365E+OO RH-106 l.205E+OO 1.028E+OO RU-106 1.205E+OO 1.028E+OO CD-109 4.055E-01 1.941E+OO SN-126 2.608E-02 l.249E-01 CE-141 9.847E+OO 3.973E+Ol TL-208 2. 641E-01 7.368E-02 PB-210 2.671E+OO 3.598E+OO PB-212 8.023E-01 1.119E-01 BI-214 9.224E-01 1.635E-01 PB-214 1.185E+OO 1.580E-01 RN-222 9.224E-01 l.635E-01 RA-226 9.224E-01 1.635E-01 TH-228 8.023E-01 1.119E-01 TH-230 9.221E-01 l.635E-01 PA-231 1.003E+OO 5.530E-01 TH-234 3.806E-01 1.673E+OO U-234 9.221E-01 1.635E-01 U-235 2.202E-01 3.258E-01 U-238 3.806E-01 1.673E+OO AM-243 l.618E-01 8.137E-02 ANH-511 1. 028E-01 5.685E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4353 of 5809 Key-Line Activity (pCi/GRAM 2.103E+OO 2.263E-02 O.OOOE+OO 3.341E-03 1.455E-01 O.OOOE+OO O.OOOE+OO 1.118E-02 K.L. Cnt Uncert ( 1. 96-sigma) 8.541E+OO 3.835E-02 1. 960E+41 2. llOE-02 3.348E-01 1.073E+04 2.904E+02 5.531E-02 MDA (pCi/GRAM 6.736E-01 8.265E-01 8.265E-01 1.693E+OO l.092E-01 3.272E+Ol 5.153E-02 2.670E+OO 9.156E-02 l.144E-01 1.019E-01 l.144E-01 l.144E-01 9.156E-02 l.143E-01 5.207E-01 1. 517E+OO 1.143E-01 3.296E-01 l.517E+OO 7. llOE-02 4.379E-02 MDA (pCi/GRAM 1.735E+Ol 8.532E-02 O.OOOE+OO 5.056E-02 6.793E-01 O.OOOE+OO O.OOOE+OO 1.083E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 l.252E-01 4.148E-01 8.212E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.944E-02 4.150E-02 7.234E-02 NOT IDENT. C0-58 -l.763E-01 4.682E-01 8.355E-01 NOT IDENT. FE-59 l.482E+OO 6.619E+OO 1.333E+Ol NOT IDENT. C0-60 2.241E-02 3.014E-02 7.007E-02 FAIL ABUN ZN-65 5.364E-02 l.523E-01 2.933E-01 NOT IDENT. GE-68 -l.261E-01 1. 861E+OO 3.752E+OO NOT IDENT. AS-73 -5.461E-01 4.568E+OO 8.583E+OO NOT IDENT. AS-74 O.OOOE+OO 4.121E+03 O.OOOE+OO SHORT HLIF SE-75 -7.514E-03 .1. 710E-01 3.196E-01 NOT IDENT. BR-77 O.OOOE+OO 3.342E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.979E+02 0.000E+OO SHORT HLIF RB-83 -2.305E-01 5.087E-01 9.239E-01 NOT IDENT. KR-85 5 .112E+OO 5.638E+OO 1.141E+Ol NOT IDENT. SR-85 5.040E-01 5.581E-01 1.129E+OO NOT IDENT. RB-86 O.OOOE+OO 1. 716E+04 O.OOOE+OO SHORT HLIF Y-88 3.545E-02 2.028E-01 4.448E-01 NOT IDENT. Y--91 2.840E+02 4.399E+02 9.527E+02 NOT IDENT. NB-94 l.661E-02 3.025E-02 6.099E-02 NOT IDENT. NB-95 2.592E-02 7.292E-01 1.379E+OO NOT IDENT. NB-95M 8. 731E-01 2.068E+OO 3.784E+OO NOT IDENT. ZR-95 9.818E-01 1.218E+OO 2.454E+OO FAIL ABUN NB-97 0.000E+OO 1. 259E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 68 9E+4 l O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.388E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 2.804E-03 3.232E-02 5.442E-02 NOT I DENT'. RH-102 -2.559E-02 5.229E-02 9.278E-02 NOT IDENT. RU-103 -2.462E-02 4.020E+OO 7.849E+OO FAIL ABUN AG-108M 7.692E-04 2.295E-02 4.483E-02 FAIL ABUN AG-llOM -3. 411E-02 8.526E-02 1.504E-01 F-AIL ABUN SN-113 6.533E-02 1.539E-01 3.220E-01 NOT IDENT. CD-115 O.OOOE+OO 3.473E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.443E+04 O.OOOE+OO SHORT HLIF TE-123M -3. 991E-02 l.152E-01 2.000E-01 NOT IDENT. SB-124 -8.677E-01 1. 251E+OO 2.061E+00 FAIL ABUN SB-125 6.802E-02 8.319E-02 l.778E-01 NOT IDENT. TE-125M 3. 041E+Ol 2.320E+02 4.273E+02 NOT IDENT. I-126 0.000E+OO 5.188E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.290E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.595E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.524E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.028E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.026E+25 O.OOOE+OO SHORT HLIF BA-133 4.539E-02 5.178E-02 6.865E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 7.700E-02 9.666E-02 FAIL ABUN CS-135 4.088E-02 1.409E-01 2.537E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 1.572E+05 O.OOOE+OO SHORT HLIF BA-137M 2.377E-02 3. 696E-02 7.412E-02 NOT IDENT. CS-137 2. 511E-02 3.904E-02 7.830E-02 NOT IDENT. CE-139 -6.957E-03 9. 511E-02 l.694E-01 NOT IDENT. BA-140 O.OOOE+OO 6.666E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.283E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO l.281E+41 O.OOOE+OO SHORT HLIF CE-144 -2.494E-02 2.867E-01 5.177E-01 NOT IDENT. PM-144 -4.298E-03 4.781E-02 8.976E-02 NOT IDENT. PR-144 -3.856E-01 4.137E+OO 7.764E+00 NOT IDENT. PM-146 -3. 211E-03 3.908E-02 7.458E-02 NOT IDENT. ND-147 O.OOOE+OO 1. 810E+07 O.OOOE+OO SHORT HLIF PM-147 1.414E+02 7.047E+02 1.308E+03 NOT IDENT. PM-149 O.OOOE+OO 5.532E+39 0.000E+OO SHORT HLIF EU-150 -l.318E-02 2.075E-02 3.774E-02 FAIL ABUN EU-152 3.094E.:.02 7.822E-02 1.583E-01 NOT I DENT .. GD-153 -5.501E-02 1.629E-01 2.674E-01 NOT IDENT. EU-154 3.306E-02 9.801E-02 2.084E-01 FAIL ABUN EU-155 7. 278E'-02 9. 118E-02 1.782E-01 FAIL ABUN TB-160 4.628E-01 1. 511E+OO 3.047E+OO FAIL ABUN H0-166M -7.262E-03 4. 619E-.02 8.655E-02 NOT IDENT. TM-171 -3.157E+OO l.160E+Ol 2.151E+Ol NOT IDENT. HF-172 -2 .114E-02 2.275E-01 3.755E-01 FAIL ABUN LU-172 l.170E-02 8.097E-02 l.618E-01 FAIL ABUN LU-176 -1.219E-03 1. 764E-02 3.133E-02 FAIL ABUN HF-181 1. 071E+OO 3.102E+OO 6.336E+00 NOT IDENT. TA-182 -2.480E-01 7.955E-01 1.499E+OO FAIL ABUN RE-183 6.950E-01 1. 742E+OO 3.381E+OO NOT IDENT. Page 4354 of 5809 RE-184 1.265E+Ol 2.306E+Ol 4.817E+Ol NOT IDENT. W-188 2.977E+Ol 8.254E+Ol 1.544E+02 FAIL ABUN IR-192 9. 2 61E-02 3.407E-Ol 6.881E-01 FAIL ABUN HG-203 -1.126E+OO 1.852E+OO 3.412E+OO NOT IDENT. BI-207 9.041E-03 4.043E-02 8.457E-02 FAIL ABUN BI-211 O.OOOE+OO 4.353E-01 8.295E-01 FAIL ABUN PB-211 -6.994E-02 5.213E-01 1.002E+OO NOT IDENT. BI-212 8.436E-01 5.042E-01 1.119E+OO NOT IDENT. RN-219 4.697E-02 3.294E-01 6.471E-01 FAIL ABUN RA-223 -1. 475E-01 4.706E-01 8.903E-01 FAIL ABUN RA-224 O.OOOE+OO 8.524E-01 1.364E+OO FAIL ABUN AC-227 -1.198E-01 1.890E-01 3.496E-01 FAIL ABUN TH-227 -1.198E-01 1.890E-01 3.496E-01 FAIL ABUN AC-228 O.OOOE+OO 2.267E-01 4.972E-01

FAIL ABUN RA-228 O.OOOE+OO 2.267E-01 4.972E-01 FAIL ABUN TH-229 -l.695E-01 3.839E-01 7.320E-01 FAIL ABUN TH-231 -1. 475E-01 4.706E-01 8.903E-01 FAIL ABUN TH-232 O.OOOE+OO 2.267E-01 4.972E-01 FAIL ABUN PA-233 -1.104E-02 4.417E-02 8.476E-02 FAIL ABUN PA-234 2. 651E-02 1.818E-01 3.933E-01 FAIL ABUN PA-234M 6.646E+OO 5.427E+OO 7.908E+OO FAIL ABUN NP-237 -l.104E-02 4.417E-02 8.476E-02 FAIL ABUN NP-238 O.OOOE+OO 6.108E+40 O.OOOE+OO SHORT HLIF NP-239 -7.460E-02 2.160E-01 3.816E-01 NOT IDENT. PU-239 2.427E+02 4.952E+02 5.470E+02 FAIL ABUN AM-241 l.781E-02 9.076E-02 l.726E-01 NOT IDENT. CM-243 -9.227E-03 8.586E*-02 1.559E-01 NOT IDENT. BK-247' -3.439E-03 6.820E-02 1.193E-01 NOT IDENT. CM-247 9.215E-03 2.991E-02 5.985E-02 NOT IDENT. CF-249 -7. 496E-03 2.820E-02 5.354E-02 NOT IDENT. CF-251 5.177E-03 9.199E-02 1.831E-01 NOT IDENT. Page 4355 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:54:37.31 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 282 10.66* 1. 312E+OO 1.049E+Ol l.049E+Ol 13.27 RH-106 621.93 34 9.93* 2.582E+OO 6. 971E-01 1.205E+OO 87.04 1050.41 ------1. 56 1. 721E+OO ------Line Not Found ------RU-106 621.93 34 9.93* 2.582E+OO 6.971E-01 1.205E+OO 87.04 1050.41 ------1. 56 1. 721E+OO ------Line Not Found ------CD-109 88.03 69 3.70* 6.851E+OO 1.412E+OO 2.195E+OO 89.18 SN-126 64.28 13 9.60 4.813E+OO 1.467E-01 l.467E-01 448.65 86.94 69 8.90 6.851E+OO 5.870E-01 5.870E-01 89.18 87.57 69 37.00* 6. 851E+OO l.412E-01 l.412E-01 89.18 CE-141 145.44 34 48.29* 7.360E+OO 4.997E-02 2.619E+Ol 151.00 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 117 85.00* 2. 719E+OO 2. 641E-01 2. 641E-01 28.47 860.56 19 12.50 2.0lOE+OO 3.924E-01 3.924E-01 86.73 PB-210 46.54 44 4.25* 2.063E+OO 2.605E+00 2. 671E+OO 137.44 BI-211 72. 87 ------1. 23 5.823E+00 ------Line Not Found ------351.06 331 12.92* 4.084E+OO 3.265E+OO 3.265E+OO 13.60 PB-212 74.82 209 10.28 6.005E+OO 1. 762E+OO 1. 762E+00 30.05 77 .11 300 17.10 6.187E+00 l.477E+00 1.477E+OO 21.12 238.63 373 43.60*: 5.554E+OO 8.023E-01 8.023E-01 14.23 300.09 48 3.30 4.648E+OO l.625E+OO 1. 625E+00 56.28 BI-214 *609.32 212 45.49* 2.627E+OO 9.221E-01 9.224E-01 18.09 1120.29 57 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 1764.49. 37 15.30 l.106E+00 1.131E+OO 1.132E+OO 32.03 PB-214 74.82 209 5.80 6.005E+00 3.123E+OO 3.124E+OO 30.05 77 .11 300 9.70 6.187E+OO 2.603E+00 2.604E+00 21.12 87.09 69 3.41 6.851E+OO l.532E+OO 1.533E+OO 89.18 242.00 80 7.25 5.503E+OO 1.040E+OO 1.040E+OO 47.31 295.22 216 18.42 4. 710E+OO l.296E+00 1. 297E+OO 18.01 351. 93 331 35.60* 4.084E+OO l.185E+00 1.185E+OO 13. 60 RN-222 609.32 212 45.49* 2.627E+OO 9.221E-01 9.224E-01 18.09 1120.29 57 14.92 1. 635E+OO 1.218E+OO 1.218E+OO 41. 93 1764.49 37 15.30 1.106E+OO l.131E+OO 1.132E+OO 32.03 RA-224 240.99 80 4.10* 5.503E+OO 1.838E+OO 1.838E+OO 47.31 RA-226 609.32 212 45.49* 2.627E+OO 9.221E-01 9.224E-01 18.09 1120.29 57 14.92 l.635E+OO 1.218E+OO 1.218E+OO 41. 93 1764.49 37 15.30 l.106E+OO 1.131E+OO 1.132E+OO 32.03 TH-228 74.82 209 10.28 6.005E+00 1.762E+OO 1.762E+OO 30.05 77 .11 300 17.10 6.187E+00 1. 477E+00 1. 477E+OO 21.12 238.63 373 43.60* 5.554E+00 8.023E-01 8.023E-01 14.23 300 :09 48 3.30 4.648E+OO 1.625E+OO 1.625E+OO 56.28 TH-230 609.32 212 45.49* 2.627E+OO 9. 221E-01 9.221E-01 18.09 1120.29 57 14.92 l.635E+00 l.218E+OO l.218E+00 41. 93 1764.49 37 15.30 l.106E+OO 1.131E+OO 1.131E+OO 32.03 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 48 5.35* 4.648E+OO 1.003E+OO 1.b03E+OO 56.28 TH-234 63.29 13 3.70* 4.813E+OO 3.806E-01 3.806E-01 448.65 92.59 92 4.23 7.094E+OO 1. 596E+OO 1. 596E+OO 89.29 Page 4356 of 5809 Nuclide Line Activity Report (continued)* Sample ID : G405235061 Acquisition date Page : 2 3-0CT-2016 05:52:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error U-234 609.32 212 45.49* 2.627E+OO 9.221E-01 9.221E-01 18.09 1120.29 57 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 1764.49 37 15.30 1.106E+OO 1.131E+OO 1.131E+OO 32.03 U-235 89. 96 ------3.47 6.978E+OO ------Line Not Found ------93.35 92 5.60 7.094E+OO 1. 205E+OO 1.205E+OO 89.29 143.76 34 10.96* 7.360E+OO 2.202E-01 2.202E-01 151. 00 163.33 ------5.08 7.024E+OO ------Line Not Found ------185. 72 99 57.20 6.562E+OO 1. 374E-01 l.374E-01 54.37 205.31 ------5.01 6.171E+OO ------Line Not Found ------U-238 63.29 13 3.70* 4.813E+OO 3.806E-01 3.806E-01 448.65 92.59 92 4.23 7.094E+OO 1. 596E+OO 1. 596E+OO 89.29 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 209 67.20* 6.005E+OO 2. 696E-01 2. 696E-01 30.05 ANH-5ll 511. 00 60 100.00* 3.020E+OO l.028E-01 1.028E-01 56.43 Flag: "*" Key line Page 4357 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235061 Acquisition date 3-0CT-2016 05:52:51 Total number of lines in spectrum 37 Number of unidentified lines 5 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 RH-106 RU-106 CD-109 SN-126 CE-141 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 371. 80D 371. 80D 461. 40D 2.30E+05Y 32. 510 1.41E+10Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600. DOY . 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1.41E+10Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 73 1. 73 1. 55 1. 00 524. 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 049E+Ol 6.971E-01 6.971E-01 l.412E+OO 1. 412E-01 4.997E-02 2.641E-01 2.605E+OO 3.265E+OO 8.023E-01 9.221E-01 1.185E+OO 9. 221E-01 1.838E+OO 9.221E-01 8. 023E-01' 9. 221E-01 1.003E+OO 3.806E-01 9.221E-01 2.202E-01 3.806E-01 2. 696E-01 1.028E-01 3.122E+Ol 3.122E+Ol Decay Corr pCi/GRAM 1.049E+Ol 1.205E+OO 1.205E+OO 2.195E+OO l.412E-01 2.619E+Ol 2.641E-01 2. 671E+OO 3.265E+00 8.023E-01 9.224E-01 1.185E+OO 9.224E-01 1.838E+OO 9.224E-01 8.023E-01 9. 221E-01 1.003E+OO .3. 806E-01 9. 221E-01 2.202E-01 3.806E-01 2.696E-01 l.028E-01 5.923E+Ol 5.923k+o1 86.49% Decay Corr 2-Sigma Error 0.139E+Ol l.049E+OCi 1.049E+OO 1.957E+OO l.259E-01 3.955E+Ol 0.752E-01 3.671E+OO 0.444E+OO 1.142E-01 1.669E-01 0.161E+OO l.669E-01 0.870E+OO l.669E-01 1.142E-01 1.668E-01 0.564E+OO 17. 08E"'-01 1.668E-01 3.324E-01 17.08E-01 0.810E-01 0.580E-01 "M" Manually accepted 2-Sigma .%Error 13.27 87.04 87.04 89.18 89.18 151.00 28.47 137.44 13. 60 14.23 18.09 13.60 18.09 47.31 18.09 14.23 18.09 56.28 448.65 18.09 151. 00 448.65 30.05 56.43 Flags: "K" = Keyline not found "E" =-Manually edited "A" = Nuclide specific ab_n. limit Page 4358 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235061 Acquisition date : 3-0CT-2016 05:52:51 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 129.70 22 140 1. 40 259.47 253 8 5.17E-03 **** 7.53E+OO T 0 209.70 24 102 1. 39 419.38 415 8 5.92E-03 **** 6.08E+OO T 0 270.20 48 79 1. 58 540.33 535 9 l.20E-02 77.1 5.05E+OO T 4 304. 96 26 24 2.01 609.83 595 21 6.44E-03 **** 4.59E+OO T 2 356.36 21 32 1. 71 712.60 697 19 5.26E-03 **** 4.04E+OO T 0 723. 27 69 43 11. 05 1446.45 1431 31 *1. 85E-02 64.9 2.30E+OO T 1 763.00 19 31 1. 83 1525.94 1518 23 5. l8E:....03 **** 2.21E+OO T 1 768.40 39 21 1. 84 1536.75 1518 23 1. 06E-02 51.1 2.19E+OO 0 7*96.11 33 14 3. 96 1592.18 1583 18 9.02E-03 63.6 2.14E+OO T 0 911. 42 85 8 1. 78 1822.93 1818 11 2.35E-02 25.9 1.92E+OO T 0 1001.94 19 8 3.13 2004 .11 1994 16 5.34E-03 83.3 1. 79E+OO T 0 1156. 21 20 4 2.57 2312.95 2308 11 5.70E-03 61. 7 1.59E+OO 0 1305.58 17 2 3.63 2612.04 2608 10 4.74E-03 58.8 1. 44E+oo* 0 1320.12 5 5 1. 29 2641.15 2636 7 1.49E-03 **** 1. 43E+OO 0 1332.48 5 3 1. 23 2665.90 2661 7 l.57E-03 **** 1. 42E+OO T 0 1587.68 18 0 2.16 3177.11 3172 11 5.28E....:03 45.9 1.22E+OO Flags: "T" = Tentatively associated Page 4359 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:54:54.27 *******************************************************************************
GEL Laboratories LLC *
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Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l *
Acquisition date 3-0CT-2016 05:52:51 Sensitivity 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.55 Half life ratio : ***** *
Sample date 14-DEC-2015 13:47:00 Nuclide Library : SOLID *
Sample ID G405235061 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : l.4423E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 30-JUN-2'016 06: 52: 39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;'15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 RH-106 RU-106 CD-109 SN-126 CE-1'41 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.863E-01 3.648E-01 3.648E-01 8.009E-01 5.169E-02 1. 52 6E+Ol 2.265E-02 1.242E+OO 4.275E-02 5 .116E-02 4.594E-02 5.116E-02 5 .116E-02 4.275E-02 5 .114E-02 2.308E-01 7.161E-01 5 .114E-02 1.557E-01 7.161E-01 3.369E-02 1.950E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4360 of 5809 Le (rci/GRAM 7.678E+OO 3.670E-02 O.OOOE+OO l.875E-02 2.983E-01 0.000E+OO O.OOOE+OO 4.749E-02 3.616E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH....:101 RH-102 RU-103 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 4361 of 5809 O.OOOE+OO 3.375E-02 3.573E-01 5.929E+OO 2.949E-02 1. 2 69E-01 1.598E+OO 4.012E+OO O.OOOE+OO 1. 465E-01 O.OOOE+OO 0.000E+OO 4.047E-01 5.123E+OO 5.068E-01 O.OOOE+OO 1.775E-01 4.190E+02 2.744E-02 6 .112E-01 1. 766E+OO 1.084E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.550E-02 4.055E-02 3.465E+OO 2.009E-02 6.390E-02 1.435E-01 O.OOOE+OO O.OOOE+OO 9.318E-02 6.516E-01 8.036E-02 2.010E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.127E-02 O.OOOE+OO 4.320E-02 1.179E-01 O.OOOE+OO O.OOOE+OO 3.376E-02 3.566E-02 7.890E-02 O.OOOE+OO 0. OOOE.+00 O.OOOE+OO 2.406E-01 3.954E-02 3.420E+OO 3.358E-02 O.OOOE+OO 6 .116E+02 O.OOOE+OO 1. 706E-02 7.229E-02 l.254E-01 8.953E-02

8.378E-02 1.323E+OO 3.757E-02 1. 006E+Ol 1. 7 60E-01 7.180E-02 1. 396E-02 2.822E+OO 6.474E-01 1.591E+OO 2.104E+Ol SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL. ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT.IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT .. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 RA-224 AC-227 TH-227 AC-228 RA-228 TH-229 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4362 of 5809 7.014E+Ol 3.128E-01 1.562E+OO 3.660E-02 4 .. 012E-01 4.481E-01 5.129E-01 2.935E-01 4.033E-01 6.496E-01 1. 601E-01 1.601E-01 2 .. 343E-01 2.343E-01 3.399E-01 4.033E-01 2.343E-01 3.817E-02 1. 648E-01 3.480E+OO 3.817E-02 0.000E+OO 1. 784E-01 2.579E+02 8.140E-02 7.306E-02 5.489E-02. 2.717E-02 2.385E-02 8. 521E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL AB.UN FAIL ABUN FAIL ABUN

SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. -NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06: 54: 59. 6*6 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l * *Acquisition date 3-0CT-2016 05:52:51 Sensitivity : 3.000 *
Detector ID GAM20 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:14.55 Half life ratio : ***** *
Sample date 14-DEC-2015 13:47:00 Nuclide Library : SOLID *
Sample ID G405235061 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : 1.4423E+02 GRAM * * *Quantity Err(%) : 1.3866E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.049E+Ol 1.471E+00 RH-106 1.205E+OO 1. 031E+OO RU-106 1.205E+OO 1.031E+OO CD-109 4.084E-01 1.954E+OO SN-126 2.627E-02 1.257E-01 CE-141 9.847E+OO 3.975E+Ol TL-208 2. 641E-01 7.453E-02 PB-210 2.671E+OO 3.604E+OO PB-212 8.023E-01 1.197E-01 BI-214 9.224E-01 1.682E-01 PB-21.4 l.185E+OO l.655E-01 RN-222 9.224E-01 l.682E-01 RA-226 9.224E-01 1.682E-01 TH-228 8.023E-01 1.197E-01 TH-230 9. 221E-01 1.682E-01 PA-231 1.003E+OO 5.929E-01 TH-234 3.806E-01 1.675E+OO U-234 9. 221E-01 l.682E-01 U-235 2.202E-01 3.260E-01 U-238 3.806E-01 1.675E+OO AM-243 1.619E-01 8.306E-02 ANH-511 1.028E-Ol 5.701E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 . SC-46 V-48 CR-51 MN-54 Page 4363 of 5809 Key-Line Activity (pCi/GRAM 2.103E+OO 2.263E-02 1.000E+41 3. 341E-03 l.455E-01 -9.514E+02 3.303E+Ol 1.118E-02 K.L Act error ( 1. 96-sigma) 8.542E+OO 3.836E-02 3.879E+41 2. lllE-02 3.349E-01 1.073E+04 2.904E+02 5.532E-02 TPU ( 1. 96-sigma) 1.471E+OO 1. 031E+OO 1. 031E+OO 1.954E+OO 1.257E-01 3.975E+Ol 7.453E-02 3.604E+OO l.197E-01 l.682E-01 l.655E-01 1.682E-01 1.682E-01 l.197E-01 1.682E-01 5.929E-01 1. 675E+OO l.682E-01 3.26.0E-01 1.675E+OO 8.306E-02 5.701E-02 TPU (1. 96-sigma) 8.594E+OO 3. 969E-02 O.OOOE+OO 2.116E-02 3.412E-01 1.074E+04 2.908E+02 5.555E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT . FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.252E-Ol 4.148E-01 4.187E-01 NOT IDENT. MN-56 1.000E+41 3.350E+41 O.OOOE+OO SHORT HLIF C0-57 -1.944E-02 4.151E-02 4.243E-02 NOT IDENT. C0-58 -l.763E-01 4.682E-01 4.749E-01 NOT IDENT. FE-59 l.482E+OO 6.620E+OO 6.653E+OO NOT IDENT. C0-60 2.241E-02 3.015E-02 3*.180E-02 FAIL ABUN ZN-65 5.364E-02 1.523E-01 l.542E-01 NOT IDENT. GE-68 -1.261E-01 1. 861E+OO l.862E+OO NOT IDENT. AS-73 -5.461E-01 4.569E+OO 4.576E+OO NOT IDENT. AS-74 1. 281E+02 4 .121E+o3 4.122E+03 SHORT HLIF SE-75 -7.514E-03 1.710E-01 1. 711E-01 NOT IDENT. BR-77 2.395E+37 2.031E+38 O.OOOE+OO SHORT HLIF SR-82 -3.985E+02 4.983E+02 5.296E+02 SHORT HLIF RB-83 -2.305E-01 5.097E-01 5.202E-01 NOT IDENT. KR-85 5 .112E+OO 5.642E+OO 6.094E+OO NOT IDENT. SR-85 5.040E-01 5.584E-01 6.029E-01 NOT IDENT. RB-86 -5.600E+03 . 1. 716E+04 l.735E+04 SHORT HLIF Y-88 3.545E-02 2.028E-01 2.034E-01 NOT IDENT. Y-91 2.840E+02 4.401E+02 4.583E+02 NOT IDENT. NB-94 1.661E-02 3.025E-02 3 .117E-02 NOT IDENT. NB-95 2.592E-02 7.292E-01 7.293E-01 NOT IDENT. NB-95M 8.731E-01 2.069E+OO 2.106E+OO NOT IDENT. ZR-95 9.818E-01 l.219E+OO l.297E+OO FAIL ABUN NB-97 1. OOOE+41 l.260E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.689E+41 O.OOOE+OO SHORT HLIF M0-99 -1.627E+30 3.388E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.919E+41 O.OOOE+oo SHORT HLIF RH-101 2.804E-03 3.232E-02 3.235E-02 NOT IDENT. RH-102 -2.559E-02 5.233E-02 5.359E-02 NOT IDENT. RU-103 -2.462E-02 4.020E+OO 4.020E+00 FAIL ABUN AG-108M 7.692E-04 2.295E-02 2.295E-02 FAIL ABUN AG-llOM -3. 411E-02 8.528E-02 8.665E-02 FAIL ABUN SN-113 6.533E-02 1.540E-01 l.568E-01 NOT IDENT. CD-115 -1.109E+38 3.478E+38 O.OOOE+OO SHORT HLIF SN-117M -l.240E+04 6.445E+04 6.469E+04 SHORT HLIF TE-123M -3.991E-02 l.153E-01 l.167E-01 NOT IDENT. SB-124 -8.677E-01 l.252E+OO 1. 311E+OO FAIL ABUN SB-125 6.802E-02 8.323E-02 8.870E-02 NOT IDENT. TE-125M 3. 041E+Ol 2.320E+02 2.324E+02 NOT IDENT. I-126 2.887E+05 5.203E+05 5.363E+05 SHORT HLIF SB-126 -2.392E+05 6.305E+05 6.397E+05 SHORT HLIF SB-127 -3.615E+21 8.197E+21 0.000E+OO SHORT HLIF I-131 4.626E+07 2.524E+09 2.524E+09 SHORT HLIF I-132 -1. OOOE+41 l.813E+42 O.OOOE+OO SHORT HLIF TE-132 5.459E+25 8.315E+25 O.OOOE+OO SHORT HLIF BA-133 4.539E-02 5 .181E-02 5. 571E-02 FAIL ABUN I-133 -l.000E+41 6.569E+41 O.OOOE+OO SHORT HLIF. CS-134 1.235E-01 7. 718E-02 9.516E-02 FAIL ABUN GS-135 4.088E-02 l.409E-01 1. 421E-01 NOT IDENT. I-135 1. OOOE+41 7.522E+41 O.OOOE+OO SHORT HLIF CS-136 5.635E+04 l.573E+05 l.594E+05 SHORT HLIF BA-137M 2.377E-02 3.697E-02 3.850E-02 NOT IDENT. CS-137 2. 511E-02 3.906E-02 4.067E-02 NOT IDENT. CE-139 -6.957E-03 9.512E-02 9.517E-02 NOT IDENT. BA-140 -1.382E+05 '6. 667E+05 6. 696E+05 SHORT HLIF LA-140 -4.039E+04 2.283E+05 2.291E+05 SHORT HLIF CE-143 l.000E+41 1.284E+41 O.OOOE+OO SHORT HLIF CE-144 -2.494E-02 2.867E-01 2.869E-01 NOT IDENT. PM-144 -4.298E-03 4.781E-02 4.785E-02 NOT IDENT. PR-144 -3.856E-01 4.137E+OO 4 .141E+OO NOT IDENT. PM-146 -3. 211E-03 3.909E-02 3. 911E-02 NOT IDENT. ND-147 8.346E+06 1. 811E+07 1.850E+07 SHORT HLIF PM-147 1.414E+02 7.047E+02 7.076E+02 NOT IDENT. PM-149 -1. 701E+39 5.545E+39 O.OOOE+OO SHORT HLIF EU-150 -l.318E-02 2.076E-02 2.159E-0,2 FAIL ABUN EU-152 3.094E-02 7.824E-02 7.947E-02 NOT IDENT. GD-153 -5. 501E-02 1. 629E-01 1.648E-01 NOT IDENT. EU-154 3.306E-02 9.802E-02 9.915E-02 FAIL ABUN EU-155 7.278E-02 9.132E-02 9.704E-02 FAIL ABUN TB-160 4.628E-01 1. 511E+OO l.526E+OO FAIL ABUN H0-166M -7.262E-03 4.620E-02 4.631E-02 NOT IDENT. TM-171 -3.157E+00 1.160E+Ol l.169E+Ol NOT IDENT. HF-172 -2 .114E-02 2.275E-01 2.277E-01 FAIL ABUN LU-172 l.170E-02 8.098E-02 8 .115E-02 FAIL ABUN LU-176 -l.219E-03 l.764E-02 1.764E-02 FAIL ABUN HF-181 l.071E+00 3.103E+OO 3.140E+OO NOT IDENT. TA-182 -2.480E-01 7.956E-01 8.034E-01 FAIL ABUN RE-183 6.950E-01 1. 746E+OO 1. 774E+OO NOT IDENT. Page 4364 of 5809 RE-184 1.265E+Ol 2.325E+Ol 2.394E+Ol NOT IDENT. W-188 2.977E+Ol 8.261E+Ol 8.369E+Ol FAIL ABUN IR-192 9.261E-02 3.408E-01 3.433E-01. FAIL ABUN HG-203 -1.126E+OO 1.852E+OO 1. 921E+OO NOT IDENT. BI-207 9. 041E-03 4.044E-02 4.064E-02 FAIL ABUN BI-211 3.265E+00 4.589E-01 1.542E+OO FAIL ABUN PB-211 -6.994E-02 5.213E-01 5.222E-01 NOT IDENT. BI-212 8.436E-01 5.060E-01 6.330E-01 NOT IDENT. RN-219 4.697E-02 3.295E-01 3.301E-01 FAIL ABUN RA-223 -1. 475E-01 4.706E-01 4.753E-01 FAIL ABUN RA-224 l.838E+OO 8.580E-01 1.193E+OO FAIL ABUN AC-227 -1.198E-01 1.897E-01 1. 972E-01 FAIL ABUN TH-227 -l.198E-01 1. 897E-01 1.972E-01 FAIL ABUN AC-228 8.942E-01 2.313E-01 4.647E-01 FAIL ABUN RA-228 8.942E-01 2. 313E-01 4.647E-01 FAIL ABUN TH-229 -1.695E-01 3.840E-01 3.915E-01 FAIL ABUN TH-231 -1.475E-01 4.706E-01 4.753E-01 FAIL ABUN TH-232 8.942E-01 2. 313E-01 4.647E-01 FAIL ABUN PA-233 -1.104E-02 4.417E-02 4.445E-02 FAIL ABUN PA-234 2.651E-02 1.843E-01 1.847E-01 FAIL ABUN PA-234M 6.646E+OO 5.435E+OO 6.206E+OO FAIL ABUN NP-237 -1.104E-02 4.417E-02 4.445E-02 FAIL ABUN NP-238 -4.446E+39 6.108E+40 O.OOOE+OO SHORT HLIF NP-239 -7.460E-02 2.161E-01 2.187E-01 NOT IDENT. PU-239 2.427E+02 4.953E+02 5. 072E+02 FAIL ABUN AM-241 1. 7 8 lE-02 9.077E-02 9 .112E-02 NOT IDENT. CM-243 -9.227E-03 8.586E-02 8. 596E-02 NOT IDENT. BK-247 -3.439E-03 6.820E-02 6.822E-02 NOT IDENT. CM-247 9.215E-03 2.995E-02 3.024E-02 NOT IDENT. CF-249 -7. 496E-03 2.820E-02 2. 841E-02 NOT IDENT. CF-251 5.177E-03 9.200E-02 9.203E-02 NOT IDENT. Page 4365 of 5809

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 75.1192 87.09 102.7180 136.47 55.5957 45.60 58.7096 87.57 102.7840 140.51 0.0000 46.54 58.8187 88.03 102.8478 143.76 53.5666 49. 72 0.0000 88.34 102.8904 144.24 53.5914 51. 35 69.0737 88.47 102.9079 145.44 65.0358 51. 87 77.7827 89. 96 103 .1115 152.43 71.2017 52.39 77.8568 1093.63 103.2035 153.25 0.0000 52.97 -79.0217 91.11 0.0000 323.87 73.7805 53.44 71. 5052 92.59 103.4658 156.02 0.0000 54.07 69.4170 93.35 103.5674 158.56 0.0000 57.36 0.0000 94. 56 70.6888 159.00 66.6991 57.53 66.5680 94.65 70.6972 162.33 84.2467 57.98 75.3564 94. 67 70.6991 162.66 0.0000 59.27 86.4683 94.87 70. 7169 163.33 64.4827 59. 32 86.4756 97.43 81.7423 165.86 63.3866 59.54 86.5078 98.43 74.1235 176.31 61. 8789 60. 96 '84.8854 98.44 74.1245 176.60 0.0000 61.17 84.9152 99.53 89.3015 177.52 59.4325 62.93 94.7065 100 .11 74.2778 181.07 0.0000 63 .29 94.7624 102.03 63.9832 181.52 61. 7345 63.58 94.8072 103.18 90.8665 184.41 65.6729 64.28 94.9150 103.37 76.9047 143.76 69.9595 66.73 112.2775 105.21 63.0612 193.51 66.1664 67.24 84.2754 105.31 63.0687 197.03 51. 8919 125.81 99.1294 106.12 81.8347 198.01 56.1890 67.75 99.1403 106.47 81.8689 201.83 63.1910 69.67 . 113. 5360 109.28 79.7931 203.43 65.8351 70.83 102.5868 111. 00 78.7768 205.31 69. 3572 72. 81 105.8774 111.76 0.0000 210.85 59.3348 72. 87 105.8868 114. 06 53.0956 215. 65 51. 7841 74.66 108.7861 116. 30 0.0000 222 .11 58.1043 74.82 108.8120 116.74 78.1096 227.09 49.6129 74.97 108.8356 119.76 71.2473 227.38 49.6234 77 .11 109.1768 121.12 64.2181 228.16 0.0000 78.74 97.7757 121. 22 64.2251 228.18 40.0703 79.69 96.4017 121.78 66.6448 116.74 40.0703 80.12 84.4027 122.06 76.1885 235.69 55.1756 80.19 0.0000 122.92 63.1526 235.96 55.1859 80.57 93.5052 123.07 60.7796 238.63 66.6995 81. 00 95.0710 265.00 65.5899 238.98 0.0000 81. 07 104.1359 125.81 78.0913 240.99 66.8100 81. 75 102. 7242 127.23 71. 8245 242.00 51. 4624 83.79 115 .1349 127.91 64. 6888 244.70 37.0166 84.00 103.0452 129.30 55.9856. 252.40 0.0000 85.43 121. 4673" 131.20 59.3022 252.80 36.3363 86. 55 102.6432 133.02 63.8303 254.15 0.0000 86.79 102.6762 133.52 60.2486 256.23 51.5217 86. 94 102.6974 136.00 56.7771 260.90 0.0000 Page 4366 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 41. 8060 355.39 0.0000 584.27 17.7512 264.80 41. 8098 356.01 28.2880 595.83 0.0000 265.00 45.5682 364.49 0.0000 427.87 18.9104 268.22 51. 0358 366.42 0.0000 602.52 0.0000 269.46 43.9088 372. 51 29.4863 604.72 12. 6260 270.03 43.9247 375.05 27.6206 607.14 22 .1151 271.23 45.7529 377.52 32.4242 609.32 24.2410 273.65 0.0000 356.01 36.3564 610.33 24.2503 276.40 38.7045 388.16 25.8887 614.28 19.0056 277.37 47.7347 388.63 0.0000 618.01 23.7891 277.60 49.5439 391. 69 17.2899 620. 36 19.0481 278.00 46.8531 264.66 31.8398 621.93 19.0583 279.20 50.4959 401.81 29.9272 630.19 0.0000 279.54 50.5062 402.40 28.0047 631. 29 22.3099 279.70 44.1979 404.85 26.1046 633.25 18.0729 280.46 39.7067 410. 95 31. 0313 634.78 0.0000 283.69 32.5532 413.71 20.3916 635.95 21.2826 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 38.9250 423.72 0.0000 645.85 20. 2896 285.90 0.0000 427.09 27.3631 657.76 11.7958 287.50 29.9116 427.87 18.5744 657.90 0.0000 290.67 27.2461 433.94 24.5102 661.66 22.5492 293.27 0.0000 439.40 18.6749 664.57 0.0000 351.93 32.7861 453.88 28.6938 666.33 0.0000 295. 96 16.4008 463.37 22.8545 666.50 0.0000 879.38 16.4268 468.07 24.8937 667.71 0.0000 299.98 20.5508 473.00 0.0000 677.62 19.4341 300.09 20.5522 475.06 22. 9729 685.70 0.0000 300.13 20.5527 476.78 19.9915 695.00 0.0000 301.36 20.5678 477.60 16.9986 696.49 19.5579 302.85 20.5861. 482.18 18.0344 696. 51 19.5579 256.23 20.6067 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.3893 306.78 23.3859 497.08 19.1585 697.49 16.3037 308.46 16.5242 505.52 27.3224 702.65 19.5974 311. 90 31.2760 507.63 0.0000 706.68 23.9846 316.51 29.5156 511. 00 22.3138 711. 68 16.3800 319.41 0.0000 514. 00 . 13.7098 720.70 0.0000 320.08 0.0000 514.00 13.7098 721.93 0.0000 321.04 29.5931 520.40 22.4010 722.78 15.3433 323.87 36.1253 520.69 0.0000 722.91 15.3438 325.23 42.6421 522.65 0.0000 723. 31 15.3461 328.76 0.0000 527.90 0.0000 724 .19 15.3507 333.37 28.8695 528.26 17.3652 727. 33 15.3660 333.97 40.0588 529.59 20.4411 733.00 11. 5455 334.37 50.3174 529.87 0.0000 735.93 7.7044 338.28 34.5520 531.02 0.0000 333.97 16.5173 338.32 34.5528 537.26 0.0000 739.50 0.0000 311. 90 86.0179 546.56 0.0000 747.24 15.4640 340.48 86.0179 552.55 18.5662 748.06 17.6777 340.55 0.0000 5.63.25 26.9310 752.31 16.5948 344.28 30.9187 569.33 14.5355 753.82 0.0000 345.93 39.3870 946.00 17. 6509 756.73 9.9708 351.06 28.2123 569.70 17.6523 756.80 9.9712 351. 93 28.2257 583.19 17.7436 884.68 19.9871 Page 4367 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 19.9980 1274.44 8.5342 1620.50 4.0537 766.42 20.0024 1001.03 5.3403 1621. 92 6.0820 766.84 20.0046 1002.74 5.3427 1678.03 0.0000 772.60 0.0000 1004.73 8.5523 1690.97 4.1033 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.0385 778.90 8.9242 1028.54 0.0000 1063.66 3 .1183 783.70 0.0000 1037.84 14.3730 1771.35 0.0000 785.37 15.6480 1038.76 0.0000 1791.20 0.0000 792.07 15 .1199 631.29 9.9030 1808.65 2.0919 794.95 7.8468 1048.07 0.0000 1810.72 0.0000 795.86 7.8491 1049.04 9.9083 1836.06 4. 2021 810.06 11.2606 1050.41 6.3074 810.29 12.3875 1063.66 11.7519 344.28 14.6403 1077.00 0.0000 810.76 15.7682 1077.34 11.7908 815.77 0. 0.000 1085.87 13. 6331 1048.07 0.0000 1093.63 19.1210 832.01 11. 3338 1099.45 19.1479 834.85 14.7461 1112. 07 12.5416 835.71 12.4806 1112. 84 10.2443 836.80 0.0000 1115. 54 10.2512 846.75 0.0000 1120.29 11. 9114 846.77 14.7969 1120.55 11. 9122 856.80 0.0000 1221.41 11. 9146 860.56 10.2847 1129. 67 6.4279 871.09 16.0462 1131.51 0.0000 873.19 19.4965 1147.95 0.0000 875.33 0.0000 1173.23 11.1299 879.38 11. 4884 1177.95 9.2847 880.51 11.4921 1189.05 16.7542 . 883.24 12.6507 1204.77 11.2083 884.68 14. 9572 1221.41 16.8739 889.28 12. 6722 1231. 02 15. 9697 894.76 12.6914 1235.36 0.0000 898.04 10.3934 1238.28 19.7580 900.72 11. 5568 1260.41 0.0000 903.28 10.4084 1271.87 14.2154 911.20 11. 58 98 1274.44 9.4818 912.08 11.5926 1274.54 7.5854 923.98 0.0000 1291.59 10.4676 926.50 13. 9658 1298.22 0.0000 929 .11 12.8110 1312 .11 0.0000 937.49 . 17.5085 1332.49 9.2133 944.13 0.0000 1362.66 0.0000 946.00 7. 8967 1365 .19 6.7625 949.00 9.6592 1368.63 0.0000 667.71 0.0000 1384.29 0. 9697 962. 31 21.1487 1408.01 2.9229 964. 08 22.0398 1457.56 0.0000 966 .17 43.2219 1460.82 10.8268 911.20 16.7717 1489.16 2.9687 96.8. 97 16.7717 1505.03 3.9700 983.53 0.0000 1584.12 4.8331 984.45 0.0000 1596.21 0.0000 Page 4368 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:55:31.25 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : 2-0CT-2016 11:02:08. Sample date 14-DEC-2015 13:10:00 Acquisition date : 3-0CT-2016 05:53:13. Sample ID G405235062 Sample quantity 1.46441E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.31 Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 *16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 8 8 0 0 0 5 5 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 5 5 Page 4369 of 5809 Energy 63.67* 74.95* 77.07* 87.35 90.00 93.03* 185.92* 209.69 229.01 238.59* 241.87 295.42* 327.91* 329.89* 332.46 338.28 351.98* 388.58 463.83 477.51 482.27 505.99 510.80* 583.24* 609.52* 661. 7 6 727. 92 754.46 768.34 794.98 820.27 911. 40* 964. 7 5 969.39 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 25 71 133 24 43 79 70 49 19 234 57 89 26 14 16 47 155 27 12 15 14 10 29 56 107 17 8 16 17 16 6 52 18 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 104 111 86 188 59 120 90 87 44 37 56 56 14 9 13 31 32 19 19 21 9 5 26 5 10 9 17 2 3 2 3 9 10 4 1.10 0.94 0.95 0.93 0.95 1. 81 1. 33 1. 93 0.59 1.12 1. 79 1. 07 1. 32 1. 32 1.13 0.98 1.18 0.91 0.68 4 *. 35 1. 43 1. 57 2.46 1. 23 1. 24 1. 30 0.95 2.30 1. 53 1. 00 1. 37 1.24 2.70 1. 53 127 .. 31 149.86 154 .11 174.68 179.97 186.03 371.83 419.37 458.01 477.16 483.73 590.82 655.80 659.76 664.90 67 6. 54 703.94 777.13 927.63 954.97 964. 50 1011. 94 1021. 55 1166.40 1218.96 1323.41 1455.71 1508.78 1536.53 1589.79 1640.37 1822.58 1929.24 1938.50 123 146 146 169 178 178 366 413 454 465 465 586 652 652 663 672 700 771 921 946 959 1009 1015 1162 1213 1319 1450 1504 1533 1585 1637 1816 1923 1923 8 7.06E-03 .73.9 12 l.96E-02 25.9 9.68E-01 12 3.70E-02 14.9 10 6.68E-03108.5 14 1.19E-02 28.1 1.95E+OO 14 2.19E-02 31.7 12 1. 95E-02 30. 6 12 1. 35E-02 41. 8 8 5.17E-03 66.8 24 6.50E-02 8.0 3.77E+OO 24 1.58E-02 33.6 9 2.48E-02 18.7 11 7.36E-03 34.1 2.77E+OO 11 4.00E-03 4B.9 6 4 . .S2E-03 42.l 10 1.30E-02 26.4 11 4.31E-02 10.9 11 7.62E-03 36.3 9 3.45*E-03 70.5 13 4.30E-03 67.8 9 3.96E-03 46.2 6 2.91E-03 44.6 13 8.0lE-03 49.2 10 1.56E-02 16.0 13 2. 98E-02 11. 9 9 4.72E-03 40.0 11 2.18E-03107.0 10 4. 38E-03 31. 2 7 4.67E-03 30.4 9 4.41E-03 30.3 6 1.76E-03 58.0 13 1.43E-02 19.2 19 5.08E-03 42.0 1.21E+OO 19 5.03E-03 33.7 Peak Search Report (continued) Page : 2 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1053.83 6 7 0.60 2107.33 2102 7 1.67E-03 83.7 36 0 1121.35* 24 9 0.79 2242.31 2234 17 6.62E-03 35.3 37 0 1173.95 9 2 1. 53 2347.47 2344 7 2. 61E-03 39.9 38 0 1188.54 8 3 1. 23 2376.64 2373 7 2.25E-03 51.1 39 0 1233.94 13 0 o*. 98 2467.38 2462 10 3.61E-03 27.7 40 0 1461.11* 145 6 2.00 2921. 49 2915 13 4.04E-02 9.2 41 0 1765.02* 16 0 1. 50 3528.90 3522 11 4.37E-03 28.7 Flag: "*" = Peak area was by background subtraction Page 4370 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 06:55:33 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 14-DEC-2015 13:10:00 G405235062 Acquisition date : Sample quantity Sample geometry Detector* geometry: 3-0CT-2016 05:53:13 146.44 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide PB-214 PB-214 PB-214 PB-214 -PB-214 PB-214 PB-214 PB-214 Page 4371of5809 Line 242.00 87.09 87.09 87.09 ' 74. 82 74.82 74.82 351.93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.31 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Nuclide* Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status BE-7 477.60 10.44* 1.801E+OO 4.525E-01 2.075E+Ol 135.53 OK K-40 1460.82 10.66* 6.546E-01 1.027E+Ol l.027E+Ol 18.32 OK CD-109 88.03 3.70* 4.301E+OO 6.347E-02 9.868E-023326.46 OK SN-126 64.28 9.60 2.509E+OO 6.880E-01 6.880E-01 147.76 OK 86.94 8.90 4.301E+OO 2.639E-02 2.639E-023326.46 OK 87.57 37.00* 4.301E+OO 6.347E-03 6.347E-033326.46 OK BA-137M 661. 66 89.90* 1.335E+OO 7.558E-02 7.699E-02 80.01 OK CS-137 661.66 85.10* 1.335E+OO 7.984E-02 8.133E-02 80.01 OK TL-208 277.37 6.60 3.041E+OO Line Not Found Absent 583.19 85.00* 1.496E+OO 2.377E-01 2.377E-01 32.07 OK 860.56 12.50 1.058E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.327E+OO Line Not Found Absent 351.06. 12.92* 2.414E+OO l.316E-01 l.316E-01 893.25 OK PB-212 74.82 10.28 3.492E+OO 7.150E-01 7.150E-01 96.01 OK 77 .11 17.10 3.653E+OO 1. 371E+OO 1. 371E+OO 29. 79 OK 238.63 43 .. 60* 3.500E+OO 8.970E-01 8.970E-01 '15. 92 OK 300.09 3.30 2.819E+OO Line Not Found Absent BI-214 609.32 45.49* l.437E+00 8.806E-01 8.809E-01 23.71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.685E-01 70. 51' OK 1764.49 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 OK PB-214 74.82 5.80 3.482E+OO Line Not Found <<INT Reject 77 .11 9.70 3.653E+OO 2.416E+OO 2.417E+OO 29. 79 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found <<INT Reject 295.22 18.42 2.862E+OO 9.735E-01 9.738E-01 37.36 OK 351. 93 35.60* 2.414E+00 Line Not Found <<INT RejeC:t RN-222 609.32 45.49* l.437E+OO 8.806E-01 8.809E-01 23.71 OK 1120.29 14.92 8.365E-01 9.682E-01 9 .*685E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 OK RA-224 240.99 4.10* 3.457E+OO 6.254E-01 6.254E-01 272.29 OK RA-226 609.32 45.49* 1.437E+OO 8.806E-01 8.809E-01 23. 71 OK 1120. 29 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 OK AC-228' 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 OK 794.95 4.25 1.134E+OO 1.725E+00 1.725E+OO 60.55 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+OO 1.029E+OO 1.029E+OO 38.34 OK 968.97 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 OK 794.95 4.25 l.134E+00 1.725E+OO l.725E+00 60.55 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+OO 1. 029E+OO 1.029E+OO 38.34 OK 968. 97 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 OK TH-228 74.82 10.28 3.492E+OO 7.150E-01 7.150E-01 96. 01 OK 77.11 17.10 3.653E+OO 1.371E+OO l.371E+00 29.79 OK 238.63 43. 60"" 3.500E+OO 8.970E-01 8.970E-01 15.92 OK 300.09 3.30 2.819E+00 Line Not Found Absent Page 4372 of 5809 Nuclide Line Activity Report (continued) Page : 3 sample ID : 8405235062 Acquisition date 3-0CT-2016 05:53:13 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 1.437E+OO 8.806E-01 8.806E-01 23.71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 OK TH-232 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+OO 1.029E+OO 1.029E+OO 38.34 OK 968. 97 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 OK TH-234 63.29 3.70* 2.509E+OO 1. 785E+OO 1. 785E+OO 147.76 OK 92. 59 4.23 4.565E+OO 2.580E+OO 2.580E+OO 63.39 OK U-234 609.32 45.49* 1.437E+OO 8.806E-01 8.806E-01 23.71 OK 1120. 29 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 OK U-235 89. 96 3.47 4.432E+OO 1.762E+OO 1. 762E+OO 56.15 OK 93.35 5.60 4.565E+OO 1.949E+OO 1.949E+OO 63.39 OK 143.76 10.96* 4.954E+00 Line Not Found Absent 163.33 5.08 4.674E+OO Line Not Found Absent 185.72 57.20 4.300E+00 1.704E-01 1.704E-01 61.18 OK 205.31 5.01 3.984E+OO Line Not Found Absent U-238 63.29 3.70* 2.509E+OO 1.785E+OO 1. 785E+00 147.76 OK 92.59 4.23 4.565E+OO 2.580E+OO 2.580E+OO 63.39 OK AM-243 43.53 5.90 5.957E-01 Line Not Found Absent 74.66 67.20* 3.492E+OO 1.094E-01 1.094E-01 96. 01 OK CF-249 252.80 2.50 3.319E+OO Line Not Found Absent 333.37 14.60 2.552E+OO 2.482E-01 2.486E-01 84.24 OK 388.16 66.00* 2.193E+OO 1.062E-01 1.064E-01 72.51 OK ANH-511 511. 00 100.00* 1.690E+OO 9.326E-02 9.326E-02 98.40 OK Flag: "*" = Keyline Page 4373 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:55:34.75 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l *
Acquisition date 3-0CT-2016 05:53:13 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live t.ime: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.31 Half life ratio : ***** *
Sample date 14-DEC-2015 13:10:00 Analyst initials: MXRl *
Sample ID G405235062 Sample Quantity l.4644E+02 GRAM * *Batch.Number 1596254 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
EfL File* : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) BE-7 2.075E+Ol 2.756E+Ol K-40 l.027E+Ol l.844E+OO CD-109 9.868E-02 3.217E+OO SN-126 6.347E-03 2.069E-01 BA-137M 7.699E-02 6.037E-02 CS-137 8 .133E-02 6.377E-02 TL-208 2.377E-01 7.468E-02 BI-211 l.316E-01 l.152E+OO PB-212 8.970E-01 l.399E-01 BI-214 8.809E-01 2.047E-01 PB-214 l.022E+OO 2.188E-01 RN-222 8.809E-01 2.047E-01 RA-224 6.254E-01 1.669E+OO RA-226 8.809E-01 2.047E-01 AC-228 l.029E+OO 3.868E-01 RA-228 l.029E+00 3.868E-01 TH-228 8.970E-01 l.399E-01 TH-230 8.806E-01 2.046E-01 TH-232 l.029E+OO 3.868E-01 TH-234 1. 785E+00 2.585E+OO U-234 8.806E-01 2.046E-01 U-235 4.347E-02 l.917E-01 U-238 1. 785E+OO 2.585E+OO AM-243 l.094E-01 1. 029E-01 CF-249 l.064E-01 .7. 559E-02 ANH-511 9.326E-02 8.994E-02 Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 Page 4374 of 5809 Key-Line Activity (pCi/GRAM -6.126E-03 O.OOOE+OO -l.378E-03 -5.265E-02 K.L. Cnt Uncert ( 1. 96-sigma) 5.722E-02 l.960E+41 4.784E-02 3.170E-01 MDA (pCi/GRAM* 2.757E+Ol 6.783E-01 2.295E+OO l.484E-01 7.037'E-02 7.434E-02 6.431E-02 4.287E-01 9.570E-02 l.436E-01 3. 941E-01 l.436E-01 l.028E+OO l.436E-01 3 .133E-01 3.133E-01 9.570E-02 l.436E-01 3.133E-01 2.083E+OO l.436E-01 3.691E-01 2.083E+OO 8. 911E-02 8.007E-02 6. 738.E-02 MDA (pCi/GRAM l.193E-01 O.OOOE+OO l.048E-01 6.522E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO l.141E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.444E+02 O.OOOE+OO SHORT HLIF MN-54 -4.324E-02 8. 256E-02* l.466E-01 NOT IDENT. C0-56 2.954E-02 6.216E-01 l.240E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 4.853E-02 4.361E-02 9.479E-02 NOT IDENT. C0-58 -3. 751E-01 7.033E-01 l.254E+OO NOT IDENT. FE-59 8.973E-01 7.129E+OO l.572E+Ol NOT IDENT. C0-60 -3.067E-02 4.656E-02 8.343E-02 FAIL ABUN ZN-65 8.957E-02 1. 722E-01 3.974E-01 NOT IDENT. GE-68 . -1. 790E+OO 3.451E+OO 5.921E+OO NOT IDENT. AS-73 -4.405E+OO 6.594E+OO l.298E+Ol NOT IDENT. AS-74 0.000E+OO 4.829E+03 O.OOOE+OO SHORT HLIF SE-75 9.369E-02 2.400E-01 4. 714E-01 NOT IDENT. BR-77 O.OOOE+OO 4.210E+36 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 7.000E+02 O.OOOE+OO SHORT HLIF RB-83 l.164E-01 7. 901E-01 l.640E+OO NOT IDENT. KR-85 3.266E+OO 9.559E+OO l.828E+Ol NOT IDENT. SR-85 3.223E-01 9.467E-01 l.811E+OO NOT IDENT. RB-86 0.000E+OO 3.064E+04 O.OOOE+OO SHORT HLIF Y-88 -l.449E-01 2.736E-01 4. 941E-01 NOT IDENT. Y-91 -l.986E+Ol 6.917E+02 l.418E+03 NOT IDENT. NB-94 -l.361E-02 4.281E-02 8.025E-02 NOT IDENT. NB-95 8.616E-01 8.284E-01 l.972E+OO NOT IDENT. NB-95M 1. 931E+OO 2.329E+OO 4.802E+OO NOT IDENT. ZR-95 -4.345E-01 l.564E+OO 2.653E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8. 754E+40 . O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 4.292E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -3.487E-02 3.226E-02 5.667E-02 NOT IDENT. RH-102 5.146E-02 6. 391E-02 l.504E-01 FAIL ABUN RU-103 3.935E+OO 5.572E+OO l.270E+Ol FAIL ABUN RH-106 l.OlOE-02 5.234E-01 l.099E+OO NOT IDENT. RU-106 l.OlOE-02 5.234E-01 l.099E+OO NOT IDENT. AG-108M -5.706E-03 2.759E-02 5.582E-02 NOT IDENT. AG-llOM -7.338E-03 l.186E-01 2.375E-01 NOT IDENT. SN-113 -6. 791E-02 2.628E-01 4.673E-01 NOT IDENT. CD-115 O.OOOE+OO 5.243E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 0. OOOE+OO . 7.064E+04 O.OOOE+OO SHORT HLIF TE-123M -4.641E-02 l.303E-01 2.429E-01 NOT IDENT. SB-124 -5. 841E-01 l.929E+OO 4.131E+OO NOT IDENT. SB-125 -7.819E-03 9.643E-02 2.005E-01 FAIL ABUN TE-125M 1. 764E+Ol 2.612E+02 5.179E+02 NOT IDENT. I-126 O.OOOE+OO 6. 941E+05 0. 00.0E+OO SHORT HLIF SB-126 O.OOOE+OO 9.374E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.084E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.450E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.159E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 915E+2 6 O.OOOE+OO SHORT HLIF BA-133 7. 281E-03 4.577E-02 8.249E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 l.123E-01 6.664E-02 l.519E-01 FAIL ABUN CS-135 -7.422E-02 1. 766E-01 3.124E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.865E+05 O.OOOE+OO SHORT HLIF CE-139 3.731E-02 l.164E-01 2.298E-01 NOT IDENT. BA-140 O.OOOE+OO 9. 772E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.535E+05 0.000E+OO SHORT HLIF CE-141 8.082E-01 2.146E+Ol 4.067E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 9.830E-02 3.553E-01 7. lOlE-01 NOT I DENT'. PM-144 -3.112E-02 6.164E-02 l.129E-01 FAIL ABUN PR-144 -2.719E+OO 5.332E+OO 9.750E+OO NOT IDENT. PM-146 3.664E-02 4.769E-02 l.084E-01 NOT IDENT. ND-147 O.OOOE+OO 2.842E+07 O.OOOE+OO SHORT HLIF PM-147 6.002E+02 7. 814E+02 l*. 648E+03 NOT IDENT. PM-149 O.OOOE+OO 8.538E+39 O.OOOE+OO SHORT HLIF EU-150 .1. 621E-02 2.924E-02 5 .185E-02 FAIL ABUN. EU-152 -4.821E-02 l.OlOE-01 l.745E-01 FAIL ABUN GD-153 -l.030E-01 1. 758E-01 3.082E-01 NOT IDENT. EU-154 -l.926E-02 l.395E-01 2.892E-01 NOT IDENT. EU-155 -9.589E-03 9.956E-02 1. 966E-01 FAIL ABUN TB-160 -l.407E+OO 2.244E+OO 3.855E+OO FAIL ABUN H0-166M 4.556E-02 5.973E-02 l.410E-01 NOT IDENT. TM-171 4.841E+00 l.591E+Ol 3.442E+Ol NOT IDENT. HF-172 1. 951E-01 2.167E-Ol 4.604E-01 FAIL ABUN LU-172 -9.367E-03 8.663E-02 l.715E-01 FAIL ABUN Page 4375 of 5809 LU-176 -1. 640E-02 2.777E-02 4.745E-02 FAIL ABUN HF-181 6.637E+OO 6.008E+OO 1.022E+Ol FAIL ABUN TA-182 -7.525E-01 9.199E-01 1. 580E+OO FAIL ABUN RE-183 1.549E-01 2.289E+OO 4.795E+OO NOT IDENT. RE-184 -1.067E+Ol 2.735E+Ol 5.103E+Ol NOT IDENT. W-188 1.869E+Ol l.288E+02 2.282E+02 FAIL ABUN IR-192 -1.938E-01 5.030E-01 8.880E-01 FAIL ABUN HG-203 9.781E-01 2.504E+OO 4.934E+OO NOT IDENT. BI-207 7.678E-02 5.971E-02 1. 517E-01 FAIL ABUN PB-210 -4.107E-01 2.477E+OO 5.103E+OO NOT IDENT. PB-2il -3.912E-01 7.320E-01 1.405E+OO NOT IDENT. BI-212 5.068E-01 1.063E+OO 1.476E+OO FAIL ABUN RN-219 l.230E-01 4.321E-01 9.147E-01 NOT IDENT. RA-223 9.480E-01 6. 396E-01 l.417E+OO FAIL ABUN AC-227 -2.493E-01 2.529E-01 4 .131E-01 NOT IDENT. TH-227 -2.493E-01 2.529E-01 4 .131E-01 NOT IDENT. TH-229 1.345E-01 4.614E-01 9.136E-01 FAIL ABUN PA-231 2.593E-01 5.449E-01 1. 071E+OO NOT IDENT. TH-231 9.480E-01 6.396E-01 1.417E+OO FAIL ABUN PA-233 2.404E-02 5.971E-02 1.210E-01 NOT IDENT. PA-234 -1.190E-01 3.444E-01 6.363E-01 NOT IDENT. PA-234M 2.732E+OO 5.606E+OO 1 .. 244E+Ol NOT IDENT. NP-237 2.404E-02 5.971E-02 l.210E-01 NOT IDENT. NP-238 O.OOOE+OO 7.189E+40 0.000E+OO SHORT HLIF NP-239 -2.750E-02 2 .115E-01 4:157E-01 FAIL ABUN PU-239 2.985E+02 3.061E+02 6.476E+02 NOT IDENT. AM-241 1. 746E-02 l.260E-01 2.464E-01 NOT IDENT. CM-243 6.845E-02 9.l!15E-02 1. 989E-01
FAIL ABUN BK-247 4.815E-02 8.327E-02 1.678E-01 NOT IDENT. CM-247 1.886E-02 3.649E-02 8.038E-02 NOT IDENT. CF-251 -4.609E-02 1. 096E-01 2.020E-01 NOT IDENT. Page 4376 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:55:32.31 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error BE-7 477.60 17 10.44* 1. 801E+OO 4.525E-01 2.075E+Ol 135.53 K-40 1460.82 140 10.66* 6.546E-01 1. 027E+Cll 1.027E+Ol 18.32 CD-109 88.03 30 3.70* 4. 301E+OO 9.606E-01 1.493E+OO 217.00 SN-126 64.28 32 9.60 2.509E+OO 6.880E-01 6.880E-01 147.76 86.94 30 8.90 4.301E+OO 3.994E-01 3.994E-01 217.00 87.57 30 37.00* 4. 301E+OO 9.606E-02 9.606E-02 217.00 BA-137M 661.66 18 89.90* 1.335E+OO 7.558E-02. 7.699E-02 80.01 CS-137 661. 66 18 ' 85.10* 1.335E+OO 7.984E-02 8.133E-02 80.01 TL-208 277.37 ------6.60 3.041E+OO ------Line Not Found ------583.19 59 85.00* 1. 496E+OO 2.377E-01 2.377E-01 32.07 860.56 ------12.50 1.058E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.327E+OO ------Line Not Found ------351. 06 171 12*. 92* 2.414E+OO 2.814E+OO 2.814E+OO 21.85 PB-212 74.82 89 10.28 3.492E+OO 1.264E+OO 1.264E+OO 51. 81 77 .11 167 17.10 3.653E+OO 1.371E+OO l.371E+OO 29.79 238'.63 267 43.60* 3.500E+OO 8.970E-01 8.970E-01 15.92 300.09 ------3.30 2.819E+OO ------Line Not Found ------BI-214 609.32 112 45.49* 1.437E+OO 8.806E-01 8.809E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 PB-214 74.82 89 5.80 3.492E+OO 2. 241E+OO 2.242E+OO 51. 81 77 .11 167 9.70 3.653E+OO 2.416E+OO 2.417E+OO 29. 79 87.09 30 3.41 4. 301E+OO 1.042E+OO 1.043E+OO 217.00 242.00 65 7.25 3.457E+OO 1.327E+OO 1. 328E+00 67.19 295.22 100 18.42 2.862E+OO 9.735E-01 9.738E-01 37.36 351.93 171 35.60* 2.414E+OO l.021E+00 l.022E+OO 21. 85 RN-222 609.32 112 45.49* 1.437E+OO 8.806E-01 8.809E-01 23. 71 1120.29 24 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 RA-224 240.99 65 4.10* 3.457E+OO 2.347E+00 2.347E+OO 67.19 RA-226 609.32 112 45.49* 1.437E+OO 8.806E-01 8.809E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9 .191E-01 57.44 AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 52 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 794.95 16 4.25 1.134E+OO 1.725E+OO 1.725E+OO 60.55 835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 52 25.80* 1.005E+OO 1. 029E+OO 1.029E+OO 38.34 968. 97 18 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 52 11.27 2.509E+OO 9.408E-01 9.408E-01 52.75 794.95 16 4.25 1.134E+OO 1.725E+OO l.725E+OO 60.55 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 52 25.80* 1.005E+OO 1.029E+OO 1.029E+OO 38.34 968.97 18 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 TH-228 74.82 89 10.28 3.492E+OO 1.264E+OO l.264E+OO 51. 81 77 .11 167 17.10 3.653E+OO 1.371E+OO 1. 371E+OO 29.79 Page 4377 of 5809 Nuclide Line Activity Report (continued) -Page : 2 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 267 43.60* 3.500E+OO 8.970E-01 8.970E-01 15.92 300.09 ------3.30 2.819E+OO ------Line Not Found ------TH-230 609.32 112 45.49* l.437E+00 8.806E-01 8.806E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 TH-232 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 52 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 52 25.80* 1.005E+OO 1.029E+OO 1.029E+OO 38.34 968.97 18 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 TH-234 63.29 32 3.70* 2.509E+OO l.785E+OO 1. 785E+OO 147.76 92.59 97 4.23 4.565E+OO 2.580E+OO 2.580E+OO 63.39 U-234 609.32 112 45.49* l.437E+OO 8.806E-01 8.806E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 U-235 89. 96 53 3.47 4.432E+OO 1. 762E+OO 1. 762E+OO 56.15 93.35 97 5.60 4.565E+OO 1.949E+OO l.949E+00 63.39 143.76 ------10. 96* 4.954E+OO ------Line Not Found ------163.3'3 ------5.08 4.674E+OO ------Line' Not Found ------185.72 82 57.20 4.300E+OO 1.704E-01 l.704E-01 61.18 205.31 . ------5.01 3.984E+OO ------Line Not Found ------U-238 63.29 32 3.70* 2.509E+OO 1.785E+OO l.785E+00 147.76 92.59 97 4.23 4.565E+OO 2.580E+OO 2.580E+OO 63.39 AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 89 67.20* 3.492E+OO 1.934E-01 .1.934E-01 51. 81 CF-249 252.80 ------2.50 3.319E;+OO ------Line Not Found ------333.37 18 14.60 2.552E+OO 2.482E-01 2.486E-01 84.24 388.16' 30 66.00* 2.193E+00 l.062E-01 l.064E-01 72. 51 ANH-511 511. 00 31 100.00* 1.690E+00 9.326E-02 9.326E-02 98.40 Flag: "*" Key line Page 4378 of 5809 Summary of Nuclide Activity Sample ID.: G405235062 Acquisition date Page : 3 3-0CT-2016 05:53:13 Total number of lines in spectrum 41 Number of unidentified lines 3 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Hlife 53.22D l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600. OOY l.41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 351. OOY 1.00E+09Y Decay 45.9 1. 00 1. 55 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 4.525E-01 1.027E+Ol 9.606E-01 9.606E-02 7.558E-02 7.984E-02 2.377E-01 2.814E+OO 8.970E-01 8.806E-01 1.021E+OO 8.806E-01' 2.347E+OO 8.806E-01 1. 029E+OO 1.029E+OO 8.970E-01 8.806E-01 1.029E+OO 1. 785E+OO 8.806E-01 l.704E-01 1.785E+OO 1.934E-01 1.062E-01 9.326E-02 3.177E+Ol 3.177E+Ol Decay Corr pCi/GRAM 2.075E+Ol 1.027E+Ol 1.493E+OO 9.606E:_02 7.699E-02 8.133E-02 2.377E-01 2.814E+OO 8.970E-01 8.809E-01 1.022E+OO 8.809E-01 2.347E+OO 8.809E-01 1.029E+OO l:029E+OO 8.970E-01 8.806E-01 1.029E+OO 1.785E+OO 8.806E-01 1.704E-01 1. 785E+OO l.934E-01 l.064E-01 9.326E-02 5.261E+Ol 5.261E+Ol 92.68% Decay Corr 2-Sigma Error 2.812E+Ol 0.188E+Ol 3.241E+OO 20.85E-02 6.160E-02 6.507E-02 0.762E-01 0.615E+OO 1.428E-01 2.089E-01 0.223E+OO 2.089E-01 1.577E+OO 2.089E-01 0.395E+OO 0.395E+OO 1.428E-01 2.088E:_Ol 0.395E+OO 2.638E+OO 2.088E-01 1.042E-01 2.638E+00 l.002E-01 0.771E-01 9.177E-02 "M" Manually accepted 2-Sigma %Error 135.53 18.32 217.00 217.00 80.01 80.01 32.07 21. 85 15.92 23.71 21. 85 23. 71 67.19 23.71 38.34 38.34 15.92 23.71 38.34 147.76 23.71 61.18 147.76 51. 81 72 .51 98.40 Flags: "K" Keyline not.found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4379 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235062 Acquisition date : 3-0CT-2016 05:53:13 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.69 56 101 1. 93 419.37 413 12 l.35E-02 83.6 3.92E+OO T 0 229.01 21 51 0.59 458.01 454 8 5.17E-03 **** 3.63E+OO T 1 327.91 29 16 1. 32 655.80 652 11 7.36E-03 68.3 2.59E+OO T 1 329.89 16 10 1. 32 659. 76 652 11 4.00E-03 97.8 2.57E+OO 0 463.83 13 20 0.68 927.63 921 9 3.45E-03 **** 1. 85E+OO T* 0 482.27 15 9 1. 43 964. 50 959 9 3. 96E-03 92.4 1.78E+OO T 0 505.99 11 5 1. 57 1011. 94 1009 6 2.91E-03 89.1 1. 71E+OO T 0 727. 92 8 18 0.95 1455.71 1450 11 2.18E-03 **** 1.23E+OO T 0 754.46 16 2 2.30 1508.78 1504 10 4.38E-03 62.4 1.19E+OO T 0 768.34 17 3 1. 53 1536.53 1533 7 4. 67E-03. 60.8 1.17E+OO T 0 820.27 6 3 1. 37 1640.37 1637 6 1.76E-03 **** 1.lOE+OO 5 964. 75 18 10 2.70 1929.24 1923 19 5.08E-03 84.1 9.56E-01 T 0 1053.83 6 7 0.60 2107.33 2102 7 1. 67E-03 **** 8.84E-01 0 1173.95 9 2 1. 53 2347.47 2344 7 2.61E-03 79.7 8.03E-01 T 0 1188.54 8 3 1.23 2376.64 2373 7 2.25E-03 **** 7.94E-01 T 0 1233.94 13 0 0.98 2467.38 2462 10 3. 61E-03 55.5 7.67E-01 T Flags: "T" = Tentatively associated Page 4380 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:55:49.65 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * *
DETECTOR AND SAMPLE DATA *
*. *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l *
Acquisition date 3-0CT-2016 05:53:13 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.31 Half life ratio : ***** *
Sample date 14-DEC-2015 13:10:00 Nuclide Library : SOLID *
Sample ID G405235062 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : 1.4644E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 .PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Le (pCi/GRAM 1.204E+Ol 2.392E-01 1.076E+OO 6.955E-02 2.916E-02 3. OBOK-02 2.656E-02 1.914E-01 4.310E-02 6.093E-02 1.888E-01 6.093E-02 4.629E-01 6.093E-02 1.295E-01 1.295E-01 4.310E-02 6. 091E-02 1.295E-01 9.601E-01 6.091E-02 1.711E-01 9. 601E-01 4 .137E-02 3.507E-02 2.947E-02 ----Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 Page 4381 of 5809 Le (pCi/GRAM 4.801E-02 O.OOOE+OO 3.924E-02 2.481E-01 O.OOOE+OO NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4382 of 5809 O.OOOE+OO 6.080E-02 5.280E-01 O.OOOE+OO 4.384E-02 5.141E-01 6.445E+OO 3.084E-02 1.607E-01 2.428E+OO 5.880E+OO O.OOOE+OO 2.146E-01 O.OOOE+OO O.OOOE+OO 7.190E-01 8 .111E+OO 8.032E-01 O.OOOE+OO 1.562E-01 5.976E+02 3.451E-02 8.408E-01 2.202E+OO 1. 062E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 2.582E-02 6.461E-02 5.541E+OO 4.620E-01 4.620E-01 2.389E-02 9.754E-02 2.039E-01 O.OOOE+OO O.OOOE+OO l .113E-01 1. 306E+OO 8.550E-02 2.400E+02 O.OOOE+OO O.OOOE+OO 0. OOOE+"OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.613E-02 O.OOOE+OO 6.641E-02 1.418E-01 O.OOOE+OO O.OOOE+OO 1.063E-01 O.OOOE+OO O.OOOE+OO 1.873E+Ol O.OOOE+OO 3.283E-01 4.663E-02 4.027E+OO 4.775E-02 O.OOOE+OO 7.615E+02 O.OOOE+OO 2 .. 293E-02 7.580E-02 l.415E-01 l.160E-01 9.032E-02 1.550E+OO 6.00lE-02 1.570E+01 2.130E-01 6.818E-02 2.093E-02 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL 'ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 4383 of 5809 4.506E+OO 5. 914E-0*1 2.193E+OO L 977E+Ol 1:027E+02 3.927E-01 2.235E+OO 6.494E-02 2.340E+OO 6.126E-01 6.515E-Ol 4.062E-01 6.395E-01 l.833E-01 1.833E-01 4.173E-01 4.875E-01 6.395E-01 5.362E-02 2.578E-01 5.316E+OO 5.362E-02 O.OOOE+OO l.896E-01 3.009E+02 l.134E-01 9. 211E-02 7.633E-02 3.549E-02 9.150E-02 FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT. IDENT. FAIL ABUN NOT IDENT. NOT IDENT: FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT. HLIF FAIL ABUN NOT IDENT. NOT I DENT.* FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:55:55.84 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l *
Acquisition date 3-0CT-2016 05:53:13 Sensitivity : 3.000 *
Detector ID GAM36 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.31 Half life ratio : ***** *
Sample date 14-DEC-2015 13:10:00 Nuclide Library : SOLID *
Sample ID G405235062 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity 1.4644E+02 GRAM *
Quantity Err(%) l.3657E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7 * . Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) BE-7 2.075E+Ol 2.758E+Ol K-40 1.027E+Ol 1. 921E+OO CD-109 9.868E-02 3.221E+OO SN-126 6.347E-03 2.072E-01 BA-137M 7.699E-02 6.046E-02 CS-137 8.133E-02 6.387E-02 TL-208 2.377E-01 7.537E-02 BI-211 1.316E-01 l.164E+OO PB-212 8.970E-01 l.477E-01 BI-214 8.809E-01 2.082E-01 PB-214 1.022E+OO 2.229E-01 RN-222 8.809E-01 2.082E-01 RA-224 6.254E-01 1.673E+OO RA-226 8.809E-01 2.082E-01 AC-228 1.029E+OO 3.904E-01 RA-228 1.029E+OO 3.904E-01 TH-228 8.970E-01 1.477E-01 TH-230 8.806E-01 2. 081E-01 TH-232 1.029E+OO 3.904E-01 TH-234 1.785E+OO 2.615E+OO U-234 8.806E-01 2.081E-01 U-235 4.347E-02 l.917E-01 U-238 1. 785E+OO 2.615E+OO AM-243 l.094E-01 1.037E-01 CF-249 l.064E-01 7.609E-02 ANH-511 9.326E-02 9.002E-02 Non-Identified Nuclides Nuclide* NA-22 NA-24 AL-26 SC-46 Page 4384 of 5809 Key-Line Activity (pCi/GRAM -6.126E-03 -1.000E+41 -l.378E-03 -5.265E-02 K.L Act error ( 1. 96-sigma) 5. 722E-02 3.126E+41 4.784E-02 3.170E-01 TPU (1. 96-sigma) 2.758E+Ol 1.921E+OO 3.221E+OO 2. 072E-01 6.046E-02 6.387E-02 7.537E-02 i.164E+00 l.477E-01 2.082E-01 2.229E-01 2.082E-01 1.673E+OO 2.082E-01 3.904E-01 3.904E-01 1. 477E-01 2. 081E-01 3.904E-01 2.615E+OO 2. 081E-01 1.917E-01 2.615E+OO l.037E-01 7.609E-02 9.002E-02 TPU ( 1. 96-sigma) 5.729E-02 O.OOOE+OO 4.785E-02 3.179E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 4.628E+03 1.141E+04 1-.160E+04 SHORT HLIF CR-51 -1.408E+02 4.444E+02 4.489E+02 SHORT HLIF MN-54 -4.324E-02 8.258E-02 8.485E-02 NOT IDENT. C0-56 2.954E-02 6.216E-01 6.217E-01 NOT IDENT. MN-56 1.000E+41 l.785E+42 O.OOOE+OO SHORT HLIF C0-57 4.853E-02 4.367E-02 4.885E-02 NOT IDENT. C0-58 -3. 751E-01 7.035E-01 7.236E-01 NOT IDENT. FE-59 8.973E-01 7.129E+OO 7 .141E+OO NOT IDENT. C0-60 -3.067E-02 4.657E-02 4.858E-02 FAIL ABUN ZN-65 8.957E-02 l.722E-01 1.769E-01 NOT IDENT. GE-68 -l.790E+OO 3. 451E+OO 3.544E+OO NOT IDENT. AS-73 -4.405E+OO 6.656E+OO 6.946E+OO NOT IDENT. AS-74 3.866E+02 4.829E+03 4.833E+03 SHORT HLIF SE-75 9.369E-02 2.400E-01 2.437E-01 NOT IDENT. BR-77 2.698E+37 2.288E+38 O.OOOE+OO SHORT HLIF 4.558E+02 7.003E+02 7.299E+02 SHORT HLIF RB-83 1.164E-01 7.902E-01 7.920E-01 NOT IDENT. KR-85 3.266E+OO 9.560E+OO 9.672E+OO NOT IDENT. SR-85 3.223E-01 9.468E-01 9.579E-01 NOT IDENT. RB-86 -l.146E+04 3.064E+04 3.108E+04 SHORT HLIF Y-88 -l.449E-01 2.738E-01 2.815E-01 NOT IDENT. Y-91 -1.986E+Ol 6.917E+02 6.918E+02 NOT IDENT. NB-94 -1. 361E-02 4.282E-02 4.326E-02 NOT IDENT. NB-95 8.616E-01 8.292E-01 9.157E-01 NOT IDENT. NB-95M 1. 931E+OO 2.334E+OO 2. 491E+OO NOT IDENT. ZR-95 -4.345E-01" 1.564E+OO 1.577E+OO NOT IDENT. NB-97 l.000E+41 4.922E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 8.763E+40 O.OOOE+OO SHORT HLIF M0-99 -1. 941E+31 4.294E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.395E+41 O.OOOE+OO SHORT HLIF RH-101 -3.487E-02 3.287E-02 3.644E-02 NOT IDENT. RH-102 5.146E-02 6.404E-02 6.812E-02 FAIL ABUN RU-103 3.935E+OO 5.575E+OO 5.850E+OO FAIL ABUN RH-106 1 .. 0lOE-02 5.234E-01 5.234E-01 NOT IDENT. RU-106 1.0lOE-02 5.234E-01 5.234E-01 "NOT IDENT. AG-108M -5.706E-03 2.759E-02 2. 771E-02 NOT IDENT. AG-110M -7.338E-03 1.186E-01 l.186E-01 NOT IDENT. SN-113 -6.791E-02 2.628E-01 2.646E-01 NOT IDENT. CD-115 8.343E+37 5.246E+38 O.OOOE+OO SHORT HLIF SN-117M -l.342E+04 7.066E+04 7.092E+04 SHORT HLIF TE-123M -4.641E-02 1.303E-01 l.320E-01 NOT IDENT. SB-124 -5.841E-01 1.929E+OO l.947E+OO NOT IDENT. SB-125 -7.819E-03 9.644E-02 9.650E-02 FAIL ABUN TE-125M 1.764E+Ol -2.612E+02 2.613E+02 NOT IDENT. I-126 -l.316E+05 6.943E+05 6. 968E+05 SHORT HLIF SB-126 2.394E+05 9.384E+05 9.446E+05 SHORT HLIF SB-127 -2.769E+21 8.005E+21 O.OOOE+OO SHORT HLIF I-131 -2.580E+09 3.452E+09 3.643E+09 SHORT HLIF I-132 -l.OOOE+41 1.814E+42 O.OOOE+OO SHORT HLIF TE-132 1.462E+26 2.001E+26 O.OOOE+OO SHORT HLIF BA-133 7.281E-03 4.578E-02 4.589E-02 NOT IDENT. I-133 -1.000E+41 4.481E+41 O.OOOE+OO SHORT HLIF CS-134 1.123E-01 6.681E-02 8.382E-02 FAIL ABUN CS-135 -7.422E-02 1. 767E-01 l.799E-01 . NOT IDENT. I-135 -1.000E+41 1.472E+42 O.OOOE+OO SHORT HLIF CS-136 7.146E+04 2.867E+05 2.885E+05 SHORT HLIF CE-139 3.731E-02 1.166E-01* l.178E-01 NOT IDENT. BA-140 -3.784E+05 9.773E+05 9.921E+05 SHORT HLIF LA-140 -7.554E+04 4.535E+05 4.548E+05 SHORT HLIF CE-141 8.082E-01 2.146E+Ol 2.146E+Ol NOT IDENT. CE-143 l.000E+41 9.032E+42 O.OOOE+OO SHORT HLIF CE-144 9.830E-02 3.553E-01 3.581E-01 NOT IDENT. PM-144 -3.112E-02 6.167E-02 6.325E-02 FAIL ABUN PR-144 -2. 719E+OO 5.333E+OO 5.472E+OO NOT IDENT. PM-146 3.664E-02 4.776E-02 5.054E-02 NOT IDENT. ND-147 8.488E+05 *2. 842E+07 2.843E+07 SHORT HLIF PM-147 6.002E+02 7.819E+02 8.274E+02 NOT IDENT. PM-149 . -5.573E+39 8.622E+39 O.OOOE+OO . SHORT HLIF EU-150 1. 621E-02 *2.925E-02 3.015E-02 FAIL ABUN EU-152 -4.821E-02 l.OlOE-01 l.033E-01 FAIL ABUN GD-153 -l.030E-01 1.759E-01 l.820E-01 NOT IDENT. EU-154 -1. 926E-02 1.395E-01 l.398E-01 NOT IDENT. EU-155 -9.589E-03 9.956E-02 9. 966E-02 FAIL ABUN TB-160 -l.407E+00 2.245E+OO 2.333E+OO FAIL ABUN H0-166M 4.556E-02 5.978E-02 6.321E-02 NOT IDENT. TM-171 4.841E+00 l.592E+Ol l.607E+Ol NOT IDENT. HF-172 1.951E-01 2.190E-01 2.360E-01 FAIL ABUN LU-172 -9.367E-03 8.663E-02 8.674E-02 FAIL ABUN Page 4385 of 5809 LU-176 -1.640E-02 2.778E-02 2.874E-02 FAIL ABUN HF-181 6.637E+OO 6.015E+OO 6.718E+OO FAIL ABUN TA-182 -7.525E-01 9.203E-01 9.809E-01 FAIL ABUN RE-183 l.549E-01 2.290E+OO 2.291E+OO NOT IDENT. RE-184 -1.067E+Ol 2.746E+Ol 2.788E+Ol NOT IDENT. W-188 1. 8 69E+Ol 1. 288E+02 l.291E+02 FAIL ABUN IR-192 -1.938E-01 5.031E-01 5.106E-01 FAIL ABUN HG-203 9.781E-01 2.505E+OO 2.543E+OO NOT IDENT. BI-207 7.678E-02 5.979E-02 6.908E-02 FAIL ABUN PB-210 -4.107E-01 2.477E+OO 2.484E+OO NOT IDENT. PB-211 -3.912E-01 7.323E-01 7.532E-01 NOT IDENT. BI-212 5.068E-01 1. 063E+OO 1.087E+OO FAIL ABUN RN-219 l.230E-01 4.324E-01 4.359E-01 NOT IDENT. RA-223 9.480E-01 . 6. 423E-01 7. 715E-01 FAIL ABUN AC-227 -2.493E-01 2.550E-01 2.787E-01 NOT IDENT. TH-227 -2.493E-01 2.550E-01 2.787E-01 NOT IDENT. TH-229 1.345E-01 4.615E-01 4.654E-01 FAIL ABUN PA-231 2.S93E-01 5.477E-01 5.601E-01 NOT IDENT. TH-231 9.480E-01 6.423E-01 7.715E-01 FAIL ABUN PA-233 2.404E-02 5.972E-02 6.070E-02 NOT IDENT. PA-234 -1.190E-01 3.703E-01 3.742E-01 NOT IDENT. PA-234M 2.732E+OO 5.608E+00 5. 741E+OO NOT IDENT. NP-237 2.404E-02 5. 972E-02 6.070E-02 NOT IDENT. NP-238 -9.649E+39 7.189E+40 O.OOOE+OO SHORT HLIF NP-239 -2.750E-02 2 .115E-01 2 .119E-01 FAIL ABUN PU-239 2.985E+02 3.064E+02 3.346E+02 NOT IDENT. AM-241 1.746E-02 1.260E-01 l.262E-01 NOT IDENT. CM-243 6.845E-02 9.436E.'....Q2 9.928E-02 FAIL ABUN BK-247 4.815E-02 8.383E-02 8.659E-02 NOT IDENT. CM-247 1.886E-02 3.663E-02 3.761E-02 NOT IDENT. CF-251 -4.609E-02 1.098E-01 l. ll 7E-01 NOT IDENT. Page 4386 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 74.66 14.0690 105.31 75.1328 131.20 57.5436 879.38 39.3639 86.79 75.1725 133.02 48. 0972 46.54 37.1209 86.94 75.1979 133.52 45.2487 228.16 0.0000 87.09 75.2233 136.00 47.3656 52.39 32.8973 87.57 75.3034 136.47 45.4667 1093.63 35.3626 88.03 75.3796 739.50 0.0000 52.39 31.3953 306.78 75.4310 140.51 0.0000 125.81 37.0976 88.47 38.9052 143.76 47.9525 53.44 41.9977 143.76 56.7739 144.24 51.9058 54.07 38.8423 90.64 48.5659 145.44 43.1722 293.27 0.0000 531.02 0.0000 152.43 58.5067 482.18 44.9726 92.59 48.7692 1048.07 0.0000 57.98 37.6630 93.35 48.8481 154.21 40.7648 59.27 42.7356 94.56 48. 9728 158.56 .. o. 0000 59.32 42.7417 311. 90 48.9820 159.00 47.0595 59.54 41.6723 946.00 48.9840 162.33 40.2423 60. 96 55.0547 94.87 33.4665 537 .'26 0.0000 61.17 44.0700 97.43 45.6604 163.33 48.3596 62.93 46.5021 98.43 39.7337 165.86 44.4881 63.29 46.5484 98.44 39.7347 427.87 47.1820 290.67 46.5856 103.37 39.8226 176.60 0.0000 87.57 46.6752 116.74 39.8226. 177.52 38.0123 66.73 59.2907 100 .11 39.8693 181. 07 0.0000 67.24 48.7291 102.03 49.1188 181.52 37.1810 67.68 47.9446 103.18 31. 9089 184.41 38.3584 1221.41 47.9533 103.37 39.2171 185.72 38.4233 97.43 54 .1138 911.20 44.8504 193.51 32. 5132 279.20 59.3632 105.31 44.8593 197.03 40.0294. 1063.66 47.7298 106.12 44.0127 198.01 40.0781 72.87 47.7371 106.47 41.2901 201.83 42.3846 351.06 47.7371 109.28 52.5825 2b3.43 39.2820 74.66 56.5128 111. 00 48.1255 205.31 31.2128 238.63 56.5350 111. 76 0.0000 210.85 35.3460 351.93 56.5350 114. 06 33.5075 215.65 35.5439 238.63 56.5350 116. 30 0.0000 222 .11 28.2118 74.97 56.5561 116.74 38.3480 227.09 45.1005 77 .11 56. 8517 119.76 47.9600 227.38 42.2043 78.74 50.7327 264.66 44.3049 228.16 0.0000 256.23 53.1585 121. 22 35.8274 228.18 22.9418 133;52 52.0555 344.28 37.7499 235.69 27.5368 364.49 0.0000 122.06 31.1591 235. 96 27.5448 711. 68 46.3204 122.92 52.0098 238.63 27.6241 356.01 43.4692 1274.44 52.0232 238.98 0.0000 323.87 43.4761 123.68 53.0255 240.99 27.6936 81. 75 54.8669 125.81 35.1636 242.00 27.7233 83.79 51.3333 127.23 55.2545 244.70 32. 6213 265.00 51. 3580 127.91 55.3186 685.70 0.0000 193.51 74.9447 129.30 39 .1964 388.16 28.0369 ! Page 4387 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 507.63 0.0000 345.93 23.1818 569.50 10.3582 256.23 36.0127 351.06 23.2774 569.70 9.4173 527.90 0.0000 351. 93 23.2937 583.19 7.5889 264.66 28.3737 355.39 0.0000 584.27 7.5931 264.80 28.3775 356.01 14.7590 595.83 0.0000 265.00 24.9769 364.49 0.0000 600.60 13.4024 268.22 39.8621 366.42 0.0000 602.52 0.0000 269.46 33.0693 372. 51 22.4231 604.72 8.6342 270.03 34.2279 375.05 14.9777 607.14 11. 5264 401. 81 26.2723 377.52 17.5064 609.32 10.5779 273.65 0.0000 383.85 25.1276 610.33 10.5833 276.40 30.9955 388.16 16.8050 614.28 2.8922 583.19 27. 5771 666.33 0.0000 618.01 9.6590 277.60 26.4337 391.69 18.9546 884.68 17.4067 402.40 27.5940 400.66 21.1980 621. 93 7.7425 279.20 25.3234 401.81 17.8213 630.19 0.0000 279.54 29.9371 402.40 13.5837 631. 29 5.8342 279.70 31. 0935 404.85 19.5607 633.25 11. 6797 280.46 28.8109 410.95 18.7912 634.78 0.0000 301.36 25.4308 413. 71 23. 9622 635.95 9.7461 284.31 0.0000 720.70 0.0000 636.99 0.0000 285.41 30.1030 423. 72 0.0000 1690.97 9.7937 285.90 0.0000 427.09 11. 2287 657.76 8.8656 287.50 23.2013 427.87 12.0990 657.90 0.0000 290.67 24.8210 433.94 13.8844 661. 66 7.8952 293.27 0.0000 439.40 16.5481 664.57 0.0000 295.22 26.8717 453.88 10.5515 666.33 0.0000 316.51 26.8893 463.37 11. 5009 666.50 0.0000 298.58 42.1875 468.07 10.6482 667.71 0.0000 299.98 18.7739 473.00 0.0000 677.62 12.9275 300.09 23.4698 631.29 16.0430 685.70 0.0000 300.13 23.4705 696.49 16.0602 695.00 0.0000 311. 90 23.4705 477.60 16.0682 696.49 12.0386 301.36 27.0205 482.18 9.3998 696. 51 12.0386 302.85 36.4681 487.02 0.0000 697.00 0.0000 304.50 24.7401 492.35 0.0000 697.30 12.0430 304.85 0.0000 497.08 9.0342 697.49 14.0513 306.78 27.1518 505.52 10.8962 702.65 . 16.0964 308.46 21.2805 507.63 0.0000 706.68 11. 08 68 311. 90 15.4157 511. 00 16.3976 711. 68 5.0509 316.51 25.0016 514.00 16.4268 720.70 0.0000 319.41 0.0000 514.00 16.4268 721. 93 0.0000 320.08 0.0000 520.40 13.7402 722. 78 9.1370 321.04 35.8557 520.69 0.0000 722. 91 6.0916 323.87 9.5847 667.71 0.0000 723. 31 6.0928 325.23 19.1914 . 527. 90 0.0000 756.73 10.6666 1596.21 0.0000 528.26 8.2819 727. 33 9.1556 333.37 20.9325 529.59 11. 9717 733.00 12.2378 333.97 12.0825 529.87 0.0000. 735.93 10.2116 334.37 7.2519 531.02 0.0000 737.46 8.1748 338.28 25.4637 537.26 0.0000 739.50 0.0000 338.32 25.4643 1260.41 0.0000 747.24 7.1834 340.48 24.2944 552.55 14. 9271 748.06 11.2923 340.55 0.0000 795. 8 6 15.0150 752.31 7. 7133 344.28 20.7141 569.33 10.3573 753.82 0.0000 Page 4388 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 756.73 7.7283 968.97 5.5929 1505.03 4.8950 756.80 7.7283 983.53 0.0000 1584.12 5.9843 763.94 10.8529 984.45 0.0000 1596.21 0.0000 765.81 3.1033 996.26 4.5168 1620.50 5.0284 1001.03 9.3124 1001.03 5.6551 1621. 92 2.0120 766.84 9.3138 .1002.74 5.6584 1678.03 0.0000 772. 60 0.0000 1004.73 10.1920 1690.97 2.0430 776.52 0.0000 1021. 30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 1.0377 778.90 5.2008 1028.54 0.0000 1770.23 6.2333 783.70 0.0000 1037.84 5.7255 1771. 35 3 .1174 785.37 7.3008 1038.76 0.0000 1791.20 0.0000 903.28 10.9819 1046.59 9.1868 1808.65 3.1415 794.95 6.2827 1048.07 0.0000 1810.72 0.0000 795.86 10.9990 1049.04 6.8955 1836.06 3.1591 801.95 11.5514 1050.41 6.8989 810. 0.6 11.5899 1063.66 2. 3096 810.29 11. 5908 1077.00 0.0000 810.45 11. 5917 1077.34 11. 5983 810.76 11. 5931 1085.87 4.6520 815.77 0.0000 1093.63 5.8293 818.51 0.0000 1099.45 6.1323 832.01 7.4406 1112. 07 5.2767 834.85 12.7700 1112. 84 8.7970 835.71 9.5808 1115. 54 2.8174 836.80 0.0000 1120.29 7.0537 846.75 0.0000 1120.55 7 .* 0542 846.77 10.6917 1121.30 7.0562 856.80 0.0000 1808.65 7.0742 860.56 8.5993 1131.51 0.0000 871.09 4.3171 1147.95 0.0000 873.19 12. 9614 1332.49 3.5840 875.33 0.0000 1177.95 2.8713 879.38 10. 82*68 1189.05 7.2017 880.51 8.6650 1204.77 9.9479 883.24 6.5056 1221.41 8.1788 884.68 7.5939 1231.02 2.9160 889.28 4.3470 1235.36 0.0000 894.76 6.5339 1238.28 1.4610 1836.06 7.6320 1260.41 0.0000 900. 72 5.4569 1271.87 7.3740 903.28 6.5547 1274.44 6.4570 911.20 7.6694 1274.54 6.4574 912.08 7. 6719 1291.59 2.7805 984.45 0.0000 1298.22 0.0000 926.50 7. 7124 1312 .11 0.0000 929 .11 9.9254 1332. 49 6.5599 937.49 9.9554 1362. 66 0.0000 983.53 0.0000 1365.19 3.7810 946.00 8.8763 1368.63 0.0000 949.00 4.4429 1384.29 7. 5996 954.55 0.0000 1408.01 2. 8672 962.31 3.3479 1457.56 0.0000 964. 08 5.5833 1460.82 1.9370 966 .17 5.5874 1489.16 1. 9504 Page 4389 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:56:28.72
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date. : Z-OCT-2016 11:02:28. Sample date 14-DEC-2015 13:15:00 Acquisition date : 3-0CT-2016 05:53:40. Sample ID G405235063 Sqmple quantity l.47883E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.75 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID ., 1596254 Detector SN# Matrix Spike_ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 4 4 1 1 0 4 4 4 0 0 0 0 3 3 3 6 6 0 0 0 0 0 1 l' 0 0 0 5 5 0 0 0 0 0 Page 4390. of 5809 Energy 63.34* 65.77 74. 80. 77.17* 84.27 87.25 89.87 92.67* 110. 26 144.83 154.39 185.93* 205.54 209.50 211. 70 238.68* 241.60 270.36 295.45 300.07 338.64 352.00* 401.23 405.01 .463. 97 511.35* 520.52 543.58 546.66 583.42* 609.58* 678.72 711. 57 728.58 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 28 22 58 122 35 48 41 54 36 20 21 62 25 35 27 340 77 23 147 37 65 202 24 21 19 56 11 10 15 84 154 7 13 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 84 74 125 99 105 112 142 118 121 98 81 122 60 61 79 65 100 50 79 37 96 51 24 18 37 22 16 6 10 33 53 12 12 31 1. 37 1. 09 0.93 1. 06 1. 37 0.95 1. 45 1. 46 1. 05 1. 24 0.83 1. 29 1.56 1. 20 1. 57 1.10 1. 82 1. 37 1.11 1. 75 1. 32 1. 30 1. 53 1. 53 2.60 2.47 0.87 1. 56 1. 65 1.19 1. 54 0.61 0.64 1. 89 127 .13 131.99 150.05 154.81 169.00 174.98 180.22 185.81 221.01 290.17 309.31 372.41 411. 64 419.57 423. 96 477. 96 483.79 541.35 591.55 600.78 677.96 704.69 803.20 810.76 928.75 1023.57 1041.91 1088.05 1094.23 1167. 77 1220.14 1358.50 1424.23 1458.28 124 124 147 147 167 172 172 172 217 287 306 367 408 408 408 473 473 537 586 597 672 700 799 799 922 1017 1038 1086 1086 1162 1214 1352 1420 1449 11 7.86E-03 11 6 .15E-03 13 l.60E-02 13 3.40E-02 6 9.84E-03 20 l.33E-02 20 l.14E-02 20 l.50E-02 9 1. OOE-02 7 5.65E-03 6 5.83E-03 10 1. 73E-02 29 6.99E-03 29 9.60E-03 29 7.55E-03 17 9.44E-02 17 2.14E-02 9 6.37E-03 12 4.08E-02 7 l.02E-02 14 1. 80E-02 10 5.61E-02 19 6.79E-03 19 5.78E-03 10 5.24E-03 16 l.56E-02 8 3.06E-03 12 2.87E-03 12 4.25E-03 10 2.33E-02 15 4.28E-02 8 2.00E-03 8 3.49E-03 14 5.12E-03 55.9 60.8 31. 6 16.3 48.3 35.9 56.l 44.0 57.6 84.0 71. 2 36.6 55.0 42.4 65.5 6.8 34.5 59.2 14.7 32.0 34.2 9.8 38.3 45.3 64.9 28.4 69.8 36.7 45.8 17.2 13. 6 95.l 55.7 68.5 Fit 1. 27E+OO l.70E+OO 7.lOE-01 9.60E-01 9.83E-01 l.54E+OO 8.91E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 746.85 12 5* .1. 29 1494.85 1491 7 3. 31E-03 43.0 36 0 773.10 15 13 1. 59 1547.37 1541 10 4.21E-03 53.4 37 0 776.26 10 0 0.95 1553.70 1551 6 2.78E-03 31. 6 38 0 795.67 12 27 0.63 1592.54 1584 12 3.37E-03 90.4 39 0 840.54 15 8 1. 51 1682.34 1678 8 4.28E-03 40.6 40 0 862.77 . 11 31 1. 71 1726.83 1719 15 2.97E-03116.3 41 0 911. 20* 87 25 1. 62 1823.77 1815 18 2. 41E-02 17.8 42 0 969.25* 31 20 2.05 1939.94 1935 10 8.70E-03 32.7 43 0 1000.74 22 3 0.97 2002.97 1998 11 6.12E-03 25.9 44 0 1120.34 51 17 1. 56 2242.37 2235 14 1.42E-02 22.2 45 0 1377.40 7 ' 4 0.55 2756 .*93 2752 8 1.94E-03 62.3 46 0 1460.71* 261 14 2.25 2923.72 2917 14 7.26E-02 7.0 47 0 1764.37 25 4 2.04 3531.65 3525 11 6.81E-03 27.1 Flag: "*" = Peak area was modified by background subtraction Page 4391 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 06:56:30 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 14-DEC-2015 13:15:00 G405235063 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:53:40 147.88 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214. 351. 93 Page 4392 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.75 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.030E+00 l.163E+Ol 1.163E+Ol 13.95 OK CD-109 88.03 3.70* 4.459E+OO 7.567E-01 1.176E+OO 179.82 OK TE-125M 109.28 0.27* 5.627E+00 l.475E+Ol 5 .118E+02 115 .11 OK SN-126 64.28 9.60 2.050E+OO 9.341E-01 9.341E-01 111.73 OK 86.94 8.90 4.459E+00 3.146E-01 3.146E-01 179.82 OK 87.57 37.00* 4.459E+OO 7.567E-02 7.567E-02 179.82 OK CE-141 145.44 48.29* 5.912E+00 1.345E-02 7.054E+00 560.68 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent 583.19 85.00* 2.178E+OO 2.434E-01 2.434E-01 34.32 OK 860.56 12.50 1.592E+OO Line Not Found Absent PB-212 74.82 10.28 3.338E+OO 4.161E-01 4.161E-01 170.92 OK 77.11 . 17 .10 3.578E+00 1.279E+OO 1.279E+OO 32.68 OK 238.63 43.60* 4.585E+00 9.891E-01 9.891E-01 13.62 OK 300.09 3.30 3.818E+OO 1.663E+OO 1.663E+OO 64.02 OK BI-214 609.32 45.49* 2. lOlE+OO 8.600E-01 8.603E-01 27.23 OK 1120.29 14.92 1. 288E+OO 1. 341E+OO 1. 341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 OK PB-214 74.82 5.80 3.340E+00 Line Not *Found <<INT Reject 77 .11 9.70 3.578E+OO 2.254E+OO 2.255E+OO 32.68 OK 87.09 3.41 4.447E+00 Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.868E+OO 1.177E+OO 1.178E+OO 29.49 OK 351. 93 35.60* 3.336E+OO 9.566E-01 9.569E-01 19.55 OK RN-219 271.23 10.80 4.160E+OO 2.940E-01 2.940E-01 118.36 OK 401.81 6.60* 2.983E+OO 6.899E-01 6.899E-01 76.53 OK RN-222 609.32 45.49* 2 .101E+OO 8. 600E-01. 8.603E-01 27.23 OK 1120.29 14.92 l.288E+OO 1.341E+OO 1.341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 OK RA-224 240.99 4.10* 4.543E+OO 3.268E-01 3.268E-01 542.80 OK RA-226 609.32 45.49* 2.101E+OO 8.600E-01 8.603E-01 27.23 . OK 1120.29 14.92 l.288E+OO 1.341E+OO 1.341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 OK 794.95 4.25 1.695E+OO 8.749E-01 8.749E-01 180.84 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911. 20 25.80* 1.521E+OO 1.136E+OO 1.136E+OO 35.58 OK 968. 97 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32. 11. 27 3.448E+OO 9.424E.:_01 9.424E-01 68.32 OK 794.95 4.25 8.749E-01 8.749E-01 180.84 OK 835. 71 1. 61 1.630E+OO Line Not Found Absent 911. 20 25.80* l.521E+OO 1.136E+00 1.136E+OO 35.58 OK 968.97 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 OK TH-228 74.82 10.28 3.J38E+OO 4.161E-01 4.161E-01 170.92 OK 77 .11 17.10 3.578E+OO 1.279E+OO 1.279E+OO 32.68 OK 238.63 43.60* 4.585E+OO 9.891E-01 9.891E-01 13.62 OK 300.09 3.30 3.818E+OO l.663E+OO 1.663E+OO 64.02 OK TH-229 85.43 14.70 4.223E+OO 3.627E-01 3.627E-01 96. 63 OK Page 4393 of 5809 Nuclide Line Activity Report (continued) Page : 3 .Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 i Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 88.47 24.00 4.459E+OO 1.1.67E-01 1.167E-01 179.82 OK 193.51 4.41* 5.283E+OO Line Not Found Absent 210.85 2.80 4.994E+OO 1.143E+OO 1.143E+OO 131. 04 OK . TH-230 609.32 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 OK 1120.29 14.92 l.288E+OO 1. 341E+OO 1.341E+OO 44.37 OK 1764.49 1.5.30 8.674E-01 8.854E-01 8.855E-01 54.19 OK PA-231 283.69 1. 70 4.000E+OO Line Not Found Absent 301.36 5.35* 3.818E+OO. 1.026E+OO 1.026E+OO 64.02 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1.521E+OO l.136E+OO 1.136E+00 35.58 OK 968. 97 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 OK TH-234 63.29 3.70* 2.050E+OO 2.424E+OO 2.424E+OO 111.73 OK 92.59 4.23 4.835E+00 1.664E+OO 1.664E+OO 88.03 OK U-234 609.32 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 OK 1120.29 14.92 l.288E+OO 1.341E+OO 1. 341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.854E-01 54.19 OK U-235 89. 96 3.47 4.649E+OO 1.608E+OO 1.608E+OO 112. 29 OK 93.35 5.60 4.835E+OO 1.257E+OO 1.257E+OO -88.03 OK 143.76 10. 96* 5.918E+OO Line Not Found <<INT Reject 163.33 5.08 5.731E+OO Line Not Found Absent 185.72 57.20 5.403E+OO 1.197E-01 1.197E-01 73.11 OK 205.31 5.01 5.091E+OO 5.815E-01 5.815E-01 109.95 OK U-238 63.29 3.70* 2.050E+OO 2.424E+OO 2.424E+00 111.73 OK 92.59 4.23 4.835E+OO 1.664E+00 1.664E+OO 88.03 OK AM-243 43.53 5.90 1.573E-01 Line Not Found Absent 74.66 67.20* 3.338E+00 6.366E-02 6.366E-02 170.92 OK CM-247 278.00 3.40 4.067E+OO Line Not Found Absent 287.50 2.00 3.956E+OO Line Not Found Absent 402.40 "72.00* 2.983E+OO 6.324E-02 6.324E-02 76.53 OK ANH-511 511. 00 100.00* 2.429E+OO 1.255E-01 1.255E-01 56.85 OK Flag: "*" = Keyline Page 4394 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:56:32.59

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l * *Acquisition date 3-0CT-2016 05:53:40 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
Sample date 14-DEC-2015 13:15:00 Analyst initials: MXRl *
Sample ID G405235063 Sample Quantity 1.4788E+02 GRAM *
Batch Number 1596254 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * *******************************************************************************" * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides . Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.163E.+01 1.590E+OO . CD-109 1.176E+OO 2.073E+OO TE-125M 5 .118E+02 5.773E+02 SN-126 7.567E-02 1.334E-01 CE-141 7.054E+OO 3.876E+Ol TL-208 2.434E-01 8.186E-02 PB-212 9.891E-01 l.321E-01 BI-214 8.603E-01 2. 296E-01 PB-214 9.569E-01 l.834E-01 RN-219 6.899E-01 S.174E-01 RN-222 8.603E-01 2.296E-01 RA-224 3.268E-01 1.738E+OO RA-226 8.603E-01 2.296E-01 AC-228 1.136E+OO 3.959E-01 RA-228 1.136E+OO 3.959E-01 TH-228 9.891E-01 1. 321E-01 TH-229 2.170E-01 4. 726E-01 TH-230 8.600E-Ol 2.295E-01 PA-231 1. 026E+OO 6.435E-01 TH-232 l .136E+OO 3.959E-01 TH-234 2.424E+OO 2.654E+OO U-234 8.600E-01 2.295E-01 U-235 1.909E-01 3.144E-01 U-238 2.424E+OO 2.654E+OO AM-243 6 .. 366E-02 l.066E-01 CM-247 6.324E-02 4.743E-02 ANH-511 l.255E-01 6.992E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4395 of 5809 Key-Line Activity (pCi/GRAM 3.200E+00 2.212E-02 0.000E+OO K.L. Cnt Uncert ( 1. 96-sigma) 9.086E+OO 4.504E-02 l.321E+41 MDA (pCi/GRAM 8.231E-01 1.870E+OO 5.037E+02 1.212E-01 4.035E+Ol 7.148E-02 8.930E-02 1.248E-01 1.327E-01 7.187E-01 1.248E-01 9.576E-01 l.248E-01 2.269E-01 2.269E-01 8.930E-02 9.051E-01 1.248E-01 8. 960E-01 2.269E-01 2.806E+OO l.248E-01 3.688E-01 2.806E+OO l.039E-01 6.597E-02 4. 576.E-02 MDA (pCi/GRAM 1.926E+Ol 9.953E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3.SOSE-02 3.864E-02 5.5S3E-02 NOT IDENT. SC-46 -3.425E-01 4.021E-01 7.099E-01 FAIL ABUN V-48 O.OOOE+OO 1.221E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.083E+02 O.OOOE+OO SHORT HLIF MN-54 7.283E-02 7 .115E-02 1.545E-01 NOT IDENT. C0-56 -9.726E-02 5.283E-01 9.622E-01 NOT IDENT. MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.636E-02 4.904E-02 9.535E-02 NOT IDENT. C0-58 -9.557E-02 4.462E-01 8.454E-01 NOT IDENT. FE-59 8.441E+OO 6. 596E+OO l.562E+Ol NOT IDENT. C0-60 -1.242E-02 3.931E-02 7.482E-02 NOT IDENT. ZN-65 7.991E-02 2.182E-01 4.074E-01 NOT IDENT. GE-68 l.089E+OO l.922E+00 4.429E+OO NOT IDENT. AS-73 l.684E+OO 1. 37 4E+Ol 2.770E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.651E+03 O.OOOE+OO SHORT HLIF SE-75 -5.889E-02 1.904E-01 3.335E-01 FAIL ABUN BR-77 O.OOOE+OO 3. 969E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 3.812E+02 O.OOOE+OO SHORT HLIF RB-83 5.872E-01 8.037E-01 l.285E+OO FAIL ABUN KR-85 6.739E+OO 6.693E+OO 1.462E+Ol NOT IDENT. SR-85 6.637E-01 6.624E-01 1.447E+OO NOT IDENT. RB-86 0.000E+OO 1. 785E+04 O.OOOE+OO SHORT HLIF Y-88 -1. 821E-01 1. 963E-01 3.046E-01 NOT IDENT. Y-91 -2.375E+02 5.230E+02 9.574E+02 NOT IDEN'.I'. NB-94 1. 32 6E-02 2. 681E-02 5.712E-02 NOT IDENT. NB-95 l.592E-01 8.432E-01 1.645E+OO NOT IDENT. NB-95M 2.462E-01 2.407E+OO 4.064E+OO NOT IDENT. ZR-95 2.142E-01 1.564E+OO 3.024E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.899E+31 O.OOOE+OO SHORT HLIF TC-99M 0.000E+OO 1.350E+41 O.OOOE+OO SHORT HLIF RH-101 -4.416E-02 3.278E-02 5.433E-02 NOT IDENT. RH-102 3.669E-02 5.999E-02 1. 2 66E-01 NOT IDENT. RU-103 -2.181E+00 5.050E+OO 9.321E+OO FAIL ABUN RH-106 -3.128E-02 4.938E-01 9.513E-01 NOT IDENT. RU-106 -3.128E-02 4.938E-01 9.513E-01 NOT IDENT. AG-108M -4.664E-03 2.191E-02 4.286E-02 NOT IDENT. AG-llOM 5.776E-03 l.062E-01 2.169E-01 FAIL ABUN SN-113 -l.233E-01 l.936E-01 3.552E-01 NOT IDENT. CD-115 O.OOOE+OO 4.675E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 7. 516E+04 O.OOOE+OO SHORT HLIF TE-123M 8.559E-02 1.297E-01 2.549E-01 NOT IDENT. SB-124 -l.613E-01 2.258E+OO 4. 571E+00 NOT IDENT. SB...:.125 9.090E-02 l.187E-01 2.475E-01 FAIL ABUN I-126 O.OOOE+OO 6.620E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8. llOE+OS 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 7.638E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.869E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.095E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.122E+26 O.OOOE+OO SHORT HLIF BA-133 4.348E-02 3.887E-02 8.122E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5. 696E-02 l.009E-01 l.189E-01 FAIL ABUN CS-135 4.569E-03 1. 301E-01 2. 381E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.334E+05 O.OOOE+OO SHORT HLIF BA-137M 2.924E-02 4.049E-02 8.363E-02 NOT IDENT. CS-137 3.089E-02 4.277E-02 8.834E-02 NOT IDENT. CE-139 -8.175E-02 l.103E-01 1.906E-01 NOT IDENT. BA-140 0.000E-i-00 8.554E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.004E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 8.105E+40 O.OOOE+OO SHORT HLIF CE-144 6.516E-02 3.306E-01 6.369E-01 NOT IDENT. PM-144 l.627E-02 5.329E-02 1. 078E-01 NOT IDENT. PR-144 1.408E+OO 4. 614E*+oo 9.333E+OO NOT IDENT. PM-146 -9.657E-03 4.266E-02 8.149E-02 FAIL ABUN ND-147 O.OOOE+OO 2.385E+07 O.OOOE+OO SHORT HLIF PM-147 3.574E+02 8.541E+o2 l.674E+03 *NOT IDENT. PM-149 O.OOOE+OO 6.978E+39 O.OOOE+OO SHORT HLIF EU-150 7.598E-03 2.569E-02 4.787E.:_02 FAIL ABUN EU-152 -5.850E-03 l.064E-01 1.873E-01 NOT IDENT. GD-153 7.267E-02 1. 730E-01 3.248E-01 NOT* IDENT. EU-154 5.439E-02 1.108E-01 2.448E-01 NOT IDENT. EU-155 1.034E-01 1.159E-01 2.362E-01 FAIL ABUN TB-160 5. 961E-01 1. 754E+OO 3.768E+OO FAIL ABUN H0-166M 6.590E-02 7.199E-02 1.304E-01 FAIL ABUN TM-171 -9.680E+OO 3.579E+Ol 6.997E+Ol FAIL ABUN Page 4396 of 5809 HF-172. l.058E-01 2 .131E-01 4. 231E-01 FAIL ABUN LU-172 -4.453E-02 8.206E-02 1. 496E-Ol FAIL ABUN LU-176 8.463E-03 2.022E-02 4.260E-02 FAIL ABUN HF-181 -2.553E-01 3. 431E+OO 6.756E+OO NOT IDENT. TA-182 2.742E-01 9. 965E-01 2.034E+OO FAIL ABUN RE-183 -5.749E-01 4.043E+OO 7.973E+OO FAIL ABUN RE-184 -8.429E+OO 2.806E+Ol 5.256E+Ol NOT IDENT. W-188 -8.826E+Ol l.089E+02 1. 752E+02 FAIL ABUN IR-192 l.715E-02 4.312E-01 8.591E-01 FAIL ABUN HG-203 -6.890E-01 1. 883E+OO 3.655E+OO NOT IDENT. BI-207 l.354E-02 5.154E-02 1. 075E-01 FAIL ABUN PB-210 2.430E+OO 7.416E+OO l.544E+Ol NOT IDENT. BI-211 0.000E+OO 5.050E-01 8.217E-01 FAIL ABUN PB-211 1. 031E+OO 9.151E-01 l.377E+OO FAIL ABUN BI-212 7*. 967E-Ol l.070E+OO l.324E+OO FAIL ABUN RA-223 *2.211E-01 5.556E-01 l.147E+OO FAIL ABUN AC-227 3.202E-02 2.304E-01 4.249E-01 FAIL ABUN TH-227 3.202E-02 2.304E-01 4.249E-01 FAIL ABUN TH-231 2. 211E-01 5.556E-01 l.147E+OO FAIL ABUN PA-233 9.428E-03 5.455E-02 l.108E-01 FAIL ABUN PA-234 -5. 251E-02 2.831E-01 5:586E-Ol FAIL ABUN PA-234M 9.446E+OO 4.798E+OO l.099E+Ol FAIL ABUN NP-237 9.428E-03 5.455E-02 l.108E-01 FAIL ABUN NP-238 O.OOOE+OO 6.618E+40 O.OOOE+OO SHORT HLIF NP-239 -l.518E-01 2.458E-01 4.429E-01 NOT IDENT. PU-239 3.049E+02 2.953E+02 6.070E+02 NOT IDENT. AM-241 l.400E-01 l.970E-01 4. lllE-01 NOT IDENT. CM-243 -4.340E-02 l.027E-01 1. 901E-01 NOT IDENT. BK-247 -5.989E-03 6. 501E-02 l.177E-01 FAIL ABUN CF-249 -8.936E-03 3.328E-02 6.415E-02 NOT IDENT. CF-251 -8.984E-02 l.146E-01 l.957E-01 NOT IDENT. Page 4397 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:56:29.65 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error *K-40 1460.82 252 10.66* 1.030E+OO
1.163E+Ol 1.163E+Ol 13.95 CD-109 88.03 60 3.70* 4.459E+OO 1. 842E+OO 2.863E+OO 71. 81 TE-125M 109.28 44 0.27* 5.627E+OO 1.475E+Ol 5 .118E+02 115 .11 SN-126 64.28 36 9.60 2.050E+OO 9.341E-01 9.341E-01 111.73 8.6. 94 60 8.90 4.459E+OO 7.657E-01 7.657E-01 71. 81 87.57 60 37.00* 4.459E+OO l.842E-01 l.842E-01 71. 81 CE-141 145.44 24 48.29* 5.912E+OO 4.332E-02 2. 272E+Ol 168.05 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 89 85.00* 2.178E+OO 2.434E-01 2.434E-01 34.32 860.56 ------12.50 1.592E+OO ------Line Not Found ------BI-211 72. 87 ------1.23 3 .135E+OO ------Line No.t Found ------351. 06 224 12.92* 3.336E+OO 2.636E+OO 2.636E+00 19.55 PB-212 74.82 73 10.28 3.338E+OO 1.080E+OO 1.080E+OO 63.29 77 .11 154. 17.10 3.578E+OO 1.279E+OO 1.279E+OO 32.68 238.63 389 43.60* 4.585E+OO 9.891E-01 9.891E-01 13.62 300.09 41 3.30 3.818E+00 1.663E+OO 1. 663E+O'O 64.02 BI-214 609.32 162 45.49* 2 .101E+OO 8.600E-01 8.603E-01 27.23 1120.29 51 14.92 1.288E+OO 1.341E+OO l.341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 PB-214 74.82 73 5.80 3.338E+OO l.915E+00 1.915E+OO 63.29 77 .11 154 9.70 3.578E+00 2.254E+OO 2.255E+OO 32.68 87.09 60 3.41 4.459E+OO l.998E+00 1.999E+OO 71. 81 242.00 88 7.25 4.543E+OO 1.362E+OO 1.363E+OO 69.10 295.22 165 18.42 3.868E+OO 1.177E+OO 1.178E+OO 29.49 351. 93 224 35.60* 3.336E+OO 9.566E-01 9.569E-01 19.55 RN-219 271.23 26 10.80 4.160E+OO 2.940E-01 . 2. 940E-01 118. 36 401.81 27 6.60* 2.983E+OO 6.899E-01 6.899E-01 76.53 RN-222 609.32 162 45.49* 2.101E+OO 8.600E-01 8.603E-01 27.23 1120.29 51 14.92 l.288E+OO 1.341E+OO 1.341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 RA-224 240.99 88 4.10* 4.543E+OO 2.409E+OO 2.409E+OO 69.10 RA-226 609.32 162 45.49* 2.101E+OO 8.600E-01 8.603E-01 27.23 1120.29 51 14.92 1.288E+OO 1. 341E+OO l.341E+00 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 AC-228 105.21 ------1.10 5.460E+00 ------Line Not Found ------338.32 72 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 794.95 12 4.25 1.695E+OO 8.749E-01 8.749E-01 180.84 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 88 25.80* 1.521E+OO 1.136E+OO l.136E+OO 35.58 968. 97 31 15.80 1.448E+00 6.987E-01 6.987E-01 65.47 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 72 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 794.95 12 4.25 1.695E+00 8.749E-01 8.749E-01 180.84 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 88 25.80* 1. 521E+OO 1.136E+OO 1.136E+OO 35.58 968. 97 31 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 TH-228 74.82 73 10.28 3.338E+OO 1.080E+OO 1.080E+00 63. 29 Page 4398 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235063 Acquisition date 3-*ocT-2016 05:53:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 154 17.10 3.578E+OO 1. 279E+OO 1. 27 9E+OO 32.68 238.63 389 43.60* 4.585E+OO 9*.891E-01 9.891E-01 13.62 300.09 41 3.30 3.818E+OO 1. 663E+OO 1.663E+OO 64.02 TH-229 85.43 44 14.70 4.223E+OO 3.627E-01 3.627E-01 96. 63 88.47 60 24.00 4.459E+OO 2.839E-01 2.840E-01 71. 81 193.51 ------4.41* 5.283E+OO ------Line Not Found ------210.85 31 2.80 4.994E+OO l.143E+OO l.143E+OO 131. 04 TH-230 609.32 162 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 1120.29 51 14.92 l.288E+OO 1.341E+OO 1. 341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.855E-01 54.19 PA-231 283.69 ------1. 70 4.000E+OO ------Line Not Found ------301.36 41 5.35* 3.818E+OO 1.026E+OO 1.026E+OO 64.02 TH-232 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 72 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 88 25.80* 1. 521E+OO l.136E+OO 1.136E+OO 35.58 968. 97 31 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 TH-234 63.29 36 3.70* 2.050E+OO 2.424E+OO 2.424E+OO 111. 73 92.59 67 4 :23 4.835E+OO 1. 664E+OO 1.664E+OO 88.03 U-234 609.32 162 45.49* 2 .101E+OO 8.600E-01 8.600E-01 27.23 1120.29 51 14.92 l.288E+OO 1.341E+OO 1.341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.854E-01 54.19 U-235 89. 96 51 3.47 4.649E+OO l.608E+OO 1.608E+OO 112. 29 93.35 67 5.60 4.835E+OO 1.257E+OO 1.257E+OO 88.03 143.76 24 10. 96* 5.912E+OO l.909E-01 l.909E-01 168.05 163.33 ------5.08 5.731E+OO ------Line Not Found ------185.72 73 57.20 5.403E+OO 1.197E-01 l.197E-01 73 .11 205.31 29 5.01 5.091E+OO 5.815E-01 5.815E-01 109.95 U-238 63. 29 36 3.70* 2.050E+OO 2.424E+OO 2.424E+00 111.73 92.59 67 4.23 4.835E+OO 1.664E+OO 1.664E+OO 88.03 AM-243 43.53 ------5.90 1.573E-01 ------Line Not Found ------74.66 73 67.20* 3.338E+OO 1.653E-01 1.653E-01 63.29 CM-247 278.00 ------3.40 4.067E+OO ------Line Not Found ------287.50 ------2.00 3.956E+OO -------Line Not Found ------402.40 27 72. 00* 2.983E+OO 6.324E-02 6.324E-02 76.53 ANH-511 511. 00 60 100.00* 2.429E+OO 1.255E-01 1.255E-01 56.85 Flag: "*" Key line Page 4399 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Total number of lines in spectrum 47 Number of unidentified lines 5 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Hlife l.25E+09Y 461.40D 57.40D 2.30E+05Y 32.51D l.41E+10Y 7.04E+08Y 1.41E+l0Y 1600. OOY 1600.00Y 7.04E+08Y 1600. OOY 1.41E+10Y 1600. DOY l.41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.56E+07Y l.OOE+09Y Decay 1. 00 1. 55 34.7 1. 00 524. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.163E+Ol 1.842E+OO 1.475E+Ol 1.842E-01 4.332E-02 2.434E-01 2.636E+OO 9.891E-01 8.600E-01 9.566E-01 6.899E-01 8.600E-01 2.409E+OO 8.600E-01 l.136E+OO l.136E+OO 9.891E-01 2.839E-01 8.600E-01 l.026E+OO l.136E+OO 2.424E+OO 8.600E-01 l.909E-01 2.424E+OO 1.653E-01 6.324E-02 l.255E-01 5.177E+Ol 5.177E+Ol Decay Corr pCi7GRAM 1.163E+Ol 2.863E+OO 5 .118E+02 1.842E-01 2.272E+Ol 2.434E-01 2.636E+OO 9.891E-01 8.603E-01 9.569E-01 6.899E-01 8.603E-01 2.409E+OO 8.603E-01 l.136E+OO l.136E+OO 9.891E-01 2.840E-01 8.600E-01 l.026E+00 1.136E+OO 2.424E+OO 8.600E-01 1.909E-01 2.424E+OO l.653E-01 6.324E-02 l.255E-01 5.725E+02 5.725E+02 89.36% Decay Corr 2-Sigma Error 0.162E+Ol 2.056E+OO 5.891E+02 l.323E-01 3.818E+Ol 0.835E-01 0.515E+OO 1. 34 7E-01 2. 343E:__Ol 1. 871E-01 5.280E-01 2.343E-01 1. 664E+OO. 2.343E-01 0.404E+OO 0.404E+OO 1. 34 7E-01 2.039E-01 2.342E-01 *o.657E+OO 0.404E+OO 2.708E+OO 2.342E-01 3.208E-01 2.708E+OO l.046E-01 4.840E-02 0.713E-01 "M" Manually accepted 2-Sigma %Error 13 .*95 71. 81 115 .11 71. 81 168.05 34.32 19.55 13.62 27.23 19.55 76.53 27.23 69.10 27.23 35.58 35.58 13.62 71. 81 27.23 64.02 35.58 111. 73 27.23 168.05 111.73 63.29 76.53 56.85 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4400 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235063 Acquisition date : 3-0CT-2016 05:53:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 65.77 28 94 1. 09 131. 99 124 11 6.15E-03 **** 2.34E+00 T 0 154.j9 25 96 0.83 309.31 306 6 5.83E-03 **** 5.83E+00 T 3 209.50 40 71 1. 20 419.57 408 29 9.60E-03 84.7 5.03E+OO 1 405.01 23 20 1. 53 810.76* 799 19 5.78E-03 90.5 2.96E+OO T 0 463.97 20 40 2.60 928.75 922 10 .5.24E-03 **** 2.64E+OO T 0 520.52 12 17 0.87 1041.91 1038 8 3.06E-03 **** 2.39E+OO T 5 543.58 11 6 1. 56 1088.05 1086 12 2.87E-03 73.4 2.31E+OO 5 546.66 16 11 1. 65 1094.23 1086 12 4.25E-03 91. 6 2.30E+OO T 0 67 8. 72 8 12 0.61 1358.50 1352 8 2.00E-03 **** 1.93E+OO T 0 711.57 13 13 0.64 1424.23 1420 8 3.49E-03 **** 1.85E+OO T 0 728.58 19 32 1. 89 1458.28 1449 14 5.12E-03 **** 1.82E+OO T 0 746.85 12 5 1. 29 1494.85 1491 7 3.31E-03 85.9 1. 78E+OO T 0 773.10 16 13 1. 59 1547.37 1541 10 4.21E-03 **** 1.73E+OO T 0 776.26 10 0 0.95 1553.70 1551 6 2.78E-03 63.2 1.73E+OO T 0 840.54 16 8 1. 51 1682.34 1678 8 4.28E-03 81.1 1. 62E+OO 0 8 62. 77 11 32 1. 71 1726.83 1719 15 2.97E-03 **** 1.59E+OO 0 1000.74 22 3 0.97 2002.97 1998 11 6.12E-03 51. 8 1. 41E+OO T 0 1377.40 7 4 0.55 2756.93 2752 *8 l.94E-03 **** 1.08E+00 Flags: "T" = Tentatively associated Page 4401 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:56:47.05 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l* * *Acquisition date 3-0CT-2016 05:53:40 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
Sample date 14-DEC-2015 13:15:00 Nuclide Library : SOLID *
Sample ID G405235063 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : 1.4788E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 CE-141 TL-208 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 3 .487E-01 8.669E-01 2.351E+02 5.617E-02 1.884E+Ol 3.193E-02 4.106E-02 5.504E-02 6.037E-02 3.232E-01 5.504E-02 4.403E-01 5.504E-02 9.566E-02 9.566E-02 4.106E-02 4.216E-01 5.502E-02 4.129E-01 9.566E-02 1.306E+OO 5.502E-02 1.732E-01 l.306E+OO 4.868E-02 2. 967E-02 1.997E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4402of5809 Le (pCi/GRAM 8.423E+OO 4.235E-02 O.OOOE+OO 1.978E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124* SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 4403 of 5809 3.038E-01 O.OOOE+OO O.OOOE+OO 6.903E-02 4.206E-01 O.OOOE+OO 4.461E-02 3.481E-01 6.897E+OO 3. 051E-02 1. 793E-01 1.870E+OO 1.287E+Ol O.OOOE+OO 1.510E-01 O.OOOE+OO O.OOOE+OO 5.730E-01 6.603E+OO 6.532E-01 O.OOOE+OO 9.627E-02 4.074E+02 2.481E-02 7.262E-01 1.882E+OO 1.336E+OO o:oOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.502E-02 5.619E-02 4.102E+OO 4.164E-01 4.164E-01 l.862E-02 9. 451E-02 l.565E-01 O.OOOE+OO O.OOOE+OO 1.192E-01 l.814E+OO 1.134E-01 *O. OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.695E-02 O.OOOE+OO 5.315E-02 l.083E-01 O.OOOE+OO O.OOOE+OO 3.777E-02 3.990E-02 8.833E-02 0.000E+OO O.OOOE+OO O.OOOE+OO 2.959E-01 4.734E-02 4.099E+OO 3.626E-02 O.OOOE+OO 7.831E+02 0.000E+OO 2.178E-02 8.547E-02 l.509E-01 l.042E-01 1. llOE-01 l.637E+OO 5.821E-02 3.241E+Ol 1. 969E-01 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RA-223 AC-227 TH-'227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4404 of 5809 6.347E-02 1. 92 6E-02 2.958E+OO 8.903E-01 3.709E+OO 2.252E+Ol 7.922E+Ol 3.923E-01 l.656E+OO 4.668E-02 7.168E+OO 3.945E-01 6.251E-01 6.043E-01 5.235E-01 l.951E-01 1. 951E-01 5.235E-01 5.040E-02 2.400E-01 4.908E+OO 5.040E-02 O.OOOE+OO 2.056E-01 2.841E+02 1.927E-01 8.842E-02 5.321E-02 2.856E-02 9.031E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:56:54.34 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road * * . Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l * *Acquisition date 3-0CT-2016 05:53:40 Sensitivity : 3.000 *
Detector ID GAM44 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
Sample date 14-DEC-2015 13: 15: 0.0 Nuclide Library : SOLID *
Sample ID G405235063 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : 1.4788E+02 GRAM *
Quantity Err(%) : 1.3524E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 * * . Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.163E+Ol l.702E+OO CD-109 1.176E+OO 2.086E+OO TE-125M 5 .118E+02 5. 781E+02 SN-126 7.567E-02 l.341E-01 CE-141 7.050E+OO 3.878E+Ol TL-208 2.434E-01 8.251E-02 PB-212 9.891E-01 1.421E-01 BI-214 8.603E-01 2.325E-01 PB-214 9.569E-01 1.876E-01 . RN-219 6.899E-01 5.246E-01 RN-222 8.603E-01 2.325E-01 RA-224 3.268E-01 1. 744E+OO RA-226 8.603E-01 2.325E-01 AC-228 1.136E+OO 4.002E-01 RA-228 1.136E+OO 4.002E-01 TH-228 9. 8 91E-01 1.421E-01 TH-229 2.170E-01 4. 727E-01 TH-230 8.600E-01 2.324E-01 PA-231 l.026E+OO 6.797E-01 TH-232 l.136E+OO 4.002E-01 TH-234 2.424E+OO 2.708E+OO U-234 8.600E-01 2.324E-01 U-235 1.909E-Ol 3.145E-01 U-238 2.424E+OO 2.708E+OO AM-243 6.366E-02 1. 075E-01 CM-247 6.324E-02 4.861E-02 ANH-511 l.255E-01 7.0lOE-02 Non-Identified Nuclides *Nuclide BE-7 NA-22 NA-24 Page 4405 of 5809 Key-Line Activity (pCi/GRAM 3.200E+OO 2.212E-02 -1.000E+41 K.L Act error (1.96-sigma) 9.087E+OO 4.505E-02 1.388E+41 TPU ( 1 . 96-sigma ) 1. 702E+OO 2.086E+OO 5.781E+02 1.341E-01 3.878E+Ol 8. 251E-02 1.421E-01 2.325E-01 l.876E-01 5.246E-01 2.325E-01 1.744E+OO 4.002E-01 4.002E-01 1. 421E-01 4. 727E-01 2.324E-01 6.797E-01 4.002E-01 2.708E+OO 2.324E-01 3.145E-01 2.708E+OO 1. 075E-01 4.861E-02 7.0lOE-02 TPU (1.96-sigma) 9.201E+OO 4.614E-02 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3.505E-02 3.870E-02 4.180E-02 NOT IDENT. SC-46 -3.425E-01 4.024E-01 4.310E-01 FAIL ABUN V-48 4.727E+Ol l.221E+04 l.221E+04 SHORT HLIF CR-51 4.340E+Ol 3.083E+02 3.090E+02 SHORT HLIF MN-54 7.283E-02 7.122E-02 7.842E-02 NOT IDENT. C0-56 -9.726E-02 5.283E-01 5.301E-01 NOT IDENT. MN-56 -l.000E+41 5.144E+41 O.OOOE+OO SHORT HLIF C0-57 1. 636E-02 4.904E-02 4.959E-02 NOT IDENT. C0-58 -9.557E-02 4.462E-01 4.483E-01 NOT IDENT. FE-59 8.441E+OO 6.624E+OO 7.639E+OO NOT IDENT. C0-60 -l.242E-02 3.932E-02 3.971E-02 NOT IDENT. ZN-65 7.991E-02 2.182E-01 2.212E-01 NOT IDENT. GE-68 l.089E+OO 1.922E+OO l.984E+OO NOT IDENT. . AS-73 1.684E+OO 1.375E+Ol 1.377E+Ol NOT IDENT. AS-74 3.817E+02 4.651E+03 4.654E+03 SHORT HLIF SE-75 -5.889E-02 l.904E-01 l.923E-01 FAIL ABUN BR-77 2.973E+37 2.520E+38 O.OOOE+OO SHORT HLIF SR-82 6.151E+02 3.823E+02 4. 723E+02 SHORT HLIF RB-83 5.872E-01 8.077E-01 8.500E-01 FAIL ABUN KR-85 6.739E+OO 6.698E+OO 7.355E+OO NOT IDENT. SR-85 6.637E-01 6.630E-01 7.274E-01 NOT IDENT. RB-86 1.616E+04 1.787E+04 l.930E+04 SHORT HLIF Y-88 -l.821E-01 1. 967E-01 2 .131E-01 NOT IDENT. Y-91 -2.375E+02 5. 231E+02 5.339E+02 NOT IDENT. NB-94 1. 32 6E-02 2.682E-02 2.748E-02 NOT IDENT. NB-95 l.592E-01 8.433E-01 8 .. 463E-01 NOT IDENT. NB-95M 2.462E-01 2.407E+OO 2.410E+OO NOT IDENT. ZR-95 2.142E-01 1.564E+OO 1.567E+OO NOT IDENT. NB-97 l.OOOE+41 7.694E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 7.676E+41 O.OOOE+OO SHORT HLIF M0-99 2.974E+31 3.905E+31 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 1.353E+41 O.OOOE+OO SHORT HLIF RH-101 -4.416E-02 3.374E-02 NOT IDENT. RH-102 3.669E-02 6.006E-02 6.230E-02 NOT IDENT. RU-103 -2.181E+OO 5.052E+OO 5.146E+OO FAIL ABUN RH-106 -3.128E-02 4.938E-01 4. 941E-01 NOT IDENT. RU-106 -3.128E-02 4.938E-01 4. 941E-01 NOT IDENT. AG-108M -4.664E-03 2 .191E-02 2.201E-02 NOT IDENT. AG-110M 5.776E-03 1.062E-01 l.062E-01 FAIL ABUN SN-113 -l.233E-01 l.937E-01 2.015E-01 NOT IDENT. CD-115 2.448E+38 -4. 696E+38 O.OOOE+OO SHORT HLIF. SN-117M 1.310E+04 7.518E+04 7.541E+04 SHORT HLIF TE-123M 8.559E-02 1.298E-01 l.354E-01 NOT IDENT. SB-12-4 -l.613E-01 2.258E+OO 2.259E+OO NOT IDENT. SB-125 9.090E-02 l.187E-01 l.256E-01 FAIL ABUN I-126 -4.375E+05 6.646E+05 6.933E+05 SHORT HLIF SB-126 -1. 847E+05 8 .11 7E+05 8.160E+05 SHORT HLIF SB-127 -1.244E+21 7.820E+21 O.OOOE+OO SHORT HLIF I-131 -l.666E+09 2.870E+09 2. 967E+09 SHORT HLIF I-132 -1. OOOE+41 1.814E+42 0.000E+OO SHORT HLIF TE-132 -5.729E+25 1. 145E+2 6 O.OOOE+OO SHORT HLIF BA-133 4.348E-02 3.891E-02 4.357E-02 NOT IDENT. I-133 l.000E+41 7.702E+41 O.OOOE+OO SHORT HLIF CS-134 5. 696E-02 1.0lOE-01 l.042E-01 FAIL ABUN CS-135 4.569E-03 l.301E-01 1. 301E-01 NOT IDENT. I-135 1.000E+41 7.470E+41 O.OOOE+OO SHORT HLIF CS-136 -1.183E+05 2.337E+05 2.397E+05 SHORT HLIF BA-137M 2.924E-02 4.051E-02 4.260E-02 NOT IDENT. CS-137 3.089E-02 4.279E-02 4.500E-02 NOT IDENT. CE-139 -8.175E-02 1.116E-01 l.175E-01 NOT IDENT. BA-140 1.573E+05 8.555E+05 8.584E+05 SHORT HLIF LA-140 6.169E+04 3.004E+05 3.017E+05 SHORT HLIF CE-143 1.000E+41 8.166E+40 O.OOOE+OO SHORT HLIF CE-144 6.516E-02 3.306E-01 3.319E-01 NOT IDENT. PM-144 l.627E-02 5.330E-02 5.3ff0E-02 NOT IDENT. PR-144 l.408E+00 4.615E+OO 4.658E+OO NOT IDENT. PM-146 -9.657E-03 4.266E-02 4.289E-02 FAIL ABUN ND-147 -2:092E+07 2.388E+07 2.567E+07 SHORT HLIF PM-147 3.574E+02 8.542E+02 8.693E+02 NOT IDENT. PM-149 -1.286E+39 6.984E+39 O.OOOE+OO SHORT HLIF EU-150 7.598E-03 2.569E-02 2.592E-02 FAIL ABUN EU-152 -5.850E-03 l.064E-01 l.064E-01 NOT IDENT. GD-153 7.267E-02 1.731E-01 1. 761E-01 NOT IDENT. EU-154 5.439E-02 1.108E-01 l.135E-01 NOT IDENT. EU-155 1.034E-01 l.161E-01 l.251E-01 FAIL ABUN TB-160 5. 961E-01 1. 754E+OO 1.774E+00 FAIL ABUN H0-166M *6.590E-02 7.208E-02 7. 796E-02 FAIL ABUN TM-171 -9.680E+OO 3.580E+Ol 3.607E+Ol FAIL ABUN Page 4406 of 5809 HF-172 1.058E-01 2.137E-01 2.190E-01 FAIL ABUN LU-172 -4.453E-02 8.219E-02 8.460E-02 FAIL ABUN LU-176 8.463E-03 2.023E-02 2.058E-02 FAIL ABUN HF-181 -2.553E-01 3.431E+00 3.433E+OO NOT IDENT. TA-182 2.742E-01 9. 965E-01 1.004E+OO FAIL ABUN RE-183 -5.749E-01 4.044E+OO 4.052E+00 FAIL ABUN RE-184 -8.429E+OO 2.813E+Ol 2.838E+Ol NOT IDENT. W-188 -8.826E+Ol l.093E+02 1.163E+02 FAIL ABUN IR-192 1.715E-02 4.312E-01 4. 313E-01 FAIL ABUN HG-203 -6.890E-01 l.883E+00 1.908E+OO NOT IDENT. BI-207 1.354E-02 5.154E-02 5.190E-02 FAIL ABUN PB-210 2.430E+OO 7.419E+OO 7.499E+OO NOT IDENT. BI-211 2.636E+OO 5.186E-01 1.296E+OO FAIL ABUN. PB-211 1. 031E+OO 9.166E-01 1.028E+OO FAIL ABUN BI-212 7. 967E-01 1. 071E+OO 1.129E+OO FAIL ABUN RA-223 2. 211E-01 5.557E-01 5.646E-01 FAIL ABUN AC-227 3.202E-02 2.304E-01 2.309E-01 FAIL ABUN TH-227 3.202E-02 2.304E-01 2.309E-01 FAIL ABUN TH-231 2. 211E-01 5.557E-01 5.646E-01 FAIL ABUN PA-233 9.428E-03 5.455E-02 5.471E-02 FAIL ABUN PA-234 -5.251E-02 2.894E-01 2.904E-01 FAIL ABUN PA-234M 9.446E+OO 4.816E+OO 6.428E+OO FAIL ABUN NP-237 9. *428E-03 5.455E-02 5. 471E-02 FAIL ABUN NP-238 1.001E+40 6.618E+40 O.OOOE+OO SHORT HLIF NP-239 -l.518E-01 2.461E-01 2.555E-01 NOT IDENT. PU-239 3.049E+02 2.956E+02 3.260E+02 NOT IDENT. AM-241 1. 400E-01 1.973E-01 2. 072E-01 NOT IDENT. CM-243 -4.340E-02 1. 028E-01 1. 046E-01 NOT IDENT. BK-247 -5.989E-03 6.502E-02 6.508E-02 FAIL ABUN CF-249 -8.-936E-03 3.329E-02 3.353E-02 NOT IDENT. CF-251 -8.984E-02 1.lSOE-01 1.220E-01 NOT IDENT. Page .4407 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.5689 87.09 53.8617 136.47 61.2174 45.60 47.9465 87.57 53.9151 140.51 0.0000 46.54 49.8688 *88.03 53.9656 143.76 69.4795 49. 72 0.0000 88.34 53.9998 144.24 67.3556 51. 35* 60.5342 88.47 54.0139 145.44 66.7464 51. 87 64.2452 89.96 54.1766 152.43 61.5482 52.39 55.2794 1093.63 54.2504 153.25 0.0000 52.97 47.2020 91.11 0.0000 323.87 67.2083 53.44 51. 8100 92.59 54.4606 156.02 0.0000 54.07 58.2764 93.35 54.5420 158.56 0.0000 57.36 0.0000 94.56 42.6699. 159.00 55.4504 57 .-53 58.8362 94.65 42.6774 162.33 66.8381 57.98 62.5892 94.67 42.6790 162.66 0.0000 59.27 52.6458" 94.87 42.6956 163.33 54.6570 59.32 52.6528 97.43 48.2692 165.86 70.5078 59.54 59.1533 98.43 60.4509 176.31 46.5041 60. 96 68.0330 98.44 60.4520 176.60 o*. 0000 61.17 68.0702 99.53 65.6244 177.52 64.7504 62. 93 59.6769 100 .11 65.6953 181.07 0.0000 63.29 59.7314 102.03 67.9584 181.52 66.9740 63.58 59.7755 103.18 69.1180 184.41. 64.1553 64.28 59.8813 103.37 69.1424 143.76 64.2578 66.73 57.7368 105.21 60.1920 193.51 52 .1157 67.24 54.0387 105.31 60.2028 197.03 58.1444 125.81 66.6775 106.12 .70. 8499 198.01 55.8816 67.75 66.6883 106.47 70.8943 201.83 56.1270 69.67 75.8466 109.28 65. 7 67 6 203.43 46.8573 70.83 66.5484 111. 00 65. 9658 205.31 51.6518 72.81 92. 9632 111.76 0.0000 210.85 51.9707 72. 87 92. 97 65 114.06 55.2616 215.65 52.2440 74.66 72.8967 116. 30 0.0000 222 .11 45.4329 74.82 72. 9234 116.74 69.7383 227.09 54.0843 74.97 72.9483 119. 76 70.0895 227.38 54.1008 77 .11 73.3003 121.12 60.8099 228.16 0.0000 78.74 60.6591 121.22 60.8201 228.18 64.9753 79.69 55.6121 121.78 68.2224 116.74 64.9753 80.12 64.7257 122.06 63.0034 235.69 50.1189 80.19 0.0000 122.92 66.2458 235. 96 50.1322 80.57 62.1973 123.07 65.2104 238.63 43.7816 81. 00 60.9584 265.00 62 .1163 238.98 0.0000 81. 07 50.5900 125.81 49.6517 240.99 43.8849 81. 75 61. 0564 127.23 75.1742 242.00 43.9294 83.79 65.2359 127.91 78.4353 244.70 32.6274 84.00 70.4861 129.30 48.8631 252.40 0.0000 85.43 74.6246 131.20 67.1201 252.80 40. 6961 86.55 51.1776 133.02 65.1709 254.15 0.0000 86.79 51.2026 133.52 53.4599 256.23 39.5928 86. 94 51. 2188 136.00 54.7346 260.90 0.0000 Page 4408 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.1668 355.39 0.0000 584.27 13.9098 264.80 31.1829 356.01 17.4886 595.83 0.0000 265.00 31.1882 364.49 0.0000 427.87 18.6980 268.22 33.7838 366.42 0.0000 602.52 0.0000 269.46 32.5698 372.51 19.9702 604.72 20.2974 270.03 32.5865 375.05 31. 8291 607.14 28.1371 271.23 27.6041 377.52 30.0627 609.32 18.7786 273.65 0.0000 356.01 30.1976 610.33 18.7874 276.40 35.2974 388.16 25.6997 614.28 17.2553 277.37 44.5807 388.63 0.0000 618.01 17.8100 277.60 44.5894 391.69 26.6825 620.36 18.8789 278.00 34.5062 264.66 26.8471 621.93 15.7446 279.20 37. 0713 401.81 26.8677 630.19 0.0000 279.54 48.8809 402.40 26.8789 631.29 13.7067 279.70 50.5737 404.85 26.9232 633.25 22.1621 280.46 47.2340 410.95 23.4912 634.78 0.0000 283.69 42.2943 413. 71 26.1492 635.95 14.7935 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 47.4414 423.72 0.0000 645.85 15.9241 285. 9.0 0.0000 427.09 27.3214 657.76 22.4167 287.50 39.8905 427.87 28.2776 657.90 0.0000 290.67 44.6814 433.94 17.0328 661. 66 19.2488 293.27 0.0000 439.40 26.5872 664.57 0.0000 351.93 35.8853 453.88 24.9124 666.33 0.0000 295. 96 35.9083 463.37 20.2386 666.50 0.0000 879.38 15.4237 468.07 23.1958 667.71 0.0000 299.98 42.4655 473.00 0.0000 677. 62 11. 3101 300.09 42.4696 475.06 23.2930 685.70 0.0000 300.13 42.4706 476.78 18.4592 695.00 0.0000 301.36 46.3799 477.60 12.6361 696.49 14.1204 302.85 20.6392 482.18 17.5437 696. 51 14.1209 256.23 38.7524 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.0391 306.78 24.1588 497.08 23.5947 697.49 14.1267 308.46 25.0564 505.52 16.2996 702.65 9.8020 311. 90 31.1931 507.63 0.0000 706.68 9.8192 316.51 36.5295 511. 00 15.8548 711. 68 24. 6011 319.41 0.0000 514.00 15.8815 **720.70 0.0000 320.08 0.0000 514.00 15.8815 721. 93 . 0.0000 321.04 30.5524 520.40 16.9343 722.78 8.2397 323.87 30.6222 520.69 0.0000* 722.91 9.8881 325.23 42.9179 52.2. 65 0.0000 723.31 9.8899 328.76 0.0000 527.90 0.0000 724.19 21. 4360 333.37 34.3789 528.26 16.0072 727.33 13.2090 333.97 29.1033 529.59 17.0201 733.00 19.8611 334.37 34.4059 529.87 0.0000 735.93 17.6758 338.28 33.6257 531.02 0.0000 333.97 19.8984 338.32 33.6265 537.26 0.0000 739.50 0.0000 311. 90 33.6829 546.56 0.0000 747.24 4.9949 340.48 33.6829 552.55 19.2582 748.06 9.9932 340.55 0.0000 563.25 22.4243 752.31 15. 5723 344.28 37.3370 569.33 14.3150 753.82 0.0000 345.93 30.2633 946.00 14.3162 756.73 17.8294 351. 06 33.9551 569.70 14.3179 756.80 17.8301 351. 93 33.9767 583.19 23.6851 884.68 15.6469 Page 4409 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 16.7773 1274.44 7.2983 1620.50 3.2291 766.42 19.0185 1001.03 7.3098 1621. 92 6.4603 766.84 16 .1127 1002.74 8.7765 1678.03 0.0000 772.60 0.0000 1004.73 11.7098 1690.97 5.4636 776.52 0.0000 507.63 0.0000 1750.46 0.0000, 739.50 0.0000 1025.87 o. o*ooo 1764.49 3.5500 778.90 11. 8061 1028.54 0.0000 1063.66 2.2214 783.70 0.0000 1037.84 12.9447 1771.35 1.1110 785.37 12.4005 1038.76 0.0000 i791.20 0.0000 792.07 10.1730 631.29 10.1984 1808.65 7.8348 794.95 13.5791 1048.07 0.0000 1810.72 0.0000 795.86 15.2820 1049.04 12.0621. 1836.06 5.4015 810.06 12.5214 1050.41 14.8525 810.29 12.5227 1063.66 12.1177 344.28 9.1077 1077.00 0.0000 810.76 9.1090 1077.34 5.6162 815.77 0.0000 1085.87 11.2617 1048.07 0.0000 1093.63 15.9925 832.01 11.4795 1099.45 6. 5967 834.85 11. 4917 1112. 07 18.9197 835.71 13.7949 1112.84 18.3827 836.80 0.0000 1115. 54 13. 6362 846.75 0.0000 1120.29 13.2762 846.77 18.4701 1120.55 13.2771 856.80 0.0000 1221. 41 13.2797 860.56 12.7635 1129. 67 12.3621 871. 09. 20.9663 1131. 51 0.0000 873.19 17.4854 1147.95 0.0000 875.33 0.0000 1173.23 17.3353 879.38 11.3913 1177.95 5.7861 880.51 10.5194 1189.05 17.4133 883.24 19.3044 1204.77 15.5469 884.68 14.9248 1221.41 13.6667 889.28 21.1055 1231.02 13.7026 894.76 15.8604 : 1235.36 0.0000 898.04 14. 9964 1238.28 16.6721 900. 72 12.3619 1260.41 0.0000 903.28 15.1507 1271.87 15.8350 911.20 9.7492 1274.44 6.9325 912.08 9.7522 1274.54 6.9325 923.98. 0.0000 1291.59 6. 9641 926.50 7.1284 1298.22 0.0000 929 .11 11. 5940 1312 .11 0.0000 937.49 11. 6277 1332.49 9.0500 944.13 0.0000 1362. 66 0.0000 946.00' 14.3530 1365.19 5.0696 949.00 10.7758 1368.63 0.0000 667. 71 0.0000 1384.29 4.0752 962.31 16.2367 1408.01 8.1982 964. 08 10.1090 1457.56 0.0000 966.17 17.3420 1460.82 1.0. 3796 911. 20 22.6021 1489.16 4.1797 968.97 22.6021 1505.03 9.4389 983.53 *o. 0000 1584.12 9.6103 984.45 0.0000 1596.21 0.0000 Page 4410 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:47:05.68 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Z-OCT-2016 11:00:01. Sample date 14-DEC-2015 13:25:00 Acquisition date : 3-0CT-2016 05:44:14. Sample ID G405235064 Sample quantity : 1.74637E+02 GRAM Detector name : GAM02 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.40 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit : 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 0 0 2 2 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Q 0 0 0 Page 4411 of 5809 Energy 63.31* 69.84* 74.62* 77.01 84.14* 87.30 89.95 92.51* 128.68 185.97* 209.88 238.55* 241. 65 269.89 276.36 294.95 299.94 315.18 338.30* 351 .. 90* 403.01 438.14 511. 01* 528.15 583.31* 597.29* 609.23* 726.96 793.58 835.02 838.66 859.44* 911. 40* 953.87 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 47 31 111 151 56 57 72 97 33 105 47 398 114 26 25 168 61 13 70 290 12 14 34 18 121 10 204 56 39 18 12 20 81 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 136 203 182 160 149 159 100 159 132 145 118 75 92 99 108 93 42 55 89 62 51 29 55 30 31 28 26 26 12 9 8 24 17 13 1. 09 1. 45. 1. 33 1. 47 1. 31 1.13 1. 08 1. 37 0.62 1. 44 0.87 1. 44 1. 65 1.25 3.45 1.20 2.83 2.17 1. 01 1. 33 L34 1. 83 1. 73 3.38 1. 36 1. 89 1. 71 1.16 4.48 1. 57 0.57 0. 96 1. 69 2.61 12 6. 12 139.18 148.73 153.51 167.76 174.06 179.37 184.48 256.75 371. 24 419.00 476.30 482.49 538.93 551.85 589.00 598.97 629.42 675.63 702.80 804.94 875.14 1020.76 1055.03 1165.26 1193. 20 1217.06 1452.3Z! 1585.49 1668.29 1675.58 1717.11 1820.94 1905.84 123 135 135 135 165 172 177 177 252 367 414 469 469 536 547 582 595 624 . 670 696 799 871 1014 1049 1157 1185 1212 1446 1579 1665 1672 1710 1814 1900 8 l.30E-02 48.5 22 8.52E-03 85.4 22 3.09E-02 24.2 22 4.19E-02 16.5 7 1.55E-02 39.7 6 1. 58E-02 37. 3 13 2. OlE-02 21. l 13 2.69E-02 27.9 8 9.llE-03 63.2 12 2.91E-02 26.4 10 1.29E-02 46.3 19 1. lOE-01 6. 5 19 3.18E-02 18.9 8 7.13E-03 70.2 11 6.97E-03 82.4 13 4.67E-02 14.2 8 1. 69E-02 22. 5 8 3. 63E-03101. 4 12 1.95E-02 29.9 15 8.07E-02 8.5 10 3.40E-03112.0 8 4.00E-03 69.1 13 9.44E-03 56.1 11 4.88E-03 65.2 16 3.36E-02 14.1 10 2.84E-03107.0 12 5.67E-02 8.8 12 l.55E-02 23.0 12 1. 08E-02 23. 9 8 5.06E-03 36.0 8 3.33E-03 50.0 14 5.45E-03 58.9 15 2.24E-02 16.6 12 3.94E-03 56.0 Fit 1.69E+OO 3.86E+OO 1. 64E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969.35* 39 32 1. 51 1936.78 1929 14 1. 09E-02 35.9 36 0 1003.26 33 9 1. 70 2004.55 1997 18 9.17E-03 27.5 37 0 1058.18 12 8 1. 80 2114. 32 2110 9 3.35E-03 52.6 38 0 1074.10 17 13 3.21 2146.13 2139 14 4.76E-03 51. 9 39 0 1087.17 8 13 0.74 2172.26 2163 11 2.12E-03100.3 40 0 1119.91* 64 10 2.42 2237.70 2230 14 1.78E-02 17.0 41 0 1125. 22 18 7 2.73 2248.31 2244 10 5.00E-03 36.7 42 0 1232.75 9 14 0.90 2463.23 2457 10 2.49E-03 86.8 43 0 1334. 41 9 7 3.85 2666.45 2661 12 2.60E-03 62.2 44 0 1379.13 12 17 2. 96 2755.82 2748 14 3.32E-03 79.5 45 0 1460.70* 341 11 1. 94 2918.88 2911 15 9.47E:..._02 5.9 46 0 1589.05 9 6 1. 46 3175.44 3166 11 2.43E-03 62.8 47 0 1764.11* 36 0 2.29 3525.39 3518 13 9.98E-03 .18.8 48 0 1847.41 11 0 1.24 3691.91 3687 9 3.06E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 4412 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:47:08 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 14-DEC-2015 13:25:00 G405235064 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 05:44:14 174.64 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA2 0 01:00:00.00 1. 50 keV No, Linear 75.00 Interference Report Interfering Nuclide Page 4413of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87 .. 57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:00.40 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.059E+OO l.272E+Ol 1. 272E+Ol 11. 85 OK MN-54 834.85 99.98* l.673E+OO 4.977E-02 9.556E-02 71. 97 OK CD-109 88.03 3.70* 4.852E+OO 8.019E-01 1.247E+OO 182. 02 OK SN-126 64.28 9.60 2.482E+OO 1.218E+OO l.218E+OO 97.07 OK 86.94 8.90 4.852E+OO 3.334E-01 3.334E-01 182.02 OK 87.57 37.00* 4.852E+OO 8.019E-02 8.019E-02 182.02 OK TL-208 277.37 6.60 4.186E+OO 4.795E-01 4.795E-01 164.82 OK 583.19 85.00* 2.233E+OO 3.057E-01 3.057E-01 28.18 OK 860.56 12.50 1.635E+00 4. 371E-01 4.371E-01 117.87 OK BI-211 72. 87 1. 23 3.574E+OO Line Not *Found Absent 351. 06 12.92* 3.417E+OO 5.lOOE-02 5.lOOE-022158.25 OK PB-212 74.82 10.28 3.755E+OO 1.086E+OO 1. 086E+OO 80.71 OK 77 .11 17.10 3.991E+OO 1.347E+OO 1.347E+OO 33.05 OK 238.63 43.60* 4.702E+OO 1.042E+OO 1.042E+OO 13.04 OK 300.09 3.30 3.912E+00 2.461E+OO 2.461E+OO 44.99 OK BI-214 609.32 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 OK 1120.29 14.92 1.323E+OO 1.424E+OO 1.425E+OO 34.02 OK 1764".49 15.30 8.933E-01 1.075E+OO 1. 075E+OO 37.62 OK PB-214 7'4.82 5.80 3.775E+00 Line Not Found <<INT Reject 77 .11 9.70 3.991E+OO. 2.375E+00 2.375E+OO 33.05 OK 87.09 3.41 4.837E+OO Line Not Found <<INT Reject 242.00 7.25 4. 651E+OO Line Not Found <<INT Reject 295.22 18.42 3. 967E+OO l.204E+00 l.205E+OO 28.34 OK 351. 93 35.60* 3.416E+OO Line Not Found <<INT Reject RN-219 271.23 10.80 4.267E+OO 2.947E-01 2.947E-01 140.49 OK 401.81 6.60* 3.043E+OO 3.069E-01 3.069E-01 224.08 OK RN-222 609.32 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 OK 1120.29 14.92 l.323E+OO l.424E+OO l.425E+00 34.02 OK 1764.49 15.30 8.933E-01 l.075E+OO 1.075E+OO 37.62 OK RA-224 240.99 4.10* 4.656E+OO 1.086E+OO 1.086E+00 125.05 OK RA-226 609.32 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 OK 1120. 29 14.92 l.323E+OO l.424E+OO 1.425E+OO 34.02 OK 1764.49 15.30 8.933E-01 l.075E+OO 1.075E+OO 37.62 OK AC-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO 9.078E-01 9.078E-Ol 59.76 OK 794.95 4.25 1.742E+00 2.423E+OO 2.423E+OO 47.83 OK 835.71 1. 61 1. 673E+OO 3.090E+OO 3.090E+OO 71. 97 OK 911.20 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 OK 968.97 15.80 1.486E+OO 7.497E-01 7.497E-01 71. 73 OK RA-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 OK 794.95 4.25 1. 742E+OO 2.423E+OO 2.423E+00 47.83 OK 835.71 1. 61 1. 673E+00 3.090E+OO 3.090E+OO 71.97 OK 911. 20 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 OK 968. 97 15.80 l.486E+OO 7.497E-01 7.497E-01 71. 73 OK TH-228 74.82 10.28 3.755E+OO 1. 086E+OO 1. 08 6E+OO 80.71 OK 77.11 17.10 3.991E+OO 1.347E+OO 1. 34 7E+00 33.05 OK 238.63 43.60* 4.702E+OO 1.042E+OO l.042E+00 13.04 OK 300.09 3.30 3.912E+OO 2.461E+OO 2.461E+OO 44.99 OK Page 4414of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide* Energy %Abn %Eff pCi/G.RAM pCi/GRAM %Error Status TH-229 85.43 14.70 4.615E+OO 4. 966E-01 4.967E-01 79.31 OK 88.47 24.00 4.852E+OO 1. 236-E-01 1.236E-01 182.02 OK 193.51 4.41* 5.427E+OO Line Not Found Absent 210.85 2.80 5.154E+OO 1. 760E+OO 1. 760E+OO 92. 62 OK TH-230 609.32 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 OK 1120.29 14.92 l.323E+OO 1.424E+OO 1.424E+OO 34.02 OK 1764.49 15.30 8.933E-01 1.075E+OO 1.075E+OO 37.62 OK PA-231 283.69 1. 70 4.097E+OO Line Not Found Absent 301.36 5.35* 3.912E+00 1.518E+OO 1.518E+OO 44.99 OK TH-232 105.21 1.10 5.776E+00 Line Not Found Absent 338.32 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 OK 835.71 1. 61 1. 673E+00 3.090E+OO 3.090E+OO 71. 97 OK 911.20 25.80* 1. 561E+OO 9.028E-01 9.028E-01 33.11 OK 968. 97 15.80 1. 486E+OO 7.497E-01 7.497E-01 . 71. 73 OK TH-234 63.29 3.70* 2.482E+OO 3.160E+OO 3.160E+OO 97.07 OK 92.59 4.23 5.192E+OO 2.639E+OO 2.639E+OO 55.72 OK U-234 609.32 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 OK 1120.29 14.92 1. 323E+OO 1.424E+OO 1. 424E+OO 34.02 OK 1764.49 15.30 . 8. 933E-01 . 1. 075E+OO 1.075E+OO 37.62 OK U-235 89. 96 3.47 5.033E+OO 2.479E+OO 2.479E+OO 42 .11 OK 93.35 5.60 5.192E+OO 1.994E+OO 1.994E+OO 55. 72 OK 143.76 10. 96* 6.127E+OO Line Not Found Absent 163.33 5.08 5.908E+OO Line Not Found Absent 185.72 57.20 5.554E+OO 1.823E-01 1.823E-01 52.89 OK 205.31 5.01 5. 230E+OO . Line Not Found Absent U-238 63. 29 3.70* 2.482E+OO 3.160E+OO 3.160E+OO 97.07 OK 92.59 4.23 5.192E+00 2.639E+OO 2.639E+OO 55. 72 OK AM-243 43.53 5;90 2.878E-01 Line Not Found Absent 74.66 67.20* 3.755E+OO 1.661E-01 1.661E-01 80.71 OK CM-247 278.00 3.40 4.166E+OO Line Not Found Absent 287.50 2.00 4.052E+OO Line Not Found Absent 402.40 72. 00* 3.043E+OO 2.813E-02 2.813E-02 224.08 OK ANH-511 511. 00 100.00* 2.490E+OO 6.665E-02 6.665E-02 112. 29 OK Flag: "*" = Keyline Page 4415 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:47:09.75 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l * *Acquisition date 3-0CT-2016 05:44:14 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
Sample date 14-DEC-2015 13:25:00 Analyst initials: MXRl * *Sample ID G405235064 Sample Quantity 1.7464E+02 GRAM *
Batch Number 1596254 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0'.00000 *
Nuclide LiQrary : SOLID.NLB;6 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.'GAMMA]EFF GAM02 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 272E+Ol 1. 477E+OO MN-54 9.556E-02 6.740E-02* CD-109 1. 24 7E+OO 2.224E+OO SN-126 8.019E-02 l.430E-01 TL-208 3.057E-01 8.443E-02 BI-211 5.lOOE-02 1.079E+OO PB-212 1.042E+OO 1.331E-01 BI-214 9.937E-01 1. 713E-01 PB-214 1.223E+OO 2.035E-01 RN-219 3.069E-01 6.739E-01 RN-222 9.937E-01 1. 713E-01 RA-224 1. 086E+OO 1. 331E+OO RA-226 9.937E-01 1. 713E-01 AC-228 9.028E-01 2.929E-01 RA-228 9.028E-01 2.929E-01 TH-228 1.042E+OO 1. 331E-01 TH-229 1.250E-01 4.421E-01 TH-230 9.933E-01 1. 713E-01 PA-231 1.518E+OO 6.692E-01 TH-232 9.028E-01 2.929E-01 TH-234 3.160E+OO 3.006E+OO 9.933E-01 1.713E-01 U-235 -7. 491E-02 l.838E-01 U-238 3.160E+OO 3.006E+OO AM-243 l.661E-01 1.3l4E-01 CM-247. 2. 813E-02 6.177E-02 ANH-511 6.665E-02 7.334E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4416of5809 Key-Line Activity (pCi/GRAM 1.088E+Ol -l.702E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.085E+Ol 4. OOlE-02 1.251E+41 MDA (pCi/GRAM 7.189E-01 l.149E-01 1. 967E+OO 1.508E-01 5.768E-02 3.163E-01 8.452E-02 1. 291E-01 3.143E-01 6.562E-01 1.291E-01 9.062E-01 1.291E-01 2.437E-01 2.437E-01 8.452E-02 9.032E-01 1.291E-01 7 .117E-01 2.437E-01 2.481E+OO 1. 291E-01 3.330E-01 2. 481E+OO 9.466E-02 6.023E-02 5.493E-02 MDA (pCi/GRAM 2.334E+Ol 7.256E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -9.232E-03 2.320E-02 4.616E-02 NOT IDENT. SC-46 -1.475E-02 3.957E-01. 7.508E-01 FAIL ABUN V-48 O.OOOE+OO 1.085E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 3.364E+02 O.OOOE+OO SHORT HLIF C0-56 -2.600E-01 3.995E-01 7.243E-01 NOT IDENT. MN-56 O.OOOE+OO 1.518E+41 O.OOOE+OO SHORT HLIF C0-57 -6. 523E-03* 4.895E-02 9.082E-02 NOT IDENT. C0-58 3.314E-01 5.276E-01 1.143E+OO NOT IDENT. FE-59 -1. 219E+OO 6.200E+OO l.175E+Ol NOT.IDENT. C0-60 2.207E-02 3. 626E-02 7.555E-02 NOT IDENT. ZN-65 4.758E-02 1.785E-01 3.255E-01 NOT IDENT. GE-68 -1.153E+OO 2.337E+OO 3.562E+OO NOT IDENT. AS-73 -1.207E+Ol 1.115E+Ol 2.043E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.512E+03 O.OOOE+OO SHORT HLIF SE-75 -2.044E-01 1. 851E-01 3.319E-01 NOT IDENT. BR-77 O.OOOE+OO 3.984E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.435E+02 O.OOOE+OO SHORT HLIF RB-83 -l.391E-01 5. 710E-01 1.064E+OO FAIL ABUN KR-85 6.033E+OO 7.159E+OO 1.380E+Ol NOT IDENT. SR-85 5.946E-01 7.088E-01 1.366E+OO NOT IDENT. RB-86 O.OOOE+OO 2.096E+04 O.OOOE+OO SHORT HLIF Y-88 -9.246E-02 1.747E-01 3.255E-01 NOT IDENT. Y-91 -9. 496E+Ol 5.123E+02 9.572E+02 NOT IDENT. NB-94 3.664E-03 2.747E-02 5.653E-02 NOT IDENT. NB-95 -8.729E-01 8.362E-01 1.457E+OO NOT IDENT. NB-95M 2.955E-01 2.090E+OO 3.799E+OO NOT IDENT. ZR-95 8.121E-01 1.261E+OO 2.744E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.404E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.338E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.122E+41 O.OOOE+OO SHORT HLIF RH-101 5.339E-02 6. 611E-02 5.970E-02 FAIL ABUN RH-102 4.409E-02 5.775E-02 l.210E-01 NOT IDENT. RU-103 3.718E+OO 4.577E+00 9.788E+OO FAIL ABUN RH-106 -4.159E-01 5.380E-01 9.006E-01 NOT IDENT. RU-106 -4.159E-01 5.380E-01 9.006E-01 NOT IDENT. AG-108M 5.923E-04 2.712E-02 4.742E-02 NOT IDENT. AG-llOM 8.109E-02 9.835E-02 2.165E-01 NOT IDENT. SN-113 -1.032E-01 2.043E-01 3.756E-01 NOT IDENT. CD-115 O.OOOE+OO 8.051E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 6.476E+04 O.OOOE+OO SHORT HLIF TE-123M 4.731E-02 1.162E-01 *2.425E-01 NOT I DENT. SB-124 -2.392E-01 1.213E+OO 2. 681E+OO NOT IDENT. SB-125 -3.662E-02 9.281E-02 1. 719E-01 NOT IDENT. TE-125M -2.925E+02 2.589E+02 4.455E+02 NOT IDENT. I-126 O.OOOE+OO 6.235E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.780E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.450E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.725E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO 9.878E+25 O.OOOE+OO SHORT HLIF BA-133 -1.518E-02 4.015E-02 6.663E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.298E-02 5.356E-02 1.068E-01 NOT IDENT. CS-135 1.528E-01 1.562E-01 3.015E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2. 031E+05 0.000E+OO SHORT HLIF BA-137M -3. 502E-0.3 3.806E-02 7.222E-02 NOT IDENT. CS-137 -3.700E-03 4. 021E-02 7.629E-02 NOT IDENT. CE-139 -4.424E-03 l.005E-01 2.034E-01 NOT IDENT. BA-140 O.OOOE+OO 9. 511E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2. 471E+05 O.OOOE+OO SHORT HLIF CE-141 7.282E-01 2.150E+Ol 3.986E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.038E+40 O.OOOE+OO SHORT HLIF CE-144 -1.791E-01 3.233E-01 5.761E-01 NOT IDENT. PM-144 -L 047E-02 4.936E-02 9.708E-02 NOT IDENT. PR-144 -9.336E-01 4.269E+OO 8.391E+OO NOT IDENT. PM-146 1.112E-02 4.142E-02 8.249E-02 NOT IDENT. ND-147 O.OOOE+OO 2.362E+07 O.OOOE+OO SHORT HLIF PM-147 6.477E+02 8 .134E+02 1.625E+03 NOT IDENT. PM-149 O.OOOE+OO 6.019E+39 O.OOOE+OO SHORT HLIF. EU-150 4.356E-03 4.795E-02 FAIL ABUN . EU-152 2.032E-02 8.833E-02 1. 763E-01 FAIL ABUN GD-153 3.802E-02 1.813E-01 3.527E-01 FAIL ABUN EU-154 -3. 965E-02 9.886E-02 1.803E-01 FAIL ABUN EU-155 -7.531E-03 1.115E-01 2.103E-01 FAIL ABUN TB-160 6.434E-01 1.659E+OO 3.503E+OO FAIL ABUN H0-166M 4.141E-02 5.548E-02 1.204E-01 NOT IDENT. Page 4417 of 5809 TM-171* -3.264E+OO 2.766E+Ol 5.478E+01 NOT IDENT. HF-172 -3.543E-02 2.395E-01 4.074E-01 FAIL ABUN LU-172 4.526E-02 7.501E-02 1.603E-01 FAIL ABUN LU-176 3.419E-03 2.244E-02 4.478E-02 FAIL ABUN HF-181 1. 829E+OO 3. 811E+OO 7.745E+00 NOT IDENT. TA-182 -l.155E-01 8.680E-01 1. 641E+OO FAIL ABUN RE-183 -1. 8 69E+OO 3.170E+OO. 6.016E+OO NOT IDENT. RE-184 2.810E+Ol 2.895E+Ol 6.354E+Ol NOT IDENT. W-188 -2.330E+Ol l.129E+02 1.943E+02 FAIL ABUN IR-192 3.450E-01 6.857E-01 7. 965E-01 FAIL ABUN HG-203 -6.008E-01 2.439E+OO 4.185E+OO FAIL ABUN BI-207 -2.806E-02 4.443E-02 7.019E-02 FAIL ABUN PB-210 1.929E+OO 5.088E+OO 1. 041E+Ol NOT IDENT. PB-211 5.414E-02 6.578E-01 1.161E+OO NOT IDENT. BI-212 O.OOOE+OO 9.352E-01 1.426E+OO FAIL ABUN RA-223 -1.002E-01 5.604E-01 l.079E+OO FAIL ABUN AC-227 -3.852E-02 2.002E-01 3.924E-01 FAIL ABUN TH-227 -3.852E-02 2.002E-01 3.924E-01 FAIL ABUN TH-231 -l.002E-01 5.604E-01 l.079E+00 FAIL ABUN PA-233 -1.392E-02 5.856E-02 1.013E-01 FAIL ABUN PA-234 7.504E-02 2.552E-01 5.316E-01 NOT IDENT. PA-234M -9.695E-02 4.935E+OO 9.043E+OO NOT IDENT. NP-237 -1.392E-02 5.856E-02 1.013E-01 FAIL ABUN NP-238 O.OOOE+OO 6.697E+40 O.OOOE+OO SHORT HLIF NP-239 -9.472E-02 2.333E-01 4.260E-01 FAIL ABUN PU-239 4.859E+02 6.018E+02 6.403E+02 FAIL ABUN AM-241 9.787E-02 1.635E-01 3.158E-01 NOT IDENT. CM-243 -2.158E-02 9.944E-02 1. 8 60E-01 FAIL ABUN BK-247 -8.514E-02 6.822E-02 l.207E-01 FAIL ABUN CF-249 3.085E-02 3.463E-02 7.356E-02 NOT IDENT. CF-251 -5.730E-03 1.044E-01 2.106E-01 NOT IDENT. Page 4418of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-'-2016 06:47:06.52 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 334 10.66* 1.059E+OO 1. 272E+Ol 1.272E+Ol 11. 85 MN-54 834.85 19 99.98* 1.673E+OO 4.977E-02 9.556E-02 71. 97 CD-109 88.03 80 3. 70.* 4.852E+OO 1.912E+OO 2.972E+OO 74.55 SN-126 64.28 68 9.60 2.482E+OO 1.218E+OO 1.218E+OO 97.07 86.94 80 8.90 4.852E+OO 7.949E-01 7.949E-01 74.55 87.57 80 37.00* 4.852E+OO 1.912E-01 1.912E-01 74.55 TL-208 277.37 31 6.60 4.186E+OO 4.795E-01 4.795E-01 164.82 583.19 135 85.00* 2.233E+OO 3.057E-01 3.057E-01 28.18 860.56 21 12.50 1.635E+OO 4.371E-01 4.371E-01 117. 87 BI-211 72.87 ------1. 23 3.574E+OO ------Line Not* Found ------351.06 346 12.92* 3.417E+OO 3.370E+OO 3.370E+OO 16.97 PB-212 74.82 158 10.28 3.755E+OO 1.765E+OO 1. 765E+OO 48.42 77 .11 214 17.10 3.991E+OO 1.347E+OO 1.347E+OO 33.05 238.63 497 43.60* 4.702E+OO 1.042E+OO 1.042E+OO 13. 04 300.09 74 3.30 3.912E+OO 2.461E+OO 2.461E+OO 44.99 BI-214 609.32 226 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 1120.29 65 14.92 1.323E+OO l.424E+00 1.425E+OO 34.02 1764.49 34 15 .*30 8.933E-01 1.075E+OO 1.075E+OO 37.62 PB-214 74.82 158 5.80 3.755E+OO 3.128E+OO 3.130E+OO 48.42 77 .11 214 9.70 3.991E+OO 2.375E+OO 2.375E+OO 33.05 87.09 80 3.41 4.852E+OO 2.075E+OO 2.075E+OO 74.55 242.00 143 7.25 4.656E+OO 1.819E+OO 1.819E+OO 37.83 295.22 205 18.42 3. 967E+OO 1.204E+OO 1.205E+OO 28.34 351. 93 346 35.60* 3.417E+OO 1.223E+OO 1.223E+OO 16.97 RN-219 271. 23 32 10.80 4.267E+OO 2.947E-01 2.947E-01 140.49 401.81 14 6.60* 3.043E+OO 3.069E-01 3.069E-01 224.08 RN-222 609.32 226 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 1120.29 65 14.92 1.323E+OO l.424E+OO l.425E+OO 34.02 1764.49 34 15.30 8.933E-01 1.075E+OO 1. 07 5E+OO 37.62 RA-224 240.99 143 4.10* 4.656E+OO 3.216E+OO 3.216E+OO 37.83 RA-226 609.32 226 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO 1.425E+OO 34.02 1764.49 34 15.30 8.933E-01 1. 075E+OO 1. 07 5E+OO 37.62 AC-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 84 11. 27 3.533E+OO 9.078E-01 9.078E-01 59. 76 794.95 42 4.25 1. 7 42E+OO 2.423E+OO 2.423E+OO 47.83 835.71 19 1. 61 1. 673E+OO 3.090E+OO 3.090E+OO 71. 97 911.20 85 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 968. 97 41 15. 80. l.486E+00 7.497E-01 7.497E-01 71.73 RA-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 84 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 794.95 42 4.25 1. 742E+OO 2.423E+OO 2.423E+OO 47.83 835. 71 19 1. 61 1. 673E+OO 3.090E+OO 3.090E+OO 71. 97 911.20 85 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 968.97 41 15.80 1.486E+OO 7.497E-01 7.497E-01 71. 73 TH-228 74.82 158 10.28 3.755E+OO 1. 765E+OO 1. 765E+OO 48.42 77 .11 214 17.10 3.991E+OO 1.347E+OO 1.347E+OO 33.05 Page 4419of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235064 Acquisition date 3-0CT-.2016 05:44:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 497 43.60* 4.702E+00 l.042E+00 1.042E+OO 13.04 300.09 74 3.30 3.912E+OO 2. 461E+OO 2. 461E+OO 44.99 TH-229. 85.43 78 14.70 4.615E+OO 4. 966E-01 4. 967E-01 79.31 88.47 80 24.00 4.852E+OO 2.948E-01 2.948E-01 74 .. 55 193.51 ------4.41* 5.427E+OO ------Line Not Found ------210.85 59 2.80 5.154E+OO 1.760E+OO 1. 760E+OO 92. 62 TH-230 609.32 226 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO 1.424E+OO 34.02 1764.49 34 15.30 8.933E-01 1. 075E+OO . 1. 075E+OO 37.62 PA-231 283.69 ------1. 70 4.097E+OO ------Line Not Found ------301.36 74 5.35* 3.912E+OO 1.518E+OO 1.518E+OO 44.99 TH-232 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 84 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 835.71 19 1. 61 1.673E+OO 3.090E+OO 3.090E+OO 71. 97 911. 20 85 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 968. 97 41 15.80 1. 486E+OO 7.497E-01 7.497E-01 71. 73 TH-234 63.29 68 3.70* 2.482E+OO 3.160E+OO 3.160E+00 97.07 92.59 135 4.23 5.192E+OO 2. 639E+OO . 2.639E+OO 55. 72 U-234 . 609.32 226 45.49* 2.155E+OO 9*. 933E-0rl 9.933E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO 1.424E+OO 34.02 .1764. 49 34 15.30 8.933E-01 1. 075E+OO 1. 07 5E+OO 37.62 U-235 89. 96 101 3.47 5.033E+00 2.479E+00 2.479E+OO 42 .11 93.35 135 5.60 5.192E+00 1.994E+OO 1.994E+OO 55.72 143.76 ------10.96* 6.127E+OO ------Line Not Found ------163.33 ------5.08 5.908E+00 ------Line Not Found ------185. 72 135 57.20 5.554E+OO 1.823E-01 l.823E-01 52.89 205.31 ------5.01 5.230E+OO ------Line Not Found ------U-238 63.29 68 3.70* 2.482E+OO 3.160E+00 3.160E+OO 97.07 92.59 135 4.23 5.192E+OO 2.639E+OO 2.639E+OO 55.72 AM-243 43.53 ------5.90 2.878E-01 ------Line Not Found ------74.66 158 67.20* 3.755E+OO 2.700E-01 2.700E-01 48.42 CM-247 278.00 ------3.40 4.166E+OO ------Line Not Found ------287.50 ------2.00 4.052E+OO ------Line Not Found ------402.40 14 72.00* 3.043E+00 2.813E-02 2.813E-02 224.08 ANH-511 511. 00 39 100.00* 2. 490E+OO. 6.665E-02 6.665E-02 112. 29 Flag: "*" Key line Page 4420 of 5809 Summary of Nuclide Activity Sample ID : G405235064 Acquisition date Page : 3 3-0CT-2016 05:44:14 Total number of lines in spectrum 48 Number of unidentified lines 9 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 MN-54 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214* PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH'--230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 . CM-24 7 ANH-511 Hlife 1.25E+09Y 312.050 461.40D 2.30E+05Y l.41E+l0Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 7.04E+08Y 1600.00Y 1.41E+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+l0Y 1. 41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y *7.04E+08Y 4.47E+09Y 7370.00Y l.56E+07Y l.00E+09Y Decay 1. 00 1. 92 1:55 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 272E+Ol 4.977E-02 1.912E+OO l.912E-01 3.057E-01 3.370E+OO l.042E+00 9.933E-01 l.223E+OO 3.069E-01 9.933E-01 3.216E+OO 9.933E-01 9.028E-01 9.028E-01 l.042E+OO 2.948E-01 9.933E-01 l.518E+00 9.028E-01 3.160E+OO 9.933E-01 l.823E-01 3.160E+OO 2.700E-01 2. 813E-02 6.665E-02 4.173E+Ol 4.173E+Ol Decay Corr pCi/GRAM 1.272E+Ol 9.556E-02 2.972E+OO 1.912E-01 3.057E-01 3.370E+OO 1.042E+OO 9.937E-01 l.223E+OO 3.069E-01 9.937E-01 3.216E+OO 9.937E-01 9.028E-01 9.028E-01 l.042E+OO 2.948E-01 9.933E-01 l.518E+OO 9.028E-01 3.160E+OO 9.933E-01 l.823E-01 3.160E+OO 2.700E-01 2.813E-02 6.665E-02 4.284E+Ol 4.284E+Ol 81.25% Decay Corr 2-Sigma Error 0 .151E+Ol 6.877E-02 2.216E+OO l.425E-01 0.862E-01 0.572E+OO 0.136E+OO 1.748E-01 0.208E+OO 6.876E-01 1. 748E-01 l.216E+OO 1. 748E-01 2.989E-01 2.989E-01 0.136E+OO 2.198E-01 l.748E-01 0.683E+00 2.989E-01 3.068E+OO l.748E-01 0. 964E-01 3.068E+00 l.308E-01 6.303E-02 7.484E-02 "M" Manually 2-Sigma %Error 11. 85 71. 97 74.55 74.55 28.18 16.97 13.04 17.59 16.97 224.08 17.59 37.83 17.59 33.11 33.11 13. 04 74.55 17.59 44.99 33 .11 97.07 17.59 52.89 97.07 48.42 224.08 112. 29 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4421 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235064 Acquisition date : 3-0CT-2016 05:44:14 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 69.84 44 291 1. 45 139.18 135 22 8.52E-03 **** 3.25E+OO T 0 128.68 44 177 0.62 256.75 252 8 9.llE-03 **** 6.17E+OO T 0 315.18 16 66 2.17 629.42 624 8 3.63E-03 **** 3.75E+OO T 0 438.14 17 33 1. 83 875.14 871 8 4.00E-03 **** 2.83E+OO T 0 528.15 20 34 3.38 1055.03 1049 11 4.88E-03 **** 2.42E+OO T 0 597.29 11 31 1. 89 1193.20 1185 10 2.84E-03 **** 2.19E+OO T 0 726.96 60 29 1.16 1452.34 1446 12 l.55E-02 45.9 1.87E+OO T 0 838.66 13 8 0.57 1675.58 1672 8 3.33E-03 **** 1.67E+OO 0 953.87 15 13 2.61 1905.84 1900 12 **** 1.51E+OO T 0 1003.26 34 9 1. 70 2004.55 1997 18 9.17E-03 55.0 1.45E+OO T 0 1058.18 12 8 1. 80 2114.32 2110 9 3.35E-03 **** 1.39E+OO 0 1074.10 18 13 3.21 2146.13 2139 14 4.76E-03 **** 1.37E+OO 0 1087.17 8 14 0.74 2172.26 2163 11 2.12E-03 **** 1.36E+OO T 0 1125. 22 18 7 2.73 2248.31 2244 10 5.00E-03 73.5 l.32E+00 0 1232.75 9 14 0.90 2463.23 2457 10 2.49E-03 **** 1. 22E+OO 0 1334.41 9 7 3.85 2666.45 2661 12 2.60E-03 **** 1.14E+OO 0 1379.13 12 17 2. 96 2755.82 2748 14 3.32E-03 **** 1. llE+OO 0 1589.05 8 6 1. 46 3175.44 3166 11 2.43E-03 **** 9.83E-01 0 1847.41 10 0 1. 24 3691.91 3687 9 3.06E-03 60.3 8.55E-01 Flags: "T" = Tentatively associated Page 4422 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:47:25.30 *******************************************************************************
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2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l * *Acquisition date 3-0CT-2016 05:44:14 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
Sample date 14-DE'C-2015 13:25:00 Nuclide Library : SOLID *
Sample ID G405235064 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.7464E+02 GRAM *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 22-AUG-2016 09:02:05. Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 3.073E-01 5.055E-02 9.283E-01 7.183E-02 2.564E-02 l.442E-01 3.922E-02 5.837E-02. 1.522E-01 2.976E-01 5.837E-02 4.205E-01 5.837E-02 1.070E-01 1.070E-01 3.922E-02 4.254E-01 5.835E-02 3.261E-01 1. 070E-01 l.170E+OO 5.835E-02 1. 571E-01 1.170E+OO 4.477E-02 2.732E-02 2.502E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4423 of 5809 Le (pCi/GRAM l.065E+Ol 3. OllE-02 O.OOOE+OO 1. 635E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 4424 of 5809 3.327E-01 O.OOOE+OO 0.000E+OO 3 .115E-Ol 0 .. OOOE+OO 4.284E-02 5.091E-Ol 5 .114E+OO 3.204E-02 1.424E-01 l.494E+OO 9.587E+OO O.OOOE+OO 1. 52 6E-01 O.OOOE+OO O.OOOE+OO 4.735E-01 6.304E+OO 6.238E-01 O.OOOE+OO 1.165E-01 4.193E+02 2.511E-02 6.479E-01 1.772E+OO 1.225E+OO O.OOOE+OO o*. OOOE+OO O.OOOE+OO O.OOOE+OO 2.805E-02 5.453E-02 4.424E+OO 4.005E-01 4.005E-01 2.133E-02 9.663E-02 1. 700E-01 0.000E+OO O.OOOE+OO l.143E-01 9.497E-01 7. 725E-02 2.088E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.022E-02 O.OOOE+OO 4.809E-02 l.417E-01 O.OOOE+OO O.OOOEtOO 3. 271E-02 3.456E-02 9.579E-02 O.OOOE+OO O.OOOE+OO 1.881E+Ol O.OOOE+OO 2.691E-01 4.304E-02 3. 719E+OO 3.746E-02 O.OOOE+OO 7.676E+02 O.OOOE+OO 2.215E-02 8.120E-02 l.669E-01 7.497E-02 9.927E-02 1.544E+OO 5.435E-02 2.577E+Ol FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.* NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT*IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. *NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI...:207 PB-210 PB-211 BI-212 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page.4425 of 5809 l.914E-01 7.073E-02 2.067E-02 3.519E+OO 7.150E-01 2.817E+OO 2.863E+Ol 9.006E+Ol 3.667E-01 l.948E+OO 2.921E-02 4.908E+OO 5.267E-01 6.646E-01 4.971E-01 l.814E-01 l.814E-01 4.971E-01 4.642E-02 2.329E-01 4.031E+OO 4.642E-02. O.OOOE+OO l.997E-01 3.038E+02 1. 48 9E-01 8.753E-02 5.555E-02 3.381E-02 9.890E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT-I DENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:47:31.94 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l *
Acquisition date 3-0CT-2016 05:44:14 Sensitivity : 3.000 *
Detector ID GAM02 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.40 Half life ratio : *
Sample date 14-DEC-2015 13:25:00 Nuclide Library : SOLID *
Sample ID G405235064 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity 1.7464E+02 GRAM *
Quantity Err(%) 1.1452E-03 % *
Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0. 00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * *
Eff. Cal. date 22-AUG-2016 09:02:05 'Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1. 272E+Ol l.619E+OO 1.619E+OO MN-54 9.556E-02 6.752E-02 6.752E-02 CD-109 1. 24 7E+OO 2.236E+00 2.236E+OO SN-126 8.019E-02 1.438E-01 1.438E-01 TL-208 3.057E-01 8.543E-02 8.543E-02 BI-211 5.lOOE-02 l.098E+OO 1.098E+OO PB-212 1.042E+OO l.442E-01 1.442E-01 BI-214 9.937E-01 l.766E-01 1. 766E-01 PB-214 l.223E+OO 2.098E-01 2.098E-01 RN-219 3.069E-01 6.750E-01 6.750E-01 RN-222 9.937E-01 1.766E-01 1.766E-01 RA-224 1.086E+OO 1.339E+OO 1.339E+OO RA-226 9.937E-01 l.766E-01 1. 766E-01 AC-228 9.028E-01 2.965E-01 2. 965E-01 RA-228 9.028E-01 2.965E-01 2. 965E-01 TH-228 l.042E+OO l.442E-01 1.442E-01 TH-229 1.250E-01 4.422E-01 4.422E-01 TH-230 9.933E-01 1. 765E-01 1. 765E-01 PA-231 l.518E+00 7.436E-01 7.436E-01 TH-232 9.028E-01 2. 965E-01 2. 965E-01 TH-234 3.160E+00 3.087E+OO 3.087E+OO U-234 9.933E-01 1.765E-01 1. 765E-01 U-235 -7.491E-02 1.839E-01 1.839E-01 U-238 3.160E+OO 3.087E+OO 3.087E+OO AM-243 l.661E-01 1. 324E-(H l.324E-01 CM-247 2.813E-02 6.195E-02 6.195E-02 ANH-511 6.665E-02 7.339E-02 7.339E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 1. 088E+Ol 1.086E+Ol 1.192E+Ol NOT IDENT. NA-22 -l.702E-02 4.00lE-02 4.074E-02 NOT IDENT. NA-24 l.OOOE+41 1.322E+41 O.OOOE+OO SHORT HLIF Page 4426 of 5809 AL-26 -9.232E-03 2. 321E-02 2.358E-02 NOT IDENT. SC-46 -1. 475E-02 3.957E-01 3.957E-Ol FAIL ABUN V-48 4.653E+03 1.085E+04 l.105E+04 SHORT HLIF CR-51 2.221E+02 3.366E+02 3.512E+02 SHORT HLIF C0-56 -2.600E-01 3.996E-01 4.165E-01 NOT IDENT. "MN-56 -l.OOOE+41 1.518E+41 O.OOOE+OO SHORT HLIF C0-57 -6.523E-03 4.895E-02 4.904E-02 NOT IDENT. C0-58 3.314E-01 5.278E-Ol 5.486E-01 NOT IDENT. FE-59 -1.219E+OO 6.201E+OO 6.225E+OO NOT IDENT. C0-60 2.207E-02 3.627E-02 3.761E-02 NOT IDENT. ZN-65 4.758E-02 l.785E-01 l.798E-01 NOT IDENT. GE-68 -l.153E+OO 2.337E+OO 2.394E+OO NOT IDENT. AS-73 -1.207E+Ol l.142E+Ol 1.265E+Ol NOT IDENT. AS-74 3.580E+03 7.517E+03 7.689E+03 SHORT HLIF SE-75 -2.044E-01 1.853E-01 2.070E-01 NOT IDENT. BR-77 3 .119E+37 2.644E+38 O.OOOE+OO SHORT HLIF SR-82 -2. 871E+o2 5.437E+02 5.588E+02 SHORT HLIF RB-83 -1. 391E-01 5.713E-01 5.748E-01 FAIL ABUN KR-85 6.033E+OO 7.163E+OO 7.662E+OO NOT IDENT. SR-85 5.946E-01 7.092E-01 7.581E-01 NOT IDENT. RB-86 -3.928E+03 2. 096E+04 2.103E+04 SHORT HLIF Y-88 -9.246E-02 1.748E-01 1. 797E-01 NOT IDENT. Y-91 -9. 496E+Ol 5.123E+02 5 .141E+02 NOT IDENT. NB-94 3.664E-03 2.747E-02 2. 752E-02' NOT IDENT. NB-95 -8. 729E-01 8.371E-01 9.250E-01 NOT IDENT. NB-95M 2.955E-01 2.090E+OO 2.094E+OO NOT IDENT. ZR-95 8 .121E-01 1.262E+OO 1.314E+OO NOT IDENT. NB-97 1.000E+41' 2.401E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 1.404E+41 O.OOOE+OO SHORT HLIF M0-99 1.398E+31 3.340E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.127E+41 O.OOOE+OO SHORT HLIF RH-101 5.339E-02 6.682E-02 7.102E-02 FAIL ABUN RH-102 4.409E-02 5.787E-02 6 .118E-02 NOT IDENT. RU-103 3.718E+OO 4.581E+OO 4.878E+00 FAIL ABUN RH-106 -4.159E-01 5.387E-01 5.704E-01 NOT IDENT. RU-106 -4.159E-01 5.387E-01 5.704E-01 NOT IDENT. AG-108M 5*. 923E-04 2.712E-02 2.712E-02 NOT IDENT. AG-llOM 8.109E-02 9.844E-02 1.050E-01 NOT IDENT. SN-113 -l.032E-01 2.044E-01 2. 096E-01 NOT IDENT. CD-115 6.303E+38 8.129E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 2.618E+04 6.483E+04 6.590E+04 SHORT HLIF 'TE_.:123M 4.731E-02 1.162E-01 1.181E-01 NOT IDENT. SB-124 -2.392E-01 l.213E+OO 1.218E+OO NOT IDENT. SB-125 -3.662E-02 9.282E-02 9.428E-02 NOT IDENT. TE-125M -2.925E+02 2.594E+02 2.910E+02 NOT IDENT. I-126 3.144E+05 6.250E+05 6.408E+05 SHORT HLIF SB-126 1. 351E+05 7.784E+05 7.808E+05 SHORT HLIF SB-127 -4.343E+21 8.707E+21 O.OOOE+OO SHORT HLIF I-131
1. 720E+09 2.726E+09 2.834E+09 . SHORT HLIF I-132 1.000E+41 1.827E+42 O.OOOE+OO SHORT HLIF TE-132 l.081E+26 1. 078E+26. O.OOOE+OO SHORT HLIF BA-133 -l.518E-02 4.015E-02 4.073E-02 FAIL ABUN I-133 1.000E+41 3.479E+41 O.OOOE+OO SHORT HLIF CS-134 4.298E-02 5.360E-02 5.699E-02 NOT IDENT. CS-135 1.528E-01 l.565E-01 1.710E-01 NOT IDENT. I-135 1.000E+41 7.010E+41 O.OOOE+OO SHORT HLIF CS-136 4.291E+04 2.032E+05 2. 041E+05 SHORT HLIF BA-137M -3.502E-03 3.806E-02 3.810E-02 NOT IDENT. CS-137 -3.700E-03 4. 021E-02 4.025E-02 NOT IDENT. CE-139 -4.424E-03 1.005E-01 .1.005E-01 NOT IDENT. BA-140 5.977E+05 9.515E+05 9.889E+05 SHORT HLIF LA-140 -2.225E+04 2.471E+05 2.473E+05 SHORT HLIF CE-141 7.282E-01 2.150E+Ol 2 .151E+Ol NOT IDENT. CE-143 l.000E+41 5 .136E+40 O.OOOE+OO SHORT HLIF CE-144 -1.791E-01 3.235E-01 3.334E-01 NOT IDENT .. PM-144 -1. 047.E-02 4.936E-02 4.959E-02 NOT IDENT. PR-144 -9.336E-01 4.270E+OO 4.290E+OO NOT IDENT. PM-146 l .112E-02 4.143E-02 4.173E-02 NOT IDENT. ND-147 6.753E+06 2.362E+07 2.382E+07 SHORT HLIF PM-147 6.477E+02 8.139E+02 8.647E+02 NOT IDENT. PM-149 -2.136E+39 6.037E+39 O.OOOE+OO SHORT HLIF EU-150 4.356E-03 2.689E-02 2.696E-02 FAIL ABUN EU-152 2.032E-02 8.834E-02 8.881E-02 FAIL ABUN GD-153 3.802E-02 1.813E-01 l.821E-01 FAIL ABUN EU-154 -3. 965E-02 9.887E-02 l.005E-01 FAIL ABUN EU-155 -7.531E-03 l .115E-01 1.116E-01 FAIL ABUN TB-160 6.434E-01 1. 660E+OO* l.685E+OO FAIL ABUN H0-166M 4.141E-02 5.553E-02 5.858E-02 NOT IDENT. Page 4427 of 5809 TM-171 -3.264E+OO 2.766E+Ol 2.770E+Ol NOT IDENT. HF-172 -3.543E-02 2. 396E-01 2. 401E-01 FAIL ABUN LU-172 *4.526E-02 7.515E-02 7.787E-02 FAIL ABUN LU-176 3.419E-03 2.244E-02 2.249E-02 FAIL ABUN HF-181 1. 829E+OO 3.812E+OO 3.900E+00 NOT IDENT. TA-182 -l.155E-01 8.680E-01 8. 696E-01 FAIL ABUN RE-183* -l.869E+OO 3.184E+OO 3.293E+OO NOT IDENT. RE-184 2.810E+Ol 2. 969E+Ol 3.228E+Ol NOT IDENT. W-188 -2.330E+Ol l.130E+02 l.134E+02 FAIL ABUN IR-192 3.450E-01 6.859E-01 7.033E-01 FAIL ABUN HG-203 -6.008E-01 2.440E+OO 2.455E+OO FAIL ABUN BI-207 -2.806E-02 4.444E-02 4.621E-02 FAIL ABUN PB-210. 1.929E+OO 5.091E+OO 5.165E+OO NOT IDENT. PB-211 5.414E-02 6.578E-01 6.583E-01 NOT IDENT. BI-212 *2.079E+OO 9. 411E-01 1.328E+OO FAIL ABUN RA-223 -l.002E-01 5.604E-01 5.622E-01 FAIL ABUN AC-227. -3.852E-02 2.003E-01 2.0lOE-01 FAIL ABUN TH-227 -3.852E-02 2.003E-01 2.0lOE-01 FAIL ABUN TH-231 -l.002E-01 5.604E-01 5.622E-01 FAIL ABUN PA-233 -1.392E-02 5.857E-02 5.890E-02 FAIL ABUN PA-234 7.504E-02 2.692E-01 2.713E-01 NOT IDENT. PA-234M -9.695E-02 4.935E+00 4.935E+00 NOT IDENT. NP-237 -l.392E-02 5.857E--:02 5.890E-02 FAIL ABUN NP-238 -1.062E+40 6.697E+40 0.000E+OO SHORT HLIF NP-239 -9. 472E-02 2.335E-01 2.373E-01 FAIL ABUN PU-239 4.859E+02 6.022E+02 6.408E+02 FAIL ABUN AM-241 9.787E-02 1.636E-01 l.695E-01 NOT IDENT. CM-243 -2.158E-02 9.946E-02 9.993E-02 FAIL ABUN BK-247 -8.514E-02 7.035E-02 8.014E-02 FAIL ABUN CF-249 3.085E-02 3.473E-02 3.741E-02 NOT IDENT. CF-251 -5.730E-03 1.044E-01 l.045E-01 NOT IDENT. Page 4428 of 5809
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 85.3859 87.09 112. 3177 136.47 82.6104 45.60 87.9392 87.57 134.9020 140.51 0.0000 46.54 74.8432 88.03 94.5115 143.76 89.5613 49.72 0.0000 88.34 94.5660 144.24 93. 3011 51. 35 84.1319 88.47 94.5884 145.44 92.2199 51. 87 90.4867 89. 96 100.8687 152.43 100.5022 52.39 87.4844 1093.63 100.9935 153.25 0.0000 52.97 109.5193 91.11 0.0000 323.87 72.1274 53.44 106.5184 .92. 59 101.3485 156.02 0.0000 54.07 76.3562 93.35 101.4862 158.56 0.0000 57.36 0.0000 94.56 66.7905 159.00 80.0664 57.53 97.0614 94.65 66.8012 162.33 82.9069 57.98 87.6618 94.67 66.8034 162.66 0.0000 59.27 80.5184 94.87 66.8267* 163.33 89.7153 59.32 80.5279 97.43 86.9583 165.86 89.1485 59.54 "74.9162 98.43 71.0617 176.31 85.9934 60.96 79.4233 98.44 71. 0631 176.60 0.0000 61.17 92.2331 99.53 98.7551 177.52 80.9970 62. 93 90.8300 100 .11 116.0939 181.07 0.0000 63.29 90:9049 102.03 83.0286 181.52 87.3616 63.58 90. 9655 103.18 83.1879 184.41 76.0448 64.28 91.1106 103.37 91. 3046 143.76 85.1909 66.73 75.4458 105.21 96.2189 193.51 80.7118 67.24 66.8986 105.31 96.2347 197.03 94.0836 125.81 87.8445 106.12 88.2357 B8.01 54.9391 67.75 87.8575 106.47 84.8011 201.83 88.4325 69.67 100.8815 109.28 106.1907 203.43 80.6862 70.83 101.1320 111. 00 91. 2700 205.31 80.4041 72.81 101.5556 111.76 0.0000 210.85 62.3028 72. 87 101.5683 114. 06 83.4788 69.2648 74.66 101.9465 116. 30 0.0000 222 .11 75.0697 74.82 101.9799 116.74 86.1857 227.09 71. 8408 74.97 102. 0118 119.76 88.9532 227.38 67.3691 77 .11 lOi. 4567 121.12 74.8731 228.16 0.0000 78.74 116. 4234 121. 22 74.8841 228.18 53.9368 79.69 100.4014 121.78 92.7910 116.74 53. 936.8 80.12 93.0978 122.06 96.4001 235.69 61.1115 80.19 0.0000 122.92 98.9057 235. 96 61. 1272 80.57 95.3984 123.07 98.9279 238.63 55.3781 81. 00 103.6207 265.00 88.2798 238.98 0.0000 81. 07 103.6349 125.81 84.5663 240.99 55.4991 81. 75 103.7717 127.23 76.7454 242.00 55.5506 83.79 99.7155 127.91 87.6243 244.70 58.8835 84.00 99.7551 129.30 104.2351 252.40 0.0000 85.43 111. 9690 131. 20 70.7498 252.80 55.1758 86.55 112.2047 133.02 95.5158 254.15 0.0000 86.79 112. 2551 133.52 81.0633 256.2.3 54.4212 86.94 112.2864 136.00 72.8439 260.90 0.0000 Page 4429 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 65.9717 355.39 0.0000 584.27 21.5598 264.80 70.6269 356.01 38.8754 595.83 0.0000 265.00 70.6392 364.49 0.0000 427.87 13.7217 268.22 57.3197 366.42 0.0000 602.52 0.0000 269.46 74.1738 372.51 42.3384 604. 72 10.3107 270.03 70.0089 375.05 47.4590 607.14 18.9244 271. 23 57.9333 377.52 50.5707 609.32 29.8499 273.65 0.0000 356.01 32.5000 610.33 29.8636 276.40 61.0010 388.16 28.5178 614.28 10.3561 277.37 61.0499 388.63 0.0000 618.01 21.8999 277.60 61.0618 391.69 38.7909 620. 36 19.6154 278.00 69.0692 264.66 24.6401 621. 93 33.4864 279.20 66.3161 401. 81 31.8502 630.19 0.0000 279.54 57.8665 402.40 31. 8615 631.29 17.3932 279.70 57.8740 404.85 30.8813 633.25 22.0507 280.46 48.0231 410.95 27.8992 634.78 0.0000 283.69 57.5921 413. 71 26.9119 635.95 18. 5911 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 54.8364 423.72 0.0000 645.85 29.7593 285.90 0.0000 427.09 35.4810 657.76 22.8754 287.50 42.6178 427.87 32.3661 657.90 0.0000 290.67 58.3932 433.94 26.7202 661.66 27.3208 293.27 0.0000 439.40 26.8069 664.57 0.0000 351. 93 38.5941 453.88 28.6243 666.33 0.0000 295.96 38.6172 463.37 28.7803 666.50 0.0000 879.38 25.7981 468 .. 07 28.8567 667. 71 0.0000 299.98 41. 6096 473.00 0.0000 677. 62 25.7325 300.09 41.6132 475.06 26.8239 685.70 0.0000 300.13 41. 6140 476.78 20.4055 695.00 0.0000 301.36 40.2184 477.60 21. 4893 696.49 23.2531 302.85 37.3885 482.18 25.8525 696. 51 23.2531 256.23 48.3800 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.1556 306.78 45.1956 497.08 18.4609 697.49 21.4731 308.46 47.1796 505.52 21.2714 702.65 19.7253 311. 90 40.5465 507.63 0.0000 706.68 24.2487 316.51 47.9551 511. 00 35.0081 711.68 18.8986 319.41 0.0000 514.00 23.0104 720. 70 0.0000 320.08 0.0000 514.00 23.0104 721. 93 0.0000 321.04 40.8276 520.40 25.2854 722.78 20.2487 323.87 49.6802 520.69 0.0000 722. 91 18.8037 325.23 39.9798 522.65 0.0000 723.31 18.806.8 328.76 0.0000 527.90 0.0000 724.19 13.0245 333.37 55.9134 528.26 26.4922 727.33 19.0178 333.97 45.6334 529.59 26.5107 733.00 15.5603 334.37 41. 2292 529.87 0.0000 735.93 19.0832 338.28 41.3463 531.02 0.0000 333.97 20.9132 338.32 41.3472 537.26 0.0000 739.50 o .*oooo 311. 90 42.8902 546.56 0.0000 747.24 20.0812 340.48 42.8902 552.55 35.7578 748.06 22.8264 340.55 0.0000 563.25 26.9600 26.5229 344.28 41.5232 569.33 20.2800 753.82 0.0000 345.93 46.0260 946.00 20.2815 756.73 15.5743 351.06 35.7620 569.70 16.9031 756.80 17.4072 351. 93 35.7832 583.19 21.5490 884.68 22.9675 Page 4430 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:58:23.64 ********************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 14-DEC-2015 13:56:00 Acquisition date : 3-0CT-2016 05:57:14. Sample ID G405235065 Sample quantity : 1.47836E+02 GRAM Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.55 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix $pike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 0 0 4 4 0 0 0 0 7 7 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4432 of 5809 Energy 46.44* 63.16* 77.20* 84.17* 87.07' 89.80 92.88* 128.38 143.37* 186.18* 208.76 238.80* 241.74 270.43 295.25* 300.81 338.56* 352.23* 463.82 481.66 493.76 511.14* 567.01 583.50* 609.37* 629.40 678.03 703.73 719.29 723.13 728.25 756.56 764.38 768.17 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 40 25 369 35 109 70 90 43 23 92 42 442 94 52 191 54 117 322 61 24 2 30 15 143 203 13 9 13 15 9 21 16 9 31 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 119 241 186 110 150 82 190 118 136 138 80 73 101 53 78 35 69 62 24 31 16 57 9 34 45 20 6 36 9 14 30 24 19 13 0.86 0.77 0.79 1. 21 1. 36 0.89 1.27 1. 40 0.62 1. 08 0.99 1.11 1. 44 1. 66 1. 08 1. 68 1.25 1.13 2.14 2.95 1. 29 1. 51 1. 64 1. 29 1. 56 0.64 1.27 0.62 0.56 0.78 2.45 0.95 0.99 1. 38 92.38 125.82 153.89 167.84 173. 63 179.09 185.25 256.24 286.21 371. 83 416.97 477.05 482.93 540.33 589.95 601.08 676.58 703.92 927 .11 962. 81 987.00 1021.77 1133. 53 1166. 52 1218.28 1258.35 1355.63 1407.06 1438.19 1445.87 1456.11 1512.75 1528.39 1535.97 89 123 152 166 171 177 177 254 283 367 414 470 470 536 584 597 670 698 921 957 984 1016 1130 1160 1211. 1253 1352 1398 1434 1441 1449 1506 1520 1531 7 1. lOE-02 51. 5 8 6. 83E-03115. 5 6 1.02E-01 8.0 5 9.62E-03 50.4 6 3.04E-02 20.0 15 1. 95E-02 19. 5 15 2.49E-02 30.8 8 1. 21E-02 45. 9 8 6.28E-03 93.7 10 2.55E-02 27.2 7 1.16E-02 38.6 19 1. 23E-01 5. 8 19 2.62E-02 22.1 9 1.46E-02 29.0 12 5.32E-02 11.9 11 1.49E-02 26.0 14 .3.24E-02 18.1 12 8. 96E-02 7. 5 14 1.70E-02 21.4 11 6.80E-03 48.0 6 5.86E-04317.8 15 8.24E-03 65.8 7 4 .18E-03 41. 6 14 3.97E-02 12.2 14 5.63E-02 10.1 12 3.54E-03 76.8 7 2.44E-03 59.5 11 3.71E-03 90.9 8 4.17E-03 44.2 9 2.60E-03 78.2 11 5.70E-03 56.5 12 4.44E-03 66.1 11 2.55E-03 98.0 9 8.52E-03 28.1 Fit 1.37E+OO 2.17E+00 Peak Search Report (continued) Page : 2 Sample ID : ,G4 052 35 0 65 *Acquisition date 3-0CT-2016 05:57:14 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 788.47 30 21 5.45 1576.59 1568 19 8.33E-03 42.7 36 0 795.50 14 11 1. 86 1590.66 1586 9 3.78E-03 52.1 37 0 860.86 16 24 1. 03 1721. 44 1711 16 4.58E-03 70.8 38 0 870.66* 11 15 1. 03 1741.04 1737 10 3.lOE-03 73.1 39 0 877.54 13 20 0.85 1754.80 1748 14 3.67E-03 78.l 40 0 911. 22* 102 12 1. 80 1822.20 1814 16 2.83E-02 12:8 41 0 929.74 16 5 1. 04 1859.25 1853 9 4.40E-03 35.2 42 0 969.29* 67 10 1. 34 1938.39 1934 11 1. 85E-02 16.7 '43 0 1008.96 8 4 2. 72 2017.77 2013 8 2.29E-03 54.2 44 0 1064.60 16 13 4.05 2129.13 2122 16 4.46E-03 54.6 45 0 1120.51* 56 13 1. 51 2241.02 2233 17 l.57E-02 19.9 46 0 1339.15 8 .6 0.64 2678.61 2669 14 2.22E-03 77.6 47 0 1460.76* 366 9 2.07 2922.03 2913 16 1. 02E-01 5.6 48 0 1571. 36 9 3 0.63 3143.45 3137 li 2.59E-03 47.4 49 0 1730.34 7 4 0.81 3461. 74 3455 9 1.84E-03 69.3 50 2 1763.43 26 8 2.44 3528.00 3519 18 7.29E-03 31.2 9.69E-01 51 2 1765.85* 12 4 1. 97 3532.83 3519 18 3. 21E-03 52.6 Flag: "*" = Peak area was modified by qackground subtraction Page 4433 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:58:25 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 14-DEC-2015 13:56:00 G405235065 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:57:14 147.84 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA25 0 01:00:00.00 1.50 keV No Linear . 75. 00 Interference Report *Interfering Nuclide Page 4434 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 . 87. 09 87.09 351. 93 Elapsed* real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 . SN-126 SN-126 CD-109 BI-211 Line 240.99. 86.94 87.57 88.03 351. 06 CAN
0 01:00:00.55 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report \_ Page : 2 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* l.131E+00 1. 486E+Ol 1.486E+Ol 11.10 OK NB-94 702.65 99.81* 2.143E+OO 3.288E-02 3.288E-02 181. 73 OK 871. 09 99.89 1. 793E+OO 3.212E-02 3.212E-02 146.30 OK NB-95 765.81 99.81* 2.000E+OO 2.402E-02 5.772E-01 196.03 OK ZR-95 724 .19 44.27 2.095E+OO 5.293E-02 1.272E+OO 156.31 OK 756.73 54.38* 2.017E+OO 7.627E-02 l.833E+OO 132.29 OK CD-109 88.03 3.70* 9.279E+OO 8.157E-01 l.268E+OO 105.12 OK SN-126 64.28 9.60 9.545E+OO l.744E-01 l.744E-01 231.10 OK 86.94 8.90 9.279E+OO 3.391E-01 3. 391E-01 105.12 OK 87.57 37. 00*. 9.279E+OO 8.157E-02 8.157E-02 105.12 OK TL-208 277.37 6.60 4.809E+OO. Line Not Found Absent 583.19 85.00* 2.509E+OO 3.592E-01 3.592E-01 24.49 OK 860.56 12.50 l.810E+OO 3.759E-01 3.759E'--01 141.57 OK PB-210 46.54 4.25* 9.121E+OO 6.790E-01 6. 963E-01 102.93 OK BI-211 72.87 1.23 9.424E+OO Line Not Found Absent 351.06 12.92* 3.891E+OO l.187E-02 l.187E-028508.91 OK PB-212 74.82 10.28 9.405E+OO Line Not Found Absent 77 .11 17.10 9.382E+OO 1. 471E+OO l.471E+OO 16.04 OK 238.63 43.60* 5.475E+OO l.078E+OO l:078E+OO 11. 56 OK 300.09 3.30 4.476E+OO 2. 071E+OO 2.071E+OO 52.03 OK BI-214 609'.32 45.49* 2.419E+OO 9.839E-01 9.843E-01 20.11 OK 1120.29 14.92 l.443E+OO l.318E+OO l.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 OK PB-214 74.82 5.80 9.405E+OO Line Not Found Absent 77 .11 9.70 9.382E+OO 2.594E+OO 2.595E+OO 16.04 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.551E+OO l.304E+OO l.305E+OO 23.76 OK 351. 93 35.60* 3.894E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 OK 1120. 29 14.92 l.443E+OO l.318E+OO l.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.803E-01 62. 46 OK RA-224 240.99 4.10* 5.418E+OO l.653E-01 l.653E-01 738.01 OK RA-226 609.32 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 OK 1120. 29 14.92 l.443E+OO l.318E+OO l.318E+OO 39.79 OK 1764. 49 15.30 9.342E-01 8.800E-01 8.803E-01 62. 46 o*K AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.030E+00 l.448E+OO l.448E+OO 36.11 OK 794.95 4.25 l.934E+OO 8.621E-01 8.621E-01 104.16 OK 835.71 1. 61 l.856E+OO Line Not Found Absent 911.20 25.80* l.725E+OO l.174E+OO l.174E+OO 25.50 OK 968. 97. 15.80 l.637E+OO l.313E+OO 1. 313E+OO 33.42 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.030E+OO l.448E+OO l.448E+OO 36.11 OK 794.95 4.25 l.934E+OO 8.621E-01 8.621E-01 104.16 OK 835.71 1. 61 l.856E+OO Line Not Found Absent 911.20 25.80* 1. 725E+OO l.174E+OO l.174E+OO 25.50 OK 968. 97 15.80 1.637E+OO l.313E+OO 1. 313E+OO 33.42 OK TH-22°8 74.82 10.28 9.405E+OO Line Not Found Absent Page 4435 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 77 .11 17.10 9.382E+OO 1.471E+OO 1.471E+OO 16.04 OK 238.63 43.60* 5.475E+OO 1.078E+OO 1.078E+OO 11. 56 OK 300.09 3.30 4.476E+OO 2. 071E+OO 2. 071E+OO 52.03 OK TH-229 85.43 14.70 9.312E+OO 1.608E-01 l.608E-01 100.75 OK 88.47 24.00 9.244E+OO l.997E-01 l.997E-01 38.94 OK 193.51 4.41* 6. 496E+OO Line Not Found Absent 210.85 2.80 6.071E+OO Line Not Found Absent TH-230 609.32 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 OK 1120.29 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 OK PA-231 283.69. 1. 70 4. 715E+OO Line Not Found Absent 301.36 5.35* 4.476E+OO 1.278E+OO 1. 278E+OO 52.03 OK TH-232 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.030E+OO 1.448E+OO 1. 448E+OO 36 .11 OK 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1. 725E+OO 1.174E+00 1.174E+OO 25.50 OK 968. 97 15.80 1.637E+OO 1.313E+OO 1.313E+OO 33.42 OK TH-234 63.29 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 OK 92.59 4.23 9. 201E+OO 1.453E+OO 1. 453E+OO 61.52 OK U-234 609.32 45.49* 2.419E+OO 9.839E-01 9.839E-01 20.11 OK 1120.29 14.92 1.443E+OO l.318E+00 1.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 OK U-235 89. 96 3.47 9.244E+OO l.381E+OO 1.381E+OO 38.94 OK 93.35 5.60 9.201E+OO 1.098E+OO 1.098E+OO 61. 52 OK 143.76 10. 96* 7.933E+OO l.581E-01 1. 581E-01 187.34 OK 163.33 5.08 *7. 333E+OO Line Not Found Absent 185. 72 57.20 6.688E+OO l.426E-01 1.426E-01 54.41 OK 205.31 5.01 6.202E+OO Line Not Found Absent U-238 63.29 3.70* 9.545E+00 4.526E-01 4.526E-0.1 231.10 OK 92.59 4.23 9.201E+OO l.453E+00 1.453E+OO 61. 52 OK ANH-5,11 511. 00 100.00* 2 :809E+*oo 5.731E-02 5. 731E-02 131.62 OK Flag: "*" = Keyline Page 4436 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:58:27.09 *******************************************************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l *
Acquisition date 3-0CT-2016 05:57:14 Sensitivity : 3.000 *
Detector ID GAM25 _ Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
Sample date 14-DEC-2015 13:56:00 Analyst initials: MXRl *
Sample ID G405235065 Sample Quantity :. l.4784E+02 GRAM *
Batch Number 1596254 Wet Weight 0.00000 *
Wet wt corr 1,00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * * *
CALIBRATION INFORMATION * *
Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKAlOO': [CANBERRA.GAMMA]EFF.GAM25 CAN.CNF;l5
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM K-40 1.486E+Ol l.616E+OO 7.067E-01 NB-94 .3.288E-02 5.856E-02 5.875E-02 NB-95 5.772E-01 l.109E+OO . 9. 378E-01 ZR-95 l.833E+OO 2.376E+00 2.466E+OO CD-109 l.268E+OO l.306E+OO 1.203E+OO SN-126 8.157E-02 8.404E-02 6.914E-02 TL-208 3.592E-01 8.621E-02 5.023E-02 PB-210 6. 963E-01 7.023E-01 5.653E-01 BI-211 l.187E-02 9.898E-01 2.940E-01 PB-212 l.078E+OO l.221E-01 7.821E-02 BI-214 9.843E-01 l.940E-01 l.289E-01 PB-214 l.309E+OO l.920E-01 3.340E-01 RN-222 9.843E-01 l.940E-01 l.289E-01 RA-224 l.653E-01 l .196E+OO 8.397E-01 RA-226 9.843E-01 l.940E-01 1.289E-01 AC-228 1.174E+OO 2.934E-01 2.334E-01 RA-228 l.174E+OO 2.934E-01 2.334E-01 TH-228 l.078E+OO l.221E-01 7.821E-02 TH-229 -l.970E-01 3.778E-01 6.735E-01 TH-230 9.839E-01 l.939E-01 1.289E-01 PA-231 l.278E+OO 6.515E-01 6.390E-01 TH-232 l.174E+OO 2.934E-01 2.334E-01 TH-234 4.526E-01 l.025E+OO 7.537E-01 U-234 9.839E-01 l.939E-01 1.289E-01 U-235 l.581E-01 2.903E-01 2.564E-01 U-238 4.526E-01 l.025E+OO 7.537E-01 ANH-5.11 5.731E-02 7.393E-02 5.250E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -6.901E+00 l.161E+Ol l.818E+Ol .NOT IDENT. NA-22 -4.344E-03 4.848E-02 9.269E-02 NOT IDENT. NA-24 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF Page 4437 of 5809 AL-26 -l.085E-02 2.661E-02 5.204E-02 NOT IDENT. SC-46 -5.542E-02 3.828E-01 7.426E-01 FAIL ABUN V-48 O.OOOE+OO l.104E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.892E+02 O.OOOE+OO SHORT HLIF MN-54 -3.158E-03 5. 967E-02 1.184E-01 NOT IDENT. C0-56 l.014E-02 4.465E-01 8.920E-01 NOT IDENT. MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 4.635E-03 3.497E-02 6.847E-02 NOT IDENT. C0-58 3.920E-02 4.089E-01 8.651E-01 NOT IDENT. FE-59 -l.522E+OO 6.602E+OO 1. 2 60E+Ol NOT IDENT. C0-60 2.932E-02 4.520E-02 9.091E-02 NOT IDENT. ZN-65 2.576E-02 l.345E-01 2.573E-01 NOT IDENT. GE-68 l.431E-01 2.646E+OO 5.160E+OO NOT IDENT. AS-73 -3.791E-02 1.465E+OO 2.988E+OO NOT IDENT. AS-74 O.OOOE+OO 4.502E+03 O.OOOE+OO SHORT HLIF SE-75 l.137E-01 1. 752E-01 3.437E-01 NOT IDENT. BR-77 O.OOOE+OO 3.641E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.229E+02 O.OOOE+OO SHORT HLIF RB-83 2.900E-01 5.290E-01 1.112E+OO NOT IDENT. KR-85 -2.600E+OO 6.358E+OO '1.163E+Ol NOT IDENT. SR-85 -2.606E-01 6.293E-01 l.150E+OO NOT IDENT. RB-86 O.OOOE+OO 2.452E+04 O.OOOE+OO SHORT HLIF Y-88 -8.054E-02 l.823E-01 3.509E-01 NOT IDENT. Y-91 -2.273E+02 5.631E+02 1.008E+03 NOT IDENT. NB-95M 2.939E-01 1.931E+OO 3.343E+00 NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO . 3. 757E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 4.981E-02 4.539E-02 FAIL ABUN RH-102 -l.785E-02 5.444E-02 8. 725E-02 FAIL ABUN RU-103 -9. 8 91E-01 6.045E+OO 1.00lE+Ol FAIL ABUN RH-:106 3.707E-01 4.672E-01 9.915E-01 NOT IDENT. RU-106 3.707E-01 4.672E-01 9.915E-01 NOT IDENT. AG-108M 5. 613E--03 2.548E-02 5.105E-02 FAIL ABUN AG-llOM 1.575E-02 l.022E-01 2.017E-01 FAIL ABUN SN-113 -8.336E-02 2.169E-01 4.077E-01 NOT IDENT. CD-115 O.OOOE+OO 3.930E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 5.153E+04 O.OOOE+OO SHORT HLIF TE-123M 5. 296E-02 9.254E-02 1.856E-01 NOT IDENT. SB-124 5.497E-02 1. 745E+OO 3.873E+OO FAIL ABUN SB-125 -1.972E-02 8.097E-02 1.560E-01 FAIL ABUN TE-125M 5.498E+Ol 1.728E+02 3.461E+02 NOT IDENT. I-126 O.OOOE+OO 6.895E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.695E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.675E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.636E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.377E+25 O.OOOE+OO SHORT HLIF BA-133 1.043E-02 3.553E-02 6.661E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.612E-02 5.729E-02 1.050E-01 FAIL ABUN CS-135 2.022E-02 1.320E-01 2.266E-01 NOT IDENT. I-135 O.OOOE+OO l.398E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.470E+05 O.OOOE+OO SHORT HLIF BA-137M 3.077E-02 3.495E-02 7.330E-02 NOT IDENT. CS-137 3.251E-02 3.693E-02 7.743E-02 NOT IDENT. CE-139 -8.346E-02 8. 969E-02 1.565E-01 NOT IDENT. BA-140 O.OOOE+OO 7.917E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.978E+05 O.OOOE+OO SHORT HLIF CE-141 -4.775E+00 1.867E+Ol 3.237E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.565E+40 O.OOOE+OO SHORT HLIF CE-144 -2 .116E-01 2.579E-01 4.657E-01 NOT IDENT. PM-144 -1.456E-02 6.253E-02 9. 960E-02 NOT IDENT. PR-144 -1.218E+00 5.419E+OO 8.647E+OO NOT IDENT. PM-146 1.254E-02 3.599E-02 7.402E-02 NOT I DENT*. ND-147 O.OOOE+OO 2.163E+07 O.OOOE+OO SHORT HLIF PM-147 -1.949E+Ol 6.185E+02 1.197E+03 NOT IDENT. PM-149 O.OOOE+OO 5.747E+39 O.OOOE+OO SHORT HLIF EU-150 1.532E-02 2.339E-02 4.532E-02 FAIL ABUN EU-152 6. 961E-02 7.899E-02 l.597E-01 NOT IDENT. GD-153 -7.477E-02 l.056E-01 1.809E-01 NOT IDENT. EU-154 2.279E-02 l.154E-01 2.332E-01 FAIL ABUN EU-155 4.990E-02 7.185E-02 1.476E-01 FAIL ABUN TB-160 -4.775E-01 1. 793E+OO 3.005E+OO FAIL ABUN H0-166M -1.525E-02 6.095E-02 l.097E-01 NOT IDENT. TM-171 l.164E+00 3.402E+00 7.105E+OO NOT IDENT. HF-172 8.276E-02 l.772E-01 3.322E-01 FAIL ABUN Page 4438 of 5809 LU-172 -2.428E-02 8.992E-02 1.664E-01 FAIL ABUN LU-176 5.709E-04 2.073E-02 3.787E-02 FAIL ABUN HF-181 6.843E+OO 6.438E+OO 8.037E+OO FAIL ABUN TA-182 -l.754E-02 l.012E+OO 1.920E+OO FAIL ABUN RE-183 -5.597E-01 7.075E-01 1.382E+OO NOT IDENT. RE-184 1.302E+Ol 3.003E+Ol 6.065E+Ol NOT IDENT. W-188 -2.242E+Ol 9.657E+Ol 1.562E+02 FAIL ABUN IR-'-192 -l.148E-01 3.812E-01 7. 391E-01 FAIL ABUN HG-203 4.076E-01 2.104E+oo* 3.893E+OO NOT IDENT. BI-207 7.335E-02 7. 851E-02 9. 962E-02 FAIL ABUN PB-211 5.527E-01 9.563E-01 NOT IDENT. BI-212 7.749E-01 8.578E-01 1.269E+OO FAIL ABUN RN-219 9.840E-02 3.435E-01 6.934E-01 FAIL ABUN RA-223 -l.676E-01 4.941E-01 9.544E-01 FAIL ABUN AC-227 -l.276E-01 l.984E-01 3.376E-01 FAIL ABUN TH-227 -1.276E-01 l.984E-01 3.376E-01 FAIL ABUN TH-231 -l.676E-01 4.941E-01 9.544E-01 FAIL ABUN PA-233 -2.903E-02 5 .116E-02 9.687E-02 FAIL ABUN PA-234 -8.797E-02 2.785E-01 5.257E-01 NOT IDENT. PA-234M 2.684E+OO 4.477E+OO 9. 596E+OO NOT IDENT. NP-237 -2.903E-02 5 .116E-02 9.687E-02 FAIL ABUN NP-238 0.000E+OO 6.207E+40 O.OOOE+OO SHORT HLIF NP-239 -1.210E-01 l.705E-01 3.152E-01 NOT IDENT. PU-239 O.OOOE+OO 4.534E+02 4. 901E+02 FAIL ABUN AM-241 5.032E-03 3.900E-02 7. 996E-02 NOT IDENT. AM-243 O.OOOE+OO 3. SllE-02 7. 7 41E-02 NOT IDENT. CM-243 * -2.975E-02 6.169E-02 1.175E-01 NOT IDENT. BK-247 7 .139E-02 6.064E-02 1.258E-OI FAIL ABUN CM-247 5.325E-03 3.107E-02 6.211E-02 NOT IDENT. CF-249 9.598E-03 3.310E-02 6.711E-02 NOT IDENT. CF-251 -2.393E-02 9.529E-02 l.755E-01 NOT IDENT. Page 4439 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:58:24.43 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Erro*r K-40 1460.82 353 10.66* 1.131E+OO 1.486E+Ol l.486E+Ol 11.10 NB-94 702.65 14 99.81* 2.143E+OO 3.288E-02 3.288E-02 181.73 871.09 11 99.89 1. 793E+OO 3.212E-02 3.212E-02 146.30 NB-95 765.81 9 99.81* 2.000E+OO 2.402E-02 5.772E-01 196. 03 ZR-95 724 .19 10 44.27 2.095E+OO 5.293E-02 1.272E+OO 156.31 756.73 16 54.38* 2.017E+OO 7.627E-02 1.833E+OO 132.29 CD-109 88.03 136 3.70* 9.279E+OO 2.018E+OO 3.136E+00 40.08 SN-126 64.28 31 9.60 9.545E+OO l.744E-01 1. 744E-01 231.10 86.94 136 8.90 9.279E+OO 8.388E-01 8.388E-01 40:08 87.57 136 37.00* 9.279E+OO 2.018E-01 2.018E-01 40.08 TL-208 277.37 ------6.60 4.809E+OO ------Line Not Found ------583.19 151 85.00* 2.509E+00 3.592E-01 3.592E-01 24.49 860.56 17 12.50 1.810E+OO 3.759E-01 3.759E-01 141.57 PB-210 46.54 52 4.25* 9 .121E+OO 6.790E-01 6. 963E-01 102.93 BI-211 72.87 ------1.23 9.424E+OO ------Line Not Found ------351.06 357 12.92* 3.891E+OO 3.605E+OO 3.605E+OO 14.97 PB-212 74.82 ------10.28 9.405E+OO ------Line Not Found ------77 .11 465 17.10 9.382E+OO 1.471E+00 1. 471E+OO 16.04 238.63 507 43.60* 5.475E+00 1. 078E+OO 1. 078E+OO 11. 56 300.09 60 3.30 4.476E+OO 2. 071E+OO 2.071E+00 52.03 BI-214 609.32 213 45.49* 2.419E+00 9.839E-01 9.843E-01 20 .11 1120. 29 56 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 PB-214 74.82 ------5.80 9.405E+OO ------Line Not Found ------77 .11 465 9.70 9.382E+OO 2.594E+OO 2.595E+OO 16.04 87.09 136 3.41 9.279E+00 2.189E+OO 2.190E+00 40.08 242.00 108 7.25 5.418E+OO 1.398E+OO 1.398E+OO 44 .11 295.22 215 18.42 4. 551E+OO 1.304E+OO 1.305E+OO 23.76 351. 93 357 35.60* 3.891E+OO 1.308E+OO 1.309E+OO 14.97 RN-222 609.32 213 45.49* 2.419E+00 9.839E-01 9.843E-01 20 .11 1120.29 56 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39 _*79 1764.49 25 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 RA-224 240.99 108 4.10* 5.418E+OO 2.471E+OO 2.471E+00 44 .11 RA-226 609.32 213 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 1120.29 56 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39. 79 1764.49 25 15.30 9.342E-01 8.800E-01 8.803E-01 62. 46 AC-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 130 11. 27 4.030E+OO 1.448E+OO l.448E+OO 36.11 794.95 14 4.25 1.934E+OO 8.621E-01 8.621E-01 104.16 835. 71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 103 25.80* 1.725E+OO 1.174E+OO 1.174E+OO 25.50 968. 97 67 15.80 1.637E+OO 1.313E+OO l.313E+OO 33.42 RA-228 105.21 ------1.10 8.977E+00 ------Line Not Found ------338.32 130 11. 27 4.030E+OO 1.448E+OO l.448E+OO 36.11 794.95 14 4.25 1.934E+OO 8. 621E-01 8.621E-01 104.16 835.71 ------1. 61 1.856E+OO -*-----Line Not Found ------911.20 103 25.80* 1. 725E+OO 1.174E+OO 1.174E+OO 25.50 Page 4440 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968.97 67 15.80 l.637E+OO 1.313E+OO 1.313E+OO 33.42 TH-228 74.82 ------10.28 9.405E+OO ------Line Not Found ------77 .11 465 17.10 9.382E+OO 1.471E+OO l.471E+OO 16.04 238.63 507 43.60* 5.475E+OO 1. 078E+OO 1.078E+OO 11.56 300.09 60 3.30 4.476E+OO 2. 071E+OO 2.071E+OO 52.03 TH-229 85.43 43 14;70 9.312E+OO 1.608E-01 l.608E-01 100.75 88.47 87 24.00 9.244E+OO l.997E-01 l.997E-01 38.94 193.51 ------4.41* 6.496E+OO ------Line Not Fo.und ------210.85 ------2.80 6. 071E+OO ------Line Not Found ------TH-230 609.32 213 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 1120.29 56 14'. 92 l.443E+OO 1.318E+OO l.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 PA-231 283.69 ------1. 70 4.715E+OO ------Line Not Found ------301.36 60 5.35* 4.476E+OO 1.278E+OO 1.278E+OO 52.03 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 130 11. 27 4.030E+OO 1.448E+OO l.448E+OO 36 .11 835.71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 103 25.80* 1.725E+OO 1.174E+OO l.174E+00 25.50 968. 97 67 15.80 1.313E+OO 1.313E+OO 33.42 TH-234 63.29 31 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 92.59 111 4.23 9.201E+OO l.453E+OO l.453E+00 61.52
U-234 609.32 213 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 1120.29 56 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 U-235 89. 96 87 3.47 9.244E+OO 1.381E+OO 1.381E+OO 38.94 93.35 111 5.60 9.201E+OO 1.098E+OO 1.098E+OO 61.52 143.76 27 10.96* 7.933E+OO l.581E-01 l.581E-01 187.34 163.33 ------5.08 7.333E+OO ------Line Not Found ------185. 72 107 57.20 6.688E+OO 1.426E-01 1.426E-01 54.41 205.31 ------5.01 6.202E+OO ------Line Not Found ------U-238 63.29 31 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 92.59 111 4.23 9.201E+OO l.453E+OO l.453E+OO 61.52 ANH-511 511. 00 32 100.00* 2.809E+OO 5. 731E-02 5.731E-02 131. 62 Flag: "* ,, Keyl"ine Page 4441 of 5809 Page : 3 Summary of Nuclide Activity S.ample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Total number of lines in spectrum 51 Number of unidentified lines 9 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 NB-94 NB-95 ZR-95 CD-109 SN-126 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 . TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Hlife 1.25E+09Y 20300.00Y 64.03D 64.03D 461.40D 2.30E+05Y 1. 41E+10Y 22.20Y 7.04E+08Y 1.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1.41E+10Y 1600. OOY 1. 41E+10Y 1.41E+10Y l.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 1.00E+09Y Decay 1. 00 1. 00 24.0 24.0 1. 55 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.*00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.486E+Ol 3.288E-02 2.402E-02 *7.627E-02 2.018E+OO 2.018E-01 3.592E-01 6.790E-01 3.605E+OO 1.078E+OO 9.839E-01 1.308E+OO 9.839E-01 2.471E+OO 1.174E+OO 1.174E+OO 1.078E+OO 1.997E-01 9 .. 839E-01 1. 278E+OO 1.174E+00 4.526E-01 9.839E-01 1. 581E-01 4.526E-01 5. 731E-02 3.883E+Ol 3.883E+01 Decay Corr pCi/GRAM 1.486E+Ol 3.288E-02 5.772E-01 1.833E+OO 3.136E+OO 2.018E-01 3.592E-01 6. 963E-01 3.605E+OO 1.078E+OO 9.843E-01 1.309E+OO 9.843E-01 2.471E+OO 9.843E-01 1.174E+OO 1.174E+OO 1.078E+OO 1.997E-01 9.839E-01 1.278E+OO 1.174E+00 4.526E-01 9.839E-01 1.581E-01* 4.526E-01 5. 731E-02 4.227E+Ol 4.227E+Ol 82.35% Decay Corr 2-Sigma Error 0.165E+Ol 5.976E-02 11.31E-01 2. 424E+OO 1.257E+OO 0.809E-01 0.880E-01 7.167E-01 0.540E+OO 0.125E+OO 1. 979E-01 0 .196E+OO 1. 979E-01 1.090E+OO 1. 979E-01 0.299E+OO 0.299E+OO 0.125E+OO 0.778E-01 1. 97 9E-01 0.665E+OO 0.299E+OO 10.46E-01 1. 97 9E-01 2. 962E-01 10.46E-01 7.543E-02 "M" Manually accepted 2-Sigma %Error 11.10 181. 73 196. 03 132.29 40.08 40.08 24.49 102.93 14.97 11. 56 20 .11 14.97 20 .11 44 .11 20 .11 25.50 25.50 11. 56 38.94 20 .11 52.03 25. 50 ' 231.10 20 .11 187.34 231.10 131. 62 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4442 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235065 Acquisition date : 3-0CT-2016 05:57:14 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 128.38 53 142 1. 40 256.24 254 8 l.21E-02 91. 8 8.38E+OO T 0 208.76 48 93 0.99 416.97 414 7 l.16E-02 77.2 6.12E+OO 0 270.43 59 60 1. 66 540.33 536 9 1.46E-02 58.0 4.92E+OO T 0 463.82 66 26 2.14 927.11 921 14 1. 70E-02 42.8 3.05E+00 T 0 481.66 26 33 2.95 962.81 957 11 6.80E-03 96.0 2. 96E+OO T 0 493.76 2 17 1. 29 987.00 984 6 5.86E-04 **** 2.89E+OO T 0 567.01 16 9 1. 64 1133. 53 1130 7 4.18E-03 83.3 2.57E+OO 0 62 9. 40 13 21 0.64 1258.35 1253 12 3.54E-03 **** 2.35E+OO T 0 678.03 9 6 1. 27 1355. 63 1352 7 2.44E-03 **** 2.21E+OO T 0 719.29 16 9 0.56 1438.19 1434 8 4.17E-03 88.4 2.lOE+OO T 0 728.25 21 32 2.45 1456.11 1449 11 5.70E-03 **** 2.08E+OO T 0 768.17 32 14 1. 38 1535.97 1531 9 8.52E-03 56.2 1.99E+OO T 0 788.47 31 22 5. 45* 1576.59 1568 19 8.33E-03 85.3 1. 95E+OO 0 877.54 13 20 0.85 1754.80 1748 14 3.67E-03 **** 1.78E+OO 0 929.74 16 5 1. 04 1859.25 1853 9 4.40E-03 70.4 1.70E+OO T 0 1008.96 8 4 2. 72 2017. 77 2013 8 2.29E-03 **** 1.58E+OO 0 1064.60 16 13 4.05 2129.13 2122 16 4.46E-03 **** 1. 51E+OO T 0 1339 .15 8 6 0.64 2678.61 2669 14 2.22E-03 **** 1.23E+OO 0 1571.36 9 3 0.63 3143.45 3137 11 2.59E-03 94.8 1.05E+OO 0 1730.34 6 4 0.81 3461.74 3455 9 1.84E-03 **** 9.53E-01 2 1765.85 11 4 1. 97 3532. '83 3519 18 3. 21E-03 **** 9.33E-01 Flags: "T" = Tentatively associated Page 4443 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:58:39.29 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l *
Acquisition date 3-0CT-2016 05:57:14 Sensitivity 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed time: 0 01:00:00.55 Half life ratio : ***** *
Sample date 14-DEC-2015 13:56:00 Nuclide Library : SOLID *
Sample ID G405235065 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : 1.4784E+02 GRAM *
Wet wt corr 1. 00000 Wet Weight
0. 00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-94 NB-95 ZR.:..95 CD-109 SN-126 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Le (pCi/GRAM 2. 961E-01 2.610E-02 3. 843E-'01 1.080E+OO 5. 681E-01 3.243E-02 2.181E-02 2.630E-01 1.329E-01 3.610E-02 5.807E-02 1.619E-01 5.807E-02 3.877E-01 5.807E-02 1.0lOE-01 1.0lOE-01 3.610E-02 3 .116E-01 5.805E-02 2.896E-01 1.0lOE-01 3.560E-01 5.805E-02 1.199E-01 3.560E-01 2.374E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4444 of 5809 Le (pCi/GRAM 8.046E+OO 3.967E-02 O.OOOE+OO 1.844E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-95M NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115. SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 'EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 4445 of 5809 3.263E-Ol 0.000E+OO 0.000E+OO 5.199E-02 3.929E-01 O.OOOE+OO 3.213E-02 3.672E-Ol 5.488E+OO 3.923E-02 1.068E-01 2.274E+OO 1.400E+OO O.OOOE+OO 1. 586E-01 O.OOOE+OO 0.000E+OO 4.956E-01 5.199E+OO 5.141E-01 0.000E+OO l.232E-01 4. 401E+02 1.546E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2 .119E-02 3.741E-02 4.525E+OO 4.443E-01 4.443E-01 2.310E-02 8.859E-02 1.857E-01 O.OOOE+OO O.OOOE+OO 8.641E-02 1.500E+OO 6.910E-02 1.625E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.017E-02 O.OOOE+OO 4.696E-02 1.043E-01 O.OOOE+OO O.OOOE+OO 3.312E-02 3.499E-02 7.277E-02 0.000E+OO 0.000E+OO 1.519E+Ol O.OOOE+OO 2.166E-01 4.408E-02 3.828E+00 3.314E-02 0.000E+OO 5.617E+02 O.OOOE+OO 2. 081E-02 7.284E-02 8.402E-02 1.002E-01 6.949E-02 1. 285E+OO 4.873E-02 3.333E+OO 1.558E-01 7.313E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247' CF-249 CF-251 Page 4446 of 5809 1. 720E-02 3.656E+OO 8.462E-01 6.498E-01 2.702E+Ol 7.096E+Ol 3.378E-01 1.802E+OO 4.354E-02 4.235E-01 5. 841E-01 3.156E-01 4.346E-01 l.542E-01 l.542E-01 4.346E-01 4.415E-02 2.281E-01 4.278E+OO 4.415E-02 O.OOOE+OO l.470E-01 2.313E+02 3.784E-02 3.755E-02 5.482E-02 5.813E-02 2.820E-02 3.053E-02 8 .172E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN . FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:58:44.63 ****************************************.***************************************

GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l *
Acquisition date 3-0CT-2016 05:57:14 Sensitivity : 3.000 *
Detector ID GAM25 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
Sample date 14-DEC-2015 13:56:00 Nuclide Library : SOLID *
Sample ID G405235065 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : l.4784E+02 GRAM *
Quantity Err(%) : 1.3529E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * *
CALIBRATION INFORMATION * * *
Eff. Cal. date 1-AUG-201'6 08: 41: 33 Eff. Geometry : CAN *
Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.486E+Ol 1. 793E+OO NB-94 3.288E-02 5.858E-02 NB-95 5.772E-01 1.109E+OO ZR-95 1.833E+OO 2.377E+OO CD-109 1. 268E+OO 1.331E+OO SN-126 8.157E-02 8.550E-02 TL-208 3.592E-01 8.755E-02 PB-210 6. 963E-01 7.049E-01 .BI-211 1.187E-02 1.014E+OO PB-212 1.078E+OO 1. 34 7E-01 BI-214 9.843E-01 1.985E-01 PB-214 l.309E+OO l.995E-01 RN-222 9.843E-01 l.985E-01 RA-224 1.653E-01 1.205E+OO RA-226 9.843E-01 l.985E-01 AC-228 1.174E+OO 2.995E-01 RA-228 1. l 74E+OO 2.995E-01 TH-228 1.078E+OO l.347E-01 TH-229 -l.970E-01 3.779E-01 TH-230 9.839E-01 1.985E-01 PA-231 l.278E+OO 7.062E-01 TH-232 1.174E+OO 2.995E-01 TH-234 4.526E-01 1.030E+OO U-234 9.839E-01 l.985E-01 U-235 1.581E-01 2.904E-01 U-238 4.526E-01 1.030E+OO ANH-511 5.731E-02 7. 396E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4447of5809 Key-Line Activity (pCi/GRAM . -6.901E+OO -4.344E-03 l.OOOE+41 K.L Act error ( 1. 96-sigma) 1.161E+Ol 4.848E-02 4.017E+41 TPU ( 1. 96-sigma) 1. 793E+OO 5.858E-02 1.109E+OO 2.377E+OO 1. 331E+OO 8.550E-02 8.755E-'-02 7.049E-01 1.014E+OO '1. 347E-01 l.985E-01 1.995E-01 1.985E-01 1.205E+OO 1.985E-01 2.995E-01 2.995E-01 1. 347E-01 3:779E-01 1.985E-01 7.062E-01 2.995E-01 1.030E+OO 1.985E-01 2.904E-01 1.030E+OO 7.396E-02 TPU ( 1. 96-sigma) 1.202E+Ol 4.852E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -l.085E-02 2.662E-02 2.706E-02 NOT IDENT. SC-46 -5.542E-02 3.828E-01 3.836E-01 FAIL ABUN V-48 -3.132E+03 1.104E+04 l .113E+04 SHORT HLIF CR-51 -4.443E+Ol 2.892E+02 2.899E+02 SHORT HLIF MN-54 -3.158E-03 5. 967E-02 5. 969E-02 NOT IDENT. C0-56 1.014E-02 4.465E-01 4.465E-01 NOT IDENT. MN-56 l.OOOE+41 3.824E+42 O.OOOE+OO SHORT HLIF C0-57 4.635E-03 3.497E-02 3.504E-02 NOT IDENT. C0-58 3.920E-02 4.089E-01 4.093E-01 NOT IDENT. FE-59 -1.522E+OO 6.603E+OO 6.638E+OO NOT IDENT. C0-60 2.932E-02 4.521E-02 4. 711E-02 NOT IDENT. ZN-65 2.576E-02 1.345E-01 1.350E-01 NOT IDENT. GE-68 1. 431E-01 2.646E+OO 2.647E+OO NOT IDENT. AS-73 -3.791E-02 1.465E+OO 1.465E+OO NOT IDENT. AS-74 -4.534E+02 4.502E+03 4.507E+03 SHORT HLIF SE-75 1.137E-Ol 1. 753E-01 1.826E-01 NOT IDENT. BR-77 3.215E+37 2.726E+38 O.OOOE+OO SHORT HLIF SR-82 1.189E+o2 6.229E+02 6.253E+02 SHORT HLIF RB-83 2.900E-01 5.305E-01 5.463E-01 NOT IDENT. KR-85 -2.600E+OO 6.359E+OO 6.466E+OO NOT IDENT. SR-85 -2.606E-01 6.294E-01 6.402E-01 NOT IDENT. RB-86 2.732E+03 2.452E+04 2.455E+04 SHOE.T HLIF Y-88 -8.054E-02 1.824E-01 1. 860E-01 NOT IDENT. Y-91 -2.273E+02 5.632E+02 5.724E+02 NOT IDENT. NB-95M 2.939E-01 1.931E+OO 1.935E+OO NOT IDENT. NB-97 -l.000E+41 1. 996E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 3.460E+41 O.OOOE+OO SHORT HLIF M0-99 -8.368E+30 3.758E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.833E+41 O.OOOE+OO SHORT HLIF RH-101 5.539E-02 5.081E-02 5.662E-02 FAIL ABUN RH-102 -1.785E-02 5.445E-02 5.505E-02 FAIL ABUN RU-103 -9. 891E-01 6.046E+OO 6.062E+OO FAIL ABUN RH-106 3.707E-01 . 4.678E-01 4. 968E-01 NOT IDENT. RU-106 3.707E-01 4.678E-01 4. 968E-01 NOT IDENT. AG-108M 5.613E-03 2.548E-02 2.561E-02 FAIL ABUN AG-llOM 1.575E-02 1.022E-01 1.025E-01 FAIL ABUN SN-113 -8.336E-02 2.169E-01 2.201E-01 NOT IDENT. CD-115 -1.938E+38 3.945E+38 O.OOOE+OO SHORT HLIF SN-117M 2.954E+04 5.165E+04 5.334E+04 SHORT HLIF TE-123M 5,296E-02 9.257E-02 9.560E-02 NOT IDENT. SB-124 5.497E-02 1. 745E+OO 1. 746E+OO FAIL ABUN SB-125 -1. 972E-02 8.098E-02 8.146E-02 FAIL ABUN TE-125M 5.498E+Ol 1. 728E+02 1. 746E+02 NOT IDENT. I-126 -l.155E+04 6.895E+05 6.896E+05 SHORT HLIF. SB-126 8.890E+05 9.974E+05 SHORT HLIF SB-127 -2.120E+21 8.188E+21 O.OOOE+OO SHORT HLIF I-131 -2.499E+08 2.636E+09 2.639E+09 SHORT HLIF I-132 1.000E+41 1.866E+42 O.OOOE+OO SHORT HLIF TE-132 4.300E+25 9.532E+25 O.OOOE+OO SHORT HLIF BA-133 l.043E-02 3.553E-02 3.584E-02 NOT IDENT. I-133 l.000E+41 3.942E+41 O.OOOE+OO SHORT HLIF CS-134 5.612E-02 5.734E-02 6.267E-02 FAIL ABUN CS-135 2.022E-02 l.320E-01 1.323E-01 NOT IDENT. I-135 -l.OOOE+41 6. 781E+41 O.OOOE+OO SHORT HLIF CS-136 -2. 961E+04 2.470E+05 2.474E+05 SHORT HLIF BA-137M 3*: 077E-02 3.498E-02 3.763E-02 NOT IDENT. CS-137 3.251E-02 3.695E-02 3.975E-02 NOT IDENT. CE-139 -8.346E-02 9.125E-02 9.870E-02 NOT IDENT. BA-140 4.143E+05 7.919E+05 8.136E+05 SHORT HLIF LA-140 2.034E+05 2.979E+05 3.117E+05 SHORT HLIF CE-141 -4.775E+OO 1.867E+Ol 1.879E+Ol NOT IDENT. CE-143 1.000E+41 5.654E+40 O.OOOE+OO SHORT HLIF CE-144 -2 .116E-01 2. 581E-01 2.752E-01 NOT IDENT. PM-144 -l.456E-02 6.253E-02 6.288E-02 NOT IDENT. PR-144 -1.218E+OO 5.420E+OO 5.447E+OO NOT IDENT. PM-146 1.254E-02 3.600E-02 3.644E-02 NOT IDENT. ND-147 -8.930E+06 2.164E+07 2.201E+07 SHORT HLIF PM-147 -1.949E+Ol 6 .185E+o2 6 .185E+02 NOT IDENT. PM-149 -l.566E+39 5.757E+39 O.OOOE+OO SHORT HLIF EU-150 1.532E-02 2.340E-02 2.440E-02 FAIL ABUN EU-152 6.961E-02 7.909E-02 8.508E-02 NOT IDENT. GD-153 -7.477E-02 l.057E-01 l.109E-01 .NOT IDENT. EU-154 2.279E-02 l.154E-01 l.158E-01 FAIL ABUN EU-155 4.990E-02 7.194E-02 7.537E-02 FAIL ABUN TB-160 -4.775E-01 1. 793E+OO 1.806E+OO FAIL ABUN H0-166M -1.525E-02 6.095E-02 6.134E-02 NOT IDENT. TM-171 1.164E+OO 3.403E+OO 3.443E+OO NOT IDENT. HF-172 8.276E-02 l.777E-01 1.816E-01 FAIL ABUN Page 4448 of 5809 LU-172 -2.428E-02 8. 996E-02 9.062E-02 FAIL ABUN LU-176 5.709E-04 2.073E-02 2.073E-02 FAIL ABUN HF-181 6.843E+OO 6.445E+OO 7.145E+OO FAIL ABUN TA-182 -1. 7 54E-02 1.012E+OO l.012E+OO FAIL ABUN RE-183 -5.597E-01 7.127E-01 7. 561E-01 NOT IDENT. RE-184 1.302E+Ol 3.019E+Ol 3.076E+Ol NOT IDENT. W-188 -2.242E+Ol 9.660E+Ol 9. 713E+Ol FAIL ABUN IR-192 -l.148E-01 3.812E-01 3.847E-01 FAIL ABUN HG-203 4.076E-01 2.104E+OO 2 .112E+OO NOT IDENT. BI-207 7.335E-02 7.856E-02 8.523E-02 FAIL ABUN PB-211 -5. 729E-01 5.534E-01 6.107E-01 NOT IDENT. BI-212 7.749E-01 8.587E-01 9.270E-01 FAIL ABUN RN-219 9.840E-02 3.437E-01 3.466E-01 FAIL ABUN RA-223 -1. 67 6E-01 4.942E-01 5.000E-01 FAIL ABUN AC-227 -1.276E-01 1.991E-01 2. 072E-01 FAIL ABUN TH-227 -l.276E-01 l.991E-01 2. 072E-01 FAIL ABUN TH-231 -1. 67 6E-01 4.942E-01 5.000E-01 FAIL ABUN PA-233 -2.903E-02 5 .117E-02 5.282E-02 FAIL ABUN PA-234 -8.797E-02 2. 961E-01 2.988E-01 NOT IDENT. PA-234M 2.684E+OO 4.478E+OO 4.639E+OO NOT IDENT. NP-237 -2.903E-02 5. ll 7E-02 5.282E-02 FAIL ABUN NP-238 4 .101E+40 6.210E+40 0.000E+OO SHORT HLIF NP-239 -l.210E-01 l.708E-01 1.793E-01
NOT IDENT. PU-239 5.042E+02 4.539E+02 5.077E+02 FAIL ABUN AM-241 5.032E-:-03 3.900E-02 3.907E-02 NOT IDENT. AM-243 1.656E-01 3.655E-02 8.313E-02 NOT IDENT. CM-243 -2.975E-02 6.175E-02 6.319E-02 NOT IDENT. BK-247 7.139E-02 6.232E-02 7.014E-02 FAIL ABUN CM-247 5.325E-03 3.109E-02 3 .118E-02 NOT IDENT. CF-249' 9.598E-03 3. 311E-02 3.339E-02 NOT IDENT. CF-251 -2.393E-02 9,533E-02 9.594E-02 NOT IDENT. Page 4449of5809
GEL Laboratories LLC *
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Charleston, SC 29407 *
GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 43.2225 87.09 76.7587 136.47 81.2058 45.60 59.6870 87.57 76.8707 140.51 0.0000 46.54 59. 9619 88.03 97.5052 143.76 68. 7161 49.72 0.0000 88.34 97.5965 144.24 68.7845 51. 35 74.7906 88.47 97.6348 145.44 73.5501 51. 87 70.4681 89. 96 84.8797 152.43 75.9177 52.39 66.8749 1093.63 85.0506 153.25 0.0000 52.97 67.0474 91.11 0.0000 323.87 61.1471 53.44 71.7157 92.59 85.5377 156.02 0.0000 54.07 74.9415 93.35 85. 7258 158.56 0.0000 57.36 0.0000 94.56 86.0247 159.00 49.5720 57.53 90.6494 94.65 86.0465 162.33 66.1733 57.98 98.5142 94.67 86.0518 162.66 0.0000 59.27 83.5621 94.87 86.1007 163.33 58.1368 59.32 95 .1872 97.43 69.1454 165.86 80.9528 59.54 95.2726 98.43 52.8850 176.31 59.5127 60. 96 111.1378 98.44 52.8864 176.60 0.0000 61.17 111. 2309 99.53 64.5389 177.52 66. 9619 62.93 96.5634 100 .11 61. 9849 181.07 0.0000 63.29 96.6986 102.03 61. 4189 181.52 68.8295 63.58 96.8069 103.18 75.0016 184.41 69.1679 64.28 97.0678 103.37 75.0400 143.76 64. 7222 66.73 100.8901 105.21 69.1227 193.51 62.3348 67.24 107.4656 105.31 69.1409 197.03 51. 8804 125.81 100.7129 106.12 65.6884 198.01 60.6211 67.75 101.5384 106.47 81. 9605 201'. 83 63.1658 69.67 115.9398 109.28 71. 6703 203.43 62.2324 70.83 122.8900 111. 00 77.4508 205.31 55.4793 72.81 237.7312 111. 76 0.0000 210.85 83.9252 72.87 237.7802 114.06 86.3084 215.65 60.0612 74.66 133.2836 116. 30 0.0000 222 .11 57.2645 74.82 128.9833 116.74 81.3318 227.09 66.7216 74.97 118.1129 119.76 65.1668 227.38 72.4063 77 .11 179.2810 121.12 78.4520 228.16 0.0000 78.74 78.6349 121. 22 78.4706 228.18 53.2336 79.69 85.5456 121.78 73.8968 116.74 53.2336 80.12 77.8777 122.06 74.8816 235.69 47.3092 80.19 0.0000 122.92 83.4735 235. 96 47.3268 80.57 86.9042 123.07 79.7498 238.63 48.2664 81. 00 94.5558 265.00 79. 8626 238.98 0.0000 81. 07 94.5773 125.81 65.4634 240.99 48.4215 81. 75 83,. 87 91 127.23 70.7263 242.00 48.4875 83.79 84.4223 127.91 67.0412 244.70 61. 7 952 84.00 90.1099 129.30 68.5195 252.40 0.0000 85.43 69.5810 131.20 67.5364 252.80 57.3845 86.55 76.6324 133.02 78.6818 254.15 0.0000 86.79 76.6880 133.52 77.8075 256.23 49.4052 86.94 76.7237 136.00 77.2607 260.90 . 0. 0000 Page 4450 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 35.6689 355.39 0.0000 584.27 14. 6711 264.80 29.7295 356.01 26.2988 595.83 0.0000 265.00 28.5476 364.49 0.0000 427.87 26.4699 268.22 41. 4005 366.42 0.0000 602.52 0.0000 269.46 43.0587 372. 51 39.1866 604.72 23.8834 270.03 43.0895 375.05 35.7088 607.14 27.6398 271.23 43.1532 377.52 37.5806 609.32 27.6779 273.65 0.0000 356.01 26.1007 610.33 27.6948 276.40 50.6633 388.16 29.8176 61,4.28 20. 8211 277.37 50.7222 388.63 0.0000 618.01 25.6846 277.60 50. 7363 391.69 41. 6969 620.36 30.0075 278.00 55.5950 264.66 29.2389 621.93 15.0180 279.20 44.7821 401.81 30.1835 630.19 0.0000 279.54 53.2759 402.40 30.1990 631.29 16.1816 279.70 53.2866 404.85 34. 8496 633.25 30.7811 280.46 41.2134 410.95 36.8791 634.78 0.0000 283.69 34.0712 413.71 29.5736 635.95 15.1444 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 45 .1141 423. 72 0.0000 645.85 20.6730 285.90 0.0000 427.09 29.9108 657.76 18.6256 287.50 29.3350 427.87 23.3831 657.90 0.0000 290.67 37.6221 433.94 27.2613 661.66 17.5690 293.27 0.0000 439.40 24.5506 664.57 0.0000 351.93 19.7319 453.88 20.0618 666.33 0.0000 295. 96 19.7485 463.37 27.9120 666.50 0.0000 879.38 24.7595 468.07 18.8371 667. 71 0.0000 299.98 31. 4115 473.00 0.0000 677.62 14.4044 300.09 31.4154 475.06 24.2803 685.70 0.0000 300.13 31.4170 476.78 24.7981 695.00 0.0000 301.36 31.4602 477.60 29.1925 696.49 23.5122 302.85 29.8542 482.18 20.5057 696. 51 23. 5131 256.23 26.5859 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.1628 306.78 32.4841 497.08 31.1014 697.49 20.1643 308.46 36. 7168 505.52 19*. 3719 702.65 21.3448 311. 90 45.2318 507.63 0.0000 706.68 25.3317 316.51 42.9327 511. 00 29.9207 711. 68 24.8359 319.41 0.0000 514.00 29.9841 720. 70 0.0000 320.08 0.0000 514.00 29.9854 721. 93 0.0000 321.04 33. 8371 520.40 16.0645 722.78 13.6270 323.87 37.3327 520.69 0.0000 722. 91 13.6279 325.23 45.8833 522.65 0.0000 723. 31 13.6309 328.76 0.0000 527.90 0.0000 724 .19 13. 6372 333.37 39.8474 528.26 19 .. 1825 727. 33 27.3193 333.97 30.8687 529.59 17.1785 733.00 15.0708 334.37 36.0280 529.87 0.0000 735.93 17.1515 338.28 26.6993 531. 02 0.0000 333.97 10.2993 338.32 26.6999 537.26 0.0000 739.50 0.0000 311. 90 26.7586 546.56 0.0000 747.24 12.6516 340.48 26.7586 552.55 25.6612 748.06 16.1089 340.55 0.0000 563.25 23.2599 752.31 13.8379 344.28 22. 0962 569.33 18.6826 753.82 0.0000 345.93 29.5100 946.00 20.2411 756.73 16.6430 351.06 29.6608 569.70 20.2443 756.80 16.6436 351.93 29.6864 583.19 14.6614 884.68 10.4399 Page 4451 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 6. 9663 1274.44 15.4409 1620.50 1. 8811 766.42 6. 9685 1001.03 12.5695 1621. 92 3.7635 766.84 6.9700 1002.74 11.0575 1678.03 0.0000 772. 60 0.0000 1004.73 23.2390 1690.97 3.8291 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 8.7697 778.90 13.1474 1028.54 0.0000 1063.66 16.5883 783.70 0.0000 1037.84 12.7509 1771.35 7.8082 785.37 16.8826 1038.76 0.0000 1791.20 0.0000 792.07 0.0000 631. 29 13.7778 1808.65 3.9383 794.95 14.1348 1048.07 0.0000 1810.72 0.0000 795.86 14.1411 1049.04 18.7159 1836.06 3. 9631 810.06 10.6787 1050.41 9.8553 810.29 9.7898 1063.66 20.8000 344.28 9.7908 1077.00 0.0000 810.76 9*.7922 1077.34 17.9198 815.77 0.0000 1085.87 7.9897 1048.07 0.0000 1093.63 21. 0320 832.01 17.9834 1099.45 15.0549 834.85 18.0072 1112. 07 15.1245 835.71 18.9153 1112.84 16.1367 836.80 0.0000 1115. 54 6.4609 846.75 0.0000 *1120.29 12.1348 '846.77 18.1067 1120.55 12 '.1362 856.80 0.0000 1221.41 12.1392 860.56 9 .1107 1129. 67 11.1611 871.09 19.0404 1131. 51 0.0000 873.19 14.6602 1147.95 0.0000 875.33 0.0000 1173.23 24. 7251 879.38 14.7007 1177.95 14.4460 880.51 13.2372 1189. 05 19.6796 883.24 13.2535 1204.77 20.8252 884.68 15.7879 1221.41 18.8470 889.28 19.3792 1231. 02 13.6554 894.76 15.7258 1235.36 0.0000 898.04 21.3070 1238.28 24.2171 900. 72 .20. 4041 1260.41 0.0000 903.28 16.9782 1271.87 10.6439 911. 20 13.9751 1274.44 10.6525 912.08 13.9806 1274.54 12.7837 923.98 0.0000 1291.59 9.6394 926.50 12.0039 1298.22 0.0000 92 9 .11 13.5193 1312 .11 0.0000 937.49 18.8434 1332.49 6.9422 944 .13 0.0000 1362.66 0.0000 946.00 17.9650 1365.19 8.7642 949.00 13.2536 1368.63 0.0000 667.71 0.0000 1384. 29 3.3052 962.31 20.9419 1408.01 7.7661 964.08 16.7659 1457.56 0.0000 966 .17 12.2039 1460.82 9.0107 911. 20 20.0445 1489.16 6.3574 968. 97 20.0445 1505.03 7.2977 983.53 0.0000 1584.12 6.5218 984.45 0.0000 1596.21 0.0000 Page 4452 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:59:13.60 ********************************************************************************
GEL Laboratories LLC *
2040 .savage Road *
Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l Background file . DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 14-DEC-2015 14:00:00 Acquisition date : 3-0CT-2016 05:57:37. Sample ID G405235066 Sample quantity 1.57422E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.75 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6. 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 2 2 0 0 0 0 0 0 0 0 0 0 0 0 4 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1 0 0 Page 4453 of 5809 Energy 74.91* 77.25 87.89 93.42* 125.24 143.63* 186.03* 209.91 238.60* 241. 76 269.71 295.54 300.53 327.86* 332.76 3-38. 30* 352.00* 403.07 479.37 482.57 493.30 511. 28* 537.31 547.20 550.83 583.44* 609.29* 665.62 727. 48 761. 4 7 768.68 781. 60 822.07 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 77 157 65 92 25 36 88 49 23 292 98 57 205 27 25 26 80 256 8 12 7 16 27 18 13 16 134 181 66 30 16 22 18 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 158 131 258 176 45 103 81 96 45 139 80 82 67 42 45 28 23 27 45 47 25 20 80 29 15 15 24 43 20 19 24 26 9 13 1. 21 1. 22 1.16 1.16 0.94 1.16 1. 28 1. 09 0.97 1. 00 1. 44 1. 73 1. 28 1. 79 1. 91 1. 31 1. 38 1. 34 1. 03 3.51 1. 47 2.85 1. 90 0.55 0.76 1. 50 1. 52 1.19 4.94 0.73 1. 76 1. 77 1.12 0.85 149.90 154.58 17 5. 82 186.86 250.43 287.15 371.86 419.56 464.70 476.88 483.18 539.02 590.63 600.60 655. 21 665.00 676. 08 703.46 805.49 957.98 964. 37 985.82 1021. 76 1073.78 1093.56 1100. 81 1165. 99 1217.67 1330.28 1453.95 1521.90 1536.32 1562.17 1643.08 145 145 171 182 249 283 368 415 462 473 481 533 585 598 646 646 646 700 800 945 960 980 1014 1066 1087 1098 1159 1211 1319 1449 1507 1507 1557 1636 15 2.14E-02 29.0 1.19E+OO 15 4.35E-02 15.3 11 1.80E-02 49.8 11 2.55E-02 32.0 4 6.95E-03 42.7 8 1.00E-02 54.3 8 2.44E-02 22.9 10 1.35E-02 40.5 6 6.26E-03 51.6 8 8.12E-02 9.3 6 2.72E-02 18.1 13 1.60E-02 34.9 13 5.68E-02 11.0 8 7.38E-03 45.9 37 7.03E-03 55.2 1.28E+OO 37 7.30E-03 41.0 37 2.21E-02 16.4 9 7.12E-02 7.3 10 2.33E-03150.6 14 3.44E-03122.5 8 1.93E-03128.9 11 4.34E-03 60.4 19 7.51E-03 90.0 14 5.06E-03 68.9 10 3. 67E-03 61. 2 7 4.55E-03 45.5 16 3.72E-02 12.2 14 5.03E-02 10.8 28 l.84E-02 23.0 10 8.44E-03 32.7 40 4:46E-03 62.3 2.89E+OO 40 6.19E-03 46.4 9 5.00E-03 38.2 9 2.77E-03 73.2 Peak Search Report (continued) Page : 2 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 831.18 10 9 1. 62 1661.31 1656 9 2.77E-03 62. 8 36 0 849.74 12 7 1. 61 1698.41 1695 7 3.21E-03 48.4 37 0 861.28 19 8 2.06 1721.49 1717 11 5.39E-03 36.4 38 o* 873.87 14 1 1. 76 1746.67 1744 6 3.81E-03 30.2 39 0 911.84* 75 43 1. 50 1822.62 1815 17 2.09E-02 23.2 40 0 934.32 28 12 0.99 1867.57 1860 16 7:91E-03 32.9 41 0 964.85 15 13 1. 04 1928.63 1925 8 4.23E-03 49.1 42 0 969.82* 49 30 1. 84 1938.57 1933 16 l.36E-02 28.7 43 0 1079.64 16 7 1. 58 2158.25 2154 10 4.47E-03 40.2 44 0 1121. 57* 16 27 1. 67 2242.13 2233 12 4.51E-03 69.7 45 0 1209.50 16 22 3.74 2418.06 2408 18 4.39E-03 74.7 46 0 1225.89 11 5 1. 39 2450.86 2448 7 3.12E-03 44.7 47 0 1279.54 10 7 1. 01 2558.22 2552 10 2.88E-03 57.6 48 0 1295.04 11 6 3.42 2589.24 2582 11 2.92E-03 53.1 49 0 1378.23 12 3 1. 29 2755.74 2750 9 3.46E-03 35.9 50 0 1461.07* 356 4 1. 78 2921.53 2914 17 9.90E-02 5.5 51 0 1764.76* 43 0 1. 87 3529.59 3524 11 1.19E-02 16.0 Flag: "*" == Peak area was modified by background subtraction Page 4454 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:59:15 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 14-DEC-2015 14:00:00 G405235066 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 05:57:37 157.42 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA33 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4455 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66' TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.75 . 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM. %Error Status K-40 1460.82 10.66* 1.133E+OO 1. 363E+Ol 1.363E+Ol 11. 02 OK CD-109 88.03 3.70* 4.949E+OO 8.003E-01 1.244E+OO 275.99 OK SN-126 64.28 9.60 2.578E+OO Line Not Found Absent 86.94 8.90 4.949E+OO 3.327E-01 3.327E-01 275.99 OK 87.57 37.00* 4.949E+OO 8.003E-02 8.003E-02 275.99 OK CS-135 268.22 16.00* 4.353E+OO 4.598E-01 4.598E-01 69.88 OK TL-208 277.37 6.60 4.258E+OO Line Not Found Absent 583.19 85.00* 2.333E+OO 3.468E-01 3.468E-01 24.30 OK 860.56 12.50 1. 726E+OO 4.421E-01 4.421E-01 72. 71 OK PB-212 74.82 10.28 3.809E+00 3.818E-01 3.818E-01 194.45 OK 77 .11 17.10 4.047E+OO 1.422E+OO 1.422E+OO 30.55 OK 238.63 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 OK 300.09 3.30 3.995E+OO 1. lllE+OO 1. lllE+OO 91. 90 OK BI-214 609.32 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 OK 1120. 29 14.92 1. 406E+OO 3.689E-01 3.690E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 OK PB-214 74.82 5.80 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.047E+OO 2.507E+OO 2.508E+00 30.55 OK 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4.727E+OO Line Not Found <<INT Reject 295.22 18.42 4.049E+OO 1.515E+OO 1.516E+OO 21.95 OK 351.93 35.60* 3.512E+OO 1.112E+OO 1.112E+OO 14.65 OK RN-222 609.32 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 OK 1120.29 14.92 1. 406E+OO 3.689E-01 3.690E-01 139.45 OK 1764.49 15.30 9.590E-01 l.318E+00 1.318E+OO 31. 95 OK RA-224 240.99 4.10* 4.731E+OO l.683E-01 1.683E-01 703.88 OK RA-226 609.32 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 OK 1120.29 14.92 1.406E+OO 3.689E-01 3.690E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+00 1.318E+OO 31. 95 OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 . 11. 27 3.628E+OO 1.061E+OO 1. 061E+OO 32.79 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835.71 1. 61 1.766E+OO Line Not Found Absent 911.20 25.80* 1.652E+00 B.612E-01 8.612E-01 46.46 OK 968. 97 15.80 1.575E+00 9. 513E-01 9.513E-01 57.. 44 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.628E+OO 1.061E+OO 1. 061E+OO 32.79 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835. 71 . 1. 61 1. 766E+00 Line Not Found Absent 911.20 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 OK 968.97 15.80 1.575E+OO 9.513E-01 9.513E-01 57.44 OK TH-228 74.82 10.28 3.809E+OO 3.818E-01 3.818E-01 194.45 OK 77 .11 17.10 4.047E+OO 1.422E+OO 1.*422E+OO 30.55 OK 238.63 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 OK 300.09 3.30 3.995E+OO 1. lllE+OO 1. lllE+OO 91. 90 OK TH-230 609.32 45.49* 2.255E+00 9.030E-01 9.030E-01 21. 54* OK 1120.29 14.92 1.406E+OO 3.689E-01 3.689E:-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO l.318E+00 31. 95 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent Page 4456 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 301.36 5.35* 3.995E+OO 6.853E-01 6.853E-01 91. 90 OK TH-232 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.628E+OO l.061E+OO l.061E+OO 32.79 OK 835.71 l.61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 OK 968. 97 15.80 l.575E+OO 9. 513E-01 9.513E-01 57.44 OK U-234 609.32 45.49* 2.255E+OO 9.030E-01 9.030E-01 21. 54 OK 1120.29 14.92 l.406E+OO 3.689E-01 3.689E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 OK U-235 89. 96 3.47 5.092E+OO Line Not Found Absent 93.35 5.60 5.306E+OO 1.904E+OO l.904E+OO 64.00 OK 143.76 10. 96* 6.182E+OO 3.160E-01 3.160E-01 108.58 OK 163.33 5.08 5. 963E+OO Line Not Found Absent 185.72 57.20 5.613E+OO 1.579E-01 l.579E-01 45.87 OK 205.31 5.01 5.295E+OO Line Not Found Absent AM-243 43.53 5.90 2. 461E-01 Line Not Found Absent 74.66 67.20* 3.809E+OO 5.841E-02 5.842E-02 194.45 OK CM-247 278.00 3.40 4. 251E+OO Line Not Found Absent 287.50 2.00 4 .139E+OO' Line Not Found Absent 402.40 72.00* 3.142E+OO l.980E-02 l.980E-02 301.27 OK ANH-511 511. 00 100.00* 2.591E+OO 5. 441E-02 5. 441E-02 179.92 OK Flag: "*" = Keyline Page 4457 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:59:16.99

GEL Laboratories LLC *
2040 Savage Road * *
Charleston, SC 29407 * ******************************************************************************* * *
DETECTOR AND SAMPLE DATA * * *
Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l *
Acquisition date 3-0CT-2016 05:57:37 Sensitivity : 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
Elapsed real time: 0 Half life ratio : ***** *
Sample date 14-DEC-2015 14:00:00 Analyst initials: MXRl *
Sample ID G405235066 Sample Quantity 1.5742E+02 GRAM *
Batch Number 1596254 Wet Weight 0.00000 *
Wet wt corr 1.00000 Dry Weight 0.00000 *
Nuclide Library : SOLID.NLB;6 * * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 07:00:49 Eff. Geometry : CAN *
Eff. File : DKA100: [CANBERRA*. GAMMA] EFF GAM33 CAN. CNF; 8
Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.363E+Ol 1.472E+00 5.902E-01 CD-109 1.244E+OO 3.365E+OO 2.309E+OO SN-126 8.003E-02 2.165E-01 l.495E-01 CS-135 4.598E-01 3.149E-01 2.140E-01 TL-208 3.468E-01 8.259E-02 5.293E-02 PB-212 7.919E-01 l.436E-01 l.133E-01 BI-214 9.033E-01 l.907E-01 9.393E-02 PB-214 1.112E+OO 1.597E-01 1.158E-01 RN-222 9.033E-01 l.907E-01 9.393E-02 RA-224 1.683E-01 1.161E+OO 1.280E+OO RA-226 9.033E-01 *1.907E-01 9.393E-02 AC-228 8.612E-01 3.921E-01 2.092E-01 RA-228 8.612E-01 3. 921E-01 2.092E-01 TH-228 7.919E-01 l.436E-01 l .133E-01 .TH-230 9.030E-01 1.906E-01 9.390E-02 PA-231 6.853E-01 6.171E-01 6.582E-01 TH-232 8.612E-01 3.921E-01 2.092E-01 U-234 9.030E-01 l.906E-01 9.390E-02 U-235 3.160E-01 3.363E-01 3.024E-01 AM-243 5.842E-02 l .113E-01 9.349E-02 CM-247 1. 98 OE-02 5.846E-02 5.853E-02 ANH-511 5.441E-02 9.595E-02 5.050E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -7.443E+OO 1.216E+Ol 1.933E+Ol NOT IDENT. NA-22 5.034E-03 3.635E-02 7.094E-02 NOT IDENT. NA-24 0.000E+OO 1.084E+41 O.OOOE+OO SHORT HLIF AL-26 l.OOlE-02 2.018E-02 5.505E-02 NOT IDENT. SC-4 fr -1.658E-02 2.739E-01 5.499E-01 FAIL ABUN V-48 O.OOOE+OO 8.568E+o3 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.904E+02 O.OOOE+OO SHORT HLIF MN-54 -9.583E-03 7.195E-02 1.188E-01 NOT IDENT. Page 4458 of 5809 C0-56 9.684E-03 3.839E-01 6.840E-Ol NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF *co-57 3.917E-02 4.439E-02 9.045E-02 NOT IDENT. C0-58 3.632E-02 4.861E-01 9.623E-Ol NOT IDENT. FE-59 -l.466E+OO 4.479E+OO 8.864E+OO NOT IDENT. C0-60 -2.054E-03 3.394E-02 6.952E-02 NOT IDENT. ZN-65 8.785E-02 1. 742E-01 3.432E-01 NOT IDENT. GE-68 -7.222E-02 2.336E+OO 4.200E+OO NOT IDENT. AS-73 -8.102E+OO 9.377E+OO 1. 747E+Ol NOT IDENT. AS-74 0.000E+OO 4.162E+03 O.OOOE+OO SHORT HLIF SE-75 4.292E-03 1. 801E-01 3.074E-01 NOT IDENT. BR-77 0.000E+OO 4.280E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.437E+02 0. OOOE+OO
SHORT HLIF RB-83 -3.002E-01 6.108E-01 l.125E+OO NOT IDENT. KR-85 3.992E-01 6.342E+OO l.252E+Ol NOT IDENT. SR-85 3.821E-02 6.279E-01 l.239E+OO NOT IDENT. RB-86 O.OOOE+OO 2.069E+04 O.OOOE+OO SHORT HLIF Y-88 -2.956E-03 1.405E-01 3.267E-01 NOT IDENT. Y-91 -8.607E+Ol 4.232E+02 7.321E+02 NOT IDENT. NB-94 1. 978E-02 2.529E-02 5.579E-02 NOT IDENT. NB-95 3.569E-02 6.525E-01 1.295E+OO NOT IDENT. NB-95M -8.355E-02 2.648E+OO 3.860E+OO NOT IDENT. ZR-95 l.340E+OO 1.345E+OO 2.946E+OO NOT IDENT. NB-97 O.OOOE+OO 1.626E+41 O.OOOE+OO SHORT HLIF ZR-97 o:ooOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.769E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1.292E-02 3.346E-02 5.627E-02 NOT IDENT. RH-102 9.594E-03 5.214E-02 1.054E-01 NOT IDENT. RU-103 3. 710E+OO 4.479E+OO 9.260E+00 FAIL ABUN RH-106 -3.908E-02 4 .115E-01 8.046E-01 NOT IDENT. RU-106 -3.908E-02 4 .115E-01 8.046E-01 NOT IDENT. AG-108M -5.630E-03 2.295E-02 4.462E-02 NOT IDENT. AG-llOM -4.578E-02 8.237E-02 1.433E-01 NOT IDENT. SN-113 -9.855E-02 1. 996E-01 3.762E-01 NOT IDENT. CD-115 O.OOOE+OO 4.335E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.958E+04 O.OOOE+OO SHORT HLIF TE-123M -7.498E-02 l.300E-01 2.304E-01 NOT IDENT. SB-124 -3. 960E-01 1.728E+OO 3.476E+OO NOT IDENT. SB-125 -4.793E-02 8.678E-02 l.618E-01 NOT IDENT. TE-125M l.504E+02 2.528E+02 5.027E+02 NOT IDENT. I-126 O.OOOE+OO l.505E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.793E+05 O.OOOE+OO SHORT HLIF SB-127 0. OOOE+OO 6.305E+21 O.OOOE+oo* SHORT HLIF I-131 O.OOOE+OO 2.421E+09 O.OOOE+OO SHORT HLIF I"-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9. 296E+25 O.OOOE+OO SHORT HLIF BA-133* -5.271E-03 4.182E-02 7.372E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 3.738E-02 5.'.386E-02 1.113E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO l.999E+05 O.OOOE+OO SHORT HLIF BA-137M 4.766E-02 3.147E-02 7.311E-02 NOT IDENT. CS-137 5.035E-02 3.325E-02 7.724E-02 NOT IDENT. CE-139 3.106E-02 l. lOlE-01 2.090E-01 NOT IDENT. BA-140 O.OOOE+OO 1.802E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.768E+05 O.OOOE+OO SHORT HLIF CE-141 -3.102E+OO 1. 965E+Ol 3.367E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 727E+41 O.OOOE+OO SHORT HLIF CE-144 -8.942E-02 3.272E-01 6.048E-01 NOT IDENT. PM-144* -5. OllE-02 4.621E-02 7.339E-02 NOT IDENT. PR-144 -4.339E+OO 4.00lE+OO 6.355E+OO NOT IDENT. PM-146 7.869E-03 4.209E-02 8.461E-02 NOT IDENT. ND-147 0.000E+OO 2.171E+07 O.OOOE+OO SHORT HLIF PM-147 4.383E+02 7.779E+02 1.549E+03 NOT IDENT. PM-149 0.000E+OO 5.583E+39 O.OOOE+OO SHORT HLIF EU-150 4.121E-02 3.312E-02 4.265E-02 FAIL ABUN EU-152 -l.339E-02 8.072E-02 l.523E-01 FAIL ABUN GD-153 ..:.7.730E-02 l.786E-01 3.028E-01 NOT IDENT. EU-154 2.384E-02 9.217E-02 l.843E-01 FAIL ABUN EU-155 8.918E-02 9.900E-02 2.042E-01 FAIL ABUN TB-160 -1. 67 9E+OO 1.579E+OO 2.394E+OO FAIL ABUN H0-166M 3.825E-02 4.747E-02 l.048E-01 NOT IDENT. TM-171 -4.540E+OO 2.330E+Ol 4.649E+Ol NOT IDENT. HF-172 2.887E-01 2.414E-01 4.283E-01 FAIL ABUN LU-172 4. 950E-.02 7.020E-02 1. 572E-01 FAIL ABUN LU-176 -l.364E-02 2.107E-02 3.977E-02 FAIL ABUN HF-181 2.028E+OO 5.125E+OO 7.441E+00 FAIL ABUN Page 4459 of 5809 TA-182 1.052E-01 1.00lE+OO 1. 788E+OO FAIL ABUN RE-183 1.676E+OO 3.108E+OO 6.473E+OO NOT IDENT. RE-184 8.704E-01 2.489E+Ol 4.835E+Ol NOT IDENT; W-188 -6. 511E+OO 1.029E+02 l.851E+02 NOT IDENT. IR-192 1.746E-01 3.605E-01 7.621E-01 FAIL ABUN HG-203 1.610E-01 2.000E+OO 4.038E+OO NOT IDENT. BI-207 5.367E-03 3.978E-02 8.420E-02 FAIL ABUN PB-210 4.628E+OO 4.679E+OO 1.033E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.400E-01 7.767E-01 FAIL ABUN PB-211 -9.432E-02 6.226E-01 l.093E+OO FAIL ABUN BI-212 1.163E+OO 7.461E-01 1.189E+OO FAIL ABUN RN-219 2.160E-01 6.377E-01 7.285E-01 FAIL ABUN RA-223 -2. 711E-01 5.497E-01 9.297E-01 FAIL ABUN AC-227 9.681E-02 2.199E-01 4.205E-01 FAIL ABUN TH-227 9.681E-02 2.199E-01 4.205E-01 FAIL ABUN TH-229 -4.881E-01 4.351E-01 7.145E-01 FAIL ABUN TH-231 -2. 711E-01 5.497E-01 9.297E-01 FAIL ABUN PA-233 1.288E-02 5.506E-02 l.123E-01 FAIL ABUN PA-234 -2.113E-01 2.665E-01 4. 331E-01 FAIL ABUN PA-234M 3.533E+OO 4.433E+OO 9.538E+OO NOT IDENT. TH-234 -2.287E-01 l.460E+OO 2.912E+OO FAIL ABUN NP-237 l.288E-02 5.506E-02 1.123E-01 FAIL ABUN NP-238 O.OOOE+OO 5.388E+40 O.OOOE+OO SHORT HLIF U-238 -2.287E-01 1.460E+OO 2.912E+OO FAIL ABUN NP-239 1.425E-01 2.245E-01 4.513E-01 NOT IDENT. PU-239 3.127E+02 3 .111E+02 6.297E+02 NOT IDENT. AM-241 6.229E-02 l.526E-01 3.129E-01 NOT IDENT. CM-243 -9. 302E...:.02 9.417E-02 l.660E-01 . NOT !DENT. BK-247 -2.424E-02 6.537E-02 1.043E-01 NOT IDENT. CF-249 -l.814E-02 3.201E-02 5.995E-02 FAIL ABUN CF-251 6.243E-02 1. 047E-01 2.058E-01 NOT IDENT. Page 4460 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:59:14.34 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 345 10.66* 1.133E+OO 1. 363E+Ol l.363E+Ol 11. 02 CD-109 88.03 84 3.70* 4.949E+OO 2.197E+OO 3.415E+OO 99.57 SN-126 64.28 ------9.60 2.578E+OO ------Line Not Found ------8 6. 94 84 8.90 4.949E+OO 9.133E-01 9.133E-01 99.57 87.57 84 37.00* 4.949E+OO 2. 197E-0.1 2.197E-01 99.57 CS-135 2 68. 22 67 16.00* 4.353E+OO 4.598E-01 4.598E-01 69.88 TL-208 277.37 ------6.60 4.258E+OO ------Line *Not Found ------583.19 144 85.00* 2.333E+OO 3.468E-01 3.468E-01 24.30 860.56 20 12.50 1.726E+OO 4.421E-01 4.421E-01 72. 71 BI-211 72. 87 ------1. 23 3. 591E+OO ------Line Not Found ------351.06 291 12.92* 3.512E+OO 3.064E+OO 3.064E+OO 14.65 PB-212 74.82 102 10.28 3.809E+OO 1.237E+OO 1.237E+OO 58.08 77 .11 206 17.10 4.047E+OO 1.422E+OO 1.422E+OO 30.55 238.63 346 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 300;09 31 3.30 3.995E+OO 1.lllE+OO 1. lllE+OO 91. 90 BI-214 609.32 194 45.49* 2. 255E+00' 9.030E-01 9.033E-01 21. 54 1120.29 16 14.92 l.406E+OO 3.689E-01 3. 690E.-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 PB-214 74.82 102 5.80 3.809E+OO 2.192E+OO 2.193E+OO 58.08 77 .11 206 9.70 4.047E+OO 2.507E+OO 2.508E+OO 30.55 87.09 84 3.41 4.949E+OO 2.384E+OO 2.384E+OO 99.57 242.00 116 7.25 4. 731E+OO 1.610E+OO 1. 611E+OO 36.10 295.22 237 18.42 4.049E+OO 1.515E+OO 1.516E+OO 21. 95 351. 93 291 35.60* 3.512E+OO 1.112E+OO 1.112E+OO 14.65 RN-222 609.32 194 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 1120.29 16 14.92 1.406E+00 3.689E-01 3.690E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 RA-224 240.99 116 4.10* 4.731E+OO 2.848E+OO 2.848E+OO 36.10 RA-226 609.32 194 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 1120.29 16 14.92 1.406E+OO 3.689E-01 3.690E-01 139.45 1764.49 41 15.30 9.590E-01 l.318E+OO 1.318E+OO 31. 95 AC-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 91 11. 27 3.628E+OO 1. 061E+OO 1.061E+OO 32.79 794.95 ------4.25 l.835E+OO ------Line Not Found ------835. 71 ------1. 61 1.766E+OO ------Line Not Found ------911.20 77 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 968. 97 50 15.8.0 1.575E+OO 9.513E-01 9.513E-01 57.44 RA-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 91 11. 27 3.628E+OO 1.061E+OO 1.061E+OO 32.79 794.95 ------4.25 l.835E+OO ------Line Not Found ------835. 71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 77 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 968. 97 50 15.80 1. 575E+OO 9. 513E-01 9.513E-01 57.44 TH-228 74.82 102 10.28 3.809E+OO 1.237E+OO 1.237E+OO 58.08 77 .11 206 17 .10 4.047E+OO 1.422E+OO 1.422E+OO 30.55 238.63 346 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 300.09 31 3.30 3.995E+OO 1. lllE+OO 1. lllE+OO 91. 90 Page 4461of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-230 609.32 194 45.49* 2.255E+OO 9.030E-01 9.030E-01 21. 54 1120.29 16 14.92 l.406E+OO 3.689E-01 3.689E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 31 5.35* 3.995E+OO 6.853E-01 6.853E-01 91. 90 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 91 11. 27 3.628E+OO 1.061E+OO 1.061E+OO 32.79 835.71 ------1. 61 1.766E+OO ------Line Not Found ------911.20 77 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 968. 97 50 15.80 1.575E+OO 9.513E-01 9.513E-01 57.44 U-234 609.32 194 45.49* 2.255E+OO 9.030E-01 9.030E-01 21. 54 1120.29 16 14.92 1.406E+00 3.689E-01 3.689E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 U-235 89. 96 ------3.47 5.092E+OO ------Line Not Found ------93.35 119 5.60 5.306E+OO 1.904E+OO 1.904E+OO 64.00 143.76 45 10. 96* 6.182E+00 3.160E-01 3.160E-01 108.58 163.33 ------5.08 5. 963E+OO ------Line Not Found ------185.72 106 57.20 5.613E+00 1. 579E-01 1. 579E-01 45.87 205.31 ------5.01 5.295E+OO ------Line Not Found ------AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 102 67.20* 3.809E+OO 1.892E-01 1.892E-01 58.08 CM-247 278.00 ------3.40 4. 251E+OO ------Line Not Found ------287.50 ------2.00 4.139E+OO ------Line Not Found ------402.40 9 72.00* 3.142E+OO 1. 98 OE-02 1.980E-02 301.27 ANH-511 511. 00 30 100.00* 2.591E+00 5.441E-02 5. 441E-02 179.92 Flag: "*" Key line Page 4462 of 5809 Page : 3 Surrunary of Nuclide Activity Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Total number of lines in spectrum 51 Number of unidentified lines 15 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 TL-208 BI....:211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 CM-247 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 1.41E+10Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600.00Y 1600. OOY 1.41E+10Y 1600. OOY 1.41E+10Y 1.41E+l0Y 1.41E+10Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1. 56E+07Y 1.00E+09Y Decay 1. 00 1. 55 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Total Activity Uncorrected pCi/GRAM 1. 363E+Ol 2.197E+OO 2.197E-01 4.598E-01 3.468E-01 3.064E+OO 7.919E-01 9.030E-01 1.112E+00 9.030E-01 2.848E+OO 9.030E-01 8.612E-01 8.612E-01 7.919E-01 9.030E-01 6.853E-01 8.612E-01 9.030E-01 3.160E-01 1.892E-Ol 1.980E-02 5.441E-02 3.382E+Ol 3.382E+Ol Decay Corr pCi/GRAM 1.363E+Ol 3.415E+OO 2.197E-01 4.598E-01 3.468E-01 3.064E+OO 7.919E-01 9.033E-01 .1.112E+OO 9.033E-01 2.848E+OO 9.033E-01 8.612E-01 8.612E-01 7.919E-01 9.030E-01 6.853E-01 8.612E-01 9.030E-01 3.160E-01 1.892E-01 1. 980E-02 5.441E-02 3.504E+Ol 3.504E+Ol 70.59% Decay Corr 2-Sigma Error 0.150E+Ol 3.400E+OO 2.187E-01 3.213E-01 0.843E-01 0.449E+OO 1.465E-01 1. 946E-01 0.163E+OO 1. 946E-01 1. 028E+OO 1.946E-01 4.00lE-01 4.00lE-01 1. 465E-01 1.945E-01 6.297E-01 4. OOlE-01 1.945E-01 3. 431E-01 l.099E-01 5. 965E-02 9.790E-02 "M" Manually accepted 2-Sigma %Error 11:02 99.57 99.57 69.88 24.30 14. 65 . 18.50 21. 54 14.65 21. 54 36.10 21. 54 46.46 46.46 18.50 21. 54 91. 90 46.46 21. 54 108.58 58.08 301.27 179.92 "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit. Page 4463 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235066 Acquisition date : 3-0CT-2016 05:57:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 125.24 32 57 0.94 250.43 249 4 6.95E-03 85.3 6.21E+OO T 0 209.91 58 115 1. 09 419.56 415 10 l.35E-02 80.9 5.22E+OO T 0 232.51 27 54 0.97 464.70 462 6 6.26E-03 **** 4.87E+OO 4 327.86 29 52 1. 91 655.21 646 37 7.03E-03 **** 3.72E+OO T 4 332.76 30 33 1. 31 665.00 646 37 7.30E-03 82.Q 3.68E+OO T 0 479.37 14 51 3.51 957.98 945 14 3.44E-03 **** 2.73E+OO 0 482.57 8 28 1. 47 964. 37 960 8 1. 93E-03 **** 2. 71E+OO T 0 493.30 17 22 . 2. 85 985.82 980 11 4.34E-03 **** 2.67E+OO T 0 537:31 20 31 0.55 1073.78 1066 14 5.06E-03 **** 2.49E+OO T 0 547.20 14 16 0.76 1093.56 1087 10 3.67E-03 **** 2.45E+OO T 0 550.83 18 16 1. 50 1100.81 1098 7 4.55E-03 90.9 2.44E+OO 0 665.62 70 21 4.94 1330.28 1319 28 1. 84E-02 46.0 2.lOE+OO T 0 727.48 32 20 0.73 1453.95 1449 10 8.44E-03 65.5 1.97E+OO T 1 761. 47 17 25 1. 76 1521. 90 1507 40 4.46E-03 **** 1.90E+OO 1 768.68 23 27 1. 77 1536.32 1507 40 6.19E-03 92.9 1.88E+OO 0 781. 60 19 9 1.12 1562.17 1557 9 5.00E-03 76.4 1.86E+OO 0 822.07 i"o 14 0.85 1643.08 1636 9 2.77E-03 **** 1. 7 9E+OO 0 831.18 10 . 9 1. 62 1661.31 1656 9 2.77E-03 **** l.77E+00 T 0 849.74 12 8 1. 61 1698.41 1695 7 3.21E-03 96. 8 l.74E+OO 0 873.87 14 1 1. 76 1746.67 1744 6 3.81E-03 60.5 1. 71E+OO T 0 934.32 29 12 0.99 1867.57 1860 16 7. 91E-03 65.9 1-. 62E+OO 0 964. 85 16 13 1. 04 1928.63 1925 8 4.23E-03 98.3 1.58E+OO T 0 1079.64 16 7 1. 58 2158.25 2154 10 4.47E-03 80.3 l.45E+00 0 1209.50 16 22 3.74 2418.06 2408 18 4.39E-03 **** 1.32E+OO 0 1225.89 11 5 1. 39 2450.86 2448 7 3.12E-03 89.5 1.31E+OO 0 1279.54 10 7 1. 01 2558.22 2552 10 2.88E-03 **** l.27E+00 0 1295.04 10 5 3.42 2589.24 2582 11 2.92E-03 **** 1.25E+OO 0 1378.23 12 2 1. 29 2755.74 2750 9 3.46E-03 71. 9 1.19E+OO Flags: "T" = Tentatively associated Page 4464 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:59:28.94 *******************************************************************************
GEL Laboratories LLC *
2040 Savage Road *
Charleston, SC 29407 * ******************************************************************************* * * *
DETECTOR AND SAMPLE DATA * *
Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l *
Acquisition date 3-0CT-2016 05:57:37 Sensitivity 3.000 *
Detector ID GAM33 Energy tolerance: 1.500 *
Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: O 01:00:00.75 Half life ratio : ***** *
Sample date 14-DEC-2015 14:00:00 Nuclide Library : SOLID *
Sample ID G405235066 Analyst initials: MXRl *
Batch Number 1596254 Sample Quantity : 1.5742E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
Dry Weight : 0.00000 * ******************************************************************************* * * *
CALIBRATION INFORMATION * *
Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
Eff. File . * : DKAlOO: [CANBERRA. GAMMA] EFF GAM33 CAN. CNF; 8
Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 CM-247 ANH-511 Le (pCi/GRAM 2.413E-01 1. 096E+OO 7.093E-02 9.730E-02 2.310E-02 5.339E-02 4.047E-02 5.248E-02 4.047E-02 6. 051E-01 4.047E-02 8.915E-02 8.915E-02 5.339E-02 4.046E-02 2.973E-01 8.915E-02 4.046E-02 1. 410E-01 4.'.399E-02 2.630E-02 2.267E-02 ----Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4465 of 5809. Le (pCi/GRAM 8.591E+OO 2.909E-02 O.OOOE+OO 2.061E-02 2.305E-01 O.OOOE+OO O.OOOE+OO 5.223E-02 2.893E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4466 of 5809 0.000E+OO 4.246E-02 4.162E-01 3.644E+OO 2.884E-02 1.505E-01 1. 803E+OO 8.016E+OO O.OOOE+OO l.394E-01 O.OOOE+OO 0.000E+OO 5.007E-0°1 5.630E+OO 5.572E-01 O.OOOE+OO l.157E-01 3.047E+02 2.460E-02 5.632E-01 1. 793E+OO 1.320E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.620E-02 4.644E-02 4.135E+00 3. 501E-01 3.501E-01 l.980E-02 5.953E-02 l.692E-01 O.OOOE+OO O.OOOE+OO l.077E-01 1.336E+00 7.168E-02 2.364E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.357E-02 O.OOOE+OO 5.012E-02 O.OOOE+OO O.OOOE+OO 3.300E-02 3.486E-02 9.816E-02 O.OOOE+OO O.OOOE+OO 1.562E+Ol O.OOOE+OO 2.820E-01 3.094E-02 2.679E+00 3. 831E-02 O.OOOE+OO 7.260E+02 O.OOOE+OO 1.938E-02 6.875E-02 l.413E-01 7.647E-02 9.576E-02 9.815E-01 4.627E-02 2.138E+Ol 2.009E:._01 6.883E-02 1.804E-02 3.348E+00 7.852E-01 SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238. NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4467 of 5809 3.024E+OO 2. 091E+Ol 8.493E+Ol 3.474E-01 l.864E+OO 3.600E-02 4.800E+OO 3.737E-01 4.898E-01 5.439E-01 3.319E-01 4.198E-01 1.944E-01 .1. 944E-01 3.290E-01 4 .-198E-01 5.164E-02 1.824E-01 4.261E+OO l.379E+oo* 5.164E-02 O.OOOE+OO 1.379E+OO 2 .114E-01 2.973E+02 1.465E-01 7.714E-02 4.699E-02 2.682E-02 9.599E-02 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.}}

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