Text

Revision 003 to CP 3804L, PASS Containment Air Sample
	ML16014A224
Person / Time
Site:	Millstone
Issue date:	12/29/2015
From:	; Dominion Nuclear Connecticut
To:	; Document Control Desk, Office of Nuclear Reactor Regulation
References
	CP 3804L, Rev. 3
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TPCKOZ PASSPORT DOCUMENT To :DOCUMENT CONTROL DESK Facility :MP Department: TRANSMITTAL Address :U.S. NUCLEAR REGULATORY COMMISSION DOCUMENT CONTROL DESK (0140)

From Date/Time WASHINGTON, DC 20555-0001

CONTROLLED

12/29/15 13:

DOCUMENTS Dlillllii Page:

Di1111 Trans No. : 000153267 Transmittal Group Id: 1511845 Total Items: 00001 Item Facility Type Sub Document Number/ITitle Sheet Revision Doc Date Copy # Media Copies

0001 MP PROC CH CP 3804L 003 P 01 PASS CONTAINMENT AIR SAMPLE Please check the appropri~ate response and return form to NDS Bldg 475/3 Millstone Power Station or Fax to 860-440-2057.

3 All documents received.

Documents noted above not received (identify those not received).

Iolonger require distribution of these documents.

Date: Date:Signature:

I , ,

S Dominio-° A dministrative Correction A uthorization CP 3804L - *03 PASS Containment Air Sample

4. Requestor(s) Print Name(s) / Locations 5. Date 6. Requestor Phone Greg D'Auria 12/29/15 4575

7. Applicable Nuclear Station(s)

Millstone [] North Anna LI Surry LI

8. Please check below to indicate the type of administrative correction needed.

[] Updating titles, names, phones numbers, document format, procedure numbers, or references LI Misspellings (e.g., "adn" instead of "and")

LI Incorrect step number sequencer eg. "6.3.1, 6.3.3, 6.3.2" instead of"'6.3.1, 6.3.2, 6.3.3")

LI Incorrect page numbers in the headers and attachments (e.g., "PAGE 82 of 80" instead of "PAGE 82 of 82")

LI Incorrect pagination, such as incorrect page breaks Lii Incorrect transitions, branches, and references (e.g., referenced procedure has been renumbered)

LI Mistakes occurring during duplication (cloning) of procedures (e.g., Unit 1 panel number, equipment location number, or procedure number in a Unit 2 procedure)

LI Incorrect equipment location numbers, if the noun descriptor fits the application LI Incorrect noun descriptor, if the equipment location number is accurate LI Mistakes or computer file corruptions that occurred during the posting process

[] Other: Changed instances of VERIFY to CHECK or ENSURE as applicable.

Errors in setpoints, measurements, or quantitative acceptance criteria shall not be considered an administrative correction Authorization for Permanent Administrative Correction

9. Procedure Process Management SignatureA 10. Date

11. M'anager Nuclear Operations Signature (Required for E--s FCAs, or FSGs) 12. Date N/A Administrative Correction Completed By ____________

Jeff D. Urgitis ** /**12/29/15 NOTE: The individual(s) posting an Administrat~,e *orrection to EDM re responsible for ensuring Nuclear E-Forms is updated.

16. Nuclear E-Forms Updated for Site(s)? 17. Nuclear E-Forms Updated Print Namne/Signature 18. Date LIMP LINA LISU M]N/A NIA

19. Technical Procedure Number: 20. Revision: 21. Effective I~ate.

cP 3804. 003/i Form No. 730689(May 2015)

MILLSTONE POWER STATION CHEMISTRY PROCEDURE STOP THINK Aii¸i¸ CTii* RE'IE PASS Containment Air Sample

[e*.Ref. 6.28]

CP 3804L Rev. 003 NOTE A review by the Emergency Planning Department is required whenever this procedure is revised or whenever changes are made to this procedure which impact the ability to collect and analyze a PASS sample.

12/29/15 12/29/15 DatUe:

Apprval EffetiveuDate Level of Use Continuous

Millstone Unit 3 Chemistry Procedure PASS Containment Air Sample TABLE OF CONTENTS

1. PURPOSE.................................................. 2

2. PREREQUISITES ........................................... 2

3. PRECAUTIONS ............................................. 7

4. JINSTRUCTIONS ............................................ 8 4.1 Preparation for PASS Sample Acquisition ..................... 8 4.2 Sample Acquisition..................................... 15 4.3 System Flush Prior To Sample Retrieval ..................... 17 4.4 Retrieval of Containment Air Samples ...................... 18 4.5 Sample Analysis........................................ 21 4.6 Gas Isotopic Analysis.................................... 22 4.7 Gas Composition Analysis ............................... 24 4.8 Restoration from PASS Sample Acquisition .................. 25

5. REVIEW AND4T SIGNOFF............. ........................ 31

6. REFERENCES ............................................. 31

7.

SUMMARY

OF CHANGES ................................... 33 ATTACHMENTS ANT) FORMS Attachment 1, "Initial System Alignment Check" ................... 35 Attachment 2, "Gas Activity Worksheet" .......................... 36 Attachment 3, "C3SSP-SAS2 Septum Replacement" .................. 37 Attachment 4, "Containment Air PASS Simplified Drawing". .......... 38 CP 3804L-OO1,"PASS Containment Air Sample Data" CP 3804L-OO2,"PASS Containment Air Sample Restoration Lineup" Level of Use CP 3804L Continuous STOP THINK ACT REVIEW Rev. 003

1. PURPOSE 1.1 Objective Provide instructions for operation of the Unit 3 containment air post accident sample system for containment air sample acquisition when high i radioactivity levels, may preclude the normal (conventional) sampling method.

This procedure satisfies regulatory commitment B 18443-01 to maintain contingency plans for obtaining and analyzing highly radioactive samples of the containment atmosphere.

This procedure was developed using the reactor technical manual for the containment air PASS (Ref.6.2) and other documents identified herein. I 1.2 Discussion If conditions arise that will not allow Sections 4.1 through 4.4 to be completed, the procedure user will be directed to Section 4.8, "Restoration from PASS Sample Acquisition," to return the system to normal.

Attachment 4 contains a simplified drawing of the containment air post accident sample system. I i

1.3 Applicability This procedure is applicable when in-plant radioactivity levels are too i high to permit containment air sampling via the normal (conventional) -@

method.

1.4 Frequency As required during periods of elevated in-plant levels. E

2. PREREOUISITES 2.1 General

/ 2.1.1 Heat tracing panel 3HTS-PNLA3 (OP 3352) has been energized for at least 1/2 hour.

/ 2.1.2 To prevent condensation and iodine plate-out in the sample lines, verify containme~nt temperature is less than or equal to 1'70° E Level of Use CP 3804L Continuous STOP THINK ACT REVIEW Rlev. 003 2 of 38

2.1.3 Key has been obtained to unlock the following:

Train A Train B 3SSP*V51 3SSP*V52 3SSP*V59 3SSP*V60 3HCS*V2 3HCS*V9 3HCS*V3 3HCS*V10 3HCS*V6 3HCS*V13 2.1.4 Health Physics has been notified that a containment air PASS sample will be taken.

2.1.5 Health Physics has evaluated need for RWP.

2.1.6 Lab ventilation is operating.

2.1.7 Lead brick shielding has been placed in lab ventilation hood.

2.1.8 Computer radioisotopic analysis system in operation and calibrated.

2.1.9 Gas chromatograph has been set up and calibrated, or calibration has been initiated for PASS containment air sample analysis if desired.

2.1.10 Proper operation of sample syringes in PASS suitcase has been verified.

Lee/fU 2.1.11 13 cc gas vial has been stoppered and evacuated.

Cotna/ *0 2.1.12 One train of SLCRS in operation.

CP 3804L ACT REVIEW Rev. 003 STOP THINK 3 of 38

2.1.13 Manager of Radiological Dose Assessment (MRDA) or the Assistant Manager of Radiological Dose Assessment (AMRDA) has requested a containment air sample to include the following:

Check Reouested Analysis Samnle Eauioment Needed

-- -- i-- I I

[]Gas isotopic "GAS ISOTOPIC" syringe, stoppered and evacuated 13 cc gas vial *0 EI] Gas composition "GAS COMP" syringe Check Sample Point I] Hydrogen Recombiner Train A

[] Hydrogen Recombiner Train B 2.1.14 Containment Air PASS Team has completed pre-job brief as follows:

Manager of Operational Support Center (MOSC) -

designates, assembles, and briefs the Containment Air PASS Team for implementation of this procedure o Operational Support Center Assistant Radiological Protection Supervisor (OSC ARPS) with the concurrence of the Manager of Radiological Consequence Assessment (MRCA) - specifies the radiological controls required for implementation of this procedure 2.2 Documents 2.2.1 C CP 803.12, "Operation and Calibration of the Varian CP-4900 Micro - GC" 2.2.2 C CP 803.6, "Gamma Spectroscopy Counting System Maintenance and Operation" 0 2.2.3 CP 3804K Attachment, "PASS Sample Equipment Inventory" 2.2.4 PI-AA- 200, "Corrective Action" 2.2.5 WM-AA- 100, "Work Management" 2.2.6 RWIP for PASS sample collection.

2.2.7 Gas sample isotopic printout Level of Use I CP 3804L ContinuousI STOP THINK ACT REVIEW Rev. 003 4 of 38

2.3 Personnel 2.3.1 Assistant Director, Technical Support (ADTS) 2.3.2 Manager of Radiological Dose Assessment (MRDA) or Assistant Manager of Radiological Dose Assessment (AMRDA) 2.3.3 Manager of Operational Support Center (MOSC) 2.3.4 Operational Support Center Assistant Radiological Protection Supervisor (OSC ARPS) 2.3.5 Manager of Control Room Operations (MCRO) 2.3.6 Manager of Radiological Consequence Assessment (MRCA) 2.3.7 Containment Air PASS Team consisting of the following personnel:

At least two Chemistry Technicians

At least one Health Physics Technician Level of Use ,, CP 3804L Continuous STOP THINK ACT, REVIEW Rev. 003 5 of 38

2.4 Tools and Consumables 2.4.1 Located in Unit 3 Chemistry Lab

13 cc gas vial

13 cc gas vial stopper

24 Lead bricks

PASS transport cart o, Syringe transfer container

250 rtl syringe labeled "GAS ISOTOPIC"

2.0 ml syringe labeled "GAS COMP"

Key to 3SSP-PNL2 (Issued to U3 Chemistry personnel)

Key to the following valves: I Train A Train B 3SSP*V51 3SSP*V52 3SSP*V59 3SSP*V60 3HCS*V2 3HCS*V9 3HCS*V3 3HCS*V10 3HCS*V6 3HCS*V13

Watch 2.4.2 Located in PASS Cabinet in 112 Recombiner Building I

Spare syringe needles

3SSP-SAS2 septums

1/2" Socket wrench

Phone headset

Scribe

Tweezers

Septum insertion tool

Calculator

Damper operating tool

Flat-tipped screwdriver I

Valve wrench I 2.5 Responsibilities 2.5.1 The ADTS shall make the decision to obtain a sample using PASS.

2.5.2 The Manager of Operational Support Center designates, assembles and briefs the PASS team.

ILevel of Use [ "CP 3804L ContinuousI STOP THINK ACT REVIEW' Rev. 003

.. """* 6 of 38

2.5.3 The Manager of Radiological Consequence Assessment specifies PASS team radiological controls.

2.5.4 The Operational Support Center Assistant Radiological Protection Supervisor assigns HIP technicians and briefs the PASS team on radiological conditions.

2.5.5 The Manager of Radiological Dose Assessment or the Assistant Manager of Radiological Dose Assessment specify PASS team sampling and analysis requirements.

2.6 Definitions 2.6.1 SLCRS - supplementary leak collection and release system 2.6.2 CR - Condition Report

3. PRECAUTIONS 3.1 The inside of 3SSP-SAS2, containment air sample module, is potentially contaminated. Proper Health Physics practices and RWP requirements must be followed to prevent the spread of contamination.

3.2 Nitrogen pressures > 100 psig can damage the tubing in 3SSP-PNL2.

CP 3804L Level of Use Continuous ACT REVIEW Rev. 003 STOP THINK 7 of 38

4. INSTRUCTIONS 4.1 Preparation for PASS Sample Acquisition 4.1.1 PERFORM the following and INITIAL CP 3804L-001:

ENSURE "General Prerequisites" have been completed

REVIEW Section 3, "Precautions"

____4.1.2 IF during performance of Sections 4.1 through 4.8 any operational problems are encountered, RECORD noted problems on CP 3804L- 001.

_____4.1.3 IF during performance of Sections 4.1 through 4.4, operational problems are encountered that will not allow sampling to be completed, Go To Section 4.8, "Restoration from PASS Sample Acquisition."

_____4.1.4 PROCEED to containment air sample module with the following:

Stoppered and evacuated 14.4 cc gas vial

Key to 3SSP-PNL2 (Issued to U3 Chemistry personnel)

Key to the following valves:

Train A Train B 3SSP*V51 3SSP*V52 3SSP*V59 3SSP*VC0 3HCS*V2 3HCS*V9 3HCS*V3 3HCS*V10 3HCS*V6 3HCS*V13

Watch

CP 3804L-001 and CP 3804L-002

Syringe transfer container

___4.1.5 UNLOCK 3SSP-PNL2, containment air sample remote panel.

_____4.1.6 Refer To Attachment 1 and CHECK system alignment.

Level of Use cP 3804L Continuous STOP THINK ACT REVIEW Rev. 003

4.1.7 NOTIFY MCRO of the following:

a. 3HVR*DMP60 will be opened

b. IF in operating Modes 1-4, Enter LCO 3.6.6.2 for 3HVR*DMP60 [Ref. 6.1]

c. PERFORM one of the following:

1) IF hydrogen recombiner train A was selected in step 2.1.13, NOTIFY MCRO that the following valves will be opened if not already open:

3HCS*V2, recombiner lA supply outer isolation

3HCS*V3, recombiner lA supply inner isolation

3HCS*V6, recombiner RBNR- 1A return isolation

2) IF hydrogen recombiner train B was selected in step 2.1.13, NOTIFY MCRO that the following valves will be opened if not already open:

3HCS*V9, recombiner lB supply outer isolation

3HCS*V1O, recombiner 1B supply inner isolation

3HCS*V13, recombiner RBNR-1lB return isolation

d. IF in operating Modes 1-4, Track Tech Spec surveillance requirements of 4.6.1.1.a for the valves opened in step 4.1.7 c.

NOTE Constant commnunications with the control room are required when 3HCS*V2, 3HCS*V3, 3HCS*V6, 3HCS*V9, 3HCS*V10, or 3HCS*V13 are opened in Modes 1-4.

___4.1.8 IF in operating Modes 1-4, DON phone headset and ESTABLISH communications with Control Room.

CP 3804L Level of Use Continuous STOP THINK ACT REVIEW Rev. 003 9 of 38

I O

4.1.9 PERFORM the following:

a. Using damper operating tool, OPEN 3HVR*DMP60, 3SSP- SAS1/SAS2 exhaust isolation damper [Ref. 6.1]

b. OPEN 3HVR-DMP1301, 3SSP-SAS2 exhaust damper

[Ref. 6.1].

4.1.10 PERFORM the following at 3SSP-PNL2, containment air sample remote panel:

a. ZERO timer.

b. PUSH and HOLD "POWER ON" button for 1 to 2 seconds to energize remote operating module and RECORD time:

NOTE I

A lit fuse indicator light indicates the fuse is blown.

____c. CHECK line fuses and blower fuse indicator lights are not lit.

___d. OPEN 3SSP-V53, nitrogen supply to containment air sample PNL2.

NOTE 3SSP-PCV82 may require periodic adjustment to maintain 45.-50 psig outlet pressure.

Nitrogen pressures > 100 psig can damage the tubing in 3SSP-PNL2.

e. ADJUST 3SSP-PCV82, nitrogen pressure regulator, to 45-50 psig.

CP 3804L Level Continuousof Use STOP THINK ACT REVIEW Rev. 003 10 of 38

~ALARA The inside of 3SSP-SAS2, containment air sample module, is potentially contaminated. Proper Health Physics practices and RWP requirements must be followed to prevent the spread of contamination.

At 3SSP-SAS2, containment air sample module, CHECK I

____4.1.11 exhaust fan is running.

4.1.12 IF exhaust fan is not running, PERFORM the following at 3SSP-PNL2, containment air sample remote panel:

____a. PUSH "POWER ON" button to de-energize panel.

____b. PUSH and HOLD "POWER ON" button for 1 to 2 seconds to energize remote operating module and RECORD time:

____c. At 3SSP-SAS2, containment air sample module, CHECK exhaust fan is running.

____d. IF exhaust fan is not running, NOTIFY MOSC.

Level of Use I CP 3804L ContinuousI STOP THINK ACT REVIEW Rev. 003 11 of 38

I .

NOTE If hydrogen recombiner train A is running, the following valves will already be open:

3HCS*V2, recombiner 1A supply outer isolation

3HCS*V3, recombiner 1A supply inner isolation

3HCS*V6, recombiner RBNR- lA return isolation N/ CAUTION V It is imperative unless not to pushisinobtained.

SM/US permission on the hand

-Thiswheel when engages theoperating the following clutch override valves and could result in damage to the valve.

Train A Train B 3HCS*V2 3HCS*V6 3SSP*V59 3HCS*V9 3FHCS*V13 3SSP*V60 3IICS*V3 3SSP*V51 3HCS*V10 3SSP*V52 4.1.13 IF hydrogen recombiner train Awas selected in step 2.1.13, UNLOCK and OPEN the following valves:

3HCS*V2, recombiner lA supply outer isolation

3HCS*V3, recombiner 1A supply inner isolation

3HCS*V6, recombiner RBNR- lA return isolation

3SSP*V51, containment air sample return cross-connect

3SSP*V59, containment air sample supply cross-connect CP 3804L Level of Use Continuous STOP THINK ACT REVI EW Rev. 003 12 of 38

V CAUTION It is imperative not to push in on the hand wheel when operating the following valves unless SM/US permission is obtained. This engages the clutch override and could result in damage to the valve.

Train A Train B 3HCS*V2 3HCS*V6 3SSP*V59 3HCS*V9 3HCS*V13 3SSP*V60 3HCS*V3 3SSP*V51 3HCS*V10 3SSP*V52 NOTE If hydrogen recombiner train B is running, the following valves will already be open:

31{CS*V9, recombiner lB supply outer isolation

3HCS*V10, recombiner lB supply inner isolation

311CS*V13, recombiner RBNR-1B return isolation 4.1.14 IF hydrogen recombiner train B was selected in step 2.1.13, UNLOCK and OPEN the following valves:

3HCS*V9, recombiner lB supply outer isolation

____ 3I-CS*V10, recombiner lB supply inner isolation

___

3HCS*V13, recombiner RBNIR-1B return isolation

3SSP*V52, containment air sample return cross-connect

3SSP*V60, containment air sample supply cross-connect 4.1.15 At 3SSP-PNL2, containment air sample remote panel, POSITION the following valves as indicated:

___a. 3SSP-V2037 to "OPEN."

____ b. 3SSP-V2035 to "SAMPLE."

c. 3SSP-V112 to "01FF."

d. 3SSP-V2034 to "OFF."

Level of Use CP 3804L Continuous[ STOP THINK ACT REVIEW Rev. 003 13 of 38

hAALARA 3SSP-PNL2, containment air sample remote panel, requires a 15 minute warm-up period. The time that the instrument was energized is recorded on Chem Form 3804L- 1. The PASS Team Health Physics Technician will determine the best location to wait for the completion of the warm-up.

___4.1.16 REQUEST Health Physics Technician determine most appropriate location to wait for completion of 15 minute warm-up of 3SSP-PNL2, containment air sample remote panel.

- End of Section 4.1 -

Level of Use I CP 3804L ContinuousI STOP THINK ACT REVIEW Rev. 003 14 of 38

4.2 Sample Acquisition

____4.2.1 Refer To step 4.1.10 b. or step 4.1.12 b. and ENSURE 15 minute warm-up of 3SSP-PNL2, containment air sample remote panel, is complete.

____4.2.2 Refer To CF 3804L- 001 and MARK box corresponding to hydrogen recombiner train being sampled.

____4.2.3 At 3SSP-PNL2, containment air sample remote panel, POSITION 3SSP-V112 to "SAMPLE INFLUENT."

4.2.4 At 3SSP*PNL3, post accident sample panel, PERFORM the following:

___a. ROTATE 'AIlR SAMPLE PUMP P4 SPEED CONTROL' knob fully clockwise.

____b. PUSH 'A*IR SAMPLE PUMP P4" start button to start 3SSP-P4

____ ~4.2.5 RECORD time purge started: _____

____4.2.6 At 3SSP-PNL2, containment air sample remote panel, RECORD flow rate: pm l_____

____4.2.7 PERFORM the following calculation to determine purge time in minutes.

Purge time =220 / purge flow rate in 1pm Purge time = 220 / =______minutes l_____pm 4.2.8 WHEN purge time has passed, ISOLATE sample as follows:

____a. At 3SSP*PNL3, post accident sample panel, ADJUST 3SSP-P4 speed control to achieve a sample flow rate of 10 to 121lpm indicated on 3SSP-PNL2, containment air sample remote panel.

____b. At 3SSP-PNL2, containment air sample remote panel, RECORD flow rate: _____pm

____c. POSITION 3SSP-V2037 to "CLOSE."

Level of Use cF 3804L Continuous STOP THINK ACT REVIEW Rev. 003 15 of 38

d. CHECK that flow rate is less than value recorded in step 4.2.8 b.

e. WAIT 1 minute.

f. POSITION 3SSP-V2035 to "BYPASS AND FLUSH."

g. Refer To CF 3804L-001 and RECORD sample date and time.

h. POSITION 3SSP-V112 to "OFF."

4.2.9 At 3SSP*PNL3, post accident sample panel, PUSH "AIR SAMPLE PUMP P4" stop button to stop 3SSP-P4.

- End of Section 4.2 -

Level of Use CF 3804L ACT REVIEW Rev. 003 ContinuousI STOP THINK 16 of 38

4.3 System Flush Prior To Sample Retrieval 4.3.1 At 3SSP-PNL2, containment air sample remote panel, INITIATE nitrogen purge as follows:

a. POSITION the following valves as indicated:

1) 35SFP-V112 to "NITROGEN FLUSH."

2) 3SSP-V2037 to "OPEN."

3) 3SSP-V2034 to "CON."

___b. RECORD flow rate: pm l____

_____c. WAIT 3 minutes.

______d. POSITION 3SSP-V2037 to "CLOSE."

______e. CHECK that flow rate is less than value recorded in step 4.3.1 b.

_____f. WAIT 3 minutes.

g. POSITION the following valves as indicated:

1) 3SSP-V2034 to "OFF."

2) 3SSP-V112 to "OFF."

3) 3SSP-V2037 to "OPEN."

lHealth /* 4.3.2 Based on radiation reading in sample module room, DIRECT Tehnsician Chemistry Technicians to perform one of the foloig

____ Go To step 4.3.1 and REPEAT flush

Go To Section 4.4 and retrieve samples

- End of Section 4.3 -

CP 3804L ILevel Continuous of Use ACT REVIEW Rev. 003 STOP THINK 17 of 38

4.4 Retrieval of Containment Air Samples 4.4.1 At 3SSP-SAS2, containment air sample module, OPEN cabinet door.

4.4.2 IF gas isotopic sample was requested in step 2.1.13, PERFORM the following:

a. ENSURE needle is screwed fully into 250 [1 syringe labeled "GAS ISOTOPIC."

NOTE I 3ssP-v2036 is open when handle is inline with needle guide.

b. OPEN 3SSP-V2036, containment air sample module internal bypass valve.

c. INSERT syringe into needle guide until syringe nut is engaged.

~ALARA

1. Do not unscrew syringe body more than 2 turns counterclockwise.

Excessive turns will disengage needle from syringe.

2. Steps 4.4.2 d. through g. should be performed rapidly to minimize exposure.

d. Rapidly DRAW 250 *1 gas sample into syringe and TURN syringe body 2 turns counterclockwise to lock sample in syringe.

e. REMOVE syringe from needle guide and INSERT needle into stoppered 13 cc gas vial.

E0

f. HOLD syringe tip and TURN syringe body 2 turns clockwise to unlock syringe and INJECT contents of syringe into stoppered 13 cc gas vial.

E0

g. PLACE syringe and gas vial into syringe transfer container and PLACE lid on syringe transfer container.

Level of Use [ CP 3804L Continuous STOP THINK ACT REVIEW Rev. 003 18 of 38

____h. CLOSE 3SSP-V2036, containment air sample module internal bypass valve.

4.4.3 lI__gas composition sample was requested in step 2.1.13, PERFORM the following:

____a. ENSURE needle is screwed fully into 2.0 ml syringe labeled "GAS COMP."

___b. OPEN 3SSP-V2036, containment air sample module internal bypass valve.

____c. INSERT syringe into needle guide until syringe nut is engaged.

1. Do not unscrew syringe body more than 2 turns counterclockwise.

Excessive turns will disengage needle from syringe.

2. Steps 4.4.3 d. and e. should be performed rapidly to minimize exposure.

d. Rapidly DRAW 1 cc gas sample into syringe and TURN syringe body 2 turns counterclockwise to lock sample in syringe.

e. REMOVE syringe from needle guide and PLACE syringe into syringe transfer container and PLACE lid on syringe transfer container.

f. CLOSE 3SSP-V2036, Containment air sample module internal bypass valve.

4.4.4 CLOSE cabinet door.

Level of Use I CP 3804L ACT REVIEW Rev. 003 ContinuousI STOP THINK 19 of 38

NOTE If sufficient personnel are available, Sections 4.5 and 4.8 may be performed simultaneously.

4.4.5 WHEN all samples requested in step 2.1.13 have been retrieved, PERFORM the following:

___ *TRANSPORT samples to laboratory and Go To Section 4.5, "cSample Analysis"

___ Go To Section 4.8, "Restoration from PASS Sample Acquisition"

- End of Section 4.4 -

CP 3804L Level of Use Continuous STOP THINK ACT REVIEW Rev. 003 20 of 38

4.5 Sample Analysis 4.5.1 DETERMINE handling requirements as follows:

Physics Health 1 Technician

a. OPEN transport container cover and MEASURE dose rate.

b. IF dose rate is greater than or equal to 1 rem/hr, NOTIFY OSC ARIPS and REQUEST instructions for handling.

c. IF dose rate is less than 1 rem/hr, DIRECT Chemistry Technicians to handle samples as normal radioactive samples and to minimize radiation exposure when performing required analyses.

4.5.2 PERFORM PASS sample analysis as follows:

Chemistry Technician

Refer To the following Sections as applicable and PERFORM analysis:

Section 4.6, "Gas Isotopic Analysis"

Section 4.7, "Gas Composition Analysis" 4.5.3 WHEN analyses are complete, REPORT results to MRDA or AMRDA.

4.5.4 Refer To CP 3804L-O01 and SIGN and DATE "Performed By" section.

4.5.5 IFI copies of results are requested, FAX or SEND copies of the following to requesting individuals:

Attachment 2

CP 3804L-001 4.5.6 IF Section 4.8, "Restoration from PASS Sample Acquisition," has not been completed, Go To Section 4.8 and COMPLETE PASS system restoration.

- End of Section 4.5 -

Level of Use I CP 3804L ACT REVIEW Rev. 003 Continuous STOP THINK 21 of 38

4.6 Gas Isotopic Analysis

_____4.6.1 PLACE 2.5 cm shelf in detector to be used for gas isotopic analysis.

4.6.2 DETERMINE gas isotopic activity as follows:

______a. Using the following information, Refer To C CP 803.6, "Gamma Spectroscopy Counting System Maintenance and Operation," and ANALYZE sample:

Open cave

Applicable geometry for shelf being used

Five minute count time

General library

Sample volume of 0.250 cc

Sample date and time as recorded on CP 3804L-001

b. IF dead time is greater than or equal to 20%, PERFORM the following:

1) ABORT count.

2) REPLACE shelf with next higher shelf.

3) Go To step 4.6.2.

______c. STORE gas vial in shielded location.

SLevel of Use CP 3804L Continuous STOP THINK ACT REVIEW Rev. 003 22 of 38

d. DETERMINE background as follows:

1) Using the following information, Refer To C CP 803.6, "Gamma Spectroscopy Counting System Maintenance and Operation," and PERFORM background count on detector that was used for gas isotopic analysis. L

Open cave

Applicable geometry for shelf that was used

Five minute count time

General library

Sample volume of 0.250 cc

2) RECORD all identified isotopes and their associated background activity levels in p.Ci/cc on Attachment 2.

e. Refer To Attachment 2 and CALCULATE gas activity as follows:

1) Refer To gas isotopic printout and RECORD all identified isotopes and their associated activity levels in itCi/cc.

2) For each isotope listed, SUBTRACT background activity from printout activity and RECORD as isotope activity in

tCi/cc.

3) ADD isotope activities and RECORD as gas activity in

tCi/cc.

4) Refer To CP 3804L- 001 and RECORD gas activity in ptCi/cc in "Sample Data" table.

4.6.3 PLACE empty "GAS ISOTOPIC" syringe in shielded location.

- End of Section 4.6 -

Level of Use I CP 3804L ContinuousI STOP THINK ACT REVIEW Rev. 003 23 of 38

I . .

4.7 Gas Composition Analysis NOTE The "GAS COMP" results are for information only and are not used in any sample calculations.

Refer To C CP 803.12, "Operation and Calibration of the Varian I

___4.7.1 CP-4900 Micro-GC," and ANALYZE 2.0 ml syringe labeled "GAS COMP" for the following:

% hydrogen

% oxygen

% nitrogen

___4.7.2 PLACE empty "GAS COMP" syringe in shielded location.

___4.7.3 WHEN analysis is complete, Refer To CF 3804L-001 and RECORD gas composition results in % in "Sample Data" table.

- End of Section 4.7 -

Level of Use I CP 3804L ContinuousI STOP THINK ACT REVIEW Rev. 003 24 of 38

I -

4.8 Restoration from PASS Sample Acquisition NOTE Entry into Section 4.8 may occur at any time during performance of Sections 4.1 through 4.4. Some steps in Section 4.8 may already be completed depending on the entry point.

4.8.1 IF sample flow was achieved at any time during PASS sample, FLUSH PASS system as follows:

______a. IF Section 4.3, "System Flush," has not been performed, PERFORM Section 4.3.

______b. At 3SSP-PNL2, containment air sample remote panel, POSITION 3SSP-V2035 to "SAMPLE."

c. INITIATE nitrogen purge as follows:

1) POSITION 3SSP-V112 to "NITROGEN FLUSH."

2) POSITION 3SSP-V2037 to "OPEN."

3) POSITION 3SSP-V2034 to "ON."

___d. RECORD flow rate: pm l____

_____e. WAIT 3 minutes.

______f. POSITION 3SSP-V2037 to "CLOSE."

______g. ChECK that flow rate is less than value recorded in step 4.8.1 d.

_____h. WAIT 3 minutes.

4.8.2 POSITION the following valves as indicated:

_____a. 3SSP-V2034 to "OFF."

______b. 3SSP-V112 to "OFF"

______c. 3SSP-V2037 to "OPEN."

lLevel of Use CP 3804L Continuous STOP THINK ACT REVIEW Rev. 003

25 of 38

4.8.3 Refer To CP 3804L-002 and ENSURE or INITIAL valve lineup for valves at 3SSP-PNL2.

4.8.4 CLOSE 3SSP-V53, nitrogen supply to containment air sample PNL2.

4.8.5 PUSH "POWER ON" button to de-energize panel.

4.8.6 CLOSE and LOCK panel door.

4.8.7 PERFORM the following:

a. CLOSE 3HVR-DMP1301, 3SSP-SAS2 exhaust damper

[Ref. 6.1].

b. Using damper operating tool, CLOSE 3HVR*DMP60, 3SSP-SAS1/SAS2 exhaust isolation damper [Ref. 6.1]

Level of Use CP 3804L Continuous STOP THINK ACT REVIEW Rev. 003 26 of 38

V CAUTION It is imperative not to push in on the hand wheel when operating the following valves unless SM/US permission is obtained. This engages the clutch override and could result in damage to the valve.

Train A Train B 3H{CS*V2 3HCS*V6 3SSP*V59 3HCS*V9 3HCS*V13 3SSP*V60 3H{CS *V3 3SSP *V51 3HCS *V10j 3SSP*V52

c. IF hydrogen recombiner train A was Selected in step 2.1.13, PERFORM the following:

1) CLOSE and LOCK the following valves

3SSP*V51, containment air sample return cross- connect

3SSP*V59, containment air sample supply cross - connect

2) IFF train A hydrogen recombiner is not running, CLOSE and LOCK the following valves:

I

3HCS*V2, recombiner 1A supply outer isolation

3HCS*V3, recombiner 1A supply inner isolation

3HCS*V6, recombiner RBNR-1lA return isolation CP 3804L Level of Use Continuous STOP THINK ACT REVIEW Rev. 003 27 of 38

NY CAUTION NY It is imperative not to push in on the hand wheel when operating the following valves unless SM/US permission is obtained. This engages the clutch override and could result in damage to the valve.

Train A Train B 3HCS*V2 3HCS*V6 3SSP*V59 3HCS*V9 3HCS*V13 3SSP*V60 3HCS*V3 3SSP*V51 3HCS*V10 3SSP*V52

d. liP hydrogen recombiner train B was selected in Step 2.1.13, PERFORM the following:

1) CLOSE and LOCK the following valves

3SSP*V52, containment air sample return cross - connect

___ 3SSP*V60, containment air sample supply cross -connect

2) IF train B hydrogen recombiner is not running, CLOSE and LOCK the following valves:

I

___ 3HCS*V9, recombiner lB supply outer isolation

___ 3HCS*V1O, recombiner lB supply inner isolation

3HCS*V13, recombiner RBNR- lB return isolation

___4.8.8 Refer To CP 3804L- 002 and ENSURE remainder of valve lineup.

4.8.9 Refer To CP 3804L- 002 and PERFORM. independent verification of system lineup.

CP 3804L Level Continuous of Use ACT REVIEW Rev. 003 STOP THINK 28 of 38

NOTE When this step is completed, constant communications with the control room in Modes 1-4 is no longer required.

______4.8.10 NOTIFY MCRO of the following:

IF closed in step 4.8.7 c.2), the following valves are closed I and locked:

3HCS*V2, recombiner lA supply outer isolation,

3HCS*V3, recombiner 1A supply inner isolation

3HCS*V6, recombiner RBNR- lA return isolation

IF closed in step 4.8.7 d.2), the following valves are closed l and locked: I

3HCS*V9, recombiner lB supply outer isolation

3HCS*V10, recombiner lB supply inner isolation

3HCS*V13, recombiner RBNR-1B return isolation IF in operating Modes 1-4, NOTIFY MCRO that tracking requirements of Tech Spec surveillance 4.6.1.1.a are no longer required for valves that were reported closed and 3HVR*DMPC0 is closed I

IF in operating Modes 1-4, REQUEST MCRO exit LCO 3.6.6.2 for 3HVR*DMPC0 [Ref. 6.1].

PASS system is secured.

IF in operating Modes 1-4, REQUEST permission to secure constant communications with control room

______4.8.11 RETURN valve key.

______4.8.12 SUBMIT completed CP 3804L-002 to Chemistry Supervision for review.

SLevel of Use CP 3804L Continuous STOP THINK ACT REVIEW Rev. 003 29 of 38

4.8.13 IF operational difficulties were encountered, PERFORM one or both of the following:

Refer To WM-AA- 100, "Work Management" and INMTIATE Condition Report for applicable equipment and RECORD CR number on CP 3804L-001

____ *Refer To PI-AA-200, "Corrective Action," and INITIATE CR and RECORD CR number on CP 3804L-001 0

____4.8.14 RECORD number of needle punctures for the containment air septum in PASS log.

Step 4.8.15 may not be performed due to the radiation levels in the hydrogen recombiner building.

4.8.15 OBTAIN permission from MOSC and PERFORM the following:

IFF containment air septum has been punctured 10 times or more since its last replacement, Refer To Attachment 3 and REPLACE septum

____

Refer To CP 3804K Attachment, "PASS Sample Equipment Inventory," and INVENTORY PASS sampling equipment and LOCK PASS cabinet door handle

___4.8.16 SIGN and DATE "Performed By" block on CP 3804L-001.

4.8.17 SUBMIT the following completed documents to Chemistry Supervision.

___ CP 3804L-001

____ CP 3804K Attachment, "PASS Sample Equipment Inventory" 4.8.18 SUBMIT copy of reviewed CP 3804L- 001 and applicable CR's to Chemistry Supervision system engineer.

- End of Section 4.8 -

Level of Use I CP 3804L ContinuousI STOP THINK ACT REVIEW Rev. 003 30 of 38

5. REVIEW ANDJT SIGNOFF 5.1 The review and signoff for this procedure is located in the following attachments and forms:

Attachment 2

Attachment 3

CP 3804L-001

CP 3804L-002

6. REFERENCES 6.1 PIR 3-93-021, "SLCRS Boundary Breach" 6.2 Technical Manual for Containment Air Post Accident Sample System,"

General Dynamics Corporation, Electric Boat Division, Reactor Plant Services 6.3 Installation, Operating, and Maintenance Instructions Model MB- 151 Post Accident Air Sample Compressor 6.4 Regulatory Guide 1.97 6.5 Post Accident Sample System Component Instruction Literature 6.6 IINPO Good Practice CT-707, "cPost-Accident Sampling Preparedness" 6.7 NUJREG 0737 6.8 Millstone DWG. No 12179-EM-155A 6.9 Millstone DWG. No 12179-EM-li5A 6.10 Millstone DWG. No 12179-CP-402001 6.11 Millstone DWG. No 12179-CP-402002 6.12 Millstone DWG. No 12179-CP-402003 6.13 Millstone DWG. No 12179-CP-402004 6.14 Millstone DWG. No 12179-CP-402006 Level of Use cP 3804L Continuous STOP THINK ACT REVIEW Rev. 003 31 of 38

6.15 Millstone D~WG. No 12179-CP-402009 6.16 Millstone DWG. No 12179-CP-4020014 6.17 Millstone DWG. No 12179-CP-4020015 6.18 Millstone DWG. No 12179-CP-4020053 6.19 Millstone DWG. No 12179-CP-4020054 6.20 Millstone DWG. No 12179- CP-4020056 6.21 Millstone DWG. No 12179-CP-402700 6.22 Correspondence B11121, "Millstone Nuclear Power Station, Unit No. 3, Response to Chemical Engineering Branch DSER Open Item," dated April 9, 1984, from Northeast Utilities to the NRC 6.23 Correspondence Bl11177, "Millstone Nuclear Power Station, Unit No. 3, Response to Chemical Engineering Branch DSER Open Item," dated May 10, 1984, from Northeast Utilities to the NRC 6.24 NUJREG-1031, "Safety Evaluation report related to the operation of Millstone Nuclear Power Station, Unit No. 3," dated August 2, 1984.

6.25 DCR M3-98034, "cSetpoint Change to 3GSN-PCV106, 3SSP-PCV80, and 3SSP-PCV82" 6.26 DCN DM3-00-0638-98, "Setpoint Change to 3GSN-PCV1O6, 3SSP-PCV80, and 3SSP-PCV82" 6.27 Engineering Calculation 3SSP -01632-I-3 II 6.28 NRC, B18443 Dated July 31, 2001.

CP 3804L Level of Use ACT REVIEW Rev. 003 Continuous STOP THINK 32 of 38

7.

SUMMARY

OF CHANGES Summary of Changes Rev. 003 7.1 Performed the following Administrative Corrections to update references:

RP 16 replaced by WM-AA- 100

CP 2803/3803P replaced by C CP 803.12 7.2 Changed instances of VERIFY to CHECK or ENSURE as applicable, no revision bars used.

Summary of Changes Rev. 002-02 7.3 Added prerequisite for the verification of containment temperature being at or below 170° F.

7.4 Removed Note statement on cover page that required document to be reviewed by Nuclear Fuels Safety Analysis.

7.5 Removed references to Technical Specifications and E-Plan in Objective Section and added regulatory commitment B18443-01.

7.6 Removed references to SERO and SERO activation throughout the document.

7.7 Changed volume of gas vial from 14.4 cc to 13 cc.

7.8 Updated Documents Section and references to su~perseded and cancelled documents throughout.

Summary of Changes Rev. 002-01 7.9 Editorial Correction; Added Reference 6.28 NRC commitment letter.

B18443. AIR #01005693-01.

Summary of Changes Rev. 002-00 7.10 Added simplified drawing of containment air PASS system.

7.11 Added flat-tipped screwdriver and valve wrench to tools and consumables.

7.12 Deleted "(Obtained from MCRO)" from valve key description.

7.13 Changed basis for 45-50 psig on 3SSP-PCV82 to Engineering Calculation 3SSP-01632-I-3.

Level of Use cP 3804L Continuous STOP THINK ACT REVIEW Rev. 003 33 of 38

7.14 Added caution associated with remotely operated valves that have clutches.

7.15 Added numerous signoffs to substeps.

7.16 Added initial system alignment check and deleted associated steps in body of procedure.

7.17 Deleted step to remove counting shelf when counting background.

7.18 Changed steps to allow hydrogen recombiner isolations to remain open if hydrogen recombiner is running.

7.19 Added steps to generate TR and/or CR when operational difficulties are encountered.

7.20 Added bullet to request permission from SM/US prior to securing constant communications.

7.21 Added requirement to obtain permission from MOSC to changeout septum and inventory PASS equipment. Added alara above step.

7.22 Changed septum changeout frequency to every 10 punctures.

7.23 Added containment air equipment to CP 3804K (Att), "PASS Sample Equipment Inventory," and deleted inventory list from this procedure.

Added requirement to lock PASS cabinet door handle when inventory is completed.

7.24 Added step to submit PASS inventory to Chemistry Supervision.

7.25 Added step to submit copy of reviewed chemistry form CP 3804L- 001 and applicable CR's to system engineer.

7.26 A note was added to the cover page of this procedure to ensure a review is performed by the Radiological Engineering Services whenever modifications to this procedure are made that may impact dose limit time and motion study calculations. This is in response to AR 99005798-06.

Level of Use CP 3804L ContinuousI STOP THINK ACT REVIEW R~ev. 003 34 of 38

Attachment 1 Initial System Alignment Check (Sheet 1 of 1)

Component ID Description I Performed PoiinInitial Date 3SSP- PNL2 3SSP-V2027 Containment air remote module N2 supply OP

,isolation valve 3SSP-V2029 Containment air remote module N2 stor- CL age tank isolation valve 13SSP-V2030 IContainment air remote module N2 stor- CL age tank vent valve 3SSP- PCV82 Nitrogen pressure regulator Backed Off

~Observe caution sign at 3SSP-.V46 3SSP-V46 Air sample pump P4 inlet isolation valve OPI Post Accident Sample Module Room 3SSP-V2036 Containment air sample module internal CL Ibypass valve 3SSP-V1 88 3-way divert valve to iodine filter FLT1 BYP 3SSP-V1 89 Iodine filter FLT1 outlet isolation valve CL 3P-11iodine filter FLT1 inlet isolation valve CL Level of Use CP 3804L ACT REVIEW Rev. 003 Continuous STOP THINK 35 of 38

Attachment 2 Containment Air Gas Activity Worksheet (Sheet 1 of 1)

PrintoutActivity - Background = Isotope Activity Isotope Printout Activity Background Isotope Activity (2- place accuracy) (2- place accuracy)

(pCilcc) (pCi/cc) (pCi/cc)

______ I ______ i ______ I ______

4 -I I 4 4 1 4 4 1 NOTE: Gas Activity summation of Gas Activity (2-place accuracy) (pCi/cc) all isotope activities.

Prepared by:__________ Date:

SUBMIT completed attachment to Chemistry Supervision.

Level of Use I CP 3804L ContinuousI ACT REVIEW Rev. 003 STOP THINK 36 of 38

Attachment 3 3SSP- SAS2 Septum Replacement (Sheet 1 of 1)

I NOTE The required tools and consumables can be found in the PASS cabinet located in the H2 recombiner building.

DON protective clothing as directed by Health Physics.

______2. Using 1/2" socket, UNSCREW and REMOVE needle guide.

______3. IF old septum did not come out with septum holder, REMOVE old septum using scribe or tweezers.

______4. Using tweezers and septum insertion tool, INSTALL new septum.

______5. Using 1/2" socket wrench, INSTALL needle guide.

6. RECORD septum replacement in PASS log.

Replaced by: Date:

SUBMIT completed attachment to Chemistry Supervision.

CP 3804L SLevel of Use Continuous STOP THINK ACT REVIEW Rev. 003 37 of 38

0 S 0 Attachment 4 Containment Air PASS Simplified Drawing (Sheet 1 of 1)

Suction Line of:

Train A Hydrogen Recombiner Nitrogen Flush S ample From Containment Suction Line of: -p--

Train B Hydrogen Recombiner Return Lines of:

Train A Hydrogen Recombiner Return To Containment Return Lines of:.-

Train B Hydrogen Recombiner Level of Use CP 3804L