ML073300611

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Groundwater Monitoring Report - Plant Vogtle Landfills 2 and 3, Solid Waste Permit Nos. 017-006D(L)(I) and 017-007D(L)(I), Burke County, Georgia, March 2004
ML073300611
Person / Time
Site: Vogtle  Southern Nuclear icon.png
Issue date: 03/17/2004
From: Carr W
Southern Nuclear Operating Co
To: Gillespie H
Office of Nuclear Reactor Regulation, State of GA, Environmental Protection Div
References
017-006D(L)(I), 017-007D(L)(I), EV-04-0432
Download: ML073300611 (199)


Text

{{#Wiki_filter:Southern Nuclear Operating Company, Inc. Post Office Box 1295 Birmingham, Alabama 35201-1295 Tel 205.992.5000 SOUTHERNA. COMPANY Energy to Serve Your World"" File: E.03.40C Log: EV-04-0432 March 17, 2004 FEDERAL EXPRESS Vogtle Electric Generating Plant Landfill #2 and #3 Solid Waste Permit No. 017-006D(L)(I) Solid Waste Permit No. 017-007D(L)(I) Mr. Harold C. Gillespie Unit Coordinator - Industrial Solid Waste Unit Georgia Environmental Protection Division 4244 International Parkway, Suite 104 Atlanta, GA 30354

Dear Mr. Gillespie:

Pursuant to EPD Solid Waste Rule 391-3-4-.14 and in accordance with the approved Plant Vogtle Landfill #2 and #3 Groundwater Monitoring Plans, Southern Nuclear is submitting the attached semi-annual groundwater monitoring report which was prepared for Southern Nuclear by the Dextra Group. This report presents the analytical results for the semi-annual groundwater monitoring samples and annual Appendix II assessment monitoring samples taken in December 2003. As discussed in Sections 5 and 6 of the attached report, there was no statistically significant increase in the concentration of any detected parameter in the compliance well samples compared to the background well samples at Landfill #2. At Landfill #3 there was a statistically significant increase over background for barium, 1,1-dichloroethane and cis-1,2-dichloroethane in wells GWC-13/MW-13 and GWC-14/MW-14; chlorobenzene and 1A-dichlorobenzene in well GWC-14/MW-14 and trichlorofluoromethane in well GWC-13/MW-13. There was also a detection of mercury, an Appendix II parameter, in the sample from well GWC-14/MW-14. Statistical analyses of mercury concentrations were not performed since this was only the second analysis for this parameter. A copy of this letter and the attached report will be placed in the operating record within 14 days to serve as the notice to the operating record in accordance with EPD Solid Waste Rules 391-3-4. The next scheduled semi-annual sampling event is June 2004. In addition to the regular semi-annual monitoring for Appendix I parameters, all wells will continue to be analyzed for mercury. The next annual assessment monitoring for Appendix II parameters in wells GWC-13/MW-13, GWC-14/MW-14 and GWA-15/MW-15 will be conducted in December 2004.

EV-04-0432 Page 2 Georgia Environmental Protection Division Mr. Harold C. Gillespie If you have any questions, please contact Rachel Grimes at (205) 992-7025. Sincerely, ~ W. C. Carr Manager - Environmental Services WCC/RLG:ahl cc: Mr. Michael Kemp (w/o) Mr. Earl Hinkle (w/o) Mr. Kurt Batsel (w/o) Attachment

EV-04-0432 Page 3 Georgia Environmental Protection Division Mr. Harold C. Gillespie bc: P. D. Rushton (w/o) A. Harris (w/o) W. F. Kitchens (w/o) N. J. Stringfellow (w/o) M. E. Wilder (w/o) I. A. Kochery (w/o) B. D. Carter (w/o) S. Sundaram (w/o) C. M. Burke (w/o) (Return Receipt) SNC Document Management - Vogtle (Return Receipt)

GROUNDWATER MONITORING REPORT PLANT VOGTLE LANDFILLS #2 AND #3 SOLID WASTE PERMIT Nos. 017-006D(L)(I) AND 017-007D(L)(I) BURKE COUNTY, GEORGIA MARCH 2004 PREPARED FOR: Southern Nuclear Operating Company, Inc. 40 Inverness Center Parkway Birmingham, Alabama 35201 PREPARED By: Dextra Kurt R. Batsel, P.E. Georgia License Number 16594 The Dextra Group, LLC 4665 Lower Roswell Road, #154 Marietta, Georgia 30068

TABLE OF CONTENTS 1 - Introduction 1 2 - Monitoring Well Network 1 3 - Groundwater Flow Rate and Directional Data 2 3.1 Geology/Hydrogeology 3.2 Groundwater Elevations and Gradients 4 - Sampling Procedures and Parameter Analyses 3 4.1 Procedures and Field Measurements 4.2 Parameter Analyses 5 - Groundwater Quality Evaluation 4 5.1 Detected Parameters 5.2 Statistical Analyses 5.2.1 Landfill #2 5.2.2 Landfill #3 6 - Conclusions 6 In Order Following Page 7 Tables 1 - Groundwater Elevations and Monitoring Well Construction Details, Landfill #2 2 - Groundwater Elevations and Monitoring Well Construction Details, Landfill #3 3 - Groundwater Sampling Field Measurements, Landfill #2 4 - Groundwater Sampling Field Measurements, Landfill #3 5 - Constituents for Detection Monitoring 6 - Constituents for Assessment Monitoring 7 - Summary of Detected Parameters, Landfill #2 8 - Summary of Detected Parameters, Landfill #3 Figures 1 - Potentiometric Surface Map Landfill #2, December 17, 2003 2 - Groundwater Contour Elevation Map Landfill #3, December 16, 2003 Appendices A - Laboratory Analytical Reports B - Statistical Analyses

1 - Introduction This report presents the results of groundwater sampling conducted in December 2003 at two private solid waste landfills (Landfill #2 and Landfill #3) operated by Southern Nuclear Operating Company, Inc. (SNC) at Plant Vogtle in Waynesboro, Georgia. Groundwater monitoring was initiated in 2002 in accordance with the approved Groundwater Monitoring Plan for the landfills. The landfills are used for disposal of non-putrescible, non-liquid office and solid waste as well as construction/demolition debris such as asbestos insulation, wooden pallets, and concrete. The landfills are operated under Solid Waste Permit #s 017-006D(L)(I) and 017-007D(L)(I). The active trench at Landfill #2 is used only for asbestos disposal. Landfill #3, permitted in 1987, has been utilized for construction and demolition debris disposal since 1992. Sampling, analyses and data evaluation were conducted in accordance with the rules of the Georgia Department of Natural Resources Environmental Protection Division, Chapter 391-3-4, the September 1991 "Manual for Groundwater Monitoring" and the approved Groundwater Monitoring Plan for the landfills. The findings of the initial four sampling events, conducted from August 2002 through December 2002, and subsequent semi-annual sampling events were presented in reports previously submitted to the Department. This report presents the results of the December 2003 semi-annual detection monitoring sampling event and annual assessment monitoring. Subsequent reports will be prepared upon completion of semi-annual sampling events as scheduled in the Groundwater Monitoring Plan. 2 - Monitoring Well Network The groundwater monitoring well network consists of four permanent monitoring wells located along the north, east and south waste unit management boundaries of Landfill #2 (Figure 1), and seven permanent monitoring wells located along the perimeter of the waste management unit boundary of Landfill #3 (Figure 2). As shown in the figures, the wells are located outside of, but as close as practical to, the waste disposal areas. The wells are screened within the uppermost water-producing zones underlying the landfills, which occur from approximately 35 to 60 feet below land surface at Landfill #2 and from approximately 30 to 50 feet below land surface at Landfill #3. The four permanent groundwater monitoring wells at Landfill #2 were installed in September 2001 after advancing a total of eight deep soil borings around the landfill boundary. The upgradient well is GWA-2/MW-2 and the downgradient, or compliance, wells are GWC-3/MW-3 and GWC-ll/MW-

11. Well GWB-4/MW-4 is best characterized as a cross-gradient well, but is evaluated as a compliance well for this report. The well construction details are presented in Table 1.

The seven permanent groundwater monitoring wells at Landfill #3 were installed in September 2001 and in July 2002. The well construction details are presented in Table 2. Wells GWA-7/MW-7 and GWA-15/MW-15 are located at the south and southwest portions of the landfill boundary. Wells GWC-5/MW-5, GWC-13/MW-13 and GWC-14/MW-14 are located along the eastern portion of the landfill boundary, and wells GWB-6/MW-6 and GWB-16/MW-16 are located along the northern landfill boundary. As discussed in Section 3.2, well GWA-15/MW-15 is the designated background well, and the remaining wells are designated compliance wells. No surface water monitoring stations were present at the landfill at the time of the December 2003 sampling event. However, two new stormwater sedimentation ponds, constructed in accordance with the approved Design and Operational Plan, were completed at Landfill #3 after the December 2003

sampling event. It is anticipated that the surface water monitoring stations associated with the new sedimentation ponds will be sampled during the next semi-annual sampling event in June 2004. 3 - Groundwater Flow Rate and Directional Data 3.1 GeoloJ!l/HydrogeoloJ!l The geology of the Plant Vogtle site consists of sedimentary deposits within the Coastal Plain physiographic province of Georgia. These sediments consist of unconsolidated sands, silts and clays comprised of marine and non-marine fluvial deposits. Marls and limestone were also encountered at depth in deep borings completed at the landfills. A boring completed to approximately 126 feet below land surface at the northwest boundary of Landfill #2 appears to have been completed just into or immediately on top of the Utley Limestone member. The marls encountered during drilling were components of the Irwinton Sand member. Either all or parts of the Barnwell Group members (except the Utley Limestone member) were also encountered in the other borings conducted at the landfills. Underlying the Barnwell Group is the Lisbon Formation with its uppermost unit, the Blue Bluff Marl, located immediately under the Utley Limestone. This marl layer, approximately 70 feet thick, is a near-impermeable layer that effectively conftnes the Tertiary and Cretaceous aquifers, the two conftned aquifers beneath the Plant site. The occurrence of groundwater underlying the landfills appears in conftned, semi-confmed, unconftned, and perched hydrogeologic units. Groundwater is found primarily in sands, silty sands, clayey sands and marl limestone interfaces. The main difference between boring/well water production characteristics and aquifer conftning characteristics appears to be the thickness of the water-producing zone, the grain size of the sand component, the sand/clay ratio and the characteristics of the marl/limestone interface. Groundwater may also exist in an unconfmed water table aquifer in the Barnwell sands and limestone that overlie the marl. The water table aquifer at the site is on an interfluvial ridge, or a topographically high area in which the groundwater in the water table discharges along streams that surround the topographic high. The streams eventually discharge to the Savannah River. 3.2 Groundwater Elevations and Gradients During well installation, the occurrence of groundwater was determined by collecting continuous split spoon samples beginning approximately ftve feet above the location of expected groundwater-producing zones. At both landfills, groundwater was generally found in water producing zones less than one foot thick and is frequently under semi-confmed or conftned conditions. Upon completion of all drilling activities, measuring points were located on the tops of the well casings and surveyed relative to mean sea level (msl). During each sampling event, depth to water measurements were recorded in the wells from the surveyed elevations using an electronic water-level indicator. The water level measurements were then subtracted from the appropriate measuring point elevations to determine groundwater elevations in the wells. Hydraulic conductivity (K) in the wells was measured on September 26,2001. The values ranged from 5.634 x 10.4 em/sec in GWB-6/MW-6 to 3.064 x 10.2 cm/sec in GWA-2/MW-2. Landfill #2 Depth to water measurements and groundwater elevations for the wells at Landfill 2 are presented in Table 1. Based on groundwater elevations measured during the sampling events to date, groundwater 2

underneath Landfill 2 trends from a relatively higher elevation at the eastern portion of the landfill (GWA-2/MW-2) to relatively lower elevations in the west to southwest direction beneath the landfill (Figure 1). Well GWC-ll is not used to construct the potentiometric surface map because the uppermost water-bearing unit at this location appears to be within a different hydrologic zone based on the significantly lower groundwater elevation measured in well GWC-ll compared to wells GWA-2, GWC-3 and GWB-4. The hydraulic gradient (shown on Figure 1 for December 2003) was calculated using a three-point problem from potentiometric surface elevations in monitoring wells GWA-2/MW-2, GWC-3/MW-3 and GWB-4/MW-4. The hydraulic gradient has ranged from a minimum of 0.01 (October 2002) to a maximum of 0.08 Oune 2003). Landfill #3 Depth to water measurements and groundwater elevations for the wells at Landfill #3 are presented in Table 2. Based on the measured groundwater elevations to date, it appears that the groundwater elevation, or hydraulic 'head,' is greatest beneath the center area of the landfill, and decreases to the southeast, to the northeast and to the west-southwest beneath the landfill. This mounding effect is believed to be the result of natural inf1ltration in the sandy soils within the topographically high area in the center of the landfill. This topographically high area, which encompasses a broad area within the landfill, is a natural site feature that was present prior to any landfilling operations. As discussed previously, the water-bearing stratigraphy beneath Landfill #3 is composed of individual saturated sand units within a clayey/marl matrix. These units mayor may not be interconnected. As such, groundwater elevations in the monitoring wells may reflect head in multiple perched layers and may not represent groundwater 'flow' direction beneath the landfill. Figure 2 presents a map depicting the saturated head contours measured on December 16, 2003. Monitoring well GWA-15/MW-15 is the well most representative of background water quality at the site because of the distance between the well and the current landfilled area, and the location of the area of relatively higher head located between the well and the current landfilled area on the eastern portion of the site. This well is therefore used as a background well to evaluate groundwater quality at the landf1ll. The hydraulic gradient was calculated using a three-point problem from groundwater elevations in the monitoring wells as follows for each main direction of head difference: Southeast: GWA-7/MW-7, GWC-13/MW-13, and GWC-14/MW-14; Northeast: GWB-6/MW-6, GWC-13/MW-13, and GWC-5/MW-5; and West-Southwest: GWA-7/MW-7, GWB-6/MW-6, and GWA-15/MW-15. The calculated hydraulic gradient is presented on the contour map (Figures 2). To date the steepest hydraulic gradient has been consistently to the north-northeast. The north-northeast trending gradient has ranged from a minimum of 0.08 (October and December 2002) to a maximum of 0.17 Oune 2003). 4 - Sampling Procedures and Parameter Analyses 4.1 Procedures and Field Measurements Prior to sample collection during each sampling event, depth to water measurements are recorded in each well from the surveyed elevations using an electronic water level indicator. The water level indicator is decontaminated using a potable water and Alconox wash and a potable water rinse 3

between use at each well. The water level measurements are then subtracted from the appropriate measuring point elevations to determine the groundwater elevations in the wells. Groundwater samples were collected from all monitoring wells after the wells were properly purged according to the EPA document entided "Low-Flow Purging & Sampling of Groundwater Monitoring Wells (Bulletin QAD023)". The wells were purged and sampled using QED SamplePro pumps equipped with Teflon bladders. Purge rates were matched to the recovery rates of the wells, verified by periodic depth to water measurements to determine draw-down during purging. Purging was conducted until at least three consecutive stable readings of pH, conductivity, and turbidity were recorded. Groundwater samples were then collected direcdy into pre-preserved sample containers supplied by the laboratory. Final measurements of pH, conductivity, and turbidity were performed to verify that these parameters remained stable during sampling. All field instruments were calibrated in the field daily prior to use and at the conclusion of each sampling event. The field measurements are provided in Tables 3and4. After each sample was collected, the SamplePro pumps and airlines were decontaminated according to the following protocol: The pump and air line were placed on clean plastic; The pump was disassembled and the bladder was removed; The pump was sprayed with a potable water and Alconox solution, followed with a distilled water rinse until all soap residue was removed; A new pump bladder was then installed in the pump prior to reassembly; and The pump airline was placed in a clean plastic bag between use at each well. 4.2 ParameterAna!yses In accordance with the approved Groundwater Monitoring Plan, the groundwater samples and field and laboratory quality assurance/quality control (QA/Qc) samples were analyzed for the Chapter 391-3-4 Appendix I list of parameters, which consists of total metals and volatile organic compounds (Table 5). The field QA/QC samples consisted of duplicate samples, trip blanks and equipment blanks. Metals analyses were conducted using EPA Methods 6010B/7841, and VOCs analyses were conducted using EPA Methods 6010B/8260B and 504.1 to provide sufficiendy sensitive quantitation limits for comparison with maximum contaminant limits. Advanced Chemistry Labs, Inc., Adanta, Georgia performed the laboratory analyses. The complete laboratory analytical reports, which include field and laboratory QA/QC results and chain-of-custody forms, are provided in AppendixA. In addition, assessment monitoring was conducted at Landfill #3 for the December 2003 sampling event based on the results of previous detection monitoring events in which statistically significant concentrations of barium and several organic parameters were indicated in the GWC-13 and GWC-14 well samples. Mercury was also detected previously in the GWC-13 and GWC-14 well samples. Assessment monitoring consisted of analyses of the Chapter 391-3-4 Appendix II list of parameters for the GWA-15, GWC-13 and GWC-14 well samples, and mercury for all well samples. 5 - Groundwater Quality Evaluation 5.1 Detected Parameters Tables 6 and 7 present a summary of all analyzed parameters that were detected above the laboratory method reporting limits. 4

Lmdfil/#2 At Landfill #2, barium was detected at 0.022 milligrams per liter (mg/l) in the GWC-ll sample. The maximum contaminant level (MCL) for barium is 2.0 mg/I. The organic parameter trichlorofluoromethane was also detected at 6 micrograms per liter (ug/l) in the GWB-4 sample. There is no MCL for this parameter. No parameters were detected in any of the field or laboratory QA/QC samples, and the laboratory QA/QC checks were within acceptable limits. LJndfill#3 At Landfill #3, barium was detected at concentrations below the MCL in the samples from wells GWC-5, GWC-13, and GWC-14 and zinc was also detected in background well GWA-7, and wells GWC-5 and GWC-14. As shown in Table 7, a number of additional metals were also detected in the samples from GWC-5 and GWC-14. All detected concentrations were below the MCLs except for Mercury at 0.01 mg/l (MCL of 0.002 mg/l) and cadmium at 0.011 mg/l (MCL of 0.005 mg/l), both of which occurred in well GWC-14. It should be noted that the turbidity measured in wells GWC-5 (79.7 ntu's) and GWA-7 (100 ntu's) was significantly higher than in previous sampling events, and higher than the recommended maximum of 10 ntu's. In addition, well GWC-13 required 6 gallons of purging to reduce the turbidity below 10 ntu's compared to 1 to 2.5 gallons purged in previous sampling events. In GWC-14, there was insufficient water to facilitate sample collection using the low-flow pump assembly. The well was sampled using a bailer after purging the previous evening. No indicator parameters were measured during sampling of GWC-14 due to the lack of water in the well during purging. The increased detections of metals and VOCs in the wells during this sampling event is likely due to the increased turbidity in the wells, an indication that particles from the aquifer were suspended in the samples during collection. The VOCs 1,1-dichloroethane, and cis-l,2-dichloroethene were detected in the GWC-13 and GWC-14 samples. Chlorobenzene and 1,4-dichlorobenzene were also detected in the GWC-14 sample. Trichlorofluoromethane was detected in samples from GWA-7, and GWC-13. Xylenes were also detected in the sample from GWC-14. All of the detected VOCs were reported at concentrations below the MCLs, where applicable. No parameters were detected in any of the field or laboratory QA/QC samples, and the laboratory QA/QC checks were within acceptable limits. The Department collected split samples from wells GWC-5, GWC-13, GWC-14 and GWA-15 for VOCs and metals analyses. 5.2 StatisticalAnalYses In accordance with the approved Groundwater Monitoring Plan, statistical analyses were conducted for each constituent detected in the compliance well samples for this sampling event. The analyses were conducted to help identify any significant increase in constituent concentrations in downgradient, or compliance, well samples over samples representative of background water quality. The analyses were conducted consistent with U.S. EPA recommended methods as detailed in the guidance document "Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities - Interim Final Guidelines" (1989) and the corresponding Addendum (1992). 5

The following methodology was used to evaluate the data: The distribution of the data was first evaluated for normality using the Shapiro-Wilkes Test as recommended in the 1992 EPA guidance. The test indicates that the concentrations of the detected parameters in all wells at both landfills do not follow normal distributions. For the well data sets at both landfills, the Kruskal-Wallis non-parametric analysis of variance method was used to compare the concentrations of individual parameters in each compliance well to the concentrations of these parameters in the background wells. This method is recommended by the 1992 EPA guidance for sample sets that do not follow a normal distribution or that have between 15% and 90% non-detects. The detailed statistical analyses are provided in Appendix B and the results are summarized below. 5.2.1 Landfill #2 At Landfill #2, barium was detected in the sample from compliance well GWC-11/MW-11 and trichlorofluoromethane was detected in the GWB-4 well sample. The analyses indicate no statistically significant increase in the concentrations of these parameters in the compliance well samples as compared to the concentrations in the background well samples. 5.2.2 Landfill #3 Compared to background wells GWA-7/MW-7 and GWA-15/MW-15, the analyses indicate statistically significant higher concentrations of the following parameters: Barium in wells GWC-13/MW-13 and GWC-14/MW-14; 1,1-dichloroethane and cis-1,2-dichloroethene in wells GWC-13 and GWC-14; CWorobenzene and 1,4-dichlorobenzene in well GWC-14/MW-14; and Trichlorofluoromethane in well GWC-13/MW-13. The Appendix II parameter, mercury, was also detected in the GWC-14/MW-14 well sample at 0.01 mg/I. The MCL for mercury is 0.002 mg/I. Statistical analyses of mercury concentrations were not performed since this parameter was only analyzed for the second time as a component of assessment monitoring for this event. 6 - Conclusions Since a statistically significant increase over background is indicated for several analyzed parameters in wells GWC-13/MW-13 and GWC-14/MW-14 at Landfill #3, SNC will place a notice in the operating record within 14 days of submittal of this report as required by Chapter 391-3-4. The notice will indicate which constituents have shown statistically significant higher concentrations than in the background wells. The notice will also include detection of the Appendix II parameter, mercury, in well sample GWC-14/MW-14. SNC will continue assessment monitoring per the requirements of paragraphs (20) through (33) of Chapter 391-3-4-.14. Based on detection of the Appendix II parameter mercury during this sampling event, future semi-annual sampling will include analysis for mercury in all wells. In addition, the December 2004 sampling event will include the complete Appendix II analyses in wells GWA-15/MW-15, GWC-13/MW-13 and GWC-14/MW-14 to satisfy the assessment monitoring program requirement for annual Appendix II analysis in wells showing statistically significant increases of 6

baseline monitoring parameters. After completion of 4 semi-annual sampling events for mercury, this parameter will be added to the routine statistical analysis that is currently performed for the Appendix I parameters. 7

TABLES

Table 1 Southern Nuclear Operating Company Plant Vogtle Landfill #2 Groundwater Elevations and Monitoring Well Construction Details Total Boring Total Well Riser Groundwater Measuring Point Elevation Ground Surface Elevation Depth to Water Depth Depth Height Screened Interval Elevation WelllD Date (feet, msl) (feet, msl) (feet, topvc) (feet, bls) (feet, topvc) (feet) (feet, msl) (feet, msl) GWA-2/MW-2 9/26/2001 249.41 246.76 40.02 57 47.30 2.70 191.76 to 201.76 209.39 7/29/2002 41.69 207.72 9/9/2002 41.64 207.77 10/21/2002 42.72 206.69 12/3/2002 40.69 208.72 6/24/2003 37.58 211.83 12/17/2003 39.98 209.43 GWC-3/MW-3 9/26/2001 250.41 247.81 50.45 50 52.08 2.66 187.81 to 197.81 199.96 7/29/2002 50.05 200.36 9/9/2002 50.79 199.62 10/21/2002 49.30 201.11 12/3/2002 50.26 200.15 6/24/2003 51.58 198.83 12/1712003 47.89 202.52 GWB-4/MW-4 9/26/2001 242.40 239.83 39.84 54 48.80 2.60 183.83 to 193.83 202.56 7/29/2002 40.06 202.34 9/9/2002 41.27 201.13 10/21/2002 40.50 201.90 12/4/2002 39.65 202.75 6/24/2003 38.10 204.30 12/17/2003 39.53 202.87 GWC-11/MW-11 7/29/2002 227.53 225.09 64.80 65 68.95 2.44 158.58 to 168.58 162.73 9/9/2002 59.99 167.54 10/21/2002 65.27 162.26 12/4/2002 65.49 162.04 6/24/2003 59.72 167.81 12/17/2003 59.33 168.20 Notes: Ground surface measured at survey bolt set in concrete pad at base of protective casing. msl = mean sea level. topvc =measured from top of pvc riser. bls = below land surface. Page 1 of 1

Table 2 Southern Nuclear Operating Company Plant VogUe Landfill #3 Groundwater Elevations and Monitoring Well Construction Details Total Boring Total Well Riser Groundwater Measuring Point Elevation Ground Surface Elevation Depth to Water Depth Depth Height Soreened Interval Elevation Well 10 Olte (feet, mIl) (feet, mIl) (feet, topvc) (feet, bll) (feet, topvc) (feet) (feet, msl) (feet, mIl) GWC-5IMW-5 912612001 251.96 249.11 48.65 57 5741 2.89 185.11 to 195.11 203.31 712912002 50.21 201.75 91912002 5043 201.53 1012112002 49.26 202.70 12/312002 49.26 20270 612412003 44.60 207.36 1211612003 47.55 204.41 GWB-6IMW-6 912612001 278.87 276.45 4747 67 64.34 243 202.45 to 212.45 231.40 712912002 48.52 230.35 91912002 48.55 230.32 1012112002 49.21 229.66 121312002 48.86 230.Q1 612412003 46.92 231.95 12/1612003 46.30 232.57 GWA-7IMW-7 912612001 261.33 259.39 31.11 50 4022 1.90 211.11 t0221.11 23022 712912002 33.16 22817 91912002 33.25 228.08 1012112002 33.20 228.13 121312002 32.94 228.39 612412003 27.51 233.82 1211612003 30.59 230.74 GWC-131MW-13 712912002 273.08 270.99 40.92 50 50.14 209 222.94 to 232.94 232.16 91912002 41.00 232.08 1012112002 40.94 232.14 121312002 40.48 232.60 612412003 36.90 236.18 1211612003 39.17 233.91 GWC-14IMW-14 712912002 262.88 260.66 40.05 60 53.38 2.22 209.50 to 229.50 222.83 91912002 42.31 220.57 1012112002 42.79 220.09 1213/2002 42.35 220.53 612412003 44.29 218.59 12/1612003 51.52 211.36 GWA*15IMW-15 712912002 268.15 265.34 45.94 55 56.86 2.81 211.29 to 22129 222.21 91912002 46.05 222.10 1012112002 46.19 221.96 121312002 46.23 221.92 612412003 41.76 226.39 1211612003 43.29 224.86 GWB*161MW-16 712912002 256.95 254.57 DRY 65 67.39 2.38 189.56 to 209.56 DRY 91912002 DRY DRY 1012112002 DRY DRY 121312002 DRY DRY 612412003 DRY DRY 12/1612003 DRY DRY Notes: Ground surface measured at survey bolt set in concrete pad at base of protective casin9. msl = mean sea level; topvc = measured from top of pvc riser; bls = below land surface Page 1 of 1

Table 3 Southern Nuclear Operating Company Plant Vogtle Landfill #2 Groundwater Sampling Field Measurements Gallons WelllD Date pH Conductivity1 Turbidity2 Purged Odor Color Notes GWA-2/MW-2 9/2612001 Well development only 7/29/2002 4.69 19 13.8 2.5 none none 9/912002 4.51 24.9 7.53 none none 10/21/2002 5.17 18 1.31 3.1 none none 12/312002 5.30 13 9.1 3.5 none none 6/24/2003 6.28 26.9 5.76 1.0 none none 12/17/2003 4.93 22.7 4.5 3.5 none none GWC-3/MW-3 9/2612001 Well development only 7/29/2002 4.08 27.9 22.2 1.3 none none 9/912002 6.03 36.5 4.08 0.5 none none 10/21/2002 176 35.6 <0.5 gal Too little water to purge and sample 12/312002 5.51 488 14.0 <0.5 gal Too little water to purge and sample 6/24/2003 <0.5 gal none none Too little water to purge and sample 12/17/2003 6.59 22.7 2.79 2.0 none none GWB-4/MW-4 9/2612001 4.73 36.0 15.5 35.0 Well development only 7/29/2002 4.21 269 3.63 2.0 none none 9/912002 4.35 34.8 0.55 2.0 none none 10/21/2002 5.01 25 6.44 3.0 none none 12/412002 5.51 98.7 2.60 4.0 none none 6/24/2003 5.33 36.0 5.27 2.0 none none 1211712003 4.62 3.55 0.00 1.5 none none GWC-11/MW-11 7/29/2002 5.30 67.5 36.6 4.0 none pale white 9/912002 6.24 97.0 6.51 2.0 none none 10/21/2002 5.05 75.0 8.05 1.8 none none 12/412002 5.72 57.1 8.10 2.0 none none 6/24/2003 6.93 70.0 2.70 2.5 none none 1211712003 7.04 69.2 11.2 4.5 none none Notes: _. =no data recorded 1 - Conductivity in units of umhoslsec 2 - Turbidity in units of NTU 1 of 1

Table 4 Southern Nuclear Operating Company Plant Vogtle Landfill #3 Groundwater Sampling Field Measurements Gallons Well 10 Date pH Conductivity' Turbidity' Puraed Odor Color Note. GWC-5/MW-5 912612001 5.11 47.5 28.6 6.0 none doudy Well development only 712912002 5.41 24.4 283 1.75 none none 91912002 813 365 4.11 20 none none 1012112002 121312002 5.94 117 78 20 none none 612412003 5.18 29 3.5 6.0 none none 1211612003 6.27 210 79.7 3.0 none doudy Split with GAEPD GWB-6IMW-6 912612001 713 242 256 2.0 none Well development only 712912002 6.75 1,338 0.35 1.5 none none 91912002 4.13 198 6.43 1.5 none none 1012112002 6.72 573 0.44 2.5 none none 121312002 6.14 116 0.45 1.5 none none 612412003 7.09 155 9.1 1.5 none none 12/1712003 6.82 126 2.27 1.5 none none GWA-7IMW-7 912612001 doudy 300 Well development only 712912002 6.97 251 8.33 2.5 none none 91912002 7.52 327 9.97 5.0 none none 1012112002 4.39 92 3.14 2.0 none none 121312002 6.51 188 7.3 2.5 none none 612412003 7.02 163 101.3 4.0 none dark brown Turbidity >100 ntu for 2 hours. 12/1612003 5.73 627 100 4.0 none mod. brown Turbidity 85-100 ntu for 1 hour. GWC-13/MW-13 712912002 6.52 421 0.66 9/912002 5.96 77.5 6.40 1.0 none none 10121/2002 6.19 73.4 3.09 2.5 none none 121312002 6.54 481 100 2.5 none none 612412003 5.95 271 2.02 2.5 none none 12/1612003 5.65 294 0.75 6.0 none none Split with GAEPD GWC-14IMW-14 712912002 6.49 448 1.15 none none 9/912002 5.57 717 5.19 none none 1012112002 6.00 674 4.65 3.2 none none 121312002 5.54 547 2.7 4.5 none none 612412003 5.97 197 3.61 2.5 none none 12/1712003 Split with GAEPD-VOCs & metals GWA-15IMW-15 712912002 5.70 95.8 112 4.0 none none 9/912002 5.92 118 8.53 2.5 none none 1012112002 5.19 81 1.88 4.5 none none 121312002 7.58 78.2 36 2.5 none none 612412003 7.44 48.0 5.38 2.5 none none 12/1712003 6.93 39.4 4.55 6.5 none none Split with GAEPD GWB-16IMW-16 7129/2002 Well Dry 919/2002 Well Dry 1012112002 Well Dry 121312002 Well Dry 6124/2003 Well Dry 12/1612003 Well Dry Notes: -- = no data recorded; 1 - Conductivity in units of umhoslsec; 2 - TUrbidity in units of NTU. 1 of 1

Table 5 Southern Nuclear Operating Company Plant Vogde Landfills #2 and #3 Appendix I to Part 40 CFR Part 258: Constituents for Detection Monitoring (1) Common Name (2) Inorganic Constituents: (1) Antimony (2) Arsenic (3) Barium (4) Beryllium (5) Cadmium (6) Chromium (7) Cobalt (8) Copper (9) Lead (10) Nickel (11) Selenium (12) Silver (13) Thallium (14) Vanadium (15) Zinc Organic Constituents: (16) Acetone (17) Acrylonitrile (18) Benzene (19) Bromochloromethane (20) Bromodichloromethane (21) Bromoform; Tribromomethane (22) Carbon disulfide (23) Carbon tetrachloride (24) Chlorobenzene (25) Chloroethane; Ethyl chloride (26) Chloroform; Trichloromethane (27) Dibromochloromethane; Chlorodibromomethane (28) 1,2-Dibromo-3-chloropropane; DBCP (29) 1,2-Dibromoethane; Ethylene dibromide; EDB (30) o-Dichlorobenzene; 1,2-Dichlorobenzene (31) p-Dichlorobenzene; 1,4-Dichlorobenzene (32) trans-l,4-Dichloro-2-butene (33) 1,I-Dichloroethane; Ethylidene chloride (34) 1,2-Dichloroethane; Ethylene dichloride (35) 1,I-Dichloroethylene; 1,I-Dichloroethene; Vinylidene chloride (36) cis-l,2-Dichloroethylene; cis-l,2-Dichloroethene (37) trans-l,2-Dichloroethylene; trans-l,2-Dichloroethene (38) 1,2-Dichloropropane; Propylene dichloride (39) cis-l,3-Dichloropropene (40) trans-l,3-Dichloropropene (41) Ethylbenzene (42) 2-Hexanone; Methyl butyl ketone (43) Methyl bromide; Bromomethane (44) Methyl chloride; Chloromethane Page 1 of 2 EPA Method 6010B/7041 6010B/7061 6010B/7091 6010B/7091 6010B/7131 6010B/7191 6010B/7201 6010B/7211 6010B/7421 6010B/7520 6010B/7741 6010B/7761 6010B/7841 6010B/7911 6DI0B/7951 8260

Table 5 (continued) Southern Nuclear Operating Company, Inc. Plant Vogtle Landfills #2 and #3 Appendix I to Part 40 CFR Part 258: Constituents for Detection Monitoring (1) Common Name (2) (45) Methylene bromide; Dibromomethane (46) Methylene chloride; Dichloromethane (47) Methyl ethyl ketone; MEK; 2-Butanone (48) Methyl iodide; Iodomethane (49) 4-Methyl-2-pentanone; Methyl isobutyl ketone (50) Styrene (51) 1,1,1, 2-Tetrachloroethane (52) 1,1,2,2-Tetrachloroethane (53) Tetrachloroethylene; Tetrachloroethene; Perchloroethylene (54) Toluene (55) 1, 1, I-Trichloroethane; Methylchloroform (56) 1,1, 2-Trichloroethane (57) Trichloroethylene; Trichloroethene (58) Trichlorofluoromethane; CFC-ll (59) 1,2, 3-Trichloropropane (60) Vinyl acetate (61) Vinyl chloride (62) Xylenes EPA Method 8260 (1) This list contains 47 volatile organics for which possible analytical procedures provided in EPA Report SW-846 "Test Methods for Evaluating Solid Waste, " third edition, November 1986, as revised December 1987,includes Method 8260; and 15 metals for which SW-846 provides either Method 6010 or a method from the 7000 series of methods. (2) Common names are those widely used in government regulations, scientific publications, and commerce; synonyms exist for many chemicals. Page 2 of 2

I 1.. _.: 6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ Acenaphthene Acenaphthylene Acetone Acetonitrile; Methyl cyanide Acetophenone 2-Acetylaminofluorene; 2-AAF Acrolein Acrylonitrile Aldrin Allyl chloride 4-Aminobiphenyl Anthracene Antimony Arsenic Barium Benzene Benzo[a]anthracene; Benzanthracene.... CAS RN \\3\\ 83-32-9 208-96-8 67-64-1 75-05-8 98-86-2 53-96-3 107-02-8 107-13-1 309-00-2 107-05-1 92-67-1 120-12-7 (Total) (Total) (Total) 71-43-2 56-55-3 Chemical abstracts service index name \\4\\ Acenaphthylene, 1,2-dihydro-.. Acenaphthylene 2-Propanone Acetonitrile

Ethanone, 1-phenyl-Acetamide, N-9H-fluoren-2-yl-.

2-Propenal 2-Propenenitrile 1, 4:5, 8-0imethanonaphthalene, 1,2,3,4,10,10-hexachloro-1,4,4a,5,8,8a-hexahydro-(lcx,4cx,4af3,5 cx,8cx,8af3)- I-Propene, 3-chloro-.. '"..... [l,1\\1\\-Biphenyl]-4-amine Anthracene Antimony Arsenic Barium Benzene Benz[a]anthracene Page 1 of 16 Suggested methods \\5\\ 8100 8270 8100 8270 8260 8015 8270 8270 8030 8260 8030 8260 8080 8270 8010 8260 8270 8100 8270 6010 7040 7041 6010 7060 7061 6010 7080 8020 8021 8260 8100 8270 PQL (p giL) \\6\\ 200 10 200 10 100 100 10 20 5 100 5 200 0.05 10 5 10 20 200 10 300 2000 30 500 10 20 20 1000 2 0.1 5 200 10

T.. _~~ 6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Corrunon Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (]J giL) \\6\\ Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[ghi]perylene Ben zo [a] pyrene Benzyl alcohol Beryllium alpha-BHC beta-BHC delta-BHC garruna-BHC; Lindane 205-99-2 207-08-9 191-24-2 50-32-8 100-51-6 (Total) 319-84-6 319-85-7 319-86-8 58-89-9 Benz [e]acephenanthrylene Benzo[k]fluoranthene Benzo[ghi]perylene Benzo[a]pyrene Benzenemethanol Beryllium Cyclohexane, 1,2,3,4,5,6-hexachloro-, (lcx,2cx,3f),4& alpha;,5f),6f))-. Cyc1ohexane, 1,2,3,4,5,6-hexachloro-, (lcx,2f),3cx,4& beta;,5cx,6f))-. Cyclohexane, 1,2,3,4,5,6-hexachloro-, (lcx,2cx,3cx,4 f),5cx,6f))-. Cyclohexane, 1,2,3,4,5,6-hexachloro-, (lcx,2cx,3f),4& alpha;,5cx,6f))-. 8100 200 8270 10 8100 200 8270 10 8100 200 8270 10 8100 200 8270 10 8270 20 6010 3 7090 50 7091 2 8080 0.05 8270 10 8080 0.05 8270 20 8080 0.1 8270 20 8080 0.05 8270 20 Bis(2-ch10roethoxy)methane Bis(2-chloroethyl) ether; Dichloroethyl ether. 111-91-1 Ethane, 1,1\\1\\- [methylenebis(oxy)]bis[2-chloro-. 111-44-4 Ethane, 1,1\\1\\-oxybis[2-chloro-Page 2 of 16 8HO 8270 8HO 8270 5 10 3 10

TaUle 6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (j.l giL) \\6\\ Bis-(2-chloro-1-methy1ethyl) ether; 2,2\\1\\-Dichlorodiisopropyl ether;

DCIP, See note 7

Bis(2-ethylhexyl) phthalate Bromochloromethane; Chlorobromomethane Bromodichloromethane; Dibromochloromethane. Bromoform; Tribromomethane 4-Bromopheny1 phenyl ether Butyl benzyl phthalate; Benzyl butyl phthalate. Cadmium Carbon disulfide Carbon tetrachloride Chlordane p-Chloroaniline Chlorobenzene Chlorobenzilate 108-60-1 117-81-7 74-97-5 75-27-4 75-25-2 101-55-3 85-68-7 (Total) 75-15-0 56-23-5 See Note 8 106-47-8 108-90-7 510-15-6

Propane, 2,2\\1\\-oxybis[1-chloro-.

1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) ester.

Methane, bromochloro-
Methane, bromodichloro-
Methane, tribromo-
Benzene, 1-bromo-4-phenoxy-...

1,2-Benzenedicarboxylic acid, butyl pheny1methyl ester. Cadmium Carbon disulfide

Methane, tetrachloro-4,7-Methano-1H-indene, 1,2,4,5,6,7,8,8-octachloro-2,3,3a,4,7,7a-hexahydro-.

Benzenamine, 4-ch1oro-

Benzene, chloro-Benzeneacetic acid, 4-chloro-a-(4-ch1orophenyl)-

a-hydroxy-, ethyl ester. Page 3 of 16 8110 10 8270 10 8060 20 8021 0.1 8260 5 8010 1 8021 0.2 8260 5 8010 2 8021 15 8260 5 8110 25 8270 10 8060 5 8270 10 6010 40 7130 50 7131 1 8260 100 8010 1 8021 0.1 8260 10 8080 0.1 8270 50 8270 20 8010 2 8020 2 8021 0.1 8260 5 8270 10

l~~.e 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Corrunon Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (].1 giL) \\6\\ p-Chloro-m-cresol; 4-Chloro methylphenol. Chloroethane; Ethyl chloride Chloroform; Trichloromethane... '".... 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenyl phenyl ether Chloroprene Chromium Chrysene Cobal t Copper m-Cresol; 3-methylphenol o-Cresol; 2-methylphenol p-Cresol; 4-methylphenol Cyanide 2,4-D; 2,4-Dichlorophenoxyacetic acid. 59-50-7

Phenol, 4-chloro-3-methyl-....

8040 5 8270 20 75-00-3

Ethane, chloro-...............

8010 5 8021 1 8260 10 67-66-3 Methane, trichloro-........... 8010 0.5 8021 0.2 8260 5 91-58-7 Naphthalene, 2-chloro-........ 8120 10 8270 10 95-57-8

Phenol, 2-chloro-.............

8040 5 8270 10 7005-72-3

Benzene, 1-chloro-4-phenoxy-..

8110 40 8270 10 126-99-8 1,3-Butadiene, 2-chloro-...... 8010 50 8260 20 (Total) Chromium...................... 6010 70 7190 500 7191 10 218-01-9 Chrysene...................... 8100 200 8270 10 (Total) Cobalt........................ 6010 70 7200 500 7201 10 (Total) Copper........................ 6010 60 7210 200 7211 10 108-39-4

Phenol, 3-methyl-........... "

8270 10 95-48-7

Phenol, 2-methyl-.............

8270 10 106-44-5

Phenol, 4-methyl-.......... '"

8270 10 57-12-5 Cyanide....................... 9010 200 94-75-7 Acetic acid, (2,4-8150 10 dichlorophenoxy)-. Page 4 of 16

Tavie 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (fl giL) \\6\\ 4,4\\1\\-000 4,4\\1\\-DDE 4,4\\1\\-DOT Oia11ate Dibenz[a,h]anthracene Dibenzofuran Oibromoch1oromethane; Ch1orodibromomethane. 1,2-Dibromo-3-ch1oropropane; DBCP..... 1,2-Dibromoethane; Ethylene dribromide; EOB. Oi-n-butyl phthalate o-Dich1orobenzene; 1,2-0ichlorobenzene m-Dichlorobenzene; 1,3-Dichlorobenzene 72-54-8 72-55-9 50-29-3 2303-16-4 53-70-3 132-64-9 124-48-1 96-12-8 106-93-4 84-74-2 95-50-1 541-73-1 Benzene 1,1\\1\\-(2,2-dichloroethylidene)bis[4-chloro-. Benzene, 1,1\\1\\- (dichIoroethyenylidene)bis[4-chloro-. Benzene, 1,1\\1\\-(2,2,2-trichIoroethylidene)bis[4-chloro-. Carbamothioic acid, bis(l-methyIethyI)-,S-(2,3-dichIoro-2-propenyl) ester. Dibenz[a,h]anthracene Dibenzofuran

Methane, dibromochloro-
Propane, 1,2-dibrome-3-chloro-
Ethane, 1,2-dibromo-1,2-Benzenedicarboxylic acid, dibutyl ester.
Benzene, 1,2-dichloro-
Benzene, 1,3-Dichloro-Page 5 of 16 8080 0.1 8270 10 8080 0.05 8270 10 8080 0.1 8270 10 8270 10 8100 200 8270 10 8270 10 8010 1

8021 0.3 8260 5 8011 0.1 8021 30 8260 25 8011 0.1 8021 10 8260 5 8060 5 8270 10 8010 2 8020 5 8021 0.5 8120 10 8260 5 8270 10 8010 5 8020 5 8021 0.2

T~h,.e 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (p giL) \\6\\ 156-59-2 Ethene, 1,2-dichloro-, (Z)-... 156-60-5

Ethene, 1, 2-dichloro-,

(E) -... p-Oichlorobenzene; 1,4-0ichlorobenzene 3,3\\1\\-Oichlorobenzidine trans-1,4-0ichloro-2-butene Oichlorodifluoromethane; CFC 12; 1,1-Dichloroethane; Ethyldidene chloride. 1,2-Dichloroethane; Ethylene dichloride. 1,1-Dichloroethylene; 1,1-Oichloroethene; Vinylidene chloride. cis-1,2-Dichloroethylene; cis-1,2-Oichloroethene. trans-1,2-0ichloroethylene trans-1,2-Oichloroethene. 2,4-Dichlorophenol 2,6-Dichlorophenol 1,2-0ichloropropane; Propylene dichloride. 106-46-7 91-94-1 110-57-6 75-71-8 75-34-3 75-35-4 120-83-2 87-65-0 78-87-5 Benzene, 1,4-dichloro- [l,1\\1\\-BiphenylJ-4,4\\1\\-

diamine, 3,3\\1\\-dichloro-.

2-Butene, 1,4-dichloro-, (E)-. Methane, dichlorodifluoro-....

Ethane, 1,1-dichloro-
Ethane, 1,1-dichloro-
Ethene, 1,1-dichloro-
Phenol, 2, 4-dichloro-
Phenol, 2,6-dichloro-
Propane, 1,2-dichloro-Page 60f16 8120 10 8260 5

8270 10 8010 2 8020 5 8021 0.1 8120 15 8260 5 8270 10 8270 20 8260 100 8021 0.5 8260 5 8010 1 8021 0.5 8260 5 8010 0.5 8021 0.3 8260 5 8010 1 8021 0.5 8260 5 8021 0.2 8260 5 8010 1 8021 0.5 8260 5 8040 5 8270 10 8270 10 8010 0.5 8021 0.05 8260 5

1.. ~e 6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Conunon Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (ll giL) \\6\\ 8060 5 8270 10 8141 5 8270 20 8141 3 8270 20 8270 10 8270 10 8270 10 8040 5 8270 10 8060 5 8270 10 8270 20 1,3-Dichloropropane; Trimethylene dichloride. 2,2-Dichloropropane; Isopropylidene chloride. 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Dieldrin Diethyl phthalate O,O-Diethyl 0-2-pyrazinyl phosphorothioate; Thionazin. Oimethoate p-(Dimethylamino)azobenzene 7, 12-0imethylbenz[a]anthracene 3,3\\1\\-Oimethylbenzidine 2,4-0imethylphenol; m-Xylenol Dimethyl phthalate m-Dini trobenzene 142-28-9

Propane, l,3-dichloro-594-20-7
Propane, 2,2-dichloro-563-58-6 I-Propene, 1,1-dichloro-10061-01-5 I-Propene, 1,3-dichloro-,

(2)- 10061-02-6 I-Propene, l,3-dichloro-, (E)- 60-57-1 2,7:3,6-Dimethanonaphth[2,3-b]oxirene, 3,4,5,6,9,9-hexa, chloro-1a,2,2a,3,6,6a,7,7a-octahydro-, (lacx,2~,2acx, 3~,6~,6acx,7 ~,7acx)-. 84-66-2 l,2-Benzenedicarboxylic acid, diethyl ester. 297-97-2 Phosphorothioic acid, 0,0-diethyl O-pyrazinyl ester. 60-51-5 Phosphorodithioic acid, 0,0-dimethyl S-[2-(methylamino) oxoethyl] ester. 60-11-7 Benzenamine, N,N-dimethyl (phenylazo)-. 57-97-6 Benz[a]anthracene, 7,12-dimethyl-. 119-93-7 [l,l\\1\\-Biphenyl]-4,4\\1\\-

diamine, 3,3\\1\\-dimethyl-.

105-67-9

Phenol, 2,4-dimethyl-131-11-3 1,2-Benzenedicarboxylic acid, dimethyl ester.

99-65-0

Benzene, 1,3-dinitro-Page 7 of 16 8021 8260 8021 8260 8021 8260 8010 8260 8010 8260 8080 8270 0.3 5

0.5 15 0.2 5 20 10 5 10 0.05 10

Taole 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring 534-52-1

Phenol, 2-methyl-4,6-dinitro..

51-28-5

Phenol, 2,4-dinitro-..........

121-14-2

Benzene, 1-methyl-2,4-dinitro-606-20-2
Benzene, 2-methyl-1,3-dinitro-Common Name \\2\\

4,6-Dinitro-o-cresol 4,6-Dinitro methylphenol. 2,4-Dinitrophenol; 2,4-Dinitrotoluene 2,6-Dinitrotoluene Dinoseb; DNBP; 2-sec-Butyl-4,6-dinitrophenol. Di-n-octyl phthalate Diphenylamine Disulfoton Endosulfan I Endosulfan II Endosulfan sulfate CAS RN \\3\\ 88-85-7 117-84-0 122-39-4 298-04-4 959-98-8 33213-65-9 1031-07-8 Chemical abstracts service index name \\4\\

Phenol, 2-(1-methylpropyl)-4,6-dinitro-.

1,2-Benzenedicarboxylic acid, dioctyl ester. Benzenamine, N-phenyl-Phosphorodithioic acid, 0,0-diethyl S-[2-(ethylthio) ethyl] ester. 6,9-Methano-2,4,3-benzodioxathiepin, 6,7,8,9,10,10-hexa-chloro-1,5,5a,6,9,9a-hexahydro-, 3-

oxide, 6,9-Methano-2,4,3-benzodioxathiepin, 6,7,8,9,10,10-hexa-chloro-1,5,5a,6,9,9a-hexahydro-,

3-

oxide, (3o:,5ao:,613,9 13,9ao:)-.

6,9-Methano-2,4,3-benzodioxathiepin, 6,7,8,9,10,10-hexa-chioro-1,5,5a,6,9,9a-hexahydro-,3 dioxide. Page 8 of 16 Suggested methods \\5\\ 8040 8270 8040 8270 8090 8270 8090 8270 8150 8270 8060 8270 8270 8140 8141 8270 8080 8270 8080 8270 8080 8270 PQL (ll giL) \\6\\ 150 50 150 50 0.2 10 0.1 10 1 20 30 10 10 2 0.5 10 0.1 20 0.05 20 0.5 10

TaOle6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (p giL) \\6\\ 8020 2 8221 0.05 8260 5 8015 5 8260 10 8270 10 8270 20 8270 20 8100 200 8270 10 8100 200 8270 10 8080 0.05 8270 10 Endrin Endrin aldehyde Ethylbenzene Ethyl methacrylate Ethyl methanesulfonate Famphur Fluoranthene Fluorene Heptachlor 72-20-8 2,7:3,6-0imethanonaphth[2,3-b]oxirene, 3,4,5,6,9,9-hexachloro-la,2,2a,3,6,6a,7,7a-octahydro-, (laex, 2f3,2af3,3ex,6 ex,6af3,7f3,7a ex)-. 7421-93-4 1,2,4-Methenocyclopenta[cd]pentalen e-5-carboxaldehyde, 2,2a,3,3,4,7-hexachlorodecahydro-, (lex,2f3,2af3, 4f3,4a(3,5f3,6a (3,6bf3,7R*)-. 100-41-4 Benzene, ethyl-. '" 97-63-2 2-Propenoic acid, 2-methyl-, ethyl ester. 62-50-0 Methanesulfonic acid, ethyl ester. 52-85-7 Phosphorothioic acid, 0-[4- [(dimethylamino)sulfonyl]phen yl] O,O-dimethyl ester. 206-44-0 Fluoranthene 86-73-7 9H-Fluorene 76-44-8 4,7-Methano-1H-indene, 1,4,5,6,7,8,8-heptachloro-3a,4,7,7a-tetrahydro-. Page 9 of 16 8080 8270 8080 8270 0.1 20 0.2 10

Taule 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Corrunon Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (]l giL) \\6\\ 87-68-3 1,3-Butadiene, 1,1,2,3,4,4-hexachloro-. 1024-57-3 2,5-Methano-2H-indeno[1,2-b]oxirene, 2,3,4,5,6,7,7-heptachloro-1a,lb,5,5a,6,6a-hexahydro-, (lao:,

1br5, 20:,

50:,

5ar5, 6r5, 6ao:).

118-74-1

Benzene, hexachloro-465-73-6 1,4,5,8-Dimethanonaphthalene,1,2,3,4, 10,10- hexachloro-1,4,4a,5,8,8a hexahydro-(10:,40:,4ar5,5 r5,8r5,8ar5)-.

78-59-1 2-Cyclohexen-1-one, 3,5,5-trimethyl-. 120-58-1 1,3-Benzodioxole, 5-(1-propenyl)-. 8120 0.5 8270 10 8021 0.5 8120 5 8260 10 8270 10 8120 5 8270 10 8120 0.5 8260 10 8270 10 8270 10 8260 50 8100 200 8270 10 8015 50 8240 100 8270 20 8260 10 1 10 60 10 10 8080 8270 8090 8270 8270 1,3-Cyclopentadiene, 1,2,3,4,5,5-hexachloro-.

Ethane, hexachloro-I-Propene, 1,1,2,3,3,3-hexachloro-.

2-Hexanone Indeno(1,2,3-cd)pyrene I-Propanol, 2-methyl-67-72-1 77-47-4 78-83-1 591-78-6 193-39-5 1888-71-7 Hexachlorobenzene Hexachlorobutadiene Heptachlor epoxide Hexachlorocyclopentadiene Hexachloroethane Hexachloropropene 2-Hexanone; Methyl butyl ketone Indeno(1,2,3-cd)pyrene Isodrin Isobutyl alcohol Isophorone Isosafrole Page 10 ofl6

Tab... 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring 108-10-1 2-Pentanone, 4-methyl-143-50-0 1,3,4-Metheno-2H-cyclobuta[cd]pentalen-2-one, 1, la, 3, 3a, 4, 5, 5, 5a, 5b, 6-decachlorooctahydro-. (Total) Lead 6010 400 7420 1000 7421 10 7470 2 8015 5 8260 100 8270 100 8080 2 8270 10 8010 20 8021 10 8010 1 8021 0.3 8270 10 8015 10 8260 100 8010 40 8260 10 8015 2 8260 30 8270 10 8270 10 8140 0.5 8141 1 8270 10 8015 5 Cornmon Name \\2\\ Kepone Lead Mercury Methacrylonitrile Methapyrilene Methoxychlor Methyl bromide; Bromomethane Methyl chloride; Chloromethane 3-Methylcholanthrene Methyl ethyl ketone; MEK; 2-Butanone.. Methyl iodide; Iodomethane Methyl methacrylate Methyl methanesulfonate 2-Methylnaphthalene Methyl parathion; Parathion methyl 4-Methyl-2-pentanone; Methyl isobutyl CAS RN \\3\\ (Total) 126-98-7 91-80-5 72-43-5 74-83-9 74-87-3 56-49-5 78-93-3 74-88-4 80-62-6 66-27-3 91-57-6 298-00-0 Chemical abstracts service index name \\4\\ Mercury 2-Propenenitrile, 2-methyl-1,2-Ethanediamine, N.N-dimethyl-N\\1\\-2-pyridinyl-N11 2-thienylmethyl)-. Benzene,l,l\\l\\- (2,2,2,trichloroethy1idene)bi s[4-methoxy-.

Methane, bromo-
Methane, chloro-Benz [j]aceanthrylene, 1,2-dihydro-3-methy1-.

2-Butanone

Methane, iodo-2-Propenoic acid, 2-methyl-,

methyl ester. Methanesulfonic acid, methyl ester. Naphthalene, 2-methyl-..... '" Phosphorothioic acid, 0,0-dimethyl. Suggested methods \\5\\ 8270 PQL (]J giL) \\6\\ 20 Page 11 ofl6

i T~..,.e 6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (].l giL) \\6\\ ketone. Methylene bromide; Dibromomethane..... Methylene chloride; Dichloromethane... Naphthalene 1,4-Naphthoquinone 1-Naphthy1amine 2-Naphthylamine Nickel o-Nitroaniline; 2-Nitroaniline m-Nitroaniline; 3-Nitroanile p-Nitroaniline; 4-Nitroaniline Nitrobenzene o-Nitrophenol; 2-Nitrophenol p-Nitrophenol; 4-Nitrophenol N-Nitrosodi-n-butylamine N-Ni trosodiethy1amine N-Nitrosodimethylamine N-Nitrosodipheny1amine N-Nitrosodipropylamine; N-Nitroso-N-dipropylamine; Di-n-propylnitrosamine. 74-95-3 75-09-2 91-20-3 130-15-4 134-32-7 91-59-8 (Total) 88-74-4 99-09-2 100-01-6 98-95-3 88-75-5 100-02-7 924-16-3 55-18-5 62-75-9 86-30-6 621-64-7

Methane, dibromo-Methane, dichloro-Naphthalene 1,4-Naphthalenedione 1-Naphthalenamine 2-Naphthalenamine Nickel Benzenamine, 2-nitro-Benzenamine, 3-nitro-Benzenamine, 4-nitro Benzene, nitro-
Phenol, 2-nitro-
Phenol, 4-nitro-1-Butanamine, N-butyl-N-nitroso-.

Ethanamine, N-ethyl-N-nitroso-Methanamine, N-methyl-N-nitroso-. Benzenamine, N-nitroso-N-phenyl-. 1-Propanamine, N-nitroso-N-propyl-. 8260 100 8010 15 8021 20 8260 10 8010 5 8021 0.2 8260 10 8021 0.5 8100 200 8260 5 8270 10 8270 10 8270 10 8270 10 6010 150 7520 400 8270 50 8270 50 8270 20 8090 40 8270 10 8040 5 8270 10 8040 10 8270 50 8270 10 8270 20 8070 2 8070 5 8070 10 Page 12 of 16

Tawe6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ N-Nitrosomethylethalamine N-Nitrosopiperidine N-Nitrosopyrrolidine 5-Nitro-o-toluidine Parathion Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol p-Phenylenediamine Phorate Polychlorinated biphenyls; PCBs; Aroclors. Pronamide Propionitrile; Ethyl cyanide Pyrene Safrole Selenium Silver CAS RN \\3\\ 10595-95-6 100-75-4 930-55-2 99-55-8 56-38-2 608-93-5 82-68-8 87-86-5 62-44-2 85-01-8 108-95-2 106-50-3 298-02-2 See Note 9 23950-58-5 107-12-0 129-00-0 94-59-7 (Total) (Total) Chemical abstracts service index name \\4\\ Ethanamine, N-methyl-N-nitroso-Piperidine, 1-nitroso-Pyrro1idine, 1-nitroso-Benzenamine, 2-methyl-5-nitro-Phosphorothioic acid, 0,0-diethyl 0-(4-nitropheny1) ester. Benzene, pentachloro-Benzene, pentachloronitro-Phenol, pentachloro-Acetamide, N-(4-ethoxyphenl).. Phenanthrene Phenol 1,4-Benzenediamine Phosphorodithioic acid, 0,0-diethy1 S-[(ethylthio)methyl] ester. I,l'-Biphenyl, ch1oro derivatives. Benzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)-. Propanenitrile Pyrene 1,3-Benzodioxo1e, 5-(2-propeny1)-. Selenium Silver Suggested methods \\5\\ 8270 8270 8270 8270 8141 8270 8270 8270 8040 8270 8270 8100 8270 8040 8270 8140 8141 8270 8080 8270 8270 8015 8260 8100 8270 8270 6010 7740 7741 6010 7760 7761 PQL (fl giL) \\6\\ 10 20 40 10 0.5 10 10 20 5 50 20 200 10 1 10 2 0.5 10 50 200 10 60 150 200 10 10 750 20 20 70 100 10 Page 13 ofl6

TaUle6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Common Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL ()l giL) \\6\\ Silvex; 2,4,5-TP Styrene Sulfide 2,4,5-T; 2,4,5-Trichlorophenoxyacetic acid. l,2,4,5-Tetrachlorobenzene l,l,l,2-Tetrachloroethane l,l,2,2-Tetrachloroethane Tetrachloroethylene; Tetrachloroethene; Perchloroethylene. 2,3,4,6-Tetrachlorophenol Thallium Tin Toluene o-Toluidine Toxaphene l,2,4-Trichlorobenzene 1, 1, I-Trichloroethane; Methylchloroform. 93-72-1 100-42-5 18496-25-8 93-76-5 95-94-3 630-20-6 79-34-5 127-18-4 58-90-2 (Total) (Total) 108-88-3 95-53-4 See Note 10 120-82-1 71-55-6 Propanoic acid, 2-(2,4,5-trichlorophenoxy)-.

Benzene, ethenyl-Sulfide Acetic acid, (2,4,5-trichlorophenoxy)-.
Benzene, l,2,4,5-tetrachloro-.

Ethane, l,l,l,2-tetrachloro-..

Ethane, l,l,2,2-tetrach1oro-..
Ethene, tetrachloro-
Phenol, 2, 3, 4, 6-tetrachloro-..

Thallium Tin Benzene, methyl-Benzenamine, 2-methyl-Toxaphene Benzene, l,2,4-trichloro-Ethane, l,l,l-trichloro-8150 2 8020 1 8021 0.1 8260 10 9030 4000 8150 2 8270 10 8010 5 8021 0.05 8260 5 8010 0.5 8021 0.1 8260 5 8010 0.5 8021 0.5 8260 5 8270 10 6010 400 7840 1000 7841 10 6010 40 8020 2 8021 0.1 8260 5 8270 10 8080 2 8021 0.3 8120 0.5 8260 10 8270 10 8010 0.3 8021 0.3 8260 5 Page 14 of 16

TaUle 6 Southern Nuclear Operating Company Plant Vogtle Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Cornmon Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (].1 giL) \\6\\ 1,1,2-Trichloroethane Trichloroethylene; Trich1oroethene.... Trichlorofluoromethane; CFC-11 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 1,2,3-Trichloropropane 0,0,0-Triethy1 phosphorothioate sym-Trinitrobenzene Vanadium Vinyl acetate Vinyl chloride; Chloroethene Xylene (total) Zinc 79-00-5 79-01-6 75-69-4 95-95-4 88-06-2 96-18-4 126-68-1 99-35-4 (Total) 108-05-4 75-01-4 See Note 11 (Total)

Ethane, 1,1,2-trichloro-Ethene, trichloro-
Methane, trichlorofluoro-.....
Phenol, 2,4,5-trichloro-
Phenol, 2, 4, 6-trichloro-
Propane, 1,2,3-trichloro-.....

Phosphorothioic acid, 0,0,0-triethylester. Benzene, 1,3,5-trinitro-Vanadium Acetic acid, ethenyl ester

Ethene, chloro-
Benzene, dimethyl-Zinc 8010 0.2 8260 5

8010 1 8021 0.2 8260 5 8010 10 8021 0.3 8260 5 8270 10 8040 5 8270 10 8010 10 8021 5 8260 15 8270 10 8270 10 6010 80 7910 2000 7911 40 8260 50 8010 2 8021 0.4 8260 10 8020 5 8021 0.2 8260 5 6010 20 7950 50 7951 0.5 Notes \\1\\ The regulatory requirements pertain only to the list of substances; the right hand columns (Methods and PQL) are given for informational purposes only. See also footnotes 5 and 6. Page 15 of 16

i Tau£e 6 Southern Nuclear Operating Company Plant Vogde Landfills # 2 and #3 Appendix II to Part 40 CFR Part 258: Constituents for Assessment Monitoring Corrunon Name \\2\\ CAS RN \\3\\ Chemical abstracts service index name \\4\\ Suggested methods \\5\\ PQL (11 giL) \\6\\ \\2\\ Corrunon names are those widely used in government regulations, scientific publications, and corrunerce; synonyms exist for many chemicals. \\3\\ Chemical Abstracts Service registry number. Where "Total" is entered, all species in the ground water that contain this element are included. \\4\\ CAS index are those used in the 9th Collective Index. \\5\\ Suggested Methods refer to analytical procedure numbers used in EPA Report SW-846 "Test Methods for Evaluating Solid Waste", third edition, November 1986, as revised, December 1987. Analytical details can be found in SW-846 and in documentation on file at the agency. CAUTION: The methods listed are representative SW-846 procedures and may not always be the most suitable method(s) for monitoring an analyte under the regulations. \\6\\ Practical Quantitation Limits (PQLs) are the lowest concentrations of analytes in ground waters that can be realiably determined within specified limits of precision and accuracy by the indicated methods under routine laboratory operating conditions. The PQLs listed are generally stated to one significant figure. PQLs are based on 5 mL samples for volatile organics and 1 L samples for semivolatile organics. CAUTION: The PQL values in many cases are based only on a general estimate for the method and not on a determination for individual compounds; PQLs are not a part of the regulation. \\7\\ This substance is often called Bis(2-chloroisopropyl)

ether, the name Chemical Abstracts Service applies to its noncorrunercial isomer,
Propane, 2,2[sec]-oxybis[2-chloro-(CAS RN 39638-32-9).

\\8\\ Chlordane: This entry includes alpha-chlordane (CAS RN 5103-71-9), beta-chlordane (CAS RN 5103-74-2), garruna-chlordane (CAS RN 5566-34-7), and constituents of chlordane (CAS RN 57-74-9 and CAS RN 12789-03-6). PQL shown is for technical chlordane. PQLs of specific isomers are about 20 llg/L by method 8270. \\9\\ Polychlorinated biphenyls (CAS RN 1336-36-3); this category contains congener chemicals, including constituents of Aroclor 1016 (CAS RN 12674-11-2), Aroclor 1221 (CAS RN 11104-28-2), Aroclor 1232 (CAS RN 11141-16-5), Aroclor 1242 (CAS RN 53469-21-9), Aroclor 1248 (CAS RN 12672-29-6), Aroclor 1254 (CAS RN 11097-69-1), and Aroclor 1260 (CAS RN 11096-82-5). The PQL shown is an average value for PCB congeners. \\10\\ Toxaphene: This entry includes congener chemicals contained in technical toxaphene (CAS RN 8001-35-2), i.e., chlorinated camphene. \\11\\ Xylene (total): This entry includes a-xylene (CAS RN 96-47-6), m-xylene (CAS RN 108-38-3), p-xylene (CAS RN 106-42-3), and unspecified xylenes (dimethylbenzenes) (CAS RN 1330-20-7). PQLs for method 8021 are 0.2 for 0-xylene and 0.1 for m-or p-xylene. The PQL for m-xylene is 2.0 llg/L by method 8020 or 8260. Page 16 of 16

Table 7 Southern Nuclear Operating Company Plant Vogtle Landfill #2 Summary of Detected Parameters July 2002 CONSTITUENT MCl WEll SAMPLES GWA-2/MW-2 GWC-3/MW-3 GWS-4/MW-4 GWC-11/MW-11 Metals1 Sarium 2 0.027 SQl 0.021 0.085 Zinc NA SQl SQl SQl 0.034 Organics2 1,1-Dichloroethane NA SQl SQl SQl SQl Chlorobenzene 100 SQl SQl SQl SQl 1A-Dichlorobenzene 75 SQl SQl SQl SQl Methylene chloride 5 SQl SQl cis-1,2-Dichloroethene 70 SQl SQl SQl SQl Trichlorofluoromethane NA SQl SQl 5 SQl 1,1-Dichloroethene 7 SQl SQl SQl SQl Xylenes (Total) 10000 SQl SQl SQl SQl Vinyl chloride 2 SQl SQl SQl SQl SQl - Selow quantification level MCl - Maximum Contaminant level per Georgia EPD Rule Chapter 391-3-5; NA - None available 1Metals concentrations in mg/l 20rganics concentrations in ug/l or ppb Indicates exceedance of MCl Page 1 of6

Table 7 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #2 Summary of Detected Parameters September 2002 CONSTITUENT Metals1 WEll SAMPLES MCl GWA-2/MW-2 GWC-3/MW-3 GWS-4/MW-4 GWC-11/MW-11 Sarium Zinc Organics2 1,1-Dichloroethane Chlorobenzene 1,4-Dichlorobenzene Methylene chloride cis-1,2-Dichloroethene Trichlorofluoromethane 1,1-Dichloroethene Xylenes (Total) Vinyl chloride 2 NA NA 100 75 5 70 NA 7 10000 2 SOL SOL 0.021 0.020 SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL - Selow quantification level MCl - Maximum Contaminant level per Georgia EPD Rule Chapter 391-3-5; NA - None available 1Metals concentrations in mg/l 20rganics concentrations in ug/I or ppb Indicates exceedance of MCl Page 2 of6

Table 7 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #2 Summary of Detected Parameters October 2002 CONSTITUENT MCL WELL SAMPLES GWA-2/MW-2 GWC-3/MW-33 GWS-4/MW-4 GWC-11/MW-11 Metals1 Sarium 2 SOL NS 0.021 0.025 Zinc NA SOL NS SOL SOL Organics2 1,1-Dichloroethane NA SOL NS SOL SOL Chlorobenzene 100 SOL NS SOL SOL 1A-Dichlorobenzene 75 SOL NS SOL SOL Methylene chloride 5 SOL NS SOL SOL cis-1,2-Dichloroethene 70 SOL NS SOL SOL Trichlorofluoromethane NA SOL NS SOL SOL 1,1-Dichloroethene 7 SOL NS SOL SOL Xylenes (Total) 10000 SOL NS SOL SOL Vinyl chloride 2 SOL NS SOL BOL BOL - Below quantification level MCl - Maximum Contaminant Level per EPD Rule Chapter 391-3-5; NA - None available 1Metals concentrations in mg/L 20rganics concentrations in ug/I or ppb 3Dry well, not sampled (NS) Indicates exceedance of MCL Page 3 of6

CONSTITUENT Metals1 Table 7 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #2 Summary of Detected Parameters December 2002 M WELL SAMPLES CL GWA-2/MW-2 GWC-3/MW-3 GWS-4/MW-4 GWS-4/MW-43 GWC-11/MW-11 Sarium Zinc Organics2 1,1-Dichloroethane Chlorobenzene 1,4-Dicholorbenzene Methylene chloride cis-1,2-Dichloroethene Trichlorofluoromethane 1,1-Dichloroethene Xylenes (Total) Vinyl chloride 2.00 NA NA 100 75 5 70 NA 7 10000 2 0.015 0.020 0.021 0.020 0.018 SOL 0.047 SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL - Selow quantification level MCL - Maximum Contaminant Level per EPD Rule Chapter 391-3-5; NA - None available 1Metals concentrations in mg/L 20rganics concentrations in ug/l or ppb 3Replicate sample of GWS-4/1MW-4 well Indicates exceedance of MCL Page 4 of6

Table 7 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #2 Summary of Detected Parameters June 2003 CONSTITUENT Metals1 WEll SAMPLES MCl GWA-2/MW-2 GWC-3/MW-3 GWS-4/MW-4 GWC-11/MW-11 Sarium Zinc Organics2 1,1-Dichloroethane Chlorobenzene 1,4-Dicholorbenzene Methylene chloride cis-1,2-Dichloroethene Trichlorofluoromethane 1,1-Dichloroethene Xylenes (Total) Vinyl chloride 2.00 NA NA 100 75 5 70 NA 7 10000 2 Sal NS Sal Sal Sal NS Sal 0.029 Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal NS Sal Sal Sal - Selow quantification level MCl - Maximum Contaminant level per EPD Rule Chapter 391-3-5; NA - None available NS - Not sampled; well dry 1Metals concentrations in mg/l 20rganics concentrations in ug/l or ppb Indicates exceedance of MCl Page 50f6

Table 7 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #2 Summary of Detected Parameters December 2003 CONSTITUENT Metals1 WEll SAMPLES MCl GWA-2/MW-2 GWC-3/MW-3 GWS-4/MW-4 GWC-11/MW-11 Sarium Zinc Organics2 1,1-Dichloroethane Chlorobenzene 1,4-Dicholorbenzene Methylene chloride cis-1,2-Dichloroethene Trichlorofluoromethane 1,1-Dichloroethene Xylenes (Total) Vinyl chloride 2.00 NA NA 100 75 5 70 NA 7 10000 2 Sal Sal Sal 0.022 Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal 6 Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal - Selow quantification level MCl - Maximum Contaminant level per EPD Rule Chapter 391-3-5; NA - None available NS - Not sampled; well dry 1Metals concentrations in mg/l 20rganics concentrations in ug/l or ppb Indicates exceedance of MCl Page 6 of6

Table 8 Southern Nuclear Operating Company Plant Vogtle Landfill #3 Summary of Detected Parameters July 2002 CONSTITUENT MCl WEllS1 GWC-5IMW-5 GWS-6/MW-6 GWA-7/MW-7 GWA-7-2JMW-7-23 GWC-13/MW-13 GWC-14/MW-14 GWA-15/MW-15 Metals1 Sarium 2 Sal Sal Sal Sal 0.077 0.068 Sal Zinc NA Sal Sal Sal Sal Sal Sal Sal Organics2 1,1-Dichloroethane NA Sal Sal Sal Sal Sal 13 Sal Chlorobenzene 100 Sal Sal Sal Sal Sal Sal Sal 1A-Dichlorobenzene 75 Sal Sal Sal Sal Sal 20 Sal Methylene chloride 5 Sal cis-1,2-Dichloroethene 70 Sal Sal Sal Sal Sal 10 Sal Trichlorofluoromethane NA Sal Sal 177 192 300 43 Sal 1,1-Dichloroethene 7 Sal Sal Sal Sal Sal Sal Sal Xylenes (Total) 10000 Sal Sal Sal Sal Sal 8 Sal Vinyl chloride 2 Sal Sal Sal Sal Sal Sal Sal Sal - Selow quantification level MCl - Maximum Contaminant level per Georgia EPD Rule Chapter 391-3-5; NA - None available 1Metals concentrations in mg/l 20rganics concentration units in ug/l or ppb 3Replicate sample of GWA-7/MW-7 well sample .e i_Indicates exceedance of Mel Page 1 of6

Table 8 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #3 Summary of Detected Parameters September 2002 CONSTITUENT MCL WELL SAMPLES GWC-51MW-5 GWS-6/MW-6 GWA-7IMW-7 GWC-13IMW-13 GWC-141MW-14 GWC-14-2IMW-14-23 GWA-15IMW-15 Metals' Sarium 2 0.020 SaL saL 0.085 0.092 0.095 saL Zinc NA SaL saL saL 0.023 saL saL saL Organics2 1,1-DiChloroethane NA saL saL saL 6 21 21 saL Chlorobenzene 100 saL saL saL saL 8 8 saL l,4-Dichlorobenzene 75 saL saL saL saL 37 36 saL Methylene chloride 5 SaL saL saL saL saL saL saL cis-l,2-Dichloroethene 70 saL saL saL saL 19 18 saL Trichlorofluoromethane NA saL saL 32 381 47 48 saL 1,1-Dichloroethene 7 saL saL saL saL Xylenes (Total) 10000 SaL saL saL saL 23 23 saL Vinyl chloride 2 SaL saL saL saL saL - saL saL - Selow quantification level MCL - Maximum Contaminant Level per Georgia EPD Rule Chapter 391-3-5; NA - None available 'Metals concentrations in mglL 20rganics concentration units in ugn or ppb 3Replicate sample ot GWS-14/1MW-14 well sample Ifll:~****** lndlicates exceedance ot MCL Page 20t6

Table 8 (continued) Southern Nuclear OperatIng Company Plant Vogtle Landfill #3 Summary of Detected Parameters October 2002 CONSTITUENT MCl WEll SAMPLES GWC-5IMW-5 GWS-6/MW-6 GWA-7/MW-7 GWC-13/MW-13 GWC-14/MW-14 GWA-15/MW-15 GWA-15-21MW-15-23 Metals' Sarium SOL SOL SOL 0.083 0.064 SOL SOL Zinc SOL SOL SOL 0.027 SOL SOL SOL Organics2 1,1-Dichloroethane NA SOL SOL SOL 6 17 SOL SOL Chlorobenzene 100 SOL SOL SOL SOL 9 SOL SOL 1,4-Dicholorbenzene 75 SOL SOL SOL SOL 35 SOL SOL Methylene chloride 5 SOL SOL SOL SOL - SOL SOL cis-l,2-Dichloroethene 70 SOL SOL SOL SOL 16 SOL SOL Trichlorofluoromethane NA SOL SOL 221 348 31 SOL SOL 1,1-Dichloroethene 7 SOL SOL SOL SOL SOL SOL SOL Xylenes (Total) 10000 SOL SOL SOL SOL 11 SOL SOL Vinyl chloride 2 SOL SOL SOL SOL SOL SOL SOL SOL - Selow quantification level MCl - Maximum Contaminant level per EPD Rule Chapter 391-3-5; NA - None available 'Metals concentrations in mg/l 20rganics concentration units in ugll or ppb 3Replicate sample of GWA-15/IMW-15 well 11******1 Indicates exceedance of MCl Page 3 of6

Table 8 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #3 Summary of Detected Parameters December 2002 CONSTITUENT Metals1 MCl WEll SAMPLES GWC-5/MW-5 GWS-6/MW-6 GWA-7/MW-7 GWC-13/MW-13 GWC-14/MW-14 GWA-15/MW-15 Sarium Zinc 2.00 NA 0.018 SOL SOL SOL 0.015 SOL 0.082 0.027 0.106 SOL SOL SOL Organics2 1,1-Dichloroethane NA SOL SOL SOL 7 16 SOL Chlorobenzene 100 SOL SOL SOL SOL 10 SOL 1,4-Dicholorbenzene 75 SOL SOL SOL SOL 39 SOL Methylene chloride 5 SOL SOL SOL SOL SOL SOL cis-1,2-Dichloroethene 70 SOL SOL SOL SOL 19 SOL Trichlorofluoromethane NA SOL SOL 210 391 27 SOL 1,1-Dichloroethene 7 SOL SOL SOL SOL Xylenes (Total) 10000 SOL SOL SOL SOL 21 SOL Vinyl chloride 2 SOL SOL SOL SOL SOL Chloroform3 0.1 SOL SOL SOL 5 SOL SOL SOL - Selow quantification level MCl - Maximum Contaminant level per EPD Rule Chapter 391-3-5; NA - None available 1Metals concentrations in mg/l 20rganics concentration units in ug/l or ppb 3Applies only to Community Water Systems serving 10,000 Indicates exceedance of MCl Page 4 of6

Table 8 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #3 Summary of Detected Parameters June 2003 CONSTITUENT MCl WEll SAMPLES GWC-5/MW-5 GWS-6/MW-6 GWA-7/MW-7 GWC-13/MW-13 GWC-13/MW-135 GWC-14/MW-14 GWA-15/MW-15 Metals' Sarium 2.00 Sal Sal 0.036 0.029 0.030 0.051 Sal Zinc NA Sal Sal 0.034 Sal Sal Sal Sal Copper 1.3 Sal Sal 0.035 Sal Sal Sal Sal Mercurl 0.002 NA NA NA 0.0005 0.0005 - Sal Organics2 1,1-Dichloroethane NA Sal Sal Sal 9 9 10 Sal Chlorobenzene 100 Sal Sal Sal Sal Sal 7 Sal 1,4-Dicholorbenzene 75 Sal Sal Sal Sal Sal 16 Sal Methylene chloride 5 Sal Sal Sal Sal Sal Sal Sal cis-1,2-Dichloroethene 70 Sal Sal Sal 6 6 10 Sal Trichlorofluoromethane NA Sal Sal 23 41 47 5 Sal 1,1-Dichloroethene 7 Sal Sal Sal Sal Sal Sal Sal Xylenes (Total) 10000 Sal Sal Sal Sal Sal Sal Sal Vinyl chloride 2 Sal Sal Sal Sal Sal Sal Sal Chloroform3 0.1 Sal Sal Sal Sal Sal Sal Sal Sal - Selow quantification level MCl - Maximum Contaminant level per EPD Rule Chapter 391-3-5; NA - None Available or Not Analyzed 'Metals concentrations in mg/l 20rganics concentration units in ugll or ppb 3Applies only to Community Water Systems serving 10,000 'Appendix 1\\ parameter; NA reflects that this parameter was not analyzed for those wells not included in the Assessment Monitoring Program 5Replicate sample of well GWC-13/MW-13 sample Nill!lli~IlI¥J***** lndicates exceedance of MCl Page 5 of6

Table 8 (continued) Southern Nuclear Operating Company Plant Vogtle Landfill #3 Summary of Detected Parameters December 2003 CONSTITUENT MCL WELL SAMPLES GWC-5/MW-5 GWS-6/MW-6 GWA-7/MW-7 GWC-13/MW-13 GWC-13/MW-135 GWC-14/MW-14 GWA-15/MW-15 Metals1 Sarium 2.00 0.142 SOL SOL 0.033 0.032 0.169 SOL Zinc NA 0.032 SOL 0.023 SOL SOL 0.127 SOL Copper 1.36 0.025 SOL SOL SOL SOL 0.026 SOL Mercury' 0.002 SOL SOL SOL SOL SOL - SOL Chromium (total) 0.1 0.026 SOL SOL SOL SOL 0.091 SOL Seryllium 0.004 SOL SOL SOL SOL SOL 0.004 SOL Cadmium 0.005 SOL SOL SOL SOL SOL - SOL Nickel NA SOL SOL SOL SOL SOL 0.034 SOL Lead 0.0156 SOL SOL SOL SOL SOL 0.015 SOL Vanadium NA SOL SOL SOL SOL SOL 0.060 SOL Organics2 1,1-Dichloroethane NA SOL SOL SOL 20 21 10 SOL Chlorobenzene 100 SOL SOL SOL SOL SOL 19 SOL 1,4-Dicholorbenzene 75 SOL SOL SOL SOL SOL 33 SOL Methylene chloride 5 SOL SOL SOL SOL SOL SOL SOL cis-1,2-Dichloroethene 70 SOL SOL SOL 14 14 17 SOL Trichlorofluoromethane NA SOL SOL 34 102 97 SOL SOL 1,1-Dichloroethene 7 SOL SOL SOL SOL SOL SOL SOL Xylenes (Total) 10000 SOL SOL SOL SOL SOL 10 SOL Vinyl chloride 2 SOL SOL SOL SOL SOL SOL SOL Chloroform) 0.1 SOL SOL SOL SOL SOL SOL SOL SOL - Selow quantification level MCL - Maximum Contaminant Level per EPD Rule Chapter 391-3-5; NA - None Available or Not Analyzed lMetals concentrations in mg/L 20rganics concentration units in ugll or ppb )Applies only to Community Water Systems serving 10,000 4Appendix II parameter; NA reflects that this parameter was not analyzed for those wells not included in the Assessment Monitoring Program 5Replicate sample of well GWC-13/MW-13 sample 6Action Level IIIIl!11 _Indicates exceedance of MCL Page 6 of6

FIGURES

ApPENDIX A - LABORATORY ANALYTICAL REPORTS

LANDFILL #2

ADVANCED CHEMISTRY LABS, INC. IACL I Phone: (770) 40~9~-1~4:":'4~4----------------~30~3~9~A:-m-w-:i:-le-r

'Ro-a-d~*-::S:-u~ite~10~0~*-:A~tl:-an-:t-a,-:G~A~3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: ac/@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 V.O. (50308/82608)

  • Appendix I GWA-21MW-2 Sample 10:

ACL Sample #: 210466 Analyte Acetone Acrylonitrile Senzene Sromochloromethane Sromodichloromethane Bromoform ""-'rbon disulfide ..bon tetrachloride Chlorobenzene Chloroethane Chloroform 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane trans-1,4-Dichloro-2-butene 1,2-Dichlorobenzene 1A-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1.2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 2-Hexanone Methyl bromide Methyl chloride Methyl ethyl ketone .~ethyl iodide 1ethyl-2-pentanone BOl = Below Quanlilalion lim~ J =less than Ouantitation llmiL Approximate Value POL =Practical Quantilation limit Units: Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal /Jg/L PQL 100 50 5 5 5 5 5 5 5 10 5 20 5 5 10 5 5 5 5 5 5 5 5 5 5 5 50 10 10 100 5 50 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Analyte Methylene bromide Methylene chloride Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m & p-Xylenes o-Xylene Water 12/1712003 12/30/2003 RP Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal PQL 5 5 5 5 5 5 5 5 5 5 5 5 50 2 10 5

ADVANCED CHEMISTRY LABS, INC. !ACL I Phone: (770) 40~9~-1~4:":'4":"4----------------~30~3~9-:A~m-w~i1:-er-:R::"o-a-:d:-*"'::S~u~ite~10~O:-*-:A~t1-an~ta-,~G~A~30~3~6~O-Fax: (770) 409-1844 P.O. Box 88610

  • Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004

Contact:

Mr. Mark Mitchell V.o. (50308/82608)

  • Appendix I PQL 5

5 5 5 5 5 5 5 5 5 5 5 50 2 10 5 Result BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl Sal Sal Sal BOl Sal Water 12/17/2003 12130/2003 RP Analvte Methylene bromide Methylene chloride Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m & p-Xylenes o-Xylene GWC-3/MW-3 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Sample 10: ACL Sample #: 210467 Units: IJg/L Analvte Result PQL Acetone BOl 100 Acrylonitrile BOl 50 Benzene BOl 5 Bromochloromethane BOl 5 Bromodichloromethane BOl 5 Bromoform BOl 5 "'arbon disulfide BOl 5 ..;arbon tetrachloride BOl 5 Chlorobenzene BOl 5 Chloroethane BOl 10 Chloroform BOl 5 1,2-Dibromo-3-chloropropane BOl 20 Dibromochloromethane BOl 5 1,2-Dibromoethane BOl 5 trans-1,4-Dichloro-2-butene BOl 10 1,2-Dichlorobenzene BOl 5 1,4-Dichlorobenzene BOl 5 1,1-Dichloroethane BOl 5 1,2-Dichloroethane BOl 5 1,1-Dichloroethene BOl 5 cis-1,2-Dichloroethene BOl 5 trans-1,2-Dichforoethene BOl 5 1,2-Dichloropropane BOl 5 cis-1,3-Dichloropropene BOl 5 trans-1,3-Dichloropropene BOl 5 Ethylbenzene BOl 5 2-Hexanone BOl 50 Methyl bromide BOl 10 Methyl chloride BOl 10 Methyl ethyl ketone BOl 100 Methyl iodide BOl 5 -Methyl-2-pentanone BOl 50 BOL =Below Quanlilation Llm~ J =Less than Ouantilalion Limit, Approximate Value POL =Practical Ouanlilation LIm~

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9-.1-4-4-4----------------'!"30~3~9~A~m-w~i1~e~r R~o-a~d-*~S~u~ite-10!"""0-*~A"t1-an-ta-,-G!""'A--30"!"'3!"""6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/1912003 01/06/2004 v.o. (50308/82608)

  • Appendix I GWB-4/MW-4 SamplelD:

ACL Sample #: 210468 Analyte Acetone Acrylonitrile Senzene Sromochloromethane Sromodichloromethane Sromoform -'arbon disulfide ,arbon tetrachloride Chlorobenzene Chloroethane Chloroform l,2-Dibromo-3-chloropropane Dibromochloromethane l,2-Dibromoethane trans-1,4-Dichloro-2-butene 1,2-Dichlorobenzene . 1A-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 2-Hexanone Methyl bromide Methyl chloride Methyl ethyl ketone _!v1ethyt iodide Methyl-2-pentanone SOL =Below Quantilation limit J =less than OuantUtion limit. Approximate Value POL =Practical Ouanlitalion limit Units: Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal SOL Sal Sal Sal SOL Sal SOL SOL SOL SOL SOL Sal SOL SOL SOL Sal ~g/L PQL 100 50 5 5 5 5 5 5 5 10 5 20 5 5 10 5 5 5 5 5 5 5 5 5 5 5 50 10 10 100 5 50 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Analyte Methylene bromide Methylene chloride Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m & p-Xylenes o-Xylene Water 12/1712003 1213012003 RP Result Sal SOL SOL SOL SOL SOL SOL SOL SOL Sal 6 SOL SOL SOL SOL SOL PQL 5 5 5 5 5 5 5 5 5 5 5 5 50 2 10 5

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40~9~-1~44:"":"":"4----------------"='30~3~9~Am~Wl"':"~le-r R~o-a~d~*~S~u':':"ite~10~0~*~A~t1~an"':'ta-,"':'G~A~3~03~6~O-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acf-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 v.o. (5030B/8260B)

  • Appendix I GWC-11/MW-11 Sample 10:

ACl Sample #: 210472 Analyte Acetone Acrylonitrile Senzene Sromochloromethane Sromodichloromethane Sromoform 'ubon disulfide ....arbon tetrachloride Chlorobenzene Chloroethane Chloroform 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane trans-1,4-Dichloro-2-butene 1,2-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 2-Hexanone Methyl bromide Methyl chloride Methyl ethyl ketone ..Methyl iodide Methyl-2-pentanone BQL =Below QuanUlalion Limit J =Less than Quanlitalion LimK. ApPIOximate Value POL =Practical Quanlitation LimK Units: Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal IJg/L PQl 100 50 5 5 5 5 5 5 5 10 5 20 5 5 10 5 5 5 5 5 5 5 5 5 5 5 50 10 10 100 5 50 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Analyte Methylene bromide Methylene chloride Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m &p-Xylenes o-Xylene Water 12/1712003 12/30/2003 RP Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal PQl 5 5 5 5 5 5 5 5 5 5 5 5 50 2 10 5

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 409-~1~4~44~--------------~3~03~9~A!"""m-w~il-er~R~o-ad~* S~u~ite~10~0-.""!'A""tla-n-ta-. ~GA~3"!"03'!""!6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Miscellaneous Organics (504.1)

  • AppendiX II ACl Sample #: 210466 Units:

~g/L Analvte Result PQl 1.2.0ibromo-3-chloropropane SQL 0.20 1.2-0ibromoethane SQL 0.05 Sample 10: GWA-21MW-2 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/23/2003 Date Analyzed: 12130/2003 Analyst: SS SOL =Below Quantitation Linlt J =less than Ouantilallon Linit. APllfOximale Value POL =Practical Ouanlitatlon limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9-~1~44"':"'4~-----------~--"":3~03~9~A~m-w":':i1-er"":R~o-ad":".~S~u~lt-e ~10~O~*"":'A~t1a-n":"ta-, ~GA~30~3:-:6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemlstrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080~0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Miscellaneous Organics (504.1) - Appendix II ACL Sample #: 210467 Units: 1J9/L Analyte Result PQL 1,2-Dibromo-3-chloropropane Sal 0.20 1,2-Dibromoethane Sal 0,05 Sample 10: GWC-3/MW-3 Matrix: Water Date Sampled: 12/1712003 Date Extracted: 12/23/2003 Date Analyzed: 12/30/2003 Analyst: SS BQl =Below Quanlilatlon limit J.. Less than Quanlilatlon linit. ADDroxmale Value POL=Practical Quant\\lalion Limit ~-~--------- ---- _._--


~--------------- ----- -

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1~4"':"44~--------------""'::3~0~39~A~m-w~iI~er""'::R~o-a"':"d -.S:"u~it~e"':"10~0~.""'::A~tla-n"':"ta-,~G~A""'::3~0~36~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACL Sample #: 210468 Units:

J.lg/L AnaIvte Result PQL 1,2-Dibromo-3-chloropropane Sal 0.20 1,2-Dibromoethane Sal 0.05 Sample 10: GWB-4/MW-4 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/23/2003 Date Analyzed: 01/0212004 Analyst: SS BQl =Below Quanlilation limit J =less than Quantltatlon limit. ADOroximate Value pal =Pradical Ouantilallon limit

IA CL 1~~ A_D_V;_~_N~C~'E~'D~c:--'H~"E-:-'M-='L~'S-:-TR~Y-:-L~A-:-B-:,S~, l~'N~C_. Phone: (770) 409-1444 3039 Amwiler Road* Suite 100* Atlanta. GA 30360 Fax: (770) 409*1844 P.O. Box 88610* Atlanta. GA 30356 a-mail: acl@acl-labs.net www.advancedchamistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client ProJ #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACl Sample #: 210472 Units:

IJg/L Analyte Result PQl 1,2-Dibromo-3-chloropropane SQl 0.20 1,2-Dibromoethane SQl 0.05 Sample 10: GWC-11/MW-11 Matrix: Water Date Sampled: 12117/2003 Date Extracted: 12/23/2003 Date Analyzed: 01/0212004 Analyst: SS BOl " Below Quantilalion lim~ J " less than Ouantilalion Limit, Approximate Value PQl"P~akaIO~mml~

ADVANCED CHEMISTRY LABS, INC. IACL I Phone: (770) 409~-1~4"":"44~--------------~3~O~39~A~m-w~il~er~R~o-a"":"d-' S~u~it-e"":"10~O~'~A~t1-an-ta-.~G"":"A~3~0~36~O-Fax: (770) 409-1844 P.O. Box 88610' Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (60108/7841) ACL Sample #: 210466 Units: mg/L Analvte Result PQL Antimony BOl 0.006 Arsenic BOl 0.010 Barium BOl 0.020 Beryllium BOL 0.004 Cadmium BOL 0.005 Chromium BOL 0.020 ~obalt BOL 0.050 .;opper BOL 0.020 lead BOL 0.010 Nickel BOl 0.020 Selenium BOL 0.040 Silver BOl 0.010 Thallium BOl 0.002 Vanadium BOL 0.050 Zinc BOL 0.020 Sample ID: GWA-21MW-2 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12130/2003 SW/AD BQl =Below Quanlitation Linit J =less than Quantitation limit. AllD/OXimate Value PQl =Practical Quantitalion limit


~--- ---- ----

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9-.1~44"!"4~--------------""'!3~0~39~A~m-W-il~er""'!R~o-a""!"d-. S~u""!"it-e""!"10""0-*-A-tla-n-ta-.~G-A-3~O""36"'0-Fax: (770) 409-1844 P.O. Box 88610

  • Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (60108/7841) ACl Sample #: 210467 Units: mg/l Analyte Result PQl Antimony Sal 0.006 Arsenic Sal 0.010 Sarium Sal 0.020 Seryllium Sal 0.004 Cadmium Sal 0.005 Chromium Sal 0.020 '~obalt Sal 0.050 opper Sal 0.020 lead Sal 0.010 Nickel Sal 0.020 Selenium Sal 0.040 Silver Sal 0.010 Thallium Sal 0.002 Vanadium Sal 0.050 Zinc Sal 0.020 Sample 10: GWC-3/MW-3 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12/30/2003 SW/AD BQl,. Below Quantilalion limit J =less than Quanlilalion LimiL Approxinate Value PQl,. Praclical QuanlDlion limit

IACL I Phone: (770) 409-1444 Fax: (770) 409*1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRYLABS, INC. 3039 Amwiler Road' Suite 100

  • Atlanta. GA 30360 P.O. Box 88610' Atlanta. GA 30356 www.advancedchemistrylabs.com Client:

Contact:

. Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 ACL Sample #: 210468 Units: mg/L Analvte Result PQL Antimony Sal 0.006 Arsenic Sal 0.010 Sarium Sal 0.020 Seryllium Sal 0.004 Cadmium Sal 0.005 Chromium Sal 0.020 'obalt Sal 0.050 ...opper Sal 0.020 lead Sal 0.010 Nickel Sal 0.020 Selenium Sal 0.040 Silver Sal 0.010 Thallium Sal 0.002 Vanadium Sal 0.050 Zinc Sal 0.020 Sample 10: Appendix I Metals (60108/7841) GWB-4/MW-4 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12/30/2003 SW/AD BOl =Below Quanlitalion limit J =less than Ouantilation Linit. AoDroxlmate Value POL =Practical Ouantilation limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~.1~44"":"4~--------------~3~0~39~Am~w~i1:-er~R~o-a~d-. ~Su~it:-e~1~00~*~A~t1~an-ta-.~GA~3~0~36~0~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (6010B/7841) ACL Sample #: 210472 Units: mg/L Analyte Result PQL Antimony BOl 0.006 Arsenic BOl 0.010 Barium 0.022 0.020 Beryllium BOl 0.004 Cadmium Sal 0.005 ~. Chromium Sal 0.020 'obalt Sal 0.050 Copper Sal 0.020 lead BOL 0.010 Nickel Sal 0.020 Selenium SOL 0.040 Silver SOL 0.010 Thallium SOL 0.002 Vanadium Sal 0.050 Zinc SOL 0.020 Sample ID: GWC-11/MW-11 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/1712003 12130/2003 SW/AD BOl =Below Quantitation lim~ J =less than Quanlitation limit, Approximate Value POL =Practical Ouantitation limit ~---- ~ .~ ~~--' _.~---

LANDFILL #3

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1:-:4~4~4----------------~30~3~9~A~m-w~i1~er~R~o-a~d~*-:S~u~ite~1 0~0-.~A~t1-an~ta-,~G~A~30~3~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client: Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004

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Mr. Mark Mitchell V.O. (5030B/8260B) - Appendix I PQL 5 5 5 5 5 5 5 5 5 5 5 5 50 2 10 5 Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal 12/30/2003 RP Water 12/16/2003 Analvte Methylene bromide Methylene chloride Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-TriChloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m & p-Xylenes o-Xylene GWC-5/MW-5 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Sample 10: ACL Sample #: 210469 Units: IJg/L Analvte Result PQL Acetone Sal 100 Acrylonitrile Sal 50 Senzene Sal 5 SromochJoromethane Sal 5 Sromodichloromethane Sal 5 Sromoform Sal 5 'arbon disulfide Sal 5 ....arbon tetrachloride Sal 5 Chlorobenzene Sal 5 Chloroethane Sal 10 Chloroform Sal 5 1,2-Dibromo-3-chloropropane Sal 20 Dibromochloromethane Sal 5 1,2-Dibromoethane Sal 5 trans-1,4-Dichloro-2-butene Sal 10 1,2-Dichlorobenzene Sal 5 1A-Dichlorobenzene Sal 5 1,1-Dichloroethane Sal 5 1.2-Dichloroethane Sal 5 1,1-Dichloroethene Sal 5 cis-1,2-Dichloroethene Sal 5 trans-1,2-Dichloroethene Sal 5 1,2-Dichloropropane Sal 5 cis-1,3-Dichloropropene Sal 5 trans-1,3-Dichloropropene Sal 5 Ethylbenzene Sal 5 2-Hexanone Sal 50 Methyl bromide Sal 10 Methyl chloride Sal 10 Methyl ethyl ketone Sal 100 _Methyl iodide Sal 5

  • MethyI-2-pentanone Sal 50 BOL =Below Quantitalion Limit J =less than Ouanlitalion Limit. Approximale Value POL =Practical Ouanlitalion limit

IA CL 1~~ A_D_VA_N~C~'E~'D~CH~'E_'M~1.~S_T~'R_Y~LA_B~S.....,~IN~C_. Phone: (770) 409-1444 3039 Amwiler Road* Suite 100* Atlanta. GA 30360 Fax: (770) 409-1844 P.O. Box 88610

  • Atlanta. GA 30356 a-mail: acl@acl-fabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 V.O. (50308/82608)

  • Appendix I GWB-6/MW-6 Sample 10:

ACL Sample #: 210470 Analvte Acetone Acrylonitrile Senzene Sromochloromethane Sromodichloromethane Sromoform lrbon disulfide ....arbon tetrachloride Chlorobenzene Chloroethane Chloroform 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane trans-1,4-Dichloro-2-butene 1,2-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1.2-Dichloroethane 1.1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1.3-Dichloropropene trans-1.3-Dichloropropene Ethylbenzene 2-Hexanone Methyl bromide Methyl chloride Methyl ethyl ketone ,..Methyl iodide Methyl-2-pentanone eOl " Below Quanlilation limij J "less !han Ouantilation limit. Approximate Value pal" Practical Ouantllalion limit Units: Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal ~g/L PQL 100 50 5 5 5 5 5 5 5 10 5 20 5 5 10 5 5 5 5 5 5 5 5 5 5 5 50 10 10 100 5 50 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Analvte Methylene bromide Methylene chloride Styrene 1.1.1.2-Tetrachloroethane 101,2.2-Tetrachloroethane Tetrachloroethene Toluene 1.1 0i-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1.2,3-Trichloropropane Vinyl acetate Vinyl chloride m & p-Xylenes o-Xylene Water 12/17/2003 12/30/2003 RP Result Sal Sal Sal Sal Sal Sal Sal Sal Sal SOL Sal Sal SOL Sal Sal Sal PQL 5 5 5 5 5 5 5 5 5 5 5 5 50 2 10 5

ADVANCED CHEMISTRY LABS, INC. IACL I Phone: (770) 40~9-.1~4~44~-----~---------~30~3~9~A~m-w~il~er~R~o-a~d-*~S~u~jte~10~0-*~A-'t1-an-ta-.~G~A~30~3~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 v.o. (50308/82608)

  • Appendix I GWA-7/MW-7 Sample ID:

ACL Sample #: 210471 Analvte Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform - 1rbon disulfide Jrbon tetrachloride Chlorobenzene Chloroethane Chloroform 1,2-Dibromo-3-chloropropane Dibromochloromethane 1.2-Dibromoethane trans-1.4-Dichloro-2-butene 1,2-Dichlorobenzene 1A-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 2-Hexanone Methyl bromide Methyl chloride Methyl ethyl ketone ,jv1ethyl iodide V1ethyl-2-pentanone BOl =Below Quanlilalion lim~ J =less than Quantilalion Liml ADDroximale Value PQl =Practical Quanlilalion limit Units: Result SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL BOL SOL SOL SOL BOL SOL SOL SOL SOL SOL SOL SOL SOL BOL SOL SOL BOL Sal Sal SOL SOL IJg/L POL 100 50 5 5 5 5 5 5 5 10 5 20 5 5 10 5 5 5 5 5 5 5 5 5 5 5 50 10 10 100 5 50 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Analvte Methylene bromide Methylene chloride Styrene 1.1.1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m & p-Xylenes o-Xylene Water 12/16/2003 12/30/2003 RP Result SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL 34 Sal Sal SOL Sal SOL POL 5 5 5 5 5 5 5 5 5 5 5 5 50 2 10 5

IACL I Phone: (770) 409-1444 Fax: (770) 409-1644 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRY LABS, INC. 3039 Amwiler Road* Suite 100* Atlanta, GA 30360 P.O. Box 88610* Atlanta, GA 30356 www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant VogUe 44014 12/19/2003 01/06/2004 v.o. (5030B/8260B)

  • Appendix II Sample 10:

GWC-13/MW-13 Matrix: Water Date Sampled: 12/16/2003 Date Extracted: Date Analyzed: 12/29/2003 ACl Sample #: 210461 Units: IJg/l Analyst: RP Analvte Result PQl Analvte Result PQl Acetone Sal 100 cis-1,3-Dichloropropene Sal 5 Acetonitrile Sal 100 trans-1,3-Dichloropropene Sal 5 Acrolein Sal 100 Ethyl methacrylate Sal 10 Acrylonitrile Sal 50 Ethylbenzene Sal 5 Allyl chloride Sal 10 2-Hexanone Sal 50 Senzene Sal 5 Isobutyl alcohol Sal 50 'romochloromethane Sal 5 Methacrylonitrile Sal 100 Jromodichloromethane Sal 5 Methyl bromide Sal 10 Sromoform Sal 5 Methyl chloride Sal 10 Carbon disulfide Sal 5 Methyl ethyl ketone Sal 100 Carbon tetrachloride Sal 5 Methyl iodide Sal 5 Chlorobenzene Sal 5 Methyl methacrylate Sal 30 Chloroethane Sal 10 4-Methyl-2-pentanone Sal 50 Chloroform Sal 5 Methylene bromide Sal 5 Chloroprene Sal 20 Methylene chloride Sal 5 1,2-Dibromo-3-chloropropane Sal 20 Naphthalene Sal 5 Dibromochloromethane Sal 5 Propionitrile Sal 150 1,2-Dibromoethane Sal 5 Styrene Sal 5 trans-1,4-Dichloro-2-butene Sal 10 1,1,1,2-Tetrachloroethane Sal 5 1.2-Dichlorobenzene Sal 5 1,1,2,2-Tetrachloroethane Sal 5 1,3-Dichlorobenzene Sal 5 Tetrachloroethene Sal 5 1,4-Dichlorobenzene Sal 5 Toluene Sal 5 Dichlorodifluoromethane Sal 5 1,1,1-Trichloroethane Sal 5 1,1-Dichloroethane 20 5 1,1,2-Trichloroethane Sal 5 1,2-Dichloroethane Sal 5 Trichloroethene Sal 5 1.1-Dichloroethene Sal 5 Trichlorofluoromethane 102 5 cis-1,2-Dichloroethene 14 5 1,2,3-Trichloropropane Sal 5 trans-1,2-Dichloroethene Sal 5 Vinyl acetate Sal 50 1,2-Dichloropropane Sal 5 Vinyl chloride Sal 2 1,3-Dichloropropane Sal 5 m &p-Xylenes Sal 10 ~,2-Djchloropropane SOL 15 o-Xylene SOL 5 ,,1-Dichloropropene Sal 5 Jl~~.$ ~ BOl =Below Quantitalion limit J =less lhan Ouanlilalion limit. APDlOximale Value Markorios Digitally signed by Markorios MIdaIaIAdib.QNacMinaaer Adaire POL =Practical Ouanlitalion limit ON: CN =Markorios Adaire. C = Adafre-.- US, 0 =Advanced Chemistry let>s;!nc. Oata02OO4.03.04 16:46:36 -05'00'

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1~4~4~4----------------~30~3~9~A~m-w"":':il~er~R~o-a~d-*~S~u~ite~10~0~.~A~tl-an~ta-,~G~A~30~3~6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta. GA 30356 a-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 v.o. (50308/82608)

  • Appendix II Sample 10:

GWC-13/MW-13-(Dupe) Matrix: Water Date Sampled: 12/1612003 Date Extracted: Date Analyzed: 12/29/2003 ACL Sample #: 210462 Units: 1J9/L Analyst: RP Analvte Result PQL AnaIyte Result PQL Acetone SOL 100 cis-1,3-Dichloropropene SOL 5 Acetonitrile SOL 100 trans-1,3-Dichloropropene SOL 5 Acrolein SOL 100 Ethyl methacrylate SOL 10 Acrylonitrile SOL 50 Ethylbenzene SOL 5 Allyl chloride SOL 10 2-Hexanone SOL 50 Senzene SOL 5 Isobutyl alcohol SOL 50 ,romochloromethane SOL 5 Methacrylonitrile SOL 100 ..:lromodichloromethane Sal 5 Methyl bromide SOL 10 Sromoform Sal 5 Methyl chloride Sal 10 Carbon disulfide SOL 5 Methyl ethyl ketone SOL 100 Carbon tetrachloride SOL 5 Methyl iodide Sal 5 Chlorobenzene SOL 5 Methyl methacrylate SOL 30 Chloroethane SOL 10 4-Methyl-2-pentanone SOL 50 Chloroform SOL 5 Methylene bromide SOL 5 Chloroprene Sal 20 Methylene chloride SOL 5 1,2-Dibromo-3-chloropropane SOL 20 Naphthalene SOL 5 Dibromochloromethane SOL 5 Propionitrile Sal 150 1,2-Dibromoethane SOL 5 Styrene SOL 5 trans-1,4-Dichloro-2-butene SOL 10 1,1,1,2-Tetrachloroethane SOL 5 1,2-Dichlorobenzene SOL 5 1,1,2,2-Tetrachloroethane SOL 5 1.3-Dichlorobenzene Sal 5 Tetrachloroethene Sal 5 1A-Dichlorobenzene SOL 5 Toluene Sal 5 Dichlorodifluoromethane SOL 5 1,1,1-Trichloroethane SOL 5 1,1-Dichloroethane 21 5 1,1,2-Trichloroethane SOL 5 1.2-Dichloroethane SOL 5 Trichloroethene SOL 5 1,1-Dichloroethene SOL 5 Trichlorofluoromethane 97 5 cis-1,2-Dichloroethene 14 5 1,2,3-Trichloropropane SOL 5 trans-1,2-Dichloroethene SOL 5 Vinyl acetate SOL 50 1,2-Dichloropropane SOL 5 Vinyl chloride Sal 2 1,3-Dichloropropane SOL 5 m & p-Xylenes Sal 10 - 2,2-Dichloropropane SOL 15 o-Xylene Sal 5 ,,1-Dichloropropene SOL 5 eOL =Below Quanlilation Lillit J =Less than Ouantilation lina. Approximate Value POL =Practical Ouantilation lima

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40~9:--1~4:"':'4~4----------------~30~3~9~Am:--w-::lI:-er-:R::"o-a-:d-."'::S:-u~ite-1':"':0~0:-*-::A~t1a-n"':'ta-,~G~A~30~3~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 v.o. (5030B/8260B)

  • Appendix II Sample 10:

GWC-15/MW-15 Matrix: Water Date Sampled: 12117/2003 Date Extracted: Date Analyzed: 12/29/2003 ACL Sample #: 210463 Units: IJg/L Analyst: RP Analyte Result PQL Analvte Result PQL Acetone Sal 100 cis-1,3-Dichloropropene Sal 5 Acetonitrile Sal 100 trans-1,3-Dichloropropene Sal 5 Acrolein Sal 100 Ethyl methacrylate Sal 10 Acrylonitrile Sal 50 Ethylbenzene Sal 5 Allyl chloride Sal 10 2-Hexanone Sal 50 Senzene Sal 5 Isobutyl alcohol Sal 50 'omochloromethane Sal 5 Methacrylonitrile Sal 100 ,omodichloromethane Sal 5 Methyl bromide Sal 10 Sromoform Sal 5 Methyl chloride Sal 10 Carbon disulfide Sal 5 Methyl ethyl ketone Sal 100 Carbon tetrachloride Sal 5 Methyl iodide Sal 5 Chlorobenzene Sal 5 Methyl methacrylate Sal 30 Chloroethane Sal 10 4-Methyl-2-pentanone Sal 50 Chloroform Sal 5 Methylene bromide Sal 5 Chloroprene Sal 20 Methylene chloride Sal 5 1,2-Dibromo-3-chloropropane Sal 20 Naphthalene Sal 5 Dibromochloromethane Sal 5 Propionitrile Sal 150 1,2-Dibromoethane Sal 5 Styrene Sal 5 trans-1,4-Dichloro-2-butene eOl 10 1,1,1,2-Tetrachloroethane Sal 5 1,2-Dichlorobenzene Sal 5 1,1,2,2-Tetrachloroethane Sal 5 1,3-Dichlorobenzene Sal 5 Tetrachloroethene Sal 5 1A-Dichlorobenzene Sal 5 Toluene Sal 5 Dichlorodifluoromethane Sal 5 1,1,1-Trichloroethane Sal 5 1,1-Dichloroethane Sal 5 1,1,2-Trichloroethane Sal 5 1,2-Dichloroethane Sal 5 Trichloroethene Sal 5 1,1-Dichloroethene Sal 5 Trichlorofluoromethane Sal 5 cis-1,2-Dichloroethene Sal 5 1,2,3-Trichloropropane Sal 5 trans-1,2-Dichloroethene Sal 5 Vinyl acetate Sal 50 1,2-Dichloropropane Sal 5 Vinyl chloride Sal 2 1,3-Dichloropropane Sal 5 m & p-Xylenes Sal 10 .2,2-Dichloropropane Sal 15 o-Xylene Sal 5 l-Dichloropropene Sal 5 BOl =Below Ouantitalion lim~ J '" less than Ouantilalion limit. Approximate Value POL =Practical Ouantitation Limit

IACL I Phone: (770) 409-1444 Fax: (770) 409-1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRY LABS, INC. 3039 Amwiler Road* Suite 100

  • Atlanta. GA 30360 P.O. Box 88610* Atlanta, GA 30356 www.advancedchemistryfabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 v.o. (50308/82608)

  • Appendix II Sample 10:

GWC-14/MW-14 Matrix: Water Date Sampled: 12117/2003 Date Extracted: Date Analyzed: 12/30/2003 ACl Sample #: 210473 Units: IJg/L Analyst: RP Analvte Result PQl Analvte Result PQl Acetone Sal 100 cis-1,3-Dichloropropene Sal 5 Acetonitrile Sal 100 trans-1,3-Dichloropropene Sal 5 Acrolein Sal 100 Ethyl methacrylate Sal 10 Acrylonitrile Sal 50 Ethylbenzene Sal 5 Allyl chloride Sal 10 2-Hexanone Sal 50 Senzene Sal 5 Isobutyl alcohol Sal 50 )mochloromelhane Sal 5 Methacrylonitrile Sal 100 _,omodichloromethane Sal 5 Methyl bromide Sal 10 Sromoform Sal 5 Methyl chloride Sal 10 Carbon disulfide Sal 5 Methyl elhyl ketone Sal 100 Carbon tetrachloride Sal 5 Methyl iodide Sal 5 Chlorobenzene 19 5 Methyl methacrylate Sal 30 Chloroethane Sal 10 4-Methyl-2-pentanone Sal 50 Chloroform Sal 5 Methylene bromide Sal 5 Chloroprene Sal 20 Methylene chloride Sal 5 1,2-Dibromo-3-chloropropane Sal 20 Naphthalene Sal 5 Dibromochloromethane Sal 5 Propionitrile Sal 150 1,2-Dibromoethane Sal 5 Styrene Sal 5 trans-1,4-Dichloro-2-butene Sal 10 1,1,1,2-Tetrachloroethane Sal 5 1,2-Dichlorobenzene Sal 5 1,1,2,2-Tetrachloroethane Sal 5 1,3-Dichlorobenzene Sal 5 Tetrachloroethene Sal 5 1,4-Dichlorobenzene 33 5 Toluene Sal 5 Dichlorodifluoromethane Sal 5 1,1,1-Trichloroethane Sal 5 1,1-Dichloroethane 10 5 1,1,2-Trichloroethane Sal 5 1,2-Dichloroethane Sal 5 Trichloroethene Sal 5 1,1-Dichloroethene Sal 5 Trichlorofluoromethane Sal 5 cis-1,2-Dichloroethene 17 5 1,2,3-Trichloropropane Sal 5 trans-1,2-Dichloroethene Sal 5 Vinyl acetate Sal 50 1,2-Dichloropropane Sal 5 Vinyl chloride Sal 2 1,3-Dichloropropane Sal 5 m & p-Xylenes Sal 10 -2,2-Dichloropropane Sal 15 o-Xylene 10 5 1-Dichloropropene Sal 5 BOL =Below Ouantitalion Limit J =Less than Ouantilalion Lim~. Approximate Value POL =Practical Ouantilalion Limit

ADVANCED CHEMISTRY LABS, INC. IACL I Phone: (770) 40~9~-1~4~44-:----------------~3~0~3~9 "'!"A-m-w':"!"'i1e-r"=R~oa-d~*~S~u~ite~1 0~0~*~A~t1a-n"'!"ta-.~G~A-3~0~3~60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Acid Extractables (8270C)

  • Appendix II ACL Sample #: 210461 Units:

~g/L AnaIvte Result PQL 4-Chloro-3-methylphenol Sal 20 2-Chlorophenol Sal 10 m & p-Cresol Sal 10 o-Cresol Sal 10 2,4-Dichlorophenol Sal 10 2,6-Dichlorophenol Sal 10 "- 4-Dimethylphenol Sal 10 .o-Dinitro-2-methylphenol Sal 50 2,4-Dinitrophenol Sal 50 2-Nitrophenol Sal 10 4-Nitrophenol Sal 50 Pentachlorophenol Sal 50 Phenol Sal 10 2,3,4,6-Tetrachlorophenol Sal 10 2.4,5-Trichlorophenol Sal 10 2,4,6-Trichlorophenol Sal 10 Sample 10: GWC-13/MW-13 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/16/2003 12/2212003 12/23/2003 RB BOL =Below Ouantitalion Limit J =Less than Ouantltatlon Limit. Approximate Value POL =Practical Quanlilalion Limit

IACL I Phone: (770) 409-1444 Fax: (770) 409-1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRY LABS, INC. 3039 AmwiJer Road, Suite 100

  • Atlanta, GA 30360 P.O. Box 88610' Atlanta, GA 30356 www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II Sample 10:

GWC-13/MW-13 Matrix: Water Date Sampled: 12/1612003 Date Extracted: 12/22/2003 Date Analyzed: 12/23/2003 ACL Sample #: 210461 Units: IJg/L Analyst: RB Analvte Result PQL Analyte Result PQL Acenaphthene SOL 10 Diethyl phthalate Sal 10 Acenaphthylene SOL 10 Dimethoate Sal 10 Acetophenone SOL 10 Dimethyl phthalate Sal 10 2-Acetylaminofluorene Sal 20 p-(Dimethylamina)azobenzene Sal 10 4-Aminobiphenyl Sal 20 7,12-Dimethylbenz(a)anthracene Sal 10 Anthracene SOL 10 3,3'-Dimethylbenzidine Sal 10 -- 'nzo(a)anthracene Sal 10 m-Dinitrobenzene Sal 20 A~nzo(a )pyrene SOL 10 2,4-Dinitrotoluene Sal 10 Senzo(b)fluoranthene SOL 10 2,6-Dinitrotoluene Sal 10 Senzo(g,h,i)perylene Sal 10 Diphenylamine Sal 10 Senzo(k)fluoranthene SOL 10 Disulfoton SOL 10 Senzyl alcohol SOL 20 Ethyl methanesulfonate SOL 20 Sis(2-chloroethoxy)methane SOL 10 Famphur SOL 20 Sis(2-chloroethyl)ether SOL 10 Fluoranthene SOL 10 Sis(2-chloroisopropyl)ether SOL 10 Fluorene SOL 10 Sis(2-ethylhexyl)phthalate SOL 10 Hexachlorobenzene SOL 10 4-Sromophenyl phenyl ether SOL 10 Hexachlorobutadiene SOL 10 Sutyl benzyl phthalate SOL 10 Hexachlorocyclopentadiene SOL 10 p-Chloroaniline SOL 20 Hexachloroethane SOL 10 Chlorobenzilate SOL 10 Hexachloropropene SOL 10 2-Chloronaphthalene SOL 10 Indeno(1,2,3-cd)pyrene SOL 10 4-Chlorophenyl phenyl ether SOL 10 Isodrin SOL 20 Chrysene SOL 10 Isophorone SOL 10 Di-n-butyl phthalate SOL 10 Isosafrole SOL 10 Di-n-octyl phthalate SOL 10 Kepone SOL 20 Diallate SOL 10 Malathion SOL 50 Dibenz(a,h)anthracene SOL 10 Methapyrilene SOL 100 Dibenzofuran SOL 10 Methyl methanesulfonate SOL 10 1,2-Dichlorobenzene SOL 10 Methyl parathion SOL 10 1.3*Dichlorobenzene SOL 10 3-Methylcholanthrene SOL 10 ..j A-Dichlorobenzene SOL 10 2-Methylnaphthalene BOL 10 3'-Dichlorobenzidine SOL 20 Naphthalene Sal 10 BQL =Below Quantilalion Lim~ J =Less than Quanlilation Limit. Approximate Value PQL =Practical Quantilalion Limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1:-:4~44~--------------~3::":0:-=3':"9 ~A-m-W1':':"'*le-r"=R~oa-d':"".-:S~u":':'ite~10::":0~*-:A":':t1a-n~ta-."=G~A~3::":0:-=3':":60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II Sample 10:

GWC-13/MW-13 Matrix: Water Date Sampled: 12/16/2003 Date Extracted: 12/22/2003 Date Analyzed: 12/23/2003 ACl Sample #: 210461 Units: ",g/L Analyst: RB Analvte 1,4-Naphthoquinone 1-Naphthylamine 2-Naphthylamine 5-Nitro-o-toluidine 2-Nitroaniline 3-Nitroaniline "litroaniline lrobenzene N-Nitroso-di-n-butylamine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodipropylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine Parathion Pentachlorobenzene Penlachloronitrobenzene Phenacetin Phenanthrene p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene Thionazin 0-Toluidine 1,2,4-Trichlorobenzene ..2,0,0-Triethyl phosphorothioate '3,5-Trinitrobenzene BOL " Below Quantilalion Lim~ J " Less than Ouanlilation Lim~. Approximate Value POL" Practical Ouanlilalion Limit Result Sal Sal Sal Sal sal Sal Sal sal Sal Sal BOl BOl BOl BOl BOl BOl BOl Sal Sal BOl Sal Bal BOl Sal BOl BOl BOl Sal sal Sal Sal BOl PQl 10 10 10 10 50 50 20 10 10 20 10 10 10 10 20 40 20 10 20 20 10 10 10 10 10 10 10 20 10 10 50 10

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~.1~4"':"44~--------------~3~0~3~9"':"A-m-w~i1e-r~R~oa-d':'"*~S~u~it-e ~10~0~*~A~tl-an~ta-,~G~A-3~0~3~60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Acid Extractables (8270C)

  • Appendix II ACL Sample #: 210462 Units:

IJg/L Analvte Result PQL 4-Chloro-3-methylphenol Sal 20 2-Chlorophenol Sal 10 m & p-Cresol Sal 10 o-Cresol Sal 10 2,4-Dichlorophenol Sal 10 2,6-Dichlorophenol Sal 10 -0 4-Dimethylphenol Sal 10 3-Dinitro-2-methylphenol Sal 50 2,4-Dinitrophenol Sal 50 2-Nitrophenol Sal 10 4-Nitrophenol Sal 50 Pentachlorophenol Sal 50 Phenol Sal 10 2,3,4,6-Tetrachlorophenol Sal 10 2,4,5-Trichlorophenol Sal 10 2,4,6-Trichlorophenol Sal 10 Sample 10: GWC-13/MW-13-(Dupe) Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/16/2003 12/22/2003 12/23/2003 RB BOl =Below Quanlilallon limit J =less than Ouanlilalion liml. Approximate Value POL =Practical Ouantitalion limit

IA CL 1~~ A_D_Jl:_~_N~C~'E~D~C_'H~E~'M~L~S_TR~Y_L_A_B~S~,l......N......C_. Phone: (770) 409-1444 3039 Amwiler Road, Suite 100' Atlanta, GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant VogUe 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II Sample 10:

GWC-13/MW-13-(Dupe) Matrix: Water Date Sampled: 12/16/2003 Date Extracted: 12/22/2003 Date Analyzed: 12/23/2003 ACL Sample #: 210462 Units: IJg/l Analyst: RB Analvte Result PQl Analvte Result Pgl Acenaphthene BOl 10 Diethyl phthalate BOl 10 Acenaphthylene BOl 10 Dimethoate BOl 10 Acetophenone BOl 10 Dimethyl phthalate BOl 10 2-Acetylaminofluorene Sal 20 p-(Dimethylamino)azobenzene BOl 10 4-Aminobiphenyl BOl 20 7,12-Dimethylbenz(a)anthracene BOl 10 Anthracene BOl 10 3,3'-Dimethylbenzidine BOl 10 ~. --nzo(a)anthracene BOl 10 m-Dinitrobenzene BOl 20 I1zo(a)pyrene BOl 10 2,4-Dinitrotoluene BOl 10 Benzo(b)f1uoranthene BOl 10 2,6-Dinitrotoluene BOl 10 Benzo(g,h,i)peryJene BOl 10 Diphenylamine BOl 10 Benzo(k)f1uoranthene BOl 10 Disulfoton BOl 10 Benzyl alcohol Sal 20 Ethyl methanesulfonate BOl 20 Bis(2-ehloroethoxy)methane BOl 10 Famphur BOl 20 Bis(2-ehloroethyl)ether BOl 10 Fluoranthene BOl 10 Bis(2-chloroisopropyl)ether BOl 10 Fluorene BOl 10 Bis(2-ethylhexyl)phthalate BOl 10 Hexachlorobenzene BOl 10 4-Bromophenyl phenyl ether BOl 10 Hexachlorobutadiene BOl 10 Butyl benzyl phthalate BOl 10 Hexachlorocyclopentadiene BOl 10 p-Chloroaniline BOl 20 Hexachloroethane BOl 10 Chlorobenzilate BOl 10 Hexachloropropene BOl 10 2-Chloronaphthalene BOl 10 Indeno(1,2,3-cd)pyrene BOl 10 4-ChlorophenyJ phenyl ether BOl 10 Isodrin Sal 20 Chrysene BOl 10 Isophorone BOl 10 Di-n-butyl phthalate BOl 10 Isosafrole BOl 10 Di-n-octyl phthalate BOl 10 Kepone BOl 20 Diallate BOl 10 Malathion BOl 50 Dibenz(a,h)anthracene BOl 10 Methapyrilene BOl 100 Dibenzofuran BOl 10 Methyl methanesulfonate BOl 10 1,2-Dichlorobenzene BOl 10 Methyl parathion Sal 10 1,3-Dichlorobenzene BOl 10 3-Methylcholanthrene BOl 10 .!,4-Dichlorobenzene BOl 10 2-Methylnaphthalene BOl 10 "-Dichlorobenzidine BOl 20 Naphthalene BOl 10 BQL =Below Quantilalion Limit J =Less than Quantitation Lim~. Approximate Value PQL =Practical Quanlilalion Lim~

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 40~9~-1~4:-:'4~4---------------~30~3~9~A-m-w~i1e-r"=R~o-ad~.*~S~u~it-e""!"10~O~.-A~t1~an-ta-.~G~A~30~3 Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II Sample 10:

GWC-13/MW-13-(Dupe) Matrix: Water Date Sampled: 12/16/2003 Date Extracted: 12/2212003 Date Analyzed: 12/23/2003 ACl Sample #: 210462 Units: IJg/L Analyst: RB Analvte 1A-Naphthoquinone 1-Naphthylamine 2-Naphthylamine 5-Nitro-o-toluidine 2-Nitroaniline 3-Nitroaniline ..~ Nitroaniline Lrobenzene N-Nitroso-di-n-butylamine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodipropylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolldine Parathion Pentachlorobenzene Pentachloronitrobenzene Phenacetin Phenanthrene p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2A,5-Tetrachlorobenzene Thionazin o-Toluidine 1,2,4-Trichlorobenzene 2,o,o-Triethyl phosphorothioate 3,5-Trinitrobenzene BOL =Below Ouanlitalion Lima J =Less than Quantitation Limit Approximate Value POL =Practical QuantllalJon Linll Result Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal Sal SOL SOL SOL SOL PQl 10 10 10 10 50 50 20 10 10 20 10 10 10 10 20 40 20 10 20 20 10 10 10 10 10 10 10 20 10 10 50 10

IACL I Phone: (770) 409-1444 Fax: (770) 409*1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRYLABS, INC. 3039 Amwiler Road' Suite 100* Atlanta. GA 30360 P.O. Box 88610

  • Atlanta, GA 30356 www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 ACl Sample #: 210463 Units: ~g/L Analvte Result Pgl 4-Chloro-3-methylphenol BOl 20 2-Chlorophenol BOl 10 m &p-Cresol BOl 10 o-Cresol Sal 10 2.4-0ichlorophenol BOl 10 2,6-0ichlorophenol BOl 10 1-0imethylphenol BOl 10 ,d-Oinitro-2-methylphenol BOl 50 2,4-0initrophenol SOL 50 2-Nitrophenol BOl 10 4-Nitrophenol BOl 50 Pentachlorophenol BOl 50 Phenol BOl 10 2,3.4,6-Tetrachlorophenol Sal 10 2.4,5-Trichlorophenol BOl 10 2,4,6-Trichlorophenol BOl 10 Sample 10: Acid Extractables (8270C)

  • Appendix II GWC-15/MW-15 Matrix:

Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12/22/2003 12/23/2003 RB BOl =Below Ouantilalion limit J =less than Ouantilation lmil. Approxmale Value POL = Practical Ouantilalion lim~

IACL I ADVANCEDCHEMISTRYLABS,INC Phone: (770) 40~9:--1:-:4~44-:----------------~3:":0:":'3':"9 "':"A-m-W1::-'le-r-=R~oa-d':""~S~u~ite~100~'""'!A-'t1-an~ta-,~G~A-3~0:":'3~60~ Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004

IA CL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40~9~-1:-::4~44~----------------:3~0~39~Am-w~i1e-r'=R~oa-d~'-:S:-u~ite~10~0~'-:A~t1a-n~ta-, "'.:G~A~3~0~3~60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: ac/@acl-Iabs.net www.advancedchemistryJabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C) - Appendix II Sample 10: GWC-15/MW-15 Matrix: Water Date Sampled: 12117/2003 Date Extracted: 12/22/2003 Date Analyzed: 12/23/2003 ACl Sample #: 210463 Units: IJg/L Analyst: RB Analyte 1A-Naphthoquinone 1-Naphthylamine 2-Naphthylamine 5-Nitro-o-toluidine 2-Nitroaniline 3-Nitroaniline "Jitroaniline .*lrobenzene N-Nitroso-di-n-butylamine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodipropylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine Parathion Pentachlorobenzene Pentachloronitrobenzene Phenacetin Phenanthrene p-Phenylenedlamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene Thionazin 0-Toluidine 1,2,4-Trichlorobenzene -0.0.0-Triethyl phosphorothioate 3,5-Trinitrobenzene BOl =Below Ouantilalion limit J =less than Ouantilalion limit, Approximate Value POL =Practical Ouantilalion Urnit Result sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal sal PQl 10 10 10 10 50 50 20 10 10 20 10 10 10 10 20 40 20 10 20 20 10 10 10 10 10 10 10 20 10 10 50 10

IACL I Phone: (770) 409-1444 Fax: (770) 409-1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRYLABS, INC. 3039 Amwiler Road* Suite 100* Atlanta, GA 30360 P.O. Box 88610* Atlanta, GA 30356 www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 ACl Sample #: 210461 Units: 1J9/L Analvte Result PQl Aldrin SOL 0.05 Arochlor-1016 SOL 0.50 Arochlor-1221 SOL 0.50 Arochlor-1232 SOL 0.50 Arochlor-1242 SOL 0.50 Arochlor-1248 SOL 0.50 \\rochlor-1254 SOL 0.50 Arochlor-1260 SOL 0.50 a-SHC SOL 0.05 b-SHC SOL 0.05 d-SHC SOL 0.05 g-SHC SOL 0.05 Chlordane SOL 0.10 4,4'-DDD SOL 0.05 4,4'-DDE SOL 0.05 4,4'-DDT SOL 0.05 Dieldrin SOL 0.05 Endosulfan I SOL 0.05 Endosulfan II SOL 0.05 Endosulfan sulfate SOL 0.05 Endrin SOL 0.05 Endrin aldehyde SOL 0.05 Heptachlor SOL 0.05 Heptachlor epoxide SOL 0.05 Methoxychlor SOL 0.05 Toxaphene SOL 2.00 Sample 10: Pesticides/PCBs (8081A18082)

  • Appendix II GWC-13/MW-13 Matrix:

Water Date Sampled: 12/1612003 Date Extracted: 12/22/2003 Date Analyzed: 12/29/2003 Analyst: SS BOl=Below Quanlitation limit J =less than Ouanlllation limit. Approximate Value POL =Practical Quantialion Limi

IACL 1~~ A_D_~_~_N~C=-=-'E~'D-:,:C~'ll~"E-:-M~1.~S~TR~Y~L-.-A-.-B~S~, l~N~C_. Phone: (nO) 409-1444 3039 Amwiler Road* Suite 100* Atlanta, GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Pesticides/PCBs (8081A18082)* Appendix II ACl Sample #: 210462 Units: IJg/L Analvte Result PQl Aldrin Sal 0.05 Arochlor-1016 Sal 0.50 Arochlor-1221 SOL 0.50 Arochlor-1232 SOL 0.50 Arochlor-1242 SOL 0.50 Arochlor-1248 Sal 0.50 - 'ochlor-1254 SOL 0.50 .ochlor-1260 SOL 0.50 a-BHC SOL 0.05 b-BHC SOL 0.05 d-BHC SOL 0.05 g-BHC SOL 0.05 Chlordane SOL 0.10 4,4'-DDD SOL 0.05 4,4'-DDE SOL 0.05 4,4'-DDT SaL 0.05 Dieldrin Sal 0.05 Endosulfan I SOL 0.05 Endosulfan II SOL 0.05 Endosulfan sulfate SOL 0.05 Endrin SaL 0.05 Endrin aldehyde SOL 0.05 Heptachlor SaL 0.05 Heptachlor epoxide SOL 0.05 Methoxychlor SaL 0.05 Toxaphene SOL 2.00 Sample 10: GWC-13/MW-13-(Dupe) Matrix: Water Date Sampled: 12/16/2003 Date Extracted: 12/22/2003 Date Analyzed: 12/29/2003 Analyst: SS BOL =Below Ouantilalion Linit J =Less lhan Ouanlilalion Limit, Approximate Value POL =Practical Quanlitation Limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1~44~4~---------------:3~03:-:9~A~m-w-::i1:-er-:R~o-ad~. S~u"':':ite~1O:-:O~.~A~tla-n":""ta-. ~G":""A-:3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client ProJ #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Pesticides/PCBs (8081A18082). Appendix II ACL Sample #: 210463 Units: ~g/L Analvte Result P9L Aldrin SOL 0.05 Arochlor-1016 SOL 0.50 Arochlor-1221 SOL 0.50 Arochlor-1232 SOL 0.50 Arochlor-1242 SOL 0.50 Arochlor-1248 SOL 0.50 - '\\rochlor-1254 SOL 0.50 .rochlor-1260 SOL 0.50 a-SHC Sal 0.05 b-SHC Sal 0.05 d-SHC Sal 0.05 g-BHC Sal 0.05 Chlordane Sal 0.10 4,4'-000 SOL 0.05 4,4'-DDE Sal 0.05 4,4'-DDT Sal 0.05 Dieldrin Sal 0.05 Endosulfan I Sal 0.05 Endosulfan II SOL 0.05 Endosulfan sulfate Sal 0.05 Endrin Sal 0.05 Endrin aldehyde Sal 0.05 Heptachlor Sal 0.05 Heptachlor epoxide Sal 0.05 Methoxychlor Sal 0.05 Toxaphene Sal 2.00 Sample 10: GWC-15/MW-15 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/22/2003 Date Analyzed: 12/29/2003 Analyst: SS BOL :: Below Quanlitatlon Lima J "less than Ouantilation limit, Approximate Value pal:: Practical Quantilatlon limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 409~-1~4~44~--------------~3~0~39~A~m-W~i1~er~R~O-ad~' S~u~it-e~10~O~.~A~t1a-n~ta-,~G~A~3~03~6~O-Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 a-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Chlorinated Herbicides (8151A) - Appendix II ACL Sample #: 210461 Units: ~g/L Analyte Result PQL 2,4-0 BQL 1.0 Oinoseb BQL 1.0 2,4,5-TP (Silvex) BQL 1.0 2,4,5-T BQL 1.0 Sample 10: GWC-13/MW-13 Matrix: Water Date Sampled: 12116/2003 Date Extracted: 12/23/2003 Date Analyzed: 12129/2003 Analyst: SS BOl =Below Quantitation limit J =less than Quantilalion limit, APD/llxlmate Value POL =Praclical Ouanlilalion limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1~4~44O:----------------~3~0~39~A':"'m-WJ~'I~er~R~o-a~d-. ~Su~it~e~10~0~.~A~t1-an~ta-,~G~A~3~0"!"36~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 a-mail: acl@acl-Iabs.nat www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Chlorinated Herbicides (8151A)

  • Appendix II ACL Sample #: 210462 Units:

~g/L Analvte Result PQL 2,4-0 Sal 1.0 Oinoseb Sal 1.0 2,4,5-TP (Silvex) Sal 1.0 2.4,5-T Sal 1.0 Sample 10: GWC-13/MW-13-(Dupe) Matrix: Water Date Sampled: 12116/2003 Date Extracted: 12/23/2003 Date Analyzed: 1212912003 Analyst: . SS BOl =Below Quantitalion limit J =less than Ouantitslion limit, Approximate Value POL =Practical Quantitalion limit

IA CL 1~ A_D_~_:4_N~C~'E~V~C~'H~'E __M~l~'S__TR~Y__L-.-A_B"""",!,S~,L~'N......C_. Phone: (770) 409-1444 3039 Amwiler Road* Suite 100* Atlanta. GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Chlorinated Herbicides (8151A)

  • Appendix II ACl Sample #: 210463 Units:

~g/L Analvte Result PQl 2,4-D Sal 1.0 Dinoseb Sal 1.0 2,4,5-TP (Silvex) Sal 1.0 2,4,5-T Sal 1.0 Sample 10: GWC-15/MW-15 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/23/2003 Date Analyzed: 12/29/2003 Analyst: SS BOL =Below Quanlilation Linil J =Less than Ouanlilatlon Limit, ADO/Oxlmale Value POL=Practical Ouanlilation lim~

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40:":9~-1~4~44~--------------""'::3~0~39~A~m-W1-::'I:-er""'::R~o-a"":"d -.S~u-::it-e"":"10~0:-*""'::A~t1a-n~ta-.~G~A""'::3~0~36~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACL Sample #: 210461 Units:

~g/L Analvte Result PgL 1,2-Dibromo-3-chloropropane SOL 0.20 1,2-Dibromoethane SOL 0.05 Sample 10: GWC-13/MW-13 Matrix: Water Date Sampled: 12/16/2003 Date Extracted: 12/23/2003 Date Analyzed: 12/30/2003 Analyst: SS BOl =Below Quantilation limit J =less than Quanlilatlon linil APP/'Oxlmate Value pal =Practical Quanlilation linR

IACL i Phone: (770) 409*1444 Fax: (770) 409-1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRY LABS, INC. 3039 Amwiler Road* Suite 100. Atlanta, GA 30360 P.O. Box 88610* Atlanta, GA 30356 www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 ACL Sample #: 210462 Units: IJg/L AnaIvte Result PQL 1,2-Dibromo-3-chloropropane Sal 0.20 1,2-Dibromoethane Sal 0.05 Sample ID: Miscellaneous Organics (504.1) - Appendix II GWC-13/MW-13-(Dupe) Matrix: Water Date Sampled: 12116/2003 Date Extracted: 12123/2003 Date Analyzed: 12/30/2003 Analyst: SS BQL =Below Quanlilation Limit J =Less than Quanlilalion Limlt. Approxinate Value PaL =Pradical Quanlilalion Lilli

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9--1~444~--------------~3~03~9"":A-m-W1~*le-r~R-oa~d~.-:S~ui~te"":1~00~*~A~t1~an~ta-.-:G~A~3~03~6!"!'0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACl Sample #: 210463 Units:

~g/L Analvte Result Pgl 1.2-Dibromo-3-chloropropane aOL 0.20 1,2-Dibromoethane aOL 0.05 Sample 10: GWC-15/MW-15 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12123/2003 Date Analyzed: 12/30/2003 Analyst: SS BOL :: Below Quanlitatlon Limit J =less than Quantilation Limil. Approximate Value POL =Practical Quanlitalion limit

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40:":9~.1~44~4~---------------::3~03~9:-Am~W1~*I:-er""':R:-o-ad~. S=-u~it-e~100~*""':A":':'tla-nt~a-, '=GA~3~0~36:":0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemlstrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Miscellaneous Organics (504.1) - Appendix II ACL Sample #: 210469 Units: ~g/L Analvte Result 'PQL 1.2-Dibromo-3-chloropropane BOl 0.20 1.2-Dibromoethane BOl 0.05 Sample 10: GWC-S/MW-5 Matrix: Water Date Sampled: 1211612003 Date Extracted: 12123/2003 Date Analyzed: 01/0212004 Analyst: SS BOl=Below Quanlilalion limit J =less than Ouanlitation llmK. Approximate Value pal =Practical Quanlilation limit


--_._------------------ -~.~_._- -

ADVANCED CHEMISTRYLABS, INC IACL I Phone: (770) 409~.1~4~44~--------------~3~0~39~A~m-W1~*~le~r R::"o-a""':'d-*~Su""':'it~e""':'1~00~*~At~I~an-ta-,~G~A-3~0~36~0~ Fax: (770) 409*1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACl Sample #: 210470 Units:

~g/L Analvte Result PQl 1.2-Dibromo-3-chloropropane Sal 0.20 1,2-Dibromoethane BOl 0.05 Sample 10: GWB-6/MW-6 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/23/2003 Date Analyzed: 01/02/2004 Analyst: SS BOL =Below Quantilallon Limit J = Less than Ouantilalion Limit. APIllOxmate Value POL =Practical Ouantilation Limit

IACL I ADVANCED CHEMISTRYLABS,INC Phone: (770) 40~9-.1~4~44~--------------~3~03~9~A~m-W1~*J-er~Ro~ad~'~S~u~it-e ~10~0~'~A~tJa-n-ta-, ~GA~3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant VogUe 44014 12119/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II Sample 10:

GWA-7/MW-7 Matrix: Water Date Sampled: 12116/2003 Date Extracted: 12/23/2003 Date Analyzed: 01/0212004 ACl Sample #: 210471 Units: ~g/L Analyst: SS Analvte 1,2-Dibromo-3-chloropropane 1.2-Dibromoethane BQL =Below Quanlitallon llmJl J =lestthan Quantilalion UmII. Aplll'Oxinale Value POL =Practical auantitallon limit Result SOL SOL Pgl 0.20 0.05

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1!""!'4~44~-------------~3~03~9-:Am-w~ile-r~R-Oa~d~.~S~ui~te-:1~OO~.~A~t1-an~ta-.~G"!"A-:3"!"03~6"!"0-Fax: (770) 409-1844 P.O. Box 88610* AUanta, GA 30356 e-mail: acl@act-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACL Sample #: 210473 Units:

~g/L Analvte Result PQL 1,2-Dibromo-3-chloropropane Sal 0.20 1,2-Dibromoethane sal 0.05 Sample 10: GWC-14/MW-14 Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12123/2003 Date Analyzed: 01/0212004 Analyst: SS BOl=Below Quantllalion limit J " less than Ouantlatlon lim" AllIlIOxlmate Value POL =Praelicat QuantUtion limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~.1~444~--------------~3~03~9~A:-m-w-::i1:-er-:R~o-ad~. S~u~it-e~10~0:-."":'A":":'t1a-n~ta-. ~G":"'A-:3~03~6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix II Metals (6010B/7470A/7841) Sample 10: GWC-13/MW-13 Matrix: Date Sampled: Date Extracted: Date Analyzed: ACL Sample #: 210461 Units: mg/L Analyst: Water 12/16/2003 12/30/2003 SW/AD/JR Analyte Antimony Arsenic Barium Beryllium Cadmium Chromium

        • ~obalt

';opper lead Mercury Nickel Selenium Silver Thallium Tin Vanadium Zinc BOl =Below QuanlJlalion Unit J =Less lhan Quanlilallon Limit, Approximate Value POL =PracIIcal Quantilalion limit Result BOl BOl 0.033 BOl BOl BOl SOL SOL SOL SOL SOL BOl BOl SOL SOL SOL BOl PQL 0.006 0.010 0.020 0.004 0.005 0.020 0.050 0.020 0.010 0.0005 0.020 0.040 0.010 0.002 0.025 0.050 0.020

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~.1:-:4":"44~---------------=:3~03::':9:-:A:-m-w~i1-er-=:R~o-ad"':"".~S:-u~it-e ~1OO:-:-.~A~tla-n"':""ta-, ~GA~30~3~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix II Metals (6010B/7470A/7841) ACL Sample #: 210462 Units: mg/L Analvte Result PQL Antimony BOl 0.006 Arsenic BOl 0.010 Barium 0.032 0.020 Beryllium BOl 0.004 Cadmium BOl 0.005 Chromium BOl 0.020 ~obalt BOl 0.050

opper BOl 0.020 lead BOl 0.010 Mercury BOl 0.0005 Nickel BOl 0.020 Selenium BOl 0.040 Silver BOl 0.010 Thallium BOl 0.002 Tin BOl 0.025 Vanadium BOl 0.050 Zinc BOl 0.020 Sample 10

GWC-13/MW-13-(Dupe} Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12116/2003 12/30/2003 SW/AD/JR BOl =Below Quantilalion limit J =less than Quanliation linit, Approximate Value pal =Pradical Quanlilalion lim.

IACL I ADVANCED CHEMISTRYLABS, INC Phone: (770) 40~9~.1:"":'4":"44~---------------::3~03~9~A~m-w-::i1-er-::R~o-ad":"'.~S~u~ite~10~0~*"":'A~tla-n":""ta-. G~A":""-::3~03~6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@aci-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (60108/7841) Sample 10: GWC-5/MW-5 Matrix: Date Sampled: Date Extracted: Date Analyzed: ACL Sample #: 210469 Units:. mg/l Analyst: Water 12/16/2003 12130/2003 SW/AD Analvte Antimony Arsenic Barium Beryllium Cadmium Chromium ~obalt ';opper lead Nickel Selenium Silver Thallium Vanadium Zinc BOL " Below Ouanlilation Limit J " Less than Quanlilalion limit. AllPlOxmate Value pal" Practical Ouanlitation Limit Result SaL Sal 0.142 Sal Sal 0.028 Sal 0.025 Sal Sal Sal SOL Sal Sal 0.032 PQL 0.006 0.010 0.020 0.004 0.005 0.020 0.050 0.020 0.010 0.020 0.040 0.010 0.002 0.050 0.020

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~.1~4~44~--------------~3:":O~39~A~m-Wl-:'*I:-er~R~o-a"":"d-. S~u~it~e~10~0:-*~A~tla-n"'!"'ta-.~G~A~3:":0~36~0-Fax: (770) 409-1844 P.O. Box 88610' Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (60108/7841) ACL Sample #: 210470 Units: mg/L Analvte Result PQL Antimony Sal 0.006 Arsenic Sal 0.010 Sarium Sal 0.020 Seryllium Sal 0.004 Cadmium Sal 0.005 Chromium Sal 0.020 -'":obalt Sal 0.050 ~opper Sal 0.020 lead Sal 0.010 Nickel Sal 0.020 Selenium Sal 0.040 Silver Sal 0.010 Thallium Sal 0.002 Vanadium Sal 0.050 Zinc Sal 0.020 Sample 10: GWB-6/MW-6 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/1712003 12130/2003 SW/AD BOL.. Below Quanlilation limit J.. less than Quanlilalion limit. Approximate Value POL" Practical Ouantitalion limit

IA CL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 40~9~-1~4~44~--------------~3~03~9~A~m-w~i1~er~R~o-ad-:--* S~u~it-e~10~0~*~A~t1a-n~ta-. ":G~A~3~0~36~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (60108/7841) ACL Sample #: 210471 Units: mg/L Analyte Result PQL Antimony Sal 0.006 Arsenic Sal 0.010 Sarium Sal 0.020 Seryllium Sal 0.004 Cadmium Sal 0.005 Chromium Sal 0.020 Sal 0.050 'obalt ..;opper Sal 0.020 lead Sal 0.010 Nickel Sal 0.020 Selenium Sal 0.040 Silver Sal 0.010 Thallium Sal 0.002 Vanadium Sal 0.050 Zinc 0.023 0.020 Sample 10: GWA-7/MW-7 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/16/2003 12/30/2003 SW/AD SOL =Below Quantltallon LIm~ J =Less than Ouantitalion Limit, Approximate Value POL '" Practical Quantilalion LImil

IA CL 1~~ A_D_~_:4_N~C~'E~1J~C_'H!!!"""E~M~L_'S_TR~Y~L_A_B""",!,,S~, l~'N~C_. Phone: (770) 409-1444 3039 Amwiler Road* Suite 100* Atlanta. GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-labs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix II Metals (6010B/7470A/7841) ACl Sample #: 210473 Units: mg/L Analvte Result PQl Antimony Sal 0.006 Arsenic Sal 0.010 Sarium 0.189 0.020 Seryllium 0.004 0.004 Cadmium 0.011 0.005 Chromium 0.091 0.020 'obalt Sal 0.050 ...opper 0.026 0.020 lead 0.015 0.010 Mercury 0.0100 0.0005 Nickel 0.034 0.020 Selenium Sal 0.040 Silver Sal 0.010 Thallium Sal 0.002 Tin Sal 0.025 Vanadium 0.060 0.050 Zinc 0.127 0.020 Sample 10: GWC-14/MW-14 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/1712003 12/30/2003 SW/AD/JR BOl =Below Ouanlilalion limil J =less than Ouanlltalion limit. Approxlmate Value POL =Practical Quantitallon linit

IACL I ADVANCEDCHEMISTRYLABS,INC. Phone: (770) 40~9~-1~4~44~--------------~3~0"!"39~A"l'"m-w~i!'"'le-r R!!!""o-a~d-*"!"Su~it-e~1"!"OO~*-A~t1~an-ta-,""!!G~A-3""""'O"'36"0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-labs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix II Metals (6010B/7470A/7841) ACl Sample #: 210463 Units: mg/L Analvte Result PQl Antimony BOl 0.006 Arsenic BOl 0.010 Barium BOl 0.020 Beryllium BOl 0.004 Cadmium BOl 0.005 Chromium BOl 0.020 ~obalt BOl 0.050 ";opper BOl 0.020 lead BOl 0.010 Mercury BOl 0.0005 Nickel BOl 0.020 Selenium BOl 0.040 Silver BOl 0.010 Thallium BOl 0.002 Tin BOl 0.025 Vanadium BOl 0.050 Zinc BOl 0.020 Sample 10: GWC-15/MW-15 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/1712003 12/30/2003 SW/AD/JR BOl =Below Quantilallon limit J =less than Ouanlllalion Limit. Approximate Value POL =Practical Ouanfilatlon Limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 409-~1"'!"44~4~-------------"'"":'30~3::':'9~Am-w~i1e-r"=R-oa""':d:-*~S""':ui~te~1~OO:-*""':At:-=:I-an~ta-.~G~A~3~03~60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client: Genesis Project Client ProJ #: Plant Vogtle 1258 Concord Rd. ACL Project #: 44014 Smyrna, GA 30080-0000 Date Received: 12119/2003 Date Reported: 01/06/2004

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Mr. Mark Mitchell Date Sample ID ACL# Analvte Matrix Result PQL Y!!!!! Analyzed GWC-13/MW-13 210461 Cyanide (9012A) Water BOL 0.020 mg/L 12123/2003 GWC-13/MW-13 210461 Sulfide (9034) Water BOL 1.0 mg/L 12123/2003 BOL =Below Cluanlilatlon Limit J.= Less than QuantiationLinit. AllllIOximaIe Value POL =Practical Quenlilatlon Limit

IACL 1~~ AD_V:_:4_N~C~'E~'D~C_'H~E~MWO"!L~S~TR"!"!,,,Y~L~A_B~S,,!,,,",l""""""N......C_. Phone: (770) 409-1444 3039 Amwiler Road* Suite 100* Atlanta. GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client: Genesis Project Client Proj #: Plant Vogtle 1258 Concord Rd. ACl Project #: 44014 Smyrna, GA 30080-0000 Date Received: 12/19/2003 Date Reported: 01/06/2004

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Mr. Mark Mitchell Date Sample 10 Analvte Matrix Result PQl Y!!!t! AnalYZed GWC-13/MW-13-(Oa10462 Cyanide (9012A) Water SOL 0.020 mglL 12/23/2003 GWC-13/MW-13-(Oa10462 Sulfide (9034) Water SOL 1.0 mglL 12/2312003 BOL =Below Quanllallon Llmll J =Less than Quanlllatlon Limit. AllllIOximaIe Value POL '" Practical Quanlilalion Limi

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 409~-1~44~4~-------------~3~03~9~Am~w1"::"le"r"'=R~oa"d:-'=S~uit~e~1~OO~*-A~t1:-'an""':'ta""."'=G~A-:3:O:::0'::":36~O-Fax: (770) 409-1844 P.O. Box 88610

  • Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Genesis Project Client Proj #: Plant VogUe 1258 Concord Rd. ACL Project #: 44014 Smyrna, GA 30080-0000 Date Received: 12/19/2003 Date Reported: 01/06/2004

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Mr. Mark Mitchell Date Sample 10 ACL# Analvte Matrix Result PQL Units Analyzed GWC-15/MW-15 210463 Cyanide (9012A) Water SOL 0.020 mg/L 12123/2003 GWC-15/MW-15 210463 Sulfide (9034) Water SOL 1.0 mg/L 12/23/2003 BOl =Below Quanlltatlon llmil J:: less than Quantilalion linll. AllPlOxinale Value PQl =Practical Quanlitation limit

IA CL 1...


AD-Jl:-'AN~CE!""!"1J~CH~'E-'M~lS~l:~'R~Y

....L-AB~S~,~IN~C_. Phone: mO) 409-1444 3039 Amwiler Road* SUite 100

  • Atlanta. GA 30360 Fax: (770) 409-1844 P.O. Box 88610
  • Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Genesis Project Client Proj #: Plant Vogtle 1258 Concord Rd. ACL Project #: 44014 Smyrna, GA 30080-0000 Date ReceIved: 12119/2003 Date Reported: 01/06/2004

Contact:

Mr. Mark Mitchell Date Sample 10 ~ Analvte Matrix Result P9L Units Analyzed EO-Blank 210464 Cyanide (9012A) Water BOL 0.020 mg/L 12123/2003 EO-Blank 210464 Sulfide (9034) Water BOL 1.0 mglL 12123/2003 eal =BeloW Quanliation limit J =less than Quantllallon Unll. ApproUnale Value PaL =Pradicat auantilalionlimit

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 409~*1~44~4:---------------"""':'30~3~9-:Am""'W1':':"*Ie-r ':::'Ro-ad-:-*":Su-:ite~1~OO~*-:A~tla-n"":"'ta-. ":GA~3~03~6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client: Genesis Project Client Proj #: Plant Vogtle 1258 Concord Rd. ACL Project #: 44014 Smyrna. GA 30080-0000 Date Received: 12119/2003 Date Reported: 01/06/2004

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Mr. Mark Mitchell Date Sample 10 A£U Analvte Matrix Result PQL Units Analyzed GWC-5/MW-5 210469 Mercury (7470A) Water Sal 0.0005 mg/L 12124/2003 Bal =Below Quantllallon Linit J =less IIlan Quanlllallon llml AllOIOxinate Value PaL=Plaetical Quantbllon Limit

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 409~.1!""!'444~--------------~30~3~9""'!!Am-W1~*le-r"=!Ro-a'""'!d~.~S'""'!ui~te""'!!1~00~*'""'!A~t\\-an-ta-. "=!G~A""!!3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 a-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client: Genesis Project Client Proj #: Plant Vogtle 1258 Concord Rd. ACl Project #: 44014 Smyrna, GA 30080-0000 Date Received: 12119/2003 Date Reported: 01/06/2004

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Mr. Mark Mitchell Date Sample 10 ACl# Analvte Matrix Result PQl Units Analyzed GWS-6/MW-6 210470 Mercury (7470A) Water Sal 0.0005 mg/L 12124/2003 8Ql =Below Quanlitalion limil J =less !han Quantitalion lmil, AllI)IOJlinaIe Value POL=PradIcaI QuantiIalion lilllll

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 409-~1~44~4:-----------------::'30~3::o::'9'"":'Am-W1~'le-r '='Ro-a-'d-*~Su-'ite~1':":OO~*-'A~tla-n~ta-. '='GA~3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610* AUanta. GA 30356 e-mail: aci@acI-labs.net www.advancedchemistrylabs.com Client: Genesis Project Client ProJ #: Plant Vogtle 1258 Concord Rd. ACL Project #: 44014 Smyrna, GA 30080-0000 Date Received; 12/19/2003 Date Reported: 01/0612004

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Mr. Mark Mitchell Date Sample ID ACL# Analvte Matrix Result PQL Units Analyzed GWA-7/MW-7 210471 Mercury (7470A) Water BOL 0.0005 mg/L 12/24/2003 Bel =Below Quantbtion linI J.. less than QuardatlonUn" AiJIlloxinale Value PQl.. Practical Quantllalion limit

LABORATORY QA/QC RESULTS

IACL I Phone: (770) 409-1444 Fax: (770) 409-1844 e-mail;acl@acJ-labs.net ADVANCED CHEMISTRYLABS, INC. 3039 Amwiler Road* Suite 100* Atlanta, GA 30360 P.O. Box 88610* Atlanta. GA 30356 www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 v.o. (5030B/8260B)

  • Appendix II Sample 10:

EO-Blank Matrix: Water Date Sampled: 12/17/2003 Date Extracted: Date Analyzed: 12/30/2003 ACL Sample #: 210464 Units: IJg/l Analyst: RP Analyte Result PQL Analyte Result PQL Acetone Sal 100 cis-1,3-Dichloropropene Sal 5 Acetonitrile Sal 100 trans-1.3-Dichloropropene Sal 5 Acrolein Sal 100 Ethyl methacrylate Sal 10 Acrylonitrile Sal 50 Ethylbenzene Sal 5 Allyl chloride Sal 10 2-Hexanone Sal 50 Senzene Sal 5 Isobutyl alcohol Sal 50 - 'omochloromethane Sal 5 Methacrylonitrile Sal 100 .Jromodichloromethane Sal 5 Methyl bromide Sal 10 Sromoform Sal 5 Methyl chloride Sal 10 Carbon disulfide Sal 5 Methyl ethyl ketone Sal 100 Carbon tetrachloride Sal 5 Methyl iodide Sal 5 Chlorobenzene Sal 5 Methyl methacrylate Sal 30 Chloroethane Sal 10 4-Methyl-2-pentanone Sal 50 Chloroform Sal 5 Methylene bromide Sal 5 Chloroprene Sal 20 Methylene chloride Sal 5 1.2-Dibromo-3-chloropropane Sal 20 Naphthalene Sal 5 Dibromochloromethane Sal 5 Propionitrile Sal 150 1,2-Dibromoethane Sal 5 Styrene Sal 5 trans-1,4-Dichloro-2-butene Sal 10 1,1,1,2-Tetrachloroethane Sal 5 1,2-Dichlorobenzene Sal 5 1,1,2,2-Tetrachloroethane Sal 5 1,3-Dichlorobenzene sal 5 Tetrachloroethene Sal 5 1A-Dichlorobenzene Sal 5 Toluene Sal 5 Dichlorodifluoromethane sal 5 1,1.1-Trichloroethane Sal 5 1,1-Dichloroethane Sal 5 1,1.2-Trichloroethane Sal 5 1,2-Dichloroethane sal 5 Trichloroethene sal 5 1,1-Dichloroethene Sal 5 Trichlorofluoromethane Sal 5 cis-1,2-Dichloroethene Sal 5 1,2,3-Trichloropropane Sal 5 trans-1.2-Dichloroethene Sal 5 Vinyl acetate Sal 50 1,2-Dichloropropane sal 5 Vinyl chloride Sal 2 1,3-Dichloropropane Sal 5 m & p-Xylenes sal 10 ..2,2-Dichloropropane sal 15 a-Xylene Sal 5 ,1-Dichloropropene Sal 5 BOl =Below Quantitation Limit J =less than Ouantitation limR. Approximate Value POL =Practical Ouantitation limit

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 409~-1~4~4"'!'4----------------""!"3~03~9~A~m-w~i~le-r ~Ro-a-d~'~S~u~ite~10~0-'-A~t1-an-ta-,~G~A~3~03~6""!"0-Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 V.O.(5030B/8260B)

  • Appendix II Sample 10:

Trip Blank Matrix: Water Date Sampled: 12/16/2003 Date Extracted: Date Analyzed: 12/29/2003 ACL Sample #: 210465 Units: 1J9/L Analyst: RP Analvte Result PQL Analvte Result PQL Acetone SOL 100 cis-1,3-Dichloropropene SOL 5 Acetonitrile SOL 100 trans-1,3-Dichloropropene SOL 5 Acrolein SOL 100 Ethyl methacrylate SOL 10 Acrylonitrile SOL 50 Ethylbenzene SOL 5 Allyl chloride SOL 10 2-Hexanone SOL 50 Senzene SOL 5 Isobutyl alcohol SOL 50 fomochloromethane SOL 5 Methacrylonitrile SOL 100 dromodichloromethane SOL 5 Methyl bromide SOL 10 Sromoform SOL 5 Methyl chloride SOL 10 Carbon disulfide SOL 5 Methyl ethyl ketone SOL 100 Carbon tetrachloride SOL 5 Methyl iodide SOL 5 Ch/orobenzene SOL 5 Methyl methacrylate Sal 30 Chloroethane SOL 10 4-Methyl-2-pentanone SOL 50 Chloroform SOL 5 Methylene bromide SOL 5 Chloroprene SOL 20 Methylene chloride SOL 5 1,2-Dibromo-3-chloropropane SOL 20 Naphthalene Sal 5 Dibromochloromethane Sal 5 Propionitrile Sal 150 1,2-Dibromoethane SOL 5 Styrene SOL 5 trans-1,4-Dichloro-2-butene SOL 10 1,1,1,2-Tetrachloroethane SOL 5 1,2-Dichlorobenzene SOL 5 1,1.2,2-Tetrachloroethane SOL 5 1,3-Dichlorobenzene SOL 5 Tetrachloroethene SOL 5 1,4-Dichlorobenzene SOL 5 Toluene SOL 5 Dichlorodifluoromethane SOL 5 1,1.1-Trichloroethane SOL 5 1,1-Dichloroethane SOL 5 1,1,2-Trichloroethane SOL 5 1,2-Dichloroethane SOL 5 Trichloroethene SOL 5 1,1-Dichloroethene SOL 5 Trichlorofluoromethane SOL 5 cis-1,2-Dichloroethene SOL 5 1,2,3-Trichloropropane SOL 5 trans-1,2-Dichloroethene SOL 5 Vinyl acetate Sal 50 1,2-Dichloropropane SOL 5 Vinyl chloride Sal 2 1,3-Dichloropropane SOL 5 m & p-Xylenes SOL 10 ... (,2-Dichloropropane SOL 15 o-Xylene sal 5 .,1-Dichloropropene Sal 5 BOl " Below Quantitation limit J =less than Ouanlilation limit, ApJl(Oximate Value POL" Practical Ouanlilation lillil .... _-_.. _ ~

IACL I ADVANCED CHEMISTRY LABS, INC Phone: (770) 40~9~-1~4~44-:---------------~3~0~3':"9 ":"A-m-Wl~*le-r~R~oa-d':""*-:S:-u~ite~10~0~.-:A~t1a-n"':"ta-.~G"':"A~3~0~36':":0=-- Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client ProJ #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Acid Extractables (8270C) - Appendix II ACL Sample #: 210464 Units: jJg/L Analvte Result PQL 4-Chloro-3-methylphenol Sal 20 2-Chlorophenol Sal 10 m & p-Cresol Sal 10 o-Cresol Sal 10 2,4-Dichlorophenol Sal 10 2,6-Dichlorophenol Sal 10 Dimethylphenol Sal 10 .6-Dinitro-2-methylphenol Sal 50 2,4-Dinitrophenol Sal 50 2-Nitrophenol Sal 10 4-Nitrophenol Sal 50 Pentachlorophenol Sal 50 Phenol Sal 10 2.3,4,6-Tetrachlorophenol Sal 10 2.4,5-Trichlorophenol Sal 10 2,4,6-Trichlorophenol Sal 10 Sample 10: EQ-Blank MatrIx: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12/2212003 12123/2003 RB BOL =Below Quantilalion Limit J =Lesslhan Ouantitation Lim~. Approximate Value POL =Practical Quanlilation Limi

IACL I ADVANCEDCHEMISTRYLABS,lNC. Phone: (770) 40~9~-1~4""!'44~---------------3~0~3~9~A-m-W~i1e-r"'=R~o-ad~*~S~u~it-e""!"10~0~*~A~t1-an-ta-,~G~A-3~0~3~60~ Fax: (770) 409-1844 P.O. Sox 88610* Atlanta, GA 30356 e-mail: aCI@acl*labs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant VogUe 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C) - Appendix II Sample 10: EO-Blank Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/22/2003 Date Analyzed: 12/23/2003 ACl Sample #: 210464 Units: lJg/L Analyst: RB Analyte Result Pgl Analvte Result POL Acenaphthene Sal 10 Diethyl phthalate Sal 10 Acenaphthylene Sal 10 Dimethoate Sal 10 Acetophenone Sal 10 Dimethyl phthalate Sal 10 2-Acetylaminofluorene Sal 20 p-(Dimethylamino)azobenzene Sal 10 4-Aminobiphenyl Sal 20 7,12-Dimethylbenz(a)anthracene Sal 10 Anthracene Sal 10 3,3'-Dimethylbenzidine Sal 10 'enzo(a)anthracene Sal 10 m-Dinitrobenzene Sal 20 .Jenzo(a)pyrene Sal 10 2,4-Dinitrotoluene Sal 10 Senzo(b)fluoranthene Sal 10 2,6-Dinitrotoluene Sal 10 Senzo(g,h.i)perylene Sal 10 Diphenylamine Sal 10 Senzo(k)f1uoranthene Sal 10 Disulfoton Sal 10 Senzyl alcohol Sal 20 Ethyl methanesulfonate Sal 20 Sis(2-chloroethoxy)methane Sal 10 Famphur Sal 20 Sis(2-chloroethyl)ether Sal 10 Fluoranthene Sal 10 Sis(2-chloroisopropyl)ether Sal 10 Fluorene Sal 10 Sis(2-ethylhexyl)phthalate Sal 10 Hexachlorobenzene Sal 10 4-Sromophenyl phenyl ether Sal 10 Hexachlorobutadiene Sal 10 Sutyl benzyl phthalate Sal 10 Hexachlorocyclopentadlene Sal 10 p-Chloroaniline Sal 20 Hexachloroethane Sal 10 Chlorobenzilate Sal 10 Hexachloropropene Sal 10 2-Chloronaphthalene Sal 10 Indeno(1,2.3-cd)pyrene Sal 10 4-Chlorophenyl phenyl ether Sal 10 Isodrin Sal 20 Chrysene Sal 10 Isophorone Sal 10 Di-n-butyl phthalate Sal 10 Isosafrole Sal 10 Di-n-octyl phthalate Sal 10 Kepone Sal 20 Diallate Sal 10 Malathion Sal 50 Dibenz(a,h)anthracene Sal 10 Methapyrilene Sal 100 Dibenzofuran Sal 10 Methyl methanesulfonate Sal 10 1,2-Dichlorobenzene Sal 10 Methyl parathion Sal 10 1,3-Dichlorobenzene Sal 10 3-Methylcholanthrene Sal 10 o,1,4-Dichlorobenzene Sal 10 2-Methylnaphthalene Sal 10 .3'-Dichlorobenzidine Sal 20 Naphthalene Sal 10 eOL =Below Ouanli1ation Limit J =Less than Ouantitalion Lilla. Approximate Value POL =Practical Quantitalion Limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 409~-1~4"":"44~--------------~3~0~3~9"":"A-m-w~i1e-r~R~oa-d~*~S~u~ite~10~0~*~A~1I-ant-a-,~G~A-3~0~3~60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II Sample 10:

EO-Blank Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/22/2003 Date Analyzed: 1212312003 ACL Sample #: 210464 Units: ~g/L Analyst: RB Analvte 1A-Naphthoquinone 1-Naphthylamine 2-Naphthylamine 5-Nitro-o-toluidlne 2-Nitroaniline 3-Nitroaniline .-Nitroaniline .Jitrobenzene N-Nitroso-di-n-butylamine N-Nitrosodiethylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodipropylamine N-Nitrosomethylethylamine N-Nitrosopiperidine N-Nitrosopyrrolidine Parathion Pentachlorobenzene Pentachloronitrobenzene Phenacetin Phenanthrene p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5-Tetrachlorobenzene Thionazin o-Toluidine 1,2,4-Trichlorobenzene .....0,0,0-Triethyl phosphorothioate 1,3.5-Trinitrobenzene Sal =Below Ouantitalion Limit J " less lhan Quanlilalion limit, ADDlOximale Value pal =Praclical Quanlilalion Limit Result Sal Sal Sal Sal Sal SOL Sal Sal Sal SOL SOL Sal Sal SOL Sal Sal Sal SOL Sal Sal Sal SOL Sal Sal Sal Sal SOl Sal Sal Sal Sal Sal PQL 10 10 10 10 50 50 20 10 10 20 10 10 10 10 20 40 20 10 20 20 10 10 10 10 10 10 10 20 10 10 50 10

ADVANCED CHEMISTRY LABS, INC. IACL I Phone: (770) 40~9-:.1~444~--------------~3~03::':9:-A:-m-w~il:-er-:R::-o-ad~* S::"u~it-e~100::'::-.-:A~t1-an~ta-.":G~A-:3~0~36~0~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Pesticides/PCBs (8081A18082)

  • Appendix II ACl Sample #: 210464 Units:

J.Ig/L Analvte Result PQl Aldrin Sal 0.05 Arochlor-1016 Sal 0.50 Arochlor-1221 Sal 0.50 Arochlor-1232 Sal 0.50 Arochlor-1242 Sal 0.50 Arochlor-1248 Sal 0.50 -~rochlor-1254 Sal 0.50 Jochlor-1260 Sal 0.50 a-SHC Sal 0.05 b-SHC Sal 0.05 d-SHC Sal 0.05 g-SHC Sal 0.05 Chlordane Sal 0.10 4,4'-000 Sal 0.05 4,4'*00E Sal 0.05 4,4'-00T Sal 0.05 Dieldrin Sal 0.05 Endosulfan I Sal 0.05 Endosulfan II Sal 0.05 Endosulfan sulfate Sal 0.05 Endrin Sal 0.05 Endrin aldehyde Sal 0.05 Heptachlor Sal 0.05 Heptachlor epoxide Sal 0.05 Methoxychlor Sal 0.05 Toxaphene Sal 2.00 Sample 10: EQ-Blank Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12/22/2003 12/29/2003 SS SOL =Selow QuantitaUon lim~ J =less than OuantMUon limit. Approximate Value POL =Practical Ouanlilaoon limit

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40~9~-1~4~44~--------------~3~03~9~A~m-w~i1~er-:R~o-ad~' S~u~it-e-10~0~'-:A-'t1a-n~ta-, ~G-A-'3"'0~36""'0-Fax: (770) 409*1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Chlorinated Herbicides (8151A)

  • Appendix II ACL Sample #: 210464 Units:

~g/L Analvte Result PQL 2,4-0 SOL 1.0 Oinoseb SOL 1.0 2.4,5-TP (Silvex) SOL 1.0 2,4,5-T SOL 1.0 Sample ID: EO-Blank Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/23/2003 Date Analyzed: 12/29/2003 Analyst: S8 BOl,. Below Quanlilalion lim~ J,. less than Quantilalion lmK. Approximate Value pal" Practical QuanUlation lmi!

IACL I ADVANCEDCHEMISTRYLABS,lNC. Phone: (770) 4Q9..~1~44":""4:-----------------::3~03~9~Am:--W1-::*I~er-:Ro~ad~' S::"u~it-e~10~0~'-:A":":'tla-n"':"ta-, ~G"':"A-:3~03=-:6~0-Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Miscellaneous Organics (504.1)

  • Appendix II ACL Sample #: 210464 Units:

J,Jg/L Analvte Result PQL 1,2-Dibromo-3-chloropropane SOL 0.20 1,2-Dibromoethane SOL 0.05 Sample 10: EO-Blank Matrix: Water Date Sampled: 12/17/2003 Date Extracted: 12/23/2003 Date Analyzed: 12/30/2003 Analyst: SS Sal =Below Quanlialion limK J =less than Ouanlilalion Limit. APPIOximale Value pal =Praclical Quanlilalion limR

IACL I ADVANCED CHEMISTRYLABS,INC Phone: (770) 40~9~-1~4~44~--------------~3!"!'0~39!'""A~m-w~lI~er~R!""o-a~d -.S~u"'!'it-e"'!'10~0~'~A-'t1a-n-ta-,~G"'!"A-3""'!'0~360~- Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabS.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix II Metals (6010B/7470A/7841) ACL Sample #: 210464 Units: mg/L Analvte Result PQL Antimony BOl 0.006 Arsenic BOl 0.010 Barium BOl 0.020 Beryllium BOl 0.004 Cadmium BOl 0.005 Chromium SOL 0.020 -obalt SOL 0.050 Jpper BOl 0.020 Lead BOl 0.010 Mercury SOL 0.0005 Nickel SOL 0.020 Selenium BOL 0.040 Silver BOl 0.010 Thallium Sal 0.002 Tin BOl 0.025 Vanadium Sal 0.050 Zinc BOl 0.020 Sample ID: EO-Blank Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/17/2003 12/30/2003 SW/AD/JR BOl =Below Quantitatlon Limit J =less than Quanlilation lim~. Approximate Value POL =Practical Quanlitalion limit

IACL 1"'-- AD_VA_N_C_13_D~CH-E-M-IS-T-'R-Y-LA-B~S,-IN-C. Phone: (770) 409-1444 3039 Amwiier Road* Suite 100* Atlanta, GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 Outside GA: (800) 277-0520 www.advancedchemistrylabs.com e-mail: acl@mindspring.com QUALITY CONTROL SECTION

IACL 1"-- A_D_v:_:4_N~C~'E-'D"""'!!C-'H~'E~M"""'!"L""!"'S-TR......Y"""'!"'L~A-B......S-,l""!",,,!N~C__ Phone: (770) 409-1444 3039 Amwiler Road-Suite 100' Atlanta, GA 30360 Fax: (770) 409-1844 P.O. Box 88610' Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 409~-1~4~4~4----------------~30~3~9~A~m-w~il~er~R~o-a~d-*~S~u~ite-1~0~0-*~A~t1-an-ta-,~G~A~30~3~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Jabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Pro) #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 v.o. (50308/82608)

  • Appendix II Sample 10:

Matrix: Water Date Sampled: Date Extracted: Date Analyzed: 12/30/2003 ACL Sample #: Blank Units: jJg/L Analyst: RP Analvte Result PQL Analvte Result PQL Acetone Sal 100 cis-1,3-Dichloropropene Sal 5 Acetonitrile Sal 100 trans-1.3-Dichloropropene Sal 5 Acrolein 80l 100 Ethyl methacrylate 80l 10 Acrylonitrile 80l 50 Ethylbenzene 80l 5 Allyl chloride Sal 10 2-Hexanone 80l 50 Senzene 80l 5 Isobutyl alcohol Sal 50 romochloromethane 80l 5 Methacrylonitrile Sal 100 t:3romodichloromethane 80l 5 Methyl bromide 80l 10 Sromoform 80l 5 Methyl chloride 80l 10 Carbon disulfide Sal 5 Methyl ethyl ketone Sal 100 Carbon tetrachloride 80l 5 Methyl iodide Sal 5 Chlorobenzene 80l 5 Methyl methacrylate Sal 30 Chloroethane 80l 10 4-Methyl-2-pentanone 80l 50 Chloroform 80l 5 Methylene bromide Sal 5 Chloroprene Sal 20 Methylene chloride 80l 5 1,2-Dibromo-3-chloropropane 80l 20 Naphthalene Sal 5 Dibromochloromethane 80l 5 Propionitrile Sal 150 1.2-Dibromoethane Sal 5 Styrene Sal 5 trans-1,4-Dichloro-2-butene Sal 10 1,1,1.2-Tetrachloroethane Sal 5 1,2-Dichlorobenzene Sal 5 1,1.2.2-Tetrachloroethane Sal 5 1,3-Dichlorobenzene Sal 5 Tetrachloroethene Sal 5 1,4-Dichlorobenzene Sal 5 Toluene Sal 5 Dichlorodifluoromethane Sal 5 1,1,1-Trichloroethane 80l 5 1,1-Dichloroethane Sal 5 1,1,2-Trichloroethane Sal 5 1,2-Dichloroethane Sal 5 Trichloroethene Sal 5 1,1-Dichloroethene Sal 5 Trichlorofluoromethane 80l 5 cis-1,2-Dichloroethene Sal 5 1,2,3-Trichloropropane Sal 5 trans-1,2-0ichloroethene Sal 5 Vinyl acetate Sal 50 1,2-Dichloropropane Sal 5 Vinyl chloride Sal 2 1,3-0ichloropropane Sal 5 m & p-Xylenes Sal 10 2,2-Dichloropropane Sal 15 o-Xylene BOl 5 1,1-Dichloropropene 80l 5 80l =Below Ouanlllation limit J =less than Quantilation limit, Approximate Value PQl =Praaical Quantilation Lirnit

IACL I Phone: (770)409-1444 Fax: (770) 409-1844 e-mail: acl@acl-Iabs.net ADVANCED CHEMISTRYLABS, INC. 3039 Amwiler Road* Suite 100* Atlanta, GA 30360 P.O. Box 88610

  • Atlanta, GA 30356 www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 v.o. (50308/82608)

  • Appendix I Analvte Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform 1rbon disulfide

....arbon tetrachloride Chlorobenzene Chloroethane Chloroform 1,2-Dibromo-3-chloropropane Dibromochloromethane 1.2-Dibromoethane trans-1,4-Dichloro-2-butene 1,2-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1.2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene 2-Hexanone Methyl bromide Methyl chloride Methyl ethyl ketone

    • Methyl iodide

-Methyl-2-pentanone Sample 10: ACl Sample #: Blank Units: Result BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl BOl Sal Sal Sal Sal Sal Sal Sal sal Sal ~g/l Pgl 100 50 5 5 5 5 5 5 5 10 5 20 5 5 10 5 5 5 5 5 5 5 5 5 5 5 50 10 10 100 5 50 Matrix: Water Date Sampled: Date Extracted: Date Analyzed: 12130/2003 Analyst: RP Analvte Result PQl Methylene bromide BOl 5 Methylene chloride BOl 5 Styrene BOl 5 1,1,1,2-Tetrachloroethane BOl 5 1,1,2,2-Tetrachloroethane BOl 5 Tetrachloroethene BOl 5 Toluene BOl 5 1,1,1-Trichloroethane BOl 5 1,1,2-Trichloroethane BOl 5 Trichloroethene BOl 5 Trichlorofluoromethane BOl 5 1,2.3-Trichloropropane BOl 5 Vinyl acetate BOl 50 Vinyl chloride BOl 2 m & p-Xylenes BOl 10 o-Xylene BOl 5 BQl =Below Quanlilalion Limit J =less than Quanlitalion limit. AoolOximate Value pal =Practical Ouanlilalion limit

IACL 1~~ A_D_V:_:4_N="C~'E~1J~C~'H~E~M.~L~SJ:_'R~Y_L_A_B.....S....., I....N_C_. Phone: (770) 409-1444 3039 AmwiJer Road* Suite 100* Atlanta, GA 30360 Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-labs.netWNW.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant VogUe 44014 12/19/2003 01/06/2004 V.O. (50308/82608)

  • Appendix II SURROGATE PERCENT RECOVERY

SUMMARY

Water Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene (77-137) (72-138) (84-112) (77-125) ACL Sample # 210461 107 115 94 103 210462 106 116 96 104 210463 108 116 95 103 210464 108 114 95 102 210465 105 116 95 104 210473 106 114 95 105

    • Matrix Interference DO=Diluted Out

~-----

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 40~9~-1~44":""4:-----------------:::3~03::'::9~Am~w"::"i1e-r"=R-oa~d~."::S""':ul~te~1~00~.~A~t1-an~ta-. "::G~A~3~03~6~O-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 V.O. (50308/82608)

  • Appendix I SURROGATE PERCENT RECOVERY

SUMMARY

Water Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene (77-137) (72-138) (84-112) (77-125) ACL Sample # 210466 107 115 95 102 210467 107 115 94 103 210468 109 114 95 102 210469 107 115 96 104 210470 107 115 97 105 210471 106 115 95 103 210472 108 113 94 103

    • Matrix Interference DO=Diluted Out

'"v...."".,"'" chlorobenzene 20.00 0.00 19.82 SPIKE MSD MSD ADDED CONCENTRATION QC LIMITS COMPOUND (ual/) Cual/) REC RPD # RPD REC. 1,1-dichloroethene 20.00 21.79 109.0 3.2 14 (54-144) benzene 20.00 21.35 106.8 2.3 11 82-132 trichloroethene 20.00 21.16 105.8 2.6 14 73-128 toluene 20.00 22.43 112.2 0.5 13 (83-130 chlorobenzene 20.00 19.93 99.7 0.6 13 88-123 Values outside of QC limits RPD: 0 out of 5 outside limits Spike Recovery: 0 out of 10 outside limits Comments: ., I.

ADVANCED CHEMISTRY LABS, INC. GCIMS UNIT # 2 WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Sequence Date: 12-30-03 Matrix Spike - Sample No.: 210538 5061 SAMPLE MS MS ac. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (ua/I) (ualll (ua/l) REC REC. 1,1-dichloroethene 5.00 0.00 5.34 106.8 54-144 benzene 5.00 0.00 5.30 106.0 82-132 trichloroethene 5.00 0.00 5.19 103.8

73-128 toluene 5.00 0.00 5.56 111.2 83-130 chlorobenzene 5.00 0.00 4.90 98.0 88-123 SPIKE MSD MSD ADDED CONCENTRATION ac LIMITS COMPOUND (uO!J)

(ua/J) REC RPD RPD REC. 1,1-dichloroethene 5.00 5.18 103.6 3.0 14 54-144 benzene 5.00 5.19 103.8 2.1 11 82-132 trichloroethene 5.00 5.10 102.0 1.7 14

73-128 toluene 5.00 5.35 107.0 3.8 13 83-130 chlorobenzene 5.00 4.62 92.4 5.9 13 88-123
  1. Column to be used to flag recovery and RPD values with an asterisk Values outside of ac limits RPD:

0 out of 5 outside limits Spike Recovery: 0 out of 10 outside limits Comments:

SPIKE MSD MSD ADDED CONCENTRATION QC LIMITS COMPOUND (uo/l) (ua/l) REC RPD RPD REC. 1,1-dichloroethene 20.00 21.95 109.8 1.3 14 54-144) benzene 20.00 21.36 106.8 0.0 11 82-132) trichloroethene 20.00 21.07 105.4 2.6 14 ~3-128 toluene 20.00 22.20 111.0 0.2 13 83-130 chlorobenzene 20.00 19.27 96.4 0.1 13 88-123

  1. Column to be used to flag recovery and RPD values with an asterisk Values outside of QC limits RPD:

0 out of 5 outside limits Spike Recovery: 0 out of 10 outside limits Comments:

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40~9~-1:-:44"':"4~---------------:3:":0~39:-A':""m"W1-::"le~r R~o-a-:d-*~S-:ui:-te-:1~00:-'-A~t1:-an-:ta-.~G:-:A-3~0~3':":60=- Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 a-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client ProJ #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Acid Extractables (8270C)

  • Appendix II Sample 10:

ACL Sample #: Blank Units: IJg/L Analvte Result PQL 4-Chloro-3-methylphenol Sal 20 2-Chlorophenol SOL 10 m & p-Cresol SOL 10 o-Cresol SOL 10 2.4-Dichlorophenol SOL 10 ._2.6-Dichlorophenol Sal 10 4-Dimethylphenol SOL 10 ....6-Dinitro-2-methylphenol Sal 50 2.4-Dinitrophenol SOL 50 2-Nitrophenol SOL 10 4-Nitrophenol SOL 50 Pentachlorophenol SOL 50 Phenol BOL 10 2.3,4.6-Tetrachlorophenol SOL 10 2,4,5-Trichlorophenol BOL 10 2.4.6-Trichlorophenol SOL 10 BOl =Below Ouanlilatlon LimR J=less lIIan Quanlftalion limit, A\\lIlroxinale Value POL =Practical Quanlitation linit Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12122/2003 12/23/2003 RB

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 40!:':9~.1~4~44~--------------~3:":0~3':"9~A-m-w'::"i1e-r-=R~oa-d':".~S~u~jte~10:":0~*~A~t1-an~ta-.~GA~3~0~3~60~ Fax: (770) 409*1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACl Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II Sample 10:

Matrix: Water Date Sampled: Date Extracted: 12/2212003 Date Analyzed: 12123/2003 ACl Sample #: Blank Units: ~g/L Analyst: RP Analyte Result PQl Analyte Result Pgl Acenaphthene Sal 10 Diethyl phthalate Sal 10 Acenaphthylene Sal 10 Dimethoate Sal 10 Acetophenone Sal 10 Dimethyl phthalate Sal 10 2-Acetylaminofluorene sal 20 p-(Dimethylamino)azobenzene Sal 10 4-Aminoblphenyl Sal 20 7,12-Dimethylbenz(a)anthracene Sal 10 Anthracene Sal 10 3,3'-Dimethylbenzidine Sal 10 1enzo(a)anthracene sal 10 m-Dinitrobenzene Sal 20 denzo(a)pyrene Sal 10 2,4-Dinitrotoluene Sal 10 Senzo(b)fluoranthene Sal 10 2,6-Dinitrotoluene Sal 10 Senzo(g,h,i)perylene Sal 10 Diphenylamine Sal 10 Senzo(k)fluoranthene Sal 10 Disulfoton SOL 10 Benzyl alcohol Sal 20 Ethyl methanesulfonate SOL 20 Sis(2-chloroethoxy)methane SOL 10 Famphur SaL 20 Sis(2-ehloroethyl)ether SOL 10 Fluoranthene SaL 10 Sis(2-chloroisopropyl)ether Sal 10 Fluorene SaL 10 Sis(2-ethylhexyl)phthalate Sal 10 Hexachlorobenzene SaL 10 4-Sromophenyl phenyl ether Sal 10 Hexachlorobutadiene SOL 10 Sutyl benzyl phthalate SOL 10 Hexachlorocyclopentadiene SOL 10 p-Chloroaniline Sal 20 Hexachloroethane Sal 10 Chlorobenzilate Sal 10 Hexachloropropene SaL 10 2-Chloronaphthalene SaL 10 Indeno(1,2,3-cd)pyrene SOL 10 4-Chlorophenyl phenyl ether Sal 10 Isodrin SaL 20 Chrysene Sal 10 Isophorone BOL 10 Di-n-butyl phthalate Sal 10 Isosafrore Sal 10 Di-n-octyl phthalate Sal 10 Kepone SaL 20 Dial/ate Sal 10 Malathion SOL 50 Dibenz(a,h)anthracene SOL 10 Methapyrilene Sal 100 Dibenzofuran Sal 10 Methyl methanesulfonate Sal 10 1,2-Dichlorobenzene Sal 10 Methyl parathion SOL 10 1,3-Dichlorobenzene Sal 10 3-Methylcholanthrene SaL 10 1A-Dichlorobenzene Sal 10 2-Methylnaphthalene Sal 10 3,3'-Dichlorobenzidine Sal 20 Naphthalene SOL 10 BOl =Below OuantilaUon lim~ J =less than QuanUtation limit, Approximate Value POL =Practical QuanlitaUon Limit

ADVANCED CHEMISTRY LABS, INC. IACL I Phone: (770) 40:-:9~-1~44~4~---------------3~0~3~9~A-m-w~ile-r"'=R~o-ad"':'"*~S~u~it-e~100~*~A~t1~an-ta-,~G~A~30~3--60~ Fax: (770) 409-1844 P.O. Box 88610* Atlanta, GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemlstrylabs.com Client:

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Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Base Neutral Extractables (8270C) - Appendix II Sample 10: ACL Sample #: Blank Analyte 1,4-Naphthoquinone 1-Naphthylamine 2-Naphlhylamine S-Nilro-o-loluidine 2-Nitroaniline 3-Nitroaniline ~-Nitroanjljne Nitrobenzene N-Nilroso-di-n-butylamine N-Nilrosodielhylamine N-Nilrosodimelhylamine N-Nilrosodiphenylamine N-Nilrosodipropylamine N-Nitrosomethylethylamine N-Nilrosopiperidine N-Nilrosopyrrolidine Parathion Penlachlorobenzene Penlachloronilrobenzene Phenacelin Phenanlhrene p-Phenylenediamine Phorale Pronamide Pyrene Safrole 1,2,4,S-Telrachlorobenzene Thionazin 0-Toluidine 1,2,4*Trichlorobenzene o,o,o-Triethyl phosphorothioate 1,3,5-Trinilrobenzene BOl =Below Ouanlilation Limit J =Less lhan Ouanlilalion liM, Approximate Value PQl =Practical Quanlkalion Limit Units: Result SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL SOL 1J9/L PQL 10 10 10 10. 50 50 20 10 10 20 10 10 10 10 20 40 20 10 20 20 10 10 10 10 10 10 10 20 10 10 50 10 Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/22/2003 1212312003 RP

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 409~*1~44~4--------------"'!"'30~3"'!"'9~A-mw~i~le~r R~o-ad~*S~u~ite-1~0"'!"'0-*A-t-lan-ta-.~G"'A""'!3"'03~6"'0-Fax: (770) 409*1844 P.O. Box 88610

  • Atlanta. GA 30356 e-mail: acl@acl*labs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Acid Extractables (8270C)

  • Appendix II SURROGATE PERCENTRECOVERY

SUMMARY

Water Phenol-d6 2-Fluorophenol 2,4,6-Trlbromophenol (10-94) (21-100) (10-123) ACL Sample # 210461 14 24 35 210462 17 28 49 210463 17 27 49 210464 16 24 56 .. Matrix Interference DO=Diluted Out

IA CL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40~9~.1~44':"":4~-------------~30::'::3~9"":'A"mWl-'*!:""'le""":r R='"o....ad"':'-:*S=:-u~ite"1:"::0~0-.A~tl:-an"":'ta-,~G~A~3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Base Neutral Extractables (8270C)

  • Appendix II SURROGATE PERCENT RECOVERY

SUMMARY

Water Nltrobenzene-d5 2.fluorobiphenyl Terphenyl-d14 (35-114) (43-116) (33-141) ACL Sample # 210461 41 51 62 210462 54 64 64 210463 53 68 73 210464 53 69 65

  • " Matrix Interference DO=Diluted Out

ADVANCED CHEMISTRY LABS, INC. SEMI-VOL GCIMS UNIT # 4 ACID EXTRACTABLES (8270C) WATER SEMI-VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Sequence Date: 12-23-03 Matrix Spike

  • Sample No.:

LCS122203 SPIKE SAMPLE MS MS ac. COMPOUND ADDED CONCENTRATION CONCENTRATION LIMITS (ua/L) (!JQ/L) (IJQ/L) REC REC. Pentachlorophenol 200 0 77 38.5 9-103) Phenol 200 0 39 19.5 12-89) 2-Chlorophenol 200 0 98 49.0 27-123) 4-Chloro-3-methylphenol 200 0 134 67.0 23-97) 4-Nitrophenol 200 0 -42 21.0 10-80) SPIKE MSD MSD ac LIMITS COMPOUND ADDED CONCENTRATION (!JaiL) (!JaIL) REC RPD RPD REC. Pentachlorophenol 200 74 37.0 4.0 50 9-103) Phenol 200 35 17.5 10.8 42 12-89) 2-Chlorophenol 200 88 44.0 10.8 40 27-123) 4-Chloro-3-methylphenol 200 133 66.5 0.7 42 23-97) 4-Nitrophenol 200 45 22.5 6.9 50 10-80)

  1. Column to be.used to flag recovery and RPD values with an asterisk Values outside of ac limits RPD:

0 out of 5 outside limits Spike Recovery: 0 out of 10 ~utside limits Comments:

ADVANCED CHEMISTRY LABS, INC. SEMI-VOL GC/MS UNIT # 4 BASE/NEUTRAL EXTRACTABLES (8270C) WATER SEMI-VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY Sequence Date: 12-23-03 Matrix Spike - Sample No.: LCS122203 SPIKE SAMPLE MS MS ac. ADDED CONCENTRATION CONCENTRATION LIMITS COMPOUND (IJr::I/L) (IJQ/L) (lJp/U REC REC. 1,2,4-Trichlorobenzene 100 0 75 75.0 39-98) Acenaphthene 100 0 63 63.0 46-118 2,4-Dinitrotoluene 100 0 73 73.0 24-96) Di-n-butyl phthalate 100 0 76 76.0 11-117 Pyrene 100 0 68 68.0 26-127 N-Nitrosodi-n-oroovlamine 100 0 67 67.0 41-116 1,4-Dichlorobenzene 100 0 59 59.0 36-97) SPIKE MSD MSD ADDED CONCENTRATION ac LIMITS COMPOUND lJoIL IJr::IlL REC RPD RPD REC. 1.2.4-Trichlorobenzene 100 74 74.0 1.3 28 39-98) Acenaohthene 100 62 62.0 1.6 31 46-118 2,4-Dinitrotoluene 100 72 72.0 1.4 38 24-96) Di-n-butvl phthalate 100 76 76.0 0.0 40 11-117 IPyrene 100 70 70.0 2.9 31 26-127 N-Nitrosodi-n-propyJamine 100 62 62.0 7.8 38 41-116 1,4-Dichlorobenzene 100 57 57.0 3.4 28 36-97)

  1. Column to be used to flag recovery and RPD values with an asterisk Values outside ofac limits RPD:

0 out of 7 outside limits Spike Recovery: 0 out of 14 outside limits Comments:

IACL I ADVANCED CHEMISTRYLABS, INC. Phone: (770) 40='=9~-1~44":"'4:----------------~3~03='=9~A:-m-w~i1-er-:R~o-ad~. S~u"':':'it-e~100~.""':'A~t1a-n~ta-. '=G":"'A-:3~03~6~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.aclvancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Pesticides/PCBs (8081A18082)

  • Appendix II Sample 10:

ACL Sample #: Blank Units: ~g/L Analyte Result PQL Aldrin SOL 0.05 Arochlor-1 016 BOl 0.50 Arochlor-1221 BOl 0.50 Arochlor-1232 SOL 0.50 Arochlor-1242 BOl 0.50 ,_, Arochlor*1248 SOL 0.50 \\rochlor-1254 SOL 0.50 Arochlor-1260 BOl 0.50 a-SHC SOL 0.05 b-SHC SOL 0.05 d-SHC BOl 0.05 g-SHC BOl 0.05 Chlordane SOL 0.10 4,4'-000 SOL 0.05 4,4'-00E SOL 0.05 4.4'-00T SOL 0.05 Dieldrin BOl 0.05 Endosulfan I SOL 0.05 Endosulfan II SOL 0.05 Endosulfan sulfate SOL 0.05 Endrin SOL 0.05 Endrin aldehyde SOL 0.05 Heptachlor SOL 0.05 Heptachlor epoxide BOl 0.05 Methoxychlor BOl 0.05 Toxaphene Sal 2.00 BQL =Below Quanlilalion limR J =less than Quanlilalion lmR. APPlOxmate Value POL =Praclical Ouantitation lin~ Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/22/2003 12/29/2003 SS

IA CL I ADVANCED CHEMISTRYLABS, INC Phone: (770) 409~*1~444~-------------~30~3~9~A-mw""':i':"'le-:r R~o-ad"':"'*""':S~u~ite-1~0~0 -.A~t1:-an'"'!"ta-.~G"':"'A~3~03~6~0-Fax: (770) 409*1844 P.O. Box 88610* Atlanta. GA 30356 a-mail: acl@acl-Iabs.net www.advancedchemlstrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client ProJ #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Pesticides/PCBs (8081A18082). Appendix II SURROGATE PERCENT RECOVERY

SUMMARY

Water TCMX DCBP (30-130) (30-130) ACL Sample # 210461 217** 95 210462 232** 89 210463 67 90 210464 63 93 .. Matrix Interference DO=Diluted Out

Advanced Chemistry Labs Pesticides Spike/Spike Dup. Report(EPA Method 60B / SW-B46 Method BOB1A) Instrument 10: HP5890A-ECD Column: RTx-CLPII, 30m, 0.42tJm, O.53mm ACL #: LCSW122203 Matrix: Water Extraction Date: 12122103 Analysis Date: 12129/03 Initial Volume: 1000.0 ml Final Volume: 1 ml Dilution Factor: 1 Unit: tfg/L orppb Pestlelde I R.T. I AI'H IActualI% Rec. Cone. I R.T. I Area IActua'I"Rec. \\SamP/e %D I MS MS MS MS MSD MSD MSD MSD Cone. (RPD) TCMX(SS#1) 7.354 640086 0.314 62.79% 0.500 7.365 714419 0.350 70.0'% 0.000 10.98% a-BHC 8.968 1739790 0.640 127.96% 0.500 8.977 1948650 0.717 143.32% 0.000 11.33% g-BHC (Lindane) 10.016 1592170 0.633 126.60% 0.500 10.025 1737480 0.691 138.16% 0.000 8.73% b-BHC 10.269 624078 0.505 101.00-" 0.500 10.278 653153 0.529 105.70% 0.000 4.55% d-BHC 11.215 1482970 0.741 14'.27% 0.500 11.224 1513520 0.757 151.33% 0.000 2.04% Heptachlor 11.379 1653580 0.531 106.19% 0.500 11.387 1839150 0.591 118.10-" 0.000 10.63% Aldrin 12.489 1731550 0.687 137.31% 0.500 12.497 1888460 0.749 149.75% 0.000 8.67% Heptachlor Epoxide 14.479 1576570 0.658 131.55% 0.500 14.486 1627330 0.679 135.79% 0.000 3.17°k a-Endosulfan I 15.936 1460990 0.653 130.60% 0.500 15.942 1492260 0.667 133.39"" 0.000 2.12% ODE 16.258 1540210 0.663 132.57% 0.500 16.264 1540140 0.663 132.57% 0.000 0.00% Dieldrin 16.945 1439470 0.632 126.49% 0.500 16.951 1456500 0.640 127.99% 0.000 1.18% Endrin 18.104 1181450 0.650 130.09"" 0.500 18.109 1193420 0.657 131.41% 0.000 1.01% DOD 18.455 1293590 0.806 161.11% 0.500 18.461 1280260 0.797 159.45% 0.000 1.04% b-Endosulfan II 18.914 1323020 0.645 129.07% 0.500 18.919 1314610 0.641 128.25% 0.000 0.64% DDT 19.630 1025390 0.605 121.06% 0.500 19.635 1039340 0.614 122.70% 0.000 1.35% Endrin Aldehyde 20.183 1031110 0.722 1.....34% 0.500 20.187 1045050 0.731 146.29% 0.000 1.34% Endosulfan Sulfate 21.279 1176900 0.684 136.75% 0.500 21.283 1179280 0.685 137.03% 0.000 0.20% Methoxychlor 22.411 534387 0.548 109.65% 0.500 22.415 541706 0.556 111.15% 0.000 1.36% Mirex 23.581 562785 0.258 51.62% 0.500 23.583 562319 0.258 51.58% 0.000 0.080/0 Endrin Ketone 23.751 1257640 0.596 119.23"" 0.500 23.752 1261190 0.598 119.54% 0.000 0.27% DCBP(SS#2) 31.585 955235 0.390 78.05% 0.500 31.586 954099 0.390 n,96% 0.000 0.12%

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 40~9-~1~444~--------------~3~03~9~Am~w"::'i1e-r~R~oa-d~'~S~ui~te~1~00~' A~tl~an~ta-.~G~A~3~0~36~0-Fax: (770) 409-1844 P.O. Box 88610* Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12119/2003 01/06/2004 Chlorinated Herbicides (8151A)

  • Appendix II Sample 10:

ACL Sample #: Blank Units: ",giL Analvte Result PQL 2,4-0 BOl 1.0 Oinoseb BOl 1.0 2.4,5-TP (Silvex) BOl 1.0 2,4,5-T BOl 1.0 BOl=Below Quantitatlon limit J =less than Quantitallon limit, Approximate Value pal =Practical auantilation limit Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/23/2003 12/29/2003 SS

IACL I ADVANCED CHEMISTRYLABS, INC Phone: (770) 40~9-~1~44~4~-------------~3~03~9~Am-w~i1e-r ~Ro-a"':"d-'S~u~ite~10~0-' ~AtI'!'"'a-nta-.""!!!G~A~3~0~36~0-Fax: (770) 409-1844 P.O. Box 88610' Atlanta. GA 30356 a-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: Plant Vogtle ACL Project #: 44014 Date Received: 12/19/2003 Date Reported: 01/06/2004 Chlorinated Herbicides (8151A)

  • Appendix II SURROGATE PERCENT RECOVERY

SUMMARY

Water oeAA (30-130) ACLSample# 210461 69 210462 68 210463 67 210464 66 ... Matrix Interference DO=Diluted OUt

Advanced Chemistry Labs Herbicides Spike/Spike Dup. Report SW-846 Method 8151A Instrument 10: HP5890A-ECD/FID Column: RTx-1, 30m, O.25pm, O.25mm 10 ACL #: LCSW122303 Matrix: Water Extraction Date: 12123/03 Analysis Date: 12/29/03 Initial Volume: 1000 ml FmalVowme: 4 ml Dilution Factor: 1 Unit: WIL or ppb Herbicide Spike I R.T. I Area ISpike Cone. I Actual I% Recovery RPD OCAA(SS) 18.993 1183812 16.000 9.865 61.66% 3.96% 2,4-0 21.438 632680 4.000 3.197 79.94% 8.25% Silvex 23.593 747029 0.800 0.683 85.40% 5.00% 2.4,5-T 23.923 627427 0.800 0.620 77.52% 5.05% Oinoseb 25.000 422722 0.800 0.139 17.35% 18.91% Herbicide Spike Dup. I R.T. I Area ISpike Cone. I Actual I% Recovery Cone. OCAA(SS) 18.994 1137886 16.000 9.483 59.27% 0.000 2,4-0 21.438 582581 4.000 2.944 73.61% 0.000 Silvex 23.594 710621 0.800 0.650 81.24% 0.000 2.4,5-T 23.924 596503 0.800 0.590 73.70% 0.000 Oinoseb 25.001 349677 0.800 0.115 14.35% 0.000 °Herb. Calculation based on curve prep. on 12/16103

ADVANCED CHEMISTRYLABS, INC. IACL I Phone: (770) 409-~1~4~44~--------------~3~03~9~A~m-w~i1~er~R~o-ad~* S~u~it-e-10~0~*~A"t1a-n-ta-. ~G"A~3""'!"0"!""36"""'0-Fax: (770) 409*1844 P.O. Box 88610

  • Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemistrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna, GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant VogUe 44014 12119/2003 12/30/2003 Appendix II Metals (6010B/7470A/7841) Sample 10: ACL Sample #: Blank Units: mg/L Analyte Result PQL Antimony Sal 0.006 Arsenic Sal 0.010 Sarium sal 0.020 Seryllium sal 0.004 Cadmium Sal 0.005 Chromium Sal 0.020 ~obalt sal 0.050 Copper Sal 0.020 lead Sal 0.010 Mercury Sal 0.0005 Nickel Sal 0.020 Selenium Sal 0.040 Silver Sal 0.010 Thallium Sal 0.002 Tin Sal 0.025 Vanadium Sal 0.050 Zinc Sal 0.020 eOl :: Below Ouanlilalion limit J :: less than Ouanlitalion limit. Approximate Value PQL :: Practical Quanlilalion limit Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12130/2003 SW/AD/JR

ADVANCED CHEMISTRY LABS, INC. Appendix II Metals Water Matrix Spike for Method (6010B/7470A) Sample 10 ACL Sample Number L_C"-S SPIKE SAMPLE MATRIX SPIKE MS MS ADDED RESULT RESULT REC RANGE COMPOUND (mg/L) (mg/L) (mg/L) (%) (%) Antimonv 0.040 0.000 0.038 94 75--125 Arsenic 0.100 0.000 0.108 108 75--125 Barium 1.000 0.000 0.753 75 75--125 Beryllium 0.100 0.000 0.105 105 75-125 Cadmium 0.025 0.000 0.025 101 75--125 Chromium 0.100 0.000 0.102 102 75--125 Cobalt 0.100 0.000 0.099 99 75--125 Copper 0.100 0.000 0.107 107 75--125 Lead 0.100 0.000 0.097 97 75-125 Mercury 0.0020 0.000 0.0022 109 75--125 Nickel 0.100 0.000 0.100 100 75--125 Selenium 0.025 0.000 0.022 87 75--125 Silver 0.020 0.000 0.019 94 75--125 Thallium 0.040 0.000 0.040 100 75--125 Tin 0.200 0.000 0.192 96 75--125 Vanadium 0.250 0.000 0.249 100 75--125 Zinc 0.100 0.000 0.107 107 75--125 Comment: ---'~-~'--'~

IACL I ADVANCED CHEMISTRY LABS, INC. Phone: (770) 40::-:9~-1~4~44O:----------------~3~0~39~A:-m-w-::il~er~R~o-a~d -.S="u"":':it-e~10~0:-*~A~t1a-n~ta-.~G~A~3~0~36~0-Fax: (770) 409-1844 P.O. Box 88610

  • Atlanta. GA 30356 e-mail: acl@acl-Iabs.net www.advancedchemlstrylabs.com Client:

Contact:

Genesis Project 1258 Concord Rd. Smyrna. GA 30080-0000 Mr. Mark Mitchell Client Proj #: ACL Project #: Date Received: Date Reported: Plant Vogtle 44014 12/19/2003 01/06/2004 Appendix I Metals (60108/7841) Sample 10: ACL Sample #: Blank Units: mg/L Analvte Result PQL Antimony BOl 0.006 Arsenic BOl 0.010 Barium BOl 0.020 Beryllium BOl 0.004 Cadmium BOl 0.005 -Chromium BOl 0.020 obalt BOl 0.050 Copper BOl 0.020 lead BOl 0.010 Nickel BOl 0.020 Selenium BOl 0.040 Silver BOl 0.010 Thallium BOl 0.002 Vanadium BOl 0.050 Zinc BOl 0.020 BOl =Below Quantilalion linit J =less than Quantilalion limit, AlllIfOXimale Value POL =Pradical Ouanlilalion Limit Matrix: Date Sampled: Date Extracted: Date Analyzed: Analyst: Water 12/3012003 SW/AD

Sample 10: ADVANCED CHEMISTRY LABS, INC. Appendix I Metals Water Matrix Spike for Method (601 OBn841) GWC-11/MW-11 ACL Sample Number :__--.-;;;2;.;.104~7..:;;;,2 SPIKE SAMPLE MATRIX SPIKE MS MS ADDED RESULT RESULT REC RANGE COMPOUND (mg/L) (mg/L) (mg/L) (%) (%) Antimony 0.040 0.000 0.041 103 75--125 Arsenic 0.100 0.000 0.100 100 75--125 Barium 1.000 0.022 0.786 76 75--125 Bervllium 0.100 0.000 0.104 104 75**125 Cadmium 0.025 0.000 0.025 101 75--125 Chromium 0.100 0.000 0.106 106 75--125 Cobalt 0.100 0.000 0.101 101 75-125 Copper 0.100 0.000 0.100 100 75--125 Lead 0.100 0.000 0.099 99 75--125 Nickel 0.100 0.000 0.103 103 75--125 Selenium 0.025 0.000 0.024 94 75--125 Silver 0.020 0.000 0.019 97 75--125 Thallium 0.040 0.000 0.038 96 75--125 Vanadium 0.250 0.000 0.255 102 75--125 linc 0.100 0.000 0.114 114 75-125 Comment:

I-A-c-L-I__~~~~~~~~~A~D~\\I.~~~N~CE~D~c~H~EM~/~S~~~R~Y~LA~B=!!iS~I~/N~C~. 3039 Amwiler Road' Suite 100* Atlanta, GA 30360. P. O. Box 88610* Atlanta, GA 30356. (770) 409-1444

  • Fax (770) 409-1844 Company Name:

Company AddresS: Phone #: 7'10" 311-7).17 Site Location: CHAIN-OF CUSTODY RECORD AND ANALYSIS REQUEST Remarks Ql -0 0 Cl

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.2 z .I J j j Ii V .J .I ~rDJ' rks ./ IJ':"1J LV'!cC?d /.,) 5,,1<-</,-/'1<-1 (;4 (;.4 Aurte r,o~ ~ Project Manager: Client Project (#) PIWlf VOJlle r ~ Il/lCA/-i /vI,'Ul':-I/ (Name) I~ ltr- -{ ~ I attest that the proper field sampling Sampler Name (Print): ~ I"i .~ I~ ~ : ~ 1_ ~~ ~ procedures were used during the / JI I':§ ~ J\\I~ ~ ~ collection ofthese samples. ,JJ.)t -rJirtr:<P(5"n ~ III _~ 'Ii; ...; ~ ~ ct'1_~.Jl ~ I------...:..-w--r---M-a-tr-ix-------':":M~et:":"'h-o"':"d -"""-5--1-'--4........ ~~ L. 1 L. ""3 ~ "l..: ...... ~ Field ._~ '-,---,r--r--,-----r-+--r_p,...re_s.,..erv-r-ed-.--+-_a_m_p..-m_g--ll~$: ~ F;!I ~ ,-'~ l::i 1:)..... Sample J!l ,~~ j J ~ ;-:: ~ ~. ~:; "I 10 ~ ~ ~ J~ \\.J c:t.1"t: '<;t:.", '" j~I~t-S Q ~ ~ Fax~ CUSTODY RECORD RelinqUished by Sampler: jJ --fj Lj33 111/9~3 I /~~~ R_le_ce_lv_e_d.....;blY_:------ ~, Relinqui~-.: -i// / t./ Date Ti~ Received by: I Relinquished by : Date Time Received by ~al>.or:jl~q[Y,j ~

  • I.

Waybill# N*I1JLViJf1n1S 'oL//9,()3

ApPENDIX B - STATISTICAL ANALYSES

LANDFILL #2

Shapiro-Wilks Test of Normality Parameter: Trichlorofluoromethane All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =11; Samples =22 i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 x(i) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 5 6 x(n-i+1) 6 5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 x(n-1 +1 )-x(i)a(n-i+1) 3.5 0.459 2.5 0.3156 o 0.2571 o 0.2131 o 0.1764 o 0.1443 o 0.115 o 0.0878 o 0.0618 o 0.0368 o 0.0122 o o o oo ooo o -2.5 -3.5 b(i) 1.6065 0.789 oo o ooo o o o Sum of b values = 2.3955 Sample Standard Deviation = 0.89612 W Statistic =0.340284 5% Critical value of 0.911 exceeds 0.340284 Evidence of non-normality at 95% level of significance 1% Critical value of 0.878 exceeds 0.340284 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Trichlorofluoromethane Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-2/MW-2 7/30/2002 BQL2.5 10.5 9/24/2002 BQL2.5 10.5 10/21/2002 BQL2.5 10.5 12/4/2002 BQL2.5 10.5 6/25/2003 BQL2.5 10.5 12/17/2003 BQL2.5 10.5 Rank Sum = 63 Rank Mean = 10.5 Background Rank Sum = 63 Background Rank Mean = 10.5 Compliance Wells WelllD Date Result Rank GWB-4/MW-4 7/30/2002 5 21 9/24/2002 BQL2.5 10.5 10/21/2002 BQL2.5 10.5 12/4/2002 - BQL2.5 10.5 6/25/2003 BQL2.5 10.5 12/17/2003 6 22 Rank Sum = 85 Rank Mean = 14.1667 GWC-11/MW-117/30/2002 BQL2.5 10.5 9/24/2002 BQL2.5 10.5 10/21/2002 BQL2.5 10.5 12/4/2002 BQL2.5 10.5 6/25/2003 BQL2.5 10.5 12117/2003 BQL2.5 10.5 Rank Sum = 63 Rank Mean = 10.5 GWC-3/MW-3 7/30/2002 BQL2.5 10.5 9/24/2002 BQL2.5 10.5 12/4/2002 BQL2.5 10.5 12/17/2003 BQL2.5 10.5 Rank Sum = 42 Rank Mean = 10.5 Calculation Results: Kruskal-Wallis H Statistic =1.3913 Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 5.5873

95% Confidence comparison value is 7.81472 at 3 degrees offreedom 1.3913 < 7.81472 indicating no significant group difference at 5% significance level 5.5873 < 7.81472 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Barium All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =11; Samples =22 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 x(i) 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.015 0.018 0.02 0.02 0.0205 0.021 0.021 0.021 0.022 0.025 0.027 0.085 x(n-i+1) 0.085 0.027 0.025 0.022 0.021 0.021 0.021 0.0205 0.02 0.02 0.018 0.015 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.075 0.017 0.015 0.012 0.011 0.011 0.011 0.0105 0.01 0.01 0.003 -0.003 -0.01 -0.01 -0.0105 -0.011 -0.011 -0.011 -0.012 -0.015 -0.017 -0.075 0.459 0.3156 0.2571 0.2131 0.1764 0.1443 0.115 0.0878 0.0618 0.0368 0.0122 b(i) 0.034425 0.0053652 0.0038565 0.0025572 0.0019404 0.0015873 0.001265 0.0009219 0.000618 0.000368 3.66e-005 Sum of b values = 0.0529411 Sample Standard Deviation = 0.0158984 W Statistic = 0.528029 5% Critical value of 0.911 exceeds 0.528029 Evidence of non-normality at 95% level of significance 1% Critical value of 0.878 exceeds 0.528029 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Barium Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-2/MW-2 7/3012002 0.027 21 9/24/2002 BQLO.01 5.5 10/21/2002 BQLO.01 5.5 12/4/2002 0.015 11 6/25/2003 BQLO.01 5.5 12117/2003 BQLO.01 5.5 Rank Sum =54 Rank Mean =9 Background Rank Sum =54 Background Rank Mean =9 Compliance Wells WelllD Date Result Rank GWB-4/MW-4 7/3012002 0.021 16 9/24/2002 0.021 17 10/21/2002 0.021 18 12/412002 - 0.0205 15 6/25/2003 BQLO.01 5.5 12/17/2003 BQLO.01 5.5 Rank Sum =77 Rank Mean =12.8333 GWC-11/MW-117/30/2002 0.085 22 9/24/2002 0.02 13 10/21/2002 0.025 20 12/412002 0.018 12 6/25/2003 BQLO.01 5.5 12/17/2003 0.022 19 Rank Sum =91.5 Rank Mean =15.25 GWC-3/MW-3 7/3012002 BQLO.01 5.5 9/24/2002 BQLO.01 5.5 12/4/2002 0.02 14 12/17/2003 BQLO.01 5.5 Rank Sum =30.5 Rank Mean =7.625 Calculation Results: Kruskal-Wallis H Statistic =4.56769 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =5.03697

95% Confidence comparison value is 7.81472 at 3 degrees offreedom 4.56769 < 7.81472 indicating no significant group difference at 5% significance level 5.03697 < 7.81472 indicating no significant group difference at 5% significance level when adjusted for ties

LANDFILL #3

Shapiro-Wilks Test of Normality Parameter: Chlorobenzene All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K = 18; Samples = 36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 7 8 9 10 19 x(n-i+1) 19 10 9 8 7 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 16.5 7.5 6.5 5.5 4.5 oo o o o o o o o o o o o o o o o o o ooo oo oo -4.5 -5.5 . -6.5 -7.5 -16.5 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 6.7122 2.10975 1.56975 1.16655 0.84735 o o o o o o o o o o o o o Sum of b values = 12.4056 Sample Standard Deviation =3.27627 W Statistic = 0.409646 5% Critical value of 0.935 exceeds 0.409646 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.409646 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Chlorobenzene Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQL2.5 16 9/24/2002 BQL2.5 16 10/21/2002 - BQL2.5 16 12/3/2002 BQL2.5 16 6/24/2003 BQL2.5 16 12/17/2003 BQL2.5 16 Rank Sum =96 Rank Mean =16 GWA-7/MW-7 7/30/2002 - BQL2.5 16 9/24/2002 BQL2.5 16 10/21/2002 BQL2.5 16 12/3/2002 BQL2.5 16 6/24/2003 BQL2.5 16 12/17/2003 BQL2.5 16 Rank Sum =96 Rank Mean =16 Background Rank Sum =192 Background Rank Mean =16 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQL2.5 16 9/24/2002 BQL2.5 16 10/21/2002 BQL2.5 16 1213/2002 BQL2.5 16 6/24/2003 BQL2.5 16 12/17/2003 BQL2.5 16 Rank Sum =96 Rank Mean =16 GWC-13/MW-137/30/2002 BQL2.5 16 9/24/2002 BQL2.5 16 10/21/2002 BQL2.5 16 12/3/2002 BQL2.5 16 6/2412003 - BQL2.5 16 12117/2003 - BQL2.5 16 Rank Sum =96 Rank Mean =16 GWC-14/MW-147/30/2002 BQL2.5 16 9/24/2002 - 8 33 10/21/2002 9 34 12/3/2002 10 35

6/24/2003 7 32 12/17/2003 19 36 Rank Sum =186 Rank Mean =31 GWC-5/MW-5 7/3012002 BQL2.5 16 9/24/2002 BQL2.5 16 10/21/2002 BQL2.5 16 12/3/2002 BQL2.5 16 6/24/2003 BQL2.5 16 12/17/2003 BQL2.5 16 Rank Sum =96 Rank Mean =16 Calculation Results: Kruskal-Wallis H Statistic =10.1351 Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 28.0249 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 10.1351 > 9.48773 indicating a significant group difference at 5% significance level 28.0249 > 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o o 15 o Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 16 Well Mean Rank GWB-6/MW-6 16 GWC-13/MW-1316 GWC-14/MW-1431 GWC-5/MW-5 16 Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o o 15 o Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 16 Well Mean Rank GWB-6/MW-6 16 GWC-13/MW-1316 GWC-14/MW-1431 GWC-5/MW-5 16

Shapiro-Wilks Test of Normality Parameter: 1,4-Dichlorobenzene All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K = 18; Samples = 36 i x(i) x(n-i+1 ) x(n-1 +1 )-x(i)a(n-i+1) b(i) 1 2.5 39 36.5 0.4068 14.8482 2 2.5 36.5 34 0.2813 9.5642 3 2.5 35 32.5 0.2415 7.84875 4 2.5 33 30.5 0.2121 6.46905 5 2.5 20 17.5 0.1883 3.29525 6 2.5 5 2.5 0.1678 0.4195 7 2.5 5 2.5 0.1496 0.374 8 2.5 5 2.5 0.1331 0.33275 9 2.5 5 2.5 0.1179 0.29475 10 2.5 5 2.5 0.1036 0.259 11 2.5 2.5 0 0.09 0 12 2.5 2.5 0 0.077 0 13 2.5 2.5 0 0.0645 0 14 2.5 2.5 0 0.0523 0 15 2.5 2.5 0 0.0404 0 16 2.5 2.5 0 0.0287 0 17 2.5 2.5 0 0.0172 0 18 2.5 2.5 0 0.0057 0 19 2.5 2.5 0 20 2.5 2.5 0 21 2.5 2.5 0 22 2.5 2.5 0 23 2.5 2.5 0 24 2.5 2.5 0 25 2.5 2.5 0 26 2.5 2.5 0 27 5 2.5 -2.5 28 5 2.5 -2.5 29 5 2.5 -2.5 30 5 2.5 -2.5 31 5 2.5 -2.5 32 20 2.5 -17.5 33 33 2.5 -30.5 34 35 2.5 -32.5 35 36.5 2.5 -34 36 39 2.5 -36.5 Sum of b values =43.7055 Sample Standard Deviation = 10.7832 W Statistic =0.469364 5% Critical value of 0.935 exceeds 0.469364 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.469364 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test IParameter: 1,4-Dichlorobenzene Original Data (Not Transformed) Non-Detects Replaced with 1/2 Dl Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BOl2.5 16 9/24/2002 BOl2.5 16 10/21/2002 - BOl2.5 16 12/3/2002 BOL2.5 16 6/24/2003 BOl5 16 12/17/2003 BOl5 16 Rank Sum =96 Rank Mean = 16 GWA-7/MW-7 7/30/2002 - BOl2.5 16 9/24/2002 BOl2.5 16 10/21/2002 BOl2.5 16 12/3/2002 BOl2.5 16 6/2412003 BOl2.5 16 12/17/2003 BOl2.5 16 Rank Sum =96 Rank Mean =16 Background Rank Sum = 192 Background Rank Mean = 16 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BOl2.5 16 9/24/2002 BOl2.5 16 10/21/2002 BOl2.5 16 12/3/2002 BOL2.5 16 6/2412003 BOl2.5 16 12/17/2003 BOL2.5 16 Rank Sum = 96 Rank Mean =16 GWC-13/MW-137/30/2002 BOl2.5 16 9/24/2002 BOl2.5 16 10121/2002 BOl2.5 16 12/3/2002 BOL2.5 16 6/24/2003 - BOl5 16 12117/2003 - BOl5 16 Rank Sum =96 Rank Mean =16 GWC-14/MW-147/30/2002 20 32 9/24/2002 - 36.5 35 10/21/2002 35 34 12/3/2002 39 36

6/24/2003 12/17/2003 Rank Sum =186 Rank Mean =31 BQL5 33 16 33 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 1213/2002 6/24/2003 12/17/2003 Rank Sum =96 Rank Mean = 16 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 16 16 16 16 16 16 Calculation Results: Kruskal-Wallis H Statistic =10.1351 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =28.0249 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 10.1351 > 9.48773 indicating a significant group difference at 5% significance level 28.0249> 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o o 15 o Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 16 Well Mean Rank GWB-6/MW-6 16 GWC-13/MW-1316 GWC-14/MW-1431 GWC-5/MW-5 16 Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg oo 15 o Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 16 Well Mean Rank GWB-6/MW-6 16 GWC-13/MW-1316 GWC-14/MW-1431 GWC-5/MW-5 16

Shapiro-Wilks Test of Normality Parameter: 1,1-Dichloroethane All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 Dl K =18; Samples =36 i x(i) x(n-i+1) x(n-1+1 )-x(i)a(n-i+1) b(i) 1 2.5 21 18.5 0.4068 7.5258 2 2.5 20.5 18 0.2813 5.0634 3 2.5 17 14.5 0.2415 3.50175 4 2.5 16 13.5 0.2121 2.86335 5 2.5 13 10.5 0.1883 1.97715 6 2.5 10 7.5 0.1678 1.2585 7 2.5 10 7.5 0.1496 1.122 8 2.5 9 6.5 0.1331 0.86515 9 2.5 7 4.5 0.1179 0.53055 10 2.5 6 3.5 0.1036 0.3626 11 2.5 6 3.5 0.09 0.315 12 2.5 2.5 0 0.077 0 13 2.5 2.5 0 0.0645 0 14 2.5 2.5 0 0.0523 0 15 2.5 2.5 0 0.0404 0 16 2.5 2.5 0 0.0287 0 17 2.5 2.5 0 0.0172 0 18 2.5 2.5 0 0.0057 0 19 2.5 2.5 0 20 2.5 2.5 0 21 2.5 2.5 0 22 2.5 2.5 0 23 2.5 2.5 0 24 2.5 2.5 0 25 2.5 2.5 0 26 6 2.5 -3.5 27 6 2.5 -3.5 28 7 2.5 -4.5 29 9 2.5 -6.5 30 10 2.5 -7.5 31 10 2.5 -7.5 32 13 2.5 -10.5 33 16 2.5 -13.5 34 17 2.5 -14.5 35 20.5 2.5 -18 36 21 2.5 -18.5 Sum of b values =25.3853 Sample Standard Deviation =5.46286 W Statistic =0.616956 5% Critical value of 0.935 exceeds 0.616956 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.616956 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: 1,1-Dichloroethane Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQL2.5 13 9/24/2002 BQL2.5 13 10/21/2002 - BQL2.5 13 12/3/2002 BQL2.5 13 6/24/2003 BQL2.5 13 12/17/2003 BQL2.5 13 Rank Sum =78 Rank Mean =13 GWA-7/MW-7 7/30/2002 - BQL2.5 13 9/24/2002 BQL2.5 13 10/21/2002 BQL2.5 13 12/3/2002 BQL2.5 13 6/24/2003 BQL2.5 13 12/17/2003 BQL2.5 13 Rank Sum =78 Rank Mean =13 Background Rank Sum =156 Background Rank Mean =13 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQL2.5 13 9/24/2002 BQL2.5 13 10/21/2002 BQL2.5 13 1213/2002 BQL2.5 13 6/24/2003 BQL2.5 13 12/17/2003 BQL2.5 13 Rank Sum =78 Rank Mean =13 GWC-13/MW-137/30/2002 BQL2.5 13 9/24/2002 6 26 10/21/2002 6 27 12/3/2002 7 28 6/24/2003 - 9 29 12/17/2003 - 20.5 35 Rank Sum =158 Rank Mean =26.3333 GWC-14/MW-147/30/2002 13 32 9/24/2002 - 21 36 10/21/2002 17 34 1213/2002 16 33

6/24/2003 10 30 12/17/2003 10 31 Rank Sum =196 Rank Mean =32.6667 GWC-5/MW-5 7/3012002 BQL2.5 13 9/24/2002 BQL2.5 13 10/21/2002 BQL2.5 13 12/3/2002 BQL2.5 13 6/24/2003 BQL2.5 13 12/17/2003 BQL2.5 13 Rank Sum =78 Rank Mean =13 Calculation Results: Kruskal-Wallis H Statistic =20.7057 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =31.1186 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 20.7057> 9.48773 indicating a significant group difference at 5% significance level 31.1186 > 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o 13.3333 19.6667 o Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 13 Well Mean Rank GWB-6/MW-6 13 GWC-13/MW-1326.3333 GWC-14/MW-1432.6667 GWC-5/MW-5 13 Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o 13.3333 19.6667 o Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 13 Well Mean Rank GWB-6/MW-6 13 GWC-13/MW-1326.3333 GWC-14/MW-1432.6667 GWC-5/MW-5 13

Shapiro-Wilks Test of Normality Parameter: cis-1,2-Dichloroethene All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K=18; Samples =36 i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 6 10 10 14 16 17 18.5 19 x(n-i+1) 19 18.5 17 16 14 10 10 6 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 x(n-1 +1 )-x(i)a(n-i+1) 16.5 0.4068 16 0.2813 14.5 0.2415 13.5 0.2121 11.5 0.1883 7.5 0.1678 7.5 0.1496 3.5 0.1331 o 0.1179 o 0.1036 o 0.09 o 0.077 o 0.0645 o 0.0523 o 0.0404 o 0.0287 o 0.0172 o 0.0057 o o o o o o ooo o -3.5 -7.5 -7.5 -11.5 -13.5 -14.5 -16 -16.5 b(i) 6.7122 4.5008 3.50175 2.86335 2.16545 1.2585 1.122 0.46585 oo o o o o o o o o Sum of b values =22.5899 Sample Standard Deviation =5.21055 W Statistic =0.537024 5% Critical value of 0.935 exceeds 0.537024 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.537024 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: cis-1,2-Dichloroethene Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQL2.5 14.5 9/24/2002 BQL2.5 14.5 10/21/2002 - BQL2.5 14.5 12/3/2002 BQL2.5 14.5 6/24/2003 BQL2.5 14.5 12/17/2003 BQL2.5 14.5 Rank Sum =87 Rank Mean =14.5 GWA-7/MW-7 7/30/2002 - BQL2.5 14.5 9/24/2002 BQL2.5 14.5 10/21/2002 BQL2.5 14.5 12/3/2002 BQL2.5 14.5 6/24/2003 BQL2.5 14.5 12/17/2003 BQL2.5 14.5 Rank Sum =87 Rank Mean =14.5 Background Rank Sum =174 Background Rank Mean =14.5 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQL2.5 14.5 9/24/2002 BQL2.5 14.5 10/21/2002 BQL2.5 14.5 12/3/2002 BQL2.5 14.5 6/24/2003 BQL2.5 14.5 12/17/2003 BQL2.5 14.5 Rank Sum =87 Rank Mean =14.5 GWC-13/MW-137/30/2002 BQL2.5 14.5 9/24/2002 BQL2.5 14.5 10/21/2002 BQL2.5 14.5 12/3/2002 BQL2.5 14.5 6/24/2003 - 6 29 12/17/2003 - 14 32 Rank Sum =119 Rank Mean =19.8333 GWC-14/MW-147/30/2002 10 30 9/24/2002 - 18.5 35 10/21/2002 16 33 12/3/2002 19 36

6/24/2003 10 31 12117/2003 17 34 Rank Sum =199 Rank Mean =33.1667 GWC-5/MW-5 7/30/2002 BQL2.5 14.5 9/24/2002 BQL2.5 14.5 10/21/2002 BQL2.5 14.5 12/3/2002 BQL2.5 14.5 6/24/2003 BQL2.5 14.5 12117/2003 BQL2.5 14.5 Rank Sum =87 Rank Mean =14.5 Calculation Results: Kruskal-Wallis H Statistic =15.1832 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =28.6621 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 15.1832> 9.48773 indicating a significant group difference at 5% significance level 28.6621 > 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o 5.33333 18.6667 o Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 14.5 Well Mean Rank GWB-6/MW-6 14.5 GWC-13/MW-1319.8333 GWC-14/MW-1433.1667 GWC-5/MW-5 14.5 Critical Value 11.8902 11.8902 11.8902 11.8902 Diffrom Bkg o 5.33333 18.6667 o Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 14.5 Well Mean Rank GWB-6/MW-6 14.5 GWC-13/MW-1319.8333 GWC-14/MW-1433.1667 GWC-5/MW-5 14.5

Shapiro-Wilks Test of Normality Parameter: Trichlorofluoromethane All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =18; Samples =36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 5 23 27 31 32 34 43 44 47.5 99.5 184.5 210 221 300 348 381 391 x(n-i+1) 391 381 348 300 221 210 184.5 99.5 47.5 44 43 34 32 31 27 23 5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 388.5 378.5 345.5 297.5 218.5 207.5 182 97 45 41.5 40.5 31.5 29.5 28.5 24.5 20.5 2.5 o o -2.5 -20.5 -24.5 -28.5 -29.5 -31.5 -40.5 -41.5 -45 -97 -182 -207.5 -218.5 -297.5 -345.5 -378.5 -388.5 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 158.042 106.472 83.4382 63.0998 41.1435 34.8185 27.2272 12.9107 5.3055 4.2994 3.645 2.4255 1.90275 1.49055 0.9898 0.58835 0.043 o Sum of b values =547.842 Sample Standard Deviation = 117.993 W Statistic = 0.615931 5% Critical value of 0.935 exceeds 0.615931 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.615931 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Trichlorofluoromethane Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date GWA-15/MW-157/30/2002 9/24/2002 10/21/2002 - 12/3/2002 6/24/2003 12/17/2003 Rank Sum =60 Rank Mean =10 GWA-7/MW-7 7/30/2002-9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum = 163 Rank Mean = 27.1667 Result BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 184.5 32 221 210 23 34 Rank 10 10 10 10 10 10 30 24 32 31 21 25 Background Rank Sum = 223 Background Rank Mean =18.5833 Compliance Wells WelllD Date GWB-6/MW-6 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum = 60 Rank Mean = 10 GWC-13/MW-137/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 - 12/17/2003 - Rank Sum = 194 Rank Mean =32.3333 GWC-14/MW-147/30/2002 9/24/2002 - 10/21/2002 12/3/2002 Result BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 300 381 348 391 44 99.5 43 47.5 31 27 Rank 10 10 10 10 10 10 33 35 34 36 27 29 26 28 23 22

6/24/2003 12/17/2003 Rank Sum =129 Rank Mean =21.5 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum =60 Rank Mean =10 5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 BQL2.5 20 10 10 10 10 10 10 10 Critical Value 11.8902 11.8902 11.8902 11.8902 Critical Value 11.8902 11.8902 11.8902 11.8902 Calculation Results: Kruskal-Wallis H Statistic =18.6419 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =21.8473 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 18.6419> 9.48773 indicating a significant group difference at 5% significance level 21.8473> 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 18.5833 Well Mean Rank Dif from Bkg GWB-6/MW-6 10 -8.58333 GWC-13/MW-1332.3333 13.75 GWC-14/MW-1421.5 2.91667 GWC-5/MW-5 10 -8.58333 Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 18.5833 Well Mean Rank Dif from Bkg GWB-6/MW-6 10 -8.58333 GWC-13/MW-1332.3333 13.75 GWC-14/MW-1421.5 2.91667 GWC-5/MW-5 10 -8.58333

Shapiro-Wilks Test of Normality Parameter: Xylenes (total) All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K = 17; Samples = 35 i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 x(i) 2.5 2.5 2.5 2.5 2.5 2.5 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 10 10 21 x(n-i+1) 21 10 10 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 3.75 2.5 2.5 2.5 2.5 2.5 2.5 x(n-1 +1 )-x(i)a(n-i+1) 18.5 0.4096 7.5 0.2834 7.5 0.2427 2.5 0.2127 2.5 0.1883 2.5 0.1673 1.25 0.1487 1.25 0.1317 1.25 0.116 1.25 0.1013 1.25 0.0873 1.25 0.0739 1.25 0.061 1.25 0.0484 1.25 0.0361 1.25 0.0239 1.25 0.0119 o -1.25 -1.25 -1.25 -1.25 -1.25 -1.25 -1.25 -1.25 -1.25 -1.25 -1.25 -2.5 -2.5 -2.5 -7.5 -7.5 -18.5 b(i) 7.5776 2.1255 1.82025 0.53175 0.47075 0.41825 0.185875 0.164625 0.145 0.126625 0.109125 0.092375 0.07625 0.0605 0.045125 0.029875 0.014875 Sum of b values = 13.9944 Sample Standard Deviation = 3.25609 W Statistic = 0.543294 5% Critical value of 0.934 exceeds 0.543294 Evidence of non-normality at 95% level of significance 1% Critical value of 0.91 exceeds 0.543294 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Xylenes (total) Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BOL5 16.5 9/24/2002 BOL5 16.5 10/21/2002 a BOL5 16.5 12/3/2002 BOL2.5 16.5 6/24/2003 - BOL3.75 16.5 12/17/2003 - BOL3.75 16.5 Rank Sum =99 Rank Mean =16.5 GWA-7/MW-7 7/30/2002 - BOL5 16.5 9/24/2002 BOL5 16.5 10/21/2002 BOL5 16.5 12/3/2002 BOL2.5 16.5 6/24/2003 - BOL3.75 16.5 12/17/2003 - BOL3.75 16.5 Rank Sum =99 Rank Mean =16.5 Background Rank Sum =198 Background Rank Mean =16.5 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BOL5 16.5 9/24/2002 BOL5 16.5 10/21/2002 BOL5 16.5 12/3/2002 BOL2.5 16.5 6/24/2003 - BOL3.75 16.5 12/17/2003 - BOL3.75 16.5 Rank Sum =99 Rank Mean =16.5 GWC-13/MW-137/30/2002 BOL5 16.5 9/24/2002 BOL2.5 16.5 10/21/2002 BOL5 16.5 6/24/2003 - BOL3.75 16.5 12/17/2003 - BOL3.75 16.5 Rank Sum =82.5 Rank Mean =16.5 GWC-14/MW-147/30/2002 BOL5 16.5 9/24/2002 - 10 33 10/21/2002 BOL5 16.5 12/3/2002 21 35 6/24/2003 - BOL3.75 16.5

12/17/2003 - Rank Sum =151.5 Rank Mean =25.25 10 34 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 - 12/17/2003 - Rank Sum = 99 Rank Mean = 16.5 BQL5 BQL2.5 BQL5 BQL2.5 BQL3.75 BQL3.75 16.5 16.5 16.5 16.5 16.5 16.5 Calculation Results: Kruskal-Wallis H Statistic =3.625 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =15.3697 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 3.625 < 9.48773 indicating no significant group difference at 5% significance level 15.3697> 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Critical Value 11.5643 12.3112 11.5643 11.5643 Diffrom Bkg o o 8.75 o Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 16.5 Well Mean Rank GWB-6/MW-6 16.5 GWC-13/MW-1316.5 GWC-14/MW-1425.25 GWC-5/MW-5 16.5 Critical Value 11.5643 12.3112 11.5643 11.5643 Diffrom Bkg o o 8.75 o Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 16.5 Well Mean Rank GWB-6/MW-6 16.5 GWC-13/MW-1316.5 GWC-14/MW-1425.25 GWC-5/MW-5 16.5

Shapiro-Wilks Test of Normality Parameter: Barium All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K = 18; Samples = 36 x(n-1 +1)-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 0.005 0.005 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.015 0.018 0.02 0.0295 0.0325 0.036 0.051 0.064 0.068 0.077 0.082 0.083 0.085 0.0935 0.106 0.142 0.189 x(n-i+1) 0.189 0.142 0.106 0.0935 0.085 0.083 0.082 0.077 0.068 0.064 0.051 0.036 0.0325 0.0295 0.02 0.018 0.015 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.005 0.005 0.184 0.137 0.096 0.0835 0.075 0.073 0.072 0.067 0.058 0.054 0.041 0.026 0.0225 0.0195 0.01 0.008 0.005 o o -0.005 -0.008 -0.01 -0.0195 -0.0225 -0.026 -0.041 -0.054 -0.058 -0.067 -0.072 -0.073 -0.075 -0.0835 -0.096 -0.137 -0.184 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.0748512 0.0385381 0.023184 0.0177104 0.0141225 0.0122494 0.0107712 0.0089177 0.0068382 0.0055944 0.00369 0.002002 0.00145125 0.00101985 0.000404 0.0002296 8.6e-005 o Sum of b values = 0.22166 Sample Standard Deviation =0.0439553 W Statistic =0.726579 5% Critical value of 0.935 exceeds 0.726579 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.726579 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Barium Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date GWA-15/MW-157/30/2002 9/24/2002 10/21/2002 - 12/3/2002 6/24/2003 12/17/2003 Rank Sum =60 Rank Mean =10 GWA-7/MW-7 7/30/2002-9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum = 85 Rank Mean =14.1667 Result BQLO.01 BQLO.01 BQLO.01 BQLO.005 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 0.015 0.036 BQLO.01 Rank 10 10 10 10 10 10 10 10 10 20 25 10 Background Rank Sum =145 Background Rank Mean =12.0833 Compliance Wells WelllD Date GWB-6/MW-6 7/30/2002 9/24/2002 10/21/2002 1213/2002 6/24/2003 12117/2003 Rank Sum =60 Rank Mean =10 GWC-13/MW-137/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 - 12/17/2003 - Rank Sum =169 Rank Mean = 28.1667 GWC-14/MW-147/30/2002 9/24/2002 - 10/21/2002 12/3/2002 Result BQLO.01 BQLO.01 BQLO.01 BQLO.005 BQLO.01 BQLO.01 0.077 0.085 0.083 0.082 0.0295 0.0325 0.068 0.0935 0.064 0.106 Rank 10 10 10 10 10 10 29 32 31 30 23 24 28 33 27 34

Critical Value 11.8902 11.8902 11.8902 11.8902 Critical Value 11.8902 11.8902 11.8902 11.8902 6/24/2003 0.051 26 12/17/2003 0.189 36 Rank Sum =184 Rank Mean =30.6667 GWC-5/MW-5 7/3012002 BQLO.01 10 9/24/2002 0.02 22 10/21/2002 BQLO.01 10 1213/2002 0.018 21 6/24/2003 BQLO.01 10 12/17/2003 0.142 35 Rank Sum =108 Rank Mean =18 Calculation Results: Kruskal-Wallis H Statistic =21.4227 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =25.1062 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 21.4227 > 9.48773 indicating a significant group difference at 5% significance level 25.1062 > 9.48773 indicating a significant group difference at 5% significance level when adjusted for ties Individual Well Comparisons at 1.25% Significance Level per Comparison 1.25% Z score is 2.25713 Mean background rank is 12.0833 Well Mean Rank Dif from Bkg GWB-6/MW-6 10 -2.08333 GWC-13/MW-1328.1667 16.0833 GWC-14/MW-1430.6667 18.5833 GWC-5/MW-5 18 5.91667 Individual Well Comparisons at Groupwise 5% Significance Level (1.25% Significance Level per comparison) 1.25% Z score is 2.25713 Mean background rank is 12.0833 Well Mean Rank Dif from Bkg GWB-6/MW-6 10 -2.08333 GWC-13/MW-1328.1667 16.0833 GWC-14/MW-1430.6667 18.5833 GWC-5/MW-5 18 5.91667

Shapiro-Wilks Test of Normality Parameter: Beryllium All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K = 18; Samples = 36 x(n-1 +1 )-x(i}a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 xCi) 0.0015 0.0015 0.0015 0.0015 0.0015 0.0015 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.004 x(n-i+1) 0.004 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.002 0.0015 0.0015 0.0015 0.0015 0.0015 0.0015 0.0025 0.0005 0.0005 0.0005 0.0005 0.0005 ooo o o o o o o o oo o o o o oo o o o o o o -0.0005 -0.0005 -0.0005 -0.0005 -0.0005 -0.0025 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.001017 0.00014065 0.00012075 0.00010605 9.415e-005 8.3ge-005 ooo o o o o ooo o o Sum of b values = 0.0015625 Sample Standard Deviation = 0.00039541 W Statistic = 0.446145 5% Critical value of 0.935 exceeds 0.446145 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.446145 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Beryllium Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQLO.002 18 9/24/2002 BQLO.002 18 10/21/2002 - BQLO.002 18 12/3/2002 BQLO.0015 18 6/24/2003 BQLO.002 18 12/17/2003 BQLO.002 18 Rank Sum =108 Rank Mean =18 GWA-7/MW-7 7/30/2002 - BQLO.002 18 9/24/2002 BQLO.002 18 10/21/2002 BQLO.002 18 12/3/2002 BQLO.0015 18 6/24/2003 BQLO.002 18 12/17/2003 BQLO.002 18 Rank Sum =108 Rank Mean =18 Background Rank Sum =216 Background Rank Mean =18 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQLO.002 18 9/24/2002 BQLO.002 18 10/21/2002 BQLO.002 18 12/3/2002 BQLO.0015 18 6/24/2003 BQLO.002 18 12/17/2003 BQLO.002 18 Rank Sum =108 Rank Mean =18 GWC-13/MW-137/30/2002 BQLO.002 18 9/24/2002 BQLO.002 18 10/21/2002 BQLO.002 18 12/3/2002 BQLO.0015 18 6/24/2003 - BQLO.002 18 12/17/2003 - BQLO.002 18 Rank Sum =108 Rank Mean =18 GWC-14/MW-147/30/2002 BQLO.002 18 9/24/2002 - BQLO.002 18 10/21/2002 BQLO.002 18 12/3/2002 BQLO.0015 18

6/24/2003 12/17/2003 Rank Sum = 126 Rank Mean =21 GWC-5/MW-5 7/3012002 9/24/2002 10/21/2002 12/312002 6124/2003 12/17/2003 Rank Sum = 108 Rank Mean =18 BQLO.002 0.004 BQLO.002 BQLO.002 BQLO.002 BQLO.0015 BQLO.002 BQLO.002 18 36 18 18 18 18 18 18 Calculation Results: Kruskal-Wallis H Statistic =0.405405 Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 5 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.405405 < 9.48773 indicating no significant group difference at 5% significance level 5 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Cadmium All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K=18; Samples =36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.011 x(n-i+1) 0.011 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 0.0085 o o o oo o o o o o o o o o o o o o o o o o o o o o o o o o o o o o -0.0085 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.0034578 o o ooo oo o o o o o ooo o o Sum of b values =0.0034578 Sample Standard Deviation = 0.00141667 W Statistic =0.170214 5% Critical value of 0.935 exceeds 0.170214 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.170214 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Cadmium Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQLO.0025 18 9/24/2002 BQLO.0025 18 10/21/2002 - BQLO.0025 18 12/3/2002 BQLO.0025 18 6/24/2003 BQLO.0025 18 12/17/2003 BQLO.0025 18 Rank Sum =108 Rank Mean =18 GWA-7/MW-7 7/30/2002 - BQLO.0025 18 9/24/2002 BQLO.0025 18 10/21/2002 BQLO.0025 18 12/3/2002 BQLO.0025 18 6/24/2003 BQLO.0025 18 12/17/2003 BQLO.0025 18 Rank Sum =108 Rank Mean =18 Background Rank Sum =216 Background Rank Mean =18 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQLO.0025 18 9/24/2002 BQLO.0025 18 10/21/2002 BQLO.0025 18 12/3/2002 BQLO.0025 18 6/24/2003 BQLO.0025 18 12/17/2003 BQLO.0025 18 Rank Sum =108 Rank Mean =18 GWC-13/MW-137/30/2002 BQLO.0025 18 9/24/2002 BQLO.0025 18 10/21/2002 BQLO.0025 18 12/3/2002 BQLO.0025 18 6/24/2003 - BQLO.0025 18 12/17/2003 - BQLO.0025 18 Rank Sum =108 Rank Mean =18 GWC-14/MW-147/30/2002 BQLO.0025 18 9/24/2002 - BQLO.0025 18 10/21/2002 BQLO.0025 18 12/3/2002 BQLO.0025 18

6/24/2003 12/17/2003 Rank Sum =126 Rank Mean =21 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum =108 Rank Mean =18 BQLO.0025 0.011 BQLO.0025 BQLO.0025 BQLO.0025 BQLO.0025 BQLO.0025 BQLO.0025 18 36 18 18 18 18 18 18 Calculation Results: Kruskal-Wallis H Statistic =0.405405 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =5 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.405405 < 9.48773 indicating no significant group difference at 5% significance level 5 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Chromium All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =18; Samples =36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 xCi) 0.005 0.005 0.005 0.005 0.005 0.005 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.028 0.091 x(n-i+1) 0.091 0.028 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.005 0.005 0.005 0.005 0.005 0.005 0.086 0.023 0.005 0.005 0.005 0.005 o o o o o o o o o o o o o o o oo o o o o o o o -0.005 -0.005 -0.005 -0.005 -0.023 -0.086 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.0349848 0.0064699 0.0012075 0.0010605 0.0009415 0.000839 o o o o o o oo o o o o Sum of b values = 0.0455032 Sample Standard Deviation = 0.0140436 W Statistic =0.299959 5% Critical value of 0.935 exceeds 0.299959 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.299959 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Chromium Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQLO.01 17.5 9/24/2002 BQLO.01 17.5 10/21/2002 - BQLO.01 17.5 12/3/2002 BQLO.005 17.5 6/24/2003 BQLO.01 17.5 12/17/2003 BQLO.01 17.5 Rank Sum =105 Rank Mean =17.5 GWA-7/MW-7 7/30/2002 - BQLO.01 17.5 9/2412002 BQLO.01 17.5 10/21/2002 BQLO.01 17.5 1213/2002 BQLO.005 17.5 6/24/2003 BQLO.01 17.5 12/17/2003 BQLO.01 17.5 Rank Sum =105 Rank Mean =17.5 Background Rank Sum =210 Background Rank Mean =17.5 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQLO.01 17.5 9/24/2002 BQLO.01 17.5 10/21/2002 BQLO.01 17.5 12/3/2002 BQLO.005 17.5 6/24/2003 BQLO.01 17.5 12/17/2003 BQLO.01 17.5 Rank Sum =105 Rank Mean =17.5 GWC-13/MW-137/30/2002 BQLO.01 17.5 9/24/2002 BQLO.01 17.5 10/21/2002 BQLO.01 17.5 12/3/2002 BQLO.005 17.5 6/24/2003 - BQLO.01 17.5 12/17/2003 - BQLO.01 17.5 Rank Sum =105 Rank Mean =17.5 GWC-14/MW-147/30/2002 BQLO.01 17.5 9/24/2002 - BQLO.01 17.5 10/21/2002 BQLO.01 17.5 12/3/2002 BQLO.005 17.5

6/24/2003 12/17/2003 Rank Sum = 123.5 Rank Mean = 20.5833 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12117/2003 Rank Sum =122.5 Rank Mean = 20.4167 BQlO.01 0.091 BQlO.01 BQlO.01 BQlO.01 BQlO.005 BQlO.01 0.028 17.5 36 17.5 17.5 17.5 17.5 17.5 35 Calculation Results: Kruskal-Wallis H Statistic =0.649399 Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 4.11905 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.649399 < 9.48773 indicating no significant group difference at 5% significance level 4.11905 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Copper All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K = 18; Samples = 36 i x(i) x(n-i+1) x(n-1 +1 )-x(i)a(n-i+1) b(i) 1 0.01 0.035 0.025 0.4068 0.01017 2 0.01 0.026 0.016 0.2813 0.0045008 3 0.01 0.025 0.015 0.2415 0.0036225 4 0.01 0.0125 0.0025 0.2121 0.00053025 5 0.01 0.0125 0.0025 0.1883 0.00047075 6 0.01 0.0125 0.0025 0.1678 0.0004195 7 0.01 0.0125 0.0025 0.1496 0.000374 8 0.01 0.0125 0.0025 0.1331 0.00033275 9 0.01 0.0125 0.0025 0.1179 0.00029475 10 0.01 0.01 0 0.1036 0 11 0.01 0.01 0 0.09 0 12 0.01 0.01 0 0.077 0 13 0.01 0.01 0 0.0645 0 14 0.01 0.01 0 0.0523 0 15 0.01 0.01 0 0.0404 0 16 0.01 0.01 0 0.0287 0 17 0.01 0.01 0 0.0172 0 18 0.01 0.01 0 0.0057 0 19 0.01 0.01 0 20 0.01 0.01 0 21 0.01 0.01 0 22 0.01 0.01 0 23 0.01 0.01 0 24 0.01 0.01 0 25 0.01 0.01 0 26 0.01 0.01 0 27 0.01 0.01 0 28 0.0125 0.01 -0.0025 29 0.0125 0.01 -0.0025 30 0.0125 0.01 -0.0025 31 0.0125 0.01 -0.0025 32 0.0125 0.01 -0.0025 33 0.0125 0.01 -0.0025 34 0.025 0.01 -0.015 35 0.026 0.01 -0.016 36 0.035 0.01 -0.025 Sum of b values =0.0207153 Sample Standard Deviation =0.0053545 W Statistic = 0.427639 5% Critical value of 0.935 exceeds 0.427639 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.427639 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Copper Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date GWA-15/MW-157/30/2002 9/24/2002 10/21/2002 - 12/3/2002 6/24/2003 12/17/2003 Rank Sum =102 Rank Mean =17 GWA-7/MW-7 7/30/2002-9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum =121 Rank Mean =20.1667 Result BQLO.01 BQLO.01 BQLO.01 BQLO.0125 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.0125 0.035 BQLO.01 Rank 17 17 17 17 17 17 17 17 17 17 36 17 Background Rank Sum =223 Background Rank Mean = 18.5833 Compliance Wells WelllD Date GWB-6/MW-6 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum = 102 Rank Mean =17 GWC-13/MW-137/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 - 12/17/2003 - Rank Sum = 102 Rank Mean =17 GWC-14/MW-147/30/2002 9/24/2002 - 10/21/2002 12/3/2002 Result BQLO.01 BQLO.01 BQLO.01 BQLO.0125 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.0125 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.0125 Rank 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17 17

6/24/2003 12117/2003 Rank Sum = 120 Rank Mean =20 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum =119 Rank Mean = 19.8333 BQLO.01 0.026 BQLO.01 BQLO.01 BQLO.01 BQLO.0125 BQLO.01 0.025 17 35 17 17 17 17 17 34 Calculation Results: Kruskal-Wallis H Statistic =0.461712 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =2.00868 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.461712 < 9.48773 indicating no significant group difference at 5% significance level 2.00868 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Lead All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =18; Samples =36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.0075 0.0075 0.0075 0.0075 0.0075 0.0075 0.015 x(n-i+1 ) 0.015 0.0075 0.0075 0.0075 0.0075 0.0075 0.0075 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.01 0.0025 0.0025 0.0025 0.0025 0.0025 0.0025 o o o o o o o o o o o o oo o o o o o o o o -0.0025 -0.0025 -0.0025 -0.0025 -0.0025 -0.0025 -0.01 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.004068 0.00070325 0.00060375 0.00053025 0.00047075 0.0004195 0.000374 o o o o o o o o o o o Sum of b values =0.0071695 Sample Standard Deviation =0.00185271 W Statistic =0.427853 5% Critical value of 0.935 exceeds 0.427853 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.427853 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Lead Original Data (Not Transformed) Non-Detects Replaced with 1/2 Dl Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-1S/MW-1S7/30/2002 BQlO.OOS 18 9/24/2002 BQlO.OOS 18 10/21/2002 - BQlO.OOS 18 12/3/2002 BQlO.007S 18 6/24/2003 BQlO.OOS 18 12/17/2003 BQlO.OOS 18 Rank Sum = 108 Rank Mean = 18 GWA-7/MW-7 7/30/2002 - BQlO.OOS 18 9/24/2002 BQlO.OOS 18 10/21/2002 BQlO.OOS 18 12/3/2002 BQlO.007S 18 6/24/2003 BQlO.OOS 18 12/17/2003 BQlO.OOS 18 Rank Sum = 108 Rank Mean = 18 Background Rank Sum = 216 Background Rank Mean = 18 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQlO.OOS 18 9/2412002 BQlO.OOS 18 10/21/2002 BQlO.OOS 18 1213/2002 BQlO.007S 18 6/24/2003 BQlO.OOS 18 12/17/2003 BQlO.OOS 18 Rank Sum = 108 Rank Mean = 18 GWC-13/MW-137/30/2002 BQlO.OOS 18 9/24/2002 BQlO.OOS 18 10/21/2002 BQlO.OOS 18 12/3/2002 BQlO.007S 18 6/24/2003 - BQlO.OOS 18 12117/2003 - BQlO.OOS 18 Rank Sum = 108 Rank Mean = 18 GWC-14/MW-147/30/2002 BQlO.OOS 18 9/24/2002 - BQlO.OOS 18 10/21/2002 BQlO.OOS 18 12/3/2002 BQlO.007S 18

6/24/2003 12/17/2003 Rank Sum = 126 Rank Mean = 21 GWC-5/MW-5 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum = 108 Rank Mean = 18 BOlO.005 0.015 BOlO.005 BOlO.005 BOlO.005 BOlO.00l5 BOlO.005 BOlO.005 18 36 18 18 18 18 18 18 Calculation Results: Kruskal-Wallis H Statistic =0.405405 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =5 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.405405 < 9.48773 indicating no significant group difference at 5% significance level 5 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Nickel All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =18; Samples =36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 xCi) 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.02 0.02 0.02 0.02 0.02 0.02 0.034 x(n-i+1) 0.034 0.02 0.02 0.02 0.02 0.02 0.02 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.024 0.01 0.01 0.01 0.01 0.01 0.01 ooo o o o o o o oo o o o o o o o o ooo -0.01 -0.01 -0.01 -0.01 -0.01 -0.01 -0.024 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.0097632 0.002813 0.002415 0.002121 0.001883 0.001678 0.001496 o o o o o o o o o o o Sum of b values = 0.0221692 Sample Standard Deviation =0.0052915 W Statistic = 0.501503 5% Critical value of 0.935 exceeds 0.501503 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.501503 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Nickel Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQLO.01 18 9/24/2002 BQLO.01 18 10/21/2002 - BQLO.01 18 12/3/2002 BQLO.02 18 6/24/2003 BQLO.01 18 12/17/2003 BQLO.01 18 Rank Sum =108 Rank Mean =18 GWA-7/MW-7 7/30/2002 - BQLO.01 18 9/24/2002 BQLO.01 18 10/21/2002 BQLO.01 18 12/3/2002 BQLO.02 18 6/24/2003 BQLO.01 18 12/17/2003 BQLO.01 18 Rank Sum =108 Rank Mean =18 Background Rank Sum =216 Background Rank Mean =18 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQLO.01 18 9/24/2002 BQLO.01 18 10/21/2002 BQLO.01 18 1213/2002 BQLO.02 18 6/24/2003 BQLO.01 18 12/17/2003 BQLO.01 18 Rank Sum =108 Rank Mean =18 GWC-13/MW-137/30/2002 BQLO.01 18 9/24/2002 BQLO.01 18 10/21/2002 BQLO.01 18 1213/2002 BQLO.02 18 6/24/2003 - BQLO.01 18 12/17/2003 - BQLO.01 18 Rank Sum =108 Rank Mean =18 GWC-14/MW-147/30/2002 BQLO.01 18 9/24/2002 - BQLO.01 18 10/21/2002 BQLO.01 18 12/3/2002 BQLO.02 18

6/24/2003 BQLO.01 18 12/17/2003 0.034 36 Rank Sum = 126 Rank Mean = 21 GWC-5/MW-5 7/30/2002 BQLO.01 18 9/24/2002 BQLO.01 18 10/21/2002 BQLO.01 18 12/3/2002 BQLO.02 18 6/24/2003 BQLO.01 18 12/17/2003 BQLO.01 18 Rank Sum = 108 Rank Mean = 18 Calculation Results: Kruskal-Wallis H Statistic =0.405405 Kruskal-Wallis H Statistic (adjusted for tied non-detects) = 5 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.405405 < 9.48773 indicating no significant group difference at 5% significance level 5 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Vanadium All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =18; Samples =36 i x(i) x(n-i+1) x(n-1 +1 )-x(i)a(n-i+1) b(i) 1 0.005 0.06 0.055 0.4068 0.022374 2 0.005 0.025 0.02 0.2813 0.005626 3 0.005 0.025 0.02 0.2415 0.00483 4 0.005 0.025 0.02 0.2121 0.004242 5 0.005 0.025 0.02 0.1883 0.003766 6 0.005 0.025 0.02 0.1678 0.003356 7 0.025 0.025 0 0.1496 0 8 0.025 0.025 0 0.1331 0 9 0.025 0.025 0 0.1179 0 10 0.025 0.025 0 0.1036 0 11 0.025 0.025 0 0.09 0 12 0.025 0.025 0 0.077 0 13 0.025 0.025 0 0.0645 0 14 0.025 0.025 0 0.0523 0 15 0.025 0.025 0 0.0404 0 16 0.025 0.025 0 0.0287 0 17 0.025 0.025 0 0.0172 0 18 0.025 0.025 0 0.0057 0 19 0.025 0.025 0 20 0.025 0.025 0 21 0.025 0.025 0 22 0.025 0.025 0 23 0.025 0.025 0 24 0.025 0.025 0 25 0.025 0.025 0 26 0.025 0.025 0 27 0.025 0.025 0 28 0.025 0.025 0 29 0.025 0.025 0 30 0.025 0.025 0 31 0.025 0.005 -0.02 32 0.025 0.005 -0.02 33 0.025 0.005 -0.02 34 0.025 0.005 -0.02 35 0.025 0.005 -0.02 36 0.06 0.005 -0.055 ,'.~.'.' W** ___

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,,,-*,*_~*___~,,,_,_,*",_**_'~"'______ YN~.'~'~'_A___ '-'-***'*'--_"*'.~=~'_~V~__' ___' ________*~__V__.*__.'~.___*"_*___.*~*'*'~~"O_~"~"""" __*_"_"_"~~_~m~_'_", .-.__'_.__ "~'A_'~.~_"y.,~~,w~, Sum of b values = 0.044194 Sample Standard Deviation =0.00989127 W Statistic =0.570367 5% Critical value of 0.935 exceeds 0.570367 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.570367 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Vanadium Original Data (Not Transformed) Non-Detects Replaced with 1/2 Dl Kruskal Wallis Ranks Background Wells WelllD Date Result Rank GWA-15/MW-157/30/2002 BQlO.025 18 9/24/2002 BQlO.025 18 10/21/2002 - BQlO.025 18 12/3/2002 BQlO.005 18 6/24/2003 BQlO.025 18 12/17/2003 BQlO.025 18 Rank Sum =108 Rank Mean =18 GWA-7/MW-7 7/30/2002 - BQlO.025 18 9/24/2002 BQlO.025 18 10/21/2002 BQlO.025 18 12/3/2002 BQlO.005 18 6/24/2003 BQlO.025 18 12/17/2003 BQlO.025 18 Rank Sum =108 Rank Mean =18 Background Rank Sum =216 Background Rank Mean =18 Compliance Wells WelllD Date Result Rank GWB-6/MW-6 7/30/2002 BQlO.025 18 9/24/2002 BQlO.025 18 10/21/2002 BQlO.025 18 12/3/2002 BQlO.005 18 6/24/2003 BQlO.025 18 12/17/2003 BQlO.025 18 Rank Sum =108 Rank Mean =18 GWC-13/MW-137/30/2002 BQlO.025 18 9/24/2002 BQlO.025 18 10/21/2002 BQlO.025 18 12/3/2002 BQlO.005 18 6/24/2003 - BQlO.025 18 12/17/2003 - BQlO.025 18 Rank Sum =108 Rank Mean =18 GWC-14/MW-147/30/2002 BQlO.025 18 9/24/2002 - BQlO.025 18 10/21/2002 BQlO.025 18 12/3/2002 BQlO.005 18

6/24/2003 BQlO.025 18 12/17/2003 0.06 36 Rank Sum = 126 Rank Mean = 21 GWC-5/MW-5 7/30/2002 BQlO.025 18 9/24/2002 BQlO.025 18 10/21/2002 BQlO.025 18 12/3/2002 BQlO.005 18 6/24/2003 BQlO.025 18 12/17/2003 BQlO.025 18 Rank Sum = 108 Rank Mean = 18 Calculation Results: Kruskal-Wallis H Statistic =0.405405 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =5 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 0.405405 < 9.48773 indicating no significant group difference at 5% significance level 5 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties

Shapiro-Wilks Test of Normality Parameter: Zinc All Wells Normality Test of Parameter Concentrations Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL K =18; Samples =36 x(n-1 +1 )-x(i)a(n-i+1) i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 x(i) 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.023 0.023 0.027 0.027 0.032 0.034 0.127 x(n-i+1) 0.127 0.034 0.032 0.027 0.027 0.023 0.023 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.117 0.024 0.022 0.017 0.017 0.013 0.013 o o o o o oo o o o oo o oo o o o o o o o -0.013 -0.013 -0.017 -0.017 -0.022 -0.024 -0.117 0.4068 0.2813 0.2415 0.2121 0.1883 0.1678 0.1496 0.1331 0.1179 0.1036 0.09 0.077 0.0645 0.0523 0.0404 0.0287 0.0172 0.0057 b(i) 0.0475956 0.0067512 0.005313 0.0036057 0.0032011 0.0021814 0.0019448 o o o o o o o o o o o Sum of b values =0.0705928 Sample Standard Deviation =0.0202016 W Statistic =0.348885 5% Critical value of 0.935 exceeds 0.348885 Evidence of non-normality at 95% level of significance 1% Critical value of 0.912 exceeds 0.348885 Evidence of non-normality at 99% level of significance

Kruskal-Wallis Non-Parametric Test Parameter: Zinc Original Data (Not Transformed) Non-Detects Replaced with 1/2 DL Kruskal Wallis Ranks Background Wells WelllD Date GWA-15/MW-157/30/2002 9/24/2002 10/21/2002 - 12/3/2002 6/24/2003 12/17/2003 Rank Sum =90 Rank Mean =15 GWA-7/MW-7 7/30/2002-9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum =125 Rank Mean =20.8333 Result BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 0.034 0.023 Rank 15 15 15 15 15 15 15 15 15 15 35 30 Background Rank Sum =215 Background Rank Mean = 17.9167 Compliance Wells WelllD Date GWB-6/MW-6 7/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 12/17/2003 Rank Sum = 90 Rank Mean =15 GWC-13/MW-137/30/2002 9/24/2002 10/21/2002 12/3/2002 6/24/2003 - 12/17/2003 - Rank Sum =141 Rank Mean =23.5 GWC-14/MW-147/30/2002 9/24/2002 - 10/21/2002 12/3/2002 Result BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 0.023 0.027 0.027 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 BQLO.01 Rank 15 15 15 15 15 15 15 31 32 33 15 15 15 15 15 15

6/24/2003 BQLO.01 15 12/17/2003 0.127 36 Rank Sum =111 Rank Mean =18.5 GWC-5/MW-5 7/30/2002 BQLO.01 15 9/24/2002 BQLO.01 15 10/21/2002 BQLO.01 15 12/3/2002 BQLO.01 15 6/24/2003 BQLO.01 15 12/17/2003 0.032 34 Rank Sum =109 Rank Mean =18.1667 Calculation Results: Kruskal-Wallis H Statistic =2.05631 Kruskal-Wallis H Statistic (adjusted for tied non-detects) =4.3066 95% Confidence comparison value is 9.48773 at 4 degrees of freedom 2.05631 < 9.48773 indicating no significant group difference at 5% significance level 4.3066 < 9.48773 indicating no significant group difference at 5% significance level when adjusted for ties}}