ML061380594

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Alan J. Blotcky Reactor Facility, Omaha Veterans Administration Medical Center, Characterization Qa/Qc Data, Appendix E
ML061380594
Person / Time
Site: 05000131
Issue date: 05/02/2006
From:
US Dept of Veterans Affairs, Medical Ctr, Omaha, NE
To:
NRC/FSME
References
Download: ML061380594 (140)
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{{#Wiki_filter:Alan J. Blotcky Reactor Facility Omaha Veterans Administration Medical Center Omaha, Nebraska Characterization QA/QC Data APPENDIX E

G A M M A S P E C T R U M A N A L Y S I S Report Generated On Detector Sample I.D. C:\\GEI Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance 11/17/02 5:58:08 PM DET01 NIE2K\\CAMFILES\\ENCAL01.CNF 1L STD 1 Liter marinelli with 1.15 g/cc 1 3.50 100 - 8192 100 - 8192 1.00 keV Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time Background Type 1.OOOE+000 Unit 11/13/02 6:58:59 PM P. Jones 3600.0 seconds 3649.2 seconds 1.35 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 1 Performed & Reviewed By Supervisory Review ~. f-AZ - Date IJ / 71/ OQA Date .al 17 L/_ -

Peak Locate Analysis Report 11/17/02 5:58:08 PM Page 2 P E A K L O C A T E R E P O R T

I Detector Sample I.D.

Spectrum Number Sample Description Sample Type DET01 C:\\GENIE2K\\CAMFILES\\ENCALO1.CNE 1L STD 1 Liter marinelli with 1.15 g/cc ma Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence 11/17/02 100 8192 3.50 5.00 5:58:07 PM Peak Centroid No. Channel Centroid Uncertainty Energy Peak (keV) Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 168.08 237.05 351.06 487.21 544.98 662.54 1019.41 1115.98 1566.22 2646.37 3255.39 3592.21 4693.53 5301.17 5331.04 7346.82

0. 1473
0. 0624
0. 0471
0. 0523 0.0949
0. 0557
0. 1865
0. 1188
0. 0556 0.0373 0.2135
0. 0469
0. 0341
0. 1591 0.0341 0.0471 42.24 59.55 88.05 122.08 136.51 165.89 255.07 279.18 391.70 661.60 813.79 897.96 1173.15 1325.22 1332.44 1836.15 16.82 80.33 135.12 105.71 31.99 84.33 7.78 17.67 71.45 132.96 4.03 76.29 127.33 6.27 121.74 54.14
0. 6779
1. 1273
1. 1351
1. 1318
1. 1796 1.1936
1. 1377 1.2757
1. 4194 1.6737
1. 5370
1. 8 903
2. 1958
2. 3383
2. 3431
2. 8199 Errors quoted at
1. 96 sigma

Peak Analysis Report 11/17/02 5:58:08 PM Page 3 P E A K A N.A L Y S I S R E P O R T i Detector Sample I.D. Spectrum Number Sample Description DET01 C:\\GENIE2K\\CAMFILES\\ENCALO1.CNF 1L STD 1 Liter marinelli with 1.15 g/cc matrix Peak Analysis Peak Analysis Peak Analysis Peak ROI ROI No. start end Performed on From Channel To Channel Peak En( centroid (1 11/17/02 5:58:07 PM 100 8192 ergy Net Peak Net Area Continuum ceV) Area Uncert. Counts F F F F F F F F F F F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 164-221-334-474-535-652-1012-1107-1550-2625-3246-3576-4664-5288-5288-7322-173 246 366 501 562 682 1030 1124 1588 2675 3269 3614 4721 5357 5357 7372 167.77 237.02 351.08 487.28 545.02 662.60 1019.49 1115.97 1566.26 2646.38 3255.44 3592.27 4693.54 5302.11 5331.03 7346.82 42.24 59.55 88.05 122.08 136.51 165.89 255.07 279.18 391.70 661.60 813.79 897.96 1173.15 1325.22 1332.44 1836.15 1.89E+003 3.22E+004 7.37E+004 4.15E+004

5. 48E+003 2.64E+004 6.88E+002 1.88E+003 1.54E+004
4. 85E+004 2.05E+002
1. 75E+004 5.11E+004 3.42E+002 4.66E+004 1.12E+004 110.49 369.12 531.53 406.72 188.50 327.06 120.69 135.19 251.02 423.44 82.36 266.28 431.13 55.80 411.65 202.77 3.19E+003 2.32E+004 3.12E+004
1. 83E+004
1. 43E+004 1.40E+004 6.72E+003 5.81E+003
8. 62E+003 7.09E+003 2.89E+003 5.49E+003 3.42E+003
8. 68E+002
9. OOE+002
3. 07E+002 M - First peak in m = Other peak in F = Fitted singlet a multiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/17/02 5:58:08 PM Page 4 I ***** N.UCLIDE IDENTIFICATION REPORT 6 Sample I.D. C:\\GENIE2K\\CAMFILES\\ENCALO1.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 1.000 122.06* 136. 48* 0.999 1173.22* 1332.49* 0.998 898.02* 1836.01* 1.000 88.03* 1.000 255.12* 391.69* 1.000 661.65* 1.000 165.85* 1.000 279.19* 1.000 59.54* Yield Activity (%) (uCi/Unit) 85.51 1.172E-002 10.60 1.230E-002 100.00 4.676E-002 100.00 4.735E-002 93.40 1.376E-002 99.38 1.416E-002 3.72 6.251E-001 1.93 1.067E-002 64.90 9.315E-003 85.12 3.265E-002 80.35 8.028E-003 77.30 7.675E-004 35.90 8.013E-002 Activity Uncertainty 7.119E-004 9.358E-004 2.375E-003 2.550E-003 6.863E-004 1.205E-003 6.101E-002 2.292E-003 6.117E-004 1.884E-003 5.384E-004 7.771E-005 8.331E-003

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/17/02 5:58:08 PM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\ENCALO1.CNF IL STD 62 s-Date /i/ /7/d2_ Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/Unit) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-8-8 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 1.000 0.999 0.998 1.000 1.000 1.000 1.000 1.000 1.000

1. 19E-002 4.70E-002 1.39E-002 6.25E-001 9.41E-003 3.27E-002 8.03E-003 7.68E-004
8. 01E-002 5.67E-004 1.74E-003
5. 96E-004
6. 1OE-002 5.91E-004
1. 88E-003 5.38E-004 7.77E-005 8.33E-003 4.7 3.7 4.3 9.8 6.3 5.8 6.7 10.1 10.4

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/17/02 5:58:08 PM Page 6 U N I D E N T I F I E D P E A K S Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 F 11 M 14 42.24 813.79 1325.22 5.2527E-001 5.6830E-002 9.5011E-002 5.84 40.26 16.31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

4 /o z l 1 ANALYTICS 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318

  • U.S.A.

Phone (404) 352-8677 Fax (404) 352-2837 CERTIFICATE OF CALIBRATION Standard Radionuclide Source 62866-521 1.0 Liter Solid in 133N GA-MA Beaker This standard radionuclide source was prepared using aliquots mea-sured gravimetrically from master radionuclide solution sources. The Am-241 was calibrated by 4 pi alpha liquid scintillation count-ing. All other radionuclides were calibrated using a germanium gam-ma spectrometer system. Calibration and purity were checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains traceability to the National Institute of Stan-daids and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Rev. 1, February, 1979. US Patent 4,430,258; UK Patent GB2,149,194B; CA Patent 1,196,776. Density of solid matrix 1.15 g/cc. Calibration date: January 1, 2002 12:00 EST GAMMA-RAY ENERGY GAMMA-RAYS PER SECOND TOTAL UNCERTAINTY ISOTOPE HALF-LIFE Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-137 Y-88 Co-60 Co-60 Y-88 59.5 88 122 166 279 392 662 898 1173 1332 1836 432 462.6 271.79 137.6 46.61 115.1 30.07 106.6 5.2714 5.2714 106.6 y d d d d d y d y y d 1057 1390 838. 8 1159 2828 1470 1032 3931 1928 1941 4112 5.0 4.8 4.9 4.5 4.6 4.2 4.0 4.2 4.0 4.0 4.2 P 0 NUMBER 14531, It SOURCE PREPARED BY: Q A APPROVED: t 4

m. D. Currie, Rad ochemist

_j r I C This standard will expire one year after the calibration date.

Certificate File Listing Report 11/13/2002 7:56:16 PM Page 1 CERTIFICATE FILE REPORT Filename: C:\\GENIE2K\\CAMFILES\\100201.CTF Certificate

Description:

Certificate

Title:

62866-521 1L Solid Matrix in mar Quantity 1.00 units Assay date 1/1/2002 12:00:00 PM Nuclide Name Half-Life (Days) Energy (keV ) Emission Rate GPS/Unit Emission Rate % Uncert.(+-) Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-137 Y-88 -60 -60 88 1.579E+005 4.640E+002 2.709E+002 1.377E+002 4.660E+001 1.151E+002 1.102E+004 1.066E+002 1.925E+003 1.925E+003 1.066E+002 59.537*

88. 032 122.063 165. 853 279.189 391. 688 661.649*

898.021 1173.220 1332.490 1836.010* 1057.0 1390.0 838.8 1159.0 2828.0 1470.0 1032.0 3931.0 1928.0 1941.0 4112.0 5.00 4.80 4.90 4.50 4.60 4.20 4.00 4.20 4.00 4.00 4.20

  • - Used for Calib/INIT

G A M M A S P E C T R U M A N A L Y S I S F I name: C:\\GENIE2K\\CAMFILES\\ENCAL01.CNF Report Generated On

11/13/2002 8:51:43 PM Sample Title Spectrum Description Sample Identification Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels)

Peak Area Range (in channels) Identification Energy Tolerance

1 Liter Water calibration spectrum
Calibration Spectrum
IL STD
1
5.00 1-4096 1-4096 1.000 keV Sample Size
1.OOOE+000 Unit Sample Taken On Acquisition Started Live Time Real Time Dead Time
11/13/2002 6:58:59 PM 3600.0 seconds 3649.2 seconds 1.35 %

Energy Calibration Used Done On Efficiency Calibration Used Done On Efficiency ID

11/13/2002
11/13/2002
1

Efficiency Calibration Report 11/13/2002 8:52:15 PM Page 1 E F F I C I E N C Y C A L I B R A T I O N R EPORT ~ i Detector Name: DET01 Sample

Title:

1 Liter Water calibration spectrum Geometry

Description:

1 Efficiency Calibration Performed on: 11/13/2002 8:36:02 PM by: Geometry Type Used: DUAL Efficiency Triplets Energy Efficiency Error 59.54 88.03 122.06 165.85 279.19 391.69 661.65 898.02 1173.22 1332.49 1836.01 8.41E-003 2.37E-002

3. 1OE-002 3.14E-002 2.13E-002
1. 97E-002 1.34E-002 9.76E-003 8.29E-003 7.50E-003 5.96E-003 4.25E-004 1.14E-003 1.53E-003 1.43E-003 1.46E-003 8.49E-004 5.39E-004 4.19E-004 3.34E-004 3.02E-004 2.57E-004 DUAL Efficiency Calibration Equation

= -======== Single Equation Terms -> Offset: Slope: Quadratic: Cubic: 4th Order: 5th Order: 6th Order: 7th Order: 8th Order: 9th Order: -441.296 355. 603 -115. 039

18. 562

-1.496 0.048 0.000

0. 000 0.000 0.000

Energy Calibration Report 11/13/2002 8:48:10 PM Page 1 E N E R G Y C A L I B R A T I O N R E P O R T ,W Detector Name: Sample

Title:

DETO1 1 Liter Water calibration spectrum ENERGY CALIBRATION COEFFICIENTS Energy Calibrpte Performed on: 11/13/2002 8:26:10 PM by: t-- ZaMJ Energy Calibrate Type: POLY Energy(keV) = 0.320 + 0.250*ch + 0.00E+000*ch^2 + 0.OOE+000*chA3 SHAPE CALIBRATION COEFFICIENTS Shape Calibrate Performed on: 11/13/2002 8:26:10 PM by: FWHM 0.623 + 0.046*E^1/2 LOW TAIL = 6.9E-001 + 8.4E-004*E ENERGY CALIBRATION RESULTS TABLE Centroid Channel 237.04 351.09 487.28 662.58 1116.02 1566.26 2646.36 3592.25 4693.53 5331.04 7346.81 Centroid error 0.03 0.03 0.02 0.03 0.10 0.03 0.03 0.03 0.04 0.04 0.04 Energy (keV ) 59.54 88.03 122.06 165.85 279.19 391.69 661.65 898.02 1173.22 1332.49 1836.01 SHAPE CALIBRATION RESULTS TABLE Energy (keV ) 59.54 88.03 122.06 165.85 279.19 391.69 661.65 898.02 1173.22 1332.49 1836.01 FWHM channels 4.34 4.53 4.59 4.87 5.19 5.70 6.74 7.60 8.78 9.36 11.26 FWHM error 0.07 0.06 0.05 0.06 0.26 0.07 0.06 0.06 0.07 0.08 0.07 TAIL channels 2.57 3.16 3.82 4.80 2.85 4.60 5.47 6.09

6. 83 7.47 8.51 TAIL error 0.21 0.29 0.48 1.48 0.71 0.59 0.41 0.42 0.34 0.45 0.33 G A N M A S P E C T R U M A N A L Y S I S

Dual Efficiency Calibration Curve I- - - Low Energy Measured High Energy 0 500 1000 1500 2000 Energy (keV) 2500 Datasource: DET01 in(Eft) = -4.413e+002 + 3.556e+002*(n(E) - 1.150e+002*In(E)^2 + 1.856e+001*In(E)^3 1.496e+000*ln(E)A4 + 4.810e-002*1n(E)A5

Energy Calibration Curve U Measured Calculated 0UU0-2000- ,I C rum I__ I__ I__ I__ I _ __ __ __ _ _I k V 1000 500 0'I-amu 0 1024 2048 3072 4096 Channel 5120 6144 7168 8192 Datasource: DET01 Energy a 3.203eO001 keV FWHM = 6.229e-001 keV Lo Tail

  • 6.87le-0O1 keV

+ 2.499e 001lCh + 4.624e*021E^1/2 + 8.395e*004*E I L %5o1.J

(I-i C ( Date: 11-14-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S(N 64091-486 Duratek# 080201 I CSA.._A As:..:4.. A_ Yield

ource Radvixy on

'MJt0,'2I Count Date: Total Source Activity Uncertainty Current a~ I. ' :,i l1, ffiz,,. 4wi,1 Activity Original 1 Isotope Energy (keV) Activity Activity pamjsec) (uCI) g 7-485E-1 Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-137 Y-88 Co-60 Co-60 Y-88 59.5 88 122 166 279 392 662 898 1173 1332 1836 ,.ovSTL..U 1.008E+00 2.303E-02 3.552E-02 7.821E-02 6.516E-02 3.187E-02 1.008E-01 4.868E-02 4.934E-02 1.037E-01 Activity % difference -2.95 -3.57 -4.12 -2.76 -5.13 -2.21 -0.52 -5.96 0.12 0.25 -1.56 I ' I

1. Source quantification following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from "Radioactive Decay Data Tables D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*100 CC.

'4

G A M M A S P E C T R U M A N A L Y S I S i Report Generated On-Detector Sample I.D. C:\\GEI Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance 11/14/02 6:47:11 PM DET01 NIE2K\\CAMFILES\\250ml calibration.CNF 250mL STD 250 mL marinelli with 1.58 g/cc 1 3.50 100 - 8192 100 - 8192 1.00 keV Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time Background Type 1.OOOE+000 Unit 11/13/02 9:02:22 PM P. Jones 2913.9 seconds 3000.1 seconds 2.87 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 Performed & Reviewed By -6/51 9 Date __ / a _/ Supervisory Review Date /Z: / /7/ °O-I'

Peak Locate Analysis Report 11/14/02 6:47:12 PM Page 2 P E A K L O C A T E R E P O R T Detector Sample I.D. Spectrum Number Sample Description Sample Type DETOI C:\\GENIE2K\\CAMFILES\\250ml calibration.CNF 250mL STD 250 mL marinelli with 1.58 g/cc mat Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence 11/14/02 100 8192 3.50 5.00 6:4.7:11 PM Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 168.20 236.72 281.49 290.11 350. 84 487.01 544.85 662.31 953.88 1019.60 1115.89 1406.80 1566.03 2042.67 2436.10 2646.16 3255.77 3592.00 4693.29 5300.52 5330.79 7346.57 0.1301

0. 0648 0.2916 0.2180
0. 0427
0. 04 66
0. 0852
0. 0432 0.1977
0. 1221
0. 0486 0.2443
0. 0394
0. 1790 0.2437
0. 0367
0. 1427
0. 0341 0.0333 0.1275
0. 0335
0. 0351 42.37 59.46 70.65 72.73 87.99 122.03 136.46 165.84 238.70 255.11 279.18 352.02 391.66 510.79 609.05 661.56 813.89 897.91 1173.10 1324.97 1332.40 1836.09 21.06 74.13 3.70 8.04 163.74 132.04 39.61 142.77 6.79 16.66 100.92 3.92 141.25 5.29 4.11 138.78 7.96 143. 02 133.75 8.82 124.43 97.72 0.7627
1. 1540 1.0578 1.0637
1. 1771
1. 1932 1.2068 1.2526
0. 9910 1.3060
1. 3384
1. 8353
1. 4687
2. 3836
0. 8965
1. 7402
1. 9374
1. 9935 2.2802
2. 4640
2. 4688
2. 9765 Errors quoted at
1. 96 sigma

Peak Analysis Report 11/14/02 6:47:12 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector Sample I.D. Spectrum Number Sample Description DET01-C:\\GENIE2K\\CAMFILES\\250ml calibration.CNF 25OmL STD 250 mL marinelli with 1.58 g/cc matrix Peak Analysis Peak Analysis Peak Analysis Performed on From Channel To Channel 11/14/02 6:47:11 PM 100 8192 Peak ROI ROI No. start end Peak centroid Energy Net Peak Net Area (keV) Area Uncert. Continuum Counts F F M m F F F F F F -F Sw F F F F F F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 164-221-265-265-333-474-532-642-. 947-1009-1107-1401-1541-2027-2430-2624-3247-3569-4671-5286-528 6-7317-176 252 294 294 367 505 562 681 960 1029 1138 1416 1590 2056 2443 2671 3270 3620 4728 5359 5359 7374 168.27 236.68 281.45 289.79 350.86 487.09 544.82 662.40 953.97 1019.64 1115.98 1407.48 1566.12 2042.86 2436.06 2646.21 3255.83 3592.07 4693.33 5301.13 5330.83 7346.55 42.37 59.46 70.65 72.73 87.99 122.03 136.46 165.84 238.70 255.11 279.18 352.02 391.66 510.79 609.05 661.56 813.89 897.91 1173.10 1324. 97 1332.40 1836.09 3.74E+003 3.25E+004

1. 10E+003
1. 33E+003 1.18E+005 7.21E+004 9.42E+003 7.60E+004 6.45E+002 2.45E+003 3.28E+004 5.02E+002 5.91E+004 1.13E+003
1. 84E+002 5.68E+004 7.72E+002
6. 40E+004 6.02E+004 9.44E+002 5.49E+004 3.98E+004 144.40 386.71 207.95 223.82 669.60 533.89 253.42 537.95 159.38 173.91 365.30 135.17 469.08 133.91 96.25 459.91 112.68 486.48 468.90 88.33 446.12 378.57 6.88E+003 4.17E+004 2.29E+004 2.-28E+004
5. 41E+004
3. 67E+004 3.05E+004 3.42E+004 1.OOE+004
1. 27E+004
1. 67E+004 6.25E+003 1.75E+004
8. 19E+003 3.54E+003
1. 30E+004 4.42E+003
1. 06E+004 5.38E+003 2.07E+003 2.13E+003 9.06E+002 M= First peak in m = Other peak in F = Fitted singlet aFmultiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/14/02 6:47:12 PM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\250ml calibration.CNF Nuclide Library Used-C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) CO-57 1.000 122.06* 136.48* CO-60 0.998 1173.22* 1332.49* Y-88 0.999 898.02* 1836.01* CD-109 1.000 88.03* SN-113 1.000 255.12* 391.69* CS-137 0.999 661.65* CE-139 1.000 165.85* HG-203 1.000 279.19* AM-241 0.999 59.54* Yield Activity (%) (uCi/Unit) 85.51 10.60 100.00 100.00 93.40 99.38 3.72 1.93 64.90 85.12 80.35 77.30 35.90

1. 611E-002 1.657E-002 4.637E-002 4.704E-002 4.190E-002 4.316E-002 8.240E-001 2.967E-002 2.871E-002 3.162E-002 1.796E-002 1.051E-002 7.258E-002 Activity Uncertainty 9.356E-004 1.158E-003 2.586E-003 2.782E-003 2.141E-003 3.718E-003 7.999E-002 4.091E-003 1.736E-003 1.897E-003 1.070E-003 6.597E-004 7.792E-003

= Energy line found in the spectrum. @ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/14/02 6:47:12 PM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\250ml calibration.CNF 250mL STD -T7 0: Date ___ /Z/ 10 Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/Unit) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 1.000 0.998

0. 999 1.000 1.000 0.999 1.000 1.000
0. 999
1. 63E-002
4. 67E-002 4.22E-002 8.24E-001 2.89E-002 3.16E-002 1.80E-002 1.05E-002 7.26E-002 7.28E-004 1.89E-003 1.86E-003 8.OOE-002 1.60E-003
1. 90E-003 1.07E-003
6. 60E-004 7.79E-003 4.5 4.1 4.4 9.7 5.5 6.0 6.0 6.3 10.7

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/14/02 6:47:12 PM Page 6 U N I D E N T I F I E D P E A K S Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 M 3 m 4 F 9 F 12 F 14 F 15 F 17 M20 42.37 70.65 72.73 238.70 352.02 510.79 609.05 813.89 1324.97 1.2839E+000 3.7665E-001 4.5612E-001 2.2139E-001 1.7244E-001 3.8689E-001 6.3069E-002 2.6505E-001 3.2411E-001 3.86 18.95 16.84 24.71 26.90 11.88 52.37 14.59 9.35 M = First peak in a multiplet region -m =-Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

ANALYTICS K) 1380 Seaboardn kwudus 81 Adanta, Geoagia 30318 U.SA

  • zo-oz.

X'rcL(( OFLAC)O Pe(4042-a Fax (404) 352-2837 CERTIFICATE OF CALIBRATION Standard Radionuclide Source 64091-466 Sand in 250 mL Marinelli Beaker Filled to Top This standard radionuclide source was prepared using aliquots mea-sured gravimetrically from master radionuclide solution sources. The Am-241 was calibrated by 4 pi alpha liquid scintillation count-ing. All other radionuclides were calibrated using a germanium gam-ma spectrometer system. Calibration and purity were checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains traceability to the National Institute of Stan-dards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Rev. 1, February, 1979. Calibration date: July 1, 2002 12:00 EST TOTAL GAMMKA-RAY GAMMA-RAYS UNCERTAINTY ISOTOPE ENERGY HALF-LIFE PER SECOND Am-241 59.5 432 y 994.2 5.0 Cd-109 88 462.6 d 1439 5.0 Co-57 122 271.79 d 759.8 4.7 Ce-139 166 137.6 d 1086 4.3 Hg-203 279 46.61 d 2358 4.1 Sn-113 392 115.1 d 1600 4.1 Cs-137 662 30.07 y 1009 4.8 Y-88 898 106.6 d 3704 4.2 Co-60 1173 5.2714 y 1799 4.1 Co-60 1332 5.2714 y 1821 4.2 Y-88 1836 106.6 d 3873 4.0 490 grams/310 mL of sand. P 0 NUMBER 14630, Item 2 SOURCE PREPARED BY: V( t D. D

rrie, Radiochemist Q A APPROVED:

/ r/v/4-This standard will expire one year after the calibration date.

~LL.4L t s (-VI 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 - U.SA. 6° Phone (404) 352-8677 Fax (404) 352-2837 email: analytics~mindspring.com www.analyticsinc.com ANALYSIS OF UNCERTAINTY BATCH 109 MIXED GAMMA STANDARDS WITH Am-241 CALIBRATION DATE: July 1, 2002 12:00 EST GGAMMA RAY RANDOM ERROR % SYSTEMATIC ERROR % TOTAL % ENERGY (keV) (99 % CL) 59.5 2.0 3.0 5.0 88 1.8 3.2 5.0 122 2.0 2.7 4.7 166 1.5 2.8 4.3 279 1.1 3.0 4.1 392 1.3 2.8 4.1 662 1.8 3.0 4.8 898 1.2 3.0 4.2 1173 1.3 2.8 4.1 1332 1.4 2.8 4.2 1836 1.0 3.0 4.0 The systematic error includes the error in calibration standards, weighing error, and estimated counting corrections. All uncertain-ties are stated at the 99% confidence level. No interfering gamma emitting impurities were detected during calibration. Depending on the resolution and energy dispersion (kev/channel) of the measuring system, the following spectral conflicts may occur: (1) between the 88 keV gamma-ray and the X-rays emitted in the decay of Eg-203, (2) between the 1333 keV gamma-ray and the 1325 keV single escape peak from the 1836 keV gamma-ray.

Dual Efficiency Calibration Curve Low Energy a Measured High Energy 0 500 1000 1500 2000 Energy (keV) 2500 Datasource: DET01 In(Eff) = -4.144e+002 + 3.289e+002*ln(E) - 1.047e+002*1n(E)A2 + 1.664e+001*In(E)A3

  • 1.322e+000*ln(E)Y4 + 4.197e.002*tn(E)^5 A t 4,

~, / z./f7 /o -a---

Certificate File Listing Report 11/13/2002 7:51:08 PM Page 1 C E R T I F I C A T E F I L E R E P O R T Filename: C:\\GENIE2K\\CAMFILES\\080201.CTF Certificate

Description:

Certificate

Title:

64091-466 250 mL Sand Matrix in Quantity 1.00 units Assay date 7/1/2002 12:00:00 PM Nuclide - Name Half-Life (Days) Energy (keV ) Emission Rate GPS/Unit Emission Rate % Uncert.(+-) Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-137 Y-88 o-60 _-60 T-8 8 1.579E+005 4.640E+002 2.709E+002 1.377E+002

4. 660E+001 1.151E+002 1.102E+004 1.066E+002 1.925E+003 1.925E+003 1.066E+002 59.537*

88.032 122.063 165. 853 279. 189 391. 688 661. 649* 898. 021 1173.220 1332. 490 1836. 010* 994.2 1439.0 759.8 1086.0 2358.0 1600.0 1009.0 3704.0 1799.0 1821.0 3873.0 5.00 5.00 4.40 4.30 4.40 4.20 4.30 4.40 4.40 4.60 4.40

  • = Used for Calib/INIT LL 21131/o; Illn/O z f.

v G A M M A S P E C T R U M A N A L Y S I S-*** Report Generated On Detector Sample I.D. C:\\GE: Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time Background Type 12/12/02 1:21:05 PM DET01 ,NIE2K\\CAMFILES\\QC 120802C.CNF QC120802C.CNF Mixed Gamma un 250ml Marinelli Marinelli 2 3.50 100 - 8192 100 - 8192 1.50 keV 1.000E+000 ea 12/8/02 3:09:01 PM L. Finn 600.0 seconds 616.2 seconds 2.63 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 , I /--, Za  - Performed & Reviewed By Date L /. A/ ecL)- Supervisory Review p Date t2 /ja /

Peak Locate Analysis Report 12/12/02 1:21:05 PM Page 2 P E A K L O C A T E R E P O R T as Detector DET01 Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120802C.CNF Spectrum Number QC120802C.CNF Sample Description Mixed Gamma un 250ml Marinelli Sample Type Marinelli Peak Locate Performed on 12/12/02 1:21:04 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 164.13 236.05 350.08 486.26 543.75 661.37 1018.85 1114.82 1564.84 2644.94 3590.82 4691.98 5297.71 5329.39 7344.88 0.1939 0.1145

0. 0754
0. 0816
0. 1478 0.0768
0. 1967
0. 0911
0. 0661
0. 0570
0. 0541
0. 0499
0. 1827 0.0499 0.0525 41. 61 59.33 87.83 121.86 136.25 165.62 254.92 278.92 391.38 661.26 897.60 1172.77 1324.24 1332.04 1835.69 10.81 16.91
40. 72 34.45 9.98 36.84 5.75 24.43 43.88 52.29 53.28 57. 06 3.55 53.87 43.66
0. 9661 1. 6042
1. 5861
1. 5877
1. 5778
1. 6371 1.5360
1. 7360
1. 7717 1.9741 2.1372 2.3375 2.4677 2.4727 2.7699 Errors quoted at 1.96 sigma

Peak Analysis Report 12/12/02 1:21:05 PM Page 3 ~ ***** P E A K A N A L Y S I S R E P O R T AW)************************************* Detector DET01 Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120802C.CNF Spectrum Number QC120802C.CNF Sample Description Mixed Gamma un 250ml Marinelli Peak Analysis Performed on 12/12/02 1:21:04 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area (keV) Area Uncert. Continuum Counts No. start end centroid F F F F F F F F F i-F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 160-220-335-473-536-650-1010-1101-1553-2 631-3573-4 674-5283-5283-7323-175 244 365 501 553 679 1028 1124 1585 2664 3608 4712 5349 5349 7367 165.23 236.15 350.22 486.38 544.00 661.52 1018.89 1114.92 1565.00 2645.00 3590.81 4692.02 5298.21 5329.40 7344.95 41.61 59.33 87.83 121.86 136.25 165.62 254.92 278.92 391.38 661.26 897. 60 1172.77 1324.24 1332.04 1835.69

8. 87E+002
7. 01E+003 2.43E+004 1.47E+004
1. 77E+003 1.41E+004 4.75E+002 4.70E+003
1. 10E+004
1. 19E+004
1. 15E+004 1.24E+004 2.20E+002 1.13E+004
7. 12E+003 67.93 173.13 288.90 229.72 109.27 221.26 75.55 137.51 196.15 206.29 204.13 211. 05 37.30 201.31 161.77
1. 58E+003
6. 14E+003 8.81E+003 6.13E+003
3. 32E+003
4. 58E+003
2. 09E+003 2.39E+003 2.28E+003 1.70E+003 1.38E+003
6. 43E+002
2. 98E+002
3. 05E+002
1. 53E+002 First peak in a multiplet region Other peak in a multiplet region Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/12/02 1:21:05 PM Page 4 IL N U C L I D E I D E N T I F I C A T I O N R E P O R T / Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120802C.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) Yield Activity (%) (uCi/ea ) CO-57 CO-60 Y~ 88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.997 122.06* 136.48* 0.986 1173.22* 1332.49* 0.990 898.02* 1836.01* 0.997 88.03* 0.994 255.12* 391.69* 0.989 661.65* 0.996 165.85* 0.995 279.19* 0.997 59.54* 85.51 10.60 100.00 100.00 93.40 99.38 3.72

1. 93
64. 90 85.12 80.35 77.30 35.90 1.599E-002 1.510E-002 4.636E-002 4.689E-002 3.646E-002 3.754E-002 8.286E-001 2.791E-002 2.584E-002 3.215E-002
1. 613E-002 7.313E-003 7.682E-002 Activity Uncertainty 9.552E-004 1.349E-003 2.678E-003 2.871E-003 1.953E-003 3.322E-003 8.094E-002 5.531E-003 1.616E-003 1.991E-003 9.862E-004 5.OOOE-004 8.480E-003
  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.500 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 12/12/02 1:21:05 PM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number Performed & Reviewed By -C:\\GENIE2K\\CAMFILES\\QC 120802C.CNF QC120802C.CNF Date la/jvj3- /0.- Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.997 0.986 0.990 0.997 0.994 0.989 0.996 0. 995 0.997

1. 57E-002
4. 66E-002
3. 67E-002 8.29E-001
2. 60E-002 3.21E-002
1. 61E-002 7.31E-003
7. 68E-002
7. 80E-004
1. 96E-003
1. 68E-003
8. 09E-002 1.55E-003
1. 99E-003
9. 86E-004 5.OOE-004 8.48E-003 5.0 4.2 4.6 9.8 6.0 6.2 6.1 6.8
11. 0

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/12/02 1:21:05 PM U N I D E N T I F I E D P E A K S

          • i Page 6

Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 41.61 M 13 1324.24 1.4782E+000 3.6716E-001 7.66 16.93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

I 1j.V9 P i X . -7, T. 1.'.. 11 ( C Date: 12-07-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S/N 64091-466 Duratek# 080201 Isotope Energy (keV) Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-1 13 Cs-137 Y-88 Co-60 Co-60 Y-88 59.5 88 122 168 279 392 662 898 1173 1332 1836 Source Activity on Yield Activity Activity UI (gam/dIs. (gam.lsec) (uCi) 0.359 O~2 7.485E-02 0.0372 1 1.045E;00 :!1 0.8551 T+ 2.401 E-02 0.8035 1 3.653E-02 g 0.773 S$ 8.244E-02. 0.649 ~-.~O 6.663E-02 0.8512 I00 3.204E-02 0.934 1 1.072E-01 1 'I9 4.862E I 1~t 4.922E-02 0.9938 1.053E 1..0 Count Date:

  • otal Source Activity ncertainty Current
10)

(UCi) - -- ------ 1. Activity Original (uCi) Activity % difference Isotope %2 life 8.136E-02 1.074E+00 2.388E-02 3.697E-02 8.377E-02 6.774E-02 3.313E-02 1.043E-01 5.009E-02 5.009E-02 1.043E-01 R 8.70 2.74 -0.55 1.20 1.61 1.66 3.41 -2.67 3.01 1.77 -0.96 I

1. Source quantification following calibration on Nov. 13 2002
2. Gamma ray yields obtained from ZRadioactive Decay Data Tables" D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*100

G AM MA SP EC TR U M ANAL Y SI S @4** Report Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in char Peak-Area Range (in channe Identification Energy Tole Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time Background Type 1/21/03 12:39:11 PM DET01 C:\\GENIE2K\\CAMFILES\\QC 120702B.CNF QC120702B.CNF Mixed Gamma in Marinelli Marinelli 2 3.50 Lnels) 100 - 8192 1ls) 100 - 8192 rance 1.50 keV 1.OOOE+000 ea 12/7/02 1:30:01 PM L. Finn 600.0 seconds 616.6 seconds 2.70 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By ....an. o Date Z /Z7/ a Date _ /x7/03_ Supervisory Review

Peak Locate Analysis Report 1/21/03 12:39:11 PM Page 2 P E A K L O C A T E R E P O R T Detector Sample I.D. C:\\ Spectrum Number Sample Description Sample Type Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence DET01 \\GENIE2K\\CAMFILES\\QC 120702B.CNF QC120702B.CNF Mixed Gamma in Marinelli Marinelli 1/21/03 100 8192 3.50 5.00 12:39:11 PM Peak Centroid No. Channel Centroid Uncertainty Energy (key) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1 6 163.65 236.55 350.46 486.69 544.34 662.03 1019.37 1115.74 1566.19 2647.15 3256.09 3593.76 4695.82 5303.14 5333.69 7351.16 0.2001

0. 1002
0. 0666 0.0724 0.1305
0. 0684
0. 1900 0.0793
0. 0609 0.0532 0.2324
0. 0514
0. 0480 0.1578
0. 0473
0. 0505
41. 45 59.42 87.91 121. 94 136.33 165.77 255.17 279.14 391.70 661. 80 813.98 898.33 1173.73 1325.57 1333.10 1837.19 9.29 27.25
58. 89 49.11 15.23
53. 18 6.45 35.54 57.01 64.09 4.00 62.26 65.68 5.80 64.18 49.83
0. 9089
1. 3447
1. 3043
1. 3099
1. 3014
1. 3678
1. 4929
1. 4051
1. 5030 1.6974
1. 1527 1.8955 2.1014 2.2157 2.2206 2.5209 Errors quoted at
1. 96 s igma

Peak Analysis Report 1/21/03 12:39:11 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector Sample I.D. Spectrum Number Sample Description Peak Analysis Perf4 Peak Analysis From Peak Analysis To C] DET01 C:\\GENIE2K\\CAMFILES\\QC 120702B.CNF QC120702B.CNF Mixed Gamma in Marinelli armed on 1/21/03 12:39:11 PM Channel 'hannel 100 8192 Peak ROI ROI Peak No. start end centroid Energy (keV) Net Peak Area Net Area Uncert. Continuum Counts F F F F F F F F F F F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 160-220-341-478-531-645-1013-1104-1556-2 633-324 9-357 9-4 677-5290-52 90-7330-173 164.61 247 236.51 361 350.54 496 486.73 558 544.31 675 662.10 1029 1019.88 1127 1115.82 1579 1566.25 2659 2647.19 3272 3256.21 3608 3593.76 4712 4695.86 5350 5303.52 5350 5333.64 7371 7350.98 41.45 59.42 87.91 121.94 136.33 165.77 255.17 279.14 391.70 661.80 813.98 898.33 1173.73 1325.57 1333.10 1837.19 8.25E+002 7.47E+003 2.49E+004

1. 47E+004
1. 85E+003 1.45E+004
5. 11E+002 5.05E+003
1. 09E+004 1.21E+004
9. 94E+001
1. 16E+004 1.24E+004 2.57E+002
1. 17E+004 7.21E+003 67.74 178.70 301. 78 237.10 111. 67 231.43 77.74 145.03 200.93 212.94 44.16 207.87 213.80 38.39 207.86 163.96 1.48E+003
6. 95E+003 6.39E+003 4.28E+003 5.25E+003
4. 95E+003 1.98E+003 2.37E+003
1. 70E+003
1. 41E+003 8.73E+002 1.11E+003 7.26E+002 2.38E+002
2. 63E+002 1.33E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

interference Corrected Activity Report 1/21/03 12:39:11 PM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120702B.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.999 122.06* 136.48* 0.978 1173.22* 1332.49* 0.947 898.02* 1836.01* 0.999 88.03* 1.000 255.12* 391.69* 0.998 661.65* 0.999 165.85* 1.000 279.19* 0.999 59.54* Yield (%) 85.51 10.60 100.00 100.00 93.40 99.38 3.72

1. 93 64.90 85.12 80.35 77.30 35.90 Activity (uCi/ea

)

1. 601E-002 1.581E-002 4.622E-002 4.863E-002 3.677E-002 3.802E-002 8.474E-001 3.006E-002 2.572E-002 3.284E-002 1.664E-002 7.867E-003 8.131E-002 Activity Uncertainty 9.578E-004 1.396E-003 2.675E-003 2.977E-003 1.972E-003 3.377E-003 8.278E-002 5.790E-003 1.613E-003 2.035E-003 1.019E-003 5.359E-004 8.914E-003
  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.500 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 1/21/03 12:39:11 PM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T C:\\EI2\\AFLSQ 272.N Sample I.D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\QC 120702B.CNF QC120702B.CNF Date )F/7 3 Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Activity Uncertainty % Wt mean Activity Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.999

0. 978 0.947 0.999 1.000 0.998 0.999 1.000 0.999 1.59E-002 4.73E-002 3.71E-002
8. 47E-001
2. 60E-002 3.28E-002
1. 66E-002 7.87E-003 8.13E-002
7. 90E-004
1. 99E-003
1. 70E-003 8.28E-002
1. 55E-003 2.04E-003 1.02E-003 5.36E-004
8. 91E-003 5.0 4.2 4.6 9.8 6.0 6.2 6.1 6.8 11.0

? = nuclide is part of an undetermined solution-X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 1/21/03 12:39:11 PM

                    • U N I D E N T I F I E D P E A K S
          • i Page 6

Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 F 11 M 14 41.45 813.98 1325.57 1.3750E+000 1.6572E-001 4.2850E-001 8.21 44.41

14. 93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma
    • A***************A*******L***I********************************************
        • G A MMA S PE C TR UM A NA LY SI S***

Report Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in chan Peak-Area Range (in channe Identification Energy Tole Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time Background Type 1/21/03 12:51:38 PM DET01 C:\\GENIE2K\\CAMFILES\\QC 120602.CNF QC120602.CNF Mixed Gamma in 250ml Marinelli 2 3.50 Lnels) 100 - 8192 ls) 100 - 8192 Xrance 1.50 keV 1.000E+000 ea 12/6/02 6:37:12 AM L. Finn 600.0 seconds 616.6 seconds 2.70 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 79f~ Performed & Reviewed By Date _ /fJ/4g Supervisory Revew Date L/5Z'2 Supervisory Review Date I / AZ/_L

Peak Locate Analysis Report 1/21/03 12:51:38 PM Page 2 P E A K L O C A T E R E P 0 R T Detector Sample I.D. C: Spectrum Number Sample Description Sample Type Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence DET01 \\GENIE2K\\CAMFILES\\QC 120602.CNF QC120602.CNF Mixed Gamma in 250ml Marinelli 1/21/03 100 8192 3.50 5.00 12:51:38 PM Peak Centroid No. Channel Centroid Uncertainty Energy Peak (keV) Significance FWHM (keV) 1 2 3 4 S 6 7 8 9 10 11 12 13 14 15 168.21 236.44 350.50 486.81 544.55 662.08 1019.87 1115.58 1565.81 2645.96 3591.90 4693.30 5299.60 5330.75 7346.51 0.1849

0. 1021
0. 0680 0.0740 0.1354 0.0703 0.1917
0. 0832
0. 0628
0. 0557
0. 0533
0. 0500
0. 1865
0. 0507
0. 0538 42.31 59.40 87.92 121.97 136.36 165.79 255.20 279.10 391.61 661.51 897. 90 1173.09 1324.87 1332.39 1836.07 12.12
27. 61 59.29 50.55 13.88 52.90 5.94 32.99 54.13 58.78 57.14 58.24 3.70 53.90 40.85
0. 6248
1. 3222
1. 3366
1. 3431 1.3346
1. 3896 1.3719
1. 5037
1. 5859 1.8568 2.0569 2.3502 2.5461
2. 5510 2.9951 Errors quoted at 1.96 sigma

Peak Analysis Report 1/21/03 12:51:38 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector DET01 Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120602.CNF Spectrum Number QC120602.CNF Sample Description Mixed Gamma in 250ml Peak Analysis Performed on 1/21/03 12:51:38 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI No. start end Peak centroid Energy Net Peak Net Area Continuum (keV) Area Uncert. Counts F F F F F F F F F F F M m F 1 164-2 220-3 333-4 472-5 530-6 652-7 1014-8 1104-9 1551-10 2623-11 3577-12 4667-13 5288-14 5288-15 7320-172 252 367 504 552 681 1029 1131 1585 2671 3618 4722 5357 5357 7371 168.03 236.44 350.58 486.83 544.41 662.20 1019.99 1115.67 1565.91 2646.03 3592.01 4693.31 5300.71 5330.79 7346.48 42. 31 59.40 87.92 121.97 136.36 165.79 255.20 279.10 391.61 661.51 897.90 1173.09 1324.87 1332.39 1836.07 5.63E+002 6.87E+003 2.38E+004 1.44E+004

1. 73E+003
1. 38E+004 4.06E+002 4.96E+003
1. 07E+004
1. 17E+004
1. 15E+004 1.24E+004 1.81E+002 1.11E+004 7.27E+003 65.06 173.83 295.69 234.23 111.00 226.61 76.35 143.50 198.65 207.34 206.13 211.48 38.32 199.34 162.07 8.22E+002 8.21E+003
1. 09E+004 7.35E+003
4. 42E+003 4.74E+003
1. 95E+003 2.92E+003
2. 66E+003
2. 60E+003 1.74E+003
9. 64E+002 3.49E+002 4.30E+002
2. 03E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 1/21/03 12:51:38 PM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120602.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) Yield Activity (%) (uCi/ea ) CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.999 122.06* 136.48* 0.999 1173.22* 1332.49* 0.999 898.02* 1836.01* 0.999 88.03* 1.000 255.12* 391.69* 0.999 661.65* 1.000 165.85* 0.999 279.19* 0.999 59.54* 85.51 10.60 100.00 100.00 93.40 99.38 3.72 1.93

64. 90 85.12 80.35 77.30 35.90 1.559E-002 1.479E-002 4.635E-002 4.608E-002 3.645E-002 3.832E-002
8. 113E-001 2.386E-002 2.517E-002

-3.159E-002 -1.582E-002 7.728E-003 7.489E-002 Activity Uncertainty 9.336E-004 1.344E-003 2.679E-003 2.823E-003 1.954E-003 3.391E-003 7.928E-002 5.302E-003 1.580E-003 1.960E-003 9.708E-004 5.271E-004 8.241E-003

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.500 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 1/21/03 12:51:38 PM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\QC 120602.CNF QC12002.CNF Date _7_ Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.999 0.999 0.999 0.999

1. 000 0. 999 1.000
0. 999 0.999 1.53E-002
4. 62E-002
3. 69E-002 8.11E-001 2.51E-002
3. 16E-002
1. 58E-002 7.73E-003 7.49E-002
7. 67E-004
1. 94E-003
1. 69E-003
7. 93E-002
1. 51E-003 1.96E-003 9.71E-004 5.27E-004 8.24E-003 5.0 4.2 4.6 9.8 6.0 6.2 6.1 6.8 11.0

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 1/21/03 12:51:38 PM U N I D E N T I F I E D P E A K S Page 6 Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 42.31 M 13 1324.87 9.3766E-001 3.0242E-001 11.56 21.12 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

C N I t C 1

' `

, :3 1.z, k - % I 7 6,;. p. ( Date: 12-06-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics SIN 64091-466 Duratek# 080201 A_ -1.11 Source Activity on Yield Activity Activity Count Date: Total Source Activity Activity Uncertainty Current Original (%) (uCi) (uCI) Isotope Energy (k) Activity % difference Isotope Y/2 life _4._, Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-137 Y-88 Co-60 Co-60 Y-88 59.5 88 122 166 279 392 662 898 1173 1332 1836 7.495E-02 1.027E+00 2.292E-02 3.501E-02 8.107E-02 6.500E-02 3.192E-02 1.031E-01 4.890E-02 4.890E-02 1.031E-01 0.14 -1.78 -4.55 -4.16 -1.67 -2.45 -0.38 -3.82 0.58 -0.63 -2.13 I I

1. Source quantification following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from wRadioactive Decay Data Tables" D.C. Kocher
3. Activity % difference = (Original Activity - Certified Activity) / Certified Activity*l100

G A M M A S P E C T R U M A N A L Y S I S Report Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in char Peak Area Range (in channe Identification Energy Tole Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time 't/ Background Type 12/5/02 10:32:21 AM DET01 C:\\GENIE2K\\CAMFILES\\QC 120502A.CNF QC120502A.CNF Mixed Gamma in 250ml Marinelli 2 3.50 inels) 100 - 8192 sls) 100 - 8192 srance 1.50 keV 1.OOOE+000 ea 12/5/02 10:17:04 AM L. Finn 600.0 seconds 616.6 seconds 2.70 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used Performed & Reviewed ByeB' 11/13/02 11/13/02 2 Date..Lj5-1/vZ0 Supervisory Review 2!  2  4 01 4-z:::  Date /22 / 5 / 69

Peak Locate Analysis Report 12/5/02 10:32:21 AM Page 2 PE AK L OC A TE RE PO RT Detector Sample I.D. Spectrum Number Sample Description Sample Type DETO1 C:\\GENIE2K\\CAMFILES\\QC 120502A.CNF QC120502A.CNF Mixed Gamma in 250ml Marinelli Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence 12/5/02 100 8192 3.50 5.00 10:32:20 AM Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 .6 7 8 9 'V 10 11 12 13 14 15 168.10 236.18 350.23 486.53 544.32 661.91 1019.03 1115.47 1565.66 2645.86 3591.98 4693.31 5300.57 5330.82 7346.71

0. 1938 0.0955 0.0638
0. 0699 0.1256 0.0663
0. 1856 0.0794
0. 0607
0. 0543
0. 0524
0. 04 93 0.1614
0. 04 97
0. 0533 42.40 59.34 87.86 121.90 136.34 165.72 254.94 279.06 391.56 661.49 897.91 1173.10 1325.00 1332.39 1836.13 9.91 33.77 73.70 57.38 17.30 62.66 6.74 37.15 59.74 63.53 60.34 61.09 4.89 57.15 42.80 0.8441
1. 1653
1. 1865
1. 1794
1. 1220
1. 2227
1. 3252 1.3116
1. 4456
1. 7395
1. 9951 2.2829
2. 4 620
2. 4668
2. 9139 Errors quoted at
1. 96 stigma

Peak Analysis Report 12/5/02 10:32:21 AM Page 3 P E A K A N A L Y S I S R E P O R T ' V Detector Sample I.D. Spectrum Number Sample Description DET01 C:\\GENIE2K\\CAMFILES\\QC 120502A.CNF QC120502A.CNF Mixed Gamma in 250ml Peak Analysis Performed on Peak Analysis From Channel Peak Analysis To Channel 12/5/02 10:32:21 AM 100 8192 Peak ROI ROI No. start end Peak centroid Energy Net Peak Net Area (keV) Area Uncert. Continuum Counts F F F F F F F F F F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 164-225-333-468-538-651-1011-1105-1554-2626-3543-4669-5288-5288-7322-176 251 367 504 551 681 1025 1124 1585 2664 3615 4723 5359 5359 7369 168.40 236.17 350.31 486.57 544.34 661.91 1018.96 1115.49 1565.71 2645.94 3592.05 4693.33 5301.23 5330.80 7346.73 42.40 59.34 87.86 121.90 136.34 165.72 254.94 279.06 391.56 661.49 897.91 1173.10 1325.00 1332.39 1836.13 7.75E+002 6.81E+003 2.40E+004 1.41E+004 1.66E+003 1.37E+004 4.32E+002 4.68E+003 1.07E+004 1.18E+004

1. 16E+004 1.24E+004 2.74E+002 1.11E+004 7.15E+003
66. 60 175.77 301.02 235.73 110.63 230.16 75.81 142.71 200.80 209.57 207.04 212.69 40.22 200.41 161.43 1.33E+003
6. 86E+003
1. 03E+004
8. 31E+003 2.83E+003 5.07E+003 1.78E+003 2.23E+003 2.38E+003 2.01E+003 2.94E+003
9. 91E+002 2.85E+002 3.29E+002
1. 92E+002 M = First peak in m = Other peak in F = Fitted singlet a multiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/5/02 10:32:21 AM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120502A.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) CO-57 0.998 122.06* 136.48* CO-60 0.999 1173.22* 1332.49* Y-88 0.999 898.02* 1836.01* CD-109 0.998 88.03* SN-113 0.999 255.12* 391.69* CS-137 0.998 661.65* CE-139 0.999 165.85* HG-203 0.999 279.19* AM-241 0.997 59.54* Yield Activity (%) (uCi/ea ) 85.51 10.60 100.00 100.00 93.40 99.38 3.72 1.93 64.90 85.12 80.35 77.30 35.90 1.527E-002

1. 418E-002 4.640E-002 4.630E-002 3.675E-002 3.772E-002 8.191E-001 2.540E-002 2.511E-002 3.179E-002 1..571E-002 7.278E-003 7.464E-002 Activity Uncertainty 9.167E-004 1.315E-003 2.682E-003 2.837E-003 1.970E-003 3.340E-003 8.008E-002 5.373E-003 1.578E-003 1.972E-003 9.656E-004 5.016E-004 8.255E-003
  • = Energy line found in the spectrum.

Q = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.500 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 12/5/02 10:32:21 AM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number C:\\GENIE2K\\CAMFILES\\QC 120502A.CNF QC120502A.CNF Performed & Reviewed By Date V,/ 6'/ O;> Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 -Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.998

0. 999 0.999 0.998
0. 999 0.998
0. 999
0. 999 0.997 1.49E-002
4. 64E-002 3.70E-002 8.19E-001 2.51E-002 3.18E-002
1. 57E-002 7.28E-003 7.46E-002 7.52E-004 1.95E-003 1.70E-003
8. 01E-002
1. 51E-003 1.97E-003 9.66E-004 5.02E-004 8.25E-003 5.0 4.2
4. 6 9.8 6.0 6.2 6.1 6.9 11.1

? - nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/5/02 10:32:21 AM U N I D E N T I F I E D P E A K S Page 6 Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 42.40 M 13 1325.00 1.2916E+000 4.5586E-001 8.59 14.70 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

          • GA MM A S PE CT R UM A NAL Y SI S***

Report Generated On Detector Sample I.D. C:\\GE] Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time l V Background Type 12/4/02 7:36:10 AM DET01 gIE2K\\CAMFILES\\QC 120402..CNF QC120402.CNF Mixed Gamma in 250ml marinelli marinelli 2 3.50 100 - 8192 100 - 8192 1.00 keV 1.OOOE+000 ea 12/4/02 6:51:44 AM P. Jones 600.6 seconds 617.3 seconds 2.70 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By Date X1/ 5A/.Q do Supervisory Review Supevisoy ReiewDate .5( t'- Date _ / 5 lo-a

Peak Locate Analysis Report 12/4/02 7:36:10 AM Page 2 P E A K L O C A T E R E P O R T Detector Sample I.D. Spectrum Number Sample Description Sample Type DET01 C:\\GENIE2K\\CAMFILES\\QC 120402.'.CNF QC120402.CNF Mixed Gamma in 250ml marinelli marinelli Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence 12/4/02 100 8192 3.50 5.00 7:36:10 AM Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 168.17 235.93 289.43 350.05 486.22 544.04 661.54 1019.28 1115.17 1565.30 2645.42 3591.31 4692.62 5299.51 5329.92 7345.82 0.1911 0.0945 0.2926 0.0636 0.0702

0. 1232 0.0655 0.1817
0. 0785 0.0600
0. 0542
0. 0523
0. 04 92
0. 1730
0. 0495
0. 0529 42.32 59.26 72.59 87.81 121.85 136.27 165.65 255.04 278.98 391.48 661.38 897.74 1172.93 1324.69 1332.20 1835.93 9.52 35.15 4.24 73.86 58.93 18.69 60.21 7.54 39.70 60.97 62.37 60.88 61.55 3.79 57.52 43.15
0. 8000
1. 1330
0. 4750
1. 1495
1. 1803 1.1276 1.2472 1.2541 1.2710
1. 4639
1. 7440
2. 0053 2.2510
2. 4169
2. 4217
2. 8893 Errors quoted at
1. 96 sigma

Peak Analysis Report 12/4/02 7:36:10 AM Page 3

                                                                                                                                                • I**

P EAK A NAL Y SI S RE P OR T*** Detector Sample I.D. Spectrum Number Sample Description DET01 C:\\GENIE2K\\CAMFILES\\QC 120402..CNF QC120402.CNF Mixed Gamma in 250ml marinelli Peak Analysis Peak Analysis Peak Analysis Performed on From Channel To Channel 12/4/02 100 8192 7:36:10 AM Peak ROI ROI No. start end Peak centroid Energy Net Peak Net Area (keV) Area Uncert. Continuum Counts F F F F F F F F F F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 164-222-285-340-474-537-644-1012-1104-1544-2631-3567-4669-5283-5283-7322-175 246 293 366 504 552 681 1027 1124 1588 2672 3618 4718 5357 5357 7371 168.10 235.89 289.21 350.12 486.35 544.06 661.65 1019.36 1115.15 1565.36 2645.51 3591.37 4692.68 5300.01 5330.04 7345.92 42.32 59.26 72.59 87.81 121.85 136.27 165.65 255.04 278.98 391.48 661.38 897.74 1172.93 1324.69 1332.20 1835.93 7.02E+002 6.70E+003

1. 47E+002 2.31E+004 1.40E+004 1.80E+003 1.42E+004
4. 60E+002 4.72E+003 1.llE+004 1.18E+004 1.17E+004 1.23E+004 2.31E+002
1. 11E+004 7.28E+003 64.21 175.50 80.16 298.91 235.80 111.61 233.08 76.32 144.29 203.92 209.20 208.03 212.06 38.27 200.59 162.99
1. 18E+003
6. 64E+003 2.92E+003 8.33E+003
6. 92E+003 3.08E+003 6.23E+003 1.91E+003 2.36E+003
3. 06E+003 2.24E+003
1. 93E+003
8. 97E+002 3.24E+002 3.27E+002 1.97E+002 M = First peak in m = Other peak in F = Fitted singlet a multiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/4/02 7:36:10 AM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 120402..CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Name Confidence Energy (keV) CO-57 CO-60 Y-8 8 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.993 122.06* 136.48* 0.987 1173.22* 1332.49* 0.993 898.02* 1836.01* 0.992 88.03* 0.993 255.12* 391.69* 0.989 661.65* 0.994 165.85* 0.993 279.19* 0.988 59.54* Yield Activity (%) (uCi/ea 85.51 1.520E-002 10.60 1.537E-002 100.00 4.593E-002 100.00 4.608E-002 93.40 3.722E-002 99.38 3.838E-002 3.72 7.869E-001 1.93 2.703E-002 64.90 2.623E-002 85.12 3.182E-002 80.35 1.627E-002 77.30 7.344E-003 35.90 7.373E-002 Activity Uncertainty 9.128E-004 1.375E-003 2.656E-003 2.825E-003 1.993E-003 3.395E-003 7.699E-002 5.505E-003 1.644E-003 1.974E-003 9.982E-004 5.062E-004 8.196E-003 Activity

  • = Energy line found in the spectrur

@ = Energy line not used for Weighte Energy tolerance used was 1.000 Nuclide confidence index threshold = Errors quoted at 1.960 sigma Tn. I Mean 0.10

Interference Corrected Activity Report 12/4/02 7:36:10 AM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\QC 120402..CNF QC120402.CNF all$ C05%., Date Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.993 0.987 0.993 0.992 0.993 0.989 0.994 0.993 0.988

1. 53E-002
4. 60E-002 3.75E-002 7.87E-001
2. 63E-002 3.18E-002
1. 63E-002 7.34E-003 7.37E-002 7.60E-004
1. 94E-003 1.72E-003
7. 70E-002
1. 58E-003
1. 97E-003
9. 98E-004 5.06E-004 8.20E-003 5.0 4.2 4.6 9.8 6.0 6.2 6.1 6.9 11.1

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity N@ Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/4/02 7:36:10 AM U N I D E N T I F I E D P E A K S Page 6 Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 42.32 F 3 72.59 M 14 1324.69 1.1688E+000 2.4415E-001 3.8491E-001 9.15 54.66 16.55 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

          • GA MM A S PE C TR UM A NA LY SI S***

Report Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry DET01 12/3/02 6:17:57 PM DET01 QC120302.CNF Mixed Gamma in 250ml marinelli marinelli 2 Peak Locate Threshold Peak Locate Range (in channels) Peak-Area Range (in channels) Identification Energy Tolerance Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time i wBackground Type 3.50 100 - 8192 100 - 8192 1.00 keV 1.OOOE+000 ea 12/3/02 5:40:41 PM P. Jones 600.6 seconds 617.5 seconds 2.73 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By SesytRo Dt Date _~ / 3 / da-Supervisory Review Date /C/g2

Peak Locate Analysis Report 12/3/02 6:17:57 PM Page 2 P E A K L O C A T E R E P O R T Detector Sample I.D. Spectrum Number Sample Description Sample Type DET01 DET01 QC120302.CNF Mixed Gamma in 250ml marinelli marinelli Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence 12/3/02 100 8192 3.50 5.00 6:17:37 PM Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 168.53 236.68 290.27 350.78 487.00 544.59 662.24 1019.53 1115.80 1565.99 2329.93 2646.05 3256.32 3591.89 4693.23 5299.23 5330.56 5844.45 7346.41 0.1912 0.0968

0. 3021 0.0640
0. 0696
0. 1247 0.0659
0. 1980
0. 0776
0. 0596 0.2239 0.0542 0.2200
0. 0516
0. 0491
0. 1797
0. 0492
0. 1823 0.0519 42.18 59.44 72.90 87.97 122.03 136.42 165.83 255.10 279.16 391.65 582.53 661.53 814.03 897.88 1173.08 1324.75 1332.36 1460.75 1836.05 9.57 33.37 4.37 73.01 60.11 18.74 61.11 6.13 40.23 61.35 4.30 63.26 3.69 62.69 62.84 4.05 58.40 4.81 46.17
0. 6063
1. 1747
0. 3374
1. 1770
1. 1966 1.0622
1. 2350 1.2749 1.2940
1. 4515 1.2856
1. 7325 2.1298
1. 9468 2.2115
2. 3782 2.3832
1. 6900
2. 8327 Errors quoted at
1. 96 sigma

Peak Analysis Report 12/3/02 6:17:57 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector Sample I.D. Spectrum Number Sample Description DET01 DET01 QC120302.CNF Mixed Gamma in 250ml marinelli Peak Analysis Peak Analysis Peak Analysis Performed on From Channel To Channel 12/3/02 100 8192 6:17:56 PM Peak ROI ROI No. start end Peak centroid Energy Net Peak Net Area (keV) Area Uncert. Continuum Counts F F F F F F F F F F F F F F F M m F F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 164-221-284-334-472-537-653-1014-1108-1552-2324-2624-3248-3573-4671-5288-5288-5836-7323-171 248 294 367 505 557 681 1029 1129 1588 2338 2669 3269 3619 4721 5359 5359 5855 7371 167.52 236.61 290.46 350.78 487.07 544.65 662.35 1019.61 1115.88 1566.07 2329.93 2646.10 3256.39 3591.93 4693.25 5300.22 5330.68 5844.48 7346.41 42.18 59.44 72.90 87.97 122.03 136.42 165.83 255.10 279.16 391.65 582.53 661.53 814.03 897.88 1173.08 1324.75 1332.36 1460.75 1836.05 4.52E+002 6.73E+003

1. 47E+002 2.38E+004 1.44E+004 1.68E+003
1. 39E+004 3.68E+002
4. 99E+003
1. 11E+004 1.27E+002 1.18E+004
1. 65E+002
1. 18E+004
1. 21E+004
1. 94E+002 1.13E+004 9.37E+001
7. 45E+003 62.26 174.61 118.62 301.70 237.60 109.19 232.48 75.84 146.37 204.52 50.31 210.05 50.16 209.08 211.39 37.75 202.84 32.01 165.25
7. 94E+002 7.20E+003 3.80E+003
1. 08E+004 7.39E+003
3. 94E+003 4.96E+003
1. 97E+003 2.39E+003 2.64E+003 7.20E+002 2.51E+003 7.70E+002 1.72E+003
9. 87E+002 3.14E+002 3.53E+002 2.08E+002 1.42E+002 m =

F = First peak in Other peak in i Fitted singlet a multiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/3/02 6:17:57 PM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. DET01 Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 1.000 122.06* 136.48* 0.997 1173.22* 1332.49* 0.998 898.02* 1836.01* 0.999 88.03* 1.000 255.12* 391.69* 0.998 661.65* 1.000 165.85* 1.000 279.19* 0.999 59.54* Yield (%) 85.51 10.60 100.00 100.00 93.40 99.38

3. 72 1.93 64.90 85.12 80.35 77.30 35.90 Activity (uCi/ea

) 1.560E-002 1.434E-002 4.528E-002 4.688E-002 3.748E-002 3.926E-002 8.101E-001 2.159E-002

2. 621E-002 3.175E-002 1.599E-002 7.760E-003 7.308E-002 Activity Uncertainty 9.349E-004 1.313E-003
2. 622E-003 2.872E-003 2.006E-003 3.472E-003 7.917E-002 5.134E-003 1.643E-003 1.971E-003 9.821E-004 5.307E-004 8.033E-003 Activity
  • = Energy line found in the spectrur

@ = Energy line not used for Weighte( Energy tolerance used was 1.000 Nuclide confidence index threshold = Errors quoted at 1.960 sigma m. i Mean 0.10

Interference Corrected Activity Report 12/3/02 6:17:57 PM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number DET01 QC120302.CNF z2 O C2 Performed & Reviewed By Date i9/ 3 / t D_ Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 1.000 0.997 0.998

0. 999 1.000 0.998 1.000 1.000
0. 999
1. 52E-002 4.60E-002 3.79E-002
8. 1OE-001 2.58E-002 3.18E-002
1. 60E-002 7.76E-003 7.31E-002
7. 61E-004 1.94E-003 1.74E-003 7.92E-002 1.56E-003
1. 97E-003 9.82E-004 5.31E-004 8.03E-003 5.0 4.2 4.6 9.8 6.1 6.2 6.1 6.8 11.0

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at

1. 96 sigma

Interference Corrected Activity Report 12/3/02 6:17:57 PM Page 6 Peak Energy No. (keV) U N I D E N T I F I E D Peak Size in Counts per Second P E A K S Peak CPS % Uncertainty F F F F M F 1 3 11 13 16 18 42.18 72.90 582.53 814.03 1324.75 1460.75 7.5203E-001 2.4556E-001 2.1186E-001 2.7421E-001 3.2364E-001 1.5600E-001 13.78 80.42 39.54 30.46 19.42

34. 16 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet ErrQrs quoted at
1. 96 sigma

G A M M A S P E C T R U M A N A L Y S I S <W Report Generated On Detector Sample I.D. C:\\GEI Spectrum Number -Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time "'Background Type 11/26/02 8:57:42 AM DET01 gIE2K\\CAMFILES\\QC 112602.CNF QC112602.CNF Mixed Gamma in 250ml Marinelli Marinelli 2 3.50 100 - 8192 100 - 8192 1.00 keV 1.OOOE+000 ea 11/26/02 8:38:54 AM L. Finn 600.0 seconds 617.1 seconds 2.77 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By Suerior eve Dat .-. /kJ? Date __ / _6 _.? Supervisory Review Date ZA}/ _ °

Peak Locate Analysis Report 11/26/02 8:57:42 AM Page 2 P E A K L O C A T E R E P O R T Detector DET01 Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 112602.CNF Spectrum Number QC112602.CNF Sample Description Mixed Gamma in 250ml Marinelli Sample Type Marinelli Peak Locate Performed on 11/26/02 8:57:41 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 167.82 236.50 350.65 486.87 544.74 662.07 953.18 1019.24 1115.53 1565.77 2645.75 3591.60 4692.86 5299.88 5330.23 7345.75 0.1926 -0. 0986 0.0639 0.0698

0. 1294 0.0653 0.2683 0.1938
0. 0755 0.0597 0.0544 0.0516
0. 0497 0.1659 0.04 96
0. 0531 42.06 59.42 87.94 121.99 136.44 165.79 238.50 255.02 279.10 391.60 661.47 897.80 1172.99 1324.75 1332.26 1835.91 10.05 32.21 73.77 59.16 16.60 63.92
4. 17 5.48 41.31 61.61 63.12 62.22 60.55 4.83 56.98 42.29
0. 4835
1. 1743
1. 1684 1.1906 1.2064 1.2370 0.8611 1.7176 1.3119 1.4575 1.7362 1.9757 2.2664 2.4616
2. 4664
2. 9504 Errors quoted at
1. 96 sigma

Peak Analysis Report 11/26/02 8:57:42 AM Page 3 P E A K A N A L Y S I S R E P O R T h Detector Sample I.D. Spectrum Number Sample Description Peak Analysis Perfo Peak Analysis From Peak Analysis To C] DET01 C:\\GENIE2K\\CAMFILES\\QC 112602.CNF QC112602.CNF Mixed Gamma in 250ml Marinelli ormed on 11/26/02 8:57:41 AM Channel .iannel 100 8192 Peak ROI ROI No. start end Peak centroid Energy Net Peak (keV) Area Net Area Continuum Uncert. Counts F F F F F F F F F F ('V)F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 164-224-333-474-534-652-949-1004-1101-1551-2624-3570-4671-5285-5285-7323-170 251 367 505 556 681 958 1028 1129 1590 2668 3614 4713 5357 5357 7372 167.02 236.50 350.66 486.93 544.74 662.18 953.16 1019.28 1115.63 1565.87 2645.84 3591.62 4692.91 5300.25 5330.28 7345.86 42.06 59.42 87.94 121.99 136.44 165.79 238.50 255.02 279.10 391.60 661.47 897.80 1172.99 1324.75 1332.26 1835.91 3.72E+002

6. 66E+003 2.40E+004
1. 43E+004
1. 77E+003 1.47E+004 1.29E+002 5.80E+002 5.60E+003 1.13E+004
1. 16E+004 1.21E+004
1. 21E+004
2. 44E+002 1.13E+004 7.45E+003 57.41 174.76 302.94 238.17 111.61 237.45 68.34 81.01 152.69 205.91 208.76 212.33 210.93 40.28 201.74 164.44 6.81E+002
7. 41E+003
1. 09E+004 7.31E+003 4.50E+003 4.89E+003
1. 37E+003 2.90E+003 3.05E+003 2.89E+003 2.41E+003
1. 80E+003 9.95E+002
3. 60E+002 3.78E+002
1. 94E+002 M = First peak in m = Other peak in F = Fitted singlet a multiplet region a multiplet region Errors quoted at
1. 96 sigma

Interference Corrected Activity Report 11/26/02 8:57:42 AM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 112602.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Name Confidence Energy (keV) Yield Activity (%) (uCi/ea ) CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.999 122.06* 136. 48* 0.992 1173.22* 1332.49* 0.995 898.02* 1836.01* 0.999 88.03* 0.999 255.12* 391.69* 0.995 661.65* 0.999 165.85* 0.999 279.19* 0.998 59.54* 85.51 10.60 100.00 100.00 93.40 99.38 3.72 1.93 64.90 85.12 80.35 77.30 35.90 1.555E-002 1.515E-002 4.521E-002 4.684E-002 3.863E-002 3.927E-002 8.188E-001 3.409E-002 2.660E-002 3.143E-002

1. 691E-002 8.720E-003 7.248E-002 Activity Uncertainty 9.323E-004 1.365E-003 2.618E-003 2.869E-003 2.065E-003 3.471E-003 8.003E-002 6.239E-003 1.667E-003 1.952E-003 1.036E-003 5.888E-004 7.985E-003
  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/26/02 8:57:42 AM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Spectrum Number C:\\GENIE2K\\CAMF.ILES\\QC 112602.CNF QC112602.CNF Performed & Reviewed By Date 1/ /1(24a/i2Z Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.999 0.992 0.995

0. 999
0. 999 0.995
0. 999
0. 999 0.998 1.54E-002
4. 60E-002
3. 88E-002 8.19E-001 2.71E-002 3.14E-002
1. 69E-002 8.72E-003 7.25E-002 7.70E-004 1.93E-003
1. 77E-003
8. OOE-002 1.61E-003
1. 95E-003 1.04E-003 5.89E-004
7. 98E-003 5.0 4.2 4.6 9.8 5.-9 6.2 6.1 6.8 11.0

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/26/02 8:57:42 AM Page 6 U N I D E N T I F I E D P E A K S Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty F 1 42.06 F 7 238.50 M 14 1324.75 6.2016E-001 2.1574E-001 4.0689E-001 15.43 52.79 16.50 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

t tII-( Date: 11-25-02 250 ml Marinenli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S/N 64091-466 Duratek# 080201 .......... I........ I -.. - . - Isotope Energy Yield ckeV) (gamldis.) CEA.. - A AA&z.*;*%S A_ ouuiru /ActIIvity Un Activity Activity ':", B2UiN.. Count Date: Total Source Activity Uncertainty Current M (ucin Activity Original (uCi) Activity % difference Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-137 Y-88 Co-60 Co-60 Y-88 59.5 88 122 186 279 392 662 898 1173 1332 1836 0.359 0.0372 0.8551 0.8035 0.773 0.o49 0.8512 0.934 0 0.9938 7.315E-02 1.018E+00 2.287E-02 3.522E-02 7.934E-02 6.592E-02 3.280E-02 1.025E-01 4.818E-02 4.818E-02 1.025E-01 -2.27 -2.66 -4.77 -3.59 -3.77 -1.06 2.39 -4.39 -0.90 -2.10 -2.71 I I

1. Source quantification following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from *Radioactive Decay Data Tables" D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*1 00

G A M M A S P E C T R U M A N A L Y S ~I S Report Generated On Detector Sample I.D. C:\\GE Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time k)% Dead Time Background Type 11/25/02 7:41:16 AM DET01 NIE2K\\CAMFILES\\QC 112502.CNF QC112502.CNF MixedGamma in 250ml Marinelli Marinelli 2 3.50 100 - 8192 100 - 8192 1.00 keV 1.OOOE+000 ea 11/25/02 7:28:33 AM L. Finn 600.0 seconds 617.1 seconds 2.78 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By Date // /.75/O2. Supervisory Review Supervisory Review Dat Date {/ /o/ 1M

Peak Locate Analysis Report 11/25/02 7:41:16 AM Page 2 P E A K L O C A T E R E P O R T Detector DETOI Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 112502.CNF Spectrum Number QC112502.CNF Sample Description MixedGamma in 250ml Marinelli Sample Type Marinelli Peak Locate Performed on 11/25/02 7:41:15 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid No. Channel Centroid Uncertainty Energy Peak (keV) Significance FWHM (keV) 1 2 3 4 5 6 7 8 1 9 10 11 12 13 14 15 16 17 168.29 236.60 350.69 486.91 544.83 662.25 953.82 1019.58 1115.73 1566.00 2646.09 3256.72 3592.11 4693.41 5300.24 5330.94 7346.77 0.1819 0.0973

0. 0638 0.0694
0. 1276
0. 0655 0.2528
0. 1790
0. 0761
0. 0592 0.0540 0.2163
0. 0517
0. 0494
0. 1931
0. 0498 0.0526 42.24 59.45 87.96 122.00 136.. 45 165.82 238.60 255.12 279.15 391.64 661.55 814.05 897.94 1173.14 1324.81 1332.43 1836.14 10.19 32.03 73.81 60.31 17.02 62.26 4.60 7.65 41.06 63.10 64.04 4.21 61.98 60.18 4.49 56.23 43.50
0. 6879
1. 1634
1. 1759
1. 18 67
1. 1933 1.2522
0. 7317 1.2577
1. 3600
1. 4560
1. 7428
1. 1926
2. 0113 2.2477
2. 4187
2. 4235
2. 9416 Errors quoted at 1.96 sigma

Peak Analysis Report 11/25/02 7:41:16 AM Page 3 P E A K A N A L Y S I S R E P O R T V Detector Sample I.D. Spectrum Number Sample Description DET01 C:\\GENIE2K\\CAMFILES\\QC 112502.CNF QC112502.CNF MixedGamma in 250ml Marinelli Peak Analysis Peak Analysis Peak Analysis Peak ROI ROI No. start end Performed on From Channel To Channel 11/25/02 7:41:15 AM 100 8192 Peak centroid Energy (keV) Net Peak Net Area Continuum Counts Area Uncert. F F F F F F F F F F , V F F F F M m F 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 164-223-333-473-533-650-949-1014-1105-1551-2626-3250-3573-4 676-5289-528 9-7322.- 172 249 367 501 557 681 960 1030 1130 1584 2668 3265 3618 4713 5357 5357 7369 167.74 236.62 350.72 486.93 544.79 662.32 953.57 1019.69 1115.85 1566.03 2646.19 3256.48 3592.17 4693.49 5300.48 5330.99 7346.76 42.24 59.45 87.96 122.00 136.45 165.82 238.60 255.12 279.15 391.64 661.55 814.05 897.94 1173.14 1324.81 1332.43 1836.14 6.16E+002 6.73E+003 2.40E+004 1.46E+004 1.79E+003 1.46E+004

1. 38E+002 4.76E+002 5.72E+003 1.15E+004 1.20E+004 9.05E+001 1.23E+004 1.23E+004 1.57E+002
1. 09E+004
7. 65E+003 65.98 175.60 301.54 240.45 111.84 236.81 66.77 78.11 153.79 208.11 211.02 44.31 213.57 212.25 39.45 199.97 166.56
9. 10E+002 7.19E+003 1.05E+004 6.99E+003 4.89E+003 5.52E+003
1. 74E+003 2.09E+003 2.67E+003
2. 60E+003 2.28E+003 5.88E+002 1.95E+003 7.82E+002 4.01E+002 4.67E+002 1.76E+002 M = First peak in m = Other peak in F - Fitted singlet a multiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/25/02 7:41:16 AM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 112502.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) CO-57 0.999 122.06* 136.48* CO-60 0.999 1173.22* 1332.49* Y-88 0.998 898.02* 1836.01* CD-109 0.999 88.03* SN-113 1.000 255.12* 391.69* CS-137 0.999 661.65* CE-139 1.000 165.85* HG-203 1.000 279.19* AM-241 0.999 59.54* Yield Activity (%) (uCi/ea ) 85.51 10.60 100.00 100.00 93.40 99.38 3.72 1.93 64.90 85.12 80.35 77.30 35.90 1.581E-002 1.532E-002 4.588E-002 4.555E-002 3.913E-002 4.033E-002

8. 170E-001 2.801E-002 2.716E-002 3.246E-002 1.678E-002 8.906E-003
7. 312E-002 Activity Uncertainty 9.473E-004 1.374E-003 2.655E-003 2.795E-003 2.090E-003 3.563E-003 7.984E-002 5.662E-003 1.700E-003 2.012E-003 1.028E-003 6.OOOE-004 8.039E-003
  • = Energy line found in the spectrum.

Q = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Enterference Corrected Activity Report 11/25/02 7:41:16 AM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T I Sp I*D**C*******E***C*****E***C*112502**CNF Sample I. D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\QC 112502.CNF QC112502.CNF k, Ve, ~Date /1 / L5/V2S Nuclide Nuclide Id Name Confidence Wt mean Activity (uCi/ea ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty CO-57 CO-60

  • Y CD-109 SN-113 CS-137 CE-139 HG-203 AM-241
0. 999
0. 999 0.998
0. 999 1.000
0. 999 1.000 1.000
0. 999
1. 57E-002 4.57E-002 3.94E-002 8.17E-001 2.72E-002 3.25E-002 1.68E-002 8.91E-003 7.31E-002
7. 80E-004 1.92E-003
1. 80E-003 7.98E-002 1.63E-003 2.01E-003 1.03E-003 6.OOE-004 8.04E-003 5.0 4.2 4.6 9.8 6.0 6.2 6.1 6.7 11.0

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/25/02 7:41:16 AM Page 6 I** Peak Energy No. (keV) U N I D E N T I F I E D Peak Size in Counts per Second P E A K S Peak CPS % Uncertainty F F F M 1 7 12 15 42.24 238.60 814.05 1324.81 1.0263E+000 2.3070E-001 1.5083E-001 2.6110E-001 10.71 48.24 48.97 25.18 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

C ( ' Date: 11-24-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S/N 64091-466 Duratek# 080201 Source Activity on Activity Activity

  • 1iMtitw. I Count Date:

Total Source Activity Uncertainty Current oL' I Iau.hi1 Isotope Energy Yield (keV) (narn/dis.) Eg..M. I Activity Original (uCi) Activity % difference I Am-241 Cd-109 Co-57 Ce-139 Hg-203 Sn-113 Cs-1 37 Y-88 Co-6o Co-6O Y-88 59.5 0.359 88 0.0372 122 0.8551 186 0.8035 279 0.773 392 0.649 662 0.8512 898 0.934 1173 1 1332 1 1836 0.9938 7.265E-02 9.999E-01 2.252E-02 3.54BE-02 7.8962-02 6.577E-02 3.199E-02 1.023E-01 4.869E-02 4.869E-02 1.023E-01 -2.94 -4.36 -6.22 -2.93 -4.23 -1.30 -0.14 -4.53 0.15 -1.06 -2.85 I I

1. Source quantificatlon following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from Radioactive Decay Data Tables D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*1 00

G A M M A S P E C T R U M A N A L Y S I S i Report-Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry 11/24/02 8:05:06 AM DET01 C:\\GENIE2K\\CAMFILES\\QC 112402.CNF QC mixed gamma source in 250 mL mar Source 2 Peak Locate Threshold Peak Locate Range (in channels) Peak Area Range (in channels) Identification Energy Tolerance Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time %Background Type 3.50 100 - 8192 100 - 8192 1.00 keV 1.OOOE+000 unit 11/24/02 7:42:12 AM L. Finn 600.0 seconds 617.1 seconds 2.78 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 E Performed & Reviewed By Su r RiL Date // / 242/ O47-Supervisory Review Date _/ /,7i/ O.P,

Peak Locate Analysis Report 11/24/02 8:05:06 AM Page 2 P E A K L O C A T E R E P O R T ii Detector DET01 Sample I.D. C:\\GENIE2K\\CAMFILtS\\QC 112402.CNF Spectrum Number QC Sample Description mixed gamma source in 250 mL marine Sample Type Source Peak Locate Performed on 11/24/02 8:05:05 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid No. Channel Centroid Uncertainty Energy (keV) Peak Significance FWHM (keV) 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 167.94 236.44 350.47 486.80 544.37 662.03 1019.18 1115.61 1565.81 2041.36 2645.92 3255.03 3591.96 4693.32 5299.47 5330.90 7346.67 0.2026 0.0961

0. 0646 0.0697 0.1313
0. 0654
0. 1775
0. 0755 0.0589 0.2407
0. 0543
0. 2114 0.0512 0.0496 0.1707 0.0496
0. 0528 42.14 59.39 87.91 121.96 136.34 165.77 255.07 279.11 391.60 510.30 661.51 813.70 897.91 1173.10 1324.79 1332.42 1836.11
  • 9.47 33.82 70.68 59.31 16.12 64.24 8.12 41.83 63.52 3.53 63.31 4.25 63.13 60.39 5.12 56.87 42.62
0. 5938
1. 1382
1. 1746
1. 1783 1.2521 1.2443
1. 3606
1. 3389 1.4277
1. 6919
1. 7373
1. 5320
1. 9616
2. 2864
2. 4543
2. 4593
2. 9602 Errors quoted at
1. 96 sigma

Peak Analysis Report 11/24/02 8:05:06 AM Page 3

      • P E A K A N A L Y S I S R E P O R T***

I I, Detector Sample I.D. Spectrum Number Sample Description DET01 C:\\GENIE2K\\CAMFILES\\QC 112402.CNF QC mixed gamma source in 250 mL marinelli Peak Analysis Peak Analysis Peak Analysis Peak ROI ROI No. start end Performed on 11/24/02 8:05:05 AM From Channel 100 To Channel 8192 Peak Energy Net Peak Net Area Continuum centroid (keV) Area Uncert. Counts F F F F F F F F F F F F F M m F 1 164-2 220-3 334-4 475-5 530-6 643-7 1010-8 1104-9 1543-10 2025-11 2622-12 3246-13 3572-14 4668-15 5290-16 5290-17 7322-171 252 367 504 553 679 1031 1134 1581 2047 2672 3264 3618 4717 5353 5353 7374 167.37 236.38 350.52 486.79 544.35 662.13 1019.47 1115.69 1565.87 2040.87 2646.01 3255.05 3592.06 4693.35 5300.40 5330.94 7346.67 42.14 59.39 87.91 121.96 136.34 165.77 255.07 279.11 391.60 510.30 661.51 813.70 897.91 1173.10 1324.79 1332.42 1836.11

4. 48E+002
6. 65E+003 2.36E+004 1.43E+004
1. 80E+003 1.48E+004 5.57E+002
5. 78E+003 1.14E+004
1. 66E+002 1.17E+004 1.27E+002 1.23E+004 1.22E+004
2. 15E+002
1. 12E+004 7.72E+003 59.68 173.86 300.39 238.63 112.40 238.36 78.84 154.09 207.54 55.37 208.51 49.68 214.07 211.17 40.01 202.10 166.92 7.44E+002
8. 33E+003 1.07E+004
6. 90E+003 4.75E+003 6.45E+003
2. 61E+003 3.13E+003 2.92E+003 1.28E+003
2. 68E+003 7.53E+002 1.91E+003 9.42E+002 3.30E+002 4.36E+002 1.71E+002 First peak in Other peak in Fitted singlet a multiplet region a multiplet region Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/24/02 8:05:06 AM Page 4 N U C L I D E I D E N T I F I C A T I O N R E P O R T i Sample I.D. C:\\GENIE2K\\CAMFILES\\QC 112402.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Name Confidence (keV) Yield (%) Activity (uCi/unit) Activity Uncertainty CO-57 CO-60 Y-88 CD-109 SN-113 0.998 122.06* 136.48* 0.999 1173.22* 1332.49* 0.998 898.02* 1836.01* 0.998 88.03* 0.999 255.12* 391.69* 0.997 661.65* 0.999 165.85* 0.999 279.19* 0.996 59.54* 85.51 10.60 100.00 100.00 93.40 99.38 3.72 1.93 64.90 85.12 80.35 77.30 35.90 1.557E-002 1.534E-002 4.570E-002 4.678E-002 3.920E-002 4.068E-002 8.041E-001 3.274E-002 2.687E-002 3.166E-002 1.703E-002 8.999E-003 7.253E-002 9.340E-004 1.379E-003 2.644E-003 2.866E-003 2.094E-003 3.592E-003 7.862E-002 6.039E-003 1.683E-003 1.964E-003 1.043E-003 6.055E-004 8.004E-003 CS-137 CE-139 HG-203 AM-241

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Enterference Corrected Activity Report 11/24/02 8:05:06 AM Page S '1 *** I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. Sample I. D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\QC 112402.CNF QC Ok, Date /_ / 5 / 7eL Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/unit) Wt mean Activity Uncertainty Wt mean Activity % Uncertainty CO-57 CO-60 .Y-88 CD-109 SN-113 CS-137 CE-139 HG-203 AM-241 0.998

0. 999 0.998 0.998 0.999 0.997
0. 999
0. 999 0.996
1. 55E-002
4. 62E-002 3.96E-002 8.04E-001 2.73E-002 3.17E-002 1.70E-002 9.OOE-003 7.25E-002 7.73E-004 1.94E-003
1. 81E-003 7.86E-002
1. 62E-003 1.96E-003 1.04E-003 6.05E-004 8.OOE-003 5.0 4.2 4.6 9.8 5.9 6.2 6.1 6.7 11.0

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/24/02 8:05:06 AM Page 6 Peak Energy No. (keV) U N I D E N T I F I E D Peak Size in Counts per Second P E A K S Peak CPS % Uncertainty F 1 42.14 7.4604E-001 F 10 510.30 2.7651E-001 F 12 813.70 2.1176E-001 M 15 1324.79 3.5794E-001 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma 13.33 33.38 39.10 18.63

G A M M A S P E C T R U M A N A L Y S I S %W V Report Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in chan Peak Area Range (in channe Identification Energy Tole Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time % Dead Time Background Type 12/4/02 5:36:44 PM DET01 C:\\GENIE2K\\CAMFILES\\BKG120402.CNF BKG120402.CNF Bkg Check Water 2 3.50 .nels) 100 - 8192 !ls) 100 - 8192 !rance 2.00 keV 2.500E+002 ml 12/4/02 5:22:00 12/4/02 5:22:41 12/4/02 5:22:00 L. Finn PM PM PM 600.0 seconds 600.1 seconds 0.01 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By W. SuperisoryRevie Date//,. Date /.Z/' O/OZ. Supervisory Review Date / / _Z /0a5

Peak Locate Analysis Report 12/4/02 5:36:44 PM Page 2 No peak locate results available for reporting purposes P E A K A N A L Y S I S R E P O R T Detector Sample I.D. C:\\GENI] Spectrum Number Sample Description Peak Analysis Performed on Peak Analysis From Channel Peak Analysis To Channel DET01 E2K\\CAMFILES\\BKG120402.CNF BKG120402.CNF Bkg Check 12/4/02 100 8192 5:36:44 PM Peak ROI ROI Peak No. start end centroid Energy Net Peak Net Area (keV) Area Uncert. Continuum Counts One M = m = F = or more peaks were dropped due to multiplet de-convolution. First peak in a multiplet region Other peak in a multiplet region Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/4/02 5:36:44 PM Page 3 N U C L I D E I D E N T I F I C A T I O N R E P O R T i** Sample I.D. Nuclide Library Used C:\\GENIE2K\\CAMFILES\\BKG120402.CNF C:\\GENIE2K\\CAMFILES\\MYAP.NLB IDENTIFIED NUCLIDES Nuclide Id Name Confidence Energy (keV) Yield (%) Activity XuCi/ml ) Activity Uncertainty

  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 2.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

C Jnterference Corrected Activity Report 12/4/02 5:36:44 PM Page 4 I N T E R F E R E N C E C O R R E C T E D R E P O R T

  • i******

Sample I. D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\BKG120402.CNF BKG120402.CNF d2. AQ Date Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ml ) Wt mean Wt mean Activity Activity Uncertainty % Uncertainty ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma No peak search results available for nuclide analysis.

G A M M A S P E C T R U M A N A L Y S I S Report Generated On Detector Sample I.D. Spectrum Number Sample Description Sample Type Sample Geometry Peak Locate Threshold Peak Locate Range (in char Peak Area Range (in-channe Identification Energy Tole Sample Size Sample Collection Date Spectrum Collection Date Decay Corrected To Collected By Live Time Real Time (,.% Dead Time v Background Type 11/25/02 7:47:46 AM DET01 C:\\GENIE2K\\CAMFILES\\BKG112402.CNF BKG112402.CNF Weekly BKG Check Water 2 3.50 inels) 100 - 8192 .ls) 100 - 8192 xrance 1.00 keV 2.500E+002 ml 11/24/02 3:14:00 PM 11/24/02 3:14:29 PM 11/24/02 3:14:00 PM L. Finn 3600.0 seconds 3600.3 seconds 0.01 % STEP Energy Calibration Performed On Efficiency Calibration Performed On Calibration Geometry Used 11/13/02 11/13/02 2 Performed & Reviewed By Date J/A/ a25 /02 Supervisory Review _, o-?t2als Date -AR / 3Y / )Ad

Peak Locate Analysis Report 11/25/02 7:47:46 AM Page 2 P E A K L O C A T E R E P O R T Detector Sample I.D. C: Spectrum Number Sample Description Sample Type Peak Locate Performed on Peak Locate From Channel Peak Locate To Channel Peak Search Sensitivity MDA Confidence DETOI \\GENIE2K\\CAMFILES\\BKG112402.CNF BKG112402.CNF Weekly BKG Check Water 11/25/02 7:47:45 AM 100 8192 3.50 5.00 Peak Centroid No. Channel Centroid Uncertainty Energy Peak (keV) Significance FWHM (keV) 1 741.61 2 4693.58 3 5844.44

0. 2 638
0. 2048
0. 1805 185.61 1173.14 1460.82 3.83 3.95 3.76 1.1612
1. 4729
3. 0036 Errors quoted at
1. 96 sigma

Peak Analysis Report 11/25/02 7:47:46 AM Page 3 P E A K A N A L Y S I S R E P O R T / * * *** Detector DET01 Sample I.D. C:\\GENIE2K\\CAMFILES\\BKG112402.CNF Spectrum Number BKG112402.CNF Sample Description Weekly BKG Check Peak Analysis Performed on 11/25/02 7:47:45 AM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 734-F 2 4686-F 3 5837-749 4701 5852 741.52 4693.53 5844.79 185.61 1173.14 1460.82 5.95E+001 2.91E+001

5. 18E+001 18.59 11.33 16.85
6. 52E+001

-3. 99E+000

7. 70E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/25/02 7:47:46 AM Page 4 1*********

  • N U C L I D E I D E N T I F I C A T I O N R EPORT Sample I.D.

C:\\GENIE2K\\CAMFILES\\BKG112402.CNF Nuclide Library Used C:\\GENIE2K\\CAMFILES\\MYAP.NLB IDENTIFIED NUCLIDES Nuclide Id Name Confidence Energy (keV) Yield Activity (%) (uCi/ml ) K-40 CO-60 RA-226 U-235 1.000 1460.81* 0.221 1173.22* 1332.49 0.944 186.21* 0.684 89.95 143.76 185.71* 10.67 100.00 100.00 3.28 2.70 10.50 54.00 1.449E-006 7.265E-008

1. 158E-006 7.033E-008 Activity Uncertainty 4.800E-007 2.853E-008 3.693E-007 2.240E-008
  • = Energy line found in the spectrum.

@ = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/25/02 7:47:46 AM Page 5 I N T E R F E R E N C E C O R R E C T E D R E P O R T SapeID Sample I. D. Spectrum Number Performed & Reviewed By C:\\GENIE2K\\CAMFILES\\BKG112402.CNF BKG112402.CNF I' 11

  • L, Date 1/ / I 5/a 2, Nuclide Name Nuclide Id Confidence Wt mean Activity (uCi/ml

) Wt mean Activity Uncertainty Wt mean Activity % Uncertainty K-40 CO-60 ? RA-226 ? U-235 1.000 0.221 .0.944 0.684 1.45E-006 7.26E-008 1.16E-006

7. 03E-008 4.80E-007 2.85E-008 3.69E-007 2.24E-008-33.1 39.3 31.9 31.8

? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.96 sigma U N I D E N T I F I E-D P E A K S Peak Energy No. (keV) Peak Size in Counts per Second Peak CPS % Uncertainty All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

YS CALUBM( N AND TEST REQUIREMENT FOR RADIATION PROTECTION INSTRUMlTATION ( RE( =AIT-104 REVISION 0 ATTACHMENT 6.4 INITIAL REFERENCE RESPONSE TEST FORM (example) InstrumentModelNumber: 42D7 ( ,m2v)(Instrument ID I12 Scale or Reference +/-20% Value of Jig and Source Decade

Reading [

Reference Reading ID Number Geometry Remarks l LX'..

1.

./~AsiJ (E J'/o 7 - 6-_ lPerformCA by:Date 'A/;,{?2n I-Z7-01 Reviewed by/Date_ ~ /iQ a v 3 cA 4 REDSPROCWM1NS .: 0' 1 of 1 of I

CALIBRATION AND TEST REQUIREMENTS FOR RADIATION PROTECTION INSTRUMENTATION REDS-INST-104 REVISION 0 ATTACHMENT 6.3 RESPONSE TEST FORM (example) Instrument Instrument ID Pass Fail Performed by Date _ _ _7_ EA /4 / I i/a/c Reviewed by Date / REDSUPROCUINSTU04 1 of 1 .~.. ~.

c§ 1/2.TION OF THIE LUDLUM MODEL 2350 SERIES DATA LOGGERS C REDS-I(- -201 REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FORM SECTION 1 (To be completed at Initial Receint Resnonse Test) Technician Sirmnanimre Av nate: og INSRUMENT & DETEOR TON DR TO ANCE VALUEs - SOURCEN hnstnnent Model No. 3 _ q Cal Due Date Minus 10% Pls 10% Net EFF SEG MI Serial No.

7 g

~//qbs 1 Instument Serial No. CLZI6 4rG-B /o 7/ / 3o7 I 37 Cticdon Date Detector Model No. z3 -6 Cal Due Dat prrAting CodidotL: Nuclide t ,Normal I0 Abnonnral Altitude fl. Detecaor~ aNo. i3 Cablee Leng ft. 0 Teerature_ OF Avity i dpm SECTION 1 Reviewed By: Date: I 4az/C>3 SECTION 2 (To be completed by RP Teciiian) t beginning, verify the Intrument SNs listed above. IF the informaton above Is incorret DO NOT CONTINUE. I I Source Count Data T Test Type B round Denat r CountI l Count2 l Count3 Mean Toleanee Efficiency Perfo byedb L ( = e (SCRt3) Net Sidl Cf Gros BKO Gros Net [Gross INet IGross Net ContEF Technician IDate/ Unst Ui ca n i CPM l Cnts CPM CnsCPM R!te P P. ai Tile _)_ l, 1 n //fo l l 0 7 ll Time pnl /53 _W 1W 5o1< 2 sFl 4s_ l1 le3

  1. 6 / 1 7 73 9 lsa UAR
119, Reg1 /27-21lg22 l

lA Ql If /2f5~oI ILI~ i'3o ;'4 Ws9 d,,,s 1 -S }I I / I/7 t ,5 1(3 I A u71 t1 71 7 '3/ B.M ALlJCL(ZL. I 141I 1J E2kL e1.. By inP7O. 1 1iho innh 'x' hisOrm7 ,en1v7 ve cek ad e

  • 01, i

/tff-1 1-3 l I / rjk/0 M,1;I / /3fI. 1 6403 1*41.1,54I'tlf.7I 1'tf175Y l.;3 25ZP3 /1-3 PEMARK: WIT 1 B WQpa sramteters le ceked mad are verified to be correct SECTION 2 Reviewed y: -Date: / 0270-3 PAQVfr~eu

  1. riPQVM4MVV,1ll 4 IlMn

[ O7N OF THE LUDLUM MODEL _ - 23 SERIES DATA LOGGERS C. REDS-INr REVI SN-1 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SlCIION 2 Cro be cond by RP TechnMkn) l1m steMOded 735;-/ tl Se al /5 l Cal DueDate t -03 Detector Model IV-/oLZ Detector Serial I ifs l Source Seriai / i .j SourceCumvtDat-5%. 14.9 5ogC. 13-. TyeAaltrrm Dt -IPerformed by Test Test Type agrod Da2 Tolerance b .est

== I I, A I l M See Now no LS1w L" N KG Th" GM Na G im Nd iGrn R d t Err s IT IpcID I I 31 A n IpSUFS1[____ = CasO 051 OII3 T.mClM3 7 o

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, 1 / - 261/1 17 1.2 R EMARIkS: NOTE 1. By WU91W dMh Neck. d dvig e c hdI Immn s bees deed ad as varihd be o-s. SECTION 2 Reviwed% By: Date: /.i 71.) P.\\SI1B5201_4.R3UNbTdN5214.WPD 9 of 11

ofi'XION OF THE LUDLUM MODEL 23 -SERIES DATA LOGGERS ( REDS-1? ' I R.VTfON 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM

  • .1 4

SECTON 2 Cro be bM I RP Tedmidan) instmmentModel V35-I instrumsertialI //75Z6 CalDueDate 4- -03 DfteczorModel# 1/2/-0oZI DetectorSeral £ sourceseriall l _rm,_ Source Count_ So rce C tData r by Alarm' Tes pe Background Data -htsC,, Source C Dolerance Seeo Note b -ll) Ii GjGi = T

K

) Gma No., Eff T. l i f"'_ e P ITIMM" CM CM m Ct a Tim = __== = =2 7. _57.... )- 11 IT l I)0 11 ( I_ .7 11_I_1_= I 1 7 W. vz5i 7 P03 /IP-) PO- /,23I REMARKS: N(YFU 1. B xft W1Middngddgbo

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WAs leueutldlusd¶pIIUIpuy NM bee. W NMeke amidu endiW,;d/m c SECTION 2 Datete: / P.%SIraRBDSwRlOC~lrf~nvrt3zul-4.WPD 9of 11

( RATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS C : RE(-1INST-201 REVISION 4 COUNT RATE D=MCTOR RESPONSE TEST FORM SECION 1 Mo be comileted at Initial Receint Response Test) Technician Sianature: T.

c. t. A Date: 121t(8(

INSTRUIMET & DETECTOR INFORMATION DETECOR TOLERANCE VALUES H EFF SOURCE INFORMATION Instruent Model No. Cal Due Date Minus 10% Plus 10% Net EFF SEG ID I Serial No. Instrumqn" Serfsl No. 9o3 q ig-Al-03 HWI Certification ate 8 q el5 Detecto Model No. LCal Due Date Operating Conditiod: Nuclide -qq t./ o a Normal a Abnormnal a Altitde - ft. Detector Seril No. L&l U WtableLensth 5 ft. O Tcp re r0

  • Activity in dpm SECTION 1 Reviewed By:

Date:_ -72/ph SECTION 2 go be c Rmpleted by RP Teduhician) Prior to1 gInning, verify the Instrunmient SNs listed above. fF the information above i incorrect, DO NOT CONTINUB. Source Count Data Mlaria Testfaype by Test Test ype Background Dat Count I cCwnt 2 Count 3 Mean Tolerane E1dency Performed by I ($_l) I ( (sCan Net Sat/ p P Tm lrosG lKO Gross Net Gross Net Gross CuRat EFF Techian Date/ Time 1 CKG Cmt CPM Cots CPm Cot CF ?tm rme nIdo h Unod(un) Counts MNSRat Pas Pll'aFlod&MI ) Tm -l / i 1£37 SID 63(p (B 1I _W r_ t)bic 3 i 3_ o I, ,-o 17 615 57(4k' Iq-4 555 1 t1 9' ).Ab'(!4 -1 I 1 -1 -11 REMARK: NOTI

1. Byinitialingthiblock, the Instrutnent paramtrs a be checked and are verified to be correct.

SECTON 2 Reviewed ]BY,: V 0T& Dat e:/ Ip&42A P:\\SITli . AOCS\\INSWNS201 4.WPD P.. N-

OPERATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS C C REDS-TNST-201 REVISION 4 GAMMA DETECTOR RESPONSE TEST FORM SECTION 1 (To be comnleted at Initial Receipt Response Test) Technician Signature: AC. .W Date: /-Z -e2 INSTRUAME &DETECTOR ACCEPTABLE INSFRUJMENT RESPONSE RANGES SOURCEINO ATN INFORMATION Goer iu 09'~tCut ls2 NtCut E / o ImnsumentModel 2350-1 C DuO Deft S 1

3 j 3 5f4 497, 03 0 J-1-at Number

_ _ _ _ _ It -7 Jr h m i 5 4, 2 Z. 3 I Peaosiio 2 N ujcllde Serial Nutn er I I _ 3iJ 1 '1 A__ `__ CS -/13 7 Detector Model J Id EI 5,90' N um ber j @ 8lnclte 4d 3A c t ty n Detector Serial j9IUormal 0 Abnormal: a Altitude ft. Number I 0

4.

3 p d~ 'ut 0 Cable Length ft. a Temerawr 70 ep SECTION I Reviewed By:_ 0! ~ Date: 4LaZTe2. SECTION 2 (To be completed by RP Tec~hnician). Prior to beginning, verify the fnstr~ment SNs listed above. IF the above Information Is Incorret, DO NOT CON__II ACTUAL INSTRUMENT RESPONSE L Test Tie Gos RG0 Contact @ 6 Inches a la inches SceeNote I BetTyeKG C Oro" it 'N et G os iti N e 2 O~In3Pass Fanl Pech iby r 1m (i)counts CPM Counts CPM Counts CPM re&Judh SAl j 554S3 i',026 #A5A74,4jqa 51 47,714 /J4d/2 Y3L 2 ke

  • Iiv/&V 4

n2 ir -t 9 1 1ag .7 to 0 5344Ullo30q,'U T7VW _____30 7M9?40 lr" l 14V ? 9#N _____r~ t1363 le/8 I3 -F-N .. NOTE 1: By InItiaing fthi block. fth tecn canpdO$ that ibe Instrauent parameters have been cbiecked and ri Verfed to be correct. SECTION 2 Reviewed By: V pafC Date .J/p I W P:SflESREDSPROSUNS1MNS2O1.A.WPD 4 of 5  p:%SrJ?_3UW$VR0(;MS7WS201 4.WPD 4 of 5

OATION OF THE LUDLUM MODEL 2fv SERIES DATA LOGGERS C REDS-( '1 REVISION 4 GAMMA DETECTOR RESPONSE TEST CONTINUATION FORM SECTION 2 (To be completed by RP Technician). lsu = t mentSermdlul _4 ICal DeDatez t Le Detector Model d -10 Detector Serial I 16.t -I 6 Source Serial I o 4 l 1 Source Count Data TesrtI J* Bakgoud F o Jac Performed by TTest Test Tp hkpoundData 1-[ Position I Position 2 PosItion 3 [NTolerance oe =a Contact 0 C6nches @18 nhs________ Count' Grosst } eTl =_ Satl Pre Post lTim l KG B'KG l(li) Gross Net Gross Net Gross Net Technicin Date/ TUmat WR)Cont CPM = [Contj Cpm Cots jCPM Cots jCM_ L.O6 L..4ts'4 %i r 'o,- -st-es Lf1 18;tx,' 7.19o -1 __7>- I1. NOTE 1: By fntal"Ing dkl m~ock~ ft he d te wicaIcaftes 9* t instument parameters huve'Peen Oecked andf are verified to be correct. SECTON 2 RevIewed D&se Date: _ l;* i74 tob-417S;6;fi0< 7Zb=S4f B;) 8 hi P'%SlrW 'DWROMINMnwI Ii. W_- 5, - s

XC,4TO OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS ( C' REDS-INST-201 REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FORM SECTION 1 (To be completed at Initial Receipt Response Test) Technician Sianature: j Date: 16-LtS27 INSTRUMNT & DETECTOR INFORMATION DETECTOR TOLERANCE VALUES EF SOURCE IFORMATION I Jnstumme Model No. 2 50 - Cd Due Date MMnus 10% *us 10% Net EFF SEG ID J Serial No. //9G5O4 Instnwnt SeralNo. 53 IZ2. o3 /30. 5 0 0. o.. Cerdficaton Dam 9-96 Deectr Modl No. 43C-/06 Cal Due Date Iang ond"dom: Nuclidb 7e-aNormal O Abnomal a Altitude De___ Serbl No. C33qeg 4/ 03 bo Leno $ ft. a TetW 7^ -P lAcdvkty Indp 50/6 SECTION I Reviewed By: Date: SECTION 2 (ro be lby RP Technician) Prior to beginning. verifyt die Intrument SNs lis above. IF dfe nfonmadon above is Inorrect. DO NOT CONllNUE. SOW"c Count Data Alam -erformed.by Ted Tatpe .BagrNdDta i Cont1 I Count 2 Count 3 lMea Tolerace Elclen e No fle MMSCRt) I S Net I_______.___ Count am" Gross Net Gross Not Count WM -' CPMK L" CM !! !CPM A !ni e TLil to / 1{ 3001. -100 lazt3 24 /5.Ul /RI2;taL 187 /19? l 145 l l l 0 22,0 IAC

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  • Y NOTE: 1. By Initialing fti block. fth tchnic~p Inlaeola h 1MInsrnent parameters hay beep checkedl and are verified to be correct SECTION 2 Reviewed By:

Dat a _ D: / W I z ga 4

Or 'IXON OF THE LUDL1M MODEL 23SE DATA OGG ( REDS-4 RTEVICIS 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SECTION 2 Cr be cedby RP Technian) lmtrmOded 250-InnreSeraldCal Due Date 1-Detecto Modl -/4 DetecSel 39Sre Seia / I = Source Coumt Data A 7S9 Aham Te IY Dackgronnd Data -T = TercePerfomed by Cj a l l Ka b) G mI j Gum No ll NHl Tbeml _ct2p. ~ .=* g Jo l2I 1 6116 113 J4fI 37 1413A 7 1(54 '//S _502 ID/ O 3O2I 3oq 1 j.39 A5 1504 1 142 1501 124: -I 2*7 z -5 02,., .4 z _ }F i;$ /-^ S~kf -VI 10 1805 11.30 1 1395.11 156 &S4149 V 356 - -l1 /I 93 2.34 V W*/- A, /tF W 9tr = 0 2905 Zf ¢ 1 / 5 1107, ~3 II; 716 zo 6 1V 75 1107 24 I 0 __I s 29 4_ .I Il 3/4 54U7 >I 3 40 114.41 I4 .22 / IA.V A l A-r to-92k 9 13-7 fZ '311.34 i4ol iI I 1114 We /a17' SH_ => e1S+_ Z /Wt435t ig73 str.L I 99 s I 1 _I /0 /S LO 5 1 /14 1 ' IZ? .22 / sC I73D3 S 1 l P) 10 i fI g i4o ((7a P43q 117 13-_ 1_ 1___ st I'cl = S25 5 L~ J> Iia .2Z"' _ _______n tI-I 2 19 12 10W /*4S I 11 7 /43 1173 113(, iL 52 I 1+61gg //"i 131 t'), If-3 2 / VI .7 e to .+/-.. 1.22779 fll-1+/-ts-l iiqq 1415~ "HI ' 11 .22! / I .~A*a! - hO ~~ J I~4 O~i ~TOIF -4 4 1411143 .23 SECTION 2 Reviewed BY: k Date: / -+ ,IF C^S. 'g PL'~& ' 4 A0 $I P:\\SITDSREDSPROCS\\NSnWNS201_4.WPD 9 of 11

OP 76:xON OF THELUDLUM MODEL 23L.ES DATA LOGGERS C REDS-IN5 -- ' REsVIRll. 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SECTION2 (robe comby RPTemchn) IntmnienModem i35 - l mmlem Serial 9&3k) CalDueDate 1-2.2 t53 l DewcrModde I3-l DetectorSerid

1 Sa9rce Serdal I/9 50 l

Source Cown Data Perflormedb TAes Test Type Ba-ckgrmd Data t 1 I sPerformed by I __ELI" hf KGc ON cmanaCa"om__ bw Tim __IlIMtI I iia ___1_ __1Mt S~ t

T ielBGlCM G

" to l GlNWl 6a n431 xed cn. l r 2D15 Ii-2. -o -1I ,*S aI /W (O 9-Zf I.?ef, J//+ 142A I7.2.- /0-54. _/, lo

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.a;l -0 1*3-k 3 1 /51_3 0.37 /O-7 J A1 I &A*r t I W 2 I 3 1ALML VQ A?4' P131W13/ 1 fI f ) T39 9v-I __ = 1 45! zkc f t W¶' /3S I5'$)-/93- /03 l /D~r I~iE lt VJ _ r /'/" 5 144t 133 1 o-M Xl /.- -~ tJ 9 4e3 ViS t'

  • 7.7%

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4.

If -- t7'J.4' A/ V __ /0 &7b1 XZ /° f1o (IfL6 f 171{ I?'>l'?f iii pIIo LII. .v__ / (5 AW, t3.A, ,V5 /14'0 ('13 I13e 11i 1 000 t2t o7((t 16l313 ifob lo.< lA~ %o I-%/0;7o7Z7-: t& 3*1fb 3IK W 138 10Vll3 t1116 qg( Jj)-J intfl o IlVllzll v S/ tt _W 117i1 E 1>6HV tf/Mt Ift Isd 10111W ag';5 REMARKS: N vL 1.. ; ,I. NW

1.

2 ddl W*. Ily hWas -ib bb*, ha-s chm dec d fid c v becIDh SECION 2 RevieedB: B-_ Date-. / P:ASfHS\\RHDSTPROCMUNS0UN5O1-4.WPD 9 of 11

{ ,flON OF THE-LUDLUM MODEL 23(u SERIES DATA LOGGERS ( REDS-Rr RE3VIKxoN 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SECI1ON 2 (To be completed by RP Techidian) I WMWWMe odesl3rb. InstmetSeali Cal DMe D Mode

  1. ol6 Detector Serial I Sotrce Sea ba

]

Ips__

_de69 10 seI Marm Test Type natk d Data Ce__t T Performed by .vi = 0 1-Z5t ltm we lI M N IaO aM BKO I[ Goz Rd amn NeI Ga N lEffi I L1 11 I/11 zo Le l cL>3i =*

  • t s

= o6 L°7 1 3 ____c i 11 I3ia311 1 1 H II Iime IG ----I (e 1 1 m 0l to 711 V 541~8-ID4343UV H66110143 of/ o4 S) I/A' .AMc' WN~ Ios 1.3t /11M 1 11e ~ ]1-1/ t1 1 J. & C, 1 1 r1 1 /v OU3O (3t6 oIi66A'3'u (/e) I6 _.L J. 1-111 171 RME: 1.o 3Lg i r 3 d/h 8bAd di g1l dc( n3 h -u A I A. SECTION 2 Reviewed By: G J Date: p7.. -* 7.,- 5E 9 of 11

PERATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS ( I REC INST-201 REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FOR1I SECTION 1 (To be completed at Initial Receipt Response Test) Technician Signature: Date:?4-?-I -f _ ? INSIURMll & DETECTOR INFORMATION l DETECTOR TOLERANCE VALUES l EFF - SOURCE INFORMATION l Intnunen tModel No. 230 -I I CaI Due Date Minus 10% pIus 10% Net EFF SEGIDM/SerialNo. Imbm1 Serial No. q 5 34 0 0.3 8 72*5 G Certification Date - 9!k Detector Mode No. 43-106B Cal Due Date ringConditions: Nuclide rI dNomal O Abnormal O Alititude _fR. Detector Serial No. 3 9-3 oCable Length ft. a TempenwiUrF*PF Activity in dpm SECTION 1 Reviewed By: 4 Date: O 3 SECTION 2 (To be complete by RP Texhnicbn) Prloft beginning, verify the Insftnment SNs listed above. IF de infration above is Incorrect, DO NOT CONTINUE. Soure Count Data Alar TestTpe Dacground Data ylt3 Tolerance Emdicyl Perfoned by Tast Countp 1ckrondDg Count 2 Count 3 Me oevne EdqSe Naft I (gm R 1 mm S R2 Net.l Sat ar m l l l Gross l Net Gross Net Gross Net Count EFF Technician Date/ prsPs Tia) Cut BK'Gsi io Rate pass palln(Name^ riet Time CPM Cm CPM Chts CPM Cnts CPM (mom ?thd__ ___i_ Tie_ 9/ 1 'o4 - 9Y4 q3. OOS. 'o, /O p fowe4s, 1,L I11 1 1 11 it 13 91 1 11 I / /0O 11A t I 1 1f 1-1 1 1 11-1 Ir. M. I I l15

t.

l e M ThiIWU. 1 uv a.Inbiu.. del. 1.1.4. tdnieidih....a7.In i_ Dllt~e Imfm it flrmtIvS e imen eheckrnd and ue verifked tO be correct. w{, 10 2 SECTION 2 Reifewed By: ! Date p.sfm ..AOMSINSTIMNS201l4.WPD z

C> OPERATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS ( REDS-INST-201 REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FORM R1ITCTYA 1 CMn ha-t.mnleted at Initial Receint, Resnonse Test) Technician Simfature: AO-,. ztx~ flute: [INSTRUMENT & DE1TCTOR INFRMATION~i DETECTOR TOLERANCE VALUES EI SOURCE INORMATION Insrment Model No. 2 CaM Duo Date Miu~s 10% FPns 10% Ne l SRO MDI Serial No. AS 3, Insumnem SerilaNo. q~IO iZ-3 .1.54/.5CffdftdonDate Detector MdlNo.

  1. &3-/O6A Cal Du Date operating Condiio:

aucAbde -ns3 0 Normal 13 AbNucliae 7ft-230 Deteto Serial No. 13 9S',? 0 abe4enth tL0 emertue PActivity i p ~~g SECTION 1 Reviewed BY: ~ 2 ~Date: 4 SECTION 2 (ro be cpetdby RIP Tech*ncin) Prior t befinning. verfy fth Jnstnnnen Sift listed abov'e. WIphinformation above Is incorrect DO NOT CONTINUE. 1 ~Sourm Count Data Td Tast Type Racliground Data I Cu Cont 3 mean Tolerance Effcenc Peftotme by ra=m =~ tSC3M Net Salt/ 1 n aross DKO Gross Net Gross Net Gross Net Cut EFF Techicican Dtel UnTntutKG CPm Cots CPm Cuts CPm Cots CPm Rt asFi nst("de) Count -tr1 (0 '.( 39]S,?ta.L -4J -q 31 -- I A- -Z 3f34s 3~ 1ft 3?3q q*x 3b SI V. 1 jcta -11't-15-? -o% (#.9 REMARKS: I w .44-I NOTE: 1. By 'idet aIng tOM block, Ith tecmid Mdpq mh~~oIsinun parmmetermbaveftcnecwed anm are veriwe to be correct. SECTION 2 -l!/.IReviewed B: t =1'- Date: ZO3 /IN f. f

O),.IION OF T-LUDLUM MOD DELL4 231- -AUES DATA LOGGERS, REDS-INU N REVI&- Aq 4 j. COU RAt DETECTOR RESPONSE TEST CONTINUATION FORM 4 4 .9 Cro be cme by RPTeCn) [in Mode l 2M-60 j imst sen Sexig a 4 Cal Due Date I22-l Detector Modde Detecor SerialfJ t3 Souce Serialt '9,CJ4S1 Sonrc e Co Cmt Data S Tear Test B Da i = od Data D Tolerance PeKfore by I Cod wI 0 M l I I I l 11_) II I i sm On d, IM l tl MaIbe Rn1ii sNk ldet =11. _ !.......=M E ffi IWCm VKG (e. Gme. Notedi"aHaci.,sf -k -° -7 3.1 39' X 3oqo q3( 3B'73 _1 41 _1 3a 11 3" 3.3 1 %3b3/3'?'"I 3u 1(23) _1 Au.Aq{L -F3-oL ___lMS lisl~~l4w3l ___tlsgS -~ili -l ___c~kd -i ___1 I0r V 30 3 /

39o, ir3' 7

qs,3qd z 317 3 11 -6 J 39t{- q 7/ RY T 11 1iI A__ /0 40 (0~-V 0fa 1 Mh 1. 11 1 k M I d1 n a 1 \\ms hIbee.hdcked mamvalflevbqeo SECTION 2 Reviewed B:, Date:./4/D P:5ITU3UWD3U'iOUIZUrIWJ q.wrD 9 of 11

0 mTION. OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS ( REDSION41 REVISION 4 GAS FLOW PIPE DETECTOR RESPONSE FORM SECTION 1 cIo be completed at Initial Receipt Response Test) Technician Sianature: Date: DETECTOR INFORMATION DETECTOR TOLERANCE VALUES EFF SOURCE INFORMATION Deteor Model No. 1 d3 10% Plus 10% Net EF SEG inDISera No. (/ 29( 1 } DetectorSabiaNo. -erfL3t;ti / l A ii,- IlflcnDate Cal Due Date Z4 ?A Nudide 7!-2 Operatng Coions: 0 Normal o Abnormal a Altitude ft Acinvy dpm(S1 m (7106 O Cable LEn". ft in Temperanue

  • P

__I_.__ SECTION 1 Reviewed By: (2 Date: Z, SECTION 2 a be iw d by RP1 Todm) Puorm wemhg. wdf~ nt sme N. asemhw.. IF do hdimd" Abm I i Do oNcoM 0ritB Instrument Information ATet Test Type Dackground Data Source Count Tolerance Eff l onned By Test__ _Date See__ NOW_ I Count Gross BK Technician SerialNotl/Du Pre Post Time lBKG l CPM Goss l Pass Fail (NamePrinte & Date I 1 1...... 1 = 1 1=.. 1n ) Counts -3 ~ i ~ 1 1 1 I '1 Remars:

All, Note: 1. By initialing his block, the lec l

dih es dyBe instrunent parameters have been checkd antreverified to be correct. SEMCION 2 Reviewed By: M WVcs f f Date: 4 I

O'LATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS ( REDS-UC -201 REVISION 4 n

i GAS FLOW PIPE DETECTOR RESPONSE FORM (To bw cofmpleted at Initial Receint Res~onse Tesvt)

Teclmhnician Siematuirp SP!CTION 1 no,. J-..- Z- ; r-r -fi----r--, X-z I DEWECTOR INFORMAI¶ON DE ECTOR TOLERANCE VALUES 1FF SOURCE INFORMATION Detecr_ Model No. Ms 10% Plus 10% Net E P sG ID/Serial No. Dextcor Serial No.

rl/

I I l Certfication Date mi-d95 Cal Due Date I 4-/p - II I ' 39 G Nudide OperaftiConis: )4oml . a Abnorml a Alitude ft Acdvity ind pm (S6 o CableLengt ft n a Temperatire OF 977 SECTION 1 Reviewed By: Date: SECTION 2 -te b tPT ) Pyoi bel f, As h hted Ibd nPtio b I, DO HOTNCONNINMl intuetifrain Alarm Source Count Terne EfPerformed B lTIrstruatt on Test Test Type B~ackground Data Data Tolerance EfF Se Nrot~ed By Con Grs - T c ia M2350 Sati G l GIsN etl l Technician l pre Post Time 1KG CPM GoN s 1 -1 .1 hinted1 Serial NoJ~ad Due Unsat j(a)CIf Counlts CPM Ps Fal(uPntd& Time 4~ ~ = = =.,. =1 =11 1 1 1 1 1 1w 9?534 Z-j&W-e9 _jd / /lo' /c 0o ~ J-~' ."O/ W'Al-ylrw Remarks: Note: 1. By initiaIg this blocki c the technlcj A d# nstnnnent parameters have been checkyd anr verified to be correct. SECTION 2 Reviewed By: C_ Date: y42q I.- r ( ' "I --

OPERATION OF DENVER INSTRUMENT MODEL XE 3000 ANALYTICAL BALANCE REDS-CEM-216 REVISION 0 AITACIMENT 6.2 EXAMLE DENVER INSTRUMENT MODEL XE 3000 RANGE CHECK Model XE3000 S/N 3O9 Cal Due Date:3 Weight Acceptance Range Reading (grams) lg 0.9-1.1 2g 1.9-2.1 5g 4.9-5.1 10 g 9.9 - 10.1 20g 19.9 -20.1 50 g 49.9 - 50.1 /w- _ 100g 99.9-100.1 J00-O 200 g 199.9 - 200.1 500 g 499.7 - 500.3 __50____ I-kg 999.5-1000.5 ,ooo. 1.5 kg 1499.2 - 1500.8 150o. 4 2 kg 1999.0 - 2001.0 _____J.__ 2.5 kg 2498.7 - 2501.3 i J,1 3 kg 2998.5 - 3001.5 3COO/. 1 Wdght iSN, calibration date, and calibrat/on due date: cda6 x9, O/CR/oL, /O/o?/O3 erformed By: c. Date: IJ14e 02I RE~wO~~~rcH-21.O 1of. REDSMPOCSTIOCIIKWI-2 16.0 1 of 1

OPERATION OF DENVER INSTRUMENT MODEL XE 3000 ANALYTICAL BALANCE REDS-CEM-216 REVISION 0 ATTACHMENT 6.2 EXAMPLE DENVER INSTRUMENT MODEL XE 3000 RANGE CHIECK Model XE3000 SIN 3Cal 7 Due Date: //o/0-3 Weight Acceptance Range Reading (grams) I g 0.9 -1.1__ 2g 1.9-2.1 / 5g 4.9-5.1 10 g 9.9 - 10.1 20g 19.9-20.1 50 g 49.9 - 50.1 100 g 99.9 - 100.1 ,30.C) 200 g 199.9 - 200.1 __t 500 g 499.7 - 500.3 SO __3 1 kg 999.5 - 1000.5 Ii).5 1.5 kg 1499.2-1500.8 i50O° 2 kg 1999.0 - 2001.0 lOO(. O 2.5 kg 2498.7 - 2501.3 )fYO* 3 3 kg 2998.5 - 3001.5 Weigt Set SN, calibration date, and cal,09at~in due date: erformed By: a Date: ,- c \\-Iar-y- 04 .\\,Jj - fafq-0i oor-s +0 1 +o . L;,,, A e-A -u s e- -3 Y,3 0 ,,4 'sc <?E-m:.I RED6'flOcXOIMOiM-216.O 1 of 1 REMSPROCSTIWHM-216.0 1 of 1

OPERATON OF DENVER INSTRUMENT MODEL XE 3000 ANALYWICAL BALANCE REDS-CEM-216 REVISION 0 ATTACHMIENT 6.1 EXAMPLE DENVER INSTRUMENT BALANCE WEIGHING LOG Date/Time Sample Number/Description l Weight Tech o, J.

k /

J,050 'roo 0 4'-rxoa,r &PL. fSo 7 c5f 3 7a a/o ya SI-. 5"'* 3 4__ J ./4 - J 149 o lee. °; /o o AO___a __,Zr &t/4 /o./ tW .5oeo. S a-rs/n oe~ 1164 jrelo v 4 Sao J 4 0 o ~~ r__ 6<

  • S7-t /I2 do
^

4 REDSTPROMCtaM\\CZM216.0 1 of 1

Tennelec Sample Log Omaha VA Smear Analysis Date/Time Sample ID Quantity Batch Key Analyzed Counted by /2/V Z. lo-k dAoo I) a 1 bt I 0 h 7 / l 2 Z/3/ z /,O r A§Od i o 3w OA ? X Y 7. X It/3,ZzZlK2. A6001/ o w; NO 3 /0 6zL L2/&2 V /LI )d0' 03 Wthq 6 .. L2 l ziAzs z AIioo/ 6 Aib3 I L 2 6 ii§ .311 AO39 A66/ O3 k6/ fl3 Y7k

1. 33r YAIdI oI Fol I O

6b Y65 9 ,,YT,&r 2 1 , dO3 02 WI / 7 7 Y 2 /z o /Ya 43 02 w&voz /Z/,. /Z3 l966i3 OZ WO'/ Y 9 02a3vc .o' 1 l3 oZ Sj l f 6so0 1j/Y9 44m oo I oo I q ISo I L/4! /4L o S1odO3 O/ wLF A'i3S 17zu f 0 0, 1 Mi) q__ 4,,da3 6? PhFa3 6J l/ r .A/ opihlh 01?1 4o1B006/ 61 FIl Ot _ Ur.Z3 z 2/x /.700 onnol A 01 0l 26/ 6 Ato2/6 1Z

  • 06010O W/

vI LSJ6 t4A2A /PL 66oo/ 0/ &o3 / 6J1 /rl sr4 ZAJ3 Ad0 pd 0/ 142.10 /0 _v_ A/A.o2L oaoo1^o/ SiOS _r AXJ-T Y/ 3 o60 / I dF I /3 Pj3.7 4£ 2e 05J 3 ,4OQp/ WO a -6S II'YA 141 Da46/ O. fOZ /0 AY4W v 12 g D <nciO/ d 52OOS9 0zya / At/ 0/3 S3 2 -Y 2 J? Weo o la I30 Fs37 oz/o, oz3V P04 0 / /do 6 J3'

Tennelec Sample Log Omaha VA Smear Analysis Date/Time Sample ID Quantity Batch Key Analyzed Counted by 12/Y1O 3 zooO / p e i C / AXY/ /13Y/ ZOOD / 0-a W11I Z2 2 Y~S / HZ/ZI /,rJ /t oQ0 7-0 FOX 9/ X-rYP__ 12;1__L _6__AA_ 2 0 Z. 4- ,2 Ale Z04oq 01 wo3 sA L/ d Z!:2 tV A 22 4ILI/ F 4pnp A Z a So6 Z (6 rr3x v Lf1i Z e avj6 Faq o51 1.3 AS-I ,,A OZW 07 iZ. 4 4 ioO2C/ SJoZ 2 - ___7 4Zi1Z o OiIAZO SR. ___3___ h 44L4Z

4.

O ! 02 -C-Ar2k ~,1 o 2-3444ot /'444d 180 yl ( '2 i(f zz400~ (J v( Ar y J02 l1 -2: L.F )k4S 14ev Y o2-SQ O 6s Da 217/ t/Ooy 0/ fOl/ i4. 7_ D_ Att pnoY Ol WI tj __W 24 46 pp4 O wo2 / IL. £IY/ /3Ia 1nY Y/ w03 6

  • 1-i 5fi ooZoOzI-So 7 403/ I 1 t R?2f~1-wf2t

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  • /¢ oy3 4oi~r oi/

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Tennelec (15632) Control Chart ' Th-230 SN 119739 32.00 31.00 _ ti1111 II 7 i i I I I . -t E In EO3 t 4 rtP r tp qb p 131I I I Fl 1111 11111l 1111 I- ..-t I, 0- .0 0 ci a) ) 29.00 28.00 27.00 t I j ..I, I il l II I t* I T I , I 14 I I3I II -I 1-II IIIT 7

+

0 01i10 f lW -t. i' Ui-{ { Il iI

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i i i !I I I I ,i ilt I [ I Ir I U-1 lij I cI-4 r I Ihi 4 I.- I I I -* -t-- ' -W-io ' I-41 --- l 1I-411 Lower control = 27.39% Lower wamkig= 28.11% ---0-*- Mean = 29.54% Upper waning = 30.97 n-3 Upper Control = 31.69% F T I I V11. T 'r T V I i; i !j + I. 4 I I. 1-0' 4

  • A. v 01/04 01/04 A

L I i 01/26 ,P I 01/07 01/10 01/13 01/16 01/19 01/22 1 01/28013 January 2003 ) ) ),

Tennelec (15632) Control Chart Th-230 SN 119739 32.00 I i i I G'O3TT c-i 3 V ~. I l} w T I I I I I I It4 3 go 3 0 C.) CD ._) 31.00 - 30.00 - 29.00 9R nn Fl I , i i F, 1 I" P @, I i w ' I-I A Fl71 1 I-111-w W- -W'- I I-1 1- _l I_ t 1 J a-1-r."iAR I3-1 I---! ',i ,I I D I I Pr4 11 -I }-{t{"4>{ tfitl II)

  • A>-fl4 -41 I-F 4

T L"- I, III i Fly 4 !~ -4I 4 f-A I-- I I-I 1-4: 4 Lower control = 27.39% Lowerwarning 2a11% -C-- Mean = 29.54% Upper warning = 30.97 Upper Control = 31.69% ISI.. ov vv !T T T II

I T-I!I1 vT r
1 t f -tf

'A A 27.00; 12/01 i. - I II!

  • II 12/Ot
  • -1.-^ II I +

! lI 12/10 12/13 12/16 12/19 12/22 December 2002 I ! 12/25 t A 12/04 12/28 12)31 ) ) )

Tennelec (15632) Control Chart I Tc-99 SN 119715 31.00 30.50 -- >, 30.00 - 0 ci) C 29.50 - 29.00 28.50 I I I.- I CP a-, co I 7 I I I i i i 1-1 I v T-T- I I 7-I I I 1 II I i I-1-1 1-- )- -- 4 I-A I ifj III f II I l1 I I-I 0 I I -I 1, 1,+~i I If Eli C P f;iiJ -4 i i PJ icW;4;J4 it C F I 3 a - T-t -, - t -+--t-+-+--- -+- I IH ,X, -{j ib-tu -1i I Ir--* -- tFt y I ,i. I ! I I i + 'I I Il i II

  • I IIi 1

,, I 42 I I--( i I-- '--9 I--l-14W t*---{IJ3{J III M*-A A-Lower conrol = 2879% Lower warning= 29.14% Mean = 29.85% Upper wafling = 30.56% -U rn 3. Upper ConW = 30.91% I-W v W* V - I . t A  - A 1-I2/10 4 4 I I1 /.2,0J 2/01 12/04 12/01 .2/ 12/13 12/16 T 4 !i Ii 12/19 tL A 12/28 A4. 12/22 12/25 12/31 December 2002 ) ) 3

Tennelec (15632) Control Chart, Tc-99 SN 119715 31.00 I.!i . Ii I 41 m W '! 1, I I I I i 1P I IT W i

  • I m I I

t I 30.50 30.00 0 ci

  • 5 29.50 -

29.00 28.50 0 I- 'T I I Ii 7 tv I I iI-1 1 --q - I i i i l I i

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!tl t A-I I i I: I i iI--{I Il iksI I-. m i 4~ I I ,3 CO I il w i I 1 1 I 0 I I I I. I I qlP " i I-I I fP (jl -tP F-t0i-i I III -{ } IlI-I III [-{ I .T T ~A4 /! 1 i. )1/01 r-l, i Iv ! I ! 4 F j T I I Lower control = 2a79% Lower waming= 29.14% -C-Mean = 29.85% Upper warning = 30.56% Upper Conlrold 30.91% , I F AL I! I A, 4 A I 01/28 01/04 01/07 ! I - iI 01/16 i, I 013 01/10 01/13 01/19 01/22 01/25 January 2003 ) )

Packard Tri-Carb 2550 SN 401663 Duratek, Maxey Flats Disposal Site Type of Count TrItrum (3ml 12ml geometry) Source Control SEG # 029709.01 Month of December 2002 5DAY OF] H3 1 H3 B KG 5 NTASFILE NAME COMMENTS IMONTH CPM IEFF ICPM ]IITAL SDATAlx~i= 3 12518.40 0.422 18.85 TP 0.134 4 12646.50 0.427 16.49 TPKS 0.135 6 12457.90 0.420 17.26 KS 0.136 6 12451.70 tl:420 17.01 TP 0.137 7 12541.80 0.423 16.97 KS 0.138 a 12513.4 0.423 16.72 KS 0.139 9 12380.80 0.418 18.16 KS 0.140 10 12398.90 0.419 17.03 KS 0.141 11 12351.50 0.417 17.31 KS 0.142 12 12308.00 0.416 16.08 KS 0.143 13 12316.20 0A16

  • 17.09 KS 0.144 16 12605.20 0.426 17.81 TP 0.145 17 12542.60 0.424 16.65 KS 0.146 18 12591.40 0.426 15.95 KS 0.147 19 12592.00 0.426 16.70 KS 0.148 20 12582.70 0.426 17.1.

KS 0.149 21 12535.40 0.424 15.98 KS 0.15 22 12430.00 0.421 17.07 KS 0.152 23 12427.10 0.421

16.

KS 0.153 27

  • 1235120 A.18 16.66 TPKS 0.154 28 12363.60 0.419 16.76 TP

_0.15 29 12390.20 0.42 16.94 KS 0156 30 12345.50 0.418 16.75 IKS 0.157 Comment.: Reviewed by% 3 I J3 i,. Date-J2a AHK o3-T O X A3 VolSSL8909 Xad ZcC:T Co/LO/lo Zo Z road sILY1A

C ( ( It TRI-CARB 2550 #401663 BACKGROUND 3 ml Water to 12 ml Ultima Gold LLT 26 X :24 0:= 22 ~2 a 20 c -g 18 O,, 16 14 I 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 1E 19 20 21 22 23 24 25 26 27 28 29 30 31 December, 2002 l a-- -3 Sigma (14.63) -2SIgma(16.41) Mean(19.96) +2 Sigma (23.52) +3 Sigma (25.29)

. r ( ( 0.428. 0.426 0.6424 >0,422 0.42 0.418 U*0.416 0.414 0.41 U.1 TRI-CARB 2550 #401663 H3 EFFICIENCY 3 ml Water to 12 ml Ultima Gold LLT q4 1 2 3 4 5 6 7 B 9 1011 12 13 1415 1617 18 19 20 21 December, 2002 2223 24 252627 2829 3031 -3,Slgma (0.412) -2 Sigma (0.415) {-c Mean (0.420) +2 Sigma (0.424) +3 Sigma (0.427) .1

CALIBRATION AND TEST REQUREMENTS FOR RADIATION PROTECTION INSTRUMENTATION REDS-INST-104 REVISION 0 'L Wo ATTACEMENT 6.3 RESPONSE TEST FORM (example) Instrument Instrument 1D Pass Fail Performed by Date (lf 4LJ-)/ J ,3v VI I .4 /-77 /3 T'y i Lz~J ____3/ 1 o Lv~~l cX -b337 §X .7 Lti / l77 c96337T?, zz (/V-7/O7/ (4-Ui7 7 /__ - ,t-7/V L~cY22 I fe; I/ 2a/17S337 .2/i.__ e .- L4 ~- ~i-t Z$-o7 o R /337

4v4, 07 4337 V

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CALIB¶ION AND TEST REQUIRENTS FOR RADIATION PROTECTION INSTRUIMTATION REDS.lI

T-104

' REViSION 0 ATIACHMENT 6.4 INITIAL REFERENCE RESPONSE TEST FORM (example) Instrument Model Number: InA'/9? 'nstrument ID: 54 G Scale or Reference +/-20% Value of Jig and Source Decade Reading Reference Reading. ID Number Geometry Remarks 4&1Ard-7t e 3 o 70cOce AO r9< A 4/ .W I e11-7* l Performed by/Date IReviewed by/Date /7t'oe YYED8%PROCUNS%104.0 J 1 of 1 )

AM Duratek-CALIBRATION CERTIFICATE vtek Instrument Semvices 628 Gallaher Road Kingston, TN 37763 Phone: (865) 376-8337 Fax: (865) 376-8331 v) This Certificate will be accomnanied bv Calibration Charts orRendinq uwhere amlicahle CUSTOMER INFORMATION -- INSTRUMENT INFORMATION Customer Name: Duratek Instrument Services -Manufacturer: U..L = Address: 628 Gallaher Road, Kingston, TN 37763 Model: 177 Serial Number 26337 Contact Name: Thomas Scott Probe: 44-9 Serial Number: 016220 Customer Purchase Work Order Calibration Methoda Order Number. NIA Number. 2002-00893 Electronic and Source INSTRUMENT CAMIBRATION IN-O;MATION Calibration Standard Instrument comments Instrument Value

Response

Range Before After Calibrated in accordance with Calibration Calibration RP-INS-I-235 X 1 100 100 100 Pulser 120935 Cal Due: 03/18103 X 1 250 250 250 D-814:2551 CalDue 09/12/02 X 1 400 400 400 Psychron 7480 CalDue: 05J17/03 X 10 1,000 1,000 1,000 X 10 2,500 2,500 2,500 X10 4,000 4,000 4,000 Temp: 2L4°C X 100 10,000 10,000 10,000 Pressure: 745mmHg X 100 25,000 25,000 25,000 Humidity 56% X 100 40,000 40,000 40,000

Background:

60cpm X 1000 100,000 100,000 100,000 Threshold: 37mV X 1000 250,000 250,000 250,000 HY (As found = 903V) (As left 903) X 1000 400,000 400,000 400,000 BAT: SAT Volum e SAT .-..Et c1l,~ In,~flir .:..Audio SAT Geotropism: SAT X 1 EFF Tc-99#119720 2,562dpm 11.7% FIS Resp: SAT Alarm: SAT X 10 EFF Tc-99#119718 20,S20dpm 11.5% HlV Test: SAT X 100 EFF Tc-99#099606 177,000dpm 11.3% only. Use Xith 44sl probe. AVG EFF N/A N/A 11 5% MN S TA-TE NTOFCR ATON:Rte TX 0 WeC i that the instrumcat listed above was cdibrated and inspectedpriorto shipmeat and that tnut al the Manufaduius published axrating specification We fnthr cmtiy th our Calibration Measurnits are tceableto theNaticnal htibe of Standards and Tedmology. (We are not reiponsible for damage incurred during shipns or use ofthis instrumncrt Instrument CalibratedBy: Reviewed By. ( 6'(477 Date: 7_ -Z, "alibration Date: 07124102 I Calibration Due: OU24103 C aI b r t o u : 0 4 0

a

4o Ch.~ of Custody Record CN° 1379 no"e fmmf 601 SmabaM 11usd O

Mdt% N mm tu48141683 Pbt" e W)48f21 Fax E-EIRLINE X EflVICEU Prfect NamSp VwtO1bO'm / / / / / / / / /0030 send Report To: r Bampler (Pdnt ae): Nam ( / Addrse b f AL Sanrier (PttNt Name): /&gsfr,71 37763 Smmmmeteod: Fe-A -/ Mbmbe 83754 1563t ///5 oe .376-7 LM Rece:tv ektt &J4t, I/ Far. ,_7-6__7 /Special I D so" sample to Sr MCI I I 2h Coners by W / L / / / bI VA1-0.1-01Q7b Il-m (t0o f_ 100 i6wA I-- __ V. I t a I I -Reli~nqmso ImReceived &F. PS~ lavue) Dte; rw Sampl cus-o--- Rsa- (Co"Mpll By Labon"or). CAMQ Level Tuerwrmtid Sample Rewept Refn se y S0aue-reived U~r. (Sigature) ae: ToWa

  1. Contaher Rleceied Level I 0

_tie 0 COC Seas Prese? _Lel N 0 24 Hur 0 WC Sea_ _tact? h.. bSt Leve III 0 1 Weak 0 Re~ C_ aer__s Wtad_? .Oe a = ' Tem_ _tue?

SAMPLE IDENTIFICATION AND CHAIN-OF-CUSTODY REDS-CEM-101 REVISION 2 C.OP.* YA-oo1 ATTACBMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: i/haJ Ce. Al, for: Z)WttiL' (Mo-c -AA) sute Contac Addres: Phone: Sample Sample Collection Collection Remarks Number Location Date Tume 3A5 -xq &OOOC) 1Oq o1i - A5 oo_ WC( lW-(3-oz p)4co i 50 - t[3 Acct 1bi(Ajjc) I I-jj- 02-C JW Co 4-q A ooo 1b1 I1,_j-pz '4e6

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SAMPLE EDENTIFICATION AND CHAIN-OF-CUSTODY REDS-CHM-101 REVISION 2

  • Y160-5 ATTACEMENT 6.1 CHAIN OF CUSTODY RECORD (example)

Collected by: P. oz b'p for:, YA.) SAtC Contad Add: nhone: Sample Sample Collection Collection Remarks Number Location Date TIme ofe ~ 2-- 48 J/ocxI& kiol t/-.lTz c847 1__ 4 1__ REDSPROcSCHM-1OI.2 1 of I REDSPROCSCHM-10t.2 1 of I

SAMPLE [DENTIFICATION AND CHAIN-OF-CUSTODY REDS-CIM-1l1 REVISION 2 C.o,c. 4Y&6 ATTACBMIENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: L. Wt2c IA for: DA.raTe K (OMA h A 7yAJ MSU

Contact:

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  • pa IO -3 I-rA I l-ato -02 09oqB I 0i-4 1

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Per-quis

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SAMPLE IDENTIFICATION AND CHAIN-OF-CUSTODY REDS-CHM-101 REVIION 2 ot.0 t 7'4-6O7 AITACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: /J., '3a/A& for:1 zA) (8gl2. - Y,4 Ste Contac Add: Sample Sample Collection Collection Remarks Number Location Date Tume /^1o Aoo3 t{ 2wI / ij.oZ i i if / /1-17 Aocwc.3 O° JO2. -_2__ Moo__ _1 _J2 02? W40 OZ;G0 /d~o o A2533 eo340 39 l@u 02-lo_ 34-57 Aooo3 oz Fe t //-96 r '02- /1eo._ Aco3og So/ Jl@-o2_/o ___-_7 Aooo3 AL 622 // a2 62- /~,o -REDSXR ~c~M11. I 1 of 1

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SAMPLE IDENTIFCATION AND CHAIN-OF-CUSTODY REDS-CHM-101 REVISION 2 C.e'.C VA--, QO ATTACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: bJa7dd A*A'W for: )c ) C cAc_ Yg sact Coetacu astsJ Adder: ftouc Sample Sample Collection Collection Remarks Number Loction Date Tume /-5os C~p eJ Bak / \\_ a _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _1 ":I Ie.EDsXPRocS'cKM-1o1.2 1 of I REDS~TROCSCHM-101I.2 1 of I

SAMPLE IDENTFCATION AND CHAIN-OF-CUSTODY REDS-CHM-101 REVISION 2 C,eO. C 4 A-YA.15 AITACH}MENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: 2 4, for: a 14 S6te Contaet: Addrus: Phone: Sample Sample Collection Collection Remarks Number Location Date Time Acro'FOIPOI-olpZ 'o-.v-o. CUSTODY LOG Name Date/Time IName Date/T"Ime A~eP by eriquisled by A--pW by., a~db REDSnQcscHM4o1.2 1 of 1 MMM\\POMCSCM 1012 1 of 1

SAMPLE IDENTE[CATION AND CHAIN.OF-CUSTODY RE:DS-CEM-101 REVISION 2 e - 74-,0V ATTACHMENT d.1 CHAIN OF CUSTODY RECORD (example) Collected by: &97 C',,A-for -A o.- 1/4 (&7'iA Sift

Contact:

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  • 6-7 11 CUSTODY LOG____

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SAMPLE IDENTIFICATION AND CHAIN-OF-CUSTODY REDS-CEM-101 REVISION 2 ATTACHM 6.1 CHAIN OF CUSTODY RECORD (example) Collected by:57,t, CA 4-r for: C>?Za )o#. (Zur a Shc Contad I Addrmu: -XQ 61D "JMfieS Phou_ Sample Sample Collection Collection Remarks Number Location Date Time /- 9 Otf~A c /o z-3-o, I5 i "'-/9 3= I /9-1-3 cno2.,i se)4 L32- /500 /S SO I 'A /j REDSPROlCHM-1O1.2 1 of 1 REMSPROMSCHMI-101.2 1 of 1

SAMPLE IDENTIFICATION AND CHAIN-OF-CUSTODY REDS-CHM-101 REVISION 2 C.@. C wY4 - 012, ATTACEMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: y; r _rfor: 6met A4 - )'4 (Z= ) Sdte Contad: hAdd Sample Sample Collection Collection Remarks Number Location Date Time 1 -4 2co / c5/6 / 42 o 2- /6 0 a 4 n' 40/we / 1 1 /10 / O J)e3 J/___ cJeX we 2- ,O ?,W~c 5/ I__I_11 17/7 0e,1c5,53Fe/ __I_ ie z'o z A -0 3 _0_ <1~~~W 2 @M'/ ( REDsPRocsCmL-1o1.2 1 of 1 REDSUROCSCHM-IOI 2 1 of I

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74. (4i-cki I Site Cen tId-Addrs:

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SAMPLE IDENTLFICATION AND CHAIN-OF-CUSTODY REDS-CIM-101 REVISION 2 g.c,-Xq-c142 ATIACBMENT 6.1 CHAIN OF CUSTODY RECORD (example) 0 Collected by:

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  • 3

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