ML061380594

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Alan J. Blotcky Reactor Facility, Omaha Veterans Administration Medical Center, Characterization Qa/Qc Data, Appendix E
ML061380594
Person / Time
Site: 05000131
Issue date: 05/02/2006
From:
US Dept of Veterans Affairs, Medical Ctr, Omaha, NE
To:
NRC/FSME
References
Download: ML061380594 (140)
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{{#Wiki_filter:Alan J. Blotcky Reactor Facility Omaha Veterans Administration Medical Center Omaha, Nebraska Characterization QA/QC Data APPENDIX E

G A M M A S P E C T R U M A N A L Y S I S Report Generated On 11/17/02 5:58:08 PM Detector DET01 Sample I.D. C:\GEINIE2K\CAMFILES\ENCAL01.CNF Spectrum Number 1L STD Sample Description 1 Liter marinelli with 1.15 g/cc Sample Type Sample Geometry 1 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.00 keV Sample Size 1.OOOE+000 Unit Sample Collection Date Spectrum Collection Date 11/13/02 6:58:59 PM Decay Corrected To Collected By P. Jones Live Time 3600.0 seconds Real Time 3649.2 seconds 

  % Dead Time                           1.35 %

Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 1 

                         ~.

Performed & Reviewed By Date IJ/ 71/ OQA Supervisory Review f- AZ - Date .al L/_ 17 -

Peak Locate Analysis Report 11/17/02 5:58:08 PM Page 2 P E A K L O C A T E R E P O R T

I Detector DET01 Sample I.D. C
\GENIE2K\CAMFILES\ENCALO1.CNE Spectrum Number 1L STD Sample Description 1 Liter marinelli with 1.15 g/cc ma Sample Type Peak Locate Performed on 11/17/02 5:58:07 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.08 0. 1473 42.24 16.82 0.6779 2 237.05 0.0624 59.55 80.33 1. 1273 3 351.06 0.0471 88.05 135.12 1. 1351 4 487.21 0.0523 122.08 105.71 1. 1318 5 544.98 0.0949 136.51 31.99 1. 1796 6 662.54 0.0557 165.89 84.33 1.1936 7 1019.41 0. 1865 255.07 7.78 1. 1377 8 1115.98 0.1188 279.18 17.67 1.2757 9 1566.22 0.0556 391.70 71.45 1.4194 10 2646.37 0.0373 661.60 132.96 1.6737 11 3255.39 0.2135 813.79 4.03 1. 5370 12 3592.21 0. 0469 897.96 76.29 1. 8903 13 4693.53 0. 0341 1173.15 127.33 2. 1958 14 5301.17 0. 1591 1325.22 6.27 2.3383 15 5331.04 0.0341 1332.44 121.74 2.3431 16 7346.82 0.0471 1836.15 54.14 2. 8199 Errors quoted at 1.96 sigma

Peak Analysis Report 11/17/02 5:58:08 PM Page 3 P E A K A N.A L Y S I S R E PO R T i ************************************* Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\ENCALO1.CNF Spectrum Number 1L STD Sample Description 1 Liter marinelli with 1.15 g/cc matrix Peak Analysis Performed on 11/17/02 5:58:07 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak En(ergy Net Peak Net Area Continuum No. start end centroid ceV) (1 Area Uncert. Counts F 1 164- 173 167.77 42.24 1.89E+003 110.49 3.19E+003 F 2 221- 246 237.02 59.55 3.22E+004 369.12 2.32E+004 F 3 334- 366 351.08 88.05 7.37E+004 531.53 3.12E+004 F 4 474- 501 487.28 122.08 4.15E+004 406.72 1.83E+004 F 5 535- 562 545.02 136.51 5. 48E+003 188.50 1. 43E+004 F 6 652- 682 662.60 165.89 2.64E+004 327.06 1.40E+004 F 7 1012- 1030 1019.49 255.07 6.88E+002 120.69 6.72E+003 F 8 1107- 1124 1115.97 279.18 1.88E+003 135.19 5.81E+003 F 9 1550- 1588 1566.26 391.70 1.54E+004 251.02 8. 62E+003 F 10 2625- 2675 2646.38 661.60 4.85E+004 423.44 7.09E+003 F 11 3246- 3269 3255.44 813.79 2.05E+002 82.36 2.89E+003 F 12 3576- 3614 3592.27 897.96 1.75E+004 266.28 5.49E+003 F 13 4664- 4721 4693.54 1173.15 5.11E+004 431.13 3.42E+003 M 14 5288- 5357 5302.11 1325.22 3.42E+002 55.80 8. 68E+002 m 15 5288- 5357 5331.03 1332.44 4.66E+004 411.65 9.OOE+002 F 16 7322- 7372 7346.82 1836.15 1.12E+004 202.77 3. 07E+002 M - First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/17/02 5:58:08 PM Page 4 I***** N.UCLIDE IDENTIFICATION REPORT ***** 6 Sample I.D. C:\GENIE2K\CAMFILES\ENCALO1.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB 

        ....................        IDENTIFIED NUCLIDES Nuclide      Id        Energy     Yield    Activity     Activity Name      Confidence   (keV)       (%)    (uCi/Unit)   Uncertainty CO-57       1.000     122.06*     85.51 1.172E-002    7.119E-004 136. 48*    10.60 1.230E-002    9.358E-004 CO-60       0.999    1173.22*    100.00 4.676E-002    2.375E-003 1332.49*    100.00 4.735E-002    2.550E-003 Y-88        0.998     898.02*     93.40 1.376E-002    6.863E-004 1836.01*     99.38 1.416E-002    1.205E-003 CD-109      1.000      88.03*      3.72 6.251E-001    6.101E-002 SN-113      1.000     255.12*      1.93 1.067E-002    2.292E-003 391.69*     64.90 9.315E-003    6.117E-004 CS-137      1.000     661.65*     85.12 3.265E-002    1.884E-003 CE-139      1.000     165.85*     80.35 8.028E-003    5.384E-004 HG-203      1.000     279.19*     77.30 7.675E-004    7.771E-005 AM-241      1.000      59.54*     35.90 8.013E-002    8.331E-003
             * = Energy line found in the spectrum.
             @ = Energy line not used for Weighted Mean Activity Energy tolerance used was      1.000 Nuclide confidence index threshold =       0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/17/02 5:58:08 PM Page 5 

   ***     I N T E R F E R E N C E    C O R R E C T E D       R E P O R T      ***

Sample I.D. C:\GENIE2K\CAMFILES\ENCALO1.CNF 

       - Spectrum Number         IL STD Performed & Reviewed By           62     s-              Date    /i/ /7/d2_

Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/Unit) Uncertainty  % Uncertainty CO-57 1.000 1. 19E-002 5.67E-004 4.7 CO-60 0.999 4.70E-002 1.74E-003 3.7 Y-8-8 0.998 1.39E-002 5. 96E-004 4.3 CD-109 1.000 6.25E-001 6. 1OE-002 9.8 SN-113 1.000 9.41E-003 5.91E-004 6.3 CS-137 1.000 3.27E-002 1. 88E-003 5.8 CE-139 1.000 8.03E-003 5.38E-004 6.7 HG-203 1.000 7.68E-004 7.77E-005 10.1 AM-241 1.000 8.01E-002 8.33E-003 10.4 

      ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
      @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   1.96 sigma

Interference Corrected Activity Report 11/17/02 5:58:08 PM Page 6 U N I D E N T I F I E D P E A K S Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.24 5.2527E-001 5.84 F 11 813.79 5.6830E-002 40.26 M 14 1325.22 9.5011E-002 16.31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma 

                                         ,     4 /o   z    l1 1380 Seaboard Industrial Blvd.

ANALYTICS Atlanta, Georgia 30318 *U.S.A. Phone (404) 352-8677 Fax (404) 352-2837 CERTIFICATE OF CALIBRATION Standard Radionuclide Source 62866-521 1.0 Liter Solid in 133N GA-MA Beaker This standard radionuclide source was prepared using aliquots mea-sured gravimetrically from master radionuclide solution sources. The Am-241 was calibrated by 4 pi alpha liquid scintillation count-ing. All other radionuclides were calibrated using a germanium gam-ma spectrometer system. Calibration and purity were checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains traceability to the National Institute of Stan-daids and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Rev. 1, February, 1979. US Patent 4,430,258; UK Patent GB2,149,194B; CA Patent 1,196,776. Density of solid matrix 1.15 g/cc. Calibration date: January 1, 2002 12:00 EST TOTAL GAMMA-RAY GAMMA-RAYS UNCERTAINTY ISOTOPE ENERGY HALF-LIFE PER SECOND  % Am- 241 59.5 432 y 1057 5.0 Cd-109 88 462.6 d 1390 4.8 Co-57 122 271.79 d 838. 8 4.9 Ce-139 166 137.6 d 1159 4.5 Hg-203 279 46.61 d 2828 4.6 Sn-113 392 115.1 d 1470 4.2 Cs-137 662 30.07 y 1032 4.0 Y-88 898 106.6 d 3931 4.2 Co-60 1173 5.2714 y 1928 4.0 Co-60 1332 5.2714 y 1941 4.0 Y-88 1836 106.6 d 4112 4.2 P 0 NUMBER 14531, It SOURCE PREPARED BY:

m. D. Currie, Rad ochemist Q A APPROVED: .

t4 _j r - 

                            . I _   ,   . _

C This standard will expire one year after the calibration date.

Certificate File Listing Report 11/13/2002 7:56:16 PM Page 1 CERTIFICATE FILE REPORT Filename: C:\GENIE2K\CAMFILES\100201.CTF Certificate

Description:

Certificate

Title:

62866-521 1L Solid Matrix in mar Quantity . 1.00 units Assay date 1/1/2002 12:00:00 PM Nuclide Half-Life Energy Emission Rate Emission Rate Name (Days) (keV ) GPS/Unit  % Uncert.(+-) Am-241 1.579E+005 59.537* 1057.0 5.00 Cd-109 4.640E+002 88. 032 1390.0 4.80 Co-57 2.709E+002 122.063 838.8 4.90 Ce-139 1.377E+002 165. 853 1159.0 4.50 Hg-203 4.660E+001 279.189 2828.0 4.60 Sn-113 1.151E+002 391. 688 1470.0 4.20 Cs-137 1.102E+004 661.649* 1032.0 4.00 Y-88 1.066E+002 898.021 3931.0 4.20 

 . -60                     1.925E+003                   1173.220                        1928.0                      4.00
      -60                  1.925E+003                   1332.490                        1941.0                      4.00
,     88                   1.066E+002                   1836.010*                       4112.0                      4.20
* - Used for Calib/INIT

G A M M A S P E C T R U M A N A L Y S I S FI name: C:\GENIE2K\CAMFILES\ENCAL01.CNF Report Generated On  : 11/13/2002 8:51:43 PM Sample Title  : 1 Liter Water calibration spectrum Spectrum Description  : Calibration Spectrum Sample Identification  : IL STD Sample Type Sample Geometry  : 1 Peak Locate Threshold  : 5.00 Peak Locate Range (in channels)  : 1- 4096 Peak Area Range (in channels)  : 1- 4096 Identification Energy Tolerance  : 1.000 keV Sample Size  : 1.OOOE+000 Unit Sample Taken On Acquisition Started  : 11/13/2002 6:58:59 PM Live Time 3600.0 seconds Real Time  : 3649.2 seconds Dead Time  : 1.35 % Energy Calibration Used Done On  : 11/13/2002 Efficiency Calibration Used Done On  : 11/13/2002 Efficiency ID  : 1

Efficiency Calibration Report 11/13/2002 8:52:15 PM Page 1

  • ** E F F I C I E N C Y C A L I B R A T IO N R EPORT *****
         ~                           i Detector Name: DET01 Sample

Title:

- 1 Liter Water calibration spectrum Geometry

Description:

1 Efficiency Calibration Performed on: 11/13/2002 8:36:02 PM by: Geometry Type Used: DUAL Efficiency Triplets Energy Efficiency Error 59.54 8.41E-003 4.25E-004 88.03 2.37E-002 1.14E-003 122.06 3.1OE-002 1.53E-003 165.85 3.14E-002 1.43E-003 279.19 2.13E-002 1.46E-003 391.69 1. 97E-002 8.49E-004 661.65 1.34E-002 5.39E-004 898.02 9.76E-003 4.19E-004 1173.22 8.29E-003 3.34E-004 1332.49 7.50E-003 3.02E-004 1836.01 5.96E-003 2.57E-004 DUAL Efficiency Calibration Equation 

                                      =       -========

Single Equation Terms -> Offset: -441.296 Slope: 355. 603 Quadratic: -115. 039 Cubic: 18. 562 4th Order: -1.496 5th Order: 0.048 6th Order: 0.000 7th Order: 0. 000 8th Order: 0.000 9th Order: 0.000

Energy Calibration Report 11/13/2002 8:48:10 PM Page 1 E N E R G Y C A L I B R A T IO N R E P O R T ,W Detector Name: DETO1 Sample

Title:

1 Liter Water calibration spectrum ENERGY CALIBRATION COEFFICIENTS ************* Energy Calibrpte Performed on: 11/13/2002 8:26:10 PM by: t--ZaMJ Energy Calibrate Type: POLY Energy(keV) = 0.320 + 0.250*ch + 0.00E+000*ch^2 + 0.OOE+000*chA3 SHAPE CALIBRATION COEFFICIENTS ** * * ** *

  • Shape Calibrate Performed on: 11/13/2002 8:26:10 PM by:

FWHM 0.623 + 0.046*E^1/2 LOW TAIL = 6.9E-001 + 8.4E-004*E ENERGY CALIBRATION RESULTS TABLE Centroid Centroid Energy Channel error (keV ) 237.04 0.03 59.54 351.09 0.03 88.03 487.28 0.02 122.06 662.58 0.03 165.85 1116.02 0.10 279.19 1566.26 0.03 391.69 2646.36 0.03 661.65 3592.25 0.03 898.02 4693.53 0.04 1173.22 5331.04 0.04 1332.49 7346.81 0.04 1836.01 SHAPE CALIBRATION RESULTS TABLE Energy FWHM FWHM TAIL TAIL (keV ) channels error channels error 59.54 4.34 0.07 2.57 0.21 88.03 4.53 0.06 3.16 0.29 122.06 4.59 0.05 3.82 0.48 165.85 4.87 0.06 4.80 1.48 279.19 5.19 0.26 2.85 0.71 391.69 5.70 0.07 4.60 0.59 661.65 6.74 0.06 5.47 0.41 898.02 7.60 0.06 6.09 0.42 1173.22 8.78 0.07 6. 83 0.34 1332.49 9.36 0.08 7.47 0.45 1836.01 11.26 0.07 8.51 0.33 G A N M A S P E C T R U M A N A L Y S I S

Dual Efficiency Calibration Curve I- - - Low Energy

  • Measured - High Energy 0 500 1000 1500 2000 2500 Energy (keV)

Datasource: DET01 in(Eft) = -4.413e+002 + 3.556e+002*(n(E) - 1.150e+002*In(E)^2 + 1.856e+001*In(E)^3 1.496e+000*ln(E)A4 + 4.810e-002*1n(E)A5

Energy Calibration Curve U Measured Calculated 0UU0-2000- 

       ,I C rum   _ _ __ _ _ _ I__    _ _ __ _ _ _ I__ _ _ _ _ _ _ _ I__ _ _ __ _ _ _ I__ _ __ __ __ _ _I I k

V 1000 500 

                'I-amu 0

0 1024 2048 3072 4096 5120 6144 7168 8192 Channel Datasource: DET01 Energy a 3.203eO001 keV + 2.499e 001lCh FWHM = 6.229e-001 keV + 4.624e*021E^1/2 Lo Tail

  • 6.87le-0O1 keV + 8.395e*004* E IL %5o1.J

(I-i C ( Date: 11-14-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S(N 64091-486 Duratek# 080201 I CSA.._A As:..:4.. A_ - ... - - . - '

,i l1, ffiz,,.

4wi ,1

ource Radvixy on * 'MJt0,'2I Count Date:

Total Source Activity Activity Isotope Energy Yield Activity Activity Uncertainty Current Original Activity a~ I. (keV) pamjsec) (uCI) 1  % difference Am-241 59.5 g 7-485E-1 , .ovSTL..U -2.95 Cd-109 88 1.008E+00 -3.57 Co-57 122 2.303E-02 -4.12 Ce-139 166 3.552E-02 -2.76 Hg-203 279 7.821E-02 -5.13 Sn-113 392 6.516E-02 -2.21 Cs-137 662 3.187E-02 -0.52 Y-88 898 1.008E-01 -5.96 Co-60 1173 4.868E-02 0.12 Co-60 1332 4.934E-02 0.25 Y-88 1836 1.037E-01 -1.56 I ' I

1. Source quantification following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from "Radioactive Decay Data Tables D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*100 CC.
                      '4

G A M M A S P E C T R U M A N A L Y S I S i ************************************ Report Generated On- 11/14/02 6:47:11 PM Detector DET01 Sample I.D. C:\GEINIE2K\CAMFILES\250ml calibration.CNF Spectrum Number 250mL STD Sample Description 250 mL marinelli with 1.58 g/cc Sample Type Sample Geometry 1 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.00 keV Sample Size 1.OOOE+000 Unit Sample Collection Date Spectrum Collection Date 11/13/02 9:02:22 PM Decay Corrected To Collected By P. Jones Live Time 2913.9 seconds Real Time 3000.1 seconds 

     % Dead Time                                      2.87 %
,    Background Type                                  STEP Energy Calibration Performed On              11/13/02 Efficiency Calibration Performed On          11/13/02 Calibration Geometry Used Performed & Reviewed By                   -6/519                    Date   __ / a    _

_/ Supervisory Review Date / /7/ 

                                                                           /Z:     °O-I'

Peak Locate Analysis Report 11/14/02 6:47:12 PM Page 2 P E A K L O C A T E R E P O R T Detector DETOI Sample I.D. C:\GENIE2K\CAMFILES\250ml calibration.CNF Spectrum Number 250mL STD Sample Description 250 mL marinelli with 1.58 g/cc mat Sample Type Peak Locate Performed on 11/14/02 6:4.7:11 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.20 0.1301 42.37 21.06 0.7627 2 236.72 0. 0648 59.46 74.13 1.1540 3 281.49 0.2916 70.65 3.70 1.0578 4 290.11 0.2180 72.73 8.04 1.0637 5 350. 84 0. 0427 87.99 163.74 1.1771 6 487.01 0. 04 66 122.03 132.04 1.1932 7 544.85 0. 0852 136.46 39.61 1.2068 8 662.31 0. 0432 165.84 142.77 1.2526 9 953.88 0.1977 238.70 6.79 0. 9910 10 1019.60 0. 1221 255.11 16.66 1.3060 11 1115.89 0. 0486 279.18 100.92 1. 3384 12 1406.80 0.2443 352.02 3.92 1.8353 13 1566.03 0. 0394 391.66 141.25 1. 4687 14 2042.67 0. 1790 510.79 5.29 2. 3836 15 2436.10 0.2437 609.05 4.11 0. 8965 16 2646.16 0. 0367 661.56 138.78 1.7402 17 3255.77 0. 1427 813.89 7.96 1. 9374 18 3592.00 0. 0341 897.91 143. 02 1. 9935 19 4693.29 0.0333 1173.10 133.75 2.2802 20 5300.52 0.1275 1324.97 8.82 2. 4640 21 5330.79 0. 0335 1332.40 124.43 2. 4688 22 7346.57 0. 0351 1836.09 97.72 2. 9765 Errors quoted at 1.96 sigma

Peak Analysis Report 11/14/02 6:47:12 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector DET01-Sample I.D. C:\GENIE2K\CAMFILES\250ml calibration.CNF Spectrum Number 25OmL STD Sample Description 250 mL marinelli with 1.58 g/cc matrix Peak Analysis Performed on 11/14/02 6:47:11 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 176 168.27 42.37 3.74E+003 144.40 6.88E+003 F 2 221- 252 236.68 59.46 3.25E+004 386.71 4.17E+004 M 3 265- 294 281.45 70.65 1. 10E+003 207.95 2.29E+004 m 4 265- 294 289.79 72.73 1. 33E+003 223.82 2.-28E+004 F 5 333- 367 350.86 87.99 1.18E+005 669.60 5. 41E+004 F 6 474- 505 487.09 122.03 7.21E+004 533.89 3. 67E+004 F 7 532- 562 544.82 136.46 9.42E+003 253.42 3.05E+004 F 8 642-. 681 662.40 165.84 7.60E+004 537.95 3.42E+004 F 9 947- 960 953.97 238.70 6.45E+002 159.38 1.OOE+004 F 10 1009- 1029 1019.64 255.11 2.45E+003 173.91 1.27E+004 

  -F    11       1107-    1138     1115.98         279.18      3.28E+004      365.30            1. 67E+004 Sw F     12       1401-    1416     1407.48         352.02      5.02E+002      135.17            6.25E+003 F    13       1541-    1590     1566.12         391.66      5.91E+004      469.08            1.75E+004 F    14       2027-    2056     2042.86         510.79      1.13E+003      133.91            8.19E+003 F    15       2430-    2443     2436.06         609.05      1.84E+002         96.25          3.54E+003 F    16       2624-    2671     2646.21         661.56      5.68E+004      459.91            1.30E+004 F    17       3247-    3270     3255.83         813.89      7.72E+002      112.68            4.42E+003 F    18       3569-    3620     3592.07         897.91      6.40E+004      486.48            1.06E+004 F    19       4671-    4728     4693.33        1173.10      6.02E+004      468.90            5.38E+003 M 20        5286-    5359     5301.13        1324. 97     9.44E+002        88.33           2.07E+003 m 21        528 6-   5359     5330.83        1332.40      5.49E+004      446.12            2.13E+003 F 22          7317-    7374     7346.55        1836.09      3.98E+004      378.57            9.06E+002 M= First peak in aFmultiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at              1.96 sigma

Interference Corrected Activity Report 11/14/02 6:47:12 PM Page 4 

   *****    N U C L I D E    I D E N T I F I C A T IO N       R E P O R T    *****

Sample I.D. C:\GENIE2K\CAMFILES\250ml calibration.CNF Nuclide Library Used- C:\GENIE2K\CAMFILES\CALIB.NLB 

        ....................      IDENTIFIED NUCLIDES       ......................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/Unit) Uncertainty CO-57 1.000 122.06* 85.51 1. 611E-002 9.356E-004 136.48* 10.60 1.657E-002 1.158E-003 CO-60 0.998 1173.22* 100.00 4.637E-002 2.586E-003 1332.49* 100.00 4.704E-002 2.782E-003 Y-88 0.999 898.02* 93.40 4.190E-002 2.141E-003 1836.01* 99.38 4.316E-002 3.718E-003 CD-109 1.000 88.03* 3.72 8.240E-001 7.999E-002 SN-113 1.000 255.12* 1.93 2.967E-002 4.091E-003 391.69* 64.90 2.871E-002 1.736E-003 CS-137 0.999 661.65* 85.12 3.162E-002 1.897E-003 CE-139 1.000 165.85* 80.35 1.796E-002 1.070E-003 HG-203 1.000 279.19* 77.30 1.051E-002 6.597E-004 AM-241 0.999 59.54* 35.90 7.258E-002 7.792E-003 

            * = Energy line found in the spectrum.
            @ = Energy line not used for Weighted Mean Activity Energy tolerance used was     1.000 Nuclide confidence index threshold =      0.10 Errors quoted at   1.960 sigma

Interference Corrected Activity Report 11/14/02 6:47:12 PM Page 5 

   ***         I N T E R F E R E N C E            C O R R E C T E D     R E P O R T      ***

Sample I.D. C:\GENIE2K\CAMFILES\250ml calibration.CNF Spectrum Number 250mL STD Performed & Reviewed By -T7 0: Date ___ /Z/ 10 Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/Unit) Uncertainty  % Uncertainty CO-57 1.000 1. 63E-002 7.28E-004 4.5 CO-60 0.998 4. 67E-002 1.89E-003 4.1 Y-88 0. 999 4.22E-002 1.86E-003 4.4 CD-109 1.000 8.24E-001 8.OOE-002 9.7 SN-113 1.000 2.89E-002 1.60E-003 5.5 CS-137 0.999 3.16E-002 1.90E-003 6.0 CE-139 1.000 1.80E-002 1.07E-003 6.0 HG-203 1.000 1.05E-002 6. 60E-004 6.3 AM-241 0. 999 7.26E-002 7.79E-003 10.7 

        ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
        @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at             1.96 sigma

Interference Corrected Activity Report 11/14/02 6:47:12 PM Page 6 U N I D E N T I F I E D P E A K S Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.37 1.2839E+000 3.86 M 3 70.65 3.7665E-001 18.95 m 4 72.73 4.5612E-001 16.84 F 9 238.70 2.2139E-001 24.71 F 12 352.02 1.7244E-001 26.90 F 14 510.79 3.8689E-001 11.88 F 15 609.05 6.3069E-002 52.37 F 17 813.89 2.6505E-001 14.59 M20 1324.97 3.2411E-001 9.35 M = First peak in a multiplet region 

     -m =-Other peak in a multiplet region F = Fitted singlet Errors quoted at   1.96 sigma

ANALYTICS K) 1380 Seaboardn kwudus 81 Adanta, Geoagia 30318 U.SA

  • zo-oz. X'rcL(( OFLAC)O Pe(4042-a Fax (404) 352-2837 CERTIFICATE OF CALIBRATION Standard Radionuclide Source 64091-466 Sand in 250 mL Marinelli Beaker Filled to Top This standard radionuclide source was prepared using aliquots mea-sured gravimetrically from master radionuclide solution sources.

The Am-241 was calibrated by 4 pi alpha liquid scintillation count-ing. All other radionuclides were calibrated using a germanium gam-ma spectrometer system. Calibration and purity were checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains traceability to the National Institute of Stan-dards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Rev. 1, February, 1979. Calibration date: July 1, 2002 12:00 EST TOTAL GAMMKA- RAY GAMMA- RAYS UNCERTAINTY ISOTOPE ENERGY HALF-LIFE PER SECOND  % Am-241 59.5 432 y 994.2 5.0 Cd-109 88 462.6 d 1439 5.0 Co-57 122 271.79 d 759.8 4.7 Ce-139 166 137.6 d 1086 4.3 Hg-203 279 46.61 d 2358 4.1 Sn-113 392 115.1 d 1600 4.1 Cs-137 662 30.07 y 1009 4.8 Y-88 898 106.6 d 3704 4.2 Co-60 1173 5.2714 y 1799 4.1 Co-60 1332 5.2714 y 1821 4.2 Y-88 1836 106.6 d 3873 4.0 490 grams/310 mL of sand. P 0 NUMBER 14630, Item 2 SOURCE PREPARED BY: V( t D D. rrie, Radiochemist Q A APPROVED: / r/v/4-This standard will expire one year after the calibration date. 

  ' *,.  ~LL.4L       t     ... s       (-VI 1380 Seaboard Industrial Blvd.

Atlanta, Georgia 30318 - U.SA. ' 6° Phone (404) 352-8677 Fax (404) 352-2837 email: analytics~mindspring.com www.analyticsinc.com ANALYSIS OF UNCERTAINTY BATCH 109 MIXED GAMMA STANDARDS WITH Am-241 CALIBRATION DATE: July 1, 2002 12:00 EST GGAMMA RAY RANDOM ERROR % SYSTEMATIC ERROR % TOTAL % ENERGY (keV) (99 % CL) 59.5 2.0 3.0 5.0 88 1.8 3.2 5.0 122 2.0 2.7 4.7 166 1.5 2.8 4.3 279 1.1 3.0 4.1 392 1.3 2.8 4.1 662 1.8 3.0 4.8 898 1.2 3.0 4.2 1173 1.3 2.8 4.1 1332 1.4 2.8 4.2 1836 1.0 3.0 4.0 The systematic error includes the error in calibration standards, weighing error, and estimated counting corrections. All uncertain-ties are stated at the 99% confidence level. No interfering gamma emitting impurities were detected during calibration. Depending on the resolution and energy dispersion (kev/channel) of the measuring system, the following spectral conflicts may occur: (1) between the 88 keV gamma-ray and the X-rays emitted in the decay of Eg-203, (2) between the 1333 keV gamma-ray and the 1325 keV single escape peak from the 1836 keV gamma-ray.

Dual Efficiency Calibration Curve 

                               - - -  Low Energy    a   Measured    -       High Energy 0                  500                   1000                   1500              2000 2500 Energy (keV)

Datasource: DET01 In(Eff) = -4.144e+002 + 3.289e+002*ln(E) - 1.047e+002*1n(E)A2 + 1.664e+001*In(E)A3

  • 1.322e+000*ln(E)Y4 + 4.197e.002*tn(E)^5
                                                         / z./f7   /o -a---

A t ~, 4,

Certificate File Listing Report 11/13/2002 7:51:08 PM Page 1 

  '***                   C E R T I F I C A T E               F I L E     R E P O R T Filename: C:\GENIE2K\CAMFILES\080201.CTF Certificate

Description:

Certificate

Title:

64091-466 250 mL Sand Matrix in Quantity  : 1.00 units Assay date 7/1/2002 12:00:00 PM Nuclide - Half-Life Energy Emission Rate Emission Rate Name (Days) (keV ) GPS/Unit  % Uncert.(+-) Am-241 1.579E+005 59.537* 994.2 5.00 Cd-109 4.640E+002 88.032 1439.0 5.00 Co-57 2.709E+002 122.063 759.8 4.40 Ce-139 1.377E+002 165. 853 1086.0 4.30 Hg-203 4. 660E+001 279. 189 2358.0 4.40 Sn-113 1.151E+002 391. 688 1600.0 4.20 Cs-137 1.102E+004 661. 649* 1009.0 4.30 Y-88 1.066E+002 898. 021 3704.0 4.40 o-60 1.925E+003 1173.220 1799.0 4.40 _-60 1.925E+003 1332. 490 1821.0 4.60 T- 8 8 1.066E+002 1836. 010* 3873.0 4.40 

* = Used for Calib/INIT LL               21131/o; Illn/Oz        f.

v **** G A M M A S P E C T R U M A N A L Y S I S-*** Report Generated On 12/12/02 1:21:05 PM Detector DET01 Sample I.D. C:\GE:,NIE2K\CAMFILES\QC 120802C.CNF Spectrum Number QC120802C.CNF Sample Description Mixed Gamma un 250ml Marinelli Sample Type Marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.50 keV Sample Size 1.000E+000 ea Sample Collection Date Spectrum Collection Date 12/8/02 3:09:01 PM Decay Corrected To Collected By L. Finn Live Time 600.0 seconds Real Time 616.2 seconds 

        % Dead Time                                                     2.63 %

Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 

                                                           ,I Performed & Reviewed By                                 Za
                                                      /--,                 -                Date            L/. A/ ecL)-

Supervisory Review Date t2 /ja 

                                                                                                                      /

p

Peak Locate Analysis Report 12/12/02 1:21:05 PM Page 2 P E A K L O C A T E R E P O R T as Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120802C.CNF Spectrum Number QC120802C.CNF Sample Description Mixed Gamma un 250ml Marinelli Sample Type Marinelli Peak Locate Performed on 12/12/02 1:21:04 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 164.13 0.1939 41 . 61 10.81 0. 9661 2 236.05 0.1145 59.33 16.91 1 . 6042 3 350.08 0.0754 87.83 40. 72 1. 5861 4 486.26 0.0816 121.86 34.45 1. 5877 5 543.75 0. 1478 136.25 9.98 1. 5778 6 661.37 0.0768 165.62 36.84 1. 6371 7 1018 .85 0.1967 254.92 5.75 1.5360 8 1114 .82 0.0911 278.92 24.43 1. 7360 9 1564 .84 0. 0661 391.38 43.88 1. 7717 10 2644 .94 0. 0570 661.26 52.29 1.9741 11 3590.82 0. 0541 897.60 53.28 2.1372 12 4691 .98 0. 0499 1172.77 57 . 06 2.3375 13 5297.71 0. 1827 1324.24 3.55 2.4677 14 5329.39 0.0499 1332.04 53.87 2.4727 15 7344.88 0.0525 1835.69 43.66 2.7699 Errors quoted at 1.96 sigma

Peak Analysis Report 12/12/02 1:21:05 PM Page 3 -. ~***** P E A K A N A L Y S I S R E P O R T AW)************************************* Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120802C.CNF Spectrum Number QC120802C.CNF Sample Description Mixed Gamma un 250ml Marinelli Peak Analysis Performed on 12/12/02 1:21:04 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 160- 175 165.23 41.61 8. 87E+002 67.93 1. 58E+003 F 2 220- 244 236.15 59.33 7. 01E+003 173.13 6. 14E+003 F 3 335- 365 350.22 87.83 2.43E+004 288 .90 8.81E+003 F 4 473- 501 486.38 121.86 1.47E+004 229.72 6.13E+003 F 5 536- 553 544.00 136.25 1. 77E+003 109.27 3. 32E+003 F 6 650- 679 661.52 165.62 1.41E+004 221.26 4. 58E+003 F 7 1010- 1028 1018.89 254.92 4.75E+002 75.55 2. 09E+003 F 8 1101- 1124 1114.92 278.92 4.70E+003 137.51 2.39E+003 F 9 1553- 1585 1565.00 391.38 1. 10E+004 196.15 2.28E+003 10 2 631- 2664 2645.00 661.26 1. 19E+004 206.29 1.70E+003 i- F 11 3573- 3608 3590.81 897 . 60 1. 15E+004 204.13 1.38E+003 F 12 4 674- 4712 4692.02 1172.77 1.24E+004 211. 05 6. 43E+002 M 13 5283- 5349 5298.21 1324.24 2.20E+002 37.30 2. 98E+002 m 14 5283- 5349 5329.40 1332.04 1.13E+004 201.31 3. 05E+002 F 15 7323- 7367 7344.95 1835.69 7. 12E+003 161.77 1. 53E+002 First peak in a multiplet region Other peak in a multiplet region Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/12/02 1:21:05 PM Page 4 IL ***** N U C L I D E I D E N T I F I C A T IO N R E P O R T ***** 

  /  *************************************************************************

Sample I.D. C:\GENIE2K\CAMFILES\QC 120802C.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB 

         ....................      IDENTIFIED NUCLIDES Nuclide     Id        Energy     Yield     Activity     Activity Name     Confidence   (keV)        (%)    (uCi/ea )    Uncertainty CO-57      0.997     122.06*     85.51 1.599E-002     9.552E-004 136.48*     10.60 1.510E-002     1.349E-003 CO-60      0.986    1173.22*    100.00 4.636E-002     2.678E-003 1332.49*    100.00 4.689E-002     2.871E-003 Y~88       0.990     898.02*     93.40 3.646E-002     1.953E-003 1836.01*     99.38 3.754E-002     3.322E-003 CD-109     0.997      88.03*      3.72 8.286E-001     8.094E-002 SN-113    0.994     255.12*      1. 93 2.791E-002    5.531E-003 391.69*     64. 90 2.584E-002    1.616E-003 CS-137     0.989     661.65*     85.12 3.215E-002     1.991E-003 CE-139     0.996     165.85*     80.35 1. 613E-002    9.862E-004 HG-203     0.995     279.19*     77.30 7.313E-003     5.OOOE-004 AM-241     0.997      59.54*     35.90 7.682E-002     8.480E-003
             * = Energy line found in the spectrum.
             @ = Energy line not used for Weighted Mean Activity Energy tolerance used was      1.500 Nuclide confidence index threshold =       0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 12/12/02 1:21:05 PM Page 5

  • I N T E R F E R E N C E C O R R E C T E D R E P O R T Sample I.D. -C:\GENIE2K\CAMFILES\QC 120802C.CNF Spectrum Number QC120802C.CNF Performed & Reviewed By Date la/jvj3- /0.-

Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 0.997 1.57E-002 7. 80E-004 5.0 CO-60 0.986 4.66E-002 1. 96E-003 4.2 Y-88 0.990 3. 67E-002 1. 68E-003 4.6 CD-109 0.997 8.29E-001 8. 09E-002 9.8 SN-113 0.994 2. 60E-002 1.55E-003 6.0 CS-137 0.989 3.21E-002 1. 99E-003 6.2 CE-139 0.996 1.61E-002 9. 86E-004 6.1 HG-203 0 . 995 7.31E-003 5.OOE-004 6.8 AM-241 0.997 7. 68E-002 8.48E-003 11. 0 

      ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
      @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    1.96 sigma

Interference Corrected Activity Report 12/12/02 1:21:05 PM Page 6 

       **********   U N I D E N T I F I E D    P E A K S    *****i Peak   Energy            Peak Size in        Peak CPS No.    (keV)          Counts per Second   % Uncertainty F   1    41.61              1.4782E+000           7.66 M 13  1324.24              3.6716E-001          16.93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at   1.96 sigma

       . I 1j.V9
                 ".*                                                                        Pi X 1.'..
                                                                                                                    . -7,     T.11

( C Date: 12-07-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S/N 64091-466 Duratek# 080201 1..0 Count Date: 1. Source Activity on 

                                                                  *otal Source     Activity      Activity Isotope Energy          Yield         Activity Activity         UIncertainty       Current       Original           Activity       Isotope %2life (keV) (gam/dIs.       (gam.lsec) (uCi)               10)                (UCi)         (uCi) .
                                                                                                                  % difference R

Am-241 59.5 0.359 O~2 7.485E-02 8.136E-02 8.70 Cd-109 88 0.0372 11.045E;00 :!1 1.074E+00 2.74 Co-57 122 0.8551 T+ 2.401 E-02 2.388E-02 -0.55 Ce-139 168 0.8035 1 3.653E-02 g 3.697E-02 1.20 Hg-203 279 0.773 S$- 8.244E-02. 8.377E-02 1.61 Sn-1 13 392 0.649 ~-.~O 6.663E-02 6.774E-02 1.66 Cs-137 662 0.8512 I00 3.204E-02 3.313E-02 3.41 Y-88 898 0.934 1.072E-01 1 1.043E-01 -2.67 Co-60 1173 1 'I9 4.862E 5.009E-02 3.01 Co-60 1332 I 1~t 4.922E-02 5.009E-02 1.77 Y-88 1836 0.9938 1.053E-01 - 1.043E-01 -0.96

I
1. Source quantification following calibration on Nov. 13 2002
2. Gamma ray yields obtained from ZRadioactive Decay Data Tables" D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*100

G AM MA SP EC TR U M ANAL Y SI S @4** Report Generated On 1/21/03 12:39:11 PM Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120702B.CNF Spectrum Number QC120702B.CNF Sample Description Mixed Gamma in Marinelli Sample Type Marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in charLnels) 100 - 8192 Peak-Area Range (in channe1ls) 100 - 8192 Identification Energy Tole rance 1.50 keV Sample Size 1.OOOE+000 ea Sample Collection Date Spectrum Collection Date 12/7/02 1:30:01 PM Decay Corrected To Collected By L. Finn Live Time 600.0 seconds Real Time 616.6 seconds 

    % Dead Time                                 2.70 %

Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed By Date Z /Z7/ a Supervisory Review ....an. o .. .. Date _ /x7/03_

Peak Locate Analysis Report 1/21/03 12:39:11 PM Page 2 P E A K L O C A T E R E P O R T Detector DET01 Sample I.D. C:\ \GENIE2K\CAMFILES\QC 120702B.CNF Spectrum Number QC120702B.CNF Sample Description Mixed Gamma in Marinelli Sample Type Marinelli Peak Locate Performed on 1/21/03 12:39:11 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (key) Significance (keV) 1 163.65 0.2001 41. 45 9.29 0. 9089 2 236.55 0. 1002 59.42 27.25 1. 3447 3 350.46 0. 0666 87.91 58. 89 1. 3043 4 486.69 0.0724 121. 94 49.11 1. 3099 5 544.34 0.1305 136.33 15.23 1. 3014 6 662.03 0. 0684 165.77 53. 18 1. 3678 7 1019.37 0. 1900 255.17 6.45 1. 4929 8 1115.74 0.0793 279.14 35.54 1. 4051 9 1566.19 0.0609 391.70 57.01 1. 5030 10 2647.15 0.0532 661. 80 64.09 1.6974 11 3256.09 0.2324 813.98 4.00 1. 1527 12 3593.76 0. 0514 898.33 62.26 1.8955 13 4695.82 0. 0480 1173.73 65.68 2.1014 14 5303.14 0.1578 1325.57 5.80 2.2157 15 5333.69 0. 0473 1333.10 64 .18 2.2206 16 7351.16 0. 0505 1837.19 49.83 2.5209 Errors quoted at 1. 96 s igma

Peak Analysis Report 1/21/03 12:39:11 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120702B.CNF Spectrum Number QC120702B.CNF Sample Description Mixed Gamma in Marinelli Peak Analysis Perf4armed on 1/21/03 12:39:11 PM Peak Analysis From Channel 100 Peak Analysis To C]'hannel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 160- 173 164.61 41.45 8.25E+002 67.74 1.48E+003 F 2 220- 247 236.51 59.42 7.47E+003 178.70 6. 95E+003 F 3 341- 361 350.54 87.91 2.49E+004 301. 78 6.39E+003 F 4 478- 496 486.73 121.94 1. 47E+004 237.10 4.28E+003 F 5 531- 558 544.31 136.33 1.85E+003 111. 67 5.25E+003 F 6 645- 675 662.10 165.77 1.45E+004 231.43 4. 95E+003 F 7 1013- 1029 1019.88 255.17 5. 11E+002 77.74 1.98E+003 F 8 1104- 1127 1115.82 279.14 5.05E+003 145.03 2.37E+003 F 9 1556- 1579 1566.25 391.70 1. 09E+004 200.93 1. 70E+003 F 10 2 633- 2659 2647.19 661.80 1.21E+004 212.94 1. 41E+003 F 11 324 9- 3272 3256.21 813.98 9. 94E+001 44.16 8.73E+002 F 12 357 9- 3608 3593.76 898.33 1. 16E+004 207.87 1.11E+003 F 13 4 677- 4712 4695.86 1173.73 1.24E+004 213.80 7.26E+002 M 14 5290- 5350 5303.52 1325.57 2.57E+002 38.39 2.38E+002 m 15 52 90- 5350 5333.64 1333.10 1.17E+004 207.86 2. 63E+002 F 16 7330- 7371 7350.98 1837.19 7.21E+003 163.96 1.33E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

interference Corrected Activity Report 1/21/03 12:39:11 PM Page 4 

   *****           N U C L I D E           I D E N T I F I C A T IO N                                R E P O R T    *****

Sample I.D. C:\GENIE2K\CAMFILES\QC 120702B.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB 

          ....................                   IDENTIFIED NUCLIDES Nuclide          Id               Energy             Yield              Activity            Activity Name          Confidence           (keV)                 (%)           (uCi/ea )           Uncertainty CO-57           0.999            122.06*             85.51          1. 601E-002           9.578E-004 136.48*             10.60          1.581E-002            1.396E-003 CO-60           0.978           1173.22*           100.00           4.622E-002            2.675E-003 1332.49*           100.00           4.863E-002            2.977E-003 Y-88            0.947            898.02*             93.40          3.677E-002            1.972E-003 1836.01*             99.38          3.802E-002            3.377E-003 CD-109          0.999             88.03*                3.72        8.474E-001            8.278E-002 SN-113          1.000            255.12*                1. 93       3.006E-002            5.790E-003 391.69*             64.90         2.572E-002             1.613E-003 CS-137          0.998            661.65*             85.12          3.284E-002            2.035E-003 CE-139          0.999            165.85*             80.35          1.664E-002            1.019E-003 HG-203          1.000            279.19*             77.30         7.867E-003             5.359E-004 AM-241           0.999             59.54*             35.90         8.131E-002             8.914E-003
                   * = Energy line found in the spectrum.
                   @ = Energy line not used for Weighted Mean Activity Energy tolerance used was                        1.500 Nuclide  confidence          index       threshold               =          0.10 Errors quoted at            1.960      sigma

Interference Corrected Activity Report 1/21/03 12:39:11 PM Page 5 

   ***         I N T E R F E R E N C E                    C O R R E C T E D                  R E P O R T              ***

C:\EI2\AFLSQ******* *** ****** 272.N Sample I.D. C:\GENIE2K\CAMFILES\QC 120702B.CNF Spectrum Number QC120702B.CNF Performed & Reviewed By __ _ _ _ _ _ Date ) F/7 3 Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 0.999 1.59E-002 7. 90E-004 5.0 CO-60 0. 978 4.73E-002 1. 99E-003 4.2 Y-88 0.947 3.71E-002 1.70E-003 4.6 CD-109 0.999 8. 47E-001 8.28E-002 9.8 SN-113 1.000 2. 60E-002 1. 55E-003 6.0 CS-137 0.998 3.28E-002 2.04E-003 6.2 CE-139 0.999 1. 66E-002 1.02E-003 6.1 HG-203 1.000 7.87E-003 5.36E-004 6.8 AM-241 0.999 8.13E-002 8. 91E-003 11.0 

           ? = nuclide is part of an undetermined solution-X = nuclide rejected by the interference analysis
           @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                  1.96 sigma

Interference Corrected Activity Report 1/21/03 12:39:11 PM Page 6 

       **********U      N I D E N T I F I E D    P E A K S     *****i Peak       Energy         Peak Size in          Peak CPS No.       (keV)        Counts per Second    % Uncertainty F    1       41.45           1.3750E+000             8.21 F 11       813.98            1.6572E-001            44.41 M 14    1325.57             4.2850E-001            14. 93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at    1.96 sigma

**A***************A*******L***I********************************************
        ****G                  A MMA              S PE C TR UM                   A NA LY SI S***

Report Generated On 1/21/03 12:51:38 PM Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120602.CNF Spectrum Number QC120602.CNF Sample Description Mixed Gamma in 250ml Sample Type Marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in chanLnels) 100 - 8192 Peak-Area Range (in channe ls) 100 - 8192 Identification Energy Tole Xrance 1.50 keV Sample Size 1.000E+000 ea Sample Collection Date Spectrum Collection Date 12/6/02 6:37:12 AM Decay Corrected To Collected By L. Finn Live Time 600.0 seconds Real Time 616.6 seconds 

    % Dead Time                                                              2.70 %

Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 79f~ Performed & Reviewed By Date _ /fJ/4g Supervisory Review Supervisory Revew Date L/5Z'2 I /AZ/_L

Peak Locate Analysis Report 1/21/03 12:51:38 PM Page 2 P E A K L O C A T E R E P 0 R T Detector DET01 Sample I.D. C: \GENIE2K\CAMFILES\QC 120602.CNF Spectrum Number QC120602.CNF Sample Description Mixed Gamma in 250ml Sample Type Marinelli Peak Locate Performed on 1/21/03 12:51:38 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.21 0.1849 42.31 12.12 0. 6248 2 236.44 0. 1021 59.40 27. 61 1. 3222 3 350.50 0. 0680 87.92 59.29 1. 3366 4 486.81 0.0740 121.97 50.55 1. 3431 S 544.55 0.1354 136.36 13.88 1.3346 6 662.08 0.0703 165.79 52.90 1. 3896 7 1019.87 0.1917 255.20 5.94 1.3719 8 1115.58 0. 0832 279.10 32.99 1. 5037 9 1565.81 0. 0628 391.61 54.13 1. 5859 10 2645.96 0. 0557 661.51 58.78 1.8568 11 3591.90 0. 0533 897. 90 57.14 2.0569 12 4693.30 0. 0500 1173.09 58.24 2.3502 13 5299.60 0. 1865 1324.87 3.70 2.5461 14 5330.75 0. 0507 1332.39 53.90 2. 5510 15 7346.51 0. 0538 1836.07 40.85 2.9951 Errors quoted at 1.96 sigma

Peak Analysis Report 1/21/03 12:51:38 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120602.CNF Spectrum Number QC120602.CNF Sample Description Mixed Gamma in 250ml Peak Analysis Performed on 1/21/03 12:51:38 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 172 168.03 42 . 31 5.63E+002 65.06 8.22E+002 F 2 220- 252 236.44 59.40 6.87E+003 173.83 8.21E+003 F 3 333- 367 350.58 87.92 2.38E+004 295.69 1. 09E+004 F 4 472- 504 486.83 121.97 1.44E+004 234.23 7.35E+003 F 5 530- 552 544.41 136.36 1. 73E+003 111.00 4. 42E+003 F 6 652- 681 662.20 165.79 1. 38E+004 226.61 4.74E+003 F 7 1014- 1029 1019.99 255.20 4.06E+002 76.35 1. 95E+003 F 8 1104- 1131 1115.67 279.10 4.96E+003 143.50 2.92E+003 F 9 1551- 1585 1565.91 391.61 1. 07E+004 198.65 2. 66E+003 F 10 2623- 2671 2646.03 661.51 1. 17E+004 207.34 2. 60E+003 F 11 3577- 3618 3592.01 897.90 1. 15E+004 206.13 1.74E+003 12 4667- 4722 4693.31 1173.09 1.24E+004 211.48 9. 64E+002 M 13 5288- 5357 5300.71 1324.87 1.81E+002 38.32 3.49E+002 m 14 5288- 5357 5330.79 1332.39 1.11E+004 199.34 4.30E+002 F 15 7320- 7371 7346.48 1836.07 7.27E+003 162.07 2. 03E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 1/21/03 12:51:38 PM Page 4 

   *****    N U C L I D E    I D E N T I F I C A T IO       N   R E PO R T    *****

Sample I.D. C:\GENIE2K\CAMFILES\QC 120602.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/ea ) Uncertainty CO-57 0.999 122.06* 85.51 1.559E-002 9.336E-004 136.48* 10.60 1.479E-002 1.344E-003 CO-60 0.999 1173.22* 100.00 4.635E-002 2.679E-003 1332.49* 100.00 4.608E-002 2.823E-003 Y-88 0.999 898.02* 93.40 3.645E-002 1.954E-003 1836.01* 99.38 3.832E-002 3.391E-003 CD-109 0.999 88.03* 3.72 8.113E-001 7.928E-002 SN-113 1.000 255.12* 1.93 2.386E-002 5.302E-003 391.69* 64. 90 2.517E-002 1.580E-003 CS-137 0.999 661.65* 85.12 -3.159E-002 1.960E-003 CE-139 1.000 165.85* 80.35 -1.582E-002 9.708E-004 HG-203 0.999 279.19* 77.30 7.728E-003 5.271E-004 AM-241 0.999 59.54* 35.90 7.489E-002 8.241E-003 

            * = Energy line found in the spectrum.
            @ = Energy line not used for Weighted Mean Activity Energy tolerance used was      1.500 Nuclide confidence index threshold =        0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 1/21/03 12:51:38 PM Page 5 

   ***        I N T E R F E R E N C E                      C O R R E C T E D                R E P O R T             ***

Sample I.D. C:\GENIE2K\CAMFILES\QC 120602.CNF Spectrum Number QC12002.CNF Performed & Reviewed By ___ Date _7_ Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 0.999 1.53E-002 7. 67E-004 5.0 CO-60 0.999 4. 62E-002 1.94E-003 4.2 Y-88 0.999 3. 69E-002 1.69E-003 4.6 CD-109 0.999 8.11E-001 7. 93E-002 9.8 SN-113 1. 000 2.51E-002 1. 51E-003 6.0 CS-137 0 . 999 3. 16E-002 1.96E-003 6.2 CE-139 1.000 1.58E-002 9.71E-004 6.1 HG-203 0. 999 7.73E-003 5.27E-004 6.8 AM-241 0.999 7.49E-002 8.24E-003 11.0 

        ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
        @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at               1.96 sigma

Interference Corrected Activity Report 1/21/03 12:51:38 PM Page 6 

       **********   U N I D E N T I F I E D    P E A K S
  • Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.31 9.3766E-001 11.56 M 13 1324.87 3.0242E-001 21.12 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

1 ( It  :' ` , :31 .z, k - 

                                                                                                                                                   % I           76,;.     .     .
p.  %. . .

C N .- C Date: 12-06-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics SIN 64091-466 Duratek# 080201 A_ 

                                                                     -1.11      -             ....-.... :'_

Source Activity on Count Date: '. Total Source Activity Activity Isotope Energy Yield Activity Activity Uncertainty Current Original Activity Isotope Y/2 life (k) (%) (uCi) (uCI)_4._,  % difference Am-241 59.5 7.495E-02 0.14 Cd-109 88 1.027E+00 -1.78 Co-57 122 2.292E-02 -4.55 Ce-139 166 3.501E-02 -4.16 Hg-203 279 8.107E-02 -1.67 Sn-113 392 6.500E-02 -2.45 Cs-137 662 3.192E-02 -0.38 Y-88 898 1.031E-01 -3.82 Co-60 1173 4.890E-02 0.58 Co-60 1332 4.890E-02 -0.63 Y-88 1836 1.031E-01 -2.13 I I

1. Source quantification following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from wRadioactive Decay Data Tables" D.C. Kocher
3. Activity % difference = (Original Activity - Certified Activity) / Certified Activity*l100

G A M M A S P E C T R U M A N A L Y S I S Report Generated On 12/5/02 10:32:21 AM Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120502A.CNF Spectrum Number QC120502A.CNF Sample Description Mixed Gamma in 250ml Sample Type Marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in charinels) 100 - 8192 Peak Area Range (in channesls) 100 - 8192 Identification Energy Tolesrance 1.50 keV Sample Size 1.OOOE+000 ea Sample Collection Date Spectrum Collection Date 12/5/02 10:17:04 AM Decay Corrected To Collected By L. Finn Live Time 600.0 seconds Real Time 616.6 seconds 

   % Dead Time                           2.70 %

't/ Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed ByeB' Date ..Lj5-1/vZ0 Supervisory Review 2! 2 4 014-z::: Date /22 / 5 /69

Peak Locate Analysis Report 12/5/02 10:32:21 AM Page 2 

           ******           PE AK             L OC A TE            RE PO RT                                   ***

Detector DETO1 Sample I.D. C:\GENIE2K\CAMFILES\QC 120502A.CNF Spectrum Number QC120502A.CNF Sample Description Mixed Gamma in 250ml Sample Type Marinelli Peak Locate Performed on 12/5/02 10:32:20 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.10 0.1938 42.40 9.91 0.8441 2 236.18 0.0955 59.34 33.77 1.1653 3 350.23 0.0638 87.86 73.70 1.1865 4 486.53 0. 0699 121.90 57.38 1.1794 5 544.32 0.1256 136.34 17.30 1. 1220 

              .6       661.91           0.0663          165.72               62.66                 1.2227 7     1019.03           0. 1856         254.94                 6.74                1.3252 8     1115.47           0.0794          279.06               37.15                 1.3116 9     1565.66           0. 0607         391.56               59.74                 1. 4456
  'V          10      2645.86           0. 0543         661.49               63.53                 1.7395 11      3591.98           0. 0524         897.91               60.34                 1. 9951 12      4693.31           0. 04 93       1173.10               61.09                 2.2829 13      5300.57            0.1614        1325.00                 4.89                2. 4 620 14      5330.82           0. 04 97       1332.39               57.15                 2. 4668 15      7346.71           0. 0533        1836.13               42.80                 2. 9139 Errors quoted at       1. 96 stigma

Peak Analysis Report 12/5/02 10:32:21 AM Page 3 P E A K A N A L Y S I S R E P O R T ' V ******************************************* Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120502A.CNF Spectrum Number QC120502A.CNF Sample Description Mixed Gamma in 250ml Peak Analysis Performed on 12/5/02 10:32:21 AM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 176 168.40 42.40 7.75E+002 66. 60 1.33E+003 F 2 225- 251 236.17 59.34 6.81E+003 175.77 6.86E+003 F 3 333- 367 350.31 87.86 2.40E+004 301.02 1.03E+004 F 4 468- 504 486.57 121.90 1.41E+004 235.73 8.31E+003 F 5 538- 551 544.34 136.34 1.66E+003 110.63 2.83E+003 F 6 651- 681 661.91 165.72 1.37E+004 230.16 5.07E+003 F 7 1011- 1025 1018.96 254.94 4.32E+002 75.81 1.78E+003 F 8 1105- 1124 1115.49 279.06 4.68E+003 142.71 2.23E+003 F 9 1554- 1585 1565.71 391.56 1.07E+004 200.80 2.38E+003 F 10 2626- 2664 2645.94 661.49 1.18E+004 209.57 2.01E+003 F 11 3543- 3615 3592.05 897.91 1. 16E+004 207.04 2.94E+003 F 12 4669- 4723 4693.33 1173.10 1.24E+004 212.69 9.91E+002 M 13 5288- 5359 5301.23 1325.00 2.74E+002 40.22 2.85E+002 m 14 5288- 5359 5330.80 1332.39 1.11E+004 200.41 3.29E+002 F 15 7322- 7369 7346.73 1836.13 7.15E+003 161.43 1. 92E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/5/02 10:32:21 AM Page 4 

   *****    N U C L I D E    I D E N T I F I C A T IO N       R E P O R T    *****

Sample I.D. C:\GENIE2K\CAMFILES\QC 120502A.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB IDENTIFIED NUCLIDES ..................... Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/ea ) Uncertainty CO-57 0.998 122.06* 85.51 1.527E-002 9.167E-004 136.48* 10.60 1. 418E-002 1.315E-003 CO-60 0.999 1173.22* 100.00 4.640E-002 2.682E-003 1332.49* 100.00 4.630E-002 2.837E-003 Y-88 0.999 898.02* 93.40 3.675E-002 1.970E-003 1836.01* 99.38 3.772E-002 3.340E-003 CD-109 0.998 88.03* 3.72 8.191E-001 8.008E-002 SN-113 0.999 255.12* 1.93 2.540E-002 5.373E-003 391.69* 64.90 2.511E-002 1.578E-003 CS-137 0.998 661.65* 85.12 3.179E-002 1.972E-003 CE-139 0.999 165.85* 80.35 1..571E-002 9.656E-004 HG-203 0.999 279.19* 77.30 7.278E-003 5.016E-004 AM-241 0.997 59.54* 35.90 7.464E-002 8.255E-003 

            * = Energy line found in the spectrum.

Q = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.500 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 12/5/02 10:32:21 AM Page 5 

   ***     I N T E R F E R E N C E     C O R R E C T E D    R E P O R T         ***

Sample I.D. C:\GENIE2K\CAMFILES\QC 120502A.CNF Spectrum Number QC120502A.CNF Performed & Reviewed By Date 6'/ V,/ O;> Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 0.998 1.49E-002 7.52E-004 5.0 CO-60 0. 999 4. 64E-002 1.95E-003 4.2 

     -Y-88         0.999        3.70E-002      1.70E-003          4. 6 CD-109       0.998        8.19E-001      8. 01E-002         9.8 SN-113       0. 999       2.51E-002      1. 51E-003         6.0 CS-137       0.998        3.18E-002      1.97E-003          6.2 CE-139       0. 999       1. 57E-002     9.66E-004          6.1 HG-203       0. 999       7.28E-003      5.02E-004          6.9 AM-241       0.997        7.46E-002      8.25E-003         11.1
       ? - nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
      @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at    1.96 sigma

Interference Corrected Activity Report 12/5/02 10:32:21 AM Page 6 

       **********   U N I D E N T I F I E D    P E A K S Peak   Energy            Peak Size in         Peak CPS No.    (keV)          Counts per Second   % Uncertainty F   1    42.40              1.2916E+000            8.59 M 13  1325.00              4.5586E-001           14.70 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at   1.96 sigma

       *****GA                       MM A           S PE CT R UM                 A NAL   Y SI S***

Report Generated On 12/4/02 7:36:10 AM Detector DET01 Sample I.D. C:\GE]gIE2K\CAMFILES\QC 120402..CNF Spectrum Number QC120402.CNF Sample Description Mixed Gamma in 250ml marinelli Sample Type marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.00 keV Sample Size 1.OOOE+000 ea Sample Collection Date Spectrum Collection Date 12/4/02 6:51:44 AM Decay Corrected To Collected By P. Jones Live Time 600.6 seconds Real Time 617.3 seconds 

      % Dead Time                                                            2.70 %

lV Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed By _, . . Date X1/ 5A/.Q do Supervisory Review Supevisoy ReiewDate Date _ / .5( 5 lo-a t'-

Peak Locate Analysis Report 12/4/02 7:36:10 AM Page 2 P E A K L O C A T E R E P O R T Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120402.'.CNF Spectrum Number QC120402.CNF Sample Description Mixed Gamma in 250ml marinelli Sample Type marinelli Peak Locate Performed on 12/4/02 7:36:10 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.17 0.1911 42.32 9.52 0. 8000 2 235.93 0.0945 59.26 35.15 1.1330 3 289.43 0.2926 72.59 4.24 0. 4750 4 350.05 0.0636 87.81 73.86 1. 1495 5 486.22 0.0702 121.85 58.93 1. 1803 6 544.04 0. 1232 136.27 18.69 1.1276 7 661.54 0.0655 165.65 60.21 1.2472 8 1019.28 0.1817 255.04 7.54 1.2541 9 1115.17 0.0785 278.98 39.70 1.2710 10 1565.30 0.0600 391.48 60.97 1. 4639 11 2645.42 0.0542 661.38 62.37 1. 7440 12 3591.31 0.0523 897.74 60.88 2. 0053 13 4692.62 0.04 92 1172.93 61.55 2.2510 14 5299.51 0.1730 1324.69 3.79 2. 4169 15 5329.92 0.0495 1332.20 57.52 2. 4217 16 7345.82 0.0529 1835.93 43.15 2. 8893 Errors quoted at 1.96 sigma

Peak Analysis Report 12/4/02 7:36:10 AM Page 3

                                                                                                                                                • I**
       *****                 P EAK                A NAL         Y SI S           RE P OR T***

Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 120402..CNF Spectrum Number QC120402.CNF Sample Description Mixed Gamma in 250ml marinelli Peak Analysis Performed on 12/4/02 7:36:10 AM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 175 168.10 42.32 7.02E+002 64.21 1.18E+003 F 2 222- 246 235.89 59.26 6.70E+003 175.50 6.64E+003 F 3 285- 293 289.21 72.59 1. 47E+002 80.16 2.92E+003 F 4 340- 366 350.12 87.81 2.31E+004 298.91 8.33E+003 F 5 474- 504 486.35 121.85 1.40E+004 235.80 6.92E+003 F 6 537- 552 544.06 136.27 1.80E+003 111.61 3.08E+003 F 7 644- 681 661.65 165.65 1.42E+004 233.08 6.23E+003 F 8 1012- 1027 1019.36 255.04 4.60E+002 76.32 1.91E+003 F 9 1104- 1124 1115.15 278.98 4.72E+003 144.29 2.36E+003 F 10 1544- 1588 1565.36 391.48 1.llE+004 203.92 3. 06E+003 F 11 2631- 2672 2645.51 661.38 1.18E+004 209.20 2.24E+003 12 3567- 3618 3591.37 897.74 1.17E+004 208.03 1. 93E+003 F 13 4669- 4718 4692.68 1172.93 1.23E+004 212.06 8. 97E+002 M 14 5283- 5357 5300.01 1324.69 2.31E+002 38.27 3.24E+002 m 15 5283- 5357 5330.04 1332.20 1. 11E+004 200.59 3.27E+002 F 16 7322- 7371 7345.92 1835.93 7.28E+003 162.99 1.97E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/4/02 7:36:10 AM Page 4 

   *****            N U C L I D E        I D E N T I F I C A T IO N                         R E P O R T         *****

Sample I.D. C:\GENIE2K\CAMFILES\QC 120402..CNF 

     -       Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB IDENTIFIED NUCLIDES Nuclide               Id      Energy        Yield          Activity              Activity Name             Confidence   (keV)            (%)        (uCi/ea               Uncertainty CO-57                0.993   122.06*        85.51       1.520E-002             9.128E-004 136.48*        10.60       1.537E-002             1.375E-003 CO-60                0.987  1173.22*      100.00        4.593E-002             2.656E-003 1332.49*      100.00        4.608E-002             2.825E-003 Y-8 8                0.993   898.02*        93.40       3.722E-002             1.993E-003 1836.01*        99.38       3.838E-002             3.395E-003 CD-109               0.992    88.03*          3.72      7.869E-001             7.699E-002 SN-113               0.993   255.12*          1.93      2.703E-002             5.505E-003 391.69*        64.90       2.623E-002             1.644E-003 CS-137               0.989   661.65*        85.12       3.182E-002             1.974E-003 CE-139               0.994   165.85*        80.35       1.627E-002             9.982E-004 HG-203               0.993   279.19*        77.30       7.344E-003             5.062E-004 AM-241               0.988    59.54*        35.90       7.373E-002             8.196E-003
                    * = Energy line found in the spectrur Tn.
                    @ = Energy line not used for Weighte I Mean Activity Energy tolerance used was                1.000 Nuclide confidence index threshold =                          0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 12/4/02 7:36:10 AM Page 5 

   ***     I N T E R F E R E N C E     C O R R E C T E D     R E P O R T     ***

Sample I.D. C:\GENIE2K\CAMFILES\QC 120402..CNF Spectrum Number QC120402.CNF Performed & Reviewed By all$ C05%. , Date _ Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 0.993 1.53E-002 7.60E-004 5.0 CO-60 0.987 4. 60E-002 1. 94E-003 4.2 Y-88 0.993 3.75E-002 1.72E-003 4.6 CD-109 0.992 7.87E-001 7.70E-002 9.8 SN-113 0.993 2. 63E-002 1.58E-003 6.0 CS-137 0.989 3.18E-002 1.97E-003 6.2 CE-139 0.994 1. 63E-002 9.98E-004 6.1 HG-203 0.993 7.34E-003 5.06E-004 6.9 AM-241 0.988 7.37E-002 8.20E-003 11.1 

      ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
      @ = nuclide contains energy lines not used in Weighted Mean Activity N@     Errors quoted at   1.96 sigma

Interference Corrected Activity Report 12/4/02 7:36:10 AM Page 6 U N I D E N T I F I E D P E A K S Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.32 1.1688E+000 9.15 F 3 72.59 2.4415E-001 54.66 M 14 1324.69 3.8491E-001 16.55 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma 

        *****GA                       MM A           S PE C TR UM               A NA   LY SI S***

Report Generated On 12/3/02 6:17:57 PM Detector DET01 Sample I.D. DET01 Spectrum Number QC120302.CNF Sample Description Mixed Gamma in 250ml marinelli Sample Type marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak-Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.00 keV Sample Size 1.OOOE+000 ea Sample Collection Date Spectrum Collection Date 12/3/02 5:40:41 PM Decay Corrected To Collected By P. Jones Live Time 600.6 seconds Real Time 617.5 seconds 

       % Dead Time                                                          2.73 %

i wBackground Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed By Date _~ / 3 / da-Supervisory Review SesytRo Dt Date /C/g2

Peak Locate Analysis Report 12/3/02 6:17:57 PM Page 2 P E A K L O C A T E R E PO R T Detector DET01 Sample I.D. DET01 Spectrum Number QC120302.CNF Sample Description Mixed Gamma in 250ml marinelli Sample Type marinelli Peak Locate Performed on 12/3/02 6:17:37 PM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.53 0.1912 42.18 9.57 0. 6063 2 236.68 0.0968 59.44 33.37 1. 1747 3 290.27 0.3021 72.90 4.37 0. 3374 4 350.78 0.0640 87.97 73.01 1. 1770 5 487.00 0.0696 122.03 60.11 1. 1966 6 544.59 0.1247 136.42 18.74 1.0622 7 662.24 0.0659 165.83 61.11 1.2350 8 1019.53 0.1980 255.10 6.13 1.2749 9 1115.80 0. 0776 279.16 40.23 1.2940 10 1565.99 0.0596 391.65 61.35 1. 4515 11 2329.93 0.2239 582.53 4.30 1.2856 12 2646.05 0.0542 661.53 63.26 1. 7325 13 3256.32 0.2200 814.03 3.69 2.1298 14 3591.89 0.0516 897.88 62.69 1. 9468 15 4693.23 0.0491 1173.08 62.84 2.2115 16 5299.23 0. 1797 1324.75 4.05 2. 3782 17 5330.56 0.0492 1332.36 58.40 2.3832 18 5844.45 0.1823 1460.75 4.81 1. 6900 19 7346.41 0.0519 1836.05 46.17 2. 8327 Errors quoted at 1.96 sigma

Peak Analysis Report 12/3/02 6:17:57 PM Page 3 P E A K A N A L Y S I S R E P O R T Detector DET01 Sample I.D. DET01 Spectrum Number QC120302.CNF Sample Description Mixed Gamma in 250ml marinelli Peak Analysis Performed on 12/3/02 6:17:56 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 171 167.52 42.18 4.52E+002 62.26 7. 94E+002 F 2 221- 248 236.61 59.44 6.73E+003 174.61 7.20E+003 F 3 284- 294 290.46 72.90 1. 47E+002 118.62 3.80E+003 F 4 334- 367 350.78 87.97 2.38E+004 301.70 1.08E+004 F 5 472- 505 487.07 122.03 1.44E+004 237.60 7.39E+003 F 6 537- 557 544.65 136.42 1.68E+003 109.19 3.94E+003 F 7 653- 681 662.35 165.83 1. 39E+004 232.48 4.96E+003 F 8 1014- 1029 1019.61 255.10 3.68E+002 75.84 1.97E+003 F 9 1108- 1129 1115.88 279.16 4. 99E+003 146.37 2.39E+003 F 10 1552- 1588 1566.07 391.65 1. 11E+004 204.52 2.64E+003 F 11 2324- 2338 2329.93 582.53 1.27E+002 50.31 7.20E+002 F 12 2624- 2669 2646.10 661.53 1.18E+004 210.05 2.51E+003 F 13 3248- 3269 3256.39 814.03 1. 65E+002 50.16 7.70E+002 F 14 3573- 3619 3591.93 897.88 1. 18E+004 209.08 1.72E+003 F 15 4671- 4721 4693.25 1173.08 1.21E+004 211.39 9. 87E+002 M 16 5288- 5359 5300.22 1324.75 1. 94E+002 37.75 3.14E+002 m 17 5288- 5359 5330.68 1332.36 1.13E+004 202.84 3.53E+002 F 18 5836- 5855 5844.48 1460.75 9.37E+001 32.01 2.08E+002 F 19 7323- 7371 7346.41 1836.05 7. 45E+003 165.25 1.42E+002 First peak in a multiplet region m = Other peak in ia multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/3/02 6:17:57 PM Page 4 

   *****    N U C L I D E    I D E N T I F I C A T IO N        R E P O R T   *****

Sample I.D. DET01 Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB 

        ....................    . IDENTIFIED
                                  ..          NUCLIDES      .....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/ea ) Uncertainty CO-57 1.000 122.06* 85.51 1.560E-002 9.349E-004 136.48* 10.60 1.434E-002 1.313E-003 CO-60 0.997 1173.22* 100.00 4.528E-002 2. 622E-003 1332.49* 100.00 4.688E-002 2.872E-003 Y-88 0.998 898.02* 93.40 3.748E-002 2.006E-003 1836.01* 99.38 3.926E-002 3.472E-003 CD-109 0.999 88.03* 3. 72 8.101E-001 7.917E-002 SN-113 1.000 255.12* 1.93 2.159E-002 5.134E-003 391.69* 64.90 2. 621E-002 1.643E-003 CS-137 0.998 661.65* 85.12 3.175E-002 1.971E-003 CE-139 1.000 165.85* 80.35 1.599E-002 9.821E-004 HG-203 1.000 279.19* 77.30 7.760E-003 5.307E-004 AM-241 0.999 59.54* 35.90 7.308E-002 8.033E-003 

            * = Energy line found in the spectrurm.
            @ = Energy line not used for Weighte(i Mean Activity Energy tolerance used was     1.000 Nuclide confidence index threshold =       0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 12/3/02 6:17:57 PM Page 5 

   ***     I N T E R F E R E N C E   C O R R E C T E D      R E PO R T        ***

Sample I.D. DET01 Spectrum Number QC120302.CNF Performed & Reviewed By z2 O C2 Date i9/ 3 / t D_ Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 1.000 1.52E-002 7. 61E-004 5.0 CO-60 0.997 4.60E-002 1.94E-003 4.2 Y-88 0.998 3.79E-002 1.74E-003 4.6 CD-109 0. 999 8.1OE-001 7.92E-002 9.8 SN-113 1.000 2.58E-002 1.56E-003 6.1 CS-137 0.998 3.18E-002 1. 97E-003 6.2 CE-139 1.000 1.60E-002 9.82E-004 6.1 HG-203 1.000 7.76E-003 5.31E-004 6.8 AM-241 0.999 7.31E-002 8.03E-003 11.0 

      ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
      @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   1.96 sigma

Interference Corrected Activity Report 12/3/02 6:17:57 PM Page 6 U N I D E N T I F I E D P E A K S *** Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.18 7.5203E-001 13.78 F 3 72.90 2.4556E-001 80.42 F 11 582.53 2.1186E-001 39.54 F 13 814.03 2.7421E-001 30.46 M 16 1324.75 3.2364E-001 19.42 F 18 1460.75 1.5600E-001 34. 16 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet ErrQrs quoted at 1.96 sigma

G A M M A S P E C T R U M A N A L Y S I S 

  <W                                                                                 * * **  **************

Report Generated On 11/26/02 8:57:42 AM Detector DET01 Sample I.D. C:\GEIgIE2K\CAMFILES\QC 112602.CNF Spectrum Number QC112602.CNF 

  -Sample Description                                              Mixed Gamma in 250ml Marinelli Sample Type                                                     Marinelli Sample Geometry                                                 2 Peak Locate Threshold                                           3.50 Peak Locate Range (in channels)                                 100 -   8192 Peak Area Range (in channels)                                   100 -   8192 Identification Energy Tolerance                                 1.00 keV Sample Size                                                    1.OOOE+000 ea Sample Collection Date Spectrum Collection Date                                       11/26/02   8:38:54 AM Decay Corrected To Collected By                                                   L. Finn Live Time                                                         600.0 seconds Real Time                                                         617.1 seconds
   % Dead Time                                                     2.77 %
 "'BackgroundType                                                  STEP Energy Calibration Performed On                           11/13/02 Efficiency Calibration Performed On                       11/13/02 Calibration Geometry Used                                2 Performed & Reviewed By                                                          Date      __ /              _.?

_6 Supervisory Review Suerior eve Dat Date ZA}/ /kJ? 

                                                                                           .-. _ °

Peak Locate Analysis Report 11/26/02 8:57:42 AM Page 2 P E A K L O C A T E R E P O R T Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 112602.CNF Spectrum Number QC112602.CNF Sample Description Mixed Gamma in 250ml Marinelli Sample Type Marinelli Peak Locate Performed on 11/26/02 8:57:41 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 167.82 0.1926 42.06 10.05 0.4835 2 236.50 -0. 0986 59.42 32.21 1. 1743 3 350.65 0.0639 87.94 73.77 1. 1684 4 486.87 0.0698 121.99 59.16 1.1906 5 544.74 0.1294 136.44 16.60 1.2064 6 662.07 0.0653 165.79 63.92 1.2370 7 953.18 0.2683 238.50 4. 17 0.8611 8 1019.24 0.1938 255.02 5.48 1.7176 9 1115.53 0.0755 279.10 41.31 1.3119 10 1565.77 0.0597 391.60 61.61 1.4575 11 2645.75 0.0544 661.47 63.12 1.7362 12 3591.60 0.0516 897.80 62.22 1.9757 13 4692.86 0. 0497 1172.99 60.55 2.2664 14 5299.88 0.1659 1324.75 4.83 2.4616 15 5330.23 0.04 96 1332.26 56.98 2. 4664 16 7345.75 0.0531 1835.91 42.29 2. 9504 Errors quoted at 1.96 sigma

Peak Analysis Report 11/26/02 8:57:42 AM Page 3 P E A K A N A L Y S I S R E PO R T h .************************************************************************** Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 112602.CNF Spectrum Number QC112602.CNF Sample Description Mixed Gamma in 250ml Marinelli Peak Analysis Perfoormed on 11/26/02 8:57:41 AM Peak Analysis From Channel 100 Peak Analysis To C].iannel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 170 167.02 42.06 3.72E+002 57.41 6.81E+002 F 2 224- 251 236.50 59.42 6.66E+003 174.76 7. 41E+003 F 3 333- 367 350.66 87.94 2.40E+004 302.94 1. 09E+004 F 4 474- 505 486.93 121.99 1.43E+004 238.17 7.31E+003 F 5 534- 556 544.74 136.44 1.77E+003 111.61 4.50E+003 F 6 652- 681 662.18 165.79 1.47E+004 237.45 4.89E+003 F 7 949- 958 953.16 238.50 1.29E+002 68.34 1.37E+003 F 8 1004- 1028 1019.28 255.02 5.80E+002 81.01 2.90E+003 F 9 1101- 1129 1115.63 279.10 5.60E+003 152.69 3.05E+003 F 10 1551- 1590 1565.87 391.60 1.13E+004 205.91 2.89E+003 ('V)F 11 2624- 2668 2645.84 661.47 1. 16E+004 208.76 2.41E+003 F 12 3570- 3614 3591.62 897.80 1.21E+004 212.33 1.80E+003 F 13 4671- 4713 4692.91 1172.99 1. 21E+004 210.93 9.95E+002 M 14 5285- 5357 5300.25 1324.75 2. 44E+002 40.28 3.60E+002 m 15 5285- 5357 5330.28 1332.26 1.13E+004 201.74 3.78E+002 F 16 7323- 7372 7345.86 1835.91 7.45E+003 164.44 1.94E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1. 96 sigma

Interference Corrected Activity Report 11/26/02 8:57:42 AM Page 4 

   *****    N U C L I D E    I D E N T I F I C A T IO N        R E PO R T    *****

Sample I.D. C:\GENIE2K\CAMFILES\QC 112602.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB 

        ....................       IDENTIFIED NUCLIDES Nuclide     Id        Energy      Yield    Activity     Activity Name     Confidence    (keV)       (%)    (uCi/ea )    Uncertainty CO-57      0.999     122.06*      85.51 1.555E-002    9.323E-004 136. 48*     10.60 1.515E-002    1.365E-003 CO-60      0.992    1173.22*     100.00 4.521E-002    2.618E-003 1332.49*     100.00 4.684E-002    2.869E-003 Y-88       0.995     898.02*      93.40 3.863E-002    2.065E-003 1836.01*      99.38 3.927E-002    3.471E-003 CD-109     0.999      88.03*       3.72 8.188E-001    8.003E-002 SN-113     0.999     255.12*       1.93 3.409E-002    6.239E-003 391.69*      64.90 2.660E-002    1.667E-003 CS-137     0.995     661.65*      85.12 3.143E-002    1.952E-003 CE-139     0.999     165.85*      80.35 1. 691E-002   1.036E-003 HG-203     0.999     279.19*      77.30 8.720E-003    5.888E-004 AM-241     0.998      59.54*      35.90 7.248E-002    7.985E-003
            * = Energy line found in the spectrum.
            @ = Energy line not used for Weighted Mean Activity Energy tolerance used was      1.000 Nuclide confidence index threshold =       0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/26/02 8:57:42 AM Page 5 

.  ***            I N T E R F E R E N C E                               C O R R E C T E D
    **********************************************************************                             R E P O R T              ***

Sample I.D. C:\GENIE2K\CAMF.ILES\QC 112602.CNF Spectrum Number QC112602.CNF Performed & Reviewed By , _ Date 1/ /1(24a/i2Z Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ea ) Uncertainty  % Uncertainty CO-57 0.999 1.54E-002 7.70E-004 5.0 CO-60 0.992 4. 60E-002 1.93E-003 4.2 Y-88 0.995 3. 88E-002 1. 77E-003 4.6 CD-109 0. 999 8.19E-001 8. OOE-002 9.8 SN-113 0. 999 2.71E-002 1.61E-003 5.-9 CS-137 0.995 3.14E-002 1. 95E-003 6.2 CE-139 0. 999 1. 69E-002 1.04E-003 6.1 HG-203 0. 999 8.72E-003 5.89E-004 6.8 AM-241 0.998 7.25E-002 7. 98E-003 11.0 

         ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
         @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                      1.96 sigma

Interference Corrected Activity Report 11/26/02 8:57:42 AM Page 6 U N I D E N T I F I E D P E A K S Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.06 6.2016E-001 15.43 F 7 238.50 2.1574E-001 52.79 M 14 1324.75 4.0689E-001 16.50 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

t t II- ( Date: 11- 25-02 250 ml Marinenli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S/N 64091-466 Duratek# 080201 CEA..- A AA&z.*;*%S A_ .......... I........ I-..- . - . ........ ................ ouuiru /ActIIvity Un ':", B2UiN.. Count Date: Total Source Activity Activity Isotope Energy Yield Activity Activity Uncertainty Current Original Activity ckeV) (gamldis.) M (ucin (uCi)  % difference Am-241 59.5 0.359 7.315E-02 -2.27 Cd- 109 88 0.0372 1.018E+00 -2.66 Co-57 122 0.8551 2.287E-02 -4.77 Ce-139 186 0.8035 3.522E-02 -3.59 Hg-203 279 0.773 7.934E-02 -3.77 Sn-113 392 0.o49 6.592E-02 -1.06 Cs-137 662 0.8512 3.280E-02 2.39 Y-88 898 0.934 1.025E-01 -4.39 Co-60 1173 0 4.818E-02 -0.90 Co-60 1332 4.818E-02 -2.10 Y-88 1836 0.9938 1.025E-01 -2.71 I I

1. Source quantification following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from *Radioactive Decay Data Tables" D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*1 00

G A M M A S P E C T R U M A N A L Y S~I S Report Generated On 11/25/02 7:41:16 AM Detector DET01 Sample I.D. C:\GE NIE2K\CAMFILES\QC 112502.CNF Spectrum Number QC112502.CNF Sample Description MixedGamma in 250ml Marinelli Sample Type Marinelli Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.00 keV Sample Size 1.OOOE+000 ea Sample Collection Date Spectrum Collection Date 11/25/02 7:28:33 AM Decay Corrected To Collected By L. Finn Live Time 600.0 seconds Real Time 617.1 seconds k)% Dead Time 2.78 % Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed By Date // /.75/O2. Supervisory Review Supervisory Review Dat Date {//o/ 1M

Peak Locate Analysis Report 11/25/02 7:41:16 AM Page 2 P E A K L O C A T E R E P O R T Detector DETOI Sample I.D. C:\GENIE2K\CAMFILES\QC 112502.CNF Spectrum Number QC112502.CNF Sample Description MixedGamma in 250ml Marinelli Sample Type Marinelli Peak Locate Performed on 11/25/02 7:41:15 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 168.29 0.1819 42.24 10.19 0.6879 2 236.60 0.0973 59.45 32.03 1.1634 3 350.69 0. 0638 87.96 73.81 1.1759 4 486.91 0.0694 122.00 60.31 1.18 67 5 544.83 0. 1276 136.. 45 17.02 1.1933 6 662.25 0. 0655 165.82 62.26 1.2522 7 953.82 0.2528 238.60 4.60 0. 7317 8 1019.58 0. 1790 255.12 7.65 1.2577 1 9 1115.73 0. 0761 279.15 41.06 1.3600 10 1566.00 0. 0592 391.64 63.10 1. 4560 11 2646.09 0.0540 661.55 64.04 1.7428 12 3256.72 0.2163 814.05 4.21 1.1926 13 3592.11 0. 0517 897.94 61.98 2. 0113 14 4693.41 0. 0494 1173.14 60.18 2.2477 15 5300.24 0. 1931 1324.81 4.49 2. 4187 16 5330.94 0. 0498 1332.43 56.23 2. 4235 17 7346.77 0.0526 1836.14 43.50 2. 9416 Errors quoted at 1.96 sigma

Peak Analysis Report 11/25/02 7:41:16 AM Page 3 P E A K A N A L Y S I S R E P O R T V ************************************** Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 112502.CNF Spectrum Number QC112502.CNF Sample Description MixedGamma in 250ml Marinelli Peak Analysis Performed on 11/25/02 7:41:15 AM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 172 167.74 42.24 6.16E+002 65.98 9.10E+002 F 2 223- 249 236.62 59.45 6.73E+003 175.60 7.19E+003 F 3 333- 367 350.72 87.96 2.40E+004 301.54 1.05E+004 F 4 473- 501 486.93 122.00 1.46E+004 240.45 6.99E+003 F 5 533- 557 544.79 136.45 1.79E+003 111.84 4.89E+003 F 6 650- 681 662.32 165.82 1.46E+004 236.81 5.52E+003 F 7 949- 960 953.57 238.60 1. 38E+002 66.77 1.74E+003 F 8 1014- 1030 1019.69 255.12 4.76E+002 78.11 2.09E+003 F 9 1105- 1130 1115.85 279.15 5.72E+003 153.79 2.67E+003 F 10 1551- 1584 1566.03 391.64 1.15E+004 208.11 2. 60E+003 , V F 11 2626- 2668 2646.19 661.55 1.20E+004 211.02 2.28E+003 F 12 3250- 3265 3256.48 814.05 9.05E+001 44.31 5.88E+002 F 13 3573- 3618 3592.17 897.94 1.23E+004 213.57 1.95E+003 F 14 4 676- 4713 4693.49 1173.14 1.23E+004 212.25 7.82E+002 M 15 5289- 5357 5300.48 1324.81 1.57E+002 39.45 4.01E+002 m 16 528 9- 5357 5330.99 1332.43 1. 09E+004 199.97 4.67E+002 F 17 7322.- 7369 7346.76 1836.14 7.65E+003 166.56 1.76E+002 M = First peak in a multiplet region m = Other peak in a multiplet region F - Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/25/02 7:41:16 AM Page 4 

   *****    N U C L I D E    I D E N T I F I C A T IO N        R E P O R T   *****

Sample I.D. C:\GENIE2K\CAMFILES\QC 112502.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB 

        ....................    . IDENTIFIED
                                  ..          NUCLIDES       .....................

Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/ea ) Uncertainty CO-57 0.999 122.06* 85.51 1.581E-002 9.473E-004 136.48* 10.60 1.532E-002 1.374E-003 CO-60 0.999 1173.22* 100.00 4.588E-002 2.655E-003 1332.49* 100.00 4.555E-002 2.795E-003 Y-88 0.998 898.02* 93.40 3.913E-002 2.090E-003 1836.01* 99.38 4.033E-002 3.563E-003 CD-109 0.999 88.03* 3.72 8. 170E-001 7.984E-002 SN-113 1.000 255.12* 1.93 2.801E-002 5.662E-003 391.69* 64.90 2.716E-002 1.700E-003 CS-137 0.999 661.65* 85.12 3.246E-002 2.012E-003 CE-139 1.000 165.85* 80.35 1.678E-002 1.028E-003 HG-203 1.000 279.19* 77.30 8.906E-003 6.OOOE-004 AM-241 0.999 59.54* 35.90 7. 312E-002 8.039E-003 

            * = Energy line found in the spectrum.

Q = Energy line not used for Weighted Mean Activity Energy tolerance used was 1.000 Nuclide confidence index threshold = 0.10 Errors quoted at 1.960 sigma

Enterference Corrected Activity Report 11/25/02 7:41:16 AM Page 5 

  ' ***     I N T E R F E R E N C E       C O R R E C T E D     R E P O R T       ***

I Sp I*D**C*******E***C*****E***C*112502**CNF Sample I. D. C:\GENIE2K\CAMFILES\QC 112502.CNF Spectrum Number QC112502.CNF Performed & Reviewed By k, Ve, ~Date - 

                                                                      /1 / L5/V2S Nuclide          Wt mean        Wt mean          Wt mean Nuclide        Id            Activity       Activity         Activity Name       Confidence       (uCi/ea )      Uncertainty    % Uncertainty CO-57         0. 999       1. 57E-002      7. 80E-004            5.0 CO-60         0.999        4.57E-002       1.92E-003             4.2
       *Y        0.998        3.94E-002       1. 80E-003            4.6 CD-109        0.999        8.17E-001       7.98E-002             9.8 SN-113        1.000        2.72E-002       1.63E-003             6.0 CS-137        0.999        3.25E-002       2.01E-003             6.2 CE-139        1.000        1.68E-002       1.03E-003             6.1 HG-203        1.000        8.91E-003       6.OOE-004             6.7 AM-241        0.999        7.31E-002       8.04E-003            11.0
        ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
       @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at     1.96 sigma

Interference Corrected Activity Report 11/25/02 7:41:16 AM Page 6 I** * *

  • U N I D E N T I F I E D P E A K S ***
   @   Peak   Energy            Peak Size in        Peak CPS No.    (keV)          Counts per Second   % Uncertainty F   1    42.24              1.0263E+000          10.71 F   7   238.60              2.3070E-001          48.24 F 12    814.05              1.5083E-001          48.97 M 15  1324.81              2.6110E-001          25.18 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at   1.96 sigma

C ( ' Date: 11-24-02 250 mL Marinelli Beaker Filled With Sand to Top Quantification check of ISOCS at Veterans Affairs Medical Center Mixed Gamma Standard source Analytics S/N 64091-466 Duratek# 080201 Source Activity on

  • 1iMtitw. I Count Date: Eg..M.

I . Total Source Activity Activity Isotope Energy Yield Activity Activity Uncertainty Current Original Activity (keV) (narn/dis.) oL' I Iau.hi1 (uCi) _  % difference I Am-241 59.5 0.359 7.265E-02 -2.94 Cd-109 88 0.0372 9.999E-01 -4.36 Co-57 122 0.8551 2.252E-02 -6.22 Ce-139 186 0.8035 3.54BE-02 -2.93 Hg-203 279 0.773 7.8962-02 -4.23 Sn-113 392 0.649 6.577E-02 -1.30 Cs-1 37 662 0.8512 3.199E-02 -0.14 Y-88 898 0.934 1.023E-01 -4.53 Co-6o 1173 1 4.869E-02 0.15 Co-6O 1332 1 4.869E-02 -1.06 Y-88 1836 0.9938 1.023E-01 -2.85 I I

1. Source quantificatlon following calibration on Nov. 13, 2002
2. Gamma ray yields obtained from Radioactive Decay Data Tables D.C. Kocher
3. Activity % difference = ( Original Activity - Certified Activity) / Certified Activity*1 00

G A M M A S P E C T R U M A N A L Y S I S i *********************************** Report-Generated On 11/24/02 8:05:06 AM Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 112402.CNF Spectrum Number QC Sample Description mixed gamma source in 250 mL mar Sample Type Source Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in channels) 100 - 8192 Peak Area Range (in channels) 100 - 8192 Identification Energy Tolerance 1.00 keV Sample Size 1.OOOE+000 unit Sample Collection Date Spectrum Collection Date 11/24/02 7:42:12 AM Decay Corrected To Collected By L. Finn Live Time 600.0 seconds Real Time 617.1 seconds 

    % Dead Time                                         2.78 %
 %Background            Type                            STEP Energy Calibration Performed On                 11/13/02 Efficiency Calibration Performed On             11/13/02 Calibration Geometry Used                       2 E

Performed & Reviewed By Su r RiL Date // / 242/ O47-Supervisory Review Date _/ /,7i/ O.P,

Peak Locate Analysis Report 11/24/02 8:05:06 AM Page 2 P E A K L O C A T E R E PO R T i i Detector DET01 Sample I.D. C:\GENIE2K\CAMFILtS\QC 112402.CNF Spectrum Number QC Sample Description mixed gamma source in 250 mL marine Sample Type Source Peak Locate Performed on 11/24/02 8:05:05 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 167.94 0.2026 42.14 *9.47 0. 5938 2 236.44 0.0961 59.39 33.82 1. 1382 3 350.47 0. 0646 87.91 70.68 1.1746 4 486.80 0.0697 121.96 59.31 1. 1783 5 544.37 0.1313 136.34 16.12 1.2521 6 662.03 0. 0654 165.77 64.24 1.2443 7 1019.18 0. 1775 255.07 8.12 1. 3606 8 1115.61 0. 0755 279.11 41.83 1. 3389 9 1565.81 0.0589 391.60 63.52 1.4277 10 2041.36 0.2407 510.30 3.53 1.6919 11 2645.92 0. 0543 661.51 63.31 1. 7373 12 3255.03 0.2114 813.70 4.25 1. 5320 13 3591.96 0.0512 897.91 63.13 1.9616 14 4693.32 0.0496 1173.10 60.39 2.2864 15 5299.47 0.1707 1324.79 5.12 2. 4543 16 5330.90 0.0496 1332.42 56.87 2. 4593 17 7346.67 0. 0528 1836.11 42.62 2. 9602 Errors quoted at 1.96 sigma

Peak Analysis Report 11/24/02 8:05:06 AM Page 3 

        ***P                      E A K      A N A L Y S I S        R E P O R T***

I ************************************* I, Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\QC 112402.CNF Spectrum Number QC Sample Description mixed gamma source in 250 mL marinelli Peak Analysis Performed on 11/24/02 8:05:05 AM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 164- 171 167.37 42.14 4. 48E+002 59.68 7.44E+002 F 2 220- 252 236.38 59.39 6.65E+003 173.86 8. 33E+003 F 3 334- 367 350.52 87.91 2.36E+004 300.39 1.07E+004 F 4 475- 504 486.79 121.96 1.43E+004 238.63 6. 90E+003 F 5 530- 553 544.35 136.34 1. 80E+003 112.40 4.75E+003 F 6 643- 679 662.13 165.77 1.48E+004 238.36 6.45E+003 F 7 1010- 1031 1019.47 255.07 5.57E+002 78.84 2. 61E+003 F 8 1104- 1134 1115.69 279.11 5.78E+003 154.09 3.13E+003 F 9 1543- 1581 1565.87 391.60 1.14E+004 207.54 2.92E+003 F 10 2025- 2047 2040.87 510.30 1. 66E+002 55.37 1.28E+003 F 11 2622- 2672 2646.01 661.51 1.17E+004 208.51 2. 68E+003 12 3246- 3264 3255.05 813.70 1.27E+002 49.68 7.53E+002 F 13 3572- 3618 3592.06 897.91 1.23E+004 214.07 1.91E+003 F 14 4668- 4717 4693.35 1173.10 1.22E+004 211.17 9.42E+002 M 15 5290- 5353 5300.40 1324.79 2. 15E+002 40.01 3.30E+002 m 16 5290- 5353 5330.94 1332.42 1. 12E+004 202.10 4.36E+002 F 17 7322- 7374 7346.67 1836.11 7.72E+003 166.92 1.71E+002 First peak in a multiplet region Other peak in a multiplet region Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/24/02 8:05:06 AM Page 4 

,  *****    N U C L I D E    I D E N T I F I C A T IO N      R E P O R T   *****

i ************************************************************************ Sample I.D. C:\GENIE2K\CAMFILES\QC 112402.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\CALIB.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/unit) Uncertainty CO-57 0.998 122.06* 85.51 1.557E-002 9.340E-004 136.48* 10.60 1.534E-002 1.379E-003 CO-60 0.999 1173.22* 100.00 4.570E-002 2.644E-003 1332.49* 100.00 4.678E-002 2.866E-003 Y-88 0.998 898.02* 93.40 3.920E-002 2.094E-003 1836.01* 99.38 4.068E-002 3.592E-003 CD-109 0.998 88.03* 3.72 8.041E-001 7.862E-002 SN-113 0.999 255.12* 1.93 3.274E-002 6.039E-003 391.69* 64.90 2.687E-002 1.683E-003 CS-137 0.997 661.65* 85.12 3.166E-002 1.964E-003 CE-139 0.999 165.85* 80.35 1.703E-002 1.043E-003 HG-203 0.999 279.19* 77.30 8.999E-003 6.055E-004 AM-241 0.996 59.54* 35.90 7.253E-002 8.004E-003 

            * = Energy line found in the spectrum.
            @ = Energy line not used for Weighted Mean Activity Energy tolerance used was    1.000 Nuclide confidence index threshold =     0.10 Errors quoted at 1.960 sigma

Enterference Corrected Activity Report 11/24/02 8:05:06 AM Page S 

 '1 ***     I N T E R F E R E N C E    C O R R E C T E D     R E PO R T      ***

_ Sample I.D. Sample I. D. C:\GENIE2K\CAMFILES\QC 112402.CNF Spectrum Number QC Performed & Reviewed By Ok , -- Date /_ / 5 / 7eL Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/unit) Uncertainty  % Uncertainty CO-57 0.998 1. 55E-002 7.73E-004 5.0 CO-60 0.999 4. 62E-002 1.94E-003 4.2 

      .Y-88         0.998       3.96E-002      1. 81E-003          4.6 CD-109       0.998       8.04E-001      7.86E-002           9.8 SN-113       0.999       2.73E-002      1. 62E-003          5.9 CS-137       0.997       3.17E-002      1.96E-003           6.2 CE-139       0.999       1.70E-002      1.04E-003           6.1 HG-203       0.999       9.OOE-003      6.05E-004           6.7 AM-241       0.996       7.25E-002      8.OOE-003          11.0
       ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
       @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at   1.96 sigma

Interference Corrected Activity Report 11/24/02 8:05:06 AM Page 6 U N I D E N T I F I E D P E A K S *** Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty F 1 42.14 7.4604E-001 13.33 F 10 510.30 2.7651E-001 33.38 F 12 813.70 2.1176E-001 39.10 M 15 1324.79 3.5794E-001 18.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

G A M M A S P E C T R U M A N A L Y S I S %W V *********************************** Report Generated On 12/4/02 5:36:44 PM Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\BKG120402.CNF Spectrum Number BKG120402.CNF Sample Description Bkg Check Sample Type Water Sample Geometry 2 Peak Locate Threshold 3.50 Peak Locate Range (in chan.nels) 100 - 8192 Peak Area Range (in channe!ls) 100 - 8192 Identification Energy Tole!rance 2.00 keV Sample Size 2.500E+002 ml Sample Collection Date 12/4/02 5:22:00 PM Spectrum Collection Date 12/4/02 5:22:41 PM Decay Corrected To 12/4/02 5:22:00 PM Collected By L. Finn Live Time 600.0 seconds Real Time 600.1 seconds 

     % Dead Time                               0.01 %

Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed By W. Date /.Z/' O/OZ. Supervisory Review SuperisoryRevie Date Date//,. / / _Z /0a5

Peak Locate Analysis Report 12/4/02 5:36:44 PM Page 2 No peak locate results available for reporting purposes P E A K A N A L Y S I S R E P O R T Detector DET01 Sample I.D. C:\GENI]E2K\CAMFILES\BKG120402.CNF Spectrum Number BKG120402.CNF Sample Description Bkg Check Peak Analysis Performed on 12/4/02 5:36:44 PM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts One or more peaks were dropped due to multiplet de-convolution. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 12/4/02 5:36:44 PM Page 3 

  - *****        N U C L I D E                    I D E N T I F I C A T IO N                     R E P O R T   *****

i** Sample I.D. C:\GENIE2K\CAMFILES\BKG120402.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\MYAP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) XuCi/ml ) Uncertainty 

                 * = Energy line found in the spectrum.
                 @ = Energy line not used for Weighted Mean Activity Energy tolerance used was                                 2.000 Nuclide confidence index threshold =                                      0.10 Errors quoted at 1.960 sigma

C Jnterference Corrected Activity Report 12/4/02 5:36:44 PM Page 4 

      ***       I N T E R F E R E N C E                   C O R R E C T E D              R E P O R T        ***
  • i****** ********** **************************** ****************************

Sample I.D. C:\GENIE2K\CAMFILES\BKG120402.CNF Spectrum Number BKG120402.CNF Performed & Reviewed By d2.AQ Date __ Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ml ) Uncertainty  % Uncertainty 

          ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
          @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at            1.96 sigma No peak search results available for nuclide analysis.

, ****                        G A M M A          S P E C T R U M                   A N A L Y S I S Report Generated On                                               11/25/02             7:47:46 AM Detector                                                            DET01 Sample I.D.                                     C:\GENIE2K\CAMFILES\BKG112402.CNF Spectrum Number                                                     BKG112402.CNF Sample Description                                                  Weekly BKG Check Sample Type                                                         Water Sample Geometry                                                     2 Peak Locate Threshold                                               3.50 Peak Locate Range (in charinels)                                    100 -          8192 Peak Area Range (in-channe.ls)                                      100 -          8192 Identification Energy Tolexrance                                    1.00 keV Sample Size                                                       2.500E+002 ml Sample Collection Date                                            11/24/02 3:14:00 PM Spectrum Collection Date                                          11/24/02 3:14:29 PM Decay Corrected To                                                11/24/02 3:14:00 PM Collected By                                                      L. Finn Live Time                                                           3600.0 seconds Real Time                                                           3600.3 seconds

(,.% Dead Time 0.01 % v Background Type STEP Energy Calibration Performed On 11/13/02 Efficiency Calibration Performed On 11/13/02 Calibration Geometry Used 2 Performed & Reviewed By Date J/A/ a25 

                                                                                                                       /02 Supervisory Review                      _,    o-?t2als                                     Date   -AR / 3Y / )Ad

Peak Locate Analysis Report 11/25/02 7:47:46 AM Page 2 P E A K L O C A T E R E P O R T Detector DETOI Sample I.D. C: \GENIE2K\CAMFILES\BKG112402.CNF Spectrum Number BKG112402.CNF Sample Description Weekly BKG Check Sample Type Water Peak Locate Performed on 11/25/02 7:47:45 AM Peak Locate From Channel 100 Peak Locate To Channel 8192 Peak Search Sensitivity 3.50 MDA Confidence 5.00 Peak Centroid Centroid Energy Peak FWHM No. Channel Uncertainty (keV) Significance (keV) 1 741.61 0. 2 638 185.61 3.83 1.1612 2 4693.58 0. 2048 1173.14 3.95 1. 4729 3 5844.44 0. 1805 1460.82 3.76 3. 0036 Errors quoted at 1. 96 sigma

Peak Analysis Report 11/25/02 7:47:46 AM Page 3 P E A K A N A L Y S I S R E P O R T / * * *** * * *** ** * **** ** * *** ** ** * *** * ** ** ** ** * * **** ** ** ** ** * ** ** **** * ** ** * ** **

  • Detector DET01 Sample I.D. C:\GENIE2K\CAMFILES\BKG112402.CNF Spectrum Number BKG112402.CNF Sample Description Weekly BKG Check Peak Analysis Performed on 11/25/02 7:47:45 AM Peak Analysis From Channel 100 Peak Analysis To Channel 8192 Peak ROI ROI Peak Energy Net Peak Net Area Continuum No. start end centroid (keV) Area Uncert. Counts F 1 734- 749 741.52 185.61 5.95E+001 18.59 6. 52E+001 F 2 4686- 4701 4693.53 1173.14 2.91E+001 11.33 -3.99E+000 F 3 5837- 5852 5844.79 1460.82 5. 18E+001 16.85 7.70E+000 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

Interference Corrected Activity Report 11/25/02 7:47:46 AM Page 4 1********* ***** ************* ***** *** ************ **** ****** *** *********** * 

     *N            U C L I D E            I D E N T I F I C A T IO N                    R EPORT             *****

Sample I.D. C:\GENIE2K\CAMFILES\BKG112402.CNF Nuclide Library Used C:\GENIE2K\CAMFILES\MYAP.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield Activity Activity Name Confidence (keV) (%) (uCi/ml ) Uncertainty K-40 1.000 1460.81* 10.67 1.449E-006 4.800E-007 CO-60 0.221 1173.22* 100.00 7.265E-008 2.853E-008 1332.49 100.00 RA-226 0.944 186.21* 3.28 1.158E-006 3.693E-007 U-235 0.684 89.95 2.70 143.76 10.50 185.71* 54.00 7.033E-008 2.240E-008 

                 * = Energy line found in the spectrum.
                 @ = Energy line not used for Weighted Mean Activity Energy tolerance used was                1.000 Nuclide confidence index threshold =                       0.10 Errors quoted at 1.960 sigma

Interference Corrected Activity Report 11/25/02 7:47:46 AM Page 5 

  - ***           I N T E R F E R E N C E                    C O R R E C T E D                        R E P O R T      ***

SapeID Sample I.D. C:\GENIE2K\CAMFILES\BKG112402.CNF Spectrum Number BKG112402.CNF I' Performed & Reviewed By 11

  • L, Date 1/ /I 5/a2, Nuclide Wt mean Wt mean Wt mean Nuclide Id Activity Activity Activity Name Confidence (uCi/ml ) Uncertainty  % Uncertainty K-40 1.000 1.45E-006 4.80E-007 33.1 CO-60 0.221 7.26E-008 2.85E-008 39.3
        ?        RA-226               .0.944       1.16E-006                  3.69E-007                  31.9
        ?        U-235                0.684        7. 03E-008                 2.24E-008-                 31.8
        ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
        @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at                 1.96 sigma                                      -

U N I D E N T I F I E-D P E A K S Peak Energy Peak Size in Peak CPS No. (keV) Counts per Second  % Uncertainty All peaks were identified. M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.96 sigma

CALUBM( YS N AND TEST REQUIREMENT FOR RADIATION PROTECTION INSTRUMlTATION ( RE( =AIT-104 REVISION 0 ATTACHMENT 6.4 INITIAL REFERENCE RESPONSE TEST FORM (example) InstrumentModelNumber: _ 42D7 ( ,m2v)(Instrument ID I12 Scale or Decade Reference

Reading [ +/-20% Value of Reference Reading Jig and Source ID Number Geometry Remarks l LX'.. .____ 1.
                                                                           ./~AsiJ                     (E     . J'/o 7-               6-_

lPerformCA by:Date 'A/;,{?2n I-Z7-01 Reviewed by/Date_ ~ , /iQ a v 3 cA 4 , , REDSPROCWM1NS .:0' 1 of 1 of I

CALIBRATION AND TEST REQUIREMENTS FOR REDS-INST-104 RADIATION PROTECTION INSTRUMENTATION REVISION 0 ATTACHMENT 6.3 RESPONSE TEST FORM (example) Instrument Instrument ID Pass Fail Performed by Date _ _ _7_ _ _EA __ / 

                                                        /4 I    i/a/c Reviewed by                Date /

REDSUPROCUINSTU04 1 of 1  ; .~.. ~.

c§ 1/2.TIONOF THIE LUDLUM MODEL 2350 SERIES DATA LOGGERS C REDS-I(- -201 REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FORM , SECTION 1 (To be completed at Initial Receint Resnonse Test) Technician Sirmnanimre Av nate: og  :; INSRUMENT & DETEOR TON DR TO ANCE VALUEs - SOURCEN hnstnnent Model No. 3 _q Cal Due Date Minus 10% Pls 10% Net EFF SEG MI Serial No. Instument Serial No. 4rG- B 

                                                                    ;7 g
                                                                                /o 7/                              / 3o7                I             37           CLZI6 Date Cticdon
                                                                                                                                                                                       ~//qbs              1 Detector Model No.               z3 -6             Cal Due Dat         prrAting CodidotL:                                                                         Nuclide                t
                                                                        ,Normal                I0    Abnonnral                   Altitude           fl.

Detecaor~aNo. i3 Cablee Leng ft. 0 Teerature_ OF Avity i dpm SECTION 1 Reviewed By: Date: I 4az/C>3 SECTION 2 (To be completed by RP Teciiian) t beginning, verify the Intrument SNs listed above. IF the informaton above Is incorret DO NOT CONTINUE. T TestType I B round Denat I r CountI l Source Count Data Count2 l Count3 Mean Toleanee Efficiency Perfo byedb L - = ( e (SCRt3) Net Sidl Unst Ui Cf Gros BKO Gros i ca n Net [Gross CPM l Cnts INet IGross CPM CnsCPM Net ContEF R!te P P.ai Technician IDate/ Tile _)_ l, & 1 n //fo l l 0 7 ll Time _W pnl /53 2 sFl 1W 4s_ 5o1< l1 le3 9 lsa #6 /1773 UAR Reg1 /27-119, l lA 21lg22 Ql I / t ,5 I/7 1(3 I A u71 t1 71 7 '3/ ILI~ 

                      /2f5~oI              If Ws9                                                               i'3o      ;'4                __          d,,,s-S         1                            }I 141IE2kLBy                    1J      innh     e1..             hisOrm7 inP7O. ,en1v7 1 1iho        ve     cek'x'         ad             e B.M-ALlJCL(ZL.
                            *01, i     -          ..                   /tff-    1 1-3
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I rjk/0 M,1;I / /3fI.1 6403 1*41.1 ,54I'tlf.7I 1'tf175Y l.;3 25ZP3 /1-3 PEMARK: WIT 1 B WQpa sramteters le ceked mad are verified to be correct SECTION 2 Reviewed y: -Date: / 0270-3 PAQVfr~eu #riPQVM4MVV,1ll 4 IlMn

23 [ -. O7N OF THE LUDLUM MODEL _ SERIES DATA LOGGERS C. REDS-INr REVI SN-1 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SlCIION 2 Cro be cond by RP TechnMkn) l1m tl SesteMOded al 735;-/ 

                                                            /5             l Cal DueDate t      -    -03         Detector Model IV-/oLZ            Detector Serial I        ifs      l Source Seriai /     i   .j Test
             .est TyeAaltrrm Type Dt Da2Test
                                                  ==
                                                             -IPerformed I                I ,        A SourceCumvtDat-agrod I      -         l 5%. 14.9 M

5ogC. 13-. Tolerance b See Now by no LS1w IpcID L" N KG Th" I I GM Na G im 31 A Nd iGrn n Rd t s Err IT IpSUFS1[____ _/ ___ = CasO _ 051 OII3 T.mClM3 7 o sI __ 3rot 1. 

                                                                                       ,3                      Kw,11%       1//7B'l JLMJL              .3'     I                szj4                 !

04 Lc - i1. l W- I d"L i/S/43 La22 /I7'/1 /1 03.1 *E7Q / ___ o '3fl'd 111,AL6o4'3 ,o&.7 ZI&'./ f PM 3-4 IJ-7-b9 IC)t1,1 

                                 °1Z~6 58                     1*-s3 I{1IY/0S0IO tddIM 101                                   t3K.4- 11BV-              11/11 (I5<l§1l                   D .31Q'I      'S10                I Oe)171$>l3Atldt'1,letl3                               1,4-3 1/.-,ue                 Y14 Vl\           ir   q11?i J-         l, 6 12#707 1/5;23 1/^            4        /6ZT 1,2n14        1-       3            H8/l 3,4-r
                        -Vs1Q   R0 3wr   A )o1T A Ll I/A0 /. e)Z1 13,53, l 'l 4 1i53/ &10Z     Z      /J26S _;YZ--    "*l V'.vf                  5        s               =

Ba1 1--1/0 1X32elILIB1 1f 169, /5 > t /1 vt S 11 W11 1/ 1r. I 130-s>1wl>829lz*j7 1/i24 12146 ISI 1 )1 s I'i) D 13Z71 3,9167W #9_3 l4 l41 R/!'31 1n4 1V751 /3ilqt2>zo A. ,1 17 _ 1.2 / - 261/1 REMARIkS: NOTE 1. By WU91WdMhNeck. d dvig e c hdI s Immn bees deed ad as varihd be o-s. ' SECTION 2 Reviwed%By: Date: /.i 71.) P.\SI1B5201_4.R3UNbTdN5214.WPD 9 of 11

ofi'XION OF THE LUDLUM MODEL 23 -SERIES DATA LOGGERS ( REDS-1? ' I R.VTfON 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM 

                              *.1   4 SECTON 2 Cro be            bM       IRP Tedmidan) instmmentModel V35-I                instrumsertialI  //75Z6             CalDueDate 4-          -03      DfteczorModel# 1/2/-0oZI            DetectorSeral     £      sourceseriall          .

Alarm' l Tes pe Background Data _rm,_ 

                                                       -htsC,,

_ So rce Count_ Source Source C C tData Dolerance 

                                                                                                                                                         - r                by Note b Seeo GjGi Ii                                      =                 T l i       f"'_

e PITIMM" . 

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                                                           )

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7. _ _ - )- _57....

I 1 7 W. vz5i 7 P03 /IP-) PO- /,23I 

                                                                                             =                  __==                                     -                   =             =2
         --                                                                                                              11    (            IT         l                    I)0         11 I_                      __                .7                                               11_I_1_=_  _   _

REMARKS: N(YFU 1. B k. leueutldlusd¶pIIUIpuy xft W1Middngddgbo WAs bee. NM W NMeke endiW,;d/mc amidu SECTION 2 Datete: / P.%SIraRBDSwRlOC~lrf~nvrt3zul-4.WPD 9of 11

( RATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS C: RE(-1INST-201 REVISION 4 COUNT RATE D=MCTOR RESPONSE TEST FORM SECION 1 Mo be comileted at Initial Receint Response Test) Technician Sianature: T. c. t.A Date: 121t(8( INSTRUIMET & DETECTOR INFORMATION DETECOR TOLERANCE VALUES H EFF SOURCE INFORMATION Instruent Model No. Cal Due Date Minus 10% Plus 10% Net EFF SEG ID I Serial No. Instrumqn" Serfsl No. 9o3 q ig-Al-03 HWI Certification ate 8 qel5 Detecto Model No. LCal Due Date OperatingConditiod: Nuclide -qq t./ oa Normal a Abnormnal a Altitde - ft. Detector Seril No. L&l UWtableLensth 5 ft. O Tcp rer0* Activity in dpm SECTION 1 Reviewed By: -_ __ ____ ____ Date:_ -72/ph SECTION 2 go be c by RP Teduhician) Prior to1gInning, verify the Instrunmient SNs listed above. fF the information above i incorrect, DO NOT CONTINUB. Rmpleted Source Count Data Mlaria Testfaype by Test Test ype Background Dat Count I 2 cCwnt Count 3 Mean Tolerane E1dency Performed Iby 

              -                        -            .           I       ($_l)            (                       (sCan            Net Sat/     p       P         Tm       lrosG lKO                  Gross     Net    Gross       Net       Gross                 CuRat                         EFF                 Techian          Date/

Time 1 CKG Cmt CPM Cots CPm Cot CFnIdo ?tm rme h Unod(un) 

                     -l     /

Counts i . 1£37 SID 63(p MNSRat Pas (B Pll'aFlod&MI 1I _W r_ t)bic 3 

                                                                                                                                                                                                )  Tm i

I, ,-o 3_ o 17 615 57(4k' Iq-4 555 t1 19' , -. ) .Ab'(!4 

    -1                                      -                             -           I         1                       -1        -        -11 REMARK:

NOTI 1. Byinitialingthiblock, the Instrutnent paramtrs a be checked and are verified to be correct. SECTON 2 Reviewed ]BY,: V 0T& Dat Ip&42A e:/ P:\SITli . AOCS\INSWNS201 4.WPD P.. N-..

C C OPERATION OF THE LUDLUM MODEL REDS-TNST-201 2350 SERIES DATA LOGGERS _ REVISION 4 GAMMA DETECTOR RESPONSE TEST FORM SECTION 1 (To be comnleted at Initial Receipt Response Test) Technician Signature: AC. .W Date: /-Z -e2 INSTRUAME &DETECTOR ACCEPTABLE INSFRUJMENT RESPONSE RANGES SOURCEINO ATN INFORMATION Goer iu 09'~tCut ls2 NtCut E / o ImnsumentModel Number _____It 2350-1 C DuO DeftS 1 I Peaosiio

3 j 3 5f4 497, 03 0 ______ J-1-at
                                                                                                                                                                                                        -7 Serial Nutn er Jr   h m5 i    4 ,

I2 Z . 3 I 2 3iJ 1 '1 A__ `__ Nujcllde CS -/13 7 j Detector Model J Id EI 5,90' N umber @8lnclte _ _ _ _ _ _ _ _ 4d3A c t ty n Detector Serial j9IUormal 0 Abnormal: a Altitude ft. Number 0 I4. "- 3 p d~ 'ut 0 Cable Length ft. a Temerawr 70 ep SECTION I Reviewed By:_ 0! ~ Date: 4LaZTe2. SECTION 2 (To be completed by RP Tec~hnician). Prior to beginning, verify the fnstr~ment SNs listed above. IFthe above Information IsIncorret, DO NOT CON__II ACTUAL INSTRUMENT RESPONSE L r 1m Test Tie Gos RG0 Contact @6 Inches a la inches SceeNote I _ _ BetTyeKG; C Oro" it 'Net G os iti N2 e O~In3Pass Fanl ibyPech (i)counts CPM Counts CPM Counts CPM re&Judh SAl .. - j 554S3 i',026 #A5A74,4jqa 51 47,714 /J4d/2 Y3L2 ' __ ke

  • Iiv/&V
                                               -. 4     '                                                                  -t 9 1 1ag               to             n2ir            .7                               0 5344Ullo30q,'U                                      T7VW                                   7M9?40                                                   _____30 lr"l    14V          ?       9#N      _____r~       t1363        _____       le/8 I3
                                                     -           -                                _                  -F-N

.. NOTE 1: By InItiaing fthi block. fth tecn canpdO$ that ibe Instrauent parameters have been cbiecked and ri Verfed to be correct. SECTION 2 Reviewed By: V pafC Date .J/p . I W p:%SrJ?_3UW$VR0(;MS7WS201 P:SflESREDSPROSUNS1MNS2O1.A.WPD 4.WPD 4 of 5 4 of 5

OATION OF THE LUDLUM MODEL 2fv SERIES DATA LOGGERS C REDS-( REVISION 4 

                                                                                                                                                                                                        '1 GAMMA DETECTOR RESPONSE TEST CONTINUATION FORM SECTION 2 (To be completed by RP Technician).

lsu = _4 ICal DeDatez Let J* t mentSermdlul Detector Model d -10 Detector Serial I 16.t -I 6 Source Serial I o 4 l 1 Source Count Data F JacPerformed by TTest Satl TesrtI TestTp Pre 

                      =a Post     lTim Bakgoud hkpoundData

_, Count' Grosst l KG B'KG l(li) 1-[ Gross Position I Contact Net 

                                                                                                          }       Position 2 0 C6nches eTl Gross          Net        Gross PosItion 3
                                                                                                                                              @18 nhs________

Net [NTolerance o 

                                                                                                                                                                      =_  -      .- _______

Technicin oe Date/ TUmat WR)Cont CPM = [Contj Cpm Cots jCPM Cots jCM_ 

         .. L.O6                             %                      L..4ts'4            'o,-
                                                                                             %i       r     -st-es Lf1              18;tx,'          7.19o
     -      -1      -                                                 -                                                  I1.        __7>-

_ l;* i74 tob-417S;6;fi0< 7Zb=S4f B;) 8 hi NOTE 1: By fntal"Ing dkl m~ock~ fthe te d wicaIcaftes 9* t instument parameters huve'Peen Oecked andf are verified to be correct. SECTON 2 RevIewed D&se Date: P'%SlrW 

 ---         'DWROMINMnwI
                 .-        .-    ----.       Ii. W_-

5, - s

XC,4TO OF THE LUDLUM MODEL ( C' REDS-INST-201 2350 SERIES DATA LOGGERS REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FORM SECTION 1 (To be completed at Initial Receipt Response Test) Technician Sianature: &. j Date: 16-LtS27 INSTRUMNT & DETECTOR INFORMATION DETECTOR TOLERANCE VALUES EF SOURCE IFORMATION I Jnstumme Model No. 2 50 - Cd Due Date MMnus 10%*us 10% Net EFF SEG ID J Serial No. //9G5O4 Instnwnt SeralNo. 53 IZ2. o3 0 0. 5 

                                                                                   /30.                                                           o..               Cerdficaton Dam            9-96 Deectr Modl No.                 43C-/06               Cal Due Date                    ond"dom:

Iang Nuclidb 7e-aNormal O Abnomal a Altitude _ . De___Serbl No. 4/ 03 bo Leno C33qeg $ ft. a TetW 7^ -P lAcdvkty Indp 50/6 SECTION I Reviewed By: Date: SECTION 2 (ro be lby RP Technician) Prior to beginning. verifyt die Intrument SNs lis above. IF dfe nfonmadon above is Inorrect. DO NOT CONllNUE. SOW"c Count Data Alam -erformed.by Ted Tatpe .BagrNdDta i Cont1I Count 2 Count 3 lMea Tolerace Elclen e fle No 

                                                               -        _           I           S                 MMSCRt)        Net                     I_______.___

Count am" Gross Net Gross Not Count 

                                                                    !" CPMK CM !! !CPM WM -'
            /              1{to 3001.      !
                                                   -100 lazt3             24 /5.Ul /RI2;taL187 /19? l 145 l l! !l !ni L"

022,0 A e IAC

  • 1l TLil
  • Y I $- 1 lb o I o Jll? 13q7 toot'./ Lv P IV o.a'
                                                                                                                                                            '0.2tr.¢(2 1Vv1; 10                     1.

1217UaNal 7 1ue.l.I417fV lIO0 I Ot 30 7I9j Ii.- 1.1 111 V/ 1 

                                                                                                                                                            °-3 110/72 19W1 I                   111              ZkI~II2/I/tI 414CIO~ IL                                                                            /         lO2tlC~                          V*          U I 111 1z11         1 /Z) t         l7;3 [d'  174 Z        U- ,,

t7-3 kqI 

                                                                           /el      ,L5la'fI             I          Ii      I            I v 1_ 11D_5     ____r
                                                                                                                                                                . Z

___ _ /zt q e I REARKS:I I3V11 F I 17 mco/ ipl831W4e/ 126 Rlxer-r L ,,3 il NOTE: 1. By Initialing fti block. fth tchnic~p Inlaeola h 1MInsrnent parameters hay beep checkedl and are verified to be correct SECTION 2 Reviewed I By:. .. z ga _ Dat D: -- 4/ a W

Or 'IXON OF THE LUDL1M MODEL 23SE DATA OGG ( REDS-RTEVICIS 4 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SECTION 2 Cr be cedby RP Technian) lmtrmOded 250- InnreSeraldCal Due Date 1- - Modl Detecto -/4 DetecSel 39Sre Seia / I IY 

                                            =

Dackgronnd Data _ Source Coumt Data 

                                                                                                                                                                   =    TercePerfomed                        by A    7S9 Aham        Te                                                     -T Cj            al                 l    b) Ka               G    j      mI Gum         No                    NHl ll                                                    Tbeml

_ct2p. .. ~ __  ; .=* _ Jo g l2I 1 __ 6116 113 J4fI 37 14 13A 7 1(54 '//S _502 ID/ O 3O2I 3oq j.39 1 A5 1504 1 142 1501 124: -I z2*7 __ - - _ ___ _ _ -5 02 ,., S~kf -VI 10 1805 11 .30 1 1395 .11 156 &S4149 356 __ V - -l1 _ /I_ 93_ 2.34 V W*/- .4 A, -z /tF _ W _ _}F i;$ 

                                                                                                                                                                                                                                 /-^

9tr = _ 02905 Zf ¢ 1 / 5 1107, ~3 II; 716 zo 6 1V 75 1107 24 < I__I 0 29 s 4_ .I >IIl 3/454U7 3 40 114.41 I4 .22 / IA.V A l A-r to- 92k 9 13-7 fZ '311.34 i4ol iI I1114 We /a17' 

                                                                                               =>                    Z e1S+_
                                                                                                                         /Wt435t                                                                                     ig73 str.L        ISH__                .-        99             sI     _I 1                              /0        /S         LO 5        1/14           1
                                                                                                                                                  ' IZ?          .22      /   __                      sC     I73D3 S             l 1                       P)         10       i                      g      fI  ((7a  i4o P43q        117     13-_

_ 1_ 1___ _____ st I'cl = S25L~ J> 5 Iia .2Z"' _ __ _______n tI- __ I 2 191210W /*4S I 11 7 /43 1173 113(, 52 I iL 1+61gg *- //"i 131 t'), If-3 2 /VI ____ 

                            .+/-..

to 1.22779 fll- 1+/-ts-l iiqq 1415~ "HI '11 .22! / _ __ I 

                                                  .~A*a!         J       ._
                                                                         -        hO O~i I~4         ~~ ~TOIF      .. __          .7 4

__ 1411143 __ _ _ _ .23 ' _ -4 e SECTION 2 Reviewed BY: k Date: / & - 

   -+           ,IF
                  'gC^S. PL'~&'            4              A0$I P:\SITDSREDSPROCS\NSnWNS201_4.WPD 9 of 11

OP76:xON OF THELUDLUM MODEL REDS-IN5 -- ' 23L.ES DATA LOGGERS C REsVIRll . 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SECTION2 (robe comby RPTemchn) IntmnienModem - l i35mmlem Serial 9&3k) CalDueDate 1-2.2t53 l DewcrModde I3- l DetectorSerid :1 Sa9rce Serdal I/9 50 l ._ Source Cown Data Perflormedb TAes __ELI" S~ Test Type tG 

                        . hf
T Ba-ckgrmd Data KGc "to l ielBGlCM GlNWl6an431

__IlIMtI t1 ON cmanaCa"om__ I iia I ___1_ xed bw sPerformedI by cn. l __1Mt Tim r 2D15 Ii-2. -o lo AM ;l .a;l - 

                                         ,*S           -1I aI            /W         (O 9-Zf I.?ef, J//+                142A      I7.2.-         /0-54.                    _/,
                  .    -0                                                            1*3-k 3                 1    /51_3      0.37         /O-7                             J A1 I

&A*r - =__ I1t W45!2I 1ALML f zkc 3 t VQ P131W13/ W¶'A?4' /3S I5'$)-/93-1 fI 

                                                                                                                 ) f        T39
                                                                                                                           /03               9v-I l /D~r             I~iE VJ _     lt                        __

r /'/" 5 144t 133 o-M 1 ____ Xl /.- 

  -~                __        tJ      9     4e3       ViS      t'       *7.7%            P      jI(          l 131           bO      </ES)                                                         (TX-RfO?4O).l
                     /- 'f (5
                   .v__                          v&~AW, o    I          t3.A, (,~

toW. ,V5 4. /14'0 If -- ('13 I13et7'J.4'

  • 11i . 1 A/ . . V000 __ /0 t2t &7b1 XZ /° f1o< o7((t (IfL6 f 171{ 16l313 iii lA~

I?'>l'?f ifob pIIo lo.< LII . %o I-%/0;7o7Z7-: _ t& 3*1fb 3IK W 13810Vll3 t1116 qg( Jj)-J intflo . v IlVllzll S/ _ _W E tt1>6HV 117i1 tf/Mt Ift 10111W ag';5 Isd REMARKS: N vL 1. . ; ,I . - ---- NW 1. ddl 2 W*.Ily hWas -ib --- ha- s bb*, dec chm d v fid cbecIDh SECION 2 RevieedB: B-_ Date-. / ... P:ASfHS\RHDSTPROCMUNS0UN5O1-4.WPD 9 of 11

{ ,flON OF THE-LUDLUM MODEL 23(u SERIES DATA LOGGERS ( REDS-Rr RE3VIKxoN 4 COUNT RATE DETECTOR RESPONSE TEST CONTINUATION FORM SECI1ON 2 (To be completed by RP Techidian) I WMWWMe odesl3rb. InstmetSeali Cal DMe D _ _ :Ips__ _ _de69 _ _ Mode 

                                                                                                                               #ol6 10  _     _

Detector Serial I _ seI Sotrce Sea ba ] Marm Test Type natk d Data - Ce__t T Performed by ltmN we 

                 .vi IaO      =        _      0         1-      Z5t                                 '-        lI                M I

aM BKO I[ Goz Rd amn NeI Ga N lEffi L1 11 I/11 zo LecL>3i l =* *t ______ s = o6 ________ 1 L°7 3 ____c i 11 I3ia311 1 1H II Iime IG (e----I 0l 1 to 711 1 m - 541~8- V ID4343UV H66110143 of/ o4 S) I/A' - .AMc' WN~ 

                          /v       OU3O                       (3t6          oIi66A'3'u                                            (/e)                     -

I6 _.L _ J. 1-111 Ios 1.3t /11M 1 11e ~ ]1-1/ t1 1 J. &C,11 r1 1 

      -                                171 RME:    1.o i        di d/h r  3Lg          3 dc(     n3        h8bAd                      g1l                                                                -u I A.
        *_.                                                                                                  A SECTION 2 Reviewed By:                            G      J         -Date:                p7..                      * ,.
                           -* 7.,-                                                         5E            ..

9 of 11

PERATION OF THE LUDLUM MODEL ( I REC INST-201 2350 SERIES DATA LOGGERS _ REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FOR1I SECTION 1 (To be completed at Initial Receipt Response Test) Technician Signature: Date:?4-?-I -f_ ? - w{, INSIURMll &DETECTOR INFORMATION l DETECTOR TOLERANCE VALUES l EFF - SOURCE INFORMATION l Intnunen tModel No. 230 -I I CaI Due Date Minus 10% pIus 10% Net EFF SEGIDM/SerialNo. Imbm1 Serial No. q 5 34 0 0.3 8 72*5 G Certification Date - 9!k Detector Mode No. 43-106B Cal Due Date ringConditions: Nuclide rI dNomal O Abnormal O Alititude _fR. Detector Serial No. 3 9-3 oCable Length ft. a TempenwiUrF*PF Activity in dpm SECTION 1 Reviewed By: 4 Date: O 3 SECTION 2 (To be complete by RP Texhnicbn) Prloft beginning, verify the Insftnment SNs listed above. IF de infration above is Incorrect, DO NOT CONTINUE. Soure Count Data Alar TestTpe Dacground Data ylt3 Tolerance Emdicyl Perfoned by Tast Countp 1ckrondDgCount 2 Count 3 Me oevne EdqSe Naft I (gm R 1mm S R2 Net .l Sat l ar m l l Gross l Net Gross Net Gross Net Count EFF Technician Date/ prsPs Tia) BK'Gsi CPM Cut __ Cm CPM Chts CPM ioCnts CPM Rate pass palln(Name^ (mom___i_ riet 

                                                                                                                                                                                   ?thd__         _

Time Tie_ 1 'o4- 9/ 'o, 9Y4 q3. - OOS. /O p fowe4s, I/ 11A /0O t I 1 1f 1- 1 1 1 11- -_ 1 I11 1,L 1 it 11 13 1 91 1 11 10 2 Ir. M. I I l15 t. . . . . l e M . ThiIWU. 1 uv a.Inbiu.. del. 1.1.4. tdnieidih....a7.In i_ Dllt~eImfm it flrmtIvS e imen eheckrnd and ue verifked tO be correct. SECTION 2 Reifewed By:! #, Date  :,

  • z p.sfm . .AOMSINSTIMNS201l4.WPD

C> OPERATION OF THE LUDLUM MODEL ( REDS-INST-201 2350 SERIES DATA LOGGERS REVISION 4 COUNT RATE DETECTOR RESPONSE TEST FORM R1ITCTYA 1 CMn ha-t.mnleted at Initial Receint, Resnonse Test) Technician Simfature: AO-,. ztx~ flute: [INSTRUMENT & DE1TCTOR INFRMATION~i DETECTOR TOLERANCE VALUES EI SOURCE INORMATION Insrment Model No. 2 - CaM Duo Date Miu~s 10% FPns 10% Ne l SRO MDI Serial No. AS 3, Insumnem SerilaNo. q~IO iZ-3 .1.54/.5CffdftdonDate Detector MdlNo. #&3-/O6A Cal Du Date operating Condiio: aucAbde -ns3 0 Normal 13 AbNucliae 7ft-230 Deteto Serial No. 13 9S',? 0 abe4enth tL0 emertue PActivity i p ~~g SECTION 1 Reviewed BY: ~ 2 ~Date: 4 SECTION 2 (ro be cpetdby RIP Tech*ncin) Prior t befinning. verfy fthJnstnnnen Sift listed abov'e. WIphinformation above Is incorrect DO NOT CONTINUE. Td Tast Type Racliground Data 1 Cu I 

                                                                                            ~Sourm Count Data Cont 3           mean       Tolerance       Effcenc                  Peftotme by 1                                                                                                            Net
                                           =~                                                  ra=m                  tSC3M Salt/                           n       aross       DKO      Gross    Net       Gross        Net     Gross      Net       Cut                            EFF               Techicican         Dtel UnTntutKG                                        CPm       Cots   CPm        Cuts       CPm       Cots      CPm         Rt         asFi nst("de)                      Count                                                                                                                        ______
        -tr1                                        (0       '.(       39]S,?ta.L                      -4J                       31   -q   --I
                    -                    -       A-         -Z                     -

3f34s 3~ 1 ft3?3 q q*x 3b SI V. 1 jcta I 

                 -     -                 -          -             -                -11't-         15-?            -o%              (#.9          -      -

w .44-I REMARKS: NOTE: 1. By 'idet aIng tOM block, Ithtecmid Mdpq mh~~oIsinun parmmetermbaveftcnecwed anm are veriwe to be correct. SECTION 2 B: 

                                        . :-         -l!/.IReviewed t     =1'-

f Date: . f ZO3 

                                                                                                   /IN

O),.IION OF T-LUDLUM MOD DELL4 REDS-INU N 231- -AUESDATA LOGGERS, REVI&- Aq 4 j. COU RAt DETECTOR RESPONSE TEST CONTINUATION FORM 4 4 .9 Cro be cme RPTeCn) by [in Model 2M- - 60 j imst sen Sexiga 4 Cal Due Date I22- l Detector Modde - Detecor SerialfJt3 Souce Serialt '9 ,CJ4S1 Sonrce Co DataCmt - S . Tear Test B i Da= od Data . D Tolerance PeKfore by _ _ _ _ =11. IWCm. l wI VKG (e. II l Gme. I 0 

                                                                                                  !.......=MII 11_)              I ism Cod Notedi"aHaci.,sf M

Ond,IM 

                                                                                                                                                      ,l    MaIbe tl   Rn1ii ldet sNk E   ffi           _   _  _ _  _  _  _ _  _

I 

   -k      -      __               -°                -7        3.1                           41 _ 39'         3aX            3oqo                q3( 3B'73                                                            _1   _1

___ _ 11 3" 3.3 1 %3b3/3'?'"I 3u 1(23) _ _ _1 Au.Aq{L -F3-oL ___lMS ___tlsgS -~ili -l lisl~~l4w3l ___c~kd -i ___1 I0r V , 30 3 . / 39o, ir3' 7 qs,3qd z 317 3 11 -6 . J __ __ 39t{- q 7/ __ A__ __ /0 40 (0~-V 0fa RYT 11 1iI 1 Mh 1. 11- k1M -. I d1 . n a hIbee.hdcked mamvalflevbqeo 1 \ms SECTION 2 Reviewed B: , Date:./4/D P:5ITU3UWD3U'iOUIZUrIWJ q.wrD 9 of 11

0 mTION. OF THE LUDLUM MODEL ( REDSION41 2350 SERIES DATA LOGGERS REVISION 4 GAS FLOW PIPE DETECTOR RESPONSE FORM SECTION 1 cIo be completed at Initial Receipt Response Test) Technician Sianature: Date: DETECTOR INFORMATION DETECTOR TOLERANCE VALUES EFF SOURCE INFORMATION Deteor Model No. d3

  • 1 10% Plus 10% Net EF SEG inDISera No. (/ 29 ( 1 }

DetectorSabiaNo. -erfL3t;ti / l A ii,- IlflcnDate Cal Due Date Z4 ?A Nudide 7!-2 Operatng Coions: 0 Normal o Abnormal a Altitude ft Acinvy dpm(S1 m (7106 O Cable LEn". ft in Temperanue *P __I_.__ SECTION 1 Reviewed By: (2 _ Date: Z, SECTION 2 a be iwd by RP1Todm) Puorm wemhg. wdf~ ntsmeN. asemhw.. IFdo hdimd" Abm I i Do oNcoM 0ritB Instrument Information ATet Test Type Dackground Data Source Count Tolerance Eff l onned By __ __ _Date Test__ See__NOW_ I Count Gross BK Technician SerialNotl/Du Pre I Post 1 - Time lBKG l 1Counts 1 CPM 

                                                                                                     =        1 Goss l 1=..           Pass 1n Fail               (NamePrinte &
                                                                                                                                                                              )          __

Date _ _ _ -3 _ 1 1 ~ i~ 1 I - '1 Remars: All, Note: 1. By initialing his block, the lec l es dih dyBe instrunent parameters have been checkd antreverified to be correct. SEMCION 2 Reviewed By: M WVcs f f Date: 4 I  : .

O'LATION OF THE LUDLUM MODEL 2350 SERIES DATA LOGGERS ( REDS-UC -201 REVISION 4 n :i GAS FLOW PIPE DETECTOR RESPONSE FORM SP!CTION 1 (To bw cofmpleted at Initial Receint Res~onse Tesvt) Teclmhnician Siematuirp no,.* J-. .- Z-  ; I 

  -    r-    -                      ;                   r   -   -fi----r--,                                                                                    .        X-     .            z                    --         I.- ,

DEWECTOR INFORMAI¶ON DE ECTOR TOLERANCE VALUES 1FFSOURCE INFORMATION Detecr_Model No. Ms 10% Plus 10% Net E sGP ID/Serial No. Dextcor Serial No. : rl/ - l I I Certfication Datemi-d95 Cal Due Date I 4-/p - II I ' 39 G' Nudide _______ OperaftiConis: )4oml . a Abnorml a Alitude ft Acdvity indpm(S6 o CableLengt n ft a Temperatire -- OF ._ _ 977 SECTION 1 Reviewed By: __ Date: SECTION 2 b tPT ) Pyoi bel f,As hhted Ibd nPtio b I, -teDO HOTNCONNINMl intuetifrain lTIrstruatt on Alarm Test Test Type B~ackground Data SourceDataCount. Terne Tolerance EfPerformed EfF B Se Nrot~ed By Con Grs - T - - - c ia M2350 Sati GIsN G l etl l .1Technician l Serial NoJ~ad Due Unsat pre j(a)CIf Post Time 1KG CPM GoN Counlts CPM 1 Ps s -1 Fal(uPntd& - hinted1 Time 9?534 Z-j&W-e9 _ _ _ _ _jd / /lo' /c ~ J-~' 0o."O/ W'Al-ylrw 

       ~

4~ = = 1 - =.,. 1 - =1 1 =11 1 1 1w Remarks: Note: 1. By initiaIg this blocki thec technlcj A d# nstnnnent parameters have been checkyd anr verified to be correct. SECTION 2 Reviewed By: C_ Date: y42q r .:,,,. ( ' ' 

                        "I --     . . '-

OPERATION OF DENVER INSTRUMENT REDS-CEM-216 MODEL XE 3000 ANALYTICAL BALANCE REVISION 0 AITACIMENT 6.2 EXAMLE DENVER INSTRUMENT MODEL XE 3000 RANGE CHECK Model XE3000 S/N 3O9 Cal Due Date:3 Weight Acceptance Range Reading (grams) lg 0.9-1.1 2g 1.9-2.1 5g 4.9-5.1 10 g 9.9 - 10.1 20g 19.9 -20.1 50 g 49.9 - 50.1 /w- _100g 99.9- 100.1 J00-O 200 g 199.9 - 200.1 500 g 499.7 - 500.3 __50____ - I-kg 999.5- 1000.5 ,ooo. 1.5 kg 1499.2 - 1500.8 150o. 4 2 kg 1999.0 - 2001.0 _____J.__ 2.5 kg 2498.7 - 2501.3 i J,1 3 kg 2998.5 - 3001.5 3COO/. 1 Wdght iSN, calibration date, and calibrat/on due date: cda6 x9, O/CR/oL , /O/o?/O3 erformed By: c . Date: IJ14e 02I RE~wO~~~rcH-21.O 1of. REDSMPOCSTIOCIIKWI-2 16.0 1 of 1

OPERATION OF DENVER INSTRUMENT REDS-CEM-216 MODEL XE 3000 ANALYTICAL BALANCE REVISION 0 ATTACHMENT 6.2 EXAMPLE DENVER INSTRUMENT MODEL XE 3000 RANGE CHIECK Model XE3000 SIN 3Cal 7 Due Date: //o/0-3 Weight Acceptance Range Reading (grams) I g 0.9 -1.1__ _ _ _ _ _ _ _ _ 2g 1.9-2.1 / 5g 4.9-5.1 10 g 9.9 - 10.1 20g 19.9-20.1 50 g 49.9 - 50.1 __ 100 g 99.9 - 100.1 ,30.C) 200 g 199.9 - 200.1 _ _ __t 500 g 499.7 - 500.3 SO _ __3 1 kg 999.5 - 1000.5 Ii).5 1.5 kg 1499.2- 1500.8 i50O° 2 kg 1999.0 - 2001.0 lOO(. O 2.5 kg 2498.7 - 2501.3 )fYO* 3 3 kg 2998.5 - 3001.5 _ _ _ _ _ Weigt Set SN, calibration date, and cal,09at~in due date: erformed By: , < a Date: 

     ,-     c \-Iar-y-        04                       +0 1   . L; ,,,Ae-A -us e- ,,4 'sc<?E-0i oor-    s
                                                            -3 Y,3 0
                                                      +o
            .\,Jj  -       fafq-
               ,         . .       m:.I 1 of 1 RED6'flOcXOIMOiM-216.O .0 REMSPROCSTIWHM-216                                     1  of 1

OPERATON OF DENVER INSTRUMENT REDS-CEM-216 MODEL XE 3000 ANALYWICAL BALANCE REVISION 0 ATTACHMIENT 6.1 EXAMPLE DENVER INSTRUMENT BALANCE WEIGHING LOG Date/Time Sample Number/Description l Weight Tech 

                    ;k /

o, J. J,050 'roo0 4'-rxoa,r &PL. fSo 7 c5f 3 ya 7a a/o SI-. 5"'* 3 4__ J 

             ./4- 149                     Jo                                 lee.

__ °; _- /o o AO___a &t/4 /o./ __,Zr a-rs/n oe~ 1164 v 4jrelo 

                                 $                 tW               .5oeo.         S
                         ~~

Sao J 4 _ r__ _ _ _ 0 o _______ > 6< *S7-t /I2 do  ;^ 4 REDSTPROMCtaM\CZM216.0 1 of 1

Tennelec Sample Log Omaha VA Smear Analysis Date/Time Sample ID Quantity Batch Key Analyzed Counted by 

/2/V Z. lo-k                    dAoo I) a         10 I bt                              h     7 /        l Z/3/

2 z / ,Or A§Od i o 3w OA  ? XY 7. X It/3,ZzZlK2. A6001/ o NO w; 3 /0 6zL L2/&2V /LI )d0' 03 Wthq 6 .. L2l ziAzs z AIioo/ 6 Aib3I L2 __ 6 ii§ 

    .311                        AO39 A66/     O3       k6/fl3                         Y7k 1.33rYAIdI                   oI      Fol I          _       O        6b Y659 2     1                , dO37 022          WI                 /7                 Y
           ,             ,,YT ,&r
              /z
               /Ya o          43          02      w&voz

/Z/ ,. /Z3 l966i3 OZ WO'/Y 9 ___ 

                 .o' 1         02a3vc l3        oZ     Sj      l              f          6so0 1j/Y9          44moo oo I                 II          q            ISo L/4!/4L            S1odO3 o               O/         wLF                           A'i3S 4,,da3 6?           PhFa3                         .A/6J l/r opihlh                             0 0,161 01?117zuf 4o1B006/             FIl Mi)

Ot q__ _ Ur.Z3 __ z 2/x /.700onnol A 01_ 0l 26/6 Ato2/6 1Z

  • 06010O W/

vI LSJ6 t4A2A /PL 66oo/ 0// &o3 6J1 /rl ZAJ3 sr4Ad0 pd0/ 142.10 /0 _v_ ___ A/A.o2L oaoo1^o/ SiOS _r AXJ-T 3 Y/ o60 / I dF I /3 Pj3.7 4£ 2e 3 05J ,4OQp/ WO a -6S _ II'YA Da46/ 14 1 O . fOZ /0 AY4W v 12 g D <nciO/ d 52OOS9 2 J? Weo o la Fs37I30 

                   /        At/ 0zya 0/3 S3                         2 -Y 0 P04 oz/o, oz3V        /                /do            6J3'

Tennelec Sample Log Omaha VA Smear Analysis Date/Time Sample ID Quantity Batch Key Analyzed Counted by 12/Y1O 3 zooO / p e Ci / AXY/ /13Y/ ZOOD / 0-a W11I Z2 2 Y~S/ HZ/ZI /,rJ /t 7-0 oQ0 FOX 9/ X-rYP__ 12;1__L 2_ _6__AA_ 0 Z. _ 4-Ale Z04oq ,2 01 wo3sA L/ d Z!:2 tV A 22 4ILI/ F A Za 4pnp So6 Z (6 rr3x v iZ. 4 4 ioO2C/ SJoZ 2-Lf1i Z e avj6 Faq o51 1.3 ___7 AS-SR. 07 I ,,A ,- o OiIAZO OZW 4Zi1Z ___3___ h 44L4Z . 4. O  ! 02 -C- Ar2k -,- 

                            ~ .. ,1                              o 2-                                _                          ,

3444ot /'444d 180 yl ('2 i(f zz400~ (Jv( Ary J02 l1 -2: L.F 

  )k4S                                  14ev Y o2- SQO                                                        6s          Da 217/ t/Ooy                                         0/ fOl/                          i4.                 _       7_      D_

pnoY Ol WI Att tj __ __W 24 pp4 46 O wo2 . / IL. 

               £IY/ /3Ia                    1nYY/           w03                        6                  ____
            *1-i           , 5fi7 403/    ooZoOzI-So I 1 t                                               .

3 R?2f~1-wf2t '06 odz aI v Fo s6sr r2 */¢ oy3 4oi~r oi/ _____ Y 666  ; / lyt 

                           /(         4oofdl/ VOL                                        r Otc9j                 ',               A          vOpo         /                     '0                  ___         _
 ;'z/                                  eoon/ ) 9a/                                  _    _)  __  _          64-P-0 Z-/

I u/o L iqtj MO DO01 

                                      ?)oJO/6, 5oO0l jiY6 01 r

O /l2-01 6P 7 Of80i 

 ,,,/zi       ILi

________________________

  • a a

Tennelec (15632) Control Chart ' Th-230 SN 119739 32.00 7 ,  ! , i . . ti II  ; i I I ' I 1111 131 I I . -t E In EO3t 4 rtP, r tp qb p t* I T I3I 14 I II I I I 31.00 _I Fl 1111 11111l1111 I- . .-t I  ! , I IU-1 I .- I I I ' '-W-io' I, t I -* -t-- Lower control = 27.39% 0- .0 0

j lij
                                                                               . .I, Lower wamkig= 28.11%

iI :1 ij 

               -I                                                                                   I[

f lW -t. Ui-{ { Il il lII I cI-4 I- 41--- 1I-411 l r I Ihi 4 

                                                                                                                                                                ---0-*-

ci I ,i ilt a) 1- . I 

                                                                                                                                               . -              Mean = 29.54%
   ) 29.00                               i'                     I   . i II                         '; :-

I Ir i; 

                                                                                                                                               !j i
                                                                                                                                                    +I.

Upper waning = 30.97 III i i T IV - n- 3 28.00 T 7 I V11 . !I F T 'r T I I.1- 4 I Upper Control = 31.69% 0 0' 

              ;+           01/04                      4*      A. v                                                   AL                                    ,P I 1

27.00 Ii . .;. . ' 01i10 01/04 01/07 01/10 01/13 01/16 01/19 01/22 01/26 01/28013 January 2003 ) ) ),

Tennelec (15632) Control Chart Th-230 SN 119739 32.00 I G'O3TT I i ' ci 

                                          -i 3

l}w TI V~. I 3 go It 4 P @,I3 I- a- 1-r."iAR 1I3-i 31.00 I _I_ w' 

              -      Fl     I      . IA                Fl71 I      I   I 1   I-111-w W- -W'-I         I- 1        1-  _l          _-    I_
                               , i   i Lower control = 27.39%

F, 1 I" 

 %-  0 30.00 -          ,I       I Lowerwarning 2a11%

1 -C-- C.) I I---!D I ',i Pr4 1 }-{t{"4>{ tfitl *A>-fl4 -41 I-F II) I, III 4 !~-4 I 4 f-A I--I I- I 1-4: 4 4 Mean = 29.54% CD i 

 ._)

29.00 - L"- t 

                             -I                                                                                                                     Upper warning = 30.97 II Fly
I 9R nn ov vv T I..

IS 

                                                              !T               T T T-             vT        r      :1                 tf -tf I!

I1 Upper Control = 31.69% 1J 

                 'A     A
i. -

I II! *-1.-^II! lI I+ I A 27.00;

  • II
                                                                                                                           !  t 12/01           12/04 12/Ot            12/10 12/13 12/16 12/19 12/22                              12/25         12/28          12)31 December 2002

) ) )

Tennelec (15632) Control Chart I Tc-99 SN 119715 31.00 I . . I CP7 a-, co Il1 I I01,1,+~i If Eli C P f;iiJ -4 i i PJ I 3 a icW;4;J4 I  : I I i I i  ;, i 30.50 -- I.- 1-1 

                                - Iv T-I T-7-

I I I-I I -I it C F -- T-t , - t -+--t-+-+--- -+- A-I Lower conrol = 2879% I  ; 

                                                ;   1 II I

i 

  >, 30.00  -           I-      --      . 1-1     1--                                                                                              Lower warning= 29.14%

0 I IH )- -- 4 I-A I ifj I I III f -{j ib-tu -1i I 

                                                           ,X,
                                                                                   'I        i I--     I--( I--l-14W t*---{IJ3{J     III M*-A I

I Mean = 29.85% ci) Il i II C 29.50 - *I I Ii Upper wafling = 30.56% I r--* -- tFt y I 

                                                                        ,i I .! ,,         I 1
                                                                                                 '--9  I-W     v         W*    V -I I  42 I                                                .t                -Urn          3.

29.00 I i + Upper ConW = 30.91% A - A 4 4 T!i 4 tL A A4 . 1- . . . 28.50 I2/10 Ii I I1 / .2,0J .2/ I 2/01 12/04 12/01 12/13 12/16 12/19 12/22 12/25 12/28 12/31 December 2002 ) ) 3

Tennelec (15632) Control Chart , Tc-99 SN 119715 31.00 I 41 mW i W i

  • II
t m i 4~I  ! ,3  : CO qlP "_i w

1P m I.!i 

                                         '! 1, Iil i  I I

I 1 1 30.50 I I-'T. . Ii  ! I I I I Ii T I I I 7 tv II 0 I. I I I I I I- I I l Lower control = 2a79% I I I i I  ! 0 30.00 -1 Lower waming= 29.14%

i :l !tl tA-1--qI- iI--{I Il iksI (jl -tP fP - F-t0i-i I-. I III -{ } IlI- I III [-{

ci i i I i I I -C-Mean = 29.85% 

 *5 29.50 -        i       I:         I i

Upper warning = 30.56% l, i r-Iv! I T F j I , I F -- -.- 29.00 Upper Conlrold 30.91% 

             .TT                               ! 4 I

I! I 

                                                                                                                  !    A
           ~A4; :                                                   AL                    A, 4                    . I    .
                                                                        !     IiI -
             /! 1                                                                                                              i,I 28.50  i .     .

013 0)1/01 01/04 01/07 01/10 01/13 01/16 01/19 01/22 01/25 01/28 January 2003 ) )

Packard Tri-Carb 2550 SN 401663 Duratek, Maxey Flats Disposal Site Type of Count TrItrum (3ml 12ml geometry) Source Control SEG # 029709.01 Month of December 2002 5DAY OF] H3 1 H3 BKG 5 NTASFILE NAME COMMENTS IMONTH CPM IEFF ICPM ]IITAL SDATAlx~i= 3 12518.40 0.422 18.85 TP 0.134 4 12646.50 0.427 16.49 TPKS 0.135 - - _ _ 6 12457.90 0.420 17.26 KS 0.136 6 12451.70 tl:420 17.01 TP 0.137 7 12541.80 0.423 16.97 KS 0.138 _ a 12513.4 0.423 16.72 KS 0.139 9 12380.80 0.418 18.16 KS 0.140 10 12398.90 0.419 17.03 KS 0.141 11 12351.50 0.417 17.31 KS 0.142 12 12308.00 0.416 16.08 KS 0.143 13 12316.20 0A16

  • 17.09 KS 0.144 16 12605.20 0.426 17.81 TP 0.145 17 12542.60 0.424 16.65 KS 0.146 18 12591.40 0.426 15.95 KS 0.147 19 12592.00 0.426 16.70 KS 0.148 20 12582.70 0.426 17.1. KS 0.149 _

21 12535.40 0.424 15.98 KS 0.15 22 12430.00 0.421 17.07 KS 0.152 23 12427.10 0.421 16. KS 0.153 27 *1235120 A.18 16.66 TPKS 0.154 28 12363.60 0.419 16.76 TP _0.15 29 12390.20 0.42 16.94 KS 0156 30 12345.50 0.418 16.75 IKS 0.157 Comment.: 3 I Reviewed by% i,. Date-J2a J3 AHK o3-T O X A3 VolSSL8909 Xad ZcC:T Co/LO/lo Zo Z road sILY1A

( ( C It TRI-CARB 2550 #401663 BACKGROUND 3 ml Water to 12 ml Ultima Gold LLT 26 X:24 0:= 22 I 

      ~2 a  20 c
      -g 18 O,,

16 14 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 1E 19 20 21 22 23 24 25 26 27 28 29 30 31 December, 2002 l a-- -3Sigma (14.63) -2SIgma(16.41) -- Mean(19.96) +2Sigma (23.52) +3Sigma (25.29) 

   .r                                              (                                       (

U.1 TRI-CARB 2550 #401663 H3 EFFICIENCY 3 ml Water to 12 ml Ultima Gold LLT 0.428. 0.426 0.6424 

        >0,422 0.42 0.418 U*0.416 q4          0.414 0.41 1 2 3 4 5 6 7 B 9 1011 12 13 1415 1617 18 19 20 21 2223 24 252627 2829 3031 December, 2002
    ---  -3 ,Slgma (0.412)    -2 Sigma (0.415) {-c Mean (0.420)      +2 Sigma (0.424) -  +3 Sigma (0.427)
  .      -     .1

CALIBRATION AND TEST REQUREMENTS FOR REDS-INST-104 RADIATION PROTECTION INSTRUMENTATION REVISION 0 

'LWo                                                               ATTACEMENT 6.3 RESPONSE TEST FORM (example)

Instrument Instrument 1D Pass Fail Performed by Date (lf ._ ,, _ , . - 4LJ-)/ J ,3v VI _ i I Lz~J .4 

                              /-77         __      _      __     _   _              1   ____3/     T'y                         /3 o

Lv~~l cX -b337 §X 

           ,       _   __                    __                               7     .

I111,10i Lti l77 / c96337T?, zz(/V-7/O7/ i~w (4- Ui7 7 /__ - ,t- 7/V L~cY22 2a/17S337 

                                                                       .2/i.__

I e .- L ~- fe;I/ 4 

                                                                                                                          ~i-tZ$-o7             o R /337           _             _                4v4,.                               07
                        .,_        _               4337                    V                                 A I' Z,:                                                                              V.            -,          .     ,0 li/77 /1-C357
                          -.                                              /C                                               a PL3  '3         7             J..                                                 I .

tiO-g'o, 

                                              ._        _    _     _      V     /   v  _     _   _                         f g ? 4/         tRa )

L>9 L2 -Z3 2 2 / ___ b8,e .4tL ^//XG50C (a2763 

   -    --                                                     Reviewe by                          Datd 1 of 1 REDS\PROCINS1MOS "MDMPOCUNSMIX04                                              1 of 1

- CALIB¶ION AND TEST REQUIRENTS FOR REDS.lI ;T-104 RADIATION PROTECTION INSTRUIMTATION ' REViSION 0 ATIACHMENT 6.4 INITIAL REFERENCE RESPONSE TEST FORM (example) Instrument Model Number: InA'/9? 

                                                                                          'nstrument     ID: 54       G                >.

Scale or Reference +/-20% Value of Jig and Source Decade Reading Reference Reading. ID Number Geometry Remarks 4&1Ard- ___' __ 7t e 3 o 70cOce ____ AO r9< A4/ .W e11-7* I l Performed by/Date IReviewed by/Date /7t'oe YYED8%PROCUNS%104.0 1 of 1 J )

AM Duratek-CALIBRATION CERTIFICATE vtek Instrument Semvices 628 Gallaher Road Kingston, TN 37763 Phone: (865) 376-8337 v) Fax: (865) 376-8331 This Certificate will be accomnanied bv Calibration Charts orRendinq uwhere amlicahle CUSTOMER INFORMATION  ;,  :.  :  : -- INSTRUMENT INFORMATION - Customer Name: Duratek Instrument Services -Manufacturer: U..L = Address: 628 Gallaher Road, Kingston, TN 37763 Model: 177 Serial Number 26337 Contact Name: Thomas Scott Probe: 44-9 Serial Number: 016220 Customer Purchase Work Order Calibration Methoda Order Number. NIA Number. 2002-00893 Electronic and Source INSTRUMENT CAMIBRATION IN-O;MATION - Calibration Standard Instrument comments Instrument Value Response Range Before After Calibrated in accordance with Calibration Calibration RP-INS-I-235 X1 100 100 100 Pulser 120935 Cal Due: 03/18103 X1 250 250 250 D-814:2551 CalDue 09/12/02 X1 400 400 400 Psychron 7480 CalDue: 05J17/03 X 10 1,000 1,000 1,000 X 10 2,500 2,500 2,500 X10 4,000 4,000 4,000 Temp: 2L4°C X 100 10,000 10,000 10,000 Pressure: 745mmHg X 100 25,000 25,000 25,000 Humidity 56% X 100 40,000 40,000 40,000

Background:

60cpm X 1000 100,000 100,000 100,000 Threshold: 37mV X 1000 250,000 250,000 250,000 HY (As found = 903V) (As left 903) X 1000 400,000 400,000 400,000 BAT: SAT Volu m e SAT 

                                        .-..Et   c1l,~ In,~flir         -       -      -                       .:..Audio SAT         Geotropism: SAT X 1 EFF                          Tc-99#119720              2,562dpm                 11.7%          FIS Resp: SAT          Alarm: SAT X 10 EFF                          Tc-99#119718             20,S20dpm                 11.5%          HlV Test: SAT X 100 EFF                          Tc-99#099606             177,000dpm                11.3%          only. Use       Xith 44sl probe.

AVG EFF N/A N/A 11 5% 

                           ';-,-,            -           S      TA-TE MNNTOFCR   0                 ATON:Rte TX                     -

WeC i that the instrumcat listed above was cdibrated and inspectedpriorto shipmeat and that tnut al the Manufaduius published axrating specification We fnthr cmtiy th our Calibration Measurnits are tceableto theNaticnal htibe of Standards and Tedmology. (We are not reiponsible for damage incurred during shipns or use ofthis instrumncrt Instrument CalibratedBy: Reviewed By. ( 6'(477 Date: 7_ -Z, "alibration Date: 07124102 CaIbr t o u: 0 40 I Calibration Due: OU24103

a  : 4o no"e fmmf Ch.~ of Custody Record CN° 1379 601 SmabaM 11usd O Mdt% N mm tu48141683 Pbt" e W)48f21 Fax 

                                                                                                                                                   >   E-EIRLINE X            EflVICEU Prfect NamSpVwtO1bO'm                                                                     /       /       /    /        /        /     /    /   /0030 send Report To:            r          Bampler (Pdnt Nam   (

ae): / Addrse b f AL Sanrier (PttNt Name): 

   /&gsfr,71 37763                   Smmmmeteod:          Fe-A          -/

Mbmbe 83754 1563t ///5 oe .376- 7 LM Rece:tv ektt &J4t, I/ Far. ,_7-6__7  ; _ /Special ID so" sampleto Sr MCI I I 2h Coners / L / / / by WbI VA1-0.1- 01Q7b Il-m (t0o 100 f_ _ i6wA I-- __ V. It ____ ____

_ a _ - I _ _ _- - I
-Reli~nqmso ImReceived                      &F.PS~lavue)              Dte;       rw        Sampl cus-o--- Rsa- (Co"Mpll                By Labon"or).

CAMQ Level Tuerwrmtid Sample Rewept ____ Refny S0aue-reived se U~r. (Sigature) ae: ToWa # Contaher Rleceied _Lel Level_tie I 0 _ N 0_tact? 0 COC 24 Hur 0 _ WC Sea_ Seas Prese? _ h.. bSt Leve 

                                                                                           .Oe       III 0a_tue?
                                                                                                            = ' 1 Weak - 0        Re~ C_aer__s Wtad_?

Tem_ _ ___

SAMPLE IDENTIFICATION AND REDS-CEM-101 CHAIN-OF-CUSTODY REVISION 2 C.OP.* YA-oo1 ATTACBMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: i/haJ Ce. Al, for: Z)WttiL' (Mo-c -AA) sute Contac Addres: Phone: Sample Sample Collection Collection Remarks Number Location Date Tume 3A 5 -xq 1Oq &OOOC) -- i 

              - A5 o1i       _   _ oo_ WC(

_ lW-(3-oz p)4co 50 - t[3 Acct 1bi(Ajjc) II- jj- 02-C JW Co 4-q A ooo 1b1 I1,_j-pz '4e6 

          * -   *11   > Aoo W 6o I               I(- 1-o2       I 14-2

(- 1Aoolo ISo 503 II- ts-ca J4° (f6-12t A4 000 foI503 11-19-6Z W~oo 1 of 1 REDsPRQcsxcI-1o1 .2 REDSPPROMSCHM-101.2 1 of 1 

,I
      '4 SAMPLE IDENTIMCATION AND                                                       REDS-CHM-101 CHAIN-OF-CUSTODY                                                                   REVISION 2 C.O.C. # YA-o2-ATTACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) 6ZI7)dcc, CA<,dfor:       3u)1-at)

Collected by: (Affaak- -Y) Site CoutaC- Addrs: Pbonce Sample Sample Collection Collection Remarks Number Location Date rune J-9 coZ Ci1 4, I1-Z-o2.. i4L0 #+1_ 1-11 Awoo2 01 I- 

                                                    !1-01z2      140            15oo 4Ss.+

I Ao~o2ozo I I-,LI 0 1500 __41_ Atx 2- 6i tooz I-Sozo ___^6._ 4csoc 2O fJ'p 1(-a(-o2 (5oo s4a- Ago 4&E0 2 1 )vo5 -o 1500 + f,4-1 Ac0o2d~oZ A t 02 

                      \   Aoo 2 ft66)    3I-Al1             -02  15:3CX_

F -'_ _ i f i i j I I i i 1 of 1 REDSPROcSCHM-1QI .2 REWSvPRocSICWM-IOI.2 l of I

SAMLE IDENTIFICATION AND REDS-CHM-101 CHAIN-OF-CUSTODY REVISION 2 C.o'C4 4V403 AITACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: PlS ZA Ro for: -DWLQ-te 0Mh 7 Ste Contact Addcus: Phonc: Sample Sample Collection Collection Remarks Number Location Date Time I r -30 N 4oon FE I !l-o0 16 so BI' Ac, J-30 N002Ov 1W £I 1- X I DA 1(630  :- :a 2- l 

                      \A 1 of 1
                   .2 REDSPROCHM-1O1 REMSPROMSCHM-101    .2                          1 of  1

SAMPLE IDENTIFICATION AND REDS-CMA-101 CHAIN-OF-CUSTODY REVISION 2 Cc,43*, j ATTACHMEN 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: P. SZXRO for: J U a) (c t S9te Contactr Addrew: lPhone: Sample Sample Collection Collection Remarks Number Location Date Time 

                /-39      B~o /J/ i~            _______t           0&7         $

_______ 05, /01 L I - Bc lot wol II-.25^.OL 0830I LAl-lof I RDs\PROcS'CWA-1O1 .2 REDSTROMCMA-101.2 1 of I

SAMPLE EDENTIFICATION AND REDS-CHM-101 CHAIN-OF-CUSTODY REVISION 2 ATTACEMENT 6.1

  • Y160-5 CHAIN OF CUSTODY RECORD (example)

Collected by: P. b'poz for:, YA.) SAtC Contad Add: nhone: Sample Sample Collection Collection Remarks Number Location Date TIme __ _ _ __ __ ' ~ ___ ofe 2-- 48 J/ocxI& kiol t/-.lTz c847 _ _ _ _ _ _ _ _ 1__ 4 _ 1__ 1 of I 

                      .2 REDSPROcSCHM-1OI .2 REDSPROCSCHM-10t                                       1 of I

SAMPLE [DENTIFICATION AND REDS-CIM-1l1 CHAIN-OF-CUSTODY REVISION 2 C.o,c. 4Y&6 ATTACBMIENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: L.Wt2c IA for: DA.raTe K (OMA h A 7yAJ MSU

Contact:

- d u lhoac: 'dd._ . Sample Sample Collection Collection Remarks Number Location Date T~ime 

        .          it                    RlI-WdI1X-O-2

______ MmMX a-5-31 B Io 11 10I 1-,U 02- °gm1 32i4L1 ?MO 103 w 1 -JL-aL DlQ2 

             *pa                                IO 3- I-rA                                I l-ato -02                   09oqB 1     I 0i-43 sil ,                         I-,;.                             t                  >-fo i

i i t I t i i i CUSTODY LOG icSa(rae . Date/Time I u. 

                                                                                                                                                -relime C

__ _ _ _. _ _ _ _ _ _ _ A _ _ _ _ _ _ _ _ 4cEqcpy f ll. , ;Per-quis d /o; k9AJ:W I i _r . 

                                             ,,   x         I i                                                       __=
                                                                                                                                                  .wlnni .I
                     -.      r                                 -P "P -- 5'5   fnl  -0,11        4-91    -. T      - ----

oYg' 

         ,       t        Iff/,t                  ,~

I 

                                                              ~

X Rc~nqd . . tA f1ri 9 \ - Rdtq!e b\sK< A 1 of 1 REDs\PRocs\cHM-1o1 2 .2 REDSTaROMSCHM-101 1 of I

SAMPLE IDENTIFICATION AND REDS-CHM-101 CHAIN-OF-CUSTODY REVIION 2 ot.0 t 7'4-6O7 AITACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: '3a/A& /J., for:1 zA) (8gl2. - Y,4 Ste Contac Add: Sample Sample Collection Collection Remarks Number Location Date Tume 

                /^1o     Aoo3 t{ 2wI /                                           ij.oZ    / i iif
              /1-17      Aocwc.3 O°        JO2. __       -_2__     Moo__   _1

_J2 02? W40 OZ;G0 /d~oo A2533 eo340 39 l@u 02- lo_ 34-57 Aooo3 oz Fe t //-96 '02- /1eo._ r ______ Aco3og So/ Jl@-o2_/o ___-_7 _ Aooo3 AL 622 // a2 62- /~,o -REDSXR ~c~M11. 1 of 1 I

SAMPLE IDENTIFICATION AND REDS-CH3M-101 CHAIN-OF-CUSTODY REVISION 2 C.0,e, yx _00, ATTACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: J 4 , 

                                          £4c    for:       cLa             )   (0oa          c   y, 4.)

Site Contacu Addr-s hone Sample Sample Collection Collection Remarks Number Location Date TImeI 1-,4 A6eo3 O/ w J // -2. oZ /C)30-36 _ -_/Z Aowo3 e/ck/2L / .oe' 424 __3_-___ A6 6e3 ofbV405 ___4_02_ 1030 40 /lo O/ 114- 

                                                           /k -202                110I30 o5 3              Acoo3o     y, j           ____-o2                     /1430
               .1                       r CUSTODY LOG                                         _-
                   '!--M~ame               l~aterrune                    r                            D~tte/lTime
       ,U                '1                      Ifg 3.w~
                                                 /zd              r         tJX                                /

Rclnqizlhcd 5db - Awp by . q d by V-Ac-pted by Rdeinquised by 1 of I R.EDs1PRocsoIM-lO1 .2 REDSIPROMCSCM4-IOI.2 1 of I

SAMPLE IDENTIFCATION AND REDS-CHM-101 CHAIN-OF-CUSTODY REVISION 2 C.e'.C VA--, QO ATTACHMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: bJa7dd A*A'W for: )c ) C cAc_ Yg sact Coetacu astsJ Adder: ftouc ____________ Sample Sample Collection Collection Remarks Number Loction Date Tume _ ._ 

            /-5osC~p            Bak          :

eJ / 

       \_ _  _ _ _ _ _ _ _ _ a _ _ _ _ _ _ _ _ _ _ _ _   _ _ _ __ _ _ _ _ _  _ _ _ _ _ _ _ _1
                                                                                                                         ":I 1 of I Ie.EDsXPRocS'cKM-1o1    .2 REDS~TROCSCHM-101I.2                                                   1 of I

SAMPLE IDENTFCATION AND REDS-CHM-101 CHAIN-OF-CUSTODY REVISION 2 C,eO. C 4* A-YA.15 AITACH}MENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: 2 4, for: a 14 , S6te Contaet: Addrus: Phone: Sample Sample Collection Collection Remarks Number Location Date Time 

     -                    Acro'FOIPOI-olpZ 'o-           .v-o.        ______

A--pWby., a~db CUSTODY LOG Name Date/Time IName Date/T"Ime A~eP by eriquisled by 1 of 1 REDSnQcscHM4o1.2 MMM\POMCSCM 1012 1 of 1

SAMPLE IDENTE[CATION AND RE:DS-CEM-101 CHAIN.OF-CUSTODY REVISION 2 e- 74-,0V ATTACHMENT d.1 CHAIN OF CUSTODY RECORD (example) Collected by: C' , ,A-for  : &97 - Ao.- 1/4 (&7'iA Sift

Contact:

drs: A Pbonc: Sample Sample Collection Collection Remarks Number Location Date Time 1* 3 AJ10101X'O /o-I 5--e2 ~ ___

  • 6-7
              ._                                                                            11
                    .     /3                                      nqui503d by CUSTODY LOG____

Name Date/Time NmDate/Tune Colected by ~. i A o ______ 

     .         byV                                             7 Acceptedby                                                Refnquished by 1 of 1 REDSNPROMSCHM-101.2.2 REDSPROcS'CHM-lOi                                           1 of 1

SAMPLE IDENTIFICATION AND REDS-CEM-101 CHAIN-OF-CUSTODY REVISION 2 

                                                                                                /j ATTACHM 6.1 CHAIN OF CUSTODY RECORD (example)

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Sample Sample Collection Collection Remarks Number Location Date Time 

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SAMPLE IDENTIFICATION AND REDS-CHM-101 CHAIN-OF-CUSTODY REVISION 2 C.@. C wY4 - 012, ATTACEMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: , r _rfor: y; 6met A4 - )'4 (Z= ) Sdte Contad: hAdd  : Sample Sample Collection Collection Remarks Number Location Date Time 1 -4 2co / c5/6 / 42-5-o 2- /6 0 a 4 n' 40/we / 1 1 /10 / O J)e3 J/___ cJeX we __ 

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SAMLE IDENTIFICATION AND REDS-CEM-101 CHAIN-OF-CUSTODY REVISION 2 ec'.c--A* VY,#-O ATTACENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: %Yfor: A4/da/ at 74. (4i-cki ISite CentId- Addrs: Pbanc___________I______ Sample Sample Collection Collection Remarks Number Location Date Time 1- Ace. '/_ /.63k Z -*-oz / _____ 2A - _ _o __ _ _ 3 wez 4 bS ________=__ 9, I__I_-___ 2I _ w02- = _= = t3 I f ____ I _ - ~ ___ __ ___ ____ I? ___/_____Sd3_____ ____ CUSTODY LOG Name Date/rTme Name Date/Time Coepted by .in_2-d ( 7 y by 7/ A brR

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                     .2 REDS?RocS'Cm4-1O1 1 RMDS\RO;\CHM-101                                               1 of 1

SAMPLE IDENTLFICATION AND REDS-CIM-101 CHAIN-OF-CUSTODY REVISION 2 g.c,-Xq-c142 ATIACBMENT 6.1 CHAIN OF CUSTODY RECORD (example) Collected by: e. ,' for - - /4-4f ) Shte Contact, jpAd:dm-- Sample Sample Collection Cohlection Remarks Number Location Date Tume 0 Aecc41/4-ZAe/ /-2 0 193 _-__ 6 / 0e'P, We 4 0; ooz S 7 I_______I__ 

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                                     -_                               CUSTODY             LOG Name                               Date/Time                                     Name                    Date/Time
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