ML031140505
| ML031140505 | |
| Person / Time | |
|---|---|
| Site: | Susquehanna  |
| Issue date: | 04/17/2003 |
| From: | Susquehanna |
| To: | Document Control Desk, Office of Nuclear Reactor Regulation |
| References | |
| Download: ML031140505 (103) | |
Text
Apr. 17, 2003 Page 1
of 1 MANUAL HARD COPY DISTRIBUTION DOCUMENT TRANSMITTAL 2003-19757 USER INFORMATION:
GERLACH E X EMPL#:28401 CA#: 0363 Address:
SA Phone#:
54-3 TRANSMI TAL INFORMATION:
TO:
GFRLACIIR3 M
04/17/2003 LOCATION:
DOCUMENT CONTROL DESK FROM:
NUCLEAR RECORDS DOCUMENT CONTROL CENTER
'NUCSA-2)
.'HE FOLLOWING CHANGES HAVE OCCURRED TO THE HARDCOPY OR ELECTRONIC MANUAL ASSIGNED TO YOU:
115 -
115 -
CHEMISTRY SAMPLING TEAM: EMERGENCY PLAN-POSITION SPECIFIC PROCEDURE REMOVE MANUAL TABLE OF CONTENTS DATE: 03/11/2003 ADD MANUAL TABLE OF CONTENTS DATE: 04/16/2003 CATEGORY: PROCEDURES TYPE: EP ID:
EP-PS-115 REMOVE:
REV:13 REMOVE: PCAF 2003-1010 REV: N/A ADD:
REV: 14 UPDATES FOR HARD COPY MANUALS WILL BE DISTRIBUTED WITHIN 5 DAYS IN ACCORDANCE WITH DEPARTMENT PROCEDURES.
PLEASE MAKE ALL CHANGES AND ACKNOWLEDGE COMPLETE IN YOUR NIMS INBOX UPON RECEIPT OF HARD COPY. FOR ELECTRONIC MANUAL USERS, ELECTRONICALLY REVIEW THE APPROPRIATE DOCUMENTS AND ACKNOWLEDGE COMPLETE IN YOUR NIMS INBOX.
'PROCEDURE COVER SHEET PPL SUSQUEHANNA, LLC I NUCLEAR DEPARTMENT PROCEDURE l
CHEMISTRY SAMPLING TEAM EMERGENCY PLAN EP-PS-115 POSITION SPECIFIC INSTRUCTION Revision 14 Page 1 of 4 QUALITY CLASSIFICATION:
APPROVAL CLASSIFICATION:
( ) QA Program (X)
Non-QA Program
( )
Plant /",
l
,(
) Non-Plant (X)
Instru ction /
EFFECTIVE DATE:
1/ cZL23 PERIODIC REVIEW FREQUENCY:
2 Years PERIODIC REVIEWL;DUE DATE:
_/
RECOMMENDED REVIEWS:
A' ALL Procedure Owner:
Nuclear Emergency Planning Responsible Supervisor:
Chemistry Supervisor-SSES Responsible FUM:
Supv.-Nuclear Emergency Planning Responsible Approver:
Vice President-Nuclear Operations FORM NDAP-QA-0002-1, Rev. 3, Page 1 of 1
EP-PS-1 15 Revision 14 Page 2 of 4 CHEMISTRY SAMPLING TEAM Emergency Plan-Position Specific Procedure WHEN:
All Phases, Alert or higher HOW NOTIFIED:
Plant Page System REPORT TO:
Chemistry Coordinator WHERE TO REPORT:
Control Room and then TSC OVERALL DUTY:
Collect and analyze samples to obtain data required to manage the emergency.
MAJOR TASKS:
TAB:
REVISION:
BRIEFING, ASSIGNMENTS, AND PREPARATION OF RADIOCHEMISTRY LAB(S)
Report for briefing and assignment(s)
TAB A 8
Prepare In-Plant Chemistry Lab to accept TAB B 4
samples Prepare West Building Chemistry Lab to TAB C 6
accept samples PASS SAMPLING AND ANALYSIS PROCEDURES Prepare Post Accident Sample Station (PASS)
TAB D 9
for sample collection. Secure PASS after sample(s) have been taken Collect Small Volume Liquid Sample(s) from TAB E 7
PASS Collect Dissolved Gas Sample(s) and/or Large TAB F 8
Volume Liquid Sample(s) from PASS Collect 14.7cc Gas Sample(s) from PASS TAB G 7
Collect Iodine/Particulate Sample(s) from TAB H 5
PASS Prepare and Analyze PASS Small Volume TAB I 6
Liquid Sample(s)
EP-PS-1 15 Revision 14 Page 3 of 4 MAJOR TASKS:
TAB:
REVISION:
PASS SAMPLING AND ANALYSIS PROCEDURES (continued)
Prepare and Analyze PASS Dissolved Gas TAB J 7
Sample(s)
Prepare and Analyze PASS 14.7 cc Gas TAB K 7
Sample(s)
Prepare and Analyze PASS Particulate and TAB L 4
Iodine Sample(s)
VENT MONITORING AND ANALYSIS PROCEDURES Collect SPING Sample(s) from Vent TAB M 6
Monitoring System on Reactor Building 818' El.
Collect Sample(s) from Post Accident Vent TAB N 9
Sampling System (PAVSS) on Turbine 729' EL.
Prepare and Analyze Vent Monitor Sample(s)
TAB 0 7
ADDITIONAL TASKS Collect and Analyze Sample from Reactor TAB P 5
Building Sampling Station. Sample has potential to be highly radioactive.
In the event of an Unmonitored Liquid TAB Q 6
Release, collect and analyze Liquid Samples RHR Service Water samples when RHR TAB R 5
Service Water is in service but RHR-SW rad monitor is inoperable and normal sample point is unavailable
EP-PS-1 15 Revision 14 Page 4 of 4 SUPPORTING INFORMATION:
TAB:
Emergency Telephone Instructions TAB 1 Emergency Organizations TAB 2 Logkeeping TAB 3 Sampling Requirements Based on Key Indicators TAB 4 Intentionally Blank TAB 5 Area Radiation Monitors TAB 6 PAVSS Instructions TAB 7
REFERENCES:
Post Accident Sample Station User's Manual, GE, NEDC-24889 General Electric Post Accident Sample Station Manual, GEK-83344 CH-CC-01 0, Chloride - Silver Nitrate Turbidimetric Method CH-CC-030, Laboratory pH Determination CH-CC-040, Hydrogen By GC Ch-CC-043, Analytical Procedures for HACH or BETZ Portable Spectrophotometer Labs CH-GI-051, Instrument Checks at the Offsite Chemistry Lab CH-RC-010, Iodine Counting and Data Analysis CH-RC-01 6, Particulate Filter Analysis CH-RC-071, Radiochemical Analysis of High Activity Iodine Cartridge Samples CH-RC-076, Gamma Spectral Analysis Using the ND 9900 TS 5.5.3
TAB A EP-PS-1 15-A Revision 8 Page 1 of 6 MAJOR TASK:
Report for briefing and assignment(s).
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
Immediately report to the Control Room unless otherwise directed.
- 2.
If directed by the Shift Manager to obtain a Reactor Coolant Sample, obtain the following information from the Control Room:
2a. -
Obtain the following information from the control room:
Ask if RWCU and/or Reactor Recirculation Systems are isolated.
If RWCU or Recirc are isolated, proceed with the following steps to obtain a PASS Sample.
If RWCU or Recirc are NOT isolated, proceed to Step 5(b)4 and TAB P to obtain a sample from the RB Sample Station.
NOTE:
If the reactor is pressurized obtain a routine coolant sample from PASS. If the Reactor is depressurized obtain a PASS sample from RHR.
(1)
Reactor Pressure:
psig (2)
RHR Mode:
RHR Pump A & C In Service / Out of Service (circle)
RHR Pump B & D In Service / Out of Service (circle)
(3)
If a RHR sample is requested, record date and time RHR was placed in mode to be sampled.
TABA EP-PS-1 1 5-A Revision 8 Page 2 of 6 SPECIFIC TASKS:
HOW:
INITIALS
- 3.
Upon activation of the TSC report to the Chemistry Coordinator.
- 4.
Obtain briefing and assignments from 4a.
The following information:
the Chemistry Coordinator.
(1)
Team (2)
Required samples and analyses:
4b.
If PASS samples are requested, obtain the following information:
(1)
Reactor Pressure:
psig (2)
RHR Mode:
RHR Pump A&C In Service/
Out of Service. (Circle)
RHR Pump B&D In Service/
Out of Service. (Circle)
(3)
If a RHR sample is requested, record date and time RHR was placed in mode to be sampled.
4c.
If PAVSS samples are requested, perform the following:
(1) Contact l&C to reset flow totalizers on PAVSS prior to sampling.
TABA EP-PS-1 15-A Revision 8 Page 3 of 6 SPECIFIC TASKS:
HOW:
INITIALS (2)
Initialize appropriate PAVSS and place corresponding SPING in STANDBY.
HELP PAVSS Instructions See TAB 7 (3)
Record time of reactor shutdown.
Shutdown Time:
4d.
Record laboratory to be used for sample analyses and begin lab preparations:
HELP In-Plant Chemistry Lab Prep.
See TAB B HELP Offsite Chemistry Lab Prep.
See TAB C 4e.
Record extension number where Chemistry Coordinator may be contacted:
Ext. # _
- 5.
Obtain briefing from Radiation Protection Coordinator or designee.
5a.
Sign in on RWP # YYYY-8000 series unless directed otherwise; in that case, Obtain Emergency RWP and record the following:
RWP#
Team Members Allowable Exposure
TABA EP-PS-1 15-A Revision 8 Page 4 of 6 SPECIFIC TASKS:
HOW:
INITIALS 5b.
Perform the following special actions, if applicable:
(1) If collecting a SPING sample, obtain and record ARM readings on Reactor Building 818' El.
(2)
If collecting a PAVSS sample, obtain radiation readings from Turbine Building 729' El. And record.
(3)
If collecting a PASS sample, obtain radiation readings from Turbine Building 729' El. and record.
TABA EP-PS-1 15-A Revision 8 Page 5 of 6 SPECIFIC TASKS:
HOW:
INITIALS (4)
If collecting an RBSS sample, obtain and record radiation readings in sampling room, or from ARM's nearby, if available.
5c.
Determine best route to and from sample point by performing the following:
(1) If cart is required to transport sampling equipment, confirm elevator or appropriate building may be used.
(2)
Record recommended route to and from sample point:
(3)
Record any pertinent technical conditions which could affect sample collection:
TABA EP-PS-1 15-A Revision 8 Page 6 of 6 SPECIFIC TASKS:
HOW:
INITIALS HELP PASS Sample(s)
See TAB D HELP SPING Sample(s)
See TAB M HELP PAVSS Sample(s)
See TAB N HELP RBSS Sample(s)
See TAB P HELP Unmonitored Liquid Release Sample(s)
See TAB 0
TAB B EP-PS-1 15-B Revision 4 Page 1 of 4 MAJOR TASK:
Prepare In-Plant Chemistry Lab to accept samples.
SPECIFIC TASKS:
HOW:
INITIALS NOTE:
All contaminated or potentially contaminated personnel and samples should enter In-Plant Chemistry Lab through North Door onil.
- -oies
- 1.
After briefing and assignment, construct necessary lead brick shielding for sample storage and preparation.
1 a.
Construct lead brick shield in Sample Preparation Room fume hood to store radioactive samples and sample dilutions.
1 b.
Construct lead brick tunnel as shown on Attachment A, Suggested Cave/Tunnel Designs, in In-Plant Chemistry Lab fume hood closest to Sample Preparation Room.
- 2.
Obtain necessary supplies.
2a.
Obtain the following supplies:
pH meter and electrode Dilution vials Liquid syringe or Eppendorf pipettes, 1.0 ml, 0.1 ml Gas tight syringes Vials, gas and liquid Septums Capper and decapper 0.01 N Nitric Acid (HNO3)
Labels and markers Bench coat Paper towels Tongs Plastic wrap Bags Survey Meter Vacuum grease Remote handling tool(s)
Cotton gloves Plastic gloves Radiation tape Yellow trash bags
TAB B EP-PS-1 15-B Revision 4 Page 2 of 4 SPECIFIC TASKS:
HOW:
INITIALS 2b.
Store supplies within access of Sample Preparation Room fume hood.
- 3.
Initiate Emergency Sample Log and Event Log.
- 4.
Obtain equipment from In-Plant Chemistry Lab for contamination control:
4a.
Obtain the following supplies:
Herculite Step-off Pads Duct tape Plastic booties Plastic gloves Frisker Survey Meter 2 Containers for used protective clothing NOTE:
If unable to locate equipment, notify Chemistry Coordinator of needed supplies.
- 5.
Prepare Sample Preparation Room to receive radioactive samples.
5a.
Place step-off pad as shown on Attachment B, In-Plant Chemistry Lab.
5b.
Cover floor with herculite as shown on Attachment B.
- 6.
Complete In-Plant Chemistry Lab preparations.
6a.
Place containers for used protective clothing at each step-off pad.
6b.
Place clean plastic gloves, booties, and lab coats at North Door for donning prior to entrance to Sample Preparation Room.
TAB B EP-PS-1 15-B Revision 4 Page 3 of 4 ATTACHMENT A SUGGESTED CAVE/TUNNEL DESIGNS LEAD BRICK TUNNEL 18 ini 36 in.
LINE LINE l NT IA3" D
VENT MONITOR SAMPLE HOLDER
{
TOPVIEW SURVEY METER (IONIZATION CHAMBER)
END VIEW 4
23" 4
41" I
I I
I
_I
._,_*_I I_' S/is/1// I I
-II I I
I I
E
-- I SIDE VIEW
TAB B EP-PS-1 15-B Revision 4 Page 4 of 4 ATTACHMENT B IN-PLANT CHEMISTRY LAB
TAB C EP-PS-1 15-C Revision 6 Page 1 of 8 MAJOR TASK:
Prepare West Building Chemistry Lab to accept samples.
SPECIFIC TASKS:
HOW:
INITIALS NOTE:
If the security at the West Building is tripped while accessing the building, contact Corporate Security at the General Office ETN 220-5296.
- 1.
Obtain access to the West Building 1 a.
Obtain the key for the West Building from the cabinet in the Technician's office area.
or Contact Security and arrange for them to unlock the West Building.
1 b.
Obtain the security access code from Chemistry Management.
1 c.
Contact Health Physics:
(1) to determine if a Health Physics technician will accompany Chemistry to Offsite Chemistry Lab in order to perform surveys.
(2) to determine if there is a preferred route to the Offsite Chemistry Lab.
(3) to obtain frisker and other equipment that may be needed at the Offsite Chemistry Lab.
NOTE:
If gates need to be unlocked, contact Security to arrange for access.
1 d.
Proceed to the West Building.
TAB C EP-PS-1 15-C Revision 6 Page 2 of 8 SPECIFIC TASKS:
HOW:
INITIALS NOTE:
If the next three steps are not performed within 30 seconds, Corporate Security will receive an alarm.
1 e.
Unlock the front door to the West Building.
if.
Proceed through two (2) doors.
1 g.
Enter access code using the keypad inside the second door within 30 seconds.
NOTE:
If there is an entry error during the code, re-enter the correct code and contact Corporate Security at ETN 220-5296.
- 2.
Obtain the key to the Chem Lab Credenza.
- 3.
After briefing and assignment, perform the following steps to prepare Offsite Chemistry Lab.
2a.
Located in Key Box outside receptionist's office.
3a.
Ensure compressor for gamma spectroscopy detector is on and detector is cooled to operating temperature.
3b.
Ensure current Analysis Library is available for reference.
3c.
Initiate Emergency Sample Log and Event Log.
TAB C EP-PS-1 15-C Revision 6 Page 3 of 8 SPECIFIC TASKS:
HOW:
INITIALS 3d.
Label all samples NOT assigned an in-plant sample number using the following format:
EOFYY-XXX WHERE:
YY = Last 2 digits of current year XXX = Sequential number 3e.
Connect tygon from exhaust of G.C.
to hood.
- 4.
Set up detector cave purge, if 4a.
Begin purge a minimum of 30 operable.
minutes prior to receiving samples.
4b.
Set up compressed air purge line (tygon tubing) for gamma spectroscopy detector.
4c.
Open regulator valve(s) on compressed air tank to obtain slow flow of gas.
4d.
Ensure slow flow rate is obtained by placing back of hand at end of tubing. If flow rate is too high, gas bottle will be quickly exhausted.
4e.
Place end of tubing into high purity germanium detector cave to prevent any airborne radioactivity from entering cave and raising background levels.
TAB C EP-PS-1 15-C Revision 6 Page 4 of 8 SPECIFIC TASKS:
HOW:
INITIALS
- 5.
Perform instrument checks of all 5a.
Perform instrument checks on the operable equipment and log results.
following equipment, if operable, in accordance with CH-GI-051, Instrument Checks at the Offsite Chemistry Lab.
Gamma spectroscopy system Laboratory balance Turbidimeter
-,pH meter Gas chromatograph Portable frisker_
- 6.
Obtain necessary supplies and store 6a.
Obtain the following supplies:
within access of fume hood.
pH meter and electrode Dilution vials Liquid syringe or Eppendorf pipettes, 1.0 ml, 0.1 ml Gas tight syringes Gas vials Septums Capper and decapper 0.01 N Nitric Acid (HNO3)
Labels and markers Paper towels Lab coats Carboys Tongs Plastic wrap Bags Survey Meter
__Vacuum grease Remote handling tool(s)
Cotton gloves Plastic gloves Radiation tape Yellow trash bags 2 adjustable wrenches Large screwdriver Syringes and needles for liquid transfers Bench coat
TAB C EP-PS-1 15-C Revision 6 Page 5 of 8 SPECIFIC TASKS:
HOW:
INITIALS
- 7.
If required, obtain additional supplies for contamination control.
7a.
Obtain the following supplies from the D-Con room:
______Step-off pads Herculite
___Duct tape Plastic booties
___Plastic gloves Protective Clothing Containers for used PC's
- 8.
Complete Off site Chemistry Lab preparations.
8a.
Place step-off pads as shown on Attachment A, Offsite Chemistry Lab.
8b.
Place the following at each step-off pad.
(1) Containers for used protective clothing (2)
Plastic gloves (3)
Plastic booties 8c.
Install bench coat on lab benchtops, taping edges and seams.
8d.
Install double layer of herculite in Sample Handling hood.
- 9.
Construct necessary lead brick shielding for sample storage and preparation.
9a.
Construct lead brick shield in Sample Handling hood to store samples and sample dilutions.
9b.
Construct lead brick tunnel as shown on Attachment B, Suggested Cave/Tunnel Designs, on floor or other suitable location.
TAB C EP-PS-1 15-C Revision 6 Page 6 of 8 SPECIFIC TASKS:
HOW:
INITIALS
- 10.
Ensure adequate source of flush water.
1 Oa.
Check water supply demineralizer cartridges to determine if cartridges require changeout.
1 Ob.
Confirm isolation valve under sink is open.
- 11.
Ensure fume hood exhaust is operable.
11a.
Turn fume hood exhaust on.
11 b.
Tape kimwipe strips near fume hood exhaust as visual indication hood is operating.
11 c.
Leave fume hood exhaust running to purge EOF lab of any airborne radioactivity.
- 12.
Designate sink for disposal of nonradioactive solutions only.
1 2a.
Disconnect sink drain connection between steel and PVC piping.
12b.
Place 5 gallon carboy under drain and tape connection between pipe and carboy to prevent spillage.
12c.
Replace carboy when 2/3 full.
Handle carboy with extreme care due to highly acidic nature of disposed liquid.
- 13.
Place two large beakers in fume hood for disposal of solid and liquid radioactive waste.
- 14.
Set up holding area for nonradioactive 14a.
used glassware.
Dispose of glassware used for radioactive samples as solid radioactive waste immediately after use to minimize personnel exposure.
14b.
Store glassware used for nonradioactive blanks and standards in holding area for used glassware until cleaning is available.
TAB C EP-PS-1 15-C Revision 6 Page 7 of 8 ATTACHMENT A OFFSITE CHEMISTRY LAB
TAB C EP-PS-1 15-C Revision 6 Page 8 of 8 ATTACHMENT B SUGGESTED CAVE/TUNNEL DESIGNS LEAD BRICK TUNNEL 21"r I
41"-
4-.
TOPVIEW SURVEY METER (IONIZATION CHAMBER)
END VIEW I
I.,
SIDE VIEW
TAB I EP-PS-1 15-I Revision 6 Page 1 of 6 MAJOR TASK:
Prepare and Analyze PASS Small Volume Liquid Sample(s).
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
Upon return from PASS Sample Station, place sample cask in Sample Prep Room.
- 2.
Transfer required TAB E data to Attachment A, Small Volume Liquid Analysis.
- 3.
Perform pre-analysis sample 3a.
Using remote handling device, preparation in fume hood.
remove sample vial from cask.
Place sample vial behind shielding in fume hood.
3b.
Obtain contact dose rate (closed window) on sample vial. Record sample number, dose rate, dilution performed, and dilution factor on Attachment A.
(1) If 0.1 ml sample was obtained for pH analysis, record original dilution as N/A and dilution factor of 1.
(2)
If demineralized water was added to sample at time of collection, record original dilution as 0.1:10 and dilution factor of 100.
3c.
If 0.1 ml sample was obtained for pH analysis, analyze pH using flat surface membrane pH probe in accordance with CH-CC-030, Laboratory pH Determination.
Record results on Attachment A (under analysis results).
TAB I EP-PS-1 15-I Revision 6 Page 2 of 6 SPECIFIC TASKS:
HOW:
INITIALS
- 4.
Prepare sample for isotopic analysis 4a.
If demineralized water was added to sample at time of collection, determine dilution(s) required to obtain 10ml sample at <5.OmR/hr using the table below.
Original vial Dilution Dilution Vials Contact mR/hr.
ratio Factor Required 0.0- 5.0 None 1 E2 None 5.0-50 1:10 1 E3 1
50-500 0.1:10 1 E4 1
500 - 5000 0.1:10 & 1:10 1 Es 2
4b.
For a 0.0-0.5mR/hr sample, no dilution is required. GO TO Step 4i of this tab.
4c.
If applicable, label additional vial(s),
adding consecutive letters to the original sample number.
4d.
For a 5.0-5OmR/hr sample, place 9.Oml 0.01 N HNO3 diluent into the vial, cap vial, and inject 1.0ml of original sample through septum.
4e.
For a 50-500mR/hr sample, place 9.9ml 0.01 N HNO3 diluent into the vial, cap vial, and inject 0.1ml of original sample through the septum.
4f.
For a 500-50OOmR/hr sample:
(1)
Place 9.9ml 0.1 N HNO3 diluent into one vial, and 9.Oml into the second vial: cap vials.
(2)
Inject 0.1ml of original sample into the first vial.
(3)
Gently invert vial five (5) times to mix.
TAB I EP-PS-1 15-I Revision 6 Page 3 of 6 SPECIFIC TASKS:
HOW:
INITIALS (4)
Withdraw 1.Omi from the first vial and inject into the second vial.
4g.
While directing the open end of the needle toward the back of the hood, vent vial by inserting a hypodermic needle (without syringe) through the septum into the air space above the liquid, and then removing the needle.
4h.
Gently invert final vial five (5) times to mix.
4i.
Record sample number, dilution(s) performed, and dilution factor on Attachment A for each dilution prepared.
4j.
Record contact dose rate (closed window) on Attachment A for each sample dilution.
4k.
Store original sample bottle and all dilution(s) except one to be analyzed in lead brick storage cave in fume hood of Sample Prep Room.
- 41.
When sample is < 5.0 mR/hr, wrap vial in clean plastic film and transfer to Counting Room for analysis.
TAB I EP-PS-1 15-I Revision 6 Page 4 of 6 SPECIFIC TASKS:
HOW:
INITIALS
- 5.
Perform isotopic analysis on sample
<5.0 mR/hr.
5a.
Using the table below, determine Actual Coolant Volume for isotopic analysis, based on the dilutions that were performed.
Dilutions Performed None 1:10 0.1:10 0.1:10 & 1:10 Actual Coolant Volume - ml 1 E-1 1 E -2 1 E -3 1 E-4 5b.
Decay correct sample to time of collection.
5c.
Determine DEI-131 (pCi/ml) in accordance with CH-RC-010, Iodine Counting and Data Analysis.
5d.
Record Analysis Date/Time, CTE Number, and DEI-131 on Attachment A.
5e.
Attach printout of isotopic analysis to Attachment A.
5f.
Notify Chemistry Coordinator of analysis results.
- 6.
Perform additional analyses, as requested by Chemistry Coordinator.
6a.
Perform boron analysis in accordance with CH-CC-043, Analytical Procedures for HACH or BETZ Portable Spectrophotometer Labs, if required. Record results on Attachment A.
6b.
Perform chloride analysis, in accordance with CH-CC-01 0, Chloride - Silver Nitrate Turbidimetric Method, if required.
Record results on Attachment A.
6c.
Notify Chemistry Coordinator of analysis results.
TAB I EP-PS-1 15-l Revision 6 Page 5 of 6 SPECIFIC TASKS:
HOW:
INITIALS
- 7.
At completion of analyses, place sample in lead brick storage cave in fume hood of Sample Prep Room.
TAB I EP-PS-1 15-I Revision 6 Page 6 of 6 ATTACHMENT A SMALL VOLUME LIQUID ANALYSIS I.
SMALL VOLUME LIQUID ANALYSIS Sample Source Sample Date/Time Liquid Sample Temperature TI-660 OF Vial Dose Rate mR/hr Conductivity CI-663 jmho/cm @
OF II.
SAMPLE DILUTION/RESULTS Sample Original Dilution 1 Dilution 2 Dilution 3 Sample #
Dilution Ratio Dilution Factor Dose Rate Actual Coolant Volume for Isotopic Analysis ml Analysis Date/Time CTE #
DEI-131 PCVml Additional Performed Not Analysis x
Dilution =
Sample Analyses Performed Results Factor-Conc.
Boron x
=
ppm Chloride x
=
ppm pH lPerformed By Date lReviewed By Date
TABJ EP-PS-1 15-J Revision 7 Page 1 of 7 MAJOR TASK:
Prepare and Analyze PASS Dissolved Gas Sample(s).
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
Upon return from PASS Sample Station, place gas syringe behind shielding in fume hood.
- 2.
Transfer required TAB F data to Attachment A, Dissolved Gas Analysis.
- 3.
Determine contact dose rate of gas syringe.
- 4.
Determine gas concentrations of undiluted sample by gas chromatograph, if requested by Chemistry Coordinator. Perform all sample preparations in fume hood.
3a.
Obtain contact dose rate (closed window) on gas syringe. Record on Attachment A.
4a.
Inject applicable volume of sample into gas chromatograph and analyze in accordance with CH-CC-040, Hydrogen By GC.
(1) Install clean needle on locked dissolved gas syringe, if not performed previously.
(2)
Insert needle into appropriate septum of gas chromatograph.
(3)
Push green button in to unlock syringe.
(4)
Push plunger into syringe 0.5 cc or other appropriate volume, and start analysis on gas chromatograph.
(5)
Push red button in to lock syringe and remove from gas chromatograph.
4b.
Record analysis results, analysis date and time, and CTE Number on Attachment A.
- 5.
Determine Total Dissolved Gas Concentration, Hydrogen Dissolved Gas Concentration, and Oxygen Dissolved Gas Concentration.
5a.
Perform calculations in accordance with Attachment A using Initial and Final Gas Sample Pressures from P1-662.
TAB J EP-PS-1 15-J Revision 7 Page 2 of 7 SPECIFIC TASKS:
HOW:
INITIALS 5b.
Record results on Attachment A.
- 6.
Prepare sample for isotopic analysis.
6a.
Determine dilution(s) required to obtain 14.7 cc gas vial < 5.0 mR/hr.
Perform all sample preparations in fume hood.
Syringe Dose Dilution Rate - mR/hr Dilution(s)
Factor Vial(s) 0-70 1:14.7 14.7 1
70-1000 1:14.7 & 1:15.7 231 2
1000-15000 1:14.7, 1:15.7 & 1:15.7 3623 3
6b.
Prepare and label dilution vials by adding consecutive letters to the sample number.
6c.
Using a clean gas tight syringe, remove 1 cc of air from each new gas vial.
6d.
For a 0-7OmR/hr dose rate, transfer 1 cc of dissolved gas sample into a partially evacuated gas vial as follows:
(1) Ensure red button is pushed in to lock dissolved gas syringe.
Install clean needle on locked syringe, if not installed previously.
(2)
Insert dissolved gas syringe needle into septum of partially evacuated gas vial.
(3)
Push green button in to unlock syringe.
(4) Push plunger 1.0 cc into syringe.
(5) Push red button in to lock syringe. Remove syringe from gas vial septum.
TAB J EP-PS-1 1 5-J Revision 7 Page 3 of 7 SPECIFIC TASKS:
HOW:
INITIALS 6e.
For a 70-lOOmR/hr dose rate, using a clean gas tight syringe, remove 1 cc from the first (A) dilution vial and inject into the second (B) dilution vial.
6f.
For a 1000-15000 mR/hr dose rate, using a clean gas tight syringe, remove 1 cc from second (B) dilution vial and inject it into the third (C) dilution vial.
6g.
Record sample number, dilution(s) performed, and dilution factor on Attachment A for each vial prepared.
6h.
Record contact dose rate (closed window) on Attachment A for each vial prepared.
6i.
Store original sample and all dilution(s) except one to be analyzed in lead brick storage cave in fume hood of Sample Prep Room.
6j.
Wrap final dilution in clean plastic film and transfer to Counting Room for analysis.
- 7.
Perform isotopic analysis on sample <
7a.
Determine corrected vial volume 5.0 mR/hr in accordance with (after dilution) for isotopic analysis.
CH-RC-076, Gamma Spectral Analysis Using the ND 9900.
(1) Record on Attachment A.
(2) Enter corrected vial volume as actual sample volume for gamma spectroscopy analysis.
7b.
Decay correct sample to time of collection.
7c.
Record Analysis Date/Time and CTE Number on Attachment A.
7d.
Attach printout of isotopic analysis to Attachment A.
TABJ EP-PS-1 1 5-J Revision 7 Page 4 of 7 SPECIFIC TASKS:
HOW:
INITIALS 7e.
Notify Chemistry Coordinator of analysis results.
- 8.
At completion of analysis, place sample in lead brick storage cave in fume hood of Sample Prep Room.
TAB J EP-PS-1 15-J Revision 7 Page 5 of 7 ATTACHMENT A DISSOLVED GAS SAMPLE ANALYSIS I.
DISSOLVED GAS SAMPLE ANALYSIS Sample Source Sample Date/Time Initial Sample Gas Pressure (P.) P1-662 psia Temperature TI-660 OF Final Sample Gas Pressure (Pf) PI-662 psia Contact Dose Rate mR/hr II.
GAS CHROMATOGRAPH ANALYSIS 1Analysis Date/Time CTE #
% Oxygen (Co)
% Nitrogen III.
DISSOLVED GAS CONCENTRATIONS Total Dissolved Gas Concentration:
=
MFT X [Pf - (1.05 x Po) - PV]
=
x.
- (1.05 x
) -
=
scc/kg WHERE:
=
Total Dissolved Gas Concentration (scc/kg)
MFT
=
Multiplication Factor for gas and liquid loop volumes Unit 1: 6.33 Unit 2: 8.33 Pf
=
Final Sample Gas Pressure P1-662 (psia)
PO
=
Initial Sample Gas Pressure P1-662 (psia)
P
=
Liquid vapor pressure of sample © temperature TI-660 from Attachment B Dissolved Hydrogen Concentration:
=
(MFH) x (% H) x (Pf)
=
(
)x(
)x(
(TI-660 0F + 460)
+ 460) scc/kg WHERE:
=
Dissolved Hydrogen Concentration (scc/kg)
MFH
=
Multiplication Factor Unit 1: 48.6 Unit 2: 63.31
%H2
=
Percent hydrogen from gas chromatograph analysis P.
=
Final Sample Gas Pressure Pl-662 (psia)
TI-660 =
Temperature (OF) at TI-660
TAB J EP-PS-1 15-J Revision 7 Page 6 of 7 Attachment A DISSOLVED GAS CONCENTRATIONS (continued)
Ill.
DISSOLVED GAS CONCENTRATIONS, cont.
Dissolved Oxygen Concentration:
Co (MFI) x (% O0) x (Pf)
(Tf + 460)
(
) x (
)x(
)
+ 460)
(MF2 x P0)
(_
x
)
scc/kg WHERE:
Co MFE
%°2 Pf MF2
=
Dissolved Oxygen Concentration (scc/kg)
=
Multiplication Factor Unit 1: 53.5 Unit 2: 68.21
=
Percent oxygen from gas chromatograph analysis
=
Final Sample Gas Pressure P1-662 (psia) from Tab F, step 121
=
Multiplication Factor Unit 1: 1.15 Unit 2: 1.59 Initial Sample Gas Pressure P1-662 (psia) from Tab F, step 12g P0 Tf
= Temperature ( 0F) at TI-660 from Tab F, step 121 IV.
SAMPLE DILUTION FOR ISOTOPIC ANALYSIS Sample Dilution 1 Dilution 2 Dilution 3 Sample #
Dil Factor 14.7 231 3623 Volume (cc) 1 6.37 E-2 4.06 E-3 Dose Rate Analysis Date/Time CTE #
lPerformed By lDate lReviewed By lDate
TABJ EP-PS-1 15-J Revision 7 Page 7 of 7 Attachment B WATER VAPOR PRESSURE Temperature (OF)
P, (psia)
Temperature (OF)
Pv (psia) 60 0.2561 106 1.135 62 0.2749 108 1.203 64 0.2950 110 1.275 66 0.3163 112 1.351 68 0.3389 114 1.430 70-0.3629 116 1.513 72 0.3884 118 1.601 74 0.4155 120 1.693 76 0.4442 122 1.789 78 0.4746 124 1.890 80 0.5068 126 1.996 82 0.5409 128 2.107 84 0.5770 130 2.223 86 0.6152 132 2.345 88 0.6555 134 2.472 90 0.6981 136 2.605 92 0.7431 138 2.744 94 0.7906 140 2.889 96 0.8407 142 3.041 98 0.8936 144 3.200 100 0.9492 146 3.365 102 1.008 148 3.538 104 1.070 150 3.718
TAB K EP-PS-1 15-K Revision 7 Page 1 of 5 MAJOR TASK:
Prepare and Analyze PASS 14.7 cc Gas Sample(s).
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
Upon return from PASS Sample Station, place gas sample behind shielding in fume hood.
- 2.
Transfer required TAB G data to Attachment A, 14.7 cc Gas Sample Analysis.
- 3.
Determine and record (closed window) contact dose rate of gas vial on Attachment A.
- 4.
Determine gas concentrations of undiluted sample by gas chromatograph, if requested by Chemistry Coordinator. Perform all sample preparations in fume hood.
4a.
Using gas tight syringe, inject 0.25 cc gas or other appropriate volume into gas chromatograph and analyze in accordance with CH-CC-040, Hydrogen By GC.
4b.
Record analysis results, analysis date and time, and CTE Number on Attachment A.
- 5.
Determine calculated volume of sample vial at standard temperature and pressure (STP) on Attachment A.
5a.
If gas chromatograph analysis was performed, determine calculated drywell concentrations of hydrogen, oxygen, and nitrogen on Attachment A.
5b.
Notify Chemistry Coordinator of analysis results.
- 6.
Prepare sample for isotopic analysis.
6a.
Determine dilution(s) required to obtain 14.7 cc gas vial < 5.0 mR/hr.
Perform all sample preparations in fume hood.
Vial Dose Rate - mR/hr Dilution Factor Vial(s)
Dilution(s) 0-5 5-80 80-1200 1200-1 9000 Count as is 1:15.7 1:15.7 & 1:15.7 1:15.7, 1:15.7& 1:15.7 1
15.7 246 3870 None 1
2 3
TAB K EP-PS-1 15-K Revision 7 Page 2 of 5 SPECIFIC TASKS:
HOW:
INITIALS 6b.
Prepare and label dilution vial(s),
adding consecutive letters to the sample numbers.
6c.
Using clean gas tight syringe, remove 1 cc of air from each new gas vial.
6d.
Transfer 1 cc of gas sample into partially evacuated gas vial.
6e.
Perform successive dilutions from one vial to the next until gas vial dose rate of < 5.0 mR/hr is achieved.
6f.
Record sample number, dilution(s) performed, and dilution factor on Attachment A for each vial prepared.
6g.
Record contact dose rate (closed window) on Attachment A for each vial prepared.
6h.
Store original sample and all dilution(s) except one to be analyzed in lead brick storage cave in fume hood of Sample Prep Room.
6i.
Wrap final dilution in clean plastic film and transfer to Counting Room for analysis.
- 7.
Perform isotopic analysis on sample 7a.
Determine corrected vial volume
< 5.0 mR/hr in accordance with (after dilution) for isotopic analysis CH-RC-076, Gamma Spectral using calculated sample volume at Analysis Using the ND 9900.
STP.
(1)
Record on Attachment A.
(2)
Enter corrected vial volume as actual sample volume for gamma spectroscopy analysis.
7b.
Decay correct sample to time of collection.
7c.
Record Analysis Date/Time and CTE Number on Attachment A.
TAB K EP-PS-1 15-K Revision 7 Page 3 of 5 SPECIFIC TASKS:
HOW:
INITIALS 7d.
Attach printout of isotopic analysis to Attachment A.
7e.
Notify Chemistry Coordinator of analysis results.
- 8.
At completion of analysis, place sample in lead brick storage cave in fume hood of Sample Prep Room.
TAB K EP-PS-1 15-K Revision 7 Page 4 of 5 Attachment A 14.7 cc GAS SAMPLE ANALYSIS 14.7 cc GAS SAMPLE ANALYSIS SamDle Source:
Sample Date/Time:
/
Initial Sample Gas Pressure (PO) Pl-708:
psia Temperature TI-724 (T):
0F Final Sample Gas Pressure (Pf) Pl-708:
psia GAS CHROMATOGRAPH ANALYSIS Analysis Date/Time CTE #
% Oxygen (CO)
Calculated Sample Volume @ STP:
Sample Vol @ STP
=
[(Pf - P0 ) x (14.7 cc) x (4920R)1 (T + 4600R) x (14.7 psia)
Sample Vol @ STP
=
r
) x (492)1
(+
460)
= _
cc © STP CALCULATED GAS CONCENTRATIONS (Corrected for air remaining in evacuated vial)
Calculated Drvwell Hvdrogen Concentration:
Drywell H2 Conc (%) =
CH X 14.7 cc Sample Vol @ STP Drywell H2 Conc (%) =
x 14.7 l___
_ =%
H2
TAB K EP-PS-1 15-K Revision 7 Page 5 of 5 Attachment A 14.7 CC GAS SAMPLE ANALYSIS (continued)
Calculated Oxygen Concentration:
Drywell
[C (14.7 cc - Sample Vol @ STP) x 21% 1 14.7 cc 02 Conc (%)
L 14.7cc u Sample Vol @ STP Drywell
= r (14.7 -
)x 21 1 x 14.7 02 Conc (%)
L 14.7 j
%°02 Calculated Nitrogen Concentration:
Drywell FC (14.7cc-SampleVol @ STP)x78.1% 1 14.7cc N2 Conc (%)
[
14.7 cc Sample Vol @ STP Drywell F
(14.7 -
)x 78.1 1 x 14.7 N2 Conc (%)
L 14.7 I
=
% N2 II.
SAMPLE DILUTION FOR ISOTOPIC ANALYSIS Sample Original Dilution 1 Dilution 2 Dilution 3 Sample #
Dil Factor 1
15.7 246 3870 Dose Rate Analysis Date/Time CTE #
Corrected Sample Vial Volume Following Dilution: (for isotopic analysis only)
Volume 0s0tp,c
=
Sample Vol @ STP
=
Dil Factor VolumesotOpc, =
cc Performed By Date Reviewed By Date
TAB L EP-PS-1 1 5-L Revision 4 Page 1 of 3 MAJOR TASK:
Prepare and Analyze PASS Particulate and Iodine Sample(s).
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
Upon return from PASS Sample Station, place cartridge retainer behind shielding in fume hood.
- 2.
Transfer required TAB H data to Attachment A, Particulate/Iodine Sample Analysis.
- 3.
Perform pre-analysis sample 3a.
Disassemble cartridge retainer.
preparation in fume hood.
3b.
Obtain contact dose rate (closed window) on particulate filter and iodine cartridge(s). Record sample number and dose rate of each on Attachment A.
3c.
Place particulate filter in Petri dish and wrap in clean plastic film.
3d.
Wrap cartridge(s) in clean plastic film.
3e.
Transfer samples to Counting Room for analysis.
- 4.
Perform isotopic analysis on 4a.
Determine sample volume for particulate filter and each cartridge.
isotopic analysis.
(1) Record on Attachment A.
(2) Enter sample volume for gamma spectroscopy analysis.
4b.
Analyze iodine cartridges in accordance with CH-RC-071, Radiochemical Analysis of High Activity Iodine Cartridge Samples.
4c.
Analyze particulate filter in accordance with CH-RC-01 6, Particulate Filter Analysis.
4d.
Record Analysis Date/Time and Standardization Number of each sample on Attachment A.
TAB L EP-PS-1 1 5-L Revision 4 Page 2 of 3 SPECIFIC TASKS:
HOW:
INITIALS 4e.
Record activities of iodine isotopes from gamma spectroscopy analysis of each cartridge.
4f.
Determine total activity of each iodine isotope from all cartridges and record on Attachment A.
4g.
Attach printouts of all isotopic analyses to Attachment A.
4h.
Notify Chemistry Coordinator of analysis results.
- 5.
At completion of analysis, place samples in lead brick storage cave in fume hood of Sample Prep Room.
TAB L EP-PS-1 1 5-L Revision 4 Page 3 of 3 Attachment A PARTICULATE/IODINE SAMPLE ANALYSIS 1.
PARTICULATEIIODINE SAMPLE ANALYSIS Sample Source Sample Date/Time Total Sample Time sec II.
SAMPLE DILUTIONIRESULTS Particulate/lodine Sample Volume:
Volume = (3 Umin orifice flow) x (Total Sample Time in sec) x (1000 cc/L) 60 sec/min
= (50 cc/sec) x sec
=
cc Sample Particulate Cartridge #1 Cartridge #2 Cartridge #3 Sample #
Analysis Date/Time Dose Rate (mR/hr)
CTE#
Tech Cartridge 1-131 1-132 1-133 1-134 1-135
- 1
- 2
- 3 Total p Ci/cc E
Performed By Date Reviewed By Date
TAB N EP-PS-1 15-N Revision 9 Page 1 of 28 MAJOR TASK:
Collect Samples(s) from Post-Accident Vent Sampling System (PAVSS) on Turbine 729' El.
SPECIFIC TASKS:
HOW:
INITIALS NOTE:
If at any time while monitoring dose rates especially when opening sample inlet, dose rates exceed 1000 mR/hr general area GO TO step 15a in order to secure sample flow.
- 1.
Ensure flow totalizers on appropriate PAVSS have been reset prior to sampling.
- 2.
After briefing and assignment, obtain necessary equipment.
- 3.
Perform instrument checks on survey meter.
1 a.
Contact l&C to reset the totalizer(s) by pulling and reinstalling the fuse(s).
2a.
Obtain the following supplies:
Respiratory protection devices Hi-range and extremity dosimetry Survey meter Gas sample container (Nominal 75 cc)
Particulate filters Silver zeolite cartridges
__Plastic bags Tygon tubing as necessary for proper connections
.Remote handling tongs Large blade screwdriver with long handle Adjustable wrench 2 pairs of 16-inch channel locks 11/16" deep socket Rachet wrench Noble gas quick disconnects Stopwatch Calculator 5' x 5' plastic sheet Sample cask for gas container Tweezers 3a.
Check the following on survey meter:
_ Calibration has not expired.
Battery indication is good.
__Source check is satisfactory.
TAB N EP-PS-1 15-N Revision 9 Page 2 of 28 SPECIFIC TASKS:
HOW:
INITIALS
- 4.
Don protective clothing and respiratory protection as directed by Radiation Protection Coordinator.
- 5.
Ensure each team member present has required dosimetry.
- 6.
Ensure survey meter is on highest range.
- 7.
Notify Chemistry Coordinator before leaving Chemistry Lab.
7a.
Ensure appropriate PAVSS has been initialized.
7b.
Ensure corresponding SPING has been placed in STANDBY.
- 8.
Proceed to PAVSS on Turbine Building 729' Elevation via best route while continuously monitoring radiation levels and status of CAMs and ARMs.
NOTE:
Attachment A may be reviewed for location and configuration of PAVSS.
8a.
Retreat to low background area and notify Chemistry Coordinator if any of the following conditions are encountered:
(1) General area radiation levels exceed 1,000-mrem/hr at any time.
(2) Total annual whole body (TEDE) exposure approaches 2000 mrem.
- 9.
At PAVSS, check area radiation levels 9a.
and notify Chemistry Coordinator.
PAVSS general area radiation level:
mR/hr NOTE:
X in panel and switch designations denotes specific PAVSS system. X = 0 for Standby Gas Treatment System (SGTS), 1 for Unit 1 Turbine Building (TB1), and 2 for Unit 2 Turbine Building (TB2).
Attachments B and C may be reviewed for illustrations of PAVSS panels, as required.
TAB N EP-PS-1 15-N Revision 9 Page 3 of 28 SPECIFIC TASKS:
HOW:
INITIALS 9b.
Survey front of PAVSS control panels, noble gas monitors, and shielded sample carts.
Panel OC259 - Standby Gas Treatment Panel 1C259 - Unit 1 Turbine Building Vent Panel 2C259 - Unit 2 Turbine Building Vent 9c.
Ensure the following supplies are at PAVSS location:
__1 pair of 3' long steel lifting bars 2 pairs of S-hooks 9d.
Notify Chemistry Coordinator of radiation levels.
- 10.
Perform valve lineups to establish NOTE:
isokinetic flow through PAVSS.
Attachment D may be reviewed for diagrams of particulate/iodine filter assembly and sample cart, as required.
1 Oa.
Remove installed sample cart, if necessary, by disconnecting inlet and outlet disconnects between sample cart and control panel.
1 Ob.
Ensure particulate filter and silver zeolite cartridge are installed in sample cart to be used.
1 Oc.
Position sample cart under appropriate PAVSS control panel.
NOTE:
Sample lines will be crossed in front of cart after completing next two steps.
(1) Connect inlet sample line on left side of skid to inlet connection on right side of sample cart.
TAB N EP-PS-1 15-N Revision 9 Page 4 of 28 SPECIFIC TASKS:
HOW:
INITIALS (2)
Connect outlet sample line on right side of skid to outlet connection on left side of sample cart.
(3)
Lightly pull disconnects to ensure fittings are properly mated.
1 Od.
Ensure Sample System Power Switch HS-X6560 on appropriate PAVSS control panel is ON. White light should illuminate.
1 Oe.
Secure sample cart and confirm the following valve positions for the appropriate PAVSS sampling station:
(1) Sample Cart Isolation Valves are OPEN (parallel to tubing):
SGTS:
0-65-032 OPEN 0-65-033 OPEN TB1:
1-65-038 OPEN 1-65-039 OPEN TB2:
2-65-004 OPEN 2-65-005 OPEN (2) Valves between control panel and sample cart are OPEN:
SGTS:
0-65-022 OPEN 0-65-029 OPEN 0-65-031 OPEN TB1:
1-65-029 OPEN 1-65-035 OPEN 1-65-037 OPEN TB2:
2-65-010 OPEN 2-65-022 OPEN 2-65-024 OPEN
TAB N EP-PS-1 15-N Revision 9 Page 5 of 28 SPECIFIC TASKS:
HOW:
INITIALS (3)
Sample Cart Bypass Valve is CLOSED:
SGTS:
0-65-030 CLOSED TB1:
1-65-036 CLOSED TB2:
2-65-023 CLOSED (4)
Sample Inlet Valve is OPEN:
SGTS:
0-65-021 OPEN TB1:
1-65-027 OPEN TB2:
2-65-009 OPEN (5)
Atmospheric Test Valve is CLOSED:
SGTS: 0-65-017 CLOSED TB1:
1-65-019 CLOSED TB2:
2-65-016 CLOSED (6)
Sample Return Valve is OPEN:
SGTS:
0-65-018 OPEN TB1:
1-65-022 OPEN TB2:
2-65-008 OPEN (7)
Noble Gas Mon Out Valve between grab sample ports on noble gas monitor skid is OPEN:
SGTS:
0-65-026 OPEN TB1:
1-65-032 OPEN TB2:
2-65-017 OPEN
TAB N EP-PS-1 15-N Revision 9 Page 6 of 28 SPECIFIC TASKS:
HOW:
INITIALS (8)
Noble Gas Grab Sample Inlet and Outlet Valves are CLOSED:
SGTS:
0-65-027 0-65-028 CLOSED CLOSED TB1:
1-65-033 CLOSED 1-65-034 CLOSED TB2:
2-65-018 CLOSED 2-65-019 CLOSED 1 Of.
Ensure filter monitor plugs are in place on sample cart.
- 11.
Isolate sample flow to affected SPI NG 11 a.
by shutting off sample pump on Reactor Building 818' El. and closing sample line. Start sample flow to appropriate PAVSS panel.
Turn Man. Isolation Switch HS-X6562 on appropriate PAVSS control panel to CLOSE. Red light above hand switch should go OFF and amber light should illuminate.
l1 b. Turn Man. System [nit. HS-X6561 on appropriate PAVSS control panel to RUN to open sample line to PAVSS and start PAVSS pump.
(1) Sample Pump Iso Vlv SV-X6561 amber light should go OFF and red light should illuminate.
(2) Sample Pump XP261 (TB1/2) or Sample Pump OP561 (SGTS) amber light should go OFF and red light should illuminate.
TAB N EP-PS-1 15-N Revision 9 Page 7 of 28 SPECIFIC TASKS:
HOW:
INITIALS
- 12.
Flush sample lines for a minimum of three sample line volumes.
NOTE:
Sample cart must be in place during all valve adjustments and sample line flushes. At completion of valve adjustments and sample line flushes, sample cart will be removed and particulate/iodine filter assembly replaced or new sample cart installed before collecting grab sample.
12a.
If taking an SGTS vent sample, perform the following:
(1) Adjust Rad Smpl Control Valve 0-65-023 until Radiation Sample Velocity FI-06560A is within + 20% of Stack Velocity Fl-06562A.
(2)
Observe Radiation Sample Flow (CFM) FI-06560B to estimate average flow.
(3)
Record start date and time of sample flush. -
SGTS Flush Start Date/Time:
/
(4)
Flush system for approximately 5 minutes at 1 cfm or equivalent volume.
TAB N EP-PS-1 15-N Revision 9 Page 8 of 28 SPECIFIC TASKS:
HOW:
INITIALS (5)
GO TO appropriate step.
Sample to be Taken Action Collect Particulate/Iodine GO TO Step 13. Step 13 may Sample and Noble Gas be performed during sample line Sample.
flush.
Collect Noble Gas Sample GO TO Step 14.
only.
Place PAVSS on line. No Return to In-plant Chemistry Lab.
Sample Collection.
12b.
If taking TB1 or TB2 vent sample, perform the following:
(1) Adjust Total Smpl Control Valve for the appropriate sampling station until Total Sample Velocity Fl-X6561A is within + 20% of Stack Velocity FI-X6562A.
Total Smpl Vent Control Valve TB1 1-65-030 TB2 2-65-011 (2)
Observe Total Sample Flow (CFM) FI-X6561 B to estimate average flow.
(3)
Adjust Radiation Smpl Control Valve for the appropriate sampling station until Radiation Sample Velocity Fl-X6560A is within +/- 20% of Total Sample Velocity FI-X6561 A.
Radiation Smpl Vent Control Valve TB1 1-65-031 TB2 2-65-012
TAB N EP-PS-1 15-N Revision 9 Page 9 of 28 SPECIFIC TASKS:
HOW:
INITIALS (4)
Record start date and time of sample flush.
TB1/2 Flush Start Date/Time:
l (5)
Flush system for approximately 5 minutes at 1 cfm or equivalent volume.
(6) GO TO appropriate step.
Iample to be Taken Action i
Collect Particulate/Iodine GO TO Step 13. Step 13 may be Sample and Noble Gas performed during sample line flush.
Sample.
Collect Noble Gas Sample GO TO Step 14.
only.
Place PAVSS on line. No Return to In-plant Chemistry Lab.
Sample Collection.
- 13.
Determine optimum sample time for particulate/iodine grab sample.
13a.
Determine time, in hours, since reactor shutdown.
Time since shutdown:
hours 13b.
Refer to Attachment E to estimate noble gas to iodine ratio for specified time since shutdown.
NG/I Ratio:
1 3c.
Turn Channel Selector thumbwheel on appropriate Eberline Display Panel across from noble gas monitor skid to 01 to obtain current Mid-Range noble gas concentration.
Mid-Range (01):
I PCicc
TAB N EP-PS-1 15-N Revision 9 Page 10 of 28 SPECIFIC TASKS:
HOW:
INITIALS 13d.
If current Mid-Range noble gas concentration is > 7.80 E +01 pCicc, turn Channel Selector thumbwheel to 02 to obtain current High-Range noble gas concentration.
High-Range (02):
pCi/cc 13e.
Obtain the following readings from appropriate PAVSS control panel and record.
(1) Radiation Sample Flow FI-X6560B (CFM):
cfm (2)
SGTS Stack Flow FI-X06562B (CFM):
x10=
cfm (3)
TB1 or TB2 Stack Flow FI-X6562B (CFM):
x 100x =
cfm 13f.
Determine minimum sample time (minutes) of particulate/iodine grab sample by:
ST = (2.45 E -2) x (NG:l Ratio)
(NG Conc) x (Sample Flow)
=(2.45 E-2) x (
(
,PCi/cc) x(
cfm)
= _
minutes
TAB N EP-PS-1 15-N Revision 9 Page 11 of 28 SPECIFIC TASKS:
HOW:
INITIALS WHERE:
=
Sample time in seconds NG:I Ratio
=
Noble gas to iodine ratio from Attachment E based on specified time since shutdown NG Conc
=
Noble gas concentration (pCVcc) from Step 13c or 13d Sample Flow
=
Radiation Sample Flow FI-X6560B (CFM) from Step 13e.(1).
In Step 15e(4), record the Sample Length to be used as the greater of the time calculated above or 2 minutes.
- 14.
Obtain noble gas grab sample from vent. If NOT obtaining noble gas grab sample from vent, GO TO Step 15.
14a.
Attach gas sample container to local connections for appropriate system on noble gas monitor skid. Ensure stopcocks on gas container are OPEN.
14b.
Position the following valves for the appropriate system in the order shown to collect noble gas grab sample:
SGTS V-2 (0-65-027)
V-3 (0-65-028)
V-1 (0-65-026)
TB1 V-2 (1-65-033)
V-3 (1-65-034)
V-1 (1-65-032)
TB2 V-2 (2-65-018)
V-3 (2-65-019)
V-1 (2-65-017)
OPEN OPEN CLOSED OPEN OPEN CLOSED OPEN OPEN CLOSED
TAB N EP-PS-1 15-N Revision 9 Page 12 of 28 SPECIFIC TASKS:
HOW:
INITIALS 14c.
Allow sample to flow through gas sample container for 2 minutes to ensure representative sample.
14d.
Position the following valves for the appropriate system in the order shown to secure noble gas grab sample:
SGTS V-1 (0-65-026)
OPEN V-2 (0-65-027)
CLOSED V-3 (0-65-028)
CLOSED TB1 V-1 (1-65-032)
OPEN V-2 (1-65-033)
CLOSED V-3 (1-65-034)
CLOSED TB2 V-1 (2-65-017)
OPEN V-2 (2-65-018)
CLOSED V-3 (2-65-019)
CLOSED 14e.
Close gas outlet stopcock connected to V-2 followed by gas inlet stopcock connected to V-3 to secure sample.
14f.
Record noble gas grab sample date and time.
Noble Gas Sample Date/Time:
14g.
Obtain contact dose rate (closed window) on noble gas grab sample.
Noble Gas Grab Sample Dose Rate:
mR/hr 14h.
Place noble gas grab sample in plastic bag and seal.
14i.
Transfer to sample cask for transport to In-Plant Chemistry Lab.
TAB N EP-PS-1 15-N Revision 9 Page 13 of 28 SPECIFIC TASKS:
HOW:
INITIALS
- 15.
Obtain particulate/iodine grab sample from vent. If NOT obtaining particulateliodine grab sample from vent, GO TO Step 17.
15a.
Perform the following valve lineups on appropriate sampling station to secure sample cart used during flush of particulate/iodine sample lines:
(1) Open Atmospheric Test Valve:
SGTS:
0-65-017 OPEN TB1:
1-65-019 OPEN TB2:
2-65-016 OPEN (2) Close Sample Inlet Valve:
SGTS:
0-65-021 CLOSED TB1:
1-65-027 CLOSED TB2:
2-65-009 CLOSED (3)
Open Sample Cart Bypass Valve:
SGTS:
0-65-030 OPEN TB1:
1-65:036 OPEN TB2:
2-65-023 OPEN (4)
Close valves between control panel and sample cart:
SGTS:
0-65-032 CLOSED 0-65-031 CLOSED TB1:
1-65-035 CLOSED 1-65-037 CLOSED TB2:
2-65-022 CLOSED 2-65-024 CLOSED (5)
Close Sample Cart Isolation Valves (perpendicular to tubing):
SGTS:
0-65-032 CLOSED 0-65-033 CLOSED
TAB N EP-PS-1 15-N Revision 9 Page 14 of 28 SPECIFIC TASKS:
HOW:
INITIALS TB1:
1-65-038 CLOSED 1-65-039 CLOSED TB2:
2-65-004 CLOSED 2-65-005 CLOSED 15b.
Disconnect inlet and outlet disconnects between control panel and sample cart. Remove sample cart from PAVSS control panel and mark with tape to indicate cart has been used for sample flush.
15c.
Install new sample cart by performing the following:
(1)
Ensure particulate filter and silver zeolite cartridge are installed in new sample cart to be used.
(2) Position new sample cart under appropriate PAVSS control panel.
NOTE:
Sample lines will be crossed in front of cart after completing next two steps.
(3)
Connect inlet sample line on left side of skid to inlet connection on right side of sample cart.
(4)
Connect outlet sample line on right side of skid to outlet connection on left side of sample cart.
(5) Lightly pull disconnects to ensure fittings are properly mated.
TAB N EP-PS-1 15-N Revision 9 Page 15 of 28 SPECIFIC TASKS:
HOW:
INITIALS 15d.
Secure sample cart and perform the following valve lineups for the appropriate PAVSS sampling station to establish sample flow:
(1) Open Sample Cart Isolation Valves (parallel to tubing):
SGTS:
0-65-032 OPEN 0-65-033 OPEN TB1:
1-65-038 OPEN 1-65-039 OPEN TB2:
2-65-004 OPEN 2-65-005 OPEN (2) Open valves between control panel and sample cart:
SGTS:
0-65-029 OPEN 0-65-031 OPEN TB1:
1-65-035 OPEN 1-65-037 OPEN TB2:
2-65-022 OPEN 2-65-024 OPEN (3)
Close Sample Cart Bypass Valve:
SGTS:
0-65-030 CLOSED TB1:
1-65-036 CLOSED TB2:
2-65-023 CLOSED 15e.
The following steps require timing.
Read and understand steps 15e through 15h before proceeding.
Steps 15e(1) through 15e(4) need to be performed simultaneously.
(1) Open Sample Inlet Valve for appropriate sampling station:
SGTS:
0-65-021 OPEN
TAB N EP-PS-1 15-N Revision 9 Page 16 of 28 SPECIFIC TASKS:
HOW:
INITIALS TB1:
1-65-027 OPEN TB2:
2-65-009 OPEN (2)
Close Atmospheric Test Valve for appropriate sampling station:
SGTS:
0-65-017 CLOSED TB1:
1-65-019 CLOSED TB2:
2-65-016 CLOSED (3)
Press Radiation Sample Flow printer switch HS-X6560-1 on appropriate PAVSS control panel.
(4)
Using stopwatch, begin timing sequence. Collect sample for length of time as determined in Step 13f.
Sample Length __
minutes (5)
Confirm sample flow is approximatelv.20% of Stack Flow to maintain isokinetic flow. Adjust sample valve for appropriate sampling station, as required.
Radiation Smpl Vent Control Valve SGTS 0-65-023 TB1 1-65-031 TB2 2-65-012 15f.
Record particulate/iodine grab sample start date and time.
Particulate/lodine Sample Start Date/Time:
/
TAB N EP-PS-1 15-N Revision 9 Page 17 of 28 SPECIFIC TASKS:
HOW:
INITIALS 15g.
The following 3 steps should be performed simultaneously to secure particulate/iodine grab sample.
Read and understand before proceeding:
(1) Open Atmospheric Test Valve for appropriate sampling station:
SGTS:
0-65-017 OPEN TB1:
1-65-019 OPEN TB2:
2-65-016 OPEN (2)
Close Sample Inlet Valve for appropriate sampling station:
SGTS:
0-65-021 CLOSED TB1:
1-65-027 CLOSED TB2:
2-65-009 CLOSED (3)
Press Radiation Sample Flow printer switch HS-X6560-1 on appropriate PAVSS control panel.
15h.
Record particulate/iodine grab sample stop date and time.
Particulate/Iodine Sample Stop Date/Time:
I 15i.
Remove printer tape from Radiation Sample Totalized Flow FR-X6560 and record the following:
Final Totalized Sample Flow:
ft3 Initial Totalized Sample Flow:
ft3
TAB N EP-PS-1 15-N Revision 9 Page 18 of 28 SPECIFIC TASKS:
HOW:
INITIALS 15j.
Secure sample cart with particulate/iodine grab sample by performing the following valve lineups for the appropriate PAVSS sampling station:
(1) Open Sample Cart Bypass Valve:
SGTS:
0-65-030 OPEN TB1:
1-65-036 OPEN TB2:
2-65-023 OPEN (2)
Close valves between control panel and sample cart:
SGTS:
0-65-029 CLOSED 0-65-031 CLOSED TB1:
1-65-035 CLOSED 1-65-037 CLOSED TB2:
2-65-022 CLOSED 2-65-024 CLOSED (3)
Close Sample. Cart Isolation Valves (perpendicular to tubing) to isolate filter assembly during transport:
SGTS:
0-65-032 CLOSED 0-65-033 CLOSED TB1:
1-65-038 CLOSED 1-65-039 CLOSED TB2:
2-65-004 CLOSED 2-65-005 CLOSED (4)
Disconnect inlet and outlet disconnects between control panel and sample cart.
Remove cart from PAVSS control panel.
TABN EP-PS-1 15-N Revision 9 Page 19 of 28 SPECIFIC TASKS:
HOW:
INITIALS
- 16.
Install original sample cart under 16a.
Position original sample cart under appropriate PAVSS control panel.
appropriate PAVSS control panel unless dose rates on sample cart are excessive.
NOTE:
Sample lines will be crossed in front of cart after completing next two steps.
(1) Connect inlet sample line on left side of skid to inlet connection on right side of sample cart.
(2)
Connect outlet sample line on right side of skid to outlet connection on left side of sample cart.
(3) Lightly pull disconnects to ensure fittings are properly mated.
16b.
Secure sample cart and perform the following valve lineups for the appropriate PAVSS sampling station:
(1) Open Sample Cart Isolation Valves (parallel to tubing):
SGTS:
0-65-032 OPEN 0-65-033 OPEN TB1:
1-65-038 OPEN 1-65-039 OPEN TB2:
2-65-004 OPEN 2-65-005 OPEN (2)
Open valves between control panel and sample cart:
SGTS:
0-65-029 OPEN 0-65-031 OPEN TB1:
1-65-035 OPEN 1-65-037 OPEN
TABN EP-PS-1 15-N Revision 9 Page 20 of 28 SPECIFIC TASKS:
HOW:
INITIALS TB2:
2-65-022 OPEN 2-65-024 OPEN (3) Close sample cart bypass valve:
SGTS:
0-65-030 CLOSED TB1:
1-65-036 CLOSED TB2:
2-65-023 CLOSED (4) Open Sample Inlet Valve for appropriate sampling station:
SGTS:
0-65-021 OPEN TB1:
1-65-027 OPEN TB2:
2-65-009 OPEN (5) Close Atmospheric Test Valve for appropriate sampling station:
SGTS:
0-65-017 CLOSED TB1:
1-65:019 CLOSED TB2:
2-65-016 CLOSED 17a.
Obtain contact dose rate on each sample cask.
(1) If contact dose rate exceeds 2.5 R/hr above background, exit area immediately.
(2) Record contact dose rate of each sample cask.
Noble Gas Sample Cask:_ mR/hr Particulate/Iodine Cask:_
mR/hr 17b.
Remove sample cart to low traffic, low dose area.
- 17.
Obtain contact dose rate on sample casks.
TAB N EP-PS-1 15-N Revision 9 Page 21 of 28
-SPECIFIC TASKS:
HOW:
INITIALS
- 18.
Remove particulate/ iodine grab 18a.
Lay sheet of approximately 5' x 5' sample from -sample cart, if applicable.
plastic on floor near where sample cart lid will be disassembled.
18b.
Place cart lid stand on plastic sheet.
NOTE:
The following step requires two or more individuals to perform.
CAUTION IF CONTACT DOSE RATE EXCEEDS 2.5 R/hr ABOVE BACKGROUND, EXIT AREA IMMEDIATELY.
1 8c.
Remove nuts in sample cart lid.
Using lift bars and S-hook lid attachments, carefully raise lid off sample cart. Maximize distance from filter assembly to reduce personnel exposure.
18d.
Place cart lid on lid stand.
NOTE:
Attachment D may be reviewed for diagram of sample cart interior and quick release assembly.
18e.
Obtain contact dose rate (closed window) on filter assembly.
(1) Record contact dose rate on filter assembly.
Filter Assembly: __
mR/hr 18f.
Release quick disconnect with large blade screwdriver and grab filter assembly with tongs to remove assembly from sample cart.
TAB N EP-PS-1 15-N Revision 9 Page 22 of 28 SPECIFIC TASKS:
HOW:
INITIALS 18g.
Using two pairs of 12 inch channel locks, separate filter assembly into halves. Remove iodine cartridge with tongs.
(1) Place iodine cartridge in plastic bag and seal.
(2)
Obtain contact dose rate (closed window) on iodine cartridge and record.
Iodine Cartridge: __
mR/hr (3)
Transfer cartridge to sample cask for transport to In-Plant Chemistry Lab.
(4)
Obtain contact dose rate on iodine sample cask and record.
Iodine Cask:
mR/hr 18h.
Remove particulate filter from separated filter assembly with tongs.
(1) Place filter in plastic bag and seal.
(2) Obtain contact dose rate (closed window) on particulate filter and record.
Particulate Filter:
mR/hr (3) Transfer filter to sample cask for transport to Chemistry Lab.
(4)
Obtain contact dose rate on particulate filter sample cask and record.
Filter Cask:
mR/hr
- 19.
Notify Chemistry Coordinator of sample and cask dose rates.
TAB N EP-PS-1 15-N Revision 9 Page 23 of 28 SPECIFIC TASKS:
HOW:
INITIALS
- 20.
If obtaining additional vent samples, 20a.
GO TO applicable TAB.
perform the following:
HELP SPING Sample(s)
See TAB M HELP PAVSS Sample(s)
See TAB N 20b.
Notify Chemistry Coordinator to arrange transport of vent samples to lab by additional technician, if available.
- 21.
If all vent sampling is complete, GO TO TAB P.
TAB N EP-PS-1 1 5-N Revision 9 Page 24 of 28 Attachment A LOCATION OF PAVSS CONTROL PANELS AND NOBLE GAS MONITORS
- 1. Tie-in with existing Turbine Bu.Diag 1 & 2 and Standby Gas Treatment System Vent Monitor sample lines in dead space between Control Strucue and Reactor Building.
- 2. Sample lines wre routed across roof of Control structure, down west side of Control suure through roof of Turbine Build-ing.
- 3.
Down to Turbine Deck. 72W laevaBorL where samplig and monitoring equipment is loaed as shown below.
REACTOR BLDG.
CONTROL [
BLDG.
-- Jr TURBINE BL1DG If' 4
-9,-
TURBINE
-1 DECK 1
729' EL.
gM *-
hooks and lifting bars Unit 2 Turbine-Generator I-729 EL Unit 1 Turbine-Generator i
- 5.
Eberline Display Panels relay noble gas data-to SPhIG Terminals in Control Room and TSC.
- 6.
Noble Gas Monitor with mid and high range detectors for each of three vents.
OPEN HATCH D =
T 0 0 0
- 1 1 :
- 4. Air monitoring and control panels above shielded particulate/iodine sample cars.
CONTROL ROOM
TAB N EP-PS-1 15-N Revision 9 Page 25 of 28 Attachment B POST ACCIDENT VENT SAMPLING SYSTEM TURBnO BUILDING UN=
3.
STANDBY GAS TREATH=N TURB3Ef BUILDING UNIT 2 I
(three monitors or one skid)
.PQST ACCIDENT PAR.ICM=E mm IODINE SAMPLING CARTS
(
(
TAB N EP-PS-1 15-N Revision 8 Page 26 of 28 Attachment C Pnnol OC250 - Slandby OnIn Troolment Sysitm Panol I1 260 - Unil I Tiimiino Building Panol 2C269 - Unit 2 Turbino Guliding
=r::
S 1.
Slack Flow - Velocity - FPM FI1XGS6AZ
- 2.
Stack Flow-CFM Fi-*XGSG2I.TOM 2(CFl x 100)
Fl-056628 -SGTS (CFMx I0)
- 3.
Stack Flow - Totalized Flow fR-XS 562*
- 4. Slack Flow - Pointsr Switch HS-X6562-1
- 5. Total Sample Flow-Tempernture - F TIXG6SS1 S. Total Srmpte Plow-Vooctty-FPM fiX656 1A
- 7. Total Sample Flow-CF1A Fl-X6SGi3
- 0. Total Sample Flow-Totolkled Flow iRXS561;
- 9. Total Samplo Flow - PtInler Switcht HS-XC5C tl-to. Samplet System Power HwS-X6560' I t.
Sample Pump lso Vlv*.
SV-X6Ui 1
- 12. Somplo Pump *XP2'6 (Wl/2)
Samplo Pump OP561 (SCTS)
- 13. PoetAccidentVSSS Man, Syste tuWit.
HS-Xi 561.'
IrPOxTACCtDEtF VIMN Ii ISAMPLINO SYSTEM!
tOTA.
nAOIATtON SAM4PLE SAMrLE FLOW FLOW FLOW r=
14 mm m 6~
C=3
=3
=3 C==2
-4 o
0 Ml' 14, floillaton Sample Flow - Low Flow AJar
- 16. Radiation Sample Flow - Volocity - FPM F1'Xt6OA
- 16. Radlatlan Sample Flow - CFM Fl'X66606
- 17. RadiatIon Samplo Flow-Tolniltod Flow
- 18. rkadtnllon Samplo Flow-Pilnmor Swltch HS-XtCfO-l
- 1s.
Sampl-Pump Igo VIv
- 20. Ralual Floor (TS or SGTS) Mnn. lIolnlti HS-X6562 It I
i:
TAB N EP-PS-1 15-N Revision 8 Page 27 of 28 Attachment D PAVSS PARTICULATEIIODINE FILTER ASSEMBLY AND SAMPLE CART Qukkcii=
Va1vc forc moazcxng 1sr1t:lc~
r
~m d pxdcui=
fil=
rimiedor plczn cbe C= 'for
=plccdoe
(
TAB N EP-PS-1 15-N Revision 8 Page 28 of 28 Attachment E NOBLE GAS/IODINE RATIO VS. TIME POST ACCIDENT (HOURS) 120 110 100 90 NGII.
FA=0.
s0 70 so 30 40 30 10 0
=,
-'L
'n
~~~--
+..-
___~
7
~ __
__I j..
-- 1.
_~~
77 I
}.
r a
o 20 40 60 o
100 120 140 i60 IS8O 200 7ThYI POST ACCIDUTL (O0URS)
TAB O EP-PS-1 15-0 Revision 7 Page 1 of 18 MAJOR TASK:
Prepare and Analyze Vent Monitor Sample(s).
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
Place vent sample casks and/or noble gas grab sample from SPINGs or PAVSS behind shielding in fume hood.
- 2.
If noble gas grab sample was NOT taken, GO TO Step 7.
- 3.
Determine contact dose rate of noble 3a.
Transfer TAB M noble gas data from gas grab sample.
SPINGS or TAB N noble gas data from PAVSS to Attachment A, Vent Noble Gas Analysis.
3b.
Obtain contact dose rate (closed window) on noble gas grab sample.
Record sample number and dose rate of original sample on Attachment A.
3c.
If contact dose rate on noble gas grab sample is < 0.5 mR/hr, GO TO Step 5. If contact dose rate on noble gas grab sample is Ž 0.5 mR/hr, perform the following:
(1) Prepare new labeled gas vial for dilution. Add consecutive letters to sample number to distinguish dilution from original sample.
(2) Using clean gas tight syringe, remove 1 cc of air from new gas vial.
(3)
Transfer 1 cc of gas sample into partially evacuated gas vial.
(4)
Obtain contact dose rate (closed window) of sample vial. Record sample number and dose rate on Attachment A.
TAB O EP-PS-1 15-0 Revision 7 Page 2 of 18 SPECIFIC TASKS:
HOW:
INITIALS
- 4.
Determine dilution(s) needed to obtain 14.7 cc gas vial < 5 mR/hr.
Vial Dose Rate - mR/hr Dilution Dilution Factor 0-5 5-80 80-1200 1200-19000 1:14.7 1:14.7 & 1:15.7 1:14.7, 1:15.7 & 1:15.7 1:14.7,1:15.7,1:15.7, & 1:15.7 14.7 231 3623 5.69 E4 4a.
Prepare new labeled gas vials for required number of dilution(s). Add consecutive letters to sample number to distinguish dilutions from original vial.
4b.
Using clean gas tight syringe, remove 1 cc of air from each new gas vial.
4c.
Transfer 1 cc of gas sample into partially evacuated gas vial.
4d.
Perform successive dilutions, as required, until final gas vial < 5 mR/hr.
4e.
Record sample number and contact dose rate (closed window) on Attachment A for each dilution prepared.
4f.
Store original sample and all dilution(s) except one to be analyzed in lead brick storage cave in fume hood of Sample Prep Room.
4g.
Wrap final dilution in clean plastic film and transfer to Counting Room for analysis.
- 5.
Perform isotopic analysis on sample in accordance with CH-RC-076, Gamma Spectral Analysis Using the ND 9900.
5a.
If original sample was NOT diluted, record original sample volume and N/A Corrected Sample Volume Section of Attachment A.
5b.
If original sample required dilution, determine corrected vial volume (after dilution) for isotopic analysis.
(1) Record on Attachment A.
TAB O EP-PS-1 15-0 Revision 7 Page 3 of 18 INITIALS SPECIFIC TASKS:
HOW:
(2)
Enter corrected vial volume as actual sample volume for gamma spectroscopy analysis.
5c.
Decay correct sample to time of CTE collection.
5d.
Record Analysis Date/Time and CTE Standardization Number on Attachment A.
5e.
Record the concentration of each detected noble gas from gamma spectroscopy analysis on Attachment A.
5f.
Multiply each detected concentration by Stack Flow to determine release rate. Record on Attachment A.
5g.
Add release rates of all noble gases to determine Total Noble Gas Vent Release Rate. Record on Attachment A.
5h.
Attach printout of isotopic analysis to Attachment A.
5i.
Notify Chemistry Coordinator of analysis results.
- 6.
At completion of analysis, place sample in lead brick storage cave in fume hood of Sample Prep Room.
- 7.
Perform pre-analysis sample preparation of particulate/iodine grab sample in fume hood. If particulate/iodine grab sample was not taken, GO TO Step 10.
7a.
Transfer TAB M particulate/iodine data from SPINGS or TAB N particulate/iodine data from PAVSS to Attachment B, Vent Particulate/Iodine Analysis.
TAB O EP-PS-1 15-0 Revision 7 Page 4 of 18 SPECIFIC TASKS:
HOW:
INITIALS 7b.
Disassemble iodine cartridge holder, if appropriate.
(1) Transfer iodine cartridge to clam shell holder and blow instrument air through cartridge in same direction of flow as sample flow for a minimum of 1 minute, as required.
(2)
Wrap iodine cartridge in clean plastic film.
(3)
Obtain contact dose rate (closed window) on cartridge.
Record sample number and dose rate on Attachment B.
7c.
Disassemble particulate filter holder, if appropriate.
(1) Place particulate filter in clean Petri dish and wrap in clean plastic film.
(2)
Obtain contact dose rate (closed window) on Petri dish.
Record sample number and dose rate on Attachment B.
7d.
Transfer samples to Counting Room for analysis.
- 8.
Perform isotopic analysis on 8a.
Determine sample volume for particulate filter and iodine cartridge.
isotopic analysis.
(1) Record on Attachment B.
(2)
Enter sample volume for gamma spectroscopy analysis.
TAB O EP-PS-1 15-0 Revision 7 Page5 of 18 K-SPECIFIC TASKS:
HOW:
INITIALS 8b.
Analyze iodine cartridge in accordance with CH-RC-071, Radiochemical Analysis of High Activity Iodine Cartridge Samples.
(1) Record the concentration of each detected iodine from gamma spectroscopy analysis on Attachment B.
(2)
Add concentrations of all iodines to determine Total Iodine Concentration. Record on Attachment B.
(3)
Using the formula on Attachment B, multiply Total Iodine Concentration by a correction factor (for line loss and collection efficiency) and by Stack Flow in order to determine Total Iodine Vent Release Rate.
8c.
Analyze particulate filter in accordance with CH-RC-076, Gamma Spectral Analysis Using the ND9900.
(1) Record the concentration of each detected particulate from gamma spectroscopy analysis on Attachment B.
(2)
Add concentrations of all particulates to determine Total Particulate Concentration.
Record on Attachment B.
(3)
Using the formula on Attachment B, multiply Total Particulate Concentration by a correction factor for line loss and by Stack Flow in order to determine Total Particulate Vent Release Rate.
TAB O EP-PS-1 15-0 Revision 7 Page 6 of 18 SPECIFIC TASKS:
HOW:
INITIALS 8d.
Record Analysis Date/Time and CTE Standardization Number of each sample on Attachment B.
8e.
Attach printouts of all isotopic analyses to Attachment B.
8f.
Notify Chemistry Coordinator of analysis results.
- 9.
At completion of analysis, place samples in lead brick storage cave in fume hood of Sample Prep Room.
- 10.
Perform pre-analysis sample 1 Oa.
Obtain contact dose rate on center preparation of previous bottom of sample cask. Record on particulate/iodine sample removed Attachment C, SPING from SPINGs. Perform all sample Particulate/Iodine Samples.
preparations in fume hood.
1 Ob.
If contact dose rate is > 2.5 R/hr on center bottom of sample cask, sample contains > 5 Curies.
Perform the following:
(1) Determine sample activity in Curies from Attachment D.
Record on Attachment C.
(2)
Determine Vent Release rate in accordance with Attachment C, page 2.
(3) GO TO Step 12.
1 Oc.
If contact dose rate is < 2.5 R/hr on center bottom of sample cask, remove sample holder from sample cask.
(1) Do not remove sample holder from two plastic bags.
(2)
Stand ionization chamber at 36 inch line of lead brick tunnel.
Align center of detector with expected center of sample holder.
TAB O EP-PS-1 15-0 Revision 7 Page 7 of 18 SPECIFIC TASKS:
HOW:
INMTIALS (3)
Place back of sample holder flush with back of lead brick tunnel.
(4)
Obtain dose rate 36 inches from sample.
1 Od.
If dose rate is > 300 mR/hr at 36 inches, sample contains > 800 mCuries.
(1) Replace sample holder in cask.
(2)
Determine sample activity in Curies from Attachment E.
Record on Attachment C.
(3)
Determine Vent Release Rate in accordance with Attachment C, page 2.
(4)
GO TO Step 12.
1Oe.
If dose rate is < 300 mR/hr at 36 inches, obtain dose rate 18 inches from sample.
(1)
If dose rate is > 50 mR/hr at 18 inches, replace sample holder in cask.
(2)
Determine sample activity in mCuries from Attachment F.
Record on Attachment C.
(3)
Determine Vent Release Rate in accordance with Attachment C, page 2.
(4)
GO TO Step 12.
1Of.
If dose rate is < 50 mR/hr at 18 inches, obtain contact dose rate (closed window) on sample.
(1)
If contact dose rate is > 50 mR/hr, replace sample holder in cask.
TAB O EP-PS-1 15-0 Revision 7 Page 8 of 18 SPECIFIC TASKS:
HOW:
INITIALS (2)
Determine number of mCuries on sample by:
- mCi = Contact Readinq on Sample Record on Attachment C.
(3)
Determine Vent Release Rate in accordance with Attachment C, page 2.
(4)
GO TO Step 12.
1Og.
If contact dose rate is < 50 mR/hr, remove sample holder from two plastic bags.
(1) Remove sample(s) from sample holder(s).
(2)
Transfer iodine cartridge to clam shell holder and blow instrument air through iodine cartridge in same direction of flow as sample flow for approximately 1 minute, as required.
(3)
Wrap iodine cartridge in clean plastic film.
(4)
Place particulate filter in Petri dish and wrap in clean plastic film.
(5)
Transfer samples to Counting Room for analysis.
- 11.
Perform isotopic analysis on 11 a.
Determine sample volume for particulate filter and iodine cartridge.
isotopic analysis.
(1) Record on Attachment B.
(2)
Enter sample volume for gamma spectroscopy analysis.
TAB O EP-PS-1 15-0 Revision 7 Page 9 of 18 K
SPECIFIC TASKS:
HOW:
INITIALS 11 b.
Analyze iodine cartridges in accordance with CH-RC-071, Radiochemical Analysis of High Activity Iodine Cartridge Samples.
(1) Record the concentration of each detected iodine from gamma spectroscopy analysis on Attachment B.
(2)
Add concentrations of all iodines to determine Total Iodine Concentration. Record on Attachment B.
(3)
Using the formula on Attachment B, multiply Total Iodine Concentration by a correction factor (for line loss and collection efficiency) and by Stack Flow in order to determine Total Iodine Vent Release Rate.
11 c.
Analyze particulate filter in accordance with CH-RC-076, Gamma Spectral Analysis Using the ND9900.
(1) Record the concentration of each detected particulate from gamma spectroscopy analysis on Attachment B.
(2)
Add concentrations of all particulates to determine Total Particulate Concentration.
Record on Attachment B.
(3)
Using the formula on Attachment B, multiply Total Particulate Concentration by a correction factor for line loss and by Stack Flow in order to determine Total Particulate Vent Release Rate.
TAB O EP-PS-1 15-0 Revision 7 Page 1 0 of 18 SPECIFIC TASKS:
HOW:
INITIALS 11d.
Record Analysis Date/Time and CTE Standardization Number of each sample on Attachment B.
11e.
Attach printouts of all isotopic analyses to Attachment B.
1 1f.
Notify Chemistry Coordinator of analysis results.
- 12.
At completion of analysis, place samples in lead brick storage cave in fume hood of Sample Prep Room.
TAB O EP-PS-1 15-0 Revision 7 Page 11 of 18 Attachment A VENT NOBLE GAS ANALYSIS II.
VENT NOBLE GAS ANALYSIS Sample Source Sample DateMme SPING Sample Flow cc/min Stack Flow cc/min PAVSS Sample Flow cfm x 2.83 E 4 =
cc/min PAVSS Stack Flow cfm x 2.83 E4 =
cc/min SAMPLE DILUTIONllSOTOPIC ANALYSIS Sample Original Dilution 1 Dilution 2 Dilution 3 Dilution 4 Sample #
Dil Factor 1
14.7 231 3623 5.69 E +4 Dose Rate Corrected Sample Volume Following Dilution: (for isotopic analysis only)
Volumemoq
=
14 7 cc Sample Vol =
14 7 Dil Factor Volumewop
=
cc Analysis Date/Time I CTE STANDARDIZATION #
Noble Gas Concentration x
Stack Flow
=
Release Rate (p Cdcc)
(cc/min)
(p CMfnin)
Kr-85 x
Kr-85m x
(Given Above) =
Kr-87 x
(Given Above) =
Kr-88 x
(Given Above) =
Xe-133 x
(Given Above) =
Xe-1 35 x
(Given Above) =
x (Given Above) =
x (Given Above) =
Total Noble Gas Vent Release Rate p Cimin Perfrmed By Date Reviewed By Date
TAB O EP-PS-1 15-0 Revision 7 Page 12 of 18 Attachment B VENT PARTICULATE/IODINE ANALYSIS NOTE:
Computer Program 'Vent" may be used instead of this form (Surveillance).
I.
VENT PARTICULATE/IODINE ANALYSIS Sample Source I Sample DateMme SPING Sample Flow cc/min SPING Stack Flow cc/min Sample Start Date/Time Sample Stop Date/Time Sample Flow: ccImin x Sample Duration:
min = Sample Vol:
cc Iodine Cask Dose Rate mR/hr Filter Cask Dose Rate mR/hr PAVSS Sample Flow cfm x 2.83 E 4 cc/ft3 =
cc/min PAVSS Stack Flow cfm x 2.83 E 4 cc/ft3 =
ccmin Sample Volume = (Final Totalizer Flow -Initial Totalizer Flow) x 2.83 E 4 ccft3 Sample Volume = (
ft -
ft3) x 2.83 E 4 ccft3 cc II.
SAMPLE DATA Sample Particulate Iodine Sample #
Analysis Date/Time CTE Standardization #
Dose Rate Tech Ill.
IODINE RESULTS lodines Concentration p Ct/cc 1-131 1-132 1-133 1-134 1-135 Total Iodine Concentration Total Iodine Release Rate (p Ci/min) = Total Iodine Conc. (p Ci/cc) x Corr. Factor x Stack Flow (cc/min)
=_uCi/cc x A* x cc/min
.Ci/min
- A=1.7 for SPING; A=1.8 for PAVSS
TAB O EP-PS-1 15-0 Revision 7 Page 13of 18 Attachment B VENT PARTICULATE/IODINE ANALYSIS (continued)
IV.
PARTICULATE RESULTS Particulates Concentration p Ci/cc Sr-91 Sr-92 Y-92 Zr-95 Zr-97 Mo-99 Ru-103 Te-132 Cs-34 Cs-37 Cs-1 38 Ba-140 La-140 Ce-141 Ce-144 Total Particulate Concentration Total Particulate Release Rate (p CUmin) = Total Part. Conc. (p Ci/cc) x Corr. Factor x Stack Flow (cc/min) h, Cicc x *B_
x cctmin
=p Cmin
- B=3.6 for SPING; B=4.3 for PAVSS Pereormed By Date Reviewed By Date
TAB O EP-PS-1 15-0 Revision 7 Page 14 of 18 Attachment C
- 1.
SPING PARTICULATE/IODINE SAMPLES Sample Source l Sample #
I Survey Meter #
Sample Start Date/Time Sample Stop Date/Time Sample Duration minutes Stack Flow cc/min SPING PARTICUALTE-IODINE SAMPLE Sample ActMty = Contact Reading on Sample 1 00 mR/hr/mC4 Perform isotopic analysis of sample
TABO EP-PS-1 15-0 Revision 7 Page 15 of 18 Attachment C SPING PARTICULATE/IODINE SAMPLES (continued)
FOR SAMPLES > 50 mR/HR ON CONTACT:
- 1.
Convert sample activity (Ci or mCi) to V Ci:
pCa=
Curies x (1 E 6 p) OR mCuries x (1 E 3 C Ci mCi
=
pCi
- 2.
Determine sample volume:
cc
=
(Sample Flow) x (Sample Duration)
=
(
cc/min) x (
minutes)
=
cc
- 3.
Divide sample activity by sample volume to determine sample concentration:
p CVcc
=
Sample Activity =0 Sample Volume cc P C~lcc
- 4.
Multiply sample concentrabon by Stack Flow to determine Vent Release Rate:
p CUmin
=
(Sample Concentration) x (Stack Flow)
=
(
,p CLUcc) x (
cc/min)
Performed By Date
.Reviewed By Date
TABO EP-PS-1 15-0 Revision 7 Page 16 of 18 Attachment D SAMPLE ACTIVITY BASED ON CONTACT DOSE RATE AT BOTTOM OF PARTICULATE/IODINE SAMPLE CASK 140 Y
'V
'V V
/
120 100
.a C
.cZ 80 60 I IT 40 20 0
10 20 30 40 50 60 RFhr at bottom of sample cask
TAB O EP-PS-1 15-0 Revision 7 Page 17 of 18 Attachment E SAMPLE ACTIVITY BASED ON DOSE RATE AT 36 INCHES FROM PARTICULATE/IODINE SAMPLE 8
7 6
5~
.E4 2
0 500 1000 1500 2000 2500 mFlhr at 36 inches
TAB O EP-PS-1 15-0 Revision 7 Page 18 of 18 Attachment F SAMPLE ACTIVITY BASED ON DOSE RATE AT 18 INCHES FROM PARTICULATE/IODINE SAMPLE 600 500 400 CD 200 100 0
200 400 600 800 mRlhr at 18 inches
TAB P EP-PS-1 15-P Revision 5 Page 1 of 8 v MAJOR TASK:
Collect and analyze sample from Reactor Building Sample Station. Sample has potential to be highly radioactive.
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
After briefing and assignment and following setup of appropriate Chemistry Lab.
la.
Obtain the following supplies:
,Respiratory protection devices Hi-range and extremity dosimetry Survey meter calibrated at highest range Sample bottles (250 mL polyethylene preferred)
Remote handling device Plastic Bags Key to Reactor Building Sample Station, if required 1 b.
Check the following on survey meter:
Calibration has not expired.
Battery indication is good.
Source check is satisfactory.
1c.
Place survey meter in plastic bag and seal.
- 2.
If Reactor Water Recirc sample is required, request Operations ensure the following valves are OPEN:
2a.
Sample trip valve HV-1 F019 (HV-2F01 9).
2b.
Sample trip valve HV-1 F020 (HV-2F020).
- 3.
Don protective clothing and respiratory protection as directed by Radiation Protection Coordinator.
- 4.
Ensure each team member present has required dosimetry (TLD, SRD, and required special dosimetry).
- 5.
Ensure survey meter is on highest range.
- 6.
Notify Chemistry Coordinator before leaving Chemistry Lab.
TAB P EP-PS-1 15-P Revision 5 Page 2 of 8 SPECIFIC TASKS:
HOW:
INITIALS
- 7.
Proceed to Reactor Building Sample Station via best route while continuously monitoring radiation levels and status of CAMs and ARMs.
7a.
Retreat to low background area and notify Chemistry Coordinator if any of the following conditions are encountered:
(1) General area radiation levels exceed 1,000 mrem/hr at any time.
(2)
Total annual whole body exposure (TEDE) approaches 2000 mrem.
- 8.
Monitor general area dose rates at the Sample Station.
NOTE:
If general area radiation levels exceed 1,000 mremlhr at any time, immediately retreat to low background area and notify Chemistry Coordinator.
8a.
Continuously monitor radiation levels while entering Sample Station.
8b.
Record Reactor Building Sample Station area radiation monitor reading and report to the Chemistry Coordinator.
RBSS ARM=
mR/hr.
Chemistry Coordinator notified.
8c.
Ensure hood ventilation is functioning prior to collecting sample.
8d.
Ensure sample cask is available at Sample Station.
TAB P EP-PS-15-P Revision 5 Page 3 of 8 SPECIFIC TASKS:
HOW:
INITIALS CAUTION IF CONTACT RADIATION LEVELS ON SAMPLE CONTAINER EXCEED 5000 MRIHR ABOVE BACKGROUND AT ANY TIME DURING SAMPLE COLLECTION, IMMEDIATELY SHUT OFF SAMPLE FLOW AND NOTIFY CHEMISTRY COORDINATOR.
- 9.
Obtain required sample.
9a.
Check applicable sample at Grab Sample and Bypass (GSB) Module to confirm flow through module has been established.
NOTE:
If flow was NOT Previously established, allow sufficient flush time through module at approximate flow of 1200 m/min before collecting sample.
Sample Flush Time Rx H20 Influent 2 minutes Rx H20 Recirc 4 minutes 9b.
Open appropriate sample valve and flush approximately 30 mL.
9c.
Collect approximately 100 ml of sample using remote handling device if necessary.
(1) Continuously monitor sample container for quick detection of high dose rates.
(2)
Highest general area dose rates may occur at center of sample station due to location of cooler.
9d.
Shut sample valve and cap bottle.
Rinse bottle with demin water and wipe dry.
9e.
Place sample bottle in plastic bag.
TAB P EP-PS-115-P Revision 5 Page 4 of 8 SPECIFIC TASKS:
HOW:
INITIALS
- 10.
Obtain contact dose rate on sample 10a.
Obtain contact dose rate (closed bottle and determine approximate window),on sample bottle.
sample volume.
Sample Bottle dose rate:
mR/hr 1 Ob.
If contact dose rate on sample bottle is < 100 mrem/hr (closed window) above background place sample in plastic bucket for transport to lab.
1 Oc.
If contact dose rate on sample bottle is > 100 mrem/hr (closed window) above background, place sample in lead cask for transport to lab.
(1) Obtain contact dose rate on sample cask.
Cask dose rate:
mR/hr (2)
If contact dose rate on sample cask is greater than 100 mrem/hr above background, notify Chemistry Coordinator for instructions.
1Od.
Record sample source and sample date and time.
(1)
Sample Source:
(2)
Sample Date/Time:
l (3)
Sample Volume:
ml
- 11.
Notify Chemistry Coordinator of sample dose rates.
- 12.
Upon leaving Sample Station, notify Chemistry Coordinator sampling is complete.
- 13.
Notify Chemistry Coordinator upon arrival at Chemistry Lab.
- 14.
Prepare and analyze sample obtained 14a.
Place sample cask in Sample Prep from Reactor Building Sample Station.
Room.
TAB P EP-PS-1 15-P Revision 5 Page 5 of 8 L
SPECIFIC TASKS:
HOW:
INITIALS 1 4b.
Transfer TAB Q data to Attachment A, Reactor Building Sample Analysis.
- 15.
Perform pre-analysis sample 15a.
Label clean liquid PASS sample preparation in fume hood.
vial.
1 5b.
Pipette 10 ml of sample into clean liquid PASS sample vial.
15c.
Place original sample bottle in lead brick storage cave in fume hood of Sample Prep Room.
1 5d.
Obtain contact dose rate (closed window) on 10 ml sample vial.
Record dose rate on Attachment A.
- 16.
Determine dilution(s) required to Vial Dose Dilution obtain 10 ml sample < 5 mR/hr.
Rate - mR/hr Dilution Factor 0-5 Count as is 1
5-50 1:10 10 50-500 0.1:10 1.OE +2 500-5000 0.1:10 & 1:10 1.OE +3 16a.
Label required number of clean liquid PASS sample vials. Add consecutive letters to sample number to distinguish dilutions from original vial.
16b.
Prefill each clean labeled vial with required amounts of diluent and 0.01 N HNO3. Perform dilutions as follows:
(1) Use hypodermic syringe to transfer sample aliquot to prefilled liquid vial.
(2) 1:10 dilution: Add 1 ml sample to 9 ml diluent (0.01 N HNO3).
(3) 0.1:10 dilution: Add 0.1 ml sample to 9.9 ml diluent (0.01 N HNO3).
(4) Cap all vials, as required.
TAB P EP-PS-1 15-P Revision 5 Page 6 of 8 SPECIFIC TASKS:
HOW:
INITIALS 1 6c.
Record sample number, dilution(s) performed, and dilution factor on Attachment A for each dilution prepared.
1 6d.
Record contact dose rate (closed window) on Attachment A for each sample dilution.
1 6e.
Store original sample bottle and all dilution(s) except one to be analyzed in lead brick storage cave in fume hood of Sample Prep Room.
1 6f.
When diluted sample is < 5 mR/hr, wrap vial in clean plastic film and transfer to Counting Room for analysis.
- 17.
Perform isotopic analysis on sample <
1 7a.
Enter the applicable actual coolant 5 mR/hr.
volume for isotopic analysis to account for all sample dilutions.
Record on Attachment A.
Dilutions Actual Coolant Performed Volume - ml As is 10 1:10 1
0.1:10 1E-1 0.1:10 & 1:10 1E-2 17b.
Decay correct sample to time of collection.
17c.
Determine DEI-131 (pCi/ml) in accordance with CH-RC-010, Iodine Counting and Data Analysis.
1 7d.
Record Analysis Date/Time, CTE Number, and DEI-131 on Attachment A.
17e.
Attach printout of isotopic analysis to Attachment A.
17f.
Notify Chemistry Coordinator of analysis results.
TAB P EP-PS-1 15-P Revision 5 Page 7 of 8 SPECIFIC TASKS:
HOW:
INITIALS
- 18.
Perform additional analyses, as requested by Chemistry Coordinator.
18a.
Perform boron analysis in accordance with CH-CC-043, Analytical Procedures for HACH or BETZ Portable Spectrophotometer Labs, if required. Record results on Attachment A.
18b.
Perform chloride analysis in accordance with CH-CC-010, Chloride - Silver Nitrate Turbidimetric Method, if required.
Record results on Attachment A.
1 8c.
Perform pH analysis in accordance with CH-CC-030, Laboratory pH Determination, if required.
(1)
Use 0.1 ml of undiluted sample and flat surface pH probe to perform analysis.
(2)
Record results on Attachment A.
1 8d.
Notify Chemistry Coordinator of analysis results.
- 19. At completion of analyses, place sample in lead brick storage cave in fume hood of Sample Prep Room.
TAB P EP-PS-1 15-P Revision 5 Page 8 of 8 Attachment A REACTOR BUILDING SAMPLE ANALYSIS I
rarATprn iiiili nwnf cAMRbI c AmA vicc II.
Sample Source lSample Date/Time Sample Dose Rate mR/hrl SAMPLE DILUTION/RESULTS Sample Original Dilution 1 Dilution 2 Dilution 3 Sample #
Dilutions NA 1:10 0.1:10 0.1:10 & 1:10 Dilution Factor NA 10 1.0 E +2 1.0 E +3 Dose Rate Actual Coolant Volume for Isotopic Analysis ml Analysis Date/Time CTE #
l DEI-131 PCVmi Additional Performed Not Analysis x
Dilution =
Sample Analyses Performed Results Factor Results Boron x
=
ppm Chloride x
ppm pH Perforrned By lDate Reviewed By lDate
TAB Q EP-PS-1 1 5-Q Revision 6 Page 1 of 2 MAJOR TASK:
In the event of an Unmonitored Liquid Release, Collect and Analyze Liquid Samples.
SPECIFIC TASKS:
HOW:
INITIALS
- 1.
After receiving sampling instructions from Chemistry Coordinator or OSC, proceed to Cooling Tower Blowdown Sampler.
1 a.
Collect grab sample from blowdown line composite sampler.
1 b.
Collect grab samples from other locations as determined by Chemistry Coordinator.
- 2.
Transport sample(s) to Chemistry Lab for analysis.
- 3.
Perform isotopic analysis on undiluted sample.
3a.
Label sample(s) with sample location, sample number, and sample date and time.
3b.
Record the following on Attachment A, Sample Analyses for Unmonitored Liquid Release.
(1) Sample Location (2)
Sample Date/Time (3)
Sample Volume 3c.
Analyze sample in accordance with CH-RC-076, Gamma Spectral Analysis Using the ND 9900.
(1) Decay correct sample to time of collection.
(2) Record Analysis Date/Time, Standardization Number, and total activity (pCi/ml) on Attachment A.
(3)
Attach printout of isotopic analysis to Attachment A.
3d.
Notify Chemistry Coordinator/Shift Manager of analysis results.
TAB Q EP-PS-1 1 5-Q Revision 6 Page 2 of 2 Attachment A SAMPLE ANALYSES FOR UNMONITORED LIQUID RELEASE 1.
SAMPLE ANALYSES FOR UNMONITORED LIQUID RELEASE Sample Location Sample Date/Time Sample Volume ml Analysis Date/Time CTE #
Total Activity pCiml Sample Location Sample Date/Time Sample Volume ml Analysis Date/Time CTE #
Total Activity pCi/ml Sample Location Sample Date/Time Sample Volume ml Analysis Date/Time CTE #
Total Activity pCi/m Sample Location Sample Date/Time Sample Volume ml Analysis Date/Time CTE#
Total Activity pCi/ml Sample Location Sample Date/Time Sample Volume ml Analysis Date/Time CTE #
Total Activity pCi/ml Sample Location Sample Date/Time Sample Volume ml Analysis Date/Time CTE#
Total Activity pCi/ml llPerformned By lDate ILReviewed By lDate
(
(
(
Tab 2 EP-PS-1 15-2 EMERGENCY ORGANIZATION CONTROL ROOM EMERGENCY DIRECTOR (SHIFT MANAGER)
I I
OPERATORS EMERGENCY PLAN COMMUNICATOR SHIFT TECHNICAL ADVISOR (STA)
EP-AD-000-406, Revision 15, Page 1 of 3
(
(7 Tab 2 EP-PS-1 15-2 TSC ORGANIZATION
- EMERGENCY DIRECTOR
- Operations Coordinator
- Severe Accident Management Coordinator
- Denotes minimum staffing.
Rev. 41, 03/03 Susquehanna Steam Electric Station Units I and 2 Emergency Plan TSC ORGANIZATION FIGURE 6.2 EP-AD-000-406, Revision 15, Page 2 of 3
(
(
(
Tab 2 EP-PS-1 15-2 EOF ORGANIZATION lENGINEER lDOSE LIAISON SUPPORT ASSESSMENT SUPPORT EOF SUPPORT SUPERVISOR SUPERVISOR SUPERVISOR SUPERVISOR l NUCLEAR DOSE COUNTY IEl FUELS ASSESSMENT LIAISONS COMMUl ENGINEER STAFFER(S)
ELECTRICAL FIELD TEAM NEP I SUPPORT FIDIREC TORPLAN ENGINEER DRCO MECHANICAL SUPPORT RDAD!
ENGINEER MONITORING ASSIS ENGINEERTEAM ISYSTEMS LEAD ENVIRONMENTALE ENGINEER m
SAMPLINi TEAM 6E gl
- Designates minimum requirements in accordance with Table 6.2, SSES Emergency Plan.
EP-AD-000-406, Revision 15, Page 3 of 3