Text

Discharge Self-Monitoring Report for 2nd Quarter of 2015
	ML15217A234
Person / Time
Site:	Diablo Canyon
Issue date:	07/20/2015
From:	Cortese K; Pacific Gas & Electric Co
To:	; Office of Nuclear Reactor Regulation, State of CA, Central Coast Regional Water Quality Control Bd
References
	DCL-2015-532
	Download: ML15217A234 (133)
	v • d • e

Electric Gas SPacific Company and Diablo Canyon Power Plant P.O9. Box 56 Avila B~each, CA 93424 PG&E Letter DCL-2015-532 I Electronic Submission CIWQS Web Application July 20, 201*5 California Regional Water Quality Control Board Central Coast Region Attn: Monitoring and Reporting Review Section 895 Aerovista, Suite #101 San Luis Obispo, CA 93401-7906 In accordance with Order 90-09, NPDES No. CA0003751, the 2 nd Quarter 2015 report on Discharge Self-Monitoring at Diablo Canyon Power Plant (DCPP) is provided. This letter and accompanying report summary has been attached to the State CIWQS application data submittal (eSMR). State DMR Forms are additionally incorporated in the CIWQS electronic data submittal (eDMR).

Facility Name: Pacific Gas & Electric Company Diablo Canyon Power Plant Address: P.O. Box 56 Avila Beach, CA 93424 Contact Person: Bryan Cunningham Job

Title:

Supervisor, Environmental Operations Phone Number: (805) 545-4439 Order No. 90-09, NPDES No. CA0003751 WDRJNPDES Order Number:

Type of Report: (check one) QUARTERLY ANNUAL Quarter: (check one): I st 2 nd 3 rd 4 th

[] -I. LI Year: 2015 (Annual Reports for DCPP are Jan-Dec)

Violation(s) (Place an X by the [] No (there are no violations to report) LI Yes appropriate choice):

7H(-

PG&E Letter DCL-2015-532 CRWQCB Central Coast Region July 20, 2015 Page 2 If Yes is marked (complete a-g):

a) Parameter(s) in Violation:

b) Section(s) of WDRJNPDES Violated:

c) Reported Value(s):

d) WDR/NPDES Limit/Condition:

e) Dates of Violation(s): (If "*YES", see overview section of attached report)

(reference page of report/data sheet) t') Explanation of Cause(s): (If "YES", see overview section of attached report)

(attach additional information as needed) g) Corrective Action(s): (If "YES", see overview section of attached report)

(attach additional information as needed)

PG&E Letter DCL-2015-532 CRWQCB Central Coast Region July 20, 2015 Page 3 1 certify under penalty of law that this document, the CIWQS data submittal, and all associated attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. The results of the influent and effluent monitoring presented are the observed results of the measurements and analyses required by the monitoring program, and is neither an assertion of the adequacy of any instrument reading or analytical result, nor an endorsement of the appropriateness of any analytical or measurement procedure. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

If you have any questions or concerns regarding the report provided, or require additional information, please contact Bryan Cunningham at (805) 545-4439.

Sincerely, Name: Kenneth W. Cortese

Title:

Manager, Chemistry and Environmental Operations- Diablo Canyon Power Plant 201 5532/j1kbkc

PG&E Letter DCL-2015-532 CRWQCB Central Coast Region Juiy 20, 2015 Page 4 cc: PDF Formatted Copy of CIWQS Application Submittal:

Regional Administrator Licensing Assistant, Operations Branch U.S. Nuclear Regulatory Commission Region IV 1600 East Lamar Boulevard Arlington, TX 76011-4511 Hardcopy Print-Out of CIWQS Application Submittal:

U.S. Nuclear Regulatory Commission Document Control Desk Washington, D.C. 20555-0001 Thomas Hipschman Senior Resident Inspector U.S. Nuclear Regulatory Commission Diablo Canyon Power Plant 104/5

PACIFIC GAS AND ELECTRIC COMPANY Second Quarter 2015 REPORT ON DISCHARGE MONITORING AT DIABLO CANYON POWER PLANT TABLE OF CONTENTS OVERVIEW........................................................... 1

SUMMARY

OF MONITORING PROGRAM A. Monitoring of Plant Influent and Effluent ................... 2 B. Monitoring of Receivinq Waters............................. 2 C. Sodium Bromide Treatment Program ...................... 2 APPENDIX 1: NPDES Discharge Points

OVERVIEW

1. During the second quarter of 2015, discharges occurred from Discharge Paths 001 (once through cooling water), 001 B, 001 D, 001 E, 001 F, 001 (3, 001 H, 001 L, 001 M, 001 N, 001 P, and 002 through 005. No discharges occurred from Discharge Paths 0011I, 001 J, 001K, 006 through 015, 016, and 017. A list of all of the permit discharge pathways, including name and number, is provided in Appendix "1.-

2. The substances listed in Table B of the California Ocean Plan were each analyzed for and reported in the permit renewal application and application updates for Diablo Canyon Power Plant (DCPP) submitted in 1994, 2001, and 2011. There have been no changes in activities conducted at the plant that would have significantly affected the results previously reported in the above referenced documents. Ocean Plan Table B substances not analyzed for this quarter were not added to any plant discharge streams..

3. During the second quarter of 2015, maintenance activities that required draining of closed cooling water systems were performed, and are summarized below. PG&E received concurrence from the CCRWQCB in response to letters dated July 19, 1995 (PG&E Letter DCL-95-1 56), May 23, 1996 (PG&E Letter DCL-96-522), and May 19, 1997 (PG&E Letter DCL-97-533) regarding the use of glutaraldehyde and isothiazolin to control microbiological growth and corrosion in DCPP's closed cooling water systems.

Discharges are drained at a flow rate such that the chronic toxicity level remains below the "No Observable Effect Concentration" (NOEC) at NPDES Discharge 001.

VolumeGlutarldehyd Isothazolin Total Ol&Ges Volue Gltaradehde Iothizoln usie&nGeas at Sytm (gallons) (mg/I) (mg/I as Cr) Solids (mg/I) __mgll)___

0/91toUnit 1 ICW 200 0.0 3.2 2.6 < 1.4 04/23/15

4. Two events affected the results of continuous chlorine monitoring at Discharge 001 during the second quarter 2015. For each of these events, an engineering evaluation was subsequently completed as authorized by the Regional Board in accordance with PG&E's January 5, 1994 letter. Event intervals, affected monitor, number of affected results, the cause(s), and corrective action(s) have been tabulated below. The engineering evaluations were based on recorded chemical injection rates, and main condenser waterbox inlet chlorine monitoring results for the respective unit. These factors were used to calculate estimates of actual chlorine concentration for the respective monitor at Discharge 001 during the event interval. The estimates were then used to replace results indicated by the affected monitor. Results from the engineering evaluations were all below the applicable calculated California Ocean Plan discharge limit of 89-pg/L.

Interval Affected Replaced Cause Corrective Actions Monitor Readings _____________ ____ _______

Monitor over-response 05/29/15 to Unit 2 29 indicated by QC check result Monitor calibrated.

06/03/15 that was greater than upper control limit.

Monitor over-response 06/06/15 to Unit 2 72 indicated by QC check result Monitor probe replaced &

06/17/15 that was greater than upper monitor calibrated.

______________________________control limit.

SUMMARY

OF MONITORING PROGRAM A. Monitoringq of Plant Influent and Effluent

1. The results of the April, May, and June 2015 plant influent and effluent monitoring have been reported via the CIWQS web application to which this letter is attached.

2. The laboratory report for one acute bioassay on water sampled from Discharge 001, performed May 12-16, 2015, is attached to the ClWQS application submittal. The acute bioassay results show that toxicity was 0.0 TUa (no acute toxicity).

Note: The 0. 0 TUa value is not included in the CIWQS application spreadsheet as the formatting of the data spreadsheet does not accommodate zero value entries.

3. The laboratory report for one chronic bioassay on water sampled from Discharge 001, performed May 12-14, 2015, is attached to the ClWQS application submittal.

The chronic bioassay results show that toxicity was 1.0 TUc (no chronic toxicity).

B. Monitoring of Receivinq Waters

1. Ecological Studies at Diablo Canyon Ecological studies in the vicinity of Diablo Cove conducted during the second quarter continued under the Diablo Canyon Receiving Water Monitoring Program (RWMP) as requested in a letter from the Central Coast Regional Water Quality Control Board (CCRWQCB) dated December 9, 1998, and as detailed in a letter (PG&E Letter DCL-99-503) dated January 8, 1999. This program includes tasks from the Ecological Monitoring Program (EMP) with additional stations and increased sampling frequencies. The RWMP replaces the EMP and the Thermal Effects Monitoring Program (TEMP).

2. In Situ Bioassay Results of the Mussel Watch Program will be reported to the CCRWQCB directly from the California Department of Fish and Wildlife in the Department's periodic report for this program.

C. Sodium Bromide Treatment Program Diablo Canyon Power Plant is continuing the use of sodium bromide and sodium hypochlorite to control macrofouling growth for both Units. Both circulating water conduits of each Unit can be chemically treated simultaneously. Each treated conduit typically receives a twenty-minute injection every four hours (six injections a day) of sodium bromide in combination with sodium hypochlorite.

Each chemical injection treatment attempts to achieve a target concentration in the range of 250-300 parts per billion (ppb) Total Residual Oxidant (TRO) when measured at the inlet waterbox of the condenser. Discharge TRO concentrations measured at the plant outfall remained below NPDES permit limitations and the calculated Ocean Plan limit throughout the quarter.

Both conduits of Unit 1 were treated with simultaneous injections of sodium bromide and sodium hypochlorite six times a day throughout the second quarter with one brief interruption in May due to an equipment power supply failure.

Both conduits of Unit 2 were treated with simultaneous injections of sodium bromide and sodium hypochiorite six times a day throughout the second quarter with one brief interruption in May due to an equipment power supply failure.

APPENDIX 1 DIABLO CANYON POWER PLANT NPDES DISCHARGE POINTS DISCHARGE NUMBER DESCRIPTION 001 Once-Though Cooling Water 001 A Firewater Systems 001 B Auxiliary Salt Water Cooling System 001 C Discharge Deleted 001 D Liquid Radioactive Waste Treatment System 001 E Service Cooling Water System 001 F Turbine Building Sump 001 G Make-Up Water System Waste

__________________________Effluent 001 H Condensate Demineralizer Regenerant 001 I Seawater Evaporator Blowdown 001 J Condensate Pumps Discharge

__________________________Header Overboard 001 K Condenser Tube Sheet Leak

_________________________ Detection Dump Tank Overboard 001 L Steam Generator Blowdown 001 M Wastewater Holding and Treatment System 001 N Sanitary Wastewater Treatment System 001 P Seawater Reverse Osmosis System Blowdown 002 Intake Structure Building Floor Drains 003 Intake Screen Wash 004 Bio Lab and Storm Water Runoff 005, 008, 009, 013, 014, 015 Yard Storm Drains 006, 007, 010, 011, 012 Storm Water Runoff 016 Bio Lab Seawater Supply Pump

__________________________Valve Drain 017 Seawater Reverse Osmosis System

_________________________Blowdown Drain

CIWQS Web Application Submittal Print Out and Attached Supporting Documents eSMR PDF Report Summary: Quarterly SMR ( MONNPDES ) report for Q2 2015 Summary: Quarterly SMR ( MONNPDES ) report for Q2 2015 submitted by Kenneth Cortese (No Title) on 07/20/2015.

Facility Name: PG&E Diablo Canyon Power Plant Order Number: R3-1990-0009 Waterboard Office:Region 3 - Central Coast Case Worker: Peter Von Langen Report Effective Dates: 04/01/2015 - 06/30/2015 No Discharge Periods

N a mee ::: *'7, ::::Description> ,: :*Dates~i: :* *: ,:;::Comments ':,.,,:::: :i:*..

iablo M-O01 Diablo M-001D Diablo MV-00O.F Diablo M-O01G Diablo M-001H Diablo M-0011 04/01/2015 - 06/30/2015 *ant Seawater Evaporators no ionger in

_____________________ervice.

Diablo M-O01J 04/01/2015 - 06/30/2015 ]ondensate Pump Discharge Header not Jrained during 2Q15. No effluent

_____________________ ischarqed.

Diablo M-001K 04/01/2015 - 06/30/2015 Plant Condenser Tube Sheet Leak Detection

____________________________________________________________________________________ ________p__Tank____oumonankro logerenrsevice Dablo M-001L Diablo lM-001M Dablo M-001N Diablo M-001P Dablo M-002 Dablo M-003 laiabl M-004 laiabl M-005 Diablo M-008 D4/01/2015 - 06/30/2015 No storm water run-off or other

____________________precipitation discharge events during 2015.

Dablo M-009 D4/01/2015 - 06/30/2015 No storm water run-off or other

____________________precipitation discharge events during 2015.

laiabl M-013 D4/01/2015 - 06/30/2015 No storm water run-off or other

_____________________ precipitation discharge events during 2015.

liablo M-015 D4/01/2015 - 06/30/2015 No storm water run-off or other

_____________________precipitation discharge events during 2015.

)iablo M-016 :4/01/2015 - 06/30/2015 Bio Lab Seawater Supply Line Valve Box not drained during 2Q15. No effluent

_____________________ ischarqed.

)ablo M-017 :4/01/2015 - 06/30/2015 Seawater RO System Blowdown Line not

_____________________ _______________________________________________________________ __drained___dur__nq__2raied.duingc0h5. qischrgeerrelyused l)ablo M-INF Self-Determined Violations No Violations Entered Attachments Page 1 of 29

Cover Letter (Uploaded File)

PGE DCL2015532

... 2nd-Q: 2015 .... DSMR

... Summary.pdf

.. i : : .. Tte* . . i,;:,:,Dt07/20/2015Ulae 1073058:

Fie zbytes" Data Summary Analytical Results Location Parameter= Anal. Method. Sample , Analysis Qual= Result Units 'MDL ,ML *!RL:* Review QA, Comments Data Source:

............ ,: "DatefTime Date :*

Priority Codes,:I '*

M-001 Ammonia, Total (as N) A4500NH : 04/29/2015 : 05/09/2015 = 0.56 mg/L No See Attachment 2, CDFAnalytical Standard Method 07:41:00 Contract Lab Report Calculated_072C (19gth) 4500-NH: 2015.zip

Nitrogen

'(Ammonia)

M-001 Chromium (Total) DU : Data 04/02/2015 : 04/21/2015 ND ug/L 5 NIo !CDFAnalytical Unavailable 09:57:00 Calculated_072(

_______ _____2015 .zip M-001 Chromium (Total) DlU : Data 05/07/2015 : 05/14/2015 ND ug/L 5 Nlo CDFAnalytical_

Unavailable 09:55:00 Calculated_072

________2015 .zip Mv-001 Chromium (Total) DU : Data 06/09/2015 : 06/10/2015 ND ug/L 5 N1o CDFAnalytical_

Unavailable 07:22:00 Calculated_072

______ ______________2015 .zip M~-001 Chronic Toxicity DU : Data 05/11/2015 : 05/12/2015 = 1 TUc No See Attachment 2. CDFAnalytical_

Unavailable 07:30:00 Contract Lab Report Calculated_072C

______ _____________2015.zip Mv-001 Copper, Total DU : Data 04/02/2015 : 04/21/2015 DNQ 8.2 ug/L 5 10 Nlo LDFAnalytical_

Unavailable 09:57:00 Calculated_072

______ ______________2015 .zip M-001 Copper, Total DO : Data 05/07/2015 : 05/14/2015 DNQ 6 ug/L 5 10 Nlo CDFAnalytical Unavailable 09:55:00 Calculated 072(

_____ ______ _____________2015 .zip M-001 Copper, Total DO : Data 06/09/2015 : 06/10/2015 DNQ 7 ug/L 5 10 Nlo CDFAnalytical_

Unavailable 07:22:00 Calculated_072C

_______ _____ ______ _____2015 .zio M-001 Nickel, Total DO : Data 04/02/2015 : 04/21/2015 ND ug/L 5 INo CDFAnalytical_

Unavailable 09:57:00 Calculated_072(

_______ ______ _______ _________ __________ 015zip 2015_

M-001 Nickel, Total DU : Data 05/07/2015 : 0)5/14/2015 ND ug/L 5 No CDFAnalytical_

Unavailable 09:55:00 Calculated_072(

_________________ ______ __________________ ____2015 .zip M-001 Nickel, Total DO : Data 06/09/2015 : =06/10/2015 ND ug/L 5 No CDFAnalytical_

Unavailable 07:22:00 Calculated 072C

____________ ____ __2015.015zii Page 2 of 29

,Location :.,:Parameter:: , "Anal.. Method: ::*Sample!

Date..Time... Analysis: :ual~i,: Result ,Units: MDL RI.::*Priority,

iReview Codest*: 'QA , :,Comments, : :1 ,Data Source.

M:L'.::

.. Date ::* ::

Mv-o01 pH A4500HB : 04/02/2015 :04/02/2015 = 7.72 SU No CDFAnalytical Standard Method 09:57:00 Calculated_072(

(19th) 4500-H+ B 2015.zip pH by E=lectrometric VMethod______________

M-001 pH A,4500HB : 05/07/2015 : 05/07/2015 =7.75 SU NJo CDFAnalytical_

Standard Method 09:55:00 Calculated_072(

(,19th) 4500-H+ B: 2015.zip pH by Electrometric Mlethod ________ __ __ ________

M-001 pH A,4500HB : 06/09/2015 : 06/09/2015 =7.95 SU No -CDFAnalytical_

Standard Method 07:22:00 Calculated_072(

(,19th) 4500-H+ B: 2015.zip pH by Electrometric Method________ ____________

M-001 Zinc, Total U:U : Data 04/02/2015 : 04/21/2015 ND :uglL 5 No -CDFAnalytical_

Unavailable 09:57:00 C*alculated_072(

_______ ____ ____ ______2.015.zip M-001 Zinc, Total U)U : Data 05/07/2015 : 05/14/2015 ND ug/L 5 No CDrAnalytical_

Unavailable 09:55:00 Calculated_072(

_______ ____ ____ ______2015 .zip M-001 Zinc, Total U)U : Data 06/09/2015 06/10/2015 ND uglL 5 No CDFAnalytical_

Unavailable 07:22:00 Calculated_072(

_______ ____ ____ ______ _____________2015 .zip M-001D Oil and Grease E1664A : HEM ant 05/26/2015 : 05/26/2015 ND mg/L 1.4 N1o Monthly avg result. CDFAnalytical_

SGT-HEM by 11:32:00 See Attachment 1, Calculated_072(

Extraction and Tab 6 2015.zip Gravimetry. Rev.

'A ____ _____________

M-O01D Oil and Grease E1664A : HEM ant 06/25/2015 : 06/25/2015 ND mg/L 1.4 Nlo Monthly avg result. CDFAnalytical_

SGT-HEM by 11:14:00 See Attachment 1. Calculated_072(

Extraction and Tab 7 2015.zip Gravimetry, Rev.

M-001F Oil and Grease E1664A : HEM ant 04/02/2015 : 04/16/2015 ND mg/L 1.4 Nlo CDrAnalytical_

SGT-HEM by 07:10:00 Calculated_072 Extraction and 2015.zip Gravimetry, Rev.

A_______

M-O01F Oil and Grease E1664A : HEM anc 05/04/2015 : 05/20/2015 ND mg/L 1.4 N1o C:DFAnalytical_

SGT-HEM by 12:45:00 C2alculated_072 Extraction and 2015.zip Gravimetry, Rev.

_______________A___________

M-001F Oil and Grease E1664A : HEM anc 06/01/2015 : u)6/2312015 ND mg/L 1.4 Nlo CDF Analytical_

SGT-HEM by 07:20:00 C*alculated_072(

Extraction and 2015.zip Gravimetry, Rev.

________________________A_______ ___________________

M-001G Oil and Grease E1664A : HEM ant 04/09/2015 : u4/23/2015 ND mg/L 1.4 N1o CDF Analytical_

SGT-HEM by 09:55:00 C*alculated_072(

Extraction and 2015.zip Gravimetry, Rev.

_________________ ______________ __________ _______________ ___ _________ __A____

Page 3 of 29

Location ... Parameter ,::: Anal. MethOd' =:Sample,! Analysis. :Qual *Result : Units: ,MDL M I1 *::RL. :::Review :* QA: Comments .... Data Source, M-001G rotal Suspended Solids A2540D : 04/09/2015 04/09/2015 ND mg/L 2 -No CDFAnalytical_

(TSS) Standard Method 09:55:00 Calculated_072(

(19th) 2540 D: 2015.zip Tot. Sus. Solids

_________________Dried 103-105C__________ ____________

M-001G Total Suspended Solids A2540D : 05/06/2015 : 050612015 ND mg/L 2 -No CDFAnalytical_

(TSS) Standard Method 11:38:00 Calculated_072{

(19th) 2540 D: 2015.zip Tot. Sus. Solids

________________Dried 103-105C _______________ ________

M-O01G Total Suspended Solids IA2540D : 06/02/2015 : (16/02/2015 ND mg/L 2 No CDF Analytical (TSS) IStandard Method 12:34:00 Calc-ulated_072*

(19th) 2540 D: 2015.zip Tot. Sus. Solids

_________________ Dred 103-105C________ ___________

M-O01M Oil and Grease E1664A : HEM anc 06/13/2015 : (16/23/2015 ND mg/L 1.4 No CDFAnalytical_

SGT-HEM by 05:10:00 Calculated_072(

E-xtraction and 2015.zip Gravimetry, Rev.

M-001M Total Suspended Solids A2540D : 06/13/2015 : (16/13/2015 DNQ 3 mg/L 2 5 No CDFAnalytical_

(TSS) iStandard Method 05:10:00 Calculated_072(

(19th) 2540 0: 2015.zip

-ot. Sus. Solids

________________Dried 103-105C________________

M-001P Oil and Grease E-1664A : HEM anc 04/13/2015 : 04/23/2015 ND mg/L 1.4 No CDFAnalytical_

SGT-HEM by 10:03:00 Calculated_072[

Extraction and 2015.zip Gravimetry, Rev.

A_________________

M-003 Oil and Grease E1664A : HEM anc 04/02/2015 04/23/2015 ND mg/L 1.4 No CDF Analytical_

S*GT-HEM by 12:21:00 C*alculated_072(

Extraction and 2015.zip Gravimetry. Rev.

A________ ___ ___ ____________

M-003 pH A4500HB : 04/01/2015 : 04/01/2015 = 7.77 SU No CDFAnalytical_

Standard Method 12:20:00 Calculated_072(

(19th) 4500-H+ B: 2015.zip pH by Electrometric Method ___ _________

M-003 pH A4500HB : 05/05/2015 : 05/05/2015 = 7.81 SU NJo CDFAnalytical Standard Method 09:17:00 Calculated_072(

(19th) 4500-H+ B: 2015.zip pH by Electrometric Method________________

M-003 pH A4500HB : 06/01/2015 : 06/01/2015 =7.8 SU N1o CDFAnalytical_

Standard Method 12:17:00 Calculated_072(

(19th) 4500-H+ B: 2015.zip pH by Electrometric Method ____ _________

M-004 Oil and Grease E1664A : HEM ant 04/01/2015 : u)4/16/2015 ND mg/L 1.4 N1o CDF Analytical_

SGT-HEM by 12:26:00 Calculated_072*

Extraction and 2015.zip Gravimetry. Rev.

__________________ A____________ ___ ______________________________ _____A___

Page 4 of 29

Location .,*:Pa~rameter* Anal. Method"

iSample AnalysiS Qual *'*ReSult*' Units* MDL: *iV, RI:L *Review :i*QA i ZComments*Y iData Source' Ml-004 pHA450OHB : 04/01/2015 :04/01/2015 =7.52 SU No CDF Analytical_

Standard Method 12:26:00 Calculated_072C (19th) 4500-H+ B: 2015.zip pH by Electrometric Method_____

Ml-004 pHA4500HB : 05/05/2015 :05/05/2015 =7.69 SU No CDFAnalytical_

Standard Method 09:26:00 Calculated_072C (19th) 4500-H+ B: 2015.zip pH by Electrometric Method_______

Ml-004 pH A4500HB : 06/08/2015 : 06/08/2015 =7.72 SU No CDFAnalytical_

Standard Method 13:13:00 Calculated_0721 (19th) 4500-H+ B 2015.zip pH by Electrometric Method _____ ____

Ml-INF Ammonia, Total (as N) A4500NH : 04/29/2015 : 05/09/2015 =0.92 mg/L No See Attachment 2, CDFAnalytical_

Standard Method 0)7:30:00 Contract Lab Report Calculated_072C (19th) 4500-NH: 2015.zip Nitrogen (Ammonia) _______________________

Ml-INF pHA4500H : 04/02/2015 : 04/02/2015 =7.68 SU No CDFAnalytical_

Standard Method 09:46:00 Calculated_0721 (19th) 4500-H+: 2015.zip

)H Value _________________

M]-INF pHA4500H : 0)5/07/2015 : 05/07/2015 =7.74 SU No CDF Analytical_

Standard Method 09:43:00 Calculated_0721 119th) 4500-H+: 2015.zip PH ValUe ____

MI-INF pHA4500H : 06/09/2015 : 06/09/2015 =7.93 SU No CDFAnalytical_

Standard Method 07:10:00 C.alculated_072G (19th) 4500-H+: 2015.zip

___________________________H Value _____ _____________ ______ ___________ ________ ______

Calculated Values

Location , Parameter. i: Calculation Sample ... Analysis. Qual I *Resulti Units; :MDL ML

RL :Review,*

f: *QA

Comments;* :Data Source

TYpe. !i :,Date/Time DateI :*Pr i rlty Codes ,*. . .. ..

..........,,indica, tor* ,:

M-001 Chlorine Usage 30-Day Average 0)4/01/2015 : 04/30/2015 = 585 10/day No Monthly avg result. CDFAnalytical_

of Daily Averages 00:00:00 See Attachment 1, Calculated 072(

______ ________ ____ ___ ___Tab 2 2.015.zip M-001 Chlorine Usage 30-Day Average 0)5/01/2015 : 05/31/2015 =561 lb/day No Monthly avg result. CDFAnalytical of Daily Averages '00:00:00 See Attachment 1, Calculated_072(

_______ __________________ ____ ______________ _________Tab 3 ?015.zip M-001 Chlorine Usage 30-Day Average 06/01/2015 : 06/30/2015 = 681 10/day No Monthly avg result. CDFAnalytical_

of Daily Averages 00:00:00 See Attachment 1, Calculated_072

_______ab T__ 4 ?015.zip M-001 Chlorine, Total Residual 30-Day Average 04/01/2015 : 04/30/2015 = 33 ug/L No Monthly avg result. CDFAnalytical_

of Daily 00:00:00 See Attachment 1, Calculated_072(

2

______ aximums ____ __ ____ab T_____2 015.zip M-001 Chlorine, Total Residual 30-Day Average 05/0:1/2015 : 05/31/2015 = 24 ug/L No Monthly avg result. CDFAnalytical_

of Daily 00:00:00 See Attachment 1, Calculated_072(

2

______ aximums __ __ _______ab T____3 " 015.zip M-001 Chlorine, Total Residual 30-Day Average 06/01/2015 : 06/30/2015 = 30 ug/L No Monthly avg result. CDFAnalytical_

of Daily 00:00:00 See Attachment 1. Calculated_072(

_________________ laximums ____ _________________ ____ab T_____4 2015.zip M-001 I-low D)aily Discharge 04/01/2015 : 04/01/2015 = 2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

___________ _____ ______ ____ ____ _________ ______ __________ 0__5.ziDzi Page 5 of 29

Location,, :*,!i:;Parameter ;:>

Calculation,* *,:*sample A,:nalysis :::Qual': Result:* Units:, iMDiI ML: i:RI- Revtew;* :Q C0mmentsi:* Data Source*

Mv-O01 Flow Daily Discharge 04/02/2015 :04/02/2015 = 2486 MIGD No CDFAnalytical 00:00:00 Calculated_D72(

________ ____________2015 .zip M-001 Flow Daily Discharge 04/03/2015 :04103/2015 = 2486 MlGD No CDFAnalytical 00:00:00 Calculated_D72(

________ _____ ____ _____________2015 .zip M-D01 Flow Daily Discharge i04/04/2015 :04/04/2015 =2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

_________ ____ 015 .zio M-001 F-low Daily Discharge 04/05/2015 :04/05/2015 = 2486 MlGD No CDFAnalytical_

00:00:00 Calculated 072

_____2015.zip Mv-001 Flow Daily Discharge 04/06/2015 :04/06/2015 = 2486 MlGD No CDFAnalytical_

,00:00:D0 Calculated_072(

________ _______________ ____2015.zip M-001 Flow Daily Discharge :04/07/2015 : 04/07/2015 =2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

________ _______ 015 .zio M-001 Flow Daily Discharge 04/08/2015 : 04/08/2015 = 2486 VMGD No CDFAnalytical_

00:00:00 Calculated_072(

____ ____ ____________2015.zip M-001 Flow Daily Discharge 04/09/2015 : 04/09/2015 = 2486 VMGD No CDFAnalytical_

00:00:00 Calculated_072(

________ ____ _____________2015.zip M-001 F-low Daily Discharge 04/10/2015 : 04/10/2015 = 2486 VMGD No CDFAnalytical_

00:00:00 Calculated_072

____ ______________ 015.zip M-001 Flow Daily Discharge 04/11/12015 : 04/11/2015 = 2486 MIGD No CDFAnalytical_

00:00:00 Calculated_072(

________ _______ __________ ____ ______2015.zip Mv-001 Flow Daily Discharge 04/12/2015 : 04/12/2015 = 2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

_______ ______________2015 .zip M-001 Flow Daily Discharge 04/13/2015 :i 04/13/2015 = 2486 'MGD NoD CDF Analytical_

00:00:00 Calculated_072(

________ _______ ____2015 .zip M-001 Flow Daily Discharge 04/14/2015 : 04/14/2015 -- 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072(

________ ____________ _____________2015.zip M-001 Flow Daily Discharge 04/15/2015 : 034/15/2015 2486 MdGD NJo CDFAnalytical_

00:00:00 Calculated_072(

________ _______ ___ _____2015.zip M-001 Flow Daily Discharge 34/16/2015 : 0)4/16/2015 = 2486 MGD NJo- CDFAnalytical 00:00:00 Calculated_072(

________ _______ ___ _____2015.zip M-001 Flow Daily Discharge 04/17/2015 : 0]4/17/2015 -- 2486 MGD NoD CDFAnalytical_

00:00:00 Calculated_072(

______________ __________2015.zip M-001 Flow Daily Discharge 04/18/2015 : 04/18/2015 = 2486 MGD N1o CDFAnalytical_

00:00:00 Calculated 072(

________ _________________2015.zip M-001 Flow Daily Discharge 04/19/2015 : 04/19/2015 =2486 MGD NoD CDF Analytical_

00:00:00 Calculated 072(

_______ ______2015.zip M-001 Flow Daily Discharge 04/20/2015 : 04/20/2015 =2486 MGD NJo CDFAnalytical_

00:00:00 Calculated_072(

2015.zip M-001 Flow D~aily Discharge 04/21/2015 : 04/21/2015 = 2486 MGD NJo CDFAnalytical 00:00:00 Calculated_072

___________ __________________ ___ _____ ______ _________ 0___

5.zizi Page 6 of 29

LoEcation* , Parameter:,* *:i:*:Calculation : Sample: *AnaIYsis Qua! '*ReUlt~, *Units: *MDL* ŽML.*I RL*'* :Review: :*Q*; *:**,Comments*; *Data Source!

M-001 Flow Daily Discharge 04/22/2015 : 4/22/2015 =2486 MGD No CDF Analytical_

00:00:00 Calculated_072(

________ ______ _________ ____ ______ _____________2015 .zip M-001 Flow Daily Discharge 04/23/2015 :04/23/2015 = 2486 vMGD No CDF Analytical_

00:00:00 Calculated 072(

____ ______________2015.zip M-001 Flow Daily Discharge 04/24/2015 :04/24/2015 =2486 MGD Nlo CDFAnalytical 00:00:00 Calculated_072(

____ ______________2015 .zip M-001 Flow D)aily Discharge 04/25/2015 : 04/25/2015 = 2486 MGD Nlo CDFAnalytical_

00:00:00 Calculated_072(

______________2015 .zip M-001 Flow Daily Discharge 04/26/2015 : 0:4/26/2015 =2486 MGD Nlo CDFAnalytical_

00:00:00 Calculated 072(

_____ ______________2015 .zip M-001 Flow Daily Discharge 04/27/2015 : 04/27/2015 = 2486 MGD Nlo CJDFAnalytical_

00:00:00 Calculated_072(

_____ ______________2015 .zip M-001 Flow Daily Discharge 04/28/2015 : 04/28/2015 = 2486 MGD Nlo CDFAnalytical_

00:00:00 Calculated_072(

_______ _____2015 .zip M-001 Flow Daily Discharge 04/29/2015 : 04/29/2015 = 2486 MGD N1o CDFAnalytical_

00:00:00 Calculated_072(

______ ______ _____________2015.zip M-001 Flow Daily Discharge 04/30/2015 : 04/30/2015 =2486 MGD Nlo CDFAnalytical_

00:00:00 Calculated_072(

2015.zip M-001 Flow Daily Discharge 05/01/2015 : 35/01/2015 = 2486 MGD Nlo CDFAnalytical_

00:00:00 Calculated_072(

______ _______2015.zip M-001 Flow Daily Discharge 05/02/2015 : 05/02/2015 =2486 MGD Nlo CDF Analytical_

00:00:00 Calculated_072(

________ _____________________ _____2015 .zip M-001 Flow Daily Discharge 05/03/2015 : 05/03/2015 = 2486 MGD N1o CDFAnalytical 00:00:00 Calculated_072C

________ ________ ______ _____________20 15 .zio M-001 Flow Daily Discharge 05/04/2015 : 0*5/04/2015 = 2486 MGD NJo CDF Analytical_

00:00:00 Calculated_072C

________ ______2015 .zip M-001 Flow Daily Discharge 05/05/2015 : 0)5/05/2015 = 2486 MGD ,No CDFAnalytical_

00:00:00 Calculated 072*

________ _____________2015 .zip M-001 Flow Daily Discharge 05/06/2015 : 0)5/06/2015 = 2486 MGD ,No CDFAnalytical_

00:00:00 Calculated_072C

_______________2015.zip M-001 Flow Daily Discharge 05/07/2015 : 0)5/07/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

________ ________________ ______2015

_____________________ .zio M-001 Flow Daily Discharge 05/08/2015 : 0)5/08/2015 = 2486 MGD No CDFAnalytical 00:00:00 Calculated 072*

_______________2015 .zip M-001 Flow Daily Discharge 05/09/2015 : 05/09/2015 = 2486 MGD No CDF Analytical_

00:00:00 Calculated_072*

_______ ____________ _____ _____20 15.zip M-001 Flow Daily Discharge 05/10/2015 : 0)5/10/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

_______ ____________ _____ ______2015 .zip M-001 Flow Daily Discharge 05/11/2015 : 05/11/12015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

___________ ______ ____ ____ ___ _____ _______________ 2___ 5.zi.zi Page 7 of 29

"Oaln:: *Prmtr!: Loato

Prmee'<

Caclain~

acatype

Smpe Date/Timei*ua* Anlyi Qa DateitPriorityRCodes Rslt

!:R~ul U its MDL ML R Review*: *iQ : :i Com~ments ,i Data Source M-001 Flow D)aily Discharge 05/12/2015 : 05/12/2015 = 2486 VlGD No CDFAnalytical_

00:00:00 Calculated_072(

_____ ______ _____________ 015.zip M-001 Flow D)aily Discharge 05/13/2015 :05/13/2015 = 2486 VMGD No CDFAnalytical_

00:00:00 Calculated_072

_______ ____ ____ _____________2015.zip, M-001 Flow D)aily Discharge 05114/2015 : 05/14/2015 = 2486 MCGD No CDFAnalytical_

00:00:00 Calculated_072(

________ ________________ ______ ___ ____ ____ ______ _____________ 015 .zip M-001 Flow Daily Discharge 05/15/2015 : 05/15/2015 = 2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

_________ _______ ___ ____ _____________ 0 15.zip M-001 Flow Daily Discharge 05/16/2015 : 05/16/2015 = 2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

________ ________________ _______ ___ ____ ______ ____________120 15.zip M-001 Flow D)aily. Discharge 05/17/2015 : 05/17/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072(

_______ ____ ____ ______ _____________2015 .zio M-001 Flow D)aily Discharge 05/18/2015 : 05/18/2015 = 2486 MGD NO CDF Analytical_

00:00:00 Calculated_072(

_______ ____ ____ ______2015.zip M-001 Flow Daily Discharge 05/19/2015 :05/19/2015 = 2486 ,vGD No CDFAnalytical_

00:00:00 Calculated_072(

_______ ____ ____ ______2015.zip M-001 Flow D)aily Discharge 05/20/2015 : 05/20/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072(

___________ ____2015 .zip M-001 Flow D)aily Discharge 05/21/2015 : 05/21/2015 = 2486 MGD Nlo CDFAnalytical_

00:00:00 Calculated_072(

_______ ____2015.zip M-001 Flow D)aily Discharge 05/22/2015 : 05/22/2015 = 2486 MGD N!o CDFAnalytical_

00:00:00 Calculated_072(

________ ________________ ___________ ____ _____________2015 .zip M-001 Flow D)aily Discharge 05/23/2015 05/23/2015 =2486 MGD N1o CDFAnalytical_

00:00:00 Calculated_072(

_____ ______________20 15 .zip M-001 Flow D)aily Discharge 05/24/2015 :05/24/2015 = 2486 MGD N1o CDF Analytical_

00:00:00 Calculated_072

_____ _____________20 15.zip M-001 Flow Daily Discharge 05/25/2015 : 05/25/2015 =2486 MGD NIo CDFAnalytical_

00:00:00 Calculated_072(

______________20 15.zip M-001 Flow D)aily Discharge 05/26/2015 : 05/26/2015 = 2486 MGD Nlo CDF Analytical_

00:00:00 Calculated_072(

______________20 15.zip M-001 Flow D)aily Discharge 05/27/2015 : 0)5/27/2015 = 2486 MGD NJo CDFAnalytical_

00:00:00 Calculated 072(

_________________________ ___________20 15.zip M-001 Flow ;Daily Discharge 05/28/2015 : 0)5/28/2015 = 2486 MGD Nlo CDFAnalytical 00:00:00 Calculated_072(

______________2015.zip M-001 Flow :Daily Discharge 05/29/2015 : 0)5/29/2015 = 2486 MCD Nlo LDFAnalytical_

00:00:00 Calculated_072(

_____________________2015.zip M-001 Flow :Daily Discharge 05/30/2015 : 05/30/2015 = 2486 MGD NJo CDFAnalytical 00:00:00 Calculated_072(

_______2015.zip M-001 Flow Daily Discharge 05/31/2015 : 05/31/2015 = 2486 MCD N*o CDFAnalytical_

00:00:00 Calculated_072(

________ _______ ______ _______ _____ __________ ____ ______ ___________ 2015.0z1izp Page 8 of 29

M-001 Flow Daily Discharge 06101/2015 :06/01/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072*

_________________2015.zip M1-001 Flow Daily Discharge 06/02/2015 :06/02/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

________2015.zip M1-001 Flow Daily Discharge 06/03/2015 : 06/03/2015 = 2486 MGD No CDFAnalytical_

0)0:00:00 Calculated_0721

________ _______ ______2015.zip M1-001 Flow Daily Discharge 06/04/2015 :06/04/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C 2015 .zip Ml-001 Flow Daily Discharge 06/05/2015 : 06/05/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_0721

________ _______ _______2015 .zip Ml-001 Flow Daily Discharge 06/06/2015 : 06/06/2015 = 2486 MGD No CDF Analytical_

00:00:00 Calculated_0721 2015 .zip Ml-001 Flow Daily Discharge 06/07/2015 : 06/07/2015 =2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

_______ _____ ______ ______20 15.zip Vl-001 Flow Daily Discharge 06/08/2015 : 06/08/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

_______________2015 .zip M-001 Flow Daily Discharge 06/09/2015 : 06/09/2015 = 2486 MGOD No CDFAnalytical_

00:00:00 Calculated_072C

________ ________________ ______ _____2015.zip M-001 Flow Daily Discharge 06/10/2015 : 06/10/2015 - 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072q

______________________ _____________2015.zip Vl-001 Flow Daily Discharge 06/11/12015 : 06/11/12015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

_______________________ _____ ______20 15.zip Ml-001 Flow Daily Discharge 06/12/2015 : 06/12/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072C

________2015.zip M-001 Flow Daily Discharge 06/13/2015 : 06/13/2015 = 2486 MGD No CDF Analytical_

00:00:00 Calculated_072C

______ __________________2015 .zip M-001 Flow Daily Discharge 06/14/2015 : 06/14/2015 = 2486 MOD No CDFAnalytical_

00:00:00 Calculated_0721

_________________ ____________20 15.zip M1-001 Flow Daily Discharge 06/15/2015 : 06/15/2015 = 2486 MOD No CDFAnalytical_

00:00:00 Calculated_072C

_____ _____________2015 .zip MI-001 Flow Daily Discharge 06/16/2015 : 06/16/2015 = 2486 MOD No CDF Analytical_

00:00:00 Calculated_072C

________________ ______________________________ ______2015 .zip Ml-001 Flow Daily Discharge 06/17/2015 : 06/17/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072[

_____________________________ _____________2015.zip Ml-001 Flow Daily Discharge 06/18/2015 :06/18/2015 = 2486 MOD No CDFAnalytical 00:00:00 Calculated_072C

_____ ______ _____________2015.zip Ml-001 Flow Daily Discharge 06/19/2015 :06/19/2015 = 2486 AGD No CDFAnalytical_

00:00:00 Calculated_072C

___________________________________ ___________ _____________2015.zip Ml-001 Flow Daily Discharge 06/20/2015 : 06/20/2015 = 2486 MOD No CDFAnalytical_

00:00:00 Calculated_072[

______ __________________ ________ ____ ______ ____ _________ 20__ 5015.ip Page 9 of 29

Loctin Cacultin Parmeer amle nayss Qal Reul Unts MD M RLi Review, QA:, ,:::Comments:: *Data Source:

M-001 Flow Daily Discharge 06/21/2015 : 06/21/2015 =2486 IAGD No CDF Analytical_

00:00:00 Calculated_072(

_____ ______________ 015.zip M-001 Flow Daily Discharge 06/22/2015 :06/22/2015 =2486 VlGD No CDF Analytical_

00:00:00 Calculated_072(

_____________ __________________2015.zip M-001 Flow Daily Discharge 06/23/2015 :06/23/2015 2486 MlGD No CDF Analytical_

00:00:00 calculated_072(

____________ ______________ 015 .zip M-001 Flow Daily Discharge 06/24/2015 : 06/24/2015 =2486 MlGD No CDFAnalytical_

00:00:00 Calculated_072(

____________ ______ ______________20 15.zip M-001 Flow Daily Discharge 06/25/2015 : :06/25/20*15 =2486 MGD No CDF Analytical_

00:00:00 Calculated_072(

_______ ____ ______ _____________2015 .zip M-001 Flow Daily Discharge 06/26/2015 : 06/26/2015 =2486 MGD Nlo CDF Analytical_

00:00:00 Calculated_072(

________________________ ______ ____ ____ _____________2015 .zip M-001 Flow Daily Discharge 06/27/2015 : 06/27/2015 =2486 4GD N~o CDrAnalytical_

00:00:00 Calculated_072(

_____ _______ _______________2015.zip M-001 Flow Daily Discharge 06/28/2015 : 06/28/2015 = 2486 MGD No CDFAnalytical_

00:00:00 Calculated_072(

_______ ____ _____________2015.zip M-001 Flow Daily Discharge 06/29/2015 : 06/29/2015 = 2486 MGD N~o CDFAnalytical_

00:00:00 Calculated_072(

____________ ___________________20 15.zip M-001 Flow Daily Discharge 06/30/2015 : 06/30/2015 = 2486 MGD N1o CDFAnalytical 00:00:00 Calculated_072(

_________________ _______________2015 .zip M-001 Temperature :24-hour Average 04/01/2015 : 04/01/2015 =69.8 Degrees Nlo CDF Analytical 00:00:00 F Calculated_072*

________________________ ____2015.zip M-001 Temperature 24-hour Average 04/02/2015 : 04/02/2015 68.9 Degrees N1o CDFAnalytical_

00:00:00 F Calculated 072(

________ ________________ ______ _____2015.zip M-001 remperature 24-hour Average 04/03/2015 : 04/03/2015 =69.3 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072(

_________________ ____________20 15.zip M-001 Temperature 2*4-hour Average 04/04/2015 : 04/04/2015 =69.3 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072(

________ ______________2015.Zip M-001 Temperature 24-hour Average 04/05/2015 : 04/05/2015 =69 Degrees N1o CDFAnalytical_

00:00:00 F Calculated 072C

______________ _____________2015.zip M-001 Temperature 24-hour Average 04/06/2015 : 04/06/2015 =69.5 Degrees :No CDFAnalytical_

00:00:00 F Calculated_072C

____________ ______ _________ 2015.015zip M-001 Temperature 24-hour Average 04/07/2015 : 04/07/2015 70.3 Degrees No CDF Analytical_

00:00:00 F Calculated_0721

______________ ______20 15.zip M-001 Temperature 24-hour Average 04/08/2015 : 04/08/2015 =70.6 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

___________________________________ ______2015.zip M-001 Temperature 24-hour Average 04/09/2015 : 04/09/2015 =70.2 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

______________________ ______2015.zip M-001 Temperature 24-hour Average 04/10/2015 : 04/10/2015 =70.6 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

______ __________________ ___ _____ ______ ________ 2015.z01 ipi Page 10 of 29

Locationl i %Parameter- Calculaj~l Ty ion* Sampale/Tm... lysis. Qua Oii

..Result .........

-:MDL ML! RL R:Peviie 1codesn Dat Sourc,:

M-001 Temperature 24-hour Average 04/11/12015:04/11/12015 =69.9 Degrees No CDF Analytical_

00:00:00 F Calculated_072(

________ ________________ ___________ ____ _____________2015.zip M-001 emperature 24-hour Average 04/12/2015 i0411212015 =69 Degrees No --DFAnalytical_

00:00:00 F Calculated_072(

________ ________________ ____2015 .zip M-001 Iemperature 24-hour Average 04/13/2015 04/13/2015 =70.3 Degrees No -CDFAnalytical_

00:00:00 FCalculated_072

________ ________________ ___ ____ _____________2015.zip M-001 Temperature 24-hour Average 04/14/2015 :04/14/2015 =69.9 Degrees No CDFAnalytical_

00:00:00 FCalculated 072

________ ________________ _______ ___ ____ 015.zip M-001 remperature 24-hour Average 04/15/2015 :04/15/2015 =68.9 Degrees No CDFAnalytical_

00:00:00 F alculated_072(

________ ________________ ___ ____ _____________2015.zip M-001 Temperature 24-hour Average 04/16/2015 :04/16/2015 = 69.8 Degrees No CDF Analytical_

00:00:00 F Calculated_072

________ _______________ _________ ______ _____________2015.zip M-001 remperature 24-hour Average 04/17/2015 :04/17/2015 = 70.9 Degrees No C"DFAnalytical_

00:00:00 F-Calculated_072(

________ _______________ ____________ ________ ______ _____________2015.zip M-001 temperature 24-hour Average 04/18/2015 :04/18/2015 = 70.2 Degrees No -CDFAnalytical_

00:00:00 FCalculated_072(

________ _______________ _______ ___ ____ ______ ____________20 15.zip M-001 temperature 24-hour Average 04/19/2015 : 04/19/2015 = 70.4 Degrees No CDF Analytical 00:00:00 F C*alc-ulated_072-

___________ I_____

____ ______ __ ____________ 2015 .zip M-001 Temperature 24-hour Average 04/20/2015.' 04/20/2015 = 70.7 Degrees No iCDF Analytical 00:00:00 F *Calculated_072-

___________ ____2015.zip M-001 Temperature 24-hour Average 04/21/2015 : 04/21/2015 =70.8 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

________ _______2015.zip M-001 Temperature 2*4-hour Average 0)412212015 04/22/2015 = 71.3 Degrees N~o CDF Analytical_

00:00:00 F Calculated_072

________ ________________ ____________ _____________2015.zip M-001 Temperature 24-hour Average 04/23/2015 : 0)4/23/2015 = 71.2 Degrees N4o CDFAnalytical 00:00:00 F Calculated_072(

________ ________________ _____ ____________20 15.zip M-001 Temperature 24-hour Average 04/24/2015 : 04/24/2015 = 70.8 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072(

_________ _______________2015.zip M-001 Temperature :24-hour Average 04/25/2015 : 04/25/2015 = 70.7 Degrees N~o CDFAnalytical 00:00:00 F Calculated_072(

________ _____________2015.zip M-001 Temperature 24-hour Average 04/26/2015 : 04/26/2015 =69.7 Degrees N1o CDF Analytical_

00:00:00 F Calculated_072(

______ _____ _____ _____________2015.zip M-001 Temperature 24-hour Average 04/27/2015 : U412712015 =69.7 Degrees* No CDF Analytical 00:00:00 F Calculated_072(

______ _____________2015.zip MV-001 Temperature 24-hour Average 04/28/2015 : 04/28/2015 =70.5 Degreesl No CDF Analytical_

00:00:00 F Calculated 072,

______ _______________2015.zip M-001 Temperature 24-hour Average 04/29/2015 : 04/29/2015 = 69.9 Degrees, No CDFAnalytical_

00:00:00 F Calculated 072,

_____________________________________ ______ _____________20 15.zip M-001 Temperature 24-hour Average 04/30/2015 : 04/30/2015 = 71.1 Degrees, No CDFAnalytical_

00:00:00 F Calculated_072C

_____________ ______ ____ ____ ___ _____ _______________ 2015.201zii Page 11 of 29

Locatio Calcu~tlon ~.

Paramter Smple Anlysis ual Reslt Unis MDL LmmRLnRview Q:CommenstaDat uSourc M-001 Temperature 24-hour Average 05/01/2015 :05/01/2015 = 73.1 Degrees %1o CDFAnalytical_

00:00:00 F Calculated_072(

____ ____ ______________2015 .zip M-001 Temperature 24-hour Average 05/02/2015 05/02/2015 = 72 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

_____ _____2015 .zip M-001 Temperature 24-hour Average 05/03/2015 : 05/03/2015 = 71.9 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

_____ 2015 .zip M-001 Temperature 24-hour Average 05/04/2015 : 1)5/04/2015 =71.6 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

______ 20 15.zip M-001 remperature 24-hour Average 05/05/2015 : 1)5/05/2015 = 71.1 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

________ _________________2015 ,zip M-001 remperature 24-hour Average 05/06/2015 : 05/06/2015 = 70.2 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

________ ________________ ____ _____________2015 .zip M-001 Temperature 24-hour Average 05/07/2015 : 1)5/07/2015 = 70.3 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

________ _______2015

________________ .zip M-001 remperature 24-hour Average 05/08/2015 : 1)5/08/2015 = 71.4 Degrees N1o CDFAnalytical_

00:00:00 F Calculated 072(

________ _________________2015 .zip M-001 Temperature 24-hour Average 05/09/2015 : 1)5/09/2015 = 71.3 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

________ ________________ _____ _____________20 15.zip M-001 Temperature 24-hour Average 05/10/2015 : 05/10/2015 = 69.8 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

________ _________________2015 .zip M-001 Temperature '24-hour Average 05/11/2015 : 05/11/2015 -- 69.2 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

________ ______ ______________2015 .zip M-001 Temperature 24-hour Average 05/12/2015 : 1)5/12/2015 = 69.1 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

_____2015 .zip M-001 Temperature 24-hour Average 05/13/2015 : u5/1312015 = 69 Degreesl No CDFAnalytical_

00:00:00 F Calculated_072C

________ ________________ ______2015 ____________ .zip M-001 Temperature 24-hour Average 05/14/2015 : 05/14/2015 =70.3 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

______ _____________20 15.zip M-001 Temperature 24-hour Average 05/15/2015 : 05/15/2015 =71.1 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072*

_________ _____20 15 .zip M-001 Temperature 24-hour Average 05/16/2015 : 1)5/16/2015 =70.5 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

________ ___________ _____ ______ _____ ________________________ _________ 015.ip 20__ 5 M-001 Temperature 24-hour Average 05/17/2015 : 05/17/2015 =70.3 Degrees* No CDFAnalytical_

00:00:00 F Calculated 072C

______________2015.zip M-001 Temperature 24-hour Average 05/18/2015 : 1)5/18/2015 70.6 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

______________ ______________2015 .zip M-001 Temperature 24-hour Average 05/19/2015 : 1)5/19/2015 =70.1 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

2015 .zip M-001 Temperature 24-hour Average 05/20/2015 : 1)5/20/2015 =70.3 Degrees NIo CDFAnalytical_

00:00:00 F Calculated_072(

___________ _________ _________ 2015.015zzi Page 12 of 29

Location :i,*Parameter":i'%

C alculation iSample !!*!Analysis: Q:ual : Result: !Units! MDL: :ML

RL :':Review: ComntData

Source:

M-001 Temperature 24-hour Average 05/21/2015 :05/21/2015 = 71 Degrees No CDFAnalytical_

00:00:00 F Calculated_072[

________________ _______ ________ ______ _____________2015 .zip M-001 Temperature 24-hour Average 05/22/2015 : 0)5/22/2015 = 71.1 Degrees No CDFAnalytical_

00:00:00 F Calculated_072[

____ __ __ ________ 2015 .zip M-001 Temperature 24-hour Average 05/23/2015 :05/23/2015 = 70.6 Degrees No CDF Analytical_

00:00:00 F Calculated_072C

________ ________________ ___________ ____ _____________2015 .zip M-001 Temperature 24-hour Average 05/24/2015 : 05/24/2015 = 69.7 Degrees No CDFAnalytical_

00:00:00 F Calculated_072

________ ______________________ ____ _____________2015 .zip M-001 Temperature 24-hour Average 05125/2015 : 05/25/2015 = 69.7 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

________ ________________ _______ ___ ______ ____ _____________2015 .zip M-001 Temperature 24-hour Average 05126/2015 : 05/26/2015 = 70.2 Degrees N1o CDF Analytical_

00:00:00 F Calculated_072C

___________ ____2015 .zip M-001 Temperature 2*4-hour Average 05/27/2015 :05/27/2015 = 70.1 Degrees NIo CDF Analytical 00:00:00 F Calculated_072C

_______ _____2015 .zip M-001 Temperature 24-hour Average 05/28/2015 : 05/28/2015 = 70.1 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072C

___________ ____2015 .zio M-001 Temperature 24-hour Average 05/29/2015 : 05/29/2015 = 69.8 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

_______ ____2015 .zip M-001 Temperature 24-hour Average 05/30/2015 : 05/30/2015 =70.7 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

________ ________________ _______ ____ ____2015 .zip M-001 Temperature 24-hour Average 05/31/2015 : 05/31/2015 = 71.1 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072(

________ ____________________________ _____________2015 .zip M-001 Temperature 24-hour Average 06/01/2015 : 06/01/2015 = 71.7 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072*

________ ________________ _______ ______ ____ ____ ____________20 15 .zip M-001 Temperature 24-hour Average 06/02/2015 : 06/02/2015 =71.3 Degrees N1o CDF Analytical_

00:00:00 F Calculated_072C

________ ____________________________ _____________20 15.zip M-001 Temperature 24-hour Average 06/03/2015 : 06/03/2015 = 70.5 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072C

_________________ _____________2015 .zip M-001 Temperature 24-hour Average 06/04/2015 : 06/04/2015 = 70.2 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

_________________ __________ _____ ____________20 15 .zip Mi-00 Temperature 24-hour Average 06/05/2015 : 06/05/2015 = 71.1 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

_________ ______________________________ _____ ________ __________ 015zip 20__5 M-001 Temperature 24-hour Average 06/06/2015 : 06/06/2015 = 72.2 Degrees N1o CDF Analytical_

00:00:00 F Calculated 072C

________ ________________ _____________2015 .zip M-001 Temperature 2*4-hour Average 06/07/2015 : 06/07/2015 = 71.7 Degrees N1o CDFAnalytical 00:00:00 F Calculated_072C

________ ________________ ____ _____________2015 .zip M-001 Temperature 24-hour Average 06/08/2015 : 06/08/2015 = 71.6 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

________ ________________ _________ _____________2015 .zip i-001 Temperature 24-hour Average 06/09/2015 : 06/09/2015 -= 72.3 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

_______________ ___________ _____ ______ _____ ___ ____ ____ ______ ____ ________ 2015.201z.z Page 13 of 29

Location; 2*:'i S~Parameter

::., :-:::I i::;:. :: Calculatlon? :Sample, 'Analysis*

Type ;, ,:IDate/Time Qual' Da....Priri.y.C Riesult

...... :*Units! MDL :ML: ;*RL,, ;Review i*QT, des.. C!**,!omments,;*i .Data Source Ml-001 Temperature 24-hour Average 06/10/2015 06/10/2015 =72.2 Degrees No CDF Analytical_

00:00:00 F Calculated_0721

________ ________________ ______ ___________ ______2015.zip vM-001 femperature 24-hour Average 06/11/2015 06/11/2015 71.8 Degrees No CDFAnalytical_

00:00:00 F Calculated_0721

________ _______ ____2015_____ .zip vM-001 Temperature 24-hour Average 06/12/2015 :06/12/2015 = 71.8 Degrees No CDFAnalytical_

00:00:00 F Calculated_0721

_________________2015.zip vM-001 lemperature 24-hour Average 06/13/2015 :06/13/2015 =72.3 Degrees No CDF Analytical_

00:00:00 F Calculated_0721

________2015.zip vM-001 Temperature 24-hour Average 0}6/14/2015 :06/14/2015 = 72.7 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

_________ _______2015 .zip vN-001 lemperature 24-hour Average 06/15/2015 :06/15/2015 = 71.5 Degrees No CDFAnalytical_

030:00:00 F Calculated_0721

________ _______2015.zip vM-001 Temperature 24-hour Average 036/16/2015 :06/16/2015 =71.2 Degrees No CDFAnalytical 030:00:00 F Calculated_072(

________2015.zip vM-001 1emperature 24-hour Average 06/17/2015 :06/17/2015 =71.7 Degrees No ODFAnalytical_

00:00:00 F Calculated_072

_______ _____________2015 .zip vM-001 Temperature 24-hour Average 06/18/2015 :06/18/2015 =72.4 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

____20 15.zip vI-001 Temperature 24-hour Average 036/19/2015 :06/19/2015 = 71.2 Degrees No CDFAnalytical 00:00:00 F Calculated_072[

________ ______2015.zip M-001 Temperature 24-hour Average 036/20/2015 :06/20/2015 =70.1 Degrees No CDFAnalytical_

0)0:00:00 F Calculated_072

_________ ___________ _____ _____ ____ _______________2015 .zip M-001 temperature 24-hour Average 0)6/21/2015 :06/21/2015 = 70.5 Degrees No UDFAnalytical_

00:00:00 F Calculated_072

________ _______________ ____ ___________ 2015.zip M-001 remperature 24-hour Average 06/22/2015 :06/22/2015 *= 70.2 Degrees No CDF Analytical 00:00:00 F alc-ulated_072]

________ _____________________ ______ _____________2015.zip M-001 temperature 24-hour Average 0)6/23/2015 :06/23/2015 = 70.1 D)egrees No CDF Analytical_

00:00:00 F alculated 072

_______ ____ ____ ______2.015.zip M-001 remperature 24-hour Average 0)6/24/2015 :06/24/2015 =70.4 D)egrees No -CDFAnalytical_

00:00:00 FCalculated_072(

_______ _____________2.015.zip M-001 temperature 24-hour Average 06/25/2015 : 06/25/2015 =71 D)egrees No CDFAnalytical_

00:00:00 F alculated_072(

2015.zip M-001 lemperature 24-hour Average 06/26/2015 : 06/26/2015 =72.5 !Degrees N1o CDrAnalytical_

00:00:00 F- Calculated_072

____ ____ _____________2015.zip M-001 temperature 24-hour Average 06/27/2015 :06/27/2015 = 72.8 :Degrees No CDF Analytical 00:00:00 :IF Calculated 072*

_______ _____________20 15 zip M-001 remperature 24-hour Average 06/28/2015 : 06/28/2015 = 72 Degrees Nlo "CDFAnalytical_

00:00:00 F Calculated_072{

____ ______________ 015.zip M-001 remperature 24-hour Average 06/29/2015 : 06/29/2015 = 71.1 Degrees N!o ICDF Analytical_

00:00:00 F Calculated_072{

________ _______ _____ ______ _____ ___ _____ ______ _________ zi 2015.0zi Page 14 of 29

iLocation :':*Parameter;!,*: : Cal!culation * :!,:sample*:; Analysis, !iQual*i Result: Unts MDL* 7:MF::: RL Rev'iew ~ Cm et aaSuc i-001 Temperature 24-hour Average 06/30/2015 :06/30/2015 = 72.1 IDegrees No CDF Analytical 00:00:00 !F Calculated_072-

_________ i_______________________ ________ 2015.zip M-001 Temperature D)aily Maximum 0000004/30/2015 :04/30/2015 = 71.3 DegreesF No :aCuae_7{DF-Analytical M-001 Temperature D)aily Maximum 05/31/2015 : 05/31/2015 = 73.1 Degrees No CDFAnalytical_

00:00:00 IF *Calculated_072

________ ________________ ___________ ____ ______20 15.zip i-001 Temperature Daily Maximum 06/30/2015 : 06/30/2015 =72.8 Degrees No CDFAnalytical 00:00:00 F Calculated_072(

________ ________________ ___________ ____ ______2015.zip M-001 Temperature Delta from 04/01/2015 : 04/01/2015 =18.7 Degrees Nlo CDFAnalytical_

.Background 00:00:00 F Calculated_072

________ _________________2015.zip M-001 Temperature Delta from 04/02/2015 : 04/02/2015 =18.7 Degrees N1o CDFAnalytical_

Background 00:00:00 F Calculated_072

_______ ___________________________2015.zip M-001 Temperature Delta from 04/03/2015 : 04/03/2015 =18.7 Degrees N1o CDFAnalytical_

Background 00:00:00 F Calculated_072(

___________ _____2015.zip M-001 Temperature Delta from 04/04/2015 : u410412015 =18.7 Degrees N1o CDFAnalytical_

Background 00:00:00 F Calculated_072

______ _____________2015.zip M-001 remperature Delta from 04/05/2015 : 034/05/2015 =18.7 Degrees, No CDFAnalytical_

Background 00:00:00 F Calculated_072,

_______20 ___________ 15.zip M-001 Temperature Delta from 04/06/2015 : 04/06/2015 = 18.7 Degrees N1o CDF Analytical Background 00:00:00 F Calc-ulated_072T

______________ _____________2015 .zip M-001 Temperature Delta from 04/07/2015 : u410712015 = 18.7 Degrees :No CDFAnalytical Background 00:00:00 F Calculated_072C

______________ ______2015 .zip M-001 Temperature Delta from 04/08/2015 : 04/08/2015 =18.8 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_072C

______________ ______2015 .zip M-001 Temperature Delta from 04/09/2015 : 04/09/2015 = 18.9 Degrees No CDF Analytical Background 00:00:00 F Calc-ulated_072-

_______ ______ _____2015.zip M-001 Temperature Delta from 04/10/2015 : 04/10/2015 =18.8 Degrees No CDFAnalytical Background 00:00:00 F Calculated_072C

_____ _____________20 15.zip M-001 Temperature Delta from 04/11/2015 : 04/11/12015 = 18.6 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_072C

_____ ______________2015 .zip M-001 Temperature Delta from 04/12/2015 : :04/12/2015 = 18.7 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_072C

_________ ________________ ______________________________________________________ _____ ______ _____ _________ 2015.015zip M-001 Temperature Delta from 04/13/2015 : 04/13/2015 = 18.7 Degrees No CDF Analytical Background 00:00:00 F Calc-ulated_072-

______________2015.zip Mv-001 Temperature Delta from 04/14/2015 : 04/14/2015 = 18.8 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_0721

________________________ ______ _____________2015.zip M-001 Temperature Delta from 04/15/2015 : 04/15/2015 = 18.7 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated 072C

_______________ ____________ ______ _________ 2015.z01ipi M1-001 Temperature Delta from 04/16/2015 : 04/16/2015 =18.6 Degrees No CDF Analytical Background 00:00:00 F Calculated_072C

_______ _____ _______ ____ ____ _________ __________________ 2015.0ziozi Page 15 of 29

M-0O1 Temperature Delta from 04/17/2015 :,04/17/2015 = 18.7 D:egrees No CDF Analytical_

Background 00:00:00 F alculated_072(

________ ___________________________ _____________2015.zip M-001 Temperature Delta from 04/18/2015 :04/18/2015 = 18.8 Degrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ ________________ ____ ___ _____ ______2015.zip M-001 Temperature Delta from 04/19/2015 : 04/19/2015 =18.8 Degrees No CDFAnalytical_

Background 00:00:00 F alculated_072

________ ________________ ____ ____2015.zip M-001 temperature Delta from 04/20/2015 : 04/20/2015 = 18.8 Degrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ ____ ___ _____ ______2015 .zip M-001 lemperature Delta from 04/21/2015 : 04/21/2015 = 18.8 :Degrees No CDF Analytical_

Background 00:00:00 F alculated_072(

_________ ____ ____________________2015.zip M-001 jemperature Delta from 04/22/2015 : 04/22/2015 = 19.1 :Degrees No UDFAnalytical_

Background 00:00:00 F alculated_072(

________ _______________ ________ ______ _____________2015 .zip M-001 lemperature :Delta from 04/23/2015 : 04/23/2015 = 18.7 :Degrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ _______________ ________ ______ _____________20 15.zip M-001 Femperature Delta from 04/24/2015 : 04/24/2015 = 18.8 :Degrees No UDFAnalytical_

Background 00:00:00 F alculated_072(

___________ _______________ _____________20O15.zip M-001 temperature Delta from 04/25/2015 : 04/25/2015 = 18.8 :Degrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ _______________ _______ __________ ____ ______2015.zip M-001 Femperature Delta from 04/26/2015 .04/26/2015 = 18.8 Degrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ ___________ ____ ______2015.zip M-001 Femperature Delta from 04/27/2015 : 04/27/2015 = 18.7 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_072(

_______ ______________2015.zip M-001 Femperature Delta from 04/28/2015 : 04/28/2015 = 18.8 iDegrees No CDF Analytical_

Background 00:00:00IF Calculated_072(

________ _______________ ______ ___ ____ ______2015.zip M-001 iemperature :Delta from 04/29/2015 : 04/29/2015 = 18.7 IDegrees No CDFAnalytical_

Background 00:00:00 iF Calculated_072(

________________ ____ ______ 015,zip M-001 remperature Delta from 04/30/2015 : 04/30/2015 = 18.8 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ _______________ ______ ____ ________ _____________2015.zip M-001 Femperature Delta from 05/01/2015 : 05/01/2015 = 19 iDegrees N1o UDFAnalytical Background 00:00:00 F Calculated_072(

________ _______________ ________ _____________ 015.zip M-001 Femperature Delta from 05/02/2015 :: 05/02/2015 = 19 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

____________________ ______________ 01__5.zipi M-001 Femperature Delta from 05/03/2015 :i 05/03/2015 = 19 Degrees NIo CDFAnalytical Background 00:00:00 1 F Calculated_072(

______ ____________________ _____________2015,zip M-001 Femperature Delta from 05/04/2015 : 05/04/2015 = 18.9 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ _______________________ ____ ______ 015.zip M-001 ernperature Delta from 05/05/2015 : 05/05/2015 = 18.8 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ _______________ ____________ ___ ____ ______2015.zip M-001 Femperature D)elta from 05/06/2015 : 05/06/2015 = 18.6 Degrees No CDFAnalytical_

Background 00:00:00 :iF Calculated_072(

___________ _____ ______ ____ ____ _________ ______ ______________ 015.z01izi Page 16 of 29

SLocation Parmeer Calculationi; !Sample*! *AnaiYSiS' :Qual :Result :Units* vD 1M17: RL Review *Q i;?iComments : Data SoUrce M-001 Temperature Delta from u)5/07/2015 :05/07/2015 = 18.7 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_072C

_______ _______ ______2015 .zip M-001 Temperature Delta from u)5/08/2015 05/08/2015 =18.6 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0721

_________________2015.zip M-001 Temperature Delta from 05/09/2015 : 05/09/2015 18.9 Degrees No CDFAnalytical Background 00:00:00 F Calculated_072C

_________ _______2015.zip Ml-001 Temperature Delta from 05/10/2015 : 05/10/2015 =18.9 Degrees No CDFAnalytical Background 00O:00:00 F Calculated_072C

_________2015.zip Ml-001 Temperature Delta from 0)5/11/2015 : 05/11/12015 =18.7 Degrees No CDF Analytical_

Background 0)0:00:00 F Calculated_0721

______________________2015.zip Ml-001 Temperature Delta from 0)5/12/2015 : 05/12/2015 =18.8 Degrees No CDFAnalytical_.

Background 0)0:00:00 F Calculated_072C

________ ____________2015.zip M1-001 Temperature Delta from D5/13/2015 : 05/13/2015 =18.7 ;Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

________ _______ _____2015.zip Ml-001 Temperature Delta from D)5/14/2015 : 05/14/2015 =18.7 Degrees No CDF Analytical_

Background 0*0:00:00 F Calculated_072{

________ _______2015.zip Ml-001 Temperature Delta from D)5/15/2015 : 05/15/2015 18.9 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

________ ____________2015.zip Ml-001 Temperature Delta from 05/16/2015 . 05/16/2015 -19 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

_________ ________ ____ __________ _____ _______2015.zip M4-001 Temperature Delta from uS5/17/2015 : 05/17/2015 =19 Degrees No CDF Analytical.

Background 00:00:00 F Calculated_0720

_____ __________2015.zip Ml-001 Temperature Delta from 05/18/2015": 05/18/2015 =19.2 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated 0720 2015.zip IM-001 Temperature Delta from 05/19/2015 : 05/19/2015 18.9 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_0720

_______2015.zip MI-001 Temperature Delta from 05/20/2015 : 05/20/2015 18.9 Degrees No CDFAnalytical Background 00:00:00 F Calculated_0720

______ _____2015 .zip MI-001 Temperature Delta from 05/21/2015 : 05/21/2015 =19.1 Degrees No C.DF Analytical_

Background 00:00:00 F Calculated_0720

__________________ ____2015 .zip M*-001 Temperature Delta from 0)5/22/2015 : 05/22/2015 =18.9 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_0720

________ ___________ _____ ____2015.zip M-001 lemperature Delta from 05/23/2015 :05/23/2015 =18.8 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_0720

________ ___________ _____ ____2015.zip M-001 1emperature Delta from 05/24/2015 :05/24/2015 =18.8 D)egrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

________ __________ __________ _____________2015 zip M-001 Temperature Delta from 05/25/2015 : 05/25/2015 =18.8 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_0720

________ _________________2015.zip M-001 Femperature Delta from 0)5/26/2015 : 05/26/2015 =18.7 D)egrees No CDFAnalytical Background 0)0:00:00 F Calculated_0720

___________ _____ ______ ____ ____ _________ ______ ________2015.201zii Page 17 of 29

Lo*Ecation i , i Parameter ::*:::Calculation>ii :, Sample! *'Analysis:, *Qual,. Result*' Units: :MDL ::ML::: RL, :Review, '~iA ' :*Comments ': Data Source:

M-001 Femperature Delta from U5/27/2015 :05/27/2015 = 18.8 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_072(

_____________ _______2015 .zip M-001 1-emperature Delta from u)5/2812015 :05/28/2015 = 18.9 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated 0720

_________ ____2015 .zip Mv-001 remperature Delta from :)512912015 05/29/2015 = 18.6 Degrees No CDFAnalytical Background 00:00:00 F Calculated_0720

________2015.zip M-001 remperature Delta from u513012015 : 05/30/2015 = 18.8 Degrees No CDF Analytical-Background 00:00:00 F .Calculated_0721

_________________ ______2015 .zip M]-001 Temperature Delta from S351312015 : 05/31/2015 = 18.9 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_0720

_______2.015.zip Ml-001 Temperature Delta from 0)6/01/2015 06/01/2015 = 18.9 Degrees No CDF Analytical_

Background 00:00:00 F Calculated_0720

_________________ ____ ___________2.015.zip Ml-001 Temperature Delta from 06/02/2015 : 06/02/2015 = 18.9 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ ______2015 .zip Ml-001 Temperature Delta from 06/03/2015 : 06/03/2015 = 18.9 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated 072(

___________20 15 .zip Ml-001 Temperature Delta from 0)6/04/2015 : 06/04/2015: = 18.9 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

______ ___ _____ ______2015 .zip Ml-001 Temperature Delta from 0)6/05/2015:.06/05/2015 - 18.8 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

________ ________________ _________________2015 .zip M-001 Temperature Delta from 06/06/2015 : 06/06/2015 = 19 Degrees No CDFAnalytical_

Background 0)0:00:00 F Calculated_0720

________ ______ ____2015 .zip

M-001 temperature Delta from 06/07/2015 : 06/07/2015 = 19.1 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_0720

________ ___________ _____ ____2015 zip M-001 remperature Delta from 0)6/08/2015 : 06/08/2015 = 19.1 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated_0726

__________________ ____20 15 .zip M-001 femperature Delta from 06/09/2015 : 06/09/2015 =19 Degrees No CDFAnalytical_

Background 00:00:00 F Calculated 0720

__________________ ____20 15 .zip M-001 Temperature Delta from 06/10/2015 : 06/10/2015 = 18.9 Degrees No CDFAnalytical_

Background 00:00:00 F alculated_0720

________ _________________ ___ ____ ____ _______ _____________20 15 .zip M~-001 Temperature Delta from 06/11/2015 : 06/11/2015 = 19 Degrees No CDFAnalytical_

Background 0)0:00:00 F alculated_0720

________ ____ _____________ _____________20 15 .zip M-001 temperature Delta from !06/12/2015 : 06/12/2015 = 19.1 Degrees No ODFAnalytical_

Background !00:00:00 F alculated 0720

________ _______________ ____ ____2015.zip Mv-001 Femperature Delta from 06/13/2015 : 06/13/2015 = 19 Degrees No CDF Analytical Background 00:00:00 F alculated_072*

________ _______________________ ____ ____2015 .zip Mv-001 Temperature Delta from 06/14/2015 :06/14/2015 = 19.1 Degrees No CDFAnalytical_

Background 00:00:00 FCalculated_072(

__________20 15 .zip M-001 -emperature Delta from !06/15/2015 :06/15/2015 = 19.1 Degrees No CDFAnalytical Background *00:00:00 F alculated_0720

___________ _____ ______ ____ ____ _________ ______ __________ 015.015zzp Page 18 of 29

L~ocation: ,***,Parameter:** , :,Calculation ,::Sample,*. *Analysis :Qual Result* ,Units :MDL : ML, ':::Rl. Reviewi Q A* C;;iomments*, *!:*Data Source*

M-001 Temperature Delta from 06/16/2015 :06/16/2015 = 19 Degrees No CDFAnalytical_

B~ackground 00:00:00 F alculated_072(

______ ______ _________ 015 .zip M-001 emperature Delta from 06117/2015 :06/17/2015 = 18.9 D)egrees No CDPAnalytical_

Background 00:00:00 F alculated_072

________________ ____ ___015.zip M-001 Temperature D)elta from 06/18/2015 : 06/18/2015 = 19 D)egrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ ____________________ ____ 0 15.zip M-001 Temperature D)elta from 06/19/2015 :06/19/2015 = 19 D)egrees No CDFAnalytical Background 00:00:00 F alculated_072(

________ _______________ ________ _____________ 015.zip M-001 temperature D)elta from 06/20/2015 : 06/20/2015 = 19.1 D)egrees No CDFAnalytical_

Background 00:00:00 F alculated_072{

________ ________________ ___ _________________ ___ 0 15.zip M-001 temperature D)elta from 06/21/2015 :06/21/2015 = 18.8 D)egrees No CDFAnalytical_

Background 00:00:00 F alculated_072(

________ _______________ ______ _____________2015 .zip M-001 temperature D)elta from 06/22/2015 : 06/22/2015 = 19 D)egrees No CDF Analytical_

Background 00:00:00 F alculated_072

________ _______________ ____ ___ ______ _____________ 015.zip M-001 temperature D)elta from 06/23/2015 : 06/23/2015 = 19 Degrees No CDF Analytical_

Background 00:00:00 F Calculated 072(

________ _______________ _______ ___ ____ ______ _____________2015.zip M-001 temperature D)elta from 06/24/2015 : 106/24/2015 =19 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ _______________ _______ ___ ____ _____________2015.zip M-001 iemperature D)elta from 06/25/2015 : 06/25/2015 = 18.9 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

_________ _________________________ ____ _______________2015.zip M-001 remperature D)elta from 06/26/2015 : 06/26/2015 = 18.9 Degrees N*o CDF Analytical_

Background 00:00:00 F Calculated_072(

________ _______________ _______ ____ _____ _____________2015.zip M-001 temperature Delta from 06/27/2015 : 06/27/2015 = 19 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ _______________ _______ _________ ____________20 15.zip M-001 qemperature D)elta from 06/28/2015 : 036/28/2015 = 19.1 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ ________________ _____ _____________20 15.zip MI-001 Temperature D)elta from 06/29/2015 : 0:6/29/2015 = 19 Degrees Nlo CDFAnalytical_

Background 00:00:00 F Calculated_072(

_________________20 15.zip M-001 Temperature D)elta from 06/30/2015 : 0:6/30/2015 = 19.1 Degrees N~o CDFAnalytical_

Background 00:00:00 F Calculated_072(

________ ________________ ____________2015 .zip MI-001 Temperature Monthly Average 04/30/2015 : 04/30/2015 = 70.1 Degrees N1o CDFAnalytical_

of Daily Averages 00:00:00 F Calculated 072C

________ ________ ______20 15 zip M-001 remperature Monthly Average 05/31/2015 : 05/31/2015 = 70.6 Degrees Nlo CDFAnalytical_

of Daily Averages 00:00:00 F Calculated_072C

________2015,zip M-001 remperature Monthly Average 06/30/2015 : 06/30/2015 = 71.5 Degrees: No CDFAnalytical_

of Daily Averages 00:00:00 F Calculated 072(

2015 .zip M-001D Cadmium, Total 90-Day Mean 0411512015 : 06/11/12015 = 0.52 ug/L N~o See Attachment 2, CDFAnalytical_

00:00:00 Contract Lab Report Calculated_072

______________ ____ ____20 15.zip M-001D Chromium (Total) 90-Day Mean 04/15/2015 : 06/11/12015 DNQ 1.8 ug/L 1 2 o See Attachment 2, CDFAnalytical_

00:00:00 Contract Lab Report Calculated_072,

___________ _________ ______ _________ 2015.015zip Page 19 of 29

Lrocation :.:'i:iiParameter *i~,i *Calculation: Samplell Analysis, *Qual ::;Result *units: MDL ?ML *RL *'Review, :Q :**Comments

Data Sour:e*

M-001D Copper, Totai g0-Day Mean 04/15/2015 0 C6/11/2015 =8.5 ug/L No See Attachment 2, CDFAnalytical 00:00:00 Contract Lab Report Calculated_072(

________ ___________ ___ ______ _____________2015 .zip M-001D Lead, Total 90-Day Mean 04/15/2015 0

6/11/2015 =1.3 ug/L No See Attachment 2, CDFAnalytical 00:00:00 Contract Lab Report Calculated_072(

_____________ _______2015 .zio M-001D Mercury, Total 90-Day Mean 04/15/2015 06/11/2015 ND ug/L .08 Nlo See Attachment 2, CDFAnalytical_

00:00:00 Contract Lab Report Calculated 072C 2015 .zip M-O01D Nickel, Total 90-Day Mean 04/15/2015 : 0)6/11/2015 =2.7 ug/L No See Attachment 2, CDF Analytical_

00:00:00 Contract Lab Report Calculated_072(

_____________2015 .zip M-O01D Oil and Grease 30-Day Average 04/15/2015 : 0)4/30/2015 < 5 mg/L N1o Monthly avg result. CDFAnalytical_

00:00:00 See Attachment 1, Calculated_072(

____ab 5 2015.zip M-001D Silver, Total 90-Day Mean 04/15/2015 : 0)6/11/2015 ND ug/L .11o See Attachment 2, COFAnalytical 00:00:00 Contract Lab Report Calculated_072C

______________ ___________________2015 .zio M-001D Total Suspended Solids 30-Day Average 04/15/2015 : u)4/30/2015 < 5 mg/L N1o Monthly avg result. CDFAnalytical (TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_072C

____ab 5 T_____ 2015.zip M-001D rotal Suspended Solids 30-Day Average 05/14/2015 : u5126/2015 < 5 mg/L No Monthly avg result. COFAnalytical (TSS) of Daily Averages 00:00:00 See Attachment 1. Calculated_072C

____ _____________ ___ab 6 2015 .zip M-001D Total Suspended Solids 30-Day Average 06/03/2015 : u6/25/2015 < 5 mg/L No Monthly avg result. CDF Analytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_072,

______ ____ab 7 2015.zip M-001D Zinc, Total 90-Day Mean 0411512015 : 06/11/2015 = 310 ug/L Nlo See Attachment 2, CDFAnalytical 00:00:00 Contract Lab Report Calculated_072C

_______________ _____2015 .zip M-001F Cadmium, Total 7-Day Average 04/10/2015 : u411712015 ND ug/L 5 Nlo CDFAnalytical_

(Mean) 00:00:00 Calculated_072C

________________ ____________ ___________ _____2015 .zip M-001F Chromium (Total) 1-Day Average 04/10/2015 : u411712015 ND ug/L 5 No CDFAnalytical_

(Mean) 00:00:00 Calculated_072*

_______ ______ _____2015 .zio M-001F Copper, Total 1-Day Average 04/10/2015 : 0)4/17/2015 DNQ 9.2 ug/L 5 10 No CDFAnalytical (Mean) 00:00:00 Calculated_072C

________ _____________2015.zip M-OO1F Lead, Total 7-Day Average 04/10/2015 : 04/17/2015 = 16.3 ug/L No CDFAnalytical_

(Mean) 00:00:00 Calculated_072C

________ _____________2015 .zip M-001F Mercury, Total 7-Day Average 04/10/2015 : 04/17/2015 ND ug/L .08 No See Attachment 2, CDFAnalytical (Mean) 00:00:00 Contract Lab Report Calculated_0721

________ _____________2015 .zip M-001F Nickel, Total 7-Day Average 04/10/2015 : 04/17/2015 ND ug/L 5 No CDFAnalytical_

(Mean) 00:00:00 Calculated_0721

______ _______ _____________ __________ 2015.zip.zi M-001F Silver, Total 7-Day Average 04/10/2015 : 0)4/17/2015 ND ug/L 5 -No CDFAnalytical_

(Mean) 00:00:00 Calculated 072C

______________ _____ _____ _____________2015.zip M-001F Total Suspended Solids 30-Day Average 05/04/2015 0 5/04/2015 DNQ* 2 mg/L 2 5 No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 12:45:00 See Attachment 1, Calculated_072C

_____________ __________ ____ab 12 2015.zip M-O01F Total Suspended Solids 30-Day Average 06/01/2015 : 06/01/2015 DNO 2 mg/L 2 5 No Monthly avg result. COFAnalytical_

(TSS) of Daily Averages 07:20:00 See Attachment 1, Calculated_072C

_______ ______________ _____ _____ ____ __________ab 13 2015.zip M-001F rotal Suspended Solids 30-Day Average 04/02/2015 : :)4/02/2015 ND mg/L 2 No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 07:10:00 See Attachment 1, Calculated_072C

___________ _________ ___Tab_____1__20ab11.z15zi Page 20 of 29

L~ocation .: *:Parameteri :,,* CalculatiOn Sample: iiAnalysis~ Quali *Resultl Units MI~DL: I:L:I:*RL :Review :*QI *Comments : Data Source; M-001F Zinc, Total 7-Day Average 04/10/2015 : 0411712015 = 15.3 ug/L No CDF Analytical_

(,Mean) 00:00:00 Calculated_072(

____________ ______ ______________2015 .zip M-001H Cadmium, Total YO0-Day Mean 04/06/2015 :06/08/2015 ND ug/L 5 No Avg of qtrly C2DFAnalytical QO:00:00 composites. See Att Calculated_072(

_________ ________ 1, Tab 1 i2015.zip M-001H Chromium (Total) 9)0-Day Mean 04/06/2015 :06/08/2015 = 10 ug/L No Avg of qtrly !CDFAnalytical 00:00:00 composites. See Att *Calculated_072*

_____ ______ _____ 1, Tab 1 2015.zip M-001H Copper, Total 9)0-Day Mean 04/06/2015 : 06/08/2015 = 23 ug/L No Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att C3alculated 072(

________ ____ 1, Tab 1 2015.zip M-OO1H Lead, Total 9)0-Day Mean 04/06/2015 :0C6/08/2015 = 17 ug/L No Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072C

_____ ____ _1., Tab 1 2015.zip M-O01H Mercury, Total 9)0-Day Mean 04/06/2015 :06/08/2015 ND ug/L .08 Nlo See Attachment 2, CDFAnalytical_

00:00:00 Contract Lab Report Calculated_072{

_________ _________________________ ____ ____________ _______________2015 .zip M-001H Nickel, Total 9)0-Day Mean 0J410612015 : 06/08/2015 < 10 ug/L Nlo Avg of qtrly CDFAnalytical 00:00:00 composites. See Att Calculated_072{

______________________ _____I , Tab 1 2015.zip M-001H Oil and Grease Mlonthly Average 04/01/2015 :04/02/2015 ND mg/L 1.4 Nlo Avg result for qtrly CDFAnalytical_

(,Mean) 00:00:00 samples. See Att 1, Calculated_072C

_______ _____________ _____ ____Tab 1 2015.zip M-O01H Silver, Total 9)0-Day Mean 04/06/2015 06/08/2015 ND ug/L 5 N[o Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072{

_______ _____________ _____ ____1, Tab 1 2015.zip M-001H Total Suspended Solids 30-Day Average 04/01/2015 04/02/2015 ND mg/L 2 NJo Monthly avg result. CDFAnalytical_

I(TSS) of Daily Averages 00:00:00 See Attachment 1. Calculated_072C

_________________________Tab 11 2015.zip M-001H Total Suspended Solids 30-Day Average 05/01/2015 : 05/02/2015 ND mg/L 2 N1o Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated 072C

____________________ __Tab 12 2015.zip M-001H rotal Suspended Solids 30-Day Average 06/01/2015 : 06/02/2015 ND mg/L 2 - o Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_072C

_________________T__ab 13 2015.zip M-001H Zinc, Total 9)0-Day Mean 04/06/2015 : 06/08/2015 < 10 ug/L Nlo Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072C 1,Tab I 2015.zip M-O01L Cadmium, Total 9)0-Day Mean 04/01/2015 : 06/10/2015 ND ug/L 5 N1o Avg of qtrly CDF Analytical_

00:00:00 composites. See Att Calculated 072{

1, Tabl ? 015.zip M-O01L Chromium (Total) 90-Day Mean 04/01/2015 : 06/10/2015 ND ug/L 5 N]o Avg of qtrly CDF Analytical_

00:00:00 composites:.See Att Calculated_072{

IrTab 1 2015.zip M-001L Copper, Total I90-Day Mean 04/01/2015 : 06/10/2015 ND ug/L 5 Nlo Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072{

__________________1. Tab 1 2015.zip M-001L Lead, Total 90-Day Mean 04/01/2015 : 06/10/2015 ND ug/L 5 N]o Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072{

1,Tab 1 2015.zip M-001L Mercury, Total 90-Day Mean 04/01/2015 : 06/10/2015 ND ug/L .08 Nlo Qtrly avg- Att 1 Tab 1 CDFAnalytical_

00:00:00 & Att 2 Contract Lab Calculated_072

_______ _____________ __________ _____Report 2015.zip M-001L Nickel, Total 90-Day Mean 04/01/2015 : 0)6/10/2015 ND ug/L 5 Nlo Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072C

___________ _____ ___ ___1, Tab 1 2015.zip M-001L Oil and Grease Monthly Average 04/09/2015 : 04/09/2015 ND mg/L 1.4 Nlo Avg result for qtrly CDF Analytical_

(Mean) 00:00:00 samples. See Att 1, Calculated_072C

______ ____ _____ ___ ____ _______0__ab.zip.z Tab Page 21 of 29

M-001L Silver, Total 90-Day Mean 04/01/2015 :06/10/2015 ND ug/L 5 No Avg of qtrly CDF Analytical_

00:00:00 Composites. See Att Calculated_072C

_______________ ____ ______i, Tab 1 2015.zip Ml-001L rotal Suspended Solids 30-Day Average 04/09/2015 :04/09/2015 ND mg/L 2 -No Monthly avg result. CDFAnalytical (TSS) of Daily Averages 00:00:D0 See Attachment 1, Calculated_072C

_______ _____________ ____ab 11 2015.zip MI-OO1L Total Suspended Solids 30-Day Average 05/06/2015 : 05/06/2015 ND mg/L 2 No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_072C

__________________ ab 12 2015.zip Ml-001L Total Suspended Solids 30-Day Average 06/01/2015 : 06/01/2015 ND mg/L 2) No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated 072C

______ ___________ ____ab 13 2015.zip MI-0O1L Zinc, Total 90-Day Mean 04/01/2015 : 06/10/2015 ND ug/L S No Avg of qtrly CDFAnalytical_

00:00:00 composites. See Att Calculated_072C

_________1__ , Tab 1 2015.zip N1-O01N Oil and Grease 30-Day Average 04/01/2015 : 0)4/29/2015 DNQ 0.6 mg/L r24 5 NO Monthly avg - Att 1 CDFAnalytical_

of Daily Averages 00:00:00 Tab 8 & Att 2 Contr. Calculated_072C

_____ ___ _____ Lab Rpt. 2015.zip M-001N Oil and Grease 30-Day Average 05/06/2015 : 05/26/2015 DNQ 1 mg/L .24 5 No Monthly avg - Att 1 CDFAnalytical_

of Daily Averages 00:00:00 lab 9 & Att 2 Contr. Calculated_072C

____Lab Rot. 2015.zip M-O01N Oil and Grease 30-Day Average 06/02/2015 : 06/22/2015 DNQ 0.3 mg/L .24 - No Monthly avg - Att 1 CDFAnalytical_

of Daily Averages 00:00:00 Tab 10 & Att 2 Contr. Calculated_072C

______________ ____ _____ ____Lab Rot. 2015.zip M-O01N Settleable Solids 30-Day Average 04/01/2015 : 04/29/2015 = 0.1 ml/l No Monthly avg - Att 1 CDF Analytical_

00:00:00 Tab 8 & Att 2 Contr. Calculated_072C

_____Lab Rot. 2'015.zip M-O01N Settleable Solids 30-Day Average 05/06/2015 : 05/26/2015 DNQ 0.1 ml/L .1 .1 No Monthly avg - Att 1 CDF Analytical_

00:00:00 Tab 9 & Att 2 Contr. Calculated_072C

____Lab Rot. 2015.zip M-001N Settleable Solids 30-Day Average 06/02/2015 : 06/22/2015 .DNQ 0.1 ml/L .1 .1 No Monthly avg - Att 1 CDFAnalytical_

00:00:00 Tab 10 & Att 2 Contr. Calculated_072{

______________ _____ _____ ____ __________ ____Lab Rot. 2015.zip M-001N Total Suspended Solids 30-Day Average 04/01/2015 : ]04/29/2015 = 14 mg/L No Monthly avg - Att 1 CDF Analytical_

(TSS) of Daily Averages 00:00:00 Tab 8 & Att 2 Contr. Calculated_072C

__________Lab______________ Rot. 2015.zip Ml-001N rotal Suspended Solids 30-Day Average 05/06/2015 : 05/26/2015 = 7 mg/L No Monthly avg - Att 1 CDFAnalytical_

(TSS) of Daily Averages 00:00:00 Tab 9 & Att 2 Contr. Calculated_072C

_________________ ____Lab Rpt. 2015.zip M-001N Total Suspended Solids 30-Day Average 06/02/2015 : 106/22/2015 = 11 mg/L No Monthly avg - Att 1 CDF Analytical_

(TSS) of Daily Averages 00:00:00 Tab 10 & Att 2 Contr. Calculated_072C

_________________Lab Rpt. 2015.zip M-001P pH Daily Average 04/13/2015 : 04/13/2015 =7.6 SU No See Attachment #1, CDF Analytical (Mean) 14:42:00 Tab 11 Calculated_072C

________ ________________ ______ _____________ 2015.zip M-O01P pH Daily Average 05/05/2015 : 05/05/2015 =7.6 SU No See Attachment #1, CDFAnalytical_

(Mean) 10:45:00 Tab 12 Calculated_072C

___________________ _____________ ________ 2015.z01.zp M-O01P pH Daily Average 06/08/2015 : 06/08/2015 =7.7 50 No See Attachment #1, CDF Analytical_

(Mean) 13:24:00 Tab 13 Calculated_072[

________ ________________ _____ _____________2015 .zip M-O01P Total Suspended Solids 30-Day Average 04/13/2015 : 04/13/2015 6 mg/L No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, CalculatedO072C

______T____ab 11 2015.zip M-00TP Total Suspended Solids 30-Day Average 05/05/2015 : 05/05/2015 DNO 3 mg/L 2 5 No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_072C

______________ ____ _____ ____ab 12 2015.zip M-001P Total Suspended Solids 30-Day Average 06/08/2015 : 06/08/2015 DNQ 4 mg/L 2 5 No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_072C

___________ _________ ____Tab___13__20ab13.z15zp Page 22 of 29

,Lo'catin j:** *P~arameter :*i ::Calculation Sapl >nalysiSl *Qual ! 7~jRes;u!ti Unit*s MD ML: ,* RL : i.Review: !Q; *::*iCOmments: *Data Sourcej*

M-002 Oil and Grease Mlonthly Average 04/01/20:15 : 04/01/2015 DNQ 1.4 mng/k [.4 5 No Avg result for qrtrly CDF Analytical_

(Mean) 00:00:00 samples. See Att 1, Calculated_0720

______ ___T ___ab 1 2015 .zip M-002 pH Daily Average 04/01/2015 : 04/01/2015 = 7.8 SU No See Attachment #1, CDFAnalytical_

(Mean) 00:00:00 Tab 11 Calculated_0720

________ _____ ______ ______________2015 .zip M-002 pH Daily Average 05/07/2015 : 05/07/2015 = 7.7 5U No See Attachment #1, CDF Analytical (Mean) 00:b0:00 Tab 12 Calc-ulated_0720

________ ______________2015 .zip M-002 pH Daily Average 06/01/2015 : 06/01/2015 =7.9 5U No See Attachment #1, CDFAnalytical_

(Mean) 00:00:00 Tab 13 Calculated 0720

________ ______2015 .zip M-002 Total Suspended Solids 30-Day Average 04/01/2015 : 04/01/2015 DNQ 3 mg/L 2 5 No Monthly avg result. CDFAnalytical_

ITSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_0720

_________ ____ ____ _ Tab 11 2015.zip M-002 Total Suspended Solids 30-Day Average 05/07/2015 : 05/07/2015 DNQ) 2 mg/L 2 5 No Monthly avg result. CDFAnalytical (TSS) of Daily Averages 00:00:00 See Attachment 1, Calculated_0720

______________ T__ab12 2015.zip M-002 Total Suspended Solids 30-Day Average 0)6/01/2015 : 06/01/2015 ND mg/L 2 No 'Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 0)0:00:00 ,See Attachment 1, Calculated_0720

_______ ____ ______Tab 13 2015.zip M-003 Total Suspended Solids 30-Day Average 0)4/01/2015 : 04/01/2015 = 20 mg/L No Monthly avg result. CDFAnalytical_

(TSS) of Daily Averages 12:20:00 See Attachment 1, Calculated_072g

______ ___T___ab 11 2015.zip M-003 Total Suspended Solids 30-Day Average 0)5/05/2015 : 05/05/2015 DNQ 3 mg/L 2. 5 No Monthly avg result. CDF Analytical_

ITSS) of Daily Averages 09g:17:00 See Attachment 1, Calculated_0720

_______ ______ ____ ________ Tab 12 2.015.zip IM-003 Total Suspended Solids 30-Day Average 06/01/2015 : 06/01/2015 DNQ 4 mg/L 2 - 5 No Mlonthly avg result. CDFAnalytical (TSS) of Daily Averages 12:17:00 See Attachment 1, Calculated_072(

_____________ab 13 2015.zip M-INF Chromium (Total) 90-Day Mean 0)4/02/2015 : 06/10/2015 ND ug/L S No Q~uarterly avg result. CDFAnalytical_

0)0:00:00 See Attachment 1, Calculated 0720

_________ ____ _________ _ Tab 1. 2015.zip M-INF Copper, Total 90-Day Mean 0)4/02/2015 : 06/10/2015 DNQ 6.7 ug/L 5 10 No Quarterly avg result. CDFAnalytical_

0)0:00:00 See Attachment 1, Calculated_0720 1.

T________ab 2015.zip MI-INF Nickel, Total g0-Day Mean 04/02/2015 : 06/10/2015 ND ug/L 5 No Q*uarterly avg result. CDFAnalytical_

0)0:00:00 See Attachment 1. Calculated_072(

_____ __T______ab 1. 2015.zip M-INF lemperature 24-hour Average 0)4/01/2015 : 04/01/20151 = 51.1 Degrees .No CDFAnalytical 0:)000:00 F Calculated_0720

___________________2015.zip M-INF Temperature 24-hour Average 0)4/02/2015 :04/02/2015 = 50.2 Degrees No CDFAnalytical_

0)0:00:00 F Calculated_0720

________ ______________2015________________ .zip iM-INF Temperature 24-hour Average 0)4/03/2015 : 04/03/2015 =50.6 Degrees No CDF Analytical_

0)0:00:00 F Calculated 0720

________ ________ ________ _____ _______ _____ _____________2015 .zip M-INF Temperature 24-hour Average 0)4/04/2015 : 04/04/20151 = 50.6 Degrees No CDFAnalytical_

0)0:00:00 F Calculated_0720

__________ ______ ____2015 .zip M-INF Temperature 24-hour Average 0)4/05/2015 :04/05/2015 = 50.3 D)egrees No CDFAnalytical_

0)0:00:00 F Calculated_0720

________ ________ _____ ______ ____2015 .zip M-INF Temperature 24-hour Average u)410612015 : 04/06/2015 = 50.8 Degrees No CDFAnalytical 0)0:00:00 F Calculated_072(

_________2.015.zip

M-INF Temperature 24-hour Average 0)4/07/2015 : 04/07/2015 = 51.6 Degrees No CDFAnalytical_

0)0:00:00 F Calculated_0720

________________ ______ __________ _____________ zi 2015.z01 Page 23 of 29

fLocation' :,:Parameter: iCalculation' : Sample: Analysis ::Qual Result : Units: MDL: ::MLi RI!: Review ::QA ' *Commentsi~ ; Data Source M-INF Temperature 24-hour Average 04/08/2015 :04/08/2015 = 51.8 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

_______ _____ ______ _____________2015 .zip M-INF Temperature 24-hour Average 0)410912015 : 14/0g/2015 =51.3 'Degrees No CDF Analytical_

00:00:00 F Calculated_072(

_______ ____ _________ ______2015.zip M-INF Temperature 24-hour Average 04/10/2015 : 1411012015 = 51.8 Degrees No CDFAnalytical_

00:00:00 F Calculated 072(

________ ________________ ___________ ____ _____________2015 .zip Mv-INF Temperature 24-hour Average 04/11/12015 =i04111/2015 = 51.3 IDegrees No ICDFAnalytical_

00:00:00 ,F Calculated 072(

________ _______________________ ______ ___ ____ ______ 015.zip M-INF Temperature 24-hour Average 04/12/2015 : '04/12/2015 =50.3 :Degrees No 'CDFAnalytical_

00:00:00 iF Calculated_072(

M-INF Temperature 24-hour Average 04/13/2015 : 04/13/2015 =51.6 Deres015.zAnyica 00:00:00 F Calculated_072(

________ ________________ ___________ ____ ______2015 .zip M-INF Temperature 24-hour Average 04/14/2015 : 04/14/2015 51.1 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

___________ ____2015.zip M-INF Temperature 24-hour Average 04/15/2015 :04/15/2015 =50.2 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072(

_______ ____2015 .zip M-INF Temperature 24-hour Average 04/16/2015 : 04/16/2015 =51.2 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072

________ _______2015

________________ .zip M-INF Temperature 24-hour Average 04/17/2015 : 04/17/2015 =52.2 Degrees N1o CDF Analytical_

00:00:00 F Calculated_072(

_______ _____2015 .zip M-INF Temperature 24-hour Average 04/18/2015 : 04/18/2015 =51.4 Degrees N1o CDFAnalytical_

00:00:00 F Calculated 072

_________ _________________ ____ _____2015 .zip M-INF Temperature 24-hour Average 04/19/2015 : 04/19/2015 =51.6 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

______________________ _____________2015 .zip M-INF Temperature 24-hour Average 04/20/2015 : 04/20/2015 =51.9 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

________ _______ _____ ______ _____________2015 .zip M-INF Temperature 24-hour Average 04/21/2015 : 04/21/2015 =52 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

_____ ______________2015.zip M-INF Temperature 24-hour Average 04/22/2015 : 04/22/2015 =52.2 Degrees N1o CDFAnalytical_

00:00:00 F Calculated_072C

_________ _______ ____ _____2015 .zio M-INF Temperature 24-hour Average 04/23/2015 : 04/23/2015 =52.5 Degrees N1o CDFAnalytical_

00:00:00 F Calculated 072,

________ _______________________ _____________2015 .zip M-INF remperature 24-hour Average 04/24/2015 : 04/24/2015 =52 Degrees= No CDFAnalytical_

00:00:00 F Calculated_072,

_______________2015.zip M-INF Temperature 24-hour Average 04/25/2015 : 04/25/2015 51.9 Degrees, No CDFAnalytical_

00:00:00 F Calculated_072C

________ ______________2015 .zip M-INF Temperature 24-hour Average 04/26/2015 : :)4/26/2015 =50.9 Degrees N1o CDFAnalytical 00:00:00 F Calculated_072C

_______________20 15.zip M-INF Temperature 24-hour Average 04/27/2015 : 0)4/27/2015 =51 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072,

___________ ______ ____ ____ ___ _____ ______________2015.zi01 lzi Page 24 of 29

M-INF Temperature 24-hour Average 04/28/2015 : 04/28/2015 = 51.7!Degrees No CDFAnalytical_

00:00:00 F Calculated_0721 2

________ _____ __________ .015.zip M-INF Temperature 24-hour Average 04/29/2015 :04/29/2015 = 51.2 Degrees No CDF Analytical_

00:00:00 F Calculated_0721

________________ _________ ____2.015.zip M-INF Temperature 24-hour Average 04/30/2015 :04/30/2015 = 52.3 Degrees No CDFAnalytical_

00:00:00 F Calculated_0721

________ ________ _____20 15.zip M-INF Temperature 24-hour Average 05/01/2015 : 05/01/2015 = 54.1 Degrees No CDFAnalytical 00:00:00 F Calculated_0721 2

_______ 015.zip M-INF Temperature 24-hour Average 05/02/2015 : 0510212015 =53 Degrees No CDFAnalytical 00:00:00 F Calculated_0721

_________ ________ _____ _____ _______2015 .zip M-INF [emperature 24-hour Average 05/03/2015 : 05/03/2015 = 52.9 Degrees No CDFAnalytical 00:00:00 F Calculated_072(

________ ____ ____ ______2015 .zip M-INF Temperature 24-hour Average 05/04/2015 :05/04/2015 =52.7 Degrees No CDFAnalytical 00:00:00 F Calculated_072(

_________ _____ ____ _______2015 .zip M-INF Temperature 24-hour Average 05/05/2015 :05/05/2015 =52.3 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

________ _____ _____ ______2015.zip M-INF Temperature 24-hour Average 05/06/2015 : 05/06/2015 = 51.6 Degrees No CDFAnalytical_

00:00:00 F Calculated 072(

________ ___________ _____ ____2015 .zip M-INF Temperature 24-hour Average 05/07/2015 .05/07/2015 = 51.6 Degrees No LDFAnalytical_

00:00:00 F Calculated_072(

___________ ______2015.zip M-INF Temperature 24-hour Average 05/08/2015 :05/08/2015 = 52.8 Degrees No CDFAnalytical 00:00:00 F Calculated_072{

________ ___________ _____ ____2015 .zip M-INF Temperature 24-hour Average 0)5/09/2015 :05/09/2015 = .52.4 Degrees No CDFAnalytical 0)0:00:00 FCalculated_072(

_________________2015.zip M-INF Temperature 24-hour Average 0)5/10/2015 :05/10/2015 =50.9 Degrees No CDFAnalytical_

0)0:00:00 FCalculated_072

________ __________ _____ ____ ___ ______ _____________2015 .zip M-INF Temperature 24-hour Average 05/11/12015 :05/11/12015 = 50.5 Degrees No CDF Analytical_

0)0:00:00 FCalculated 072(

________ _______________ ____ ______ _____________2015.zip M-INF Temperature 24-hour Average 105/12/2015 : 05/12/2015 = 50.3 Degrees No CDFAnalytical_

0)0:00:00 FCalculated_072(

______ _____________2015.zip M-INF Temperature 24-hour Average 05/13/2015 :05/13/2015 = 50.3 D)egrees No CDFAnalytical_

00:00:00 FCalculated_072(

________ ___________________________________________ ________________________ 015.01zip M-INF Temperature 24-hour Average 05/14/2015 :05/14/2015 = 51.6 D)egrees No CDFAnalyticai_

00:00:00 FCalculated 072(

________ _______ ____ ___________2015 .zip M-INF Femperature 24-hour Average 05/15/2015 :05/15/2015 = 52.2 Degrees No CDF Analytical_

00:00:00 F alculated_072(

________ ____ ___________2015.zip M-INF Temperature 24-hour Average 05/16/2015 : 05/16/2015 =51.5 iDegrees No CDF Analytical_

00:00:00 IF Calculated_072(

________ _______ ___ ____ ______ _____________2015.zip M-INF Femperature 24-hour Average 05/17/2015 : 05/17/2015 =51.3 IDegrees No CDFAnalytical 00:00:00 F Calculated_072(

___________ _____ ______ ____ ____ ___ _____ ______ _________ 015.z01izi Page 25 of 29

C:ilomments,;, !Data Source*

iLocationi -=: :'Parameter '* Caicua~cltion: :,Sample:* *Analysisl :,Qual* : ResUlt. Units :MDL' *ML* 'RL :

...... cator :7A' Review vM-INF Temperature 24-hour Average 05/18/2015 : 0511812015 =51.4 Degrees No CDF Analytical_

00:00:00 F Caicuiated_072C

_______________2015 .zip Ml-INF Temperature 24-hour Average 05/19/2015 :05/19/2015 = 51.2 Degrees No CDF Analytical 030:00:00 F Calculated_072C

_________________2015.zip Ml-INF Temperature 24-hour Average 05/20/2015 :05/20/2015 =51.4 Degrees No CDFAnalytical 030:00:00 F Calculated_072C

_________________ _____2015.zip MI-INF Temperature 24-hour Average 035/21/2015 : 0)512112015 =51.9 Degrees No CDFAnalytical_

00:00:00 F Calculated_072[

_______ ____________2015.zip vM-INF Temperature 24-hour Average 05/22/2015 : 05/22/2015 = 52.2 Degrees No CDFAnalytical_

030:00:00 F Calculated_072C

_________________ ______2015.zip MI-INF Temperature 24-hour Average 035/23/2015 : 05/23/2015 = 51.8 Degrees No CDF Analytical_

030:00:00 F Calculated_072C

________________ _______ ______2015 .zip MI-INF Temperature 24-hour Average 035/24/2015 : 05/24/2015 = 50.9 Degrees No CDFAnalytical_

030:00:00 F Calculated_072C

________ ~2015 .zip MI-INF Temperature 24-hour Average 05/25/2015 : 05/25/2015 = 50.9 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C 20 15.zip MI-INF remperature 24-hour Average 05/26/2015 :05/26/2015 = 51.5 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

_________________2015.zip MI-INF Temperature 24-hour Average 05/27/2015 : 05/27/2015 = 51.3 Degrees No CDFAnalytical_

030:00:00 F Calculated_072C

______2015,zip M-INF Temperature 24-hour Average 05/28/2015 : 05/28/2015 =51.2 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

________ _______2015 .zip vM-INF Temperature 24-hour Average 05/29/2015 :05/29/2015 = 51.2 Degrees No CDFAnalytical_

00:00:00 F Calculated_0720

_________2015.zip MI-INF Temperature 24-hour Average 05/30/2015 : 05/30/2015 = 51.9 Degrees No CDFAnalytical_

030:00:00 F Calculated_0721

________ ____ ____2015 .zip MI-INF Temperature 24-hour Average 05/31/2015 : 05/31/2015 = 52.2 Degrees No CDFAnalytical_

00:00:00 F Calculated_0721

_________________ ____ _____2015.zip MI-INF ]emperature 24-hour Average 06/01/2015 : 06/01/2015 = 52.8 Degrees No CDFAnalytical 00:00:00 F Calculated_0720

__________2015,zip vM-INF Temperature 24-hour Average 06/02/2015 : 06/02/2015 = 52.4 Degrees No CDFAnalytical_

00:00:00 F Calculated_0720

_________ _____ _______ ______________2015 .zip MI-INF Temperature 24-hour Average 06/03/2015 :06/03/2015 = 51.6 Degrees No CDFAnalytical_

00:00:00 F Calculated_0720

_________________________ ____2015.zip VM-INF Temperature 24-hour Average 06/04/2015 :06/04/2015 = 51.3 Degrees No CDF Analytical 00:00:00 F Calculated_0720 2015.zip MI-INF lemperature 24-hour Average 06/05/2015 : 06/05/2015 = 52.3 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

_________________ __________________2015 .zip Vl-INF Temperature 24-hour Average 06/06/2015 : 06/06/2015 = 53.2 Degrees No CDFAnalytical_

00:00:00 F Calculated_072O

___________________ ______ ____ ____ ___ _____ ______ ________ 2015_20zizi Page 26 of 29

Location :;'*iiParameter :* Calculation* iSample'*! *Analysis: QuaIl :Result?' units; MDiEi MLiF : RI Review QA<! *i;Comments: i*Data Source M-INF Temperature 24-hour Average 06/07/2015 :06/07/2015 = 52.6 !Degrees NJo !CDF Analytical_

00:00:00 F Calculated_072

________ ________________ ______ ______ _____ ____ ______ _____________2015,zip M-INF Temperature 24-hour Average 0)6/08/2015 : 06/08/2015 = 52.5 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072(

_________________ ______ ____ ____ ______2015 .zio M-INF Temperature 24-hour Average 06/09/2015 : 06/0g/2015 = 53.3 Degrees No CDFAnalytical_

00:00:00 F Calculated 072*

_____ ____ ____2015.zip M-INF Temperature 24-hour Average 06/10/2015 : 06/10/2015 = 53.3 Degrees N4o CDFAnalytical 00:00:00 F Calculated_072[

_____2015.zip M-INF Temperature ,24-hour Average 06/11/2015 : u)6/11/2015 = 52.8 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

______2015.zip M-INF Temperature 24-hour Average 06/12/2015 : 06/12/2015 -- 52.7 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072*

________ ______ _____2015 .zip M-INF Temperature 24-hour Average 06/13/2015 : 0)6/13/2015 = 53.3 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated 072 2015.zip M-INF remperature 24-hour Average 06/14/2015 : 06/14/2015 = 53.6 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

______________2015.zip M-INF remperature 24-hour Average 06/15/2015 : 06/15/2015 = 52.4 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated 072[

________20 15.zip MI-INF remperature 24-hour Average 06/16/2015 : u6/16/2015 = 52.2 Degrees Nlo CDFAnalytical_

00:00:00 F Calculated_072[

_______________2015.zip M-INF Temperature 24-hour Average 06/17/2015 : 06/17/2015 = 52.8 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

________________ ______2015.zip M-INF Temperature 24-hour Average 06/18/2015 : 06/18/2015 = 53.4 Degrees No CDFAnalytical_

00:00:00 F Calculated_0721

_______________2015.zip M-INF Temperature 24-hour Average 06/19/2015 : 06/19/2015 = 52.2 Degrees No CDF Analytical_

00:00:00 F Calculated_072C

_______ _____20 15.zip M-INF Temperature 24-hour Average 06/20/2015 : 06/20/2015 = 51 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

_________________ _____ ______ _____20 15.zip M-INF Temperature 24-hour Average 06/21/2015 : 0)6/21/2015 = 51.7 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

________________ ____________ _____2015.zip M-INF Temperature 24-hour Average 06/22/2015 : !06/22/2015 = 51.2 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

________________________ _____ ______2 015.zip M-INF Temperature 24-hour Average 06/23/2015 : 06/23/2015 =51.1 Degrees No CDF Analytical_

00:00:00 F Calculated_072C

______________________ ______2015.zip M-INF Temperature 24-hour Average 06/24/2015 : 06/24/2015 = 51.4 Degrees No CDFAnalytical 00:00:00 F Calculated_0721

_______ ____ _______2015.zip M-INF Temperature 24-hour Average 06/25/2015 : 06/25/2015 = 52.1 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

_____2015.zip M-INF Temperature 24-hour Average 06/26/2015 : 06/26/2015 = 53.6 Degrees No CDFAnalytical_

00:00:00 F Calculated_072C

___________ ______ ____ ____ ___ _____ _______________ 2015.201zzi Page 27 of 29

'Location*; i : Parameter*:i: .Calc,,lation '"Sample: Analysis'. QOual! *Result;* *Units, :MDL* ML RL Reviewi *II:*A* !*;Comments':,* .'Data *Source M-INF [emperature 24-hour Average U6/27/2015:06/27/2015 = 53.8 Degrees No CDF Analytical_

0:0:00:00 F Calculated_072

________ ______________________ ______ _____________ 2015 .zip M-INF *emperature 24-hour Average U6128/2015 06/28/2015 = 52.9 Degrees No CDF Analytical_

00:00:00 F Calculated_072(

________ _________________ ____ ____ ______2015 .zip M-INF Femperature 24-hour Average 06/29/2015 06/29/2015 = 52.1 Degrees No CDFAnalyticaL 0)0:00:00 F Calculated_072(

________ _________________ ______2015,zip M-INF Femperature 24-hour Average 06/30/2015 : 06/30/2015 = 53 Degrees No CDFAnalytical.

00:00:00 .F Calculated_072(

________ _________________ ____ _______ _____________ 2015.zip M-INF Femperature Daily Maximum 04/30/2015 :04/30/2015 = 52.5 Degrees No CDFAnalytical_

00:00:00 F Calculated_072(

________ __________ __________ _____________ 2015.zip M-INF 1emperature Daily Maximum 0)5/31/2015 :05/31/2015 = 54.1 D)egrees No CDF Analytical_

00:00:00 F Calculated_072(

________ ___________ _____ ____ ____________ 2l5 .zip M-INF Femperature Daily Maximum 06/30/2015 : 06/30/2015 = 53.8 Degrees No CDFAnalytical_

0)0:00:00 F alculated_072(

________ _______________ ____ ____ ______ _____________ 2015 zip M-INF 1emperature Monthly Average 04/30/2015 : 04/30/2015 = 51.4 Degrees No CDFAnalytical_

of Daily Averages 0)0:00:00 F alculated_072

________ ___________ ______ _____________ 015 .zip M-INF Femperature Monthly Average 05/31/2015 :05/31/2015 = 51.7 D)egrees No CDFAnalytical_

of Daily Averages 00:00:00 F alculated_072(

________ __________________ ____ ___ ______ _____________ 015 .zip M-INF Femperature Mvonthly Average 06/30/2015 :06/30/2015 = 52.5 Degrees No CDFAnalytical_

of Daily Averages 00:00:00 F alculated_072(

___________ _____ ______ ____ ____ ____ _____ ______ _________0__ 5.z1.zp M-INF Zinc, Total 90-Day Mean 04/02/2015 : 06/10/2015 DNQ 4.3 ug/L 5 10 No Quarterly avg result. CDFAnalytical_

00:00:00 See Attachment 1, Calculated_072(

______ ______ ____ ___Tab_____.___ 0b1..zi5zl Certificate I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

I certify that I am Kenneth Cortese and am authorized to submit this report on behalf of PG&E Diablo Canyon Power Plant. I understand that I am submitting the following report(s):

-Quarterly SMR ( MONNPDES ) report for Q2 2015 (due 07/20/2015)

I understand that data submitted in this report(s) can be used by authorized agencies for water quality management related analyses and enforcement actions, if required.

I am also aware that my user ID, password, and answer to a challenge question constitute my electronic signature and any information I indicate I am electronically certifying contains my signature. I understand that my electronic signature is the legal equivalent of my handwritten signature. I certify that I have not violated any term in my Electronic Signature Agreement and that I am otherwise without any reason to believe that the confidentiality of my password and challenge question answers have been compromised now or at any time prior to this submission. I understand that this attestation of fact pertains to the implementation, oversight, and enforcement of a federal environmental program and must be true to the best of my knowledge.

Name: Kenneth Cortese Page 28 of 29

Title:

No Title Page 29 of 29

Attachment 1 -2015 2nd Qtr DCPP NPDES Worksheets.xlsm Diablo Canyon Power Piant - NPDES Data Worksheets 2nd Quarter 2015 Tab Information i GO ToTabt i 1 Quarterly Averages GoToTab IMiscellaneous Go To Tab 2 2 Circulatina Water Chlorine Residual - Anril Go To Tab23 ici~ic ~~ hlrn eija n Go ToTa 3 Circulating Water Chlorine Residual - May iGo To Tab 4 4 Circulating Water Chlorine Residual - June SGo To Tab 5 5 0010 Flow Weighted Averages For TSS and O&G - April IGo To Tab 6 6 0010 Flow Weighted Averages For TSS and O&G - May iGo To Tab 7 7 0010 Flow Weighted Averages For TSS and O&G -June SGo To Tab 8 8 001N TSS, SS and O&G -April iGo To Tab9 9 001N TSS, SS and O&G -May SGo To Tabl10 10 001N TSS, SS and O&G - June Go To Tab 11 1 Miscellaneous Duplicates - April Go To Tab 1i2 12 Miscellaneous Duplicates - May SGo To Tab 13 13 Miscellaneous Duplicates - June Navigation

Attachment 1- 2015 2nd Qtr DCPP NPDES Worksheets.xlsrn IA I B* C 0 E F G [H I I J K 1i I I I I I 2 Miscellaneous Quarterly Average Calculations For Quarterly e6MR 10 6

Parameter Results Result for Daily Numerical Reporting Average 7 Sample Dats Analysisne Lab Averaoe 8

4/21/2015. DCPP 0 0 ND(5) _______

Ini/uent 9T 5/7/2015 5/14/20156: DCPP Influent 0 10 6/9/2015 6/10/2015* DCPP Inftuent 0 13 tntuuen 6 7 - DNQ(7) ________

14 4/2/20)15 4/21/201,5I[

5/14/2015 iDCPP DCPP 7 Intluen 15 L 5/7/2015 6/10/i295 -: DCPP 7 16 17 4/2/2015 I 4/21/2016 0 0 0 ND(5) 16 6/7/2015 ,;*5/14/2015.,

16 6/9/2015 '6/1"0/2015 0 0 20 . . . . . . I.. . . . .. 0 0 21 4/21/2015 Influent Zn IDNQ(6.7) 7 7T 6/14/2015,. I DCPP 4

______ 5/7/20156 DCPP 22 ]Inhuent Znl ND(5) 0 0 C6/9/2015 6/10/2016 DCPP 6 6 Inhluent Zn DNO(5.8) 24 26 Quarterly Oil and Grease Averages 26 [5.Omg/Lis D P lab I DIL.

+/- Result for Numencal Reporting Average 26 20 Sample Date Analysis Date Lcto ILcto Unit Parameter Results Average Daily Average Quarterily Average .b for Quarter 30 4/212015 4/23/2016 IOO1H ND0(1.4) 0.0 0.0 ND(1 .4) 1 31 -____-4/1/2015 -4/23/2016 lOIH ND0(1.4) 0.0 2

33 - 4/9/2015 4/23/2015 COIL ND0(1.4) 0.0 0.0 0.0 ND(I.4) 34 4/6/2016 4/23/2015 ODIL 2

36 - 4/1/2015 4/16/2015 002 374/1/2016 4/1112015 002 1 36 36 40 SSOL CPP tab MDL

________ _________ r __________ I _________ t _________________ I ________________ I _________________

FirstDate Atiquot LastDate AliquotLoain Loaon Ut Ui Parameter Result for Numerical Reporting Average Results Averana fliartarkv Avnrrmn, far fl,,nrt 4/6/2016 6/8/2015 C001H 1 AgND(5)-------- 0' ND(5)__ _ _ __ _

-4/6/2015 C 6/6/2016 001H 2 Ag ND(S) 0 4/6/2015 : :6/8/2015 C,001H Cd ND(5)

II *~ ;6/6/2015 OQIH 0

4/6/2015 2 ]Cd ND(S)

!6/6/2015 OIN01 1 JCr 20 II , 4/6/2015:

10 2 Cr

-:, 6/6/2016 OQI01 4/6/2015

- 616/2015 :OO1H 1 2 21___ 23 23 _ _____

24

/8/2015 iOlHN 1V Ni 12 12 6 <10 4~/6/2015 ,f 6/8/201 5 "!001

___2 Ni___ DNQ(6) 031 14/612015

6/8/2016 O01N C '6/6/2015

OO01H 2 Pb 11

4/6/2015, 411/2,015

-. 6/6/2015 Q001H T IL 7 <10O ]__ _ __ _

,':6/812015 OOIH 2V 0 DNQ(7) 4.16/2015 86/10/2015 00lL T ND(5) 0

-- /1/2015 :6/10/2015: Q001L

.7 Ag2 ND(S) (~

0 4/1/2015

- 6110/2015 ,Q00L 6/B10/2015* .tolL 0 0V ND(5) 1411/2015C cd NO(5) 0 S6/10/2015 OI00L Cr ND(5) 0 0

4/1/2015 ;6/10/20"15. tOIL 2 Cr ND(5) 0

.4/1/2015 I.

4/1/2015

6/10/2015 O001L 1 Cu ND(5) oV

-V ND(5) oV 4/1/2015 C6110/2015 tOI1L 4/1/2016 6/10/2015 ",OI0L ND(5) oV 0 ND(5)

,6/10/2015 i 001L NI ND(5) j 0 _______

411/2015.

. 6/10/2015 tOI1L Pb ND(S) 0 0 ii NI 2 Pb ND(5) 0 4/1/2015 ?;,6110/20t5 tO01L 4/1/2015 1 Zn ND(5) 0V 0

, !,6/10/2015: tOIL 2___ n ND(5) ____

.6/10/2015 001L 1 gND(S) 0 _

4/1/2015 : :6/10/2015 C001L Hg ND(5)

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm A B C- 3 E F G H I J K L M N O3 P 2 ___________Chlorine for eSMR ____

3 I_____________

4 __________FILL IN ONLY SHADEDIL.OLORED CELLS 6______________ Date _____

7

41112015* 4/212015 41312015 41412015 41512015 41612015 41712015 41812015 41912015 411012015 411112015 411212015 411312015 411412015 411512015 8 UnitlTRC(ppb) _____ 19 ____ *:19 _____ 19: , "_ 16 - 21 ____ 16 ___ 25 ____ 23 ___ 2 28_ .2: 31 2: .28 29 : 28 .:23, .. 23 9 .,:,::;12 __ 19 21 ___' 19 ___ :,:;19 , 23 :i:'.,:

.: 25,, ':=;, 23, - . .25 * ., 28 '

,**281 : 28~* i:.:*232, *.>'25= ' .23 11 _______ ,..... 14 _. __ 21 ______19 _____16, '18____ 25 _____ 21 ______ 25 -., 33 *: : 25 : 268 : 28 ... :: 11

_____25 28 12 .25 /,21 ___18 ___ 21. .,,21 __ 25 __ 19 ,". ,25 28 :.. 23 ':22 28 ::=,12 _ _28 <.31 13 _ _ __ _ _ 18 __ 19 .__ 16 _ _ _ 16 _ _ _" 18 25 ;:: 25 28 ,.i 25 : 19 22 : 31 ,' , 19 _ _ _ 23 :.: 28 14 UnitlICl2 Use (Ibs) : 288 2:*;,:=882 88 288 : ..... 288 ... ,288 288 .288

., "288 : ="288 : 288 ,:':288 ' ,**288 ". 288 288 15 UniITRC:pbt' 30 30 , 33 30. 30 28 40 33 .36 ___ 403 ___!?, 36 __ 0 3. 28 __ 28 16 ,: _3:3(___

.__ 33 :,*33 " : .33 '30 33! 40 .... 33 :_ *36 ___; 40] ___ : 36 __:_ 35 : 36 ___ 30 , '°30 17 ,,° ' :28 :30 30 "30~ " 28 :28 36 ' .33 .40 ___: 36 __ 35 _ _42 " 25 ~ :.,28 28 18 .___" "33 . 30 ":*33 30 . 30 40 38>* 33., 44 "__361__ : 34 ___ 33 , 16 ____30 .30 19 : :, 36*, 33 ::33 " ;30 :' 30 . , , : 40 30 : 36* ____ 40 ___ 36 : , '34 :, : ,36 *:,:: 11 .:*"25 ': 39 20 ___ ;: 30:,*,*':::' 30} ::30 .'

28 '* ] =',28 : 40 !: '. .. 33 :: ;: ;36i ____:: "40] _:_: __:,: 30i :: ::.'28 , i 36 " :i 23

i::2' 8 : 3 0 21 Unit 2 CI2Use (Ibst *:288 , *i288 :: :288 : 288 288 2:88 2

288 88 288: :: 288 "':::.288 :::i*288 : :: 288 ,288 ::288 23 25 21 21 21 21 25 25 28 33 31 34 31 28 28 31 24 36 33 33 33 30 40 40 36 44 40 36 42 36 30* 30 25 Daily Maximum TRC (ppb) 36 33 33 33 30 40 40 36 44 40 36 42 36 30 31 26 DailyCI2Use(lbs) 576 576 576 576 576 576 576 576 576 576 576 576 576 576 576 28 29 30 r 1 F 1- 1 t +/-

35 a ___________ c ___________ .1___________ 1 ___________ L ___________ +/- ___________ £ ___________ .1___________

2

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm 0 R S T U V W X Y Z AA AB AC AD AE AF AG 1 __________ __________ __________

7 4/1612015 411712015 411812015 4/1912015 4120/2015 412112015 4122/2015 412312015 412412015 412512015 412612015 4127120,15 4/28/2015 4129/2015 4130120158 _____

8 ,,/ ,:28,,_:___ 19: ___ ,.16 __ _ 23 16 l ";19 ____: ,21 : - :* 18 =.' '21 'i,13 *: !"z18 ____:,= 18* ____18 i: ____:' 23 :

9 ___ 28 ___'* 18 .. .19 , 23 **: ,16 13 , 15 ___ 21 ., 23 ____ 19 ,; , 18 ! ;23 _ _ :115 __ _ :16 - 18 ;_ _ ___

11', , 23

-! -- ,16 :,,' 25 - ; 19 , 19 , *:= 19 : : 21 _ _ _ 21 21 _ _: :18 _ _ 16 _ _ " _ 21 , 13 ___ 19 : 10 __ _ _ _

123 215 , 13 , 23 :,15 13 " 15 "_ -16 .... 18--- 21 __ _ 16 ___ 21* __ 6_ 18.. . 16

.13 <10 : 1 13 :.*. 15E ;:2 1<:2 8 :::: .2_.__,_! 8 8 268818___2 2 8 :,"J".i'8 8 _ '::..;8

_ _ 821;:* "'28 _ _ 13 ___. __ 19, 8 _: _ __ : 288125! __* 1928 ?;!813; ... ",;"

14 288

36 88: 288, 16 '2889 288 28 *:'-'268 . 288 :" : 3 , :,288:

"i~.__8 288 288.,:!3 288 288 >2830 __ ,

16 '*33 17' 10-' :. *24 ' ... 21 : ,: '*17 '**:'*21 "-23>%.. .33 -'i:. *28 _ _ 30 : '::30 -,;30 "30 _ _*':36.

17 33 - ,23 . 27 :, 24 . 21 . 21: *.= 28 *,_ _ 2 - 33 _ _ 3 _ _ _.... 30 ...... , 23- 25...._2 _ _ 28 _ _ 2 18 . 1:28 :,17 ' "32- i;i 25 : ,21 '23 "_ 25 , '-<;33- -': 33 21' 21_ -33 _ _ ;33 :',17 _ 25-":: *'*;,19 ,....

19 -, 23 12 28 : T 16 13., 21 : , 25 -",,28-; 30 :,:; ,25-: 33 ____: 28 ,;:,18- .. 25 , " 15 21 288 , , 288 288 ;: , 288 288 :: 302.4 :. 316.8 316.8 . .. 316.8 ,316.8 316.8 " 316.8 : 316.8 :: .. 316.8 ':::: 316.8 .. :

23 28 19 26 23 19 21 21 21 23 21 21 23 18 19 23 0 24 36 23 32 27 21 25 28 33 33 28 33 33 30 30 36 0 25 36 23 32 27 21 25 28 33 33 28 33 33 30 30 36 0 26 576 576 576 576 576 590 605 605 605 605 605 605 605 605 605 0 27_________ ____ ________________Chlorine (ppb) (lbs/day) 28 Monthly 33 .585

_________ Average 29MONTHLY CHLORINE USE: 17,554 lbs. Maximum 44 605 30 Minimum 21 576 31 Verify that values have corl a 32 6/25/2015 -- Verflied that atl catca end at AE for 3( da*

33 I I 34 I I 2

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheetsexism 5//215 /2201 5//21 5//21 5/F21 5G/21 5H 1 5//21 5J21 5K021 5/121 5/221 5N321 5/421 5P521 8 UntlT~pp) 15 10 10 10 1 21 19 ___16 <0 _ __ 6 __ 23 18____19 __ 3<1 11 1 1 _ 3 _ _1 3 _ _1 > 13 <01 ' 2 _ 6_ _ 9 _ _1 1 15 Unit2TRC(ppb), . f"t5 * -13:1 ... .... 121 .i <1 23

125. :: 233 ___ 33 28*1:, 2:1 10 30:,;

16 :: :2 30 : 258 . 25.

1 23 ,:' ,<14 917 <10 ! <10 ___ 1_ ,": 123 '25' 36 14 133 250 28 1 , i: 28 256 259 19 <17 12 10 ,;::<10 !*160 _ 25 , 408 _ _,_ 301 _ _ 33 " ' 10 23 :,:1 28 25: 28,:,

19 25 19 19*

13-: <10 °::: 1 10 14 _ _ 30 21 _, _ 30*',_ _ 339 _

21 28 ',; 1 14: 25 ; : .:28 25:

1 25 :; 25 _ _ 23 19 21" C

214 Unit 2 C12 Use (Ibs) 304 :.31.2.345.6 3456. 3456.8 : :*3456. 34568 ::3456. 3456 3456 ::*,3 .4': 316 345.6.331.231688*::.. 280° ';!:288: 31628. :88.

316 15Ui2 R~ p]., *15": 13 : 12 1321 , 21 233 233 18 16 2 :31 2

30 21 23 23 19 18:17 ' 14 : 16 230 40* 36 . 40: i 36 25 30:: 33"12 28 ' 25 231 21 25 Dal Mxmm R (p) 17 :<14 16. 30* ,:i 40 303 40 36 1 25*, 230: "28 33 25 8 .:,25 23 21,1c 26 Unit ~2UCeI2s 6s(bs 34: 662:: 356 :3562 662 662* 6462**

3566. 35( 66356'356::356::312 6 6 3 3605 :: '3605 : 1605 3605 28 29 30 32j__________ ____ _____ _____ ____

33 I ____________________ ________ _________ _________ ________ _________

35 3

Attachment 1 - 2015 2nid Qtr DCPP NPDES Worksheets.xlsm

_ R S T U V W X Y Z AA AB AC At) AE AF AG 4

5 6

7 5161!2015 511712015 511812015 5119/2015 512012015 512112015 512212015 512312015 512412015 5/2512015 512612015 512712015 5/2812015 512912015 5/30/2015 5131/2015 _____

8 , 11 : v11 .. ,11, 12 _ __ 13 12 noiniection no iniection 'no Injection .. ___ 10 ___ 11 <10 _____ 15 ____ 15 : ',13 :': :<10 ____

9 '/, " 16 ::: 16 *:13 1' <10 *t 11: _______ 11 no iniection :no iniection :noihjection ____10 ,* 13 ;: ,<;10 <'; ___.___ 18

13 13

<10 _____

10 ____19 17 13 <10 _ __ 11 . <10 noiniection noiniection no injection ____ 10 <10 ::",<10 , ,16 ___ 11__ 11 ,: <10 ____

11 _,:__, ,::1t6 :, :13. ,::,<10 ... :; "13 : 15 :"12 noinecio no ine cto 10 . 1 <10 ___,____ 12 :::... 1*6______ 18 ____ 11<10 ____

12 ____ "19 ". 10 <10! <10 10 :; <10 noiniection ;noiniection* .. : <10 ____15 <10 _____12 :., '16 , ___ 15 _____ 10 ,<;10 ____

13 _____, : 19.

151: . . 121:, I 11 "10 ____ 1I0 noiniection'noiniection.. '*:*12 :.11 . ....... 11 ____ 15 18 _____: '13 ... i:<10,;,._.:;':,<10 14 288.0 288.0 ':" ;273.6 ' . 259.2 259.2

259.2 .... 0.03:.... 0.0 86.4*" :, 259.2 . 259.2 268.8 288.0

288.0 '288.0'.. . 288.0 _____

15 ___., _ ,17 - 17 :, 17.- ,:. 23 ,.17 *.: .16'.noiniection no injection ': ':,., 0 .... 28 ____ 33 _____*:*:12 1:-:

7 ____ :21 __ '_ ,18 ' : . 18 ____

16 ______ 16 :: 19 .14 '. 21 21 ' : 19 nolnjectio'n no injection _____ 0l___- 30 ___: _ 33 - _,_!;_ : 13 .. , 17 _____ _ 21* ", 19 17 17 ____ 21 '<. 21 , , 21 . .::: 21 ., .'17 ., :19 nolnjection ,no injection _____0i _____ 30 ______28 _,_'_ .... 13 :.' : 18 ,, ,21 : 18 .18 18 ,_____, 19 .: '.*16 ,:. 19: , :!:::25 :21' . 21 rnolnjection nhoinjectjon 10! ': ,331 <10 :_____;;' 14 <:*':21 19 ':' 18 '17 19 19 '17 , 16 .' : 21 : 19 .19 noinjection no injection , 211 , 33 ,___10 , ,16": ' 21

14 16..16.

t6__ 1 _

20 _____,___: 25 :: *:21 : . 21 :::: 19 ,:: 19': 719 no injection no injection 2 . 333 13: 17 :::23 ' 18 , : 16 17 _____

21 i, 31568 o 316.8 309:6 , 302.4 302.4 302.4 ' ,0.0 ' 0.0 ' i18;81 2736! 283:2 . :309.6 ,,,316.8 . 316.8 316.8 316.8 ___

24 25 21 21 25 21 21 0 0 28 33 33 17 23 21 19 18 ____

25 25 21 21 25 21 .21 0 0 28 33 33 17 23 21 19 18 _

26 605 605 583 562 562 562 0 0 205 533 542 578 605 6015 605 605 __

27___Chlorine (ppb) (lbslday)

Monthly 2 6 286____ Average 2 6 29MONTHLY CHLORINE USE: 17,404 lbs. Maximum 40 662 30 M iniu 0 I 0 31 __ ___ ____ ____ ____ ____ ___ ___ ____ ____ ____I Verify that values have cc 32 _ _I_ _ _ _ _ _ _ _ _I_ _ _ _ _ _ _ _ _I_ _0_t_ _ _ _ _ _j6/25/2015 -Ved~ed that all calcs end atAF for 31 d 33 I I

_______ I________ _______ I ________ I________ ________ [

_______ I ________ I _______ _______ II _______ I ________

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm

[

I A C-D D E F G H I J K L M NO 2Chlorinefor esMR _____ _____ _:__

4 FILL IN ONLY SHADEDICOLORED CELLS B.." Date .

7;* 61112015; 6/2/2015 61312015 61412015 615/2015 6/612015l 61712015 6/612015* 619/2015 6/10/2015 6/11t/2015 612122015 6/32015 611412015 6/1112015 8UnitlTRCppbl " ,<10. : <10 ' ':10 ,Li' :19 ;: 18 , ,i. 161'" 13 *: 18 i <10 " 15 . ':13 _ _ 12, 10 ' : <10 ... .

10 ::i!<10 <10 12 : 18 :;;/ 1 16 is i is __ :;.:1 ::

13 , *"

_ _ i12 '19 .10. *.: 15 :.: 13 11: <10 10 , /23 i 19 ,19 _:: 16__ 16 ', 19 1 _":16 15

.__ 15 ... .. 16 " . 13" <10 - : '11 . .. 15 13<10 ' 15 ,19 19 16 161 .. 18 ,, 19c ____:: 12 .. 11 .. ; 19 16 <10 12 13 14 UnttlCl2 Use CIbs) 292.8 316.8 !331.2 , 331.2 . *33 , , .:,3312.2.

,;::331.2 331.2,

... 331.2 3312

32 .... 331.2 331.2 331.2: .331.2 338.4 15Unit2TRC(ppb) i* ' 17/!;*- " 16 * :::34 ,:47 . 36 ' 34:; 37:1 24> 21 , ;. .23. .:::

25 21 ;20 :19. ;21 16"__ _ _*__ _ _'1 17 :37 47 ... 36 .. , 401 39"

24* _ _ _ 22 :: . 241 ... .27 , 24* *24 ,.19 .:24 Th _ _ _ _ _ ___ 15 33 :

-: 36 :47 , _ 36 __ 39l __ 39. 22* .... 21 ,:, " 26 ,; 27 :.,23 21 - -26 0' :22 20

_ _ _ _ _ _ _ _ _ 15- 35 ,* . ;:38 .. 36-* *i':'35 ____ ,.. 38J ___ 41 -_____?.., '23. : !___. 23 *::;* ::24 ,::* 25 , 23 *19 ::: ::i20 : :22 21 Unit 2 C12 Uae (ibs) " 3166 .8: . 331.2 345.6 . 345.6 :::"345.6 345.6. 345.6 ° 3456*... 345.6 1:, 345.6 ; 345.6 3456* 345.6 .... 345.6 , 345.6 23 15 23 25 21 181 19 19 16 18l 25 19* 12 15 16; 2417 35 41 47 38 441 43 24 25 261 27 24* 24 22 24 25Da*y.aimum TRC~pb) 17 35 41 47 38 44 43 24 25 26 27 24 24 22 24 26allyCi2Useoiba) 610 648 677 677 677 677 677 677 677 6771 677 677 67 677 684 27 ________I 28i 29i 30 33 ___________*________________ "

351 4

Attachment I - 2015 2nid Qtr DCPP NPDES Worksheets.xlsm Q R S T U., V W X Y Z AA AB AC" AD AE AF AG 3

4 5

6 7 611612015 611712015 611812015 611912015 612012015 612112015 612212015 6/2312015 612412015 612512015 6/2612015 6127/2015 6/2812015 612912015 613012015 ____

8 .

15-* 10 : , 10 ,, .<10 .:* 15 ," 16 17 19c* 19 12 11 :* <10 ' <103 :: ,<10.: ,: <10 :K

9 K. "*==:15 10'* " <10 .' <10* 19 ,* : 16 --- ,!"; 22 -- 19 , IS .8"* 12 '*11 : <10:=*I;; <103 .. .. *<10 _____!: 10 ,

10 '15 " 12 . ._ <1ID , 11 ' 15 ": *19 115 19!, 18 12 <10 '* <10 -- <103 <10 ______ 10 ________

11- .:::"13 K-: 2 - <1 =,=! 12 ,18 7 '17 ,..*: -<-19, 18 ' 16 I::"13.,. --

.<10-.--.., <10 .. ==, <=10 -= : =<10 , :" <10 " "::;

12. 2 1: :=12 - <10 - , 12 :16 :" 18 : '18 19c , 16 13 <10 " <10- <10 __ _10 ""<10 '

13 ...

,':;12 :.",>.:,13<. *i'=,'

10 15 ,.,:19 ,*: = 16 .:;=:18 _ _ ,19c -*

.12 .. 12 ., , <10.,*::: <10 "<10--.. 12 *i <10 == ';*

14 345.6 -. '345.6 ,345.6 ,34568 :*. 345.6 -: 345.6 , 345.6 --, 345.6 345.6 ': 345.6 345.6 - 345.6 345.6 - 345.6 345.6 ,

15- , ,,23, - .22 22:::, .,.:21 : -..

,303 :..30. -.

,30:___ :33 ... ' : 33. 36 -,36 ___ 17 ___ 18 ___ 17 ___;, :17 ,, ..

16 -

26 _____ 22 "_____,:: 21 -: 22l -33 , :30

-: ---*:,32 -: *,33<i*'-*::i,30- - - 43 :' 25 : - 22. : ' 20 21 __ _ 19,'*.

17 *27 _ _19- 19 _ .. 22 .. .. 30' '::28 5 , ".vi27 i' : 33i.'-, ,*30 - 33. 25 -14< : .. 19 _ _19 ___ 19, _. ___,*

18-':*' 24 ,-: 22 -K::--22;---.= 25=: -,30-- ': : :28 .30 :'! i,-27 K.K:::i36-7 -.;:!'39- 25 .:" 21 ___21. i:, 27 ____ 13 :____' ....

19 ii 23. - 251 -'i :21 *.. . 22 ___ __303 __ _ 28 ___ ,_33 "-.: <i30-- - 39- -- !,:i36 . 27 ":21 _____ :21 22 -_ __ "12 __ _ :_ _ _

20 ,,!* ,22 _ __,;,22 *: :::'22 _ _ _ 27i _ , _ 33 _ __:i :30 _ _ :*:*30:

_ _ _ ?_ 30 39: : :!36 17 _ _ ,,* _ 14 _ __: :::19 :" =21 *11 _ _ _ __.

21 !,"'.345.6 *"345.6 345.6 ,345. 6 345.6 345.6 : 345.6, "345.6 345.6 ; 345.6 345.6 :345.6 345.6 ','345.6 345.6 ______

22 23 15 13 10 15 19 19 22 19 19 13 11 03 0 12 103 0 24 27 25 22 27 33 30 33 33 39 43 36 22 21 27 19 0 25 27 25 22 27 33 30 33 33 39 43 36 22 21 27 19 0 __

26 691 691 691 691 691 691 691 691 691 691 691 691 691 691 691 0 27 _________ Chiorine (ppb) (lbs/day)

Monthly 30 68 28 _____Average 3 8 29 MONTHLY CHLORINE USE: 20,431 lbs. Maximum 47 691 30 Minimum 17 610 31 ______Verify that values have correct references.

32 ____ 06/25/2015 -Ve'fifed that att calcs end at AE fora 30 day month - M6BX 33_ _ _ _ _ _ _ _ _ _ _I_ __

4

Attachment 1 - 2015 2nd Qtr DCPP NPOES Worksheets.xlsm 2

LRW TSS Data 5 2,0 mg/LIs MDL .8, mgiL Is Reporting Limit.

Results are reported to the Water Board to whole numnbers ony (no tenths).

8 System Batch Tank Volume Discharge Date Status Filter I Filter 2 Net TSS TSS for avg. Unused Volumes Weight Weighted TSS 9 LRW 13 DRR 0-1 9,185 4/1512015 12:06 0 1.8 #N/A ND(2) 0027.0 10 LRW 14 LOT 0-1 14,796 4/17/2015 11:17 0 1.8 #iN/A NOD(2) 0 0.44 0.00 33 LRW LT01dp14#/ D2 134 _ LRW CDT___-2 dup__13_8__0.3__3_5 35 LRW 36 LRW 37 LRW 38 __ LRW 39 W 40 toaL oueoRapeWak: 382____ oa u f ouewihs .0Mehe R S vrg _____

41LR 42 ReotLoRWetO~-uR 43 W 51 LRW 1 R - ,8 /521 20 O14 . .700 353__ LRW 5834 _ LRW 357 _ LRW ___

5836 _ LRW_______

5- __ LRW ________

6140 __ total volume of samnpled tanks: 33,832 total sum of volume weights: oRWTn 1.00 Monthly Average 42 _ _Re___ort____<__5___to_ e iCDTi Relet2CT -2RLR Re____ect 643 _ _ I_ _j_ _ _ _ _ _ _

44_ _ _ _ _ _ _I _ _ _ _ _ _

5

Attachment 1 - 2015 2nd Ctr DCPP NPDJES Worksheets.xlsm 2 A B C O LRW TSS Data 5 2.0 mgJL Is MDL 5.0 mg/L Is Reporting Limit.

Results are reported to the WateT Board to whole numbers oniy no tenths, 29 LRW 1 W - ,6 /421 25 . NA< .5O0 30 LRW 18__ CDT_0-1 _461. 5___205_1:32__3_0_N _ 38.0_3_4_0.5_1.8 311 __ LRW CDT___-1 dup_36.7_#N___36.7 32 LRW 19___ PWR____ _-2_5____201_12:26_9,2 133 _ LRW ____

34 LRW 35 LRW 36 LRW 37 LRW _____

38 LRW 39 LR 40 LRW_ttlvlm fsmldtnk: 953ttlsmo ouewigt: 10 atd R S vrg 41 LRW________ ______ ~ ~ 18 42 LRW_______ enl 10RfetCT - L__

43 LR 29I ___ LRW 1 DO1 41952/05:0 0 Nl14 . .000 ______

61 toe ouec a edlny 42 ______LRW____ oa umo ouewihs .0 otl & vrg 631R 64 LRW___________

35 LRW___________ ___ ________

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheetasxlsm LRW TSS Data__

5 2.0 mglL is MDL 5.0 mgWLIs Reportingr Limtt.

Results are reported to the Water Board to whoie numbers only no tenths) 40 Systte vlm Bal c ofsm edTanks 40,133 ae Sau Fle itr2N Ttatocag S um of volum S aei Unts edV1.00 e Wethlht L W elhStAerTSe 10__LRW ReTort-25Because1C#NI0-22.R 1 LDW O&G Dat-a499 /021 :3 . NA<.0003300 41___1 .4mgLRW ML5. Rep LT 0-s or7 #NLim2t.

814 tota voum3 fa led-2 tanks:05 515 tota su1f5oueegts1.08otlyO1Av 02 LW 2 W 0162/05 14 ,3 83 LW 2 D02 5862/051:1 61032. 5003"03 84 LWCT02du 57132.

185 LW 2 - /9/051:61,8

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm 3 001N Monthly Average Calculations________

4 NOTE: Values <Reporting Limit are treated as 0 when averaged with values

RL. ________

5 All Results on this sheet are included in Vendor Laboratory Data 6 II-_ _

7 0.24 mg/L is O&G method 1664 MDL for BSK Lab.

8. 5.0 mglL is O&G Method 1664 Reporting Limit.

9 Results are reported to the Water Board to the nearest tenth mg/L. ____________

10 11 Oil and Grease (mg/L)

_________________Numerical Daily RslsfrMnhy Rpr otl 14 Date Result Average Average Qualifier Avesuagefo Mothy veprtonhl 15____ 41215 DNQ(0.69) 0.23 DNQ 0.23 0.6 16 ____ND(0.24) Report DNQ(0.6) 17 ____JND(0.24) 1_ ______ ii*!',151 *, ND(0.24) 0.46 DNQ 0.46 Daily Maximum 19 DNQ0.79)1.5 21 4ii/13/201'51:i ND(0.24) 0.13 DNQ 0.13 24 4/22/2*!015S:= DNQ(1.4) 1.5 DNQ 1.5 27 ii:4/29/20"15 : DNQ(0.29) 0.46 DNQ 0.46

____Total Suspended Solids (mglL)

Date Result Numerical Result Monthly Average 35 4111215_1 11 14 36- 4/8/2015 18 18 37 4/13/2015 6 6 Daily Maxim um 38 4/22/2015 31 31 31 ________

39 4/29/2015 6 6

- Settleable Solids (milL)

Date Result Numerical Result Monthly Average 4,5 4/1/2015 DNQ(0.1) 0.0 0.1 46- 4/8/2015 DNQ(0.1) 0.0 47 4/13/2015 DNQ(0.1) 0.0 Daily Maximum 48 4/22/2015 0.5 0.5 0.5 49 4/29/2015 DNQ(0.1) 0.0 8

Attachment 1 -2015 2nd Qtr DCPP NPDES Worksheets.xlsm A B C 0D E 1 FGH 3 00tN Monthly Average Calculations _______ _______

4 NOTE: Values <Reporting Limit are treated as 0 when averaged with values ;: RL.

5 All Results on this sheet are included in Vendor Laboratory Data 7 0.24 mg/'L is O&G method 1664 MDL for BSK Lab.

8 5.0 mglL is O&G Method 1664 Reporting Limit.

9 ____Results are reported to the Water Board to the nearest tenth mglL, 11 ___ Oil and Grease (mglL)

Numeica Daly verae QaliierResults for Monthly Report Monthly 14 Date Result NueiaDil Average Qulfe Average Average 15 *':5/6/20115 DNQ(1.5) 2.3 DNQ 2.3 1.03 16 DN(3.5)Report DNQ(1.0)

-6iiii~~5" 01 . DNQ(0.78) 0.9 DNQ 0.9 Daily Maximum 19DNQ0.70)2.3 21 "5/20/*2015 ,*DNQ(0.8) 0.5 DNQ 0.5 24 5/26/201i5**: DNQ(0.59) 0.4 DNQ 0.4 35 5/6/205.454) 36 N/12/21524) 37 5/20/2015:: 101 al aiu

To~Sttabl sene Solids (milL)

Date Result Numerical Result Monthly Average 45 5/6/2015 40. 0. 7N(0 46 5/12/2015 <0. 0.

47 5/20/2015 010 0.0 Daily Maxim um 48 5/26/2015 <0. 0. 10.

5239 __ _____ _____ _________________________________________

2

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm A BCD I E ] FGH 3 O01N Monthly Average Calculations________

4 _____NOTE: Values <Reporting Limit are treated as 0 when averaged with values > RL.

5 ___ All Results on this sheet are included in Vendor Laboratory Data 6~ I 7 ____0.24 mg/L is O&G method 1664 MDL for BSK Lab.

8 ____5.0 mglL is O&G Method 1664 Reporting Limit.

9 ____Results are reported to the Water Board to the nearest tenth mg/L.

11 ____Oil and Grease (mg/L)

Dt Reut Numerical Daily RslsfrMnhy Report Monthly 14 [at Reut Average Average Qualifier Aveltfrag Average 15 i i6/2/201511* ND(0.24) 0.00 ND 0.00 0.30 16 6/2/2015 ND(0.24) Report DNQ(0.30) 17 I,.6/2/2015 ND(0.24) ________

18 ,6/10/()2015, DNQ(0.58) 0.62 DNQ 0.62 Daily Maximum 19 NQ(070)0.62 6101215 2 161/15 ND02)0.13 DNQ 0.13 24 ,*6/22/2015' DNQ(0.30) 0.43 DNQ 0.43 35 6/2/12015 9NQ90.69 38 6/22/2015 9NQ(0.16 40

J ~ SToteablSsene Solids (mi/L) 44Date Result Numerical Result Monthly Average 45 ____ 6/2/2015 <0. 0. DQ01) 46 ____ 6/10/2015 <01 0.0 47 6/16/2015 <0. 0. Daily Maximum 48 ___ 6/22/2015 <0. 0. 0.0 49 ____

10

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm

__,_c E IF G H JKLMN

{

3 Miscellaneous Daily DuplicatelAverage and Monthly Average Calculations for eSMR 7 Date Time Analysis Date~ Location ~Unit Parameter Result Average_ ___

9 4/13/2015 14:42 4/13/2015 O*P.NA. H" 7.64 7.6 10 4/13/2015 14:42 4/13/2015 7.64N/

12 4/1/12015 9:40 4/1/2015 02 1 pf~i:iiiH* 7.73 7.8 13 ___ 4/1/2015 9:45 4/1/2015 7.78 19 182ml

____Results 2

sML. 5 mglL is Reporting Limit.

Loain Ui

}-t______

are reported to the Water Board to whole numbers only (no tenths).

TSS for Daily Numerical Monthly Reported Monthly 21Date Time Analysis Date Lato Unt Sample TSS Filtrate TSS Net TSS Average Average Average Average 23 ___ 4/2/2015 7:10 4/2/2015 i :i00:1F *: N/A 1.3 0.0 1.3 0.0 0.0 0.0 ND(2) 24 ___ 4/2/2015 7:10 4/2/2015 D F i

ii00 N/A 1.1 0.0 1.1 0.0 26 4/2/2015 2: 30 4/2/2015 ' OOH*:'

1

':".,::,*, <0.1 <0.1 <2.0 0.0 0.0 0.0 ND(2) 27 4/1/2015 12:10 4/1/12015 !; : :0011-1 :*2 ;; 0.2 0.1 <2.0 0.0 0.0 29 4/9/2015 10:48 4/9/2015 . OL 1 <2.0 #N/A <2.0 0.0 0.0 0.0 NO(2) 30 4/9/2015 10:58 4/9/2015 ODL 2 <2.0 #N/A <2.0 0.0 32 ___ 4/13/2015 10:03 4/13/2015 OO1:**P: ::! N/A:: 9.3 0.5 8.8 8.8 5.6 5.8 6 33 4/13/2015 12:15 4/13/2015 'O"i N/A 8.5 0.4 8.1 8.1 34 4/13/2015 14:42 4/13/2015 i:i: OQI

:: N/At* 3.7 1.0 2.7 0.0 36 ___ 4/1/2015 9:40 4/1/2015 3/4)02 1 3.3 0.7 2.6 2.6 3.4 3.4 DNQ(3) 37 ___ 4/1/2015 9:45 4/1/2015 02 2 4.6 0.4 4.2 4.2 339 4/1/12015 12:20 4/1/12015 " 003 N/A*;'*: 19.4 0.8 18.6 18.6 19.7 19.7 20 40 ____ 4/1/2015 12:20 4/1/12015 00 NM 21.3 0.5 20.8 20.8 11

Attachment 1 - 2015 2nd Qtr DCPP NPDES Worksheets.xlsm A B C I D E F G H IJKLMN 2

3 Miscellaneous Daily Duplicate/Average and Monthly Average Calculations for eSMR 4

5 Duplicate pH Averages _____ ______

6 7 Date Time Analysis Date Location Unit Parameter Result Average 81 511/2015 15:20 5151/2015 *i p* .: 7.54 7.6__

105/5/2015 10:45 5/5/2015 P N/7.58_____ .

10 5/5/2015 10:45 5/5/2015 P./A 00 1 pp .. . 75 7.74 7.7 ______

13 ___ 5/7/2015 15:25 5/7/2015 02 2 *.~p 7.73 16 Monthly TSS Averages______ _____ ______

18 2 gLis MDL. 5 g/L is Reporting Limit.______

19 Results are rep*orted to the Water Board to whole numbers only (no tenths). Numerical Reported 20 FiltrateUnitTSS for Daily Monthly Monthly 221 ae Tm Anyi atSmpl TSS _Filtrat TS e eTS Average Average Average Average 23 5/4/2015 12:45 5/4/2015 JOOE NA 1.9 0.0 1.9 1.9 1.7 1.7 DNQ(2) 24 ___ 5/4/2015 12:45 5)4/2015 O:"*:i'0iF-

; N/A: 1.7 0.2 1.5 1.5 26 5/2/2015 8:45 5/2/2015 OOH 1 0.2 0.0 0.2 0.2 0.2 0.3 ND(2) 27 5/1/2015 16:10 5/1/2015 0I 2, 0.4 0.0 0.4 0.4 0.4 28 ______:_0.0__ND(2)_

29 5/6/2015 13:43 5/8/2015 01L 1 .0#N/A 0.0 0.0 0.2 0.2ND2 30 5/8/2015 13:48 5/8/2015 00i: .)2 0.4 #N/A 0.4 0.4 332 5/5/2015 7:53 5/5/2015 *:: "O'** iP** 'N/A:"*::,*,,,: 3.2 0.5 2.7 2.7 2.5 2.5 DNQ(3) 335/5/2015 10:45 5/6/2015 OO1P' N/A:::::::::: 4.5 0.73.38 34 ____ 5/5/2015 13:55 5/5/2015 JK;* :i;00*1 P-I! : N/Ail 1.7 0.8 0.9 0.9 38536 __ 5/7/2015 15:20 5/11/2015 '0 2. 1 2.3 0.2 2.1 2.1 1.9 1.9 DNQ(2) 37 ___ 5/7/2015 15:25 5/11/2015 :'0i;*(02 2 2.1 0.5 1.6 1.6 339 5/5/2015 9:17 5/5/2015 , : '003.. : N/A~i 3.4 0.2 3.2 3.2 2.8 2.8 DNQ(3) 40 /5/2015 5___ 9:17 5/5/2015 0 NA 2.7 0.4 2.3 2.3 ______

43 ___

44 ___

12

Attachment 1 -2015 2nd Qtr DCPP NPDES Worksheets.xlsm 2A B CI D E IFI G H MN 3 Miscellaneous Daily DuplicatelAverage and Monthly Average Calculations for eSMR 4

5 Duplicate pH Averages______________

6 7 Date Time Analysis Date Location Unit Parameter Result Average 8

9 6/8/2015 13:24 6/8/2015 ,*,001P' N/A i';pH* 7.67 7.7 10 6/8/2015 13:24 6/8/2015 D

001P N/A pH : 7.70 12 6/1/12015 12:31 6/1/12015 i, :002',:: 1 * .: p:H i= .: 7.85 7.9 13 61/12015 8___ 12:35 6/1/12015 02 2 pH 7.886 ______

16 ____MnhyTSS Averages____________ _ ______

18 2 m_/L is MDL.5 glL isReporting Limit.__ _____

19 ___ Results are reported to the Water Board to whole numbers only (no tenths). Numerical Reported 21 ae Tm nayi ae{ Un it TSS for Daily Monthly Monthly 22 ae Tm nlssDt Location Ui 1 Sample TSS Filtrate TSS Net TSS Average Average Average Average 23 __ _ 6/1/12015 7:20 6/1/2015 "DO{)IF, N/AK 2.0 0.1 1.9 1.9 1.5 1.5 DNQ(2) 24 __ _ 6/1/12015 7:20 6/1/12015 001F, ';N/A ' 1.3 0.2 1.1 1.1 25 ___. .. , ..

26 ___ 6/1/2015 3:20 6/1/2015 :* 001ll ,

": 1 :, <0.1 <0.1 <2 0.0 0.0 0.0 ND(2) 27 ___ 6/2/2015 3:30 6/2/2015 OH .2 0.2 <0.1 <2 0.0 29 __ 6/1/12015 9:48 6/1/12015 OO1Q*L." I, ' 0.0 #N/A 0.0 0.0 0.0 0.0 ND(2) 30 ___ 6/1/2015 9:53 6/1/2015 .' O011" ;*2 ' 0.0 #N/A 0.0 0.0 31 :: ,,

32 ___ 6/8/2015 7:20 6/8/2015 O:i:00P:"N/A 14.0 1.8 12.2 12.2 4.1 4.1 DNQ(4) 33 ___ 6/8/2015 10:29 6/8/2015 OO1P,,

00F*,,N/A 2.5 1.6 0.9 0.0

!34 ___ 6/8/2015 13:24 6/8/2015 ... O 01P i : :N/A: 2.3 1.1 1.2 0.0 36 __ 6/1/12015 12:31 6/1/12015 :' ,002 ' 1 i 1,0 0.3 0.7 0.7 0.9 0.9 ND(2) 37 6/1/12015 12:35 6/1/12015 ' 00'Q2' 2, ' 1.5 0.5 1.0 1.0 39 6/1/2015 12:17 6/1/2015 p00:i*d3;* N/A: 4.5 0.4 4.1 4.1 4.0 4.0 DNQ(4) 40 6/1/2015 12:17 6/1/2015 ... ::003,*,:: N/A i 4.3 0.5 3.8 3.8 41 42 43____

13

Diablo Canyon Power Plant 2015 Second Quarter Contract Lab Results POE Page Description 2 -4 001N Oil &Grease -04/01/2015 5 -7 001N Oil &Grease-04/08/2015 8 -10 001N Oil &Grease -0411312015 11 -13 O01N Oil &Grease -04/2212015 14 -16 001IN Oil &Grease -0412912015 17 -19 O01N Oil & Grease - 05/06/2015 20 - 22 001 N Oil & Grease - 05/12/2015 23 -25 001N Oil & Grease - 05/20/2015 26 -28 001N Oil &Grease -0512612015 29 -31 001N Oil & Grease -06/02/2015 32 -34 001N Oil &Grease -06/10/2015 35 -37 001N Oil &Grease -06/16/2015 38 -40 001N Oil &Grease -06/22/2015 41 001N Suspended Solids, Settleable Solids- 0410112015 42 001 N Suspended Solids, Settleable Solids - 04/08/2015 43 001 N Suspended Solids, Settleable Solids -- 04/13/2015 44 001 N Suspended Solids, Settleable Solids - 04/22/2015 45 001 N Suspended Solids, Settleable Solids - 04/29/2015 46 001 N Suspended Solids, Settleable Solids - 05/06/2015 47 001 N Suspended Solids, Settleable Solids - 05/12/2015 48 001 N Suspended Solids, Settleable Solids - 05/20/2015 49 001 N Suspended Solids, Settleable Solids - 05/26/2015 50 001 N Suspended Solids, Settleable Solids - 06/02/2015 51 001 N Suspended Solids, Settleable Solids - 06/10/2015 52 001 N Suspended Solids, Settleable Solids - 06/16/2015 53 001 N Suspended Solids, Settleable Solids - 06/22/2015 001 H, Unit 2 Mercury - 04/06/2015 to 06/08/2015 Composite 54 O01L, Unit I Mercury- 0410112015 to 06/10/2015 Composite

________001 L, Unit 2 Mercury - 04/01/2015 to 06/10/2015 Composite 001 H, Unit 1 Metals - 04/06/2015 to 06/08/2015 Composite 55 0010 Mercury, Metals - 04/15/2015 to 06/11/2015 Composite

______001 OF Mercury - 04/10/2015 to 04/17/2015 Composite 56 -57 Intake, Discharge 001 Ammonia as Nitrogen - 04/29/2015 58 - 62 Discharge 001 Acute Toxicity Test - 05/11/2015 63 - 77 Discharge 001 Chronic Toxicity Test - 05/11/2015

A5D0192 Main Project.-e COC Trace (MDLs)

Associates Engineer ab oratories. 15-1853 DCWW'TP Analsis Sample ID: A5D0192-01 Sample Date - Time: 04/01/15 - 11:57 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 04/09/15 J 0.69 0.24 5.0 mg/L 1 A503908 04/08/15 A5D0192 FINAL 04162015 1443 Printed: 04/16/2015 QA-RP-0001-10 Final~rpt www.BSKAssociates.com Page 3 of 11

A5D01 92 Associates Main Project- e COC Trace (MDLs)

Engineer2rZaboratories 15-1 853 DCWWdTP Certificate of Analysis Sample ID: ASD01 92-02 Sample Date - Time: 04/01/15 - 12:12 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L A503908 04/08/15 04/09/15 A500192 FINAL 04162015 1443 Printed: 04/16/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 4 of 11

A5D01I92 Associates Main Project - e COC Trace (MDrs)

J 15-1 853 DCWW'N-P Engineer2r*ab oratories Sample ID: A5D0192-03 oFrAalsns Sample Date - Time: 04/01/15 - 12:27 Sampled By: Client Certissciates Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

-- S - . -. -.... . .. A.

Oil and Grease (1664)

Total Oil & Grease EPA 1664A 04/09/15 ND 0.24 5.0 mg/L 1 A503908 04/08/15 A5D0192 FINAL 04162015 1443 Printed: 04/16/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates~com Page 5 of 11

A5D0927 Associates Main Project - e COC Trace (MDLs) 15-2037 DCWW'I'P Engineer~raboratories Certificate of Analysis Sample ID: A500927-O1 Sample Date - Time: 04/08/15 - 12:25 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A504426 04/21/15 04122/15 A5D0927 FINAL 04232015 1542 Printed: 04/23/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com S;Page 3 of 11:

A5D0927 Associates Main Project - e COC Trace (MDLs)

Engineer~raboratories 15-2037 DCWWTP Analsns Sample ID: A5D0927-02 Sample Date - Time: 04/08/15 - 12:34 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

- -. S Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.79 0.24 5.0 mg/1. 1 A504426 04/21/15 04/22/15 J A500927 FINAL 04232015 1542 Printed: 04/23/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 4 of 11

A5D0927 Main Project- e COC Trace (MDLs)

Associates 15-2037 DCVWWTP Engineer~raboratories Certificate of Analysis Sample ID: A5D0927-03 Sample Date - Time: 04/08/15 - 12:46 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics S -. ......

Oil and Grease 11664)

Total Oil & Grease EPA 1664A 04/22/15 J 0.59 0.24 5.0 mg/L 1 A504426 04/21/15 A5D0927 FINAL 04232015 1542 Printed: 04/2312015 QA-RP-0001-10 Final.rpt QA-R-000-10 inaIrptwww.BSKAssociates.com I:Page 5 of *11

A5D1 257 Associates Main Project- e COC Trace (MDLs) 15-2124 DCVWVTP Engineer 4 Caboratories Certificate of Analysis Sample ID: A5D1257-01 Sample Date - Time: 04/13/15 - 09:45 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (16641 Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A504503 04/22/15 04/23/15 A5D1257 FINAL 04282015 1418 Printed: 04/28/2015 QA-RP-0001-10 Final.rpt www,BSKAssociates.com ]:Pa'ge 3 of *1li

A5D1 257 Main Project- e COC Trace (MDLs)

Associates 15-2124 DCWV-I-P Engineer 4 Taboratories Certificate of Analysis Sample ID: A5D1257-02 Sample Date -Time: 04/13/15- 10:00 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Orqanics Oil and Grease (1664)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A504503 04/22/15 04/23115 A5D1257 FINAL 04282015 1418 Printed: 04/28/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Paget4 of=1:1 :: 1

A5D1257 Main Project - e COC Trace (MDLs)

Associates 15-2124 DCWWMTP Engineer*Eab oratories Certificate of Analysis Sample ID: A5DJ1257-03 Sample Date - Time: 04/13/15 - 10:12 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1 664A 0.40 03.24 5.0 mg/L 1 A504503 04/22/15 04/23/15 A5D1257 FINAL 04282015 1418 Printed: 04/28/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates.com SPage 5 of 11:=

A5D2221I Associates Main Project - e COC Trace (MDLs)

Engineer~raboratories 15-2347 DCWWTP Analsis Sample ID: A5D2221-01 Sample Date - Time: 04/22/15- 13:40 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

- a Oil and Grease (1664}

Total Oil & Grease 05/'05/15 EPA 1664A 1.4 0.24 5.0 mg/L 1 A504910 05/04/15 A5D2221 FINAL 05072015 1635 Printed: 05/07/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com P

age 3 of 11 ;*

A5D2221 Associates Main Project - e COC Trace (MDLs) 15-2347 DCVWWTP Engineer~raboratories Sample ID: A5D2221-02 oFrAalsis Sample Date - Time: 04/22/15 - 13:49 Sampled By: Client Certificiates Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

-- a - *.. . . C Oil and Grease (1664)

Total Oil &Grease 05/05/15 J EPA 1664A 1.9 0.24 5.0 mg/L 1 A504910 05/04/15 A5D2221 FINAL05072015 1635 Printed: 05/07/2015 QA-RP-0001-10 Final.rpt www, BSKAssociates.com Page 4 of 11

A5D2221 Main Project.-e COC Trace (MDLs)

Associates 15-2347 DCWWJTP Engineer~faboratories Sample ID: A5D2221-03 oFrAalsis Sample Date - Time: 04/22/15 - 14:13 Sampled By: Client Certificiates Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

-. S - -. *..... ., 0 Oil and Grease (1664)

Total Oil & Grease EPA 1664A 1.1 0.24 5.0 mg/L 1 A504910 05/04/15 05/05/15 J A5D2221 FINAL 05072015 1635 Printed: 05/07/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates.com Page 5 of 11

A5D2626 Main Project- e COC Trace (MDLs)

Associates 15-2459 DCWWNTP Engineer~1boratories Analsis Sample ID: A5D2626-01 Sample Date - Time: 04/29/15 - 10:42 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm -3 Sample Type: Grab BSK Associates Fresno Organ ics

-.- S -~ -. ... .. *1 Oil and Grease (1664)

Total Oil & Grease EPA 1664A 05/09/15 J 0.29 0.24 5.0 mg/L 1 A505087 05/07/15 A5D2626 FINAL 05142015 1533 Printed: 05/14/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 3 of 11

A5D2626 Associates Main Project - e COC Trace (MDLs)

Engineer~~ab oratories 15-2459 DCWWITP Certificate of Analysis Sample ID: A5D2626-02 Sample Date - Time: 04/29/15 - 11:00 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm -4 Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease 11664)

Total Oil & Grease EPA 1 664A 0.59 0.24 5.0 mg/L 1 A505087 05/07115 05/09/15 J A5D2626 FINAL 05142015 1533 Printed: 05/14/2015 QA-RP-0001-10 Final.rpt QA-R-000-10 inalrptwww, BSKAssociates.com Page 4 of 11

A5D2626 Main Project - e COC Trace (MDLs)

Associates 15-2459 DCVWW'IP Engineer~.aboratories Analsis Sample ID: A5D2626-03 Sample Date - Time: 04/29/15 - 11:21 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm -5 Sample Type: Grab BSK Associates Fresno Organ ics S - ., C.

Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.49 0.24 5.0 mg/L 1 A505087 05/07/15 05/08/15 ~J A5D2626 FINAL 05142015 1533 Printed: 05/14/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 5 of 11

A5E0541 Main Project - e COC Trace (MDLs)

Associates 15-2605 DCWWNTP Engineer~1aboratories Certificate of Analysis Sample ID: A5E0541-01 Sample Date - Time: 05/06/15 - 12:10 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 1.5 0.24 5.0 mg/L 1 A505367 05/14/15 05/17/15 J A5E0541 FINAL 05202015 1411 Printed: 05/20/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com I:Page 3 o°f 1 ":;

1

A5E0541 Main Project - e COC Trace (MDLs)

Associates 15-2605 DCWWTP Engineer~1aboratories Certificate of Analysis Sample ID: A5E0541 -02 Sample Date - Time: 05/06/15 - 12:21 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 3,5 0.24 5.0 rng/L 1 A505367 05/14/15 05/17/15 J A5E0541 FINAL 05202015 1411 Printed: 05/20/2015 QA-RP-0001-10 Final.rpt www,BSKAssociates.com I:Page 4 of:111 :

A5E0541 Main Project - e COC Trace (MDLs)

Associates 15-2605 DCWW]'P Engineer*L'ab oratories Certificate of Analysis Sample ID: A5E0541 -03 Sample Date - Time: 05/06/15 - 12:36 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A A505367 05/14/15 05/17/15 J 1.9 0.24 5.0 mg/L A5E0541 FINAL 05202015 1411 Printed: 05/20/2015 QA-RP-0001-1 0 Final.rpt www,BSKAssociates.com SPageS5 of 11*,

A5E1 347 Main Project- e COC Trace (MDLs)

Associates 15-2732 DCVWW'P Engineer*Tab oratories Certificate of Analysis Sample ID: A5E1347-01 Sample Date - Time: 05/12/15 - 08:42 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics S -- .. "., . -. 0 Oil and Grease (1664)

Total Oil & Grease EPA 1664A A505742 05/26/15 05/27/15 J 0.78 0.24 5.0 mg/L A5E1347 FINAL 05292015 1643 Printed: 05/29/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 3 of 11

A5E1 347 Main Project- e COC Trace (MDLs)

Associates 15-2732 DCWWTP Engineer*/*ab oratories Certificate of Analysis Sample ID: A5E1347-02 Sample Date - Time: 05/12/15 - 08:56 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.70 0.24 5.0 mg/L 1 A505742 05/26/15 05/27/15 J A5E1347 FINAL 05292015 1643 Printed: 05/29/2015 QA-RP-0001 -10 Final~rpt www.BSKAssociates.com Page 4 of 11

A5E1 347 Associates Main Project - e COC Trace (MDLs)

Engineer*L~ab oratories 15-2732 DCWWNTP Certificate of Analysis Sample ID: A5E1347-03 Sample Date - Time: 05/12/15 - 09:10 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 1.3 0.24 5.0 mg/L 1 A505742 05/26/15 05/27/15 A5E1347 FINAL05292015 1643 Printed: 05/29/2015 QA-RP-0001-1O Final.rpt www.BSKAssociates~com Page 5 of 11

A5E1 886 Main Project- e COC Trace (MDLs)

Associates 15-2895 DCVWWTP Engineer aboratories Certificate of Analysis Sample ID: A5E1886-01 Sample Date - Time: 05/20/15 - 12:45 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.80 0.24 6.0 mg/L 1 A505975 05/30/15 06/01/15 'J A5E1 886 FINAL 06052015 1354 Printed: 61512015 QA-RP-0001-10 Final.rpt QA-RP-0001-0 FinaI~rptwww.BS KAssociates.com Pg f1

A5E1 886 Associates Main Project- e COC Trace (MDLs)

Engineer~'aboratories 15-2895 DCWWJTP Certificate of Analysis Sample ID: A5E1886-02 Sample Date - Time: 05/20/15 - 13:00 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A505975 05/30/15 06101/15 A5E:1886 FINAL 06052015 1354 Printed: 6/5/2015 QA-RP-0001-1 0 Final~rpt www.BSKAssociates.com" Page 4 of 11

A5E1886 Associates Main Project - e COC Trace (MDLs)

Engineerfaboratories 15-2895 DCWWTIP Certificate of Analysis Sample ID: A5E1886-03 Sample Date - Time: 05/20/15 - 13:15 Sampled By: Cilent Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil &Grease EPA 1664A 0.59 0.24 5.0 mg/L 1 A505975 05/30/15 06/01/15 J A5E1 886 FINAL 06052015 1354 Printed: 6/5/2015 QA-RP-0001-10 Final.rpt QA-RP-0001-0 Final~rptwww, BS KAssociates.com Pg f1

A5E21 73 Main Project- e COC Trace (MDLs)

Associates 15-2990 DCWWTP Engineer~faboratories Analsns Sample ID: ASE2173-01 Sample Date - Time: 05/26/15 - 08:58 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (16641 Total Oil & Grease EPA 1664A 05/31/15 J 0.59 0.24 5.0 mg/L 1 A505972 05/29/15 A5E2173 FINAL 06082015 1305 Printed: 06/08/2015 OA-RP-0001-10 FinaL~rpt www.BSKAssociates.com Page 3 of 11

A5E21 73 Main Project- e COC Trace (MDLs)

Associates 15-2990 DCWWTP Engineer~l~aboratories Certificate of Analysis Sample ID: A5E2173-02 Sample Date - Time: 05/26/15 - 09:10 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

2 - -. - *6. ** -

Oil and Grease (1664)

Total Oil & Grease EPA 1664A A505972 05/29/15 05/31/15 J 0.50 0.24 5.0 mg/L A5E2173 FINAL 06082015 1305 Printed: 06/08/2015 QA-RP-0001-10 FinaI.rpt www, BSKAssociates.com Page 4 of 11

A5E21 73 Associates Main Project - e COC Trace (MDLs)

Engineer 4 Oab oratories 15-2990 DCWWI"TP Certificate of Analysis Sample ID: A5E2173-03 Sample Date - Time: 05/26/15 - 09:22 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A505972 05129/15 05/31/15

.A5E2173 F1NAL 06082015 1305 Printed: 06/08/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates.com Page 5 of 11

A5F0282 Associates Main Project - e COC Trace (MDLs)

Engineer~4aboratories 15-3129 DCWWI'P Analsis Sample ID: A5F0282-01 Sample Date - Time: 06/02/15 - 10:32 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 06/16/15 ND 0.24 5.0 mg/L 1 A506574 06/12/15 A5F0282 FINAL 06162015 1654 Printed: 06/16/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates.com :age P: :3 o0f' 11!;

A5F0282 Main Project - e COC Trace (MDLs)

Associates 15-3129 DCWWATP Engineer2*ab oratories

'-N Analsis Sample ID: A5F0282-02 Sample Date - Time: 06/02/15 - 10:44 Sampled By: Client Certificiateso Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 06/16/15 ND 0.24 5.0 rng/L 1 A506574 06/12/15 A5F0282 FINAL 06162015 1654 Printed: 06/16/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates.com P**age 4 of 11

A5F0282 Associates Main Project - e COC Trace (MDLs) 15-3129 DCWWJTP Engineer~faboratories Certificate of Analysis Sample ID: A5F0282-03 Sample Date -Time: 06/02/15 - 10:59 Sampled By: Client Matrix: Water Sample.Descriptioni: Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A506574 06/12/15 06/16/15 ASF0282 FINAL 06162015 1654 Printed: 06/16/2015 QA-RP-0001 -10 Final.rpt www.BSKAssociates.com Page 5 of 11

A5F1130 Main Project- e COC Trace (MDLs)

Associates 15-3317 DCWMNrP Engine er*fab oratories Certificate of Analysis Sample ID: A5F1130-01 Sample Date - Time: 06/10/15 - 08:26 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab" BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease 06/18/15 J EPA 1664A 0.58 0.24 5.0 mg/L 1 A506712 06/16/15 A5F1130 FINAL 06192015 1511 Printed: 06/19/2015 QA-RP-0001-10 FinaI~rpt www.BSKAssociates.com Page 3 of 11

A5F1130 Main Project - e COC Trace (MDLs)

Associates 15-3317 DCWWf'P Engineer~1a~boratories Certificate of Analysis Sample ID: A5F1130-02 Sample Date - Time: 06/10/15 - 08:40 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type:

BSK Associates Fresno Organ ics a -..- *. . -S Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.70 0.24 5.0 mg/L A506712 06116115 06/18/15 J A5F1130 FINAL 06192015 1511 Printed: 06/19/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates~com ]::/:.Page 4 of ! 11

A5F1130 Main Project- e COC Trace (MDLs)

Associates 15-3317 DCWW~TP Engineer~'r~ab o atories Certificate of Analysis Sample ID: A5F1130-03 Sample Date - Time: 06/10/15 - 08:51 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type:

BSK Associates Fresno Organ ics Oil and Grease (16641 Total Oil & Grease EPA 1664A 0.59 0.24 5.0 mg/L 1 A506712 06116/15 06/18/15 J A5F1130 FINAL 06192015 1511 Printed: 06/19/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Pa~ge5 of 11:

A5F1572 Main Project - e COC Trace (MDLs)

Associates 15-3429 DCWW1-P Engineer*Tib oratories Certificate of Analysis Sample ID: A5F1572-01 Sample Date - Time: 06/16/15 - 12:30 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1654)

Total Oil & Grease EPA 1664A ND 0.24 5.0 mg/L 1 A507163 06/26/15 06/28/15 A5F1572 FINAL 06292015 1708 Printed: 06/29/2015

Page 3

of, 1 QA-RP-0001-10 Final.rpt QA-R-000-10 inalrptwww, BSKAssociates.com

A5F1 572 Main Project- e COC Trace (MDLs)

Associates 15-3429 DCWWITP Engineer2*ab oratories Sample ID: A5F1572-02 oFrAalsis Sample Date - Time: 06/16/15 - 12:42 Sampled By: Client Certificiates Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics

- .. .g .-.

Oil and Grease (1664)

Total Oil & Grease 06/28/15 EPA 1664A ND 0.24 5.0 rmg/L 1 A507163 06/26115 A5F1572 FINAL 06292015 1708 Printed: 06/29/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates~com ] *Page 4of;; 11 I

A5F1572 Main Project- e COC Trace (MDLs)

Associates 15-3429 DCWW'TP Engineer.2iab oratories Certificate of Analysis Sample ID: A5F1572-03 Sample Date - Time: 06/16/15 - 12:54 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.39 0.24 5.0 mg/L 1 A507163 06/26/15 06/28/15 J A5F1572 FINAL 06292015 1708 Printed: 06/29/2015 QA-RP-0001-1 0 Final.rpt www.BSKAssociates.com Page 5 of 11

A5F1 992 Main Project- e COC Trace (MDLs)

Associates 15-3536 DCWW'rNP Engineer"aib orato ties Sample ID: A5F1992-01 oFrAelsis Sample Date - Time:' 06/22/15 - 09:09 Sampled By: Client CeKAificiates Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics U - -. ......

Oil and Grease (1664)

Total Oil & Grease EPA 1664A 07102/15 J 0.30 0.24 5.0 mg/L 1 A507339 07/01/15 A5F1992 FINAL 07062015 1445 Printed: 7/6/2015 QA-RP-0001-10 Final.rpt wiww.BSK(4ssociates.com IZPage 30of 11!

A5F1 992 Main Project- e COC Trace (MDLs)

Associates 15-3536 DCWVVWTP Engineer*Cab oratories Certificate of Analysis Sample ID: A5F1992-02 Sample Date - Time: 06/22/15 - 09:21 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organ ics Oil and Grease (1664I Total Oil & Grease EPA 1664A 0.69 0.24 5.0 mg/L 1 A507339 07/01/15 07/02115 J A5F1992 FINAL 07062015 1445 Printed: 7/6/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 4 of 11

A5F1992 Main Project- e COC Trace (MDLs)

Associates 15-3536 DCWWTP Engineer~caboratories Certificate of Analysis Sample ID: A5F1992-03 Sample Date - Time: 06/22/15 - 09:33 Sampled By: Client Matrix: Water Sample

Description:

Decant Arm Sample Type: Grab BSK Associates Fresno Organics Oil and Grease (1664)

Total Oil & Grease EPA 1664A 0.30 0.24 5.0 mg/L 1 A507339 07101/15 07/02/15 J A5F1992 FINAL 07062015 1445 Printed: 7/6/2015 QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 5 of 11

Abalone Coast Analytical, Inc. Order #: 15-1853 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 4/1/15 1353 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWtITP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP

~Sample #Sample Description~ Datel/Time Analysis Method Result MDL RL Dil Factor Units Completed I-1 Decant Arm Suspended Solids SM 2540 0. 11. 2.57 3. 1 mgIL

-2 Deca nt Arm 1411115 1157 411115 0800 Settleable Solids SM 2540 F. III <0.1 0.1 1 mL/L 040415 04/0115 SUB Oil &Grease Report Completion date: 416115 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNQ= Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RI. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RI = Reporting Limit MDL = Method Detection Limit State of California C:DPH ELAP 2661 ppm = parts per million mg/L = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mI/L = millilieters per liter (ppm)

OQA/QC Results Description Run Date Test Method Result Units Difference % Acceptable 15-1869-4 414/2015 Suspended Solids SM 2540D 3160. mg/L Duplicate 15-1869-4 4/4/2015 Suspended Solids Dup. SM 2540D 3060. mg/L < 5% of Average 97% Rec Blank ASTM II water 41412015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2037 141 Suburban Rd, Ste C-I San Luis Obispo CA, 93401 Date/Time Rec'd: 4/8/15 1422 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP

~Sample #Sample Description~ Date / Time Analysis Method Result MDL RL Dil Factor Units Completed I-1 Decant Arm ~418115 1225

-2 Decant Arm 418115 0835 Suspended Solids Settleable Solids SM 2540 D.

SM 2540 F.

Zili 18.

<0.1 2.57 JI 3.

0.1 1 mg/L 1 mL/L 04111115 04108115 SUB Oil & Grease Report Completion date: 411 3/15 Reviewed:

Amanda Smith, Lab Director ND =Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNQ. = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RL. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit

MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm =parts per million mg/L = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

QA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 15-2019-1 4/111/2015 Suspended Solids SM 2540D 138. mg/L Duplicate 15-2019-1 4/111/2015 Suspended Solids Dup. SM 2540D 150. mg/L < 5% of Average 108% Rec Blank ASTM II water 4111/2015 Suspended Solids SM 2540D <3. mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2124 141 Suburban Rd, Ste C-I San Luis Obispo CA, 93401 Date/Time Rec'd: 4/13/15 1405 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWITP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # Sample Description

-1 Decant Arm Date I Time 4113115 0945 Analysis Suspended Solids Method SM 2540 D. -- Result 6.

MDL 2.57 RL 3.

Dil Factor Units Completed 1 mg/L 04/14115

-2 Decant Arm SUB Oil & Grease 4113115 1000 Settleable Solids SM 2540 F.

+ <0.1 0.1 1 mL/L 04113115 Report Completion date: 411 6/15 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNQ = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RI. This result is estimated or qualitative due to matrix b~ackground noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/I = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

OQA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 15-2105-3 411412015 Suspended Solids SM 2540D 103. mg/L Duplicate 15-2105-3 4/14/2015 Suspended Solids Dup. SM 2540D 103. mg/L < 5% of Average Rec 100%

Blank ASTM IIwater 4/14/2015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2347 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 4/22/15 1619 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: James Hampton Project: DCWWTP Sample # Sample Description Date / Time Analysis Method Result MDL RL Dii Factor Units Completed I-1 Decant Arm 4122115 1340 ,Suspended Solids SM 2540 0. 31. 2.57 3. 1 mg/L 04123115

-2 Decant Arm SUB OilI& Grease 4122115 1346 ,Settleable Solids SM 2540 F. 0.5

+ 0.1 1 mL/L 04/22115 Report Completion date: 4124/15 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNQ.= Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RI. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/I = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

QA/QC Results Description Run Date Test Method Result Units Difference % Acceptable 2347-1 4/23/2015 Suspended Solids SM 2540D 31. mg/L Duplicate 2347-1 412312015 Suspended Solids Dup. SM 2540D 29. mg/L < 5% of Average Rec 91%

Blank ASTMlIIwater 4/23/2015 Suspended Solids SM 2540D <3. <3.

mg/L

Abalone Coast Analytical, Inc. Order #: 15-2459 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 4/29/15 1430 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP

Sample #Sample Description~ DatelITime Analysis Method Result MDL RL Di atr Units Completed I-1 Decant Arm 14129115 1042 ISuspended Solids SM 2540 D. 6. 2.57 3. ct 1 mg/L 04/30115

-2 Decant Arm 4129/15 1100 Settleable Solids SM 2540 F. <0.1 0.1 1 mL/L 04/29115 SUB Oil & Grease Report Completion date: 4/30115 Reviewed:

6~ ~A*~ 6~L~

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDI

Result detected below the RL are estimated concentration DNQ = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RI. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RI = Reporting Limit MDI = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/I = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mI/I = millilieters per liter (ppm)

QA/QC Results Description Run Date Test Method Result Units Difference % Acceptable

15-2449-3 123.

4/3012015 Suspended Solids SM 2540D mg/L Duplicate 15-2449-3 4/30/2015 Suspended Solids Dup. SM 2540D 120. mg/L < 5% of Average 97% Rec Blank ASTM IIwater 4/30/2015 Suspended Solids SM 2540D mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2605 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 5/6/15 1341 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # Sample Description Date I Time Analysis Method Result MLJ RL Dil Factor Units Completed

-1 Decant Arm 516115 1210 Suspended Solids SM 2540 D. 4. 3. 1 mg/L 05107/15

-2 Decant Arm SUB Oil & Grease 516115 0816 Settleable Solids SM 2540 F.

+ <0.1 0.1 1 mL/L 05106115 Report Completion date: 517/15 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNQ= Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RL. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/L = milligrams per liter (ppm) Estimated (eat) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

QA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 15-2590-1 5(712015 Suspended Solids SM 2540D 11. mg/L Duplicate 15-2590-1 5/7/2015 Suspended Solids Dup. SM 2540D 11. mg/L <5% of Average 100% Rec Blank ASTM IIwater 51712015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2732 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 5/12/15 1403 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # Sample Descriptions Date/ITime

-1 Decant Arm 15112115 0842 Analysis Suspended Solids Method SM 2540 D.

Result 9.

IMDL I2.57 RL 3.

Dil Factor Units Completed 1 mg/L 05/131.15

-2 Decant Arm 511 2115 0900 Settleable Solids SM 2540 F. <0.1 0.1 1 mL/L 05112/15 SUB Oil &Grease Report Completion date: 5I131315 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RLare estimated concentration DNQ.= Detected, not quantified. This applies to trace values where anaiytes are detected between the MDL and the RL. This resuit is estimated or qualitative due to matrix background noise or values failing below the lowest point of a calibration c:urve.

RL = Reporting Limit MDL = Method Detection Limit State of California C:DPH ELAP 2661 ppm =parts per million mg/L = miliigrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOO may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

QA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 15-2682-2 511312015 Suspended Solids SM 2540D 21. mg/L Duplicate 15-2682-2 5/13/2015 Suspended Solids Dup. SM 2540D 22. mg/L < 5% of Average 104% Rec Blank ASTM IIwater 511312015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2895 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 5/20/15 1410 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # Sample Description Date / Time Analysis Method Result . MDL RL Dil Factor Units Completed

-1 Decant Arm 5120115 1245 ~Suspended Solids SM 2540 D. 10. 2.57 3. i1mg/LI 05/21115

-2 Decant Arm 5/20115 0911 Settleable Solids SM 2540 F. <0.1 0.1 1 mL/L 05120/15 SUB Oil & Grease Report Completion date: 5/22/15 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNQ = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RL. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/L =milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

QA/QC Results Description Run Date Test Method Result Units Difference % Acceptable 2874-1 5/21/2015 Suspended Solids SM 2540D 29. mg/L Duplicate 2874-1 5121/2015 Suspended Solids Dup. SM 2540D 30. mg/L < 5% of Average Rec 102%

Blank ASTMlIIwater 5121/2015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-2990 141 Suburban Rd, Ste C-I San Luis Obispo CA, 93401 Date/Time Rec'd: 5/26/15 1449 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWiTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP

~Sample # Sample Description DatelITime Analysis Method Result MDL RL Dil Factor Units Completed I-1 Decant Arm 5126/15 0858 ISuspended Solids SM 2540 D. 5. 2.57 3. 1 mg/L 05127115

-2 Decant Arm 5126115 0915 Settleable Solids SM 2540 F. <0.1 0.1 1 mL/L 05126115 SUB Oil & Grease Report Completion date: 5128115 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Resuit detected below the RL are estimated concentration DNQ = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RL. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/L = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOO may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

OQA/QC Results Test Method Result Units Difference % Acceptable Description Run Date 15-3005-2 512712015 Suspended Solids SM 2540D 23. mg/L Duplicate 15-3005-2 512712015 Suspended Solids Dup. SM 2540D 26. mgIL < 5% of Average 110% Rec Blank ASTM IIwater 5127/2015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-3129 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 6/2/15 1422 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # Sample Description Date / Time IAnalysis Method Result IMDL RL jDil Factor IUnitsI Completed

-1 Decant Arm *6121t5 1032 Suspended Solids SM 2540 D. 9. 2.57 3. 1 mg/L 06103115

-2 Decant Arm 612115 1045 06102115 ISettleable Solids ISM 2540 F. <0.1 I I 0.1 1lmL/LI SUB Oil &Grease Report Completion date: 6/4115 Reviewed:

6c~?~2 Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RL are estimated concentration DNO. = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RL This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/L = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mL/L = millilieters per liter (ppm)

OQA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 15-3123-2 613I2015 Suspended Solids SM 2540D 22. mg/L Duplicate 15-3123-2 6/3/2015 Suspended Solids Dup. SM 2540D 21. mg/L < 5% of Average 105% Rec Blank ASTM IIwater 61312015 Suspended Solids SM 2540D <3. mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-3317 141 Suburban Rd, Ste C-I San Luis Obispo CA, 93401 Date/Time Rec'd: 6/10/15 1342 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # Sample Description Date / Time Analysis Method Result MDL RL Dil Factor Units Completed I-1 Decant Arm 6110115 0826 iSuspended Solids SM 2540 D. 16. 2.57 3. 1 mg/L 06115115

-2 Decant Arm 6110115 0845 Settleable Solids SM 2540 F. <0.1 0.1 1 mLIL 06/10/15 SUB Oil & Grease Report Completion date: 611 5/15 Reviewed:

~~~gjyLL Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RI are estimated concentration DNQ =Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RI. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RI = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm = parts per million mg/L = milligrams per liter (ppm) Estimated (est) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU = Turbidity Units mI/I = millilieters per liter (ppm)

QA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 15-3305-2 96.

6/15/2015 Suspended Solids SM 2540D mg/L Duplicate 15-3305-2 611 5/2015 Suspended Solids Dup. SM 2540D 92. mg/L < 5% of Average 96% Rec Blank ASTM II water 6/15/2015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-3429 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 6/16/15 1422 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WW~TP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP Sample # ,Sample Description Date / Time Analysis Method Result MDL RL Dil Factor Units Completed I-1 Decant Arm 6116115 1230 Suspended Solids SM 2540 D. 8. 2.57 3. 1 mg/L 06/16/15

-2 Decant Arm SUB Oil & Grease 6/16/15 1245 Settleable Solids SM 2540 F.

+ <0.1 0.1 1 mL/L 06/16/15 Report Completion date: 6/17/15 Reviewed:

Amanda Smith, Lab Director ND = Analyte NOT DETECTED at MDL

Result detected below the RLare estimated concentration DNO. = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RL. This result is estimated or qualitative due to matrix background noise or values falling below the lowest point of a calibration curve.

RL = Reporting Limit MDL = Method Detection Limit State of California CDPH ELAP 2661 ppm =parts per million mg/L = milligrams per liter (ppm) Estimated (eat) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be slighly higher than indicated.

NTU =Turbidity Units mL/L = millilieters per liter (ppm)

QA/QC Results Run Date Test Method Result Units Difference %

Description Acceptable 3390-1 6I1612015 Suspended Solids SM 2540D 28. mg/L Duplicate 3390-1 611612015 Suspended Solids Dup. SM 2540D 29. mg/L < 5% of Average Rec 103%

Blank ASTM IIwater 6/1612015 Suspended Solids SM 2540D <3.

mg/L <3.

Abalone Coast Analytical, Inc. Order #: 15-3536 141 Suburban Rd, Ste C-i San Luis Obispo CA, 93401 Date/Time Rec'd: 6/22/15 1448 Phone: 595-1080 Fax: 595-1080 Diablo Canyon WWTP

Contact:

Jim Wysong 320 Beta Court Phone: 550-1217 Arroyo Grande, CA 93420 Sampler: Jim Wysong Project: DCWWTP t

Sample # Sample Description Date / Time Analysis Method Result MDL RL Di actor Units Completed I-1 Decant Arm 16122115 0909 Suspended Solids SM 2540 D. 9. 2.57 3. 06/23115

-2 Decant Arm 6122/15 0930 Settleable Solids SM 2540 F. <0.1 0.1 06/22/15 SUB Oil &Grease Report Completion date: 6123115 Reviewed:

Amanda Smith, Lab Director ND = Anaiyte NOT DETECTED at MDL

Result detected below the RI are estimated concentration DNO. = Detected, not quantified. This applies to trace values where analytes are detected between the MDL and the RI. This result is estimated or quaiitative due to matrix background noise or values failing below the iowest point of a calibration curve.

RLI Reporting Limit MDL = Method Detection Limit State of Calfornia CDPH ELAP 2661 ppm = parts per million mg/L = miliigrams per liter (ppm) Estimated (eat) results are due to the sample dilutions being too high where the change in dissolved oxygen is such MPN = Most Probable Number that it cannot be accurately quantified. Actual BOD may be siighly higher than indicated.

NTU = Turbidity Units mI/L = millillieters per liter (ppm)

QA/QC Results Description Run Date Test Method Result Units Difference % Acceptable 3526-1 6/23/2015 Suspended Solids SM 2540D 18. mg/L Duplicate 3526-1 6I23/2015 Suspended Solids Dup. SM 2540D 17. mg/L < 5%of Average Rec 94%

Blank ASTM II water 6I23/201 5 Suspended Solids SM 2540D <3.

mg/L <3.

Client Sample Results Client: PG&E Corporation TestAmerica Job ID: 160-12487-2 Project/Site: Diablo Canyon Power Plant Client Sample ID: 001iH U-2 CDRS 2nd Qtr 2015 Composite Lab Sample ID: 160-12487-4 Date Collected: 06117115 10:00 Matrix: Water Date Received: 06125115 08:30 VMethod: 245.1 - Mercury (CVAA) 11.* !

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DiI Fac

_Mercury, ND 0.20 0.080 ug/L 07/15/15 13:01 07/15/15 17:16 1 Client Sample ID: 001 L U-I SGBD 2nd Qtr 2015 Composite Lab Sample ID: 160-12487-5 Date Collected: 06117115 10:00 Matrix: Water Date Received: 06125115 08:30 FMethod: 245.1 - Mercury (CVAA)

Analyte Lercury Result Qualifier ND.

RL 0.20 MDL Unit 0.080 ug/L D Prepared 07/15/15 13:01 Analyzed 07/15/15 17:25 Dil Fac 1 H1 Client Sample ID: 00IL U-2 SGBD 2nd Qtr 2015 Composite Lab Sample ID: 160-12487-6 Date Collected: 06117115 10:00 Matrix: Water LMethod:

Date Received: 06125115 08:30 Analyte Merur 245.1 - Mercury (CVAA)

Result Qlualifier RL MDL Unit 0 Prepared Analyzed DII Fac ND 0.20 0.080 ug/L 07/15/15 13:01 07/15/15 17:28 1 TestAmerica St. Louis Page 12 of 14

Client: PG&E Corporation Client Sample Results TestAmerica Job ID: 160-12487-1 Project/Site: Diablo Canyon Power Plant Client Sample ID: 001H U-I CDRS 2nd Qtr 2015 Composite Lab Sample ID: t60-12487-1 Date Collected: 06/17/15 10:00 Matrix: Water Date Received: 06125/15 08:30 Method: 200.8 - Metals (ICPIMS)

Analyte Result Qualifier RL MDL Uni~t D Prepared Analyzed Dii Faa Silver NO Fl 50 5.0 ug/L 06/30/15 08:29 07103/15 19:25 50 Cadmium 3.3 J Fl 5.0 2.2 ug/L 06/30/15 08:29 07/03/15 19:25 50 Chromium 130 Fl 100 50 ug/L 06/30/15 08:29 07/03/15 19:25 50 Copper 760 "50 " 25 ug/L 06/30/15 08:29 07/03/15 19:25 50 Nickel 56 Fl 50 20 ug/L 06/30/15 08:29 07/03/15 19:25 50 Lead 4.2 J Fl 15 3.0. ug/L 06/30/15 08:29 07/03/15 19:25 50 Zinc ND 1000 140 ug/L 06/30/15 08:29 07/03/15 19:25 50 Client Sample ID: 001D LRW 2ND QTR 2015 COMPOSITE Lab Sample ID: 160-12487-2 Date Collected: 06/17/15 10:00 Matrix: Water Date Received: 06125115 08:30 Method: 200.8 - Metals (ICP/MS)

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac Silver NO 1.0 0.10 uglL 06/30/15 08:29 07/04/15 10:52 1 Cadmium 0.52 0.10 0.043 uglL 06/30/15 08:29 07/04/15 10:52 1 Chromium 1.8 J 2.0 1.0 ug/L 06/30/15 08:29 07/04/15 10:52 1 Copper 8.5 1.0 0.50 Ug/L 06/30/15 08:29 07/04/15 10:52 1 Nickel 2.7 1.0 0.40 ug/L 06/30/15 06:29 07/04/15 10:52 1 Lead 1.3 0.30 0.060 ug/L 06/30/15 08:29 07/04/15 1.0:52 1 Zinc 310 20 2.8 ug/L 06/30/15 08:29 07/04/15 10:52 1

-Method: 245.1 - Mercury (CVAA)

Analyte .Result Qualifier RL MDL Unit D Prepared Analyzed Dii Fac Mercury ND 0.20 0.080 ug/L -- 06/29/15 13:18 06/29/15 18:32 1-Client Sample ID: 001F OWS 2nd Qtr 2015 Composite Lab Sample ID: 160-12487-3 Date Collected: 06/17/15 10:00 L

Matrix: Water Date Received: 06/25/15 08:30 Method: 245.1 - Mercury (CVAA)

AlyeResult Qualifier RL MDL Unit D Prepared Analyzed Dii Fac Mercury ND 0.20 0.060 ug/L 07/15/15 13:01 07/15/15 17:13 1 TestAmerica St. Louis Page 13 of 18

0@@0 BABCOCK Laboratories, Inc.

The Standard ,f E'*dlent?/oI Ove~r /00 flars Client Name: Diablo Canyon Power Plant Analytical Report: Page 2 of 6

Contact:

Rich Dong Project Name: Diablo Canyon Power Plant-C Address: P.O. Box 56-MS Space 104-5-9B Project Number: NPDES/IAvila Beach, CA Avila Beach, CA 93424 Work Order Number: B5D3043 Report Date: 12-May-2015 Received on Ice (Y/N): Yes Temp: 1 °C Laboratory Reference Number B5D3043-01 Sample Description Matrix Sampled Date/Time Received Date/Time Intake Liquid 04/29/15 07:30 04/30/15 10:15 Analyte(s) Result RDL MDL Units Method Analysis Date Analyst Flag Nutrients Ammonia-Nitrogen 0.92 0.10 0.059 mg/L SM4500NH3H 05109115 01:38 JMA Page 2 of 6 P 951 653 3351 CA E.A.P No. 2698 mailing P.O. Box 432 6100 Quail Valley Court F 951 653 1662 EPA no. CA00102 Riverside, CA 92502-0432 location Riverside, CA 92507-0704 www.babcocklabs.com LACSD No., 10119

BABCOCK Laboratories, Inc.

[ke StanardJ*fEcdU',c*fo OverI00Oea*s Client Name: Diablo Canyon Power Plant Analytical Report: Page 3 of 6

Contact:

Rich Dong Project Name: Diablo Canyon Power Plant-C Address: P.O. Box 56-MS Space 104-5-9B Project Number: NPDES /Avila Beach, CA Avila Beach, CA 93424 Work Order Number: B5D3043 0

Report Date: 12-May-2015 Received on Ice (Y/N): Yes Temp: 1 C Laboratory Reference Number B5D3043-02 Sample Description Matrix Sampled Date/Time Received Date/Time

Discharge Liquid 04/29/15 07:41 04/30/15 10:15 Analyte(s) Result RDL MDL Units Method Analysis Date Analyst Flag Nutrients Ammonia-Nitrogen 0.56 0.10 0.059 mg/L SM4500NH3H 05/09/15 01:39 JMA Page 3 of 6 loca tion P 951 653 3351 CA ELAP No. 2698 mail.'ng P.O. Box 432 6100 Quail Valley Court F 951 653 1662 EPA no. CA00 102 Riverside, CA 92502-0432 Riverside, CA 92507-0704 www.babcocklabs.com LACSD No., 10119

aquatic, .

consulting laboratories, inc June 5, 2015 Mr. Jim Kelly PG&E- Diablo Canyon Power Plant 9 Miles NW Avila Beach Avila Beach, CA 93424

Dear Mr. Kelly:

We are pleased to present the enclosed bioassay report. The test was conducted under guidelines prescribed in Guidelines for Performing Static Acute Fish Bioassays in Municipal and Industrial Waste Waters as provided to us by Frederic R. Kopperdahl, Fish and Wildlife Water Pollution Control Laboratory, Department of Fish and Game.

"All acceptability criteria were met and the concentration-response was normal. This is a valid test." Results were as follows:

CLIENT: PG&E- Diablo Canyon Power Plant SAMPLE I.D.: Discharge 001- Acute DATE RECEIVED: 12 May - 2015 AB C LAB. NO.: PGE0515.142 ACUTE ABALONE SURVIVAL BIOASSAY LC50 = 100 % Survival inl100% Sample TUa = 0.00 SLabortoryo~ Di*rect or*_

29 north olive st. ventura, ca 93001 (805) 643 5621 wwvw.aquabio.org

Repo rt Date: 04 Jun-16 10:04 (p 1 of 1)

CETI SoummedAaryoRepSurtia Test Code: PGE0515.142 ]04-6338-1 822 96 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.

Batch ID: 09-4151-7635 Test Type: Survival (96h) Analyst:

Start Date: 12 May-15 15:34 Protocol: Kopperdahl (1976) Diluent: Laboratory Seawater Ending Date: 16 May-15 14:40 Species: Haliotis rufescens Brine: Not Applicable Duration: 95h Source: Cultured Abalone Age:

Sample ID: 11-0966-5383 Code: PGEO515.142 Client: Pacific Gas & Electric Co.

Sample Date: 11 May-15 07:30 Material: Sample Water Project:

Receive Date: 12 May-15 10:15 Source: Bioassay Report Sample Age: 32h (5.2 =0) Station: Discharge 001- Acute Comparison Summary Analysis ID Endpoint NOEL LOEL TOEL PMSD TU Method 19-3122-2398 96h Survival Rate 100 >100 NA NA 1 Equal Variance t Two-Sample Test Point Estimate Summary AnalysislID Endpoint Level % 95% LCL 95% UCL TU Method 06-0437-8723 96h Survival Rate EC5 >100 N/A N/A <1 Linear Interpolation (IOPIN)

EC10 >100 N/A N/A <1 EC15 >100 N/A N/A <1 EC20 >100 N/A N/A <1 EC25 >100 N/A N/A <1 EC40 >100 N/A N/A 100 N/A N/A <1 96h Survival Rate Summary C-% Control Type Count Mean 96% LCL 95% UCL Mmn Max Std Err Std Dev CV% %Effect 0 Negative Control 2 1 1 1 1 1 0 0 0.0% 0.0%

100 2 1 1 1 1 1 0 0 0.0% 0.0%

96h Survival Rate Detail C-% Control Type Rep I Rep 2 0 Negative Control 1I 100 1 1 96h Survival Rate Binomials

-%Control Type Rep I Rep 2 0 Negative Control 10/10 10/10 100 10/10 10/10 000-055-186-3 vl .8.7.11 000-55-16-3CETISTM *Analyst: ._*]*,. QA:___*

CETIS Analytical Report Report Date: 04 Jun-15 10:04 (p 1 of 1)
Test Code: PGE0515.142 I 04-6338-1822 96 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 19-3122-2398 Endpoint: 96h Survival Rate CETIS Version: CETiSvI.8.7I Analyzed: 04 Jun-15 10:03 Analysis: Parametric-Two Sample Official Results: Yes Data Transform Zeta Alt Hyp Trials Seed Test Result Angular (Corrected) NA C> T NA NA Passes 96h survival rate Equal Variance t Two-Sample Test SControl vs C-% Test Stat Critical MSD DF P-Value P-Type Decision(a:5%)]
SNegative Control 100 0 2.92 2 1.0000 CDF Non-Significant Effect ANOVA Table Source Sum Squares Mean Square DF F Stat P-Value Decision(a:5%)
Between 0 0 1 65540 <0.0001 Significant Effect Error 0 0 2 Total 0 3 96h Survival Rate Summary 0_-%Control Type Count Mean 95% LCL 95% UCL Median MIn Max std Err CV% %Effect 0 Negativeu Control 2 1 1 1 1 1 1 .0 0.0% 0.0%
1100 2 1 1 1 1 1 1 0 0.0% 0.0%
Angular (Corrected) Transformed Summary C-% Control Type .Count Mean 95% LCL 95% UCL Median MIn Max Std Err CV% %Effect 0 Negative Contr 2 1.412 1.409 1.415 1.412 1.412 1.412 0 0.0% 0.0%
100 2 1.412 1.409 1.415 1.412 1.412 1.412 0 0.0% 0.0%
96h Survival Rate Detail C-% Control Type' Rep I Rep 2 0 Negative Control 1 1 100 1 1 SAngular (Corrected) Transformed Detail
-%Control Type Rep I Rep 2 0 Negative Control 1.412' 1.412 100 1.412 1.412 96h Survival Rate Binomials C-% Control Type Rep I Rep 2 0Negative Control 10110 10110
.100 10/10 10/10 Graphics LO 1.010'00 0.9 C 0.,II 0.4 q0-02 0.2 0.0 0.0 - I O0E400 S .
0N 100 -1.0 -1.0 -.0. 0.,0 0.5 1.0 1.5 C-9001015*
I) 000-055-186-3 v1 .8.7.11 000-55-16-3CETISTM Analyst:______
CETIS Analytical Report Report Date: 04 Jun-15 10:04 (p 1 of 1)
Test Code: *PGE0515.;142 I 04-6338-1 822 96 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 06-0437-8723 Endpoint: 96h Survival Rate CETiS Version: CETISvl .8.7 Analyzed: 04 Jun-15 10:03 Analysis: Linear Interpolation (ICPIN) Official Results: Yes Linear interpolation Options X Transform Y Transform Seed Resamples Exp 95% CL Method Linear Linear 0 280 Yes Two-Point Interpolation Point Estimates Level % 95% LCL 95% UCL TU 95% LCL 95% UCL EC5 >100 N/A N/A <1 NA NA ECI0 >100 NIA N/A <1 NA NA ECl15 >100 N/A N/A <1 NA NA EC2O >100 N/A N/A <1 NA NA EC25 > 100 N/A N/A <1 NA NA EC40 >100 N/A N/A <1 NA NA EC50 > 100 N/A N/A <1 NA NA 96h Survival Rate Summary Calculated Variate(A/B)
C-% Control Type Count Mean Min Max Std Err Std Dev CV% %Effect A B 0 Negative Control 2 1 1 1 0 0 0.0% 0.0% 20 20 100 2 1 1 .1 0 0 0.0% 0.0% 20 20 96h Survival Rate Detail C% Control Type Rep 1 Rep 2 0 Negative Control 1 1 100 1 1 96h Survival Rate Binomlias C-% Control Type Rep 1 Rep 2 0 Negative Control 10/10 10/10 100 10/10 10(10 Graphics 1.0!
Os 0.7 0.0 0.2 0.0 0 20 40 , 60 00 III 000-55-186-3Analyst:.
,,' QA:_____
000-055-186-3 CETISTM vl.8.7.11
Report Date: 04 Juna15 10:04 (p 1 of 1)
CETIS Measurement Report Test Code: PGE0515.142 04-6338-1822 95 Hour Red Abalone Survival Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 09-4151-7635 Test Type: Survival (96h) Analyst:
Start Date: 12 May-15 15:34 Protocol: Kopperdahl (1976) Dlluent: Laboratory Seawater Ending Date: 16 May-15 14:40 Species: Haliotis rufescens Brine: Not Applicable Duration: 95h Source: Cultured Abalone Age:
Sample ID: 11-0966-5383 Code: PGE0515.142 Client: Pacific Gas & Electric Co.
Sample Date: 11 May-15 07:30 Material: Sample Water Project:
Receive Date: 12 May-15 10:15 Source: Bioassay Report Sample Age: 32h (5.2 0C) Station: Discharge 001- Acute Dissolved Oxygen-mglL
-%Control Type Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 Negative Contr 10 6.96 6.677 7.243 6.4 7.6 0.1249 0.395 5.68% 0 100 10 7.62 7.409 7.631 7.3 7.8 0.04899 0.1549 2.06% 0 Overall 20 7.24 6.4 7.8 0 (0%)
pH-Units C-% Control Type Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 Negative Contr 10 7.37 7.294 7.446 7.3 7.6 0.0335 0.1059 1.44% 0 100 10 7.42 7.375 7.465 7.3 7.5 0.02 0.06325 0.85% 0 Overall 20 7.395 7.3 7.6 0 (0%)
Sallnity-ppt CControl Type Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 Negative Contr 10 34 34 34 34 34 0 0 0.0% 0 100 10 34 34 34 34 34 0 0 J 0.0% 0 Overall 20 34 34 34 0 (0%)
Temperature-0 C C-% Control Type Count Mean 95% LCL 95% UCL MIn Max Std Err Std Dev CV% QA Count o Negative Contr 10 14.59 14.24 14.94 14.2 15.6 0.1545 0.4886 3.35% 0 100 10 14.48 14.36 14.6 14.1 14.7 0.05121. 0.1619 1.12% 0 Overall 20 14.54 14.1 15.6 0 (0%)
Dissolved Oxygen-mglL C-% Control Type 1 2 3 4 5 6 7 8 9 10 0 Negative Contr 6.4 6.6 7 6.8 7 6.5 7.6 7.4 7 7.3 100 7.3 7.4 7.5 7.4 7.5 7.4 7.8 7.6 7.6 7.7 pH-Units CControl Type 1 2 3 4 5 6 7 8 9 10 0 Negative Contr 7.5 7.6 7.3 7.3 7.3 7.3 7.3 7.3 7.4 7.4 100 7.5 7.5 7.4 7.4 7.3 7.4 7.4 7.4 7.4 7.5 Salinity-ppt C-%/ Control Type 1 2 3 4 5 6 7 8 9 10 0 Negative Contr 34 34 34 34 34 34 34 34 34 34 100 34 34 34 34 34 34 34 34 34 34 Temperature-°C CControl Type 1 2 3 4 5 6 7 8 9 10 0 N egative Contr 15.4 15.6 14.4 14.5 14.3 14.2 14.3 14.4 14.4 14.4 100 14.4 14.1 14.5 14.5 14.4 14.6 14.7 14.6 14.5 14.5 TM 000-055-186-3 v1 .8.7.11 000-55-186-3CETIS Analyst: *{'*J QA: F
aquatic ~
laboratories, inc June 5, 2015 Mr. Jim Kelly PG&E- Diablo Canyon Power Plant 9 Miles NW Avila Beach Avila Beach, CA 93424
Dear Mr. Kelly:
We are pleased to present the enclosed bioassay report. The test was conducted under guidelines prescribed in Short-Term Methods for Measuring the Chronic Toxicity of Effluents and Receiving Waters to West Coast Marine and Estuarine Organisms, EPA-R-95/136. "All acceptability criteria were met and the concentration-response was normal.
This is a valid test." Results were as follows:
CLTENT: PG&E- Diablo Canyon Power Plant SAMPLE I.D.: Discharge 001 DATE RECEIVED: 12 May - 2015 ABC LAB. NO.: PGE0515.143 CHRONIC ABALONE LARVAL DEVELOPMENT BIOASSAY NOEC = 100.00 %
TUc = 1.00 EC25 = >100.00 %
EC50O >100.00 %
Your e y, scott Jo *son '
Laboratory Direct~r 29 north olive st. ventura, ca 93001 (805) 643 5621 www.aquabio.org
CETIS Summary Report Report Date:
Test Code:
04.Jun-15 09:49 (p 1 of 1)
PGE0515.143abs I01-7510-2626 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 19-1085-7063 Test Type: Development Analyst:
Start Date: 12 May-i5 13:34 Protocol: EPA/6001R-95/1 36 (1995) Diluent: Laboratory Seawater Ending Date: 14 May-I5 14:00 Species: Haliotis rufescens Brine: Not Applicable Duration: 48h ~ Source: Cultured Abalone Age:
Sample ID: 15-3255-6323 Code: PGE0515.143a Client: Pacific Gas & Electric Co.
Sample Date: 11 May-I15 07:30 Materal: Sample Water Project: Toxicity Testing Receive Date: 12 May-15 10:15 Source: Bioassay Report Sample Age: 30h (5.2 °C) Station: Discharge 001 Comparison Summary Analysis ID Endpoint NOEL LOEL TOEL PMSD TU Method 10-0345-4308 Proportion Normal 100 >100 NA NA 1 Fisher Exact Test Point Estimate Summary AnalysislID Endpoint Level % 95% LCL 95% UCL Tru Method 17-6414-3938 Proportion Normal EC5 >100 N/A NIA <1 Linear Interpolation (ICPIN)
ECI0 >100 N/A NIA <1 EC15 >100 N/A NIA <1 EC20 >100 N/A NIA <1 EC25 >100 N/A N/A <1 EC40 >100 N/A N/A <1 EC50 >100 N/A N/A <1 Test Acceptability Analysis ID Endpoint Attribute Test Stat TAC Limits Overlap Decision 10-0345-4308 Proportion Normal Control Resp 1 0.8- NL Yes Passes Acceptability Criteria 17-6414-3938 Proportion Normal Control Resp 1 0.8 - NL Yes Passes Acceptability Criteria Proportion Normal Summary C-% Control Type Count Mean 95% LCL 95% UCL Mmn Max Std Err Std Dev CV% %Effect
0. Negative Control 5 1 1 1 1 1 0 0 0.0% 0.0%
10 5 1 1 1 1 1 0 0 0.0% 0.0%
18 5 1 1 1 1 1 0 0 0.0% 0.0%
32 5 1 1 1 1 1 0 0 0.0% 0.0%
56 5 1 1 1 1 1 0 0 0.0% 0.0%
100 .5 1 1 1 1 1 0 0 0.0% 0.0%
Proportion Normal Detail
-%Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 1 1 1 1 1 10 1 1 1 1 1 18 1 1 1 1 1 32 1 1 1 1 1 56 1 1. 1 1 1 100 1 1 1 1' 1 Proportion Normal Binomials C-% Control Type Repit Rep 2 Rap 3 Rep 4 Rap 5 0 Necative Control 100/100 100/100 100/100 100/100 100/100 10 100/10 100/100 100/100 100/100 100/100 18 100/100 100/1100 100/100 100/1 00 100/100 32 100/100 100/1 00 100/1 00 100/1 00 100/100 56 100/100 100/1 00 100/1 00 100/1 00 100/100 100 100/100 100/1 00 100/1100 100/1 00 100/100
.00-5518-6Analyst:__
- C'*
A:___*
.000-055-186-6 CETISTM vl.8.7.11
CETIS AnalYtical Rel~ort Report Date: 04 Jun-15 09:49 (p 1 of 2)
Test Code: PGE0515.143abs I 01-7510-2626 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
AnalysislID: 17-6414-3938 EndpoInt: Proportion Normal CETIS Version: CETiSvl.8.7 Analyzed: 04 Jun-15 9:48 Analysis: LinearlInterpolation (ICPIN) Official Results: Yes Linear Interpolation Options X Transform Y Transform Seed Resamples Exp 95% CL Method Linear Linear 0 280 Yes Two-Point Interpolation Point Estimates Level % 95% LCL 95% UCL TU 95% LCL 95% UCL EC5 >100 N/A N/A <1 NA NA ECI10 >100 N/A N/A <1 NA NA EC15 >100 N/A NIA <1 NA NA EC20 >100 N/A N/A <1 NA NA EC25 >100 N/A N/A <1 NA NA EC40 >100 N/A N/A <1 NA NA EC50 >100 N/A N/A <1 NA NA Proportion Normal Summary Calculated Varlate(ANB)
C% Control Type Count Mean MIn Max Std Err Std 0ev CV% %Effect A B 0 Negative Control 5 1 1 1 0 0 0.0% 0.0% 600 500 10 5 1 1 1 0 0 0.00/ 0.0% 500 500 18 5 1 1 1 0 0 0.0% 0.0% 500 500 32 5 1 1 1 0 0 0.0% 0.0% 500 500 56 5 1 1 1 0 0 0.0% 0.0% 500 500 100 5 1 1 1 0 0 0.0% 0.0% 500 500 Proportion Normal Detail
-% Control Type Rep 1 Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 1 1 1 1 1 10 1 1 1 1 1 18 1 1 1 1 1 32 1 1 1 1 1 56 1 1 1 1 1 100 1 1 1 1 1 Proportion Normal Binomials C-% Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 100/100 100/1 00 100/1 00 100/100 100/100 10 100/100 100/100 100/100 100/100 100/100 18 100/100 100/100 100/100 100/100 100/100 32 100/100 100/100 100/100 100/100 100/100 56 100/100 100/100 100/100 100/100 100/100 100 100/100 100/100 100/100 100/100 100/100 000-055-186-3 CETISTM v1 .8.7.11 Anls:. -Q:* _
Report Date: 04 Jun-i 509:49 (p 2 of 2)
CETIS Analytical Report Test Code: PGE0515.143abs j01-7510-2626 Aquatic Bloassay & Consulting Labs, Inc.
I Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.]
Red Abalone Larval Development TestEndpoint: Proportion Normal CETIS Version: CETISvi.B.7 An.alysis ID: 1-4433 Analysis: Linear Interoolatlon i
(ICPIN*
l r Official Results: Yes lI ...... * .... .. ... . ...... * ....
Graphics
.+g 0.fl 018 S0.4 0,1 0 20 40 0I 00 100 000 863 *,_J'\,*
CTIS vi.8..11Analyst:
QA:
000-055-186-3 CETISTM v1.8.7.11
Report Date: 04 Jun-15 09:49 (p 1 of 1)
CETIS Analytical Report Test Code: PGEO515.143abs I 01-7510-2626 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 10-0345-4308 Endpoint: Proportion Normal CETIS Version: CETISvl.8.7 Analyzed: 04 Jun-15 9:48 Analysis: Singlle 2x2 Contingency Table Official Results: Yes Data Transform Zeta Alt Hyp Trials Seed NOEL LOEL TOEL TU Untransformed C> T NA NA 100 >100 NA 1 Fisher Exact Test Control vs C-% Test Stat P-Value P-Type Declsion(a:5%)
Negative Control 10 1 1.0000 Exact Non-Significant Effect 18 1 1.0000 Exact Non-Significant Effect 32 1 1.0000 Exact Non-significant Effect 56 1 1.0000 Exact Non-Significant Effect 100 1 1.0000 Exact Non-Significant Effect Data Summary
-%Control Type NR R NR + R Prop NR Prop R %Effect 0 Negative Contr 500 0 500 1 0 0.0%
10 500 0 500 1 0 0.0%
18 500 0 500 1 0 0.0%
32 500 0 500 1 0 0.0%
56 500 0 500 1 0 0.0%
100 500 0 500 1 0 0.0%
Proportion Normal Detail C-% Control Type Rep t Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 1 1 1 1 1 10 1 1 1 1 1 18 1 1 1 1 1 32 1 1 1 1 1 56 1 1 1 1 ~ I 100 1 1 1 1 1 Proportion Normal Binomials
-%Control Type Rep 1" Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 100/100 100/100 1001/100 100/100 100/100 10 100/100 1001100 100/100 100/100 100/100 18 100/100 100/100 100/100 1001100 100/100 32 100/100 100/100 100/100 100/100 100/100 56 100/100 100/100 100/100 100/100 100/100 100 1001100 100/100 100/100 100/100 100/100 Graphics 1.0 0 S 0.9 0.8 0.7 0.6
-e 0.9 0.3 0.2 0.0 III 00 0 00 32 06 100 000-055-186-3 CETISTM vl.8.7.11
CETIS Measurement Report Report Date:
Test Code:
04 Jun-15 09:49 (p 1 of 2)
PGEO5I5.I43abs I 01-7510-2626 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 19-1065-7053 Test Type: Development Analyst:
Start Date: 12 May-15 13:34 Protocol: EPAI600IR-951136 (1995) Diluent: Laboratory Seawater Ending Date: 14 May-15 14:00 Species: Hallotis rufescens Brine: Not Applicable Duration: 48h Source: Cultured Abalone Age:
Sample ID: 15-3255-6323 Code: PGE0515.143a Client: Pacific Gas & Electric Co.
Sample Date: 11 May-15 07:30 Material: Sample Water Project: Toxicity Testing Receive Date: 12 May-i5 10:15 Source: Bioassay Report Sample Age: 30h (6.2 °C) Station: Discharge 001 Parameter Acceptability Criteria Parameter Min Max Acceptability Limits Overlap Decision Salinity-ppt 34 34 32 - 36 Yes Results Within Limits Temperature-°C 14.1 14.3 14 - 16 Yes Results Within Limits Dissolved Oxygen-mg/L
-%Control Type Count Mean 95% LCL 95% UCL Mmn Max Std Err Std Dev CV% QA Count 0 Negative Contr 2 6.75 -2.78 16.28 6 7.5 0.75 1.061 15.71% 0
10. 2 6.5 -4.936 17.94 5.6 7.4 0.9 1.273 19.58% 0 18 2 6.3 -8.947 21.55 5.1 7.5 1.2 1.697 26.94% 0 32 2 6.35 -8.262 20.96 5.2 7.5 1.15 1.626 25.61% 0 56 2 6.1 -11.69 23.89 4.7 7.5 1.4 1.98 32.46% 0 100 2 6.7 -3.465 16.86 5.9 7.5 0.8 1.131 16.89% 0 Overall 12 6.45 4.7 7.5 0 (0%)
pH.U nits 0%Control Type Count Mean 95% LCL 95% UCL Mmn Max Std Err Std Dev CV% QA Count O Negative Contr 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 10 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 18 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 32 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 56 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 100 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 Overall 12 7.85 7.8 7.9 0 (0%)
Salinity-ppt CControlIType Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 Negative Contr 2 34 34 34 34 34 0 0 0.0% 0 10 2 34 34 34 34 34 0 0 0.0% 0 18 2 34 34 34 34 34 0 0 0.0% 0 32 2 34 34 34 34 34 0 0 0.0% 0 56 2 34 34 34 34 34 0 0 0.0% 0 100 2 34 34 34 34 34 0 0 0.0% 0 Overall 12 34 34 34 0 (0%)
Tern perature-°C
-%ControlIType Count Mean 95% LCL 95% UCL Mmn Max Std Err Std Dev CV% QA Count 0 NegatIve Contr 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 10 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 18 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 32 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 56 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 100 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 Overall 12 14.2 14.1 14.3 0 (0%)
000-055-186-6 ~~CETISTM v1 .8.7.11Anys:____
000-055-186-6 An alyst:,_*_.__*QA:_*
Report Date: 04 Jun-16 09:49 (p 2 of 2)
CETIS Measurement Report Test Code: PGE0515.143abs I 01-7510-2626 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Dissolved Oxygen-mg/L C.% Control Type 1 2 0 Negative Contr 7.5 6 10 7.4 5.6 18 7.5 5.1 32 7.5 5.2 56 7.5 4.7 100 7.5 5.9 pH-Units C-% Control Type 1 2 0 Negative Contr 7.9 7.8 10 7.9 7.8 18 7,9 7.8 32 7.9 7.8 56 7.9 7.8 100 -7.9 7.8 Salinlty-ppt C-% Control Type 1 2 0 Negative Contr 34 34 10 34 34 18 34 34 32 34 34 56 34 34 100 34 34 Tern perature-°C C-% Control Type t 2 0 Negative Contr 14.1 14.3 10 14.1 14.3 18 14.1 14.3 32 14.1 14.3 56 14.1 14.3 100 14.1 14.3 000-055-186-6 86-6~CE-TISTM vl .8.7.11Anyt:____
000-055-1 Analyst:. *'*: P
CHAIN OF CUSTODY RECORD Client: Project Name/Number: Analysis Pacific Gas & Electric Co Toxicity Testing Address: Project Mgr:
9 Miles NW Avila Beach Jim Kelly Avila Beach, Ca. 93424 P.O. #"
.9 .2 0 0
____(805) 545-3194 , . _ I-Phon Nuber -* * " .9 I-1 I.-
oE -.9 Volume / 4: 2 Date Time Matrdx Sample ID Number Comments 03 5/11/2015 511112015 a ?23 V?3 5 X _
X Seawater
_Seawater Dischargle 001 Dischargle 001 42615 gal 4271,1, gal X
- X I_ ________
--- M*3-- 1 Relinquished By:(srgnature) "*,/.-, - f*,i 4*'.JCk Date / Time Relinquished By: (signature) Date / Time Received By:(signature) Date / Time Received By:(signature) Date I Time
" iQ
-'&* t* [J Temperature upon samnple receipt: degrees C Consulting Labortories Aquatic
-29 N. Olive Street and Bioassay Ventura, Ca. 93001 Phone: (805) 643-5621 Fax: (805) 643-2930
aquatic*,
laboratories, inc CHRONIC ABALONE DEVELOPMENT BIOASSAY DATE: 12 May 2015 STANDARD TOXICANT: Zinc NOEC = 56.00 ug/1 EC25 = 66.19 ug/l EC50 = 77.46 ug/1 Yours very truly,.
Scott Johnson Laboratory Director 29 north olive st. ventura, ca 93001 (805) 643 5621wwaqbior www.aquabio.org
Report Date: 04 Jun-15 09:33 (p 1 of 1)
CETIS Summary Report Test Code: ABS051215 ] 15-5178-2921 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 12-4467-1331 Test Type: Development Analyst:
Start Date: 12 May-I15 13:30 Protocol: EPA/600/R-95/136 (1995) Diluent: Laboratory Seawater Ending Date: 14 May-15 14:00 Species: 1-aliotis rufescens Brine: Not Applicable Duration: 49h Source: Cultured Abalone Age:
Sample ID: 17-7724-2730 Code: ABS051215a Client: Internal Lab Sample Date: 12 May-15 13:30 Material: Zinc Project: "REF TOX Receive Date: Source: Reference Toxicant Sample Age: NA Station: REF TOX comparison Summary Analysis ID Endpoint NOEL LOEL TOEL PMSD TU Method 17-1674-8585 Proportion Normal 56 100 74.83 2.11% Steel Many-One Rank Sum Test Point Estimate Summary AnalysislID Endpoint Level lI~gIL 95% LCL 95% UCL TU Method 14-3861-1439 Proportion Normal EC5 57.17 44.41 58.71 Linear Interpolation (ICPIN)
EC10 59.43 56.28 60.89 EC15 61.68 58.71 63.06 EC2O 63.93 61.14 65.23 EC25 66.19 63.57 67.41 EC40 72.95 70.85 73.92 ECSO 77.46 75.71 78.27 Test Acceptability Analysis ID Endpoint Attribute Test Stat TAC Limits Overlap Decision 14-3861-1439 Proportion Normal Control Resp 1 0.8 - NL Yes Passes Acceptability Criteria 17-1674-8585 Proportion Normal Control Resp 1 0.8 - NL Yes Passes Acceptability Criteria 17-1674-8585 Proportion Normal NOEL 56 NL -56 No Above Acceptability Criteria 17-1674-8585 Proportion Normal PMSD 0.021 07 NL - 0.2 No Passes Acceptability Criteria Proportion Normal Summary C-jig/L ControlIType Count Mean 95% LCL 95% UCL Mmn Max Std Err Std Dev CV% %Effect 0 Negative Control 5 1 1 1 1 1 0 0 0.0% 0.0%
18 5 1 1 1 1 1 0 0 0.0% 0.0%
32 5 1 1 1 1 1 0 0 0.0% 0.0%
56 5 0.976 0.9094 1 0.88 1 0.024 0.05367 5.5% 2.4%
100 5 0 0 0 0 0 0 0 100.0%
180 5 0 0 0 0 0 0 0 100.0%
Proportion Normal Detail C-gI~gL Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 1 1 1 1 1 18 1 1 1 1 1 32 1 1 1 1 1 56 1 1 1 0.88 1 100 0 0 0 0 0 180 0 0 0 0 0 Proportion Normal Binomials C-pg/L Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 NegatIve Control 100/100 100/100 100/100 100/100 100/100 18 100/100 100/100 100/100 100/100 100/100 32 1001100 100/100 1001100 100/100 100/100 56 100/100 100/100 100/100 88/100 1001100 100 01100 0/100 0/100 0/100 0/100 180 0/1 00 0/100 0/1 00 0/100 0/1 00 000-055-186-6 CETISTM vl.8.7.11 K/
000-05-18-6CTIS~
i .87.11Analyst:.
QA:________
CETIS Analytical Report Report Date:
Test Code:
04 Jun-15 09:33 (p1 of 2)
ABS051215 I 15-5178-2921 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 17-1 674-8585 Endpolnt: Proportion Normal CETIS Version: CETISvI.8.7 Analyzed: 04 Jun-15 9:33 Analysis: Nonparametric-Control vs Treatments Official Results: Yes Data Transform Zeta Alt Hyp Trials Seed PMSD NOEL LOEL TOEL TU Angular (Corrected) NA C> T NA NA 2.11% 56 100 74.83 Steel Many-One Rank Sum Test Control vs C-pglL Test Stat Critical Ties DF P-Value P-Type Decision(a:5%)
Negative Control 18 27.5 17 1 8 0.7500 Asymp Non-Significant Effect 32 27.5 17 1 8 0.7500 Asyrnp Non-Significant Effect 56 25 17 1 8 0.5314 Asymp Non-Significant Effect ANOVA Table Source Sum Squares Mean Square DF F Stat P-Value Declsion(a:5%)
Between 0.01 383694 0.004612315 3 1 0.41 82 Non-Significant Effect Error 0.07379703 0.004612315 16 Total 0.08763397 19 Distributional Tests Attribute Test Test Stat Critical P-Value Declsion(a:1%)
Variances Mod Levene Equality of Variance 1 5.953 0.4262 Equal Variances Variances Levene Equality of Variance 7.111 *5.292 0.0030 Unequal Variances Distribution Shapiro-Wilk W Normality 0.4969 0.866 <0.0001 Non-normal Distribution Distribution Kolmogorov-Smirnov D 0.45 0.2235 <0.0001 Non-normal Distribution Distribution D'Agostino Skewness 4.576 2.576 <0.0001 Non-normal Distribution Distribution D'Agostino Kurtosis 4.175 2.576 <0.0001 Non-normal Distribution Distribution D'Agostino-Pearson K2. Omnibus 38.38 9.21 <0.0001 Non-normal Distribution Distribution Anderson-Darling A2 Normality 4.585 3.878 <0.0001 Non-normal Distribution Proportion Normal Summary C-pg/L ControlIType Count Mean 95% LCL 95% UCL Median Mmn Max Std Err CV% %Effect 0 Negative Control 5 1 1 1 1 1 1 0 0.0% 0.0%
18 5 1 1 1 1 1 1 0 0.0% 0.0%
32 5 1 1 1 1 1 1 0 0.0% 0.0%
56 5 0.976 0.9094 1 1 0.88 1 0.024 5.5% 2.4%
100 5 0 0 0 0 0 0 0 100.0%
180 5 0 0 0 0 0 0 0 . 100.0%
Angular (Corrected) Transformed Summary C-pglL ControlIType Count Mean 95% LCL 95% UCL Median Mmn Max Std Err CV% %Effect 0 Negative Contr 5 1.521 1.521 - 1.521 1.521 1.521 1.521 0 0.0% 0.0%
18 5 1.521 1.521 1.521 1.521 1.521 1.521 0 0.0% 0.0%
32 5 1.521 1.521 1.521 1.521 1.521 1.521 0 0.0% 0.0%
56 5 1.46 1.291 1.629 1.521 1.217 1.521 0.06074 9.3% 3.99%
100 5 0.05002 0.05001 0.05003 0.05002 0.05002 0.05002 0 0.0% 96.71%
180 5 0.05002 0.05001 0.05003 0.05002 0.05002 0.05002 0 0.0% 96.71%
Proportion Normal Detail C-iglL Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 1 1 1 1 1 18 1 1 1 1 1 32 1 1 1 1 1 56 1 1 1 0.88 1 100 0 0 0 0 0 180 0 0 0 0 0 000-055-1 86-3 CETISTV vl.8.7.11 Analyst: X....Ž "t QA:_
Report Date: 04 Jun-15 09:33 Cp2 of 2)
CETIS Analytical Report Test Code: ABS051215I 15-5178-2921 Red Abalone Larval Development Test Aquatic Btoassay & Consulting Labs, Inc.
Analysis ID: 17-1674-8585 Endpoint: Proportion Normal CETIS Version: CETISv1.8.7 Analyzed: 04 Jun-15 9:33 Analysis: Nonparametric-Control vs Treatments Official Results: Yes Angular (Corrected) Transformed Detail C-pg/L Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5
0 Negative Control 1.521 1.521 1.521 1.521 1.521 118 1.521 1.521 1.521 1.521 1.521 32 1.521 1.521 1.521 1.521 1.521 56 1.521 1.521 1.521 1.217 1.521 100 0.05002 0.05002 0.05002 0.05002 0.05002 180 0.05002 0.05002 0.05002 0.05002 0.05002 Proportion Normal Binomaias C-psglL Controi Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 100/100 100/100 100/100 1001100 100/100 18 100/100 100/100 100/100 100/100 100/100 32 100/100 100/100 100/100 100/100 100/100 56 100/100 100/100 100/100 88/100 100/100 100 0/100 0/100 0/100 0/100 01100 180 0/100 0/100 0/100 0/100 0/100 Graphics 1.0
0.10 0.9 0.10 00.0 0.4
-0.10 0.3
-0.10 0.2
-0.20 0.1 0.0 I .0,.0I 0I I 00f 10 30 00 000 100 -. ,5 -2.0 15 "l10 0,5 0.0 0.0 1.0 1.1 0.0 2.0
<-t 1 "*QA:
000-55-16-3CETI~
v.8..11Analyst: (9 000-055-186-3 CETISTM v1.8.7.11
CETIS Analytical Report Report Date: 04 Jun-15 09:33 (p 1 of 2)
Test Code: ABS051215 I 15-5178-2921 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Analysis ID: 14-3861-1439 Endpoint: Proportion Normal CETIS Version: CETISvl.8.7 Analyzed: 04 Jun-15 9:33 Analysis: Linear Interpolation (ICPIN) Official Results: Yes Linear interpolation Options X Transform Y Transform Seed Resamples Exp 96% CL Method Linear Linear 0 280 Yes Two-Point Interpolation Point Estimates Level pig/L 95% LCL 95% UCL EC5 57.17 44.41 58.71 ECl0 59.43 56.28 60.89 EC15 61.68 58.71 63.06 EC20 63.93 61.14 65.23 EC25 66.19 63.57 67.41 EC4O 72.95 70.85 73.92 EC50 77.46 75.71 78.27 Proportion Normal Summary Calculated Varlate(A/B)
C-gI~gL Control Type Count Mean Mmn Max Std Err Std Dev CV% %Effect A B 0 Negative Control 5 1 1 1 0 0 0.0% 0.0% 500 500 18 5. 1 1 1 0 0 0.00/ 0.0% 500 500 32 5 1 1 1 0 0 0.0%h 0.0% 500 500 56 5 0.976 0.88 1 0.024 0.05367 5.5% 2.4% 488 500 100 5 0 0 0 0 0 100.0% 0 500 180 5 0 0 0 0 0 100.0% 0 500 Proportion Normal Detail C-pg/L Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 1 1 1 1 1 18 1 1 1 1 1 32 1 1 1 1 1 56 1 1 1 0.88 1 100 0 0 0 0 0 180 0 0 0 0 0 Proportion Normal Binomials C-pglL Control Type Rep I Rep 2 Rep 3 Rep 4 Rep 5 0 Negative Control 100/100 1001100 100/100 100/100 100/100 18 100/100 100/100 100/100 1001100 100/100 32 100/100 100/100 100/100 100/100 100/100 56 100/100 100/100 100/100 88/100 100/100 100 0/100 0/100 0/100 0/100 0/100 180 0/100 0/100 0/100 0/100 01100 000-055-186-3 CETISTM v1 .8.7.11 Analyst:_____ QA:____
Report Date: 04 Jun-15 09:33 (p 2 of 2)
CETIS Analytical Report Test Code: ABS051215 ] 15-5178-2921 SRed Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
IAnalysislID: 14-3861-1439 Endpolnt: Proportion Normal CETIS Version: CETISv1.8.7 IAnalyzed: 04 Jun-I 5 9:33 Analysis: Linear Interpolatiori (IIPIN) Official Results: Yes Graphics I.0 0.9 0.8 0.0.7 0.4 0.3 0.2 0.I 0.0 v = L. . . . .1. .
0 0 40 60 00 100 100 040 1&0 060 C~pgjL 000-055-186-3 ~CETISTM 000-055-186-3 vil.8.7.11 Aayt___
Ana yst:. '*'N/QA:*__.
Report Date: 04 Jun-15 09:33 (p 1 of 2)
CETIS Measurement Report Test Code: ABSO51215 I 15-5178-2921 Red Abalone Larval Development Test Aquatic Bioassay & Consulting Labs, Inc.
Batch ID: 12-4467-1 331 Test Type: Development Anaiyst:
Start Date: 12 May-I15 13:30 Protocol: EPAI6001R-95/1 36 (1995) Diluent: Laboratory Seawater Ending Date: 14 May-15 14:00 Species: Hallotis rufescens BrIne: Not Applicable Duration: 49h Source: Cultured Abalone Age:
Sample ID: 17-7724-2730 Code: ABS05I215a Client. Internal Lab Sample Date: 12 May-15 13:30 Materal:h Zinc Project: REF TOX Receive Date: Source: Reference Toxicant Sample Age: NA Station: REF TOX Parameter Acceptability Criteria Parameter MIn Max AcceptabilIty Limits Overlap Decision Salinity-ppt 34 34 32 - 36 Yes Results Within Limits Temperature-°C 14.1 14.3 14 - 16 Yes Results Within Limits Dissolved Oxygen-mg/L C-pgIL ControlIType Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 Negative Contr 2 6.75 -2.78 16.28 6 7.5 0.75 1.061 15.71% 0 18 2 6.65 -2.88 16.18 5.9 7.4 0.75 1.061 15.95% 0 32 2 6.65 -2.88 16.18 5.9 7.4 0.75 1.061 15.95% 0 56 2 6.65 -2.88 16.18 5.9 7.4 0.75 1.061 15.95% 0 100 2 6.65 -2.58 16.18 5.9 7.4 0.75 1.061 15.95% 0 180 2 6.65 -2.88 16.18 5.9 7.4 0.75 1.061 15.95% 0 Overall 12 6.667 5.9 7.5 0 (0%)
pH-Units C-pg/L Control Type Count Mean 95% LCL 95% UCL Mmn Max Std Err Std Dev CV% QA Count 0 Negative Contr 2 7.65 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 18 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 32 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0,9% 0 56 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 100 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 180 2 7.85 7.215 8.485 7.8 7.9 0.05 0.07071 0.9% 0 Overall 12 7.85 7.8 7.9 0 (0%)
Salinity-ppt C-pg/L Control Typ~e Count Mean 95% LCL 95% UCL Min Max Std Err Std Dev CV% QA Count 0 Negative Contr 2 34 34 34 34 34 0 0 0.0% 0 18 2 34 34 34 34 34 0 0 0.0% 0 32 2 34 34 34 34 34 0 0 0.0% 0 56 2 34 34 34 34 34 0 0 0.0% 0 100 2 34 34 34 34 34 0 0 0.0% 0 180 2 34 34 34 34 34 0 0 0.0% 0 Overall 12 34 34 34 0 (0%)
Tem perature-=C C-IAglL Control Type Count Mean 95% LCL 95% UCL MIn Max Std Err Std Dev CV% QA Count 0 Negative Contr 2 14.2 12.93 15.47 14.1 14.3 0,1 0.1414 1.0% 0 18 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 32 2 14.2 12.93 15.47 14.1 14.3 .0.1 0.1414 1.0% 0 56 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 100 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 180 2 14.2 12.93 15.47 14.1 14.3 0.1 0.1414 1.0% 0 Overall 12 14.2 14.1 14.3 0 (0%)
000-0551 86-6Analyst:____
-'__QA:_____
000-055-186-6 CETISTM vl.8.7.11

DCL-2015-532, Discharge Self-Monitoring Report for 2nd Quarter of 2015

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