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| {{#Wiki_filter:RADIOLOGICAL. | | {{#Wiki_filter:}} |
| ANALYS;Is
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| - Page 5lof 118
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| Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)
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| SDG MISR.I04-1807 Method/Analvsis Information Product: Am241,Cm, Liquid-ALL Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Batch Number: 347826 Sample ID Client ID
| |
| * 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001
| |
| *115774018 MW-I 06S-0204-001 115774019 MW-I06D-0204-001 1200660111 Method Blank (MB) 1200660114 Laboratory Control Sample (LCS)
| |
| .1200660112 115774016(MWV-103S-0204-001) Sample Duplicate (DUP) 1200660113 115774016(MW-103S-0204-00 1)Matrix Spike (MS)
| |
| SOP Reference - ,
| |
| Procedure for preparation, analysis and reporting of'analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 I REV# 13.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774016 (MW-103S-0204-00l).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| .Preparation Information All preparation criteria have been met for these analyses.
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| Page 52 of 118
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| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Manual Integration No manual integrations were performed on data in this batch.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Alphaspec Pu, Liquid-ALL Analytical Method: DOE EML HASL-300, Pu-I I-RC Modified Analytical Batch Number 347828 Sample ID Client ID
| |
| *115774016 MW-103S-0204-001 115774017 MW-104S-0204-001 115774018 MW-106S-0204-001 115774019 MW1- 106D-0204-001 1200660120 Method Blank (MB) 1200660123 Laboratory Control Sample (LCS) 1200660121 115774016(MW-103S-0204-001) Sample Duplicate (DUP) 1200660122 115774016(MW-103S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-0 II REV# 13.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry . -
| |
| All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774016 (MW-103S-0204-001).
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| Page 53 of 118
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| E QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prcp/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Manual Integration Manual integration of alpha spectroscopy spectra 1200660120 (MB) was performed to fully separate counts in Regions of Interest which would have been biased.
| |
| qualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Liquid Scint Pu241, Liquid-ALL Analytical Method: DOE EML HASL-300, Pu-i I-RC Modified Analytical Batch Number: 347829 Sample ID Client ID 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001 115774018 MW-106S-0204-001 115774019 MW-106D-0204-001 1200660132 Method Blank (MB) 1200660135 Laboratory Control Sample (LCS) 1200660133 115774016(MW-103S-0204-001) Sample Duplicate (DUP) 1200660134 115774016(MW-103S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 5.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
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| Page 54 of 118
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| | |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (pC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC - . -
| |
| The following sample was used for QC: 115774016 (MWV-103S-0204-001).
| |
| QC Information . ,; - ,
| |
| All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prepfRe-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Manual Integration No manual integrations were performed on data in this batch.
| |
| Qualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information :- ., I ... I ,I . . .
| |
| Product: Gammaspec, Gamma,Liquid-ALL,GAM2,STND,NIIX,PENN,LF Analytical Method: EPA 901.1 Analytical Batch Number 346796 Sample ID Client ID 115774001 MWV-108S-0204-001 115774002 MWV-122S-0204-001 115774003 MW-1 14S-0204-001 115774004 MW-125S 115774005 MWV-124S 115774006 MWV-IOID-0204-001 115774007 EQF2-0204-001 115774008 MW-I01S-0204-001 115774009 MW-123S-0204-001 115774010... MWIOOD-0204-001 Page 55 of 118
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| | |
| U 115774011 MW507D-0204-001 115774012 MW507S-0204-001 115774013 MW503-0204-001 115774014 MW502-0204-001 115774015 MW505-0204-001 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001 115774018 MW-106S-0204-001 115774019 MW-106D-0204-001 1200657513 Method Blank (MB) 1200657516 Laboratory Control Sample (LCS) 1200657514 115774001(MWV-108S-0204-001) Sample Duplicate (DUP) 1200657515 115774001(MW-108S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774001 (MW-108S-0204-00 1).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced Page 56 of 118
| |
| | |
| SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Oualifier information Qualifier Reason Analte l Samp Ie g4l -Data rejected due to no valid peak. Manganese-54 1115774013 l A.
| |
| Mlethod/Analysis Information Product: Gross A/B, liquid-ALLSTNDMIX,PENNLF Analytical Method: EPA 900.0 Analytical Batch Number 350128 Sample ID Client ID 115774001 MW-108S-0204-001 115774002 MV- 122S-0204-001 115774003 MV- I14S-0204-001 115774004 MMW-125S 115774005 MW-124S 115774006 MW-10ID-0204-001 115774007 EOF2-0204-001 115774008 MW-I01S-0204-001 115774009 MW-123S-0204-001 115774010 MW100D-0204-001 --
| |
| 115774011 MW507D-0204-001 115774012 MW507S-0204-001 115774013 MW503-0204-001 115774014 MW502-0204-001 115774015 MW505-0204-001
| |
| .115774016 MW-V035-0204-001 115774017 MW-104S-0204-001 115774018 MW-106S-0204-001 115774019 MW-106D-0204-001 1200665719 Method Blank (MB) 1200665723 Laboratory Control Sample (LCS) 1200665720 115774001(MW-108S-0204-001) Sample Duplicate (DUP) 1200665721 115774001(MW-108S-0204-001) Matrix Spike (MS) 1200665722 115774001(MW-108S-0204-001) Matrix Spike Duplicate (MSD)
| |
| SOP Reference Procedure for preparation', analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-00 1 REV# 8.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration recquirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Page 57 of 118
| |
| | |
| L Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774001 (MW-108S-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis Samples 115774001 (MW-108S-0204-001) and 1200665720 (MWV-108S-0204-001) were recounted due to high relative percent difference/relative error ratio.
| |
| Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Gross AlphalBeta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments Alpha duplicate rpd fails at 155%, however when the duplicate result is raised to the mda, the calculation passes at 81%.
| |
| Qualifier information Manual qualifiers were not required.
| |
| Mlethod/Analvsis Information Product: GFPC, Sr9O, liquid-ALL,MIIX Analytical Method: EPA 905.0 Modified Analytical Batch Number 351394 Sample ID Client ID 115774001 MW-108S-0204-001 Page 58 of 118
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| * 115774002 MW-122S-0204-001 -
| |
| 115774003 MW-1 14S-0204-001 115774004 MW-125S
| |
| * 115774005 MW-124S 115774006 Mw-101 D-0204-001 115774007 EOF2-0204-001 115774008 MW-IOIS-0204-001 115774009 MW-123S-0204-001
| |
| ,115774016 MWV-103S-0204-001 115774017' MWV-104S-0204-001
| |
| * 115774018 MWI- 106S-0204-001
| |
| * 115774019 MW-106D-0204-001 1200668742 Method Blank (MB) 1200668745 Laboratory Control Sample (LCS) 1200668743 115774005 (MW-124S) Sample Duplicate (DUP)
| |
| * 1200668744 115774005(MW-124S) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation,'analysis and reporting of an'alytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 8.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ounlity Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774005 (MW-124S).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time ' -
| |
| All sample procedures for this sample set were performed within the required holding time.
| |
| ' Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prepfRe-analysis Samples were reprepped due to high relative percent difference/relative error ratio.
| |
| Chemical Recoveries Page 59 of 118
| |
| | |
| U All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments Samples 115774004 (NIMV-125S), 115774016 (MWV-103S-0204-001) and 115774018 (MW-106S-0204-001) were verified by the gross beta results.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Liquid Scint Tc99, Liquid-ALL Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number 346017 Sample ID Client ID 115774016 MW-103S-0204-001 115774017 MNV-104S-0204-001 115774018 MW-106S-0204-001 115774019 MW-106D-0204-001 1200655689 Method Blank (MB) 1200655692 Laboratory Control Sample (LCS) 1200655690 115774016(MW-103S-0204-001) Sample Duplicate (DUP) 1200655691 115774016(MW-103S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 11.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774016 (MNV-103S-0204-001).
| |
| Page 60 of 118
| |
| | |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time ~I All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| qualifier information Manual qualifiers were not required.
| |
| * Method/Analysis Information Product: : Liquid Scint FeS5, Liquid-ALL Analytical Method: DOE RESL Fe-l, Modified Analytical Batch Number 345524 K>
| |
| Sample ID *ClientDID 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001
| |
| * 115774018 MW-106S-0204-001 115774019 MW-106D-0204-001 1200654552 Method Blank (MB) 1200654555 *Laboratory Control Sample (LCS) 1200654553 I I5774016(MWV-103S-0204-001) Sample Duplicate (DUP)
| |
| .1200654554 115774016(MW-103S-0204-001) Matrix Spike (MS)
| |
| '' SOP Reference Procedure for preparation, analysis and reporting of analytical 'data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 2. ' ':
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met. .
| |
| Standards Information . : ''
| |
| Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.'
| |
| Page61 of 118 I . .~; . .
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| | |
| - - 111-Ooality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774016 (MW-103S-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments The following samples have large negative results due to the Iron-59 cross-talk correction: 115774016 (MW--103S-0204-001), 115774017 (MW--104S-0204-001), 115774018 (MNV-106S-0204-001), 115774019 (MW-106D-0204-001), 1200654552 (MB) and 1200654553 (MW-103S-0204-001).
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/Analvsis Information Product: Liquid Scint Ni63, Liquid-ALL Analytical Method: DOE RESL Ni-1, Modified Analytical Batch Number 345523 Sample ID Client ID 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001 115774018 MNV-106S-0204-001 115774019 MW-106D-0204-001 1200654548 Method Blank (MB) 1200654551 Laboratory Control Sample (LCS) 1200654549 115774016(MW-103S-0204-001) Sample Duplicate (DUP) 1200654550 115774016(MW-103S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in Page 62 of 118
| |
| | |
| accordance with GL-RAD-A-022 REV# 6.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774016 (MW-103S-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prepfRe-analysis
| |
| - None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| qualifier information Manual qualifiers were not required.
| |
| .Method/Analvsis Information Product; LSC, Tritium Dist, LUquid-ALLSTND,MIIX,PENN Analytical Method:
| |
| * EPA 906.0 Modified Analytical Batch Number 345392 Sample ID Client ID 115774001 MW-108S-0204-001 115774002 MIV-122S-0204-001 115774003 MW-114S-0204-001
| |
| .115774004 MWV-125S Page 63 of 118
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| | |
| -- a-115774005 MW-124S 115774006 MW-IOID-0204-001 115774007 EOF2-0204-001 115774008 MW-101S-0204-001 115774009 MW-123S-0204-001 115774010 MWIOOD-0204-001 115774011 MW507D-0204-001 115774012 MW507S-0204-001 115774013 MW503-0204-001 115774014 MW502-0204-001 115774015 MW505-0204-001 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001 115774018 MNV-106S-0204-00t 115774019 MW-106D-0204-001 1200654328 Method Blank (MB) 1200654331 Laboratory Control Sample (LCS) 1200654329 115774001(MW-108S-0204-001) Sample Duplicate (DUP) 12006S4330 115774001(MW-108S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 9.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774001 (MWV-108S-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis Page 64 of 118
| |
| | |
| Samples 115774003 (MW-I 14S-0204-001) and I15774005 (MW-124S) were recounted due to the quench number being outside the calibration range.
| |
| Miscellaneous Information:
| |
| . NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments Samples 115774011 (MW507D-0204-001) and 115774012 (MW507S-0204-001) were received and ran preserved with client permission per e-mail from Dave Keefer dated 7/12/04.
| |
| Qualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: .. Liquid Scint C14, Liquid-ALL Analytical Method: EPA EERF C-01 Modified Analytical Batch Nun iber 345987 Sample ID Client ID 115774016 MW-103S-0204-001 115774017 MW-104S-0204-001 115774018 MW-106S-0204-001 115774019 MW-106D-0204-001 1200655617 Method Blank (MB) 1200655620 Laboratory Control Sample (LCS) 1200655618 115774016(MWV-103S-0204-001) Sample Duplicate (DUP) 1200655619 115774016(MW-103S-0204-00l) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP): The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 7.
| |
| Calibration Information:
| |
| Calibration Information
| |
| - All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s):
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| . Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115774016 (MW-103S-0204-001).
| |
| *Page 65 of 118
| |
| | |
| /
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Timc All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Onalifler information Manual qualifiers were not required.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| The following data validator verified the information presented in this case narrative:
| |
| ( 01WkJ &LUC J JJ91Le0z Reviewer:
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| Page 66 of 118
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| . . It : ~..;. ''
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| * I I I
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| SAMPLE DATA e . . . . . .
| |
| | |
| ==SUMMARY==
| |
| ... .. s h . .
| |
| Page 67 of 118
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| | |
| 0-GENERAL ENGINEERING-LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Hladdam Neck Plant 362 Injun Hollow Road -
| |
| East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater P0# 002337 Page I of 2 Client Sample ID: MW-108S-0204-001 Proiect: YANK00304
| |
| * Samplc ID: 115774001 Client ID. YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch ltd.
| |
| Rad Gamma Spec Analysis Gammaspe4 Gammna.Liquid-ALl, GAM2,STND,MIXPENNLF Americium-241 U 3.74 +/-10.3 8.96 +/-10.0 18.9 pCIIL SRB 07121/04 1423 346796 1 Cesium-134 U 0.667 +/-1.84 159 +1-1.80 356 p~ilL Cesium-137 U -0.215 +1-1.89 1.56 +1-1.86 3.43 p~ilL Cobalt-60 U 5.25 +/-2.64 2.70 +1-259 5.87 p~i/L Europium-152 U -3.42 +/-5.71 4.33 +1-559 9.29 pcitL Europium-154 U 0.457 +/-5.26 4.27 +1-5.15 9.84 p~ilL Europium-lS5 U 0.673 +1-6.73 5.71 +/-6.60 12.0 pci/L Manganese-54 U -0.585 +/-1.90 150 +/-1.86 3.33 pCVtL Niobium-94 U 1.71 +/-1.66 154 +/-1.63 3.35 pCVlL Silver-108m U 150 +/-1.73 1.50 +/-1.69 3.24 p~ilL Rad Gas Flow Proportional Counting GFPC,Sr9O, liquid-A U.MIX Strontium-90 U 0.0577 +1-0.567 0.623 +1-0567 1.40 pcilL HOBI 07127/04 0836 351394 2 Gross A/B, liquid.AL4STNDMIX PENNLF Alpha 3.90 +/-1.64 1.16 +/-1.67 255 pCV/L ATHI 07127/04 1403 350128 4 Beta 5.72 +1-1.74 1.40 +1-1.76 2.92 pC11L Rad Uquld Scintillation Analysis LSC Tritium Dist Iiquid-ALSTNDMl( PENN Tritium U 136 +/-154 126 +1-154 251 pCilL JLB I 07/14/04 1135 345392 5 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 The following Analytical Methods were performed Method Description 1 EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 68 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556.8171 - www.geL.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-IOBS-0204-001 Project: YANK00304 Sample)): 115774001 ClientID: YANKOOl Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch h Surrogatelrracer recovery Test -Recovery% Acceptable limits Carrierflraccr Recovery GFPC, Sr9O, liquid-ALLMIX '72 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.*
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| 4A- fQC 1O..
| |
| Reviewed by Page 69 of 118
| |
| | |
| a-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: lladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424. Report Datc: July 27,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 1 of 2 Client Sample ID: MW-122S-0204-001 Proiect: YANK00304 Sample ID: 115774002 Client ID: YANK00I Matrx: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 1 28-JUN-04 Collector: Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspe4 Gam'aLiquid-ALL GAM2,STND,MIXPENN,LF Americium-241 U 13.0 +/-18.0 13.8 +1-17.7 28.8 pCiIL SRB 07/21/04 1424 346796 1 Cesium-134 U 2.44 +1-4.14 2.01 +/-4.06 4AI pCV1L Cesium-137 U 0.551 +/-2.12 1.77 +/-2.08 3.87 pCVtL Cobalt-60 U 0.857 +1-2.32 2.02 +1-2.28 4.55 pCV1L Europium-152 U 0.606 +1-6.21 5.20 +1-6.08 11.1 pCV1L Europium-154 U 3.66 +/-5.61 4.72 +1-5.49 10.8 pCi1L Europium-155 U -2.81 +1-9.19 7.27 +1-9.01 15.1 pCi/L Manganese-54 U 0.584 +/-1.81 1.59 +1-1.78 3.55 pCiIL Niobium-94 U 0.651 +1-1.77 1.49 +1-1.74 3.29 pCiIL Silver-108m U -1.58 +1-2.07 157 +1-2.03 3.41 pCiIL Rad Gas Flow Proportional Counting GFPC, Sr90 liquid-ALL.MlX Strontium-90 U 0.568 +/-0.493 0.429 +1-0510 0.977 pCV/L IIOBI 07127/04 0836 351394 2 GrossAtB, liquid-ALL.STNDMOXPENN.LF Alpha 4.88 +1-1.33 0.732 +/-1.36 1.60 pCi/L ATHI 07/22/04 0451 350128 4 Beta 8.40 +1-154 1.07 +1-1.56 2.21 pCi/L Rad Liquid Scintillation Analysis LSC, Tritium Dist Liquid-AL4STNDMIXJPENN Tritium 645 +1-158 116 +1-158 233 pClL JLBI 07/14/04 1237 3453925 The following Prep Methods were performed Method Description . Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI1 07/14/04 1721 345045 The following Analytcal Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 70 of 118
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC
| |
| - 2040 Savage Road Charleston SC 29407 (843) 556-8171 - www.gel.com K-;
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-122S-0204-001 Proiect: YANK00304 SapeID:
| |
| SampleI 115774002 Client ID: yANKOOI Vol. Recv.:
| |
| : Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| SurrogateiTracer recovery Test Recovery% Acceptable U1mits CarrieriTracer Recovery GFPC, SO9O, liquid-ALl,MIX 96 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank-BD Flag for results below the MDC or a flag for low tracer recovery. C E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 4I Analytical holding time exceeded.
| |
| _J. Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed forbut not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary p'ackage or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah KozliL.
| |
| Reviewed by Page 71 of 118
| |
| | |
| - W-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 1 of 2 Client Sample ID: MW-1 14S-0204-001 Proiect- YANK00304 Samplel ID: 115774003 Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-0 Collector Client Parameter Qualifier Result Uncertainty LC TPU MIDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspe4 GammaLiquid-AL.GAM2,STNDAfEXPENN,LF Amcricium-241 U 6.68 +1-13.1 10.1 +/-12.8 21.0 pCi/L SRB 07/21/04 1426 346796 1 Cesium-134 U -1.58 +1-2.16 1.63 +1-2.12 3.58 pCiIL Cesium-137 U 1.57 +1-1.89 1.70 +1-1.85 3.68 pcV/L Cobalt-60 U 1.17 +/-1.83 1.67 +1-1.79 3.76 pCi/L Europium-152 U 0.770 +/-5.79 4.82 +/-5.68 10.2 pCiIL Europium-154 U 1.31 +1-4.87 4.23 +1-4.78 9.61 pCi/L Europium-155 U 0.0514 +1-7.39 6.03 +/-7.25 12.6 pCiIL Manganese-54 U -0.0794 +1-1.77 1.45 +1-1.74 3.20 pCiIL Niobium-94 U -0.379 +/-1.61 1.31 +1-1.58 2.86 pCi/L Silver-108m U 0.386 +1-2.01 1.66 +,-1 .97 3.53 pCi/L Rad Gas Flow Proportional Counting GFPC,Sr90, liquid-ALL,MlX Strontium-90 U 0.541 +/-0.571 0.528 +/-0.588 1.19 pCW/L HOB1 07/27/04 0931 3513942 Gross/AIB, liquid-ALSTNDAMIXPENMLF Alpha 6.29 +1-1.19 0.495 +/-1.22 1.11 pCzIL AlIll 07/22/04 0451 3501284 Beta 8.11 +1-1.45 1.02 +/-1.46 2.08 pCV/L Rad Liquid Scintillation Analysis LSC Tritium Dist, Liquid-AULSTNDML(PENN Tritium 6730 +1-420 214 +/-433 427 pCi/L JLBI 07/21/04 2102 345392 5 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQH1 07/14/04 1721 345045 The following Analytlcal Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 72 of 118
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| LLC GENERAL ENGINEERING LABORATORIES, GEN ERAL 'ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556 8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddarn Neck Plant 362 Injun Hollow Road East Hamrpton, Connecticut 06424 Report Date: July 27,2004 Contact Mr. Dave Keefer Prject Quarterly Groundwater PO# 002337 - I Page 2 of 2
| |
| .. - I Client Sample ID: MW-114S-0204-001 Project: YANK003D4 Sample ID: 115774003 Client ID: YANKOO1 Vol. Rek
| |
| * Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate TIme Batch Mtd.
| |
| - lf - -- A -- f.M,. T 9t...h saurul~u~aasss*uszs ^ -T x ''}x
| |
| * m --
| |
| Carrier/ITracer Recovery - GFPC, Sr9O, liquid-ALMJX 84 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| -1 Analytical holding time exceeded.
| |
| __J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed forbut not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please seecase narrative, data sunmary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an Was received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| * q{ & A Reviewed by (y iO Page 73 of 118
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| | |
| EGINERIN GENEAL LL LABRATRIES a-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27.2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PON 002337 Page 1 of 2 Client Sample ID: MW-125S Project: YANK00304 Sample ID: 115774004 Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 22-JUN-04 Receive Date 28-JUN-04 Collectort Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time BatchMtL Rad Gamma Spec Analysis Gammraspec, Gamma,Liquid-ALL CAM2,STND,MIX PENN,LF Americium-241 U -0.984 +1.15.3 11.0 +1-15.0 23.0 pCiIL SRB 07/21/04 1426 346796 1 Cesium-134 U 0.500 +/-2.12 1.79 +/-2.08 3.93 pCV1L Cesium-137 U 1.26 +/.2.03 1.79 +/-1.99 3.88 pCilL Cobalt-60 U 1.95 +1.1.78 1.64 +1-1.74 3.71 pCV/L Europium-152 U -3.97 +/-6A2 4.99 +1-6.29 10.6 pCiLL Europium-154 U 3.35 +1-5.5 4.98 +1-5.40 11.1 pQi/L Europium-155 U 2.71 +/8.859 6.97 +/-8.42 14.5 pCziL Manganese-54 U -0.535 +/-2.08 1.65 +1-2.04 3.62 pCiIL Niobium-94 U 1.15 +/-2.23 1.52 +/-2.18 3.30 pCiIL Silver-108m U 0.854 +/-2.00 1.67 +/-1 .96 3.57 pCiIL Rad Gas Flow Proportional Counting GFPC, Sr90, liquid-ALLAIX Strontium-90 1.78 +1-0.742 0.505 +/-0.881 1.15 pCWLi HOB I 07/27/04 0931 351394 2 GrossA/B, liquid-ALLSTNDMlXPENNLF Alpha 2.36 +/-0.789 0.366 +/-0.795 0.860 pClIL ATHI 07/22/04 0451 3501284 Beta 11.8 +1-1.52 0.982 +1-1.55 2.02 pCV/L Rad Liquid Scintillation Analysis LSC Tritium Dist, Liquid-AL4STNDMIXPENN Tritium 2170 +1-197 118 +1-200 236 PCVL JLBI 07/14/04 1442 3453925 The following Prep Methods were performed Method Description Analyst Date lime Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I EPA901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 S EPA 906.0 Modified Page 74 of 118
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| GENERAL ENGINEERING GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road Eait Hampton, Connecticut 06424 Report Date July 27,2004 Contact Mr. Dave Keefer Projcct: - Quarterly Groundwater PO# 002337 - , - Page :2 of 2 Client Sample ID:
| |
| * MW-125S Proiect: YANK00304 Sample ID: 115774004 Client ID: YANKOOX Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnabstDate Time Batch Mtd.
| |
| SurrogatelTracer recovery Recovery% Acceptable Umits Carrierfrracer Recovery GFPC, Sr9O, liquid-ALLMIX 83 :
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated biank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| Ks 1Indicates an estimated value. The result was greater than the detection linit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 75 of 118
| |
| | |
| GENERAL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hiollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW-124S Proiect: YANK0030O4 Sample ID: 115774005 Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualiller Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GamnimLiquid-ALLGAM2,STND.MIXPENN,LF Americium-241 U 19.2 +1-24.3 11.5 +1-23.8 24.1 pCVL SRB3 07/21/04 1427 346796 1 Cesium-134 U 0.340 +1-1.96 1.42 +/-1.92 3.19 pCV1L Cesium-137 U -0.912 +/-1.91 1.47 +1-1.87 3.22 pCVL Cobalt-60 U -0.263 4.-2.05 1.65 +1-2.01 3.74 Europium-152 U 1.35 +/-5.43 4.16 +1-5.32 8.91 PCVL Europium-154 U 1.00 +/4.36 3.76 +/-4.27 8.72 pCtLL I Europium-155 U 4.87 +/-6.93 5.95 +1-6.79 12.4 pCiIL Manganese-54 U 0.268 +/-1.66 1.37 +1-1.63 3.05 pCV/L Niobium-94 U 1.12 +1-1.84 1.59 +/-1.80 3.43 pC/LL Silver-108m U 2.19 +1.1.69 1.60 +/-1.66 3.42 pCVrL Rad Gas Flow Proportional Counting GFPC, Sr90, liquid-AlLLAX Strontium-90 U 1.33 +/-0.791 0.664 +/-0.872 1.47 pCiQL iHOBI 07/27/04 0931 351394 2 Gross A/B, liquid-AL.STND.AIX, PENN,LF Alpha U 1.09 +/-1.32 1.04 +/-1.32 2.20 pCiQL ATlI 07/22/04 0412 350128 4 Beta 4.98 +/-1.66 1.28 +1-1.67 2.62 pCiL Rad Llquid Scintillation Analysis LSC, Tritium Dist, Liquid-ALL.STD.ML PENN Tritium 1770 +1-296 205 +/-298 410 pCVL JLB 1 07/21/04 2205 3453925 The following Prep Methods were performed Method Description Analyst Date rTme Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 76 of 118 LIC ENGINEERING LABORATORIES,
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address : Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 -Page 2 of 2 Client Sample ID: MW-124S Proiect: YANK00304 Sample ID: 115774005 Clien.ID: YANRc001 Parameter Qualifier Result Uncertainty LC TPU SODA Units DF. AnalystDate Time Batch Mtd.
| |
| SurrogateiTracerrecovery Test Recovery% Acceptable Limits CarrierlTraccr Recovery - GFPC, S9, liquid-AlLMIX 80 Notes:
| |
| The Qualifiers in Us report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 'I Analytical holding time exceeded.
| |
| Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiLm-Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with Geineral Engineering Laboratories, LC standard operating procedures. Please direct any questions to your Project Manager, Sarah Xozlik.
| |
| 'Reviewed by Page 77 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: H addam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW-IOID-0204-001 Project: YANK00304 Samrle ID: 115774006 Client ID: YANK001 Matrix: Ground Water Vol. Recv:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 Collector: Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Arnalysis Gammaspec, GanmmLiquid-AL4.GAM2,STND,AfZXPEPJN,LF Americium-241 U -0.665 +1-13.7 9.77 +/-13.4 20.4 pCi/L SRB 07/21/04 1428 346796 1 Cesium-134 U -0.136 +/-2.23 1.78 +/-2.19 3.92 pCi/L Cesium-137 U 1.38 +1-1.81 1.61 +/-1.77 3.52 pCi/L Cobalt-60 U 1.97 +1-1.73 1.71 +1-1.70 3.90 pCi/L Europium-152 U -0.267 +/-6.05 4.77 +1-5.93 10.1 pCi/L Europium-154 U 2.68 +/-5.81 4.75 +/-5.70 10.8 pci/L Europium-155 U 5.14 +1-7.58 6.03 +/-7.43 12.6 pCitL Manganese-54 U 0.0144 +/-2.14 1.71 +1-2.10 3.76 pCi/L Niobium-94 U -1.44 +/-2.03 1.25 +/-1.99 2.77 pCi/L Silver-108m U -0.828 +/t1.83 1.47 +/-1.79 3.17 pCitL Rad Gas Flow Proportional Counting GFPC,Sr90, liquid-ALL.WIX Stronlium-90 U 0.0309 +/-0.490 0.542 +/-0.490 1.23 pCi/L HOB I 07t27/04 0931 351394 2 GrossA/B, liquid-ALL.STNDMIXPENNMLF Alpha 8.50 +1-1.34 0.575 +/-1.58 1.26 pCilL ATHI 07/22/04 0412 350128 4 Beta 6.18 +/-1A0 1.00 +/-1.42 2.06 pCi/L Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-ALLSTNDML1XPENN Tritium U 15.5 +1-145 121 +/-145 242 pCi/L JLBI 07/14104 1647 3453925 The foUowing Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI1 07/14/04 1721 345045 The following Analytical Methods were performed Method Description 1 EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 78 of 118
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| | |
| LLC GENERAL ENGINEERING LABORATORIES,
| |
| .GENERAL-ENGINEERING LABORATORIES., LLC
| |
| * 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Addreis: Haddam Neck Plant 362 Injun Hollow Road
| |
| : East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project:- Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-IOID-0204-001
| |
| * Proiect: YANK00304 Sample ID: ' 115774006 Client ID: YANKOOI
| |
| * Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carriertracer Recovery GFPC, Sr9O, liquid-ALI.MIX 79 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| - E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 'I Analytical holding time exceeded. -
| |
| Ki> Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamnna spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 79 of 118
| |
| | |
| LLC LABORATORIES, ENGINEERING GENERAL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 1 of 2 Client Sample ID: EOF2-0204-001 Proiect: YANK00304 Sample ID: 115774007 Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter. Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Garmna Spec Analysis Gammaspec, GammaLiquid-A GAM2STNDAfIXPENNLF Americium-241 U -2.78 +1-10.6 8.61 +1-10.4 18.0 pCi/L SRB 07/21/04 1428 346796 1 Cesium-134 U 0.192 +/-1.82 1.47 +/-1.78 3.26 pCi/L Cesium-137 U 0.605 +/-1.79 1.50 +1-1.76 3.27 pCV/L Cobalt-60 U 0.179 +/-2.03 1.47 +/-1.99 3.33 pCi/L Europium-152 U 4.12 +/-5-54 4.85 +/-5.43 10.2 pCVIL Europium-154 U -0.808 +1-3.94 3.10 +/-3.86 7.27 pCV1L Europiumn155 U -5.68 +1-7.40 5.76 +/-7.25 12.0 pCb'L Manganese-54 U 0.174 +/-1.73 1.47 +1-1.69 3.23 pCVL Niobium-94 U 0.293 +/-1.80 1.48 +1-1.77 3.18 pCVfL Silver-108m U 1.32 +/-1.78 1.55 +/-1.74 3.30 pCVL Rad Gas Flow Proportional Counting GFPC, Sr9O, liquid-ALL.MlX Strontiun-90 U -0.131 +/-0.504 0.596 +/-0.506 1.34 pCilL HOBI 07/27/04 0931 351394 2 Gross AM, liquid-ALLSTNDMIX.PENNLF Alpha 2.58 +/4.825 . 0.418 +/-0.855 0.949 pCi/L ATill 07/22/04 0412 350128 4 Beta 3.30 +1-1.40 1.09 +/-1.41 2.24 pCi/L Rad Liquid Scintillation Analysis LSC, TritiumDist, Liquid-A lLSTNDM1X PENN Tritium U 196 +/-176 143 +/-176 286 pCi/L JLB1 07/14/04 1749 3453925 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14104 1721 345045 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 80 of 118
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| | |
| LLC GENERAL ENGINEERING LABORATORIES, IGENERAL ENGINEERINGLA'BORATORIES, LLC
| |
| -2040 Savage Road aileston SC 29407 - (843) 556-8171 - ww.gel.com Certificate'of 'Analysis .
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004 Contact. Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 - IPage 2 of 2 Client Sample ID:.' EOF2-0204-001 ' Proiect: YANK00304 Sample ID: 115774007 Client ID: YANKO1I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Tlme Bitch Mtd.
| |
| SuqrrwmatefTrrer recnvcrv - Test RenvPrvV.
| |
| 1
| |
| - - - - - - - -I -
| |
| Arentabli lAmlnts Carierfrracer Recovery GFPC, Sr9O, liquid-ALl,MIX 75 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blankl BID Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| Y Analytical holding time exceeded.
| |
| Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sarnple preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 81 of 118
| |
| | |
| a-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PON 002337 Page 1 of 2 Client Sample ID: MW-IOIS-0204-001 Proiect: YANK00304 Sample ID: 115774008 Client ID: YANKOOI Matnx: Ground Water Vol. Recm.:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysts Gammaspec, Gamna,Liquid-ALGAAf2,STND,M1XPENN,LF Americium-241 U 1.22 +/-3.40 2.93 +/-3.33 6.11 pCiIL SRB 07/21/04 1429 346796 1 Cesiumn-134 U -0.693 +/-2.11 1.67 +/-2.07 3.68 pCaiL Cesium-137 U -0.254 +/-2.00 1.65 +/-1.96 3.59 pCill Cobalt-60 U 0.503 +1-1.94 1.67 +/-1.90 3.78 pCU/L Europium-152 U 2.10 +1-4.96 4.25 +/-4.86 9.04 pCi1L Europium-154 U 0.0777 +t-6.34 5.26 +1-6.21 11.7 pCV/L Europium-155 U 2.00 +1-5.53 4.66 +/-5.42 9.72 pCV/L Manganese-54 U -1.17 +/-1.94 1.47 +/-1.90 3.26 pCi/L Niobium-94 U -0.645 +/-1.81 1.45 +/-1.77 3.16 pCiIL Silver-108m U 0.851 +/-1.78 1.51 +/-1.74 3.24 pCV/L Rad Gas Flow Proportional Counting GFPC, Sr9O, liquid-ALLMIX Strontium-90 U -0.242 +/-0.414 0.527. +/-0.420 1.20 pCV1L IIOB I 07/27/04 0931 351394 2 GrossA/B, liquid-ALLSTND,MlXPENNLF Alpha 1.59 +/-0.939 0.665 +/40.949 1.44 pCV1L ATHII 07/22n04 0412 350128 4 Beta 3.27 +/-1.40 1.09 +/-1.41 2.25 pCV/L Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid- ALU4SNDMEXPENN Tritium U 252 +/-179 144 +/-179 288 pCU/L JLBI 07/14/04 1852 345392 5 The following Prep Methods were performed Method Description Analyst Date Tlme Prep Batch SW846 3005A ICP-MS 3005 PREP CQH1 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 82 of 118
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| - Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 'Page 2 of :2 Client Sample ID:
| |
| * MW-IOIS-0204-001 Project: YANK00304:
| |
| Sample ID: 115774008 Client ID: YANKOOI Vatlp
| |
| . R- .. . I Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time BatchMtd.
| |
| Surrogaterrracer recovery Test Recovery% Acceptable Ufmits
| |
| * 79 CarrierTrracer Recovery GFPC, 'Sr90, liquid-ALLMIX Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| I Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection lirnit.
| |
| UT Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah KozliL Reviewed by Page 83 of 118
| |
| | |
| - a GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW-123S-0204-001 Proiect: YANK00304 Sample ID: 115774009 Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualilfier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GamrmALUquid-AL4GAM2.S7ND AMIX PENNLF Americium-241 U 12.9 +/-16.8 13.8 +/-16.5 29.0 pCifL SRB 07/21/04 1429 346796 1 Cesium-134 U 1.84 +/-2.80 1.58 +/-2.74 3.47 pCilL Cesium-137 U 2.46 +1-1.98 1.83 +/-1.94 3.93 pCiQll Cobalt-60 U 0.781 +/-1.78 1.59 +1-1.75 3.59 pCiQL Europium-152 U 0.146 +/-5.52 4.42 +1-5.41 9.42 pCi/L Europium-154 U 0.979 +/-4.73 4.07 +/4.63 9.27 pCi/L Europium-155 U 0.191 +/-7.12 6.02 +/-6.98 12.6 pCiL Manganese-54 U -0.696 +/-1.69 129 +/-1.66 2.88 pCi/L Niobium-94 U -1.22 +/-2.08 1.37 +/-2.04 2.99 pCi/L Silver-108m U 0.323 +/-1.84 1.58 +1-1.80 3.37 pCiQl Rad Gas Flow Proportional Counting GFPC, Sr9O, liquid-AL4MJX Strontium-90 U 0.471 +/-0.617 0.605 +1-0.629 1.34 pCi/Q HIOBI 07/27104 0931 351394 2 GrossA/B, liquid-ALLSTNDM1XPENNLF Alpha 4.63 +/-1.12 0.572 +1-1.21 1.25 ATHlI 07/22/04 0419 350128 4 pCi/L Beta 19.6 +/-1.84 1.12 +/-1.98 2.29 Rad LiquId Scintllation Analysis pCV/L LSC, Tritium Dist, LUquid-ALU.STNDMXPENN Tritium U 174 +/-187 153 +/-188 306 JLBI 07114/04 1954 3453925 The following Prep Methods were performed Method Description Analyst Date TIme Prep Batch SW846 3005A ICP-MS 3005 PREP CQH1 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 905.0 Modified 4 EPA 900.0 5 EPA 906.0 Modified Page 84 of 118
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| LLC GENERAL ENGINEERING LABORATORiES, GENERAL ENGINEERING LABORATORIESs LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424
| |
| * Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Prject: Quarterly Gioundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-123S-0204-001 - Proiect: YANK00304 -
| |
| Sample ID: 115774009 Client ID: YANKOOl Id1 I_, .
| |
| -VI. EVA V.;:
| |
| Parameter Qualifier Result Uncertainty LC TPU - MDA Units DF AnalystDate Thme Batch Mtd.
| |
| Surrogate/Tracer recovery Recovery% - Acceptable Lrnits Carrier/Tracer Recovery GFPC, Sr9O, liquid-AllMIX '86 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated biank.
| |
| BD Flag for reslts below the MDC or a flag for low tracer recovey.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 'I Analytical holding time exceeded.
| |
| YJ Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit U Indicates the target analyte was analyzed forbut not detected above the detection linit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 85 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - wvw.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW100D-0204-001 Proiect: YANK00304 Samnple ID: 115774010 Client ID: YANKOO1 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GammaULiquid-AL4GAM2,S7ND.M1XPENN.LF Americium-241 U 1.61 +1-3.52 2.98 +/-3.45 6.22 pCz/L SRB 07121lO4 1430 346796 1 Cesium-134 U 3.84 +1-4.84 2.43 +1-4.74 5.28 pCi/L Cesium-137 U 0.390 +/-2.32 1.99 +/-2.27 4.32 pCV/L Cobalt-60 U 5.20 +1-2.37 2.54 +/-2.32 5.63 pCit'L Europium-152 U 0.428 +1-6.06 5.03 +/-5.94 10.7 pOi/L Europium-154 U -0.717 +1-5.85 4.83 +1-5.73 11.2 pCi/l, Europium-155 U -3.34 +1-5.90 4.56 +/-5.78 9.55 pCi1L Manganese-54 U -0.415 +/-2.48 2.01 +/-2.43 4.42 pO/1L Niobium-94 U -0.828 +1-2.35 1.91 +/-2.31 4.13 pCU/L Silver-108m U -2.46 +1-2.14 1.53 +/-2.10 3.32 pOi/L Rad Gas Flow Proportional Counting GrossAM, Iiquid-ALLSTND.AJXPENNLF Alpha 2.38 +1-1.01 0.679 +/-1.03 1.46 pOi/L ATHI 07/22104 0419 350128 2 Beta U 1.02 +1-137 1.12 +/-1.37 2.29 pO/1L Rad Liquid Scintillation Analysis LSC Tritium Disr, Liquid-AaLSTNDMfEXPENN Tritium U 1.80 +/-183 153 +/-183 306 pCV/L JLB1 07/14/04 2057 345392 3 The following Prep hMethods were performed Method Description Analyst Date Tine Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 lbe following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| lThe Qualifiers in this report are defined as follows:
| |
| B Target analytc was detected in the sample as well as the associated blank.
| |
| Page 86 of 118
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| LLC GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIESt,LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424
| |
| * Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 -.. . . . IPage 2 of 2 Client Sample ID: MWIOOD-0204-00l - Proiect: YANK00304 Sample ID: 115774010 Client ID: YANKOOl
| |
| * vA1 ID_ .
| |
| P ue. Utv.; D . T a d Parameter QuAfler Result Uncrtainty LC Tl'U ; -;' MDA .units DF AnatystDate 71me Batch Mtd' BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded. -
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| V Sample preparation or preservation holding time exceeded.
| |
| "-Theabove sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 87 of 118
| |
| | |
| EOI
| |
| -GE GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Nock Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW507D-0204-O01 Proiect: YANK003W4 Samle ID: 115774011 Client ID: YANKOOI Matnrx: Ground Water Vol. Recv.:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 Collector: Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Ga-maspec, Gamn4Lriquid-T ALL GAM2,STND.MIX PENN LF Americium-241 U -0.462 +/-8.97 6.69 +1-8.79 13.8 pcV/L SRB 07/21/04 1939 346796 1 Cesium-134 U -0.0531 +/-1.42 1.17 +4-1.40 2.51 pCV/L Ccsium-137 U 0.474 +/-131 1.13 +/-1.29 2.39 pCi/L Cobalt-60 U -0.597 +1-159 1.27 +1-1.56 2.75 pCL/L Europium-152 U -0.753 +/-3.96 3.24 +/-3.88 6.75 pCU1L Europium.154 U 2.96 +14.13 3.66 +14.05 7.90 pCiIL Europium- 155 U -1.98 +/-5.46 4.39 +1-5.35 9.03 pCi/L Manganese-54 U -0.166 +/-1.26 1.02 +/-1.23 2.20 Niobium-94 U 0.612 +/-1.18 1.02 +1-1.15 2.16 pCi/L Silver-108m U -0.437 +/-1.38 1.10 +1-1.35 2.31 pCV1L Rad Gas Flow Proportional Counting Gross AI, liquid-ALL STND,MEIXPENN, LF Alpha 28.8 +1-2.16 0.492 +/-3.04 1.09 pCiLL ATHI 07/22/04 0419 350128 2 Beta 15.2 +/-1.71 1.08 +1-1.78 2.21 pC/L' Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-AL4STNDMlXYPENN Tritium U 112 +/-186 153 +/-186 306 pCi/L JLB I 07t14/04 2159 345392 3 The following Prep Methods were performed Method Descriptlon Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are dcfined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| Page 88 of 118
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| | |
| LLC GENERAL ENGINEERING LABORATORIES, GENERAL' ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo
| |
| -Address: Haddam Neckc Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004 Contact Mr. Dave Keefer.
| |
| - Project. Quarterly Groundwater PO# 002337 I Page 2 of 2 Client Sample ID - MW507D-0204-001 Proiect: YANK00304 Sample ID: 115774011 Client ID: YANKOO0 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate rome Batch Mtd.
| |
| BD Flag for results blow the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit U Indicates the target analyte was analyzed for but not detected above the detection limnit.:
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| <k.A Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| j' {C Reviewed by C,, ;,'-
| |
| Page 89 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Iladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PON 002337 Page I of 2 Client Sample ID: MW507S-0204-001 Proiect: YANK0030O4 Sample ID: 115774012 Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-04 Collector: Client Parameter Qualifler Result Uncertainty LC TPU NIDA UnIts DF AnalystDate Time Batch ltd.
| |
| Rad Gamma Spec Analysis Gammaspec, GarmmaLiquid-All, GAM2,STNDMIXPENAMLF Americium-241 U 5.48 +/-7.99 5.99 +1-7.83 12.4 pCWL SRB 07/21/04 1955 346796 1 Cesium-134 U 0.397 +/-1.35 1.13 +/-1.32 2.43 pCVL Cesium-137 U -0.208 +/-1.29 1.05 +/-1.27 2.25 pCV1L Cobalt-60 U 1.00 +1-1.34 1.21 +/-1.32 2.64 pCiIL Europium-152 U -0.657 +1-3.85 3.04 +1-3.77 6.37 pCi/L Europium-154 U -0.325 +/-3.49 2.86 +4-3.42 633 pCi/L Europium-155 U 3.66 +1-4.68 4.08 +/-4.59 8.42 pCVLL Manganese-54 U 0.612 +/-1.22 1.04 +1-1.20 2.23 pCVL Niobium-94 U 0.703 +/-1.36 1.03 +/-1.34 2.20 pCVL, Silver-108m U 0.830 +1-1.92 0.988 +/-1.88 2.09 pCiIL Rad Gas Flow Proportional Counting Gross A/, liquid-AU.STNDMfJPENNLF Alpha U 1.42 +/-0.962 0.700 +/-0.968 1.51 pCilL ATHiI 07/22/04 0419 350128 2 Beta 3.95 +/-1.49 1.15 +/-1.49 2.36 pCilL Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-AL STNDAfXPENN Tritium U 47.7 +/-176 146 +1-176 292 pCilL iJLB1 07/14/04 2302 345392 3 The following Prep Methods were performed Method Description Analyst Date TIme Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 The following Analytical Methods were performed Mfethod Description I EPA 90i.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| Page 90 of 118
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddamn Neck Plant
| |
| ;362 Injun Hollow Road East Hampton, Connecticut 06424. Report Date: July 27,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 -. I Page 2 of 2 Client Sample ID: MW507S-0204-001 Proiect: -. YANK00304 Sample ID: 115774012 Client ID: YANKOOI Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch V BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 91 of 118
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| | |
| LC LA NG GE GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW503-0204-001 Proiect: YANK00304 Samrnle ID: 115774013 Client ID: YANKO01 Mattnx: Ground Water Vol. Recv.:
| |
| Collect Date: 22-JUN-04 Receive Date: 28-JUN-04 Collector: Client Parameter Qualifier Result Uncertainty LC TPU MlDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamma4Liquid-A4l-GAM2,STND,M14XPENNLF Americium-241 U 5.17 +1-9.57 6.53 +/-9.38 13.5 pCi/L SRB 07/21/04 1957 346796 1 Cesium-134 U -0.588 +J 1.52 1.17 +/-1.49 2.52 pCi/L Cesium-137 U -0.615 +/-1.40 1.10 +1-1.38 2.35 pCi/L Cobalt-60 U 0.0962 +/-1.38 1.13 +1-1.35 2.50 pcVtL Europium-152 U 1.34 +/-4.08 3.29 +J-3.99 6.88 pCi/L Europium- 154 U -3.43 +1-4.10 2.98 +/-4.02 6.61 pCi/L Europium-155 U 1.60 +1-4.54 3.89 +1-4.45 8.04 pCiLL Manganese-54 U 0.00 +/-3.48 1.06 +/-3.41 2.28 pCi/L Ul Niobium-94 U -0.278 +1-1.26 0.997 +/-1.23 2.13 pCi/L Silver-108m U 0.132 +/-1.25 1.05 +/-1.22 2.22 pci/L Rad Gas Flow Proportional Counting GrossA/B, liquid-ALLSTNDMIXPENNLF Alpha 3.23 +1-0.890 0.439 +/-1.29 0.985 pCi/L ATHII07/22104 0421 350128 2 Beta U 1.74 +1-1.30 1.04 +1-1.31 2.14 pCilL Rad Liquid Scintillation Analysis LSC, Tritium Di, Liquid-ALLSTNDMIXPENN Tritium U 168 +/-186 151 +/-186 303 pCi/L JLB I 07/15/04 0004 345392 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQII 07/14/04 1721 345045 The following Analytical Methods were performed Mlethod - Description I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report arc defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| Page 92 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Chadeston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analsis Company: CYAPCo Address: Haddarn Neck Plant
| |
| - 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW503-0204-001 Proiect: *YANK003O4 Sample ID: 115774013 Client ID: YANKOO1 VAN 17V ,.
| |
| V UA. ACV..
| |
| Parameter Quallhfer Result UncertaInty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed forbut not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| x Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| ,A Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance 'with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Page 93 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savago Road Charleston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: lladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PON 002337 Page I of 2 Client Sample ID: MW502-0204-001 Proiect: YANK00304 Sample ID: 115774014 Client ID: YANK001 Matrix: Ground Water Vol. Remv.:
| |
| Collect Date: 22-JUN-04 Receive Date: 28-JUN-04 Collector. Client Parameter Qualifler Result Uncertainty LC TPU AIDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gamnaspec, Gamm4Liquid-ALr, GAM2 STND, MIX,PEN, LF Americium-241 U -2.99 +/-11.7 8.96 +t-11.5 18.6 pcVfL SRB 07t21/04 2008 346796 1 Ccsium-134 U 0.405 +/-1.35 1.13 +/-1.33 2.43 pCi/L Cesium-137 U 0.00859 +1-2.48 1.06 +4-2.43 2.26 pCi/L Cobalt-60 U 0.176 +/-1.43 1.05 +1 1.40 231 pCV/L Europium-152 U 1.64 +t-3.S7 3.17 +1-3.79 6.62 pCV/L Europium-154 U -0.694 +/-3.61 2.94 +t-3.54 6.45 pCi/L Europium-155 U 2.48 +t4.92 4.23 +t-4.82 8.75 pCi/L Manganese-54 U -0.638 +t-1.23 0.944 +1-1.20 2.04 pCV/L Niobium-94 U 0.341 +/-1.03 0.871 +/-1.01 1.86 pCi/L Silver-108m U 0.562 +/-1.13 0.987 +1-1.11 2.08 pCIIL Rad Gas Flow Proportional Counting GrossA/B, liquid-ALUSTNDMJXPENNLF Alpha U 1.65 +/-1.12 0.832 +/-1.18 1.77 pci/L ATHI 07/22104 0421 350128 2 Beta 5.02 +1-1.39 1.03 +1-1.48 2.12 pci'L Rad Liquid Scintillation Analysis LSC Tritium Dist, Uquid-AL.STND.M1XPENN Tritium U 141 +1-184 151 +1-184 302 pCi1L JLBI 07/15/04 0107 345392 3 The following Prep Methods were performed Mfethod Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 Ihe following Analytical Methods were performed Method Description I EPA901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| Page 94 of 118
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| LLC GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road EFst Hampton, Connecticut 06424 Report Date: July 27,2004 Contact. Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW502-0204-001 - Proiect: YANKO0304 -
| |
| Sample ID: 115774014 Client ID: . YANK001 V1 IN-.
| |
| P . . Q enP DF. a ea d Parameter Quali~er Result Uncertalnty LC TPU -MDA Units DF. Analystl):te LMie Batch Mtd.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration'range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| a Sample preparation or preservation holding time exceeded.
| |
| above sample is reported on an "as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| .,c CJ, Reviewed by Page 95 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater POt#002337 Page I of 2 Client Sample ID: MW505-0204-001 Proiect: YANK00304 Samnple ID: 115774015 Client ID: YANKOOI Matnx: Ground Water Vol. Recv.:
| |
| Collect Date: 22-JUN-04 Receive Date: 28-JUN-04 Collector. Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamm4Liquid-ALLrGAM2,STNDA1OXPENNLF Americium-241 U 1.95 +/-2.48 2.11 +1-2.43 4.34 pCV/L SRB 07/21/04 2009 346796 1 Cesium-134 U -0.123 +/-1.95 1.61 +/-1.91 3.43 pCi/L Cesium-137 U IA2 +/-1.84 1.47 +411.81 3.12 pCV/L Cobalt-60 U -0.459 +1-1.85 1.51 +/-1.81 3.30 pCV/L Europium-152 U 0.542 +/-3.97 3.30 +/-3.89 6.92 pCVlL Europium-154 U -2.45 +/-4.65 3.69 +/-4.55 8.12 pCV/L Europium-155 U -2.45 +1-4.15 3.24 +/-4.07 6.69 pCV/L Manganese-54 U -1.86 +/-1.76 1.32 +/-1.72 2.84 pCV/L Niobium-94 U 0.898 +1-1.61 IA0 +1-1.58 2.96 pCV/L Silver-108m U 0.0578 +1-1.40 1.14 +/-1.37 2.40 pCY/L Rad Gas Flow Proportional Counting Gross AB, liquid-AL4STNDMlXPENMLF Alpha 1.82 +/-0.738 0.411 +/-0.756 0.934 pCo'L ATIil 07/23/04 0311 3501282 Beta 4.88 +/-1.44 1.08 +1-1.45 2.22 pCVL Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-ALLSTND.MlXPENN Tritium U -11.6 +/-169 142 +/-169 284 pCi/L JLB 1 07/15/04 0209 345392 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQII1 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| Page 96 of 118
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| LLC GENERAL ENGINEERING LABORATORIES,
| |
| -GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Projects Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID:
| |
| * MW505-0204-001 Project: YANK00304 Sample ID: I15774015 Client ID: YANK00 '
| |
| Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF' AnalystDate Time Batch Mtd.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary packaje or contact your project manager for details.
| |
| k na Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on' an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik Reviewed by
| |
| : .- I Page 97 of 118
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| | |
| a-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PON 002337 Page I of 3 Client Sample ID: MW-103S-0204-001 Proiect: YANK00304 Sample ID: 115774016 Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU hIDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Alpha Spec Analysis AlphaspecPu ULiquid-ALL Plutonium-238 U 0.0612 +1-0.108 0.0795 +/-0.109 0.230 pCi/L JASI 07/17/04 1640 347828 1 Plutonium-239/240 U -0.0127 +/-0.0175 0.0425 +/-0.0176 0.156 pCilL Am241,Cm Liquid-ALL Americium-241 U 0.0029 +/-0.091 0.0954 +1-0.091 0.256 pCitL JASI 07/17/04 1640 347826 2 Curium-242 U -0.0128 +1-0.0553 0.043 +1-0.0553 0.158 pCVL Curium-243/244 U 0.0329 +1-0.102 0.0915 +/-0.102 0.248 pCitL Liquid Scint Pu241, Liquid-ALL II Plutonium-241 U -8.25 +1-8.25 7.11 +t-8.28 14.5 pCVL JASI 0721/04 0656 347829 3 Rad Gamma Spec Analysis Gammaspec, GammaLiquid-ALL GAf2, STND MX, PENN,LF Americium-241 U -3.5 +/-8.16 657 +/-8.00 13.5 pCitL SRB 07121/04 2015 3467964 Cesium-134 U 1.61 +/-2.18 1.72 +/-2.13 3.68 pCtL Cesium-137 7.50 +1-5.54 1.57 +1-5.43 3.33 pCitL Cobalt-60 11.4 +/-3.62 1.42 +1-3.55 3.13 pCitL Europium-152 U -0.506 +1-5.19 4.27 +1-5.08 8.90 pCitL Europium-154 U -1.84 +1-5.20 4.06 +1-5.09 8.90 pCitL Europium-155 U 0.135 +1-6.76 5.44 +t-6.62 11.2 pCitL Manganese-54 U -0.731 +/-1.81 1.46 +t-1.77 3.13 pCitL Niobium-94 U 1.03 +1-1.86 1.55 +1-1.83 3.27 pCVL Silver-108m U 0.802 +/-1.89 1.59 +t-1.86 3.31 pCitL Rad Gas Flow Proportional Counting GFPC, Sr90, liquid-ALL,M/X Strontium-90 1.34 +1-0.661 0.474 +/-0.751 1.08 pCtL HOBI 07/27/04 0930 351394 5 GrossA/B, liquid-AL4LSND.MlXPENNLF Alpha 233 +/-1.00 0.666 +t-1.02 1.44 pCitL ATHI 07/23/04 0311 3501287 Beta 23.5 +/-1.91 1.10 +/-2.14 2.25 pCi/L Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-ALSTND,MlXPENN Tritium 5300 +t-304 151 +/-315 302 pCitL JLB1 07/15/04 0312 345392 8 Liquid Scint C14, Liquid-ALL Carbon-14 U -2.65 +/-6.75 5.74 +/-6.75 1 1.8 pCi/L MWX 07/03/04 0837 345987 9 1
| |
| LUquid Scit Fe55, Lquid-ALL Iron-55 U -17.9 +1-11.5 5.26 +1-11.5 10.8 pCi/L JLBI 07/11/04 0412 345524 10 Liquid Scint Ni63. Liquid-ALL Page 98 of 118
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| GEEA NIERN AOAOIS L GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charieston SC 29407- (843)55-8171 - www.gel.com Certificate -ofAnalysis Company: CYAPCo Address: -Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July27, 2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 3 Client Sample ID: MW-103S-0204-001 Proiect: YANK00304 Sample ID: 115774016 Client ID: . YANKO01 Vol. Recv.:
| |
| Parameter Q ualifier Result Uncertainty LC TPU . MDA Units DF AnalystDate i1me Batch Mtd.
| |
| Rad Llquid Sdntlllatlon Analysis LiquidScit Ni63, Liquid-ALL Nickel-63 U 5.72 +/-8.17 6.70 +/-8.17 13.8 PCiiL JLBI 07/09104 1659 345523 11 Liquid Scint Tc9, Liqud-ALL Technetium-99 U -0.421 +1-5.25 4.42 +1-5.25 9.00 POfL. DAJI 07/17/04 2346 346017 12 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch W46 3005A ICP-MS 3005 PREP CQHI 07114/04. 1721 345C45 ;
| |
| The foUowing Analyticai Methods were performed
| |
| .Method Description DOE EML HASL-300, Pu-I1-RC Modified DOE EML HASL-300, Am-05-RC Modified DOE EML HASL-300, Pu-I1-RC Modified 4 EPA 901. 1 5 EPA 905. DModified 6 EPA 905.1DModified 7 EPA 900.1 8 EPA 906.1DModified 9 EPAEER F C-01 Modified 10 DOERES SL Fe-l, Modified 11 DOE RESSL Ni-1, Modified 12 DOE EMILHASLo300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Plutonium-242 Alphaspec Pu, liquid-ALL 88 (15%-125%)
| |
| Americium-243 Am241,Cm. Liquid-ALL 88 (25%-125%).
| |
| CarrierTrracerRecovery Liquid Scint Pu241, Liquid-ALL 90 Carrier/Tracer Recovery GFPC, Sr9O, liquid-ALi.LMIX 83 Carrier/Tracer Recovery Liquid Scint F6SS, Liquid-ALL .89 Carrier/Tracer Recovery liquid Scint Ni63, Liquid-ALL 82 Carriertlraccr Recovery Liquid Scint Tc99, Liquid-ALL 100 Page 99 of 118
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 55-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: liaddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 3 of 3 Client Sample ID: MW-103S-0204-001 Proiect: YANK00304 Sample ID: 115774016 Client ID: YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 1i Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UT Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| (4NjC u Reviewed by Page 100 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SO 29407 - (843) 556-8171 - wrw.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road Easi Hampton, Connecticut 06424 -* : Report Date: July 27.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PON 002337 Page Iocf 3 Client Sarnple ID: - MW-104S40204-001 Proiect: YANK00304 -
| |
| SampleID: ' - . 115774017 Client ID: YANK0OI.
| |
| - Matrix: Ground Water Vol. Recv.:
| |
| .'- Collect Date: 23-JUN-04
| |
| - -- -Receive Date: ' 28-JUN-04' :.
| |
| f~n-t Parameter .. Quallifer. Result Uncertainty LC TPU MDA Units DF AnalystDate TIme Batch Mtd.
| |
| Rad Alpha Spec Analysis Alphaspec Pu, Liquid-ALL Plutonium-238 U 0.0504 +1-0.126 0.110 +/-0.126 0293 pCniL JASI 07/17/04 1640 347828 1 Plutonium-239/240 U 0.115 41-0.120 0.0529 +/4.120 0.178 pCi/L Am241Cmn.4quid-ALL Americiumr-241 U - 0.0S88 +1-0.0938 0.0641 4-.0941 0.190 JASI *07/17/04 1640 347826 2 0.0449- +/40.0717 pCi/L Curium-242 U . 0.0291 +14.0719 0.127 Curium-243/244 U 0.00184 +/-0.0707 0.0742 +/-0.0707
| |
| * 0211 pCifL liquidScint Pu241, Liquid-ALL Plutonium-241 - U 0.693 +/-8.41 7.04 +1-8AI .14.4 JASI 07/21/04 0727 347829 3 Rad Gamma Spec Analysis pCi/L Gammapec, Ga-maLlquid-ALLGAMZSTND.MIXPEPNLF Americium-241 U -139 +/-7.12 6.06 +-6.98 12.6' SRB 07/21V04 2031 346796 4 Cesium-134 U 1.03 +1-1.4S 1.27 ,+1-IA2 2.72 Cesium-137 U -0.227 +/-1.28 1.05 +/-1.26 2.26 pCa/L Cobalt-60 6.28 +1-2.06 2.08 +/-2.02 4A0 Europiuin-152 U 3.01 +14.16 3.49 +1-4.08 7.28 Europium-154 U *0.259 *+/-3.69 2.98. +1-3.62 6.60 pCiIL Europium-lSS U -1.23 +14.84 4.05 +t-4.75 837 Manganese-54 U 1.82 +1-1.94 1.08 +/-1.90 233 Niobium-94 . U 1.11 +1-1.19 1.06 +1-1.16 2.26 Silver-108m U 0.885 +1-1.25 1.04 +/-1.22 2.21 Rad Gas Flow Proportional Counting pCi/L GFPC,Sr90, liquid-ALEMJX
| |
| -Strontium-90 ' U -0.0679 +140.528 0.605 +/-0.528 135 pCi/L HOBI 07127/04 0931 351394 5 GrossABI liquid-AL.STND,MIXPENNLF Alpha ' . 2.49 +/-0.789 0.357 - +/-0.796 0.838 ATHI 07123/04 1622 350128 7
| |
| * Bcta. 6.23 +1-135- 0.966' +1-1.36 ' 1.99 pCi/L
| |
| .Rad Liquid Sdntillation Analysts LSC Titium Dist LJquld-ALSTNDMlXPElN Tritium. U . 241 4+1-190 153. +/-190 306 pCi(L JLBI 07/15/04 Oi4 3453928 LiquidScint C14, Liquid-ALL . .+ :
| |
| Carbon-14 U 1.35 +/-6.84 5.70 +t-6.84 11.7 pCi/L MWX 07/03/04 0908 345987 9 tfquidScti FeSS, Lquid-ALL Iron-55 U . -27.1 +/-12.3 5.66 :+/-12.4 11.6 pCi/L JLBI 07/11/04 0545 345524 10
| |
| . ' . LiquidScm: Ni63,Liquid-ALL Page 101 of 118
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| | |
| _ _ _ a-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5564171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 2 of 3 Client Sample ID: MW-104S-0204-001 Project: YANK00304 Sample ID: 115774017 Client ID: YANK001 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU AIDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Liquid Scintillation Analysis LiquidScintNi63, Liquid-ALL Nickel-63 U 6.13 +/-750 6.12 +t-750 12.6 pCi/L JLBI 07/09104 1731 345523 11 Liquid Scint Tc99, Liquid-ALL Technetium-99 U 0.557 +1-5.24 4.39 +l-5.24 8.94 pCWlL DAJI 07118104 0034 346017 12 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQIII 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Pu-i I-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA901.1 5 EPA 905.0 Modified 6 EPA 905.0 Modified 7 EPA 900.0 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE RESL Fe-l, Modified 11 DOE RESL Ni-l, Modified 12 DOE EML IIASL-300, Tc-02-RC Modified SurrogatelTracer recovery Test Recovery% Acceptable Limits Plutonium-242 Alphaspec Pu, Liquid-ALL 98 (15%-125%)
| |
| Arnericium-243 Am241,Cm, Liquid-ALL 91 (25%-125%)
| |
| CarrierfTracer Recovery Liquid Scint Pu241, Liquid-ALL 92 Carrier/Tracer Recovery GFPC, Sr90, liquid-ALL,MIX 82 Caffier/Tracer Recovery Liquid Scint Fe55, Liquid-ALL 88 Carrier/Tracer Recovery Liquid Scint Ni63, Liquid-ALL 91 Carrierlrracer Recovery Liquid Scint Tc99, Liquid-ALL 101 Page 102 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company:' CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwatcr PD# 002337 Page 3 of 3 Client Sample ID: MW-104S-0204-001 Proiect: YANK00304 Sample ID: 115774017. Client liD: YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Tine Batch Mtd.
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instnument calibration range.
| |
| 1:H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summamy package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlk.
| |
| Reviewed by Page 103 of 118
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hlampton, Connecticut 06424 Report Date: July 27,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 3 Client Sample ID: MW-106S-0204-001 Proiect: YANK00304 Sample ID: 115774018 Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 22-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Alpha Spec Analysis Alphaspec Pu, Liquid-ALL Plutonium-238 U 0.0261 +/-0.114 0.115 +/-0.114 0.294 PaiL JASI 07117/04 1640 347828 1 Plutonium-2391240 U -0.0228 +/-0.0223 0.0541 +/-0.0224 0.172 PaiL Am241,Cm, Liquid-ALL Americium-241 U -0.0265 +l-0.0683 0.093 +/-0.0684 0.264 pCi/L JAS I 07/17/04 1640 347826 2 Curium-242 U -0.0309 +1-0.0699 0.0733 +l-0.0699 0.234 pCiIL Curium-243/244 U -0.0532 +P-0.0968 0.132 +1-0.0971 0.342 pCi/L LiquidScint Pu241, Liquid-ALL Plutonium-241 U -4.0 +1-8.70 7.39 +/-8.71 15.1 pCi/L JAS I 07/21/04 0759 347829 3 Rad Gamma Spec Analysis Gammaspe4, GainmmuLiquid-ALL GA3I2,STNDM1XPENMLF Americium-241 U 9.75 +/-15.7 9.51 +1-15.4 19.6 pCfl, SRB 07121/04 2032 346796 4 Cesium-134 U 0.585 +1-1.59 1.32 +l-1.56 2.84 pCiVL Cesium-137 U 0.532 +/-1.46 1.22 +/-1.44 2.61 pCifL Cobalt-60 U 0.809 +1-1.55 135 +/-1.52 2.95 pCVL Europium-152 U -1.18 +/-4.16 3.40 +/-4.08 7.14 pCliL Europium-154 U 1.32 +/-3.63 3.13 +/-3.55 6.96 Europium-155 U -0.226 +l-6.46 5.19 +1-6.33 10.7 pCiLL Manganesc-54 U 0.217 +/-1.43 1.22 +/-1.40 2.63 PCVL Niobium-94 U -0.426 +1-1.25 0.969 +/-1.22 2.09 pCVL Silver-108m U -0.0648 +l-1.32 1.09 +1-1.30 2.30 pCVL Rad Gas Flow Proportional Counting GFPC, Sr90, liquid-AlLMlX Strontium-90 3.17 +/-0.961 0.582 +1-1.33 1.31 pCi/L HOBI 07/27/04 0947 351394 5 Gross AB, liquid-ALLSTND,M4IXPENNLF Alpha 2.73 +/-1.09 0.600 +l-1.42 1.34 pCi/L ATH 1 07124/04 0410 350128 7 Beta 19.5 +l-2.05 1.26 +l-2.82 2.58 pCi/L Rad Liquid Scintillation Analysis LSC Triuium Dist, Liquid-ALSNDAMfXPENN Tritium 850 +/-205 151 +/-205 302 pCi/L JLB I 07115/04 0517 345392 8 LiquidScint C14, Liquid-ALL Carbon-14 U -4.53 +/-6.67 5.74 +l-6.67 11.8 pCiIL MWX 07/03/04 0940 345987 9 1
| |
| LiquId Scint Fe55, Liquid-ALL Iron-55 U -213 +l-12.5 5.60 +/-12.5 11.5 PaVli JLBI 07/11/04 0718 345524 10 Liquid Scint Ni63, Liquid-ALL Page 104 of 118
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| | |
| GEEA ENIERN GENERAL ENGINEERING LABORATORIES, LLC.
| |
| 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddarn Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 3 Client Sample ID: MW-106S-0204-001 Proiect: YANK00304 Sample ID: 115774018 Client ID: YANKOOI.
| |
| Vnl. Rscv-:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA . Units DF AnalystlDate Time Batch Mtd.
| |
| Rad Liquid Scintllation Analysis LiquidScintNi63, Liquid-ALL Nickcl-63 U -0.217 +1-6.74 5.66 +t-6.74 11.7 pCiIL, lLBI 07/09/04 1803 345523 11 Liquid Scint Tc99, Liquid-ALL Technetium-99 U -7.78 +/-8.26 7.08 +t-8.26 14.4 pCi/L DAJI 07/18/04 0122 34601712
| |
| -ML- hJ7VW A W .4%' A. .-.-- -
| |
| Method Description Analyst - Date TIme Prep Batch
| |
| * WA63005A 1CP-MS 300S PREP CQHI 07114/04 1721 345045 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Pu-1lI-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 901.1 S EPA 905.0 Modified 6 EPA 905.0 Modified 7 EPA 900.0 8 EPA 906.0 Modified 9 EPA EERF C-01 Modified 10 DOE RESL Fe-l, Modified 11 DOE RESL Ni-I, Modified 12 DOE EML HASL-300, Tc-02-RC Modified Surrogatetlracer recovery Test Recovery% Acceptable Limits Plutoniur-242 Alphaspec Pu, Liquid-ALL 93 (159-125%)
| |
| Americium-243 Am241,Crn, Liquid-ALL 80 (25%-125%)
| |
| * Carrier/Tracer Recovery Liquid Scint Pu241, Liquid-ALL 87 Carrier/Tracer Recovery GFPC, Sr9O, liquid-All,MIX 76 Carrier/Tracer Recovery Liquid Scint Fe55, Liquid-ALL 92
| |
| *Carrier/Tracer Recovery Liquid Scint Ni63, Liquid-ALL 97 Carrier/Tracer Recovery Liquid Scint Tc99, Liquid-ALL- 62 Page 105 of 118
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| | |
| GENERAL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Ilollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO#002337 Page 3 of 3 Client Sample ID: MW-106S-0204-001 Proect: YANK00304 Sample ID: 115774018 Client ID: YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the insthument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by Wi C-L9 Page 106 of 118 LLCLABORATORIES, ENGINEERING
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| | |
| GENERAL~~~~~~AOAOIS ENIERN L GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556 8171 - www.gel.com Certificate of Analysis Company: CYAPCo -
| |
| Address: Haddam Neck Plant 362 Injun Hollow Road East Hamptoni Connecticut 06424 Report Date:' July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project8 'Quarterly Groundwater PO# 002337 Page 1 of 3 Client Sample ID: MW-106D-0204-001 Proiect: YANK00304 Sample ID: 115774019 I Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date:. JUN-04 Receive Date: 28-JUN-04 -
| |
| Collector. ' Client Parameter, . Qualifier. Result Uncertainty LC TPU MDA Units DF AnalystDate Time BatchMtd.
| |
| Rad Alpha Spec Analysis AIphaspecPu,Liquid-ALL-
| |
| 'Plutonium-238 U 0.0251 +/-0.0706 0.055 /4-0.0707 0.175 pCV[L JAS I 07/17/04 1640 3478281 Plutonium-2391240 U 0.0125 +/-0.0499 0.0389 +1-0.0499 0.143 pCV/L Am241,Cm, Liquid-ALL Americium-241 U 0.0901 +t-0.135 - 0.101 +/-0.136 0275 pCi/L JASt 07/17/04 16403478262 Curium-242 U -0.061 " +1-0.105 0.0681 +t-0.106 0217 pOi/L Curium-243/244 U -0.0881 +1-0.0952 -0.144 +/-0.0958 0360 pOi/L K..Liquid Scffnt Pa241, Liquid-ALL Plutonium-241 U -IA9 .+/-836 7.05 ' +-8.37 14A JASI 07/21/04 0831 347829 3 Rad Gamma Spec Analysis Gamnuaspec, GammaLiquid-
| |
| .ALI.GAZSZND,MIxPFNNLF Amcricium-241 U 4.40 +/-10.4 838 +t-10.2 17.4 ..pCi/L SRB 07/21/04 2047 3467964 Cesium-134 U 0.105 +1-133 1.09 +/-131 237 pOi/L Cesium-137 U -0.302 +1-1.22 0.981 +1-1.19 2.11 pCi/L Cobalt-60 U 0.167 +/-1.26 1.06 41-1.24 236 pOi/L Europium-152 U .123 +t-3.98 '326 +1-3.90 6.83 pCi/L Europium-154 U 1.74 +1-331 2.94 +1-325 6.51 pO/l.
| |
| Europium-155 U *0386 +1-5.22 *4.47 +1-5.12 9.23 pcd/L Manganese-54 U 0.0915 +1-138 0.988 +/-1.35 2.14 pa/L MNobium-94 U 0.354 +1-1.13 0.951 +1-1.10 2.04 palL.
| |
| Silver-108m U -0215 +/-1.23 1.04 +1-121 2.19 pOi/L Rad Gas Flow Proportional Counting GFPC Sr90, liquid-AELMIX Strontium-90 U 0.549 +-0580 0.528 +14.601 1.20 ..pO/L HOBI1 07T27/04 0947 351394 5 GrossAB, liquid-AFllSTND,MIXPEWNLF Alpha 1.16 -+-0.687 -' -0.4341 +1-0.692' 0.983 pCi . ' ATHI 07124/04'0420 350128 7 Beta 323 '+-14A91 1.17 +/-IA9 2.40 ' pOCL Rad Liquid Sdntllatlon Analysis LSC, Trium Disr, Liquid-ALL.SNDMAXPENW Tritium 1520 +/-219 '149 +/-221 297 pCilL. JLB I 07/15104 0619 345392 8 Liquid Scint C14, Liquid-ALL MWX 07/03/04 1012 345987 9 Carbon-14 U 3.53 +/-6.99 5.77 +/-7.00 11.9 I pO/IL Liquid Scntme55, F Lquid-AZL Iron-55 U -25.1 +/-12.4 5.67 +/-12.5 11.6 ' pCi/L "LI 07/11/04 0851 345524 10
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| <,.iquidScint Ni63, Liquid-ALL Page 107 of 118
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 27, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 3 Client Sample ID: MW-106D-0204-001 Proiect: YANK00304 Sample ID: 115774019 Client ID: YANK001 Vol. Recv.:
| |
| Parameter Quallfi4 lr Result Uncertainty LC TPU MIDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Liquid Scintillation Analysis LiquidScint Ni63, Liquid-ALL Nickel-63 U -3.19 +/-7.74 6.59 +/-7.74 13.6 pcV/L JLBI 07/09/04 1835 345523 11 LiquidScint Tc99, Liquid-ALL Technetiumn-99 U -4.65 +1-5.15 4.41 +1-5.15 8.99- pCiIL DAJI 07/18/04 0210 346017 12 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/14/04 1721 345045 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Pu-lI-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EhlL HASL-300, Pu-I I-RC Modified 4 EPA 901.1 5 EPA 905.0 Modified 6 EPA 905.0 Modified 7 EPA 900.0 8 EPA 906.0 Modified 9 EPAEERFC-01 Modified 10 DOE RESL Fe-l, Modified 11 DOE RESL N-, Modified 12 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Plutonium-242 Alphaspec Pu, Liquid-ALL 98 (15%-125%)
| |
| Americium-243 Amn241,Cm, Liquid-ALL 96 (25%-125%)
| |
| Carrier/Tracer Recovery Liquid Scint Pu241, Liquid-ALL 91 Carrier/Tracer Recovery GFPC. Sr9O, liquid-ALLWMiX 76 Carrier/Traccr Recovery Liquid Scint Fe55, Liquid-ALL 89 CarrierdTracer Recovery Liquid Scint Ni63, Liquid-ALL 75 Carrier/Tracer Recovery Liquid ScintTc99. Liquid-ALL 100 Page 108 of 118
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis
| |
| - Company: CYAPCo Address: Haddam Nock Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ReportDate: July 27,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 3 of 3 Client Sample ID: MW-106D-0204-001 Proiect: YANK00304 Sample ID: 115774019 Client ID: YANK001 VAl Rp" -
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Tlme Batdc Mtd.
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytdal holding time exceeded.
| |
| 1 Indicates an estimated value. The result was greater than the detection lirnit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| \,X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| hI Sample preparation orpreservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| 0JcoS Reviewed by Page 109 of 118
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| w-QUALITY CONTROL DATA Page 110 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Renort Date: July 27,2004
| |
| *Client:' CYAPCo Page I of 8 lladdam Neck Plant I362 Injun Hollow Road East Hampton, Connecticut
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Vorkorder: .115774 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alnha Spee Batch 347826
| |
| * QC1200660112 115774016 DUP Americium-241 U 0.0029 U ' 0.0525 pCi/L 179 (0% - 100%) JASI 07/17/04 16:40 Uncert: +/-0.091 - +/-0.147 TPU: +1-0.091 ./-0.147 Curium-242 U -0.0128 U -0.0428 , pCi/L N/A (0% - 100%)
| |
| Uncert: +/-0.0553 .+/-0.0317 TPU: +/-0.0553 +/-0.0321 Curium-243/244 U 0.0329 U -0.036 pCi/L N/A (0%- 100%)
| |
| Uncert: +/-0.102 +/-0.0914
| |
| .1 TPU: +/-0.102 +/-0.0915 QC1200660114 LCS iAmericium-241 10.7 10.3 pCi/L 96 (75%-125%)
| |
| Uncert: +/-1.00 TPU: +/-1.60
| |
| .um-242 U . -0.00501 pCi/L Uncert: +1-0.0558 TPU: +1-0.0558 Curium-243/244 13.8 14.3 pCi/L 104 Uncert: +/-1.17 TPU: +1-2.08 QC12006601 11 MB Americium-241 U -0.0053 pCi/L 07/17/04 16:40 Uncert: +1-0.059 TPU: +/-0.059 Curium-242 U -0.0322 pCU1L Uncert: +I/-0.0282 TPU: +I-0.0285 Curium-243/244 U -0.0434 pCi/L Uncert: +1-0.0664 TPU: +1-0.0666
| |
| * QC1200660113 115774016 MS Americium-241 10.7 U 0.0029 9.84 pCi/L 92 (75%-125%) 07/17/04 16:40 Uncert: +1-0.091 +1-0.951 TPU: +/-0.091 * +/-1.50
| |
| . Curium-242 U *-0.0128 U -0.0115 pCi/L Uncert: +/-0.0553 +1-0.0595 TPU: +1-0.0553 +/-0.0596 Curium-2431244 13.8 U 0.0329 13.2 pCi/L 95 Uncert: +/-0.102 +1-1.10 TPU: +/-0.102 +/-1.91 Batch 347828 QC1200660121 115774016 DUP ronium-238 U 0.0612 U 0.00102 pCi/L 193. (0% - 100%) JASI -07/17/04 16:40 Page 111 of 118
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| *1-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Chadeston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 115774 Page 2 or 8 Parmname NOM Sample Qual QC Units Rl'D% REC% Range Anist D)ate Time Rad Alpha Spec Batch 347828 Uncert: +/-0.108 +/-0.0554 TPU: +/-0.109 +1-0.0554 Plutonium-239/240 U -0.0127 U 0.00713 pCi/L NMA (0% - 100%)
| |
| Unceit: +1-0.0175 +/-0.054 TPU: +/-0.0176 +/-0.054 QC1200660123 LCS Plutonium-23S U 0.000976 pCi/L (75%-1 25%) 07/17/04 16:40 Uneert: +/-0.0531 TPU: +/-0.0531 Plutonium-239/240 9.56 9.78 pCi/L 102 (75%-125%)
| |
| Uncert: +I-0.960 TPU: +/-1.35 QC1200660120 NIB Plutonium-238 U -0.0324 pCi/L 07/17/04 16:40 Uncert: +/-0.0259 TPU: +/-0.0261 Plutonium-239/240 U -0.0162 pCi/L Uncct: +/-0.0183 TPU: +/-0.0184 QC1200660122 115774016 NMS Plutonium-238 U 0.0612 U -0.0181 pCi/L (75%- 125%) 07/17/04 16:40' -
| |
| Uncert: +/-0.108 +1-0.0617 TPU: +/-0.109 +1-0.0617 Plutonium-239/240 9.56 U -0.0127 10.4 pCi/L 109 (75%-125%)
| |
| Uncerlt: +/-0.0175 +/-1.03 TPU: +/-0.0176 +1- 1.46 Batch 347829 QC1200660133 115774016 DUP Plutonium-241 U -8.25 U -0.996 pCi/L N/A (0% - 100%) JAS I 07/21/04 09:34 Unceit: +/-8.25 +/-8.02 TPU: +/-8.28 +/-8.02 QC1200660135 LCS Plutonium-241 142 116 pCi/L 82 (75%-125%) 07121/04 10:38 Uncert: +/-10.6 TPU: +/-14.5 QC1200660132 NIB Plutonium-241 U -9.32 pCi/L 07/21/04 09:02 Uncert: +1-8.68 TPU: +/-8.76 QC1200660134 115774016 MIS Plutonium-241 142 U -8.25 110 pCi/L 78 (75%-125%) 07/21/04 10:06 Uncert: +/-8.25 +/-10.2 TPU: +/-8.28 +/-16.0 Rad Gamma Spec Batch 346796 QC1200657514 115774001 DUP Americium-241 U 3.74 U -1.61 pCi/L N/A SRB 07/21/04 19:50 Uncert: +/-10.3 +/-8.60
| |
| +/-8.42 Page 112 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary WVorkorder. 115774 3- VI 0P
| |
| - . , . JL-Ugc OU ol Parmname ' NONI ' Sample:Qual' QC Units' RPD% REC% Range AnIst Date Time Rad Gamma Spec Batch 346796 TPU: +/-10.0 Cesium-134 0.667 U 0.905 pCi/L 30 (0% -' I00%)
| |
| Uncent: +/-1.84 +/-1.37 TPU: +/-1.80 +/-1.35 Cesium-137 -0.215 U 0.376 pCilL N/A (0%- 100%)
| |
| Uncert: +/-1.89 +/-1.29 U +1-1.86 - +/-1.27 TPU:
| |
| Cobalt-60 U 5.25 U 1.02 pCi/L 135 (0%- 100%)
| |
| Uncert: 4-2.64 +1-132 TPU: +/-2.59 4+-1.29 Europium-152 U -3.42 U 0.993 pCiL N/A (0%- 100%)
| |
| Uncert: +/-5.71 +1-3.86 TPU: +/-5.59 +/-3.78 Europium-154 U 0.457 U 0.700 pCi/L 42 (0%- 100%)
| |
| Uncert: +/-5.26 - +/-3.80 TPU: +/-5.15 +/-3.73 Europium-155 0.673 U -1.69' pCuiL N/A (0%- 100%)
| |
| Uncert: +1-6.73 +/-5.14 U
| |
| TPU: +/-6.60 +/-5.04 iganese-54 U -0.585 U .'-0.193 pCi/L NIA (0%- 100%)
| |
| Uncert: +/-1.90 +/-1.24 TPU: +/-1.86 +/-1.21 Niobium-94 U 1.71 U 0.326 pCilL 136 (0%- 100%)
| |
| Uncert: +/-1.66 +/-1.12 TPU: +/-1.63 +/-1.10 Silver-lOSm U 1.50 U- 0.203 pCi/L 152 (0%- 100%)
| |
| +/-1.73 +/-1.20 TPU: +/-1.69 +/-1.18 QC1200657516 LCS Uncent:
| |
| Americium-241 '1170 .1210 pCilL 104 (75%-125%) 07/21/04 19:14 Uncert: - +/-231
| |
| * +/-226 Cesium-134 U -12.1 pCi/L TPU:
| |
| Uncet: +/-13.9 TPU: ' +/-13.6 Cesium-137 461 469 pCi/L 102 (75%-125%)
| |
| Uncert: +/-70.0 9 (75%-125%)
| |
| TPU: +/-68.6 Cobalt-60 709 '705 pCi/L. .99 (75%-125%)
| |
| Uncert: -'. +/-74A TPU: +/-72.9 Europium-152 ' -10.8 pCi/L
| |
| +/-33.0
| |
| : +/-323 Europium-154 U -9.1 pCi/L Uncert:
| |
| TPU: +1-25.1
| |
| -w-opium-155 U 18.1 *pCiL Page 113 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gei.com OC Summary Workorder: 115774 Page 4 of 8 Parmname NOM Sample Oual OC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 346796 Uncert: +1-48.6 TPU: +1-47.7 Manganese-54 4.75 pCiIL Uncert: +1-13.3 TPU: +/-13.0 Niobium-94 -1.37 pCiIL Uncert: +/-12.8 TPU: +/-12.5 Silver- 108m -1.91 pCiL Uncert: +/-12.5 TPU: +/-12.2 QC1200657513 MB Americium-24 1 4.76 pCiAL 07/21/04 20:48 Uncert: +/-6.22 TPU: +/-6.09 Cesium- 134 0.476 pCiIL Unceilt: +/-1.46 TPU: +/-1.43 Cesium- 137 0.0541 pCiIL Uncet: +/-1.26 TPU: +/-1.24 Cobalt-60 -1.21 pCiL Uncelt: +1-1.51 TPU: +/-1.48 Europium-1 52 -2.39 pCi/L Unccrt: +/4.07 TPU: +/-3.99 Europium-154 4.53 pCi/L Uncert: +/-4.04 TPU: +/-3.96 Europium- 155 3.56 pCi/L Uncert: +/-4.11 TPU: +/-4.02 Mangancse-54 -0.705 pCiIL Uncenl: +/-1.26 TPU: +/-1.24 Niobium-94 -0.846 pCilL Unceit: +/-1.37 TPU: +1-1.35 Silver-108m -1.02 pCi/L Unceut: +/-1.37 TPU: +/-1.34 QC1200657515 115774001 MS Americium-24 1 9360 U 3.74 9620 pCi/L 103 07/21/04 18:59 Uncert: +1-103 +/-2780 TPU: +/-10.0 +/-30300 Cesium-134 U 0.667 U -114 pCiIL Uncert: +1-1.84 +/-129 TPU: +/-1.80 +/-380 Page 114 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407'- (843) 556-8171 - www.gel.com QC Summary Workorder: 115774 Page 5of 8 Parmname NOM Sample Oual - Units RPD% REC% Range Anlst Date Time z
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| . Rad Gamma Spec Batch 346796 Cesium-137 3690 U -0.215 3710 pCi/L 101 Uncert: +/-1.89 -+/499 TPU: +/-1.86 +/-11700 Cobalt-60 5650 U 5.25 6050 IpCV/L 107 Uncert: +/-2.64 +/-730 TPU: +/-2.59 +1-19000 Europium-152 U -3.42 U -76.9 pCi/L Uncert: +/-5.71 +/-342 TPU: +/-5.59 +/-413 Europium-154 U 0.457 U -171 pCa/L Uncert: +/-5.26 +/-378 TPU: +1-5.15 +/-651 Europium-155 U 0.673 U -458 pCi/L Uncert: +/-6.73 +/-408 TPU: +/-6.60 +/-1490 Manganese-54 U -0.585 U 4.06 pCi/L Uncert: +1-1.90 +/-141 TPU: +/-1.86 +/-138
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| - -bium-94 U 1.71 U -492 pCi/L Uncert: +/-1.66 +1-123 TPU: +/-1.63 +/-196 Silver-108m U 1.50 U -77.5 pCU/L Uncert: +/-1.73 +/-115 TPU: +/-1.69 +/-268 Rad Gas Flow Batch 350128 QC1200665720 115774001 DUP Alpha 3 .90 U 0499 pCilL 155* (0%- 100%) ATHI 07/27/04 14:03 Uncert: +/-I1 .64 +/-0.849 TPU: +/-I, .67 +/-0.850 5 .72 U 2.03. pCi/L 95 (0%- 100%)
| |
| Uncert: +1.14 .74 +/-1.64 TPU: +/-1. .76 +/-1.64 QC1200665723 LCS Alpha . 108 116 pCi/I. 108 (75%-125%) 07/23/04 09:40 Uneert: +/-12.1 TPU: +/-14.8 Beta 367 331 pCi/I. 90 (75%-125%)
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| Uncert: +/-15.2 TPU: +/-20.1 QC1200665719 MNB Alpha U ,,-0.111 pCi/I. 07/24/04 04:20 Uncert: '+/-0.593 TPU: '+1-0.593 Beta U. -0.435 'pCi/L Uncert: +/-1.28
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| -TPU: +/-1.28 nCl200665721 115774001 MS Page 115 of 118
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| - 11 s-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary W~orkorder: 115S774 Page 6 or 8 Parninanie NONI Samnle OuDl OC Units RPD% REC%5' Rnge AnMst Date Time Rad Gas Flow Batch 350128 Alpha 108 3.90 126 pCi/L 113 (75%-125%)
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| Uncert: +1-1.64 +1-13.1 TPU: +1-1.67 +/-16.0 Beta 367 5.72 336 pCi/L 90 (75%-125%)
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| Uncert: +/-1.74 +1-15.5 TPU: +1-1.76 +1-19.8 QC1200665722 115774001 MSD Alpha 108 3.90 132 pCi/L 4* 119 (75%-125%) 07123/04 09:40 Uncert: +/-1.64 +/-12.9 TPU: +1-1.67 +1-15.1 Beta 367 5.72 358 pCi/L 6* 96 (75%-125%)
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| Uncert: +/-1.74 +/-15.9 TPU: +/-1.76 +1-22.2 Batch 351394 QC1200668743 115774005 DUP Strontium-90 U 1.33 U -0.275 pCi/L N/A (0% - 100%) IIOBI 07/27/04 12:22 Uncert: +/-0.791 +/-0.392 TPU: +/-0.872 +/-0.398 QC1200668745 LCS Strontium-90 61.1 52.1 pCi/L 85 (75%-125%)
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| Uncert: +1-3.48 TPU: +/-17.2 QC1200668742 MB Strontium-90 U -0.73 pCi/L Uncert: +/-0.347 TPU: +/-0.410 QC1200668744 115774005 NIS Strontium-90 122 U 1.33 108 pCi/L 87 (75%-125%)
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| Uncert: +/-0.791 +1-6.96 TPU: +/-0.872 +1-34.1 Rad Liquid Scintillation Batch 345392 QC1200654329 115774001 DUP Tritium U 136 U 10.0 pCi/L 0 (0%- 100%) JLBI 07/15/04 08:24 Uncert: +1-154 +/-171 TPU: +/-154 +/-171 QC1200654331 LCS Tritium 3220 3000 pCi/L 93 (75%-125%) 07/15/04 10:29 Uncert: +/-249 TPU: +/-253 QC1200654328 MIB Tritium U 62.1 pCi/L 07/15/04 07:21 Uncert: +/-157 TPU: +/-157 QC1200654330 115774001 fiS Tritium 3230 U 136 3030 pCi/L 90 (75%-125%) 07/15104 09:26 Uncert: +/-154 +/-252 TPU: +/-154 +/-257 Batch 345523 Page 116 of 118
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder. 115774 Page 7 of 8 .
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| NI MI SAmnlp Oulal '' OC- lUnins UPnm UPRF ID-v Anl,#t In.#. Tr:mP
| |
| }rnrmname
| |
| __- - *.--*---l-----"<
| |
| - . v- -- .a- Ae va1.
| |
| axn -t H..,
| |
| * Rad Liquid Scintillation Batch 345523 QC1200654549 115774016 DUP Nickel-63 U 5.72 U 10.6 pCi/L 0 (0% -100%) JLBI' 07/09/04 19:39 Uncert: +1-8.17 +1-8.94 TPU: +/-8.17. +/-8.95 QC1200654551 LCS Nickel-63 366 320 pCYL 88 (75%-125%) 07/09/0421:49 Uncert: +1-14.4 TPU: +/-15.4 QC1200654548 MB Nickel-63 U 4.42 pCi/L 07/09104 19:07 Uncert: +1-7.87 TPU: ; +1-7.87 QC1200654550 115774016 MS Nickel-63 366 U 5.72 314 pCi/L 84 (75%-125%) 07/09/04 20:11 Uncert: +/-8.17 +1-14.8 I TPU: +/-8.17 +1-15.9
| |
| .Batch 345524 QC1200654553 115774016 DUP lron-55 U -17.9 U -19.9 pCi/L N/A (0%- 100%) JLBI 07/11/04 11:58 Uncert: +1-11.5 +/-125 TPU: +1-115 +/-125 0 1 QC1200654555 LCS Iron-55 399 353 pCz/L 88* (0%-%) 07/11l0O4 15:04 Uncert: +1-17.8
| |
| . TPU: +/-22.7 QC1200654552 MIB Iron-55 U -32.7 pai/L 07/11/0 10:25 Uncert: +/-13.0 TPU: . . I
| |
| +/-13.0 QC1200654554 115774016 MS Iron-55 401 U -17.9 363 pCa/L .90* (0%-%) 07/11/04 13:31 Uncent: +1-1 15 +1-175 TPU: +1-1 15 +/-22.8 345987 QC1200655618 115774016 DUP Carbon-14 U i -2.65 U
| |
| * 2.92 pCa/L N/A (0% - 100%) M~WX 07/03/04 11:16 Uncert: +1-6.75 -+/-7.04
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| . TPU: +1-6.75 +/-7.05 QC1200655620 LCS Carbon-14 329 339 pCi/L - 103 (75%-125%) 07/03/04 12:20 Uncert: +1-14.5 TPUI: .+/-21.7 ;
| |
| QC1200655617 NIB Carbon-14 *.U 3.40 pCk' 07/03/04 10:44 Uncert: . . .U +1-6.94 TPU: +/-6.95 QC1200655619 115774016 MS Carbon-14 329
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| * U -2.65 374. pcY/L 114 (75%-125%) 07/03/04 11:48 Uncert: +/-6.75 +/-15.2 Page 117 of 118
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| *1-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 115774 Page 8 of 8 Parmname NOAM San)pl Qual C Units RPD% REC% Rtane Anlst Date Time1!
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| Rad Liquid Scintillation Batch 345987 TPU: +1-6.75 +1-23.4 Batch 346017 QC1200655690 115774016 DUP Technetium-99 U -0.421 U -1.92 pCi/L NIA (0% - 100%) DA1I 07/18/04 03:45 Uncert: +1-5.25 +/-4.89 TPU: +1-5.25 +1-4.89 QC1200655692 LCS Technetium-99 523 528 pCi/L 101 (75%-125%) 07/18/04 05:21 Uncert: +/-12.4 TPU: +1-17.2 QC1200655689 SIB Tcchnetium-99 U -5.76 pCi/L 07/18/04 02:57 Uncert: +/-5.17 TPU: +/-5.17 QC1200655691 115774016 NIS Technctium-99 523 U -0.421 543 pCi/L 104 (75%-125%) 07/18/04 04:33 Uncert: +/-5.25 +/-12.5 TPU: +/-5.25 +/-17.5 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| B3D Flag for results below the NIDC or a (lag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
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| 11 Analytical holding time exceeded.
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| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
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| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| x Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
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| N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.
| |
| ** Indicates analyte is a surrogate compound.
| |
| A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
| |
| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
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| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard tnless qualified on the QC Sutmmary.
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| Page 118 of 118
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| wa ENC/IA JJ ( GENERAL ENGINEERING LABORATORIES, LLC
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| 'U' Dy\ O aMember of THE GEL GROUP, INC.
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| <, , (I ) Meeting Today's Needs with a Vsion for Tomorrow O409 o '
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| July 30, 2004 Mr. Dave Keefer CYAPCo Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 RE: Quarterly Groundwater PO# 002337 WorkOrder: 116165 SDG: MSR#04-1807
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| | |
| ==Dear Mr. Keefer:==
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| | |
| General Engineering Laboratories, LLC (GEL) appreciates the opportunity to provide the following analytical results for the sample(s) we received on July 02, 2004. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time.
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| This data report has been prepared and reviewed in accordance with GEL's standard operating procedures. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4475.
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| Sincerely, Purchase Order: 002337 Chain of Custody: 2004-00103, 2004-00107, 2004-00113, 2004-00114, 2004-00115, 2004-001 16, 2004-00118, 2004-00119,2004-00120 and 2004-00121 Enclosures RO. Box 30712
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| * Charleston, SC 29417
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| * 2040 Savago Road (29407)
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| Phono (843) 556-8171
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| * Fax (843) 766-1178 - www.gel.com
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| | |
| U-CONNECTICUT YANKEE RE: Quarterly Groundwater PO# 002337 Work Order: 116165 SDG: MSR#04-1807 116165001 NIIW llOS 116165002 NMW 122D 116165003 MW 109D-0204-001 116165004 MWI-107S-0204-001 116165005 IN 1O7D-0204-001 116165006 MiV1 1OD-0204-001 116165007 MWXV113S-0204-001 116165008 MIW112S-0204-001 116165009 MW1O2S-0204-001 116165010 NIW-1 11S-0204-001 116165011 NIV-109S-0204-001 116165012 NIW-3-0204-001 116165013 NIWl-0204-001 116165014 N-IlW-105D-0204-001 116165015 IN 1O3D-0204-001 116165016 NWIW105S-0204-001 116165017 MW600-0204-001 116165018 MW508D-0204-001 116165019 NIW-IOOS-0204-001 116165020 MW-504-0204-001 116165021 NIWV-508S-0204-001
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| Table of Contents Case Narrative ............. ones.
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| * mo. ................. a.....a............ 1 Chain of Custody .................................................. a...... 4 Cooler Receipt Checklist ............................................ 15 Inorganic Analysis................................................................ 26 Radiological Analysis ..... . m..................................... 54 Sample Data Summary ............................................ 75 Quality Control Data ............................................ 122
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| - - - s -
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| CASE NARRATIVE 1
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| CASE NARRATIVE For CONNECTICUT YANKEE RE: Quarterly Grouniidwater PO# 002337 Work Order: 116165 SDG: MSR#04-1807 July 30,2004 Laboratory Identification:
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| General Engineering Laboratories, LLC Mailing Address:
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| P.O. Box 30712 v..
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| Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:
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| 2040 Savage Road Charleston, South Carolina 29407 Telephone Number:
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| (843) 556-8171 Summary:
| |
| Sample receipt The samples for the Quarterly Groundwater Project for work order 116165 arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina July 2, 2004 for environmental analysis. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures. ,
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| The laboratory received the following groundwater samples:
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| MWV 110S MV-3-0204-001 MW 122D MW1-0204-001 MW 109D-0204-001 MW-105D-0204-001 MNW-107S-0204-001 MW103D-0204-001 MW 107D-0204-001 MW105S-0204-001 MW11OD-0204-001 MW600-0204-001 MW1 13S-0204-001 MW508D-0204-001 MWV112S-0204-001 MW-10OS-0204-001 MW102S-0204-001 MW-504-0204-001 MWV-I1IS-0204-001 MW-508S-0204-001 MNV-109S-0204-001 GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
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| P.O. Box 30712 - Charleston, SC 29417 - 2040 Savage Road (29407)
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| Phone (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com AL~
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| | |
| Items of Note:
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| There are no items to note.
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| Case Narrative:
| |
| Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.
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| Analvtical Request:
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| Ten groundwater samples were analyzed for MIX, four were analyzed for STND, four were analyzed for ALL, and two groundwater samples were analyzed for STND and Sr-90.
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| Internal Chain of Custodv:
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| Custody was maintained for all of these samples.
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| Data Packagtg:
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| The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Laboratory Certifications, and Radiochemistry.
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| I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.
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| GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
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| RO. Box 30712 - Charleston, SC 29417
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| * 2040 Savage Road (29407)
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| Phone (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com
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| | |
| CHAIN OF CUSTODY 4
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| | |
| Health Physics Procedure GPP-GGGR-R5 104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00121 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 Codiea STmpe CoSizner Analytical Lab (Name, City, State): Code &Type General Engineering Lab (GEL), 2040 Savage Rd, Code X Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) <
| |
| Priority: [145 D. Z 30 D. El 14 D. El 7 D.
| |
| Other:
| |
| Sample Designation Date Time Comment, Preservation Lab Sample ID M Jl 1OS 0l3010Y 0 WG G 4L, 1L =< O ,
| |
| =N0 1 _ _M
| |
| \ W 122 D 6130Ja qI !5 WG G 4L, IL XnoA WG G 4L,lL L WG G 4L,1L L WG G 4L, IL NOTES: PO#: 002337 MSR#: 04-1807 El LTP QA El Radwaste QA Z Non QA Samples Shipped Via: Internal Container 0 Fed Ex Temp.:_Deg.C.
| |
| El UPS Requested analyses should be performed to typical groundwater program MDC's. LI Hand Custody Sealed?
| |
| YO NO
| |
| : 1) Relinquished By: Date/Time 2) R e ived By Date/Time Custody Seal Intact?
| |
| : 3) Relinquished By
| |
| - 76 /'/.c 7/
| |
| Date/Time 4)
| |
| /
| |
| eived By 7 /)j(q Dattrrime Li Other__
| |
| D
| |
| _ O . Y NO Bill of Lading #
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time I
| |
| I
| |
| | |
| ~- - HealC ehysics Procedure C GPP-GGGR-R5 104-003-Attachment B-C 2 001 Major Connecticut Yankee Atomic Power Compatny--fCutdyFr.-...- ChainofCsdyFr No. 2004-00114 362 Injun Hollow Road, East Hampton, Cr 06424.
| |
| ~860-267-2SS6 ---
| |
| Proj ect Name: Haddam Neck Decommissioning .Analyses Requested ___ Lab Use Only,. ;%4-.--
| |
| Contact Name &Phone:- :7-*. 4 .. ,-. ,.:.7 ,7 Rich McGrath 860-267-3573 MdaSml otie
| |
| _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Code Type . Size- -
| |
| Analytical Lab (Name, City, State): Code &Type tt 2 General Engineering Lab (GEL), 2040 Savage Rd,Coe.. .
| |
| Charleston, SC 29407,- 843.556.8171 (Sarah Kozlik) 7VV Priority: E145 D. Z30D.F- 14 D.EM7D.' 4 Oth e r:. _ _ _ _........_...
| |
| Sample Designation Date time ____Comment, Preservation Lb Sampile I
| |
| ___II_________- u e S WG G 4L,IL - 483J03 t~- Jvq..
| |
| W- /07S -67.O-0V1 /9o 13/0 WG G 4L,IL X ~ - ..
| |
| _ __WG G 4L, IL _ _ _ _ _ _ _ _
| |
| _ _ _ _ _ WG G 4L, IL ... . .~
| |
| _ __ _ _ _ WG G 4L,1IL _ _ _ _ _ _ _ _ _ _ _ _
| |
| NOTES: P0 #: 02337 MSR #:04-1807 l LTP QA FIJRadwaste QA Z No'n QA Samples Shipped Via: Itra oti~
| |
| De Fed Ex TMP C.
| |
| Requested analy'ses'should be performed to typical groundwater program MDC's. EHadCustody Sealed l)ei~hcB.Dt/ie 2) Rec i'ved By Dat ElOthemCutod Sea l intat
| |
| : 3) Relinquished By Date/Time .. 4) Aecived gy Dat'e/Time _________ ON Bill of Lading I 5ReiqihdB-.Date/Time 6) Received By .Date/Time
| |
| | |
| Health Physics Procedure GPP-GGGR-R5 104-003-Attaclmient B-CY-00 1Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00119 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommnissioning Analyses Requested Lab Use Only Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 Mcdia Code Sample Type Container Size-Analytical Lab (Name, City, State): Code &Type General Engineering Lab (GEL), 2040 Savage Rd, C ff<
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) ¢ Priority: 0 45 D. [ 30 D. El 14 D. E 7 D.
| |
| Other:
| |
| Sampleepesignation Date Time Comment, Preservation Lab Sample ID wŽc/cD( I 3co' /c3c6 WG G 4L, 1L - _
| |
| -i _ _____- _
| |
| *)l~ullXN~O3 tOOI e13 )3,k.l WG G 4L, IL 7- ___ - - 4 WG G 4L,1L /
| |
| WG G 4L,1L L
| |
| _ _ _ _i_ _W G G L 4L, ILi___1____
| |
| NOTES: PO#: 002337 MSR#: 04-1807 El LTP QA E RadwasteQA 1 NonQA Samples Shipped Via: Internal Container El Fed Ex Temp.: - Deg. C El UPS Requested analyses should be performed to typical groundwatcr program MDC's. El Hand Custody Sealed?
| |
| -YO NO0
| |
| : 1) Relinquisb By:
| |
| 7///OL(
| |
| Date/Time
| |
| //..&
| |
| : 2) Re cived By
| |
| - 7 / p/2,LI/&1 4w de Date/Tine oOhr
| |
| /~y,3 lOther Custody Seal Intact?
| |
| : 3) Relinquished By Date/Tite 4yRtceivt/d By Date/Time . _. Y.O NO Bill of Lading #
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time
| |
| (
| |
| | |
| Heal~ti r'hysics Procedure
| |
| ( GPP-GGGR-R5 104-003-Attachment .B-C-UI01 Major
| |
| - -ChainofCsoyFr Connecticu't Yainkee' Atomfic i Poweir Company oCutdFrmNo. 2004-00103 362 Injun Hollow Road, East Hampton, CT 0642.4 860-267-2556 _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
| |
| Project Name: Haddam Neck Decommissioning Analyses Requested 'a s.ny Contact Name & Phone: ',r Rich McGrath 860-267-3573 MdaSml Code Type otie Size-
| |
| ...--- 4
| |
| ''~-~' -
| |
| Analytical Lab (Name, City, State): Code &Type LI General Engineering Lab (GEL), 2040 Savage Rd, Cd Charlest'on, SC 29407, 843.556.8 171 (Sarah KozUi)
| |
| Priority:45 D. 30 D. Ij4lbDME7D.
| |
| Other: ___ __ - 74~4*4~~4
| |
| "'J Sample Designation Date Time Comment, Preservation L_" Liihb S1mple 11)b o '~10 t Woc IO 3O WG . G 4L, IL 1,1,WJ
| |
| ( 3. WG G 4L,1IL_ _ _ _ _ _ _ _ _ _ _
| |
| __ _WG G 4L,IL _ _ _ _ _ _~
| |
| WG G 4L 1L_ _ _ _ _ _ _ _
| |
| WG G 4L,IL _ _ _ _ _ _ _ _ _ _ _ _
| |
| NOTES:'P0 MI002337 MSR #M04-1807 ] UTP QA El Radwaste QA Z Non QASapeShpdVi: nenlCotnr 0Fed Ex Tm e Requested' analyses should be performed to.!ypical groundwater program MDC's. 5 Hand ,CsdySaed?'
| |
| Y0 N 1)Relinquished By-... D tWITime 2)R By DtlireCsol Sa nat
| |
| .. Oter 4r, 5)Relinquished By Date/Time 6)Rceive By Date/Time _
| |
| 444 *Bill'4of4Lading
| |
| . .44 -
| |
| | |
| Health Physics Procedure GPP-GGGR-R5 104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00115 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 Media Code Sample Type Contaer Size-Analytical Lab (Name, City, State): Code &Type General Engineering Lab (GEL), 2040 Savage Rd, Code Charleston, SC 29407, 843.556.8171 (Sarah Kozlik)
| |
| Priority: El45 D. 30 D. 14 D. 7 D.
| |
| Other: 0 Sample Desiglation Date Time Comment, Preservation Lab Sample ID v \ *S-CDQ9lfo Y142 91q R/° I WG G 4L, IL -l -l - t J
| |
| . k v^\i I3-&2- WG G 4L, 1L - X ... LA:NLi , M t.t_ .KL1A -
| |
| WG G 4L, 1L __'__a
| |
| * H~C3
| |
| __ _ WG G 4L,1L L WG G 4L,iL L NOTES: PO#: 002337 MSR 04-1807 El LTP QA El Radwaste QA 3 Non QA Samples Shipped Via: Internal Container.
| |
| Fed Ex Temp.: _ Deg. C ElUPS Requested analyses should be performed to typical groundwater program MDC's. El Hand Custody Sealed?
| |
| - YO NO
| |
| : 1) Relinquis ed By: Date/time 2) Received By Date/Time Custody Seal Intact?
| |
| u~o~~-. El Otiler 7/J/jc1 /0:1% 0 7/861/
| |
| : 3) Relinquished By Date/Time 4) eceivel By Date/Time . YO NO Bill of Lading #
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time
| |
| (
| |
| i
| |
| | |
| H~eal~>fiysics Procedure ( GPP-GGGR-R5 104-003-Attachment B-CQJ0 1 Major
| |
| *Connefctict Yantk~eeAtomi Pow'er_ Comipan'y . Cano CsoyFr No. 2004-00113 3621Injun Hollow Road, East Hampton, Cr06424
| |
| -.. 860-267-2556 - .. -
| |
| Project Name: Haddam Neck Decommissioning Analyses Requested ___Lab. Use Ol Contact Name &-Phone: ~.. ,.,.K...~.
| |
| Rich McGrath 860-267-3573Coe Tp Sie .,,1 Analytical Lab (Name, City, State): Code &Type General Engineering Lab (GEL), 2040 Savage Rd, Coe .
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) 0 7 .......-.
| |
| Priority:- LI 45 D.[D30 D. E]14D. El7D.
| |
| -Other: **
| |
| Sample Designation Date Time ____Comment, Preservation -'5:-Lab 'Sample iD ntw-I09_S-0ozjt~ooJ .o1/2~ WG G 4L,IL - - ./JJ_____
| |
| ~r^vqIl-pOg& W ~4J16 Iqj1j Go' WG G 4L,IL
| |
| * T __ _ 1Ao,' NM~ ____
| |
| ____ __ ___ WG G 4L, IL _ _ _ _ _ _ _ _ _ _ _
| |
| __ _ ___ __ W G G A L,1IL_ ___ _ _ _ _ _ _
| |
| 7
| |
| _ _ _ _ _ _ _ _ _ _ _ _ _ _ W G G 4L,1IL_ _ _ __ _ _ _ _
| |
| NOTES: P0O# 002337 :MSR #: 04-1807 II1 UP QA LI Radw'aste QA Z Non QA Samples Shipped Via: Itra otie~
| |
| Fed ExTep DgC Requiested analyses should be performed to _typical groundwater program MDC's. I] Hand CutdySeld
| |
| : 1) Relinquish Byce .pae/imD~ate/Time*. .. - CsoySaInct
| |
| : 3) Relinquished By Date/Time 4)Re eBy 6a________ime Bill of Lading
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time.
| |
| - -. - . ..-. I . ........
| |
| | |
| Health Physics Procedure GPP-GGGR-R5104-003-Attaclunent B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No.. 2004-00107 362 Injun Hollow Road, East Haampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 Media Sample Container Code Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Lab (GEL), 2040 Savage Rd, Code Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) ....
| |
| Priority: :1 45 D. Z 30 D. El 14 D. El 7 D.
| |
| Other:
| |
| Sample Designation 01w %oS Mr 03- o:_ - oo I 10o9-004pe6o, Date 6-_ o 9- A o61 Time
| |
| _ __a_
| |
| 1W\3 WG WG G
| |
| G 4L, 1 L 4L, IL -
| |
| Z -<
| |
| Comment, Preservation
| |
| _o Lab Sample ID WG G 4L,1L _I WG G 4L, 1L WG G 4L,1L L =
| |
| NOTES: PO#: 002337 MSR#: 04-1807 El LTP QA El Radwaste QA [ Non QA Samples Shipped Via: Internal Container 1 Fed Ex Temp.: Deg. C O UPS Requested analyses should be performed to typical groundwater program MDC's. El land Custody Sealed?
| |
| ..Y NO I) Relinquishe By: Datc/Timc 2) Rectived By Date/Time Custody Seal Intact?
| |
| -1, t /-79o6 o: Elo Other
| |
| : 3) Reinquished By Date/Time 4)IRedeived By bDateTrime YO NO Bill of Lading #
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time
| |
| ( .. (
| |
| i
| |
| | |
| (..
| |
| Health tphysics P~rocedure GPP-GGGR-R5 104-003-Attachment B-CY-UO01 Major
| |
| -.Chain'of Custody Form N.20-01
| |
| -Cofinectficut Yankee Ato m-ic Po"Wer Co'mpaniy -
| |
| 362 Tnjun Hollow Road, East Hampton, Cr 06424 860-267-2556 - _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
| |
| Project Name: Haddam Neck Decommissioning 7) nlssRqetd ___:LnbUse.9l Contact Naine & Phone:
| |
| Rich McGrath 860-267-3573 Medide Sample Sotiner Cod oTye Sizpe-Analytical Lab (Name, City, State): Cd Tp General Engineering Lab (GEL), 2040'Savage Rd, od
| |
| 'Charleston, SC 29407, 843.556.8171 (Sarah Kdzlik) 7; Priority ~ D.Z 0D. 14 D.E 7 D.
| |
| Other:..........
| |
| Sample Designation Date Time Coment, Preservation abSamfple ID-foiS-oqo1 -Ac4 IYYd WG G 4L, iL Li ______
| |
| 'o-IW15) 2 t44 Io WG G 4L, IL1 ~o.
| |
| ___ __ WG G 4L,1IL, _ _ _ _ _ _ _
| |
| ___ WG G 4L; IL .. t
| |
| _ __- WG G - 4Lt4L_ _ _ _ _ _
| |
| NO0TES: P0O#: 00'2337 . MSR #:04-1807 I LTP QA FLIRadwaste QA 0 Non QA Samples Shipped Via: ntera Cha,'tier Fed Ex Tep.. De ,
| |
| Requested analyses should be performed to typical groundwater program MDC's. El Hand .,-,.Custody.Sealeid?~'"-~
| |
| 1)RelinquishS~yfD /ie 2 eeve ~DtfieL Cutdy elIna
| |
| : 3) Relinquished By Datefrime, 4) Received By! b't~efime __________YO' NO0 4 4Bill of Lading#
| |
| : 5) Relinquished By DatefTime 6) Received By Date/Time 4,
| |
| | |
| Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00120 362 Injun Hollow Road, East Hanpton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 86-6-53Media ceia Sample ymc Container Contnr:-..:
| |
| RihM~ahCode Type Size-Analytical Lab (Name, City, State): Code &Type General Engineering Lab (GEL), 2040 Savage Rd, Code Charleston, SC 29407, 843.556.8171 (Sarah Kozlik)
| |
| Priority: El45 D. z 30 D. El 14 D. E 7 D.
| |
| Other:
| |
| Sample Designation Date Time Comment, Preservation Lab Sample ID M 10io3- 1-'cRct I -%-e; , I WG G 4L, IL ;/A,03 o__ _ -______
| |
| 4 ^ o2- , 6--3o-c i WG G 4L, IL _ _ _
| |
| WG G 4L,1L __
| |
| WG G 4L, IL WG G 4L,1L = =
| |
| NOTES: PO#: 002337 MSR el 04-1807 El LTP QA E Radwaste QA Non QA Samples Shipped Via:
| |
| Fed Ex Intemnal Container Temp.: _ Deg. C Requested analyses should be performed to typical groundwater program MDC's. El Hand Custody Sealed?
| |
| _ __ _ _ _ _ __ _ __ _ __ __ _ _ _ _ _Y .O N O.
| |
| : 1) Relinquished.8y: Date/Tinie 2) Rjc ved By Datc/Time Custody Seal Intact?
| |
| 7/6 711/$I It 3- oEl Other
| |
| : 3) Relinquished By Date/Time 4) geceived By Datc/Tim e Y.O NO By ate/TiBill of Lading #
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time K. I I
| |
| | |
| . .. .. ,. (
| |
| Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00116 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested LabUseOnl y ; .;-E:- -; ;t .>
| |
| Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 Medi Code Sample Type Coner Size- 4 ........
| |
| Analytical Lab (Name, City, State): Code &Type .,
| |
| Geneal Engineering Lab (GEL), 2040 Savage Rd, Code Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) % . . .........
| |
| Priority: n 45 D. 0 30 D. Li 14 D. 0 7 D. . . . ...
| |
| Other: . . n ....
| |
| Sample Designation Date Time Comment, Preservation bLaSample ID
| |
| . /co S-C00'1.ooI W /iO 0 WG G 4L, IL X--_ IL._._ m t qL ' P.;03 o3;1.,,.
| |
| ; M@-Liitl 12ib/ot e-, WG G 4L, IL _ _ IL..0 - Lo. "N. 3 OS S-W SSp WI/o /5D' 4,1 L Nof4t: % HA0 IGG ; 4>'al;t't-t-
| |
| ._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ WG G 4L,1L . ._ _L _. _ _ _ _TT _- _
| |
| .__ __ __ _ _W G G 4L,1LL . ._ __;_________
| |
| Sapls Shpe L lftsih Cz tfi;; hi NOTES: PO#: 002337 MSR#: 04-1807 i LTP QA L Radwaste QA 1 Non QA SamplesShippedVia: Container.
| |
| Fed Ex T Tn-p-.--....D D ,;
| |
| Requested analyses should be performed to typical groundwater program MDC's. 0 Hand Custody Sealed?;
| |
| : 1) Relinquish.d By: Date/Time 2) ived By 1 ate/Time Custdy seal Infact?
| |
| 3///t l/ta / 0 - lbl bi {8 El Ot er -, .lLl.
| |
| : 3) Relinquished By Date/Time 4 edAy' Date/Time NO N_______Y Bill of Lading #
| |
| : 5) Relinquished By . Date/Time 6) Received By Date/Time L,f z
| |
| | |
| COOLER RECEI PT CHECKLIST 15
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/Time Received: 1lf lC)J SDGtl: O' 0' Ii lg9 1 Work Order Number: .1 1t e 5 Shipping'Container ID: il Chain of Custody #i. ac. 4-' .s . I I.. Custody Seals on shipping container intact? Yes [go [ ]
| |
| : 2. Custody Seals dated and signed?. Yes [ []
| |
| : 3. Chain-of-Custody record present?' Yes [+No I ]
| |
| : 4. Cooler temperature
| |
| : 5. Vermiculite/packing materials is: Wet [ ] Dry [ ]
| |
| .6.- Number of samples in shipping container:
| |
| : 7. Sample holding times exceeded? Yes [ ] No
| |
| : 8. Samples have:
| |
| -ehazard labels A n dy seals _ ppropriate sample labels
| |
| : 9. Samples are:
| |
| 4/ good condition leaking broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [ No
| |
| : 11. Description o5fnomalies (include sample numbers):
| |
| ^ 116St1 ;-()b
| |
| .tA IN\ , C (jXL/
| |
| Sample Custodian/Laboratory.
| |
| Telephoned to: On By 16 '
| |
| | |
| Connecticut Yankee Statement of Work for Analytical
| |
| - Lab Services CY-ISC-SOW-0O 1 Figure 1. Sample Check-in List Date/Time Received: '\ 6q1 SDG#: AO1 Work Order Number:
| |
| Shipping Container ID: q9 1 q d 76 Chain of Custody # , oo..I -6b1lJ
| |
| : 1. Custody Seals on shipping container intact? Yes [I' IL]
| |
| : 2. Custody Seals dated and signed? Yes [w° [ I
| |
| : 3. Chain-of-Custody record present? Yes fTlNo [ ]
| |
| : 4. Cooler temperature R T
| |
| : 5. Vermniculite/packing materials is: jJ 'T ' Wet [ ] Dry [ ]
| |
| : 6. Number of samples in shipping container:
| |
| : 7. Sample holding times exceeded? Yes [ ] No [Q4
| |
| : 8. Samples have:
| |
| -tape _ hazard labels lCustody seals ___appropriate sample labels
| |
| : 9. Samples are:
| |
| -iiigood condition leaking broken _ have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes[] No
| |
| : 11. Description of anomalies (include sample numbers): iLye ((eu' &L
| |
| , w-l- 16-ao I--cof L (A4 L at-}al SV - jjo' 5/ -~061 X1Fa)
| |
| Sample Custodian/Laboratory:- Date:
| |
| Telephoned to:_ On By 17
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-OOI Figurel. Sample Check-in List Date/rime Received:
| |
| .DI
| |
| / a /o/
| |
| SDG#: - - L(W-t 16)-'
| |
| m Work Order Number:
| |
| Shipping Container ID.: { gi
| |
| &Ar 9/4;- Chain of Custody# c- c6/t- Oo//q
| |
| : 1. Custody Seals on shipping container intact? Yes [LJNac []
| |
| : 2. Custody Seals dated and signed? Yes Ko [1
| |
| : 3. Chain-of-Custody record present? Yes LA-No
| |
| : 4. -Cooler temperature - °C)
| |
| : 5. Vermiculite/packing materials is: J A Lt Wet ( ] Dry t3
| |
| : 6. Number of samples in shipping container (°
| |
| : 7. Sample holding times exceeded? Yes [ ] No ;
| |
| : 8. Samples have:
| |
| _. p se ____hazard labels Ticstdy seals appropriate sample labels
| |
| : 9. Samples are:
| |
| god condition leaking broken have air bubbles I0. Were any anomalies identified in sample receipt? Yes [ No (
| |
| I 1. Description of anomalies (include sample numbers): MW 101 D t Be x IL
| |
| *d/. Wk /S/
| |
| I )pey 44
| |
| . . .. . . I . . (6 Sample Custodian/Laboratory._ - ~ ~ ~~Date:
| |
| Telephoned to:_ -__. -_ _:---_On - By.
| |
| 18 '
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-O0 I Figure 1. Sample Check-in List Date/Time Received: 1 lL l) It/
| |
| SDG#: -O' 19)0\
| |
| Work Order Number:
| |
| Shipping Container ID:i) C9 Jla A(6 -hainof Custody #
| |
| : 1. Custody Seals on shipping container intact? Yes [DL'I]
| |
| : 2. Custody Seals dated and signed? Yes [j o[ ]
| |
| : 3. Chain-of-Custody record present? Yes U-o--
| |
| : 4. Cooler temperature
| |
| : 5. Vermiculite/packing materials is: & A Wet [ ] Dry [ I
| |
| : 6. Number of samples in shipping container:
| |
| : 7. Sample holding times exceeded? Yes [ ] No t
| |
| : 8. Samples have:
| |
| hazard labels
| |
| _ustody seals _ - ie sample labels
| |
| : 9. Samples are:
| |
| __ _ 'd condition leaking l_ broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [] No I3-
| |
| : 11. Description of anomalies (include sample numbers):
| |
| Vq 1 1 3 S -c.bu6W1- nc> ( I Al L- (,)t ) Y, 1 Pe{SDA.- kIvt il)1 Sample Custodian/Laboratory:. Date:
| |
| Telephoned to: On By_
| |
| j 19
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-00 1 Figure 1. Sample Check-in List Date/Time Received: I I- l zL SDG#: mA1tO\ l Work Order Number: ' t 1 b tS C o s #
| |
| Shipping Container ID: )C ' 74qJ il( Chain of Custody # 0ha0 I1Ob1{
| |
| : 1. Custody Seals on shipping container intact? Yes H-rNo [1]
| |
| : 2. Custody Seals dated and signed? Yes [J-No [I
| |
| : 3. Chain-of-Custody record present? Yes h-.No [I
| |
| : 4. Cooler temperature C
| |
| : 5. Vermiculite/packing materials is: T,14<Wet[1] Dry []
| |
| : 6. Number of samples in shipping container: %(1
| |
| : 7. Sample holding times exceeded? Yes [ ] No [Ho<
| |
| : 8. Samples have:
| |
| _____ _____hazard labels custody seals appropriate sample labels
| |
| : 9. Samples are:
| |
| _ in good condition leaking broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes { I No
| |
| : 11. Description of anomalies (include sample numbers): A' I(*LYK i b) Ali, 2mw-3-b~LM qa)dg (al As 6 Sample Custodian/Laboratory.: Date:
| |
| Telephoned to: -On -- By 20 '
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-00 1 Figure 1. Sample Check-in List Date/Time Received: <k) y SDG#: % §___A L4- I Work Order Number:
| |
| Shipping Container ID: dfJ q9 L/ 9/ f Chain of Custody # a ,oL]- 'z6 1I3
| |
| : 1. Custody Seals on shipping container intact? Yes L.-No [ ]
| |
| : 2. Custody Seals dated and signed? Yes L.-rfo [ ]
| |
| : 3. Chain-of-Custody record present? Yes +-V'o[1
| |
| : 4. Cooler temperature
| |
| : 5. Vermiculite/packing materials is: et [ ] Dry [
| |
| : 6. Number of samples in shipping container: to
| |
| : 7. Sample holding times exceeded? Yes [ No
| |
| : 8. Samples have:
| |
| :tape hazard labels M y seals _ appropriate sample labels
| |
| : 9. Samples ar in good condition leaking
| |
| _ broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [ ] No v
| |
| : 11. Description of anomalies (include sample numbers):
| |
| OA W 0 q 5Size 4z~-1 ep X)s/t (5JiA Sample Custodian/Laboratory: _ Date: _
| |
| Telephoned to: On By 21
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-00 1 Figure 1. Sample Check-in List Date/Time Received: /
| |
| SDG#: Sn~ OA on Work Order Number:_
| |
| Shipping Container ID.: )
| |
| D gI -- 9A/4ichain of Custody # _)co-I-coto 7
| |
| : 1. Custody Seals on shipping container intact? Y <No [I
| |
| : 2. Custody Seals dated and signed? Yes - [ ]
| |
| : 3. Chain-of-Custody record present? Yes LJNo [ ]
| |
| : 4. Cooler temperature ~ I
| |
| : 5. Vermiculite/packing materials is: N o Zk [-], Dry [ ]
| |
| : 6. Number of samples in shipping container-IN Y
| |
| : 7. Sample holding times exceeded? Yes [ )No PWe
| |
| : 8. Samples have:
| |
| tape hazard labels
| |
| ___ custodyseals -eppi-priate sample labels
| |
| : 9. Samples are:
| |
| _5igod condition Leaking broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes I] No lLJL. 2
| |
| : 11. Description of anomalies (include sample'numbers):
| |
| AW -OA7601 N (L 3 );
| |
| . I ..
| |
| Sample Custodian/Laboratory:. . . . . . .
| |
| Date:
| |
| Telephoned to: -
| |
| .P4I B_
| |
| y.
| |
| 22 -
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-00 1 Figure 1. Sample Check-in List Date/Time Received:i ,/&
| |
| SDG#: C%3 RA°O °A-Mm Work Order Number:
| |
| Shipping Container ID: (1 /Id A/gJ 9 3Jr/Chain of Custody #_ ,)L~oo-/ - 66 /I?
| |
| I. Custody Seals on shipping container intact? Yes *o [I
| |
| : 2. Custody Seals dated and signed? Yes [L4-lqo [ I
| |
| : 3. Chain-of-Custody record present? Yes H-lo [ ]
| |
| : 4. Cooler temperature _ 1
| |
| : 5. Verniculite/packing materials is: Wet [ I Dry [ ]
| |
| : 6. Number of samples in shipping container:
| |
| : 7. Sample holding times exceeded? Yes [ I No [-
| |
| : 8. Samples have:
| |
| ________e hazard labels lstody seals appropriate sample labels
| |
| : 9. Samples are:
| |
| _____in good condition leaking l_ broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [ ] No
| |
| : 11. Description of anomalies (include sample numbers): Ve grave '
| |
| 1< WIba - Acts - a/1 [ 3)/ tJx
| |
| { - = .
| |
| Sample Custodian/Laboratory:- Date:
| |
| Telephoned to:_ On By 4
| |
| 23 '
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/Time Received: -
| |
| SDG#: .C!, 9_W C q p Work Order Number:.
| |
| Shipping Container ID.I: . °t 2d af\2hain of Custody# C
| |
| : l. Custody Seals'on shipping container intact? Yes [go[ ]
| |
| : 2. Custody'Seals dated and signed? Yes [3lo [1
| |
| : 3. Chain-of-Custody record present? Yes 1 J.No [ ]
| |
| 4.. Cooler temperature - - 9
| |
| : 5. Vermiculite/packing materials is: Wet 1 Dry []
| |
| : 6. Number of samples in shipping container
| |
| : 7. Sample holding times'exceeded? YeIs ]No[q"
| |
| : 8. Samples have:
| |
| fp ___hazard labels
| |
| - jcustody seals prrpriate sample labels
| |
| : 9. Samples are:
| |
| in good condition . _leaking
| |
| .broken ___have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? - Yes I] No I1. . Description of anomalies (include sample numbers):
| |
| Sample Custodian/Laboratory: - - Date:_
| |
| Telephoned to: On - By 24
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-lsc-soW-00 I Figure 1. Sample Check-in List n I J1 Date/Time Received:
| |
| -I _
| |
| l l il J A,
| |
| )/
| |
| SDGII: n5WLV?<)
| |
| Work Order Number:
| |
| Shipping Container ID: ' qL23OChain of Custody . ""Xn O1~Oo jI 1
| |
| : 1. Custody Seals on shipping container intact? Yes [ o [I
| |
| : 2. Custody Seals dated and signed? Yes [LJ4o [ I
| |
| : 3. Chain-of-Custody record present? Yes [E.go [ I
| |
| : 4. Cooler temperature _
| |
| : 5. Venniculite/packing materials is: Wet [ ] Dry [ ]
| |
| : 6. Number of samples in shipping container:
| |
| : 7. Sample holding times exceeded? Yes ] Ne-t<
| |
| : 8. Samples have:
| |
| tlape hazard labels stotody seals r pra priate sample labels
| |
| : 9. Samples are:
| |
| 'ain good condition leaking broken ____have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [] No
| |
| : 11. Description of anomalies (include sample numbers):
| |
| MwS 0rs - /L (I46 AOL!offL) ,V, 0 o fw 1005- otl o f(( fly1 (Ijy4L 1 Sample Custodian/Laboratory_ Date:
| |
| Telephoned to: On nly-J 25
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| | |
| /y 3,))
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| JIV (
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| INORGANIC ANALYSIS 26;
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| | |
| -- a-Metals Fractional Narrative Connecticut Yankee Atomic Power Co. (YANK)
| |
| SDG MISR#04.1807 Method/Analysis bnrornialion Analytical Batch: 346377, 346379 Prep Batch: 346376, 346378 Standard Operating Procedures: GL-MA-E-014 REV# 9, GL-MA-E-006 REV# 9 Analytical Metho(l: SW846 6020 Prep Method: SW846 3005A Sample Analysis Sample ID Client ID 116165001 MW I IOS 116165002 MW 122D 116165003 MW 109D-0204-001 116165004 MW- 107S-0204-001 116165005 MWI 07D-0204-00 I 116165006 MWI IOD-0204-001 116165007 MWI 13S-0204-001 116165008 MW 112S-0204-001 116165009 MWI02S-0204-001 116165010 MW-I I IS-0204-001 116165011 MW-109S-0204-001 116165012 MW-3-0204-00 I 116165013 MWI-0204-001 116165014 MW-I 05D-0204-001 116165015 MWI 03D-0204-001 116165016 MWI05S-0204-001 116165017 MW600-02W4-001I 27
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| | |
| 116165018 MW508D-0204-001 116165019 MW-IOOS-0204-001 116165020 MW-504-0204-001 116165021 MW-508S-0204-001 1200656526 Method Blank (MB) in batch 346377 1200656531 Method Blank (MB) in batch 346379 1200656527 Laboratory Control Sample (LCS) in batch 346377 1200656532 Laboratory Control Sample (LCS) in batch 346379 1200656530 116165001(MW I 10SL) Serial Dilution (SD) in batch 346377 1200656535 116165021(MW-508S-0204-001L) Serial Dilution (SD) in batch 346379 1200656528 116165001(MW I 10SD) Sample Duplicate (DUP) in batch 346377 1200656533 116165021(MW-508S-0204-OOID) Sample Duplicate (DUP) in batch 346379 1200656529 116165001(MW 1OSS) Matrix Spike (MS) in batch 346377 1200656534 116165021(MW-508S-0204-OIS) Matrix Spike (MS) in batch 346379 Preparation/Analytical Method Verification The SOP stated above has been prepared based on technical research and testing conducted by General Engineering Laboratories, LLC. and with guidance from the regulatory documents listed in this "Method/Analysis Information' section.
| |
| System Conriguration The ICP-MS analysis was performed on a Perkin Elmer Elan 6100E inductively coupled plasma mass spectrometer (ICP-MS). The instrument is equipped with a cross-flow nebulizer, quadrupole mass spectrometer, and dual mode electron multiplier detector. Internal standards of scandium, germanium, indium, and tantalum were utilized to cover the mass spectrum. Operating conditions are set at 1400W power and combined argon pressures of 360+/-7 kPa for the plasma and auxiliary gases, and 0.85 1mrin carrier gas flow, and an initial lens voltage of 5.2.
| |
| The ICP-MS analysis was performed on a Perkin Elmer ICP-MS ELAN 9000. The instrument is equipped with a cross-flow nebulizer, quadrupole mass spectrometer, and dual mode electron multiplier detector. Internal standards of scandium, germanium, indium, and tantalum were utilized to cover the mass spectrum. Operating conditions are set at 1400W power and combined argon pressures of 360+/-7.kPa for the plasma and auxiliary gases, and 0.85 I~min carrier gas flow, and an initial lens voltage of 5.2.
| |
| Calibration Information --
| |
| Instrument Calibration All initial calibration requirements have been met for this sample delivery group (SDG).
| |
| CRDL Requirements All CRDL standard(s) met the referenced advisory control limits.
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| 28:
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| | |
| ICSAIICSAB statement All interference check samples (ICSA and ICSAB) associated with this SDG met the established acceptance criteria.
| |
| Continuing Calibration Blank (CCB) Requirements All continuing calibration blanks (CCB) bracketing this batch met the established acceptance criteria.
| |
| Continuing Calibration Verification (CCV) Requirements All continuing calibration verifications (CCV) bracketing this SDG met the acceptance criteria.
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| Oualitv Control (QC) Information Method Blank (NIMB) Statement The MBs analyzed with this SDG met the acceptance criteria.
| |
| Laboratory Control Sample (LCS) Recovery The LCS spike recoveries met the acceptance limits.
| |
| Quality Control (QC) Sample Statement Samples 116165001 (MW I lOS) and 116165021 (MWV-50SS-0204-001) were selected as the quality control (QC) samples for this SDG.
| |
| Matrix Spikc (MS) Recovery Statement The percent recoveries (%R) obtained from the MS analyses are evaluated when the sample concentration is less than four times (4X) the spike concentration added. All applicable elements met the acceptance criteria.
| |
| Duplicate Relative Percent Difference (RPD) Statement The RPD obtained from the designated sample duplicate (DUP) is evaluated based on acceptance criteria of 20%
| |
| when the sample is 5X the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control of +/-RL is used to evaluate the DUP results. All applicable analytes met these requirements.
| |
| Serial Dilution % Difference Statement The serial dilution is used to assess matrix suppression or enhancement. Raw element concentrations that are 25X the IDL for CVAA, SOX the IDL for ICP, and IOOX the IDL for ICP-MS analyses are applicable for serial dilution assessment. All applicable analytes met the acceptance criteria of less than 10% difference (%D).
| |
| Technical Information Holding Time Specifications GEL assigns holding times based on the associated methodology, which assigns the date and time from sample collection of sample receipt. Those holding times expressed in hours are calculated in the AlphaLIMS system. Those holding times expressed as days expire at midnight on the day of expiration. All samples in this SDG met the specified holding time.
| |
| Preparation/Analytical Method Verification All procedures were performed as stated in the SOP.
| |
| Sample Dilutions Dilutions are performed to minimize matrix interferences resulting from elevated mineral element concentrations present in soil samples and/or to bring over range target analyte concentrations into the linear calibration range of the instrument. The samples in this SDG did not require dilutions.
| |
| Preparation Information The samples in this SDG wvere prepared exactly according to the cited SOP.
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| 29
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| | |
| Miscellaneous Information Nonconformance Documentation Nonconformance reports (NCRs) are generated to document procedural anomalies that may deviate from referenced SOP or contractual documents. A NCR was not required for this SDG.
| |
| Additional Comments Additional comments were not required for this SDG.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| -The following data validator verified the information presented in this case narrative:
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| Reviewefz2 - Date: 7/3-o 30
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com U
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 3D,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 1 of I Client Sample ID: MW 110S Proiect: YANK00304 Sample ID: 116165001 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 10:07 Receive Date: 02-JUL-04 i
| |
| - Collector: Client Parameter Qualificr Result - DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-NIS 3005/6020 Boron-A LJSTND. IX Boron 291 0.540 16.0 ug/L I PRB 07/26/04 1910 346377 I The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW8463005A ICP-MS 3005 PREP C0 07/16/04 1844 346376 The rollowing Analytical Methods were perfornmcci Method Description Analyst Comments IK)
| |
| I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiL Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| l1eviewed by 6 31
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, GENERALENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - vvww.gel.com Certificate of Anilysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| -East Hampton, Connecticut 06424 Report Date: July 30,2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PON 002337 Page I of I Client Sample ID: MW 122D Proiect: YANK00304' Sample ID: 116165002 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 16:51 Receive Date: 02-JUL-04 Collector: Client Paramiter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MIS 3005/6020 Boronz-AULSTND,AIIX Boron 223 0540 16.0 ug/L I PRB 07r26/04 1926 346377 1 The following Prep Methods were performed Method Description Analyst Date Time *PrepBatch SV846 3005A ICP-MS 3005 PREP C) 07/16/04 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 1i Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul. Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 32
| |
| | |
| GENEALEGINERIN LABRATRIES LL GENERAL ENGINEERING, LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keeler Project Quarterly Groundwater PON 002337 Page 1 of I Client Sample ID: MW 109D-0204-001 Proiect- YANK00304 Sample ID: 116165003 Client ID: YANK001 Matrix: Ground Water Collect Date: 29-JUN-04 09:55 Receive Date: 02-JUL-04 Collector irent Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MlS 3005/6020 Boron-AL4STNDIfX Boron 191 0.540 16.0 ugtL I PRB 07/26/04 1928 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 300516020 KJ Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiL UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by NJ 33
| |
| | |
| GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com
| |
| - Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| - East Hampton, Connecticut 06424 Report Date: July 30,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 - Page 1 of I Client SampleID:.` '-Ml V-107S-0204-0O1 Proiect: YANKO0304 Sample ID: ' - l'II( 6165004 Client ID: YANK001 Matrix: Or(rund Water Collect Date: 29-JUN-04 13:10 Rerive- Daite:- A T1 If AA -- ;'
| |
| Collector Client Parameter 'Qualifier' Result DL RL Units DF Analys'tDate Tune Batch Method Metals Analysis-ICP-MS 3005/6020Boron-AUSTND,h4IX Boron 177 0.540 16.0 ug/L I PRB 07/26/4 1931 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP C] 07116/04 1844 346376 MTe following Analytical Methods were performed Method Description Analyst Comments SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limitn but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiLt Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded. -
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.'
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project ManagerSarah Kozlik'.
| |
| Reviewed by 34
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 558-8171 - www.gel.com
| |
| )J Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I or I Client Sample ID: MW 107D-0204-001 Proiectz YANK00304 Sample ID: 116165005 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 10:30 Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result DL RIL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-M%1S 3005/6020 Boron-AL4.STND, MX Boron 32.1 0.540 16.0 ug/L I PRB 07f26104 1934 346377 1 The following Prep Methods were perronned Mlethod Description Analyst Date Time Prep Batch SW8463005A ICP-MS 3005 PREP Ci 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 \K)
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiL Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by I
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| 35
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| ' East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater POd 002337 Page I of I Client Sample ID: MWI IOD-0204-001 Proiect: YANK00304 Sample ID: 116165006 Client ID: YANK001 Matrix: Ground Water Collect Date: 30-JUN-04 13:12 Receive Date: 02-JUL-04 Collector Client Parameter - . Qualifier Result DL RL Units DF AnalystDate Time Batch Mlethod Metals Analysis-ICP-MS 3005/6020 Boron-ALlTNDllIX Boron 236 0540 16.0 ug/L I PRB 07126104 1936 346377 1 The following Prep Mrethiods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. -The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. - -;
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories,'LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik."' '
| |
| Reviewed by 36:
| |
| | |
| , GENERAL ENGINEERING LABORATORIES, LLC
| |
| - 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quartcrly Groundwater PO# 002337 Page 1 of I Client Sample ID: MWI 13S-0204-001 Proiect: YANK00304 Sample ID: 116165007 Client ID: YANKOOI Matrix: Ground Water Collect Date: 29-JUN-04 10:30 Receive Date: 02-JUL-04 Collector Clipnt Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-NIS 3005/6020 Boron-ALLSTNDM1X Boron 110 0.540 16.0 ug/L I PRB 07/26/04 1939 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16/04 1844 346376 The rolloiwing Analytical Methods were performed Method Description Analyst Comments I SWV846 300516020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 37.
| |
| | |
| ENGINEERING LABORATORIES, LLC GENERAL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date. July 30.2004,
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PON 002337 Page I of I Client Sample ID: MWI12S-43204-001 Proiect: YANK00304 Sample ID: 116165002 Client ID: YANKOOI Matrix: Ground W ater Collect Date: 29-JUN-04 4 12:35 Receive Date: 02-JUL-0I rnmlecno
| |
| _v^Swuv .
| |
| fI;n-LllenL Parameter Qualifier Result DL RL Units DF AualystDate Tlmc Batch Method Metals Analysis-ICP-MS 3005/6020 Boron4ALLSTNDAfX Boron 47.8 0540 16.0 ugIL I PRB 07/26/04 1942 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments SW846 3005/6020 Notes:
| |
| The Qualifiers in'this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limiL U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identi fication for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 38
| |
| | |
| . GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater P0# 002337 Page 1 of I Client Sample ID: MW102S-0204-001 Proiect: YANK00304 Sample ID: 116165009 Client ID: YANKOO0 Matrix: Ground Water Collect Date: 28-JUN-04 15:20 Receive Date: 02-JUL-04 Collector client Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-AIS 3005/6020Boron-ALUSTNDWMIX Boron 91.2 0.540 16.0 ug/L I PRB 07/26/04 1944 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 Tie following Analytical Methods were performed Method Description Analyst Comments I SW946 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specitic qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has mnet all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| R-iewea by 39
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| ' Ceftiiiicate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun tHollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 1 of I Client Sample ID: MW-Il1S-0204-001 , Proiect: YANKO03O4 Sample ID: 116165010 Client ID: YANKOl Matrix: Ground Water Collect Date: 29-JUN-04 16:10 Receive Date: 02-JUL-04
| |
| ;LUleaorU Client Parameter Qualifier Result DL iRL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-NIS 3005/6020 Borovn-AL4STNDA1iIX Boron 55.5 0.540 16.0 ug/L I PRB 07126/04 1947 346377 1 The following Prep Methods were performed Method Description -Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J. Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection lirmit;-
| |
| Ul Uncertain identification for gamma spectroscopy. C :
| |
| X Lab-specific qualifier-please see case narrative, data summaary package or contact your project inanager for'details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engifieering Laboratories, LLC standard operating procedures. Please direct any questionrs to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 40
| |
| | |
| ---------- 11L-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-817i - www.gel.corr J
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I Of I Client Sample ID: MW- 109S-0204-001 Proiect: YANK00304 Sample ID: 116165011 Client ID: YANKOOI Matrix: Ground Water Collect Date: 28-JUN-04 15:25 Receive Date: 02-JUL-04 Collector. riePnt Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-NIS 3005/6020 Boron-A"l4STNDUIX Boron 124 0.540 16.0 ugIL I PRB 07/26/04 1955 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP C. 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 300516020
| |
| '' )
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| U1. Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewedby 41
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: liaddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 - Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater POP 002337 Page 1 of I Client Sample ID: MW-3-0204-001 Proiect: YANKoO3O4 Sample ID: 116165012 Client ID: YANKOOI Matrix: Ground Water Collect Date: 29-JUN-04 16:52 Receive Date: 02-JUL-04 Collector ri;pnt Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-NIS 300516020 Boron-ALLSTNDIIX Boron J 5.67 0540 16.0 ug/L I PRB 07126104 1957 346377 1 Thie following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments 1 SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD KFlag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 11 Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limitbut less than the reporting limit. -
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Samplepreparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by v 42
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 55-8171 - www.gel.com I
| |
| Certificate of Analysis Company: CYAPCo Address: Hladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MWI-0204-001 Proiect: YANK00304 Sample ID: 116165013 Client ID: YANKOOI Matrix: Ground Water Collect Date: 28-JUN-04 14:58 Receive Date: 02-JUL-04 Collector Cient Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MS 3005/6020 Boron-ALlSTNDMIX Boron J 5.08 0.540 16.0 ug/L I PRIB 07/26/04 2000 346377 1 mTe following Prep Mlethods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| * Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ut Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data sununary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 43
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Ceftificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MW-105D-0204-001 Project: YANK00304 Sample ID: 116165014 Client ID: YANKOOI Matrix: Ground Water Collect Date: 29-JUN-04 11:05 Rece-ive*'v~Date:
| |
| '- '~
| |
| t"
| |
| 'J ITTI U L-%"
| |
| f Collector Client
| |
| 'Parameter'- - Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MIS 3005/6020 Boron-ALlSTND.AIX Boron 60.8 0.540 16.0 ug/L I PRB 07/26/04 2003 346377 1 The following Prep Methods were performed Method Description - Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performcd Method Description Analyst Comments 1 SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value:-The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NEL'AP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance'with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 44
| |
| | |
| ILO GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MWI03D-0204-001 Proiect: YANK00304 Sample ID: 116165015 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 09:15 Receive Date: 02-JUL-04 Collector rlient Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MIS 3005/6020 Boron-ALtSTND.flX Boron 57.1 0.540 16.0 ug/L I PRB 07/26/04 2005 346377 1 The following Prep Mcthods were performed Method Description Analyst Date Time Prep Batch SW8463005A ICP-MS3005PREP CJ 07116/04 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments
| |
| ' )
| |
| I SW846 300516020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limiL U Indicates the target analyte was analyzed for but not detected above the detection limiL UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 45
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, I- ~. , .. 1. 4 -. I l ,
| |
| .GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate ofAnalysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| :East Hampton. Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 - Page I of Client Sample ID: MWI05S-0204-001 Proiect: YANK00304 Sample ID: 116165016 Client ID: YANKOOI Matrix: Ground Water Collect Date: 29-JUN-04 14:40 Receive Date: 02-JUL-04 Collector ('Ip-t Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MS 3005/6020 Boron-AL4STND, MtIX Boron 484 60540 16.0 ug/L I PRB 07126104 2008 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16/04 1844 346376 TLe following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a nag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded. ,
| |
| J Indicates an estimated value. The result 'was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project Manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis. ,.4 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 46 '-
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.oom Certificate of Analysis Company: CYAPCo Address:* Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MW600-0204-001 Proiect YANK00304 Sample ID-. 116165017 Client ID: YANK001 Matrix Ground Water Collect Date: 29-JUN-04 14:40 Receive Date: 02-JUL-04 lien' Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-hiS 3005/6020 Boron-A LLSTND.fLK Boron 518 0.540 16.0 ug/L I PRB 07/26/04 2011 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07116/04 1844 346376 The following Analytical Methods wrere performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| It Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was'analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 47
| |
| | |
| GE A GENERAL-ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| : East Hampton, Connecticut 06424
| |
| * Report Date: July 30,2004 Contact Mr. Dave Keefer . .1P Project: -Quarterly Groundwater PON 002337 Page I of I Client Sample ID: MW508D-0204-001 . Proiect - *YANK00304 Sample ID: 116165018 Client ID: YANK001 Matrix: Ground Water Collect Date: 30-JUN-04 15:45 Receive Date: 02-JUL-04 0nile-t-Paramter er - Pesul Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MS 3005/6020 Boron-A USTND,MJ1X Boron ' 66.1 0.540 16.0 ug/L I PRB 07/26104 2013 346377 1 The following Prep Methods were performed Method Description , Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BE Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| U' Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an was received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 48
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com I
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MW-I OOS-0204-001 Proiect: YANK00304 Sample ID: 116165019 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 10:00 Receive Date: 02-JUL-04 Collector Oin-t An,,
| |
| Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-]CP-MIS 3005/6020 Boron-A USND.M1X Boron 25.3 0.540 16.0 ug/L I PRB 07126/04 2016 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16104 1844 346376 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| II Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| U1 Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by
| |
| -I 49
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, GENERAL 'ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East tlampton, Connecticut 06424 Report Date: July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 1 of I Client Sample ID: MW-504-0204-001 Proiect: YANK00304 Sample ID: - 116165020 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 12:45 Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-1CP-MS 3005/6020 Boron-ALLSTNDA1iX Boron 42.7 0.540 16.0 ugIL I PRB 07/26/04 2019 346377 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16W04 1844 346376 The following Analytical Methods were performed Method Description Analyst Conunents SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ut Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager fordetails.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewedby 50
| |
| * GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| )J Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date. July 30,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MNV-508S-0204-001 Proiect: YANK00304 Sample ID: 116165021 Client ID: YANKOOI Matrix: Ground Water Collect Date: 30-JUN-04 15:50 Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MS 3005/6020 Boron-AL4SINDMfX Boron 41.9 0.540 160 ugfL I BAJ 07122/04 0932 346379 1 The following Prep Methods were performed AMethod Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP FGA 07115104 1000 346378 Tie following Anailytical Methods were performed Mlethod Description Analyst Comments I SW846 300516020 Notes:
| |
| The Qualificrs in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| 11 Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| RVewed by 51
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - wwvv.gel.com QC Summary Rewort Date: July 30,2004 Client: CYAPCo Page I of 2 Haddam Neck Plant 362 Injun llooow Road East llampton, Connecticut
| |
| | |
| ==Contact:==
| |
| - Mr. Dave Keefer.
| |
| Workorder: 116165 Parmname NOM' Sample Qual QC Units RPD% REC% Range Anist Date arme
| |
| . .I..
| |
| Metals Analysis - ICPI7S Batch 346377 QC1200656528 116165001 DUP Boron 291 301 ugsL 3 (0%-20%) PRB 07n26/04 19:13 QC1200656527 LCS Boron 100 114 ugL- 114 (80%-120%) 07126/04 19:0S QC1200656526 MB Boron J 2.51 ug/L 07/26/04 19:05 QC1200656529 116165001 MS Boron 100 291 404 ug/L 113 (75%-125%) 07126/04 19:15 QC1200656530 116165001 SDILT Boron 291 18.9 ugtL 675 07126/04 19:18 Batch 346379 QC1200656533 116165021 DUP Boron 41.9 41.8 ug/L 0 A (+1-16.0) BAJ 0722/04 09:34 QCI20056532 LCS.
| |
| Boron 100 108 ug/L 108 (80%-120%) 07n22/04 09:29 QCt200S631 MB Boron U ND ugtL 0722104 09:26 QC1200656534 116165021 MS Boron 100 41.9 153 uglL 111 (75%-125%) 07/2204 09:37 QC1200656535 116165021 SDILT Boron 41.9 J 8.34 uglL .356 0722/04 09:39 Notes:
| |
| TIhe Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| 52:
| |
| | |
| . GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston, SC 29407- (843) 556-8171 - www.gel.com OC Summary Workorder: 116165 Page 2of 2 Parmname NONM Sample Qual QC Units RPD% RECKS Range Anist Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.
| |
| A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/-
| |
| the RL is used to evaluate the DUP result.
| |
| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
| |
| 53
| |
| | |
| .1 t .iI i RADIOLOGICAL A .;;S ...S.
| |
| ANALYS IS 54 -
| |
| | |
| Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)
| |
| SDG NISR#04-1807 Method/lAnalysis Information Product: Am241,Cm, Liquid-ALL Analytical Method: DOE EML HASL-300, Am-05-RC Modified Analytical Batch Number 350485 Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MWIO3D-0204-001 116165016 MWIO5S-0204-001 116165017 MW600-0204-001 1200666549 Method Blank (MB) 1200666552 Laboratory Control Sample (LCS) 1200666550 116165014(MW-105D-0204-001) Sample Duplicate (DUP) 1200666551 116165014(MW-105D-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Enginecring Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-0 II REV# 13.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165014 (MW-105D-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| 55
| |
| | |
| I Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Manual Integration No manual integrations were performed on data in this batch.
| |
| Ounalifier information Manual qualifiers were not required.
| |
| Method/Analvsis Information Product: Alphaspec Pu, Liquid-ALL Analytical Method: DOE EML HASL-300, Pu-Il RC Modified Analytical Batch Number 350489 Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MWI03D-0204-001 116165016 MW105S-0204-001 116165017 MW600-0204-001 1200666553 Method Blank (MB) 1200666556 Laboratory Control Sample (LCS) 1200666554 116165014(MW-105D-0204-001) Sample Duplicate (DUP) 1200666555 116165014(MW-105D-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 13.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information: '
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165014 (MW-105D-0204-001).
| |
| 56:
| |
| | |
| -AL-QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prepfRe-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. The following NCR was generated for this SDG:
| |
| NCR 129765 was generated due to Failure to maintain Custody. 1. The analyst did not scan the samples into the batch prior to analysis, however the samples did remain in their custody at all times. The error has been corrected and the analyst has been instructed on proper scanning procedures. 1. Reporting results.
| |
| Manual Integration No manual integrations were performed on data in this batch.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Liquid Scint Pu241, Liquid-ALL Analytical Method: DOE EML HASL-300, Pu-I I-RC Modified Analytical Batch Number 350490 Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MWI03D-0204-001 116165016 MWV105S-0204-001 116165017 MW600-0204-001 1200666557 Method Blank (MB) 1200666560 Laboratoiy Control Sample (LCS) 1200666558 116165014(MW-105D-0204-001) Sample Duplicate (DUP) 1200666559 116165014(MW-105D-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 5.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| 57
| |
| | |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165014 (MW-1 05D-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentatione',
| |
| Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. The following NCR was generated for this SDG:
| |
| NCR 131016 was generated due to Failure to maintain Custody. 1. Samples 116165014,116165015,116165016 and 116165017were not scanned into thebatch dueproblems with theAlpha Lims system. 1. Reporting results.
| |
| Manual Integration No manual integrations were performed on data in this batch.
| |
| Qualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Gammaspec, GammaLiquid-ALL,GA12,STNDMIXPENN,LF Analytical Method: EPA 901.1 Analytical Batch Number 346800 Sample ID Client ID -
| |
| 116165001 MW IIHS 116165002 MW 122D 116165003 MW 109D-0204-001 116165004 MW-107S-0204-001 116165005 MW107D-0204-001 58-
| |
| | |
| 116165006 MWI1OD-0204-001 116165007 MWI 13S-0204-001 116165008 MW1 12S-0204-001 116165009 MWI02S-0204-001 116165010 MW-IIIS-0204-001 116165011 MW-109S-0204-001 116165012 MW-3-0204-001 116165013 MWI-0204-001 116165014 MW-105D-0204-001 116165015 MWI03D-0204-001 116165016 MW105S-0204-001 116165017 MW600-0204-001 116165018 MW508D-0204-001 116165019 MW-100S-0204-001 116165020 MW-504-0204-001 1200657517 Method Blank (MB) 1200657520 Laboratory Control Sample (LCS) 1200657518 116165001(MW 11S) Sample Duplicate (DUP) 1200657519 116165001(MW IIOS) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample wasused forQC: 116165001 (MW IlOS).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis 59
| |
| | |
| Sample 1200657519 (MW IIOS) was recounted due to low/high recovery.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| qualifier information Qualifier Reason Analyte Sample UlData rejected due to low abundance. Cesium-137 116165003 116165008 116165009 e Cobalt-60 116165003 UI ata rejected due to no valid peak. Manganese 116165009 II_ I_ 116165010 Method/Analysis Information Product: Gammaspec, GammaLiquid-ALL,GA12,STND,MIIX,PENN,LF Analytical Method: EPA 901.1 Analytical Batch Number: 346820 Sample ID Client ID 116165021 MW-508S-0204-001 1200657581 Method Blank (MB) 1200657584 Laboratory Control Sample (LCS) 1200657582 116165021 (MW-508S-0204-001) Sample Duplicate (DUP) 1200657583 116165021(MW-508S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165021 (MW-508S-0204-001).
| |
| 60
| |
| | |
| QC Information -)
| |
| All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep[Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Gross A/B, liquid-ALLSTND,1IXPENN,LF Analytical Method: EPA 900.0 Analytical Batch Number 350139 Sample ID Client ID 116165001 MW I WS 116165002 MW 122D 116165003 MW 109D-0204-001 116165004 MWV-107S-0204-001 116165005 MW107D-0204-001 116165006 MWIIOD-0204-001 116165007 MWI13S-0204-001 116165008 MWI 12S-0204-001 116165009 MW102S-0204-001 116165010 MW-I I IS-0204-001 1200665742 Method Blank (MB) 1200665746 Laboratory Control Sample (LCS) 1200665743 116852001(C-0000000355) Sample Duplicate (DUP) 1200665744 116852001(C-0000000355) Matrix Spike (MS) 1200665745 116852001(C-0000000355) Matrix Spike Duplicate (MSD)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-00 I REV# 8.
| |
| Calibration Information:
| |
| Calibration Information 61
| |
| | |
| All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ounaliti Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116852001 (C-0000000355).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due 'to moisture -
| |
| absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alphalbeta efficiencies arc assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/AnalVsis Information Product: Gross A/B, liquid-ALLSTNDTIXPENN,LF Analytical Method: EPA 900.0 Analytical Batch Number: 350566 62
| |
| | |
| Sample ID Client ID 116165011 MW-109S-0204-001 116165012 MW-3-0204-001 116165013 MWI-0204-001 116165014 MNV-105D-0204-001 116165015 MWI03D-0204-001 116165016 MWl05S-0204-001 116165017 MW600-0204-001 116165018 MW508D-0204-001 116165019 MW-100S-0204-001 116165020 MW-504-0204-001 116165021 MW-508S-0204-001 1200666709 Method Blank (MB) 1200666713 Laboratory Control Sample (LCS) 1200666710 11616501 1(MW-109S-0204-001) Sample Duplicate (DUP) 1200666711 11616501 1(MW-109S-0204-001) Matrix Spike (MS) 1200666712 11616501 1(MW-109S-0204-001) Matrix Spike Duplicate (MSD)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-00I REV# 8.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s). )
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165011 (MWV-109S-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis Sample 1200666710 (MW-109S-0204-001) was recounted due to high relative percent'difference/relative error ratio.
| |
| 63
| |
| | |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration'date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.'
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165001 (MW IIOS).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments Samples 116165002 (MW 122D), 116165004 (MW-107S-0204-001), 116165016 (MWIO5S-0204-001) and 116165017 (MW600-0204-001) were verified by recounting at least five days from the separation date.
| |
| Qualifier information Manual qualifiers were not required. .
| |
| Method/Analysis Information Product: Liquid Scint Tc99, Liquid-ALL Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 348813 65
| |
| | |
| Sample 1200666711 (MW-109S-0204-001) was recounted due to low/high recovery.
| |
| Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| qualifier information Manual qualifiers were not required.
| |
| M\ethod/Analysis Information Product: GFPC, Sr90, liquid-ALLMIX Analytical Method: EPA 905.0 Modified Analytical Batch Number. 347780 Sample ID Client ID 116165001 MW IOWS 116165002 MW 122D 116165003 MW 109D-0204-001 116165004 MW-107S-0204-001 116165005 MWI07D-0204-001 116165006 MWIIOD-0204-001 116165007 MWI 13S-0204-001 116165008 MWI 12S-0204-001 116165009 MWI02S-0204-001 116165010 MW-11IS-0204-001 116165011 MW-109S-0204-001 116165012 MNV-3-0204-001 116165013 MWI-0204-001 116165014 MW-105D-0204-001 116165015 MWI03D-0204-001 116165016 MWI05S-0204-001 116165017 MW600-0204-001 1200659983 Method Blank (MB) 1200659986 Laboratory Control Sample (LCS) 1200659984 116165001(MW I IOS) Sample Duplicate (DUP) 1200659985 116165001(MW I IOS) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in:
| |
| accordance with GL-RAD-A-004 REV# 8.
| |
| 64
| |
| | |
| Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MW103D-0204-001 116165016 MW1O5S-0204-001 116165017 MW600-0204-001 1200662485- Method Blank (MB) 1200662488 Laboratory Control Sample (LCS) 1200662486 116165014(MW-105D-0204-001) Sample Duplicate (DUP) 1200662487 116165014(MW-105D-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 11.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165014 (MW-105D-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information: -
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referernced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| 66,;
| |
| | |
| ---------- a-Oualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: Liquid Scint Fe55, Liquid-ALL Analytical Method: DOE RESL Fe-I, Modified Analytical Batch Number. 349214 Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MWl03D-0204-001 116165016 MIW105S-0204-001 116165017 MW600-0204-001 1200663486 Method Blank (MB) 1200663489 Laboratory Control Sample (LCS) 1200663487 116165014(MW-105D-0204-001) Sample Duplicate (DUP) 1200663488 116165014(NIW-105D-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 2.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration datc(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (0C) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165014 (MW-105D-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis 67
| |
| | |
| Sample 1200663488 (MW-105D-0204-001) was recounted due to low/high recovery.
| |
| Samples 116165014 (MW-105D-0204-001) and 116165015 (MWI03D-0204-001) were recounted due to verify activity. Second counts are being reported.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Ouslifier information Manual qualifiers were not required.
| |
| Mlethod/Analysis Information Product: - Liquid Scint Ni63, Liquid-ALL Analytical Method: DOE RESL Ni-I, Modified Analytical Batch Number: 349216 Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MW103D-0204-001 116165016 MW105S-0204-001 116165017 MW600-0204-001 1200663494 Method Blank (MB) 1200663497 Laboratory Control Sample (LCS) 1200663495 116165014(MW-105D-0204-001) Sample Duplicate (DUP) 1200663496 116165014(MW-105D-0204-001) Matrix Spike-(MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 6. - ;
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry -
| |
| All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information . . '
| |
| The blank volume is representative of the sample volume in this batch.
| |
| Designated QC ;
| |
| The following sample was used forQC: 116165014 (MWV-105D-0204-001).
| |
| QC Information 68
| |
| | |
| All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| qualifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: LSC, Tritium Dist, Liquid-ALL,STNDMIX,PENN Analytical Method: EPA 906.0 Modified Analytical Batch Number 348827 Sample ID Client ID 116165001 MW 10S 116165002 MW 122D, 116165003 MW 109D-0204-001 116165004 MW-107S-0204-001 116165005 MWI07D-0204-001 116165006 MWI IOD-0204-001 116165007 MW1 13S-0204-001 116165008 MW I12S-0204-001 116165009 MW102S-0204-001 116165010 MW-IIIS-0204-001 116165011 MW-109S-0204-001 116165012 MW-3-0204-001 116165013 MWI-0204-001 116165014 MW-105D-0204-001 116165015 MW103D-0204-001 116165016 MWIO5S-0204-001 116165017 MW600-0204-001 116165018 MW508D-0204-001 116165019 MW-IOOS-0204-001 116165020 MIW-504-0204-001 116165021 MW-508S-0204-001 1200662538 Method Blank (MB) 1200662541 Laboratory Control Sample (LCS) 1200662539 116165001(MW I IOS) Sample Duplicate (DUP) 1200662540 116165001(MW I IOS) Matrix Spike (MS) 69
| |
| | |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 9.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information',
| |
| Standard solution(s) for these analyses are NIST traceable and used before the expirationi date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116165001 (MW 1 OS).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis Samples 116165004 (MWV-107S-0204-001) and 1200662538 (MB) were recounted due to spectral interference.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Qualifier Information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: -Liquid Scint C14, Liquid-ALL Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 347077 70',
| |
| | |
| Sample ID Client ID 116165014 MW-105D-0204-001 116165015 MW103D-0204-001 116165016 MW105S-0204-001 116165017 MW600-0204-001 1200658272 Method Blank (MB) 1200658275 Laboratory Control Sample (LCS) 1200658273 115840001 (SW-6) Sample Duplicate (DUP) 1200658274 115840001(SW-6) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparaiion, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 7.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 115840001 (SWV-6).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments There was no daily check run on 7/10/04 for LSCBROWN. The daily for the instrument passed on both 7/9 and 71
| |
| | |
| 7/11. All qc's pass requirements.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| The following data validator verified the information presented in this case narrative:
| |
| Reviewer:
| |
| 72 -
| |
| | |
| General Engineering Laboratories NCR Report No.: 129765 Form GEL-XXX Revision No.:
| |
| Rev. 06/02 COMPANY - WIDE NONCONFORMANCE REPORT Mo.Day Yr. Division: Type:
| |
| 26-JUL-04 Radiochemistry Process InstrumentType: Quality Criteria: Client Code:
| |
| ALPHA SPECTROMETER Specifications YANK Test / Method: Matrix Type: Batch ID: Sample Numbers:
| |
| DOE EML HASL-300, Pu-i 1-RC Liquid 350489 See Below
| |
| -Modifed Potentially affected work order(sXtSDG): 116165(MSR#04-1807)
| |
| Application Issues:
| |
| Failure to maintain Custody Specification and Requirements NRG Disposition:
| |
| Nonconformance
| |
| | |
| == Description:==
| |
| : 1. The analyst did not scan the samples into the batch prior to analysis, 1. Reporting results.
| |
| however the samples did remain in their custody at all times. The error has been corrected and the analyst has been instructed on proper scanning procedures.
| |
| ' )
| |
| Originators Name: Data Validator/Group Leader:
| |
| Lesley Anderson 26-JUL-04 Scott Moreland 27-JUL-04 Quality Review: Corrective Action:
| |
| Director Corrective Action ID and Complete Date:
| |
| Page 1 73
| |
| | |
| General Engineering Laboratories NCR Report No.: 131016 Form GEL-XXX Revision No.:
| |
| Rev. 06/02 COMPANY - WIDE NONCONFORMANCE REPORT Mo.Day Yr. Division: Type:
| |
| 30-JUL-04 Radiochemistry Process Instrument Type: Ouallty Criteria: Client Code:
| |
| LSC Specifications YANK Test / Method: Matrix Type: Batch ID: Sample Numbers:
| |
| DOE EML HASL-300, Pu-11 -RC Uquid 350490 See Below Modified Potentially affected work order(s)(SDG):ll 6 l5 (MSRt807)
| |
| Application issues:
| |
| Failure to maintain Custody Specification and Requirements NRG Disposition:
| |
| Nonconformance
| |
| | |
| == Description:==
| |
| | |
| 1.Samples 116165014,116165015,116165016and 116165017were 1. Reporting results.
| |
| not scanned Into the the batch due problems with the Alpha Ums system.
| |
| I.
| |
| Originator's Name: Data Validator/Group Leader:
| |
| Jimmy Hartley 30-JUL-04 Joseph Jones 30-JUL-04 Quality Review: Corrective Action:
| |
| Director: Corrective Action ID and Complete Date:
| |
| Page 1 74K
| |
| | |
| SAMPLE DATA
| |
| | |
| ==SUMMARY==
| |
| | |
| 75
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis' Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton.'Connecticut 06424 Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW 110S Project: YANK00304 Sample ID: 116165001 Client ID: YANKOOI Matrix: - Ground Water Vol. Recv.:
| |
| Collect Date: 30-JUN-04 '
| |
| Receive Date: 02-JUL-04 Collector. Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamma LJquid-AILGAM2,STNDM1XPFNJN,LF Americium-241 U 0.753 +1-2.45 2.05 ,.+/-2.40 4.22 IpCi/L- ,SRB 07/19/04 2220 346800 1 Cesium-134 U -0.753 +/-1.87 1.50 +1-1.83 3.21 pa/L ,
| |
| Cesiunu-137 U IA5 +1-1.86 1.44 +/-1.82 3.05 poall,~
| |
| Cobalt-60 U 0.194 41-1.86 1.58 '+-1.82 3.42 pCi/L Europium-152 U 0.288 +1-3.89 3.23 +1-3.81 6.77 pCi/L
| |
| 'Iuropium-154 U 2.66 +1-4.74 ' 4.22 *+14.64 9.18 pCi/L;
| |
| , Zuropium-155 U -1.15 +/-420 3.32 -+/4.11 6.86 .PCi/L Manganese-54 U 0.368 +/-1.70 1.44 +/-1.67 3.06 pci&L Niobium-94 U 0.0195 +/-1.70 126 +/-1.67 2.68 pCi/L Silver-108m U -1.55 +1-1.40 1.04 +/-1.37 2.20 pCi/ll-Rad Gas Flow Proportional Counting GFPC,Sr9O, liquid-ALWMX I . .,! : . -
| |
| Strontium-90 U 0.689 +/-0.637 0.612 ,+/-0.661 130 pCi1L HOB I 07/13/04 1652 347780 2 Gross A/B, liquid-AUSTNDM1XPENNLF Alpha U -0.0535 +1-0.988 1.04 +1-0.988 2.44 pCi/L ATHI 07f22/04 1803 350139 3 Beta 4.35 +/-1.33 0.951 +1-1.33 2.05 pCi/L Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-AL4STND.MlXPENNf Tritium 1010 +/-220 155 +/-220 310 pCi/L JLB1I 07119/04 1611 348827 4 The following Prep Methods were perfonned Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16/04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified 76
| |
| | |
| GENERAL ENGINEERING LABORATORiES; LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 55-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: liaddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW 1lOS Proiect YANK00304 Sample ID: 116165001 Client ID: YANKOOI Vol. Remv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Tlime Batch Mtd.
| |
| SurrogateiTracer recovery Test Recovery% Acceptable LImIts Canier/Tracer Recovery GFPC, SO9O, liquid-All.MIX 90 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limiL U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 77
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gelcom Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ReportDate: July3l,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Kcefer
| |
| ..Project: Quarterly Groundwater PO# 002337 - - Page 1 of 2 Client Sample ID: MW 122D - - Proiect: YANK00304 '
| |
| Sample ID: 116165002 -'I Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date 30-JUN-04 Receive Date: 02-JUL-04 Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GammLiquid-ALLGAMZ,STND,MIPENN,LF Americium-241 U 1.31 +1-14.4 8.64 +/-14.1 18.1 pCi/L SRB 07/20104 1110 346800 1, Cesium-134 U 1A7 +1-2.03 1.81 +/-1.99 .- 3.94 pCi/L Cesium-137 U -0.756 +1-1.8S 1.50 +1-1.84 3.28 pol'l Cobalt-60 U -1.17 +l-2.07 1.57 +l-2.03 3.56 pCi/L Europium-152 U 3.7S, +l-5.33 4.62 +/-5.22 9.81 IpC/L'L' Europium-154 U 3.59 +/-5.51 4.99 - +1-5AO 11.1 .pCilL k :uropium-155 U -0.326 +l-7.49 6.09 +1-7.34 12.7 Pal'l K--Manganese-54 U 0.356 4+/-1.85 1.56 +1-1.82 3.41 pci/L Niobium-94 U -0.283 +/-1.84 1.51 +/-1.81 3.27 pCi'L Silver-108m U 2.23 +/-1.80 1.62 +/-1.76 3A5 Rad Gas Flow Proportional Counting GFPC.Sr90, liquid-ALLMIfX Strontium-90 3.29 +/-0.768 0.541 +/-1.13 1.15 .pCill, HOBI 07/13/04 1652 3477802 GrossA, liquid-ALSTNDM1XPENNLF Alpha 7.14 +/-2.19 0.997 +1-2.25 2.37 _ _ pCi/L ATH I 07J22/04 1803 350139 3 Beta 5.21 +/-1.58 1.19 +/-1.58 2.55 pCi/L Rad Uquid Scintillation Analysis LSC, Tritium Dist, Llquid-ALSTND.M1X.PENN Tiitium U 222 +/-165 132 +/-165 264 pCi/L JLBBI 07/19/04 1715 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed Method Dcscription I 3EPA 901.1 2 EPA 905.0 Modifled 3 EPA 900.0 4 EPA 906.0 Modified Surrogatetrracer recovery Test Recovery% Acceptable Limits 78
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - vww.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31.2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PON 002337 I Page 2 of 2 Client Sample ID: MW 122D Proiect YANK003O4 Sample ID: 116165002 Client ID: YANKO01 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Carrieriracer Recovery GFPC, SW9O, liquid-ALLMIX 89 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 79
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 '; Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| -Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 1 of 2 Client Sample ID: MW 109D-0204-001 Prpiect: YANK00304 Sample ID: 116165003 Client 1D: YANKOO1 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04 Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamma.LJquid-AUIGAM2,STNDMIXPENNF Americium-241 U -1.6 +1-11.4 9.24 +1-11.2 19.1 pCV/L SRB 07/20/04 1008 346800 1 Cesium-134 U 0.364 +1-2.82 2.40 +1-2.76 5.26 pCiIL Cesium-137 U 0.00 +t-4.47 4.19 +4-4.38 8.77 pCV/L UI w2 7 . .
| |
| Cobalt-60 U 0.00 +1-3.44' 2.71 +/-3.37 6.01 pCi/L Ul
| |
| \,-Europium-152 U -5.94 +l-7.28 5.66 +1-7.14 12.0 pCi/L.
| |
| Europium-154 U 2.24 +l-7.20 6.17 +/-7.05 13.9 pCVL Europium-155 U 537 +/-933 7.70 +4-9.14 16.0 Manganese-54 U -1.28 +/-2.36 1.84 +1-2.31 4.09 pCi/L Niobium-94 U -0.431 +/-2.42 1.89 +1-2.37 4.13 PaiL Silver-108m U -0.462 +1-2.52 2.03 +1-2.47 4.35 - pCi/L Rad Gas Flow Proportional Counting GFPC,Sr9O, liquid-AL4MIX Strontium-90 U 0.473 +t-0.555 0.545 +10.567 1.16 pCiLL HOBI 07/13/04 1652 3477802 GrossxA/B lquid-ALL.STND.MIlXPENN.LF Alpha 7.78 +/-2.23 0.819 +/-2.25 2.03 pCi/L ATHI 07122J04 1803 350139 3 Beta 9.21 +1-1.70 0.912 +/-1.70 1.98 pCV/L Rad Liquid Sdntlllation Analysis ISC, Tritium Dist, Liquid-ALLSTNDMIX PENN Tritium 3140 +/-246 129 +/-251 258 pCiJL JLB1 07/19/04 1818 3488274 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP C0 07/16104 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified 80
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| 'Uv Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton. Connecticut 06424
| |
| * Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW 109D-0204-001 Project: YANK003O4 Sample ID: 116165003 Client ID YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| SurrogatelTracer recovery Test Recovery% Acceptable Limits CarrierfTracer Recovery GFPC, Sr90, liquid-AllflX 92 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| dCQ& Ca Reviewed by 81
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC
| |
| .GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate fAnalysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW-107S-0204-001 -' Proiect: YANK00304 Sample ID: 116165004 Client ID: YANKOO1 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04, Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammospec, Gamma Liquid-ALL GAM2.STND.MIXPENNLF Americium-241 U 332 +/-10.6 8.88 +/-10.4 18.5 PMV SRB 07/20/04 1009.346800 1 Cesium-134 U 0.453 +/-2.09 1.71 +/-2.05 3.73 pCIIL Cesium-137 U 1.07 +1-1.82 1.57 +/-1.79 3.39 pCVLl Cobalt-60 U -0.142 +/-222 1.80 +1-2.17 4.00 pCi/L.
| |
| Europium-152 U 2.21 +J-5.13 4.41 +/-5.02 9.35
| |
| -3.11 +1-5.47 4.09 +/-5.36 9.26 pCV1L 3uropium-154 U pCVL
| |
| \.%sFuropium-155 U 2.74 +t-7A6 6.17 +1-731 12.8
| |
| -0333 IpCVL-Manganese-54 U +1-157 1.29 +/-1.54 2.86 Niobium-94 U -0.559 +/-1.66 1.29 +/-1.63 2.80 pC/LL Silver-108m U 0395 +/-1.73 1A6 +/-1.70 3.12 pCiIL Rad Gas Flow Proportional Counting GFPC Sr90, liquid-ALLMIX Strontium-90 2.69 +/-0.741 0.558 +/-0.992 1.19 pCilL HiOBI 07/13104 1652 34i7802 GrossA/B, liquid-ALLSTND,MlX,PENINLF Alpha
| |
| * U 0.317 +/-1.17 1.13 +/-1.17 2.66 pCitL
| |
| * ATHI 07122J04 i803 350139 3 Beta U 1.69 +/-1.08 0.940 +/-1.08 2.04 pCi/L Rad Liquid Scintillation Analysis LSC, Tritium Dist, Liquid-ALLS7DM4IXPENN Tritium U -133 +/-205 176 +/-205 352 pCi/L JLBI 07/28/04 2341 3488274 The following Prezp Methods were performed Method Description Analyst Date Time Prep Batch SW8463005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 ModIfied
| |
| -rrogatefTracer recovery Test Recovery% Acceptable Limits 82-
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| "-)
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-107S-0204-001 Proiect: YANK00304 Sample ID: 116165004 Client ID: YANK001 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Carrierfrracer Recovery GFPC. SO9O, liquid-ALLMIX 92 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiL UI Uncertain identification forgamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| 1U h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Beet~ ( Q Reviewed by 83
| |
| | |
| GEEA NIERN AOAOIS L IGENERAiL ENGINEERING LABORATORIES., LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| ; East Hampton, Connecticut 06424 Report Date: July 31.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer ag .o.I .
| |
| Project Quarterly Groundwater PO# 002337 . I IPage I of 2 Client Sample ID: MWI07D-0204-001 Project: YANK00304 Sample ID: - 1116165005 .. Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 30-JUN-04 -
| |
| * Receive Date: 02-JUL-04 t w.AJLscLuL; LUlCIU.. P. I
| |
| ...el tLt D .A yt t m.. M.
| |
| Parameter Qtualifler Result Uncertalnty LC -TPV MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamma.quid-ALL GAM2S7WND.MIXJPENNLF Americium-241 U 2.12 +/-3.64 3.17 +1-3.57 6.59 pCmI SRB 07/20/04 1009 346800 1 Cesium-134 U -1.75 +t-2.30 1.73 +l-2.26 '3.80 pCslL Cesium-137 U -1A2 +1-2.13 1.66 +l-2.08 3.61 pCV/L Cobalt-60 U 0.452 +1-2.18 1.86 +/-2.14 4.16 pCi/L Europium-152 U -0.225 +1-5.32 4.40 '+/.5.21 934 pC/LL uropium-154 U 1.05 +l-6.58 5.56 4/-6.45 12.3 pCi/L K uropium-1 5 5 U 6.45 +/-5.97 5.18 +1-5.85 10.7 .pCi/L Manganese-54 U 0.487 *+l-2.24 1.65 +t-2.19 - 3.61 pCiLL Niobium-94 U 0.734 +/-1.88 1.62 +/-1.84 3.50 pCi/L Silver-108m U -0.297 +/-1.95 1.57 +1-1.91 3.35 .pCi/L Rad Gas Flow Proportional Counting GFPC,Sr9O, liquid-ALLMfX Strontium-90 U 0.262 +1-0555 0.565 +1-0.558 120 pCi/L BOB I 07/13/04'2041 347786 2 Gross A/B, iquiSdALI4.ND DAfJXPENN,LF Alpha U 0.548 +/-1.27 1.10 +/-1.28 2.53 -pCL' ATHI 07/22/04,1803 350139 3 Beta 7.00 +/-1.58 1.02 +1-1.59 2.20 Rad Liquid ScInUllation Analysis pCi/L LSC, Tritium Dist, Jquid-AL TSNDAEX(PENN Tritium 656 +/-172 125 +l-i72 249 3LB1I 07119/04 2025 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 The following Analytical Methods were performed IMethod Description.
| |
| I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified Rurrogate'Tracer recovery Test Recovcry% Acceptable Limits 84
| |
| | |
| GENEALLABRATRIES EGINERIN LL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Iladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW107D-0204-001 Proiect: YANK00304 Sample ID: 116165005 Client ID: YANKOOI VnI Thev -
| |
| *Parameter I Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time BatchMtd.
| |
| CarrierlTracer Recovery GFPC, Sr9O. liquid-ALL.MIX 95 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limiL U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by SQCu um 85
| |
| | |
| GENEAL EGINERIN GENERAL'ENGINEERING LABORATORIES, LLC
| |
| ' 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ReportDate: -July31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: :'Quarterly Groundwater PO# 002337 ; Page I of 2 Client Sample ID: -- - MWIIOD-0204-00l Proiect: YANK003O4 Samnple ID: -. ~ 116165006 Client ID: YANK001 :
| |
| Matrix: Ground Water Vol. Recv.:
| |
| - Collect Date: JUN-04
| |
| - I : Receive Date: 02-JUL-04 ..
| |
| : r. . .
| |
| I %.., . - I1. . . I . -
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GammaLiquid-ALL.GAM2,STND MIXPENNLF .. I ..
| |
| Americium-241 U 1.46 +/-7.34 5.80 +1-7.19 12.0 . pCd/L - ,: SRB 07/1-9/04 2153 346800 1 Cesium-134 U 0.265 +t-l.42 1.17 +/-1.39.-* 2.51 1.94 pCtiL Cesium-137 U -0.836 +/-1.17 0.898 41-1.15 Cobalt-60 U 0.0068 +I-IA9 1.23 +/-1.46 2.69 . I Europium-152 U *0.828 +/-3.79 3.07 +1-3.72 6.44
| |
| 'uropium-154 U 2.09 +1-3.74 I 3.29 - +/-3.67 7.19 pCilL ropium-155 U -2.17 +/4.77 3.97 +/4.67 8.20 .pCi/L Manganese-54 U 1.18 +/-1.27 1.11 .-- +/-1.24 238 Niobium-94 U 0.664 +/-1.25 1.06 +1-1.22 2.25 Silver-108m U -1A7 +/-1.11 0.845 +/-1.09 1.80 Rad Gas Flow Proportional Counting . PCiJL GFPC Sr90, liquid-ALLMIX pCi/L -
| |
| Strontium-90 U 0.441 +/-0.547 0538 41.559 1.15 HOB1 07/13104 2041 3477802 Gross A/, liquid-ALUsTNDAfIXPENNLF pCi/L Alpha 5.63 +/-1.94 0.988 +1-2.02 233 ATHI 07/22/04 2016 350139 3 Beta 8.50 +1-1.65 ) 0.952 +J-1.65 2.06 Rad Liquid Sdntillation Analysis LSC, Tritium Dist, Liquid-ALlSTNDAMIXPENN Tritium 8300 +/-363 139 +/-386 278 pCa/L JLB1 07/19/04 2128 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 -EPA 905.0 Modified 3 .. EPA 900.0 4 EPA 906.0 Modificd Suirrogatefrracer recovery Test Recovery% Acceptable Lriits 86-
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddarn Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MWI IOD-0204-001 Proiect: YANK00304 Sample ID: 116165006 Client ID: YANKOOI
| |
| ! Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| CarrierJTracer Recovery GFPC, Sr90, liquid-ALLMIX 87 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limnit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| I) h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| -kQ Reviewed by Chx 87
| |
| * GENERAL ENGINEERING LABORATORIES, LLC IGENERAL ENGINEERING:L;ABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| / .East Hampton, Connecticut 06424 *ReportDate: July3l.2004 Contact Mr. Dave Keefer Project: . Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: -** MWI13S-0204-001 Proiect: YANK003O4 Sample ID: . - 116165007 Client ID: YANKOOI Matnx: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04 Receive Date: -.. ,02-JUL-04 Collector: - - Client RMI . . M Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammarpec, GamnaLiquid-AL4GAM2 STNDMIXPENNLF Americium-241 U -0.0669 +/-755 5.84 +1-7A40 12.2 'pCi/L SRB 07/19/04 2156 346800 1 Cesium-134 U 0.548 +1-1.36 1.17 +1-1.34 2.52 pCi/L -
| |
| Cesium-137 U -0.106 +1-1.27 1.05 , +/-1.25 226 pCiIL Cobalt-60 U 2.58 +/-2.80 2.16 +1-2.75 4.55 pCi/'L I I . - .- - 1.
| |
| Europium-152 U .333 +4-3.70 3.14. +1-3.62
| |
| * 6.60 pCi/L
| |
| 'Puropium-154 U -133 +1-3.85
| |
| * 2.92 +1-3.78 6.49 . pCiIL aropium-155 U -0.381 +14.84 4.07 +1-4.74 8.41 .pCiIL 8-Alanganese-54 U -0.167. +/-1.33 1.08 +1-1.30 2.32 pCi/L .
| |
| Niobium-94 U 0.713 - +1-1.24 1.07 +/-1.21 2.28 pCiIL'.
| |
| Silver-108m U 1.57 +I-IA2 0.990 +I-IA0 2.10 pCi/L Rad Gas Flow Proportional Counting . I . ... 7 . ..
| |
| GFPC, Sr90. liquid-ALLVfJX .-
| |
| Strontium-90 U 0.665 +1-0.602 - 0.577 +1-0.627 1.23 pCi/L IIOBI 07/13/04 2041 3477802 GrossA/B, liquid-ALITND,MIXPENNLF Alpha U '0.989 +1-1.26 1.00 +/-1.26 2.38 pCi/L ATHI 07/22/04 2016 350139 3 Beta 830 +/-1.79 1.19 +/-1.79 2.54 pCi/L Rad Ltquid Scintillation Analysis LSC, Ttium Dit, Liquid-AL4STNDMIXPENN Tritium U 180 +1-163 131 +/-163 263 pCi/L JLBI 07/19/04 2231 348827 4 The followlng Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed Method . Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified Surrogatel/racer recovery Test Recovery% Acceptable Limits 88'
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sarnple ID: MWI13S-0204-001 Proiect YANK00304 Sample ID: 116165007 Client ID: YANKOOI VoL Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Carrier/rracer Recovery GFPC, Sr9O, liquid-ALLMIX 84 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection lirnit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| 'C )
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 89
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Ceftificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| 'East Hampton, Connecticut 06424 '!Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: ' Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW1 12S-0204-001 ' Proiect: YANK00304 Sample ED: 116165008 Client ID: YANKOO1 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04 Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA . Units, DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamma.Liquid-AULGAM2.STND,MIX PENNLF Americium-241 U -18.8 +/-18.2 13.0 +/-17.9 273 pCilL SRB 07i/2004 1009 346800 1 Cesium-134 U 1.16 +1-238 1.47 +1-2.33 ,3.26 pCilL Cesium-137 U 0.00 +1-2.15 2.08 +/-2.11 4A3 pCiIL Ul Cobalt-60 U -0.456 +1-1.87 1.49 +1-1.83 3.39 pCd/L
| |
| 'lropium-152 U 0.143 +1-5.48 439 +1-5.37 935 pCziL iropium-154 U '0.712 +1-4.67 3.99 .1-458 9.11 pcV/L d'-uropium-155 U -5.38 +1-6.64 5.34 +1-651 11.2 pCiL'L Manganese-54 U 1.69 +1-1.82 1.64 +1-1.78 3.57 pCiIL Niobium-94 U 0.816 +1-1.73 1.49 +1-1.69 3.22 pCi/L Silver-108m U 0.723 +1-1.70 1.49 +1-1.66 3.19 pCi/L Rad Gas Flow Proportional Counting GFPC,Sr90, liquid-ALMZIX Strontium-90 U ' 0.697 +1-0.590 0560 +/-0.616 1.19 pCiIL 110DI 07113/04 2041-3477802 GrossA'B, liquid-ALL4 STND.MEXPENNLF Alpha U 1.56 +1-1.10 0.713 +1-1.10 1.77 pCi/L ATHI 07122/42i016 350139 3 Beta . U 0.641 +1-0.944 0.908 +1-0.944, 1.97 PaiL-Rad Liquid Scintillation Analysis LSC Trtiwn Dist, Liquid-ALLSTND.MDX4PEVN Tritiurn U 102 +1-169 139 +/-169 277 pCi/L JLB 1 07/19/04 2334 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07116/04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified 90 '
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com K)
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton. Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MWI12S-0204-001 Project YANK00304 Sample ID: 116165008 Client ID YANK001 Vol. Recv.:
| |
| Parameter Quallfier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, liquid-ALLMIX 89 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded. I/
| |
| 1 Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit. k' UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by COU Reviewed by 91
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road
| |
| * East Hampton, Connecticut 06424 ReportDate: July3l,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 - Page I of 2 Client Sample ID: -: MW102S-0204-001 Proiect: YANK00304 Sample ID: - 116165009 Client ID: YANKOO1 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 28-JUN-04
| |
| - Receive Date: 02-JUL-04 rI..n#
| |
| aU ef R I . . .L Parameter Qualifier Result Uncertainty LC TPU MDA Units, DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammpec, GammaLiquid-ALLGAM2 STNDMIXPENN.LF Americium-241 U -8.79 +/-7.68 5.31 +/-7.53 10.8 pCilL SRB 07119/04 2006 346800 1 Cesium-134 U 0.721 +/-1.61 1.39 +1-1.58 2.93 . pCi/L Cesium-137 U 0.00 +/-3.02 2.46 +/-2.96 5.06 *pCi/L.
| |
| Ul Cobalt-60 U 0.869 +/-154 132 +1-1.51 2.83 pCi/L
| |
| '*ropium-152 U -1.28, +/4.20 3.43 +/-4.12 7.10 pCilL
| |
| \ ,ropium-l54 U -0.714 +1-3.95 3.16 +1-3.87 6.84 pCaL Europium-lS5 U 5.11 +t-6.89 436 +1-6.75 8.90 pCilL Manganese-54 U 0.00 +1-3.00 1.09 +/-2.94 2.32 pCilL Ul Niobium-94 U 0.829 +/-1.48 1.22 +/-1.45 2.55 pCi/L Silver-l OSm U 0.958 +I-IA6 1.23 +1-1.43 2.55 pCi/L Rad Gas Flow Proportional Counting GFPCSr9O, liquid-AL4MIX Strontium-90 U 0.289 +1-0.555 0.562 +/-0.559 1.20 pCi/L HOB I 07/13/04 2244 347780 2 GrossAB. liquid-ALlSTNDAMIPENNLF Alpha U 1.66 +/-1.31 0.980 *Ft-1.31 . 2.30 pCi/L ATHI 07/22/04 2016 350139 3 Beta U 2.05 +1-1.13 0.951 +/-1.13 2.06 pCiL Rad Liquid Scintillation AnalysIs LSC Tritium Dist,Liquid-ALLSTND.MIXPENN Tritium 5740 +/-332 150 +/-344 300 pCi/L JLBI 07/20t04 00373488274 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified 92
| |
| | |
| A-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| 'U Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contac.t: Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW102S-0204-001 Proiect: YANK00304 Sample ID: 116165009 Clent ID: YANKOQI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| SurrogatelTracer recovery Test Recovery% Acceptable Limlts Carrierfrracer Recovery GFPC, Sr9O, liquid-ALlMIX 94 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| 1 Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit. I )
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 93
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIESj-LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo .
| |
| Address: lladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 'Rcport Dite: July 31,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page l-of 2-Clienl Sample ID:' MW-IIIS-0204-001 ; .Project: YANK003O4 Sample ID: 116165010 ' Client ID: YANK001
| |
| -- - Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04 Receive Date: 02-JUL-04
| |
| .ollector. IUilent Parameter Qualifier Result Uncertainty LC TPU MDA :'Unlts'- DF 'AnalystDate Time BatchMtd.
| |
| Rad Gamma Spec Analysis Gammaspec. Gam.=4Liquid-ALI.GAM2,STNDMIXPENN,LF Americium-241 U -5.14 +/-9.11 631 +/-8.93 13.1 pCd1L SRB 07/19104 2213 346800 1 Cesium-134 U 0.418 +/-IA7 1.21 +/-1.44 2.60 pCilL ' ,
| |
| Cesium-137 U 0.663 +/-133 1.13 +/-1.30 2A0 *.pCi/L1 II Cobalt-60 U 0.0721 +1-1.44 1.18 +/-lAI 2.60. I. PCi/L -
| |
| Europium-152 U -1.01 +/-4.03 3.14 +/-3.95 6.58 pCiLL
| |
| 'uropium-154 U -1.74 +1-4.11 3.18 +t14.02 6.99 :..+-pCi/L _
| |
| \ ._,uropium-l55 U -0.20 +1-4.60 3.88 +1-4.51 8.03 ' :.pCi/L -
| |
| Manganese-54 U 0.00 +/-1.85 1.06 +/-1.81 2.29 FaVll. ,
| |
| Ul Niobium-94 U -0.669 +/-133 1.03 +1-1i30
| |
| * 2.20 pCi/L Silver-108m U 0.104 +/-1.30 1.09 +1-1.27 2.30 : pCiL Rad Gas Flow Proportional Counting
| |
| . .I . . ..
| |
| GFPC, Sr9O, liquid-AL4MIX ................
| |
| Z I ,
| |
| Strontium-90 U -0.0552 +/-0.485 0.523 +/-0.485 1.11 ' ' ' pCilL '' HOBI 07/13/04 2244 3477802**
| |
| GrossAID, liquid-AI.STNDMIXPENNLF Alpha U -0.239 +/-1.03 1.08 +t-1.03 2A9 pCVL ATH'I 07/22104 2016 350139 3 Beta U 2.06 +/-1.18 1.02 +t-1.18 2.20 pCaL Rad Liquid Scintillation Analysis LSC, Tritiwn Dist, Liquid-AL4.SNDM1XPENN Tritium U 233 +/-180 144 +/-180 288 pCi/L JLBI 07I2'0/04 0140 348827 4 The following Prep Methods were performed Method Description Analyst Date' Tume Prep Batch SW8463005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 The followlng Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified 94-
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-IIIS-0204-001 Project: YANK00304 Sample ID: .116165010 Client ID: YANKOOI Vnol Recv-!
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate T1me Batch Mtd.
| |
| Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrierfrracer Recovery GFPC, Sr9O, liquid-ALLMIX 88 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| K)
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| 9dm.. C OCA Reviewed by 95
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL, ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis :
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ReportDate: July3l,2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 -, . .Page I of-2 Client Sample ID-. *MW-109S-0204-001 Proiect: YANK00304 Sample ID: 116165011 Client ID: YANK001 '
| |
| Matrix: Ground Water Vol. Recv.:
| |
| Collect Date:. - 28-JUN-04 Receive Date: 02-JUIL-04 '
| |
| UU 1 I . . .-
| |
| Parameter QualIfier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysls Gammaspec, Gammra.Lquid-A1LGAM2,STNDMIXPENMNLF 0 Americium-241 U 2.95 +/-7.67 5.82 +/-7.51
| |
| * 12.0 pCu/L SRB - 07/19104 2011 346800 1 Cesium-134 U -0.0876 +/-1.25 1.02 ./-1.22 2.17 pCU/L Cesium-137 U 0.0362 +/-1.18 0.984 +i/-1.15 2.08 pCiIL Cobalt-60 U .- 0.337 +t-1.26 1.02 +1-1.23 2.20 pCi/L Europium-152 U -0.975 +/-3.54 .-2.88 +/-3.47
| |
| * 5.99 pCi/L'
| |
| .uropium-154 U -194 +/-3.82 2.52 +1-3.74 5.50 pCVfL
| |
| \.__,,uropium-155 U 1.01 +1-4.72 3.88 +14.63 7.95 pCV/L Manganese-54 U - -0.593 +/-1 39 0.939 +1-1.36 2.00 pCV/L Niobium-94 U -0.407 +/-1.20 0.839 +1-1.18 1.78 :pCi/L Silver-108m U 0.372 +1-1.19 0.984 +/-1.17 2.05 pci[L Rad Gas Flow Proportional Counting GFPC,Sr9O, tiquid-ALLMIX Strontium-90 U 0.801 +/-0.537 0.496 +/-0.569 1.06 pCi/L HOBI 07/13/04 2244 3477802 GrossA/B, liquid-AL4STND,MlXPENNLF Alpha U 0.441 +/-1.12 1.02 +/-1.12 232 pcifL ATHI 07/26/04 1608 350566 3
| |
| 'Beta 6.53 +/-1.16 0.619 +/-1.17 134 pCiLL Rad Llquid Scintillation Analysis LSC Triuium Dirt, Llquid-ALLSTNDMIXPENN Tritium U -9.7 +/-164 138 +t-164 275 pci/L JLB1 07/20104 0243 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16/04 1844 346376 The following Analytical Methods were performed Method . Description 1 EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 . EPA 906.0 Modified 5 Acceptable Limits RurrogateIrracer recovery Test Recovery%
| |
| 96 .
| |
| | |
| -a-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID MW-109S-0204-001 Proiect: YANK00304 Sample ID: 116165011 Client ID: YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| CarrierfTracer Recovery GFPC, Sr9O, liquid-ALLMIX 97 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for garnma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| ,1 t( u \YC Reviewed by 97
| |
| | |
| GENERAL ENGINEERING LABORATORIES, GENERAL- ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Anal ysis -
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road .. . . .
| |
| :East Hampton, Connecticut 06424 . ReportDate: July3l,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 , - . Page l'of 2 Client Sample ID: - MW-3-0204-001- Proiect YANK00304 Sanple 1D: '- 116165012 Qient ID: YANKOI Matrix: '' Ground Water Vol. Recv.:
| |
| - Co2lect Date: 29-JUN-04
| |
| - Receive Date: 02-JUL-04 Collector:,-- - Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gamnmspec. Gammna.Liquid-AUIGAMZSTND,MIXPENN,LF Americium-241 U -12A +/-17.4 935 +/-17.1 193 pCi1L.-- SRB 07/19/04 2150 346800 1 Cesium-134 U 0.0365 +1-1.69 135 +/-1.65 2.90 PCaIL Cesium-137 U -0.627 +I-IA8 1.15 +l-IA6 2.47 PCi/L Cobalt-60 U 0.383 +/-1A9 126 +1-1.46 2.78 pCiIL Europium-152 U. :-4.884 - 4/-431 1 3.54 +14.23 7A2 pCi/L 1uropium-154 U -2.25 +1-4.05: 3.08 +1-3.97 6.85 tropium-155 U -1.4 +1-634 5.05 +/-6.21 10.4
| |
| '' fanganese-S4 U 0.202 . +1-139 1.19 +1-136 2.55 pCi/L Niobium-94 U -0.436 +1-1.40 1.09 +1-137 234 Silver-108m U 0.574 +1-1.45 1.23 +/-1 .42 2.58 pCi/L Rad Gas Flow Proportional Counting GFPC,Sr90, liquid AILMlX Strontium-90 U 0.582 +1-0.599' 0.581 -+1-0.619 '1.24 'pCiYL HOB i 07/13/04 2244 347i7802.
| |
| GrossA/R. lqutid-ALSTND.M1XPENN.LF Alpha U -0.168 +/-0.763 0.792 +/-0.763 ATHI 07n2604 1608 3501566 3 Beta U 0.788 +/10.765 0.690 +1-0.765 1.49 pCi/L Rad Liquld Scintllatlon AnalysIs LSr, Tritiwn Disr. Liquid-ALl,STNDM&YPENN Tritium U 15.6 +/-147 123 +/-147, 245 pCLL JLB I 07/20/04 0424 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP ' C 07/16/04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 MOdificd Surrogatefrracer recovery Test Recovery% AcceptablemIrlts 98
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ReportDate: July3l,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-3-0204-001 cProlect:D YANK00304 Sample ID: 116165012 Client ID: YANKOO0
| |
| .Vol. Recv.:
| |
| Parameter Qualifier Result UncertaLnty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Carrier/Tracer Recovery GFPC, Sr9O, liquid-ALLMlX 84 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed forbut not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. K) h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| q-k~~Q~ uL Reviewed by 99
| |
| | |
| GENERAL ENGINEERING LABORATORIES,-LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis :
| |
| Company: CYAPCo Address: Haddam Nock Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ' Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: . Quarterly Groundwater PO# 002337 I Page I of 2 Client Sample ID: -MWI-0204-001 Proiect: YANK003O4 Samnple ID: .116165013 Client ID: YANK001 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: '. 28-JUN-04
| |
| . Receive Date: . 02-JUL-04 W-oLICLeco C~lient I ,,I -, . ,'. ..
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gzmmaipec. GammazLiquid-AULGAM2 STNDM)XPENN.LF Americium-241 U -1.81 +1-2.35 1.94 +1-2.30 i 4.00 pCL'L, SRB 07/19/04 2214 346800 1 Cesium-134 U 1.02 ./-1.47 1.28 +/ 1.44 , 2.73 -pCi/L Cesium-137 U -0.248 +1-1.39 1.13 +/-1.35 2AI Cobalt-60 U 0.750 +1-1.58 1.36 +/-1.55 2.95 pCi/L Europium-152 U 1.50 .+/-357 3.03 +/-350 - 633 pCilL
| |
| 'ropium-154 U -1.42 ./-4.10 3.26 +1.4.01 ' 7.13
| |
| .ropiuxn-155 U 3.94 +/-3.94 338 +1-3.86 6.94 IpCi/L
| |
| -M-anganese-54 U
| |
| * 1.41 . . .
| |
| .+/-1.43
| |
| - 1.26 *+/-1.40 . - 2.69 Niobium-94 U -0.174 +1-1.29 1.07 +1-1.27 226 IPCi/L Silver-I108m U 0.784 +/-1.20 1.02 +/-1.18 2.15 Rad Gas Flow Proportional Counting pCi/L GFPC,Sr9O, liquid-AL4MIX Strontium-90 U 0.944 +/-0.726 0.677 +/-0.766 1.47 HOBI 07/15/04 1245 3477802 GrossA/B, liquid-ALSUTNDUfIXPENN.LF Alpha U 0.302 +1-0.939 0.879 +1-0.939 2.00 pCi/L ATH I 07I26104 1608 350566 3 Beta U 0.234 +1.0.875 0.866 +/-0.875 1.84 pCifl.
| |
| Rad LiquId Scintillation Analysis LSC Tritium Dist, Uquid-ALLSTNDMXTPENN Tritium U 223 +/-172 137 +1-172 274 pCi/L JLBI 07f20/04 0527 348827 4 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Ci 07/16104 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified Surrogate/rracer recovery Test Recovery%. Acceptable Limits 100
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com J
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Datc: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MWI-0204-001 Proiect: YANK00304 Sample ID: 116165013 Client ID: YANK.OI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Carier/Pracer Recovery GFPC. 5r90, liquid-ALLMIX 88 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details. x-,)
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 101
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424
| |
| * ReportDate: luly31,2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I of 3 Client Sample ID: ; MW-105D-0204-001 Proiect: YANKO00304 Sample ID: 116165014 Client ID: YANKOO0 Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04 Receive Date: 02-JUL-04 Collector Client Parameter - _ Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time BatchMtd.
| |
| Rad Alpha Spec Analysis Alphaspec Pu, Lquid-ALL Plutonium-238 U -0.0134 +/-0.0691 0.0849 +1-0.0691 0.252 pCi/L BJB1 07/24/04 1532 350489 1 Plutonium-239M240 U -0.0146 +/-0.0202 0.049 +/-0.0203 0.180 pCi/.
| |
| Am241,Cmn Liquid-ALL Aneaicium-241 U 0.0272 +1-0.142 0.139 - +/-0.142 0.358 pCiL BJBI 07/24/04 :1532 350488 2 Curium-242 - U 0.00132 +/0.0717 0.0751 +/-Q0.717 0.240 pCitL Curium-243/244 U .0.064 +/-0.153 0.135 +/-0.153 0.350 juidScintPu241, Liquid-ALL p~ilL
| |
| '' .Autonium-241 - - U 0.00 . +/-653 5A8 +/-6.53 11.3 BJBI 07/28/04 1123,350490 3 Rad Gamma Spec Analysis -pCi/L Gammaspec, GammaLiquid-AULGAM2 S.NDMIXPENNLF Americium-241 U 4.62 +1-10.4 8.38 +/-10.2 17A pcifL SRB' 07 /19/04 2159 3468004 Cesium-134 U 0.895 +/-1.32 1.15 +/-1.29 2.47 p~ilL':
| |
| Cesium-137 U 0.318 +/-1.29 1.09 +/-1.27 233 pCUL Cobalt-60 U .0.017 +/-1.46 1.21 +/-1.43 2.65 pCidL Europium-152 U -0.699 +/-3.97 3.15 +/-3.90 6.62 Europium-154 U 0.0175 +/-3.44 2.85 +/-3.37 6.34 pCiLl pClL Europium-155 U -0.388 +1-5.16 4A0 +/-5.06 9.08 pCVL Manganese-54 U 0.180 +/-1.28 1.05 +/-1.26 2.27 Niobium-94 U -0.17 +/-1.29 0.911 .1-1.26 1.96 pCitL Silver-108m U -1.01 +/-1.21 0.973 +/-1.19 2.06 pcifL pilL Rad Gas F7ow Proportional Counting pCitL GFPCSr9O, liquid-ALLMIX Strontium-90 U 1.11 +/-0.656 0.575 +/4.711 1.26 OB I 07/15104 1245 3477805 Graojs A, iquid-ALS71DMNJXPF2NLF Alpha 5.30 +1-1.86 . 1.30 +/-1.94 2.84 ATHI 07/26/04 1743 350566 6 Beta 5.67 +/-1.22 0.787 +1-1.22 1.68 pCitL Rad liquid Scintllatlon Analysis LSC, Tritium Dist, Liquid-ALL STNDMIXPEWN Tritium 1280 +/-208 138 +/-209 277 -JLB1 07/2/4 0630 348827 7 Liquid Scint C14, Liquid-A LL Carbon-14 U -3.61 +1-43.9 36.9 +1-43.9 74.5 pCiL: PD 07/09/04 1215 347077 8 liquid Schnt Fe5S, Liquid-ALL Iron-55 U 6.19 +/-12.9 5.72 +-12.9 11.8 pCilL JLBI 07/29/04 0532 349214 9 Lfquid ScintM63, Liquid-ALL 102:
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Iladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 3 Client Sample ID: MW-105D-0204-001 Prmiect: YANK00304 Sample ID: 116165014 Client ID: YANK001 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Liquid Scintillation Analysis LiquldScintNWi6, Liquid-ALL Nickec-63 U -4.97 +1-7.69 6.57 +1-7.69 13.4 pCi/L JLB I 07/21/04 1141 349216 10 Liquid Scint Tc99 Liquid-ALL Technetium-99 U -4.26 -./-4.70 4.07 +1-4.70 8.36 pCi/L DAMI 07/25/04 2046 348813 11 The following Prep Methods were performed Method Description Analyst Date Tune Prep Batch SW846 3005A ICP-MS 3005 PREP C1 07/16104 1844 346376 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Pu- I1-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA901.1 5 EPA 905.0 Modified 6 EPA 900.0 7 EPA 906.0 Modified 8 EPA EERF C-01 Modified 9 DOE RESL Fe-l, Modified 10 DOERESLNi-l.Modified 11 DOE EML HASL-300, Tc-02-RC Modified SurrogateJrracer recovery Test Recovery% Acceptable Limits Plutonium-242 Alphaspec Pu, Liquid-ALL 96 (15%-125%)
| |
| Americium-243 Am241,Cm. Liquid-ALL 98 (25%-125%)
| |
| CarrierfTracer Recovery Liquid Scint Pu241, Liquid-ALL 93 Carrier/Tracer Recovery GFPC, Sr90, liquid-ALLMIX 91 CarrieriTracer Recovery Liquid Scint Fe55, Liquid-ALL 93 Carrier/Tracer Recovery Liquid Sci Ni63, Liquid-ALL 79 CarrierlTracer Recovery Liquid Scint Tc99, Liquid-ALL 99 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| 103
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES,- LLC 2040 Savage Road Charleston SO 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project
| |
| * Quarterly Groundwater PO# 002337 Page 3 of 3 Client Sample ID: - MW-105D-0204-001 Proiect: YANK00304 Sample ID: 116165014 Client ID: YANKOO0 Vnl D-Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate TILme Batch Mtd.
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| * B Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limiL U Indicates the targetanalyte was analyzed for but not detected above the detection limnit.
| |
| UIl Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data surnmmay package or contact your project manager for details.
| |
| k i Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah KozUlk.
| |
| CA) Q/O-Reviewed by
| |
| !I 104
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wuw.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 1 of 3 Client Sample ID: MW103D-0204-001 Proiect YANK003O4 Sample ID: 116165015 Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 30-JUN-04 Receive Date: 02-JUL-04 Collectori Client Parameter Qualilfier Result Uncertainty LC TPU MDA Units DF AnalystDate TIme Batch Mtd.
| |
| Rad Alpha Spec Analysis Alphaspec Pu, Liquid-ALL Plutonium-238 U -0.0644 +-0.1 17 0.160 +1-0.118 0.414 pCVL BJBI 07/24/04 1532 3504891 Plutonium-239/240 U 0.123 +1-0.139 0.0564 +/-0.140 0.208 pCi/L Am241,Cm, Liquid-ALL Americium-241 U -0.0447 +1-0.108 0.140 +/-0.108 0.369 pCiiL BJB I 07t24/04 1532 350488 2 Curium-242 U -0.0263 +1-0.0297 0.072 +/-0.0299 0.243 pCVL Curium-243/244 U -0.0619 +1-0.0839 0.130 +/-0.0843 0349 pCiL LiquidScint Pu241, Liquid-ALL Plutonium-241 U 4.81 +/-6.78 5.56 +/-6.79 11.4 pCi/L BJBI 0728/o4 1210 350490 3 Rad Gamma Spec Analysis Gammaspe4 Gamma,Liquid-ALLGAM2, STNDMIX PENNLF Americium-241 U 3.07 +1-103 8.77 +t-10.1 18.1 pCitL SRB 07/19/04 2159 346800 4 Cesium-134 U 0.601 +/-1.38 1.15 +/-1.35 2.48 pCi/L Cesium-137 U 1.44 +/-2.07 1.05 +1-2.03 2.23 pCi/L Cobalt-60 U 0.568 +/-1.43 1.22 +/-1.40 2.67 pCilL Europium-152 U 0.424 +1-3.80 3.23 +/-3.72 6.74 pCi/L Europium-154 U -0.468 +/-3.69 3.00 +/-3.62 6.59 pCi/L Europium-155 U -1.44 +/-4.98 4.07 +t-4.88 8AI pCi/L Manganese-54 U 0.0734 +/-1.33 1.07 +/-1.31 2.30 pCilL Niobium-94 U 0.546 +/-1.20 1.01 +1-1.I8 2.15 pCi/L Silver-108m U -0.589 +/-1.26 1.02 +/-1.23 2.14 pCi/L Rad Gas Flow Proportional Counting GFPC, Sr9O, liquid-ALLMiX Strontium-90 U 1.26 +1-0.720 0.628 +/-0.788 137 pCi/L HOBI 07/15104 1245 347780 5 GrossA/P, liquid-ALL STND.M XPENNLF Alpha 2.72 +1-131 0.892 +1-1.34 2.02 pCi/L ATHI 07/26/o4 1949 350566 6 Beta 336 +/-0.947 0.620 +/-0.948 134 pCi/L Rad LIquid Scintillation Analysis LSC, Tntidn Dist, Liquid ALZSTNDMLXPENN.
| |
| Tritium 6530 +/-313 127 +/-330 254 pCilL JLBI 07nl0)4 0733 348827 7 Liquid Scinr C14, Liquid-ALL Carbon-14 U -4.07 +/-43.3 36.4 +/-43.3 73.5 pCi/L PD 07/09/04 1348 347077 8 Liquid Scint Fe5S, Liquid-ALL Iron-55 U 2.08 +/-12.6 5.97 +1-12.6 123 pCiJL JLBI 07n29/04 0635 349214 9 Liquid Scint Ni63, Liquid-ALL 105
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| | |
| GEEA ENIERN AOAOIS L GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hamnpton, Connecticut 06424 Report Date: July 31,2004 Contact Mr. Dave Keefer Projec8 Quarterly Groundwater PO# 002337 . I - 'I, Page 2 of 3 Client Sarnple ID: ' -MWI03D-0204-001 I Proiect: YANK003D4 Sample ID:
| |
| * 116165015 Client ID: YANK001 - -
| |
| Vol. Recv.:
| |
| Parameter _Qualifier Result Uncertainty *LC TPU MDA Units - DF AnalystDate - 'lme Bateh Mtd.
| |
| Rad Liquid Scintillation Analysis Liquid Scint Ni63, Liquid-ALL Nickel-63 U -5.64 .1-6.72 5.77 +1-6.72 11.8 pCi/L JLBI 07121104 1212 349216 10 Liquid Scint Tc99, Liquid-ALL Tcchnctium-99 U -3.4 +/-4.70 4.04 W-4.70 831 paz/L DAJi 07t25/04 2118 348813 11
| |
| .1 . . . - .
| |
| ,1 ., . . -
| |
| The fouowing Prep Methods were perfonmed Method Description Analyst Date Time Prep Batch
| |
| -'R46 3005A ICP-MS 3005 PREP CJ . 07/16/04 1844 346376 i.ue following Analytical Methods were performed Method Description 1n lRRtflJ L A .flfl( .. RC.ndifie flfl 'V I
| |
| 2 DOE EML HASL-300 Am-05-RC 1 Modified 3 DOE EML HASL-300, Pu-5I -RC Modified
| |
| : 4. EPA 901.1 EPA 905.0 Modified 6 EPA900.0 f 7 EPA 906.0 Modified 8 EPA EERF C-01 Modified
| |
| : 9. DOE RESL Fe-I, Modified 10 DOE RESL Ni-l, Modified 11 DOE EML HASL,300, Tc-02-RC Modified SurrogatelTracer recovery Test Recovery% Acceptable Limits Plutonium-242 Alphaspec Pu, Liquid-ALL 94 (15%4125%)
| |
| Americium-243 Am241,Cm, Liquid-ALL 81 (25%-125%)
| |
| Carrier/Tracer Recovery Liquid Scint Pu241, Liquid-ALL 90 Carrier/Tracer Recovery GFPC, Sr90, liquid-ALL,MIX 89 Carrier/Tracer Recovery Liquid Scint Pe55, Liquid-ALL 82 Carrier/Tracer Recovery Liquid Scint Ni63. Liquid-ALL 82 Carrier/Tracer Recovery Liquid Scint Tc99, Liquid-ALL 100 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| 106
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| GENERAL ENGINEERiNG LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project. Quarterly Groundwater PO# 002337 Page 3 of 3 Client Sample ID:' *MWI03D-0204-001 Proiect: YANK00304 Sample ID: 116165015 Client ID: YANK001 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd..
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| 13D Flag for results below the MDC or a flag for low tracer recovery.
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| E Concentration of the target analyte exceeds the instrument calibration range.
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| H Analytical holding time exceeded.
| |
| J Indicates an estimated value The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X. Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis. .1J This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| M '~i~QW xQ Reviewed by 107
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis 7 Company: CYAPCo Address: Haddam Neck Plant 362 Injun l1dilow Road
| |
| ;East Hampton' Conniecticut 06424 ReportDate: July31 2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 - . Page I of 3 Client Sample ID: " '-MW105S-0204-001 Proiect: YANK00304 Sample ID: - - - 116165016 Client 1D: YANK001 Matrix: Ground Water Vol. Recv.:
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| Collect Date: JUN Receive Date: 02-JUL-04 Conlltriv lie-nt Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate 'Time Batch Mtd.
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| Rad Alpha Spec Analysis AlphaspecPu, Liquid-ALL Plutonium-238 U 0.0669 +/-0.170 0.155 +/-0.170 0.392 pCVIL BIB 1 07/24104 1532 350489 1:.
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| Plutonium-239/240 U 0.062 +/-0.107 0.0693 +/-0.107 0.221 Am241,Cm, Liquid-ALL pCi/L Americium-241 U - -0.0224 +1-0.0254 0.0615 +1-0.0255 0.207 BIB1 07124/04 1532 3504882 pCi/L Curium-242 U 0.00 +/-0.0681 - 0.00 +1-0.0681 0.0941 pci'L Curium-243/244 U -0.00375 +/1-0.118 0.128 +/-0.118 0341 uid Scint Pu241, Liquid-ALL
| |
| \_iutonium-24 -1 U 832 +1-7.85 637 +/-7.89 13.1 pCi/L BlBI 07/28/04 12563504903 Rad Gamma Spec Analysis Gammaspec, Gaima,Liquid-ALLGAM2,SMND MIXPENNLF Americium-241 U 2.96 +1-7.67. 6A1 +/-7.52 13.2 .pCi/L SRB 07/19/04 2202 346800 4 Cesium-134 U 0.651 +/-131 1.09 +/-1.28 2.34 *pCi/L Cesium-137 U -0.409 +/-1.22 0.952 +1-1.19 2.03 pCi/ll Cobalt-60 U 0.984 +/-1.30 1.15 +/-1.27 2.50 pCi/L Europium-152 U 2.86 +1-4.15 3.09 +/4.07 6.44 pCi/L Europium-154 U 0348 +/-3.15 2.63 +/-3.09 5.79 pCi/L Europium-155 U -0.109 +1-533 4.33 +/-5.23 8.89 pCi/L Manganese-54 U -0.828 +/-1.25 0.997 +/-1.23 2.13 pCi/L Niobium-94 U 0.968 +/-1.15 0.988 +1-1.13 2.09 pc/L' Silver-108m U 0.352 +/-IA3 1.06 +/-lA0 2.21 pc/LL Rad Gas Flow Proportional Counting GFPC, Sr90, liquid-ALEMIX Strontium-90 16.2 +/-1.71 0.633 +1-4.32 1.38 pCiUL HOB I 07/15/04 1408 347780 5 Gross AI, liquid-ALS7NDMIXPENNLF Alpha U 0.163 +/-1.18 0.876 +/-1;20 2.01 *ATH I 0`7/26/04 1949 350566 6 Beta 443 +/-2.70 0.688 +t-2.74 IA8 Rad Liquid Scintillation Analysis
| |
| .LSC, TritiumDist,Liquid-ALS7NDMrXPENN pcu/L Tritium 3350 +/-263 138 +/-268 277 JLBi 0,7/204 0836 348827 7 pci/L Liquid Scin C14, Liquid-ALL
| |
| *Carbon-14 U -14.7 +/-43.6 36.8 +/-44.0 743 PD) 07/09/04 1521 347077 8 Liquid Scnt Fe5S Liquid-ALL Iron-55 U 9.02 +/-13.4 6.11 +/-13.4 12.6 JLB I 0`7121/ 2328 349214 9 LiquidSci Ni63, Liquid-ALL 108
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| | |
| *NIERNGEEA AOAOIS L
| |
| '-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charileston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysisi.
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 2 of 3 Client Sample ID: MWI05S-0204-001 Project: YANK00304 Sample ID: 116165016 Client ID: YANK001 Vol. Remv.:
| |
| Parameter Qualifier Resuit Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Liquid Scintillation Analysis Liquid Scint M;63, Liquid-ALL Nickel-63 U -0.892 +/-7.62 6.41 +1-7.62 13.1 pCilL JLBI 07/2l/04 1244 349216 10 LiquidScint Tc99, Liquid-ALL Tcchnedum-99 U -2.65 +/4.74 4.05 +/-4.74 8.33 pCi/L DAMI 07/25/04 2151 348813 11 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW8463005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed i )
| |
| Method Description I DOE EML HASL-300, Pu-1lI-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-i I-RC Modified 4 EPA 901.1 5 EPA 905.0 Modified 6 EPA 900.0 7 EPA 906.0 Modified 8 EPA EERP C-01 Modified 9 DOE RESL Fe-l, Modified 10 DOERESLNi-1,Modified 11 DOE EML HASL-300. Tc-02-RC Modified Surrogatefrracer recovery Test Recovery%, Acceptable Limits Plutonium-242 Alphaspec Pu, Liquid-ALL 91 (15%-125%)
| |
| Americium-243 Am241,Cm, Liquid-ALL 84 (2.5%-125%)
| |
| Carriertlracer Recovery Liquid Scint Pu241, Liquid-ALL 78 Carrier/Tracer Recovery GFPC, Sr9O, liquid-ALLMIX 94 Carrier/Tracer Recovery Liquid Scint Fe55, Liquid-ALL 84 Carrier/Tracer Recovery Liquid Scint Ni63, Liquid-ALL 80 Carrier/Tracer Recovery Liquid Scint Tc99, Liquid-ALL 100 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| 109
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| GENERAL ENGINEERING LABORATORIES, LLC GENERAL-ENGINEERING LABORATORIES,-.LLC 2040 Savage Road Charleston SC 29407- (843) 55-8171 - www.gel.com Certificate of Analysis.-
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 3 of 3 Client Sample ID: MW1O5S-0204-001 Proiect: YANKO0304 Sample ID: -116165016 .. .. Clientn.ID: YANK001 :
| |
| . I:
| |
| Oral voL. £¶.cCv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU . MDA Units DF AnalystDate 7lme Batch Mtd.
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value.; The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| U) Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| _A, Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by i ,'I
| |
| . I .
| |
| 110I
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES,.LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 3 Client Sample ID: MW600-0204-001 Proiect: YANK00304 Sample ID: 116165017 Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 29-JUN-04 Receive Date: 02-JUL-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Alpha Spec Analysis Aiphaspec Pu, Liquid-ALL Plutonium-238 U -0.00849 +1-0.0166 0.0403 +1-0.0167 0.176 pCi/L BJBI 07/24/04 1532 350489 1 Plutonium-239/240 U 0.0368 +4-0.103 0.0806 +1-0.104 0.257 pCVL Am24],Cm, Liquid-ALL Arnericium-241 U -0.014 +/-0.0724 0.0889 +1-0.0724 0.264 pctLL BJBI 07/2410415323504882 Curium-242 U -0.0256 +/-0.0289 0.0701 +/-0.0291 0.236 pCi/L Curium-243/244 U 0.0689 +/-0.164 0.145 +t-0.165 0.377 pCV/L LiquidScint Pu241, Liquid-ALL Plutonium-241 U 6.14 +1-6.59 5.37 +J-6.61 11.0 pC/LL BJBI 07/28/04 1343 3504903 Rad Gamma Spec Analysis Gammaspec, GammaLiquid-ALL, GAM2ZSTND,MlX PENNMLF Americium-241. U -0.466 +1-3.55 2.90 +/-3.48 6.07 PCi/L SRB 0720/04 1010 346800 4 Cesium-134 U 1.80 +/-3.45 2.16 +/-3.38 4.73 pCi/L Cesium-137 U -1.62 +/-2551 1.98 +/-2.46 4.32 pCi/L Cobalt-60 U 1.78 +/-2.09 2.01 +/-2.05 456 pCi/L Europium-152 U -2.89 +1-5.06 3.94 +1-4.96 852 pCi/L Europium-154 U -2.95 +/-7.66 6.12 +/-7.51 13.7 pCi/L Europium-155 U 1.05 +/-5.77 4.67 +1-5.65 9.78 pCiLL Manganese-54 U 0.381 +/-2.34 1.97 +1-2.29 4.33 pCi/L Niobium-94 U 0.716 +/-2.15 1.86 +1-2.10 4.04 pCi/L Silver-108m U 0.469 +/-1.75 1.46 +/-1.71 3.17 pCi/L Rad Gas Flow Proportional Counting GFPC,Sr90, liquid-AL4lIX Strontium-90 16.8 +/-1.73 0.609 +1-4.73 1.33 pCi/L HOBi 07/15/04 1408 347780 5 GrossAI, liquid-ALLSTND.M]XPENNLF Alpha U 0.257 +/-1.19 0.942 +1-1.19 2.14 pCi'L ATHI 07/26104 1949 350566 6 Beta 43.2 +/-2.72 0.860 +/-2.75 1.83 pCV/L Rad Uquld Scintillation Analysis LSC, Tritium Dist, Liquid-AL4STNDMLXPENN Tritium 3270 +/-260 138 +1-266 276 pCV/L JLBI 07120/04 0939 348827 7 Liquid Scint C14, Liquid-ALL Carbon-14 U -13.2 +/-44.0 -37.1 +1-44.3 74.9 pCi/L PD. 07109/04 1655 347077 8 Liquid Scint FeSS, Liquid-ALL Iron-55 U 1.85 +/-11.3 5.28 +/-11.3 10.9 pCi/L JLBI 07/22t04 0030 349214 9 LiquidScintNi63, Liquid-ALL 111
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES., LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis.
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton. Connecticut 06424 ReportDate: July31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer I . . .
| |
| Project: Quarterly Groundwater PO# 002337 - I Page 2 of 3 Client Sample ID: : ' MW600-0204-001 Project YANK00304- .
| |
| Sample ID: . 116165017 Client ID: YANKOOI -
| |
| Vol. Recv.:
| |
| Parameter . Qualifier Result Uncertainty LC
| |
| * TPV MDA Units - DF AnalystDate Tlme Batch Mtd.
| |
| Rad Liquid Sclntillatlon Analysis Liquid ScintNi63, Liquid-ALL Nickel-63 U -4.7 +/-7.26 6.21 +/-7.26 12.7 pCi/L JLBI 07/21104 1315 349216 10 Liquid Scint Tc9, Liquid-ALL Technctium-99 U -2.31 +/-4.78 4.08 +1-4.78 8.39 pCi/L DAI1 07/25/04 2223 348813 11 Ihe following Prep Methods were performed Method Description Analyst Date - Time .PrepBatch S46 3005A ICP-MS 3005 PREP - CJ 07/16/04 1844 346376
| |
| ,.e following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Pu-11-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HAS1300. Pu-11-RC Modified 4 EPA 901.1 5 EPA 905.0 Modified 6 EPA 900.0 7 EPA 906.0 Modified 8 EPA EERF C-01 Modified 9 DOE RESLFc-1, Modified 10 DOE RESLNi-l,1Modified 11 DOE EML HASL-300, Tc-02-RC Modified Surrogatefracer recovery Test Recovery% Acceptable Limits Plutonium-242 Alphaspec Pu, Liquid-ALL 84 (15%-125%)
| |
| .Americium-243 Am241.Cm, Liquid-ALL 91 (25%-125%)
| |
| Carrier/lracer Recovery liquid Scint Pu241. Liquid-ALL 92 CarrierlTracer Recovery GFPC, Sr90, liquid-ALLMIX 86 Carrierfrracer Recovery Liquid Scint Fc55, Liquid-ALL 87 CarrierJIracer Recovery Liquid Scint Ni63, Liquid-ALL 81 Carrierlracer Recovery Liquid Scint Tc99, Liquid-ALL 99 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| 112
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Chauleston SC 29407 - (843) 556-8171 - www.gel.com KJ
| |
| * Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project. Quarterly Groundwater PO# 002337 Page 3 of 3 Client Sample ID: MW600-0204-001 Proiect: YANK00304 Sample ID: 116165017 Client ID: YANKOO1 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UT Unccrtain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewe Qby4 Reviewed by 113
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31,2004 Contact Mr. Davc Keefer Project: 'Quarterly Groundwatei PO# 002337 Page lof 2 Client Sample ID: - MW508D-0204-001: Projiect: YANK00304 Sample ID: I - 116165018 1 Client ID: YANK001 Matrix: Ground Water Vol. Recy.:
| |
| Collect Date: 30-JUN-04
| |
| -i Receive Date: 02-JUL-04 Collector. Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysts Gammarpec, GammaLiquid-AU4 GAMS2,TND,MJXPENNLF Arnericium-241 U -431 +/-9.85 7.87 +1-9.6S
| |
| * 16.2 pCi/L - SRB ' 07/19/04 2230 346800 1 Cesium-134 U .0.616 +/-157 1.33 +/-1.54 2.83 - pCi/L Cesium-137 U 0557 +/-153 1.31 +/-150 2.76 - pCi/L. . . , . ..
| |
| Cobalt-60 U 0.145 +1-159 1.33 +1-155 2.87 pCOIL Europium-152 U 0.207 4+-4.29 351 +/-4.21 733 pCiIL.
| |
| iropium-154 U -2.0 +-450 3.00 +1-4.41 657 - pCi/L
| |
| ' _uropium-155 U -0.886 +/-5.94 4.71 +/-5.82 9.69 - pCilL Manganese-54 U -0.871 +1-1.36 1.05, .+/-1.34 2.26 pCi/L Niobium-94 U -0.55 +/-1.33 1.07 +/-1.30 2.26 pCill S I . I .
| |
| Silver-108m U 0.137 +/-1.43 1.16 +/-1.40 2.44 pCi/L-Rad Gas Flow Proportional Counting . I GrossA/B, liquid-ALSTNDM1XPENNLF I I . I . I - .. . .
| |
| Alpha 758 +/-1.85 0.915 +/-196 - 2.07 pCi/L ATHI 07t26t04 1949 350566 2 Beta 6.68 +/-1.22 0.677 +/-1.22 IA6 pCUL Rad Liquild Scintillation Analysis LSC, Tritium Dist, Uquid-ALL1S7ND.MIX.PENN Tritium U -11.5 +1-161 135 +/-161 270 pCi/L JLB1 07/20/04 1042 3488273 .
| |
| The following Prep Methods were performed Method Description Analyst Date Tune Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16t04 1844 346376 The following Analytical Methods were performed Method Descriptlon I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are defimed as follows:
| |
| 1 Target analyte was detected in the sample as well as the associated blank.
| |
| 114
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Chaleston SC 29407 - (843) 556-8171 - www.gel.com K)
| |
| Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton. Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW508D-0204-001 Proiect: YANK00304 Sample ID: 116165018 Client ID: YANKOOI Vol. Recv.:
| |
| Parameter Qualrifer Result UncertaLnty LC TPU MDA Units DF AnalystDate Time Batch Mtd BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC K).-
| |
| standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 115
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES,,LLC
| |
| '2040 Savage Road Charleston SC 29407. (843) 556-8171 - www.gel.com Certificate of Analysis,-
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 ReportDate: July31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer . P e..IoI Project: Quartetly Groundwater PO# 002337 -. ,I~ Page I of -2 Client Sample ID: -
| |
| * MW-100S-0204-001 Project: YANK003O4 -.
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| Sample ID: -_116165019 Client ID: YANKOOl ~'.
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| Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 30-JUN-04 Receive Date: - 02-JUL-04 .
| |
| Collector. Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GammaLiquid-AL4GAW2,S7ND,MIX,PENNLF Americium-241 U 4.94 +/-12.2 9.64 +/-11.9 20.0 pCiLL SRB 07/19104 2216 346800 1 Cesium-134 U 0.331 l4/-}25 1.05 +1-1.23 2.26 pCilL Cesium-137 U 0.612 +l-2.43.7 : 1.04 +/-2.38 2.21 pCilL Cobalt-60 U 0.0636 +/-120 1.01 +/-1.18 2.22 .pCUL,--
| |
| Europium-152 U 3.57 +1-4.29 3.15 +/-421 6.59 pCi/L, -
| |
| '4ropium-154 U 2.53 +l-3.62 324 +t-3.55 7.03 pCi/'L
| |
| ,luropium-155 U -3.37 +1-4.72 3.87 +/-4.62 8.01 Mangancsc-54 U 0.200 +1-131, 1.08 +/-1.28 230 Niobium-94 U 0.136 +/-1.14 0.947 *+/-1.12 2.02 pCi/L Silver-108m U 0.410 +/-1.12 0.966 -: +/-1.09 2.04 Rad Gas Flow Proportional Counting pci/L GrossAMB, liquid-ALL.STNDM1XPEIVNLF pCi/L Alpha U 0.253 +/-1.04 1.02 +/-1.04 2.27 Anhii 07W2/04I1D29 350566 2 Beta 1.51 +/-0.849 0.700 +/-0.849 1.50 Rad Liquid Scintillation Analysis LSC Tritium Dist, Liquid-AILSTNDMIXPENN Tritium lU 80.4 +/-172 142 +/-172 284 pCi/L .JLBI 07/20'04 1145 348827 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP Cl 07/16/04 1844 346376 The following Analytical Methods were performed Method Description I
| |
| * EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| Mie Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| 116
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| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date. July 31,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-I00S-0204-001 Proiect: YANK00304 Sample ID: 116165019 Client ID: YANKOOI Vol. Recv.:
| |
| Parameter Quallfer Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The resultwas greater than the detection limit, but less than the reporting limiL U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification forgamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 117
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| | |
| GENERAL ENGINEERiNG LABORATORiES, LLC GENERAL' ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 - ReportDate: July3l,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MW-504-0204-001 Proiect: YANK00304 Samlle ID: 116165020 Client ID: YANKOOI Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 30-JUN-04
| |
| -- Receive Date: 02-JULs04 P ruliemor Reult U L T Ut --
| |
| -, Parameter Quallfier Result Uncertainty LC TPU MDA UnItS DF AnalystDate Time BatchMtd.
| |
| Rad Gamma Spec Analysis Goammaspec., Gamma4Liquid-AL 4 GAM2 S7NDMIXPENNLF Americium-241 U 10.1 +1-7.82 6.25 +1-7.67 12.! pCilL SRBS - 07/19/04 2308 346800 1 Cesium-134 U -1.5 +1-134 0.927 * +1-132 2.03 pCi/L Cesium-137 U 0.716 +1-1.29 ' - 1.10 +1-1.26 234 pCitL -. : _ : J-., - - - - I- . I Cobalt-60 U 0.186 +1-135 1.11 +t-132 2A6 , pCi/LL , -1 , . - - . . ., . . ;
| |
| Europium-152 - U 2.15 +1-3.97 ' 3.44 3.89
| |
| + 7.18 pCi/L;
| |
| 'uropium-154 U 3.40 +1-538 2.93 +1-5.28 650 pCVL.
| |
| K--uropium-15S U -0.575 +1-4.65 3.85 +1 456 7.96 pCi/L Manganese-54 U -0.528 +/-133 1.08 +1-131 233 PCI/L Niobium-94 U -0.449 +1-1;2!1 0.943 +1-1.19 2.02 pCitL Silver-108m U 0.255 +/-1.19 ' 1.00 +1-1.17 2.12 pCitL Rad Gas Flow Proportional Counting Gross AJB, liquid-A~LSTNDMIX.PENNPJLF Alpha U 0.767 +1-1.01 0.872 +t-1.01 1.97 pCi/L - - ATHi 0721/04 1029 350566 2 '
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| Beta 3.40 +1-0.945 0.621 +/-0.945 1.35 pCi/L Rad Llquid Scintillation Analysis lSC Tritium Dist Liquid-AL.STND.MIX.PENN Tritiurn 276 +1-174 138 +1-174 275 pCirL JLB1 07/20/04 1249 348827 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CJ 07/16t04 1844 346376 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| 118 -
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| GENERAL ENGINEERING LABORATORiES, LLC GENERAL ENGINEERING LABORATORIES., LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample 1D: MW-504-0204-0O1. Proiect: YANK00304 Sample ID: 116165020 Client ID: YANK001 Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| fif Camp y Reviewed by 119
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| GENERAL ENGINEERING LABORATORIES, GENERAL ENGINEERING LABORATORIES., LLC 2040 Savage Road Chaleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant
| |
| ,362 Injun Hollow Road East Hampton. Connecticut 06424 .'ReportDate: July3l,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project. Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID:: ., ::; MW-508S-0204-001- : CProiect: YANK00304 ;
| |
| Sample ID: -'116165021 Client ID: YANK001I
| |
| - Matrix: ' Ground Water Vol. Recv.:
| |
| Collect Date: 30-JUN-04 Receive Date: 02-JUL-04.
| |
| Collector. Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, Gamma Liquid-AL1 GAMZSTND,MTX PENNMLF Americium-241 U 6.14 +/-9.72 8.63 +1-9.53 18.2 pCi/L SRB 07/25/04 1611 346820 1.
| |
| Cesium-134 U -0.251 +/-1.86 1.50 +/-1.82 3.37 pCi/L Cesium-137 U 0.576 +/-1.63 1.42 *+l-1.60 3.16 pCi/L Cobalt-60 U 5.24 *+1-2.64 2.69 +1-2.58 5.87 1pCi1L I:
| |
| .uropium-152 U -1.32 +1-5.16 4.04 +1-5.06 8.71 pCi/L ropium-154 U 139 +14.77 4.05 +14.67 9.40 pCi/L iropium-155 U 524 +/-6.92 6.07 +/-6.79 12.7 pCiJL Manganese-54 U -0.0592 +1-1.68 1.37 +/-1.64 I 3.08 pCi/L Niobium-94 U -0.304 +/-155 1.25 +1-1.51 2.78 pCi/L Silver-108m U -0.0515 +t-1.76 1A0 +1-1.73 3.03 ' pCi/L Rad Gas Flow Proportional Counting Gross AM, liquid-ALUSTNDMlXPENNLF Alpha U 0.356 +1-1.12 1.02 +/-1.12 2.28 pCi/L ATHI 07127104 1430 3505662 -:
| |
| Beta 4.50 +1-1.09 0.719 +/-1.09 154 pCi/L Rad Liquid Sclntlllatlon Analysis LSC Tritium Dist, Liquid-ALl.SZNDMlX.PENN Tritium U 157 +/-174 141 +/-174 282 pCi/L JLBI 07/20/04 1352 348827 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP FG4 07/15/04 1000 346378 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 900.0 3 EPA 906.0 Modified Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| 13 Target analyte was detected in the sample as well as the associated blank.
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| 120
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| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: July 31, 2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sample ID: MW-508S-0204-001 Proiect: YANK00304 Sample ID: 116165021 Client ID: YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch MtdL BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limnit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 121
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| : 9. ,i QUALITY CONTROL DATA 122 -
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Rewort Date: July 31, 2004 Client: CYAPCo Page 1 of 12 lHaddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut
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| | |
| ==Contact:==
| |
| llr. Dave Keefer Workorder: 116165 Parnmame NObl Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 3504SS QC1200666550 116165014 DUP Amcricium-241 U 0.0272 U 0.05S4 pCi/L 73 (0% - 100%) BIB I 07(24/04 15:32 Uncert: +/-0.142 +/-0.101 TPU: +1-0.142 +t-0.101 Curium-242 U 0.00132 U 0.0319 pCi/L 184 (0% - 100%)
| |
| Uncert: +/-0.0717 +/-0.0626 TPU: +/-0.0717 +/-0.0627 Curium-243/244 U 0.064 U 0.0103 pCi/L 145 (0%- 100%)
| |
| Uncert +l-0.153 +/-0.107 TPU: +/-0.153 +1-0.107 QC1200666552 LCS Americium-241 13.4 13.4 pCi/L 100 (75%-125%) 07124/04 15:32 Uncert: +l-1.25 TPU: +/-2.03 Curium-242 U -0.00739 pCi/L Uncert +/-0.0621 1TU: +/-0.0622 Curium-243/244 17.2 17.1 pCiL 99 Uncert: +/-1.42 TPU: +/-2.48 QC1200666549 MB Americium-241 U 0.0784 pCi/L 07(24/04 15:32 Uncert: +1-0.155 TPU: +1-0.155 Curium-242 U -0.0242 pCi/L Uncert +/-0.0274 TPU: +/-0.0275 Curium-243/244 U 0.0465 PaI/L Uncerte +/-0.158 TPU: +1-0.158 QC1200666551 116165014 MS Americium-24 1 U 0.0272 12.5 pCi/L (75%-125%) 07/24/04 15:32 Uncert: +/-0.142 +/-1.27
| |
| '[PU: +/-0.142 +1-1.99 Curium-242 U 0.00132 U -0.0074 PCi/L Uncert +/-0.0717 +1-0.0823 TPU: +/-0.0717 +1-0.0823 Curium-243/244 U 0.064 18.5 pCi/L Uncert: +/-0.153 +l-1.55 TPU: +/-0.153 +l-2.75 Batch 350489 QC1200666554 116165014 DUP Plutonium-238 U -0.0134 U -0.0193 pCi/L NIA (0% - 100%) BJB I 07/24/04 15:32
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| 'j 123
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary XVV-k1 9 cc 1161
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| ........ I..
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| : a. I) .- Page 2of 12 Parmname . NON - Sample Qua] : OC Units RPD% REC% Range Anist Date Time Rad Alnha Soec Batch 350489 Uncert: +1-0.0691 +/-0.0657 IPU: +1-0.0691 +/-0.0658 Plutonium-239/240 u -0.0146 U; -0.0272 pCilL N/A (0% - 100%)
| |
| Uncert: +/-0.0202 - +/-0.0266 TPU: +/40.0203 : +/-0.0267
| |
| . QC1200666556 LcS Plutonium-238 U 0.290 pCi/L (75%-125%) 07/24/04 15:32 Uncert: +/-0.225 1PU: +-0.228 t/
| |
| Plutonium-239/240 12.0 I. 10.7 pCi/L : 90 (75%-125%)
| |
| Uncert: +/-1.13.
| |
| lPU: +/-1.67 QC1200666553 MB Plutonium-238 U 0.0694 pCi/L 07124/04 15:32 Uncert: - +/-0.106 TPU: +1-0.106 Plutonium-239t240 U . 0.214 pCilL Uncert: +/-0.171 WPU: +/-0.172 QC1200666555 116165014 IMS
| |
| 'lutonium-238 -0.0134 U 0.0349 pCi/L (75%-125%) 07124/04 15:32 Uncert: +1-0.0691 +/-0.0787 TPU: +1-0.0691 +1-0.0788 Plutonium-239/240 12.0 U -0.0146 11.1 , pCi/L - 93 (75%-125%)
| |
| Uncert: +1-0.0202 +1-1.08 TPU: +1-0.0203 +1-1.64:
| |
| Batch 350490 QC1200666558 116165014 DUP Plutonium-24 1 U 0.00 U 1.38 pCi/L 0 (0%- 100%) DIB 1 07/28/04 15:16 Uncert: +/-6.53 +1-633 TPU: +/-653 - +1-6.33 QC1200666560 LCS Plutonium-24 1 70.7 67.8 pcV/L 96. (75%-125%) 07128/04 16:49 Uncert: +1-458 TPU: +1-735 QC1200666557 MB Plutonium-241 U 1.21 pCi/L 07128/04 14:29 Uncert: -. +/-2.81 TPU: .+/-2.81 QC1200666559 116165014 MS Plutonium-241 177 U 0.00 -1 161 PCVL 91 (75%-125%) 07128104 16:02 Uncert: +/-653 .- I+/-10.6 .
| |
| TPU: +1-653 +-17.2.
| |
| Rad Gamma Spec Batch 346800 QC1200657518 116165001 DUP Americium-24 1 U 0.753 U -7.51 pCi/L N/A: (0% - 100%) SRB 07/21204 14:41 Uncert: +1-2A5 +/-13.3
| |
| +/-13.1 124 .
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 116165 Page 3 or 12 Parnmame NONM Sample Qual QC Units RPD% REC% Range Anist Date Time Red Gannma Spec Batch 346soo TPU: +/-2A0 Cesium-134 U -0.753 U 1.23 pCiL NIA (0%- 100%)
| |
| Uncert: +/-1.87 +1-3.33 TPU: +1-1.83 +1-3.27 Cesium-137 U 1.45 U 0.526 pCi/L 93 (0%- 100%)
| |
| Uncen +1-1.86 +1-2.31
| |
| [PU: +/-1.82 +/-2.26 Cobalt-60 U 0.194 U -1.34 pCi/L N/A (0%O-100%)
| |
| Uncent: +/-1.86 +1-2.01 TPU:
| |
| lPU: +1-1.82 +1-1.97 Europium-152 U 0.288 U -0.445 pCi/L NIA (0% - 100%)
| |
| Uncert: +/-3.89 +1-7.36
| |
| +/-3.81 +1-7.21 Europium-154 U 2.66 U -0572 pCilL NIA (0%- 100%)
| |
| Uncent +1-4.74 +1-5.09 TPU: +14.64 +14.99 Europium- 155 U -1.15 U 3.38 pCiJL N/A (0%- 100%)
| |
| Uncent +14.20 +I-8.34 TPU:
| |
| TPU: +1/4.11 +I-8.17 Manganese-54 U 0.368 U 0.0673 pCi/L 138 (0% - 100%)
| |
| Uncert: +/-1.70 +1-2.01
| |
| +/-1.67 +1-1.97 Niobium-94 U 0.0195 U -1.81 pCilL NIA (0% - 100%)
| |
| Uncent +1-1.70 +1-1.88 TPU: +1-1.67 +1-1.85 Silver- 10Sm U -1.55 U -1.84 pCilL NIA (0% - 100%)
| |
| Uncert: +I-IA0 +1-2.34 TPU: +/-1.37 +1-2.29 QC1200657520 WCS Americium-24 1 1170 1300 pCi/L III (75%-125%) 07/20/04 16:06 Uncert:
| |
| Uncert: +1-254 lPU: +/-24S Cesium-134 U 1.95 pCi/L
| |
| +1-13.8 TPU: +1-13.5 Cesium-137 461 523 pCi/L 114 (75%-125%)
| |
| Uncert +1-50.6 lPU: +/49.6 Cobalt-60 70S 738 pCiL 104 (75%-125%)
| |
| Uncent +1-69.5
| |
| +1-68.1 Europium-152 U 20.5 pCi/L Unceit +/-283 IPU: +/-27.7 Europium-154 U 4.16 pCifL Uncein +/-25.0
| |
| +1-24.5 Europium-155 .U 38.2 pCi/L 125
| |
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Rohd Charleston SC 29407 - (843) 556-8i71 - www.gelxcom
| |
| -QCSummary :--
| |
| NWork-order 116165 . QPage 4f 12 Parmname - . NONM Sample QualF,' QC Units RPD% RFC% Range Anlst Date Tlme RD-A C-masS~
| |
| Batch 3446SOO Uncert: +143.4 1WU: ' +1425 Manganese-54 U -6.23 pCV/L Uncert: +1-10.8 IPU: +1-10.6 Niobium-94 U ' -6.01 pCV/L Uncert +1-10.2 TPU: +/-10.0 Silver-lOSm U - 0.426 pci/L Uncert +1-9.57 TPU: * +1-937 QC1200657517 MB Americium-241 U 1.21 pCi/L 07/20104 10:10 Uncert: . +/-10.9 TPU: +/-10.7 Cesium-134 U 0.173 pCi/L Uncert: +/-2.07 TPU: +/-2.02 Cesium-137 U -0.48 pCa/L Uncert: +/-1.95 TPU: . +/-1.91
| |
| \,obalt-60 U -0.159 pCi/L
| |
| * Uncert: +/-2.02 TPU: +/-1.98 Europium-152 U -0.246 PCVL Uncert: +/-5.07 TPU: *- +14.97 Europium-154 U 0.0444 p.CiL
| |
| * Uncert: +1-5.49 flPU: +/-5.38 Europium-155 U . 3.62 pCiIL Uncert: +/-5.23 IPU: +/-5.12 Manganese-54 U.- 1.17 pCiIL Uncert: +/-1.92 TPU: +/-1.89 Niobium-94 U 0.331 PCiIL Uncert: +/-1.65 IPU: +/-1.62 Silver-108m U . 0.257 pCV/L Uncert ; +/-1.60 IPU: +/-1I57 QC1200657519 116165001 MS Americium-241 9360 U 0.753 8440 pCi/L 90 07/22t04 17:28 Uncert: , +/-2.45 I . .+/-1610, TPU: +1-2AO . +/-26500 Cesium-134 Ui -0.753 U -72.4 pCilL Uncert: +/-1.87 +-167 lPU: +1-1.83 +/-280 126
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 116165 Page 5 of 12 V--mnnmn ?,r%I C nl%..!.I rn , ' T :2.. nn - n n n n-w, - -.,.
| |
| ... -I.. *'I 'J... '.p.p.. umAs u.iua , ru" y lJL..'o e AfISL vaic a'e Inime Rad Gamma Spec Batch 346800 Cesium- 137 3690 U 1.45 4130 pCi/L 112 Uncert: +/-1.86 +/-524 TPU1: +t-1.82 +/-13000 Cobalt-60 5640 U 0.194 6770 pCi/L 120 Uncert: +/-1.86 +1-633 TIPU* +/-1.82 +/-21200 Europium- 152 U 0.288 U 121 pCilL Uncert: +/-3.89 +/-384 TPU:1: +t-3.81 +/-535 Europium-154 U 2.66 U 269 pCi/L Uncert +/-4.74 +/-277 TPU: +1/4.64 +/-886 Europiumn-155 U -1.15 U 420 pCiL Uncert: +/-4.20 +/-446 TPU: ': +/-4.11 +/-1390 Manganese-54 U 0.368 U 89.6 pCi/L Uncer: +1-l.70 +1-148 IPU: +/-1.67 +/-316 Niobium-94 U 0.0195 LI 115 pCVL Uncert +/-1.70 +/-131 TPU: +/-1.67 +/-383 Silver- 108m U -1.55 U -67.4 pCi/L Uncert: +/-1.40 +/-148 TPU: +/-1.37 +/-257 Batch 346s20 QC1200657552 116165021 DUP Americium-24 1 U 6.14 U -3.43 pCi/L N/A SRB 07/26/04 09:35 Uncert: +/-9.72 +/-1 1.0 TPU : +/-9.53 +/-10.7 Cesium-134 U -0.251 U 0.827 pCVL N/A (0% - 100%)
| |
| Uncett: +/-1.86 +/-2.01 TPU -: +1-1.82 +/-1.97 Cesium-137 U 0.576 U 1.80 pCi/L 103 (0%- 100%)
| |
| Uncert +/-1.63 +/-1.95 TPU:1: +/-1.60 +/-1.91 Cobalt-60 U 5.24 U 0.703 pCi/L 153 (0%- 100%)
| |
| Uncert +/-2.64 +/-1.68 TPU : +/-2.58 +/-1.65 Europium-152 U -1.32 U -0.25 pCi/L N/A (0%- 100%)
| |
| Uncert: +/-5.16 +/4.83 TPU *: +/-5.06 +/-4.73 Europium-154 U 1.39 U 2.34 pCi/L 51 (0% - 100%)
| |
| Uncert: +/-4.77 +/4.98 TPU: +/-4.67 +/4.88 Europium-155 U 5.24 U 3.27 pCi/L 47 (0% - 10D%)
| |
| Unclit +/-6.92 +/-6.74 IT'll; +/-6.79 +/-6.60 Manganese-54 U -0.0592 U -0.761 pciVL N/A (0%- 100%)
| |
| 127
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com QC Summary Workorder 116165 Page 6cr 12 PsrmnnmP . WTnX1q . C. n.. "f, 117-11 """M- T)Vflef A . "-.- ,
| |
| rAr.lL - *f.S I - -atp- IC Wl u-.,ls nr-£o .V -rfto At 'IM1L Arait uFmt Rad Gamma Spec Batch 346520 Uncert +1-1.68 " +/-1.60 1
| |
| 11U: +/-1.64 '+/-1.57 Niobium-94 U -0.304 U -0.177 pCi/L N/A (0% - 100%)
| |
| Uncen +/-155 +/+1-1.60
| |
| -TPU: +1-1.51 +1-157 Silver-10Sm U -0.0515 U 0388 pCi/L NIA: (0% -100%)
| |
| Uncent: +/-1.76 +/-1.62 .
| |
| TPU: +/-1.73 +/-1.59 QC1200657584 LCS Americium-241 1170 1230 pCi/L 105 (75%-125%) 07/28/04 12:19 Uncert: +1-163 TPU: +/-159 Cesium-134 U ' -3.13 pCi/L Uncert: :+-7.92 TPU: +/-7.77 Cesium-137 461 480 pCi/L 104 (75%-125%)
| |
| Uncert: +/4 1.0 1PU: +/40.2 Cobalt-60 709 762 pCVL 108 (75%-125%)
| |
| Uncert: +/-605
| |
| - PU: +/-593
| |
| \ -iropium-152 U -5.35 pCi/L Uncert: +/-193 lPU: +/-18.9 Europium-154 U -6.69 pCi/L Uncert: +/-17.4 TPU: +/-17.0 Europium-155 U -14.5 pCi/L Uncert: +/-27.6 TPU: +/-27.0 Manganese-54 U -5.14 pCi/L Uncert: - +/-8.21 TPU: +/-8.05 Niobium-94 U ' 3.62 pCi/L Uncent +/-6.89 TPU: +/-6.75 Silver-108m U -1.26 'pCi/L Uncert: +/-6.90 TPU: : +/-6.77 QC1200657551 NIB Americium-24 1 U .- 5.76 07/25/04 16:12 Uncert: .+/-15.4 TPU: * /-15.1 Cesium-134 U -2.01 pCi/L Uncert: +/-3.16 TIPU: +/-3.09 Cesium-137 .U 1.01 .pCi/L Uncertn '+/-1.97 ITU: +/-1.93 128
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder 116165 Page 7nr 12 Parmname NOM . Sample Qual QC Units RPD% REC% Range AnIst Date Time Rnd Gamma Spec Batch 346820 Cobalt-60 U 0.188 pCitL Uncert +1-1.83 TPU: +/-1.80 Europium-152 U 2.13 pCVL Uncert. +/-5.65 TPU: +1-5.53 Europium-154 U -0515 pCi/L UncerLt +/-5.15 TPU: +1-5.05 Europium-15S U -2.67 pCi/L Uncert +/-7.64 TPU: +1-7.48 Manganese-54 U -0.241 pCi/L Uncent: +/-2.05 TPU: +/-2.01 Niobium-94 U 0.258 pCi/L Uncert: +/-1.97 TPU: +/-1.93 Silver-108m U -0.831 pCi/L Uncert +/-2.08 TPU: +/-2.04 QC12006575S3 116165021 MS Americium-241 9360 U 6.14 10200 pCi/L 109 07/26/04 14:47 Uncert: +1-9.72 +1-1530 TPU +/-9.53 +/-32200 Cesium-134 U -0.251 U -80.3 pCi/L Uncert +/-1.86 +/-113 TPU +/-1.82 +/-275 Cesium- 137 3690 U 0.576 3870 pCi/L 105 Uncert: +/-1.63 +1-440 TPU +/-1.60 +/-12100 Cobalt-60 5700 U 5.24 6280 pCi/L 110 Uncert +/-2.64 +/-614
| |
| +1-2.58 +1-19700 Europium-152 U -1.32 U 97.9 pCi/L Uncert +1-5.16 +1-219 TPU +1-5.06 +/-375 Europium-154 U 1.39 U -13.6 pCifL Uncert +1-4.77 +1-246 TPU +/-4.67 +1-245 Europium-lSS U 5.24 U 98.6 pCi/L Uncert: +/-6.92 +/-275 TPU: +/-6.79 +1410 Manganese-54 U -0.0592 U -50.9 pCi/L Uncert: +/-1.68 +/-98.7 TPU: +/-1.64 +/-187 Niobium-94 U -0.304 U -8.44 pCV/L Uncert +1-155 +1-89.8 129
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage hRad Charleston SC 29407 - (843) 556-81 71 - vww.gel corni QC Summarry Workorder: 116165 Page 8 or 12 Parmname NONM 'Sample Qual QC Units RPD% REC% Range Anist - Date TIme 1, .
| |
| Rad Gamma Spec Batch 346S20 IPU: 4-1.51 +1-91.9 Silver-lOSm U -0.0515 U ' -58.6 pCi/L' Uncert: 41-1.76 +/-85.8 TPU: +/-1.73 +/-202 Rad Gas Flow Batch 347780 QC12006599S4 116165001 DUP Strontium-90 U 0.689 U 1.10 pCi/L 0 (0% -100%) IIOBI 07/15/04 15:46 Uncert: +/-0.637 +/-0.729 TPU: +/-0.661 +/-0.782 QC12006599S6 LCS Strontium-90 61.2 523 pCVL 86 (75%.125%)
| |
| Uncert: +/-2.81 TPU: +1-12.4 QC1200659983 MB Strontium-90 U 0391 pCi/L 07/15104 14:08 Uncert: +/-0.657 TPU: +/.0.665 QC1200659955 116165001 MS Strontium-90 122 U 0.689 115 pCi/U 93 (75%-125%) 07/15/04 15:46 Uncert: +/10.637 ; +1-5.96 TPU: +/-0.661 +/-29.0 Batch 350139 QC1200665743 116S52001 DUP Alpha U 1.65 U 0.638 pCi/L 0 (0% - 100%) ATIII 07123104 10:17 Uncert: +/-1.09 1/-0.974 IPU: +/-1.10 +/-0.977 Beta U 0.275 U 0.454 pCi/L 0 (0%- 100%)
| |
| Uncert: +1-0.848 +/-0.908 TPU: +/-0.848 +I-0.908 QC1200665746 LCS Alpha 71.9 70.1 pCi/L 98 (75%-125%) 0723/0 10:14 Uncert: +1-8.58 TPU: . /-12.2 Beta 244 243 pCi/L 100 (75%-125%)
| |
| Uncert: *+/-10.7 TPU: .+/-11.1 QC1200665742 MB Alpha U 2.72 pCi/L 07/23/04 10:17 Uncert +/-1.59 TPU: +/-1.61 Beta U . 0.654 pCi/L Uncert: +/-1.00 IPU: +/-1.00 QC1200665744 116852001 MS Alpha 71.9 U 1.65 77.0 pCi/L 105 (75%-125%) 07/23/04 09:17 Uncert: +1-1.09 +/-8.44 TPU: +/-1.10 +/-9.75 Beta 245 U 0.275 251 pCilL 102 (75%-125%)
| |
| 130
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
| |
| ''')
| |
| QC Summary Workordcr: 116165 Page 9or 12.
| |
| Parnname NONM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gas Flow Batch 350139 Uncert +/-0.848 +/-10.7 1TPU: +/-0.848 +I-10.8 QC1200665745 116852001 MSD Alpha 71.9 U 1.65 76.1 pCi/L 1* 104 (75%-125%)
| |
| Uncert: +1-1.09 +1-8.47 TIPU: +1-1.10 +1-11.4 Beta 245 U 0.275 249 pCi/L 1* 102 (75%-125%)
| |
| Uncert: +1-0.848 +/-10.7 TPU: +1-0.848 +1-11.1 Batch 350566 QC1200666710 116165011 DUP Alpha u 0.441 U -. 474 pCi/L N/A (0% - 100%) ATIII 07t29/04 16:14 Uncert: +/-1.12 +1-0.975 TPU: +1-1.12 +1-0.975 Beta 6.53 3.64 pCitL 57 (0%- 100%)
| |
| Uncett +1-1.16 +1-0.994 TPU: +1-1.17 +/-0.994 QC1200666713 LCS Alpha 71.9 60.9 pCU/L 85 (75%-125%) 07126/04 18:52 Uncert: +/-7.61
| |
| 'TU: +1-8.54 Beta 244 245 pCiIL 100 (75%-125%)
| |
| i Uncert: +1-10.5 TPU: +1-10.7 QC1200666709 MB Alpha U -0.774 pCVL 07/27/04 14:30 Uncert: +1-0.560 TPU: +/-0.566 Beta U -0.0404 pCi/L Uncent: +/-0.676 TPU: +/-0.676 QC1200666711 116165011 MIS Alpha 71.9 U 0.441 54.9 pCiIL 76 (75%-125%) 07/30104 18:59 Uncert: +/-1.12 +1-8A41 1TPU: +/-1.12 +1-9.69 Beta 245 6.53 253 pCiIL 101 (75%-125%)
| |
| Uncert: +/-1.16 +1-10.6 TPU: +/-1.17 +/-10.7 QC1200666712 116165011 MSD Alpha 71.9 U 0.441 62.0 pCi/L 12* 86 (75%-125%) 07/26/04 18:52 Uncett +1-1.12 +/-9.32 TPU: +1-1.12 +/-11.4 Beta 245 6.53 269 pCi/L 6* 107 (75%-125%)
| |
| Uncett +/-1.16 +/-1 1.0 TPU: +1-1.17 +1-11.3 Rad Uquld ScIntflation Batch 347077 QC120065S273 115S40001 DUP 131
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| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 116165 Page loor 12 Parmname NONI Sample Qual OC Units RPD% *REC% Range Anlst Date Time Rad Llquid Scintfllation Batch 347077 Carbon-14 U 0.0761 U OA61 pCilL 0 (0%- 100%) PD 07/10/0400:45 Uncert: +/-324 +1-3.42 TPU:1 +/-3.24 +1-3.42 QC1200658275 LCS Carbon-14 202 201 pCi/L 100 (75%-125%) 07/10/04 03:15 Uncert: +/-5.73 TPU +/-8.58 QC1200658272 MB Carbon-14 U -2.14 pCi/L 07/09/04 23:12 Uncert +1-332 TPU : +1-332 QC1200658274 115S40001 MS Carbon-14 202 U 0.0761 212 pCi/L 105 (75%-125%) - 07/10/04 01:59 Uncert: +1-3.24 +1-5.96 TPUU * +/-3.24 +t-8.99 Batch 34SS13 QC12006624S6 116165014 DUP Technetium-99 U 4.26 U -2.09 pCi/L N/A (0% - 100%) DA1 07/25/C 23:28 Uncert: +/4.70 +/4.65 TPU +/4.70 +/4.65 QC120066248S LcCS
| |
| ..echnetium-99 470 491 pCi/L 104 (75%-125%) 07/26/04 00:33 Uncert: +/-13.7 TPU: +/-17.7 QC1200662485 MB Technetium-99 U -0.445 pCi/L 07/25/04 22:56 Uncert: +1495 TPU +1/495 QC12006624S7 116165014 MS Technetium-99 470 U 4.26 493 pCi/L 105 (75%-125%) 0761o04 00:00 Uncert: +/4.70 +/-16.2 TPU: +/-4.70 +/-19.7 Batch 348827 QC1200662539 116165001 DUP Tritium 1010 789 pCiL' 24 (0% - 100%) JLB I 07120/04 15:58 Uncert +/-220 +/-171 Ti'U +/-220 +/-172 QC1200662541 LCS Tritium 3220 2820 88 (75%-125%) 07/20/04 18:05 Uncert: +/-238
| |
| 'PU:
| |
| T 4+-242 .pCi/L QC1200662533 MB Tritium U - -97.5. 0729/0402:50 Uncert: +/-205 TPU +/-205 QC1200662540 116165001 MS Tritium 3230 1010 3500 pCiIL 77 (75%-125%)- 07120/04 17.02 Uncert: +/-220 +/-261 TPU +/-220 +/-267 132
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| | |
| 11-GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder 116165 Page IIof 12 Parnname NOINI Sample Qual QC Units RPD% REC% Range Anist Date Tlme Rad Uquld Scintillatlon Batch 349214 QCt200663437 116165014 DUP Iron-55 U 6.19 U 2.27 pCitL 0 (0% - 100%) JLBI 07/22104 02:35 Uncert +1-12.9 +1-11.3 TPU: +1-12.9 +1-1,13 QC12006634S9 LCS Iron-55 56.3 47.6 pCt/L 84* (0%-%) 0722t04 04:40 Uncert +/-12.5 TPU: +/-12.7 QC12006634S6 MB Iron-55 U 3.35 pCi/L 07122/04 01:32 Uncert: +/-12.0 TPU: 4.12.0 QC12006634SS 116165014 MS Iron-55 57.1 U 6.19 55.4 pCb'L 86* (0%-%) 07129/04 08:39 Uncert: +1-12.9 +1-12.7 lPU: +1.12.9 +1-12.9 Batch 345n216 QC1200663495 116165014 DUP Nickel-63 U 4.97 U -6.43 pCitL NIA (0%-100%) JLBI 07121/0414:18 Uncert: +1-7.69 +1-7.78 TPU: +1-7.69 +t-7.78
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| * QC1200663497 LCS Nickel-63 261 310 pCi/L 119 (75%-125%) 07121/04 15:21 Uncert: +1-13.6 TPU: +1-17.3 QC1200663494 NIB Nickel-63 U 0.213 pCi/L 07/21/04 13:47 Uncert: +/-7.06 TPU: +1-7.06 QC1200663496 116165014 MS Nickel-63 261 U -4.97 288 pCi/L 110 (75%-125%) 07/21/04 14:50 Unceit +1-7.69 +/-13.1 TPU: +1-7.69 +/-16.5 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
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| BD nlag for results below the MDC or a flag for low tracer recovery.
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| E Concentradon of the target analyte exceeds the instrument calibration range.
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| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
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| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
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| h Sample preparation or preservation holding ti me exceeded.
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| 133
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 --.www.gel.com I QC Summary.
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| Workorder: 116165 Page 12 or 12 Parrname NONI Sample Qual QC Units RPD% REC% Range AnIst Date Time N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.
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| ** Indicates analyte is a surrogate compound.
| |
| A^lTe Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than SX the RL, a control limit of t/- the RL is used to evaluate the DUP result.
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| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
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| 134
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| GENERAL ENGINEERING LABORATORIES, LLC 0 a Member of THE GEL GROUP, INC.
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| U Meeting Today's Needs with a Vision for Tomorrow 0it~1 o1>Xt August 05, 2004 Mr. Dave Keefer CYAPCo Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 RE: Quarterly Groundwater PO# 002337 Work Order: 116418 SDG: MSR#04-2114
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| ==Dear Mr. Keefer:==
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| | |
| General Engineering Laboratories, LLC (GEL) appreciates the opportunity to provide the following analytical results for the sample(s) we received on July 08, 2004. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time.
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| This data report has been prepared and reviewed in accordance with GEL's standard operating procedures. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4475.
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| Sincerely, Sarah Kozl Project Manager Purchase Order: 002337 Chain of Custody: 2004-00126 Enclosures RO. Box 30712 - Charleston, SC 29417
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| * 2040 Savage Road (29407)
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| Phone (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com
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| | |
| CONNE CTICUT YANKEE RE: Quarterly Groundwvater
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| ... . PO# 002337.
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| Work Order:.116418 :
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| SDG: MSR#04-2114 116418001 AMW2-0204-001 116418002 AIBI117S-0204-001 116418003 AMN102D-0204-001
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| Table of Contents Case Narrative .......................................................... 1 Chain of Custody ........................................................ 4 Cooler Receipt Checklist ......................... ..... . ..
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| *.. 7 Inorganic Analysis .................. me"I............a.......... ........ 9 Radiological Analysis .......................... s... 17 Sample Data Summary ............................................. 24 Quality Control Data ............................................. 31
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| C CASE NARRATIVE
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| -1
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| I -0 CASE NARRATIVE For CONNECTICUT YANKEE RE: Quarterly Groundwater 0
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| PO# 002337 Work Order: 116418 SDG: NISR#04-2114 August 5, 2004 Laboratory Identification:
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| General Engineering Laboratories, LLC Mailing Address:
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| P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:
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| 2040 Savage Road Charleston, South Carolina 29407 Telephone Number:
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| (843) 556-8171 Summary:
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| Sample receipt The samples for the Quarterly Groundwater Project for work order 116418 arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina July 8, 2004 for environmental analysis. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.
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| The laboratory received the following groundwater samples:
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| MW2-0204-001 MWI 17S-0204-001 MW102D-0204-001.
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| GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
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| RO. Box 30712
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| * Charleston, SC 29417
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| * 2040 Savage Road (29407)
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| Phone (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com
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| | |
| Items of Note:
| |
| There are no items to note.
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| Case Narrative:
| |
| Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.
| |
| Analytical Reauest:
| |
| Two groundwater samples were analyzed for MI and one was analyzed for STND.
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| Internal Chain of Custodv:
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| Custody was maintained for all of these samples.'
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| Data Package:
| |
| The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Laboratory Certifications, and Radiochemistry.
| |
| I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.
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| GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
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| P.O. Box 30712
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| * Charleston, SC 29417 - 2040 Savage Road (29407)
| |
| Phone (843) 556-8171
| |
| * Fax (843) 766-1178
| |
| * www.gel.com
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| .3
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| CHAIN OF CUSTODY
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| .\
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| Health Physics Procedure
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| ( GPP-GGGR-R51 04-003-Attachmnent B-CY-U0 1 Major C
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| Chan-f CstdyForm C6 ecnti-cUt Yankee Atomic PowerCompany . . C No. 2004-00126
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| *362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 -
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| ProjectName: HaddamNeckDecommissioning lnalysesRequested Lab Contact Name & Phone: Media Spe Conta..er.. .. '
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| Rich McGrath 860-267-3573- Media Sample Container .-
| |
| _ __ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Code Type Size- .,
| |
| Analytical Lab (Name, City, State): Code &Type . .
| |
| General Engineering Lab (GEL), 2040 Savage Rd,. Code, Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) _ . -, ,,
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| Priority:El45 D.E3ob.E 14D.EJ7D. . .
| |
| Other: ; i; !'-'!_A.F ;*..s; Sample Designation Date Time -amp.elD- Comment, Preservation La MA N -cO%- 7..-SIO .WG. G 4L,.1L - .- - __
| |
| MW I 19I- opoq-oa( I,a5-5 WG G 4L, IL Ž5 - -
| |
| .... _ - WG. .G 4Lj1L __. _,r_____;__
| |
| _________ WG. G. .4L, 1L . . _ ...
| |
| .__. WG .G 4L,1L L_. . . .
| |
| NOTES: PO #: 002337 MSR #:. O4-+7- . LTP QA M Radwaste QA ZNon QA Samples Shipped Via: l al yFed Ex Tem"" eg; C LiUPS Requested analyses should be peifdrmed to typical groundwater program MDC's. ! Hand Custo Sealed? :
| |
| 1)Relin he Date/Time 2) Receid Date/Time - Custody;Seal Intact c-yfi'~f4~jt. 1 4 ~y j338 7...$3/P /D L Other -
| |
| 3)Relinquishedy - Date/Time 4) Received By Date/Time ______________- N
| |
| - .,Bill of Lading #
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| : 5) Relinquished By Date/Time 6) Received By Date/Time .
| |
| | |
| Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00122 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 //6 __ _ _
| |
| Project Name: Haddam Neck Decommissioning Analyses Requested Lb Use Only -'
| |
| Contact Name & Phone: :2.i :r!'
| |
| Rich McGrath 860-267-3573 Media Sample Container Code Type Size-.....
| |
| Analytical Lab (Name, City, State): Code &Type . 4, ".- -.-
| |
| General Engineering Lab (GEL), 2040 Savage Rd, Cod .... _; .. ..
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) . 2 Priority:L 45 D.E 30 D. E] 14 D. 7 D. .
| |
| O ther: :__:_______T -_________,
| |
| Sample Designation Date Time Comment, Preservation :.Lab Sample ID.
| |
| mML ohD-oaog-oo) -,-4-ot1 o9go WG G 4L L WG G 4L, 1L
| |
| .___ _ WG G 4L,1L . .I WG G 4L,1LL__________
| |
| WG G 4L,1L L__________
| |
| NOTES: P0O# 002337 MSR # 04-4 8O:7 LILT QA I Radwaste QA Non QA Samples Shipped Via: PInt~ernal.Container ,v Fed Ex Tep4 e .C ElIUPS Requested analyses should be performed to typical groundwater program MDC's. El Hand ',-Custody Seale?-"
| |
| 1~cdB:Date/Time q 2) Receijv]"Byft-Date/Timte CsoySanat
| |
| .L Li 13 D El -~ 'Other
| |
| : 3) Relinquished By -Date/Time 4) Received By Date/Time ________Y N Bill of Lading#
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time -~4 Q
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| C. I. I .
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| | |
| COOLER
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| -RECEIPT CHECKLIST 7
| |
| | |
| -onnecticut Yankee . .
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| . I. .
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| Statement of Work for Analytical Lab Services CY-ISC-SOW-001
| |
| . I Figure 1. Sample Check-in List Date/Time Received: 7-i VK (1o V SDG#: - )J Work Order Number: u\ (Ao 9 Shipping Container ID: 74A4 79iq1 O ajfyjt
| |
| % Chain of Custody # K- ',oI.J <t yd
| |
| '1. Custody Seals on shipping container intact? Yes 1 No [ AJIV -
| |
| : 2. Custody Seals dated and signed? Yes [] No [..
| |
| : 3. Chain-of-Custody record present? Yes I~o []
| |
| . 4. Cooler temperature Yi* et / IJ .
| |
| : 5. Vermniculite/packing materials is: Wet [ ] Dry
| |
| : 6. Number of samples in shipping container ___
| |
| : 7. Sample holding times exceeded? Yes [ ] No
| |
| : 8. Samples have:
| |
| .tape ___hazard labels K) custody seals appropriate sample labels
| |
| : 9. Samples are:
| |
| _____n good condition leaking broken . ____have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [No <
| |
| : 11. Description of anomalies (include sample numbers):
| |
| Sample Custodian/Labora toriaoAroILy le" ---- Date: 7--Y ' '.
| |
| Telephoned to: On RVJ-
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| | |
| INORGANIC ANALYSIS
| |
| : 9. ,
| |
| | |
| Metals Fractional Narrative Connecticut Yankee Atomic Power Co. (YANK)
| |
| SDG MISR#04-2114 Mcthod/Analvsis Information Analytical Batch: 348554 Prep Batch: 348553 Standard Operating Procedures: GL-MA-E-014 REV# 9, GL-MA-E-006 REV# 9 Analytical Method: SW846 6020 Prep Method: SW846 3005A Sample Analysis Sample ID Client ID 116418001 MW2-0204-001 116418002 MWI 17S-0204-001 116418003 MW102D-0204-001 1200661879 Method Blank (MB) 1200661880 Laboratory Control Sample (LCS) 1200661883 116418001 (MW2-0204-00 L) Serial Dilution (SD) 1200661881 116418001(MW2-0204-001D) Sample Duplicate (DUP) 1200661882 116418001(MW2-0204-001S) Matrix Spike (MS)
| |
| Preparation/Analytical Method Verification The SOP stated above has been prepared based on technical research and testing conducted by General Engineering Laboratories, LLC. and with guidance from ihe regulatory documents listed in this "Method/Analysis Information" section.
| |
| System Confituration The ICP-MS analysis was performed on a Perkin Elmer Elan 6100E inductively coupled plasma mass spectrometer (ICP-MS). The instrument is equipped with a cross-flow nebulizer, quadrupole mass spectrometer, and dual mode electron multiplier detector. Internal standards of scandium, germanium, indium, and tantalum were utilized to cover the mass spectrum. Operating conditions are set at 1400W power and combined argon pressures of 360+/-7 kPa for the plasma and auxiliary gases, and 0.85 Lrmin carrier gas flow, and an initial lens voltage of 5.2.
| |
| 10
| |
| | |
| 7~ :1 Calibration Information Instrument Calibration All initial calibration requirements have been met for this sample delivery group (SDG).
| |
| CRDL Requirements All CRDL standard(s) met the referenced advisory control limits.
| |
| ICSAIICSAB statement All interference check samples (ICSA and ICSAB) associated with this SDG met the established acceptance criteria.
| |
| Continuing Calibration Blank (CCB) Requirements All continuing calibration blanks (CCB) bracketing this batch met the established acceptance criteria.
| |
| Continuing Calibration Verification (CCV) Requirements All continuing calibration verifications (CCV) bracketing this SDG met the acceptance criteria.
| |
| Quality Control (OC) Information Method Blank (MB) Statement The MB analyzed with this SDG met the acceptance criteria.
| |
| Laboratory Control Sample (LCS) Recovery The LCS spike recoveries met the acceptance limits.
| |
| Quality Control (QC) Sample Statement -
| |
| Sample 116418001 (MW2-0204-001) was selected as the quality control (QC) sample for this SDG.
| |
| Matrix Spike (MS) Recovery Statement The percent recoveries (%R) obtained from the MS analyses are evaluated when the sample concentration is less than four times (4X) the spike concentration added. All applicable elements met the acceptance criteria.
| |
| Duplicate Relative Percent Difference (RPD) Statement The RPD obtained from the designated sample duplicate (DUP) is evaluated based on acceptance criteria of 20%
| |
| when the sample is 5X the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control of +/-RL is used to evaluate the DUP results. All applicable analytes met these requirements.
| |
| Serial Dilution % Difference Statement The serial dilution is used to assess matrix suppression or enhancement. Raw element concentrations that are 25X the IDL for CVAA, 50X the IDL for ICP, and 1OOX the IDL for ICP-MS analyses are applicable for serial dilution assessment. All applicable analytes met the acceptance criteria of less than 10% difference (%D).
| |
| Technical Information Holding Time Specifications GEL assigns holding times based on the associated methodology, which assigns the date and time from sample collection of sample receipt. Those holding times expressed in hours are calculated in the AlphaLIMS system. Those holding times expressed as days expire at midnight on the day of expiration. All samples in this SDG met the specified holding time.
| |
| Preparation/Analytical Method Verification All procedures were performed as stated in the SOP.
| |
| Sample Dilutions Dilutions are performed to minimize matrix interferences resulting from elevated mineral element concentrations 11
| |
| | |
| present in soil samples and/or to bring over range target analyte concentrations into the linear calibration range of the instrument. The samples in this SDG did not require dilutions.
| |
| Preparation Information The samples in this SDG were prepared exactly according to the cited SOP.
| |
| Miscellaneous Information Nonconformance Documentation Nonconformance reports (NCRs) are generated to document procedural anomalies that may deviate from referenced SOP or contractual documents. A NCR was not required for this SDG.
| |
| Additional Comments Additional comments were not required for this SDG.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| The following data validator verified the information presented in this case narrative:
| |
| Reviewerd Z,<a , 4 4 Date: - 5i .
| |
| 12
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 2,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwter PO# 002337 Page 1 of I Client Sample ID: MW2-0204-001 Proiect: YANK00304 Sample ID: 116418001 Client ID: YANK001 Matrix: Ground Water Collect Date: 01-JUL,04 12:50 Receive Date: 08-JUL-04 Collector client -
| |
| Parameter Qualifier Result DL 1RL Units DF AnalystDate Time Batch Method Metals Analvsis-1CP-MS . I 3005/6020 Boron-A LSTNDAflX Boron J 15.5 0.540 16.0 ug/L I BAJ 07122/04 0952 348554 1 The following Prep Mlettiods were performed XteIMI- fcslrnton. Ans-1.j Dat 7ime Prc Btnclh SW8463005A ICP-MS 3005 PREP CQHI 07/15/04 1717 348553
| |
| ,The followying Analytical Methods were performed Method Description Analyst Comments SW846 300516020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| BI Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| * Analytical holding time exceeded. .
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summnary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received" basis.
| |
| W~here the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Plea-e direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by r 13
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Hladdam Neck Plant 362 Injun Hollow Road East Hampton. Connecticut 06424 Report Date: August 2, 2004 Contact Mr. Dave Kecrer Project Quarterly Groundwater PON 002337 Page I of I Client Sample ID: MWI 17S-0204-001 Proiect: YANK003O4 Sample ID: 116418002 Client ID: YANK001 Matrix: Ground Water Collect Date: 01-JUL-04 12:56 Receive Date: 08-JUL-04 Collector Client Parameter Qualifier Result DL RL Units DF AnalystDate Time Batcd Method Metals Analysis-ICP-NIS 3005/6020 Boron-ALSTND,/JX Boron 68.5 0540 16.0 ug/L I BAJ 07/22/04 1003 348554 1 The follouing Prep Methods were performed Method Description Analyst Date Time Prep Batch SW846 3005A lCP-MS 3005 PREP CQHI 07115/04 1717 348553 The following Analytical Methods were performed Method Description Analyst Comments I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a nag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by (/
| |
| 14
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: lladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 2,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 1 of I Client Sample ID: MWI02D-0204-001 Proiect: YANK00304 Sample ID: 116418003 Client ID: YANKOO0 Matrix: Ground Water Collect Date: 06-JUL-04 09:20 Receive Date: rSimtin Collector: ClIi ent Parameter Qualifier Result DL RL Units DF AnalystDate Time Batch Method Metals Analysis-ICP-MS 3005/6020Boron-ALLSTNDMIX Boron 97.1 0.540 16.0 ugfL I BAJ 07/22/04 1006 348554 -1 The rollowing Prep Methods were performed Method Description Analyst Date Time Prep Batch SW8463005A ICP-MS 3005 PREP CQHI 07/15/04 1717 348553 The following Analytical Methods were perfonned Method Description Analyst Commcnts I SW846 3005/6020 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limiL UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| 1Reviewed by "
| |
| 15
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www-gel.com QC Summary Renort Date: August 2,2004 Client: CYAPCo Page I of I Haddam Neck Plant 362 Injun Hlollowv Road East Hampton, Connecticut
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Workorder: 116418 Pannname NOM Sample Oual OC Units RPD% REC% Ranre Anist Date Time Metals Analysis - ICPMS Batch 348554 QC1200661881 116418001 DUP Boron 1 15.5 J 14.0 ug/L 10 A (+1-16.0) BAJ 07/22/04 09:55 QC12006618S0 LCS Boron 100 114 ug/L 114 (80%-120%) 07122/04 09:50 QC1200661879 MB Boron U ND ug/L 07122/04 09:47 QC1200661892 116418001 MS Boron 100 J 15.5 131 ugIL 115 (75%-125%) 07122/04 09:58 QC1200661S83 11641S001 SDILT Boron I 15.5 J 221 ugIL 28.9 07/22/04 10:00 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| II Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limiL U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone, by a factor of 4 or more.
| |
| A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than SX the RL, a control limit of +/-
| |
| the RL is used to evaluate the DUP result.
| |
| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
| |
| NVhere the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
| |
| 16
| |
| | |
| RADIOLOGICAL .
| |
| ANALYSIS -
| |
| 17'
| |
| | |
| Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)
| |
| SDG MlSRIY04-21 14 Method/Analysis Information Product: Gammaspec, GammaLiquid-ALL,GsAM2,STNDMIX,PENN,LF Analytical Method: EPA 901.1 Analytical Batch Number 349017 Sample ID Client ID 116418001 MW2-0204-001 116418002 MW1I7S-0204-001 116418003 MWI02D-0204-001 1200663002 Method Blank (MB) 1200663005 Laboratory Control Sample (LCS) 1200663003 116418001(MW2-0204-001) Sample Duplicate (DUP) 1200663004 116418001 (MW2-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116418001 (MWV2-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-preplRe-analysis 18
| |
| | |
| None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Method/Analvsis Information Product: Gross A/B, liquid-ALLSTND,MIIX,PENN,LF Analytical Method: EPA 900.0 Analytical Batch Number. 350569 Sample ID Client ID 116418001 MW2-0204-001 116418002 MW1I7S-0204-001 116418003 MW102D-0204-001 1200666718 Method Blank (MB) 1200666722 Laboratory Control Sample (LCS) 1200666719 116418002(MWI17S-0204-00l) Sample Duplicate (DUP) 1200666720 116418002(MW1I7S-0204-001) Matrix Spike (MS) 1200666721 116418002(MW1 17S-0204-001) Matrix Spike Duplicate (MSD)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-001 REV# 8.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (0C) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used forQC: 116418002 (MWI17S-0204-001). -- -
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| 19
| |
| | |
| I Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Gross Alpha/Beta Preparation Information High hygroscopic salt content in evaporated samples can cause the sample mass to fluctuate due to moisture absorption. To minimize this interference, the salts are converted to oxides by heating the sample under a flame until a dull red color is obtained. The conversion to oxides stabilizes the sample weight and ensures that proper alpha/beta efficiencies are assigned for each sample. Volatile radioisotopes of carbon, hydrogen, technetium, polonium and cesium may be lost during sample heating.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Ounlifier information Manual qualifiers were not required.
| |
| Method/Analysis Information Product: GFPC, Sr9O, liquid-ALL,NIIX Analytical Method: EPA 905.0 Modified Analytical Batch Number: 348452 Sample ID Client ID 116418001 MIW2-0204-001 116418002 MW 17S-0204-001 116418003 MWI02D-0204-001 1200661600 Method Blank (MB) 1200661603 Laboratory Control Sample (LCS) 1200661601 116418001 (MW2-0204-001) Sample Duplicate (DUP) 1200661602 116418001 (MW2-0204-00 1) Matrix Spike (MS)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 8.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information 20
| |
| | |
| Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry I All counting sources were prepared in the same geometry as the calibration standards.
| |
| Ouality Control (0C0 Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116418001 (MW2-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.
| |
| Miscellaneous Information:
| |
| NCR Documentation' Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Otialifier information Manual qualifiers were not required.
| |
| Miethod/Analysis Information Product: LSC, Tritium Dist, Liquid-ALL,STNDAIXPENN Analytical Method: ,EPA 906.0 Modified l Analytical Batch Number: 350326 Sample ID Client ID 116418001 MW2-0204-001 116418002 MWI 17S-0204-001 116418003 MW 102D-0204-001 1200666133 Method Blank (MB) -
| |
| 1200666136 Laboratory Control Sample (LCS).
| |
| 1200666134 *116418001(MW2-0204-0I) Sample Duplicate (DUP) 1200666135 I16418001(MW2-0204-001) Matrix Spike (MS)
| |
| SOP Reference 21.
| |
| | |
| Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 9.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Onality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 116418001 (MW2-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prep/Re-analysis Sample 116418001 (MW2-0204-001) was recounted due to high relative percent difference/relative error ratio.
| |
| Samples 116418001 (MW2-0204-001), 116418002 (MWI 17S-0204-001), 1200666133 (MB) and 1200666134 (MW2-0204-001) were recounted due to high lumex and low quench numbers.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR wvas not generated for this SDG.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| 22
| |
| | |
| The following data validator verified the information presented in this case narrative:
| |
| a I 60-teW k - Q~j UOcx ,FS i WIA Reviewer:
| |
| 23
| |
| | |
| I S-a SAMPLE DATA
| |
| | |
| ==SUMMARY==
| |
| | |
| 24
| |
| | |
| LLC - - - -
| |
| LABORATORIES, GENERAL ENGINEERING GENERAL ENGINEERING LABORATORIES,- LLC 2040 Savago Road Charleston SC 29407 - (843) 5568171 - www.gel.com Certificate of Analysis :
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton. Connecticut 06424
| |
| * Report Date: . August 6.2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample lD: . MW2-0204-001 Proiect: YANK00304 SampleID: ; 116418001 ClientlD: YANKO0l Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 01-JU1L04 Receive Date: 08-JUL-04 Collector: Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Tlime Batch Mtd.
| |
| flU GammaL OJeC AORMIs Gammaspec, GammaUquid-AlL,GAM2f.SND.M1XPENN,LF Americium-241 U -2.02 +/-9.69 8.21 +/-9.SD, 173 PCV'L MJ1H1 0810UD4 1006 349017 1 Cesium-134 U 0.129 +1-1.89 1.57 +/-1.85 3.52 pci/L Cesium-137 U 0.322 +/-1.88 1.60 +/-1.85 3.51 pCi/L Cobalt-60 U 1.08 +/-3.74 1.62 +t-3.67 3.73 Europium-152 U 3.88 +1-5.35 4.58 +4-5.24 9.78 pCiIL Europium-154 U 1.60 +/4.82 4.13 +/-4.72 9.56 PCVL Europium-155 U -1.68 +/-6.80 5.66 +1-6.66 119 pCVL
| |
| \ Manganese-54 U -0.154 +1-1.92 1.56 44-1.88 3.47 PCVL Niobium-94 U 1.33 * +1-1.66 1.50 +/-1.62 3.28 pCi1L Silver-108m U 0.666 +/-1.61 135 +1-1.58 2.93 PCVL Rad Gas Flow Proportional Counting GFPC Sr90, liquid-ALLMKX Strontium-90 . U -0.131 +1-0.374 0.450 +1-0.376 1.02 PCVL HOD] 07/17104 1654 3484522 GrossAI, liquid-AL.STNDMMXPENN.LF Alpha U 0.416 +1-0.660 0.544 +/-0.661 1.29 pCi/L ATHI 07128/04 1834 350569 3 Beta 4.43 +/-1.43 1.17 +/-1.43 2.46 pCVL Rad LIquid Scintillation Analysis LSC, Titium Dist, UquId-AL.STNDAflXPENN Tritium U -251 .+/-229 199 +/-229 397 pCi/L ILJ31 08/0204 1940 350326 4 j he following Prep Methods were performed -
| |
| Method Descripion Analyst Date - -----Time PrepBatch i
| |
| SW846 3005A ICP-MS 3005 PREP CQi l 07/15/04 1717 348553 The following Analytical Methods were performed ___
| |
| Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified 25:
| |
| | |
| LLC LABORATORIES, GENERAL ENGINEERING GENERAL ENGINEERING. LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 -www.gel.com Certificate of Analysis, Company: CYAPCo Address: iiaddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 6,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater P0# 002337 Page 2 of 2 Client Sample ID: MW2-0204-001 Proiect: YANK00304 Sample ID: 116418001 Client iD: YANKOOI Vol. Recv.:
| |
| Parameter Qualifier Result Uncertalnty LC TPU NIDA Units DF AnalystDate Time Batch Mtd.
| |
| SurrgateiTracer recovery Test Recovery% Acceptable Limits CarrierlTracer Recovery GFPC, S;r9o, liquid-ALL,MKC 74
| |
| : Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyto exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain idendfication for gamma spectroscopy. '' ,.
| |
| X Lab-specific qualifier-please sec case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlilc Reviewed by 26
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage R6ad Charleston SC 29407- (843) 556-8171 -'www.gel.com Certificate of Analv'is.
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hamipton, Connecticut 06424 Report Date: August 6,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of 2 Client Sample ID: MWI 17S-0204-001 Prpiect: YANK003D4 Sample ID: 116418002 .PClient ID: YANK001 Matrix: Ground Water Vol. Remy.:
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| Collect Date: 01-JUL-04 Receive Date: 08-JUL-04 Collector. Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
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| Rad Gamnma Spec Analysis Gammaspec. GammaCLquid-ALL, GAM2,STNDM1X PENN,LF
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| * Americium-241 U -2.76 +1-18.3 13.1 .1-17.9 275 pCi'L MJHI 08104/04 1007 349017 1 Cesium-134 U 0.0363 +1-1.96 1.57 .1-1.92 . 3.54 IpcV/L
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| * Cesium-137 U -0372 +1-2.37 1.87 .1-2.32 4.08 pCiIL .
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| Cobalt-60 U 2.12 +1-2.22 2.10 ./-2.17 4.71 pCV/L Europium-152 U -0.0575 +1-6.31 524 41-6.18 112 pCil/L Europium-154 U 2.22 +1-5.70 - 5.01 41/-.559 11.4 PaliL Europiumi-155 U -2.22 +1-9.14 7.25 *1-8.95 15.1 pCi/L --
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| _jMinganese-54 U -1.04 +1-2.18 1.73 ,+1-2.14- 3.83 pCi'll I Niobium-94 U 1.22 +/-1.93 1.67 +1-1.90 3.64 pCU/L Silver-108m U -0.686 +/-2.03 139 +/-1.99 3.04 pCaiL Rad Gas Flow Proportional Counting GFPC, Sr90, liquid-ALI,MIX Strontium-90 U 0.791 +1.0.516 0.421 +/-0563 0.952 PCU/L BOBI 07/17/04 1654 348452 2 GrossAB. liquid-ALL.STNDf1XPEJNLF Alpha U 0.410 +1-0.S37 0.654 +1-0.83S 1.44 pCULL ATH I 07(29/D4 04-48 350569 3 Beta 7.28 +1-1.55 1.12 +/-1.57 230 pCi/L Rad Liquid Scintillatlon Analysis LSC, Tritium Dist, LJquid-ALLSTND.M1X, PENN Tritium U 25.1 4/-194 162 +/-194 324 pCiL JLB1 0713C0D4 2258 3503264 The following Prep Methods were performed Metbod Description Analyst Date Time Prep Batch SW846 3005A ICP-MS 3005 PREP CQHI 07/15104 1717 348553 The following Analytical Methods were'performed Method Description I EPA901.1 2 EPA 905.0 Modificd 3 EPA 900.0 4 EPA 906.0 Modified Surrogate/Iracer recovery Test .Recovery% Acceptable Lhnits
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| : 27. .
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com
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| <i Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road Fast Hampton. Connecticut 06424 Report Date: August 6,2004 Contact Mr. Dave Keefer Project Quarterly Groundwater PO# 002337 Page 2 of 2 Client Sarnple ID. MWI 17S-0204-001 Project: YANK00304 Sarnple ID: 116418002 C.icenttD: YANKO0I Vol. Recm:
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| Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
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| Carrierfrracer Recovery GFPC. Sr90. liquid-ALL.MIX 78 Notes:
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| The Qualifiers in this report are defined as follows:
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| B Target analyte was detected in the sample as well as the associated blank.
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| BD Flag for results below the MDC or a flag for low tracer recovery.
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| E Concentration of the target analyte exceeds the instrument calibration range.
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| H Analytical holding time exceeded.
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| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
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| U Indicates the target analyte was analyzed for but not detected above the detection limit.
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| Ul Uncertain identification for gamma spectroscopy.
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| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
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| h Sample preparation or preservation holding time exceeded. '-\f)
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| The above sample is reported on an "as received basis.
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| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
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| Reviewed by 28
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| I GEEA ENINERN LAOATRESL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 -www.gol.com Certiflcate of Analysis Company: CYAPCo Address: Haddam Neck Plant
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| .362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 6,2004
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| ==Contact:==
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| Mr. Dave Keefer Project: Quarterly Groundwater POO 002337 Page I of 2 Client Samnpic ID: MW102D-0204-001 Proiect: YANK00304 Saunple ID: 116418003 Client ID: YANKOOI Matnx: Ground Water Vol. Recv.:
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| Collect Date: 06-JUL-04 Receive Date: 08-JUL-04 Collector Client Parametcr Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mid.
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| Rad Gamma Spec Analysis Gammaspec, GammaLiquid-ALLGAM2,5TNDMIXPENN,LF Arnericium-241 U 0.708 +1-12.1 9.09 +1-11.9 .19.0 pCUfL MJHI 08/04104 1007 3490171 Cesium-134 U 0.438 +1-1.68 1.44 +/-1.65 320 pCl/L Cesium-137 U 0.235 +/-1.86 1.57 +/-1.82 3.43 pc/LL Cobalt-60 U 1.52 +1-1.84 1.72 +1-1.81 3.87 pci/L Europium-152 U -7.03 +1-5.61 4.15 41-5.50 8.87 pC/LL Europium-154 U -1A1 +J-559 4.48 +1-5.48 10.1 pc/LL Europium-15S U 3.25 +1-7.77 6.46 +t-7.61 13.4 pC/L '
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| < Manganese-54 U 0.678 +1-1.93 1.65 +/-1.89 3.60 pCV/L Niobium-94 U 1A0 +1-1.64 1.48 +1-1.61 3.21 pCV/L Silver-108m U 0.0407 +1-1.84 150 +/-1.80 3.21 pCi/L.
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| Rad Gas Flow Proportional Counting GFPC.Sr90, liquid-AMLMIX Strontium-90 U 0.928 44-0.580 0.484 +/-0.641 1.08 pCUL HOB I 0`7/17/04 1654 34452 2 GrossAI, I1quid-ALLSTND.MIXPENNLF AlIrsh. R 41177 n72n 41-l R7 I 44 pCVfL ATH I 07(2804 1834 350569 3 Beta 9.95 +/-1.72 1.18 +/-1.75 2A8 pCi/L
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| * Rad Lquid Scintlliation Analysis LSC, Tritium Dist, Uquid-ALLSTNDMlXPENN Tritium 4690 +t-253 114 +1-264 229 pCV1L JLD1 0r7/30/04 1440 350326 4 T. e foUowing Prep Methods were performed Method Description Analyst Date Time Prep Batch SW8463005A ICP-MS 3005 PREP CQHI 07/15/04 1717 348553 The following Analytical Methods were performed Method Description I EPA 901.1 2 EPA 905.0 Modified 3 EPA 900.0 4 EPA 906.0 Modified Surrogate/Tracer recovery Test Recovery% Acceptable Lmits 29
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 6, 2004
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| ==Contact:==
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| Mr. Dave Keefer Project: Quarterly Groundwater PO* 002337 Page 2 of 2 Client Sample ID: MWI02D-0204-001. Proiect YANK003O4 Sample ID: 116418003 Citent ID: YANK00 Vol. Recy.:
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| Parameter Quaimfier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
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| Carricr/Tracer Recovery GFPC, Sr9O. liquid-ALLMIX 75 Notes:
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| The Qualifiers in this report are defined as follows:
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| B Target analyte was detected in the sample as well as the associated blank.
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| BD Flag for results below the MDC or a flag for low tracer recovery.
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| E Concentration of the target analyte exceeds the instrument calibration range.
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| 11 Analytical holding time exceeded.
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| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
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| U Indicates the target analyte was analyzed for but not detected above the detection limit.
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| Ul Uncertain identification for gamma spectroscopy.
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| X Lab-specific qualificr-please see case narrative, data summary package or contact your project manager for details.
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| h Sample preparation or preservation holding time exceeded.
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| The above sample is reported on an 'as received basis.
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| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
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| /tR CLal4'3.W CU Reviewed by 30
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| I:I..
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| QUALITY CONTROL DATA.
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| 31
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: August 6t 2004 Client: CYAPCo Page 1 of 5 Iladdam Neck lPlant 362 Injun Hollow Road East lampton, Connecticut
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| ==Contact:==
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| Mr. Dave Keefer
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| *Workorder: 11641S Parmname NOM Sample Qual QC Units RPD% REC% Range AnIst Date Mme Rad Ganma Spec Batch 349017 QC1200663003 116418001 DUP Americium-24 1 U -2.02 U -11.9 pCi/L N/A (0% - 100%) MJ1l 08/04/04 23:01 Uncert +/-9.69 +/-14.3 TPU: +/-950 +/-14.0 Cesium-134 U 0.129 U -1.66 pCi/l N/A (0% - 100%)
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| Uncenr +t-1.89 +/-1.89 TPU: +1-1.85 +/-1.85 Cesium-137 U 0.322 U 1.64 pCi/L 134 (0% - 100%)
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| Uncert: +/-1.88 +/-1.65 TPU: +/-1.85 +/- 1.62 Cobalt-60 U 1.08 U -0.265 pCiL N/A (0% - 100%)
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| Uncert: +/-3.74 +1-157 TPU: +/-3.67 +/-154 Europium-152 U 3.88 U -2.24 pCi/L N/A (0%- 100%)
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| Uncert +1-535 +/-5.32 TPU: +/-5.24 +/-5.21 Europium-154 U 1.60 U 6.80 pCi/L 124 (0% - 100%)
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| Uncert: +/4.82 +/4.32 TPU: +/4.72 +/4.24 Europium-155 U -1.68 U 7.66 pCi/L N/A (0%- 100%)
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| Uncert: +/-6.80 +/-7.05 TPlU: +1-6.66 +/-6.91 Manganese-54 U -0.154 U 1.86 pCi/L NIA (0%- 100%)
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| Uncert: +/-1.92 +/-1.83 TPU: +/-1.88 +/-1.80 Niobium-94 U 1.33 U 2.26 pCVL 52 (0% - 100%)
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| Uncertn +/-1.66 +/-1.66 TPU: +/-1.62 +/-1.63 Silver-108m U 0.666 U 0349 pCiL 63 (0% - 100%)
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| Uncert: +/-1.61 +/-1.84 TPlU: +/-1.58 +/-1.81 QC1200663005 LCS Americium-241 1170 1390 pCi/L 119 (75%-125%) 08A4/04 12:49 Uncert: +/-229 TPU: +/-224 Cesium-134 U -11.6 pCi/L Uncert: +1-12.8 TPU: +/-12.6 Cesium-137 461 475 pCi/L 103 (75%-125%)
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| Uncen: +/43.7 TPU: +/42.8 Cobalt-60 704 819 pCi/L 116 (75%-125%)
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| Uncet. +/-65.7 32
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29ioi- (843) 556-81i1 - www.gel.com QC Summary Workorder: 116418 Page 2of 5 Parmname NflM1 1OrC -
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| mnle Oual Units' RPDo REC% Range Anist Date Time Rad Ganuma Spec Batch 349017 TPU: * +1-64.4 Europium-152 U -1.09. PCr/L Uncert: +/-28.6 TPU: - +/-28.0 Europium-154 U -9.84 PCr/L Uncert: +/1-31.6 TPU: +/-31.0 Europium- 155 U -30.6 PaiIL Uncert: +1-37.8 TPU: +/-37.0 Manganese-54 U 1.28 pCiIL Uncert: :. +111l.1 TPU: +/-10.9 Niobium-94 U -1.97 PCiIL Uncert: '+/-10.3 TPU: . +/-10.1 Silver-108m U -5.64 PCi/b Uncert: +/-8.92 TPU: +1-8.74 QC1200663002 MB mnericium-24 1 U -1.42 pCi/b 08/04/04 11:32 Uncert: '+/-13.1 TPU: +/-12.8 Cesium-134 U 0.0508 pCi/b Uncert: +/-2.02 TPU: +/-1.98 Cesium-137 U -0.591 PCi/b Uncert: ' +/-1.62 TPU: +/-1.59 Cobalt-60 U -0.388 pCi/b Uncert: +/1-159 TPU: - +1-1.55 Europium-152 U 0.521 paI/b Uncert: +I-5.36 TPU: +/-5.26 Europium-154 U -0.747 pCi/b Uncert: *$ +I-5.04 TPU: +1-4.93 Europium-155 U -4.05 pCi/b Uncert: +/-6.10 TPU: +/-5.98 Manganese-54 U .--1.94 pCi/b Uncert: +/-1.86 TPU: +/-1.82 Niobium-94 U 0.642 PCi/b Uncert -+/-1.69 TPU: +/-1.66 Silver-lOSm U 0.S46 PCi/L 33
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| GENERAL ENGINEERING LABORATORIES,- LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 116418 Page 3 or s Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date TimE Rad Ganuma Spec Batch. 349017 Uncert: +/-1.78 TPU: +/-1.75 QC1200663004 11641S001 MS Americium-241 9360 U -2.02 10500 pCi/L 112 08104/04 10:08 Uncert: +1-9.69 +/-2360 lPU: +1-9.50 +/-33000 Cesium-134 U 0.129 -72.2 pCi/L Uncert +/-1.89 +/-153 TPU: +1-1.85 +/-272 Cesium- 137 3690 U 0.322 3960 pCVL 107 Uncert: +I-1.S8 +1-546 IPU: +/-1.85 +1-12400 Cobalt-60 5700 U 1.08 5430 pCi/L 95 Uncert: +/-3.74 +/-721 TPU: +1-3.67 +/-17000 Europium-152 U 3.88 -104 pCI/L Uncert: +1-5.35 +1-342 TPU: +/-5.24 +1-467 Europium-154 U 1.60 146 PCUL Uncert: +/-4.82 +/-309 TPU: +/-4.72 +/-549 Eiuropium-155 U -1.68 -115 pOi/L Uncert: +/-6.80 +/-431 1PU: +/-6.66 +1-556 Manganese-54 u -0.154 83.4 pO/L Uncen: +/-1.92 +/-133 TPU: +/-1.88 +/-292 Niobium-94 U 1.33 -153 pCi/L Uncert: +1-1.66 +/-110 TPU: +/-1.62 +/1492 Silver-108m U 0.666 -73.9 pOi/L Uncen: +1-1.61 +/-113 TPU: +/-158 * +/-257 Rad Gas Flow Batch 34S452 QC1200661601 116418001 DUP Strontium-90 U -0.131 U 0.642 pCiL N/A (0% - 100%) IIOBI 07/17/0421:08.
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| Uncert: +/-0.374 +/-0.374 lPU: +1-0.376. +/-0.423 QC1200661603 LCS Stmntium-90 61.1 73.1 pCi/L 120 (75%-125%).
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| Unceit +/-2.61 TPU: +/-24.6 QC1200661600 MB Strontium-90 U 0.129 pcIL 07/17/04 21:09 Uncert: +/-0.363 TPU: +/-0.366 QC1200661602 116418001 MS I
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| 34
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| I GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407.- (843) 556-8171 - www.gel.com QC Summary Workorder. 116418 Page 4 of S -.
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| Parmname NONM Sample Qual OC Units RPD% REC% Ranee Anist Date Time -.
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| Rad Gas nlow Batch 348452 Strontium-90 122 U -0.131 148 pCi/L 121 (75%-125%)
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| Uncert: .140.374 +14.99 TPU: +1-0.376 +/-45.9 Batch 350569 QC1200666719 . 116418002 DUP Alpha U 0.410 U 1.25 pCilL 0 (0% - 100%) ATHI 07129/0404:48 Uncert: +/40.837 +1-0.834 TPU: +/40.838 +1-0.844 Beta 7.28 8.65 pCi/L 17 (0% - 100%)
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| Uncert: +1-1.55 ./-1.58
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| * TPU: +/-1.57 +/-1.65 QC1200666722 LCS Alpha 719 88.2 pCi/L 123 (75%-125%) 07l8104 20:01 Uncert: +/-8.67 TPU: +/-12.1 Beta 244 230 pCML 94 (75%-125%)
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| Uncert: +1-10.4 TPU: .+/-16.3 QC1200666718 NIB Alpha U -0.384 pCilL .07129/04 14:18 Uncert: +/-0.351 TPU: .+/-0.352 4.eta U 0.0197 pCilL Uncert: +1/0.997 TPU: +140.997 QC1200666720 11641S002 MS Alpha 108 U 0.410 104 pCi/L 96 (75%-125%) 0728/04 20.01 Uncert: +/40.837 +/-12.8 TPU: +/-0.838 '+1-14.9 Beta 367 7.28 391 pCi/L 105 (75%-125%).
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| Uncert: +/-1.55 +/-17.0 TPU: +/-1.57 +/-223 QC1200666721 116418002 NISD Alpha 108 U 0.410 117 pCitL. 12* 108 (75%-125%)
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| Uncert: +/-0.837 +/-13.4 TPU: +/-0.838 +/-16.1 Beta 367 7.28 405 pCi/L 3* 108 (75%-125%)
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| Uncert: +1-1.55 +1-17A TPU: +/-1.57 +1-23.3 Rad Liquid Scintllation Batch 350326 QC1200666134 116418001 DUP Tritium U -251 U 48.7. pCi/L N/A (0%-100%) JLBI 07/31/0401:04 Uncert: +/-229 +/-206 TPU: +/-229 +/-206 .
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| QC1200666136 LCS Tritium 3240 2650 pCVL 82 (75%-125%) 07130104 18:54 Uncert: +/-208 35.
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| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.comr QC Summary Workorder. 116418 Page Sof S Parmname NOM Samnle Chal OC Units' RPD% REC%7 Ranpe Anist Date Tme Rad Llquld Scintillation Batch 350326 TPU: +/-212 QC1200666133 MB Tritium U 82.6 pCiIL 07131/0400:01 Uncert: +/-209 TPU: +/-209 QC1200666135 11641S001 MS Tritium 3250 U -251 2790 pCi/L 86 (75%-125%) 07130/04 17:50 Uncert: +1-229 +/-214 TPU: +/-229 +/-218 Notes:
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| The Qualifiers in this report are defined as follows:
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| B Target analyte was detected in the sample as well as the associated blank.
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| BD Flag for results below the MDC or a flag for low tracer recovery.
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| E Concentration of the target analyte exceeds the instrument calibration range.
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| II Analytical holding time exceeded.
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| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
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| U Indicatels the target analyte was analyzed for but not detected above the detection limit.
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| Ul Uncertain identification for gamma spectroscopy.
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| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
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| h Sample preparation or preservation holding time exceeded.
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| N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.
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| ** Indicates analyte is a surrogate compound.
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| A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
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| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
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| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
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| 36
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| die, AtGENERAL ENGINEERING LABORATORIES, LLC 0 a Member of THE GEL GROUP, INC.
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| 1Z\.
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| p .Ej Meeting Today's Needs with a Vision for Tomorrow B4rows*
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| August 03, 2004 Mr. Dave Keefer CYAPCo Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 RE: Quarterly Groundwater PO# 002337 Work Order: 118053 .I SDG: MSR#04-1807
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| ==Dear Mr. Keefer:==
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| General Engineering Laboratories, LLC (GEL) appreciates the opportunity to provide the following analytical results for the sample(s) we received on June 28, 2004. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time.
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| This data report has been prepared and reviewed in accordance with GEL's standard operating procedures. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4475. -
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| Sincerely, -
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| Purchase Order: 002337 Enclosures RO. Box 30712
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| * Charleston, SC 29417
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| * 2040 Savage Road (29407)
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| Phono (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com
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| I CONNECTICUT YANKEE RE: Quarterly Groundwater PO# 002337 Work Order: 118053.
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| SDG: MSR#04-1807 118053004 MW100D-0204-001 118053005 118053006 r\'W-103S-0204-001 rvIW-104S-0204-001 9
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| 118053003 MW-1O1D-0204-001 118053001 MW-108S-0204-001 118053002 MW-125S
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| Table of Contents Case Narrative .................................................................... 1 Chain of Custody ..................................... 4 Cooler Receipt Checklist ............................................. 11 Radiological Analysis .................................... 20 Sample Data Summary:;.......... 23 Quality Control Data .................. ......................... 30
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| -1.
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| all CASE NARRATIVE 1 1
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| CASE NARRATIVE For CONNECTICUT YANKEE RE: Quarterly Groundwater PO# 002337 Work Order: 118053 SDG: MSR#04-1807 August 3, 2004 Laboratory Identification:
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| General Engineering Laboratories, LLC Mailing Address:
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| P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:
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| 2040 Savage Road Charleston, South Carolina 29407 Telephone Number:
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| (843) 556-8171 Summary:
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| Sample receipt The soil samples for SDG# MSR#04-1807 arrived at General Engineering-Laboratories, LLC, (GEL) in Charleston, South Carolina June 28, 2004. The samples were originally assigned to GEL WO# 115774 and per the request of Dave Keefer on July 29, 2004, six groundwater samples were re-assigned to WO# 118053. All sample containers arrived without any visible'signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.
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| The laboratory prepared the following sample::
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| 118053004 MW100D-0204-001 118053005 MW-103S-0204-001 118053006 MW-104S-0204-001 118053003 MW-IOID-0204-001 118053001 MW-108S-0204-001 118053002 MW-125S.
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| GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
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| P.O. Box 30712 - Charleston, SC 29417 - 2040 Savage Road (29407)
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| Phone (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com
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| Items of Note: '\ v There are no items to note.
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| Case Narrative:
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| Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.
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| Analytical Request:
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| Six soil samples were analyzed for Gammaspec(Co-60).
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| Internal Chain of Custody:
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| Custody was maintained for all of these samples.
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| Data Package:
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| The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Laboratory Certifications, and Radiochemistry.
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| I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.
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| Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
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| RO. Box 30712 - Charleston, SC 29417 a 2040 Savage Road (29407)
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| Phone (843) 556-8171
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| * Fax (843) 766-1178
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| * www.gel.com 3
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| I, I
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| i j
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| CHAI N i t
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| . 4
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| .nr .
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| ; . a_ 1 j
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| CUST-ODY . M i
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| j . ,
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| i t
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| .i i
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| .4
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| ci.
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| Health Physics Procedure \ - G4-~fGR-R5104-003-Attacliment B-CY-00lI Major Connecticut Yankee Atomic Power CompanyChiofusdyFr No. 2004.00108 362 Injun Hollow Road, East Hampton, CT 06424 8 60 -26 7-2 556 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
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| Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only~K~-
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| Contact Name & Phone: * +:~. ~ ~ .
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| Rich McGrath 860-267-3573 ei Sa pe Cnanr-.
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| Code Type Size- .- . . . -
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| Analytical Lab (Name, City, State): Code &TypC 4~,
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| General Engineering Lab (GEL), 2040 Savage Rd,Coe > -
| |
| ChalesonSC29407,843.556.8171 (Sarah K zi Priority:-145 D.Z30 D.E 14 D.I7 D. . iV O ther . .. , .* .
| |
| Sample Designation Date Time Comment, Preservation Lab.Sample ID-"
| |
| /MW-io95.02o-0qo,~ U-/-YA. Lw WG G 4L,1IL X - - _____
| |
| MA- 2.Z_~O2.oy-e~,,, 9 xk'/ /2,0 WG G 4L,lIL ~- - _ _ _ _
| |
| _ _ __ _ __ _ _ _ _ _ _ _ WG G 4L , I1L_ __ _ _ _ _ _
| |
| _ __ _ _ _ _ _ _ _ _ _ _ WG G 4L, IL
| |
| _ __ __ _ __ _ _ _ _ _ _ _ _ _ WG G 4 L , IL _ __ _ _ _ _ _
| |
| rer4 NOTES: P0OM 002337. MSR #: 04-1807 El LTP QA- El Radwaste QA Non QA Samples Shipped Via: InenlCnainer 0Fed Ex Temp. ~ eg. C Requested analyses should be performed to typical groundwater program MDC's. El Hand Custody Seald quished By. Date/Time ) eFvdBy DtCustody Seal nat
| |
| '6qU 0'N5 El Other
| |
| : 3) Rel quished By. Date/Time 4) Received By Date_________NO,`_
| |
| Bill of Ladingf
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time. .
| |
| C C
| |
| | |
| C. (6( 1 Health Physics Procedure I 1 GPP-GGGR-R5104-003-Attachnient B-CY'-001 Major .
| |
| Cdonnectic'ut Yankee Atomic Pbwer Companiy .- Cano utd omN.20-00
| |
| .362 Injun Hollow Road, East Hampton, CT 06424 ..-
| |
| 860-267-2556 Project Name: Haddam Neck Decommissioning .Analyses Requested .Lab .UseO Iniy;c .
| |
| Contact Name & Phone:
| |
| Rich McGrath, 860-267-3573 __
| |
| Media Code Sample Type '
| |
| Container Size-.
| |
| ~
| |
| Alica! Lab (Namne, City, State):-- Code &Type Geneal ngieering Lab (GEL), 2040 Savage Rd, oe x-- .* -. * ~
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Kozlik). W.... .~
| |
| Ptiority: El45 D. [0 30 D.'El 14 D. El7 D. - . .
| |
| aml )igaif Date' Time- . Comment, Preservation Lab Samrple ID' maIs &-LI.- ogI 16c WG_ G 4L, IL ZHL-11~.O U
| |
| 1U - IN ; G-" 41o,-
| |
| L, IL -ZL(
| |
| 1!M7o,/.4ry
| |
| __*G: 'G- 4L,-IL
| |
| _ _ WG. 4L,IL _ _ _ _ _ _ _
| |
| . VG G 4LL_
| |
| NTSPO 0037 MR:04-1807 ir1LTP Q E]Radwvaste QA aroner Fed Ex Tm A e El UPS Requested analy~ses, should be performed to typical groundwater program MDC's. ElHand Cf~ad I) R quse y ae ie 2) A eived By Date/Time CsoySa nat
| |
| .!%L El1 Other -
| |
| ~4-_
| |
| : 3) R fquished By Date/Time 4) Received By Date/Timne _________
| |
| Bill of Lading YI
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time
| |
| | |
| Healthlhy'sic'sProc'edure '- ' HGPP-GGGR-R5 104-003-Attachment B-CY-001 Major Chain of Custody Form N.20-01 Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning nalyses Requested.
| |
| Contact Name & Phone:
| |
| Rich McGrath 860-267-3573 ,edia Code Sample Type onainer Size- ~ ,,;
| |
| 3.
| |
| Analytical Lab (Name, City, State): - Code &Typ c . . r-General Engineering Lab (GEL), 2040 Savage Rd, -. Co c 4 Z .. '.''i r , ; .'
| |
| Charleston, SC -29407, 843.556.8171 (Sarah Kozik) .
| |
| Priority: 0 45 D. 30 D. l 14 D. F1 7 D. , , . .
| |
| Other:
| |
| Sample Designation Date Time . Comment, Preservation Lab Sapl I'D'IQ.
| |
| PA Iu WG G 4L, ILT
| |
| ____zcy_ j ~ 1/WG G 4L,1L _ - - r AI4J ,.l WG G 4L,1L L_ '
| |
| ._ WG G 4L,1LL - . --
| |
| WG G 4L,1L . . . . , 4. i.
| |
| NOTES: PO#: 002337 MSR#: 04-1807 El LTP QA n Radwaste QA El Non QA Samples Shipped Via: . a Fed S Ex T'Deg .- :C..-.
| |
| El UPS Requested analyses should be performed to typical groundwater program MDC's. El Hand Custoy Sealed?
| |
| l)Rtinquished By Date/Time 2) R ived By Date/Time CustodySeal Intact?
| |
| 6/2- )aS4 y El Other 3)Rfinquished By Date/Time 4) Received By Date/Time _,-'.':.:Y, ''N 0 Relinquished By 5). D 6)R e By D of Lading........ ,Bill 5)Relinquished By 'Date/Time 6) Received By Date/Time -..,,;,9^.,:';; ,;......,,
| |
| U C (
| |
| r
| |
| | |
| *:. C .. -- (,
| |
| .Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2004-00105 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 '- '-__- -
| |
| Project Name: Haddam Neck Decommissioning Analyses Requested La, bUscuniy .L* .. .
| |
| Contact Name & Phone:- ,
| |
| Rich McGrath 860-267-3573 Media Code Sample Type - Container Size- - ' ';- . .
| |
| Analytical Lab (Name, City, State): . . Code &Type .
| |
| General Engineering Lab (GEL), 2040 SavageRd, Code M -; '
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Kozlik) .r . ." ..
| |
| Priority:f]45D;l30D.;EIi4D.[l7D. - . . . t O th er :.
| |
| 'q4 /Time(--
| |
| Sample Designation I- c-o I *Date 5' ~
| |
| Time^ - . - -
| |
| -~
| |
| - Comment, Preservation ' ab ~'Sample ..PieID II-tAjX,7-o2tg~o1" /29t52.7 WG G 4L, IL -_ -. a3 -.
| |
| q gz/ 1 O o$LJ& WG -- G . 4L, IL =_._ - - . - Ao3 - __;;;__,
| |
| 4L, IL B 2 -
| |
| WG G 4L, IL .Z- .
| |
| , _.._._ ___ .r - .
| |
| .- .' . - C p Y.;-;
| |
| .. ,....;=;eE' ;':;.'
| |
| --_ __ _ __ _ =_ _ _ _ _ _ ___
| |
| '..''-' .. . - ~ . .,;*- i.
| |
| * JI tl
| |
| ^.
| |
| * I- 4 l i Requested ..
| |
| NOTES: 1POanalyses
| |
| #: 002337should be MSR performed
| |
| #: 04-1807 to typical groundwater E1 LTP QApgramEl Radwaste QA lg Non QA I. ISamples
| |
| ]DC's.
| |
| ' HandShipped Via:
| |
| i___ 'w.. .j, USC'fgSeakd?
| |
| lntemia3..ontatner.
| |
| -l''-.',. '-N 1)?41quishedBy . .ate/Time 2 e e ed Date/ Custody Seai lnitacti.
| |
| 8 Pt /45y 1.0 w , i 0 0G __ /Other '.
| |
| : 3) Retinquished By" - DatetTime - 4) eived By DatelAime.
| |
| ..... Bill of Lading#
| |
| : 5) Relinquished By. Date/Time 6)Received By Date/Time .r ..
| |
| | |
| Hd0 oBC1Ma Health Ptysics Procedure .qPP-GGGR-R5 104-003-Attaclunent B-CY-001 Major Connecticut Yankee Atomic Power CompanChain of Custody Form 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested = Lab Use Only- - - .; 5. 1
| |
| & Phone:
| |
| Contact NameConac :;a'-i-'''-- -- --:
| |
| Po~e:Media Nme Sample Container RichMcGrath 860-267-3573 Code Sile .
| |
| Analytical Lab (Name, City, State): Code &Type * --.
| |
| General Engineering Lab (GEL), 2040 Savage Rd, Code Charleston, SC-29407, 843.556.8171 (Sarah Kozlik) ':
| |
| Priority: E 45 D.N 30 D. El 14 D. n 7 D.
| |
| Other: _____
| |
| Sample Designation Date Time __Comment, Prcserva-tion "Lab Sample ID '
| |
| AAUJ I ozoy-cvi
| |
| -I WG 1 4L, IL 1 *. t 1 t I I
| |
| .Hi, , I i^to-io WA-31ol I/ 1 36 Wo G 4L, IL HdItu, dJOf WG G 4L,1LL ,,. -- -::_:"''"
| |
| WG G 4L,1L L ==-____:,;;
| |
| WG G 4L,1L L ;:' -; .'_ .-
| |
| NOTES: PO#: 002337 MSR#: 04-1807 E0 LTP QA El Radwaste QA ED Non QA SamplesShippedVia: InternalContainer 0 FedEx Temp r'3:Deg;C
| |
| .. UPS -.
| |
| Requested analyses should be performed to typical groundwater program MDC's. O Hand ' .Ctstody'Sealed?.
| |
| . -iY G--N O I) inquished By: Date irie - 'R~ceivedB. Date/Time Custody Seal Intact?
| |
| G(s -X/Y aex L@ Qyt-o . '~ L[& El Other -
| |
| : 3) Retinquished By Date/Time 4) Received By . Date/Time - . YI N O' Bill of Lading #
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time C C(
| |
| | |
| CF .:C -R. .1 Y- Mjor Health Physics Procedure GPP-GGGR-R5104-003-Attaichment B-CY-001 Major Chain of Custody Form Connecticut Yankee Atomic Power Company No. 2004-00109 362 Injun Hollow Road, East Hampton, Cl 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Contact Name &Phone: _ . . . . . .,
| |
| Rich McGrath 860-267-3573 Media Sample Container Code Type Size--
| |
| Analytical Lab (Name, City, State): Code &Type e i- .
| |
| General Engineering Lab (GEL), 2040 Savage Rd,, C .!, ;
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Kozlik)
| |
| Priority: []45 D. 30 D. 14 D. El 7 D. -- 717:',
| |
| Sample Designation Date Time Comment, Preservation . Lab sample ID 4V1-10 -6 4.z.c0 ( 2.3 6y 1 12Lo WG G 4L, IL - -;
| |
| wvtsI-lj-b t' I-coz l t '- Ci) WG G 4L,1L Z - - - -
| |
| .___ ____ WG G 4L,1LL; -.
| |
| WG G 4L,1LL.<::,;i.
| |
| WG G 4L,1L .
| |
| NOTES: PO: 002337 MSR 04-1807 LTP QA =Radwaste QA Non QA Samples Shipped Via: . Internal Confitainier:
| |
| 0l Fed Ex ,ep~~Dg Requested analyses should be performed to typical groundwater program MDC's. El Hand .C tody Seed? +
| |
| I) *nquished By . Date/Time 2) Recived By Date/Time Custody seal Intact 9
| |
| - , My s El%8Other
| |
| : 3) inquished By Date/Time 4) Received By Date/Time Bill of Lading #;
| |
| : 5) Relinquished By Date/Time 6) Received By Date/Time . . '.1
| |
| .__________________________________________ r~- r' l;5 E! "^'
| |
| | |
| -1 k>- `
| |
| COOLER RECEIPT CHECKLIST K)I GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP, INC.
| |
| P.O. Box 30712
| |
| * Charleston, SC 29417 - 2040 Savage Road (29407)
| |
| =i I11
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-OO1 I Figure I.-Sample Check-in List Date/TimeReceived: tA 4S AR\
| |
| SDG9#. M( R -t:X Ioie Work Order Num Il
| |
| * Shipping C !(O Clhain of Custody# 0OO't -0o 1Ot
| |
| : 1. Custody Seals on shipping container intact? Yes (4 No [1
| |
| : 2. Custody Seals dated and signed? Yes t] No[]
| |
| : 3. Chain-of-Custody record present? Yes (4 No []
| |
| : 4. Cooler temperature 3. k-
| |
| : 5. Vermiculite/pack-ing materials is: Wet [ Dry [vf
| |
| : 6. Number of samples inshipping container. __
| |
| : 7. Sample holding times exceeded? Yes ]. No .
| |
| S. Samples have:
| |
| J tape _ hazard labels custody seals -appropriate sample labels
| |
| : 9. Samples are:
| |
| n good condition leaking
| |
| _ broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [t4 No [1 I1. Description of anomalies (include sample numbers):
| |
| -Sample CustodianlLaboratoiy: Q U Date:________
| |
| Telephoned to: - 0 nn By
| |
| . . . .. . I 12
| |
| | |
| /
| |
| Connecticut Yankee Statement of Work
| |
| _ for Analytical Lab Services CY-ISC-SOW-001 Figure ]. Sample Check-in List KIU Date/Time Received: - 9 As 1- / 8: '
| |
| SDG#: ( S q S >
| |
| Work Order Numb \\ 9 Shipping Container ID: 960 I Chain of Custody # 2 oo4 -.ooioa I. Custody Seals on shipping container intact? Yes (L-No
| |
| : 2. Custody Seals dated and signed? Yes [ti1o 1I (II
| |
| : 3. Chain-of-Custody record preqent? Yes 4,%io
| |
| : 4. . Cooler temperature G94t $
| |
| : 5. Vermniculite/packing materials is: Wet [ ] Dry [t.
| |
| : 6. Number of samples in shipping container CO
| |
| : 7. Sample holding times exceeded? Yes [eNo [ ]
| |
| : 8. Samples have:
| |
| K) tape hazard labels Custody seals appropriate sample labels
| |
| : 9. Samples are:
| |
| ____n good condition leaking broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes [ ] No ['<
| |
| : 11. Description of anomalies (include sample numbers):
| |
| .~- . . .
| |
| Sample Custodian/Laboratory: (1 'J , /XI - Date: -_
| |
| Telephoned to: On
| |
| -By
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-1sc-sow-001
| |
| - I Figure 1. Sample Check-in List I/ v-. t ' : , < A _
| |
| Date/Time Received: ( s. ) - -' 1tAdd aOfy SDG#. -
| |
| Work Order Nuiier: \\5j\
| |
| Shipping Container IDi Afl l?..zfl\5 (tain of Custody #. I Awok-coOt-0
| |
| : 1. Custody Seals on shipping container intact? Yes.f'T .No [ ]
| |
| : 2. Custody Seals dated and signed?' Yes [V No (]
| |
| : 3. , Chain-of-Custody record present? Yes [MNo [I
| |
| .4. Cooler temperature c 5, '5
| |
| : 5. Verrmiculite/packing materials is: Wet [ - Dry [bb
| |
| : 6. Number of samples in shipping container:
| |
| : 7. , Sample holding times exceeded? Yes,[] No M KI I
| |
| : 8. Samples have:
| |
| /tape -hazard labels
| |
| _custody seals . appropriate sample labels
| |
| : 9. Samples arc: - --
| |
| V/ in good condition leaking
| |
| ._l_broken have air bubbles 0, A
| |
| : 10. ; Were any anomalies identified in sample receipt? . - Yes No'
| |
| : 1. Dneun
| |
| ...I 1. Description of anomalies (include samnple numbers):
| |
| LXitkt$L L --. ea s MWle Sample .CistodianiLaboratoryy.. .Iate:e:,&J/ q Tclcphoned to: _I On I-
| |
| -J By - . . .
| |
| 1 4:
| |
| | |
| Connecticut Yankee Statement of Work for Analytical
| |
| - Lab Services CY-ISC-SOW-o0I Figure 1. Sample Check-in List Date/Time Received: &) ;G"I OL / 4 SDG#: -
| |
| Work Order Number. l Shipping Container ID: r9i i .Chain 44 of Custody#_ r~)2o04Ooo 0S
| |
| : 1. Custody Seals on shipping container intact? Yes [To [ ]
| |
| : 2. Custody Seals dated and signed? Yes (T9 I ]
| |
| : 3. Chain-of-Custody record present? Yes [*No [ I
| |
| : 4. Cooler temperature . jgq
| |
| : 5. Vermiculite/packing materials is: Wet [Wlry [ ]
| |
| : 6. Number of samples in shipping container.
| |
| : 7. Sample holding times exceeded? Yes (<No [ ]
| |
| : 8. Samples have:
| |
| tape hazard labels custody seals _ _propriate sample labels
| |
| : 9. Samples are:
| |
| _ in good condition leaking broken ___have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes (ql'No 1 :
| |
| : 11. Description of anomalies (include sample numbers): .ZU'p " A M ) Seo s.(Ia)
| |
| I"VVw 5 i 1Dt)2.. Sre.! cv (1.D. t lt C Sampl CusodianALnhorntr:( uae) >
| |
| Telephoned to: On By.
| |
| | |
| Connecticut Yankee
| |
| . Statement of Work for Analytical Lab Services I ' -! CY-ISC-SOW-001
| |
| - Figure 1. Sample Check-in List
| |
| . Date/Time Received: - g o 8- 4
| |
| -. SDn{ m :"V~, -4()4- Ot7 . ,-
| |
| - Work OrderNumbe) \\1A'A. c5 Shipping'Container ID. 7M2 to 7151 4475: Chain of Custody # ' ;Ot) - 0°° li I. Custody Seals on shipping container intact? Yes El/rNo[]
| |
| : 2. Custody Seals dated and signed? Yes f[ 4/No ]I
| |
| : 3. Chain-of-Custody record present? Yes [qNo'[]
| |
| : 4. Cooler temperature CX-( 4 G
| |
| : 5. Vermniculitelpacking materials is: 'Wet [ ] Dry [i(
| |
| : 6. Number of samples in shipping container. .,
| |
| : 7. ISample holding times exceeded? * ~ Yes EJ] No'[ ]
| |
| S. Samples have:
| |
| .tape ' azard labels
| |
| * 1, custody seals appropriate sample labels
| |
| : 9. Samples are:
| |
| in good condition .' 'leaking
| |
| . _'_,broken - have air bubbles
| |
| : 10. Were 'any anomalies identified in sample receipt? Yes [ No'.'-
| |
| I 11. Description of anomalies (include sample numbers):
| |
| .rip.
| |
| Sample Custodian/Laborator. H O Date Telephoned to: On - By -
| |
| | |
| JR-Connecticut Yankee Statement of Worik for Analytical Lab Services CY-ISC-SOW-00 1 Figure 1. Sample Check-in List Date/Time Received:G - C': 4 7 t L/2 SDGN: ni Work Order Number.
| |
| ShippingContainer ID7q264 7(5 &L153 ChainofCustody# 7 I1
| |
| : 1. Custody Seals on shipping container intact? Yes s No [ ]
| |
| : 2. Custody Seals dated and signed? Yes tTNo ( ]
| |
| : 3. Chain-of-Custody record present? Yes [-Hlo ( ]
| |
| : 4. Cooler temperature ab.*
| |
| : 5. Vermiculite/packing materials is: Wet [] Dry (Vr
| |
| : 6. Number of samples in shipping container C
| |
| : 7. Sample holding times exceeded? Yes two II
| |
| : 8. Samples have:
| |
| "_tape hazard labels custody seals ___appropriate sample labels
| |
| : 9. Samples are:
| |
| n good condition leaking l broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes 'No t' ]
| |
| : 11. Descriptionofanomalies(includesamplenumbers): C e UUA 103S Ho Sample CustodianlLaboratoryf'
| |
| * Date: - 6L1 Telephoned to: On By 17
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/Time Received wcfA-1' SDG#: -
| |
| .Work OrderNumbec k VYt hp eColi b (ll 3 Chain of Custody# 0 (ZO_
| |
| I ! Custody Seals on shipping container intact? Yes [%f No ..
| |
| : 2. .Custody Seals dated and signed? Yes No [1
| |
| : 3. 'Chain-of-Custody record present? Yes A No [ ]
| |
| : 4. Cooler temperature Ho 1)?
| |
| : 5. Vermiculite/pack-ing materials is: Wet [ Dry (v%
| |
| : 6. Number of samples in shipping container __
| |
| 7.; Sample holding times exceeded? Yes ]No-M
| |
| : 8. Samples have:
| |
| .ŽZltape -hazard labels custody seals' __-_appropriate sample labels . -
| |
| : 9. Samples are:
| |
| n good condition -_ leaking
| |
| __ broken _____have air bubbles :-
| |
| : 10. Were any anomalies identified in sample receipt? Yes -j No ]
| |
| A11.-. Description of anomalies (include sample numbers):
| |
| SamplepCushodmt:ry- 1L Date:. ,x /_f Telephoned to: - - On B
| |
| | |
| Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-SOW-oo1 Figure 1. Sample Check-in List DatelTime Received - 4 C9- - oq / . go)
| |
| SDGN: th °A \ c Work Order Numbe Shipping Container ID: '55D r'( _ Q5iChain of Custody #t ab I lIob
| |
| : 1. Custody Seals on shipping container intact? Yes MNo 1]
| |
| : 2. Custody Seals dated and signed? Yes [Li-o [
| |
| : 3. Chain-of-Custody record present? Yes /No I I
| |
| : 4. Cooler temperature c/. f
| |
| : 5. Vermiculite/packing materials is: Wet [ 1 Dry ('f-
| |
| : 6. Number of samples in shipping container
| |
| : 7. Sample holding times exceeded? Yes [ INo [ ]
| |
| : 8. Samples have:
| |
| _____hazard labels
| |
| -.. custody seals _appropriate sample labels
| |
| : 9. Samples a in good condition leaking
| |
| _l_broken have air bubbles
| |
| : 10. Were any anomalies identified in sample receipt? Yes (tPI Ig ]
| |
| : 11. Description of anomalies (include sample numbers): j 1 OcI4rA4L (
| |
| --~~~~~~~1 8.se aI itgdM l
| |
| : Sample Custodian/Laboratory: Q *R(YO IDate:(:,- D, - 0 j Telephoned to: On By_
| |
| IQ
| |
| | |
| . . I d , di RADIOLOGICAL
| |
| -ANALYS IS 20;
| |
| | |
| Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)
| |
| Work Order 118053 Method/Analysis Information Product: Gammaspec, Gamma,Liquid-Co-60 Recount Analytical Method: EPA 901.1 Analytical Batch Number 354048 Sample ID Client ID 118053001 MW-108S-0204-001 118053002 MW-125S 118053003 MW-IOID-0204-001 118053004 MWIOOD-0204-001 118053005 MW-103S-0204-001 118053006 MW-104S-0204-001 1200675120 Method Blank (MB) 1200675123 Laboratory Control Sample (LCS) 1200675121 118053001(MW-108S-0204-001) Sample Duplicate (DUP) 1200675122 118053001(MW-108S-0204-001) Matrix Spike (MS)
| |
| SOP Reference Procedures for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information: ~,j Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 118053001 (MNV-108S-0204-001).
| |
| QC Information Allof the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| 21
| |
| | |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-prepfRe-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| AMiseellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Oualifier information Manual qualifiers were not required.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| The following data validator verified the information presented in this case narrative:
| |
| Reviewer:
| |
| 22
| |
| | |
| SAMPLE DATA SAM PL E DATA
| |
| | |
| ==SUMMARY==
| |
| | |
| \KJ 23
| |
| | |
| LLC LABORATORIES, ENGINEERING GENERAL GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407- (843) 556-8171 -www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddaxn Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date August 3,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project Quarterly Groundwater PON 002337 -, - Page I of I.
| |
| Client Sample ID: MW-108S-0204-001 Prpiect: YANK00304 SamnpleID: 118053001 ClientID: YANKC00 Matrix Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-UN-04 Collector Client Parameter Qualifler - Result Uncertainty LC TPU MDA Units DF - AnalystDate Time -Batch Mtd.
| |
| Rad Gamma Spec Analysis
| |
| . Ganmaspec. GammngLiquid-Co-60Recount Cobalt-60 ' U 4A1 41-3.05 2.25 +/-2.99 5.01 pCUL AKB 08102/04 1236 354048 1
| |
| -he following Analytical Methods were performed'-
| |
| K~letlod Description -
| |
| I EPA 901.1 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration ofthe target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.:
| |
| J Indicates an estimated value.' The result was greater than the detection limit, but'less than the reporting linit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit. -
| |
| U1. Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an was received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozllc' Reviewed by 24
| |
| | |
| LIC LABORATORIES, GENERAL ENGINEERING GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charieston SC 29407- (843) 558-8171 - www.gei.com Certificate of Analysis Company: CYAPCo Address: Haddamn Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Dato: August 3,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MW-125S Prpiece YANK00304 Sample ID: 118053002 Cl.int ID: YANK001 Matri Ground Water Vol. Recv.:
| |
| Collect Date: 22-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rxd Gamma Spec Analysis Gammaspec, Ganma. iquld-Co-60Recount Cobalt-60 U 0.291 +1-2.04 1.72 +/-2.00 3.87 pCi/L AKB 08/02/04 1237 354048 1 The foilowinag Analytical Methods were performed Method . Description I - EPA 901.1 K)1, Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| U! Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC.
| |
| standard operating procedures. Please direct any question's to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 25.
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568-171 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 3,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO 002337 - Page I of I Client Sample ID: ; MW-IOID-0204-001 Pr.Piect- YANKCO304 Sample ID: .118053003 VClient ID: YANKOOI Matrix: Ground Water Vol. Recy.:
| |
| Collect Date: 23-JUN.04 Receive Date: 28-JUN-04 Collector Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate - TIme BatchMtd.
| |
| Rad Gamma Spec Analysis Ganmaspec, GammaLiquid-Co-60 Recount Cobalt-60 U 0.634 +/-1.82 1.60 +/-1.78 3.67 pCi/L AKB 08102.04 1237 354048 I The foflowlag Analytical Methods were performed Method Description
| |
| - EPA 901.1 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.'
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UlI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data suimasy package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| 4icc&u CD ad Reviewied by 26 -
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - ww.gel.comn
| |
| .KJ Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 3,2004
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 1 of 1 Client Sample ID:
| |
| * MWIOOD-0204-001 Peiect: YANK00034 Samele ID: 118053004 Clent ID: YANK001 Matnrx Ground Water Vol. Recv.:
| |
| Collect Date: 23-JIN-04 Receive Date: 28-JUN-04 P me aa t Qualifer. Rr . iU DT Parameter QuzUfler Result Uncertainty -Lt TPU MDA Units DF AnalystDate *Time Batch Mtd.
| |
| Rad Gammna Spec Analysis Gammaspec, GammaLiquid-C660Recount Cobalt-60 U -0.521 +/-2.74 1.89 +1-2.68 4.28 pCPL AKB 08/02/04 1238 3540481 The following Analytical Methods were performed Method Decription I EPA 901.1 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The-result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| !kca&.i9 Reviewed by CQx C&3 27
| |
| | |
| LLC LABORATORIES, ENGINEERING GENERAL GENERAL ENGINEERING LABORATO RIES, LLC 2040 Savage Road Charleston SC 29407- (843) 5564171 - ww.gel.comn
| |
| . Certificate of Analysis -'''
| |
| Company: CYAPCo Address: Haddam Neck Plant 362 Injum Hollow Road Eist Hampton, Connecticut 06424 Report Date: August 3,2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 - Page I of.1 Client Sample ID: MW-103S-0204-001 Priect: YANK00304 Sample ID: 118053005 Clent ID: YANKOO0 Matrix: Ground Water Vol.Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-04 Collector Client
| |
| .. Parameter Qualfler Result Uncertainty LC TPU - MDA Units . ' DF AnalystDate Ttme Batch Mtd.
| |
| Rad Gamma Spec Analysts kmimaspec, GammaLlquld-Co-60Recount Cobalt-60 13.7 +/4.93 1.78 +/-4.83 4.04; pCiL . AKB 08/02104 1238 354048 1 The folowlng Analytical Methods were performed - -
| |
| *ethod Description EPA9011 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| .U Indicates the target analyte was analyzed for but not detected above the detection limit.'
| |
| Ul Uncertain identification for garmma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| - h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordaine with General Engineering Laboratories, LLC -
| |
| standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlik.
| |
| Reviewed by 28:
| |
| | |
| G R E GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 5568171 - www.gel.corn K-i
| |
| - Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424
| |
| * Report Datce August 3, 2004 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page I of I Client Sample ID: MW-l 04S-0204-001 Pzrpect: YANKO00304 Samele ID: 118053006 Client VD: YANKOOI Matrix Ground Water Vol. Recv.:
| |
| Collect Date: 23-JUN-04 Receive Date: 28-JUN-04 oliectnro Client Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec. Gammnalqul Co-60 Recount Cobalt-60 U -0.163 +/-2.17 1.77 +/-2.13. 4.00 PCI/L AKB 08/02/04 1239 3540481 -
| |
| The following Analytical Methods were performed Method Description EPA 901.1 :
| |
| Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration' ofthe target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection linit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit..
| |
| UI. Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data sumnmary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an "as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozilk.
| |
| Reviewed by 29
| |
| | |
| QUALITY CONTROL DATA-30
| |
| | |
| : lI GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: August 3,2004 Client: CYAPCo Page 1 of 1 Hladdam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Workorder 118053 Parmname NOM Sample Qual QC Units RPD% REC% Range AnIst Date Time Rad Gamma Spec Batch 354048 QC1200675121 118053001 DUP Cobalt-60 U 4.41 U 0.317 pCVL 173 (0%- 100%) AKB 08102/04 18:04 Uncert: +1-3.05 +/-1.46 TPU: +/-2.99 +/-1.43 QC1200675123 LCS Cobalt-60 563 570 pCiIL 101 (75%-125%) 08/03/04 12:05 Unccrt: +/-70.9 TPU: +/-71.8 QC1200675120 MB Cobalt-60 U -0.456 pCi/L 08/02104 12:39 Uncert: +1-2.12 TPU: +1-2.08 QC1200675122 118053001 MS Cobalt-60 5710 U 4.41 6410 pCi/L 112 08/03/04 12:04 Uncert +/-3.05 +1-672 TPU: +/-2.99 +/-20100 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| Ul Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.
| |
| ** Indicates analyte is a surrogate compound.
| |
| A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +1-the RL is used to evaluate the DUP result.
| |
| For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
| |
| Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
| |
| 31
| |
| | |
| CONNECTICUT YANKEE RE: Quarterly Groundwater PO# 002337 Work Order: 118907 SDG: MSR#04-1807 118907001 MW-103S-0204-001 118907002 MW-103S-0204-001-rllter
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC
| |
| '\ r Cw a Member of THE GEL GROUP, INC.
| |
| 7 gM2 0 Meeting Today's Needs with a Vslon for Tomorrow August 24, 2004 Mr. Dave Keefer CYAPCo Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 RE: Quarterly Groundwater PO# 002337 Work Order: 118907 SDG: MSR#04-1807
| |
| | |
| ==Dear Mr. Keefer:==
| |
| | |
| General Engineering Laboratories, LLC (GEL) appreciates the opportunity to provide the following analytical results for the sample(s) we received on June 28, 2004. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time.
| |
| This data report has been prepared and reviewed in accordance with GEL's standard operating procedures. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4475.
| |
| Sincerely, Purchase Order: 002337 Enclosures RO. Box 30712 - Charleston, SC 29417
| |
| * 2040 Savage Road (29407)
| |
| Phone (843) 556-8171
| |
| * Fax (843) 766-1178 *.www.gel.corn
| |
| | |
| Table of Contents Case Narrative ..... ..................................... .............. 1 Chain Of Custody ................. ................................... 4 Radiological Analysis .......................... ........................ 6 Sample Data Summary ............. ................................. 11 Quality Control Data .............................................. 14
| |
| | |
| CASE NARRATIVE i 1
| |
| ,I
| |
| | |
| CASE NARRATIVE For CONNECTICUT YANKEE RE: Quarterly Groundwater PO# 002337 Work Order: 118907 SDG: MSR#04-1807 August 24, 2004 Laboratory Identification:
| |
| General Engineering Laboratories, LLC Mailing Address:
| |
| P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery-and Shipping Address:
| |
| 2040 Savage Road Charleston, South Carolina 29407 Telephone Number: -
| |
| (843) 556-8171 Summarv:
| |
| Sample receipt :
| |
| The groundwater samples for SDG# MSR#04-1807 arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina June 28, 2004. The samples were originally assigned to GEL WO# 115774 and per the request of Dave Keefer on August 4, 2004, one groundwater sample and it's filter counterpart were re-assigned to WO# 118907. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.
| |
| The laboratory prepared the following sample:
| |
| MW-103S-0204-001 MW-103S-0204-001-filter.
| |
| Items of Note:
| |
| There are no items to note.
| |
| GENERAL ENGINEERING LABORATORIES, LLC a Member of.THE GEL GROUP, INC.
| |
| P.O. Box 30712
| |
| * Charleston, SC 29417 - 2040 Savage Road (29407)
| |
| Phone (843) 556-8171
| |
| * Fax (843) 766-1178
| |
| * www.gel.com
| |
| | |
| Case Narrative:
| |
| Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.
| |
| Analytical Request:
| |
| One groundwater and one filter sample were analyzed for Gammaspec(Co-60).
| |
| Internal Chain of Custody: -
| |
| Custody was maintained for all of these samples.
| |
| Data Package:
| |
| The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Laboratory Certifications, and Radiochemistry.
| |
| I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.
| |
| <-/
| |
| GENERAL ENGINEERING LABORATORIES; LLC a Member of THE GEL GROUP, INC.
| |
| RO. Box 30712
| |
| * Charleston, SC 29417
| |
| * 2040 Savage Road (29407)
| |
| Phone (843) 556-8171 s Fax (843) 766-1178
| |
| * w(w.gel.com 5.
| |
| | |
| r II I ..lI
| |
| ,I .j, HAIN OF.
| |
| ,,CUSTDY'---
| |
| II.
| |
| I I i I I
| |
| I
| |
| '- , . I a .
| |
| . .. i . I.
| |
| . . . I .
| |
| I I
| |
| I A
| |
| U
| |
| | |
| Health PhyescsProcedulre GPP-GGGR-RS 104-003-Attachment B-CY-00 1 Major.;'
| |
| *.. .. ... .Chain of Custody Form 20-01 Co'nfiecticut-Yankee Atomic, Power Company . .~20-01 362 Injun Hollow~Road, East Hamption, CT 06424
| |
| * ~~860-267-2556 ___ ____
| |
| Project Name: Haddam Neck Decommissioning Anialyses Requested. a s ny.t .*'~~~
| |
| Contct Nme &Phon:r.
| |
| ~ 1 W*.. ~L4 . *...
| |
| Contct Phne:Media' Rich McGrath 860-267-3573 ame Cd Sample
| |
| ~Code Container ie ~ . .
| |
| LabityStat):e STize ~;X~ . ..-
| |
| Analytical Lb(Name, tat. :**Code.&Typ- Cody',x General Engineering Lab (GEL),'2040 Savage Rd, . A...
| |
| Charleston, SC 29407, 843.556.8171 (Sarah Ko'zlik)
| |
| Priority: EI45D.0E30D.E14 D.EI7D. .
| |
| Sample Designation' Date Time _____Comment, Preservation ",..Lab Sample IaD.
| |
| f-OS t3) WG G. 4L, IL Jx
| |
| _ __ __ _WG G 4L,1IL_ _ _ _ _
| |
| __ _ _ _ __ _ __ _ WG G 4L, IL 1
| |
| __ __ _ _ _ _ __ _ _ _ WG G I4L,1IL N~OTES: P0O~ 002337. MSR~:04-1807'-LPQ awat A~NnQ Samples Shipped Via: ?n~~a oti.r Fed Ex .T~~
| |
| Requested analyses should be performned to' typical groundwater programiMDC's. El Hand CutdySaed?
| |
| I) insed By. Date/Timne
| |
| * gR~ ceivdy at/ue* utody:Seal Intact?
| |
| G(1-57/oyj . L 0 Oth~er ~..
| |
| : 3) Reamquished By . *Date/Time 4) Received By . . Date/Time . NC Bill'of Lading I.
| |
| : 5) Relinquished By . .Date/Timne 6) Received By . ~ Date/Time .. .. \.y I . . . ( C.
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| | |
| RADIOLOGICAL i.
| |
| ANALYS IS 7..
| |
| 6:
| |
| | |
| Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)
| |
| SDG MISRW04-1807 Method/Analysis Information Product: Gammaspec, Gamma,Liquid-Co-60 Recount Analytical Method: EPA 901.1 Analytical Batch Number 358134 Sample ID Client ID 118907001 MW-103S-0204-001 1200684760 Method Blank (MB) 1200684763 Laboratory Control Sample (LCS) 1200684761 118907001(MW-103S-0204-001) Sample Duplicate (DUP)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry K}
| |
| All counting sources were prepared in the same geometry as the calibration standards.
| |
| 0uality Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 118907001 (MW-103S-0204-001).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| Sample Re-preplRe-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| 7
| |
| | |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Oualifier information Manual qualifiers were not required.
| |
| M Aethod/Analysis Information Product: Gammaspec, Gamma, Filter Analytical Method: EPA 901.1 Prep Method: Filter Prep Analytical Batch Number: 358269 Prep Batch Number: 357165 Sample ID ClieritID 118907002 MW-.-103S-0204-001-filter 1200685054 Meth.od Blank (MB) 1200685056 Labo ratory Control Sample (LCS) ' '-
| |
| 1200685055 1189 07002(MW-103S-0204-001-filter) Sample Duplicate (DUP)
| |
| SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 10.
| |
| Calibration Information:
| |
| Calibration Information ''
| |
| All initial and continuing calibration requirements have been met: ' ' '
| |
| Standards Information '
| |
| Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards. ' ' '
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume in this batch.
| |
| Designated QC The following sample was used for QC: 118907002 (MW-103S-0204-001-filter).
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| 8'
| |
| | |
| Sample Re-preplRe-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| Miscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| qualifier information Manual qualifiers were not required.
| |
| Mlethod/Analysis Information Product: Laboratory Composite Analytical Method: GL-RAD-A-026 Analytical Batch Number: 357177 Sample ID Client ID 118907001 MW-103S-0204-001 SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-026 REV# 9.
| |
| .Calibration Information:
| |
| Calibration Information All initial and continuing calibration requirements have been met.
| |
| Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).
| |
| Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.
| |
| Oualitv Control (OC) Information:
| |
| Blank Information The blank volume is representative of the sample volume(s) in this batch.
| |
| Designated QC None of the samples were designated for QC analysis.
| |
| QC Information All of the QC samples met the required acceptance limits.
| |
| Technical Information:
| |
| Holding Time All sample procedures for this sample set were performed within the required holding time.
| |
| Preparation Information All preparation criteria have been met for these analyses.
| |
| 9
| |
| | |
| Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.
| |
| IMiscellaneous Information:
| |
| NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. An NCR was not generated for this SDG.
| |
| Additional Comments Per instructions sample 118907001 (MW-103S-0204-001) was filtered and prepared for analysis via gamma spec.
| |
| The sample was filtered using a 47mm 1.5 micron borosilicate glass fiber filter.
| |
| Qualifier Information Manual qualifiers were not required.
| |
| Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless othervise noted in the analytical case narrative.
| |
| Review Validation:
| |
| GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.
| |
| The followving data validator verified the information presented In this case narrative:
| |
| Reviewer
| |
| .7 .
| |
| I 10 '
| |
| | |
| SAMPLE DATA
| |
| | |
| ==SUMMARY==
| |
| | |
| 11
| |
| | |
| LABRATRIES LL GENEAL EGINERIN
| |
| ,GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Coinpany: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 Report Date: August 24,2004 Contact Mr. Dave Keefer Project: -Quarterly GroundwaterPO 002337 Page 1 of I Client Sample ID: MW-103S-0204-001 Project: YANKOO3O4 Sanple ID: - 118907001. ClientAD: YANKOOl Matrix: Ground Water Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date: 28-JUN-04 Collector Client Parameter - Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammaspec, GammaLiquid-Co-6ORecounr Cobalt-60 10.1 +1-2-56 0.967 +/-2.50 2.09 pCi/L CAM108/21/04 1300 358134 1 Solid Preparation LaboratoryComposite he foowing Prep Methods were performed Method Description Analyst Date Time Prep Batch GL-RAD-A.026 Laboratory sample composite MiMI 08/13/04 1600 357177 The following Analytical Methods were performed Method Description 1 EPA 901.1 2 GOLRAD-A-026 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| -1BDFlag for results below the MDC or a flag for low tracer recovery. I E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.: -
| |
| * J Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.'
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit. -
| |
| Ul Uncertainidentificationforgammaspectroscopy. -- -.
| |
| X Lab-specific qualifier-please see case narrative, data surmmary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| KThe above sample is reported on an 'as received" basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozilk.
| |
| Reviewed by 7-
| |
| - 12.
| |
| | |
| LLC GENERAL ENGINEERING LABORATORIES, 1.GENERAL ENGINEERING LABORATORIES,' LLC 2040 Savage Road* Charleston SC 29407 - (843) 558-81 71 - www.gel.com Certificate of Analysis Company: CYAPCo Address: Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut 06424 *Report Date: August 24,20O4 Contact Mr. Dave Keefer Project: Quarterly Groundwater PO# 002337 Page 1 of I Client Sample ID: MW-103S-0i04-00l-filter
| |
| * Proiect: YANK00304 Sample ID: 118907002 Client ID: YANKOOl Matnx: Filter Vol. Recv.:
| |
| Collect Date: 24-JUN-04 Receive Date 28-JUN-04 0-11-tr-
| |
| * lan Parameter Qualifier Result Uncertainty LC TPU MDA Units DF AnalystDate Time Batch Mtd.
| |
| Rad Gamma Spec Analysis Gammarpec Gamma, Fiter Cobalt-60 U 0.680 +1-2.55 0.940 +1-2.50 2.04 pCi/Filter Nf-ll 08&21/04 1259 358269 1 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch FilterPrep FilterPrep AFI 08113/04 1600 357165 The following Analytical Methods were performed Method Description 1 EPA 901.1 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| The above sample is reported on an 'as received' basis.
| |
| This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Sarah Kozlilc.
| |
| Reviewed by 13
| |
| | |
| QUALITY CONTROLK:
| |
| -DATA-14
| |
| | |
| GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com I
| |
| QC Summary ReDort Date: August 24,2004 Client: CYAPCo Page 1 or 2 Haddam Neck Plant 362 Injun Hollow Road East Hampton, Connecticut
| |
| | |
| ==Contact:==
| |
| Mr. Dave Keefer Workorder: 118907 Parmname NOM Sample Qual QC Units RPD% ' REC% Range AnIst Date Time Rad Gamma Spec Batch 358134 QC1200684761 118907001 DUP Cobalt-60 1I.1 9.70 pCi/L 4 (0%- 100%)7AMI 08/2210411:31 Uncert: +/-2.56 +/-6.18 TPU: +1-2.50 +/-6.05 QC1200684763 LCS Cobalt-60 700 762 pCiUL 109 (75%-125%) 08/22/04 11:32 Uncert: +/-70.6 TPU: +1-69.2 QC1200684760 MB Cobalt-60 U 0.519 pCi/L 08/21/04 13:01 Uncert: +1-1.17 TPU: +1-1.15 Batch 358269 QC1200685055 118907002 DUP Cobalt-60 U 0.680 U 0.369 pCi/Filter 59 (0% - 100%) MJHI 08122104 11:36 Uncert: +/-2.55 +/-1.99 ''
| |
| TPU: +/-2.50 +/-1.95 QC1200685056 LCS Cobalt-60 280 283 pCi/Filter 101 08/22/04 11:48 Uncert: +/-30.0 TPU: +/-29.5 QC1200685054 MSB Cobalt-60 U -0.131 pCi/Filter 08/21/04 12:59 Uncert +1-1.13 TPU: +/-1.11 Notes:
| |
| The Qualifiers in this report are defined as follows:
| |
| B Target analyte was detected in the sample as well as the associated blank.
| |
| BD Flag for results below the MDC or a flag for low tracer recovery.
| |
| E Concentration of the target analyte exceeds the instrument calibration range.
| |
| H Analytical holding time exceeded.
| |
| I Indicates an estimated value. The result was greater than the detection limit, but less than the reporting limit.
| |
| U Indicates the target analyte was analyzed for but not detected above the detection limit.
| |
| UI Uncertain identification for gamma spectroscopy.
| |
| X Lab-specific qualifier-please see case narrative, data summary package or contact your project manager for details.
| |
| h Sample preparation or preservation holding time exceeded.
| |
| 15
| |
| | |
| Appendix E Rank Order Plots for the March and June 2004 Sample Events
| |
| | |
| Appendx E1 March 2004 Rank Trerd Resudts 2-sigan Reqd Cono. WU MDC MDC Allquot Rank Wel tD Nudide (DCULI) pCI) (KCA) (0CUL) Lab Flag Voene L) Order MWIIOS GrossAlpha -0.164 0.582 1.33 - 3 U 0.15 1 MWIOOS GrossAlpa -0.007 125 2.8 3 U 0.15 2 MWtOCO Goss Alpha 0.187 0.453 0.952 3 U - 0.15 3 MWI14S GrossAlpha 0217 1.07 1.79 3 U 0.15 4
| |
| .Ia1O2S GrossAlpha 0.245 0.731 1.5 3 U 0.15 5 MWI12S GrossAlpha 0259 0.488 0.98 3 U 015 e MWIOIS GrossAlpha .3tt 0.515 0.977 .3 U 015 7 MWIOSS GrossAlpa 39 . ,0SS1 1.11 3 U 0.15 8 MWIO7S GrossAlpha 0.392 0.37 128 3 U 0.15 9 MWIO6S (5W.) Gross Apa 0.53 1.01 1.tS 3 U 0.15 10 MW1U3S Gross lpAk 0.542 0.983 1.93 3 U 0.15 1t1 kWIo9S GrossAlpa 0.571 o.784 1.37 3 U 0.15 12 MWI24S Gmss Alpht 0.82 0.833 1.81 3 U 0.15 13 MW122S GrossAlpha 0.7t 0.88 158 3 U 0.15 14 MWIIIS GrsAlpha 0.731 o0509 o.78 3 0.15 15 MWI2sS GroswAlpha o.s8o O 122 3 . U 0.15 18 4ll4SDupltceReph GrossAlpha 12 IM 2.85 3 U 0.15 17 MWIIT7S GrssAlpha 1.21 tA. 2.97 3 U 0.15 18 MwIO4S GrossAlpha 1.25 0.718 0.998 3 0.15 19 MWIO7D Gross Aipha 1.33 0.752 1.09 3 0.15 20 MWIISS GrossAlpha !1A2! 1.09 1.e7 3 U 0.15 21 MuW103S GrossAlpha 1.53 0.879 1.14 3 0.15 22 MWIOSs GrOSS Alpha 1.54 O.935 131 3 0.15 23 MW105S GrossAp 1.6 1.78 1.2 3 0.15 24 MWEOF2 Gross Alpha 1.73 1.05 155 3 0.15 25 MWI06D (Sol.) Gross Alpha 1.74 0.984 1.5 3 0.15 28 MW114SDrL,8cate Gross Alphai-1.79 1.41 1.91 3 U 0.15 27 MWI0Ss (Sot) Gross Alpha 2.42 .4 0.877 3 0.15. 28 MWI1OO Gross Alpha 2.59 0.795 0.949 3 0.15 29 MVI050(Sol.) Gross Alpha 2.7 0.811 0.978 3 0.15 30 MW1080 Gross Alpha 2.75 0.77 0.89 3 0.15 31 MW123S Gross Alpha 4.1S 1.49 1.98 3 0.15 32 MWI03D GrossAlpha 5.19 -S.. 1.1_. 1.04 3 . 0.15. 33 MW122D GrossAlpha 6.2 128 122 3 0.15 34 MWIOID Gross Alpha 6.2 1.38 125 3 0.15 35 MWI09O Gross Alpha .95 1.15 0.782 3 0.15 38 MWIItD GrossAlpha 7.07 1.51 1.5 3 0.s 37 MNWI2D GrossAlpha 11.3 2.18 2.33 3 0.15 38 fr 38 38 38.
| |
| Average: 2.1262 1.0120 1.4455 Sdev 2.5250 0.3917 0.5659 Sdev 119% 39% 39%
| |
| MIX .0.1840 0.4530 08780 Mao 11000 ztsoo2 .9700 Medarl 12900 0.9490 12950
| |
| | |
| Appendix El March 2004 Rat Trend Results 2-slorna ReqtAred We 10 Ndlidt (VCmt)
| |
| TPU (POl&
| |
| MDC (pCbt)
| |
| MDC (pCLI Aiqut Lab Ftao Voksnme( 'U aC Btank GrossA4A 0121 0.505 ic0 3 U 0.15 aC Blan G Wi Aoss 0.119 01372 0713 3 U 0.15 0C SBat Gross Aia -0.0321 0.484 112 3 U 0.15 3 3 3 Average: 0.0893 0.4537 0.9743 Sdev. 0.0878 0.0715 02268 Sder 127% 18% 23%
| |
| -0.0321 0.3720 0.7130 Maxc 0.1210 0.5050 1.1200 Rank Results for March 2004 20
| |
| * 15 U
| |
| * Gross Alpha 010 -Zero Mean 0
| |
| - Sigma As 5 +2-SAgma
| |
| -Ave. MDC-u 'O 10 . - Me
| |
| -5 0 10 20 30 Rank Order Rank Results for March 2004 2
| |
| 0c 0.5
| |
| : a. iITTTl*I~f4U44ll4- 1 -Zero Gross Alpha Mean II[ MIT I i IIII'I Sigma 0 jjtjjlt1t+2-Sigma
| |
| -Ave. MDC
| |
| -1.5 0 5 10 15 20 25 30 Rank Order
| |
| | |
| MaN 20e4 Ra* TreW Result.
| |
| 2-sigma Required i Con. TPU MOC WC MDquo Rari Wen ID Nucide (oClA) (pCVUL (pCVlQ (pDlt) Lab Flog Vol- (L) Order MWI 2S GrossBeta '0.778 1.17 2.38 4 U 0.15 1 mWIOOO Gross Beta 1.21 2.4 4 U 0.15 2 MW107S Gross Beta 1.5 0.778 1.3 4 0.15 3 MWI1ID Gross Beta 1.7 0.858 1.51 4 0.15 4 mWIO1S Gross Beta 1.87 o.m 1.3 4 0.15 5 Mwilos Gross Beta 1.8 0.7e5 127 4 0.15 a MW102S Gross Beta 2.26 0.837 1.38 4 0.15 7 MW1O0S Gross Beta 2.63 1.2 2.21 4 0.15 8 MWI0sD Gross Beta 3.56 0.707 0.94s 4 0.15 9 MwtOs (Sot.) Gross Beta 73 0.729 0.977 4 M.1s 10 mw1O4S GrossBeta 4.11 148 2.59 4 0.15 11 MWiO6D Gross Beta 4.12 0.697 0.847 4 0.1s 12 MWIOOS Gross Beta 423 1.78 328 4 0.15 13 Wills Gross Beta 465 1.41 2.37 4 0.15 14 MWI24S GrossBeta 5.12 1.05 1.44 4 0.15 15 MWII7S Gross Beta 5.41 1.8 323 4 0.15 18 MWEOF2 GrossBeta .48 1.61 2.73 4 0.15 17 MW107D Gross Beta 5.79 o.s 1.15 4 0.15 18 MWI03D Gross Beta 600 0.881 1.08 4 0.15 19 mW10o6(SoI.\ Gross Beta 821 0.884 1.04 4 0.15 20 MW122S Gross Beta S64 1.17 Is 4 0.1s 21 mW122D Gross Beta S.64 0.977 .1.12 4 0.15 22 MWI02D Gross Beta 5.9 1.19 151 4 0.15 23 MWIiOD
| |
| * Gross Beta 7.14 1.17 1.48 4 0.15 24 MWI09D GrossBeta 7.6 0.88 0.892 4 0.15 25 MwIISs GrossBeta U62 129 1.5 4 0.15 28
| |
| :MW12SS GrossBeta 5.89 1.24 1.35 4 0.15 27 MwIt0s Gross Beta .3 1.02 1.0 4 0.15 28
| |
| .-Mwtom Gros 1et U 123 1.16 4 0.15 29 MWo6 (ScOL) Gross Beta 14.1 1.32 1.4 4 0.15 30 MWI23S GrossBeta 14.7 1.54 1.49 4 015 31 MWI13S GrossBeta 153 2.07 2.73 4 0.15 32 MW14SDuplcate GrossBeta 15. 1.8s 151 4 0.15 33 MWI14S GrossBeta .1. 1.55 -1.4 - 4.0.1.5 34 MWI14SDuplicateReplicate GrossBeta 20.S 1.85 1.62 4 0.15 35 MWI03S Gross Beta 27 2.43 2.58 4 0.15 38 MW105S Gross Beta 192 3.82 1.08 4 0.1S 37 frW105S(SoL) GCrssBeta 203 3.9 1.02 4 0.15 38 rC 38 38 . 38 Aere: 17.6847 1.34'5 1.6289 Sdev: 43.3987 0.7210 0.8712 Sdev 245% 53% 41%
| |
| MNr o07780 0.6970 0.8470 Max: 283.00 3.900 3.2808 Medam: .1350 . 1.1950 1.4208
| |
| | |
| Apperdx E.1 March 2004Rank Trend Resutit 2-sigma Reqtired Cone. TPIJ MDC MDC uo Wel 1D Nucke IDCVLI (DCL~j (DCL'L (pM1 Lob Flstg Vokine (IU "I,,
| |
| 0Cetank Goses Beta 40915 0.818 1.48 4 U 0.15 cCstan Goses Beta 0231 0.514 0.948 4 U 0.15 OC Slr Gows Beta -0.0634 1.14 2.43 4 U 0.15 It 3 3 3 Average: .0.2471 0.58 1.0120 Sdev. 0.5978 0.3359 0.7538 Sdev. -242%A 44% 47%
| |
| Mire .091 50 0.5140 0.9460 Max 0.2370 1.1400 2.4300 Rank Results for March 2004 250 q 200
| |
| * Gross Beta
| |
| -9150 0
| |
| C -Zero MeCan
| |
| ~ 100-2-Sigma
| |
| +2-Sigma 0C 50 C --.)- * -Ave. MDC00**
| |
| 0
| |
| -50 0 10 .20 30 Rank Order Rank Results for March 2004 10
| |
| 'Gross Beta C -Zero Mean
| |
| - Sigma C n I+2-Sigma
| |
| -Ave. MDC
| |
| -5 0 10 20 Rank Order I-_
| |
| | |
| APperdE.l Mach 2004 Rank Trend RedSS 2-sma ReqLed Cono. TPU MDC MDC Afqutc Ratk Wd OD Nuido- (PCLt) (pX) (pOCt) (PM) Lab Flag Vodune (L) O0der Mw1os 1S-3 - 157 is9 271 -400 U I MWIO8S FK3 0 18O 263 400 U 2 MW123S H-3 27.5 150 249 , 400 U 3 Mw&113s 3 30.5 157 260 400 U 4 MWIo0s H-3 30.8 169 279 400 U 5 MW112S H-3 32 165 272 400 U a MW122D 1-3 32.9 180 298 400 U 7 MW117s H-3 33.3 171 - 283 400 U 8 MW100D H-3 81.5 181 282 400 U 9 MWEOF2 13 8z3 183 285 400 U 10 MWi11S 143 63.2 18s 269 400 U II MW1OID H-3 91.3 171 278 40D U 12 MwI0Os 143 942 187 287 400 U 13 MWI22D Replate K3 945 177 285 400 U 14 MWt07s -3 VL.s7n 190 291 400 U 15 MWI04S H-3 285 183 269 400 18 MW10os (So.) . -3 405 189 285 400 17
| |
| * MWI06S Repcate H-3 494 194 283 400 18 MW105s "a3 542 202 271 400 19 MW1O7D -3 'T32 222 288 400 20
| |
| * MWI22S H-3 750 220 283 400 21 MWIOSO (Sol.) H-3 802 213 282 400 . 22 MW105D 13 953 227 270 400 23 MWiO6D (So.) 13 1000 235 283 400 24 MWI03s F-3 1990 228 258 400 24 MWI06D H-3 1110 243 287 400 28 MWI14S - -3 1350 280 292 400 - 27 MWI24S -3 1530 283 283 400 28 MWII4SDuptcate -3 157 288 284 400 29 MwiIos H-3 2050 287 282 400 30 MWu2sS H-3 2350 311 298 400 31
| |
| , MWI09D 13 4550 393 290 400 32 MWI02D F-3 4940 411 298 400 33
| |
| ! MW105S - K3 5520 422 273 400 34 MWI*ss 14-3 8740 432 290 400 35 MW10s (Sol.) H-3 S8O * .434 275 400 38 MW10D -3 8890 424 275 400 . 37 MWI02S -3 6740 489 298 400 38 MW103D0-3 12000 58o 259 400 - 39
| |
| . 39 - - 39 .39 Average: 1771.5 251.6 278.5 Sdev: 2e5827 109.87 12.52 Sdevw 150% 44% 5%
| |
| Mur e10 150 249 Mac 12000 580 298 Medar 732 213 275
| |
| .. - . ,1
| |
| | |
| it-AppendiEl Marc 2004 RankTrendResUIt 2-sigma RequWred Cogi_ TPU MDC MDC Weld Nudde (MUL I(eCLt) (CaMI (rCLc Labflao VduMe I QC 8strk 1-3 .129 183 292 400 U aC BarI* 14-3 -31 154 264 400 U e 2 2 2 Average: . -8.000)0, 15W5000 278.0000 Sdev: 692965 6.3640 19.7990 Sde: -87% 4% 7%
| |
| Mkc -129.0 154.0 264.0 Mar -31.0 163.0 292.0 Rank Results for March 2004 14000 12000 10000
| |
| * H-3 e 8000 -Zero Mean
| |
| * 6000 + Sigma c 4000 +2-Sigma C 2000 p -Ave. MDC
| |
| -2000 0 10 20 30 40 Rank Order Rank Results for March 2004 1000 800
| |
| ° 600 *H-3 e . -Zero Mean 3 400 Sigma
| |
| +2-Sigma 200 -Ave. MDC
| |
| -200 0 5 10 15 20 Rank Order J11
| |
| | |
| Apperix El1 March 2004 Rank Trend Results 2-sigma Reqt*ied Cone. W MDC MDC MAqul Rank Wel ID Nuckdeo O'1J (oClt1 - (pCkt) (oCULt Lab MFlag Volkne (t) Order MWI03S C-14 11.9 99.4 .i70 200 U 0.01 I MW1000 (Sol.) C-14 164 87.7 150 200 U 0.01 2 MWi13D C-14 31.3 8a&I 150 200 U 0.01 3 MWtOSD C-14 33.9 e8 .151 200 U 0.01 4 MW1O4S C-14 75 89.7 151 200 U 0.01 5 mW105S C-14 83.5 91 t152 200 U 0.01 6 MW1OS (Sol.) C-14 e5.6 90.1 '151 200 U 0.01 7 UW106D C-14 85.7 902 151 200 U 0.01 8 MwIOss C-14 68.1 90.5 .151 200 U .O01 9 MW106D (Sol.) C-14 90.4 90.8 151 200 U 0.01 . 10 MWlOsDReplcate 14III 184 200 U 0.0 11 AWIOSS(Sol.) C-14 92.3 I."40.3 152 200 U 001 - 12 i 12 12 .12 Average: 72.3107 92.4e67 1551333 Sdev 40.9678 .5s594 10o5s87 Sdev 57% 7% 7%
| |
| MWC 11.900 87.700 150.00o Max: 140.00D0 111.0000 184.0000 Meda: 84.s500 90.3500 151.0000 2-sIgma Required Con- WTJ MDC MDC Atl"l Wen ID Nudide (cCL1.) (DCLI.) (pCl) (pOtL) Lab Flag Voltue CL)
| |
| QC Blar C-14 3.31 98.9 168 200 U 0.01 n '1 1 1 Average: 3.3100 9s.900c 188.0000 Sdev -
| |
| MNn 3.3100 98.9000 168.0000 Max: 3.3100 9t9.9o 1e8.0000 Rank Results for March 2004 250
| |
| .150 200 I I 4 .0 4 IL)* 100I C 50 -Zero Mean 0 o-.2-Sigma c -50 +2-Sigma
| |
| -100 -Ave. MDC 0
| |
| .-150
| |
| -200
| |
| -250 0 5 10 Rank Order
| |
| | |
| a-Appenx E.1 Marc 2004 Ra* Trerd Rests 2-sigms Requird ConO TPU MDC MoC Aliquot Ra*
| |
| Wel ID Ndde fPCVLI (pe/LI (P0/L) (PCVLI Lab Flag Vdxe (U Orde MW102D MhI,4 -212 1.5 Z98 50 U 2 1 MWiClO Mn-54 -1.97 Z22 345 50 U 2 2 MW101D Mn-54 .11.88 Zo. 349 50 U 2 3 MW110s Mn.54 .1.24 1.44 Z38 50 U 2 4 MWEOF2 Mn.54 -096 Z23 3.8 50 U 2 5 Mw1o9s Mn54 -0.927 1.83 3.19 50 U 2 8 MWIO4S . Mn54 -0.902 125 Z12 50 U 2 7 MWIOBS(SoL) M-4 .0.868 1.59 2.7 50 U 2 8 MW10SS Mn-54 40.694 1.11 1.89 50 U 2 9 MWl06SRepncate Mn-54 .0.852 1.87 3.32 50 U 2 10 MW1O3S Mn-54 -08 1.39 2.34 50 U 2 11 Mwl14souvkca Mnr54 -0.381 2.81 4.71 50 U 2 12 MWI14S Mn.54 -0.377 2.35 4.19 50 U 2 13 MWI02S Mn-4 -035 Z04 152 50 U 2 14 MW103D Mn-54 .0290 1.3 222 50 U 2 15 hMwliss M.54 -0278 1.72 3.05 50 U 2 18 MW125S M-4 -228 1.51 2.82 50 U 2 17 MW124S Mn.54 -0.218 1.92 3.41 50 U 2 18 MlWoss(Sol.) Mn.4 4211 1.22 211 50 U 2 19 MW107D Mn-54 4117 228 4.03 50 U 2 20 MWIo7S Mn-54 4108 .Z15 3.93 50 U 2 21 MW122ORepkato Mn-54 -. 0531 1.24 Z12 50 U 2 22 MW109D Mn54 4.0433 1.12 1.96 50 U 2 23 MWil7S Mn-54 -0.03 2.5 3.89 50 U 2 24 MWI12S Mn.54 0 0 3.84 50 U 2 25 Mwio0s Mn-54 0.072 1.05 1.88 50 U 2 20 MW10CS Mn.54 018S 1.78 328 50 U 2 27 MW106D Mn-54 0.2f3 202 a7 50 U 2 28 MWiO5D(Sot) Mnr54 055 1.13 1.95 50 U 2 29 MW108S Mn-54 0.379 1.78 3.3 50 U 2 30 MWio06 Mn-.54 0.427 1.2 214 50 U 2 31 Mwi1ls MI-54 0.442 1.82 3.35 50 U 2 32 MW1003 (Sol.) Mn.54 0.569 1.47 2.32 50 U 2 33 MW11oS Mn.54 0.725 V11 3.87 50 U 2 34 MW122D Mn-54 1.18 1.68 3.05 50 U 2 35 MWIO0S Mn454 1.78 3.49 4.44 50 U 2 3#
| |
| MWI23S Mn-54 1.78 3.49 4.44 50 U 2 37 MWI22S Mon54 C 2.03; 1.81 2.2 50 U 2 38 Mw11s3s mn54 f2.e4<;- 2 2.83 50 U 2 39 f 39 39 39 Average: .0.038 1.7854 3.0715 Sdev: 1.0053 0.8391 0.8138 Sdev -1576% 38% 26%
| |
| Mirc -12 0 1.88 Ma: 2.84 3.49 4.71 Medarc 4117 1.81 3.19
| |
| | |
| Appendx E.A March 2004 Rark Trend Resdts 2-sgrma Req*ed Cof. TPU - WDC MDC Aistq Well ID Nudibe (fPaI IpCU) LI)(pCUL) Lab Flag Volwme [L) tpCJA)
| |
| QCabk MOtt .0.717 1.10 1.98 50 U 2 CC St3ank Mt-U 0.e85 1.85 305 50 U 2 rc 2 2 2 Average: 40.010 1.500 25150 Sde. 0.1188 0.4879 0.7568 Sdev: *15% 32% 30%
| |
| Mti 40.8850 1.1600 1.t380 max 40.7170 1.8598 3.0500 Rank Results for March 2004 10 5.
| |
| o i i i* Mn-54 7M1 .I -Zero Mean
| |
| ° Sigma C + 2-Sigma I. -Ave. MDC co .5
| |
| -10 0 10 20 30 Rank Order
| |
| | |
| A_
| |
| Appendx El March 204 Rank Trend ResLfs 2-sima Reqired Cons TPU MDc MDC "t Rank Wed ID Nudkl (sCUL) (PClA) (PCVt) (VAtL) Lab Fag Vodan (L Order MWIOSS(Sd.) FoSS -45.7 .91 1725 25 U 0.55 1 MW1086 Fe-55 -442 9U8 V88 25 U 0.55 2 MWtO5D Fe-55 -43.7 7.97 6.85 25 U 0.55 3 mW104S FeoS -384 112 10.3 25 U 0.55 4 MW105D (So.) Fe-55 -30.1 9.07 6.99 25 U 0.55 5 MWIO6DO(SOd.) Fe455 -272 10.9 8.51 25 U 0.55 a UWio5S Fe-55 -22.9 10.1 7.77 25 U 0.55 7 MWIOSS(SOI.) Fe-55 -15.5 11.8 9 25 U 0.55 8 MWtOBO Rep2kale Fe-55 -7.54 15.9 14.8 25 U 0.55 9 MW103D Fo5s 2.59 13.8 11.7 25 U 055 10 MW1OS8 . Fe-55 7.32 11 842 25 U 0.55 11 MWI03S Fo-55 9.53 12.7 101 25 U 055 12 it 12 12 12 Average: -21.3107 11.0942 91942 Sdev: 20.4318 Z2340 2.2341 Sdev: -98% 20% 24%
| |
| Mis 45.7 7.97 6.85 Maxc 9.53 15.9 14.8 Medam -25.05 10.95 8.875 2-sigma Required Conr. WTi MWC MDC Alat We4ID Nuclide (iCa) (PCVQ CCL) (pCVL) Lab Fag Vod- (L)
| |
| CCBlank Foe55 -17.7 14.8 124 25 U 0.55 re: I I I Average: -17.7000 14.8000 12.4000 Sdev - -
| |
| Mh: -17.7000 14.8000 12.4000
| |
| ?Aic -17.7000 14.6000 12.4000
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| | |
| APP4x EA Marci 2004 Rank Trened Resfts 24Ignia Reqtdred Conc TM MDC MDC Aklqut Rark We* ID NucIde (oCUt) (DCVQ (pClL) (pCIIQ Lab Flag Vdw*e () order MWI4S Co-6O 43.31 3.38 4.49 -25 U 2 1 -
| |
| MWI17S Co-CO -1.42 2.34 401 25 U 2 2 MWIIOD CO-CO .1.34 2.32 3.89 25 U 2 3 MWI25S Co-CO .0.94 15 2.54 - 25 U 2 4 MWI05D Co-CO 4939 1,42 2.42 25 U 2 5 MW114SDucstO CO-CO .0885 2.48 4.31 25 U 2 8 UW124S Co-CO .0.654 2.19 3.89 25 U 2 7 IWFNI06S Co-C .0592 1.94 3.41 25 U 2 8 MWI12S Co-CO .0.535 '2.3 4.17 25 U 2 9 MW1225 Co-CO .0.493 189 3.4 25 U 2 10 WIto1D Co-C .0.492 123 2.13 25 U 2 11 kW!122D Repcae co-O .0.4b5 12 2.07 25 U 2 12 MWI13S Co-CO .0.406 2.22 399 25 U 2 13 MWI07S Co-CO .0.18 2.3 4.18 25 U 2 14 MWIOCSReplcate Co-CO .0.0143 1.74 3.24 25 U 2 15 MWIosS (So.) Co-6O 0 2.4 227 25 2 18 MWIOCOD co-C 0.0719 -1.7 3.37 25 U 2 17 MWIOOD Co-O 00743 122 227 25 U 2 18 MWI02D Co-SO 0.158s 2.13 4.05 25 U 2 19 MWIO4S Co-60 0247 ' 129 ' .32 25 U , 2 20 Mwi1os Co-C 0291 ZC02 3.86 25 U 2 21 UWt02S Co-O 0.387 2.12 4.02 25 U 2 22 MW1Is Co-CO 0.3e7 224 37S 25 U 2 23 MWIOOS Cco-O 0.389 1.9 3.81 25 U 2 24 MWIoss Co-CO 0423 128 Z3 25 U 2 25 MWIO3O Co-CO 0.541 1.48 2.74 . 25 U 2 28 MWIos(sot.) Co-CO oet 1.55 2.81 25 U 2 27 MW1O6D(Sol.) Co-O. 0.644 1.45 Z7t 25 U- .2 28 MWIOSD(Sol.) CoCo0 0.783 1.13 5 .41 25 U 2 29
| |
| -WI0O7D C Co-SO. 0.731. 1z35 4.49 25 U 2 30 MWIOID Co-CO 0.85s 227 4.28 25 U 2 31 MWEOF2 Co-60 0.925 2.2 4.27 25 U 2 32 MWt220D Co-CO 1.19 1.94 3.93 25 U, 2 33 MW1t5s Co-CO 1.28 1.88 3.83 25 U 2 34 MWI03S CoC60 1.43 1.55 2.92 25 U 2 35 MWIosS Co-CO Cre'J1.74 1.88 3.79 25 U 2 36 MWIoIS Co-CO z94 4.58 4.15 25 U 2 37 MW123S Co-CO z94 4.58 4.15 25 U 2 38 MW1OSS Co-CO 3.23 0os 1.93 25 2 39 tc 39 . 39 39 Average: 0.2451 Z0374 3.3862 SdevC 12300 0.7550 0.817t sdev 502% 37% 24%
| |
| Mift .3.31 1.13 1.93 Maxc 3.23 4.58 4.49 Meclar 0247 1.94 3.78
| |
| | |
| Apperdx E1 Marh 2004 Rar* Traed Resmls 2-slgma ReqLred
| |
| ' TPU MO MoC A" Well tO Nudide (pCIL) (DCat) (pCLI8) (dlt) Lb Flab Vokvno (L) oC Bbl" Coe60 0.76 1.15 2.2 25 U 2 QC Bank Co-eo 0.485 2.o0 3.98 25 U 2 2 2 2 Average 0.25 1.6050 3.000 .
| |
| Sdev 0M1945 0.e435 12445 Sdev 31% 40% 40%
| |
| Mh: 0.4850 1.150 22000 Max: 0.70 2.0600 3.9600 Rank Results for March 2004 10
| |
| -Mill Co-60 a
| |
| 0i -Zero Mean C
| |
| s5o - II.- il .
| |
| Sigma
| |
| +2-Sigma a il -Ave. MDC
| |
| -10 0 10 20 30 Rank Order
| |
| | |
| Apperdxcl1 March 2004 Ra* Tresd Rest 2-signa Reqrired Conc. TPU MDC MDC AqtUD Rank Well tD Nuclde (PCVa) pCVaj (pCVL) (pCU) Lab Flag VobkweCL) Order MWIo3D Ne-63 -5.23 3.59 S41 15 U 0.55 , 71 MWl0o6DRekate N- -3.95 .384 a 8.43 15 U , 0.55 , 2, MWI05D N- -336 5j4 9.87 15 U 0.55 3 MW105D (Sol.) Ne-63 -333 2.72 4.83 15 'U 0.55 4 MWI04S NM -323 324 5,71 15 U 0.55. ,.5 MWI06S NM-3 499 325 5.72 15 .U 0.55, 8a MWIOSS(SoI.) Nn3 218 ',2.92 5.11 15 U 0.55 ' 7 MWI06D 1NM-3 -0 3.79 8S.1 15 U O.55 ,8 MWI0tS - N- .1.42 3.17 5.51 15 U 0.55 *9 MW1OBD(Sol.) NM3 0.512 2.56 4.42 15 U 0.55- 10 MWIOS (SCl.) 1-63 ,0 3.18 542 1I U O5 1 MWI03S N1-3 0.483 3.77 848 15 U 0.55 12 1
| |
| 12 12 12 Average: -23149 3.4458 60250 Sdev 1.7031 0.76U 1.4is5 s . .74% 22% 22%
| |
| Mln: .5.23 2.5 4.42 Max: 0.483 a54 9.87 Medlan: Z575 3245 5.715 2-sigra Reqored CWnc. TPU M1rDC MDC Aquot Wen 10 N- ade (OM)
| |
| Coc) (C) (cDM) Lab Fla* Vokie (LI C
| |
| ocIank Nt-63 -3.26 ,3.44 8,06 15 U 0.55 n: I - I Average: .3.280 3.4400 6,0800
| |
| - Sdev - - ' '
| |
| Sdew. I
| |
| * Miro -3.2600 a4400 8.0600 Max: d2600 a4400 8.06oo Rank Results for March 2004 10 iG 5.
| |
| -Zero Mean c:
| |
| 0 I I J-2-Sigma ll ° .'+2-Sigma
| |
| ° -10 11 -Ave. MDC 0 5o 0 5 10 Rank Order
| |
| | |
| AL-Appldx El March 2004 Rank Trend Resl 2-sigra Reqtked Consc TPU MDC MDC Awquot Ra-*
| |
| Wet 10 Nudide (fDC/ (OCa) (oCt) (fCrL) Lab Fb V ine (L) Order MWI1oS Sr-go -0.753 0.648 1.7 2 U 0.4 1 UWIoSs Sr-go 4.324 0.279 0.887 2 U 0.4 2 MW122DRer8cate Sr-go 40239 0445 1.15 2 U 0.4 3 MWI020 St-go .0213 0.434 1.11 2 U 0.4 4 MWI030 Sr-go 4.0758 0.298 0.815 2 U. 0.4 . 5 MW105D Sr-00 -0.0604 0.299 0.811 2 U 0.4 8 MW112S Sr-Go -0.0217 0291 0.785 2 U 0.4. 7 MW1M45 St-go 4.004U 0258 0.885 2 U 0.4 8 MWi1ls St-go 0.0142 0.307 0.788 2 U 04 9 MW124S Sr-go 0.0515 0.469 1.12 2. u 0.4 10 MW105D(Sdl.) Sr-50 0118 0.401 0.973 2 U 0.4 . 11 MWIo2S Sr-90 0.122 0.507 12 2. U 0.4 12 MWIOID Sr-90 0.168 0.497 1.18 2 U 0.4 13 MW109S Sr-G0 0.181 0475 1.11 2 U 0.4 14 MWI17S Ser-40 0.19 0457 1.09 2 U . 0.4 15 MWI07D Sr-go 0.224 OS33 123 2 U 0.4 18 MW1060(Sol.) Sr-go 0237 0457 1.05 2 U 0.4 17 MW1W7S Sr-go 0.322 0.599 1.37 2 U. 0.4 18 MWIO8D Sr-Go 0.325 0.515 1.17 2 U 0.4 19 MW113S Sre-0 dM.373,! 0354 0739 2 U 0.4 20 MWto0 Se-go 0.391 0.457 1.01 2 U 0.4 21 MWI10S Sr-go 0.438 0.539 1.2 2 U 0.4 22 MW122D Sr-G0 , 0o529-z 0.527 1.14 2 U 0.4 23 MW122S Se-GO t]0.644 0.544 1.17 2 U 0.4 24 MWM=CD Sr-GO 0.8S7 0.85 1.42 2 U 0.4 25 MWI23S Se-G0 .,;O88S. 0.551 1.13 2 U 0.4 28 MW1MS Se-90 i12iS 0.7 1.29 2 U 0.4 27 MWMt55 Se-G0 1.64 0.723 1.42 2 0.4 28 MW1O8SRepncate Sr-G0 167 0.422 0554 2 n4 29 MW106S (Sol.) Sr-go 1.68 0.842 1 2 0.4 30 MWIOMS Se-90 2.27 0.62 0.788 2 0.4 31 MW125S Sr-90 115 0.788 129 2 0.4 32 MW1145 Duicate Sr-go 3.39 a728 1.11 2 0.4 33 MW14S Sr-G0 3.92 0.793 121 2 0.4 34 MWio8S (Sol.) Sr-G0 16.5 1.43 0.72 2 R 0.4 35 MWI15S Sr-G0 91.8 34S 0.815 2 0.4 38 MW105S (Sl.) Sre-0 92.4 3.45 0.822 2 0.4 37 r 37 37 37 Average: 8.0491 0.3901 1.0543 Sdev 21.0414 0.7004 0.2449 Sdev 348% 101% 23%
| |
| MIre 4753 0258 0.554 Max: 92.4 3.45 1.7 Medam 0.325 0.515 1.11
| |
| | |
| Appentx El March 2004 Rank TrendResurts 2-stma Reqtred
| |
| - Com TPU MDC MDC Wei ID - Nmfde' tndUL (DOU (OCU¶i (0=L1 Lab Rag Vobe (M CBta QC Sr-go n.165 0.499 1.17 2 - U 0.4 QCBtank Sr4-0 -0.0411 0262 0.E89 2 .U 0.4 2 2 2 Averager O.OS2D 0.3805 0.9195 Sder 0.1457 0.1676 0.3543 Sdev 235% 44% *39%
| |
| Man: -0.0411 02620 O.6890 Max: 0.1650 0.4990 1.1700 Rank Results for March 2004 160 140 j120 rx100 4t *Sr-90 100 80 .4.. -Zero Mean
| |
| .. - . Sigma 60 60 +2-Sigma
| |
| @ 40 -Ave. MDC 0.)20 . . *:
| |
| -20 0 10 20 . 30 Rank Order Rank Results for March 2004 2
| |
| 1_5 05
| |
| * Sr-90 9 0_
| |
| = Il li TII Il1 11Uitl l11 tt I
| |
| ;~ 0.5 1.I 11
| |
| -Zero Mean 0C -05 li I- Sigma
| |
| +2-Sigma
| |
| -Ave. MDC
| |
| -1.5
| |
| -2 0 5 10 15 20 25 30 Rank Order
| |
| | |
| Aperdhf E1 March 2004 Rar* Trenr Remft 2-sigma Required Conc TPU MDC MDC Aqt(Lt Ra*
| |
| Wel ID Nulda (sK) rPCV) (vCL( (pQL) t bFisa Vone () 0 MW102S. Nb-94 .1.2r 1.9 3.1 50 U 2 I MWIOOS Nb-94 .125 1.88 3.02 50 u 2 2 MWIOD Nb-94 -1.1 1.81 3.08 50 U 2 3 MW114SOupkate Nb-94 4999 2.46 4.08 50 U 2 4 MW1C0S Nb-94 4799 121 Z15 50 U 2 5 MW12Ss Nb-94 4783 121 Z02 50 u 2 6 MWI14S Nb-94 4732 228 4.02 50 u, 2 7 MWiO4S Nb-94 4494 123 2.03 50 U 2 8 MWIOS Nb-94 -0.178 1.06 1.78 50 U 2 9 MWIOSS Recate Nb-94 0.112 1.79 &.13 5o U 2 10 MW100S Ns-94 aL129 1.88 328 50 U 2 i1 MWIO7S Nb-94 0.144 1.84 328 50 U 2 12 MWIISS Nb-94 0252 1.4 29 50 u 2 13 Mwi17S Nb-94 0.259 1.91 3.48 50 U 2 14 MW105O(Sol.) Nb-94 0274 0.985 1.71 50 . U 2 15 MW105S(SOt) Nb-94 0.27 1.09 1.95 50 U 2 16 MWI02D Nb.94 0.303 2.09 .71 50 u 2 17 MWi1os N1.94 0,432 1.84 3.04 50 u 2 is MWI22S Nb.94 0.433 1.85 3.34 50 u 2 19 MW0D90 Nb-94 0.453 1.C5 1.91 50 u 2 20 MWI24S Nb-94 0.471 1.81 3.34 50 u 2 21 MW10S NS-94 0.498 1.72 .19 50 u 2 22 UWiOSS Nb-94 0.518 0.95 1.68 50 U 2 23 MW1035 Ns-94 0.815 1.34 Z11 50 u 2 24 mW106o(Sod) Nb-94 0.881 1.77 2.31 50 U 2 25 MW122DRepkcate Nb-4 0.754 1.07 1.94 50 U 2 2S MWlO7D Nb-94 0.783 3.89 4.31 50 U 2 27 UWIO8S(So.) NS-94 0.855 153 284 5O u 2 28 MWEOF2 ,,b. 5-94 0.918 1.88 3.48 50 u 2 29 MWiOCD Nb-94 1.12 233 3.88 50 U 2 30 MWI1OD NS-94 1.13 1.92 3.57 50 u 2 31 MWi11S N-94 12 1.57 325 50 U 2 32 MWIO8O Nb-94 '- 1 1.03 1.97 so U 2 33 MW1220 Nb-94 1.58 1.88 328 50 u 2 34 MW112S Nb-94 1.83 1tt8 328 so U 2 35 MWI03D N1594 "' 18iL' 125 2.34 50 U 2 36 MWIo1S W-94 187 2.27 4A1 50 u 2 37 MWI23S N1594 1.87 2.27 4.41 so u 2 38 MWI13S 145-94 ;j2. Z4 3.39 so U 2 39 ro 39 39 39 Average: 0.4587 1.7180 Z9538 Sdew. 0.9345 0.5803 0.8018 Sdv. 205% 33% 27%
| |
| Mkx -127 0.95 1.88 Maxc Z78 3.89 4.41 Medam 0453 1.77 3.13
| |
| | |
| AppendxE l March 2004 Rark Tred Results 240m Requiredt Cc. . .WtJ . MDC MDC . Alkwl.
| |
| Wei ID Nudkle IDCUI (oclI (oCV=j (oQUkl Lob Flaa Voltd e (LI OC Blark Nb-94 -0.575 121 1.99 50 U 2 QC BlaE Nb-94 004 1.73 .17 50 U 2 n: 2 2 : 2
| |
| - Average: 0.0355 1.4700 258O0 Sdev: 0.7630 0.3B77 08344 Sdev: -2149% 25% 52%
| |
| Mn: -0.5750 1.2100 1.9900 Max: 0-040 1.7300 317CO Rank Results for March 2004 5
| |
| I. i III U
| |
| .. ,I*I ' I I I .1. II11j1ITI WW ITIIII
| |
| * Nb-94
| |
| -Zero Mean 0 11111,I11 Il 4l44l t Sigma C
| |
| 0 +2-Sigma
| |
| -0
| |
| . -Ave. MDC_
| |
| -l1l , . I. . .
| |
| -5 0 10 20 . 30 Rank Order
| |
| | |
| Appendx E.1 Mwd 20C4Rank Trend Resta 2-sigma Required Cone. TPU MDC MDC Aliquot Rank Wei ID Nudide (pClt) (PClM) (cuL) (poO) Lab Flag Volune (Ll Order MW105D To-g -4.95 5.85 10.3 15 U 025 1 MWIO3S TC-99 -3.57 8.25 10.9 15 U 025 2 MWt0OS(Sol.) TC-99 .320 5.7 9.94 15 U 025 3 MWIO6S (Sol.) - TO-99 -3.25 5.57 9.71 15 U 0.25 4 MW1050 (Sol.) Tc-99 -Z72 5.81 10.1 15 U 0.25 5 MW1060 Tc-99 -Z47 5.82 10.1 15 U 0.25 6 MWtC5S (Sol.) Tr-99 -1.88 528 10.9 15 U 0.25 7 MWIO5S Tc-99 -1.5 5.92 10.2 15 U 0.25 8 MWIOSS To-99 -0.923 8.45 11.1 I5 U 0.25 9 MWIO4S TO-99 -0.45 0.29 10.8 15 U 0.25 10 MWI03D TO-99 0 8.98 11.9 15 U 0.25 11 MWIOC0Repllcale Tr-99 0.71 5.68 9.87 15 U 0.25 12 r 12 12 12 Average -2.0203 8.0487 10.46e3 Sdev: 1.6577 0.4057 0.6802 Sdev -8 7% 8%
| |
| Mle -4.95 5.57 9.87 Mac 0.71 0.90 11.9 Medlarr -2.165 5.885 1025 2-sigma Reqcired Conc TPU MDC MDC Mqut Wed ID NudIde (rCaU (1prA (pClL) (eCIL ' Lab Flag Volane Ul QC Bla To-99 0.669 &15 10.5 15 U 025 rr. I I Average 0.66s0 1500 10.5000 Sdev. - . -
| |
| Sdev:, _ _
| |
| Mim 0.6090 8.1500 105OOO Ma O.b660 O.1500 10t5000 I
| |
| Rank Results for March 2004 15 2 10 5 *Tc-99 0 5 . i -Zero Mean 0 Sigma
| |
| ;5 -Ave. MDC
| |
| -15 0 5 10 Rank Order
| |
| | |
| A*pedx El1 March 2004 Rank Treed Resgis 2-sima Required COnc. TPU MDC 11DC AJquot Rark Well 10 NudIde (PCM)Ll (OCUL) (KA)LI (PCLI Lab Flag Volume CL) Order MWEOF2 A(-10m -227 Z15 3.41 50 U 2 1 MW108SRepicaie Ag-108m 1.64 221 3.14 50 U 2 2 MW102S Ag-10m 1.45 1.88 '37 50 U 2 3 MWtO7S AG-1Osm -1.15 1.85 313 50 U 2 4 MWtO7D Ag-108m -0.964 243 4.05 50 U 2 5 MWIOID G-10Sm 4.95 2.1 353 50 U 2 6 MWI24S AO-lo0m .0.78 '1.76 '.95 o0 U 2 7 MWI13S Ag-108m -0.721 1.87 3.23 50 U 2 8 MW1220 AG-108m -0.724 1.79 3,18 50 U 2 9 MW106S AO-lom 4.S89 1.11 1.86 50 U 2 10 MW114S Ag-iOem -0.612 22 3.73 50 U 2 11 MW109S AG-l~om -0.805 1.78 3.02 50 U 2 12 LMW10tD Ag-10m -0542 1.43 2.32 50 U 2 13 W115S A-10Brn 4.445. 1.6 z2.8 50 U 2 14 MW104S Ag-lOnm -0.434 129 2.17 50 U 2 15 MW105D Ag-10m 40.429 121 2.01 50 U 2 16 MW106D Ag-106m 4 391 1.08 1.89 50 U 2 17 MWI05S(Sot) Ag-108m -0291 1.18 1.9 50 U 2 18 MWIIO Ag-10Bm -0224 1.85 3.3 50 U 2 19 MW1220 RepIcale Ag-108m -. 18 1.05 1.4 50 U 2 20 MWI22S Ag-10m 407.33 1.95 3.28 50 U 2 21 MWOSS (SOL) Ag-O1n 0.108 1.55 2.63 50 U 2 22 MW0ltS Ag-10m 0182 1.9 3.46 50 U 2 23 MWI23S Ag-'10m 0.182 1.95 3.48 50 U 2 24 MW125S 'Ag-10m 0.174 1.5 2.72 50 U 2 25 MVW lS. lO-108m 0273 1.69 3.12 50 U .2 26 MV/W05S Ag-108m 0291 1.05 1.82 50 U 2 27 MWI02D Ag-108m 0.343 2.08 3.74 50 U 2 28 MWI12S Ag.108m 0.403 1.67 3.08 50 U 2 29 MW100S Ag-10m 0.455 1.85 3.31 50 U 2 30 MWI03S Ag-10m 0.489 1.45 2.47 50 U 2 31 IIWll7S Ag-106m 0.603 227 3.92 50 U 2 32 MWtOOD Ag-108m 0.693 2.07 3.63 50 U 2 33 MWIO8S Ag-108m 0.693 1.74 329 50 U 2 34 MWItOSD(So.) Ag-108m 0.839 - 1.09 1.95 50 U 2 35 MWll4SDupnate Ag-108m 0.844 3.34 4.71 50 U 2 38 MW109D Ag-108m A29Z 1.1 1.97 50 U 2 37 MWI06D (So.) Ag-10m 1.35 1.51 2.61 50 U 2 38 MWillS Ag-108m tX.84; 1.87 3.3 50 U 2 39 cc 39 39 39 Average: -0.1169 1.7251 Z9472 Sdev 0.8458 0.4687 0.7119 Sdev: -723% 27% 24%
| |
| Mln: 2.27 1.05 1.82 Max: 1.84 3.34 4.71 Medan: -0.18 1.78 3.13
| |
| | |
| Apperhx El Mamh 2004 Rar* Trend Remits 2-sW- Reqired CanC_ TPU MDC MDC AlkW Wel 10 Nude (PCLt (vPCl&) (oCUl.) (PMt) Lob Flg Vdlu (L)
| |
| OC SW* Ag-108m 0.6SI 1.06 1.95 50 U 2 QC BLV* Agtce10 o-05 1.64 2.89 50 U 2 m 2 2 2 Averaoe 0.C5C0 1.3eco Z4200 Sdv. 0.8570 03960 0.6647 Saw. 17t4% 29% 27%
| |
| Mim -OS580 1.0680 1.5sc Mac 0.e5s0 1.6400 2.esco Rank Results for March 2004 10
| |
| * Ag-108m
| |
| -Zero Mean c 0 Sigma
| |
| +2-Sigma I -5 -Ave. MDC
| |
| -10 0 10 20 30 Rank Order II/
| |
| | |
| Appedx El March 2004 Rank Treed Rests 2-sigma Requied Conc. TPU MDC MDC AAWM Rank Well ID Nudide (cCvL) (CL) (OL) (OCM) Lab Flag Vodwne L) Order MWI07S Cs-134 .122 22 -'359 14- u 2 1-MWiO8S Cs-134 12 1.95 A325 . 14 u 2 2 MWIOIS C-134 .1.04 2.85 -4.97 14 u 2 3 MWI23S C3-134 -1.04 285 4.97 14 U 2 4 MW125S Cs-134 .101 175 2.91 14 u 2 5 MWIICC Cs-134 .0.791 22 3.72 14 u 2 e MWI13S Cs-134 .0.814 1.95 3.33 14 u 2 7 MW103D Cs-134 40.522 15-W 2.63 ,14 u 2 8 uW1O9S Cs-134 .0.478 1.82 3.1 14 u 2 9 UW1OSS Cs-134 .0.309 12 1.99 14 u 2 10 8WI050 Cs-134 .029 15 2.81 14 U 2 11 MWI02D Cs-134 -020S 2.37 4.13 14 u 2 12 MWIoss Cs-134 .0.183 1.17 1.96 14 u 2 13 MWI0S (Sol.) Cs-134 .0.158 1.78 3.12 14 u 2 14 MWI0SD (Sol.) C.134 .0.14 1.54 2s. 14 u 2 15 MWI05D (So.) Cs-134 0.103 122 2.09 14 u 2 18 MWI00D Cs.134 0.123 - 225 4.1 14 u 2 17 MWEOF2 Cs.134 0.129 Z08 3.78 14 u 2 18 MW122S Cs-134 0.347. 1.91 3.49 14 u 2 19 MWI02S Cs134 0.383 2.24 4.02 14 u 2 20 MW122D Cs-134 0.392 1.84 3.4 14 u 2 21 MWl06D Cs-134 0.415 127 228 14 u 2 22 MWIO9OD C&-134 0.541 1.24 228 14 u 2 23
| |
| .UI22DRepate Cs-134 o051 1.18 2.11 14 u 2 24 MWI05S (Sol.) C4-134 0.44 1.31 , 2.39 14 u 2 25 MWI1os Cs134 0739 2.01 3.75 14 u 2 28 MWI03S Cs-134 0798 1.42 2.5 14 u 2 27 MWI14S ,CS-134 1.2 .2.74. 4.72 14 u 2 28 MWIOID Cs.134 128 2.35 4.43 . 14 u 2 29 MWIOS Repicate Cs-134 . 129 208 . 3.87 . 14 u 2 30 MIWIss Cs-134 1.31 1
| |
| : 1. .3.855 14 u. 2 31
| |
| * MW1O7D Cs-134 1.32 2.54 4.71 14 u 2 32 MWI24S Cs.134 1.48 2.15 4.13 14 u 2 33 MW112S Cs-134 1.51 1.88 3.7 14 u 2 34
| |
| * MWtO4S Cs.134 1.41 IAI554> 2.5 14 u 2 35 MWII7S Cs-134 1.85 2.3 4.45 14 u 2 38 MWIODS Cs.134 1.78 2.05 3.91 14 u 2 37 MWIUSDupiate Cs-134 2.28 2.88 5.85 14 u 2 38 MWIIIS Cs.134 .j;3.~33 , 2.4 4 14 U 2 39 nI 39 39 .39 Average: 0.4088 1.9308 3.4592 S4ev 1.0435 0.4983 O.9393 Sdev 255% 26% 27%
| |
| Mirn -122 1.18 - 1.98 Max 3.33 2.8 5.85 Medasx 0.383 1.95 3.59
| |
| | |
| AppenxE 1 Mach 2004 Rank Trend Respt 2-segma Reqrred Cone. TPU MOC MDC Aqt Wd ID Nudide (Pt) (pCII) (pClL) (pCIat) Lab Flg Voime (L) oC Btan C-134 .1.11 1.33 2.09 14 U 2 QC BI* Cs-134 1 1.94 3.69 14 U 2 n: 2 2 2 Averae. -0.0550 1.6=3 2.8M90 Sdev: 1.4920 0.4313 1.1314 Sdew *2713% 26% 39%
| |
| Mir .1.1100 1.330 2.0980 Max: 1.0080
| |
| . 1.90 3.6C0 Rank Results for March 2004 107 I Ii !' *Cs-134
| |
| ~1.1 -zero Mean iii0 .Yeiiiiiai liI.II Sigma IIHII.* .+2-Sigma 0I-Ave. MDC
| |
| -10.
| |
| 0 10 20 30 Rank Order
| |
| * Appidx El Mardc2004 Rank Trend Remt 2-stma Requeed Co-.C TPU UDC UDC M M RBank Well ID Nudnde (Pc&) (vCUtl (oaUL) (pCLIL) Lab Flag Vokxne (L) Order MWEOF2 Cs-t37 .72 2.18 3.48 15 U 2 1 MWtt7S Cs-137 .2e7 2.38 3.7B 15 U 2 2 MwiIIS Cs-137 .2.13 227 3O 15 U. 2 3 MWIOOS Cs-137 -UA4 1.u 3.13 15 U 2 4 UW102S Cst-37 .127 2.21 3.e7 15. U 2 8 MW122S Cs-137 .127 t.7 - 3.31 15 U 2 a MWt1OD Cs-137 -1.19 2.01 3.34 Is U 2 7 MWI24S Cs-137 .0.928 1.92 3.32 15 U 2 8 MWI04S Cs-137 -0.923 1.3 2.09 15 U 2 9 MWIO8O (Sal.) Cs-137 .0.727 1.39 z35 15 U 2 10 LWm0oS CS-137 .0505 1.13 1.86 Is U 2 11 MW10O9 Cs-137 .0.48e 1.17 Z02 15 U 2 12 MWI10D Cs-137 40.42 1.43 2.48 15 U 2 13 MWI14S Cs.137 .0.398 Z28 4.12 , 15 U 2 14 MWI0SS Replicate Cs-137 .0.352 1.96 3.39 15 U 2 15 MWI12S Cs.137 :O.335 1.96 3.44 15 U 2 18 MWII3S Cs-137 .0.281 1.8 3.18 15 U 2 17 MWI07D Cs-137 0194 2.88 4.4 15 U 2 18 MW106S Cs-137 .118 1.17 1.98 15 U 2 19 MW12ZO Replicatb Cs-137 -0.0877 1.19 2.08 15 U 2 20 MWN09S Cs-137 .0.0687 1.92 3. 15 U 2 21 MWIOID Cs-137 0 3.81 7.09 15 2 22 MWIOBS (Sal.) Cs-137 0 2.96 5.01 15 2 23 MWI1USDupk9ae Cs-t37 0 4.48 875 15 2 24
| |
| - ,MW1105 Cs-137 0.128 Ina 3.41 ts U 2 25 MW1O00 Cs-137 0.194 1.94 3.59 15 U 2 28
| |
| *.WN105D(Sol) Cs-137 0.151 1.81 3.41 15 U 2 27
| |
| -:MWt6D Cs 137 0.81 1.24 224 15 U 2 28
| |
| - WI105 (Sol.) Cs-137 0.752 1.18 z21 15 U 2 29 MW12Ss -*Ct137 0.849 1.53 2S. 15 . U 2 30 MWItoS: Cs-137 1.11 11.48 5.a 15 U 2 31 MW102D Cs.137 1.24 2.07 3.92 15 U 2 32 LW103D Cst-137 1.34 .1.48 27 15 U 2 33 MW1o7S Cs4137 1.4 1.82 3.52 t15 U 2 34 MWI15S Cs437 ~2.84 1.75 3.8 , s U 2 35 MW122D Cs137 §.:3.19% 2.4 4.65 15 U 2 3I MW10tS Cs-137 3.84 5.7 4.31 15 U 2 37 MW123S Cs.137 3.84 5.7 4.31 15 U 2 38 MIWI03S Cs.137 22.4 3.45 , 2.83 15 2 39 eK 39 39 39 Average: 0.e518 2.1651 3.4390 Sdev: 3.8853 1.1119 1.3418 Sdev: 593% 51% 39%
| |
| Mine 272 1.11 1.88 Max: 22.4 5.7 8.75 Medarr -0.077 ;, 1.94 3.38
| |
| | |
| Appadx Et Match2004 Rank TrentdResits 2-sigma Reqokd cor: TPU MIC MoC Aquot Wdn 10t Nunde (PC) (tPM) (lDCll 0W ~CL-Lab Flag Vohzune (L Qc BW* C0137 0.1O3 1.19 2.07 IS U 2 QC tank C4137 -0.708 1U8 .39 15 U 2 2 2 2 Avermve .027 UZ9 Z73 SOW. 0.62 0.s 0.93 Sde" -228% 35% 34%
| |
| 471 1.1t 2.07 Maw .10 t .98 3.9 Rank Results for March 2004 30 25 20I 15 .Cs-137
| |
| -Zero Mean 10 mlma S -- --.- 41 +2-Sigma c o - m 11 tr+di,.IllIHmI tit' MDC
| |
| "-Ave.
| |
| -10 0 10 20 30 Rank Order Rank Results for March 2004
| |
| ;I 10
| |
| '_ 5 U S I III
| |
| * Cs-137 c I III .. 11I+t 0 *C l titll -Zero
| |
| -- Zero MeanMeanll~
| |
| Sigma C l l l l 't' - X- 1- +2-SigmatttlTl
| |
| +2-S-gma tt11111 I-4 I II -Ave. MDC c -5 0
| |
| J I
| |
| -10 0 10 20 30 Rank Order i
| |
| I I
| |
| I
| |
| | |
| Appendx El Mach 2004 Rar* Trerd Refts 2-ftgma Reqtked Conc. WTJ MDC MDC Atso Rank Wd ID Nueflde (pCU4) pM.)) (pC) (fCVL Lab Fbg VoLue (L) Order MW1tOt Eu-1S? -8.26 s8 9.4 50 U 2 1 MWIOIS Eu-1s2 .5.84 5.8 9.33 50 U 2 2 MWI23S Eu-1S2 .5.84 . 5.78 9.33 50 U 2 3 MWtOD1S Eu-152 .5. 591 9.77 50 U 2 4 MWto2S Eu-152 -4.98 5.4 9.43 50 U 2 5 MWEOF2 Eu-152 .3.83 628 10.5 50 U 2 a MWI07D Eu-152 -3.35 a.0o 13.6 50 U 2 7 MwIIss EL-152 .2.52 524 8.6 50 U 2 8 MWIt7S Et-152 -2.15 as 9.47 50 U 2 9 MWI22D Eu152 -2.09 5.34 '0.8 50 U 2 10 MWI0SD Eu-152 -1.94 344 5.74 50 U 2 11 MWt225 Eu-152 -1.94 .3 10.4 50 U 2 12 MW1095 Eu-152 -1.73 5.37 928 50 U 2 13 MWI9o Eu-152 -1.58 359 5.88 50 U 2 14 MW105D(Sol.) Eu-1152 -1.4 3.07. 528 50 U 2 15 MWI2SS E-Is?2 .1.19 4.57 7.61 50 U 2 18 UMWIO2 Eu-152 -1.01 a44 11.3 50 U 2 17 MWIO6s Eu-152 40.785 e,15 10.4 50 U 2 18 MWIO4S EL-152 .0.481 3.U4 67 50 U 2 19 MWIO3S Repcate Eu-152 -0292 5.85 10.3 50 U 2 20 MWIltS Eu-152 -0273 5.42 921 50 U 2 21 MWIO3D Eu1152 .028 4.54 7.55 50 U 2 22 MWtoSS(Sol.) Eu152 .0200 3.57 598 50 U 2 23 MWIoss ELU15 >.0.19 3.22 5-54 50 U 2 24 MWI24S Eu.152 0.383 5.9 104 50 U 2 . 25 MWIOB0 EL-152 .0.c3 13.64 6.14 50 U 2 28 MWII4SDupkate Eu1152 0.965 7.68 135 50 U 2 27 MWtO6S Eu-1S?2 I , 3.23 5.71 -50 U 2 28 MWIC3S . EL152 1.37 429 '7.38 50 U 2 29 MWIOO (SOL) Eu.152 253 4.7 7.68 50 U . 2 30 MWI22DReplkale EL.152 2.5 3.48 5.98 50 U 2 31 MWII7S E.152 321 72 126 50 U 2 32 MWI12S Eu.152 3.51 5.91 11 50 U 2 33 MWI14S Eu-152 3.95 5.89 10.9 50 U 2 34 MW110D EL.152 4.07 5.79 105 50 U 2 35 MWIIoS Eu1152 428 5.5 9.98 50 U 2 38 MWIOS (Sol.) EI52 VyRes R4, 4.8 8.17 50 U 2 37 MtWI13S EL.152 e :93 gJ 5.03 981 50 U 2 38 MWII00 ELu152 t 6.95 10.8 50 U 2 39 n: 39 39 39 Average: -0.1857 5.3315 as9687 Sdev. 3.4519 123766 22026 Sdev -2083% 26% 25%
| |
| Min: -e28 3.07 528 Max: 8.83 5.8 13.8 Medam -0292 5.5 9.33
| |
| | |
| Appendix E1 March 2004 Ran Trend Resta 2-sigma Requtred Cart. WFJ MDC MDC AtquIA Weld10 Nudw( Lab Ftag Voktm (L)
| |
| QC Blank Eu.152 4.498 3.47 8.08 s0 U 2 QC Bta,* Eu-152 1.88 5.35 9.35 50 U 2 2 2 2 Average: 0.8 4.41 7.71 Sdev: 1.67 1.33 Z33 Sdev: 245% 30% 30%
| |
| Mitt 4 50 3.47 8.08 Max 1.86 5.35 9.35 Rank Results for March 2004 20 10 R Eu-152 C -Zero Mean
| |
| -15.
| |
| 0 Sigma 5 +2-Sigma 1 ~'-Ave.
| |
| I 1111 MDC 0 10 20 30 Rank Order
| |
| | |
| Apenix E1 Marth 2004 Rank Trend Results 2-sigma Reqired Cant TPU MDC MDC Alquot Rank Wel ID Nudide (PCI/L. (pCMt) - (DCLIj (PCt-) Lab Flag Volnue 1 Order MW1t4S Eu-154 -7.34. 7.01 11.3 50 U . 2 1 MW122D Eu-154 .8.2B 5.09 7.72 50 U 2 2 MW101D Eu-154 .2.67 5.3 9 50 U 2 3 MW106S Repkate Eu-154 Z34 4.41 7.8 50 U 2 4 MW103S Eu-154 .Z14 3.9S 875 50 U 2 5 MW112S Eu-154 -Z12 5.74 10 50 U 2 a MW122D Repicate Eu-154 -Z03 324 5.47 50 U 2 7 MWI01S Eu-154 -1.95 7.2 137 50 U 2 8 UWI23S Eu.154 -1.95 7.52 13.7 50 U 2 9 MW122S Eu.154 -1.9 5.3 9.43 50 U 2 10 MW103S (Sol.) Eu.154 -1.78 4.31 728 50 U 2 II MWl14SDtiocate Eu.154 .1.54 6.97 12.5 50 U 2 12 MWI05D (Sol.) Eu-154 .1.49 3.06 5.19 50 U 2 13 MWI07D Eu.154 .1.15 754 13.5 50 U 2 14 MW103S Eu-154 *0.564 3.21 5.57 50 U 2 15 MW106D Eu.154 .0202 3.34 5,01 50 U 2 16 MW104S Eu.154 .0.122 349 6.19 50 U 2 17 MW105S Eu.154 0.154 2.69 . 4.8 50 U 2 18 MW125S Eu.154 0205 4.18 7.83 50 U 2 19 MWII7S Eu.154 0.292 . 4.71 9.27 50 U 2 20 MWI24S Eu-154 0.344 5.88 9.68 50 U 2 21 MWEOF2 Eu-154 0352 5.95 11.1 50 U 2 22 MWi1oS Eu.154 0.463 423 639 50 U 2 23 MWIIS3S Eu-154 OS12 4.77 9.21 50 U 2 24 MWIO3O Eu.154 0.e22 4.42 7.06 50 U 2 25 MW10D (Sal.) Eu.154 1.44 372 8.95 50 U 2 28 MW109D Eu-154 1.49 3.28 6.08 50 U 2 27 MW109S Euw154 1.67 4.46 809 50 U 2 28 MW103D Eu-154 :187 4.85 9.88 50 U 2 29 MW105D Eu.154 1.98 '4.19 7.82 50 U 2 30 MWi1Ss Euw154 Z03 5.22 9.9 50 U 2 31 MW102S Eu-154 .18 5.81 10.3 50 U 2 32 MW107S Eu154 Z42 5.68 11.2 , 50 U 2 33 MWIOSS (Sl.) Eu154 Z82 347 6.54 50 U 2. 34 MW1OOS Eu.154 Z71 5.6 10.9 50 U 2 35 MW110D EuL154 U85 7.33 11.9 50 U 2 38 MW108S Eu-154 324 5.45 112 50 U 2 37 M11iS Eu.154 3.44 5.58 11.3 50 U 2 38 MW102D ELF154 4.74 6.19 11.9 50 U 2 39 Ft 39 39 39 Average: 40017 4.9915 9.0249 Sdev: Z4933 1.3810 25026 Sdev: 147628% 27% 28%
| |
| Mli .7.34 Z69 4.8 Max: 4.74 7.54 13.7 Medlan 0.292 4.85 921
| |
| | |
| Appendx El Mardc2004 Rank Trend Resfit 2-sigma Required Cal; TPU MDC MDC Aliquot Wef0 Nudift (CJL&) (pCI&) (oCLL) (pCLIt) Lab Flag Vohmne -t)
| |
| QC Blank Eu.154 1.78 328 e`18 50 U 2 QC Blank Eu-154 .1.47 4.68 S38 50 U 2 m 2 2 2 Average: 0.16 3.97 7.27 Sdev: 2 30 0.98 1.54 Sdev: 1483% 25% 21%
| |
| Mln -1.47 3.28 8.18 Max 1.78 4.68 838 Rank Results for March 2004 20
| |
| -15
| |
| -210
| |
| - 0 Eu1154 5 -Zero Mean 0 Sigma
| |
| -5 M 1111112-Sigma +19
| |
| ~ -1 I-Ave.tt''II' MDC
| |
| -15 0 10 20 30 Rank Order
| |
| | |
| Appendlx E1 Mardc2004 Rank Trend Results 2419ma Required Conc. TPU MDC MDC Aliquot Rark Wed ID Nudide (pCt (pCVtL (pCl) (pCVt) Lab Flag Vol-eCL) Order MWI145Dupcate Eu-155 -5.85 9.33 15.1 50 U 2 I MWIOSRepicate Eu-155 *4.71 7.59 12.4 50 U 2 2 MWI'7S Eu-155 4.09 8.84 15 50 U 2 3 MW101D Eu-155 .325 7.5 12.3 50 U 2 4 MWEOF2 Eu-155 Z94 8.1 13.5 50 U 2 5 MW122D Eu-155 .288 6.88 I1.9 50 U 2 a MWI1oS Eu.155 -2.38 7.84 13 50 U 2 7 MW109S Eu-155 Z31 7.39 12.3 50 U 2 8 MWI12S Eu-155 .1.82 735 12.5 50 U 2 9 MWI02D Eu-155 .1.79 9.38 15,5 50 U 2 10 MWI00D Eu-155 .1.58 7.83 133 50 U 2 11 MW113S EU-155 -1.5 e.98 11.9 50 U 2 12 MWIo6D Eu-155 .1.42 4.74 825 50 U 2 13 MWi03D Eu-135 -1.38 5.4 9.39 s0 U 2 14 MWI07S EU-155 .1.28 724 .12.5 50 U 2 15 MW1100 Eu-155 .0.703 7A7 13.1 50 U 2 1a MW1IS Eu-155 .0.577 5.8 9.35 50 U 2 17 MWI23S Eu.155 -0.577 5.8 9.35 50 U 2 18 MW100D (Sol.) EU-155 .0298 5.81 9.8 50 U 2 19 MWIo5O Eu-155 -0.080 335 5.51 50 U 2 20 MWI22D Repcate E1s55 -0.00359 429 7.48 50 U 2 21 MW104S EU-155 0.0548 5.87 932 50 U 2 22 MWIos0 EL,155 0.171 . 42 7.17 50 U 2 23 MW124S Eu-155 0.21a 7.54 le. 50 U 2 24 MWIOS(SO.) Eu,155 0.78s 58 9.54 50 U 2 25 MWI02S Eu-155 0.838 7.e4 122 50 U 2 28 MW10sD (Sol.) Eu-155 0.935 4.19 7.15 50 U 2 27 MW1055(Sot.) Eu-155 0.948 452
| |
| * 7.9 50 U 2 28 MWI03S
| |
| * E-155 124 5.84 9.45 50 U 2 29 MW105S . E-155 129 4.34 727 50 U 2 30 MWI2Ss Eu-155 137 5.9 10.8 50 U 2 31 MWII4S Eu-155 2.14 5.77 9.9 50 U 2 32 MW1O0D EuI155 2.87 4.34 7.69 50 U 2 33 MWIO8s Eu-155 2.98 7.51 13.7 SO U 2 34 MW107D Eu-155 4 10.3 17.5 50 U 2 35 MWI11S Eu-155 425 7.07 1Z8 50 U 2 38 MWIISS EL-155 5.11 8.8e 12 50 U 2 37 MW10os EL-155 524 8.81 12.5 50 U 2 38 MWI22S Eu-155 858 7.84 142 50 U 2 39 nt 39 39 39 Average: -0.0154 65559 112108 Scev: 2.7578 1.250 2.7447 Sdev. -17868% 25% 24%
| |
| Mit .5.85 3.35 5.51 Max 6.58 103 17.5 Mediant .0.0601 e.88 12
| |
| | |
| Appendx El Mardc2004 Rage Trend Resits 2-sigma Reqhred Conc. TPU MDC MDC A"qs Wel 10 Nods (pCItU (pCVt) (pCaU) (pCUt) Lab Flag Vokue (L)
| |
| QC Stank EU-155 -0.667 3.62 (18 50 U 2 QC Blank Eu-155 -3. 5.38 9.19 50 U 2 It 2 2 2 Aveage: -. 1985 4.5000 7.6850 Sdev: Z1659 12445 Z1284 Sdecr -9% 28% 28%
| |
| Mlr -3.7300 3.200 &1800 Maxc -. 8870 S.3000 L1900
| |
| | |
| Apperx E.1.
| |
| March 2004 Rank TrentdResdts 2-sigma Reqtred Corr-' WT ' MDC - MDC . Aqt Rank Wen D11 Nudde (Datit (OCUL) (foCU (Dt}C tLabFlea Vohxne(LI Order MwioS 238 ' 0027 0.a26s' ,MM 0.125 I 0.5 U 02 . 1
| |
| * MWI05 (SD.) Pu238 -0.0144 0.051t 0.-51 0.5 U 02 2 Mw10Ss PU-238 -4o.o714 0.014 .0.085 0.5 U 0.2 t MWIOO Pu-238 4000139 00335 0.103 0.5 U 0.2 4 MW10'#3S I,> 0 a.oz4' o0407 0.5 U 02 5 MW10613Reptiate Pu-238 0 0.0295. 0.04o 0.5 - U .2 e
| |
| * MW105S(Soi.) PL-238 0,0039 ao3 0.0845 e 0.5 U 02 7 eUWIOS (Solt) Pu-238 0.0207 'C.07M 0.198 0.5 U 0.2 e8 MW1OD - P-238 0.0263 ao0689 0.144 0.5 U 02 9 MWI06S Pum2a8 0.0355 0.0704 0.M4 . 0.5 U 02 10 MW1060 Pu-238 '0.0439 0.070 0.137 0.5 U 0.2 -11 MWIO6D (Sol.) Pu-238 '.77 a .0867 0.14 0.5 a U a2 12 12 12 12 Average: 0.0135 0.0499 0.1165 Sdev 0a.029 0.0257 0a0468 Sdev 214%S 52% 40%
| |
| Mter 4.0271 0.014 o00407 Max: oa0778 0.0879 a0s9 Medlan: 0.003475 0.04255 0.131 2-singa Reqtired Con TPU MDC MDC Alquot We7 ID .NDde (=v , (Pct) (OCK) (pCMl) Lab Fag Volane (L OC Blade PL-238 4.0297 r'0.045 0.158 0.5 U 02 rc I I 1 Average: 4.097 0.0456 0.158 Sdev. - ' -
| |
| Sde%, , . .
| |
| MtI .0.0297 0.0458 0.1580 MML 4.097 0.0458 0.2580 Rank Results for March 2004 0.3 0.2 a0.1 i i*Pu-238
| |
| -Zero Mean 0 .. t-t-- I .. fF- I-2-Slgiga C +2-Sigma
| |
| - eQ1 -Ave. MDC 0
| |
| Q -0.2
| |
| -0.3 . . . '. . . .'
| |
| 0 5 10 Rank Order ; ' '
| |
| | |
| Append E.1 March 2004 Ran Trend Resdt 2-sigma Reqtired Conc W . MDC MDC A~qtgA Ran Wei 10 Nulrde (DCUt) (=CL) (pCVI) (pO=) Lab Flag Voksie (L) Order MWiO90 Pu-239.240 -0.0153 0.0849 0.178 0.5 U 02 1 MW1C5S (Sol.) Pu-239240 4.00014 0.0338 0104 0.5 U 02 2 MW109g Pu-239240 0 0.0281 0.0389 0.5 U 02 3 MWI04S Pu-239240 0.0095 0.0437 0.113 0.5 U 0.2 4 MW105g P-239240 0.007 0.031 0.085 05 U 02 5 MW103S Pu-239240 0.00728 0.0489 0.127 05 . U 0.2 8 MWI130 Pu.239,240 0.01383 0.0432 0.103 0.5 U 0.2 7 MW105D(SOL) Pu-239,240 0.014 0.0275 0.038 0.5 -U 02 8 MW108 (Sot) Pu-239.240 0.0142 . 0.0444 0.108 0.5 U 0.2 9 MW105D Puw239.240 0.02 0.0393 0.0804 0.5 U 02 10 MWI0OMRelicate Pu-239240 0.0225 0.0443 0.0908 0.5 U 02 11 MW18O (Sot.) Pu.239,240 0.0311 0.0574 0.115 0.5 U 02 12 rr 12 12 12 Average: 0.0101 . 0.0422 0.0982 Sdev: 0.0121 0.0114 0.0375 Sdev 120% 27% 38%
| |
| MW 4.0153 0.0275 0.038 Mac 0.0311 0.0849 0.178 Medan: 0.01054 0.04345 01035 2-sigma Reqdred Con. TpW MDC MDC Alkqjt Wel 10 NUcido (pCo) (PCVL) (PCLI.) (pCo) Lab Flag Vobm,. (LI aC Blank Pu-239.240 -0.0517 0.0383 0.167 0.5 U 02 It I I I Average: 0.0517 0.0383 01870 Sdev, Sdev:.
| |
| Mlt .0.0517 0.0383 0.1870 Mac -0.0517 0.0383 0.1870 Rank Results for March 2004 0.3
| |
| , 0.2 U
| |
| * Pu-239,240 0.. I -Zero Mean
| |
| ° t0 Sigma
| |
| +2-Sigma
| |
| -0.1 -Ave. MDC
| |
| -0.2
| |
| -0.3 0 5 10 Rank Order
| |
| | |
| Apendx El TiMed RestIt March 2031 Rar Reqjred t Rank 1 Oqc. 2r_ m A'kLv u60 M Wee ID ;
| |
| 1DI U 0.
| |
| 12.1 2 442 7'.12 ' 1 /U02 MWIO3O(W.
| |
| Pu-24l li 71.89 ~a?
| |
| 13 IS; 1U Pt-241 -0.94 A22 7 mW1 o60 ICE .39 114~ I IIs IS
| |
| .2 U P241 Au241 *0. 1 O9 1 O6(,SSp MW10s0 MAW t 2.293. i 6
| |
| *PL-24 7.81 13.2 L 02 jig- 14.8 is m~lo~s PL-24 8.84 u 0.2:540 PL-241 3.58 7.1 12 WIS d P-24l PL, 0.2
| |
| : 0. a 15 UU 12 80 7.31
| |
| . 123 1342 uU 0.2 0.2 Pu.241 &7 7 3.7' 1742 s
| |
| * tPU.24i 10.6 03 Pu241 Mf30~
| |
| MW MW ' U
| |
| ' 2: 14.07 12 12 3.544 Avege. 1.04 2.342 1605 17% is Sd-v 1%
| |
| Sdev 175> 7.1 12, 2J3 Ml: -242 OWWC W~epkat 7.87 13.3 Modfan 1.99 24012 15 U00 ZUOO 9.130 o a U21
| |
| \>
| |
| | |
| Apperndx E1 Marrch2004 Rank Trend Rerft 2-sigma Reqrked Coct TPU MDC MDC A"quc4 Rank Wed ID Nucide (nCLt) ( (PCtL PCC.) (pCLIi Lab Fbao Vokmne (.) Order MW1t73 Am-241 (gamma) .17.9 18.5 22.8 0.5 U 2 1 MW107S Am-241 (ganmra) .13.2 1Z4 17.9 0.5 U 2 2 MW10BD(Sd.) Am-241 (gamma) 888 12.5 15.0 0.5 U 2 3 MWi15s Am-241 (gamma) -588 11.2 17.1 0.5 U 2 4 MW1000 A.m-241(ganima) -526 12 20.7 0.5 U 2 5 MWII0 Am-241 (gamma) .7.41 10.2. 23.4 0.5 U 2 6 MW1035 Am-241 (gamma) -5.6! 9.35 14 0.5 U 2 7 MWI19D Am-241 (gamma) -523 6.83 11.7 0.5 U 2 8 MW102S Am-241 (gamma) -3.91 15.1 22.2 0.5 U 2 9 MW14SDuptkate Am-241 (gamma) -3.22 11 18.4 0.5 U 2 10 MW108s Am-241 (gamma) -2.93 18 26.1 0.5. U 2 II MW1C2D Am-241 (gamma) -2.32 20.2 30.5 0.5 U 2 12 MWEOF2 Am-241 (gamma) -1.71 14 21.0 0S U 2 13 MWIOSS(SOL) Am-241(gamma) -1.31 7.8 12.4 0.5 U 2 14 MW1Z2D Am-241 (gamma) -1.14 17.5 28.5 0.5 . U 2 Is MW106S Repcato Am-241 (gamma) -107 11.1 19 0.5 U 2 16 MWIDO Am-241 (gamma) -0.531 9.81 16 0.5 U 2 17 MW104S Amr241(gamma) -0.0BO9 10.8 18 0.5 U 2 18 MWI00S Am241 (gamma) 0 1t 17.6 0.5 2 19 MWI12S Am-241 (gamma) 0.342 11.1 19.7 0.5 U 2 20 MWI13S Am-241 (gamma) 0.435 152 267 0.5 U 2 21 MWIOSO Am-241 (gamma) 0.e8 219 3.73 0.5 U 2 22 MW122DORepcate Am-241(gamma) 1.38 7.04 11.5 0.5 U 2 23 MW10oS Am-241 (gamma) 1.45 3.75 e.57 0.5 U 2 24 MWI23S Am-241 (gamma) 1.45 375 0.57 0.5 U 2 25 MW103D Am-241 (gamma) 1.98 9.02 14.8 0.5 U 2 26 MWIIIS Am-241 (gamma) Z12 11.4 19 0.5 U 2 . 27 MAW18S I Am-241 (gamma) 2.31 6,48 11.4 0.5 U 2 26 MWI24S Am-241 (gamma) 285 11.5 20.3 0.5 U 2 29 MWIOOS(SO.) Arn241 (gamma) 3.32 725 12.2 0.5 U 2 30 MW114S Am-241 (gamma). 3.42 3.72 8.68 0 . U 2 31 MWI22S Amn241(gamma) 3.59 13.5 22.4 0.5 U 2 32 MW105D (Sd.) Am-241 (gamma) 3.95 9.92 15.8 0.5 U 2 33 MWI1ID Am-241 (gamma) 4 10.3 15.7 0.5 U 2 34 MWI05S An-241 (ganmma) 4.44 8.84 10.9 05 U 2 35 MWI1OS Am-241 (gamma) 4.B 10.1 17.3 05 U 2 36 MWIo1S Am-241 (gamma) 5.15 12.4 19.5 0.5 U 2 37 MWI25S Am-241 (gamma) 11.4 12.4 21.3 0.5 U 2 38 MWI07D Am-241 (gamma) 15.9 18.5 29.5 0.5 U 2 39 re 39 39 39 Average: .0.4405 11.01B7 17.5G03 Sder - e1817 4.109 83824 Sdev. -1384% 38% 38%
| |
| Min: -17.9 Z19 3.73 Max 16.9 20.2 30.5 Medarn 1342 11.1 17.9
| |
| | |
| Afperdx E1 March 2004 Rank Trer4 Resmts 2-Sgma Reqnked 7 Coi. TPU. -MOC MD . Ai~qunt We ID Nuclde - (pct
| |
| . (Pat) .(pOCl) (COLI)
| |
| . Labfla . Volume lL)
| |
| QC slanr* A-241 (gwa) 2.95 7.e1 10.22
| |
| * 0.5 U 2 C Btark Am-241 (gamma) 10.4 11.8 19 0.5 U 2
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| * 2 2 2 Avage:
| |
| age 750 9.8060 14.6=0 Sdev 52679 28214 . e225 Sdev: .79% 29% .43%
| |
| Mhr 2.950 ' 7.J10 10205 Max: 10.40o 11tBX0 19.0X00 Rank Results for March 2004.
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| 30 C10 10 I o444jJ=
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| l i
| |
| I1111111III1 7111111 - Zero-2-Sigma.Mean IanAm-241 (gamma) 20 1 j 0Illll~lI-Ave.
| |
| 3 MDC V -20
| |
| -30 . . . . . . . . . . . . .
| |
| 0 10 20 30 Rank Order
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| | |
| AppendtKE1 March 2004 Rark Trend Resaits 2-sigma ReqUred Coryc TPU MDC MDC A" Rar'J Wed tO Nucde tpCUL) (pCVL) (tXCL2 (poCaLA Lab Flag Vduwe tL) Order MW124S An-24t 0.0s3 0.117 0.48u 0.5 U 0.2 1 MWI23S Arn-241 40.0842 0.042 0.284 0.5 U 0.2 2 MwI1os AM-241 .0.0429 0.104 0.354 0.5 U 0.2 3 MW117S Ar-241 4.0415 0.0384 0.27 0.5 U 0.2 4 MWI08O Repncatm Ay-241 .0.0392 0.0344 0.255 0.5 U 0.2 5 MW1O7D An1241 40388 0o072 0.301 0.5 U 0.2 8 MW10s (Sol.) An-241 -0.0251 0.0525 0.188 0.5 U 0.2 7 MWi1ss AM-241 -0.02t4 0.0242 0.198 0.5 U 0.2 a MWI03D Am-241 -0.0188 0.023 0.121 05 U 0.2 9 MWIls Ani-241 .0.014 0.0724 0284 0.5 U 02 10 MWI02D AI-241 -0.0138 0.0711 0259 0.5 U 02 11 MW113S AzO-241 -0.0131 0.0879 0248 0.5 U 02 12 MW1060(Sol.) An-241 0 0.119 0238 0.5 U 0.1 13 MW112S A-241 0 0.0e77 o.o03t 0.5 U 02 14 MW1100 Am241 0.00352 01 0.311 0.5 U 02 1s MW12ss Am-241 0.0108 0.112 0.307 0.5 U 02 18 MWIOSO (So.) Ama241 0.0109 0.0825 0.259 0.5 U 0.2 17 MW1220 Repiate Arm-241 0.0156 0.0832 0.15 0.5 U 0.2 Is MW1220 A-241 0.022e 0.08 .148 0.5- U 0.2 19 MWI04S Ani-241 0.0229 0.0451 0.0921 0.5 U 02 20 MWiOID Am-241 0.0287 o.os98 0.28 0.5 U 02 21 Mw1oss Am-241 0.0339 0.0834 0.0919 0.5 U 02 22 6WI06o Repicat Am-241 0.034 00874 0.139 0.5 U 02 23 Mw1oss Anl-241 0.0379 0.0852 0.129 0.5 U .02 24 MWIO3S Aja-241 0.0413 0.0o85 0.0995 05 U 02 25 MW106D Aam-241 0.0442 0.0522 0.0417 0.5 02 28 MWl14SDLcte Amr241 0.487 0.105 0243 0.5 U 02 27 MWI090 Ah-241 0.0494 0.153 0.373 0.5 U 02 28 MWI00S Am.241 0.os3 0.0843 .19S8 0.5 U 02 29 MWIOss . Am-241 0.0539 0.155 0.389 05 U 0.2 30 MWI08S Am.241 0.0809 0.0878 oals 0.5 . U 02 31 MWIO2S Am-241 0.0819 0.155 0.38 0.5 U 0.2 32 MwIoss(sl.) Ar-241 0.0829 0.0818 0.0428 0.5 0.2 33 MW10O Am-241 0.071 0.112 0.218 0.5 U 0.2 34 MWIOIS Am-241 0.0783 0.139 0.298 0.5 U 02 35 MWI14S Am-241 0.0928 0.135 0259 0.5 U 02 30 MWt000 Am-241 o.o0e9 0.119 0.173 0.5 U 0.2 37 IAW122S Am-241 0.104 a.1ss 0.317 0.5 U 02 38 MWEOF2 Av*241 0.108 0.143 0257 0.5 U 02 39 MW107S Am-241 .11 0.178 0373 0.5 U 02 40 r 40 40 40 Average: 0.0234 0.0898 02308 Sdev 0.0488 0.0408 o.10oo Sdev 208% 45% 44%
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| mln -0083 0.023 0.0417 Max: .11 0.178 0.458 Medan 0.0248 0.07935 0.2515
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| | |
| AppendxE.1 March 2D(XRarwTered Re" 2-1gma Reaqred We* ID NC Con PU . DC ,uot Weel Nudide tUI ) W 1 (pC) (PCVI Lab Flag Volwne (L) oCCBar( AmI-241 .tG232 0.115 .0372 0.5 U 0.2 QCCMar An-241 0.00122 .0O.63 0.221 05 U 0.2 0C Sla Ame-241 0.0235 0.098 -0222 0.5 U.- 02 OCBlanrk Am-241 .0.0541 0.112 : 0.245 0.5 U 0.1 QC Blank Amt-241 .0.0401 0o0834 0.33 0.5 U 02 n: 5 8 5 Average: -.00185 0.0953 0278O Sdevw 0.0313 0.0204 0.o089 Sdev: .189% 21% 25%
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| Mir 4.00541 0.03 02210 Maxc 0.35 .0.1150 0.3720
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| | |
| Appetds l March 2004 Rank TremrResJt 2-Mgma Requred Conc. TPU MOC MDC AMqUwt Rark wen Wl Nrxlide (PCVLI (PDl) (dCLt) CoUa) Lab Flag Volne (L) Order MWI036 Cm-242 -0.0265 0.0514 0.175 0.5 U 02 .1 MWI04S Cm-242 40167 0.0232 0.122 0.5 U 02 2 MWt050 (SO) Cm-242 -0.0102 0.0199 0.212 0.5 U 02 3 MW103S Cmr242 -. 0093 0.04? 0.152 0.5 U 02 4 MWI05S Cm-242 0 0.0326 0.0451 0.5 U 02 5 MW15S (SOI.) Cm-242 0 0.0336 0.0465 0.5 U 02 8 tW1060 (Sot) Repk6a Cm-242 0 0.0477 0.066 0.5 U 0.1 7 MW10BS (Sct.) Cm-242 0.00882 0.0391 0107 0.5 U 02 8 MW1060 Repicate Cm-242 0.0149 0.0293 0.0404 0.5 U 0.2 9 mWio8o (SOl.) Cm-242 0.0157 0.0532 0.115 0.5 U 0.1 10 MW10BS Cm-242 0.0165 0.0518 0.123 0.5 U 02 11 MW1050 Cm-242 0.0167 0.0328 0.0453 0.5 U 0.2 12 MWI030 Cm-242 0.0357 0.0495 0.0484 0.5 U 02 13
| |
| ¢ 13 13 13 Average: 0.0035 0.0393 0.0996 Soev: 0.0188 0.0115 0.0588 Sdw. 478% 29% 57%
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| Mire .0.0265 0.0199 0.0404 Max: 0.0357 0.0532 0212 Medla¢ 0 0.0391 0.107 2-slgma Requred Comf: TPU MDC MDC AIpquc We4 10 Nuckde (pCo) (oCltU (pCo) (DCCl) Lab Flag Volume (L)
| |
| OC Olar* Cmn242 4.0168 0.0232 0.122 0.5 U 0.2 OC Bbr* Cm-242 0 0.0287 0.0369 05 U 01 2 2 2 Average: -0.00B4 0.0250 0.07D5 Sdv. 0.0119 0.0025 0.0602 Sder -141% 10% 76%
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| Mi¢ .0.0168 0.0232 0.0369 Max: 0.0000 00267 0.1220 Rank Results for March 2004 0.3
| |
| . 0.2
| |
| "- 0.1
| |
| * Cm-242
| |
| .I I. -Zero Mean 0 oht t t V Sigma C +2-Sigma a -0.1 -Ave. MDC C
| |
| 0 u -0.2
| |
| -0.3 0 5 10 Rank Order
| |
| | |
| IAppedx E1 March 2004 Rank Trend ResAtfs 2-sbma Requted Corc. wTP MDC MDC A"t Rank Wel ID *tNume (pM)l (apOL) (-PM) (rl-M) LablF'ag Voc t)l Order MW1060 CM-243.244 .0089 0.0652 0.234 0.5 U 0.2 MWI06S Cm-243.244 .0.0708 0,0944 0.263 05 U 0.2 2 MW1060(501.) Cm-243.244 .0.0288 .00971 0215 0.5 U 0.1 3 MWtOBS (SOL) Cn,243244 .0.0249 0.0281 0.13 0a5 U 0.2 4 MWIO8O Repkate Cm243.2" .0.00804 0.094 0225 0.5 U 02 5 MW105S Cm-243.2 .0.000305 0.052 0.142 . 0.5 U - 0.2 B MW105D Cn-243.2U 0 .00302 0.0417 05 U 02 7 MWI05S(SOt) Cm-243.2U 0 0.0308 0.0428 05 U 02 S TWI06D (WS.)Reoa Cm-2432" 0 0.0435 0.O002 05 U 0.1 9 MWI04S Cm-243.244 0.00759 ,0.0337 0.0923 0.5 U 0.2 10 MWI030 Cr-243.244 0.00815 0.0381 0.099 0.5 U 02 1I MW103S Cm.243.244 00157 0.095 0218 0.5 U 02 12 MW1050 (Sol.) Cm-243244 0.0452 0.1B 0.48 0a5 U 0.2 13 n: 13 13 13 Average 40111 0.0682 0.171B Sdev 0.0358 0.0451 0.1181 Sde. .320% 86% 88%
| |
| Mim .0.0 9 00281 0.0417 Mac 0.0452 ,0.18 0.48 Meadam .0 0.052 0.142 2-sigma Reqmired Coic. WPU MDC MDC Afiquot We D10 NLdide (pCULI (fCVlQ (DCI1) (pDCU) Lab Flag Vdutre (L)
| |
| QC BEN* Cm-243.244 .0.0338 0.101 0259 0.5 U 0.2 QC Stan Cm-243244 0.027 0.0837 0.162 0.5 U 0.1 n: 2 .2 2 Average: .0.0034 0.0924 0.2105 Sdev: 0.040 0.0122 0.0T88 Sdev -12B4% 13% 33%
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| Min .0.0338 o0837 0.1820 Mac 0.0270 0.1010 02590 Rank Results for March 2004 0.3
| |
| - 0.2 a 0.1 I I
| |
| * Cm-243,244 o
| |
| C 0
| |
| C 5LD-0.1 0r
| |
| .2 0
| |
| vftt{-H-4+ -Zero Mean Sigma
| |
| +2-Sigma
| |
| -Ave. MDC
| |
| -0.3 0 5 10 Rank Order
| |
| | |
| Appendx El March 2004 Rank Trend ResuLt Reqjred Conot l4Jgma MDC MDC AMqt Rank We4 ID Nudide (uCt) TPU (uG&) (uLt) (uiCA) tab Fag Vokrne (L) Order MWItOD Boron 19. - 0.54 15 1 MW107 Boron 38 0.54 15 2 MW10iS Boron 49 0.54 Is 3 MW1OID Boron 49.4 - 0.54 15 4 MW102S Boron 60.8 0.54 15 5 MW105D Boron 67.5 0.54 15 a MW10 (Sl) Boron 18.? 0.54 15 7 MW10ED Boron 74.3 0.54 15 8 MW105D(Sol.) Boron 76.5 054 Is 9 MWtO3S Boron 65.7 0.54 15 10 MWI03D Boron 90.9 0.54 15 11 MW123S Boron 107 0.54 15 12 MW1020 Boron 113 - 054 15 13 NW114S Boron 173 0.54 15 14 MW114SDupiCate Born 174 0.54 15 15 MW1100 Boron 179 0.54 15 is MW1O7S Boron 192 - 0.54 15 17 NWiiSS Boron 195 0.54 15 18 MW10SD Boron 210 . 0.54 15 19 MWIODS Boron 212 - 0.54 15 20 MW122D Repkcate Boron 223 0.54 15 21 MWI22D Boron 224 0.54 15 22 MWI24S Boron 228 - 0.54 15 23 MW1IOS Boron 236 - 0.54 15 24 MW103S Boron 254 0.54 15 25 MWI04S Boron 2 - 0.54 15 20 MWI22S Boron 317 - 0.54 15 27 MWI25S Boron 390 . 0.54 15 28 iWI06S(Scl.)Repkca Boron C35 0.54 15 29 MWI06S (501.) Boron 670 0.54 is 30 MW105S Boron 735 0.54 15 31 MWIOSS (50.) Boron 767 - 0.54 15 32 r 32 0 32 Average: 225.490D 0-5400 Sdes 204.4375 0.0000 Sdev 91% - 0%
| |
| Mh: 19.9 0 054 Max: 787 0 0.54 Medbt 185.5 0.54
| |
| | |
| Appendx E.1 Mach 2004 Rark Trefd Rests
| |
| .Required Conc. -sigma MDC MDC Alquotx
| |
| *WelID NucHde (uG/Ii WU (uGt)l (uGA)
| |
| WI U Lab Flab Vo&.ne ILI OC Blank Boon - 14.4 4.88 15 J OC Bean .Boron 1.84 - 0.54 15
| |
| - 0.54 J OC Ban Boron &q 15 It S 0 3 Average. 6.7133 Sdwv e.73et 2.057 Sdwv 100% 126%
| |
| Mint 1.8400. 0.5400 0.0000 4.U8OO Mac 14.4000 Rank Results for March 2004 900 800 g 700
| |
| , 600 l
| |
| * Boron c 500 5-Zero Mean
| |
| -a E400
| |
| * 400 Sigma Cf 300 c +2-Sigma 0 2-Ave. MDC r_200 0 100 .* s, ** -
| |
| 0
| |
| -100 0 10 20 30 Rank Order Rank Results for March 2004 200 150 tBoron
| |
| ' 100 -Zero Mean E5 *0* Sigma
| |
| .
| |
| * 42-Sigma C t -Ave. MDC 0
| |
| 00
| |
| -50 . . , . .
| |
| . 0 5 10 15 20 Rank Order
| |
| | |
| AppeWIX t1 March 2004 Rank Trnd Resutts Requied Co. ti4gma MoC MDC Aliquot Rank Wel ID Nudcde (uW TPUNWu.) (LOX) (uGA) LiabFlag Volume (L) Order MW107D Boron 30 4.88 15 J MW118D Boron 141 - 4.88 15 2 MWIO7S Boron 145
| |
| * 4.88 15 3 MWI14S Boron 146 4.88 15 4 MWI14SD~ttate Boron 148 - 4.88 15 5 MWI1Ss Boron 155 4.88 15 8 MWIIOS Boron 191 4.88 15 7 MW122D Boron 197 4.88 15 8 MW122D Recale Boron In - 4.88 19 9 MWI22S Boron 252 4.88 15 10 MWI25S Boon 315 - 4.88 15 11 Mr II 0 II Average: 17455 - 4.8800 Sdev 71.9983 0.Ooco Sder: 41% - 0%
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| Min: 30 0 4.88 Max: 315 0 4.88 Medan: 155 4.88
| |
| | |
| Appeinx El March 2004 Rank Tend Resits Reqtred CoWd . 4IgrtrSa MDC MDC . ASCIt w.JI W IJ.n4LA4. iAd'lA TWIitd'.A % f. IA furtq la rba~tv & z1 OC 8Btak oron 14.4 ., -4.t88 15 J
| |
| .1 e~
| |
| Average' 14.4000 , - 4.tW80 Sde Sde 14.4C00 O.O00 Mh: 14.4000 0.0000 4jW00 Rank Results for March 2004 350 300 A
| |
| .
| |
| * Boron
| |
| '025 200 .* '
| |
| : -Zero Mean Sigma rt 1 50 150 42-Sigma
| |
| +2-Sigma 00 -Ave. MDC 0
| |
| 50 0 .
| |
| 0 5 ' 1 10 Rank Order Rank Results for March 2004 350 300 c 250
| |
| * Boron o 200 4
| |
| * 4
| |
| -Zero Mean Sigma E 150 *50 * + - +2-Sigma c 100 -Ave. MDC 00 50 50 SO 0 5 10 Rank Order
| |
| | |
| Apperolf t_2 Jvme2004 RardiTnrmlResti 2-sigma Reqect Oom. 7PI MDC MDC Aquot Rank Well ID Ntride (pCA&) (dCO) (PCLI.) (PCt)) Lab Flag Vodme (L) Order MWlOGSRepkcate GrosSAlpha -. 474 0.975 Z38 3 U 0.15 1 MW111S , GrossAlpha -0.239 1.03 249 3 U 0.15 2 MW3 GossAlpha -0168 0.783 1.81 3 U 0.15 3 MWilos GrossAlpha -0.0535 0.988 244 3 U 0.15 4 MWtO5S Gross Alpha 0.163 1.18 Z01 3 U 0.15 5 MWIOOS Gross Alpha 0253 1.04 227 3 U 0.15 8.
| |
| MWIOSSDuplcate Gioss Alpha 0.257 1.19 Z14 3 U 0.15 7 MW1 Gross Alpha 0.302 0.939 2 3 U 0.15 8 MWtO7S Gross Alpha 0.317 1.17 +/-88 3 U 0.15 9 MW50tS Gross Alpha 0.358 1.12 228 3 U 0.15 tO MWi17S Gross Alpha 0.41 0.837 1.44 3 U 0.1 11 MW2 GrossAlpha 0.410 0.86 129 3 U 0.15 12 MWIO9S GrossAlpha 0.441 1.12 Z32 3 U 0.15 13 MWIO8SReplicate GrossAlpha 0.499 0.849 1.65 3 . U 0.1 14 MWIO7D Gross Alpha 0.548 127 2t53 3 U 0.15 15 MW504 Gross Alpha 0.787 1.01 1.97 3 U 0.15 is MW113S GrossAlpha 0.989 128 2+/-38 3 U 0.15 17 MWt245 GlossAlpha 1.09 1.2 22 3 U 0. 18 MWIO6D Gross Alpha 1.16 0.887 0a98 3 0.1 19 MWIT7SRepkate G Atpha g 1.25> 0.834 125 3 U 0.1 20 MW507S Gross Alpha 1.427 0.982 1.51 U 0.1 21 MWII2S GrssAlpha k.1. 0 1.1 1.77 3 U 0.15 22 MWI0IS GrossAlpha 1.59 0.939 1.44 3 0.1 23 MW502 GrossAlpha 1.85'Wt 1.12 1.77 3 U 0.1 24 MWIO2S. GrssAlpha I.. 1681.31 2.3 3 U 0.15 25 MW505 Gross Alpha 1.82 0.738 0.934 3 0.1 2t MWIO3S GrossAtpha 2.33 1 1.44 3 0.1 27 MWI25S GrossAlpha Z36 0.789 0.88 3 0.1 28 MWtOOD GrossAlpha Z3t 1.01 1.48 3 0.1 29 MWIO4S GrossAlpha 2.49 0.789 0.838 3 0.1 30 EOF2 Gross Alpha Z58 0.825 0.949 3 0.1 31 MW1OD GrossAlpha 2.72 1.31 2.02 3 0.15 32 MWIO6S GrossAlpha 2.73 1.09 1.N4 3 0.1 33 Mw5w3 Gross Alpha 323 0.89 0.985 3 0.1 34 MWIWOS GrossAlpha 39 1.64 2.55 3 0.1 38 MWi23S GrossAlpha 4.83 1.12 125 3 0.1 38 MWI22 GrossAlpha 4.88 1.33 1.8 3 0.1 37 MWIOSD GrossAlpha 5.3 1.88 2.84 3 0.15 38 MWItOD GrossAlpha 5.83 1.94 Z33 3 0.15 39 MWI14S GrossAlpha 8.29 1.19 1.11 3 0.1 40 MW1220 Gross Alpha 7.14 2.19 .Z37 3 0.15 41 MW5080 Gross Alpha 7.58 1.85 2.07 3 0.15 42 MWIOSD Gross Alpha 7.78 2.23 Z03 3 0.5 43 UWIOID GrossAlpha 8.5 1.34 128 3 0.1 44 UWtO2D GrossAp 8.51 1.77 1.65 3 0.15 45 MW507D GrossAlpha 28.8 Z.16 1.09 3 0.1 48 e4 48 48 Average: Z9944 1.1899 1.7882 Sdev. 4.8393 0.4053 0.5027 Sdev. 155% 34% 31%
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| Mirc -0.4740 0.6600 0.8380 Max 26.80 Z2300 2.8400 Medaft 1.8200 1.1100 1.7900
| |
| | |
| AppendxE2 June 2004 Rank TrendResuts 2-igma Reqked Co. TFU MDC MDC Aqut Wet ID Nudide (PCM&) (PiO - (fpat) (pQ'L) LabFRa Vokwne (L) aC Blank Gross "pha .0.774 0.58 1.7 3 . U 0.15 QC Etank Gwrss Apha -0.384 0.351 0991 3 U 0.15 OC Blank Goss Ipha .0.111 0,593', 1.11 3 . U 0.1 QC Blak Geoss AlphaI& iZn- 159 2.75 3 U 0.15 It ,I 4 4 4 Average: 0.3628 0.7735 1.6378 Sdev . 1.5949 0.55t8 80L37 Sdev: 440% 72% 49%
| |
| Mlr 47740 0.3510 .0.9910 Max: 27200 1.5900 2-7500 Rank Results for June 2004 30
| |
| -25
| |
| . 20
| |
| * Gross Alpha S 15 -Zero Mean Sigma.
| |
| 10 . i+ t 2-Sigma s '.l .. -Ave. MDC 00 t5 0 10 20 30 40.
| |
| Rank Order Expanded Rank Results for June 2004 2
| |
| 1.5 C -1 0.5 I+111f Hi
| |
| ~
| |
| tfP4f1 ll~l*Gross Sigma Alpha
| |
| -1.5
| |
| -2 ...............
| |
| 0 5 10 15 20 25 30 Rank Order
| |
| | |
| U-Atpnh E2-Juwe2004 Rank Trend Resuts 2-sigma Reqtkred Co W MMDC DC A i Rank Wet D Nudlde eC)t) (LCLIJ (oCL4 IPCLI. iab Flag Vkmae IL) Order MW1I Gross Beta 0.234 0.875 1.84 4 b 0.15 1 MWI12S Gross Beta 0.e41 0.944 1.97 4 U 015 2 MW3 GrossBes 7S 0.785 1.49 4 U 0.15 3 MWICXD Goss Bets 1.02 1.37 Z29 4 U 01 4 mW10tS Gross Beta 1.51 0.849 1.5 4 ft15 S MWI75 Go Bela r'1.60'! 1.06 Z04 4 U 0.15 6 MW503 Gross Bets j74 1.3 2.14 4 U 0.1 C 7 MW10SRepiate G Bea ':2.05' 1.64 3.1 4 U 0.1 MW1025 GrossBets '. 2.05U'V 1.13 2.08 4 U 0.15 9 mWitlS GrossBeta 2.058I 1.t1 2.2 4 U 0.15 10 MWIOD GrossBet 3.23 1.49 2.4 4 0.1 tl MWIfOS Grss Bets 3.27 1.4 2.25 4 0.1 12 EOF2 GrossBeta 3.3 1.4 2.24 4 0.1 13 MWI030 Gross Bet 3.36 0.947 1.34 4 0.15 14 MW5tl4 Gross Bets 4 0.95 1.35 4 0.15 15 MWIOOS Repcate Gross Beta 364 0.994 1.45 4 0.15 16 MW507S Gross Bets 3.95 1.49 Z38 4 0.1 17 MWioS Gross Bet 4.35 1.33 2.05 4 0.15 18 MW2 Gross Bets 4.43 1.43 2.46 4 0.15 19 MW5m Gross Bet 45 1.09 1.54 4 0.15 20 MW5S0 Gross Beta 4.88 1.44 2.22 4 01 21 MWt24S Gross Beta 4.9t 1.68 2.62 4 0.1 22 mWS02 Gross Beta 5.02 1.39 Z12 4 0.1 23 MW1220 Gross Beta 5.21 1.58 255 4 0.15 24 MWtOD5 Gross Beta 5.t7 1.22 1.88 4 0.15 25 MWtO3S . GrossBeta 572 1.74 2.92 4 0.1 28 MW1010 Gross Beta 6a1 1.4 2.06 4 0.1 27 MWI10S Gross Beta 6.23 1.35 1.99 4 0.1 28 MW109S - Gross Beta 6.53 1.18 1.34 4 0.15 29 MW508 Gross Beta at 1.22 1.48 4 0.15 30 MWI07D Gross Beta 7 1.58 22 4 0.15 31 MWlt7S Gros Beta 7.28 1.55 2.3 4 0.1 32 MW14S Gross Beta .11 1.45 2.08 4 0.1 33 MW113S Gross Bets 8.3 1.79 2.54 4 0.15 34 MWt22S Gross Bets 6.4 1.54 221 4 0.1 35 MWtIOD GrossBeta 6.5 1.65 Z0t 4 0.15 36 MW117SReplkate GrossBets 6.65 1.58 2.2 4 0A 37 MWIO9 Gross Bets 921 1.7 1.98 4 015 38 MWIO2D Gross Beta 9.95 1.72 2.48 4 0.15 39 MWI25S Gross Bets 11.t 1.52 202 4 0.1 40 NW507D Gross Beta 15.2 1.71 221 4 0.1 41 MW1O85 Gross Beta 19.5 2.05 Z58 4 0.1 42 MWI23S Gross Beta 19.6 1.64 Z29 4 0.1 43 MWiO3S Gros Beta 23.5 1.91 Z25 4 0.1 44 MWIOSSDuopata Gross Bets 43.2 2.72 1.83 4 0.15 45 MW105S Gross Beta 44.3 2.7 1.48 4 0.15 48 n: 48 46 48 Average: 7.8433 1.452t 2.0626 Sdev. 9.2128 0.4035 0.4112 Sdev 117% 28% 20%
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| Mlse 0.2340 0.7650 1.3400 Max 44.30 2.7200 3.10t0 Medam 5.1150 1.4350 2.1300
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| | |
| App&dx E2 June 2004 Ran Trend Resuts 241ona - I Reqired Cot TPU MDC MDC AMDt Well ID Nudide toCYL) (DClU ieCU2Ip teCLI LabFLu Vokane (Li
| |
| * oC sa* Goss Beta 40.435 128 223 4 U 0.1 OC Stan GMs3 Beta -0.0404 0.878 1.49 4 U 0.15 QC B GrossBeta 0.0197 0.997 2.02 4 U 0.15
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| * C Macr Goss Beta 0.854 t1 2.07 4 U 015 n: 4 4 4 Average: 0.0496 0.9883 1.9525 Sdev: 0.45so 0.24es 0.3211
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| ,Sde: 9g9% 25% 16%
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| Mih -04350 0.e7e0 1A4900 Max: 0.6540 12ez 22300 Rank Results for June 2004 50 U 40 0
| |
| * Gross Beta 30 C. . -Zero Mean 0
| |
| 20 +4 sigma E t I +2-Sigma
| |
| '10 0
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| C> ,,4, 4 *+*t++t+$+ 4 4444 4 -Ave. MDC 0 0 -, . . .
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| U
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| -10 0 10 20 30 40 Rank Order Expanded Rank Results for June 2004 10
| |
| -J a
| |
| * Gross Beta Q.
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| C 5
| |
| I I I 1I 11 .111 -Zero Mean 0
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| II I t t 1.1'' Sigma E +2-Sigma CD 0 -Ave. MDC c0 U
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| -5 0 10 20 Rank Order
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| Apoldx E2 June 2004 Rank TrendResults 2-sigma Reqr*ded Ca - TPU MDC MDC Akfqt Rat Wel D Nudid (pCl& (pCl&) (pOt) (pCLl) Lab Flag Vodme (L) Order MW2 H4 .251 229 397 400 U I MWIOS -3 -133 205 352 400 U 2 MWSO5 13 -11.8 109 284 400 U 3 MW5C8 H14 -h1A 181 270 400 U 4 MWIogs 1-3 -9.7 184 275 400 U 5 MW10tOC 1-3 1.8 183 306 400 U 8 MWIOBSRepUeate 11- 10 171 288 400 U 7 mW1C1D 1-3 15.5 145 242 400 U 8 MW3 13 15.8 14? 245 400 U 9 MW117S 1-3 25.1 194 324 400 U 10 MWSC75 -3 47.7 178 29 400 U II MW2 Repicate -3 4&7 208 342 400 U 12 MWI0DS I-3 80.4 172 284 400 U 13 mWII2S 1-3 102 169 277 400 U 14 MW507D IS3 112 188 308 400 U IS Mwioes IS3 138 154 251 400 U 18 MWS52 H-3 141 184 302 400 U 17 SAMwss 113 157. 174 282 400 U 18 MW503 H-3 1e8 188 303 400 U 19 MW1235 I13 174 187 306 400 U 20 MW113S 11-3 s 18q 18 263 400 U 21 EOF2 113 ? 9l ' 17m 286 400 U 22 MW1220 I-3 " 22 165 2e4 400 U 23 MWI 1-3 K;223a 172 274 400 U 24 MW111S 11-3 v-A aJ 18o 288 400 U 25 MWI04S H1-3
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| * 241 190 306 400 U 26 mw1Ols H3 252 179 288 400 U 27 MW504 H-3 276 174 275 400 28 MW122S. H13 645 158 233 400 29 MWI07D 113 656 172 249 400 30 MWI1OSRepleate 113 789 171 241 400 31 MWIOCS 113 850 205 302 400 32 MWI1oS 13 1010 220 310 400 33 Mwi2so 11-3 1280 208 277 400 34 MW106D 1-3 1520 219 297 400 35 MWI24S 13 177o 298 410 400 38 MW125S -3 2170 197 236 400 37 MW10SO I-3 3140 248 258 400 38 MW105SDtvkata H-3 3270 260 276 400 39 MWMOS 1-3 3350 263 277 400 40 MW1020 11-3 4690 253 229 400 41 MWIo3S H-3 5300 304 302 400 42 MWI02S 11-3 5740 332 300 400 43 MWI03D 13 6530 313 254 400 44 iW114S H3 6730 420 427 400 45 MW Coo 11-3 8300 383 278 400 48 t 40 48 48 Average: 1312 207.8 2e8.7 Sde: 215012 60.08 4Z21 Sdev 164% 29% 15%
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| Mlr .251 145 229 Maxc 200 420 427 Medarx 223 185 284
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| .Apperdx E2 .
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| .kme2004 Rank TrendResdtf
| |
| * 2.1.gma - Reqrired Conm .Wi MDC MDC Aqt.ql WdniD Nudkte .MrinlA n rarA gDLii INCU t sbLh F Vokm.e ILl QC Blank -87.5 205 350 40W U K3 C BMark H-3 82.1 t57 260 . 400 U oC Blar H-3 82.6 209 348 400 U K 3 . 3 3 Average: M5=333 1903333 318.8687 Sdev: S5972 2S9a87 50.8482 Sdev e27% 15% 18%
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| Mlr .97.5 157.0 260.0 Max: 82.6 209.0 350.0 Rank Results for June 2004 10000 8000 q
| |
| a.t ++4
| |
| * H-3 C
| |
| cL 6000 44 -Zero Mean 0
| |
| 4000 Sigma C
| |
| 4*4 +2-Sigma 2000 2-Ave. MDC S
| |
| C 0 &64*.***
| |
| U -~-. ---- 4-F .
| |
| -2000 0 10 20 30 40 Rank Order Expanded Rank Results for June 2004 1000 800
| |
| ;F 0.
| |
| 600
| |
| * H-3 CL
| |
| -Zero Mean 400 Sigma 0
| |
| I I I I +2-Sigma U
| |
| .200 -Ave. MDC 0
| |
| C3 0 ,.IIlI ll'4-ilIII I I , ,I I I I I I I I I . .
| |
| -200 I t I I I I ! ' II ! .
| |
| 0 5 10 .15 20 Rank Order
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| Apperdx E2 June 2004 Rank Trend Resuft 2-sIgma Requred Corot TPU MDC MDC Al"qu Rank Wed tD Nscxlde (pOdt) (pCOL) (pO~t) (pCit) Lab Rlag Vodes (L) Order MW105S C-14 -14.7 43.8 74.3 200 U 0.025 I MWtO55 DWae C-14 *132 44 74.9 200 U 0.025 2 MWI06S C-14 -4.53 8.87 11.8 200 U 02 3 MWI03D C-14 *4.07 43 3 73.5 200 U 0.025 4 MWtO5D C-14 -3.46 43.9 74.5 200 U 0.025 5 MWtO3S 0-14 -Z.65 875 11.8 200 U 0.2 6 MW1045 Ct4 1.35 t884 11.7 200 U 0.2 7 MWIt3S Relcate Ct4 2.92 7.04 12 200 U 0.2 8 MWtO6D 0-14 3.53 8.99 11.9 200 U 0.2 9 r 9 9 9 Average: -3.8844 232322 39.0WM Sdev. 8.4681 19.4187 32.9214 Sdev. -188% 84% 83%
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| Mik .14.70W t.8700 11.7000 Max 3.53W 44.0X0 74.9XO Meam 43.6100 7.0400 12.00 2-sigma Required Conc TPU MDC MDC Aliquot WerttD Nucdke (pOCL) (pCL) - (PCDL) (pUL) LabFam Vofine (LI C BSa* C-14 -Z14 3.32 5.87 200 U 0.325 Xt aiark C-14 3.4 6.94 11.8 200 U 02
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| *o 2 2 2 Average 0.8300 5.13W0 8.735 Sdev. 3.9174 2.5597 4.3348 Sdew: 822% 50% 50%
| |
| Mk *-2.14W 3.3200 5.8700 Max: 3.4000 t.9400 1.8W00 Rank Results for June 2004 100
| |
| ,'Il)
| |
| ,50 G-14
| |
| ° . I t-Zer tMean I I +2-Sigma
| |
| ,-50 ~-50 IJJI-Ave. MDC
| |
| .100 0 5 Rank Order
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| Apergx E2 June 2004 Ran* Trend Resdts 2-ingm .. Reqied Coic. W 'U MDC MDCA" Rank Well ID Nudlde 1OC0 OL1 (o1 Lab 9 VkCMeL) voe L) Order MW5O M-54 .tee 1.78 284 50 U. 2 1 MW109s Mn-54 *128 Z38 4.09 50 U 2 2 MW1O0S Mn-S4 .1.17 1.94 328 50 U 2 3 MW1I7S Mn-54 .1.04 18 3.83 50 U 2 4 Mw50sD Mn.54 .0.871 1.38 228 50 U 2 5 MW10Ss Mn-54 .0.82 1.25 2.13 50 U 2 6 Mw e08s Repkat Mn-54 .0.7o1 1.8 z8s 50 U. 2 7 MWI03S Mn-54 -0.731 1.81 '3.13 50 U 2 8 MWI23S Mns4 -. 898m 1.89. z88 50 U 2 9 Mw5i2 Mn-54 .0.83 123 2.04 50 U. 2 10 MW109S Mn-54 .0.593 1.39 2 50 U 2 11 MW10oS Mn.54 .0.585 .9 3.33 50 U 2 12 MWI2Ss Mn.54 -0=535 z2e 382 50 U 2 13 MW504 Mn-54 -m528 1.33 2z33 50 U 2 14 MW100D Mn-54 a.415 2.48 4.42 50 U 2 15 MWIO7S Mn-54 a333 1.57 2.88 50 U 2 18 MWIOS Reptalte Mn.54 -0.193 124 . 2 50 U 2 17 MWI13S Mn-54 .0.1e7 133 Z32 50 U 2 18 MW5o7D Mn-54 .0188 128 2.2 50 U 2 19
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| *MW2 Mn.u .a154 1.2 3.47 50 U 2 .20 MW1145 Mn-54 ao794 1.7 32 50 U 2 21 Mw5sos mn-u4 .0.92 1.88 3.08 50 U 2 22 MW102 Mn54 0 3 Z32 50 2 23 MW111S Mn-4U 0 1.85-- Z29 50 2 24 Mw153 Mn-54 0 . 3.48 28 50 2 25 MWIOID Mn-54 0.0144 2.14 3.78 50 U 2 28 MW11OSReplncate Mn-54 0.0873 Zo01 3.84; .50 U , .2 27, MWI03D Mn4 0.0734. 1.33 . 23 50 U !2 28 MWIOBD Mri-54 0.0915 1.3 Z14 50 U 2 .'29 EOF2 . Mn-54 0.174 ,1.73 :3.23 50 U 2 30 MW10s0 M-54 0.18 1.28 2.27 so ,U 2 31 MW100S Ma54 02 1.31 z3 50 U 2 32 MW3 Mn-54 0202 1.3 255 so U. 2 33 MW10S Mn-54 0217 1.43 2.83 50 U 2 34 MWI24S MM-4 0.268 1.66 3.05 50 U 2 35 MWI22D Mn-U54 0.35 1.85 3.41 50 U 2 38 MWilos Mo-54 0.3e8 1.7 3.08 50 U 2 37 sWlOSSDtplcate Min-4 0.381 2.34 4.33 50 U 2 :38 MWI07D Mn54 0.487 224 3.81 50 U 2 39 MW1225 Mn-54 0a84 1.81 3.55 50 U 2 40 MWS07S Mn-54 0.812 1.22 , 223 50 U 2 41 MW102D Mn-54 0.78 1.93 3.8 50 U 2 42 MWIID Mn-54 1.18 127 2.38 50 U 2 43 MWI Mn54 1.41 1.43 z29 50 U 2 44 MWI 125 Mn54 1.89 1.82 3.57 U 2 45 Mw104S Mn-54 1.82 1.94 2.33 50 u 2 48 MW2 Replcate Mn-U4 .,1.88 . 1.83 3.85 50 U 2 47 n: 47 47 47 Averane -0.0184 1.7553 z9257 Sdev 0.7789 a4878 0.6650 Sdev -4740% 27% 23%
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| Mm: .1.88 122 2 Max,: 1.88 3.48 4.42 MedLvr 0 1.73 zee
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| Appdix E2 June 2004 Rank Trend Results 2-sigma Reqtred Coec. TPU MDC MDC AlkW Wel 10 Nuckdo (pCV) (pstL) (pal.) (pCtt) Lab Flag Vdune (I)
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| XCBtank Mn-54 .1.94 1.88 2.87 50 U 2 oC Slank Mn4J 4705 12t 2.18 50 U 2 QC Bla* Mna54 -0.241 Z05 3.75 50 U 2 ac Bal* Mn44 1.17 1.92 3.63 50 U 2 e 4 4 4 Aveae: 44290 .T25 3.1075 Sder 1.2847 0.3507 0.7309 Sdev: -299% 20% 24%
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| Mile -1.940 1.26C0 Z1800 Mac 1.1700 2.080 3.7500 Rank Results for June 2004 5
| |
| Ci I. *Mn-514
| |
| -Zero Mean 0 Sigma
| |
| -~ +2-Sig'ma ii. *-Ave. MDC
| |
| .5 0 10 20 30 40 Rank Order
| |
| | |
| Appencx E.2 June 2004 Rank Trend Resulls 2-stma Required Coec WT MDC DC M Ct Rank Wed ID Nudde (fCp) (PoM) (fCdt) (cCU) Lob Flag Vohne (L) Order MWI04S Fe55 -27.1 12.3 11.6 25 U 0375 1 MWiO6O Fe-55 -25.1 124 11.6 '25 U 0.375 2 mW106S Fe-55 -213 1Z5 115 25 U 0.375 3 MWIO3SRekcae Fe-55 -19.9 1Z5 11.7 25 U 0.375 4 UW103S Fe-55 -17.9 11.5 10.8 25 U 0.375 5 MWF10S Duplicate Fe-55 1.85 11.3 10.9 25 U 0525 6 UW103D Fe55 2.08 12e 12.3 25 U 0525 7 MWl05DRepflcate Fo-55 227 11.3 10.6 25 U 0525 a MW105D Fe55 6.19 1Z9 11.8 25 U 0m525 9 mW1055 FeM5 9.02 13.4 12.8 25 U 0.525 10 rc 10 10 10 Average: a.9890 122700 11.5400 Sdev, 14.3724 O.B977 0.633 Sdev. -16% 6% e%
| |
| min: .27.1 11.3 10.6 Mac 9.02 13.4 12.
| |
| Meda o
| |
| .6s025 12.45 11.6 2-ig1ma Required cov_ TPU U DC mDC 1 Wel gD Nuclkie fpCI/I) (PCtI) (ePCL) (pCLL) Lab Flag Vodue (I QC Bbnk FeP5 3.35 12 115 25 U Om25 QOCBlank Fe-55 -32.7 13 12.1 25 U 0375 ft 2 2 2 Average: 14.750 12.5000 11lB0 Sdev 25.4912 0.7071 0.4243 Sdev .174% 6% 4%
| |
| Min: -32.7000 12.0000 11.5000 Max: 3.3500 13.0000 1Z1000 Rank Results for June 2004
| |
| .50.
| |
| :40 30 :
| |
| 20 l I *Fe-55 dO10 I~ -Zero Mean 0 Sigma c -10 I I 2-Sigma
| |
| -20 l l -Ave. MDC 00-30I
| |
| -40
| |
| -50 0 5 10 Rank Order
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| Appeaix E2 June 2004 Rak Trend Resdts 2-s Reqkd Cone. TPU MDC MDC Altk Rar WellD NdIde (paL (pCtL) (pCtL4 (CcuL) Lab Flag Vofne (L) Order MWIIOSRepcate Co40 *1.34 2.01 342 25 U 2 1 MWI22D Co-0 .1.17 Zo7 358 25 U 2 2 Mw5O7D Co-0 -0.597 1.59 z75 25 U 2 3 MWIOO Replcate Co-o -0.521 Z74 4.28 25 U 2 4 MW505 Co-CO -0.459 1.85 &3 25 U 2 5 MWI12S CO-CO .0.458 1t7 339 25 U 2 a MWIDOS Co-C0 4337 126 Z2 25 U 2 7 MW2 Repkate Co-Co 4265 2.5 Z93 25 U 2 a MW1245 Co-Co .0263 2.05 J74 25 U 2 9 MWI04SRepcate co-CO 4163 Z17 4 25 U 2 10 MW1o7S Co-CO e 142 222 4 25 U 2 11 MWIO9D Co-Co 0 3.44 5.0 25 2 12 MWII0D Co-CO 0.0o58 1.49 2.69 25 U 2 13 MWI05D Co-oC o0.17 1.48 z65 25 U 2 14 MWIODS Co-Co 0.063 1.2 2.22 25 U- 2 1s MWiIIS CO-CO 0.0721 1.44 ZS 25 U 2 1s MW503 Co-80 0.0982 1.38 Z5 25 U 2 17 MW508D Co-oC 0145 159 Z87 25 U 2 18 MWIO6D Co-Co 0167 126 Z3 25 U 2 19 MW502 Co- o o178 1.43 Z31 25 U 2 20 EOF2 Co- o179 00 Z03 3.33 25 U 2 21 MWso4 Co-Co 0186 1J35 Z48 25 U 2 22 MW1los Co-CO 0194 1.86 342 25 U 2 23 MW1253 Replicate Co-C0 0.291 Z04 3.87 25 U 2 24 MWlOSSReplate Co-CO0 0J17 1.46 262 25 U 2 25 MW3 Co-Go 0.383 1.49 z78 25 U 2 28 MWIO7D . Co-C0 0.452 Z18 4.18 25 U 2 27 MWIMIS Co-CO 0.503 1.94 3.78 25 U 2 28 MWIoD . Co-Co 0.568 1.43 z27 25 U 2 29 MW1O1DRepkcate Co-Co 0.634 1.82 3.67 25 U 2 30 MW50sS Replcate Co-60 0.703 1.66 3.44 25 U 2 31 MWI Co-Co 0.75 1.58 295 25 U 2 32 MW123S . Co-60 0.781 1.78 3.59 25 U 2 33 MW10iS Co-Co 0.809 1.55 295 25 U 2 34 MW122S co-0O 0.857 Z32 4.55 25 U 2 35 MWi02S Co-Co o.e89 1.54 2.83 25 U 2 38 MW10sS Co-CO 0.984 1.3 2.5 25 U 2 37 AW567S Co-60 1 1.34 2.64 25 U 2 38 MWI03S Replate Co-Co 1.02 1.32 254 25 U 2 39 MW2 Co-Co 1.06 3.74 3.73 25 U 2 40 MWI14S . Co-60 1.17 1.J3 3.78 25 U 2 41 MWI02D Co-60 1.52 1.84 3.87 25 U 2 42 Mwl0s5Doupcate Co-60 1.78 209 4.58 25 U 2 43 MWI25S Co-CO e : 892 1.78 3.7 25 U 2 4 MW101D Co-C8 -60 97Ct 1.73 3.9 25 U 2 45 MWi17S Co-CO 2.12 2.22 4.71 25 U 2 48 MWI3S Co-CO 258 zs 455 25 U 2 4?
| |
| MWI06S Replcate Co-CO 4440i! 3.05 5.01 25 U 2 48 MWI00D Co-C0 . 5.2-; 237 5.63 25 U 2 49 MW5O8S Co-Co . s.24,. 284 5.87 25 U 2 50 MWIO8S Co-60 , s.25si 2.84 5.87 25 U 2 SI MWI14S Co-60 6.28 206 4.4 25 2 52 MWI03S Co-60 11.4 3.62 3.13 25 2 53 MWI03S Replcate Co-60 13.7 4.93 4.04 25 2 54 i 54 54 54 Average: 1.3363 1.989 3.5420 Sdev: Z7543 0.7185 0.9713 Sdev: 208% 36% 27%
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| Mhc -1.34 12 Z2 Max 13.7 4.93 8.01 Medai 0.4775 1.835 3.43
| |
| | |
| Appwer E2 June 2004 Rank Trend Reayi 2-*tma Reqdired com TMU MOC Moe Afquot Wen ID Nuode (oCIL) (pCut) (pCML) (pCt) Lab Flag Vokone (L)
| |
| QCCBtak ' lo- -121 151 2.43 25 U 2 QCBtank Co40 -0.458 221 383 25 U 2 OC BLae* C-cO -0.388 1.59 2.95 25 U 2 OC Blank CCO-0 -0.159 2.02 3.7 -25 U 2 CC Blank CO-8O 0.188 1.3 3.59 25 U 2 et 5 8 5 Avere: -0.4050 1.8t40 3.3000 Sdev 0.5155 02641 0.5925 Sdev -127% 15% 18%
| |
| Min -12100 1.5100 24300 Mac 0.1880 271200 .8300
| |
| | |
| Appaenlx E2 June 2004 Rank Trend Resbts 2-sigma Reqired Conr. TPU M4C MDC AMqo Rank We ID Nucde (PCVL) (oCLL) (pCVL) (pCSO) Lab Flag Vomne (LI Order MWIOSDRep"c N 3 -643 7.78 13.7 15 U 0.525 1 MW103D NM3 -5.64 .72 11.8 15 U 0.525 2 MW105O NMe3 -4.97 7.69 13.4 15 U 0.525 3 MW100S Dtpcate NMe3 -4.7 726 127 15 U 0.525 4 MW1C6D NMs3 419 7.74 13.0 15 U 0.375. 5 MWI00S NI-s3 -0.892 7.62 13.1 15 U 0.525 . 6 MW106S NI-s3 -217 6.74 11.7 15 U 0.375 7 MW103S NMe3 5.72 8.17 13.8 15 U 0.375 8 MWIo4S NMe3 e 13 7.5 12z 15 U o0.75 9 MWI03S Repca NIe3 = 3 8.94 14.8 15 U 0.375 10 m 10 10 10 Average: -03589 7.6160 11200 Sdev 5.8910 0.6513 0.9506 Sdev -1641% 9% 7%
| |
| Mhi -843 872 11.7 Mac 10.6 8.94 14.8 Medar -Z041 7.655 13.25 2-sigma ReqWed Cono TPU MDC MDC Aiquot Wed ID Nulide (PCSI) (pCW PI& (PCS) Lab Flag Vo L NMe3 0.213 7.06 121 15 U 0.525 CC QC Stank Blar*k NI.3 4.42 7.87 13.3 15 U 0.375 c 2 2 2 Average: 2.3165 7.4650 12.7000 Sdev, 2.9748 0.5728 0.8485 Sdev 128% 8% 7%
| |
| Mh: 0.2130 7.0600 121000 Mac 4.4200 7.8700 13.300 Rank Results for June 2004 20 15 10
| |
| : a. . NI-63 c -Zero Mean go 0 r HXt I I t1 -- 2-Sigma
| |
| +2-Sigma
| |
| ~ II I-Ave. MDC
| |
| -15
| |
| -20 0 5 10 Rank Order
| |
| | |
| Appendi E2 June 2004 Rank Trend Resuih 2-etma Rqmred Coec. WU MDC MDC Aiquot Rank Well ID - Nucide (DoCU) (pCI&) (nCM) (DCV1) Lab Flag Vokxne (L) Order MW124SRercate sr-90 -0275 0.392 1.14 2 U 0.3 1 MWIOIS sr-go -0242 0.414 1.2 2 U 0.3 2 EOF2 Sr-go -0131 0.504 1.34 2 U 0.3- 3 MW2 sr-go -.131 0.374 1.02 2 U 03 4 MW1O4S St-go -o.o79 0.52B 1.5 2 U 03 5 MWI11S St-90 -0.0552 0.485 1.11 2 U 0.3 6 MWIOID sr-go 0.0309 0.49 123 2 U 03 7 MW108S St-go 0.0577 0.5s7 1.4 2 U 03 8 HW107D Sr-90 0262 0.555 1.2 2 U 0.3 9 MWI02S sr-go 0.289 0.555 1.2 2 U 0.3 10 MW10oo Sr-Do 0.41 0.547 1.15 2 U 0.3 11 MWI23S sr-go 0.471 0.617 1.34 2 U 0.3 12 MWI09D Sr-go 0.473 0.555 1.16 2 U 03 13 MWI14S Sr-go 0.541 0571 1.19 2 U 0.3 14 HWIOD Sr-90 0.549 0.58 1.2 2 U 03 1S MW122S Sr-GO 0O.s88 O 0.493 0.977 2 U 03 1c MW3 Sr-0 0.582 0.599 1.24 2 U 0.3 17 MW2Replckae sr-go 0.82 i 0.374 0.684 2 U 0.3 18 MWI13S Sr-90 .
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| 6
| |
| .. 0.6 2- 123 2 - U 0.3 19 MWIIOS Sr-go pLO. ss l 0.637 1.3 2 U 03 20 MWI12S Sr-go ,.o697I' 0.59 1.19 2 U 03 21 MWII7S Sr-go Zn791 0.516 0.952 2 U 0.3 22 MWIODS Sr-90 "'8O1 0.537 1.06 2 U 0.3 23 MWI02D Sr-go 70.928: 0s5 1.06 2 U 0.3 24 MWI Sr-go .726 0.9444 1.47, 2 U 0.3 25 MWIIOSRepnlcate Sr-90 I. A 0.729 1.44 2 U 03 26 MWto5s sr-go S ii1 O.858 1.26 2- U 0.3 27.
| |
| S-90 SrW103D n 72 2 1.37 2 U 03 28 MWI24S r-90 1.33 :; 0.791 1.47 2 U 03 29 MWI03S Sr-go 134 0.61 1.06 2 0.3 30 MWI2Ss sr-go 1.78 0.742 1.15 2 0.3 31 MWI07S st-go 2.69 0.741 1.19 2 0.3 32 MW106S Sr-go 3.17 0.961 1.31 2 0.3 33 IWI22D - Sr-90 3.2 0.768 1.15 2 0.3 34 Mwoss S-GO 16.2 -1.71 1.38 2 - 0.3 35 MW105S DIcale Sr-90 18&S 1.73 1.33 2 03 3C r: 36 38 38 Average: 1.6553 0.6555 12066 Sdev 3.7492 0.2900 o01593 Sdev: 227% 44% 13%
| |
| MWin .0275 0.374 0.684 Max: 16e 1.73 1.47 Mela: 0.es35 0.58 1.2
| |
| | |
| ApperndhE2 June 2004 Rark TrendResadi 2-sigma Req"d Corn TPU MDC MDC Mqwt We ID NudIde (pcLfL) (PCIM) (PCiL) (pCit) Lab Fla" Voklme (LI QC Blar Sr-90 -0.73 0.347 1.32 2 U 0.3 QC Btat St.90 0129 0.383 o.803 2 U 0.3 0 391 0.657 1.47 2 U 0.3 3 3 3 Average: -0.0700 0.4557 1.19"7 Sdv. 0.5884 0.1745 03499 Sdew. 38% 29%
| |
| Mia -7300 0.3470 0.8ea0 Mac 0.3910 0.6570 1.4700 Rank Results for June 2004 215.
| |
| U .
| |
| * Sr-90 o .- Zero Mean Sigma c S+2-Sigma
| |
| -Ave. MDC 0 .
| |
| -5 0 10 20 30 Rank Order Expanded Rank Results for June 2004 2
| |
| a U
| |
| 1.5 I
| |
| 1
| |
| .*I tIll
| |
| * Sr-90 0.
| |
| I I II II 11 I II It I I I-Zero Mean 0.5 0.5 I 1 + , , . Sigma 0r c +2-SigT1a 0 -Ave. MDC 3
| |
| 0
| |
| -0.5
| |
| _1
| |
| ,1 [
| |
| 0 5 10 15 20 25 30 Rank Order
| |
| | |
| pe2dx E2 June 2004 Rank Tretd Resufts 2-sigma Req dtre Cn WT MDC MDC Asqut Rank Well ID Nucnde opCVI) (pCM.) (opt) (pClt) Lab Fbag Volune (L) Order MWIIOSRep8cate Nb-94 *1.81 1.88 3.04 50 U 2 1 MW110tD Nb-94 -1.44 2.03 2.77 50 U 2 2 MWI23S Nb-94 -122 2.08 2.99 50 U 2 3 MWI00D Nb-94 -0.828 2.35 4.13 50 U 2 4 MWI11S Nb-94 *0.689 1.33 22 50 U 2 5 MWIOIS Nb-94 .845 1.81 3.16 50 U 2 8 MW107S Nb-94 0.559 1.88 2.8 50 U 2 7 MW508D Nb-94 -0.55 1.33 226 50 U 2 8.
| |
| MW504 Nb-94 O.U9 121 2.02 50 U 2 9 MW3 Nb-94 .0.438 1.4 234 S0 U 2 10 MW109D Nb-94 .0.431 2.42 4.13 50 U 2 t1 MW106S Nb-94 -0.428 125 :-2.09 50 U 2 12 MWIo9S Nb-94 .0.407 12 1.78 50 U 2 13 MW1i4S Nb-94 .0.379 1.61 2.86 50 U 2 14 MW508S Nb-94 .0.304 1.55 2.78 50 U 2 15 MW122D Nb-94 .0283 1.84 327 50 U 2 18 tW503 Nb-94 .0278 1.28 2.13 50 U 2 17 MW5BS Replicate Nb-94 0.177 1.6 2.8 50 U 2 18 MWI Nb-94 40.174 129 228 50 U 2 19 MW105D Nb-94 -0.17 129 1.98 50 U 2 20 MWi1oS Nb-94 0.0195 1.7 2.88 50 U 2 21 MWI00S Nb-U 0.138 1.14 2.02 50 U 2 22 EOF2 Nb-U4 0293 1.8 3.18 50 U 2 23 MW108S Repicate Nb-94 0.32 1.12 1.96 50 U 2 24 MW502 Nb-94 0.341 1.03 1.86 50 U 2 25 MW10ED Nb-94 0354 1.13 2.04 50 U 2 26 MW103D Nb-04 0.548 1.2 2.15 50 U 2 27 MW507D Nb-94 0.612 1.18 .2.18 50 U 2 28 MW122S Nb-04 0.651 1.77 329 50 U 2 29 MWII1D Nb-04 0.664 1.25 225 50 U 2 30 MW507S Nb-94 0.703 1.38 2.2 50 U 2 31 MWI13S Nb-94 0.713 124 228 50 U 2 32 MW105S Dicate Nb-04 0.718 2.15 4.04 50 U 2 33 MW107D Nb-94 0.734 1.88 3.5 50 U 2 34 MW112S Nb-U 0.818 1.73 322 50 U 2 35 MW1025 Nb-U 0.829 1.48 255 50 U . 2 38 MW505 Nb-U 0.898 1.61 2.96 50 U 2 37 MW1o5s Nb-U 0.968 1.15 2.09 50 U 2 38 MW1O3S Nb-U 1.03 1.86 327 50 U 2 39 MWiO4S Nb-U 1.11 1.19 226 50 U 2 40 MW124S Nb-U 1.12 1.84 3.43 50 U 2 41 MW12Ss Nb-94 1.15 2.23 3.3 50 U 2 42 MWI17S Nb-94 122 1.93 3.84 SO U 2 43 MW2 Nb-U 1.33 188G 328 SO U 2 44 MW102D Nb-U 14 1.64 3.21 50 U 2 45 MW10oS Nb-U _ i7f T7 1.68 3.35 50 U 2 46 MW2Reptkae Nb-U
| |
| * 2 I 1.66 3.35 50 U 2 47 a: 47 47 47 Average: 02344 1.5740 Z7509 Sdev 0.8481 0.3573 0.8417 Sder 362% 23% 23%
| |
| Min: -1.81 1.03 1.78 Max: 226 Z42 4.13 Meatda 0.328 1.61 2.78
| |
| | |
| Appendix E.2 ane 2004 Rank Trend Resuns 2-sigma Reqied Conec TPU MDC MDC AIqwnt Well D NrdoA focLI (OCULI0CdUt loaVLL ab Fba Vokine (ii KJ QC Bank Nb-94 -0.840 1.7 224 50 U 2 OC Sank Nb-94 0.258 1.97 3.52 50 U 2 aC eat Nb-94 0.331 1.85 3.02 50 U 2 QC Blank Nb-94 0.842 1.69 3.17 50 _U 2 C 4 4 4 Averagc 0.09o3 1.8700 29875 Sdev. 0.8499 02455 0-540 sda: e75% 15% 18%
| |
| Mh: -0.840 1.3700 2.2400 Max: 0.8420 1.9700 3.5200 Rank Results for June 2004 5
| |
| 8i I ..IcilIII .Nb9
| |
| : -Zero Mean i0rft#1+t.{4444+4¶4ft4 Sigma
| |
| +2-SIgma tI I.'I .j . . . -Ave. MDC
| |
| -5 0 10 20 30 Rank Order
| |
| | |
| APP&-4x E2 June 2004 Rank Trend Rests 2-ftma ' Retred Coenc. W PU DC MDC qt Ran Wen D Nulde (PCitI (PCML) (PnC) (PM)L Lab Flag Volume (LI Order MW103s To-O .7.78 828 14.4 15 U 0.225 1 MWI06D To-O9 -4.85 5.15 8.99 15 U 0.225 2 MW105D Tc-99 .4.26 4.7 8.3 15 U. 025 3 MW103= Tc-9D9 -4 4.7 831 15 U 025 : 4 IW1o5S Tc-O99 2.65 4.74 8.33 15 U 025 5 MW105S Duplicate Tc-9O -231 4.78 8.39 15 U 025 8 MW105D Replcate To-G9 -209 4.65 8.14 15 U 025 .*7 MW103S Recate Tc-O -1.92 4.89 8.43 15 U 0225 8 MW103S T0-99 4421 525 9 Is U 0225 .9 MW1o4S Tc-99 0.557 5.24 8.94 is U. 022 :10 n 10 10 10 Average: .2.8924 52360 9.1290 Sdev: 23357 1.0875 1.8788 Sdev ^81% 21% 21%
| |
| Mlix .7.78 4.65 8.14 Maxc 0.557 8.28 14.4 Medla -248 4.835 8.41 2-sigma I Req ted Conc. TPU MDC MDC AlIqut Wet ID NudIde (Put) (PClt) (OCVlt (pCLt) tab Flag Vokxne (L oC lank Tc-G9 .0.445 4.95 8.58 15 U 025 CC Blank T-G99 -5.78 5.17 9.08 15 U 0.225 2 2 2 Average: -3.1025 5.0600 8.8100 Sdev: 3.7583 0.1558 0.3538 Sdev: -121% 3% 4%
| |
| Min: -5.7600 4.9500 S5M0 Max: -0.4450 5.1700 9.0600 Rank Results for June 2004 15
| |
| - 10 CL 5
| |
| .. g ° l 111 1 Tc-99
| |
| -Zero Mean ol
| |
| ' -+2-Sigma -Ave. MDC 0 5 10 Rank Order
| |
| | |
| Appeidx E2 "e 2004 Rar* Trawl Resuih 2-Jgma . Reqed Coo TPU MDC MDC A4qut Ran Welt0 Nudifd (PCVL) (pCLI (pCUI (pCA(L) Lab VWmi ( L)Order (LVs MWIDOO Ao-108°n -2.48 24 3.12 50 U 2 1 MI1OSRepkale A-loeOm .1.84 z34 3.68 50 U 2 2 MWI22s Ag-1o0m -1. 2.07 3.41 50 U 2 3 Mwilos Ag-o0m 1.55 14 22 50 U. 2 4 MW110D Aq.108m .1.47 1.11 1.8 s 0 U 2 s MWI05D AG.108m .1.01 1.21 2.08 50 U
| |
| * 2 a MW10tD Ago108m *0.828 1.83 3.17 50 U 2 7 MwII7s AG-108m -0.e86 203 3.04 s0 U 2 8 MWt03D AgOsm os.8 1.28 Z14 50 U 2 9 MW1O9D Ao-t0sm -0.442 2.52 4.35 50 U 2 10 MW5O7D Aa-108m 4437 1.38 2.31 50 U 2 11 MWI07D Ao-tosm -0297 1.95 335 00 U 2 12 MWIOsD Ag-108m *0215 123 z19 50 U 2 13 MwtOSs Ag-lom -0.848 1.32 2.3 s0 U 2 14 Mw0soS AO-108m o0.0o15 1.78 3.03 50 U 2 15 MW1O2D Ag-1rm 0.0407 1.84 321 50 U 2 16 MWs05 A-lOrom 0.0578 1.4 2.4 50 U 2 17 MWIIIS Ag-108 m 0.104 1.3 2.3 50 U 2 18 MWso3 Ag-18M 0.132 125 2.22 50 U 2 19 Mw5soe Ag-lOSm 0.W 1.43 244 50 U 2 20 MWIOSRocat 4108m A 0.203 12 z2 50 U 2 21 MWs04 Ag-aoem 0255 1.19 Z12 00 U 2 22 MWI23S Ag-1Osm 0.323 1.84 3.37 50 U 2 23 MW2Repkate Ag-ernm 0.349 1.84 334 50 U 2 24 MWt0oS AG-loSm 0.352 1.43 Z21 50 U 2 25 Mwioos Ag-lO0m 0.372 1.19 z0o so U 2 26 MWI14S Ag-1O0m 0.388 2.01 3.53 50 U 2 27 MW08S Repicate Ag-Oesm 0.388 1.82 2.99 50 U 2 28 MWIo7s Ag-lO8m 0.395 1.73 3.12 s0 U 2 . 29 MWlOOS Ag-o10m 0.41 1.12 2.04 s0 U 2 30 MWIOss Dupttcat4 Ag-108m 0.489 1.75 3.17 50 U 2 31 MW502 Ag-lO0m 0.582 1.13 2.08 50 U 2 32 MW3 Ag-1o0m 0.574 1.43 z28 50 U 2 33 MW2 Ag-eosm 0.58 1.81 .z93 50 U 2 34 MWII2S Ag-loSm 0.723 1.7 3.19t 0 U 2 35 MWI Ag-o10m 0.784 12 Z1S s0 U 2 38 MWIO3S Ag-lOm 0.802 1.89 3.31 50 U 2 37 MW507S Ag-lOsm 0.83 1.92 2.09 50 U 2 38 MWIOIS Ag-lOoM 0.851 1.78 3.24 s0 U 2 39 MWI25S Ag-loam 0.854 2 3.57 s0 U 2 40 MW1O4S Ao-loem 0.85 1.25 221 00 U 2 41 MWIO2S A-108m 0.958 t.48 2.55 s0 U 2 42 EOF2 Ag-lO0m 1.32 1.78 3.3 so U 2 43 MW1os8 Ag-losm 1s 1.73 3.24 50 U 2 44 MWII3S Ag-108rn '.'M-57$" 1.42 z1 s0 U 2 45 MWI24S Ag tosm Zq19~ 1.89 3.42 00 U 2 46 MWtZ2D Ag-lOom . 1.8 3.45 so U 2 47 It 47 47 47 Avaeage t1730 1.6084 2.7738 Sde 0.0822 0.3484 0.8135 Sdev 558% 22% 22%
| |
| Mbc .2.48 1.21 1.8 Mac 223 z52 4.35 Medam 0.349 1.82 2.93
| |
| * Apperdx E2 Jure 2004 RankTrend TleeRtes I 2-sigma Reqidred
| |
| . . nc. - TPU - MDC MDC - Mqt .
| |
| WentD Nucide (pCVij (DCULI (ot/i (oCM - Lab Faag Vokse (L)
| |
| OC Blank AO-loom -1.02 1 37 1.97 50 U 2 acCS* AG-108m .0.831 2.08 3.55 50 U 2 QC Blar AG-lOsm 0.257 1.5 2.95 50 U 2 XC Elar AG-lOsm 0.848 1.78 3.39 50 U 2 fr. 4 4 '4 Average: -0.1870 1.7075 2.9550 Sdev 0.8894 0.2997 0.7102 Sdev. -478% 18% 24%
| |
| KMl -1.0200 1.3700 1.9700 M 0 .84e 20800 3.5500 Rank Results for June 2004 5
| |
| -ZeoiMan D l~ IIilI- -Ave. MDC
| |
| -- .M.C Ave 0 10 20 30 40 Rank Order
| |
| | |
| -s-Appwxx E2 "e 2004 Rank Trml Reads 2-sgma Reqired Cons. TWU MDC MDC A"t Rank Wel tD Nucfide (PCLI.) (PCldL) (ocLM (pCIL) Lab FRa Vobne (L) Order MW1070 CS-134 .1.75 2.3 3.8 14 U 2 1 MW2 RepIcata CS-134 .1.68 1.89 2.98 14 U 2 2 MW114S Cs-134 -1.58 2.18 3.58 14 U 2 3 MW504 Cs134 -1.5 1.34 2.03 14 U 2 4 MWilos Cs-134 -0.753 1.87 3.21 14 U 2 5 uwtots Cs-134 -0.893 2.11 3.68 14 U 2 6 MW503 Cs-134 -0.588 1.52 2.52 14 U 2 7 Mwso8S Cs-134 -0.251 1.86 3.37 14 U 2 8 MWIOIO Cs-134 -0.138 223 3.92 14 U 2 9 MWsos C-134 -0123 1.95 3.43 14 U 2 10 Mw1o0s Cs-134 -. 00878 125 2.17 14 U 2 11 MW5070 Cs-134 -0.0531 1.42 2.51 14 U 2 12 MwI17s Cs-134 0.0383 1.96 3.54 14 U 2 13 MW3 Cs-134 0.0385 1.69 2.9 14 U- 2 14 MwioeO Cs-134 00os 1.33 2.37 14 U 2 15 MW2 Cs-134 0t29 1.89 3.52 14 U 2 1a EOF2 Cs-134 0o192 1.82 328 14 U 2 17 MWI110 Ca.134 0265 1.42 2.51 14 U 2 l8 MWIOOS Cs-134 0.331 1.25 226 14 U 2 19 MWI24S Cs-134 0.34 1.98 3.19 14 U 2 20 MWIO9O Cs-134 0.384 2.82 528 14 U 2 21 MWso7S Cs-134 0o397 1.35 2.43 14 U 2 22 MWS02 Cs134 0.405 1.35 2.43 14 U 2 23 MWittS Cs-134 0.418 1.47 2.5 14 U 2 24 MWt020 . C-134 . 0.43 1.Ba 32 14 U 2 25 MwIo7s C-134 . 0.453 2.09 3.73 14 U 2 28 MWI2Ss Ce-134 0.5 2.12 3.93 14 U 2 27 MWII3S Ca-134 o.s4a 1.38 2.52 14 U 2 28 MWosS Cs-134 0.585 1.59 2.84 14 U 2 29 MWt030 Cs-34 0.e01 1.38 2.4a 14 U. 2 30 MWso8O Cs-134 0.818 1.7 Z83 14 U . 2 31 MWIO5S Cs-134 0.851 1.31 234 14 U 2 32 MWIo1S Cs-134 0.67 1.84 3.58 14 U 2 33 MWIO2S Cs-134 0.721 1a1 293 14 U 2 34 MW5O8SRepcate CS-134 0.827 201 3.75 14 U 2 35 MWIoso Cs-134 0895 1.32 2.47 14 U 2 36 MWIO8SReplicate Cs-134 0905 1.37 2.47 14 U 2 37 MWI C0-134 1.02 1.47 Z73 14 U 2 38 MW1O4S Cs-134 1.03 1.45 772 14 U 2 39 Mwli2s Cs-134 1.18 238 3.28 14 U 2 40 MWllOSRepriate Cs-134 123 3.33 4.59 14 U 2 41 MW1220 C-134 1.47 2.03 3.94 14 U 2 42 MWIO3S Cs134 181 2.18 3.88 14 U 2 43 Mwtoss Dupcate Cs-34 1.8 3.45 4.73 14 U 2 44 MWI23S Cs-134 1.84 2.8 3.47 14 U 2 45 MWI22S Cs-134 2.44 4.14 4.41 14 U 2 48 MWtOOO Cs-134 3.84 484 528 14 U 2 47 n 47 47 47 Average: 0.4190 1.9474 32194 Sdev 1.0169 0.7469 0.7890 Sdev 243% 38% 25%
| |
| Mic .1.75 1.25 2.03 Max: 3.84 4.84 528 Medai 0.418 1.84 32
| |
| | |
| Apperx>E2 June 2004 Rar* Tred Resnft
| |
| -. 2-sigma - ReqLired CoDc. TPU O M LbFa Volme Well D Ntade fpC~t) (DCtt) roCS,¶. rDoet) Lab FaVown v (1)
| |
| Cs-134 -201 3.18 428 14 U 2 OC 8bnk CS-134 e.0so8 2.02 3.65 14 U 2 CC Blank Ca-134 0.173 2.07 3.7 14 U 2 QC Stank Cs.134 0.478 1.48 2.5 14 U 2 rc 4 4 4 Average. .327 '2.1775 3.5525 Sdey: 1.1358 0.7110 0.70ee Sdev -347% 33% 20%
| |
| Mn: -. 0100 1.4800 2.s80 M-a 0.4780 3.1eW0 42800 Rank Results for June 2004 10
| |
| _. ftf.i14If{ . 4i4IlCil Cs-134
| |
| -Zero Mean o i llllili il~llIXi i461 4+1
| |
| .... t II- l. Sigm III,. I+2-Slgma
| |
| .l II. -Ave. MIDC O 0 .'
| |
| - 0. . ..
| |
| 0 10 20 30 40 Rank Order
| |
| | |
| AppendxE.2 June 2004 Rarh Trend Resutts 2-slgma Reqt*ed Conc- TPU MDC MDC AlqUmt Rank Wel ID Nuclde Will.) (tCa) (POL) (pCA.) Lab Flag Vo;w Orde MW105S Dup .ate Cs-137 .1.82 Z51 4.32 15 u 2 1 MW107[t CF-137 -1.42 213 3.61 15 u 2 2 MW124S CS-137 -0.912 1.91 3.22 15 u 2 3 MWi11D C N137 -0.838 1.17 1.94 15 u 2 4 MW12203 C-137 A758 1.88 3.28 15 u 2 5 MW3 Co-137 -a827 1.48 2.47 15 u 2 6 MWS03 CF137 -0.415 1.4 2.35 15 u 2 7 MW1tOS Cs-137 -0.409 1.22 2.03 1s u 2 8 MW 7S CO131 A372 2.37 4.08 15 u 2 9 MWI06D Cs-137 4302 1.22 2.11 Is u 2 10 MWI1IS CS137 *0.254 2 3.59 15 u 2 11 MWI Cs-137 4248 1.38 2.41 15 u 2 12 MWI145 CF137 -227 1.28 228 15 u 2 13 MW1OSS Cs-137 -0.215 1.89 3.43 15 u 2 14 MW507S Cs-137 -208 129 225 15 u 2 IS MWI13S Cs-137 41o06 1.27 220 15 u 2 18 MWIO2S CS-137 0 3.02 5.08 15 2 17 MWtO9t CF137 0 4.47 &77 15 2 18 MWtt2S CF-137 0 2.15 4.43 15 2 19 MW502 Cs-137- 0.00859 2.48 228 15 u 2 20 MW1C9S CS-137 0.03e2 1.18 2.08 15 u 2 21 MW102D Cs-137 0235 1.88 3.43- 15 u 2 22 MW105D Cs-137 0.318 129 233 15 u 2 23 MW2 CF137 0322 1.88 3.51 15 u 2 24 MWlOBSRepkase CF137 0.378 129 2.26 15 u 2 25 MW1M CON137 0.39 2.32 4.32 1S u 2 26 MWS07D Cs-137 0.474 1.31 239 Is u 2 27 MWIIOSRepicate CO137 0.528 2.31 4.23 15 u 2 28 MWIOS Cs-137 0.532 1.48 2.61 15 u 2 29 MW122S Cs-137 0.551 212 3.87 1S u 2 30 mws08m CS-137 0.557 1. 2.78 15 u 2 31 MWSO8S Cs-137 0.576 1.83 3.18 15 u 2 32 EOF2 Cs-137 0.80c 1.79 327 15 u 2 33 MWI0S Cs-137 0.812 2.43 2.21 1s u 2 34 MWils Cs-137 0.863 1.33 2.4 Is U 2 35 MW504 Cs-137 0.718 1.29 2.34 15 u 2 38 MWIO7S Cs-137 1.07 1.82 3.39 15 u 2 37 MWI25S CF-137 1.26 2.03 3.88 15 u 2 38 MWIOID Cs-137 1.38 1.81 3.52 15 u 2 39 MW505 Cs-137 1.42 1.84 3.12 15 u 2 40 MW103D Cs-137 1.44 2.07 223 15 u 2 41 MWios Cs-137 1.45 1.88 3.05 15 u 2 42 MWII4S Cs137 t.57 1.89 3.88 15 u 2 43 MW2Repcate Cs-137 1.84 1.85 3.31 15 u 2 44 MWSM SRepllcat Cs-137 1.8 1.95 3.79 15 u 2 45 MWi23S Cs-137 . u2.48F 1t9 3.93 15 u 2 48 MWIO3S Cs-137 7.5 5.54 3.33 15 2 47 m 47
| |
| * 47 47 Aveage: 0.4545 1.9145 32028 Sdev. 1.3512 0.7940 1.1427 Sdev 297% 41% 38%
| |
| Min -1.82 1.17 1.94 Max 7.5 5.54 a7n Mediam 0.322 1.88 3.22
| |
| | |
| Appencli E2 JAne2004 Rank Trend Resat 2-igmna Reqtred
| |
| . conc_ TPU moc MDC AlqUt Wel ID Nudide poC1L) (pCIfL) (Wcl) (DMt) Lab Flag Voue (L)
| |
| OC Blank Cs-137 .0.591 1.62 284 15 U 2 QC Blank Cs-137 .0.48 1.95 5139 15 U 2 OC Blank Cs-137 a05.41 128 22 15 U 2 aC Blank CS-137 1.01 1.97 3.73 15 U 2 n: 4 4 4 Average: 0.00 1.70 3.04 Sdev 0.73 0.33 0.67 Sdev -42372% 20% 22%
| |
| IMh: .0.59 126 220 Ilax: 1.01 1.97 .73 Rank Results for June 2004 15 10.
| |
| . .* Cs-137 c 5 -Zero Mean
| |
| , .- 2-Sigma 0 ~+2-Sigma'
| |
| -Ave. MDC o -5
| |
| --10 .
| |
| 0 10 20 30 40 Rank Order Rank Results for June 2004 10 0Cs-137 5 II1. .
| |
| * I I I.* .I I IlZ~oen Mean
| |
| ~I444t44444444-Zero 0 0 0 Sigma III II, . ~.+2-Sigma ro .I -Ave. MDC
| |
| -10 0 10 20 30 Rank Order
| |
| | |
| ApwaS EE2 km 2004 Rark Trend Resdts 2-sgma Regrred Con TPU MOC Moe AkIM R;rk WO ID Nucd (pOM) (pCLl i(pCLtL) (pCA.l Lab Flag Volw*
| |
| w L) Order MWI020 Eu-S12 *7.03 5.61 as? 50 U 2 1 MWI003 Ew-S2 -5.94 728 12 50 U 2 2 MWI125S E-152 -3.97 6.2 10.6 50 U 2 3 MW1065 Eu-152 -3.42 5.71 929 50 U 2 4 MW1O5SOi4caw Eu-152 .2.89 5.06 8.52 50 U 2 5 MW2Repcat Eu-152 .2.24 5.32 928 50 U 2 6 MWso6S Eu-152 .1.32 5.16 871 50 U 2 7 MWi02S EU-152 -1.28 4.2 7.1 so U 2 8 MWI16S Ea-152 -1.18 4.18 7.14 50 U 2 9 MWi11S Eu-152 -1.01 4.03 6.5 50 U 2 10 Mwtoss Eu-iS -0.975 3.54 5.99 50 U 2 11 MW3 Eu-S52 -0.884 4.31 7.42 50 U 2 12 MW507D Eu-1S2 -0.753 3.96 8.75 50 U 2 13 MW10s Eu-152 -. 699 3.97 6.82 50 U 2 14 MWS07S EU-152 .0.657 3.85 837 50 U 2 15 MWI03S Eu-152 .o.6 5.19 8.9 50 U 2 16 MW1IOSReplcate Eu-152 0445 7.38 1Z4 50 U 2 17 MW101D E-152 -0.267 6.05 101 50 U 2 18 MW50S0Rep oat Eu-152 -0.25 4.83 8.72 50 U 2 19 MW1070 Eu-152 -0.225 5.32 9.34 50 U 2 20 MWI17S EI5s2 -0.0575 6.31 11.2 50 U 2 21 MW112S Et-152 0.143 5.48 9.35 50 U 2 22 MWI23S Eu-152 0.148 5.52 9.42 50 U 2 23 MNWS06 Eu-152 0207 429 7.33 50 U 2 24 MWilos Eu152 0288 3.8 677 50 U 2 25 MW1030 Eu-152 0424 38 6.74 50 U 2 2e MWI00D Eu-152 0.42S 8.0e 10.7 50 U 2 27 MW505 Eu-152 0.542 3.97 6.92 50 U 2 28 MWI22S Eu-152 o.06W . 621 11.1 50 U 2 29 MWI14S Eu1s2 . 0.77 579 102 50 U 2 30 MW11OD Eu152 0.828 3.79 6.4 50 U 2 31 MW1EOSReplicate Eu152 0.993 388 6.78 50 U 2 32 MWIDO6 Eu-1s2 1.23 3.96 68.3 50 U 2 33 MW503 EC-152 1.34 4.0S 6.88 50 U 2 34 MWI24S Eu-1s2 1.35 5.43 6.91 50 u 2 35 MWt Eo-152 1.5 3.57 8.33 50 U 2 38 MW502- EU.152 1.64 3.67 6.62 50 U 2 37 MW101S Eu-152 2.1 4.98 9.04 50 U 2 38 MW504 Et-152 Z15 3.97 7.18 s5 U 2 39 MWIWS Eu-152 221 5.13 9.35 50 U 2 40 MWI05S Eu.152 2.86 4.15 8.44 50 U 2 41 MWI04S E-S152 3.01 4.16 728 50 U 2 42 MW113S Eu-152 3.33 3.7 8.6 50 U 2 43 MWI1OS Eu-152 3.57 429 8.59 50 U 2 44 MW1220 Eu-1s2 3.75 5.33 9.81 50 U 2 45 MW2 Eu-12 3.88 5.35 9.78 50 U 2 48 EOF2 Eu-152 4.12 s.54 10.2 50 U 2 47 ii 47 47 47 Average: o.1578 4.8470 8.3298 Sdev 2.3248 0.9a31 1.7309 Sdew. 1473% 20% 21%
| |
| Mki -7.03 3.54 5.99 Max 4.12 7.38 124 Meua UV207 4.83 8.52
| |
| | |
| Apperex E2 June 2004 Rarn Trend Restft 2-sigma Required
| |
| .Couc. TPU. - MDC MDC A t Wed ID Nut~de (POItL) (cCV) (oWCU) (o0C.) Lab Flag Vodae (L1 QC Blar Eu152 .239 4.07 6.07 0 U 2 OC 81a* Eu-152 -a249 5.07 8'58 50 U 2 QC e1ar* EuL152 0.521 5.3 9.31 50 U 2 QCCSW* Eu.152 2.13 5.65 ID4 50 U 2 n: 4 4 4 Average: 0.00 5.04 &59 Sdev. 1.88 069 1.84 Sdew 50091% 14% 21%
| |
| mIn: .239 4.07 e07 Max: 2.13 5.65 10.40 Rank Results for June 2004 15
| |
| -10 0 Eu-1 52 tft c -Zero Mean 0
| |
| c lip5* Sigma
| |
| -Ave. MDC 0 .10 0 10 20 30 40 Rank Order
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| | |
| Appendx E2 June 2004Rant Trend Resdt 2-sigma Reqnled Comc TPU MDC MDC AlkIt Rat Wel ICD Nudibd (pCIL) (Co) PClA) (pCVL) tab Fag Vchn e (L) Order MW503 E-154 -3.43 4.1 e.e1 so U 2 1 MWI07S Eo-154 411 5.47 926 50 U 2 2 MWlosOupICale Eu154 -2.95 7.68 13.7 50 U 2 3 MwO5m Eu-154 -2.45 4.65 S12 so U 2 4 MW3 Eu-154 -225 4.05 6.85 50 U 2 5 MW5080 EOu154 -2 4.5 e.57 50 U 2 8 MWIogS EL-154 .1.94 3.82 5.5 50 U 2 7 MWI03S Eo.154 -1.84 5.2 8.9 50 U 2 8 MWI11S EL-154 .1.74 4.11 6.99 50 U 2 9 MWI Eu-154 .1.42 4.1 7.13 50 U 2 10 MW102D Eu-154 .1.41 5.59 10.1 50 U 2 1t MWII35 Eu-154 .1.33 3.85 6.49 50 U 2 12 EOF2 Eu-14 -46os 3.94 727 50 U 2 13 MWIOO EU-154 -0717 5.85 11.2 50 U 2 14 MWI02S EOu154 -0.714 3.95 6.84 50 U 2 15 MWS02 Eu-154 8.e94 3.61 6.45 50 U 2 1t MWIlOSReplate EOu154 0572 5.09 9.3 50 U 2 t7 MWI030 Ew1S4 -a488 3.09 8.59 50 U 2 18 MWSW7S Eu-154 0325 3.49 6.33 50 U 2 19 MWI5so EOu154 0.0175 3.44 834 50 U 2 20 MWI1iS Eu-1N o.om 6.34 11.7 50 U 2 21 MWIO4S E-154 0.259 3.89 6.6 50 U 2 22 MWI0sS Eu-154 0.348 3.15 5.79 50 U 2 23 MWIOss E0u14 0.457 526 98S4 so U 2 24 MWlOSSReplcate Eu1S4 0.7 3.6 8.9 50 U - 2 25 MWI12S Eto154 0.712 4.67 9.11 50 U 2 26 MWI23S Eu154 0.979 4.73 9.27 50 U 2 27 MW124S Eu-154 1 4.36 82 50 U 2 26 MWI07D Eu-1$4 1.05 6.5 1Z3 50 U. 2 29 MW114S EU-154 1.31 4.87 9.61 50 U 2 30 MWI06S Eu-154 1.32 3.83 6.95 50. U 2 31 MWSosS Eu-14 1.39 4.77 9.4 50 U 2 32 MW2 Etb-154 1.6 4.82 9.56 50 U 2 33 MWIO8 Eu-154 1.74 3.31 851 50 U 2 34 MW1IO E*-14 2.09 3.74 7.19 50 U 2 35 MwII7s Eu-154 Z22 5.7 11.4 50 U 2 36 MWIOSO E15S4 224 7.2 13.9 50 U 2 37 MWSO6Replcato Eu-154 Z34 4.98 10.1 50 U 2 38 MWIOOS Eu-154 253 3.82 7.03 50 U 2 39 MwIIos EL-154 86e 4.74 9.18 50 U 2 40 MWIOI Eu-154 268 5.81 10.8 50 U 2 41 MW507o EL-14 z96 4.13 7.9 50 U 2 42 MWi2sS Eu.154 3.35 5.51 11.1 50 U 2 43 MW504 Eu154 3.4 5.38 6.5 50 U 2 44 MW1220 Eu-154 3.59 5.51 11.1 so U 2 45 MW122s ELu-4 3.6S . 5.81 10.8 50 U 2 46 MW2 Replicate E0,154 ,,8ee.' 4.32 10.2 50 U 2 47 47 47 47 Average: 0.4960 4.6891 8.84s5 Sdev: 2.148s 1.0324 Z1523 Sdev 433% 22% 25%
| |
| Mbi .3.43 3.15 5.5 Mac 6.8 7.6s 13.9 Medaac 0.457 4.65 82
| |
| | |
| Apperdx E.2 June 2004 Ra* Trend Results
| |
| - I : 24igma Required Co. TM mDC MDC AIQUt Wel ID Nudie fOCMI oCtttj (DCLU 10CUt'L IAb FLa Vokw(e Li-CC stark EuI154 .0747 5.04 - 9.4 50 U 2 aoc Bbnk Eu-154 .0.5t5 .25.15 9.69 50 - U 2 ac Ben* EuIF54 0.0444 '5.49 10.3 50 U 2 ac BLAnk Eu.154 453 4.04 754 50 U 2 ii 4 4 -4 Average: 0.83 ! 4.93 923 Sdev: Z49 0.62 .1.19 Sdev: 301% 13% 13%
| |
| Mit .0.75 41.04 ' 7.
| |
| Max 4.53 5.49 '10.30 Rank Results for June 2004 15
| |
| -10 o
| |
| S . , .1'.
| |
| .5 .11 i*Eu-154
| |
| $-Zero Mean 0 Sigma
| |
| - 42-Sigmai I ' !-Ave. MDC
| |
| -10
| |
| .5 0 10 20 30 40 Rank Order
| |
| * Alperdx E 2 Jue 2004 Ra* Trend Re4ts 2-sinma Req*ed Con TPU MDC MOC AlqjAt Rank Wed tQ Nudice (P02) (pCI&) (PM) (PCI) Lab Flag Vodve (LI Order EOF2 EU-155 -5.68 7.4 12 50 U 2 1 MW112S EU-155 -5.38 564 112 50 U 2 2 IWI10S Eu.155 .337 4.72 o01 50 U 2 3 MWI100 Eu-155 -3M4 5.9 9.55 50 U 2 4 MWI22S E1O55 -2.81 9.19 15.1 50 U 2 5 MW505 E1s55 -2.45 4.15 8.89 50 U 2 8 MWi17S EA-155 -2.22 9.14 15.1 50 U 2 7 MWII0 Eu-155 -2.17 4.77 82 50 U 2 a MWso7C Eul55 .t1.9 5.48 9.03 50 U 2 9 Re ate MWI10itS Eu.155 -1.69 514 8.48 50 U 2 10 MW2 Eu-155 .1.68 8.8 11.9 50 U 2 11 MWIO3 E1s55 -1.44 4.98 .41 50 U 2 12 MW3 E1s55 -1.4 8.34 104 s5 U 2 13 UW104S El55 .1.23 4.84 .37 50 U 2 14 MW1io Ew155 .1.15 42 .886 s5 U 2 15 MWXm8C EL,15S 4886 5.94 9.e8 50 U 2 18 MWs04 Eu-15 4.575 4.88 7.96 so U 2 17 MWIOS5 Ew1s5 -0388 5.18 9.06 s0 U 2 18 MW11JS Eu-155 40.381 4.84 841 s0 U 2 19 MW1220 E1s55 .0326 7.49 127 50 U 2 20 MW108S E-155 -0226 6.4U 10o7 50 U 2 21 MWIIIS Eu1-ss -02 4.6 8.03 50 U 2 22 MWI0sS E-lss 4109 5.33 8.89 s0 U 2 23 MWI14S E-Oss 0.0514 7.39 12z 50 U 2 24 MWI03S Eu-1s aL135 .76 112 50 U 2 25 MW123S Eu-1Os a191 7.12 12.6 50 U 2 26 MW108 E-lOs5 0.388 522 923 50 U 2 27 MWIoss Eu-Os5 o.673 8.73 12 50 U 2 28 MWIODS Eu-1Os 1.01 . 4.72 7.95 so U 2 29 MW105S DOkabe Eu-lOs 1.05 5.77 78 50 U 2 30 MW503 E-lss 1.8 4.54 8.04 50 U 2 31 MWIo1s Eu-155 2 553 9.72 50 U 2 32 MW5o2 Eu55 .Z48U 4.92 7s X0 U ,2 33 MW12SS Eu-155 2.71 8.59 14.S s0 . U . 2 34 MW1O7S E-155s Z74 7.48 12.8 s U - 2 35 MW1020 Eu-155 325 7.7 13.4 50. U 2 36 MaWsM Rep4icat E-lJS 327 8.74 12 X0 U 2 3t MWI1OSReplicate Eu-15s 3.38 8.34 151 50 U 2 38 IWX07S Eu-15S 3.86 4.88 8.42 50 U 2 39 MWI Eu155 39 4 3s94 8&94 s0 U 2 40 MW124S Eulss 4.87 69.3 1Z4 50 U 2 41 MWI02S Eta-lS 5.11 8.89 8.9 50 U 2 42 MW1010 E-lss S.14 7.58 . 12.6 50 U 2 43 MwsOss Eu-1ss 524 6.92 12.7 50 U 2 44 MWIo90 Eu-155 5.37 9.33 1a 0o U 2 45 MWIOo Eu-155 ?
| |
| V6.4s 5.97 1o.7 50 U 2 48 MW2ReM8cate Eu-1OS .885Y) 7.05 12.9 50 U 2 47 m 47 47 47 Avrae o.e886 &1921 10.5530 Sdev 3.0549 1.4346 z4705 Sdev 459% 23% 23%
| |
| Mui -5.68 3.94 6.69 Max 7.68 9.33 1l Mecla 0.0514 5.97 9.78
| |
| | |
| Appendix E.2 Jume2004 Rank Trend Result 2-"ilgm Reqd~ed
| |
| . Conc . TPU .. MDC mDC - '- Niquot We5 ID NLHCide 10CLL ItpCIII ioO)i noCutI Lanb aFb Vohhn f QC Blat Eu.155 4.05 8e.1 10.8 50 U 2 QC Blat Eu-155 487 7.e4 1Me 80 U '2 QC Blat Eu.155 3.5 4.11 7.35 50 U 2 QC Blink Eu-155 3.?2 523 9.78 so U 2 4 -4 .4 Average: 01150 5.7700 10.0775 Sdev 4.05M20 1.4892 Z1738 Sde: 3523% 26% 22%
| |
| Mim: .4.0560 4.1100 73500 Max: 3.e20c 7.8400 1Ec0 Rank Results for June 2004 15 10 0S5 *Eu-155
| |
| -Zero Meani 1111111+2-Sigma Sigma o0 0 10 20 30 40 Rank Order
| |
| | |
| ApprifdtE2 Je 2004 Rark Trend Results 2-sigma Required Conc. TPU MOC MDC Aqut Rank Wei to Nudide (PciL) fpCVLt (pCi&) (pCLt) Lob Flag Volurno (I1 Order MW1030 PU-238 -0.0644 a011r 0414 0.5 U - 02 MW1080Re,9e Pu23t 4.0193 0.0657 0247 0.5 U 02 2 MWIWro Pt23 o0.0134 0.0691 0252 0.5 U 02 3 MWIOSS Duplicate Pu238 4.00649 0.016f 0176 0.5 U. . 02 T 4
| |
| MWI03S Rqeplcate Pu-3 0.00102 0.054 0185 0.5 U 025 5 MW10S Pu-238 0.0161 0.114 0.294 0.5 U 025 0 kWIO6O PL,238 0O251 0.070e 0175 0.5 US 025 7 MWI04S PU.238 0.0504 0.126 0.293 0.5 U. 025 8 MW103S PL-238 0.0612 0.108 0.23 05 U 025 9 mW1085 PLO3= 0.0869 0.17 0392 o0 U 0.2 10 10 10 10 Average 0.0115 0.0912 M2888
| |
| .Sder 0.0410 0.O4 0.0844 Sder. 358% 48% 32%
| |
| Mtnc 4.0044 0.0186 0.175 MaW: 0.089 0T17 0.414 Mdat 0.tXO56 0.0M93 02496
| |
| * 2-sigma Required Conc TPU MDC MOC Altqrl Wett tO Nonde (pCUI) (DCLIL) (pCL-) (CLI.) Lab FLag Volurne (LI QC 1lark Pu-235 0.0o84 0.108 0.202 0.5 U 02 CCBlank I Pi238 4.0324 0.0259 a187 0.5 U 025 2 2 2 I Average 0.0185 0.0680 0.1945 Sdev e.o720 a008 0.0106 Sdev 389% 88% 5%
| |
| Virv 40.0324 0.0259 0.1870 Max 0.0894 0.1080 0.2020 Rank Results for June 2004 0.3 20.2 0.1I . I
| |
| * Pu-238 c0 1 .. , , -Zero Mean 0 1t4+-T-----t-I Sigma fJI' 'I'J +2-Sigma 3 -0.1 -Ave. MDC
| |
| -0.2
| |
| -0.3 0 5 10 Rank Order
| |
| | |
| Apperdlx E2 Jue 2004 Rank Traed Results 2-sigma Reqtred .'
| |
| Con. . TPU MDC MDC Aflqut Rank Wet ID NWM:fde (cC)L) (ItCIL) (PCat) '(pCI) Lab Flag Vodine CL) Order MvW105DRepncate Pu239.240 .0.27n 0.0268 0208 . 05 U 02 1 AW1o6S Pu-239,240 -00228 0.0223 0.172 .0.5 'U 025 2.
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| MWI05D Pu.239.240 40148 0.022 .0.18 0.5 U 02 3 MWI03S : Pu239,240 .0127 0.0175 0.158 05 u 025 .. 4 MWI03SRepkate Pu-239.240 0.00713 0.054 0.169 0.5 U 025 5 MWIO8O Pu.239.240 0.0125 0.0499 0.143 0.5 U 025 a MWIM5S Dupkate Pu.239.240 0.0388 0.103 0257 0.5 U 02 7 MWI05S Pu-239.240 0.062 0107 0221 05 U 02 8 MWIO4S Pu239.240 0.115 ,0.12 0.178 0.5 U 025 9
| |
| &IWI03D Pu239.240 0.123 0.139 - 0208 0.5 U 02 10 n: 10 .10 10 Average: 0.0279 0.0860 -0.1890 Sdev: 0.0554 0.0467 0.0340 Sdev: 198% 71% 18%
| |
| Mk .0.0272 0.0175 0.143 Max: 0.123 0.139 0257 M = 0.009815 0.05195 0179 2.slgma Reqtked Ccnc - TPU MDC MDC A t Well 10 Nudlde (PCVa) (Pata) WmC)t (pnCL) Lab bFla Volae (L)
| |
| OC Blank P.239,240 .0.0162 0.0183 0.15 0.5 U 0.25 OC Blank Pu-239,240 2. < 0.171 0.221. 0.5 U 0.2 M 2 2 2 Average: 0.089 0.0947 . 0.1855 Sdev: 0.1828 0.1080 0.0502 Sdev: 185% 114% 27%
| |
| Vin: -0.0162 0.0183 0.1560 Mai: 0.2140 0.1710 0.2210 Rank Results for June 2004 0.3 0.2E o.
| |
| 0.1
| |
| * Pu-239,240
| |
| , ,. -Zero Mean E o-2-Sigma 42-Sigma O -0.1 -Ave. MDC o .-0.2
| |
| -0.3 . . . . . .-
| |
| 0 5 10 Rank Order
| |
| | |
| Appadx E.2 Je 2004 Rank Trend Resfta 2-sigma Reqwre Coni. TPU MDC MkC Alquot Rank W.d In h~i-M. rdliq I MMC t) (pC t) (1,P) I ahFLa Vdanetl rVA mW1O3S I Pu-241 -825 0.25 14.5 I5 U 0.5 1 mW100S Pu-241 -4 87 15.l 15 U. 0.5 2 mW1060 Pu-241 -1.49 8S3 14.4 15 U 05 3 MW1I03S Repcale Pu-241 as9s 80.2 13.8 1I U . 0.5 4 lWtCSD Pw241 0 5.53 11.3 15 U 0.4 5 MW MO4S PwU24 0.6DA 8.41 14.4 15 U 0.5 a UW10O Repica" Pu-241 1.38 833 10.8 1s U 0.4 7 MW1030 Pu-241 4.81 .S1 11.4 `S U 0.4 8 MW1OSSpi~cate PU.241 8.14 B.59 11 15 U . 0.4' 9 mWIo5S Pu-241 C 3 7.85 13.1 15 U 0.4 1o rr 10 10 10 Average: 0.67 r7520 12.O Sdev 4.8918 0.9160 1.8838 Sder: 740% 12% 13%
| |
| Mlr 425 133 10.8 ma 8.32 8.7 15.1 Medan 0.34t5 7.s3s 13.45 2-sigma Reqited Coe. TPU MDC MDC A"qut Wei to Nucld (PCIt OLoCiLI (dCtI (DCIL4 Lab Flao Voltme (LI aC lank Pt-241 -9.32 0.68 15.3 15 U 05 O0 Blank Pt-241 1.21 2.1 4.77 15 U I e 2 2 2 ,
| |
| Average: 4.0550 5.7450 10.0150 Slev: 7.4458 4.1507 7.4458 Sdev: -184% 72% 74%
| |
| Min -9.3200 2.8100 4.7700 Mac 1.2100 S.600 15.3050 Rank Results for June 2004 20 15 0
| |
| * Pu-241 c 5. - Zero Mean 0-2-Slgma 0 +2-Sigma
| |
| -Ave. MDC C -10
| |
| -15
| |
| -20 0 5 10 Rank Order
| |
| | |
| Appex E2 JuLe 20C4 Rank Trend Restf 2.4lma Required Cor: TPU MDC M t R We" ID Nuclde (PCVLI (pCVL) (pM)L WNA)L Lab Flag Vdune (L) Order MWt12S Am-241 (gamma) -88 18.2 27.3 05 U - 2 1 mwm A.,-24 (ganrna) -tZ4 17.4 19.3 0.5 U 2 2 MW2 Repcae Am-241 (gamma) -11.9 143 23.9 0.5 U 2 3 MW102S Am-241 (gamma) -8.79 7.88 10.8 05 U 2 4 MW1IOSReocate An-241 (gamma) .7.51 13.3 213 0.5 U 2 5 MwIlls Am-241 (garma) -5.14 9.ii - 13.1 05 U 2 8 MW508 Am241 (gamma) .4.31 9.85 162 0.5 U 2 7 MW1O3S Am-241 (garma) .3. . 8.18 13.5 0.5 U 2 8 MWsosRepkate Ar-241 (gamma) .3.43 1t 172 0.5 U 2 9 MWso2 Am-241(gamma) .99 11.7 18.6 . 0.5 U 2 10 EOF2 Ar-241 (gamma) z78 10.6 18 0.5 U 2 1t MWII7S An-241 (garma) -z78s 18.3 27.5 0.5 U 2 12 MW2 An-24t (gamma) Z02 9.69 17.3 Os U 2 13 Mwl Am-241 (gamma) -1.81 235 4 0.5 U 2 14 MWlOSS Repkate Am-241 (gamma) .1.81 8.8 12.9 0.5 U 2 15 MWI9OD Am-241 (gamma) 1.6 114 19.1 0.5 U 2 18 MWI04S Anm.241(gamma) .1.39 7.12 12.6 0.5 U 2 17 MWI2sS Am-241 (gamma) .0.984 15.3 23 05 U 2 18 MWIOID Am-241 (garana) .0.e65 13.7 20.4 0.5 U 2 19 MWI0tSOSwcate Am241 (gamma) .0.466 3.55 6.07 os U 2 20 MW507D Am-241 (gamma) .42 8.97 13.8 0.5 U 2 21 MWII3S A-241 (gamma) -0.0689 7.55 122 05 U 2 22 MW1O2D Amn241 (gamm) 0.7068 1Z 19 0.5 U 2 23 MWIl0S Am.2411 (gamia) 0.753 2.45 422 0.5 U 2 24 MWIOIS Am.241 (gamma) 122 3.4 6.11 0.5 U 2 25 MWt22D Am-241 (gamma) 1.31 14.4 18.1 0.5 U 2 2e MWIIOD Arm241(gamma) 1.4 7.34 12 0.5 U 2 27 MWIOOD Am-241 (gamma) 1t81 3.52 822 0.5 U 2 28
| |
| - MWsos Am-241 (gama) 1.95 2.48 4.34 0.5 U 2 29 MW107D Am241 (gamma) 2.12 3.84 8.59 0.5 U 2 30 MW1o9S Arm241 (gamma) 2.95 7.67 12 0.5 U 2 31 MWtO5S Abnm241 (gamma) 2.96 7.87 132 0.5 U 2 32 MIW03D .Am.241 (gamra) -3.07 10.3 -- 181 . S0.5 U - 2 33 M/WlO7S Am-241(gamina) 3.32 10.8 18.5 0.5 U 2 34 MWtO185 AM-241 (gamma) 3.74 10.3 189 0.5 U 2 35 MWI06o Am-241 (gamma) 4.4 10.4 17.4 0.5 U 2 36 MWtOSD Arn241 (gamma) 4.62 10.4 17.4 0.5 U 2 37 MWtOOS Am-241 (gamma) 4.94 12.2 20 0.5 U 2 38 MW53 Am-241 (gamma) 5.17 9.57 13.5 0.5 U 2 39 MW507S Am-241 (gammna) 5.48 7.99 1Z4 0.5 U 2 40 MW508S Arn-241(gamma) 8.14 9.72 18.2 0.5 U 2 41 MWIt4S Ain241 (gamma) ee8 13.1 21 05 U 2 42 MWtO8S Am-241 (gamma) 9.75 15.7 19.6 0.5 U 2 43 MW504 Am-241 (gamnma)2S1.0l' . 7.82 12.9 0.5 U 2 44 MWt23S Am,-241(gawna) 12.9 18.8 29 0.5 U 2 45 MWt22S Am-241 (garnna) 13 18 28.8 0.5 U 2 46 MWI24S An-241 (gamnma) 192 243 24.1 0.5 U 2 47 r 47 47 47 Average: 0.7270 10.4191 18.1628 Sdev: 8.6622 4.7548 6.4197 Sdev: 918% 46% 40%
| |
| Min: .18.8 235 4 Max: 192 243 29 Medan: 0.753 1.3 17.4
| |
| | |
| Appedx E2 June 2004 Ran Trend Results 2-sigma Reqed Con. TPU MOC MOC Well 10 Ndide [(OCUL oaU
| |
| ((CVU (OClt)
| |
| Lab Fba Vokmie dI
| |
| _y . _ .. _ ,_,
| |
| OC Blank Am-241(gamma) J.18 15.4 22.8 0.5 U 2 OC Blark Am-241 (gamma) -1.42 131 21.7 0.5 U 2 QC Blank ArF-241(gamma) 1.21 10.9 1e.7 0.5 U 2 OC Blank Am-241(gamma) 4.76 6.22 11.4 0.5 U 2 4 4 4 Average: 43025 11.4050 1&1500 Sder 4.4328 3.9140 5.2240 Sd. .1485% 34% 29%
| |
| Mm -5.7e00 6.2200 11.4000 Max: 4.7600 15.4060 22.8000 Rank Results for June 2004 40
| |
| __ 30 111ll. r -Zeo Me1.
| |
| a 20 eb I II I I
| |
| * Am-241 (gamma) 10
| |
| -"Zero Mean 0
| |
| 1.1111 I, llllllil44 8 + +III,,l Sigma 11l110 C - MM+2-Sigm111a III +2-Sigma c -10 0C-20 I1-2-A1 Ie.'M11' I -Ave. MDC
| |
| -30
| |
| -40 .......... I.........I...........................
| |
| 0 10 20 312 40 Rank Order
| |
| | |
| i: -': :1'"-'' ;' '
| |
| Apperdx E2 June 2004 Ratk Trere Restfs 2-sigma Reqeked Corn TWU MDC MDC Ai Rar*
| |
| WelD I NucIde ' (oCCI) (pt (pP)
| |
| K) fo(Ct) Lab Flag Vol-u L) Order MWI03D Am-241 .0.0447 0.106 0.389 0.5 U 0.2 1 uWIMoS Ar241 -0.0255 0.0683i 0.264 0.5 IU 025 2 mW105S Af-241 -0.0224 0.0254 0.207 0.5 U 0.2 3 MWIo5S DWiate Ar241 4014 0.0724 .0264 0.5 U 0.2 4 MWI03S Am.241 0.0029 0.091 0.256 0.5 U 025 5 MW105O Arn-241 0.0272 ''0.142 ' 0.358 0.5 U 0.2 a MWtO35 Repl)ate An241 0.0525 0.147 o034 0.5 U ' 025 '7 MWI05D Repktc1 AM-241 0.05o4 0.101 ' 0.208 0.5 U 0.2 - a Mw04s Am-241 0.0588 0.03i 0 . 19 0.5 U 025 9 MW10O6 Am-241 0.0901 0.135 0.275 0.5 U 025 10 r 10 10 10 Average: 0.0182 0.0984 0.2731 Sdev 0.0454 0.0375 o0.S40 Sdev: 249% '38% 23%
| |
| Mirx .0.0447 0.0254 0.19 Mac 0.0901 0.147 0.309 Medam 0.01505 0.0974 0264 2-sigma Requdred
| |
| -Conc. MDC MUDC Alioeo WenlID Nucilda (opCVL (pOt) '(tC) (PCIM) LarbFlag Volume (LI oCBiark Ar-241 0.0784 0.155 0.341 0.5 U 02 C BMank An-241 -0.0053 0.059 - 0207 0.5 U 025 rr 2 2 2 Average: 0.0366 0.1070 02740 Sdev: 0.0592 0.0679 0.0948 Sdev. 162% 63% 35%
| |
| Mir -0.0053 0.0590 0.2070 Mac 0.0784 0.1550 0.3410 Rank Results for June 2004 0.3 o1 1 - -- lI I I l
| |
| * -Zero Mean 0
| |
| e 0 Sigma c- . .2-Sigma' I .0.1 -Ave. MDC 0
| |
| lu -0.20 ..
| |
| -0.3 0 5 10 Rank Order
| |
| | |
| Appelx E2 June 2004 Ratk Ted Resuits 2-sigma Reqtdred Conc TPU MDC MDC Aliqut Rank Wedl D Nuclide (OCA) (oCL&) (vCIA) (bl& LabFlag Vohune (Li Order MW103S Replicate Cen-242 -0.0428 0.0317 0222 - 0.5 U 025 1 MWI1os5 Cm-242 40.0309 0.0599 0234 0.5 U 025 2 MWI03D Cm-242 -0.0283 00297 0243 0.5 U 02 3 MW1oSS DLicat Cm-242 -0.025t 0.0289 0238 0.5 U 02 4 MW1015 Cm-242 -0.0128 0.0W53 0.158 0.5 U 025 5 MW1055 Cm-242 0 0.0861 0.0941 0.5 U 0.2 6 MWI05D Cm-242 0.00132 0.0717 0.24 0.5 U 0.2 7 MWI050 Replicate Cm-242 0.0319 0.0828 0.0886 0.5 U 0.2 8 MWI10S Cm-242 0.0449 0.0717 0.127 0.5 U 0.25 9 MW1048 Cm-242 0.0815 0105 021? 0.5 U 0.25 10 10 10 10 Average: 0.0001 0.0595 0.1858 Sdev 0.0350 0.0240 0.0831 Sdev: 48875% 40% 34%
| |
| Mh: -0.0428 0.0289 0.086S Max 0.081 0.105 0243 Medlam -0.0084 0.08535 02195 2sigma Required Com TPU MDC MDC Akquo4 Wedl Dw N1i1de loCLIt
| |
| .- w bnlIt fsCVl1%
| |
| . v_.__
| |
| /wtlmw_
| |
| v_.
| |
| t ahFla,
| |
| ,w__ iS Vo/unm iI w_.ws 0C BLat Cm-242 40322 0.0282 0.209 0.5 U 0.25 QC BSar Cm-242 -0.0242 0.0274 0.224 0.5 U 0.2 n: 2 2 2 Average: -0.0282 0.0278 0.2165 Sdev 0.0057 0.0008 0.0100 Sdew: -20% 2% 5%
| |
| MIC -0.0322 0.0274 02090 Max -0.0242 0.0282 02240 Rank Results for June 2004 0.3 J 0.2 Ci0.1 I *Cm-242 o
| |
| 0
| |
| .- Zero Mean 0 Sigma
| |
| +2-Sigma
| |
| -0.1 -Ave. MDC O -0.2
| |
| -0.3 0 5 10 Rank Order
| |
| 'I
| |
| | |
| Appendx E2 June 2004 Ra*k Trend Resuit 2-nma Required c I -cTPU MDC m- c Aliquot Ran W.d in NuMdid InIA I IDCU I Mr MMSIr I- h FLg Vdne, - IL) 0 MWIO6D Cm-243,244 0.O061 0.0952 0.38 0.5 U 025 1 MW103D , Cm243.2441 0.0619 0.0e39 0.349 0.5 -U 02 2 MW110S Cin243,244 .0.0s32 0.0968 0.342 0.5 U 025 3 MWI0MS Repicate Cm-243.244 .0.038 0.0914 *0291 0.5 U 0.25 I4 MW1108S Ci-243.244 .0.00375 0118 *0.341 0.5 U 02 5 MWI04S Cm-243.244 0.00184 0.0707 - 0.211 0.5 U 025 r'6 e MWI0so Repicate Cv-243,244 0.0103 0.107 0.29 0.5 'U 02 - 7 MW1103S CM-243244 0.0329 0.102 0.248 0.5 U 025 a MW10sI Can-243.244 0.084 0.153 0.35 0.5 U 02 9 MW105S Dulcute Cm-243.244 0.0o89 . 0.184 0.377 0.5 U 02 10 e 10 10 10 Average: -0.0085 0.1082 0.3184 Sdev 0.0531 ao 295 0.0s37 Sdev -816% 27% 17%
| |
| Min¢ O.O.881 0.0707 0.211 Max: 0.0889 c.184 0.377 Medan: -0.000965 0.0994 0.3415 2-sigma Required Concm: WU MDC MDC Aliquot Well ID Nualde tomt) 'fDCau (pCVlt (oCULI LaibFlaa Vdlurne (L) -
| |
| aC Blank Cm-243.244 .0.0434 0.0664 0.272 0.5 U 025 OC Blankw Cmr243244 00485 0.158 0.383 0.5 U 02 I
| |
| at 2 2 2 Average: 0.0818 0.1122 0.3275 Sdev. 0.0638 0.048 0.0785 Sdev 4101% !s 58% - 24%
| |
| Ml¢t .0.0434 '0.0684 0.2720 Max: 0.0485 0.1580 0.3830 Rank Results for June 2004 0.4 -.
| |
| _ 0.3 CILI 0o1 1 I -Zero Cm-243.244 Mean 0 -~--j-] Sigma
| |
| -0.1° l +2-Sigma o 2 I0 I -Ave. MDC 0 ' -0.2
| |
| -0.3
| |
| -0.4 0 5 10 Rank Order
| |
| | |
| Apperdx E2 Jrz 2004 R&A Terod ReuAls Reqrkd Cone. 1-sgma MDC MOC AnqUtr Ran Wed ID NorMs (uG&) TPU(uGLI (uGt) (tCA) Lab Flag Vdune (IL) Ordor MWI . Boman .00 - 0.54 is J . 1 MW3 Boron 5.67 0.54 15 J 2 MW1OMD Boron 10.4 - 0.54 15 . J. - 3 MW503 Boron 10.7 - 0.54 tS J 4 MW2 Repncale Boron 14 - 0.54 15 J S MW2 Boron 15.5 . 0.54 . 15 J MWIOS Boron 25.3 0.54 15 7 UWIOD. Boron 32.1 - 054 15 a MW507D Boron 87 0.54 15 9 MW503S Replicate Boron 41.8 - 0.54 15 . 10 MW508S Boron 41. - 0.54 15 11 MWS04 Boron 42.17 0.54 15 12 MWIi2S Boron 47.8 0.54 is 13 MW5075 Boron 52. 0.54 15 14 MW101D Boron 54 - 0.54 15 15 MW5S05 Boron 54.4 0.54 Is 1a MWills Boron S.5 - 0.54 . 15 I7 MWI03D Boron 57.1 0.54 15 13 UW105D Boron 60.8 - 0.54 15 19 EOF2 Boron 6e4 0.54 15 20 MWIO3 Boron 64.7 0.54 15 21 MW502 Boron 65.2 0.54 15 22 MW50D Boron 81 - 054 15 23 MW103S Boron 8.3 . 0.54 15 24 MW117S Boron 6as 0.54 15 25 MW1 5 Boron 6W8 0.54 15 28 MW10SSRepocate Boron 687 - 0.54 15 27 MW1235 Boron 90.8 - 0.54 15 28 MWI02S Boron 91.2 - 0.54 15 29 MWI020 Boron 67.1 - 0.54 15 30 MWI13S Boron 110 0.54 15 31 MW109S Boron 124 0.54 15 32 MW103S Boron 165 0.54 15 33 MWIOTS Boron 177 . 0.54 15 34 MWIO9 Boron 191 . 0.54 15 35 MW1220 Boron 223 0.54 15 36 MWI24S Boron 225 0.54 15 37 MW110D Boron 236 0.54 15 38 MW104S Boron 274 0.54 15 39 MWI1OS Boron 291 0.54 15 40 MW110SReplcate Boron 301 0.54 15 41 MW122S Boron 307 - 0.54 15 42 MWI25S Boron 445 0.54 15 43 MW105S Boron 484 - 0.54 15 44 MWI06S Boron 490 0.54 15 45 MW105l Dupgcale Boron 516 0.54 15 48 U114S Boron 1260 0.54 15 47 e 41 0 47 Average: 1552734 - 05400 Sdev 214.1698 . 0.0000 Sdev 138% - 0%
| |
| Mlt 5.08 0.54 Mac 1260 0 0.54 Medan 68.3 - 0.54
| |
| | |
| AppendxE2 Xme 2004 Ran Trend Remft Required
| |
| .' Cam tbma mm tMDC A" qtU(
| |
| Well 9D Nudlde (uGt) WU (tCA) (uGt) (uG&) Lob Flag Vokrne (L}
| |
| CC Blank Boro 0.789 0.54 15 .
| |
| OC Blank Boron 1 0.54 15 J XBCtank Domn I5 . 0.54 15 U OCBElank omn Is 054 15 U IC 4 0 4 Average: 0.3198 - 0.5400 Sdev. 7.7484 0.0000 Sdev: 93% 0%
| |
| l6111 0.7890 0.0000 0.5400 Max: 15.000O 0.0000 0.5400 Rank Results for June 2004 1400 1200 a 1000 c 800 0
| |
| 600 I
| |
| * 400 *0 00
| |
| -200 10 20 30 40 Rank Order
| |
| | |
| Appendix F Boron Time Series Plots
| |
| | |
| C (C. C.
| |
| Boron Concentration in MW-lOOD/S 1400 1200 1000 800 02 ., I
| |
| -07 100D
| |
| .C 0 1-aOOS' I..
| |
| 600 400 200 0
| |
| Jul-98 Dec-99 . ., Apr-01 Sep-02. . Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result. The Indicated value Isthe reported minimum detectable concentration.
| |
| | |
| Boron Concentration in MW-10ID/S 300 250 200 1
| |
| $ 101D C 150 0 1--w-101S 0
| |
| 100 50 ML--
| |
| 0 Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Samnpflng Event; Note: An open marker indicates a non-detect result. The indicated value is the reported minimum detectable concentration.
| |
| ( C C.
| |
| | |
| C C. C, Boron Concentration in MW-1 02DIS I 450 400 350 300
| |
| -j 250
| |
| , .102D 0 I.* 162S co 0 200 150 100 50 L-j 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Note: An open marker indicates a non-detect result The Indicated value
| |
| - Sampling Event - isthe reported minimum detectable concentration.
| |
| | |
| Boron Concentration in MW-103D/S 400 350 300 250 P gm C 200
| |
| + 103D 0 -5*- 103S 0
| |
| M 150 F 100 00,- M\1k 50 41 0 I -
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Note: An open marker indicates a non-detect result. The indicated value Sampling Event Isthe reported minimum detectable concentration.
| |
| ( C C
| |
| | |
| (7 ( (7 Boron Concentration in MW-104S - -
| |
| 350 300 250 2 200 In C -
| |
| 2 0
| |
| m 150 100 50 0 4-Juf-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 ESampling Eent Note: An open marker indicates a non-detect result The Indicated value is the reported minimum detectable concentration.
| |
| | |
| Boron Concentration in MW-105DIS 12000 10000 8000
| |
| -I I+* 105D C 6000 Ilos 105S M
| |
| 0 4000 2000 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| - 'EetNote: An open marker indicates a non-detect result. The indicated value Sampling Event ithe reported minimum detectable concentraton.
| |
| { C. ("
| |
| | |
| C a. C Boron Concentration in MW-106D/S 2500
| |
| -j
| |
| +4 106D I-2 -- 106S m
| |
| 0 I --- _ M Jul-98 Dec-99 AprA01 Sep-02 Jan-04 May-05 Sampling EVent Note: An open marker Indicates a non-detect result. The Indicated value isthe reported minimum detectable concentration.
| |
| | |
| Boron Concentration in MW-107D/S 300 250 200
| |
| -j I 107D I C 150 0 I *-107Sl 0
| |
| 100 50 Q.a 0
| |
| i1-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result. The indicated value is the reported minimum detectable concentration.
| |
| ( (
| |
| (_
| |
| | |
| ( C c Boron Concentration in MW-108S - --
| |
| 300
| |
| -j 0
| |
| c0o
| |
| ...,-9..
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Note: An open marker Indicates a non-detect result The Indicated value Sampling Event Is the reported minimum detectable concentration.
| |
| | |
| Boron Concentration in MW-109DIS 700 600 500 Z^ 400
| |
| $ 109Dl C
| |
| l_*-109Sl 0
| |
| m 300 200 100 0 4-Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 SEe Note: An open marker Indicates a non-detect result. The Indicated value amplng Isthe reported minimum detectable concentration.
| |
| C
| |
| | |
| ( ( (
| |
| Boron Concentration in MW-110D/S 600 500 400
| |
| -J tn.
| |
| . 300 2
| |
| co 200
| |
| .100 o 4-
| |
| . Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event. Note: An open marker indicates a non-detect result The indicated value
| |
| -- -¢ is the reported minimum detectable concentration.
| |
| | |
| ( C C I
| |
| ( ( 7 Boron Concentration in MW-115S 250 -
| |
| 200 -
| |
| 150 -
| |
| 0 0
| |
| 100 50 0*
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event
| |
| '( '' C (.
| |
| | |
| (c (7 C Boron Concentration in MW-117S 80 70-60 50 40-30 /
| |
| 20 10 Jul-98 Dec-99 Apr-1 Sep2 Jan-04 May-05 Sampling Event -.
| |
| | |
| Boron Concentration in MW-122D/S 350 300 250 j 200
| |
| : 0) *+ 122Dl
| |
| --- 122SI 0
| |
| al 150 100 50 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event
| |
| ( C. (,.,
| |
| | |
| Boron Concentration inMW-123S 120-100-80 60 40-20-0 Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| .Sampling Event
| |
| | |
| Boron Concentration in MW-124S 400 350 11A A lauuf I 250-a 200 0
| |
| 0 150 100 50 0 I Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 MaV-05 Sampling Event C C C.
| |
| | |
| C C (i*
| |
| Boron Concentration in MW-125S 600 500 .
| |
| 400 -
| |
| i 300 .
| |
| 0 200 -
| |
| 100 .
| |
| 0 Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event
| |
| | |
| Boron Concentration in AST-1 60 50 40
| |
| -i 0)
| |
| ^3 30 30 20 10 0 I-Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect resuit The indicated value is the reported minimum detectable concentration.
| |
| ( C C,
| |
| | |
| : ( C Boron Concentration in MAT SUMP 200 -
| |
| 180 -
| |
| 160 140 120 -
| |
| 3 100 W=,
| |
| 0 80 60 -
| |
| 40 20 -
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 Mai-05
| |
| - Samnlina Event.;
| |
| | |
| Boron Concentration in EOF 2 80 70 I&:
| |
| 60 50
| |
| -J C 40 0
| |
| to .W**
| |
| 20 10 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event
| |
| (
| |
| (
| |
| (
| |
| | |
| C Boron Concentration in TW-1 250 200 150 tM 0
| |
| 100 50 0 i-
| |
| 't41-QR Dec-99 Apr-01 Sep-02 Jan-04 -- - . May-05 Note: An open marker indloates a non-detect result. The Indicated value Sampling Event Is the reported minimum detectable concentation.
| |
| | |
| Boron Concentration in MW-13 60 50 40 c 30 0
| |
| 0 20 10 0 4-Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Note: An open marker indicates a non-detect result. The indicated value Sampling Event is the reported minimum detectable concentration.
| |
| C . c (
| |
| | |
| Appendix G Tritium Time Series Plots
| |
| | |
| C C C Tritium Concentration in MW-100D/S
| |
| -j C.,
| |
| 0.
| |
| I 01001) I ER I B-500S it Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 SInnpiln Event NoteI anopen marker indicates a non-detect result. The Indicated value Isthe reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW-101DIS 1200
| |
| -j U
| |
| : a. 0 101D E 1-S101S 1..
| |
| it.
| |
| I I Jul-98 Dec-99 Af r-01 Sep-02 Jan-04 May-05
| |
| .-. Sampling Event Note: An open marker indicates a non-detect result. The Indicated value Is the reported minimum detectable concentration.
| |
| ( (7 C
| |
| | |
| (C (7 (7 Tritium Concentration in MW-I02DIS 35,000-30,000 -
| |
| 25,000-
| |
| -J 20,000
| |
| -4102C P U102%'
| |
| - ,ooolA 0 -
| |
| Jul.98 Dec-99 Apr-a1 Sep-02 Jan-04 May-05
| |
| - - Sampling Event Note: An open marker Indicates a non-detect result The Indicated value Is the reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW 103D/S 25,000 20,000
| |
| -,w t 2 15,000 C.,
| |
| + 103D a.
| |
| I- - - 103S 10,000
| |
| 'W4 V
| |
| 5,000 M I w 0 I I I Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Note: An open marker indicates a non-detect result. The indicated value Sampling Event1 is the reported minimum detectable concentration.
| |
| (. C C
| |
| | |
| C (7 C Tritium Concentration in MW-104S
| |
| , )
| |
| 1200 1000 800
| |
| -j V < .,
| |
| C.,
| |
| E. 600 it 400 200
| |
| . 0 Ju1-98 Dec-99 Apr-01 Sw/>'\ Ap/S<* Sep-02 Jan-04 May-05 I-}
| |
| eI I ii- Sampling Event Note: An open marker Indicates a non-detect result. The Indicated value is the reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW-105DIS 160,000 140,000 120,000 100,000
| |
| -I U
| |
| : a. $ 105D E 80,000 -111 05SI a-I-
| |
| 60,000 40,000 20,000 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event
| |
| ( ( C(I r
| |
| | |
| ( (7 c Tritium Concentration in MW-106D/S 30,000 25,000 20,000 :I
| |
| -j
| |
| : 0. l-- 106D 15,000 I N106S a..
| |
| 10,000;
| |
| .I 5,000 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| - Sampling Event X
| |
| | |
| Tritium Concentration in MW-107DIS 1200
| |
| *1000 800
| |
| -j 0.
| |
| CS 600 l-O 107D I l_-107S 400 200 N1I?
| |
| 0 Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker Indicates a non-detect result. The indicated value is the reported minimum detectable concentration.
| |
| ( (, (
| |
| | |
| C( C Tritium Concentration in MW-108S 1200 1000 800
| |
| *E 600-400 200 -
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| . . .Sampling Event Note: An open marker Indicates a non-detect result. The indicated value Isthe reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW-109D/S 35,000 30,000 25,000
| |
| _ 20,000 X
| |
| a.
| |
| . E
| |
| = 15,000 10,000 5,000 04-Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker Indicates a non-detect result. The indicated value is the reported minimum detectable concentration.
| |
| (_ C C
| |
| | |
| C C C Tritium Concentration in MW-IllS, MW-112S, MW-113S 1200 1000 800
| |
| -j a.
| |
| 600 I-400 200 0 4-Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result. The indicated value isthe reported minimum detectable concentration.
| |
| ( -
| |
| ( C.
| |
| | |
| c (7 C Tritium Concentration in MW-115S 7000 6000 5000
| |
| -J 4000 i_ 3000 I-.
| |
| 2000 1000 0 4-Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result. The indicated value is the reported minimum detectable concentration.
| |
| ( c
| |
| | |
| C (: C Tritium Concentration in MW-117S
| |
| -J 0.
| |
| E Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| ; S: I samplini Event Note: An open marker indicates a non-detect result. The Indicated value is the reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW-122D/S 1000 900 800 700 600
| |
| -j
| |
| [122Dl E 500 --- 122SI 400 4.
| |
| 300 200 100
| |
| ,I I .I 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result The indicated value ai E Isthe reported minimum detectable concentration.
| |
| *C ( C
| |
| | |
| C Tritium Concentration in MW-123S
| |
| ; 400
| |
| -j C-
| |
| .2 Pt.
| |
| 0 I I I Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result The indicated value isthe reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW-124S 6000 5000 4000
| |
| -J C 3000 E
| |
| 2000 1000 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result. The indicated value isthe reported minimum detectable concentration.
| |
| (
| |
| ( (~
| |
| | |
| ( (
| |
| Tritium Concentration in MW-125S 2500 2000
| |
| - 1500 Ua. '
| |
| E I- 1000
| |
| * 500 0 l- - III Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| - Note, An open marker Indicates a non-detect result The indicated value Sampling Event Is the reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in AST-1 1200 1000 800
| |
| -J 0 0 400 200
| |
| .0 1-Ju1-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Note: An open marker Indicates a non-detect result. The indicated value Sampling Event is the reported minimum detectable concentration.
| |
| ( C((..
| |
| (
| |
| | |
| C, (I C Tritium Concentration In MW-EOF 2 1200 -
| |
| 1000 800 - l i-600-E 400 -
| |
| 200 -
| |
| 0 Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| .Sampling Event Note: An open marker Indicates a non-detect result. The indicated value Isthe reported minimum detectable concentration.
| |
| ( (_
| |
| r
| |
| | |
| (7 C (
| |
| Tritium Concentration in TW-1 1200 1000 800 I-j C.,
| |
| 600 I.-
| |
| 400 200 Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05
| |
| - 1 Sampling Event Note: An open marker Indicates a non-detect result The Indicated value Isthe reported minimum detectable concentration.
| |
| | |
| Tritium Concentration in MW-13 1200 1000 -
| |
| 800 /
| |
| C.,
| |
| 600 E
| |
| 400 200 0
| |
| Jul-98 Dec-99 Apr-01 Sep-02 Jan-04 May-05 Sampling Event Note: An open marker indicates a non-detect result The indicated value isthe reported minimum detectable concentration.
| |
| C. (_ (.
| |
| | |
| Appendix H Cesium-137 and Strontium-90 Time Series Plots
| |
| | |
| ( C, C.
| |
| Cesium-137 Concentration in MW-IOOD 9
| |
| 8 7
| |
| 6
| |
| -j 5
| |
| 0.
| |
| I.1 N.. 4 3
| |
| 2 I
| |
| 0 A A A A A A A A
| |
| ,o s 0 ,oP (P -,<o S*,< SP I?IS ,& ,05 ,05 9¢ . ,0 ,,S,0 4P3 qzotb,0 ,<04z l t-N,0 ZK.$k Note: An open marker Indicates a non-detect result. The Indicated value Is Sampling Event the reported'rn&nlmum detectable concentration.
| |
| | |
| Cesium-137 Concentration in MW-1OOS 8
| |
| 7 6
| |
| 5 4
| |
| C.,
| |
| 3 2
| |
| 1 0 1.. I , .I I ..I I ,, . ... i. II ,
| |
| g, &t &G<05§i, >qg5< ¢fi< 0 g?° Sfi$ S:C5aft t>,bC <04c S>Pd 0i* 5kR Zt. Gto&
| |
| Note: An open marker indicates a non-detect result The indicated value Is Sampling Event the reported minimum detectable concentration.
| |
| C (' (_
| |
| | |
| C (7- (
| |
| Cesium -137 and Strontium-90 In MW-101D 10.0 1.4 9.0 8.0 7.0 I A .1.2
| |
| *1.0
| |
| ;~~~ a C, 6.0
| |
| *0.8 _
| |
| 0.
| |
| 5.0 _9 Cs-1371 v0 Sr-90 0.6 CO-4.0 1 3.0 0.4 2.0-0.2 1.0 -
| |
| 0.0- 0.0
| |
| * - &0 &C R;)4; & ,P ,0P p ,-- ,5P - R @ 0 P-of 05z? e iR- ? ,@
| |
| 4z Note: An open marker Indicates a non-detect result The indicated value Is Sampling Event the reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 in MW-101S 10.0 1.8 9.0 P -1.6 8.0 1.4 7.0
| |
| - 1.2
| |
| -j 6.0 1-j C.,
| |
| 1- 5.0 ok --6 Cs-1 37l Cq
| |
| -0.808 °, TL l Sr-90l C.) 4.0 r/ / lm',
| |
| 3.0 a:::: - 0.6 2.0 j - 0.4 1.0 - 0.2 0.0 . ., . .. . ...
| |
| . . . .. . . . . O Sapin Event Note: An open marker indicates a non-detect result. The Indicated value is ampl E the reported minimum detectable concentration.
| |
| C ( C
| |
| | |
| (c c C Cesium-137 and Strontium-90 Concentrations in MW-102D a.
| |
| _ -i13 Cs-1 37 .
| |
| 0.8 .1 Sr-90
| |
| ,ps Af ,0P -
| |
| R f-as 5S5 - - SP p, - ,0 N,05 ', -,0 QP , N ,5--
| |
| : .~, ~Note: An open marker Indicates a non-detect result The Indicated value Is
| |
| . Event
| |
| - . - Sampling Event the reported minimum detectable c6ncentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-102S 12.0 1.4 1.2 10.0 1.0 8.0
| |
| :r U 0.8 ,
| |
| : 0. CL r 6.0
| |
| . I -- Cs-1 37l i) 0.6 It -- Sr-90
| |
| '\~~~ O /9 I/
| |
| *4.0 : " </R g 'Y/
| |
| 0.4 2.0 I) 0.2 0.0 1 I I, I I .I I , . , . , . I . I, . ,
| |
| . I
| |
| . , . , . 0.0 PR IQ I % go,& 59 &O ss, GO~ Spgf ,,dp Sp Od, g 0c bg ts A
| |
| . . - li E t Note: An open marker indicates a non-detect result. The indicated value Is S-.ampling Event the reported minimum detectable concentration c1 ( C-
| |
| | |
| (7 C (7 Cesium-137 and Strontium-90 Concentrations in MW-103D
| |
| .6 U
| |
| : 0. C.n 1-.
| |
| - I'
| |
| : 1to,
| |
| : 42. Sr-90 g0
| |
| (,
| |
| 0.00 .I o5 &dge <cel vQR "O O O,..N i,, a, ,, Q s &"-' ,P QAd ee;i
| |
| ~ c AtboJgo<
| |
| sr ", ,R & b O 4& ,..
| |
| Note: An open marker Indicates a non-detect result The Indicated value Sampling Event isthe reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-103S 100.0 20.0 90.0 18.0 80.0 16.0 II 70.0 14.0 60.0 12.0
| |
| -I' -
| |
| 0L 50.0 C.0 M-Cs-1371 CD I Sr-90 1
| |
| .I- v
| |
| . 40.0 ~ Al 8.0 v) 30.0 6.0 20.0 4.0 10.0 2.0 0.0 0.0 N cR% fA0 g3rflbN~OR e, ° 2 Q e tNft GsA NR Sampling Event Note: An open marker indicates a non-detect result The Indicated value Isthe reported rNinimum detectable concentration.
| |
| C ( C
| |
| | |
| C C Cesium-137 and Strontium-90 Concentrations in MW-104S
| |
| *10.00 5 9.00 4.5 8.00 4 7.00 3.5 Xi 6.00 3
| |
| .- j r
| |
| T- C.),
| |
| o 4.00 2 "'
| |
| 3.00 1.5 2.00 1.00 0.5 0.00 0 Note: An open marker Indicates a non-detect result The Indicated value Is Sampling Event the'reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-105D 16.00 1.6 14.00 1.4 12.00 1.2 10.00 I 0.
| |
| -o A 8.00 ii) 6.00 0.6 4.00 0.4 2.00 0.2 0.00 0 Note: An open marker indicates a non-detect result. The indicated value is Sampling Eventthe reported minimum detectable concentration.
| |
| ( ( (
| |
| | |
| C. (7 (7 Cesium-137 and Strontium-90 Concentrations in MW-105S 14.0 . 210.0 12.0- .180.0 10.0 .150.0
| |
| -j 8.0 .120.0 -.
| |
| C., C.,)i 1I-- a~ jECs-137j U,
| |
| C., 6.01 .90.0 -'M F:C,,
| |
| 4.0 60.0 2.0 30.0 An 0.0
| |
| -.- I - I , I - I - - I - , . I I . - - I . . . . . . . . . . . .
| |
| -cj11%
| |
| - P11% P -C 'N 1q, S§l, & Sv & 5§1 - SP -SP -- (P 0 . .4Z5 0 o, 5k 4, P, &,e 0 vs SO VO &"e <0 4 -s')" lingEvent Note:
| |
| V!P &"e qV vs 'sO An open markermn'detectable Indicates aconcentration.
| |
| . I Sam Sampling the reported rminimu non-detect result The Indicated value Is
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-106D 16.0 1.6 14.0 1.4 12.0 1.2 10.0- -I/ 1.0 l
| |
| -j
| |
| -i C.,
| |
| /:-7 /
| |
| 0-. 8.0 r., -
| |
| 6.0 -
| |
| 0.6 4,
| |
| 4.0 , \ N 0.4 e' -
| |
| 2.0 - 0.2 0.0 . I . . . . I . I I I . . I I . I I I I I . I 0.0 Sampling Event Note: An open marker indicates a non-detect result The Indicated value is the reported minimum detectable concentration.
| |
| ( C,
| |
| | |
| C C C Cesium-137 and Strontium-90 in MW-106S 20.0 20.0 18.0 it18.0 16.0 16.0 14.0 14.0
| |
| -j 12.0 12.0 I-V)
| |
| U, 10.0 '10.0 .
| |
| C-,
| |
| C-8.0 8.0 6.0 6.0 4.0 2.0 2.0 0.0 0.0 j . Q, IrgCNJq° <0S&° Q-b & G& Jo fo
| |
| ( <&
| |
| IS 4z- 4:5 0 4 -A5p 4zf , C,0 2 Sa n E n Note: An open marker indicates a non-detect result. The Indicated value Is
| |
| - .t am.n the reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-107D 12.0 1.8 10.0 1.5 8.0 1.2 C.,
| |
| ,co 6.0 0.9 1 iCs-137 0.
| |
| M.
| |
| is, C,,
| |
| 4.0 0.6 2.0 0.3 0.0 0.0 ge,C ZOQ,° Ve. ssbR o o,8
| |
| &95 ei<,c, vsR >:h° :9ocpv P, oe° gso :v Sampling Event Note: An open marker indicates a non-detect resulL The indicated value is the reported minimum detectable concentration.
| |
| c_ C
| |
| | |
| C C C Cesium-I137 and Strontium-90 Concentration-fs in MW-I107S 14.0- 3.0 2.7 12.0 10.0 7. 2.4 2.1
| |
| -j 8.0 A K
| |
| * 1.8
| |
| -j
| |
| /
| |
| (3 0.C I.,
| |
| .XR - .
| |
| * 1.5 .~ I~-137 U
| |
| T Sn 6.0
| |
| ..a;5-O r:90
| |
| .1.2 4.0 11 0.9 I
| |
| . I -
| |
| 2.0 'S yl 1/2 b---El 0.6 0.3 0.0 . I . . I I I I a . I . . . . I I . . I . I . . 0.0
| |
| ~,"'l / /// -14t@-
| |
| / _a
| |
| / /, 1,'~Pl C~
| |
| Sampling Event Note: An open marker Indicates a non-detect result. The Indicated value Is the reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 in MW-108S 10 9
| |
| 8 7
| |
| 6
| |
| -a 0.
| |
| 5 0 Sr-90 1fl-VI --ECs-137 U7 4
| |
| 3 2
| |
| I 0 I I . .. I I I I I I I I I I a
| |
| ,1,0,, "V aN',
| |
| <;e If Q)
| |
| S C Qvp b Adr^A Q) 5O I0 ', 'b>P'b t, N k 0.A C Pie y3 zo P $ 'j C4
| |
| -n Evnt Note: An open marker indicates a non-detect result. The indicated value is Sampling Event the reported minimum detectable concentration.
| |
| ( (
| |
| | |
| C C C Cesium-137 and Strontium-90 Concentrations in MW-109D 20.0 - 2.0 18.0 - 1.8 16.0 -- 1.6 14.0- 1.4 12.0 - 1.2 1 00 - .o U s-137l
| |
| '8.0 0.8.
| |
| 6.0 0.6 4.0 0.4 2.0 0.2 0.0 0.0 Note: An open marker Indicates a non-detect result. The Indicated value Is Samping E n the reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-109S 18.0 1 1.8 16.0 AI\ I 1.6 14.0 4-I L 1.4 12.0 /
| |
| F 4- - 1.2
| |
| -J Af- -1 iZ310.0 1.0 a.
| |
| O. 1--
| |
| C.8 Cs-1 37 vT 8.0 _ x 0.8 90 -- r9 C. U) 6.0 rL 0.6 4.0 z 0.4 Li wZ 2.0 1- 0.2 0.0 .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0.0
| |
| ,QP P N
| |
| 1'1 I 5§1,
| |
| -/' V ' cp" Public' ROD vs P
| |
| 1,b (,
| |
| VZO 0
| |
| &I- 0 e "(O 01 -SO 0 4Z 5%
| |
| C Sampling Event Note: An open marker indicates a non-detect result. The indicated value is the reported minimum detectable concentration.
| |
| ( ( (3
| |
| | |
| C C C Cesium-137 and Strontium-90 Concentrations in MW-IOD 14.0 3.5 12.0 3.0 10.0 2.5
| |
| -j 8.0 2.0 -~
| |
| C., 2- 5 .I Cs-137
| |
| .L l Sr-90 0
| |
| : 0. , fI - *. .
| |
| 6.0 1.5 co 4.0 1.0 2.0 0.5 0.0 0.0 I N'j N C~ & . & &
| |
| 5~, 5I P -pb
| |
| '° 9, ce'° o31>~Ce t 'Zo MAR S >39 &
| |
| & e Ce,<° 9<G 1.0111z~- 1t' &
| |
| &§ QP t q?<'bc, IhSampling Event - Note: An open marker Indicates a non-detect result. The indicated value Is the reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-110S 10.0 2.0 9.0 1.8 8.0 1.6 7.0 \I A Ix
| |
| : 1.4 6.0 r7 / 1.2
| |
| -j .
| |
| -j C., C.)
| |
| f 50 r-4 1.0 i-Cs-137
| |
| --E3 o 4.0 T- / I 0.8w
| |
| '.. l--Sr-90 l 3.0 I X~I 0.6 2.0 / Vx 0.4 1.0 0.2 0.0 T . T r I ...
| |
| 1 .
| |
| l .
| |
| I I I
| |
| I I . v v . i i I i
| |
| . A A n nJ N I
| |
| ,P,0 0 s-,,
| |
| PIV CPN, 4bo
| |
| ,e ? 5 5 0 "o &-e W ok, 0 0 41 N N 01 Note: An open marker indicates a non-detect result. The Indicated value is Sampling Event the reported minimum detectable concentration.
| |
| C (I (
| |
| | |
| C C C, Cesium-137 and Strontium-90 Concentrations In MW-111S 14.0 1.2 12.0 1.0 10.0 0.8 C.,
| |
| U 8.0 -A a
| |
| 0.6 - II I'- 1 1.
| |
| mn 6.0 U, 0
| |
| 0.4 4.0 0.2 2.0 0.0 0.0 J,0 &
| |
| RO 0 1S 0CP0 ,0s ,0 ,0 0 '0O-sR Sampling Event Note: An open marker Indicates a non-detect result The Indicated value Is the reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 in MW-112S 9.0 0 /A\0 8.0 7.0 6.0
| |
| *5.0 . / \
| |
| -E-Sr-90 0.
| |
| -- Cs-1 37 4.0
| |
| .I d 3.0 2.0
| |
| , , B Id * *
| |
| * 1.0 0.0 P"l, Sv 5§1, Sl, 0 01 0 0 0 0 0 0 0 d, 0 0 'Q 0 0 0 0 0 10q CPI 10 do 10", ? 4 vs 40 ls P 10 Cr io e S121",else 10 01 -. 011 Sampling Event Note: An open marker Indicates a non-detect result. The indicated value Is the reported minimum detectable concentration.
| |
| ( (' C
| |
| | |
| C ( C Cesium-137 and Strontium-90 Concentrations in MW-113S 12.0 1.8 10.0 1.5 8.0 1.2
| |
| -j C., C.,
| |
| 6.0 e) ItI C.
| |
| 4.0 0.6 2.0 0.3 0.0 0.0 cw TN tnAdlce Rke a nn-d ct re3J TheindlcatedvaIuels Sampling Event the reported minimum detectable concentration.
| |
| | |
| - / (
| |
| C c C Cesium-137 and Strontium-90 in MW-115S 4.8 4.2 3.6
| |
| -j 3.0 0.
| |
| 'C.)
| |
| 2.4 QL-~M Cs-1 37 In.
| |
| M.
| |
| v- ; S 90 -^.
| |
| en 1.8 1.2 0.6 0.0
| |
| . 1 <i
| |
| - , o--,o- -O ,--&o o-&- &,oe , 'I, b~0 N,5a, 05bs - 0 - 5k ,0 SE nt Note: An openminimum the reported marker indicates a nondetect result. The Indicated value Is detectable concentration.
| |
| | |
| Cesium-137.and Strontium-90 in MW-117S 10.0 2.0 9.0 1.8 8.0 1.6 7.0 X\
| |
| \ 1.4 6.0 1.2
| |
| -j 0
| |
| : 0. C.)
| |
| 1-. 5.0 0a- -i3-Cs-137l Cl en. l0 r s 1 4.0
| |
| / V // --E 3.0 .0.6 2.0 -0.4 1.0 0.2 0.0 . . . . . . . . . . . . . . . . . . . . 0.0
| |
| ,cW c~,
| |
| dAd 49& ,<e', V0srQ Mob , &? 4U& 'O, Q S§ Sampling Event Note: An open marker Indicates a non-detect result. The Indicated value is the reported minimum detectable concentration.
| |
| C. C. (.
| |
| | |
| C C C Cesium-137 and Strontium-90 Concentrations in MW-122D 14.0 3.5 12.0 3.0 10.0 2.5 j 8.0 a.
| |
| I .- CL
| |
| ( 6.0 U
| |
| 4.0
| |
| .,-' "Cs'1. 1.0 2.0 -0.5 0.0 4 I p0.0
| |
| * - ,ob--- ,b - - v
| |
| * Sampling Event n E n
| |
| - the Note: An open marker indicates a non-detect result:The Indicated value is reported minimum detectable concentration.
| |
| | |
| Cesium-137 and Strontium-90 Concentrations in MW-122S 12.0 2.0 1.8 10.0 i\\ ' A 1.6 1.4 8.0
| |
| -J 1.2 0.
| |
| a.- 6.0 1.0 OX I El CS-137l C,
| |
| U)
| |
| C., /\ / " c?
| |
| S-
| |
| -- Sr-90I 0.8 U) 4.0 0.6 0.4 2.0 0.2 0.0 0.0
| |
| ¢6 Q(9O n 92 3& ~91 &I (9) l 0 0 0 5z E :r(Z INN 4z k "I Sampling Event Note: An open marker indicates a non-detect result The indicated value is the reported minimum detectable concentration.
| |
| (7 ,,(
| |
| (
| |
| | |
| C C.
| |
| Cesium-1 37 and Strontium-90 Concentrations in MW-123S 12.4DO - 1.8 10;. 00 1 1.5 8.1DO 1.2
| |
| -J C.,
| |
| X0. C.,
| |
| I' 6.'00 / 0.9 X; CS-137 C ..
| |
| as Cn-L4-Sr-90 4.'00 D 0.6 2.Z00 . 0.3 0.'.00DO I b -. bI I O0 0
| |
| -SampngSaEventhe gEvent Note: An open marker Indicates a non-detect result. The Indicated value is reported minimum detectable concentration.
| |
| | |
| (
| |
| C C C Cesium-137 and Strontium-90 Concentrations in MW-125S
| |
| . 8.0 \ 7.0 7.0 6--
| |
| .0 6.0 5 -.
| |
| 0 5.0
| |
| -J C.,
| |
| 1fi 4.0 , . , -- 4.0 ~
| |
| g I-19-Cs-1371 Ii) 3.0 Cr6' 3.0
| |
| --2.0 2.0 1.0 1.0 0.0 I I I I II -0.0 Note: An open marker Indicates a non-detect result The Indicated value is Samping vent the reported minimum detectable concentration.}}
| |
