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| {{#Wiki_filter:ZION STATION RESTORATION PROJECT FINAL STATUS SURVEY RELEASE RECORD SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C REVISION 1 | | {{#Wiki_filter:}} |
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C PREPARED BY / DATE: Robert Yetter III Final Status Survey Specialist REVIEWED BY / DATE: Robert Yetter Director, Radiological Site Closure APPROVED BY / DATE: Sarah Roberts Vice President, Radiological Programs
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| [2]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C TABLE OF CONTENTS
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| : 1. EXECUTIVE
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| ==SUMMARY==
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| ................................................................................................... 7
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| : 2. SURVEY UNIT DESCRIPTION ......................................................................................... 7
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| : 3. CLASSIFICATION BASIS .................................................................................................. 8
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| : 4. DATA QUALITY OBJECTIVES (DQO) ......................................................................... 10
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| : 5. SURVEY DESIGN .............................................................................................................. 15
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| : 6. SURVEY IMPLEMENTATION........................................................................................ 22
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| : 7. SURVEY RESULTS............................................................................................................ 23
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| : 8. QUALITY CONTROL ....................................................................................................... 32
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| : 9. INVESTIGATIONS AND RESULTS ............................................................................... 33
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| : 10. REMEDIATION AND RESULTS ..................................................................................... 33
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| : 11. CHANGES FROM THE SURVEY PLAN ....................................................................... 33
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| : 12. DATA QUALITY ASSESSMENT (DQA) ........................................................................ 34
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| : 13. ANOMALIES....................................................................................................................... 34
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| : 14. CONCLUSION .................................................................................................................... 34
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| : 15. REFERENCES .................................................................................................................... 35
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| : 16. ATTACHMENTS ................................................................................................................ 36 ATTACHMENT 1 - FIGURE AND MAPS ............................................................................... 37 ATTACHMENT 2 - SCAN DATA ........................................................................................... 43 ATTACHMENT 3 - CONSULTATION TRIGGERS FOR RESIDENTIAL AND COMMERCIAL/INDUSTRIAL SOIL CONTAMINATION ............................... 52 ATTACHMENT 4 - SIGN TEST ............................................................................................. 54 ATTACHMENT 5 - QC SAMPLE ASSESSMENT ..................................................................... 56 ATTACHMENT 6 - GRAPHICAL PRESENTATIONS ................................................................ 59 ATTACHMENT 7 - SAMPLE ANALYTICAL REPORTS ............................................................ 66 ATTACHMENT 8 - EBERLINE ANALYTICAL REPORTS ................................................... 393
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| [3]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C LIST OF TABLES Table 1 - Dose Significant Radionuclides and Mixture.......................................................................... 12 Table 2 - Base Case DCGLs for Surface Soils (BcDCGLSS) ................................................................ 13 Table 3 - Base Case DCGLs for Subsurface Soils (BcDCGLSB) .......................................................... 13 Table 4 - Operational DCGLs for Surface Soils (OpDCGLSS) ............................................................. 14 Table 5 - Operational DCGLs for Subsurface Soils (OpDCGLSB) ....................................................... 14 Table 6 - Surrogate Ratios ...................................................................................................................... 15 Table 7 - Investigation Levels ................................................................................................................ 17 Table 8 - Systematic Sample Measurement Locations ........................................................................... 19 Table 9 - Synopsis of Survey Design ..................................................................................................... 21 Table 10 - Instruments and Detectors ..................................................................................................... 23 Table 11 - Synopsis of Scan Results....................................................................................................... 24 Table 12 - Summary of Gamma Spectroscopy Results for Surface Soil Samples Comprising the Statistical Sample Population ............................................................................................... 26 Table 13 - Summary of Gamma Spectroscopy Results for Investigation/Judgmental Surface Soil Samples ................................................................................................................................. 27 Table 14 - Summary of Gamma Spectroscopy Results for Subsurface Soil Samples............................ 27 Table 15 - Off-Site Analysis Results ...................................................................................................... 28 Table 16 - Summary of Gamma Spectroscopy Results for QC Soil Samples ........................................ 30 Table 17 - Sum of Fractions for Individual Systematic Surface Soil Samples, when compared to the OpDCGLs ................................................................................................................... 30 Table 18 - Sum of Fractions for Investigation/Judgmental Surface Soil Samples, when compared to the OpDCGLs ................................................................................................................... 31 Table 19 - Sum of Fractions for Individual Subsurface Soil Samples, when compared to the OpDCGLs ............................................................................................................................. 32 Table 20 - Sum of Fractions for Individual QC Soil Samples, when compared to the OpDCGLs ........ 32 Table 21 - Basic Statistical Properties of Systematic Sample Population .............................................. 32 Table 22 Relocated Systematic Sample Locations............................................................................... 34 LIST OF FIGURES Figure 1 - Class 3 Open Land Survey Units from Figure 2-6 of the LTP ................................................ 8 Figure 2 - The Four Class 1 Open Land Survey Units Created from the Original Class 3 Survey Unit 10221B .............................................................................................................. 10
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| [4]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C LIST OF ACRONYMS AND ABBREVIATIONS ALARA As Low As Reasonably Achievable AMCG Average Member of the Critical Group BcDCGL Base Case Derived Concentration Guideline Level BcSOF Base Case Sum of Fractions C/LT Characterization/License Termination cpm Counts per minute DQO Data Quality Objective DCGL Derived Concentration Guideline Level EMC Elevated Measurement Comparison FSS Final Status Survey GPS Global Positioning System HTD Hard-to-Detect HSA Historical Site Assessment IC Insignificant Contributor LBGR Lower Bound of the Gray Region LTP License Termination Plan MARSSIM Multi-Agency Radiation Survey and Site Investigation Manual MDC Minimum Detectable Concentration MDCR Minimum Detectable Count Rate NAD North American Datum NaI Sodium Iodide OpDCGL Operational Derived Concentration Guideline Level OpSOF Operational Sum of Fractions QC Quality Control RA Radiological Assessment RE Radiological Engineer ROC Radionuclides of Concern SOF Sum of Fractions
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| [5]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C TEDE Total Effective Dose Equivalent TSD Technical Support Document UBGR Upper Bound of the Gray Region VSP Visual Sample Plan ZNPS Zion Nuclear Power Station ZSRP Zion Station Restoration Project
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| [6]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
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| : 1. EXECUTIVE
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| ==SUMMARY==
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| This Final Status Survey (FSS) Release Record for Survey Unit 10221C, South of Protected Area - Inland, has been generated for the Zion Station Restoration Project (ZSRP) in accordance with ZionSolutions procedure ZS-LT-300-001-005, Final Status Survey Data Reporting (Reference 1) and satisfies the requirements of Section 5.11 of the Zion Station Restoration Project License Termination Plan (LTP) (Reference 2).
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| An FSS package (L1-10221C-F) was developed in accordance with ZionSolutions procedure ZS-LT-300-001-001, Final Status Survey Package Development (Reference 3), the ZSRP LTP, and guidance from NUREG-1575, Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) (Reference 4).
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| This open land survey unit has a MARSSIM classification of one. A survey plan was designed based upon use of the Sign Test as the nonparametric statistical test for compliance. Both the Type I () and Type II () decision error rates were set at 0.05. Seventeen (17) systematic surface soil samples were acquired from the survey unit. In addition, surface scanning was performed on 100% of the total surface area in the survey unit under the FSS Sample Plan. No areas of elevated activity were detected during the scans under the FSS Sample Plan. However, scans were performed earlier under a Radiological Assessment (RA) on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas one meter beyond the ballast gravel. The RA survey identified two (2) small areas of elevated activity (see Section 9 for further discussion). The analytical results for all soil samples (systematic and investigation) taken in survey unit 10221C indicated that the Sum of Fractions (SOF) for each sample, when compared to the Operational Derived Concentration Guideline Levels (OpDCGL), was less than 1.0. For the systematic samples, the maximum Operational SOF (OpSOF) was 0.262 with a mean OpSOF of 0.067. For the systematic samples, the mean Base Case SOF (BcSOF), when the analytical results were compared to the Base Case DCGLs (BcDCGL), was 0.017, which results in a dose assigned to the survey unit of 0.427 mrem/year Total Effective Dose Equivalent (TEDE).
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| Therefore, the null hypothesis is rejected and survey unit 10221C is acceptable for unrestricted release.
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| : 2. SURVEY UNIT DESCRIPTION Survey unit 10221C, South of Protected Area - Inland, is a Class 1 open land survey unit and is 1,959 m2 in size. It is bounded on the west by survey unit 10221B, the east by survey unit 10221D, the north by survey units 10209C thru 10209E, and the south by survey units 10220H and 10220I.
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| The topography of the survey unit is mainly flat with some small dips and depressions. The soil is mostly loam. A rail spur, with a ballast made up of gravel, runs through the southern half of the survey unit.
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| [7]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Illinois State Plane System North American Datum (NAD) 1983 East. The reference coordinates associated with the sample locations in this survey unit are presented in Table 8.
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| : 3. CLASSIFICATION BASIS Survey unit 10221C was classified in accordance with ZionSolutions procedure ZS-LT-300-001-002, Survey Unit Classification (Reference 5).
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| The area encompassing this survey unit was described as South of Fenced Area - Lakeshore and was located within survey unit 10221 as identified in Figure 4 of the Zion Station Historical Site Assessment (HSA) (Reference 6). Subsequently, this area was described as South of Protected Area - Inland (survey unit 10221B) in Table 2-29 and Figure 2-6 of the ZSRP LTP which is replicated below as Figure 1. This area was initially classified in both the HSA and LTP as Class 3.
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| Figure 1 - Class 3 Open Land Survey Units from Figure 2-6 of the LTP
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| [8]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The HSA states that this area contained a parking area. It also discusses the potential for low levels of radiological contamination due to elevated environmental sample results from the 1970s. The elevated environmental samples appeared to have consisted primarily of tritium with the highest concentration (80 pCi/ml) found in the south ditch. The source was believed to be backup from storm drains that tied into the south Oil Separator and the Fire Sump system.
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| A Characterization Survey was performed in May and June of 2013 for the Class 3 survey unit 10221B. The following data was obtained:
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| * Five (5) judgmental surface samples taken in the drainage ditch on the east side of the survey unit.
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| * Twenty (20) random surface samples and two (2) random subsurface samples.
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| * One (1) investigation surface sample and one (1) investigation subsurface sample taken in an area identified by a scan alarm.
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| * NaI walkover scans of approximately 26% of the survey unit.
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| The results of the characterization survey were:
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| * Two (2) of the five (5) judgmental surface samples were positive for Cs-137 with the highest activity being 0.068 pCi/g.
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| * All twenty (20) of the random surface samples and the two (2) random subsurface samples were less than the Minimum Detectable Concentration (MDC) for the Radionuclides of Concern (ROC).
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| * The one (1) investigation surface sample and one (1) investigation subsurface sample were both <MDC for the ROC.
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| On July 15, 2016, due to changing radiological and operational conditions brought about by site decommissioning activities inside or adjacent to this area, survey unit 10221B was reclassified as a Class 1 open land survey unit, and divided into 4 survey units: 10221A, 10221B, 10221C and 10221D to comply with the survey unit size recommendations from MARSSIM Section 4.6.
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| The following figure shows the boundaries of the resulting Class 1 survey units. The change in classification was a conservative response which ensured that the survey unit was surveyed with the appropriate rigor.
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| [9]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Figure 2 - The Four Class 1 Open Land Survey Units Created from the Original Class 3 Survey Unit 10221B A Radiological Engineer (RE) and a Characterization/License Termination (C/LT) Supervisor performed a visual inspection and walk-down of the survey unit on July 24, 2019, prior to performing FSS. The purpose of the walk-down was to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.
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| A final classification assessment was performed in accordance with procedure ZS-LT-300-001-002, Survey Unit Classification as part of the survey design for FSS. The assessment confirmed that survey unit 10221C was correctly classified as Class 1.
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| : 4. DATA QUALITY OBJECTIVES FSS planning and design hinges on coherence with the Data Quality Objective (DQO) process to ensure, through compliance with explicitly defined inputs and boundaries, that the primary objective of the survey is satisfied. The DQO process, utilized in accordance with MARSSIM, is described in the ZSRP LTP. The appropriate design for a given survey is developed using the DQO process as outlined in Appendix D of MARSSIM.
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| The DQO process incorporated hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline
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| [10]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis, was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would indicate that residual activity within the survey unit does not exceed the release criteria.
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| Therefore, the survey unit would satisfy the primary objective of the FSS sample plan.
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| The primary objective of the FSS sample plan is to demonstrate that the level of residual radioactivity in survey unit 10221C does not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).
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| ZionSolutions Technical Support Document (TSD) 11-001, Technical Support Document for Potential Radionuclides of Concern During the Decommissioning of the Zion Station (Reference 7), established the basis for an initial suite of potential ROC for the decommissioning of the Zion Nuclear Power Station (ZNPS).
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| ZionSolutions TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms (Reference 8), was written to refine the initial selection of ROC for decommissioning at the ZSRP. The list of ROC was evaluated using Containment and Auxiliary Building concrete core analysis data to evaluate the dose significance of each radionuclide in the end state model.
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| Section 4.4 of TSD 14-019 evaluated the results of the characterization data of surveys taken of soils. The following conclusion was reached: The results of surface and subsurface soil characterization in the impacted area surrounding Zion indicate that there is minimal residual radioactivity in soil. Essentially all of the soil results were reported as non-detectable. Other than Cs-137 at very low levels, and Co-60 at a concentration of 0.24 pCi/g in one sample, the results for all radionuclides were less than MDC. Therefore, the direct determination of radionuclide mixture fractions for initial suite radionuclides in soil is not technically feasible due to the MDC biasing issues discussed above. Based on a generalized assumption that the contaminated water that caused concrete contamination would be similar to the source of soil contamination, the ROC and radionuclide mixture derived for the Auxiliary Building concrete was considered to be reasonably representative of soils for FSS planning and implementation.
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| [11]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The ROC for surface soils are listed in Table 1 below (from Table 5-2 of the LTP):
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| Table 1 - Dose Significant Radionuclides and Mixture Auxiliary Building Radionuclide % of Total Activity (normalized)(1)(2)
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| Co-60 0.92%
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| Ni-63 23.71%
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| Sr-90 0.05%
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| Cs-134 0.01%
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| Cs-137 75.32%
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| (1) Based on maximum percent of total activity from Table 20 of TSD 14-019, normalized to one for the dose significant radionuclides (2) Does not include dose significant radionuclides for activated concrete (H-3, Eu-152, Eu-154).
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| A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of DCGLs. The DCGLs represent average levels of radioactivity above background levels and are presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soils.
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| Surface soil is defined as soil residing in the first 0.15 m (6 inches) layer of soil. A subsurface soil category, which is defined as a layer of soil beginning at the surface but extending to a depth of 1 m, is also assessed to allow for flexibility in compliance demonstration if contamination deeper than 0.15 m is encountered. Site-specific DCGLs for soil were calculated for both the 0.15 m and 1 m thicknesses. Based on characterization data and historical information, there are no expectations of encountering a source term geometry that is comprised of a clean surface layer of soil over a contaminated subsurface soil layer. ZionSolutions TSD 14-011, Soil Area Factors (Reference 9) and LTP, Section 6.8 provide the exposure scenarios and modeling parameters that were used to calculate the site-specific DCGLs for soils (referred to as BcDCGL in this Release Record).
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| At ZNPS, compliance is demonstrated through the summation of dose from four distinct source terms (basements, soils, buried pipe and groundwater) for the end-state. Basements are comprised of the summation of four structural source terms (surfaces, embedded pipe, penetrations and fill). When applied to soil, the DCGLs are expressed in units of activity per unit of mass (pCi/g). The unity rule is applied when there is more than one ROC. The measurement results for each singular ROC present in the mixture are compared against their respective DCGL to derive a dose fraction.
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| [12]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The surface and subsurface soil BcDCGLs for the unrestricted release of open land survey units are listed in Tables 5-5 and 5-6 of the LTP and are reproduced below in Table 2 and Table 3, respectively. The Insignificant Contributor (IC) dose percentage of 10% was used to adjust the DCGLs in soils to account for the dose from the eliminated IC radionuclides.
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| Table 2 - Base Case DCGLs for Surface Soils (BcDCGLSS)
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| Surface Soil DCGL Radionuclide (pCi/g)
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| Co-60 4.26 Cs-134 6.77 Cs-137 14.18 Ni-63 3,572.10 Sr-90 12.09 Table 3 - Base Case DCGLs for Subsurface Soils (BcDCGLSB)
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| Subsurface Soil Radionuclide DCGL (pCi/g)
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| Co-60 3.44 Cs-134 4.44 Cs-137 7.75 Ni-63 763.02 Sr-90 1.66 Each radionuclide-specific BcDCGL is equivalent to the level of residual radioactivity (above background levels) that could, when considered independently, result in a TEDE of 25 mrem/year to an Average Member of the Critical Group (AMCG). To ensure that the summation of dose from each source term is 25 mrem/year or less after all FSS is completed, the BcDCGLs are reduced based on an expected, or a priori, fraction of the 25 mrem/year dose limit from each source term. The reduced DCGLs, or Operational DCGLs, can be related to the BcDCGLs as an expected fraction of dose based on an a priori assessment of what the expected dose should be based on the results of site characterization, process knowledge and the extent of planned remediation. The OpDCGL is then used as the DCGL for the FSS design of the survey unit (calculation of surrogate DCGLs, investigations levels, etc.). Details of the OpDCGLs derived for each dose component and the basis for the applied a priori dose fractions are provided in ZionSolutions TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey (Reference 10).
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| [13]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The OpDCGLs for the FSS of surface and subsurface soils are listed in Tables 5-7 and 5-8 of the LTP and are reproduced below in Table 4 and Table 5, respectively.
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| Table 4 - Operational DCGLs for Surface Soils (OpDCGLSS)
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| Surface Soil DCGL Radionuclide (pCi/g)
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| Co-60 1.091 Cs-134 1.733 Cs-137 3.630 Ni-63 914.458 Sr-90 3.095 Table 5 - Operational DCGLs for Subsurface Soils (OpDCGLSB)
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| Subsurface Soil Radionuclide DCGL (pCi/g)
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| Co-60 0.881 Cs-134 1.137 Cs-137 1.984 Ni-63 195.333 Sr-90 0.425 In accordance with NUREG-1757, Appendix G, if the HSA indicates that there is no likelihood of substantial subsurface residual radioactivity, subsurface surveys are not necessary. The HSA, as well as the results of the extensive characterization of subsurface soils in the impacted area surrounding the Zion facility have shown that there is minimal residual radioactivity in subsurface soil. Consequently, the ZSRP performed minimal subsurface sampling during FSS.
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| Instrument DQOs included a verification of the ability of the survey instrument to detect the radiation(s) of interest at the required scan MDC, which for Class 1 open land survey units, is the a priori DCGL Elevated Measurement Comparison (DCGLEMC). Survey instrument response checks were required prior to issuance and after the instrument had been used. Control and accountability of survey instruments was required to ensure the quality and prevent the loss of data.
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| [14]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C As part of the DQOs applied to laboratory processes, analysis results were reported as actual calculated results. The actual recorded value was used as the recorded FSS result for measurement and/or sample values that are less than MDC. Negative values were recorded as zero. For radionuclides less than MDC, the value representing the highest abundance was selected. Results were not reported as less than MDC. Sample report summaries included unique sample identification, analytical method, radionuclide, result, uncertainty, laboratory data qualifiers, units, and the observed MDC.
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| In accordance with the LTP, for laboratory analysis, MDCs less than 10% of the OpDCGL were preferable while MDCs up to 50% of the OpDCGL were acceptable. The maximum acceptable MDC for measurements obtained using field instruments was the a priori DCGLEMC, which was calculated using the methodology described in the LTP, Section 5.6.4.3.
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| : 5. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. Guidance for preparing FSS plans is provided in ZS-LT-300-001-001, Final Status Survey Package Development.
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| The DQO process determined that Co-60, Ni-63, Sr-90, Cs-134 and Cs-137 would be the ROC in survey unit 10221C. During FSS, concentrations for Hard-to-Detect (HTD) ROC Ni-63 and Sr-90 were inferred using a surrogate approach. Cs-137 is the principle surrogate radionuclide for Sr-90 and Co-60 is the principle surrogate radionuclide for Ni-63. The mean, maximum and 95% Upper Confidence Level (UCL) of the surrogate ratios for concrete core samples taken in the Auxiliary Building basement were calculated in TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms, and are presented in Table 6. The maximum ratios will be used in the surrogate calculations during FSS unless area specific ratios are determined by continuing characterization.
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| Table 6 - Surrogate Ratios Auxiliary Building Ratios Mean Max 95%UCL Ni-63/Co-60 44.143 180.450 154.632 Sr-90/Cs-137 0.001 0.002 0.002 For the FSS of survey unit 10221C, the surrogate OpDCGLs for Co-60 and Cs-137 were computed based on the maximum ratios from Table 6.
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| [15]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The equation for calculating a surrogate DCGL is as follows:
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| Equation 1 1
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| =
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| 1 2 3
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| + + +
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| 2 3 Where: DCGLSur = Surrogate radionuclide DCGL DCGL2,3n = DCGL for radionuclides to be represented by the surrogate Rn = Ratio of concentration (or nuclide mixture fraction) of radionuclide n to surrogate radionuclide Using the OpDCGLs for surface soils presented in Table 4 and the maximum ratios from Table 6, the following surrogate calculations for surface soils were performed:
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| Equation 2 1
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| (137) = = 3.622 /
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| 1 0.002 3.630 +
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| (137) 3.095 (90)
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| The surrogate OpDCGL for surface soils that was used for Cs-137 in this survey unit for direct comparison of surface soil sample results to demonstrate compliance is 3.622 pCi/g.
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| Equation 3 1
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| (60) = = 0.898 /
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| 1 180.45 1.091 +
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| (60) 914.458 (63)
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| The surrogate OpDCGL for surface soils that was used for Co-60 in this survey unit for direct comparison of surface soil sample results to demonstrate compliance is 0.898 pCi/g.
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| Using the BcDCGLs presented in Table 2 and the maximum ratios from Table 6, the following surrogate calculations were performed:
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| Equation 4 1
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| (137) = = 14.15 /
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| 1 0.002 14.18 +
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| (137) 12.09 (90)
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| The surrogate BcDCGL for surface soils that was used for Cs-137 in this survey unit for calculating the DCGLEMC is 14.15 pCi/g.
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| [16]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Equation 5 1
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| (60) = = 3.51 /
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| 1 180.45 4.26 +
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| (60) 3572.10(63)
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| The surrogate BcDCGL for surface soils that was used for Co-60 in this survey unit for calculating the DCGLEMC is 3.51 pCi/g.
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| For this Class 1 open land survey unit, the Investigation Levels for area scanning and soil sample measurement results are those levels specified in LTP, Table 5-25, and are reproduced below in Table 7.
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| Table 7 - Investigation Levels Direct Investigation Classification Scan Investigation Levels Levels
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| >Operational DCGL or >MDCscan if Class 1 > Operational DCGL MDCscan is greater than Operational DCGL The MDCscan for the 2350-1/44-10 was calculated using the methodology of ZionSolutions TSD-11-004, Ludlum Model 44-10 Detector Sensitivity (Reference 11) with the following parameters:
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| * background count rate of 5,000 counts per minute (cpm)
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| * scan speed of 0.5 m/sec
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| * distance from detector to surface of 2 inches
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| * isotopic mix of 95% Cs-137 and 5% Co-60 The calculated MDCscan value was 3.75 pCi/g, which was greater than the calculated surrogate DCGLs, therefore the scan investigation level was set at the MDCscan of the 2350-1/44-10. The collimator was used during the scan surveys to lower the background count rate.
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| The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.
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| The number of soil samples for FSS was determined in accordance with ZS-LT-300-001-001.
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| The relative shift (/) for the survey unit data set is defined as shift (), which is the Upper Bound of the Gray Region (UBGR), or the DCGL (SOF of 1.0), minus the Lower Bound of the Gray Region (LBGR) (SOF of 0.5), divided by sigma (), which is the standard deviation of the data set used for survey design. The optimal value for / should range between one and three.
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| The largest value the / can have is three. If the / exceeds three, then the value of three will
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| [17]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C be used for /. For this survey design, a conservative estimate of the sample variability of 0.30 was used as the coefficient of variation to calculate /.
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| The calculated relative shift was 1.67. Both the Type I error, or value, and the Type II error, or value, was set at 0.05. The sample size from Table 5.5 of MARSSIM that equates to the Type I and Type II error of 0.05 for use with the Sign Test is an N value of 17.
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| The computer program Visual Sample Plan (VSP) was used to generate the sample map, in accordance with ZS-LT-300-001-001. The map used was provided by the Survey Mapping/Computer Assisted Design Specialist, with coordinates based on the Illinois State Plane NAD 1983 standard topographical grid coordinate system. The number of samples generated by VSP for a systematic triangular grid was 17. The Prospective Power Curve generated by VSP showed adequate power for the survey design.
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| In accordance with section 5.6.4.3 of the LTP, the a priori DCGLEMC values were calculated for the gamma emitting ROC to ensure that the MDCscan of the selected instrument was sufficient to detect small areas of elevated activity in the survey unit. The calculations were:
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| 1959
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| * To calculate the area bounded by the systematic samples: = = 17
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| = 115.2 2
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| * From the LTP, Table 5-16, the Area Factors for the next larger area (300 m2) were used:
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| o Cs-137 - 1.46 o Cs-134 - 1.30 o Co 1.16
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| * The DCGLEMC is the Surrogate Base Case DCGL times the Area Factor:
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| o The DCGLEMC for Cs-137 = 1.46 14.15 = 20.66 /
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| o The DCGLEMC for Cs-134 = 1.30 6.77 = 8.80 /
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| o The DCGLEMC for Co-60 = 1.16 3.51 = 4.07 /
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| The calculated MDCscan, 3.75 pCi/g, is less than the DCGLEMC values calculated above, therefore, the spacing of the statistical systematic sampling and measurement locations was adequate to detect small areas of elevated radioactivity. No adjustment to the sample number was required.
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| The implementation of quality control (QC) measures as referenced by LTP, Section 5.9 and ZionSolutions procedure ZS-LT-01, Quality Assurance Project Plan (for Characterization and FSS) (QAPP) (Reference 12) includes the collection of a soil sample for split sample analysis on 5% of the soil samples taken in a survey unit with the locations selected at random.
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| One (1) surface soil sample (L1-10221C-FQGS-012-SS) was selected randomly for split sample analysis for the FSS of this survey unit.
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| In accordance with section 5.7.1.6.2 of the LTP, a subsurface soil sample was taken at 10%
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| of the systematic surface soil sample locations in the survey unit with the location(s) selected at random. Locations L1-10221C-FSGS-005-SB and L1-10221C-FSGS-013-SB were
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| [18]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C selected for this survey unit.
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| The locations of the seventeen (17) systematic samples are listed in Table 8. Also included are the locations of the two (2) subsurface samples. A map of the systematic sample locations is included in Attachment 1.
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| Table 8 - Systematic Sample Measurement Locations NORTHING EASTING MEASUREMENT ID (meters) (meters)
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| L1-10221C-FSGS-001-SS 641486.29 343565.68 L1-10221C-FSGS-002-SS 641486.29 343577.21 L1-10221B-FSGS-003-SS 641496.28 343559.91 L1-10221B-FSGS-004-SS 641496.28 343571.45 L1-10221B-FSGS-005-SS 641496.28 343582.98 L1-10221B-FSGS-006-SS 641506.27 343565.68 L1-10221B-FSGS-007-SS 641506.27 343577.21 L1-10221B-FSGS-008-SS 641506.27 343588.75 L1-10221B-FSGS-009-SS 641516.26 343571.45 L1-10221B-FSGS-010-SS 641516.26 343582.98 L1-10221B-FSGS-011-SS 641526.25 343565.68 L1-10221B-FSGS-012-SS 641526.25 343577.21 L1-10221B-FSGS-013-SS 641526.25 343588.75 L1-10221B-FSGS-014-SS 641536.24 343571.45 L1-10221B-FSGS-015-SS 641536.24 343582.98 L1-10221B-FSGS-016-SS 641536.24 343594.52 L1-10221B-FSGS-017-SS 641546.23 343577.21 L1-10221B-FSGS-005-SB 641496.28 343582.98 L1-10221B-FSGS-013-SB 641526.25 343588.75 ZSRP LTP, Section 5.1 states that soil samples will be collected during FSS to confirm the HTD to surrogate radionuclide ratios (provided in Table 6). Ten percent (10%) of the FSS samples collected from open land survey units will be analyzed for HTD ROC. Only HTD radionuclides included as ROC (Ni-63 and Sr-90 for soils) will be analyzed in the FSS confirmatory samples. For soil samples with positive results for both a HTD ROC and the corresponding surrogate radionuclide (Cs-137 or Co-60), the HTD surrogate ratio will be derived and compared against the maximum ratio. The maximum ratios will be used unless specific survey information supports the use of a surrogate ratio that is specific to the area. In these cases, the survey unit-specific radiological data and the derived surrogate ratios will be submitted to the NRC for approval. If approved, then the survey unit-specific ratios used and the survey data serving as the basis for the surrogate ratios will be documented in the release record for the survey unit.
| |
| [19]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C In addition, LTP Chapter 5, Section 5.1 states that if levels of residual gamma radioactivity in an individual soil sample exceed an OpSOF of 0.1, then the sample(s) will be analyzed for HTD ROC. Six (6) samples: L1-10221C-FSGS-012-SS, L1-10221C-FSGS-013-SS, L1-10221C-FSGS-014-SS, L1-10221C-FSGS-013-SB, L1-10221C-FIGS-101-SS and L1-10221C-FIGS-103-SS exceeded an OpSOF of 0.1 during the FSS of survey unit 10221C.
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| These samples satisfy the requirement that 10% of the samples collected for the FSS of survey unit 10221C be analyzed for HTD ROC. Each selected sample was sent off-site (Eberline Analytical) for analysis of the HTD ROC as specified in LTP, Section 5.1. Eberline analytical reports are provided in Attachment 8.
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| Table 9 provides a synopsis of the survey design for survey unit 10221C.
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| [20]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 9 - Synopsis of Survey Design FEATURE DESIGN CRITERIA BASIS Survey Unit Area 1,959 m2 GPS measurements of area
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| * = 0.30
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| * UBGR = SOF of 1
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| * LBGR = SOF of 0.5 Number of Surface 17 (Systematic)
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| * Type I error = 0.05 Soil Samples
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| * Type II error = 0.05
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| * / = 1.67 (MARSSIM Table 5.5)
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| Grid Spacing 11.5 m (LTP, Section 5.6.4.5.2)
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| * Co 1.091 pCi/g
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| * Cs-134 - 1.733 pCi/g Operational DCGLs for Surface DCGLs
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| * Cs-137 - 3.630 pCi/g Soils, (LTP, Table 5-7)
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| * Ni 914.458 pCi/g
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| * Sr 3.095 pCi/g A minimum of two (2) soil samples HTD ROC Analysis (LTP, Section 5.1) selected for HTD ROC analysis Measurement Operational DCGL (LTP, Table 5-25)
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| Investigation Level Scan Survey Area 100% (LTP, Table 5-24)
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| Coverage One (1) surface soil sample selected QC (LTP, Section 5.9) randomly for split sample analysis Number of Two (2) - systematic surface soil sample Subsurface Soil (LTP, Section 5.7.1.6.2) locations 5 and 13 Samples
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| [21]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
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| : 6. SURVEY IMPLEMENTATION Survey instructions for this FSS were incorporated into and performed in accordance with FSS sample plan L1-10221C-F, which was developed in accordance with ZS-LT-300-001-001. The FSS unit was inspected and controlled in accordance with ZionSolutions procedure ZS-LT-300-001-003, Isolation and Control for Final Status Survey (Reference 13).
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| For survey unit 10221C, compliance with the unrestricted release criteria was demonstrated through a combination of surface scanning with a Ludlum Model 44-10 gamma detector and the sampling of surface soil for isotopic analysis. In accordance with the LTP Chapter 5, two (2) subsurface samples were obtained and analyzed. Also, if during the performance of FSS, the analysis of a surface soil sample, or the results of a surface gamma scan indicated the potential presence of residual radioactivity at a concentration of 75% of the subsurface Operational DCGL, then a biased subsurface soil sample(s) would be taken to the appropriate depth within the area of concern as part of the investigation. This threshold was encountered during a RA survey on June 17, 2019. While performing a gamma scan of the railroad ballast located in survey unit 10221C, and the soil areas 1 meter beyond the ballast gravel, two (2) small areas of elevated activity were identified. A small radioactive particle was identified in one of the areas and was captured. Surface and subsurface investigation soil samples were taken at these locations (L1-10221C-FIGS-100-SS thru L1-10221C-FIGS-113-SS, L1-10221C-FIGS-100-SB and L1-10221C-FIGS-101-SB).
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| FSS field activities were conducted under FSS sample plan L1-10221C-F. A Field Log (ZS-LT-300-001-001, Attachment 14) was used to document field activities and other information pertaining to the performance of the FSS. FSS field activities were projected to take four (4) working days to complete. Daily briefings were conducted to discuss the expectations for job performance and to review safety aspects of the job. The survey required field activities were performed during normal working hours starting on June 11, 2019, and concluding September 17, 2019.
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| The seventeen (17) systematic surface soil sample locations were marked with flags based on GPS coordinates provided by VSP. Three (3) samples were relocated because they fell on the railroad ballast, which consists of gravel and not soil. The relocated sample points are listed in Table 22 and are shown on the systematic sample map in Attachment 1 and the posting plot in Attachment 6.
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| Under the FSS sample plan, gamma scans were performed on 100% of the surface area of the survey unit using a Ludlum 2350-1 paired with a Model 44-10 (2 x 2) NaI detector operated in the rate-meter mode and using audio response. The probe was positioned within 2-inches to the ground and was moved at a scan speed of approximately 0.5 meters per second. No areas of elevated activity were detected during the scans under the FSS Sample Plan. However, scans were performed at an earlier date under an RA on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas 1 meter beyond the ballast gravel. The RA survey
| |
| [22]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C identified two (2) small areas of elevated activity (see Section 9 for further discussion). Each detector was subjected to an Operation Response Check daily, prior to and following use, in accordance with ZionSolutions procedure ZS-RP-108-004-011, Operation of the Ludlum Model 2350-1 Data Logger (Reference 14). The daily Operational Response Check compared the background response and the response to check sources ranges, established for normal background and detector source response, to ensure that the detector was working properly.
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| The instruments and detectors used for this survey are presented in Table 10. The instruments and detectors were verified to be properly calibrated prior to use.
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| Table 10 - Instruments and Detectors Instrument/Detector Type Serial # Calibration Due Date Ludlum 2350-1/Ludlum 44-10 293136/PR316938 06/18/20 Ludlum 2350-1/Ludlum 44-10 304712/PR372143 09/9/20 Ludlum 2350-1/Ludlum 44-10 266657/PR308037 05/13/20 Ludlum 2350-1/Ludlum 44-10 304718/PR363311 12/13/19 Ludlum 2350-1/Ludlum 44-10 304730/PR375273 01/16/20 Ludlum 2350-1/Ludlum 44-10 304711/PR321902 01/18/20 Ludlum 2350-1/Ludlum 44-10 304726/PR363452 09/06/19 In accordance with the survey design, seventeen (17) surface soil samples were collected at the designated systematic sample points along with two (2) subsurface samples taken at randomly selected locations. In addition, fourteen (14) surface samples and two (2) subsurface samples were collected as part of the investigation of two (2) areas of elevated activity identified during surface scans performed under an RA; and eight (8) judgmental surface samples were taken adjacent to the railroad ballast on both sides.
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| Six (6) samples (L1-10221C-FSGS-012-SS, L1-10221C-FSGS-013-SS, L1-10221C-FSGS-014-SS, L1-10221C-FSGS-013-SB, L1-10221C-FIGS-101-SS and L1-10221C-FIGS-103-SS) were selected for HTD radionuclide analysis. One (1) surface soil sample (L1-10221C-FQGS-012-SS) was selected randomly for QC sample analysis.
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| : 7. SURVEY RESULTS One hundred percent (100%) of the surface of the survey unit was scanned for elevated radiation levels. Sixty-eight (68) 1-meter wide scan rows, as shown on the map in Attachment 1, were marked in the field and scanned with the 2350-1/44-10 using latching mode. Readings were recorded at approximately 10-meter intervals during the scans. No elevated measurements locations were identified by surface scan under the FSS Sample Plan. However, scans were performed at an earlier date under an RA on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas 1 meter beyond the ballast gravel. The RA survey
| |
| [23]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C identified two (2) small areas of elevated activity (see Section 9 for further discussion). Table 11 provides an overview of the scan results. Complete scan results are provided in Attachment 2.
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| Table 11 - Synopsis of Scan Results Highest Logged Scan Action Level(1) # of Scan Reading Investigation Samples Area Alarms (cpm) (cpm)
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| Row 1 2090 2285 None None Row 2 2178 2285 None None Row 3 2198 2285 None None Row 4 1996 2285 None None Row 5 1815 2285 None None Row 6 1767 2285 None None Row 7 1840 2285 None None Row 8 1939 2285 None None Row 9 1875 2244 None None Row 10 1806 2244 None None Row 11 1943 2244 None None Row 12 2049 2244 None None Row 13 1946 2244 None None Row 14 1984 2244 None None Row 15 1972 2244 None None Row 16 1923 2244 None None Row 17 2070 2456 None None Row 18 2345 2456 None None Row 19 2292 2456 None None Row 20 2197 2456 None None Row 21 2408 2456 None None Row 22 2246 2456 None None Row 23 2340 2456 None None Row 24 2258 2456 None None Row 25 2359 2771 None None Row 26 2472 2771 None None Row 27 2349 2771 None None Row 28 2261 2771 None None Row 29 2227 2771 None None Row 30 2426 2771 None None Row 31 2554 2771 None None Row 32 2520 2771 None None Row 33 2574 3120 None None
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| [24]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 11 (continued) - Synopsis of Scan Results Scan Highest Logged Action Level(1) # of Scan Reading Investigation Samples Area Alarms (cpm) (cpm)
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| Row 34 2765 3120 None None Row 35 2813 3120 None None Row 36 2718 3120 None None Row 37 3011 3120 None None Row 38 3109 3120 None None Row 39 2928 3120 None None Row 40 3057 3120 None None Row 41 3103 3566 None None Row 42 3275 3566 None None Row 43 3067 3566 None None Row 44 3252 3566 None None Row 45 3063 3566 None None Row 46 3063 3566 None None Row 47 3109 3566 None None Row 48 3188 3566 None None Row 49 3359 3576 None None Row 50 3076 3576 None None Row 51 3544 3576 None None Row 52 3316 3576 None None Row 53 3337 3576 None None Row 54 3054 3576 None None Row 55 3202 3576 None None Row 56 3198 3576 None None Row 57 3059 3327 None None Row 58 3276 3327 None None Row 59 3128 3327 None None Row 60 3000 3327 None None Row 61 3024 3463 None None Row 62 3053 3463 None None Row 63 3188 3463 None None Row 64 2971 3463 None None Row 65 2799 3463 None None Row 66 2729 3463 None None Row 67 2929 3463 None None Row 68 2712 3463 None None
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| : 1) The action level is based on the measurement Minimum Detectable Count Rate (MDCR) plus background in accordance with the FSS plan
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| [25]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The seventeen (17) systematic surface soil samples taken for non-parametric statistical testing, the twenty-two (22) biased surface soil samples (investigation and judgmental) and the four (4) subsurface soil samples were analyzed using the on-site gamma spectroscopy system.
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| Summaries of the sample analysis results are provided in Tables 12, 13 and 14, respectively. The basic statistics for the systematic sample population are summarized in Table 21. For the systematic samples, the gamma spectroscopy results revealed seven (7) samples with activity levels above MDC for Cs-137, two (2) samples with activity levels above MDC for Co-60 and no samples with activity levels above MDC for Cs-134. The concentrations for Ni-63 and Sr-90 were inferred based on the maximum ratios as specified in Table 6. The mean of the gamma spectroscopic analysis results for the sample population indicated that Cs-137 was present at levels lower than the concentrations of Cs-137 expected to be found in off-site soil in the vicinity of the ZNPS as presented in ZionSolutions TSD 13-004, Examination of Cs-137 Global Fallout In Soils At Zion Station (Reference 15). The complete gamma spectroscopy reports are presented in Attachment 7.
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| Table 12 - Summary of Gamma Spectroscopy Results for Surface Soil Samples Comprising the Statistical Sample Population Co-60(1) Cs-134(1) Cs-137(1) Ni-63(2) Sr-90(2)
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| MEASUREMENT ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L1-10221C-FSGS-001-SS 1.95E-02 1.05E-02 1.71E-02 3.52E+00 3.42E-05 L1-10221C-FSGS-002-SS 2.85E-02 1.31E-02 2.68E-02 5.14E+00 5.36E-05 L1-10221C-FSGS-003-SS 9.10E-03 0.00E+00 3.65E-02 1.64E+00 7.30E-05 L1-10221C-FSGS-004-SS 6.14E-03 5.33E-03 0.00E+00 1.11E+00 0.00E+00 L1-10221C-FSGS-005-SS 4.16E-02 4.82E-03 7.47E-02 7.51E+00 1.49E-04 L1-10221C-FSGS-006-SS 2.46E-02 1.30E-03 5.20E-02 4.44E+00 1.04E-04 L1-10221C-FSGS-007-SS 3.26E-02 0.00E+00 9.37E-02 5.88E+00 1.87E-04 L1-10221C-FSGS-008-SS 1.02E-02 1.12E-02 0.00E+00 1.84E+00 0.00E+00 L1-10221C-FSGS-009-SS 2.92E-02 1.66E-02 1.61E-02 5.27E+00 3.22E-05 L1-10221C-FSGS-010-SS 0.00E+00 0.00E+00 1.43E-02 0.00E+00 2.86E-05 L1-10221C-FSGS-011-SS 5.21E-02 3.65E-02 4.53E-03 9.40E+00 9.06E-06 L1-10221C-FSGS-012-SS 2.59E-02 5.26E-02 3.18E-01 4.67E+00 6.36E-04 L1-10221C-FSGS-013-SS 9.66E-02 2.34E-02 1.41E-01 1.74E+01 2.82E-04 L1-10221C-FSGS-014-SS 1.05E-01 4.43E-02 4.32E-01 1.89E+01 8.64E-04 L1-10221C-FSGS-015-SS 2.33E-02 2.28E-02 4.24E-02 4.20E+00 8.48E-05 L1-10221C-FSGS-016-SS 2.67E-02 3.22E-02 5.17E-02 4.82E+00 1.03E-04 L1-10221C-FSGS-017-SS 1.06E-02 1.20E-02 9.70E-04 1.91E+00 1.94E-06 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
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| (2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
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| [26]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 13 - Summary of Gamma Spectroscopy Results for Investigation/Judgmental Surface Soil Samples Co-60 (1) Cs-134(1) Cs-137(1) Ni-63(2) Sr-90(2)
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| MEASUREMENT ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L1-10221C-FIGS-100-SS 4.22E-03 5.24E-03 1.97E-02 7.61E-01 3.94E-05 L1-10221C-FIGS-101-SS 1.09E-01 3.79E-02 5.69E-01 1.97E+01 1.14E-03 L1-10221C-FIGS-102-SS 2.60E-02 1.53E-02 9.16E-02 4.69E+00 1.83E-04 L1-10221C-FIGS-103-SS 5.84E-02 5.71E-03 1.58E-01 1.05E+01 3.16E-04 L1-10221C-FIGS-104-SS 2.70E-02 6.48E-03 7.55E-03 4.87E+00 1.51E-05 L1-10221C-FIGS-105-SS 4.93E-02 0.00E+00 2.82E-02 8.90E+00 5.64E-05 L1-10221C-FIGS-106-SS 2.97E-02 0.00E+00 4.60E-02 5.36E+00 9.20E-05 L1-10221C-FIGS-107-SS 8.24E-03 5.03E-02 1.39E-02 1.49E+00 2.78E-05 L1-10221C-FIGS-108-SS 2.41E-02 6.42E-04 1.17E-02 4.35E+00 2.34E-05 L1-10221C-FIGS-109-SS 8.17E-03 0.00E+00 5.13E-02 1.47E+00 1.03E-04 L1-10221C-FIGS-110-SS 1.75E-02 3.92E-03 2.51E-02 3.16E+00 5.02E-05 L1-10221C-FIGS-111-SS 0.00E+00 0.00E+00 3.55E-02 0.00E+00 7.10E-05 L1-10221C-FIGS-112-SS 1.37E-02 4.34E-03 8.17E-03 2.47E+00 1.63E-05 L1-10221C-FIGS-113-SS 2.82E-02 0.00E+00 0.00E+00 5.09E+00 0.00E+00 L1-10221C-FJGS-001-SS 8.17E-04 1.74E-02 1.28E-02 1.47E-01 2.56E-05 L1-10221C-FJGS-002-SS 4.26E-02 0.00E+00 7.32E-02 7.69E+00 1.46E-04 L1-10221C-FJGS-003-SS 1.50E-02 0.00E+00 0.00E+00 2.71E+00 0.00E+00 L1-10221C-FJGS-004-SS 1.97E-02 1.13E-02 5.00E-02 3.55E+00 1.00E-04 L1-10221C-FJGS-005-SS 4.25E-03 3.06E-02 0.00E+00 7.67E-01 0.00E+00 L1-10221C-FJGS-006-SS 0.00E+00 0.00E+00 4.68E-02 0.00E+00 9.36E-05 L1-10221C-FJGS-007-SS 3.55E-02 1.03E-02 3.26E-02 6.41E+00 6.52E-05 L1-10221C-FJGS-008-SS 3.28E-02 1.36E-03 1.34E-02 5.92E+00 2.68E-05 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
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| (2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
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| Table 14 - Summary of Gamma Spectroscopy Results for Subsurface Soil Samples Co-60(1) Cs-134(1) Cs-137(1) Ni-63(2) Sr-90(2)
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| MEASUREMENT ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L1-10221C-FSGS-005-SB 1.25E-02 3.85E-03 4.63E-03 2.26E+00 9.26E-06 L1-10221C-FSGS-013-SB 6.59E-02 3.57E-03 1.49E-01 1.19E+01 2.98E-04 L1-10221C-FIGS-100-SB 0.00E+00 1.00E-02 3.56E-02 0.00E+00 7.12E-05 L1-10221C-FIGS-101-SB 0.00E+00 4.49E-02 2.18E-02 0.00E+00 4.36E-05 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
| |
| (2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
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| [27]
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| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C The off-site laboratory, Eberline Analytical, processed the six (6) samples selected for HTD ROC analysis. Samples L1-10221C-FSGS-012-SS, L1-10221C-FSGS-013-SS, L1-10221C-FSGS-014-SS, L1-10221C-FSGS-013-SB, L1-10221C-FIGS-101-SS and L1-10221C-FIGS-103-SS were selected. Only HTD radionuclides included as ROC (Ni-63 and Sr-90 for soils) were included in the analysis. All analyses met the required MDC. Co-60 and Ni-63 were positively detected in only one (1) of the samples at a concentration greater than MDC. The HTD to surrogate ratio for this sample was 6.10 (see sample L1-10221A-FSGS-014SS-A) which is well below the maximum Ni-63/Co-60 ratio of 180.450 listed in Table 6. The off-site analysis results are provided in Table 15.
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| Table 15 - Off-Site Analysis Results Sample # L1-10221C-FSGS-012-SS-A Result Uncertainty MDC ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| Co-60 -1.16E-02 1.07E-01 1.34E-01 No Cs-134 -2.28E-01 1.38E-01 1.27E-01 No Cs-137 1.78E-01 1.04E-01 1.62E-01 Yes Ni-63 -9.66E-01 2.02E+00 3.54E+00 No Sr-90 1.12E-01 3.71E-01 7.80E-01 No Sample # L1-10221C -FSGS-013-SS-A Result Uncertainty MDC ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| Co-60 1.80E-02 9.42E-02 1.55E-01 No Cs-134 9.24E-03 2.70E-02 1.17E-01 No Cs-137 1.76E-01 9.04E-02 1.39E-01 Yes Ni-63 -1.38E+00 2.05E+00 3.61E+00 No Sr-90 2.71E-01 2.71E-01 5.48E-01 No Sample # L1-10221C -FSGS-014-SS-A Result Uncertainty MDC ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| Co-60 5.93E-01 9.00E-02 1.17E-01 Yes Cs-134 7.28E-03 2.90E-02 5.86E-02 No Cs-137 2.29E+00 2.83E-01 1.47E-01 Yes Ni-63 3.62E+00 2.18E+00 3.58E+00 Yes Sr-90 7.79E-02 3.72E-01 7.86E-01 No
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| [28]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 15 (Continued) - Off-Site Analysis Results Sample # L1-10221C-FSGS-013-SB-A Result Uncertainty MDC ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| Co-60 5.71E-02 5.36E-02 7.05E-02 No Cs-134 1.11E-02 2.59E-02 5.16E-02 No Cs-137 8.93E-02 5.74E-02 9.00E-02 No Ni-63 -6.98E-01 1.83E+00 3.19E+00 No (1)
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| Sr-90 4.90E-02 3.43E-02 6.77E-02 No Sample # L1-10221C-FIGS-101-SS-A Result Uncertainty MDC ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| Co-60 2.45E-01 5.59E-02 6.76E-02 Yes Cs-134 1.30E-02 2.24E-02 5.57E-02 No Cs-137 1.06E+00 1.48E-01 1.07E-01 Yes Ni-63 6.32E-01 2.03E+00 3.46E+00 No Sr-90 3.55E-01 3.07E-01 7.39E-01 No Sample # L1-10221C-FIGS-103-SS-A Result Uncertainty MDC ROC >MDC (pCi/g) (pCi/g) (pCi/g)
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| Co-60 9.13E-02 6.23E-02 1.12E-01 No Cs-134 1.66E-02 2.41E-02 1.04E-01 No Cs-137 1.73E-01 8.28E-02 1.26E-01 Yes Ni-63 2.41E+00 1.96E+00 3.26E+00 No Sr-90 3.73E-01 3.20E-01 6.40E-01 No (1) Sr-90 recounted February 19, 2020, to achieve adequate MDC The implementation of survey specific QC measures included the collection of one (1) systematic sample (L1-10221C-FQGS-012-SS) and two (2) biased samples (L1-10221C-QJGS-001-SS and L1-10221C-QIGS-110-SS) for split sample analysis. The on-site laboratory analyzed the QC samples using the on-site gamma spectroscopy system. Gamma spectroscopy results are summarized in Table 16. The concentrations for Ni-63 and Sr-90 were inferred based on the maximum ratios as specified in Table 6.
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| [29]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 16 - Summary of Gamma Spectroscopy Results for QC Soil Samples Co-60(1) Cs-134(1) Cs-137(1) Ni-63(2) Sr-90(2)
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| MEASUREMENT ID (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g)
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| L1-10221C-FQGS-012-SS 1.35E-04 6.96E-02 1.52E-01 2.44E-02 3.04E-04 L1-10221C-QJGS-001-SS 1.80E-02 0.00E+00 1.26E-02 3.25E+00 2.52E-05 L1-10221C-QIGS-110-SS 2.05E-02 3.01E-02 5.65E-02 3.70E+00 1.13E-04 Note: (1) Bold font indicates ROC positively detected at concentration greater than MDC.
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| (2) Ni-63 and Sr-90 are inferred concentrations using the maximum HTD ratio.
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| The SOF or unity rule is the mathematical test used to evaluate compliance with radiological criteria for license termination when more than one radionuclide has been determined to be potentially present. The equation for the unity rule is:
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| Equation 6 C1 C2 Cn
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| + +............ 1 DCGL1 DCGL 2 DCGL n Where: Cn = concentration of radionuclide n DCGLn = DCGL of radionuclide n.
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| The results of the unity rule calculations for the ROC in the systematic sample population when compared against the OpDCGLs for surface soils for survey unit 10221C are presented in Table 17. The results of the unity rule calculations for the ROC for the biased surface samples are presented in Table 18, the results for the subsurface samples are presented in Table 19, and the results for the QC samples are presented in Table 20.
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| Table 17 - Sum of Fractions for Systematic Surface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID OpSOF Co-60 Cs-134 Cs-137 Ni-63 Sr-90 L1-10221C-FSGS-001-SS 1.79E-02 6.06E-03 4.71E-03 3.85E-03 1.11E-05 0.033 L1-10221C-FSGS-002-SS 2.61E-02 7.56E-03 7.38E-03 5.62E-03 1.73E-05 0.047 L1-10221C-FSGS-003-SS 8.34E-03 0.00E+00 1.01E-02 1.80E-03 2.36E-05 0.020 L1-10221C-FSGS-004-SS 5.63E-03 3.08E-03 0.00E+00 1.21E-03 0.00E+00 0.010 L1-10221C-FSGS-005-SS 3.81E-02 2.78E-03 2.06E-02 8.21E-03 4.83E-05 0.070 L1-10221C-FSGS-006-SS 2.25E-02 7.50E-04 1.43E-02 4.85E-03 3.36E-05 0.043 L1-10221C-FSGS-007-SS 2.99E-02 0.00E+00 2.58E-02 6.43E-03 6.05E-05 0.062 L1-10221C-FSGS-008-SS 9.35E-03 6.46E-03 0.00E+00 2.01E-03 0.00E+00 0.018 L1-10221C-FSGS-009-SS 2.68E-02 9.58E-03 4.44E-03 5.76E-03 1.04E-05 0.047 L1-10221C-FSGS-010-SS 0.00E+00 0.00E+00 3.94E-03 0.00E+00 9.24E-06 0.004 L1-10221C-FSGS-011-SS 4.78E-02 2.11E-02 1.25E-03 1.03E-02 2.93E-06 0.080
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| [30]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 17 (continued) - Sum of Fractions for Systematic Surface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID OpSOF Co-60 Cs-134 Cs-137 Ni-63 Sr-90 L1-10221C-FSGS-012-SS 2.37E-02 3.04E-02 8.76E-02 5.11E-03 2.05E-04 0.147 L1-10221C-FSGS-013-SS 8.85E-02 1.35E-02 3.88E-02 1.91E-02 9.11E-05 0.160 L1-10221C-FSGS-014-SS 9.62E-02 2.56E-02 1.19E-01 2.07E-02 2.79E-04 0.262 L1-10221C-FSGS-015-SS 2.14E-02 1.32E-02 1.17E-02 4.60E-03 2.74E-05 0.051 L1-10221C-FSGS-016-SS 2.45E-02 1.86E-02 1.42E-02 5.27E-03 3.34E-05 0.063 L1-10221C-FSGS-017-SS 9.72E-03 6.92E-03 2.67E-04 2.09E-03 6.27E-07 0.019 Systematic Measurements Number of Systematic Measurements = 17
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| # of Systematic Measurements with OpSOF > 1 = 0
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| # of Systematic Measurements with OpSOF > 0.1 (HTD Assessment) = 3 Max Individual Systematic Measurement OpSOF = 0.262 Mean Systematic Measurement OpSOF = 0.067 Table 18 - Sum of Fractions for Investigation/Judgmental Surface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID OpSOF Co-60 Cs-134 Cs-137 Ni-63 Sr-90 L1-10221C-FIGS-100-SS 3.87E-03 3.02E-03 5.43E-03 8.33E-04 1.27E-05 0.013 L1-10221C-FIGS-101-SS 9.99E-02 2.19E-02 1.57E-01 2.15E-02 3.68E-04 0.300 L1-10221C-FIGS-102-SS 2.38E-02 8.83E-03 2.52E-02 5.13E-03 5.92E-05 0.063 L1-10221C-FIGS-103-SS 5.35E-02 3.29E-03 4.35E-02 1.15E-02 1.02E-04 0.112 L1-10221C-FIGS-104-SS 2.47E-02 3.74E-03 2.08E-03 5.33E-03 4.88E-06 0.036 L1-10221C-FIGS-105-SS 4.52E-02 0.00E+00 7.77E-03 9.73E-03 1.82E-05 0.063 L1-10221C-FIGS-106-SS 2.72E-02 0.00E+00 1.27E-02 5.86E-03 2.97E-05 0.046 L1-10221C-FIGS-107-SS 7.55E-03 2.90E-02 3.83E-03 1.63E-03 8.98E-06 0.042 L1-10221C-FIGS-108-SS 2.21E-02 3.70E-04 3.22E-03 4.76E-03 7.56E-06 0.030 L1-10221C-FIGS-109-SS 7.49E-03 0.00E+00 1.41E-02 1.61E-03 3.32E-05 0.023 L1-10221C-FIGS-110-SS 1.60E-02 2.26E-03 6.91E-03 3.45E-03 1.62E-05 0.029 L1-10221C-FIGS-111-SS 0.00E+00 0.00E+00 9.78E-03 0.00E+00 2.29E-05 0.010 L1-10221C-FIGS-112-SS 1.26E-02 2.50E-03 2.25E-03 2.70E-03 5.28E-06 0.020 L1-10221C-FIGS-113-SS 2.58E-02 0.00E+00 0.00E+00 5.56E-03 0.00E+00 0.031 L1-10221C-FJGS-001-SS 7.49E-04 1.00E-02 3.53E-03 1.61E-04 8.27E-06 0.014 L1-10221C-FJGS-002-SS 3.90E-02 0.00E+00 2.02E-02 8.41E-03 4.73E-05 0.068 L1-10221C-FJGS-003-SS 1.37E-02 0.00E+00 0.00E+00 2.96E-03 0.00E+00 0.017 L1-10221C-FJGS-004-SS 1.81E-02 6.52E-03 1.38E-02 3.89E-03 3.23E-05 0.042 L1-10221C-FJGS-005-SS 3.90E-03 1.77E-02 0.00E+00 8.39E-04 0.00E+00 0.022 L1-10221C-FJGS-006-SS 0.00E+00 0.00E+00 1.29E-02 0.00E+00 3.02E-05 0.013
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| [31]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID OpSOF Co-60 Cs-134 Cs-137 Ni-63 Sr-90 L1-10221C-FJGS-007-SS 3.25E-02 5.94E-03 8.98E-03 7.01E-03 2.11E-05 0.054 L1-10221C-FJGS-008-SS 3.01E-02 7.85E-04 3.69E-03 6.47E-03 8.66E-06 0.041 Table 19 - Sum of Fractions for Subsurface Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Subsurface Soils MEASUREMENT ID OpSOF Co-60 Cs-134 Cs-137 Ni-63 Sr-90 L1-10221C-FSGS-005-SB 1.42E-02 3.39E-03 2.33E-03 1.15E-02 2.18E-05 0.031 L1-10221C-FSGS-013-SB 7.48E-02 3.14E-03 7.51E-02 6.09E-02 7.01E-04 0.215 L1-10221C-FIGS-100-SB 0.00E+00 8.80E-03 1.79E-02 0.00E+00 1.68E-04 0.027 L1-10221C-FIGS-101-SB 0.00E+00 3.95E-02 1.10E-02 0.00E+00 1.03E-04 0.051 Table 20 - Sum of Fractions for QC Soil Samples compared to the OpDCGLs Fraction of the OpDCGLs for Surface Soils MEASUREMENT ID OpSOF Co-60 Cs-134 Cs-137 Ni-63 Sr-90 L1-10221C-FQGS-012-SS 1.24E-04 4.02E-02 4.19E-02 2.66E-05 9.82E-05 0.082 L1-10221C-QJGS-001-SS 1.65E-02 0.00E+00 3.47E-03 3.55E-03 8.14E-06 0.024 L1-10221C-QIGS-110-SS 1.88E-02 1.74E-02 1.56E-02 4.05E-03 3.65E-05 0.056 Table 21 - Basic Statistical Properties of Systematic Sample Population Mean Median Max Min Std. Dev. BcDCGL Avg. SOF Avg. Dose ROC (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) (pCi/g) per ROC Per ROC Co-60 3.19E-02 2.59E-02 1.05E-01 0.00E+00 0.029 4.26 7.48E-03 1.87E-01 Cs-134 1.69E-02 1.20E-02 5.26E-02 0.00E+00 0.016 6.77 2.49E-03 6.23E-02 Cs-137 7.78E-02 3.65E-02 4.32E-01 0.00E+00 0.120 14.18 5.48E-03 1.37E-01 Ni-63 5.75E+00 4.67E+00 1.89E+01 0.00E+00 5.246 3572.1 1.61E-03 4.02E-02 Sr-90 1.56E-04 7.30E-05 8.64E-04 0.00E+00 0.000 12.09 1.29E-05 3.22E-04 The mean BcSOF for survey unit 10221C is 0.017, which equates to a dose of 0.427 mrem/year TEDE.
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| The mean of all identified isotopes is less than the Consultation Triggers for Residential and Commercial/Industrial Soil Contamination depicted in Table H.1 of NUREG 1757, Vol. 1, (MOU Table 1). The full table is included in Attachment 3 of this Release Record.
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| : 8. QUALITY CONTROL The on-site laboratory processed three (3) split samples, L1-10221C-FQGS-012-SS, L1-10221C-QJGS-001-SS and L1-10221C-QIGS-110-SS, using gamma spectroscopy analysis. The data was evaluated using acceptance criteria specified in ZS-LT-01.
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| For L1-10221C-FQGS-012-SS, there was not acceptable agreement between field split results when using Cs-137 due to the fact that it is present in the samples at relatively low concentrations.
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| [32]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C However, when using K-40, which is present in the samples at higher concentrations, there was acceptable agreement. No further action was deemed necessary For the remaining samples, there was acceptable agreement between the field split results. Refer to Attachment 5 for data and QC analysis results.
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| : 9. INVESTIGATIONS AND RESULTS An investigation was performed based on the results of gamma scans performed under an RA on June 17, 2019 on the railroad ballast located in survey unit 10221C and the soil areas 1- meter beyond the ballast gravel. The RA identified two (2) small areas of elevated activity (a map of these areas is included in Attachment 1). One area was less than 100 cm2 with a reading of 4,000 cpm. One (1) surface soil sample was taken at this location: L1-10221C-FIGS-101-SS. Four (4) additional samples were taken in the immediate vicinity (within 0.5 meters): L1-10221C-FIGS-102-SS through L1-10221C-FIGS-105-SS. The second location was a 1-meter by 2-meter area with a maximum reading of 7,000 cpm. A small radioactive particle was captured in this area and one (1) surface soil sample was taken at the location: L1-10221C-FIGS-100-SS. Eight (8) additional samples were taken in the immediate vicinity (within 1.0 meter): L1-10221C-FIGS-106-SS through L1-10221C-FIGS-113-SS. Gamma spectroscopy results revealed five (5) samples with activity levels above MDC for Cs-137 and no samples with activity levels above MDC for Co-60 and Cs-134. Since the OpSOF for the investigation samples were all less than 1.0, with a maximum OpSOF of 0.300, no further action was necessary. The investigation is documented in an Attachment 13 (from ZS- LT-300-001-004), Final Status Survey Investigation. The gamma spectroscopy results are summarized in Table 13, and the OpSOFs summarized in Table 18.
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| Also included in Table 13 and Table 18 are the results of the eight (8) judgmental surface soil samples that were taken adjacent to the railroad ballast. Maps of the judgmental sample locations are included in Attachment 1.
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| : 10. REMEDIATION AND RESULTS The small radioactive particle identified in the previous investigation was captured. No other remediation was performed in this survey unit.
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| : 11. CHANGES FROM THE SURVEY PLAN Three (3) systematic samples were relocated to the closest adjacent suitable location due to the original locations falling on the railroad ballast which is made up of gravel and not soil. The coordinates of the relocated samples are listed in the table below. The map included in Attachment 1 shows the original and relocated sample points.
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| [33]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Table 22 Relocated Systematic Sample Locations NORTHING EASTING MEASUREMENT ID (meters) (meters)
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| L1-10221C-FSGS-002-SS 641482.36 343575.98 L1-10221C-FSGS-003-SS 641491.28 343558.46 L1-10221C-FSGS-004-SS 641499.50 343573.75
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| : 12. DATA QUALITY ASSESSMENT The DQO sample design and data were reviewed in accordance with ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment (Reference 16) for completeness and consistency. Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs. The sampling design had adequate power as indicated by the Retrospective Power Curve.
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| The analytical results of all samples were less than an OpSOF of one when compared to the OpDCGLs.
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| Although MARSSIM states that the Sign Test need not be performed in the instance that no measurements surpass the DCGL, the test was conducted to demonstrate coherence to the statistical principles of the DQO process. The Sign Test was performed on the data and compared to the original assumptions of the DQOs. The evaluation of the Sign Test results clearly demonstrates that the survey unit passes the unrestricted release criteria, thus, the null hypothesis is rejected. The Sign Test is included in Attachment 4.
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| The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). All data were considered valid including negative values, zeros, values reported below the MDC, and values with uncertainties greater than two standard deviations. The mean and median values for each ROC were well below the respective OpDCGLs. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criteria with adequate power as required by the DQOs.
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| The data for Co-60 and Cs-137 are represented graphically through a frequency plot and a quantile plot. All graphical representations are provided in Attachment 6.
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| : 13. ANOMALIES No anomalies were observed during the performance or analyses of the survey.
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| : 14. CONCLUSION Survey unit 10221C has met the DQOs of the FSS plan. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved. The EMC for soils was not needed for this survey unit.
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| [34]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C All identified ROC were used for statistical testing to determine the adequacy of the survey unit for FSS. Evaluation of the data shows that none of the ROC concentration values exceed the OpDCGL or any investigational levels; therefore, in accordance with the LTP Section 5.10, the survey unit meets the release criterion.
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| The sample data passed the Sign Test. The null hypothesis was rejected. The Retrospective Power Curve showed that adequate power was achieved.
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| The mean BcSOF, when the analytical results were compared to the BcDCGLs, was 0.017, which results in a dose contribution from soil in survey unit 10221C of 0.427 mrem/year TEDE, based on the average concentration of the ROC in samples used for non-parametric statistical sampling.
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| The conclusion of this Release Record is that survey unit 10221C is acceptable for unrestricted release.
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| : 15. REFERENCES
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| : 1. ZionSolutions procedure ZS-LT-300-001-005, Final Status Survey Data Reporting
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| : 2. Zion Station Restoration Project License Termination Plan
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| : 3. ZionSolutions procedure ZS-LT-300-001-001, Final Status Survey Package Development
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| : 4. NUREG-1575, Multi-Agency Radiation Survey and Site Investigation Manual
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| : 5. ZionSolutions procedure ZS-LT-300-001-002, Survey Unit Classification
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| : 6. Zion Station Historical Site Assessment
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| : 7. ZionSolutions TSD 11-001, Technical Support Document for Potential Radionuclides of Concern During the Decommissioning of the Zion Station
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| : 8. ZionSolutions TSD 14-019, Radionuclides of Concern for Soil and Basement Fill Model Source Terms
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| : 9. ZionSolutions TSD 14-011, Soil Area Factors
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| : 10. ZionSolutions TSD 17-004, Operational Derived Concentration Guideline Levels for Final Status Survey
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| : 11. ZionSolutions TSD 11-004, Ludlum Model 44-10 Detector Sensitivity
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| : 12. ZionSolutions procedure ZS-LT-01, Quality Assurance Project Plan (for Characterization and FSS)
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| : 13. ZionSolutions procedure ZS-LT-300-001-003, Isolation and Control for Final Status Survey
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| : 14. ZionSolutions procedure ZS-RP-108-004-011, Operation of the Ludlum Model 2350-1 Data Logger
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| [35]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
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| : 15. ZionSolutions TSD 13-004, Examination of Cs-137 Global Fallout In Soils At Zion Station
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| : 16. ZionSolutions procedure ZS-LT-300-001-004, Final Status Survey Data Assessment
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| : 16. ATTACHMENTS
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| : 1. Attachment 1 - Figures and Map
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| : 2. Attachment 2 - Scan Data
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| : 3. Attachment 3 - Consultation Triggers for Residential and Commercial/Industrial Soil Contamination
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| : 4. Attachment 4 - Sign Test
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| : 5. Attachment 5 - QC Sample Assessment
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| : 6. Attachment 6 - Graphical Presentations
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| : 7. Attachment 7 - Sample Analytical Reports
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| : 8. Attachment 8 - Eberline Analytical Reports
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| [36]
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| ATTACHMENT 1 FIGURES AND MAP
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| [37]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Final Status Survey Boundaries and Systematic Sample Points
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| [38]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Final Status Survey Boundaries with Relocated Systematic Sample Points
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| [39]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Elevated Areas Discovered during Radiological Assessment
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| [40]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Judgmental Sample Points taken Adjacent to Railroad Ballast
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| [41]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Survey Unit 10221C Final Status Survey Scan Rows
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| [42]
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| ATTACHMENT 2 SCAN DATA
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| [43]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR363311 304718 10221C GS001 7/24/2019 13:17 2090 1668 2285 No 44-10 PR363311 304718 10221C GS001 7/24/2019 13:19 1975 1668 2285 No 44-10 PR363311 304718 10221C GS001 7/24/2019 13:21 1917 1668 2285 No 44-10 PR363311 304718 10221C GS001 7/24/2019 13:23 1955 1668 2285 No 44-10 PR363311 304718 10221C GS002 7/24/2019 13:25 2035 1668 2285 No 44-10 PR363311 304718 10221C GS002 7/24/2019 13:27 2178 1668 2285 No 44-10 PR363311 304718 10221C GS002 7/24/2019 13:29 2063 1668 2285 No 44-10 PR363311 304718 10221C GS003 7/24/2019 13:33 2198 1668 2285 No 44-10 PR363311 304718 10221C GS003 7/24/2019 13:35 1967 1668 2285 No 44-10 PR363311 304718 10221C GS003 7/24/2019 13:37 2022 1668 2285 No 44-10 PR363311 304718 10221C GS003 7/24/2019 13:39 1979 1668 2285 No 44-10 PR363311 304718 10221C GS004 7/24/2019 13:41 1931 1668 2285 No 44-10 PR363311 304718 10221C GS004 7/24/2019 13:43 1996 1668 2285 No 44-10 PR363311 304718 10221C GS004 7/24/2019 13:45 1909 1668 2285 No 44-10 PR363311 304718 10221C GS004 7/24/2019 13:47 1871 1668 2285 No 44-10 PR363311 304718 10221C GS005 7/24/2019 13:49 1704 1668 2285 No 44-10 PR363311 304718 10221C GS005 7/24/2019 13:51 1815 1668 2285 No 44-10 PR363311 304718 10221C GS005 7/24/2019 13:53 1800 1668 2285 No 44-10 PR363311 304718 10221C GS005 7/24/2019 13:55 1692 1668 2285 No 44-10 PR363311 304718 10221C GS006 7/24/2019 14:13 1767 1668 2285 No 44-10 PR363311 304718 10221C GS006 7/24/2019 14:15 1740 1668 2285 No 44-10 PR363311 304718 10221C GS006 7/24/2019 14:17 1745 1668 2285 No 44-10 PR363311 304718 10221C GS006 7/24/2019 14:19 1760 1668 2285 No 44-10 PR363311 304718 10221C GS007 7/24/2019 14:21 1744 1668 2285 No 44-10 PR363311 304718 10221C GS007 7/24/2019 14:23 1840 1668 2285 No 44-10 PR363311 304718 10221C GS007 7/24/2019 14:25 1685 1668 2285 No 44-10 PR363311 304718 10221C GS007 7/24/2019 14:27 1712 1668 2285 No 44-10 PR363311 304718 10221C GS008 7/24/2019 14:29 1706 1668 2285 No 44-10 PR363311 304718 10221C GS008 7/24/2019 14:31 1939 1668 2285 No 44-10 PR363311 304718 10221C GS008 7/24/2019 14:33 1839 1668 2285 No 44-10 PR363311 304718 10221C GS008 7/24/2019 14:35 1716 1668 2285 No 44-10 PR321902 304711 10221C GS033 7/24/2019 12:56 2574 2382 3120 No 44-10 PR321902 304711 10221C GS033 7/24/2019 12:58 2481 2382 3120 No 44-10 PR321902 304711 10221C GS033 7/24/2019 13:00 2113 2382 3120 No 44-10 PR321902 304711 10221C GS033 7/24/2019 13:03 2467 2382 3120 No
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| [44]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR321902 304711 10221C GS034 7/24/2019 13:06 2039 2382 3120 No 44-10 PR321902 304711 10221C GS034 7/24/2019 13:09 2380 2382 3120 No 44-10 PR321902 304711 10221C GS034 7/24/2019 13:12 2620 2382 3120 No 44-10 PR321902 304711 10221C GS034 7/24/2019 13:14 2765 2382 3120 No 44-10 PR321902 304711 10221C GS035 7/24/2019 13:17 2813 2382 3120 No 44-10 PR321902 304711 10221C GS035 7/24/2019 13:19 2544 2382 3120 No 44-10 PR321902 304711 10221C GS035 7/24/2019 13:21 2215 2382 3120 No 44-10 PR321902 304711 10221C GS035 7/24/2019 13:23 2464 2382 3120 No 44-10 PR321902 304711 10221C GS036 7/24/2019 13:26 2127 2382 3120 No 44-10 PR321902 304711 10221C GS036 7/24/2019 13:29 2674 2382 3120 No 44-10 PR321902 304711 10221C GS036 7/24/2019 13:31 2718 2382 3120 No 44-10 PR321902 304711 10221C GS036 7/24/2019 13:35 2565 2382 3120 No 44-10 PR321902 304711 10221C GS037 7/24/2019 13:38 3011 2382 3120 No 44-10 PR321902 304711 10221C GS037 7/24/2019 13:40 2804 2382 3120 No 44-10 PR321902 304711 10221C GS037 7/24/2019 13:42 2775 2382 3120 No 44-10 PR321902 304711 10221C GS037 7/24/2019 13:45 2405 2382 3120 No 44-10 PR321902 304711 10221C GS038 7/24/2019 13:48 2420 2382 3120 No 44-10 PR321902 304711 10221C GS038 7/24/2019 13:50 2642 2382 3120 No 44-10 PR321902 304711 10221C GS038 7/24/2019 13:52 2881 2382 3120 No 44-10 PR321902 304711 10221C GS038 7/24/2019 13:57 3109 2382 3120 No 44-10 PR321902 304711 10221C GS039 7/24/2019 14:02 2928 2382 3120 No 44-10 PR321902 304711 10221C GS039 7/24/2019 14:05 2889 2382 3120 No 44-10 PR321902 304711 10221C GS039 7/24/2019 14:08 2808 2382 3120 No 44-10 PR321902 304711 10221C GS039 7/24/2019 14:10 2686 2382 3120 No 44-10 PR321902 304711 10221C GS040 7/24/2019 14:13 2944 2382 3120 No 44-10 PR321902 304711 10221C GS040 7/24/2019 14:16 3057 2382 3120 No 44-10 PR321902 304711 10221C GS040 7/24/2019 14:18 2933 2382 3120 No 44-10 PR321902 304711 10221C GS040 7/24/2019 14:21 2972 2382 3120 No 44-10 PR375273 304730 10221C GS009 7/24/2019 12:50 1875 1633 2244 No 44-10 PR375273 304730 10221C GS009 7/24/2019 12:52 1689 1633 2244 No 44-10 PR375273 304730 10221C GS009 7/24/2019 12:54 1658 1633 2244 No 44-10 PR375273 304730 10221C GS009 7/24/2019 13:03 1693 1633 2244 No 44-10 PR375273 304730 10221C GS010 7/24/2019 13:05 1680 1633 2244 No 44-10 PR375273 304730 10221C GS010 7/24/2019 13:07 1679 1633 2244 No 44-10 PR375273 304730 10221C GS010 7/24/2019 13:09 1772 1633 2244 No 44-10 PR375273 304730 10221C GS010 7/24/2019 13:11 1806 1633 2244 No
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| [45]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR375273 304730 10221C GS011 7/24/2019 13:13 1943 1633 2244 No 44-10 PR375273 304730 10221C GS011 7/24/2019 13:15 1938 1633 2244 No 44-10 PR375273 304730 10221C GS011 7/24/2019 13:17 1788 1633 2244 No 44-10 PR375273 304730 10221C GS011 7/24/2019 13:19 1754 1633 2244 No 44-10 PR375273 304730 10221C GS012 7/24/2019 13:21 1772 1633 2244 No 44-10 PR375273 304730 10221C GS012 7/24/2019 13:23 2049 1633 2244 No 44-10 PR375273 304730 10221C GS012 7/24/2019 13:25 1763 1633 2244 No 44-10 PR375273 304730 10221C GS012 7/24/2019 13:27 1830 1633 2244 No 44-10 PR375273 304730 10221C GS013 7/24/2019 13:29 1753 1633 2244 No 44-10 PR375273 304730 10221C GS013 7/24/2019 13:31 1946 1633 2244 No 44-10 PR375273 304730 10221C GS013 7/24/2019 13:33 1946 1633 2244 No 44-10 PR375273 304730 10221C GS013 7/24/2019 13:35 1871 1633 2244 No 44-10 PR375273 304730 10221C GS014 7/24/2019 13:37 1911 1633 2244 No 44-10 PR375273 304730 10221C GS014 7/24/2019 13:39 1984 1633 2244 No 44-10 PR375273 304730 10221C GS014 7/24/2019 13:41 1741 1633 2244 No 44-10 PR375273 304730 10221C GS014 7/24/2019 13:43 1775 1633 2244 No 44-10 PR375273 304730 10221C GS015 7/24/2019 13:45 1850 1633 2244 No 44-10 PR375273 304730 10221C GS015 7/24/2019 13:47 1972 1633 2244 No 44-10 PR375273 304730 10221C GS015 7/24/2019 13:52 1864 1633 2244 No 44-10 PR375273 304730 10221C GS015 7/24/2019 14:03 1885 1633 2244 No 44-10 PR375273 304730 10221C GS016 7/24/2019 14:06 1674 1633 2244 No 44-10 PR375273 304730 10221C GS016 7/24/2019 14:08 1669 1633 2244 No 44-10 PR375273 304730 10221C GS016 7/24/2019 14:10 1728 1633 2244 No 44-10 PR375273 304730 10221C GS016 7/24/2019 14:12 1923 1633 2244 No 44-10 PR308037 266657 10221C GS025 7/24/2019 12:56 2359 2082 2771 No 44-10 PR308037 266657 10221C GS025 7/24/2019 13:00 2163 2082 2771 No 44-10 PR308037 266657 10221C GS025 7/24/2019 13:02 1980 2082 2771 No 44-10 PR308037 266657 10221C GS025 7/24/2019 13:04 1925 2082 2771 No 44-10 PR308037 266657 10221C GS026 7/24/2019 13:09 2082 2082 2771 No 44-10 PR308037 266657 10221C GS026 7/24/2019 13:12 2181 2082 2771 No 44-10 PR308037 266657 10221C GS026 7/24/2019 13:14 2318 2082 2771 No 44-10 PR308037 266657 10221C GS026 7/24/2019 13:16 2472 2082 2771 No 44-10 PR308037 266657 10221C GS027 7/24/2019 13:18 2277 2082 2771 No 44-10 PR308037 266657 10221C GS027 7/24/2019 13:20 2349 2082 2771 No 44-10 PR308037 266657 10221C GS027 7/24/2019 13:22 2031 2082 2771 No 44-10 PR308037 266657 10221C GS027 7/24/2019 13:25 2055 2082 2771 No
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| [46]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR308037 266657 10221C GS028 7/24/2019 13:29 2011 2082 2771 No 44-10 PR308037 266657 10221C GS028 7/24/2019 13:32 2134 2082 2771 No 44-10 PR308037 266657 10221C GS028 7/24/2019 13:35 2244 2082 2771 No 44-10 PR308037 266657 10221C GS028 7/24/2019 13:37 2261 2082 2771 No 44-10 PR308037 266657 10221C GS029 7/24/2019 13:40 2227 2082 2771 No 44-10 PR308037 266657 10221C GS029 7/24/2019 13:42 2196 2082 2771 No 44-10 PR308037 266657 10221C GS029 7/24/2019 13:44 2055 2082 2771 No 44-10 PR308037 266657 10221C GS029 7/24/2019 13:47 1926 2082 2771 No 44-10 PR308037 266657 10221C GS030 7/24/2019 13:51 2103 2082 2771 No 44-10 PR308037 266657 10221C GS030 7/24/2019 13:54 2158 2082 2771 No 44-10 PR308037 266657 10221C GS030 7/24/2019 13:56 2282 2082 2771 No 44-10 PR308037 266657 10221C GS030 7/24/2019 13:59 2426 2082 2771 No 44-10 PR308037 266657 10221C GS031 7/24/2019 14:03 2554 2082 2771 No 44-10 PR308037 266657 10221C GS031 7/24/2019 14:06 2336 2082 2771 No 44-10 PR308037 266657 10221C GS031 7/24/2019 14:08 2118 2082 2771 No 44-10 PR308037 266657 10221C GS031 7/24/2019 14:11 2051 2082 2771 No 44-10 PR308037 266657 10221C GS032 7/24/2019 14:13 1998 2082 2771 No 44-10 PR308037 266657 10221C GS032 7/24/2019 14:16 2304 2082 2771 No 44-10 PR308037 266657 10221C GS032 7/24/2019 14:18 2520 2082 2771 No 44-10 PR316938 293136 10221C GS049 7/24/2001 13:49 3019 2779 3576 No 44-10 PR316938 293136 10221C GS049 7/24/2001 13:52 3080 2779 3576 No 44-10 PR316938 293136 10221C GS049 7/24/2001 13:54 3320 2779 3576 No 44-10 PR316938 293136 10221C GS049 7/24/2001 13:56 3359 2779 3576 No 44-10 PR316938 293136 10221C GS050 7/24/2001 14:00 2986 2779 3576 No 44-10 PR316938 293136 10221C GS050 7/24/2001 14:02 3076 2779 3576 No 44-10 PR316938 293136 10221C GS050 7/24/2001 14:07 3060 2779 3576 No 44-10 PR316938 293136 10221C GS050 7/24/2001 14:09 3055 2779 3576 No 44-10 PR316938 293136 10221C GS051 7/24/2001 14:13 2989 2779 3576 No 44-10 PR316938 293136 10221C GS051 7/24/2001 14:16 3069 2779 3576 No 44-10 PR316938 293136 10221C GS051 7/24/2001 14:18 3162 2779 3576 No 44-10 PR316938 293136 10221C GS051 7/24/2001 14:21 3544 2779 3576 No 44-10 PR316938 293136 10221C GS052 7/24/2001 14:26 2945 2779 3576 No 44-10 PR316938 293136 10221C GS052 7/24/2001 14:29 3251 2779 3576 No 44-10 PR316938 293136 10221C GS052 7/24/2001 14:31 3168 2779 3576 No 44-10 PR316938 293136 10221C GS052 7/24/2001 14:33 3316 2779 3576 No 44-10 PR316938 293136 10221C GS053 7/24/2001 14:37 2976 2779 3576 No
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| [47]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR316938 293136 10221C GS053 7/24/2001 14:39 3264 2779 3576 No 44-10 PR316938 293136 10221C GS053 7/24/2001 14:41 3174 2779 3576 No 44-10 PR316938 293136 10221C GS053 7/24/2001 14:43 3337 2779 3576 No 44-10 PR316938 293136 10221C GS054 7/24/2001 14:47 3035 2779 3576 No 44-10 PR316938 293136 10221C GS054 7/24/2001 14:50 2987 2779 3576 No 44-10 PR316938 293136 10221C GS054 7/24/2001 14:52 3054 2779 3576 No 44-10 PR316938 293136 10221C GS054 7/24/2001 14:54 2804 2779 3576 No 44-10 PR316938 293136 10221C GS055 7/24/2001 14:58 3037 2779 3576 No 44-10 PR316938 293136 10221C GS055 7/24/2001 15:00 2983 2779 3576 No 44-10 PR316938 293136 10221C GS055 7/24/2001 15:02 3202 2779 3576 No 44-10 PR316938 293136 10221C GS055 7/24/2001 15:05 3188 2779 3576 No 44-10 PR316938 293136 10221C GS056 7/24/2001 15:08 2981 2779 3576 No 44-10 PR316938 293136 10221C GS056 7/24/2001 15:10 2959 2779 3576 No 44-10 PR316938 293136 10221C GS056 7/24/2001 15:12 3198 2779 3576 No 44-10 PR316938 293136 10221C GS056 7/24/2001 15:15 2875 2779 3576 No 44-10 PR363452 304726 10221C GS041 7/24/2019 13:49 3021 2770 3566 No 44-10 PR363452 304726 10221C GS041 7/24/2019 13:53 2951 2770 3566 No 44-10 PR363452 304726 10221C GS041 7/24/2019 13:56 2866 2770 3566 No 44-10 PR363452 304726 10221C GS041 7/24/2019 13:59 3103 2770 3566 No 44-10 PR363452 304726 10221C GS042 7/24/2019 14:02 2794 2770 3566 No 44-10 PR363452 304726 10221C GS042 7/24/2019 14:04 3064 2770 3566 No 44-10 PR363452 304726 10221C GS042 7/24/2019 14:08 3275 2770 3566 No 44-10 PR363452 304726 10221C GS042 7/24/2019 14:10 3061 2770 3566 No 44-10 PR363452 304726 10221C GS043 7/24/2019 14:12 3023 2770 3566 No 44-10 PR363452 304726 10221C GS043 7/24/2019 14:14 3067 2770 3566 No 44-10 PR363452 304726 10221C GS043 7/24/2019 14:16 3027 2770 3566 No 44-10 PR363452 304726 10221C GS043 7/24/2019 14:18 2809 2770 3566 No 44-10 PR363452 304726 10221C GS044 7/24/2019 14:21 2908 2770 3566 No 44-10 PR363452 304726 10221C GS044 7/24/2019 14:23 3050 2770 3566 No 44-10 PR363452 304726 10221C GS044 7/24/2019 14:25 3252 2770 3566 No 44-10 PR363452 304726 10221C GS044 7/24/2019 14:27 2983 2770 3566 No 44-10 PR363452 304726 10221C GS045 7/24/2019 14:29 3007 2770 3566 No 44-10 PR363452 304726 10221C GS045 7/24/2019 14:31 3063 2770 3566 No 44-10 PR363452 304726 10221C GS045 7/24/2019 14:33 2866 2770 3566 No 44-10 PR363452 304726 10221C GS045 7/24/2019 14:35 2944 2770 3566 No 44-10 PR363452 304726 10221C GS046 7/24/2019 14:37 2995 2770 3566 No
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| [48]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR363452 304726 10221C GS046 7/24/2019 14:39 3011 2770 3566 No 44-10 PR363452 304726 10221C GS046 7/24/2019 14:41 3063 2770 3566 No 44-10 PR363452 304726 10221C GS046 7/24/2019 14:43 2831 2770 3566 No 44-10 PR363452 304726 10221C GS047 7/24/2019 14:45 2970 2770 3566 No 44-10 PR363452 304726 10221C GS047 7/24/2019 14:47 3109 2770 3566 No 44-10 PR363452 304726 10221C GS047 7/24/2019 14:49 2881 2770 3566 No 44-10 PR363452 304726 10221C GS047 7/24/2019 14:51 2854 2770 3566 No 44-10 PR363452 304726 10221C GS048 7/24/2019 14:53 2851 2770 3566 No 44-10 PR363452 304726 10221C GS048 7/24/2019 14:55 3094 2770 3566 No 44-10 PR363452 304726 10221C GS048 7/24/2019 14:57 3188 2770 3566 No 44-10 PR363452 304726 10221C GS048 7/24/2019 14:59 2982 2770 3566 No 44-10 PR308037 266657 10221C GS032 7/25/2019 7:12 2616 2353 3087 No 44-10 PR363311 304718 10221C GS002 7/25/2019 13:06 2407 1801 2443 No 44-10 PR316938 293136 10221C GS057 7/25/2001 8:10 3002 2562 3327 No 44-10 PR316938 293136 10221C GS057 7/25/2001 8:13 3044 2562 3327 No 44-10 PR316938 293136 10221C GS057 7/25/2001 8:15 2922 2562 3327 No 44-10 PR316938 293136 10221C GS057 7/25/2001 8:17 3059 2562 3327 No 44-10 PR316938 293136 10221C GS058 7/25/2001 8:20 2985 2562 3327 No 44-10 PR316938 293136 10221C GS058 7/25/2001 8:23 3030 2562 3327 No 44-10 PR316938 293136 10221C GS058 7/25/2001 8:25 2826 2562 3327 No 44-10 PR316938 293136 10221C GS058 7/25/2001 8:27 3276 2562 3327 No 44-10 PR316938 293136 10221C GS059 7/25/2001 8:32 2803 2562 3327 No 44-10 PR316938 293136 10221C GS059 7/25/2001 8:34 2918 2562 3327 No 44-10 PR316938 293136 10221C GS059 7/25/2001 8:36 2982 2562 3327 No 44-10 PR316938 293136 10221C GS059 7/25/2001 8:38 3128 2562 3327 No 44-10 PR316938 293136 10221C GS060 7/25/2001 8:42 2653 2562 3327 No 44-10 PR316938 293136 10221C GS060 7/25/2001 8:45 2886 2562 3327 No 44-10 PR316938 293136 10221C GS060 7/25/2001 8:47 2917 2562 3327 No 44-10 PR316938 293136 10221C GS060 7/25/2001 8:49 3000 2562 3327 No 44-10 PR363452 304726 10221C GS061 7/25/2019 8:06 3024 2680 3463 No 44-10 PR363452 304726 10221C GS061 7/25/2019 8:09 2858 2680 3463 No 44-10 PR363452 304726 10221C GS061 7/25/2019 8:11 2752 2680 3463 No 44-10 PR363452 304726 10221C GS062 7/25/2019 8:14 2732 2680 3463 No 44-10 PR363452 304726 10221C GS062 7/25/2019 8:16 2890 2680 3463 No 44-10 PR363452 304726 10221C GS062 7/25/2019 8:18 3053 2680 3463 No 44-10 PR363452 304726 10221C GS063 7/25/2019 8:20 3188 2680 3463 No
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| [49]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR363452 304726 10221C GS063 7/25/2019 8:22 2950 2680 3463 No 44-10 PR363452 304726 10221C GS063 7/25/2019 8:24 2816 2680 3463 No 44-10 PR363452 304726 10221C GS064 7/25/2019 8:27 2971 2680 3463 No 44-10 PR363452 304726 10221C GS064 7/25/2019 8:29 2810 2680 3463 No 44-10 PR363452 304726 10221C GS065 7/25/2019 8:32 2799 2680 3463 No 44-10 PR363452 304726 10221C GS065 7/25/2019 8:34 2788 2680 3463 No 44-10 PR363452 304726 10221C GS066 7/25/2019 8:37 2729 2680 3463 No 44-10 PR363452 304726 10221C GS067 7/25/2019 8:40 2929 2680 3463 No 44-10 PR363452 304726 10221C GS068 7/25/2019 8:44 2712 2680 3463 No 44-10 PR372143 304712 10221C GS017 9/17/2019 9:12 1905 1812 2456 No 44-10 PR372143 304712 10221C GS017 9/17/2019 9:14 1906 1812 2456 No 44-10 PR372143 304712 10221C GS017 9/17/2019 9:16 1927 1812 2456 No 44-10 PR372143 304712 10221C GS017 9/17/2019 9:18 2070 1812 2456 No 44-10 PR372143 304712 10221C GS018 9/17/2019 9:20 2345 1812 2456 No 44-10 PR372143 304712 10221C GS018 9/17/2019 9:23 2091 1812 2456 No 44-10 PR372143 304712 10221C GS018 9/17/2019 9:25 1913 1812 2456 No 44-10 PR372143 304712 10221C GS018 9/17/2019 9:27 1861 1812 2456 No 44-10 PR372143 304712 10221C GS019 9/17/2019 9:29 1946 1812 2456 No 44-10 PR372143 304712 10221C GS019 9/17/2019 9:31 1985 1812 2456 No 44-10 PR372143 304712 10221C GS019 9/17/2019 9:33 2263 1812 2456 No 44-10 PR372143 304712 10221C GS019 9/17/2019 9:36 2292 1812 2456 No 44-10 PR372143 304712 10221C GS020 9/17/2019 9:38 2197 1812 2456 No 44-10 PR372143 304712 10221C GS020 9/17/2019 9:40 2156 1812 2456 No 44-10 PR372143 304712 10221C GS020 9/17/2019 9:42 2020 1812 2456 No 44-10 PR372143 304712 10221C GS020 9/17/2019 9:44 1873 1812 2456 No 44-10 PR372143 304712 10221C GS021 9/17/2019 9:47 1966 1812 2456 No 44-10 PR372143 304712 10221C GS021 9/17/2019 9:49 1987 1812 2456 No 44-10 PR372143 304712 10221C GS021 9/17/2019 9:51 2353 1812 2456 No 44-10 PR372143 304712 10221C GS021 9/17/2019 9:53 2408 1812 2456 No 44-10 PR372143 304712 10221C GS022 9/17/2019 9:56 2246 1812 2456 No 44-10 PR372143 304712 10221C GS022 9/17/2019 9:58 2180 1812 2456 No 44-10 PR372143 304712 10221C GS022 9/17/2019 10:00 1976 1812 2456 No 44-10 PR372143 304712 10221C GS022 9/17/2019 10:02 1931 1812 2456 No 44-10 PR372143 304712 10221C GS023 9/17/2019 10:04 1834 1812 2456 No 44-10 PR372143 304712 10221C GS023 9/17/2019 10:07 2158 1812 2456 No 44-10 PR372143 304712 10221C GS023 9/17/2019 10:09 2180 1812 2456 No
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| [50]
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| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Scan Avg Action Detector Detector M2350- Survey Logged Scan Location Date/Time Background Level Type ID 1 ID Unit Result Alarms (cpm) (cpm) (cpm) 44-10 PR372143 304712 10221C GS023 9/17/2019 10:11 2340 1812 2456 No 44-10 PR372143 304712 10221C GS024 9/17/2019 10:13 2258 1812 2456 No 44-10 PR372143 304712 10221C GS024 9/17/2019 10:15 2099 1812 2456 No 44-10 PR372143 304712 10221C GS024 9/17/2019 10:17 2168 1812 2456 No 44-10 PR372143 304712 10221C GS024 9/17/2019 10:19 1946 1812 2456 No
| |
| [51]
| |
| | |
| ATTACHMENT 3 CONSULTATION TRIGGERS FOR RESIDENTIAL AND COMMERCIAL/INDUSTRIAL SOIL CONTAMINATION
| |
| [52]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
| |
| [53]
| |
| | |
| ATTACHMENT 4 SIGN TEST
| |
| [54]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
| |
| [55]
| |
| | |
| ATTACHMENT 5 QC SAMPLE ASSESSMENT
| |
| [56]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
| |
| [57]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C
| |
| [58]
| |
| | |
| ATTACHMENT 6 GRAPHICAL PRESENTATIONS
| |
| [59]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Posting Plot
| |
| [60]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C QUANTILE PLOT FOR Co-60 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 3.19E-02 pCi/g Quantile Plot For Co-60 1.20E-01 1.00E-01 Concentration (pCi/g) 8.00E-02 6.00E-02 4.00E-02 2.00E-02 0.00E+00 0% 20% 40% 60% 80% 100%
| |
| Percentage
| |
| [61]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C QUANTILE PLOT FOR Cs-137 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 7.78E-02 pCi/g Quantile Plot For Cs-137 5.00E-01 4.50E-01 4.00E-01 Concentration (pCi/g) 3.50E-01 3.00E-01 2.50E-01 2.00E-01 1.50E-01 1.00E-01 5.00E-02 0.00E+00 0% 20% 40% 60% 80% 100%
| |
| Percentage
| |
| [62]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C HISTOGRAM FOR Co-60 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 3.19E-02 pCi/g Median: 2.59E-02 pCi/g ST DEV: 0.029 Skew: 1.694 Frequency Plot For Co-60 10 9 8 8
| |
| 7 Frequency 6 5 5
| |
| 4 3 2 2 2
| |
| 1 0 0 0
| |
| 1.75E-02 3.50E-02 5.25E-02 7.00E-02 8.75E-02 1.05E-01 Upper End Value (pCi/g)
| |
| Observation Observation Upper Value Frequency %
| |
| 1.75E-02 5 29%
| |
| 3.50E-02 8 47%
| |
| 5.25E-02 2 12%
| |
| 7.00E-02 0 0%
| |
| 8.75E-02 0 0%
| |
| 1.05E-01 2 12%
| |
| TOTAL 17 100%
| |
| [63]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C HISTOGRAM FOR Cs-137 Survey Unit: 10221C Survey Unit Name: South of Protected Area - Inland Mean: 7.78E-02 pCi/g Median: 3.65E-02 pCi/g ST DEV: 0.120 Skew: 2.305 Frequency Plot For Cs-137 14 12 12 10 Frequency 8
| |
| 6 4 3 2 1 1 0 0 0
| |
| 7.20E-02 1.44E-01 2.16E-01 2.88E-01 3.60E-01 4.32E-01 Upper End Value (pCi/g)
| |
| Observation Observation Upper Value Frequency %
| |
| 7.20E-02 12 71%
| |
| 1.44E-01 3 18%
| |
| 2.16E-01 0 0%
| |
| 2.88E-01 0 0%
| |
| 3.60E-01 1 6%
| |
| 4.32E-01 1 6%
| |
| TOTAL 17 100%
| |
| [64]
| |
| | |
| FSS RELEASE RECORD - REV. 1 SOUTH OF PROTECTED AREA - INLAND SURVEY UNIT 10221C Prospective and Retrospective Power Curves for Survey Unit 10221C
| |
| [65]
| |
| | |
| ATTACHMENT 7 SAMPLE ANALYTICAL REPORTS
| |
| [66]
| |
| | |
| 6/12/2019 12:23:23PM Page 1 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10014 Sample Description : L1-10221C-FSGS-001SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.582E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:15:00AM Acquisition Started : 6/12/2019 12:08:14PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77295 Fill Height : 1581.63 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:23:16PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [67]
| |
| | |
| 6/12/2019 12:23:23PM Page 2 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.60 472 - 480 477.38 4.91E+01 15.30 8.59E+01 0.83 2 352.00 699 - 708 703.94 6.39E+01 11.58 3.11E+01 1.45 3 609.26 1212 - 1223 1218.09 6.68E+01 9.50 9.16E+00 1.60 4 1461.04 2915 - 2928 2922.14 1.49E+02 12.97 7.00E+00 1.84 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 2.78E+00 2.70E-01 Bi-211 0.87 351.07
| |
| * 13.02 3.80E-01 7.55E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 6.85E-02 2.20E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.64E-01 2.54E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 [68]
| |
| | |
| 6/12/2019 12:23:23PM Page 3 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.39E-01 2.76E-02 785.96 1.06
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.992 2.78E+00 2.70E-01
| |
| ? Bi-211 0.871 3.80E-01 7.55E-02 Pb-212 1.000 6.85E-02 2.20E-02 Bi-214 1.000 1.64E-01 2.54E-02
| |
| ? Pb-214 1.000 1.39E-01 2.76E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [69]
| |
| | |
| 6/12/2019 12:23:23PM Page 4 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:23:16PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.30E-02 5.00E-02 5.00E-02 BE-7 477.60 10.44 1.67E-01 3.28E-01 3.28E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.78E+00 3.31E-01 3.31E-01 Mn-54 834.85 99.98 5.17E-03 3.70E-02 3.70E-02 Co-60 1173.23 99.85 5.95E-03 3.87E-02 3.98E-02 1332.49 99.98 1.95E-02 3.87E-02 Nb-94 702.65 99.81 2.69E-03 2.66E-02 2.93E-02 871.09 99.89 2.12E-03 2.66E-02 Ag-108m 79.13 6.60 -5.35E-02 2.88E-02 9.13E-01 433.94 90.50 3.75E-03 2.88E-02 614.28 89.80 -2.46E-02 4.21E-02 722.94 90.80 -1.83E-02 3.12E-02 Sb-125 176.31 6.84 5.57E-02 9.11E-02 4.22E-01 380.45 1.52 1.10E-01 1.75E+00 427.87 29.60 -3.28E-02 9.11E-02 463.36 10.49 4.71E-02 2.86E-01 600.60 17.65 -9.94E-02 1.53E-01 606.71 4.98 -2.05E-01 1.04E+00 635.95 11.22 1.41E-02 2.55E-01 [70]
| |
| | |
| 6/12/2019 12:23:23PM Page 5 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.54E-01 9.11E-02 1.76E+00 Ba-133 79.61 2.65 -2.55E-01 5.63E-02 2.16E+00 81.00 32.90 -1.27E-01 1.52E-01 276.40 7.16 1.04E-01 4.00E-01 302.85 18.34 4.68E-02 1.53E-01 356.01 62.05 -2.35E-02 5.63E-02 383.85 8.94 3.93E-02 3.13E-01 Cs-134 475.36 1.48 1.28E+00 3.88E-02 2.26E+00 563.25 8.34 -3.85E-02 3.61E-01 569.33 15.37 3.13E-02 1.73E-01 604.72 97.62 -1.42E-02 4.57E-02 795.86 85.46 1.05E-02 3.88E-02 801.95 8.69 4.13E-02 4.07E-01 1038.61 0.99 1.85E-01 3.81E+00 1167.97 1.79 -1.27E-01 2.05E+00 1365.19 3.02 2.71E-01 9.76E-01 Cs-137 661.66 85.10 1.71E-02 4.11E-02 4.11E-02 Eu-152 121.78 28.67 -3.07E-02 9.76E-02 9.76E-02 244.70 7.61 4.31E-02 3.95E-01 295.94 0.45 3.06E+00 6.90E+00 344.28 26.60 -1.08E-04 1.15E-01 367.79 0.86 7.47E-01 3.48E+00 411.12 2.24 1.60E-01 1.16E+00 443.96 2.83 1.34E-01 9.90E-01 488.68 0.42 3.96E-02 6.91E+00 563.99 0.49 -3.93E-01 6.03E+00 586.26 0.46 7.77E+00 8.73E+00 678.62 0.47 3.25E+00 6.96E+00 688.67 0.86 7.52E-01 3.20E+00 719.35 0.28 -2.34E+00 9.87E+00 778.90 12.96 6.84E-02 2.62E-01 810.45 0.32 6.77E+00 1.28E+01 867.37 4.26 -1.09E-01 6.89E-01 919.33 0.43 -2.78E+00 9.36E+00 964.08 14.65 -4.93E-02 2.67E-01 1085.87 10.24 2.43E-01 3.95E-01 1089.74 1.73 -4.48E-01 2.02E+00 1112.07 13.69 -5.26E-02 2.87E-01 1212.95 1.43 -4.29E-02 3.29E+00 1249.94 0.19 -2.95E+00 2.02E+01 1299.14 1.63 -4.87E-02 2.41E+00 1408.01 21.07 -2.20E-02 1.25E-01 1457.64 0.50 -2.17E+00 2.50E+01 1528.10 0.28 -3.28E+00 7.04E+00 Eu-154 123.07 40.40 -3.92E-02 6.79E-02 6.79E-02 247.93 6.89 -1.89E-01 3.50E-01 591.76 4.95 2.05E-01 6.75E-01 692.42 1.78 5.14E-02 1.63E+00 723.30 20.06 -2.16E-03 1.55E-01 756.80 4.52 -1.60E-01 6.30E-01 873.18 12.08 9.59E-02 2.36E-01
| |
| [71]
| |
| | |
| 6/12/2019 12:23:23PM Page 6 of 6 Analysis Report for 12-Jun-19-10014 L1-10221C-FSGS-001SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 2.45E-02 6.79E-02 3.58E-01 1004.76 18.01 1.91E-01 2.43E-01 1274.43 34.80 -3.89E-02 1.08E-01 1596.48 1.80 -1.97E-01 1.73E+00 Eu-155 45.30 1.31 2.38E+00 1.53E-01 8.99E+00 60.01 1.22 1.76E+00 1.09E+01 86.55 30.70 1.36E-02 1.53E-01 105.31 21.10 4.67E-03 1.57E-01 Ra-226 186.21 3.64 3.81E-01 8.50E-01 8.50E-01 Pa-231 27.36 10.30 7.17E-01 1.06E+00 1.06E+00 283.69 1.70 6.26E-01 1.47E+00 300.07 2.47 -4.03E-01 1.14E+00 302.65 2.20 3.90E-01 1.27E+00 330.06 1.40 -1.98E-01 1.98E+00 U-235 143.76 10.96 -1.60E-02 5.46E-02 2.58E-01 163.33 5.08 4.60E-02 6.21E-01 185.71 57.20 3.54E-02 5.46E-02 202.11 1.08 -8.96E-01 2.73E+00 205.31 5.01 -1.69E-01 5.93E-01 Am-241 59.54 35.90 1.07E-01 3.90E-01 3.90E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [72]
| |
| | |
| 6/12/2019 12:23:34PM Page 1 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10015 Sample Description : L1-10221C-FSGS-002SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.800E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:20:00AM Acquisition Started : 6/12/2019 12:08:21PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.0 seconds Dead Time : 0.11 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77296 Fill Height : 1799.83 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:23:24PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [73]
| |
| | |
| 6/12/2019 12:23:34PM Page 2 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.85 948 - 961 955.51 6.17E+01 14.34 5.13E+01 0.78 2 295.30 1176 - 1185 1181.09 1.61E+01 7.97 2.09E+01 0.50 3 352.01 1402 - 1413 1407.76 4.26E+01 9.55 1.94E+01 0.62 4 1460.83 5835 - 5852 5843.14 1.20E+02 12.22 9.00E+00 1.42 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1.00 1460.82
| |
| * 10.66 2.87E+00 3.18E-01 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.08E-01 2.65E-02 300.09 3.30 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 7.46E-02 3.74E-02 351.93
| |
| * 35.60 1.16E-01 2.76E-02 785.96 1.06
| |
| [74]
| |
| | |
| 6/12/2019 12:23:34PM Page 3 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 1.000 2.87E+00 3.18E-01 X Bi-211 0.869 Pb-212 0.993 1.08E-01 2.65E-02 Pb-214 0.999 1.01E-01 2.22E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [75]
| |
| | |
| 6/12/2019 12:23:34PM Page 4 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:23:24PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.53E-02 5.58E-02 5.58E-02 BE-7 477.60 10.44 2.98E-01 4.16E-01 4.16E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.87E+00 5.08E-01 5.08E-01 Mn-54 834.85 99.98 7.74E-03 4.25E-02 4.25E-02 Co-60 1173.23 99.85 2.23E-02 4.64E-02 4.96E-02 1332.49 99.98 2.85E-02 4.64E-02 Nb-94 702.65 99.81 -9.07E-03 3.74E-02 4.19E-02 871.09 99.89 1.55E-02 3.74E-02 Ag-108m 79.13 6.60 1.27E+00 3.52E-02 1.70E+00 433.94 90.50 -1.71E-02 3.87E-02 614.28 89.80 -8.05E-03 5.55E-02 722.94 90.80 -4.20E-03 3.52E-02 Sb-125 176.31 6.84 -4.91E-01 1.25E-01 4.69E-01 380.45 1.52 -6.81E-01 2.00E+00 427.87 29.60 -3.21E-02 1.25E-01 463.36 10.49 -1.04E-01 3.26E-01 600.60 17.65 -1.44E-01 1.80E-01 606.71 4.98 1.36E+00 1.05E+00 635.95 11.22 2.32E-03 2.70E-01 [76]
| |
| | |
| 6/12/2019 12:23:34PM Page 5 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 4.85E-01 1.25E-01 1.91E+00 Ba-133 79.61 2.65 3.56E+00 6.95E-02 4.13E+00 81.00 32.90 -2.17E-01 2.72E-01 276.40 7.16 5.71E-02 4.71E-01 302.85 18.34 7.32E-02 1.87E-01 356.01 62.05 -4.88E-03 6.95E-02 383.85 8.94 2.13E-01 3.60E-01 Cs-134 475.36 1.48 7.87E-01 4.51E-02 2.89E+00 563.25 8.34 -2.04E-01 3.64E-01 569.33 15.37 -2.75E-02 1.94E-01 604.72 97.62 -5.18E-02 4.51E-02 795.86 85.46 1.31E-02 4.60E-02 801.95 8.69 -7.39E-02 4.43E-01 1038.61 0.99 -5.36E-01 3.98E+00 1167.97 1.79 -2.65E+00 2.62E+00 1365.19 3.02 4.82E-01 1.17E+00 Cs-137 661.66 85.10 2.68E-02 5.12E-02 5.12E-02 Eu-152 121.78 28.67 -2.76E-02 1.16E-01 1.33E-01 244.70 7.61 4.20E-01 5.50E-01 295.94 0.45 7.55E+00 8.90E+00 344.28 26.60 8.07E-02 1.16E-01 367.79 0.86 7.18E-01 4.06E+00 411.12 2.24 1.01E+00 1.53E+00 443.96 2.83 -6.33E-01 1.19E+00 488.68 0.42 7.60E-01 7.64E+00 563.99 0.49 -1.37E-01 6.35E+00 586.26 0.46 9.67E+00 1.08E+01 678.62 0.47 3.37E+00 7.83E+00 688.67 0.86 -2.26E+00 3.60E+00 719.35 0.28 -1.18E+01 1.06E+01 778.90 12.96 1.64E-01 3.33E-01 810.45 0.32 -7.77E+00 1.04E+01 867.37 4.26 -1.11E+00 8.47E-01 919.33 0.43 3.94E+00 8.78E+00 964.08 14.65 2.55E-02 3.40E-01 1085.87 10.24 -2.91E-01 4.36E-01 1089.74 1.73 -2.71E-01 2.66E+00 1112.07 13.69 5.01E-02 3.31E-01 1212.95 1.43 1.71E-01 3.46E+00 1249.94 0.19 6.03E+00 2.18E+01 1299.14 1.63 -1.33E+00 2.70E+00 1408.01 21.07 1.06E-01 2.03E-01 1457.64 0.50 7.08E+01 3.02E+01 1528.10 0.28 7.02E-01 1.05E+01 Eu-154 123.07 40.40 -4.92E-03 9.53E-02 9.53E-02 247.93 6.89 4.32E-01 5.48E-01 591.76 4.95 1.52E-01 7.25E-01 692.42 1.78 2.93E-01 2.06E+00 723.30 20.06 -1.66E-02 1.59E-01 756.80 4.52 -4.61E-01 8.40E-01 873.18 12.08 1.93E-01 3.00E-01
| |
| [77]
| |
| | |
| 6/12/2019 12:23:34PM Page 6 of 6 Analysis Report for 12-Jun-19-10015 L1-10221C-FSGS-002SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -2.98E-02 9.53E-02 3.91E-01 1004.76 18.01 -3.27E-02 2.29E-01 1274.43 34.80 3.79E-02 1.29E-01 1596.48 1.80 -3.80E-02 1.70E+00 Eu-155 45.30 1.31 5.15E+00 2.32E-01 2.78E+01 60.01 1.22 2.49E+00 2.64E+01 86.55 30.70 1.42E-01 2.32E-01 105.31 21.10 1.04E-01 2.51E-01 Ra-226 186.21 3.64 8.62E-01 1.04E+00 1.04E+00 Pa-231 27.36 10.30 8.21E-01 1.36E+00 2.42E+00 283.69 1.70 -2.88E-01 1.91E+00 300.07 2.47 -6.38E-01 1.36E+00 302.65 2.20 9.76E-02 1.53E+00 330.06 1.40 -3.92E-02 2.39E+00 U-235 143.76 10.96 -1.77E-01 6.43E-02 3.30E-01 163.33 5.08 -1.70E-01 6.41E-01 185.71 57.20 1.27E-02 6.43E-02 202.11 1.08 9.98E-01 3.29E+00 205.31 5.01 3.55E-02 6.86E-01 Am-241 59.54 35.90 2.80E-02 9.36E-01 9.36E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [78]
| |
| | |
| 6/12/2019 12:23:49PM Page 1 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10016 Sample Description : L1-10221C-FSGS-003SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.805E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:25:00AM Acquisition Started : 6/12/2019 12:08:31PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77297 Fill Height : 1804.99 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:23:40PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [79]
| |
| | |
| 6/12/2019 12:23:49PM Page 2 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.76 950 - 960 954.63 1.01E+02 13.04 2.87E+01 1.13 2 338.40 1349 - 1356 1352.68 1.07E+01 6.65 1.53E+01 0.53 3 351.89 1400 - 1415 1406.58 7.80E+01 12.76 2.80E+01 1.09 4 583.20 2326 - 2336 2330.90 1.78E+01 6.12 8.25E+00 0.71 5 609.27 2429 - 2441 2435.13 4.76E+01 9.66 1.74E+01 0.85 6 661.75 2640 - 2650 2644.88 2.30E+01 5.69 3.96E+00 0.40 7 1460.41 5828 - 5849 5839.58 1.86E+02 13.64 0.00E+00 1.48 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82
| |
| * 10.66 4.00E+00 3.41E-01 Cs-137 0.99 661.66
| |
| * 85.10 3.65E-02 9.27E-03 Tl-208 1.00 583.19
| |
| * 85.00 2.58E-02 9.04E-03 Bi-211 0.89 351.07
| |
| * 13.02 5.21E-01 9.50E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.57E-01 2.38E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.33E-01 2.82E-02 768.36 4.89 806.18 1.26 [80]
| |
| | |
| 6/12/2019 12:23:49PM Page 3 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.91E-01 3.47E-02 785.96 1.06 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 8.00E-02 5.04E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20 25.80 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [81]
| |
| | |
| 6/12/2019 12:23:49PM Page 4 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.973 4.00E+00 3.41E-01 Cs-137 0.999 3.65E-02 9.27E-03 Tl-208 1.000 2.58E-02 9.04E-03
| |
| ? Bi-211 0.898 5.21E-01 9.50E-02 Pb-212 0.997 1.57E-01 2.38E-02 Bi-214 1.000 1.33E-01 2.82E-02
| |
| ? Pb-214 1.000 1.91E-01 3.47E-02 Ac-228 1.000 8.00E-02 5.04E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [82]
| |
| | |
| 6/12/2019 12:23:49PM Page 5 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:23:40PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.58E-02 4.66E-02 4.66E-02 BE-7 477.60 10.44 1.68E-01 3.40E-01 3.40E-01
| |
| + K-40 1460.82
| |
| * 10.66 4.00E+00 6.19E-02 6.19E-02 Mn-54 834.85 99.98 3.17E-03 4.38E-02 4.38E-02 Co-60 1173.23 99.85 6.93E-03 4.85E-02 4.90E-02 1332.49 99.98 9.10E-03 4.85E-02 Nb-94 702.65 99.81 -7.02E-04 3.34E-02 3.34E-02 871.09 99.89 7.69E-03 3.47E-02 Ag-108m 79.13 6.60 -1.52E-01 3.44E-02 1.03E+00 433.94 90.50 1.46E-02 3.44E-02 614.28 89.80 -2.61E-02 5.05E-02 722.94 90.80 -4.24E-02 3.83E-02 Sb-125 176.31 6.84 1.15E-01 1.03E-01 4.06E-01 380.45 1.52 -9.03E-01 1.90E+00 427.87 29.60 4.54E-02 1.03E-01 463.36 10.49 4.42E-02 3.15E-01 600.60 17.65 1.72E-03 1.92E-01 606.71 4.98 1.48E+00 1.22E+00 635.95 11.22 6.43E-02 2.58E-01 [83]
| |
| | |
| 6/12/2019 12:23:49PM Page 6 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.01E+00 1.03E-01 1.97E+00 Ba-133 79.61 2.65 -9.89E-01 6.13E-02 2.48E+00 81.00 32.90 -1.84E-01 1.64E-01 276.40 7.16 4.45E-02 4.05E-01 302.85 18.34 5.84E-02 1.58E-01 356.01 62.05 -1.36E-02 6.13E-02 383.85 8.94 -1.96E-02 3.24E-01 Cs-134 475.36 1.48 1.39E+00 4.43E-02 2.39E+00 563.25 8.34 -7.52E-01 3.75E-01 569.33 15.37 -4.59E-03 2.01E-01 604.72 97.62 -3.45E-02 5.48E-02 795.86 85.46 -3.18E-04 4.43E-02 801.95 8.69 1.37E-01 4.10E-01 1038.61 0.99 1.38E+00 3.83E+00 1167.97 1.79 -1.33E-01 2.73E+00 1365.19 3.02 3.57E-01 1.41E+00
| |
| + Cs-137 661.66
| |
| * 85.10 3.65E-02 2.10E-02 2.10E-02 Eu-152 121.78 28.67 2.30E-02 9.39E-02 1.04E-01 244.70 7.61 3.56E-01 4.20E-01 295.94 0.45 9.97E-01 8.42E+00 344.28 26.60 -1.52E-01 9.39E-02 367.79 0.86 1.13E+00 3.80E+00 411.12 2.24 -2.45E-01 1.44E+00 443.96 2.83 -3.98E-01 9.56E-01 488.68 0.42 -1.63E+00 7.13E+00 563.99 0.49 -1.18E+01 5.86E+00 586.26 0.46 5.05E+00 8.86E+00 678.62 0.47 1.76E-01 6.90E+00 688.67 0.86 -9.09E-01 3.83E+00 719.35 0.28 -5.90E+00 1.24E+01 778.90 12.96 -3.17E-02 3.11E-01 810.45 0.32 2.18E-02 9.02E+00 867.37 4.26 2.52E-01 8.35E-01 919.33 0.43 1.48E+00 9.55E+00 964.08 14.65 2.96E-02 3.18E-01 1085.87 10.24 -4.57E-02 4.55E-01 1089.74 1.73 -5.08E-01 2.75E+00 1112.07 13.69 -4.84E-02 3.30E-01 1212.95 1.43 -5.25E-01 3.86E+00 1249.94 0.19 -1.56E+01 2.40E+01 1299.14 1.63 -2.30E+00 2.70E+00 1408.01 21.07 -5.54E-02 2.14E-01 1457.64 0.50 8.34E+01 3.12E+01 1528.10 0.28 3.37E+00 1.05E+01 Eu-154 123.07 40.40 1.67E-02 7.27E-02 7.27E-02 247.93 6.89 -4.75E-02 4.20E-01 591.76 4.95 -2.46E-01 5.86E-01 692.42 1.78 -1.50E-01 1.81E+00 723.30 20.06 -1.31E-01 1.77E-01 756.80 4.52 2.07E-01 6.99E-01 873.18 12.08 3.89E-02 2.88E-01
| |
| [84]
| |
| | |
| 6/12/2019 12:23:49PM Page 7 of 7 Analysis Report for 12-Jun-19-10016 L1-10221C-FSGS-003SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -5.59E-02 7.27E-02 3.93E-01 1004.76 18.01 -7.42E-02 2.12E-01 1274.43 34.80 -2.84E-02 1.12E-01 1596.48 1.80 2.05E+00 2.93E+00 Eu-155 45.30 1.31 2.07E+00 1.56E-01 1.02E+01 60.01 1.22 7.93E-01 1.11E+01 86.55 30.70 6.60E-02 1.69E-01 105.31 21.10 4.46E-02 1.56E-01 Ra-226 186.21 3.64 7.13E-01 9.01E-01 9.01E-01 Pa-231 27.36 10.30 5.84E-01 1.16E+00 1.16E+00 283.69 1.70 2.44E-01 1.72E+00 300.07 2.47 -1.50E+00 1.24E+00 302.65 2.20 8.74E-01 1.34E+00 330.06 1.40 -3.65E-01 2.06E+00 U-235 143.76 10.96 6.12E-02 5.58E-02 2.74E-01 163.33 5.08 1.08E-01 5.38E-01 185.71 57.20 2.60E-02 5.58E-02 202.11 1.08 -7.82E-01 2.79E+00 205.31 5.01 -1.11E-01 5.90E-01 Am-241 59.54 35.90 -6.17E-02 3.74E-01 3.74E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [85]
| |
| | |
| 6/12/2019 12:23:55PM Page 1 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10017 Sample Description : L1-10221C-FSGS-004SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.640E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:30:00AM Acquisition Started : 6/12/2019 12:08:37PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77298 Fill Height : 1640.39 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:23:43PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [86]
| |
| | |
| 6/12/2019 12:23:55PM Page 2 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.68 948 - 961 955.18 5.89E+01 12.48 3.51E+01 0.88 2 295.18 1173 - 1187 1180.93 2.54E+01 9.53 2.26E+01 0.62 3 583.18 2328 - 2337 2332.05 2.79E+01 6.85 7.14E+00 0.93 4 1460.44 5833 - 5854 5842.15 1.34E+02 12.30 4.91E+00 0.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82
| |
| * 10.66 2.76E+00 2.80E-01 Tl-208 1.00 583.19
| |
| * 85.00 3.93E-02 9.94E-03 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 9.13E-02 2.07E-02 300.09 3.30 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 1.05E-01 4.00E-02 351.93 35.60 785.96 1.06
| |
| [87]
| |
| | |
| 6/12/2019 12:23:55PM Page 3 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.978 2.76E+00 2.80E-01 Tl-208 1.000 3.93E-02 9.94E-03 Pb-212 1.000 9.13E-02 2.07E-02 Pb-214 1.000 1.05E-01 4.00E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [88]
| |
| | |
| 6/12/2019 12:23:55PM Page 4 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:23:43PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 4.18E-02 4.39E-02 4.39E-02 BE-7 477.60 10.44 -1.71E-01 3.02E-01 3.02E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.76E+00 3.49E-01 3.49E-01 Mn-54 834.85 99.98 1.18E-02 3.61E-02 3.61E-02 Co-60 1173.23 99.85 6.14E-03 4.28E-02 4.28E-02 1332.49 99.98 5.70E-03 4.52E-02 Nb-94 702.65 99.81 -3.21E-02 2.56E-02 3.64E-02 871.09 99.89 -1.36E-02 2.56E-02 Ag-108m 79.13 6.60 -8.44E-01 2.98E-02 1.12E+00 433.94 90.50 -1.95E-02 2.98E-02 614.28 89.80 -2.96E-04 4.69E-02 722.94 90.80 -2.13E-02 3.77E-02 Sb-125 176.31 6.84 -5.34E-02 9.48E-02 3.64E-01 380.45 1.52 2.13E+00 2.00E+00 427.87 29.60 -6.52E-02 9.48E-02 463.36 10.49 -4.03E-03 2.05E-01 600.60 17.65 9.27E-02 1.83E-01 606.71 4.98 -1.26E-01 8.84E-01 635.95 11.22 2.38E-01 2.81E-01 [89]
| |
| | |
| 6/12/2019 12:23:55PM Page 5 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.49E+00 9.48E-02 1.53E+00 Ba-133 79.61 2.65 1.02E+00 5.34E-02 2.80E+00 81.00 32.90 -1.42E-01 1.94E-01 276.40 7.16 1.73E-01 3.96E-01 302.85 18.34 -5.72E-03 1.50E-01 356.01 62.05 -9.40E-03 5.34E-02 383.85 8.94 -1.31E-01 2.92E-01 Cs-134 475.36 1.48 1.40E+00 3.89E-02 2.33E+00 563.25 8.34 -3.44E-01 3.10E-01 569.33 15.37 -2.64E-02 1.95E-01 604.72 97.62 -2.97E-03 4.27E-02 795.86 85.46 5.33E-03 3.89E-02 801.95 8.69 3.34E-02 3.54E-01 1038.61 0.99 -2.13E+00 3.05E+00 1167.97 1.79 -1.04E+00 2.44E+00 1365.19 3.02 -7.37E-01 1.14E+00 Cs-137 661.66 85.10 -8.75E-03 4.11E-02 4.11E-02 Eu-152 121.78 28.67 1.36E-03 1.02E-01 1.02E-01 244.70 7.61 -6.38E-02 3.49E-01 295.94 0.45 6.31E+00 7.80E+00 344.28 26.60 -2.52E-02 1.05E-01 367.79 0.86 1.93E+00 3.28E+00 411.12 2.24 -1.06E-02 1.22E+00 443.96 2.83 -4.45E-02 9.83E-01 488.68 0.42 -1.90E-01 7.40E+00 563.99 0.49 -5.60E+00 5.27E+00 586.26 0.46 4.63E+00 1.01E+01 678.62 0.47 5.61E+00 6.82E+00 688.67 0.86 -1.54E+00 3.03E+00 719.35 0.28 -4.80E+00 1.30E+01 778.90 12.96 -2.83E-01 2.89E-01 810.45 0.32 -2.76E+00 7.60E+00 867.37 4.26 -7.61E-02 7.58E-01 919.33 0.43 -1.58E+01 8.54E+00 964.08 14.65 6.57E-03 3.41E-01 1085.87 10.24 -3.10E-01 3.03E-01 1089.74 1.73 1.46E+00 2.17E+00 1112.07 13.69 -1.66E-02 2.60E-01 1212.95 1.43 -1.75E-01 2.98E+00 1249.94 0.19 1.12E+01 2.35E+01 1299.14 1.63 -1.81E+00 2.50E+00 1408.01 21.07 -2.57E-02 1.58E-01 1457.64 0.50 6.39E+01 2.65E+01 1528.10 0.28 4.02E+00 1.09E+01 Eu-154 123.07 40.40 -2.39E-02 7.01E-02 7.01E-02 247.93 6.89 -6.20E-02 3.36E-01 591.76 4.95 2.32E-01 6.45E-01 692.42 1.78 2.17E-01 1.95E+00 723.30 20.06 -1.97E-02 1.71E-01 756.80 4.52 -1.10E-01 7.64E-01 873.18 12.08 -2.37E-01 1.75E-01
| |
| [90]
| |
| | |
| 6/12/2019 12:23:55PM Page 6 of 6 Analysis Report for 12-Jun-19-10017 L1-10221C-FSGS-004SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.32E-01 7.01E-02 3.48E-01 1004.76 18.01 -8.99E-02 2.09E-01 1274.43 34.80 -7.15E-02 1.23E-01 1596.48 1.80 -1.08E+00 1.91E+00 Eu-155 45.30 1.31 -1.43E+00 1.68E-01 1.55E+01 60.01 1.22 1.03E+00 1.83E+01 86.55 30.70 1.17E-02 1.68E-01 105.31 21.10 2.10E-02 1.77E-01 Ra-226 186.21 3.64 -7.89E-02 8.17E-01 8.17E-01 Pa-231 27.36 10.30 9.92E-01 1.11E+00 1.74E+00 283.69 1.70 5.45E-02 1.53E+00 300.07 2.47 -3.38E-01 1.11E+00 302.65 2.20 3.74E-01 1.26E+00 330.06 1.40 -4.46E-01 1.96E+00 U-235 143.76 10.96 -1.70E-01 5.27E-02 2.69E-01 163.33 5.08 -2.42E-01 4.87E-01 185.71 57.20 1.50E-02 5.27E-02 202.11 1.08 1.82E+00 2.71E+00 205.31 5.01 6.08E-02 5.74E-01 Am-241 59.54 35.90 3.42E-01 6.49E-01 6.49E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [91]
| |
| | |
| 6/12/2019 12:47:23PM Page 1 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10018 Sample Description : L1-10221C-FSGS-005SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.690E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:35:00AM Acquisition Started : 6/12/2019 12:32:11PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77299 Fill Height : 1689.99 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:47:14PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [92]
| |
| | |
| 6/12/2019 12:47:23PM Page 2 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.46 472 - 481 477.10 6.79E+01 16.71 8.91E+01 1.23 2 295.25 588 - 595 590.56 3.67E+01 10.92 3.93E+01 1.10 3 351.92 699 - 708 703.79 4.71E+01 11.63 3.89E+01 1.49 4 583.24 1162 - 1170 1166.09 3.13E+01 8.71 2.08E+01 1.24 5 609.25 1213 - 1223 1218.08 5.85E+01 8.92 8.45E+00 1.59 6 661.65 1319 - 1328 1322.83 5.45E+01 9.10 1.25E+01 1.58 7 1460.89 2916 - 2928 2921.84 1.64E+02 13.63 8.24E+00 2.05 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 3.00E+00 2.82E-01 Cs-137 1.00 661.66
| |
| * 85.10 7.47E-02 1.33E-02 Tl-208 1.00 583.19
| |
| * 85.00 3.95E-02 1.13E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 9.36E-02 2.43E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.42E-01 2.33E-02 768.36 4.89 806.18 1.26 934.06 3.11 [93]
| |
| | |
| 6/12/2019 12:47:23PM Page 3 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 1.35E-01 4.16E-02 351.93
| |
| * 35.60 1.01E-01 2.63E-02 785.96 1.06
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 3.00E+00 2.82E-01 Cs-137 1.000 7.47E-02 1.33E-02 Tl-208 1.000 3.95E-02 1.13E-02 X Bi-211 0.890 Pb-212 0.996 9.36E-02 2.43E-02 Bi-214 1.000 1.42E-01 2.33E-02 Pb-214 1.000 1.11E-01 2.22E-02
| |
| [94]
| |
| | |
| 6/12/2019 12:47:23PM Page 4 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [95]
| |
| | |
| 6/12/2019 12:47:23PM Page 5 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:47:14PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.27E-02 4.81E-02 4.81E-02 BE-7 477.60 10.44 1.13E-01 3.17E-01 3.17E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.00E+00 3.43E-01 3.43E-01 Mn-54 834.85 99.98 1.49E-02 3.96E-02 3.96E-02 Co-60 1173.23 99.85 4.16E-02 4.24E-02 5.72E-02 1332.49 99.98 1.60E-02 4.24E-02 Nb-94 702.65 99.81 -2.81E-03 3.20E-02 3.20E-02 871.09 99.89 4.88E-03 3.54E-02 Ag-108m 79.13 6.60 3.22E-01 2.97E-02 9.38E-01 433.94 90.50 -2.00E-03 2.97E-02 614.28 89.80 -5.11E-03 4.51E-02 722.94 90.80 1.30E-02 3.08E-02 Sb-125 176.31 6.84 -2.98E-01 9.48E-02 4.29E-01 380.45 1.52 6.67E-01 1.85E+00 427.87 29.60 1.46E-02 9.48E-02 463.36 10.49 1.20E-01 2.71E-01 600.60 17.65 5.20E-02 1.78E-01 606.71 4.98 -2.00E-01 9.77E-01 635.95 11.22 1.47E-01 2.91E-01 [96]
| |
| | |
| 6/12/2019 12:47:23PM Page 6 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 2.08E-01 9.48E-02 1.67E+00 Ba-133 79.61 2.65 5.30E-01 5.90E-02 2.24E+00 81.00 32.90 -7.30E-02 1.56E-01 276.40 7.16 -1.46E-01 3.65E-01 302.85 18.34 7.13E-02 1.65E-01 356.01 62.05 -1.56E-02 5.90E-02 383.85 8.94 -4.23E-02 3.02E-01 Cs-134 475.36 1.48 7.20E-01 3.90E-02 2.32E+00 563.25 8.34 -4.13E-02 3.94E-01 569.33 15.37 5.69E-02 2.07E-01 604.72 97.62 -1.47E-02 4.19E-02 795.86 85.46 4.82E-03 3.90E-02 801.95 8.69 -1.20E-01 3.26E-01 1038.61 0.99 1.81E+00 4.08E+00 1167.97 1.79 -2.05E+00 2.61E+00 1365.19 3.02 -3.64E-01 1.11E+00
| |
| + Cs-137 661.66
| |
| * 85.10 7.47E-02 2.87E-02 2.87E-02 Eu-152 121.78 28.67 1.95E-02 9.93E-02 9.93E-02 244.70 7.61 -2.04E-02 4.00E-01 295.94 0.45 6.48E+00 7.82E+00 344.28 26.60 -1.49E-02 1.02E-01 367.79 0.86 -3.99E-01 2.90E+00 411.12 2.24 1.84E-01 1.39E+00 443.96 2.83 2.27E-01 9.37E-01 488.68 0.42 1.76E+00 7.02E+00 563.99 0.49 6.82E-01 6.77E+00 586.26 0.46 -3.47E+00 1.01E+01 678.62 0.47 1.07E+00 6.24E+00 688.67 0.86 4.78E-01 3.53E+00 719.35 0.28 -5.51E-01 8.90E+00 778.90 12.96 2.25E-02 2.73E-01 810.45 0.32 5.59E+00 1.07E+01 867.37 4.26 -1.83E-01 7.19E-01 919.33 0.43 -5.21E+00 8.21E+00 964.08 14.65 8.15E-02 2.82E-01 1085.87 10.24 -4.06E-02 3.89E-01 1089.74 1.73 2.54E-01 2.31E+00 1112.07 13.69 -7.28E-02 2.62E-01 1212.95 1.43 -6.28E-01 3.12E+00 1249.94 0.19 -2.18E+00 2.21E+01 1299.14 1.63 -2.26E+00 1.72E+00 1408.01 21.07 -8.38E-02 1.40E-01 1457.64 0.50 -2.16E+00 2.61E+01 1528.10 0.28 -2.35E+00 1.11E+01 Eu-154 123.07 40.40 -1.68E-02 6.77E-02 6.77E-02 247.93 6.89 -1.27E-01 3.79E-01 591.76 4.95 1.75E-01 7.02E-01 692.42 1.78 -1.41E-01 1.71E+00 723.30 20.06 5.88E-02 1.39E-01 756.80 4.52 -2.31E-02 6.99E-01 873.18 12.08 9.34E-02 3.10E-01
| |
| [97]
| |
| | |
| 6/12/2019 12:47:23PM Page 7 of 7 Analysis Report for 12-Jun-19-10018 L1-10221C-FSGS-005SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.11E-01 6.77E-02 3.75E-01 1004.76 18.01 -1.04E-01 1.77E-01 1274.43 34.80 4.35E-02 1.16E-01 1596.48 1.80 -1.67E+00 1.91E+00 Eu-155 45.30 1.31 -2.99E+00 1.57E-01 9.40E+00 60.01 1.22 1.92E+00 1.05E+01 86.55 30.70 7.49E-02 1.57E-01 105.31 21.10 2.88E-02 1.67E-01 Ra-226 186.21 3.64 -1.05E-01 8.17E-01 8.17E-01 Pa-231 27.36 10.30 3.10E-01 9.45E-01 9.45E-01 283.69 1.70 -4.84E-01 1.50E+00 300.07 2.47 2.26E-01 1.26E+00 302.65 2.20 5.94E-01 1.38E+00 330.06 1.40 5.76E-01 2.10E+00 U-235 143.76 10.96 -4.45E-02 5.33E-02 2.32E-01 163.33 5.08 9.39E-03 5.87E-01 185.71 57.20 9.96E-03 5.33E-02 202.11 1.08 1.23E+00 2.83E+00 205.31 5.01 -1.36E-01 5.92E-01 Am-241 59.54 35.90 5.14E-02 3.60E-01 3.60E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [98]
| |
| | |
| 6/12/2019 12:47:30PM Page 1 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10019 Sample Description : L1-10221C-FSGS-006SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.723E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:40:00AM Acquisition Started : 6/12/2019 12:32:18PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.2 seconds Dead Time : 0.14 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77300 Fill Height : 1722.60 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:47:21PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [99]
| |
| | |
| 6/12/2019 12:47:30PM Page 2 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.64 946 - 960 954.67 1.36E+02 17.49 5.93E+01 0.78 2 295.16 1176 - 1185 1180.53 2.17E+01 8.49 2.23E+01 1.03 3 352.08 1401 - 1412 1408.05 3.55E+01 10.70 3.15E+01 1.02 4 583.27 2327 - 2337 2332.30 3.30E+01 7.67 1.00E+01 0.37 5 661.63 2641 - 2651 2645.62 2.94E+01 7.56 1.16E+01 0.59 6 911.33 3638 - 3650 3644.26 3.28E+01 7.38 8.19E+00 1.03 7 1460.90 5833 - 5854 5843.44 2.32E+02 15.88 5.50E+00 1.88 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 5.59E+00 4.54E-01 Cs-137 1.00 661.66
| |
| * 85.10 5.20E-02 1.38E-02 Tl-208 0.99 583.19
| |
| * 85.00 5.37E-02 1.29E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 2.38E-01 3.62E-02 300.09 3.30 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 1.01E-01 4.04E-02 351.93
| |
| * 35.60 9.72E-02 3.03E-02 785.96 1.06 [100]
| |
| | |
| 6/12/2019 12:47:30PM Page 3 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 2.38E-01 5.44E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 5.59E+00 4.54E-01 Cs-137 1.000 5.20E-02 1.38E-02 Tl-208 0.999 5.37E-02 1.29E-02 Pb-212 1.000 2.38E-01 3.62E-02 Pb-214 0.998 9.86E-02 2.43E-02 Ac-228 0.999 2.38E-01 5.44E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [101]
| |
| | |
| 6/12/2019 12:47:30PM Page 4 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:47:21PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 7.44E-02 6.17E-02 6.17E-02 BE-7 477.60 10.44 1.84E-01 4.84E-01 4.84E-01
| |
| + K-40 1460.82
| |
| * 10.66 5.59E+00 4.42E-01 4.42E-01 Mn-54 834.85 99.98 -3.28E-03 4.10E-02 4.10E-02 Co-60 1173.23 99.85 2.05E-02 6.05E-02 6.05E-02 1332.49 99.98 2.46E-02 6.22E-02 Nb-94 702.65 99.81 -1.87E-02 4.41E-02 4.91E-02 871.09 99.89 3.62E-02 4.41E-02 Ag-108m 79.13 6.60 1.22E+00 3.85E-02 1.75E+00 433.94 90.50 3.37E-03 3.85E-02 614.28 89.80 3.96E-02 6.49E-02 722.94 90.80 -1.30E-02 5.05E-02 Sb-125 176.31 6.84 1.40E-01 1.27E-01 5.48E-01 380.45 1.52 2.28E+00 2.50E+00 427.87 29.60 -4.35E-02 1.27E-01 463.36 10.49 6.28E-02 3.95E-01 600.60 17.65 -3.92E-02 2.30E-01 606.71 4.98 1.03E+00 1.24E+00 635.95 11.22 -8.65E-02 3.39E-01 [102]
| |
| | |
| 6/12/2019 12:47:30PM Page 5 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -2.34E+00 1.27E-01 2.28E+00 Ba-133 79.61 2.65 1.10E+00 7.75E-02 4.12E+00 81.00 32.90 -1.64E-01 2.81E-01 276.40 7.16 2.25E-01 5.11E-01 302.85 18.34 -1.98E-03 2.10E-01 356.01 62.05 -6.73E-02 7.75E-02 383.85 8.94 2.45E-01 4.27E-01 Cs-134 475.36 1.48 3.79E+00 5.59E-02 3.36E+00 563.25 8.34 2.07E-01 5.13E-01 569.33 15.37 -1.23E-01 2.66E-01 604.72 97.62 -1.67E-02 5.59E-02 795.86 85.46 1.30E-03 5.82E-02 801.95 8.69 1.64E-01 5.58E-01 1038.61 0.99 2.89E+00 5.64E+00 1167.97 1.79 1.54E+00 3.64E+00 1365.19 3.02 -6.55E-01 1.52E+00
| |
| + Cs-137 661.66
| |
| * 85.10 5.20E-02 3.68E-02 3.68E-02 Eu-152 121.78 28.67 -5.23E-03 1.43E-01 1.54E-01 244.70 7.61 2.54E-01 5.42E-01 295.94 0.45 5.98E-01 9.01E+00 344.28 26.60 7.59E-02 1.43E-01 367.79 0.86 2.61E+00 3.97E+00 411.12 2.24 -9.13E-02 1.81E+00 443.96 2.83 1.56E-03 1.33E+00 488.68 0.42 2.74E+00 9.69E+00 563.99 0.49 2.08E+00 8.72E+00 586.26 0.46 4.17E+00 1.20E+01 678.62 0.47 -3.00E+00 7.90E+00 688.67 0.86 3.72E+00 5.63E+00 719.35 0.28 -2.93E+00 1.51E+01 778.90 12.96 1.07E-02 2.94E-01 810.45 0.32 2.69E-01 1.34E+01 867.37 4.26 -1.92E+00 9.35E-01 919.33 0.43 -1.19E+01 1.02E+01 964.08 14.65 -2.41E-01 3.43E-01 1085.87 10.24 -2.51E-01 4.52E-01 1089.74 1.73 -2.00E-01 2.53E+00 1112.07 13.69 1.39E-01 4.61E-01 1212.95 1.43 -3.03E+00 4.25E+00 1249.94 0.19 -1.01E+01 2.90E+01 1299.14 1.63 -2.07E-01 3.29E+00 1408.01 21.07 1.19E-01 2.14E-01 1457.64 0.50 1.16E+02 3.97E+01 1528.10 0.28 -2.36E+00 1.38E+01 Eu-154 123.07 40.40 -2.91E-02 1.09E-01 1.09E-01 247.93 6.89 1.90E-01 5.13E-01 591.76 4.95 7.76E-02 8.47E-01 692.42 1.78 -2.77E-01 2.66E+00 723.30 20.06 1.01E-01 2.29E-01 756.80 4.52 -1.73E-01 9.97E-01 873.18 12.08 -1.46E-01 3.57E-01
| |
| [103]
| |
| | |
| 6/12/2019 12:47:30PM Page 6 of 6 Analysis Report for 12-Jun-19-10019 L1-10221C-FSGS-006SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.62E-01 1.09E-01 4.61E-01 1004.76 18.01 1.91E-01 2.81E-01 1274.43 34.80 -1.16E-01 1.67E-01 1596.48 1.80 -7.29E-01 2.65E+00 Eu-155 45.30 1.31 -3.61E+00 2.54E-01 2.82E+01 60.01 1.22 2.22E+01 3.04E+01 86.55 30.70 -1.64E-01 2.54E-01 105.31 21.10 -1.41E-01 2.54E-01 Ra-226 186.21 3.64 2.51E-01 1.04E+00 1.04E+00 Pa-231 27.36 10.30 6.10E-01 1.55E+00 3.17E+00 283.69 1.70 1.17E+00 2.18E+00 300.07 2.47 -1.10E+00 1.55E+00 302.65 2.20 -3.01E-01 1.75E+00 330.06 1.40 -1.05E+00 2.76E+00 U-235 143.76 10.96 1.84E-01 6.73E-02 3.77E-01 163.33 5.08 -1.69E-02 7.78E-01 185.71 57.20 3.23E-02 6.73E-02 202.11 1.08 1.04E+00 3.31E+00 205.31 5.01 -4.01E-01 7.25E-01 Am-241 59.54 35.90 7.36E-01 1.10E+00 1.10E+00
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [104]
| |
| | |
| 6/12/2019 12:47:53PM Page 1 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10020 Sample Description : L1-10221C-FSGS-007SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.679E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:45:00AM Acquisition Started : 6/12/2019 12:32:25PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77301 Fill Height : 1678.91 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:47:44PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [105]
| |
| | |
| 6/12/2019 12:47:53PM Page 2 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.72 949 - 962 954.45 1.12E+02 15.33 4.40E+01 1.15 2 338.47 1349 - 1358 1352.95 2.85E+01 9.07 2.35E+01 0.82 3 351.92 1402 - 1412 1406.69 3.30E+01 9.51 2.40E+01 0.79 4 609.39 2429 - 2442 2435.59 4.27E+01 8.43 1.03E+01 0.30 5 661.53 2636 - 2650 2644.02 5.84E+01 8.64 5.64E+00 0.63 6 964.40 3851 - 3860 3855.01 9.00E+00 4.52 5.00E+00 0.52 7 1460.33 5829 - 5850 5839.24 1.95E+02 14.30 2.53E+00 1.80 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.96 1460.82
| |
| * 10.66 4.28E+00 3.64E-01 Cs-137 0.99 661.66
| |
| * 85.10 9.37E-02 1.50E-02 Bi-211 0.89 351.07
| |
| * 13.02 2.23E-01 6.68E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.75E-01 2.78E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.21E-01 2.50E-02 768.36 4.89 806.18 1.26 934.06 3.11 [106]
| |
| | |
| 6/12/2019 12:47:53PM Page 3 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 8.15E-02 2.44E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 2.16E-01 7.11E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20 25.80 964.77
| |
| * 4.99 3.18E-01 1.60E-01 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [107]
| |
| | |
| 6/12/2019 12:47:53PM Page 4 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.961 4.28E+00 3.64E-01 Cs-137 0.997 9.37E-02 1.50E-02 X Eu-152 0.593
| |
| ? Bi-211 0.891 2.23E-01 6.68E-02 Pb-212 0.999 1.75E-01 2.78E-02 Bi-214 1.000 1.21E-01 2.50E-02
| |
| ? Pb-214 1.000 8.15E-02 2.44E-02 Ac-228 0.998 2.33E-01 6.50E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [108]
| |
| | |
| 6/12/2019 12:47:53PM Page 5 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:47:44PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 4.79E-02 4.76E-02 4.76E-02 BE-7 477.60 10.44 1.68E-01 4.38E-01 4.38E-01
| |
| + K-40 1460.82
| |
| * 10.66 4.28E+00 2.85E-01 2.85E-01 Mn-54 834.85 99.98 -1.30E-02 3.81E-02 3.81E-02 Co-60 1173.23 99.85 3.26E-02 5.30E-02 6.18E-02 1332.49 99.98 5.17E-03 5.30E-02 Nb-94 702.65 99.81 -2.20E-03 3.69E-02 3.69E-02 871.09 99.89 -4.11E-03 3.82E-02 Ag-108m 79.13 6.60 -2.03E-01 3.83E-02 1.07E+00 433.94 90.50 8.71E-03 3.83E-02 614.28 89.80 -4.85E-02 5.22E-02 722.94 90.80 -1.62E-02 4.36E-02 Sb-125 176.31 6.84 2.48E-02 1.14E-01 3.76E-01 380.45 1.52 6.15E-02 1.90E+00 427.87 29.60 3.01E-03 1.14E-01 463.36 10.49 2.31E-01 3.86E-01 600.60 17.65 -5.01E-02 1.68E-01 606.71 4.98 1.40E+00 1.07E+00 635.95 11.22 8.09E-02 3.51E-01 [109]
| |
| | |
| 6/12/2019 12:47:53PM Page 6 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.46E+00 1.14E-01 1.83E+00 Ba-133 79.61 2.65 7.20E-02 5.55E-02 2.62E+00 81.00 32.90 -2.06E-01 1.69E-01 276.40 7.16 7.06E-02 3.99E-01 302.85 18.34 9.31E-02 1.75E-01 356.01 62.05 -2.29E-02 5.55E-02 383.85 8.94 0.00E+00 3.19E-01 Cs-134 475.36 1.48 1.64E+00 4.12E-02 3.06E+00 563.25 8.34 -3.56E-01 4.65E-01 569.33 15.37 -4.34E-02 1.86E-01 604.72 97.62 -3.49E-02 4.12E-02 795.86 85.46 -9.05E-04 4.40E-02 801.95 8.69 6.58E-02 4.05E-01 1038.61 0.99 1.68E+00 4.01E+00 1167.97 1.79 -7.59E-01 3.25E+00 1365.19 3.02 -1.07E-01 1.58E+00
| |
| + Cs-137 661.66
| |
| * 85.10 9.37E-02 2.66E-02 2.66E-02 Eu-152 121.78 28.67 -5.50E-02 9.32E-02 9.32E-02 244.70 7.61 -2.56E-02 3.99E-01 295.94 0.45 2.88E-01 7.92E+00 344.28 26.60 -2.57E-03 1.22E-01 367.79 0.86 -1.51E+00 3.03E+00 411.12 2.24 5.01E-01 1.54E+00 443.96 2.83 2.54E-01 1.13E+00 488.68 0.42 -4.03E+00 7.09E+00 563.99 0.49 -1.52E+01 6.58E+00 586.26 0.46 7.14E+00 1.03E+01 678.62 0.47 2.72E+00 7.00E+00 688.67 0.86 2.71E-01 3.70E+00 719.35 0.28 8.65E+00 1.58E+01 778.90 12.96 8.89E-02 2.29E-01 810.45 0.32 -1.26E+01 9.50E+00 867.37 4.26 -2.60E-01 9.14E-01 919.33 0.43 -2.99E+00 8.55E+00 964.08
| |
| * 14.65 1.08E-01 1.73E-01 1085.87 10.24 9.76E-02 4.21E-01 1089.74 1.73 2.97E-01 2.96E+00 1112.07 13.69 5.52E-02 3.58E-01 1212.95 1.43 -1.66E+00 3.85E+00 1249.94 0.19 6.35E+00 2.56E+01 1299.14 1.63 6.75E-01 2.91E+00 1408.01 21.07 -4.17E-02 2.10E-01 1457.64 0.50 9.26E+01 3.27E+01 1528.10 0.28 -9.63E+00 8.27E+00 Eu-154 123.07 40.40 -5.68E-03 7.04E-02 7.04E-02 247.93 6.89 -6.01E-02 4.18E-01 591.76 4.95 -3.54E-02 6.99E-01 692.42 1.78 -1.64E-01 1.80E+00 723.30 20.06 1.60E-03 1.98E-01 756.80 4.52 -4.58E-01 8.39E-01 873.18 12.08 1.19E-01 3.31E-01
| |
| [110]
| |
| | |
| 6/12/2019 12:47:53PM Page 7 of 7 Analysis Report for 12-Jun-19-10020 L1-10221C-FSGS-007SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.51E-01 7.04E-02 3.68E-01 1004.76 18.01 8.81E-02 2.16E-01 1274.43 34.80 -9.92E-02 1.34E-01 1596.48 1.80 8.34E-01 2.03E+00 Eu-155 45.30 1.31 -2.53E-01 1.53E-01 9.98E+00 60.01 1.22 1.41E+00 1.08E+01 86.55 30.70 -7.71E-02 1.53E-01 105.31 21.10 -2.22E-02 1.57E-01 Ra-226 186.21 3.64 7.00E-01 8.05E-01 8.05E-01 Pa-231 27.36 10.30 9.39E-01 1.21E+00 1.21E+00 283.69 1.70 -6.50E-01 1.77E+00 300.07 2.47 -2.43E+00 1.25E+00 302.65 2.20 3.23E-01 1.45E+00 330.06 1.40 7.70E-01 2.25E+00 U-235 143.76 10.96 -2.94E-02 5.11E-02 2.62E-01 163.33 5.08 1.64E-01 5.57E-01 185.71 57.20 5.05E-02 5.11E-02 202.11 1.08 -1.54E+00 2.40E+00 205.31 5.01 -4.45E-01 5.11E-01 Am-241 59.54 35.90 1.58E-01 3.84E-01 3.84E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [111]
| |
| | |
| 6/12/2019 12:47:45PM Page 1 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10021 Sample Description : L1-10221C-FSGS-008SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.674E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:50:00AM Acquisition Started : 6/12/2019 12:32:33PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77302 Fill Height : 1674.19 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 12:47:36PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [112]
| |
| | |
| 6/12/2019 12:47:45PM Page 2 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 186.02 739 - 748 744.82 2.93E+01 9.62 2.77E+01 0.54 2 238.61 949 - 961 954.90 6.68E+01 14.52 5.02E+01 0.88 3 351.83 1401 - 1414 1407.32 4.07E+01 10.37 2.43E+01 0.99 4 477.44 1905 - 1914 1909.32 2.20E+01 6.72 1.00E+01 0.67 5 583.01 2326 - 2337 2331.37 3.06E+01 7.01 7.41E+00 0.66 6 609.02 2429 - 2442 2435.34 3.36E+01 8.28 1.24E+01 1.51 7 1460.53 5830 - 5853 5842.49 1.70E+02 15.16 1.47E+01 2.03 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty BE-7 0.99 477.60
| |
| * 10.44 2.24E-01 7.04E-02 K-40 0.98 1460.82
| |
| * 10.66 3.48E+00 3.45E-01 Tl-208 0.99 583.19
| |
| * 85.00 4.30E-02 1.02E-02 Bi-211 0.91 351.07
| |
| * 13.02 2.66E-01 7.12E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.03E-01 2.39E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 9.08E-02 2.30E-02 768.36 4.89 806.18 1.26 [113]
| |
| | |
| 6/12/2019 12:47:45PM Page 3 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 9.74E-02 2.60E-02 785.96 1.06 Ra-226 0.99 186.21
| |
| * 3.64 4.85E-01 1.64E-01 U-235 0.98 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 3.09E-02 1.04E-02 202.11 1.08 205.31 5.01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| BE-7 0.995 2.24E-01 7.04E-02 K-40 0.986 3.48E+00 3.45E-01 [114]
| |
| | |
| 6/12/2019 12:47:45PM Page 4 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| Tl-208 0.995 4.30E-02 1.02E-02
| |
| ? Bi-211 0.912 2.66E-01 7.12E-02 Pb-212 1.000 1.03E-01 2.39E-02 Bi-214 0.994 9.08E-02 2.30E-02
| |
| ? Pb-214 0.999 9.74E-02 2.60E-02
| |
| ? Ra-226 0.994 4.85E-01 1.64E-01
| |
| ? U-235 0.989 3.09E-02 1.04E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [115]
| |
| | |
| 6/12/2019 12:47:45PM Page 5 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 12:47:36PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.25E-02 4.85E-02 4.85E-02
| |
| + BE-7 477.60
| |
| * 10.44 2.24E-01 1.96E-01 1.96E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.48E+00 5.93E-01 5.93E-01 Mn-54 834.85 99.98 2.67E-02 4.34E-02 4.34E-02 Co-60 1173.23 99.85 1.02E-02 4.37E-02 4.57E-02 1332.49 99.98 4.76E-04 4.37E-02 Nb-94 702.65 99.81 5.94E-03 3.28E-02 3.28E-02 871.09 99.89 3.09E-02 4.72E-02 Ag-108m 79.13 6.60 5.45E-01 2.81E-02 1.30E+00 433.94 90.50 -6.79E-03 2.81E-02 614.28 89.80 -2.49E-02 5.50E-02 722.94 90.80 3.86E-02 5.30E-02 Sb-125 176.31 6.84 -1.25E-02 1.03E-01 4.28E-01 380.45 1.52 -2.63E-01 1.99E+00 427.87 29.60 4.93E-02 1.03E-01 463.36 10.49 1.42E-01 3.03E-01 600.60 17.65 1.07E-01 2.18E-01 606.71 4.98 1.22E+00 1.06E+00 635.95 11.22 -2.13E-01 3.38E-01 [116]
| |
| | |
| 6/12/2019 12:47:45PM Page 6 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 6.30E-01 1.03E-01 1.48E+00 Ba-133 79.61 2.65 1.24E+00 6.19E-02 3.07E+00 81.00 32.90 -3.64E-01 2.00E-01 276.40 7.16 3.95E-01 4.24E-01 302.85 18.34 5.74E-02 1.63E-01 356.01 62.05 -3.42E-02 6.19E-02 383.85 8.94 1.68E-01 3.66E-01 Cs-134 475.36 1.48 1.39E+00 4.51E-02 2.68E+00 563.25 8.34 -9.81E-02 4.32E-01 569.33 15.37 -3.87E-02 2.13E-01 604.72 97.62 -4.66E-03 5.13E-02 795.86 85.46 1.12E-02 4.51E-02 801.95 8.69 1.73E-01 4.29E-01 1038.61 0.99 1.39E+00 4.28E+00 1167.97 1.79 1.92E+00 2.81E+00 1365.19 3.02 -4.21E-01 1.43E+00 Cs-137 661.66 85.10 -4.65E-03 4.44E-02 4.44E-02 Eu-152 121.78 28.67 -8.18E-02 1.06E-01 1.11E-01 244.70 7.61 2.31E-01 4.14E-01 295.94 0.45 8.08E-01 8.11E+00 344.28 26.60 -1.01E-01 1.06E-01 367.79 0.86 6.42E-01 3.31E+00 411.12 2.24 -4.85E-01 1.29E+00 443.96 2.83 -4.25E-01 1.06E+00 488.68 0.42 4.84E+00 7.82E+00 563.99 0.49 3.67E+00 7.53E+00 586.26 0.46 5.87E+00 9.76E+00 678.62 0.47 2.79E+00 5.04E+00 688.67 0.86 -1.14E+00 3.93E+00 719.35 0.28 -5.29E+00 1.41E+01 778.90 12.96 -2.21E-01 2.45E-01 810.45 0.32 8.75E+00 1.10E+01 867.37 4.26 7.84E-02 1.09E+00 919.33 0.43 -1.94E+00 1.04E+01 964.08 14.65 1.28E-01 3.40E-01 1085.87 10.24 -1.61E-01 3.95E-01 1089.74 1.73 1.55E+00 2.63E+00 1112.07 13.69 2.39E-01 3.08E-01 1212.95 1.43 -2.04E+00 3.27E+00 1249.94 0.19 4.54E+00 2.78E+01 1299.14 1.63 1.70E+00 3.00E+00 1408.01 21.07 8.33E-02 2.16E-01 1457.64 0.50 8.35E+01 3.01E+01 1528.10 0.28 -4.30E+00 9.97E+00 Eu-154 123.07 40.40 1.07E-02 7.92E-02 7.92E-02 247.93 6.89 -1.72E-01 4.16E-01 591.76 4.95 1.58E-01 6.77E-01 692.42 1.78 6.36E-01 2.05E+00 723.30 20.06 1.61E-01 2.42E-01 756.80 4.52 7.82E-02 8.55E-01 873.18 12.08 2.30E-01 4.01E-01
| |
| [117]
| |
| | |
| 6/12/2019 12:47:45PM Page 7 of 7 Analysis Report for 12-Jun-19-10021 L1-10221C-FSGS-008SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 2.95E-02 7.92E-02 3.66E-01 1004.76 18.01 1.04E-01 1.78E-01 1274.43 34.80 -6.88E-02 1.03E-01 1596.48 1.80 -7.13E-01 1.90E+00 Eu-155 45.30 1.31 5.11E+00 1.75E-01 1.74E+01 60.01 1.22 -1.65E+01 1.69E+01 86.55 30.70 9.70E-02 1.95E-01 105.31 21.10 -9.10E-02 1.75E-01
| |
| + Ra-226 186.21
| |
| * 3.64 4.85E-01 4.94E-01 4.94E-01 Pa-231 27.36 10.30 9.15E-01 1.26E+00 1.78E+00 283.69 1.70 -2.55E-01 1.65E+00 300.07 2.47 -1.29E+00 1.26E+00 302.65 2.20 8.46E-01 1.36E+00 330.06 1.40 -8.48E-01 2.23E+00
| |
| + U-235 143.76 10.96 -1.34E-01 3.14E-02 2.68E-01 163.33 5.08 -1.06E-01 6.20E-01 185.71
| |
| * 57.20 3.09E-02 3.14E-02 202.11 1.08 -1.53E+00 2.67E+00 205.31 5.01 1.20E-02 6.05E-01 Am-241 59.54 35.90 -3.86E-01 5.98E-01 5.98E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [118]
| |
| | |
| 6/12/2019 1:12:57PM Page 1 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10022 Sample Description : L1-10221C-FSGS-009SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.767E+03 grams Facility : Default Sample Taken On : 6/11/2019 8:55:00AM Acquisition Started : 6/12/2019 12:57:45PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77303 Fill Height : 1766.91 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:12:48PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [119]
| |
| | |
| 6/12/2019 1:12:57PM Page 2 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.67 473 - 481 477.52 1.33E+02 18.79 9.87E+01 1.21 2 295.39 587 - 593 590.84 4.59E+01 10.20 3.01E+01 1.37 3 338.18 673 - 680 676.33 3.24E+01 9.85 3.16E+01 1.27 4 351.95 698 - 708 703.85 7.71E+01 12.84 3.69E+01 0.85 5 583.11 1160 - 1171 1165.82 7.00E+01 10.00 1.20E+01 0.78 6 609.43 1212 - 1222 1218.45 5.25E+01 9.82 1.85E+01 1.27 7 911.15 1818 - 1828 1821.74 3.53E+01 8.07 1.17E+01 1.54 8 1460.89 2914 - 2928 2921.83 2.59E+02 16.43 3.75E+00 1.77 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 4.70E+00 3.61E-01 Tl-208 0.99 583.19
| |
| * 85.00 8.77E-02 1.36E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.83E-01 2.97E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.27E-01 2.48E-02 768.36 4.89 806.18 1.26 934.06 3.11 [120]
| |
| | |
| 6/12/2019 1:12:57PM Page 3 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 1.68E-01 3.97E-02 351.93
| |
| * 35.60 1.65E-01 3.05E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 2.13E-01 6.70E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.95E-01 4.53E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [121]
| |
| | |
| 6/12/2019 1:12:57PM Page 4 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 4.70E+00 3.61E-01 Tl-208 0.999 8.77E-02 1.36E-02 X Bi-211 0.882 Pb-212 1.000 1.83E-01 2.97E-02 Bi-214 0.999 1.27E-01 2.48E-02 Pb-214 0.999 1.66E-01 2.42E-02 Ac-228 0.999 2.00E-01 3.75E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [122]
| |
| | |
| 6/12/2019 1:12:57PM Page 5 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:12:48PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.89E-02 4.72E-02 4.72E-02 BE-7 477.60 10.44 2.97E-01 3.49E-01 3.49E-01
| |
| + K-40 1460.82
| |
| * 10.66 4.70E+00 2.54E-01 2.54E-01 Mn-54 834.85 99.98 1.44E-03 3.42E-02 3.42E-02 Co-60 1173.23 99.85 2.92E-02 3.99E-02 5.79E-02 1332.49 99.98 -5.65E-04 3.99E-02 Nb-94 702.65 99.81 -1.48E-02 2.26E-02 2.26E-02 871.09 99.89 5.18E-03 3.21E-02 Ag-108m 79.13 6.60 5.65E-01 3.43E-02 1.08E+00 433.94 90.50 -2.02E-02 3.43E-02 614.28 89.80 -2.85E-02 4.68E-02 722.94 90.80 1.14E-03 4.04E-02 Sb-125 176.31 6.84 2.42E-01 1.10E-01 4.89E-01 380.45 1.52 2.26E-01 1.86E+00 427.87 29.60 5.87E-02 1.10E-01 463.36 10.49 1.12E-01 3.00E-01 600.60 17.65 4.51E-03 1.74E-01 606.71 4.98 -8.78E-02 9.99E-01 635.95 11.22 -7.75E-02 2.75E-01 [123]
| |
| | |
| 6/12/2019 1:12:57PM Page 6 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.05E+00 1.10E-01 1.72E+00 Ba-133 79.61 2.65 8.93E-01 6.29E-02 2.55E+00 81.00 32.90 -1.29E-01 1.72E-01 276.40 7.16 1.60E-03 4.03E-01 302.85 18.34 -3.01E-02 1.52E-01 356.01 62.05 -1.26E-02 6.29E-02 383.85 8.94 -3.84E-02 2.90E-01 Cs-134 475.36 1.48 1.92E+00 4.26E-02 2.51E+00 563.25 8.34 1.07E-02 3.85E-01 569.33 15.37 1.45E-02 1.99E-01 604.72 97.62 -1.96E-03 4.26E-02 795.86 85.46 1.66E-02 4.51E-02 801.95 8.69 -3.16E-01 3.50E-01 1038.61 0.99 -3.05E-01 3.35E+00 1167.97 1.79 2.17E+00 3.16E+00 1365.19 3.02 6.71E-01 1.15E+00 Cs-137 661.66 85.10 1.61E-02 4.41E-02 4.41E-02 Eu-152 121.78 28.67 2.06E-02 1.01E-01 1.04E-01 244.70 7.61 -6.65E-02 4.42E-01 295.94 0.45 5.16E+00 7.77E+00 344.28 26.60 -1.24E-01 1.01E-01 367.79 0.86 -1.15E+00 3.13E+00 411.12 2.24 2.05E-01 1.27E+00 443.96 2.83 -9.91E-02 9.83E-01 488.68 0.42 -1.10E+00 6.28E+00 563.99 0.49 -1.24E+00 6.28E+00 586.26 0.46 -4.04E+00 1.12E+01 678.62 0.47 3.80E+00 6.92E+00 688.67 0.86 1.90E-01 3.64E+00 719.35 0.28 -4.85E-01 1.17E+01 778.90 12.96 -3.20E-01 2.66E-01 810.45 0.32 -3.18E+00 9.05E+00 867.37 4.26 1.34E-01 7.12E-01 919.33 0.43 -3.34E-01 8.65E+00 964.08 14.65 -2.20E-01 3.19E-01 1085.87 10.24 -2.07E-01 3.60E-01 1089.74 1.73 3.25E-01 2.43E+00 1112.07 13.69 -1.83E-01 3.33E-01 1212.95 1.43 1.16E+00 3.32E+00 1249.94 0.19 2.98E+00 2.42E+01 1299.14 1.63 -8.99E-01 2.41E+00 1408.01 21.07 1.07E-01 1.74E-01 1457.64 0.50 -2.07E+00 3.12E+01 1528.10 0.28 6.38E+00 1.22E+01 Eu-154 123.07 40.40 -3.19E-02 7.17E-02 7.17E-02 247.93 6.89 -1.27E-01 4.04E-01 591.76 4.95 -2.36E-01 6.14E-01 692.42 1.78 2.51E-01 1.77E+00 723.30 20.06 1.15E-02 1.86E-01 756.80 4.52 3.54E-02 5.81E-01 873.18 12.08 2.93E-02 2.52E-01
| |
| [124]
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| 6/12/2019 1:12:57PM Page 7 of 7 Analysis Report for 12-Jun-19-10022 L1-10221C-FSGS-009SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -6.92E-02 7.17E-02 3.42E-01 1004.76 18.01 6.59E-02 2.09E-01 1274.43 34.80 6.97E-02 1.33E-01 1596.48 1.80 8.94E-02 1.98E+00 Eu-155 45.30 1.31 -3.65E-01 1.56E-01 1.00E+01 60.01 1.22 4.32E+00 1.14E+01 86.55 30.70 -1.69E-02 1.56E-01 105.31 21.10 7.88E-02 1.72E-01 Ra-226 186.21 3.64 4.31E-01 9.09E-01 9.09E-01 Pa-231 27.36 10.30 1.07E+00 1.15E+00 1.21E+00 283.69 1.70 -2.38E-01 1.52E+00 300.07 2.47 -1.21E+00 1.15E+00 302.65 2.20 -2.50E-01 1.27E+00 330.06 1.40 8.31E-01 2.29E+00 U-235 143.76 10.96 -1.33E-01 5.69E-02 2.37E-01 163.33 5.08 1.02E-02 6.39E-01 185.71 57.20 9.17E-03 5.69E-02 202.11 1.08 1.39E+00 2.87E+00 205.31 5.01 -5.95E-01 5.49E-01 Am-241 59.54 35.90 9.19E-02 3.99E-01 3.99E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [125]
| |
| | |
| 6/12/2019 1:13:04PM Page 1 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10023 Sample Description : L1-10221C-FSGS-010SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.763E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:00:00AM Acquisition Started : 6/12/2019 12:57:52PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.3 seconds Dead Time : 0.15 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77304 Fill Height : 1762.74 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:12:55PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [126]
| |
| | |
| 6/12/2019 1:13:04PM Page 2 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.77 946 - 961 955.17 1.47E+02 18.90 7.04E+01 0.84 2 295.16 1175 - 1188 1180.53 4.99E+01 12.37 3.71E+01 0.66 3 352.04 1400 - 1415 1407.90 8.93E+01 11.42 1.37E+01 1.27 4 583.26 2327 - 2338 2332.27 3.52E+01 7.95 1.08E+01 1.20 5 609.33 2432 - 2445 2436.47 4.79E+01 9.76 1.71E+01 0.40 6 911.43 3638 - 3653 3644.67 4.36E+01 8.37 8.38E+00 0.33 7 1460.90 5832 - 5855 5843.42 3.07E+02 17.88 3.13E+00 1.65 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 7.37E+00 5.36E-01 Tl-208 0.99 583.19
| |
| * 85.00 5.71E-02 1.33E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 2.56E-01 3.90E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.49E-01 3.17E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 [127]
| |
| | |
| 6/12/2019 1:13:04PM Page 3 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 2.32E-01 6.05E-02 351.93
| |
| * 35.60 2.44E-01 3.68E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 3.14E-01 6.18E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [128]
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| 6/12/2019 1:13:04PM Page 4 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 7.37E+00 5.36E-01 Tl-208 0.999 5.71E-02 1.33E-02 X Bi-211 0.860 Pb-212 0.997 2.56E-01 3.90E-02 Bi-214 1.000 1.49E-01 3.17E-02 Pb-214 0.999 2.41E-01 3.14E-02 Ac-228 0.998 3.14E-01 6.18E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [129]
| |
| | |
| 6/12/2019 1:13:04PM Page 5 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:12:55PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 7.39E-02 5.67E-02 5.67E-02 BE-7 477.60 10.44 3.01E-01 4.38E-01 4.38E-01
| |
| + K-40 1460.82
| |
| * 10.66 7.37E+00 3.63E-01 3.63E-01 Mn-54 834.85 99.98 -1.15E-02 5.04E-02 5.04E-02 Co-60 1173.23 99.85 -5.67E-02 5.27E-02 6.51E-02 1332.49 99.98 -4.74E-02 5.27E-02 Nb-94 702.65 99.81 1.40E-02 4.39E-02 5.25E-02 871.09 99.89 -3.16E-02 4.39E-02 Ag-108m 79.13 6.60 1.09E+00 4.53E-02 2.06E+00 433.94 90.50 -4.82E-04 4.53E-02 614.28 89.80 -1.47E-03 6.36E-02 722.94 90.80 -1.86E-02 6.14E-02 Sb-125 176.31 6.84 5.92E-02 1.25E-01 5.83E-01 380.45 1.52 -1.74E+00 2.45E+00 427.87 29.60 -4.59E-02 1.25E-01 463.36 10.49 3.65E-02 4.01E-01 600.60 17.65 8.39E-02 2.65E-01 606.71 4.98 -6.57E-01 1.42E+00 635.95 11.22 1.93E-01 3.96E-01 [130]
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| 6/12/2019 1:13:04PM Page 6 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.63E+00 1.25E-01 2.61E+00 Ba-133 79.61 2.65 5.31E+00 7.56E-02 5.04E+00 81.00 32.90 -3.22E-01 3.34E-01 276.40 7.16 3.55E-02 5.03E-01 302.85 18.34 2.78E-02 2.09E-01 356.01 62.05 -7.61E-03 7.56E-02 383.85 8.94 -2.91E-01 4.05E-01 Cs-134 475.36 1.48 4.18E-01 5.34E-02 2.93E+00 563.25 8.34 3.73E-01 4.56E-01 569.33 15.37 -6.62E-03 2.45E-01 604.72 97.62 -5.48E-02 6.47E-02 795.86 85.46 -2.19E-02 5.34E-02 801.95 8.69 -4.43E-01 4.67E-01 1038.61 0.99 1.63E+00 5.61E+00 1167.97 1.79 2.40E+00 3.97E+00 1365.19 3.02 -3.83E-01 1.33E+00 Cs-137 661.66 85.10 1.43E-02 5.22E-02 5.22E-02 Eu-152 121.78 28.67 5.75E-02 1.46E-01 1.77E-01 244.70 7.61 5.08E-01 6.04E-01 295.94 0.45 2.10E+00 1.08E+01 344.28 26.60 -2.66E-02 1.46E-01 367.79 0.86 -4.24E-01 4.47E+00 411.12 2.24 -2.15E+00 1.65E+00 443.96 2.83 -5.14E-01 1.42E+00 488.68 0.42 2.45E+00 9.43E+00 563.99 0.49 9.19E-01 7.62E+00 586.26 0.46 6.23E+00 1.27E+01 678.62 0.47 4.93E+00 8.68E+00 688.67 0.86 6.43E-01 4.99E+00 719.35 0.28 4.12E+00 1.84E+01 778.90 12.96 -1.06E-01 3.65E-01 810.45 0.32 -4.01E-01 1.56E+01 867.37 4.26 3.27E-01 1.00E+00 919.33 0.43 -3.97E+00 1.27E+01 964.08 14.65 -2.32E-01 3.73E-01 1085.87 10.24 2.96E-01 6.46E-01 1089.74 1.73 5.12E-01 3.47E+00 1112.07 13.69 7.75E-03 4.09E-01 1212.95 1.43 9.04E-01 5.05E+00 1249.94 0.19 1.93E+01 3.74E+01 1299.14 1.63 7.76E-01 3.88E+00 1408.01 21.07 -5.02E-02 2.38E-01 1457.64 0.50 1.59E+02 4.48E+01 1528.10 0.28 -2.27E+00 1.05E+01 Eu-154 123.07 40.40 3.68E-02 1.24E-01 1.24E-01 247.93 6.89 -1.76E-01 5.50E-01 591.76 4.95 -2.56E-01 9.01E-01 692.42 1.78 -3.93E-01 2.72E+00 723.30 20.06 1.17E-02 2.84E-01 756.80 4.52 1.15E-01 9.39E-01 873.18 12.08 -2.31E-01 4.01E-01
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| [131]
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| 6/12/2019 1:13:04PM Page 7 of 7 Analysis Report for 12-Jun-19-10023 L1-10221C-FSGS-010SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 6.41E-02 1.24E-01 4.58E-01 1004.76 18.01 1.63E-01 3.01E-01 1274.43 34.80 -1.61E-02 1.91E-01 1596.48 1.80 -2.78E+00 1.47E+00 Eu-155 45.30 1.31 -3.25E-01 2.67E-01 3.08E+01 60.01 1.22 -3.65E+00 2.87E+01 86.55 30.70 9.27E-02 2.86E-01 105.31 21.10 -1.49E-01 2.67E-01 Ra-226 186.21 3.64 7.94E-01 1.21E+00 1.21E+00 Pa-231 27.36 10.30 3.89E+00 1.66E+00 3.96E+00 283.69 1.70 8.77E-01 2.15E+00 300.07 2.47 -3.56E-01 1.66E+00 302.65 2.20 3.57E-01 1.74E+00 330.06 1.40 1.80E+00 3.00E+00 U-235 143.76 10.96 -1.48E-01 7.50E-02 3.94E-01 163.33 5.08 9.19E-04 7.82E-01 185.71 57.20 1.41E-02 7.50E-02 202.11 1.08 2.79E-02 3.51E+00 205.31 5.01 -4.56E-01 7.02E-01 Am-241 59.54 35.90 -1.19E-01 1.03E+00 1.03E+00
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| [132]
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| 6/12/2019 1:13:27PM Page 1 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10024 Sample Description : L1-10221C-FSGS-011SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.687E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:05:00AM Acquisition Started : 6/12/2019 12:57:59PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.04 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77305 Fill Height : 1686.99 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:13:20PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
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| [133]
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| 6/12/2019 1:13:27PM Page 2 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.33 306 - 314 309.83 5.73E+01 16.04 9.28E+01 0.48 2 238.76 948 - 961 954.63 1.64E+02 21.36 1.02E+02 1.01 3 295.23 1173 - 1186 1180.21 8.42E+01 14.30 4.38E+01 0.38 4 338.29 1346 - 1358 1352.26 4.04E+01 11.23 3.26E+01 0.82 5 351.93 1398 - 1413 1406.74 1.38E+02 14.71 2.61E+01 0.93 6 582.94 2324 - 2337 2329.88 5.73E+01 9.89 1.47E+01 0.78 7 609.17 2428 - 2441 2434.74 9.94E+01 11.93 1.56E+01 1.07 8 910.83 3634 - 3648 3640.76 5.69E+01 8.45 5.10E+00 1.11 9 1460.33 5828 - 5851 5839.28 3.86E+02 20.18 5.52E+00 1.90 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.96 1460.82
| |
| * 10.66 8.44E+00 5.73E-01 Tl-208 0.99 583.19
| |
| * 85.00 8.44E-02 1.54E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 2.56E-01 3.93E-02 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77.11
| |
| * 17.10 3.98E-01 1.19E-01 87.35 3.97 [134]
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| 6/12/2019 1:13:27PM Page 3 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb212-XR 0.99 89.78 1.46 Bi-214 0.99 609.32
| |
| * 45.49 2.82E-01 3.78E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 3.54E-01 6.64E-02 351.93
| |
| * 35.60 3.41E-01 4.54E-02 785.96 1.06 Pb214-XR 0.99 74.82 5.80 77.11
| |
| * 9.70 7.02E-01 2.12E-01 87.35 2.24 89.78 0.82 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 3.07E-01 8.88E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 3.73E-01 5.78E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
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| [135]
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| 6/12/2019 1:13:27PM Page 4 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.963 8.44E+00 5.73E-01 Tl-208 0.990 8.44E-02 1.54E-02 X Bi-211 0.888 Pb-212 0.997 2.56E-01 3.93E-02
| |
| ? Pb212-XR 0.996 3.98E-01 1.19E-01 Bi-214 0.999 2.82E-01 3.78E-02 Pb-214 1.000 3.45E-01 3.75E-02
| |
| ? Pb214-XR 0.996 7.02E-01 2.12E-01 Ac-228 0.993 3.53E-01 4.84E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [136]
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| 6/12/2019 1:13:27PM Page 5 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:13:20PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 9.09E-02 6.58E-02 6.58E-02 BE-7 477.60 10.44 1.83E-01 3.87E-01 3.87E-01
| |
| + K-40 1460.82
| |
| * 10.66 8.44E+00 4.01E-01 4.01E-01 Mn-54 834.85 99.98 1.74E-03 5.54E-02 5.54E-02 Co-60 1173.23 99.85 7.42E-02 5.73E-02 7.23E-02 1332.49 99.98 3.70E-02 5.73E-02 Nb-94 702.65 99.81 -1.11E-03 4.67E-02 4.67E-02 871.09 99.89 3.42E-02 5.51E-02 Ag-108m 79.13 6.60 -4.21E-01 4.41E-02 1.31E+00 433.94 90.50 -2.76E-03 4.41E-02 614.28 89.80 -6.12E-02 5.69E-02 722.94 90.80 2.14E-02 5.81E-02 Sb-125 176.31 6.84 1.19E-01 1.37E-01 5.00E-01 380.45 1.52 6.09E-01 2.51E+00 427.87 29.60 -3.13E-02 1.37E-01 463.36 10.49 2.23E-02 4.32E-01 600.60 17.65 2.52E-01 2.71E-01 606.71 4.98 3.11E+00 1.54E+00 635.95 11.22 -1.90E-01 3.65E-01 [137]
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| 6/12/2019 1:13:27PM Page 6 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -7.59E-01 1.37E-01 2.18E+00 Ba-133 79.61 2.65 -1.17E+00 7.13E-02 3.18E+00 81.00 32.90 -2.83E-01 2.02E-01 276.40 7.16 2.22E-02 5.28E-01 302.85 18.34 5.13E-02 2.05E-01 356.01 62.05 -1.35E-02 7.13E-02 383.85 8.94 1.40E-01 4.32E-01 Cs-134 475.36 1.48 -2.23E-02 5.58E-02 2.66E+00 563.25 8.34 -1.24E-01 5.88E-01 569.33 15.37 -1.35E-01 2.54E-01 604.72 97.62 -1.09E-02 6.97E-02 795.86 85.46 2.09E-02 5.58E-02 801.95 8.69 1.28E-01 5.44E-01 1038.61 0.99 1.59E+00 5.52E+00 1167.97 1.79 -1.99E-03 3.78E+00 1365.19 3.02 -6.98E-01 1.62E+00 Cs-137 661.66 85.10 2.30E-02 6.06E-02 6.06E-02 Eu-152 121.78 28.67 -3.65E-02 1.25E-01 1.25E-01 244.70 7.61 1.90E-01 5.43E-01 295.94 0.45 2.40E+00 1.12E+01 344.28 26.60 -6.34E-02 1.37E-01 367.79 0.86 2.61E+00 3.81E+00 411.12 2.24 -3.82E-01 1.69E+00 443.96 2.83 -4.34E-01 1.40E+00 488.68 0.42 4.20E+00 1.01E+01 563.99 0.49 -1.34E+01 9.09E+00 586.26 0.46 -2.91E+00 1.32E+01 678.62 0.47 6.84E+00 8.95E+00 688.67 0.86 2.64E+00 5.10E+00 719.35 0.28 -1.25E+01 1.44E+01 778.90 12.96 5.96E-02 3.42E-01 810.45 0.32 -1.83E+01 1.18E+01 867.37 4.26 -5.17E-01 1.27E+00 919.33 0.43 6.49E+00 1.12E+01 964.08 14.65 4.38E-01 5.09E-01 1085.87 10.24 -1.53E-01 5.16E-01 1089.74 1.73 1.46E+00 3.26E+00 1112.07 13.69 -1.63E-01 4.41E-01 1212.95 1.43 7.16E-01 5.46E+00 1249.94 0.19 6.99E+00 3.58E+01 1299.14 1.63 -6.26E-03 3.27E+00 1408.01 21.07 2.14E-02 2.56E-01 1457.64 0.50 1.72E+02 4.56E+01 1528.10 0.28 -3.63E+00 1.48E+01 Eu-154 123.07 40.40 -4.03E-02 9.00E-02 9.00E-02 247.93 6.89 -4.01E-01 4.84E-01 591.76 4.95 1.03E-01 8.19E-01 692.42 1.78 -9.17E-02 2.57E+00 723.30 20.06 1.45E-01 2.71E-01 756.80 4.52 -3.49E-01 1.03E+00 873.18 12.08 -1.39E-01 4.52E-01
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| [138]
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| 6/12/2019 1:13:27PM Page 7 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 2.34E-01 9.00E-02 5.83E-01 1004.76 18.01 9.49E-02 2.93E-01 1274.43 34.80 6.51E-02 2.04E-01 1596.48 1.80 -1.87E+00 2.16E+00 Eu-155 45.30 1.31 5.55E+00 2.28E-01 1.41E+01 60.01 1.22 -1.41E+00 1.30E+01 86.55 30.70 1.44E-01 2.30E-01 105.31 21.10 -5.85E-02 2.28E-01 Ra-226 186.21 3.64 1.08E+00 1.12E+00 1.12E+00 Pa-231 27.36 10.30 4.88E-01 1.49E+00 1.49E+00 283.69 1.70 8.75E-01 2.16E+00 300.07 2.47 -1.44E+00 1.55E+00 302.65 2.20 4.32E-01 1.70E+00 330.06 1.40 1.92E-02 2.99E+00 U-235 143.76 10.96 1.37E-01 7.10E-02 3.48E-01 163.33 5.08 4.42E-01 7.31E-01 185.71 57.20 8.13E-02 7.10E-02 202.11 1.08 1.77E-01 3.10E+00 205.31 5.01 -5.34E-01 6.42E-01 Am-241 59.54 35.90 -1.72E-01 4.41E-01 4.41E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [139]
| |
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| 6/13/2019 6:00:00AM Page 1 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10024 Sample Description : L1-10221C-FSGS-011SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.687E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:05:00AM Acquisition Started : 6/12/2019 12:57:59PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 1800.0 seconds Real Time : 1800.7 seconds Dead Time : 0.04 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/13/2019 Efficiency Calibration Description :
| |
| Sample Number : 77305 Fill Height : 1686.99 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/13/2019 5:59:52AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [140]
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| 6/13/2019 6:00:00AM Page 2 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.38 307 - 316 310.04 1.20E+02 23.43 1.85E+02 0.61 2 90.16 359 - 365 361.09 3.45E+01 15.09 1.02E+02 0.32 3 186.33 737 - 752 745.18 1.24E+02 24.65 1.61E+02 0.61 4 238.76 948 - 960 954.63 3.99E+02 29.29 1.73E+02 1.02 5 295.27 1173 - 1188 1180.35 1.47E+02 21.98 1.12E+02 0.65 6 338.32 1346 - 1359 1352.36 6.73E+01 16.66 7.57E+01 0.76 7 351.97 1402 - 1413 1406.87 2.90E+02 20.11 4.57E+01 1.06 8 488.01 1946 - 1955 1950.48 1.57E+01 8.59 2.53E+01 0.30 9 511.03 2032 - 2049 2042.49 8.21E+01 18.44 7.89E+01 1.00 10 558.64 2226 - 2241 2232.77 3.37E+01 12.48 4.03E+01 0.62 11 583.01 2323 - 2338 2330.16 1.27E+02 14.93 3.21E+01 1.24 12 609.21 2428 - 2442 2434.87 1.90E+02 17.36 3.88E+01 0.89 13 910.88 3633 - 3650 3640.97 1.08E+02 12.66 1.62E+01 1.48 14 933.72 3726 - 3738 3732.31 1.50E+01 7.96 1.80E+01 0.56 15 968.81 3863 - 3880 3872.64 4.85E+01 12.33 3.15E+01 0.64 16 1120.39 4471 - 4487 4478.96 4.98E+01 10.79 2.13E+01 0.61 17 1460.32 5826 - 5851 5839.20 8.02E+02 30.22 2.60E+01 1.93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty
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| [141]
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| 6/13/2019 6:00:00AM Page 3 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 1.00 511.00
| |
| * 100.00 4.78E-02 1.12E-02 K-40 0.96 1460.82
| |
| * 10.66 8.76E+00 5.04E-01 Tl-208 0.99 583.19
| |
| * 85.00 9.35E-02 1.23E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 3.12E-01 3.40E-02 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77.11
| |
| * 17.10 4.18E-01 9.20E-02 87.35 3.97 89.78
| |
| * 1.46 1.01E+00 4.54E-01 Bi-214 0.99 609.32
| |
| * 45.49 2.70E-01 2.95E-02 768.36 4.89 806.18 1.26 934.06
| |
| * 3.11 4.16E-01 2.21E-01 1120.29
| |
| * 14.92 3.24E-01 7.14E-02 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 3.09E-01 5.24E-02 351.93
| |
| * 35.60 3.59E-01 3.80E-02 785.96 1.06 Ra-226 0.99 186.21
| |
| * 3.64 1.02E+00 2.19E-01 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 2.55E-01 6.65E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 3.54E-01 4.43E-02 964.77 4.99 968.97
| |
| * 15.80 2.71E-01 6.99E-02 1588.20 3.22 U-235 0.95 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 6.50E-02 1.39E-02 202.11 1.08 205.31 5.01
| |
| [142]
| |
| | |
| 6/13/2019 6:00:00AM Page 4 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| An Pk 1.000 4.78E-02 1.12E-02 K-40 0.960 8.76E+00 5.04E-01 Tl-208 0.995 9.35E-02 1.23E-02 X Bi-211 0.880 Pb-212 0.998 3.12E-01 3.40E-02 Pb212-XR 0.993 4.41E-01 9.01E-02 Bi-214 0.998 2.80E-01 2.70E-02 Pb-214 1.000 3.42E-01 3.07E-02 X Pb214-XR 0.993
| |
| ? Ra-226 0.998 1.02E+00 2.19E-01 Ac-228 0.994 3.12E-01 3.26E-02 X Ac228-XR 0.998 X Th-231 0.315
| |
| ? U-235 0.958 6.50E-02 1.39E-02 X U235-XR 0.998
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [143]
| |
| | |
| 6/13/2019 6:00:00AM Page 5 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/13/2019 5:59:52AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide 8 488.01 8.71951E-03 54.70 Tol. Eu-152 10 558.64 1.87275E-02 37.04 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 4.78E-02 3.34E-02 3.34E-02 BE-7 477.60 10.44 1.68E-01 2.84E-01 2.84E-01
| |
| + K-40 1460.82
| |
| * 10.66 8.76E+00 4.23E-01 4.23E-01 Mn-54 834.85 99.98 7.31E-03 3.76E-02 3.76E-02 Co-60 1173.23 99.85 5.21E-02 3.77E-02 4.92E-02 1332.49 99.98 2.02E-02 3.77E-02 Nb-94 702.65 99.81 4.88E-03 3.37E-02 3.37E-02 871.09 99.89 1.71E-02 3.69E-02 Ag-108m 79.13 6.60 1.60E-01 2.99E-02 9.24E-01 433.94 90.50 -1.33E-02 2.99E-02 614.28 89.80 -2.57E-02 4.25E-02 722.94 90.80 -1.09E-02 3.94E-02 Sb-125 176.31 6.84 4.27E-02 9.52E-02 3.54E-01 380.45 1.52 -5.90E-02 1.74E+00 427.87 29.60 2.74E-02 9.52E-02 463.36 10.49 9.70E-02 2.88E-01 600.60 17.65 3.22E-02 1.73E-01 [144]
| |
| | |
| 6/13/2019 6:00:00AM Page 6 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 606.71 4.98 3.09E+00 9.52E-02 1.08E+00 635.95 11.22 -3.01E-02 2.46E-01 671.44 1.79 -9.10E-02 1.71E+00 Ba-133 79.61 2.65 5.26E-01 5.27E-02 2.26E+00 81.00 32.90 -1.18E-01 1.42E-01 276.40 7.16 2.50E-01 3.77E-01 302.85 18.34 1.64E-02 1.43E-01 356.01 62.05 -5.15E-02 5.27E-02 383.85 8.94 -1.20E-01 3.05E-01 Cs-134 475.36 1.48 -7.96E-01 4.02E-02 1.86E+00 563.25 8.34 -4.23E-02 4.01E-01 569.33 15.37 -7.81E-02 1.76E-01 604.72 97.62 -2.07E-02 4.76E-02 795.86 85.46 3.65E-02 4.02E-02 801.95 8.69 3.33E-01 3.79E-01 1038.61 0.99 6.51E-01 3.53E+00 1167.97 1.79 -1.62E+00 2.40E+00 1365.19 3.02 -4.52E-01 9.86E-01 Cs-137 661.66 85.10 4.53E-03 4.04E-02 4.04E-02 Eu-152 121.78 28.67 -4.88E-02 8.89E-02 8.89E-02 244.70 7.61 2.47E-02 3.90E-01 295.94 0.45 1.04E+01 7.84E+00 344.28 26.60 -8.02E-02 9.47E-02 367.79 0.86 1.01E+00 2.74E+00 411.12 2.24 2.95E-01 1.28E+00 443.96 2.83 9.63E-02 9.59E-01 488.68 0.42 2.48E-02 6.73E+00 563.99 0.49 9.85E-01 6.28E+00 586.26 0.46 -2.56E+00 9.40E+00 678.62 0.47 4.14E+00 6.57E+00 688.67 0.86 -4.32E-01 3.44E+00 719.35 0.28 -6.91E+00 1.07E+01 778.90 12.96 -5.26E-02 2.46E-01 810.45 0.32 -9.64E+00 9.52E+00 867.37 4.26 -2.55E-01 8.58E-01 919.33 0.43 7.17E+00 8.21E+00 964.08 14.65 1.36E-01 3.51E-01 1085.87 10.24 3.83E-02 4.02E-01 1089.74 1.73 5.14E-01 2.43E+00 1112.07 13.69 -1.49E-01 3.25E-01 1212.95 1.43 1.09E+00 3.73E+00 1249.94 0.19 1.31E+01 2.54E+01 1299.14 1.63 -6.58E-02 2.42E+00 1408.01 21.07 4.57E-02 1.61E-01 1457.64 0.50 1.85E+02 3.29E+01 1528.10 0.28 -1.53E+00 9.44E+00 Eu-154 123.07 40.40 -3.14E-02 6.36E-02 6.36E-02 247.93 6.89 -3.49E-01 3.60E-01 591.76 4.95 -1.26E-01 5.46E-01 692.42 1.78 -4.22E-01 1.73E+00 723.30 20.06 -4.78E-02 1.82E-01
| |
| [145]
| |
| | |
| 6/13/2019 6:00:00AM Page 7 of 7 Analysis Report for 12-Jun-19-10024 L1-10221C-FSGS-011SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 756.80 4.52 -5.31E-01 6.36E-02 6.81E-01 873.18 12.08 8.50E-03 3.11E-01 996.29 10.48 3.24E-01 3.86E-01 1004.76 18.01 -7.96E-03 2.02E-01 1274.43 34.80 -9.17E-02 1.20E-01 1596.48 1.80 -8.58E-01 1.40E+00 Eu-155 45.30 1.31 4.23E+00 1.56E-01 9.56E+00 60.01 1.22 -4.68E+00 9.48E+00 86.55 30.70 1.47E-01 1.56E-01 105.31 21.10 -1.00E-02 1.57E-01
| |
| + Ra-226 186.21
| |
| * 3.64 1.02E+00 6.37E-01 6.37E-01 Pa-231 27.36 10.30 7.95E-01 1.04E+00 1.04E+00 283.69 1.70 1.43E-01 1.44E+00 300.07 2.47 2.05E-01 1.10E+00 302.65 2.20 1.82E-01 1.19E+00 330.06 1.40 1.58E+00 2.09E+00
| |
| + U-235 143.76 10.96 -2.01E-02 4.05E-02 2.41E-01 163.33 5.08 4.48E-01 5.24E-01 185.71
| |
| * 57.20 6.50E-02 4.05E-02 202.11 1.08 -1.25E+00 2.20E+00 205.31 5.01 -2.61E-01 4.78E-01 Am-241 59.54 35.90 -7.93E-02 3.31E-01 3.31E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [146]
| |
| | |
| 6/12/2019 1:13:21PM Page 1 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10025 Sample Description : L1-10221C-FSGS-012SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.409E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:10:00AM Acquisition Started : 6/12/2019 12:58:06PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.04 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77306 Fill Height : 1408.71 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:13:12PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [147]
| |
| | |
| 6/12/2019 1:13:21PM Page 2 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 186.12 739 - 749 745.22 4.23E+01 14.01 6.47E+01 0.50 M 2 238.64 949 - 975 955.02 1.94E+02 14.73 5.28E+01 1.06 m 3 241.80 949 - 975 967.67 4.67E+01 8.62 5.74E+01 1.06 4 295.17 1174 - 1188 1180.88 7.50E+01 13.18 3.40E+01 1.36 5 351.75 1401 - 1413 1407.00 1.25E+02 14.90 3.70E+01 1.20 6 583.15 2326 - 2339 2331.93 7.13E+01 12.28 2.87E+01 1.22 7 609.21 2427 - 2443 2436.09 1.18E+02 13.10 1.71E+01 0.55 8 661.56 2636 - 2655 2645.43 2.01E+02 16.47 2.00E+01 1.47 9 910.96 3633 - 3650 3642.87 6.40E+01 9.67 8.99E+00 0.36 10 1460.37 5828 - 5857 5841.86 4.41E+02 22.07 1.04E+01 2.01 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.96 1460.82
| |
| * 10.66 9.45E+00 6.26E-01 Cs-137 0.99 661.66
| |
| * 85.10 3.18E-01 3.23E-02 Tl-208 1.00 583.19
| |
| * 85.00 1.04E-01 1.90E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 3.09E-01 3.43E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 3.31E-01 4.18E-02[148]
| |
| | |
| 6/12/2019 1:13:21PM Page 3 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99
| |
| * 7.25 4.50E-01 9.05E-02 295.22
| |
| * 18.42 3.17E-01 6.13E-02 351.93
| |
| * 35.60 3.09E-01 4.44E-02 785.96 1.06 Ra-226 0.99 186.21
| |
| * 3.64 7.20E-01 2.46E-01 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 4.14E-01 6.49E-02 964.77 4.99 968.97 15.80 1588.20 3.22 U-235 0.98 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 4.58E-02 1.56E-02 202.11 1.08 205.31 5.01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
| |
| [149]
| |
| | |
| 6/12/2019 1:13:21PM Page 4 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.968 9.45E+00 6.26E-01 Cs-137 0.999 3.18E-01 3.23E-02 Tl-208 1.000 1.04E-01 1.90E-02 X Bi-211 0.928 Pb-212 1.000 3.09E-01 3.43E-02 Bi-214 0.999 3.31E-01 4.18E-02 Pb-214 0.996 3.31E-01 3.34E-02
| |
| ? Ra-226 0.999 7.20E-01 2.46E-01 Ac-228 0.997 4.14E-01 6.49E-02
| |
| ? U-235 0.981 4.58E-02 1.56E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [150]
| |
| | |
| 6/12/2019 1:13:21PM Page 5 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:13:12PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.41E-02 6.18E-02 6.18E-02 BE-7 477.60 10.44 -1.77E-01 4.06E-01 4.06E-01
| |
| + K-40 1460.82
| |
| * 10.66 9.45E+00 5.57E-01 5.57E-01 Mn-54 834.85 99.98 -1.36E-02 5.35E-02 5.35E-02 Co-60 1173.23 99.85 2.59E-02 7.33E-02 8.00E-02 1332.49 99.98 -3.18E-03 7.33E-02 Nb-94 702.65 99.81 1.69E-02 4.71E-02 5.08E-02 871.09 99.89 -4.22E-02 4.71E-02 Ag-108m 79.13 6.60 -4.47E-01 4.87E-02 1.81E+00 433.94 90.50 -1.36E-02 4.87E-02 614.28 89.80 -2.11E-02 8.29E-02 722.94 90.80 -1.19E-02 5.95E-02 Sb-125 176.31 6.84 2.98E-01 1.42E-01 5.95E-01 380.45 1.52 1.10E+00 2.69E+00 427.87 29.60 -4.51E-02 1.42E-01 463.36 10.49 2.20E-01 4.25E-01 600.60 17.65 4.12E-02 2.80E-01 606.71 4.98 2.70E+00 1.66E+00 635.95 11.22 -1.26E-01 3.94E-01 [151]
| |
| | |
| 6/12/2019 1:13:21PM Page 6 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 3.35E-01 1.42E-01 2.28E+00 Ba-133 79.61 2.65 9.30E-01 9.13E-02 4.39E+00 81.00 32.90 -7.55E-01 2.89E-01 276.40 7.16 -5.89E-02 6.07E-01 302.85 18.34 1.75E-01 2.43E-01 356.01 62.05 -6.35E-02 9.13E-02 383.85 8.94 3.67E-02 4.60E-01 Cs-134 475.36 1.48 -1.10E+00 6.38E-02 2.87E+00 563.25 8.34 3.35E-01 5.30E-01 569.33 15.37 -1.37E-01 3.18E-01 604.72 97.62 -3.05E-02 8.10E-02 795.86 85.46 5.26E-02 6.38E-02 801.95 8.69 -6.84E-01 5.72E-01 1038.61 0.99 -3.19E-01 5.81E+00 1167.97 1.79 4.69E-01 4.55E+00 1365.19 3.02 1.01E+00 1.83E+00
| |
| + Cs-137 661.66
| |
| * 85.10 3.18E-01 4.96E-02 4.96E-02 Eu-152 121.78 28.67 -3.61E-02 1.58E-01 1.62E-01 244.70 7.61 -2.14E-02 6.03E-01 295.94 0.45 1.40E+01 1.15E+01 344.28 26.60 -6.86E-02 1.58E-01 367.79 0.86 7.91E-02 4.94E+00 411.12 2.24 4.31E-02 1.90E+00 443.96 2.83 3.19E-01 1.64E+00 488.68 0.42 -5.78E+00 1.06E+01 563.99 0.49 -3.75E+00 8.75E+00 586.26 0.46 1.35E+01 1.56E+01 678.62 0.47 -1.46E+00 8.60E+00 688.67 0.86 5.56E-01 5.53E+00 719.35 0.28 2.55E-01 1.68E+01 778.90 12.96 -6.66E-01 3.71E-01 810.45 0.32 -6.95E+00 1.59E+01 867.37 4.26 -1.02E+00 1.13E+00 919.33 0.43 -1.37E+01 1.07E+01 964.08 14.65 4.45E-01 4.76E-01 1085.87 10.24 1.96E-01 6.65E-01 1089.74 1.73 1.52E-01 4.16E+00 1112.07 13.69 -2.99E-03 4.81E-01 1212.95 1.43 2.47E+00 5.55E+00 1249.94 0.19 -9.42E+00 3.56E+01 1299.14 1.63 -6.04E+00 3.71E+00 1408.01 21.07 -1.76E-01 2.51E-01 1457.64 0.50 2.08E+02 4.79E+01 1528.10 0.28 1.17E+01 1.75E+01 Eu-154 123.07 40.40 6.97E-02 1.16E-01 1.16E-01 247.93 6.89 -3.47E-01 5.70E-01 591.76 4.95 -1.86E-01 9.14E-01 692.42 1.78 -4.11E-01 2.77E+00 723.30 20.06 2.44E-02 2.69E-01 756.80 4.52 -6.04E-01 1.01E+00 873.18 12.08 3.73E-02 4.08E-01
| |
| [152]
| |
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| 6/12/2019 1:13:21PM Page 7 of 7 Analysis Report for 12-Jun-19-10025 L1-10221C-FSGS-012SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 2.52E-01 1.16E-01 6.03E-01 1004.76 18.01 2.20E-01 3.24E-01 1274.43 34.80 2.05E-01 2.00E-01 1596.48 1.80 1.00E+00 2.75E+00 Eu-155 45.30 1.31 7.93E+00 2.55E-01 2.40E+01 60.01 1.22 2.16E+01 2.64E+01 86.55 30.70 -8.63E-02 2.58E-01 105.31 21.10 1.54E-02 2.55E-01
| |
| + Ra-226 186.21
| |
| * 3.64 7.20E-01 7.66E-01 7.66E-01 Pa-231 27.36 10.30 2.77E+00 1.87E+00 2.69E+00 283.69 1.70 -2.35E-01 2.55E+00 300.07 2.47 1.18E+00 1.87E+00 302.65 2.20 1.38E+00 2.01E+00 330.06 1.40 -1.37E+00 2.91E+00
| |
| + U-235 143.76 10.96 -1.87E-01 4.88E-02 3.98E-01 163.33 5.08 -4.49E-01 7.84E-01 185.71
| |
| * 57.20 4.58E-02 4.88E-02 202.11 1.08 -2.32E+00 3.86E+00 205.31 5.01 -2.85E-01 8.74E-01 Am-241 59.54 35.90 -5.22E-01 8.95E-01 8.95E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [153]
| |
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| 6/12/2019 1:33:25PM Page 1 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10026 Sample Description : L1-10221C-FQGS-012SS Sample Type : Soil Unit :
| |
| Sample Point :
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| Sample Size : 1.593E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:10:00AM Acquisition Started : 6/12/2019 1:18:13PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.4 seconds Dead Time : 0.04 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
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| Sample Number : 77307 Fill Height : 1592.65 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:33:16PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
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| [154]
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| 6/12/2019 1:33:25PM Page 2 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.06 305 - 317 309.56 4.50E+01 16.40 7.50E+01 0.80 2 185.86 740 - 752 744.15 6.12E+01 15.70 6.88E+01 0.86 3 238.61 946 - 960 954.92 1.85E+02 21.99 1.04E+02 0.74 4 295.12 1173 - 1188 1180.72 7.57E+01 15.09 5.03E+01 0.76 5 351.79 1398 - 1413 1407.17 1.27E+02 16.39 4.75E+01 0.96 6 583.14 2325 - 2341 2331.88 9.89E+01 11.23 9.11E+00 1.65 7 609.27 2428 - 2443 2436.33 1.21E+02 13.68 2.19E+01 0.86 8 661.50 2637 - 2651 2645.16 9.87E+01 11.19 9.26E+00 1.55 9 910.96 3636 - 3650 3642.88 5.24E+01 9.11 1.06E+01 1.47 10 1120.18 4474 - 4486 4479.99 2.61E+01 7.93 1.39E+01 0.53 11 1460.47 5828 - 5854 5842.26 4.78E+02 22.21 3.47E+00 2.15 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.98 1460.82
| |
| * 10.66 9.89E+00 6.29E-01 Cs-137 0.99 661.66
| |
| * 85.10 1.52E-01 1.95E-02 Tl-208 1.00 583.19
| |
| * 85.00 1.40E-01 1.80E-02 Pb-212 1.00 115.18 0.60 238.63
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| * 43.60 2.87E-01 4.13E-02 300.09 3.30 [155]
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| | |
| 6/12/2019 1:33:25PM Page 3 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb212-XR 1.00 74.82 10.28 77.11
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| * 17.10 4.19E-01 1.59E-01 87.35 3.97 89.78 1.46 Bi-214 1.00 609.32
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| * 45.49 3.30E-01 4.22E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29
| |
| * 14.92 3.23E-01 9.90E-02 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
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| * 18.42 3.13E-01 6.71E-02 351.93
| |
| * 35.60 3.05E-01 4.65E-02 785.96 1.06 Pb214-XR 1.00 74.82 5.80 77.11
| |
| * 9.70 7.38E-01 2.82E-01 87.35 2.24 89.78 0.82 Ra-226 0.98 186.21
| |
| * 3.64 1.02E+00 2.74E-01 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 3.28E-01 5.87E-02 964.77 4.99 968.97 15.80 1588.20 3.22 U-235 0.99 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 6.49E-02 1.75E-02 202.11 1.08 205.31 5.01
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| [156]
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| 6/12/2019 1:33:25PM Page 4 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS
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| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
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| ? = Manually edited nuclide.
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| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| K-40 0.981 9.89E+00 6.29E-01 Cs-137 0.996 1.52E-01 1.95E-02 Tl-208 1.000 1.40E-01 1.80E-02 X Bi-211 0.920 Pb-212 1.000 2.87E-01 4.13E-02
| |
| ? Pb212-XR 1.000 4.19E-01 1.59E-01 Bi-214 1.000 3.29E-01 3.88E-02 Pb-214 0.998 3.08E-01 3.82E-02
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| ? Pb214-XR 1.000 7.38E-01 2.82E-01
| |
| ? Ra-226 0.980 1.02E+00 2.74E-01 Ac-228 0.997 3.28E-01 5.87E-02
| |
| ? U-235 0.998 6.49E-02 1.75E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [157]
| |
| | |
| 6/12/2019 1:33:25PM Page 5 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:33:16PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 8.67E-02 6.06E-02 6.06E-02 BE-7 477.60 10.44 4.43E-02 4.45E-01 4.45E-01
| |
| + K-40 1460.82
| |
| * 10.66 9.89E+00 3.37E-01 3.37E-01 Mn-54 834.85 99.98 2.10E-02 5.57E-02 5.57E-02 Co-60 1173.23 99.85 1.35E-04 5.83E-02 7.19E-02 1332.49 99.98 -1.52E-02 5.83E-02 Nb-94 702.65 99.81 3.48E-02 5.32E-02 5.46E-02 871.09 99.89 -4.66E-04 5.32E-02 Ag-108m 79.13 6.60 6.30E-01 4.58E-02 1.54E+00 433.94 90.50 -2.63E-02 4.58E-02 614.28 89.80 -4.83E-02 9.03E-02 722.94 90.80 6.09E-03 5.97E-02 Sb-125 176.31 6.84 -7.96E-01 1.52E-01 5.48E-01 380.45 1.52 8.59E-01 2.87E+00 427.87 29.60 5.32E-02 1.52E-01 463.36 10.49 3.55E-01 4.25E-01 600.60 17.65 -2.99E-02 2.68E-01 606.71 4.98 2.75E+00 1.72E+00 635.95 11.22 1.01E-01 4.34E-01 [158]
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| 6/12/2019 1:33:25PM Page 6 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 8.54E-01 1.52E-01 2.74E+00 Ba-133 79.61 2.65 1.63E-01 9.32E-02 3.67E+00 81.00 32.90 6.09E-02 2.52E-01 276.40 7.16 -6.45E-02 5.75E-01 302.85 18.34 1.33E-02 2.27E-01 356.01 62.05 -3.21E-02 9.32E-02 383.85 8.94 9.28E-02 4.94E-01 Cs-134 475.36 1.48 -1.11E+00 6.48E-02 3.03E+00 563.25 8.34 -8.40E-01 5.44E-01 569.33 15.37 5.26E-02 3.23E-01 604.72 97.62 8.84E-03 8.30E-02 795.86 85.46 6.96E-02 6.48E-02 801.95 8.69 -5.10E-01 5.13E-01 1038.61 0.99 3.79E-01 5.48E+00 1167.97 1.79 3.76E+00 4.00E+00 1365.19 3.02 -3.35E-01 1.66E+00
| |
| + Cs-137 661.66
| |
| * 85.10 1.52E-01 3.13E-02 3.13E-02 Eu-152 121.78 28.67 -1.19E-01 1.60E-01 1.60E-01 244.70 7.61 1.48E-01 6.17E-01 295.94 0.45 9.63E+00 1.18E+01 344.28 26.60 9.00E-02 1.69E-01 367.79 0.86 -1.29E+00 4.45E+00 411.12 2.24 -4.44E-01 1.98E+00 443.96 2.83 1.59E-01 1.52E+00 488.68 0.42 9.26E-02 9.48E+00 563.99 0.49 -1.33E+00 9.90E+00 586.26 0.46 1.48E+01 1.54E+01 678.62 0.47 -1.48E+00 9.99E+00 688.67 0.86 2.40E+00 6.12E+00 719.35 0.28 -3.44E+00 1.74E+01 778.90 12.96 -3.30E-01 3.94E-01 810.45 0.32 6.28E+00 1.49E+01 867.37 4.26 -4.40E-01 1.17E+00 919.33 0.43 -8.62E+00 1.25E+01 964.08 14.65 3.81E-01 4.85E-01 1085.87 10.24 2.78E-01 6.26E-01 1089.74 1.73 -1.08E+00 3.60E+00 1112.07 13.69 -2.74E-01 4.85E-01 1212.95 1.43 3.05E+00 5.28E+00 1249.94 0.19 -5.51E+00 3.82E+01 1299.14 1.63 -1.87E+00 4.24E+00 1408.01 21.07 -2.29E-01 2.59E-01 1457.64 0.50 2.09E+02 4.79E+01 1528.10 0.28 -3.51E+00 9.06E+00 Eu-154 123.07 40.40 9.03E-02 1.15E-01 1.15E-01 247.93 6.89 1.41E-01 5.70E-01 591.76 4.95 1.03E+00 9.29E-01 692.42 1.78 -2.41E-01 2.79E+00 723.30 20.06 -6.46E-03 2.77E-01 756.80 4.52 6.11E-02 1.15E+00 873.18 12.08 2.56E-01 4.60E-01
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| [159]
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| 6/12/2019 1:33:25PM Page 7 of 7 Analysis Report for 12-Jun-19-10026 L1-10221C-FQGS-012SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 4.57E-01 1.15E-01 5.55E-01 1004.76 18.01 1.49E-01 3.42E-01 1274.43 34.80 -1.43E-01 2.00E-01 1596.48 1.80 -1.83E+00 2.65E+00 Eu-155 45.30 1.31 6.42E+00 2.54E-01 2.41E+01 60.01 1.22 -1.94E+01 2.51E+01 86.55 30.70 3.27E-01 2.81E-01 105.31 21.10 -2.79E-01 2.54E-01
| |
| + Ra-226 186.21
| |
| * 3.64 1.02E+00 8.18E-01 8.18E-01 Pa-231 27.36 10.30 2.30E+00 1.78E+00 2.69E+00 283.69 1.70 -4.56E-01 2.22E+00 300.07 2.47 7.19E-02 1.78E+00 302.65 2.20 -4.36E-03 1.90E+00 330.06 1.40 3.37E+00 3.07E+00
| |
| + U-235 143.76 10.96 9.94E-02 5.21E-02 4.45E-01 163.33 5.08 -3.27E-02 7.92E-01 185.71
| |
| * 57.20 6.49E-02 5.21E-02 202.11 1.08 1.18E+00 3.89E+00 205.31 5.01 -1.16E+00 8.33E-01 Am-241 59.54 35.90 -3.72E-01 8.85E-01 8.85E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| [160]
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| 6/12/2019 1:35:24PM Page 1 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10027 Sample Description : L1-10221C-FSGS-013SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.419E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:15:00AM Acquisition Started : 6/12/2019 1:20:14PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.4 seconds Dead Time : 0.04 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77308 Fill Height : 1419.47 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:35:16PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
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| [161]
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| 6/12/2019 1:35:24PM Page 2 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.63 472 - 481 477.45 2.03E+02 24.20 1.67E+02 1.05 2 295.06 587 - 594 590.18 7.72E+01 13.95 5.78E+01 1.67 3 351.87 700 - 708 703.68 1.35E+02 17.15 7.33E+01 1.41 4 583.20 1162 - 1171 1166.01 6.66E+01 11.53 2.94E+01 0.86 5 609.40 1212 - 1224 1218.37 1.30E+02 15.50 4.21E+01 1.64 6 661.74 1317 - 1328 1323.01 9.93E+01 12.83 2.57E+01 1.78 7 911.53 1818 - 1828 1822.52 4.38E+01 9.49 1.93E+01 1.11 8 1120.71 2236 - 2247 2240.96 4.33E+01 9.65 1.97E+01 1.62 9 1173.39 2342 - 2352 2346.38 4.90E+01 10.26 2.20E+01 1.63 10 1332.79 2660 - 2672 2665.39 5.53E+01 9.12 1.07E+01 1.38 11 1460.92 2915 - 2929 2921.90 4.39E+02 21.31 5.48E+00 2.26 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
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| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 8.43E+00 5.49E-01 Co-60 0.99 1173.23
| |
| * 99.85 8.66E-02 1.85E-02 1332.49
| |
| * 99.98 1.06E-01 1.80E-02 Cs-137 0.99 661.66
| |
| * 85.10 1.41E-01 2.02E-02 Tl-208 1.00 583.19
| |
| * 85.00 8.74E-02 1.60E-02 Pb-212 1.00 115.18 0.60 [162]
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| 6/12/2019 1:35:24PM Page 3 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-212 1.00 238.63
| |
| * 43.60 2.89E-01 4.16E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 3.28E-01 4.38E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29
| |
| * 14.92 4.97E-01 1.13E-01 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 2.93E-01 5.80E-02 351.93
| |
| * 35.60 3.00E-01 4.51E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 2.54E-01 5.62E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
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| [163]
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| 6/12/2019 1:35:24PM Page 4 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.998 8.43E+00 5.49E-01 Co-60 0.991 9.66E-02 1.29E-02 Cs-137 0.999 1.41E-01 2.02E-02 Tl-208 1.000 8.74E-02 1.60E-02 X Bi-211 0.904 Pb-212 1.000 2.89E-01 4.16E-02 Bi-214 0.996 3.50E-01 4.09E-02 Pb-214 0.998 2.97E-01 3.56E-02 Ac-228 0.995 2.54E-01 5.62E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [164]
| |
| | |
| 6/12/2019 1:35:24PM Page 5 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:35:16PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 9.29E-02 6.06E-02 6.06E-02 BE-7 477.60 10.44 4.81E-02 3.71E-01 3.71E-01
| |
| + K-40 1460.82
| |
| * 10.66 8.43E+00 3.12E-01 3.12E-01 Mn-54 834.85 99.98 -2.12E-03 5.01E-02 5.01E-02
| |
| + Co-60 1173.23
| |
| * 99.85 8.66E-02 3.98E-02 5.00E-02 1332.49
| |
| * 99.98 1.06E-01 3.98E-02 Nb-94 702.65 99.81 -4.16E-02 3.95E-02 3.95E-02 871.09 99.89 -2.80E-02 4.42E-02 Ag-108m 79.13 6.60 9.10E-01 3.92E-02 1.32E+00 433.94 90.50 -5.35E-03 3.92E-02 614.28 89.80 -1.01E-02 6.99E-02 722.94 90.80 -1.15E-02 5.40E-02 Sb-125 176.31 6.84 5.72E-02 1.27E-01 5.63E-01 380.45 1.52 -1.15E+00 2.21E+00 427.87 29.60 2.89E-02 1.27E-01 463.36 10.49 1.22E-01 3.65E-01 600.60 17.65 -2.42E-02 2.37E-01 606.71 4.98 -4.43E-04 1.58E+00 635.95 11.22 -1.90E-01 3.46E-01 [165]
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| 6/12/2019 1:35:24PM Page 6 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -7.93E-01 1.27E-01 2.14E+00 Ba-133 79.61 2.65 1.06E+00 8.89E-02 3.04E+00 81.00 32.90 -3.77E-01 2.01E-01 276.40 7.16 1.61E-01 5.40E-01 302.85 18.34 1.10E-01 2.10E-01 356.01 62.05 -8.97E-03 8.89E-02 383.85 8.94 -5.05E-02 4.08E-01 Cs-134 475.36 1.48 1.34E+00 5.95E-02 2.76E+00 563.25 8.34 -5.84E-02 4.40E-01 569.33 15.37 6.67E-02 2.38E-01 604.72 97.62 7.29E-03 6.77E-02 795.86 85.46 2.34E-02 5.95E-02 801.95 8.69 -4.40E-01 4.33E-01 1038.61 0.99 1.04E+00 5.22E+00 1167.97 1.79 -5.08E+00 3.81E+00 1365.19 3.02 -6.90E-02 1.39E+00
| |
| + Cs-137 661.66
| |
| * 85.10 1.41E-01 4.32E-02 4.32E-02 Eu-152 121.78 28.67 3.27E-02 1.36E-01 1.36E-01 244.70 7.61 -2.23E-01 5.42E-01 295.94 0.45 6.21E+00 1.03E+01 344.28 26.60 -7.97E-02 1.54E-01 367.79 0.86 -2.41E+00 3.83E+00 411.12 2.24 7.07E-01 1.79E+00 443.96 2.83 -1.59E-01 1.35E+00 488.68 0.42 4.99E+00 9.67E+00 563.99 0.49 6.88E-01 7.38E+00 586.26 0.46 -2.75E+00 1.35E+01 678.62 0.47 3.62E+00 8.38E+00 688.67 0.86 6.54E-01 4.53E+00 719.35 0.28 5.07E-01 1.66E+01 778.90 12.96 -2.62E-01 3.04E-01 810.45 0.32 -2.05E+00 1.33E+01 867.37 4.26 3.45E-02 1.05E+00 919.33 0.43 -3.52E-01 1.17E+01 964.08 14.65 1.09E-01 4.41E-01 1085.87 10.24 -2.99E-02 5.86E-01 1089.74 1.73 2.36E+00 3.68E+00 1112.07 13.69 -1.53E-01 4.75E-01 1212.95 1.43 -8.42E-01 4.47E+00 1249.94 0.19 5.53E+00 3.23E+01 1299.14 1.63 -2.99E-01 3.67E+00 1408.01 21.07 1.41E-02 2.14E-01 1457.64 0.50 -2.51E+00 4.27E+01 1528.10 0.28 -4.13E+00 1.17E+01 Eu-154 123.07 40.40 1.17E-02 9.45E-02 9.45E-02 247.93 6.89 1.61E-01 5.35E-01 591.76 4.95 -3.41E-01 8.06E-01 692.42 1.78 5.60E-01 2.54E+00 723.30 20.06 7.21E-02 2.51E-01 756.80 4.52 4.37E-01 9.95E-01 873.18 12.08 3.11E-02 4.09E-01
| |
| [166]
| |
| | |
| 6/12/2019 1:35:24PM Page 7 of 7 Analysis Report for 12-Jun-19-10027 L1-10221C-FSGS-013SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 9.31E-02 9.45E-02 5.47E-01 1004.76 18.01 2.15E-01 3.35E-01 1274.43 34.80 -6.35E-02 1.67E-01 1596.48 1.80 -1.76E+00 1.90E+00 Eu-155 45.30 1.31 -1.62E+00 2.07E-01 1.28E+01 60.01 1.22 -4.27E-01 1.41E+01 86.55 30.70 2.01E-01 2.21E-01 105.31 21.10 -1.07E-02 2.07E-01 Ra-226 186.21 3.64 9.36E-01 1.17E+00 1.17E+00 Pa-231 27.36 10.30 6.32E-01 1.28E+00 1.28E+00 283.69 1.70 -8.58E-01 2.00E+00 300.07 2.47 -4.14E-01 1.56E+00 302.65 2.20 9.15E-01 1.75E+00 330.06 1.40 4.36E-01 2.80E+00 U-235 143.76 10.96 -6.11E-02 7.54E-02 3.09E-01 163.33 5.08 -2.15E-01 7.95E-01 185.71 57.20 6.46E-02 7.54E-02 202.11 1.08 9.18E-01 3.54E+00 205.31 5.01 -4.76E-01 7.57E-01 Am-241 59.54 35.90 2.17E-02 4.99E-01 4.99E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [167]
| |
| | |
| 6/12/2019 1:35:35PM Page 1 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10028 Sample Description : L1-10221C-FSGS-014SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.696E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:20:00AM Acquisition Started : 6/12/2019 1:20:22PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.8 seconds Dead Time : 0.20 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77309 Fill Height : 1696.06 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:35:26PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [168]
| |
| | |
| 6/12/2019 1:35:35PM Page 2 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.29 307 - 316 309.90 5.80E+01 15.91 8.60E+01 0.75 2 238.72 947 - 961 954.97 1.43E+02 21.32 1.08E+02 0.89 3 295.26 1174 - 1189 1180.93 7.61E+01 14.98 4.89E+01 0.51 4 352.08 1402 - 1416 1408.04 1.35E+02 15.42 3.58E+01 1.30 5 583.19 2324 - 2342 2331.97 7.98E+01 12.01 1.92E+01 1.15 6 609.54 2431 - 2445 2437.32 6.18E+01 11.74 2.63E+01 1.58 7 661.76 2638 - 2654 2646.15 2.43E+02 17.37 1.88E+01 1.39 8 1173.36 4685 - 4699 4692.63 4.63E+01 10.01 1.87E+01 0.85 9 1332.70 5323 - 5338 5330.27 4.45E+01 8.87 1.15E+01 0.52 10 1460.99 5832 - 5855 5843.79 4.00E+02 20.00 0.00E+00 1.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 9.70E+00 6.42E-01 Co-60 0.99 1173.23
| |
| * 99.85 1.03E-01 2.26E-02 1332.49
| |
| * 99.98 1.07E-01 2.18E-02 Cs-137 0.99 661.66
| |
| * 85.10 4.32E-01 4.03E-02 Tl-208 1.00 583.19
| |
| * 85.00 1.30E-01 2.11E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 2.51E-01 4.26E-02[169]
| |
| | |
| 6/12/2019 1:35:35PM Page 3 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-212 0.99 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77.11
| |
| * 17.10 6.98E-01 2.04E-01 87.35 3.97 89.78 1.46 Bi-214 0.99 609.32
| |
| * 45.49 1.94E-01 3.87E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 3.56E-01 7.57E-02 351.93
| |
| * 35.60 3.71E-01 5.17E-02 785.96 1.06 Pb214-XR 0.99 74.82 5.80 77.11
| |
| * 9.70 1.23E+00 3.65E-01 87.35 2.24 89.78 0.82
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [170]
| |
| | |
| 6/12/2019 1:35:35PM Page 4 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.995 9.70E+00 6.42E-01 Co-60 0.995 1.05E-01 1.57E-02 Cs-137 0.998 4.32E-01 4.03E-02 Tl-208 1.000 1.30E-01 2.11E-02 Pb-212 0.999 2.51E-01 4.26E-02
| |
| ? Pb212-XR 0.997 6.98E-01 2.04E-01 Bi-214 0.997 1.94E-01 3.87E-02 Pb-214 0.998 3.66E-01 4.27E-02
| |
| ? Pb214-XR 0.997 1.23E+00 3.65E-01
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [171]
| |
| | |
| 6/12/2019 1:35:35PM Page 5 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:35:26PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.72E-02 6.81E-02 6.81E-02 BE-7 477.60 10.44 2.85E-01 5.16E-01 5.16E-01
| |
| + K-40 1460.82
| |
| * 10.66 9.70E+00 6.97E-02 6.97E-02 Mn-54 834.85 99.98 -4.60E-03 5.38E-02 5.38E-02
| |
| + Co-60 1173.23
| |
| * 99.85 1.03E-01 5.48E-02 6.17E-02 1332.49
| |
| * 99.98 1.07E-01 5.48E-02 Nb-94 702.65 99.81 -1.07E-02 5.80E-02 5.80E-02 871.09 99.89 3.71E-02 5.82E-02 Ag-108m 79.13 6.60 -5.69E-01 5.56E-02 2.20E+00 433.94 90.50 1.59E-02 5.56E-02 614.28 89.80 -3.59E-02 7.86E-02 722.94 90.80 5.26E-03 6.67E-02 Sb-125 176.31 6.84 -5.44E-01 1.67E-01 6.68E-01 380.45 1.52 1.63E+00 3.23E+00 427.87 29.60 -9.78E-03 1.67E-01 463.36 10.49 1.77E-01 5.35E-01 600.60 17.65 1.90E-01 2.87E-01 606.71 4.98 -6.13E-01 1.50E+00 635.95 11.22 9.19E-02 4.65E-01 [172]
| |
| | |
| 6/12/2019 1:35:35PM Page 6 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 2.21E-01 1.67E-01 2.96E+00 Ba-133 79.61 2.65 -5.88E-01 9.91E-02 5.37E+00 81.00 32.90 -2.34E-01 3.62E-01 276.40 7.16 -1.13E-01 6.33E-01 302.85 18.34 -5.35E-02 2.54E-01 356.01 62.05 -2.01E-02 9.91E-02 383.85 8.94 -2.84E-02 5.51E-01 Cs-134 475.36 1.48 1.30E+00 6.43E-02 3.58E+00 563.25 8.34 -3.16E-01 5.15E-01 569.33 15.37 1.44E-01 3.42E-01 604.72 97.62 -3.38E-02 6.43E-02 795.86 85.46 4.43E-02 6.95E-02 801.95 8.69 4.45E-02 6.02E-01 1038.61 0.99 3.00E+00 7.03E+00 1167.97 1.79 -1.96E+00 5.69E+00 1365.19 3.02 -1.43E-01 1.53E+00
| |
| + Cs-137 661.66
| |
| * 85.10 4.32E-01 5.11E-02 5.11E-02 Eu-152 121.78 28.67 -9.69E-02 1.66E-01 1.82E-01 244.70 7.61 1.05E-01 6.75E-01 295.94 0.45 6.77E+00 1.29E+01 344.28 26.60 5.03E-02 1.66E-01 367.79 0.86 -6.46E-01 5.07E+00 411.12 2.24 9.26E-03 2.22E+00 443.96 2.83 -4.50E-01 1.84E+00 488.68 0.42 4.08E+00 1.14E+01 563.99 0.49 -3.54E+00 8.96E+00 586.26 0.46 -9.81E-01 1.69E+01 678.62 0.47 7.53E+00 1.16E+01 688.67 0.86 -2.07E+00 6.07E+00 719.35 0.28 -8.32E+00 1.94E+01 778.90 12.96 3.60E-02 3.67E-01 810.45 0.32 -1.25E+01 1.52E+01 867.37 4.26 -1.84E-01 1.44E+00 919.33 0.43 2.35E+00 1.34E+01 964.08 14.65 4.02E-01 5.11E-01 1085.87 10.24 -1.91E-01 6.91E-01 1089.74 1.73 -3.10E-01 3.86E+00 1112.07 13.69 -1.26E-01 4.76E-01 1212.95 1.43 1.97E+00 5.68E+00 1249.94 0.19 1.28E+01 4.01E+01 1299.14 1.63 -7.33E-01 4.06E+00 1408.01 21.07 -8.05E-02 2.41E-01 1457.64 0.50 1.96E+02 5.08E+01 1528.10 0.28 -1.09E+01 1.71E+01 Eu-154 123.07 40.40 -9.02E-02 1.28E-01 1.28E-01 247.93 6.89 5.16E-02 6.68E-01 591.76 4.95 8.94E-01 1.14E+00 692.42 1.78 1.23E+00 2.91E+00 723.30 20.06 1.71E-01 3.13E-01 756.80 4.52 4.35E-01 1.24E+00 873.18 12.08 -5.75E-01 4.12E-01
| |
| [173]
| |
| | |
| 6/12/2019 1:35:35PM Page 7 of 7 Analysis Report for 12-Jun-19-10028 L1-10221C-FSGS-014SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -2.32E-01 1.28E-01 5.70E-01 1004.76 18.01 1.95E-01 3.69E-01 1274.43 34.80 -1.13E-01 1.67E-01 1596.48 1.80 7.86E-01 2.78E+00 Eu-155 45.30 1.31 1.43E+01 3.24E-01 4.00E+01 60.01 1.22 1.07E-01 3.88E+01 86.55 30.70 1.31E-01 3.39E-01 105.31 21.10 -1.49E-01 3.24E-01 Ra-226 186.21 3.64 -3.59E-01 1.43E+00 1.43E+00 Pa-231 27.36 10.30 4.10E+00 1.95E+00 4.45E+00 283.69 1.70 1.33E+00 2.80E+00 300.07 2.47 -1.19E-01 1.95E+00 302.65 2.20 8.32E-01 2.13E+00 330.06 1.40 6.85E-01 3.62E+00 U-235 143.76 10.96 2.50E-01 8.98E-02 4.82E-01 163.33 5.08 -3.22E-01 9.08E-01 185.71 57.20 4.55E-03 8.98E-02 202.11 1.08 3.68E+00 4.70E+00 205.31 5.01 -5.07E-01 9.19E-01 Am-241 59.54 35.90 -4.11E-01 1.36E+00 1.36E+00
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [174]
| |
| | |
| 6/12/2019 1:35:55PM Page 1 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10029 Sample Description : L1-10221C-FSGS-015SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.635E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:25:00AM Acquisition Started : 6/12/2019 1:20:29PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77310 Fill Height : 1634.99 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:35:48PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [175]
| |
| | |
| 6/12/2019 1:35:55PM Page 2 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 186.35 741 - 751 745.27 3.13E+01 11.89 4.57E+01 0.91 2 238.75 948 - 960 954.59 1.47E+02 18.40 7.29E+01 0.84 3 295.36 1171 - 1186 1180.72 6.90E+01 12.13 2.60E+01 0.87 4 351.97 1399 - 1414 1406.89 1.05E+02 12.87 2.01E+01 1.31 5 463.19 1846 - 1855 1851.31 2.01E+01 6.71 1.09E+01 0.67 6 582.92 2323 - 2338 2329.80 5.12E+01 9.62 1.38E+01 1.28 7 609.28 2429 - 2442 2435.16 6.58E+01 10.09 1.32E+01 1.12 8 911.29 3637 - 3649 3642.63 2.20E+01 7.53 1.30E+01 0.34 9 1460.39 5826 - 5852 5839.48 4.17E+02 21.14 6.75E+00 1.82 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82
| |
| * 10.66 9.19E+00 6.13E-01 Sb-125 0.42 176.31 6.84 380.45 1.52 427.87 29.60 463.36
| |
| * 10.49 2.06E-01 7.06E-02 600.60 17.65 606.71 4.98 635.95 11.22 [176]
| |
| | |
| 6/12/2019 1:35:55PM Page 3 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Sb-125 0.42 671.44 1.79 Tl-208 0.98 583.19
| |
| * 85.00 7.58E-02 1.50E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 2.31E-01 3.44E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.88E-01 3.09E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 2.91E-01 5.63E-02 351.93
| |
| * 35.60 2.61E-01 3.82E-02 785.96 1.06 Ra-226 0.99 186.21
| |
| * 3.64 5.17E-01 2.01E-01 Ac-228 0.48 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00
| |
| * 4.40 4.91E-01 1.68E-01 794.95 4.25 911.20
| |
| * 25.80 1.45E-01 5.02E-02 964.77 4.99 968.97 15.80 1588.20 3.22 U-235 0.95 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 3.29E-02 1.28E-02 202.11 1.08 205.31 5.01
| |
| [177]
| |
| | |
| 6/12/2019 1:35:55PM Page 4 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.970 9.19E+00 6.13E-01 Sb-125 0.420 1.45E-01 7.37E-02 Tl-208 0.989 7.58E-02 1.50E-02 X Bi-211 0.878 Pb-212 0.998 2.31E-01 3.44E-02 Bi-214 1.000 1.88E-01 3.09E-02 Pb-214 0.999 2.70E-01 3.16E-02
| |
| ? Ra-226 0.997 5.17E-01 2.01E-01 Ac-228 0.483 1.45E-01 5.01E-02
| |
| ? U-235 0.955 3.29E-02 1.28E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [178]
| |
| | |
| 6/12/2019 1:35:55PM Page 5 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:35:48PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 9.50E-02 5.81E-02 5.81E-02 BE-7 477.60 10.44 2.29E-01 3.67E-01 3.67E-01
| |
| + K-40 1460.82
| |
| * 10.66 9.19E+00 4.69E-01 4.69E-01 Mn-54 834.85 99.98 -2.70E-02 4.96E-02 4.96E-02 Co-60 1173.23 99.85 2.33E-02 5.09E-02 6.39E-02 1332.49 99.98 -1.64E-02 5.09E-02 Nb-94 702.65 99.81 -1.72E-02 4.19E-02 4.65E-02 871.09 99.89 -2.29E-03 4.19E-02 Ag-108m 79.13 6.60 1.65E+00 4.10E-02 1.35E+00 433.94 90.50 4.63E-03 4.10E-02 614.28 89.80 -4.01E-03 5.87E-02 722.94 90.80 2.51E-02 5.39E-02
| |
| + Sb-125 176.31 6.84 4.17E-01 1.24E-01 4.66E-01 380.45 1.52 1.03E-01 2.29E+00 427.87 29.60 2.87E-04 1.24E-01 463.36
| |
| * 10.49 2.06E-01 2.04E-01 600.60 17.65 6.11E-02 2.19E-01 606.71 4.98 2.00E+00 1.34E+00 635.95 11.22 1.54E-01 3.53E-01 [179]
| |
| | |
| 6/12/2019 1:35:55PM Page 6 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 2.90E-01 1.24E-01 2.19E+00 Ba-133 79.61 2.65 3.39E+00 6.89E-02 3.22E+00 81.00 32.90 -3.73E-01 2.03E-01 276.40 7.16 1.26E-01 4.81E-01 302.85 18.34 1.80E-01 2.12E-01 356.01 62.05 -6.34E-03 6.89E-02 383.85 8.94 6.39E-02 3.81E-01 Cs-134 475.36 1.48 -9.81E-01 5.54E-02 2.50E+00 563.25 8.34 3.12E-02 5.39E-01 569.33 15.37 2.60E-02 2.71E-01 604.72 97.62 -2.90E-02 5.92E-02 795.86 85.46 2.28E-02 5.54E-02 801.95 8.69 3.40E-01 5.63E-01 1038.61 0.99 -1.43E+00 5.05E+00 1167.97 1.79 -1.25E+00 3.51E+00 1365.19 3.02 4.91E-01 1.49E+00 Cs-137 661.66 85.10 4.24E-02 5.72E-02 5.72E-02 Eu-152 121.78 28.67 2.61E-02 1.15E-01 1.15E-01 244.70 7.61 1.20E-01 5.04E-01 295.94 0.45 5.11E+00 9.83E+00 344.28 26.60 -8.29E-03 1.23E-01 367.79 0.86 1.91E-01 3.97E+00 411.12 2.24 -6.53E-01 1.52E+00 443.96 2.83 -5.48E-01 9.92E-01 488.68 0.42 3.22E+00 8.63E+00 563.99 0.49 -9.93E+00 8.43E+00 586.26 0.46 -1.37E+00 1.27E+01 678.62 0.47 2.62E+00 9.61E+00 688.67 0.86 -1.78E+00 4.57E+00 719.35 0.28 -4.20E-01 1.54E+01 778.90 12.96 -2.07E-01 2.81E-01 810.45 0.32 -1.03E+01 1.34E+01 867.37 4.26 -1.42E-01 1.07E+00 919.33 0.43 4.67E+00 1.11E+01 964.08 14.65 4.16E-01 4.77E-01 1085.87 10.24 -5.38E-02 5.61E-01 1089.74 1.73 -2.02E-01 3.38E+00 1112.07 13.69 2.49E-02 3.75E-01 1212.95 1.43 -5.77E-01 5.06E+00 1249.94 0.19 -8.61E-01 3.24E+01 1299.14 1.63 4.77E+00 4.20E+00 1408.01 21.07 1.73E-01 2.39E-01 1457.64 0.50 1.93E+02 4.75E+01 1528.10 0.28 6.90E+00 1.42E+01 Eu-154 123.07 40.40 1.79E-02 8.01E-02 8.01E-02 247.93 6.89 -3.52E-01 4.60E-01 591.76 4.95 4.48E-01 7.83E-01 692.42 1.78 -3.59E-01 2.32E+00 723.30 20.06 3.30E-02 2.44E-01 756.80 4.52 -9.95E-02 9.25E-01 873.18 12.08 -2.50E-01 3.48E-01
| |
| [180]
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| | |
| 6/12/2019 1:35:55PM Page 7 of 7 Analysis Report for 12-Jun-19-10029 L1-10221C-FSGS-015SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 6.48E-03 8.01E-02 4.88E-01 1004.76 18.01 6.91E-03 2.95E-01 1274.43 34.80 -1.14E-01 1.58E-01 1596.48 1.80 2.35E-01 2.91E+00 Eu-155 45.30 1.31 -5.30E+00 1.94E-01 1.12E+01 60.01 1.22 7.21E-01 1.29E+01 86.55 30.70 1.01E-03 1.94E-01 105.31 21.10 -8.78E-02 2.07E-01
| |
| + Ra-226 186.21
| |
| * 3.64 5.17E-01 6.36E-01 6.36E-01 Pa-231 27.36 10.30 1.06E+00 1.29E+00 1.29E+00 283.69 1.70 -9.38E-01 1.87E+00 300.07 2.47 -5.26E-01 1.47E+00 302.65 2.20 1.82E+00 1.80E+00 330.06 1.40 3.88E-01 2.59E+00
| |
| + U-235 143.76 10.96 9.97E-02 4.05E-02 3.12E-01 163.33 5.08 2.62E-01 6.67E-01 185.71
| |
| * 57.20 3.29E-02 4.05E-02 202.11 1.08 5.77E-01 3.28E+00 205.31 5.01 -2.15E-01 6.66E-01 Am-241 59.54 35.90 -7.55E-02 4.57E-01 4.57E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [181]
| |
| | |
| 6/12/2019 1:57:52PM Page 1 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10030 Sample Description : L1-10221C-FSGS-016SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.527E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:30:00AM Acquisition Started : 6/12/2019 1:42:42PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.04 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77311 Fill Height : 1526.95 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:57:45PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [182]
| |
| | |
| 6/12/2019 1:57:52PM Page 2 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.64 473 - 481 477.46 1.13E+02 19.92 1.29E+02 1.13 2 338.58 675 - 680 677.12 2.47E+01 9.10 3.23E+01 1.18 3 352.04 699 - 708 704.01 8.63E+01 12.74 3.37E+01 1.63 4 583.33 1160 - 1170 1166.27 4.38E+01 10.75 3.03E+01 1.40 5 609.25 1213 - 1223 1218.07 8.80E+01 12.17 2.50E+01 1.50 6 911.27 1818 - 1828 1821.99 3.98E+01 8.59 1.42E+01 0.87 7 968.72 1934 - 1942 1936.91 2.02E+01 7.93 1.98E+01 1.20 8 1460.91 2914 - 2929 2921.87 3.31E+02 18.36 2.02E+00 2.14 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 6.23E+00 4.39E-01 Tl-208 0.99 583.19
| |
| * 85.00 5.64E-02 1.43E-02 Bi-211 0.86 351.07
| |
| * 13.02 5.17E-01 8.70E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.59E-01 3.08E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 2.18E-01 3.29E-02 768.36 4.89 806.18 1.26 [183]
| |
| | |
| 6/12/2019 1:57:52PM Page 3 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.89E-01 3.18E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 1.67E-01 6.28E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 2.27E-01 4.99E-02 964.77 4.99 968.97
| |
| * 15.80 1.95E-01 7.72E-02 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [184]
| |
| | |
| 6/12/2019 1:57:52PM Page 4 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 6.23E+00 4.39E-01 Tl-208 0.997 5.64E-02 1.43E-02
| |
| ? Bi-211 0.862 5.17E-01 8.70E-02 Pb-212 1.000 1.59E-01 3.08E-02 Bi-214 1.000 2.18E-01 3.29E-02
| |
| ? Pb-214 0.999 1.89E-01 3.18E-02 Ac-228 0.997 2.02E-01 3.49E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [185]
| |
| | |
| 6/12/2019 1:57:52PM Page 5 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:57:45PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.30E-02 5.18E-02 5.18E-02 BE-7 477.60 10.44 1.92E-01 3.68E-01 3.68E-01
| |
| + K-40 1460.82
| |
| * 10.66 6.23E+00 2.12E-01 2.12E-01 Mn-54 834.85 99.98 -2.91E-02 4.29E-02 4.29E-02 Co-60 1173.23 99.85 1.68E-02 5.70E-02 5.81E-02 1332.49 99.98 2.67E-02 5.70E-02 Nb-94 702.65 99.81 -1.58E-02 3.39E-02 3.62E-02 871.09 99.89 -6.77E-03 3.39E-02 Ag-108m 79.13 6.60 5.06E-01 3.73E-02 1.19E+00 433.94 90.50 -7.16E-03 3.73E-02 614.28 89.80 -1.87E-02 5.32E-02 722.94 90.80 -2.83E-02 4.17E-02 Sb-125 176.31 6.84 1.96E-01 1.24E-01 5.14E-01 380.45 1.52 1.07E+00 2.19E+00 427.87 29.60 3.49E-03 1.24E-01 463.36 10.49 -9.92E-02 2.98E-01 600.60 17.65 8.69E-02 2.27E-01 606.71 4.98 -3.39E-01 1.31E+00 635.95 11.22 -8.33E-02 3.02E-01 [186]
| |
| | |
| 6/12/2019 1:57:52PM Page 6 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.36E+00 1.24E-01 2.21E+00 Ba-133 79.61 2.65 1.67E-01 6.69E-02 2.73E+00 81.00 32.90 -1.78E-01 1.88E-01 276.40 7.16 -8.18E-02 4.41E-01 302.85 18.34 1.23E-01 1.82E-01 356.01 62.05 -4.88E-02 6.69E-02 383.85 8.94 -1.23E-02 3.63E-01 Cs-134 475.36 1.48 1.05E+00 4.72E-02 2.66E+00 563.25 8.34 -1.16E-01 4.02E-01 569.33 15.37 8.64E-02 2.39E-01 604.72 97.62 -2.30E-02 5.85E-02 795.86 85.46 3.22E-02 4.72E-02 801.95 8.69 -1.24E-01 4.25E-01 1038.61 0.99 6.23E-02 5.05E+00 1167.97 1.79 -2.31E+00 2.97E+00 1365.19 3.02 1.98E-01 1.23E+00 Cs-137 661.66 85.10 5.17E-02 6.02E-02 6.02E-02 Eu-152 121.78 28.67 4.01E-03 1.06E-01 1.06E-01 244.70 7.61 1.57E-02 4.90E-01 295.94 0.45 3.36E+00 8.78E+00 344.28 26.60 -1.03E-01 1.22E-01 367.79 0.86 -1.25E-01 3.59E+00 411.12 2.24 -8.80E-01 1.39E+00 443.96 2.83 -1.82E-01 1.06E+00 488.68 0.42 -4.06E-01 8.14E+00 563.99 0.49 -1.90E+00 6.91E+00 586.26 0.46 -4.11E+00 1.13E+01 678.62 0.47 -3.89E+00 7.48E+00 688.67 0.86 1.84E+00 4.99E+00 719.35 0.28 2.17E+00 1.33E+01 778.90 12.96 -1.43E-01 3.15E-01 810.45 0.32 -8.27E-01 1.18E+01 867.37 4.26 -6.46E-01 8.11E-01 919.33 0.43 -4.99E+00 8.02E+00 964.08 14.65 -3.02E-01 3.79E-01 1085.87 10.24 2.92E-02 4.54E-01 1089.74 1.73 1.45E+00 3.05E+00 1112.07 13.69 6.09E-02 3.44E-01 1212.95 1.43 -9.07E-01 4.29E+00 1249.94 0.19 -3.01E+00 2.93E+01 1299.14 1.63 1.79E+00 3.31E+00 1408.01 21.07 7.18E-02 1.93E-01 1457.64 0.50 0.00E+00 3.59E+01 1528.10 0.28 2.42E+00 1.08E+01 Eu-154 123.07 40.40 -2.81E-02 7.32E-02 7.32E-02 247.93 6.89 2.81E-02 4.84E-01 591.76 4.95 -1.70E-01 6.81E-01 692.42 1.78 2.37E-01 2.19E+00 723.30 20.06 -6.29E-03 2.02E-01 756.80 4.52 2.53E-01 8.26E-01 873.18 12.08 1.18E-02 2.87E-01
| |
| [187]
| |
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| 6/12/2019 1:57:52PM Page 7 of 7 Analysis Report for 12-Jun-19-10030 L1-10221C-FSGS-016SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -8.62E-03 7.32E-02 4.20E-01 1004.76 18.01 3.25E-02 2.50E-01 1274.43 34.80 -5.55E-02 9.83E-02 1596.48 1.80 -1.37E+00 1.49E+00 Eu-155 45.30 1.31 -1.49E+00 1.76E-01 1.22E+01 60.01 1.22 1.19E-01 1.27E+01 86.55 30.70 -3.44E-02 1.76E-01 105.31 21.10 3.84E-02 1.88E-01 Ra-226 186.21 3.64 1.99E-01 9.75E-01 9.75E-01 Pa-231 27.36 10.30 5.64E-01 1.10E+00 1.10E+00 283.69 1.70 4.20E-01 1.92E+00 300.07 2.47 -1.43E+00 1.34E+00 302.65 2.20 1.02E+00 1.52E+00 330.06 1.40 9.90E-01 2.73E+00 U-235 143.76 10.96 -1.77E-02 6.32E-02 2.89E-01 163.33 5.08 3.51E-02 6.81E-01 185.71 57.20 2.57E-02 6.32E-02 202.11 1.08 7.20E-01 3.18E+00 205.31 5.01 -2.37E-01 6.91E-01 Am-241 59.54 35.90 -1.26E-01 4.22E-01 4.22E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [188]
| |
| | |
| 6/12/2019 1:58:00PM Page 1 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS GAMMA SPECTRUM ANALYSIS Sample Identification : 12-Jun-19-10031 Sample Description : L1-10221C-FSGS-017SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.558E+03 grams Facility : Default Sample Taken On : 6/11/2019 9:35:00AM Acquisition Started : 6/12/2019 1:42:49PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.5 seconds Dead Time : 0.16 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/12/2019 Efficiency Calibration Description :
| |
| Sample Number : 77312 Fill Height : 1558.30 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/12/2019 1:57:53PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [189]
| |
| | |
| 6/12/2019 1:58:00PM Page 2 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.11 306 - 314 309.16 3.15E+01 12.99 6.35E+01 0.67 2 186.03 741 - 749 744.41 4.37E+01 12.75 5.53E+01 0.99 3 238.66 947 - 961 954.72 1.30E+02 20.77 1.05E+02 0.68 4 295.19 1173 - 1188 1180.65 4.64E+01 14.18 5.06E+01 1.04 5 351.87 1402 - 1413 1407.23 1.05E+02 13.49 3.05E+01 1.35 6 510.91 2038 - 2048 2043.00 1.86E+01 9.15 2.74E+01 0.54 7 583.16 2327 - 2339 2331.86 4.52E+01 10.03 2.08E+01 1.05 8 609.20 2430 - 2441 2435.97 6.66E+01 10.01 1.34E+01 1.12 9 911.68 3639 - 3652 3645.67 4.12E+01 7.74 6.78E+00 0.44 10 1460.91 5832 - 5855 5843.46 3.41E+02 19.15 6.27E+00 1.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 0.99 511.00
| |
| * 100.00 2.44E-02 1.21E-02 K-40 0.99 1460.82
| |
| * 10.66 8.45E+00 6.00E-01 Tl-208 1.00 583.19
| |
| * 85.00 7.51E-02 1.73E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 2.32E-01 4.15E-02 300.09 3.30 Pb212-XR 1.00 74.82 10.28 [190]
| |
| | |
| 6/12/2019 1:58:00PM Page 3 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb212-XR 1.00 77.11
| |
| * 17.10 3.85E-01 1.64E-01 87.35 3.97 89.78 1.46 Bi-214 0.99 609.32
| |
| * 45.49 2.13E-01 3.45E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 2.20E-01 6.96E-02 351.93
| |
| * 35.60 2.91E-01 4.43E-02 785.96 1.06 Pb214-XR 1.00 74.82 5.80 77.11
| |
| * 9.70 6.79E-01 2.90E-01 87.35 2.24 89.78 0.82 Ra-226 0.99 186.21
| |
| * 3.64 8.31E-01 2.52E-01 Ac-228 0.98 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 3.06E-01 5.89E-02 964.77 4.99 968.97 15.80 1588.20 3.22 U-235 0.98 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 5.29E-02 1.60E-02 202.11 1.08 205.31 5.01
| |
| [191]
| |
| | |
| 6/12/2019 1:58:00PM Page 4 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| An Pk 0.999 2.44E-02 1.21E-02 K-40 0.999 8.45E+00 6.00E-01 Tl-208 1.000 7.51E-02 1.73E-02 X Bi-211 0.902 Pb-212 1.000 2.32E-01 4.15E-02
| |
| ? Pb212-XR 1.000 3.85E-01 1.64E-01 Bi-214 0.999 2.13E-01 3.45E-02 Pb-214 1.000 2.71E-01 3.73E-02
| |
| ? Pb214-XR 1.000 6.79E-01 2.90E-01
| |
| ? Ra-226 0.995 8.31E-01 2.52E-01 Ac-228 0.989 3.06E-01 5.89E-02
| |
| ? U-235 0.989 5.29E-02 1.60E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [192]
| |
| | |
| 6/12/2019 1:58:00PM Page 5 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/12/2019 1:57:53PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 2.44E-02 3.97E-02 3.97E-02 BE-7 477.60 10.44 -5.90E-02 4.41E-01 4.41E-01
| |
| + K-40 1460.82
| |
| * 10.66 8.45E+00 5.01E-01 5.01E-01 Mn-54 834.85 99.98 1.66E-02 5.64E-02 5.64E-02 Co-60 1173.23 99.85 7.14E-03 6.38E-02 7.09E-02 1332.49 99.98 1.06E-02 6.38E-02 Nb-94 702.65 99.81 3.76E-02 5.15E-02 5.57E-02 871.09 99.89 -1.06E-02 5.15E-02 Ag-108m 79.13 6.60 4.93E-01 4.98E-02 1.97E+00 433.94 90.50 5.73E-03 4.98E-02 614.28 89.80 -8.14E-02 6.82E-02 722.94 90.80 1.43E-02 6.31E-02 Sb-125 176.31 6.84 -1.97E-01 1.43E-01 6.11E-01 380.45 1.52 1.30E+00 2.77E+00 427.87 29.60 -1.07E-01 1.43E-01 463.36 10.49 1.13E-01 5.18E-01 600.60 17.65 -6.64E-02 2.59E-01 606.71 4.98 1.68E+00 1.52E+00 635.95 11.22 -1.02E-01 4.01E-01 [193]
| |
| | |
| 6/12/2019 1:58:00PM Page 6 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -8.68E-01 1.43E-01 2.57E+00 Ba-133 79.61 2.65 1.33E+00 8.87E-02 4.72E+00 81.00 32.90 1.16E-01 3.15E-01 276.40 7.16 3.00E-01 6.24E-01 302.85 18.34 8.78E-03 2.33E-01 356.01 62.05 -1.13E-01 8.87E-02 383.85 8.94 2.37E-01 4.62E-01 Cs-134 475.36 1.48 2.32E+00 5.68E-02 3.20E+00 563.25 8.34 2.40E-01 5.04E-01 569.33 15.37 -3.25E-02 2.60E-01 604.72 97.62 -3.37E-02 7.29E-02 795.86 85.46 1.20E-02 5.68E-02 801.95 8.69 -9.67E-02 5.52E-01 1038.61 0.99 -2.84E-01 6.07E+00 1167.97 1.79 1.98E+00 4.10E+00 1365.19 3.02 1.17E+00 1.73E+00 Cs-137 661.66 85.10 9.70E-04 7.02E-02 7.02E-02 Eu-152 121.78 28.67 1.20E-01 1.58E-01 1.83E-01 244.70 7.61 3.19E-02 6.21E-01 295.94 0.45 9.62E+00 1.17E+01 344.28 26.60 4.41E-02 1.58E-01 367.79 0.86 -1.12E+00 4.38E+00 411.12 2.24 -6.25E-01 1.76E+00 443.96 2.83 -3.58E-01 1.49E+00 488.68 0.42 -5.96E-01 9.07E+00 563.99 0.49 3.93E+00 8.56E+00 586.26 0.46 1.13E+01 1.48E+01 678.62 0.47 -6.33E+00 1.06E+01 688.67 0.86 -1.90E+00 5.76E+00 719.35 0.28 -6.60E+00 1.80E+01 778.90 12.96 -2.20E-01 3.50E-01 810.45 0.32 7.04E+00 1.55E+01 867.37 4.26 -1.49E-01 1.28E+00 919.33 0.43 -8.70E+00 1.23E+01 964.08 14.65 1.74E-01 4.40E-01 1085.87 10.24 1.26E-01 5.54E-01 1089.74 1.73 -1.36E+00 3.23E+00 1112.07 13.69 1.56E-01 4.44E-01 1212.95 1.43 4.19E+00 4.73E+00 1249.94 0.19 -4.37E+00 3.17E+01 1299.14 1.63 -4.03E+00 3.93E+00 1408.01 21.07 5.76E-02 2.11E-01 1457.64 0.50 1.85E+02 4.90E+01 1528.10 0.28 2.67E+00 1.60E+01 Eu-154 123.07 40.40 -6.53E-02 1.24E-01 1.24E-01 247.93 6.89 1.62E-02 5.77E-01 591.76 4.95 5.31E-01 8.89E-01 692.42 1.78 2.23E-02 2.64E+00 723.30 20.06 4.89E-02 2.92E-01 756.80 4.52 1.23E+00 1.28E+00 873.18 12.08 1.43E-01 4.27E-01
| |
| [194]
| |
| | |
| 6/12/2019 1:58:00PM Page 7 of 7 Analysis Report for 12-Jun-19-10031 L1-10221C-FSGS-017SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.15E-01 1.24E-01 5.48E-01 1004.76 18.01 1.41E-01 3.77E-01 1274.43 34.80 -5.84E-02 1.56E-01 1596.48 1.80 -5.91E-02 2.31E+00 Eu-155 45.30 1.31 1.00E+01 2.76E-01 3.36E+01 60.01 1.22 7.31E+00 3.18E+01 86.55 30.70 -2.75E-02 2.76E-01 105.31 21.10 3.11E-02 3.11E-01
| |
| + Ra-226 186.21
| |
| * 3.64 8.31E-01 7.58E-01 7.58E-01 Pa-231 27.36 10.30 2.79E+00 1.78E+00 3.55E+00 283.69 1.70 -8.55E-01 2.28E+00 300.07 2.47 9.02E-01 1.78E+00 302.65 2.20 2.64E-01 1.98E+00 330.06 1.40 1.65E+00 3.01E+00
| |
| + U-235 143.76 10.96 -7.92E-02 4.82E-02 4.08E-01 163.33 5.08 7.73E-02 8.76E-01 185.71
| |
| * 57.20 5.29E-02 4.82E-02 202.11 1.08 -1.84E+00 3.69E+00 205.31 5.01 -4.90E-01 8.35E-01 Am-241 59.54 35.90 1.34E-01 1.12E+00 1.12E+00
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [195]
| |
| | |
| 6/18/2019 11:23:30AM Page 1 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10030 Sample Description : L1-10221C-FJGS-001SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.518E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:12:00AM Acquisition Started : 6/18/2019 11:08:20AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77463 Fill Height : 1517.73 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 11:23:23AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [196]
| |
| | |
| 6/18/2019 11:23:30AM Page 2 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.60 472 - 481 477.38 1.01E+02 16.45 7.38E+01 1.21 2 351.89 698 - 708 703.72 5.34E+01 11.75 3.56E+01 1.05 3 510.54 1016 - 1026 1020.76 3.64E+01 10.24 2.86E+01 0.74 4 583.20 1163 - 1171 1166.01 4.54E+01 8.38 1.16E+01 1.41 5 911.70 1819 - 1828 1822.84 3.30E+01 7.22 7.96E+00 1.38 6 1461.13 2916 - 2928 2922.31 2.03E+02 14.82 6.50E+00 1.72 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 0.96 511.00
| |
| * 100.00 3.72E-02 1.08E-02 K-40 0.98 1460.82
| |
| * 10.66 3.82E+00 3.25E-01 Tl-208 1.00 583.19
| |
| * 85.00 5.86E-02 1.14E-02 Bi-211 0.89 351.07
| |
| * 13.02 3.21E-01 7.51E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.42E-01 2.58E-02 300.09 3.30 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.17E-01 2.74E-02 785.96 1.06 [197]
| |
| | |
| 6/18/2019 11:23:30AM Page 3 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Ac-228 0.98 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.89E-01 4.20E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| An Pk 0.966 3.72E-02 1.08E-02 K-40 0.985 3.82E+00 3.25E-01 Tl-208 1.000 5.86E-02 1.14E-02
| |
| ? Bi-211 0.899 3.21E-01 7.51E-02 Pb-212 1.000 1.42E-01 2.58E-02
| |
| ? Pb-214 1.000 1.17E-01 2.74E-02 Ac-228 0.988 1.89E-01 4.20E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [198]
| |
| | |
| 6/18/2019 11:23:30AM Page 4 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 11:23:23AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 3.72E-02 3.16E-02 3.16E-02 BE-7 477.60 10.44 5.71E-02 3.04E-01 3.04E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.82E+00 3.18E-01 3.18E-01 Mn-54 834.85 99.98 7.43E-03 3.53E-02 3.53E-02 Co-60 1173.23 99.85 8.17E-04 2.92E-02 4.81E-02 1332.49 99.98 -4.36E-03 2.92E-02 Nb-94 702.65 99.81 -1.23E-03 2.78E-02 2.96E-02 871.09 99.89 -6.31E-03 2.78E-02 Ag-108m 79.13 6.60 5.34E-01 2.37E-02 1.01E+00 433.94 90.50 -2.24E-02 2.37E-02 614.28 89.80 -2.97E-02 4.61E-02 722.94 90.80 5.74E-03 3.23E-02 Sb-125 176.31 6.84 -7.81E-02 9.07E-02 4.39E-01 380.45 1.52 5.26E-01 1.68E+00 427.87 29.60 3.08E-02 9.07E-02 463.36 10.49 4.58E-02 3.06E-01 600.60 17.65 8.55E-02 1.76E-01 606.71 4.98 1.05E+00 9.68E-01 635.95 11.22 6.82E-02 2.93E-01 [199]
| |
| | |
| 6/18/2019 11:23:30AM Page 5 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -2.84E-01 9.07E-02 1.96E+00 Ba-133 79.61 2.65 1.32E+00 5.57E-02 2.43E+00 81.00 32.90 -9.73E-02 1.57E-01 276.40 7.16 -1.85E-02 3.54E-01 302.85 18.34 5.76E-02 1.53E-01 356.01 62.05 -2.52E-03 5.57E-02 383.85 8.94 -4.21E-02 2.75E-01 Cs-134 475.36 1.48 7.87E-01 4.08E-02 2.11E+00 563.25 8.34 1.00E-01 3.58E-01 569.33 15.37 -1.92E-02 2.08E-01 604.72 97.62 -1.52E-02 4.08E-02 795.86 85.46 1.74E-02 4.59E-02 801.95 8.69 -7.99E-02 3.70E-01 1038.61 0.99 -1.31E+00 3.15E+00 1167.97 1.79 -1.68E+00 2.34E+00 1365.19 3.02 2.90E-01 9.87E-01 Cs-137 661.66 85.10 1.28E-02 4.66E-02 4.66E-02 Eu-152 121.78 28.67 -2.12E-02 9.29E-02 9.72E-02 244.70 7.61 -7.31E-02 3.76E-01 295.94 0.45 4.98E+00 8.03E+00 344.28 26.60 -1.06E-01 9.29E-02 367.79 0.86 -1.17E+00 3.11E+00 411.12 2.24 8.23E-03 1.28E+00 443.96 2.83 -4.92E-01 9.44E-01 488.68 0.42 -1.35E+00 6.99E+00 563.99 0.49 1.87E+00 6.18E+00 586.26 0.46 -3.79E+00 1.03E+01 678.62 0.47 1.50E+00 7.38E+00 688.67 0.86 -4.01E-01 3.39E+00 719.35 0.28 2.43E-01 9.11E+00 778.90 12.96 5.25E-02 2.70E-01 810.45 0.32 -1.94E+00 8.27E+00 867.37 4.26 -5.47E-01 5.49E-01 919.33 0.43 -4.27E+00 6.74E+00 964.08 14.65 -1.05E-01 2.70E-01 1085.87 10.24 -1.79E-01 4.00E-01 1089.74 1.73 1.15E+00 2.32E+00 1112.07 13.69 -3.74E-02 2.29E-01 1212.95 1.43 5.47E-01 2.95E+00 1249.94 0.19 7.66E+00 2.27E+01 1299.14 1.63 7.67E-01 2.29E+00 1408.01 21.07 1.04E-02 1.67E-01 1457.64 0.50 -6.68E+00 2.92E+01 1528.10 0.28 1.38E-01 9.19E+00 Eu-154 123.07 40.40 -3.35E-02 6.54E-02 6.54E-02 247.93 6.89 -3.24E-02 3.76E-01 591.76 4.95 -9.52E-02 6.43E-01 692.42 1.78 1.05E+00 1.76E+00 723.30 20.06 2.63E-02 1.46E-01 756.80 4.52 -3.58E-01 7.31E-01 873.18 12.08 8.87E-03 2.54E-01
| |
| [200]
| |
| | |
| 6/18/2019 11:23:30AM Page 6 of 6 Analysis Report for 18-Jun-19-10030 L1-10221C-FJGS-001SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -8.37E-02 6.54E-02 3.46E-01 1004.76 18.01 1.22E-01 2.16E-01 1274.43 34.80 -1.83E-02 9.05E-02 1596.48 1.80 4.48E-02 1.49E+00 Eu-155 45.30 1.31 -5.38E+00 1.42E-01 8.77E+00 60.01 1.22 2.86E+00 1.15E+01 86.55 30.70 -5.25E-03 1.42E-01 105.31 21.10 3.53E-02 1.62E-01 Ra-226 186.21 3.64 3.32E-01 8.93E-01 8.93E-01 Pa-231 27.36 10.30 4.28E-01 9.97E-01 9.97E-01 283.69 1.70 9.28E-01 1.67E+00 300.07 2.47 -1.09E+00 1.11E+00 302.65 2.20 4.80E-01 1.27E+00 330.06 1.40 -3.19E-01 2.01E+00 U-235 143.76 10.96 4.57E-02 5.62E-02 2.61E-01 163.33 5.08 -3.31E-01 5.96E-01 185.71 57.20 1.83E-02 5.62E-02 202.11 1.08 -2.86E-01 2.76E+00 205.31 5.01 -3.30E-01 5.50E-01 Am-241 59.54 35.90 8.21E-02 4.02E-01 4.02E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [201]
| |
| | |
| 6/18/2019 12:55:04PM Page 1 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10031 Sample Description : L1-10221C-QJGS-001SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.613E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:12:00AM Acquisition Started : 6/18/2019 12:39:54PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77473 Fill Height : 1612.68 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 12:54:57PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [202]
| |
| | |
| 6/18/2019 12:55:04PM Page 2 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.72 474 - 482 477.61 1.06E+02 16.41 7.58E+01 1.15 2 351.98 700 - 708 703.91 5.65E+01 10.43 2.45E+01 1.52 3 583.46 1160 - 1170 1166.52 2.67E+01 8.09 1.63E+01 1.02 4 609.28 1215 - 1223 1218.14 3.68E+01 8.35 1.52E+01 0.84 5 911.52 1819 - 1826 1822.50 2.21E+01 6.32 8.87E+00 1.69 6 1461.14 2915 - 2929 2922.34 1.62E+02 13.15 3.75E+00 2.16 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.98 1460.82
| |
| * 10.66 3.01E+00 2.77E-01 Tl-208 0.98 583.19
| |
| * 85.00 3.40E-02 1.05E-02 Bi-211 0.87 351.07
| |
| * 13.02 3.35E-01 6.75E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.48E-01 2.57E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 9.01E-02 2.12E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 [203]
| |
| | |
| 6/18/2019 12:55:04PM Page 3 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.23E-01 2.47E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.24E-01 3.59E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [204]
| |
| | |
| 6/18/2019 12:55:04PM Page 4 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.984 3.01E+00 2.77E-01 Tl-208 0.988 3.40E-02 1.05E-02
| |
| ? Bi-211 0.876 3.35E-01 6.75E-02 Pb-212 0.999 1.48E-01 2.57E-02 Bi-214 1.000 9.01E-02 2.12E-02
| |
| ? Pb-214 1.000 1.23E-01 2.47E-02 Ac-228 0.995 1.24E-01 3.59E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [205]
| |
| | |
| 6/18/2019 12:55:04PM Page 5 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 12:54:57PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 7.27E-02 4.80E-02 4.80E-02 BE-7 477.60 10.44 1.60E-01 2.73E-01 2.73E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.01E+00 2.60E-01 2.60E-01 Mn-54 834.85 99.98 -7.94E-03 2.67E-02 2.67E-02 Co-60 1173.23 99.85 -1.75E-02 4.08E-02 4.15E-02 1332.49 99.98 1.80E-02 4.08E-02 Nb-94 702.65 99.81 -8.97E-03 2.74E-02 3.63E-02 871.09 99.89 -8.80E-05 2.74E-02 Ag-108m 79.13 6.60 -5.17E-02 2.83E-02 9.51E-01 433.94 90.50 3.33E-03 2.83E-02 614.28 89.80 -1.53E-02 3.90E-02 722.94 90.80 -8.37E-03 3.94E-02 Sb-125 176.31 6.84 -1.26E-01 8.95E-02 4.37E-01 380.45 1.52 -4.00E-01 1.70E+00 427.87 29.60 -1.79E-02 8.95E-02 463.36 10.49 1.30E-01 2.55E-01 600.60 17.65 -5.09E-03 1.88E-01 606.71 4.98 -7.35E-01 9.74E-01 635.95 11.22 -1.79E-02 1.99E-01 [206]
| |
| | |
| 6/18/2019 12:55:04PM Page 6 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 2.66E-01 8.95E-02 1.75E+00 Ba-133 79.61 2.65 -2.19E-01 5.58E-02 2.27E+00 81.00 32.90 -7.82E-02 1.63E-01 276.40 7.16 1.85E-01 4.04E-01 302.85 18.34 3.45E-02 1.47E-01 356.01 62.05 -3.62E-02 5.58E-02 383.85 8.94 -4.35E-03 3.01E-01 Cs-134 475.36 1.48 -7.47E-01 3.94E-02 1.63E+00 563.25 8.34 -3.10E-02 3.41E-01 569.33 15.37 6.73E-03 1.83E-01 604.72 97.62 -5.32E-02 4.55E-02 795.86 85.46 -2.54E-03 3.94E-02 801.95 8.69 -6.65E-02 3.90E-01 1038.61 0.99 -6.38E-01 3.79E+00 1167.97 1.79 -1.70E+00 2.59E+00 1365.19 3.02 4.37E-01 9.71E-01 Cs-137 661.66 85.10 1.26E-02 4.09E-02 4.09E-02 Eu-152 121.78 28.67 -1.87E-02 9.50E-02 9.50E-02 244.70 7.61 -2.06E-01 3.91E-01 295.94 0.45 1.50E+00 6.92E+00 344.28 26.60 1.34E-02 1.14E-01 367.79 0.86 3.06E-01 3.10E+00 411.12 2.24 -2.86E-02 1.30E+00 443.96 2.83 1.29E-01 8.58E-01 488.68 0.42 3.04E+00 7.88E+00 563.99 0.49 -8.59E-01 5.69E+00 586.26 0.46 -4.07E+00 8.86E+00 678.62 0.47 1.39E-01 6.17E+00 688.67 0.86 -5.36E-01 3.10E+00 719.35 0.28 -2.28E+00 1.11E+01 778.90 12.96 -1.69E-02 2.46E-01 810.45 0.32 2.81E+00 1.02E+01 867.37 4.26 -2.93E-01 6.42E-01 919.33 0.43 -2.30E+00 7.72E+00 964.08 14.65 -1.97E-01 3.08E-01 1085.87 10.24 -4.06E-02 3.09E-01 1089.74 1.73 6.14E-01 2.23E+00 1112.07 13.69 -1.86E-01 3.34E-01 1212.95 1.43 2.74E-01 2.62E+00 1249.94 0.19 1.05E+01 2.12E+01 1299.14 1.63 -1.87E+00 2.10E+00 1408.01 21.07 -1.52E-01 1.14E-01 1457.64 0.50 -4.71E+00 2.55E+01 1528.10 0.28 -4.65E+00 8.11E+00 Eu-154 123.07 40.40 5.05E-03 6.84E-02 6.84E-02 247.93 6.89 -5.15E-02 3.82E-01 591.76 4.95 -1.93E-01 5.83E-01 692.42 1.78 -1.65E-01 1.62E+00 723.30 20.06 -2.02E-02 1.81E-01 756.80 4.52 -2.98E-01 7.35E-01 873.18 12.08 9.62E-02 2.35E-01
| |
| [207]
| |
| | |
| 6/18/2019 12:55:04PM Page 7 of 7 Analysis Report for 18-Jun-19-10031 L1-10221C-QJGS-001SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 7.10E-02 6.84E-02 4.01E-01 1004.76 18.01 -2.63E-02 2.18E-01 1274.43 34.80 -2.72E-02 1.04E-01 1596.48 1.80 -1.12E+00 1.31E+00 Eu-155 45.30 1.31 -1.66E+00 1.41E-01 8.98E+00 60.01 1.22 -6.99E-01 9.87E+00 86.55 30.70 -3.39E-02 1.41E-01 105.31 21.10 1.46E-01 1.77E-01 Ra-226 186.21 3.64 3.60E-01 8.90E-01 8.90E-01 Pa-231 27.36 10.30 7.41E-01 1.06E+00 1.08E+00 283.69 1.70 -7.74E-01 1.46E+00 300.07 2.47 -1.02E+00 1.06E+00 302.65 2.20 2.87E-01 1.23E+00 330.06 1.40 2.75E-01 2.15E+00 U-235 143.76 10.96 -1.36E-02 5.66E-02 2.36E-01 163.33 5.08 2.43E-01 6.12E-01 185.71 57.20 1.67E-02 5.66E-02 202.11 1.08 1.47E+00 2.77E+00 205.31 5.01 -2.32E-01 5.67E-01 Am-241 59.54 35.90 -4.59E-02 3.43E-01 3.43E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [208]
| |
| | |
| 6/18/2019 11:24:20AM Page 1 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10032 Sample Description : L1-10221C-FJGS-002SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.739E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:14:00AM Acquisition Started : 6/18/2019 11:09:05AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.0 seconds Dead Time : 0.11 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77464 Fill Height : 1738.60 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 11:24:09AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [209]
| |
| | |
| 6/18/2019 11:24:20AM Page 2 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.55 947 - 960 954.28 1.04E+02 14.57 3.86E+01 0.78 2 295.06 1175 - 1186 1180.14 1.70E+01 8.34 2.10E+01 0.46 3 351.70 1401 - 1410 1406.53 2.70E+01 7.99 1.60E+01 0.53 4 582.81 2324 - 2336 2330.43 2.75E+01 7.25 9.50E+00 0.31 5 608.82 2429 - 2440 2434.45 2.74E+01 6.26 4.60E+00 0.71 6 1459.83 5829 - 5849 5839.16 1.41E+02 12.22 2.50E+00 1.38 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.85 1460.82
| |
| * 10.66 3.38E+00 3.29E-01 Tl-208 0.97 583.19
| |
| * 85.00 4.47E-02 1.21E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.83E-01 2.95E-02 300.09 3.30 Bi-214 0.98 609.32
| |
| * 45.49 8.56E-02 2.02E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 [210]
| |
| | |
| 6/18/2019 11:24:20AM Page 3 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.98 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 7.92E-02 3.94E-02 351.93
| |
| * 35.60 7.37E-02 2.26E-02 785.96 1.06
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.855 3.38E+00 3.29E-01 Tl-208 0.977 4.47E-02 1.21E-02 X Bi-211 0.938 Pb-212 0.999 1.83E-01 2.95E-02 Bi-214 0.984 8.56E-02 2.02E-02 Pb-214 0.994 7.51E-02 1.96E-02
| |
| [211]
| |
| | |
| 6/18/2019 11:24:20AM Page 4 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [212]
| |
| | |
| 6/18/2019 11:24:20AM Page 5 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 11:24:09AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 7.07E-02 5.43E-02 5.43E-02 BE-7 477.60 10.44 1.35E-01 3.36E-01 3.36E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.38E+00 3.11E-01 3.11E-01 Mn-54 834.85 99.98 -2.49E-02 3.78E-02 3.78E-02 Co-60 1173.23 99.85 -1.66E-02 5.00E-02 5.00E-02 1332.49 99.98 4.26E-02 6.20E-02 Nb-94 702.65 99.81 7.84E-04 3.88E-02 3.90E-02 871.09 99.89 1.62E-02 3.88E-02 Ag-108m 79.13 6.60 4.73E-01 3.87E-02 1.64E+00 433.94 90.50 1.47E-02 4.04E-02 614.28 89.80 -2.29E-02 3.87E-02 722.94 90.80 3.46E-03 4.72E-02 Sb-125 176.31 6.84 -2.36E-02 1.18E-01 4.68E-01 380.45 1.52 -7.82E-01 2.09E+00 427.87 29.60 -1.82E-02 1.18E-01 463.36 10.49 3.77E-01 3.98E-01 600.60 17.65 -5.02E-02 2.11E-01 606.71 4.98 9.79E-01 1.03E+00 635.95 11.22 -7.26E-02 2.63E-01 [213]
| |
| | |
| 6/18/2019 11:24:20AM Page 6 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.79E+00 1.18E-01 2.32E+00 Ba-133 79.61 2.65 -1.55E+00 5.93E-02 3.82E+00 81.00 32.90 -1.40E-01 2.76E-01 276.40 7.16 -1.88E-01 4.22E-01 302.85 18.34 -9.37E-03 1.62E-01 356.01 62.05 -4.50E-02 5.93E-02 383.85 8.94 -1.12E-01 3.67E-01 Cs-134 475.36 1.48 -3.56E-01 4.02E-02 2.41E+00 563.25 8.34 1.12E-01 3.67E-01 569.33 15.37 9.51E-02 2.15E-01 604.72 97.62 -1.40E-02 5.29E-02 795.86 85.46 -2.76E-02 4.02E-02 801.95 8.69 -2.90E-01 3.55E-01 1038.61 0.99 1.09E+00 4.54E+00 1167.97 1.79 2.70E+00 3.12E+00 1365.19 3.02 -9.78E-01 1.18E+00 Cs-137 661.66 85.10 7.32E-02 6.32E-02 6.32E-02 Eu-152 121.78 28.67 -6.97E-02 1.20E-01 1.22E-01 244.70 7.61 3.92E-02 4.32E-01 295.94 0.45 1.47E+00 8.42E+00 344.28 26.60 6.36E-02 1.20E-01 367.79 0.86 -1.41E+00 3.64E+00 411.12 2.24 8.07E-01 1.46E+00 443.96 2.83 8.19E-01 1.23E+00 488.68 0.42 3.36E+00 7.82E+00 563.99 0.49 3.77E+00 6.39E+00 586.26 0.46 -3.33E+00 1.13E+01 678.62 0.47 -7.92E+00 6.32E+00 688.67 0.86 4.50E-01 4.56E+00 719.35 0.28 -6.08E+00 1.19E+01 778.90 12.96 -1.55E-02 3.01E-01 810.45 0.32 -5.61E+00 1.18E+01 867.37 4.26 -6.54E-02 9.33E-01 919.33 0.43 6.69E+00 1.09E+01 964.08 14.65 3.04E-01 3.42E-01 1085.87 10.24 4.27E-02 4.64E-01 1089.74 1.73 9.32E-01 2.53E+00 1112.07 13.69 -1.30E-01 2.68E-01 1212.95 1.43 -4.99E-01 3.49E+00 1249.94 0.19 1.52E+00 2.53E+01 1299.14 1.63 5.17E-01 2.72E+00 1408.01 21.07 -1.43E-01 1.85E-01 1457.64 0.50 7.45E+01 3.10E+01 1528.10 0.28 4.72E+00 1.28E+01 Eu-154 123.07 40.40 1.63E-02 9.24E-02 9.24E-02 247.93 6.89 1.40E-01 4.43E-01 591.76 4.95 5.26E-02 7.70E-01 692.42 1.78 -1.75E-01 2.30E+00 723.30 20.06 -1.44E-02 2.14E-01 756.80 4.52 1.79E-01 8.86E-01 873.18 12.08 2.18E-02 2.92E-01
| |
| [214]
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| 6/18/2019 11:24:20AM Page 7 of 7 Analysis Report for 18-Jun-19-10032 L1-10221C-FJGS-002SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 2.22E-01 9.24E-02 4.28E-01 1004.76 18.01 -1.37E-02 2.51E-01 1274.43 34.80 1.79E-02 1.21E-01 1596.48 1.80 9.19E-01 2.24E+00 Eu-155 45.30 1.31 1.53E+00 2.42E-01 2.83E+01 60.01 1.22 7.98E-01 2.70E+01 86.55 30.70 -3.63E-02 2.42E-01 105.31 21.10 4.02E-02 2.50E-01 Ra-226 186.21 3.64 -3.11E-01 1.00E+00 1.00E+00 Pa-231 27.36 10.30 1.67E+00 1.27E+00 3.09E+00 283.69 1.70 2.86E-01 1.99E+00 300.07 2.47 -1.91E-02 1.27E+00 302.65 2.20 1.82E-01 1.35E+00 330.06 1.40 1.60E-02 2.49E+00 U-235 143.76 10.96 -4.28E-02 6.61E-02 3.65E-01 163.33 5.08 -2.26E-01 6.96E-01 185.71 57.20 2.30E-03 6.61E-02 202.11 1.08 -3.35E+00 2.88E+00 205.31 5.01 1.73E-01 6.56E-01 Am-241 59.54 35.90 1.76E-01 9.87E-01 9.87E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [215]
| |
| | |
| 6/18/2019 11:24:25AM Page 1 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10033 Sample Description : L1-10221C-FJGS-003SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.635E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:16:00AM Acquisition Started : 6/18/2019 11:09:14AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77465 Fill Height : 1635.46 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 11:24:16AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [216]
| |
| | |
| 6/18/2019 11:24:25AM Page 2 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.88 946 - 960 955.08 7.34E+01 12.89 3.26E+01 0.91 2 295.06 1174 - 1183 1179.52 2.45E+01 8.00 1.75E+01 0.86 3 351.94 1400 - 1415 1406.76 7.77E+01 9.23 2.25E+00 1.04 4 609.23 2430 - 2441 2434.98 3.90E+01 7.36 6.00E+00 0.76 5 1460.38 5830 - 5850 5839.46 1.62E+02 12.73 0.00E+00 1.51 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.96 1460.82
| |
| * 10.66 3.57E+00 3.20E-01 Bi-211 0.88 351.07
| |
| * 13.02 5.28E-01 7.58E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.15E-01 2.23E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.11E-01 2.21E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 [217]
| |
| | |
| 6/18/2019 11:24:25AM Page 3 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 1.03E-01 3.48E-02 351.93
| |
| * 35.60 1.93E-01 2.77E-02 785.96 1.06
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.969 3.57E+00 3.20E-01 Bi-211 0.887 2.46E-01 1.21E-01 Pb-212 0.991 1.15E-01 2.23E-02 Bi-214 1.000 1.11E-01 2.21E-02 Pb-214 0.999 1.03E-01 3.48E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [218]
| |
| | |
| 6/18/2019 11:24:25AM Page 4 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 11:24:16AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 4.06E-02 4.52E-02 4.52E-02 BE-7 477.60 10.44 1.05E-01 3.06E-01 3.06E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.57E+00 6.33E-02 6.33E-02 Mn-54 834.85 99.98 1.64E-02 3.83E-02 3.83E-02 Co-60 1173.23 99.85 1.50E-02 3.20E-02 5.42E-02 1332.49 99.98 -5.48E-04 3.20E-02 Nb-94 702.65 99.81 1.85E-02 3.74E-02 4.24E-02 871.09 99.89 6.88E-03 3.74E-02 Ag-108m 79.13 6.60 9.99E-01 2.94E-02 1.04E+00 433.94 90.50 -1.82E-02 2.94E-02 614.28 89.80 -2.21E-02 4.60E-02 722.94 90.80 2.05E-02 4.15E-02 Sb-125 176.31 6.84 1.16E-01 7.79E-02 3.32E-01 380.45 1.52 -9.51E-01 1.54E+00 427.87 29.60 -4.13E-02 7.79E-02 463.36 10.49 2.66E-01 3.37E-01 600.60 17.65 -1.68E-01 1.73E-01 606.71 4.98 1.16E+00 1.07E+00 635.95 11.22 -1.79E-02 2.77E-01 [219]
| |
| | |
| 6/18/2019 11:24:25AM Page 5 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 6.23E-01 7.79E-02 2.01E+00 Ba-133 79.61 2.65 1.37E+00 5.80E-02 2.46E+00 81.00 32.90 -1.90E-01 1.50E-01 276.40 7.16 4.96E-02 3.66E-01 302.85 18.34 -2.95E-02 1.45E-01 356.01 62.05 1.07E-02 5.80E-02 383.85 8.94 1.23E-02 2.68E-01 Cs-134 475.36 1.48 2.04E+00 3.79E-02 2.19E+00 563.25 8.34 -1.66E-01 3.75E-01 569.33 15.37 7.06E-02 1.87E-01 604.72 97.62 -3.34E-02 4.69E-02 795.86 85.46 -1.53E-02 3.79E-02 801.95 8.69 -2.93E-01 4.08E-01 1038.61 0.99 3.29E-01 3.79E+00 1167.97 1.79 1.07E+00 3.12E+00 1365.19 3.02 5.33E-01 1.39E+00 Cs-137 661.66 85.10 -3.74E-03 4.10E-02 4.10E-02 Eu-152 121.78 28.67 3.15E-02 1.04E-01 1.04E-01 244.70 7.61 -4.89E-03 3.95E-01 295.94 0.45 6.39E+00 7.82E+00 344.28 26.60 -2.79E-02 1.06E-01 367.79 0.86 -3.18E-01 2.99E+00 411.12 2.24 9.56E-01 1.35E+00 443.96 2.83 -4.66E-01 9.54E-01 488.68 0.42 -5.24E-01 6.46E+00 563.99 0.49 -1.14E+00 6.10E+00 586.26 0.46 8.48E+00 1.03E+01 678.62 0.47 1.85E-02 7.81E+00 688.67 0.86 2.71E-01 3.72E+00 719.35 0.28 -5.60E+00 1.05E+01 778.90 12.96 -3.00E-02 2.46E-01 810.45 0.32 3.80E+00 1.14E+01 867.37 4.26 -2.06E-02 8.29E-01 919.33 0.43 4.34E+00 8.85E+00 964.08 14.65 -8.12E-02 3.63E-01 1085.87 10.24 2.19E-01 4.24E-01 1089.74 1.73 -1.98E-01 2.45E+00 1112.07 13.69 -2.28E-01 3.05E-01 1212.95 1.43 2.33E+00 3.74E+00 1249.94 0.19 1.89E+01 2.52E+01 1299.14 1.63 -2.32E+00 2.18E+00 1408.01 21.07 1.03E-01 2.33E-01 1457.64 0.50 7.60E+01 2.99E+01 1528.10 0.28 1.23E-01 1.34E+01 Eu-154 123.07 40.40 4.29E-02 7.42E-02 7.42E-02 247.93 6.89 -3.45E-02 3.84E-01 591.76 4.95 1.97E-01 6.53E-01 692.42 1.78 1.52E+00 2.22E+00 723.30 20.06 8.59E-02 1.88E-01 756.80 4.52 2.48E-01 6.48E-01 873.18 12.08 2.77E-01 3.68E-01
| |
| [220]
| |
| | |
| 6/18/2019 11:24:25AM Page 6 of 6 Analysis Report for 18-Jun-19-10033 L1-10221C-FJGS-003SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 8.21E-02 7.42E-02 3.81E-01 1004.76 18.01 1.23E-01 2.35E-01 1274.43 34.80 4.37E-02 1.49E-01 1596.48 1.80 -9.80E-02 2.53E+00 Eu-155 45.30 1.31 3.36E+00 1.50E-01 9.86E+00 60.01 1.22 2.76E+00 1.01E+01 86.55 30.70 9.26E-03 1.51E-01 105.31 21.10 -8.31E-02 1.50E-01 Ra-226 186.21 3.64 6.71E-01 8.44E-01 8.44E-01 Pa-231 27.36 10.30 9.58E-01 1.12E+00 1.13E+00 283.69 1.70 -3.91E-01 1.52E+00 300.07 2.47 -7.16E-01 1.12E+00 302.65 2.20 -4.66E-01 1.22E+00 330.06 1.40 -3.27E-01 2.05E+00 U-235 143.76 10.96 4.86E-02 5.21E-02 2.29E-01 163.33 5.08 -1.68E-01 4.47E-01 185.71 57.20 1.72E-02 5.21E-02 202.11 1.08 2.37E-01 2.45E+00 205.31 5.01 -2.50E-01 4.94E-01 Am-241 59.54 35.90 4.18E-02 3.64E-01 3.64E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [221]
| |
| | |
| 6/18/2019 12:25:12PM Page 1 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10034 Sample Description : L1-10221C-FJGS-004SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.701E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:18:00AM Acquisition Started : 6/18/2019 12:09:59PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.9 seconds Dead Time : 0.10 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77467 Fill Height : 1700.89 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 12:25:03PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [222]
| |
| | |
| 6/18/2019 12:25:12PM Page 2 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.38 948 - 959 953.62 5.79E+01 12.51 3.81E+01 0.66 2 351.77 1402 - 1414 1406.80 3.45E+01 9.03 1.75E+01 0.66 3 609.08 2431 - 2441 2435.48 2.50E+01 6.37 5.99E+00 0.54 4 1459.87 5830 - 5849 5839.32 1.02E+02 10.86 4.61E+00 1.65 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.86 1460.82
| |
| * 10.66 2.48E+00 2.84E-01 Bi-211 0.92 351.07
| |
| * 13.02 2.59E-01 7.09E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.02E-01 2.34E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 7.85E-02 2.05E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 [223]
| |
| | |
| 6/18/2019 12:25:12PM Page 3 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 9.46E-02 2.59E-02 785.96 1.06
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.865 2.48E+00 2.84E-01
| |
| ? Bi-211 0.925 2.59E-01 7.09E-02 Pb-212 0.991 1.02E-01 2.34E-02 Bi-214 0.996 7.85E-02 2.05E-02
| |
| ? Pb-214 0.997 9.46E-02 2.59E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [224]
| |
| | |
| 6/18/2019 12:25:12PM Page 4 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 12:25:03PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 4.92E-02 5.30E-02 5.30E-02 BE-7 477.60 10.44 1.73E-01 3.95E-01 3.95E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.48E+00 3.93E-01 3.93E-01 Mn-54 834.85 99.98 -2.13E-02 3.90E-02 3.90E-02 Co-60 1173.23 99.85 1.97E-02 4.70E-02 5.85E-02 1332.49 99.98 1.42E-02 4.70E-02 Nb-94 702.65 99.81 3.03E-05 3.78E-02 4.31E-02 871.09 99.89 -3.63E-03 3.78E-02 Ag-108m 79.13 6.60 3.13E-01 3.42E-02 1.57E+00 433.94 90.50 1.06E-02 3.42E-02 614.28 89.80 3.22E-03 4.59E-02 722.94 90.80 -2.51E-03 4.57E-02 Sb-125 176.31 6.84 2.33E-01 9.01E-02 5.00E-01 380.45 1.52 1.14E+00 2.18E+00 427.87 29.60 -9.38E-02 9.01E-02 463.36 10.49 2.09E-01 3.66E-01 600.60 17.65 3.17E-04 1.91E-01 606.71 4.98 4.51E-01 9.72E-01 635.95 11.22 7.21E-02 3.52E-01 [225]
| |
| | |
| 6/18/2019 12:25:12PM Page 5 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -2.01E+00 9.01E-02 2.07E+00 Ba-133 79.61 2.65 -2.68E+00 5.45E-02 3.59E+00 81.00 32.90 -2.65E-01 2.59E-01 276.40 7.16 2.40E-01 4.84E-01 302.85 18.34 5.20E-02 1.88E-01 356.01 62.05 -2.20E-02 5.45E-02 383.85 8.94 2.62E-01 3.82E-01 Cs-134 475.36 1.48 1.63E-01 3.90E-02 2.62E+00 563.25 8.34 2.36E-01 4.59E-01 569.33 15.37 -1.69E-01 2.06E-01 604.72 97.62 -3.91E-02 4.67E-02 795.86 85.46 1.13E-02 3.90E-02 801.95 8.69 -1.25E-01 3.25E-01 1038.61 0.99 4.65E-01 4.31E+00 1167.97 1.79 5.61E-01 3.26E+00 1365.19 3.02 -1.63E-01 1.01E+00 Cs-137 661.66 85.10 5.00E-02 6.10E-02 6.10E-02 Eu-152 121.78 28.67 9.51E-03 1.20E-01 1.29E-01 244.70 7.61 -8.73E-02 4.49E-01 295.94 0.45 5.02E+00 9.01E+00 344.28 26.60 4.43E-02 1.20E-01 367.79 0.86 -6.31E-02 3.80E+00 411.12 2.24 9.08E-01 1.44E+00 443.96 2.83 2.91E-01 1.44E+00 488.68 0.42 2.06E-01 7.42E+00 563.99 0.49 3.89E+00 7.80E+00 586.26 0.46 1.23E+01 1.10E+01 678.62 0.47 1.92E-01 7.38E+00 688.67 0.86 -8.08E-01 3.26E+00 719.35 0.28 2.72E+00 1.23E+01 778.90 12.96 1.04E-01 2.62E-01 810.45 0.32 2.41E+00 1.01E+01 867.37 4.26 5.38E-01 1.01E+00 919.33 0.43 -1.71E+00 8.59E+00 964.08 14.65 1.83E-01 3.57E-01 1085.87 10.24 -2.13E-02 5.00E-01 1089.74 1.73 8.13E-01 2.83E+00 1112.07 13.69 -7.09E-02 3.25E-01 1212.95 1.43 -3.77E-01 3.50E+00 1249.94 0.19 2.20E+01 2.84E+01 1299.14 1.63 -1.77E+00 1.82E+00 1408.01 21.07 1.07E-01 2.06E-01 1457.64 0.50 4.96E+01 2.73E+01 1528.10 0.28 6.64E+00 1.48E+01 Eu-154 123.07 40.40 4.03E-02 9.54E-02 9.54E-02 247.93 6.89 -8.26E-02 4.49E-01 591.76 4.95 -1.46E-01 6.73E-01 692.42 1.78 5.12E-01 1.93E+00 723.30 20.06 1.67E-01 2.15E-01 756.80 4.52 9.52E-02 8.28E-01 873.18 12.08 5.64E-02 3.23E-01
| |
| [226]
| |
| | |
| 6/18/2019 12:25:12PM Page 6 of 6 Analysis Report for 18-Jun-19-10034 L1-10221C-FJGS-004SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.42E-01 9.54E-02 4.07E-01 1004.76 18.01 1.67E-01 2.38E-01 1274.43 34.80 6.32E-03 1.67E-01 1596.48 1.80 1.08E+00 2.40E+00 Eu-155 45.30 1.31 -5.97E+00 1.97E-01 2.30E+01 60.01 1.22 1.55E+00 2.40E+01 86.55 30.70 -1.67E-01 2.12E-01 105.31 21.10 -9.18E-02 1.97E-01 Ra-226 186.21 3.64 8.39E-01 9.01E-01 9.01E-01 Pa-231 27.36 10.30 2.32E+00 1.50E+00 2.83E+00 283.69 1.70 -1.17E+00 1.76E+00 300.07 2.47 3.49E-01 1.50E+00 302.65 2.20 3.94E-01 1.57E+00 330.06 1.40 -6.98E-01 2.07E+00 U-235 143.76 10.96 -2.60E-03 5.60E-02 3.32E-01 163.33 5.08 3.51E-02 6.48E-01 185.71 57.20 2.35E-02 5.60E-02 202.11 1.08 -1.42E+00 3.12E+00 205.31 5.01 -2.89E-01 6.31E-01 Am-241 59.54 35.90 -5.28E-02 8.59E-01 8.59E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [227]
| |
| | |
| 6/18/2019 12:25:17PM Page 1 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10035 Sample Description : L1-10221C-FJGS-005SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.718E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:20:00AM Acquisition Started : 6/18/2019 12:10:06PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77468 Fill Height : 1717.57 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 12:25:08PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [228]
| |
| | |
| 6/18/2019 12:25:17PM Page 2 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.70 948 - 961 954.38 7.95E+01 13.62 3.85E+01 1.04 2 352.13 1400 - 1413 1407.52 5.51E+01 8.64 6.85E+00 0.64 3 583.19 2326 - 2335 2330.88 1.73E+01 6.08 8.72E+00 0.30 4 609.19 2429 - 2441 2434.80 3.60E+01 7.18 5.99E+00 0.79 5 911.11 3637 - 3646 3641.91 2.00E+01 4.47 0.00E+00 0.83 6 1460.58 5830 - 5850 5840.27 1.29E+02 12.12 5.01E+00 1.44 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 2.81E+00 2.90E-01 Tl-208 1.00 583.19
| |
| * 85.00 2.54E-02 9.05E-03 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.24E-01 2.35E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.02E-01 2.12E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 [229]
| |
| | |
| 6/18/2019 12:25:17PM Page 3 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.36E-01 2.39E-02 785.96 1.06 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.31E-01 2.98E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [230]
| |
| | |
| 6/18/2019 12:25:17PM Page 4 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.991 2.81E+00 2.90E-01 Tl-208 1.000 2.54E-02 9.05E-03 Pb-212 0.999 1.24E-01 2.35E-02 Bi-214 0.999 1.02E-01 2.12E-02 Pb-214 0.997 1.36E-01 2.39E-02 Ac-228 1.000 1.31E-01 2.98E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [231]
| |
| | |
| 6/18/2019 12:25:17PM Page 5 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 12:25:08PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.27E-02 4.74E-02 4.74E-02 BE-7 477.60 10.44 7.52E-02 3.47E-01 3.47E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.81E+00 3.74E-01 3.74E-01 Mn-54 834.85 99.98 5.97E-03 3.32E-02 3.32E-02 Co-60 1173.23 99.85 4.25E-03 4.07E-02 4.96E-02 1332.49 99.98 -3.79E-03 4.07E-02 Nb-94 702.65 99.81 -3.55E-03 2.82E-02 3.21E-02 871.09 99.89 1.47E-02 2.82E-02 Ag-108m 79.13 6.60 6.53E-01 3.02E-02 9.36E-01 433.94 90.50 -6.88E-03 3.02E-02 614.28 89.80 4.73E-03 3.94E-02 722.94 90.80 1.73E-02 3.78E-02 Sb-125 176.31 6.84 9.95E-02 1.04E-01 3.60E-01 380.45 1.52 -8.61E-01 1.58E+00 427.87 29.60 5.03E-03 1.04E-01 463.36 10.49 -1.02E-02 2.58E-01 600.60 17.65 -1.45E-01 1.76E-01 606.71 4.98 1.14E+00 1.04E+00 635.95 11.22 -8.85E-02 2.30E-01 [232]
| |
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| 6/18/2019 12:25:17PM Page 6 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -2.80E-01 1.04E-01 1.60E+00 Ba-133 79.61 2.65 2.21E+00 5.10E-02 2.33E+00 81.00 32.90 -1.26E-01 1.55E-01 276.40 7.16 2.48E-01 3.81E-01 302.85 18.34 1.73E-02 1.44E-01 356.01 62.05 -2.09E-02 5.10E-02 383.85 8.94 1.94E-01 3.09E-01 Cs-134 475.36 1.48 8.13E-01 4.08E-02 2.30E+00 563.25 8.34 -4.05E-01 3.79E-01 569.33 15.37 2.62E-02 2.22E-01 604.72 97.62 -3.04E-02 4.83E-02 795.86 85.46 3.06E-02 4.08E-02 801.95 8.69 -5.03E-02 3.71E-01 1038.61 0.99 -2.32E+00 3.36E+00 1167.97 1.79 -1.84E-01 2.76E+00 1365.19 3.02 -2.74E-01 1.26E+00 Cs-137 661.66 85.10 -1.14E-02 3.62E-02 3.62E-02 Eu-152 121.78 28.67 3.90E-02 9.25E-02 9.25E-02 244.70 7.61 3.23E-02 3.74E-01 295.94 0.45 3.24E+00 6.77E+00 344.28 26.60 4.40E-02 1.00E-01 367.79 0.86 -4.81E-01 2.87E+00 411.12 2.24 -5.23E-01 1.22E+00 443.96 2.83 5.34E-01 1.05E+00 488.68 0.42 1.45E+00 6.68E+00 563.99 0.49 -1.24E+01 5.77E+00 586.26 0.46 9.46E+00 9.45E+00 678.62 0.47 7.66E-01 5.91E+00 688.67 0.86 -5.23E-01 3.49E+00 719.35 0.28 1.21E+00 9.30E+00 778.90 12.96 1.14E-02 2.85E-01 810.45 0.32 4.64E+00 1.01E+01 867.37 4.26 -1.56E-01 6.90E-01 919.33 0.43 5.55E+00 8.26E+00 964.08 14.65 8.97E-02 3.49E-01 1085.87 10.24 -2.23E-01 4.19E-01 1089.74 1.73 1.86E+00 2.49E+00 1112.07 13.69 3.18E-02 3.34E-01 1212.95 1.43 -7.92E-01 2.57E+00 1249.94 0.19 -5.98E+00 1.98E+01 1299.14 1.63 5.18E-01 2.46E+00 1408.01 21.07 -1.13E-01 1.76E-01 1457.64 0.50 6.31E+01 2.72E+01 1528.10 0.28 5.96E+00 1.33E+01 Eu-154 123.07 40.40 8.18E-03 6.31E-02 6.31E-02 247.93 6.89 -1.26E-01 3.43E-01 591.76 4.95 3.88E-01 6.20E-01 692.42 1.78 5.13E-02 1.92E+00 723.30 20.06 -5.82E-02 1.67E-01 756.80 4.52 -2.70E-01 6.64E-01 873.18 12.08 -2.11E-02 2.34E-01
| |
| [233]
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| 6/18/2019 12:25:17PM Page 7 of 7 Analysis Report for 18-Jun-19-10035 L1-10221C-FJGS-005SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 2.22E-01 6.31E-02 3.45E-01 1004.76 18.01 -1.62E-01 1.88E-01 1274.43 34.80 -1.23E-01 1.22E-01 1596.48 1.80 -5.99E-01 1.55E+00 Eu-155 45.30 1.31 -5.92E-01 1.36E-01 7.73E+00 60.01 1.22 3.28E-01 9.48E+00 86.55 30.70 1.46E-02 1.47E-01 105.31 21.10 -4.93E-02 1.36E-01 Ra-226 186.21 3.64 1.14E-01 6.57E-01 6.57E-01 Pa-231 27.36 10.30 6.58E-01 9.83E-01 9.83E-01 283.69 1.70 -9.72E-01 1.44E+00 300.07 2.47 -9.73E-01 1.03E+00 302.65 2.20 2.65E-01 1.20E+00 330.06 1.40 1.17E+00 2.02E+00 U-235 143.76 10.96 -1.61E-01 4.24E-02 2.25E-01 163.33 5.08 9.18E-02 5.23E-01 185.71 57.20 1.58E-02 4.24E-02 202.11 1.08 -1.31E+00 1.85E+00 205.31 5.01 2.23E-01 4.78E-01 Am-241 59.54 35.90 -4.44E-02 3.12E-01 3.12E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [234]
| |
| | |
| 6/18/2019 12:25:34PM Page 1 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10036 Sample Description : L1-10221C-FJGS-006SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.618E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:22:00AM Acquisition Started : 6/18/2019 12:10:14PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77469 Fill Height : 1618.20 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 12:25:26PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [235]
| |
| | |
| 6/18/2019 12:25:34PM Page 2 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.53 948 - 959 954.59 6.05E+01 11.45 2.75E+01 1.37 2 295.29 1177 - 1186 1181.36 2.35E+01 7.25 1.16E+01 0.69 3 351.75 1402 - 1413 1407.01 3.50E+01 7.08 6.00E+00 0.70 4 609.00 2428 - 2441 2435.26 2.73E+01 8.40 1.57E+01 0.49 5 1460.57 5832 - 5852 5842.64 1.42E+02 13.37 1.03E+01 0.58 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 2.92E+00 3.03E-01 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 9.39E-02 1.93E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 7.41E-02 2.32E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 [236]
| |
| | |
| 6/18/2019 12:25:34PM Page 3 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 9.66E-02 3.09E-02 351.93
| |
| * 35.60 8.43E-02 1.83E-02 785.96 1.06
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.990 2.92E+00 3.03E-01 X Bi-211 0.928 Pb-212 0.998 9.39E-02 1.93E-02 Bi-214 0.993 7.41E-02 2.32E-02 Pb-214 0.997 8.75E-02 1.58E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [237]
| |
| | |
| 6/18/2019 12:25:34PM Page 4 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 12:25:25PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 2.36E-02 4.37E-02 4.37E-02 BE-7 477.60 10.44 -2.22E-02 3.36E-01 3.36E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.92E+00 4.84E-01 4.84E-01 Mn-54 834.85 99.98 0.00E+00 3.62E-02 3.62E-02 Co-60 1173.23 99.85 -4.46E-02 4.28E-02 4.51E-02 1332.49 99.98 -5.14E-04 4.28E-02 Nb-94 702.65 99.81 -1.71E-02 3.15E-02 3.23E-02 871.09 99.89 1.05E-02 3.15E-02 Ag-108m 79.13 6.60 -2.83E-01 2.54E-02 1.14E+00 433.94 90.50 -1.64E-03 2.54E-02 614.28 89.80 -2.74E-02 5.71E-02 722.94 90.80 5.15E-04 3.45E-02 Sb-125 176.31 6.84 1.51E-01 9.79E-02 3.95E-01 380.45 1.52 -6.93E-01 1.96E+00 427.87 29.60 5.80E-02 9.79E-02 463.36 10.49 -9.56E-02 2.87E-01 600.60 17.65 -9.00E-02 1.83E-01 606.71 4.98 6.48E-01 1.02E+00 635.95 11.22 -7.37E-02 2.50E-01 [238]
| |
| | |
| 6/18/2019 12:25:34PM Page 5 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -7.36E-01 9.79E-02 1.91E+00 Ba-133 79.61 2.65 -9.27E-01 5.13E-02 2.69E+00 81.00 32.90 1.53E-03 2.06E-01 276.40 7.16 -2.37E-01 4.00E-01 302.85 18.34 -2.38E-02 1.43E-01 356.01 62.05 -1.26E-02 5.13E-02 383.85 8.94 -8.14E-03 3.42E-01 Cs-134 475.36 1.48 -2.21E-01 4.00E-02 2.16E+00 563.25 8.34 -1.54E-01 2.84E-01 569.33 15.37 3.04E-02 1.91E-01 604.72 97.62 -1.10E-02 4.89E-02 795.86 85.46 -1.84E-02 4.00E-02 801.95 8.69 1.05E-01 3.76E-01 1038.61 0.99 2.30E+00 3.57E+00 1167.97 1.79 1.61E+00 2.62E+00 1365.19 3.02 2.32E-01 1.25E+00 Cs-137 661.66 85.10 4.68E-02 5.54E-02 5.54E-02 Eu-152 121.78 28.67 9.57E-03 9.39E-02 1.12E-01 244.70 7.61 2.28E-01 3.32E-01 295.94 0.45 4.65E+00 7.15E+00 344.28 26.60 -1.56E-02 9.39E-02 367.79 0.86 8.15E-01 3.25E+00 411.12 2.24 -1.98E-01 1.30E+00 443.96 2.83 9.99E-02 9.00E-01 488.68 0.42 -3.57E+00 6.33E+00 563.99 0.49 -1.80E+00 4.83E+00 586.26 0.46 5.29E+00 8.81E+00 678.62 0.47 -1.37E-01 6.53E+00 688.67 0.86 5.85E-01 3.35E+00 719.35 0.28 -3.86E+00 1.03E+01 778.90 12.96 5.96E-02 2.54E-01 810.45 0.32 3.27E+00 9.04E+00 867.37 4.26 -1.21E+00 7.83E-01 919.33 0.43 -4.39E+00 7.88E+00 964.08 14.65 1.82E-01 2.89E-01 1085.87 10.24 1.85E-01 3.99E-01 1089.74 1.73 -3.17E-01 2.42E+00 1112.07 13.69 -1.13E-01 3.03E-01 1212.95 1.43 -7.50E-01 3.37E+00 1249.94 0.19 1.35E+01 2.54E+01 1299.14 1.63 5.31E-01 2.42E+00 1408.01 21.07 1.22E-01 1.98E-01 1457.64 0.50 6.03E+01 2.76E+01 1528.10 0.28 -2.12E+00 1.01E+01 Eu-154 123.07 40.40 2.75E-02 8.04E-02 8.04E-02 247.93 6.89 1.04E-01 3.58E-01 591.76 4.95 -2.62E-01 6.46E-01 692.42 1.78 4.35E-01 1.71E+00 723.30 20.06 7.95E-03 1.60E-01 756.80 4.52 -4.87E-02 7.99E-01 873.18 12.08 6.79E-02 2.52E-01
| |
| [239]
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| 6/18/2019 12:25:34PM Page 6 of 6 Analysis Report for 18-Jun-19-10036 L1-10221C-FJGS-006SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -5.15E-02 8.04E-02 3.69E-01 1004.76 18.01 2.00E-01 2.37E-01 1274.43 34.80 4.51E-02 1.23E-01 1596.48 1.80 -1.85E-01 1.91E+00 Eu-155 45.30 1.31 1.06E+00 1.52E-01 1.45E+01 60.01 1.22 -5.56E+00 1.83E+01 86.55 30.70 -1.70E-01 1.52E-01 105.31 21.10 4.52E-02 1.77E-01 Ra-226 186.21 3.64 9.53E-01 8.14E-01 8.14E-01 Pa-231 27.36 10.30 7.21E-01 1.22E+00 1.76E+00 283.69 1.70 -1.44E+00 1.47E+00 300.07 2.47 -8.16E-01 1.22E+00 302.65 2.20 -1.02E-01 1.22E+00 330.06 1.40 5.43E-02 2.17E+00 U-235 143.76 10.96 -1.11E-01 5.04E-02 2.66E-01 163.33 5.08 -1.94E-01 4.73E-01 185.71 57.20 4.28E-02 5.04E-02 202.11 1.08 -2.48E-02 2.69E+00 205.31 5.01 3.52E-01 5.47E-01 Am-241 59.54 35.90 -2.31E-01 6.50E-01 6.50E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [240]
| |
| | |
| 6/18/2019 1:03:45PM Page 1 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10037 Sample Description : L1-10221C-FJGS-007SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.549E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:24:00AM Acquisition Started : 6/18/2019 12:30:05PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 1800.0 seconds Real Time : 1801.7 seconds Dead Time : 0.09 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77470 Fill Height : 1549.03 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 1:03:17PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [241]
| |
| | |
| 6/18/2019 1:03:45PM Page 2 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.46 949 - 960 953.92 9.03E+01 15.94 6.47E+01 0.86 2 294.88 1175 - 1183 1179.41 2.12E+01 8.72 2.58E+01 0.79 3 351.64 1401 - 1412 1406.28 5.31E+01 11.57 3.19E+01 0.95 4 477.22 1904 - 1912 1908.30 3.08E+01 7.40 1.13E+01 0.65 5 582.72 2324 - 2336 2330.10 4.17E+01 8.45 1.13E+01 0.75 6 609.05 2429 - 2440 2435.36 3.17E+01 8.07 1.33E+01 0.45 7 661.25 2638 - 2650 2644.09 3.61E+01 7.92 9.92E+00 1.03 8 910.63 3634 - 3649 3641.47 3.62E+01 7.31 5.82E+00 0.98 9 1172.26 4681 - 4696 4688.23 3.71E+01 7.40 5.90E+00 1.42 10 1331.69 5321 - 5332 5326.23 2.50E+01 5.71 3.00E+00 1.05 11 1459.89 5829 - 5849 5839.38 1.45E+02 12.04 0.00E+00 1.63 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty BE-7 0.97 477.60
| |
| * 10.44 1.85E-01 4.63E-02 K-40 0.87 1460.82
| |
| * 10.66 1.80E+00 1.69E-01 Co-60 0.88 1173.23
| |
| * 99.85 4.22E-02 8.58E-03 1332.49
| |
| * 99.98 3.08E-02 7.15E-03 Cs-137 0.97 661.66
| |
| * 85.10 3.26E-02 7.43E-03 Tl-208 0.96 583.19
| |
| * 85.00 3.47E-02 7.33E-03[242]
| |
| | |
| 6/18/2019 1:03:45PM Page 3 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 8.05E-02 1.56E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 5.08E-02 1.33E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.98 241.99 7.25 295.22
| |
| * 18.42 5.04E-02 2.11E-02 351.93
| |
| * 35.60 7.42E-02 1.72E-02 785.96 1.06 Ac-228 0.98 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.34E-01 2.78E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
| |
| [243]
| |
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| 6/18/2019 1:03:45PM Page 4 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| BE-7 0.977 1.85E-01 4.63E-02 K-40 0.870 1.80E+00 1.69E-01 Co-60 0.882 3.55E-02 5.49E-03 Cs-137 0.973 3.26E-02 7.43E-03 Tl-208 0.966 3.47E-02 7.33E-03 X Bi-211 0.950 Pb-212 0.995 8.05E-02 1.56E-02 Bi-214 0.995 5.08E-02 1.33E-02 Pb-214 0.986 6.47E-02 1.33E-02 Ac-228 0.984 1.34E-01 2.78E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [244]
| |
| | |
| 6/18/2019 1:03:45PM Page 5 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 1:03:17PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.02E-02 3.61E-02 3.61E-02
| |
| + BE-7 477.60
| |
| * 10.44 1.85E-01 1.17E-01 1.17E-01
| |
| + K-40 1460.82
| |
| * 10.66 1.80E+00 3.57E-02 3.57E-02 Mn-54 834.85 99.98 1.36E-02 2.63E-02 2.63E-02
| |
| + Co-60 1173.23
| |
| * 99.85 4.22E-02 1.51E-02 1.95E-02 1332.49
| |
| * 99.98 3.08E-02 1.51E-02 Nb-94 702.65 99.81 -5.61E-03 2.26E-02 2.45E-02 871.09 99.89 -1.84E-02 2.26E-02 Ag-108m 79.13 6.60 5.09E-01 2.57E-02 9.66E-01 433.94 90.50 5.53E-03 2.57E-02 614.28 89.80 -2.48E-02 2.77E-02 722.94 90.80 9.24E-03 3.03E-02 Sb-125 176.31 6.84 2.34E-03 7.61E-02 3.17E-01 380.45 1.52 -9.36E-01 1.40E+00 427.87 29.60 -3.09E-02 7.61E-02 463.36 10.49 9.95E-02 2.33E-01 600.60 17.65 4.81E-02 1.23E-01 606.71 4.98 4.23E-01 6.15E-01 635.95 11.22 1.91E-01 2.30E-01 [245]
| |
| | |
| 6/18/2019 1:03:45PM Page 6 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.52E-01 7.61E-02 1.13E+00 Ba-133 79.61 2.65 1.19E+00 3.83E-02 2.31E+00 81.00 32.90 -4.24E-02 1.70E-01 276.40 7.16 -1.93E-01 2.85E-01 302.85 18.34 1.89E-02 1.25E-01 356.01 62.05 -1.06E-02 3.83E-02 383.85 8.94 1.10E-01 2.51E-01 Cs-134 475.36 1.48 1.84E+00 2.70E-02 1.90E+00 563.25 8.34 2.01E-01 2.72E-01 569.33 15.37 -1.31E-01 1.26E-01 604.72 97.62 -1.52E-03 3.07E-02 795.86 85.46 1.03E-02 2.70E-02 801.95 8.69 5.54E-02 2.67E-01 1038.61 0.99 1.26E+00 2.46E+00 1167.97 1.79 -3.18E-01 2.53E+00 1365.19 3.02 -3.65E-01 5.20E-01
| |
| + Cs-137 661.66
| |
| * 85.10 3.26E-02 1.84E-02 1.84E-02 Eu-152 121.78 28.67 2.10E-02 8.07E-02 8.42E-02 244.70 7.61 1.71E-01 3.15E-01 295.94 0.45 -1.04E-02 5.00E+00 344.28 26.60 -4.49E-02 8.07E-02 367.79 0.86 -8.05E-02 2.49E+00 411.12 2.24 1.82E-01 8.88E-01 443.96 2.83 -2.10E-01 7.77E-01 488.68 0.42 3.93E+00 5.79E+00 563.99 0.49 2.89E+00 4.62E+00 586.26 0.46 -5.56E+00 6.68E+00 678.62 0.47 -3.47E+00 3.95E+00 688.67 0.86 1.43E+00 2.88E+00 719.35 0.28 -1.18E+00 8.78E+00 778.90 12.96 -1.13E-01 1.58E-01 810.45 0.32 -3.22E+00 7.78E+00 867.37 4.26 -2.55E-01 5.51E-01 919.33 0.43 4.48E+00 6.16E+00 964.08 14.65 -2.94E-02 2.10E-01 1085.87 10.24 1.51E-02 2.50E-01 1089.74 1.73 4.53E-01 1.49E+00 1112.07 13.69 1.22E-01 2.43E-01 1212.95 1.43 -2.03E-01 2.06E+00 1249.94 0.19 7.56E+00 1.49E+01 1299.14 1.63 -4.54E-01 1.55E+00 1408.01 21.07 -4.07E-02 1.23E-01 1457.64 0.50 4.00E+01 1.63E+01 1528.10 0.28 1.92E+00 9.48E+00 Eu-154 123.07 40.40 1.81E-02 6.13E-02 6.13E-02 247.93 6.89 6.89E-02 3.43E-01 591.76 4.95 2.42E-01 4.27E-01 692.42 1.78 -4.85E-01 1.40E+00 723.30 20.06 2.50E-02 1.37E-01 756.80 4.52 -2.25E-01 5.28E-01 873.18 12.08 1.85E-01 2.03E-01
| |
| [246]
| |
| | |
| 6/18/2019 1:03:45PM Page 7 of 7 Analysis Report for 18-Jun-19-10037 L1-10221C-FJGS-007SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.03E-01 6.13E-02 2.83E-01 1004.76 18.01 -1.98E-01 1.47E-01 1274.43 34.80 -6.33E-03 7.80E-02 1596.48 1.80 -1.12E-01 1.15E+00 Eu-155 45.30 1.31 5.21E-01 1.31E-01 1.72E+01 60.01 1.22 -1.37E+01 1.56E+01 86.55 30.70 -8.66E-02 1.31E-01 105.31 21.10 -8.78E-02 1.42E-01 Ra-226 186.21 3.64 3.18E-01 6.22E-01 6.22E-01 Pa-231 27.36 10.30 1.74E+00 8.95E-01 2.00E+00 283.69 1.70 8.31E-01 1.23E+00 300.07 2.47 3.05E-01 8.95E-01 302.65 2.20 4.54E-01 1.06E+00 330.06 1.40 3.57E-01 1.56E+00 U-235 143.76 10.96 2.30E-01 3.98E-02 2.28E-01 163.33 5.08 -2.92E-01 4.14E-01 185.71 57.20 1.52E-02 3.98E-02 202.11 1.08 -2.36E+00 1.93E+00 205.31 5.01 -1.76E-01 4.35E-01 Am-241 59.54 35.90 -1.98E-01 5.75E-01 5.75E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [247]
| |
| | |
| 6/18/2019 12:45:27PM Page 1 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS GAMMA SPECTRUM ANALYSIS Sample Identification : 18-Jun-19-10038 Sample Description : L1-10221C-FJGS-008SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.644E+03 grams Facility : Default Sample Taken On : 6/17/2019 8:26:00AM Acquisition Started : 6/18/2019 12:30:13PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 6/18/2019 Efficiency Calibration Description :
| |
| Sample Number : 77471 Fill Height : 1644.14 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/18/2019 12:45:17PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [248]
| |
| | |
| 6/18/2019 12:45:27PM Page 2 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.15 305 - 314 309.13 2.45E+01 9.92 3.25E+01 0.89 2 238.71 948 - 962 954.42 6.91E+01 12.70 3.09E+01 0.94 3 352.04 1401 - 1414 1407.18 4.35E+01 7.70 5.48E+00 0.37 4 582.89 2325 - 2334 2329.67 2.00E+01 5.59 5.00E+00 0.30 5 1460.66 5829 - 5849 5840.58 1.14E+02 11.15 2.69E+00 1.91 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 2.51E+00 2.68E-01 Tl-208 0.98 583.19
| |
| * 85.00 2.96E-02 8.47E-03 Bi-211 0.86 351.07
| |
| * 13.02 2.95E-01 5.74E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.08E-01 2.18E-02 300.09 3.30 Pb212-XR 1.00 74.82 10.28 77.11
| |
| * 17.10 1.72E-01 7.17E-02 87.35 3.97 89.78 1.46 Pb-214 0.99 241.99 7.25 295.22 18.42 [249]
| |
| | |
| 6/18/2019 12:45:27PM Page 3 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-214 0.99 351.93
| |
| * 35.60 1.08E-01 2.10E-02 785.96 1.06 Pb214-XR 1.00 74.82 5.80 77.11
| |
| * 9.70 3.03E-01 1.27E-01 87.35 2.24 89.78 0.82
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.996 2.51E+00 2.68E-01 Tl-208 0.986 2.96E-02 8.47E-03
| |
| ? Bi-211 0.860 2.95E-01 5.74E-02 Pb-212 0.999 1.08E-01 2.18E-02
| |
| ? Pb212-XR 1.000 1.72E-01 7.17E-02
| |
| ? Pb-214 0.999 1.08E-01 2.10E-02
| |
| ? Pb214-XR 1.000 3.03E-01 1.27E-01
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [250]
| |
| | |
| 6/18/2019 12:45:27PM Page 4 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/18/2019 12:45:17PM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 4.49E-02 4.52E-02 4.52E-02 BE-7 477.60 10.44 8.44E-03 2.81E-01 2.81E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.51E+00 2.99E-01 2.99E-01 Mn-54 834.85 99.98 -1.37E-02 3.13E-02 3.13E-02 Co-60 1173.23 99.85 2.25E-03 4.69E-02 4.79E-02 1332.49 99.98 3.28E-02 4.69E-02 Nb-94 702.65 99.81 2.15E-03 3.22E-02 3.56E-02 871.09 99.89 2.89E-03 3.22E-02 Ag-108m 79.13 6.60 -1.85E-01 2.29E-02 8.44E-01 433.94 90.50 -3.88E-02 2.29E-02 614.28 89.80 -3.50E-02 4.17E-02 722.94 90.80 9.22E-03 3.54E-02 Sb-125 176.31 6.84 -3.82E-02 8.35E-02 3.35E-01 380.45 1.52 -1.12E+00 1.72E+00 427.87 29.60 -2.02E-02 8.35E-02 463.36 10.49 2.12E-01 3.16E-01 600.60 17.65 -1.47E-01 1.42E-01 606.71 4.98 6.84E-01 8.53E-01 635.95 11.22 2.93E-02 2.77E-01 [251]
| |
| | |
| 6/18/2019 12:45:27PM Page 5 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.09E-01 8.35E-02 1.61E+00 Ba-133 79.61 2.65 -6.53E-01 4.98E-02 2.03E+00 81.00 32.90 -5.57E-02 1.35E-01 276.40 7.16 -4.90E-02 3.57E-01 302.85 18.34 -4.47E-02 1.19E-01 356.01 62.05 4.31E-03 4.98E-02 383.85 8.94 1.05E-02 2.67E-01 Cs-134 475.36 1.48 1.24E+00 3.42E-02 2.02E+00 563.25 8.34 -3.59E-01 4.03E-01 569.33 15.37 -1.21E-02 1.83E-01 604.72 97.62 -3.22E-02 3.80E-02 795.86 85.46 1.36E-03 3.42E-02 801.95 8.69 -4.49E-03 3.24E-01 1038.61 0.99 1.06E+00 3.53E+00 1167.97 1.79 -3.47E+00 2.41E+00 1365.19 3.02 5.17E-01 1.15E+00 Cs-137 661.66 85.10 1.34E-02 4.17E-02 4.17E-02 Eu-152 121.78 28.67 5.18E-02 7.25E-02 7.25E-02 244.70 7.61 5.72E-02 3.48E-01 295.94 0.45 2.23E+00 6.17E+00 344.28 26.60 2.21E-02 9.55E-02 367.79 0.86 -2.18E+00 2.52E+00 411.12 2.24 5.96E-01 1.29E+00 443.96 2.83 -9.32E-01 1.04E+00 488.68 0.42 -5.07E+00 5.35E+00 563.99 0.49 -1.21E+01 5.68E+00 586.26 0.46 -7.97E+00 8.70E+00 678.62 0.47 -6.44E+00 6.87E+00 688.67 0.86 8.73E-01 4.08E+00 719.35 0.28 -3.15E+00 1.05E+01 778.90 12.96 8.49E-02 2.38E-01 810.45 0.32 1.99E+00 8.45E+00 867.37 4.26 1.82E-01 6.67E-01 919.33 0.43 -2.78E+00 9.07E+00 964.08 14.65 -2.60E-02 3.00E-01 1085.87 10.24 7.43E-02 3.64E-01 1089.74 1.73 8.86E-01 1.82E+00 1112.07 13.69 6.26E-03 3.21E-01 1212.95 1.43 1.44E+00 2.60E+00 1249.94 0.19 -1.72E+01 1.92E+01 1299.14 1.63 -6.29E-01 2.18E+00 1408.01 21.07 -3.04E-02 1.35E-01 1457.64 0.50 5.50E+01 2.60E+01 1528.10 0.28 -3.01E+00 9.63E+00 Eu-154 123.07 40.40 -3.10E-02 4.89E-02 4.89E-02 247.93 6.89 -3.60E-02 3.46E-01 591.76 4.95 1.57E-01 5.67E-01 692.42 1.78 7.48E-01 1.89E+00 723.30 20.06 -1.26E-02 1.56E-01 756.80 4.52 1.38E-02 6.47E-01 873.18 12.08 -1.49E-01 2.57E-01
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| [252]
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| 6/18/2019 12:45:27PM Page 6 of 6 Analysis Report for 18-Jun-19-10038 L1-10221C-FJGS-008SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.60E-02 4.89E-02 2.69E-01 1004.76 18.01 -1.33E-01 1.74E-01 1274.43 34.80 9.66E-03 1.05E-01 1596.48 1.80 -2.53E+00 1.74E+00 Eu-155 45.30 1.31 5.07E-01 1.34E-01 7.66E+00 60.01 1.22 1.47E+00 9.25E+00 86.55 30.70 6.29E-02 1.34E-01 105.31 21.10 -1.04E-02 1.45E-01 Ra-226 186.21 3.64 5.36E-01 6.96E-01 6.96E-01 Pa-231 27.36 10.30 5.44E-01 9.24E-01 1.07E+00 283.69 1.70 6.57E-01 1.50E+00 300.07 2.47 -6.02E-01 9.24E-01 302.65 2.20 -3.36E-01 1.01E+00 330.06 1.40 1.38E-01 1.82E+00 U-235 143.76 10.96 4.21E-03 4.36E-02 2.00E-01 163.33 5.08 2.29E-01 4.54E-01 185.71 57.20 1.56E-02 4.36E-02 202.11 1.08 -3.24E-01 1.97E+00 205.31 5.01 -1.64E-01 4.04E-01 Am-241 59.54 35.90 1.25E-01 3.29E-01 3.29E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [253]
| |
| | |
| 6/24/2019 8:18:14AM Page 1 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS GAMMA SPECTRUM ANALYSIS Sample Identification : 24-Jun-19-10009 Sample Description : L1-10221C-FIGS-100SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.375E+03 grams Facility : Default Sample Taken On : 6/20/2019 9:50:00AM Acquisition Started : 6/24/2019 8:03:01AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/24/2019 Efficiency Calibration Description :
| |
| Sample Number : 77579 Fill Height : 1374.75 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/24/2019 8:18:05AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [254]
| |
| | |
| 6/24/2019 8:18:14AM Page 2 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.62 948 - 961 954.93 6.04E+01 12.41 3.36E+01 0.89 2 295.45 1177 - 1187 1182.03 2.10E+01 7.42 1.40E+01 1.11 3 351.92 1402 - 1413 1407.67 3.23E+01 8.31 1.47E+01 0.60 4 510.74 2037 - 2047 2042.46 2.91E+01 7.94 1.39E+01 0.34 5 582.99 2325 - 2336 2331.28 3.20E+01 6.88 6.03E+00 0.43 6 609.08 2427 - 2443 2435.57 4.79E+01 7.38 2.08E+00 0.57 7 911.00 3638 - 3649 3643.02 1.75E+01 5.99 6.46E+00 0.77 8 1460.41 5833 - 5853 5842.03 1.15E+02 11.47 4.77E+00 1.33 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 0.99 511.00
| |
| * 100.00 3.51E-02 9.86E-03 K-40 0.97 1460.82
| |
| * 10.66 2.49E+00 2.71E-01 Tl-208 0.99 583.19
| |
| * 85.00 4.70E-02 1.05E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 9.66E-02 2.13E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.35E-01 2.24E-02 768.36 4.89 806.18 1.26 [255]
| |
| | |
| 6/24/2019 8:18:14AM Page 3 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 8.94E-02 3.24E-02 351.93
| |
| * 35.60 8.05E-02 2.17E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.14E-01 3.93E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [256]
| |
| | |
| 6/24/2019 8:18:14AM Page 4 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| An Pk 0.990 3.51E-02 9.86E-03 K-40 0.974 2.49E+00 2.71E-01 Tl-208 0.994 4.70E-02 1.05E-02 X Bi-211 0.891 Pb-212 1.000 9.66E-02 2.13E-02 Bi-214 0.996 1.35E-01 2.24E-02 Pb-214 0.998 8.33E-02 1.80E-02 Ac-228 0.998 1.14E-01 3.93E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [257]
| |
| | |
| 6/24/2019 8:18:14AM Page 5 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/24/2019 8:18:05AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 3.51E-02 2.73E-02 2.73E-02 BE-7 477.60 10.44 5.67E-02 3.26E-01 3.26E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.49E+00 3.59E-01 3.59E-01 Mn-54 834.85 99.98 3.19E-02 3.88E-02 3.88E-02 Co-60 1173.23 99.85 4.22E-03 3.89E-02 4.38E-02 1332.49 99.98 -9.16E-03 3.89E-02 Nb-94 702.65 99.81 1.58E-02 3.21E-02 3.21E-02 871.09 99.89 8.14E-04 4.37E-02 Ag-108m 79.13 6.60 1.34E+00 3.35E-02 1.30E+00 433.94 90.50 7.95E-03 3.35E-02 614.28 89.80 -3.53E-02 5.34E-02 722.94 90.80 2.24E-02 3.86E-02 Sb-125 176.31 6.84 2.80E-01 9.07E-02 3.76E-01 380.45 1.52 8.82E-01 2.10E+00 427.87 29.60 1.55E-02 9.07E-02 463.36 10.49 -3.61E-02 3.24E-01 600.60 17.65 -9.38E-02 1.87E-01 606.71 4.98 5.52E-01 1.07E+00 635.95 11.22 4.99E-02 2.61E-01 [258]
| |
| | |
| 6/24/2019 8:18:14AM Page 6 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 8.25E-01 9.07E-02 1.95E+00 Ba-133 79.61 2.65 2.75E+00 5.40E-02 3.14E+00 81.00 32.90 -2.74E-01 2.14E-01 276.40 7.16 1.45E-01 3.74E-01 302.85 18.34 -3.59E-02 1.40E-01 356.01 62.05 -1.67E-02 5.40E-02 383.85 8.94 -2.48E-01 3.17E-01 Cs-134 475.36 1.48 -6.74E-03 4.28E-02 2.26E+00 563.25 8.34 -2.39E-01 3.65E-01 569.33 15.37 1.84E-01 2.30E-01 604.72 97.62 5.24E-03 5.22E-02 795.86 85.46 -4.59E-03 4.28E-02 801.95 8.69 3.62E-02 3.71E-01 1038.61 0.99 -2.03E+00 3.48E+00 1167.97 1.79 -1.49E+00 2.30E+00 1365.19 3.02 5.83E-01 1.20E+00 Cs-137 661.66 85.10 1.97E-02 3.71E-02 3.71E-02 Eu-152 121.78 28.67 1.08E-02 1.08E-01 1.08E-01 244.70 7.61 1.14E-01 3.86E-01 295.94 0.45 2.89E+00 7.28E+00 344.28 26.60 4.29E-02 1.08E-01 367.79 0.86 -8.23E-01 3.09E+00 411.12 2.24 1.99E-01 1.17E+00 443.96 2.83 -1.28E-01 1.07E+00 488.68 0.42 7.35E+00 8.59E+00 563.99 0.49 -4.12E-01 6.57E+00 586.26 0.46 1.08E+01 1.03E+01 678.62 0.47 -1.14E+01 6.46E+00 688.67 0.86 -2.86E+00 4.04E+00 719.35 0.28 -6.94E+00 1.10E+01 778.90 12.96 -3.56E-01 2.19E-01 810.45 0.32 -7.18E+00 8.72E+00 867.37 4.26 5.38E-02 9.27E-01 919.33 0.43 -3.17E-01 9.39E+00 964.08 14.65 1.58E-01 3.25E-01 1085.87 10.24 -2.22E-01 3.18E-01 1089.74 1.73 1.09E+00 1.97E+00 1112.07 13.69 -2.47E-01 2.91E-01 1212.95 1.43 -1.42E+00 2.56E+00 1249.94 0.19 2.18E+01 2.66E+01 1299.14 1.63 9.27E-01 2.80E+00 1408.01 21.07 9.58E-02 1.84E-01 1457.64 0.50 5.81E+01 2.61E+01 1528.10 0.28 -6.98E+00 1.32E+01 Eu-154 123.07 40.40 1.57E-02 7.62E-02 7.62E-02 247.93 6.89 -3.73E-01 3.84E-01 591.76 4.95 2.24E-01 6.20E-01 692.42 1.78 7.68E-01 1.96E+00 723.30 20.06 -3.23E-02 1.67E-01 756.80 4.52 4.02E-01 8.66E-01 873.18 12.08 1.21E-01 3.42E-01
| |
| [259]
| |
| | |
| 6/24/2019 8:18:14AM Page 7 of 7 Analysis Report for 24-Jun-19-10009 L1-10221C-FIGS-100SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.56E-01 7.62E-02 3.65E-01 1004.76 18.01 1.79E-01 2.31E-01 1274.43 34.80 3.77E-02 1.21E-01 1596.48 1.80 -3.78E+00 1.33E+00 Eu-155 45.30 1.31 1.85E+00 1.63E-01 1.60E+01 60.01 1.22 -2.54E+01 1.57E+01 86.55 30.70 7.20E-02 1.78E-01 105.31 21.10 -2.44E-02 1.63E-01 Ra-226 186.21 3.64 3.64E-01 8.02E-01 8.02E-01 Pa-231 27.36 10.30 1.27E+00 1.15E+00 1.95E+00 283.69 1.70 7.92E-01 1.55E+00 300.07 2.47 -4.60E-01 1.21E+00 302.65 2.20 -7.79E-01 1.15E+00 330.06 1.40 6.24E-01 1.96E+00 U-235 143.76 10.96 -8.15E-02 5.07E-02 2.54E-01 163.33 5.08 6.71E-03 5.37E-01 185.71 57.20 1.77E-02 5.07E-02 202.11 1.08 -8.33E-01 2.52E+00 205.31 5.01 -4.91E-02 5.44E-01 Am-241 59.54 35.90 -5.85E-01 5.80E-01 5.80E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [260]
| |
| | |
| 6/25/2019 8:44:44AM Page 1 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS GAMMA SPECTRUM ANALYSIS Sample Identification : 25-Jun-19-10013 Sample Description : L1-10221C-FIGS-101SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.518E+03 grams Facility : Default Sample Taken On : 6/24/2019 9:00:00AM Acquisition Started : 6/25/2019 8:29:13AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 6/25/2019 Efficiency Calibration Description :
| |
| Sample Number : 77600 Fill Height : 1517.55 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 6/25/2019 8:44:35AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [261]
| |
| | |
| 6/25/2019 8:44:44AM Page 2 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.62 950 - 961 954.94 6.91E+01 15.89 6.99E+01 0.85 2 295.15 1176 - 1186 1180.84 2.28E+01 10.21 3.42E+01 0.93 3 351.80 1402 - 1412 1407.20 3.67E+01 9.99 2.63E+01 1.06 4 609.13 2430 - 2442 2435.79 2.77E+01 8.56 1.73E+01 0.73 5 661.48 2636 - 2654 2645.10 3.66E+02 21.46 2.82E+01 1.36 6 911.16 3638 - 3650 3643.69 2.88E+01 6.32 4.18E+00 0.87 7 1173.18 4683 - 4700 4692.10 6.83E+01 9.81 8.70E+00 1.66 8 1460.45 5830 - 5851 5842.16 1.71E+02 14.17 8.08E+00 0.74 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82
| |
| * 10.66 3.59E+00 3.36E-01 Cs-137 0.99 661.66
| |
| * 85.10 5.69E-01 4.78E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.08E-01 2.64E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 7.64E-02 2.40E-02 768.36 4.89 806.18 1.26 934.06 3.11 [262]
| |
| | |
| 6/25/2019 8:44:44AM Page 3 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 9.49E-02 4.32E-02 351.93
| |
| * 35.60 8.94E-02 2.54E-02 785.96 1.06 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.83E-01 4.08E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [263]
| |
| | |
| 6/25/2019 8:44:44AM Page 4 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.978 3.59E+00 3.36E-01 Cs-137 0.995 5.69E-01 4.78E-02 X Bi-211 0.918 Pb-212 1.000 1.08E-01 2.64E-02 Bi-214 0.998 7.64E-02 2.40E-02 Pb-214 0.998 9.08E-02 2.19E-02 Ac-228 1.000 1.83E-01 4.08E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [264]
| |
| | |
| 6/25/2019 8:44:44AM Page 5 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS UNIDENTIFIED PEAKS Peak Locate Performed on : 6/25/2019 8:44:35AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide 7 1173.18 7.58874E-02 14.37 Tol. Co-60 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 4.58E-02 5.66E-02 5.66E-02 BE-7 477.60 10.44 3.40E-01 4.71E-01 4.71E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.59E+00 4.50E-01 4.50E-01 Mn-54 834.85 99.98 3.44E-02 4.76E-02 4.76E-02 Co-60 1173.23 99.85 1.09E-01 8.69E-02 9.70E-02 1332.49 99.98 8.80E-02 8.69E-02 Nb-94 702.65 99.81 1.10E-02 4.55E-02 4.68E-02 871.09 99.89 -1.14E-02 4.55E-02 Ag-108m 79.13 6.60 -3.82E-01 4.72E-02 1.40E+00 433.94 90.50 1.12E-03 4.72E-02 614.28 89.80 1.10E-02 5.66E-02 722.94 90.80 1.84E-03 5.13E-02 Sb-125 176.31 6.84 3.61E-02 1.37E-01 4.48E-01 380.45 1.52 5.04E-01 2.22E+00 427.87 29.60 3.07E-02 1.37E-01 463.36 10.49 2.97E-01 4.48E-01 600.60 17.65 2.58E-01 2.39E-01 606.71 4.98 1.25E+00 1.14E+00 [265]
| |
| | |
| 6/25/2019 8:44:44AM Page 6 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 635.95 11.22 -2.54E-01 1.37E-01 3.25E-01 671.44 1.79 -3.18E-02 2.08E+00 Ba-133 79.61 2.65 4.81E-01 6.96E-02 3.42E+00 81.00 32.90 -2.47E-01 2.40E-01 276.40 7.16 1.49E-01 5.48E-01 302.85 18.34 8.63E-02 2.16E-01 356.01 62.05 -4.48E-02 6.96E-02 383.85 8.94 -1.27E-01 3.72E-01 Cs-134 475.36 1.48 2.35E-01 5.25E-02 3.32E+00 563.25 8.34 -3.90E-02 4.35E-01 569.33 15.37 1.03E-01 2.41E-01 604.72 97.62 -3.43E-02 5.54E-02 795.86 85.46 3.79E-02 5.25E-02 801.95 8.69 -2.44E-01 4.39E-01 1038.61 0.99 -4.06E+00 4.28E+00 1167.97 1.79 -1.49E-01 5.45E+00 1365.19 3.02 3.53E-01 9.60E-01
| |
| + Cs-137 661.66
| |
| * 85.10 5.69E-01 5.58E-02 5.58E-02 Eu-152 121.78 28.67 2.29E-02 1.31E-01 1.31E-01 244.70 7.61 8.43E-02 5.30E-01 295.94 0.45 2.28E+00 9.70E+00 344.28 26.60 -5.11E-03 1.33E-01 367.79 0.86 -2.43E+00 4.19E+00 411.12 2.24 -4.44E-01 1.88E+00 443.96 2.83 7.81E-01 1.74E+00 488.68 0.42 2.64E+00 8.66E+00 563.99 0.49 -3.87E+00 7.18E+00 586.26 0.46 8.04E+00 1.10E+01 678.62 0.47 -2.64E+00 8.31E+00 688.67 0.86 -1.63E+00 4.54E+00 719.35 0.28 -1.84E+00 1.53E+01 778.90 12.96 -1.64E-01 2.88E-01 810.45 0.32 -5.77E+00 1.22E+01 867.37 4.26 -7.14E-01 1.10E+00 919.33 0.43 -8.81E+00 9.55E+00 964.08 14.65 3.11E-01 4.14E-01 1085.87 10.24 3.26E-01 5.29E-01 1089.74 1.73 9.35E-01 3.14E+00 1112.07 13.69 -2.78E-01 3.65E-01 1212.95 1.43 -4.93E+00 3.77E+00 1249.94 0.19 1.77E+01 2.74E+01 1299.14 1.63 1.86E+00 3.08E+00 1408.01 21.07 1.24E-01 2.01E-01 1457.64 0.50 8.15E+01 3.05E+01 1528.10 0.28 -6.24E+00 1.42E+01 Eu-154 123.07 40.40 -3.30E-02 9.19E-02 9.19E-02 247.93 6.89 1.34E-01 5.25E-01 591.76 4.95 -8.94E-01 7.56E-01 692.42 1.78 -1.56E+00 2.20E+00 723.30 20.06 -8.69E-02 2.30E-01 756.80 4.52 -2.64E-01 8.89E-01
| |
| [266]
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| | |
| 6/25/2019 8:44:44AM Page 7 of 7 Analysis Report for 25-Jun-19-10013 L1-10221C-FIGS-101SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 873.18 12.08 2.46E-01 9.19E-02 3.88E-01 996.29 10.48 1.68E-01 4.11E-01 1004.76 18.01 -1.05E-01 2.73E-01 1274.43 34.80 -5.67E-02 1.42E-01 1596.48 1.80 -3.26E+00 1.95E+00 Eu-155 45.30 1.31 -1.16E+01 2.00E-01 1.98E+01 60.01 1.22 -1.86E+01 1.84E+01 86.55 30.70 -4.30E-02 2.10E-01 105.31 21.10 5.31E-02 2.00E-01 Ra-226 186.21 3.64 1.12E+00 1.04E+00 1.04E+00 Pa-231 27.36 10.30 1.66E+00 1.64E+00 2.33E+00 283.69 1.70 -1.81E+00 2.18E+00 300.07 2.47 -8.68E-01 1.64E+00 302.65 2.20 7.41E-01 1.80E+00 330.06 1.40 1.12E-01 2.57E+00 U-235 143.76 10.96 -1.42E-01 6.56E-02 3.16E-01 163.33 5.08 -1.69E-01 6.54E-01 185.71 57.20 5.18E-02 6.56E-02 202.11 1.08 8.95E-03 3.36E+00 205.31 5.01 -8.29E-01 6.82E-01 Am-241 59.54 35.90 -9.99E-02 6.90E-01 6.90E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [267]
| |
| | |
| 7/9/2019 10:24:30AM Page 1 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10026 Sample Description : L1-10221C-FIGS-102SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.647E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:45:00PM Acquisition Started : 7/9/2019 10:09:18AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
| |
| Sample Number : 77834 Fill Height : 1646.93 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:24:21AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [268]
| |
| | |
| 7/9/2019 10:24:30AM Page 2 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.66 469 - 481 477.51 1.26E+02 22.18 1.39E+02 1.21 2 295.33 586 - 595 590.72 3.99E+01 12.48 5.11E+01 1.02 3 351.88 700 - 708 703.71 6.24E+01 11.66 3.46E+01 1.03 4 583.21 1161 - 1171 1166.03 5.53E+01 9.91 1.77E+01 0.94 5 609.44 1215 - 1223 1218.46 3.82E+01 8.99 1.98E+01 1.18 6 661.88 1318 - 1328 1323.29 6.66E+01 10.73 2.04E+01 1.34 7 911.31 1817 - 1826 1822.07 4.38E+01 8.30 1.12E+01 1.19 8 1460.91 2915 - 2929 2921.88 2.35E+02 16.01 7.50E+00 1.84 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 4.32E+00 3.50E-01 Cs-137 0.99 661.66
| |
| * 85.10 9.16E-02 1.57E-02 Tl-208 1.00 583.19
| |
| * 85.00 7.02E-02 1.33E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.74E-01 3.38E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 9.33E-02 2.27E-02 768.36 4.89 806.18 1.26 [269]
| |
| | |
| 7/9/2019 10:24:30AM Page 3 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 1.48E-01 4.76E-02 351.93
| |
| * 35.60 1.35E-01 2.74E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 2.45E-01 4.76E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [270]
| |
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| 7/9/2019 10:24:30AM Page 4 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 4.32E+00 3.50E-01 Cs-137 0.992 9.16E-02 1.57E-02 Tl-208 1.000 7.02E-02 1.33E-02 X Bi-211 0.900 Pb-212 1.000 1.74E-01 3.38E-02 Bi-214 0.999 9.33E-02 2.27E-02 Pb-214 0.999 1.38E-01 2.38E-02 Ac-228 0.999 2.45E-01 4.76E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [271]
| |
| | |
| 7/9/2019 10:24:30AM Page 5 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:24:21AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.28E-02 5.01E-02 5.01E-02 BE-7 477.60 10.44 2.42E-01 3.78E-01 3.78E-01
| |
| + K-40 1460.82
| |
| * 10.66 4.32E+00 3.44E-01 3.44E-01 Mn-54 834.85 99.98 8.97E-05 3.24E-02 3.24E-02 Co-60 1173.23 99.85 1.55E-02 5.11E-02 5.57E-02 1332.49 99.98 2.60E-02 5.11E-02 Nb-94 702.65 99.81 1.85E-02 3.33E-02 3.39E-02 871.09 99.89 -2.60E-02 3.33E-02 Ag-108m 79.13 6.60 6.64E-01 3.26E-02 1.12E+00 433.94 90.50 -6.76E-03 3.26E-02 614.28 89.80 -2.05E-02 4.57E-02 722.94 90.80 -2.31E-02 4.04E-02 Sb-125 176.31 6.84 -9.61E-02 9.29E-02 4.53E-01 380.45 1.52 1.79E-01 1.97E+00 427.87 29.60 -6.27E-02 9.29E-02 463.36 10.49 8.41E-02 3.40E-01 600.60 17.65 -4.03E-02 1.87E-01 606.71 4.98 -5.67E-01 1.02E+00 635.95 11.22 -9.57E-03 2.73E-01 [272]
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| 7/9/2019 10:24:30AM Page 6 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.65E-01 9.29E-02 1.80E+00 Ba-133 79.61 2.65 5.50E-01 6.42E-02 2.59E+00 81.00 32.90 -1.98E-01 1.74E-01 276.40 7.16 1.08E-01 4.46E-01 302.85 18.34 2.08E-01 1.87E-01 356.01 62.05 -1.46E-02 6.42E-02 383.85 8.94 -3.50E-03 3.21E-01 Cs-134 475.36 1.48 1.76E+00 4.39E-02 2.67E+00 563.25 8.34 7.23E-02 3.85E-01 569.33 15.37 -7.64E-03 1.89E-01 604.72 97.62 -4.63E-02 4.39E-02 795.86 85.46 1.53E-02 4.64E-02 801.95 8.69 -3.41E-01 3.63E-01 1038.61 0.99 -1.39E+00 4.18E+00 1167.97 1.79 4.37E-01 3.13E+00 1365.19 3.02 -4.73E-01 1.02E+00
| |
| + Cs-137 661.66
| |
| * 85.10 9.16E-02 3.64E-02 3.64E-02 Eu-152 121.78 28.67 1.26E-02 1.06E-01 1.06E-01 244.70 7.61 4.45E-03 4.44E-01 295.94 0.45 1.17E+00 7.81E+00 344.28 26.60 -1.05E-01 1.09E-01 367.79 0.86 -4.47E-01 3.57E+00 411.12 2.24 4.30E-01 1.38E+00 443.96 2.83 2.64E-01 1.06E+00 488.68 0.42 3.48E+00 7.68E+00 563.99 0.49 2.53E+00 6.54E+00 586.26 0.46 -1.44E-01 1.12E+01 678.62 0.47 7.21E-01 6.77E+00 688.67 0.86 -1.54E+00 3.55E+00 719.35 0.28 4.32E+00 1.17E+01 778.90 12.96 -8.68E-02 2.27E-01 810.45 0.32 4.48E+00 1.12E+01 867.37 4.26 -3.11E-01 7.97E-01 919.33 0.43 6.78E-01 8.78E+00 964.08 14.65 -1.11E-02 3.69E-01 1085.87 10.24 1.17E-01 4.00E-01 1089.74 1.73 -1.05E+00 2.27E+00 1112.07 13.69 4.01E-02 3.74E-01 1212.95 1.43 -2.65E+00 3.26E+00 1249.94 0.19 6.43E+00 2.59E+01 1299.14 1.63 -3.92E-01 2.17E+00 1408.01 21.07 -3.98E-02 1.71E-01 1457.64 0.50 -2.60E+00 3.04E+01 1528.10 0.28 -3.33E+00 8.99E+00 Eu-154 123.07 40.40 -4.43E-02 6.99E-02 6.99E-02 247.93 6.89 -2.92E-02 4.12E-01 591.76 4.95 9.25E-02 6.70E-01 692.42 1.78 5.43E-01 1.82E+00 723.30 20.06 -6.40E-02 1.96E-01 756.80 4.52 5.03E-02 7.45E-01 873.18 12.08 1.36E-01 3.17E-01
| |
| [273]
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| 7/9/2019 10:24:30AM Page 7 of 7 Analysis Report for 09-Jul-19-10026 L1-10221C-FIGS-102SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -8.33E-03 6.99E-02 3.04E-01 1004.76 18.01 1.45E-01 2.49E-01 1274.43 34.80 4.53E-02 1.35E-01 1596.48 1.80 1.14E-01 2.02E+00 Eu-155 45.30 1.31 2.26E+00 1.70E-01 1.12E+01 60.01 1.22 -4.41E+00 1.08E+01 86.55 30.70 9.49E-02 1.70E-01 105.31 21.10 -6.96E-03 1.80E-01 Ra-226 186.21 3.64 2.39E-02 8.54E-01 8.54E-01 Pa-231 27.36 10.30 8.34E-01 1.14E+00 1.14E+00 283.69 1.70 9.46E-02 1.76E+00 300.07 2.47 3.09E-01 1.26E+00 302.65 2.20 1.73E+00 1.55E+00 330.06 1.40 2.97E-01 2.17E+00 U-235 143.76 10.96 -1.38E-02 5.60E-02 2.68E-01 163.33 5.08 -1.34E-01 6.32E-01 185.71 57.20 2.66E-02 5.60E-02 202.11 1.08 -1.43E+00 2.81E+00 205.31 5.01 -2.01E-01 6.36E-01 Am-241 59.54 35.90 -7.79E-02 3.91E-01 3.91E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [274]
| |
| | |
| 7/9/2019 10:24:40AM Page 1 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10027 Sample Description : L1-10221C-FIGS-103SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.543E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:47:00PM Acquisition Started : 7/9/2019 10:09:29AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.2 seconds Dead Time : 0.13 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
| |
| Sample Number : 77835 Fill Height : 1542.77 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:24:33AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [275]
| |
| | |
| 7/9/2019 10:24:40AM Page 2 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.52 945 - 961 954.16 1.22E+02 17.32 5.60E+01 0.85 2 351.77 1402 - 1414 1406.80 5.22E+01 9.68 1.58E+01 0.99 3 477.16 1903 - 1913 1908.06 3.00E+01 9.08 2.20E+01 0.62 4 510.79 2038 - 2047 2042.49 1.41E+01 8.20 2.29E+01 0.41 5 582.61 2325 - 2335 2329.64 3.19E+01 7.01 7.05E+00 0.40 6 608.83 2429 - 2443 2434.50 4.54E+01 7.79 5.57E+00 0.80 7 661.39 2637 - 2651 2644.65 8.73E+01 10.19 5.67E+00 0.55 8 910.57 3636 - 3646 3641.25 1.81E+01 5.87 5.92E+00 0.71 9 1459.91 5829 - 5849 5839.47 1.76E+02 13.96 5.25E+00 1.53 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 0.99 511.00
| |
| * 100.00 1.84E-02 1.08E-02 BE-7 0.96 477.60
| |
| * 10.44 3.59E-01 1.12E-01 K-40 0.87 1460.82
| |
| * 10.66 4.37E+00 3.95E-01 Cs-137 0.98 661.66
| |
| * 85.10 1.58E-01 2.08E-02 Tl-208 0.94 583.19
| |
| * 85.00 5.32E-02 1.21E-02 Bi-211 0.92 351.07
| |
| * 13.02 3.99E-01 8.06E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 2.18E-01 3.56E-02[276]
| |
| | |
| 7/9/2019 10:24:40AM Page 3 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-212 0.99 300.09 3.30 Bi-214 0.98 609.32
| |
| * 45.49 1.46E-01 2.65E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.46E-01 2.95E-02 785.96 1.06 Ac-228 0.98 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.34E-01 4.40E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [277]
| |
| | |
| 7/9/2019 10:24:40AM Page 4 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| An Pk 0.993 1.84E-02 1.08E-02 BE-7 0.969 3.59E-01 1.12E-01 K-40 0.876 4.37E+00 3.95E-01 Cs-137 0.988 1.58E-01 2.08E-02 Tl-208 0.948 5.32E-02 1.21E-02
| |
| ? Bi-211 0.925 3.99E-01 8.06E-02 Pb-212 0.998 2.18E-01 3.56E-02 Bi-214 0.985 1.46E-01 2.65E-02
| |
| ? Pb-214 0.998 1.46E-01 2.95E-02 Ac-228 0.981 1.34E-01 4.40E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [278]
| |
| | |
| 7/9/2019 10:24:40AM Page 5 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:24:33AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 1.84E-02 3.62E-02 3.62E-02
| |
| + BE-7 477.60
| |
| * 10.44 3.59E-01 3.29E-01 3.29E-01
| |
| + K-40 1460.82
| |
| * 10.66 4.37E+00 4.39E-01 4.39E-01 Mn-54 834.85 99.98 4.52E-02 4.86E-02 4.86E-02 Co-60 1173.23 99.85 5.84E-02 6.40E-02 6.83E-02 1332.49 99.98 5.69E-02 6.40E-02 Nb-94 702.65 99.81 -1.25E-02 4.10E-02 4.25E-02 871.09 99.89 -2.80E-02 4.10E-02 Ag-108m 79.13 6.60 8.99E-01 3.83E-02 1.73E+00 433.94 90.50 -5.88E-02 3.83E-02 614.28 89.80 -1.01E-02 4.69E-02 722.94 90.80 -9.04E-03 5.78E-02 Sb-125 176.31 6.84 1.70E-01 1.31E-01 5.76E-01 380.45 1.52 1.34E+00 2.74E+00 427.87 29.60 4.40E-02 1.31E-01 463.36 10.49 -6.43E-02 4.29E-01 600.60 17.65 -9.04E-02 2.12E-01 606.71 4.98 1.58E+00 1.22E+00 635.95 11.22 1.10E-01 4.02E-01 [279]
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| 7/9/2019 10:24:40AM Page 6 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 8.69E-01 1.31E-01 2.07E+00 Ba-133 79.61 2.65 1.75E+00 7.00E-02 4.13E+00 81.00 32.90 -2.49E-01 2.84E-01 276.40 7.16 2.60E-01 5.17E-01 302.85 18.34 1.32E-01 2.07E-01 356.01 62.05 -7.81E-03 7.00E-02 383.85 8.94 1.64E-02 4.44E-01 Cs-134 475.36 1.48 3.17E+00 6.05E-02 3.98E+00 563.25 8.34 8.48E-03 4.30E-01 569.33 15.37 -3.99E-02 2.39E-01 604.72 97.62 -3.56E-02 6.05E-02 795.86 85.46 5.71E-03 6.23E-02 801.95 8.69 1.94E-01 6.24E-01 1038.61 0.99 -3.16E+00 5.27E+00 1167.97 1.79 -1.42E+00 3.40E+00 1365.19 3.02 -4.55E-01 1.44E+00
| |
| + Cs-137 661.66
| |
| * 85.10 1.58E-01 3.02E-02 3.02E-02 Eu-152 121.78 28.67 -9.37E-03 1.55E-01 1.55E-01 244.70 7.61 -3.78E-01 4.90E-01 295.94 0.45 -2.73E+00 8.84E+00 344.28 26.60 7.58E-02 1.65E-01 367.79 0.86 1.76E+00 3.87E+00 411.12 2.24 7.73E-01 1.74E+00 443.96 2.83 -1.35E-01 1.35E+00 488.68 0.42 -4.51E+00 8.98E+00 563.99 0.49 4.16E+00 7.44E+00 586.26 0.46 -6.95E+00 1.21E+01 678.62 0.47 3.59E-01 7.34E+00 688.67 0.86 -1.58E-01 4.87E+00 719.35 0.28 2.05E+00 1.54E+01 778.90 12.96 2.46E-02 3.88E-01 810.45 0.32 -1.33E+01 1.04E+01 867.37 4.26 -3.32E-01 8.17E-01 919.33 0.43 3.32E-01 1.05E+01 964.08 14.65 3.02E-01 4.82E-01 1085.87 10.24 -1.22E-01 4.11E-01 1089.74 1.73 4.51E-01 2.60E+00 1112.07 13.69 -4.41E-01 3.81E-01 1212.95 1.43 1.65E+00 3.69E+00 1249.94 0.19 -1.94E+00 3.37E+01 1299.14 1.63 -3.07E+00 2.03E+00 1408.01 21.07 -5.81E-02 2.55E-01 1457.64 0.50 9.61E+01 3.60E+01 1528.10 0.28 2.78E-01 1.52E+01 Eu-154 123.07 40.40 2.47E-02 1.07E-01 1.07E-01 247.93 6.89 -2.54E-02 5.33E-01 591.76 4.95 4.75E-01 8.55E-01 692.42 1.78 1.03E+00 2.49E+00 723.30 20.06 -1.17E-01 2.55E-01 756.80 4.52 -2.83E-01 1.17E+00 873.18 12.08 3.08E-01 3.75E-01
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| [280]
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| 7/9/2019 10:24:40AM Page 7 of 7 Analysis Report for 09-Jul-19-10027 L1-10221C-FIGS-103SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.18E-02 1.07E-01 4.05E-01 1004.76 18.01 5.41E-02 2.51E-01 1274.43 34.80 7.58E-02 1.30E-01 1596.48 1.80 1.26E+00 2.60E+00 Eu-155 45.30 1.31 -7.78E+00 2.40E-01 2.99E+01 60.01 1.22 1.35E+01 3.00E+01 86.55 30.70 -9.35E-02 2.40E-01 105.31 21.10 4.94E-03 2.63E-01 Ra-226 186.21 3.64 1.01E+00 1.17E+00 1.17E+00 Pa-231 27.36 10.30 1.28E+00 1.47E+00 3.16E+00 283.69 1.70 -9.07E-01 2.08E+00 300.07 2.47 -1.09E+00 1.47E+00 302.65 2.20 5.65E-01 1.68E+00 330.06 1.40 4.57E-01 2.65E+00 U-235 143.76 10.96 -1.61E-01 7.46E-02 3.70E-01 163.33 5.08 5.63E-02 7.61E-01 185.71 57.20 6.29E-02 7.46E-02 202.11 1.08 -8.90E-01 3.33E+00 205.31 5.01 -4.62E-02 7.65E-01 Am-241 59.54 35.90 -1.50E-01 1.03E+00 1.03E+00
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [281]
| |
| | |
| 7/9/2019 10:24:59AM Page 1 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10028 Sample Description : L1-10221C-FIGS-104SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.648E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:49:00PM Acquisition Started : 7/9/2019 10:09:37AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
| |
| Sample Number : 77836 Fill Height : 1648.34 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:24:52AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [282]
| |
| | |
| 7/9/2019 10:24:59AM Page 2 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.42 307 - 316 310.21 2.05E+01 10.68 4.05E+01 0.73 2 238.68 949 - 962 954.30 7.55E+01 12.77 3.15E+01 0.86 3 351.97 1401 - 1413 1406.90 4.55E+01 9.47 1.65E+01 1.08 4 477.59 1902 - 1916 1908.83 4.08E+01 8.55 1.13E+01 1.02 5 911.25 3638 - 3648 3642.46 2.21E+01 6.11 5.93E+00 0.45 6 1460.33 5830 - 5850 5839.28 1.46E+02 13.26 8.07E+00 0.46 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty BE-7 1.00 477.60
| |
| * 10.44 4.34E-01 9.62E-02 K-40 0.96 1460.82
| |
| * 10.66 3.21E+00 3.23E-01 Bi-211 0.87 351.07
| |
| * 13.02 3.09E-01 6.89E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.18E-01 2.22E-02 300.09 3.30 Pb212-XR 0.99 74.82 10.28 77.11
| |
| * 17.10 1.42E-01 7.55E-02 87.35 3.97 89.78 1.46 Pb-214 1.00 241.99 7.25 [283]
| |
| | |
| 7/9/2019 10:24:59AM Page 3 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-214 1.00 295.22 18.42 351.93
| |
| * 35.60 1.13E-01 2.52E-02 785.96 1.06 Pb214-XR 0.99 74.82 5.80 77.11
| |
| * 9.70 2.51E-01 1.34E-01 87.35 2.24 89.78 0.82 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.46E-01 4.08E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| BE-7 1.000 4.34E-01 9.62E-02 K-40 0.963 3.21E+00 3.23E-01
| |
| ? Bi-211 0.878 3.09E-01 6.89E-02 Pb-212 1.000 1.18E-01 2.22E-02
| |
| ? Pb212-XR 0.992 1.42E-01 7.55E-02
| |
| ? Pb-214 1.000 1.13E-01 2.52E-02
| |
| ? Pb214-XR 0.992 2.51E-01 1.34E-01 Ac-228 1.000 1.46E-01 4.08E-02 [284]
| |
| | |
| 7/9/2019 10:24:59AM Page 4 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [285]
| |
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| 7/9/2019 10:24:59AM Page 5 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:24:52AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.53E-02 4.84E-02 4.84E-02
| |
| + BE-7 477.60
| |
| * 10.44 4.34E-01 2.36E-01 2.36E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.21E+00 4.71E-01 4.71E-01 Mn-54 834.85 99.98 1.24E-02 3.73E-02 3.73E-02 Co-60 1173.23 99.85 2.70E-02 3.77E-02 4.90E-02 1332.49 99.98 1.97E-02 3.77E-02 Nb-94 702.65 99.81 2.89E-03 3.44E-02 3.63E-02 871.09 99.89 6.19E-03 3.44E-02 Ag-108m 79.13 6.60 1.55E-01 3.36E-02 8.46E-01 433.94 90.50 2.04E-02 3.36E-02 614.28 89.80 -2.79E-02 4.60E-02 722.94 90.80 -4.32E-02 3.90E-02 Sb-125 176.31 6.84 -2.42E-01 9.55E-02 3.35E-01 380.45 1.52 1.75E-01 1.63E+00 427.87 29.60 -1.25E-02 9.55E-02 463.36 10.49 1.03E-01 3.16E-01 600.60 17.65 -7.28E-03 1.52E-01 606.71 4.98 1.30E+00 9.56E-01 635.95 11.22 -2.11E-01 2.55E-01 [286]
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| 7/9/2019 10:24:59AM Page 6 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 9.33E-01 9.55E-02 1.71E+00 Ba-133 79.61 2.65 4.51E-01 5.57E-02 2.08E+00 81.00 32.90 -1.12E-01 1.26E-01 276.40 7.16 4.41E-03 4.08E-01 302.85 18.34 -2.43E-02 1.47E-01 356.01 62.05 -1.68E-02 5.57E-02 383.85 8.94 -1.17E-01 2.62E-01 Cs-134 475.36 1.48 -2.73E-01 3.85E-02 3.11E+00 563.25 8.34 -3.18E-01 3.74E-01 569.33 15.37 1.03E-01 2.05E-01 604.72 97.62 -2.42E-02 3.85E-02 795.86 85.46 6.48E-03 4.32E-02 801.95 8.69 3.51E-02 4.07E-01 1038.61 0.99 -4.18E+00 3.39E+00 1167.97 1.79 -1.38E+00 2.60E+00 1365.19 3.02 -1.82E+00 1.21E+00 Cs-137 661.66 85.10 7.55E-03 4.25E-02 4.25E-02 Eu-152 121.78 28.67 4.45E-02 9.46E-02 9.46E-02 244.70 7.61 2.76E-01 3.93E-01 295.94 0.45 1.91E+00 7.91E+00 344.28 26.60 3.52E-02 1.01E-01 367.79 0.86 6.28E-01 3.22E+00 411.12 2.24 9.53E-01 1.36E+00 443.96 2.83 2.20E-01 8.77E-01 488.68 0.42 2.68E+00 7.14E+00 563.99 0.49 -4.27E+00 5.96E+00 586.26 0.46 8.65E+00 1.01E+01 678.62 0.47 6.21E+00 7.35E+00 688.67 0.86 -2.34E+00 3.52E+00 719.35 0.28 -3.25E+00 1.37E+01 778.90 12.96 1.39E-01 2.99E-01 810.45 0.32 3.74E+00 9.87E+00 867.37 4.26 2.29E-01 8.51E-01 919.33 0.43 -6.79E+00 6.23E+00 964.08 14.65 5.76E-02 3.24E-01 1085.87 10.24 1.26E-01 3.89E-01 1089.74 1.73 6.76E-01 2.75E+00 1112.07 13.69 -2.87E-01 3.04E-01 1212.95 1.43 4.65E-01 3.58E+00 1249.94 0.19 1.33E+01 2.16E+01 1299.14 1.63 3.37E-01 2.48E+00 1408.01 21.07 -5.14E-02 1.78E-01 1457.64 0.50 6.94E+01 2.97E+01 1528.10 0.28 5.16E+00 1.26E+01 Eu-154 123.07 40.40 2.38E-02 6.73E-02 6.73E-02 247.93 6.89 -3.53E-01 3.57E-01 591.76 4.95 1.09E-01 7.14E-01 692.42 1.78 -2.15E-01 1.71E+00 723.30 20.06 -1.08E-01 1.84E-01 756.80 4.52 4.23E-01 8.59E-01 873.18 12.08 -4.12E-01 2.57E-01
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| [287]
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| 7/9/2019 10:24:59AM Page 7 of 7 Analysis Report for 09-Jul-19-10028 L1-10221C-FIGS-104SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 6.47E-02 6.73E-02 3.70E-01 1004.76 18.01 -2.49E-02 2.10E-01 1274.43 34.80 9.15E-02 1.31E-01 1596.48 1.80 6.98E-01 1.90E+00 Eu-155 45.30 1.31 1.52E+00 1.54E-01 8.61E+00 60.01 1.22 4.66E+00 1.05E+01 86.55 30.70 1.17E-01 1.64E-01 105.31 21.10 4.06E-02 1.54E-01 Ra-226 186.21 3.64 1.42E-01 7.51E-01 7.51E-01 Pa-231 27.36 10.30 9.28E-01 1.09E+00 1.09E+00 283.69 1.70 -5.86E-02 1.50E+00 300.07 2.47 -9.36E-01 1.24E+00 302.65 2.20 4.30E-01 1.23E+00 330.06 1.40 8.08E-01 2.12E+00 U-235 143.76 10.96 2.46E-02 4.91E-02 2.69E-01 163.33 5.08 3.32E-02 5.22E-01 185.71 57.20 1.90E-02 4.91E-02 202.11 1.08 5.93E-01 2.32E+00 205.31 5.01 -5.99E-02 5.20E-01 Am-241 59.54 35.90 1.40E-01 3.72E-01 3.72E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [288]
| |
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| 7/9/2019 10:25:05AM Page 1 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10029 Sample Description : L1-10221C-FIGS-105SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.613E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:51:00PM Acquisition Started : 7/9/2019 10:09:45AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
| |
| Sample Number : 77837 Fill Height : 1612.90 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:24:55AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [289]
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| 7/9/2019 10:25:05AM Page 2 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.61 950 - 962 954.90 9.43E+01 13.38 2.97E+01 1.15 2 351.97 1403 - 1413 1407.87 3.71E+01 9.06 1.89E+01 0.40 3 477.71 1905 - 1917 1910.41 2.72E+01 7.73 1.18E+01 0.60 4 583.19 2326 - 2337 2332.07 2.17E+01 7.44 1.33E+01 0.44 5 609.44 2431 - 2444 2437.04 2.77E+01 7.44 9.28E+00 0.64 6 661.79 2642 - 2651 2646.35 1.84E+01 5.37 4.61E+00 0.50 7 969.04 3870 - 3881 3875.23 2.60E+01 5.10 0.00E+00 0.58 8 1460.72 5831 - 5853 5843.24 1.50E+02 13.12 5.65E+00 1.41 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty BE-7 0.99 477.60
| |
| * 10.44 2.79E-01 8.15E-02 K-40 0.99 1460.82
| |
| * 10.66 3.10E+00 3.02E-01 Cs-137 0.99 661.66
| |
| * 85.10 2.82E-02 8.41E-03 Tl-208 1.00 583.19
| |
| * 85.00 3.07E-02 1.07E-02 Bi-211 0.87 351.07
| |
| * 13.02 2.44E-01 6.29E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.46E-01 2.39E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 7.54E-02 2.07E-02[290]
| |
| | |
| 7/9/2019 10:25:05AM Page 3 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 8.94E-02 2.30E-02 785.96 1.06 Ac-228 0.57 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20 25.80 964.77 4.99 968.97
| |
| * 15.80 2.76E-01 5.54E-02 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [291]
| |
| | |
| 7/9/2019 10:25:05AM Page 4 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| BE-7 0.998 2.79E-01 8.15E-02 K-40 0.998 3.10E+00 3.02E-01 Cs-137 0.997 2.82E-02 8.41E-03 Tl-208 1.000 3.07E-02 1.07E-02
| |
| ? Bi-211 0.879 2.44E-01 6.29E-02 Pb-212 1.000 1.46E-01 2.39E-02 Bi-214 0.999 7.54E-02 2.07E-02
| |
| ? Pb-214 1.000 8.94E-02 2.30E-02 Ac-228 0.571 2.76E-01 5.54E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [292]
| |
| | |
| 7/9/2019 10:25:05AM Page 5 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:24:55AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 7.68E-02 5.08E-02 5.08E-02
| |
| + BE-7 477.60
| |
| * 10.44 2.79E-01 2.27E-01 2.27E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.10E+00 3.86E-01 3.86E-01 Mn-54 834.85 99.98 2.58E-02 3.94E-02 3.94E-02 Co-60 1173.23 99.85 4.93E-02 4.15E-02 5.18E-02 1332.49 99.98 2.67E-02 4.15E-02 Nb-94 702.65 99.81 1.34E-02 3.72E-02 4.02E-02 871.09 99.89 -8.59E-03 3.72E-02 Ag-108m 79.13 6.60 -3.56E-01 3.19E-02 1.24E+00 433.94 90.50 3.66E-03 3.19E-02 614.28 89.80 -1.56E-02 5.14E-02 722.94 90.80 -6.71E-03 4.09E-02 Sb-125 176.31 6.84 -2.00E-01 9.81E-02 3.75E-01 380.45 1.52 -1.14E+00 1.77E+00 427.87 29.60 -2.51E-02 9.81E-02 463.36 10.49 1.43E-01 2.83E-01 600.60 17.65 1.95E-01 1.96E-01 606.71 4.98 5.67E-01 9.03E-01 635.95 11.22 -1.80E-01 2.70E-01 [293]
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| 7/9/2019 10:25:05AM Page 6 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.40E-01 9.81E-02 1.48E+00 Ba-133 79.61 2.65 5.34E-01 6.03E-02 2.96E+00 81.00 32.90 -2.45E-01 2.03E-01 276.40 7.16 1.44E-01 4.51E-01 302.85 18.34 -6.13E-03 1.68E-01 356.01 62.05 -2.46E-02 6.03E-02 383.85 8.94 1.51E-01 3.31E-01 Cs-134 475.36 1.48 1.73E+00 3.90E-02 2.79E+00 563.25 8.34 -3.43E-01 3.20E-01 569.33 15.37 -3.62E-02 1.92E-01 604.72 97.62 -4.09E-02 4.09E-02 795.86 85.46 -1.98E-02 3.90E-02 801.95 8.69 -1.84E-01 4.05E-01 1038.61 0.99 -2.04E+00 3.69E+00 1167.97 1.79 -1.40E+00 2.68E+00 1365.19 3.02 -7.44E-02 1.08E+00
| |
| + Cs-137 661.66
| |
| * 85.10 2.82E-02 2.12E-02 2.12E-02 Eu-152 121.78 28.67 2.63E-02 8.99E-02 1.14E-01 244.70 7.61 1.13E-01 3.81E-01 295.94 0.45 1.74E+00 7.41E+00 344.28 26.60 -8.43E-02 8.99E-02 367.79 0.86 1.75E-01 3.52E+00 411.12 2.24 1.01E-01 1.32E+00 443.96 2.83 -2.68E-01 1.14E+00 488.68 0.42 6.38E-02 7.55E+00 563.99 0.49 -2.05E+00 5.43E+00 586.26 0.46 7.58E+00 1.00E+01 678.62 0.47 2.80E+00 6.03E+00 688.67 0.86 -1.48E+00 3.15E+00 719.35 0.28 1.41E+00 1.23E+01 778.90 12.96 -8.64E-02 2.40E-01 810.45 0.32 7.21E+00 1.31E+01 867.37 4.26 2.83E-01 9.45E-01 919.33 0.43 -2.25E+00 9.00E+00 964.08 14.65 -2.21E-01 4.16E-01 1085.87 10.24 -1.56E-01 3.18E-01 1089.74 1.73 -3.34E-01 2.48E+00 1112.07 13.69 -1.00E-01 3.18E-01 1212.95 1.43 -7.21E-01 3.44E+00 1249.94 0.19 7.17E+00 2.03E+01 1299.14 1.63 -1.90E+00 2.82E+00 1408.01 21.07 2.94E-02 1.75E-01 1457.64 0.50 6.55E+01 2.78E+01 1528.10 0.28 -3.03E+00 1.10E+01 Eu-154 123.07 40.40 -2.55E-02 7.79E-02 7.79E-02 247.93 6.89 -2.16E-01 3.41E-01 591.76 4.95 2.24E-01 6.59E-01 692.42 1.78 3.45E-02 1.71E+00 723.30 20.06 5.64E-02 1.88E-01 756.80 4.52 -8.29E-03 7.50E-01 873.18 12.08 -2.78E-01 3.22E-01
| |
| [294]
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| 7/9/2019 10:25:05AM Page 7 of 7 Analysis Report for 09-Jul-19-10029 L1-10221C-FIGS-105SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -6.16E-02 7.79E-02 3.59E-01 1004.76 18.01 1.33E-01 1.98E-01 1274.43 34.80 -8.32E-02 1.16E-01 1596.48 1.80 -9.49E-01 1.63E+00 Eu-155 45.30 1.31 -7.25E+00 1.82E-01 1.54E+01 60.01 1.22 -7.21E+00 1.86E+01 86.55 30.70 -1.51E-03 1.83E-01 105.31 21.10 -7.81E-02 1.82E-01 Ra-226 186.21 3.64 8.41E-02 8.51E-01 8.51E-01 Pa-231 27.36 10.30 1.30E+00 1.36E+00 1.76E+00 283.69 1.70 -2.98E-01 1.88E+00 300.07 2.47 -5.02E-01 1.36E+00 302.65 2.20 -2.12E-01 1.41E+00 330.06 1.40 -1.23E+00 2.39E+00 U-235 143.76 10.96 -1.27E-01 5.43E-02 2.82E-01 163.33 5.08 -2.34E-01 5.86E-01 185.71 57.20 1.43E-02 5.43E-02 202.11 1.08 3.08E-01 2.57E+00 205.31 5.01 -4.31E-01 5.65E-01 Am-241 59.54 35.90 -7.23E-03 6.67E-01 6.67E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [295]
| |
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| 7/9/2019 10:42:53AM Page 1 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10030 Sample Description : L1-10221C-FIGS-106SS Sample Type : Soil Unit :
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| Sample Point :
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| Sample Size : 1.676E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:53:00PM Acquisition Started : 7/9/2019 10:27:41AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
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| Sample Number : 77838 Fill Height : 1675.50 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:42:44AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
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| [296]
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| 7/9/2019 10:42:53AM Page 2 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.81 474 - 481 477.81 1.04E+02 15.63 6.75E+01 1.55 2 352.00 700 - 708 703.94 6.90E+01 11.44 2.90E+01 1.51 3 583.32 1161 - 1169 1166.24 3.66E+01 8.34 1.54E+01 1.14 4 609.09 1212 - 1223 1217.76 6.79E+01 9.13 6.07E+00 1.24 5 661.79 1319 - 1328 1323.11 3.35E+01 7.86 1.25E+01 0.85 6 1460.85 2916 - 2928 2921.76 1.65E+02 13.55 6.80E+00 1.64 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
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| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1.00 1460.82
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| * 10.66 3.03E+00 2.82E-01 Cs-137 0.99 661.66
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| * 85.10 4.60E-02 1.11E-02 Tl-208 0.99 583.19
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| * 85.00 4.63E-02 1.09E-02 Bi-211 0.87 351.07
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| * 13.02 4.07E-01 7.50E-02 Pb-212 0.99 115.18 0.60 238.63
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| * 43.60 1.44E-01 2.46E-02 300.09 3.30 Bi-214 0.99 609.32
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| * 45.49 1.65E-01 2.43E-02 768.36 4.89 806.18 1.26 934.06 3.11 [297]
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| 7/9/2019 10:42:53AM Page 3 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
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| * 35.60 1.49E-01 2.74E-02 785.96 1.06
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| * = Energy line found in the spectrum.
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| - = Manually added nuclide.
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| ? = Manually edited nuclide.
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| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| K-40 1.000 3.03E+00 2.82E-01 Cs-137 0.997 4.60E-02 1.11E-02 Tl-208 0.997 4.63E-02 1.09E-02
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| ? Bi-211 0.872 4.07E-01 7.50E-02 Pb-212 0.995 1.44E-01 2.46E-02 Bi-214 0.997 1.65E-01 2.43E-02
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| ? Pb-214 1.000 1.49E-01 2.74E-02
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| [298]
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| 7/9/2019 10:42:53AM Page 4 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS
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| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
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| [299]
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| 7/9/2019 10:42:53AM Page 5 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:42:44AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
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| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
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| An Pk 511.00 100.00 6.26E-02 4.62E-02 4.62E-02 BE-7 477.60 10.44 2.33E-01 3.39E-01 3.39E-01
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| + K-40 1460.82
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| * 10.66 3.03E+00 3.21E-01 3.21E-01 Mn-54 834.85 99.98 3.11E-03 2.83E-02 2.83E-02 Co-60 1173.23 99.85 2.97E-02 3.69E-02 4.62E-02 1332.49 99.98 1.24E-02 3.69E-02 Nb-94 702.65 99.81 1.23E-02 3.47E-02 3.49E-02 871.09 99.89 1.85E-02 3.47E-02 Ag-108m 79.13 6.60 1.37E-01 3.05E-02 9.77E-01 433.94 90.50 -2.18E-03 3.05E-02 614.28 89.80 -4.17E-02 4.34E-02 722.94 90.80 7.90E-03 3.85E-02 Sb-125 176.31 6.84 7.07E-03 9.95E-02 4.43E-01 380.45 1.52 -1.07E-01 1.95E+00 427.87 29.60 -1.02E-02 9.95E-02 463.36 10.49 5.29E-02 3.02E-01 600.60 17.65 1.06E-02 1.89E-01 606.71 4.98 -1.85E-01 1.02E+00 635.95 11.22 6.58E-02 2.63E-01 [300]
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| 7/9/2019 10:42:53AM Page 6 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
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| (keV)
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| Sb-125 671.44 1.79 6.32E-02 9.95E-02 1.57E+00 Ba-133 79.61 2.65 1.88E-01 6.03E-02 2.32E+00 81.00 32.90 -1.14E-01 1.64E-01 276.40 7.16 -2.25E-01 3.91E-01 302.85 18.34 9.78E-02 1.56E-01 356.01 62.05 -3.08E-02 6.03E-02 383.85 8.94 -1.15E-01 2.85E-01 Cs-134 475.36 1.48 1.18E+00 3.49E-02 2.45E+00 563.25 8.34 -4.32E-02 3.51E-01 569.33 15.37 -5.93E-03 1.92E-01 604.72 97.62 -7.83E-03 4.55E-02 795.86 85.46 -2.09E-02 3.49E-02 801.95 8.69 -6.80E-02 3.86E-01 1038.61 0.99 4.98E-01 3.67E+00 1167.97 1.79 -2.25E+00 2.07E+00 1365.19 3.02 -4.63E-01 8.40E-01
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| + Cs-137 661.66
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| * 85.10 4.60E-02 2.87E-02 2.87E-02 Eu-152 121.78 28.67 -5.86E-03 1.00E-01 1.00E-01 244.70 7.61 -3.30E-01 3.81E-01 295.94 0.45 6.27E+00 7.40E+00 344.28 26.60 -5.27E-02 1.16E-01 367.79 0.86 -7.09E-01 3.01E+00 411.12 2.24 7.15E-01 1.53E+00 443.96 2.83 -5.13E-03 9.79E-01 488.68 0.42 -3.33E+00 6.12E+00 563.99 0.49 -5.40E-01 5.96E+00 586.26 0.46 -7.87E+00 1.02E+01 678.62 0.47 -5.03E-01 5.39E+00 688.67 0.86 -1.54E-01 3.47E+00 719.35 0.28 5.13E+00 1.10E+01 778.90 12.96 -2.98E-02 2.54E-01 810.45 0.32 2.07E+00 1.09E+01 867.37 4.26 1.10E-01 8.61E-01 919.33 0.43 7.27E-01 8.22E+00 964.08 14.65 -9.45E-02 3.05E-01 1085.87 10.24 -1.98E-01 3.16E-01 1089.74 1.73 6.05E-01 2.16E+00 1112.07 13.69 -4.76E-02 2.83E-01 1212.95 1.43 1.94E+00 3.30E+00 1249.94 0.19 -7.14E+00 1.81E+01 1299.14 1.63 -5.81E-01 1.62E+00 1408.01 21.07 1.03E-01 1.94E-01 1457.64 0.50 -7.71E+00 2.59E+01 1528.10 0.28 3.38E+00 1.12E+01 Eu-154 123.07 40.40 -1.45E-03 6.95E-02 6.95E-02 247.93 6.89 -9.90E-02 4.03E-01 591.76 4.95 2.38E-02 7.20E-01 692.42 1.78 -2.05E-01 1.75E+00 723.30 20.06 7.32E-02 1.82E-01 756.80 4.52 2.26E-01 7.29E-01 873.18 12.08 -8.34E-02 2.41E-01
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| [301]
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| 7/9/2019 10:42:53AM Page 7 of 7 Analysis Report for 09-Jul-19-10030 L1-10221C-FIGS-106SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.99E-01 6.95E-02 2.93E-01 1004.76 18.01 3.20E-02 1.93E-01 1274.43 34.80 1.45E-02 9.96E-02 1596.48 1.80 4.65E-01 1.45E+00 Eu-155 45.30 1.31 5.57E+00 1.47E-01 1.06E+01 60.01 1.22 8.65E+00 1.23E+01 86.55 30.70 3.98E-02 1.48E-01 105.31 21.10 -6.52E-02 1.47E-01 Ra-226 186.21 3.64 3.37E-01 8.89E-01 8.89E-01 Pa-231 27.36 10.30 6.17E-01 1.01E+00 1.01E+00 283.69 1.70 5.71E-01 1.75E+00 300.07 2.47 -1.49E+00 1.07E+00 302.65 2.20 8.15E-01 1.30E+00 330.06 1.40 -1.92E-01 2.12E+00 U-235 143.76 10.96 7.07E-02 5.70E-02 2.66E-01 163.33 5.08 1.26E-01 6.35E-01 185.71 57.20 3.62E-02 5.70E-02 202.11 1.08 9.69E-03 2.87E+00 205.31 5.01 -2.76E-01 5.88E-01 Am-241 59.54 35.90 3.21E-01 4.36E-01 4.36E-01
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| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
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| > = MDA value not calculated
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| @ = Half-life too short to be able to perform the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| [302]
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| 7/9/2019 10:43:04AM Page 1 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10031 Sample Description : L1-10221C-FIGS-107SS Sample Type : Soil Unit :
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| Sample Point :
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| Sample Size : 1.657E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:55:00PM Acquisition Started : 7/9/2019 10:27:51AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.0 seconds Dead Time : 0.11 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
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| Sample Number : 77839 Fill Height : 1657.29 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:42:55AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
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| [303]
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| 7/9/2019 10:43:04AM Page 2 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.58 948 - 959 954.43 6.53E+01 13.62 4.77E+01 0.67 2 351.69 1400 - 1415 1406.48 5.77E+01 10.46 1.74E+01 1.18 3 582.78 2325 - 2337 2330.32 2.83E+01 7.35 9.75E+00 1.22 4 609.04 2429 - 2442 2435.34 4.25E+01 7.76 6.51E+00 1.20 5 910.76 3638 - 3647 3642.01 1.65E+01 5.99 8.46E+00 0.74 6 1460.04 5830 - 5849 5839.98 1.42E+02 12.94 7.41E+00 1.50 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
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| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.90 1460.82
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| * 10.66 3.45E+00 3.49E-01 Tl-208 0.97 583.19
| |
| * 85.00 4.63E-02 1.24E-02 Bi-211 0.94 351.07
| |
| * 13.02 4.34E-01 8.62E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.15E-01 2.58E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.34E-01 2.58E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 [304]
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| 7/9/2019 10:43:04AM Page 3 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
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| * 35.60 1.59E-01 3.15E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.21E-01 4.41E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
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| [305]
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| 7/9/2019 10:43:04AM Page 4 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| K-40 0.906 3.45E+00 3.49E-01 Tl-208 0.974 4.63E-02 1.24E-02
| |
| ? Bi-211 0.941 4.34E-01 8.62E-02 Pb-212 1.000 1.15E-01 2.58E-02 Bi-214 0.995 1.34E-01 2.58E-02
| |
| ? Pb-214 0.995 1.59E-01 3.15E-02 Ac-228 0.990 1.21E-01 4.41E-02
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| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
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| [306]
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| 7/9/2019 10:43:04AM Page 5 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:42:55AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
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| (keV)
| |
| An Pk 511.00 100.00 6.37E-02 5.27E-02 5.27E-02 BE-7 477.60 10.44 8.24E-02 4.00E-01 4.00E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.45E+00 4.90E-01 4.90E-01 Mn-54 834.85 99.98 0.00E+00 4.32E-02 4.32E-02 Co-60 1173.23 99.85 8.24E-03 3.77E-02 5.66E-02 1332.49 99.98 3.20E-03 3.77E-02 Nb-94 702.65 99.81 -7.92E-04 3.85E-02 3.85E-02 871.09 99.89 6.85E-03 3.92E-02 Ag-108m 79.13 6.60 7.43E-01 3.77E-02 1.61E+00 433.94 90.50 -3.97E-03 3.77E-02 614.28 89.80 -1.03E-02 4.61E-02 722.94 90.80 3.62E-02 4.68E-02 Sb-125 176.31 6.84 2.48E-02 1.08E-01 4.79E-01 380.45 1.52 -9.56E-01 2.25E+00 427.87 29.60 -4.21E-02 1.08E-01 463.36 10.49 1.29E-02 3.41E-01 600.60 17.65 -1.13E-01 2.16E-01 606.71 4.98 1.27E+00 1.18E+00 635.95 11.22 2.09E-01 4.01E-01 [307]
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| 7/9/2019 10:43:04AM Page 6 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.35E+00 1.08E-01 2.50E+00 Ba-133 79.61 2.65 7.58E-01 6.34E-02 3.83E+00 81.00 32.90 -1.11E-01 2.72E-01 276.40 7.16 6.58E-02 4.60E-01 302.85 18.34 1.00E-01 1.96E-01 356.01 62.05 -5.63E-03 6.34E-02 383.85 8.94 5.84E-02 3.79E-01 Cs-134 475.36 1.48 1.36E+00 5.40E-02 2.82E+00 563.25 8.34 7.19E-02 3.79E-01 569.33 15.37 5.94E-02 2.22E-01 604.72 97.62 -1.55E-02 5.77E-02 795.86 85.46 5.03E-02 5.40E-02 801.95 8.69 2.36E-01 4.51E-01 1038.61 0.99 0.00E+00 4.83E+00 1167.97 1.79 -8.98E-01 3.15E+00 1365.19 3.02 -1.80E+00 9.16E-01 Cs-137 661.66 85.10 1.39E-02 5.04E-02 5.04E-02 Eu-152 121.78 28.67 -4.63E-02 1.30E-01 1.44E-01 244.70 7.61 -2.14E-01 4.97E-01 295.94 0.45 7.37E-01 8.45E+00 344.28 26.60 1.36E-02 1.30E-01 367.79 0.86 1.81E+00 4.03E+00 411.12 2.24 7.47E-01 1.63E+00 443.96 2.83 6.11E-01 1.29E+00 488.68 0.42 -3.65E+00 8.03E+00 563.99 0.49 -7.01E-01 6.60E+00 586.26 0.46 -1.71E+00 1.12E+01 678.62 0.47 -2.08E+00 8.31E+00 688.67 0.86 2.41E+00 4.70E+00 719.35 0.28 -1.23E+01 1.16E+01 778.90 12.96 -5.13E-01 2.96E-01 810.45 0.32 1.08E+01 1.32E+01 867.37 4.26 7.47E-02 8.62E-01 919.33 0.43 -5.76E+00 7.29E+00 964.08 14.65 8.69E-02 3.84E-01 1085.87 10.24 -2.90E-02 4.44E-01 1089.74 1.73 2.09E+00 2.78E+00 1112.07 13.69 8.55E-02 3.56E-01 1212.95 1.43 2.21E-01 3.97E+00 1249.94 0.19 6.15E+00 1.67E+01 1299.14 1.63 -3.41E+00 2.41E+00 1408.01 21.07 4.07E-02 2.07E-01 1457.64 0.50 8.00E+01 3.23E+01 1528.10 0.28 -2.43E+00 1.30E+01 Eu-154 123.07 40.40 -6.72E-03 9.93E-02 9.93E-02 247.93 6.89 1.19E-01 4.78E-01 591.76 4.95 -7.67E-02 8.04E-01 692.42 1.78 -1.32E-01 2.10E+00 723.30 20.06 2.01E-01 2.16E-01 756.80 4.52 6.27E-02 8.33E-01 873.18 12.08 1.56E-02 3.43E-01
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| [308]
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| 7/9/2019 10:43:04AM Page 7 of 7 Analysis Report for 09-Jul-19-10031 L1-10221C-FIGS-107SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -6.21E-02 9.93E-02 3.14E-01 1004.76 18.01 6.44E-02 2.53E-01 1274.43 34.80 -1.54E-01 1.57E-01 1596.48 1.80 -2.37E+00 2.11E+00 Eu-155 45.30 1.31 1.08E+01 2.35E-01 2.70E+01 60.01 1.22 -4.57E+00 2.64E+01 86.55 30.70 2.27E-01 2.67E-01 105.31 21.10 1.24E-02 2.35E-01 Ra-226 186.21 3.64 1.90E-01 9.28E-01 9.28E-01 Pa-231 27.36 10.30 1.50E+00 1.41E+00 2.92E+00 283.69 1.70 -6.87E-01 1.82E+00 300.07 2.47 -2.90E-01 1.41E+00 302.65 2.20 1.09E+00 1.62E+00 330.06 1.40 8.05E-01 2.67E+00 U-235 143.76 10.96 9.47E-02 5.78E-02 3.68E-01 163.33 5.08 3.60E-01 7.35E-01 185.71 57.20 -1.62E-03 5.78E-02 202.11 1.08 -1.02E+00 3.02E+00 205.31 5.01 -1.61E-01 6.57E-01 Am-241 59.54 35.90 -6.30E-01 8.83E-01 8.83E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [309]
| |
| | |
| 7/9/2019 10:43:17AM Page 1 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10032 Sample Description : L1-10221C-FIGS-108SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.641E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:57:00PM Acquisition Started : 7/9/2019 10:28:01AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
| |
| Sample Number : 77840 Fill Height : 1640.53 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:43:10AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [310]
| |
| | |
| 7/9/2019 10:43:17AM Page 2 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.81 946 - 961 954.80 6.68E+01 13.86 4.12E+01 0.42 2 609.57 2431 - 2441 2436.31 3.16E+01 6.84 6.36E+00 0.52 3 911.18 3635 - 3648 3642.19 2.92E+01 5.85 1.77E+00 0.68 4 1460.41 5830 - 5849 5839.57 1.30E+02 12.80 9.71E+00 1.11 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82
| |
| * 10.66 2.87E+00 3.08E-01 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.05E-01 2.33E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 9.03E-02 2.03E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 [311]
| |
| | |
| 7/9/2019 10:43:17AM Page 3 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.93E-01 3.95E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.973 2.87E+00 3.08E-01 Pb-212 0.996 1.05E-01 2.33E-02 Bi-214 0.996 9.03E-02 2.03E-02 Ac-228 1.000 1.93E-01 3.95E-02
| |
| [312]
| |
| | |
| 7/9/2019 10:43:17AM Page 4 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [313]
| |
| | |
| 7/9/2019 10:43:17AM Page 5 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:43:10AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.18E-02 4.69E-02 4.69E-02 BE-7 477.60 10.44 1.90E-01 3.69E-01 3.69E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.87E+00 4.96E-01 4.96E-01 Mn-54 834.85 99.98 2.18E-02 3.73E-02 3.73E-02 Co-60 1173.23 99.85 -3.02E-03 4.11E-02 4.45E-02 1332.49 99.98 2.41E-02 4.11E-02 Nb-94 702.65 99.81 1.64E-02 3.16E-02 3.16E-02 871.09 99.89 1.80E-02 4.02E-02 Ag-108m 79.13 6.60 1.36E-01 3.05E-02 9.78E-01 433.94 90.50 -2.87E-02 3.05E-02 614.28 89.80 -6.67E-02 4.48E-02 722.94 90.80 9.10E-03 3.90E-02 Sb-125 176.31 6.84 -2.14E-02 1.02E-01 3.41E-01 380.45 1.52 -5.70E-01 1.60E+00 427.87 29.60 4.40E-02 1.02E-01 463.36 10.49 -9.38E-02 2.80E-01 600.60 17.65 -1.32E-01 1.52E-01 606.71 4.98 7.16E-01 9.65E-01 635.95 11.22 1.72E-01 3.42E-01 [314]
| |
| | |
| 7/9/2019 10:43:17AM Page 6 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -2.20E-01 1.02E-01 1.97E+00 Ba-133 79.61 2.65 2.55E-01 4.83E-02 2.35E+00 81.00 32.90 -1.24E-01 1.60E-01 276.40 7.16 1.99E-01 4.15E-01 302.85 18.34 7.60E-02 1.42E-01 356.01 62.05 -5.29E-02 4.83E-02 383.85 8.94 5.09E-02 2.93E-01 Cs-134 475.36 1.48 1.73E+00 4.12E-02 2.62E+00 563.25 8.34 -1.01E+00 3.59E-01 569.33 15.37 -1.40E-01 1.73E-01 604.72 97.62 -5.37E-02 4.19E-02 795.86 85.46 6.42E-04 4.12E-02 801.95 8.69 1.21E-01 4.07E-01 1038.61 0.99 1.83E+00 4.67E+00 1167.97 1.79 -3.22E-01 2.34E+00 1365.19 3.02 -6.76E-01 1.33E+00 Cs-137 661.66 85.10 1.17E-02 4.01E-02 4.01E-02 Eu-152 121.78 28.67 4.69E-02 9.16E-02 9.16E-02 244.70 7.61 -3.99E-02 3.85E-01 295.94 0.45 6.62E+00 7.87E+00 344.28 26.60 -4.16E-02 9.97E-02 367.79 0.86 -4.41E-01 3.13E+00 411.12 2.24 2.64E-01 1.23E+00 443.96 2.83 -7.53E-02 1.14E+00 488.68 0.42 1.54E-01 6.73E+00 563.99 0.49 -7.74E+00 6.10E+00 586.26 0.46 1.11E+01 9.63E+00 678.62 0.47 -1.92E+00 5.97E+00 688.67 0.86 -1.63E+00 3.20E+00 719.35 0.28 5.07E+00 1.27E+01 778.90 12.96 -1.88E-01 2.22E-01 810.45 0.32 -2.13E+00 8.84E+00 867.37 4.26 -2.99E-01 8.97E-01 919.33 0.43 2.39E+00 8.08E+00 964.08 14.65 1.34E-01 3.00E-01 1085.87 10.24 2.80E-01 4.01E-01 1089.74 1.73 1.34E-01 2.16E+00 1112.07 13.69 2.13E-02 2.86E-01 1212.95 1.43 -2.97E-01 4.08E+00 1249.94 0.19 8.60E+00 2.70E+01 1299.14 1.63 -1.06E+00 2.06E+00 1408.01 21.07 1.02E-02 1.78E-01 1457.64 0.50 6.21E+01 2.83E+01 1528.10 0.28 -4.52E+00 1.07E+01 Eu-154 123.07 40.40 -2.08E-02 6.47E-02 6.47E-02 247.93 6.89 4.53E-02 3.88E-01 591.76 4.95 1.22E-01 5.35E-01 692.42 1.78 1.19E+00 1.71E+00 723.30 20.06 3.45E-02 1.73E-01 756.80 4.52 -2.18E-01 7.13E-01 873.18 12.08 9.71E-02 3.02E-01
| |
| [315]
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| 7/9/2019 10:43:17AM Page 7 of 7 Analysis Report for 09-Jul-19-10032 L1-10221C-FIGS-108SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 8.20E-02 6.47E-02 3.81E-01 1004.76 18.01 1.68E-02 1.97E-01 1274.43 34.80 2.28E-02 1.23E-01 1596.48 1.80 -1.08E+00 2.05E+00 Eu-155 45.30 1.31 -1.15E+00 1.44E-01 8.43E+00 60.01 1.22 -7.39E+00 9.16E+00 86.55 30.70 2.88E-02 1.44E-01 105.31 21.10 3.03E-02 1.65E-01 Ra-226 186.21 3.64 1.03E-01 7.47E-01 7.47E-01 Pa-231 27.36 10.30 8.71E-01 1.11E+00 1.11E+00 283.69 1.70 -6.96E-01 1.46E+00 300.07 2.47 -8.40E-01 1.16E+00 302.65 2.20 8.05E-01 1.19E+00 330.06 1.40 -5.33E-01 1.87E+00 U-235 143.76 10.96 -5.16E-02 4.89E-02 2.09E-01 163.33 5.08 1.77E-01 5.44E-01 185.71 57.20 3.77E-02 4.89E-02 202.11 1.08 -9.17E-01 2.16E+00 205.31 5.01 -1.63E-01 4.89E-01 Am-241 59.54 35.90 -2.03E-01 3.20E-01 3.20E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [316]
| |
| | |
| 7/9/2019 10:43:24AM Page 1 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS GAMMA SPECTRUM ANALYSIS Sample Identification : 09-Jul-19-10033 Sample Description : L1-10221C-FIGS-109SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.658E+03 grams Facility : Default Sample Taken On : 7/8/2019 12:59:00PM Acquisition Started : 7/9/2019 10:28:11AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 7/9/2019 Efficiency Calibration Description :
| |
| Sample Number : 77841 Fill Height : 1657.61 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/9/2019 10:43:16AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [317]
| |
| | |
| 7/9/2019 10:43:24AM Page 2 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 185.77 740 - 751 743.79 3.38E+01 10.36 2.92E+01 0.50 2 238.54 948 - 961 954.65 9.44E+01 12.74 2.46E+01 1.03 3 351.95 1401 - 1415 1407.78 5.00E+01 9.68 1.50E+01 1.06 4 609.30 2431 - 2442 2436.47 3.49E+01 7.10 6.06E+00 0.67 5 1460.98 5833 - 5854 5844.30 1.30E+02 11.83 2.64E+00 0.93 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 2.67E+00 2.69E-01 Bi-211 0.88 351.07
| |
| * 13.02 3.28E-01 6.87E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.46E-01 2.30E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 9.45E-02 2.00E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 [318]
| |
| | |
| 7/9/2019 10:43:24AM Page 3 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.20E-01 2.51E-02 785.96 1.06 Ra-226 0.96 186.21
| |
| * 3.64 5.61E-01 1.78E-01 U-235 1.00 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 3.57E-02 1.13E-02 202.11 1.08 205.31 5.01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.996 2.67E+00 2.69E-01
| |
| ? Bi-211 0.884 3.28E-01 6.87E-02 Pb-212 0.999 1.46E-01 2.30E-02 Bi-214 1.000 9.45E-02 2.00E-02
| |
| ? Pb-214 1.000 1.20E-01 2.51E-02
| |
| ? Ra-226 0.969 5.61E-01 1.78E-01 [319]
| |
| | |
| 7/9/2019 10:43:24AM Page 4 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| ? U-235 1.000 3.57E-02 1.13E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [320]
| |
| | |
| 7/9/2019 10:43:24AM Page 5 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS UNIDENTIFIED PEAKS Peak Locate Performed on : 7/9/2019 10:43:16AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 3.67E-02 4.74E-02 4.74E-02 BE-7 477.60 10.44 4.11E-01 3.94E-01 3.94E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.67E+00 2.75E-01 2.75E-01 Mn-54 834.85 99.98 3.44E-04 2.84E-02 2.84E-02 Co-60 1173.23 99.85 -4.12E-02 2.55E-02 3.10E-02 1332.49 99.98 8.17E-03 2.55E-02 Nb-94 702.65 99.81 -6.35E-03 2.80E-02 3.57E-02 871.09 99.89 -1.89E-02 2.80E-02 Ag-108m 79.13 6.60 -2.07E-01 3.35E-02 1.17E+00 433.94 90.50 -2.48E-04 3.35E-02 614.28 89.80 -2.55E-02 5.60E-02 722.94 90.80 -2.05E-03 3.43E-02 Sb-125 176.31 6.84 -5.42E-02 9.31E-02 4.46E-01 380.45 1.52 7.97E-01 1.65E+00 427.87 29.60 -6.95E-02 9.31E-02 463.36 10.49 7.76E-02 2.94E-01 600.60 17.65 -1.14E-02 1.82E-01 606.71 4.98 1.15E+00 1.00E+00 635.95 11.22 2.32E-01 3.14E-01 [321]
| |
| | |
| 7/9/2019 10:43:24AM Page 6 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.73E-01 9.31E-02 1.70E+00 Ba-133 79.61 2.65 -7.20E-01 5.89E-02 2.86E+00 81.00 32.90 -2.29E-01 2.04E-01 276.40 7.16 -1.12E-01 3.96E-01 302.85 18.34 4.31E-02 1.73E-01 356.01 62.05 -4.86E-03 5.89E-02 383.85 8.94 -1.01E-01 2.82E-01 Cs-134 475.36 1.48 -1.51E-01 3.68E-02 2.58E+00 563.25 8.34 1.93E-01 4.03E-01 569.33 15.37 -1.27E-01 2.27E-01 604.72 97.62 -1.43E-02 4.66E-02 795.86 85.46 -2.29E-02 3.68E-02 801.95 8.69 1.69E-01 3.74E-01 1038.61 0.99 2.29E+00 3.55E+00 1167.97 1.79 9.74E-01 2.12E+00 1365.19 3.02 6.21E-01 1.19E+00 Cs-137 661.66 85.10 5.13E-02 4.95E-02 4.95E-02 Eu-152 121.78 28.67 -4.45E-02 1.04E-01 1.08E-01 244.70 7.61 2.07E-01 4.00E-01 295.94 0.45 1.46E+00 7.62E+00 344.28 26.60 -5.14E-02 1.04E-01 367.79 0.86 1.47E+00 3.31E+00 411.12 2.24 9.16E-01 1.49E+00 443.96 2.83 -1.16E+00 8.96E-01 488.68 0.42 -8.26E-01 6.56E+00 563.99 0.49 -4.17E-01 6.84E+00 586.26 0.46 6.65E+00 9.24E+00 678.62 0.47 2.54E+00 6.65E+00 688.67 0.86 3.41E+00 3.94E+00 719.35 0.28 1.84E+00 1.05E+01 778.90 12.96 -1.61E-01 1.92E-01 810.45 0.32 8.39E-02 8.67E+00 867.37 4.26 -8.82E-02 7.56E-01 919.33 0.43 -1.09E+01 8.07E+00 964.08 14.65 2.44E-01 3.25E-01 1085.87 10.24 9.74E-02 3.29E-01 1089.74 1.73 -2.46E+00 1.87E+00 1112.07 13.69 -2.18E-01 2.68E-01 1212.95 1.43 2.38E+00 3.55E+00 1249.94 0.19 -7.60E+00 2.22E+01 1299.14 1.63 -3.09E-02 2.57E+00 1408.01 21.07 -7.32E-02 1.57E-01 1457.64 0.50 5.77E+01 2.56E+01 1528.10 0.28 2.40E+00 8.96E+00 Eu-154 123.07 40.40 -1.06E-01 7.28E-02 7.28E-02 247.93 6.89 -1.60E-01 3.58E-01 591.76 4.95 3.40E-01 7.11E-01 692.42 1.78 1.72E+00 2.16E+00 723.30 20.06 1.69E-02 1.55E-01 756.80 4.52 2.19E-01 6.11E-01 873.18 12.08 -3.28E-01 2.22E-01
| |
| [322]
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| 7/9/2019 10:43:24AM Page 7 of 7 Analysis Report for 09-Jul-19-10033 L1-10221C-FIGS-109SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.29E-01 7.28E-02 3.57E-01 1004.76 18.01 -1.21E-01 1.71E-01 1274.43 34.80 4.13E-02 1.42E-01 1596.48 1.80 -8.77E-01 1.90E+00 Eu-155 45.30 1.31 9.14E-01 1.66E-01 1.56E+01 60.01 1.22 1.95E+00 1.77E+01 86.55 30.70 -4.13E-02 1.79E-01 105.31 21.10 -2.92E-02 1.66E-01
| |
| + Ra-226 186.21
| |
| * 3.64 5.61E-01 5.30E-01 5.30E-01 Pa-231 27.36 10.30 9.34E-01 1.30E+00 1.84E+00 283.69 1.70 -5.07E-01 1.67E+00 300.07 2.47 -1.79E+00 1.30E+00 302.65 2.20 -1.54E-01 1.43E+00 330.06 1.40 4.11E-01 1.99E+00
| |
| + U-235 143.76 10.96 1.01E-01 3.37E-02 2.73E-01 163.33 5.08 -2.52E-01 5.21E-01 185.71
| |
| * 57.20 3.57E-02 3.37E-02 202.11 1.08 -2.09E-01 2.51E+00 205.31 5.01 -7.65E-02 5.20E-01 Am-241 59.54 35.90 -2.34E-01 6.12E-01 6.12E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [323]
| |
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| 8/1/2019 7:44:46AM Page 1 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS GAMMA SPECTRUM ANALYSIS Sample Identification : 01-Aug-19-10008 Sample Description : L1-10221C-FIGS-110SS Sample Type : Soil Unit :
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| Sample Point :
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| Sample Size : 1.535E+03 grams Facility : Default Sample Taken On : 7/31/2019 9:30:00AM Acquisition Started : 8/1/2019 7:29:33AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 8/1/2019 Efficiency Calibration Description :
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| Sample Number : 78402 Fill Height : 1534.89 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 8/1/2019 7:44:36AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
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| [324]
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| 8/1/2019 7:44:46AM Page 2 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 92.68 367 - 379 371.95 3.93E+01 11.22 3.27E+01 0.30 2 185.95 741 - 749 744.53 2.30E+01 9.54 3.10E+01 0.76 3 238.64 949 - 961 955.03 7.26E+01 13.12 3.64E+01 0.92 4 351.90 1400 - 1413 1407.61 6.43E+01 10.37 1.57E+01 0.82 5 583.14 2325 - 2339 2331.89 3.88E+01 7.71 7.18E+00 0.72 6 609.30 2429 - 2444 2436.45 4.66E+01 8.91 1.04E+01 0.83 7 1460.76 5833 - 5854 5843.40 1.69E+02 14.36 1.03E+01 1.31 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
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| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
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| * 10.66 3.53E+00 3.37E-01 Tl-208 1.00 583.19
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| * 85.00 5.55E-02 1.15E-02 Bi-211 0.89 351.07
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| * 13.02 4.27E-01 7.71E-02 Pb-212 1.00 115.18 0.60 238.63
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| * 43.60 1.14E-01 2.25E-02 300.09 3.30 Bi-214 1.00 609.32
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| * 45.49 1.28E-01 2.57E-02 768.36 4.89 806.18 1.26 934.06 3.11 [325]
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| 8/1/2019 7:44:46AM Page 3 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
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| * 35.60 1.56E-01 2.82E-02 785.96 1.06 Ra-226 0.98 186.21
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| * 3.64 3.85E-01 1.63E-01 Ac228-XR 0.95 89.96 1.90 93.35
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| * 3.10 1.24E+00 4.08E-01 Th-234 0.99 92.38 2.13 92.80
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| * 2.10 1.88E+00 5.96E-01 112.81 0.21 U-235 0.99 143.76 10.96 163.33 5.08 185.71
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| * 57.20 2.45E-02 1.04E-02 202.11 1.08 205.31 5.01 U235-XR 0.96 89.96 3.47 93.35
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| * 5.60 6.86E-01 2.08E-01 105.60 1.32
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
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| [326]
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| 8/1/2019 7:44:46AM Page 4 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| K-40 0.999 3.53E+00 3.37E-01 Tl-208 1.000 5.55E-02 1.15E-02
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| ? Bi-211 0.895 4.27E-01 7.71E-02 Pb-212 1.000 1.14E-01 2.25E-02 Bi-214 1.000 1.28E-01 2.57E-02
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| ? Pb-214 1.000 1.56E-01 2.82E-02
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| ? Ra-226 0.989 3.85E-01 1.63E-01
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| ? Ac228-XR 0.957 1.24E+00 4.08E-01
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| ? Th-234 0.999 1.88E+00 5.96E-01
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| ? U-235 0.994 2.45E-02 1.04E-02
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| ? U235-XR 0.962 6.86E-01 2.08E-01
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| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
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| [327]
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| 8/1/2019 7:44:46AM Page 5 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS UNIDENTIFIED PEAKS Peak Locate Performed on : 8/1/2019 7:44:36AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
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| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 3.71E-02 4.61E-02 4.61E-02 BE-7 477.60 10.44 -1.01E-01 2.56E-01 2.56E-01
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| + K-40 1460.82
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| * 10.66 3.53E+00 4.94E-01 4.94E-01 Mn-54 834.85 99.98 3.67E-02 4.42E-02 4.42E-02 Co-60 1173.23 99.85 1.75E-02 3.05E-02 4.97E-02 1332.49 99.98 -3.07E-02 3.05E-02 Nb-94 702.65 99.81 -1.32E-02 3.20E-02 3.20E-02 871.09 99.89 -1.08E-02 3.39E-02 Ag-108m 79.13 6.60 7.83E-01 3.62E-02 1.30E+00 433.94 90.50 1.08E-02 3.62E-02 614.28 89.80 1.64E-02 6.02E-02 722.94 90.80 1.93E-03 5.06E-02 Sb-125 176.31 6.84 1.92E-01 1.15E-01 4.34E-01 380.45 1.52 1.28E+00 1.88E+00 427.87 29.60 -1.70E-02 1.15E-01 463.36 10.49 1.88E-01 3.03E-01 600.60 17.65 -1.21E-01 2.08E-01 606.71 4.98 9.04E-01 1.12E+00 635.95 11.22 -3.21E-01 2.60E-01 [328]
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| 8/1/2019 7:44:46AM Page 6 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -6.62E-01 1.15E-01 1.77E+00 Ba-133 79.61 2.65 9.33E-01 6.77E-02 3.02E+00 81.00 32.90 -2.77E-01 1.96E-01 276.40 7.16 -1.63E-02 4.69E-01 302.85 18.34 4.04E-02 1.61E-01 356.01 62.05 -2.47E-02 6.77E-02 383.85 8.94 2.56E-01 3.38E-01 Cs-134 475.36 1.48 -9.61E-02 4.24E-02 1.75E+00 563.25 8.34 9.90E-02 4.34E-01 569.33 15.37 6.72E-02 2.16E-01 604.72 97.62 -6.03E-02 5.45E-02 795.86 85.46 3.92E-03 4.24E-02 801.95 8.69 -2.63E-01 3.70E-01 1038.61 0.99 5.51E-01 4.46E+00 1167.97 1.79 1.10E+00 2.82E+00 1365.19 3.02 -1.58E-01 1.37E+00 Cs-137 661.66 85.10 2.51E-02 4.72E-02 4.72E-02 Eu-152 121.78 28.67 -1.10E-02 1.14E-01 1.18E-01 244.70 7.61 4.17E-02 4.29E-01 295.94 0.45 1.74E+00 7.96E+00 344.28 26.60 5.39E-03 1.14E-01 367.79 0.86 -1.27E+00 3.02E+00 411.12 2.24 5.07E-01 1.26E+00 443.96 2.83 -5.96E-01 9.09E-01 488.68 0.42 -2.16E+00 7.15E+00 563.99 0.49 4.33E+00 7.47E+00 586.26 0.46 1.15E+01 1.01E+01 678.62 0.47 -4.80E+00 7.22E+00 688.67 0.86 2.56E+00 3.84E+00 719.35 0.28 7.87E+00 1.39E+01 778.90 12.96 1.14E-01 2.36E-01 810.45 0.32 2.11E+00 1.04E+01 867.37 4.26 3.34E-01 9.38E-01 919.33 0.43 2.81E+00 7.47E+00 964.08 14.65 4.04E-02 3.31E-01 1085.87 10.24 9.99E-02 4.24E-01 1089.74 1.73 3.90E-02 2.51E+00 1112.07 13.69 1.05E-01 3.36E-01 1212.95 1.43 -2.21E+00 2.58E+00 1249.94 0.19 2.05E+01 2.84E+01 1299.14 1.63 -1.48E+00 2.18E+00 1408.01 21.07 -1.40E-01 1.78E-01 1457.64 0.50 8.32E+01 3.04E+01 1528.10 0.28 -7.84E-01 1.20E+01 Eu-154 123.07 40.40 -1.48E-02 8.13E-02 8.13E-02 247.93 6.89 -6.54E-02 4.00E-01 591.76 4.95 2.51E-02 6.29E-01 692.42 1.78 3.44E-01 1.64E+00 723.30 20.06 1.78E-01 2.37E-01 756.80 4.52 2.35E-01 6.43E-01 873.18 12.08 -6.72E-02 2.81E-01
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| [329]
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| 8/1/2019 7:44:46AM Page 7 of 7 Analysis Report for 01-Aug-19-10008 L1-10221C-FIGS-110SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -3.79E-02 8.13E-02 3.64E-01 1004.76 18.01 5.96E-03 2.19E-01 1274.43 34.80 -7.27E-02 1.25E-01 1596.48 1.80 -8.29E-01 2.29E+00 Eu-155 45.30 1.31 -3.00E-01 1.76E-01 1.55E+01 60.01 1.22 -8.26E+00 1.66E+01 86.55 30.70 8.83E-02 1.76E-01 105.31 21.10 4.90E-02 1.83E-01
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| + Ra-226 186.21
| |
| * 3.64 3.85E-01 5.16E-01 5.16E-01 Pa-231 27.36 10.30 1.73E+00 1.30E+00 1.88E+00 283.69 1.70 -3.12E-01 1.85E+00 300.07 2.47 -2.42E+00 1.30E+00 302.65 2.20 6.66E-01 1.36E+00 330.06 1.40 8.03E-01 2.00E+00
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| + U-235 143.76 10.96 -1.58E-01 3.29E-02 2.59E-01 163.33 5.08 5.59E-02 5.72E-01 185.71
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| * 57.20 2.45E-02 3.29E-02 202.11 1.08 1.85E+00 3.04E+00 205.31 5.01 -3.68E-01 6.44E-01 Am-241 59.54 35.90 -4.39E-02 6.05E-01 6.05E-01
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| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| [330]
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| 8/1/2019 8:46:11AM Page 1 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS GAMMA SPECTRUM ANALYSIS Sample Identification : 01-Aug-19-10009 Sample Description : L1-10221C-QIGS-110SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.529E+03 grams Facility : Default Sample Taken On : 7/31/2019 9:30:00AM Acquisition Started : 8/1/2019 8:30:59AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
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| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 8/1/2019 Efficiency Calibration Description :
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| Sample Number : 78403 Fill Height : 1528.92 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 8/1/2019 8:46:02AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
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| [331]
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| 8/1/2019 8:46:11AM Page 2 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 186.21 740 - 750 745.55 3.16E+01 10.44 3.24E+01 0.77 2 238.63 949 - 960 954.99 7.05E+01 13.13 4.05E+01 1.07 3 295.28 1173 - 1185 1181.35 4.10E+01 9.76 2.00E+01 1.14 4 338.38 1348 - 1359 1353.58 3.84E+01 7.74 8.62E+00 0.91 5 351.70 1401 - 1413 1406.81 6.15E+01 10.36 1.75E+01 0.65 6 511.13 2040 - 2051 2044.00 2.86E+01 8.40 1.64E+01 0.65 7 583.24 2326 - 2338 2332.30 4.20E+01 7.44 4.97E+00 0.98 8 1460.55 5834 - 5852 5842.57 1.40E+02 13.30 1.13E+01 2.00 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
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| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 0.99 511.00
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| * 100.00 3.23E-02 9.75E-03 K-40 0.98 1460.82
| |
| * 10.66 2.93E+00 3.06E-01 Tl-208 0.99 583.19
| |
| * 85.00 6.01E-02 1.12E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.10E-01 2.24E-02 300.09 3.30 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 1.71E-01 4.28E-02 351.93
| |
| * 35.60 1.50E-01 2.79E-02[332]
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| 8/1/2019 8:46:11AM Page 3 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-214 0.99 785.96 1.06 Ra-226 1.00 186.21
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| * 3.64 5.30E-01 1.80E-01 Ac-228 0.57 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 2.87E-01 6.24E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20 25.80 964.77 4.99 968.97 15.80 1588.20 3.22 U-235 0.97 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 3.37E-02 1.15E-02 202.11 1.08 205.31 5.01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| An Pk 0.997 3.23E-02 9.75E-03 K-40 0.988 2.93E+00 3.06E-01 Tl-208 0.999 6.01E-02 1.12E-02 X Bi-211 0.938 Pb-212 1.000 1.10E-01 2.24E-02 Pb-214 0.995 1.56E-01 2.34E-02
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| ? Ra-226 1.000 5.30E-01 1.80E-01 Ac-228 0.571 2.87E-01 6.24E-02 [333]
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| 8/1/2019 8:46:11AM Page 4 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| ? U-235 0.972 3.37E-02 1.15E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [334]
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| 8/1/2019 8:46:11AM Page 5 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS UNIDENTIFIED PEAKS Peak Locate Performed on : 8/1/2019 8:46:02AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 3.23E-02 2.81E-02 2.81E-02 BE-7 477.60 10.44 3.62E-01 3.70E-01 3.70E-01
| |
| + K-40 1460.82
| |
| * 10.66 2.93E+00 4.93E-01 4.93E-01 Mn-54 834.85 99.98 -2.73E-02 4.06E-02 4.06E-02 Co-60 1173.23 99.85 2.09E-05 4.48E-02 4.98E-02 1332.49 99.98 2.05E-02 4.48E-02 Nb-94 702.65 99.81 6.88E-04 3.56E-02 3.56E-02 871.09 99.89 -1.95E-02 4.40E-02 Ag-108m 79.13 6.60 2.49E-01 3.22E-02 1.32E+00 433.94 90.50 -8.97E-03 3.22E-02 614.28 89.80 -1.50E-02 5.70E-02 722.94 90.80 -2.70E-03 4.63E-02 Sb-125 176.31 6.84 5.82E-03 1.07E-01 4.43E-01 380.45 1.52 -1.86E-02 2.07E+00 427.87 29.60 8.19E-03 1.07E-01 463.36 10.49 -1.33E-01 3.12E-01 600.60 17.65 1.35E-01 2.20E-01 606.71 4.98 1.38E+00 1.15E+00 635.95 11.22 -8.44E-02 2.85E-01 [335]
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| 8/1/2019 8:46:11AM Page 6 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 5.92E-01 1.07E-01 1.97E+00 Ba-133 79.61 2.65 1.10E+00 6.18E-02 3.19E+00 81.00 32.90 -1.74E-01 2.12E-01 276.40 7.16 3.59E-02 4.50E-01 302.85 18.34 9.82E-02 1.82E-01 356.01 62.05 -3.78E-02 6.18E-02 383.85 8.94 -1.61E-01 3.13E-01 Cs-134 475.36 1.48 -5.87E-02 4.85E-02 2.47E+00 563.25 8.34 -1.11E-01 3.70E-01 569.33 15.37 -6.86E-02 2.24E-01 604.72 97.62 6.66E-03 5.31E-02 795.86 85.46 3.01E-02 4.85E-02 801.95 8.69 -3.66E-01 3.81E-01 1038.61 0.99 2.69E-01 4.46E+00 1167.97 1.79 1.72E+00 2.71E+00 1365.19 3.02 5.63E-01 1.16E+00 Cs-137 661.66 85.10 5.65E-02 5.28E-02 5.28E-02 Eu-152 121.78 28.67 2.00E-02 1.10E-01 1.14E-01 244.70 7.61 3.85E-01 4.49E-01 295.94 0.45 7.34E+00 8.72E+00 344.28 26.60 -3.05E-02 1.10E-01 367.79 0.86 1.45E+00 3.32E+00 411.12 2.24 -1.86E-01 1.50E+00 443.96 2.83 1.37E-01 1.16E+00 488.68 0.42 2.08E+00 6.81E+00 563.99 0.49 -3.36E+00 6.15E+00 586.26 0.46 1.11E+01 1.09E+01 678.62 0.47 4.20E+00 7.78E+00 688.67 0.86 9.20E-01 4.09E+00 719.35 0.28 1.25E+00 1.34E+01 778.90 12.96 -1.82E-01 2.76E-01 810.45 0.32 4.03E+00 1.28E+01 867.37 4.26 -7.75E-01 1.13E+00 919.33 0.43 -1.58E+01 7.98E+00 964.08 14.65 2.05E-01 3.52E-01 1085.87 10.24 -1.91E-01 3.22E-01 1089.74 1.73 -8.30E-01 2.14E+00 1112.07 13.69 -2.34E-01 2.82E-01 1212.95 1.43 -5.49E+00 3.49E+00 1249.94 0.19 -4.26E+01 2.20E+01 1299.14 1.63 1.36E+00 2.93E+00 1408.01 21.07 -4.12E-03 1.40E-01 1457.64 0.50 7.18E+01 2.83E+01 1528.10 0.28 5.73E+00 1.27E+01 Eu-154 123.07 40.40 -2.36E-02 7.89E-02 7.89E-02 247.93 6.89 1.46E-01 4.18E-01 591.76 4.95 8.69E-02 6.55E-01 692.42 1.78 6.29E-01 2.09E+00 723.30 20.06 3.13E-02 2.13E-01 756.80 4.52 3.50E-01 7.23E-01 873.18 12.08 -1.09E-01 3.46E-01
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| [336]
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| 8/1/2019 8:46:11AM Page 7 of 7 Analysis Report for 01-Aug-19-10009 L1-10221C-QIGS-110SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.24E-02 7.89E-02 3.22E-01 1004.76 18.01 8.19E-02 2.13E-01 1274.43 34.80 7.63E-02 1.42E-01 1596.48 1.80 4.98E-02 1.94E+00 Eu-155 45.30 1.31 3.73E+00 1.79E-01 1.60E+01 60.01 1.22 -2.23E+01 1.60E+01 86.55 30.70 5.36E-02 1.86E-01 105.31 21.10 -1.28E-01 1.79E-01
| |
| + Ra-226 186.21
| |
| * 3.64 5.30E-01 5.49E-01 5.49E-01 Pa-231 27.36 10.30 6.74E-01 1.44E+00 1.88E+00 283.69 1.70 8.45E-01 1.87E+00 300.07 2.47 -1.95E+00 1.44E+00 302.65 2.20 1.01E+00 1.53E+00 330.06 1.40 3.44E-01 2.39E+00
| |
| + U-235 143.76 10.96 -4.62E-02 3.50E-02 3.10E-01 163.33 5.08 9.55E-02 6.39E-01 185.71
| |
| * 57.20 3.37E-02 3.50E-02 202.11 1.08 -2.32E-01 2.93E+00 205.31 5.01 -1.22E-01 6.36E-01 Am-241 59.54 35.90 -3.43E-01 5.90E-01 5.90E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [337]
| |
| | |
| 8/1/2019 9:07:17AM Page 1 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS GAMMA SPECTRUM ANALYSIS Sample Identification : 01-Aug-19-10010 Sample Description : L1-10221C-FIGS-111SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.728E+03 grams Facility : Default Sample Taken On : 7/31/2019 9:32:00AM Acquisition Started : 8/1/2019 8:51:59AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.02 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 8/1/2019 Efficiency Calibration Description :
| |
| Sample Number : 78407 Fill Height : 1728.28 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 8/1/2019 9:07:08AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [338]
| |
| | |
| 8/1/2019 9:07:17AM Page 2 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.73 950 - 961 955.39 7.68E+01 11.72 2.43E+01 0.40 2 351.62 1401 - 1414 1406.47 5.55E+01 10.31 1.85E+01 0.92 3 583.29 2325 - 2338 2332.48 3.60E+01 7.43 7.00E+00 0.54 4 609.11 2428 - 2443 2435.69 5.51E+01 9.21 9.95E+00 0.42 5 910.96 3636 - 3649 3642.88 2.73E+01 5.66 1.72E+00 0.32 6 1460.66 5832 - 5854 5843.01 1.61E+02 13.40 5.17E+00 2.13 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 3.26E+00 3.07E-01 Tl-208 0.99 583.19
| |
| * 85.00 5.03E-02 1.08E-02 Bi-211 0.95 351.07
| |
| * 13.02 3.61E-01 7.32E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.18E-01 2.04E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.48E-01 2.63E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 [339]
| |
| | |
| 8/1/2019 9:07:17AM Page 3 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.32E-01 2.67E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.68E-01 3.56E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [340]
| |
| | |
| 8/1/2019 9:07:17AM Page 4 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.996 3.26E+00 3.07E-01 Tl-208 0.998 5.03E-02 1.08E-02
| |
| ? Bi-211 0.953 3.61E-01 7.32E-02 Pb-212 0.999 1.18E-01 2.04E-02 Bi-214 0.997 1.48E-01 2.63E-02
| |
| ? Pb-214 0.991 1.32E-01 2.67E-02 Ac-228 0.997 1.68E-01 3.56E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [341]
| |
| | |
| 8/1/2019 9:07:17AM Page 5 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS UNIDENTIFIED PEAKS Peak Locate Performed on : 8/1/2019 9:07:08AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 2.86E-02 4.13E-02 4.13E-02 BE-7 477.60 10.44 2.63E-01 3.78E-01 3.78E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.26E+00 3.57E-01 3.57E-01 Mn-54 834.85 99.98 2.26E-02 3.73E-02 3.73E-02 Co-60 1173.23 99.85 -1.86E-02 4.21E-02 4.92E-02 1332.49 99.98 -1.27E-02 4.21E-02 Nb-94 702.65 99.81 1.07E-02 3.73E-02 3.73E-02 871.09 99.89 5.39E-03 4.35E-02 Ag-108m 79.13 6.60 -3.67E-01 3.42E-02 1.23E+00 433.94 90.50 9.10E-03 3.42E-02 614.28 89.80 -1.93E-02 5.96E-02 722.94 90.80 -2.43E-02 3.49E-02 Sb-125 176.31 6.84 9.75E-02 1.05E-01 4.09E-01 380.45 1.52 -8.56E-01 1.98E+00 427.87 29.60 -7.04E-02 1.05E-01 463.36 10.49 1.21E-01 3.45E-01 600.60 17.65 3.13E-02 1.67E-01 606.71 4.98 9.33E-01 1.12E+00 635.95 11.22 6.62E-02 2.84E-01 [342]
| |
| | |
| 8/1/2019 9:07:17AM Page 6 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -5.48E-01 1.05E-01 1.77E+00 Ba-133 79.61 2.65 1.29E+00 5.81E-02 3.04E+00 81.00 32.90 -2.40E-01 2.08E-01 276.40 7.16 7.80E-02 4.22E-01 302.85 18.34 -7.20E-03 1.70E-01 356.01 62.05 -3.42E-02 5.81E-02 383.85 8.94 1.90E-02 3.39E-01 Cs-134 475.36 1.48 5.39E-01 3.85E-02 2.49E+00 563.25 8.34 -2.19E-01 3.67E-01 569.33 15.37 1.20E-01 2.08E-01 604.72 97.62 -7.61E-03 5.43E-02 795.86 85.46 -5.50E-04 3.85E-02 801.95 8.69 -1.39E-01 4.00E-01 1038.61 0.99 -3.64E+00 4.05E+00 1167.97 1.79 -4.72E-01 2.41E+00 1365.19 3.02 -1.20E-01 9.29E-01 Cs-137 661.66 85.10 3.55E-02 5.03E-02 5.03E-02 Eu-152 121.78 28.67 -6.89E-02 1.09E-01 1.09E-01 244.70 7.61 2.71E-01 4.28E-01 295.94 0.45 4.81E-02 8.42E+00 344.28 26.60 5.01E-02 1.13E-01 367.79 0.86 4.01E-01 3.45E+00 411.12 2.24 6.22E-01 1.46E+00 443.96 2.83 -2.15E-01 1.01E+00 488.68 0.42 8.18E-01 7.76E+00 563.99 0.49 3.63E+00 6.58E+00 586.26 0.46 9.42E+00 9.87E+00 678.62 0.47 4.21E+00 7.04E+00 688.67 0.86 7.31E-01 3.40E+00 719.35 0.28 -9.41E+00 1.13E+01 778.90 12.96 -1.24E-01 2.91E-01 810.45 0.32 -9.03E-02 1.09E+01 867.37 4.26 -1.03E-01 1.02E+00 919.33 0.43 -5.55E+00 8.00E+00 964.08 14.65 2.67E-01 3.37E-01 1085.87 10.24 2.58E-02 4.22E-01 1089.74 1.73 2.37E+00 2.66E+00 1112.07 13.69 2.21E-01 3.41E-01 1212.95 1.43 1.96E+00 3.71E+00 1249.94 0.19 -4.24E+00 2.27E+01 1299.14 1.63 -1.53E-01 2.47E+00 1408.01 21.07 1.20E-01 1.95E-01 1457.64 0.50 7.09E+01 2.84E+01 1528.10 0.28 -3.37E+00 7.67E+00 Eu-154 123.07 40.40 -2.48E-02 7.86E-02 7.86E-02 247.93 6.89 1.89E-01 4.37E-01 591.76 4.95 1.35E-01 5.49E-01 692.42 1.78 -4.63E-01 1.82E+00 723.30 20.06 -2.38E-02 1.62E-01 756.80 4.52 -1.19E-01 6.86E-01 873.18 12.08 -2.15E-01 3.55E-01
| |
| [343]
| |
| | |
| 8/1/2019 9:07:17AM Page 7 of 7 Analysis Report for 01-Aug-19-10010 L1-10221C-FIGS-111SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -4.26E-02 7.86E-02 3.54E-01 1004.76 18.01 1.88E-01 2.28E-01 1274.43 34.80 3.31E-02 1.18E-01 1596.48 1.80 7.72E-01 1.88E+00 Eu-155 45.30 1.31 -1.01E+01 1.71E-01 1.52E+01 60.01 1.22 8.54E-01 1.73E+01 86.55 30.70 1.10E-02 1.88E-01 105.31 21.10 9.72E-02 1.71E-01 Ra-226 186.21 3.64 7.78E-01 9.30E-01 9.30E-01 Pa-231 27.36 10.30 1.52E+00 1.40E+00 2.02E+00 283.69 1.70 -4.88E-01 1.68E+00 300.07 2.47 -1.61E+00 1.40E+00 302.65 2.20 4.05E-01 1.45E+00 330.06 1.40 1.34E+00 2.18E+00 U-235 143.76 10.96 2.98E-02 5.95E-02 2.84E-01 163.33 5.08 -2.64E-02 5.75E-01 185.71 57.20 7.09E-02 5.95E-02 202.11 1.08 6.01E-01 2.66E+00 205.31 5.01 -2.58E-01 5.67E-01 Am-241 59.54 35.90 1.41E-01 6.16E-01 6.16E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [344]
| |
| | |
| 8/1/2019 9:24:35AM Page 1 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS GAMMA SPECTRUM ANALYSIS Sample Identification : 01-Aug-19-10011 Sample Description : L1-10221C-FIGS-112SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.531E+03 grams Facility : Default Sample Taken On : 7/31/2019 9:34:00AM Acquisition Started : 8/1/2019 9:09:24AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 8/1/2019 Efficiency Calibration Description :
| |
| Sample Number : 78408 Fill Height : 1530.94 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 8/1/2019 9:24:26AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [345]
| |
| | |
| 8/1/2019 9:24:35AM Page 2 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 185.92 740 - 748 744.41 2.91E+01 9.18 2.59E+01 1.17 2 238.84 948 - 960 955.82 7.33E+01 13.74 4.37E+01 1.09 3 295.09 1173 - 1185 1180.58 2.79E+01 8.35 1.51E+01 0.58 4 351.87 1399 - 1416 1407.47 6.20E+01 9.56 9.00E+00 1.08 5 583.07 2327 - 2336 2331.58 2.27E+01 6.95 1.13E+01 0.30 6 609.11 2430 - 2444 2435.71 6.10E+01 8.90 5.97E+00 0.61 7 1460.66 5832 - 5853 5843.00 1.64E+02 13.22 2.80E+00 2.03 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 3.44E+00 3.14E-01 Tl-208 0.99 583.19
| |
| * 85.00 3.25E-02 1.01E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.15E-01 2.34E-02 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.68E-01 2.65E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 [346]
| |
| | |
| 8/1/2019 9:24:35AM Page 3 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22
| |
| * 18.42 1.16E-01 3.59E-02 351.93
| |
| * 35.60 1.51E-01 2.62E-02 785.96 1.06 Ra-226 0.98 186.21
| |
| * 3.64 4.88E-01 1.59E-01 U-235 0.99 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 3.11E-02 1.01E-02 202.11 1.08 205.31 5.01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.996 3.44E+00 3.14E-01 Tl-208 0.998 3.25E-02 1.01E-02 X Bi-211 0.903 Pb-212 0.994 1.15E-01 2.34E-02 [347]
| |
| | |
| 8/1/2019 9:24:35AM Page 4 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| Bi-214 0.997 1.68E-01 2.65E-02 Pb-214 0.999 1.39E-01 2.12E-02
| |
| ? Ra-226 0.987 4.88E-01 1.59E-01
| |
| ? U-235 0.995 3.11E-02 1.01E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [348]
| |
| | |
| 8/1/2019 9:24:35AM Page 5 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS UNIDENTIFIED PEAKS Peak Locate Performed on : 8/1/2019 9:24:26AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 5.21E-02 4.92E-02 4.92E-02 BE-7 477.60 10.44 1.40E-01 3.55E-01 3.55E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.44E+00 2.92E-01 2.92E-01 Mn-54 834.85 99.98 2.63E-02 3.83E-02 3.83E-02 Co-60 1173.23 99.85 1.37E-02 4.84E-02 4.97E-02 1332.49 99.98 3.13E-03 4.84E-02 Nb-94 702.65 99.81 -5.06E-02 3.95E-02 3.95E-02 871.09 99.89 5.38E-03 4.09E-02 Ag-108m 79.13 6.60 8.95E-02 3.31E-02 1.29E+00 433.94 90.50 1.26E-02 3.31E-02 614.28 89.80 -1.19E-02 6.38E-02 722.94 90.80 1.41E-02 5.51E-02 Sb-125 176.31 6.84 2.89E-02 9.46E-02 4.40E-01 380.45 1.52 1.41E+00 1.96E+00 427.87 29.60 -5.41E-02 9.46E-02 463.36 10.49 2.55E-01 3.15E-01 600.60 17.65 1.82E-04 2.02E-01 606.71 4.98 1.91E+00 1.17E+00 635.95 11.22 3.24E-02 2.85E-01 [349]
| |
| | |
| 8/1/2019 9:24:35AM Page 6 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 1.70E-01 9.46E-02 1.55E+00 Ba-133 79.61 2.65 1.71E+00 6.29E-02 3.20E+00 81.00 32.90 -2.43E-01 2.07E-01 276.40 7.16 1.17E-01 4.53E-01 302.85 18.34 5.65E-02 1.48E-01 356.01 62.05 2.01E-02 6.29E-02 383.85 8.94 8.31E-02 3.00E-01 Cs-134 475.36 1.48 2.25E+00 4.25E-02 2.42E+00 563.25 8.34 2.07E-01 4.46E-01 569.33 15.37 7.35E-02 2.37E-01 604.72 97.62 -3.09E-02 5.42E-02 795.86 85.46 4.34E-03 4.25E-02 801.95 8.69 -7.76E-02 4.10E-01 1038.61 0.99 2.86E+00 4.73E+00 1167.97 1.79 -5.35E-02 2.97E+00 1365.19 3.02 -8.18E-01 1.32E+00 Cs-137 661.66 85.10 8.17E-03 3.94E-02 3.94E-02 Eu-152 121.78 28.67 -2.04E-02 1.04E-01 1.07E-01 244.70 7.61 5.72E-02 4.67E-01 295.94 0.45 3.00E+00 7.17E+00 344.28 26.60 -9.43E-03 1.04E-01 367.79 0.86 1.16E+00 3.78E+00 411.12 2.24 4.20E-01 1.50E+00 443.96 2.83 -3.47E-01 1.04E+00 488.68 0.42 -3.09E+00 7.94E+00 563.99 0.49 7.20E-01 7.47E+00 586.26 0.46 7.53E+00 9.94E+00 678.62 0.47 1.58E+00 7.08E+00 688.67 0.86 1.89E+00 3.58E+00 719.35 0.28 1.02E+00 1.48E+01 778.90 12.96 7.12E-02 2.88E-01 810.45 0.32 2.00E+00 1.04E+01 867.37 4.26 -4.43E-01 9.94E-01 919.33 0.43 -8.67E+00 9.73E+00 964.08 14.65 2.12E-01 3.61E-01 1085.87 10.24 -2.20E-02 4.14E-01 1089.74 1.73 5.03E-01 2.46E+00 1112.07 13.69 -1.68E-01 3.30E-01 1212.95 1.43 -3.52E+00 3.42E+00 1249.94 0.19 6.61E+00 2.57E+01 1299.14 1.63 -6.48E-01 2.86E+00 1408.01 21.07 -2.65E-01 2.08E-01 1457.64 0.50 7.88E+01 2.96E+01 1528.10 0.28 2.46E+00 9.15E+00 Eu-154 123.07 40.40 2.38E-02 7.71E-02 7.71E-02 247.93 6.89 6.89E-02 4.44E-01 591.76 4.95 -4.19E-01 6.54E-01 692.42 1.78 3.57E-01 2.02E+00 723.30 20.06 -4.62E-02 2.47E-01 756.80 4.52 2.63E-01 7.76E-01 873.18 12.08 7.63E-02 3.46E-01
| |
| [350]
| |
| | |
| 8/1/2019 9:24:35AM Page 7 of 7 Analysis Report for 01-Aug-19-10011 L1-10221C-FIGS-112SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 1.86E-01 7.71E-02 4.35E-01 1004.76 18.01 -1.40E-01 2.24E-01 1274.43 34.80 4.82E-02 1.25E-01 1596.48 1.80 -2.27E+00 2.18E+00 Eu-155 45.30 1.31 4.53E+00 1.83E-01 1.64E+01 60.01 1.22 -3.84E+00 1.71E+01 86.55 30.70 -1.12E-02 1.89E-01 105.31 21.10 3.61E-02 1.83E-01
| |
| + Ra-226 186.21
| |
| * 3.64 4.88E-01 4.71E-01 4.71E-01 Pa-231 27.36 10.30 2.63E+00 1.11E+00 2.15E+00 283.69 1.70 -1.43E-01 1.75E+00 300.07 2.47 -9.34E-01 1.11E+00 302.65 2.20 3.90E-01 1.26E+00 330.06 1.40 -1.38E-01 2.26E+00
| |
| + U-235 143.76 10.96 5.32E-02 3.00E-02 2.90E-01 163.33 5.08 -3.01E-01 5.60E-01 185.71
| |
| * 57.20 3.11E-02 3.00E-02 202.11 1.08 8.96E-01 2.87E+00 205.31 5.01 -4.98E-02 6.04E-01 Am-241 59.54 35.90 -1.46E-01 6.10E-01 6.10E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [351]
| |
| | |
| 8/1/2019 9:41:10AM Page 1 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS GAMMA SPECTRUM ANALYSIS Sample Identification : 01-Aug-19-10012 Sample Description : L1-10221C-FIGS-113SS Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.769E+03 grams Facility : Default Sample Taken On : 7/31/2019 9:36:00AM Acquisition Started : 8/1/2019 9:25:58AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.2 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 8/1/2019 Efficiency Calibration Description :
| |
| Sample Number : 78409 Fill Height : 1768.92 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 8/1/2019 9:41:01AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [352]
| |
| | |
| 8/1/2019 9:41:10AM Page 2 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.57 948 - 962 954.76 1.06E+02 14.59 3.72E+01 1.29 2 351.74 1401 - 1414 1406.95 6.01E+01 10.32 1.69E+01 0.93 3 609.28 2429 - 2445 2436.37 6.19E+01 8.98 6.07E+00 0.68 4 911.30 3639 - 3650 3644.26 2.16E+01 5.71 4.38E+00 0.70 5 1460.80 5833 - 5853 5843.56 1.69E+02 14.05 7.84E+00 1.10 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 1.00 1460.82
| |
| * 10.66 3.42E+00 3.20E-01 Bi-211 0.93 351.07
| |
| * 13.02 3.91E-01 7.40E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 1.62E-01 2.59E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.66E-01 2.60E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 [353]
| |
| | |
| 8/1/2019 9:41:10AM Page 3 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.43E-01 2.70E-02 785.96 1.06 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.32E-01 3.54E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| [354]
| |
| | |
| 8/1/2019 9:41:10AM Page 4 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 1.000 3.42E+00 3.20E-01
| |
| ? Bi-211 0.931 3.91E-01 7.40E-02 Pb-212 0.999 1.62E-01 2.59E-02 Bi-214 1.000 1.66E-01 2.60E-02
| |
| ? Pb-214 0.997 1.43E-01 2.70E-02 Ac-228 1.000 1.32E-01 3.54E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [355]
| |
| | |
| 8/1/2019 9:41:10AM Page 5 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS UNIDENTIFIED PEAKS Peak Locate Performed on : 8/1/2019 9:41:01AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 3.69E-02 5.03E-02 5.03E-02 BE-7 477.60 10.44 -2.55E-02 3.30E-01 3.30E-01
| |
| + K-40 1460.82
| |
| * 10.66 3.42E+00 4.23E-01 4.23E-01 Mn-54 834.85 99.98 3.09E-02 4.08E-02 4.08E-02 Co-60 1173.23 99.85 2.35E-02 4.19E-02 4.52E-02 1332.49 99.98 2.82E-02 4.19E-02 Nb-94 702.65 99.81 -1.55E-02 3.39E-02 3.39E-02 871.09 99.89 2.26E-02 3.81E-02 Ag-108m 79.13 6.60 -1.63E-01 3.32E-02 1.25E+00 433.94 90.50 -5.38E-03 3.32E-02 614.28 89.80 -8.00E-04 6.09E-02 722.94 90.80 9.90E-03 4.68E-02 Sb-125 176.31 6.84 -3.17E-01 1.03E-01 3.98E-01 380.45 1.52 -8.45E-01 2.19E+00 427.87 29.60 6.93E-03 1.03E-01 463.36 10.49 -1.18E-01 2.83E-01 600.60 17.65 -4.41E-04 2.02E-01 606.71 4.98 1.86E+00 1.19E+00 635.95 11.22 1.67E-02 2.94E-01 [356]
| |
| | |
| 8/1/2019 9:41:10AM Page 6 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.35E+00 1.03E-01 1.80E+00 Ba-133 79.61 2.65 4.89E-01 6.51E-02 3.00E+00 81.00 32.90 -2.32E-01 2.02E-01 276.40 7.16 1.11E-01 4.51E-01 302.85 18.34 9.74E-02 1.71E-01 356.01 62.05 -2.54E-02 6.51E-02 383.85 8.94 -1.48E-01 3.70E-01 Cs-134 475.36 1.48 6.58E-01 4.38E-02 2.25E+00 563.25 8.34 -7.98E-02 3.73E-01 569.33 15.37 7.73E-02 2.07E-01 604.72 97.62 -2.39E-02 5.51E-02 795.86 85.46 -8.46E-04 4.38E-02 801.95 8.69 -2.72E-01 3.98E-01 1038.61 0.99 -1.50E+00 3.94E+00 1167.97 1.79 3.32E-01 2.34E+00 1365.19 3.02 2.79E-01 1.32E+00 Cs-137 661.66 85.10 -9.24E-03 3.83E-02 3.83E-02 Eu-152 121.78 28.67 -6.21E-02 1.12E-01 1.19E-01 244.70 7.61 -4.01E-02 4.04E-01 295.94 0.45 1.74E+00 8.27E+00 344.28 26.60 -6.17E-02 1.12E-01 367.79 0.86 4.89E-01 3.32E+00 411.12 2.24 -2.34E-01 1.28E+00 443.96 2.83 -1.49E-01 1.02E+00 488.68 0.42 6.74E-01 7.08E+00 563.99 0.49 2.46E+00 6.44E+00 586.26 0.46 7.25E+00 1.00E+01 678.62 0.47 3.19E+00 7.81E+00 688.67 0.86 1.29E-01 4.33E+00 719.35 0.28 2.70E+00 1.48E+01 778.90 12.96 -3.65E-01 2.79E-01 810.45 0.32 5.37E+00 1.22E+01 867.37 4.26 -1.78E+00 8.53E-01 919.33 0.43 -1.17E+01 9.23E+00 964.08 14.65 1.77E-01 3.40E-01 1085.87 10.24 5.66E-02 3.81E-01 1089.74 1.73 6.94E-01 2.49E+00 1112.07 13.69 5.20E-02 3.32E-01 1212.95 1.43 1.66E-01 3.87E+00 1249.94 0.19 9.29E+00 2.65E+01 1299.14 1.63 -4.34E-01 2.46E+00 1408.01 21.07 9.95E-02 1.79E-01 1457.64 0.50 7.90E+01 2.94E+01 1528.10 0.28 -7.76E+00 1.69E+01 Eu-154 123.07 40.40 1.75E-02 8.74E-02 8.74E-02 247.93 6.89 -6.45E-02 4.21E-01 591.76 4.95 3.18E-02 6.59E-01 692.42 1.78 1.12E+00 2.07E+00 723.30 20.06 8.47E-02 2.12E-01 756.80 4.52 2.80E-01 7.86E-01 873.18 12.08 1.78E-01 3.22E-01
| |
| [357]
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| 8/1/2019 9:41:10AM Page 7 of 7 Analysis Report for 01-Aug-19-10012 L1-10221C-FIGS-113SS Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -1.15E-01 8.74E-02 3.97E-01 1004.76 18.01 -3.23E-02 2.06E-01 1274.43 34.80 -3.65E-02 1.40E-01 1596.48 1.80 -1.75E+00 1.99E+00 Eu-155 45.30 1.31 -4.42E+00 1.81E-01 1.64E+01 60.01 1.22 2.93E+00 2.08E+01 86.55 30.70 5.57E-02 1.90E-01 105.31 21.10 -4.69E-02 1.81E-01 Ra-226 186.21 3.64 4.79E-01 9.38E-01 9.38E-01 Pa-231 27.36 10.30 8.39E-01 1.43E+00 1.75E+00 283.69 1.70 2.72E-01 1.79E+00 300.07 2.47 -1.10E+00 1.45E+00 302.65 2.20 3.87E-01 1.43E+00 330.06 1.40 -9.08E-01 2.02E+00 U-235 143.76 10.96 -5.42E-02 6.01E-02 2.82E-01 163.33 5.08 2.21E-02 5.80E-01 185.71 57.20 -2.04E-03 6.01E-02 202.11 1.08 1.28E+00 2.84E+00 205.31 5.01 -3.22E-01 5.79E-01 Am-241 59.54 35.90 -6.27E-02 7.11E-01 7.11E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [358]
| |
| | |
| 7/31/2019 10:38:10AM Page 1 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB GAMMA SPECTRUM ANALYSIS Sample Identification : 31-Jul-19-10018 Sample Description : L1-10221C-FSGS-005SB Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.519E+03 grams Facility : Default Sample Taken On : 7/30/2019 3:09:00PM Acquisition Started : 7/31/2019 10:22:58AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P40818B Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 901.1 seconds Dead Time : 0.12 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/29/2019 Efficiency Calibration Used Done On : 7/31/2019 Efficiency Calibration Description :
| |
| Sample Number : 78348 Fill Height : 1519.21 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2012 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/31/2019 10:38:03AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [359]
| |
| | |
| 7/31/2019 10:38:10AM Page 2 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.64 948 - 962 954.65 9.22E+01 17.17 6.98E+01 0.78 2 338.10 1348 - 1356 1352.17 2.68E+01 7.27 1.22E+01 0.88 3 351.96 1401 - 1415 1407.57 6.52E+01 12.46 3.08E+01 0.98 4 583.14 2325 - 2338 2331.76 3.17E+01 7.81 1.03E+01 0.37 5 609.26 2431 - 2443 2436.19 4.47E+01 8.19 8.26E+00 0.52 6 911.10 3638 - 3649 3643.35 3.06E+01 5.83 1.38E+00 0.70 7 1460.54 5831 - 5852 5841.98 2.11E+02 14.87 2.66E+00 1.97 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.98 1460.82
| |
| * 10.66 5.28E+00 4.36E-01 Tl-208 1.00 583.19
| |
| * 85.00 5.31E-02 1.34E-02 Bi-211 0.88 351.07
| |
| * 13.02 5.00E-01 1.04E-01 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.65E-01 3.35E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.44E-01 2.77E-02 768.36 4.89 806.18 1.26 934.06 3.11 [360]
| |
| | |
| 7/31/2019 10:38:10AM Page 3 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.83E-01 3.79E-02 785.96 1.06 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 2.30E-01 6.53E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 2.29E-01 4.46E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [361]
| |
| | |
| 7/31/2019 10:38:10AM Page 4 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.987 5.28E+00 4.36E-01 Tl-208 1.000 5.31E-02 1.34E-02
| |
| ? Bi-211 0.881 5.00E-01 1.04E-01 Pb-212 1.000 1.65E-01 3.35E-02 Bi-214 1.000 1.44E-01 2.77E-02
| |
| ? Pb-214 1.000 1.83E-01 3.79E-02 Ac-228 0.998 2.29E-01 3.68E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [362]
| |
| | |
| 7/31/2019 10:38:10AM Page 5 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB UNIDENTIFIED PEAKS Peak Locate Performed on : 7/31/2019 10:38:03AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 9.47E-02 6.03E-02 6.03E-02 BE-7 477.60 10.44 1.36E-01 4.24E-01 4.24E-01
| |
| + K-40 1460.82
| |
| * 10.66 5.28E+00 3.37E-01 3.37E-01 Mn-54 834.85 99.98 -2.22E-02 4.88E-02 4.88E-02 Co-60 1173.23 99.85 5.21E-02 5.77E-02 7.14E-02 1332.49 99.98 2.17E-02 5.77E-02 Nb-94 702.65 99.81 -9.30E-03 3.89E-02 4.34E-02 871.09 99.89 -1.05E-02 3.89E-02 Ag-108m 79.13 6.60 3.45E-01 4.44E-02 1.71E+00 433.94 90.50 -1.09E-02 4.44E-02 614.28 89.80 -2.72E-02 5.57E-02 722.94 90.80 2.90E-02 5.28E-02 Sb-125 176.31 6.84 2.14E-01 1.45E-01 5.13E-01 380.45 1.52 1.27E-01 2.29E+00 427.87 29.60 3.25E-02 1.45E-01 463.36 10.49 2.48E-01 4.37E-01 600.60 17.65 6.18E-02 2.21E-01 606.71 4.98 1.71E+00 1.24E+00 635.95 11.22 9.30E-02 3.34E-01 [363]
| |
| | |
| 7/31/2019 10:38:10AM Page 6 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 5.85E-01 1.45E-01 2.22E+00 Ba-133 79.61 2.65 2.12E+00 7.16E-02 4.19E+00 81.00 32.90 -1.17E-01 2.86E-01 276.40 7.16 8.88E-02 4.96E-01 302.85 18.34 -1.73E-02 1.95E-01 356.01 62.05 -1.23E-02 7.16E-02 383.85 8.94 2.91E-01 4.17E-01 Cs-134 475.36 1.48 1.43E+00 5.74E-02 2.99E+00 563.25 8.34 -5.49E-02 4.47E-01 569.33 15.37 -3.41E-02 2.40E-01 604.72 97.62 -2.29E-02 5.74E-02 795.86 85.46 2.71E-03 5.81E-02 801.95 8.69 1.70E-01 5.36E-01 1038.61 0.99 -1.09E-01 4.94E+00 1167.97 1.79 -2.17E-01 3.59E+00 1365.19 3.02 -4.19E-02 1.63E+00 Cs-137 661.66 85.10 2.73E-03 4.53E-02 4.53E-02 Eu-152 121.78 28.67 -9.45E-02 1.27E-01 1.44E-01 244.70 7.61 -1.81E-01 5.09E-01 295.94 0.45 5.97E+00 9.94E+00 344.28 26.60 3.21E-02 1.27E-01 367.79 0.86 5.94E-01 3.97E+00 411.12 2.24 1.44E+00 1.67E+00 443.96 2.83 -5.55E-01 1.14E+00 488.68 0.42 -6.34E+00 7.75E+00 563.99 0.49 -4.94E+00 7.60E+00 586.26 0.46 -2.87E+00 1.20E+01 678.62 0.47 8.35E-01 8.48E+00 688.67 0.86 -5.69E-01 4.61E+00 719.35 0.28 -4.88E+00 1.40E+01 778.90 12.96 9.02E-02 3.39E-01 810.45 0.32 -7.61E+00 1.25E+01 867.37 4.26 -1.53E+00 7.88E-01 919.33 0.43 6.79E+00 9.72E+00 964.08 14.65 1.74E-01 3.60E-01 1085.87 10.24 4.00E-01 5.58E-01 1089.74 1.73 1.79E+00 3.43E+00 1112.07 13.69 -3.12E-02 3.64E-01 1212.95 1.43 -2.83E-01 4.39E+00 1249.94 0.19 -1.26E+01 3.13E+01 1299.14 1.63 6.61E-01 3.65E+00 1408.01 21.07 1.80E-02 2.48E-01 1457.64 0.50 1.11E+02 3.90E+01 1528.10 0.28 -2.08E+00 1.43E+01 Eu-154 123.07 40.40 -1.83E-02 1.06E-01 1.06E-01 247.93 6.89 -1.94E-01 5.12E-01 591.76 4.95 6.74E-01 8.83E-01 692.42 1.78 -7.78E-01 2.19E+00 723.30 20.06 7.79E-02 2.39E-01 756.80 4.52 -9.18E-02 9.71E-01 873.18 12.08 9.47E-02 3.76E-01
| |
| [364]
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| 7/31/2019 10:38:10AM Page 7 of 7 Analysis Report for 31-Jul-19-10018 L1-10221C-FSGS-005SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -7.57E-02 1.06E-01 3.81E-01 1004.76 18.01 -1.01E-01 1.67E-01 1274.43 34.80 -4.53E-02 1.44E-01 1596.48 1.80 -2.74E-01 2.74E+00 Eu-155 45.30 1.31 -1.18E+01 2.33E-01 2.74E+01 60.01 1.22 -8.08E+00 3.11E+01 86.55 30.70 1.95E-01 2.54E-01 105.31 21.10 -1.24E-01 2.33E-01 Ra-226 186.21 3.64 6.48E-01 1.12E+00 1.12E+00 Pa-231 27.36 10.30 2.41E+00 1.48E+00 3.45E+00 283.69 1.70 1.69E-01 2.12E+00 300.07 2.47 -1.62E-01 1.48E+00 302.65 2.20 8.23E-02 1.65E+00 330.06 1.40 8.25E-01 2.62E+00 U-235 143.76 10.96 5.26E-03 6.82E-02 3.68E-01 163.33 5.08 -2.53E-01 6.96E-01 185.71 57.20 -1.03E-02 6.82E-02 202.11 1.08 -8.00E-01 3.34E+00 205.31 5.01 -3.43E-01 6.81E-01 Am-241 59.54 35.90 -4.79E-01 1.11E+00 1.11E+00
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [365]
| |
| | |
| 8/1/2019 12:38:31PM Page 1 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB GAMMA SPECTRUM ANALYSIS Sample Identification : 01-Aug-19-10033 Sample Description : L1-10221C-FSGS-005SB Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.519E+03 grams Facility : Default Sample Taken On : 7/30/2019 1:09:00PM Acquisition Started : 8/1/2019 12:08:17PM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 1800.0 seconds Real Time : 1800.6 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 8/1/2019 Efficiency Calibration Description :
| |
| Sample Number : 78430 Fill Height : 1519.21 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 8/1/2019 12:38:21PM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [366]
| |
| | |
| 8/1/2019 12:38:31PM Page 2 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 185.76 367 - 376 371.84 8.64E+01 22.34 1.81E+02 0.84 2 238.62 473 - 481 477.42 2.37E+02 26.68 2.15E+02 1.04 3 295.27 585 - 595 590.59 7.84E+01 19.62 1.25E+02 1.32 4 338.25 671 - 681 676.47 1.01E+02 16.44 7.13E+01 1.43 5 351.92 698 - 707 703.77 1.88E+02 18.82 7.36E+01 1.19 6 511.03 1016 - 1027 1021.75 1.22E+02 14.74 3.83E+01 1.65 7 583.20 1162 - 1170 1166.00 7.68E+01 12.60 3.83E+01 1.40 8 609.27 1213 - 1223 1218.13 9.75E+01 14.35 4.55E+01 1.53 9 911.25 1817 - 1827 1821.96 5.90E+01 10.91 2.50E+01 1.36 10 969.02 1933 - 1944 1937.49 4.36E+01 10.37 2.34E+01 1.45 11 1460.67 2913 - 2928 2921.40 5.60E+02 23.92 4.00E+00 2.04 12 1764.04 3525 - 3532 3528.92 1.91E+01 5.38 4.94E+00 0.73 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty An Pk 1.00 511.00
| |
| * 100.00 6.29E-02 8.74E-03 K-40 0.99 1460.82
| |
| * 10.66 5.27E+00 3.21E-01 Tl-208 1.00 583.19
| |
| * 85.00 4.96E-02 8.66E-03 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.66E-01 2.31E-02[367]
| |
| | |
| 8/1/2019 12:38:31PM Page 3 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb-212 1.00 300.09 3.30 Bi-214 0.99 609.32
| |
| * 45.49 1.21E-01 1.92E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49
| |
| * 15.30 1.44E-01 4.11E-02 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 1.47E-01 3.86E-02 351.93
| |
| * 35.60 2.07E-01 2.65E-02 785.96 1.06 Ra-226 0.96 186.21
| |
| * 3.64 6.45E-01 1.75E-01 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 3.39E-01 6.20E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.68E-01 3.19E-02 964.77 4.99 968.97
| |
| * 15.80 2.11E-01 5.11E-02 1588.20 3.22 U-235 1.00 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 4.10E-02 1.11E-02 202.11 1.08 205.31 5.01
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma
| |
| [368]
| |
| | |
| 8/1/2019 12:38:31PM Page 4 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| An Pk 1.000 6.29E-02 8.74E-03 K-40 0.996 5.27E+00 3.21E-01 Tl-208 1.000 4.96E-02 8.66E-03 X Bi-211 0.892 Pb-212 1.000 1.66E-01 2.31E-02 Bi-214 0.995 1.25E-01 1.74E-02 Pb-214 1.000 1.88E-01 2.18E-02
| |
| ? Ra-226 0.969 6.45E-01 1.75E-01 Ac-228 1.000 2.06E-01 2.48E-02
| |
| ? U-235 1.000 4.10E-02 1.11E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [369]
| |
| | |
| 8/1/2019 12:38:31PM Page 5 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB UNIDENTIFIED PEAKS Peak Locate Performed on : 8/1/2019 12:38:21PM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| + An Pk 511.00
| |
| * 100.00 6.29E-02 1.86E-02 1.86E-02 BE-7 477.60 10.44 5.12E-02 2.22E-01 2.22E-01
| |
| + K-40 1460.82
| |
| * 10.66 5.27E+00 1.38E-01 1.38E-01 Mn-54 834.85 99.98 -7.32E-03 2.54E-02 2.54E-02 Co-60 1173.23 99.85 1.25E-02 2.48E-02 3.52E-02 1332.49 99.98 -9.72E-03 2.48E-02 Nb-94 702.65 99.81 -3.30E-03 2.33E-02 2.33E-02 871.09 99.89 2.65E-04 2.40E-02 Ag-108m 79.13 6.60 4.15E-01 2.35E-02 7.46E-01 433.94 90.50 6.66E-03 2.35E-02 614.28 89.80 -2.12E-03 3.45E-02 722.94 90.80 1.11E-02 2.89E-02 Sb-125 176.31 6.84 7.78E-02 6.63E-02 3.21E-01 380.45 1.52 -2.21E-01 1.32E+00 427.87 29.60 -8.62E-03 6.63E-02 463.36 10.49 1.29E-01 2.22E-01 600.60 17.65 2.35E-02 1.34E-01 606.71 4.98 4.28E-02 7.49E-01 635.95 11.22 -1.20E-01 2.20E-01 [370]
| |
| | |
| 8/1/2019 12:38:31PM Page 6 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.16E-01 6.63E-02 1.24E+00 Ba-133 79.61 2.65 5.62E-01 4.69E-02 1.75E+00 81.00 32.90 -1.46E-01 1.17E-01 276.40 7.16 -2.03E-02 2.92E-01 302.85 18.34 6.83E-02 1.17E-01 356.01 62.05 -7.66E-02 4.69E-02 383.85 8.94 -1.35E-02 2.21E-01 Cs-134 475.36 1.48 -8.44E-02 3.01E-02 1.49E+00 563.25 8.34 -2.17E-01 2.31E-01 569.33 15.37 2.32E-02 1.45E-01 604.72 97.62 -3.68E-03 3.28E-02 795.86 85.46 3.85E-03 3.01E-02 801.95 8.69 -5.12E-02 2.76E-01 1038.61 0.99 -2.09E+00 2.63E+00 1167.97 1.79 1.08E+00 2.05E+00 1365.19 3.02 -4.07E-02 6.80E-01 Cs-137 661.66 85.10 4.63E-03 2.91E-02 2.91E-02 Eu-152 121.78 28.67 1.27E-02 7.48E-02 7.48E-02 244.70 7.61 2.32E-02 3.15E-01 295.94 0.45 -7.37E-01 5.77E+00 344.28 26.60 -3.10E-02 7.73E-02 367.79 0.86 3.86E-01 2.27E+00 411.12 2.24 4.72E-01 9.56E-01 443.96 2.83 -1.37E-01 7.50E-01 488.68 0.42 9.72E-01 5.33E+00 563.99 0.49 -3.59E+00 3.87E+00 586.26 0.46 -3.90E+00 7.36E+00 678.62 0.47 -1.87E+00 4.27E+00 688.67 0.86 -6.94E-01 3.02E+00 719.35 0.28 -3.50E+00 8.23E+00 778.90 12.96 -6.63E-03 1.87E-01 810.45 0.32 -3.64E+00 6.88E+00 867.37 4.26 -7.61E-01 5.22E-01 919.33 0.43 6.57E-02 6.36E+00 964.08 14.65 -7.33E-02 2.45E-01 1085.87 10.24 -7.84E-02 2.73E-01 1089.74 1.73 -4.58E-01 1.74E+00 1112.07 13.69 8.96E-02 2.61E-01 1212.95 1.43 -1.03E+00 2.21E+00 1249.94 0.19 -4.47E+00 1.55E+01 1299.14 1.63 -1.08E+00 1.75E+00 1408.01 21.07 -3.44E-02 1.29E-01 1457.64 0.50 -4.39E-01 2.34E+01 1528.10 0.28 3.96E+00 8.34E+00 Eu-154 123.07 40.40 1.27E-02 5.30E-02 5.30E-02 247.93 6.89 -5.63E-02 2.99E-01 591.76 4.95 -4.92E-02 4.55E-01 692.42 1.78 -4.67E-01 1.45E+00 723.30 20.06 5.22E-02 1.32E-01 756.80 4.52 2.09E-02 5.54E-01 873.18 12.08 1.54E-01 2.07E-01
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| [371]
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| 8/1/2019 12:38:31PM Page 7 of 7 Analysis Report for 01-Aug-19-10033 L1-10221C-FSGS-005SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 9.85E-02 5.30E-02 2.66E-01 1004.76 18.01 6.77E-02 1.56E-01 1274.43 34.80 -2.02E-02 8.60E-02 1596.48 1.80 -1.28E+00 1.32E+00 Eu-155 45.30 1.31 -6.60E-02 1.11E-01 6.95E+00 60.01 1.22 1.46E+00 8.19E+00 86.55 30.70 2.98E-02 1.11E-01 105.31 21.10 -1.42E-02 1.15E-01
| |
| + Ra-226 186.21
| |
| * 3.64 6.45E-01 5.35E-01 5.35E-01 Pa-231 27.36 10.30 3.42E-01 6.83E-01 6.83E-01 283.69 1.70 -8.58E-01 1.08E+00 300.07 2.47 2.70E-01 8.74E-01 302.65 2.20 5.69E-01 9.78E-01 330.06 1.40 1.18E+00 1.64E+00
| |
| + U-235 143.76 10.96 5.13E-02 3.41E-02 1.86E-01 163.33 5.08 2.47E-01 4.56E-01 185.71
| |
| * 57.20 4.10E-02 3.41E-02 202.11 1.08 -1.49E-02 2.08E+00 205.31 5.01 -1.44E-01 4.59E-01 Am-241 59.54 35.90 3.26E-03 2.83E-01 2.83E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [372]
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| | |
| 7/31/2019 10:19:05AM Page 1 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB GAMMA SPECTRUM ANALYSIS Sample Identification : 31-Jul-19-10016 Sample Description : L1-10221C-FSGS-013SB Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.409E+03 grams Facility : Default Sample Taken On : 7/29/2019 3:20:00PM Acquisition Started : 7/31/2019 10:03:51AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 352 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 7/31/2019 Efficiency Calibration Description :
| |
| Sample Number : 78346 Fill Height : 1408.64 gram Certificate Name : Eu155-Na22 Certificate Date : 1/7/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/31/2019 10:18:53AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [373]
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| 7/31/2019 10:19:05AM Page 2 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 77.33 305 - 315 310.65 2.50E+01 15.23 8.20E+01 0.57 2 185.82 739 - 751 743.99 5.41E+01 16.29 7.99E+01 1.26 3 238.71 946 - 962 955.32 1.79E+02 22.29 1.02E+02 1.05 4 295.22 1176 - 1190 1181.09 9.12E+01 14.47 3.98E+01 1.14 5 338.22 1348 - 1358 1352.92 3.62E+01 11.38 3.88E+01 1.21 6 351.90 1401 - 1414 1407.61 1.02E+02 15.20 4.68E+01 0.97 7 583.20 2325 - 2339 2332.12 7.08E+01 11.34 2.02E+01 0.61 8 609.43 2429 - 2446 2436.99 1.10E+02 13.08 1.91E+01 1.34 9 661.55 2638 - 2654 2645.39 9.42E+01 12.61 1.98E+01 1.11 10 911.42 3639 - 3653 3644.72 4.02E+01 9.30 1.58E+01 0.75 11 1460.68 5830 - 5856 5843.09 4.67E+02 21.61 0.00E+00 2.10 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 1.00E+01 6.36E-01 Cs-137 0.99 661.66
| |
| * 85.10 1.49E-01 2.19E-02 Tl-208 1.00 583.19
| |
| * 85.00 1.03E-01 1.77E-02 Pb-212 0.99 115.18 0.60 238.63
| |
| * 43.60 2.85E-01 4.23E-02 300.09 3.30 [374]
| |
| | |
| 7/31/2019 10:19:05AM Page 3 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Pb212-XR 0.99 74.82 10.28 77.11
| |
| * 17.10 2.33E-01 1.44E-01 87.35 3.97 89.78 1.46 Bi-214 0.99 609.32
| |
| * 45.49 3.08E-01 4.11E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 1.00 241.99 7.25 295.22
| |
| * 18.42 3.86E-01 6.86E-02 351.93
| |
| * 35.60 2.53E-01 4.27E-02 785.96 1.06 Pb214-XR 0.99 74.82 5.80 77.11
| |
| * 9.70 4.11E-01 2.54E-01 87.35 2.24 89.78 0.82 Ra-226 0.97 186.21
| |
| * 3.64 9.22E-01 2.87E-01 Ac-228 0.99 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32
| |
| * 11.27 2.75E-01 8.94E-02 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 2.60E-01 6.11E-02 964.77 4.99 968.97 15.80 1588.20 3.22 U-235 0.99 143.76 10.96 163.33 5.08 185.71
| |
| * 57.20 5.87E-02 1.83E-02 202.11 1.08 205.31 5.01
| |
| [375]
| |
| | |
| 7/31/2019 10:19:05AM Page 4 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.997 1.00E+01 6.36E-01 Cs-137 0.998 1.49E-01 2.19E-02 Tl-208 1.000 1.03E-01 1.77E-02 X Bi-211 0.894 Pb-212 0.999 2.85E-01 4.23E-02
| |
| ? Pb212-XR 0.996 2.33E-01 1.44E-01 Bi-214 0.999 3.08E-01 4.11E-02 Pb-214 1.000 2.90E-01 3.63E-02
| |
| ? Pb214-XR 0.996 4.11E-01 2.54E-01
| |
| ? Ra-226 0.975 9.22E-01 2.87E-01 Ac-228 0.998 2.65E-01 5.05E-02
| |
| ? U-235 0.999 5.87E-02 1.83E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [376]
| |
| | |
| 7/31/2019 10:19:05AM Page 5 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB UNIDENTIFIED PEAKS Peak Locate Performed on : 7/31/2019 10:18:53AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 8.77E-02 6.49E-02 6.49E-02 BE-7 477.60 10.44 3.99E-01 4.67E-01 4.67E-01
| |
| + K-40 1460.82
| |
| * 10.66 1.00E+01 6.17E-02 6.17E-02 Mn-54 834.85 99.98 1.72E-02 4.93E-02 4.93E-02 Co-60 1173.23 99.85 6.59E-02 6.59E-02 7.94E-02 1332.49 99.98 2.82E-02 6.59E-02 Nb-94 702.65 99.81 -1.36E-02 4.56E-02 4.56E-02 871.09 99.89 -3.38E-03 4.99E-02 Ag-108m 79.13 6.60 -4.51E-01 4.77E-02 1.49E+00 433.94 90.50 -4.83E-03 4.77E-02 614.28 89.80 2.74E-03 8.64E-02 722.94 90.80 4.72E-02 5.85E-02 Sb-125 176.31 6.84 -3.00E-01 1.55E-01 5.49E-01 380.45 1.52 -3.69E-01 2.86E+00 427.87 29.60 8.69E-02 1.55E-01 463.36 10.49 -2.08E-01 4.16E-01 600.60 17.65 4.00E-02 2.69E-01 606.71 4.98 3.46E+00 1.65E+00 635.95 11.22 -8.28E-02 4.19E-01 [377]
| |
| | |
| 7/31/2019 10:19:05AM Page 6 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -4.41E-02 1.55E-01 2.47E+00 Ba-133 79.61 2.65 -6.60E-01 9.02E-02 3.59E+00 81.00 32.90 -2.04E-01 2.35E-01 276.40 7.16 -5.08E-01 5.11E-01 302.85 18.34 6.90E-02 2.21E-01 356.01 62.05 -5.52E-02 9.02E-02 383.85 8.94 -9.30E-02 4.77E-01 Cs-134 475.36 1.48 7.70E-01 6.50E-02 3.13E+00 563.25 8.34 2.53E-01 5.26E-01 569.33 15.37 -1.11E-01 2.70E-01 604.72 97.62 -1.47E-02 7.59E-02 795.86 85.46 3.57E-03 6.50E-02 801.95 8.69 -4.95E-01 5.79E-01 1038.61 0.99 -3.78E+00 4.93E+00 1167.97 1.79 3.38E+00 4.35E+00 1365.19 3.02 6.34E-01 1.97E+00
| |
| + Cs-137 661.66
| |
| * 85.10 1.49E-01 4.78E-02 4.78E-02 Eu-152 121.78 28.67 -6.25E-02 1.49E-01 1.49E-01 244.70 7.61 -3.75E-01 6.21E-01 295.94 0.45 2.18E+01 1.21E+01 344.28 26.60 -1.58E-01 1.56E-01 367.79 0.86 2.78E+00 4.38E+00 411.12 2.24 6.38E-01 1.96E+00 443.96 2.83 -3.17E-01 1.40E+00 488.68 0.42 6.89E+00 1.03E+01 563.99 0.49 4.26E+00 8.92E+00 586.26 0.46 1.20E+01 1.48E+01 678.62 0.47 -1.43E+00 9.76E+00 688.67 0.86 2.70E+00 4.56E+00 719.35 0.28 -2.47E+00 1.68E+01 778.90 12.96 -1.05E-02 3.67E-01 810.45 0.32 1.70E+00 1.59E+01 867.37 4.26 -3.44E+00 1.15E+00 919.33 0.43 7.84E+00 1.19E+01 964.08 14.65 4.87E-01 5.38E-01 1085.87 10.24 -2.31E-01 5.85E-01 1089.74 1.73 -2.06E+00 3.34E+00 1112.07 13.69 -3.52E-01 4.39E-01 1212.95 1.43 2.31E+00 5.55E+00 1249.94 0.19 1.68E+01 3.72E+01 1299.14 1.63 1.29E+00 4.14E+00 1408.01 21.07 -1.78E-01 1.91E-01 1457.64 0.50 2.17E+02 4.89E+01 1528.10 0.28 -1.44E+01 1.05E+01 Eu-154 123.07 40.40 -2.19E-03 1.08E-01 1.08E-01 247.93 6.89 4.67E-01 6.28E-01 591.76 4.95 4.84E-01 9.23E-01 692.42 1.78 -1.55E-01 2.35E+00 723.30 20.06 1.38E-01 2.67E-01 756.80 4.52 1.85E-01 1.17E+00 873.18 12.08 1.83E-01 3.96E-01
| |
| [378]
| |
| | |
| 7/31/2019 10:19:05AM Page 7 of 7 Analysis Report for 31-Jul-19-10016 L1-10221C-FSGS-013SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 4.40E-01 1.08E-01 5.54E-01 1004.76 18.01 2.05E-02 3.05E-01 1274.43 34.80 1.71E-02 1.89E-01 1596.48 1.80 -2.25E+00 2.83E+00 Eu-155 45.30 1.31 -1.17E+01 2.38E-01 2.14E+01 60.01 1.22 1.25E+00 2.45E+01 86.55 30.70 -2.02E-02 2.54E-01 105.31 21.10 3.98E-02 2.38E-01
| |
| + Ra-226 186.21
| |
| * 3.64 9.22E-01 8.89E-01 8.89E-01 Pa-231 27.36 10.30 2.82E+00 1.86E+00 2.61E+00 283.69 1.70 1.42E+00 2.39E+00 300.07 2.47 -8.71E-02 1.86E+00 302.65 2.20 1.01E+00 1.86E+00 330.06 1.40 3.08E-01 2.87E+00
| |
| + U-235 143.76 10.96 -3.36E-01 5.66E-02 3.98E-01 163.33 5.08 1.83E-01 7.99E-01 185.71
| |
| * 57.20 5.87E-02 5.66E-02 202.11 1.08 2.30E+00 3.84E+00 205.31 5.01 -8.12E-01 7.67E-01 Am-241 59.54 35.90 -5.20E-02 8.69E-01 8.69E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [379]
| |
| | |
| 7/31/2019 10:37:54AM Page 1 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB GAMMA SPECTRUM ANALYSIS Sample Identification : 31-Jul-19-10017 Sample Description : L1-10221C-FIGS-100SB Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.257E+03 grams Facility : Default Sample Taken On : 7/30/2019 9:54:00AM Acquisition Started : 7/31/2019 10:22:45AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : 324 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 4096 Peak Area Range (in channels) : 120 - 4096 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 9/29/2018 Efficiency Calibration Used Done On : 7/31/2019 Efficiency Calibration Description :
| |
| Sample Number : 78347 Fill Height : 1257.48 gram Certificate Name : Eu155-Na22 Certificate Date : 1/30/2013 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/31/2019 10:37:48AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 4096
| |
| [380]
| |
| | |
| 7/31/2019 10:37:54AM Page 2 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.65 473 - 481 477.49 1.04E+02 16.71 8.13E+01 1.17 2 351.80 700 - 708 703.54 6.92E+01 12.35 3.88E+01 1.20 3 583.18 1162 - 1171 1165.97 4.88E+01 8.34 9.19E+00 1.66 4 609.27 1215 - 1223 1218.13 4.74E+01 8.52 1.16E+01 0.98 5 911.28 1818 - 1828 1822.00 3.26E+01 8.34 1.54E+01 1.01 6 1460.74 2915 - 2928 2921.53 2.37E+02 15.39 0.00E+00 2.11 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.99 1460.82
| |
| * 10.66 4.75E+00 3.71E-01 Tl-208 1.00 583.19
| |
| * 85.00 6.64E-02 1.20E-02 Bi-211 0.91 351.07
| |
| * 13.02 4.35E-01 8.51E-02 Pb-212 1.00 115.18 0.60 238.63
| |
| * 43.60 1.52E-01 2.74E-02 300.09 3.30 Bi-214 1.00 609.32
| |
| * 45.49 1.24E-01 2.35E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 [381]
| |
| | |
| 7/31/2019 10:37:54AM Page 3 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 1.00 1155.21 1.63 1238.12 5.83 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16 Pb-214 0.99 241.99 7.25 295.22 18.42 351.93
| |
| * 35.60 1.59E-01 3.11E-02 785.96 1.06 Ac-228 1.00 129.07 2.42 209.25 3.89 270.24 3.46 328.00 2.95 338.32 11.27 409.46 1.92 463.00 4.40 794.95 4.25 911.20
| |
| * 25.80 1.97E-01 5.11E-02 964.77 4.99 968.97 15.80 1588.20 3.22
| |
| * = Energy line found in the spectrum.
| |
| - = Manually added nuclide.
| |
| ? = Manually edited nuclide.
| |
| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT
| |
| [382]
| |
| | |
| 7/31/2019 10:37:54AM Page 4 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
| |
| K-40 0.999 4.75E+00 3.71E-01 Tl-208 1.000 6.64E-02 1.20E-02
| |
| ? Bi-211 0.919 4.35E-01 8.51E-02 Pb-212 1.000 1.52E-01 2.74E-02 Bi-214 1.000 1.24E-01 2.35E-02
| |
| ? Pb-214 0.998 1.59E-01 3.11E-02 Ac-228 1.000 1.97E-01 5.11E-02
| |
| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
| |
| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
| |
| [383]
| |
| | |
| 7/31/2019 10:37:54AM Page 5 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB UNIDENTIFIED PEAKS Peak Locate Performed on : 7/31/2019 10:37:48AM Peak Locate From Channel : 120 Peak Locate To Channel : 4096 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide All peaks were identified.
| |
| M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| An Pk 511.00 100.00 6.69E-02 5.18E-02 5.18E-02 BE-7 477.60 10.44 8.76E-02 3.33E-01 3.33E-01
| |
| + K-40 1460.82
| |
| * 10.66 4.75E+00 5.76E-02 5.76E-02 Mn-54 834.85 99.98 1.13E-02 4.15E-02 4.15E-02 Co-60 1173.23 99.85 -1.13E-02 3.60E-02 3.83E-02 1332.49 99.98 -9.97E-04 3.60E-02 Nb-94 702.65 99.81 -1.61E-02 2.97E-02 2.97E-02 871.09 99.89 6.24E-03 3.42E-02 Ag-108m 79.13 6.60 -9.08E-02 2.76E-02 1.01E+00 433.94 90.50 -1.21E-02 2.76E-02 614.28 89.80 -1.00E-03 4.48E-02 722.94 90.80 -3.67E-03 4.02E-02 Sb-125 176.31 6.84 -1.67E-01 9.65E-02 4.56E-01 380.45 1.52 -6.56E-01 1.92E+00 427.87 29.60 2.59E-02 9.65E-02 463.36 10.49 2.05E-01 3.47E-01 600.60 17.65 6.39E-02 2.30E-01 606.71 4.98 -9.74E-01 1.09E+00 635.95 11.22 -4.70E-02 2.41E-01 [384]
| |
| | |
| 7/31/2019 10:37:54AM Page 6 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Sb-125 671.44 1.79 -1.42E+00 9.65E-02 1.80E+00 Ba-133 79.61 2.65 1.21E+00 6.37E-02 2.53E+00 81.00 32.90 -3.99E-02 1.76E-01 276.40 7.16 6.91E-02 4.16E-01 302.85 18.34 2.43E-02 1.60E-01 356.01 62.05 -2.74E-02 6.37E-02 383.85 8.94 -1.80E-02 3.34E-01 Cs-134 475.36 1.48 4.51E-01 5.05E-02 2.24E+00 563.25 8.34 9.77E-02 4.13E-01 569.33 15.37 1.38E-02 2.40E-01 604.72 97.62 -8.00E-02 5.05E-02 795.86 85.46 1.00E-02 5.13E-02 801.95 8.69 -1.41E-02 4.65E-01 1038.61 0.99 4.75E-01 4.69E+00 1167.97 1.79 -1.41E+00 2.19E+00 1365.19 3.02 2.19E-01 1.36E+00 Cs-137 661.66 85.10 3.56E-02 5.18E-02 5.18E-02 Eu-152 121.78 28.67 2.02E-02 1.05E-01 1.05E-01 244.70 7.61 -2.75E-01 4.08E-01 295.94 0.45 6.58E+00 8.24E+00 344.28 26.60 -1.03E-01 1.13E-01 367.79 0.86 9.59E-01 3.44E+00 411.12 2.24 4.25E-01 1.47E+00 443.96 2.83 -4.12E-02 1.13E+00 488.68 0.42 1.68E+00 7.33E+00 563.99 0.49 5.18E-01 6.91E+00 586.26 0.46 -2.04E+00 1.08E+01 678.62 0.47 5.08E+00 8.58E+00 688.67 0.86 -1.99E+00 3.97E+00 719.35 0.28 -2.14E+00 1.26E+01 778.90 12.96 -1.90E-01 2.63E-01 810.45 0.32 -6.39E+00 1.07E+01 867.37 4.26 8.64E-02 7.35E-01 919.33 0.43 -6.95E+00 8.29E+00 964.08 14.65 1.60E-01 3.54E-01 1085.87 10.24 -1.27E-01 3.76E-01 1089.74 1.73 1.64E+00 2.86E+00 1112.07 13.69 6.92E-02 3.35E-01 1212.95 1.43 -1.75E+00 3.65E+00 1249.94 0.19 1.23E+01 3.04E+01 1299.14 1.63 -1.41E-01 2.66E+00 1408.01 21.07 8.61E-02 1.85E-01 1457.64 0.50 -1.15E+01 3.26E+01 1528.10 0.28 2.55E+00 1.15E+01 Eu-154 123.07 40.40 9.48E-03 7.45E-02 7.45E-02 247.93 6.89 -1.92E-01 4.06E-01 591.76 4.95 -2.64E-01 6.67E-01 692.42 1.78 8.36E-01 1.99E+00 723.30 20.06 -2.42E-02 1.79E-01 756.80 4.52 -1.37E-01 8.02E-01 873.18 12.08 -1.28E-01 2.76E-01
| |
| [385]
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| 7/31/2019 10:37:54AM Page 7 of 7 Analysis Report for 31-Jul-19-10017 L1-10221C-FIGS-100SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 996.29 10.48 -2.25E-02 7.45E-02 3.83E-01 1004.76 18.01 6.24E-02 2.61E-01 1274.43 34.80 -5.87E-02 1.19E-01 1596.48 1.80 -2.32E-01 1.98E+00 Eu-155 45.30 1.31 7.30E-01 1.62E-01 1.00E+01 60.01 1.22 -3.62E+00 1.07E+01 86.55 30.70 9.46E-02 1.62E-01 105.31 21.10 6.72E-02 1.70E-01 Ra-226 186.21 3.64 3.35E-01 9.32E-01 9.32E-01 Pa-231 27.36 10.30 1.80E-01 9.77E-01 9.77E-01 283.69 1.70 4.07E-01 1.78E+00 300.07 2.47 -2.09E+00 1.11E+00 302.65 2.20 2.03E-01 1.33E+00 330.06 1.40 5.72E-02 2.10E+00 U-235 143.76 10.96 8.30E-02 5.96E-02 2.63E-01 163.33 5.08 -6.70E-02 6.64E-01 185.71 57.20 2.22E-02 5.96E-02 202.11 1.08 -1.31E+00 2.84E+00 205.31 5.01 -2.32E-01 6.48E-01 Am-241 59.54 35.90 -8.25E-03 3.87E-01 3.87E-01
| |
| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
| |
| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
| |
| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
| |
| [386]
| |
| | |
| 7/31/2019 10:18:43AM Page 1 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB GAMMA SPECTRUM ANALYSIS Sample Identification : 31-Jul-19-10015 Sample Description : L1-10221C-FIGS-101SB Sample Type : Soil Unit :
| |
| Sample Point :
| |
| Sample Size : 1.409E+03 grams Facility : Default Sample Taken On : 7/29/2019 3:10:00PM Acquisition Started : 7/31/2019 10:03:34AM Procedure : 130G_SOIL_1 Operator : Administrator Detector Name : P11314 Geometry : 130G_SOIL_1 Live Time : 900.0 seconds Real Time : 900.3 seconds Dead Time : 0.03 %
| |
| Peak Locate Threshold : 3.00 Peak Locate Range (in channels) : 120 - 8192 Peak Area Range (in channels) : 120 - 8192 Identification Energy Tolerance : 1.000 keV Energy Calibration Used Done On : 1/24/2019 Efficiency Calibration Used Done On : 7/31/2019 Efficiency Calibration Description :
| |
| Sample Number : 78345 Fill Height : 1409.48 gram Certificate Name : Eu155-Na22 Certificate Date : 12/22/2008 12:00:00PM PEAK ANALYSIS REPORT Peak Analysis Performed on : 7/31/2019 10:18:36AM Peak Analysis From Channel : 120 Peak Analysis To Channel : 8192
| |
| [387]
| |
| | |
| 7/31/2019 10:18:43AM Page 2 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM No. (keV) start end Centroid Area Uncertainty Counts (keV) 1 238.83 948 - 960 954.91 8.48E+01 15.20 5.52E+01 1.07 2 558.48 2226 - 2238 2232.12 2.78E+01 6.55 5.18E+00 1.17 3 583.03 2325 - 2339 2330.25 5.20E+01 8.96 9.96E+00 1.01 4 609.19 2429 - 2441 2434.81 5.93E+01 9.21 9.75E+00 1.01 5 1460.45 5828 - 5851 5839.74 2.63E+02 17.27 8.87E+00 1.97 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma No background subtract performed on this spectrum.
| |
| NUCLIDE IDENTIFICATION REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB IDENTIFIED NUCLIDES Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty K-40 0.97 1460.82
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| * 10.66 6.06E+00 4.77E-01 Tl-208 0.99 583.19
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| * 85.00 8.00E-02 1.46E-02 Pb-212 0.99 115.18 0.60 238.63
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| * 43.60 1.37E-01 2.69E-02 300.09 3.30 Bi-214 0.99 609.32
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| * 45.49 1.75E-01 2.92E-02 768.36 4.89 806.18 1.26 934.06 3.11 1120.29 14.92 1155.21 1.63 1238.12 5.83 [388]
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| 7/31/2019 10:18:43AM Page 3 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB Nuclide Id Energy Yield(%) Activity Activity Name Confidence (keV) (pCi/grams) Uncertainty Bi-214 0.99 1280.98 1.43 1377.67 3.99 1385.31 0.79 1401.52 1.33 1407.99 2.39 1509.21 2.13 1661.27 1.05 1729.59 2.88 1764.49 15.30 1847.43 2.03 2118.51 1.16
| |
| * = Energy line found in the spectrum.
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| - = Manually added nuclide.
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| ? = Manually edited nuclide.
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| @ = Energy line not used for Weighted Mean Activity Energy Tolerance : 1.000 keV Nuclide confidence index threshold = 0.30 Errors quoted at 1.000sigma INTERFERENCE CORRECTED REPORT Nuclide Nuclide Wt mean Wt mean Comments Name Id Activity Activity Confidence Uncertainty (pCi/grams)
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| K-40 0.978 6.06E+00 4.77E-01 Tl-208 0.996 8.00E-02 1.46E-02 Pb-212 0.994 1.37E-01 2.69E-02 Bi-214 0.999 1.75E-01 2.92E-02
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| ? = nuclide is part of an undetermined solution X = nuclide rejected by the interference analysis
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| @ = nuclide contains energy lines not used in Weighted Mean Activity Errors quoted at 1.000sigma
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| [389]
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| 7/31/2019 10:18:43AM Page 4 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB UNIDENTIFIED PEAKS Peak Locate Performed on : 7/31/2019 10:18:36AM Peak Locate From Channel : 120 Peak Locate To Channel : 8192 Peak CPS (%) Peak Tolerance Peak No. Energy (keV) Peak Size (CPS) Uncertainty Type Nuclide 2 558.48 3.09091E-02 23.54 M = First peak in a multiplet region m = Other peak in a multiplet region F = Fitted singlet Errors quoted at 1.000sigma NUCLIDE MDA REPORT Nuclide Library Used : C:\Canberra\Apex\Root\Default\Library\ZION LIB-BNL.NLB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
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| (keV)
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| An Pk 511.00 100.00 6.57E-02 5.28E-02 5.28E-02 BE-7 477.60 10.44 -1.96E-01 3.25E-01 3.25E-01
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| + K-40 1460.82
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| * 10.66 6.06E+00 5.29E-01 5.29E-01 Mn-54 834.85 99.98 -1.36E-02 4.08E-02 4.08E-02 Co-60 1173.23 99.85 -5.63E-04 4.91E-02 6.04E-02 1332.49 99.98 -7.13E-03 4.91E-02 Nb-94 702.65 99.81 1.35E-02 3.79E-02 3.85E-02 871.09 99.89 -2.81E-02 3.79E-02 Ag-108m 79.13 6.60 3.33E-01 3.72E-02 1.16E+00 433.94 90.50 6.65E-03 3.72E-02 614.28 89.80 -5.49E-02 5.70E-02 722.94 90.80 1.71E-02 5.00E-02 Sb-125 176.31 6.84 3.52E-01 1.21E-01 4.57E-01 380.45 1.52 4.43E-01 2.21E+00 427.87 29.60 5.70E-02 1.21E-01 463.36 10.49 1.84E-01 3.65E-01 600.60 17.65 1.67E-02 2.03E-01 606.71 4.98 1.90E+00 1.31E+00 [390]
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| 7/31/2019 10:18:43AM Page 5 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
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| (keV)
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| Sb-125 635.95 11.22 -9.51E-02 1.21E-01 3.44E-01 671.44 1.79 -3.07E-01 2.12E+00 Ba-133 79.61 2.65 -2.98E-02 5.71E-02 2.79E+00 81.00 32.90 -1.08E-01 1.94E-01 276.40 7.16 -1.19E-01 4.14E-01 302.85 18.34 8.35E-02 1.96E-01 356.01 62.05 -3.87E-02 5.71E-02 383.85 8.94 8.43E-02 3.82E-01 Cs-134 475.36 1.48 -1.48E+00 5.35E-02 2.21E+00 563.25 8.34 -2.68E-01 4.85E-01 569.33 15.37 1.79E-02 2.33E-01 604.72 97.62 -7.31E-03 5.50E-02 795.86 85.46 4.49E-02 5.35E-02 801.95 8.69 -2.54E-01 4.35E-01 1038.61 0.99 -1.83E+00 4.56E+00 1167.97 1.79 -2.56E-01 2.97E+00 1365.19 3.02 5.98E-02 1.45E+00 Cs-137 661.66 85.10 2.18E-02 5.69E-02 5.69E-02 Eu-152 121.78 28.67 -6.68E-02 1.06E-01 1.06E-01 244.70 7.61 3.38E-01 4.81E-01 295.94 0.45 -3.31E+00 8.83E+00 344.28 26.60 4.74E-02 1.19E-01 367.79 0.86 1.04E+00 3.51E+00 411.12 2.24 6.40E-01 1.64E+00 443.96 2.83 -9.76E-01 1.15E+00 488.68 0.42 4.73E-01 8.26E+00 563.99 0.49 -1.12E+00 7.24E+00 586.26 0.46 -1.76E+00 1.26E+01 678.62 0.47 4.61E-01 7.64E+00 688.67 0.86 1.01E+00 4.33E+00 719.35 0.28 -6.68E+00 1.32E+01 778.90 12.96 1.68E-02 2.78E-01 810.45 0.32 -2.70E+00 1.24E+01 867.37 4.26 -7.24E-01 8.87E-01 919.33 0.43 -9.65E+00 9.93E+00 964.08 14.65 9.47E-02 4.46E-01 1085.87 10.24 -3.19E-01 4.06E-01 1089.74 1.73 -4.05E-01 2.81E+00 1112.07 13.69 -1.20E-01 4.05E-01 1212.95 1.43 -1.59E+00 4.32E+00 1249.94 0.19 -1.36E+01 3.11E+01 1299.14 1.63 1.09E+00 3.05E+00 1408.01 21.07 -1.18E-01 1.76E-01 1457.64 0.50 1.33E+02 4.02E+01 1528.10 0.28 1.63E+00 1.48E+01 Eu-154 123.07 40.40 1.60E-02 8.19E-02 8.19E-02 247.93 6.89 -2.50E-01 4.20E-01 591.76 4.95 -6.01E-01 6.35E-01 692.42 1.78 -1.64E+00 2.01E+00 723.30 20.06 1.18E-01 2.27E-01 756.80 4.52 -6.67E-01 7.83E-01
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| [391]
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| 7/31/2019 10:18:43AM Page 6 of 6 Analysis Report for 31-Jul-19-10015 L1-10221C-FIGS-101SB Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA Name (pCi/grams) (pCi/grams) (pCi/grams)
| |
| (keV)
| |
| Eu-154 873.18 12.08 6.24E-02 8.19E-02 3.23E-01 996.29 10.48 1.04E-01 4.08E-01 1004.76 18.01 8.17E-02 2.51E-01 1274.43 34.80 -1.87E-01 1.10E-01 1596.48 1.80 6.10E-02 2.14E+00 Eu-155 45.30 1.31 -4.78E+00 1.76E-01 9.61E+00 60.01 1.22 -2.15E+00 1.06E+01 86.55 30.70 -3.41E-03 1.76E-01 105.31 21.10 1.29E-01 1.91E-01 Ra-226 186.21 3.64 -5.67E-01 8.66E-01 8.66E-01 Pa-231 27.36 10.30 6.64E-01 1.20E+00 1.20E+00 283.69 1.70 3.73E-01 1.96E+00 300.07 2.47 -1.56E+00 1.48E+00 302.65 2.20 3.86E-01 1.62E+00 330.06 1.40 4.25E-01 2.46E+00 U-235 143.76 10.96 1.10E-01 5.63E-02 2.94E-01 163.33 5.08 6.09E-02 5.74E-01 185.71 57.20 -1.38E-02 5.63E-02 202.11 1.08 1.28E-01 2.84E+00 205.31 5.01 -4.31E-01 6.14E-01 Am-241 59.54 35.90 -9.68E-02 3.66E-01 3.66E-01
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| + = Nuclide identified during the nuclide identification
| |
| * = Energy line found in the spectrum
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| > = MDA value not calculated
| |
| @ = Half-life too short to be able to perform the decay correction
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| ? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
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| [392]
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| | |
| ATTACHMENT 8 EBERLINE ANALYTICAL REPORTS
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| [393]
| |
| | |
| EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 ANALYTICAL PHONE (865) 481-0683 FAX (865) 483-4621 EBS-OR-46230 October 22, 2019 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099
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| * CASE NARRATIVE Work Order# 19-09001-0R SAMPLE RECEIPT This work order contains sixteen soil samples received 09/03/2019. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.
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| CLIENT ID LABID CLIENT ID LAB ID Ll-1022 lA-FSGS-004-SS-A 19-09001-04 Ll-10221A-FIGS-003-SS-A 19-09001-12 Ll-1022 lA-FSGS-002-SS-A 19-09001-05 Ll-1022 lA-FIGS-004-SS-A 19-09001-13 Ll-10221 C-FSGS-012-SS-A 19-09001-06 Ll-10220I-FJGS-005-SS-A 19-09001-14 Ll-10221C-FSGS-013-SS-A 19-09001-07 Ll-10220I-QJGS-005-SS-A 19-09001-15 Ll-10221 C-FSGS-014-SS-A 19-09001-08 L 1-1022 lA-FIGS-003-SB-A 19-09001-16 Ll-1022 lA-FIGS-001-SS-A 19-09001-09 Ll-1022 lA-FIGS-001-SB-A 19-09001-1 7 L 1-1022 lA-QIGS-OO 1-SS-A 19-09001-10 L 1-10221 A-FIGS-004-SB-A 19-09001-18 L 1-1022 lA-FIGS-002-SS-A 19-09001-11 L 1-1022 lA-FIGS-002-SB-A 19-09001-19 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.
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| Gamma Spectroscopy was performed using EPA Method 901.1 Modified; Laboratory qualifiers are as follows:
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| U - Result is less than the MDA.
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| ANALYTICAL RESULTS Combined Standard Uncertainty is reported at I-sigma value.
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| Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
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| Page 1 of 3
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| ANALYTICAL RES UL TS CONTINUED TOTAL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filters were reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.
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| Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.
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| TRITIUM A representative aliquot of each sample was equilibrated with tritium free water. Equilibrates were transferred into a round-bottomed distillation flask and attached to a single stage still. A portion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.
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| Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.
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| Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.
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| NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion.
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| Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.
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| Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.
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| GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.
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| Page 2 of 3
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| ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Cobalt-60, Cesium-137 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.
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| CERTIFICATION OF ACCURACY I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data c::_**~~'.'.'.'.'.'
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| contained in this hard copy data package has been authorized by the cognizant project manager or his/her to be accurate as verified by the following signature.
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| l '\__ ~
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| M.RcMctlou:> .
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| Laboratory Manager Date: 10/22/2019 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.
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| Page 3 of 3
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| | |
| Printed: 101211201911:34AM Page 1 of 21 Report To: Work Order Details:
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| Patricia Giza 19-09001 Eberline Analytical Zion Solutions
| |
| * ,*m**,~*-, *------**w**
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| Purchase Order:
| |
| SDG:
| |
| 677118
| |
| ***- - - - * - - - - " " - - - - - - - - - - - ~ * - "'""'-''-""'''*-A~ __,,
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| Final Report of Analysis 2701 Deborah Ave Analysis Category: ... ....... E.=_N..Y:~RONflll_E:~TAL:... ________ .
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| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09001-01 LCS KNOWN 09/04/19 00:00 9/3/2019 9/24/2019 19-09001 Tritium LANL ER-210 Modified 2.04E+02 7.34E+OO 19-09001-01 LCS SPIKE 09/04/19 00:00 9/3/2019 9/24/2019 19-09001 Tritium LANL ER-210 Modified 2.03E+02 7.79E+OO 1.38E+01 5-70E+OO 19-09001-02 MBL BLANK 09/04/19 00:00 9/3/2019 9/24/2019 19-09001 Tritium LANL ER-210 Modified 4.61E+OO 3.45E+OO 3.46E+OO 5.69E+OO
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| .....-------------------------, --- 06/06/1912:20 9/3/2019 9/24/2019 19-09001 Tritium . LANL ER~--21*orc,~difi~d 19-09001-03 DUP L 1-10221A-FSGS-004-SS-A I <
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| * 1.49E+OO 3.25E+OO 3-25E+OO 5.54E+OO 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/24/2019 19-09001 Tritium LANL ER-210 Modified 3-14E+OO 3.27E+OO 3.28E+OO 5.48E+OO
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| *-* -*-*--~,--,,--~-
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| 19-09001-05 TRG L1-10221A-FSGS-002-SS-A 06/06/19 12:10 9/3/2019 9/24/2019 19-09001 Tritium LANL ER-210 Modified -7.35E-01 3-11E+OO 3-11E+OO 5.45E+OO 19-09001-06 TRG L 1-10221 C-FSGS-012-SS-A 06/11/19 09:10 9/24/2019 19-09001 Tritium LANL ER-210 Modified 1.46E+OO 3-17E+OO 3.17E+OO 5.41E+OO 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/24/2019 Tritium LANL ER-210 Modified -1.14E+OO 3.20E+OO 3.20E+OO 5.62E+OO 19-09001-08 TRG L 1-10221C-FSGS-014-SS-A 06/11/19 09:20 9/24/2019 Tritium LANL ER-210 Modified -9.46E-01 3.20E+OO 3.20E+OO 5.61E+OO 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11/1912:15 Tritium LANL ER-210 Modified 1.09E+OO 3.13E+OO 3.13E+OO 5.37E+OO 19-09001-10 : TRG L1-10221A-QIGS-001-SS-A 06/11/19 12:15 Tritium LANL ER-210 Modified 3.29E+OO
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| -------------------------------+---------------i---------------------'-----"-------------------------------1------------------'-------,------------'----'--.:...:::.=-.__,_;_::..:..;:__:_:_ ____---'5.49E+OO
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| -___;_:::__:__:_ ___::____.____'.:..:.:.:::._-1 19-09001-11 TRG L 1-10221A-FIGS-002-SS-A 06/11/19 12:17 Tritium LANL ER-210 Modified 3.28E+OO 5.54E+OO
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| -*-*-'"-'""*--~-,-~,a_, _____ ,_, __ _. '"'"'"""--,----*---
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| 19-09001-12 TRG L1-10221A-FIGS-003-SS-A 06/11/19 12:19 Tritium LANL ER-210 Modified 3.05E+OO 5.37E+OO 19-09001-13 TRG L1-10221A-FIGS-004-SS-A 06/11/19 12:21 3.16E+OO 5.50E+OO 07/09/19 -210 Modified 3.09E+OO 5.45E+OO 07/09/19 08:30 3.07E+OO 5.30E+OO LANL ER-210 Modified 3.16E+OO 5.47E+OO LANL ER-210 Modified 3.20E+OO 5.43E+OO Tritium LANL ER-210 Modified 3-19E+OO 5.40E+OO u pCi/g 19-09001-19 TRG Tritium LANL ER-210 Modified 3.26E+OO 3.26E+OO 5.53E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
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| ( ~
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| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 2 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG.
| |
| 677118 Final Report of Analysis 2701 Deborah Ave ..... Analysis Category: . ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method MDA Qualifier ID Type ID Date Date Date ID Units 19-09001-01 LCS KNOWN 09/04/19 00:00 9/3/2019 9/23/2019 ASTM 3500-Ni Modified 19-09001-01
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| --,-.,., LCS SPIKE 09/04/19 00:00
| |
| ,_,_,_____,__,---*~* ---- -w*--*-------"*--*-----*- 9/3/2019 9/23/2019 ASTM 3500-Ni Modified 3.45E+OO 19-09001-02 MBL BLANK 09/04/19 00:00 9/3/2019 9/23/2019 Nickel-63 ASTM 3500-Ni Modified 3.53E+OO u
| |
| ......!~:09-0~.1.:.°-~--- -~~---L_1:.1..~~-2.:_A-_FSG~?_04_-S_S:_I\___. 06/06/19 12:20 , 9/312_0_1_9__9_12_312019 .19-:0_9~?_1 _ --~ckel~---_....__A__ ST_M_3_5_o_o__-_N
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| ____i __M_o___d_ifi_e__d******** ___1_.9_8E
| |
| __+o_1___ ,_____2 2.95E+OO
| |
| ___._7_1E_+_o_o*-*-**--*-**---* * *3.76E+OO 1
| |
| 19-09001-04 DO L1-10221A-FSGS-004-SS-A 06/06/1912:20 : 9/3/2019 9/23/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 2.69E+OO 2.92E+OO 3.75E+OO
| |
| /-** *-----*******-****-----***--*-*-------*-******------*******---***-+** .. ***-------+-*--*-**-*-------*********---**-**---'--------*--*--*-*-
| |
| 19-09001-05 TRG L1-10221A-FSGS-002-SS-A 06/06/1912:10 9/23/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.73E+OO u
| |
| **---"-'' "<rn"_ _ _ .......,.__, *--*--*-----
| |
| 19-09001-06 TRG L1-10221C-FSGS-012-SS-A 06/11/19 09:10 9/23/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.54E+OO u 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/23/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.61E+OO u
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| ********-***--***----*----***********--- ***----*---**------***--l-********--------+-*-*--------------******-*******-------*-***-1--**---------******--+-------*--=****------+**-**-*-****------
| |
| 19-09001-08 TRG L1-10221C-FSGS-014-SS-A 06/11/19 09:20 9/23/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.58E+OO
| |
| -*--*---*-- ****-***-*******-***------------------ t*******-------+-------~----.,.----*-*-**** ---t-*--------***+******--------;--------,-----*--
| |
| 19-09001-09 TRG L1-10221A-FIGS-001-SS-A 06/11/1912:15 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.62E+OO 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.60E+OO
| |
| -----*-*-**--*--------------*------------J---**************----j---------****-------***'* ****-1------*----*-----'-**-*******-----------*-------+---*--*-*-***--
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.71E+OO u
| |
| *--*--*-----------*+----*-***---**--**+----~---*-*------******-******-*----,-----*---*-****--+---*--*---------+*****-**---...;-------------***---
| |
| 19-09001-12 TRG L1-10221A-FIGS-003-SS-A 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.54E+OO pCi/g
| |
| ***--------- -------- -***t*---------*----*---~----**-*---**---***--**r*-------**1--..*-------*--***--*-------;---------,-----***--0-----------
| |
| 19-09001-13 TRG L1-10221A-FIGS-004-SS-A 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.57E+OO pCi/g 19-09001-14 L1-102201-FJGS-005-SS-A 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 3.81E+OO u 19-09001-15 TRG L1-10220I-QJGS-005-SS-A 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified u 19-09001-16 TRG 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified u pCi/g 19-09001-17 TRG 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified u
| |
| ------------'"*=-"-*-----------------1------*---**--+-*---*----f-----*-*------------------------
| |
| 19-09001-18 TRG 06/26/19 10: 9/24/2019 19-09001 i Nickel-63 ASTM 3500-Ni Modified 3.60E+OO u pCi/g
| |
| ------;-----,..--------*---"""r-~---------+---------*---~--------+-------c-------*------------
| |
| 19-09001-19 TRG 06/26/1910:02 9/3/2019 9/24/2019 19-09001 Nickel-63 ASTM 3500-Ni Modified 2.11E+OO 3.60E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma};MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( "'M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/201911:34 AM Page 3 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical **-**-*.,***-***-- ...
| |
| Zion Solutions SDG:
| |
| ****A*---*~-*--=--*--- -A- _V,___,,
| |
| Final Report of Analysis 2701 Deborah Ave Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report ID Date Date Analyte Method Result cu CSU MDA Qualifier ID Type Date ID Units 19-09001-01 LCS 09/04/19 00:00 9/3/2019 9/24/2019 19-09001 Strontium-90 EIChroM SRW01 Modified 5.09E+01 2 _ 85E-01
| |
| -*------**** *-**-*--*----~--- ---- --* .. ----;----*--------,----------
| |
| 19-09001-01 09/04119 00:00 9/3/2019 9/24/2019 19-09001 Strontium-90 EIChroM SRW01 Modified 5-D1E+01 U9E+OO U5E+01 7 _ 94E-01 19-09001-02 MBL BLANK 09/04/19 00:00 9/3/2019 9/24/2019 19-09001 Strontium-90 EIChroM SRW01 Modified -2,75E-02 3.49E-01 3.49E-01 7.48E-01 u 19-09001-03 DUP L 1-10221A-FSGS-004-SS-A 06/06/1912:20 . 9/3/2019 9/24/2019 09001 - ----i-****-*--* 4.18E-02 3 _ 33E-01 3 _ 33E-01 u pCi/g 19-09001-04 DO L 1-10221 A-FSGS-004-SS-A 06/06/19 12:20 19-09001 3 _ 72E-01 3--73E-01 7 _ 97E-01 u 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A 3.60E-01 3.62E-01 7.79E-01 u 19-09001-06 TRG L 1-10221 C-FSGS-012-SS-A 3.71E-01 3.73E-01 7.SOE-01 u 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 2.71E-01 2.87E-01 5.48E-01 u 19-09001-08 TRG L 1-10221 C-FSGS-014-SS-A 3.72E-01 3.73E-01 7.86E-01 u 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11/19 12:15 3.45E-01 3.SOE-01 7.55E-01 u 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 3.40E-01 3.51E-01 7.00E-01 19-09001-11 TRG L 1-10221A-FIGS-002-SS-A 3.18E-01 3.27E-01 6.56E-01 u 19-09001-12 TRG L 1-10221A-FIGS-003-SS-A 06/11/19 12:19 3.34E-01 3.69E-01 6.65E-01 u 19-09001-13 TRG L 1-10221A-FIGS-004-SS-A 06/11/19 12:21 3.33E-01 3.59E-01 6.67E-01 u L1-102201-FJGS-005-SS-A 3.SSE-01 3.96E-01 8.0SE-01 u TRG L1-10220!-QJGS-005-SS-A 4.36E-01 4.38E-01 9.43E-01 u TRG L 1-10221A-FIGS-003-SB-A 3.29E-01 3.29E-01 7.13E-01 u L 1-10221A-FIGS-001-SB-A 3.87E-01 4.44E-01 8.SSE-01 u 3.14E-01 3.19E-01 6.52E-01 u 3.57E-01 7.37E-01 u EPA 901.1 Modified EPA 901.1 Modified EPA SPIKE EPA901.1 Modified CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( '"MJ EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 4 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118
| |
| """"'~- --- "-------''"'""- *----~--------*-
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report JO Date Date Date JO Analyte Method Result cu CSU MOA Qualifier 10 Type Units 19-09001-02 MBL BLANK 09/04/19 00:00 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 6.98E-02 7.46E-02 7.47E-02 19-09001-02 MBL BLANK 09/04/19 00:00 9/3/2019 9/10/2019 19-09001 Silver-108m EPA 901.1 Modified 1.64E-03 3.23E-02 3.23E-02 u pCi/g
| |
| """' '" *-*-----¥-*---- """-----*,.,,-,.-----~ "--------,----*''"
| |
| 19-09001-02 MBL BLANK 19-09001 Americium-241 EPA 901.1 Modified 5.81E-03 4.03E-02 4.03E-02 6.08E-02 19-09001-02 MBL BLANK
| |
| ***--***--******-***-*****--J**--********---****** **<***---*-*-**------~--------*-***-
| |
| 19-09001 Barium-133
| |
| +****----***-*****------*-*-**-*-*--- ""*********-****-*--*-*****--
| |
| EPA 901.1 Modified 2.87E-02 4.84E-02 4.84E-02 6.11E-02
| |
| ----~*----------,,,*--**---------*-*---+**--********** *-*----*******-**--*-------**-****-**-"********* .,,_,,_,__ ---* '""" ***,.*--**---********----
| |
| 19-09001-02 19-09001 Bismuth-214 EPA 901.1 Modified 7.51E-02 7.51E-02 1.19E-01 19-09001-02 19-09001 Cobalt-60 EPA 901.1 Modified 3.11E-02 3.11E-02 4.87E-02 19-09001-02 MBL BLANK 19-09001 Cesium-134 EPA901.1Modified 4.14E-02 4.95E-02
| |
| *-*--*--------*-"-*---- *-.-*-------------*----*----------+--*----*--*-**-*-+******----,-------***-----*-*-** *******----****+*-***---------*---,...,....,.____..,..... *****--*---+-----*-****-*****-**
| |
| 19-09001-02 MBL BLANK 19-09001 Cesium-137 3.33E-02 3.34E-02 5.34E-02 1--------****-****-----*********--*-----**********---*--------+-*--*---*--***--*--------------*******-**-***-**** **********-*----*-******,***-****------*-***-**---*-***---------******
| |
| MBL BLANK 19-09001 7 .08E-02 9.03E-02 9.04E-02 1.04E-01 19-09001-02 MBL BLANK 19-09001 -6.27E-03 9.34E-02 9.34E-02 5.22E-02
| |
| ---~***---*-*--*---~------~--------*---*----,,,,--t--***************--**"*~--------***----*--*---********-******-----*-****1***-**------**-***-**--*------*-*---**-***--*--~--****----
| |
| 19-09001-02 MBL BLANK 19-09001 EPA 901.1 Modified -2.87E-02 4.89E-02 4.89E-02 6.67E-02
| |
| - ' -"""_____,_"________,________ ----+--------***********--------**-------------**--~*******-***---*-*---------------**********-+**----***--***----*-***~,---------
| |
| 19-09001-02 MBL BLANK 19-09001 Holmium-166m EPA901.1 6.76E-02 6.76E-02 3.71E-02
| |
| ------,------------------"-------------------------------------*-------------+-*--------*-~-------,.---**---..-----,----*-**--****--+----*-*-*--*---l ***--*-*----e---------------
| |
| 19-09001-02 MBL BLANK 19-09001 lodine-129 EPA 901.1 3.51E-02 3.51E-02 5.03E-02
| |
| ---*~-----*------------------------,---t---*------,.----**-----*---------********-- -------------+---*-*------*--***------------------------
| |
| 19-09001-02 MBL BLANK 19-09001 EPA 901.1 Modified 3.04E-01 3.04E-01 6.49E-01
| |
| -~------------------+-------------------i---------r--*---***-'-**-----l--*-*****-***--**----*****----i------**-------*****-*--------
| |
| 19-09001-02 , MBL BLANK 19-09001 3.81E-02 3.81E-02 5.57E-02
| |
| ***---------**--*******--******-*----*-**---**---+**---*****-*******-f--****-......O---....;.-------'----:C... -...----1--*--****--*---*-,--*----***.--*-----**------
| |
| 3.43E-02 4.38E-02 2.94E-02 4.81E-02 3.34E-01 5.65E-01 4.17E-02 6.94E-02 8.81E-02 1.42E-01 7.51E-02 7.51E-02 8.58E-02 8.58E-02 3.76E-01 3.77E-01 EPA 901.1 Modified 1.01E-01 1.01E-01 EPA901.1 Modified 1.33E-01 1.33E-01 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control SampJe;MBL=BJank;OUP=Ouplicate;TRG=Normal Sample;OO=Ouplicate OriginaJ;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 5 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical ____
| |
| Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| --,~-----*--
| |
| Final Report of Analysis 2701 Deborah Ave
| |
| *-------- .Analysis.Category: . ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19*09001-03 DUP L1-10221 A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA901.1 Modiiied 5.98E-01 3 05E-01 3.07E-01 5.39E-01
| |
| "-" ,----~------------ ----- --- ,,,-,,- ---~-****- " ' - * - - * - * - - - - - - - . - - , , w_rn_,, ___ _,'
| |
| 19*09001-03 DUP L1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Silver-108m EPA 901.1 Modiiied -4.26E-02 8.25E-02 8.25E-02 1.05E-01 19-09001-03 DUP L1-10221 A-FSGS-004-SS-A ~~!°.~_9_12_:_2-D___ 9/3/2019 9/1.".0_D..1.?.... 19-090D_1_ ,.*.. Americium-241 EPA 901.1 Modified 1.06E-01 1.59E-01 1.59E-01 2.11E-01 19-09001-03 DUP L1-10221A-FSGS-004-SS-A 06/06/1912:20 9/3/2019 9/10/2019 19-09001 Barium-133 EPA901.1 Modiiied 6.50E-02 7.66E-02 7.67E-02 1.56E-01
| |
| ---------"*----*--*, *--*-------"-------------~-----*----- ................... ---*---------------------~-----
| |
| 19-09001-03 DUP L1-10221A-FSGS-004-SS-A 06/06/1912:20 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA 901.1 Modiiied 5.50E-01 2.16E-01 2.18E-01 3.26E-01
| |
| .................................................... - ..---*-****------- **---*-**--*----**'------***------------~---*-- -------***----
| |
| 19*09001*03 DUP l1*10221A-FSGS-004*SS-A 06/06/1912:20 9/10/2019 19-09001 Cobalt-60 EPA 901.1 Modified 2.52E+OO 2.37E-01 2.70E-01 1.87E-01
| |
| *-*-----*-*"wmw,"',*** "" "" _ _ _ _ _ ,_, __, , _ , _ , , ~ ~ - - - - * - * " ' " ' " " '_ _ _ , *-**-*+**----*-*-*--*-,.,"*****--****-**-*--,**-----**-**-------
| |
| 19-09001-03 DUP L1-10221A-FSGS-004-SS-A 06/06/1912:20 19-09001 Cesium-134 4.81E-02 4.81E-02 9.53E-02
| |
| ---------*------------*---------*-----------*---t****-*-----** ..----------*+----..C....--...............,_ ------*+****-----------------------------------------*----*---**---,------*
| |
| 06/06/19 12:20 1.01E+OO 1.89E-01 3.05E-01 2.90E-01 19-09001-03 DUP L1-10221A-FSGS-004-SS-A EPA901.1 Modilied 1.09E-01 1.49E-01
| |
| -----~ ' -'-"" -
| |
| 19-09001-03 DUP L1-10221A-FSGS-004-SS-A EPA901.1 Modiiied 19-09001-03 DUP L1-10221A-FSGS-004-SS-A EPA 901.1 Modified
| |
| *------------------------------+-*---------***+------------~'-----r---*--;...-,_*-------1--c-c-~--*--------'-*-***----*--,---*--**c:--..,.-----------------'------.:.........:::.._-f 19-09001-03 L1-10221A-FSGS-004-SS-A 06/06/1912:20 lodine-129 EPA901.1 Modified
| |
| --*--------+*-----------0----...,--------------------+-------------+*
| |
| L1-10221 A-FSGS-004-SS-A 06/06/19 12:20 Potassium-40 EPA 901.1 Modiiied 1.04E+OO
| |
| "----~ t"----------*+ ... -*-*------***------------;-----*--**--*----,--------------*---*-----......;
| |
| *------------*---**-**--------------L_1-__10_2_2_1_A-_F_S_G_s_-0_04- __s_s_-A _______-t-_o~o_611~_2:2_0--9_13_12_0_1_9-r-_9_11012019 1.28E-01 19-0900_1___ Manganese-54-i--*-*-E_P_____A___9_0__1_.1_M_o_d_ifi_,e_d____-+-----------~-------------------------*------------*------*--*--t L1-10221A-FSGS-004-SS-A 06/06/19 12:20 i 9/3/2019 9/10/2019~ 19-09001 __ Molybdenum-93+---------------+------,-------~-------------------------------i 4.87E-02 DUP L1-10221A-FSGS-004-SS-A 06/06/19 12:20 ! 9/3/2019 9/10/2019
| |
| * 19-09001 Niobium-94 9.88E-02 1--------**-+--------*-*------*-------------;--0-6-/06/... 19_1_2_:2_0___ -l_9_/3_/2_0_1_9......._9_/1-0-/2-0-19-.-19-09001 Lead-2_1_0-+--::E,-::P*A,*-:9*co:-1.""1-----+----:c-*:---:***-'--:--:*=-:-::--i--*---:--:-:-::=-:c-*~-:-:---*-,--.:...*...:::.._;
| |
| DUP L1-10221A-FSGS-004-SS-A 2.87E+OO
| |
| --+---=---------***---*----*------+----------------!-------*-+*---*-----+--*--*-~----'----*--"-;;;__*------1 DUP L1-10221A-FSGS-004-SS-A 1----------,'------*---'***--------------------*------+--06_1_06_119 12:20 i 9131201_9-+_9_11_0_,2_0_1_9-+-_19-?_9_00_1 ____L..:~~:_21_2__ t------------,**-*--- 3.27E-01 DUP L1-10221A-FSGS-004-SS-A 06106119 12:20 -r-9/3/2019 9/10/2019 19-09001 Lead-214 3.49E-01 pCi/g
| |
| *------------+- ----+----,-
| |
| DUP L1-10221A-FSGS-004-SS-A 1----------'-*-----c-*-----*---------------+--06/06/19 12:20 I 9/3/2019 9/10/2019 19-09001 u pCi/g DUP L1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Radium-226 3.26E-01 pCi/g DUP L1-10221A-FSGS-004-SS-A 3.69E-01 u 19-09001-03 DUP L1-10221A-FSGS-004-SS-A 1.40E+OO 1.78E+OO u pCi/g 19-09001-03 DUP L1-10221A-FSGS-004-SS-A 1.01E-01 1.11E-01 pCi/g 19-09001-03 DUP L1-10221A-FSGS-004-SS-A 4.58E-01 6.15E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 1012112019 11 :34 AM Page 6 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah
| |
| -"'""'" _______ ,,._"'Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/312019 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 5.30E-01 2.49E-01 2.50E-01 4.55E-01 pCi/g
| |
| *-*---*----------A,__ " ' " " " " .---'<=~-"''""'m'"'=" - " ' " ' " m - - = _ , , _ , , _ , __ ,_
| |
| 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019
| |
| -*------------""'"<"''---------*-*---~~--- "'
| |
| 9/10/2019 19-09001 Silver-108m EPA 901.1 Modified -1.09E-02 4.03E-02 4.03E-02 9.41E-02 19-09001-04 DO L 1-10221 A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019
| |
| ---*-------~-- . .,,,_,,___-<*---------"*--,------
| |
| 19-09001 Americium-241 EPA901.1 Modified -1.62E-01 1.69E-01 1.69E-01 2.04E-01 u pCi/g 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Barium-133 EPA 901.1 Modified -1.66E-02 5.22E-02 5.22E-02 1.41E-01 u
| |
| -*----......;-----*--- ------------***-----*---*------- **-*----------* -----~----- m,~,-~-*--**-n, 19-09001-04 DO L1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA901.1 Modified 5.07E-01 1.76E-01 1.78E-01 3.28E-01 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 2.52E+OO 2.36E-01 2.69E-01 1.82E-01
| |
| ,~---~------ *---~- ------*--*--------- . ----------*
| |
| 19-09001-04 DO L 1-10221 A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Cesium-134 EPA 901.1 Modified -5.53E-02 6.12E-02 6.12E-02 8.97E-02 u
| |
| ---*- -*--*------,,.*--..- - ~....-*---*--*---*
| |
| 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 Cesium-137 EPA 901.1 Modified 8.24E+OO 9.40E-01 1.03E+OO 1.81E-01
| |
| -----*----.. .~-----¥*------------- -------'"'" ___
| |
| 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified -6.65E-02 3.09E-01 3.09E-01 2.83E-01 u 19-09001-04 DO L 1-10221A-FSGS-004-SS-A
| |
| . -~----*,=*-----..--
| |
| 06/06/19 12:20 ,__,._,. 9/3/2019 , 9/10/2019 19-09001 ,_/_, _______ , ______
| |
| Europium-154 EPA 901.1 Modified 3.88E-04 1.68E-01 1.68E-01 1.44E-01 u 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20
| |
| ---*------~¥ 9/3/2019 9/10/2019 19-09001 Europium-155 EPA 901.1 Modified 1.19E-01 1.43E-01 1.43E-01 1.89E-01 u
| |
| --*------ , ....---*--..-------------*-*--*------* "-------~---
| |
| 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/10/2019 19-09001 Holmium-166m EPA 901.1 Modified 1.06E-01 1.06E-01 1.11E-01 u 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/10/2019 19-09001 lodine-129 EPA 901.1 Modified 2.01E+01 4.16E+OO u 19-09001-04 DO L 1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/10/2019 19-09001 Potassium-40 EPA 901.1 Modified 1.25E+01 1.86E+OO 1.97E+OO 8.55E-01 19-09001-04 DO L1-10221A-FSGS-004-SS-A 06/06/19 12:20 9/1012019 19-09001 Manganese-54 EPA901.1 Modified 9.08E-02 1.29E-01 u 19-09001-04 DO Molybdenum-93 5.98E-02 8.88E-02 u 19-09001-04 DO Niobium-94 7.72E-02 8.53E-02 u 19-09001-04 DO Lead-210 2.38E+OO 3.93E+OO u 19-09001-04 DO Lead-212 1.59E-01 3.61E-01 19-09001-04 DO Lead-214 2.12E-01 2.14E-01 3.77E-01 19-09001-04 DO 1.16E+OO 19-09001-04 DO EPA 901.1 Modified 1.76E-01 1.78E-01 3.28E-01 19-09001-04 f DO _..______________ EPA901.1 Modified 1.16E-01 2.23E-01 2.23E-01 3.75E-01 u 19-09001-04 DO L1-10221A-FSGS-004-SS-A EPA901.1 Modified 5.20E-01 1.44E+OO u 19-09001-04 DO L 1-10221A-FSGS-004-SS-A Thallium-208 1.05E-01 19-09001-04 DO L1-10221A-FSGS-004-SS-A 06/06/19 12:20 Uranium-235 5.13E-01 5.13E-01 6.22E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/2019 11 :34 AM Page 7 of 21 Report To: Work Order'Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave ...... Ana/ysisCategory: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier ID Units 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A 06/06/19 12:10 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 5.67E-01 2.19E-01 2.21E-01 4.71E-01 pCi/g 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A 06/06/19 12:10 9/3/2019 9/10/2019 19-09001 Silver-108m 6.34E-02 6.35E-02 1.09E-01 U pCi/g
| |
| --- ****-------------------------------------- -*-* *****-----* ,,,._ ,----,~----- ---
| |
| 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A 06/06/19 12:10 9/10/2019 19-09001 Americium-241 8.94E-02 8.95E-02 1.24E-01 U pCi/g
| |
| ,--*-------"-------*--, ..j--- * - * * * - * - * - - * - - - - - - - , - - - - - - - - - - - - * - * ....._. . . . . . . . . , - * - - - v*ce-*----""
| |
| 19-09001-05 TRG L1-10221A-FSGS-002-SS-A 9/10/2019 19-09001 Balium-133 EPA 901.1 Modified 1.18E-01 1.18E-01 1.32E-01 U 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A 19-09001 Bismuth-214 EPA 901.1 Modified 4.88E-01 1.62E-01 1.64E-01 2.50E-01 pCi/g
| |
| .. *-* -- ---------------------*-****----*---**-* - ---------------------*---t-----------------***---*----*-- -------------0-------------1-----------*----------------------
| |
| 19-09001-05 TRG L1-10221A-FSGS-002-SS-A 19-09001 Cobalt-60 EPA901.1 Modified 5.12E-01 1.07E-01 1.10E-01 1.41E-01
| |
| '""""' _ _ _ _,_,v' 19-09001-05
| |
| -------------~---'"'"""'
| |
| 19-09001-05 TRG TRG L1-10221A-FSGS-002-SS-A L1-10221A-FSGS-002-SS-A 19-09001 19-09001 Cesium-134 Cesium-137 EPA 901.1 Modified EPA901.1 Modified 4.37E-02 2.27E-01 4.37E-02 2.45E-01 1.18E-01 1.50E-01 u
| |
| , __ , _ _ _ "'"'"-""'"<""- os* , - - - - - - - " ' ' " " " ' _ _ _ _ _ _ , _ , _ _ _ **---***--*****-*-**--***--******--*****---.*--*--***'---*--***
| |
| ----------*---~------**------------***---------~---
| |
| 19-09001-05 TRG L1-10221A-FSGS-002-SS-A 19-09001 EPA901.1 Modified 1.29E-01 1.29E-01 2.29E-01 U 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 2.65E-01 1.10E-01 U 19-09001-05 TRG , L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 1.01 E-01 1.63E-01 U
| |
| ----------------------------------------- ------1----------------i--------,-----------****-------------------------11---------------* --,----------------*--------,--------------------------------------1 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 1.07E-01 8.25E-02 U
| |
| ------------*-*-----****----- ----*-----t-------------~c-----;-----*----*------*--*----*"-------1--*-*--*----**--*-*----********-*--*-------+-------;-----------------------*---------*--*----------1 19-09001-05 TRG L1-10221A-FSGS-002-SS-A EPA 901.1 Modified 2.30E-01 3.28E-01 U 19-09001-05 TRG L1-10221A-FSGS-002-SS-A pCi/g
| |
| -----~---'-'-"
| |
| 19-09001-05 TRG L1-10221A-FSGS-002-SS-A EPA901.1 Modified 7.70E-02 1.18E-01 U 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 5.42E-02 9.43E-02 U pCi/g 0
| |
| ~=--------*-*-----------1-----------*-+-----+-----*-*---*--*---------*---1--**-***--**-----*---*4*--*--*--******----+-------------*--------t 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 6.09E-02 9.36E-02 U
| |
| ,__19-09001-05 TRG L 1-10221A-FSGS-002-SS-A pCi/g 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 1.24E-01 2.85E-01 19-09001-05 TRG L 1-10221A-FSGS-002-SS-A EPA 901.1 Modified 3.29E-01 TRG L 1-10221A-FSGS-002-SS-A u pCiig 19-09001-05 TRG L1-10221A-FSGS-002-SS-A EPA 901.1 Modified 2.50E-01 pCi/g 19-09001-05 TRG L1-10221A-FSGS-002-SS-A 06/06/19 12:10 EPA 901.1 Modified 3.38E-01 u u
| |
| CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 8 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave
| |
| *-,---*----~--- Analysis_ Category: *- ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Date Date Analyte Method Result cu CSU MDA Qualifier ID Type ID Date ID Units 19-09001-06 TRG L1-10221C-FSGS-012-SS-A 06/11/19 09:10 9/3/2019 9/10/2019 19-09001 2.70E-01 5.24E-01 u 19-09001-06 TRG L1-10221C-FSGS-012-SS-A _ 06/1_1/19 0910 .. 9~2~_9 9/10/2019 19-09001 7.64E-02 9.64E-02 u 19-09001-06 TRG L1-10221C-FSGS-012-SS-A 06/11119 09:10 9/3/2019 9/10/2019 19-09001 1.10E-01 1.10E-01 1.58E-01 u 19-09001-06 TRG L1-10221C-FSGS-012-SS-A 06/11/19 09:10 9/3/2019 9/10/2019 19-09001 Barium-133 EPA 901.1 Modified 1.23E-01 1.24E-01 1.86E-01 u TRG L1-10221 C-FSGS-012-SS-A 06/11/19 09:10 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA 901.1 Modified 1.47E-01 1.51E-01 5.11E-01 TRG L1-10221C-FSGS-012-SS-A --~~~19 09: 10 : 9/3/20~ _ 9/10/2019 ---~-09001 _ EPA 901.1 Modified ..__,,*.....*.**.---*----*,*---------*-
| |
| J~alt-6_°. _____1____________________ 1.07E-01 ___1__ 1.34E-01 u
| |
| .0_7_E-_0_1 -------*--------*-**---*-*-----------*--t TRG L1-10221 ________________
| |
| '""""" C-FSGS-012-SS-A
| |
| . 9/3/2019
| |
| -,--*---------*--*--+---**
| |
| 9/10/2019 19-09001 EPA 901.1 Modified 1.38E-01 1.39E-01 1.27E-01
| |
| "'"'" -----,-----~= -+---------------------*-----*--*-------------------,---*--**"------! u TRG L1-10221 C-FSGS-012-SS-A EPA 901.1 Modified 1.04E-01 1.05E-01 1.62E-01 TRG L1-10221 C-FSGS-012-SS-A EPA 901.1 Modified 1.55E-01 1.55E-01 2.50E-01 u TRG L1-10221C-FSGS-012-SS-A EPA 901.1 Modified 2.57E-01 2.57E-01 1.29E-01 u
| |
| -***---~-----** ***------------**-**+---------+-----'*--*---*--*---*-r-----;-----------t---*--
| |
| """""'19-09001-06 TRG
| |
| """"'"'""""___________,__________ L1-10221C-FSGS-012-SS-A
| |
| "_'_"=--------------- EPA 901.1 Modified 9.18E-02 9.19E-02 1.94E-01 u 19-09001-06 TRG L1-10221C-FSGS-012-SS-A EPA 901.1 Modified 1.42E-01 1.42E-01 8.56E-02 u TRG L1-10221 C-FSGS-012-SS-A EPA 901.1 Modified 7.97E-02 1.11E-01 u 19-09001-06 TRG L1-10221C-FSGS-012-SS-A EPA 901.1 Modified 2.27E+OO 1.45E+OO 19-09001-06 TRG L1-10221C-FSGS-012-SS-A 8.72E-02 1.52E-01 u
| |
| *-****---------------------*--**--------------+-~----.;__---':---------,------,--t---=---------jl---=---.-~-:------,---,-----=***-**---:----,-~--:-*-*+*----,-~-----*----
| |
| 19-09001-06 TRG L1-10221C-FSGS-012-SS-A 8.07E-02 9.06E-02 u 19-09001-06 TRG L1-10221 C-FSGS-012-SS-A 7.27E-02 9.44E-02 u TRG L1-10221 C-FSGS-012-SS-A 8.56E-01 1.31E+OO u 19-09001-06 TRG 1.28E-01 2.20E-01 pCi/g 3.69E-01 pCilg 1.38E-01 u 5.11E-01 3.06E-01 u Thorium-234 1.50E+OO 2.49E+OO u Thallium-208 EPA901.1 Modified 1-73E-01 3.09E-01 L1-10221 C-FSGS-012-SS-A Uranium-235 EPA901.1 Modified 3.51E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/2019 11 :34 AM Page 9 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09001-07 TRG L 1-10221 C-FSGS-013-SS-A 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA 901 _1 Modified 4_84E-01 2.01E-01 4_07E-01
| |
| -----------~-
| |
| 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 Silver-108m 8.27E-02 u pCi/g
| |
| ''"'"----*----------------- °'----------,--=- --*--*-" -*---
| |
| 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 Americium-241 EPA 901 _1 Modified
| |
| ,-,--------*--*----*-----,, __ ,,,---.*-*------,- __ ,-1.28E-01 9_25E-02 9.27E-02 1.24E-01
| |
| __,_,__,__,, ___,_,_,._,,--w----------------*---*--**- U 19-09001-07 TRG
| |
| ---,----~----
| |
| L1-10221C-FSGS-013-SS-A ____ _________ --~
| |
| , 06/11/1909:15
| |
| ____________ , 9/3/2019 9/10/2019 19-09001
| |
| ""'""'=-------~------*-------,w--,w Barium-133
| |
| *A' EPA 901 _1 Modified 2_91E-02 1_17E-01 1_17E-01 1.41E-01 U 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/1909:15 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA901.1 Modified 7.43E-01 1_75E-01 1_79E-01 2_26E-01
| |
| _____L_1___1_0___2_2____1___c_____F_S_G_._s_____o._1__
| |
| 3_-S-S--A-----+---0-6_/_1._1_/_1_9__o*-9*---:15 ' 9/3/2019 . 9/10/2019 ____ - ; 9 ~ Cobalt-60 EPA 901 _1 Mo--d--ifi*-,e-d*---*---------*----------------------
| |
| 19-09001-07 TRG 1.SOE-02 9.42E-02 9.42E-02 1.55E-01 u 19-09001-0_'.._ __ TRG _____ ----~_1.:1022:~:tSGS-013-SS-A _ 06/11/19 09:15 9/3/2019
| |
| __,_,,_._ w-------'-"**--- ""' w-,-
| |
| 9/10/2019 19-09001
| |
| - - - * - :~*
| |
| Cesium-134
| |
| __ w, EPA901_1 Modified 9.24E-03 2.70E-02 2.70E-02 1_17E-01 u 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/1909:15 9/3/2019 9/10/2019 19-09001 Cesium-137 EPA901_1 Modified 1_76E-01 9_04E-02 9.09E-02 1.39E-01
| |
| ,-------------------- -------------*------------------------------*-t--- --*-***-m**-*-~ --~-,-----=**---____ ,_"\me
| |
| -------+-----------------------------r------------------------------>*---------------------*-*------'-------~---1 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 Europium-152 EPA 901_1 Modified 1_23E-01 1_97E-01 1_97E-01 1.91E-01 u 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified -1.42E-02 2_53E-01 2.53E-01 9_92E-02 u 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified 1.23E-01 1_23E-01 1.88E-01 u 19-09001-07 TRG __________________
| |
| L1-10221C-FSGS-013-SS-A " _____, 06/11/19 09:15 9/3/2019 9/10/2019 19-09001 EPA 901 _1 Modified -1_69E-02 9_63E-02 8_61E-02 u 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/10/2019 19-09001 EPA901_1 Modified 6_07E-02 2.25E-01 3_32E-01 u 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/10/2019 19-09001 EPA 901.1 Modified 2.05E+01 4_02E+OO 1_13E+OO
| |
| -----,------------------------------t-------------------~-----+--------------------+---------+-------------------f-----------,----~,--------------------:-----'---=----1 19-09001-07 . TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 9/10/2019 19-09001 EPA901_1 Modified 1_74E-02 7_27E-02 1.19E-01 u
| |
| -------------------------*--------------------+-----------------i-----c-----------<---------''-------+--------------------+-----------C---------~----------------------------------"---;;:_---1 19-09001-07 TRG L1-10221C-FSGS-013-SS-A ___,1------
| |
| 06/11/19 09:15 EPA 901.1 Modified . 9.84E-03 5.20E-02 5_20E-02 8.58E-02 u
| |
| _ _ _ _ _ _ _ _ _ 'f""' _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
| |
| ----- *------~--- - - - -
| |
| 19-09001 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 EPA 901 _1 Modified -2.00E-02 5_34E-02 5_34E-02 8_30E-02 u TRG L 1-10221C-FSGS-013-SS-A EPA 901_1 Modified 1.32E+OO 1_25E+OO 1_25E+OO 2.08E+OO u TRG L 1-10221C-FSGS-013-SS-A EPA901_1 Modified 1_16E-01 2_05E-01 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A EPA901_1 Modified 1.49E-01 2.44E-01 19-09001-07 TRG L 1-10221 C-FSGS-013-SS-A 06/11/19 09:15 19-09001 EPA 901_1 Modified 1.50E-01 2.23E-01 u 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 19-09001 EPA 901.1 Modified 1_79E-01 2.26E-01 pCi/g 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 19-09001 EPA901.1 Modified 1_93E-01 2_53E-01 u pCi/g 19-09001-07 TRG L1-10221C-FSGS-013-SS-A 06/11/19 09:15 19-09001 EPA901_1 Modified u pCi/g TRG L1-10221 C-FSGS-013-SS-A 06/11/19 09:15 19-09001 EPA 901.1 Modified 19-09001-07 TRG L 1-10221C-FSGS-013-SS-A 06/11/19 09:15 19-09001 Uranium-235 EPA 901_1 Modified u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( "'M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 101211201911:34AM Page 10 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: . ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date ID Units 19-09001-08 TRG 06/11/19 09:20 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 3.24E-01 2.23E-01 2.24E-01 3.84E-01 pCi/g 19-09001-08 TRG Si1ver-108m
| |
| ----,f---*
| |
| EPA901.1Modified 5.45E-02 5.45E-02 7.08E-02 _____
| |
| pCi/g 19-09001-08 TRG Americium-241 EPA901.1 Modified 1.10E-01 1.10E-01 1.45E-01
| |
| ----******-* ------- - - - - --* ----*--***** +*----*--*-**********---~----***--***-*---------*-*********-------*---*****---*****-+-
| |
| 19-09001-08 TRG L1-10221C-FSGS-014-SS-A 06/11/1909:20 9/3/2019 9/10/2019 19-09001 Barium-133 EPA901.1 Modified -1.81E-01 1.07E-01 1.07E-01 9.57E-02 19-09001-08 ~--T-RG*-~""i'1"~10221C-F.sG*s--0 ..SS-A 06/11/1909:20 I 9/3/2019 ' 9/10/2019 19-osoo1""~w--Bi~-u-th--2-14 EPA901.1 Modified 3.55E-01 1.08E-01 1.09E-01 1.66E-01
| |
| ***********-*--*****--*-**-*-**-------**********------**--*-***************-******-f-- -*-*-***-------t-**--*-******-******--****-------------~---***
| |
| 19-09001-08 TRG L1-10221C-FSGS-014-SS-A
| |
| ---------~-,_,__ 06/11/19 09:20 9/3/2019 9/10/2019 19-09001 Cobalt-60 EPA 901.1 Modified 5.93E-01 9.00E-02
| |
| _.,,. __ ,_ - - - * *- --,-- --~----- ,.,,, _____________ --------------~-,-
| |
| 9.50E-02 1.17E-01
| |
| . ******- pCi/g 19-09001-08 . TRG L1-10221C-FSGS-014-SS-A 06/11/1909:20 9/3/2019 9/10/2019 19-09001 Cesium-134 EPA901.1 Modified 7.28E-03 2.90E-02 2.90E-02 5.86E-02 u 9/3/2019 9/10/2019 19-09001 Cesium-137 EPA 901.1 Modified 2.29E+OO 2.83E-01 3.06E-01 1.47E-01
| |
| --------------,-----* ,--"----~'""
| |
| 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified 6.00E-02 2.23E-01 2.23E-01 2.00E-01 u 19-09001-08 TRG L1-10221C-FSGS-014-SS-A 9/3/2019 9/10/2019 EPA 901.1 Modified 7.62E-02 1.36E-01 1.36E-01 9.93E-02 u 19-09001-08 , TRG L1-10221C-FSGS-014-SS-A 9/3/2019 9/10/2019 EPA901.1 Modified 5.02E-02 5.03E-02 1.41E-01 u 19-09001-08 TRG L1-10221 C-FSGS-014-SS-A 06/11/19 09:20 9/3/2019 9/10/2019 EPA 901.1 Modified 8.25E-02 8.25E-02 7.86E-02 u
| |
| ***--*------~l---------l-----i----------*--c--***----*-----l-----------;*********-**-------*------;,.---*---*-**--------**---***------------.:....::...---1 19-09001-08 TRG L1-10221C-FSGS-014-SS-A 9/3/2019 9/10/2019 EPA901.1 Modified -1.54E+OO 7.48E+OO 7.48E+OO 3.13E+OO u
| |
| -'"""'----~----*--~--------------*----..---,--"
| |
| 19-09001-08 TRG L1-10221 C-FSGS-014-SS-A 9/3/2019 9/10/2019 1.29E+01 19-09001-08 TRG L1-10221C-FSGS-014-SS-A -2.52E-02 8.07E-02 u 1 - - - - - - + - .- - * - * - - - - - **--*
| |
| 19-09001-08 TRG L1-10221C-FSGS-014-SS-A -3.90E-03 5.93E-02 u 19-09001-08 TRG L 1-10221C-FSGS-014-SS-A 4.46E-02 4.46E-02 6.58E-02 u 19-09001-08 TRG L1-10221 C-FSGS-014-SS-A 1.73E+OO 1.73E+OO u 19-09001-08 TRG L1-10221C-FSGS-014-SS-A EPA901.1 Modified 4.83E-01 1.03E-01 3.30E-01 pCi/g 19-09001-08 TRG L1-10221C-FSGS-014-SS-A EPA901.1 Modified 6.07E-01 1.59E-01 2.75E-01 pCi/g TRG L1-10221C-FSGS-014-SS-A EPA901.1 Modified 9.65E-01 8.09E-01 9.80E-01 u
| |
| -----+*-------+-----+----*---*-------:------*-------;----------****-,*-*-----,
| |
| L1-10221C-FSGS-014-SS-A EPA 901.1 Modified 1.66E-01 u pCVg EPA 901.1 Modified u pCVg Thallium-208 EPA 901.1 Modified pCi/g Uranium-235 EPA 901.1 Modified -2.28E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 11 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Catefjory E NVI RON MENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Date Date Analyte Method Result cu CSU MDA Qualifier ID Type Date ID Units 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11/19 12:15 9/312019 9/10/2019 19-09001 Actinium-228 EPA901.1 Modified 4-77E-01 5.95E-01 5.96E-01 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 Silver-108m EPA 901-1 Modified U1E-01 U1E-01
| |
| ""' * - - - * - o w e * -------
| |
| 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11/1912:15 9/3/2019 9/10/2019 19-09001 Americium-241 1.48E-01 1.48E-01
| |
| *- ---"'~-------
| |
| 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11/19 12:15 9/312019 9/10/2019 19-09001 Barium-133 1.06E-01 1.06E-01 u
| |
| ---*-------*--*- '""" - -~---*----------- ---**-------*-*--------------*
| |
| 19-09001-09 TRG L1-10221A-FIGS-001-SS-A 06111/19 12:15 9/312019 9/10/2019 19-09001
| |
| ,w, 0 Bismuth-214
| |
| ,,-,*=------------~ mm-,
| |
| 3.07E-01 3.08E-01 4.42E-01 u 19-09001-09 TRG L 1-10221A-FIGS-001-SS-A 06/11119 12:15 9/312019 9110/2019 19-09001 Cobalt-60 4.04E-01 4.74E-01 2.52E-01
| |
| --"*-------~--*---*~*------*---~-- '"-------~----
| |
| 19-09001-09 TRG 1.76E-01 1.76E-01 2.04E-01 u 1.15E+OO 1.26E+OO 3.24E-01 4.91E-01 4.91E-01 4.15E-01 u 2.48E-01 2.49E-01 2.12E-01 u 1.90E-01 1.90E-01 2.76E-01 u 7.31E-02 7.31E-02 1.48E-01 u 19-09001-09 TRG 5.33E-02 2.21E-01 u TRG 1.88E+OO 1.66E+OO TRG 1.71E-01 2.82E-01 u TRG 1.15E-01 u 1.83E-01 u 06/11/19 12:15 1.91E+OO u 06/11/19 12:15 4.74E-01 06/11/19 12:15 4.72E-01 TRG L 1-10221A-FIGS-001-SS-A 06/11/19 12:15 9/10/2019 2.45E-01 u TRG L 1-10221A-FIGS-001-SS-A 9/10/2019 19-09001 Radium-226 4.42E-01 u TRG L1-10221A-FIGS-001-SS-A 9/10/2019 19-09001 Antimony-125 7.38E-01 u TRG L1-10221A-FIGS-001-SS-A 9/10/2019 19-09001 Thorium-234 u pCi/g TRG L 1-10221A-FIGS-001-SS-A 9/10/2019 19-09001 Thallium-208 EPA901.1 u pCi/g TRG L 1-10221A-FIGS-001-SS-A 9/10/2019 19-09001 Uranium-235 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 12 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: _ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 8.03E-01 2.69E-01 2.72E-01 4.13E-01 pCilg 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 9/10/2019 19-09001 Si1ver-108m EPA 901.1 Modified 5.26E-04 ___
| |
| 6.72E-02 ___
| |
| 6.72E-02 1.03E-01 u 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 9/10/2019 19-09001 Americium-241 EPA901.1 Modified -1.26E-01 9.46E-02 9.49E-02 1.26E-01 u 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/1912:15 9/10/2019 19-09001 Barium-133 EPA 901.1 Modified 1.24E-01 1.12E-01 1.12E-01 1.50E-01 u pCi/g 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA 901.1 Modified 3.24E-01 1.43E-01 1.44E-01 2.84E-01
| |
| -------- ----*---- --> m-.-'-"-.N"-- > ------------~* '
| |
| *******+---
| |
| 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 Cobalt-60 EPA 901.1 Modified 4.96E-01 9.43E-02 9.77E-02 1.25E-01 pCi/g
| |
| , , , , _ mv _ _ _ _ , _ _ _ _ _ _
| |
| ._,,m, ,_,_, * - - - - ' " ' ' -
| |
| 19-09001-10 : TRG . L1-10221A-QIGS-001-SS-A 06/11/1912:15 9/3/2019 9/10/2019 Cesium-134 EPA 901.1 Modified 6.42E-03 4.74E-02 4.74E-02 1.18E-01 u 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/1912:15 9/3/2019 9/10/2019 Cesium-137 EPA 901.1 Modified 2.14E+OO 2.85E-01 3.06E-01 1.40E-01 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/1912:15 9/3/2019 9/10/2019 EPA901.1 Modified -1.93E-01 2.53E-01
| |
| ----*-***** *-*--*-**********-----**-***--1--*---**----*******-i*---------*-****"""-*******---'----'-----+-*---***-*---'---------****t--*---=**.........../-...::....~:.::.________....::.:.:..::.....:.._
| |
| 2.53E-01 2.28E-01 u 19-09001 ~ - - - L1-102}_1_1,:_<?_19'S-001-~~---* 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified -7.59E-02 1.64E-01 1.64E-01 1.18E-01 u 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified 7.72E-02 1.12E-01 1.12E-01 1.66E-01 u
| |
| **-*---*---*+***-*-------********---****-*--***~--------*******--*--'----****-****l*****--****--********-*---*-*-*+*-------C-*-*----**--*-*-*-**---*****-
| |
| 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified -1.36E-02 1.18E-01 1.18E-01 8.34E-02 u
| |
| **-*-**-*********-*************-**----------****--***-*--l-***--**-**-- -'***--***--****-*---C---******--********-*****--l,*******----***-**----+*--*-*--'-**---************--*-**-
| |
| 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/19 12:15 9/3/2019 9/10/2019 19-09001 lodine-129 EPA 901.1 Modified 3.24E-02
| |
| ' 7.32E-02 7.33E-02 1.10E-01 u 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/1912:15 9/10/2019 19-09001 Potassium-40 EPA 901.1 Modified 1.60E+OO 1.68E+OO 7.97E-01
| |
| *--*-**-****-*-***-***-**-------******-**--*-J---*-**---***-**+-------**-***-****-**-------~---******-*-***-1-----*---------++--*'"-**-**------*******<---***----
| |
| 19-09001-10 TRG L1-10221A-QIGS-001-SS-A 06/11/1912:15 9/10/2019 7.77E-02 1.32E-01 u
| |
| ****-------------***--!--**-*--*--*---,****-*-------**--*****----r------1---*
| |
| L1-10221A-QIGS-001-SS-A 06/11/19 12:15 9/10/2019 6.78E-02 8.39E-02 u 6.11E-02 9.31E-02 u 8.15E-01 1.36E+OO u 19-09001 1.12E-01 2.36E-01 19-09001 1.29E-01 3.70E-01 9/10/2019 19-09001 9.33E-02 1.29E-01 u 9/10/2019 19-09001 9/10/2019 19-09001 L1-10221A-QIGS-001-SS-A 06/11/19 9/10/2019 19-09001 u pCi/g L1-10221A-QIGS-001-SS-A 06/11/19 9/10/2019 19-09001 1.65E-01 2.42E-01 pCi/g TRG L1-10221A-QIGS-001-SS-A 9/10/2019 19-09001 3.30E-01 4.73E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( "'M> EBERLINE ANAL YT! CAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34AM Page 13 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions ___ ____ , Purchase Order:
| |
| SDG.
| |
| 677118 Final Report of Analysis 2701 Deborah Ave _.. Analysis. Category: .. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date ID Analyte Method Result cu CSU MDA Qualifier Date Units 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/19 12:17 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 2.28E-01 3A9E-01 3A9E-01 5.71E-01 u pCi/g 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/1912:17 w,'---*-*-- 9/3/2019 9/10/2019 " _____
| |
| .... . . ., ____________________ 19-09001 . --**--'""*-------
| |
| Silver-108m EPA 901.1 Modified -3.68E-02 8-57E-02 8-57E-02 1.30E-01 u
| |
| ',-w,**--*--**----*----"''-""'--*---*----
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/1912:17 9/3/2019 9/10/2019 19-09001 Americium-241 EPA 901.1 Modified 1-01E-01 1A3E-01 u pCi/g
| |
| - - * - - * - * - - - - " " "">'- - - - ,-------m-o~--'"-"-"''-* '""'
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/1912:17 9/3/2019 9/10/2019 19-09001 Barium-133
| |
| , _ _, _______ EPA90U Modified
| |
| ,,,, -+*---*-----------------------*--*- 7.86E-02 1.53E-01 u pCi/g 19-09001-11 TRG L 1-10221A-FIGS-002-SS-A 06/11/19 12:17 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA901.1 Modified 6.11E-01 1-75E-01 1.78E-01 4.10E-01
| |
| *- *------'--------*------- ,,,*--------------*+--------*------*---*----- ---.-----------------*-:----------------
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/19 12:17 9/3/2019 9/10/2019 19-09001 Cobalt-60 EPA 901-1 Modified 3.13E+OO 3.21E-01 3-59E-01 2.31E-01 19-09001-11 TRG L1-10221A-FIGS-002-SS-A Cesium-134 4A2E-02 4A2E-02 1A9E-01 19-09001-11 TRG L1-10221A-FIGS-002-SS-A Cesium-137 8-68E-01 9.85E-01 1.88E-01 EPA 901.1 Modified 3.27E-01 3.27E-01 2.78E-01 EPA 901.1 Modified -1.39E-02 2.39E-01 2.39E-01 1A5E-01 19-09001-11 TRG L1-10221 A-FIGS-002-SS-A 9A4E-02 U5E-01 U5E-01 1-69E-01 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/19 12:17 19-09001 Modified -3.74E-02 1-31E-01 1-31E-01 1-0SE-01 U pCi/g
| |
| ------------------------------------*-1-------------------------------------*--------------s----------t-----------------*-----,------*-------*---------------------------------------------<
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/1912:17 19-09001 lodine-129 EPA 901-1 Modified -1A2E-02 1A4E-01 1A4E-01 4.33E-01 U pCi/g
| |
| -----*--**---1-----------------;-------------------------------+--,-----------,-------------------------------*---------------~---------------------------------------<
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/1912:17 EPA 901-1 Modified 1.53E+01 3.08E+OO U4E+OO 19-09001-11 TRG L1-10221A-FIGS-002-SS-A EPA 901.1 Modified 6.25E-02 1-03E-01 1.67E-01 19-09001-11 TRG L1-10221A-FIGS-002-SS-A EPA 901-1 Modified 4.54E-02 7.22E-02 7.23E-02 1.0SE-01 19-09001-11 TRG L1-10221A-FIGS-002-SS-A EPA901.1 Modified 1.54E-02 9-34E-02 9.34E-02 1.09E-01 19-09001-11 TRG EPA901.1 Modified 1.12E+OO
| |
| - -L1-10221A-FIGS-002-SS-A
| |
| - - ----------------1-----: 06/11/19
| |
| _____________ 12:17 _;______ ,_ ________;,____-+------------l----------*- 1.06E+OO 1.75E+OO 19-09001-11 - TRG L1-10221A-FIGS-002-SS-A 06/11/1912:17 EPA901.1 Modified 4.74E-01 4.73E-01
| |
| '----*-*=--*------* -
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/19 12:17 EPA901.1 Modified 4.75E-01 3.67E-01 1----------*----*=
| |
| 19-09001-11 TRG L1-10221A-FIGS-002-SS-A 06/11/19 12:17 EPA901.1 Modified -6AOE-02 2.85E-01 u pCi/g L1-10221A-FIGS-002-SS-A EPA 901.1 Modified 6.11E-01 4.10E-01 L1-10221A-FIGS-002-SS-A EPA 901.1 Modified 36E-01 5.07E-01 u L 1-10221A-FIGS-002-SS-A EPA 901-1 Modified 5.66E-01 1-32E+OO u 19-09001-11 TRG L1-10221A-FIGS-002-SS-A Thallium-208 4.76E-01 5.15E-01 u 19-09001-11 TRG L1-10221 A-FIGS-002-SS-A Uranium-235 EPA 901-1 Modified 2.00E-01 5.98E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34 AM Page 14 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical - ~,v._.,__,_,., * - -
| |
| * Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: .. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09001-12 TRG L 1-10221 A-Fl GS-003-SS-A 06/11119 12:19 9/3/2019 Actinium-228 EPA901.1 Modified 5.38E-01 2.63E-01 TRG L 1-10221A-FIGS-003-SS-A 06/11/1912:19 9/3/2019 9/10/2019 Si1ver-108m EPA 901.1 Modified 2.SSE-02 6.48E-02 19-09001-12 TRG L 1-10221A-FIGS-003-SS-A 06/11119 12:19 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified 1.20E-01 u 19-09001-12 TRG L 1-10221A-FIGS-003-SS-A 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified 1.19E-02 3.82E-02 3.82E-02 1.26E-01 u EPA901.1 Modified 2.83E-01 2.0SE-01 2.0SE-01 3.68E-01 u EPA 901.1 Modified 2.06E-01 2.27E-01 1.98E-01 EPA 901.1 Modified 1.20E-02 3.52E-02 3.53E-02 1.23E-01 u EPA 901.1 Modified 5.89E-01 6.64E-01 1.82E-01 EPA 901.1 Modified 2.71E-01 2.71E-01 2.20E-01 u 19-09001-12 TRG L 1-10221A-FIGS-003-SS-A 06/11119 12:19 9/3/2019 9/10/2019 EPA901.1 Modified 2.14E-01 2.14E-01 1.12E-01 u
| |
| ---------------*-*- ---*---*---*---------*-*-*- '"' -*---------+-------*-*-----*-*
| |
| 19-09001-12 TRG L1-10221A-FIGS-003-SS-A 06/11119 12:19 ' ---- 9/312019 9/10/2019 EPA901.1 Modified 9.54E-02 9.54E-02 1.35E-01 u 19-09001-12 TRG L 1-10221A-FIGS-003-SS-A 06/11/1912:19 i 9/3/2019 9/10/2019 19-09001 EPA 901.1 Modified 1.07E-01 107E-01 9.10E-02 u 19-09001-12 TRG L 1-10221 A-FIGS-003-SS-A 06/11/19 12:19 ' 9/312019 9/10/2019 19-09001 EPA 901.1 Modified 9.56E-02 9.56E-02 3.75E-01 u 19-09001-12 TRG L 1-10221A-FIGS-003-SS-A 06/11/1912~*+* 9/3/2019 9/10/2019 19-09001 Potassium-40 EPA901.1 Modified 2.45E+OO 2.52E+OO 1.44E+OO 19-09001-12 L 1-10221A-FIGS-003-SS-A 06111/19 12:19 9/3/2019 9/10/2019 19-09001 Manganese-54 4.74E-02 4.74E-02 1.23E-01 u 19-09001-12 L1-10221A-FIGS-003-SS-A 06/11/19 12:19 9/3/2019 9/10/2019 19-09001 Molybdenum-93 5.44E-02 6.41E-02 u 19-09001-12 L 1-10221A-FIGS-003-SS-A 06/11/19 12:19 ! 9/3/2019
| |
| ------------=-
| |
| 9/10/2019 19-09001 Niobium-94 7.0SE-02 9.56E-02 u 19-09001-12 L 1-10221A-FIGS-003-SS-A 06/11/1912:19 9/10/2019 19-09001 Lead-210 1.34E+OO u L 1-10221A-FIGS-003-SS-A 9/10/2019 19-09001
| |
| -- Lead-212 2.89E-01 9/10/2019 19-09001 Lead-214 3.63E-01 u u
| |
| 9/10/2019 19-09001 Promethium-145 2.31E-01 9/10/2019 .,.. 19-09001 Radium-226 3.68E-01 u L 1-10221 A-FIGS-003-SS-A 9/3/2019 9/10/2019 19-09001 Antimony-125 4.07E-01 u L 1-10221A-FIGS-003-SS-A 06/11/1912:19 9/3/2019 9/10/2019 _..._ 19-09001 Thorium-234 u L 1-10221A-FIGS-003-SS-A 06/11/1912:19 9/3/2019 9/10/2019
| |
| * 19-09001 Thallium-208 L 1-10221A-FIGS-003-SS-A 06/11/1912:19 9/3/2019 9/10/2019 19-09001 Uranium-235 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 1012112019 11 :34 AM Page 15 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical SDG:
| |
| Final Report of Analysis Zion Solutions ______ 677118 Purchase Order: . __ --'-"""'-**-***-**-----*
| |
| , __ 2701 Deborah Ave .. Analysis Category:, ENVIRONMENTAL Zion, IL 60099 Sample Matrix.* so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09001-13 ' TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019
| |
| .. 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 2.39E-01 3.74E-01 3.75E-01 6.21E-01 u pCi/g
| |
| -*---*-----~----,"** --**- **-** ¥*------*--*----
| |
| 19-09001-13 TRG L 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 __,_____
| |
| 9/10/2019 19-09001 Silver-108m EPA 901.1 Modified -3.87E-02 R96E-02 8.96E-02 U6E-01 u pCi/g
| |
| ' " '"'"""- *---~------------- a - * - -**-* ---~---*-------
| |
| ,--"-*- ,,_ _ _._,m_ ,
| |
| "'"'"""'""*---~--"'
| |
| 19-09001-13 TRG _______
| |
| l 1-10221 A-FIGS-004-SS-A "' ________ 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 Americium-241
| |
| ,------*- *---"----------,-.-~-~--- ----------
| |
| EPA 901. 1 Modified -1.01E-01 1.23E-01
| |
| *--~~~-*--"'
| |
| 1.23E-01 1.70E-01 u pCi/g u
| |
| -------*--*--*--*---.l-,---~--"-'' ,_, __ ' _.....
| |
| 19-09001-13 TRG l1-10221A-FIGS-004-SS-A 06/11/1912:21 9/3/2019 9/10/2019 19-09001 Barium-133 EPA901.1 Modified -3.94E-02 4.61E-02 4.62E-02 1.96E-01 pCi/g
| |
| -----*- '""" - ---*--*-----*--*--***~ *----* i -* *-----------
| |
| 19-09001-13 TRG l1-10221A-FIGS-004-SS-A
| |
| ---** '" ___ 06/11/1912:21 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA 901.1 Modified 6.98E-01 2.03E-01 2.07E-01 1.08E-01 pCi/g
| |
| ,_ 19-09001-13 i' ________________
| |
| TRG l 1-10221
| |
| ______ A-FIGS-004-SS-A -
| |
| 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 : Cobalt-60
| |
| --,- EPA 901.1 Modified 1.41E+OO 1.59E--01 1.74E-01 1.91E-01 pCi/g 19--09001-13 TRG l 1-10221 A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 Cesium-134 EPA901.1 Modified 4.20E-02 6.23E-02 6.23E-02 1.51E-01 u pCi/g 19-09001-13 TRG l 1-10221 A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 Cesium-137 EPA 901.1 Modified 5.83E+OO 6.94E-01 7.55E-01 2.15E-01 pCi/g
| |
| ----~- . . ----
| |
| ____________ ___ TRG
| |
| "' ..., __ l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001
| |
| ----""''"'""'-~--
| |
| LUl...-,...,.,.,11-1.JL EPA 901.1 Modified 5.74E-02 3.21E-01 3.21E-01 3.12E-01 u pCi/g 19-09001-13
| |
| -------------------, TRG
| |
| "---------~-"-'"" _______
| |
| l 1-10221A-FIGS-004-SS-A
| |
| " _______ 06/11/19 12:21
| |
| - f---,--,------,w,-* '
| |
| 9/3/2019 9/10/2019 19-09001 ________
| |
| Europium-154... ... _ EPA901.1 Modified -1.67E-01 2.20E-01 2 . 20E-01 1.60E-01 u pCi/g 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 , :::u, -,*-* "- ,55 EPA 901.1 Modified 5.04E-03 1.47E--01 i 1.47E-01 2.12E-01 u pCi/g
| |
| -----------,.-------------------**-- ------------~--
| |
| 19-09001-13 TRG ________________________
| |
| l 1-10221A-FIGS-004-SS-A " ____ 06/11/19 12:21 i
| |
| 9/3/2019 9/10/2019 19-09001 ; Holmium-166m EPA901.1 Modified 8.59E-02 8.90E-02 8.91E-02 1.12E-01 u pCi/g 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/1912:21 9/3/2019 9/10/2019 19-09001 ! lodine-129 EPA901.1 Modified : 2.26E-01 1.09E-01 1.10E-01 1.69E-01 u pCi/g
| |
| --------,-~---------*---------------
| |
| f-*
| |
| 19-09001-13 TRG l 1-10221A-FIGS--004-SS-A
| |
| ---------~-- '"'""""
| |
| 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 i - ..4n EPA901.1 Modified 9.33E+OO 1.70E+OO i 1.77E+OO 1.15E+OO pCi/g 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 : ...... ... .................
| |
| ,:,, , EPA 901.1 Modified -4.06E-03 1.10E--01 1.10E--01 1.73E-01 u pCi/g 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 i " "1"h-<-n .. m M EPA 901.1 Modified 8.61E-04 8.53E-02 i 8.53E--02 7.90E-02 u pCi/g 19-09001-13 i TRG i l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 i Niobium-94 EPA901.1 Modified 2.11E-02 9.58E-02 9.58E-02 1.27E-01 u pCi/g 19-09001-13
| |
| * TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19--09001 i lead-210 EPA901.1 Modified : 1.05E+OO 1.01E+OO 1.01E+OO 1.53E+OO u pCi/g 19--09001-13 i TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 ; 9/3/2019 9/10/2019 19-09001
| |
| * Lead-212 EPA 901.1 Modified 2.74E-01 : 2.0SE-01 2.09E-01 3.44E-01 u pCi/g 19-09001-13 ' TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 i
| |
| 9/3/2019 9/10/2019 i 19-09001 Lead-214 EPA 901.1 Modified 5 . 18E-01 i 2.82E-01 i 2.83E-01 4 . 55E-01 i pCi/g i u 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 19-09001 Promethium-145 EPA901.1 Modified 5.13E-02 8.22E-02 . 8.22E--02 1.88E--01 pCi/g
| |
| ! 9/3/2019 ___,
| |
| 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/1912:21 9/10/2019 i 19-09001 Radium-226 EPA901.1 Modified 6.98E-01 : 2.03E-01 i 2.07E-01 1 . 08E-01 . pCi/g 19-09001-13 i TRG l 1-10221A-FIGS-004-SS-A 06/11/1912:21 I 9/3/2019 9/10/2019 19-09001 Antimony-125 EPA901.1 Modified -2.18E-02 i 3.88E-01 i 3.88E-01 5.24E-01 u pCi/g i---
| |
| 19-09001-13 TRG l 1-10221A-FIGS--004-SS-A 06/11/1912:21 9/3/2019 9/10/2019 ' 19-09001 Thorium-234 EPA 901.1 Modified i 1.26E+OO ; 1.13E+OO 1.13E+OO 1.71E+OO ! u pCi/g i
| |
| 19-09001-13 TRG L1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019
| |
| ---~------- i 9/10/2019
| |
| * 19-09001 Thallium-208 EPA 901.1 Modified 3.28E-01 l 1.44E-01 i 1.45E-01 1.57E-01 : pCi/g 19-09001-13 TRG l 1-10221A-FIGS-004-SS-A 06/11/19 12:21 9/3/2019 9/10/2019 i 19-09001 Uranium-235 EPA 901.1 Modified 2.46E-01 I 4.34E-01 i 4.34E-01 6.52E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201911:34 AM Page 16 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical " ______ _____
| |
| Zion , Solutions
| |
| _ Purchase Order:
| |
| SDG.*
| |
| 677118 Final Report of Analysis 2701 ________
| |
| ____ Deborah Ave--*--
| |
| ,,, ~f1_a/ysis Cat'!J!ory: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Date Analyte Method Result cu CSU MDA Qualifier ID Type ID Date ID Units 19-09001-14 TRG L1-10220!-FJGS-005-SS-A 07 /09/19 08:30 19-09001 '"'_, ___________
| |
| Actinium-228 EPA 901.1 Modified 9.41E-01 2.58E-01 2.63E-01 4.49E-01 pCi/g 19-09001-14 TRG L1-102201-FJGS-005-SS-A 07 /09/19 08:30 19-09001 Silver-108m EPA 901.1 Modified 2.65E-02 6.04E-02 6.04E-02 1.08E-01 u 19-09001-14 TRG L1-10220!-FJGS-005-SS-A 07 /09/19 08:30 Americium-241 EPA 901.1 Modified 1.72E-01 1.85E-01 1.85E-01 2.55E-01 u
| |
| *-----**-** -----**- *****- **1--*-*******--**-****--,-----~---*---:**-***** --*****-i******--*--*****
| |
| 19-09001-14 .. TRG L1-10220!-FJGS-005-SS-A 07/09/19 08:30 Barium-133 EPA 901.1 Modified 1.47E-04 6.39E-02 6.39E-02 1.57E-01 u 19-09001-14 TRG L1-10220!-FJGS-005-SS-A 07/09/19 08:30 19-09001 Bismuth-214 "W_WC _ _ _ _ _
| |
| EPA 901.1 Modified 2.26E-01 2.33E-01 2.94E-01 19-09001-14 TRG l 1-102201-FJGS-005-SS-A 19-09001 Cobalt-60 EPA 901.1 Modified 1.14E-01 1.64E-01
| |
| -*--'"-...,."-'"m _ _ _ _ "'"'""' _ _ _ _ '"'"'' -*e'-- ....,.......... .
| |
| 19-09001-14 TRG L1-10220!-FJGS-005-SS-A 19-09001 Cesium-134 EPA 901.1 Modified 3.0SE-02 9.89E-02 u 19-09001-14 TRG 19-09001-14 TRG L1-10220!-FJGS-005-SS-A L1-102201-FJGS-005-SS-A
| |
| "" ------------ 07/09/19 08:30 9/3/2019 2019 19-09001 Cesium-137
| |
| ----"-"''"'*----,----- -----~,,____________
| |
| 9/10/20~- __1_9~-"..~99~ _ Europium-152
| |
| ,, ____ EPA 901.1 Modified EPA 901.1 Modified 4.74E-01 2.35E-01 1.76E-01 3.00E-01 19-09001-14 TRG l 1-10220!-FJGS-005-SS-A 07/09/19 08:30 1_9_i3_i2_0_1_9__,__9_i1_0_i2_0_19 _ __1_9~~-001 Europium-154 ..J---E_P_A_9__0__1_.1__M_o__d_ifi_1e__ d _____ c******8_.__ 2.21E-01 64_E_-_02__ .. c.......2_.2_1_E_-0__1_____r*--*--****-**-*-**---------------'--..:::. .._-1 1
| |
| 19-09001-14 TRG L1-102201-FJGS-005-SS-A -* 07/09/19_ 08:30 / ~!312_0_19---i_9i_1_0i_2_01_9__1_9_-09"._01_ -~-ur_op_iu_m_-_1s_s-+__ E_PA_9_01_._1__
| |
| M_o_d_ifi_1e_d___ 0 1.82E-01 1.82E-01 19-09001-14 TRG L1-10220I-FJGS-005-SS-A 07/09/19 08:30 9/3/2019 9/10/2019 19-09001 Holmium-166m EPA 901.1 Modified 1.30E-01 1.30E-01
| |
| -***---**** :-------+-*------**-*c-*-----....+-------*-**---***-**i--**--*----...;........_ _ ___:__________________________:___:::__-1 19-09001-14 . TRG L1-10220I-FJGS-005-SS-A Cl"i'/09/19 ".._8~~? 9/3/2019 : 9/10/2019 *--~ 9-~~-- lodine_-1_2_9_+-_E_P_A_90_1_.1_M_od__ifi_1e__d_______ +----- 7.19E+OO 19-09001-14 L1-10220!-FJGS-005-SS-A *** -~~?f_19_0_8~.9_ , 9/3/2019 , 9/1012_:>.1_9__ 19_:-_(_J~~- ---~-ot_a_ss_iu_m_~-t-----E_P__A__9_0_1_.1__M_o_d_ifi_e_d __..... _, ______ *****--*-i--*-*--*--r---------------*-*-_..;_ __:___:;:.__
| |
| --------------*- .----- 1 19-09001-14 TRG L1-102201-FJGS-005-SS-A 07/09/19 08:30 ' 9/3/2019 9/10/2019 19-09001 Manganese-54 EPA901.1 Modified
| |
| --------~*"-----
| |
| 19-09001-14 TRG l 1-10220!-FJGS-005-SS-A 07/09/19 08:30 ! 9/3/2019 ' 9/10/2019 19-09001
| |
| * Molybdenum-93*+****--E-P-*A***-9-0*1-.*1-*-M--o-d-ifi-ed-*-****;*-----*-**-'-*------*-*'------------c.--------'-**-::__---1 19-09001-14 TRG l 1-102201-FJGS-005-SS-A ***07/09/1908:30T 9/3/2019 9/10/2019 19-0900*1--N;;;;;;~;;:,-94 EPA 901.1 Modified
| |
| -----+----*--*-***--*--'-------*---*-----~,--*--------------,--*-*-'-__;;::___-I 19-09001-14 TRG l 1-10220!-FJGS-005-SS-A -~°-?/09/19 08:30 i 9/3/2019 ' 9/10/2019 19-09001 Lead-210 EPA 901.1 Modified
| |
| *-**-"***--------j----:---------**-**---;---------~----:-:-::--:---c------------:---:--'--"---------*---:----t 19-09001-14 TRG L1-102201-FJGS-005-SS-A 07/09/19 08:30 9/3/2019 9/10/2019 19-09001 Lead-212 EPA 901.1 Modified 4.36E-01
| |
| ----------------*-***-1--
| |
| 19-09001-14 TRG L1-10220!-FJGS-005-SS-A 07/09/19 08:30 9/3/2019 9/10/2019 19-09001 Lead-214 EPA 901.1 Modified 19-09001-14 TRG L1-102201-FJGS-005-SS-A 07/09/19 08:30 9/3/2019 9/10/2019 19-09001 ' Promethium-145 EPA 901.1 Modified
| |
| *-------------------1--------1--------:- ----+------------***---i----------..:.----_..;.-----------'-------~-'--..::.._-1 TRG L1-102201-FJGS-005-SS-A 07/09/19 08:30 9/3/2019 9/10/2019 19-09001 Radium-226 EPA 901.1 Modified
| |
| ----------******---*----***-+--------,---------****----- . -----+--*-**-------*---+--------L------+-----------i------*--'-,;:__--1 l 1-102201-FJGS-005-SS-A 9/10/2019 19-09001 Antimony-125 EPA901.1 Modified 2.00E-01 3.26E-01
| |
| ---19-t-9/_1_0/-20_1__ 9 19-09001 Thorium-234 i*---_E--PA--9-01-_=-1-M-o-difi_e_d--+*---:-*~--~--;---:-1_=-69=-E=-+=-o-:o--c-1-.6=-9=-E-+=-oo----:=-:-:-t--:---:---:-----=---;
| |
| L1-10220!-FJGS-005-SS-A
| |
| ---}-----------*. -----+----------i-----*--+-----.;.-----------+-----;---'---=---1 l 1-10220!-FJGS-005-SS-A 9/10/2019 19-09001 Thallium-208 EPA901.1 Modified 1.61E-01 1.64E-01 1.63E-01
| |
| -----+---------;------l-------i---*---------'----**-c---'---=----1 L1-10220!-FJGS-005-SS-A 07/09/19 08:30 ! 9/3/2019 9/10/2019 19-09001 Uranium-235 EPA 901.1 Modified 5.37E-01 5.37E-01 6.90E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/2019 11 :34 AM Page 17 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical --*-* ,_ ______________
| |
| Zion Solutions _ Purchase Order:
| |
| SDG:
| |
| 677118 Final Report of Analysis 2701 Deborah Ave
| |
| _Analysis Category: __ _i:~Y!~Q-~~ E~J:.A.!::_
| |
| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report
| |
| , Type Date Date ID Analyte Method Result cu CSU MDA Qualifier ID ID Date Units 19-09001-15 TRG L 1-102201-QJGS-005-SS-A *--- 07/09/1908:30 : 9/3/2019 9/10/2019 ____1~-090~- Act~um-228 _ EPA901.1 Modified 6.54E-01 : 2.39E-01 2.41E-01 4.40E-01 pCi/g 19-09001-15 TRG L 1-102201-QJGS-005-SS-A . __ -** 07/09/19 08:30 _ J .~'.3/202_\l ____ 9/10/2019___~0900.!._ ---~lver::_:?8..":...__,___ E_PA 901.1 Modified -5.37E-03 3.41 E-02 3.41 E-02 9.17E-02 U pCi/g 19-09001-1*5**-**,,--*****T*--R*G*--*-*--*-L*-*1*--1--0*--2*2**01-QJGS-005-SS-A 07/09/19 08:30 9/31~°.:.'.'.. .J1:1°.~~0_19__ . __ 19_-0_9_00_1 -~":'':._nc._iu_m._-2_4_1_+--*-E__P.A_ 9_0_1__.. 1 *._M_o_d_i.fi_,e___d***-----*-*8*_*2_8.*E....-.o.*.2.....~ __
| |
| 1._51_E_-0__1_.____1__.51 E-01 2.04E-01 u pCi/g 19-09001-15 , TRG L 1-10220!-QJGS-005-SS-A ---*-**-**- _o_7!£9!_19 08:30 , 9/312-?1.9**-***9!_1_~_01_9_ _ 19_-~°.0~ -~-~~um-~~--***-*--E__ PA__ 9_0.1.1 Modified [ 9.64E-03 4.71E-02 4.71E-02 1.25E-o.1_.-**-***--*****-u*-*------***-*-*-p-Cil_g __ ,
| |
| 19-09001-15 TRG L 1-10220!-QJGS-005-SS-A 07/09/19 08:30 9/3/2019 9/1012019 19-09001 Bismuth-214 EPA 901.1 Modified 1 8.02E-01 1.65E-01 1.71E-01 2.36E-01 pCi/g
| |
| ""-""-"-""'"'-"""""""" _____ ,__,_____,.______,______* "---v-""""'""*--*-----*-**-** *********----***** I******** *********-**-***********---**-****+***----***-***-***-****-*******
| |
| 19-09001-15 TRG L1-102201-QJGS-005-SS-A 07/09119 08:30 [ 9/3/2019 9/10/2019 19-09001 , Cobalt-60 EPA 901.1 Mo_d_ifi_,e_d_*--***"'****-5 __._47_E_-0_1__,___9_. _1..7_..E.._-_0_2..**.* , ..__
| |
| 9_.5_9E_-_o.2_**--************1*****6*_0.E_.-_o._1 _____.__**--*-*---pCil_g____,
| |
| 19-09001-15 : TRG L1-102201-QJGS-005-SS-A 07/09/1908:30 : 9/3/2019 9/10/2019 19-09001 : Cesium-134 EPA901.1 Modified : 2.22E-02 ' 3.58E-02 3.58E-02 7.99E-02 U pCi/g
| |
| ----"-***--------------------,-,---------~*-----<--*---------+*-***-*---------------*-------!-**
| |
| 19-09001-15 TRG L1-10220I-QJGS-005-SS-A 07/09/1908:30 I 9/3/2019 9/10/2019 19-09001 : Cesium-137 EPA901.1 Modified : 2.65E+OO i 3.41E-01 3.67E-01 1.40E-01 pCi/g
| |
| - - - - - , _ _ _ _ _ _ _ _ , _ _ _ _ _ _ _ _ , _ _ _ _ _ _ , _ _ ,w _ _ _ , , _ _,_****------*-***-*--*-------**-------e-***-------1-**---*******-***
| |
| 19-09001-15 , TRG L1-10220I-QJGS-005-SS-A 07109/19 08:30 : 9/3/2019 , 9/10/2019 19-09001 : ;:"'-c*-* 152 EPA901.1 Modified -9.65E-03 3.03E-01 ' 3.03E-01 2.87E-01 U pCi/g 1
| |
| , *..._1_._9_-._o.._9..0__0_1_-_1_5___,:___T_R_G__,,_.._L._.1..-.._1..o.*2._2_._rn_-o_J_G_s_-0_0_5-_s_s_-A*-***-----;--o_1_10.__9_1_1_9_o8_:3_o_,--;9_13_1_2_0_1_9_. ___._9_1__1__
| |
| 01_20_1_9___1_9_-09_0.o_._1 __** _.:::__ "'-.-"*-_*_.1.54. __ ___ EP!'_.90_1_._1__M_o.d_ifi_,.e_d_***----+--1_.2_2E_-_0_1__,1__7_.8_7_E-_0_2___1_..8_9_E__ -0_2*--*-**-*1__.e_1_E.__ -0_1______ u_._.____P_Ciig_ ___,
| |
| 1
| |
| __ .1_~~001::.:~___ T_RG
| |
| ____~:_1_°.2.~~~---Q__ JG_S.::."._Cl_5-_S_S:~.... 07/09/19 08:30 ; 9/3/2019 9._1_1._0_12,_0_19__1_9_-o._9_00_1.__ 1:::_"'_*--*._15._5 __...._ _E_P_A_9.01.1 Modified 6.46E-02 7.46E-02 7.47E-02 2.06E-01 U pCi/g 19-09001-15 TRG L1-10220I-QJGS-005-SS-A 07/09/1908:30 : 9/3/2019 9/10/2019 19-09001 ! Holmium-166m EPA901.1 Modified 6.18E-02 9.77E-02 9.78E-02 1.07E-01 U pCi/g
| |
| *19-:00001-1~-T-R--G-.,-1 -L-1--1-o-220~-Q-JG-S---ooS-"sS::-A _____,__0_7_/0_9_/1*-9*-o-8,-3o--*,-9--/3-l-20--1-9-**.-*-9-/1*-01-2--0*1-9--1-9--0-90-0--1-,-...l-1-od-in-e--1-2-9--**t-****-*--E**P--A-9_0_1_.-1--M--od-ifi-,e-d-*-********-4-.5._6_E_+_oo__,___1._93_E_+_0_1-.**--1.-93--E*-+--0--1-***--*-*-4*-.7-4..E--+*o***o*--*---***-*u****---*-----pCi/-g---:1 19-09001-15 TRG : L1-102201-QJGS-005-SS-A 07/09/1908:30 : 9/3/2019 : 9/10/2019 19-09001 ! - --- ... ,n EPA901.1 Modified 1.73E+01 2.52E+OO 2.67E+OO 1.46E+OO pCi/g 19-09001-15 TRG L1-10220I-QJGS-005-SS-A 07/09/1908:30 ! 9/3/2019 9/10/2019 19-09001 ! Manganese-54 EPA901.1 Modified -6.33E-03 : 7.17E-02 7.17E-02 1.10E-01 U pCi/g 19-09001-15 TRG L 1-10220!-QJGS-005-SS-A 07 /09/19 08:30 i 9/3/2.0_1_9__,_ __9_11_01_20_1_9_ 19-09001 : Molybdenum-93 EPA 901.1 Modified 6.44E-03 5.22E-02 5.22E-02 7 .83E-02 U pCi/g 19-09001-15 : TRG ' L 1-10220!-QJGS-005-SS-A 07/09/19 08:30 1 9/3/2019 9/10/2019 19-09001 , Niobium-94 EPA 901.1 Modified -6.73E-03 : 6.15E-02 : 6.15E-02 8.52E-02 U pCi/g l-*-**-*******-******---*-**-*----*-*----~--*-----*------*----;--------;-------*-----**-
| |
| 19-09001-15 , TRG : L1-102201-QJGS-005-SS-A 07/09/1908:30 l 913/2019 9/10/2019 19-09001 j Lead-210 EPA901.1 Modified 6.90E+OO
| |
| ---+-------*--**-*'-~----\.---_:..----*------_:..-::.:::__ _ _ _ ____:_______~:-::'.---1 l 3.20E+OO 3.22E+OO 4.86E+OO pCi/g
| |
| ___ 19_-_o9__0_01_-1_5_~ ___ _!_RG_....,'_ _ L 1_-1_0_22__0_1-_o_JG_s_-0_~5-_s_s_-A_______ . _0_1_10_91_1__ 9_o8_:_3o_ _9_J3_12_0__1_9._ _ 9i.1_0_12_0_19___ 19_-_o9_09~_-+!__L_e_ad_-_21_2__-+-*--E_PA_90_._1_....1__M_o_d_ifi_e_d--**-+--7_.5_2_E_-0_1___i-_1_A_6_E_-0_1___,__ 1._51_E_-0_1______ 3._17_E_-_01_ _ '_*---'---'p_C_ii-'-g--1 19-09001-15 TRG L1-102201-QJGS-005-SS-A 07/09/1908:30 [ 9/3/2019 9/10/2019 19-09001 : Lead-214 EPA901.1 Modified 8.38E-01 ( 1.99E-01 i 2.04E-01 3.22E-01 pCi/g 1------------,-~-----*--------*- ---------i-----+--
| |
| l-1_9_-o._9_00_1_-1_5~,__ TR_G_**-**+--L_1-_10_2_2rn __-O_J__
| |
| G_S_-0_0_5-_s__s_-A__.,.. - - + 07/09/19 08:30 9/3/2019 9/10/2019 19-09001 i Promethium-145 EPA 901.1 Modified 1.38E+OO 1.20E+OO l 1.20E+OO 1.48E+OO ' U pCi/g 19-09001-15 TRG , L1-10220I-QJGS-005-SS-A 07/09/1908:30 ; 9/3/2019 9J10i2019' 19-09001 I Radium-226 EPA901.1 Modified 8.02E-01 1.65E-01 1.71E-01 2.36E-01 pCi/g 1---**------**---------*------*----t-------+-
| |
| 19-09001-15 , TRG L1-102201-QJGS-005-SS-A 07/09/1908:30 / 9/3/2_0_19-_9_11_0_12_0:_!:._.._1_9_-0_9_00_1__An_1,_*m_o_ny_-_12_5-j- EPA901.~~~~E~_n:'.;~117'..=::l=._n~?-i-__.!.:.1.:'.:6.'..'.1E:::-~01'._j-:__'_1::'.6.'.:1E:::-::'.o1_,_____ :_2_:.'.'.8'.:.1=:E-~0~1_'_~u~--c--!:'.':'.'pCi,g_ig_.
| |
| L11_:9~-0::9~00~1~--1::5'..;._T_l:R~G~~--L~1':::.~*M~on*::.cr:::1*-::-~-'.l!-*::-~~~~-:~*1_______J_0_7._I0_91_19_0_8_:3_0_i_9i~-2-01_9__,,_9_i1_0_i2_0_19__ ,1_9_-0_9_0o_1-+,_T_ho_n_*u_m_-2_3_4_4-__E__P_A __9_o_1._1_Mo_difi_e_d __;!__-_1.2._4E-_0_1--_1._46_E_+_o_o_-+__1_.4_6E_+_o_o_ _1_.8_9_E+_o_o____u _ _ __:_P_:.Ci/g'--*~
| |
| 19-09001-15 TRG j L1-10220I-QJGS-005-SS-A 07/09/19 08:30 ! 9/3/2019 9/10/2019 : 19-09001 i Thallium_-_20_8--j[--E_PA ___9o._1_.1_M_o__d_.i_fi_,e_d_-ri_5_.6_6_E_-o_1--t__1_.2_7_E_-o_1_-j1____1_._3_1E_-01_ _ _ 1._29_E_-_01_,___ _-+__P--,--Cii_g_--1 19-09001-15 I TRG ! L1-102201-QJGS-005-SS-A 07/09/1908:30 i 9/3/2019 9/10/2019 19-09001 J Uranium-235 EPA901.1 Modified 2.43E-01 4.39E-01 1 4.39E-01 5.92E-01 U
| |
| * pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ""M>
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 1012112019 11 :34 AM Page 18 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 cc,cc,,,c,c,,,_,, ,,,,,,,,
| |
| c,c,c,,,c,,,-------------c,,cccc ---- ------- --
| |
| Final Report of Analysis 2701 Deborah Ave _Analysis Category* _____ENVIRONMENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09001-16 TRG L1-10221A-FIGS-003-S8-A 06/26/19 10:04 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 3,94E-01 __
| |
| _ _,,_,,c,cc,O,cc,_____ 1.76E-01 1.77E-01 3A9E-01 '"''"""''
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| pCi/g 19-09001-16 TRG L1-10221A-FIGS-003-SB-A 9/10/2019 19-09001 Silver-108m EPA 901.1 Modified 6,01E-02 7.38E-02 u
| |
| ----------------------------------cc, 19-09001-16 TRG L1-10221A-FIGS-003-S8-A 9/10/2019 19-09001 Americium-241 EPA 901.1 Modified 8,90E-02 U1E-01 u
| |
| '""""""""-"""""_'_"'""'""W""""" '"'"'" ~'"'""v-w" , - a - - - * " - " " " ' " ' - - "
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| 19-09001-16 TRG L1-10221A-FIGS-003-SB-A 06/26/1910:04 9/10/2019 19-09001 Barium-133 EPA90U Modified V9E-02 1,22E-01 u ------ pCi/g _
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| 1------------r---------'" ------------------c -------*-*-*--*--*- '"-~v -*---"'"-*----=-------***- : "'"----**-*-***-----**--~* --* _,,,,, -
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| 19-09001-16 TRG L1-10221 A-FIGS-003-SB-A 06/26/19 10:04 ~9/3/20!~ _9,~1_?/2019 09001___ Bismuth-21~ EPA 901.1 Modified U5E-01 1,52E-01 19-09001-16 TRG 06/26/1910:04 9/3/2019 9/10/2019 19-09001 Cobalt-60 EPA 901.1 Modified 8.95E-02 1,50E-01 u
| |
| ---,1-,.----------------+------r----------------: - -------------------
| |
| 19-09001-16 06/26/19 10:04 9/3/2019 9/10/2019
| |
| '""''---+--------------,,,c__ ,,_,____,,_,_.____ +--------,c,,c,,-,,,,,,___,____-'-----------------+-*-*cc,-,,-----+----
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| EPA 901.1 Modified 9-22E-02 9.72E-02 u 19-09001-16 TRG L1-10221A-FIGS-003-SB-A 06/26/19 10:04 EPA 901.1 Modified 3,83E-01 9,54E-02 974E-02 U6E-01 19-09001-16 TRG L1-10221A-FIGS-003-SB-A 06/26/19 10:04 EPA 901-1 Modified 8,69E-02 1.20E-01 1.20E-01 1.73E-01 u 19-09001-16 TRG L1-10221A-FIGS-003-S8-A 2,25E-01 8,98E-02 u 19-09001-16 TRG L1-10221A-FIGS-003-SB-A 1,01E-01 1_62E-01 19-09001-16 TRG C L1-10221A-FIGS-003-SB-A 8A2E-02 7-24E-02 u 19-09001-16 TRG L1-10221A-FIGS-003-S8-A 2.16E-01 3,00E-01 u 19-09001-16 TRG L 1-10221A-FIGS-003-S8-A 3,09E+OO 2,01E+OO 19-09001-16 TRG L1-10221 A-FIGS-003-SB-A 5A6E-02 1.01E-01 u pCi/g 19-09001-16 TRG L1-10221A-FIGS-003-S8-A u 19-09001-16 TRG
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| *---*----=_,___,L________________
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| 1-10221A-FIGS-003-S8-A 19-09001-16 TRG L1-10221A-FIGS-003-SB-A u
| |
| -----~"--"------
| |
| 19-09001-16 TRG L1-10221A-FIGS-003-S8-A EPA 901-1 Modified 1.98E-01 19-09001-16 TRG L1-10221A-FIGS-003-SB-A EPA 901-1 Modified 3,28E-01 U4E-01 2.37E-01 19-09001-16 TRG L1-10221A-FIGS-003-SB-A EPA 901-1 Modified 1A1E-01 2.05E-01 u 19-09001-16 Radium-226 EPA 901.1 Modified 4_31E-01 L15E-01 1-52E-01 19-09001-16 EPA 901-1 Modified 2,39E-02 1,SOE-01 1_80E-01 2.51E-01 u pCi/g 19-09001-16 TRG L1-10221A-FIGS-003-S8-A Thorium-234 EPA 901-1 Modified 4,35E-01 7A4E-01 7A4E-01 U1E+OO u pCi/g 19-09001-16 TRG L1-10221A-FIGS-003-S8-A Thallium-208 EPA 901-1 Modified 4.75E-01 1,97E-01 1-99E-01 3.06E-01 pCi/g 19-09001-16 i TRG L1-10221A-FIGS-003-SB-A Uranium-235 EPA 901-1 Modified 91E-01 2.51E-01 2,51E-01 3A7E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10121/201911:34 AM Page 19 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical . ,.,.,.,.,
| |
| Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 10:00 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA 901.1 Modified 7.03E-01 3.18E-01 3.20E-01 5.47E-01 pCVg 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 10:00 9/3/2019 9/10/2019 19-09001 Silver-108m EPA 901.1 Modified -5.84E-03 7.53E-02 7.53E-02 1.12E-01 u
| |
| '". ---**--'"-''""''" -----------~-.. --------"""
| |
| 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 10:00 9/10/2019 Americium-241 EPA 901.1 Modified 1.24E-01 1.24E-01
| |
| *-----****-******-*-***-** ""-cc------------**"""__ _
| |
| 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 9/10/2019 Barium-133 4.23E-02 4.23E-02 19-09001-17 TRG
| |
| ........................................................... L1-10221A-FIGS-001-SB-A
| |
| - ......... -----~---*-----------------<*** . 06/26/19 10:00
| |
| *****----.. -***- 9/10/2019 Bismuth-214 2.00E-01 2.02E-01 3.66E-01 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 10:00 9/10/2019 Cobalt-60 7.87E-02 7.99E-02 1.20E-01 19-09001-17 19-09001-17 TRG TRG L1-10221A-FIGS-001-SB-A L1-10221A-FIGS-001-SB-A
| |
| ___ 06/26/19 10:00 9/10/2019 19-09001
| |
| .........--;------***----,..**-----~..*---***---- ...-----*****......
| |
| 9/10/2019 19-09001 Cesium-134 Cesium-137 EPA901.1 Modified EPA 901.1 Modified 6.99E-03 3.96E-02 1.54E-01 3.96E-02 1.59E-01
| |
| _____ _. .............................____________............-+..- -..........____;--..-*---..,.....**---*****-*-**-*-...---<-***-****----*--*---1-----*-******................. +----..--*-*--*--*---*--'-**----------*-----*....C--------*-**-*:........::.........~
| |
| 1.38E-01 3.49E-01 u
| |
| 19-09001-17 TRG L1-10221A-FIGS-001-SB-A
| |
| ___...............................- - - - - - - - - -..----*--+*--------*-----..*-*---;--*..................,.........
| |
| 9/10/2019 19-09001 Europium-152 EPA 901.1 Modified 1.07E-02 1.82E-01 1.82E-01 2.62E-01 u 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 9/10/2019 19-09001 EPA 901.1 Modified -4.59E-02 2.43E-01 2.43E-01 1.37E-01 u
| |
| --~-------,-,,.---,--------*'-**----*-------------*
| |
| 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 10:00 9/3/2019 9/10/2019 19-09001 EPA901.1 Modified 1.39E-01 2.17E-01 u
| |
| --*------ --*- ................................-----------+-*-*--**----.....~---------------*------------'--'-----+***-*------------*-*
| |
| 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 06/26/19 10:00 9/10/2019 19-09001 EPA 901.1 Modified
| |
| - - - - - - - ...---*----.----**--*-------..* - - - - + - - - - - - - - - ~ - - - * - - - ; - - - - - - - - * - * - - '..... - - - - + * * - - * * - - - * * * * - - - -..*****~------+---------,-------------**--......._________..:..... ...:::........-1 1.52E-01 1.01E-01 u 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 EPA 901.1 Modified 6.71E-02 1.24E-01 u 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 EPA 901.1 Modified 1.80E+OO 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 EPA901.1 Modified 1.24E-01 u 19-:0000--:i::;1* ...... TRG--L-1:102'i"1A-FIGS-001-SB-A 19-09001 EPA 901.1 Modified 1.13E-01 u 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 EPA901.1 Modified 1.16E-01 u
| |
| ------**----------... ----****-------**-*-*-l---**-***--+--*----*--*--*----*----....:....C---**---**---l**-*-----*-****-*-*-+--------'-------+----**-----;-----***'---=:.....-1 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 Lead-210 EPA901.1 Modified 1.43E+OO u
| |
| ----*---**-**+------....:-------!-*--*--***---***---+-*-----**-**-+---------*.........--;----*-********---------------------*-**--*---*..:......::......--1 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 Lead-212 EPA901.1 Modified 2.83E-01 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 Lead-214 3.15E-01 pCi/g l------+--------
| |
| ,_, 19-09001 -17 ________
| |
| ________________ , TRG , ______
| |
| L1-10221A-FIGS-001-SB-A 19-09001 19-09001 Radium-226 u pCVg pCi/g 19-09001-17 j _ _!~G L1-10221A-FIGS-001-SB-A ---+*----------i------'-------'----+-----*+******--*------*,'**------+-------------*---'-------....:........;;:......--1 19-09001-17 . TRG L1-10221A-FIGS-001-SB-A 19-09001 u
| |
| -*--------*-*-*-""""""""\"" --*----.--
| |
| 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 Thorium-234 u 19-09001-17 TRG L1-10221A-FIGS-001-SB-A 19-09001 Thallium-208 EPA901.1 pCVg 19-09001-17 i TRG~10221A-FIGS-001-SB-A 19-09001 Uranium-235 u pCVg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-<letect
| |
| ( ""M>
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 1012112019 11 :34 AM Page 20 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical .. ...
| |
| Zion Solutions SDG:
| |
| Purchase Order: 677118
| |
| *---*-------*---**-*m**--*,--**** *---*-*--+ .-* ,. -*-* -*-*----******-----***-***--
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report Date Analyte Method cu CSU MDA Qualifier ID Type ID Date Date ID Units 19-09001-18 TRG L 1-10221A-FIGS-004-SB-A 06/26/19 10:06 9/3/2019 9/10/2019 19-09001 Actinium-228 2.25E-01 2.26E-01 4.23E-01 19-09001-18 TRG L 1-10221A-FIGS-004-S8-A 06/26/19 10:06 9/3/2019 9/10/2019 19-09001 Silver-108m 6.72E-02 6.72E-02 7.04E-02 u
| |
| -*--*----------*"'"'"'--,-* ----** -------*------: *-*----*-------~--------*---*----*---------
| |
| 19-09001-18 TRG L 1-10221A-FIGS-004-S8-A 06/26/19 10:06 9/3/2019 9/10/2019 19-09001 Americium-241 EPA 901.1 Modified -1.35E-01 9.03E-02 9.05E-02 1.19E-01 u
| |
| *------*-*---*----*-*-----*1'-*--------~~--~-*- -------~---------*-------------- ***-~-----*----- "
| |
| 19-09001-18 TRG L 1-10221A-FIGS-004-S8-A 06/26/19 10:06 9/3/2019 9/10/2019 19-09001 Barium-133 EPA901.1 Modified -8.22E-03 2.87E-02 2.87E-02 1.24E-01 u
| |
| --------*-*-+-------
| |
| 19-09001-18 TRG L 1-10221A-FIGS-004-SB-A 06/26/19 10:06 9/3/2019 9/10/2019 19-09001 Bismuth-214 EPA 901.1 Modified 3.22E-01 1.25E-01 1.26E-01 1.84E-01 L1-10221A-FIGS-004-S8-A 06/26/19 10:06 m-----~-*--***-**---*-*.s*-*-*--'""V-~
| |
| 9/3/2019 9/10/2019 19-09001 Cobalt-60 EPA 901.1 Modified 2.40E-01 7.SOE-02 1.39E-01 19-09001-18 TRG 7.60E-02
| |
| ----------*- -----~---*---**-*-*-----*--*
| |
| 19-09001-18 TRG L 1-10221A-FIGS-004-SB-A 06/26/19 10:06 9/3/2019 9/10/2019 EPA901.1 Modified 8.19E-03 3.50E-02 3.50E-02 1.0SE-01 u 19-09001-18 TRG L 1-10221A-FIGS-004-S8-A 06/26/19 10:06 EPA 901.1 Modified 1.89E-01 8.86E-02 8.92E-02 1.33E-01
| |
| -+-------------**-------*---*--*-*------*----*------------ ....-,
| |
| 19-09001-18 TRG L 1-10221A-FIGS-004-S8-A 06/26/19 10:06 EPA 901.1 Modified 3.38E-02 9.46E-02 9.46E-02 1.76E-01 u 19-09001-18 TRG L1-10221A-FIGS-004-S8-A EPA 901 .1 Modified 1.94E-01 1.94E-01 9.07E-02 u
| |
| ---~------------------------A*A-,-a TRG L1-10221A-FIGS-004-S8-A EPA 901.1 Modified 8.59E-02 8.59E-02 1.30E-01 u 1.13E-01 1.13E-01 7.45E-02 u pCi/g 2.18E-01 3.15E-01 u TRG L1-10221A-FIGS-004-SB-A 19-09001 Potassium-40 EPA901.1 Modified 3.50E+OO 1.34E+OO pCi/g 1--------*-*--------:------'------*---*---------***--*+-------------+------------*--------------*-~-----+--*-------*****
| |
| TRG L 1-10221A-FIGS-004-S8-A 19-09001 9.12E-02 1.41E-01 pCi/g TRG L 1-10221A-FIGS-004-S8-A 8.43E-02 u pCi/g TRG L 1-10221 A-FIGS-004-SB-A Niobium-94 8.08E-02 u L1-10221A-FIGS-004-S8-A 06/26/19 10:06 Lead-210 1.33E+OO u L1-10221A-FIGS-004-SB-A 06/26/19 10:06 Lead-212 EPA 901.1 Modified 2.08E-01 Lead-214 EPA901.1 Modified 2.09E-01 pCi/g 06/26/19 10:06 EPA 901.1 Modified 2.08E-01 u 06/26/19 10:06 EPA901.1 Modified 1.84E-01 pCi/g EPA901.1 Modified 2.67E-01 u pCi/g EPA901.1 Modified 1.16E+OO u EPA 901.1 Modified 3.63E-01 pCi/g 06/26/19 10:06 EPA 901.1 Modified 2.48E-01 3.87E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-<letect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-462!
| |
| | |
| Printed: 10/21/2019 11 :34 AM Page 21 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09001 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order 677118 Final Report of Analysis 2701 Deborah Ave
| |
| ---------------- Analysis Category: _______ ENVIRQt;J~_(~J*,J:r~~
| |
| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 Actinium-228 EPA901.1 Modified 5.16E-01 2.76E-01 2.77E-01 5.44E-01 u pCiig
| |
| '""*----------,- ~-
| |
| 19-09001-19 TRG L1-10221A-FIGS-002-S8-A 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 Silver-108m EPA901.1 Modified -1.43E-03 3.25E-02 3.25E-02 9.18E-02 u
| |
| -------------- - ---- --- --------------------------------------------------+-*v*--,-.-,--,--- *-,---,m-,,_,_ * ---------------- ---------****---------.----------------------------
| |
| 19-09001-19 TRG L 1-10221A-FIGS-002-SB-A 06/26/1910:02 9/3/2019 9/10/2019 19-09001 Americium-241 EPA 901.1 Modlfied -6.68E-02 1.03E-01 1.03E-01 1.42E-01 u 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 **
| |
| * 9/3/2019 9/10/2019 19-09001 ' Barium-133 EPA 901.1 Modlfied 1.83E-02 3.57E-02 3.58E-02 1.67E-01 u 19-09001-19 . TRG*-----------L-1--1-02---2--1----A------F--IG--S--0-0-2--S--B--A---------- ---------------------=------------------------.-**-------------- ----------,--***------------------------ -----------
| |
| 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 Bismuth-214
| |
| ,-~------"-- ____ _.,,., ---------------**---------------------,-------------"-
| |
| EPA 901.1 Modified 1.72E-01 1.73E-01 3.06E-01 u 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 Cobalt-60 EPA 901.1 Modlfied 6.94E-02 6.97E-02 1.63E-01 u
| |
| --------------------------------------------+--------------------------------
| |
| 19-09001-19 TRG L1-10221A-FIGS-002-S8-A 06/26/1910:02 9/3/2019 9/10/2019 19-09001 Cesium-134 EPA 901.1 Modlfied 4.18E-02 4.19E-02 1.21E-01 u
| |
| ---- ----------------------------------------+---------------------------,------------------------------+ ----------,------l----------------------
| |
| 19-09001-19 TRG L1-10221 A-FIGS-002-SB-A 06/26/1910:02 .
| |
| ,____ ,, ___,___ ,,, _ 9/3/2019 9/10/2019
| |
| _ _,a_,_.,,_,_~ 19-09001
| |
| ___._., _ ______ Cesium-137
| |
| _ _ _ _ _, EPA 901.1 Modlfied 1.45E-01 1.SOE-01 1.40E-01 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 Europium-152 EPA 901.1 Modlfied -1.97E-02 1.89E-01 1.89E-01 2.27E-01 u 1-----------*-- '"'"~-------wmcos-------*~"'"'--l-**----------*-*-+
| |
| 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 9.20E-02 1.98E-01 1.98E-01 1.16E-01 u 19-09001-19
| |
| -------------,-- TRG ..__, _______________
| |
| L1-10221A-FIGS-002-S8-A L1-10221A-FIGS-002-SB-A 06/26/19 10:02 06/26/19 10:02 9/3/2019 9/3/2019 9/10/2019 19-09001 9.29E-02 1.20E-01 1.ZOE-01 1.81E-01 u u
| |
| 19-09001-19 TRG ---,-m,-,--,~ : _ _,_,__ ' 9/10/2019 19-09001 -2.42E-02 1.23E-01 1.23E-01 8.34E-02 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 9/3/2019 9/10/2019 19-09001 7.49E-02 7.49E-02 1.14E-01 u
| |
| ----~--------~---------------------'"'" -------"----------
| |
| . 9/3/2019 .
| |
| 19-09001-19 TRG L1-10221A-FIGS-002-SB-A 06/26/19 10:02 9/10/2019 19-09001 1.90E+OO 1.97E+OO 1.44E+OO 19-09001-19 TRG 8.44E-02 1.33E-01 u 6.33E-02 6.33E-02 8.54E-02 u 6.86E-02 6.86E-02 1.06E-01 u pCi/g 1.22E+OO u 2.59E-01 u pCi/g u pCi/g u pCi/g 1.41E+OO u pCi/g 3.15E-01 u 4.52E-01 u pCiig CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonmal Sample;DO=Duplicate Original;U=Non-detect
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| ( ""M>
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| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
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| ~
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| ZS-WM-131 REC'D SEP O3 2019 Revision 0 Information Use ZIONSOLUTIONSrrc An EnergySolu/ions Company 19:-oeoo1 Ll-12201A-AJGS-042-SS-A NA NA SOIL 500 ml 5/9/2018 FULL SUITE MARINELLI I 1300 NA 697.25g L1-12202C-AJGS-042-SS-A NA NA SOIL 500 ml 5/9/2018 FULLSUJTE MARINELLI I 1030 NA 633.95g Ll-1220IC-AJGS-042-SS-A NA NA SOIL 500 ml 5/9/2018 FULL SUITE MARINELLI I 1230 NA 671.0lg NA NA SOIL 500 ml 5/9/2018 FULL SUITE Ll-1220 IB-AJGS-042-SS-A MARINELLI I 1245 NA 782.55g Ll-1211IA-AJGS-040-SS-A NA NA SOIL 500 ml 4/25/2018 FULL SUITE MARINELLI I 0825 NA 746.35g Ll-1220IB-AJGS-040-SS-A NA NA SOIL 500 ml 4/25/2018 MARINELLI I 1013 FULL SUITE NA 931.94g Ll-122020-AJGS-040-SS-A NA NA SOIL 500 ml I
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| 4/25/2018 FULL SUITE MARINELLI 0830 NA 793.65g Ll-12201C-AJGS-040-SS-A NA NA SOIL 500 ml 4/25/2018 FULL SUITE MARINELLI I 1008 NA 625.83g L1-12202C-AJGS-039-SS-A NA NA SOIL 500 ml MARINELLI 4/18/2018 FULL SUITE I 0825 NA 615.18g Ll-12201B-AJGS-039-SS-A NA NA SOIL 500 ml MARINELLI 4/18/2018 FULL SUITE I 0950 NA 786.02g L1-1220IA-AJGS-039-SS-A NA NA SOIL 500 ml MARINELLI 4/18/2018 FULL SUITE I 1005 NA 601.73g Ll-I220IC-AJGS-039-SS-A NA NA SOIL 500 ml MARINELLI 4/18/2018 FULL SUITE 1 0935 NA 628.76g Ll-10221A-FSGS-004-SS-A NA NA SOIL 500 ml MARINELLI 6/6/2019 5ROC HTD 1 1220 NA 698.04g Ll-10221A-FSGS-002-SS-A NA NA SOIL 500 ml MARINELLI 6/6/2019 5ROCHTD 1 1210 NA 798.64g Ll-10221C-FSGS-012-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 5ROCHTD NA 0910 823.06g Ll-10221C-FSGS-013-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 5 ROC HTD NA 0915 774.57g Ll-10221C-FSGS-014-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 0920 5 ROC HTD NA 1013.99g Ll-10221A-FIGS-001-SS-A NA NA SOIL 500 ml MARINELLI I 6/11/2019 5ROCHTD NA 1215 900.99g t Ll-10221A-QIGS-001-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 1215 5ROCHTD NA 932.77g 3 of9
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| . ~
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| REC'D SEP o3 2019 ZS-WM-131 Revision 0 Information Use ZIONSOLUTIONSuc An EnergySo/uiions Company 1tf-0900 1 l( Ll-10221A-FIGS-002-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 1217 5ROCHTD NA 922.34g Ll-10221A-FIGS-003-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 5ROCHTD NA 1219 929.16g LI-1022IA-FIGS-004-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 5 ROC HTD NA 1221 925.96g Ll-102201-FJGS-005-SS-A NA NA SOIL 500 ml MARINELLI 1 7/9/2019 5ROCHTD NA 0830 572.09g Ll-102201-QJGS-005-SS-A NA NA SOIL 500 ml MARINELLI 1 7/9/2019 5 ROC HTD NA 0830 648.58g L1-10221A-FIGS-003-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5 ROC HTD 1 1004 NA 812.22g 17 L1-10221A-FIGS-001-SB-A NA NA SOIL 500 ml MARINELLI 1
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| 6/26/2019 1000 5ROCHTD NA 677.47g Jg Ll-10221A-FIGS-004-SB-A NA NA SOIL 500 ml MARINELLI 1
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| 6/26/2019 1006 5ROCHTD NA 757.61g
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| {? Ll-10221A-FIGS-002-SB-A NA NA SOIL 500 ml MARINELLI I
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| 6/26/2019 1002 5 ROC HTD NA 756.86g Ll-I0221A-QIGS-001-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5 ROC HTD 1 1000 NA 614.42g Ll-1022IA-FJGS-007-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5ROCHTD 1 0856 NA 710.95g Ll-10221B-FJGS-002-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5ROCHTD 1 0830 NA 714.12g Ll-1022IA-FJGS-002-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5ROCHTD I 0846 NA 771.65g Ll-10221A-FJGS-00I-SS-A NA NA SOIL 500 ml MARINELLI I 6/17/2019 5ROC HTD NA 0844 707.40g Ll-10221A-FIGS-005-SS-A NA NA SOIL 500 ml MARINELLI 1 6/13/2019 SROC HTD NA 0745 774.76g Ll-10221A-FIGS-006-SS-A NA NA SOIL 500 ml MARINELLI 1 6/13/2019 5ROCHTD NA 0747 783.08g Ll-10221A-FIGS-007-SS-A NA NA SOIL 500 ml MARINELLI 1 6/13/2019 5 ROC HTD NA 0749 708.49g Ll-I0221A-FIGS-008-SS-A NA NA SOIL 500 ml MARINELLI 1 6/13/2019 5ROCHTD NA 794.16g 0751 Ll-1022IA-FIGS-009-SS-A NA NA SOIL 500 ml MARINELLI 1 6/13/2019 5 ROC HTD NA 774.52g 0753 4 of9
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| REC'D SEP O5 2019
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| ~
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| ZS-WM-131 Revision 0 Information Use ZIONSOLUTIONSru An EnergySolutions Company 19*09001 Ll-1022ID-FIGS-021-SS-A NA NA SOIL 500 ml MARINELLI 5 ROC HTD Ll-10221D-FIGS-OOI-SS-A NA NA SOIL 500 ml MARINELLI 5 ROCHTD Laboratory: Date Submitted To Lab: Ship Container No.: Cooler Temperature: FULL SUITE EBERLINE LABS NA NIA Date Time: Date: (mm/dd/yyyy):
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| ~ft: ):
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| Relinquished by:
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| l)vf)
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| Relinquished by: Date Time:
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| (mm/dd/yyyy):
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| Comments 9 of9
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| EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD
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| * EBERLINE OAK RIDGE, TENNESSEE 37830
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| ~ ANALYTICAL PHONE (865) 481-0683 FAX (865) 483-4621 EBS-OR-46231 October 22, 2019 Patricia Giza Zion Solutions, LLC 101 Shiloh Blvd Zion, IL 60099 CASE NARRATIVE Work Order# 19-09012-0R SAMPLE RECEIPT This work order contains sixteen soil samples received 09/03/2019. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.
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| CLIENT ID LAB ID CLIENT ID LAB ID Ll-1022 lA-FJGS-002-SS-A 19-09012-04 Ll-10221 C-FIGS-103-SS-A 19-09012-12 Ll-1022 lA-FJGS-001-SS-A 19-09012-05 L 1-10221B-FIGS-102-SS-A 19-09012-13 Ll-1022 lA-FIGS-005-SS-A 19-09012-06 Ll-10221B-FIGS-103-SS-A 19-09012-14 Ll-1022 lA-FIGS-006-SS-A 19-09012-07 Ll-1022 lB-FIGS-l 04-SS-A 19-09012-15 Ll-1022 lA-FIGS-007-SS-A 19-09012-08 L 1-1022 lB-FIGS-105-SS-A 19-09012-16 Ll-1022 lA-FIGS-008-SS-A 19-09012-09 Ll-10221 D-FIGS-005-SS-A 19-09012-17 L 1-1022 lA-FIGS-009-SS-A 19-09012-10 Ll-1022 lD-FIGS-006-SS-A 19-09012-18 Ll-1022 lB-FIGS-l 00-SS-A 19-09012-11 Ll-1022 lD-FIGS-007-SS-A 19-09012-19 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.
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| Gamma Spectroscopy was performed using EPA Method 901.1 Modified.
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| Laboratory qualifiers are as follows:
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| U - Result is less than the MDA.
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| ANALYTICAL RESULTS Combined Standard Uncertainty is reported at 1-sigma value.
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| Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
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| Page 1 of 3
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| ANALYTICAL RESULTS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were then mounted on 47mm filters. Filters were reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.
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| Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are reported from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.
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| TRITIUM A representative aliquot of each sample was equilibrated with tritium free water. Equilibrates were transferred into a round-bottomed distillation flask and attached to a single stage still. A pottion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.
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| Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique.
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| Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.
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| NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into an appropriately sized beaker. Stable elemental Nickel carrier was added to each sample prior to digestion.
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| Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.
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| Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.
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| GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.
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| Page2of3
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| ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as reported. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228, Bismuth-214 and Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.
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| CERTIFICATION OF ACCURACY I ce1tify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her desi~i::_ee to be accurate as verified by the following signature.
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| M.R. McDougall Laboratory Manager Date: 10/22/2019 Eberline Analytical wants and encourages your feedback regarding our perfonnance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.
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| Page 3 of 3
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| Printed: 10/21/2019 12:02 PM Page 1 of 21 Report To: Worl< Order Details:
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| Patricia Giza 19-09012 Eberline Analytical Zion Solutions Purchase Order:
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| SDG:
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| 677118 Final Report of Analysis 2701 Deborah Ave
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| *-----------,--~ __ Ana/ysis._Category: ___ ENV.1_.13Qt:-JMEt\J1~~---***
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| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Analysis Batch Report Date Analyte Method Result cu CSU MDA Qualifier ID Type ID Date ID Units 19-09012-01 LCS KNOWN 10/1/2019 Tritium LANL ER-210 Modified 2.08E+02 7.48E+OO pCi/g 19-09012-01 LCS SPIKE 10/1/2019 Tritium LANL ER-210 Modified 2.04E+02 7.87E+OO 1.39E+01 5.89E+OO pCi/g
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| ********-------+-------,-,,-,--,,,,,,,,,.. ----------~- ------------*-*-------~-----------~---------t 19-09012-02 MBL BLANK 10/1/2019 Tritium LANL ER-210 Modified 1.33E+OO 3.38E+OO 3.38E+OO 5.79E+OO U pCi/g
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| **-*,****-----* ------------*-*********--*--*,--* ******--*--***--***-+-----***-*--------+---*******----*-***********-*--*--*----**---*--------**** -----*--*-----
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| 19-09012-03 DUP L1-10221A-FJGS-002-SS-A 06/17/19 08:46 10/1/2019 19-09012 Tritium LANL ER-210 3.24E+OO 3.47E+OO 3.48E+OO 5.82E+OO U
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| *******--****-----***** ____..,... l--*-*******-***---;.*-------***--****----------*-****-
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| 19-09012-04 . DO L1-10221A-FJGS-002-SS-A 06/17/19 08:46 10/1/2019 19-09012 Tritium LANL ER-210 Modified 5.14E+OO 3.53E+OO 3.54E+OO 5.81E+OO U
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| ********-*--*-*****--************-**-------*-*** -********----******* -*---1*---*-*------0----*------**-**-~-----*-..*---------+---***--*-****--*----********** **'*********-*-*******-****** ***'**---------+-**-*----------*---***-*****----**--*--*----1 19-09012-05 TRG L1-10221A-FJGS-001-SS-A ____o~~1_?~9 08:~- , 9/3/2019 .. __10/1/2~~ __19-09012 ____T LANL ER-210 Modified
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| __n_*t_iu_m*-****-+----*-***---------*---*+- 2.69E+OO 3.47E+OO 3.48E+OO 5.86E+OO U pCi/g 19-09012-06;_T._~_G*.- ....-.* - _-_-_L*1=--_1*0_2_21_A_-_F_IG_S_-o_os_*:~~:~~=~~ 06/13/19 07:45
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| * 9/3/2019
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| * 10/1/2019 19-09012 Tritium LANL ER-210 Modified 3.03E+OO 3.44E+OO 3.44E+OO 5.78E+OO U 19-09012-07 TRG L1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 10/1/2019 19-09012 Tritium LANL ER-210 Modified 4.00E+OO 3.50E+OO 3.SOE+OO 5.82E+OO u 19-09012-08 ' . TRG L1-10221A-FIGS-007-SS-A 06/13/1907:49 10/1/2019 19-09012 Tritium LANL ER-210 Modified 3.06E+OO 3.48E+OO 3.48E+OO 5.8SE+OO u 19-09012:°-9 *--- !~_9__ L1-1022:~_:~IGS-008-_SS-l:_______1___0_6_.*1_13_1_19_07__:5_1.__, _________1_0_11_12_0_1_9_0 _ _19-09012 _ _ _ _ _ _. *, .
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| Tritium LANL ER-210 Modified -1.88E-01 3.30E+OO 3.30E+OO 5.73E+OO
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| ----*---..J------********----****+-*-----*--;--,.-----**.--**--*-----*-*----**---"-**-------****---'-*** u 19-09012-10 TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 19-09012 Tritium LANL ER-210 Modified 4.53E+OO 3.48E+OO 3.49E+OO 5.76E+OO u 19-09012-11 TRG L1-102218-FIGS-100-SS-A 05120119 09:55 19-09012 Tritium LANL ER-210 Modified 2.99E+OO 3.40E+OO 5.71E+OO u pc*
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| ********-************-***-**--------------******-**-- **----*-**+--*---------+,-------*- -----*-*--***-*****; ... -----**-*--*+-----------*----+-----***--*-*-i-------'**-******---------*----------------..:..-
| |
| 19-09012-12 ... *........:~~ __':.1_:.10221C-FIGS-!°-~:SS-A __ 07/08/19 12:47 19-09012 Tritium LANL ER-210 Modified 1.86E-01 3.28E+OO 5.68E+OO u 19-09012-13 TRG L1-102218-FIGS-102-SS-A 07/08/19 13:10 19-09012 Tritium LANL ER-210 Modified 2.03E+OO 3.32E+OO 3.32E+OO 5.62E+OO u 19-09012-14 TRG L1-102218-FIGS-103-SS-A 07/08/19 13:12 10/1/2019 19-09012 Tritium LANL ER-210 Modified 5.61E+OO u 19-09012-15 07/08/19 13:14 10/1/2019 19-09012 Tritium LANL ER-210 Modified 5.SSE+OO u 19-09012-16 10/1/2019 19-09012 Tritium LANL ER-210 Modified 5.47E+OO u 19-09012-17 10/1/2019 19-09012 Tritium LANL ER-210 Modified 5.56E+OO u 19-09012-18 TRG L1-102210-FIGS-006-SS-A 10/2/2019 19-09012 Tritium LANL ER-210 Modified S.57E+OO u 19-09012-19 TRG L1-102210-FIGS-007-SS-A 10/2/2019 19-09012 Tritium LANL ER-210 Modified SASE+OO u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
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| ( ~
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| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 2 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave ..... AnalysisCategory: ENVIRONMENTAL ,_,,_,, ____
| |
| Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09012-01 LCS KNOWN 09/05/19 00:00 9/3/2019 10/1/2019 19-09012 Nickel-63 pCi/g 19-09012-01 09/05/19 00 :00 9/3/2019 LCS SPIKE 10/1/2019 19-09012 Nickel-63 3.29E+OO pCi/g 19-09012-02 BLANK 09/05/19 00:00 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 6.96E-01 1.86E+OO 1.86E+OO 3.17E+OO u pCi/g a-*,------
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| 19-09012-03 L1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.85E+OO 2.01E+OO 201E+OO 3.37E+OO u 19-09012-04 DO L1-10221 A-F JGS-002-SS-A 06/17/19 08:46 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 2.14E+OO 2.03E+OO 2.03E+OO 3.39E+OO 19-09012-05 TRG L1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.18E+OO 1.95E+OO 1.95E+OO 3.30E+OO
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| *------*-*---------------*------ --------'>------------------------------~--,----- -;--~-----------
| |
| 19-09012-06 TRG L1-10221A-FIGS-005-SS-A 06/13/19 07:45 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified O.OOE+OO 1.84E+OO 1.84E+OO 3.17E+OO
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| ___19-09012-07 TRG L1-10221A-FIGS-006--SS-A 06/13/19 07:47 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.85E+OO 1.85E+OO 3.14E+OO 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.93E+OO 1.93E+OO 3.30E+OO
| |
| --------~-- -------"*------------------- ---------~------------------- ----------
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| 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.12E+OO 2.01E+OO 2.01E+OO 3:40E+OO
| |
| -*----"--*-.,**---------,-,----------*-"~~-----
| |
| 19-09012-10 TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 2.51E+OO 1.97E+OO 1.98E+OO 3.27E+OO 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified -3.27E-01 2.29E+OO 2.29E+OO 3.97E+OO -09012-12~ . TRG ' L1-10221C-FIGS-103-SS-A --"'---*-* --------
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| 07/08/19 12:47 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 2:41E+OO 1.96E+OO 1.96E+OO 3.26E+OO
| |
| -----"',-----------,- -c--c 19-09012-13 TRG L1-10221 B-FIGS-102-SS-A 07/08/19 13:10 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 2.14E+OO 3.61E+OO 19-09012-14 TRG L1-10221 B-FIGS-103-SS-A 07/08/19 13:12 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.88E+OO 3.18E+OO
| |
| --~---,-------------------. *----*-
| |
| L1-10221B-FIGS-104-SS-A 07/08/19 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.93E+OO 3.34E+OO L1-10221 B-FIGS-105--SS-A 07/08/19 13:16 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.89E+OO 3.25E+OO L1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 2.05E+OO 3:40E+OO
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| * - - - - - >----*-'*-------~ . --"--' ---*--
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| 19-09012-18 TRG L1-102210-FIGS-006--SS-A 07/08/19 12:32 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 1.96E+OO 3.34E+OO
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| ---------,-----*---~*--,-----
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| 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07/08/19 12:34 ! 9/3/2019 10/1/2019 19-09012 Nickel-63 ASTM 3500-Ni Modified 2.08E+OO 3.49E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non--detect
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| ( ""M>
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 3 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order:.. **-*--* ......... 677118 ...... _.._.........- .................................
| |
| Final Report of Analysis 2701 Deborah Ave .... . Analysis_Category: ......~_NV_IRONMENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09012-01 LCS KNOWN 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified pCVg
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| 'n,-w,,,--*
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| 19-09012-01 LCS SPIKE 09/05/19 00:00 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified ........_ ..___.____ 1.78E+01 7.98E-01 pCi/g 19-09012-02 MBL BLANK 09/05/19 00:00 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM
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| ...................-*+-........_ .....____ SRW01 Modified
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| ... ___ . _ _....... 5.10E-01 3.02E-01 3.50E-01..... ______ 5.89E-01 U pCi/g
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| ------ ------*-"~--, '------ ' ---.
| |
| 19-09012-03 DUP.....-,_ ..L....1..-.:92_2_1A_-_F::l9S-~~~--s_s_-_A _0~171~9-_o~:4_6_ .. _9-'.'.~/~~1.9-...._~0_12_12_0_1_9_1~.:~~91_~- Strontium_-9_0-,_E__ 1C__h._r..o..M_....s_R_w_o_1_M_o.*d...i_fi..e_d**-'<-------...............................3.*.3...o_E_-_o..._1........-3....:4
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| .._2_E
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| __-0_1______._6_.7._7_E__
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| -0__1 u *---- pCVg L1-10221A-FJGS-002-SS-A 06/17/1908:46 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified' -8.57E-02 3.21E-01 3.23E-01 6.96E-01 U
| |
| ..... _________________ ........ *----*-**------*****----- ................................_. _ _ _ _ _ -*--** ---* ................ ___ _. ......... _ .. ;.........C.-..J 19-09012-05 TRG L1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified 1.84E-01 3.14E-01 3.21E-01 6.52E-01 U
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| ---***---***--**-*--* ***** ------**-*- ----------*******--- - -----*--**-----*******- ***---**--***----*---------..*-----** ................... ., ...... *- - *------* *-*------*---*--*-----** -*~-*------*-***----**-**-*'---'--!
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| 19-09012-06 TRG L1-10221A-FIGS-005-SS-A 06/13/19 07:45 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified 3.72E-01 2.98E-01 3.25E-01 5.95E-01 U
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| - - - - - - - - - * - * - , '
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| 19-09012-07 TRG L1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified 2.98E-01 3.21E-01 3.37E-01 6.52E-01 U
| |
| ---------***--*-- *------------- -------* -----------~--,-.,---,~-- **------*----------------,------------------..----;-------------*----*-----------*----..*--+------------*-----*-**-***--*-****----..... _;___:_.......-1 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified 2.59E-02 3.45E-01 3:45E-01 7.33E-01 U
| |
| -*--------+--------..-----**..**-*--.;.-..- -------*----,-
| |
| 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified 2.55E-01 3.46E-01 3.57E-01 7.11E-01 U
| |
| -*---*-*- .....................................-.. .. .------J***-***-------*-*--****-*---*--*-------*---*--*-------..*-*--+---*-**--------*****-0---*--------*--..*-*--**---*-** ......----*-*-..*-*-*-**-**--*-- --------'--'-''----!
| |
| 19-09012-10 TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 10/2/2019 19-09012 Strontium-90 EIChroM SRW01 Modified 3.39E-01 4.09E-01 4.26E-01 8.38E-01 U
| |
| ____... . -*-*-****...*. *****s----*-*------*. **--*-**----l---.. **--*-------*-<-*-***----------*----------****-*--**---*--*----+-------*---------**--+------*----*----*~-----***----..-*-----*-**-**-*--*---------'..-.C..:::..--1 19-09012-11 TRG L1-10221 B-FIGS-100-SS-A 06/20/19 09:55 10/2/2019 19-09012 Strontium-90 1.42E-01 3.82E-01 3.85E-01 8.01E-01 U 19-09012-12 TRG L1-10221C-FIGS-103-SS-A 07/08/1912:47 10/2/2019 19-09012 Strontium-90 3.73E-01 3.20E-01 3.45E-01 6.40E-01 19-09012-13 TRG L1-10221 B-FIGS-102-SS-A 07/08/19 13:10 9/3/2019 10/2/2019 3.67E-01 3.88E-01 7.44E-01 u
| |
| *-----------~-------
| |
| 19-09012-14 TRG L1-10221B-FIGS-103-SS-A 07/08/19 13:12 10/2/2019 3.58E-01 3.63E-01 7:47E-01 u 19-09012-15 TRG L1-10221B-FIGS-104-SS-A 07/08/19 13:14 10/2/2019 2.86E-01 2.87E-01 6.10E-01 u 1----------*-*-*--,---*-
| |
| 19-09012-16 TRG L1-10221B-FIGS-105-SS-A 07/08/19 13:16 10/2/2019 3.12E-01 3.17E-01 6.50E-01 u 19-09012-17 TRG 3.61E-01 3.67E-01 7.52E-01 u 6.01E-01 u pCVg 5.52E-01 u 19-09012-01 LCS KNOWN Cobalt-60 5.10E+OO pCi/g 19-09012-01 KNOWN Cesium-137 3.39E+OO pCi/g 19-09012-01 LCS SPIKE Cobalt-60 1.02E+01 1.25E+01 9.61E-01 19-09012-01 LCS SPIKE Cesium-137 9.07E+OO 1.00E+01 1.09E+OO pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 101211201912:02 PM Page 4 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions ___ ,_ ----
| |
| Purchase___Order:
| |
| SDG:
| |
| 677118
| |
| --- ''""""------*------ - "'"-"'-' -----,-w, _
| |
| Final Report of Analysis 2701 Deborah Ave
| |
| ....,. -*-- _ . , Analysis Category: ______
| |
| ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so I '
| |
| Lab Sample Client Sample Receipt Analysis Batch ' Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date , Date Date ID Units
| |
| __ 1_9_:CJ_~12-,0_2_____,____M__B__L____ ,,B._LAN, ____K*---------- 09/05/19 00:00 : 9/3/2019 9/10/2019 19-09012 Actinium-228 EPA 90U Modified 2.49E-02 7,21E-02 ' 7,21E-02 U4E-01 U pCi/g
| |
| **sii;;~~:ios.;;-* *u-----
| |
| 1 19-09012-02 MBL BLANK 09,05,19 00:00 91312019 9110,2019 19-09012 - ~-EP--A-901.1M~~'=-~-** ~-~-~9~~:_oi-:-_-_2_-:0_6_E_-0_2___2_:0 __
| |
| 6~~0~~~~-3.-31-E--02.~. pci~
| |
| c-- *19-09012-02 ., MBL BLANK 09/05/19 00:*o--o*-*r***9,-/--3/*2*0-*1**-9*--c-*-9-/1*0*-,2-o-*1-9 19-09012 Amelicium-241 EPA 901.1 Modffied -5.66E-02 4.02E-02 4.03E-02 5.25E-02 U pCi/g
| |
| **------*------------*- --------*-+----*-------*-"'---------"""'"'"''""'''""Y""'**-----1----*-----*------*-------
| |
| _:1_~:Cl_~°.2~:_CJ.~-- . -~B~---~-K___ ---*-*-------------.._09_10~1_1_9 00:00 _ 9/3/2019 91_19!~-~:9_ _ .: 9.::~~_CJ:1_2_ --- Ba~':':.!~- EPA 901. 1 Modifi<e~ _ --- -1 05E-02 3.04E-02 3.04E-02 3.97E-02 U pCi/g 19-09012-02 MBL**--*----B_LA ____N-K__________,,,.,, 09/05/19 _o_o__:_o__o_,__9.i_3__,2_0_19__,-,_9_J_10_,_20.._1_9"'"" 19-09012 Bismuth-214 EPA 901.1 Modified 3.81E-02 4.31E-02 4.32E-02 7.73E-02 U pCi/g
| |
| __1_9__ -o_9__0___
| |
| 12,__-0_2~-------M*_B__L______,.______
| |
| B_LA_N_K____ -______,._________ -___ *------1-0-9--10__5_11_9_0_0:..o__o____+'_,9_13_12_0_1_9_, __9_11_0_,2_01_9_______1__9__ --0_90-__1_2_ -----c_o_b_a_tt-_6_0_ __~~~~:,'.,~-~!!ied _ "------1_.2__4__E,--o,_2,____ -_2_.1_3_E_-0_2_;_2_._13_E_-0_2__________3_,__ o7_E_-_0__2,______ u_____________.:,P_Ci/:.g____--1 1 1 1 19-09012-02 MBL BLANK 09/05/1900:00 ; 9/3/2019
| |
| * 9/10/2019 19-09012 Cesium-134 EPA901.1 Modified 3.48E-03
| |
| * 2.40E-02 1 2.40E-02 2.93E-02 U pCi/g
| |
| .. :1~:°.~o~~~--*---~~~-,--BLA __ ~~ ----------------1--0_91_05__119 __ __0,_o_:o_o___,* ..._91_3_120,,1__
| |
| 9 ____9_1_11_o_,2__0
| |
| __1__9,, _____19-09012 Cesiu':1::2:3_~-- ___ EPA_901._:1 Modified___
| |
| * 2,99E-03
| |
| * 1.81 E-02 1,81 E-0__ 2_-,,_-___
| |
| 3,9___1E__-0____2__*--------*--- u
| |
| __ __ ,_______,, _____P_Cii_g_____,
| |
| 19-09012-02 MBL BLANK 09/05/1900:00 , 9/3/2019
| |
| * 9/10/2019 19-09012 Europium-152 EPA901.1 Modified 1.79E-02
| |
| * 8.29E-02 8,29E-02 5.86E-02 U pCi/g
| |
| --------------------------------------------,-l----------------*-+-----------------,----------------'-----1-----------------------------,,.,,,______________________________ , , _ _ _ _ _ ,,____---------------'---"----l 19-09012-02 MBL BLANK 1 09/05/19 00:00 ' 9/3/2019 9/10/2019 19-09012 Europium-154 EPA 901. 1 rvl~~e.~4_.__6_9E___-_02______,.___ 7_,o_7E_-_02_~,-7_.0_8_E-_o-2______2_ ..,9___4__E
| |
| __-__o-2_ _ _u pCi/g 19-09012-02 MBL BLANK 09/05/19 00:00 i 9/3/2019 9/10/2019 19-09012 Europium-155 EPA901.1 Modified -1.52E-02 2.90E-02 2.91E-02 4.09E-02 U pCi/g
| |
| """" --------------*-*-**--" ----*--*-----------*---*-,.*----,---+----,-------+---,---+--- __,_ ------*-*-**--0*------"---*--'--*-----"----------*--~---------,-----,,-----1 19-09012-02 MBL BLANK 09/05/19 00:00 : 9/3/2019 9/10/2019 19-09012 Holmium-166m EPA 901.1 Modified -1.47E-02 4.09E-02 ; 4.09E-02 3.16E-02 U pCi/g l--19--09_0_______,_M ___B__L_____,___ B_LA,,,N--K------------ "" ,,,________ , __, __0,_9_/0-5/_1_9_00~-9/3~. 9110-,2-019 . 19-09012 ' lodine-129,-t-__ ,___ E_P_A_9_01-.1-_M,o__d_ifi-,e--d*---,-G--6-.4_6,-E**--0-2~--1.-09-E--0-1---i---1-.1""0E"--01_______1___6_5E--'0"'1" -----"""u"'"'""'"___:__pC__i_/g"----l
| |
| ,______ ------"""'"**-*--~---,------*-----* ---*----~.-----+-- ----*--*----------1---------------------------------~----------i-----'---,,,____,,_ _ _ _,_
| |
| 19-09012-02 MBL BLANK 09/05/1900:00 . 9/3/2019 9/10/2019 19-09012 I Potassium-40 EPA901.1 Modffied 1 4.95E-01 3,12E-01
| |
| * 3.13E-01 7,81E-01 U pCi/g
| |
| -------- .------1-----------------*+------------------+----+---------------'---------'-"----I 19-09012-02
| |
| * MBL BLANK 09/05/1900:00 9/3/2019 9/10/2019 19-09012 Manganese-54 EPA901.1 Modified 3.56E-03
| |
| * 2.02E-02 2.02E-02 4,09E-02 U pCilg
| |
| ~---------*---- '. ,----* ----*----------~ ~ ----'-------+----------,--'----------------0....-----',------------------------,----------'--_;;,_--'1 19-09012-02 MBL BLANK 09/05/1900:00 i 9/3/2019 9/10/2019 19-09012
| |
| * Molybdenum-93 EPA901.1 Modified , -L02E-03 1.01E-02 ' 1.01E-02 2.99E-02 U pCi/g 19-09012-02 MBL ____ B_LAN_K________________ --+-0-9-,0-51_19_00:00"'" 9/3/2019 9/1012019 "-19-09012 i--N:.io-b-iu-m--9-4-l------E-P_A__9_01___ 1 -M-od-ifi-,e*d----',--_-3_-8_2__E___
| |
| o3-,'----2.os-E--02--'-*--2-,o-8E'---02___.;;:3'-_2--5::.E_*-o-2----------u*------,-,__c:_pc"'i:..::/g:....-1
| |
| !----------*- --------------- - -----<------'--------,- ---------~----------------------i------f---------------------*''"""'___:__:_;;:..__--'I 19-09012-02 MBL BLANK 09/05/19 00:00 9/3/2019 9/10/2019 19-09012 Lead-210 EPA 901.1 Modffied i 3.70E-01 ' 4,21E-01
| |
| * 4.21E-01 6,60E-01 U pCi/g
| |
| --',-------+-------------~--------------,--r------+----------------'---"'--1 19-09012-02 MBL , BLANK 09/05/19 00:00 9/3/2019 i 9/10/2019 19-09012 Lead-212 EPA 901.1 Modified 3.27E-02 , 2,93E-02 ' 2.94E-02 5.17E-02 U pCi/g J - - - - - - - - - - - , - - - - - - - ' - - - - - - - - - - - - - - - - - , - - , - - - - - - - - - - - - - - - , , - ~ - - - - - + - - - - - - - - - , - - - - - - - - * - - - - - - - - + * - - - - - - - - - - . . ; . . , , _ , ,______i----------+------------'------"--.:::____ ,
| |
| t--1_9_-0_9_0_12_-o-.2__,! ___ M_B_L_____+-__ B_LA_N_K--.--------------,--0-9.1_0_51_1_9_oo:oo i 9/3/2019 9/10/2019 19-09012 Lead,-_2_14__ -+___E_P__A_9_0_1._1__M_o_difi_e_d__+-__11._06E_-02_i,___4.68_E-_02__-i--- 4,6_8E-_02....._1_ ,5_1_ E-0_2-~__u__,_,.__ _,_PC'-il_;;g:__~
| |
| 19-09012-02 MBL BLANK 09/05/19 00:00 9/3/2019 9/10/2019 ; 19-09012 : Promethium-145 EPA901.1 Modified -4.08E-02
| |
| * 7.12E-02 7,12E-02 , 1.01E-01 U pCi/g 1--1-9--0--9-0-12--0-2--i)*--M-B_L_,______ B__LA_N_K____________+-_0_9_/0-5/_1__ 9_00-:0-0-<---9-/3-/2-0-1-9--;--9/-1-0/-20-1-9~--19-09012 Radium-226 EPA 90U Modified 3.81E-02 4,31 E-02 4,32E-02 7,73E-02 U pCi/g 1---------~*---------------------+--------+------+----,--- -"------+------------,,--------+----+---------------+------I 19-09012-02 ; MBL BLANK 09/05/1900:00 9/3/2019 9/10/2019 19-09012 Antimony-125 EPA901.1 Modified 1.21E-02 2,75E-02 2,75E-02 R58E-02 U pCi/g 19-09012-02 i MBL 1-----.:------,----------------"--I---------
| |
| BLANK 09/05/1900:00 9/3/2019 9/10/2019 19-09012 Thorium-234 EPA901.1 Modified 4,09E-01
| |
| ------+---,--:--.:--t---:-:-:--:-:--:--------,-t---:::-:--:--:+----_;,_----,-------,------------'---=---'I 3,05E-01 3,06E-01 4,96E-01 ' U pCi/g 19-09012-02 , MBL
| |
| * BLANK 09/05/19 00:00 9/3/2019 1 9/10/2019 19-09_0_1_2_,-_Th_a_mu_m_-_20_8_,,1---E_PA_90_1_.1_M_o_d_ifi__ ,e_d_______1_1.1_0E_-02--._1. __
| |
| '.8_4E_-02_,_1_r,_85E_-02_ _ _ 1,18_E-0_11_____u_____ ._P_C_ii_g_--1 19-09012-02 ; MBL , BLANK 09/05/1900:00 9/3/2019 i 9/10/2019 19-09012 Uranium-235 EPA901.1 Modified -3.29E-02 9,91E-02 9.91E-02 1.44E-01 U pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 5 of 21 Report To: Worn: Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical ** ****nm.-----*-----**v*n* *
| |
| * Zion Solutions SDG:
| |
| Purchase****-*-----_,
| |
| Order: _____________
| |
| 677118
| |
| '"""'"'" _____""""~---*- ,,_
| |
| --------*---- ,,-rn _ _ _
| |
| Final Report of Analysis 2701 Deborah Ave
| |
| "''"""=---------------
| |
| Analysis Category:_ . ENVIRONMENTAL v-v- ---"-'
| |
| Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier 19-09012-03 DUP L1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Actinium-228 EPA 901.1 Modified 5.38E-01 1.61E-01 1.64E-01 2.71E-01 19-09012-03 DUP L1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Silver-108m EPA 901.1 Modified 4.82E-02 4.83E-02 5.ZOE-02 u 19-09012-03 19-09012-03 DUP DUP L 1-10221A-FJGS-002-SS-A L 1-10221 A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Americium-241
| |
| ; 9/3/2019 _ 9/10/2019 ____ 19-09012 _, ___ Barium-133 EPA 901.1 Modified EPA 901.1 Modified 3.73E-02 O.OOE+OO 9.39E-02 3.09E-02 9.39E-02 3.09E-02 1.26E-01 8.53E-02 u
| |
| u 19-09012-03 DUP L1-10221A-FJGS-002-SS-A 9/3/2019 9/10/2019 Bismuth-214 EPA 901.1 Modified 4.0SE-01 1.06E-01 1.0SE-01 1.75E-01
| |
| -----------,,*----*-*"""'""' " ' " _ ,_ _ _ _ v v m " " " " - * - - - * - - v m e
| |
| * v ***-+-------~--**--*---*--
| |
| 19-09012-03 DUP L 1-10221A-FJGS-002-SS-A 9/3/2019 9/10/2019 EPA901.1 Modified 1.07E-01 4.63E-02 4.66E-02 8.72E-02 19-09012-03 DUP L 1-10221A-FJGS-002-SS-A 9/3/2019 9/10/2019 EPA901.1 Modified 2.29E-02 2.29E-02 5.49E-02 u 19-09012-03 DUP L 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 EPA 901.1 Modified 6.79E-01 1.11E-01 1.16E-01 7.96E-02 19-09012-03 DUP L 1-10221 A-F JGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 EPA 901.1 Modified 3.53E-02 1.31E-01 1.31E-01 1.63E-01 u 19-09012-03 DUP L1-10221A-FJGS-002-SS-A 9/3/2019 9/10/2019 EPA 901.1 Modified 8.96E-03 1.35E-01 1.35E-01 8.31E-02 u 19-09012-03 . DUP L1-10221A-FJGS-002-SS-A 06/17/19 08:46 : 9/3/2019 9/10/2019
| |
| ,v,m-*,-s-------,,m,_,.,
| |
| EPA901.1 Modified 4.04E-03 9.38E-02 9.38E-02 1.22E-01 u 19-09012-03 DUP L 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Holmium-166m EPA 901.1 Modified 3.0SE-02 6.SSE-02 6AOE-02 u 19-09012-03 DUP L 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019
| |
| _,_, 19-09012 lodine-129 EPA901.1 Modified 3.02E+OO u
| |
| ------~---*
| |
| 19-09012-03 DUP L1-10221A-FJGS-002-SS-A 06/17/19 08:46 ! 9/3/2019 9/10/2019 19-09012 Potassium-40 EPA 901.1 Modified 1.82E+OO 7.40E-01 19-09012-03 DUP
| |
| ,-------,----~--------------
| |
| L 1-10221A-FJGS-002-SS- 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Manganese-54 EPA 901.1 Modified 7.40E-02 u 19-09012-03 DUP L1-10221A-FJGS-002-SS-A -06/17/19 08:46 9/3/2019 9/10/2019 19-09012 ; Molybdenum-93__ EPA901.1 Modified 3.97E-02 u 19-09012-03 DUP 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Niobium-94 5.34E-02 u 19-09012-03 L 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Lead-210 EPA 901.1 1.92E+OO u L 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 j Lead-212 EPA901.1 1.69E-01 06/17/19 08:46 9/3/2019 9/10/2019 19-09012! Lead-214 EPA901.1 2.06E-01 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 i Promethium-145 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Radium-226 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Antimony-125 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Thorium-234 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 i Thallium-208 06/17/19 08:46 9/3/2019 9/10/2019 ' 19-09012 Uranium-235 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 1012112019 12:02 PM Page 6 of 21 Report To. Worf< Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical *-***---*-
| |
| Zion Solutions m*w 0
| |
| SDG:
| |
| Order:
| |
| 677118 Final Report of Analysis 2701 Deborah Ave
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| *--*~*-----** -*------***
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| Analysis Category:
| |
| ~------ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch : Report ID Type ID Date Date Date ID
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| * Analyte Method Result cu CSU MDA Qualifier Units 19-09012-04 _., DO
| |
| ,, l 1-10221A-FJGS-002-SS-A w, _ _ _ _ _ _ _ _ _ , _ _ _ _ _ _ _ _ -----*-****
| |
| 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Actinium-228 EPA 901.1 Modified 4.25E-01 1.78E-01 1.80E-01 3.45E-01 pCi/g 19-09012-04 DO l 1-10221 A-F JGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Silver-108m EPA901.1 Modified -2.10E-02 4.17E-02 4.18E-02 5.01E-02 u pCi/g
| |
| ~ - - - - '.---~-----*---------*----*---------** - -------=*" --***-------- **-*-* *-----*--*-----------,----,--****- **--- *----
| |
| 19-09012-04 DO L 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Americium-241 EPA 901.1 Modified -1.28E-02 9.44E-02 9.44E-02 1.21E-01 u pCi/g
| |
| ------~--------.-----*---*- -*-----..----------~---- -*-- -*---=* w **--"*---*----
| |
| 19-09012-04 DO l 1-10221 A-F JGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Barium-133 EPA 901.1 Modified 1.48E-03 2.96E-02 2.96E-02 7.55E-02 u pCi/g
| |
| *----""" _ _ _ ,
| |
| * m e " " " * * * - - * = = , - - - - - * - - - --------*-----**
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| 19-09012-04 DO l 1-10221 A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-090 Bismuth-214 EPA901.1 Modified 4.34E-01 1.19E-01 1.21E-01 1.75E-01
| |
| *-------- **-- "--**~-- -.,-.-----"------**
| |
| "" --*--*-----*---;---. i 19-09012-04 DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 : Cobalt-60 EPA901.1 Modified 1.25E-01 4.98E-02 5.02E-02 9.17E-02 pCi/g 19-09012-04 DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Cesium-134 EPA 901.1 Modified -1.51E-02 2.39E-02 2.40E-02 5.72E-02 u pCi/g 19-09012-04 DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 i Cesium-137 EPA 901.1 Modified 6.28E-01 1.04E-01 1.09E-01 7.49E-02 pCi/g 19-09012-04 DO l1-10221. r -- -- ~'.::
| |
| * 06/17/19 08:46 ; 9/3/2019 9/10/2019 19-09012 * =***--'**- :.s2 EPA901.1 Modified -2.94E-02 . 1.77E-01 1.77E-01 1.55E-01 u pCi/g 19-09012-04 ' DO l 1-10221 A-F JGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 i <=,*---'**- ~.s EPA901.1 Modified -1.70E-02 1.28E-01 1.28E-01 8.06E-02 u *pcitg -
| |
| 19-09012-04 DO i l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 i 9/3/2019 9/10/2019 19-09012 , =~~--'**- "': EPA 901.1 Modified 1.10E-01 9.01E-02 9.02E-02 1.23E-01 u pCi/g 19-09012-04 DO ' l 1-10221 A-F JGS-002-SS-A 06/17/19 08:46 i 9/3/2019 9/10/2019 19-09012 j Holmium-166m EPA901.1 Modified -8.47E-04 ! 6.76E-02 6.76E-02 6.37E-02 u pCi/g 19-09012-04 DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 i 9/3/2019 9/10/2019 19-09012 , lodine-129 EPA901.1 Modified 2.20E+OO ' 9.51E+OO 9.51E+OO 3.02E+OO u pCi/g 19-09012-04 DO l1-10221. r---- ~'.::' 06/17/19 08:46 i 9/3/2019 9/10/2019 , 19-09012 : Potassium-40 EPA901.1 Modified 1.29E+01 1.84E+OO i 1.96E+OO 1.02E+OO pCi/g
| |
| **----~-~---
| |
| 19-09012-04 DO i l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019
| |
| * 19-09012 ! Manganese-54 EPA901.1 Modified r.78E-03 : 4.16E-02 ! 4.16E-02 6.67E-02 u pCi/g 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 : Molybdenum-93 EPA901.1 Modified -9.58E-03
| |
| . u 19-09012-04 DO l 1-10221A-FJGS-002-SS-A
| |
| ----+-------- ; .. -*--- : 3.50E-02 3.50E-02 5.14E-02 i pCi/g 19-09012-04 / DO i l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019 9/10/2019 19-09012 Niobium-94 EPA901.1 Modified 3.13E-03 ! 3.07E-02 i 3.07E-02 5.57E-02 u pCi/g
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| - **- -- : i 19-09012-04 ! DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 ' 9/3/2019
| |
| * 9/10/2019 , 19-0901 -210 EPA 901.1 Modified 3.64E-01 1.14E+OO 1.14E+OO 1.78E+OO u pCi/g
| |
| .. i 19-09012-04 DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 ! 9/3/2019 , 9/10/2019 19-0901 212 EPA901.1 Modified 3.70E-01 8.22E-02 8.44E-02 1.47E-01 pCi/g 19-09012-04 DO l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 : 9/3/2019
| |
| * 9/10/2019 19-09012 t lead-214 EPA901.1 Modified 4.50E-01 i 1.25E-01 t 1.27E-01 i 1.98E-01 pCi/g 19-09012-04 ! DO i l 1-10221 A-F JGS-002-SS-A 06/17/19 08:46 l 9/3/2019 9/10/2019 19-09012 i Promethium-145 EPA901.1 Modified 8.62E-01 ! 7.49E-01 ! iE-01 9.33E-01 u pCi/g 19-09012-04 DO I l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 1 9/3/2019 9/10/2019 19-09012 !
| |
| --+i Radium-226 EPA 901.1 Modified 4.34E-01 i 1.19E-01 1.21E-01 1.75E-01 pCi/g 19-09012-04 DO i l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 i 9/3/2019 9/10/2019 : 19-09012 Antimony-125 EPA901.1 Modified -8.35E-02 ! 1.05E-01 i 1.05E-01 1.53E-01 u pCi/g 19-09012-04 DO ' l1-10221' c1r::<:Jln?.<'<'
| |
| * 06/17/19 08:46 i 9/3/2019 9/10/2019 19-09012 i Thorium-234 EPA 901.1 Modified 3.60E-01 ! 9.21E-01 9.22E-01 1.24E+OO i u : pCi/Q 19-09012-04 DO i l 1-10221A-FJGS-002-SS-A 06/17/19 08:46 9/3/2019
| |
| -9/3/2019 9/10/2019 19-09012 jThallium-208 EPA .1 Modified 1.43E-01 I 6.15E-02 6.19E-02 9.03E-02 pCi/g 19-09012-04 ! DO l 1-10221A-FJGS-002-SS-A 06117/19 08:46 9/10/2019 19-09012 i Uranium-235 EPA 901.1 Modified -1.06E-02 I 2.88E-01 2.88E-01 3.74E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 101211201912:02 PM Page 7 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical > , v* ---*-**---mm,m**"Sv-s*-
| |
| Zion Solutions SDG:
| |
| Purchase Order: 677118
| |
| *--*------------*"-~-------"- -- -V*--------* *"''""' ""' --- **"'""'"-----*------.------*--**-*---*-*
| |
| Final Report of Analysis 2701 Deborah Ave . Analysis Category: ENVIRONMENTAL
| |
| ""'' ---*-- ------*-"'"'""rn*--"' '"'- -*-*--,--,~---*-*
| |
| Zion, IL 60099 Sample Matrix.* so Lab Sample Client Sample Receipt Analysis Batch Report Date Date ID Analyte Method Result cu CSU MDA Qualifier Units ID Type ID Date 19-09012-05 TRG L1-10221 A-F JGS-001-SS-A 06/17/19 08:44 9/3/2019 9/10/2019 19-09012 Actinium-228 EPA901.1 Modified 3.07E-01 3.09E-01 5.98E-01
| |
| " -- -----*--*--- ----------*-~-----*-*-
| |
| 19-09012-05 TRG L1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 9/10/2019 19-09012 Silver-108m EPA 901.1 Modified 8.26E-02 8.26E-02 9.82E-02 u 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 9/10/2019 19-09012 Americium-241 EPA 901.1 Modified -8.15E-02 1.06E-01 1.06E-01 1.47E-01 u
| |
| --------- **,-we~*----------,-~---------*-- -----*---*
| |
| 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 9/10/2019 19-09012 Barium-133 EPA 901.1 Modified -2.96E-02 2.85E-02 2.86E-02 1.63E-01 u 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 9/10/2019 19-09012 Bismuth-214 EPA901.1 Modified 3.39E-01 1.59E-01 1.60E-01 4.10E-01 u 19-09012-05 TRG L1-10221A-FJGS-001-SS-A 06/17/19 08:44 9/3/2019 19-09012 Cobalt-60
| |
| -------- _____ __ --*-*- EPA901.1 Modified 1.39E-01 6.65E-02 6.69E-02 2.10E-01 u
| |
| ----------=------------------------ _,
| |
| 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A 06/17/19 08:44 . Cesium-134 EPA 901.1 Modified 2.27E-02 1.30E-01 u
| |
| -*-----*-** .................... *************-*--****--*--------** -**---+--**-------*-***--+----->----~--****-**.;.-***-***-**** ****---**----!-------*-**-*+-*-*----**---***----*****-***-**--+-------****----------*-****--*-**--**-,*--:........;:c..--t 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A EPA 901.1 Modified 3.14E-01 2.01E-01
| |
| -**---* .......+----*-**----**-******si------***---,s*****-*----******-*--*--*-*****-*1-------------**-***_)**--**---**--*-*~*-**-*-*--*S--*--*----*-**************-**-***--*****---,.****,.***-*-****--'-=--***--1 19-09012-05 TRG EPA901.1 Modified 8.36E-02 1.28E-01 1.29E-01 2.29E-01 u 19-09012-05 TRG L1-10221A-FJGS-001-SS-A 06/17/19 EPA 901.1 Modified -8.13E-02 2.12E-01 2.12E-01 1.16E-01 u
| |
| *----*---------*******--------*----**-**--+*-----***-***-----+--------*--..c._---*--*~--------*--***-'---_.:'-***--*--*+-*---****-*--*--------**-,***----*****-*s--
| |
| 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A EPA901.1 Modified 9.43E-03 1.26E-01 1.85E-01 u 19-09012-05 TRG L1-10221A-FJGS-001-SS-A EPA901.1 Modified 1.36E-01 1.29E-01 8.26E-02 u 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A EPA901.1 Modified -2.12E-02 1.16E-01 u 19-09012-05 TRG L1-10221A-FJGS-001-SS-A EPA901.1 1.36E+01 1.20E+OO 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A 06/17/19 08:44 EPA 901.1 Modified -9.68E-03 1.43E-01 u 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A EPA 901.1 Modified 1.29E-02 7.37E-02 u 19-09012-05 TRG L 1-10221 A-F JGS-001-SS-A EPA901.1 Modified -7.32E-02 7.84E-02 u 19-09012-05 ___----1--**
| |
| TRG , _ ___ ______
| |
| _,,. " L 1-10221A-FJGS-001-SS-A Lead-210 EPA901.1 Modified 1.30E+OO u 19-09012-05 TRG L1-10221A-FJGS-001-SS-A Lead-212 2.73E-01 pCi/g 19-09012-05 L1-10221A-FJGS-001-SS-A Lead-214 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A Radium-226 EPA901.1 Modified u 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A Antimony-125 EPA901.1 Modified u 19-09012-05 TRG L1-10221A-FJGS-001-SS-A Thorium-234 EPA 901.1 Modified 2.35E+OO u 19-09012-05 TRG L 1-10221A-FJGS-001-SS-A Thallium-208 EPA901.1 Modified 1.72E-01 19-09012-05 TRG L1-10221A-FJGS-001-SS-A 19-09012 Uranium-235 EPA901.1 Modified 4.87E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 8 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical *--------*-s--v-'**-*~*--**=---
| |
| " Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave v--""-""-"""-------~-~--m"-""v**
| |
| __ Analysis Category: __ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Sample Client Sample Receipt Analysis Batch Report ID Date Date ID Analyte Method Result cu CSU MDA Qualifier Type Date Units TRG L 1-10221A-FIGS-005-SS-A Actinium-228 EPA 901.1 Modified 5.92E-01 2.11E-01 2.13E-01 3.07E-01 19-09012-06 TRG L1-10221A-FIGS-005-SS-A Silver-108m EPA 901.1 Modified -2.27E-02 5.66E-02 5.66E-02 6.62E-02 u
| |
| '""""~-----*-----*-------***----. ------*
| |
| 19-09012-06 TRG L1-10221 A-Fl GS-005-SS-A EPA901.1 Modified 2.79E-03 2.97E-02 2.97E-02 1.09E-01 u
| |
| -*---*--*--"-*---------------""'"-'"--"""""'""*--m*"
| |
| 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A 06/13/19 07:45 Barium-133 EPA 901.1 Modified 1.99E-02 3.05E-02 3.05E-02 1.17E-01 u 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A 06/13/19 07 :45 EPA901.1 Modified 4.07E-01 1.32E-01 1.34E-01 1.83E-01 19-09012-06 TRG L1-10221A-FIGS-005-SS-A 06/13/19 07:45 EPA 901.1 Modified 8.58E-02 6.59E-02 6.61E-02 1.29E-01 u 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A 06/13119 07:45 -1.17E-02 3.52E-02 3.53E-02 9.32E-02 u pCi/g 19-09012-06 L 1-10221A-FIGS-005-SS-A 06/13119 07:45 1.50E-01 7.32E-02 7.36E-02 1.10E-01 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A 9/10/2019 -8.47E-02 1.74E-01 1.74E-01 1.64E-01 u 19-09012-06 TRG L1-10221A-FIGS-005-SS-A 9/10/2019 -1.42E-01 1.93E-01 1.94E-01 8.27E-02 u
| |
| ~----**-*--"'*:.c--------------*-----------~--*
| |
| 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A 9/10/2019 EPA901.1 Modified 5.63E-02 6.93E-02 6.94E-02 1.17E-01 u 19-09012-06 TRG L 1-10221 A-FIGS-005-SS-A 9/10/2019 EPA 901.1 Modified -5.87E-02 9.25E-02 6.79E-02 u 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A EPA 901.1 Modified 2.00E-01 2.87E-01 u
| |
| . EPA901.1 Modified 1.40E+01 3.02E+OO 1.83E+OO 19-09012-06 TRG 19-09012-06 EPA901.1 Modified 1.47E-02 5.27E-02 9.03E-02 u 19-09012-06 EPA901.1 Modified 7.84E-02 u EPA901.1 Modified 7.75E-02 u Lead-210 EPA901.1 Modified 1.36E+OO u Lead-212 EPA 901.1 Modified Lead-214 u pCi/g pCi/g L 1-10221A-FIGS-005-SS-A 9/10/2019
| |
| * u 19-09012-06 TRG L1-10221 A-FIGS-005-SS-A 06/13/19 07:45 9/3/2019 9/10/2019 pCi/g 19-09012-06 TRG L1-10221A-FIGS-005-SS-A 06/13/19 07:45 ! 9/3/2019 ; 9110/2019 19-09012 I Thallium-208 pCi/g
| |
| ----~- ---t---
| |
| Uranium-235 u pCi/g 19-09012-06 TRG L 1-10221A-FIGS-005-SS-A 06/13/19 07:45 9/3/2019 9/10/2019 19-09012 I CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 1012112019 12:02 PM Page 9 of 21 Report To: Worl< Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical ****-******
| |
| Zion Solutions SOG:
| |
| Purchase Order: 677118
| |
| -- ---~--* " ***---*-*
| |
| Final Report of Analysis 2701 Deborah Ave __ _ Analysis Category:*- ENVIRONMENTAL so Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date Analyte Method Result cu CSU MDA Qualifier ID Units 19-09012-07 TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 ; Actinium-228 EPA 901.1 Modified
| |
| ' -8.65E-02 2.87E-01 2.87E-01 4.48E-01 u pCi/g
| |
| -*-*
| |
| * w _ m_ _ _ ' " " "
| |
| '""*-*----,,-*-*---------**-------~*--~"'
| |
| 19-09012-07 TRG L1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 Silver-108m EPA901.1 Modified -1.82E-02 6.96E-02 6.96E-02 9.45E-02 u pCi/g
| |
| *--*---------~*-'""i*"*-------**--***-------**-**--*--"""-----------~"---*- -*----------*---*-* ---- ,--------oc*-- ~
| |
| 19.09012-07 TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 Americium-241 EPA 901.1 Modified -4.67E-02 ; 9.91E-02 9.92E-02 1.38E-01 u pCi/g
| |
| ----*----- * ----*------*------***---------*-*--*We*
| |
| 19-09012-07 : TRG l 1-10221 A-F IGS-006-SS-A 06/13/19 07 :4 7 9/3/2019 9/10/2019 19-09012
| |
| * Barium-133 EPA901.1 Modified 2.14E-01 1.09E-01 1.09E-01 1.66E-01 u pCi/g 19-09012-07 TRG L1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 Bismuth-214 EPA 901.1 Modified 4.52E-01 1.52E-01 1.54E-01 2.73E.Q1 pCi/g
| |
| ---*-*---*-*--*---*-*-~*~***-**------*---------- '
| |
| 19-09012-07 , TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 Cobalt-60 EPA 901.1 Modified l 2.92E-01 8.31E-02 8.44E-02 1.24E-01 pCi/g 19-09012-07 ; TRG L 1-10221A-FIGS.006-SS-A
| |
| -"-----"---~ *-*----w='--
| |
| 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 Cesium-134 EPA 901.1 Modified -7.13E-03 2.50E-02 2.50E-02 1.12E-01 u pCi/g 19-09012-07 TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 Cesium-137 EPA 901.1 Modified 9.35E-01 1.62E-01 1.69E-01 1.75E-01 pCi/g
| |
| ----- '"'"-------~-----------------
| |
| 19-09012-07 TRG L 1-10221A-FIGS-006-SS-A
| |
| ""=*-,----------------------
| |
| __. 06/13/19 07:47 , 9/3/2019 9/10/2019 19-09012 '. -
| |
| L.Ul ..... l"',.,.,:1-1.JL EPA 901.1 Modified 1.21E-01 1.90E-01 1.90E-01 2.35E-01 u pCi/g 19-09012-07 TRG L1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 i Cu, . . . l"' ..... 11- 54 EPA 901.1 Modified -1.28E-01 2.02E-01 2.03E-01 1.23E-01 u pCi/g 19-09012.07 , TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 9/10/2019 19-09012 I ~,..u ..... r--,-*11- .55 EPA 901.1 Modified 2.50E-02 1.16E-01 1.16E.01 1.72E-01 u pCi/g 19-09012-07 , TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 I 9/3/2019 9/10/2019 19-09012 ! Holmium-166m EPA 901.1 Modified -4.86E-02 1.31E-01 1.31E-01 8.13E-02 u pCi/g 19.09012-07 ' TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 ; 9/3/2019 9/10/2019 19-09012 i lodine-129 EPA 901.1 Modified 4.09E-03 7.72E-02 7.72E-02 1.14E-01 ; u pCi/g 19-09012-07 TRG """'""" ____ ________________
| |
| L 1-10221 ..A-FIGS-006-SS-A 06/13/19 07:47 ; 9/3/2019 9/10/2019 ' 19-09012 Potassium-40 EPA901.1 Modified 8.63E+OO
| |
| ' 1.81E+OO 1.86E+OO 1.79E+OO pCi/g 19-09012-07 ! TRG l 1-10221A-FIGS-006-SS-A 06/13/19 07:47 l 9/3/2019 9/10/2019 , 19-09012 i .,_, *~-* *--- ...... EPA901.1 Modified 3.02E-02 ' 8.64E-02 8.64E-02 1.46E-01 ; u pCi/g 19-09012.07 ; TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 ; 9/3/2019 , 9/10/2019 19-09012 *""- --
| |
| M EPA901.1 Modified 2.85E-02 i 5.29E-02 5.29E-02 8.51E-02 ; u pCi/g 19-09012-07 i TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 : 9/10/2019 ' 19-09012 : Niobium-94 EPA 901.1 Modified 3.27E-03 7.25E-02 7.25E-02 1.05E-01 u pCi/g 19-09012-07 : TRG L 1-10221A-FIGS-006-SS-A
| |
| -- 06/13/19 07:47 '---- : -----,
| |
| ; 9/3/2019 9/10/2019 I 19-09012 .
| |
| --+------*--
| |
| Lead-210 EPA901.1 Modified 9.95E-02 I 8.04E.01 8.04E-01 1.18E+OO u pCi/g
| |
| ; 06/13/19 07:47 --,
| |
| 19-09012-07 ; TRG L 1-10221A-FIGS-006-SS-A 9/3/2019 9/10/2019 19-09012 I Lead-212 EPA 901.1 Modified 5.03E-01 1.46E-01 : 1.48E-01 2.46E-01 pCi/g 19-09012-07 TRG L1-10221A-FIGS.006-SS-A 06/13/19 07:47 I 9/3/2019 9/10/2019 19-09012 1 Lead-214 EPA 901.1 Modified 5.22E-01 i 1.53E-01 : 1.56E-01 2.49E-01 pCi/g 19-09012-07 TRG L 1-10221A-FIGS-006-SS-A 06/13/19 07:47 ! 9/3/2019 9/10/2019 I 19-09012 l Promethium-145 EPA 901.1 Modified -5.09E-02 l 9.38E-02 : 9.38E-02 1.32E-01 u pCi/g 19-09012-07 TRG L 1-10221A-FIGS.006-SS-A 06/13/19 07:47 f 9/3/2019 9/10/2019 19-09012 'i Radium-226 EPA901.1 Modified 4.52E-01 l 1.52E-01 1.54E-01 2.73E-01 pCi/g 19-09012.07 ; TRG
| |
| *-* L1-10221A-FJGS-006-SS-A ~------
| |
| 06/13/19 07:47 ___--4 ___ 9/3/2019 9/10/2019 19-09012 _j Antimony-125 EPA 901.1 Modified -1.56E-01 2.30E-01 2.30E-01 2.93E.01 I u ; pCi/g
| |
| """' /'\i'\I'\~: /'\~ ; TRG L1-10221 A-FIGS-006-SS-A ____
| |
| 06/13/19 07:47 ......,,.__i 9/3/2019 9/10/2019 19-09012 i ' Thorium-234 EPA901 Modified 2.90E-01 : 8.99E-01 8.99E-01 1.34E+OO I u pCi/g 19-09012-07 [ TRG ' l 1-10221A-FIGS-006-SS-A 06/13/19 07:47 T
| |
| 9/3/2019 9/10/2019 19-09012 ! Thallium-208 EPA 901.1 Modified 4.49E-01 i 1.42E-01 1.44E-01 1.58E-01 pCi/g 19-09012.07 i TRG L1-10221A-FIGS-006-SS-A 06/13/19 07:47 9/3/2019 l 9/10/2019 i 19-09012 I Uranium-235 EPA901.1 Modified 3.80E-01 i 2.98E-01 2.98E.01 4.75E-01 \ u I pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("MJ EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 860/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/2019 12:02 PM Page 10 of 21 Report To: Wori< Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118 Final Report of Analysis 2701 Deborah Ave Analysis _Category: _ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 19-09012 Actinium-228 1.66E-01 3.42E-01 pCi/g 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/1907:49 9/3/2019 9/11/2019 19-09012 Silver-108m EPA901.1 Modified 2 07E-02 3.41E-02 3.41E-02 5.44E-02 u pCi/g
| |
| -------* -----,-* *-*"--*--------------- *-**------. ,,_,___,~*~"'-----=---------- -* ---- ,. ---- - - - - -
| |
| * 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 19-09012 Americium-241 EPA901.1 Modified 1.14E-01 9.95E-02 9.96E-02 1.42E-01 u
| |
| -----=~---- --0------- -s----~---------,,,-*- *----------- ----------*+**-***--*********-***
| |
| 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 19-09012 Barium-133 EPA 901.1 Modified 1.47E-02 3.84E-02 3.84E-02 7.25E-02 u pCi/g 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 19-09012 Bismuth-214 EPA 901.1 Modified 4.77E-01 1.08E-01 1.11E-01 1.67E-01
| |
| ****-******-*********-*****-****** .. ********-*-*- ****--**-----*--*-** *-*-****-*-*---****-*---------*------**---**-*----+----******
| |
| 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/1907:49 9/3/2019 9/11/2019 19-09012 Cobalt-60 EPA 901.1 Modified 5.65E-02 5.93E-02 5.93E-02 1.07E-01 u
| |
| ***-*--***---**-----************---****+*----***-***---yo-** **--*--**-**--*--+**---------
| |
| 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 9/3/2019 9/11/2019 19-09012 Cesium-134 EPA 901.1 Modified -8.23E-03 2.37E-02 2.37E-02 5.50E-02 u
| |
| .......*----~----------,----*<<--------------------,----- *-*------------*-- "
| |
| 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 19-09012 Cesium-137 EPA 901.1 Modified 2.87E-01 8.26E-02 8.39E-02 1.04E-01 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07 :49 9/3/2019 9/11/2019 EPA901.1 Modified -2.92E-02 2.07E-01 2.07E-01 1.90E-01 u 19-09012-08 ' TRG . L1-10221A-FIGS-007-SS-A. . 06/13/19 07:49 9/3/2019 9/11/2019 EPA 901.1 Modified 3.25E-02 1.16E-01 1.16E-01 9.49E-02 u
| |
| ***--*----**-******------******-*****----*-----*****-----.+----~-----**---*-**-----,**-----*-----*-;...*-*****'***-**----+----*----***-**---+----*-******,***-**----*------*-----**----*--*--****---*******-**-*--*-*--.:.........:::...... -1 19-09012-08 **--** TRG ___ ~0221..J:FIGS-007:~~~---* 06/13/19 07:49 9/3/2019 9/11/2019 EPA901.1 5.71E-02 1.03E-01 1.03E-01 1.38E-01 u 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 EPA 901.1 Modified -4.26E-02 8.31E-02 8.31E-02 7.34E-02 u 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/3/2019 9/11/2019 EPA 901.1 Modified 4.39E+OO 1.84E+01 1.84E+01 3.41E+OO u 19-09012-08 TRG L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/11/2019 EPA 901.1 Modified 9.29E+OO 1.51E+OO 1.58E+OO 8.40E-01
| |
| ------------------~<<--------------
| |
| 19-09012-08 . TRG , L1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/11/2019 EPA 901.1 Modified -1.83E-03 4.74E-02 4.74E-02 7.38E-02 u 19-09012-08 TRG l 1-10221A-FIGS-007-SS-A 06/13/19 07:49 9/11/2019 EPA 901.1 Modified 1.60E-03 4.05E-02 4.05E-02 6.32E-02 u 06/13/19 07 :49 9/11/2019 EPA 901.1 Modified 4.04E-02 4.04E-02 6.33E-02 u L1-10221A-FIGS-007-SS-A Lead-210 EPA 901.1 Modified 1.99E+OO 1.08E+OO 1.09E+OO 2.29E+OO L1-10221A-FIGS-007-SS-A Lead-212 EPA901.1 Modified 3.67E-01 9.14E-02 9.34E-02 1.97E-01 L1-10221A-FIGS-007-SS-A Lead-214 EPA901.1 Modified 4.60E-01 1.25E-01 1.93E-01 L1-10221A-FIGS-007-SS-A EPA901.1 Modified 8.78E-01 8.33E-01 9.63E-01 u L1-10221A-FIGS-007-SS-A Radium-226 EPA 901.1 Modified 4.77E-01 1.11E-01 1.67E-01 L1-10221A-FIGS-007-SS-A 5.54E-02 1.00E-01 1.77E-01 u L1-10221A-FIGS-007-SS-A Thorium-234 1.40E+OO u pCi/g L1-10221A-FIGS-007-SS-A 1.41E-01 L1-10221A-FIGS-007-SS-A 2.89E-01 3.80E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/2019 12:02 PM Page 11 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118 Final Report of Analysis 2701 Deborah Ave .... ___ Analysis ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date Analyte Method Result cu CSU MDA Qualifier ID Units 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Actinium-228 2.83E-01 2.85E-01 5.19E-01 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Silver-108m 6.72E-02 6.72E-02 8.93E-02 u 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Americium-241 EPA 901.1 Modified -5.79E-02 9.74E-02 9.74E-02 1.36E-01 u
| |
| '""'"", *---v-,--,~----,--**-- '.---m----*-"-**-------*------------
| |
| 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Barium-133 EPA 901.1 Modified . -2.25E-03 3.53E-02 . 3.53E-02 1.SOE-01 u 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Bismuth-214 EPA 901.1 Modified 4.29E-01 1.29E-01 1.31E-01 2.02E-01
| |
| *--**----*-""'"'""""""' ---*-*--*---*---------* -*------*----*---*-- . -*-------***-***-*-----**-****----**---*--**-***-*-*-*****-**---*--***-** ****--*----+-*-----*---------***--**********-*-i***--*--**-**
| |
| 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Cobalt-60 EPA 901.1 Modified 5.09E-02 9.40E-02 9.40E-02 1.59E-01 u
| |
| "'"""*----*-<---- *--*--*-"""""' "*-**- ---*-~-----*--<*-----------*----*- *-----~--------------*-~t--- mn,-,---*--*---*--v---*,
| |
| 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 Cesium-134 EPA901.1 Modified 7.34E-03 3.64E-02 3.64E-02 1.07E-01 u 19-09012-09 TRG L1-10221A-FIGS-008-SS-A _________________
| |
| 06/13/19 07:51 ----------
| |
| 9/3/2019___.___9/11/2019 19-09012 EPA 901.1 Modified 3.48E-01 1.22E-01 1.23E-01 1.72E-01 19-09012-09 TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/3/2019 9/11/2019 19-09012 EPA 901.1 Modified -7.16E-02 1.90E-01 1.90E-01 2.23E-01 u 19-09012-09 TRG ~-L1_-_10_2_2'.~_::'.I_G_s_-o_o_s-.s_s_-_A_ _ __ _ 06/13/19 07:~/3/2019 . 9/1112019 -~~?.~.1.~-' ,. EPA901.1 Modified 7.57E-02 2.02E-01 Euro_p*_,u_m_-1_5_4_+-**-**-*-*-----**-**-**---,--------*-**--*-**--*--- 2.02E-01
| |
| __ .___________ u 1_.1_3_E_-_0_*1**-******-*---*----...:.---''--I
| |
| . 19-09012-09 . TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 ; 9/3/2019 9/11/2019 19-09012 Europium-155 EPA 901.1 Modified 1.25E-01 1.10E-01 1.10E-01 1.82E-01 u
| |
| *******---*-*-*------- 06/13/19 07:51 : 9/3/2019 . 9/11/2019 ' Holmium-1._66-m-;----***-*---******---*---*,*--*----*****-,---**---*--*----*-***-**--***-******7****-.9-6*-E**_**o-2***--*--------*-***--f 19-09012-09 TRG L1-10221 A-FIGS-008-SS-A EPA 901.1 Modified 3.24E-02 1.29E-01 1.29E-01 u TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 9/11/2019 lodine-129 EPA901.1 Modified -3.70E-02 7.48E-02 7.49E-02 u 19-09012-09 -t-- TRG : L1-10221A-FIGS-008-SS-A . 06/13/19 07:51 9/11/2019 Potassium-40 EPA901.1 Modified 1.32E+01 2.11E+OO 2.21E+OO
| |
| --,--,,~-, "
| |
| *--**--*--+*---*-*-----i----~***-----+-----.;--------**--+*---********--*----+***-*-**-*---i---------*-'--
| |
| TRG L1-10221A-FIGS-008-SS-A 06/13/19 9/11/2019 EPA 901.1 Modified 8.14E-02 8.14E-02 u TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 EPA 901.1 Modified 6.11E-03 6.58E-02 6.58E-02 u TRG EPA 901.1 Modified 6.14E-02 u TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 1.16E+OO u TRG L1-10221A-FIGS-008-SS-A 06/13/19 07:51 2.06E-01 pCi/g L1-10221 A-FIGS-008-SS-A 06/13/19 07 :51 2.34E-01 pCi/g u pCi/g pCi/g u pCi/g EPA901.1 Modified 9.06E-01 1.35E+OO pCi/g EPA 901.1 Modified 1.63E-01 1.48E-01 pCi/g 9/3/2019 9/11/2019 EPA 901.1 Modified 3.09E-01 4.49E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-462!
| |
| | |
| Printed: 10/21/201912:02 PM Page 12 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| **-------- *-----*"*--*"""*---~---* ****--*---**------*--"=* ----*------------ ---** ..
| |
| Final Report of Analysis 2701 Deborah Ave .. .. "'"*-- ***- - . Analysis Category: ... ENVIRONMENTAL
| |
| - - * - - " ~ - - - - - - - * - - - - "'""°'"' - * - * *
| |
| * Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09012-10 : TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Actinium-228 EPA 901.1 Modified ' 6.87E-01 1.91E-01 1.95E-01 2.91E-01 19-09012-10 , TRG L 1-10221 A-FIGS-009-SS-A 06/13/19 07,53 9/3/2019 9/11/2019 ! Silver-108m EPA901.1 Modified 5.28E-03 2.16E-02 2.16E-02 7.48E-02 u pCi/g
| |
| *****-** --~--------*- ***----**---*-*--*-- .. - -**----*-** -~--- ***--------*- *- ***------~- ,... ----
| |
| 19-09012-10 ; TRG L1-10221 A-FIGS-009-SS-A 06/13/19 07 ,53 9/3/2019 9/11/2019 19-09012 Americium-241 EPA 901.1 Modified 2.41E-02 4.32E-02 : 4.32E-02 1.03E-01 u pCi/g 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Barium-133 EPA 901.1 Modified -9.57E-03 4.20E-02 4.20E-02 1.11E-01 u pCi/g
| |
| -**- ***-----------*---*-,,,-----:--------**.---~---------------- ,--- **-
| |
| 19-09012-10 : TRG L 1-10221A-FIGS-009-SS-A
| |
| *******-* _,,,_ _________~-----------------------------*"---
| |
| 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Bismuth-214 EPA 901.1 Modified ! 4.58E-01 1.43E-01 1.45E-01 1.59E-01 pCi/g 19-09012-10 ' TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Cobalt-60 EPA901.1 Modified l 1.20E-01 5.91E-02 5.94E-02 1.05E-01 pCi/g 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 : Cesium-134 EPA901.1 Modified i -1.45E-02 1.SOE-02 : 1.SOE-02 8.67E-02 u pCi/g 19-09012-10 : TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/1112019 19-09012 Cesium-137 EPA901.1 Modified 5.42E-01 1.20E-01 1.23E-01 1.43E-01 pCi/g 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 ' 9/3/2019 9111/2019 19-09012 -~v, *c --*- EPA901.1 Modified 3.93E-02 ' 1.78E-01 1.78E-01 1.58E-01 u pCi/g 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 -~"'"~'""' ,v
| |
| - EPA901.1 Modified : 2.43E-02 2.06E-01 2.06E-01 8.30E-02 u pCi/g 19-09012-10 ! TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07 :53 9/3/2019 9/11/2019 19-09012 i ~"'-c -*
| |
| *ss EPA901.1 Modified 4.18E-02 : 8.19E-02 8.19E-02 1.23E-01 u
| |
| ------~----------*--*-*----------- 1 --
| |
| 19-09012-10 , TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07 :53 9/3/2019 9/11/2019 19-09012 Holmium-166m EPA901.1 Modified i -4.02E-02 7.00E-02 7.00E-02 7.33E-02 u pCi/g
| |
| ------- '-*-=,- *-----
| |
| 19-09012-10 TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 : 9/3/2019 9/11/2019 19-09012 lodine-129 EPA901.1 Modified 2.44E-01 ' 2.17E-01 2.17E-01 3.14E-01 u pCi/g 19-09012-10 TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 , Potassium-40 EPA901.1 Modified i 9.01E+OO i 2.02E+OO 2.07E+OO 7.16E-01 pCi/g 19-09012-10 \ TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Manganese-54 EPA 901.1 Modified 5.02E-02 6.55E-02 : 6.55E-02 1.18E-01 u pCilg 19-09012-10 l TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 f 9/3/2019 9/1112019 19-09012 i ...., ""'
| |
| no EPA 901.1 Modified -1.65E-02 ' 4.50E-02 4.50E-02 6.98E-02 u pCi/g 19-09012-10 , TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07 :53 i 9/3/2019 ' 9/11/2019 19-09012 Niobium-94 EPA901.1 Modified 5.78E-03 4.51E-02 ; 4.51E-02 6.65E-02 u pCi/g 19-09012-10 : TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Lead-210 EPA 901.1 Modified 1.20E+OO 8.25E-01 8.28E-01 1.29E+OO u pCi/g 19-09012-10 TRG L 1-10221 A-FIGS-009-SS-A 06/13/19 07 :53 f 9/3/2019 ' 9/1 19-09012 Lead-212 EPA 901.1 Modified 3.06E-01 9.00E-02 i 9.14E-02 19E-01 pCi/g 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 9/11/2019 19-09012 Lead-214 EPA 901.1 Modified
| |
| ' 4.18E-01 1.18E-01 i 1.19E-01 1.82E-01 pCi/g 1: ---* 1,* .. c TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 1 9/3/2019 9/11/2019 19-09012 Promethium-145 EPA 901.1 Modified : 1.58E-02 1.36E-01 U6E-01 2.01E-01 u pCi/g 19-09012-10 TRG : L 1-10221A-FIGS-009-SS-A 06/13/19 07 :53 9/3/2019 , 9/11/2019 19-09012 i Radium-226 EPA 901.1 Modified 4.58E-01 1.43E-01 1.45E-01 1.59E-01 pCilg 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 913/2019 ' 19-09012 ' Antimony-125
| |
| .. EPA901.1 Modified -9.24E-02 , 1.68E-01 1.68E-01 2.15E-01 u pCi/g 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07 :53 9/3/2019 ~9/11/2019 : 19-09012 ' Thorium-234 EPA901.1 Modified 5.84E-01 6.28E-01 6.29E-01 1.05E+OO u pCilg 19-09012-10 TRG L 1-10221A-FIGS-009-SS-A 06/13/19 07:53 : 9/3/2019 i 9/11/2019 ) 19-09012 Thallium-208 EPA901.1 Modified 3.03E-01 2.23E-01 ' 2.23E-01 3.SOE-01 u ' pCilg 19-09012-10 TRG L1-10221A-FIGS-009-SS-A 06/13/19 07:53 9/3/2019 i 9/11/2019 : 19-09012 Uranium-235 EPA 901.1 Modified 2:07E-01
| |
| ' 2.39E-01 ! 2.40E-01 3.74E-01 u
| |
| * pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 1012112019 12:02 PM Page 13 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions....... .._____ ,,, ,,,,, ..........., ........... .. Purchase Order:
| |
| SDG:
| |
| ___ , __ , a _ , _ , _ * * * * ' - ' ' ' ' " - ' , _ , , '
| |
| 677118 Final Report of Analysis 2701 Deborah Ave __ Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09012-11 _ TRG L1-102218-FIGS-100-SS-A
| |
| '-*-------""""""~---------*-
| |
| 06/20/19 09:55 9/3/2019 9/11/2019 19-09012 Actinium-228 EPA 901.1 Modified 2.62E-01 2.16E*01 2.16E-01 3.86E-01 19-09012-11 19-09012-11 TRG TRG L1-102218-FIGS-100-SS-A L1-102218-FIGS-100-SS-A 06/20119 09:55 06/20/19 09:55 9/3/2019 9/3/2019 9/11/2019 9/11/2019 .;,_
| |
| 19-09012 19-09012 Si1ver-108m Arnericium-241 EPA 901.1 Modified EPA 901.1 Modified
| |
| -3.45E-02 2.68E-02
| |
| __ ""-~'
| |
| 5.69E-02 1.18E-01 5.70E-02 1.18E-01 5.63E-02 1.58E-01
| |
| ,__........... , ___________ ,,,,,,,_,,,,.. **--- ..- ------------- '"'"-----~----------* ''"
| |
| m,,,_, _ _ _ _ _ _ _ _ _ _ _ _ ,="" _ _ ,,,
| |
| 19-09012-11 TRG L1-102218-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 9/11/2019 19-09012 Barium-133 EPA 901.1 Modified -4.23E-03 4.60E-02 4.60E-02 9.SOE-02 19-09012-11 TRG L1-102218-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 9/11/2019 19-09012 Bismuth-214 EPA 901.1 Modified 4.53E-01 1.31E-01 1.33E-01 2.01E-01
| |
| *----------------- ---------*----*---,-----------***-- -------------" --------------~----~-------~-- --------*---
| |
| 19-09012-11 TRG L1-102218-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 9/11/2019 19-09012 Cobalt-60 EPA901.1 Modified 8.15E-02 4.67E-02 4.69E-02 1.02E-01
| |
| ------+-------~----,-------------------, ..................------------,-----..----------------------------C---"---..----J 19-09012-11
| |
| ----------0--*----,------ TRGV L1-102218-FIGS-100-SS-A
| |
| ,-,-~,,,________________ , __ _ 06/20/19 09 :55 9/3/2019 9/11/2019 19-09012 Cesium-134 EPA901.1 Modified 1.02E-02 2.82E-02 2.82E-02
| |
| - - - -..+,..--..-------- *--.... ----------*-------------*-------~---------------------------1 7.01E-02 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 9/11/2019 19-09012 Cesium-137 EPA 901.1 Modified 2.66E-01 9.61 E-02 9.70E-02 1.35E-01 19-09012-11 TRG***--*"* L-1--1-o-22-18~FiG_s___1_00---s-S--A 06120119 09:55 1 9/3/2019 9/11/2019 ---E-P-A ____9__0**---1--_--1---M-o_d_ifi_,e__d____ _,_ ___5____ 2_5E---02________ -----9-.2**-7-E--o-2*-'--9-_2_7_E--o-2_____ 1_-99_E___
| |
| o_1---------
| |
| --~A--------,-------
| |
| 19-09012-11 TRG L1-102218-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 9/11/2019 EPA 901.1 Modified -1.70E-01 1.97E-01 1.97E-01 1.00E-01
| |
| -----------~-------------------------*--------+*---*-----------***------~-------..*--------------.."--------------+---------------*-*--'------...... -----------------.--------------------------------------------1 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/1909:55 9/3/2019 9/11/2019 EPA901.1 Modified 5.79E-03 1.13E-01 1.13E-01 1.46E-01 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 9/11/2019 EPA 901.1 Modified O.OOE+OO 8.09E-02 8.09E-02 8.63E-02
| |
| ------------~-------
| |
| 19-09012-11 TRG L1-102218-FIGS-100-SS-A 06/20/19 09:55 9/3/2019 EPA901.1 Modified 2.04E+OO 9.54E+OO 9.54E+OO 3.87E+OO 1------i---------------*--*------------------------*+-*---*------------~--- *----*---*--'-----------,-----*-------+---*-*-*--
| |
| 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/1909:55 9/3/2019 EPA901.1 Modified 1.15E+01 1.79E+OO 1.89E+OO 7.20E-01
| |
| _ _ _,______________ ,___________-----~-----~------i----------------l----------*--------~----------"-***-*-------------------*-*-----------------*----'----"---1 19-09012-11 TRG L1-102218-FIGS-100-SS-A 06/20/1909:55 9/3/2019 EPA901.1 Modified -1.14E-02 6.08E-02 6.0SE-02 9.10E-02
| |
| --+------*---*-- -:........... ____c,_________;._, _______ .........CC--------*-*l---------. .--..--+---*--------+--
| |
| 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/1909:55 9/3/2019 EPA901.1 Modified 5.18E-02 4.12E-02 4.12E-02 6.30E-02
| |
| ---------------------'-----*'-----1
| |
| _1_9_-0_9_01_2_-1_1--j-_ TRG L1-10221B-FIGS-100-SS-A -!--0-__6:.;/2~-0=-/1:_;9_0:.;9_:_:5:__5:__;~9-/3_12=-0=-1-:9_.__;__;_ _____;_:_:__:_;__;__:,.._ ______________ --J----E_P_A ______9___0___
| |
| 1._1_M_o_d_ifi_ed___ +__-3_._25_E_-_02_________ , .... 4.30E-02 4.30E-02 5.78E-02 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/1909:55 EPA901.1 Modified 2.18E+OO 1.60E+OO 1.61E+OO
| |
| ,-------,--.. ----*-*----------*-J.-----------*-*-------*--*----,-*-----i-------..L .. - ....----+------*-*--*--*-*--*------i-----*----------------~-----------'-*---------'--.::._-----1 19-09012-11 TRG L1-10221B-FIGS-100-SS-A 06/20/19 09:55 EPA 901.1 Modified 4.67E-01 1.03E-01 1.06E-01 1-------------i-------------------------------*+*---------;----------'-------+*-----,-------------+---------
| |
| 19-09012-11 TRG L1-10221 B-FIGS-100-SS-A 06/20/19 09:55 EPA 901.1 Modified 1.33E-01 1.35E-01 1.12E+OO 2.01E-01 2.05E-01 L1-10221B-FIGS-100-SS-A EPA901.1 1.17E+OO 1.58E+OO
| |
| -i------
| |
| 19-09012-11 --4-___~~~221B-FIGS-100-SS-A Thallium-208 EPA 901.1 1.05E-01 1.22E-01 19-09012-11 i TRG i L1-10221B-FIGS-100-SS-A Uranium-235 3.07E-01 3.0SE-01 4.47E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/48!-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/2019 12:02 PM Page 14 of 21 Report To: Work Order Details:
| |
| Eberline Analytical Patricia Giza
| |
| -*---'-'""~'*--,****"=--*------
| |
| SDG: 19-09012 Zion Solutions ~- .. ---*----- Purchase Order: 677118
| |
| *--*-***-~- "--*-*------- -*- ----------------------~-----*
| |
| Final Report of Analysis 2701 Deborah Ave "''"' ____ ____ Analysis_Category: __ ENVIRONMENTAL Zion, IL 60099 Sample Mattix: so Lab Sample Client Sample Analysis Batch Report ID Type ID Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 9/11/2019 19-09012 Actinium-228 EPA901.1 Modified 6.27E-01 1.88E-01 1.91E-01 3.77E-01 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 9/11/2019 19-09012 Silver-108m EPA 901.1 Modified 3.54E-02 5.90E-02 5.91E-02 7.24E-02 u 19-09012-12 TRG L1-10221C-FIGS-103-SS-A 9/11/2019 19-09012 Americium-241 EPA 901.1 Modified -5.64E-02 8.37E-02 8.37E-02 1.16E-01 u
| |
| -------~-------------~*-, ""*-*----*-*=--
| |
| 19-09012-12 TRG L1-10221C-FIGS-103-SS-A 9/11/2019 19-09012 Barium-133 EPA901.1 Modified 1.47E-02 3.60E-02 3.60E-02 1.33E-01 u
| |
| -*--*-**-----"-""------.,-------*"*-----~-------------*--------*-*-** ------------*----*: "'--*----.~-*--- -*-- --*-*-*--*---- ---------*---~---
| |
| 19-09012-12 TRG L1-10221C-FIGS-103-SS-A
| |
| *-*------------...,..,---**-----*--~--~--*-*------ ----------**---~- _,,,,, __________'""\''"----------*'"'"
| |
| 07/08/19 12:47 9/3/2019 9/11/2019 ""'. __ ,,
| |
| _________ ___ --------,,0--,---,,---~--
| |
| 19-09012 , ___ , Bismuth-214, EPA 901.1 Modified 3.35E-01 1.47E-01 1.48E-01 2.80E-01 19-09012-12 TRG L1-10221C-FIGS-103-SS-A 07/08/19 12:47 9/3/2019 9/11/2019 19-09012 Cobalt-60 EPA 901.1 Modified 9.13E-02 6.23E-02 6.25E-02 1.12E-01 u
| |
| -----------J-----'""----,-------------..----**--*~,
| |
| ______ 19-09012-12 "' ______________ _____
| |
| .. _____ ____........-, .......... TRG , __ ...
| |
| l 1-10221C-FIGS-103-SS-A ,___,,, ____. -* 07/08/19 12:47 9/3/2019 9/11/2019 19-09012 Cesium-134 EPA 901.1 Modified
| |
| -----*----*---~----
| |
| 1.66E-02 2.41E-02 2.41E-02 1.04E-01 u 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A ___________ ,,, 07/08/19 12:47 9/3/2019 9/11/2019 19-09012 Cesium-137 EPA901.1 Modified 8.33E-02 1.26E-01 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 07/08/19 12:47 9/3/2019 9/11/2019 19-09012 Europium-152 EPA 901.1 Modified
| |
| .......-*----*-~
| |
| 7.34E-02 1.87E-01 u 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 07/08/19 12:47 EPA901.1 Modified 1.53E-01 9.92E-02 u u
| |
| ..- ...........--~***-*-----*----..* - - - - * - - - ,.. ..._,__,-,,-----
| |
| 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 07/08/19 12:47 19-09012 Europium-155 EPA 901.1 Modified 9.91E-02 1.49E-01 19-09012-12 TRG L1-10221 C-FIGS-103-SS-A 07/08/19 12:47 19-09012 Holmium-166m EPA901.1 Modified 6.88E-02 u 19-09012-12 TRG L 1-10221 C-FIGS-103-SS-A 19-09012 lodine-129 EPA901.1 Modified 9.90E-02 u 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 19-09012 Potassium-40 EPA 901.1 Modified 1.10E+OO pCi/g 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 19-09012 Manganese-54 EPA 901.1 Modified 1.04E-01 u 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 19-09012 Molybdenum-93 EPA901.1 Modified u
| |
| ----------..*-*--..--~ *-*--------*-"
| |
| 19-09012-12 TRG L 1-10221 C-FIGS-103-SS-A 19-09012 Niobium-94 EPA 901.1 Modified u 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 19-09012 Lead-210 1.01E-01 u 19-09012-12 TRG L1-10221C-FIGS-103-SS-A 19-09012 Lead-212 2.71E-01 19-09012-12 TRG L 1-10221 C-FIGS-103-SS-A 07/08/19 12:47 ' 9/11/2019 19-09012 Lead-214 EPA 901.1 Modified 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 07 /08/19 12:47 9/3/2019 9/11/2019 19-09012 i Promethium-145 EPA 901.1 Modified pCi/g TRG L1-10221 C-FIGS-103-SS-A 07/08/19 12:47 9/3/2019 9/11/2019 19-09012 Radium-226 EPA 901.1 Modified TRG L 1-10221 C-FIGS-103-SS-A 07/08/19 12:47 9/3/2019 9/11/2019 19-09012 . Antimony-125 EPA901.1 Modified u TRG L 1-10221C-FIGS-103-SS-A 07/08/19 12:47 i 9/3/2019 9/11/2019 19-09012 : Thorium-234 EPA901.1 Modified 1.16E+OO u pCi/g 9/11/2019 19-09012 '
| |
| Thallium-208 EPA 901.1 Modified 2.02E-01 19-09012-12 TRG L 1-10221 C-FIGS-103-SS-A 07/08/19 12:47 9/3/2019 19-09012-12 TRG L 1-10221C-FIGS-103-SS-A 07/08/19 12:47 i 9/3/2019 9/11/2019 19-09012 Uranium-235 EPA901.1 Modified 2.98E-01 3.96E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/2019 12:02 PM Page 15 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical '""'''''"'""'""""""'
| |
| Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| ---- ,,----~------*------- ---- -------------.--- -
| |
| Final Report of Analysis 2701 f"""'-----*-*----.------~-
| |
| Deborah Ave e - - - - - - -----------*--*------ e**-*--~--1***
| |
| ,cw-*
| |
| Analysis,Category: _ ___E_N_V_IR_O_N_I\J1_ENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch ' Report Analyte Method Result CU CSU MDA Qualifier ID , Type ID Date Date Date ID \ Units 19-09012-13 TRG L1-10221 B-FIGS-102-SS-A 07/08/19 13:10 9/3/2019 9/11/2019 19-09012 Actinium-228 EPA 901.1 Modified 3.53E-01 ' 275E-01 2,75E-01 5,65E-01 U pCi/g
| |
| '"'"'"'"'""'""""''"''''"'""""""" _____________ ,____________''""'''"'"'___ ------+--------,----"''""''"" ______ ""--,------"'*""'""'""'""'--'""''"'"!"' ''""
| |
| 19-09012-13 TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 , 9/3/2019 9/11/2019 19-09012 : Silver-108m EPA901,_1___ M_od_ifi_,e_d_+___-_3,_93 __E_-_02__, ___6_,_6S__E 02_ 6.66E-02 8-77E-02 U pCi/g
| |
| _1_9_-o_90_1_2-_13-____ _:_F:_~---L_1_-1_02~1~-:~1Gs-_102-~~;:;----- 07/08/1913:10 91_3_1_2_0_1__9___ ,-9___11_1_12_0_19__,_1_9"_-0_9_01_2-+_Am_e__n_ci__u_m_-_2___ 4_1_ EPA 90U Modified -1A4E-01 ' 8.57E-02 8-60E-02 U2E-01 u pCi/g __ _
| |
| 19-09012-13 TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019
| |
| -------------------------------------'"'-----l---.:;_ _________;,._"_" _______9/11/2019 19-09012
| |
| ,____,_,,_,,_--~-------*""''" Barium-133 EPA 901-1 Modified -3,11E-02
| |
| '"'"'''"'""'"-""-"T''"----i--'"'""""""
| |
| 9,87E-02 9,87E-02 125E-01
| |
| """"""'""''"""''"'---------*---,-----C---,C"'"""-1 U pCi/g
| |
| _}_9-:~9-~2:1~~3-. ~R~"----~1:_1022-1B_-_Fl~~~:_?_2-_S-S:_.t; ______ I- __ 0_7i_08_i_19_1_3_:1_0___ ,'___9i__3__i2__
| |
| 0_1"9______9_1,1__1_12_0_19---'-__1_9_-_o__9_0__1__12--"'__B_is_m_u_th_-_2__1_4____ + EPA 901-1 Modified 5.30E-01 1-52E-01 1,SSE-01 1.60E-01 , pCi/g --
| |
| ,,,,1,9,:!_9012-1 ~-- __":i:~~--L_1-_10_2~~--F_IG~_:1_?2:_~~-~-- .,,., 07/08/19 13:10 : 9/3/2019 9/11/2019 19-09012 Cobalt-60 *_ EPA 901-1 Modified 5,0SE-01 1,08E-01 1.11 E-01 ____ 1_.8_2_E_-_01______________;__pC__i _g_0 ___---1 19-09012-13 TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 ; Cesium-134 EPA90U Modified '22E-03 1-96E-02 1,96E-02 9.82E-02 U pCi/g
| |
| - ___,___ "" *"""' -'-"'-""" - - - - - '"""'"--,-,_m-+-*----------+-""'"""""-""'___ "__________+-----*-"'"'"'"' ""'"""'
| |
| __19_-_09_0_12_-~~" " _L_1-_10_2_21_B:~G_s_-1_0_2-_s_s:;:;________ -1 __0_1___10__8_11._9_1 __3__:"1__ 0 _____9_13_1_20_,_1__9"_____9_11_1_12_01_9,_____1_9_-o_90_1_2_,l+-_c_e_s__i__ um----1_37_ _, ___E_P_A ___9_0--1_____1____
| |
| M__o__
| |
| difi_,e_d____ _;__9__ 82_E_-0_1_ _ ,_1._s_oE__-_0"__1_ ---"- ____
| |
| 1__s1__E___-_01_____1_,s,_sE_-"0___
| |
| 1 _______,____:__pCi-'-ig_-1 1
| |
| 19-09012-13 TRG L1-10221B-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 :::v,ve,v .. , ,52 EPA90U Modified 2,64E-01 ; 1,93E-01 1,93E-01 1,96E-01 U pCi/g 0
| |
| 1-19-09012-13
| |
| * TRG""" -c;-.:-10-22_1_s_-FIGS--10-2--s-s;_*------,-1---07-/0-8--/1_9_1_3*:*1--o---~-9/_3_/2-01-9-~--9--/1_1_1_2_0_19_____1_9_,__0_9_0-12-+- 1-Eu_r.op-iu_m___ 154---1----E-P-A"'"9"01 1 Modified 3.38E-02 2_ 10E-01 2_ 10E-01 1 _02E-01 u pCi/g
| |
| ,------------------+--------,--------------*"""'---;----------- ---------
| |
| 19-09012-13 ' TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 , Europium-155 EPA901.1 Modified 1.58E-04 8.83E-02 8.83E-02 1.29E-01 U pCi/g 1 - - - - ' - ' " ' " ' " " ' ' " " " ' " " - ' - - - - - - - - - - - - - - - - - - - - - - - - - - i - - - - - - - * - - ---------"-- ----- t--------+-*-"""'""'""""' ------------+------r--------'""''"'"'""*-*--*------------------'---"-------1 19-09012-13 TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 : 9/3/2019 9/11/2019, 19-09012 \ Holmium-166m EPA90U Modified -7AOE-02 ; UOE-01 UOE-01 7.63E-02 U pCi/g 1-------,-----------------------*""'"--j-'------+----------- i--------------- "'""'"'"'''""'"'-------+---,--i----------,."_______________:_ _ _ _ _ __, ___ ,:;"''----1
| |
| __ 1S-v,v "-~::; ! __:R~-"-- L1-10221~~1GS-102-~~---- __ 07/08/19 13:10---~~-0~ __ ?111/20:_9-_ 19-09012 l lodine-129 ---l------E__P__A ___9_0_1__,1_M_o_d_ifi_1e_d__+-_2__2_o_E_-0_1__,__ ""2_.34 __E__ -o_1_-_____2 ___34_E__-0_1___3_,_4__ 1E_-0_1_~__u_______"p_Ci/-'-g--1 l--~9-09012-13 TRG _ L1-102218-FIGS-102-SS-A '""' 07/08/1913:10 9/3/2019 9/11/2019 __ 19-09012 [ Potassium-40 EPA9"0"_1_",_1__ M_od_ifi_e_d_+_1_1.s_oE_+o1___3_._1s_E___ +_o_o________3___-_26_E_+_oo_ _ _ 8_.2_4E__-0_1__* _ _ _"'C"""""'_pCi_ig___-t 19-09012-13 TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 Manganese-54 EPA901.1 Modified 8A8E-02 8-87E-02 8,89E-02 1A7E-01 U pCi/g
| |
| -~--"---
| |
| 19-09012-13 TRG
| |
| ----*-L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 Molybdenum-93 EPA901,1 Modified 4.85E-02 ! 5,26E-02 5.27E-02 9,10E-02 U pCi/g 19-09012-13 ; TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 , Niobium-94 EPA901.1 Modified -4.31E-02 6A8E-02 6A8E-02 8.65E-02 U pCi/g 19-09012-13 ; TRG , L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 Lead-210 EPA90U Modified 6A2E-01 , 8.90E-01 , 8,91E-01 1,35E+OO U pCi/g 19-09012-13 t TRG U-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 i Lead-212 EPA90U Modified 4,56E-01 1.18E-01 1,20E-01 2,54E-01 pCi/g 19-09012-13 : TRG U-102218-FIGS-102-SS-A 07/08/1913:10 ! 9/3/2019 9/11/2019 i 19-09012 Lead-214 EPA 901-1 Modified 4,20E-01 f 1.24E-01 1.26E-01 2.31E-01 19-09012-13 I TRG , L1-102218-FIGS-102-SS-A 07/08/19 13:10 9/3/2019 9/11/2019 i 19-09012 -,v, ,v::,v, ,- ~: EPA 901.1 Modified 5,61E-02 ! 1.52E-01 1,52E-01 2,26E-01 U pCi/g 19-09012-13 : TRG -----~1-102218-FIGS-102-SS-A 07/08/1913:10 ! 9/3/201_9-1,__9_1_1_11_20_1_9_ '_19_-_o9_0_1_2+_Ra_d_iu_m_-_22_s_l-__E_PA __ 90____1___1_M_od_ifi_,e_d_+__s__3_o_E_-0_1--i1-1__s-::2E~-0_1_, __ 1__s_s_E_-0_1" _ _,1__ s_oE'CC"-,01--c-T"''--c-:-----P'-C:-cii::g_-l 0
| |
| 19-09012-13 : TRG L1-102218-FIGS-102-SS-A 07/08/191 9 ' 9/11/2019 19-09012 Antimony-125 EPA901.1 Modified 1.63E-01 2.02E-01 / 2.02E-01 3.03E-01 , U pCi/g
| |
| -----+---\-----'---+---------+----:-+--~~~-+-----~---~-:-'----:~--'-:c:_--1 19-09012-13 [ TRG L1-102218-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 +---Th_o_ri_um_-_2_34_+-__E_P_A_9_0_1.__ 1_M_o_difi_,e_d_+-__ 9.7__1_E-0_1___ 7'._36E_-o1_':""_7',,_38E __-o__1 ____1_,1_4E_+_o_o_,___u ______ pCii_g_""'1 19-09012-13 I TRG ' L1-10221B-FIGS-102-SS-A 07/08/1913:10 9/3i2?_1_9-4-_91_1_11_20_1_9_;,__19_-_o9_o_1_2+_T_h_a_lliu_m_-_20_8__ ___
| |
| 1 E_PA_90_1_.1_M ____
| |
| od_ifi_e_d--+_4_,.o~-2~Ec_-O n1,--l_2_.21_1E_-0___1__',---2._21_E_-0__1_____ 3._s_oE_-_01_ _ ._----'---P,__Cii_::;_g----i 19-09012-13 i TRG '. L,-.~;:;:;;:;-FIGS-102-SS-A 07/08/1913:10 9/3/2019 9/11/2019 19-09012 Uranium-235 EPA901.1 Modified 1'-"~c-v, 2.60E-01 [ 2,61E-01 3.97E-01 ' U pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 16 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical SOG:
| |
| Zion Solutions
| |
| ,,, *-----~"*--, Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave
| |
| ------------*--,---*--------- - . . . Analysis Category<. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date Analyte Method Result cu CSU MDA Qualifier ID Units 19-09012-14 TRG L 1-10221 B-FIGS-103-SS-A 07/08119 13:12 9/3/2019 9/1112019 19-09012 Actinium-228 EPA 901.1 Modified 2.23E-01 1.85E-01 1.85E-01 3.29E-01 19-09012-14 TRG L 1-102218-FIGS-103-SS-A 07108119 13:12 9/312019 9/11/2019 19-09012 Silver-108m EPA 901.1 Modified -1.18E-02 4.49E-02 4.49E-02 5-76E-02
| |
| --------"""-~------------
| |
| 19-09012-14 19-09012-14 TRG TRG L1-10221 B-FIGS-103-SS-A L1-102218-FIGS-103-SS-A 07/08119 13:12
| |
| *---'""'""'_m_,,_.,,,, _ _ _ _ _
| |
| 0710811913:12 91312019 913/2019 "S-____ .----,----
| |
| 9/11/2019 9111/2019 19-09012 19-09012
| |
| =
| |
| Americium-241 Barium-133 EPA 901.1 Modified EPA901.1 Modified
| |
| -1.36E-01 1.09E-01
| |
| ,,_ -----~-+------*----*-**--*----*------***+-----**--------*------*--***---------**------
| |
| 2.80E-02 2.80E-02 1.26E-01 7.83E-02 u
| |
| u
| |
| ,_._ _ _ _ ""- " ' " " " " ' " " " ' " _ _ , _ , _ ,_ _ _ _ _ _ _, _ , _ _ e
| |
| - - - . ~ - - - - - - - - - - * "'"m,_, _ _ _ _ , - , - - = - - - ' " " " ' - " " " " ' - " " " , . , . , , . . , _ , , , . . , , . , _ ,..... , , . , , ,. .. , , , . ,
| |
| 19-09012-14 TRG L1-102218-FIGS-103-SS-A 07/0811913:12 9/3/2019 9/1112019 19-09012 Bismuth-214 EPA901.1 Modified 1.20E-01 1.21E-01 2.04E-01 19-09012-14 TRG L1-102218-FIGS-103-SS-A
| |
| ----------,-=-,--------*----------------
| |
| 07108/19 13:12
| |
| ----------------*0 913/2019 9/1112019 19-09012 ____ , ___ --~ Cobalt-60 EPA901.1 Modified 5.51E-02 5.63E-02 9.50E-02 19-09012-14 : TRG L 1-102218-FIGS-103-SS-A 07/08/1913:12 9/3/2019 9/11/2019 19-09012 Cesium-134 EPA 901.1 Modified 4.08E-02 4.09E-02 5.63E-02 u
| |
| *--*--------~------***----*------------------------ - - * - - - - " - " " , ----m"""' +~- -~-~-w- --""'
| |
| 19-09012-14 TRG L1-102218-FIGS-103-SS-A 07108119 13:12 91312019 9/11/2019 19-09012 Cesium-137 EPA901.1 Modified 1.52E-01 1.62E-01 7.67E-02 19-09012-14 TRG L 1-102218-FIGS-103-SS-A 07108/19 13:12 9/312019 9111/2019 19-09012 1.92E-01 1.77E-01 u 19-09012-14 TRG L1-10221 B-FIGS-103-SS-A 07/08119 13:12 9/3/2019 911112019 19-09012 1.49E-01 1.49E-01 9.42E-02 u 07108/19 13:12 9/3/2019 9111/2019 19-09012 9.62E-02 9.63E-02 u 19-09012-14 TRG L 1-102218-FIGS-103-SS-A 07108119 13:12 9/11/2019 19-09012 2.46E-02 6.93E-02 u 19-09012 : 8.55E+OO 3.43E+OO u 1.76E+OO 1.56E+OO 19-09012-14 ___________L1-10221 TRG ,_ B-FIGS-103-SS-A 07/08119 3.41E-02 6.96E-02 u 19-09012-14 TRG L1-10221 B-FIGS-103-SS-A 3.40E-02 5.59E-02 u TRG L 1-10221 B-FIGS-103-SS-A 07108/19 13:12 3.62E-02 5.55E-02 u 19-09012-14 TRG L 1-10221B-FIGS-103-SS-A 07108119 13:12 1.38E+OO 2.29E+OO u 19-09012-14 TRG L 1-10221 B-FIGS-103-SS-A 07108/19 13:12 EPA 901.1 Modified 1.83E-01 19-09012-14 TRG L 1-102218-FIGS-103-SS-A 07/08119 13:12 EPA 901.1 Modified 19-09012-14 TRG L 1-102218-FIGS-103-SS-A 07/08119 13:12 EPA 901.1 Modified 19-09012-14 TRG L1-10221 B-FIGS-103-SS-A EPA901.1 Modified 19-09012-14 TRG L 1-10221 B-FIGS-103-SS-A EPA901 . 1 Modified 1.08E-01 u 19-09012-14 TRG L 1-10221 B-FIGS-103-SS-A 9.58E-01 1.30E+OO u pCi/g 19-09012-14 TRG L 1-10221 B-FIGS-103-SS-A 07108119 13:12 Thallium-208 7.63E-02 9.85E-02 pCi/g 19-09012-14 TRG L1-10221 B-FIGS-103-SS-A 07108119 13:12 Uranium-235 2.79E-01 3.92E-01 u pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/2019 12:02 PM Page 17 of 21 Report To: Work Order Details:
| |
| Eberline Analytical Patricia Giza SDG: 19-09012 Zion Solutions Purchase
| |
| ~,- -~-,~- Order:
| |
| ---------- ___ 677118
| |
| **---*---------m ' , ,_, , , __
| |
| Final Report of Analysis 2701 Deborah Ave *-**--------1 Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09012-15 TRG L 1-102218-FIGS-104-SS-A 07/08/19 13:14 9/11/2019 19-09012 Actinium-228 2.22E-01 2.23E-01 3.59E-01
| |
| ---------- - ,,--*----~-------------""=--------
| |
| 19-09012-15 TRG L1-10221B-FIGS-104-SS-A 07/08/19 13:14 9/11/2019 19-09012 Si1ver-108m 5.80E-02 5.80E-02 8.18E-02 19-09012-15 TRG 07/08/19 13:14 9/1112019 19-09012 Americium-241 8.90E-02 8.91E-02 1.21E-01 19-09012-15 TRG L 1-10221B-FIGS-104-SS-A 07108/19 9/11/2019 19-09012 Barium-133 2.56E-02 2.56E-02 1.35E-01 19-09012-15 TRG L1-10221 B-FIGS-104-SS-A 07108/19 13:14 9/11/2019 19-09012 Bismuth-214 3.11E-01 1.22E-01 1.23E-01 2.56E-01 19-09012-15 TRG L1-10221 B-FIGS-104-SS-A 07/08/19 13:14 9111/2019 Cobalt-60 EPA 901.1 Modified -1.42E-02 7.83E-02 7.83E-02 1.17E-01
| |
| --*******-'********---********-*---~---------********-----*-**********---'-__;'---1 19-09012-15 TRG L 1-10221 B-FIGS-104-SS-A 9/11/2019 EPA 901.1 Modified -1.58E-01 1.05E-01 1.06E-01 1.01E-01 19-09012-15 TRG L 1-102218-FIGS-104-SS-A 9.07E-02 9.14E-02 1.31E-01 1.53E-01 1.53E-01 1.86E-01 1.06E-01 1.06E-01 9.22E-02 19-09012-15 TRG 1.03E-01 1.03E-01 1.43E-01 19-09012-15 TRG 9.73E-02 9.73E-02 6.56E-02 19-09012-15 TRG 6.44E-02 6.44E-02 9.15E-02 19-09012-15 TRG 1.66E+OO 9.19E-01 19-09012-15 TRG 7.16E-02 1.13E-01 19-09012-15 TRG EPA901.1 Modified 8.24E-02 19-09012-15 TRG EPA 901.1 Modified 8.28E-02 EPA 901.1 Modified 1.06E+OO u EPA 901.1 Modified 1.79E-01 EPA 901.1 Modified 2.44E-01 EPA901.1 Modified 1.14E-01 u L1-10221B-FIGS-104-SS-A EPA 901.1 Modified 2.56E-01 TRG L 1-10221 B-FIGS-104-SS-A EPA901.1 Modified 2.54E-01 u 19-09012-15 TRG L1-102218-FIGS-104-SS-A EPA901.1 Modified 9.64E-01 1.78E+OO u 19-09012-15 TRG L1-10221 B-FIGS-104-SS-A EPA 901.1 Modified 2.91E-01 2.76E-01 pCi/g 19-09012-15 TRG L 1-102218-FIGS-104-SS-A EPA901.1 1.34E-01 4.14E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| | |
| Printed: 10/21/201912:02 PM Page 18 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| "'____""----------*-" ~--*-*" --'"""*----*----- ---~---------
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category:____ ENVIRONMENTAL __________________ ........-----*-*-------*-- ______ _
| |
| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Report ID Type ID Date Date Date Method Result cu CSU MDA Qualifier Units 19..09012-16 TRG L1-10221 B-FIGS-105-SS-A 07/08/19 13:16 9/3/2019 9/11/2019 EPA901.1 Modified 3.60E-01 2.35E-01 2.36E-01 4.73E-01 u 19-09012-16 TRG L1-10221 B-FIGS-105-SS-A 07/08/19 13:16 9/3/2019 9/11/2019 EPA 901.1 Modified -1.53E-03 3.55E-02 3.55E-02 8.25E-02 u
| |
| -------------"""'"'1"'"""""'"'' -----\------------**-'-----*-*-*-.. -**-*
| |
| 19-09012-16 TRG L1-10221B-FIGS-105-SS-A 07/08/19 13:16 9/3/2019 9/11/2019 EPA 901.1 Modified -1.21E-01 8.16E-02 8.19E..02 1.05E-01 u 19-09012-16 TRG L1-10221B-FIGS-105-SS-A 07/08/19 13:16
| |
| : 9/3/2019 9/11/2019
| |
| --,~-. cm-.--.*~---*------------ EPA 901.1 Modified 2.07E-02 2.44E-02 2.44E-02 1.08E-01 u 19-09012-16 TRG L1-102218-FIGS-105-SS-A 07/08/19 13:16 9/3/2019 9/11/2019 19-09012 Bismuth-214 EPA 901.1 Modified 2.93E..01 1.34E-01 1.35E-01 1.62E-01
| |
| ---*--------*-*-*--*-----* ----------*.-*--------*----*------- . -*-------*-------------+-*-----*-----*----------------;-----*-*-----:----------*,*---*-----------*------
| |
| 19-09012-16 TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 9/3/2019 9/11/2019 19-09012 . Cobalt-60 EPA901.1 Modified 2.64E-02 7.89E-02 7.89E-02 1.35E..01 u
| |
| . 19-09012-16 ~ TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 : 9/3/2019 9/11/2019 19-09012 -----+--E--P----A--9-0__1___1_M_o*d--ifi*,-e-d----**----------------*-*--**-----------------
| |
| 3.00E-02 3.00E-02 8.99E-02 u 19-09012-16 TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 ' 9/11/2019 - EPA901.1 Modified 1.58E-01 8.22E-02 8.26E-02 1.25E-01 19-09012-16 TRG L1-10221 B-FIGS-105-SS-A 07/08/19 13:16 9/11/2019 EPA 901.1 Modified 1.03E-01 1.03E-01 1.61E-01 u TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 9/11/2019 EPA901.1 Modified 2.03E-01 2.07E-01 8.50E-02 u
| |
| ---*--*-------*--+----------;-------+-----*---*--------------+--'-----*----~------*-----------*---+-'*------'-------------------------*--
| |
| TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 9/11/2019 EPA901.1 Modified 1.71E-01 1.19E-01 1.64E-01
| |
| '""'""'"'+------+------*---------*,*-----*-----*--*-----,*-
| |
| 19-09012-16 TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 EPA901.1 Modified 9.83E-02 6.69E-02 u
| |
| ---*----*---------~-- ' ----------
| |
| 19-09012-16 TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 2.92E-01 u
| |
| ---*----*------*-*--+------*--*----*-----*-----**---*--ls---*----+----**-*-*-------*---*----*--*i--------+--*--**-------*--i--**-*------*---*-*----*+-----**-*--~----
| |
| 19-09012-16 TRG L1-102218-FIGS-105-SS-A 07/08/1913:16 3.83E-01
| |
| -*--------~-----------*---*--**-----+--------*---------'-*--*------+---*------l---*-------*---!-------+*--------~--------*--
| |
| 19-09012-16 ' TRG L1-10221 B-FIGS-105-SS-A 1.37E-01 u 19-09012-16 ; TRG ~2218-FIGS-105-SS-A . u TRG L1-10221B-FIGS-105-SS-A u TRG L1-102218-FIGS-105-SS-A u 19-09012-16 TRG L1-102218-FIGS-105-SS-A 1.08E..01 2.10E-01 19-09012-16 L1-10221B-FIGS-105-SS-A 9.67E..02 2.12E..01 19-09012-16 1.33E-01 1.82E-01 u 19-09012-16 1.35E-01 1.62E-01 19-09012-16 1.90E-01 2.24E-01 u 1.02E+OO u 3.11E-01 3.76E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 19 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical -
| |
| Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| ,_ >SW .
| |
| --------*- ------------ ''""-~---*-- ,,,.
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category:
| |
| 'r'----*-A ENVIRONMENTAL
| |
| ,-.o--~--**-* -----'-' *-- ...
| |
| so U A- s* _ _ _ _ _._, --- m -------
| |
| Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09012-17 TRG L______________
| |
| 1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/312019 9/11/2019 19-09012 Actinium-228 EPA 901.1 Modified 7.04E-01 2.10E-01 2.13E-01 4.77E-01 pCilg 19-09012-17 TRG
| |
| -------------- -------v------------- ___,____ --------- "'"' _____________
| |
| L 1-102210-FIGS-005-SS-A 07/08/19 12:30
| |
| -------~-*-**-
| |
| 91312019
| |
| ----~---**
| |
| 9/11/2019 19-09012 Silver-108m
| |
| -----=-------~-~- .. ,--**----
| |
| EPA901.1 Modified -7.90E-02 6.59E-02 6.60E-02 7.20E-02 u pCi/g 19-09012-17 TRG L1-102210-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9111/2019 19-09012 Americium-241 EPA 901.1 Modified 4.43E-03 1.37E-01 1.37E-01 1.80E-01 u pCi/g
| |
| "'"''"'*---------------,*---*-"'*------------**------------------- - --------,-----------------------,- ------------------.-----~----
| |
| 19-09012-17 TRG L 1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9111/2019 19-09012 Barium-133 EPA 901.1 Modified i 2.37E-02 3.51E-02 3.51E-02 1.03E-01 u pCi/g
| |
| "'""'"'""'---~----,-----*------------ -------- - - - , ----,-=--------, --------------,-'O' ---------' ~-~~ >-**-**
| |
| 19-09012-17 TRG L1-102210-FIGS-005-SS-A
| |
| ~ ------>--------- ------ "'"""'-"""**----------------------
| |
| 07/08119 12:30 9/3/2019 911112019 19-09012 Bismuth-214 EPA 901.1 Modified : 6.09E-01 1.50E-01 1.54E-01 2.45E-01 pCi/g 19-09012-17 TRG L1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/312019 9/11/2019 19-09012 i Cobalt-60 EPA 901.1 Modified 2.58E-01 6.06E-02 6.20E-02 4.98E-02 pCi/g
| |
| ----------~------- --------------** ------------*-------~--- . - - - * . ------~"-
| |
| 19-09012-17 : TRG L 1-10221 D-FIGS-005-SS-A 07108/19 12:30 9/312019 9/11/2019 19-09012 Cesium-134 EPA901.1 Modified !
| |
| -8.27E-03
| |
| ' 2.05E-02 2.05E-02 6.88E-02 u pCi/g 19-09012-17 , TRG L 1-102210-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9111/2019 19-09012 ' Cesium-137 EPA 901.1 Modified ! 1.39E+OO 2.09E-01 2.21E-01 1.48E-01 pCi/g 19-09012-17 TRG L 1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9/11/2019 19-09012 ! -
| |
| cu1 <CO
| |
| ..... '"', ... ,:1-,...,.._ EPA 901.1 Modified -7.00E-02 2.21E-01 2.21E-01 2.24E-01 u pCi/g 19-09012-17 TRG l 1-102210-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9/11/2019 19-09012 ' cu, ... '"''"''11-1..>"t EPA 901.1 Modified -2.42E-02 1.90E-01 1.90E-01 1.19E-01 u pCi/g
| |
| --------------------s-------------*---**-------- -
| |
| 19-09012-17 TRG L 1-102210-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9/11/2019 19-09012 : Europium- .55 EPA 901.1 Modified 7.09E-02 6.61E-02 6.62E-02 1.88E-01 u pCi/g -*-
| |
| 19-09012-17 i TRG L 1-10221 D-FIGS-005-SS-A 07108/19 12:30 : 9/3/2019 9111/2019 ' 19-09012 Holmium-166m EPA 901.1 Modified 1.00E-01
| |
| ' 8.52E-02 8.53E-02 9.56E-02 u pCilg 19-09012-17 ; TRG L 1-10221 D-FIGS-005-SS-A 07/08119 12:30 9/3/2019 9111/2019 19-09012 i lodine-129 EPA 901.1 Modified 3.29E+OO 1.43E+01 1.43E+01 4.26E+OO u pCi/g 19-09012-17 i TRG L1-102210-FIGS-005-SS-A 07/08/19 12:30 : 913/2019 9/11/2019 19-09012 : Potassium-40 EPA 901.1 Modified 1.35E+01
| |
| ' 2.00E+OO 2.12E+OO 5.20E-01 pCi/g 19-09012-17 [ TRG L1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/312019 9/11/2019 19-09012 ; Manganese-54 EPA 901.1 Modified 5.61E-02 5.73E-02 5.74E-02 9.37E-02 u pCi/g 19-09012-17 ! TRG L 1-10221 D-FIGS-005-SS-A 07108/19 12:30 9/312019 9/11/2019 19-09012 ! ""''"'"""''- M EPA 901.1 Modified 6.43E-03 !
| |
| 4.61E-02 4.61E-02 7.16E-02 u pCi/g
| |
| --"--*----------------- i 19-09012-17 TRG L 1-10221 D-FIGS-005-SS-A 07/08119 12:30 i 9/3/2019 9/11/2019 19-09012 Niobium-94 EPA 901.1 Modified 3.61E-02 5.09E-02
| |
| ' 5.09E-02 8.14E-02 u pCi/g 19-09012-17 ; TRG l 1-10221 D-FIGS-005-SS-A 07/08119 12:30 9/3/2019 9/11/2019 19-09012 , Lead-210 EPA 901.1 Modified 2.87E+OO 2.30E+OO 2.30E+OO 3.72E+OO u pCi/g 19-09012-17 t TRG L 1-102210-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 , 9/11/2019 19-09012 : Lead-212 EPA 901.1 Modified 6.53E-01 i 1.36E-01 1.40E-01 2.29E-01 : pCi/g i
| |
| 19-09012-17 , TRG L1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 i 9/11/2019 , 19-09012 Lead-214 EPA 901.1 Modified i 7.25E-01 1.78E-01 1.82E-01 2.84E-01 pCi/g 19-09012-17 i TRG L 1-10221 D-FIGS-005-SS-A 07/08/19 12:30 913/2019 9/11/2019 ' 19-09012 i Promethium-145 EPA901.1 Modified i 6.59E-01 i 9.07E-01 9.07E-01 1.30E+OO u pCi/g
| |
| ---,-----------**---* 1 19-09012-17 ; TRG L 1-10221 D-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9111/2019 19-09012 Radium-226 EPA 901.1 Modified 6.09E-01 1.50E-01 ' 1.54E-01 2.45E-01 pCi/g 19-09012-17 i TRG L 1-102210-FIGS-005-SS-A 07108119 12:30 9/3/2019 9/11/2019 19-09012 Antimony-125 EPA901.1 Modified 4.16E-02 1.48E-01 1.48E-01 2.47E-01 u pCi/g i
| |
| 19-09012-17 J TRG L 1-102210-FIGS-005-SS-A 07/08119 12:30 9/3/2019 9/11/2019 19-09012 ' Thorium-234 EPA901.1 Modified 3.82E-01 1.28E+OO 1.28E+OO 1.71E+OO u pCi/g
| |
| ''O'----r--
| |
| 19-09012-17 i TRG L1-102210-FIGS-005-SS-A 07/08/19 12:30 9/3/2019 9/11/2019 19-09012 ! Thallium-208 EPA 901.1 Modified 4.04E-01 1.17E-01 l 1.19E-01 2.12E-01 pCi/g 19-09012-17 i TRG L 1-10221 D-FIGS-005-SS-A 07108/19 12:30 i 9/3/2019 9/11/2019 i 19-09012 ! Uranium-235 EPA 901.1 Modified -8.1 4.07E-01 : 4.07E-01 5.21E-01 i u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/21/201912:02 PM Page 20 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions
| |
| **----.-**w*--**--***
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| SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: ____ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09012-18 TRG L1-10221 D-FIGS-006-SS-A 07/08/19 12:32 9/3/2019 9/11/2019 19-09012 Actinium-228 EPA 901.1 Modified 6.21E-01 3.16E-01 3.17E-01 7.23E-01 u pCi/g
| |
| --------------------------------~-----------
| |
| 19-09012-18 TRG L 1-10221 D-FIGS-006-SS-A 07/08/19 12:32 9/3/2019 9/11/2019 19-09012 EPA 901.1 Modified 1.00E-01 1.00E-01 1.22E-01 u pCi/g 19-09012-18 TRG L1-10221D-FIGS-006-SS-A 07/08/19 - 9/11/2019 EPA 901.1 Modified 1.50E-01 1.50E-01 2.14E-01 u
| |
| *-----------"""""'" *-**--*~--------------*-
| |
| 19-09012-18 TRG L1-102210-FIGS-006-SS-A EPA901.1 Modified 6.89E-02 6.89E-02 2.51E-01 u pCi/g 19-09012-18 TRG L1-10221 D-FIGS-006-SS-A EPA901.1 Modified 2.78E-01 2.79E-01 4.89E-01 19-09012-18 TRG L 1-102210-FIGS-006-SS-A 07/08/19 12:32 EPA 901.1 Modified 2.01E-01 1.39E-01 1.39E-01 2.37E-01 u
| |
| ---**----- .-------* *--*-------"'---------*------1---------------------------------------------------------,-----------------------~--------------------------
| |
| 19-09012-18 TRG L1-102210-FIGS-006-SS-A 07/08/1912:32 EPA 901.1 Modified
| |
| --*----*-*-------------, -*-*---*--------------- ----+--------------;-----------i---**--------------:----------------+--- -------------------------------------------------
| |
| 5.54E-02 5.45E-02 5.46E-02 1.79E-01 u 19-09012-18 TRG L1-102210-FIGS-006-SS-A 07 /08/19 12:32 EPA901.1 Modified 8.30E-01 1.70E-01 1.76E-01 1.40E-01 19-09012-18 TRG L1-10221D-FIGS-006-SS-A 07/08/1912:32 EPA 901.1 Modified
| |
| -----------**-------*--+----------------r---*----'*-------------------------o,*****----;_________________ +-----*------
| |
| 1.73E-01 2.16E-01 2.17E-01 3.13E-01 u 19-09012-18 TRG L1-10221D-FIGS-006-SS-A 07/08/1912:32 EPA901.1 Modified -3.02E-02 3.04E-01 3.04E-01 1.SSE-01 u pCi/g
| |
| -------c -------------****--------------
| |
| 19-09012-18 TRG L1-10221D-FIGS-006-SS-A 07/08/1912:32 EPA 901.1 Modified 8.28E-02 1.SOE-01 1.SOE-01 2.68E-01 u 19-09012-18 TRG L1-102210-FIGS-006-SS-A 07/08/19 12:32 EPA 901.1 Modified 6.06E-02 1.83E-01 1.83E-01 1.22E-01 u 19-09012-18 TRG L1-10221 D-FIGS-006-SS-A EPA 901.1 Modified -6.17E-02 1.40E-01 1.40E-01 1.99E-01 u 19-09012-18 TRG L1-10221 D-FIGS-006-SS-A EPA 901.1 Modified 1.24E+01 2.52E+OO 2.60E+OO 2.16E+OO
| |
| - - - * : -*-*-- TRG L1-102210-FIGS-006-SS-A EPA 901.1 Modified -3.66E-02 1.19E-01 1.19E-01 1.86E-01 u TRG L1-10221 D-FIGS-006-SS-A EPA 901.1 Modified 5.62E-02 9.28E-02 9.28E-02 1.46E-01 u TRG L1-102210-FIGS-006-SS-A EPA901.1 Modified 1.61E-02 9.14E-02 9.14E-02 1.35E-01 u TRG L1-102210-FIGS-006-SS-A EPA 901.1 Modified 1.81E+OO 2.02E+OO 2.03E+OO 3.38E+OO u L1-10221 D-FIGS-006-SS-A EPA 901.1 Modified 9.85E-01 2.35E-01 2.41E-01 3.32E-01 pCi/g EPA901.1 Modified 8.92E-01 2.30E-01 2.34E-01 3.63E-01 pCi/g EPA901.1 Modified 3.52E-03 1.37E-01 1.37E-01 2.26E-01 u EPA901.1 Modified 5.20E-01 2.78E-01 2.79E-01 4.89E-01 L1-10221 D-FIGS-006-SS-A EPA 901.1 Modified 2.40E-01 2.65E-01 L1-10221 D-FIGS-006-SS-A EPA 901.1 Modified 1.22E+OO 1.40E+OO 1.40E+OO L1-10221 D-FIGS-006-SS-A EPA901.1 Modified 5.24E-01 2.12E-01 2.14E-01 L1-10221 D-FIGS-006-SS-A Uranium-235 EPA 901.1 Modified 1.0SE-01 4.53E-01 4.53E-01 6.81E-01 CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/21/2019 12:02 PM Page 21 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09012 Eberline Analytical Zion Solutions Purchase Order:
| |
| SOG:
| |
| 677118 Final Report of Analysis 2701 Deborah Ave ___,.....___A__n_alysis Category: ---~f'J_~l-~Q-~~-E_N_T~~
| |
| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report Type 10 Date Date Date ID Analyte Method Result cu CSU MOA Qualifier 10 Units 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07/08/19 12:34 9/3/2019 9111/2019 19-09012 Actinium-228
| |
| ~-----**-*--*------~-----*---**-----
| |
| 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07/08/19 12:34 9/3/2019 9/1112019 19-09012 Silver-108m 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07/08/1912:34 9/312019 9/11/2019 19-09012 Amelicium-241
| |
| **-*-****-****-***---*****--******--'**--*******-******** ***--------------*--***--- OA'----,----~-~- *-*----0-~----"'--"' * ------"'"''""
| |
| 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07/08/1912:34 9/312019 911112019 19-09012 Balium-133 19-09012-19 TRG L1-102210-FIGS-007-SS-A 19-09012-19 TRG L1-102210-FIGS-007-SS-A 19-09012-19 ' TRG . L1-10221D-FIGS-007-SS-A TRG L 1-102210-FIGS-007-SS-A TRG L1-10221 D-FIGS-007-SS-A EPA 901-1 Modified 9 . 37E-04 1. 82E-01 3.04E-01 U
| |
| ""'""'""""-"' **--"'""'""_ _ _ _ ,___________________,,_,,, + - - - - - - - - - - - - * - * - - - - - - * * * - - * * * - * - - - - * " - * - - - - - - - - - + - - - + - - - - - l - - - - - - * - - - - - - - - - - - - - - ~ - - - * * * * - * * - - - - * . - - - - - - - ~ - - - - - - - - - - * - * - - - - - - - - - - - - - - - * - - f 19-09012-19 TRG L1-102210-FIGS-007-SS-A EPA 901.1 Modified -2.29E-01 3.44E-01 3.44E-01 1.56E-01 U
| |
| -*----**"--t-----*--*----~-----~---*-***------------**--**----**-*-------*-----*----***--1 19-09012-19 TRG L1-10221 D-FIGS-007-SS-A EPA901.1 Modified 3.25E-01 1.68E-01 1.69E-01 3.00E-01
| |
| --*------*--r--**---"--
| |
| 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07108/1912:34 EPA901.1 Modified 1.52E-01 1.26E-01 U
| |
| -----****--------***-**+----------'----**-------------..;..... _________-i---------+-----------*-+-----*--*------------------------------_;,..-;;_ __....
| |
| 19-09012-19 TRG L1-102210-FIGS-007-SS-A 07108119 EPA901.1 Modified -7.26E-01 6.10E-01 6.11E-01 7.74E-01 U
| |
| --------------*--------""'"""---~------------t-*---------~---***--*----------*-*---*--***--*----------i------------------+----*----4-->*-------*---------------------------
| |
| 19-09012-19 TRG L1-102210-FIGS-007-SS-A EPA901.1 Modified 4.87E+OO 5.03E+OO 1.81E+OO
| |
| ----------------*----------1---------*-*l---------------*-----'--*----+----**--*------*---* --+---------~------'--------------------------------~---_;,.._c_--1 19-09012-19 TRG L1-102210-FIGS-007-SS-A EPA901.1 Modified 9.08E-02 9.08E-02 1.48E-01 U
| |
| ----------*-*+--*-----+-------------------+-_;;;_________+---*-*-*------*-------**-+-----'-----------------------------'-_;__.;;.__.........
| |
| 19-09012-19 TRG L1-102210-FIGS-007-SS-A EPA901.1 Modified 7.68E-02 7.68E-02 1.20E-01 U pCilg CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MOA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Ouplicate;TRG=Normal Sample;DO=Ouplicate Original;U=Non-detect
| |
| ( ~
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| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
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| ZS-WM-131
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| . ~ REC'D SEP O3 2019 Revision 0 Information Use ZIONSOLUTIONSLLC An EnergySolutions Company
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| ., 9 :a- O9 0 1 2 Ll-10221A-FIGS-002-SS-A NA NA SOIL 500 ml MARINELLI l 6/11/2019 5 ROC HTD NA 1217 922.34g Ll-10221A-FIGS-003-SS-A NA NA SOIL 500 ml MARINELLI l 6/11/2019 5ROCHTD NA 1219 929.16g L 1-10221 A-FIGS-004-SS-A NA NA SOIL 500 ml MARINELLI 1 6/11/2019 5ROC HTD NA 1221 925.96g LJ-102201-FJGS-005-SS-A NA NA SOIL 500 ml MARINELLI I 7/9/2019 5ROC HTD NA 0830 572.09g I
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| Ll-102201-QJGS-005-SS-A NA NA SOIL 500 ml MARINELLI I 7/9/2019 5 ROC HTD NA 0830 648.58g Ll-1022IA-FIGS-003-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5ROC HTD l 1004 NA 812.22g L1-1022JA-FIGS-001-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5ROCHTD J 1000 NA 677.47g LI-10221A-FIGS-004-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5 ROC HTD l 1006 NA 757.61g Ll-I0221A-FIGS-002-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5ROCHTD J 1002 NA 756.86g Ll-10221A-QIGS-OOI-SB-A NA NA SOIL 500 ml MARINELLI 6/26/2019 5ROC HTD l 1000 NA 614.42g Ll-1022IA-FJGS-007-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5ROCHTD 1 0856 NA 710.95g LI-102218-FJGS-002-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5ROC HTD l 0830 NA 714.12g Ll-I0221A-FJGS-002-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5ROCHTD l 0846 NA 771.65g Ll-10221A-FJGS-00I-SS-A NA NA SOIL 500 ml MARINELLI 6/17/2019 5 ROC HTD NA 0844 707.40g Ll-I0221A-FIGS-005-SS-A NA NA SOIL 500 ml MARINELLI I 6/13/2019 5 ROCHTD NA 0745 774.76g Ll-1022IA-FIGS-006-SS-A NA NA SOIL 500 ml MARINELLI I 6/13/2019 5 ROC HTD NA 0747 783.08g LI-10221A-FIGS-007-SS-A NA NA SOIL 500 ml MARINELLI l 6/13/2019 5ROC HTD NA 0749 708.49g Ll-10221A-FIGS-008-SS-A NA NA SOIL 500 ml MARINELLI 1 6/13/2019 5ROCHTD NA 0751 794.16g Ll-10221A-FIGS-009-SS-A NA NA SOIL 500 ml MARINELLI l 6/13/2019 5 ROC HTD NA 0753 774.52g 4 of9
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| ~
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| ZS-WM-131 Revision 0 Information Use ZIONSOLUTIONSrrc An EnergySo/utions Company
| |
| \ \ Ll-10221B-FIGS-100-SS-A NA NA SOIL 500 ml MARINELLI 1 6/20/2019 0955 5 ROCHTD NA- '
| |
| 627.14g
| |
| ;;l Ll-10221C-FJGS-103-SS-A NA NA SOIL 500 ml MARINELLI l 7/8/2019 5ROC HTD NA 1247 860.24g LI-10221B-FIGS-102-SS-A NA NA SOIL 500 ml MARINELLI l 7/8/2019 5 ROC HTD NA 3 1310 680.87g l '"f LI-1022IB-FIGS-103-SS-A NA NA SOIL 500 ml MARINELLI l 7/8/2019 1312 5ROC HTD NA 723.59g rs L 1-10221 B-FIGS-104-SS-A NA NA SOIL 500 ml MARINELLI 1 7/8/2019 1314 5 ROC HTD NA 824.34g J IP L 1-1022 IB-FIGS-105-SS-A NA NA SOIL 500 ml MARINELLI 1 7/8/2019 1316 5 ROCHTD NA 703.93g LI-10221D-FIGS-005-SS-A NA NA SOIL 500 ml MARINELLI l 7/8/2019 SROCHTD NA 1230 626.47g Ll-1022ID-FIGS-006-SS-A NA NA SOIL 500 ml MARINELLI 1 7/8/2019 5ROC HTD NA 1232 649.53g Ll-10221D-FIGS-007-SS-A NA NA SOIL 500 ml MARINELLI l 7/8/2019 5 ROC HTD NA 1234 485.57g Ll-1022ID-FIGS-008-SS-A NA NA SOIL 500 ml MARINELLI 1 7/8/2019 5 ROC HTD NA 1236 530.46g Ll-10221C-AJGS-109-SB-A NA NA SOIL 500 ml MARINELLI 1 6/5/2019 FULL SUITE NA 1236 920.33g Ll-10221C-AJGS-102-SB-A NA NA SOIL 500 ml MARINELLI l 6/5/2019 FULL SUITE NA 1222 868.46g L l-10209C-AJGS-110-SB-A NA NA SOIL 500 ml MARINELLI 1 6/6/2019 FULL SUITE NA 0738 730.63g LI-10209C-AJGS-109-SB-A NA NA SOIL 500 ml MARINELLI 1 6/6/2019 FULL SUITE NA 0736 782.82g LI-10209C-AJGS-108-SB-A NA NA SOIL 500 ml MARINELLI l 6/6/2019 FULL SUITE NA 0734 897.48g Ll-10209C-AJGS-107-SB-A NA NA SOIL 500 ml MARINELLI l 6/6/2019 FULL SUITE NA 0732 654.16g Ll-10209C-AJGS-104-SB-A NA NA SOIL 500 ml MARINELLI l 6/6/2019 FULL SUITE NA 0726 782.70g LI-10209C-AJGS-103-SB-A NA NA SOIL 500 ml MARINELLI 1 6/6/2019 FULL SUITE NA 0724 806.24g Ll-I0209C-AJGS-102-SB-A NA NA SOIL 500 ml MARINELLI I 6/6/2019 FULL SUITE NA 0722 787.15g
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| :I<- '"' - C {£i 5 of9
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| ~
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| ZS-WM-131 REC'D SEP O3 Revision 0 ZIONSOLUTIONSrrc *-gr*-
| |
| ., r-- O9 0 1 2 2079 Infonnation Use An EnergySolulio!Js Company Ll-10221D-FIGS-021-SS-A NA NA SOIL 500 ml MARINELLI 5 ROC HTD L1-1022ID-FIGS-001-SS-A NA NA SOIL 500 ml MARINELLI 5 ROCHTD Laboratory: Date Submitted To Lab: Ship Container No.: Cooler Temperature: FULL SUITE EBERLINE LABS NIA
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| ~s Date Time: Date: (mm/dd/yyyy):
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| ):
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| Relinquished by:
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| /oDf)
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| Relinquished by: Date Time:
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| (mm/dd/yyyy):
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| Comments 9 of9
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| | |
| EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TENNESSEE 37830 ANALYTICAL PHONE (865) 481-0683 FAX (865) 483-4621 EBS-OR-46288 November 6, 2019 Patricia Giza Zion Solutions, LLC 2701 Deborah Avenue Zion, IL 60099 CASE NARRATIVE Work Order# 19-09014-0R SAMPLE RECEIPT This work order contains sixteen soil samples received 09/03/2019. Samples were analyzed for Total Strontium, Tritium, Nickel-63 and by Gamma Spectroscopy.
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| CLIENT ID LAB ID CLIENT ID LABiD L 1-10220A-FSGS-006-SS-A 19-09014-04 Ll-10220H-FJGS-001-SS-A 19-09014-12 L 1-10220A-FSGS-O 16-SS-A 19-09014-05 L 1-10221 D-FIGS-004-SS-A 19-09014-13 L 1-1022 lB-FSGS-006-SS-A 19-09014-06 Ll-10220H-FJGS-004-SS-A 19-09014-14 L 1-1022 lD-FJGS-007-SS-A 19-09014-07 Ll-1022 lD-FIGS-O 10-SS-A 19-09014-15 L 1-10221C-FIGS-101-SS-A 19-09014-08 Ll-1022 lD-FIGS-O 14-SS-A 19-09014-16 L 1-10220I-FJGS-001-SS-A 19-09014-09 L 1-1022 lD-QIGS-013-SS-A 19-09014-17 L 1-10220I-FJGS-002-SS-A 19-09014-10 L 1-10221D-FIGS-013-SS-A 19-09014-18 L 1-102201-FJGS-004-SS-A 19-09014-11 L 1-10221D-FIGS-018-SS-A 19-09014-1 9 ANALYTICAL METHODS Total Strontium was analyzed using EIChroM Method SRWOl Modified. Tritium was performed using Method LANL ER-210 Modified. Nickel-63 was performed using Method ASTM 3500-Ni Modified.
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| Gamma Spectroscopy was performed using EPA Method 901.1 Modified.
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| Laboratory qualifiers are as follows:
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| U - Result is less than the MDA.
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| ANALYTICAL RES UL TS Combined Standard Unce1tainty is reported at I-sigma value.
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| Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific. MDA measurements are determined based on factors and conditions including instrument settings, aliquot size and matrix type.
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| Page l of 3
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| ANALYTICAL RES UL TS CONTINUED TOT AL STRONTIUM Samples were prepared by acid digestion as appropriate for the matrix. Digested samples were acidified and selectively extracted and precipitated. Precipitates were mounted on 4 7mm filters. Filters were reweighed to determine aliquot size. Sample activities were determined by gas flow proportional counting.
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| Samples demonstrated acceptable results for all Total Strontium analyses. Strontium-90 results are repmted from Total Strontium assuming secular equilibrium. Chemical recovery was acceptable for all samples. The Total Strontium method blank demonstrated an acceptable result. Results for the Total Strontium duplicate demonstrated an acceptable relative percent difference and normalized difference.
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| Results for the Total Strontium laboratory control sample demonstrated an acceptable percent recovery.
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| TRITIUM A representative aliquot of each sample was equilibrated with Tritium free water. Equilibrates were transferred into round-bottomed distillation flasks and attached to single stage stills. A pmtion of each middle distillation fraction was transferred to a liquid scintillation vial and cocktail was added. Samples were counted by beta liquid scintillation.
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| Samples demonstrated acceptable results for all Tritium analyses. The Tritium method blank demonstrated an acceptable result. Results for the Tritium duplicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Tritium laboratory control sample demonstrated an acceptable percent recovery.
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| NICKEL-63 A representative aliquot of each sample was prepared by leaching in acids. Aliquots were placed into appropriately sized beakers. Stable elemental Nickel carrier was added to each sample prior to digestion.
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| Samples were digested in concentrated Nitric acid. After digestion, sample pH was adjusted and Nickel-63 was precipitated selectively with Dimethylglyoxime. Precipitates were selectively separated, redissolved, and residual acid was effectively neutralized. Sample residuals were placed into scintillation vials, scintillation cocktail was added and Nickel-63 activity was determined by beta liquid scintillation.
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| Samples demonstrated acceptable results for all Nickel-63 analyses. The Nickel-63 method blank demonstrated an acceptable result. Results for the Nickel-63 duplicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Nickel-63 laboratory control sample demonstrated an acceptable percent recovery.
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| GAMMA SPECTROSCOPY Samples for Gamma Spectroscopy analysis were prepared by transferring a known mass of each homogenized sample to a standard geometry container. Samples were counted on High Purity Germanium (HPGe) gamma ray detectors.
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| Page 2 of 3
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| ANALYTICAL RESULTS CONTINUED GAMMA SPECTROSCOPY CONTINUED Samples demonstrated acceptable results for all gamma-emitting radionuclides as repo1ied. The method blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228 and Bismuth-214 replicate demonstrated a high relative percent difference; however, normalized difference is within acceptable limits for the analytical technique. Results for the Potassium-40 replicate demonstrated an acceptable relative percent difference and normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated an acceptable percent recovery.
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| CERTIFICATION OF ACCURACY I ce1iify that this data report is in compliance with the terms and conditions of the Purchase Order, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the cognizant project manager or his/her ee to be accurate as verified by the following signature.
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| M.R. McDougall Laboratory Manager Date: 11/6/2019 Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please visit http://eberlineanalytical.com/ to provide us with feedback on our services.
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| Page 3 of 3
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| Printed: 10/30/2019 3:09 PM Page 1 of 21 Report To: Work Order Details:
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| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
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| 677118 *----"*_, _______
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| "-'-'"---------~~- -------------*--"*--* ,_,_, ____
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| Final Report of Analysis 2701 Deborah Ave ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-01 LCS KNOWN 09/05/19 00:00 1017/2019 19-09014 Tritium LANL ER-210 Modified 7.56E+OO 19-09014-01 LCS SPIKE 09/05/19 00:00 1017/2019 19-09014 Tritium LANL ER-210 Modified 7.99E+OO 1.48E+01 5.58E+OO 19-09014-02 . MBL BLANK 09/05/19 00:00 1017/2019 19-09014 Tritium LANL ER-210 Modified 3.31E+OO 3.32E+OO 5.58E+OO u
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| -~-~---~-------~*------" --~ *~*---*---. **-*-*-~~*-
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| 19-09014-03 DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 1017/2019 19-09014 Tritium LANL ER-210 Modified 3.19E+OO 3.19E+OO 5.38E+OO u 06/03/19 1017/2019 19-09014 Tritium LANL ER-210 Modified 3.17E+OO 3.18E+OO 5.37E+OO u
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| ~----"'*---- -~
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| 1017/2019 19-09014 Tritium LANL ER-210 Modified 3.29E+OO 3.29E+OO 5.71E+OO u 1017/2019 19-09014 Tritium 3.35E+OO 5.59E+OO u 1017/2019 19-09014 Tritium 3.19E+OO 5.58E+OO u 1017/2019 19-09014 Tritium 5.48E+OO u 19-09014-09 TRG 19-09014 Tritium LANL ER-210 Modified 5.53E+OO u 19-09014-10 TRG 19-09014 Tritium LANL ER-210 Modified 5.47E+OO u 19-09014-11 TRG 19-09014 Tritium LANL ER-210 Modified 5.45E+OO u 19-09014-12 TRG Tritium LANL ER-210 Modified 5.41E+OO u 1017/2019 Tritium LANL ER-210 Modified 3.20E+OO 5.59E+OO u 19-09014-14 1017/2019 Tritium LANL ER-210 Modified 3.07E+OO 5.30E+OO u 19-09014-15 1017/2019 Tritium 3.23E+OO 5.58E+OO u 19-09014-16 TRG L 1-10221 D-FIGS-014-SS-A 1017/2019 Tritium 3.19E+OO 5.52E+OO u 1-----------*****'"----------*--**--+-----*********-+*****---*-+--*********-----*****>***-*--*---*+
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| 19-09014-17 TRG L 1-102210-QIGS-013-SS-A 07/09/19 08:51 1017/2019 Tritium 3.12E+OO 5.36E+OO u
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| ---**----*******-------****--+----...;********--*-*........;-*-*****-:*-**--*******;*******-*--+**-**---****-*-----i-----'.,----****-------=-----..;___ _:...::...::..... -J 19-09014-18 TRG L 1-102210-FIGS-013-SS-A 07/09/19 08:51 10/8/2019 Tritium 3.17E+OO 5.39E+OO u TRG L1-10221D-FIGS-018-SS-A 07115/19 13:45 9/3/2019 10/8/2019 Tritium 3.16E+OO 5.49E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
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| ( "1fJ>
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| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
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| Printed: 10/30/2019 3:09 PM Page 2 of 21 Report To: Work Order Details:
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| Patricia Giza 19-09014 Eberline Analytical Zion Solutions Purchase Order:
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| SDG:
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| 677118
| |
| ----"---------~-,mm,-
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| Final Report of Analysis -------**
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| 2701 Deborah Ave Analysis Category: ~'ll'IRONMENTAL _________________________ _
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| Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-01 LCS KNOWN 09/05/19 00:00 9/3/2019 10/23/2019 19-09014 Nickel-63 ASTM 3500-Ni Modified 1.48E+03 4.44E+01 pCi/g 19-09014-01 LCS SPIKE 09/05/19 00:00 9/3/2019 10/23/2019
| |
| * 19-09014 Nickel-63 ASTM 3500-Ni Modified 1.47E+03 1.28E+01 8.75E+01 3.23E+OO 19-09014-02 MBL BLANK 09/05/19 00:00 , 9/3/2019 10/23/2019 19-09014 Nickel-63 ASTM 3500-Ni Modified -2.24E+OO 1.85E+OO 1.85E+OO 3.29E+OO u 19-09014-03 DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 10/24/2019 19-09014 ________________
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| Nickel-63 , ASTM 3500-Ni Modified -1.49E+OO 1.90E+OO 1.91E+OO 3.36E+OO u
| |
| -------= -------,
| |
| 19-09014-04 DO L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 10/24/2019. 19-09014 Nickel-63 ASTM 3500-Ni Modified -3.48E-01 1.92E+OO 1.92E+OO 3.33E+OO u
| |
| ------*------*-*-----"-------* ---------------------,-0,-~-----------: ------
| |
| 19-09014-05 TRG L 1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 10/24/2019 19-09014 Nickel-63 ASTM 3500-Ni Modified -6.21E-01 1.95E+OO 1.95E+OO 3.40E+OO u 1--****------------+-**-----------**--****-----*----***---+--------------,-----------*-*-----------*****-c-*------*-***-***------+**-*
| |
| 19-09014-06 ,_ _:i:i'<.<3______ L1-1022_1,8-.:.~~GS-006-SS-A ----+-0_61__ 1o_,_19_1_3_:3_5 --~3!2.°-19 10/24/2019 19-0901_~--, ___ __f:li_:~':_l-6_3_-l-****A_S_T_M_____35__o_o_-.N -1.50E+OO 1.92E+OO 1.92E+OO
| |
| ____i _M_od_i_fie_d___,----------**-*-*-*--**-****'*--*-*--*-*-**-- 3.38E+OO u
| |
| ,__1_9_-0_9_0_14-_0_7___T_R_G_____ ~_1_:_1_ 0221.~:~~_G_S_-_00_7~_s_-_A____ ''' _ 06/1~/1912:3~_!)~3.:~1?, _1_0,_2_41_2_01_9__1_9-_0_90_1_4 Nickel-63 2.14E+OO 3.52E+OO u L 1-10221C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 10/24/2019 19-09014 Nickel-63 2.03E+OO 3.46E+OO u
| |
| ,----------------*--**--*--------*-*-----*-----*---+----- - - - - + - - - - :..---~-----
| |
| L1-102201-FJGS-001-SS-A 06/27/19 09:40 9/3/2019 10/24/2019. 19-09014 Nickel-63 2.06E+OO 3.51E+OO u L 1-102201-FJGS-002-SS-A 06/27/19 09:42 10/24/2019 1.87E+OO 1.87E+OO 3.30E+OO u L 1-102201-FJGS-004-SS-A 06/27/19 09:46 10/24/2019 Nickel-63 1.96E+OO 1.96E+OO 3.40E+OO u L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 10/24/2019 Nickel-63 1.98E+OO 1.98E+OO 3.43E+OO u L 1-102210-FIGS-004-SS-A 06/27/19 09:36 Nickel-63 2.14E+OO 2.14E+OO 3.65E+OO u
| |
| ----r-----
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| 19-09014-14 TRG
| |
| ---- L 1-10220H-FJGS-004-SS-A 07/09/19 08:20 Nickel-63 2.03E+OO 2.03E+OO 3.50E+OO u 19-09014-15 TRG L 1-102210-FIGS-010-SS-A 07 /09/19 08:45 Nickel-63 2.12E+OO 2.13E+OO 3.53E+OO u 19-09014-16 TRG L 1-10221 D-FIGS-014-SS-A 07 /09/19 08:53 Nickel-63 1.92E+OO 1.92E+OO 3.37E+OO u 1 19-09014-17 L 1-102210-QIGS-013-SS-A 07/09/19 08:51 19-09014 Nickel-63 1.93E+OO 1.94E+OO 3.39E+OO u
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| - - - - - - ~ - - - ,. . . _, _________________
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| 19-09014-18 TRG L 1-10221 D-FIGS-013-SS-A 07/09/19 08:~ 9/3/2019 1_0_,2_4_12_0_1_9-*-19-09014--
| |
| -+ -----------
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| Nickel-63 2.07E+OO 2.07E+OO 3.61E+OO u 19-09014-19 TRG L1-10221D-FIGS-018-SS-A 07/15/19 13:45 i 9/3/2019 , 10/24/2019, 19-09014 ; Nickel-63 2.12E+OO 2.12E+OO 3.66E+OO u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
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| Printed: 1013012019 3:09 PM Page 3 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| "~~~-*~------,--",m'""=---*~-= -**** -****,. --..--*-**---..-*********-****---*-
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| Final Report of Analysis " " ' , ,_,,,_ ._ . ___
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| 2701 ------~,- Deborah Ave __ '"'"**----
| |
| ....- ...., ...... Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date , Date ID Analyte Method Result cu CSU MDA Qualifier Units
| |
| ~9-09,914:.°-~--L_c_s __ **- K!'_o_w_N______________ ___0~1£5-l:1:1.£°-°-~--~3/2019 10/11/2019 19-£~°-1*~- ~:ro_nt_iu_m-_9<!___ EIChroM SRW01 Modified , 5.02E+01 2.81E-01 pCi/g
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| 19-09014-03 DUP L1-10220A-FSGS-006-SS-A 06/03/19 06:55 . 9/3/2019 10/11/2019 19-09014 Strontium-90 EIChroM SRW01 Modified 3.09E-01 3.75E-01 3.90E-01 9.22E-01 U pCi/g
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| 19-09~-- , ..*. TRG _ L1-10220A-FSGS-016-SS-A **-**-* 06/03/19 07:15 9/3/2019 10/11/2019 : 19-09014 __s_t_r_o__n___n__u_m_-_9_0-+-E_IC_h_r_o__M ____s__
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| 19-09014-06 TRG L1-102218-FSGS-006-SS-A 06/10/19 13:35 : 9/3/2019 10/11/2019 19-09014 Strontium-90 EIChroM SRW01 Modified , 5.69E-02 3.44E-01 : 3.44E-01 8.75E-01 U pCi/g
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| ~~=TRG- *;:1--1-02-2-1D:F--JG-S--0-07--S-S---A-****--*-*-~/1912:30 i 9/3/2019 10/11/2019 19-09014 Strontium-90 EIChroM SRW01 Modified 7.41E-01 3.63E-01 4.45E-01 8.34E-01 U pCi/g
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| 19-09014-11 TRG L1-1022DI-FJGS-004-SS-A 06/27/19 09:46 ! 9/3/2019 ' 10/11/2019: 19-09014 Strontium-90 EIChroM SRW01 Modified i -2.22E-01 3.35E-01 3.43E-01 8.90E-01 U pCi/g 1 1 19-09014-12 TRG L1-10220H-FJGS-001-SS-A 06/27/1909:48 9/3/2019 10/11/2019 19-09014 Strontium-90 EIChroMSRW01 Modified 1.73E-01 2.97E-01 i 3.03E-01 7.40E-01 U pCi/g 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 06/27/19 09:36 j 9/3/2019 10/11/2019 19-09014 1 Strontium-90 EIChroM SRW01 Modified 1.98E-01 3.63E-01 ; 3.69E-01 9.06E-01 U pCi/g
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| 19-09014-15 TRG L1-102210-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 10/11/2019 19-09014 Strontium-90 EIChroM SRW01 Modified ' 4.57E-01 ' 4.70E-01 4.96E-01 1.14E+OO U pCi/g 19-09014-16 : TRG L1-10221D-FIGS-014-SS-A 07/09/190~9/3/2019 . 10/11/2019 19-09014 ! Strontium-90 EIChroMSRW01 Modified 3.49E-01 , 3.29E-01 , 3.50E-01 7.96E-01 U pCi/g
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| :=1=9=-0=9=01=4-=1=9==l==T=R=G===----*-----~--1-=--1_0-=2-2_~1_0*-=--F_1-G:s_--_o-=1*8_--s_-s:-A:_*:=*=---~-T::*_0*1_=1_1-5_i_1_-9_1_3_:4_5_-~:_91_3_t2_01_9__,_'_1_0,_1_1,_20_1_9_____1_9_:o9014 1 Strontium-90 EIChroM SRW01 Modified 2.38E-01 : 3.78E-01 3.87E-01 9.38E-01 U pCi/g 1-------*--*-+-*----**--*-------------------1---------~------~'---~-----*""<-----**- + - - - - - - - - - - - ~ - - - - - - - - - - - - - ~ - - - - - - - - * - * * * - - - * - * * * * - - - - - - - - - 1
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| -o_9_01__4_-0_1__+*--*L_c_s____ K_N__o__w_N______________________, ___0_9_10_51_19 00:00 9/3/2019 9/13/2019 19-09014 _____c_o_b_a_1t_-6_0_..,._ __E __P__A_9__0_1_.1_M_o_d_ified_~__ 11._31_1E_+o__2___..___s_.1_0E_+_o_o~j_____________________P_C_i1g_......
| |
| 14-01 LCS KNOWN 09/05/19 00:00 : 9/3/2019 9/13/2019 19-09014 i Cesium-137 EPA 901.1 Modified 8.26E+01 3.39E+OO / pCi/g 14-01 LCS SPIKE 09/05/1900:00 ~ 0 1 9 I 9/-13-/2-0-19___1_9_-0_90_1_4~,--*C;;-balt-60 EPA901.1 Modified 1.42E+02 i 1.03E+01 : 1.26E+01 8.42E-01 pCi/g
| |
| ,__19--0-9-0-14--0-*1-"'1*--L-C-s*---.....--S-P-IK-E*-***--------***-*-<--o-9*10*5-,1-9*0*0,-oo-l 9/3/2019 9/13/2019 --19-09014 Cesium*---13*7--<c---E-PA_9_0_1__1*-M-*o-d-ifi*-,e-d-+--8-.5-2.-E+--o-1*-*1-9___3_3_E_+o*o~-1-.0-3_E_+_o1----1.-06_E_+_o_o__________p_C_i/_g___,
| |
| CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Ouplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 4 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| ~~~-,-*---"--~-~-----*------" ,,, ._ " r n V O - - A , o ' - ,_ _. _ _ , _ ,__ ,____________ *---------
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report 10 Type 10 Date Date Date 10 Analyte Method Result cu CSU MOA Qualifier Units 19-09014-02 MBL BLANK 09/05/19 00:00 9/3/2019 Actinium-228 2.37E-02 1.44E-01 u 19-09014-02 MBL BLANK 09/05/19 00:00 9/3/2019
| |
| -------------- ,.--------*-------~----
| |
| Silver-108m 2.38E-02 3.47E-02 u 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 Americium-241 EPA 901.1 Modified 3.62E-02 4.79E-02 u
| |
| ------*---- -------~ *--*-----***------- ___ ----*--*-*
| |
| 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 Barium-133 EPA 901.1 Modified 1.33E-02 3.53E-02 u 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 Bismuth-214 EPA 901.1 Modified 5.74E-02 8.51E-02 u
| |
| "" ~-------*----~--*--------*---*-*-*-----
| |
| 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 Cobalt-60 EPA 901.1 Modified 2.23E-02 4.21E-02 u 19-09014-02 MBL BLANK 9/13/2019 19-09014 Cesium-134 EPA 901.1 Modified 3.00E-02 4.13E-02 u
| |
| . --------***-------*---*..... ------------- -*-------*-- -*-----*~------"'------*
| |
| 19-09014-02 MBL BLANK 09/05/19 9/13/2019 19-09014 Cesium-137 EPA 901.1 Modified 2.18E-02 2.19E-02 4.69E-02 u
| |
| -----c--------- ---------------,---*-* -"'----~--
| |
| 19-09014-02 MBL BLANK 09/05/19 00:00 9/3/2019 9/13/2019 19-09014 : Europium-152 EPA 901.1 Modified 6.SOE-02 6.SOE-02 6.10E-02 u
| |
| ---------------------' --------- . ---------*----*-------------- ----~.~----------------
| |
| 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 EPA901.1 Modified 1.07E-01 1.07E-01 3.11E-02 u 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 EPA 901.1 Modified 2.92E-02 2.92E-02 4.33E-02 u
| |
| ---------------,------=----------------,---
| |
| 19-09014-02 MBL BLANK 09/05/19 00:00 9/13/2019 19-09014 Holmium-166m EPA901.1 Modified 4.01E-02 4.01E-02 3.07E-02 u 19-09014-02 MBL BLANK 9/13/2019 lodine-129 EPA 901.1 Modified 1.11E-01 1.58E-01 u 19-09014-02 MBL 9/1312019 Potassium-40 3.50E-01 3.50E-01 4.67E-01 u 19-09014-02 .,_ MBL BLANK 9/13/2019 1.33E-02 1.33E-02 1.85E-02 u 19-09014-02 MBL BLANK 1.89E-02 1.89E-02 3.19E-02 u 19-09014-02 MBL BLANK Niobium-94 EPA901.1 Modified 1.86E-02 1.86E-02 3.40E-02 u 19-09014-02 MBL BLANK Lead-210 EPA 901.1 Modified 4.00E-01 4.00E-01 6.21E-01 u
| |
| --------- *-----------------~
| |
| 19-09014-02 MBL BLANK Lead-212 EPA 901.1 Modified 3.84E-02 6.37E-02 u 19-09014-02 MBL BLANK Lead-214 EPA901.1 Modified 3.66E-02 6.35E-02 u 19-09014-02 MBL BLANK EPA 901.1 Modified 7.26E-02 1.06E-01 u 19-09014-02 MBL BLANK EPA 901.1 Modified 5.74E-02 8.51E-02 u 19-09014-02 MBL BLANK EPA901.1 Modified 7.32E-02 1.06E-01 u 19-09014-02 MBL BLANK EPA901.1 Modified 2.20E-01 2.84E-01 2.84E-01 4.46E-01 u 19-09014-02 MBL BLANK EPA901.1 Modified 1.93E-02 6.39E-02 6.39E-02 1.03E-01 u 19-09014-02 MBL BLANK EPA901.1 Modified 9.55E-02 9.55E-02 1.47E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MOA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;OUP=Ouplicate;TRG=Normal Sample;OO=Ouplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 5 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions ......
| |
| SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL so Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report
| |
| : Analyte Method Result cu CSU MDA Qualifier ID : Type ID Date Date Date ID Units 19-09014-03 ; DUP L 1-10220A-FSGS-006-SS-A 06/03119 06:55 9/312019 9/1312019 19-09014 Actinium-228 EPA 901.1 Modified 2.63E-01 1.89E-01 1.90E-01 3.60E-01 u pCi/Q 19-09014-03 : DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Silver-108m
| |
| - *-- ---*-* -~*
| |
| EPA 901.1 Modified 1.36E-02 5.48E-02 5.48E-02 5.68E-02 u pCi/g
| |
| ~----*----*---------------*-*---------------~--"---------------
| |
| 19-09014-03 DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 j Americium-241 EPA 901.1 Modified -7.23E-02 8.08E-02 8.09E-02 1.11E-01 u pCi/g 19-09014-03 : DUP L 1-10220A-FSGS-006-SS-A 06/03119 06:55 9/312019 9/13/2019 19-09014 Barium-133 EPA 901.1 Modified -1.00E-02 1.58E-02 1.58E-02 1.18E-01 u pCilg
| |
| ----~----*"*-*-*------* -----*-*--=*----*-*------------*-----*---------,, ------*- - --
| |
| 19-09014-03 ; DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/1312019 19-09014 Bismuth-214 EPA 901.1 Modified 3.07E-01 1.38E-01 1.39E-01 2.55E-01 pCi/g 19-09014-03 : DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9113/2019 19-09014 Cobalt-60 EPA 901.1 Modified
| |
| ' 5.68E-02 6.0SE-02 6.0SE-02 6.81E-02 u pCilg
| |
| - *------------'---~~~ *-**--------'""'"'"-- -----*
| |
| 19-09014-03 DUP L 1-10220A-FSGS-006-SS-A 06103119 06:55 9/3/2019 9/1312019 19-09014 Cesium-134 EPA 901.1 Modified 4.14E-03 2.18E-02 2.18E-02 8.21E-02 u pCi/g
| |
| --*---,;*--*------*-*-------~-----*---*---*----- '
| |
| 19-09014-03 '. DUP L 1-10220A-FSGS-006-SS-A 06/03119 06:55 9/3/2019 9113/2019 19-09014 Cesium-137 EPA 901.1 Modified 5.03E-02 6.22E-02 6.22E-02 9.83E-02 u pCilg 19-09014-03 i DUP L 1-10220A-FSGS-006-SS-A 06103/19 06:55 9/3/2019
| |
| ----------0------*--*
| |
| 9/13/2019 19-09014 ' Europium-152 EPA 901.1 Modified 8.87E-03 9.18E-02 9.18E-02 1.71E-01 u pCilg 19-09014-03 i DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 : 9/3/2019 , 9/13/2019 19-09014 : Europium-154 EPA 901.1 Modified 3.58E-02 1.57E-01 1.57E-01 8.78E-02 u pCi/g 19-09014-03 i DUP L 1-10220A-FSGS-006-SS-A 06/03119 06:55 ; 9/3/2019 9/13/2019 19-09014 : !:***--'**- 155 EPA 901.1 Modified : 6.44E-02 9.02E-02 9.03E-02 1.36E-01 u pCi/g 19-09014-03 ' DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 ! 19-09014 : Holmium-166m EPA901.1 Modified i 1.41E-02 : 9.84E-02 9.84E-02 6.12E-02 u pCi/g 19-09014-03 DUP ' L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 : lodine-129 EPA 901.1 Modified -5.87E-02 5.95E-02 5.95E-02 8.19E-02 u pCi/g 19-09014-03 , DUP : L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 :. 9/3/2019 9/13/2019 19-09014 ! Potassium-40 EPA901.1 Modified ; 7.14E+OO 1.23E+OO 1.28E+OO 2.83E-01 pCi/g 19-09014-03 DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 i *o C
| |
| EPA 901.1 Modified -2.38E-02 ' 7.39E-02 1.40E-02 1.14E-01 u pCi/g 19-09014-03 : DUP . L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 913/2019 9113/2019 19-09014 I "UO M
| |
| EPA 901.1 Modified 2.52E-02 : 4.51E-02 4.52E-02 6.20E-02 u pCi/g
| |
| ' I 19-09014-03 DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Niobium-94 EPA901.1 Modified i 1.75E-02 3.89E-02 3.89E-02 6.96E-02 u pCi/g 19-09014-03 DUP L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 / Lead-210 6.32E-01 6.33E-01 9.95E-01 u pCi/g
| |
| : 9/3/2019 EPA9011t;H-~-01 19-09014-03 [ DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/13/2019 ' 19-09014 i Lead-212 EPA 901.1 -01 1.16E-01 1.18E-01 1.45E-01 pCilg 19-09014-03 f DUP : L1-1 *- -.... -.... - ~~.
| |
| 06/03/19 06:55 9/3/2019 9/13/2019 ' 19-09014 : Lead-214 EPA901.1 . 1E-01 i 1.27E-01 1.28E-01 2.43E-01 pCilg 19-09014-03 ! DUP : L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9113/2019 19-09014 : Promethium-145 EPA 901.1 Modified 1.48E-02 l 7.13E-02 7.13E-02 1.06E-01 u pCi/g 19-09014-03 : DUP L1-1 *- -.... -
| |
| ~~ ~~
| |
| 06/03/19 06:55 9/3/2019 : 9/13/2019 19-09014 : Radium-226 EPA901.1 Modified 3.07E-01 : 1.38E-01 : 1.39E-01 2.55E-01 pCi/g 19-09014-03 I DUP L1-10220A-FSGS-006-SS-A 06/03/19 06:55 ! 9/3/2019 9/13/2019 19-09014 i Antimony-125 EPA 901.1 Modified 3.34E-02 1.29E-01 1.29E-01 1.88E-01 u pCi/g 19-09014-03 i DUP L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Thorium-234 EPA 901.1 Modified 1.04E+OO i 7.09E-01 7.11E-01 1.11E+OO u
| |
| * pCilg 19-09014-03 i DUP_,,_, ___: L 1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 : 9/13/2019 19-09014 j Thallium-208 EPA 901.1 Modified 3.39E-01 . 1.41E-01 : 1.42E-01 1.11E-01 pCi/g 19-09014-03 l DUP L1-10220A-FSGS-006-SS-A 06/03/19 06:55 ! 9/3/2019 , 9/13/2019 19-09014 J Uranium-235 EPA 901.1 Modified l 1.94E-02 2.18E-01 2.18E-01 3.25E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 6 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order 677118 Final Report of Analysis 2701 _____
| |
| Deborah
| |
| " ___, _____ __ Ave ,
| |
| -------------- _Analysis Category:.. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019
| |
| ---------,m,_,,_
| |
| 19-09014 Actinium-228 EPA 901.1 Modified 4.09E-01 2.16E-01 2.17E-01 4.37E-01 u pCi/g
| |
| -----------------w ~
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Silver-108m EPA901.1 Modified 3.50E-03 6.64E-02
| |
| ""_, _ _ _ """' '""'"'"""""w - - ~ - *-, _ _ _, - * - - - - - - - - - - - - , _ ,_ _ _ ,,_ ',w., - * * - - * - - - - - ~ - - - - - " 'W __ , SWw,_"""'""""' "" ___ ,
| |
| ______ 19-09014-04 .. . ____D() ....... -~:~~~~:FSGS-006--~~_+/-:___ _ 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Americium-241 EPA 901.1 Modified -5.86E-02 1.11E-01
| |
| ----~-------*-
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Barium-133 EPA 901.1 Modified -3.15E-03 2.97E-02 ' _______________
| |
| _____2.97E-02
| |
| '" 1.31 E-01 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Bismuth-214 EPA901.1 Modified 4.84E-01 1.37E-01 1.39E-01 2.04E-01 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Cobalt-60 EPA 901.1 Modified 3.65E-02 5.87E-02 5.87E-02 9.00E-02 U
| |
| ,------ *------- ----------------~ ____ ,_____ . ----'-""----~ ,,_ -------- . _____ ,_,_____ ,-----~,-,--- ,_________ ,_,, - ,-,,-----------."'-""'_________ ---*------*----------------------!
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Cesium-134 EPA 901.1 Modified 1.14E-03 2.70E-02 2.70E-02 1.04E-01 U 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/13/2019 5.87E-02 6.90E-02 6.91E-02 1.09E-01 U
| |
| "'---------"'----~---,------------------- -+----*-------------------*---*----*-----------*---*---------,-----------------------,--
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 6.59E-02 6.59E-02 1.78E-01 U
| |
| --.-,------~-''"'"'"-""''"-"""'_____ -------1-------*-**---+... ---------.----.*---------.,.-.-;.__.___,____.__._,-j ....-.._ _.____._._,-.,_,_ _ .___-:.._ _ _ _ _._,._._.__ _,.__._,_,,~--*---*-*-*--*--.-,-.------.---.-.---.--.,--,-**--*
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 EPA 901.1 Modified 1.00E-01 1.00E-01 9.05E-02 U
| |
| ---+------------*--------C---------------------*-------:-----'-----l------*----*------------------*-+-------*---*---------**--c-----------------**---*------------
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 EPA901.1 Modified 1.21E-01 1.84E-01 U 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 EPA 901.1 Modified 1.15E-01 1.15E-01 6.79E-02 U 19-09014-04 DO 19-09014-04 DO
| |
| "'""""' ______ L1-10220A-FSGS-006-SS-A u 19-09014-04 DO L1-10220A-FSGS-006-SS-A u DO L1-10220A-FSGS-006-SS-A u DO L1-10220A-FSGS-006-SS-A 9/3/2019
| |
| -------*--------+--------------,-----~------------~-----*----+---
| |
| 9/13/2019 EPA901.1Modified 1.22E+OO ,..,_, ________
| |
| u pCi/g DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 EPA901.1 Modified 1.26E-01 1.80E-01 pCi/g DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 9/3/2019 9/13/2019 EPA 901.1 Modified 1.05E-01 1.95E-01 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 , 9/3/2019 9/13/2019 EPA 901.1 Modified 1.04E-01 u DO L1-10220A-FSGS-006-SS-A
| |
| ----*---~-----------
| |
| 06/03/19 06:55 9/3/2019 9/13/2019 19-09014 Radium-226 EPA 901.1 Modified 2.04E-01 pCi/g 1---------*---------*-----D--O---L--1---1-0-2--2-*0-A---F-SG-S----00--6--S-S---A------+---06/03/19 06:55 -- : 9/3/2019 9/13/2019 19-090141;-_An_ti_m-on-y*--1-2-5--+--*--------------,------------,--------,--*----~----2--.3-8-E--0*1-~--------,----
| |
| u 00 L1-10220A-FSGS-006-SS-A 06/03/~~~~:55 -i ~_312019
| |
| * 9/13/2019 19-09014 !--Thoriu-;;;:2-34-;----*------~---*-------------,-------1-.-11_E_+_00-------- u 19-09014-04 , DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 ' 9/3/2019 9/13/2019 19-09014 i Thallium-208
| |
| --+------*+-------------+---- 1.46E-01
| |
| -+-----__;____________________ 2.56E-01 1-------+-------'-------------*
| |
| 19-09014-04 DO L1-10220A-FSGS-006-SS-A 06/03/19 06:55 I 9/3/2019 9/13/2019 19-09014 ' Uranium-235 2.51E-01 3.64E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 7 of 21 Report To: Work Order Details:
| |
| Patricia Giza Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| -- --~--------"-----,-.-,
| |
| Final Report of Analysis -**
| |
| 2701 Deborah Ave
| |
| - * -
| |
| * w,_,, _ _ _ _ _ _ _ _ _
| |
| * _,_ Analysis. Category: .. _...
| |
| Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report Date Date Analyte Method Result cu CSU MDA Qualifier ID Type ID Date ID Units 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 Actinium-228 3.42E-01 5.00E-01 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 Silver-108m 7.15E-02 6.71E-02 u
| |
| --*----------*-~---------------*-*
| |
| 19-09014-05 TRG L 1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 9.87E-02 1.32E-01 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 9.04E-02 9.82E-02 u
| |
| ----------------------~--~--
| |
| 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 Bismuth-214 EPA 901.1 Modified 1.13E-01 1.14E-01 2.07E-01
| |
| *---0--------------*-----*-----*--*---*--***-- -*-------------+--* -**---------------------*-*--***-
| |
| 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 Cobalt-60 EPA 901.1 Modified 5.75E+OO 4.53E-01 5.41 E-01 1.52E-01 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 Cesium-134 EPA 901.1 Modified 9.15E-03 3.89E-02 3.90E-02 7.68E-02 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/1907:15 9/3/2019 9/13/2019 19-09014 Cesium-137 EPA901.1 Modified 4.39E-02 7.07E-02 7.07E-02 1.10E-01 u
| |
| --------- ------ "www*--~*-- --+----**-**--------,----**--*-*-**.:____,,__ _
| |
| 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/3/2019 9/13/2019 19-09014 EPA901.1 Modified 3.99E-02 1.90E-01 1.90E-01 1.89E-01 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 9/13/2019 19-09014 EPA901.1 Modified -8.82E-03 1.33E-01 1.33E-01 9.91E-02 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/1907:15 19-09014 EPA901.1 Modified 1.34E-01 1.01E-01 1.02E-01 1.35E-01 u 19-09014-05 TRG L 1-10220A-FSGS-016-SS-A 06/03/19 07:15 19-09014 Holmium-166m EPA901.1 Modified
| |
| _________. ,________________,________________________ _,________________f-------+-----------------*--*-----------t------------------+------------------------------------- 6.93E-02 1.17E-01 1.17E-01 6.81E-02 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 lodine-129 EPA901.1 Modified 2.68E+OO 1.14E+01 1.14E+01 3.11E+OO u
| |
| ------------,,------------------------,--+-----------;------------------------------------*-----+---------------------------------------*-,-------------------------------------------
| |
| 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/1907:15 EPA901.1 Modified 1.42E+OO 1.48E+OO 1.15E+OO 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 06/03/19 07:15 -5.09E-02 9.84E-02 9.84E-02 1.39E-01 u 19-09014-05 TRG L1-10220A-FSGS-O16-SS-A 06/03/19 07:15 3.59E-02 5.77E-02 5.78E-02 6.00E-02 u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A EPA 901.1 Modified 3.24E-01 2.03E+OO u 19-09014-05 TRG L1-10220A-FSGS-016-SS-A EPA901.1 Modified 2.33E-01 19-09014-05 TRG L1-10220A-FSGS-016-SS-A EPA 901. 1 Modified 1.49E-01 1.50E-01 3.02E-01 19-09014-05 TRG L1-10220A-FSGS-016-SS-A EPA901.1 Modified 5.96E-01 5.96E-01 8.82E-01 u pCi/g 19-09014-05 TRG L1-10220A-FSGS-016-SS-A 1.13E-01 1.14E-01 2.07E-01 TRG L1-10220A-FSGS-016-SS-A 1.30E-01 1.30E-01 2.15E-01 u TRG 9.50E-01 9.50E-01 1.26E+OO u TRG 8.34E-02 8.39E-02 1.21E-01 TRG 06/03/19 07:15 3.21E-01 3.21E-01 4.22E-01 u CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 8 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave
| |
| * * - - = ' - ' " = N e N , _ , , _ _ """"""'"
| |
| _l\naty~!s C_a_te_qory: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier ID Units 19-09014-06 TRG L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Actinium-228 EPA 901-1 Modified 5,11E-01 1,87E-01 1-89E-01 3,85E-01 19-09014-06 TRG L1-102218-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Si1ver-108m 1-76E.02 2,91E-02 2_92E-02 5,69E-02 u
| |
| -----------~*~ ,, --"-----* ---"''""'*-------~---"'---*-----
| |
| 19-09014-06 TRG L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Americium-241 EPA 901-1 Modified -8,90E-02 6,88E-02 6_89E-02 9.10E-02 u 19-09014-06 TRG L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Barium-133 EPA 901-1 Modified 5_52E-02 6,72E-02 6.72E-02 9A1E-02 u
| |
| ----------......:---*-""-*-*-------------*-*---*~-, ~-- --------------------0-- -------*"-**-- ~' ,_ ,,,,,~---****-----,----------
| |
| 19-09014-06 TRG L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Bismuth-214 EPA 901 _1 Modified 3,0SE-01 1-31E-01 1-32E-01 2,18E-01 19-09014-06 TRG L1-102218-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Cobalt-60 EPA901_1 Modified 2,72E-02 7.0SE-02 7_05E-02 USE-01 u 19-09014-06 TRG
| |
| --------------*----"-'"\"'_' L 1-10221 B-FSGS-006-SS-A
| |
| _______________ =------------------ 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 Cesium-134 EPA 901-1 Modified -1.37E-01 7.81E-02 7_84E-02 773E-02 u 19-09014-06 TRG .________
| |
| L 1-10221---<-*-------
| |
| B-FSGS-006--SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 2,83E-01 8,00E-02 8.13E-02 1-05E-01 19-09014-06 TRG L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 19-09014 7_03E-03 USE-01 1-35E-01 1.45E-01 u
| |
| ----------------------=-'='
| |
| 19-09014-06 TRG L 1-102218-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 EPA 901.1 Modified -7.31E-02 2.04E-01 2,04E-01 7.30E-02 u 19-09014-06 TRG L 1-102218-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 EPA 901-1 Modified 1.15E-01 6.86E-02 6.88E-02 1.30E-01 u L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/3/2019 9/13/2019 EPA901.1 Modified 7,81E-02 7.81E-02 5.61E-02 u L 1-102218-FSGS-006-SS-A 06/10/19 13:35 9/13/2019 EPA 901.1 Modified 1,89E-01 1.76E-01 1.77E-01 2,55E-01 u l 1-102218-FSGS-006--SS-A 06/10/19 13:35 9/13/2019 EPA 901.1 Modified 1.15E+01 2.44E+OO 2,52E+OO 1.54E+OO L 1-10221 B-FSGS-006-SS-A 06/10/19 13:35 9/13/2019 EPA 901.1 Modified 1.63E-02 4_87E-02 8.39E-02 u pCi/g L1-102218-FSGS-006--SS-A 06/10/19 13:35 9/13/2019 EPA 901.1 Modified -1.84E-02 4,0SE-02 6.24E-02 u pCi/g L1-10221 B-FSGS-006--SS-A EPA 901-1 Modified 8.98E-03 4.19E-02 6,52E-02 u L1-10221 B-FSGS-006-SS-A EPA 901-1 Modified 1,02E+OO 8.63E-01 1A2E+OO u L 1-10221 B-FSGS-006-SS-A EPA 901-1 Modified 3.75E-01 8,06E-02 1.43E-01 L 1-10221 B-FSGS-006-SS-A EPA90U 2.43E-01 1.00E-01 1.77E-01 pCi/g L 1-10221 B-FSGS-006-SS-A EPA 901.1 Modified 1.55E-01 1.09E-01 1_09E-01 1.68E-01 u 19-09014-06 TRG L 1-102218-FSGS-006--SS-A EPA 901.1 Modified 3,0SE-01 1-31E-01 1.32E-01 2.18E-01 i u 19-09014-06 ;
| |
| --------' ___TRG L 1-10221 B-FSGS-006-SS-A EPA 901.1 Modified 6.40E-02 1.34E-01 1.34E-01 1.99E-01 19-09014-06 , TRG L 1-10221 B-FSGS-006-SS-A Thorium-234 EPA 901-1 Modified 6,57E-01 5.63E-01 5_64E-01 8.70E-01 u 19-09014-06 +. TRG L1-102218-FSGS-006--SS-A Thallium-208 EPA 901,1 Modified 3.32E-01 1.65E-01 2.56E-01 19-09014-06 TRG L 1-102218-FSGS-006--SS-A Uranium-235 EPA 901-1 Modified 1.02E-01 1.91E-01 1.91E-01 2,94E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect (1fJ; EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 1013012019 3:09 PM Page 9 of 21 Report To: Wolk Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions
| |
| " ' _ _ _ _ _ _w _ _ u , o r n SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave Analysis Category: ___ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-07 TRG L 1-102210-FJGS-007-SS-A 06/18/19 12 :30 9/3/2019 9/13/2019 EPA 901.1 Modified 1.13E+OO 5.38E-01 5.41E-01 1.00E+OO 19-09014-07 TRG L1-102210-FJGS-007-SS-A ---""'"' __________
| |
| 06/18/19 12:30 9/3/2019
| |
| -'.---,-w~,
| |
| 9/13/2019 19-09014 Silver-108m
| |
| ---*---*-----=- ____,__ ,"_ -- - EPA 901 .1 Modified 1.01E-01 1.31E-01 1.31E-01 2.22E-01 u 19-09014-07 TRG L 1-102210-FJGS-007-SS-A 06/18/19 12:30 9/3/2019 9/13/2019 19-09014 Americium-241 EPA901.1 Modified -2.62E-01 2.00E-01 2.00E-01 2.68E-01 u
| |
| --~---¥*---------*--------,--
| |
| 19-09014-07 TRG L 1-10221 D-F J GS-007 -SS-A 06/18/19 12:30 9/3/2019 9/13/2019 19-09014 Barium-133 EPA 901.1 Modified 3.76E-03 9.79E-02 9.79E-02 3.25E-01 u 19-09014-07
| |
| -----~--------*
| |
| TRG _________ , ________________ '----------------*~--------~~---------------
| |
| "" " ' " ' " - - - - ' r n = - - - " ' " " " ' " - - ~ , - - ,
| |
| L 1-10221 D-F JGS-007 -SS-A 06/18/19 9/3/2019 9/13/2019 19-09014 Bismuth-214 EPA 901.1 Modified 1.33E+OO 3.56E-01 3.63E-01 5.62E-01 19-09014-07 TRG L 1-10221 D-FJGS-007-SS-A 06/18/19 12:30 9/3/2019 9/13/2019 19-09014 Cobalt-60 EPA 901.1 Modified 2.16E+OO 2.38E-01 2.63E-01 2.65E-01 19-09014-07 TRG L1-10221 D-F JGS-007-SS-A 06/18/19 12:30 9/3/2019 9/13/2019 19-09014 Cesium-134 EPA901.1 Modified 3.45E-02 9.81E-02 9.81E-02 2.43E-01 u 19-09014-07 TRG L 1-10221 D-F JGS-007 -SS-A 06/18/19 12:30 9/3/2019 9/13/2019 EPA 901.1 Modified 1.06E+01 1.22E+OO 1.34E+OO 4.28E-01 19-09014-07 TRG
| |
| ~----*-------- """'" _______________
| |
| L 1-102210-FJGS-007-SS-A 06/18/19 12:30 9/3/2019 9/13/2019 EPA 901.1 Modified 9.64E-02 4.29E-01 4.29E-01 4.73E-01 u 19-09014-07 TRG L1-102210-FJGS-007-SS-A 06/18/19 12:30 9/13/2019 EPA 901.1 Modified -5.54E-03 3.40E-01 3.40E-01 2.46E-01 u 19-09014-07 TRG L 1-10221 D-FJGS-007-SS-A 06/18/19 12:30 9/13/2019 EPA 901.1 Modified 1.18E-01 2.38E-01 2.38E-01 3.47E-01 u
| |
| ----------- ,------------------- . -------*'"''""' -~"'"--------*-.-
| |
| 19-09014-07 TRG L 1-10221 D-F JGS-007 -SS-A 06/18/19 12:30 9/13/2019 EPA901.1 Modified -4.99E-02 2.50E-01 2.50E-01 1.76E-01 u 19-09014-07 TRG L1-102210-FJGS-007-SS-A 06/18/19 12:30 9/13/2019 EPA 901.1 Modified 2.72E-01 1.70E-01 1.70E-01 2.58E-01 u 19-09014-07 TRG L1-10221 D-F JGS-007-SS-A 06/18/19 12:30 9/13/2019 EPA 901.1 Modified 2.04E+01 3.08E+OO 3.26E+OO 1.58E+OO
| |
| ---- : -*---- . ----------~---------.
| |
| TRG L1-10221 D-F JGS-007-SS-A 06/18/19 12:30 9/13/2019 EPA 901.1 Modified 2.28E-01 2.00E-01 2.00E-01 3.28E-01 u TRG L 1-10221 D-F JGS-007-SS-A 06/18/19 12:30 EPA 901.1 Modified 5.87E-02 1.33E-01 1.33E-01 1.44E-01 u TRG L 1-10221 D-F JGS-007 -SS-A EPA 901.1 Modified -6.49E-02 1.38E-01 1.38E-01 1.89E-01 u 19-09014-07 TRG L 1-10221 D-FJGS-007-SS-A Lead-210 EPA 901.1 Modified 1.61E+OO 1.61E+OO 2.68E+OO u 19-09014-07 TRG L 1-10221 D-FJGS-007-SS-A Lead-212 EPA 901.1 Modified 4.04E-01 4.13E-01 6.09E-01 19-09014-07 TRG L 1-102210-FJGS-007-SS-A EPA 901.1 Modified 3.53E-01 3.59E-01 6.33E-01 19-09014-07 TRG L 1-10221 D-F J GS-007-SS-A EPA 901.1 Modified 1.29E-01 1.29E-01 2.92E-01 u 19-09014-07 TRG L 1-102210-FJGS-007-SS-A 3.56E-01 3.63E-01 5.62E-01 19-09014-07 TRG L 1-10221 D-F JGS-007 -SS-A 06/18/19 12:30 5.91E-01 5.91E-01 7.98E-01 u 19-09014-07 TRG L 1-102210-FJGS-007-SS-A 06/18/19 12:30 1.78E+OO 1.78E+OO 2.67E+OO u 19-09014-07 TRG L1-102210-FJGS-007-SS-A 06/18/19 12:30 Thallium-208 EPA 901.1 Modified 3.05E-01 3.07E-01 4.94E-01 19-09014-07 TRG L1-10221 D-FJGS-007-SS-A 06/18/19 12:30 Uranium-235 EPA901.1 Modified -9.70E-02 5.90E-01 5.90E-01 9.50E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( "'M>
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 1013012019 3:09 PM Page 10 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118
| |
| -~-----,m"""--,=--**-*--------*-*
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 Actinium-228 EPA 901.1 Modified 2.38E-01 1.61E-01 1.61E-01 3.01E-01 u
| |
| -------------------------------------------------- - '"'"''""'+*----- ---------~------s--- "' """""'-'"
| |
| L1-10221 C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 Silver-108m EPA 901.1 Modified
| |
| - ----~,--wrne-_,___,~, -3A9E-02 4.12E-02 4.13E-02 5.38E-02 u 19-09014-08 TRG L1-10221C-FIGS-101-SS-A
| |
| ---~-----------"*~---------~----*-*-*-*---------*
| |
| 06/24/19 9/3/2019 9/13/2019 19-09014 Americium-241 EPA 901.1 Modified
| |
| "'"''' ,,,,----------+-------------------
| |
| 9.80E-02 9.80E-02 1.25E-01 u 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 06/24/19 09:00 , 9/3/2019 , 9/13/2019 19-09014
| |
| -----------------------------*"""'___ --~-------~~-----------~---' -*-----~--" ----------~*-------
| |
| Barium-133 3.10E-02 3.10E-02 7.91E-02 u 19-09014-08 TRG L1-10221 C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 Bismuth-214 EPA 901. 1 Modified 3.04E-01 1.08E-01 1.09E-01 1.84E-01
| |
| """-"""" ,----------------------------------------+-----
| |
| 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 Cobalt-60 EPA 901. 1 Modified 2A5E-01 5.59E-02 5.73E-02 6.76E-02 19-09014-08 TRG L1-10221 C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 Cesium-134 EPA 901.1 Modified 1.30E-02 2.24E-02 2.24E-02 5.57E-02 u 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 Cesium-137 EPA 901.1 Modified 1.06E+OO 1A8E-01 1.58E-01 1.07E-01 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 9/13/2019 19-09014 EPA 901.1 Modified 1.06E-01 1.78E-01 1.67E-01 U
| |
| -------------------------------------------------- ------1-----------------+-----~------------------------------1------------------------- -----------------c------------s-----------------------------------'-__;;'---1 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 9/13/2019 19-09014 EPA 901.1 Modified -4.58E-02 1.26E-01 1.26E-01 8.65E-02 U
| |
| --------"4" ___,________.------------------'"------,-----------------------+-------------------------------+------------------------------ -i----------------------------------------------------1 TRG L1-10221C-FIGS-101-SS-A 9/13/2019 19-09014 EPA 901. 1 Modified UOE-01 9.50E-02 9.52E-02 1.30E-01 u TRG L1-10221C-FIGS-101-SS-A 9/13/2019 19-09014 EPA 901. 1 Modified -7.37E-03 7.15E-02 7.15E-02 6.64E-02 u TRG L1-10221C-FIGS-101-SS-A 9/13/2019 19-09014 EPA 901.1 Modified 1.28E-01 3.64E+OO 3.64E+OO 3.38E+OO u 19-09014 EPA 901.1 Modified 7.85E+OO 1A6E+OO 1.51E+OO 1.35E+OO 19-09014 EPA 901.1 Modified 6.31E-04 4.73E-02 4.73E-02 7A2E-02 19-09014 EPA 901.1 Modified -3.75E-03 3.59E-02 5.52E-02
| |
| _________ ,"" _________ Niobium-94 EPA 901.1 Modified 2A4E-02 3A3E-02 3A3E-02 5A1E-02 19-09014-08 TRG L1-10221 C-FIGS-101-SS-A EPA 901.1 Modified 1A3E+OO 2.27E+OO 19-09014-08 TRG L1-10221C-FIGS-101-SS-A Lead-212 EPA 901.1 Modified 1.53E-01 19-09014-08 TRG L1-10221C-FIGS-101-SS-A Lead-214 EPA 901.1 Modified 2.14E-01 19-09014-08 TRG L1-10221 C-FIGS-101-SS-A EPA 901.1 Modified 9.89E-01 u 19-09014-08 TRG L1-10221C-FIGS-101-SS-A EPA 901.1 Modified 1.84E-01 19-09014-08 TRG L1-10221C-FIGS-101-SS-A EPA 901.1 Modified 1.80E-01 u 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 1.20E+OO u pCi/g 19-09014-08 TRG L1-10221C-FIGS-101-SS-A 06/24/19 09:00 EPA90U 9.59E-02 19-09014-08 L1-10221C-FIGS-101-SS-A 06/24/19 09:00 9/3/2019 Uranium-235 3.74E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( "'M>
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 11 of21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118
| |
| ,oc,--,--"--"'*--'"'"'"'""""'"-"
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category:_ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-09 TRG L 1-10220l-FJGS-001-SS-A 06/27/19 09:40 Actinium-228 7_55E-01 19-09014-09 TRG L 1-10220l-FJGS-001-SS-A Silver-108m 1_25E-01 u TRG L 1-102201-FJGS-001-SS-A 1_59E-01 u 1.81E-01 u 19-09014 2_35E-01 2_37E-01 3.66E-01 19-09014-09 TRG l 1-102201-FJGS-001-SS-A 06/27/19 09:40 9/13/2019 19-09014 1.31E-01 1_34E-01
| |
| --------------------------------------t--------
| |
| 19-09014-09 TRG l 1-102201-FJGS-001-SS-A 06/27/19 09:40 9/13/2019
| |
| ,w*--=--"-'""''""m",-~,-,"*m*-+-------------*---*-------0***-----------**-*-*---*-
| |
| 3_91E-02 3_91E-02 1.51E-01 u 19-09014-09 TRG L1-10220l-FJGS-001-SS-A 06/27/19 9/13/2019 1_91E-01 19-09014-09 TRG L 1-10220l-FJGS-001-SS-A 2.43E-01 u
| |
| ' ~---------"--------------
| |
| TRG L 1-10220l-FJGS-001-SS-A 1.24E-01 u TRG l 1-102201-FJGS-001-SS-A 2.31E-01 TRG l 1-10220l-FJGS-001-SS-A 1_06E-01 u TRG L 1-102201-FJGS-001-SS-A 4.43E-01 u TRG l 1-10220l-FJGS-001-SS-A 1.45E+OO TRG L 1-10220l-FJGS-001-SS-A 1.38E-01 u TRG L 1-10220I-FJGS-001-SS-A 6.31E-02 6.31E-02 1.0SE-01 u TRG L1-10220I-FJGS-001-SS-A 7.41 E-02 7.41 E-02 1_07E-01 u TRG L 1-102201-FJGS-001-SS-A 1 _63E+OO 1.64E+OO 2.56E+OO TRG l 1-10220I-FJGS-001-SS-A 1_54E-01 1_58E-01 2_90E-01 TRG l 1-102201-FJGS-001-SS-A 1.92E-01 1 _95E-01 3.48E-01 TRG L 1-10220I-FJGS-001-SS-A 1.30E-01 1.30E-01 2_84E-01 L 1-102201-FJGS-001-SS-A EPA901_1 Modified 2.35E-01 2_37E-01 3_66E-01 l 1-102201-FJGS-001-SS-A EPA901_1 Modified 3_97E-01 l 1-10220l-FJGS-001-SS-A EPA901_1 Modified EPA 901 _1 Modified EPA901_1 Modified CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 12 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis **-******
| |
| 2701___ Deborah ,
| |
| Ave
| |
| __.. ,-,*-"'-"'"-*~~--------- Analysis ca.regory_:_ .. ENVIRONMENTAL so Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-10 TRG L 1-102201-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 Actinium-228 EPA 901.1 Modified 3.87E-01 1.39E-01 1.41E-01 2.55E-01
| |
| -----~-"""' ----
| |
| 19-09014-10 TRG ____ ____ ___
| |
| L 1-102201-FJGS-002-SS-A
| |
| "_" , 06/27 /19 09:42 9/3/2019 9/16/2019 19-09014
| |
| ------,.--------~----------~-----~-----*
| |
| Silver-108m
| |
| '"-' m,,*mm,-,--------*=""-"'"---
| |
| * EPA 901.1 Modified -3.57E-02 4.51E-02 4.51E-02 4.05E-02 0--------------------*** ""'
| |
| u ''"'"
| |
| pCi/g
| |
| ""*_,_,_,,~----
| |
| 19-09014-10 TRG L 1-102201-FJGS-002-SS-A 06/27 /19 09:42 9/3/2019 9/16/2019 19-09014 Americium-241 EPA 901.1 Modified 6.09E-02 8.95E-02 8.96E-02 1.22E-01 u pCi/g
| |
| ---*-*-*-*- "'""''**-*--------=~---------~"~---~---*-- '
| |
| 19-09014-10 TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 Barium-133 EPA 901.1 Modified -9.67E-02 6.87E-02 u
| |
| *---------------------------.-*--------,-----**-*--*---*--*=* ,-
| |
| 6.89E-02 6.41E-02 pCi/g 19-09014-10 TRG L 1-10220!-FJGS-002-SS-A
| |
| =*"'""--*-*--~---""_"_.,,_____" ' ' - - - * - - * - - ___ ____
| |
| 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 Bismuth-214
| |
| _______ "'---~----------*--,,.-,.--~-,-,, .. ,_,, --- I***-* EPA 901.1 Modified ; 3.79E-01 1.06E-01 1.0SE-01 1.50E-01 pCilg __
| |
| 19-09014-10 , TRG L 1-10220!-FJGS-002-SS-A 06/27/19" 09:42
| |
| -- ___ ,, .,.,. 9/3/2019 9/16/2019 19-09014 Cobalt-60 EPA 901.1 Modified : 1.04E-01 3.38E-02 3.42E-02 5.0SE-02 pCi/g 19-09014-10 TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 , 19-09014 Cesium-134 EPA 901.1 Modified -6.60E-03 1.92E-02 1.92E-02 4.42E-02 u pCi/g 19-09014-10 *-----*=---"
| |
| -----*---< TRG ____________ L1-10220!-FJGS-002-SS-A
| |
| .,_____________ 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 Cesium-137 EPA 901.1 Modified 3.70E-01 8.50E-02 8.70E-02 9.95E-02 pCi/g 19-09014-10 TRG L 1-10220!-FJGS-002-SS-A
| |
| , ____. 06/27/19 09:42 i
| |
| 9/3/2019 9/16/2019 19-09014 Cui .... ,., ..... 11-152 EPA901.1 Modified : 1.11E-01 1.14E-01 1.14E-01 1.50E-01 u pCi/g 19-09014-10 TRG L1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 : 19-09014 . Eu,~~*~*,,_ 54 EPA901.1 Modified I -2.09E-02 6.50E-02 6.50E-02 7.64E-02 u pCi/g 19-09014-10 ' TRG L 1-102201-FJGS-002-SS-A
| |
| *- "'"'"'------~---*---*----,_-,
| |
| 06/27 /19 09:42 9/3/2019 : 9/16/2019 19-09014
| |
| * Eu,~~*~* ,,_ , 55 EPA 901.1 Modified : 1.02E-01 8.47E-02 8.48E-02 1.15E-01 u pCi/g 19-09014-10 i TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 i Holmium-166m EPA 901.1 Modified i -1.41E-03 5.68E-02 5.68E-02 5.78E-02 u pCi/g 19-09014-10 TRG L1-102201-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 lodine-129 EPA901.1 Modified 6.91E-01 ; 4.19E+OO 4.19E+OO 2.73E+OO u pCi/g 19-09014-10 ! TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 i Potassium-40 EPA 901.1 Modified 1.04E+01 1.48E+OO 1.57E+OO 5.00E-01 pCi/g 19-09014-10 ! TRG L 1-102201-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 , , ....... !,1 ................... 5" EPA901+~;1~:02 3.64E-02 3.64E-02 6.34E-02 u pCi/g 19-09014-10 i TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019
| |
| --~-----*-,-
| |
| 9/16/2019 , 19-09014 , Molybdenum-93 EPA901. . -03 . 3.39E-02 3.39E-02 5.00E-02 u pCi/g 19-09014-10 j TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 9/3/2019 9/16/2019 19-09014 : Niobium-94 EPA 901.1 Modified 4.72E-03 3.54E-02 . 3.54E-02 4.SOE-02 u oCi/q 19-09014-10 TRG L1-10220!-FJGS-002-SS-A 06/27/19 09:42 i 9/3/2019 9/16/2019 ! 19-09014 Lead-210 EPA 901.1 Modified 2.32E+OO 1.68E+OO 1.68E+OO 2.69E+OO u pCi/g 19-09014-10 TRG L 1-102201-FJGS-002-SS-A 06/27/19 09:42 I 9/3/2019 9/16/2019 19-09014 ; Lead-212 EPA901.1 Modified 3.85E-01 8.99E-02 9.20E-02 1.87E-01 pCi/g 19-09014-10 : TRG L 1-102201-FJGS-002-SS-A 06/27 /19 09:42 9/3/2019 9/16/2019 19-09014 Lead-214 EPA 901.1 Modified i 4.61E-01 1.11E-01 1.14E-01 1.67E-01 pCi/g 19-09014-10 ! TRG L 1-102201-FJGS-002-SS-A 06/27 /19 09:42 i 9/3/2019 9/16/2019 19-09014 Promethium-145 EPA 901.1 Modified 5.14E-01 i 6.15E-01 6.16E-01 7.71E-01 u pCi/g i
| |
| 19-09014-10 j TRG L 1-10220!-FJGS-002-SS-A 06/27 /19 09:42 9/3/2019 : 9/16/2019 19-09014 Radium-226 EPA 901.1 Modified 3.79E-01 1.06E-01 1.DSE-01 1.50E-01 pCi/g 19-09014-10 I TRG L1-102201-FJGS-002-SS-A 06/27/19 09:42 i 9/3/2019 i 9/16/2019 19-09014 Antimony-125 EPA 901.1 Modified 7.84E-02 ; 8.25E-02 8.26E-02 1.53E-01 u pCi/g 19-09014-10 TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 i 9/3/2019 9/16/2019 19-09014 , Thorium-234 EPA901.1 Modified 1.07E-01 8.71E-01 ; 8.71E-01 1.14E+OO u pCi/g 19-09014-10 TRG L 1-10220!-FJGS-002-SS-A 06/27/19 09:42 i 9/3/2019 , 9/16/2019 19-09014 Thallium-208 EPA901.1 Modified 2.57E-01 i 7.41E-02 7.52E-02 8.21E-02 pCi/g i
| |
| 19-09014-10 i TRG L 1-102201-FJGS-002-SS-A 06/27/19 09:42 I 9/3/2019 9/16/2019 ; 19-09014 Uranium-235 EPA 901.1 Modified 4.63E-02 i 2.54E-01 2.54E-01 3.37E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ("M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 13 of 21 Report To: Worl< Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118 Final Report of Analysis ,..... __ , 2701___Deborah Ave
| |
| ---*, *-*-- - __ Analysis Category-. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units ID 19-09014-11 TRG L 1-10220!-F JGS-004-SS-A 06/27/19 09:46 9/3/2019 : 9/16/2019 19-09014 Actinium-228 ___________
| |
| EPA901.1,,, Modified 5.86E-01 1.87E-01 1.89E-01 3.28E-01 pCi/g
| |
| """'"' _ _ _ _ , _ _ .,,_,n _ _ , , ,
| |
| 19-09014-11 TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 i 9/3/2019 9/16/2019 19-09014 Silver-108m EPA901.1 Modified 1.90E-02 4.81E-02 4.81E-02 7.75E-02 u pCi/g f*- **-ue,*-----*----------~,m* ,__ -----" ~-**---,-*---*--* -----*-*----*
| |
| 19-09014-11 TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 19-09014 Americium-241 EPA 901.1 Modified -172E-02 7.08E-02 7.08E-02 1.00E-01 u pCi/g
| |
| ---------*--- *-------~--------*-------------~- *----*-----**--~
| |
| 19-09014-11 TRG L1-102201-FJGS-004-SS-A 06/27 /19 09:46 9/3/2019 9/16/2019 19-09014 Barium-133 EPA901.1 Modified 2.12E-03 2.98E-02 . 2.98E-02 1.04E-01 u pCi/g 19-09014-11 TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 : 9/3/2019 9/16/2019 19-09014 Bismuth-214 EPA 901.1 Modified 5.65E-01 1.26E-01 1.30E-01 1.63E-01 pCi/g
| |
| ---- '' --~--------*--- ------------"" -
| |
| 19-09014-11 TRG L1-102201-FJGS-004-SS-A
| |
| -*,w----,-~,-,_"
| |
| 06/27/19 09:46 : 9/3/2019 9/16/2019 19-09014 Cobalt-60 EPA 901.1 Modified 1.04E-01 7.27E-02 7.29E-02 1.36E-01 u pCi/g f.,,-""'"'""'"' """'_'_'='"')'"-'' ___,_,,
| |
| 19-09014-11 L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/16/2019 Cesium-134
| |
| "---"-' EPA901.1 Modified 2.22E-03 3.15E-02 3.15E-02 8.46E-02 u TRG : 9/3/2019 19-09014 pCi/g
| |
| ****-***-*-*- --------"-~---**-------------- -- :
| |
| 19-09014-11 TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 : 9/16/2019 19-09014 Cesium-137 EPA 901.1 Modified 5.35E-01 i 9.81E-02 1.02E-01 9.68E-02 pCi/g
| |
| --*--""'<-~----*----------- ------~---"'*
| |
| 19-09014-11 TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 i 9/3/2019 9/16/2019 19-09014 Europium-152 EPA 901.1 Modified i -5.58E-02 i 1.86E-01 1.86E-01 1.56E-01 u pCi/g
| |
| ----------------*-----..--*-------,---..-------*--~--*-
| |
| 19-09014-11 TRG L1-102201-FJGS-004-SS-A 06/27 /19 09:46 : 9/3/2019 9/16/2019 19-09014 Europium-154 EPA 901.1 Modified i 3.40E-02 : 1.65E-01 1.65E-01 7.95E-02 u - pCi/g 19-09014-11 TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 19-09014.. .,..,.. Europium-155 EPA901.1 Modified 1.60E-01 9.57E-02 9.60E-02 1.47E-01 pCi/g
| |
| -**---*---- -------*-------------..---------*--- ----*~-.--,
| |
| 19-09014-11 TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 , 9/16/2019 19-09014 Holmium-166m EPA 901.1 Modified 4.06E-02 4.08E-02 i 4.09E-02 6.87E-02 u pCi/g
| |
| ~~*--*-**-*-'-*---- *--*-----~----,
| |
| 19-09014-11 TRG L1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 19-09014 lodine-129 EPA 901.1 Modified : -7.51E-02 i 1.89E-01 1.89E-01 2.69E-01 u pCi/g
| |
| - --*------- ' ----------~---*..-* --------~- i 19-09014-11 TRG L1-10220!-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 19-09014 ' Potassium-40 EPA901.1 Modified 1.35E+01 i 2.70E+OO 2.79E+OO 1.22E+OO pCi/g
| |
| ---------*--,,._,,,,-, -~---------..--- ------ i 19-09014-11 TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 19-09014 *s-* < EPA901.1 Modified 1.54E-02 ! 5.48E-02 i 5.48E-02 9.22E-02 u pCi/g 19-09014-11 : TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 ' 9/16/201 19-09014 .. _, M EPA 901.1 Modified i 5.SOE-03 i 2.SOE-02 2.SOE-02 6.35E-02 u pCi/g 19-09014-11 TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019
| |
| * 9/16/2019 19-09014 ' Niobium-94 EPA 901.1 Modified 1.67E-02 4.24E-02 4.24E-02 6.62E-02 u pCi/g u
| |
| 19-09014-11 TRG L1-10220!-FJGS-004-SS-A 06/27 /19 09:46 9/3/2019 9/16/2019 19-09014 1 Lead-210 EPA901.1 Modified i 9.63E-01 8.22E-01 . 8.24E-01 1.36E+OO pCi/g
| |
| """'"'-"'"-"'"''"'""'-*"'--"*-------"--------*,wm,,_
| |
| 19-09014-11 TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 9/312019 ! 911612019 19-09014 : Lead-212 EPA901.1 Modified 4.52E-01 i 9.76E-02 1.00E-01 1.79E-01 pCi/g 19-09014-11 i ______
| |
| TRG ___ , L 1-102201-FJGS-004-SS-A __.. 06/27/19 09:46 9/3/2019 i 9/16/2019 19-09014 Lead-214 EPA 901.1 Modified 4.0SE-01 i 1.06E-01 1.08E-01 1.80E-01 pCVg 9-09014-11 TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 i 9/3/2019 : 9/16/2019 19-09014 Promethium-145 EPA 901.1 Modified 3.58E-02 1.22E-01 i 1.22E-01 1.81E-01 u pCi/g 19-09014-11 i TRG L 1-10220!-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 i 9/16/2019 19-09014 Radium-226 EPA 901.1 Modified 5.65E-01 1.26E-01 : 1.30E-01 1.63E-01 pCi/g 19-09014-11 i TRG L 1-10220I-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 , 19-09014 i Antimony-125 EPA 901.1 Modified -2.81E-02 / 1.64E-01 i 1.64E-01 2.23E-01 u pCi/g 11 TRG L1-10220!-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 : 19-09014 Thorium-234 EPA 901.1 Modified i 5.31E-01 . 6.38E-01 : 6.39E-01 9.63E-01 u pCi/g i
| |
| 19-09014-11 i TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 i 9/16/2019 19-09014 Thallium-208 EPA901.1 Modified 3.76E-01 i 1.73E-01 1.74E-01 2.63E-01 pCi/g 19-09014-11 i TRG L 1-102201-FJGS-004-SS-A 06/27/19 09:46 9/3/2019 9/16/2019 19-09014 \ Uranium-235 EPA 901.1 Modified 1.12E-01 ! 2.36E-01 : 2.36E-01 . 3.54E-01 u i pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10130/2019 3:09 PM Page 14 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118 Final Report of Analysis
| |
| -- v, 2701 Deborah Ave .... .. .. Analysis Category: __ .. ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Analyte Method Result cu CSU MDA Qualifier ID : Type Date Date Date ID Units 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019
| |
| ,. _________ ,,, 19-09014 Actinium-228 EPA 901.1 Modified 4A5E-01 2.69E-01 2.70E-01 4.80E-01 u pCi/g
| |
| "" ----------*--- , e ' " - " _,,_, _ _ _ _ . _ . _ _ _ _ , _ _.,___.----~*
| |
| 19-09014-12 TRG L1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 Silver-108m EPA 901.1 Modified -4A2E-02 6.63E-02 6.63E-02 1.11E-01 __ u
| |
| *-*-*--*----,., ~---*--* *----*-~*-~*~=------*----*---,mvrn,, '"-""""*-- --------*- ,,,_,
| |
| 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 Americium-241 EPA 901.1 Modified ' -8.38E-02 U7E-01 1.17E-01 L63E-01 u pCi/g 19-09014-12
| |
| --*---~
| |
| TRG
| |
| *---- -*---* -~----*****---*
| |
| L 1-10220H-FJGS-001-SS-A 06/27/19 09:48
| |
| . 9/3/2019 9/16/2019 19-09014 , Barium-133
| |
| ---1--,,-,.
| |
| EPA901.1 Modified 1.08E-02
| |
| . 4.26E-02 4.26E-02 1.90E-01 u pCi/g 19-09014-12 TRG L1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 Bismuth-214 EPA 901.1 Modified 3.89E-01 2.18E-01 2.19E-01 3.38E-01 pCi/g 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 . 9/3/2019 9/16/2019 19-09014 Cobalt-60 EPA 901.1 Modified 2.03E-01 9.54E-02 9.60E-02 2.09E-01 u pCi/g
| |
| ----------*-*-- *-*------*-- wwOV-o""
| |
| *-*==*-----,,.--~,,.--e-,~~--------.;""" -------------------- t...-.--~- - - - - - - - - - - - - - -
| |
| 19-09014-12 TRG --------------_,,_ __________ -------------
| |
| L 1-10220H-FJGS-001-SS-A 06/27 /19 09:48 9/3/2019 9/16/2019 19-09014 ; Cesium-134 EPA 901.1 Modified : 1.77E-02 4.73E-02 4.73E-02 1.34E-01 u pCi/g 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 Cesium-137 EPA 901.1 Modified 1.00E+OO 1.88E-01 1.95E-01 1.71E-01 pCi/g
| |
| -----------,-.,-----~-*---- *-----
| |
| 19-09014-12 TRG ,L,1-10220H-FJGS-001-SS-A
| |
| ,,_,,,,,,,-----------~ 06/27/19 09:48
| |
| ----~------
| |
| 9/3/2019 9/16/2019
| |
| -------~"-----------
| |
| Europium-152 EPA 901.1 Modified ! 7.19E-02 2.42E-01 2.42E-01 2.54E-01 u pCi/g 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 ; 9/3/2019 9/16/2019 19-09014 ~u1 .... ~, .. ,11- l54 EPA 901.1 Modified -4.35E-02 2.40E-01 2.40E-01 1.33E-01 u pCi/g 19-09014-12 i TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 . 9/3/2019 9/16/2019 19-09014 , Europium-EPA 901.1 Modified 1.05E-01 1.38E-01 1.38E-01 2.06E-01 u pCi/g 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27 /19 09:48 : 9/3/2019 9/16/2019 19-09014 ! Holmium-166m EPA 901.1 Modified 6.91E-03 1.22E-01 1.22E-01 9.65E-02 u pCi/g 19-09014-12 TRG L1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 : lodine-129 EPA 901.1 Modified 2.90E-02 9.04E-02 9.04E-02 1.36E-01 u pCi/g
| |
| -*----------~ . ----- --------------------- :
| |
| 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 ; Potassium-40 EPA 901.1 Modified 1.05E+01 1.99E+OO 2.06E+OO 1.49E+OO pCi/g
| |
| 'i 19-09014-12 ; TRG L 1-10220H-FJGS-001-SS-A 06/27119 09:48 9/3/2019 9/16/2019
| |
| -{--*------,----*, ---*-------=-
| |
| 19-09014 i Manganese-54 EPA 901.1 Modified 5.01E-04 9.53E-02 9.53E-02 1.50E-01 u pCi/g 19-09014-12 TRG L1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 ! Molybdenum-93 EPA901.1 Modified ; 9.30E-03 : 5.48E-02 5.48E-02 9.86E-02 u pCi/g 19-09014-12 ; TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48
| |
| ; 9/3/2019 9/16/2019 19-09014 Niobium-94 EPA 901.1 Modified : -1.66E-02 ; 7.06E-02 7.06E-02 1.10E-01 u pCi/g 19-09014-12
| |
| * TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 Lead-210 EPA 901.1 Modified i 2.49E+OO ' 1.34E+OO 1.34E+OO 2.16E+OO u pCi/g 19-09014-12 TRG L 1-10220H-FJGS-001-SS-A 06/27 /19 09:48 9/3/2019 9/16/2019 19-09014 Lead-212 EPA 901.1 Modified i 6.94E-01 1.95E-01 1.99E-01 2.90E-01 pCi/g 19-09014-12
| |
| * TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 ; 9/3/2019 9/16/2019 19-09014 ' Lead-214 EPA 901.1 Modified i 4.05E-01 1.61E-01 1.63E-01 3.06E-01 pCi/g 19-09014-12 i TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48
| |
| ' 9/3/2019 9/16/2019 19-09014 ! ...... ''"" ......... 11- -,-..., EPA 901.1 Modified -1.18E-01 1.13E-01 1.14E-01 1.56E-01 u pCi/g 19-09014-12 ; TRG L 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 : Radium-226 EPA 901.1 Modified i 3.89E-01 2.18E-01 2.19E-01 3.38E-01 pCi/g 19-09014-12 : TRG l 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 i ,-,,.::, .. _ .. , .::: EPA 901.1 Modified -1.84E-02 . 2.65E-01 2.65E-01 3.64E-01 u pCi/g 19-09014-12 i TRG L .rn??m c '""'.flfl1-SS-A 06/27/19 09:48 9/3/2019 9/16/2019 19-09014 ; Thorium-234 EPA 901.1 Modified 1.58E+OO ; 1.89E+OO . 1.89E+OO 3.16E+OO u pCi/g 19-09014-12 TRG L1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019
| |
| * 9/16/2019 19-09014 J Thallium-208 EPA901.1 Modified 1.97E-01 1.59E-01 1.60E-01 3.40E-01 u pCi/g 19-09014-12 ! TRG l 1-10220H-FJGS-001-SS-A 06/27/19 09:48 9/3/2019 i 9/16/2019 19-09014 i u _,,,_,,, :::: EPA 901.1 Modified 8.79E-02 ! 3.62E-01 : 3.62E-01 5.46E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 15 of 21 Report To: Wotk Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical _ _ ,__ w ---
| |
| Zion Solutions Purchase Order:
| |
| SDG:
| |
| 677118
| |
| --~-----------------" ------'"'""'"''"-*----------~---- --*----- - ----------*-*-*----
| |
| Final Report of Analysis
| |
| -*=* , _ _2701 Deborah Ave
| |
| _ _,, ______________ ------- Analysis_Category: _____ E _____N
| |
| ______V
| |
| ____ IRONMENTAL Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09014-13 TRG L1-102210-FIGS-004-SS-A 06127/19 09:36 9/3/2019 9/16/2019 19-09014 Actinium-228 EPA 901 .1 Modified 9.53E-01 4.23E-01 1.08E+OO u
| |
| --------~-------,-------------*----*="=~-~----,--,
| |
| 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 06/27/19 09:36 9/3/2019 9/16/2019 19-09014 Silver-108m EPA901.1 Modified 6.28E-02 1.42E-01 u I--------+-*****-----------******-------------------***-+******************--**** ..
| |
| 19-09014-13 TRG L1-102210-FIGS-004-SS-A 9/16/2019 19-09014 Americium-241 EPA 901.1 Modified -2.23E-01 2.47E-01 2.97E-01 u
| |
| *-*--,.-*-'"""-**-*--* c*" _,,-,,m*------*-*-------"'"" ,_ ,------*-*-----*---------*
| |
| 19-09014-13 TRG L 1-102210-FIGS-004-SS-A 9/16/2019 19-09014 Barium-133 EPA901.1 Modified 1.86E-02 1.09E-01 2.12E-01 u EPA 901.1 Modified 2.70E-01 4.01E-01 EPA901.1 Modified 2.28E+OO 2.72E-01 2.29E-01 19-09014-13 TRG L1-102210-FIGS-004-SS-A 06/27/19 09:36 EPA 901.1 Modified 7.64E-03 4.93E-02 4.93E-02 1.10E-01 u
| |
| *--------------------------------------------------1------------+-----+----------"**---------------+----------------------i--*--------------------
| |
| 19-09014-13 TRG L1-102210-FIGS-004-SS-A 06/27/19 09:36 EPA 901.1 Modified 1.12E+O 1.23E+OO 2.84E-01 19-09014-13 TRG L1-10221D-FIGS-004-SS-A 06/27/19 09:36 EPA901.1 Modified 1.57E-01 4.31E-01 4.31E-01 u 19-09014-13 TRG L1-10221D-FIGS-004-SS-A EPA 901.1 Modified 1.46E-01 2.74E-01 2.74E-01 2.04E-01 u
| |
| ------*****--*--**-------***-J----***---i*-*--*----f----'-*****---'---;_**-*---+-*----*****-**--***-**--****~--------**<****---
| |
| 19-09014-13 I TRG L1-102210-FIGS-004-SS-A EPA 901.1 Modified 1.27E-01 1.14E-01 1.15E-01 3.12E-01 u l------~-----------------------
| |
| 19-09014-13 TRG L1-10221D-FIGS-004-SS-A EPA901.1 Modified -1.35E-01 1.74E-01 1.75E-01 1.66E-01 u 19-09014-13 TRG L1-102210-FIGS-004-SS-A EPA 901.1 Modified -1.25E+01 5.20E+01 5.20E+01 6.69E+OO u 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 06/27/19 09:36 EPA 901.1 Modified 2.28E+01 3.41E+OO 3.61E+OO 2.35E+OO 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 06/27/19 09:36 EPA901.1 Modified 1.15E-01 1.15E-01 2.02E-01 u 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 06/27/19 09:36 EPA901.1 Modified 7.31E-02 7.86E-02 7.87E-02 1.14E-01 u pCi/g 19-09014-13 TRG L1-102210-FIGS-004-SS-A 06/27119 09:36 EPA 901.1 Modified 8.63E-02 1.33E-01 u
| |
| --<--~-,--**-----*
| |
| 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A EPA 901.1 Modified 4.59E+OO 4.61E+OO 7.14E+OO 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 2.27E-01 2.34E-01 4.30E-01 19-09014-13 TRG L1-102210-FIGS-004-SS-A 3.26E-01 5.07E-01 1
| |
| 19-09014-13 TRG -,- L1-102210-FIGS-004-SS-A : 1.70E+OO 1.70E+OO 2.02E+OO u 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 2.60E-01 2.70E-01 4.01E-01 19-09014--13 TRG L1-102210-FIGS-004-SS-A 2.04E-01 4.86E-01 u 19-09014-13 TRG L1-10221 D-FIGS-004-SS-A 2.0SE+OO 2.85E+OO u 19-09014-13 TRG 2.06E-01 1.71E-01 pCi/g 19-09014-13 TRG 6.SOE-01 8.76E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( "'M> EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 16 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical SDG:
| |
| Final Report of Analysis Zion Solutions
| |
| -~--------------------"--- -****'
| |
| 2701 Deborah Ave
| |
| ------ - - Purchase Order:
| |
| - - Analysis Category: ____ ENV_IRQt.iMENIAL__ _ ___ _
| |
| ___ 677118
| |
| "'"-'""'"""*-------------- -----~------
| |
| '*--,-,"-" "---*--"-""""-"""-*-"-~--mm-Zion, IL 60099 Sample Matrix: SO Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 07/09/19 08:20 9/3/2019 9/16/2019 19-09014
| |
| '-------~-----------""'""'"""'"'""'-, ,, _, ________
| |
| Actinium-228 EPA 901.1 Modified 6.33E-01 2.40E-01 2.42E-01 5.09E-01
| |
| _1~-090_~~->-* TRG ___l:!.:.~~~20H-FJc:;_S-004-SS~---*-*--** - -- 07/091_~ 08:20 . ' -~0-~_()1~-~/2019 _19-09:'.~~. -- ~jlV_:'~:2~~m EPA 901.1 Modifi__,e_d____ _,_.....*-8.99E-03 6.83E-02
| |
| _ _ _~---****--*-*-***-- 6.83E-02 1.01E-01 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 07/09/1908:20 9/3/2019 9/16/2019 19-09014 Americium-241 EPA901.1 Modified -4.22E-02 9.58E-02 9.59E-02 1.35E-01 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 07/09/1908:20 9/3/2019 9/16/2019 19-09014 Barium-133 EPA901.1 Modified -7.34E-03 4.33E-02 4.33E-02 1.43E-01
| |
| ----*----****-* *-***************-**-*-----**---------*-********-* -*-*------* -----------****---------..,-------1-----------------*-***-*----*-***---*--*-----*-***-*>-*
| |
| 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 07/09/19 08:20 9/3/2019 9/16/2019 19-09014 Bismuth-214 EPA 901.1 Modified 5.90E-01 1.77E-01 1.SOE-01 2.74E-01
| |
| --,-"-"'"'" __ ,._m,.,,
| |
| 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 07/09/19 08:20 f , 9/16/2019 19-09014 Cobalt-60 EPA 901.1 Modified 1.72E-01 8.67E-02 8.71E-02 1.69E-01 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 19-09014 Cesium-134 EPA901.1 Modified -1.14E-02 3.18E-02 3.18E-02 1.25E-01 u 19-09014-14 TRG
| |
| -~--- L1-10220H-FJGS-004-SS-A 1.37E+OO 1.88E-01 2.01E-01 1.22E-01
| |
| "'"""'""'"*---------*---~
| |
| 19-09014-14 TRG 9.46E-03 2.75E-01 2.75E-01 2.14E-01 19-09014-14 TRG
| |
| --------------~:_-1_02_2_0H_-f'.::!G_s_-0_0_4-~~~---**-+-o_1_1_09_1 __
| |
| 19_o_s_:2__0__..;.**.* _. _ _ _ _ _ _ _ _ 19-
| |
| __o_9__0__1_4_-+*-*****-'------l---E ___P__A
| |
| __9_0__1__.1__;_M 1.63E-01
| |
| __ _;_o:..:d_;__ifi_;__ed;____..c,.--......c=--- 4*--*__.___;:_.....; __1.63E-01
| |
| _;__:..::::....:__ ____ __::..:.;._ _..:u 1.09E-01 19-09014-14 TRG___,____________
| |
| L1-10220H-FJGS-004-SS-A 07/09/19 _
| |
| ****--**-l*-_;___;__:__ 08:20 _i--__;:-: _ _ _ _ __;__:__ __ +---.:.. EPA 901.1 Modified
| |
| -,'.----:...:..:.....i-.::..----:..:: 9.15E-02
| |
| ..:::.::..:....__-i'***--_;__...:..:....*+-----_;__:_-:..:_:-:..,-._:.:..:_;_::..:.:: 2.03E-01 _____U 9.17E-02____..::__.:..:.::__:.: -:.
| |
| 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 1.0SE-01 1.0SE-01 9.32E-02 U pCi/g 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 2.63E-01 2.63E-01 3.91E-01 u pCi/g
| |
| - *------,-- ~ -r---*---------
| |
| 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 3.45E+OO 3.55E+OO 2.13E+OO 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 7.89E-02 7.89E-02 1.27E-01 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 5.43E-02 8.51E-02 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 6.45E-02 1.01E-01 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 1.07E+OO 1.69E+OO 19-09014-14 TRG L1-10220H-FJGS-004-SS-A 1.32E-01 2.14E-01 L1-10220H-FJGS-004-SS-A 1.42E-01 3.68E-01 1.83E-01 1.SOE-01 2.74E-01 9/3/2019 9/16/2019 I 19-09014 Antimony-125 2.30E-01 3.15E-01 19-09014-14 9/3/2019
| |
| -9/16/2019 19-09014 ! Thorium-234 19-09014-14 9/3/2019 9/16/2019 ! 19-09014 Thallium-208 pCi/g 19-09014-14 L1-10220H-FJGS-004-SS-A 07/09/19 08:20 9/3/2019 9/16/2019 19-09014 ; Uranium-235 EPA 901.1 Modified u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/ 481-0683 FAX 865/ 483-4621
| |
| | |
| Printed: 10/30/2019 3:09 PM Page 17 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG.
| |
| Purchase Order: 677118
| |
| -~------,----* .. """'"""'''"*""" ---*"-*--*------------*-*---**--**----* *****----**
| |
| Final Report of Analysis 2701 Deborah Ave Analysis Category: ENVIRONMENTAL ____ ,
| |
| Zion, IL 60099 Sample Matrix:
| |
| so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-15 TRG L1-102210-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 Actinium-228 :
| |
| ,, ___ EPA901.1 Modified 1.52E+OO 6.43E-01 6.48E-01 1.36E+OO pCi/g
| |
| -* --**---~----" ------------- ,---~-----
| |
| 19-09014-15 1---*-"'"""""---*----*-* __,___
| |
| TRG L 1-10221 D-FIGS-010-SS-A 07 /09/19 08:45 . 9/3/2019 9/16/2019 19-09014 Silver-108m ,,, __________________
| |
| EPA 901.1 Modified
| |
| ,,,, i 2.39E-02 : 1.36E-01 1.36E-01 2.19E-01 u pCi/g 19-09014-15 TRG L1-10221D-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 Americium-241
| |
| ~-~------------- :---*------- --. --*---------.----~------ --------*-------*
| |
| EPA901.1 Modified -1.83E-02 : 1.87E-01 1.87E-01 2.67E-01 u pCi/g 19-09014-15 TRG L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 Barium-133 EPA 901.1 Modified i 5.07E-02 1.10E-01 1.10E-01 3.18E-01 u pCi/g
| |
| " "'""" --------~-- *---------*- '-----,--""--------- *----- .
| |
| 19-09014-15 ; TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 Bismuth-214 EPA 901.1 Modified 1.17E+OO 3.05E-01 3.11E-01 1.60E-01 pCi/g
| |
| ---~-----------------,,,,,,*---*----- ,,,--------*--*-*
| |
| 19-09014-15 j TRG L1-102210-FIGS-010-SS-A 07 /09/19 08:45 9/3/2019 9/16/2019 19-09014 Cobalt-60 EPA 901.1 Modified 1.90E+OO 2.34E-01 2.54E-01 2.06E-01 pCi/g 19-09014-15 TRG L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 ; 9/3/2019 9/16/2019 19-09014 Cesium-134 EPA 901.1 Modified : -2.08E-02 i 8.0SE-02 8.0SE-02 2.41E-01 u pCi/g 19-09014-15 TRG L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 ; 9/3/2019 9/16/2019 19-09014
| |
| * Cesium-137 EPA901.1 Modified 8.29E+OO 9.SOE-01 1.07E+OO 4.18E-01 pCi/g 19-09014-15 TRG L 1-102210-FIGS-010-SS-A
| |
| -----,.........,,---*----------,---, 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 ' C,*---:**- """""
| |
| --* *r-*-*** 1'-'"- EPA901.1 Modified -7.94E-02 2.81E-01 2.81E-01 4.76E-01 u pCi/g 19-09014-15 : TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 C,*---:**-
| |
| *r-*-*** *1..,..,. EPA901.1 Modified -3.57E-01 3.84E-01 3.84E-01 2.43E-01 u pCi/g TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 ! 9/3/2019 9/16/2019 19-09014 C, -: .. -
| |
| --*-r-*-***'1'-''-'
| |
| "'"'"" EPA901.1 Modified i 2.57E-01 2.28E-01 2.28E-01 3.78E-01 u pCi/g
| |
| *----*--r------*-----*---------- :
| |
| 19-09014-15 TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 , Holmium-166m EPA 901.1 Modified 6.47E-02 2.37E-01 2.37E-01 1.66E-01 u pCi/g 19-09014-15 1 TRG L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 9/16/2019 19-09014 i lodine-129 EPA 901.1 Modified 2.76E-01 1.65E-01 1.66E-01 2.54E-01 u pCi/g 19-09014-15 : TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 9/16/2019 19-09014 j Potassium-40 EPA 901.1 Modified : 2.01E+01 .. 3.19E+OO 3.35E+OO 1.94E+OO pCi/g 19-09014-15 TRG L1-10221D-FIGS-010-SS-A 07/09/19 08:45 ; 9/3/2019
| |
| * 9/16/2019 19-09014 i .. *-* -~-* *-- : EPA901.1 Modified 1.25E-01 1.64E-01 1.64E-01 2.74E-01 u pCi/g 19-09014-15 TRG L1-10221D-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 i Molybdenum-93 EPA901.1 Modified -4.00E-02 1.47E-01 1.47E-01 1.37E-01 u pCi/g 19-09014-15 TRG L1-10221D-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 9/16/2019
| |
| * 19-09014
| |
| * Niobium-94 EPA 901.1 Modified 1.56E-01 1.38E-01 1.38E-01 1.79E-01 u pCi/g 19-09014-15 TRG L1-10221D-FIGS-010-SS-A 07 /09/19 08:45
| |
| 'i 9/3/2019 9/16/2019 ' 19-09014 i Lead-210 EPA 901.1 Modified 1.94E+OO 1.81E+OO 1.81E+OO 3.01E+OO u pCi/g 19-09014-15 TRG L1-10221D-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 Lead-212 EPA 901.1 Modified . 1.10E+OO i 2.53E-01 2.59E-01 5.51E-01 pCi/g 19-09014-15 TRG L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 9/16/2019 19-09014 i Lead-214 EPA 901.1 Modified 1.04E+OO 3.51E-01 3.55E-01 6.40E-01 pCi/g 19-09014-15 ; TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 9/16/2019 19-09014 j Promethium-145 EPA901.1 Modified 7.61E-02 1.54E-01 i 1.54E-01 2.88E-01 u pCi/g
| |
| ---- 1 19-09014-15 TRG L 1-102210-FIGS-010-SS-A
| |
| -*-------- 07/09/19 08:45 i 9/3/2019 : 9/16/2019 19-09014 Radium-226 EPA901.1 Modified i 1.17E+OO 3.05E-01 . 3.11E-01 1.60E-01 pCiig 19-09014-15 : TRG L 1-102210-FIGS-010-SS-A 07/09/19 08:45 9/3/2019 9/16/2019 19-09014 ; Antimony-125 EPA 901.1 Modified 6.02E-02 5.62E-01 5.62E-01 7.65E-01 u pCi/g 19-09014-15 TRG L 1-10221D-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 . 9/16/2019 19-09014 i Thorium-234 EPA 901.1 Modified 9.41E-01 1.76E+OO 1.76E+OO 2.62E+OO u
| |
| . pCi/g 19-09014-15 TRG i L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 : 9/3/2019
| |
| * 9/16/2019 19-09014 i ,: __:::__ -- EPA901.1 Modified 1.03E+OO
| |
| . 3.54E-01 3.57E-01 4.86E-01 pCi/g 19-09014-15 TRG l L 1-10221 D-FIGS-010-SS-A 07/09/19 08:45 i 9/3/2019 i 9/16/2019 19-09014 i Uranium-235 EPA 901.1 Modified -1.64E-01 6.42E-01 6.42E-01 9.20E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Normal Sample;DO=Duplicate Original;U=Non-detect
| |
| ( ~
| |
| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
| |
| | |
| Printed: 1013012019 3:09 PM Page 18 of 21 Report To: Work Order Details:
| |
| Patricia Giza 19-09014 Eberline Analytical Zion Solutions SDG:
| |
| Purchase Order: 677118 Final Report of Analysis 2701 Deborah Ave . Analysis. Category:_ ENVIRONMENTAL so w -------*---
| |
| Zion, IL 60099 Sample Matrix:
| |
| Lab Sample Client Sample Receipt Analysis Batch Report Analyte Method Result cu CSU MDA Qualifier ID Type ID Date Date Date ID Units 19-09014-16 TRG L1-10221D-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Actinium-228 EPA 901.1 Modified 4.27E-01 1.59E-01 1.60E-01 3.0SE-01 pCi/g 19-09014-16 TRG L1-10221D-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Silver-108m EPA 901.1 Modified 9.65E-04 1.67E-02 1.67E-02 4.61E-02 u
| |
| ------------~- .. ~"-**------h-----*""-""'_________ _
| |
| 19-09014-16 TRG L 1-102210-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Americium-241 EPA 901.1 Modified 5.99E-03 9.94E-02 9.94E-02 1.30E-01 u
| |
| -*"--*-----*- *'">***-*--*----- ow'""'~-------*-**----
| |
| 19-09014-16 TRG L1-10221D-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Barium-133 EPA901.1 Modified 1.13E-02 2.67E-02 2.67E-02 7.36E-02 u
| |
| ***-**1****9*-_*0*9**-0***1*4*-_*1**6*-*-'***********TR*****-*G**- -*---*-L1**-*10**-2_2_10 F__
| |
| IG-s*-*0-*1**4*---s-S--A-*-****-- --+--0-7 /0.9/19 08:53 : 9/3/2019 9/16/2019 19-09014 . . Bismuth-214 EPA 901.1 Modified 5.19E-01 1.11E-01 1.47E-01 19-09014~ TRG L 1-102210-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Cobalt-60 EPA 901.1 Modified 6.43E-02 4.09E-02 4.10E-02 1.01E-01 u
| |
| * * * * - - * - - - - - - - - - - - - - - - * * - - * - - * -------*****-*-- - - - - * - - - * - - - - - - - * * - * - - - - - * * - - * - - - * * * * .. +***--------*----*----,-----*-*---****,**-*----*-***-*****-**-****-----------*-***********************--*---**---I 19-09014-16 TRG L1-10221D-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Cesium-134 EPA 901.1 Modified 7.17E-03 2.18E-02 2.18E-02 5.12E-02 u 4~~- ----*----> - - -
| |
| 19-09014-16 TRG L1-10221D-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 Cesium-137 EPA 901.1 Modified 4.74E-01 9.73E-02 1.00E-01 1.02E-01
| |
| ~~------->---*---*--*--*--*-* --------***--*-~-*-------
| |
| 19-09014-16 TRG L1-10221 D-FIGS-014-SS-A 07/09/19 08:53 9/3/2019 9/16/2019 19-09014 EPA901.1 Modified 1.60E-02 1.0SE-01 1.0SE-01 1.67E-01 u
| |
| ------*"*--- :-~----- . "
| |
| 19-09014-16 TRG L1-10221 D-FIGS-014-SS-A 07/09/19 08:53 9/16/2019 19-09014 EPA 901.1 Modified -5.66E-02 1.23E-01 1.23E-01 8.59E-02 u 19-09014-16 19-09014-16
| |
| ------;--*-----*-"*----""TRG TRG L 1-10221 D-FIGS-014-SS-A L 1-102210-FIGS-014-SS-A 07/09/19 08:53 07/09/19 08:53 9/16/2019 9/16/2019 19-09014 19-09014 Holmium-166m EPA 901.1 Modified EPA 901.1 Modified 1.58E-01 1.03E-01 6.94E-02 1.04E-01 6.94E-02 1.38E-01 7.04E-02 u
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| u pCi/g 19-09014-16 TRG L 1-10221D-FIGS-014-SS-A 07/09/19 08:53 9/16/2019 19-09014 lodine-129 EPA901.1 Modified 9.58E+OO 9.58E+OO 3.02E+OO u 19-09014-16 ...., _______ TRG L1-102210-FIGS-O 14-SS-A 07/09/19 08:53 9/16/2019 19-09014 Potassium-40 EPA 901.1 Modified 1.57E+OO 1.66E+OO 1.07E+OO EPA 901.1 Modified 4.14E-02 6.59E-02 u EPA 901.1 Modified 3.59E-02 3.59E-02 5.0SE-02 u EPA 901.1 Modified 3.76E-02 3.77E-02 5.71E-02 u 1.94E+OO 1.94E+OO 3.18E+OO u L 1-102210-FIGS-014-SS-A 07/09/19 08:53 1.02E-01 1.0SE-01 1.65E-01 L 1-10221 D-FIGS-014-SS-A 07/09/19 08:53 1.45E-01 2.20E-01 L1-10221 D-FIGS-014-SS-A 07/09/19 08:53 9.29E-01 u L 1-102210-FIGS-014-SS-A 07/09/19 08:53 1.47E-01 L 1-10221 D-FIGS-014-SS-A 07/09/19 08:53 1.63E-01 u 19-09014-16 TRG L 1-102210-FIGS-014-SS-A 1.32E+OO u 1------+--- - ~ - -
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| * 19-09014-16 TRG L1-10221D-FIGS-014-SS-A Thallium-208 1.30E-01 1--------...l..-----
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| 19-09014-16 TRG L 1-102210-FIGS-014-SS-A Uranium-235 2.67E-01 3.72E-01 u pCi/g CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample;MBL=Blank;DUP=Duplicate;TRG=Nonnal Sample;DO=Duplicate Original;U=Non-detect
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| ( '"M>
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| EBERLINE ANALYTICAL EBERLINE ANALYTICAL CORPORATION 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
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| Printed: 1013012019 3:09 PM Page 19 of 21 Report To: Work Order Details:
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| Patricia Giza 19-09014 Eberline Analytical Zion Solutions Purchase Order:
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| SDG:
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| 677118
| |
| ----------~-,-,~- *--**-****-*----------------
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| Final Report of Analysis 2701 Deborah Ave _ _ Analysis Category: __ _ ENVIRONMENTAL Zion, IL 60099 Sample Matrix: so Lab Sample Client Sample Receipt Analysis Batch Report ID Type ID Date Date Date ID Analyte Method Result cu CSU MDA Qualifier Units 19-09014-17 TRG L1-10221 D-QIGS-013-SS-A "m--"-~,---------,--.- -07/09/19 08:51 '
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| 9/3/2019 9/16/2019
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| - 19-09014
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| ___ ,_,,,_,,_,}}
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