View source for TXX-4201, Forwards Responses to 840518 & 23 Ltrs Re 60 Allegations Concerning Protective Coating Practices at Facility. Responses Based on Technical Knowledge & Review of Existing Documentation.Supporting Documentation Encl

{{Adams
| number = ML20095C187
| issue date = 06/22/1984
| title = Forwards Responses to 840518 & 23 Ltrs Re 60 Allegations Concerning Protective Coating Practices at Facility. Responses Based on Technical Knowledge & Review of Existing Documentation.Supporting Documentation Encl
| author name = Fikar L
| author affiliation = TEXAS UTILITIES ELECTRIC CO. (TU ELECTRIC)
| addressee name = Bangart R
| addressee affiliation = NRC OFFICE OF INSPECTION &amp; ENFORCEMENT (IE REGION IV)
| docket = 05000445, 05000446
| license number = 
| contact person = 
| document report number = TXX-4201, NUDOCS 8408220412
| package number = ML19276C060
| document type = CORRESPONDENCE-LETTERS, INCOMING CORRESPONDENCE, UTILITY TO NRC
| page count = 320
}}

=Text=
{{#Wiki_filter:S' ' " Ap-;
                                                                                            '          '          ' ' '                 ;,,a y
        ', }';. . -i."- ~_,
                                   ..h
* r . ~*: _ ^ s'-1      l* - .; .' < -                 r             . , ,
I
                                .                     TEXAS UTILITIES GENERATING COMPANY SKYWAY TOWER
* 400 NORTH OLIVE STREET. L.B. 81
* DALLAS.TEXA513201
   ~
                     ... h.f J.'. T ...,                                                        June 22, 1984 TXX-4201 Dockets: 50-445 50-446
    -                          Mr. Richard L. Bangart, Director Region IV Comanche Peak Task Force 2                            United States Nuclear Regulatory Comission 611 Ryan Plaza Drive, Suite 1000 Arlington, TX 76011
    .                                                        COMANCHE PEAK STEAM ELECTRIC STATION
                     ~
UNITS 1 and 2 PROTECTIVE COATING ALLEGATIONS TRANSMITTED BY LETTER OF MAY 18, 1984 FILE NO. 906.1

==Dear Mr. Bangart:==
This'1etter responds to your letters of May 18 and May 23, 1984 relative to sixty allegations about protective coating practices at Comanche Peak.
To aid in an understanding of.our responses, we have repea'ted the a112ga-
     '                          tion as stated to us in your letter of May 18, 1984 followed by our
    ~                           response in the format requested by your letter of May 23, 1984.
Our responses were developed based on technical knowledge, kncwledge of actual jobsite conditions, review of existing documentation found to be analogous to certain of the allegations, and where appropriate, inter-views with cognizant QC personnel. As you will note, supporting docu-
  ^
mentation is included with certain responses as a means of shortening the length of the response.
We trust you will find the enclosed infomation helpful in expediting
<                               closure of these issues. Please advise if you require further infoma-l,                               tion.
Sint.erely yours, r     ,
l                                                        e408220412 e40007 PDR ADOCK 05000445                 PDR G
LFF: pew Enclosures cc: Mr. Thomas A. Ippolito Mr. John Collins A DivsstoM or TsxAs t:TELET1ss ELscTnte courANY                               .
: w.                   -          -                  . - - -                                       _                  -_       __--                     .
   ?-Q.C .. - L                                    .l:2m          5U:F=?                 W                                    ;; "       * ,-3   T'
               ,          5:
_ 5
                                        ~
                                           ~                    .     ..a y.+:qm:.m,y:m"                         ;u_.         3. u ;g
                                                                                                                                                              .                ;g.. " ::y Q.
g'^y~.~;,~u~;7T.'=.','~~                            .,,
I*             :                                                                                                                            .
: ~: .
:j
[' j                             TII-4201 a
06/22/84                                                                                                                                                                                  ,
             .                                                                                                                                                                                                                i
                                                                                                                                                                                                                  !           j
   ,;-                              Al' legation No. 1 Paragraph 4.3.1.2 o'f Procedure Number CCP-40 states " Imperial coatings may be applied in the following sequential order: !11S/1201/11S/1201 or 11S/1201/11/1201." Imperial {{letter dated|date=May 8, 1978|text=letter dated May 8, 1978}}, VBR-7697 to dr. Kelly
                                 -W111 b==, second paragraph, states: "Although the resultant systems
                                    #11S/1201/115/1201 or #11S/1201/11/1201 have not been qualification tested, chare is no reason to believe that they are not viable systems." Thus these two
      }
systems have not been DBA qualified.
Evaluation of Validity This allegation is correct, but is not significant because this combination of coatings occurs in limited areas. Nutec 11 or 11S and Nutec 1201 are applied to existing 11S/1201 only during a touch-up repair or during interface with previously applied adjacent coatings. This overlapping is necessary in order to achieve a smooth transition with the previously applied adjacent coatings. Due to the limited area of coatings involved in overlapping systems as a result of applications adjacent to previously coated surfaces and/or coating repairs, this issue has never been considered to be significant enough to warrant special consideration such as DBA qualification.
DBA data is unavailable for 11S/1201/11/1201 and 11S/1201/11S/1201 - the two combinations specified in the allegation. Imperial has, however, conducted i
E1cometer adhesion tests for the above systems at both high and low film thicknesses and all systems passed. (See Imperial's Report No. 759, attached).
Additionally, Imperial has developed satisfactory irradiation and DBA data for systems similar to these specified in this allegation (see response to Allegation No. 12).
6
               =--*c--       -
r-eya-       we+e ew-               ww w ew-es e-' .w----e e t.-W,p.N e t *W , -        e-
                                                                                                                                  ~ **    e,*'-I  "O=--
e    e,-tie m - --   we m -wwwwegm      -wwee--me           w-e

                                                                                                                                                                          '~ ",
awM-s;; ~~.:~::-.'.;1,:;;;_.ac.c.,;;;
                                                                                                                                                             ~, y?
: ,,                                   - r,.     ~q~T::;?.;n e=''a i:              .K~''-
pa                                               . msg                    q.ggg.,';                                  -
n             .      .::;   .. . ..,            ,,b:+ z w         n-
   -} -:r.                                                                                                                          .
            'l
            ~
     .,. - ),                                                                                                               .
:l
  . a ;)                                                                                                                                            .
i Safety Sianificance
      . :a
                .                        None
:                                                                                                                                                                       i Generic Implications on other Systems or Contractors Not applicable I
e e
I          e
 ? '              g J                                                             # '    f.       I D
I i
k -
I
         'N 3
                                                                                                                                                          *'      ~     ' ' ~
                                                                         ,             .                                           - ~ ~ ~
                        . _ -         ..         ..n__

                    "           *   ,+9               ,s.   -    E              'N                              *         "g                                                     ,'[W *li       c  et ,"M           .   "4   ,            4   .4e% &     .=          ,*M"  ea
                    ,'   ..                                            - -                                            m: :=.- - ' ,' M            -
                                                                                                                                                                  .m v                            :.3 ;e ,;\ c ~ . - . wu. .a.6.ac.=.3.: k:
                 -) t '. :.       , s.
                                                                                                                                                                                         ~
                 ])          ..
4                                                                                                                                                      *
{                                         .
    -t             .,
h' b
                  '                                                                                                                                                                                                                                                            I
                       .                                                                                  IIIII"EKIRL 2                                                                                                                    .
TECHNICAL REPORT l
i NUMBER s'                                                                                                                     759
>:.                    .                                                                                              .      .. .                   TITLE
* E1cometer Adhesion Tests Nutac Concreta Coating R4 pair Systems 115/1201/11S/1201
;i                                                                                                                                  11S/1201/11/1201                                                                                   ,
FOR Preparation for: Comanche Peak Nuclear Plant Glen Rose. Texas                                                                                                                                         i CUSTOMER Submitted by: Jerry Arno                            "
Accepted by:
Approved:
Date:                       *///7[/f SOUT1 TERN IMPERIAL COATINGS CORPOR ATIONe INC.
P. O. Box 29077,
* New Orleans, Louinana 70lM4 Phonc: (504) 254 1433 v                                                                                                                                                                                                                                                    ~
m ,                                                               eae ene,w 4.                r     0.r no ser.nm .                                    re. eews.o a sw ..sw aie.
t.twere te(.esessepeg et et ettesesse ser .te of pertent Ame.nq twpnesat %Best 40 Nteed gone estatye.est ene fees.
               ,               9 upp ateessne see eseesses, est gesmenttages-useast                .p set .te 18tig ansersetee.en       .eet.Ae* Wesennye og a latestee te es.tese g                                                         .s.o . ,e,._                         . se       e                          - .n.           .
w        @              & en.m    e       . se n
                                                                                                                                                       =               e                              e           aspe   e ..e   --ee e,-              .
_e4, , ,
  --- - ,- -                           -_,,,m.,-e-.v-             e-----.-,----egeww-'..,e---e.e.,.,p-.myww.-                                                            _ ww-p,                         _ gwmmup- W w m                                    ,_ - v_                  y-m--

                  ,.,. ;.,~ , r '..g                 .
                                                                 ~
TxW                       ~~
                                                                                                                                           ~~m,*~
                                                                                                                                      ~ ,' . y      .
                                                                                                                                                                       ~I,        '
c" M * "
                                    , . n.e y              - . , . .. :.                .     :..                 ;.L                     .     -
: .,s . ai.a          . m;;.;5 .;.  ,
       ', .] . .
P ''!
hr             

== Introduction:==
Following the installation of the 11S/1201 concrete coating system, it sometians becomes necessary to repair damaged areas or fill holidays in the original system. Also separate applications
'                                                                     sometimes result in overlap of the newly applied coatings to                                                                 :
adjacent, aged systems. The result is the application of Nutec 115 or 11 over previously applied ar.d cured 1201 topcoat. The purpose of this adhesion test is to demonstrate the validity of this practice.
procedures:                    Concrete blocks, measuring 2x4x2" were coated with the following
            '~
systems:
    ?
A]        Nutec 11S (10 mils)
                                  .                                             Nutec 1201 (3 mils)                                                                                 ,
Nutec 115 (10 mils)
Nutec 1201 (3 mils) 3]       Nutec 115 (35 mils)
Nutec 1201 (16 mils)
Nutsc 115 (35 mils)
                                               .                                Nutec 1201 (16 mils)
C]       Nutec 115 (10 mils)
                                         ,                                      Nucec 1201 (3 mils)
J''                                                     Nutec 11 (3 mils)
                   -    V                                                       Nutec 1201 (3 mils)                                             .
DT       Nutec IIS (35 mils)
Nutec 1201 (16 mils)
Nutec 11 (20 mils)
Nutec 1201,(16 mils)                                                                       -
The dry film thicknesses applied were selected to envelope the                                                          ,
thickness range actually applied at nuclear jobaites. For
                                                                   - application and curing details refer to the attached panel                                                                        -
preparation. sheets.
Six adhesion tests were conducted on each system (two testa per concrete block) using an E1cometer adhesion tester.
e e
t' e
                                                            . g
                                                                                                                                           **                                             ~*
           - e e n. .e  e-
_ aw - e   w.     -*~~*e
_     _              __            _ _ l

r                                                                                                                                ,
 *.                                       - v.my,~ ~- , .%                                                                         -
t-c _                                =
                           ,. .                                        . - ._ , . ._ T- ~ . m. c .. z nn.                                      ,    l :: - ._.y;
: b.        -
                         -l :f.y.. ~.,[; h.. . . :, ; ..u - .
s                        .                           . . :, ;-       .
            ~.' . . .
                                                                                                           ,.-- x ~.       _ 3 i; .          :.~y _, : .a;.g5&g;p s. ,
  . ; .1.                                                                                                                .
d, l.                                      -
                      .Q y.j                  4C Results:                     The attached laboratory result sheet outlines the individual results. Below are the resultant averages:
  .                                                                                                                                 Ave.            Mode of System
* PSI             Failure -
ils (10 mils)/1201 (3a11s)/113 (10 mils)/1201 (3m11s)                                            313    100% concrete ils (35 mils)/1201 (16m11s)/115 (35 mils)/1201 (16s11s)                                          337    75% concrete 25% 11S(1st Cos ils (10 mils)/1201 (3 mils)/11 (3 mils)/1201 (3 mils)                                            325    85% Concrete 71 ils 82 Clue
  .                                 Ils (35 mils)/1201 (16 m11s)/11 (20 mils)/1201 (16 mils) 313                                            85% concrete 15% 115 Conclusionst. All pulla exhibited concreta failure and surpassed the minimum 200 PSI values required by ANSI N5.12.
I 6
o p     -
       .                                                                                                                                                                      t o
                                                                                                                                                                        .e

                                                                                                                             ~
                                                                                                                                                                              . ., a-
                                                                                                                                              .m._,.,___              .._.
e               :                            . c g.,..                                                                                                                                       ,,
r u,},. .:..cq -".
a- . . s ,. . '..
  .; ] ..                                                 -
a                                                            , , . , Sa, . , . .--, , . r :            .
                                                                                                                                     .       .a,                   ..,.                       ,..
     ,v
  ,j'                     *                          .
          *        " ' '                                                                  EICOMETtR ADHESION 2X M                       @'
       'r              sk order /                O[1 E                                                                                       naa           4-/7-7/-
n.u ris t <<nce
   .H            'ani. Ty,. I ., ,s-
* I
  ] 'I         .3
                                               ~
                                                                                             ;f2.        Site'A'                           -                                                   *
     -        w ;,1 N NO.                                                                                 Oct,Z,y                                  TYPE & POSITIQH OF FAILUNZ*
    ! '}s                                                       '                                                                   #* H#                                  t' e fftI                      cwr c j s22r                        sys :""                                  DrT                  no.                    Psz
                                                                                                                                    %COilAD          %CO       LAD        %Co     nu l geo ; gf (pl & ( Il$l12.. .Jbll                         I l                         yy                                                jg WW,d{~a g                                                          2. .             -
23o              -
I fg Ul 6 %                                                                                  I                  45*                                             fn 2                  190                                               /@                 .
Gi 5 *3                                                                                      i             FIC                                              feo 3-            24o
                                                                                                                                                                         /00
     ,       lolSS H$lG : 11$/%                                                            i                            .y o.                                            jm                  -
a          i<                  is am *-
                                                 .sw$ Wito att.                                      2                           ggg            g                                    go-6(5%-                @
1                 2G0              Sc                               70-                      -
: z.                     4.gn        4-0 so.            .           .         .
(/9 G
            .v                                                                                         i               'y1. 0       v>                          -
Bo                           -
: 1.           120            2.2                                     *            -
bl5 9 II' L .3 dbl lnar                                                                                  bto i
I*                                                                            /00                            -
     ;                          $L ...i!h!$      f                                          g                          *2, } O
                                                                                                                                                               ~
                                                                                                                                                                           $O                      $Q (e l 5 s          O                         '
: i.                2.30        9.o                                    e 1                                                                                                  A                  44D                                             /vo h( ST                                                                                    'l.              2./o ' to                ,
S-                                             ,
i
                                                                                                    's                 74 0                                             /d                                               i 6I&0 ll$ l :o!It! Im! -                                                      l                             %0 W                                              10                                            :
kh                                                          1                          ~290         )o                                   7o                                              l l'            blH                &lr bi 5fdtil        .
t                   3*70                            .
two                                             \
j                                                     k                                             %                    abo           -
l00 (r%%
r./
I              vo                                               ton                                             i 1           2.vo            g                                  70                                   *
                                                                                                                                                                                                                 ~
              *C0           Cohesier.                      AD = Adhesion                                                   *
[                                                                         - .-
                                                                                             @**=_.___.__                                         **I*,I*.--*-.['E-'*--              -              $            +            -

c..~.,-~...           .;~~; . :: : .. .
                                                                                                     -.m       . : , - ~~~ -     ,~7~.
                                                                                                                                         .:      m~.
o          .~. ; ;;.: . . , .     . . -. . . ~ ~
                                                                                                                                                                                                         + -        ,x                 c -
         ..:L46 5                               .
                                                    . . .;..       p.          . .h...:      .        . <..       .:
                                                                                                                                            ~._
                                                                                                                                                               .,,   c":
a         s.     , , . , .
                                                                                                                                                                                                      ,.;a ,;; ..w      .;_ .g;
                   ,                 ..                                                                                EI4CMETtR ADHESTCH ni'.;?;                                  .
7,                          * ' work order ARof15"                                                                                                 -
one.-      4@f 6
::!.d                            ' clue Type o o ae Ee             -
I                 M yo,
* gy                                              TYPE & PCSITION OF TAIIlJRE*
                                                                                                                                                                  #E '##
    ..~ s s:zr ~
sysTzM                                      nri            No.                 Psz
                                                                                                                                                                                                    ""E7'' ' C"I 4Co l 4AD ' 4Co ll %AD 4Co SAD l gCo i s.
    '} N W b$ &
gjy O                                                             -
337 1.5                    -
1C
* 1;*     ~
O                                                        _
                                                                                                                                               ~3 2- 5               9                              85                   2
                                                             @                                                                                 313                 / s-                             Sr 4
                 >                                                                     s
* A I
j                        .                                               i                          o                                                                                                                   -
suas                                                                                                        .
                                                                                                             -                               t                                                                              .
kJ                                                      .
  .y               1 t
i i
r l ...
t
                                                                                                                           +
1
\
1 1
I                                      )
Q i
                     '                                                                                                                                                                                                              s'
:          'CQ = Cohesion                                                 AD = Adhesion                         -
s                                                                   .e l                                        - ..___-         _ -__ - - _-_-__- . . . - _ . . _ _ _ - _ _ . - . . - - _ , a-                        - _ . - . - - -- -. -- -_ .- -_-- _ _ - _ - _ - ~ _ - _ _ - - -

       . Y. _ _w. :..vy.2,.. @.>.: :.:v.WT, ^: = Vmm . -, , '-w
                                                                                             . ; '..;,-P._ ,\ ~. ~.. g~..,...c",.,:%- _.;__.
m
                                                                                                                                                                                                                                                     ~e         .
                                                          . - . . . .q . ,.                                   _
a'                     -
: i. :.: .                     .
       ;:)-                                                                 w                      .                        .
i;                           .
t            :
:      ,              ..i                          :
4 t           ,.
1                                        e               ..v               .                          .       .         .                      ..         -
    .A                .g~                              *                                  .                   :                      ,      ,
:I1                                                D                                                                             l
        .:J                                            Q                                .i*        .-}                      -        -
A                                                                                            !..i!                                                                                -
i                   :             i
    /!     ~
se              gi                          :
                                                                                                                                                                   ;i                                                            .
i                                  g                       :4                           .          6    !                       l.                     !    ;               <
O!                           l               l ,'                    l     i        i       !-                   i        l 4P'             4                            :                                       .     .-
l l
j                     i,                                    ,        i          :
                                                                     'I i                     ,                     i                                   ,.                                           :
i,   i               ;                   i 1.u                          !                       l                      ,                                              .
C!                           !                       i                                      :    !                                                                                 .
y                               mi                               -
:        i      .
i
                                                                                                                                                                         !               :      .'!          i i                                 i i
zI                                                           .
t        i        I e
                                                                                                                                                   .        i      ,
Q -                             a+                           l               l        l        i,    l i
i        !,     l     t,              i.       i.         !.
                                                                                                                                                                                                                                                         ;                        )
p_ .
O                              s      -
a g3ag                                                                :
                                                                                                                                                            !i.
i i
i n,
s.
E :a m
y m
tv i                                                                                      -
or                                        m                                 I.       i,     :.
                                                          ,_           e            -a         cs         m      w,                   i     i W44m
                                        @                   ;                                                                         s      i                                                                                                                    .               l
(    ,n.               [ 4k                           1- u.1:5     $$k                                                            ll!,:                                                      !'                                     .;
u                                                DF b sl=qi!.t.eil                         .a l ''
t
                                                                                                                                                                                               - w. ~ .q
                                                                                                                                                                                          , M SS W
: s.                                 t-4                                     :
[,'                             d                  Y            cSF olMId ci,NN NNNWIM:Sl%i:E\ NU                                                                                                                                                                          l i-Z" f      e -z:                                                     i il i
i'
                                                                                                                                                                                                              !          i j
                                                            @ J 4-
                                                          ~        4- .u                                                                            ; .!            !     .                        i A                 w y 3r:: o                                        .
                                                                                                                                                           .?       >
i               I       .
                                                                                                                                                                                                            .j           ;          . .;!                    l i,                    .
p                                                                                                           .                      .                .                                       .
                                                                   # t                                                                 !            i                                       j                            !                     :
l r-              d                                              -
i                                                  .
ll:c                            '
                                                                                                                                                                           ;i                                                                               '
J $Nd
                                        'tr i                                                                                                                                                                                                   I O
g
                                                                                                                                                 .i I'
                            .                                      j                                                                 ..        ,
p               Is         g                            .!
i O              d          2(                                                                  i  .
O        -
d c
e o 8            d em E.                                  i             1
                                                                                                                                                                           '                 :"= o   c4:M= o';              W l
c4                    l                                                               -
s, ,
O                c:                  ,c4      .
V4
                                                                                             ,        i              i l               i                      -        -
                                                                                                                                                                                              ?Ni G    ..
C                      ... d                               '
l
: i.                  x               i
                                                                                                                                                                                                                ~
                                                                                                                                                                                                                           !..I       ;
l v 1:
a                Ud8
                                                                         -o_           6 i
:                   r-x               .
i..                                ,
o              vl                                                                            :                                         es                                    i          :            i 07      cV J                                                                                                                                                                                        '
lh                                       d           W g       g                                       Ig                                M                                     M .)                         !            1.gi                        i' 63          % ,d 4
L.C l9 i i;,                          g                   ;                 .4 Mi    --                      I
                . g-,
o f           o. f-o3  pa c                                    iS si.                 I                -  o                                     . su          .
I           .,
i                                       . . .                                                      .       .

                  .                                                                                     .              .-                                                                               .                  .s                                              ..,.w....                              .a ::              -; ..
i                         .. .                                                                   ..                           .         1 .                                                                                           .
                                                                                                                                                                                                                                                   .     . . . '*    . : . ..a.b            :i ' !0'
                                                                                                                                                                                                                                                                                                .                 N
                                                                                                                                                                                                                                                                                                                      .'
* S <.: % '.
          ,...,                 s.                                    .
m.
n u.
i
                       .         c                                           .
                                                                                    .                                                             o                                                           .
                                                                                                                                                                                                                                                                                                                                       . c.
1                                                     .
u 3 PRAY 00 . q' TEST lNCs                                                                                iNSTRocTloNS                                                                                                                                                                      O.
AROI25                                                            ;
y; "
i l'*          PE E l. OF                            3.,         On \C,tN ATOR.                                                   -
A q @ p o o 7 /j PAH EL                                             C.D A'U M G -                        DU AMS                                                                                                                                                                                                                           f' A
paw a                  Slui                 s     coot                      BKica               EdaCH                  D'     W          T           R UmE/ 'b                                                    ftEMARKS                                                           . Test                        '
l                    og.            . on,                 p                                  &                     C                F F E                        H TtuE.                                  F                                                                                        g                                  33                  ,
!            Etoc<                  slos                                                                                          T T M                                                                 T                                                                                                           .
t" l-bl.r6                    /                                     -
                                                                                                                                   ./                                                                                                                                                  .
                                                                                                                                                                                                                                                                                                                       '        +
e
                                                                                                                                                                                                                                                                                                                                             .c
                                                        -.                                                                                                                                           _          .                _                                 ... .. ...                     .. ..                                 m .
                                                                                                                                  ./      -                                __                        _                      ___._                               _. _..,....
                                                                                                                                                                                                                                                                                                                                      ..t,..  .
                                                                                                                                                                                                                                                                                                                                                'g .
4k''
hlSl MD                            _     . llC                                                                       l                                                          _          . . . . _ _ . . _ _ . . . . . . .
_.3 f,6 1                                            '
i                ....__.    ..               ._          ..      J20l
                                                                                                                                                                                                                                                                                                                     ,                 i' .
8 31                                                                                                                                                                                              p' 'i-
.i                                                       _.   ._ ll            =                          .                       -        .-       __        _ _ .                      .__.        -                                                        _                       .._            . . . .                                    :,..
3.Ol                                                            3 5b                                                                                                                                                                 .
                                                                                                                                                                                                                                                                                                                                         .:      T
                                                                                                                                                                                                                                                                                                                                                 .c a          .
                                    .. f                                                                                            l                                                                                '
                               $..                                                                                                                                                                                                                                                                         . . ..                     I.t .
                                                                                                                                    /             .  ..               .        . _ . _ .              _ . .      ......._.                 --
                                                                                                                                    /
1
                                                                                                                                       /                              -
                                                                                                                                                                                                                                                                                                                                              .x .
4 I~            _bl                     . _ . _                   . . . . . . .              . _ ...                        _          /.         ..   ._..            . . .       _. _._.              __             .__'_.__
p>..
                                                                                                                                                                                                                                                                                                                                        ..t c:.3 c
                                                                                                                                     /                     .
                                                                                                                                                                                                                                                                                                                                       ,,t
  !              . d60... GXH6                                 ils                  . . . -                  -
35 48                                                                                     .            . . . .              .                  .                      .                             L.
a.
i
                                                           ..  ..m..al_                                   _ _           _.          I_b_au                 .. ..            _ . . .          _ . . .   -.                 .             . ..                                                                                             ,,
no mt I; .                         .
ve..,
190l                                                               lb afb                                                                                                                                                                                             VM
: l.        *
                                                                                                                                                                                                              .                                                                                                              .          (.
g i

   ; .r.c                                                                                                                                                                                                    w u.+               h ams %;wt
                              .<                  ...           w..y.m ar_s**        ~oce-  m.m ,.g # . m            4. .a;       w A.
                                                                                                                                      - neac c - - . _
                                                                                                                                                        .. ww. c.                                re m                 ,
      ,j y.gc.,
s          ,_
                                          ,+         '
: 3.                      -
a-          .
                          ..                                                                       ~
1                                                                              w                  .                                                             i           i       .                          .
n
   ..4 :? G.
6 a s
                                                           %                      M'y     e          ;
O 9L     .o                                                ;
                                                                                                                           ,        .....i- '
I          I            -
N                           to                             l     i       it:             .Ilillj:
b        ..
r g
s i
l!'
i 4                   <t                                                                                                      ;
i, . .,
2 I                 -
i          i               I l     .          .
                                                                           . u.i                             i             i j
i        ,                ; ;              .
             . -                                                                                                   i                ,                      ,                                      ,     .
c.!                           -t     .                                                                                   l                   .
m i                                                           ..                 .                                                .
:                                                                                                     j                      i      ,.              i       i 7                                                             ,     l       .        :      i               i                  .:       .               .          .        :
                                  .            g                              aur                    j i
i i       i i
i      i          .
ci                  ,
i p_.                          ._                               i             i        ll                             lii         ,                                  i                                i cJ                            A                                                                                     l           r I.         !                                :
m ww                                          .               .
                                                                                                                                                                   !           i i
                                                                                                                                                                                                                           .             .3 4- s    -
i-                      .          .
cd                             or                                                                                   ,           .                  :     ,
i
                                               >               .              az
                                                                                                             !             l.              I         i i
i t.
i.
i             -                                                                                              i                             .                       .           .       ,                                                           .
\
               . (-.c    'qi.
Z pus                                          !
e                         ll:.
: i.         ,
6 i
l.l
     .i .                          ..
Ear                    l                     l               l         l             .                              .
l         :        i                .
i                  '
V(.
Z dWF                %lhNNWW                                                            !           >i                 -
i         :        !                       :
c s                             ,
i         ;
: l.                      I.
v                                                                                     l                   i V                                                                    .       5           I       .          :     l. .
                                               ,A                     .
                                                                     'p i
l i
                                                                                                                                                                                                  -     I
                                                                                                                                                                                                                                             ; i t
g2                                                    -
                                                                             %                                                                                                                                     i       '                                .-
T'~         C!                                                                                                                                      I l                       l           .
y                                                                                                                               'i Q
q          .je. e
                                                                             $cd                                        .
l i.
l i
I.
i
: l.      l.
                                                                                                                                                                                                                                      .]i p           2 r
1                ,I O          d         d                                                     i                                  .
t          .
O                      u-                                       .
i                I       .
                                                                                                                                                                                                                   !.l*
g                                  M d-               .        ,
l       .        j                 i                         .
a $
N ,[l i          !       I          i
                                                                                                                                                                                                                                              '     l 0: .                             _$d     o h                                                            :            .
                                                                                                                                                                                                                               .!,I 4W i
o                                                              l                                l                                                                                 :
s                                           -I                                                  i
     , (,
W 1                                                 !q                                                           *                                                     '
g h -o
      <;                                                                                                                                                            l                                     I
                                                                                                                                                                                                                                                                !r io          I,                        --
: o.=
i*               i.
I                i
     .i                                                               q                 g                                  .
g                             e      l         .                                            .
N
       ~
     ?
e           s*..                                                O.                   JC                      l~.~$.   .
* I                  l                l
                                                                                                                                                                                                                                                                            .} ,
                            ~           ' **                     *            *#$,.*,,,.,_..
[1           4,         . _ _ _[" .                                [Y
((          -...7,._      '

              , m,a: .v.                                                     -                                           ;                                                   . ,,p v ; wm                                                                                        .x, .\,.                            ., .
                                                                                                                                                                                                                                                                                                                                                                                                  . ,.                                      .+..,...,/.,                                                                        ,
  ,' ' .M
                             ;f;.. ~.; .                                 .'..              n..
                                                                                                                                            .              r                         .
                                                                                                                                                                                                            .m.a. % &       .
                                                                                                                                                                                                                                                                         . .t                                                                            .. . v.                       ..                a. r...
                                                                                                                                                                                                                                                                                                                                                                                                                                              . . ym._.                . . .
c                -
  .~h
                                                                                                                                 -                      .... . . . _ . . .. . . _ . . ..                                          . ..._         .. . ,.....c.   . - . - . ... .
                                                                                                                                                                                                                                                                                                                                                           ~..._..
                                                                                                                                                                                                                                                                                                                                                                                               ..                   . . . .-                                      _ .4 _
9.W.M...i,k.                                                          .,;fs'SR                                                             *%55G@                                                                       Ms. , "'::9WdM MM & +r=MW.
2...._...                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                            .
4                     .                    .                .                    -                                                 .
                                                                                                                                                                                                                                             .                                                                                 1                                                                                    i               ..
i
: d. e:. >:.
3 i1.v..,.s
:.; ..n
                                                                                         ..                              .s     ..
                                                                                                                                            .,.m.,.,; t.&.,M                                                                  ., ;        .         .
_ w..,.                                                     .
                                                                                                                                                                                                                                                                                                                                  ..w.I:.: 4. :.w
: y. . n .
cg           .
m m
                                                                                                                                                                                                                                                      ...         .n  ...                               .
                                                                                                                                                                                                                                                                                                                                  . 1 y.
w..
x.%..a                                                                                     -a i                                                                                                                                 -
                                                                                                                                                                                                                                                                                       ,.: ..,                                                                                         ...                             l                                 ,
: *1                                                                                                                                                                                                                                                   _.. . .;. . ..
            .I......                                                                                                                                                    * ..                                                           w: ., . . .w                                                                                       .u. .                          . - . . ..d
    .t                                 . . .                                                                         s .- ...                                                          .                  .                                                                            -:. ..,                                   .                                                                        .                .                                   ..                ..           .
                                              ......t..4 .c
                                                    ..                                  c                                            .                    ,. .....
                                                                                                                                                                                              ..                                                                        .s
_ ..L
                                                                                                                                                                                                                                                                                                                                                                                                                                         ...,l .                                                            ,..
4 .. .                                          .
x mn~
                                                                                                                                                                                                               ;l If A-
                                                                                                                                                                                                                                ..,,. 3 s W
                                                                                                                                                                                                                                                                                                                                                                                                                                            ...l.
y                       .
7 Q               Q*',         .
                                                                                                                      '.' t -
                                                                                                                                                                                               .                ,..             .                 p
                                                                                                                                                                                                                                                          ? :1~
                                                                                                                                                                                                                                                                                                                                          *l:             .
i f
: g.                  ..
0%.                                                                                                           ;                                .
                                                                                                                                                                                                                .1                                                                                                             .                                i                   .                                 [               .
* t.
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                        .               5 i
I.
                            . .I                             e
                                                                                                                                                                                                              ..I  .
s l...
a
                                                                                                                                                                                                                                                     ~. .. ,
                                                                                                                                                                                                                                                                                                                                                    ..               ,.                                  .            .4 i
                                                                                                                                                                                                                                                                                                                                                                                                                                                       .                          .i                    ,
                                        . 'J.'* .a
                                                                                                                             . C,. . .* .
in..               .
                                                                                                                                                                                            ~
                                                                                                                                                                                                           ..r.a. .                          s .                    a.                                . i.       ..             .                 . . . , . ., . . -                       .
(
l,                  ,. ,
d%.            rg                            M(                                                                                                 ..                   .a                                        .          .s .
                                                                                                                                                                                                                                                                     .: +;
g                                                ,
                               -             mg                                                                               - ,2
                                                                                                                                  <?
I_                              -
e ..
t l ..                       .!
: i.]                                    g.
                                                                                                                                                                                                                                    .<                                                                                                                              .e..
                                                                                                                             .f              .
                                                                                                                                                                              .s.
                                                                                                                                                                                                     .     .Jp .;               .                       . . .
                                                                                                                                                                                                                                                                    ..                    c.; ,.. .                   .                   *                              ..,                             ..
                                                                                                                                                                                                                                    .. p ..-                                                                                                                                                                                                                 ..
                . . . . . .                                                                                                                             . ,                       .                           . . .e4                                     .               ...                                                        .                                          .        ..                                                                           .                                                             .
                                                    . ..                                                                                                                                    4                                                                                                                                                                                                                                                                                           l l
'                                         g%. T                                                                                .U                                                                                      '                           ;                                                         j                                 s'                                                                                                                                       g
                                                             ,.                                                                  C)
* i 8
8..I t
l.
O
                               *:y- rp q                                                                                                                      '
t i
q$.                                                                                                                                                 . ..                                                                                                                                                a                                                      s                 e               a                               s s t                                           e                                                                                           j                                     g a.
                                                             ..                                                                . x ..                                                                                                                                                                .
                        ..                                                                ..                                                                            ...               ....i             . . .                      . ..
                                                                                                                                                                                                                                                                         , ..                                                                                                                         ,. ..                .:               s.. . , .
            .. . p. . .+.h.       .              w% s.                         .      .%.
As . .c; e                    ..a                                                                           u, ..                                                                                                            .                                                                             .          .
                                                                                                                                                      ;h Y,,p$                                                                                                                                                    W W<$ W.YW~~NTf'W'Y ?Y W h..                                                                                                            ' 'W, . ,YNT
           .t*           s..':'J- ria4
                                    ? *~.G.                            ?.(...W..       "E.5 w                                         .
: s.               E. .. ,r.,
p.
                                                                                                                                                                                                                                                        .             . .                                  -l-                                                                                       g                 e                 l   .
g                             g G,                                                                      h             '                                                                                     '
s                              .s                                                   l
                                                                                                                                  '::                     N . . ..Q.                                        .I                                                                                                                                                                                                                                                                           {
                                                                                                                                                                                             <b r. ..,
                                                                 . .                                                                                                                                .                                                                                                                                                                                                                  4                                   e
                                                                 ;                                                                es                                                                                                           -                                                                  .                                                                      -
t                                           .b                   ..,.    .
                                                                                                                                                                                                                                            .9 . , , . .r                   ;i < .p.:      ...g .
                    ..                                           ;                                                           . y.
                                                                                                                                                       's.s                           .
3 acJ                  4
                                                                                                                                                                                                                                                                                                                                                                                                                  . . ,                                    ,                                               g a                                         s                                          .               .                                                                       .\
                                     .                                                                                                                                                          .. .                                                           .                                                                                                                                                                                          1 l                           -, . . .
J                              a.                    ** I           .                                      v                                  .                                                                .
                                                                                                                                                                                                                                                                                                                                                                                                                                                                           \
i     .                                             s
                 =w.  ..s.r                       .. *                                  . .                  ..
                                                                                                                            . . 64.,                         U
                                                                                                                                                                        .'.a..~.nh.s,. ,,...
                                                                                                                                                                                            ,             e. t,s,a               ...                    . .           . . . .v. .i.,
                                                                                                                                                                                                                                                                                                                     ..-             .... .a. , , _..-                                                                                  .e
                                                                                                                                                                                                                                                                                                                                                                                                                                                                       . ~, : ,             ..                 .a .
                                                                                                                                                                                                                                                                                                  ..~..;.                                                      w
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                               .~
:. ~                                            m.,,...                          .; N.' . ~.$                                                                                                              ..~.c                .*-                                                                                                                                             r                            .                                                         ...
w.
                                                                                                                       .r a
                                                                                                                                                                          .: t.
                                                                                                                                                                                   ,m.,5,                                              .,s .g :i.4 e y 9.4                                                                          .                 . t"i v. ,~- . . Q. 1,;. T .* m..-}               -
ex .ase..v~.
r.
             ...ec.w.
                *!_.q. . ...w .;;. ..
                                                 ... s ,. . .
                                                                                                                                                                                                                                                                                                .   . w         ..
                                                                                                                                                                                                                                                                                                                   ..                          ,     ..                  .,\               ...               <
                                                                                                                                                                                                                                                                                                                                                                                                            .2                              . , .j.Jv :.                                                .        .. y(,'s
                                                                    .                    .t. .            .          p u.                                      ..
: x. .
: r.        ,
                                                                                                                          -                                                                                     .1                                                                                                                                   ...                 .
y,.                  .                                                                                        ::'                                     *- ;~.
l;. .&. Q y:n;                                                                                                    n.
4                                                                                                     y.? ,.                                                                              x.*                                                  :,;..             *                                                                                                                      .; .~ :tS.'
                                                                                                                                                                                                                                                                                                                                    .ofce
                                                                                        ;.:                                                                                                                                                                                                                                                                                                                                   .~
   . .                            p . ". d                                                                                                                                                                                                                                        ,
                                                                                                                                                                                                                                                                                                                                                                                                                                                             ,             I           *,               .e          .             .. e w >. ^-
y-                           ,                         g              i;                      -
l
                                                                                                                                                                                                                                                                                                'g. ..
                                                                                                                                                                                                                                                                                                                                                      ,..- ~
g o
                                                                                                                                                        ,o                                                                              .                                                                                           ...                                                                       . .* .                       .
                        .: .s.* *. . . .                        L                        .:                              .r d
                                                                                                                                                                                                                                                                                                      -                                   s
                                                                                                                                                                                                                                                                                                                                                   *                              '                                         n ''
i                 . .                           !
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                           -l
                                                                                                                       .A m
5 5                                                    ..
q l.
                                                                                                                                     ,                                                   .                    .                                                                                                                                    .                                                                       .,                                                i,
: i.                         .                                                                                                                              .                          .                                                                              .
i
                                                                                          -.'=                            )C       -
                                                                                                                                                          '. 3             ;      .                                                ' ' . . ..s.                                   47, .T
                                                                                                                                                                                                                                                                                       ...s
                                                                                                                                                                                                                                                                                                                     .                                                                 l k
G.,
                  .~.                                  g* W                                                                                            . .. p ,e-v                           f .. 'o., ,                          , s. *,.. ;i%<                                                                                     ..                r                     , . .
                                                                                                                                                                                                                                                                                                                                                                                           .. ,, *w.s        . * . .*.          -            . . .
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                 .r."...,N,. - ..
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                  <                            ==*
sv v.,
                                                                                                                                                                         .: t -                                                                                                                                                                                                                                                                                   a..
              . .: .                            :. e                                                                     g*7r           y                                                                                         ..:..,                              .C.*,.%.'n''/7,'s,l                           ~x . ..t.. . .t,.s.                                                                                                         . ,                                                              -
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                'W g.
                                                                                         . ..t.. .-
e m .~                                         .. e                                         .,.                  . ..-v-                                                                         -                      e .Z.y.                                                                               %- .%                               r- . ,s ,                                                  .             s,            .a.? - "a                 .
r.- , ,, . ;.^ .'
Q's 4
w
                                                       . .C .
                                                                                       ==ws".
                                                                                                                                                        .l.'. &... Tm                       %'. p.                                 4..'=.=....u,*'+..?.y.                                        wtY..-r                             '. V '=. o.d'.*#,%*n * . * -
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                  *. =s^*                                .
             . 'ym
                                                       ...~=*                                               .
                                                                                                                         $              L                               l .*.                                       . .                        .                                                   1                                                                    \*.
                                                                                                                                                                                                                                                                                                                                                                         . .                             . .,w ,r.< ..                                                                                        l..
                  . .sus 4 .*-. .. ,.....<..-)"C
                                                                                                                                               . .s.                              ., ~.                                                                       ,..       +.                          ..                                                 ..                                  ,.                                                                                         ,
O                                                                                                            . ..',. !
                                                              ,,,                                                           j ~.               . -.                        s- r . ..
                                                                                                                                                                                               .p. w-t M g/ <s:.t. -.
                                                                                                                                                                                                                                                                                                                                                       ..g               . .
i*-
                                                                                                                                                                                                                                                                                                                                                                                                          .i ..~. " ..
v~
* yn;.~w-3E.;                                                                                                                                                                                                                                                                                                                        ....                                                                                                                                                                        :
t='                                                                                                                                                     ..                                            .
                                                                                                                                  >.. >.m.ql,.,e.                                y p . m.                                                                                                                                                             :'n . u, . w%                                        v. .*
o se,.,.v.                       ::x:                                       a                                                                   .:
                                                                                                                                                                                                                                    . u. .u               --.-a. . _. , ...                                                            7                                                                                                                                          :..                              ..
e,
                                               .....v.-
: 3. .~                                                                                                                                                                                                                                                                                                                                                                                                                    ,
g*                                                                   x.-                                  =                              ..                                                                                                   {
l               l ur                               2.                 t.                         .                  .                    .. i                 . .                                  ..                                                                           .                    ..                                   .               .               .                                                                             O W .WiM.      .. t c               ..e              ..        o F.!                 Un!RM.. hM. M EM                                  ,..
ME                                  l.              .h **"90                                                                                                               i
                   . .. ,-  . ..                          . . , . . .                    s, l
O
                               .         . .                    ...                                                                  .                       ,              t.,              ,,,                  .. . ,            . .                                     .                             .
                                                                                                                                                                                             , . .                                  ,                                                                                                                                                                                                                                                                                              ,I
                                                                                        ==                                  c ..                         ..                 ..y              ..                                     ,.
* v: . s. . .                         .g.
                                                . .ga,
                                                     , . . .-..,s...
ys ..*
                                                                                          .                   *                                             .              us .                                                                                                                                                                        ..~                                                    Vg.; }?' .                                                                                           ,t::
ae s
                                                                                                                                                    ,'.i
: s. . . 4 g--.....t                                                                              v. ' & :=                                                       e *.;1,,2 * * *                                                                  /< .*.k: .m.
                                                                                                                                                ,t'...                                                                             .}..c.. e. ,.                                                                  . a r. .'v .~.i". ..
                                                                                                                                                                                                                                                                                                                                        ..x                                                                            .                                                                            .
: g.                                                                                                                                          ./:*                                                                                                                .                                                                                    .
: s.,?;h. . .f#,;-.y ...                                                                       h.
                                                                                                                                   ,-                              . .r ., ..s. L, .
                                                                                                                                                                                                                                                                                                                                                                            .~4 .s. . * * " ,- . . . .                                          . .                 . . s,..                               .
                                                                                                                                                                                                                                                                          *.,.,                                                                                                                                                                                                                                              '    ti .
a.43.,.m,.,t*.                                                              .             .                                                                                                                                                                                                                                                                                              .
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                  . .t.                        <*,
                                                                                                                                                                                                                                                                                                   .,t>.. .*
                                          . A - r e. ~.                                                      s                                                 J.                                              m*,                                                                                                                    '   *   *       **'**
                                                                                                                                                                                                                                                                                                                                                                             ' ' ' , 'i.' '                                       t'                 *? .
L*s                                                             ..
* n... a.a, .a.,e,
                   .=s.:
: s. .
                                                                                                                                                            .r                  4-
* 7. .
s
                                                                                                                                                                                                                                                                                                                                                                 ,< sn                       .~             ~                                     *,                     *               *                                        ,.
Q                =                                                 e
: .s, #'i.f* *. re;<                                                                  g.                                                                                                                                                                  u .,                                                                                               ,.
e a e et.                               ...                              #.}.                       aj                     .
                                                                       .s a.r. .... .*r* . ..
              . g.M                                                                                                                                                                                                                                                                                                                                                                                                                                                 ...
g*s,_.)" . g* ,i.f,#.21.a..
s
                                         * %'1' .4 r:* > tin                    ,
                                                                                      , .T o     .
                                                                                                                            ' *J.
t .r         g. .                           .p:;$ 9
                                                                                                                                                                               . . . . , , f.4 ;Q fa,p                 ..
A res. .q.,
                                                                                                                                                                                                                                      ]) o
: c. ~. <
g 9 p.,.                    7 ',
* 4 a<
a.*,;*
: t. .
                                                                                                                                                                                                                                                                                                                                                                             ' - ~
ov;"
V' . * . .
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                     .?/?
: 3. ' 4 '"                                   ,                                        .                                                .                                                                                                                                                                                                                                     .
s ar                         .. e.a                           sa.                               .. s.*                                                                              mo                   s. *                                                               ...                  .                                                                                                                                          .. '                         ... .*tr
                   .                ...v..*.    .                         . .su.           ;. .              s..u.
v esg
                                                                                                                                                                                                                                                                           ;* .t,                    ...o                    .*
                                                                                                                                                                                                                                                                                                                                                       *,1.g? .*.,.,h
                                                                                                                                                                                                                                                                                                                                                                                 -~          *               ~.*.
2d /v ., "*.
g.. *' t *
                                                                                                             ' .1W "*                                                                                          .q..                 m;'dj .T:r f                        .
44i,,*T.*g,                    . ySl".,i. .u,)                                                                 .'
lg.I'.m-                                                      , .e                                                       ,$:.f.$i.                                    ',*., ,",'                                            - '.*J.                         . - .             'a r s*b.                  . ;.a.'.
                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                                        ./
5..                                                              '':3'r.                               .N ,
                                        .          . - . - .                                                  .                                                                                  f-                                                                                                                       . - . . .                                         ,.                 ..                        .                                              ..                                .                        .
              .g-                             . ,, * '            .
1.-
c
                                                                                                                                                    .I,    ., . I:a... g                                         ..                   i..-                     -
                                                                                                                                                                                                                                                                                              .L.y-                       ,                                              [.
                                                                                                                                                                                                                                                                                                                                                                                                               .                                                                                                    f."
                  ..: . . .                               .3 .-                                                             .O.                                                                 .a ..c                                ) . .-                    .
        -             . . . , . .. .: . s                                       .                                                           ..                                                                                                                                                                                                                                                                                                                                                                                   :
                                                                                                                                                           .,,...,..a.                                                                                                                                                                                                                                                                                               . ., .. . , . . .. . - .
                    ...,. ~                                                                                                                                                                                                            ...,.4.....
                                                                                                               . . .                                                       .s.      ..                                                              ,,,,                  .

                 *                            -     --                                          -          '~                                                                                           .             .a.,.....m,.
                      ~ ~ - -
v.
: a.        .        - . = -        . a.. ,
                                        .-              ..                                           s..-   .....     . . _ .              . . .                   .
                                                                                                                                                                                                                  +          .
e PV
: )'          g                          *                                               .                       .                                                                                                                  .
L.                 o l'. ,
p 0                                                                                             @,,.
i.Ch g c;                                 .                                                                                                                            ,
a
                                                                                                                                                                                                                                           . h*
 !k                                                                                                                                                                                                                                    . l f . R .;)
j                                                                                      TEST PANEL PREPARAT10il DATA                                                                                               .
                                                                                                                                                                                                                                                     . 2.s -
j?
    +                                                                                                                                              -
                                                                                                                                                                                                                           .                         2M l h ~;
l: 1.               PRODUCT TO BE TESTED:                    Ihstec lis/nentee 12al Ae.c incalutee 1201                                                                                     .
2.
l l                   TYPE SUBSTRATE: Concrete                                                                                                           .
[,'<
;          3.       SusFACE PREPARATI0It (Describe):                       All surfaces liehtiv virehr- hd en r e i efflorescence and/or                                                                                                      3
[. . ?.
ii Imitance, followed by a ao Pst. compressed air blow M .                                              -
                                                                                                                                                                                                                                                     .k ,
If                                                                                 .       .
:. '.)
I       7,b,
: 4. PRODUCT BATA: 5AWI.E 310. (s)                              -
6151. 61s2. 6153                                                                                                                     g                        2q l1                                                                                                                                                                                                                                                           4 i 'e       5. DATE Alm TIME CURIIIC COHPOUNDED OR PRIMER APPL.IED: n/A
                                                                                                                                                                                                                                              \
i                                             .  .
THICENESS             TIME 6 DATE                                    g&
PRODUCT                                                AP71.ICAT1018                       CONDITIONS                                                                                        ,
it. COAT                    PRODUCT                CODES             -  BATCH #                                HETHOD R/H(*F) 2R.M.                             (ins.)
* APPLIED                                       .i i, e
l                                                                                            .                                                                                    -
1               Isutec Ils                 42s6/42s7/42sg                   squeegee                                  69/s6                                12.3              4/2/s4                    -         i l '.
sprey                                     6s/62                                 3.7              4/5/s4                              I
!E ' 2                        untec                 1201                42s4/42s3 3                u tec                 its                  42s6/42s7/42ss                  squeesee                                  69/67                   .
12.1              4/7/s4
((I.
l )0 y
l 4
4,               uutec         .       1201                 42s4/4285                       Spray                -
74/74                                 3.5              4/9/s4                                          .
                                                                                                                                                                                                                                                           . *. 3 l                                                                                                  .
                                                                                                                                                                                                                                                      ,o
[i',
It l;
:                                                                   ~
                                                                                                                                                                                                                                                     'x -
4,
       .                                                                                                                                                                                                                                              ' '.,i E. 4.i .
i
                                                                             ~
60 - 100              *F       REL. IIIMIDITY              40 - s0 I HINIMUN CURE                                          a         DAY $
                                                                                                                                                                                                                                                   '{
: i. CURIIIC COIIDITICIIS: AbSIElfT TEMP.
;      .. TEST PROCEDURE:                     nicameter Adhesion                                                                                                                                                                         ,           .[. .. '
TEST PREFOAHED BY                     Imperial eDATE $UaHITTED: 4-17-se g
REPORT IIMHSER                   1st APP 90VED BY:
                                                                                                                                                                                                                               .                      p, a
                                                                                                                                                                                                                                                      ![ f[
                                                                                       -                                                                               .                                                  .                           [. ~'
tt (;
i                                                          _ _ _ . _           ._.                                                   _ _

                                                                                                                                   . . . .. . : . v .                                     .e.!
                                                                           . 2.     .........__..._-           _vc                                         .. . .. . c .c. . . & -
_g y                  *                          -
m
                                                                                                                                                                                                                               "[;
                                                                                                                                                ~
* W                                                                                 @,.
(.-                                                                                                 .                                                                             .,
I
                                              ~
                                                                                                                                                                                                                   .           I U-
                                                                                  -                                                                                                                                         u {. q TEST PANEL PREPARATIOil DATA                                                                                  .
                                                                                                                                                                                                                                           )
A. A .
: 1.      PRODUCT TO RE TESTED:          Mutee 115/uutec 1201/htee lis/uutec 1201 I      V'*
i
: 2.      TYPE SUBSTRATE:        c - rate g?.4
: 3.      SURFACE PREPARATION (Describe):                An mort.c.. limhtiv wirebr ' d to re r,w efflorene.ac. - '/ar Iaitance, followed by a 80 PSI compr,essed air blow doen. -                                    .              .
Ly{
                                                                                                                                                                                                     .                         m .~
f,.$..
4.~
: 4.      PRODUCT DATA: SAMPLE NO. (c) : _ 6154. 6155. 6156                                                                                                                                     t                                '
: 5.      DATE AND TIME CURIl0C COHPOUNDED OR PRIMER APPLIED:                                      n/A                                                                                                                         ,J, 4
                                                                                                                                                                                                                                               +.
THICKNESS                TIME & DATE                                                   , T:
i                               PR060CT                                                  APPLICATION              CONDITIONS                                                                                ,                    .
(ine.)                APPLIED COAT          PRODUCT          CODES                  RATCH #                             HETit0D R/H(*F) IR.H.                 --
r.
1            Nutec            IIS            4286/4287/4288
                                                                                    '    39"**8**                      69/86                               37.5               4/2/84               .
                                                                                                                                                                                                           .                    ,e 2            Nutec            1201           4284/42ss                              SPr*F                         68/62                                4.3               4/5/84                                             , 'i 3            Nutec            IIS .          4286/4287/4288                         Squaegee                      69/67                               11.2               4/7/84         '
                                                                                                                                                                                                                           ,   . 4l ,
4 1201           4284/4285                              Spray                         N/74                                 3.5               4/9/84                                       g p,. 7 MuJtec                                                                                                                                                                                                       Je,
                                                                                                                           ..                                                    .                                             FW
                                                                                                                                                                                                                                .n
                                                                                                                                                                                                                                'j e i-0$a
  ;URIIIC CONDITICIts: AHRIENT TEMP.                     sn ' tan *F                   REL. NIDGIDITY 40 - 80                I HINIMUH CURE                         8         DAYS l}
fEST PROCEDURE:           E1cometer Adhesion                                                                                                                                                                 ,
                                                                                                                                                                                                                                   ]
                                                                                                                                                                                                                                   'j IEST PREFORMED RT:           1 - remi                                      *DATE SUSHITTED: 4/17/84                                                                      ,
:                        REPORT IIllHReg               759                                                                         ,                                                          f-
  .PP90VfD BY:                                                                      .
                       "V                                                                                                                                                                          ,
                                                                                                                                                                                                                       . i;< l t
                                                                                                                                                                                                                                  - .g
                                                                                                                                                                               ~
                                                                                                                                                                                               .,                                 f[q
                                                                                                                                                                                           -lfJd                     .       , [ .;,_

                . :.2 : .:..              ,
:. s . . '       .. .                 ,;         . . . a :r, ,:. . . . a n : :.. -     .s.a:~:.::. w ..:; --
1 .t:. .. . .: . ..:. .:.. . a.z .+ .hi'MN' l:L f . ',''!?"m.:_                ' m.,
          ~               .                                                                                          ,
                      . < - . . ; :,      ..       ..s   ..         - u - n ... u i .:                       w ... ^.       L .                              '
g*
O O                                    .
GI             -
                                                                                                                                                                                                             .e
                                                                                                                                                                                                                       -    M}.
h{
                                                                                                                                                                                                                            ;f .,.% -
S t.
q
                                                                                                       .                                                                                                                    .-;L-q                                                                                        TEST PANEL PREPARATieII BATA                                                                            .
                                                                                                                                                                                                                            $k
                                                                                                                                                                                                                            %r., .
4       1.       F30euCT TO BE TEsTEDs                        IIntee lis/uutec pl/Ilutac II/thetee 1291
                                                                                                                                                                          .                                                 Q..
: 2.       TYPE SWesTRATE: r                  rara
: 2.       L..
Dr*
3., SWRFACE PREFABATICII (Describe): All anarfaces li=kelv wirehr- ' ' ra                                                   r--          af fiar. ra-e. - '/ar
                                                                                                                                                                                                                       . 3 .-} '
lait-e. follaued by a s0 psi c--rda==J mir hians 2---
                                                                                                                              ~
K,
                                                                                                                                                                                                                        ,   +
                                    -            -                             -       .                                                                                                                                    ?;.;          .
                                                                                                                                                                                                                            ;.~ y 3-
: 4.       PROBUCT SATA: SAtti.E 310. (s)                                6157, 685s. 6159                                                                                                                  .
  ,.                                                                                                                                                                                                  a                     s.
: 5.       DATE AIS TIME CURIIIG CGHPOIIIIDES OR PRIDIER APPL.IED:                                        N/A                                                                                                              ..;
                                                                                                                                                                                                                            ; .e 1.1 j                                                                                   .
g                                       PE30HCT                                                   APPL.ICATICII                  C00SITI000$                 TMICENESS          *1ME 6 BATE                               @r.
                                                                                                                                                                                                                              ~)
COAT         FRCSWCT                CODES               -
BATCM #                            DeETHOD R/H(*F) IR.M.                   (ins.)           APPLIED                                         1 I                                            .                                                                            .
r u
   ~
1          n=cee              - las                   42ss/42s7/42ss s ,**s**                            sofos                      12.2             4/2/s4                  .
J. . .
4'
        -2             antee                   12el               42s4/42ss                         spray                               6s/62                         4 '.3         4/s/s4 3          untec                   il                 4290/4292/42,3                    s ,mes**                            69/67            ,
4.5           4/7/s4                                    j..[
p        4*         Ihetec         .
1261               42s4/42s5                         Stray                               74f74                         3.5           4/gfg4                                   f
: k. y -
I       .
l5       ?i' i                                                                                                                               .
nw
    ,                                                                                                                                                                                                                        q q'
                                                                            .                                                                                                                                                F CMIIIS COISITIouts AISInff TBr.                                60 - les            *F       REL. M IDITY                40 - 80 E MINilRRI CURE                       a-       DAYS                                    %.
TEST ynnrenames n r                    ..e     -      -e a            g9 Imperial                                '
* BATE sustIITTES:               4/37/84                                                                                 !                ~~..
TEST PREFORBIES BY.:                                                                                                                                                                                                             .
_A[NAR
      .ernovEs av:                                                                    mErenT       uunesa              25e
                               -w                                                             -
e M>
d r       *   .'l 7
i                                                                            -
                                                                                                                                                                                                                              ?'k
                                                                                                                                                                                -                  f .,.                     .et            ..

                                   . .a ' ' . c .-                           v.        .        _ ;. :        a..            ..;;.;. c. c.;_.         3              _
                                                                                                                                                                             .. _,          , , z. ,ga u.,
                                                                      . . . .: . .                                                                                                     ;,..:              i. G rw . ' :                                     .
a.:,:.            .z-l. n          . :;;;.w . ..... . w .                                _-              .
L
!p I
O                                                                                 O                                                           -
Es                   . ~ :o.F.
s.
h   .
                                                                                                                                                                                                                                     ,          y;
                                                                                                                                                                                                                                                .s;
                                                          -                                                                                                                                                                       .-                    i,
                                                                                                                                                                                                                                     '?              ?
i,         .                                                                                      .
8, I                                                                                                                                                                                                                                                             '
TEST PANEL PREPARATI0II BATA                                   -
                                                                                                                                                                                                       .,                                       j' l
: s.   -
                                                                                                                      -                                                  l l
thetae 11sfu ee 1101I                   ., 111 meme 17en                                                                                                                                   2l?
<     1. P9000CT TO BE TESTEDs                                                                                                                            -                                                                      l          -4 .
I e                                                                                                                                                            "                                                                     !
                                                                                                                                                                                                                                                $.4
! 2. TYPE SWR $TRATE: Caecrete                                                                    -
: 3.     $UEFACE PREPARATICII (Describ ):                         att         .far.. 1s.6,E wirebrushed to r==Ei af fiar----- . '                            's--                                                              !         M
                                                                                              ~ .'                                                                                                                                              W) laitance, followed by a 40 PSI comer'-- ' mir ha                                  '--                                                                                                                           .
                                                                                                                                                                                                                                                @F 9:
                                                                                     -                                                                                                                                                          *?
: 2.        f 1
                                                                                                                                                                                                                                      -         fii, TU 6160. 6161. 6162                                                                                          -
: 4. PRODUCT DATA: SAleLE No. (s) :                                                                                                                                                                                            '          .. e
                                                                                                                                                                                                                                                }'.A
: 5. DATE AIS T1HE CURIIIG Cots'0UNDER OR PRIMER APPLIED ' isla                                                                                                                                                                .
                                                                                                                                               ~
                                                                                                                                                                                                                                                     , -. I.
APPLICATI006                 CONDITIONS                TNICEIIESS                     TIME A BATE                            .                       :
PEsuCT                                                                                                                                                                                         :
R/H(*P) 2R.M.                 (tas.)                       APPLIED COAT          P90 DUCT             CODES                      BATCN #                          HETIIOD        ,
I i, , 4 a           m.t.c                 als                 42ss/42s7/42ss              -
Sq         sa.                       69/s4                   36.o                          4/2/s4                  ,.       .
                                                                                                                                                    .                                                                                              7. s es/62                   17.4                         4/5/s4                                                o; 2            met.c                 stat                42s4/42s5                       sPr.,                                                                                                                                                            ,
i:.
3             m.t.c                  1                 4290/4292/4293                  sg         s..                        69./67                  21.9                         4/7/s4-           '
                                                                                                                                                                                                                                                  ;-j
                   ,.                                                                                                                                                                                                                                       i 4
II tec               120t 42s4/42s5                       Spray                                 74/74                   16.s                         4/9/s4
                                                                                                                                                                                                                      ~
                                                                                                                                                                                                                                                 -t.
                                                                                                                                                        *                                  .                                                     .g';;
v..
                                                                                                                                                                                                     ~
g.
                                                                                                                                                                                                                         .                            ;1
                                                                         ~
40 - so I MINItast CN E                             8-                                                                  .M-
                                                                                       *F    REL. MSIIDITY                                                                              DAYS CURIIIC COISITICIIS: ABSIEtrF TDIP.                            so - 1an                                                                                                                                                                     4r
                                                                                                                                                                                                                                                 ; 3. .
TEST PROCEnWRE:               unc---r.c =           =e                     -
I                  . .r.s e                      w Test PREroeleEB BT:                  -- - ;-sal                                    *DATE SusHITTES: silitas                    -                                                                                                                        $
APreovEn BY:
y M                   :: #
REPOR.T WIsWER 759 e
                                                                                                                                                                                                                                                'Q j.
                                                                                                                                                 .                                                        .                                     g.g
                                                                                                                                                                                                                                                .e
                                                                                                                            ..-                                                                               ' . ,2                ,
i

y; N. -                                                                           . ww.n .
;                v.:.r . r;. .- .- !.i> . s '* -    n '         -
sav     , + .
o T22-4201 06/22/94                                                                                        )
I Allegation No. 2 Specific sequencing of coatings systems not required. For example, NRC (sic) No.
C83-01752 dated 06/23/83, Disposition section, first paragraph, states: " Table A2 in Appendix A of AS 31 specifies acceptable coating systems, i.e. , primer and final coat product identification and vendors." Then goes on to say that full sequencing is not identified. "This table does not identify full system sequencing or application parameters." Does a system's sequencing change for a repair! Why? Has the repair sequence been DBA qualified?
Evaluation of Validity The allegatica is not valid. Specification 2323-AS-31 Appendix A, Table A-2 (attached) does require specific primer /copcoat sequencing. Not a 3 to the table      .
* states "It is essential that coating systems be used only as specified above, unless an alternate system is proposed by a coating asuufacturer and subsequently approved by the Engineer."
The specification limits application paraseters to " manufacturer's latest application instructions," which includes field touch-up and repair.                       :
The manufacturer's data sheets, application instructions, and letters clarifying
              . procedures were the basis for the application procedures issued for use at CPSES.
These procedures described allowable overlap during touch-up or repair and sequence of coating application.
As indicated in our response to Allegation No. 1, the coating system sequence on an area which has been repaired may differ from the coating system sequence which was subjected to DBA qualification. However, due to the limited area of coatings involved in overlapping systems as a result of coating repairs, this issue has never been considered to be significant enough to warrant special consideration
  -             such as DBA qualification.

              ,g      ,y,..
                                                      .      .         w                  .,
                                                                                                                  ..r ,: ,. . ., ,    . ,_.          .
         .~;. _e.,...,e.s.. >.
                                ..r . ~ 2d.. ,.,:_ 3, .,:. ,   , g , y,.;: _ ._ p , __, . .,,- -_ , . ,
                                                                                                               .,           ,..e  .
__   , . . sh;a , a;sg m
'j _
l
.I Safety Significance
.l I
l                              None
  ,'                                                                                                                                                               I
 . e, Generie Implications on other Systems or Contractors Not applicable e
4 4
s 4
e 4
3 4
6 6
4 4
h

           . -- -                                                    . . ' ~,      ...<.s::..:      , . . .
M ?~ *:,MLa xy 4.46.t.%+ -' .:- ? - ~ . c~M n e -
                                         ..                           e c?>mim % n ''%                           " '
* r : "    -u- - ~
                                 . _                 _                                                                                            =
                        - .'.. - . -.         . . ... .              --                                    . .   - . .       . . .        .:.    .+             -
    ]             !D l
j
* Gibbs & Hill, Inc.
Specification 2323-AS-31                                          1 j                                            ,                 ,
Revision 2                                    .
4
                                                                                            ~
March 15, 1984 Sheet 1.of.2
                                        .I
                                            )                                 -
     '                                                           -                  APPENDIX       "A" TABLE A-2 APPROVED COATING SYSTEMS FOR USE IN CONTAINMENTa                                                        l.Rav. 2.
Steell I                             Manufacturer                             Primer                                       Toccoats Ameron                                   Dimetcote 6 or E-Z                           Amercoat 66 Carboline                                Carbozine 11                                 Phenoline 305 Mobil                                    Mobil-Zinc 7(13-F-12)                         Series 89
                   !         I Epoxoline 66 Tneme-Zinc 92E-12 Tnemec                 -                                                                                                           -
2,                                                                   .
Southern Imperial                        Durazinc 560                                  Reactic 1201 Ameron/ Carboline                        Dinetcote 6             ,
Phenoline 305 Phenoline 305                  locAst,s7t.g.o
       ;                           carboline                                carboline 191 Primer
* Rev.1 Concrete
* Manufacturer                             Surfacer                                      Toccoat Ameron                                   Nu-Klad 110AA                                 Amercoat 66 Carboline                                No. 195                                       Phenoline 305 l
Mobil                                     46-x-29 Epoxy                                 Series 89 Stonehard/Tnemec                         Stanliner 5                                   Epoxoline 66 t
Southern Imperial                       NUTEC 115
* Reactic 1201 Keeler & Long                            No. 65485                                     No. 7475 DCA f
* For Repair Usa only                                                                                                 is,376 4.o i                 -
                                                                                                                                                          % .2.
4

mu        . lc.)J: n's. . ...'.Dq8:*i'                    *y). ... :..+ .. .2 h 9J..W_W?9'''<.&;i'                                                            :-                    -, . .
                                                                                               -: ,.' .\;i- ?.-W
                                                                                                            ., . . .;c:.%m.:               ;n ':(-i      .'r4'.;y.   .
   .-'          h e fz?wini          .
6-~                   w-                      :.M           sis-         '?
                                                                                                                                                                                              .   .  :% : A --                  .   .. - . w:e~.:   '
               % .. ;                       r.
                                                                      . . ...  - 2:.: a . .. z . .'* . : .
: r.               -[&:-                        .
a 4                                                                                                                                                                                                                  ..
                      .           .. . ..._                   m....                . ._ . .       .....                      ,        .
cw ... . . .n
                                 .            ,..                                  i, ,                            .....                .                                                                                                    ,
                   ?  m.                                                                                                                                      .*.
Gibbs & Hill, Inc.
Specification 2323-AS-31                                                        ,           .                         I Revision 2
                                                                  -                                                     March 15, 1984 Sheet 2 of 2 Notes
: 1.        lainier=                   surface preparation shall be near white metal blast
    ,t cleanipg per SSPC SP-10.
                                       ~
Surface                      preparation                  shall                 be             . as     recommended by the
_                                 2.                                                                         ~
nam 2factuter.
: 3.         It is essential that coating                                                           systems be used only as specified above, unless an alternate system is proposed by a and subsequently approved by the r
coating                     ==msfacturer                                                                                                                                                           '
Engineer.                                                                                                                                       .
: 4.        NUTIC 115 or NUTEC 11 may be used for touchup.                                                                                                                                       -
{                                                                                             .
      \                    ee#                                  &                               ,
4 h
I                                                                                  .                                                                                                                                                .
I      .I I 1 t
I k
       ?
e i I                                                                                                                                                                                                       .
l                       .
l i
I
(
l                                                                            -
i        .
n                           ---ow,,,.m.w--m                                                           ---,e      ~,-w      ~ww-.,w-                      .w-o-ve,,e--~-~,-w             +-,-ww-r---eew---~~---,e-w

T.,       9 e i,      <.           4     - ,        -
                                                                                                    ~
                                                            *:<.5 & '                                             - - c ~CA.ie w   ,-;2. py . .v .: --J~:<             ' *: -2
                                                       '? :             v ~
                                                                                 .   ~.,-        '
                                                                                                             =-
TIK-4201 06/22/84            -
S Allegation No. 3 DCA, No. 17,142, Rev. 2, allows Carboline 305 to be applied over another manufacturer's epoxy coating. Has this system been DBA qualified?
Evaluation of Validity
 .                       This allegation is correct. This system is not DBA qualified but has been added to the Protective Costings Exempt Log.             (See entry number 22 on Protective Coatings Exempt Log attached).
Safety Sirnificance None Generic Implications on Other Systems or Contractors Not applicable 0
e h

        '4, F'' Y,   _
s -
            ' , .~-                                                         , . _ , **       '                :**
y._ y}'   'r                               _
J                                                    ,,    ,.                 _              _           e_   ,,         _
                              *        ~~          *
         ..                    . . .      .           . . . .             . . . . .    . .             , , .   , . . ~ .         . , . . . . . . .
                                       =. _y             :,...                                 -     ''                                                        **                           **
o'se                                                                                         3$
th
* g,%   s          @*                                 2                    "              '
6                                  +           '                                                            '
59                                  w %                     W n%                            as                d'                                '                    'T L.                                       I             hhg                                       <
                                                                                                                                *k S(                 .wk a                   ,
g                                            yh                   o j
m.
4                      ji                                                     4:D n b('                                        WM                   $
y                          w                            51                                         e 1
a]ag6         -              u                     $$ 8                 a-w                             s._                        w     -
s      a         e3 G            .                E             -
                                                                                                   =23           w%             3~G                   $e  a     f          E-                  -
Di O            E g                           ug                   E'a Eu               a e g                                       2             t-                                         g                                          d.
g$e o" s tc g
w 3
                                                                                                 .3"g                            ek$                      3-
                                                                                                                                                        ,js      3
{]D l-          om
                                          "       4 E                         a8                            ==$g 9
u
                                                                                                                                                       =          4        h 0-s                                s .bc                             E8            d               wy6'3W                                     d$m Egs W                                        m                                        g               2                     $$=                 a#
x W
9-          e
                                                                                                   =:
U h
                                                                                                                                 )9 GM ND S                              32 fu..                         u)                             l'$                                               8 L.                       O                                                      6. : .                                   x             .
                                                                                                                                                        .. -x                ..
Ma             eu                              A                -
z o
g[a 331 o3                 $g             e                     EB         -
h
                                 ~
6                 $*
H 8                4'Se d (i                                                                      $$npe                            f          4 o                                  ec sa                                    glitc                                                          be
                                                                                                                  @gMm,y                        b       b 5 ap w g 2
H O
m e
E
                                                               -$.saIgla
                                                                    +
e W
55 dE 8< C{d$g Hf u                4 du 3S {
s g5 i            Yi 4e g
cd ed er   44 d
                                                                                                                                                        $N W
o o        ''pe{
C D bmi-d                                    a.6f's$           FQp3                 sp a3 S                        g i                                           s                            5d6)$g g gs c                                                                       -
3          g
                                                                    $               l? g is s.p       E
                                                                                                                                                   .. h a
e yps 45       h a1   m Ed $34c          5          3        E3i g
d k kg  g              6.._
4, H 1.As ce d $ l"l,
                                                                                                                                                        $_U c     a  j   ,se           4 sa                                         -              ..
                                                                                                                                                                         ~
             $:($hy                                   ,              db                                                -
Ne               E         --               -
l a m . s n e m u m .,. - = = w w .. a

                                  . .                .,    .        v              -.
1           e., .     >_ . _ .
                                       . : , :. . , i -a :n. , . v.;*.z .2 !: .
w,i;3. .:_ _ g_. ~ . ygs; : .,g
                                                                                                        .        - . 4,gga ;
                   .. s                                1 3                  --
11 4
i
    .                          Txx-4201
,i .
06/12/84 y
1                                                            -
f Alta== tion No. 4
    .                          DCA. No.12.374 Rev.1. allows inorganic sine primer (Carboline C2-11 ?) to be top coated by Imperial 1201. Mas this system been DBA gualified?       ,
~                                                                                                                   .
Evaluation of Validity I
The CE-11/Nutec 1201 system has been DBA qualified.                  (See attached test report indicating DBA qualification for this system). It should also be noted that DCA No. 12.374. Rev. 1 deals only with the presence of C2-11/Nutec 1201 on Richmond Inserts that are embedded in concrete. Due to the size and configuration of j                            these areas and difficulties with application details, these coatings have been classified as indeterminate and have been placed on the Protective Coatings
      -                        Essept Log (see entry number 30 on Protective Coatings Exempt Log attached).
t.
Safety Sinnificance                                                                     .
None Generic Ins 11 cations on other Systess or Contractors Not applicable 4
e

                                                           .       .O .c         . .; ~
                                                                                  .                  .. . a.:     .w
                                                                                                                        .u.-42 ai
: l.                -
l            .
3
                  ~
h      9          o g     <      %y i A                        en                =          *n 79                                                                               '
g I'
                                                                                                                     =
I
                              -            h35 4
i; i'g     t
                                                                               $           @g qiOm1      8
* 1a !_
2                 .g        Ma          e           em 5                 e    j   Wi )                     35     h           i      $S         -
e s $u t            3 s      hl j $o 55 >E3$$.           3 me 22 w
                                                              -    si          5           ==      b a          a         8 s o s"                      a'       a3                       sg 2      h
                              $                   g     *) h El                k                    =t3 y            fh w
x                          i e      s    e            $.
g S mni          o 4
b W
                                                          $        =:
U I _6                   6%3g=5             D     9 IJp                                          4
                              .$                         V                     ld fa if 5             k                 s                             d$ l ?N S 3 so : {A.i38
* l!
u yl t u r j,>il Q 1  !lI!     I Q.l o!
y                         li
                                                                                                         !8    e  e  jjf
                                                                                                                     !<d W
e o
f 44 4        14-s               t           W{ jXS,addq        45 s s g e
b        !       b h        6 al !!u!paf-f.!                              mkh' 8
I 3e ka bedg a s45Ed(5ced                           <
St    HinduH 5 il h4 f.J l,
e k            el   (           :
                                                                                    . .,. N                        O
                                                                                                                       .-           3
                         .a               ..                         .

l                                                                                                                                                       -
\,>'.-                      -
                                                                                 .                                  t   .
                                                                                                                                                   . , . , . . < ,                  .'   ~        . . i.
2..:...:..<.
                                                                                                                                                                                                                                           . . .h.w . . u. . . .w.w ..:
                                                                                                                                                                       ; .:: ?:k s.s.. . C.~;.L . -- -
                                                                                                                                                                           ~
j'.y '.                                            .                .,'               .
                                                                                                             ~'.                   .7^ "'            - ~ -                                                                                      ~_.                    .
                }               . . --                                                                                                                                                                                                                                           . .[
D
                                                                                                                                                                                  -                                                                                                                       \
t.. ;
                              .. )                                                                                                                                                                                                                                                         .
l r.~                                                                                .
i g                                               .                                                                                                                                                                                                                                         l
      ..                                                                                                                                                                                                                                                                          b
                .h
  ,             s                                                                                                                                 .
TECHNICAL REPORT l                                                                                                  .
l l
* l f
3                                                    .
NUMar.R                                                                                                 . . .                                         <
n,.
                                                                                                                                                    . 353-42.
                                 .r .
                                 .s
      > 3,      ,                                                .
                                                                                     .                                                                Tm.1 tzrr FnocaatTo rYAZUAZI; DEA FEI2CRMANCE                                                                                                                                                          ,
      '4;-                                                                        of ovrar.Ar coaz:sr sTstzus (cammet.:st/nsr:12Ar.)
                                                                                                                .        nn srAvst prn? UzIr 2.
l
      ..E                                                                                                                                                                                                                                                                                                 1
                        -                                                                                                                               FOR                                                                                                                                               I
       ..o                                                                                                                                                                        '
                  .I .                      ,                                                                                                  auss At. usr                                                    ,
! .' !.                                                                                                                                         CUSTOMEF.
98                                                                                                                                                                                                                                                                                       l
                    ~
stout Amo vrar:za               .
          ,5                                                              subadtted by: casAz.s E. Aamot.n                                                    d4 j*
4,,
Date:
e                 nossar u. TArzon-gfg                                                                             .
                        .                                                                                    nacnasa. 24.19s2.                                                                                                                      s
                        )
                 'e                                                                                        SCUTMERN DerER!A!. COATJNGS CORPORATION. !NC.                                                                                            .
         -                                                                                                F. C. Ses 'JOTT,                                   New Orleans f.4eisissa 70189                                                                                                                   <
                 'J*-                                                                                                                                                                                                                                                                                      '
Phease (504)1541433                                                                                                                                .
i i
                 * (' ;/
NO           .
                                                                                       ,                              -         . a== e                     ., -                 m-.n
                   .. r .
e e
                                                                                       .xposemeum u                      a, = ---
t te tusmumme egy une y e.seems
                                                                                                                                                  . - nmam.aus   --- sumspem.meme   = = = a.f.tuu.s,.- o.ne.es.auremm.e-                     ene fesa.                                                  -
          ...r..  -
                                                ..                 .     : = .q                . .         .
                                                                                                                                      . - , -         . - = = - . . - - .                    .
                                                                                                                                                                                                   .. . a '                                           .                            .
i, d*~                                                                                  ,/QS],J',**,gM@fjf.l4'.{'*,.h.;h;[6l         ,
                                                                                                                                                                                                                                                  . , [* f s'.  ,
: l.        ,
1
                                 '/ ' . .,'. :.' -. .a.,               a.*D               .~* '. :".*e                              7.WO*4'*J                                 %,%*M -Qll# i "
: 2. ." :                   ..
                                                                              .p g .;,..a                        .r n >...;
                                                                                                                          .        .,      3... . y.g, ;,e,g y , j, .,,- _ - - _- . - _ - .. g ,,,, ,, ,, ,y , , . g, , ,,_

                                                                                                                                                                                                                                                      ' N f,;L,[
    ! N'                        ''*  - . .-
                                                                                                              =,_a_                        ,                ';',,'*           '
                                                                                                                                                                                                         .,.        ,a .
                                                                                                                                                                                                                                  ,y 3            .
g                ,,,,,,,g 3,__,;,s,,,,;,y
                                                                                                        ._=..,=.=,..,.*=*%q,.,,..                                                                                                         *--
      ,=.=,..%
                                                . .                .               J       ''                  == -                  -
                                                                                                                                             .4          ...
w ?+-h             -
                                                                                                                                                                                                               =*=a-__.-_-
                                                                                                                                                                                                                             .*        - ae.--                          ..   * *                           ~         ,
v                                                                                                                                *                                                                                                                                                              .             *
     *3                                   .                                                                                                                     ,
                      .                                                               ..                                                                                                                                                                                       *              =
s                                                                                  .                 .                                                       -
  ,a                       .
                                       '             *                                                                                                                                                    .                               ,         a ee.r,                                                                                                                                                                                   .
e                                                                                                    .                                                  .                                                                 *
     -.a                                                                                                                    -                                                              .              .
9                                                                                                                                                                                                                                                                                              -
   , =1            i-s                 n                                            -
Test PROGRAM TO ITAZIATE DEA FER20RMANCE
    } s'41 i                                                                               or ovEst.AF coATIsa strzzus (CAR 301.INE/IMFER.IAI.)
     ';                                                                               .                               30s asATEs. vAz.tzr est: I                                                                                                                   ,
i 4
                                                                                                                                               .     .E!EE.
i                                                                                                                                                                                                seettoe                                            Pase
       ;                                                                          InnsanoC=os t                                          I - 2.
t D*                                                                        STUEE & WE33 TEE TEST SPECMEN FREFAIATIDW                                                                                       2                                          3 =* 12 FROCIDURE
      }A                                                                                                                                                                                                                            ,
     ' M,'O                                                                        STORE & WERSIER. TEST 3FECME" FREFAXa=!.W-                                                                                     3                                       g3 ,, g 3
       ,j' DA2L
:. .y                                                                                                                                                                                                                                                                        .
: o.                                                                          CRNr. EADIATIDW/ DEA FROCIDUIES                                                                                                &                                  . M 6 = 111 E, - tu
        .?
                                                                             . AnIA=as iso n A. : m.: -                                                                                                            s          .
             ,         s                                                                                                                                                            .
       *I .                                                            .                                                                                                                                                                                                                        ,
e                                                                                                  .
        . =                                                                                                                                                                                                                                   .
        .h o.
I                                              .                                                                                                                                                                                              .
O                                                                                                                                                  I l                                 .,
        .t
         .1                                                                                                                               .
d i
4                                                                                                                                                                      .
e 4
e en.
                        '                                                                                 e g                                                                 ,
t i
e
         *t                                                                                                                     .
I         N s
         .b
                .         M                                                   ,
          --                                                                                                                                     . g                                                                                           .
0          .
.          ,t                        ,
      - y ..                                       .
                                                                                                      * * * . ' '.' , . 9 6 ' h .'.* .~'..'.,.I,..                                                                          '*                            *                           *
                                                                     . ,. /. g ' .I. ,4 ,
                                                                                                                                                                  .'                              *                                                                                                         .' i
    '" *d.*' ,                                                                                                                   y=.'' .. .,,p
: f. *.               '4 *              .
a                ,
                                                                                 . .-e.
                                                                                    ..         .,,.            f . * . .,                        . . .
l .4y   . . J .' , ' ' . .                                          ,     .
                                                                                    *      ,=*        .         ..
                                                                                                                      ,,...p.,             ,
                                                                                                                                                      .g.g*
                                                                                                                                                       ... ..,v.       .
* g.. .. ,* . . .                   ..                         .                                  .               .            . , , . j

s                                                                                                   -
{%.M.; g ... t : .:.p. :j. t.:_ a * ' bli* ~. _ . f *. i ' . %:. W -                                                        ,% ? . '**                       .w                   y c;_ :                    .,     .&                  ,e< n                          ,l:5. ..,a .;; ,
                                                                                         . . , ; . L.-it'.7.*,7 fi.;:'Mi
                                                                                                 '                                               - -            _ _ _ ,            _ . -[                   T _ .., .         .
                                                                                                                                                                                                                                                     . . , . . _ ,                    ]/ , ,,,,* .
                         .             O            -   .
                                                                                                                                                                                                                                . g ..                                         . . . .. . . .
                                                                                               .                .           s.   .
                                                                                                                                                                                                 .           v
    .f            4. b                 SCDFE:
The purpose of this test was to evalnata the DBA Perfotasaca of                                                                                                                                                                        '
Carbo 11as/ Imperial afW systems for use ac 3essur Valley 1
* e Baclear Plant. Systans to be tascad ars:                                                                                                                                                                                &
i                                                                                      A]: CZ-11/191
      ,                                                                                       31 Cz-11/191/1201                                                      -
    >                                                                                         Cl CE'-11/1201 .                                                                                                                                                    *         *
  -}.                                                                                         3] Cz-11/1201/192
                                                                                          , 11 Cr-11/11s/11/1201
                                                                                       .a u                                                                                                                                                                                                                                                        .,                       _
s:
                                          .       .m . ..s . :
    -3
                                  --                             The above systems ara possible overlap combinations at Besvar                                                                                                                               '           ~~
1'y on steel imbeds. Most staaL imbeds at the:~ :'~- -
                                                                                       -----d Th11ay                                                                                                                                                                                                .
project are. already eamend with Carbolina.'e CZi-11 primer on-                                                                                                                 --            -
j
                 ~
CE-11 topcoat with #191. When the adjacent concrete is conced
       ,,                                                        with 7-=--'=1 's 115/11/1201 syscam., some of sta coated' imbeds.
                                                                            ~
2                                                         a.rS                                                   .
g gggg epee 4mmna gggg pggpaged 13333g the 44 r_ M                                                                                          .1 C 1_
and Babster by paintars as the Besvar Valley Protect. The to f--*d = t                      7;          ^'
coated =p=e '==== werer them. ==h=4 e*==8
     ;l h t            -'
coordinated, then tasting activitime at CIsr authoriand. by Stana amL.Bebsters Purchase. Order # E24476.
The.nosk: was                                                                                  ~
i e,                                           ,                  .w.             .
d,,-                                    enerant 0F'IISULTS:.                                                                                                                                                                                                               .             ..
                                                                                                                    -- were. irradisted to 2.66.z 10 7 rads and them.
       ==                                                                                                                                                                                                                                                                                               -
Allcaselh 9-                                                            BRA casted with; ==w4-= e==p=e=ence and pressure                                                                                     persmatarr of 4                                                                                                                                                                                  a--'a*==d in accord--
340*F and; 70- PSTG respectively. All, panels O.                        '                                  ance with the acceptance ee+*=*ft of ANSI N101.2-
      .L                                                                                                                                                        .
i :.-
l                                                                                                                                                                                                                                                                                                            .
l '4    -                                    730CSDUII:                                                                                                                                                                                                                                                   ._
n,                                                                                                                                                                                                                                                                                                '
s J
f)
                                                -                    The test specimens vara fabricated and; costad at the Beaver
       $                                                             Valley Euclasz 21 ant $a Shippingporr Pa. Seation.I of.this                                                                                                                                   ..
zgpagg                        n.4== the Stone and Webstar procedure for test speci-
           ,5 The ===-d#4e penal preparation, data can: be.                                                                                           ... . C;.-               .             ..
men p                       --*d l '7 d                                                        .      found in Section 3 It describes tha coating.d"--*                                                                       ,---1'd--tion.
of Stone.                                            n r .;--
1                                                          performed by Senarc Painting under the sury                                                                                      - were            allowed med Webseme quality Control. Tha coated 7 '
to cura and them.were shipped.to                                                       7--- *=1 aa=e4nte                                   Coordi-                        ,                            ,
                                                                                                                                                                                                                                                                                 ~
3                                                              nation of the testing activities was. performed                                                                           by
                                                                                                                                                                                                         '-a- dat                                                                                   ..
i                                                           through its. contract with OREL. Anchord
                                                                                                                                                                                =*d=             of this casting M                                                        - program was ande by Stone and Webster per Purchama .o..rd.e.r                                                                                   -         #E2,4476.
       '.'3..~
as          =                               ...                             .
                                                                                                                                                                                      *                                 ..s..
j ., ?)                                                                                                     .
s
             ,       't.
i.Y                                                               -
       ..:t
                                                                                                                               .s     ..;...      .w..,...
                                                                                                                                                                         -s. . . . . . . :.,. v . c. ..*.. . .
                       -                                                                                      .. . , .                                    . ..                                       g           s                     .e                                               .. -
                                                                                                                                   . . . .s s. ,:h..: .a.,:s4
* I.,.,,,g,-*                                                                   <
a s . *-                                                                                                                                      -               -                                       .
                                                                                                                                                                                                                                                                                ,~',
my, . . yps               s .g g, 'e.;.     ..s .;..x.,g<.g.       4' g.;.g;g,,,;j_ .,-
                                                                                                                                                                         .: -w ... ., . . . . :.- ~y,;;            . ., ..; ,x.,.r. .        .
                                                                                                                                                                                                                                                                                            ~      .
ze .
                                  >.~.                    . w. r y .;._-. . . -                                                                                                                                ._                                                       . ~ -
                                                                                                                      . =w.;-M-2,n. .. e.. x%,
                                                                           .                         ..s.- . .. :.:::
                                                                                                                                                                                                                                            ;  .   , .. s       -  -
                                                                                                     *,g        ::.-,u...qg.w              py." ..jz . g,.sp,; .;_..gg                 m.:.:-n . .... .
       ..                                                           .; ' u-                             '
                                                                                                                                 . .a. n.: .:Ls,,
                                                                                                                                                                                                         , ;j.;. a 7.q,;,                              .                            .               . . .
- ?-
                                                  .          -   .-4                        . .        c. ;           .                                                  .

                               ~
A ., .s . ~ ys. . .. L . . . ._                                     ..a    n.,   .e.w+ , : ..:3          .                            . g:                ,    u e:            n      .
: _ ,x_ ,g                                                          _,3           _
     .s
                                        -       . - -- . .: c c. . ..m._
                                                                                  . . ., :w - . ----- - -
                                                                                                                           ----..n..
3..                   -
   .n                                    -
:t  .                    .
:/                              Test Program To Evainste DBA. Performance of                                                                                                       '
l    .
Ovetlay Coating Systemer. (Carbolins/ha--*=T).
N.                   For Besvez Valler Osit 2                                                                       .                                 .
3 y .                 Pagm 2                                                                                                          .                                                                                      . ..
   .,3.,,
t
:.g                                                        The'tast 7                                 - were submitted to Oak Ridge M=e4aa=1 Labo -                                                                                                   .
          .                                                  retorias, where-                                     were exposed. to a, canmalative radiation.
   ~'
dose of 2.64 z 10 rada and-than DBA tasted. The test was j                                                     dee igned to be subjected.to ===4= = temperature and.pressura Ji of 280*7 and- 45 25IG respytively. Essever. during the test                                                                                                                                                                                    .
                                                        . a sudden. surge da these parameters resultad in a ===4===                                                                                                                                                                                                 j
   .i
                                                                                   =
                                                                                          = of 340*7 and a. ==-4== pressure of 70 75IG. The.                                                                                           " ~ ~ "
                                                           'esaparature/pressurs spthe lasted for only 1.5 minutes. TSn
    %}                                                        <=4e4=r 28-hours of the DE&. testad were performed. in. ther auto-
:.g                                                        slave. Thar r==minine,11 daye were conducted in a constant                                                                                                 ~
tamparature chamber- se 130*7 and' 100% II.                                                                                                                                           T- C                                                '..
r                                                                                                                                                 -
l,                            IISULTS:
:14                                                          The test results, Seccianc 5 describe tha.aand4e4a= of the --- '*
3                                                      folloeing;irradistica thee again at tha and of DEA tasting.
       . 7.                                                                                                                                                                                                                                                                  ,
CONCLU5 TORS:                                       .
Y{ *               *
* g T                                                  'The: tasted syscams.ast tha acceptance critarts of AESI E5.12.                                                                                                                                                                       .
       ,. t N,, .                              -
6 =d4=e4a- cat a =nea). and, AEST. E10I.2. (DEA t--**=9. Tua-                                                                                                              -
       ; - ' d,'                                               defects- (unacceptabla.pez AE5I7 wara noted an. pannis 4-1-4-26 O                                                        and 4-3-4-4 along.the costdag overlap arms where. the repair
      ,t easting was tied.rinto therprevisasly applied system. Some
: --                                                    minor _; - -*- was +1                                                             --. at this sacerface prior to i+                                                    sahmittal of'the penals.ta CIEL. This - ; - =                                                                    -
can ba 9
* ascributad to the taping anthod used te apply the repair coat -                                                                                                                 .
           .(                                                   tag ande the N-eh of time the tape was. allowed to remata ca.
When the specimens were received by                                                                  Y--        '=t the panels l c.h                          /                                the tape was still. intace alans the edges of tha 3.4. and 4A.                                                                                                                                                       *
         "?                                                     series. The taping resultad in: high =d"--as along the tape.
       ?                                                        lina salvene entrapumar, and exposed repair c. R . Some of the repair systam began; to peal back a short distanca frost
          .i                                                    the tapaline whentha tape was removed. As a canaequence of
: l.        .
ehmaar observattana, the minor defects.noted on penals 4-1-4-l' and. 4-3-4-4,. abould be ignored                                                                                                                        Nda -
! .'.i                                                          four psamis. 4-5-4-6 , 4-1A-4-2A 4-3&-4-44.and.4-51.i % exhfhired
                                                                                                                                                             -----4 ="y aines. the .
3   ;
no defects.
        .i 1       ,,1                                                                                                                                                                                                                                     ,
if-                -
i,,
8
' .E}
              ?                                                                                                                .
>       ^A                                                                           .                                                                                                  -
4
                     .: 7 9
: 6. ,                                                                    .            -                           -
: q.         < . *..                 v.
                                                ,., ..:;. .;i.&..:L. u ,y?5 . . .
                                                                                                                  ; : .i. .. -. .. . .:
                                                                                                                                                          .                 :. s .                      .
                                                                                                                                                                                                                                                                 - .                     .                      1
           > .'        . .s       W         M.-*                              .
                                                                                                     .....             u-                      .L           ::. :: ,;:
                                                                                                                                                                                           .- . .                                     r.                       .-                           -
9 4
a.-{ .u
                        .=: ....   ,2 w      - !~..
: t. ';; -.   .; .r,-x;.,M,;
                                                                               .. .w. ...<.
                                                                                                  ; p...,.
                                                                                                     -z.               a."                                      ...+:,';., . u....
            ..          ,;,. v    . -
                                       .,.. - . .:.. - g ? : a w .~.
                                                                           . w ;.
                                                                                                   ...s.,         . . ,
                                                                                                                                                  . , , .: ...n            ,.         - ,- ,,-                                             ....                    . . . . .
                                                                                                                                                                                                                                                                                                          - y i.
jL                       ,
                                                                                                                                                                                                                                                                          *                       .            a

        .. e. .. .
- y:w . .4%k.p/-                              .1.
:< '. '> ~ if : eu . ? y . .:., a >:                                        . + .:;. ,h. . * '. -'. , u '.?                          <
                                                                                                                                                                                              ., , ; e .J                  (;                           ,          4.,y                            .
                                                  - - .                                                                         .y......                                                   ..                  ..                                                      .
w
;j.}c.9 ," M %                                        a.c.w                  a -            -...
                                                                                                             .: L            _.                     s.               . . - -       -          ..-s.'~.- i.'h - ] ..J---
* M .~:--- y jg y. -
  ' ,u M                                                                                                                                                .                                                                                .
7y                                     Manufac::urer:                                   Imperial                                                                         Analyticai Chemistry Division
    .d "w                                                                                                                                                                    ' Gak Ridge National 1.aboratory-October 29, 1981
   .j. g'- j                                                                                 New Orleans, t.ouisiana Date:
                                                                                                       -                                                                                                                                                    .               .                             l
  ,.               - --                                                                                                                                                                                                                    ...,.--                    . . . =
ST5 TEM IDENTIFICATION                                                                       .
x Steel panel                                             Concreta bTock
     *I CI-11/1201'/191                                                                                                                                                                                                       :.. . . ..
  .?,
CI-11/1201                                                                                   .' .                                       .
    *?
  ;;..                                                                                                                                                                                                           ~
        )                                    08A M                                                                                                                                                                       .
M. ~              -                                                                                                                                                                                                             .:            .       r-         s ..           .
                                         . ORNL Mastar Analytical Manual Method No. 2 0922.                                                                                                                                                   . :-           ...                     -:r.
  ? ,,,, .                                                                                                                                                                                                              - -
OR!E.1.og Book No. A9675, A10-8-1                                                                                                                                                                      .            .             .
        ,e
          ~
famole No.                                           OBA chase                                                                        Test results                           -                                             .-
t'-                                                                                            .                                                                                                                    .          :.                           .                         :.
          ' '*                                                                                                                                                                                                                         .: . .                               .~....:
; .? i. '                           -
3-1-7-Z.                                                  spraye                                        Front:. . Coatings intact.' nerdefects.aftar=
'4:                                                                                                                                                     one day. 811 stars, #6 few, at coating-'                                                                                           -
c ,Q)
                                                                                           .                                                            interphase and weld arse at endr of'tase                                                                                    --
                                                            .          . . -                     e. .            ..s.......-     .                      Rearr Coatings intace no. defects. after                                                                                                                  -
                                                ~
                                                                   .                                                                                    one day. . ' 511starr, #6 few, at coating
       );                                                                                                                                               interphase and weld.acea at.and..af. test
         ..                                                                                                                                                                                                                                                                  ~                                     ~
   . J.i                                .? '3-3-? '                                                        spray
* Front: Coatings intact, no defects. after                                                                             7'-
:I                                                                                                                            .
one day. Blisters,. #6 few, at;weTd area:                                                                             *                                -
   '?                                                                                                                                                   at end. of test.                                                                                                                             -
                       .       o Rear: Contings intact, no defacts after l -}*! .*
t one day. 8 listers, f6 few, insert area-at and of tast.                                      ..
s -.
     .4                                           3-5-7-6                                                  spray
* Front: C'estings intact, no defects aftar . '. ,.
one day. 811starr, #4 few weld area.~andi
     ...                                                                                      .              .                                                                                                                                                                  -                    ~ ~
coating- interphase-at end of tast - -                                                                                                    .
   ;....               ....                                                                                              .                               Rear: Castings. intact, no. d,e.fe.c.t.r. '.a.fT ..                 .
, 7:.
: i ..         c.
                                      -                                                                                                                  areas.                                                                     .
* Irradiated.                                                                                                                                                .
Evaluated                                                .
   .,... ;.? ;;             .                                      .
appro,.d- .                   . Y~Y&                                                                                                                -
e-       *                                                                                             .                                                                                                      .                     L
                                                                                                                                             . ,=f_ .                          . . .               e        .                                              . .
(
t
                                                                          - . . n .. . ~
                                                                          .....          ,r . r. ,, .. .. , . .-       -
:     ---.8.
:m.v                         . . - ~.. ., .. ,.
                                                                                                                                                             . .,. - . _ g....;.
                                                                                                                                                                                                   .            . ..;. .~.-. . .- ~. - .-. . . .-...
r,.
y,..,>...
n.y.:y.,.
                                                                                                                                                                                                                                                                                                           .a_
3
                                                                                                                                                                                                                                                       . .... .. . 3. :.:.
4-.                  ;                             .
                                                          .                            u. . 2 . ..
t
                                                                                                      .. . . . ,           ,.                .. ~ . .. . .                                                                            .                                                                ,.
1 . .r --                                                                      .  .
a'
                                                                                                                                                                                                                                                                             .h j
                                                       ,, _.             .: . .. . . . g. #                       .             , - . *               -

                                                                                                      , , w . a. .c,           :,.....                                                                           .
                                                                                                                                                                                                                                         ,.n                 .,
     . . r. w. x. ~ , ~ . ,
                             - . s. -
1
                                                                  . . m. .. ,e.
4..                                                  . :n, :n                * . .
                                                                                                                                                                                      .          ,a...<.-
s j.                ,                    .
                                                                                                                                                                                                                                                                         ,,a.                   _            1 l
                                                                                                  . . ~                                 .             ..                                        ._                ..._.
                                                         ..u. . . . , , . . .                                                                                                             .
  ;:t.                                       . . .       . .            .           ..                     ..               .          . . . . .            . ..,
: e.                           ._       .      ... .... ...  .
1
     . ....=,j                ,.          .
                                                                                                -               5     -
                                                                                                                        ,                                                                    -                                               o M                                                      .
  . $.f                                                                                                                                                                                         .             .                                                                                            .
     '9 Fage 131.                                        .-
4
    .s.
I 4, . -               .                          .
         ;                         -- --                                                                                          smaanT OF REstTC.TT .                                                                                --
                                                                                                                                                                                                                                                                                                     .:n
: .. :.: 3:
                                                                                                                                                                                                                                                               -         , : .. 3: m -
          ':: : ; G..?.                                                                                                                                                                                                                                                                                                       ,
                                                                                                                                                                                                                                                 ..                                       r.         .
                                                                                                                                                                                                                                                                                          --1,.,
DEA lasults                              - '
Systan 4...
5 ._. ...
                          .-- . 7snel No.                                                                                                     .
                                                                                                                                                                                                                                                                                                  ,as            .
v---                                       -                                                                                                                                                                        . .           . . . . . .
    .j:...
                                                  ;         I/I                                           C-u/12cr .                                                                        k Defects                                                                                                 r: .. .
                                                                                                                                                                                                                           . .:: ::                    .r             - n                 .r.
7
       ,; .-                                -               1/2                                           C-n/UDI.                                                                          No Defects ':,.                       . .                  .
1 5'                     -    -                                             -
g_njugg                                 .
m 3,g ,,,,.
1j3                                                                                                                                                           ., ...,. .. ..:.. . ,.
i                                                  2/1                                          C-u/us/11/not                                                                             #su                     .
y                                                     2/r                                          cr-n/us/u/not                                                                             isu.
:                                               2/3                                          c-n/ns/n/12cr                                                                            7sE-f-
3-1-3-1                                             cr-n/1201 c-n/1201/191                                                           M at coating incaryhase and vald ara
                                                                                                                                                                                                                                                               ~..
       '.                                              3-3-3-4                                             cz- n/1201,. c -u/1201/191.                                                      Mr==1d area                                                                                                 .
c-n/I2cI c-n/1201/191 MT weld arms (front only) 2 3-5-3                                                                                                                                                      .
:y                                              4-1-4-2.                              .             C-H/191,. cr-n/U1/1201                                                           MiMi?sdiiEnion at. coating incarphas
                                                                                                                                                                                                                            .                            .                      .              .                        ~
one large blister ou 4-3 " ."
4-3-4-4                                             c-11/191 cI-11/191/120L                                                                                                 . . .
     .                           .2
        ; . s. ; 5-4-6
        -                                                                                                  cz-11/191,.c:-II/191/I201                                                        No Defects.                      ..                                 :. .                .....                 .
s-                                                               .                                                                                                                                                                  .- * * -        .
                                                                                                                                                                                                                                                                                                   '~
No Defacts..
i                  .
4-1A-4-2A- --                                       cz-11/191 cz-n/191/1201                                                    .
     .,                       .                        4-3A-4-4A                                            cz-n/191,cI-n/191/I201                                                          h Def~ects :.                       ..                                          .
4a.
cz- n/191 cz- n/191/not                                                                                                       - -
              ,                                        4-5A-4-6A                                                                                                                            so Defects -                     , .
                                                                                                                                                                                                                                                                                                          .~
         .t. .                    .
3,                           .o
                                                                                                                                                                                                                                                                                         .~             ..
i    ..,; -                                                                                                                                                                                                                            .
i . . .
: .,i :                   ..
) ..                                                                                                                                                                                                                                            . ....
       . s. .                                                                                                  .                                                                                                                                       ..
     -.      :5, l         .
t
: 1.               *                                                                                 .
i                  ,
1
             .i
            .s-c. s .             s t                                                                              .
t,. . . ..
                                                                                                      = . . .. . ..
     .q ; . . .                                  .
e.: z . .                  ;  #..~ . g:-                                            ..                .
                                                                                       %..         -!. p   ,g      x.   .y.     ..
s          r.      ;g.     .
: a.       . r.
                                                       .5    7    .  :.   . u                                                             .,       ..
p..... . ..                                                                                                                      .. . .       .                                                                                                                         . . .,
                                                              .     ...s.                  r ... . .
                                                                                   . .. . . ..,....e.... . . . .
i...,      ;. ?a.                                                                                                                                                                                                                  .                                                                                .,
_...2-

l g ...i*      -y:~   _ : . c.         . ~: .        .       ,  . , .:.   - d: . _ ..      . . .       .i .9,fS..o ;         ' kQ1${.gf.3, ;,;;.;g&_;,
f             '
l
[                                                                                                                                                                   l i
4
:              TII-4201
 !i              06/22/84
 +                                                                                                                                                      _
Allegation No. 5 Procedure No. CCP-30A, Rev. 2, page 2 of 13, paragraph 1.3.1 allows the application of Carboline 305 over the primer Dimercoce 6 by Amaron. Has this system been DBA qualified?
Evaluation of Validity We assume the term " Carboline 305" used in the allegation refers to Phenoline 305 manufactured by Carboline.
A coating system of Carboline's Phenoline 305 over Amaron's Dimatcote 6 primer has.been specifically qualified for DBA.                                    (See Carbo 11ne Testing Project 01684, '
Final Report, attached).
f Safety Significance
's               None l
l            .
1 Generic Implications on Other Syst as or Contractors l
l Not Applicable
\.
    ~
: l.                                                                                           -
l l*                                                                                                                                                             .
    ~
                       ,  e    , , - - , ,        , -,r.       ,--, ,         - , -- -. .:.-                   . - , - - ~ . - .      - --      -.--          - - -

c---                                -
                                                                                                                                                                    ~             ~                                         '
    .'!: .                  ..-* +. @ :: b N.%.y Up                       ''
                                                                                        .     ' VT ' i W       %>T..a.a          5
                                                                                                                                           .-                   % :.;;                    , 5.h ,; ~ iL '          .Q. r.    ."3
                                                                                                                      . =         . .           -..
m a.;,,,,,::          ..                  .._ .: w -       . - a..:,;; a                   a . s__-               -
                                . T ~~~ G,y,t,                       ., . ~~ l -                         ' N. .
LAECRATONYTESTREFORT                                                       [
                                                            . . . - .,q                                                                          3.jq
                                                                                                                                                                                      ~ ..
    . , , ~ , .w-~
                        -(
                                                                                               ~
[                                                            h..
                                                                                                                                                         " August __11, 1978
  .Q Testing Project: 01684                                                                                                 -
FINAL REPORT                                                          -
                          .      SU3 JECT:                         10CA; Amercoat D-4/Phenolina 305 Finish and the Comanche Peak
* TSAR 10CA Curve                               -
           ..                     HETIRINCI:                        C--ark- Ps.tk Nuclear Station; Mr. Don Sutton; E=.                                                        Iaith 7411; Mr. Dan W. McBride; Testing Projeen 01651 PURPOSE:                          To dar==4"* the performaca of Ic Amercoat D-4/lc Phenolina.305 Tinish when exposed to the Comanche Peak Stamm Electric Station,
             .                                                      ISAR 10CA enzve and evaluated according to ANSI N101.2-1972, Section 4.5 as interpreted by Carbolina.
CONCIUSIN:                        After tha seven days of the C==a*h= Peak FSAR 10CA curva, tha followi=g chibit an acceptable performance:                                                                                   ,
                                                    ~                                                                                                                           *
                                              -                                 System                                                           Primer cure 1,2 le Amercoat.D-6                                                          17 days at 67-79'T (1S-26*C)
                                                ..                            ,1c Phanolina 305 Finish                                            and 53-88". 1.E.
3,4 Ic Amercoat.D-6                                                          17 days at 95-100*!' (35-38'C)
Ic Phenolina 305 F8 #*h                                          and.100' ,R.I.
                    -                                                                 e
:%              PROCEDURE:                        A)          Test Conoces                                        -
                .w.                               .
i;                                                                           33.za:             2" x 4" x 1/4" Car **ed ASTE A36 Staal Surface Prep: Grith12sted to SSPC-SP5-43
                                                  .-                             Abrasive Media: GTE f50 grit (Cleveland Metal Abrasives, I=c.)
: 3)          Sweems Tested-                                       Esteh Numbers                    ,
Drv Film Thickness 1,2 le Amercoat D-6                                                   1503310                           2.5 - 3.5 mils
                    .                                                             (cured in Cars Cabi=at*)                                  1503210 le Phanalina 305 F*-d*h-                               .730427E                             6.2 - 8.6 mils 6E3959E 9.2 -11.1 mils                         ,.
p                                 -
3,4 Ic Amercoat D-6                                                     1503310                         2.4 - 3.3 mils (cured in High E=4dity " 1503210 Drum **)
         ~
ic Phenolina 305 F4 e.h                   ~
730427H                         4.7
                                                                                                                                                                                        - 5.4 mils 6E3959E 7.3 - 8.0 ms.ls c._                                                           .
* Care Cabinet is at ambient smyersture but, has humidity c== trolled from 50". to 90*. R.R.                                                                             -                            .
                . ;*,                                                  **11sh Humidity Drum is at 100*? (38*C) and 100*,. R.E.
Fmm the Carboline Research & Development Laborstcry                                                                                      )
C,'(
                   /
wN-
                                                                                                                                       *h . I.3           ;                                    * ' **' k -'
        & %v- wm w gwT,ww.;;;,,,
                                   ..                       [_"**                  -
                                                                                                                       ,. ,e  w .cw}_                   n-M.--       , w       , , ,
r
        $5C.Wmi*="Y1*f"""A"*"fMR E carahoIIrte-)4.t                 E, Me M.4~@ b M M db

a c.: .            .e -        u.. _ m.                    a -                                       ..       :    s. ::.     ~         ' -                '                v. ,.
_a            -
::        ~a r - _. . -                                          .       .
                                                                                                                    .      .          . .e.                 .        . . . . . ..
3......,.__....-                                                                                   -            .                                              -
                                                              .. - . r g - p .,- w .- .'
i . .-          -- .
                                                                                                                                           .O
                                                                                                                                           .x                        LA .            RATORY i a:ST. REEP, ORT
                                                                                                                                                .. w
                                                                                                                                                                                    '3
                                                           ~ ; . .. .                                                                                                                         i
                                                                                                                                            ~
         ; - $. *L.*.a t..
f
                                                                                                        .u 4s . W ^       1                                                ..
                                                                                                                                                                                            .a                                                                       ;
o r
                                                                                                                                                                                                                             .               3 August 11,1978/Page 2
.i (.                         Testing Project: 01684                                                                     '
* FINAL REPORT PROCEDURE:                      ('*-4 -=d )             .
C.                         Cure Schedule 1,1 Amercoat D-6: 17 days at 67-79*! (19-26*C) and 53-88%
Relative m =fdi.ty.                                                                                                                                     l Phenoline 305 Finish: 18 days at 71-80*T (22-27'C) and 55-70%. Relative un-4d4*y.
l
                                                                                  '3,4 Amercoat D-6:                                     17 days at 9' 5-100*F (35-38*C) and 100%
Relative haid4 ty.                                                                                        ..
Phenoline 305 Finish:. 18 days at 71-80*F (22-27'C) and 55-70% Relative Hinsidity.                           ,
D.                        Ernosure                                                                                                                            ,
Texas Utilities Generating Company,                                           '*~--@= Peak Steam Electric Station, FSAR. Figures 6.2.1-1 and 6.2.1-2.
: 1.        Time / Temperature / Pressure Profile
                                                                                                                                .m.
                .                                   Time                                                                Tennerature-                           Pressure                                     Sorav Condition U                                                                                                                                                 44 psia 1
Initial to 10 seconds                                                                   240*T (ll5'C) .                                                                            Static 10 seenods to 15 mins.                                                                  270*F.(132*C)                          58 psia                                             Dynamic 15 mins. to 1 hour o                      15 mins.                                                                   215*F (102*C)                          34 psia                                            Dynamic
              .                 I hour 15 mins. to                                                                                  .
7 days                                                                      215'T-130*F                          34-10 psia
* Dynamic .
(102*C-51*C)
(Note: 'Diis is the theoretical enzve supplied by Comanche Peak. It was followed as closely as possible with the LOCA apparatus available at
             ..                                  Carboline Company. Please refer to the recorder chart (L115-129) for                                                                                                                                   .
exact conditions of 10CA profile.)
             ..                                   .                                                            2.        Spray Solution
          .1                                                                                               .                 .
E230 3 (2000 pga as 3eron) in deioni=ed water. '
pH = 8.5 - 10.0 (NaOH added to adjust pH).
GRADIpGPROCEDURE:                                                                                                                                                   ,
                                               'Ihe tast coupons were avaluated for perfor=ance in the following areas:-
                                 ~         -                                                                               1) . Ifaterial flaking off                                .
                                                                . ..                                          . , . ,. 2) _Dah=4a= tion between coats and/or peeling                                                                                            '
[d., - (-                                 ' E 5'l: hrem the Carioline"ResearcN E Development Laboratory                                                                                                                         j               .
            ..             ...                                                                                                                                                                                                                                  b Q&               w      Q~renwMG s 'M }'1" Mesi ~ .2!=%em.gT'N                                                               _sl_
                                                                                                                                                              ~
3 de=           h    e .# a w b ==3.                       . '-"*'doe.
                                                                                                                                                                                                              ~- ~ ' " Gl                            *:
        -    ""W he h doish==s             T                                          hed se are. d i
                                                                                                                                          ]~~_] j ]-7           aw7 ^ w_ g M.$
3
                                                                                                                                                                                                   -::; M CRE*t3Cilrte~ ' ann' E ls.+.,ta-+                                             a. -@.w, ;w                                   -. r .;.-L   m yl&v4*8* 3=                          M 8.                 M y-**3=o33=d z :. .. .a .                                                                                        .   ._f.=._ _= Zw '              :
c= -i=^           _:g''- ;f.. : ,.
i .t.
an.             w .-                 .                         - ; _ , _ - y.. _         , 3 _ _, . . , ; y                 _ . .          ,_        _;            ,                                            _

                                                                                                                                                      .. w
           ..                  ..        ~                                                                                                                                        .
n.M .,g.% x.s;.L
                                                        >v.au . s._ w                                        rwa .%                                 ''-                r.        - -~. 6 : ' a:a
.._                                 a .. .,                      , - - .                                                                                                   _               - - -
_=.-                                              -                                                            -
.c            _,                                                                              ._.                         _
:-- .- ', ';_ c. m, #. p.9,,..-....     . . -
                                                         .. , . , . .               . .,+. ..,.< ....-   . .
                                                                                                                      - a.
b LABCRATORY TEST. RE!:                                          ORT -
. .. r
                          - w . : :. :.              . .. = :    .       h.,-           .Q.
D .m                          .        ..
                                                                                                                                                 -         .,/
3
,(                   "    r-                           .-
                                                                                                                                                      -August.n,1978/Page 3 Testing Project: 01684.
jI''$
                     . n m - Car                                                                                                          .
i GRADING PRCCIDt2E:                                 (Ca=edanad)                                                                                                             !
3)'          Blistaring of the. topcoat-
: 4)           Chalking of the c.cating                                                     -
: 5)           Izcassive cracking Grading proceduras specified 2n Report N101.2 - 1972 of the American National Standards Instirnta-Protective coatings for Light Latar Nucisar
                      .                   Ranctor cane =4- Facilities:
4.5 Methods of T*==4**"r and Evaluating the Ermosed Test Soecimer.s
 !                                                    Iha dynamic and/or static elevated.tamperature pressure and irradiation test panels shan be evaluated within 2 hours and again after 2 weeks after removal from the test. chamber for the following surface defacts: "t h g                                                                      ,
d=1==4*= tion and/or peeling, blistering, and chalking. Defects listed.in Subsections 4.5.1 through 4.5.4 shan be dealt with as fonovr:
4 5.1 naking. ASU D772,. Evaluating Degree of Resis ance to naking (Salin-) ofh=dar Paints, Part 21, American Sociatv for Testing and Mae=y E=,.741 d-inh 4=,Pz. 19103. Tlaking shan not be pasmitted.
4.5.2 De1==4 = tion and/or Peeline. Delamisation and/or peeling shan
* not be- pe=mitted.
: 7.      .'s             .
   ;          V                              4.5.3 311 staring. Elistaring shall be limitad to a few, i.ntact blistars,
{
Siza No. 4, ASI!1 D714, Standard Method of Ivaluating Degree of 311 staring of Paints, Part 21, American Society for Testing and Estarials, P641=d=1*h*=,
Pa.- 19103. The unnber and the sina of blistars shan be recorded.
4.5.4 Chalking. AST21 D659, Standard Mathed of Evaluating Degree of Basistanca t.: '" - N " of Irterior Paints, Part 21, American Society for Testing and Maead =1 * , Philadelphia, Pa. 19103. Heavy d = Nag shan not be pos:nittad.
                                                                                                      ~
Any other changes in coating propersias which are cot also associated with
                                            .,tha separation, or the release, of coating from the substrata shan not be a causa for rejection.                                                                            .
     . ,.f
                                          .                                                                     e  .
X
                                                 ,:         . , '- From the Carboline Research 82 Daveicpment Laboratory j
                                                                                                                                                               ~
                                                                                                                                  ;. w w e                                                                  -
L n %p+ h wwgw.a-wwmu_ = d i & .t
          '~                -
r                                                                                     _                        i==.d.4        M.--   ,  m..-                           R.
                                                                                      ^
                                                                                                 ^^
                                                                                                                        ^
                                                                                                                                       .                                    ?
                                                                                                                  , gg& _                                                                            m;;
_m m *- a n - . ; __ 1 - - "-_,-m==-ww
        -               - m -- e                               _       _,.x       _ .__ a w_                  .
                                                                                                                                                        . ,. ~ t F '', e'if ,, Q r ,'m-w m

                                                                                                                                                                              ''~ ::< mr
      . -3.b            -.,. W .. e n s- 9.:9., +. +                    .m..      .~ -       ! o. i r._ , .        ,a-        m                       -
                                                                                                                                                                                                      ', .          -k.
3 yhr . .-~ g ggg 4 ,. *             ,,          ,
                                                    ,     . /p.
g , g g g g7
 '.,.,.                    *          -                   ~
                                                                      . ,q                                                 G)                ,q D
                                                                         ~
                                                                                                            ='
                  'f                                                                                                    r     .
August *11,1978/Page 4 Tasting Project: 01684
  .c-=-Qn m m car                                                                               .
ANSI N101.2-1972 Critaria                                           ,
(As interpreted by Carboli=a)
M=v4 - = Desree of Failure Allevable
                                                                                                                                                 ~
Flaking ASti D772                                       ,,
10 (Nona) -
D=1 -4a= tion.or Peeling                                         **                                                                         Nous
* Blistering AS2! D714-56                                        311 star Size                                                   Elister Densitv' 92                                                               Sons
                       *NCE: A blistar is not                                                      #4                                                              Yew intact when. it has resultad                                               #6 Medium in coating being separated                                                 #8                                                                Medium-Densa from the test coupon.                                                                                                                                         ,                                 5 1'                                                                                                                                                                   8 *(I.ight) r
                        ^ = N ai ASE D659 l
NCE:
* Haking, blistering and chalking are all evaluated according to AS2 Standards, with a racing of 10 i=dicating that no failure was obsa=Ted in the spe*4*4 c 3=sding araa.
C mM       ,,                                                                                   .
i O
e                                                                                          *e e
s .
y e
e e
       .m.                                                                                                 ~~
p*g*                                                                   .
                                                                                =
    -                                                  From the Carboline Research & development i.aboratory                                                                                      j
{i(                                                                                                                                                                                                    }
* 9.6 2e * . * $ -q E                                               .fJ"E .&F.,   ..** *.
O
                                                                                                                                                                                                           *d-O I
                                                                                                                                                                                  . I.an;   .
M     '
bS           .**      .        fr*[                        %                                                               **O=[      F.-       ..
                             - Tha * =% rums.h.d 1. w L -                                 -- _ m d ben .i~
                                                                                                                          -- '6M   -
                                                                                                                                                        -.**W1                                               -
                              "-''**""*"r'**"*'*d-                                                                                                 $$jgliSNit
                                               ^= V*3R-         '-- ~
5.A-NA'aM_T.m s .         u
                                                                                                               , . L "_' TlC &*Kg.* ~_Q'_'RQh*
_          ---w       [cas-tmolirse .x*                  ,S,; }$

6.-
m
                                                                       "*lg .'                                              f
: h. ,h, . .h. .-- .
Ol6s4 '
                                                                                *               -                               p].                                                                       Au8=t II .            gl'dne.'''    / i. ,, I.1d'. k.
y'-
                            ;8 ( f' ci.                                                                     RESils ;J
:T-st' t-                    .
FINAL. REl%n                                                                                                                                                                                                                                                    d ll   i
                                                                                                                                                                                                                                                * ,,
* I. i                .
If4NWit                    5 O'ther
                                                                                                                                                                                                                                                ' ' ' '. ' ' l .,             [
Dry                          -    Delsmins ,                                                                                                  ,
l'criarp3p'c , i yJ hj[ysselIdentification tion or                                                                            Performance Evalent{ag * ';
I       h fl                   . and                                   Fi)m                                 Peeling                     Elisterihg                         Chalking           Characteristics
   ,l
* Casting Syslam.
T)ickness        Fisking
                                                                                                                  *                                              '                                                                            j.. , j, ;                      jE
[,   ''#
None                  10
                                                                                                                                                                                                          ----                       Acceptalqc                       ,
p.
    !           Ih.,,l) Amercoat D-6                                         3.5 mils           10       .
None
                                                                                                                                                                                              .                                             ,* .,*.                           is l
(Pr(mer Cure 53-881 R.li.
1 i
la Phenoline 305 Finish                           6.5 mils                                                                                                                                                                                         %(. .
h k g 4.,.                    ',                       .       10.0 mils                                                                                                                                                          '
{3 I
10                   ----                      Acce,)hle:.
kBle,AmercoatD-6                                            3.0 mils            10                   None                           #4 Few Intact                                                      i                                .                     J,
       ! L           CPrimercure53-88%R.II.)
13 Phenoline 305 Finish                            6.2 mils
                                                                                                                                                                                                                                          -' .').
: l. '                  9 g
9.2 mils                                                                                                                                                                                          s l
          '[           y, .
                                                                                                                                                                                                           - --                       Acceptable l
7.i 2.8 mits            10                    None              .               l Nong                       10 l $Ak ic 'Amercoat D-6
                                                                                                                                                                                                                                                         ,.                        1' t,                                                                                                                                            7 f(Primer cure 53-881 R.N.)7.7 mits b                         Ic Phenoline 305 Finish
* l' 10.5 mils d i                         i                                                                                                                                                                                                                                      -l 3.-
Acceptable
:Il
              ^               '
None                             #4 Few Intact                10 2.5 mits                                                 -
10
  ]b;2R'f14 Amercoat D-6                                   .               ~                                                                                                              .
i a
J qj(,1cPhenoline305 Finish; F
[I 8.6 Primer 11.1 mils alls      cure 53-881 R.ll.)
                                                                                                                                    *                                                                                                                    !       j' ]
p y <gg.g.
Accer*phic :j N                                                                                                                                                                                                             ---
t '; ,
None                                   None                   10
 ,                3A                                                         2.4 mits             10 V'                   u4           ,
                                                                                                                                                                                                                                                                               ?-
h.hleAmercostD-6.(Primer                                         5.4 mils    cure.1001 R.ll.)                                                                                                                               :
Ic rhenoline 305 Finish                                                                                                                                                                                                       .                      T 7.8 mits                                                                                                                                                      t
                                                                                                                                                                                                                                                                               ;p
[,: - g ..                                                                                                                                                                                                             Acceptahir '
None                                   None                  10 3.3 mils            10-
              /3sileAmercostD-6                        .
                                                                                                                                                                                                                                                      *?          !.
 -l (Primercure100%H.li.)                                  4.7 mils a
Ic Plienoline 305 Finish                                                                                                                                                                                                                              '
8A"                                                                                        .
i
        !             h{id                                                                             .
                                                                                                                                                                                                              ----                     Acceptabic                 !
[.
    /!                                                                                            to                                                                                   10
* 1,k          *$A'I Ic Amercost D-6                                        2.6 mils                                     None                                  None  *
                                                                                                                                                                                                                                                  ,                                J.
e [ Primer cure 1001 R.ll.)
s 4.7 mils
* y?.
Ic Phenoline 305 Finir.h                                                                                                                              ,"               *       *                                    .
L                            p                .
7.3 mils                                                                                                                                                                  ,
j l
None                                  No'ne lo                     ----
Accert4ble                               )r'.
2.5 mils             10
                  '$(1leAmercoatD-6 p     Primer cure 100% R.ll.)
4.9 mils
                                                                                                                                                            -      -                                          l                           .
l
                                                                                                                                                                                                                                                                  !yQ-J,Ic Phenoline 305 Finish                                                                                                                                                                                                           ,e
                                                                              ).4 miTs                                                                                                                                -
k.
4;
                                                                                                                                                                                                                                                                    .          II0 b,.

                          ,.f
                                           . - . o    . . - . . . . . . . _ . .. . .
                                                                                                                                                                                                                                                                       ,',              I,',          ,
g.
  /
I
                          .[.
                          '4 E'!                   '
                                                                                  ' Q..                               -
                                                                                                                                              , (,, )                                                     ,
Amst 11, .p-. gen
* 2.is I     y'i. '.. [/.
[,Tn tcg Pro]ect: 01684 FlNAL RF.PONT
                                                                                     .                                                RESilLT8 '
                                                                                                                                                                                                                                                                         * *, f                            g jm;g,.::
                                                                                                                                                                                                                                                                       *} '' f-                             f n
P n                                                                                              Ifry                                Dalamina-                           -       -                                    Other                                               .                     .
8.*.g'P;nelIdentifIcation                                                            .                                                                     '*                                                                                         Ppriormanc                                       i.,i .
File                                  Lion er *                                     .
Performance and                       ..
Pqeling                   Blistering                Chalking              Characteristics                              Evaluatjepl                                      '/ :
fyiy.. '.[-                      Coating System                                        Thickness                 Flaking 10              None                    #4F to #8 tin             is (Light)
* Panel suspended in tlic vapor '                                                             a.       I OAdciptablePerformance                                                                                                                                                                            -         phase                                                                      .
l Allql,N101.241972, Section 4.5,                                                                                                                                                                                                                                               ,(
iAs ptppreted by Catholine
                                                                                                                                                                                                                                                                              ,[ - .
f.r.
                                                                                                                                                                                                                                                                   ^)
                                                                                                                                                                                                                                                                                       !1:
y1 1;
                                                                                                                                    ' }}&& .. WERndf,;f.
g                       '     '
h
                                                                 ~                                                                                                                                                                                                                                      '
br [.
f;
                                                 ..                                                                                                                                                                                                                                              ~
                                                                                                                                            .llichael..p. Tellor                                 . . ; ,. John F. ifontle                       .-                        ;                         k JohnkI. adage,Jr..                                                                                                                                                                                               8l
{
                                                                                                                                ..                                                                            Vice President                                                           ?
Sopervisar
                                                                                                                                                                                                                                                                    ,                                           r
   '3             I             l 7                              Developmental Chemist.                                                                                                                                                                           '
Testing Department                               .~...-                  He'acarcli & Deirclopacnt                                      Research & Devctorment                                                   $1                       ,
jj l                         ![fl
                                                                                                                                                                                                                                                                                     ,)i    ,
i
         .XC;
                                    'h         .
fil/CJW/IM41/PDI./ilDT 8
                                                                                                                                                                                                                                                                         ,.j j     ,!-
{;l, w.
L                         f.
(.'.) )! f,.
(.                                 [. .            .
                                                                                                                                                                                                                                                              .                   .n   4, l            .
                                                                                                                                                                                                                                                                    'd f                                                           -                                                                                       .
9
: i.                                                                                                                                                                                                                                            .;                           .
                                                                                                                                  .       .                      i t,
L;                                                                                     *                                                         <                                                                                                  -
r.
                                                                                                                                                                                                      -                                                                                                        i h ,3 2
Ji                                                                                                                                            .
 .i
                                                                                                                                       '                                                                                                                                     s          .         .
{-                    .'
4 fj ./-                                                                                                                             -                                                                                                                  ..                   >
g
[                                                                                                                                                                                                                                                                                 -'
dh                          (
                                                                                                                                                                                                                                                  .                                                          V;.
s.
n':             .
(y.i-s                                                                                                                                                                                                                                                             l                    '
kllf{:hh:.
: s. 2 . : - *-
                                                                                                                                                                                                                                                                                                              +
['

                                                                                  ..:4?i_. w ;; Q.,4;,,O s;,g m       w , .;;r -     b :,  _~     -c.      a     ~:          ;&.
3
* l       .
t.
i.
TXX-4201-
               ^
06/22/84 I
Allegation No. 6 Procedure No. CCP-40 Rev. 5, page 5 of 13, paragraph 4.1.1.3 states: " Repair of embedded foreign objects such as nails, rebar chairs, bolts, wood or' plastic shall be repaired per the following guidelines before applicatien of Nutsch 115 surfacer." Have these systems been DBA qualified?
Evaluation of Validity The application of Nutec 11S over repaired embedded objects has not been DBA qualified, but this fact is without safety significance. The surface area of foreign objects. embedded in concrete is negligible in proportion to the total area of any given concrete surface receiving coatings.
m 4
In any event there is substantial evidence that objects such as nails, rebar chairs, bolts, wood or plastic embedded in concrete does'not affect the adhesion characteristics of Nutec 11S.                                            .
: 1. Observations made in Imperial's labs over the years while preparing concrete coupons for DBA teses. The concrete blocks were formed in plywood, lattice like forms which occasionally transferred wood particles and splinters to the concrete surface. No failures were ever             :
attributed to the wood in the concrete. Refer to attached imperial {{letter dated|date=March 8, 1984|text=letter dated March 8,1984}}, 

==Subject:==
Wood Splinters in Concrete.
: 2. Qualitative tests conducted by Imperial. These tests found that Nutec 11S adhered to both rebar chairs (rubber and polyethylene). Refer to attached Imperial's {{letter dated|date=March 8, 1984|text=letter dated March 8, 1984}}, 

==Subject:==
Rebar Chairs.
: 3. E1cometer Adhesion tests performed at Comanche Peak. Results averaged well above the required minimum of 200 psi. Refer to attached Interoffice Memo dated June 19, 1978, 

==Subject:==
Adhesion Test of Embedded Wood in Concrete. It is noteworthy that the mode of failure in five of the six adhesion dollies tested was concrete failure.

t ., ~~ u ., .      -                                                         ,
'/g., . e. .. c, ; . _ , ,,    ya        m.
:-M., ev' ..        +
q.g     a;: -      _, ;cm,......,.              , u 2 .,wa s;,.ub_.aa
: 4.          DBA data from Imperial.           (Report No. 462-1-81 attached).
f                                               The purpose of the test was to evaluate the feasibility of applying                                          '
Nutec 11S surfacer to steel embedded in concrete (i.e., Richmond inserts, steel embeds). These tests demonstrate adequate coating i                                                performance under DBA conditions.
I t
I I
l-                            Safety Significance j -.                         None l
l Generic Implications on Other Systems or Contractors l
l                             Not applicable i
l r
l l
l h
l i               .
I lo e
4>
I t
s.

            , . u ..:q . .~, . .r. '9f.,~ _>;;,.;A ''* a :c. . . ._ ,, . :- s + , i; w; 2._    - , : .; : ~sy
                                                                                                                                                  ,                   :s __; .. ,
                                                                                                        .-           . - - -                             ~- . . . - . -
_.                          . ~ . . ,                          .. .
                .            .e
  ': a *
       . ?.
f
  ! .'                                                                                                       -                    *a s,. ,
  ) O-;.           V 3cs M077 New Om, Lousana 70189 U S.A $04 :54 1433 ggg ' PROFESSIONAL COATINGS
                                                                                                             .               p March 08, 1984 Mr. Jerry Firtal c/o Tom Kelly - Civil Engineering Comanche Peak Nuclear Station P.O. Box 1002 Glen Rose. Texas 76043                                               ,

==SUBJECT:==
Wood Splinters in Concrete

==Dear Jerry:==

Attached is a copy of my letter of April 19, 1978 dealing with wood " splinters"
!.                          embedded in concrete. I still concur with the opinion expressed in th'a 1978 letter based on the following:
: 1. Good sound painting practices. The surface preparation that was recommended is sufficient to remove loose particles. All that remains is intact, embedded
{g              meterial.
: 2. Visual inspection of embeddeli vood in concrete surfaces at Comanche Peak be-fore and after surface preparation.
: 3. The small amount of surface area involved. The embedded material in question is not large pieces of wood, rather small hair-like splinters. The amount of wood in contact with the Nutec 11S surfacer is =4n4=1 compared with the con-crate surrounding it.
4      Observations made in.che lab over the years while preparing concrete coupons
                                - for DBA tests. Imperial's concrete blocks were formed in plywood, lattice-like forms which occasionally transferred wood particles and splinters to the concrete surface. No failures were ever attributed to wood in the concrete.
Jerry, if you have any questions please don't hesitate to call me.
Sincerely,
     -                       Jerry.irnold cr:: Jurry Firtal (Ebasco-NY)
Project Files
                '~
s-              Readinc Files d                                                                                                                                                             -
g

      .. . i ?.r.: . . ' .
                . - .           . :. .. c .. . xi. v. .. .
e s.- _'O^  "  ' '
                                                                           '<'..e-                                  ~ ~ "
                                                                                          . _ _ ' _ . ' _M-. _ " . _ _ . . . .
NS" k
                                                                                                   %s
      . W so=~ 290n h Oneens. Lousana 70189 U.S A. 504 2541433               ggg{gg I PflCFESSIONAL COATINGS
                                                                                             ~
                                                                                                                                   'I March 08, 1984 Mr. Jerry Firtel c/o Tom Kelly - Civil Engineering Comanche Peak Nuclear Station P.O. Box 1002                                                                 -
Glen Rose, Texas 76043

==SUBJECT:==
Rebar Chairs

==Dear Jerry:==

       ~
My recowenandation for handling rebar chairs in the past has been to use a mechanical tool such as a 3-M Roto Peen to cut the protruding tips flush with the concret sur-face while at the same time imparting a profile to insure adharance of the Nutec 115.
r.f.Several years ago I conducted some qualitative tests on rebar chairs for another job i.
* cita. I applied 11S to two types of rebar e hairs; rubber and polyethylene. I found p                      that the Nucec 113 adhered better to the rubber tips and Nutec 11S would adhere to polyethylene chairs with a rough profile. Because of the gecmetry of the rebar chairs E1cometer Adhesion tests are not feasible. I believe that jobsite adhesion tests woul'd substantiate my findings.            *                                                  '
Sincerely, y                                                                     ,
:s.         .                                              .
p                      ..
l J;rry Arnold cc: Jerry Firtel (Ebasco-NY) l Project Files Reading Files
?                                                                                       .
s
..t e
N
            .e%
4
\ '
3                                                                               ._

l w...                                                                               ..
: c.             . .               .
.m.na..,    . . cr>                           ..
                     % .pr.g;..o g, .yg.w,9gi.g. .,c ;.;
                                                                                             .. g. .,. , cgy g .                 ,.4     ,.. g, g.g g.g g . . .g.,g , ,, , . g M** . .                        . ~
                                                                                         ..T.:2_._              - . .:-~ .
:Y=.           =.~; :~r.--t ;. r- .; : - .':=. :- == :
                                 .e
                                                                                                           '                                                  e          35-1195                            .
      -l       *7                   v                                                                                                                     A 4-                                                                                           h                                                                   6/ 19/ 78
                         'Rewrth1oct,lnc..                                                       (W                          -                         'C                           .
W. ?,
* t
        .T
        '                                                          -                                         INTEPDFFICE MEN 0 c      -
                                                                                                                                                                                                      )             ,
;                                                 IM-14473 OATE: June 19,1978..
i TU: Pat Clarke                                                             .
1 f                                                 FROM:                      H. D. Hash, Jr.
k                                                 

==SUBJECT:==
CPSES. Job Mo. 35-1195 Adiesion Test of hiedded Wood in Concrets                                                                   .
Y                                             .
i                                                             As askedded wcod parcicles in concreta has become an increasing
* problem in surfaca prwaration of concreta substrata, the following f                                                 adhesics tasts ware pa.-f=r:md in Rccm !197 E1. 810' Upper Auxiliary.
s
                                                                                           ~
!                                                              Testing Mutac fit, P.sactic #1201 over existing wood particles:
6 s.
1 j                                                              Tert f1
: a.      900 PSI                  Concreta Failure f;                                                                                 b.       7EG P$r                 Concreta Fs11ure Concreta Failure                 Test #1 Avg PSI-816 PSI i
: c.       8Q0 PSI e
]-
a Test !Z Coatirig Failure
                                                                                 . a.       650 PSI
* J                                          .            ,
Concreta Failure l.
: b. '800 PSI i                                                                                   c. 600 PSI                       concruta Failure
)                                                                                      .
Test #2 Avg. PSI- 683 PSI The overall test average of this room is 749 PSI, which exceeds the values reconnanded by Imperial Coatings VSR-7494, April 19,1978. This J.
i should substantiata Imperial's opinion that embedded splinters and wood 3                                                   fuzz which cannot be removed by water blasting, will not be detrimental a                                                                                                                                                                      -
j                      -                            to the performanca of the concreta coating systam.
H. Q. Hasti, Jr.                       /
/,                                  .
Level III Coating Inspector L4
                     .                               cc:          U. D.' Douglas
                                                               -Or5uttorr g . g ,, g,,,
r 4               m
* a l ' O.I                        . .                           .                  .
ij              .
                         ........                       ......                 .m_                                       .
L.

      -j.4... ; b3 .. -hqi .% x , . .> ;; ; 46:y .%.:.. .; . _ + > . 2, u. . . , y ~ . x.,.
                                                                                                                           .      ..     ~ .ns. . . , la
                       ,                                                 o
  .;         .      y.       .
           ,                      g
                         '                                      ' g,                                                                                        _
4    .
g                                                                                                     ;-
E                                  TECHNICAL REPORT l
I:                                                                                           NUMBER l                                                                                         462-1-81
    .E                         .          .       ,
                                                          , ,        . .   . . .                TITLE
'-                                                                                   . . REVISION l '-  '
DESIGN BASIS ACCIDENT TEST RESULTS -NUTEC llS OVER
!'                                             CLEAN-N-STRIP AND ABRASIVE BLASTED STEEL FOR l                 .
GENERAL USE CUSTOMER
                                 . Submitted by: GERALD ARNOLD
* M ROBERT R. TAYLOR                                         db
[.                                  Approved:
',                                  Date:                       JANUARY 22, 1982 i
SOU1'HERN IMPERIAL COATINGS CORPORATION, INC.
                                                            ?. O. Box 29077,
* New Orleans, Lomusna 70139                               ,
t Phone: (504) 254 1433 f4-0                                                                                                -==.            w        . . c . .,
s
                                                          ..                m ia.. r -,. w.= w. .w ti. ia
                                                                                              .-==a            inna=mn.in,                 ,.       r 3
>                                            rm.              -n                                                                     . Hg.a   og .g.r.t.
)'
pg W.        a.st. se. Is sht? In C.na.CTt
                                                 . nn . . _ .            c W fa ifs tp . T.hc
                                                                                 .aeria   m e laforfa.f a 86 a.0 6ae.ac.g r.a. = en wi.
4i L-                                                                 .

  ., y".: d , .,;.
yv.       n . _, :. a . p.s.. .      x,.....
                                                                       . . . g.,s 4 a g . g :        , .          ,.                  , . . . . ,. . .              . ,e,       ....,,g.,,.
                                                                                            - ~ ~ ~ - " ~ - - - - ~ - - - - -                                             - - - -        - - -
_    .     :Gr.=a.                ..
o
     '? . e            .
      .h, .
      ,g               TRv462-81                    ,
j            Page 1.
1'I                    SCCPE:     The purposs of this test was to evaluate the feasibility of applying j,                                Nutec #115 surfacer to steel imbedded in cencrete (i.e. Richmond, inserts,                                                                               ;
p N.                                                                                                                                                                                        '
1'.-                              Ste9l Imbeds) in Service Level I areas of nuclear power plants.
5!                   SCOMY: Design Basis Accident test results frcm Oak Ridge National Laborateries indicate icss of adhesica en 115 coated specimens and #2 few blisters en j*
!                                 115/1201 coated specimens which had previcusly,been cleaned to bright
  !                               metal with a 3M Clean-n-Strip cup wheel.
s .
l                               On the other hand no defects were observed on the 115 surfacer ever ji                              abrasive blasted steel. Mixed results were cbtained en 11S/1201 specimens
  ; ;                             which had been abrasive blasted. Two of four faces locked excellents
  ;, .                            wheraas the two remaining faces exhibited some blistering.
P
  $ .;                            Of the eight 11S/ abrasive blasted steel interfaces, five exhibited no defects
  ?.                              and one contained very few #6 blisters (75% passing) . Of the two faces which Oak Ridge National Laboratcries reported as #2M, one appears marginal.
a 6*
* PROCIOURES:         Eight 2" ;c 4,"               x r" carben steel panels were prepared for coating:
3 4                                                                                                                                                              .
j !!
: a. Four were cleaned to bright metal with a 3M Clean-n-Strip cup wbeel.
s h                                      ~B.        Four were abrasive blasted per SS?C-SP-10, near white blast, with a working mix of G-80, G-50, G-40 steel grit to achieve 1         -
                                                            . a surface profile of 2.0 mils.
R Mutec #11S was applied to all eight panels over a two day paried (cne j                                face of each panel a day). Natec 1201 was then applied to two Clean-n-Strip q;                                panels and two blasted panels. Details of the application and curing are                                                                                        .
'i .
                         -        outlined en the attached panal preparation sheets.-                                                    .
l*
x:                                The coated panels were then submitted to Oak', Ridge National Laboratories for Cesign Basis Accident testin' ,g with maxi ==m 365= F. ,and 70 psig parameters.
l4                                                                                                              ,jg                    .
e-                 :.
:t                                                                                                           .
: a.                 . r.                              .
          -                       The tested panels were evaluated by CRN:'.;persenneljimme'diately upcn removal
?'                                 frem the autoclave and reinspected by I=perial following shipment of the panels back to New Criaans.
l O
Ih        .
a         e ii
* s'        ,
2 *
] @g.                                                                                                                                                                                        .,
1
:1 ;
1 if
!j 4                                                                     .                       . - - . -             - _ _ _ _ . .             . - - _ _ _ _ _
: f. v.~.c. . . . ..     . . . , ,  r. , f ; .; y , .. .  ,.m..>.,..   ..s..: , u.f  _ . 3. g ;, , . w ),t y, ..n : ,j . m._ .
        ..~-
     ,     s.           .
f *h.',                  .       .
 ! R*
      ' 4}
* 4.;
k.i                     CONCLUSIONS:
        ?                                                                                        _
  ;-                                          Based on the test results, application of Nutec                                     ,
  ;;.                                          115 is not recommended (for surfaces greater than e ~,
two square inches) over clean-n'-strip prepared j                                 steel in containment areas which would be exposed to the temperature and pressure conditions observed in this test.
Application of Nutec llS is reccmmended for over-lap on steel imbeds (maximum 2 inches overlap) and over imbedded steel objects (up to six square inches),
   '                                         which have been abrasive blasted or prepared with power tools which impart a surface profile (i.e.,
roto peen).
Of the eight abrasive blasted faces coated with
  -.                                         Nutec llS, five exhibited no defects and one contained only very few #6 size blisters. Oak Ridge also
    >                                        reported one face of panel 7829 (rear) as having
                                             #2 medium blisters. Imperial evaluated the panels thoroughly and believes that ORNL mistakenly eval-uated the same face (front side) twice. Imperial
* has reevaluated the rear of panel 7829 to only few
__,                           #4 blisters.         The front side of panel 7829 was border-(;,                           line.
i.
i,,                         .      r
                                           -Therefore, of the eight abrasive blasted faces tested, Imperial finds that seven comply with the ANSI N101.2 acceptance criteria (no larger than #4 few blisters) and the eight face is borderline.                  This amounts to an 87.5% success rate.
         ~
NOTE: Technical reports #353-80 and #413-80 relate E1cometer l:^ '                                      adhesion test data of Nutec 11S over abrasive blasted and power tool cleaned steel surfaces. These reports are reccmmended for review, especially for Service Level II and Balance of Plant service, when DBA testing is not required, that is, where the coating system will not be subjected to Loss of Coolant Accident conditions.
lI li l!             ** N
     ;      i 2$                                                                                                                   "I j
!j~, .
I
'(
g                                                 .
a

9 p .- . * ~ r . S s                                                     o                                                *                    '*}        .
                -                                                           * *- s                                                     '#
a
                                      .        .'- 4   #'  "B   93  .
O 4      &
                                                                                                  .        e p
                                                                                                                             --      -        - - :. *.,~ w n. wvr..ya. s..n is.c, ;gg,;g,,. _,3-.
88** hw-ed a e. g     g TT** **
a.
                                                                                                                           -     - __-g4 g, q e       e g
J . . ...                               .                                                  *
                         $#$                 -,S                   ~ ,
s o
: y.    -
           .:t. ' -
4
           . eOM                                                                                                                                                                                                                              *
           *d.$
f*.*o*
           *s'.'a                                                                      .
        '*s
* Is../.                                                                                                                                                                                                                               =
     -{                                                                                                                                                                                                                                 f e
O S
o S.
, .*                                                                               e l: .,                                                                                                                                                                       .
                   >e 4              9 e
j e!
1.,
* 3
, j ,.
t . .
      - ye e
'     * *          >                                                                                                     P N PREPARATION SHEETS                                     ,
5 *
* e L-p..
s 9
9 O
                   .O v3,                *                                                                                                                                                                                                           *
  .1'                e                                                                                                                                      .
9
* Q                g -
4        .4
* e e
8 e
6 e
. .:. g               - m. .                                  -                      .
: l.                 ...
l ig...e                                                              -                                 ..       ....                                     .
\v,::,
O
!                                                                                                                                                                                                     s I
  . - .#g e*
          *i         .O
                 -?
;* J                                                                                                                                                       6 i- .                                                 8 1+        1          ,
p.;                                     e e,
s'
: c. .                                                                                                                                                                          g d
t i l                                   .
i e A
                                                                                                                                                                            .n  ..,...
                                                                                                                                                       ?. '*
           -                                                                                                                                                                             ~e so e*e 1,                                                                                                                                *e e     f.               . J.-
M'             4 i                                                                                                             e 9
l l
M t.j                   4
  .y                 e
          .e g<
e 4           ,                                                                                                                                                O I
e
- =t                   e
        .=
l           e        4 O
            ,I         e O
,
* g
           .t
  . 1. .. a.,,,
g
                       'e 3-                                            #
                                                                                                                                                                                                                                           -g y
r I-          h'         g e
l 4.
k .. .
  ' f d tg . .A.
( "; .                                                                                                                                                                                                                              .
t.=
I

  .;i. * :.;;;.'. '; {. ~ +;-Q1           :S      <       . v C ',l  'S% S i ' > ' ' ' -~ -     *
                                                                                                            % '* " **" ' ' ' ' MI"?'O '' 'S ''E" ~ ' '                                '
            ..                       _ .. , -            +..__.                               - - -         =--=A--                      '= ~ :- -                ^ =-            "
2 , ,.            ..                                                       .
       .e 4* r                                                                 DEA AND RADIATICN TOLERANC 4
Y p                 *                                           #'
* M PAREL' s'M.uARATICN DATA
* e
         ~                                                                                                                                                 .                        i
: 1. PRODUCT IQ BE EssDr                       NUTEC #11S                                                                                     -
: 2. TIPE SC3 STRATE:                ASTM A-36 Carbon Steel                                                                   57 3 ,     2" x 4" x 3"       s
, .           3. SURFACE PPIPARATICN (Describe): Clean-n-Strip cleaned to bright metal i
J i
          ,  4.   .PRCDUCT DATA: SAMPLE NO. (s) :                           7822 CA 3 AND TI.'E CURING CCMPCCND CR PRIMER APPLIED:                                       N/A
{. 5.
j                                   PRODUCT
* APPLICATION CCNDITICPS                                    IHICKNESS             TIME & DATE
* COAT         PPCDUCT              __CCDES               3AICH #             METHOD            R/M(CF)%R.H.                            (ins.)                  APPLIED
          ; Front          NUTIC                    #11S             2417              Squeegee                  86/73                        .022 .027                        9/25/S0 2102                               .
2103                                                                       .
37.ck        NUTIC                    #113             2417              Squeegee                  84/76                        .021 .027                        9/26/80 2102 2103
          =J?)
c
                                                                                                               *                      ~
i.' ;
l                                                                                                                   .'
l
: h.     .'.         .. .
: 5. CURING CONDITICNS: AMBIENT TEMP.                           80-90             C[.'. Q , ggy g g . 70-80                                                  g MINIMUM CURE                .? 7             DAYS
: 7. TEST PROCEDURE:                DBA iE-   TESTING PERFCMED BY:
* Cak Ridge National Laboratories                                       .
3 10/13/80 r           .
APPROVT.D:                                 .    -
cs s
Q                                                                                         EST'REPCRT NO.                                462-81                           i l
s ie

p._ %iT.: ,:>: WAu _ v.-;' .::@l..~ ' ' :-mm i g-:k n%. % > . '+ - .                                                                                           . ;: .-~,. M u.. w,;n >
* w.w. <?4wntMen
                                                                                                                                                                                                                                   ~
                ..a              .
                                                                                 .w                          .
: d. .
    .r:                            -,        .                                                                                          .
      -f d' ; ~ -
     .                                                                                                             DBA AND RADIATION TOLERANCE
    -e.                                                                                                                                                                                                                                            .
                                                                                                 ,.-~.-
                                                                                                                -: TEST PAIEL PREPARATION DAR
:.?,
     .4                                                                                                                                                                                                                                               o
         '. t                 PRODUCT TO EE TESTED:                                                     nuene stig                                                                                                            -
       *. t. TYPE SUBSTRATE: AMTM A-36 carben Steel                                                                                                                                                          SI2E: 2          x'4 xh"
: t.              SURFACE PREPARATION (Describe) : Clean-n-Strip cleaned to bright metal
       . i. . PRCDCC: DAM: SAMPLE NO.(s): 7823
: h. DA':2 AND TIMECURINC COMPOUND OR PRIMER APPLIED                                                                                      v/a
  .-l
* PRODUCT                                                    APPLICATION CCNDITIONS                                                                THICENESS              TIME E DA22
               *E .                PEODUCT                          CODES                                      BATCH #          METICD               R/M(*F)%R.R. **                                                 (his . )               APPLIED
           .                                                                                                                                                           s
       .j Front NUTEC                                                  fils                                     2417            Squeegee                                     86/73                                 .022 .027               9/25/80
           .                                                                                                    2102'                                                            *
                                                                                                       *       ,2103   a c'~
' "} B2ck NUTEC                                                         tils                                    2417            Squeegee                                     84/76                                '.021 .027               9/26/80
           !                                                                                                    2102 2103
           .O
         ..a n :., . . ., s .. : & , ~ . . . + -:                       .. :. .          ..
t-b                                                                                                                  -
p           ,.: CURING CCNDITICNS: AMBIENT TEMP. 80-90                                                                                        F RE::.. HUMIDITY                                                    70480                    g MINIMUM CURE                          17                      DAYS l.i L
                                                                                                                                   ~
              ' TEST PROCEDUPJ': DBA                                                                                                                                                                                  .
8            .
:.. TESTING PERFORMED BY:                                                             Oak Ridge National Laboratorieta.:g suggg.r.:.g3                                                                              10/13/80
            ,                  e                                                                                                             APPROVED MY:
DATE:                                      1/22/82 j,                                                                                              .                   .
Maurine Lee c
o                                                                                                                                            PREPARED BY:
li '
: 1.                                                                                                                                                               Darz:                                      1/16/81
: l.                                                                                                                                   TEST REPORT E. :                                                     462-1-81 l
               , , _ - - , .-                  , , . - - . , - . . . - - - . , . - , , . . . - - _ , , _ _ .                                         -n--_,_,,,,,,,..,,,,,._.-,,.n--. - . , _ _ ~ - - - .

Q..fi9                   : * .@ ,u>1'x.%f%ciGG::7 o .h ; sn                                                 '
J i.;,m.4i % r                                         '? <- n                                  %                ' _r:1Q.1
                                                                                                      ~
                                                                                                                                                                                        .>.;"~
                                                                                                                                                                                    . . - -        ~m ~.-                               ..
g..                 .,                                                        .                      .
  .o J
         *:                                                                            DBA AND RADIATION TCLERANCE
   .                                                                s._
C        ' TEST PANEL PREPARATION DA3
 'b                                                       L
    '1.           PRODUCT TO BE TESTED:
NUTEC #115                                         ,                                                                                                     /
: 2.        TTPE SUBSTRATE:                 ASTM A-36 Carbon Steel                                                                                                                 SI2E:        2" x 4" x s"           1
                                                                                                                                                                                                                                                     ]
    ~ 3.          SURFACE PREPARATION (Describe):                                                Clean-n-Strip cleaned to bright metal.                                                                                                              j
                                                                                                                                                                                                                                                     \
: 4.        PRODUCT DAns SAMPLE NO. (s) :                                                      7824 i.5.              DATE AND TIME CURING COMPOUND CR PRIMER APPLIED:                                                                              N/A PRODUCT                                                         APPLICATION CONDITICNS                                                          MICKNESS              TIME & DATE CDAT             PXllDUCT              CODES                            BATCE 4                        METHOD                          R/M(OF) %R.E.                                    (ins.)                         APPLIED Front              NUTEC                            #11S                  2417                        Suqeegee                                           86/73                     .018 .026                             9/25/80 2102                                                       -
,                                                                                  2103
                                                                                                                    *I'*                                                                    *      ~*                             '
Back               NUTEC                            #1h.S                 2417 2102 2103 NCTIC.                 *
                                                              #1201                1958/1959                   Spray                                               74/78                    F.    .003 .004                       10/1/80
                                                                        .                                                                                                                   B .006 .007 Total Dry Film Thickness Range - Front .021 .030 Back .024 .032 c.-               ,
~
                                 .                                                                                                                                       I
                                                                                                                                                   .r                  i                      -
                                                                                                                                                                                                 '~ ''
l.]                     .s.      . p:4, _ *          "
_C.          CURIM CONDITIONS: AMBIENT N .                                                        80-06                        F NL. HUMID $TT' 70-80                                                                       %
MINIMUM CURE                                17                      DAYS 7 . TEST PROCEDURE:                               DBA                                                                                                                 ,
: g.       TESTING PERFORMED BY: Cak Ridge National Laboratories                                                                                            .
gg                  10/13/80 APPROVED:                                /M O                                                                                                                                     DST RE,cRT No.                                     4 2-81                               . ,
c o
C
             -%.,                        .,  ,,-.,,-..-----,-,,,,,.,.,,w.,             ,,,,~,e-,---,               ,-.,-----.-..,.,-.,,-,-,,-,,--,--,..--,,...,,,,,,,m                                      -,....---r,....-n.               , ,-, -

   @ ;g E.QMha.N5                                            .>           .    .?. A.'D .%5:y.8 $N"
* c                           ' ? . e: %:.                                 . -~-
                                                                                                                                                                                                    "t      L .n n      _
                                                                                                                                                                                                                             ***      ..nh W..               :~y ;
a u                                         4     .a ..z.
                                                                                                   ...                              -                      a ;;.. . . .' : , . : -.                               .
                                                                                                                                                                                                                      .s..r.        ...,r..a                  .
                                                                                                                                                    ~~                                                                         -ac;.
g p . . :-
    ,I - :                                .,         ,                                                                                 ,
   ' ,.t;.                                                                                              DBA AND RADIATION '!CLERANCE 7                                                                               <
ff'JTEST PANEL PREPARATICN DATA
    .T 1                                                                                                                                                                                        ,
    , . l. PRODUCT TO.BE- TESTED: NUTEC filS i
l!
i 2. .                     TYPE SUBSTRATE:                      ASTM A-36 Carbon Steel                                                 .                                                            gggg, 2" x 4" xV Clean-n-Strip cleaned to bright r.etal
[ 3.                       SURFACE PREPARATION (Describe):
: 4.                 PRODUCT DATA: SAMPLE NO. (s) :                                             -
7825
    '[5.
DATE AND TIME CURING COMPQUND OR PRIMER' APPLIED:                                                                                           N/A
       .                                                      PRODUC:'                                                      APPLICATION CCNDITICNS                                                       MICKNESS                   TIME & DATE
:CDAT                              PRODUCT                 CODES                      BATCE 4                           METHOD                         R/M(*F) tR.H.                                   (ins.)                     ' APPLIED
       ; front                                 NUTIC                    #115                     2417                           Squeegee                                         86/73                   .021 .026                                  9/25/8C 2102
* 2103 <.
       ;. Back                                 NUTEC            -
                                                                        $115                     2417                           Squeeges                                         84/76                   .018 .024                                  9/26/,8(
:                                                                                         2102 e                                                                                    2103
       ;g.                                                              .
       .                                       NUTEC                    #1201                    1958/1959                      Spray                                            74/78                   F .003 .004                                10/1/8(   ~
                                                                                                                                                         .                                               B .004 .006 t                                                                                                                                                                                                      '
f s
;-                                           .                          Total Dry Film Thickness Range - Front .024 .030
       -                 .                                                                                                                                   . Back .022 .030
    ..                                                                                                                                                                         g.: -
                                                                                                                             .                                                        l 3                                                                   .
       'f.                CURING CONDITICNS: AMB'[ENT TEMP.                                                                80-90              07 i,-                                               , , , ' 70-80 MINIHUM CORE                            17                                 DAYS T. TEST P.*CCIOCRE:                                                 DBA Cak Ridge National Laboratories                                                                             .
10/13/80 l - I.                   TESTING PERTCRMED BY:                                                                                                                                 .
DATE SUBMI N
       *3      .
APPROVED:                                MN                                       A
     .h                                                    .
TEST REPORT NO.                                         462-81 a
l5 e
l
           ..- - - , - - - - . - - . - -,                                              . - . .         . . . . . . - , . ,            . - - - - _ , - - - - - ~ . _ . . _ . - - . . _                                                     - . , - - - - -

cy1                2Q+_        is    ''t'-      *
                                                    .G''         ':
* 4 ' ' * -: ~. ?
                                                                                                                    '>      * :'P            <~.'s $ '             ^''n-         :'~'''--
_,_.                              . , . .. . .          ..                              _ - - . . . . .            =~.               - - -      2-      -         - --
Y                    .    --
     .5                                                                                                                                                                                -
u 4 .. .   .          ..                                                                                                                                               .
p,
* DBA AND RADIATICN "CERANE
   .a                                    .
d                                                                                                                                    .
       '.                                                    -         -   ' TEST"PANZL PREPARATICN CATA                                                              .
       ~
4:,
      .i                                                              -
l
: 1.      PROCUCT TO BE TESTED:                         NUTEC 411S                          -
:2. TYPE SUBSTRATE:                      ASTM A-36 Carbon Steel                                                                     SIE:            2" x 4" Xh"
[3. SURFACE PREPARATION (Describe):                                    Abrasive blasted per SSPC-SP-10, near white blast, with j            c surface profile of 2.0 mils as read on a Keane-Tator Profile Cergarator D:.sc.
      .)
i
: 4. PRODUCT DATA: SAMPLE HQ. (s) :                           . 7826
: 5.        CAE AND TIME CURING CCMPCUND CR PRIMER' APPLIED:                                             N/A 2
          ?
PRODUCT                                     APPLICATION CCNDITIONS                                 THICKNESS               TIME & DATT CCAT           PRODUCT                CODES              BATCH #                 METHOD             R/M(OF) %R.E.                          (ins.)                  APPLIED 5 Frent           NUTIC                       #11S            2417                 Squeegee                  86/73                      .020 .050                     9/25/SC 2102                                   -
2103        ,,,
Back          NUTEC
                                                        #115            2417                 Squeegee                   84/76                     .024 .030                     9/26/8C 2102 4.. :
h                                                             2103 q
(i I t 4
                                 .                                                                                           t
                                                                               .                                 .A                      -
g . 4. ;         >-    . ;a '.
80-90              C                                              70-80
: 3.       CURING CCNDITICNS: AMB N TEMP.                                                      y RE'.. I     HUMIDITT.                                            g MINIMUM CURE                       5r            DAYS F.      TEST PROCEDURE:                    DBA 1 -
           ,I . TESTING PE7uTRMED SY: Cak Ridge National Laboratories DAE SUBMI M                        10/13/80
:4
    ' .*        m                                                                                            APPRCVED:                     . M
?; . M                                                                                                       TEST REPOR:' NO.                          462-81                          .(
l i. .' ':
l l5
>g
!i
* i1 -
!t                                                                  .
s                                                                                                                                                                                    .

          ,. , . ,                       e a. :,,. r g _ .+. .' + . 7 % ' '''W . $_hd ? : U*A -' 53                                              ~~A ' i ,                 ***            O       *
                                                                                                                                                                                                   / ^* ' ''~ ' '                '
                                                                                                                                                                                                                                             'E       = A. $ ' ' ' "^
                                                                                                                                                                                                                                                                                               'S
                                                                                                                                         . . _                   ., _ _ .                        . . .    ?. L 4" ~~ G ~ = A ~ ~~ ~ '' '
3.g .,'                                                        .                                                                                                         .
4
* DBA AND RADIATION TOIZRANCE
      .)
3h  .I 1
i.p EsT' PANEL FREPARATION DA M 1                                                                                                                             .
I
  , ]l. PRODUCT 10,BE TESTED:                                                                                                   w - a3*e                                             *
:2. TYPE SU3 STRATE:                                                                   ASTM                      A-36      Carbon Steel                                .
SI22:            2" x 4" A"
         !3.          SURFACE PREPARATION (Describe):                                                                                           Abrasive blasted per SSPC-SP-10, near white blast, with a surface profile of 2.0 mils as read on a Keane-Tatar Profile comparter Disc.
{4. PRODUCT DA3: SAMPLE NO.(s):
7827 N/A
      }5. DATE AND TIME CURING COMPOUND CR PRIMER"APPI.IED:
          .                                                                                 PRODUCT                                                             APPLICATION CONDITICNE                                                 THICKNESS                TIME & DATE l' CORT PECDUCT                                          CODES                                BATCI 4                         METHOD                      R/M (*F) 4 R.E .                             (ins.)                      APPLIED Front                           NUTIC                                             #113                              2417                          Squeegee                             86/72                          .018 .026                             9/25/80 2102                                                                                                                                .
2103
* e               a   ,
Back                            NUTEC                                      .      #113                              2417                          Squeegee                        ,    84/76                          .'021 .027                            9/26/80 2102 2103
         'Lm:
                                                               ,                        ,            .                                         .s < -                 .
t
                                                                                                                                                                    .                        s e
a.h.
                                                                                                                                                                                                          . . . . . ..: e                                       .
: i. CURING CONDITICNS: AMBIENT TEMP.                                                                                                       80-90                         0 7;jgj.. NCMIDITE *-                                         ~
MINIMUM CURE                                            17                          DAYS TEST PPCCIDURE: enA
             .            TESTING PERFORMED BY: Cak Ridge National Laboratories                                                                                                                        -
DATE SUBMITTED                             10/13/80 l
l l.
,                           s, APPROVED:               -          JbId 1                                                                                                                                                                                        TEST REPORT NO.                                  462-61                                           i 4
1*
l'!
         . - _ . , . . . , , - . - - _ , , _         ,v.     - _ . _ _ _ _ . _ _ ._,%,_            ,_....,,,,__...._.,,.e._,,,,.,                          m.,,   ,,,m...,             ,,                 -_             .....y_._,e           _                     ,,-.m ..y,,r.,w.c,,

         ,                 ,m   .._.            .   .n..-          m.
                                                                       . . n.1               .-.. .                        ,3.m _                  --                ...                   . .                   . . -
                                                                                                                                                                                                                                              -                         -                      -m
                                                                                    ;g_                                                                                   . .. . .                          --.81---.=*i---***                          ~* -                      *'
      . .i
* 9 ., *    ,              ,
            .,                                                                                                           DEA AND RADIATION '33LTRANG
        -~% s
         '[            .
                                                                                                        .j,, TEST PANEI. PFZPARATION DATA
: 1.         PRODUCT To,BE TESTED:                                      NUTIC #115                                                                     .
T2.            ITPE SUBSTRATE:                             ASTM A-36. carbon Steel                                                                                                                                    SIZE:         2" X 4" X5"
: 3.         SUPJACE PREPARATION (Describe): Abrasive blasted per SSPC-SP-10, near white blast, with a:.rface prefile of 2.0 mils as read on a Keane-Tator Profile Comparator Disc.
: 4.          PRODUCT DA"'As                       SAMPLE NO.(s):                                           .                      7828 55            DATE AND TIME CURING CCMPOUND OR PRIMER APPLIID:                                                                                                    N/A PRODUCT                                                             APPLICATION CCNDITICNS                                                                       MICKNESS               TIME & DA7T CCAT               PRCDUCT                         _ CODES _                    BATCH #                                   METHOD                              R/M(*F) t R.H.                                              (ins.)                      APPLIED Front              NUTIC                               #115                            2417                          Squeegee                                          86/73                                     .022 .027                                9/25/8s
    .     .;                                                                                               2102                                                              .
             ;                                                                                             2103                  .,,
    .        [ Back                    NUTIC
                                                                           #115                            2417                          Squeegee                                          84/76                                     .015 .020                                9/26/8
         -*                                                                                                2102 2103
              ,.s
                                                                           #1201                           1958                           Spray                                             74/78                                    T      .003-                              10/1/8 j i, NUTIC
                                                ,..   ..               .n..          . . . . . . ... c.1959'
                                                                                                                                ' ' " ' "-                                                                                           3 .006 .007 4
Total Dry Film Thickness Range - Front .025 .031
:                                                                                                                                                           ' Back .021 .027
;             i                                                                                                                                                                                   I J.h. .          ..               .c +                -      -
: 1.          CURING CONDITICNS: AMBIZZT TZM.                                                                     80-90                              O    y'. h . HUMIbnkl'*.                                                70-80'                     g h                                                        MINIMUM CURE _                                                17                               DAYS 1                        .
i
   - T                     TEST PROCEDURE:                                          DBA 3         TESTING PERFCRMED BT                                      Cak Mdge Nadonal Wratories                                                                            -
DATE SUBMI N
: l. .
               .I,_/                                                                                                                                                         TEST PEPORT NO.                                                  462-81                                         .
,: i                                                            t
  .b  .
               ?                                                                                !                                                                                                                           *
* r L
,j.':  ,

                                                                                 .u      ..                                 -
                    .X._..,     .   .~..._._                      -.
a        . ~ - . . . .                 . - - . , .         . . .
F                                     _.c.                    .            .
g . ,*   .           4 ,.
3
     .*                                                                DBA AND RADIATICN TtX.ERAN 3
    *h
                                                                -'"hTEST PANII. PREPARATION! DATA                                                                     ,
i,
      '1. PRODUCT TC,BE EST:                             NUTEC ells                             .
                                                                                              -                                                    2"
* 4" *I" 2            TYPE SUBSTRA:Z: ASTM A-36 Carbon Steel                                                                        SI2:
: 13.              SURTACE PREPARATICU (Describe):
Abrasive blasted per SSPC-SP-10, near white blast, with  ,           ,
                                                                                                      .w      . .... . --.                            -..... ___..
o surface profile of 2.0 mils as reas ca a u us .                                                                -
7829 N. . PRCDUCT DATA: SAMPI.E NO. (s) :
: 3.              CAE AND TIME CURING CCMPCCND CR PRD1ER APPI.IID:                                  N/A PRODUC:l'                            APPIICATICN CONDITICNS                              W IC20iESS                   TIME & DATE
      ;AT                  PRODUCT            CODES             BAICH_4_            METHOD              R/M(OT) % R.H.                     (ins.)                     APPLIED e
      ; Front                  NUTEC               filS              2417           Squeegee                       86/73              .022 .027                         9/25/80 I.                                                             2102
* 2103 s
Back             NUTEC         ,
11S               2417            Squeegee                       84/76             .'020 .050                        9/26/80 2102
       ;                                                             2103 i                                _.
T .002 .003                       10/1/80 NUTIC              #1201             1958            Spray                          74/78 1959                                                             B .006 .007                           .
Total Dry Film Thickness Range - Tront .024 .030
        ;                                                                                                   Back .026 .057
* s 6
                                                                                                                   .v  ,
        ;
* 2
                                                                                                           .h         > .*;' .-
                                                                                                    , .f ;                                   ', '                  .
: 5.          CURDIG CONDITICNS: AMEIINT TIMP.                      80-90                  F "RII.. HUMIDITr
* 70-80                       g i                                                  MINIMUM CTRE                17                 DAYS l
DBA
            .        TEST Pis.t.uwE
        ,I . TZSTI:3G PERTCRMED BY: Cak Ridge National I,aboratories DAIZ SUBMITTID                     10/13/80 APPRCVED:                     Ab                         Mb E:               ...)
t*              >                                                                                     TEST REPORT NO.                       462-81                          -
r L
bh o
1-:.

p *~1cy _ ,.~. *.   ,.E.-    -s               * '*-    ,Yr s'            -
M-                 ' ~                         ..O',*          a _E _ ?. -
                                                                                                                                                                           **' s ! L:.     ._
w                           - 6:% ~     --
s'. G2 _^ -                         : '...              w'              T ~ Y:         '
: s. M --     ~b   . *:* - -
                                                                                                                                                                               ~- ~ "-'
s                    .                            -
t .**             .
             -         ~
2                                                                                                         .
e o e
6
                                                 ,e*=     '
O l .r i
        .                                                                                                                                                                            g 9                       y 9
9 e
e e                                                                                 e CRNL PROCZDURES s
9 b
w            e   4 3   *'                                                            O 1        e                                                                                           ,
n                                                                                                                             9
                                                                                                                  .t =
0 t
                                     *                                                                                   .f
                                                                                                         .,)
a..            .. . .     ,.: .-     .
t                                                                                                     ==                             ** .          .
                                                                                                             -9
                                                                                                   ..                         .)s..
I e
e e
O 8
n h
s n
b 3 '/                           et lg .
6 V -

                                                        . . .w .w.~        '
                                                                                    .,.             n . c._      .w                      .-       ..;
    - ' % . e..             . . 7.r.- a - . :n                  n..         .   ..                                      .
       *. 4.c   -L-                              .
A.] ,                    _:        ---      1.t                  _ __         _w..._
1
: m.                .   .              .
                                                         - '                                                                                                 l Imperial Manufacturer:                                               Arialytical Chemistry Division
    $y-( -
* New Orleans', LA                         Oak Ridge National Laboratory                                  ;
                                                                                             .Date:          11/13/80 Q
    . .-                                                   Report of Irradiation and DBA Testing                                              ,
(~                                   The irradiation and design basis accident (DBA) tests are conducted.
respectively, in accordance with Bechtel Corp. Secnd:rd Specificction Coat-3                           ings for NucIscr Pouer PIcnes,. specs. CP-951 and CP-956 (or with modifi-
      .i                          cations.as' noted in Table 2, DBA test conditions). The tests are designed
: f.                         to meet the specifications set in both A.N.S.I. report N 101.2-1972, Pro-
: i.                          .ective Coa:ings (Ecints) for Light Water Nuclear Reac*ar Cantair:nent f                          Facili:les, and N 5.12-1974, Prctactive Coatings (Pain:a) for the Nuclear
       <                         Industry. The DBA test spray solution and the test conditions are listed
       .!                         in Tables 1 and 2. After both the DBA and the irradiation tests, the
       ;                          coatings are examined for signs of chalking, blistering, cracking, peeling,                                   .
delamination, and flaking, according to ASTM standards where applicable.
All test panels a.re ,returney to the coating' manufacturer.
j                             . The irradiation tests are run using a spent fuel assembly, removed
      .:                         from the High-Flux Isotope Reactor (HFIR) at ORNL, as the source of radia-
       ~h
                                . tion. These_ fuel assemblies are stored under 20 feet of demineralized
       ,                         water. The fuel .is 93:; enriched U235 .as U 0s       3      ccmbined with aluminum.                              -. :
The spent fuel assemblies are removed afte'r each 23-megawatt day period.
Irradiation is done using the gamma energy from the accumulated mixed fission products. This more readily simulates conditions around a reactor than does a esbalt' source. Also,'the higher gamma activity affords
;                                shorter irradia, tion time to achieve accumuTated , doses. The dose rate four                                          .
days after removal of a fuel assembly from the rea'ctor is 1 x los rads /hr.
The fuel assembly is 20 inches high.i,-d.j20-fbotji gggi/,2Sinch diameter pipe, with one end capped, is used for the air irradiation tests.
The capped end is lowered into the four-inch opening of the center of the fuel assembly.       The open end, above the water level, is cove: ed with an "0" ring sealed flange to which is attached a steel cable and an air ouflet hose. The air inlet is located at the bottcm of the pipe. The test speci-mens are connected to the bottom of the cable and lowered into the radiation field. Also at the center of the fuef assembly is a stainless steel clad j'
               .s               cadmium tube used as a neutron absorber.               This, prevents contamination of the test specimens by induced radiation.t                                                 -
Evaluated                     2..               /b'        '
: b.                                                                            A,,,;ved W M.

aC,          .m     n: , . _ , . --           . . c. ,              ,     ,.
                                                                                    ;   c         .        ..            ._
: g.       _   _- .       ,
                                                                                          ~--                        - - -
                 ,.:- -                                -           - -.          .i a
O                Manufacturer:                   Imoerial                                    - . Analytical Chemistry Division
   ?                                                                                                ~0ak Ridge National Laboratory j                                       '
New Orleans, LA                                    Date:             11/13/80 I-                                 -
   .1:
ORNL Log Book No. A 7562;                     'A10-29-80 Table 1.           DBA solution composition, distilled water Reacent                                                   ' Concentration i                   Boric acid, H B03   3 6200 ppm 5                   Hydrazine, NH NH2   2                                                50 ppm
      $.                  Trisodium phosphate, Ha3PO[12H 2O                                     Required to adjust pH to 9.7
      .r .
: i.                                                   .
       -                                                                                                                                              ~
l ,:                              .                       Table 2.          DBA test conditions                                                 -
{;                             Temperature                Pressure
     .-"'              Time                 (*F)                     (psig)                                    Comments
      .I                                                       .
                                                                                                                                                ~
4 i           Start                   ~214
                                                                  ''                    Autoclave preheated.
:          58 s                     385                          68             Steam injected.
5 10 min                   385                          7'O            Pressure maintained by relief' valve.                     .
$i                 4 min                385-340                          70
[
6h                       340                          70                           ,..,
        -          20 s -                   220                          30             Spray soluti$n added at 75"F.
L!
l 20 min               220-250                          30             Adjustidpreksur.[swi.th N ..
2 ' '
>,-                 4 days                  250                          30                                                    -
Y        'i         20 s        .
170                       --15 Fresh spray solution added after LJ                                                                                          draining autoclave.
r          25 min               170-200                         10                                     -
f :
:          3 days                  200                          10                           -
I
,,       t                                                                                *
: p.       1
                                                                                              /.
l e b                                                                           Evaluated       Mr/ ,
                                                                                                                                   /.4[    '          .'
fjj                                                                                   Approved      4l. d [A
: r.
* l11*C (i *                                                      -

0                   g .
4 c g _. ,,. . r. y :3. . ,. . 2   2.,   .;    ,            . , , j.              ,  ,.,,,. . .. ..  , . . . ,,       ,
                                                                                                                                                                                                                                     .g.,,...
                                                                                                                                                                                                                                      ,,.e.. _c.._
cze. ~s. A m_ y 3,E .,
e                     .
                                                                                                                            =>                                       ==.
* s
                                                                                                           !                                  e                                 ,
b*          L.              e,   < , we s            6    e   e
                                                         ,e . g e. w ee es. + ammunmus",
p . e,                                      ,                e            e estee n.n 4    .4so.ame me e mosusseme.                                                                                                                                     * *
 ; . . . g.                           .                              . __
: s.                         e i               -         -     .                                               .
a
     -9                           .
i.
t t
e.
s e
* l e
o e
e S
e TEST RESULTS O                8
         .-e.)                                                           --
        -                                                                                                    .e                     e e
e e
D e
9
                                                                                                                                                                     *$            d.         p"
* ifi           e p. a1 .          .
: m. e                  ,                                           ,
                                                                                                                                                              * % 1                       .. * ,
                                                                                                                                                               - . v                             g.
e e
9
                                                                                                                                                                                                                                 ?
2 .%
[. . t. '.)-
i                                                                                                                                                                                                                                                     . .
nN

g- . . ,,.:.                  t.:    ...+,a.<   , .s , . ; .. .w, . , ., .     . , .; ..     ..s..e.   ..                         -     . . p .. n:. i..:.1 _ . t.     ,.u.;
                                                                                                                                                                     ~
                                                                              ~-
                                           . _ . = , .
                                              .            =.-
                                                                                                                          .- y        -     .       . . :..                ..
:--   t
(
jl, ,                                                       OAK RIDGE NATIONAL l ABORATORY opsnavso av J
       -                                                                  UNtoN.CARSIDE cDRPORAT1oM
  *.*                                                                                NUCLEAR DIVis!0N I.                                                         .,                 '[                                                            "
      -                                                                            POST OPPICE 80X X Cast RIOCE. TEMMESSEE 37820
>!                                                                             November 13, 1980 Ii
         ;                                Mr. Gerald E. Arnold "i                                    Technical Representative i                               Imperial Professional Coatings
'{                                        P. O. Box 2S077~
j                               Hew Orleans, Louisiana 70189                                                                                                     .
I j                               

==Dear Jerry:==

The enclosed report contains test results recently obtained i                              on the Imperial protective coatings. This test was designed to                                                               '
           .                              encompass the 385 and the 340*F envelope curves.
If we can be of further assistance, please feel free to call '
on us. .
..:                                 .-               ..           . n.    :r . . . . . ..
Sincerely, l                                                                                 4/,                              -
l.. T. Corbin, ection Head Analytical Chemistry Division    .
  ~ '
LTC:dmw                                                                    ;
a         ;
)                                          Enclosures                                                , 8,i W
                                                                                                                            . . 4 ... ~
i          e                                                                                                                                ,
e I
L b
4 P .
6              .
l n

     .h.       ~
in ., .u   :- m.    :,
                                                                        - .-       9. . , , r.t. . .._, . ,.;... m .. . e ,
:. a.    .. .           -
                                                                                                 . n- - . . .          - - - -   ;     . . _. s.       . . . . _ . . ,                  ,
: m.        ,,                                                                                                           Analytical Chemistry Division di .,          Ma,mtfactu'rer:                        imneNai                                            _
Oak Ridge National Laboratory
  @                                                     New Orleans, LA                                                  Date:              11/13/80 4
  ..~..w
    .:                                                                                                       x' Steel panel                          Concrete block
   '{              System Identification _
                                                                                                                                                                                       /
A'                                                                                                                                                                                  f j           115 (clean n' strip) j DBA Test Results ORNL Master Analytical Manual Method No. 2 0922.
-I                   ORNL Log Book No. A 7562;                               A10-29-80 i
i                                                                                                                         Coments Samole No.                 OBA phase                .
7822                     spray                             Front: loss of adhesion.
i
       '                                                        ,     ,              % ear: loss of adhesion.
1 spray                             Front:      blisters, #2 few. 4 7823                                                      Rear: blisters, #2 few.
  . ,1b)
      )            '               .
i l                           4 FQ                          aQM hub b b '" ' 0)                                   g ll               .
                         .                 i p n.,a A + m f M to A .6 8 O .
1..                                                                                                                                                                                         -
gg,4' i ~:;
L. e                                                                                              .
:                                                                                                         ,-. ..d.,;et     .....<:.*
t                                                                                                                                 .gl..         -
r
' t                        .
I*
f 7                         ,
Evaluated                     J2d             -          44.M
;fQ                                                                                              Approved I.                                                    -
h .'$
s:
l: 1 R. -

1-?l'' ? ._ 2 3 2 :    *__ _ yL v7 % _       fy -         .
                                                                               , .s ~ > = . ~ . _ _ . . . x..:9. i.. 3 , .      ,   .
     ' ..                                                                                Analytical Chemistry Division
    . .! -            .. . f acturer:
Manu                  imoerial                         _
Oak Ridge National Laboratory 1-                                                                                  Date:                11/13/80 New Orleans. LA
[
          .b           System Identification x Steel pan'el                     " Concrete block 115/1201 (clean n' strip)
DBA Test Results ORNL Master Analytical Manual Method No. 2 0922.
ORNL Log Book No. A 7562;          A10-?9-80                                                                  -
:                                                                                    Coments Samole No. 08A chase      .
spray                Front:  blisters, #2 few, 7824                                Rear: blisters, #2 few.
spray                Front: blisters, #2 few.                                                  '
7825                               Rear: blisters, #2 few.
o t                             -               .       .
c                                                                 .
s 9-l
                                                                                        .l;                     -
t
                                                                                                          .:. y .
e l
rs                                                                                           -
I o
Evaluated            Ml                              4 Approved I ,                                       -
2[O ll
* b*
* 4:          '

l c ., . -            , . , ,. ;; , .           ... .             ,.
           =
                          ;',-1               _
                                                                                    .. J..i_ .      a: _ . ...'.             l.' _ , . ;' ' _ _ _ 'a R yf'* "
a-                           e.
- i'" " -                                                                                     Analytical Chemistry civision
* gj         .. 1ianufacturer:         Imoerial                                  _
Oak Ridge National Laboratory
;; -                ,-                                                                        Cate:             11/13/80 New Orleans. LA
 .i                                         .
  .s,
  .!O
   ;               System Identification
                                                       -                        x' Steel panel ,'                      Concrete block
: t.                                                                                                                                                     1
   ;               ils
                                                                             ~
1 OBA Test Results i
ORNL Master Analytical Manual Method No. 2 0922.
ORNL Log Book No. A 7562;       A10-29-80 I
                                                     -                                              Coments
: b.                 Samole No. OBA chase                                                                                                           -
spray                  Front:      coatings intact, no defects.
7826                                           coatings intact, no defects.
I                                        ,    ,
Rear:
spray                  Front: coating's intact, no defects.
i                   7827                                Rear: coatings intact, no defects.
1 h
e       .,           _.      .     .                 ..
9                                                                                  -
:<      a         .
                                                                                        . ?;   -
s-
                                                                                                             .cg...
t                                                                                  -                                ..
i                                                                             /
Evalu ted               4dI'               .  [A Approved [                                                                        .,
6 e
e e .. . em e e. m e amp .

          .: ~    +      .
                                          ~
m
                              - . ~ ~                                     . . .                     ..:-_..      . . . . . ......._ ... , . __
Imoerial Analytical Cheraistry Division J~i ~          Minufacturer:                                          _
Oak Ridge National Laboratory
    -?; -                                                                            Date:                   11/13/80 4                                   New Orleans, LA 3                                                                                                                                         -
                                                           ^
x       _ Steel panel                          Concrete block System Identification
     ?            115/1201 i
s OBA Test Results fi
:           ORNL Master Analytical Manual Method No. 2 0922.
j            ORNL Log Book No. A 7562;         A10-29-80 k!
3                                                                                         Coments 4             Samole No.        DBA chase.                                                                                                   -
a.
spray              Front:   coatings intact, no defects.
      .!*             7828                                       blisters, #6 few.
Rear:
f Front:   blisters, #2' medium.
f               7829             spray Rear: blisters, #2 medium.                             4-                              *
      .,. s
:   g&            E $c;n W                       Q^ - " 0v- -
es . u - 4 , p _ _f v (.s nuQ
  -lh .
Pr : M&
\
c t
                                                                                     .;)             i
      *                                                                          '*    4                  .!;..s. ,
I
    ~!                                                            Evaluated / ' 42 / . ,                                      bs /
lU                                                          Approved                     ,
$i ."                                              ,

   .g. .;2        , .,           s            g a.c o                        e e                                 .. t.n u                                                            .             .qa.                              . . . .                                                  . _ , , , , . , ,_  ,
                                                                                                                                                                                                                                                                                                                                         , ._ . .; ;g, g .,,.a . .z, . .
                                                                                                                                                                                                                                                                          ---.~.-.-=                                                 .                          --                     -
_.u r?-           --
g                ....
Techtticci Report :.62-81 J. . *.       .
1
                      *                                    . z...s.,......_  . . .w +~ . ea..s.s;.^i-
                                                                                                                                         - g. , - i. =:*r.it*
                                                                                                                                                                         -- .2,, ....'. . -
    +
: .               t                                                                                                              ..         ;..                 4. .,.. .                         .....
e                   :                                                       ..              .     .                   ...         o . .,: p .2.-4.c- 4 9. 4 3
                                                                                                                          ...t,.,.. . . . ...,.2_..,.,..                 ..,.n..--.
a
                                                     . . _ . =.                             m.                          . - .ww=.-,;.e..-
                                                                                                                 . w .= -
2 .g W..
                                                                                                                                                                                   . m.            . %..
                                                    .                                                               3,                                                                   .                  . . .
:*                     ,. . r ..g . . :, O .<. W t. ::~ $ 4.* - @
   '.;                                        W                                   -
                                                                                                ~C-k % 1.g .
* N..-$                                                                  78'" -78'3 W. d$ akk.N ihh. ..Eh                                                                                                                                                                                                                                                                                                                                                 .
:                    W. 4 .4..*.w=.e.                                                                                   i =;. A m                            .. . : JesM -
r                                   .
                                            .g                                                                      ,ic                                                                 =.: r>.eb ;.
e...                        * - . .
                                                                                                                . {un                   ..                  .
ime .
                                  . %>
* Q:,
                                                                                                                     .                .+.t-*     .-                    L:ct.w
                                                 =$             .
shi}++l . *.i
* E*   q '=                                                     .;'-.^ * ^ ^                                                                             .
g
                                           .n      :
:.r.-P..                      . .- g -:+. . G. ... .3. -.~~ :i                                                                     - . . .
r 2    . . ...:.. .. ,,,
                                                                                                                                                                                                                                                                                                      .. .. ... .?        .Q.
e m.
                                                                                                                                                                                                                                                                                                                                            .,e o. ,-, . .
1 -4,,g g                                                     ,
                                                                                                                                   . *.  .. --                g,.;*48       u..                   J:""j.J.
n r
                                                                                                                                                                                                                                       - ..                  - ..,.; m. .f,.h. . .-                               .m .
                                                                                                                                                                                                                                                                                                                             .+. a.*...~. a       m.c   v..c  ~. ....-n.   - *-ee
                             .. . . a                                          .
A. >                                           :.                 .. m .
                                                                                                                                                                                                                                       -- w.~--.n:                                                                             .
Ein n ,g ,.@... G.e                                                                                   W+ r-M=v.. . g,J C E yA c., .                 t                          -
: y.             .
                                                                                                                                                      ..           ,7 .'.c. .                          ~~t                              .                         . . .                                  ..
                                                                                                                                            ... .. ee.
                                                                          -       - ~ ~'
s
                                                                                                                                                                                                                                            ..,., .,::..j,.c==:.,.,,v.:-.:.
r..c;;..    . .. f.:                            -.e 1.m e . .- ....u.:                                         f- ,q..
wr. .
                                                             . ..g.%e.- 5 3.d.n..:w.M'...                                                                                     w;Mr.                                                              wr.rre-y'c."=".            .
   .!                        .                            . e. -                                                                                                                                                                        it>p% d M M Q =,'171 @#"5r,M                                                 --
T'+                         Met-C'W.W-4
                                                   ~-$:@i:;5dnsdi'                                                                   :Fi:$ii.%                                  SG:2W~s.M-
      ,                                                  ee.:c.a.=r
                                                                                  .GMS&M:iF                t%&'"
E
:@.+5Ess+ T.,a1h # . M- [ '- *Q4 x r ,;_ .- . " " ' =
                                                                                                                                                                                                                                                                      ~.t       -
d7-L "T*N
:                                                  . - <.-W2..9@:i.
                                                                                       . ~ . - - '. ?o%.                     .W::  . . :-W-mcLgfw;m  .            =-                                                                    i                         ;r- ~~ 1                       .
                                                                                                                                                                                                                                                                                                         .                 s.. :
                                                                                                                                                                                                                                                                                                                                               .m.                .
W.
      .                                          ... . .- ..u.s,.~,   ....r.: t.>, .4                  <.m
                                                                                                                                                                                  . a c sosr5                                           I
                                                                                                                                                                                                                                                                                                                   ,                           1W .           -        ;
                                                                                                                                                                                             .ge i
f s                             i.__.4.?Ei         - . . .W'".W: *
                                                                                                                         '. u
                                                                                                                                     .w,
                                                                                                                                      .    . m.-.
                                                                                                                                                   ..v
                                                                                                                                                                               -mm~
* c      :   ..:....x
                                                                                                                                                                                                               .:.Y:
                                                                                                                                                                                                                                        ,=
                                                                                                                                                                                                                                             ,l ' l. 18 2 $ $
                                                                                                                                                                                                                                                                           '. '                          ".Q*L                         'M&
s s                                         .-.... .. ,.             .. m,                                 :: . -..... . .-gi. t y. . *,.
                                                                                                                                                                                                                                                                               .                                 b.>-     -
O..i.M W.:,..:..,;;.
                                                                                                                         . r. ..v? ~ ' A .s 6                                                           .                                   .                    ..                                                                                     .
:.                                                                                                                                                                                                                                                                         . .. t=
s                                            1.r
                                                                                   .. -..-. - -~
:<=h:8 B     ..   -       >",_.              .                    .
c
(                                                     .
                                                                                                                                                                                                                                                                                                                                       ........a
                                                                                                                                                                                                                                                                                     ..               .            ~,
p
(~...._-...
e                                                                                            -
                                                                                                                                                                                                                                                                                  .      ..             .          d.                          n .+-                                       h:
                                                                                                                                                                                                                                                            , p:                                                                                                                   ^        '
                                                                                                                                                                                                                                                                                                                 .(,--
g..-a <;--
n .                                                 . .                         .
                                                                                                                                                                                                                                                                         ~.                     ...
y                         ;
                                                                 . .w:.-. t.s.w._:n--             . .                    u                . .. m
                                                                                                                                                                                               +n=..n                                                                   .
                                                                                                                                                                                                                                                                                                                .1                                           -
                                                                                                         -
* w~:;;                       % ,.=m-esdQ   m .m 1                                            7:.:*4;;?;:y         .e-x.s-2_s &;a                            -
Adtll.~
u _ - .g_
l                                                                                                                                                                                                         l                                                           .                                                                                     (
                                                                       ..=..                                                                                                                                                                                                                             g j
                                                                      ' '""*^g;M-                                                                                                                                                                    .                                                                       .
                                                                                                                             .;c. .
 's l                                                                         * . e t,                            ,  ,,y.
d Mr2+..T.                 3"7.3,;,
:                                                                                                               'D.'*5r.w.d'
                                                      ~ ; * =:'
* u--*
                                                                                                   . t* -                .***''                                                                     **                9 .
                                                                                                                                                                                                                                              ^-t"f' jh,                                                  .W -C'$
                                     . ~'*,~:+,=.: % .. .T**.D_*J                                                 C- -,,c.,.-.a.,-
                                                                                                                           - _ . . _ ._. .x. ?- . m,.5-~.                                                                                                                                                   .3 m                                              p%e;,.J
                                                                                                                                                                                                                                        &<z                                            . ^
W           ..
W:
h h h.hh.
5.Y,# r-_-_-.--.e--
u . .- _ :                           enYNYMNIb  _ _
                                                                                                                                          . . - w s - ww                                        x. -s 5'M w;
s.-._.                 -          -                       --
                                                                                                                                                                                                                                          . ' a,.               -.qy:.: p:y*f._.; s:. .fa::=I'f*.t U ~ "4W-5.*
                                                                                 - -                                   ,5      s . .       m---
                                                                                                                                                                       - -                      q-',-;E,                                I ;' E 'i' e'.L;.
                                    -               =y=i.r""'                                                                  P '-                                                                                                                  .4g ,4;,i ,.r. , T. . . .,... u. me
                                                                                                                                                                                                                                                                                              --*:e Q..v.         .s ,+.W-i@: 4*:y--s.N . -;.=Me%.:e"
:.:;;f. ,                                                                                                                                     .-                                            G.,,.p-::.e.                          .*
                                                                                                                                                  '.                      e*
7 sr ;4)                                              .                                                                                                ...                                           w .w.                       d .+ a%...-.a.= : A                                          .. . - ~as-e e ".:d'h"%"'drd
                                                                                                                                                                                                                                                                                                                                                         '"-=*tM8w--
                                            .;..             j s :., =
                                                                                                                                                                                                                                                                       ..                             ri wglY-i
                                                                                                                                                                      .e                                                                s;                                                                                               :~-             .~w * ?'un.a '. t
      *                                             ,;;sj
                                                                                                                                                                                   ~ . .
                                                                                                                                                                                                                                        .A. s .s. :. . '.#. J .f . w-m Q.'ij we.W.m.mM.                                                    s.~-.
w.=%'- .-*.' ' a -. z.,us,-3.%.     .'          -
                                            .',i                                                n.                                            .n "o                                                                                                                                                               -
                                                                                                                                                                                                                                                                                                                                                               .+.'%nD Me..yr W-M.S M ;.n                                                              = h'.>R+g %~.
                                                                                                                                                                          .a
      -                             W!h. '
:.u.;.i,,e4[.                                                                                                                                           f*'                                                                                                                                                  .P.. 3 - $ 3
                                    , asiq a
                                                                                                                                ,             ~T. @a
                                                                                                                                               . . . ,. a. : . . . .
                                                                                                                                                                                                                 ,m                           ..._._..:. m r.,-
                                                                                                                                                                                                                                                  ,             :,q_m              m ._. ..u . m . :</emW.w m.-                        _ a,:
wi.e                                                                                       '                                                                                 '
m.wu. l u.2,ii;
                                                                                                                                               . . :- ;...                 ...v% .                     ,         l w                                                         -                                                                                                                                                                                      ,824           ,,823 R
                                    ". 9
:                        ..                              ....                                                                                                       /
                                                                                                                            .l                                         ,                                    \ .-.. ,
      .                              -. y.
l                                                     .
l
: t. .-v.m=
A                                                         l             .
t .***.'.*s.S,                                                                                                                                                            .              .
i .. .
3                                                                     t*                                                                      .             .
                                       .           . .e. .                                                                         *.3                                                    .. s.bd.i4P.                      -~w l.
i
                                                                  .m. .n.q,w.  .
4_.  - g , . : .%s,:.1:=rne~.r e, , n.s
                                                                                                                                   . . , , . ._-   ,.- -_~
u,7. .a. res. .,u:.n.,
                                                                                                                                                                                                                       .                               -e.e ;,-y g ,3
                                       .z                             -
r                           ;,,.
                                                                              . - . .:;.3 .                                                                                                                - 4,l5.Ht
(..O  /                       ...r .7.s         2..)'2''S           _~..,,iiL-kn    .f                        F. .,SD.c.m, ^ .m                                                                                                                                                                                                                                      .
::'**,YZ!lll:C1.pH_ - ,_w--- f.-
m-                         . -_
5
;                                                                                                                                               g.;-                   _-       .-m                  n "" ~
* _ M,[.M.               .-                   e'                NM~MME=~.m.'-
w 3c,:,r.;.-   , ;- ~-                        " , =u k- L;
                                                                                                             ,. . - m .:. .y._1
                                                                                                                                       =_z 2 m' _.
n
                                                                                                                                                                                                             -_. _ =
                                                                                                                                                                                                                           .-=.-
s* ...,                   v.
                                                                                                                                                                   - -                                               ^ "
                                                                                                                                                                                            --*ha.-
* o:_%.g*T                                             .we                                                                  ,., . ,
l l,                                                                                                                   a
_b. s.f
                                                         . . . NI*D..I.T. '.
e t"                                       .__                      --

__                                                         .                                                                                                                                                                 .                               ~.
                                                                                                                                                                                                                                                                                       -w                                                                                                 .. d c.u.:
L..                         .,
                                   . wg                               ,              .
                                                                                                            .          ...:.~                                 wp.                          . -
                                                                                                                                                                                                                      . _ .g
                                                                                                                                                                                                                                                ~ ~ ~ - - - - - - ---- ----
                                                                                                                                                                                                                                                                                                                           . ;2;;                   c ' - w                          .4 g --:                          . - ;                                               _ _ _ . - .
p                     ,      , -
                                                 -- + - -                               z.-              . .          ,.. .                    m . .;,.g..
                                                                                                                                         . . . ....v. 3;
                                                                                                                                                                                                  ,. .. . i/
                                                                                                                                                                                                          ,                                                                       Technics 1 Rapc:: .62-61
                                                                                                                                                                                                                                                                                                                                                                                                     ~~'
W.           *               ..                                                   --?.{it* %.: .c.                          * *~ ,n,:    :%'s*'%Ci.            u.. ,l , e.a.r%'Wm:f.':.':
s, . ., @. .. , . .
                                                                                                               , ~ ,. t.w s, y.. .      .
                                                                                                         . 2-:.a.         ..
                                                                                                                                                      . . . s. . ...
r.e .a m.. .a
                                                                                                       . : o. ., . .
                                                                                                                                           . : .- . s /..e..m.. sw ...
,y                                                                                       .                      ..
                                                                                                                                   .-*~~ . ..:. ....,s..s.
   ..                                o                                                           .       .-, y;-                                                        e2..e,w      .           p...                  .y...
J3                                   I             .                        .            :WP ar-                                       .n .s; , ,.                                        rg.:.:-*:                        . '.
                                                              .=.i;;^.T.;-_'-w w                                                         .1*::n*.i.                 g.y;;;~ -fg ;
             ..                      t                                                                                     . .                                                                                      .a _r,i
  . , ~                                                       .4                                     .'~9."* '1%.; M s.                                                                                              '-
                                                                           ,'*V-. ' " h.c'e                                                                                                                   b .r:
    >                                                                                                                y . P.+-9 .;;nsi                                                      - - ,%                       -r -.                                                                                                                                                                                                     !
                                                                              .                                           ,-   :                       j.',,, . .
                                        '.                       ;,                                                                                       .                                                     .                                                             7826-7827
 '.'.
* M LO, p.5.;W-.FW~
                                                                                                                                                   %< pef,,/i: .GQ
                                                                                 .. . . . . ~4. ........~
m.- .:r.,.,,.
                                                                                                                  .s 4 ... , I g,:
       -                                                                                                                            $..  . ?@*.Gr     .      .,                                                       M-
                                                                                                                                                               .r'..,.:.::                        ,..M'::
V-t
                                        '-      9: .:>   7 - .
* l.s           .
i.*.2.        -. ".
                                                                                                                                * .Q.                       :e                      .       .,::
w-r..:^~.,.=-_a..._...-w
                                                                                                                                                                                                                                         -                                                          --~~:- .e . r. -.: ..:.c  ,.                   .
                                                                                                                                                                                                                                                                                                                                                           .w. , .ac.a3:?.       .
m.rse-
                                                                                                                                                                                                                                                                                                                                                                                                               ,:5
                                                                                                                                                     .v                                                              29.4            . .: PM2='2-D,.:9mjw-s . ..ere.< . ..r 3. sw                                                                rm-@.: n.):.w p 2
                                                                                                      /f'                                                                                 .
                                                                                                   ..w.. .-..qu. -.?lrg.m;;;,-N.
L :.                                                    1.                    :y,.9.::--                                                    =-M.                                      ..           .    ..             a r~.             m ,               w.~
:u                                    >.-
                                                                                                                                                                                                                                                                                                                                   . -a--e -
                                                                                                                                                                                                                                                                                                                                                                           -= , u.a..z.ye
       .:                                            -.t                       .                            ;. -. T<.,.m                  su       c~-      .2 . :                                         .
                                                                                                                                                                                                 . .' 5 v ., cc -                                   ,               -
                                                                                                                                                                                                                                                                                           --                  .- n.::,e: rmc. 2.e.                                                  - -
                                                                                                                                                                                                                                                                                                                                                                                               - :;. r.:n
                                                                                                                                                   ..R.. _~..,.-
3:. .?.          .f.y-          .~i G ;~.%.f,                                                                                                                               Q. , ..,a,2M                 .-:.r%y.:.:inw.w        ,h,M9. - M,. '.%%%#4;%
                                                                                                                                                                                              . w,. ., %..
      ?,.                                         .r.t                                              .
                                                                                                                                                   . s 6:,:                .-;r..5..:3.                                                                                           c .........
                                                                                       ..                                                                                                                                      .                     7                                                                                                 .                                                               ,,
                                                                                                                                                                                                                                                       -. w . . . ;m
                                                                                                                                                              -.c::e.n.. m. :.t...,                                                   .. r .-...
                                                                                                                                                                                                                                                                                                                       . ..n  . s.... ~.      :. . -- u. r. . . . m. , %.; .               . , . . .
_e.g. , .- -N. , W-;;:me.:-.:.:
                                                                                                                                              ...w-                                 w.s.g..                                                          a. &                         ,+ m:i, g -r. m.;                                 . ~ . p. w..a                    s;yc %w,.....        . #c- s..sm..
i                               -
q.
75 vtp...m' :'a ..-4',.
                                                                                                                                                                                                                                 .                                    WK-w                                                --         s         v        w             !       w          G      :. d e
                                                                                                                                                                        .j#t;                                 s.' 5 - ,:yass                             gr F.*                         .   ..         ].                r      .    ,.      .
                                                                        ' '..s&s s
                                                                                                   #. . *,:,:s,5l5 W ... % 4G'*.."". Q....R.ge %*:..onJ
                                                                                                                ,                                                                                                                                      g                                                                                                                                    ..
 ';                                                                                                                                                                                                4 :%:an_W.d. m0M
                                                                                                                                                                                                                                                                                                                      -                     ; . .s             --               , ~ ;..z. , u
                                                                              .~.tl -vr.84 de" C.r.as4.**.+.m, a.:&na :4.4 iys:.                                                                                                                       j                     l
                                                                                                                                                                                                                                                                                                                                 @           r
                                                                                                                                                                                                                                                                                                                                                  ., :4. -                           *'
I,                                                                                                                                                                                         ,"                                                 M I :Y["qen "',''.'
                                                                                                           '.P C.- '.. -(''
                                                                        ...,'M7
                                                                    . . . - ..            . , ..., . ., .. . . . . . . . . MstI3h.DD,.,N.                                                                                                                          -       .
                                                                                                                                                                                                                                                                                        ..7g2a .                                            . ..
:                             *                                            < t m.~-                                 .
                                                                                                                           ~ *. 4.                                          .%                    , ,8g.,.              . . 4r.                                                            yy                                   ,,,,               .*.                                          .
                                                                                                                                                                                                                                                                                                                                             , .
* Q (.. ..
                                                                                                           } *.s                                          i g           .; .                                                                                            ,
                                                                                                                                                                                                                                                                                                                                            ;r
                                                                                                                                                                                                                                                         .-a              :
a.... . rc.-                                     .s. ,c.., ; .
                                                                        .            ..u              . s. - .. y.                                                                                  ..         ,...      .. -                                                                                                                            -
i                       .                                         6                        .....
                                                                 ..:4, u ,w.: .., *:...,                                                        .; ,..Q,.;c,
                                                                                                                                                                                 . p . : .. :..                                                                                               .;.
                                                                                                                                                                                                                                                                                                                                                   ..2...-
                                                                                                                                                                            ..              . q . ;. .--
                                                                        .-..?~ --::h.:4               - - ., =. r. . .LR. .,E.
                                                                                                                                                                                                     .i::                                                                 -
                                                                                                                                                                                                                                                                                                 . ;. .                                                                               . t.
y_-            _.- .. , ,, .
                                                                                                                                                                                                                                                                                                                                ,         t, J.;. g i .. .. g. . _.
                                                                                                                                                                                                                                                                                                                                            ,...~.
msg
                                                . . . . . , m_ , wm ,y                     - _-                                                                                      m                                                    -
                                                                                                                                                                                                                                                                                                  .                        .-m. e             . .
7 t
3                                                                                                                    S
                                             ?e.:w:.,i._.p% evy-:.=ypeuru!upuspa.sR.%.
if                                                                                                                                                                                                                                                                                                                                                                      u&
f *.:: i. W. L
                                            .: . . %;:~.'.W,                                                         :=r :.y .gg' '~~ R-M                                                                                                                                 i.
b.
9 w E'-a.>                                                                                                                                                                                                                                  m                           .~
                                                                                                                                                                                                   =m c                                                              ,
                                                                                                                               .. . c ,                                                                                                        ,         3.,:                                                                   n                                 . .                                       . ,...,a.s
                                                      .4 .,,a.:n,~                                               .p;g,,                            qwy"                                  ~,          _.           ~              .       .  ,=_Q.
n
_            .-                                                    -. x- --                                                                              . ..m  .
                                                                                                                                    .-                                                                 ~-- -e_is,k m =%_ . _..
w~_L.
                                                                                                                                                                                                                                                                                   .:   r. . :.-..~.,..~.
                                                                                                                                                                                                                                                                                                 . a ;1 ._em
_.7          w_,..                      ._ :. ,
                                                                                                                                                                                                                                                                                                                                                                                                      -p._ .n
                                                                                                                     . , - . y.._..--
                                                                         -_..,w--                                                                       .   . . ~                                                      .-
                                                                                                                                                                                                                                                                                                                                                                               . 4.,,.
                                              ., .:,                                                                 .                                                      ___--s.                                                --
y                                                    .
:                                  V                 w A-*= "-m-J.w                                                                                                                                                                              c,u 2,w).;s ,4:pe;.; :g;.,4g.6, g,                                                    .
5
                            ,              Wp%. .- - --                                                           .r''q p;                                              MrTmiyg4,,,, ,.,.,,y ,, g, E m_o-..g, '. ,. v. j,;*.;g _
                                           , ,Q.                                                      .              .                                                                                  y                                                  2 .ci      ..p,4v.b.els.:e .v.. . . ..t.w-                  . .... p .e                           t
                                                                                                                                                                                                                                                                                                                                                                                     .,. '.sh...
d....
                                                                                                                                                                                                                                                         ,;y?          . .ee ww.e      --, i u.   , :.g..
e :.aem.4ren*.M:W.i.c.,a.yc   '. . . M...                         ,ag;q       %%g,;
                                                                                                                                                                                                                                                                                                                                                                                    ,.,,s*,a.,,.. J: r'; ,,su
                                           >.                . ..e                                 .-                                                                                                                                                           e                                          , -. : s;e.ia-a
                                                                                                                                                                                                                                                                                                                                                                .                                                ,., .g P                                           .. - c g
                                                                 , ass s .e
                                                                                                                                                                                                                                                         ' g d e . ti pf.. y-% .. .
                                                                                                                                                                                                                                                         .sg:. :; - . - -4.g ;,x,. g ,;..p.;
g g,s..,,
                                                                                                                                                                                                                                                                                                                                                                                                      .,z, g.
yaC_.
                                            .                                                                                                                                                                                                                                                                                                                      , c; ,_
: : z , .. .'.w. ''
                                                     .n ,gi l
                                                ?* 04 /        5 (ur [ <                                                                                                          I i                             L-. ;4i.k,2.*.*.$$
Q                     =.g                  ._.e  MFi* g     .
9     <y y~_
c.~s
_        ,s@m:.        $hW*y'#i.'jir  -9
                                                                                                                                                                                                                                                                                                                                                                     . .:: .- .x.%Sq.5ih            ..::,., ug.-m o, ,.. sy                                                                                                         ...y..                             . , -                                                                            -* .                                                               _ .                     t          -                                 --
                                             -                                         }* 3O .,,,                                                                         *
* r L , e.
                                                                                      . . s.           .                            ,                               :a~m     ...       . , =. 6.v;..
:%~                                                    .                              1                                   .
                                             ;.-p c
:.z- a..-
                                                                                                                                                                                                     . O-7828-7829 R
                                             ,. . ]                                                .
l s
L.<A.$
                                             .. ;+n g 6
* a
                                             .. m .                                                                                 I
                                                .ce a dr.
                                                                                                                                  .,.s. s. ..                 -                            -
w
                                                              < *.V't@@&%ilf.'W*,@..                                                                                                  g:a.n,;gfsg'{fp                                                             7825-7829 w.,t,,                ,.
                                                                                                                                                                                                                                       ,s.. _     _
                                                                                                                                                                  ***":m
,                                                               .              , , , - = _ - _ --. r
                                                                     ,, .,y                                                 *                                                                                                .
                                                                                *                                                     .     .m'
* S*..1t 7.*:4.(:./g Y-                           *
                                                    . .I*
; . (',,. )
                ,,                                         c., icy's- h:.. ..                                                                                         -
                                                                                                                                                                                       '.-.x h." &__ h 2                                                                                                                                                                                                                5,
_m_._ D_ --
     -                                          . ' *, g,,g=66*'.de                                        aw%5      t_=.N m                                 - e;- T_-
                                                                                                                                     .y --- - ~ = ; -m,8WA- --~
                                               . ;lgy;.jg: ;.;2
                                               , . '                              w-
                                                                                               .              _ _ - , - .                          3 -                             _
                                                                                                                                                                                                 .n s.cy.x - -
_               .~
N
                                                                      .. a #.                                     r _r            w,,,'.----
                            - .           .                - , . , . - - . . . , . - - . _ . - - . -                                 . , - , _ . _                          , , _ _ _ , , .              .,m.                   . - . . . . . , _ _ _ _ _ , _ _ _ . , , , , , , _ ,                                                                         , _ _ _ . _ _ , ,                                     , _ _ ,

  '         c o        ; "                 .,                   . ,                    ~..                      -                                                                            s                                        ,. . c                               .
:.. k.
e         cn,:. ;*, a .e                                             ..,.::....w.o w                                  ;
                                                                                                                                                                                                                                                                                                                                                                                                                                                   ]
    .-                                                                                        s                       .i.                                                                                _.'                                         .
                                                                                                                                                                                                                                                                                                   ..a..:..-     -
4          .. . . , . ,          . , - :                                     . u.n ,.r.o.,                                   w.rt w.-                                                                                                                                                              7 s ::ce; o ,. g . m .u ,. g p
                                                                                                                                                                                                                                                                                                          **~#MWO S h.d.i.is                                                                                                                                                     ''""* *
* G-                                                                                                                                                                                                                                 O 3.D~E.                               . . ,. di4GG              ;l:.2.:;ffo.c.$GM*MGEs7-**q--a            Y
                                                                                                - -.-Ge>WBNM?*d. **1~".-                                                                                                                                                                  " M E m.::                M ::W                     .w21.3                     1~ s::-          M CdR' W
  ..<. . r,.n.; . :r-.....h.
M.L.g.               .gg. . .. ..
                                                                           %- ,,- --. .y 2_ .,.,r         __--- -
m . w = - ~ _ ~ - - + .                                                                                                               _ ~                         .,. mx                                                                                _. -                    -
a   ,
    .M. r :;.n .                              . . .: :.s... .-%%.,;xq.;. 7,g ,.M.W.=.!QW. c;.r;;,:l2.
                                                                                                                                                                                                                                                                   ._ , '-?.::e.rs%,,,,
l
                                                                                                                                                                                                                                                         ,y._g%g;m.,W:.:-;.i:.                                                                  = k3-, .: 4_fa.t.y                                                z.7%. 2
  . -- - W.- ~ m .:~. .. ..                                          . ;                   .,                                a                . , , .                             ..                    : ;._n                                                                                            _._m --.,;                                                                 ..
w    =r
                                                                                                                                                                                                                                                                                                                                                                                                    ;cm.4y-                                        ,
                                               %.r.2                 g.         r;     =gtp-                    -    .     ..       .rm-                 ,a-g,--y3                                ys;:ep.e.gg                                              .:.:rw.                      w.rg,r2a                        #.          3..=,ese.                                  .:s m      ,_.?-_;_,                                                I t, T. .w.g, ,,           e,3 : , . . ' - _ - - -                                                                                                                   . -                                                                 - -                                    _.                  ._ a .- -                                                                                >  . _   _   , r.                      ,
y .2,.u,m.. , y. -..                     g.      g    ,'*2.:"*               7.         =---=m                    .=c                  m                   -r.a.
_3            p            ~--                       ._
: w. . e-. _-#.           .                   ..
m..,,.                     ,.~:s.                       m       _    %          _--_;                   om_q
_         s.
                                                                                                                                                                                                                                                                     = - , .                                                  .. .                              ,_.                      m._._                          _
J
  *e
                                                                                                                                                                                                                                                                                      -                                                                                                                                                            I
: i.                                                                                                                                                                                                                                                                                                                                                                                                                                              ,
                                                               ... V..._I.if?'*';                                                                                                                                  .%
                                                                 ~
p                                                             d.T M m$ -.--';e.n~                                             _.                                                           Technical Report 462-81                                                                                                                                      l
                                                                                                                     ,hs'.:nyn.r,m.
                                                                                                                                                                                                                                                                                                                                                                                                                                   ,1
                                                   - ; .;,'.,ypi.i..:F.w'.e~        ;g.:-::en Wk                                                              %,                                   ~.                                                                                                                                                                                                                                              l
     !                                                                                                                                                                                         U                                        ::3 e.,m-r.;                                      :c.;c.                      M;iYi'.M'.:S p:.r-~
h-!!%.th.Q.Q.                                                                               5fMQ.-3:.                                                                  dme              -4 a .'2f- .- .cer.w::
                                                           . > w %:e..~no..m. w w.               .                                          3.,. . %            ..-. m. ..m".g..:
                                                                                                                             .       e          .        w             .=.                                         -
5:4
                                                              " d ? #." ?.+y;>- )lip,.> n.~.g.? e
                                                  - - .&.e-                                      ;- :--; ;m:::                                                                                                   ;m:                                                                           .
:sim Ita=                Mp                                                                   ..
                                               '.*Mkd .'. , ,,**m.s.:':.mm.l:-
5 : .: .' ,= ai W ws %                                ...=-- ,;;;,gly=J                               e
                                          ' -'1                ,       &           *.         4                                                !        -:s:c$.                                 %l,                   &
  $                                                     4%                                                                                               .$5l-tyb'W
     ':                                    [ . i, .*k"*'tg ..'Mli6Jf.i                                                 .r     4 -}:,;"'*.)r,,,gus.:
W
* 2h             '7,,j %. ,                                                                  7826-7827
                                                                                                                                                                                                                      , c4 p                .:        .,w.--
:                                                 -g O. -.                                                                              >                                                          . -          a
: v. . R:..s.                                c:~::                                        Lw. . -g . ;: sn.,,,
:. w,
                                                               .. ..:                    W y,,>.e                     .t.:                      ..s..s.
                                           .. ..b.s.
                                                     . a.; .S..~..r.e-v.,f.,.a...t. w-                                                          't ,<., -f;_:,Wm.:.
Ro.,.n.       ... p:-
                                                       .y . .                                                                                                           . .                                                                                                                                                                                                                                          __
r:n
                                                                                                                                                 .r. ,.,g -*                                                                                                                                                                                                      aedr - -.                              ~ ~ =- -
                                              ' ..Y.:).'i.             . .:N
                                                                     ~---.
                                                                                         ..W:.n           .*.?.4.-:.:.'<.:.:.:j                                                                                       W,;.=. Wf.i;ms
                                                                                                                               ..                 :.. . .e-..,' %. w.>                        .
: w.           -
aug=m:,:L"':    m i
W'ne'.PJaM:                                                   . m.,.
                                                                                    -':(                                        . :5 "*. . O'''.;i5.&*$
V                                =Ma;',,;. . = -WE
                                                                                                                                                                                   =:w                               diR %&p$*&5' 5$a'm:'   sm,,,V*        m.
                                                                                                                                                                                                                                                                                                                                                                *W;;L.%                  W     wkwm
:g.                    .          .
     *                                         ..-a
                                                                .0.:r.,m=:c.-@             --:-  '-
                                                                                                                     )~. .         ..-   :.s.:m<f .%,,,,u. L.'.,q;,j.,                                      ,. o-
                                                                                                                                                                                                                         .i           .                   -y  -                                         .
p.r .. n
                                                                                                                                                                                                                                                                                                                                                                                        .W       -.
: --------a ^:-%- ::: -^-..- , - - - -
                                                                           .=w s    ,                                                  W -~~-_ m _'_a.                                           ~d             s.~                                       7.'Un . : :. ? '_~;-:: .;:n -,. .
                                                                  .'.',p. n C <.~.-r %.
g%...,r,~.
u ~.                ;__ r m_                                                                                          g 2. , - -
                                                                                                                                                                                                                                                                                                                           ----:g,,%"*.*.*.*--                                                                           - - - -
[, -
     .,                                                  .-                                                               4                   4.#                - ---
e.
g g.
3 w          -
72 .W
                                                              -.s,,-                                                       e.rm,                        :y. g_ _ _ _ . _ . .                                                                               gss i                                                      ..     .;                                ,E.;
                                                                                                                                                                                                                                                                                                                                                                                , .,f.T"S.- -S. 1 s
                                                                                       .e:=ir.h.jt.e. ne+*er,e.4,.                                                                                           ,sene_,ge..igsgowfu w :. m- i l,..                                                                           2   ..
                                                                                                                                                                                                  ...e.w
                                                                                   +m                                                                                                                                                          .
c: . .c.;.r
                                                                 .r. ..,w
                                                                                                                                                                                                                                                                                         .                                   .                                            .                       .               s
                                                                                                               -~~.,
                                                           .                                                                                                                                                          .                                                 \
      .                                                . s . . . :.                                                                                                           c                                                                                                    h .-                                    . ::.                                                                 .~ w.
g . >fn&,.,.:                                                   .,,p...                          - . g;           .. .ny-
                                                                                                                                                                                                                   .                                       1 w vT.u.@LTr                                                                                          - -.:.,                                 s.&qg.my 1
I n''.7ca -                                                                          y..v7e              . og . . . ,
ng                           '
                                                                                                                                                                                        .v . ~ . . w*
                                                                   .              .,.: .                                                                                                           s                                                                                       . .
                                                                           .            .,...._.,....:.m.....-
a . .... ...w .; n e m. m..                                                                          ... .. - .w                                 ..a                                  M. M rnt. ..                                                 ,
                                                                                                                                                                                                                                                                                                                         . ..                                       =                                   .
                                                                       ..:..r-      .# . .                                   o               m-n.g;...g                                                  -y..                         ~
pig         l
                                                                                                                                                                                                                                                                                           .            ..                      :. .                  1         7 .. ; : .; . .
                                                                                                                                                                                                                                                                                                                                                                                            ;. .           .a. .,,.,b l
                                                                                                                                                                                                             .c . . -                                                                                     --
                                                                                                                                                                                                                                                                                                                    ..m                                                     g w.,:::                                                           i
                                                                       .z. . a -m . u...4..:..;p                                             .n.,. g 2 a. --                                                                                                      q, , ..e.
                                   .                                                                                                                                    -- -                                                                                            ll ,.                          . . . . . .?.                  .                       , . . . .
n*...,                                  . . . ,
J                                                                                                                  .                .
oc@_
                                                                                         . __ . --m            ,y_ 'st.-
                                                                                                                                                                                 .m_
                                                                                                                                                                                        - r c g2        . 4: m.
l            h .                                                                                                       .    * . **             I s
j
                                                               . .                 .@i yo                                  r-3 _ C ._-_                       ..- ;,~ - 7= NA                                                                                               ,
                                                                    * '*M'%*'??                                                                                                                                                                                   ~%                                                                                                                           ' .':..'                       ''
N'*s".'''..              . m 'O'*.5MllIlicSCWU?,*.M 7                    a.o =
                                                             . ,[,:, .. ,,' r . ,
J. $l.z.mm... ipr;=rFM'#* -
                                                                                                                                                                                                                                        .+   -
[
E:ib , .i. 1,6. s.[.
i y
                                                                                                                                                                                                                                                                                                                        -[{., ., y..:                                    : ~'W' '- * -- . ' . . ~
                                                                                                                                                                                                                                                                                                                                                              \ .,*.,,$. * . * *. ,,,, , ,
* Atf$%$:*w.e"tM.!.S                                                        -.X ' '", _m
                                                                                                                                                                                                       ^ .. .                                                                                                                                                ,
                                                     . ' r','.
_ p. - -24$34'Y                                                                                                                                                                                                                 A
                                                                                                                                                                --_-r- ~ M                                                                         i              .u k<. -w. -w* '' i V , -     __                              .. .
: 1. ; - ev._tssg,,;
(,.:j:f     r q;# . ;m ap.ss---m-e
                                                                           '                                                   - a .'.;e me"---,-C                                                                          .             e        t                        -w. :-r w ,                                                                                        - . . -
M.*g4m.y -- -
                                                                         ..                                                                                                                                                                                   3
                                                                                                                                                  ~                                --
                                                                                                                                                                                                                                                    ',                           _E                       , - _
                                                                                                                                                                                                                                                                                                                                                                    *n # %(c                          -;
T **.dY                                                                                                                                                                                            (         'D'*"-
M.anr{                                                                                         h-~---"
h..                                     . ,,,,
                                                                                                                                                                .h.            d=
f''                                  ''h          ....'".p                                                               W**%'
c,               ' f =,-_.YW "Mik I
g, l
(g W r,:.~ s.                                                                        +-                                                                                                                         ,.       Acn f>p, .2d.ss                       d                                    dipgu
                                                                                                                                                                                                                                                                                                                                     ,sa~s:ist',g., 3ymm-                                        .,$.s 6.
m                                        -
:                                         ,                                               ''r-uw                                                   s.:n.ws,ueMame,-w                                                                     f. ',q_;.,ji$,          -a44
                                                                                                                                                                                                                                                                                                                                                                                                                                        - '.i W.qese :..v 7.w/.r.., ,q                                                               a             .     :;     .         eer          -
                                                  "mo9 gys                                                                                                                                  .: .
th1it d                                                                                                     Of                                                                                              $48'E4G$MEMiNE45"E,w,O TN M                                                   "
A I                                              h                      .b                                                                           '
h.hh:dk$N:h*Nk:U ;$55'A'SM                                                                                           -
                                                 '.8<
                                                 ,::.4 y-FAnd 7*
l l
                                                                                                                                                                      ~..
                                                   .                                                                            J                                                             ..                         .
l                         ,
D>                                       W
                                                                                         . n.
r.
                                                                                                                                                                       . 'l' ' *; ,.,
                                                                                                                                                                                                       ?-
i                                                            7828-7829 R
                                                              .)'
                                                                                      .?.e                                                                  ,..   ;.               ...*.s i                       i
                                                                                                                                                                                                                                                                                                                                                                                                                                   .b
                                                  ' y.~w                                ..~..                                                                                      ...,.e,      .
A..
                                                                                                                                                                        ,e*:..
t.i .1                         **. s.em            .
                                                                                                                                                                                                       . .. s . l l                                                 At. sat-                                                                                                                       .                          ..                                           l l                                                 Nr..y                               3 ., ,:.,.                                                          . . ., ,. : r. e. . -                                                                          i
                                                                                      ...a.
t .
                                                                                                               > ..                                            ...,*s                 , n. a.
c i
r s.
                                                        . . ,* 2 I
_ sm
                                                                                                                                                                                   - ..                          .j            i
                                                                 . . . i.s. >,y,.,y.. p..                                                                                        u 9 x.a Ma. 't_                                                                       7825-78"9
                                                                                                                                     . , _. . .y                          .

  .+ " 3; , . . ,,_                                                                                                                     ._      ,            ,_                       l
: '. . - J, ~ l
:. c
                                                                                                                       , ' k..,
                                                                               . c : W ?y; ?..yj.e                                         ... e v , . .:.,:               ;
g.y ".6 ca ':o.:p .%45... &T m.'.n.     .                                                                                    _
TII-4201 06/22/84
                 'A11eastion No. 7 NCR No. C83-01986 discusses the cracking and flaking of concrete coatings systems (NUTEC 11, 115, 1201). The disposition section of this NCR states "crading of coatings is due to excessive stresses in the coating during drying and curing."
The allegation is that repairing these cracks will not remedy the condition which caused the cracks.                                                                                                                                                 n Evaluation of Validity The allegation as stated is true. The preventive measure to preclude recurrence of this condition is the proper application of the coating with emphasis on control of film thickness (see manufacturer's application bulletin attached).
Raquirements for control of the thickness of concrete coatings are included in procedures QI-QP-11.4-10, QI-QP-11.4-27 and CCP-40. If the coating is
                                                                                                 ~
inadvertently applied too thick and cracks, the inspection process notes the                                                                                      i problem and corrective action, i.e., rework of affected area, is taken.
Safety Sianificance None Generic Isolications on other Systems or Contractors i
Not applicable
                  . . - . . - - ,       _   . _ , ..-., ;._---,-~~_...~.~...,.--._-,._--..,,.~.--.__,,,,-. . - - - - -                                                      m.-.-

r (l$. i'{5O+,.?:.w l                 id:u&y:' '. silllllnk$zj.Mi?;lk.Q
                                                        ]                          g. $ Q '..2 W L.*fQ.'n'l' y ;;'..');
4 :..         z - w .~ : -            . .: a     . _ -                ..      .
            -        a                                                          ,
g_~ .. J , .                                         v                                      9 9
J*
[''_,.
                                                                                                               '"''88'"^'*^"""*
7.0 ao .w? New cemans tousana 701as u.s.A. 504 254.t 33       HEME 7
h January 19, 1983                    .
                                                                                                                                           /
NUTEC SYSTEM - FII.M THICKNESS CCNTROI.S r
i.

==Dear Customer:==
     }.
This application bulletin has been prepared as a reminder that stress cracking
:                 is possible within the Nutec 11S system if application parameters, specifically;
     ;                 film thickness, copcoat times, and thinning are not controlled.' Cracking.            '
observad to date, has been restricted to floor areas where film thicknesses
     ;                 have dramatically exceeded the reconenended tolerances. The problem is inherently difficult to detect because of the problems of accurately measuring the applied thickness of a coating on concrete. Routine wet film or dry film measuring
     ;,                cachniques do not work on concrete. On valls,the problem is not acute because                                     .
the coating vill slung or sag, revealing the excess very readily.                                                        ,
A. Two sites had' experienced minor stress cracks on floors, especially at
     .j ,m,y'                     the wall floor interface where the cornors were covered with Nutec 115.
      ;b                          Both sites recognized the lack of control on film thickness and took
:                           steps to monitor film thickness, recost times, and thinning. No j,
further occurrences have been reported.
* Numerous sites have used the Nutoc system and no cases of stress cracking have been reported to Imperial from Comanche Peak.. South Texas Project,
      ;                           Riverbend, WPPS) 1. WPPSS 3. Hopeereek, Millstone, Beaver Valler, and Shenton liarris. In addition, no cracking has been reported from the
      ;                           many non nuclear applications in which Nutec 11S has been applied.
    -I :                     B. The following is a review of application conditions which appear in Imperial's application procedures distributed to each nuclear jobsite prior to start up apinting with Nutec system.
      *l
       .I              1. Film Thickness O.,
Recommended film thickness are as follows
                  .                       1.avel 1                10-35 mils k                                  Lavel 2 & E0P           10-60 mils I:
l !. ,'y                                                                                                                              .,
        . s-4 e
n

                                ~.-
 ' y            .,e-
                    ! ~r 2        a
                                           ~
                                                         ,, f.:.1 sa        *
                                                                               - . :3. . v - ~ .
                                                                              ;,- Q v             , 4. ,., .y . y _;.,,           . ,; .
                                                                                                                                                 . .Q ., z_ ;, .y, ?.. s q.[ _
                                  ...                .w    - -            ,
                                                                                  .. --              :.... w .        ..           ..--.. .... .
           =           . "    .
p                                                          &
   '''                      2 .- Patching Voids                                                                                                                               '
Nutec 115 has been recommended for patching voida below the plane of the 1 .Qi.<.1                    surf ace (i.e., busholes) measuring \" in depth and diameter. Larger
    ;,                           voids up to 1" inch depth and 2" in diameter may be filled, but usually require at least two passes to prevent sagging. In any case, ptior to copcoating, these void areas should be cured to the extent that a fingernail                                                                   j impression can not be left in the surface.
Note: Nutec 11S is not recommended for leveling out undulating or very rough concrete. In cases where concrete has a very rough profile due to blasting or bush hammering, the film thickness restrictions outlined above must be observed.
l
     ..                     3. Topeone Times
     .j                          Attached are a table and graphs which outline the cure times recommended j'                          for various film thicknesses. Thicknesses above 35 mils require additional Stresa cracks may occur within the Nutec 115 if the topcoat 14
     ;                           cure tius.
:                           applied before the Nutec 115 his an opportunity to suf ficiently* cure through.
Application of the topcoat, before the recommended cure time has been achieved, may entrap solvent within the film, especially if the 115 has been applied
* at thicknesses above 35 mils. One can easily appreciate that a combination of a high film thicknees and inadequate cure followed by the subsequent
      ,'                         " swell" caused by introduction of the solvents in the topcoat must subsequently
      .                          be replaced by shrinkage uhich may result in stress cracks.
      'N
           ' O              4. Thinning
       !                         Haximum thinning with DL-54 solvent is 51 by volume.
j                     In summary, the cracking problema can be avoided by following the 1special
:                     application instructions, for the Nutec concrete coating system, which are present at all jobsites. Particular attention should be paid to the application
    <,                      parameters outlined above. On those projecta uhere the parameters listed above are carefully controlled, there is .no probles with cracking.
Should you have any questions concerning the topic or for names and addresses of references, please do not hesitate to contact um at (504) 254-1433.
I      ;
       -                                                                                                                      Si,ncerely.
                                                                                                                    / Ce                     Nd Nutec Product Manager
        .* s_-                                                                                                                                                                    .b.
       ?.
G r                              -
l

                                                           -                _- -         .       ~ .                             -                    --         -                       .. -                                    . . -
                   ..,,.t,       .L.          ;.
                                                                                                                                                                              . ..                       _                 , , . q,,; ,,,,e g
                                                                                                                                         ,gg. . : a ; qm.~v, , . 33,.., . .
                                                                                                                  ,,3. . ; .py.p p ...                                                                    .p,. . .g,;;. .;,g
          , _ .   ..          n, u 1.'     . s. n . ,       . c.a , :y y;:. .                                  ..                                                    .                       .
                                            -s                                                          .
                                                                                                                  ._.         .          :.: -    . . _ -          ....._..i. .. .a ..
     ". I.
g , .'                  r                                                    .        s.
     ..**                   +   .        .
       '1                s'                                                                    w f.g; ATTACMMEtrt                 "A" 2.1                                                                                                                                                                                       .
       *.,1. n , . y                                   ,
     .''h .
* HUTIC              NUTEC              NUTEC                 NUTEC           DURA 7.INC AQUATEX                             REACTIC
                                                                           #6               910                                                       8555             s1180
      'J.                                                                                                      811                    tils                                             .
t1201 /
PCT I,I2T 50*r               12 hrs             1 hrs             1 hrs                 1\ hrs          12 hrs           .N/A                                16 hrs 70*r                 S hrs            1 hr               1 hr                   1 hr            a hrs            N/A                                   8 hrs
.                                                     90*T                 4 hrs                hr             \ hr                       hr          6 hrs            N/A                                   5 hrs I1733CTIO:I
* TI'w~'~'              o
               .                                           r            N/A                N/A               N/A                   N/A             N/A                 N/A                              45 min.
50,F N/A                             N/A               N/A                                                                                        20 min.
N/A             N/A                 N/A 70,F.
90                N/A                N/A               N/A                   N/A             N/A                                                  10 min.
N,/A
           ~'
           .                    ArccAT OR o
 ,         ..                   TCPCcAT 50 r. 48 hrs                                       24 hrs             72 hrs               72 hrs           72 hrs             24-36 hrs                        7-9 hrs TI.C                  70 F. 12 hrs                         4-6 hrs            24 hrs               24 hrs           24 hrs             6-8 hrs                          4-6 hrs
               ',                                     90*T. 6 h'rs                          3 hrs             18 hrs               18 hrs           18 hrs             4-6 hrs                      '2-3 hrs''
.              ;,O                                                                                                                                                                                                                   -
           ..' # 2*iEI. CURE                                           .
f,                    TIME                  50 r               14 dys            72 hrs
* 10 dys               10 dys           72 hrs             72 hrs                           10 dys 70*r                 7 dys           24 hrs              7 dys                  7 dys         24 hrs             24 hrs                                7 dys
               -                            .         90 r.                4 dys           la hrs              6 dys                  6 dys         18 hrs             18 hrs                                6 dys
:              6 4
k Full cure.t. Lee should be used to desarmine t.ime allowed between
,                                                          coating and use of forms coated with #10                                                                         *
             ,                                        Addi:ional curing time shall be allowed for filr. thicknessesi
              ,                                                                          Ort                                           Additional curine Time                   ,
10 - 35                                                             0 115                          .         .            35 - 50                                                          24 hours                     -
             .                                                                                 50                                                      72 hours
                   ,> fs                                                               3 - 10                                                             0 L-             11                                                                                                                . 24 hcurs 10 - 20                                                                                      ,.                                               .. y
           .                                                             k

                                                                                                                                                                                                    .                                                                                                                                                                                t"
        . . . .                  -.                                                                                                                                     .                               .                                                                                                                     g NNV N                                           S..S         .i
   .           _ _ .                           . .                                               .                                                                                     .             ..              .                                                                                                         n          . . .
          .a O.
og s          =                                               .                  . _ ...
t                   ..
   \_.=l.6
   \ .g g %.}
                        . _o 4 .1.
K                                 ._
                   .$  a.. f.                                                                                                                                           .
G.                                       .                                           .                                                       .
N.. .                                                                                                                                                                      :.}. .
N.     ...              . . . .                                                                                      ..                   .                  .                                               -
: o.                       ._
                                                                                                                                                                  ..9                             .            .. .                                ..                                                                         g                .
                                       -._.9._...w                        .                                                                                         . .                      . _                         .                           ..
_.                   .g                                                    ..
                                                                                                                                                               .....1..._.
L
_ _                                        . _..w      d.    ...
g                                                         .
_ .. ....._......g
                                                             . ..                 L.. .-... __. -.                                                        .                            .              _ . . . .                                                   . . .
: d. . . _ g ..
g
                                                                                                                                                                                                                                                  . p......
:r ... 1 13.#
p         .
3 W-                                                                                      *e.
_l                   . . (. r $~o r - -                           -u
                                                                                                                                                                                                                                                                                                                            .c L          _ .g
                                                                                                                                                                                                                                                                                                                                                        .v
                                                                                                                                                                                                                             . - . . 2. w 4. u
                                                                                                                                                                                                                                                       .g.g.e                              4.o          u                               ...
       . . . .                            . . . _ . . _ _ . . _ _                                                              .            .                                           .           .. _                                     ..                                                                                                             g
                                                                                                                                                                                                                             . 1.. . a.ll3..            . w      . -.. p,     es. -eg             wp                                         . . .
d                    -
Ia                                                                  -                                                                                                                                                                                                                                                                     .
P
_ ... ._ c _.. 4w .Wsl1. w
                                                                                                                                                                                                                     ._                .                                    .                           6 G M0              'r W V
     ._ m o...                                                  .
                                                                                                                                                                                                                                              .._ m                                     g.                              ,
o
                                                                                                                                                                                                                                                                                                                             'd.
y s
     ,,. . g . .. _ . .
     .y .. s*
      ,.w.
f3 . to. .
                                                                                                                                                                ..~.                        .
                                                                                                                                                                                                ..                       ..                 .. . . .                                                                                         .. .       .[
7.,
: f. . = . . ..                                                               . . . .                            . .. . ._
k-                ,,
e.
             ,.y         .                    .                                                   .
L. .                             _                                                          _                  . _.                          .                     .                                             g.              _. .                          ;
I 5                                                .
                         .g            .
                                                                                         . .                        . la.             .                       . . . _                                                                         .                      .                                                s i
I
      ;                                    _. .. ..                                     ...,,.g                                                        . . _ .                                                                                             ..                                                                           .                                         .
      ,       .T.....
j
                                                                                                                 .3                   ..                    ...
l f                                                                                                                                                                                                                                                        .                                                                        .
                                                                                                  ..y                  jq
      ,la=,.
                                                                                                                                                                                                     ...p                                                .
                                                                                                                                                                                                                                                                                                                          .o yy . ..                                                                ..+.                        ,.                              . .. .                                                             s                . . . _ .                                 .
P yb                                                          -
                                                                                                                                                                                       %g{t,.              $                                                                                                                                                                   .
g 6 .5'                                                                                k 5. ."'/                                                                                                       l
:                                                                                                                               ~.                                *a cg H. b                                                                                        w %.
Wg E                                                   ,
                                                                                                                                                                      .                                       .h                                 .
s o           .
                 .l.             .
e                                             y                                                 a4                                          ,,                                      '">=.                                       g                                        I'"}%.
                                                                                                                                                                                                                                                                                                                                                                 . d" '.                ,
                                   "'l>                                                                                                                                                                                                                                     '"1                                                                              .
: q.                                              1%                                           ':P=
                                     "l>
s                                           Q                                                                                               -
(
SD M                                                                                                                                                        .                    .
                                                                                                                                                                                                                                                                                                                                                           . . - 1.!            p>:
m..-                                                                .
                                     .                                                                          3                      ..... . .t.v =4 y u. a w n                                                                            . . . . _ . . . . _ .                                              .             ...._...
i.
                                                                                                                                                  ...g          _          ..e         a-*      -*              .m w
                                                                                                                                                                                                                                                            ~~                - --                        ~.a=*-**             **-"*~.*

y
                                                                                                                                                                                                                                                                                                                    ./
:                                                                                                                                 +
: i i g i s . .f : :                                             . . - i              .:yi                                         l:                                                    !                          .'
O. '33.F ; .: j              l:     :     i                                                                                                                    T h,                           .         .                           . . .
1.'.
                                                                                                         . :.        l*!: R. ; L*ml "TmcwAEss                                                                       .. .
i               .               ;I , .i.                              .
g
[
: ;,,1
                                                                                                                                                                                             ~g lI                ,.           .'.'.;''                                                                                                           'i:.
                                                                                                                                                                                                                 .. . i. il.!.:i ! l . , l.. . '
8        .: .
l!:1.-
l:..         ..                  l..l i , g.i ACTEC:                                          .   ..
l                              .
REco mms.              ..
tosh ;.                             i         o lI
                                                                                         . .... i i                                                         S. ,                                                          ..                                                                                                                                            .
                             .../                                                         ..                                    .
: m. gggm ,
                                                                                                                                                                    ,I                    .i                                                                        l,          -
                              ,. ..                                         .                                            !                  ..                .            i,.I l
I..!:
i 1:la1:
                                                                                                                                                                                                                                      .s                     .i :..
                                                                                                                                                                                                                                                                             /
: ;i. ... :ill
               .             .,i' ii                     .        .I ;
                                                                                                                                        .!                    e e            i              ..
Il.i.i.l :slg3.*l                              :                             p;. g,ggg,,
wTmsama        e                                                ,.
                                                                                                                                         ! . . ., .l. ,..*
8:
:-           *:t:                                                                                                                                             l                                                                                                ;,
                                                                                                                                                                                                                                        ...i.I
                                    .g                                                   .. ;.t          ..           i. ,                                                                .l.                     :::li               .,                               :.                                                                                               ,,
: t.                            .        ..                                ...                                                                                  .                        .
i.
j
                              -             .                                                            i .          .: ;                                    i                ..                                 .?-                                   **:                                                .
:.                                                     g li.g,.!.:g 3;
g .i .          , ,..
                                                                                                                         ,,11.g.
g l .t,               .
                                                                                                                                                                                                           . ...;.                    . g l g , ,g
                                                                                                                                                                                                                                              .:. ..                                                    i                                                               o i*                        .. ...                                        .                                   .
ll
                                                                                                                                                                                                                                                                                                                                                                        '}
                                                                                                                                                               ..s.
                                                                             -                                                                                                                      6                     .                   1
    ,                         - .j                                                                  ,    ,. .            -e.i, fje            ,             .
1               . .                          .. ..                         , . . .,.,.                          (, . .-[ r. --- .  .
                                                                                                                                                                                                                                      .,ig.:.                .. .                                                 ..                                                ,
                                                                                                                                                                                                                                      .. . ..l..                                                                                                                        j
                                                                                     ,                                              ;                                                               ,a.                                                     . ;                                                                                                         ,
gs.
i                                                                                                    .
                                                                                                          -           .                                                                                ..                                                    .                                                    .                                                     r
                                  ..:.                                               :                                .             :                          ., .                          .i.. i. i..
                                                                                                                                                                                                                                                                                                                          / canexigsoaseeico /
j, p
l                     ,                                     ! ;.i.i *
                                                                                                                                                                                                                                            /                                                                              / M ene.'gbs3e,                             q.i 3
: t. v F-g i;
                                                                                                                                                                                                 .i! j.
                                                                                                                                                                                                                                        /                                  .
s g w.gss                                         I s
4,%.h
                                                                                                                                                               ;: :.                       . l;' f :.
r
       ,                i                                                                                  .          ..'.:
                                                                                                                                                                ,1:
* sg:
                                                                                                                                                                                    .                         I             .-
ll                                                          .
j::: - ; . j-:r-ll:.:
                                                                                                                             ; g --j ; -j-:'.:.- -l
                 ,                   ;::.                              .'                                                 ;ll:::;
                                                                                                                                                                                                                                                                                         .!                       l .'          in. is hes g ,..p 7J.                                g                                                                                             ,                                       ,                                              ,
                                 . ,                                                  i                    .               . .             ....
                                                                                                                                                                .l,,.                     $                                 ..                                                                          .         ..
3.,                                                                                                                ..           ..                   ;               ..               ...                 . ..                                                                               .         .                                                           ,
l.
07                                                                              .           ..
4:                     ...
                                                                                                                                                                                                                                      ; i.                                    .
                                                                                                                                             .i.
i,jg.,..;.!
                           }gv.                                                                            :..                                                                                                                                           ,. .
                                                                             -.                       -                                       .:.               i.;...          .
                                                                                                                                                                                                              .l..ii
         -0                                                                           g.. .                                                                                                                                              g,.                                                                                                                  .                   .
                                                                                                                                                                !gi t                                       -l...,                                                                                       ,.                                                               3 g p p(:                                                                                                                       .-
                                                                                                                                                                                                                                                                                    .                         i
                         .g                                                    .                                                                                     .                                                                                                   .
N
                                                                                                                                                                                                                                      ~ '
L' c,0                                                  jii-                                                                                                                                               [~
                                                                                                                                                                                         /                                       .
t
:-                                                       7y.:                                                                       .
Aun .twa (uns
                                                                                                                                                                                                                                                                      /                                  . .
i
                                                                                                                                                                                                                                                                                                                                               /                          \..
j                            '
                                                  .tf                                                                                                                                                 Ru useArs                                                                                                                                                              .
                                                                                         ,l Caoone;nr sket l                                                                                                                                                                                                                                                                                                                                                               ;;
                                                                                                                                                                                                    .Srass Gescesds                                                                                                                                t
                                                                                                                                                                                                   / mnf occur                                                                                                                               /           /r               i.
                                                                                                                                                                                             /////J'
  >                           -                                                                                                                                                                                                                                        /                                              / /         ///4                                    %
0                                                                                                                                                                  so .:                                                                                                                        6ot              [
             .\                                                                    lo                               to                             3c.                                      40                                                                         to                          - 7o                        so
                                                                                                                                                                                                                                                                            .                                 i.                                                          j:
                              ; .           .                                                                                                                                                                                                                               .                                 i.
r% wwds.                                                    (mm)                                             !
                                                                                                                                                                                                                                                                                                                                  .Q                                   ]..
                                                         .]                                                                                                                                     .J i                                                          ,
: u.            -(a.
                                                                                                                                                                                                                                                                                  .       - .                                       a.. .                   .     .
                                                                                                                                                                                                                                                                                                                                                                      .llv.g
  ,)                                                t

1
              ; . ., , - _                                                         , ~ -                                         .._-..-.
                                                            ~- ,
y+,                             ;.                ,
    .u .:n .         .e. m . 2 .
:,.             . ,gjg. g. hdMa
* iM>
* t 2 Ma ema.a. , .i1n O.
                                                                                                                                                                                                               .a TXI-4201 06/22/84                                                                                                                    .
l Allegation No. 8 4
,                            Paragraph 4.1.3 of Procedure Number CCF-30. Rev. 11, states: " .. shadows or                                                              .
tight residue of primer which may remain in the profile of the previously 4
prepared substrate is acceptable." The allegation questions the integrity of an
                                                                                                                                                           ~
inorganic sinc primer which has been applied over a steel substrate with metallic sine residue in the profile of the steel. The concern is th'at there will be coating adhesion problems, and that the zinc is isolated from the carbon steel substrate; thus the necessary galvanic action will fail to occur.
Evaluation of Validity This allegation is without technical significance. Multi coats of inorganic zine primers have basa DBA qualified.                                                 (See Carboline Testing Project Report 01978.1 Final Report, attached, and response to Allegation No. 9). The DBA tests for CZ-11/CZ-11 systems indicated no failures in delmaination, peeling, cracking or blistering. There is no question as to the ability of CZ-11 to adhere to a steel substrate, and the attached DBA test results indicate that CZ-11 will adhere acceptably to previously applied CZ-11. Therefore, the concern relative to CZ-11 adhering to a steel substrate with tight residue of primer is unwarranted.
9 Safety Sianificance None j
Generic Implications on Other Systems or Contractors Not Applicable 4                                                                    y e-          . . _ --     ,.. _.m.     --- -. - _ . - . .      .__...w.,.my_,._.          _ _ - , . - - . -   -..r..,_._.,me,-
                                                                                                                                          ,,.____,.4 m,-,.   ,m-,,,,,,   - . - , . . , - -...,,,nw. - - ..r------

                                       ,.                                                         . ...                                            . . .                                                                                                                          * . . ,s..
                                                                                                                                                                                                                                             .,,    . _ ._m
                                                                                                                                              ~, ;;; .' *i~..,.,.',k.
       .... ._.                                                              ....a..; u-. .! . - 1 '
                                                                                                                                                                                                     =
                                                                                                                                                                                                                                                                                      .                                                      .a                  ,
                                                                                                                       .J.                                                               2.a.i. ~                                 ,              . . _                     _ . . .          ..-.....-.:u....                                               -
7              s                 _. g,., g. .,
                                                                                                                                                       > ,=
  ;6..iL~.*       - .
                                        - +- i .. .n .,
                                                                                                                         .        e.gw.                                           ...%~u.              ..
                                                                                                                                                                                                                     .n. m.....
                                                                                                                                                                                                                                  . n m:w---;.amt                              - =, :w. .w. w+                             .v...
a... . .- . .. . y. . . . e , . s. ..
                                 . . 9t . .. ,. . .=. ----'S
                                                                                                                                                                            } LABORATORY' TEST REPORT                                                                                                                                y u                                                           ,.                       .
                                                                                                                                                       . ,., ,. m                                                                   -. . . .              .rw . ..u ...., t. * . ,.,.s.                             , * -
irav 14. Isa2 1-
_0197s.1                             -
m-                               Octo.
  . g.; 7.                                              twe.,: . . . .T . ; + 1. .                                                          *                                      . .
                                                                                                                                                                                                          . .                  s i :.* h                . . . . . .               as..
  .          .                    ..                ~=**:                             ...                                              e.         ..- . .
  .                   g , Final                                                            Tlrne 7 d878                                                                                            Octs of GracBrg. December 22, 1981
                                                                     .               .u.-                          .
l Tm Dodgn Test W 7 davs                                                                                         .                          ,.
Roquested by: tir. D. W. IfeBride-                                                                                                  .
I Performance of Carbo Zinc 11 Systems I.xposed to 340*F Bechtel                                                                                                                                                           '
Tm.E: CP956-2/76 10CA Curve.                                                                                                      ..~
The purpose 'oh this~testbg p oject is to em                                                                                                                                                 nehowvabious                                                            [-
Carbo Zinc.11 systems will perfor:s in the-upcoming.340*F Bechtel CP956-2/76                                                                                                                                                                                                                         -
                 . IOCA Curve tests at Oak Ridge National Laboratory. scheduled for early 1982.
The systems to be tested are:                                                                                                                 .
i
: 1.                Ic Carbo Zinc 11.6 3 mils                                                                                                      -
                                                                                                                                                                                                       ~ ...                                                                         .
: 2. Ic Carbo Zinc 11 8 6 mils                                                                                                                                                                     ,
                                   .   ..'3. 2c Carbo Zi.nc 11 8 3/2 mils                                                                                                                                  -
4
: 4. 3e Carbo-Zine 116 5/2/2 mils
: 5. 3c Carbo Zinc 11 6 3/2/2 mils                                                                                                                 ,
                                      . . 6., .1c Carbo Wald 11/le. Carbo Zine 11 S.I.5/3.0: mils                                                                                                              '
                                                                         . a ;; . %. . H '                                                        .r. ... ..                           .
                                                                                                                                                                                                                                           ,                                                    .                          n ComN                                            pi,,,, ,,f,,                                             to d oisse,
                                                                                                                                         .          . . . ..                                                    . . . .                                        .,         .                   q
                                                                .       ,.s.
                                                                          .                               v..,.,.                                     .                                                  .                                                                                                                                       -
                                                                                                  , .. e. ..                 :                    ,         .                         .
                                                                                                          .                                               .                                               .;                                           r...                   . .
s.
                                                                                                                                                      . .                t t                                                                                                 .           .              ,,
l 1
i                                                                               .                                                                                                                                        .                                                          .
1                                      .
                                                                                                        .                .. s. .
DISCUSSICN:                         -
                                             . ..... ... :.. r....2. ,. u,u.
                                                                                                                                    .,.r
                                                                                                                       -.. . :. . .n...-
                                                                                                                                                                                                                                                                                                               .. " . ;y
                                                                                                                                                                                                                                                                                                         -,..,g-
                . ;. ..4         V. . .l:9. .. .i.E.. :.d:. '.,::                               .
                                                                                                     .. 4.M - se. .:. s. ..                                      .  .:.r^:
                                                                                                                                                                                           ... .. .. ,./;. :-:z            :.     .  ::'L:-
                                                                                                                                                                                                                          .,... ~c; n: ..             ::    .    .    %. >,    ..      r......R.    -
                       . . . . . s .: y g.:.                     .. e u>..m           .
                                                                                                                                                                                                                                      .; i r,- Q q .*              ?. i
                                                                                                                                                                                                                                                                                        . -' 8: . . ;**. ca s.. r ..:. i
: 4. Q :. : ::?' v'E q. ,aiQ,: .. . .T.% .h''';5                                                                                 .~ ~:.i11.:::eLu                                                      ,A%;;.s w':;f.al;,,~:*@?c.m,.                                                                   .~-;*
                                                                                                                                                                                                                                                                                                                                   ..: , i{., l
              . . * .~                         .
                                                                                                                                                                                                                                                                                 ..;f      -     *.-                     '
     . :.                                                                 ,                                                                                                                                                                                                                                       .    +'-
                       .o                                                                                                                                                                  ev/.-3QC                                                         g ""~":
W' '                                                                                                                                                                                                                                                                                                                                    . w. '
1
                                                                                                                                                                                                                                                                                                                                             .g. ::,
     %%& _.                                                                          b #18 CarbOGrie esecrCh        :___-_                                                                                - - ~ -                           _ .
8t. Develcptrierv t.d n uivif. = .
R: y -.- tesvamm esmasnanna m Teono
                                                                                                                 ~ z.nocmasure                      . . an ein ant er ow % .t ::= mpe         _ a. .                       ..?-
g
                                                                                                                                                                                                                           $ ' ? ?~
                                                                                                                                                                                                                                                                                                          ~
m

x.; :'
: m. '. .Q;i 4 .x;v.-; W, ,___.,                                                           .* %
                                                                                                                                                                                     , 'm , . .
                    .                       ,          c                          ;                                                                9 a.V                    .
                                                                                                                                                                                                    '.                              . f.__5, m. . . _,      ._
                                                                                                         ..-                     .                                                               .        .                   i          .
        ? 4--5 Testing ProjectiF01978.1.- .
                                                                                                                                   .      .                  ~ '.' '.'"- -' '-y May- 14..iS82.~ ' ~~'.T*f?
  , , . '.,,.'.' Final Beport:                                 7' Days-Page:2..ig..,
                                                                                                                                                                                                                                            .    .3 u,.
                                   - A.           Test Coupons                                                                       -
: j. '
J.
i::
w.,;                       ..                  .-                                                            .
                                                                                                                                                                                                       .7 %. y . . .?--                   .

== Description:==
2x4x1/4 steel panels conforming to Carboline Specification
* ST1.(See. Appendix 1)                                                                                                                  ..
Surface Preparation: Gritblasted to SSPC-SP 10-63 with a 1.0-3.'0: mil profi] e .g
   .                                           . Abrasive liedium 50/50 mix of GTH #40 grit and 5230 shot.. -                                                                                                  .
Note: Before priming, the coupons were vapor degreased.                                                                                                      -
B.           Systaes Testad                                                   e
                                                                                                                                                                                               .                   Dry Film System                                                                      -                                                                                   N"=4ng Thickness Number                   Coatina System                                         Color                  Batch No.                               Th4nner Ratio                                   Ranze
: 1.                  Ic Carbo Zine 11                                    ' green                  A: 1E5640M                                    f33 -                  10% 3.0-3.3 mils'
                                                                                                        '0300                   B: IE23882                               1A2473M
: 2.                  Ic Carbo Zinc 11                                        green                A: 1E5640M                                    f33                    10% 6.2-7.3 mils 0300                 B: 1E2388Z                                1A2473M                                 .
: 3.                  Ic Carbo Zinc 11                                        green                A: 0J5543M                                    #33                     12% 3.1-3.4 mils 0300                 B: 9E16832                               CD3885M                                    -
Ic. Carbo Zine 11                                    ' green                 A: 1E5640M                         '
: f33                    50%         1.6-2.8 mils
                                       .         .                                                         0300                 B: 1E2388Z                                IID964M
                                                                                                 ~
                        .      4.                  Ic carbo Zinc 11                                        green                A: IE3640M                           ..
f33                     10% 6.4-7.0 mils
               )..
0300                 B: 1E2388I                               1A2473M Ic Carbo Zinc 11                                        3reen                A: II5640M                                    #33                    5C% 1.9-2.5 mils 0300                 B: 1E2388Z                                1A2473M
,                                                  Ic Carbo Zinc 11                                        green                A: 1E5640M                                    f33                    50% 3.5 mils 0300                 3: IE23882                                1A2473M 1
: 5.                   Ic carbo Zine 11                                       green                A: 0J5543M                                    f33                     12% 2.8-3.3 mils 0300                 B: 9E1683Z                                CD3885M Ic Carbo Zine 11                                        green                A: 1E3640M                                    f33                     50%        1.6-2.0 nr41 r 0300                 B:'1E2388Z                                IT0964M Ic Carbo Zinc 11                                       greed                A: IE5640M                                     #33                    50%         1.7-2.0 ni41=
0300                 B: 1E2388Z                                 170964M                                         -
6.
ic Carbo Weld 11                                       gray                 A: CH2879M                                     #33                       5% 1.7 mils 0700                 B: 1E23882       ,
1A2473M.
i                                                   Ic Carbo Zinc 11                                        green               A: 1E5640M                                     f33                    50% 3.0-3.5 mils
                                                                                                         '0300                  B: 1E2388Z                                 1A2473M
                                              < .. :'.,..;....'                              ..., .Y
                                                                                                                                                                            .'        '.        :, . s
                                                                                                                                                                                                       .,,.<.. ,- .Q:.~.a
                                                                                                                                                                                                                         . . . ,, . 3. .. ..:f.~,
                                                                                                                                                                                                                                                           -- y
     , . [. .
s;                                                                ,..                                                  -
a...             r....*                    ...
                                                                                                       *,,.=
r,
                                                                                                                                                                                                                 ....3
                                                                                                                                                                                                         .. y .*...*  .         s.    ' '*         n.  .. ,
                                                                                                                                                                                                                                                          ~. .
l
: j.                                                                      .

7q .f f.; t- _                                                                                      -                            s                            ..            7,a .             -
q             ..:,<                ;g.:        .1. y .y4. ; , , . _ , , . s .. . .
4     . Q. i -
                                                                .'   --r :-- .
                                                                                                                                                                                                   . .                           . . . . ,             . ...               i .' _"-* ~.            _
                                                                                            -           - - --   .._              .,:.=
(, y . 1 l' - ~ ' ; - : - .. . ~ - -r        -
                                                                                     ~
                                                                                    =.                  G i_;_.. ..                       . ?a: ::.:. u; :- :~a --_
                                                                                                                                                                                                                  ".,g_.         .                 .
                       'TesEing. Project:?01978.1@' - * "??,@9 " ? ' ;y;h*"p                                                                                                                           , ~'O~ ,1 liay 14,1982.
I'* . ~                                                                                                                                                                                *    . '  -   ~
  .i.""
Final           Repcrt: .T Days. 5.*c., , , ' ' . .~.'. ;~c' .u - ... . -
Pase 3 g                    ,
   ?-              r                                             .        . .>-.:-
                                                                                                                                           ..-..m.               .
                                                                                                                                                                              . .e. ..
                                                                                                                                                                                                                                                                             )
                                                                                                                                                                                             - ,-                                           .                              t
   . Q., L.F.(                        .                        . . .
                                                                                                                                                                                 ~                  '
  ,,    p.v.-
C. .. Cure Schedule System -                                                                                                                                        Temperature                              Humidity Number                           Coatina System                                                              ~ime                                         Range                                  Rante-                                                            '
: 1.                   - .2c carbe Zine II.                                                              2 aanths,                                  22-83*T                                    21-97%
2 weeks
                                                    . Ic Carbo Zinc 11                                                                 7 months,                              ~22-83*T                                      21-97%                                                                          j 2.
i veeks
: 3.                            Ic carbo Zine 11 7 sonths,                                  21-91*T                                   10-97%                           .
                                    .                                                                                              12 days                                                                                           .
Ic Carbo Zinc 11                                                           2 months,                                 22-83*T                                    21-97%
           -                                                                                                                       16 days .
: 4.                           Ic Carbo Zinc 11                                                           1 month                                    26-86*T                                   21-97%
Ic Carbo Zinc 11                                                      24 hours                                        70-76*T                                   39-41%                                                          .
Ic Carbo Zinc 11                                                       34 days                                        22-69'T                                   28-97%
                                                                                                                                                                                                                ~                                   ~
                                                                                                                    '~
5.--                          Ic Carbo Zine 11                                                          7 modthsT ~ ''21-91*T'                                                            .10-97%                                                               .
12 days                                                                    '
75-79'T
                                                                                                                     '                                           ~
             -                                   .,.IciCarboZinc.11
* 2- hours                          g3                                                     55-60%
                                                           '1c Carbo Zinc 11                                                           2 =onths,                         .        22-83*T-                                  21-97%.
f.,
15 iays                       -.'-.
        %-                     6.                           Ic Carbo Wald 11                                                           2 weeks                              . 28-69'T                                       29-97%
                                           .              ,Ic carbo Zinc 11                                                        20 days                       -
                                                                                                                                                                        '. 22-68*T                       ,
                                                                                                                                                                                                                         , 28-97%                                              -
j D.             Ernosure                                                                 .
Bechtel CP956 (2/767 Luca he 1        Time-Temperature-Press:re curve                                                                                                                   -
Time Ta sersture*                                                          Pressure *
* Initial                                                                                     i-lient                                                               Ambient                        -
Initial to 6 hours
* 3-2*F (171*C)                                                          70 psig                    '
6 hours to 96 hours                                                          -
2!?T (121*C)                                                           30 psig                                             -
96 hours to 7 days                                                .                         2 3*F (93*C)                                                           10 psig
                                                            *These are theoretical val:ss. The next page are graphs of the theoretical and actual DCA temperature and pressure enzves. The data for the z:tual LOCA curves are from the chart. recording for this ts.st, found on page 97, Lab . Book #230.
             .                        .-                    2. Vater thhtry                                  ..                                   .
                                                                                                           ~                                                                              .                                                                       ,
                              ,*                  .                                                                                                                            ..                           ..~
l Deion'            i zed vater pH = 7.2 ...,                                                     E. - -                                              . ...
                                                                                                                                                                                                                             .           .~ . .                     '                                    -
                        .. . . . .            .$... i's.%     . .Q.R.j. ' ;4?E *r: -    -
                                                                                         ~
                                                                                                                                              - ' 6: h ;=%. :. . .i ' u .. '~''I                                '
                                                                                                                                                                                                                                               ? ~ ~.      '
                                                                                                                                                                                                                                                                     .' . ,],'                           -
                             . ;.; ,Noce: j'.A' ll test pa'nels were sus;a:ded in;theNapoe' phase                                                                                                                       of test. . , '
("~ .'                                                                                                                                                                                                 - ,                                        ..,                 .
                                                                         . . . ~ . -
                             . n .' h.,..
                                                              * .=3  p t: -. g.;.....;w m. : ~: ,.Q 4.:;.;.::-wq .c .M...,.... ..:. ,...:,. .. .. :..-
                                                    . y.                                                                                               .                                                                                                                  .                  .
                      . b. ~"'' r                                           5                                                           MM                                                                      :+ . h_                        . . . _.                : :.kh -I n~ .t .? W h % M- m e m g ij a i m $ s) ,mW
_ -. __ m                                                 _
Y7'N.-                              .J%'~ j
                                                                                                               '                        ~
       .5,                           ? .A .' ' ~                                                                                                   _ _ ,                                        Zj                             3 f[; "' M

                                                           ,. ,                     . , . . . . . . .                      ,                                  ,_. -                       , . . ,               _                       _ _                      . . .,,_s      .
       ,m,~.                ,..
                            ...--x.,....             _
                                                               .              r.-               y. :.y. ., .. ., ... , .:.y
                                                                                                                                                                  .                                      y                    ;.
                                                                                                                                                                                                                                                             ...,..w./..,._...,.
: 3. . . . . . . ,g .,
                                                                                                    =u_
1       w ,sv                                       4fse m ' survu                                                 -
: z:necrar.2.ca4                                                       -
a.,s           *. PROJECT # 01.9.7 8 1. .                                                           .. . .._- . . _. . . . ,. . ..                                                          ...-                                    .
                                                                                                                                                                                                                                                                             . . N                                                                                     .
arah.
                                                                                                                                                           -.M..
a                                                                                .                                                                 .
J,-400 - .                              .                    .
                                                                                  ,.c,          :e.::l .
                                                                                                                     ---m..iC.,                     ..
                                                                                                                                                                                                                                                                                                  /              ,-                                .
                                                                                                                          ... - ,.. -                                 ...n.
,   s 4-
                                                                                                                                        /=                       . - ~ ~
                 .s.
                                                                                                                                  ./                                                                                                                   .
n s                                    .                 .                                                                                                         '
   .)300-P.                                                      .                          -
g                                                                               1
                                                                                                                                                                                                                                                                                   ,                                 s
                                                                                                                                  ...                                                                                                                                              ------m                                                                  .
                                                                                     /                                                                                                                             ..                                                                                                                   \                                    .
                                                                               /
* I
                                                    .                   /                                     .
                                                                                                                                                                                                                                                                           .                                                            t
                            .                                       /                                                                                                                                                                                                                                                                                  -
2Q0 -                  -                       /                                                                                                       *
                                                                                                                                                                                                                                                                           .                                                                           s
<                                                      /
                        .                        /
* p /. -              -                                                                                                                                                                  .
                         .          t                  .
       - 100 -
t
* f                                                  e                                       e                                        e                                           't        *
                          .                                                    a.                                                     .                   .                .
a a                                              a
                    ,     y1                                     .
                                                                     ' 3.0'O           .
                                                                                                                     ~101..;
2 3.02 .. ... . .                   .                .. .
103                                  . 104 105                                              106 m= (seconds)                                                        .               .
: y.                       .                                               .
        ,        3g --                                                               . .
                                                                                                                                                            .         Pressure                                                                                                                                                                                 .
t                                                                                                                                                                                                                                                               .
                                                                                                                          /
                                                                                                                                                                                                                                    \                                               g   .
                                                                                                                                                                               ..-                             . . . . .                            .                               I,
                                                           .                           ..                              f.                                     ,
63 -              -              -                                                                   I                                                                       .             .
                                                                                                             ./                                                                                                     ..                         .
i                                                           -
t i                                 .
                                                                                                              /                                                        .                                                                  .                                         t
: g.                              . ..
                                            -                         -                                     l                                                                                                        .
I                  .
                                                                                                    .j                                                                              .                                   .
x                                           .
                                                                                                                                                                                                                       ,                                                            I                                                                                   .
4g -              -                                                                                     .
                                    .                                                              1
* 1 I               .
                                                                                                                                                                               ..                   s                                                                               I-j..-                                                                              ..
i
                                           . . .                              .             I                                                                                   . . . .
t                                                                                          '
                                                                                                      ..                  ..                                                     .            .. .                                                                                                                                       g                        .
t                     .                                                       .
e
                                                                                      /.              -                                                                                           .
1a - -                                                                 g                                                                                                                                                                         .
                                                                                  )
: i.                                  .        .t
                                                                                                                                                                                                      .        ..            . , . . , . . .. . . . ..... . .. . . . ~           .
                                                                                                               ..m.                                                                                                                                                                                                                          H .,.H, p*' . > .+;-l                          . i . k.. 'z. 3 . fg,.i .:.:, Q t f%h.i*.y. 2. ...: : . ' .~ ,. n. .
i                              .                                                                                                                                                        .
q.*?                                                            3 t.*?
             * .w  G.'.s                                             ,,.                                           .
a;-
3 y , ,,/                                                   .,... ;                             .,               ,: - ...
j....
                                                                                                                                                                                   ,..                       .      :.i,                                              ,       ..
                                                                                                                                                                                                                                                                                                               ,                                   . .f/ ',4,. 4

                                                            ..- ---.. ,.,..                                                  ~.,                                                                                               _                                w ._                                             .. . ._.
                             'w:..e ; :w:: r . '. - " .
        ,.             . . . . .,                                                                                                                                           s                                                                                      ~
  .:... J y.c.c.
c d.i ' ,,"_, y 4               ,
whJ         __
                                                                                                                                                                                                                                                                                                . _ 24.#.. - - <.
r.9 e
                                                                                                                                          ~-
:.w * :_                                                 ..                         :. . . . .     '
                                                                              -a-                     ---
m y.,., : Testing Pro. ject: 01978.1 ., L.
s .; ~                                                                    .
                                                                                                                       . .'.-; -rn.r.      q%.. 4 r~;-e.:<                                  _.3.:.',               .
W .9,              .
e=.?-~-
                                                                                                                                                              ,.      ..s                   .- ;                                      .
                                                                                                                                                                                                                                                       .y,T 1 Q 19g3
                                                                                                                              - . v.. T
* C ' : O ' W, . ,#                                                                        '
Page 5
                                                                                                                   > - - .- : : < : m r ~s :9 :. ""
i
  " : .T, A ygg,13,page:..g7 Days                                              . ... ..
         -                                                                                                                                                                                                                      ~ ~ . . ,
                                                                                                                                  ,.              .s                               ,.          .,                ,                        ~.
                                                                                                                                                                                                                                                                    .-                                          .) i
   ...r                                                     . . . .
a
: r.                          .. .~                   .
         ,s .
                                               '.~~-
                                                                                                                   .              IDCA Gradinst Procedure-                                                                         .
                                                                                                           .                     ..               (As m D3911-60                    .
The test coupans are examined and evaluated within 4 hours after                                                                                                                                                                                   .
removal from the test chamber for the following coating defects:.
D.1-htion - report extent.
* Cracking - report extent                                                                        .
Peeling - report. extent Blisesring - report in accordance with Asm Method. D714 Key to Svmbols in Results 3-blistering CD-coating discoloration F-few               -
Y
                                .              s G,. .                                                                                                                                                              .                           .
J'                                                                                                                                               .
(                                                                                                                                                                                                  .
I
                                                                                                                                                                                                                                                    ~
                                                                                         .~.                           -                                                         ..                                                                                                                           .
                                                                                               .                                                                  g                                  .
                                                    ..                        *                    .-               ..          .             . . ,              . . , .
* y                                     .
                                                                                                                      )*               *,=.,_;                    ,F,,.                 l         .6 ;                                                                                                 .
                                                                                                                                                                       .' * . ~ .. .i. , .~.
                                        ..                                 'T. . .                                    .*
i
: 4.                  d             ..                                                      .                                                        . .
                                                        . .r . . .
                                                                                                                                                          +
a
                                         ..J . 7,') [ JN Ylf..,: k. '.                                                                                      q.b' . . . . . .h ' '.[QY 9. '.4'-[ .7 ~ ~
              ., yd..,. .i . .
                                                                                                                               .. 1.             .:.                                                                         ,
n
                                                                                                                   .=.'-
l . . ; < *.s                   :,.J                            .
               . V .;.s .- . a:     ..
                                                                                                                                     . :. . ' - n . . '' ..;;s. . ;. ..%. .,;*                                                 % ."                                                    *
                                                                                                           . e &_.. Q. u.;M.
                                                                                                                                                                                                                                          $h2 I.$.' W % '
                                                                        .n : >&:.. Q:h'M:C"db.,-
>        .                                                                                                                                                                                  ~                            "
1ac.;
Q                                          w.~.s'*,W                                                                                                      . .-, - -
* 2. W'%T~&~~                                                                                                                                                   _
                                                                                                                                                                                                                                                                 &bt.n,~ 5e.!;;,Q;.'
                                                                                                                                                                                                                                                                                                         . ,N        l n. .
gJg, .>$ gj
_as=r              __ . _ .- -m - e _ _re r .:----r-    -
m --- M                          -
                         . __% _ %                                                                                                                               _ --- g                               :         -
                                                                                                                                                                                                                         .2                                - c                        _ % ,,,. s
__= _ K u M' M3*p$.,                                                           *) 3 L7% .                 . . . . - _ _                        _ _ . _ _ _                                                                                                                   --w M.$

                                                                                                                                                                                                                           -r            pw            ---
               -                                                                                           .                                                                                                           .                                       [d May 14, 1982
              .T2cting Proj:ct: 01978.1 i
[f Page 6                               *-
                                                                                                                                                                                                                                                                          .j p                F.in.1 Reports 7 days h                                      '
5
                                                                                                                                                                                                                                                                   )
I ' RESULTS '
j Other.N g                                i; l      i          l' .                                         -
l'erformance k   u b'
;;               Pagel Identification:                                          Dry Film                                                                                                                                                  <
4 and Coating System                                      Thickness (nils)       Delamination                           Cracking         Peellug           Blistering              CharacLaristi,cs,                                            ,{
IAg Side A Y, f h                     ,
                 *                                                            - 3.0                      none                             none          none                 none CD          -.       W i                               Ic carbo Zine 11                                                                                 .
l Y
Side B                                                                                                                                                            .              t,:                                                           I.
A none                          > CD f ,iA:
none i            Ic carbo Zinc 11                                3.3                      none                             none                                                                                                                              ,l
                                                                                                                                                                                          . .                ,            -#e h u                         '
d             ;
2A; Side A                           -                                                                                                                                                                    i            ty j                     v 7.3                                                       none          none                 none                                      CD . ,             1.6 i                      Ic Carbo Zine il                                                         none                                                                                                                                            .
f
                                                                                                                                                                                                                           .....m..                              4  s
                                                                                                                                                                                                 ' ;                       'YiIg                             1 ZA aide n                                       .
none                       8
                                                                                                                                                                                                                    . CD it FI.
l I      '       [l, '!
ii none          none I'''         ic Carbo Zine 11                               6.2                      none                                                                                                                                                          l
* l 3As side A
                                       ~
                                                                   *                       *                                   -                                                                      'N*,
f
                                                                                                                                                                                                  .. j S L
none
                 'f                                                                                                                                     none                                                                                                                 ;
Ic carbo Zinc 11                               3.4              -
none                             mone                                   ~
l l
ic Carbo Zinc 11-                              1.6                                                                                                                       ,.,
                                                 .
* 5.0                                                                                                                                    'i
                                                                                                                                                                                                                                 ,                     ],               l :i L                    3A; Side B ,'-                                                                                                              .                                                                                                                               '
(. . Ic carbo Zine 11                                     3.3                       none                             mone         none                  none      .-                 . . i. ,                           -
n
:                                                               2.6                                                                                                      ,
4,;,
                  .'[.~.iccarboZinc11
[,ff,e fi"'
                                                                                         ~
                                                                                                                                                                                                                                                      ?                      i.
      ,              333 Side A                       -
none
                            '[f Ic Cetbo Zinc 11,                                3.2                      mone                              none         none                                      . .
                                                                                                                                                                                      , q, j,, { CD ,5 i            1
                                                                                                                                                                                                                    , 'g h gg m
e l'y.}cCarboZinc11.                                   2.8                                 ', . ',                                                                                                                                                 ;
                        .         . .                                            6.                                            .
                    ,sas,_ side s 3.1                      none
                                                                                                                                               ~
none         none none
                                                                                                                                                                                           ...,f* , CD j.lg/9                      [~'-
                          .! # Ic Carbo Zine 11 l' ,, I5
                         ')'d Ic Carbo Zinc 11                                   2.0                                                                                                           ,'i.':t/;.            '''
f.- r ,          .
5.1                                                                                                                                                                                          .
I
                    . l- ' , -,           ;                                                                                          .
                                                                                                                                                                                        ;                  ii'y't i                           j                               i
          .                   -             -                                                                                                                                                                          ;.r e.
* v.
                                                                                                                                                                                                                ' J ".
g b        i's ..                 .        , .. .                                                                ,,         ,

s ..                                        ...
I' #
esf"];1978,1 h,                                '
* Nay 1471981'.;h  .:
                                                                                                                                                                                                                     .;                       i                .
r J.1 te O,.
Page 7                                  - -
      . pol.,Betertl 7 days
                                                                                                -                                                                                                     .                                     Y ''                               -
J.                    .is -
Othec                                      l
                                                                                                                                                                                                                                                       ' (.
                                                                                                                                                                                                                                                                           '       ',.).
gy - t . .                                                                                                                                                                                                                                        ::
fi~catiisi                 -
Dry Film                                       >                                                                           Performance'                                              i*                       . '
ting System :                              Thickases (mils)                 Delanimation                Cracking                  Peeling                    Blistering'        Character (stics...                                                   i       g.
d[.                                                                                                                                                                                                                                             '.3                 l W,
                                                                                                                                                                                                                                                .:e      !'                        c.;l II*
ide%A'                                                                                                                                                                                                                                                                 1.1 3 Carpegig ~ Zinc ~ll'                                                                                                                none                          none                    CD                -
6.4    .                        name                   mens
                                                                                                                                    ~
ej                         1-)
c] Ca'abe.-Zine 11'.                                   1.9                                             -
                                                                                                                                                                                                                                                                         /
2.Carbe Zinc !! ,                                      3.5                                             .
                                                                                                                                                                                                                                             , .3 ,         (            '
                                                                                                                                                                                                                                                                                   ??
                                                                                                                     -                                                                                                                                                                  ji g
LLf            g. ,. .                                 11.8                                                                                            .                       .
                                                                                                                                                                                                                                            *'i
           ~
                                                                                                                                                                                                                                                 ..,s                                      _
,! .),-,.ME      I          WJ.-              *.
[.}
3, Cgebe 2ine 11, 7.4                             Fress edge     ,       pone                     nome                         pone                    CD          , .                              ,
                                                                                                                                                                                                                                                                                             ]l 2.5                             spreading 1/2"                                                                                                                           .a,.
p:
i                 ! Carbe.stine,Il .'
3.5                -    .       sete plane prea,                                                                   .
Carbe.Zine 11                                                                                                                                                .
4 j; . '..  .
                                                             .           13.0                       -                       .         .           -
a        ...
                                                                                                                                                                                                                                             . '. i 5
                                                                                                                                                                                                                                            ~*
        .'qide.5Ah'Zine11' 1 CerFe,                                                  3'. 8                          mene                   mene
* none                         nome                     CD                                     ,!
p,gt!                                  !:
I Carbe-; Zinc.11                                        1.6                                                                                                                                         .
                                        ~
2.0        - .                                                                      -
                                                                                                                                                                                                                                                  -l!                                ..
1 Carbe Zinc *1l -
                                                                                                                                                                                                                                                .s.
g        ..
TI              .
l-
                                                                                                                                                                                                                                                                       .           '.i
                                                   .                                                                                                                                                                                                     8                              -
                                                                                                                                                                                                                                                                              )
        . Sidp*jBfg p i                            f.
nome                          mens                     CD                 -                    -
4                 1 Carbe Zine 11                                          3a3                             mene                  some                                                                                                                                                   ,
12 Carbe*2inc.11 ,.                                       1.7                                        .                                                                                                                          .l.                              !,
l                                                                                                                                                                                                                                                     .
   ,              1: Carbo Zinc 11                                         2.0                    .
:                        'h,t
                                                       .                   7.0                -
n . .,           *Mk -                                                                                                                                                                                                                                                           "'
1 i
i                 .
1 Sid6Afx. -                            .-
peas                     none
                                                                                                                                                                          ~
none                     CD                                                                  o4:
3.1                             nona                                                                                                                                                               a j'
Iq(carbeZinc11                                                                                                                                                                                          .
l 1     Carbo Zinc 11                                       2.0                                                           .
1.7
                                                                                                                                                                                                                    ..a                             sj                         !.ip
                  !!:"Carbe 21mc II                                  ,
Q.;ISitt?                    -     .                      E8     -                                                                                                                                                                                           l b i
: w.       .                                       .                                                                                                                                                                                                        .
                                  .A ;,
4,                                                                                                                                                                                                                    *
                                  <   "~                                                                                                                                                                                                                                       l le
                                      *              .                                                                                                                                                                                                                         s l 'l i        i
                                                                                                                                                                                                                                                           *.                   f''
                                                 ,.                                                                                                                                                       ~
                                                               -                                                                                                                                                                                                                 l tr e' l .'r t.
e     ,         .r i
                                   ^*:....

                                                                                                                                                                                .             .                        .                . .        . . . .     .         .=.. . . a .                               ..
                                                                                                                                                                                                                                                                                                                                   .g s, d
                                                                                                                                                                                                                ~
u.y a, n / l. j.h(!"3
     @i@hn.1 -                          i.._.,,.
fh-
                                                                                                                                                                                                                             .              e. e .                                .          . . . ..                        u      .:,
: 5. v..:: .                                                                                       .            .                                           .                                                                             . . ...
I pV,g..                                                                                                                                                                                                                      .,,:                         ' . , , , .t I,..,-.                                                                                                                                                                                                                                         ,         g
        .                  .                                                                                                                                                                                                                                                                     .s
                                                                                                                                                                                                                                                                                                   .i; .$    ;4 .V
                                               ' i .-i. . - .                   -                                                                                                         -
Other             . . .
rea. c. . #q.
it.u ..                                      .cr rum                                                                                     .
l g                ting,3yst.m ,,g                                           Thickness (alls)                           Delaminatise                .       .,
Cracking -                          Peeling         Blistaring            Cha racteristics '.'.                                     ,
                                                                                                                                                                                                                                                                                                                       ,4             , .;
                                                ..                                                                                                                                  ..                                                                                                         . . -. f 1,                     f t:
 ,   p .ted{n                                  yp ,,,. .                                                                                    .
                                                                                                                                                                                                                                                                                                          ,,3                         7 le b Ce . Zinc-11                                                       .       2.8 .                                       mese                                        some -                        none               #2F-R CD
                                                                                                                                                                                                                                                                                                         )s' )ll!                  .
carbe Elec 11                                  -
                                                                                       . 2.3                                                                                                                                                                                -                                          -
1.1 Ic j . ' s,'! (F, :
i                                                                                                                                                                                                                                         .
ledCarbe Zinc 11                                                             - 2.s                                                                                                                                                                                           .
: ..~. ,                                    a                                                                                       .
c,.
a e
                                                                                                                                                                                                                                                                                                           ;~
          "'t!!!N."Pii-
                                                                                         -i.1 3.s .
e
                                                                                                                                                               ~
L                    ..
e                e                        C.
t s:y9.-
C.r.o,. u.a. u ,.
                                                                                           <,                                                                                                                                                                                                           .s.
: f.                   i                                                                                                                                                                         .,                                                                     ;-          i
                                                                                                                                                                                                                                                                                                                                     , ) s sidelt m*~.                                    .. ..                                                                                                                                              -            -
i,,                       y:
I              e cerYe' lield 11-1.7                            -
Free edge                                    mene                          sene              some                         CB                            ,' j        l*               (        .7 c Cerbe*Iloc 11                                                             3.5             -
_-            spreading 1/2"                                                ,
                                                                                                                                                                                                                                                                       .                    , "[.j,8                 ,
h,. .
                                             $,-                                        . 5.2                  -       -
este plass                                 -         .-
:            . e t, ,            g.,                      ,7,;
                                                                                                               .                                                                                                                                                                                    *. ;;;                                "i ;
                                    '                                                                                ~
                                                ; , n.s : . -                                  -
                                                                                                                                                                                                                           .                         .                                            ,-       l-    ,
                                                 *n ssl s .
s
                                                                                                                                                               .s -.
i_         *
                                                                                                                                                                                                                                                                                                ,   " }2_.           ,
Y i; '
               .                            P. .; :-
e.
:i                        > ;,
                                                        . . - -                                                                                                                                                                                                                                                                -!           1t
                                                   ~
                 \
                                               'i             -
                                                                                                                                                                                                                                                                                                            .g*i p<
                                                                                                                                                                                                                                                                                                                                       .+
s                    -
                                                                                                                                                                                                                                                                                                            .(    es                    ,
                                                                    =                                                                                                                                                                                                                                               ..                 a l                  ,.
A
                          , .           d.-
                                                                                                                                                           .                                                                                                     .                                      s!                              ..
x:                                                                                                                                                                                                                                        -                                                 a.
j$          .g-                  :                                                                                                                                                                                                                                                        .
t        -
g q           g.
4-                                                                                                                                                        .
                                                                                                                                                                                                                                                                                                                         ,!i
                                   .y~                                                                                                                                                                                                                                                                                          ,
t              <
                                                                                                                                                                                                                                  .                                                                                                  's; 1              ,
1 I,,g                                           .-
* i
                         ,r             ,;.                        -;                                        -
                                                                                                                                                                                                                                                                                     .                                           j r                     ..                 2
  +                           >
                                       ~=.
f,

                                                                                                                                 ..y.                            ,- .
    ~.g....             m..,...,e....                                           ,y.                        .
: e. 6 ; c.. .s...                      .., . w , b .;. j. .. , .4.w,.3. :,s. s , . . ,.. . . re ,, ., , .
                                                                                                                                             . , .                           e..my . v,.             ..s   .
                                                                                                                                                                                                                                                  .                                                                                    .                       r,
: -**9. a t .-.
w...c p. .g... .. .,.. .'. .s.r., . . . .n .,. . . a . .
                                                                                                                                                                                                                                                . : , ' .n . . .                               .            ...                                   ...,,.m._
in.y si, .'Isas.,
    ~*                                                                                                                                                                                                                                                        .                                                                                ..
                      '.''") rina n. port:Teeiin                                      7 n.rs
                                                                                                                            .c 'rrojecti'    .--- ::'.w. ._.3..P.? .: -
                                                                                                                                                                           "02s7s.'t.:" F-4'~F.TPM'.iV'!                                            .
rase s                                              -            ..
                                                . .                         .......                          . . . . . .                           . _._w                                                      . - . .                               ..                   ;                . ..
                                                                                                                                                                                                                                                                            ;-                                                                        .3               -
          +' .f..
                                                                                                                                                                                                         .-                                                                                                                                ~
                                                                                                                                                        .,...~ . p .'r.
1                                                                                          .
s.L                                          .
                                                                                                                                                                                                                                                                             , ' . . . ..                                                    s      .
                                                                                                                                                                                                                                                                                                                                                               -/
i,.f.                                         ,
1 Robert M. Resis                                                                                    Yuly Korobov                                                                    .
John Montle I.ab Technician                                                                                    Supervisor                                                                                    Vica President
              .                       Testing Department                                                                                  Testing Department                                                                            Technology
                                                                                                                                        - -                                                    'n                    . .;                               ;
bic/T.P. 01978.1/                                                                                                                                                      ,
052682                                              .,                                                           .....             .
ect            S. I.opata/D. Forthouse/J. Montle/E. Ski 14s/                                                                                                                                ,
S. Stainberg/C. Hanson/D. Mc3 ride /                                                                                                ,
N. Dugan/ Group I.saders ,                                                                                             .
                                                                                                                                                 's i                                    .                   .                                               .                       .,                                            .
V .*
                                                                            *..r                     ..                                   .;u
                                                                                                                                                               . . * . , . i . g . . . * ; ..                                                                                   4              .
                              .,                                 ,.=, ,,,. . . . . 7 .. :. . .                                                                                               ~*
                                                                                                                                                 .                               s                       .
w                                                                                                                                                                                                                                                                             e 1                                                                                                                                                                                                                                                                   .
r;           .
                                                                                                                               . . , ...                                                                                                                           ... 2..                     .
J
                                                                                                                                                                                                         .          .                                     .. .. .. . ...e...
\
1
                                                                ...'          .,.c *; ,: , & t f.; ** ,J . . .. .i e' Lt:* n .tL.*Zy,,. q. s t y. . .:.:: .v~.s                                                                                                                                 ,
s             . . :. .  ,
                                                                                                                                                                                                                                                                                    's * ' . .'..a
              "~
* h ;<:.*:' + 9 va,,:D                                                                                                                                                    , .' < ..s
* i .I i a L * ;
       . 3.,              s.
                                                               ...W...                       u             .
1 w . f . sr.L, ,,:
                                                                                                                                       $ hn. ~ .Q. p:.:.'p                               o                 t'?.t .. 3.-. '.' .. ... .. ...                                     ". .' ' '. . .   .....,.                           4. r.         ..                          ;
                                                     ,,s.               .      .   .       h.             .      .s   w.,..          .     .s         . :X
                                                                                                                                                         ... a. .:=          . . 4..f..
                                                                                                     -.>m.                                                                                ?
                                 ..+..,                                               .    . .
r    L,       .a,              . .,a,sv..'
: s.                 n       .
                                                                                                                                                             ~_.      a.   ,,                            . .;..
                                                                                                                                                                                 ,,y. ,, 3. g. , .. ..r.,.,.,.
r                                                    .'7:           .
W W N&M*I.7                          $ *t1Y.aS*k.b                                          t*WWW b..=
                                                                                      .                                                                                                                      ~
n
                                                                                                                                                                                                                                                                                                                       +cfw'5W%:&
                            -                                                                                                                                                                                                                                                                                                                                     :P *
                                                                                                                                                                                                                                                                        ~M%ad',1                                      -.4. . k.:.Wy                               .%,
                                                                                                                                                                                                                                                                                                                                                 > Ap p.
h                                                         M            q
: a.                      s           WiW                                       7'"^' M~

                                                                                                                                                                  ,,.g
                                                                                                                                                                                                    . ,3 3, , .3.. , ,-
y                            _ y., y.x, ,.. . g
                                                                                                               .                                                               g .. . . . . .
                                                                                                                                                                                                                                                                                  ., e , ,, g ,
  -, ..eu. m ....~.p._..o..
r.mpa.g}..
   .                                       .:wyy , .: i . .: .:                 .
                                                                                 .<. ,.w.n ..:._.n..w.
y- m                       ;;.g. g.; g;: .,. p. . ;,                   _           .
                                                                                                                                                                                                                                 ._4                                          , ._ _ _ . _ . . _ .
n                .
                                           ---m=--,.:,_..-                                   .
a
:g.                                                                         ...                              .                                .
                                                                                                                         ...n..                                                                               .
: s. .
M.~."-~..7 . ]~ Hay 14,1982
                                                 < . . . + w.2 r..w.                                                                                                                                                                                                                                                                                              .
E g.,ypresting Projecer . 01978.1.'                                        Days. .y ; .; . 9
: . 7. .,, , C.*.*_* , y.C.
                                                                                                                                                                                                                       "., Page 14                               -
                                                                                                        .                                   , ,, .; Ql,,                      .                 e,;f, ~                                                          ,
Ni.T_. Final.Repo . p
                                                                                                                                                                                                                                                                                            )
g ,.                                    *'
              ~ ' -.  .                                         .     ..
                                                                                                             ..             ..       gypygg 1                                                                                                                                                     .
: w.                                                         .
Carboline Saecifiention C31                                                                                                                                                                                                                                    ,
Preparation af Concrete Soecimens.
                                                    ' concrete composition Cement,AST5f'                         , Type II. I,ow alkali Gravel, ASTN C33, size 3/8 inch                                                                                                                                      .
Sand, ASTM C33                                                                                                                                        <                                     -
Water reducing ad=4*"' e-
* Air entraining admixE.gre,,                                   ASTMASTM       C260                 C494 Pozzolans, ASTH C618 Water                                 distilled         - D-=4nas-=14-ed water (o
                                                    . Concrete Precortions
                                                                                        ~                                                                            .
Cement, 7 sacks per cubic yard
-                                                       Sand-Gravel ratio, 55 sand, 45' travel by volume Pozzolans, to 15 percent replacesenc.of cement
                             -                          Ai.r entraining admixture, 4-7 percent                                                                                        ,
                                                                                                                                                                                                                                              ~
WetEE' reducing ad=4*m, as per ==nnfacturer's instructions
                                                                                                                                                                                                                                           '[,,.['
Water .to produce a 3 inch slump./                                                           x                                               .
j                   \,
Precaration of Test Spec 4=en:./                                                                   '\.s
        . q.                                                                                                               .<          .
Make and cure the specimen'according to ASTH C192, except that no form oils may be.used. . The face to be.rtasted. shall be composed to the form to s4mn1=te poured valls and the voo'd traveled surfaces:'. Broom finish top surface to simulate floors. No , test face shall be saw cut. M2en applicable, concrete enring agents compatible with the coating systes shall be used.   .                                                                1                                                                                 '
Panels:                                                                                                                              \          .
The size for concrete p=nelt shall be 2 by 4 inches by 2 inches thick i 0.2 s
inches.                                                                                                -                                                  \
Curine Time:
Before concrete spee4=-" are coated, they shall be cured a minimum of 28 days in accordance vit.h ACI 301, " Specifications for Structural Concrete for Buildings." If a concrete curing primer is used, it shall be applied on the concrete within 24 hours after removal of the forms.                                .
                                                       . Carboline SoecifieAtion STI                                                             .',,-
                                                                                                                                                                                  -                         2~.
                                                        . Steel Test Soecirxus                                                                                              -
                .            . ~
                                                                                                                                                                        ,.b'                 .-
                                                                                                                                                                                                                . . . -~;:_                        ._
                ~
                                              ' .. Panels: .The size for carbon steel p=nele shall be 2 by 4 inches by V, inch r.' c.                -     (.2 thick i 0.1 inches with rounded edges and- corners.I..The steel for each specimen                                                                                                                                               '                            -
                    .s    ',".y'~pshall meet the requirements of ASTE A36, " Standard Specifications for                                                                '
: "' - ~ ,T.s,2.                          ,.+h : .;;.j .s.y.
            . .c ' .y,3                   A .M.fStr.uctural . . v. < .; Steel."... _A         .#. .g.p p.:.qq.!$-     - D.-                   w.-
i ~~;.Q1ael-                             ^,'--                                        ..%    .
                                                                                                                                                                                                                                                              ..g                   g.,     ..              ,,
t91 ~ ' " _ ff-E T M f h __
                                                                                                                                                                                                                                          '.'                      .                4idh  .QW = ?;;. ?.N7.
S.5w.5:=-w. , -t.-
_ -___=._um~x-
                                                                                                    - ._%.                                        __% m-wn ,
7- uum            _
: m.        - _" n_                               -M                                             --                                                                                 M                                    ^
                                                                                                                                                                                                                                                                                                  -mf *<      $
_ - _ .__ _ _ _ _ - _ _. _ - _ . _. _ -__ _ __ m _.
_-__ . . _ . _ _                                                           __=m_                                --_ _; 3 m ,,--
___x                         ~=m m- g y ,;
w=~z : -                                                                     w             .=-w

       . y .a ib.a,k
                            .ly.,4                                              w.m....
_ y_.. ,y..: ,..
                                                                                                 , z,7,,. .y.~.,-
                                                                                         . .. .. :y,g. - ;'
                                                                                                                                        ..m...,..
                                                                                                                     " , ,. ,y : . v; y _           .,,           ,
    ;.                  Q v. !<- y:.4 m.
i.1.::4..c . . e--.-f x. . :. n.
                                                                                                               ~
_ c, a .
    ..n c
   ~,                                      ,
TZK-4201 N. .      ,
    *[
06/22/84                                                                                    .
V
   .J l
i
      - '                             Allegation No. 9 It.is alleged that three coats of inorganic zine primer have been applied at Comanche Peak to obtain the required dry film thickness. Paragraph 3.2.4 of Instruction Number QI-QP-11.4.5, Rev. 27, states: "Only two (2) overcoate shall be applied." It is alleged that this system would lack chemical attraction or
                                 . intercoat adhesion with itself. Is this three coat primer system qualified, for-eneple for environmental (irradiation) conditions and DBA conditions, under ANSI N101.2-19727 This is another example of the coatings systems not being l                        qualified.                                                                         .
Evaluation of Validity
             -                        It should be noted that the application of three coats of inorganic zine primer is fully consistent with QI-QP-11.4-5. An " overcoat" of primer is a primer coat applied over an existing coat of primer; "two overcoats" would amount to a 'tal of three coats of primer.
CCP-30 and CCP-30A are the two application procedures used at CPSES for Carboline and Amaron. inorganic zine primers, respectively. Both systems described in the two procedures are DBA qualified in accordance with ANSI N101.2 and are in accordance with the manufacturer's recommendations. Multi coats of inorganic zine have been specifically qualified by both Carboline and Amaron. (See attached Carboline Testing Project 01978.1 and 02182, Ameron Report TRC-089-03, and response to Allegation No. 8).
4 Safety Signific.ance 7
None Generic Implications on Other Systems or Contractors t
4 Not applica'ble
: e. > s;;.. ..
                                      ,i ars . . w . ' - .'
                                                                                                             '"='''''1'
                                                                                                                                                                     . . . l ~ ~ T'               ."
bi .
g j. .. .n .y. >. . ; . . <. . t - q, r :^ .- n -                        ~ ,' .>:+*            >           ' O - lY                        '
                                                                                                                                                                                                                  .* ~.
                                                                                                                                                ,        ,-.       ,                                   .   .e
                                             ~
                                              .             .,                                                         < =a                          - .                     .
                                                                                                                                                                                      ,. _., J' . ' yl ^       ,_
: 7.                     .
                                                                                  . _ . 21 v . LABORATORY TEST REPORT
                                                                                                                                                                                           ~
f              .
n                                                         . , . ,
                                                                                                                                                                                                                           .              ~\''
4                                                                                                                                                          May 14,1982 "i     Tg W Mer.                                  01978.1                                                   ~
Octe:
                                                                                                                 .- ....i.                                               ..
p , Final                              Time 7 d*75                                                                Date cf Grod.%: December 22, 1981 l                 Tote! W Test Duration 7 days -                                                     '
Requested by: Mr. D. W. McBride t                                                                                                                                -
Performance of Carbo Zine 11 Systems Exposed to 340*F Bechtel Till.E: CP956-2/76 LOCA Curve.
                                                              '                            ~
PURPOSE- The purpose of this testing project is to determine how various Carbo Zine 11 systems will perform in the upcoming 340*F Bechtel CP956-2/76
         .;                   LOCA Curve tests at Oak Ridge National Laboratory scheduled for early 1982.
The systens to be tested are:                                                                ,
: 1.       Ic Carbo Zinc 11 @ 3 mils                                                                    .
: 2.       Ic Carbo Zinc 11 9 6 mils                                                                                             ,
                                      .         3.       2c. Carbo Zinc 11 9 3/2 mils                                                             -                                                                                .
: 4.       3e Carbo Zine 11 @ 5/2/2 mils
: 5. 3c Carbo Zine 11 @ 3/2/2 mils 6.; Ic Carbo Weld 11/le Carbo Zine 11 9 1.5/3.0 mils
                       ) CONCLUSIONS: Please refer to "Results".                                                                                                                                                   >
                                                                                                                                                                                         .       v
    ,j                          -           -
                                                                         ,4..                                          .           ,,
1 l
s 4
i i                 DISCUSSION:
1 i
1 l
                                                                                                                                                                                                                ~
                                                                                                                         ~
I   .
1           !
4
(,
G i
(                                       From the Ccrboline Resecrch & Deve!cpment Lcbeiviuy                                                                                                                        j
                                                                                                                                                                                               ~
j                     1he sectnces dam asrwed are true and occurere so the test erour t.c_.w.
: h. no guarorvee et occuocy is own er improd.
                                                                                                                                                                                                     ' car *boline, I           i   -      ..    . TEST.-012480-1
                                                                                                   .._.a._._.s..._

p.iaw.9:,5::wF.:
v*
es s.. .?.cGpv..
a.5 5.; ~:.=;..vwww
                                                        . . : . . e :ws.'.7. c. . .c ~.   . .1- r.~.~.uT&mn.w-u
                                                                                                      . ...+ . , rw           N,.:.~s.9y
                                                                                                                                      .~      1
                                                                                                                                                 ;:y. ~.~ e. :r -".- ~ : n** v >    _
a r-
: a. . . _u
:s [-                                  -
    .3 ( ''
                                                                                                          ~
                               . *iesting Project: 01978.1                                 ,.                 $     .    ,
                                                                                                                               '''.,                      ,'          May-14, 1982                    *',             .
:]              .            Final Report: 7 Days                                                 ...
                                                                                                             .,'      ,. ,,                                           Page 2.
   .R 4
: r.        ...         .
                                                                                                                                                                                                     , . -)
f;                A.        Test Coupons                                                                                                                                                          ;
                                                                                        ,             ..                                          4                      .
    ''t                                          

== Description:==
2x4x1/4 steel panels conforming to Carboline Specification
    ))                                        , STI (See Appendix 1)                                                                .
                                                                                                                                          ~
:                                     Surface Preparation: Gritblasted to SSPC-SP 10-63 with a 1.0-3.0 mil profi] e'.
    ,,} 7                                         Abrasive Medium 50/50 mix of GTH #40 grit and S230 shot. -                                                                                                  ,
           ,                                      Note: Before priming, the coupons were vapor degreased.
            ',                          B.        Systems Tested i                                                                                                                                                    .
Dry Film System                                                   -
Thinning Thickness j                      Number           Coating System                                 Color            Batch No.                      Thinner Ratio                          Range 4                       1.            Ic Carbo Zinc 11                               green           A: 1E5640M                            #33             10% 3.0-3.3 mils E-                              B: 1E2388Z
                                                                                               ~0300                                             1A2473M 2                               2.            Ic Carbo Zinc 11'                              green           A: 1E5640M                            #33             10% 6.2-7.3 mils
    ~.                                                                                           0300            B: 1E2388Z                      1A2473M
:                      3.            Ic Carbo Zine Il                               green           A: 0J5543M                            #33             12% 3.1-3.4 mils j                                                                                   0300            B: 9E1683Z                      OD2S85M                                                           -
n
              .                                   Ic Carbo Zine 11                               green           A: 1E5640M                            #33            50%        1.6-2.8 mils 0300            B: IE2388Z                      IF0964M
     " 'i .
                       .rs
                         '       ~
: 4.            Ic Carbo Zine 11                               green           A: IE5640M                            #33             10% 6.4-7.0 mils
           .I          :- )                                                                      0300            B: 1E2388Z                      IA2473M                          .        .
Ic Carbo Zinc.11                               green           A: IE5640M                            f33            50% 1.9-2.5 mils 0300            B: 1E2388Z                  . 1A2473M
       . :t                                       Ic Carbo Zine 11                               green           A: 1E5640M                            #33            50% 3.5 mils 0300            B: 1E2388Z                      1A2473M
: 5.            le Carbo Zine 11                               green           A: 0J5543M                            #33             12% 2.8-3.3 mils
          .i ~
0300            B: 9E1683Z                      OD3885M
          'l j                                        Ic Carbo Zine 11                               green           A: 1E5640M                            #33            50%        1.6-2.0 mils
:                                                                                  0300            B: 1E23882                      IF0964M
              }                                   Ic Carbo Zinc 11                               green           A: 1E5640M                            #33             50%     '
1.7-2.0 mils 0300            B: 1E2388Z                      IIO964M 4
,~ .;                               6.            Ic Carbo Weld 11                               gray            A: 0H2879M                            #33              5% 1.7 mils
              ,                                                                                  0700            B: IE2388Z                      IA2473M
        .)                                        Ic Carbo Zinc 11                               green           A: IE5640M B: 1E23882
                                                                                                                                                       #33 1A2473M 50% 3.0-3.5 mils
:  .                                                                              0300 i         .
4 e
:l t
            -i,            (                                                                                                               -         '
                                                                                                                                                                                                           )
          'i i                                                      .            .          .           .

         . . 6..n.:.
: m. .:iq.+           ys ..p i n, vn,w   .
                                                                                   . . ;.qyrm-cr. : --!.-T
                                                                                                        .                    wr ; ,:--~. r-:; . w vun . <.n.y.pn:w ;;~ . . .. z
                                                                                                                                                                .                                                   ..                                                        .ns
                                                                                                                                                                                                                                                                                               . .~,- ey
                                  .y :.         -
                                                              .pn;.ar.s9my; pus -?.a.                                         .:                  w . ..w. . .. . u ..v ~ . ._.grz.. - . - w. -                                                                  1.     -       u..u . ,.        oncn       '
                                                                                                                                                                                                                                                            .,.            ;.       e..
   ^f *' ~ ~
* 1~?.                  ,
                                                                  .                 ,     , . . . .                 .                       .g             .. .   .            .v.                                   .~:                    ,        . . ?. . ;<: * : . '
: r.       . .. .'. q ,
                                                                                                                                                                                                                                                                                       ~~
3.H
* Testing Project: 01978.1                                                                           .f-
                                                                                                                                                                                                                           '? : May 14, 1982.
                                                                                                                                                                                                                               *                                              '                      'N'-
(                                Final Report: 7 Days                                                                 "' " " 7~
                                                                                                                                                                                   .                                                             Page 3 c_,         .
    ;g             ..                                                               ..<.
                                                                                                                        .                     3...           _
                                                                                                                                                                            .c ;-                                                                                                      -3:
i          c.                                                  .                                                                                                                                                                                      .                       :
    'c              Y                           C.         . Cure Schedule                                                                                                                                            .
   . ~p-                             System                                                                                                                             Temperature                                                    Humidity 1'
Number                    Coatina System                                                        "ime                                      Ranae                                                            Ranae
      . '!'                             2.            ..Ic Carbo Zine 11                                                        2 months,                                   22-83*F                                                              21-97%
2 weeks                                     -
       }i                                                                                                                                                                                                                     ,
: 2.                      Ic Carbo Zinc 11                                                 2 months,                                  22-83'F                                                              21-97%
         .                                                                                                                       2 weeks
      -l .
: 3.                      Ic Carbo Zinc 11                                                 7 months,                                  21-91*F                                                              10-97%                     .
         .                                   .                                                                                12 days t                                                                                    .                           .
l                                                         Ic Carbo Zine 11                                                2 months,                                   22-83*F                                                              21-97%
          .                                                                                                                   16 days .
          .                             4.                      Ic Carbo Zinc 11                                                 1 month                                    26-86'F                                                              21-97%
       ]';                                                      Ic Carbo Zinc 11                                              24 hours                                      70-76*F                                                              39-41%                                               .
Ic Carbo Zine 11                                              34 days                                       22-69'F                                                              28-97%
i
: 5.
* Ic Carbo Zinc 11 7 sonths, '                                21-91*F'                                                             10-97%
12 days
         .                                                     Ic carbo Zinc 11                                             -2. hours                                       75-79'T                                                              55-60%
l                                                     Ic Carbo Zine 11                                                2 months,                                   22-83*F                                                              21-97%
     "1                                                                                                                       15 iays i        h)                   6.                     Ic Carbo k' eld'11                                                2 weeks'                                   28-69'T                                                              29-97%
                                                                                                                                                                                                                                                                                                  ~
    .!                                                                                                                                                                      22-68'F Ic, Carbo Zinc 11                                              20 days                                                                                                            28-97%                                     -
                                           ~
                                                                                                                            '                            *          ~' '
N                                                                                                                  ']
Bechtel CP956~(2/76) LOCA" rve l          l                                                    1. Time-Temperature-Press :e Curve I
           '.;                                                 Time                                                              Ts=cerature*                                                                             Pressure
* k"                                        Initial i-lient                                                                                   Ambient Initial to 6 hours                                                               3-2*F (171*C)                                                                            70 psig l                                               6 hours to 96 hcurs                                                              22 'T (121'C)                                                                            30 psig l-                                              96 hours to 7 days                                                               2 3*F (93*C)                                                                              10 psig                                                           .
                                                               *These are theoretical val ss. The next page are graphs of j                                                   the theoretical and actua; ~.0CA temperature and pressure curves. The data for the z tual LOCA curves are from the
                               ~
        ..:                                                     chart recording for this tast, found on page 97, Lab Book #230.
        -s f                                                  2.                Water Chemistry Deionized water pH = 7.2 Note: All test panels were sus a ded in the vapor phase of test.                                                                                                                                                            .
                             )
4                                                                                                                                                                                                                                                  .    .               .      .
4                          .                            ... ..                    ..
I                                                                                                                 '4 1                                                                                                                                                                .
                                                                                                                                                                                                                                                                                            ).
8                                                                                                                                                   .
l
(
j.
l                                                                                                                                                                                                                                                     ,..y.           , , - - . - . . ~                 .-

                                                                                                                                                                                                               -prn.x<             - . m~ -r -                             -a.               <~~-...e..,..-n.~:-~-..
      ... .:Q       . . .
                                     ..,r w :.m~.ns ky5 ~'l._s.n?                       rhy.%.*H.iyb.%,&                                     .wi. 2Xms ny -E;&n.n.~..s.        s.mc-OvWE'.<:.. :<eg? ;A e .- ' 6: ;c~ w ~ ' ' u ' -
                                                                                 ;.+. - w.:c m                          > .a...ve.                         ..                                                                          .
                                                                                                                                                                                                                                                                                                       & ~ -l A *               --''e' M "
       ',                                                                                                   - .++ +. w-s .e v                                                -
4fso m 't.urvu                                                                   Tnacranca.r. -- ,---. -
T 7 PROJECT f01978 1
                                                                                                                                                     ..                                                                                                                                                 i                                             -
                                                                                                                                                                                                                                                                                 . Actual f
       .1 400 - - .                                            ,
                                                                                          . , w- ....i..
                                                                                                                                  ., e
                                                                                                                                           . -l: .; .'. Tementa
                                                                                                                                                                                                                                                                                                          -v'-~
                                                                               .,. .. ; ; p g                           s                            -,                                                                       .
         ,.                                                               ,*          - . . -                  .s               .                                                                                                                                                                       ,         ,
         .e.             Q                                                                                                                                                                     .                                                                                        .                                       .
Q..
a,*...
                                       ,c.
                                                     . . .v.: .~..iiv           h. .. T. i ~- , -                                2 7
                                                                                                                                                                                                          *-                                                                                  -             ~ ~ ' * ' ' ~
                                                                                                                                                                                                                                                                                                                                      ~y*?.h
                                                                             ...                                                              p                                 -- -,,_
                                                                                                                                                                                                                                    -___ 4
_/                                                                                                                                        I-
      . r"                     p ,                                    .
                                                                                                                                   /                                                                                                       -                   _.
                                                                                                                                                                                                                                                                           .1
                                                                                                                                                                                                                                                                                                                        .                  s
                                                                                                                             /                                                                                                                                                                                    .~
       -)a
         .1 200 -                 -
                                                                                                                        /              ,
                                                                                                                                                   . . . . -                                                                                                                      g                                                         .
[                                                        ,
      . s,,g                                                          .                                                                  . .                    .                 . .              .
g s                       .
           .j                                                   -
f                                           .,             .
24                                                                  /
                                                                                     /                                                                                                                                                                                                           -
I l
                  -u                                           .                                                    .                                                                                                                                                                                                           .
                 >                      -                                 /                                                                                                                                                                                           -                                             l              '
                  -                                                   /
200 - -                                                                                                                                                                                                                                                                                                 e
                                                                  /                                                                                                                                                                                                  .
                  's-               .                       /                                   -
              .'.a                                s..
                                                     /                                                                                                                                                                                                                                                              -
            .s.s                                e                                                                                                                                                         .
              ..s,.
U        .
k.100-u
                                                                                                                           ~
        ..y                                            -                                -
          .u                                                                                                -                                                          -
          -i                                                                                                                                                                                                                                                                                                     .            .
i                                                                                                                                              .
I                                           I                                              I                                   f                                        f                                         f                                   f
           ');,. . ''-                                                              a                                            1                                              4 a                                        a                                         3                                   4 s}}